20036_Morehead Street Redevelopment_Phase II ESA_2005.09.30

f/MACTEC
MACTEC PROJECT 6228-05-3103
SEPTEMBER 30, 2005
PREPARED BY:
MACTEC ENGINEERING AND CONSULTING, INC.
2801 YORKMONT ROAD
CHARLOTTE, NORTH CAROLINA
LANDMARK DEVELOPMENT PARTNERS, LLC
11220ELM LANE, SUITE 207
CHARLOTTE, NORTH CAROLINA
PREPARED FOR:
TAX PARCELS 073-243-01, 02 AND 03
CHARLOTTE, NORTH CAROLINA
REPORT OF
PHASE II ENVIRONMENTAL SITE ASSESSMENT
www.mactec.com
MACTECEngineering and Consulting, Inc.
2801 Yorkmont Road,Suite 100 •Charlotte,NC 28208 •Phone:704,357.8600 •Fax:704.357,8638
Attachment
KRHIRCF:jew
Kelly R. Hoffman
Staff Environmental Scientist
MACTEC ENGINEERING AND CONSULTING, INC.
Sincerely,
MACTEC appreciates this opportunity to assist you on this project. If you have questions, please
contact us.
MACTEC Engineering and Consulting, Inc. (MACTEC) is pleased to provide this Phase II
Environmental Site Assessment Report for the subject property. This report includes results of the
work performed in accordance with our proposal (Prop05chlt397,dated August 21, 2005). This
report includes a description of the site history, magnetometer survey, soil and ground-water
samplingand analysis,results,conclusionsandrecommendations.
Dear Mr. Starnes:
Phase II Environmental Site Assessment Report
West Morehead Parcels
Tax Parcels 073-243-01, 02 and 03
Charlotte, North Carolina
MACTEC Project 6228-05-3103
Subject:
Mr. Charles Starnes,Member
Landmark Development Partners,LLC
11220Elm Lane,Suite207
Charlotte,North Carolina28204
September 30, 2005
IIMACTEC
--1---engineering and constructing a better tomorrow
ii
A Boring Logs
B Field Procedures
C LaboratoryReport
LIST OF APPENDICES
1 Boring Location Plan
2 800West Morehead Street
3 822Wet Morehead Street
LIST OF FIGURES
1.1 Parcel Information
6.1 SoilAnalytical Summary (TPH)
6.2 SoilAnalytical Summary (Organic Compounds)
6.3 Groundwater Analytical Summary
LIST OF TABLES
TABLES
FIGURES
APPENDICES
7.0 CONCLUSIONSAND RECOMMENDATIONS 7-1
6.1 Soil Assessment.6-1
6.2 Groundwater Assessment 6-3
3.0 MAGNETOMETER SURVEY 3-1
4.0 SOIL SAMPLINGAND ANALYSIS 4-1
5.0 GROUNDWATER SAMPLING AND ANALYSIS 5-1
6.0 RESULTS 6-1
1.0 SITEINFORMATION AND HISTORY 1-1
2.0 GEOLOGY 2-1
2.1 Area Geology 2-1
2.2 Subsurface Conditions 2-1
TABLE OF CONTENTS
September 30, 2005Phase II Environmental Assessment Report
.MACTEC Project 6228-05-3103
1-1
During the Phase I Assessment,MACTEC reviewed historical documents relative to the site. Our
review of the City Directories and SanbornFire Insurance Maps indicated the site was occupied by
businesses or facilities including chemicalcompanies, used car sales, a gasoline station, automotive
repair shops, a car wash, a welding company and electrical supply companies. Specifically, the
.800West Morehead (a/kla Panther Parking) parcel was occupied by a service station until about
1965. No documentation of the removal of the petroleum storage system(s) was available for our
review. Nor was a Tank Closure Assessment Report available documenting soil sampling and
analysis relative to the former USTs, product piping and dispensers. The 1950 Sanborn Fire
Insurance Map illustrates the former UST location along Cedar Street. MACTEC concluded that
the potential exists for Underground Storage Tanks (USTs) related to past business to remain
buried at the subject site.Therefore, MACTEC recommended performance of a magnetometer
surveyto assist with the location ofburied tanks and soil and groundwater assessment at the site.
MACTEC completed a Phase I Environmental Site Assessment for the site (Project 6228-05-3103,
report dated August 4, 2004).
Tax Parcel ID No.Area Street Address
073-243-01 1.2acres 801McNinchStreet
073-243-02 0.5acre 822WestMoreheadStreet
073-243-03 0.53acre 800WestMorehead Street
Table 1.1- Parcel Information
The subject siteis located along the north side of West Morehead Street andbound by South Cedar
Street to the southeast and McNinch Street to the northwest in "Uptown Charlotte" in the city of
Charlotte, North Carolina. At the time of this assessment the subject site was occupied by three
buildings (Figure 1).The remaining areas of the site are primarily utilized for parking and are
covered with asphaltic-concrete pavement or gravel. A small wooded area of land is located on a
steepgradientthat traverses the southeasterntwoparcels of the property.
1.0 SITE INFORMATION AND mSTORY
September 30, 2005Phase II Environmental Assessment Report
MACTEC Project 6228-05-3103
1-2
The 822 West Morehead property was occupied by several chemical compames in the past.
MACTEC concluded that the potential exists for soil and/or groundwater contamination at this
parcel as aresult of the former land use.
September 30, 2005PhaseIIEnvironmental Assessment Report
MACTEC Project 6228-05-3103
2-1
The subsurface conditions encountered by the borings are discussed below and depicted
graphically on the Subsurface Profiles included in our Report of Preliminary Geotechnical
Exploration,dated September28,2005.
2.2 Subsurface Conditions
Often, the upper soils along drainage features and in floodplain areas are water-deposited (alluvial)
materials that have been eroded and washed down fromadjacenthigher ground. These alluvial soils
are usually soft and compressible, having never been consolidated by pressures in excess of their
present overburden.
The project site is located in the Piedmont Physiographic Province, an area underlain by ancient
igneous andmetamorphicrocks. The virgin soils encounteredin this area are the residual product of
in-place chemicalweatheringof rock which was similarto the rock presently underlyingthe site.In
areas not altered by erosion or disturbed by the activities of man, the typical residual soil profile
consists of clayey soilsnear the surface,where soilweatheringis more advanced, underlainby sandy
silts and silty sands. The boundary between soil and rock is not sharply defined. This transitional
zone termed "partially weathered rock" is normally found overlying the parent bedrock. Partially
weathered rock is defined, for engineering purposes, as residual material with standard penetration
resistances in excess of 100blows per foot. Weatheringis facilitatedby fractures,joints and by the
presence of less resistant rock types. Consequently, the profile of the partially weathered rock and
hard rock is quiteirregularand erratic,even over shorthorizontaldistances. Also, it is not unusualto
find lenses and boulders of hard rock and zones of partially weathered rock within the soil mantle,
well abovethe generalbedrocklevel.
2.1 Area Geology
As part of the due diligence effort, Landmark Development Partners, LLC authorized MACTEC to
complete a geotechnicalinvestigation of the site. Thepurpose of the geotechnical soil borings was
to provide subsurface data for use in the design of foundationsfor the proposed structures.
2.0 GEOLOGY
September 30, 2005Phase II Environmental Assessment Report
MACTEC Project 6228-05-3103
2-2
Auger refusal was encountered in each boring exceptB-1, B-2 and B-5B,at depths ranging from 1
to 15.5 feet. Refusal may result from boulders,lenses, ledges or layers or relatively hard rock
underlain by partially weathered rock or residual soil; refusal may also represent the surface of
relatively continuous bedrock. Core drilling procedures are required to penetrate refusal materials
and determine their character and continuity. Core drilling was beyond the scope of this
exploration.In borings B-4, B-4A, B-5, B-5A, B-6, B-7 and B-7A fill was encountered directly
above the refusal depths. Thus, the refusals in these borings may be due to rock or debris in the
fill.
Residual material hard enough to be designatedpartially weathered rock (N=100blows per foot or
better) was encountered in B-3 and B-7B, underlyingthe residual material, and extending to boring
termination depth. The depth to the top of the partially weathered rock was 12 and 9.5 feet in
borings B-3 and B-7B, respectively. The partially weathered rock was sampled as silty sand with
rock fragments.
Residual soils were encountered below the fill in B-1, B-3, B-5B and B-7B and below the alluvial
soils in B-2. These sampled residual soils generally consisted of firm to very dense silty sands.
The standard penetration resistances in these residual soils ranged from 16 to 65 blows per foot.
The soils containeda variable amount ofmicaparticles.
Alluvial soilswere encountered below the fill material in B-2 at a depth of 12feet and extending to
17feet. The sampled alluvial soils consisted of silty sand with a standard penetration resistance of
3blows per foot. The alluvial soils were wet and containedmedium sized organics.
Fill material was encountered in each boring to depths of up to 27 feet below ground level. The
sampled fillmaterial was variable and consisted of clayey silty sands, sandy clayey silts, sandy silts
and silty sands.The standard penetration resistance valuesranged from 3 blows per foot to 50/6"in
the fill. Some of the sampled fill contained concrete, asphalt, brick pieces, glass pieces and rock
fragments.
Asphalt with a thickness ranging from 1to 1.5inches was encountered in most borings, underlain
by gravel with an approximate thickness ranging from 3 to 10inches. Topsoil was encountered in
B-7B with an approximatethickness of 3 inches.
September 30, 2005PhaseIIEnvironmental Assessment Report
MACTEC Project 6228-05-3103
2-3
Groundwater was encountered in B-3 at 16 feet and B-SB at 29 feet at the time of drilling.
Groundwater was not encountered in the remaining borings at the time of drilling. After 24 hours,
the borings were checked for stabilized groundwater. Groundwater was measured at a depth of 14
feet in B-1 and 11.9 feet in B-3. Borings B-6 and B-7A were caved and dry at depths of 7.S feet
and 6.9 feet below the ground surface, respectively. Caved depths may indicate groundwater is
present at orjust below the depth and caused the soils to collapse into the hole.It may also be the
result of soil cuttings left in the hole when the hollow stem flight augers were removed at the end
of drilling. The boreholes were backfilled with the soil cuttings brought to the surface by the
augers.In addition, temporary wells were placed in B-2, B-SB and B-7B. Stabilized groundwater
readings in these borings were 11.7 ft,29.8 ft and S ft,respectively.
September 30, 2005PhaseIIEnvironmental Assessment Report
MACTEC Project 6228-05-3103
3-1
On September 9, 2005, a representative of Priority Locating Services, Inc. visited the site to
perform the survey. Mr. Rob Foster ofMACTEC met the representative at the site. The results of
the survey identified an apparent group of out-of-service USTs alongCedar Streetreferenced as the
"A" UST area on Figure 2. Furthermore, an apparent heating oil UST ("B") was identified at the
rear of the 800 West Morehead building (Figure 2). UST "C" was not identified during the
magnetometer survey. This tank was identified during a later phase of assessment and is discussed
in Section 5 of this report.
MACTEC retained a private underground locating service (Priority Locating Services, Inc.) to
locate buried storage tanks andproduct lines at the site. The purpose of this effort was to minimize
the potential for probing intothe petroleum storage tanks or product lines.
3.0 MAGNETOMETER SURVEY
September 30, 2005Phase II Environmental Assessment Report
MACTEC Project 6228-05-3103
4-1
MACTEC's subcontractor advanced two additional borings (P-I0 and P-ll) at the 822 West
Morehead Street parcel using direct-push equipment to assess soil with respect to the former land
use (i.e. chemical company). On September 20, 2005, MACTEC personnel cored a hole through
the concrete floor slab in the basement of the 822 West Morehead building. The hole was cored
about 18inches from a floor drain identified in the Phase Iassessment. One soil sample (P-12) was
collected manually using a decontaminated hand auger bucket. The sample depths for these three
borings are shown on Table 6.2. One soil sample was retained from each of these three borings
and analyzed by Pace for volatile and semi-volatile organic compounds by EPA Methods 8260 and
8270 and the 8RCRA metals.
On September 14, 2005, MACTEC personnel noted a small area of "chemically-stressed" asphalt
pavement at the rear of the former gasoline station site. Our subcontractor advanced probe boring
P-9 at the center of the area. The soil probe encountered dark green to black fill soil from a few
inches to about 8 feet below grade. MACTEC personnel retained a soil sample to be analyzed for
volatile and semi-volatileorganics, the 8RCRA metals andTPH, DRO.
On September 14, 2005, MACTEC's subcontractor advanced a total of 9 soil probe borings (P-1
through P-9) at the 800 West Morehead Street property. Historical maps reviewed by MACTEC
indicated that gasoline storagetanks were formerlyburied along Cedar Street (UST Area "A"). Six
borings (P-1 through P-6) were advanced around theUST "A" system and were extended to depths
ranging from 2 to 16feet below land surface.BoringsP-7 and P-8 were advanced adjacent to UST
"B" to depths ranging from 8 feet below land surface. MACTEC personnel retained one soil
sample from each boring for laboratory analysis. The sample depths for the eight borings are
shown in Table 6.1. Soil samples P-l through P-8 were submitted to Pace Analytical, Inc. in
Huntersville,North Carolina for the analysis of Total Petroleum Hydrocarbons,Gasoline Range
Organics (TPH, GRO) and Diesel Range Organics (TPH, DRO) by Method 5030/3550/8015M.
The field procedures employedby MACTEC are summarizedin Attachment A.
4.0 SOIL SAMPLING AND ANALYSIS
September 30, 2005PhaseIIEnvironmental Assessmellt Report
MACTEC Project 6228-05-3103
5-1
In a short time, the vacuum truck representative inserted a vacuum hose into the borehole at the
elevation of the small hole in the tank. The purpose was to remove oil from the borehole adjacent
to the tank. Within about an hour, a contractor retained by MACTEC arrived with an excavator to
uncover the tank and search for a buried fill pipe. The contractor initiated excavation near the
exterior wall of the building. Upon removal of the overburden soil, the fill pipe was identified and
The small hole in the tank was observed using a flashlight and oil was observed leaking from the
hole in a fine stream. MACTEC immediately retained an oil recovery crew and a vacuum truck to
pump oil fromthe borehole and tank to minimize further loss of petroleum to the subsurface.
Well B-5 was installed at the location of probe boring P-9. MACTEC's drillers installed two-inch
diameter pvc well screen and casing in the boring to a depth of about 30 feet. MACTEC
personnel attempted to develop the well by bailing on September 21st. However, the well
contained less than one foot of water and the recharge of water was very slow. Since the auger
drilling rig used to install the subject well had encountered rock refusal at the 30 foot depth,
MACTEC retained Geologic Exploration, Inc. to drill another boring using air-rotary equipment
about three feet from the first and install a second temporary monitoring well. On September 23,
2005, GeologicExploration advanced a 6-inch diameterboring 3 feet north of well B-5 (ProbeP-9)
using air-rotary equipment. During advancement of the boring, the air-drilling bit contacted an
unknown (i.e. orphan) heating oil storage tank (UST "C") and punctured a small diameter hole
(about l/8-inch in diameter) in the tank.
On September21 and 23, 2005, MACTEC personnel collected groundwater samplesfrom wells B-
2 and B-7, respectively. The samples were placed on ice and delivered to Pace Analytical, Inc.
Groundwater samples collected from the wells were analyzed for volatile and semi-volatile
organics (EPAMethod 6230D) and 8RCRA metals.
On September20,2005, MACTEC personnel installedtemporary monitoring wells in geotechnical
borings B-2, B-5 and B-7 to collect groundwater samples for chemical analysis. The boring and
well locationsare shown on Figures 1and 3. MACTECpersonnel developed wells B-2 and B-7 by
bailing. WellB-5 contained very little water andwasnot developed or sampled.
5.0 GROUNDWATER SAMPLING AND ANALYSIS
September 30, 2005PhaseIIEnvironmental Assessment Report
MACTEC Project 6228-05-3103
5-2
Boring logs including well construction information are included as Attachment B. MACTEC
abandonedtemporary wells B-2 andB-7 on September 28, 2005.
Within a few minutes, it was observedthat the tank was empty. Furthermore,the fine stream of oil
previously leaking from the tank ceased flowing. From our preliminary measurements,it appeared
the tank capacity is about 550 gallons. The tank contained about half water and half oil.
Apparently, water had been entering the tank through the fill pipe broken off below ground. About
two feet from the broken fill pipe is a drain pipe that discharges water into the soil. The water
originates on the roof of the building and travels through a down spout on the exterior wall to the
underground drain pipe. MACTEC personnel observed the soil above the tank to be dark and
stained with petroleum.It appeared that the water that entered the tank over time had displaced oil
upward out of the top of the tank. The contractor placed a plug in the fill port hole and backfilled
the small excavation.
the pump truck representative began pumping contents of tank into the truck. Two small-diameter
copper lines were observed underground connected to the tank, indicatingthat the tank was used to
-store heating oil.
September 30, 2005Phase II Environmental Assessment Report
MACTEC Project 6228-05-3103
6-1
The results of the analyses performed on soil samples P-9 through P-12 identified several petroleum
hydrocarbon compounds. The metal analyses performed on the samples did not identify elevated
totals metals concentrations.
PreparedlDate: RCF 9-29-05
CheckedlDate: ~,\·30·05
Notes: All umts reported m ppm (parts per million).
NA= Not analyzed
Shaded values exceeded the State Action Level of 10 ppm.
Samp1ej])ate ,:1 ~H-@R;O ;;VPH!:DR(j)'.
JJO):il!!kNbmbe'r:D.~pilr(feet),
mpm);(PP~Y,,,:.1
"
P-l 9-14-05 15-16 <6.9 <5.8
'P-2 9-14-05 15-16 <7.8 ~",121",~'.
!;-
;',.:",
P-3 9-14-05 15-16 <6.8 <5.7
P-4 9-14-05 2 <7.6 <6.3
P-5 9-14-05 3-4 <7.4 <6.l
P-6 9-14-05 3-4 <7.2 <6.0
P-7 9-14-05 6-7 <7.5 580".....
P-8 9-14-05 7-8 <7.6 '.~@,(i)
-~
P-9 9-14-05 7-8 NA .~,'3.~~,J',
Table 6,1 - Soil Analytical Summary (TPH)
The results of the analyses performed on soil samples retained on September 14, 2005 identified
TPH concentrations that exceeded the State Action Level in samples P-2 (UST A), P-7 and P-8
(UST B) and P-9 (UST C).
6,1 Soil Assessment
6,0 RESULTS
September 30, 2005Phase II Environmental Assessment Report
MACTEC Project 6228-05-3103
6-2
PreparedlDate: RCF 9/30/05
CheckedlDate: ~'1/"60/05
Notes: All units reported in mgIKg (milligrams per Kilogram).
MSCC - Maximum Soil Contaminant Concentration
STW - Soil-to-Water
Shaded values exceeded soil cleanup level
Table 6.2 - Soil Analytical Summary (Org~nic Compounds)
')P-9" '.'P~lJ!)'P':'l4'P-l'.2.'~rSGG.'
Constituent "(:7':'&:1'"(g)"..".(3'!)~3'19 (IS~'
".,".',.,,
Total xylenes 1.300 <0.006 <0.007 <0.006 5
Acenaphthene <0.400 <0.410 20 <0.400 8
Anthracene <0.400 <0.410 22 0.630 995
Benzo (k) fluoranthene <0.400 <0.410 "3;6-0.830 12
Benzo (b) fluoranthene <0.400 <0.410 39 0.990 1-.
Naphthalene 0.950 <0.410 -6$7 -'@.9lfO 0.58
Benzo (a) anthracene <0.400 <0.410 50 [,1"0.34
Benzo (g,h,i) perylene <0.400 <0.410 8.9 <0.4 6,720
Benzo (a) pyrene <0.400 <0.410 149'1 0.091
Chrysene <0.400 <0.410 .§:O~1.1 38-_I ~
Dibenz (a,h) anthracene <0.400 <0.410 'S~$,0Q,,<0.400 0.17
Fluoranthene 0.420 <0.410 100 2.6 276
Dibenzofuran <0.400 <0.410
](i)<0.400 4.7
rt
Pyrene <0.400 <0.410 .97 2.2 286
Phenathrene <0.400 <0.410 1~t_(i)~2.7 60
2-methylnaphthalene <0.400 <0.410 :3,.~9.~,Q.<0.400 3
Fluorene <0.400 <0.410 20 <0.400 44
Ideno (1,2,3,-cd) pyrene <0.400 <0.410 ~Sl!!7@0:0.410 3
Chlorobenzene 3.100 <0.006 <0.007 <0.006 None
1,3-dichlorobenzene 0.730 <0.006 <0.007 <0.006 24
1,2,4, - trimethylbenzene 1.400 <0.006 0.0083 <0.006 8
1,2 - dichlorobenzene 2.500 <0.006 <0.007 <0.006 7
1,4 - dichlorobenzene 4.200 <0.006 <0.007 <0.006 1
September 30, 2005Phase II Environmental Assessment Report
MACTEC Project 6228-05-3103
6-3
PreparedlDate:RCF 9/30/05
CheckedlDate:t::@ ~1~lor;
MTBE =Methyltertiary butyl ether
Shadedvaluesexceeded theNCAC 2Lstandards.
Compound B-2 B-7 NCAC2L
(Ppb)(Ppb) Standards
Benzene <0.5 ,<,'3)'J ~.'~;:1.0
Toluene 0.79 0.68 70
Ethylbenzene <0.5 0.51 29
MTBE <0.5 0.86 200
TotalXylenes <0.5 3.5 530
Naphthalene 2.7 <2.0 21
Table 6.3- Groundwater Analytical Summary
The groundwater analytical results identified detectable concentrations of several petroleum
hydrocarbons. Only benzene (well B-7) was identified at a concentration that exceeded the State
Groundwater Standards. Total Lead (0.046 mg/L) was identified in the groundwater sample
collected from well B-2 at a concentration that exceeded the NC 2L Standard.In MACTEC's
opinion, the concentration is likely the result of sediment in the sample. MACTEC collected an
additional water sample from the well. The second sample was filtered by the laboratory prior to
acid digestion and analyzed fro "dissolved" metals. The "dissolved" test didnot identify lead. The
table below summarizes the organic laboratory results. The laboratory results are included in
AttachmentC.
6.2 Groundwater Assessment
September 30, 2005Phase II Environmental Assessment Report
MACTEC Project 6228-05-3103
7-1
• The chemical containers observed in the 800 West Morehead building should be
removed and their contentsdisposed at a permitted facility.
• A hydraulic automobile lift was observed inside the former Panther Parking building.
This lift was likely used during the time period when the service station was operated
at the 800 West Morehead property. The lift equipment should be removed. If
evidence of a hydraulic oil leak is observed, the affected soil should be excavated and
disposed at the permitted facility.
• The assessment identifiedpetroleum-affected soil at the location of Probe Boring P-ll.
This sample was collected adjacent to the 822 West Morehead building. Several
polynuclear aromatic hydrocarbons (PARs) were identified at concentrations that
exceeded the State Soil Cleanup Levels in the sample. The source of the contaminants
is not known, but may be related to surface water drainage from the nearby asphalt-
paved driveway over a long period of time. The soil in the vadose zone (0 to 5 feet) at
this location shouldbe excavated and disposed offsite at a permitted facility.
• The groundwater analytical results identified benzene at a concentration of 3.6 parts
per billion (ppb), in the groundwater sample collected from temporary monitoring well
B-7 (same location as Probe Boring P-ll). Title 15A of the North Carolina
Administrative Code (NCAC), Subchapter 2L (NCAC 2L) specifies a groundwater
standard for benzene of 1.0ppb. Therefore, the identified concentration exceeded the
groundwater standardestablishedby the NCDENR.
• The assessment identified three separate UST areas (A, Band C) shown of Figure 2.
Petroleum-affected soil was identified at each of the three locations. MACTEC
recommends that the USTs be removed and petroleum-affected soil is excavated and
disposed offsite at a permitted facility. Following removal and soil cleanup,
confirmation soil sampling and analysis should be performed to verify the
effectiveness of theremediation.
The results of this assessmentaresummarizedas follows:
7.0 CONCLUSIONS AND RECOMMENDATIONS
September 30, 2005PhaseIIEnvironmental Assessment Report
MACTEC Project 6228-05-3103
September 30, 2005
FIGURES
Phase II Environmental Assessment Report
MACTEC Project 6228-05-3103
CHECKED
FIGURE
BORING LOCATION PLAN
WEST MOREHEAD STREET
CHARLOTTE,NORTH CAROLINA
APPROXIllATE SCALE IN FEET
~~~EPARED ATE'I_}()-07!REF.:SITE SURVEY PLAN PREPARED BY R.B.PHARR &ASSOCIATES,P.A., FILE NO.W-3207;DATED 08/8/2005 JOB NO.6228-05-3103~L-~~_L ~
60 ENGINEERING '" CONSULTING,INC.
CHARLOnE.NORTH CAROUNA6030 0
EPXLANA TlON
APPROXIMATE LOCATlON OF
SOIL TEST BORING
MACTEC
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SOIL PROBE LOCATION PLAN
800 WEST MOREHEAD STREET'
CHARLOnE, NORTH CAROLINA
ENCIN££RING &CONSULTING,INC.
CHARLOTTE, NORTH CAROUNA
APPROXIMATE SCALE IN FEETAPPROXIMA TE LOCA11ON OF
SOIL PROBE BORING•
25o;2.525
EPXLANA 11ON
r-..,APPROXIMATE LOCATION OF BURIEDL_J UNDERGROUND STORAGE TANK
SOIL PROBE LOCATION PLAN
800 WEST MOREHEAD STREET
CHARLOnE, NORTH CAROLINA
MACTEC
ENGINEERING &CONSULUNG,INC.,
CHARLenE.NORtH CAROliNA
.,coc'iec
APPROXDlATE SCALE IN FEETAPPROXIMATE LOCATION OF
SOIL PROBE BORING WITH MONITORING WELL-t
30o153.0APPROXIMATE LOCATION OF
SOIL PROBE BORING•
EPXLANATlON
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~ REF.:SI1£ SURVEY PLAN PREPARED BY R.B.PHARR &ASSOCIA1£S. P.A.•FILENO.W-3207;DATED 08/8/2005
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September 30,2005
ATTACHMENT A
FIELD PROCEDURES
Phase IIEnvironmental Assessment Report
MACTEC Project 6228-05-3103
The wells consisted of 2-inch diameter PVC pipe (schedule 40 with flush-threaded joints) inserted
into 6-inch diameter boreholes. The bottom section of the well was a manufactured well screen
with O.OlO-inchslots. Washed sand backfill was placed aroundthe outside of the pipe to at least 1-
foot above the top of the well screen. The sand backfill was used to stabilize the formation and to
help yield a less turbid groundwater sample. Wetted bentonite was placed above the sand backfill
to seal the borehole. The remaining annulus of the borehole was backfilled with native soil to land
surface.
MACTEC installed Type II two-inch diameter wells for collection of groundwater samples. To
reduce the potential for cross-contamination, drilling personnel steam-cleaned down-hole drilling
equipment prior to drillingthe well boring.
Well Installation Activities
The soil samples were placed in laboratory-prepared sample containers, marked with a umque
identifying number, placed on ice in a sample cooler, and delivered to Pace, a North Carolina
certified laboratory, located in Huntersville, North Carolina for analysis. The samples were
maintained under chain-of-custodyprotocol.
Soil samples were collected from borings using either Direct Push Technology employing
stainless-steel core barrels to advance the boreholes or manually using a hand auger.In probe
borings, continuous soil samples were obtained in four-foot lengths with a stainless-steel sampling
tube and acetate tube liners.
Soil Borings/Soil Sampling
The field procedures used in the performance ofMACTEC's work is as follows:
FIELD PROCEDURES
September 30, 2005PhaseIIEnvironmental Assessment Report
MACTEC Project 6228-05-3103
Prior to sampling, a MACTEC field representative purged the well of at least three casing volumes
of water. A groundwater sample was collected using a disposable teflon bailer. After sampling,
MACTEC placed the containers on ice for delivery to the laboratory. MACTEC maintained
appropriate chain-of-custody records for the sample.
A MACTEC representative developed the monitoring wells by bailing until the water's turbidity
was reduced and it was determined that the well was functioning properly. The water level was
measured with an electric water level indicator to determine depth to the water surfacefrom the top
of the PVC riser pipe. The measured water depth was used in conjunction with the total casing
depth to determinethe height of the water columnand the volume of water in the monitoring well.
Monitoring Well Groundwater Sampling
September 30, 2005PhaseIIEnvironmental Assessment Report
MACTEC Project 6228-05-3103
September 30, 2005
ATTACHMENT B
BORINGIWELL LOGS
Phase II Environmental Assessment Report
MACTEC Project 6228-05-3103
THIS RECORD IS A REASONABLE INTERPRETATION
OF SUBSURFACE CONDITIONS AT THE EXPLORATION
LOCATION. SUBSURF ACE CONDITIONS AT OTHER
LOCATIONS AND AT OTHER TIMES MAY DIFFER.
INTERFACES BETWEEN STRATA ARE APPROXIMATE.
TRANSITIONS BETWEEN STRATA MAY BE GRADUAL.
PREPARED BY:
CHECKED BY:
I ..~"'.....II8Qfh®~g~.\[.R@}Q_Q~
PRO,'ECT;W,Morehead Parcels BORING NO.: B- I
COORDN:
COORD!!::
DRILLED·:September 20,2005
.PROJ.NO,:(1228-05-3103-03 PAGE I OF I
MACTEC Engineering &Consulting,Inc.
DRILLER: J.Cain
EQUIPMENT:D-50
METHOD:Hollow-stem Auger
HOLE DIA.:6"
REMARKS:
]0 20. 30 40. 50. 60 70 80 90 100
D SOIL CLASSIFICATION L E SAMPLES PL[%)NM(%)LL(%)E E L N-COUNT ri&0 ri&P AND REMARKS G E I T ... FINES(%)T E V D y fo"'~H N E P -""'-:0 • SPT (bpf)SEE KEY SYMBOL SHEET FOR EXPLANATION OF N UJ I:·M
SYMBOLS AND ABBREVIATIONS BELOW.D (FT)E -N r"'l~ft)T 10 20 30 40 50 60 70 80 90.100-0.A,"PUAl 'AnnYnY'654.0
\'~DA lli'l 'A"";',,v In,.h,,,~·
~.~
!l~13rown:'SJiftIY Micaceous Very Silty Fine.:With Reck ragments 88-1 5-7-8 rI'--'
.FILL -Rock Fragments
~
-
~8S-2 8:6-5 11I--5 -649..0.-f-5
FILk'- BrownSilty Fine to Medium SAND with
~
Roc Fragments
88-3 S-4c3
I'-
F{LL -Or~ge 'fan Silty Fine to MealUln SAND .1:-WIth Rock ragments IXSS-4 7-4-3f-10.-
~
644.0.-f-]0
;X
FlLL - Orai§e and Brown FcR\eto Medium Sandy x:SILT with.ck Fragments.oist).
~~XSS-5 4-4-4 I~I--15 -x f-,-639.o.-"-IS~x:<,r-,-~~l-
f".-RESIDUUM -Very Dense Brown Slightly ~:.::".',:::.:.:-.Micaceous Silty Fine SAND .".'"..~.X <,".~,.""'--~,'....'
~6~:.~:~'.....SS·6 23-23-42I--20...'634.0-'--20Bon~g Terminated at 20 Ft. ..No .round Water Encountered at Time ofBonog.Ground Water at 14Ft on 9,21-05.
I-25 -f-629.0-25
'- 30 --624.0-30
r
f--35 -I--619.0-35
-
'- 40 614.0
THIS RECORD IS A REASONABLE INTERPRETATION
OF SUBSURFACE CONDITIONS AT THE EXPLORATION
LOCATION, SUBSURFACE CONDITIONS AT OTHER
LOCATIONS AND AT OTHER TIMES MAY DIFFER.
INTERFACES BETWEEN STRATA ARE APPROXIMATE.
TRANSITIONS BETWEEN STRATA MAY BE GRADUAL.
PREPARED BY:
CHECKED BY:
DRILLER:J,Cain
EQUIPMENT: 0-50.
METHOD:Hollow-stem Auger
HOLE DIA.: 6"
REMARKS:
I ~'Cl]L;;mQ~~-~[~[l~~I:J '._'_,'"'. •~>'...~"'~'" "~
PROJECT:W. Morehead Parcels
BORINGNO.: B-2
COORDN:
COORDE:
DRILLED:September 20, 2005
PROJ.NO.:6228-05-3103-03 PAGE 1 OF 1
I MACTEC Engineering & Consulting, Inc.I
1-6,19.0-
'"~
~I-35 -s
";'oo_,
e.0-'!.
-ls"''- 40.-l...-------l __L 614.0...l..-___j___j----j__J___J_:--L,-.,.L,---!-:,--I!-:-~-±:::__:!'::_~--J
10.20.30 '40.59 60. 70 80. 90 IDa
I-624.0-I-3D -
I-629.0.'-I-25 -
ID-13-l3
::••~~r.~'::'
::::.~\:{:
-20.-+-'~;O:--n~'n-g":r;",",'e-m-'ll""'n__'al:-ed-'-,'-at""~2;;;O"F"'t.----------1-...:J.;..J...:.+-6~4;0-
nupa Wafer at 16Fi'at Time of'Boring and at 11.7After24HoursorMore..
RESlDut.UM -yerl':..firm O..live Brown Tan SiltyFine to ,Coarse SA!"!) (MOlst)
\
1\
[\~6
~ 15 -1+2 I~
l--
ss-s IXI'-
ALLUVIU.IM-Ve.rvLoos~Dark~r.ray Clayev Silty ". '.'»,FlUe to Medium SA"NDwith MedfUm OrganICS (Wet)':'~".:,::;.
I-10 -
FILL -.Oral).geand Ol!ve Brown ,Sllty Fine toMediumSA~D,with Clayey Pockets and RockFragments(Mol,st)
",,:::
::
:::
":".:
:.,
::
:::::.':::::::::
:::\~:::
::
.":;:':.:::':::
:
~ 5 -
hFI""""L""",L---'O"'",,-an-.g-e'""T"""a-n""",S"'i1-;-Iy'-"':F:""'li""~-:-!o"""'M""'''''ed''''iu-m--''S;--'AN"''"'''"'D''''"-~~~with Rock Fragments (N:1oist)
FILL -Orange Very Silty Fine SAND with RockFragments
80 90 100
SOIL CLASSIFICATION
AND REMARKS
SEE kEY SYMBOL SHEET FOR EXPLANA nON OF
SYMBOLS AND ABBREVIATiONS BELOW.~(ftO')~~~~~~~~~~~~~~~====ll~~1=I.';'<;:1>l'IA.rA,.,n,.,,~;m~.;; ~~
i'~;;110"",)I,''Bh r~'';h;''~'
FILL- Brawn'Q,rangepiJIe to Medium SandyClayeySILT with Rocl\.Fragments .
LL(%)
III
L E SAMPLES PL(%)NM(%)
E L I N-COUNT III 0
G E D T ~~.~
...FINES.(.%)E v E y
N P _""""•SPT(bpf)N (I),~'l-
D (fI),E '-'~ ("'1T 10 20.30 40 50 60 70654:0
[I l---
88-1 ~4-3-2 -.S
I 88-2.~4-3-3 "1-649,0'-IL'
I 83-3 ~2-1-2 "3"---
h.-
SS-4 ~3-6-i ,8;1-644.0-
:t:.
D
Ep
T
H
THIS RECORD IS A REASONABLE INTERPRETATION
OF SUBSURFACE CONDITIONS AT THE EXPLORATION
LOCATION.SUBSURFACE CONDITIONS AT OTHER
LOCATIONS AND AT OTHER TIMES MAY DIFFER.
INTERFACES BETWEEN STRATA ARE APPROXIMATE.
TRANSITIONS BETWEEN STRATA MAY BE GRADUAL.
PREP ARED BY:
CHECKED BY:
DRILLER:J.Cain
EQUIPMENT:D-50
METHOD: Hollow-stemAuger
HOLE DIA.:6"
REMARKS:
I ~Q)Jt1:m~Q~G'PJi$f[~a@'Rll [.'<i •_'.':,~, ,'~,.,,:;I~
PROJECT:W. Morehead Parcels BORING NO.:B- 3
COORDN:
COORDE:
DRILLED:September 20, 2005
PROJ.NO.:6228-05-3103-03 PAGE 1 OF 1
I MACTEC Engineering &Consulting, Inc.I
-'---------L-____L_615.0 _L--___.____..L,------___._~I!-::O~20::--:3!-::O---l.40::--S:!-:;0:---!6-::-0-7:!:0~8-:-0-9±-::O:---:-l10=0---'
50/3"
5-5-6
17-22-31
16-10-19
LL(%)
QI)
16-17-29
SS-5 fa:
,----,
SS-4 X'--
SS-3
VSS-2 V\
c---'
R,__
-62,0.0-
'"
~~35 -'":;:
0
'"00_,
o0...l
::l0
V)'-40
-625.0-~ 30 -
I-630.0-i-25-
1-635.0-~ 20 -
~15 -~~i-640.0-
f-A'-:u::~=,er::-;R.!~e::1'[1C::,1s=alr:a=n::i'd"ilBr::o:::;ri~Il.lt::-;·,;::,re=:IIl.=]::;:in=a,7:te<::i',j--a:""t 1"~".5"Fc;::\.----j1ll-ll..l..iI
Nouround Water Pre@nl at Completion of Boring,Ground Water at 11.9 Ft on 9-21-05.
~).:~\(r-645.0-
PARTlJ\LL¥WEA..~RED RO(;,K:-Sampledas \~~~Brown Silty Fine to Coarse SAND WIth Rock .IIFragments
~10-.
RESIDUUMF-Very Dense to Dense Brown Olive toBrown Silty ine to Medium SAND ' ,
650.0-~ 5 -
FILL - Ohve SIlty Fine to l\1eQiumSANDWateronDrillRods at 3.5 Ft During Drilling
~,SOIL CLASSIFICATION LE EL SAMPLES ~(%) N~(%)
I TN-COUNT~AND REMARKS ~ ~D y ~\0 ,f"...FINES (%)
H SEE KEY SYMBOL SHEET FOR EXPLANATION OF N ~ P 1;;-g 'E •SPT (bpf)
SYMBOLS AND ABBREVIATIONS BELOW.D (FT)E ......("l ""~~)~~~~~~~~~~~~~~~~~:3~~~-r_T__+-+-+-~I~O~2TO~3~O~4TO~5rO-6TO~7r°_T80~9rO~I~0~O--~A 'I'A~~.""imnr".l 655.0:-
lr''D A f1i"..'~'QI '<;ln~l,.o·~
FILL-Brown Tan Orange Very SiltyFine SAND:?<"Xwith Rock Fragments ~SS-1
~~
?S ~
~ ~
THIS RECORD IS A REASONABLE INTERPRETATION
OF SUBSURFACE CONDITIONS AT THE EXPLORATION
LOCATION. SUBSURFACE CONDITIONS AT OTHER
LOCATIONS AND AT OTHER TIMES MAY DIFFER.
INTERFACES BETWEEN STRATA ARE APPROXIMATE.
TRANSITIONS BETWEEN STRATA MAYBE GRADUAL.
DRILLER:J.Cain
EQUIPMENT:D-50
METHOD:Hollow-stemAuger
HOLE DIA.: 6"
REMARKS:
r
~-.::_.I~e>]L\BO~G''JEESEIf'RtB@~RB ~-~"",-",,:."".7""_-e-
PROJECT:W. Morehead Parcels BORING NO.: B- 4
COORDN:
COORDE:
DRILLED:September 19,2005
PROJ.NO.:6228-05-3103-03 PAGE 1 OF 1.
I MACTEC Engineering &Consulting, Inc.I
PREPARED BY:
CHECKED BY:
10 20 3.0 40 50 60 70 80 90 100
D SOIL CLASSIFICATION
L E SAMPLES PL(%)NM(%)LL(%)E E L Ii!!0 Ii!!P I N-COUNT
T AND REMARKS G E D T .fo~fo ... FINES (%)
H E V E Y
SEE KEY SYMBOL SHEET FOR EXPLANATION OF N P t;]"E.• SPT (bpf)
SYMBOLS AND ABBREVIATIONS BELOW.D (FT)N E -N <'l
-(g)T
671.5 10 20 30 40 50 60 70 80 90 100
Auger Refusal and.BorAngTellUinated at 1.FtBoreholeBackfi lied A er Boring Completion.
-5 -f-6665-5 .
f-10 --661.5-10
f-15 --656.5-15
f- 20 --651.5-20
f-2$--646.5-2S
f- )0 --641.5-30
-3-5 -f-636.5-35
r
-40 631.5
0::o
til(!J3
oo..J
dotil
THIS RECORD IS A REASONABLE INTERPRETATION
OF SUBSURFACE CONDITIONS AT THE EXPLORATION
LOCATION. SUBSURFACE CONDITIONS AT OTHER
LOCATIONS AND AT OTHER TIMES MAY DIFFER.
INTERFACES BETWEEN STRATA ARE APPROXIMATE.
TRANSITIONS BETWEEN STRATA MAY BE GRADUAL.
PREP ARED BY:
CHECKED BY:
I SOJILJB~ElN"cr~${P mot"JRD I.qy",.,,-=~-'""1.--,- .~"'.;'"" ...-
PROJECT:W. Morehead Parcels BORING NO.: B- 4A
COORDN:
COORDE:
DRILLED:September 19,2005
I'ROJ. NO.:6228-05-3103-03 PAGE 1 OF 1
I MACTEC Engineering &Consulting, Inc.I
DRILLER:J.Cain
EQUIPMENT:D-50
METHOD:Hollow-stemAuger
HOLE DIA.:6"
REMARKS:
J0 20 30 40 50 60 70 80 90 100
D SOIL CLASSIFICATION
L E SAMPLES PL(%)NM(%)LL(%)E E L N-COUNT 0 0 0p'IAND REMARKS
G E 0 T ~~~.&FINES (%)T E V yHNEp ....."d-c • SPT (bpf)SEE KEY SYMBOL SHEET FOR EXPLANATION OF N '"'"...SYMBOLS AND ABBREVIATIONS BELOW.D (FT)E ~ N-rn
~(~)T 10 20 30 40 50 60 70 80 90 100672.0
Auger ~~~salJ~d B.oring TeJ1llmaled at 1 Ft.Borello e ac ..I ed After Boring CompJetion.
~ 5 -I-667.0-5
~ 10-1-6.62.0-10
-15 -~657.0-15
I-20 -1-652.0-20
I-25 -~647.0-25
~30--642.0-30
I-35 -I--637.0-35
l-40 632.0
THIS RECORD IS A REASONABLE INTERPRET ATION
OF SUBSURFACE CONDITIONS AT THE EXPLORATION
LOCATION. SUBSURFACE CONDITIONS AT OTHER
LOCATIONS AND AT OTHER TIMES MAY DIFFER.
INTERFACES BETWEEN STRATA ARE APPROXIMATE.
TRANSITIONS BETWEEN STRATA MAY BE GRADUAL.
PREPARED BY:
CHECKED BY:
I ,'r,$OJlh ~q~:6."TB§~-~90!qi>I
PROJECT:W.Morehead Parcels BORING NO.:B-5
COORDN:
COORDE:
DRILLED:September 19,2005
PROJ.NO.:6228-05-3103-03 PAGE 1 OF 1
I MACTEC Engineering &Consulting,Inc.I
DRILLER:J.Cain
EQUIPMENT:D-50
METHOD: Hollow-stemAuger
HOLE DIA.: 6"
REMARKS:
10.20 30 40 50 60 70 80 90 roe
D SOIL CLASSIFICATION L E SAMPLES PL(%)NM,(%)LL(%)E E L N-COUNT III '0 IIIP1
T AND REMARKS G E D T ... FINES (%)
H E V E Y ('.,>:0;0
N P :oi-'l"O-c • SPT (bpf)SEE KEY SYMBOL SHEET FOR EXPLANATION OF N rn c ~
SYMBOLS AND ABBREVIATIONS BELOW,D (FT)E -N .....(ft)T
I-0 676.0 10 20 30 40 50 60 70 80 90 100,lnr-h'A •·)\n......."··;m~'''iJn('h,.~·
',~SO;
~J.LL-Oran~ and Tan.lfrown Mic;~ccous Claye~X,ilty Fine to edium SAND witli Rock Fragmen s SS-1 3-2-3 '5'--'
FILL-Brown Very Silty Fine SAND ~
SS-2 ~2-2-1 1'-1I-5 -671.0-<,5
FILL -Olive Brown,VeR, Silty Fine SAND with X r-,Rock Fragments,Brick teces and Concrete (Moist)
1'-:6SS-3 4-25-11'--
Au~r Re~sal and Boring Terminated at pFt.No roun wate[ ~T\c~untereQat Time ~-l3ormg.
I-10 -Borehole Backfil ed Af er Boring Camp etlan.-666.0-10.
-15 --661.0-15
I-20 --656.0-20
-25 --651.0-25
I-30 --6<16.0-30
- 35 --641.0-35
-40 636,0
THIS RECORD IS A REASONABLE INTERPRETATION
OF SUBSURFACE CONDITIONS AT THE EXPLORATION
LOCATION.SUBSURFACE CONDITIONS AT OTHER
LOCATIONS AND AT OTHER TIMES MAY DIFFER.
INTERFACES BETWEEN STRATA ARE APPROXIMATE.
TRANSITIONS BETWEEN STRATA MAY BE GRADUAL.
PREPARED BY:
CHECKED BY:
I S@;It:'J~0MNr&''m$]j"~P:O:m~Ie-_.-''l:'"":'"?""."._.."_Aj.
PROJECT:W. Morehead Parcels BORING NO.: B-5A
COORDN:
COORDE:
DRILLED:September 19,2005
PROJ.NO.:6228-05-3.103.-03.PAGE I OF 1
I MACTEC Engineering & Consulting,Inc.I
DRILLER:J.Cain
EQUIPMENT:D-50
METHOD:Hollow-stem Auger
HOLE DIA.: 6"
REMARKS:
§
§
'"10 20 30 40 50 GO 70 80 90 LOa
D SOIL CLASSIFICATION
L E SAMPLES PL(%)NM(%)LL(%)E E L III-COUNT 0 e 0PANDREMARKSGEIT... FINES (%)T D ~~foEvEyHSEE KEY SYMBOL SHEET FOR EXPLANATION OF N P ~""Q"'I:'• SPT (bpf)III '"r::...SYMBOLS AND ABBREVIATIONS BELOW.D (FT)E -,M ('f'l
f--(~)T 10 20 30 40 50 60 70 80 90 100676.0
Au~rRef\lsal and Bormg Terminated al2 5 Ft.o .roun~ Wat1t ~nC0untereQ at t?me ofi'lonng.Borehole _ackfi e After Boring ompletion,
f--5 --671.0-5
f-- 10 -f--666.0-10
f--15 -1-661.0-15
f-- 20 -f--656.0-20
I-25 -1-65'1.0-25
f-- 30 -f--646..0-30
I-35 -f--641.0-3_5
'-40 636.0
;;:o
'"8_,
THIS RECORD IS A REASONABLE INTERPRETATION
OF SUBSURFACE CONDITIONS AT THE EXPLORATION
LOCATION.SUBSURFACE CONDITIONS AT OTHER
LOCATIONS AND AT OTHER TIMES MAY DIFFER.
INTERFACES BETWEEN STRATA ARE APPROXIMATE.
TRANSITIONS BETWEEN STRATA MAY BE GRADUAL.
PREPARED BY:
CHECKED BY:
....L..----------.L--_..J_636.5 _L--__L_L-----__L-1L...,0-.J.20::--:3~O-.J.40::--5~0~60=--:7:L:O~80=-:9!-::O---:-l:1o:::'o-_J
RESlDt),llM-Dense Brown SillY.Fine to MegMn.-(.:-~..:SAND with Rock Fragments and Clay Seams ~wet):::.: ':'.
,~\; ::)'i/SS-5 ~38~33-11
I-30 +-;B~o:-::r'=in-'-g""t'=!,!eJ!1l==",m--ru'7te--dra'71"i'30~Ft:-.---------"__::;l;:j....:l.~+646.5 _.~
GrQuno W8aatt!ercncouoteJedat 27 .Ftat Time of Boringandat29. Fl After 24 hours or More;
DRILLER:J.Cain
EQUIPMENT:D-50
METHOD:Hollow-stem Auger
HOLE DIA.:6"
REMARKS:
I S0E ]JDRITN@~'S~R.'B)@.@YJR!El I'v "'~"7' ,"":::~i:=......",~
PROJECT:W. Morehead Parcels BORING NO.: B- 5
COORDN:
COORDE:
DRILLED:September 20, 2005
,PROJ.NO.:6228-05-3103-03 PAGE 1 OF 1
I MACTECEngineering &Consulting, Inc.I
.."~.:.:;-.:,
:~'~::':>: ::':
-:".
"~';:~'::,:':::';.
~..>..,,:
'.•'p'-~,."...:
~
SS-4 IX651.5- ~
l-
88-3 ~,656.5-~
302-3
l-
SS-2 IX661.5-I'--'
4-4-5 9
4-4-5
-641.5-
FlLL -T~Orange Fine Sandy Very Clayey SILTwith Sand lMO!st)
FILL -Orange Tan Silty Fine to Medium SANDwithRockFragments'
FlJ,.,L-Gray Brown Silty Fine to Medium SAN,QwithClayeyPocketsand"Rock Fragments (Odor)
SOIL CLASSIFICATION
AND REMARKS
I-2S -
~20-
I-15 -
~10-
~5 -
:g
0;sf-35 -
Q::
0
'"00...I
00-lS,_40'"
SEE KEY SYMBOL SHEET FOR EXPLANATION OF
SYMBOLS AND ABBREVIATIONS BELOW.
~(~~,,~.-~~~~--~--~~--------~--~Drilled without SPT Sampling to 8.5 Ft
Fll..L -Brown Silty Fme to Medium SAND withRock Fragments
D
E
P
T
H
L E SAMPLES PL(%)NM(%)LL{%)
E L I N-COUNT 0 0 (,&
G E D T fo(o~A FINES('Yo)
E v E Y
N N P t;]"E •SPT(bpt)
0 (FT)E ......N MT 10 20 30 40 50 60 70 80 90 100676.5
~~
~
~5[
f-fi71.5-
MACTEC Engineering &Consulting;Inc.
BOR]NGNO.:B- 6W.Morehead ParcelsPROJECT:
COORD N:
COORDE,
DRILLED:
PROJ.NO.:THIS RECORD IS A REASONABLE INTERPRETATION
OF SUBSURFACE CONDITIONS AT THE EXPLORATION
LOCATION. SUB SURFACE CONDITIONS AT OTHER
LOCATIONS AND AT OTHER TIMES MAY DIFFER.
INTERFACES BETWEEN STRATA ARE APPROXIMATE.
TRANSITIONS BETWEEN STRATA MAY BE GRADUAL.
PAG.E I OF 1
September 19,2005
6228·05·3103·03
PREPARED BY:
CHECKED BY:
DRILLER:1.Cain
EQU1PMENT:D-50
METHOD:Hollow-stem Auger
HOLE DIA.:6"
REMARKS:
10 20 30 40 50 60 70 80 90 10.0
D SOIL CLASSIFICATION L E SAMPLES PL(%)NM(%)LL(%)E E L N-COUNT ~0 ~P AND REMARKS G E I T ... FINES (%)T E V D Y c ·fa eoE\0,"0HNP"t?CI~• SPT (bpi)SEE KEY SYMBOL SHEET FOR EXPLANATION OF ND(FT)E --'"t':l.
f-Cgl SYMBOLS AND ABBREVIATIONS BELOW.T 10 10 31)40 50 60 70 80 90 100AO::P'IA .Ann"";';",~"'I,.<;]"",.I,,,_<t 'r>Z 67S.0-.fvv 'l\n"'\-"Yi""~h.I'.~Tn"h~<I ~FlLL -B[owriFine to Medium Sandy Cla)(ey,SIL T
~
with Rock Fragments SS-I 3-2-4 'I~ - BraWl)Fmc \0 ~~iUIV Sandy c,:laycU'ILT
~
Rock Fragments,'rick Pieces,and ASp .It
I~S8-2 2-2-2 r-.f-,5 -~>-613.0-I'--'r---5r-:-I----8 ,t><t--.l-I----FILL ~J~toRn~twetoMedium $andy-Very Clayey S~2-50/6"NtlOOSILTwithOC·_ragments (MOist)..@.8S-3 I'-'
~,
Aug~blt~USal and Boring Terminated at -8.5Ft due to IPos8te0wrete~Iab..
>-10-No .round.-ater ,ncountered at Ti~e of~BOI:ing.f-668.0-10Borehole Caved and Dry at 75 Ft on -20-05..
<
-15 --663.0-1-5
'.
I--20 -'-658.0-10
>-25.,-1--653.0-~5
-
I--30 -f-648.0-30.
>-35 -h643.0-35
40 638.0
THIS RECORD IS A REASONABLE INTERPRETATION
OF SUBSURFACE CONDITIONS AT THE EXPLORATION
LOCATION.SUBSURFACE CONDITIONS AT OTHER
LOCATIONS AND AT OTHER TIMES MAY DIFFER.
INTERFACES BETWEEN STRATA ARE APPROXIMATE.
TRANSITIONS BETWEEN STRA TA MAY BE GRADUAL.
PREPARED BY:
CHECKED BY:
I~:$,~];L~b>J{lN'@~E~ff'®R~~jID ;1
PROJECT:W. Morehead Parcels BORING NO.: B- 7
COORDN:
COORDE:
DRILLED:September 19,2005
PROJ.NO.:6228-05-3103-03 PAGE 1 OF 1
I MACTEC Engineering &Consulting, Inc.I
DRILLER: J.Cain
EQUIPMENT: D-50
METHOD:Hollow-stem Auger
HOLE DIA.:6"
REMARKS:
10 20 30 40 50 60 70 80 90 100
D SOIL CLASSIFICATION L E SAMPLES PL(%)NM(%)LL(%)E E L N-COUNT ~0 IIIPIANDREMARKSGET... FINES (%)T 0 fo"'~E V E YHNP ~-c~• SPT (bpi)SEE KEY SYMBOL SHEET FOR EXPLANATION OF N '";::::...
SYMBOLS AND ABBREVIATIONS BELOW.D (FT)E _,N ro
(ft.)T 10 20 30 40 50 60 70 80 90 100I--0 A<;111 A "·In,..hp~'f9"&655.0r'A l 'b."'''';''''';'''~I..r,'h'''~'
~!,Th;\-n~~~~~~~e to Medium Sandy Clayey SILT ~SS-I 3"5-50/2"1-100
t .'ents
Auger Rerusal a~,dBorAng Tel1llinated at2 Ft.Boreho IeBackfilled A .erBonng Completlon.
I--5 -1-650.0-5
I--]0 -1-645.0-10
I-15 -I-6'10.0-15
I--20 -I-635.0-20
I-25 -1--630.0-25
- 30 --625,0-30
I-35 --620.0-35
L 40 615.0
THIS RECORD IS A REASONABLE INTERPRETATION
OF SUBSURFACE CONDITIONS AT THE EXPLORATION
LOCATION.SUBSURFACE CONDITIONS AT OTHER
LOCATIONS AND AT OTHER TIMES MAY DIFFER.
INTERFACES BETWEEN STRATA ARE APPROXIMATE.
TRANSITIONS BETWEEN STRATA MAY BE GRADUAL.
PREPARED BY:
CHECKED BY:
I.I~O~,~'Q~Q TEST iREGOElD I
PROJECT:W. Morehead Parcels
BORING NO.:B-7A
COORDN:
COORDE:
DRILLED:September 20,2005
.PROJ.NO.:6228-05-3103-03 PAGE 1 OF 1
I MACTEC Engineering &Consulting, Inc.I
DRILLER:1.Cain
EQUIPMENT:D-50
METHOD:Hollow-stemAuger
HOLE DIA.: 6"
REMARKS:
10 20 30 40 50 60 70 80 90 100
D SOIL CLASSIFICATION L E SAMPLES PL(%)NM(%)LL(%)E E L N-COUNT III 0 IIIPI
T AND REMARKS G E D T eot:.eo '" FINES(%)
H E V E 'f
SEEKEYSYMBOLSHEETFOREXPLANATIONOF N N p tn -g'~• SPT (bpf)
SYMBOLSANDABBREVIATIONSBELOW.D (FT)T E -N«1
-(g)655.0 10 20 30 40 50 60 70 80 90 100Ato;:pJ<'A A
:UAVl?'A .t...l·I rn,...h,.~'~
Drilled wimoufSPT Sampling to 3.5 Ft
R~ILL -~1.own ~H~Fine to Medium SAND with
~layey lit Poc ets and Glass Pieces (Moist)SS-1 2-4·2 I~I'-5 -'Y r-650.0-f---'5
FI~-Brown MICaceous Sil~me to Coarse ..x.
~
SA.with Rock Fragments oisi)III &
lS8 SS-2 3-4-2 ·n,r-r-'--'t----N( SAM!'I.I-:WI-:T 'FRY r--r-AU'tjTRefuW and Boring Termingted at ~.5n SS-3 SOfO"N~100
o roun~.ater EncounteTeS at TIme of Bffmg.
-'10 -Borehole avedand Dry at 6.Ft on 9-21-0 .f-645.0-10
-15 -r-640.Q-IS
-20-I-635.0-20
-25 -f-63D.O-25
-30 -1-625.0-30
f- 35 --620.0-3S
'-40 6\5.0
THIS RECORD IS A REASONABLE INTERPRETATION
OF SUBSURFACE CONDITIONS AT THE EXPLORATION
LOCATION. SUBSURFACE CONDITIONS AT OTHER
LOCATIONS AND AT OTHER TIMES MAY DIFFER.
INTERFACES BETWEEN STRATA ARE APPROXIMATE.
TRANSITIONS BETWEEN STRATA MAY BE GRADUAL.
PREPARED BY:
CHECKED BY:
DRlLLER:J. Cain
EQUIPMENT:D-50
METHOD:Hollow-stem Auger
HOLE DIA.:6"
REMARKS:
,~_®X,l3,~~.ijj mE$tB@@~~',
.,
PROJECT:W.Morehead Parcels BORING NO.: B- 7
COORDN:
COORDE:
DRILLED:September 20,2005
PROJ.NO.:6228-05-3103-03 PAGE 1 OF 1
I MACTECEngineering &Consulting, Inc.I
~----------------------------------L_--J_615.0~---L-L-------L~~~~~~~~~~~~~__~10 20 30,40 50 60 70 80 90 1,00
\6 }.::"1-+-1+'-+-+--+--+---11---1--1--1'"'..\
4-8-8
lQ·l0-10
LL(%)rlJ
SS·2 [X<-
F-
-620.0-
'".~a;I-35 -
c::0
'"00_,
00_,_,
isv,-40
-625.0-I-30 ~
I-630.0-I-25 -
I-635.0-f-20 -
1-640.0-f-15 -
Auger Eefusal an.!!Boring Terminated at 11 Ft.Ground Water at 5 Ft Alter 24 Hours or More.
1r E SS4~~RTIA~~W ATBEREDROCK-,s_aml1led as ~~\ 1I'~645.0-~~~..~~~Ltw~~to Medium SAND with ROCK l\\..\\\\f-10-
-5 -
RESIDUUM - Fj:nn Brown Orange ,SIltYFine toCoarse,SAND With Rock Fragments (Wet)
~SOIL CLASSIFICATION LE EL SAMPLES ~(%)Ntye1(%)
PIT N-coUNT
T AND REMARKS ~~0 y l:o ~ ~..FLNESC%)
H SEEKEYSYMBOLSHEETFOREXPLANATIONOF N ~P t;-g'-g •SPT(hpt)SYMBOLSANDABBREVIAnONS BELOW.0 (FT)E .,....,N ,..,
f-cg)+--;;'<;i'Y'ii""""i'iI'A:::===:;::-;"-=::-r-----h-r~7I_655.0 --t--T-t-t-----t--..:,.I 0::...'....:2:;:::0'--=',3.:::..0_4T'0'--=',5;::...0_6:;::O,---,7r-0.....:8:rQ'--.::!90:::......!_100TOPSOlL(Approxlmately 9 Inches).Lf.,:.~I I
F1LL-BrQYJnFine to Medium S!V1dyC]ayey_}>1LT ~¢(--IX ..WIth Rock Fragments and Glass Pieces (Moist)~K)
1S ~58.]F-2·5-3 ~8 :
September 30, 2005
ATTACHMENT C
LABORATORY RESULTS
;1
Phase II Environmental Ass~ssment Report
MACTEC Project 6228-05-3103
Charlotte Certification IDs
NCWastewater 12
NGDrinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshallnotbereproduced.exceptin full.
withoutthewrittenconsentof PaceAnalyticalServices.Inc.
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Enclosures
Annette Scott
Annette.Scottipacelabs.com
Project Manager
Sincerely,
If you have any questions concerning this report please feel free to contact me.
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic testing
was performed at our Pace Charlotte laboratory unless otherwise footnoted.
Enclosed are the analytical results for sample(s) received by the laboratory on September 14, 2005. Results
reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the
body of the report.
Dear Mr.Poster:
RE: Lab Project Number: 92103111
Client Project ID: West Morehead/6228-05-3103
Mr.Rob Poster
Mactec
2801 Yorkmont Road
Suite 100
Charlotte, NC 28208
September 29, 2005
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone:[phone]
Fax: [phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]M'lW.paoelabs,com
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall notbereproduced.exceptin full,
withoutthewrittenconsentof PaceAnalyticalServices,Inc.
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Page: 1 of 46Date:09/29/05
%
1.1 09/20/05 16:30 DHW
1.0 09/20/05 16:30 DHW 460-00-4
6.9mg/kgNO
96
Method: EPA 8015
GCVolatiles
GAS, Boil
Gasoline
4-Bramofluorobenzene (B)
1.1 09/21/05 OO:OB KeS 68334-30-5
1.0 09/21/05 00:08 KeS 629-99-2
09/15/0509/15/05
Prep/Method: EPA 3545 / EPA B015
NO mg/kg 5.B
75 %
GCSemivolatiles
TPH in Soil ~ 3545/B015
Diesel Fuel
n-Pentacosane (S)
Date Extracted
1.0 09/15/05 13:0B KBM%13.2
Method:%Moisture
WetChemistry
Percent Moisture
Percent Moisture
Units Report Limit _m:__---"An.....a=.ly...zese"'d.____.Bv"'-<--_C""AS""'-.....N"'o'-'.__.Qyal._RegLmtResults
Date Collected: 09/14/05 09:30
Date Received: 09/14/05 13:34
Project Sample Number: 92103111-001
Matrix: Soil
Lab Sample No: 926093105
Client Sample ID: P-l (15-16)
Solid results are reported on a dry weight basis
Lab Project Number: 92103111
Client Project ID: West Morehead/622B-05-3103
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax: [phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]
aceAnalytical ~
Willw.pace/abs.com
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not bereproduced,exceptin full,
without the written consentof PaceAnalyticalServices,Inc.I.'I~J"#~:C~~r~
j{Ut2Ct.;
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
Page:2 of 46Date:09/29/05
1.3 09/20/05 17:30 DHW
1.0 09/20/05 17:30 DHW 460-00-4
7.8
Method: EPA 8015
ND mg/kg
92 %
GC Volatiles
GAS, Soil
Gasoline
4-Bramof1uorobenzene (S)
%76
09/15/05
1.3 09/20/05 22:40 KeS 68334-30-5
1.0 09/20/05 22:40 KeS 629-99-2
09/15/05
EPA 8015
6.5
prep/Method: EPA 3545
12.mg/kg
GC Semivolatiles
TPH in Soil by 3545/8015
Diesel Fuel
n-Pentacosane (S)
Date Extracted
1.0 09/15/05 13:09 KBM%22.7
Method:%Moisture
Wet Chemistry
Percent Moisture
Percent Moisture
Units Report L:iJnit~_---'A""n""a"'l""y...z""ed......._"'BvOL...__,C",AS..._""No",_,_._ ~ RegLmtResultsParameterS
Date Collected: 09/14/05 09:50
Date Received: 09/14/05 13:34
Project Sample Number: 92103111-002
Matrix: Soil
Lab Sample No: 926093113
Client Sample ID: P-2 (15-16)
Lab Project Number: 92103111
Client Project ID: west Morehead/6228-05-3103
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville,NC28078
Phone: [phone]
Fax:[phone]wI'IW.pacefaDS.com
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced.except in full,
wtthout thewritten consentof PaceAnalyticalServices, Inc.
~
4j,,:!-JiQ~~,
ff ~
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
page: 3 of 46Date: 09/29/05
1.1 09/20/05 18:30 DHW
1.0 09/20/05 18:30 DHW 460-00-4
6.8
Method: EPA 8015
NO mg/kg
85 %
GC Volatiles
GAS, Soil
Gasoline
4-Bromofluorobenzene (S)
1.1 09/20/05 22:10 KBS 68334-30-5
1.0 09/20/05 22:10 KeS 629-99-2
09/15/05
EPA 8015
5.7
Prep/Method: EPA 3545
NO mg/kg
84 %
09/15/05
GC Semivolatiles
TPH in Soil by 3545/8015
Diesel Fuel
n-Pentacosane (S)
Date Extracted
1.0 09/15/05 13:09 KBM
Method:%Moisture
11.9 %
Wet Chemistry
Percent Moisture
Percent Moisture
units Report Limit _m:____.:An.....a,:ly....z""e""d,-__"Bv....'-_-,C""AS"",-",No",-.,--_~ RegLmtResultsParameters
Date Collected: 09/14/05 10:05
Date Received: 09/14/05 13:34
Project Sample Number: 92103111-003
Matrix: Soil
Lab Sample No: 926093121
Client Sample ID: P-3 (15-16)
Lab Project Number: 92103111
Client Project ID: West Morehead/6228-05-3103
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]I'Iww.pa~labs.oom
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 3n06
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced,exceptin full,
withoutthe written consent01PaceAnalyticalServices,Inc.
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Page: 4 of 46Date:09/29/05
1.3 09/20/05 18:59 DHW
1.0 09/20/05 18:59 DHW 460-00-4
7.6
Method: EPA 8015
MD mg/kg
92 %
GC Volatiles
GAS, Soil
Gasoline
4-Bromofluorobenzene (S)
68334-30-5
629-99-2
1.3 09/20/05 22:40 KBS
1.0 09/20/05 22:40 KBS
09/15/05
EPA 3545 / EPA 8015
mg/kg 6.3
%
prep/Method:
MD
93
09/15/05
GC Semivolatiles
TPH in Soil by 3545/8015
Diesel Fuel
n-Pentacosane (S)
Date Extracted
1.0 09/15/05 13:10 KBM
Method:%Moisture
20.8 %
Wet Chemistry
Percent Moisture
Percent Moisture
units Report Limit __m:___---E.Ana"""'=.ly..,:z""e."d'---"By<L.__C",AS"",--"N",o,_,_.__~ RegLmtResultsParameters
Date Collected: 09/14/05 10:15
Date Received: 09/14/05 13:34
Project Sample Number: 92103111-004
Matrix: Soil
Lab Sample No: 926093139
Client Sample ID: p-4 (2)
Lab Project NUmber: 92103111
Client Project ID: West Morehead/6228-05-3103
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville,NC28804
Phone:[phone]
Fax: [phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue,Suite 100
Huntersville, NC28078
Phone:[phone]
Fax:[phone]II;'!'...W.pacefabs.c{)m
Charlotte Certification IDs
NGWastewater 12
NG Drinking Water 37706
SG 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,exceptin full,
withoutthe written consentof PaceAnalyticalServices,Inc.
;.>o\y.I~~~'t1"l[Jelaa~
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Page: 5 of 46Date:09/29/05
1.2 09/20/05 19:29 DHW
1.0 09/20/05 19:29 DHW 460-00-4
7.4
Method: EPA 8015
ND mg/kg
88 %
GCVolatiles
GAS, Soil
Gasoline
4-Bramof1uo:r:obenzene (S)
1.2 09/20/05 23:09 KBS 68334-30-5
1.0 09/20/05 23:09 KBS 629-99-2
09/15/05
1.0 09/15/05 13:10 KBM18.4 %
Prep/Method: EPA 3545 /EPA 8015
ND mg/kg 6.1
68 %
09/15/05
GCSemivolatiles
TPH in Soil by 3545/8015
Diesel Fuel
n-Pentacosane (S)
Date EKtracted
Method:%Moisture
Wet Chemistry
Percent Moisture
Percent Moisture
units Report L:ilIIit..J2L._---"Ana=l=.;y...,z."e",d.__--'-"-By'-'-____,C...AS=-_.,N_,._o-,-._ ~ RegLmtResultsPe:r:i:oneters
Date Collected: 09/14/05 10:30
Date Received: 09/14/05 13:34
Project Sample Number: 92103111-005
Matrix: Soil
Lab Sample No: 926093147
Client Sample ID: P-5 (3-4)
Lab Project Number: 92103111
Client Project ID: west Morehead/6228-05-3103
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]
ace AnalyticalT\l
WI'l'iv.pSC-e!sbs,com
Charlotte Certification IDs
NCWastewater 12
NCDrinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,exceptin full,
whhout thewritten consentof PaceAnalyticalServices,Inc.
~ffj!~#?J~1.
Page: 6 of 46
1.2 09/20/05 19:59 DHW
1.0 09/20/05 19:59 DHW 460-00-4
1.2 09/20/05 23:39 KeS 68334-30-5
1.0 09/20/05 23:39 KeS 629-99-2
09/15/05
EPA 8015
6.0
1.0 09/15/05 13:11 KBM
Units Report Limit ...m:____,An=a"'l..y-"z",ed=-_-"'Bv'"'-__,C""AS..._!!:No~.,--_mL RegLmt
Project Sample Number: 92103111-006
Matrix: Soil
%
mg/kgNO
95
Method: EPA 8015
09/15/05
Prep/Method: EPA 3545
NO mg/kg
68 %
Method:%Moisture
17.0 %
Results
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SCEnvironmental 99030
FL NELAP E87648
Date:09/29/05
GC Volatiles
GAS, Soil
Gasoline
4-Bromofluorobenzene (S)
GC Semivolatiles
TPH in Soil by 3545/8015
Diesel Fuel
n-Pentacosane (S)
Date Extracted
wet Chemistry
Percent Moisture
Percent Moisture
Parameters
Date Collected: 09/14/05 10:40
Date Received: 09/14/05 13:34
Lab Sample No: 926093154
Client Sample ID: P-6 (3-4)
Lab Project Number: 92103111
Client Project ID: west Morehead/6228-05-3103
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville,NC 28804
Phone:[phone]
Fax:[phone]
Pace Analytical Services. Inc.
9800 Kincey Avenue. Suite 100
Huntersville,NC 28078
Phone:[phone]
Fax: [phone]
Charlotte Certification IDsNeWastewater 12
NCDrinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shallnot bereproduced.exceptin full,
without the written consentof PaceAnalyticalServices.Inc.
.,.•.t~,.~S:Lf.::~gfl.lt!I'lC·~
AshevilleCertification IDs
NGWastewater 40
NGDrinking Water 37712
SCEnvironmental 99030
FLNELAP E87648
Pal1e: 7 of 46Date: 09/29/05
1.2 09/20/05 20:29 DBW
1.0 09/20/05 20:29 DBW 460-00-4
7.5
Method: EPA 8015
ND mg/kg
88 %
GC Volatiles
GAS, Soil
Gasoline
4-Bromofluorobenzene (S)
6.2 09/20/05 23:39 KeS 68334-30-5
1.0 09/20/05 23:39 KeS 629-99-2 1
09/15/05
Prep/Method: EPA 3545 1 EPA 8015
580 mg/kg 3l.
190 %
09/15/05
GC Semivolatiles
TPH in Soil by 3545/B015
Diesel Fuel
n-Pentacosane (S)
Date Extracted
1.0 09/15/05 13:12 KBM
Method:%Moisture
20.0 %
Wet Chemistry
Percent Moisture
Percent Moisture
Units Report Limit ~ ______.Ana}""""""y...z",e...d..______.By"._--'C"'AS""'-...,N",o.:...._ Qual RegLmtResultsparameter!!
Date Collected:09/14/05 10:45
Date Received:09/14/05 13:34
Project Sample NUmber: 92103111-007
Matrix: Soil
Lab Sample No: 926093170
Client Sample ID: p-7 (6-7)
L~b Project Number: 92103111
Client Project ID: West Morehead/6228-05-3103
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax:[phone]Vll'.'w.pacelaos.com
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced,exceptinfull,
w~houtthewritten consentof PaceAnalyticalServices,Inc.
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Page: 8 of 46Date:09/29/05
%
1.3 09/20/05 20:59 DHW
1.0 09/20/05 20:59 DHW 460-00-4
7.6DIg/kgNO
109
Method: EPA 8015
GC Volatiles
GAS,Soil
Gasoline
4-Bromofluorobenzene (S)
1
6.3 09/20/05 23:09 KeS 68334-30-5
1.0 09/20/05 23:09 KeS 629-99-2
09/15/05
%173
09/15/05
prep/Method: EPA 3545 / EPA 8015
970 mg/kg 32.
GC Semivolatiles
TPH in Soil by 3545/8015
Diesel Fuel
n-Pentacosane (S)
Date Extracted
1.0 09/15/05 13:12 KBM
Method:%Moisture
21.1 %
Wet Chemistry
Percent Moisture
Percent Moisture
units Report LiJnit___m:__ _____.An...,.a..,.ly...,z.,e"'d'----"Bv''_L___,C"'A..S,___.,N"'o......_ Qual RegLmtResultsParameters
Date Collected: 09/14/05 11:00
Date Received: 09/14/05 13:34
Project Sample Number: 92103111-008
Matrix: Soil
Lab Sample No: 926093188
Client Sample ID: P-8 (7-8)
Lab Project Number: 92103111
Client Project ID: West Morehead/6228-05-3103
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville,NC28804
Phone: [phone]
Fax: [phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28018
Phone: [phone]
Fax: [phone]v/\'I\\~paceJabs.com
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in lull,
without the written consent of Pace Analytical Services, Inc,
._.,II~~......~+'~c{~~
J~C~
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
GC/MS Semivolatiles
Semivo1atile Organics Prep/Method: EPA 3545 EPA 8270
Acenaphthene MD ug/kg 400 1.2 09/17/05 06:53 BET 83-32-9
Acenaphthy1ene MD ug/kg 400 1.2 09/17/05 06:53 BET 208-96-8
Anthracene MD ug/kg 400 1.2 09/17/05 06:53 BET 120-12-7
Benzo(k)fluoranthene MD ug/kg 400 1.2 09/17/05 06:53 BET 207-08-9
Benzo(b)fluoranthene MD ug/kg 400 1.2 09/17/05 06:53 BET 205-99-2
Benzo(a)anthracene MD ug/kg 400 1.2 09/17/05 06:53 BET 56-55-3
Benzoic acid MD ug/kg 2000 1.2 09/17/05 06:53 BET 65-85-0
Benzo(g,h,i)pery1ene MD ug/kg 400 1.2 09/17/05 06:53 BET 191-24-2
Benzyl alcohol MD ug/kg 800 1.2 09/17/05 06:53 BET 100-51-6
Benzo(a)pyrene MD ug/kg 400 1.2 09/17/05 06:53 BET 50-32-8
4-Bramophenylpheny1 ether MD ug/kg 400 1.2 09/17/05 06:53 BET 101-55-3
Buty1benzy1phthalate MD ug/kg 400 1.2 09/17/05 06:53 BET 85-68-7
4-Ch1oro-3-methylphenol MD ug/kg 800 1.2 09/17/05 06:53 BET 59-50-7
4-Chloroaniline MD ug/kg 800 1.2 09/17/05 06:53 BET 106-47-8
bis(2-Ch1oroethoxy)methane MD ug/kg 400 1.2 09/17/05 06:53 BET 111-91-1
bis(2-Ch1oroethyl) ether MD ug/kg 400 1.2 09/17/05 06:53 BET 111-44-4
bis(2-Ch1oroisopropy1)ether MD ug/kg 400 1.2 09/17/05 06:53 BET 39638-32-9
2-Chloronaphtha1ene MD ug/kg 400 1.2 09/17/05 06:53 BET 91-58-7
2-Ch1orophenol MD ug/kg 400 1.2 09/17/05 06:53 BET 95-57-8
Date:09/29/05 Page: 9 of 46
1.0 09/15/05 13:13 KBM%17.0
Method:%Moisture
Wet Chemistry
Percent Moisture
Percent Moisture
1.1 09/15/05 03:30 SBB 7439-97-60.0056
Method: EPA 7471
0.028 mg/kg
Mercury, CVAAS, in Soil
Mercury
1.2 09/17/05 04:41 ALV 7440-38-2
1.2 09/17/05 04:41 ALV 7440-39-3
1.2 09/17/05 04:41 ALV 7440-43-9
1.2 09/17/05 04:41 ALV 7440-47-3
1.2 09/17/05 04:41 ALV 7439-92-1
1.2 09/17/05 04:41 ALV 7782-49-2
1.2 09/17/05 04:41 ALV 7440-22-4
09/15/05 04:30
EPA 3050 /EPA 6010
mg/kg 0.60
mg/kg 0.60
mg/kg 0.12
mg/kg 0.24
mg/kg 0.60
mg/kg 0.60
mg/kg 0.24
Prep/Method:
2.0
81.
MD
19.
82.
MD
MD
09/15/05 04:30
Metals
Metals, Trace ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Date Digested
Units Report Limit __m:__--"An""",a1"-VL<z""e""d,--__.BV...,-__,C""AS.........N",-o.!..._ ~ RegLmtResultsParameters
Date Collected:09/14/05 11:05
Date Received:09/14/05 13:34
Project Sample Number: 92103111-009
Matrix: Soil
Lab Sample No: 926093212
Client Sample ID: P-9 (7-8)
Lab Project Number: 92103111
Client Project ID: west Morehead/6228-05-3103
PaceAnalytical Services. Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax: [phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28018
Phone: [phone]
Fax: [phone]
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall notbereproduced,exceptin full,
w~houtthe written consentof PaceAnalyticalServices,Inc.~:e!>.i1~\~
Page: 10 of 46
1.2 09/17/05 06:53 BET 541-73-1
1.2 09/17/05 06:53 BET 106-46-7
1.2 09/17/05 06:53 BET 91-94-1
1.2 09/17/05 06:53 BET 120-83-2
1.2 09/17/05 06:53 BET 84-66-2
1.2 09/17/05 06:53 BET 105-67-9
1.2 09/17/05 06:53 BET 131-11-3
1.2 09/17/05 06:53 BET 84-74-2
1.2 09/17/05 06:53 BET 534-52-1
1.2 09/17/05 06:53 BET 51-28-5
1.2 09/17/05 06:53 BET 121-14-2
1.2 09/17/05 06:53 BET 606-20-2
1.2 09/17/05 06:53 BET 117-84-0
1.2 09/17/05 06:53 BET 122-66-7
1.2 09/17/05 06:53 BET 117-81-7
1.2 09/17/05 06:53 BET 206-44-0
1.2 09/17/05 06:53 BET 86-73-7
1.2 09/17/05 06:53 BET 87-68-3
1.2 09/17/05 06:53 BET 118-74-1
1.2 09/17/05 06:53 BET 77-47-4
1.2 09/17/05 06:53 BET 67-72-1
1.2 09/17/05 06:53 BET 193-39-5
1.2 09/17/05 06:53 BET 78-59-1
1.2 09/17/05 06:53 BET 91-57-6
1.2 09/17/05 06:53 BET 95-48-7
1.2 09/17/05 06:53 BET
1.2 09/17/05 06:53 BET 91-20-3
1.2 09/17/05 06:53 BET 88-74-4
1.2 09/17/05 06:53 BET 99-09-2
1.2 09/17/05 06:53 BET 100-01-6
1.2 09/17/05 06:53 BET 98-95-3
1.2 09/17/05 06:53 BET 88-75-5
1.2 09/17/05 06:53 BET 100-02-7
1.2 09/17/05 06:53 BET 621-64-7
400
400
800
400
400
400
400
400
400
2000
400
400
400
400
400
400
400
400
400
400
400
400
400
400
400
400
400
2000
2000
2000
400
400
2000
400
Report Limit ~Analyzed By CAS No.
400 1.2 09/17/05 06:53 BET 7005-72-3
400 1.2 09/17/05 06:53 BET 218-01-9
400 1.2 09/17/05 06:53 BET 53-70-3
400 1.2 09/17/05 06:53 BET 132-64-9
400 1.2 09/17/05 06:53 BET 95-50-1
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Project Sample Number: 92103111-009
Matrix: Soil
ND
ND
ND
ND
410
ND
640
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
420
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Results
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Date:09/29/05
4-Chloropheny1pheny1 ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dich1orobenzene
1,3-Dich1orobenzene
1,4-Dich1orobenzene
3,3'-Dich1orobenzidine
2,4-Dich1oropheno1
Diethy1phtha1ate'
2,4-Dimethy1pheno1
Dimethy1phtha1ate
Di-n-buty1phtha1ate
4,6-Dinitro-2-methy1pheno1
2,4-Dinitropheno1
2,4-Dinitroto1uene
2,6-Dinitroto1uene
Di-n-octy1phtha1ate
1,2-Dipheny1hydrazine
bis(2-Ethy1hexy1)phthalate
F1uoranthene
Fluorene
Hexach1oro-1,3-butadiene
Hexach1orobenzene
Hexach1orocyc1opentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methy1naphtha1ene
2-Methy1pheno1 (o-Creso1)
3&4-Methy1pheno1
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitropheno1
4-Nitropheno1
N-Nitroso-di-n-propy1amine
Parameters
Date Collected: 09/14/05 11:05
Date Received: 09/14/05 13:34
Lab Sample No: 926093212
Client Sample ID: P-9 (7-8)
Lab Project NUmber: 92103111
Client Project ID: West Morehead/6228-05-3103
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville,NC28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue,Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: 704.875,9091
'aceAna/yticat
1I'I'lIv.pacelabs.com
Charlotte Certification IDs
NGWastewater 12
NGDrinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not bereproduced.exceptinfull,
wrthoutthe written consentof PaceAnalyticalServices. Inc.
,~~'{t~!![JeIaC~
Page: 11 of 46
121 09/22/05 22:53 DLK 67-64-1
121 09/22/05 22:53 DLK 71-43-2
121 09/22/05 22:53 DLK 108-86-1
121 09/22/05 22:53 DLK 74-97-5
121 09/22/05 22:53 DLK 75-27-4
121 09/22/05 22:53 DLK 75-25-2
121 09/22/05 22:53 DLK 74-83-9
121 09/22/05 22:53 DLK 78-93-3
121 09/22/05 22:53 DLK 104-51-8
121 09/22/05 22:53 DLK 135-98-8
121 09/22/05 22:53 DLK 98-06-6
121 09/22/05 22:53 DLK 56-23-5
121 09/22/05 22:53 DLK 108-90-7
121 09/22/05 22:53 DLK 75-00-3
121 09/22/05 22:53 DLK 67-66-3
2
60.3 09/28/05 21:07 KeS 68334-30-5
1.0 09/28/05 21:07 KeS 629-99-2
09/26/05
1.2 09/17/05 06:53 BET 129-00-0
1.2 09/17/05 06:53 BET 120-82-1
1.2 09/17/05 06:53 BET 95-95-4
1.2 09/17/05 06:53 BET 88-06-2
1.0 09/17/05 06:53 BET 4165-60-0
1.0 09/17/05 06:53 BET 321-60-8
1.0 09/17/05 06:53 BET 1718-51-0
1.0 09/17/05 06:53 BET 4165-62-2
1.0 09/17/05 06:53 BET 367-12-4
1.0 09/17/05 06:53 BET 118-79-6
09/15/05
400
400
400
400
12000
600
600
600
600
600
1200
12000
600
600
600
600
600
1200
600
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
3100
MD
MD
Date: 09/29/05
Acetone
Benzene
Bromobenzene
Bromoch1oromethane
Bromodich1oromethane
Bromoform
Bramomethane
2-Butanone (HEX)
n-Buty1benzene
sec-Buty1benzene
tert-Buty1benzene
Carbon tetrachloride
Ch1orobenzene
Ch1oroethane
Chloroform
GC/MS Volatiles
GC/MS VOCs by 8260, low level Method: EPA 8260
%
Prep/Method: EPA 3545 /"EPA 8015
2300 mg/kg 300
o
09/26/05
Report Limit __.m:._Analyzed By CAS No.
400 1.2 09/17/05 06:53 BET 86-30-6
2000 1.2 09/17/05 06:53 BET 87-86-5
400 1.2 09/17/05 06:53 BET 85-01-8
400 1.2 09/17/05 06:53 BET 108-95-2
%
%
%
%
%
%
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Project Sample Number: 92103111-009
Matrix: Soil
MD
MD
MD
MD
MD
MD
MD
MD
33
55
56
53
48
50
09/15/05
Results
GC Semivolatiles
TPH in Soil by 3545/8015
Diesel Fuel
n-Pentacosane (S)
Date Extracted
N-Nitrosodipheny1amine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trich1orobenzene
2,4,5-Trich1oropheno1
2,4,6-Trich1oropheno1
Nitrobenzene-d5 (S)
2-F1uorobipheny1 (S)
Terpheny1-d14 (S)
Phenol-d5 (S)
2-F1uoropheno1 (S)
2,4,6-Tribramopheno1 (S)
Date Extracted
Parameters
Date Collected: 09/14/05 11:05
Date Received: 09/14/05 13:34
Lab Sample No: 926093212
Client Sample ID: P-9 (7-8)
Lab Project Number: 92103111
Client Project ID: West Morehead/6228-05-3103
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville,NG 28804
Phone:[phone]
Fax:[phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Huntersville, NC 28078
Phone:[phone]
Fax:[phone]www.pacefabs.com
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,exceptin full,
without the written consentof PaceAnalyticalServices,Inc.
"'~L~f~~~-t...{'~_U;:J:~!l.~%
Page: 12 of 46
121 09/22/0522:53 DLK 95-50-1
121 09/22/0522:53 DLK 5~1-73-1
121 09/22/0522:53 DLK 106-~6-7
121 09/22/0522:53 DLK 75-71-8
121 09/22/0522:53 DLK 75-34-3
121 09/22/0522:53 DLK 107-06-2
121 09/22/0522:53 DLK 75-35-4
121 09/22/0522:53 DLK 156-59-2
121 09/22/0522:53 DLK 156-60-5
121 09/22/0522:53 DLK 78-87-5
121 09/22/0522:53 DLK 1~2-2B-9
121 09/22/0522:53 DLK 594-20-7
121 09/22/0522:53 DLK 563-5B-6
121 09/22/0522:53 DLK 10061-01-5
121 09/22/0522:53 DLK 10061-02-6
121 09/22/0522:53 DLK 10B-20-3
121 09/22/0522:53 DLK 100-~1-~
121 09/22/0522:53 DLK 87-68-3
121 09/22/0522:53 DLK 591-78-6
121 09/22/0522:53 DLK 98-82-8
121 09/22/0522:53 DLK 99-87-6
121 09/22/0522:53 DLK 75-09-2
121 09/22/0522:53 DLK 108-10-1
121 09/22/0522:53 DLK 163~-0~-4
121 09/22/0522:53 DLK 91-20-3
121 09/22/0522:53 DLK 103-65-1
121 09/22/0522:53 DLK 100-~2-5
121 09/22/0522:53 DLK 630-20-6
121 09/22/0522:53 DLK 79-3~-5
121 09/22/0522:53 DLK 127-1B-~
121 09/22/0522:53 DLK 108-88-3
121 09/22/0522:53 DLK 87-61-6
600
600
600
1200
600
600
600
600
600
600
600
600
600
600
600
600
600
600
6000
600
600
600
6000
600
600
600
600
600
600
600
600
600
Analyzed BY CAS No.
09/22/0522:53 DLK 74-87-3
09/22/0522:53 DLK 95-~9-8
09/22/0522:53 DLK 106-~3-4
09/22/0522:53 DLK 96-12-8
09/22/0522:53 DLK 124-~B-1
09/22/0522:53 DLK 106-93-~
09/22/0522:53 DLK 74-95-3
Report Limit ~
1200 121
600 121
600 121
600 121
600 121
600 121
600 121
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Project Sample Number: 92103111-009
Matrix: Soil
MD
MD
MD
MD
MD
MD
MD
2500
730
4200
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
950
MD
MD
MD
MD
MD
MD
MD
Results
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
Date:09/29/05
Chloromethane
2-Ch1orotoluene
4-Ch1orotoluene
1,2-Dibramo-3-ch1oropropane
Dibramoch1oromethane
1,2-Dibramoethane(EDB)
DibrCllllCllllethane
1,2-Dich1orobenzene
1,3-Dichlorobenzene
1,~-Dichlorobenzene
Dichlorodifluoromat~e
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dich1oroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropylether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene(CUmene)
p-Isopropyltoluene
Methylenechloride
4-Methyl-2-pentanone(MIBK)
Methyl-tert-butylether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
Parameters
Date Collected: 09/1~/0511:05
Date Received: 09/l~/0513:3~
Lab SampleNo: 926093212
Client SampleID: p-9 (7-8)
Lab ProjectNUmber: 92103111
Client ProjectID: West Morehead/622B-05-3103
Pace Analytical Services. Inc.
2225 Riverside Drive
Asheville,NC28804
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville,NC 28078
Phone:[phone]
Fax:[phone]Wl'JII'.paceJsDs,com
Charlotte Certification IDs
NCWastewater 12
NCDrinking Water 37706sc99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced,exceptin lull,
without the written consent 01PaceAnalyticalServices,Inc.
e-~.:-=-'~J-!~~£delaC.~
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SC Environmental 99030
FLNELAP E87648
Palle. 13 of 46Date.09129/05
Lab Project Number:92103111
Client Project ID:West Morehead/6228-05-3103
Lab Sample No:926093212 Project Sample Number: 92103111-009 Date Collected:09/14/05 11:05
Client Sample ID:P-9 (7-8)Matrix: Soil Date Received: 09/14/05 13:34
Parameters Results Units Re120rt Limit ..1lL AnalJ1:zed ~CAS No • ~ RegLmt
1,2,4-Trichlorobenzene MD ug/kg 600 121 09/22/05 22:53 DLK 120-82-1
1,1,1-Trichloroethane MD ug/kg 600 121 09/22/05 22:53 DLK 71-55-6
1,1,2-Trichloroethane MD ug/kg 600 121 09/22/05 22:53 DLK 79-00-5
Trichloroethene MD ug/kg 600 121 09/22/05 22:53 DLK 79-01-6
Trichlorofluoramethane MD ug/kg 600 121 09/22/05 22:53 DLK 75-69-4
1,2,3-Trichloropropane MD ug/kg 600 121 09/22/05 22:53 DLK 96-18-4
1,2,4-Trimethylbenzene 1400 ug/kg 600 121 09/22/05 22:53 DLK 95-63-6
1,3,5-Trimethylbenzene MD ug/kg 600 121 09/22/05 22:53 DLK 108-67-8
Vinyl acetate MD ug/kg 6000 121 09/22/05 22:53 DLK 108-05-4
Vinyl chloride MD ug/kg 1200 121 09/22/05 22:53 DLK 75-01-4
Xylene (Total)1300 l?-g/kg 6.0 1.2 09/22/05 22:53 DLK 1330-20-7
m&:p-xylene MD ug/kg 1200 121 09/22/05 22:53 DLK
o-Xylene MD ug/kg 600 121 09/22/05 22:53 DLK 95-47-6
Toluene-d8 (S)102 %1.0 09/22/05 22:53 DLK 2037-26-5
4-Bramofluorobenzene (S)105 %1.0 09/22/05 22:53 DLK 460-00-4
Dibramofluoramethane (S)88 %1.0 09/22/05 22:53 DLK 1868-53-7
1,2-Dichloroethane-d4 (S)81 %1.0 09/22/05 22:53 DLK 17060-07-0 3
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]VIl'lw.pBcelabs.com
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshallnotbereproduced,exceptinfull,
w~houtthe writtenconsentof PaceAnalyticalServices,Inc.,~j%
~£eIaC'l
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
Lab Project Number: 92103111
Client Project ID:West Morehead/6228-05-3103
Lab Sample No:926093238 Project Sample Number: 92103111-010 Date Collected:09/14/05 12:00
Client Sample ID:P-I0(3)Matrix:Soil Date Received:09/141/05 13:34
~aramet!;!rs,Results Units RellortLimit _1!L_.Analyzed Bv CAS No.~ RegLmt
Metals
Metals, Trace rcp Prep/Method:EPA 3050 EPA 6010
Arsenic 1.9 mg/kg 0.59 1.2 09/17/05 04:46 ALV 7440-38-2
Barium 110 mg/kg 0.59 1.2 09/17/05 04:46 ALV 7440-39-3
Cadmium ND mg/kg 0.12 1.2 09/17/05 04:46 ALV 7440-43-9
Chromium 18.mg/kg 0.24 1.2 09/17/05 04:46 ALV 7440-47-3
Lead 4.9 mg/kg 0.59 1.2 09/17/05 04:46 ALV 7439-92-1
Selenium ND mg/kg 0.59 1.2 09/17/05 04:46 ALV 7782-49-2
Silver ND mg/kg 0.24 1.2 09/17/05 04:46 ALV 7440-22-4
Date Digested 09/15/05 04:30 09/15/05 04:30
Mercury, CVAAS, in Soil Method: EPA 7471
Mercury 0.011 mg/kg 0.0058 1.2 09/15/05 03:30 SHB 7439-97-6
wet Chemistry
Percent Moisture Method:%Moisture
Percent Moisture 18.9 %1.0 09/15/05 13:14 KBM
GC/MS Semivolatiles
Semivolatile Organics Prep/Method: EPA 3545 I EPA 8270
Acenaphthene ND ug/kg 410 1.2 09/17/05 02:30 BET 83-32-9
Acenaphthylene ND ug/kg 410 1.2 09/17/05 02:30 BET 208-96-8
Anthracene ND ug/kg 410 1.2 09/17/05 02:30 BET 120-12-7
Benzo(k)f1uoranthene ND ug/kg 410 1.2 09/17/05 02:30 BET 207-08-9
Benzo(b)fluoranthene ND ug/kg 410 1.2 09/17/05 02:30 BET 205-99-2
Benzo(a) anthracene ND ug/kg 410 1.2 09/17/05 02:30 BET 56-55-3
Benzoic acid ND ug/kg 2000 1.2 09/17/05 02:30 BET 65-85-0
Benzo(g,h,i)pery1ene ND ug/kg 410 1.2 09/17/05 02:30 BET 191-24-2
Benzyl alcohol ND ug/kg 810 1.2 09/17/05 02:30 BET 100-51-6
Benzo(a)pyrene ND ug/kg 410 1.2 09/17/05 02:30 BET 50-32-8
4-Bramophenylphenyl ether ND ug/kg 410 1.2 09/17/05 02:30 BET 101-55-3
Butylbenzylphthalate ND ug/kg 410 1.2 09/17/05 02:30 BET 85-68-7
4-Chloro-3-methylpheno1 ND ug/kg 810 1.2 09/17/05 02:30 BET 59-50-7
4-Chloroaniline ND ug/kg 810 1.2 09/17/05 02:30 BET 106-47-8
bis(2-Ch1oroethoxy)methane ND ug/kg 410 1.2 09/17/05 02:30 BET 111-91-1
bis(2-Ch1oroethy1) ether ND ug/kg 410 1.2 09/17/05 02:30 BET 111-44-4
bis(2-Ch1oroisopropyl)ether ND ug/kg 410 1.2 09/17/05 02:30 BET 39638-32-9
2-Ch1oronaphtha1ene ND ug/kg 410 1.2 09/17/05 02:30 BET 91-58-7
2-Ch1oropheno1 ND ug/kg 410 1.2 09/17/05 02:30 BET 95-57-8
Date: 09/29/05 Page: 14 of 46
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]\f1l'lw.pa()ela.b~.com
Charlotte Certification IDs
NCWastewater 12
NCDrinking Water 37706
SC 99006
FLNELAP EB7627
REPORT OF LABORATORY ANALYSIS
This reportshallnot be reproduced,exceptin full,
without thewritten consentof PaceAnalyticalServices,Inc,
t~\~
Page: 15 of 46
1.2 09/17/05 02:30 BET 218-01-9
1.2 09/17/05 02:30 BET 53-70-3
1.2 09/17/05 02:30 BET 132-64-9
1.2 09/17/05 02:30 BET 95-50-1
1.2 09/17/05 02:30 BET 541-73-1
1.2 09/17/05 02:30 BET 106-46-7
1.2 09/17/05 02:30 BET 91-94-1
1.2 09/17/05 02:30 BET 120-83-2
1.2 09/17/05 02:30 BET 84-66-2
1.2 09/17/05 02:30 BET 105-67-9
1.2 09/17/05 02:30 BET 131-11-3
1.2 09/17/05 02:30 BET 84-74-2
1.2 09/17/05 02:30 BET 534-52-1
1.2 09/17/05 02:30 BET 51-28-5
1.2 09/17/05 02:30 BET 121-14-2
1.2 09/17/05 02:30 BET 606-20-2
1.2 09/17/05 02:30 BET 117-84-0
1.2 09/17/05 02:30 BET 122-66-7
1.2 09/17/05 02:30 BET 117-81-7
1.2 09/17/05 02:30 BET 206-44-0
1.2 09/17/05 02:30 BET 86-73-7
1.2 09/17/05 02:30 BET 87-68-3
1.2 09/17/05 02:30 BET 118-74-1
1.2 09/17/05 02:30 BET 77-47-4
1.2 09/17/05 02:30 BET 67-72-1
1.2 09/17/05 02:30 BET 193-39-5
1.2 09/17/05 02:30 BET 78-59-1
1.2 09/17/05 02:30 BET 91-57-6
1.2 09/17/05 02:30 BET 95-48-7
1.2 09/17/05 02:30 BET
1.2 09/17/05 02:30 BET 91-20-3
1.2 09/17/05 02:30 BET 88-74-4
1.2 09/17/05 02:30 BET 99-09-2
1.2 09/17/05 02:30 BET 100-01-6
1.2 09/17/05 02:30 BET 98-95-3
1.2 09/17/05 02:30 BET 88-75-5
1.2 09/17/05 02:30 BET 100-02-7
1.2 09/17/05 02:30 BET 621-64-7
410
410
410
410
410
410
810
410
410
410
410
410
410
2000
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
2000
2000
2000
410
410
2000
410
Report Limit ~Analyzed By CAS No.
410 1.2 09/17/05 02:30 BET 7005-72-3
units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Project Sample Number: 92103111-010
Matrix: Soil
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Results
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SC Environmental 99030
FL NELAP EB7648
Date:09/29/05
4-Ch1orophenylphenylether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
1,2-Diphenylhydrazine
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlo.robenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol (o-Cresol)
3&4-Methylphenol
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
Parameters
Date Collected: 09/14/05 12:00
Date Received: 09/14/05 13:34
Lab Sample No: 926093238
Client Sample ID: P-10(3)
Lab Project Number: 92103111
Client Project ID: west Morehead/6228-05-3103
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville,NC 28804
Phone: [phone]
Fax: [phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax:[phone]
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not bereproduced,exceptin full,
w~hOutIhewritten consentof PaceAnalyticalServices,Inc.
Page, 16 of 46
1.2 09/20/05 14:55 DLK 67-64-1
1.2 09/20/05 14:55 DLK 71-43-2
1.2 09/20/05 14:55 DLK 108-86-1
1.2 09/20/05 14:55 DLK 74-97-5
1.2 09/20/0514:55 DLK 75-27-4
1.2 09/20/0514:55 DLK 75-25-2
1.2 09/20/05 14:55 DLK 74-83-9
1.2 09/20/0514:55 DLK 78-93-3
1.2 09/20/05 14:55 DLK 104-51-8
1.2 09/20/05 14:55 DLK 135-98-8
1.2 09/20/05 14:55 DLK 98-06-6
1.2 09/20/05 14:55 DLK 56-23-5
1.2 09/20/05 14:55 DLK 108-90-7
1.2 09/20/05 14:55 DLK 75-00-3
1.2 09/20/0514:55 DLK 67-66-3
1.2 09/20/05 14:55 DLK 74-87-3
1.2 09/20/05 14:55 DLK 95-49-8
1.2 09/20/05 14:55 DLK 106-43-4
1.2 09/20/0514:55 DLK 96-12-8
1.2 09/20/05 14:55 DLK 124-48-1
1.2 09/20/05 14:55 DLK 106-93-4
4
1.2 09/17/05 02:30 BET 108-95-2
1.2 09/17/05 02:30 BET 129-00-0
1.2 09/17/05 02:30 BET 120-82-1
1.2 09/17/05 02:30 BET 95-95-4
1.2 09/17/05 02:30 BET 88-06-2
1.0 09/17/05 02:30 BET 4165-60-0
1.0 09/17/05 02:30 BET 321-60-8
1.0 09/17/0502:30 BET 1718-51-0
1.0 09/17/05 02:30 BET 4165-62-2
1.0 09/17/05 02:30 BET 367-12-4
1.0 09/17/05 02:30 BET 118-79-6
09/15/05
120
6.2
6.2
6.2
6.2
6.2
12.
120
6.2
6.2
6.2
6.2
6.2
12.
6.2
12.
6.2
6.2
6.2
6.2
6.2
410
410
410
410
410
Report Lindt _.m:_Analyzed By'CAS No.
410 1.2 09/17/05 02:30 BET 86-30-6
2000 1.2 09/17/05 02:30 BET 87-86-5
410 1.2 09/17/05 02:30 BET 85-01-8
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Method: EPA 8260
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
%
%
%
%
%
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
Project Sample NUmber: 92103111-010
Matrix: Soil
ND
ND
ND
ND
ND
ND
ND
ND
49
47
53
35
26
22
09/15/05
Results
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Date,09/29/05
GC/MS Volatiles
GC/MS VOCs by 8260, low level
Acetone
Benzene
Bromobenzene
Bromochloramethane
Bromodichloramathane
Bromoform
Bromamethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane(EDB)
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
l,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl(S)
Terphenyl-d14 (S)
Phenol-d5 (S)
2-Fluorophenol(S)
2,4,6-Tribramophenol(S)
Date Extracted
Parameters
Date Collected: 09/14/05 12:00
Date Received: 09/14/05 13:34
Lab Sample No: 926093238
Client Sample ID: P-10(3)
Lab ProjectNUmber: 92103111
Client Project ID: West Morehead/6228-05-3103
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax: [phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28018
Phone: [phone]
Fax: [phone]
see Analyticat"
Wl'I\!!.paceJaDs.oom
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP EB7627
REPORT OF LABORATORY ANALYSIS
This reportshall notbe reproduced.exceptinfull,
w~houtthe written consentof PaceAnalyticalServices.Inc.
Page:17 of 46
5
1.2 09/20/05 14:55 DLK 95-50-1
1.2 09/20/05 14:55 DLK 541-73-1
1.2 09/20/05 14:55 DLK 106-46-7
1.2 09/20/05 14:55 DLK 75-71-8
1.2 09/20/05 14:55 DLK 75-34-3
1.2 09/20/05 14:55 DLK 107-06-2
1.2 09/20/05 14:55 DLK 75-35-4
1.2 09/20/05 14:55 DLK 156-59-2
1.2 09/20/05 14:55 DLK 156-60-5
1.2 09/20/05 14:55 DLK 78-87-5
1.2 09/20/05 14:55 DLK 142-28-9
1.2 09/20/05 14:55 DLK 594-20-7
1.2 09/20/05 14:55 DLK 563-58-6
1.2 09/20/05 14:55 DLK 10061-01-5
1.2 09/20/05 14:55 DLK 10061-02-6
1.2 09/20/05 14:55 DLK 108-20-3
1.2 09/20/05 14:55 DLK 100-41-4
1.2 09/20/05 14:55 DLK 87-68-3
1.2 09/20/05 14:55 DLK 591-78-6
1.2 09/20/05 14:55 DLK 98-82-8
1.2 09/20/05 14:55 DLK 99-87-6
1.2 09/20/05 14:55 DLK 75-09-2
1.2 09/20/05 14:55 DLK 108-10-1
1.2 09/20/05 14:55 DLK 1634-04-4
1.2 09/20/05 14:55 DLK 91-20-3
1.2 09/20/05 14:55 DLK 103-65-1
1.2 09/20/05 14:55 DLK 100-42-5
1.2 09/20/05 14:55 DLK 630-20-6
1.2 09/20/05 14:55 DLK 79-34-5
1.2 09/20/05 14:55 DLK 127-18-4
1.2 09/20/05 14:55 DLK 108-88-3
1.2 09/20/05 14:55 DLK 87-61-6
1.2 09/20/05 14:55 DLK 120-82-1
1.2 09/20/05 14:55 DLK 71-55-6
1.2 09/20/05 14:55 DLK 79-00-5
1.2 09/20/05 14:55 DLK 79-01-6
1.2 09/20/05 14:55 DLK 75-69-4
1.2 09/20/05 14:55 DLK 96-18-4
6.2
6.2
6.2
12.
6.2
6.2
6.2
6.2
6.2
6.2
6.2
6.2
6.2
6.2
6.2
6.2
6.2
6.2
62.
6.2
6.2
6.2
62.
6.2
6.2
6.2
6.2
6.2
6.2
6.2
6.2
6.2
6.2
6.2
6.2
6.2
6.2
6.2
Report Limit _m:_Analyzed By CAS No.
6.2 1.2 09/20/05 14:55 DLK 74-95-3
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Project Sample Number: 92103111-010
Matrix: Soil
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Results
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Date:09/29/05
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-l,3-Dichloropropene
trans-1,3~Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoramethane
1,2,3-Trichloropropane
Parameters
Date Collected: 09/14/05 12:00
Date Received: 09/-14/0513:34
Lab Sample No: 926093238
Client Sample ID: P-10(3)
Lab Project Number: 92103111
Client Project ID: west Morehead/6228-05-3103
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone:[phone]
Fax:[phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax:[phone]www.pacetabs.ccm
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not bereproduced,exceptin full,
wtthout Ihewritten consentof PaceAnalyticalServices, Inc.
c.l~."~'!',f,,~_e:;l5{J~r~
Page: 18 of 46
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Date:09/29/05
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&:p-Xy1ene
o-Xylene
Toluene-d8 (S)
4-Bramofluorobenzene (S)
Dihramofluoramethane (S)
1,2-Dichloroethane-d4 (S)
Parameta.rs
Lab Sample No: 926093238
Client Sample ID: P-10(3)
Lab Project Number:92103111
Client Project ID:west Morehead/6228-05-3103
Project Sample Number: 92103111-010 Date Collected:09/14/05 12:00
Matrix: Soil Date Received:09/14/05 13:34
Results units Rel20rtLimit __m:_Ari!!,l:!£zed~CAS No.2Y§L ReqLmt
NO ug/kg 6.2 1.2 09/20/05 14:55 DLK 95-63-6
NO ug/kg 6.2 1.2 09/20/05 14:55 DLK 108-67-8
NO ug/kg 62.1.2 09/20/05 14:55 DLK 108-05-4
NO ug/kg 12. 1.2 09/20/05 14:55 DLK 75-01-4
NO ug/kg 6.2 1.2 09/20/05 14:55 DLK 1330-20-7
NO ug/kg 12. 1.2 09/20/05 14:55 DLK
NO ug/kg 6.2 1.2 09/20/05 14:55 DLK 95-47-6
99 %1.0 09/20/05 14:55 DLK 2037-26-5
92 %1.0 09/20/05 14:55 DLK 460-00-4
101 %1.0 09/20/05 14:55 DLK 1868-53-7
90 %1.0 09/20/05 14:55 DLK 17060-07-0
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone:[phone]
Fax: [phone]
Pace Analytical Services. Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]WlVW.pacelabs.rom
Charlotte Certification IDs
NCWastewater 12
NGDrinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
.Thisreportshallnotbereproduced,exceptin full,
wtthoutthewrittenconsentof PaceAnalyticalServices,Inc.
Q'~!'~~~l.:::_.u...~"'.~!J.~].~
Page: 19 of 46
6.7 09/17/05 08:45 BET 83-32-9
6.7 09/17/05 08:45 BET 208-96-8
6.7 09/17/05 08:45 BET 120-12-7
66.6 09/17/05 08:45 BET 207-08-9
66.6 09/17/05 08:45 BET 205-99-2
66.6 09/17/05 08:45 BET 56-55-3
6.7 09/17/05 08:45 BET 65-85-0
6.7 09/17/05 08:45 BET 191-24-2
6.7 09/17/05 08:45 BET 100-51-6
66.6 09/17/05 08:45 BET 50-32-8
6.7 09/17/05 08:45 BET 101-55-3
6.7 09/17/05 08:45 BET 85-68-7
6.7 09/17/05 08:45 BET 59-50-7
6.7 09/17/05 08:45 BET 106-47-8
6.7 09/17/05 08:45 BET 111-91-1
6.7 09/17/05 08:45 BET 111-44-4
6.7 09/17/05 08:45 BET 39638-32-9
6.7 09/17/05 08:45 BET 91-58-7
6.7 09/17/05 08:45 BET 95-57-8
1.0 09/15/05 13:15 KBM
1.3 09/15/05 03:30 SHe 7439-97-6
1.2 09/17/05 04:50 ALV 7440-38-2
1.2 09/17/05 04:50 ALV 7440-39-3
1.2 09/17/05 04:50 ALV 7440-43-9
1.2 09/17/05 04:50 ALV 7440-47-3
1.2 09/17/05 04:50 ALV 7439-92-1
1.2 09/17/05 04:50 ALV 7782-49-2
1.2 09/17/05 04:50 ALV 7440-22-4
09/15/05 04:30
2200
2200
22000
22000
22000
11000
2200
4400
22000
2200
2200
4400
4400
2200
2200
2200
2200
2200
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ND
22000
36000
39000
50000
ND
8900
ND
49000
ND
ND
ND
ND
ND
ND
ND
ND
ND
Prep/Method: EPA 3545 / EPA 8270
20000 ug/kg 2200
0.0067
EPA 6010
0.61
0.61
0.12
0.24
0.61
0.61
0.24
Method:%Moisture
25.0 %
Method: EPA 7471
0.11 mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
ND
46.
120
ND
ND
09/15/05 04:30
Prep/Method: EPA 3050
17.mg/kg
130 mg/kg
Units Report Limit __m:______.,Ana""",l...,y...z""e""d___.,Bv:L...__,C""AS."._""No",_,__._ ~ RegLmt
Project Sample Number: 92103111-011
Metrix: Soil
Results
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Date:09/29/05
GC/MS Semivolatiles
Semivo1ati1e Organics
Acenaphthene
Acenaphthylene
Anthracene
Benzo(k)fluoranthene
Benzo(b)f1uoranthene
Benzo (a)anthracene
Benzoic acid
Benzo(g,h,i)pery1ene
Benzyl alcohol
Benzo(a)pyrene
4-Bramopheny1pheny1 ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Ch10roeniline
bis(2-Chloroethoxy)methane
bis(2-Ch10roethy1) ether
bis(2-Ch10roisopropy1) ether
2-Ch10ronaphthalene
2-Ch10ropheno1
Wet Chemistry
Percent Moisture
Percent Moisture
Mercury, CVAAS, in Soil
Mercury
Metals
Metals, Trace ICP
Arsenic
Barium
Cadmium
Chramium
Lead
Selenium
Silver
Date Digested
Date Collected: 09/14/05 12:15
Date Received: 09/14/05 13:34
Lab Sample No: 926093246
Client Sample ID: P-11(3)
Lab Project Number: 92103111
Client Project ID: West Morehead/6228-05-3103
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax: [phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]WWIl!.pacetabs.oom
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced.exceptin full.
withoutthe written consentof PaceAnalyticalServices.Inc.
." ~~~~oC'~
lS:_.l'_'~.'''''''!;,.~tneIaC~
Page: 20 of 46
66.6 09/17/05 08:45 BET 218-01-9
6.7 09/17/05 08:45 BET 53-70-3
6.7 09/17/05 08:45 BET 132-64-9
6.7 09/17/05 08:45 BET 95-50-1
6.7 09/17/05 08:45 BET 541-73-1
6.7 09/17/05 08:45 BET 106-46-7
6.7 09/17/05 08:45 BET 91-94-1
6.7 09/17/05 08:45 BET 120-83-2
6.7 09/~7/05 08:45 BET 84-66-2
6.7 09/17/05 08:45 BET 105-67-9
6.7 09/17/05 08:45 BET 131-11-3
6.7 09/17/05 08:45 BET 84-74-2
6.7 09/17/05 08:45 BET 534-52-1
6.7 09/17/05 08:45 BET 51-28-5
6.7 09/17/05 08:45 BET 121-14-2
6.7 09/17/05 08:45 BET 606-20-2
6.7 09/17/05 08:45 BET 117-84-0
6.7 09/17/05 08:45 BET 122-66-7
6.7 09/17/05 08:45 BET 117-81-7
66.6 09/17/05 08:45 BET 206-44-0
6.7 09/17/05 08:45 BET 86-73-7
6.7 09/17/05 08:45 BET 87-68-3
6.7 09/17/05 08:45 BET 118-74-1
6.7 09/17/05 08:45 BET 77-47-4
6.7 09/17/05 08:45 BET 67-72-1
6.7 09/17/05 08:45 BET 193-39-5
6.7 09/17/05 08:45 BET 78-59-1
6.7 09/17/05 08:45 BET 91-57-6
6.7 09/17/05 08:45 BET 95-48-7
6.7 09/17/05 08:45 BET
6.7 09/17/05 08:45 BET 91-20-3
6.7 09/17/05 08:45 BET 88-74-4
6.7 09/17/05 08:45 BET 99-09-2
6.7 09/17/05 08:45 BET 100-01-6
6.7 09/17/05 08:45 BET 98-95-3
6.7 09/17/05 08:.45BET 88-75-5
6.7 09/17/05 08:45 BET 100-02-7
6.7 09/17/05 08:45 BET 621-64-7
22000
2200
2200
2200
2200
2200
4400
2200
2200
2200
2200
2200
2200
11000
2200
2200
2200
2200
2200
22000
2200
2200
2200
2200
2200
2200
2200
2200
2200
2200
2200
11000
11000
11000
2200
2200
11000
2200
Report Limit __m:_Analyzed By CAS No.
2200 6.7 09/17/05 08:45 BET 7005-72-3
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Project Sample NUmber: 92103111-011
Matrix: Soil
NO
50000
5500
10000
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
100000
20000
NO
NO
NO
NO
9700
NO
3900
NO
NO
6700
NO
NO
NO
NO
NO
NO
NO
Results
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
Date:09/29/05
4-Ch1oropheny1pheny1ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
l,2-Dich1orobenzene
l,3-Dich1orobenzene
l,4-Dich1orobenzene
3,3'-Dich1orobenzidine
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphtha1ate
4,6-Dinitro~2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
l,2-Diphenylhydrazine
bis(2-Ethy1hexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Bexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
1ndeno(l,2,3-cd)pyrene
1sophorone
2-Methylnaphthalene
2-Methy1phenol (o-Cresol)
3&4-Methylphenol
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitropheno1
N-Nitroso-di-n-propylamdne
Parameters
Date Collected: 09/14/05 12:15
Date Received: 09/14/05 13:34
Lab Sample No: 926093246
Client Sample 1D: P-11(3)
Lab Project Number: 92103111
Client Project 1D: west Morehead/6228-05-3103
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]VilWt;pacefabs.ccm
Charlotte Certification IPs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced,exceptin full,
without the written consentof PaceilnalyticalServices,Inc.
ooac\~'!.1~{1:;....:t'
:r;....
~.!;
Pege: 21 of 46
1.3 09/20/05 18:16 DLK 67-64-1
1.3 09/20/05 18:16 DLK 71-43-2
1.3 09/20/05 18:16 DLK 108-86-1
1.3 09/20/05 18:16 DLK 74-97-5
1.3 09/20/05 18:16 DLK 75-27-4
1.3 09/20/05 18:16 DLK 75-25-2
1.3 09/20/05 18:16 DLK 74-83-9
1.3 09/20/05 18:16 DLK 78-93-3
1.3 09/20/05 18:16 DLK 104-51-8
1.3 09/20/05 18:16 DLK 135-98-8
1.3 09/20/05 18:16 DLK 98-06-6
1.3 09/20/05 18:16 DLK 56-23-5
1.3 09/20/05 18:16 DLK 108-90-7
1.3 09/20/05 18:16 DLK 75-00-3
1.3 09/20/05 18:16 DLK 67-66-3
1.3 09/20/05 18:16 DLK 74-87-3
1.3 09/20/05 18:16 DLK 95-49-8
1.3 09/20/05 18:16 DLK 106-43-4
1.3 09/20/05 18:16 DLK 96-12-8
1.3 09/20/05 18:16 DLK 124-48-1
1.3 09/20/05 18:16 DLK 106-93-4
66.6 09/17/05 08:45 BET 85-01-8
6.7 09/17/05 08:45 BET 108-95-2
66.6 09/17/05 08:45 BET 129-00-0
6.7 09/17/05 08:45 BET 120-82-1
6.7 09/17/05 08:45 BET 95-95-4
6.7 09/17/05 08:45 BET 88-06-2
1.0 09/17/05 08:45 BET 4165-60-0
1.0 09/17/05 08:45 BET 321-60-8
1.0 09/17/05 08:45 BET 1718-51-0
1.0 09/17/05 08:45 BET 4165-62-2
1.0 09/17/05 08:45 BET 367-12-4
1.0 09/17/05 08:45 BET 118-79-6
09/15/05
130
6.7
6.7
6.7
6.7
6.7
13.
130
6.7
6.7
6.7
6.7
6.7
13.
6.7
13.
6.7
6.7
6.7
6.7
6.7
22000
2200
22000
2200
2200
2200
Report Limit ~Analyzed By CAS No.
2200 6.7 09/17/05 08:45 BET 86-30-6
11000 6.7 09/17/05 08:45 BET 87-86-5
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
Method: EPA 8260
NO ug/kg
NO ug/kg
NO ug/kg
%
%
%
%
%
%
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Project Sample Number: 92103111-011
Matrix: Soil
NO
NO
110000
NO
97000
NO
NO
NO
81
83
85
59
42
48
09/15/05
Results
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SCEnvironmental 99030
FL NELAP E87648
Date:09/29/05
GC/MS Volatiles
GC/MS VOCs by 8260, low level
Acetone
Benzene
Bromobenzene
Bramoch1oramethane
Bramodich1oromethane
Bromoform
BrOlllCllllethane
2-Butanone (MEK)
n-Buty1benzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Ch1oroethane
Chloroform
Chloromethane
2-Chloroto1uene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromoch1oramethane
1,2-Dibramoethane (EDB)
N-Nitrosodipheny1amine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichloropheno1
2,4,6-Trichloropheno1
Nitrobenzene-d5 (S)
2-F1uorobipheny1 (S)
Terphenyl-d14 (S)
Pheno1-d5 (S)
2-F1uorophenol (S)
2,4,6-Tribromopheno1(S)
Date Extracted
Paramete:t"s
Date Collected: 09/14/05 12:15
Date Received: 09/14/05 13:34
Lab Sample No: 926093246
Client Sample ID: P-11(3)
Lab Project Number: 92103111
Client Project ID: West Morehead/6228-05-3103
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]wL'lw.paceJabs.com
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not bereproduced.exceptin full,
wijhout Ihewritten consentof PaceAnalyticalServices.Inc.
Page: 22 of 46
5
1.3 09/20/05 18:16 DLK 156-59-2
1.3 09/20/05 18:16 DLK 156-60-5
1.3 09/20/05 18:16 DLK 78-87-5
1.3 09/20/05 18:16 DLK 142-28-9
1.3 09/20/05 18:16 DLK 594-20-7
1.3 09/20/05 18:16 DLK 563-58-6
1.3 09/20/05 18:16 DLK 10061-01-5
1.3 09/20/05 18:16 DLK 10061-02-6
1.3 09/20/05 18:16 DLK 108-20-3
1.3 09/20/05 18:16 DLK 100-41-4
1.3 09/20/05 18:16 DLK 87-68-3
1.3 09/20/05 18:16 DLK 591-78-6
1.3 09/20/05 18:16 DLK 98-82-8
1.3 09/20/05 18:16 DLK 99-87-6
1.3 09/20/05 18:16 DLK 75-09-2
1.3 09/20/05 18:16 DLK 108-10-1
1.~.09/20/0518:16 DLK 1634-04-4
1.3 09/20/05 18:16 DLK 91-20-3
1.3 09/20/05 18:16 DLK 103-65-1
1.3 09/20/05 18:16 DLK 100-42-5
1.3 09/20/05 18:16 DLK 630-20-6
1.3 09/20/05 18:16 DLK 79-34-5
1.3 09/20/05 18:16 DLK 127-18-4
1.3 09/20/05 18:16 DLK 108-88-3
1.3 09/20/05 18:16 DLK 87-61-6
1.3 09/20/05 18:16 DLK 120-82-1
1.3 09/20/05 18:16 DLK 71-55-6
1.3 09/20/05 18:16 DLK 79-00-5
1.3 09/20/05 18:16 DLK 79-01-6
1.3 09/20/05 18:16 DLK 75-69-4
1.3 09/20/05 18:16 DLK 96-18-4
6.7
6.7
6.7
6.7
6.7
6.7
6.7
6.7
6.7
6.7
6.7
67.
6.7
6.7
6.7
67.
6.7
6.7
6.7
6.7
6.7
6.7
6.7
6.7
6.7
6.7
6.7
6.7
6.7
6.7
6.7
Report Limit _m:._Analyzed By CAS No.
6.7 1.3 09/20/05 18:16 DLK 74-95-3
6.7 1.3 09/20/05 18:16 DLK 95-50-1
6.7 1.3 09/20/05 18:16 DLK 541-73-1
6.7 1.3 09/20/05 18:16 DLK 106-46-7
13. 1.3 09/20/05 18:16 DLK 75-71-8
6.7 1.3 09/20/05 18:16 DLK 75-34-3
6.7 1.3 09/20/05 18:16 DLK 107-06-2
6.7 1.3 09/20/05 18:16 DLK 75-35-4
units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Project Sample Number: 92103111-011
Matrix: Soil
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
63.
NO
NO
69.
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
Results
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SCEnvironmental 99030
FLNELAP E87648
Date:09/29/05
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoramethane
1,1-Dichloroethane
1,2-Dich1oroethane
1,1-Dichloroethene
cis-l,2-Dichloroethene
trans-l,2-Dichloroethene
1,2-Dichloropropane
1,3-Dich1oropropane
2,2-Dich1oropropane
1,1-Dich1oropropene
cis-1,3-Dichloropropene
trans-l,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexach1oro-l,3-butadiene
2-Hexanone
Isopropy1benzene (Cumene)
p-Isopropy1toluene
Methylene chloride
4-Methyl-2-pentanone(MIBK)
Methyl-tert-butylether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrach1oroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trich1orobenzene
1,1,I-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorof1uoramethane
1,2,3-Trich1oropropane
Parameters
Date Collected: 09/14/05 12:15
Date Received: 09/14/05 13:34
Lab Sample No: 926093246
Client Sample ID: P-ll(3)
Lab Project Number: 92103111
Client Project ID: West Morehead/6228-05-3103
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]wl'/w.p80elabs.oom
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshallnot be reproduced,exceptin full,
withoutthewrittenconsentof PaceAnalyticalServices,Inc.
Asheville Certification IDs
NCWastewater 40
NGDrinking Water 37712
SC Environmental 99030
FLNELAP E87648
Page: 23 of 46Date:09/29/05
Lab Project Number:92103111
Client Project ID: West Morehead/6228-05-3103
Lab SaJJ;lleNo:926093246 Project Sample Number: 92103111-011 Date Collected:09/14/05 12:15
Client Sample ID: P-ll(3)Matrix:Soil Date Received: 09/14/05 13:34
Paramet!!rs Results Units Re[!ortLimit ..J1[_Analvzed :!'!Y CAS No .Qual ReaLmt
1,2,4-Trimethylbenzene 8.3 ug/kg 6.7 1.3 09/20/05 18:16 DLK 95-63-6
1,3,5-Trimethylbenzene NO ug/kg 6.7 1.3 09/20/05 18:16 DLK 108-67-8
Vinyl acetate NO ug/kg 67. 1.3 09/20/05 18:16 DLK 108-05-4
Vinyl chloride NO ug/kg 13. 1.3 09/20/05 18:16 DLK 75-01-4
Xylene (Total)NO ug/kg 6.7 1.3 09/20/05 18:16 DLK 1330-20-7
m&:p-Xylene NO ug/kg 13. 1.3 09/20/05 18:16 DLK
o-Xy1ene NO ug/kg 6.7 1.3 09/20/05 18:16 DLK 95-47-6
Toluene-d8 (S)91 %1.0 09/20/05 18:16 DLK 2037-26-5
4~Bromof1uorobenzene (S)74 %1.0 09/20/05 18:16 DLK 460-00-4 6
Dibromofluoromethane (S)112 %1.0 09/20/05 18:16 DLK 1868-53-7
1,2-Dichloroethane-d4(S)111 %1.0 09/20/05 18:16 DLK 17060-07-0
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone:[phone]
Fax:[phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite too
Huntersville, NC28078
Phone: [phone]
Fax: [phone]
Charlotte Certification IDs
NCWastewater 12
NCDrinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,exceptinfull,
wijhoul the written consentof PaceAnalyticalServices,Inc.~:s:::·t~{neraC~
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SC Environmental 99030
FL NELAP E87648
Page: 24 of 46Date:09/29/05
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
(S) SUrrogate
[1] The surrogate recovery was outside QC acceptance limits due to matrix interference.
[2] Surrogate standards were not recovered due to 'sampledilution.
[3] The sample was diluted to reduce matrix interference, resulting in elevated reporting limits.
[4] Acid surrogate recovery outside of control limits. The data was accepted based on valid recovery of the two
remaining acid surrogates.
[5] Cammon laboratory contaminant.
[6] Low surrogate recovery was confirmed as a matrix effect by a second analysis.
2-Chloroethyl vinyl ether has been shown to degrade in the presence of acid.
Depending on the moisture content the PRLs can be elevated for all soil samples reported on a dry weight basis.
All pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate
hold time.
Method 9071B modified to use ABE.
Dilution factor shown represents the factor applied to the reported result and reporting limit due to changes
in sample preparation, dilution of the extract, or moisture content
PARAMETER FOOTNOTES
Lab Project Number: 92103111
Client project ID: west Morehead/622B-05-3103
YIIY'tI'.pacefabs,com
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshallnotbereproduced.exceptin full.
without thewrittenconsentofPaceAnalyticalServices.Inc.,~:t:~~€~lltRl\..l\
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SC Environmental 99030
FLNELAP E8764B
Page: 25 of 46Date: 09/29/05
~TRIX SPIKE &MATRIX SPIKE DUPLICATE: 926098005 926098013
926093105 Spike MS MSD MS MSD
Parameter Units Result Cone. Result Result %Ree %Ree RPD Footnotes
Diesel Fuel mg/kg 0.6187 192.00 118.4 127.2 61 66 7
n-Pentacosane (S)80 80
SAMPLE DUPLICATE: 926098021
926093121 DUP
Parameter Units Result Result RPD Footnotes
Diesel Fuel mg/kg ND ND NC
n-Pentacosane (S)%84 89
Spike LCS LCS
Parameter Units Cone. Result %Ree Footnotes
Diesel Fuel mg/kg 166.70 148.0 89
n-Pentaeosane (S)91
LABORATORY CONTROL SAMPLE: 926097999
Blank Reporting
Par!!m!ter units Result Limit Footnotes
Diesel Fuel mg/kg ND 5.0
n-Pentacosane (S)%85
926093170926093154926093147926093139926093121926093113926093105
926093188
METHOD BLANK: 926097981
Associated Lab Samples:
926093188926093170
Analysis Method: EPA 8015
Analysis Description: TPH in Soil by 3545/8015
926093113 926093121 926093139 926093147926093105
926093154
QC Batch: 137492
QC Batch Method: EPA 3545
Associated Lab Samples:
Lab Project Number: 92103111
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax:[phone]
Pace Analytical Services. Inc.
9800 Kincey Avenue,Suite 100
Huntersville,NC 28078
Phone: [phone]
Fax: [phone]
Charlotte Certification IDs
NCWastewater 12
NCDrinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshallnot bereproduced.exceptin tull,
wtthoutthewritten consentof PaceAnalyticalServices,Inc.
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712-
SCEnvironmental 99030
FL NELAP EB764B
Page: 26 of 46Date:09/29/05
926138157 DUP
Parameter units Result Result ,RPD Footnotes
Diesel Fuel mg/kg 20.00 10.00 64 1
n-Pentacosane (S)%113 90
SAMPLE DUPLICATE: 926144247
93101
FootnotesRPD
10
%Rec %Rec
94 85
926138090
ResultunitsParameter
MSDMSMSD
Result
168.4
MS
Result
186.3
Spike
Conc.
197.600.6031mg/kgDiesel Fuel
n-Pentacosane (S)
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 926144221 926144239
mg/kgDiesel Fuel
n-Pentacosane (S)
Conc. Result
166.70 173.7
UnitsPar8lllBter
LCS
%Rec Footnotes
104
113
LCSSpike
LABORATORY CONTROL SAMPLE:926144213
Blank Reporting
P!!,;!;:~ter units Result Limit Footnotes
Diesel Fuel mg/kg ND 5.0
n-Pentacosane (S)%92
926093212
METHOD BLANK: 926144205
Associated Lab Samples:
926093212
Analysis Method: EPA 8015
Analysis Description: TPH in Soil by 3545/8015
QC Batch: 138379
QC Batch Method: EPA 3545
Associated Lab Samples:
Lab Project Number: 92103111
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville,NC28804
Phone:[phone]
Fax:[phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Huntersville,NC28078
Phone: [phone]
Fax:[phone]www.pacelabs.rom
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not bereproduced.exceptinfull.
w~houtthe written consentof PaceAnalyticalServices.Inc,
..Y·'~J~~giBel8.C~
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SC Environmental 99030
FL NELAP E87648
Page, 27 of 46Date,09/29/05
Blank Reporting
Parameter Units Result Limit Footnotes
Gasoline mg/kg ND 6.0
4-Bramofluorobenzene(S)%93
LABORATORY CONTROL SAMPLE:926115031
Spike LCS LCS
Paramet!!r Units Conc.Result %Rec Footnotes
Gasoline mg/kg 31.25 34.94 112
4-Bramof1uorobenzene(S)100
MATRIX SPIKE:926115049
926093105 Spike MS MS
Parameter Units Result Conc.Result %Rec Footnotes
Gasoline mg/kg 1.174 36.00 41.20 III
4-Bramof1uorobenzene(S)97
SAMPLE DUPLICATE:926115056
926093113 DUP
Parameter Un~ts Result Result RPD Footnotes
Gasoline mg/kg ND ND NC
4-Bramofluorobenzene(S)%92 88
926093170926093154926093147926093139926093121926093113926093105
926093188
METHOD BLANK: 926115023
Associated Lab Samples:
926093188926093170
926093147
Analysis Method: EPA 8015
Analysis Description: GAS, Soil
926093113 926093121 926093139926093105
926093154
QC Batch: 137861
QC Batch Method: EPA 8015
Associated Lab Samples:
Lab Project Number: 92103111
Client Project ID: west Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville,NG28804
Phone: [phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax:[phone]
ace Analytical 1.
www.pacelabs.com
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshallnot bereproduced,exceptin full,
w~houtthe written consentof PaceAnalyticalServices,Inc.
ji:'I!;~.
:::rJ.JeJ(J(:I<
Page: 28 of 46
Reporting
Limit Footnotes
330
330
330
330
330
330
1600
330
660
330
330
330
660
660
330
330
330
330
330
330
330
330
330
330
330
330
660
330
330
330
330
Blank
Result
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
926093238
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
926093212
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SC Environmental 99030
FL NELAP E8764B
Date:09/29/05
Acenaphthene
Acenaphthylene
Anthracene
Benzo(k)fluoranthene
Beuzo(b)fluoranthene
Benzo(a)anthracene
Benzoic acid
Benzo(g,h,i)perylene
Benzyl alcohol
Benzo(a)pyrene
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethaxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenylether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobeuzidine
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphtha1ate
Parameter
926093246
METHOD BLANK: 926100819
Associated Lab Samples:
Analysis Method: EPA 8270
Analysis Description:Semivolatile Organics
926093238 926093246926093212
QC Batch: 137520
QC Batch Method: EPA 3545
Associated Lab Samples:
Lab Project Number: 92103111
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
PaceAnalytical Services,Inc.
2225 Riverside Drive
Asheville,NC28804
Phone: [phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue,Suite 100
Huntersvifle,NC28018
Phone: [phone]
Fax: [phone]
ace Analytiear
www.pac:elaIlScccm
Charlotte Certification IDs
NCWastewater 12
NCDrinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced,exceptin full,
wrthoutthewritten consentof PaceAnalyticalServices,Inc.
Page: 29 of 46
926093238 926093246
Blank Reporting
Result LilIIit Footnotes
ND 330
NIl 330
ND 1600
ND 330
ND 330
ND 330
ND 330
ND 330
ND 330
ND 330
ND 330
ND 330
ND 330
ND 330
ND 330
ND 330
ND 330
ND 330
ND 330
ND 330
ND 1600
ND 1600
ND 1600
ND 330
ND 330
ND 1600
ND 330
ND 330
ND 1600
ND 330
ND 330
ND 330
ND 330
ND 330
ND 330
67
AshevilleCertification IDs
NCWastewater 40·
NCDrinking Water 37712
SCEnvironmental 99030
FLNELAP E87648
Date:09/29/05
!1aramater Units
Di-n-buty1phtha1ate ug/kg
4,6-Dinitro-2~thy1pheno1 ug/kg
2,4-Dinitropheno1 ug/kg
2,4-Dinitroto1uene ug/kg
2,6-Dinitroto1uene ug/kg
Di-n-octy1phtha1ate ug/kg
1,2-Dipheny1hydrazine ug/kg
bis(2-Ethy1hexy1)phtha1ate ug/kg
F1uoranthene ug/kg
Fluorene ug/kg
Hexach1oro-1,3-butadiene ug/kg
Baxachlorobeu.f.ene ug/kg
Hexach1orocyc1opentadiene ug/kg
Hexachloroethane ug/kg
Indeno(1,2,3-cd)pyrene ug/kg
Isophorone ug/kg
2-Methy1naphtha1ene ug/kg
2-Methy1pheno1 (o-Creso1) ug/kg
3&4-Methy1pheno1 ug/kg
Naphthalene ug/kg
2-Nitroaniline ug/k9.
3-Nitroaniline ug/kg
4-Nitroaniline ug/kg
Nitrobenzene ug/kg
2-Nitropheno1 ug/kg
4-Nitropheno1 ug/kg
N-Nitroso-di-n-propy1amine ug/kg
N-Nitrosodipheny1amine ug/kg
Pentachlorophenol ug/kg
Phenanthrene ug/kg
Phenol ug/kg
Pyrene ug/kg
1,2,4-Trich1orobenzene ug/kg
2,4,5-Trich1oropheno1 ug/kg
2,4,6-Trich1oropheno1 ug/kg
Nitrobenzene-d5 (S)%
926093212
METHOD BLANK: 926100819
Associated Lab Samples:
Lab Project NUmber: 92103111
Client Project ID: west Morehead/6228-05-3103
QUALITY CONTROL DATA
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]VMw.paoe£sbs.com
Charlotte Certification IDs
NCWastewater 12
NCDrinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall notbereproduced,exceptin full,
w~houtthewrittenconsentof PaceAnalyticalServices,Inc,
lo"J.~tl'oI!;_e:~~,~
~!JJt;3dl...f,
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SCEnvironmental 99030
FLNELAP E87646
LABORATORY CONTROL SAMPLE: 926100827
Spike LCS LCS
~ar~t!i!r units Conc. Result %Rec Footnotes
Acenaphthene ug/kg 1667.00 1168 70
Acenaphthylene ug/kg 1667.00 1095 66
Anthracene ug/kg 1667.00 1255 75
Benzo(k)fluoranthene ug/kg 1667.00 1092 66
Benzo(b)fluoranthene ug/kg 1667.00 1095 66
Benzo (a)anthracene ug/kg 1667.00 1104 66
Benzoic acid ug/kg 1667.00 382.3 23
Benzo(g,h,i)perylene ug/kg 1667.00 1418 85
Benzyl alcohol ug/kg 1667.00 1453 87
Benzo(a)pyrene ug/kg 1667.00 1301 78
4-Bromophenylphenyl ether ug/kg 1667.00 1208 72
Butylbenzylphthalate ug/kg 1667.00 1219 73
4-Chloro-3-methylphenol ug/kg 1667.00 1458 '88
4-Chloroaniline ug/kg 1667.00 1858 111
bis(2-Chloroethoxy)methane ug/kg 1667.00 1362 82
bis(2-Chloroethyl) ether ug/kg 1667.00 1199 72
bis(2-Chloroisopropyl) ether ug/kg 1667.00 1219 73
2-Chloronaphthalene ug/kg 1667.00 1173 70
2-Chlorophenol ug/kg 1667.00 1123 67
4-Chlorophenylphenyl ether ug/kg 1667.00 1269 76
Chrysene ug/kg 1667.00 1114 67
Dibenz(a,h)anthracene ug/kg 1667.00 1470 88
Dibenzofuran ug/kg 1667.00 1222 73
1,2-Dichlorobenzene ug/kg 1667.00 1073 64
1,3-Dichlorobenzene ug/kg 1667.00 995.3 60
Date:09/29/05 Page: 30 of 46
%
%
%
%2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d5 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
UnitsParameter
Reporting
Limit Footnotes
Blank
Result
61
66
62
62
60%
926093246926093238926093212
METHOD BLANK: 926100819
Associated Lab Samples:
Lab Project NUmber: 92103111
Client Project ID: west Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]
aceAna/yticar~
WlVII'.par:e18bs<com
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshallnotbereproduced,exceptinfull,
w~houtthe written consentof PaceAnalyticalServices,Inc.
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
QUALITY CONTROL DATA
Lab Project Number: 92103111
Client Project ID:West Morehead/6228-05-3103
LABORATORY CONTROL SAMPLE: 926100827
Spike LCS LCS
Parameter Units Cone. Result %Ree Footnotes
1,4-Dich1orobenzene ug/kg 1667.00 989.8 59
3,3'-Dich1orobenzidine ug/kg 3333.00 1313 39
2,4-Dichloropheno1 ug/kg 1667.00 1350 81
Diethy1phtha1ate ug/kg 1667.00 1297 78
2,4-Dimethy1pheno1 ug/kg 1667.00 1268 76
Dimethy1phtha1ate ug/kg 1667.00 1235 74
Di-n-buty1phtha1ate ug/kg 1667.00 1191 72
4,6-Dinitro-2-methylpheno1 ug/kg 1667.00 1150 69
2,4-Dinitropheno1 ug/kg 1667.00 796.9 48
2,4-Dinitroto1uene ug/kg 1667.00 1171 70
2,6-Dinitroto1uene ug/kg 1667.00 1273 76
Di-n-octy1phtha1ate ug/kg 1667.00 1208 72
1,2-Dipheny1hydrazine ug/kg 1667.00 1159 70
bis(2-Ethy1hexy1)phtha1ate ug/kg 1667.00 1279 77
F1uoranthene ug/kg 1667.00 1137 68-
Fluorene ug/kg 1667.00 1171 70
Hexach1oro-1,3-butadiene ug/kg 1667.00 1219 73
Bexachlorobenzene ug/kg 1667.00 1321 79
Hexachlorocyclopentadiene ug/kg 1667.00 2047 123 2
Hexachloroethane ug/kg 1667.00 1120 67
Indeno(1,2,3-cd)pyrene ug/kg 1667.00 1387 83
Isophorone ug/kg 1667.00 3060 184 2
2-Methy1naphtha1ene ug/kg 1667.00 1229 74
2-Methy1pheno1 (o-Creso1) ug/kg 1667.00 1236 74
3&4-Methy1pheno1 ug/kg 1667.00 1303 78
Naphthalene ug/kg 1667.00 1049 63
2-Nitroaniline ug/kg 1667.00 1095 66
3-Nitroaniline ug/kg 1667.00 1412 85
4-Nitroaniline ug/kg 1667.00 1174 70
Nitrobenzene ug/kg 1667.00 1381 83
2-Nitropheno1 ug/kg 1667.00 1210 73
4-Nitropheno1 ug/kg 1667.00 1296 78
N-Nitroso-di-n-propy1amine ug/kg 1667.00 1425 86
N-Nitrosodiphenylamine ug/kg 1667.00 1486 89
Pentachlorophenol ug/kg 1667.00 1340 80
Phenanthrene ug/kg 1667.00 1170 70
Phenol ug/kg 1667.00 1298 78
Date:09/29/05 Page:31 of 46
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville,NC28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC28018
Phone:[phone]
Fax:[phone]www.pacelabs.com
Charlotte Certification IDs
NCWastewater 12
NGDrinking Water 37706
SC 99006
FL NELAP E87627
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SCEnVironmental 99030
FL NELAP E87648
Pllge:32 of 46Date:09/29/05
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 926100835 926100843
926077355 Spike MS MSD MS MSD
Parameter units Result Cone. Result Result %Ree %Rec RPD Footnotes
Aeenaphthene ug/kg 0 2110.00 1315 1314 62 62 0
4-Chloro-3-methylphenol ug/kg 0 2110.00 1640 1695 78 80 3
2-Chlorophenol ug/kg 0 2110.00 1397 1348 66 64 4
1,4-Dich1orobenzene ug/kg 0 2110.00 1069 1098 51 52 3
2,4-Dinitrotoluene ug/kg 0 2110.00 1249 1258 59 60 1
4-Nitrophenol ug/kg 0 2110.00 1348 1429 64 68 6
N-Nitroso-di-n-propylamine ug/kg 0 2110.00 1531 1428 73 68 7
Pentachlorophenol ug/kg 0 2110.00 1449 1510 69 72 4
Phenol ug/kg 0 2110.00 1491 1436 71 68 4
Pyrene ug/kg 0 2110.00 1150 1180 54 56 3
1,2,4-Triehlorobenzene ug/kg 0 2110.00 1408 1389 67 66 1
Nitrobenzene-d5 (S)71 75
2-Fluorobiphenyl (S)57 63
Terphenyl-d14 (S)54 61
Phenol-d5 (S)68 70
2-Fluoropheno1 (S)63 69
2,4,6-Tribramophenol(S)64 72
Spike LCS LCS
~s;rameter units Conc.Result %Rec Footnotes
Pyrene ug/kg 1667.00 1251 75
1,2,4-Trichlorobenzene ug/kg 1667.00 1228 74
2,4,5-Trichlorophenol ug/kg 1667.00 1202 72
2,4,6-Trichlorophenol ug/kg 1667.00 1148 69
Nitrobenzene-d5 (S)84
2-Fluorobiphenyl (S)72
Terphenyl-d14 (S)78
Phenol-d5 (S)79
2-Fluorophenol (S)74
2,4,6-Tribramophenol(S)80
LABORATORY CONTROL SAMPLE: 926100827
Lab Project Number: 92103111
Client Project ID: west Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville,NC 28804
Phone:[phone]
Fax:[phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Huntersville, NC 28078
Phone:[phone]
Fax: [phone]Wv,/w.pacelabs.oom
Charlotte Certification IDs
NCWastewater 12
NCDrinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced,exceptinlull,
witholll the written consentof PaceAnalyticalServices,Inc.
,..H't,~
l"':~'-_f:::'!<'f>JJJeIaC.~
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SCEnvironmental 99030
FLNELAP E87648
SAMPLE DUPLICATE:926100942
926090432 DUP
ParlllllBtel:units Result Result RPD Footnotes
Acenaphthene ug/kg ND ND NC
Acenaphthylene ug/kg ND ND NC
Anthracene ug/kg ND ND NC
Benzo(k)fluoranthene ug/kg ND ND NC
Benzo(b)f1uoranthene uglkg ND ND NC
Benzo(a) anthracene ug/kg ND ND NC
Benzoic acid ug/kg ND ND NC
Benzo (g,h,i)perylene ug/kg ND ND NC
Benzyl alcohol ug/kg ND ND NC
Benzo(a)pyrene ug/kg ND ND NC
4-Bromopheny1pheny1 ether ug/kg ND ND NC
Butylbenzylphthalate ug/kg ND ND NC
4-Ch1oro-3-methylphenol ug/kg ND ND NC
4-Chloroaniline ug/kg ND ND NC
bis(2-Chloroethaxy)methane ug/kg ND ND NC
bis(2-Chloroethyl) ether ug/kg ND ND NC
bis(2-Chloroisopropyl)ether ug/kg ND ND NC
2-Chloronaphthalene ug/kg ND ND NC
2-Chlorophenol ug/kg ND ND NC
4-Chlorophenylphenyl ether ug/kg ND ND NC
Chrysene ug/kg ND ND NC
Dibenz (a,h)anthracene ug/kg ND ND NC
Dibenzofuran ug/kg ND ND NC
1,2-Dichlorobenzene ug/kg ND ND NC
1,3-Dichlorobenzene ug/kg ND ND NC
1,4-Dichlorobenzene ug/kg ND ND NC
3,3'-Dichlorobenzidine ug/kg ND ND NC
2,4-Dichlorophenol ug/kg ND ND NC
Diethylphthalate ug/kg ND ND NC
2,4-Dimethylphenol ug/kg ND ND NC
Dimethylphthalate ug/kg ND ND NC
Di-n-butylphthalate ug/kg ND ND NC
4,6-Dinitro-2-methylphenol ug/kg ND ND NC
2,4-Dinitrophenol ug/kg ND ND NC
2,4-Dinitrotoluene ug/kg ND ND NC
2,6-Dinitrotoluene ug/kg ND ND NC
Di-n-octylphthalate ug/kg ND ND NC
Date:09/29/05 Page: 33 of 46
Lab Project Number: 92103111
Client Project ID: west Morehead/6228-0S-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax:[phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28018
Phone: [phone]
Fax: [phone]
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not bereproduced,exceptinfull,
without the written consentof PaceAnalyticalServices,Inc.
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Page:34 of 46Date:09/29/05
QUALITY CONTROL DATA
Lab Project Number:92103111
Client Project ID:West Morehead/6228-05-3103
SAMPLE DUPLICATE: 9261009'2
926090432 DUP
:!1arameter units Result Result RPD Footnotes
1,2-Diphenylhydrazine ug/kg ND ND NC
bis(2-Ethylhexyl)phthalate ug/kg ND ND NC
Fluoranthene ug/kg ND ND NC
Fluorene ug/kg ND ND NC
Hexachloro-l,3-butadiene ug/kg ND ND NC
Hexachlorobenzene ug/kg ND ND NC
Hexachlorocyclopentadiene ug/kg ND ND NC
Hexachloroethane ug/kg ND ND NC
Indeno(1,2,3-cd)pyrene ug/kg ND ND NC
Isophorone ug/kg ND ND NC
2-Methylnaphthalene ug/kg ND ND NC
2-Methylphenol (o-Cresol) ug/kg ND ND NC
3&4-Methylphenol ug/kg ND ND NC
Naphthalene ug/kg ND ND NC
2-Nitroaniline ug/kg ND ND NC
3-Nitroaniline ug/kg ND ND NC
4-Nitroaniline ug/kg ND ND NC
'>Nitrobenzene ug/kg ND ND NC
2-Nitrophenol ug/kg ND ND NC
4-Nitrophenol ug/kg ND ND NC
N-Nitroso-di-n-propylBmine ug/kg ND ND NC
N-Nitrosodiphenylamine ug/kg ND ND NC
Pentachlorophenol ug/kg ND ND NC
Phenanthrene ug/kg ND ND NC
Phenol ug/kg ND ND NC
Pyrene ug/kg ND ND NC
1,2,4-Trichlorobenzene ug/kg ND ND NC
2,4,5-Trichlorophenol ug/kg ND ND NC
2,4,6-Trichlorophenol ug/kg ND ND NC
Nitrobenzene-d5 (S)%37 36
2-Fluorobiphenyl (S)%38 42
Terphenyl-d14 (S)%25 31
Phenol-d5 (S)%36 35 3
2-Fluorophenol (S)%38 36
2,4,6-Tribromophenol (S)%35 37
Pace Analytical Services,Inc.
2225 Riverside Drive
Asheville,NC 28804
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax:[phone]
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
Page: 35 of 46
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced.exceptin full,
wijhout the written consentof PaceAnalyticalServices,Inc.
E~
Reporting
Limit Footnotes
100
5.0
5.0
5.0
5.0
5.0
10.
100
5.0
5.0
5.0
5.0
5.0
10.
5.0
10.
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10.
5.0
5.0
5.0
5.0
5.0
926093246
Blank
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
926093238
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
926093212
Date:09/29/05
Acetone
Benzene
Bromobenzene
Bromochloroma~ane
Bromodichloromethane
Bromoform
Bromamethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibramo-3-chloropropane
Dibramochloromethane
1,2-Dibramoethane (EDB)
Dibromamethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoramethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dich1oroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
.l'ara:meter
METHOD BLANK: 926112855
Associated Lab Samples:
Analysis Method: EPA 8260
Analysis Description: GC/MS VOCs by 8260, low level
926093238 926093246926093212
QC Batch: 137786
QC Batch Method: EPA 8260
Associated Lab Samples:
Lab Project Number: 92103111
Client Project ID: west Morehead/6228-0S-3103
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]vlww.paoelsll$:com
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced.exceptin full,
wijhout the written consentof PaceAnalyticalServices.lnc.
Palle: 36 of 46
926093238 926093246
Blank Reporting
Result Limit Footnotes
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 50.
ND 5.0
ND 5.0
ND 5.0
ND 50.
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 50.
ND 10.
ND 5.0
ND 10.
ND 5.0
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SCEnvironmental 99030
FLNELAP E87648
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
926093212
Date:09/29/05
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
l,l-Dichloropropene
cis-1,3-Dichloropropene
trans-l,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
H8Xachloro-l,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
l,l,l-Trichloroethane
1,l,2-Trichloroethane
Trichloroethene
Trichlorofluoramethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
METHOD BLANK: 926112855
Associated Lab Samples:
Lab Project NUmber: 92103111
Client Project ID: west Morehead/622B-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078 '
Phone: [phone]
Fax: [phone]
Charlotte Certification IDs
NC Wastewater 12
NCDrinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced,exceptin full,
wtihout the written consentof PaceAnalyticalServices,Inc.
[ielaC''l.':_'!}.'!('t.~.;i;;
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
LABORATORY CONTROL SAMPLE: 926112863
Spike LCS LCS
!i!1!!:&!lf!!C!ill;:Units Conc. Result %_Rec Footnotes
Acetone ug/kg 100.00 84.65 B5
Benzene ug/kg 50.00 49.69 99
Bromobenzene ug/kg 50.00 50.04 100
Bramochloromethane ug/kg 50.00 44.64 89
Bromodichlor<:®ethana ug/kg 50.00 4B.45 97
Bromoform ug/kg 50.00 45.20 90
Bramamethane ug/kg 50.00 53.20 106
2-Butanone (MEK)ug/kg 100.00 99.16 99
n-Butylbenzene ug/kg 50.00 47.87 96
sec-Butylbenzene ug/kg 50.00 51.44 103
tert-Butylbenzene ug/kg 50.00 41.90 B4
Carbon tetrachloride ug/kg 50.00 52.94 106
Chlorobenzene ug/kg 50.00 46.54 93
Chloroethane ug/kg 50.00 45.36 91
Chloroform ug/kg 50.00 47.89 96
Chloromethane ug/kg 50.00 41.04 B2
2-Chlorotoluene ug/kg 50.00 49.62 99
4-Chlorotoluene ug/kg 50.00 49.66 99
1,2-Dibramo-3-chloropropane ug/kg 50.00 46.12 92
Dibromochloramethane ug/kg 50.00 45.24 90
1,2-Dibromoethane (EDB)ug/kg 50.00 46.51 93
Dibramamethane ug/kg 50.00 46.72 93
1,2-Dichlorobenzene ug/kg 50.00 50.86 102
1,3-Dichlorobenzene ug/kg 50.00 4B.39 97
1,4-Dichlorobenzene ug/kg 50.00 49.01 9B
Dichlorodifluoromethane ug/kg 50.00 36.38 73
Date: 09/29/05 Page: 37 of 46
%
%
%
%
Toluene-dB (S)
4-Bromofluorobenzene (S)
Dibromofluoramethane (S)
1,2-Dichloroethane-d4 (S)
Reporting
LilIIit Footnotes
Blank
Result
100
97
94
91
UnitsParametElr
92609324692609323B926093212
METHOD BLANK: 926112855
Associated Lab Samples:
Lab Project Number: 92103111
Client Project ID: west Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]WWW.pacelabs.rom
Charlotte Certification IDs
NCWastewater 12
NCDrinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall notbe reproduced.exceptin full,
without thewritten consentof PaceAnalyticalServices,Inc.
....HIt~t:=,t.:~l{T.JetaO~
AshevilleCertification IDs
NCWastewater 40
NGDrinking Water 37712
SCEnvironmental 99030
FL NELAP E87648
QUALITY CONTROL DATA
Lab Project Number:92103111
Client Project ID: West Morehead/6228-05-3l03
LABORATORY CONTROL SAMPLE: 926112863
Spike LCS LCS
Paramet!:!J.:Units Cone. Result %Rec Footnotes
l,l-Dichloroethane ug/kg 50.00 45.94 92
1,2-Dichloroethane ug/kg 50.00 44.49 89
l,l-Dichloroethene ug/kg 50.00 55.10 110
cis-l,2-Dichloroethene ug/kg 50.00 45.89 92
trans-l,2-Dichloroethene ug/kg 50.00 50.31 101
1,2-Dichloropropane ug/kg 50.00 49.68 99
1,3-Dichloropropane ug/kg 50.00 46.32 93
2,2-Dichloropropane ug/kg 50.00 48.49 97
l,l-Dichloropropene ug/kg 50.00 50.93 102
cis-l,3-Dichloropropene ug/kg 50.00 46.50 93
trans-l,3-Dichloropropene ug/kg 50.00 43.40 87
Diisopropyl ether ug/kg 50.00 48.62 97
Ethylbenzene ug/kg 50.00 49.32 99
Hexachloro-l,3-butadiene ug/kg 50.00 59.48 119
2-Hexanone ug/kg 100.00 92.80 93
Isopropylbenzene (Cumene) ug/kg 50.00 55.33 111
p-Isopropyltoluene ug/kg 50.00 47.46 95
Methylene chloride ug/kg 50.00 48.65 97
4-Methyl-2-pentanone (MIBK)ug/kg 100.00 100.7 101
Methyl-tert-butyl ether ug/kg 50.00 46.56 93
Naphthalene ug/kg 50.00 47.52 95
n-Propylbenzene ug/kg 50.00 50.81 102
Styrene ug/kg 50.00 47.61 95
1,1,1,2-Tetrachloroethane ug/kg 50.00 45.78 92
1,1,2,2-Tetrachloroethane ug/kg 50.00 42.68 85
Tetrachloroethene ug/kg 50.00 50.45 101
Toluene ug/kg 50.00 47.45 95
1,2,3-Trichlorobenzene ug/kg 50.00 57.58 115
1,2,4-Trichlorobenzene ug/kg 50.00 55.72 111
l,l,l-Trichloroethane ug/kg 50.00 47.72 95
1,1,2-Trichloroethane ug/kg 50.00 43.53 87
Trichloroethene ug/kg 50.00 48.20 96
Trichlorofluoramethane ug/kg 50.00 44.66 89
1,2,3-Trichloropropane ug/kg 50.00 43.36 87
1,2,4-Trimethylbenzene ug/kg 50.00 46.51 93
1,3,5-Trimethylbenzene ug/kg 50.00 48.13 96
Vinyl acetate ug/kg 100.00 2.219 2 4
Date:09/29/05 Page: 38 of 46
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NG 28804
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]www.pacelabs.c<>m
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced,exceptin full,
wtthoutthewritten consentof PaceAnalyticalServices,Inc.
Page: 39 of 46
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SC Environmental 99030
FLNELAP E87648
SAMPLE DUPLICATE: 926118449
926087339 DUP
Pa,rameter Units Result Result RPD Footnotes
Acetone ug/kg 570.0 140.0 119 1,5
Benzene ug/kg ND ND NC
Bromobenzene ug/kg ND ND NC
B%'omoch19rOroethane ug/kg ND ND NC
Bromodichloramethane ug/kg ND ND NC
Bromoform ug/kg ND ND NC
Bramomethane ug/kg ND ND NC
2-Butanone (MEK)ug/kg ND ND NC
Date:09/29/05
926087313 Spike MS MS
Para.meta,6 Units Result Conc._ Result %Rec Footnotes
Benzene ug/kg 0 61.06 73.13 120
Ch1orobenzene ug/kg 0 61.06 75.90 124
1,1-Dich1oroethene ug/kg 0 61.06 89.11 146
Toluene ug/kg 0 61.06 74.64 122
Trichloroethene ug/kg 0 61.06 75.30 123
To1uene-d8 (S)100
4-Bromofluorobenzene (S)100
Dibromofluoramethane (S)97
1,2-Dich1oroethane-d4 (S)94
MATRIX SPIKE: 926118431
Spike LCS LCS
Cone. Result %Ree Footnotes
50.00 39.60 79
150.00 148.4 99
100.00 100.2 100
50.00 48.24 96
97
99
94
87
ug/kg
ug/kg
ug/kg
ug/kg
Vinyl chloride
Xylene (Total)
m&:p-Xy1ene
o-Xy1ene'
To1uene-d8 (S)
4-Bramof1uorobenzene (S)
Dibromof1uoramethane (S)
1,2-Dich1oroethane-d4 (S)
unitsParameter
LABORATORY CONTROL SAMPLE: 926112863
Lab Project Number: 92103111
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28018
Phone: [phone]
Fax: [phone]
aceAnalytical'"
Wi'.'l!'.PBcelebS.com
Charlotte Certification IDs
MCWastewater 12
MCDrinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshallnot be reproduced.exceptinfull,
w~houtthe written consentof PaceAnalyticalServices,Inc,
"'~~.~~~fHeJaO~.
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SCEnvironmental 99030
FLNElAP E87648
QUALITY CONTROL DATA
Lab Project Number: 92103111
Client Project ID:west Morehead/6228-05-3103
SAMPLE DUPLICATE:926118449
926087339 DUP
PaJ;:aJneter Units Result Result RPD Footnotes
n-Butylbenzene ug/kg ND ND NC
sec-Butylbenzene ug/kg ND ND NC
tert-Butylbenzene ug/kg ND ND NC
Carbon tetrachloride ug/kg ND ND NC
Chlorobenzene ug/kg ND ND NC
Chloroethane ug/kg ND ND NC
Chloroform ug/kg ND ND NC
Chloromethane ug/kg ND ND NC
2-Chlorotoluene ug/kg ND ND NC
4-Chlorotoluene ug/kg ND ND NC
1,2-Dibramo-3-chloropropane ug/kg ND ND NC
Dibromochloromethane ug/kg ND ND NC
1,2-Dibramoethane (EDB)ug/kg ND ND NC
Dihromamethane ug/kg ND ND NC
1,2-Dichlorobenzene ug/kg ND ND NC
1,3-Dichlorobenzene ug/kg ND ND NC
1,4-Dichlorobenzene ug/kg ND ND NC
Dichlorodifluoramethane ug/kg ND ND NC
1,1-Dichloroethane ug/kg ND ND NC
1,2-Dichloroethane ug/kg ND ND NC
1,1-Dichloroethene ug/kg ND ND NC
cis-l,2-Dichloroethene ug/kg ND ND NC
trans-l,2-Dichloroethene ug/kg ND ND NC
1,2-Dichloropropane ug/kg ND ND NC
1,3-Dichloropropane ug/kg ND ND NC
2,2-Dichloropropane ug/kg ND ND NC
1,1-Dichloropropene ug/kg ND ND NC
cis-1,3-Dichloropropene ug/kg ND ND NC
trans-1,3-Dichloropropene ug/kg ND ND NC
Diisopropyl ether ug/kg ND ND NC
Ethylhenzene ug/kg ND ND NC
Hexachloro-1,3-butadiene ug/kg ND ND NC
2-Hexanone ug/kg ND ND NC
Isopropylbenzene (CUmene)ug/kg ND ND NC
p-Isopropyltoluene ug/kg ND ND NC
Methylene chloride ug/kg 100.0 21.00 134 1,5
4-Methyl-2-pentanone (MIBK)ug/kg ND ND NC
Date:09/29/05 Page: 40 of 46
Pace Analytical Services,Inc.
2225 Riverside Drive
Asheville,NC28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue,Suite 100
Huntersville,NC28018
Phone: [phone]
Fax:[phone]
'aceAna/ytjcal'~
www.pace/abs.ccm
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not bereproduced.exceptin full.
wtthout the written consentof PaceAnalyticalServices.Inc.
~::;:6~i~'~
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Palle:41 of 46Date:09/29/05
SAMPLE DUPLICATE: 926118449
926087339 IiUP
P!!;!;:BlIIBter Un~!;!!Result Result RPD Footnotes
Methyl-tert-butyl ether ug/kg NO NO NC
Naphthalene ug/kg NO NO NC
n-Propylbenzene ug/kg NO NO NC
Styrene ug/kg NO NO NC
1,1,1,2-Tetrachloroethane ug/kg NO NO NC
1,1,2,2-Tetrachloroethane ug/kg NO NO NC
Tetrach1oroethene ug/kg NO NO NC
Toluene ug/kg NO NO NC
1,2,3-Trichlorobenzene ug/kg NO NO NC
1,2,4-Trichlorobenzene ug/kg lID NO NC
l,l,l-Trichloroethane ug/kg NO NO NC
1,1,2-Trichloroethane ug/kg NO NO NC
Trichloroethene ug/kg NO NO NC
Trichlorofluoramethane ug/kg NO NO NC
1,2,3-Trichloropropane ug/kg NO NO NC
l,2,4-Trimethylbenzene ug/kg NO NO NC
1,3,S-'l'rimethylbenzene ug/kg NO NO NC
Vinyl acetate ug/kg NO NO NC
Vinyl chloride ug/kg NO NO NC
Xylene (Total)ug/kg NO NO NC
m&p-Xylene ug/kg NO NO NC
o-Xylene ug/kg NO NO NC
Toluene-d8 (S)%104 106
4-Bromofluorobenzene (S)%97 103
Dibromofluoramethane (S)%119 98
l,2-Dichloroethane-d4 (S)%103 96
Lab Project Number: 92103111
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services,Inc.
2225 Riverside Drive
Asheville,NC28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 KinceyAvenue,Suite 100
Huntersville, NC28018
Phone:[phone]
Fax:[phone]WW;\I.pacel8bs,com
Charlotte Certification IDs
NCWastewater 12
NC'Drinking Water 37706
SC 99006
FL NELAP EB7627
REPORT OF LABORATORY ANALYSIS
This reportshallnotbe reproduced.exceptinfull,
w~houtthe written consentof PaceAnalyticalServices.Inc,
~tl~~~I.IJ..~";
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SCEnvironmental 99030
FLNELAP EB7648
Page: 42 of 46Date:09/29/05
Result RPD Footnotes
0.01490 0NOug/gMercury
ResultUnitsParameter
926071671 DUP
SAMPLE DUPLICATE: 926094830
MSDMSMSD
Result
0.07400.0908
926072265
ResultUnitsPar8l!l8ter FootnotesRPD
20
%Ree %Rec
101 81
MS
Result
Spike
Cone.
0.07510.01483mg/kgMercury
MATRIX SPIKE ~ MATRIX SPIKE DUPLICATE: 926094814 926094822
mg/kgMercury
LCS
%Rec Footnotes
98
LCS
Result
0.0656
Spike
Conc.
0.0667
UnitsParameter
LABORATORY CONTROL SAMPLE: 926094806
METHOD BLANK:926094798
Associated Lab Samples: 926093212 926093238 926093246
Blank Reporting
Parameter Units Result LilIIit Footnotes
Mercury mg/kg NO 0.0050
Analysis Method: EPA 7471
Analysis Description:Mercury, CVAAS, in Soil
926093238 926093246926093212
QC Batch: 137409
QC Batch Method: EPA 7471
Associated Lab Samples:
Lab Project NUmber: 92103111
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services,Inc.
2225 Riverside Drive
Asheville,NG 28804
Phone:[phone]
Fax: [phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone:[phone]
Fax:[phone]
Charlotte Certification IDs
NGWastewater 12
NG Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced,exceptin full,
w~houtthewritten consentof PaceAnalyticalServices,Inc.
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
926092750 Spike MS MSD.MS MSD
Parameter units Result Cone. Result Result %Rec %Ree RPD Footnotes
Arsenic mg/kg 12.37 72.62 70.11 70.11 80 80 0
Barium mg/kg 59.92 72.62 127.8 134.7 94 103 5
Cadmium mg/kg 0 72.62 47.80 51.10 66 70 7 6,6
Chromium mg/kg 72.49 72.62 128.6 134.7 77 86 5
Lead,,mg/kg 21.84 72.62 83.97 84.76 86 87 1
Date:09/29/05 Page: 43 of 46
~TRIX SPIKE &~TRIX SPIKE DUPLICATE: 926095076 926095084
Spike LCS LCS
Parameter Units Cone. Result %Rec Footnotes
Arsenic mg/kg 50.00 48.20 96
Barium mg/kg 50.00 48.30 97
Cadmium mg/kg 50.00 46.40 93
Chromium mg/kg 50.00 47.10 94
Lead mg/kg 50.00 46.40 93
Selenium mg/kg 50.00 46.30 93
Silver mg/kg 50.00 47.40 95
LABORATORY CONTROL SAMPLE: 926095068
METHOD BLANK: 926095050
Associated Lab Samples: 926093212 926093238 926093246
Blank Reporting
Raramet~r Uni!;;s Result Limit Footnotes
Arsenic mg/kg NO 0.50
Barium mg/kg NO 0.50
Cadmium mg/kg NO 0.10
Chromium mg/kg NO 0.20
Lead mg/kg NO 0.50
Selenium mg/kg NO 0.50
Silver mg/kg NO 0.20
Analysis Method: EPA 6010
Analysis Description: Metals, Trace ICP
926093238 926093246926093212
QC Batch: 137414
QC Batch Method: EPA 3050
Associated Lab Samples:
Lab Project NUmber: 92103111
Client Project ID: west Morehead/6228-05-3103
QUALITY CONTROL DATA
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax:[phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax:[phone]www.pacefabs.com
Charlotte Certification IDs
NCWastewater 12
NCDrinking Water 37706
SC 99006
Fl N"ElAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced,exceptin full,
wnhout the written consentof PaceAnalyticalServices,Inc.
~6:~~lIJJeI(K.~
AshevilleCertification IDs
NCWastewater 40
NCDrinking Water 37712
SCEnvironmental 99030
FLNElAP E87648
Page: 44 of 46Date:09/29/05
926092768 DUP
Para!!ll!t!;!r Units Result Result RPD .Footnotes
Arsenic mg/kg 7.200 7.800 8
Barium mg/kg 45.00 49.00 8
Cadmium mg/kg ND ND MC
Chromium DIg/kg 27.00 24.00 11
Lead mg/kg 14.00 14.00 1
Selenium mg/kg ND ND NC
Silver mg/kg ND ND NC
SAMPLE DUPLICATE: 926095092
Selenium
Silver
926092750 Spike MS MSD MS MSD
Units Result Cone. Result Result %Rec %~e~RPD Footnotes
mg/kg 0 72.62 35.65 33.27 49 46 7 6,6
mg/kg 0 72.62 60.21 64.56 83 89 7
.Parameter
~TRIX SPIKE &MATRIX SPIKE DUPLICATE: 926095076 926095084
Lab Project Number: 92103111
Client Project ID: west Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NG28804
Phone: [phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]Wl\lW.pBcefabscom
Charlotte Certification IDs
NC Wastewater 12
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REPORT OF LABORATORY ANALYSIS
This report shall no!be reproduced, except infull,
w~hout the written consent ofPace Analytical Services, Inc.
Page: 45 of 46
RPD Footnotes
716.20
Result
17.30
Result
926095738 DUP
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Date: 09/29/05
%Percent Moisture
unitsParameter
SAMPLE DUPLICATE: 926096454
926093238926093212926093188926093170
Analysis Method:%Moisture
Analysis Description:PercentMoisture
926093113 926093121 926093139 926093147926093105
926093154
926093246
QC Batch: 137476
QC Batch Method:
Associated Lab Samples:
Lab Project Number: 92103111
Client Project ID: west Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville,NC 28804
Phone:[phone]
Fax:[phone]
Pace Analytical Services. Inc.
9800 Kincey Avenue,Suite 100
Huntersville. NC 28078
Phone: [phone]
Fax:[phone]v/i'/w.pacelabs.com
Charlotte Certification IDs
NC Wastewater 12
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FLNW\P E8762.7
REPORT OF LABORATORY ANALYSIS
This reportshallnotbe reproduced.exceptinlull,
wtthoutthe writtenconsentof PaceAnalyticalServices,Inc.
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Page:46 of 46Date:09/29/05
[6] The spike recovery was outside acceptance limits for the MS and lor MSD due to matrix interference. The LCS
and/or LCSD were within acceptance limits showing that the laboratory is in control and the data is
acceptable.
[4]
RPD
(S)
[1]
[2]
[3]
MDL
J
NC
ND
DUP
LCS(D)
MS(D)
Laboratory Control Sample (Duplicate)
Matrix Spike (Duplicate)
Sample Duplicate
Not detected at or above adjusted reporting limit
Not Calculable
Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
Adjusted Method Detection Limit
Relative Percent Difference
Surrogate
The calculated RPD was outside QC acceptance limits.
Recovery falls outside of QC limits, however, this compound is not found in the associated samples.
Acid surrogate recovery outside of control limits. The data was accepted based on valid recovery of the two
remaining acid surrogates.
The method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.
[5] Common laboratory contaminant.
Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate %Rec and RPD values.
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Lab Project Number: 92103111
Client Project ID: West Morehead/622B-05-3103
www.pacefabs.com
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville,NG28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville,NC28078
Phone:[phone]
Fax:[phone]
a::~a::~ ~
(!)~f-Qz0--'
~ffi~5~w ffi~-+-(/)0_Il.IcnM~il:g5s:~5~
c::0~E UJ.E :>E C 0
0:x Z0
,~.c :>
(3 W W'I"w
II)Z
"CI c..,Ill 0
!!..J j~~;:::
'5 u
D..00:>::J
IT ~N::iO a::
~:iE ~<~iii ....II)
(.)~-
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c «CD III
.,It:
c::~E 0
c U)0 c..E u..
CD E w
::>0 '"0 c
0 :;;en 0 iii
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~CI)
II)C It:
CD CD U).2 w
1ii c::::>:'!::(U
0 ITE.J:~#W3J.1 "a::
Ui D.U w<C w·II)
3Ob:J XI!:U_l/1II
oz~-o
t:•ic
---'l:-l--I---+---l ~
~E"z
1:;D
::>lIv'""
Charlotte Certification IDs
NCWastewater 12
NCDrinking Water 37706
SC 99006
Fl NElAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,exceptin full,
WIThoutthe written consent of PaceAnalyticalServices,Inc.....'1',.,,.,
00faC~~-·~~,...'";-.'It
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Enclosures
Annette Scott
Annette.Scott.pacelabs.com
Project Manager
Sincerely,
If you have any questions concerning this report please feel free to contact me.
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic testing
was performed at our Pace Charlotte laboratory unless otherwise footnoted.
Enclosed are the analytical results for sample(s) received by the laboratory on September 20, 2005. Results
reported herein conform to the most current HELAC standards. where applicable, unless otherwise narrated in the
body of the report.
Dear Mr.Foster:
R!:~ab Project Number: 92103573
Client Project ID: West Morehead/6228-05-3103
Mr.Rob Foster
Mactec
2801 Yorkmont Road
Suite 100
Charlotte, NC 28208
September 28, 2005
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: 82B.254.1116
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28018
Phone: [phone]
Fax: [phone]
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshallnotbe reproduced,except in full,
without the written consentof PaceAnalyticalServices,Inc.
..\~'i.-=-"~!t~&DekC··~
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GC/MS Semivolatiles
Semivolatile Organics Prep/Method: EPA 3545 EPA 8270
Acenaphthene NO ug/kg 400 1.2 09/24/05 06:56 BET 83-32-9
Acenaphthylene NO ug/kg 400 1.2 09/24/05 06:56 BET 208-96-8
Anthracene 630 ug/kg 400 1.2 09/24/05 06:56 BET 120-12-7
Benzo(klfluoranthene 830 ug/kg 400 1.2 09/24/05 06:56 BET 207-08-9
Benzo(blfluoranthene 990 ug/kg 400 1.2 09/24/05 06:56 BET 205-99-2
Benzo(alanthracene 1100 ug/kg 400 1.2 09/24/05 06:56 BET 56-55-3
Benzoic acid NO ug/kg 2000 1.2 09/24/05 06:56 BET 65-85-0
Benzo(g,h,ilperylene NO ug/kg 400 1.2 09/24/05 06:56 BET 191-24-2
Benzyl alcohol NO ug/kg 800 1.2 09/24/05 06:56 BET 100-51-6
Benzo(alpyrene 1000 ug/kg 400 1.2 09/24/05 06:56 BET 50-32-8
4-Bromophenylphenyl ether NO ug/kg 400 1.2 09/24/05 06:56 BET 101-55-3
Butylbenzylphthalate NO ug/kg 400 1.2 09/24/05 06:56 BET 85-68-7
4-Chloro-3-methylphenol NO ug/kg 800 1.2 09/24/05 06:56 BET 59-50-7
4-Chloroaniline NO ug/kg 1100 1.2 09/24/05 06:56 BET 106-47-8
bis(2-Chloroethoxylmethane NO ug/kg 400 1.2 09/24/05 06:56 BET 111-91-1
bis(2-Chloroethyll ether NO ug/kg 400 1.2 09/24/05 06:56 BET 111-44-4
bis(2-Chloroisopropyllether NO ug/kg 400 1.2 09/24/05 06:56 BET 39638-32-9
2-Chloronaphthalene NO ug/kg 400 1.2 09/24/05 06:56 BET 91-58-7
Data:09128/05 Paga: 1 of 22
1.0 09/20/05 17:48 KBM%17.4
Method:%Moisture
Wet Chemistry
Percent Moisture
Percent Moisture
ALV 7439-97-61.2 09/27/050.0060
Method: EPA 7471
0.15 DIg/kg
Mercury,CVAAS,in Soil
Mercury
1.1 09/24/05 01:06 ALV 7440-38-2
1.1 09/24/05 01:06 ALV 7440-39-3
1.1 09/24/05 01:06 ALV 7440-43-9
1.1 09/24/05 01:06 ALV 7440-47-3
1.1 09/24/05 01:06 ALV 7439-92-1
1.1 09/24/05 01:06 ALV 7782-49-2
1.1 09/24/05 01:06 ALV 7440-22-4
09/23/05 07:30
EPA 3050 EPA 6010
DIg/kg 0.56
DIg/kg 0.56
DIg/kg 0.11
DIg/kg 0.22
DIg/kg 0.56
DIg/kg 0.56
DIg/kg 0.22
Prep/Method:
1.8
43.
NO
58.
12.
NO
NO
09/23/05 07:30
Metals
Metals, Trace ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Date Digested
Units Report Limit .M._ __...An.....a"'ly~z"'e""d._--=By=-__,C..AS......=No><..:..._.QlmL.RegLmtResultsParameters
Date Collected: 09/20/05 12:00
Date Received: 09/20/05 16:20
Project Sample Number: 92103573-001
Matrix: Soil
Lab Sample No: 926117888
Client Sample ID: 1'-12
Solid results are reported on a dry weight basis
Lab Project Number: 92103573
Client Project ID: West Morehead/6228-05-3103
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC28078
Phone:[phone]
Fax: [phone]
·ace Analyticar
WVlW.pBcelabs.com
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
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FL NRAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced,exceptin full,
wnhout thewritten consentof PaceAnalyticalServices,Inc.
.,c>,!,~~'F~~~Y..
iIJeJaC'i
Page: 2 of 22
1.2 09/24/05 06:56 BET 7005-72-3
1.2 09/24/05 06:56 BET 218-01-9
1.2 09/24/05 06:56 BET 53-70-3
1.2 09/24/05 06:56 BET 132-64-9
1.2 09/24/05 06:56 BET 95-50-1
1.2 09/24/05 06:56 BET 541-73-1
1.2 09/24/05 06:56 BET 106-46-7
1.2 09/24/05 06:56 BET 91-94-1
1.2 09/24/05 06:56 BET 120-83-2
1.2 09/24/05 06:56 BET 84-66-2
1.2 09/24/05 06:56 BET 105-67-9
1.2 09/24/05 06:56 BET 131-11-3
1.2 09/24/05 06:56 BET 84-74-2
1.2 09/24/05 06:56 BET 534-52-1
1.2 09/24/05 06:56 BET 51-28-5
1.2 09/24/05 06:56 BET 121-14-2
1.2 09/24/05 06:56 BET 606-20-2
1.2 09/24/05 06:56 BET 117-84-0
1.2 09/24/05 06:56 BET 122-66-7
1.2 09/24/05 06:56 BET 117-81-7
1.2 09/24/05 06:56 BET 206-44-0
1.2 09/24/05 06:56 BET 86-73-7
1.2 09/24/05 06:56 BET 87-68-3
1.2 09/24/05 06:56 BET 118-74-1
1.2 09/24/05 06:56 BET 77-47-4
1.2 09/24/05 06:56 BET 67-72-1
1.2 09/24/05 06:56 BET 193-39-5
1.2 09/24/05 06:56 BET 78-59-1
1.2 09/24/05 06:56 BET 91-57-6
1.2 09/24/05 06:56 BET 95-48-7
1.2 09/24/05 06:56 BET
1.2 09/24/05 06:56 BET 91-20-3
1.2 09/24/05 06:56 BET 88-74-4
1.2 09/24/05 06:56 BET 99-09-2
1.2 09/24/05 06:56 BET 100-01-6
1.2 09/24/05 06:56 BET 98-95-3
1.2 09/24/05 06:56 BET 88-75-5
1.2 09/24/05 06:56 BET 100-02-7
400
400
400
400
400
400
400
800
400
400
400
400
400
400
2000
400
400
400
400
400
400
400
400
400
400
400
400
400
400
400
400
400
2000
2000
2000
400
400
2000
Report Limit ~Analyzed py CAS No.
400 1.2 09/24/05 06:56 BET 95-57-8
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Project Sample Number: 92103573-001
Matrix: Soil
NO
NO
UOO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
2600
NO
NO
NO
NO
NO
410
NO
NO
NO
NO
940
NO
NO
NO
NO
NO
NO
Results
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Date:09/28/05
2-Chlorophenol
4-Chlorophenylphenylether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethy1phenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
1,2-Diphenylhydrazine
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol (o-Cresol)
3&4-Methylphenol
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
Parameters
Date Collected: 09/20/05 12:00
Date Received: 09/20/05 16:20
Lab Sample No: 926117888
Client Sample ID: P-12
Lab Project Number: 92103573
Client Project ID: West Morehead/6228-05-3103
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville. NC28804
Phone:[phone]
Fax:[phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone:[phone]
Fax: [phone]
'aceAnalytical'"
wlVw.pacel8bs.rom
Charlotte Certification IDs
NCWastewater 12
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REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced.exceptinfull.
w~houtthewritten consentof PaceAnalyticalServices.Inc.
Page: 3 of 22
1.2 09/26/0514:42 DLK 67-64-1
1.2 09/26/0514:42 DLK 71-43-2
1.2 09/26/0514:42 DLK 108-86-1
1.2 09/26/0514:42 DLK 74-97-5
1.2 09/26/0514:42 DLK 75-27-4
1.2 09/26/0514:42 DLK 75-25-2
1.2 09/26/0514:42 DLK 74-83-9
1.2 09/26/0514:42 DLK 78-93-3
1.2 09/26/0514:42 DLK 104-51-8
1.2 09/26/0514:42 DLK 135-98-8
1.2 09/26/0514:42 DLK 98-06-6
1.2 09/26/0514:42 DLK 56-23-5
1.2 09/26/0514:42 DLK 108-90-7
1.2 09/26/0514:42 DLK 75-00-3
1.2 09/26/0514:42 DLK 67-66-3
1.2 09/26/0514:42 DLK 74-87-3
1.2 09/26/0514:42 DLK 95-49-8
1.2 09/26/0514:42 DLK 106-43-4
1.2 09/26/0514:42 DLK 96-12-8
1.2 09/26/0514:42 DLK 124-48-1
1
1.2 09/24/0506:56 BET 108-95-2
1.2 09/24/0506:56 BET 129-00-0
1.2 09/24/0506:56 BET 120-82-1
1.2 09/24/0506:56 BET 95-95-4
1.2 09/24/0506:56 BET 88-06-2
1.0 09/24/0506:56 BET 4165-60-0
1.0 09/24/0506:56 BET 321-60-8
1.0 09/24/0506:56 BET 1718-51-0
1.0 09/24/0506:56 BET 4165-62-2
1.0 09/24/0506:56 BET 367-12-4
1.0 09/24/0506:56 BET 118-79-6
09/22/05
120
6.0
6.0
6.0
6.0
6.0
12.
120
6.0
6.0
6.0
6.0
6.0
12.
6.0
12.
6.0
6.0
6.0
6.0
400
400
400
400
400
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
Asheville Certification IDs
NCWastewater 40
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Date:09/28/05
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloramethane
Bromoform
Bramamethane
2-Butanone(MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibramo-3-chloropropane
Dibromochloramethane
Ge/MSVolatiles
GC/MS VOCs b¥8260, low level Method: EPA 8260
%
%
%
%
%
%
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units Report Limit ~ Analvzed By CAS No.
ug/kg 400 1.2 09/24/0506:56 BET 621-64-7
ug/kg 400 1.2 09/24/0506:56 BET 86-30-6
ug/kg 2000 1.2 09/24/0506:56 BET 87-86-5
ug/kg 400 1.2 09/24/0506:56 BET 85-01-8
Project Sample Number: 92103573-001
Matrix: Soil
NO
NO
NO
2700
NO
2200
NO
NO
NO
51
43
76
36
18
31
09/22/05
Results
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pen~achlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5(S)
2-Fluorobiphenyl(S)
Terphenyl-d14(S)
Phenol-d5 (S)
2-Fluorophenol(S)
2,4,6-Tribromophenol(S)
Date Extracted
Parameters
Client Sample ID: P-12
Date Collected: 09/20/0512:00
Date Received: 09/20/0516:20
926117888Lab Sample No:
Lab ProjectNumber: 92103573
Client Project ID: west Morehead/6228-05-3103
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone:[phone]
Fax: [phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]WVAII.pacelSbs.com
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshallnotbereproduced.exceptin full.
w~houtthe written consentof PaceAnalyticalServices.Inc,
Asheville Certification IDs
NCWastewater 40
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Page,4 of 22
1.2 09/26/05 14:42 DLK 74-95-3
1.2 09/26/05 14:42 DLK 95-50-1
1.2 09/26/05 14:42 DLK 541-73-1
1.2 09/26/05 14:42 DLK 106-46-7
1.2 09/26/05 14:42 DLK 75-71-8
1.2 09/26/05 14:42 DLK 75-34-3
1.2 09/26/05 14:42 DLK 107-06-2
1.2 09/26/05 14:42 DLK 75-35-4
1.2 09/26/05 14:42 DLK 156-59-2
1.2 09/26/05 14:42 DLK 156-60-5
1.2 09/26/05 14:42 DLK 78-87-5
1.2 09/26/05 14:42 DLK 142-28-9
1.2 09/26/05 14:42 DLK 594-20-7
1.2 09/26/05 14:42 DLK 563-58-6
1.2 09/26/05 14:42 DLK 10061-01-5
1.2 09/26/05 14:42 DLK 10061-02-6
1.2 09/26/05 14:42 DLK 108-20-3
1.2 09/26/05 14:42 DLK 100-41-4
1.2 09/26/05 14:42 DLK 87-68-3
1.2 09/26/05 14:42 DLK 591-78-6
1.2 09/26/05 14:42 DLK 98-82-8
1.2 09/26/05 14:42 DLK 99-87-6
1.2 09/26/05 14:42 DLK 75-09-2 2
1.2 09/26/05 14:42 DLK 108-10-1
1.2 09/26/05 14:42 DLK 1634-04-4
1.2 09/26/05 14:42 DLK 91-20-3
1.2 09/26/05 14:42 DLK 103-65-1
1.2 09/26/05 14:42 DLK 100-42-5
1.2 09/26/05 14:42 DLK 630-20-6
1.2 09/26/05 14:42 DLK 79-34-5
1.2 09/26/05 14:42 DLK 127-18-4
1.2 09/26/05 14:42 DLK 108-88-3
1.2 09/26/05 14:42 DLK 87-61-6
1.2 09/26/05 14:42 DLK 120-82-1
1.2 09/26/05 14:42 DLK 71-55-6
1.2 09/26/05 14:42 DLK 79-00-5
1.2 09/26/05 14:42 DLK 79-01-6
1.2 09/26/05 14:42 DLK 75-69-4
6.0
6.0
6.0
6.0
12.
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
60.
6.0
6.0
6.0
60.
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
6.0
Date,09/28/05
"p_,.a""rAJIIEI"""""'t""e""r..,s'----,R""e""s""u""lt",s,--__ U",n""i""t""s,--Report Limit __.m:.._Analyzed By CAS No.
1,2-Dibramoethane(EDB)ND ug/kg 6.0 1.2 09/26/05 14:42 DLK 106-93-4
DibrCllllCllllethane ND ug/kg
1,2-Dichlorobenzene ND ug/kg
1,3-Dich1orobenzene ND ug/kg
1,4-Dich1orobenzene ND ug/kg
Dichlorodifluoromethane ND ug/kg
1,1-Dichloroethane ND ug/kg
1,2-Dich1oroethane ND ug/kg
1,1-Dichloroethene ND ug/kg
cis-1,2-Dich1oroethene ND ug/kg
trans-1,2-Dichloroethene ND ug/kg
1,2-Dichloropropane ND ug/kg
1,3-Dichloropropane ND ug/kg
2,2-Dichloropropane ND ug/kg
1,1-Dichloropropene ND ug/kg
cis-1,3-Dichloropropene ND ug/kg
trans-1,3-Dichloropropene ND ug/kg
Diisopropylether ND ug/kg
Ethylbenzene ND ug/kg
Hexach1oro-1,3-butadiene ND ug/kg
2-Hexanone ND ug/kg
Isopropy1benzene(Cumene) ND ug/kg
p-Isopropy1toluene ND ug/kg
Methylene chloride 30. ug/kg
4-Methyl-2-pentanone(MIBK) ND ug/kg
Methyl-tert-butylether ND ug/kg
Naphthalene ND ug/kg
n-Propy1benzene ND ug/kg
Styrene ND ug/kg
1,1,1,2-Tetrachloroethane ND ug/kg
1,1,2,2-Tetrachloroethane ND ug/kg
Tetrachloroethene ND ug/kg
Toluene ND ug/kg
1,2,3-Trich1orobenzene ND ug/kg
1,2,4-Trich1orobenzene ND ug/kg
1,1,I-Trichloroethane ND ug/kg
1,1,2-Trich1oroethane ND ug/kg
Trichloroethene ND ug/kg
Trich1orof1uoramethane ND ug/kg
Project Sample Number: 92103573-001
Matrix: Soil
Date Collected:09/20/0512:00
Date Received: 09/20/0516:20
Lab Sample No: 926117888
Client Sample ID: P-12
Lab Project Number: 92103573
Client Project ID: West Morehead/6228-05-3103
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville,NC 28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone:[phone]
Fax:[phone]
'aceAnalytical ",
WI>M~p8ceIabs.oom
Charlotte Certification IDs
NCWastewater 12
NCDrinking Water 37706
SC 99006
FLNElAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall notbe reproduced,exceptin full,
wijhout the written consentof PaceAnalyticalServices,Inc,
~~~ii~~!lJt2L~~
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SCEnvironmental 99030
Fl NElAP E87648
Page: 5 of 22Date:09/28/05
Lah Sample No: 926117888 Project Sample Number:92103573-001 Date Collected:09/20/05 12:00
Client Sample ID: P-12 Matrix: Soil Date Received:09/20/05 16:20
Parameters Results Units ReI!ort LilIIit__m:_An!!J,Jl~ed ~CAS No.Oual RegLmt
1,2,3-Trichloropropane ND ug/kg 6.0 1.2 09/26/05 14:42 DLK 96-18-4
1,2,4-Trimethy1ben~ene ND ug/kg 6.0 1.2 09/26/05 14:42 DLK 95-63-6
l,3,5-Trimethylben~ene ND ug/kg 6.0 1.2 09/26/05 14:42 DLK 108-67-8
Vinyl acetate ND ug/kg 60.1.2 09/26/05 14:42 DLK 108-05-4
Vinyl chloride ND ug/kg 12.1.2 09/26/05 14:42 DLK 75-01-4
Xylene (Total)ND ug/kg 6.0 1.2 09/26/05 14:42 DLK 1330-20-7
mli:p-Xylene ND ug/kg 12.1.2 09/26/05 14:42 DLK
o-Xylene ND ug/kg 6.0 1.2 09/26/05 14:42 DLK 95-47-6
Toluene-d8 (S)95 %1.0 09/26/05 14:42 DLK 2037-26-5
4-Bramofluorohenzene (8)83 %1.0 09/26/05 14:42 DLK 460-00-4
Dihramofluoramethane (S)101 %1.0 09/26/05 14:42 DLK 1868-53-7
1,2-Dichloroethane-d4 (8)100 %1.0 09/26/05 14:42 DLK 17060-07-0
Lab Project Number: 92103573
Client Project ID: west Morehead/6228-05-3103
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]
IfIww.paoell1bs,com
Charlotte Certification IDs
NCWastewater 12
NCDrinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced.exceptin full,
wnhout thewritten consentof PaceAnalyticalServices,Inc.
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FL NELAP E87648
Page: 6 of 22Date: 09/28/05
MD Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
(S) SUrrogate
[1] Acid surrogate recovery outside of control limits. The data was accepted based on valid recovery of the two
remaining acid surrogates.
[2] Common laboratory contaminant.
2-Chloroethyl vinyl ether has been shown to degrade in the presence of acid.
Depending on the moisture content the PRLs can he elevated for all soil samples reported on a dry weight basis.
All pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate
hold tilIIe•
Method 9071B modified to use ASE.
Dilution factor shown represents the factor applied to the reported result and reporting limit due to changes
in sample preparation, dilution of the extract, or moisture content
PARAMETER FOOTNOTES
Lab Project Number: 92103573
Client Project ID: west Morehead/6228-05-3l03
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone:[phone]
Fax: [phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]
ace AnaJytica(W
VJww.paoo/a/Js"com
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP EB7627
REPORT OF LABORATORY ANALYSIS
This reportshallnot be reproduced,exceptinfull,
w~houtthe written consentof PaceAnalyticalServices,Inc.
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP EB764B
METHOD BLANK: 926130154
Associated Lab Samples:926117888
Blank Reporting
Pilrametgr Units Result L:iJni.t Footnotes
Acenaphthene ug/kg NO 330
Acenaphthylene ug/kg NO 330
Anthracene ug/kg NO 330
Benzo(k)fluoranthene ug/kg NO 330
Benzo(b)fluoranthene ug/kg NO 330
Benzo(a)anthracene ug/kg NO 330
Benzoic acid ug/kg NO 1600
Benzo(g,h,i)perylene ug/kg NO 330
Benzyl alcohol ug/kg NO 660
Benzo(a)pyrene ug/kg NO 330
4-Bromophenylphenyl ether ug/kg NO 330
Butylbenzylphthalate ug/kg NO 330
4-Chloro-3-methylphenol ug/kg NO .660
4-Chloroaniline ug/kg NO 660
bis(2-Chloroethoxy)methane ug/kg NO 330
bis(2-Chloroethyl) ether ug/kg NO 330
bis(2-Chloroisopropyl) ether ug/kg NO 330
2-Chloronaphthalene ug/kg NO 330
2-Chlorophenol ug/kg NO 330
4-Chlorophenylphenyl ether ug/kg NO 330
Chrysene ug/kg NO 330
Dibenz(a,h)anthracene ug/kg NO 330
Dibenzofuran ug/kg NO 330
1,2-Dichlorobenzene ug/kg NO 330
l,3-Dichlorobenzene ug/kg NO 330
l,4-Dichlorobenzene ug/kg NO 330
3,3I-Dichloroben.zidine ug/kg NO 660
2,4-Dichlorophenol ug/kg NO 330
Diethylphthalate ug/kg NO 330
2,4-Dimethylphenol ug/kg NO 330
Dimethylphthalate ug/kg NO 330
Date:09/28/05 page:7 of 22
926117888
Analysis Method: EPA 8270
Analysis Description: Semivolatile Organics
QC Batch: 138128
QC Batch Method: EPA 3545
Associated Lab Samples:
Lab Project Number: 92103573
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
·aceAnalytical'w
www.pacelabs.com
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not bereproduced,exceptin full,
without thewritten consentofPaceAnalyticalServices,Inc.~~~.~
i~
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SCEnvironmental 99030
FLNELAP E87648
METHOD BLANK: 926130154
Associated Lab S~les: 926117888
Blank Reporting
Pilrameter Units Result Lilnit Footnotes
Di-n-butylphtha1ate ug/kg ND 330
4,6-Dinitro-2-methy1pheno1 ug/kg ND 330
2,4-Dinitropheno1 ug/kg ND 1600
2,4-Dinitrotoluene ug/kg ND 330
2,6-Dinitrotoluene ug/kg ND 330
Di-n-octylpbthalate ug/kg ND 330
1,2-Diphenylhydrazine ug/kg ND 330
bis(2-Ethy1hexyl)phthalate ug/kg ND 330
Fluoranthene ug/kg ND 330
Fluorene ug/kg ND 330
Hexachloro-l,3-butadiene ug/kg ND 330
Hexachlorobenzene ug/kg ND 330
Hexachlorocyclopentadiene ug/kg ND 330
Hexachloroethane ug/kg ND 330
Indeno(1,2,3-cd)pyrene ug/kg ND 330
Isophorone ug/kg ND 330
2-Methylnaphtbalene ug/kg ND 330
2-Methylphenol (o-Cresol) ug/kg ND 330
3&4-Methylphenol ug/kg ND 330
Naphthalene ug/kg ND 330
2-Nitroaniline ug/kg ND 1600
3-Nitroaniline ug/kg ND 1600
4-Nitroaniline ug/kg ND 1600
Nitrobenzene ug/kg ND 330
2-Nitrophenol ug/kg ND 330
4-Nitrophenol ug/kg ND 1600
N-Nitroso-di-n-propylamine ug/kg ND 330
N-NitrosodiphenylBmine ug/kg ND 330
Pentachlorophenol ug/kg ND 1600
Phenanthrene ug/kg ND 330
Phenol ug/kg ND 330
Pyrene ug/kg ND 330
1,2,4-Trichlorobenzene ug/kg ND 330
2,4,5-Trichlorophenol ug/kg ND 330
2,4,6-Trichlorophenol ug/kg ND 330
Nitrobenzene-d5 (S)%54
Date:09/28/05 Page: 8 of 22
Lab Project Number: 92103573
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone:[phone]
Fax:[phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax:[phone]
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced.exceptin full,
w~houtthewritten consentof PaceAnalyticalServices, Inc.~~~;~~t~~~naac"~
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
LABORATORY CONTROL SAMPLE: 926130162
Spike LCS LCS
Parameter Units Cone. Result %Rec Footnotes
Acenaphthene ug/kg 1667.00 1122 67
Acenaphthy1ene ug/kg 1667.00 1120 67
Anthracene ug/kg 1667.00 1263 76
Benzo(k)f1uoranthene ug/kg 1667.00 1142 68
Benzo(b)fluoranthene ug/kg 1667.00 1128 68
Benzo(a)anthracene ug/kg 1~67.00 1177 71
Benzoic acid ug/kg 1667.00 373.5 22
Benzo(g,h,i)perylene ug/kg 1667.00 973.5 58
Benzyl alcohol ug/kg 1667.00 1425 86
Benzo(a)pyrene ug/kg 1667.00 1169 70
4-Bramophenylphenylether ug/kg 1667.00 1181 71
Butylbenzy1phtha1ate ug/kg 1667.00 1333 80
4-Ch1oro-3-methylpheno1 ug/kg 1667.00 1268 76
4-Cbloroaniline ug/kg 1667.00 1216 73
bis(2-Chloroethoxy)methane ug/kg 1667.00 1151 69
bis(2-Chloroethyl) ether ug/kg 1667.00 1090 65
bis(2-Chloroisopropyl)ether ug/kg 1667.00 1112 67
2-Chloronaphthalene ug/kg 1667.00 1101 66
2-Chlorophenol ug/kg 1667.00 1090 65
4-Cblorophenylphenylether ug/kg 1667.00 1159 70
Chrysene ug/kg 1667.00 1139 68
Dibenz(a,h)anthracene ug/kg 1667.00 1178 71
Dibenzofuran ug/kg 1667.00 1164 70
1,2-Dichlorobenzene ug/kg 1667.00 1091 65
1,3-Dichlorobenzene ug/kg 1667.00 1004 60
Date:09/28/05 Page: 9 of 22
%
%
%
%
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Pheno1-d5 (S)
2-Fluoropheno1 (S)
2,4,6-Tribramopheno1 (S)
Units
Reporting
Limit Footnotes
Blank
Result
48
75
53
50
66
%
926117888
METHOD BLANK: 926130154
Associated Lab Samples:
Lab Project Number: 92103573
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]www.pacetabs.com
Charlotte Certification IDs
NCWastewater 12
NCDrinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced,exceptin full,
withoutthewritten consentof PaceAnalyticalServices,Inc.
~
~-,j-!M.r~
;..~!:i
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SCEnvironmental 99030
FLNELAP E87648
LABORATORY CONTROL SAMPLE:926130162
Spike LCS LCS
Paramat.er Units Conc. Result %Rec Footnotes
1,4-Dichlorobenzene ug/kg 1667.00 1031 62
3,3'-Dichlorobenzidine ug/kg 3333.00 1121 34
2,4-Dichlorophenol ug/kg 1667.00 1105 66
Diethylphthalate ug/kg 1667.00 1277 77
2,4-Dimethylphenol ug/kg 1667.00 1170 70
Dimethylphthalate ug/kg 1667.00 1183 71
Di-n-butylphthalate ug/kg 1667.00 1374 82
4,6-Dinitro-2-methylphenol ug/kg 1667.00 1088 65
2,4-Dinitrophenol ug/kg 1667.00 714.7 43
2,4-Dinitrotoluene ug/kg 1667.00 1145 69
2,6-Dinitrotoluene ug/kg 1667.00 1134 68
Di-n-octylphthalate ug/kg 1667.00 1223 73
1,2-Diphenylhydrazine ug/kg 1667.00 1179 71
bis(2-Ethylhexyl)phthalate ug/kg 1667.00 1392 84
Fluoranthene ug/kg 1667.00 1204 72
Fluorene ug/kg 1667.00 1179 71
Hexachloro-l,3-butadiene ug/kg 1667.00 1061 64
Hexachlorobenzene ug/kg 1667.00 1219 73
Hexachlorocyclopentadiene ug/kg 1667.00 665.8 40
Hexachloroethane ug/kg 1667.00 1050 63
Indeno(1,2,3-cd)pyrene ug/kg 1667.00 1057 63
Isophorone ug/kg 1667.00 1421 85
2-Methylnaphthalene ug/kg 1667.00 1156 69
2-Methylphenol (o-Cresol)ug/kg 1667.00 1220 73
3&4-Methylphenol ug/kg 1667.00 1215 73
Naphthalene ug/kg 1667.00 1087 65
2-Nitroaniline ug/kg 1667.00 987.1 59
3-Nitroaniline ug/kg 1667.00 992.6 60
4-Nitroaniline ug/kg 1667.00 1026 62
Nitrobenzene ug/kg 1667.00 1183 71
2-Nitrophenol ug/kg 1667.00 1055 63
4-Nitrophenol ug/kg 1667.00 1426 86
N-Nitroso-di-n-propylamdne ug/kg 1667.00 1297 78
N-Nitrosodiphenylamdne ug/kg 1667.00 1274 76
Pentachlorophenol ug/kg 1667.00 1222 73
Phenanthrene ug/kg 1667.00 1180 71
Phenol ug/kg 1667.00 1190 71
Date: 09/28/05 Page: 10 of 22
Lab Project Number: 92103573
Client Project ID: west Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax:[phone]
Pace Analytical Services, Itlc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]
'BceAnalyticar~
www,pacelabs,ccm
Charlotte Certification IDs
NCWastewater 12
NCDrinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not bereproduced,exceptin full,
wtthout thewritten consentof PaceAnalyticalServices,Inc.
it2~,,(J..1t1(:I).f.
Asheville Certification ID§
NCWastewater 40
NCDrinking Water 37712
SCEnvironmental 99030
FLNELAP E87648
page:11 of 22Date:09/28/05
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 926130188 926130196
926100918 Spike MS MSD MS MSD
P!!,;rameter Units Result _£onc.Result Result %Rec %Rec RPD Footnotes
Acenaphthene ug/kg 1610 2137.00 7113 10400 258 412 38 1,1,2
4-Chloro-3~thylphenol ug/kg 0 2137.00 1444 1494 68 70 3
2-Ch1orophenol ug/kg 0 2137.00 1301 1279 61 60 2
1,4-Dich1orobenzene ug/kg 0 2137.00 1383 1199 65 56 14
2,4-Dinitroto1uene ug/kg 0 2137.00 1240 1219 58 57 2
4-Nitrophenol ug/kg 0 2137.00 1707 1697 80 79 1
N-Nitroso-di-n-propylamdne ug/kg 0 2137.00 1711 1596 80 75 7
Pentachlorophenol ug/kg 0 2137.00 1088 981.7 51 46 10
Phenol ug/kg 0 2137.00 1409 1402 66 66 1
Pyrene ug/kg 10200 2137.00 37610 53320 1283 2018 35 1,1,2
1,2,4-Trich1orobenzene ug/kg 0 2137.00 1369 1249 64 58 9
Nitrobenzene-d5 (S)74 70
2-Fluorobiphenyl (S)68 65
Terphenyl-d14 (S)84 83
Phenol-d5 (S)66 63
2-F1uorophenol (S)54 54
2,4,6-Tribromophenol (S)64 64
Spike LCS LCS
~lI.rameter Un~ts Cone. Result %Rec Footnotes
Pyrene ug/kg 1667.00 1163 70
1,2,4-Trieh1orobenzene ug/kg 1667.00 998.1 60
2,4,5-Trich1orophenol ug/kg 1667.00 1104 66
2,4,6-Trichlorophenol ug/kg 1667.00 1103 66
Nitrobenzene-d5 (S)72
2-F1uorobiphenyl (S)68
Terpheny1-d14 (S)78
Pheno1-d5 (S)71
2-Fluorophenol (S)64
2,4,6-Tribromopheno1 (S)77
LABORATORY CONTROL SAMPLE: 926130162
Lab Project Number: 92103573
Client Project ID: west Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services,Inc.
2225 Riverside Drive
Asheville, NC28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 KinceyAvenue,Suite 100
Huntersville, NC28078
Phone:[phone]
Fax: [phone]
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall notbereproduced,exceptin full,
wtthoutthe written consentof PaceAnalyticalServices,Inc.
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP EB7648
Page: 12 of 22
NC
RPD Footnotes
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
Date:09/28/05
SAMPLE DUPLICATE: 926130170
926108473 DtJP
Par8JJleter Units Result Result
Acenaphthene ug/kg NO NO
Acenaphthy1ene ug/kg NO NO
Anthracene ug/kg NO NO
Benzo(a)anthracene ug/kg NO NO
Benzo(a)pyrene ug/kg NO NO
Benzo(b)fluoranthene ug/kg NO NO
Benzo(g,h,i)perylene ug/kg NO NO
Benzo(k)f1uoranthene ug/kg NO NO
Chrysene ug/kg NO NO
Dibenz(a,h)anthracene ug/kg NO NO
F1uoranthene ug/kg NO NO
Fluorene ug/kg NO NO
Indeno(1,2,3-cd)pyrene ug/kg NO NO
Naphthalene ug/kg NO NO
Phenanthrene ug/kg NO NO
Pyrene ug/kg NO NO
Nitrobenzene-d5 (S)%51 56
2-Fluorobipheny1 (S)%47 53
Terpheny1-d14 (S)%67 64
2-Methy1naphtha1ene ug/kg NO NO
Lab Project NUmber: 92103573
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville,NC28804
Phone:[phone]
Fax: [phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone:[phone]
Fax:[phone]
'ace Ana/yticar~
wl'lw.pacef8b$.com
Charlotte Certification IDs
NCWastewater 12
NCDrinking Water 37706
SC 99006
FL NELAP E87627
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SCEnvironmental 99030
Fl NElAP E87648
REPORT OF LABORATORY ANALYSIS
This reportshallnot be reproduced,exceptin full,
withoutthewritten consentof PaceAnalyticalServices,Inc.f~s-=ii~~~11JemC~_
Page: 13 of 22Date:09/28/05
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
Acetone
Benzene
Bramobenzene
Bramoch1oromethane
Bramodichloramethane
Bromoform
Bramomethane
2-Butanone (MEK)
n-Buty1benzene
sec-Buty1benzene
tert-Buty1benzene
Carbon tetrachloride
Chlorobenzene
Ch1oroethane
Chloroform
Chloromethane
2-Ch1oroto1uene
4-Ch1oroto1uene
1,2-Dibromo-3-ch1oropropane
Dibramochloramathane
1,2-Dibromoethane (EDB)
Dibramomethane
1,2-Dich1orobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dich1orodif1uoramethane
l,l-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-l,2-Dichloroethene
trans-l,2-Dichloroethene
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Paramater units
Blank
Result
Reporting
Limit Footnotes
100
5.0
5.0
5.0
5.0
5.0
10.
100
5.0
5.0
5.0
5.0
5.0
10.
5.0
10.
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10.
5.0
5.0
5.0
5.0
5.0
926117888
METHOD BLANK: 926142274
Associated Lab Samples:
926117888
Analysis Method: EPA 8260
Analysis Description: GC/MS VOCs by 8260, low level
QC Batch: 138342
QC Batch Method: EPA 8260
Associated Lab Samples:
Lab Project Number: 92103573
Client Project ID: west Morehead/6228-0S-3103
QUALITY CONTROL DATA
V'/L'III1.pEoelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Huntersville,NC28078
Phone: [phone]
Fax:[phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville,NC28804
Phone: [phone]
Fax:[phone]
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SC Environmental 99030
FL NELAP E87648
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,exceptinfull,
w~houtthe written consentof PaceAnalyticalServices,Inc.
$:?~}#!ltt1dl.li
Date:09/28/05 Page: 14 of 22
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
MD
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1,2-Dich1oropropane
1,3-Dich1oropropane
2,2-Dich1oropropane
1,1-Dich1oropropene
cis-l,3-Dich1oropropene
trans-1,3-Dich1oropropene
Diisopropy1 ether
Ethy1benzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (CUmene)
p-Isopropy1to1uene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrach1oroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trich1orobenzene
1,2,4-Trichlorobenzene
l,l,l-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
l,3,S-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&:p-Xylene
o-Xylene
Parameter units
Blank
Result
Reporting
Limit Footnotes
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
50.
5.0
5.0
5.0
50.
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
50.
10.
5.0
10.
5.0
926117888
METHOD BLANK: 926142274
Associated Lab Samples:
Lab Project Number: 92103573
Client Project ID: west Morehead/-6228-0S-3l03
QUALITY CONTROL DATA
vlww.par:ffiabs.com
PaceAnalytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC28018
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone:[phone]
Fax:[phone]
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshallnot be reproduced,exceptin full,
withoutthewrittenconsentof PaceAnalyticalServices,Inc.
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP EB7648
LABORATORY CONTROL SAMPLE: 926142282
Spike LCS LCS
Pg~te;[Units Cone. Result %Rec Footnotes
Acetone ug/kg 100.00 75.46 76
Benzene ug/kg 50.00 41.43 83
Bromobenzene ug/kg 50.00 38.59 77
Bromochloromethane ug/kg 50.00 42.88 86
BrOlnodichloromet.hane ug/kg 50.00 41.60 83
Bromoform ug/kg 50.00 41.48 83
BromomethaIie ug/kg 50.00 38.80 78
2-Butanone (MEK)ug/kg 100.00 91.44 91
n-Butylbenzene ug/kg 50.00 37.45 75
sec-Buty1benzene ug/kg 50.00 37.81 76
tert-Butylbenzene ug/kg 50.00 36.87 74
Carbon tetrachloride ug/kg 50.00 42.39 85
Chlorobenzene ug/kg 50.00 41.23 82
Chloroethane ug/kg 50.00 34.34 69
Chloroform ug/kg 50.00 41.68 83
Chloramethane ug/kg 50.00 44.19 88
2-Chlorotoluene ug/kg 50.00 38.13 76
4-Chlorotoluene ug/kg 50.00 40.58 81
1,2-Dibromo-3-chloropropane ug/kg 50.00 40.41 81
Dibromocbloromethane ug/kg 50.00 39.26 78
1,2-Dibromoethane (EDB) ug/kg 50.00 41.30 83
Dibramomethane ug/kg 50.00 41.56 83
1,2-Dichlorobenzene ug/kg 50.00 40.81 82
1,3-Dichlorobenzene ug/kg 50.00 41.70 83
1,4-Dichlorobenzene ug/kg 50.00 41.67 83
Dich1orodifluoramethane ug/kg 50.00 49.29 99
Date:09/28/05 Page: 15 of 22
Blank Reporting
Pari!m!i!ter Units Result Limit Footnotes
Toluene-d8 (S)%102
4-Bromof1uorobenzene (S)%102
Dibromofluoramethane (S)%98
1,2-Dichloroethane-d4 (S)%101
926117888
METHOD BLANK: 926142274
Associated Lab Samples:
Lab Project Number: 92103573
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville,NC28804
Phone:[phone]
Fax: [phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville,NC28078
Phone: [phone]
Fax:[phone]
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
Fl NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced.exceptin full,
w~houtthewritten consentof PaceAnalyticalServices.Inc.
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
Fl NELAP EB7648
QUALITY CONTROL DATA
Lab Project Number: 92103573
Client Project ID:west Morehead/6228-05-3103
LABORATORY CONTROL SAMPLE: 926142282
Spike LCS LCS
PAr~!;,er Units Cone.Result %Rec Footnotes
l,l-Dichloroethane ug/kg 50.00 37.16 74
1,2-Dichloroethane ug/kg 50.00 40.78 82
l,l-Dichloroethene ug/kg 50.00 42.68 85
cis-l,2-Dichloroethene ug/kg 50.00 37.77 76
trans-l,2-Dichloroethene ug/kg 50.00 39.80 80
1,2-Dichloropropane ug/kg 50.00 40.51 81
1,3-Dichloropropane ug/kg 50.00 41.07 82
2,2-Dichloropropane ug/kg 50.00 45.63 91
l,l-Dichloropropene ug/kg 50.00 40.87 82
cis-l,3-Dichloropropene ug/kg 50.~OO 45.03 90
trans-l,3-Dichloropropene ug/kg 50.00 48.04 96
Diisopropyl ether ug/kg 50.00 38.83 78
Ethylbenzene ug/kg 50.00 40.59 81
Hexachloro-l,3-butadiene ug/kg 50.00 40.54 81
2-Hexanone ug/kg 100.00 86.76 87
Isopropylbenzene (Cumene) ug/kg 50.00 43.27 86
p-Isopropy1toluene ug/kg 50.00 35.24 70
Methylene chloride ug/kg 50.00 34.45 69
4-Methyl-2-pentanone (MIBK)ug/kg 100.00 104.0 104
Methyl-tert-butyl ether ug/kg 50.00 41.10 .82
Naphthalene ug/kg 50.00 41.38 83
n-Propylbenzene ug/kg 50.00 38.78 78
Styrene ug/kg 50.00 44.78 90
1,1,1,2-Tetrachloroethane ug/kg 50.00 39.11 78
1,1,2,2-Tetrachloroethane ug/kg 50.00 39.39 79
Tetrachloroethene ug/kg 50.00 39.33 79
Toluene ug/kg 50.00 40.64 81
1,2,3-Trichlorobenzene ug/kg 50.00 46.61 93
1,2,4-Trichlorobenzene ug/kg 50.00 51.16 102
1,1,l-Trichloroethane ug/kg 50.00 41.34 83
1,l,2-Trichloroethane ug/kg 50.00 39.90 80
Trichloroethene ug/kg 50.00 42.63 85
Trichlorofluoromethane ug/kg 50.00 42.12 84
l,2,3-Trichloropropane ug/kg 50.00 41.86 84
l,2,4-Trimethylbenzene ug/kg 50.00 37.38 75
1,3,5-Trimethylbenzene ug/kg 50.00 35.68 71
Vinyl acetate ug/kg 100.00 495.1 495 3
Date:09/28/05 Page: 16 of 22
Pace Analytical Services,Inc.
2225 Riverside Drive
Asheville, NC28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville,NC28078
Phone: [phone]
Fax: [phone]
see Analytical'M
www.pacelabs.oom
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not bereproduced.exceptin full,
wnhout the written consentof PaceAnalyticalServices,Inc.
~l!.~~fl:'"
!J~~ff{1Jt:ld\..:~~
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP EB7648
Page:17 of 22Date:09/28/05
Spike LCS LCS
Parameter Units Cone. Result %Ree Footnotes
Vinyl chloride ug/kg 50.00 40.76 82
Xylene (Total)ug/kg 150.00 123.1 82
m&:p-Xylene ug/kg 100.00 B1.56 82
o-Xylene ug/kg 50.00 41.54 83
Toluene-dB (S)101
4-Bromofluorobenzene (S)101
Dibromofluoromethane (S)98
1,2-Dichloroethane-d4 (S)96
LABORATORY CONTROL SAMPLE: 926142282
Lab Project Number: 92103573
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville,NC28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax:[phone]
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall notbereproduced.exceptin full,
without the written consentof PaceAnalyticalServices.Inc.
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP EB7648
Page: 18 of 22Date:09/28/05
Footnotes
4,4
RPD
38
%Rec %Rec
o 0
926117888
ResultunitsParameter
MSDMSMSD
Result
0.0903
MS
Result
0.1323
Spike
Conc._
0.08070.1484mg/kgMercury
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 926131574 926131582
mg/kgMercury
Conc. Result %Rec Footnotes
0.0667 0.0637 96
unitsPar!ll!l9ter
LCSLCSSpike
LABORATORY CONTROL SAMPLE:'926130691
926117888
Analysis Method: EPA 7471
Analysis Description:Mercury, CVAAS, in Soil
QC Batch: 138149
QC Batch Method: EPA 7471
Associated Lab Samples:
Lab Project Number: 92103573
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville, NG28804
Phone: [phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]
'aceAnaJytical'~
www.pacetabS.rom
Charlotte Certification IDs
NGWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not bereproduced,exceptin full,
wijhout thewritten consentof PaceAnalyticalServices,Inc.~~!~::¥~~~IDelaCt;
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SC Environmental 99030
FLNELAP E87648
926096504 Spike MS MSD MS MSD
Par~Ur units Result Conc. Result Result %Rec %Rec RPD Footnotes
Arsenic mg/kg 1.675 61.49 59.68 58.11 94 88 3
Barium mg/kg 97.35 61.49 147.1 123.0 81 40 18 4
Cadmium mg/kg 0 61.49 55.34 54.14 90 85 2
Chromium mg/kg 5.359 61.49 66.55 65.71 100 94 1
Lead mg/kg 8.406 61.49 68.00 69.21 97 95 2
Date:09/28/05 Page: 19 of 22
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 926125329 926125337
LABORATORY CONTROL SAMPLE: 926125311
Spike LCS LCS
P~r~ter Units Cone.Result %Rec Footnotes
Arsenic mg/kg 50.00 47.90 96
Barium mg/kg 50.00 48.50 97
Cadmium mg/kg 50.00 45.30 91
Chromium mg/kg 50.00 47.20 94
Lead mg/kg 50.00 48.20 96
Selenium mg/kg 50.00 46.60 93
Silver mg/kg 50.00 48.40 97
Blank Reporting
Parameter units Result Limit Footnotes
Arsenic mg/kg ND 0.50
Barium mg/kg ND 0.50
Cadmium mg/kg ND 0.10
Chromium mg/kg ND 0.20
Lead mg/kg ND 0.50
Selenium mg/kg ND 0.50
Silver mg/kg ND 0.20
926117888
METHOD BLANK: 926125303
Associated Lab Samples:
926117888
Analysis Method: EPA 6010
Analysis Description: Metals, Trace ICP
QC Batch: 138031
QC Batch Method: EPA 3050
Associated Lab Samples:
Lab Project NUmber: 92103573
Client Project ID: west Morehead/6228-05-3103
QUALITY CONTROL DATA
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville,NC28804
Phone: [phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite toO
Huntersville, NC28018
Phone: [phone]
Fax: [phone]
ace Analyticaf'w
www.pacetabS.com
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced.exceptin full.
wtthoutthe written consentof PaceAnalyticalServices,Inc.
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Page: 20 of 22Date:09/28/05
926096504 Spike MS MSD MS MSD
Parameter Units Result Cone.Result Result %Ree %Ree RPD Footnotes
Selenium mg/kg 0 61.49 55.34 54.50 90 85 2
Silver DIg/kg 0 61.49 60.41 59.32 98 93 2
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 926125329 926125337
Lab Project Number: 92103573
Client Project ID: west Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone:[phone]
Fax:[phone]VIl'AI!.pacefabs.com
Charlotte Certification IDs
NCWastewater 12
NCDrinking Water 3n06
SC 99006
FL NEUIP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced.exceptin full,
without thewritten consentof PaceAnalyticalServices.Inc.
~~~~g!tJt::ItU-'~
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SC Environmental 99030
FL NELAP E87648
Page: 21 of 22Date:09/28/05
RPD Footnotes
227.4027.00%Percent Moisture
ResultResultUnits;parameter
926117037 DUP
SAMPLE DUPLICATE: 926118324
926117888
Analysis Method:%Moisture
Analysis Description: Percent Moisture
QC Batch: 137895
QC Batch Method:
Associated Lab Samples:
Lab Project Number: 92103573
Client Project ID: west Morehead/6228-05-3103
QUALITY CONTROL DATA
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
'BceAnalytlcar
WWW.pacel8bs,ccm
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 3n06
SG 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall notbe reproduced,exceptin full,
without the written consentof PaceAnalyticalServices,Inc.
~··.c~tr...",~...~~~
g1iielaO\
Asheville Certification IDs
NGWastewater 40
NGDrinking Water 37712
SGEnvironmental 99030
FL NELAP E87648
Page: 22 of 22
Laboratory Control Sample (Duplicate)
Matrix Spike (Duplicate)
Sample Duplicate
Not detected at or above adjusted reporting limit
Not Calculable
Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
Adjusted Method Detection Limit
Relative Percent Difference
SUrrogate
The surrogate and/or spike recovery was outside acceptance limits.
The calculated RPD was outside QC acceptance limits.
Recovery falls outside of QC limits, however, this compound is not found in the associated samples.
The spike recovery was outside acceptance limits for the MS and lor MSD due to matrix interference. The LCS
and/or LCSD were within acceptance limits showing that the laboratory is in control and the data is
acceptable.
Date:09/28/05
LCS(D)
MS(D)
DUP
ND
NC
J
MDL
RPD
(S)
[1]
[2]
[3]
[4]
Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate %Rec and RPD values.
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Lab Project Number: 92103573
Client Project ID: West Morehead/6228-05-3103
PaceAnalytical Services. Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
PaceAnalytical Services. Inc.
9800 Kincey Avenue. Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
tlce Analytical N
WW\l~pacelliJbs.com
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Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, exceptin full,
wtthout the written consent of PaceAnalyticalServices, Inc.
~.ftl:}.~(lJt:ItI,L.J:
Asheville Certification IDs
NCWastewater 40
NGDrinking Water 37712
SC Environmental 9g030
FL NELAP E87648
Enclosures
Annette Scott
Annette. Scott®pacelabs. com
Project Manager
Sincerely,
If you have any questions concerning this report please feel free to contact me.
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic testing
was performed at our Pace Charlotte laboratory unless otherwise footnoted.
Enclosed are the analytical results for samp1e(s) received by the laboratory on September 23, 2005. Results
reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the
body of the report.
Dear Mr. Foster:
RE: Lab Project Number: 92103894
Client Project ID: West Morehead/6228-05-3103
Mr. Rob Foster
Mactec
2801 Yorkmont Road
Suite 100
Charlotte, NC 28208
October 03,2005
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
ace Analyticar~
www.pacelabs.com
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
$C 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
w~hout the written consent of PaceAnalyticat Services, Inc.
., UC!:I:,.,~..p_')'_t~~
§i'J)eJa.C~
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 9!1030
FL NELAP E87648
Lab Project Number:92103894
Client Project ID: West Morehead/6228-05-3103
Lab Sample No: 926136292 Project Sample Number: 92103894-001 Date Collected:09/21/05 17:00
Client Sample ID: B-2 Matrix:Water Date Received:09/23/05 15:45
Parii!!!!et~rl!Result!! Units Re~ort Limit _Qf__Analyz~g By CAS No.Oual RegLmt
Metals
Metals by Trace ICP Prep/Method: EPA 3010 /EPA 6010
Arsenic NO mg/l 0.0050 1.0 09/30/05 05:07 ALV 7440-38-2
Barium 0.62 mg/l 0.0050 1.0 09/30/05 05:07 ALV 7440-39-3
Cadmium NO mg/l 0.0010 1.0 09/30/05 05:07 ALV 7440-43-9
Chromium 0.038 mg/l 0.0020 1.0 09/30/05 05:07 ALV 7440-47-3
Lead 0.046 mg/l 0.0050 1.0 09/30/05 05:07 ALV 7439-92-1
Selenium NO mg/l 0.0050 1.0 09/30/05 05:07 ALV 7782-49-2
Silver NO mg/l 0.0020 1.0 09/30/05 05:07 ALV 7440-22-4
Date Digested 09/28/05 06:30 09/28/05 06:30
Mercury, CVAAS, in Water Method: EPA 7470
Mercury 0.00082 mg/l 0.00020 1.0 09/29/05 15:53 EWS 7439-97-6
GC Volatiles
GC VOCs in Water Method: SM 6230D
Benzene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 71-43-2
Bromobenzene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 108-86-1
Bromochloromethane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 74-97-5
Bromodichloromethane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 75-27-4
Bromoform NO ug/l 0.50 1.0 09/29/05 09:26 PPM 75-25-2
Bromomethane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 74-83-9
n-Butylbenzene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 104-51-8
sec-Butylbenzene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 135-98-8
tert-Butylbenzene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 98-06-6
Carbon tetrachloride NO ug/l 0.50 1.0 09/29/05 09:26 PPM 56-23-5
Chlorobenzene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 108-90-7
Chloroethane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 75-00-3
Chloroform NO ug/l 0.50 1.0 09/29/05 09:26 PPM 67-66-3
Chloromethane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 74-87-3
2-Chlorotoluene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 95-49-8
4-Chlorotoluene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 106-43-4
1,2-Dibromo-3-chloropropane NO ug/l 2.0 1.0 09/29/05 09:26 PPM 96-12-8
Dibromochloromethane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 124-48-1
1,2-Dibromoethane (EDB)NO ug/l 0.50 1.0 09/29/05 09:26 PPM 106-93-4
Dibromomethane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 74-95-3
1,2-Dich1orobenzene NO ug/1 1.0 1.0 09/29/05 09:26 PPM 95-50-1
1,3-Dichlorobenzene NO ug/1 1.0 1.0 09/29/05 09:26 PPM 541-73-1
1,4-Dich1orobenzene NO ug/l 1.0 1.0 09/29/05 09:26 PPM 106-46-7
Date: 10/03/05 Page:1 of 22
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28018
Phone:[phone]
Fax: [phone]www.pace/abs.com
Charlotte Certification IDs
NOWastewater 12
NO Drinking Water 37706
SO 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not bereproduced,exceptin full,
w~houtthe written consentof PaceAnalyticalServices,Inc.
~{{=~~~~,
glnaaa~
Asheville Certification 105
NC Wastewater 40
NO Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Lab Project Number:92103894
Client Project ID:West Morehead/6228-05-3103
Lab Sample No:926136292 Project Sample Number: 92103894-001 Date Collected:09/21/05 17:00
Client Sample ID: B-2 Matrix:Water Date Received:09/23/05 15:45
!!Iu;:amet.cr!!Results Units RellortLimit __m:_Analyze!;!By CAS No.Oual RegLmt
Dichlorodifluoromethane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 75-71-8
1,1-Dichloroethane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 75-34-3
1,2-Dichloroethane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 107-06-2
1,1-Dichloroethene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 75-35-4
cis-1,2-Dichloroethene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 156-59-2
trans-l,2-Dichloroethene 1.1 ug/l 0.50 1.0 09/29/05 09:26 PPM 156-60-5
1,2-Dichloropropane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 78-87-5
1,3-Dichloropropane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 142-28-9
2,2-Dichloropropane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 594-20-7
1,1-Dichloropropene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 563-58-6
cis-l,3-Dichloropropene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 10061-01-5
trans-l,3-Dichloropropene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 10061-02-6
Diisopropyl ether NO ug/l 0.50 1.0 09/29/05 09:26 PPM 108-20-3
Ethylbenzene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 100-41-4
Hexachloro-l,3-butadiene NO ug/l 2.0 1.0 09/29/05 09:26 PPM 87-68-3
Isopropylbenzene (Cumene)NO ug/l 0.50 1.0 09/29/05 09:26 PPM 98-82-8
p-Isopropyltoluene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 99-87-6
Methylene chloride NO ug/l 2.0 1.0 09/29/05 09:26 PPM 75-09-2
Methyl-tert-butyl ether NO ug/l 0.50 1.0 09/29/05 09:26 PPM 1634-04-4
Naphthalene 2.7 ug/l 2.0 1.0 09/29/05 09:26 PPM 91-20-3
n-Propylbenzene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 103-65-1
Styrene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 100-42-5
1,1,1,2-Tetrachloroethane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 630-20-6
1,1,2,2-Tetrachloroethane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 79-34-5
Tetrachloroethene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 127-18-4
Toluene 0.79 ug/l 0.50 1.0 09/29/05 09:26 PPM 108-88-3
1,2,3-Trichlorobenzene NO ug/l 2.0 1.0 09/29/05 09:26 PPM 87-61-6
1,2,4-Trichlorobenzene NO ug/l 2.0 1.0 09/29/05 09:26 PPM 120-82-1
1,1,l-Trichloroethane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 71-55-6
1,1,2-Trichloroethane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 79-00-5
Trichloroethene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 79-01-6
Trichlorofluoromethane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 75-69-4
1,2,3-Trichloropropane NO ug/l 0.50 1.0 09/29/05 09:26 PPM 96-18-4
1,2,4-Trimethylbenzene 0.77 ug/l 0.50 1.0 09/29/05 09:26 PPM 95-63-6
1,3,5-Trimethylbenzene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 108-67-8
Vinyl chloride 0.69 ug/l 0.50 1.0 09/29/05 09:26 PPM 75-01-4
m&:p-Xylene NO ug/l 0.50 1.0 09/29/05 09:26 PPM
o-Xylene NO ug/l 0.50 1.0 09/29/05 09:26 PPM 95-47-6
l-Chloro-3-fluorobenzene (S)100 %1.0 09/29/05 09:26 PPM 625-98-9
Oat.:10/03/05 Page: 2 of 22
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]www.paoo/abs.com
Charlotte Certification IDs
NOWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not bereproduced,exceptin full,
without the written consentof PaceAnalyticalServices,Inc.
",~~_,l.~~
fHeIaO'~" "".\'~..~
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Lab Project Number:92103894
Client Project ID: west Morehead/6228-05-3103
Lab Sample No:926136300 Project Sample Number:92103894-002 Date Collected:09/23/05 14:30
Client Sample ID: B-7 Matrix:Water Date Received:09/23/05 15:45
Pjlri!lll!i!t!i!:!::§Results Units Re~ort Limit ~Anal:lzed By CAS No.Qual RegLmt
Metals
Metals by Trace ICP Prep/Method: EPA 3010 /EPA 6010
Arsenic 0.0052 mg/l 0.0050 1.0 09/30/05 16:28 SIIB 7440-38-2
Barium 0.14 mg/l 0.0050 1.0 09/30/05 16:28 SIIB 7440-39-3
Cadmium NO mg/l 0.0010 1.0 09/30/05 16:28 SIIB 7440-43-9
Chromium 0.021 mg/l 0.0020 1.0 09/30/05 16:28 SIIB 7440-47-3
Lead 0.0091 mg/l 0.0050 1.0 09/30/05 16:28 SIIB 7439-92-1
Selenium NO mg/l 0.0050 1.0 09/30/05 16:28 SIIB 7782-49-2
Silver NO mg/l 0.0020 1.0 09/30/05 16:28 SIIB 7440-22-4
Date Digested 09/27/05 11:30 09/27/05 11:30
Mercury, CVAAS, in Water Method: EPA 7470
Mercury NO mg/l 0.00020 1.0 09/29/05 15:53 EWS 7439-97-6
GC Volatiles
GC VQCs in Water Method: SM 6230D
Benzene 3.6 ug/l 0.50 1.0 09/29/05 10:09 PPM 71-43-2
Bromobenzene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 108-86-1
Bromochloromethane NO ug/l 0.50 1.0 09/29/05 10:09 PPM 74-97-5
Bromodichloromethane NO ug/l 0.50 1.0 09/29/05 10:09 PPM 75-27-4
Bromoform NO ug/l 0.50 1.0 09/29/05 10:09 PPM 75-25-2
Bromomethane NO ug/l 0.50 1.0 09/29/05 10:09 PPM 74-83-9
n-Butylbenzene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 104-51-8
sec-Butylbenzene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 135-98-8
tert-Butylbenzene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 98-06-6
Carbon tetrachloride NO ug/l 0.50 1.0 09/29/05 10:09 PPM 56-23-5
Chlorobenzene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 108-90-7
Chloroethane NO ug/l 0.50 1.0 09/29/05 10:09 PPM 75-00-3
Chloroform NO ug/l 0.50 1.0 09/29/05 10:09 PPM 67-66-3
Chloromethane NO ug/l 0.50 1.0 09/29/05 10:09 PPM 74-87-3
2-Chlorotoluene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 95-49-8
4-Chlorotoluene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 106-43-4
1,2-Dibromo-3-chloropropane NO ug/l 2.0 1.0 09/29/05 10:09 PPM 96-12-8
Dibromochloromethane NO ug/l 0.50 1.0 09/29/05 10:09 PPM 124-48-1
1,2-Dibromoethane (EDB)NO ug/l 0.50 1.0 09/29/05 10:09 PPM 106-93-4
Dibromomethane NO ug/l 0.50 1.0 09/29/05 10:09 PPM 74-95-3
1,2-Dichlorobenzene NO ug/l 1.0 1.0 09/29/05 10:09 PPM 95-50-1
1,3-Dichlorobenzene NO ug/l 1.0 1.0 09/29/05 10:09 PPM 541-73-1
1,4-Dichlorobenzene NO ug/l 1.0 1.0 09/29/05 10:09 PPM 106-46-7
Date:10/03/05 Page:3 of 22
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone:[phone]
Fax: [phone]www.pacelabs.com
Charlotte Certification IDs
NCWastewater 12
Ne Drinking Water 37706
SoC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PaceAnalytical Services, Inc,
..q~'~~.£]-~~.§tI~;
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SCEnvironmental 99030
FLNELAP E8764B
Lab Project Number: 92103894
Client Project ID:West Morehead/6228-05-3103
Lab Sample No:926136300 Project Sample Number:92103894-002 Date Collected:09/23/05 14:30
Client Sample ID: B-7 Matrix:Water Date Received:09/23/05 15:45
Pilrameters Results Units Re~ort Limit ~Analyzed By CAS No.QygJ,_RegLmt
Dichlorodifluoromethane NO ug/l 0.50 1.0 09/29/05 10:09 PPM 75-71-8
l,l-Dichloroethane NO ug/l 0.50 1.0 09/29/05 10:09 PPM 75-34-3
1,2-Dichloroethane NO ug/l 0.50 1.0 09/29/05 10;09 PPM 107-06-2
1,1-Dichloroethene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 75-35-4
cis-1,2-Dichloroethene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 156-59-2
trans-l,2-Dichloroethene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 156-60-5
1,2-Dichloropropane NO ug/l 0.50 1.0 09/29/05 10:09 PPM 78-87-5
1,3-Dichloropropane NO ug/l 0.50 1.0 09/29/05 10:09 PPM 142-28-9
2,2-Dichloropropane NO ug/l 0.50 1.0 09/29/05 10:09 PPM 594-20-7
1,1-Dichloropropene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 563-58-6
cis-1,3-Dichloropropene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 10061-01-5
trans-l,3-Dichloropropene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 10061-02-6
Diisopropyl ether NO ug/l 0.50 1.0 09/29/05 10:09 PPM 108-20-3
Ethylbenzene 0.51 ug/l 0.50 1.0 09/29/05 10:09 PPM 100-41-4
Hexachloro-l,3-butadiene NO ug/l 2.0 1.0 09/29/05 10:09 PPM 87-68-3
Isopropylbenzene (Cumene)NO ug/l 0.50 1.0 09/29/05 10:09 PPM 98-82-8
p-Isopropyltoluene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 99-87-6
Methylene chloride NO ug/l 2.0 1.0 09/29/05 10:09 PPM 75-09-2
MethYl-tert-butyl ether 0.86 ug/l 0.50 1.0 09/29/05 10:09 PPM 1634-04-4
Naphthalene NO ug/l 2.0 1.0 09/29/05 10:09 PPM 91-20-3
n-Propylbenzene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 103-65-1
Styrene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 100-42-5
1,1,1,2-Tetrachloroethane NO ug/l 0.50 1.0 09/29/05 10:09 PPM 630-20-6
1,1,2,2-Tetrachloroethane NO ug/l 0.50 1.0 09/29/05 10:09 PPM 79-34-5
Tetrachloroethene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 127-18-4
Toluene 0.68 ug/l 0.50 1.0 09/29/05 10:09 PPM 108-88-3
1,2,3-Trichlorobenzene NO ug/l 2.0 1.0 09/29/05 10:09 PPM 87-61-6
1,2,4-Trichlorobenzene NO ug/l 2.0 1.0 09/29/05 10:09 PPM 120-82-1
l,l,l-Trichloroethane NO ug/l 0.50 1.0 09/29/05 10:09 PPM 71-55-6
1,1,2-Trichloroethane NO ug/l 0.50 1.0 09/29/05 10:09 PPM 79-00-5
Trichloroethene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 79-01-6
Trichlorofluoromethane NO ug/l 0.50 1.0 09/29/05 10:09 PPM 75-69-4
l,2,3-Trichloropropane NO ug/l 0.50 1.0 09/29/05 10:09 PPM 96-18-4
1,2,4-Trimethylbenzene 0.82 ug/l 0.50 1.0 09/29/05 10:09 PPM 95-63-6
1,3,5-Trimethylbenzene NO ug/l 0.50 1.0 09/29/05 10:09 PPM 108-67-8
Vinyl chloride NO ug/l 0.50 1.0 09/29/05 10:09 PPM 75-01-4
m&p-Xylene 1.9 ug/l 0.50 1.0 09/29/05 10:09 PPM
o-Xylene 1.6 ug/l 0.50 1.0 09/29/05 10:09 PPM 95-47-6
1-Chloro-3-fluorobenzene (S)104 %1.0 09/29/05 10:09 PPM 625-98-9
Date:10/03/05 Page: 4 of 22
Pace Analytical Services,Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone:828,254,7176
Fax: 828,252.4618
Pace Analytical Services,Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: 704.875,9091www.pacelabS.com
Charlotte Certification IDs
NOWastewater 12
NC Drinking Water 37706
SoC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall notbe reproduced,exceptin lull,
without thewritten consent01PaceAnalyticalServices,Inc,
fflei.C'II~\~~.'i ti
Page:5 of 22
/EPA 6010
0.0050 1.0 10/01/05 19:15 ALV 7440-38-2
0.0050 1.0 10/01/05 19:15 ALV 7440-39-3
0.0010 1.0 10/01/05 19:15 ALV 7440-43-9
0.0020 1.0 10/01/05 19:15 ALV 7440-47-3
0.0050 1.0 10/01/05 19:15 ALV 7439-92-1
0.0050 1.0 10/01/05 19:15 ALV 7782-49-2
0.0020 1.0 10/01/05 19:15 ALV 7440-22-4
09/30/05 01:30
0.00020 1.0 09/30/05 11:00 EWS 7439-97-6
Units Report Limit __m:______!lAn~al:.;Yuz0.5e;l;!d_---!iB!J(yC,.,A...,S.____.N,_"ow.__ ~ RegLmt
Project Sample Number: 92103894-003
Matrix: Water
Method: EPA 7470
NO mg/l
EPA 3010
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/lNO
09/30/05 01:30
Prep/Method:
NO
0.15
NO
NO
NO
0.0052
Results
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
Dat.:10/03/05
Mercury, Dissolved by CVAAS
Mercury, Dissolved
Metals
Dissolved Metals, Trace ICP
Arsenic, Dissolved
Barium, Dissolved
Cadmium, Dissolved
Chromium, Dissolved
Lead, Dissolved
Selenium, Dissolved
Silver, Dissolved
Date Digested
Parameters
Date Collected: 09/21/05 17:00
Date Received: 09/23/05 15:45
Lab Sample No: 926136318
Client Sample ID: B-2 DISSOLVED
Lab Project Number: 92103894
Client Project 1D: West Morehead/6228-05-3103
Pace Analytical ServlcBs, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
aceAnalyticar"
WI\IW.paC&labs.com
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP EB7627
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, exceptin full,
wrthout the written consent of PaceAnalyticalServices, Inc,
.~;-;,
Page: 6 of 22
0.00020 1.0 09/30/05 11:00 EWS 7439-97-6
Method: EPA 7470
ND mg/l
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP EB764B
Date: 10/03/05
Mercury, Dissolved by CVAAS
Mercury, Dissolved
Metals
Dissolved Metals, Trace ICP
Arsenic, Dissolved
Barium, Dissolved
Cadmium, Dissolved
Chromium, Dissolved
Lead, Dissolved
Selenium, Dissolved
Silver, Dissolved
Date Digested
Parameters
Lab Sample No: 926136326
Client Sample ID: B-7 DISSOLVED
Lab Project Number: 92103894
Client Project ID:West Morehead/6228-05-3103
Project Sample Number: 92103894-004 Date Collected:09/23/05 14:30
Matrix:Water Date Received:09/23/05 15:45
Results Units Report Limit .J2L Analyzed By CAS No. Oual RegLmt
Prep/Method: EPA 3010 /EPA 6010
ND mg/1 0.0050 1.0 10/01/05 19:19 ALV 7440-38-2
0.083 mg/1 0.0050 1.0 10/01/05 19:19 ALV 7440-39-3
ND mg/l 0.0010 1.0 10/01/05 19:19 ALV 7440-43-9
ND mg/1 0.0020 1.0 10/01/05 19:19 ALV 7440-47-3
ND mg/l 0.0050 1.0 10/01/05 19:19 ALV 7439-92-1
ND mg/l 0.0050 1.0 10/01/05 19:19 ALV 7782-49-2
ND mg/l 0.0020 1.0 10/01/05 19:19 ALV 7440-22-4
09/30/05 01:30 09/30/05 01:30
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone:[phone]
Fax: 828.252,4618
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
see Analytical'"
www.pacetabs.com
Charlotte Certification IDs
NOWastewater 12
NC Drinking Water 37706
SoC 99006
FL NELAP E87627
Asheville Certification IDs
NCWastewater 40
NODrinking Water 37712
SC Environmental 99030
FL NELAP E87648
Page:7 of 22
Date: 10/03/05
NO Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
(S) Surrogate
2-Ch10roethyl vinyl ether has been shown to degrade in the presence of acid.
Depending on the moisture content the PRLs can be elevated for all soil samples reported on a dry weight basis.
All pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate
hold time.
Method 9071B modified to use ASE.
Dilution factor shown represents the factor applied to the reported result and reporting limit due to changes
in sample preparation, dilution of the extract, or moisture content
PARAMETER FOOTNOTES
Lab Project Number: 92103894
Client Project ID: West Morehead!6228-0S-3103
www.pacelabs.com
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax:[phone]
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshallnotbereproduced,exceptin full,
wtthoutthewritten consentof PaceAnalyticalServices,Inc.~tti~~_
.~~~
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
METHOD BLANK: 926153487
Associated Lab Samples: 926136292 926136300
Blank Reporting
Parame!;~r Units Result Lim!t Footnotes
Benzene ug/l NO 0.50
Bromobenzene ug/l NO 0.50
Bromochloromethane ug/l NO 0.50
Bromodichloromethane ug/l NO 0.50
Bromoform ug/l NO 0.50
Bromomethane ug/l NO 0.50
n-Butylbenzene ug/l NO 0.50
sec-Butylbenzene ug/l NO 0.50
tert-Butylbenzene ug/l NO 0.50
Carbon tetrachloride ug/l NO 0.50
Chlorobenzene ug/l NO 0.50
Chloroethane ug/l NO 0.50
Chloroform ug/l NO 0.50
Chloromethane ug/l NO 0.50
2-Chlorotoluene ug/l NO 0.50
4-Chlorotoluene ug/l NO 0.50
1,2-Dibromo-3-chloropropane ug/l NO 2.0
Dibromochloromethane ug/l NO 0.50
1,2-Dibromoethane (EDB)ug/l NO 0.50
Dibromomethane ug/l NO 0.50
1,2-Dichlorobenzene ug/l NO 1.0
1,3-Dichlorobenzene ug/l NO 1.0
1,4-Dichlorobenzene ug/l NO 1.0
Dichlorodif1uoromethane ug/l NO 0.50
1,1-Dichloroethane ug/l NO 0.50
1,2-Dichloroethane ug/l NO 0.50
1,1-Dichloroethene ug/l NO 0.50
cis-1,2-Dichloroethene ug/l NO 0.50
trans-1,2-Dichloroethene ug/l NO 0.50
1,2-Dichloropropane ug/l NO 0.50
1,3-Dichloropropane ug/l NO 0.50
Date:10/03/05 Page:8 of 22
Analysis Method: SM 6230D
Analysis Description: GC VOCs in Water
926136300926136292
QC Batch: 138596
QC Batch Method: SM 6230D
Associated Lab S~ple8:
Lab Project Number: 92103894
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone:[phone]
Fax:[phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax:[phone]www.pacelabs.com
Charlotte Certification IDs
NGWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of PaceAnalytical Services, Inc.
,.:tcif:!·_
i'lllelaO;
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Page: 9 of 22Date: 10/03/05
METHOD BLANK: 926153487
Associated Lab Samples:926136292 926136300
Blank Reporting
P~rameter .Units Result Limit Footnotes
2,2-Dich1oropropane ug/1 NO 0.50
1,1-Dichloropropene ug/l NO 0.50
cis-1,3-Dich1oropropene ug/1 NO 0.50
trans-1,3-Dich1oropropene ug/1 NO 0.50
Diisopropy1 ether ug/1 NO 0.50
Ethylbenzene ug/1 NO 0.50
Hexach1oro-1,3-butadiene ug/l NO 2.0
Isopropy1benzene (Cumene)ug/1 NO 0.50
p-Isopropy1toluene ug/1 NO 0.50
Methylene chloride ug/1 NO 2.0
Methyl-tert-buty1 ether ug/1 NO 0.50
Naphthalene ug/1 NO 2.0
n-Propylbenzene ug/l NO 0.50
Styrene ug/l NO 0.50
1,1,1,2-Tetrach1oroethane ug/1 NO 0.50
1,1,2,2-Tetrachloroethane ug/l NO 0.50
Tetrachloroethene ug/1 NO 0.50
Toluene ug/1 NO 0.50
1,2,3-Trichlorobenzene ug/l NO 2.0
1,2,4-Trichlorobenzene ug/l NO 2.0
1,1,1-Trich1oroethane ug/l NO 0.50
1,1,2-Trichloroethane ug/l NO 0.50
Trichloroethene ug/l NO 0.50
Trichlorof1uoromethane ug/l NO 0.50
1,2,3-Trich1oropropane ug/l NO 0.50
1,2,4-Trimethy1benzene ug/l NO 0.50
1,3,S-Trimethy1benzene ug/l NO 0.50
Vinyl chloride ug/l NO 0.50
m&p-Xylene ug/l NO 0.50
o-Xylene ug/l NO 0.50
1-Chloro-3-f1uorobenzene (S)%102
Lab Project Number: 92103894
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: 704,875.9092
Fax: [phone]
ace AnaJytica/[~
W1'1w.pa~8bs.com
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,exceptinfull.
without the written consentof PaceAnalyticalServices,Inc.
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
QUALITY CONTROL DATA
Lab Project Number: 92103894
Client Project ID: West Morehead/6228-05-3103
LABORATORY CONTROL SAMPLE &LCSO: 926153495 926153503
Spike LCS LCSO LCS LCSD
Pa:r;:emeter Units Conc.Result Result %Rec %Rec RPD Footnotes
Benzene ug/l 20.00 21.10 21.25 105 106 1
Bromobenzene ug/l 20.00 22.45 20.63 112 103 8
Bromochloromethane ug/l 20.00 22.63 23.03 113 115 2
Bromodichloromethane ug/l 20.00 22.02 22.13 110 111 1
Bromoform ug/l 20.00 21.99 21.79 110 109 1
Bromomethane ug/l 20.00 22.38 22.55 112 113 1
n-Butylbenzene ug/l 20.00 20.38 20.45 102 102 0
sec-Butylbenzene ug/l 20.00 21.00 21.12 105 106 1
tert-Butylbenzene ug/l 20.00 19.72 19.85 99 99 1
Carbon tetrachloride ug/l 20.00 20.66 15.50 103 78 29
Ch1orobenzene ug/1 20.00 22.84 22.43 114 112 2
Chloroethane ug/l 20.00 21.74 21.45 109 107 1
Chloroform ug/l 20.00 18.80 17.61 94 88 7
Chloromethane ug/l 20.00 21.54 21.60 108 108 0
2-Chlorotoluene ug/l 20.00 20.28 20.44 101 102 1
4-Chloroto1uene ug/l 20.00 22.09 22.27 110 III 1
l,2-Dibromo-3-chloropropane ug/l 20.00 21.98 21.93 110 110 0
Dibromoch1oromethane ug/1 20.00 21.75 22.90 109 115 5
1,2-Dibromoethane (EDB)ug/l 20.00 24.65 24.28 123 121 1
Dibromomethane ug/l 20.00 21.89 20.77 109 104 5
l,2-Dich1orobenzene ug/l 20.00 21.94 22.35 110 112 2
1,3-Dich1orobenzene ug/l 20.00 23.77 21.77 119 109 9
1,4-Dich1orobenzene ug/l 20.00 22.80 22.34 114 112 2
Dichlorodif1uoromethane ug/l 20.00 20.17 19.36 101 97 4
1,1-Dichloroethane ug/l 20.00 24.81 22.74 124 114 9
1,2-Dichloroethane ug/l 20.00 22.52 21.89 113 109 3
1,1-Dich1oroethene ug/l 20.00 21.95 20.96 110 105 5
cis-1,2-Dichloroethene ug/l 20.00 23.28 21.48 116 107 8
trans-1,2-Dich1oroethene ug/l 20.00 22.30 21.01 111 105 6
1,2-0ichloropropane ug/l 20.00 22.34 21.24 112 106 5
1,3-Dichloropropane ug/l 20.00 23.01 24.80 115 124 7
2,2-0ichloropropane ug/l 20.00 24.65 23.54 123 118 5
1,1-Dichloropropene ug/l 20.00 23.18 23.32 116 117 1
cis-l,3-Dichloropropene ug/l 20.00 20.47 20.12 102 101 2
trans-1,3-Dichloropropene ug/l 20.00 23.39 24.86 117 124 6
Diisopropyl ether ug/l 20.00 20.37 20.57 102 103 1
Ethylbenzene ug/l 20.00 21.74 21.89 109 109 1
Date: 10/03/05 Page: 10 of 22
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone:[phone]
Fax: 828,252.4618
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite tOO
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
'ace Ana/ytica/'M
www.pacelabs.com
Charlotte Certification IDs
NOWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of PaceAnalytical Services, Inc.
.fj~"~lff{~~
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
926126624 DUP
Pgrall\e·t~r Units Result Result RPD Footnotes
Benzene ug/1 2400 2300 1
Bromobenzene ug/l NO NO NC
Bromochloromethane ug/l NO NO NC
Bromodichloromethane ug/l NO NO NC
Bromoform ug/l NO NO NC
Bromomethane ug/l NO NO NC
Date:10/03/05 Page:11 of 22
QUALITY CONTROL DATA
Lab Project Number:92103894
Client Project ID: West Morehead/6228-05-3103
LABORATORY CONTROL SAMPLE & LCSD: 926153495 926153503
Spike LCS LCSD LCS LCSD
Parameter Units Conc.Result Result %Rec %Rec RPD Footnotes
Hexach1oro-1,3-butadiene ug/1 20.00 22.08 20.87 110 104 6
Isopropylbenzene (Cumene) ug/l 20.00 20.81 20.97 104 105 1
p-Isopropyltoluene ug/l 20.00 21.15 21.26 106 106 1
Methylene chloride ug/l 20.00 22.81 21.93 114 110 4
Methyl-tert-butyl ether ug/l 20.00 20.60 20.61 103 103 0
Naphthalene ug/1 20.00 20.68 21.14 103 106 2
n-Propy1benzene ug/l 20.00 20.88 21.00 104 105 1
Styrene ug/l 20.00 19.83 19.54 99 98 1
1,1,1,2-Tetrachloroethane ug/l 20.00 22.93 24.09 115 120 5
1,1,2,2-Tetrach1oroethane ug/1 20.00 20.12 20.07 101 100 0
Tetrachloroethene ug/l 20.00 22.96 24.71 115 124 7
Toluene ug/l 20.00 21.02 21.26 105 106 1
1,2,3-Trich1orobenzene ug/l 20.00 23.50 22.76 117 114 3
1,2,4-Trichlorobenzene ug/l 20.00 21.09 21.73 105 109 3
1,1,1-Trichloroethane ug/l 20.00 21.49 19.77 107 99 8
1,1,2-Trichloroethane ug/l 20.00 22.24 24.71 111 124 11
Trichloroethene ug/l 20.00 21.22 21.46 106 107 1
Trichlorofluoromethane ug/l 20.00 23.72 21.60 119 108 9
1,2,3-Trichloropropane ug/1 20.00 23.31 22.23 117 111 5
1,2,4-Trimethylbenzene ug/l 20.00 21.01 21.20 105 106 1
1,3,5-Trimethy1benzene ug/1 20.00 21.20 21.32 106 107 1
Vinyl chloride ug/1 20.00 20.87 19.98 104 100 4
m&p-Xylene ug/l 40.00 42.90 43.25 107 108 1
o-Xylene ug/l 20.00 20.55 21.41 103 107 4
1-Ch1oro-3-fluorobenzene (S)108 105
SAMPLE DUPLICATE: 926153511
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone:[phone]
Fax:[phone]
Pace Analytical Services,Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]www.pace/abs.com
Charlotte Certification IDs
NOWastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
withoulthe written consent of PaceAnalytical Services, Inc.
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
SAMPLE DUPLICATE:926153511
926126624 DUP
~ari!.!!leter Units Result Result RPD Footnotes
n-Butylbenzene ug/l NO NO NC
sec-Butylbenzene ug/l NO NO NC
tert-Butylbenzene ug/1 NO NO NC
Carbon tetracbloride ug/l NO NO NC
Cblorobenzene ug/l NO NO NC
Chloroethane ug/1 NO NO NC
Cbloroform ug/l NO NO NC
Chlorometbane ug/l NO NO NC
2-Chlorotoluene ug/l NO NO NC
4-Chlorotoluene ug/l NO NO NC
l,2-Dibromo-3-chloropropane ug/l NO NO NC
Dibromochloromethane ug/l NO NO NC
1,2-Dibromoethane (EDB)ug/l NO NO NC
Dibromomethane ug/l NO NO NC
1,2-Dich1orobenzene ug/l NO NO NC
1,3-Dichlorobenzene ug/l NO NO NC
1,4-Dichlorobenzene ug/l NO NO NC
Dichlorodifluoromethane ug/l NO NO NC 1
1,1-Dich1oroethane ug/l NO NO NC
1,2-Dichloroethane ug/l NO NO NC
1,1-Dichloroethene ug/l NO NO NC
cis-l,2-Dicbloroethene ug/l NO NO NC
trans-1,2-Dichloroethene ug/l NO NO NC
1,2-Dicbloropropane ug/l NO NO NC
1,3-Dichloropropane ug/l NO NO NC
2,2-Dichloropropane ug/l NO NO NC
1,1-Dichloropropene ug/l NO NO NC
cis-1,3-Dichloropropene ug/l NO NO NC
trans-1,3-Dich1oropropene ug/l NO NO NC
Diisopropyl ether ug/l NO NO NC
Ethylbenzene ug/l 970.0 950.0 2
Hexachloro-1,3-butadiene ug/l NO NO NC
Isopropylbenzene (Cumene) ug/l NO NO NC
p-Isopropyltoluene ug/l NO NO NC
Methylene cbloride ug/l NO NO NC
Methyl-tert-butyl ether ug/l NO NO NC
Naphthalene ug/l 440.0 420.0 6
Date: 10/03/05 Page: 12 of 22
Lab Project Number: 92103894
Client Project ID: West Morebead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone:[phone]
Fax: [phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]www.pacelabs.com
Charlotte Certification IDs
NOWastewater 12
NCDrinking Water 37706
SC 99006
FLNELAP E87627
Asheville Certification IDs
NCWastewater 40
NCDrinking Water 37712
SCEnvironmental 99030
FL NELAP E87648
Page:l3 of 22Date:lO/03/05
SAMPLE DUPLICATE: 926153511
926126624 DUP
Pi!ram~ter Units Result Result RPD Footnotes
n-Propylbenzene ug/1 ND ND NC
Styrene ug/l ND ND NC
1,l,l,2-Tetrachloroethane ug/l ND ND NC
1,l,2,2-Tetrachloroethane ug/l ND ND NC
Tetrachloroethene ug/l ND ND NC
Toluene ug/l 5800 5800 1
1,2,3-Trichlorobenzene ug/l ND ND NC
1,2,4-Trichlorobenzene ug/1 ND ND NC
1,1,1-Trichloroethane ug/l ND ND NC
1,1,2-Trich1oroethane ug/l ND ND NC
Trichloroethene ug/l ND ND NC
Trichlorofluoromethane ug/l ND ND NC
1,2,3-Trichloropropane ug/l ND ND NC
1,2,4-Trimethylbenzene ug/l 870.0 850.0 2
1,3,5-Trimethylbenzene ug/l 180.0 170.0 5
Vinyl chloride ug/1 ND ND NC
m&:p-Xylene ug/l 3300 3300 1
o-Xylene ug/l 1400 1400 1
1-Chloro-3-fluorobenzene (S)%103 88
Lab Project Number: 92103894
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28018
Phone: [phone]
Fax: [phone]
'ace Analytical'w
www.pacelabs.com
Charlotte Certification IDs
NGWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshallnot bereproduced.exceptinfull,
w~houtthewritten consentof PaceAnalyticalServices.Inc.
~ H.[.r:'~.~6:c ~::.:;
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Page: 14 of 22Date: 10/03/05
Footnotes
2,2
%Rec %Rec RPD
56 62 9
926103698
ResultUnitsParameter
MSDMSMSD
Result
0.0015
MS
Result
0.0014
Spike
Cone.
0.0025omg/1Mercury
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 926156340 926156357
mg/lMercury
Cone. Result %Rec Footnotes
0.0025 0.0022 88
Units
LCSLCSSpike
LABORATORY CONTROL SAMPLE: 926154246
METHOD BLANK:926154238
Associated Lab Samples: 926136292 926136300
Blank Reporting
Parameter Units Result Limit Footnotes
Mercury mg/1 NO 0.0002
Analysis Method: EPA 7470
Analysis Description: Mercury, CVAAS, in Water
926136300926136292
QC Batch: 138610
QC Batch Method: EPA 7470
Associated Lab Samples:
Lab Project Number: 92103894
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]wl'lw.pacelabs.com
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshallnot bereproduced,exceptin full.
without the written consentof PaceAnalyticalServices,Inc.
..~;-~~.....lZ:]-O~~~(JJtJtILJ.
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
Fl NELAP E87648
Page: 15 of 22Date: 10/03/05
Footnotes%Rec %Rec RPD
86 89 3
926103557
ResultUnitsParameter
MSDMSMSD
Result
0.0025
MS
Result
0.0024
Spike
~M..,__
0.00250.00023mg/lMercury, Dissolved
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 926161761 926161779
mg/lMercury, Dissolved
LCS
%Rec Footnotes
92
LCS
Result
0.0023
Spike
Conc.
0.0025
UnitsParameter
LABORATORY CONTROL SAMPLE: 926161753
METHOD BLANK:926161746
Associated Lab Samples: 926136318 926136326
Blank Reporting
Psr.rameter Units Result Limit Footnotes
Mercury, Dissolved mg/l NO 0.0002
Analysis Method: EPA 7470
Analysis Description: Mercury, Dissolved by CVAAS
926136326926136318
QC Batch: 138756
QC Batch Method: EPA 7470
Associated Lab Samples:
Lab Project Number: 92103894
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone:[phone]
Fax: [phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]Wlyw.pacelabS.rom
Charlotte Certification IDS
NOWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced, except in full,
without the written consentof PaceAnalytical SelVlces, Inc.«'~
ff~ileraQ\
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E67646
926132101 Spike MS MSD MS MSD
P§.!:§!!I&ter Units Result Conc. Result Result %Rec %Rec RPD Footnotes
Arsenic mg/l 0.00015 0.5000 0.4720 0.3090 94 62 42 2.3
Barium mg/l 0.06970 0.5000 0.5420 0.3790 94 62 35 2.3
Cadmium mg/l 0 0.5000 0.4670 0.3020 93 60 43 2.3
Chromium mg/l 0.00408 0.5000 0.4770 0.3110 95 61 42 2.3
Lead mg/l 0.01790 0.5000 0.4940 0.3250 95 61 41 2.3
Date: lO/03/0S Page: 16 of 22
MATRIX SPIKE' MATRIX SPIKE DUPLICATE: 926145129 926145137
Spike LCS LCS
Parameter Units Cone. Result %Rec Footnotes
Arsenic mg/l 0.5000 0.4950 99
Barium mg/l 0.5000 0.5010 100
Cadmium mg/l 0.5000 0.4940 99
Chromium mg/l 0.5000 0.5020 100
Lead mg/l 0.5000 0.4990 100
Selenium mg/l 0.5000 0.4930 99
Silver mg/l 0.5000 0.5010 100
LABORATORY CONTROL SAMPLE: 926145111
Blank Reporting
P~l!.!l!!iltgli:Units Result Limit Footnotes
Arsenic mg/l ND 0.0050
Barium mg/l ND 0.0050
Cadmium mg/l ND 0.0010
Chromium mg/1 ND 0.0020
Lead mg/l ND 0.0050
Selenium mg/l ND 0.0050
Silver mg/l ND 0.0020
926136300
METHOD BLANK: 926145103
Associated Lab Samples:
926136300
Analysis Method: EPA 6010
Analysis Description: Metals by Trace ICP
QC Batch: 138419
QC Batch Method: EPA 3010
Associated Lab Samples:
Lab Project Number: 92103894
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
PaceAnalytical ServicBs. Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services. Inc.
9800 Kincey Avenue,Suite 100
Huntersville. NC28078
Phone: [phone]
Fax: [phone]www.pacelabs.com
CharlotteCertificationIDs
NOWastewater 12
NC DrinkingWater 37706
SC 99006
FLNELAP E87627
AshevilleCertificationIDs
NCWastewater 40
NC DrinkingWater37712
SC Environmental99030
FLNELAP E67646
Page: 17 of 22Date: 10/03/05
Footnotes
2,3
2,3
%Rec %Rec RPD
95 60 43
95 61 44
926132101
ResultUnitsParameter
MSDMSMSD
Result
0.3080
0.3040
MS
Result
0.4790
0.4740
Spike
Cone.
0.5000
0.5000
0.00557
0.00072
mg/l
mg/l
Selenium
Silver
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 926145129 926145137
Lab Project Number: 92103894
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
Pace Analytical Services,Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax: [phone]
Pace Analytical Services,Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
'aceAnalytical'·
www.pacelabs.com
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced,exceptinfull,
without the written consentof PaceAnalyticalServices,Inc.
nera&.\\~;./I~~~
:::'":.!l1li:
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
926134487 Spike MS MSD MS MSD
Param!1;t!1;r Units Result Conc. Result Result %Rec %Rec RPD Footnotes
Arsenic mg/l 0 0.5000 0.4840 0.4850 97 97 0
Barium mg/l 0.09530 0.5000 0.5870 0.5860 98 98 0
Cadmium mg/l 0 0.5000 0.4680 0.4680 94 94 0
Chromium mg/l 0.00044 0.5000 0.4880 0.4850 98 97 1
Lead mg/l 0 0.5000 0.4860 0.4860 97 97 0
Date: 10/03/05 Page: 18 of 22
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 926150087 926150095
LABORATORY CONTROL SAMPLE: 926150079
Spike LCS LCS
Pa.t:'ametg);;Units Conc. Result %Rec Footnotes
Arsenic mg/l 0.5000 0.4710 94
Barium mg/l 0.5000 0.4730 95
Cadmium mg/l 0.5000 0.4690 94
Chromium mg/l 0.5000 0.4820 96
Lead mg/l 0.5000 0.4770 95
Selenium mg/l 0.5000 0.4820 96
Silver mg/l 0.5000 0.4690 94
Blank Reporting
.Parameter Units Resulj;Limit Footnotes
Arsenic mg/l NO 0.0050
Barium mg/l NO 0.0050
Cadmium mg/l NO 0.0010
Chromium mg/l NO 0.0020
Lead mg/l NO 0.0050
Selenium mg/l NO 0.0050
Silver mg/l NO 0.0020
926136292
METHOD BLANK: 926150061
Associated Lab Samples:
926136292
Analysis Method: EPA 6010
Analysis Description: Metals by Trace ICP
QC Batch: 138499
QC Batch Method: EPA 3010
Associated Lab Samples:
Lab Project Number: 92103894
Client Project ID: West Morehead/6228-05-3103
QUALITY CONTROL DATA
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC28078
Phone: [phone]
Fax: [phone]
'aceAna/yticaf'"
www.pacelabs.rom
Charlotte Certification 105
NGWastewater 12
NC Drinking Water 37706
SoC 99006
FLNELAP E87627
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Page: 19 of 22Date: 10/03/0S
926134495 DUP
Parameter units Result Result RPD Footnotes
Arsenic ug/l NO NO NC
Barium ug/l 130.0 129.0 1
Cadmium ug/l NO NO NC
Chromium ug/l 0.6850 1.700 0
Lead ug/1 1.760 0.6440 0
Selenium ug/l 0.00560 3.720 0
Silver ug/1 NO 0.9470 0
SAMPLE DUPLICATE: 926150103
19999
MSDMSMSD
Result
0.4840
0.4930
MS
Result
0.4810
0.4960
Spike
Conc.
0.5000
0.5000
0.00400
o
mg/l
mg/l
Selenium
Silver
Footnotes%Rec %Rec RPD
95 96 1
926134487
ResultUnitsParameter
MATRIX SPIKE &MATRIX SPIKE DUPLICATE:926150087 926150095
Lab Project Number: 92103894
Client Project ID: west Morehead/6228-05-3103
QUALITY CONTROL DATA
PaceAnalytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax:[phone]WWW.1)8c&1!bS.com
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full.
withoutlhe written consent of PaceAnalytical Services, Inc.
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99"030
FL NELAP EB7648
926136318 Spike MS MSD MS MSD
I1:!!.Iame!;;er Units Result Conc. Result Result %Rec %Ree RPD Footnotes
Arsenic,Dissolved mg/1 0.00202 0.5000 0.4900 0.4870 98 97 1
Barium,Dissolved mg/1 0.1470 0.5000 0.6380 0.6350 98 98 0
Cadmium,Dissolved mg/1 0 0.5000 0.4760 0.4750 95 95 0
Chromium, Dissolved mg/1 0.00097 0.5000 0.4890 0.4880 98 97 0
Lead, Dissolved mg/1 0 0.5000 0.4750 0.4730 95 95 0
Date: 10/03/05 Page: 20 of 22
MATRIX SPIKE' MATRIX SPIKE DUPLICATE: 926161480 926161498
Spike LCS LCS
"Parameter Units Conc. Result %Rec Footnotes
Arsenic, Dissolved mg/1 0.5000 0.4930 99
Barium, Dissolved mg/1 0.5000 0.4890 98
Cadmium, Dissolved mg/l 0.5000 0.4850 97
Chromium, Dissolved mg/l 0.5000 0.4960 99
Lead, Dissolved mg/1 0.5000 0.4800 96
Selenium, Dissolved mg/l 0.5000 0.4890 98
Silver, Dissolved mg/l 0.5000 0.4760 95
LABORATORY CONTROL SAMPLE: 926161472
METHOD BLANK: 926161464
Associated Lab Samples: 926136318 926136326
Blank Reporting
Parameter Units Result Limit Footnotes
Arsenic, Dissolved mg/l ND 0.0050
Barium, Dissolved mg/l ND 0.0050
Cadmium, Dissolved mg/1 ND 0.0010
Chromium, Dissolved mg/1 ND 0.0020
Lead, Dissolved mg/l ND 0.0050
Selenium, Dissolved mg/1 ND 0.0050
Silver, Dissolved mg/l ND 0.0020
Analysis Method: EPA 6010
Analysis Description: Dissolved Metals, Trace ICP
926136326926136318
QC Batch: 138749
QC Batch Method: EPA 3010
Associated Lab Samples:
Lab Project Number: 92103894
Client Project ID: West Morehead/6228-0S-3103
QUALITY CONTROL DATA
Pace Analytical Services,Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Pace Analytical Services,Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]www.paOOlabS.com
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
$C 99006
FL NELAP E87627
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced.exceptin full,
without thewritten consentof PaceAnalyticalServices.Inc,
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 9g030
FL NELAP E87648
Page: 21 of 22Date: 10/03/05
926136318 Spike MS MSD MS MSD
~arameter Units Result Cone.Result Result %Ree %Ree RPD Footnotes
Selenium. Dissolved mg/1 0.00520 0.5000 0.4870 0.4860 96 96 0
Silver. Dissolved mg/l 0 0.5000 0.4770 0.4770 95 95 0
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 926161480 926161498
Lab Project Number: 92103894
Client Project ID: West Morehead/6228-0S-3103
QUALITY CONTROL DATA
Pace Analytical Services.Inc.
2225 Riverside Drive
Asheville, NC28804
Phone:[phone]
Fax: [phone]
Pace Analytical Services,Inc,
9800 Kincey Avenue, Suite 100
Huntersville, NC 28018
Phone: [phone]
Fax: [phone]Wl'lw,pacalabs,oom
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87S27
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced.exceptInfull,
w~hout the written consent of PaceAnalyticalServices. Inc.
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Page: 22 of 22Date:10/03/05
[1]
[2]
RPD
(S)
MDL
J
NC
DUP
NO
LCS(D)
MS(D)
Laboratory Control Sample (Duplicate)
Matrix Spike (Duplicate)
Sample Duplicate
Not de-tectedat or above adjusted reporting limit
Not Calculable
Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
Adjusted Method Detection Limit
Relative Percent Difference
Surrogate
Sample was received by the laboratory without acid preservation as recommended by the US EPA.
The spike recovery was outside acceptance limits for the MS and lor MSD due to matrix interference. The LCS
and/or LCSD were within acceptance limits showing that the laboratory is in control and the data is
acceptable.
[3] The calculated RPD was outside QC acceptance limits.
Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate %Rec and RPD values.
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Lab Project Number: 92103894
Client Project ID: West Morehead/6228-05-3103
Pace Analytical Services, Inc.
2225 Riverside Drive
Ash9ViJi9,NC28804
Phone:[phone]
Fax:[phone]
PaceAnalytical Services, Inc.
9800 Kincey Avenue,Suite 100
Huntersville,NC28078
Phone:[phone]
Fax: [phone]
ace AnaJytica/l~
www.pace/8bs.com
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