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HomeMy WebLinkAbout20022_Mt_Hope_II_Remedial_Action_Rpt_20160710 REMEDIAL ACTION PROGRESS REPORT: 2015 ANNUAL GROUNDWATER SAMPLING MOUNT HOPE MACHINERY COMPANY 2000 Donald Ross Road Charlotte, North Carolina IHSB ID No. NONC0002101 July 10, 2015 Prepared for: Xerium 14101 Capital Blvd Youngsville, North Carolina 27596 Attn: Mr. Randy Arnott Prepared by: GTA ASSOCIATES, INC. Geotechnical and Environmental Consultants 710 Peninsula Lane, Suite B Charlotte, North Carolina (704)553-2300 www.gtaeng.com GTA Project No: 150700NC i TABLE OF CONTENTS 1.0 INTRODUCTION............................................................................................................... 1 1.1 Background ........................................................................................................................ 1 2.0 NATURAL ATTENUATION MONITORING ............................................................... 2 2.1 Evaluation of Groundwater Flow ...................................................................................... 3 2.2 Monitoring Well Sampling and Analysis .......................................................................... 3 2.3 Groundwater Analytical Results ........................................................................................ 4 3.0 SUMMARY ......................................................................................................................... 6 GBA Publication – Important Information about Your Geo-environmental Report (3 pages) LIST OF FIGURES Figure 1 - Site Location Map (color) Figure 2 - June 1, 2015 Shallow Potentiometric Map Figure 3 - June 1, 2015 Shallow Bedrock Potentiometric Map LIST OF TABLES Table 1 - Monitoring Well Information Summary Table 2 - Summary of June 2015 Groundwater Analytical Results (color) Table 3 - Summary of Historical Groundwater Analytical Data, 2009 to Present (color) Table 4 - Complete Historical Groundwater Analytical Data, 2009 to Present (color) LIST OF APPENDICES Appendix A – Laboratory Analytical Reports and Chain-of-Custody Records 1 REMEDIAL ACTION PROGRESS REPORT MOUNT HOPE MACHINERY MECKLENBURG COUNTY, NORTH CAROLINA JULY 10, 2015 1.0 INTRODUCTION 1.1 Background In 1989, a remedial investigation was initiated at the Mount Hope facility located at 2000 Donald Ross Road, Charlotte, North Carolina to assess a release of varsol and mineral spirits from a permitted subgrade septic tank system. Aware Environmental, Inc. (AEI) was engaged by the owner to evaluate the issue. This investigation revealed that both soil and groundwater were impacted by the release. The subject property is currently vacant and offered for sale by the owner. Remedial activities were conducted at the site between May 1992 and May 1998 to address the impacted soil and groundwater with regulatory oversight by the North Carolina Department of Environment and Natural Resources (NCDENR) – Groundwater Section. Remedial activities included removal of the septic tank system and surrounding soil excavation, soil vapor extraction (SVE), and shallow groundwater air sparging (AS) in proximity of the source area. Between January 1996 and November 1998, quarterly groundwater sampling was conducted at the site to evaluate groundwater remedial efforts. After Mount Hope conducted the initial soil and groundwater remedial activities, regulatory oversight of the release incident fell under the purview of the NCDENR Inactive Hazardous Sites Branch (IHSB). A more recent remedial investigation conducted in 2009 and 2013 under the IHSB’s Registered Environmental Consultant (REC) Program confirmed the presence of remaining impacted soils above the ISB Preliminary Health-Based Soil Remediation Goals (Health-SRGs) and Protection of Groundwater SRGs (GW-SRGs). In addition, groundwater impacts were detected above the NCAC 15A 2L Groundwater Quality Standards (2L Standards). Mount Hope completed a Remedial Investigation for impacted site soils and submitted a Remedial Investigation Report to the REC Program on August 6, 2010. The Remedial Investigation for Remedial Action Progress Report Mount Hope Machinery Company July 10, 2015 GTA Project No. 150700NC 2 impacted groundwater was completed in 2012 and a follow-up Addendum Remedial Investigation Report was submitted to the REC Program on September 4, 2012. Proposed soil remedial activities were presented in AEI’s Soil Remedial Action Plan dated August 2010. Remedial activities that were conducted included the excavation of approximately 1,105 tons of impacted soils from the former septic tank area and subsequent off-site Landfill disposal. Confirmatory soil analytical data verified that soils were remediated to the cleanup objectives. These soil cleanup activities and confirmatory analytical data are discussed in AEI’s Soil Remediation Completion Report – Former Septic Tank dated November 2010. Proposed groundwater Remedial Activities were presented in AEI’s Groundwater Remedial Action Plan dated June 2014. Natural attenuation was selected as the remedial option for the Mount Hope site. A discussion of the monitoring for natural attenuation is provided below. 2.0 NATURAL ATTENUATION MONITORING With the remediation of soil and shallow groundwater impacting the source area completed, it is anticipated that groundwater concentrations in the deeper aquifer associated with the release at Mount Hope will naturally attenuate with time. Recent groundwater sampling has identified five (5) compounds above 2L Standards, compounds include benzene, cis1,1- dichloroethene (cis-DCE), tetrachloroethene (PCE), trichloroethene (TCE), and vinyl chloride (VC). As discussed in the June 2014 Groundwater Remedial Action Plan (RAP), only cis-DCE can be attributed to releases at the Mount Hope facility. Benzene, PCE, TCE, and VC are considered background compounds originating from upgradient sources and not the responsibility of Mount Hope to remediate. During groundwater remedial action conducted in the 1990s, Mount Hope conducted quarterly groundwater monitoring for three (3) years; therefore, monitoring for natural attenuation began with annual groundwater sampling for the first year after the RAP approval and subsequent years until concentrations of DCA and cis-DCE decrease to below 2L Standards. Remedial Action Progress Report Mount Hope Machinery Company July 10, 2015 GTA Project No. 150700NC 3 The 2015 groundwater monitoring event included measuring water level in site wells, collection for groundwater samples from deeper wells MW-4A, MW-11A, MW-14A, and MW- 15A and shallow wells MW-5, MW-6, and MW-13. Samples were analyzed for volatile organic compounds (VOCs) by United States Environmental Protection Agency (USEPA) Method 8260. 2.1 Evaluation of Groundwater Flow Prior to purging the designated monitoring wells to be sampled, static water levels were measured in all existing monitoring wells. Monitoring well water level measurements are summarized in Table 1. Shallow and bedrock groundwater potentiometric maps have been constructed based on water table elevations calculated from static monitoring well water levels measured on June 1, 2015 (Figures 2 and 3). Shallow groundwater flow is generally to the southeast with an average horizontal gradient of 0.040 feet/foot. The deeper aquifer flow is to the south and southeast at an approximate horizontal gradient of 0.029 feet/foot. The vertical hydraulic gradients were calculated from measurements made on June 1, 2015 for well clusters MW- 4R/MW-4A, MW-14/MW-14A, and MW-16/MW-16A. Vertical gradients are summarized below: Monitoring Well Cluster Gradient (Feet/Foot) Direction MW-4R/MW-4A 0.0335 Downward MW-14/MW-14A 0.0088 Downward MW-16/MW-16A -0.00001 Upward The low vertical head gradient indicated that the groundwater flow is predominately horizontal. 2.2 Monitoring Well Sampling and Analysis On June 1, 2015, groundwater samples were collected for laboratory analysis from designated monitoring wells. Remedial Action Progress Report Mount Hope Machinery Company July 10, 2015 GTA Project No. 150700NC 4 Based upon measured monitoring well water levels, monitoring well depths, and known casing diameters, the number of gallons of standing water in each monitoring well was calculated to determine the required purge volume. Each monitoring well to be sampled was purged of approximately three (3) static monitoring well casing volumes or until the monitoring well was purged of all water. Monitoring well purging was performed using either an electric stainless steel submersible pump (in monitoring wells MW-4A, MW-5, MW-11A, MW-14A, and MW-15A) or dedicated bottom-loading bailers (in monitoring wells MW-6 and MW-13) attached to new nylon cord. Groundwater samples were collected from monitoring wells MW-4A, MW-5, MW-11A, MW-14A, and MW-15A using the submersible pump following each monitoring well evacuation. Groundwater samples were collected from monitoring wells MW-6 and MW-13 using dedicated bailers. Samples were carefully transferred from the sampling equipment into laboratory supplied 40 mL Volatile Organic Analysis (VOA) vials that were immediately placed in an insulated cooler with ice following their collection. Monitoring well development, purging and sampling methods were performed in accordance with the approved Standard Procedures/Technical Methods included in Attachment B of AEI’s June 2014 Groundwater Remedial Action Plan. 2.3 Groundwater Analytical Results GTA contracted Shealy Environmental Services in West Columbia South Carolina to complete the required analysis for the 2015 sampling event. The groundwater samples were placed in clean laboratory-provided containers, placed in a chilled cooler, and couriered to the laboratory under chain of custody documentation to be analyzed for volatile organic compounds (VOCs) by USEPA method 8260. A tabulated summary of the groundwater analytical results for the June 2015 monitoring event is presented in Table 2. Laboratory analytical reports and chain of custody records are included in Attachment A. Historical groundwater analytical results from March 2009 to the present are presented in Table 3. In the June 1, 2015 sampling event, five (5) target compounds were identified in monitoring well samples at concentrations above the North Carolina Department of Environment and Natural Resources (NCDENR) 15A NCAC 2L Groundwater Quality Standards (GQS) or interim standards (2L Standards); compounds included benzene, Cis-DCE, PCE, TCE, and VC. Remedial Action Progress Report Mount Hope Machinery Company July 10, 2015 GTA Project No. 150700NC 5 Analytical results from samples obtained from deeper source area well MW-4A detected concentrations of benzene at 1.40 µg/L, 1,1-DCA at 5.20 µg/L, 1,1-dichloroethene (1,1-DCE) at 2.90 µg/L, cis-DCE at 65.00 µg/L, methyl tert-butyl ether (MTBE) at 1.30 µg/L, PCE at 4.80 µg/L, TCE at 3.00 µg/L, and VC at 1.50 µg/L. Of the VOCs detected, benzene, PCE, TCE, and VC were detected at concentrations exceeding their respective 2L standards of 1.00 µg/L, 0.70 µg/L, 3.00 µg/L, and 0.03 µg/L respectively. Analytical results from samples obtained from downgradient shallow well MW-5 detected concentrations of cis-DCE at 2.30 µg/L and PCE at 1.30 µg/L. Of the VOCs detected PCE was detected at a concentrations exceeding its 2L standard of 0.70 µg/L. Analytical results from samples obtained from downgradient shallow well MW-6 detected a concentration of 1,1-DCA at 0.62 µg/L. The detected concentration of 1,1-DCA is below its 2L Standard of 6.00 µg/L. Analytical results from samples obtained from deeper source area well MW-11A detected concentrations of benzene at 1.30 µg/L, 1,1-DCA at 4.20 µg/L, 1,1-DCE at 2.30 µg/L, cis-DCE at 56.00 µg/L, methyl tert-butyl ether (MTBE) at 1.20 µg/L, methylene chloride at 0.52 µg/L, PCE at 5.60 µg/L, TCE at 4.20 µg/L, and VC at 2.00 µg/L. Of the VOCs detected, benzene, PCE, TCE, and VC were detected at concentrations exceeding their respective 2L standards of 1.00 µg/L, 0.70 µg/L, 3.00 µg/L, and 0.03 µg/L, respectively. Analytical results from samples obtained from shallow off-site well MW-13 detected concentrations of benzene at 0.67 µg/L, 1,1-DCA at 5.10 µg/L, 1,1-DCE at 3.40 µg/L, cis-DCE at 76.00 µg/L, PCE at 4.8 µg/L, TCE at 2.2 µg/L, trichlorofluoromethane (Freon-11) at 0.64 µg/L and VC at 0.81 µg/L. Of the VOCs detected, cis-DCE, PCE, and VC were detected at concentrations exceeding their respective 2L standards of 70.00 µg/L, 0.70 µg/L, and 0.03 µg/L, respectively. Remedial Action Progress Report Mount Hope Machinery Company July 10, 2015 GTA Project No. 150700NC 6 Analytical results from samples obtained from deeper off-site well MW-14A detected concentrations of benzene at 1.20 µg/L, 1,1-DCA at 5.50 µg/L, 1,1-DCE at 3.30 µg/L, cis-DCE at 68.00 µg/L, methyl tert-butyl ether (MTBE) at 0.62 µg/L, methylene chloride at 0.52 µg/L, PCE at 5.10 µg/L, TCE at 3.10 µg/L, Freon-11 at 0.58, and VC at 1.50 µg/L. Of the VOCs detected, benzene, PCE, TCE and VC were detected at concentrations exceeding their respective 2L standards of 1.00 µg/L, 0.70 µg/L, 3.00 µg/L, and 0.03 µg/L respectively. Analytical results from samples obtained from deeper off-site well MW-15 detected concentrations of 1,1-DCA at 2.60 µg/L, 1,1-DCE at 0.83 µg/L, cis-DCE at 30.00 µg/L, PCE at 1.10 µg/L, toluene at 0.90 µg/L, and TCE at 0.65 µg/L. Of the VOCs detected PCE was detected at a concentrations exceeding its 2L standard of 0.70 µg/L. 3.0 SUMMARY A comparison of the 2015 annual groundwater monitoring results with historical data for the same monitoring wells shows that benzene continues to be detected in the deeper monitoring wells above the 2L Standards while the shallow wells remain below the 2L Standard. This data continues to suggest that benzene impacts may have originated from an up gradient off-site source. With the exception of MW-13, cis-DCE concentrations have fallen below the 2L Standard of 70 µg/L. MW-13, which is located south east of the site (off-site) is suspected to be impacted by off- site sources flowing toward the subject site. PCE and TCE concentrations detected in samples obtained during this sampling event are also believed to be influenced by off-site sources. The VC detected is believed to be the result of degradation of the compounds identified during the sampling event and provide support that on-going natural attenuation is occurring at the site. Mount Hope will conduct the 2016 annual groundwater monitoring event in the 3rd quarter of 2016. ***** END OF REPORT ***** Figure 1. Site Location Map Figure 2. June 1, 2015 Shallow Potentiometric Map Figure 3. June 1, 2015 Shallow Bedrock Potentiometric Map TABLES Ta b l e  1 Mo n i t o r i n g  We l l  In f o r m a t i o n Mo u n t  Ho p e  Ma c h i n e r y  Co m p a n y Ch a r l o t t e ,  No r t h  Ca r o l i n a  2015  Annual  Groundwater  Sampling GTA  Project  No. 150700NC Page  1  of  1 We l l I D We l l D e p t h (f e e t ) Ele v a t i o n o f G r a d e (M S L - f e e t ) To p o f C a s i n g El e v a t i o n (M S L - f e e t ) Sc r e e n I n t e r v a l Be l o w G r a d e (f e e t ) Sc r e e n I n t e r v a l El e v a t i o n (M S L - f e e t ) We l l C o n s t r u c t i o n Da t e Wa t e r L e v e l f r o m TO C (f e e t ) Water Level Elevation (MSL-feet) MW - 1 8/ 1 / 1 9 9 1 MW - 2 3 7 . 0 0 7 2 9 . 2 0 7 2 8 . 9 0 2 2 - 3 7 7 0 7 . 2 - 6 9 2 . 2 8 / 1 / 1 9 9 1 3 0 . 2 0 6 9 8 . 7 0 MW - 3 3 5 . 0 0 7 2 7 . 6 0 7 2 7 . 2 2 2 0 - 3 5 7 0 7 . 6 - 6 9 2 . 6 8 / 1 / 1 9 9 1 3 0 . 6 0 6 9 6 . 6 2 MW - 4 3 5 . 0 0 7 2 8 . 8 0 7 2 8 . 0 1 2 0 - 3 5 7 0 8 . 8 - 6 9 3 . 8 8 / 1 / 1 9 9 1 MW - 4 R * 4 5 . 0 0 7 2 8 . 8 0 7 2 8 . 2 4 3 0 - 4 5 6 9 8 . 8 - 6 3 8 . 8 5 / 2 7 / 2 0 1 1 3 1 . 9 1 6 9 6 . 3 3 MW - 4 A 1 2 8 . 0 0 7 2 8 . 9 0 7 2 8 . 1 7 1 1 8 - 1 2 8 6 1 0 . 9 - 6 0 0 . 9 3 / 1 3 / 1 9 9 2 3 4 . 6 4 6 9 3 . 5 3 MW - 5 3 8 . 0 0 7 2 8 . 9 0 7 2 8 . 4 1 2 8 - 3 8 7 0 0 . 9 - 6 9 0 . 9 3 / 1 6 / 1 9 9 2 3 3 . 1 8 6 9 5 . 2 3 MW - 6 * * 1 4 . 0 0 6 9 6 . 6 0 6 9 8 . 2 5 1 - 1 4 6 9 5 . 6 - 6 8 1 . 6 3 / 1 7 / 1 9 9 2 4 . 4 0 6 9 3 . 8 5 MW - 7 1 8 . 0 0 7 0 5 . 5 0 7 0 7 . 1 8 8 - 1 8 6 9 7 . 6 - 6 8 7 . 5 3 / 1 7 / 1 9 9 2 1 1 . 4 2 6 9 5 . 7 6 MW - 8 3 8 . 0 0 7 3 1 . 0 0 7 3 0 . 4 3 2 8 - 3 8 7 0 3 - 6 9 3 3 / 1 3 / 1 9 9 2 3 2 . 6 1 6 9 7 . 8 2 MW - 9 3 6 . 0 0 7 3 1 . 1 0 7 3 0 . 8 4 2 6 - 3 6 7 0 5 . 1 - 6 9 5 . 1 5 / 1 8 / 1 9 9 4 3 5 . 2 3 6 9 5 . 6 1 MW - 1 0 A 1 2 2 . 0 0 7 2 9 . 2 0 7 3 0 . 4 4 1 1 2 - 1 2 2 6 1 7 . 2 - 6 0 7 . 2 1 0 / 1 3 / 1 9 9 8 3 0 . 6 0 6 9 9 . 8 4 MW - 1 1 A 9 5 . 0 0 7 0 3 . 0 0 7 0 5 . 5 7 8 5 - 9 5 6 1 8 - 6 0 8 3 / 1 0 / 2 0 1 0 1 0 . 5 0 6 9 5 . 0 7 MW - 1 2 A 9 2 . 0 0 7 3 4 . 4 0 7 3 4 . 9 5 9 0 - 9 2 6 4 4 . 4 - 6 4 2 . 2 6 / 1 0 / 2 0 1 0 3 4 . 1 8 7 0 0 . 7 7 MW - 1 3 1 8 . 0 0 6 9 5 . 0 0 6 9 6 . 5 7 8 - 1 8 6 8 7 - 6 7 7 2 / 1 3 / 2 0 1 2 6 . 2 7 6 9 0 . 3 0 MW - 1 4 1 8 . 0 0 6 9 6 . 6 0 6 9 9 . 3 8 8 - 1 8 6 8 8 . 6 - 6 7 8 . 6 2 / 6 / 2 0 1 2 6 . 9 8 6 9 2 . 4 0 MW - 1 4 A 8 4 . 0 0 6 9 6 . 6 0 6 9 8 . 8 6 7 4 - 8 4 6 2 2 . 6 - 6 1 2 . 6 2 / 1 5 / 2 0 1 2 7 . 0 4 6 9 1 . 8 2 MW - 1 5 A 8 6 . 0 0 6 9 1 . 6 0 6 9 4 . 4 7 6 6 - 8 6 6 2 5 . 6 - 6 0 5 . 6 4 / 5 / 2 0 1 2 5 . 2 6 6 8 9 . 2 1 MW - 1 6 1 3 . 0 0 6 9 4 . 1 0 6 9 5 . 9 6 8 - 1 3 6 8 6 . 1 - 6 8 1 . 6 8 / 1 / 2 0 1 2 8 . 1 9 6 8 7 . 7 7 MW - 1 6 A 9 3 . 0 0 6 9 8 . 1 0 7 0 0 . 5 7 7 3 - 9 3 6 2 5 . 1 - 6 0 5 . 1 7 / 3 1 / 2 0 1 2 1 2 . 7 0 6 8 7 . 8 7 MW - 1 7 A 9 5 . 0 0 7 0 9 . 2 0 7 1 1 . 6 9 8 0 - 9 5 6 2 9 . 2 - 6 1 4 . 2 8 / 2 / 2 0 1 2 1 5 . 9 5 6 9 5 . 7 4 AL - 1 1 1 . 5 0 6 9 7 . 7 0 7 0 0 . 4 8 6 . 5 - 1 1 . 5 6 9 1 . 2 - 6 8 6 . 2 5 / 2 4 / 1 9 9 4 7 . 9 1 6 9 2 . 5 7 AL - 2 3 6 . 0 0 7 2 4 . 4 0 7 2 3 . 9 0 2 6 - 3 6 6 9 8 . 4 - 6 8 8 . 4 5 / 2 4 / 1 9 9 4 2 9 . 7 5 6 9 4 . 1 5 No t e s : All e l e v a t i o n s a r e r e f e r e n c e d t o m e a n s e a l e v e l ( M S L ) Wa t e r  le v e l  da t a  wa s  co l l e c t e d  by  GT A  As s o c i a t e s ,  In c .  on  Ju n e  1,  20 1 5 . * ‐   MW ‐4R  is  a  re p l a c e m e n t  mo n i t o r i n g  we l l  fo r  MW ‐4.  Mo n i t o r i n g  we l l  MW ‐4  wa s  ab a n d o n e d  on  Ma y  27 ,  20 1 1 . **  ‐   MW ‐6  to p  of  ca s i n g  ch a n g e d  on  3/ 1 7 / 2 0 1 0 ,  ne w  to p  of  ca s i n g  ele v a t i o n  is  69 8 . 2 5  fe e t  ab o v e  MS L . NM ‐ No t  Me a s u r e d NA  ‐   No t  Av a i l a b l e Ab a n d o n e d W e l l Ab a n d o n e d W e l l Ab a n d o n e d M a y 2 7 , 2 0 1 1 Table 2 Summary of June 2015 Groundwater Analytical Results Mount Hope Machinery Company Charlotte, North Carolina 2015 Annual Groundwater Sampling GTA Project No. 150700NC Page 1 of 1 Monitoring Well ID MW-4A MW-5 MW-6 MW-11A MW-13 MW-14A MW-15A GQS VOCs Acetone <10 <10 <10 <10 <10 <10 <10 6,000 Benzene 1.4 <0.5 <0.5 1.3 0.67 1.20 <0.5 1 Bromodichloromethane <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.6 n-Butylbenzene <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 70 sec-Butylbenzene <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 70 Chlorobenzene <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 50 Chlorodibromomethane <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Not Specified Chloroform <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 70 Chloromethane <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 3 1,2-Dichloroethane <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 20 Dichlorodiflouromethane <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1,000 1,1-Dichloroethane 5.2 <0.5 0.62 4.2 5.1 5.5 2.6 6 1,1-Dichloroethene 2.9 <0.5 <0.5 2.3 3.4 3.3 0.83 7 Cis-1,2-Dichloroethene 65.0 2.3 <0.5 56.0 76.0 68.0 30.0 70 1,2-Dichloropropane <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.6 2-Hexanone <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 40* p-Isopropyltoluene <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 25* Methyl-tert-butyl ether (MTBE)1.30 <0.5 <0.5 1.20 <0.5 0.62 <0.5 20 Mehtylene Chloride <0.5 <0.5 <0.5 0.52 <0.5 0.52 <0.5 5 Napthalene <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 6 Tetrachloroethene 4.8 1.3 <0.5 5.6 4.8 5.1 1.1 0.70 Tetrahydrofuran NA NA NA NA NA NA NA Not Specified Toluene <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.90 600 1,2,4-Trichlorobenzene <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 70 Trichloroethene 3.0 <0.5 <0.5 4.2 2.2 3.1 0.65 3 Trichlorofluoromethane <0.5 <0.5 <0.5 <0.5 0.64 0.58 <0.5 2,000 Vinyl Chloride 1.50 <0.5 <0.5 2.00 0.81 1.50 <0.5 0.03 Notes: Samples collected by GTA Associates, Inc. on June 1, 2015 Results reported in micrograms per liter (µg/L) Only constituents detected above laboratory method detection limits are shown in this table. Volatile Organic Compounds (VOCs) analyzed by United Stated Environmental Protection Agency (USEPA) Method 8260. NCDENR Groundwater Quality Standard (GQS) (15A NCAC 02L .0202) Bold values indicated a constituent detected above laboratory method detection limits Highlighted values indicate a constituent detected above the NCAC GQS. * - Interim Maximum Allowable Concentrations NA - Not analyzed by this method. Table 3 Summary of Historical Groundwater Analytical Data 2009-Present Mount Hope Machinery Company Charlotte, NC GTA Project No. 150700NC Page 1 of 7 Monitoring Well ID MW-4A (2009)MW-4A (2010)MW-4A (2011)MW-4A (2012)MW-4A (2013)MW-4A (2014)MW-4A (2015)GQS VOCs Acetone <25 <10 <50 <10 <6.7 <10 <10 6,000 Benzene 1.30 1.4 <2.0 1.6 1.3 1.4 1.4 1 Bromodichloromethane <1.0 <1.0 <2.0 <0.5 <0.33 <0.5 <0.5 0.6 n-Butylbenzene NA <1.0 <2.0 <0.5 <0.21 <0.5 <0.5 70 sec-Butylbenzene <1.0 <1.0 <2.0 <0.5 <0.07 <0.5 <0.5 70 Chlorobenzene <1.0 <1.0 <2.0 <0.5 <0.33 <0.5 <0.5 50 Chlorodibromomethane <1.0 <1.0 <2.0 <0.5 <0.33 <0.5 <0.5 Not Specified Chloroform <1.0 <1.0 <2.0 <0.5 <0.33 <0.5 <0.5 70 Chloromethane <1.0 <1.0 <2.0 <0.5 <0.33 <0.5 <0.5 3 1,2-Dichloroethane <1.0 <1.0 <2.0 <0.5 <0.33 <0.5 <0.5 20 Dichlorodiflouromethane <1.0 <1.0 <2.0 <0.5 0.20 J <0.5 <0.5 1,000 1,1-Dichloroethane 7.2 8.30 7.48 8.10 6.80 6.10 5.20 6 1,1-Dichloroethene 4.40 4.40 4.04 4.30 3.30 3.20 2.90 7 Cis-1,2-Dichloroethene 88.7 109.0 90.8 99.0 80.0 71.0 65.0 70 1,2-Dichloropropane <1.0 <0.5 <2.0 <0.5 <0.19 <0.5 <0.5 0.6 2-Hexanone <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 40* p-Isopropyltoluene <1.0 <0.5 <2.0 <0.5 <0.07 <0.5 <0.5 25* Methyl-tert-butyl ether (MTBE)<1.0 0.53 <2.0 0.74 0.61 J 0.99 1.30 20 Mehtylene Chloride <2.0 0.58 <10.0 0.62 0.59 J 0.56 <0.5 5 Napthalene <1.0 <0.5 <2.0 <0.5 <0.4 <0.5 <0.5 6 Tetrachloroethene 4.50 5.10 3.78 4.80 4.30 4.50 4.80 0.7 Tetrahydrofuran NA NA NA NA NA NA NA Not Specified Toluene <1.0 <0.5 <2.0 <0.5 <0.33 <0.5 <0.5 600 1,2,4-Trichlorobenzene <1.0 <0.5 <2.0 <0.5 <0.5 <0.5 <0.5 70 Trichloroethene 2.5 2.5 2.2 2.8 2.4 2.6 3.0 3 Trichlorofluoromethane <1.0 <0.5 <2.0 <0.5 0.40 J <.05 <0.5 2,000 Vinyl Chloride 1.9 2.0 <2.0 2.1 2.3 1.6 1.5 0.03 Notes: MW-4A 2009-2015 NCDENR Groundwater Quality Standard (GQS) (15A NCAC 02L .0202) Bold values indicated a constituent detected above laboratory method detection limits Highlighted values indicate a constituent detected above the NCAC GQS. * - Interim Maximum Allowable Concentrations NA - Not analyzed by this method. TICS - Tentatively Identified Compounds Samples collected by on dates indicated in the table Results reported in micrograms per liter (µg/L) Only constituents detected above laboratory method detection limits are shown in this table. g p ( ) y y g y ( ) Method 8260. g p ( ) y y g y (USEPA) Method 8270. Table 3 Summary of Historical Groundwater Analytical Data 2009-Present Mount Hope Machinery Company Charlotte, NC GTA Project No. 150700NC Page 2 of 7 Monitoring Well ID MW-5 (2009)MW-5 (2010)MW-5 (2011)MW-5 (2012)MW-5 (2013)MW-5 (2014)MW-5 (2015)GQS VOCs Acetone <25 <25 <25 <10 <6.7 <10 <10 6,000 Benzene <1.0 <1.0 <1.0 <0.5 <0.13 <0.5 <0.5 1 Bromodichloromethane <1.0 <1.0 <1.0 <0.5 <0.33 <0.5 <0.5 0.6 n-Butylbenzene NA NA <1.0 <0.5 <0.21 <0.5 <0.5 70 sec-Butylbenzene <1.0 <1.0 <1.0 <0.5 <0.07 <0.5 <0.5 70 Chlorobenzene <1.0 <1.0 <1.0 <0.5 <0.33 <0.5 <0.5 50 Chlorodibromomethane <1.0 <1.0 <1.0 <0.5 <0.33 <0.5 <0.5 Not Specified Chloroform <1.0 <1.0 <1.0 <0.5 <0.33 <0.5 <0.5 70 Chloromethane <1.0 <1.0 <1.0 <0.5 <0.33 <0.5 <0.5 3 1,2-Dichloroethane <1.0 <1.0 <1.0 <0.5 <0.33 <0.5 <0.5 20 Dichlorodiflouromethane <1.0 <1.0 <1.0 <0.5 <0.20 <0.5 <0.5 1,000 1,1-Dichloroethane 1.60 1.10 1.57 1.00 0.61J <0.5 <0.5 6 1,1-Dichloroethene <1.0 <1.0 <1.0 <0.5 0.17J <0.5 <0.5 7 Cis-1,2-Dichloroethene 24.4 17.0 22.3 15.0 7.4 2.3 2.3 70 1,2-Dichloropropane <1.0 <1.0 <1.0 <0.5 <0.19 <0.5 <0.5 0.6 2-Hexanone <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 40* p-Isopropyltoluene <1.0 <1.0 <1.0 <0.5 <0.07 <0.5 <0.5 25* Methyl-tert-butyl ether (MTBE)<1.0 <1.0 <1.0 <0.5 <0.40 <0.5 <0.5 20 Mehtylene Chloride <2.0 <2.0 <5.0 <0.5 <0.33 <0.5 <0.5 5 Napthalene <1.0 <1.0 <1.0 <0.5 <0.4 <0.5 <0.5 6 Tetrachloroethene 1.90 1.40 1.53 1.80 1.30 1.30 1.30 0.70 Tetrahydrofuran NA NA NA NA NA NA NA Not Specified Toluene <1.0 <1.0 <1.0 <0.5 <0.33 <0.5 <0.5 600 1,2,4-Trichlorobenzene <1.0 <1.0 <1.0 <0.5 <0.5 <0.5 <0.5 70 Trichloroethene <1.0 <1.0 <1.0 <0.5 0.21J <0.5 <0.5 3 Trichlorofluoromethane <1.0 <1.0 <1.0 <0.5 <0.3 <0.5 <0.5 2,000 Vinyl Chloride <1.0 <1.0 <1.0 <0.5 <0.054 <0.5 <0.5 0.03 Notes: MW-5 2009-2015 TICS - Tentatively Identified Compounds NCDENR Groundwater Quality Standard (GQS) (15A NCAC 02L .0202) Bold values indicated a constituent detected above laboratory method detection limits Highlighted values indicate a constituent detected above the NCAC GQS. * - Interim Maximum Allowable Concentrations NA - Not analyzed by this method. Samples collected by on dates indicated in the table Results reported in micrograms per liter (µg/L) Only constituents detected above laboratory method detection limits are shown in this table. g p ( ) y y g y ( ) Method 8260. g p ( ) y y g y (USEPA) Method 8270. Table 3 Summary of Historical Groundwater Analytical Data 2009-Present Mount Hope Machinery Company Charlotte, NC GTA Project No. 150700NC Page 3 of 7 Monitoring Well ID MW-6 (2009)MW-6 (2010)MW-6 (2011)MW-6 (2012)MW-6 (2013)MW-6 (2014)MW-6 (2015)GQS VOCs Acetone <25 <25 <100 <10 <6.7 <10 <10 6,000 Benzene <1.0 <1.0 5.88 0.58 0.63 J 0.72 <0.5 1 Bromodichloromethane <1.0 <1.0 <4.0 <0.5 <0.33 <0.5 <0.5 0.6 n-Butylbenzene NA <1.0 <4.0 <0.5 <0.21 <0.5 <0.5 70 sec-Butylbenzene <1.0 <1.0 <4.0 <0.5 <0.07 <0.5 <0.5 70 Chlorobenzene <1.0 <1.0 <4.0 <0.5 <0.33 <0.5 <0.5 50 Chlorodibromomethane <1.0 <1.0 <4.0 <0.5 <0.33 <0.5 <0.5 Not Specified Chloroform <1.0 <1.0 <4.0 <0.5 0.43 J <0.5 <0.5 70 Chloromethane <1.0 <1.0 <4.0 <0.5 <0.33 <0.5 <0.5 3 1,2-Dichloroethane <1.0 <1.0 <4.0 <0.5 <0.33 <0.5 <0.5 20 Dichlorodiflouromethane <1.0 <1.0 <4.0 <0.5 0.22 J <0.5 <0.5 1,000 1,1-Dichloroethane 4.40 6.00 <4.0 5.00 5.50 5.30 0.62 6 1,1-Dichloroethene 3.1 3.9 <4.0 3.3 3.50 3.40 <0.5 7 Cis-1,2-Dichloroethene 63.1 96.5 68.3 83.0 86.0 84.0 <0.5 70 1,2-Dichloropropane <1.0 <1.0 <4.0 <0.5 <0.19 <0.5 <0.5 0.6 2-Hexanone <5.0 <5.0 <5.0 <5.0 <5.0 <0.5 <0.5 40* p-Isopropyltoluene <1.0 <1.0 <4.0 <0.5 <0.07 <0.5 <0.5 25* Methyl-tert-butyl ether (MTBE)<1.0 <1.0 <4.0 <0.5 <0.4 <0.5 <0.5 20 Mehtylene Chloride <2.0 <2.0 <4.0 <0.5 <0.52J 0.54 <0.5 5 Napthalene <1.0 <1.0 <4.0 <0.5 <0.4 <0.5 <0.5 6 Tetrachloroethene 4.20 5.00 <4.0 4.40 4.80 5.40 <0.5 0.70 Tetrahydrofuran NA NA NA NA NA NA NA Not Specified Toluene <1.0 <1.0 <4.0 <0.5 <0.33 <0.5 <0.5 600 1,2,4-Trichlorobenzene <1.0 <1.0 <4.0 <0.5 <0.5 <0.5 <0.5 70 Trichloroethene 1.6 1.9 <4.0 1.8 1.8 1.8 <0.5 3 Trichlorofluoromethane <1.0 1.6 <4.0 1.5 1.7 1.5 <0.5 2,000 Vinyl Chloride <1.0 1.1 <4.0 0.84 1.2 1.0 <0.5 0.03 Notes: MW-6 2009-2015 NA - Not analyzed by this method. Samples collected by on dates indicated in the table Results reported in micrograms per liter (µg/L) Only constituents detected above laboratory method detection limits are shown in this table. g p ( ) y y g y ( ) Method 8260. g p ( ) y y g y (USEPA) Method 8270. TICS - Tentatively Identified Compounds NCDENR Groundwater Quality Standard (GQS) (15A NCAC 02L .0202) Bold values indicated a constituent detected above laboratory method detection limits Highlighted values indicate a constituent detected above the NCAC GQS. * - Interim Maximum Allowable Concentrations Table 3 Summary of Historical Groundwater Analytical Data 2009-Present Mount Hope Machinery Company Charlotte, NC GTA Project No. 150700NC Page 4 of 7 Monitoring Well ID MW-11A (2009)MW-11A (2010)MW-11A (2011)MW-11A (2012)MW-11A (2013)MW-11A (2014)MW-11A (2015)GQS VOCs Acetone NA <25 <50 <10 <6.7 <10 <10 6,000 Benzene NA 1.60 <2.0 1.60 1.40 1.40 1.30 1 Bromodichloromethane NA <1.0 <2.0 <0.5 <0.33 <0.5 <0.5 0.6 n-Butylbenzene NA <1.0 <2.0 <0.5 <0.21 <0.5 <0.5 70 sec-Butylbenzene NA <1.0 <2.0 <0.5 <0.07 <0.5 <0.5 70 Chlorobenzene NA <1.0 <2.0 <0.5 <0.33 <0.5 <0.5 50 Chlorodibromomethane NA <1.0 <2.0 <0.5 <0.33 <0.5 <0.5 Not Specified Chloroform NA <1.0 <2.0 <0.5 0.43 J <0.5 <0.5 70 Chloromethane NA <1.0 <2.0 <0.5 <0.33 <0.5 <0.5 3 1,2-Dichloroethane NA <1.0 <2.0 <0.5 <0.33 <0.5 <0.5 20 Dichlorodiflouromethane NA <1.0 <2.0 <0.5 0.20 J <0.5 <0.5 1,000 1,1-Dichloroethane NA 8.5 7.0 6.9 5.9 4.9 4.2 6 1,1-Dichloroethene NA 4.4 3.8 3.7 3.1 2.9 2.3 7 Cis-1,2-Dichloroethene NA 100.0 86.00 85.0 67.0 61.0 56.0 70 1,2-Dichloropropane NA <1.0 <2.0 <0.5 <0.19 <0.5 <0.5 0.6 2-Hexanone NA <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 40* p-Isopropyltoluene NA <1.0 <2.0 <0.5 <0.07 <0.5 <0.5 25* Methyl-tert-butyl ether (MTBE)NA 0.73 <2.0 1.00 0.63 J 1.00 1.20 20 Mehtylene Chloride NA 0.64 <10 0.69 0.56 J 0.61 0.52 5 Napthalene NA <1.0 <2.0 <0.5 <0.4 <0.5 <0.5 6 Tetrachloroethene NA 6.10 4.04 4.90 4.40 5.00 5.60 0.70 Tetrahydrofuran NA NA NA NA NA NA NA Not Specified Toluene NA <1.0 <2.0 <0.5 <0.33 <0.5 <0.5 600 1,2,4-Trichlorobenzene NA <1.0 <2.0 <0.5 <0.5 <0.5 <0.5 70 Trichloroethene NA 2.6 2.80 3.10 2.9 3.50 4.20 3 Trichlorofluoromethane NA <1.0 <2.0 <0.5 0.32 J <0.5 <0.5 2,000 Vinyl Chloride NA 3.3 2.74 3.10 3.5 2.50 2.00 0.03 Notes: MW-11A 2009-2015 TICS - Tentatively Identified Compounds NCDENR Groundwater Quality Standard (GQS) (15A NCAC 02L .0202) Bold values indicated a constituent detected above laboratory method detection limits Highlighted values indicate a constituent detected above the NCAC GQS. * - Interim Maximum Allowable Concentrations NA - Not analyzed by this method. Samples collected by on dates indicated in the table Results reported in micrograms per liter (µg/L) Only constituents detected above laboratory method detection limits are shown in this table. g p ( ) y y g y ( ) Method 8260. g p ( ) y y g y (USEPA) Method 8270. Table 3 Summary of Historical Groundwater Analytical Data 2009-Present Mount Hope Machinery Company Charlotte, NC GTA Project No. 150700NC Page 5 of 7 Monitoring Well ID MW-13 (2009)MW-13 (2010)MW-13 (2011)MW-13 (2012)MW-13 (2013)MW-13 (2014)MW-13 (2015)GQS VOCs Acetone NA NA NA <10 NA <10 <10 6,000 Benzene NA NA NA <0.5 NA 0.57 0.67 1 Bromodichloromethane NA NA NA <0.5 NA <0.5 <0.5 0.6 n-Butylbenzene NA NA NA <0.5 NA <0.5 <0.5 70 sec-Butylbenzene NA NA NA <0.5 NA <0.5 <0.5 70 Chlorobenzene NA NA NA <0.5 NA <0.5 <0.5 50 Chlorodibromomethane NA NA NA <0.5 NA <0.5 <0.5 Not Specified Chloroform NA NA NA <0.5 NA <0.5 <0.5 70 Chloromethane NA NA NA <0.5 NA <0.5 <0.5 3 1,2-Dichloroethane NA NA NA <0.5 NA <0.5 <0.5 20 Dichlorodiflouromethane NA NA NA <0.5 NA <0.5 <0.5 1,000 1,1-Dichloroethane NA NA NA 3.7 NA 5.1 5.1 6 1,1-Dichloroethene NA NA NA 1.7 NA 3.2 3.4 7 Cis-1,2-Dichloroethene NA NA NA 60.0 NA 74.0 76.0 70 1,2-Dichloropropane NA NA NA <0.5 NA <0.5 <0.5 0.6 2-Hexanone NA NA NA <5.0 NA <5.0 <5.0 40* p-Isopropyltoluene NA NA NA <0.5 NA <0.5 <0.5 25* Methyl-tert-butyl ether (MTBE)NA NA NA <0.5 NA <0.5 <0.5 20 Mehtylene Chloride NA NA NA <0.5 NA 0.54 <0.5 5 Napthalene NA NA NA <0.5 NA <0.5 <0.5 6 Tetrachloroethene NA NA NA 3.10 NA 4.30 4.80 0.70 Tetrahydrofuran NA NA NA NA NA NA NA Not Specified Toluene NA NA NA <0.5 NA <0.5 <0.5 600 1,2,4-Trichlorobenzene NA NA NA <0.5 NA <0.5 <0.5 70 Trichloroethene NA NA NA 1.20 NA 1.80 2.20 3 Trichlorofluoromethane NA NA NA 1.10 NA 0.96 0.64 2,000 Vinyl Chloride NA NA NA <0.5 NA 0.90 0.81 0.03 Notes: MW-13 2009-2015 NCDENR Groundwater Quality Standard (GQS) (15A NCAC 02L .0202) Bold values indicated a constituent detected above laboratory method detection limits Highlighted values indicate a constituent detected above the NCAC GQS. * - Interim Maximum Allowable Concentrations NA - Not analyzed by this method. Samples collected by on dates indicated in the table Results reported in micrograms per liter (µg/L) Only constituents detected above laboratory method detection limits are shown in this table. g p ( ) y y g y ( ) Method 8260. g p ( ) y y g y (USEPA) Method 8270. TICS - Tentatively Identified Compounds Table 3 Summary of Historical Groundwater Analytical Data 2009-Present Mount Hope Machinery Company Charlotte, NC GTA Project No. 150700NC Page 6 of 7 Monitoring Well ID MW-14A (2009)MW-14A (2010)MW-14A (2011)MW-14A (2012)MW-14A (2013)MW-14A (2014)MW-14A (2015)GQS VOCs Acetone NA NA NA <10 NA <10 <10 6,000 Benzene NA NA NA 1.00 NA 1.20 1.20 1 Bromodichloromethane NA NA NA <0.5 NA <0.5 <0.5 0.6 n-Butylbenzene NA NA NA <0.5 NA <0.5 <0.5 70 sec-Butylbenzene NA NA NA <0.5 NA <0.5 <0.5 70 Chlorobenzene NA NA NA <0.5 NA <0.5 <0.5 50 Chlorodibromomethane NA NA NA <0.5 NA <0.5 <0.5 Not Specified Chloroform NA NA NA <0.5 NA <0.5 <0.5 70 Chloromethane NA NA NA <0.5 NA <0.5 <0.5 3 1,2-Dichloroethane NA NA NA <0.5 NA <0.5 <0.5 20 Dichlorodiflouromethane NA NA NA <0.5 NA <0.5 <0.5 1,000 1,1-Dichloroethane NA NA NA 7.2 NA 6.5 5.5 6 1,1-Dichloroethene NA NA NA 3.9 NA 3.6 3.3 7 Cis-1,2-Dichloroethene NA NA NA 84.0 NA 75.0 68.0 70 1,2-Dichloropropane NA NA NA <0.5 NA <0.5 <0.5 0.6 2-Hexanone NA NA NA <5.0 NA <5.0 <5.0 40* p-Isopropyltoluene NA NA NA <0.5 NA <0.5 <0.5 25* Methyl-tert-butyl ether (MTBE)NA NA NA <0.5 NA 0.59 0.62 20 Mehtylene Chloride NA NA NA 0.56 NA 0.68 0.52 5 Napthalene NA NA NA <1.0 NA <1.0 <0.5 6 Tetrachloroethene NA NA NA 4.20 NA 4.70 5.10 0.70 Tetrahydrofuran NA NA NA NA NA NA NA Not Specified Toluene NA NA NA <0.5 NA <0.5 <0.5 600 1,2,4-Trichlorobenzene NA NA NA <0.5 NA <0.5 <0.5 70 Trichloroethene NA NA NA 2.00 NA 2.60 3.10 3 Trichlorofluoromethane NA NA NA 0.86 NA 0.61 0.58 2,000 Vinyl Chloride NA NA NA 1.80 NA 1.80 1.50 0.03 Notes: MW-14A 2009-2015 TICS - Tentatively Identified Compounds NCDENR Groundwater Quality Standard (GQS) (15A NCAC 02L .0202) Bold values indicated a constituent detected above laboratory method detection limits Highlighted values indicate a constituent detected above the NCAC GQS. * - Interim Maximum Allowable Concentrations NA - Not analyzed by this method. Samples collected by on dates indicated in the table Results reported in micrograms per liter (µg/L) Only constituents detected above laboratory method detection limits are shown in this table. g p ( ) y y g y ( ) Method 8260. g p ( ) y y g y (USEPA) Method 8270. Table 3 Summary of Historical Groundwater Analytical Data 2009-Present Mount Hope Machinery Company Charlotte, NC GTA Project No. 150700NC Page 7 of 7 Monitoring Well ID MW-15A (2009)MW-15A (2010)MW-15A (2011)MW-15A (2012)MW-15A (2013)MW-15A (2014)MW-15A (2015)GQS VOCs Acetone NA NA NA <10 NA <10 <10 6,000 Benzene NA NA NA <0.5 NA 0.65 <0.5 1 Bromodichloromethane NA NA NA <0.5 NA <0.5 <0.5 0.6 n-Butylbenzene NA NA NA <0.5 NA <0.5 <0.5 70 sec-Butylbenzene NA NA NA <0.5 NA <0.5 <0.5 70 Chlorobenzene NA NA NA <0.5 NA <0.5 <0.5 50 Chlorodibromomethane NA NA NA <0.5 NA <0.5 <0.5 Not Specified Chloroform NA NA NA <0.5 NA <0.5 <0.5 70 Chloromethane NA NA NA <0.5 NA <0.5 <0.5 3 1,2-Dichloroethane NA NA NA <0.5 NA <0.5 <0.5 20 Dichlorodiflouromethane NA NA NA <0.5 NA <0.5 <0.5 1,000 1,1-Dichloroethane NA NA NA 4.4 NA 5.0 2.6 6 1,1-Dichloroethene NA NA NA 2.5 NA 2.9 0.83 7 Cis-1,2-Dichloroethene NA NA NA 71.0 NA 66.0 30.0 70 1,2-Dichloropropane NA NA NA <0.5 NA <0.5 <0.5 0.6 2-Hexanone NA NA NA <5.0 NA <5.0 <5.0 40* p-Isopropyltoluene NA NA NA <0.5 NA <0.5 <0.5 25* Methyl-tert-butyl ether (MTBE)NA NA NA <0.5 NA <0.5 <0.5 20 Mehtylene Chloride NA NA NA <0.5 NA <0.5 <0.5 5 Napthalene NA NA NA <0.5 NA <0.5 <0.5 6 Tetrachloroethene NA NA NA 3.80 NA 4.20 1.10 0.70 Tetrahydrofuran NA NA NA NA NA NA NA Not Specified Toluene NA NA NA <0.5 NA <0.5 0.90 600 1,2,4-Trichlorobenzene NA NA NA <0.5 NA <0.5 <0.5 70 Trichloroethene NA NA NA 1.60 NA 1.90 0.65 3 Trichlorofluoromethane NA NA NA 0.66 NA 0.66 <0.5 2,000 Vinyl Chloride NA NA NA 0.63 NA 0.57 <0.5 0.03 Notes: MW-15A 2009-2015 * - Interim Maximum Allowable Concentrations NA - Not analyzed by this method. Samples collected by on dates indicated in the table Results reported in micrograms per liter (µg/L) Only constituents detected above laboratory method detection limits are shown in this table. g p ( ) y y g y ( ) Method 8260. g p ( ) y y g y (USEPA) Method 8270. TICS - Tentatively Identified Compounds NCDENR Groundwater Quality Standard (GQS) (15A NCAC 02L .0202) Bold values indicated a constituent detected above laboratory method detection limits Highlighted values indicate a constituent detected above the NCAC GQS. Table 4 Complete Historical Groundwater Analytical Data 2009 - Present Mount Hope Machinery Company Charlotte, North Carolina GTA Project No. 150700NC Page 1 of 10 Well ID MW-2 MW-3 MW-4 MW-4 MW-4 MW-4R MW-4R MW-4R Sample Date 8/18/2009 8/18/2009 3/16/2010 5/6/2010 8/25/2010 6/1/2011 4/11/2012 5/25/2012 VOCs Acetone <25 <25 <25 <25 <10 <25 <10 <10 Benzene <1.0 <1.0 <1.0 <1.0 0.65 <1.0 <0.5 <0.5 Bromodichloromethane <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 n-Butylbenzene NA NA <1.0 <1.0 0.72 <1.0 <0.5 <0.5 sec-Butylbenzene <1.0 <1.0 1 <1.0 1 <1.0 <0.5 <0.5 Chlorobenzene <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 Chlorodibromomethane <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 Chloroform <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 Chloromethane <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 1,2-Dichloroethane <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 Dichlorodiflouromethane <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 1,1-Dichloroethane <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 1,1-Dichloroethene <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 Cis-1,2-Dichloroethene <1.0 <1.0 <1.0 <1.0 0.71 <1.0 <0.5 <0.5 1,2-Dichloropropane <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <5.0 2-Hexanone <5.0 <5.0 <1.0 <5.0 <5.0 <5.0 <5.0 <0.5 p-Isopropyltoluene <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 Methyl-tert-butyl ether (MTBE)<1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 Mehtylene Chloride <2.0 <2.0 <2.0 <2.0 <0.5 <5.0 <0.5 <0.5 Napthalene <1.0 <1.0 1.1 1.20 <0.5 <1.0 <0.5 <0.5 Tetrachloroethene <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 Tetrahydrofuran NA NA NA NA NA NA NA NA Toluene <1.0 <1.0 1.10 <1.0 <0.5 <1.0 <0.5 <0.5 1,2,4-Trichlorobenzene <1.0 <1.0 1.1 1.5 1.30 <1.0 <0.5 <0.5 Trichloroethene <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 Trichlorofluoromethane <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 Vinyl Chloride <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 VOC Tentatively Identified Compounds (TICS) NI NI NA NA NA NA NA NA SVOCs Benzo(a)anthracene NA NA <13.3 NA <1.7 <5.18 <1.0 NA Chrysene NA NA <13.3 NA <1.7 <5.18 <1.0 NA Flouanthene NA NA <13.3 NA <1.7 <5.18 <1.0 NA J-Methylnapthalene NA NA <13.3 NA 1.9 <5.18 3.1 NA Phenanthrene NA NA <13.3 NA <1.7 <5.18 <1.0 NA Pyrene NA NA <13.3 NA <1.7 <5.18 <1.0 NA VOC TICS J-Adamantanol NA NA 8.79 NA NA NA NA NA C-22 or larger alkane NA NA NI NA NA NA NA NA Unknown NA NA 86.81 NA NA NA NA NA * - Interim Maximum Allowable Concentrations NA - Not analyzed by this method. g p ( ) y y Protection Agency (USEPA) Method 8270. TICS - Tentatively Identified Compounds NCDENR Groundwater Quality Standard (GQS) (15A NCAC 02L .0202) Bold values indicated a constituent detected above laboratory method detection limits Highlighted values indicate a constituent detected above the NCAC GQS. Notes: Samples collected by on dates indicated in the table Results reported in micrograms per liter (µg/L) Only constituents detected above laboratory method detection limits are shown in this table. g p ( ) y y Agency (USEPA) Method 8260. Table 4 Complete Historical Groundwater Analytical Data 2009 - Present Mount Hope Machinery Company Charlotte, North Carolina GTA Project No. 150700NC Page 2 of 10 Well ID Sample Date VOCs Acetone Benzene Bromodichloromethane n-Butylbenzene sec-Butylbenzene Chlorobenzene Chlorodibromomethane Chloroform Chloromethane 1,2-Dichloroethane Dichlorodiflouromethane 1,1-Dichloroethane 1,1-Dichloroethene Cis-1,2-Dichloroethene 1,2-Dichloropropane 2-Hexanone p-Isopropyltoluene Methyl-tert-butyl ether (MTBE) Mehtylene Chloride Napthalene Tetrachloroethene Tetrahydrofuran Toluene 1,2,4-Trichlorobenzene Trichloroethene Trichlorofluoromethane Vinyl Chloride VOC Tentatively Identified Compounds (TICS) SVOCs Benzo(a)anthracene Chrysene Flouanthene J-Methylnapthalene Phenanthrene Pyrene VOC TICS J-Adamantanol C-22 or larger alkane Unknown MW-4A MW-4A MW-4A MW-4A MW-4A MW-4A MW-4A MW-4A MW-4A MW-4A MW-4A MW-4A MW-4A 8/18/2009 3/16/2010 3/16/2010 5/6/2010 8/25/2010 8/25/2010 6/1/2011 4/12/2012 4/12/2012 5/25/2012 5/23/2013 7/8/2014 6/1/2015 <25 <25 <25 <25 <10 <10 <50 <10 <10 <10 <6.7 <10 <10 1.30 1.4 1.4 1.4 1.4 1.3 <2.0 1.3 1.3 1.6 1.3 1.4 1.4 <1.0 <1.0 <1.0 <1.0 <0.5 <0.5 <2.0 <0.5 <0.5 <0.5 <0.33 <0.5 <0.5 NA NA <1.0 <1.0 <0.5 <0.5 <2.0 <0.5 <0.5 <0.5 <0.21 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <0.5 <2.0 <0.5 <0.5 <0.5 <0.07 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <0.5 <2.0 <0.5 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <0.5 <2.0 <0.5 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <0.5 <2.0 <0.5 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <0.5 <2.0 <0.5 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <0.5 <2.0 <0.5 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <0.5 <2.0 <0.5 <0.5 <0.5 0.20 J <0.5 <0.5 7.2 7.7 7.6 8.3 7.20 7.30 7.48 6.30 6.20 8.1 6.80 6.10 5.20 4.4 4 3.9 4.4 4.00 3.90 4.04 3.40 3.30 4.3 3.30 3.20 2.90 88.7 94.7 92.3 109 89.00 90.00 90.8 79.00 77.00 99 80 71 65.00 <1.0 <1.0 <1.0 <1.0 <0.5 <0.5 <2.0 <0.5 <0.5 <5.0 <0.19 <0.5 <0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <0.5 <0.5 <2.0 <0.5 <0.5 <0.5 <0.07 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 0.53 0.50 <2.0 0.54 0.53 0.74 0.61 J 0.99 1.30 <2.0 <2.0 <2.0 <2.0 0.58 0.57 <10.0 0.54 0.54 0.62 0.59 J 0.56 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <0.5 <2.0 <0.5 <0.5 <0.5 <0.4 <0.5 <0.5 4.5 5.1 5 4.5 4.80 4.60 3.78 4.80 4.70 4.6 4.3 4.5 4.80 NA NA NA NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <0.5 <0.5 <2.0 <0.5 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <0.5 <2.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2.5 2.5 2.4 2.4 2.40 2.40 2.2 2.40 2.40 2.8 2.4 2.6 3.00 <1.0 <1.0 <1.0 <0.5 <0.5 0.51 <2.0 <0.5 <0.5 <0.5 0.40 J <.05 <0.5 1.9 2 1.9 2 1.90 2.00 <2.0 1.90 1.90 2.1 2.3 1.6 1.50 NI NI NA NA NA NA NA NA NA NA NA NA NA <10.5 NA NA NA NA NA NA NA NA NA NA NA NA <10.5 NA NA NA NA NA NA NA NA NA NA NA NA <10.5 NA NA NA NA NA NA NA NA NA NA NA NA <10.5 NA NA NA NA NA NA NA NA NA NA NA NA <10.5 NA NA NA NA NA NA NA NA NA NA NA NA <10.5 NA NA NA NA NA NA NA NA NA NA NA NA NI NA NA NA NA NA NA NA NA NA NA NA NA 36.5 NA NA NA NA NA NA NA NA NA NA NA NA 38 NA NA NA NA NA NA NA NA NA NA NA NA Notes: Samples collected by on dates indicated in the table Results reported in micrograms per liter (µg/L) Only constituents detected above laboratory method detection limits are shown in this table. g p ( ) y y Agency (USEPA) Method 8260. g p ( ) y y Protection Agency (USEPA) Method 8270. TICS - Tentatively Identified Compounds NCDENR Groundwater Quality Standard (GQS) (15A NCAC 02L .0202) Bold values indicated a constituent detected above laboratory method detection limits Highlighted values indicate a constituent detected above the NCAC GQS. * - Interim Maximum Allowable Concentrations NA - Not analyzed by this method. Table 4 Complete Historical Groundwater Analytical Data 2009 - Present Mount Hope Machinery Company Charlotte, North Carolina GTA Project No. 150700NC Page 3 of 10 Well ID Sample Date VOCs Acetone Benzene Bromodichloromethane n-Butylbenzene sec-Butylbenzene Chlorobenzene Chlorodibromomethane Chloroform Chloromethane 1,2-Dichloroethane Dichlorodiflouromethane 1,1-Dichloroethane 1,1-Dichloroethene Cis-1,2-Dichloroethene 1,2-Dichloropropane 2-Hexanone p-Isopropyltoluene Methyl-tert-butyl ether (MTBE) Mehtylene Chloride Napthalene Tetrachloroethene Tetrahydrofuran Toluene 1,2,4-Trichlorobenzene Trichloroethene Trichlorofluoromethane Vinyl Chloride VOC Tentatively Identified Compounds (TICS) SVOCs Benzo(a)anthracene Chrysene Flouanthene J-Methylnapthalene Phenanthrene Pyrene VOC TICS J-Adamantanol C-22 or larger alkane Unknown MW-5 MW-5 MW-5 MW-5 MW-5 MW-5 MW-5 MW-5 MW-5 MW-5 8/18/2009 3/16/2010 5/6/2010 8/25/2010 6/1/2011 4/11/2012 4/25/2012 5/22/2013 7/7/2014 6/1/2015 <25 <25 <25 <10 <25 <10 <10 <6.7 <10 <10 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.13 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <.33 <0.5 <0.5 NA NA <1.0 <0.5 <1.0 <0.5 <0.5 <0.21 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.07 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.35 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.20 <0.5 <0.5 1.60 <1.0 <1.0 1.1 1.57 0.77 1 0.61 J <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 0.17 J <0.5 <0.5 24.40 9.6 5.7 17 22.30 11.00 15 7.40 2.30 2.30 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.19 <0.5 <0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.07 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.40 <0.5 <0.5 <2.0 <2.0 <2.0 <0.5 <5.0 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <.4 <0.5 <0.5 1.90 1.1 <1.0 1.4 1.53 1.30 1.8 1.30 1.30 1.30 NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.51 <0.5 <0.5 <1.0 2.5 2.4 <0.5 <1.0 <0.5 <0.5 0.21 J <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.3 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.054 <0.5 <0.5 NI NA NA NA NA NA NA NA NA NA <12.5 NA <1.0 <5.26 <1.0 NA NA NA NA NA <12.5 NA <1.0 <5.26 <1.0 NA NA NA NA NA <12.5 NA <1.0 <5.26 <1.0 NA NA NA NA NA <12.5 NA <1.0 <5.26 <1.0 NA NA NA NA NA <12.5 NA <1.0 <5.26 <1.0 NA NA NA NA NA <12.5 NA <1.0 <5.26 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 26.44 NA NA NA NA NA NA NA NA * - Interim Maximum Allowable Concentrations NA - Not analyzed by this method. g p ( ) y y Protection Agency (USEPA) Method 8270. TICS - Tentatively Identified Compounds NCDENR Groundwater Quality Standard (GQS) (15A NCAC 02L .0202) Bold values indicated a constituent detected above laboratory method detection limits Highlighted values indicate a constituent detected above the NCAC GQS. Notes: Samples collected by on dates indicated in the table Results reported in micrograms per liter (µg/L) Only constituents detected above laboratory method detection limits are shown in this table. g p ( ) y y Agency (USEPA) Method 8260. Table 4 Complete Historical Groundwater Analytical Data 2009 - Present Mount Hope Machinery Company Charlotte, North Carolina GTA Project No. 150700NC Page 4 of 10 Well ID Sample Date VOCs Acetone Benzene Bromodichloromethane n-Butylbenzene sec-Butylbenzene Chlorobenzene Chlorodibromomethane Chloroform Chloromethane 1,2-Dichloroethane Dichlorodiflouromethane 1,1-Dichloroethane 1,1-Dichloroethene Cis-1,2-Dichloroethene 1,2-Dichloropropane 2-Hexanone p-Isopropyltoluene Methyl-tert-butyl ether (MTBE) Mehtylene Chloride Napthalene Tetrachloroethene Tetrahydrofuran Toluene 1,2,4-Trichlorobenzene Trichloroethene Trichlorofluoromethane Vinyl Chloride VOC Tentatively Identified Compounds (TICS) SVOCs Benzo(a)anthracene Chrysene Flouanthene J-Methylnapthalene Phenanthrene Pyrene VOC TICS J-Adamantanol C-22 or larger alkane Unknown MW-6 MW-6 MW-6 MW-6 MW-6 MW-6 MW-6 MW-6 MW-6 MW-6 8/18/2009 3/16/2010 5/6/2010 8/25/2010 6/1/2011 4/11/2012 5/25/2012 5/22/2013 7/7/2014 6/1/2015 <25 <25 <25 <10 <100 <10 <10 <6.7 <10 <10 <1.0 <1.0 <1.0 <0.5 5.88 0.53 0.58 0.63 J 0.72 <0.5 <1.0 <1.0 <1.0 <0.5 <4.0 <0.5 <0.5 <.33 <0.5 <0.5 NA NA <1.0 <0.5 <4.0 <0.5 <0.5 <0.21 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <4.0 <0.5 <0.5 <0.07 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <4.0 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <4.0 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <4.0 <0.5 <0.5 0.43 J <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <4.0 <0.5 <0.5 <0.35 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <4.0 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <4.0 <0.5 <0.5 0.22 J <0.5 <0.5 4.4 4.4 6 4.1 <4.0 4.20 5 5.50 5.30 0.62 3.1 3 3.9 2.9 <4.0 2.80 3.3 3.50 3.40 <0.5 63.1 72.9 96.5 71 68.30 72.00 83 86.00 84.00 <0.5 <1.0 <1.0 <1.0 <0.5 <4.0 <0.5 <0.5 <0.19 <0.5 <0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <0.5 <4.0 <0.5 <0.5 <0.07 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <4.0 <0.5 <0.5 <0.40 <0.5 <0.5 <2.0 <2.0 <2.0 <0.5 <4.0 <0.5 <0.5 0.52 J 0.54 <0.5 <1.0 <1.0 <1.0 <0.5 <4.0 <0.5 <0.5 <.4 <0.5 <0.5 4.2 4.7 5 <0.5 <4.0 4.40 4.3 4.80 5.40 <0.5 NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <0.5 <4.0 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <4.0 <0.5 <0.5 <0.51 <0.5 <0.5 1.6 1.7 1.9 1.5 <4.0 1.70 1.8 1.80 1.80 <0.5 <1.0 1.5 1.6 1.4 <4.0 1.40 1.5 1.70 1.50 <0.5 <1.0 <1.0 1.1 0.77 <4.0 0.84 0.81 1.20 0.99 <0.5 NI NA NA NA NA NA NA NA NA NA NA <11.8 NA <1.0 <5.18 <1.0 NA NA NA NA NA <11.8 NA <1.0 <5.18 <1.0 NA NA NA NA NA <11.8 NA <1.0 <5.18 <1.0 NA NA NA NA NA <11.8 NA <1.0 <5.18 <1.0 NA NA NA NA NA <11.8 NA <1.0 <5.18 <1.0 NA NA NA NA NA <11.8 NA <1.0 <5.18 <1.0 NA NA NA NA NA NI NA NA NA NA NA NA NA NA NA NI NA NA NA NA NA NA NA NA NA NI NA NA NA NA NA NA NA NA Notes: Samples collected by on dates indicated in the table Results reported in micrograms per liter (µg/L) Only constituents detected above laboratory method detection limits are shown in this table. g p ( ) y y Agency (USEPA) Method 8260. g p ( ) y y Protection Agency (USEPA) Method 8270. TICS - Tentatively Identified Compounds NCDENR Groundwater Quality Standard (GQS) (15A NCAC 02L .0202) Bold values indicated a constituent detected above laboratory method detection limits Highlighted values indicate a constituent detected above the NCAC GQS. * - Interim Maximum Allowable Concentrations NA - Not analyzed by this method. Table 4 Complete Historical Groundwater Analytical Data 2009 - Present Mount Hope Machinery Company Charlotte, North Carolina GTA Project No. 150700NC Page 5 of 10 Well ID Sample Date VOCs Acetone Benzene Bromodichloromethane n-Butylbenzene sec-Butylbenzene Chlorobenzene Chlorodibromomethane Chloroform Chloromethane 1,2-Dichloroethane Dichlorodiflouromethane 1,1-Dichloroethane 1,1-Dichloroethene Cis-1,2-Dichloroethene 1,2-Dichloropropane 2-Hexanone p-Isopropyltoluene Methyl-tert-butyl ether (MTBE) Mehtylene Chloride Napthalene Tetrachloroethene Tetrahydrofuran Toluene 1,2,4-Trichlorobenzene Trichloroethene Trichlorofluoromethane Vinyl Chloride VOC Tentatively Identified Compounds (TICS) SVOCs Benzo(a)anthracene Chrysene Flouanthene J-Methylnapthalene Phenanthrene Pyrene VOC TICS J-Adamantanol C-22 or larger alkane Unknown MW-7 MW-7 MW-7 MW-7 MW-8 MW-10A MW-10A MW-10A MW-10A MW-10A MW-10A MW-10A MW-10A 8/18/2009 6/1/2011 4/12/2012 5/25/2012 8/18/2009 8/18/2009 3/16/2010 5/6/2012 8/25/2010 6/2/2011 4/12/2012 5/25/2012 5/22/2013 <25 <25 <10 <10 <25 <25 <25 <25 <10 <25 <10 <10 <6.7 <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.13 <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.33 NA <1.0 <0.5 <0.5 NA NA <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.21 <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.07 <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.33 <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.33 <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.33 <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.34 <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.33 <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.20 <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 6.20 <1.0 <0.5 <0.5 0.15 J <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 3.30 <1.0 <0.5 <0.5 <0.16 <1.0 <1.0 0.76 <0.5 <1.0 1.20 2.3 3.40 2.30 2.23 1.4 1.7 1.7 <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5'<0.19 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <0.5 <1.0 <0.5 <0.5 <0.07 <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 1.3 2.20 2.50 2.91 2.9 6.3 5.3 <2.0 <2.0 <0.5 <0.5 <2.0 <2.0 <10.0 0.54 0.54 <5.0 <0.5 <0.5 <0.33 <1.0 <1.0 <0.5 0.68 <1.0 <1.0 <2.0 <0.5 <0.5 <1.0 <0.5 <0.5 <0.4 <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 0.74 <1.0 <0.5 0.84 0.69 J NA NA NA NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <.05 <.05 <0.33 <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <.05 <.05 <0.51 <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <.05 <.05 0.21 J <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <.05 <.05 <0.3 <1.0 <1.0 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <.05 <.05 <0.054 NI NA NA NA NI NI NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA * - Interim Maximum Allowable Concentrations NA - Not analyzed by this method. g p ( ) y y Protection Agency (USEPA) Method 8270. TICS - Tentatively Identified Compounds NCDENR Groundwater Quality Standard (GQS) (15A NCAC 02L .0202) Bold values indicated a constituent detected above laboratory method detection limits Highlighted values indicate a constituent detected above the NCAC GQS. Notes: Samples collected by on dates indicated in the table Results reported in micrograms per liter (µg/L) Only constituents detected above laboratory method detection limits are shown in this table. g p ( ) y y Agency (USEPA) Method 8260. Table 4 Complete Historical Groundwater Analytical Data 2009 - Present Mount Hope Machinery Company Charlotte, North Carolina GTA Project No. 150700NC Page 6 of 10 Well ID Sample Date VOCs Acetone Benzene Bromodichloromethane n-Butylbenzene sec-Butylbenzene Chlorobenzene Chlorodibromomethane Chloroform Chloromethane 1,2-Dichloroethane Dichlorodiflouromethane 1,1-Dichloroethane 1,1-Dichloroethene Cis-1,2-Dichloroethene 1,2-Dichloropropane 2-Hexanone p-Isopropyltoluene Methyl-tert-butyl ether (MTBE) Mehtylene Chloride Napthalene Tetrachloroethene Tetrahydrofuran Toluene 1,2,4-Trichlorobenzene Trichloroethene Trichlorofluoromethane Vinyl Chloride VOC Tentatively Identified Compounds (TICS) SVOCs Benzo(a)anthracene Chrysene Flouanthene J-Methylnapthalene Phenanthrene Pyrene VOC TICS J-Adamantanol C-22 or larger alkane Unknown MW-11A MW-11A MW-11A MW-11A MW-11A MW-11A MW-11A MW-11A MW-11A MW-11A MW-11A 3/16/2010 5/6/2010 5/6/2010 8/25/2010 6/1/2011 6/1/2011 4/12/2012 5/24/2012 5/22/2013 7/7/2014 6/1/2015 <25 <25 <25 <10 <50 <50 <10 <10 <6.7 <10 <10 1.40 1.60 1.50 1.5 <2.0 <2.0 1.4 1.6 1.4 1.4 1.3 <1.0 <1.0 <1.0 <0.5 <2.0 <2.0 <0.5 <0.5 <.33 <0.5 <0.5 NA NA <1.0 <0.5 <2.0 <2.0 <0.5 <0.5 <0.21 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <2.0 <2.0 <0.5 <0.5 <0.07 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <2.0 <2.0 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <2.0 <2.0 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <2.0 <2.0 <0.5 <0.5 0.43 J <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <2.0 <2.0 <0.5 <0.5 <0.35 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <2.0 <2.0 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <2.0 <2.0 <0.5 <0.5 0.20 J <0.5 <0.5 7.1 8.2 8.5 6.9 6.4 7 5.90 6.9 5.90 4.90 4.20 3.9 4.3 4.4 3.7 3.5 3.8 3.10 3.7 3.10 2.90 2.30 79.7 98.8 100 78 71.80 86.00 70.00 85 67.00 61.00 56.00 <1.0 <1.0 <1.0 <0.5 <2.0 <2.0 <0.5 <0.5 <0.19 <0.5 <0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <0.5 <2.0 <2.0 <0.5 <0.5 <0.07 <0.5 <0.5 <1.0 <1.0 <1.0 0.73 <2.0 <2.0 0.77 1 0.63 J 1.00 1.20 <2.0 <2.0 <2.0 0.64 <10 <10 0.58 0.69 0.56 J 0.61 0.52 <1.0 <1.0 <1.0 <0.5 <2.0 <2.0 <0.5 <0.5 <.4 <0.5 <0.5 6.1 4.6 4.6 4.6 4.00 4.04 4.10 4.9 4.40 5.00 5.60 NA NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <0.5 <2.0 <2.0 <0.5 <0.5 <0.33 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <2.0 <2.0 <0.5 <0.5 <0.51 <0.5 <0.5 2.6 2.5 2.5 2.6 2.80 2.30 2.80 3.1 2.90 3.50 4.20 <1.0 <1.0 <1.0 <0.5 <2.0 <2.0 <0.5 <0.5 0.32 J <0.5 <0.5 3.1 3.1 3.2 3.3 2.74 <2.0 3.10 3 3.50 2.50 2.00 NI NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Notes: Samples collected by on dates indicated in the table Results reported in micrograms per liter (µg/L) Only constituents detected above laboratory method detection limits are shown in this table. g p ( ) y y Agency (USEPA) Method 8260. g p ( ) y y Protection Agency (USEPA) Method 8270. TICS - Tentatively Identified Compounds NCDENR Groundwater Quality Standard (GQS) (15A NCAC 02L .0202) Bold values indicated a constituent detected above laboratory method detection limits Highlighted values indicate a constituent detected above the NCAC GQS. * - Interim Maximum Allowable Concentrations NA - Not analyzed by this method. Table 4 Complete Historical Groundwater Analytical Data 2009 - Present Mount Hope Machinery Company Charlotte, North Carolina GTA Project No. 150700NC Page 7 of 10 Well ID Sample Date VOCs Acetone Benzene Bromodichloromethane n-Butylbenzene sec-Butylbenzene Chlorobenzene Chlorodibromomethane Chloroform Chloromethane 1,2-Dichloroethane Dichlorodiflouromethane 1,1-Dichloroethane 1,1-Dichloroethene Cis-1,2-Dichloroethene 1,2-Dichloropropane 2-Hexanone p-Isopropyltoluene Methyl-tert-butyl ether (MTBE) Mehtylene Chloride Napthalene Tetrachloroethene Tetrahydrofuran Toluene 1,2,4-Trichlorobenzene Trichloroethene Trichlorofluoromethane Vinyl Chloride VOC Tentatively Identified Compounds (TICS) SVOCs Benzo(a)anthracene Chrysene Flouanthene J-Methylnapthalene Phenanthrene Pyrene VOC TICS J-Adamantanol C-22 or larger alkane Unknown MW-12A MW-12A MW-12A MW-12A MW-12A MW-13 MW-13 MW-13 MW-13 6/14/2010 8/25/2010 6/1/2011 4/12/2012 5/25/2012 4/12/2012 5/25/2012 7/7/2014 6/1/2015 <20 <10 <25 <10 <50 <10 <10 <10 <10 <1.0 <0.5 <1.0 <0.5 <0.5 <0.5 <0.5 0.57 0.67 <1.0 <0.5 <1.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.0 <0.5 <1.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.0 <0.5 <1.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.0 <0.5 <1.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.0 <0.5 <1.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2.00 <0.5 <1.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 3.60 <0.5 <1.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.0 <0.5 <1.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.0 <0.5 <1.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.0 <0.5 <1.0 <0.5 <0.5 2.7 3.7 5.1 5.1 <1.0 <0.5 <1.0 <0.5 <0.5 1.3 1.7 3.2 3.4 <1.0 <0.5 <1.0 <0.5 <0.5 42 60 74 76 <1.0 <0.5 <1.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <0.5 <1.0 <0.5 <0.5 11 <0.5 <0.5 <0.5 <1.0 <0.5 <1.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.0 <0.5 <1.0 <0.5 <0.5 <0.5 <0.5 0.54 <0.5 <1.0 <0.5 <1.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.0 <0.5 <1.0 <0.5 <0.5 2.9 3.1 4.3 4.8 NA NA NA NA NA NA NA NA NA <1.0 <0.5 <1.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.0 <0.5 <1.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.0 <0.5 <1.0 <0.5 <0.5 0.99 1.2 1.8 2.2 <1.0 <0.5 <1.0 <0.5 <0.5 0.67 1.1 0.96 0.64 <1.0 <0.5 <1.0 <0.5 <0.5 <0.5 <0.5 0.9 0.81 NI NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA * - Interim Maximum Allowable Concentrations NA - Not analyzed by this method. g p ( ) y y Protection Agency (USEPA) Method 8270. TICS - Tentatively Identified Compounds NCDENR Groundwater Quality Standard (GQS) (15A NCAC 02L .0202) Bold values indicated a constituent detected above laboratory method detection limits Highlighted values indicate a constituent detected above the NCAC GQS. Notes: Samples collected by on dates indicated in the table Results reported in micrograms per liter (µg/L) Only constituents detected above laboratory method detection limits are shown in this table. g p ( ) y y Agency (USEPA) Method 8260. Table 4 Complete Historical Groundwater Analytical Data 2009 - Present Mount Hope Machinery Company Charlotte, North Carolina GTA Project No. 150700NC Page 8 of 10 Well ID Sample Date VOCs Acetone Benzene Bromodichloromethane n-Butylbenzene sec-Butylbenzene Chlorobenzene Chlorodibromomethane Chloroform Chloromethane 1,2-Dichloroethane Dichlorodiflouromethane 1,1-Dichloroethane 1,1-Dichloroethene Cis-1,2-Dichloroethene 1,2-Dichloropropane 2-Hexanone p-Isopropyltoluene Methyl-tert-butyl ether (MTBE) Mehtylene Chloride Napthalene Tetrachloroethene Tetrahydrofuran Toluene 1,2,4-Trichlorobenzene Trichloroethene Trichlorofluoromethane Vinyl Chloride VOC Tentatively Identified Compounds (TICS) SVOCs Benzo(a)anthracene Chrysene Flouanthene J-Methylnapthalene Phenanthrene Pyrene VOC TICS J-Adamantanol C-22 or larger alkane Unknown MW-14 MW-14 MW-14A MW-14A MW-14A MW-14A MW-15A MW-15A MW-15A MW-15A 4/12/2012 5/25/2012 4/11/2012 5/24/2012 7/7/2014 6/1/2015 4/12/2012 5/25/2012 7/7/2014 6/1/2015 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <0.5 <0.5 1.00 1.00 1.20 1.20 <0.5 <0.5 0.65 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.51 6 7.2 6.5 5.5 3.3 4.4 5.00 2.60 <0.5 <0.5 3.4 3.9 3.6 3.3 1.6 2.5 2.90 0.83 2.8 3.4 73 84 75 68 49 71.00 66.00 30.00 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 1.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.6 0.59 0.62 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.52 0.56 0.68 0.52 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.0 <1.0 <1.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 4.2 3.1 4.7 5.1 2.8 3.80 4.20 1.10 NA NA NA NA NA NA NA NA NA NA <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.90 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2 1.9 2.6 3.1 1.1 1.60 1.90 0.65 <0.5 <0.5 0.8 0.86 0.61 0.58 0.55 0.66 0.66 <0.5 <0.5 <0.5 1.8 1.7 1.8 1.5 0.5 0.63 0.57 <0.5 NA NA NA NA NA NA NA NA NA NA NA NA NA <11.8 NA NA <1.0 <5.18 <1.0 NA NA NA NA <11.8 NA NA <1.0 <5.18 <1.0 NA NA NA NA <11.8 NA NA <1.0 <5.18 <1.0 NA NA NA NA <11.8 NA NA <1.0 <5.18 <1.0 NA NA NA NA <11.8 NA NA <1.0 <5.18 <1.0 NA NA NA NA <11.8 NA NA <1.0 <5.18 <1.0 NA NA NA NA NI NA NA NA NA NA NA NA NA NA NI NA NA NA NA NA NA NA NA NA NI NA NA NA NA NA NA Notes: Samples collected by on dates indicated in the table Results reported in micrograms per liter (µg/L) Only constituents detected above laboratory method detection limits are shown in this table. g p ( ) y y Agency (USEPA) Method 8260. g p ( ) y y Protection Agency (USEPA) Method 8270. TICS - Tentatively Identified Compounds NCDENR Groundwater Quality Standard (GQS) (15A NCAC 02L .0202) Bold values indicated a constituent detected above laboratory method detection limits Highlighted values indicate a constituent detected above the NCAC GQS. * - Interim Maximum Allowable Concentrations NA - Not analyzed by this method. Table 4 Complete Historical Groundwater Analytical Data 2009 - Present Mount Hope Machinery Company Charlotte, North Carolina GTA Project No. 150700NC Page 9 of 10 Well ID Sample Date VOCs Acetone Benzene Bromodichloromethane n-Butylbenzene sec-Butylbenzene Chlorobenzene Chlorodibromomethane Chloroform Chloromethane 1,2-Dichloroethane Dichlorodiflouromethane 1,1-Dichloroethane 1,1-Dichloroethene Cis-1,2-Dichloroethene 1,2-Dichloropropane 2-Hexanone p-Isopropyltoluene Methyl-tert-butyl ether (MTBE) Mehtylene Chloride Napthalene Tetrachloroethene Tetrahydrofuran Toluene 1,2,4-Trichlorobenzene Trichloroethene Trichlorofluoromethane Vinyl Chloride VOC Tentatively Identified Compounds (TICS) SVOCs Benzo(a)anthracene Chrysene Flouanthene J-Methylnapthalene Phenanthrene Pyrene VOC TICS J-Adamantanol C-22 or larger alkane Unknown MW-16 MW-16A MW-17 AL-1 AL-1 AL-1 AL-1 AL-1 AL-1 AL-1 8/8/2012 8/8/2012 8/8/2012 8/18/2009 3/16/2010 5/6/2010 8/25/2010 6/1/2011 4/12/2012 5/25/2012 2.3 J 1.4 J 3.5 J <25 <25 <25 <10 <25 <10 <10 0.18 J 0.4 0.43 J <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.08 0.9 1.2 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.05 <0.05 <0.05 NA <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.05 <0.05 <0.05 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.05 0.11 J <0.5 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.12 0.49 J 0.56 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.02 2.90 7.5 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.13 0.32 J <0.13 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.06 0.14 J 0.16 J <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.06 <0.05 <0.05 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 1.9 3.30 3.00 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.1 1.80 1.50 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 5.1 36.00 15.00 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.2 <0.2 0.31 J <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 2.7 <0.06 <0.06 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 0.11 J 0.15 J 0.35 J <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <2.3 <2.3 <2.3 <2.0 <2.0 <2.0 <0.5 <5.0 <0.5 <0.5 <0.21 <0.21 <0.21 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 0.67 J 2.80 1.90 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 NA NA NA NA NA NA NA NA NA NA 0.12 J <0.4 <0.04 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.11 <0.11 <0.11 <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 0.32 J 1.20 0.7 J <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 <0.07 0.69 J 0.5 J <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 0.29 J 0.44 J 0.31 J <1.0 <1.0 <1.0 <0.5 <1.0 <0.5 <0.5 NA NA NA NI NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA * - Interim Maximum Allowable Concentrations NA - Not analyzed by this method. g p ( ) y y Protection Agency (USEPA) Method 8270. TICS - Tentatively Identified Compounds NCDENR Groundwater Quality Standard (GQS) (15A NCAC 02L .0202) Bold values indicated a constituent detected above laboratory method detection limits Highlighted values indicate a constituent detected above the NCAC GQS. Notes: Samples collected by on dates indicated in the table Results reported in micrograms per liter (µg/L) Only constituents detected above laboratory method detection limits are shown in this table. g p ( ) y y Agency (USEPA) Method 8260. Table 4 Complete Historical Groundwater Analytical Data 2009 - Present Mount Hope Machinery Company Charlotte, North Carolina GTA Project No. 150700NC Page 10 of 10 Well ID Sample Date VOCs Acetone Benzene Bromodichloromethane n-Butylbenzene sec-Butylbenzene Chlorobenzene Chlorodibromomethane Chloroform Chloromethane 1,2-Dichloroethane Dichlorodiflouromethane 1,1-Dichloroethane 1,1-Dichloroethene Cis-1,2-Dichloroethene 1,2-Dichloropropane 2-Hexanone p-Isopropyltoluene Methyl-tert-butyl ether (MTBE) Mehtylene Chloride Napthalene Tetrachloroethene Tetrahydrofuran Toluene 1,2,4-Trichlorobenzene Trichloroethene Trichlorofluoromethane Vinyl Chloride VOC Tentatively Identified Compounds (TICS) SVOCs Benzo(a)anthracene Chrysene Flouanthene J-Methylnapthalene Phenanthrene Pyrene VOC TICS J-Adamantanol C-22 or larger alkane Unknown AL-2 AL-2 AL-2 AL-2 AL-2 GQS 5/6/2010 8/25/2010 6/1/2011 4/12/2012 5/25/2012 <25 <10 <25 <10 <10 6,000 <1.0 <0.5 <1.0 <0.5 <0.5 1 <1.0 <0.5 <1.0 <0.5 <0.5 0.6 <1.0 <0.5 <1.0 <0.5 <0.5 70 <1.0 <0.5 <1.0 <0.5 <0.5 70 <1.0 <0.5 <1.0 <0.5 <0.5 50 <1.0 <0.5 <1.0 <0.5 <0.5 Not Specified <1.0 <0.5 <1.0 <0.5 <0.5 70 <1.0 <0.5 <1.0 <0.5 <0.5 3 <1.0 <0.5 <1.0 <0.5 <0.5 20 <1.0 <0.5 <1.0 <0.5 <0.5 1,000 <1.0 <0.5 <1.0 <0.5 <0.5 6 <1.0 <0.5 <1.0 <0.5 <0.5 7 <1.0 <0.5 <1.0 <0.5 <0.5 70 <1.0 <0.5 <1.0 <0.5 <0.5 0.6 <5.0 <5.0 <5.0 <5.0 <5.0 40* <1.0 <0.5 <1.0 <0.5 <0.5 25* <1.0 <0.5 <1.0 <0.5 <0.5 20 <2.0 <0.5 <5.0 <0.5 <0.5 5 <1.0 <0.5 <1.0 <0.5 <0.5 6 <1.0 <0.5 <1.0 <0.5 <0.5 0.70 NA NA NA NA NA Not Specified <1.0 <0.5 <1.0 <0.5 <0.5 600 <1.0 <0.5 <1.0 <0.5 <0.5 70 <1.0 <0.5 <1.0 <0.5 <0.5 3 <1.0 <0.5 <1.0 <0.5 <0.5 2,000 <1.0 <0.5 <1.0 <0.5 <0.5 0.03 NA NA NA NA NA NA NA NA NA NA 0.05 NA NA NA NA NA 5 NA NA NA NA NA 300 NA NA NA NA NA 1* NA NA NA NA NA 200 NA NA NA NA NA 200 NA NA NA NA NA Not Specified NA NA NA NA NA Not Specified NA NA NA NA NA Not Specified Notes: Samples collected by on dates indicated in the table Results reported in micrograms per liter (µg/L) Only constituents detected above laboratory method detection limits are shown in this table. g p ( ) y y g y ( Method 8260. g p ( ) y y g (USEPA) Method 8270. TICS - Tentatively Identified Compounds NCDENR Groundwater Quality Standard (GQS) (15A NCAC 02L .0202) Bold values indicated a constituent detected above laboratory method detection limits Highlighted values indicate a constituent detected above the NCAC GQS. * - Interim Maximum Allowable Concentrations NA - Not analyzed by this method. Appendix A Laboratory Analytical Reports and Chain-of-Custody Records SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis GTA Associates, Inc. 710 Peninsula Lane, Suite B Charlotte, NC 28273 Attention: Matt Hickey QF02090Lot Number: 1050700NCProject Number: Mount HopeProject Name: 06/09/2015Date Completed: Nisreen Saikaly Project Manager *QF02090* This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist. Page: 1 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Case Narrative GTA Associates, Inc. Lot Number: QF02090 SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Page: 2 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary GTA Associates, Inc. Lot Number: QF02090 Sample Number Sample ID Matrix Date Sampled Date Received 001 06/01/2015 1300MW-4A Aqueous 06/02/2015 002 06/01/2015 1035MW-5 Aqueous 06/02/2015 003 06/01/2015 1345MW-6 Aqueous 06/02/2015 004 06/01/2015 1030MW-11A Aqueous 06/02/2015 005 06/01/2015 1115MW-13 Aqueous 06/02/2015 006 06/01/2015 1355MW-14A Aqueous 06/02/2015 007 06/01/2015 1115MW-15A Aqueous 06/02/2015 (7 samples) Page: 3 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Executive Summary GTA Associates, Inc. Lot Number: QF02090 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 MW-4A Aqueous Benzene 8260B 1.4 ug/L 6 001 MW-4A Aqueous 1,1-Dichloroethane 8260B 5.2 ug/L 6 001 MW-4A Aqueous 1,1-Dichloroethene 8260B 2.9 ug/L 6 001 MW-4A Aqueous cis-1,2-Dichloroethene 8260B 65 ug/L 6 001 MW-4A Aqueous Methyl tertiary butyl ether 8260B 1.3 ug/L 6 001 MW-4A Aqueous Tetrachloroethene 8260B 4.8 ug/L 7 001 MW-4A Aqueous Trichloroethene 8260B 3.0 ug/L 7 001 MW-4A Aqueous Vinyl chloride 8260B 1.5 ug/L 7 002 MW-5 Aqueous cis-1,2-Dichloroethene 8260B 2.3 ug/L 8 002 MW-5 Aqueous Tetrachloroethene 8260B 1.3 ug/L 9 003 MW-6 Aqueous 1,1-Dichloroethane 8260B 0.62 ug/L 10 004 MW-11A Aqueous Benzene 8260B 1.3 ug/L 12 004 MW-11A Aqueous 1,1-Dichloroethane 8260B 4.2 ug/L 12 004 MW-11A Aqueous 1,1-Dichloroethene 8260B 2.3 ug/L 12 004 MW-11A Aqueous cis-1,2-Dichloroethene 8260B 56 ug/L 12 004 MW-11A Aqueous Methyl tertiary butyl ether 8260B 1.2 ug/L 12 004 MW-11A Aqueous Methylene chloride 8260B 0.52 ug/L 13 004 MW-11A Aqueous Tetrachloroethene 8260B 5.6 ug/L 13 004 MW-11A Aqueous Trichloroethene 8260B 4.2 ug/L 13 004 MW-11A Aqueous Vinyl chloride 8260B 2.0 ug/L 13 005 MW-13 Aqueous Benzene 8260B 0.67 ug/L 14 005 MW-13 Aqueous 1,1-Dichloroethane 8260B 5.1 ug/L 14 005 MW-13 Aqueous 1,1-Dichloroethene 8260B 3.4 ug/L 14 005 MW-13 Aqueous cis-1,2-Dichloroethene 8260B 76 ug/L 14 005 MW-13 Aqueous Tetrachloroethene 8260B 4.8 ug/L 15 005 MW-13 Aqueous Trichloroethene 8260B 2.2 ug/L 15 005 MW-13 Aqueous Trichlorofluoromethane 8260B 0.64 ug/L 15 005 MW-13 Aqueous Vinyl chloride 8260B 0.81 ug/L 15 006 MW-14A Aqueous Benzene 8260B 1.2 ug/L 16 006 MW-14A Aqueous 1,1-Dichloroethane 8260B 5.5 ug/L 16 006 MW-14A Aqueous 1,1-Dichloroethene 8260B 3.3 ug/L 16 006 MW-14A Aqueous cis-1,2-Dichloroethene 8260B 68 ug/L 16 006 MW-14A Aqueous Methyl tertiary butyl ether 8260B 0.62 ug/L 16 006 MW-14A Aqueous Methylene chloride 8260B 0.52 ug/L 17 006 MW-14A Aqueous Tetrachloroethene 8260B 5.1 ug/L 17 006 MW-14A Aqueous Trichloroethene 8260B 3.1 ug/L 17 006 MW-14A Aqueous Trichlorofluoromethane 8260B 0.58 ug/L 17 006 MW-14A Aqueous Vinyl chloride 8260B 1.5 ug/L 17 007 MW-15A Aqueous 1,1-Dichloroethane 8260B 2.6 ug/L 18 007 MW-15A Aqueous 1,1-Dichloroethene 8260B 0.83 ug/L 18 007 MW-15A Aqueous cis-1,2-Dichloroethene 8260B 30 ug/L 18 007 MW-15A Aqueous Tetrachloroethene 8260B 1.1 ug/L 19 007 MW-15A Aqueous Toluene 8260B 0.90 ug/L 19 007 MW-15A Aqueous Trichloroethene 8260B 0.65 ug/L 19 Page: 4 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Executive Summary (Continued) Lot Number: QF02090 Sample Sample ID Matrix Parameter Method Result Q Units Page (44 detections) Page: 5 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: GTA Associates, Inc. MW-4A QF02090-001 06/01/2015 1300 06/02/2015 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 06/04/2015 2117 PMM2 76590 AnalyticalCAS Parameter Number Method Result Q PQL Units Run Acetone 67-64-1 8260B ND 1ug/L10 Benzene 71-43-2 8260B 1.4 1ug/L0.50 Bromobenzene 108-86-1 8260B ND 1ug/L0.50 Bromochloromethane 74-97-5 8260B ND 1ug/L0.50 Bromodichloromethane 75-27-4 8260B ND 1ug/L0.50 Bromoform 75-25-2 8260B ND 1ug/L0.50 Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.50 2-Butanone (MEK)78-93-3 8260B ND 1ug/L5.0 n-Butylbenzene 104-51-8 8260B ND 1ug/L0.50 sec-Butylbenzene 135-98-8 8260B ND 1ug/L0.50 tert-Butylbenzene 98-06-6 8260B ND 1ug/L0.50 Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.50 Chlorobenzene 108-90-7 8260B ND 1ug/L0.50 Chloroethane 75-00-3 8260B ND 1ug/L0.50 Chloroform 67-66-3 8260B ND 1ug/L0.50 Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.50 2-Chlorotoluene 95-49-8 8260B ND 1ug/L0.50 4-Chlorotoluene 106-43-4 8260B ND 1ug/L0.50 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.50 Dibromochloromethane 124-48-1 8260B ND 1ug/L0.50 1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.50 Dibromomethane (Methylene bromide)74-95-3 8260B ND 1ug/L0.50 1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.50 1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L0.50 1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.50 Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L0.50 1,1-Dichloroethane 75-34-3 8260B 5.2 1ug/L0.50 1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.50 1,1-Dichloroethene 75-35-4 8260B 2.9 1ug/L0.50 cis-1,2-Dichloroethene 156-59-2 8260B 65 1ug/L0.50 trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.50 1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.50 1,3-Dichloropropane 142-28-9 8260B ND 1ug/L0.50 2,2-Dichloropropane 594-20-7 8260B ND 1ug/L0.50 1,1-Dichloropropene 563-58-6 8260B ND 1ug/L0.50 cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.50 trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.50 Diisopropyl ether (IPE)108-20-3 8260B ND 1ug/L0.50 Ethylbenzene 100-41-4 8260B ND 1ug/L0.50 Hexachlorobutadiene 87-68-3 8260B ND 1ug/L0.50 2-Hexanone 591-78-6 8260B ND 1ug/L5.0 Isopropylbenzene 98-82-8 8260B ND 1ug/L0.50 p-Isopropyltoluene 99-87-6 8260B ND 1ug/L0.50 Methyl tertiary butyl ether (MTBE)1634-04-4 8260B 1.3 1ug/L0.50 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria_ H = Out of holding time Page: 6 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: GTA Associates, Inc. MW-4A QF02090-001 06/01/2015 1300 06/02/2015 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 06/04/2015 2117 PMM2 76590 AnalyticalCAS Parameter Number Method Result Q PQL Units Run 4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L5.0 Methylene chloride 75-09-2 8260B ND 1ug/L0.50 Naphthalene 91-20-3 8260B ND 1ug/L0.50 n-Propylbenzene 103-65-1 8260B ND 1ug/L0.50 Styrene 100-42-5 8260B ND 1ug/L0.50 1,1,1,2-Tetrachloroethane 630-20-6 8260B ND 1ug/L0.50 1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.50 Tetrachloroethene 127-18-4 8260B 4.8 1ug/L0.50 Toluene 108-88-3 8260B ND 1ug/L0.50 1,2,3-Trichlorobenzene 87-61-6 8260B ND 1ug/L0.50 1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L0.50 1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.50 1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.50 Trichloroethene 79-01-6 8260B 3.0 1ug/L0.50 Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.50 1,2,3-Trichloropropane 96-18-4 8260B ND 1ug/L0.50 1,2,4-Trimethylbenzene 95-63-6 8260B ND 1ug/L0.50 1,3,5-Trimethylbenzene 108-67-8 8260B ND 1ug/L0.50 Vinyl acetate 108-05-4 8260B ND 1ug/L1.0 Vinyl chloride 75-01-4 8260B 1.5 1ug/L0.50 m+p - Xylenes 179601-23-1 8260B ND 1ug/L0.50 o - Xylenes 95-47-6 8260B ND 1ug/L0.50 AcceptanceRun 1 Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 87 70-130 Bromofluorobenzene 88 70-130 Toluene-d8 89 70-130 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria_ H = Out of holding time Page: 7 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: GTA Associates, Inc. MW-5 QF02090-002 06/01/2015 1035 06/02/2015 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 06/04/2015 2141 PMM2 76590 AnalyticalCAS Parameter Number Method Result Q PQL Units Run Acetone 67-64-1 8260B ND 1ug/L10 Benzene 71-43-2 8260B ND 1ug/L0.50 Bromobenzene 108-86-1 8260B ND 1ug/L0.50 Bromochloromethane 74-97-5 8260B ND 1ug/L0.50 Bromodichloromethane 75-27-4 8260B ND 1ug/L0.50 Bromoform 75-25-2 8260B ND 1ug/L0.50 Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.50 2-Butanone (MEK)78-93-3 8260B ND 1ug/L5.0 n-Butylbenzene 104-51-8 8260B ND 1ug/L0.50 sec-Butylbenzene 135-98-8 8260B ND 1ug/L0.50 tert-Butylbenzene 98-06-6 8260B ND 1ug/L0.50 Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.50 Chlorobenzene 108-90-7 8260B ND 1ug/L0.50 Chloroethane 75-00-3 8260B ND 1ug/L0.50 Chloroform 67-66-3 8260B ND 1ug/L0.50 Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.50 2-Chlorotoluene 95-49-8 8260B ND 1ug/L0.50 4-Chlorotoluene 106-43-4 8260B ND 1ug/L0.50 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.50 Dibromochloromethane 124-48-1 8260B ND 1ug/L0.50 1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.50 Dibromomethane (Methylene bromide)74-95-3 8260B ND 1ug/L0.50 1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.50 1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L0.50 1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.50 Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L0.50 1,1-Dichloroethane 75-34-3 8260B ND 1ug/L0.50 1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.50 1,1-Dichloroethene 75-35-4 8260B ND 1ug/L0.50 cis-1,2-Dichloroethene 156-59-2 8260B 2.3 1ug/L0.50 trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.50 1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.50 1,3-Dichloropropane 142-28-9 8260B ND 1ug/L0.50 2,2-Dichloropropane 594-20-7 8260B ND 1ug/L0.50 1,1-Dichloropropene 563-58-6 8260B ND 1ug/L0.50 cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.50 trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.50 Diisopropyl ether (IPE)108-20-3 8260B ND 1ug/L0.50 Ethylbenzene 100-41-4 8260B ND 1ug/L0.50 Hexachlorobutadiene 87-68-3 8260B ND 1ug/L0.50 2-Hexanone 591-78-6 8260B ND 1ug/L5.0 Isopropylbenzene 98-82-8 8260B ND 1ug/L0.50 p-Isopropyltoluene 99-87-6 8260B ND 1ug/L0.50 Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L0.50 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria_ H = Out of holding time Page: 8 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: GTA Associates, Inc. MW-5 QF02090-002 06/01/2015 1035 06/02/2015 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 06/04/2015 2141 PMM2 76590 AnalyticalCAS Parameter Number Method Result Q PQL Units Run 4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L5.0 Methylene chloride 75-09-2 8260B ND 1ug/L0.50 Naphthalene 91-20-3 8260B ND 1ug/L0.50 n-Propylbenzene 103-65-1 8260B ND 1ug/L0.50 Styrene 100-42-5 8260B ND 1ug/L0.50 1,1,1,2-Tetrachloroethane 630-20-6 8260B ND 1ug/L0.50 1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.50 Tetrachloroethene 127-18-4 8260B 1.3 1ug/L0.50 Toluene 108-88-3 8260B ND 1ug/L0.50 1,2,3-Trichlorobenzene 87-61-6 8260B ND 1ug/L0.50 1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L0.50 1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.50 1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.50 Trichloroethene 79-01-6 8260B ND 1ug/L0.50 Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.50 1,2,3-Trichloropropane 96-18-4 8260B ND 1ug/L0.50 1,2,4-Trimethylbenzene 95-63-6 8260B ND 1ug/L0.50 1,3,5-Trimethylbenzene 108-67-8 8260B ND 1ug/L0.50 Vinyl acetate 108-05-4 8260B ND 1ug/L1.0 Vinyl chloride 75-01-4 8260B ND 1ug/L0.50 m+p - Xylenes 179601-23-1 8260B ND 1ug/L0.50 o - Xylenes 95-47-6 8260B ND 1ug/L0.50 AcceptanceRun 1 Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 89 70-130 Bromofluorobenzene 90 70-130 Toluene-d8 90 70-130 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria_ H = Out of holding time Page: 9 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: GTA Associates, Inc. MW-6 QF02090-003 06/01/2015 1345 06/02/2015 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 06/04/2015 2206 PMM2 76590 AnalyticalCAS Parameter Number Method Result Q PQL Units Run Acetone 67-64-1 8260B ND 1ug/L10 Benzene 71-43-2 8260B ND 1ug/L0.50 Bromobenzene 108-86-1 8260B ND 1ug/L0.50 Bromochloromethane 74-97-5 8260B ND 1ug/L0.50 Bromodichloromethane 75-27-4 8260B ND 1ug/L0.50 Bromoform 75-25-2 8260B ND 1ug/L0.50 Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.50 2-Butanone (MEK)78-93-3 8260B ND 1ug/L5.0 n-Butylbenzene 104-51-8 8260B ND 1ug/L0.50 sec-Butylbenzene 135-98-8 8260B ND 1ug/L0.50 tert-Butylbenzene 98-06-6 8260B ND 1ug/L0.50 Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.50 Chlorobenzene 108-90-7 8260B ND 1ug/L0.50 Chloroethane 75-00-3 8260B ND 1ug/L0.50 Chloroform 67-66-3 8260B ND 1ug/L0.50 Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.50 2-Chlorotoluene 95-49-8 8260B ND 1ug/L0.50 4-Chlorotoluene 106-43-4 8260B ND 1ug/L0.50 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.50 Dibromochloromethane 124-48-1 8260B ND 1ug/L0.50 1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.50 Dibromomethane (Methylene bromide)74-95-3 8260B ND 1ug/L0.50 1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.50 1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L0.50 1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.50 Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L0.50 1,1-Dichloroethane 75-34-3 8260B 0.62 1ug/L0.50 1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.50 1,1-Dichloroethene 75-35-4 8260B ND 1ug/L0.50 cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L0.50 trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.50 1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.50 1,3-Dichloropropane 142-28-9 8260B ND 1ug/L0.50 2,2-Dichloropropane 594-20-7 8260B ND 1ug/L0.50 1,1-Dichloropropene 563-58-6 8260B ND 1ug/L0.50 cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.50 trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.50 Diisopropyl ether (IPE)108-20-3 8260B ND 1ug/L0.50 Ethylbenzene 100-41-4 8260B ND 1ug/L0.50 Hexachlorobutadiene 87-68-3 8260B ND 1ug/L0.50 2-Hexanone 591-78-6 8260B ND 1ug/L5.0 Isopropylbenzene 98-82-8 8260B ND 1ug/L0.50 p-Isopropyltoluene 99-87-6 8260B ND 1ug/L0.50 Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L0.50 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria_ H = Out of holding time Page: 10 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: GTA Associates, Inc. MW-6 QF02090-003 06/01/2015 1345 06/02/2015 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 06/04/2015 2206 PMM2 76590 AnalyticalCAS Parameter Number Method Result Q PQL Units Run 4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L5.0 Methylene chloride 75-09-2 8260B ND 1ug/L0.50 Naphthalene 91-20-3 8260B ND 1ug/L0.50 n-Propylbenzene 103-65-1 8260B ND 1ug/L0.50 Styrene 100-42-5 8260B ND 1ug/L0.50 1,1,1,2-Tetrachloroethane 630-20-6 8260B ND 1ug/L0.50 1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.50 Tetrachloroethene 127-18-4 8260B ND 1ug/L0.50 Toluene 108-88-3 8260B ND 1ug/L0.50 1,2,3-Trichlorobenzene 87-61-6 8260B ND 1ug/L0.50 1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L0.50 1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.50 1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.50 Trichloroethene 79-01-6 8260B ND 1ug/L0.50 Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.50 1,2,3-Trichloropropane 96-18-4 8260B ND 1ug/L0.50 1,2,4-Trimethylbenzene 95-63-6 8260B ND 1ug/L0.50 1,3,5-Trimethylbenzene 108-67-8 8260B ND 1ug/L0.50 Vinyl acetate 108-05-4 8260B ND 1ug/L1.0 Vinyl chloride 75-01-4 8260B ND 1ug/L0.50 m+p - Xylenes 179601-23-1 8260B ND 1ug/L0.50 o - Xylenes 95-47-6 8260B ND 1ug/L0.50 AcceptanceRun 1 Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 88 70-130 Bromofluorobenzene 89 70-130 Toluene-d8 90 70-130 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria_ H = Out of holding time Page: 11 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: GTA Associates, Inc. MW-11A QF02090-004 06/01/2015 1030 06/02/2015 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 06/04/2015 2229 PMM2 76590 AnalyticalCAS Parameter Number Method Result Q PQL Units Run Acetone 67-64-1 8260B ND 1ug/L10 Benzene 71-43-2 8260B 1.3 1ug/L0.50 Bromobenzene 108-86-1 8260B ND 1ug/L0.50 Bromochloromethane 74-97-5 8260B ND 1ug/L0.50 Bromodichloromethane 75-27-4 8260B ND 1ug/L0.50 Bromoform 75-25-2 8260B ND 1ug/L0.50 Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.50 2-Butanone (MEK)78-93-3 8260B ND 1ug/L5.0 n-Butylbenzene 104-51-8 8260B ND 1ug/L0.50 sec-Butylbenzene 135-98-8 8260B ND 1ug/L0.50 tert-Butylbenzene 98-06-6 8260B ND 1ug/L0.50 Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.50 Chlorobenzene 108-90-7 8260B ND 1ug/L0.50 Chloroethane 75-00-3 8260B ND 1ug/L0.50 Chloroform 67-66-3 8260B ND 1ug/L0.50 Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.50 2-Chlorotoluene 95-49-8 8260B ND 1ug/L0.50 4-Chlorotoluene 106-43-4 8260B ND 1ug/L0.50 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.50 Dibromochloromethane 124-48-1 8260B ND 1ug/L0.50 1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.50 Dibromomethane (Methylene bromide)74-95-3 8260B ND 1ug/L0.50 1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.50 1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L0.50 1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.50 Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L0.50 1,1-Dichloroethane 75-34-3 8260B 4.2 1ug/L0.50 1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.50 1,1-Dichloroethene 75-35-4 8260B 2.3 1ug/L0.50 cis-1,2-Dichloroethene 156-59-2 8260B 56 1ug/L0.50 trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.50 1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.50 1,3-Dichloropropane 142-28-9 8260B ND 1ug/L0.50 2,2-Dichloropropane 594-20-7 8260B ND 1ug/L0.50 1,1-Dichloropropene 563-58-6 8260B ND 1ug/L0.50 cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.50 trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.50 Diisopropyl ether (IPE)108-20-3 8260B ND 1ug/L0.50 Ethylbenzene 100-41-4 8260B ND 1ug/L0.50 Hexachlorobutadiene 87-68-3 8260B ND 1ug/L0.50 2-Hexanone 591-78-6 8260B ND 1ug/L5.0 Isopropylbenzene 98-82-8 8260B ND 1ug/L0.50 p-Isopropyltoluene 99-87-6 8260B ND 1ug/L0.50 Methyl tertiary butyl ether (MTBE)1634-04-4 8260B 1.2 1ug/L0.50 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria_ H = Out of holding time Page: 12 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: GTA Associates, Inc. MW-11A QF02090-004 06/01/2015 1030 06/02/2015 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 06/04/2015 2229 PMM2 76590 AnalyticalCAS Parameter Number Method Result Q PQL Units Run 4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L5.0 Methylene chloride 75-09-2 8260B 0.52 1ug/L0.50 Naphthalene 91-20-3 8260B ND 1ug/L0.50 n-Propylbenzene 103-65-1 8260B ND 1ug/L0.50 Styrene 100-42-5 8260B ND 1ug/L0.50 1,1,1,2-Tetrachloroethane 630-20-6 8260B ND 1ug/L0.50 1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.50 Tetrachloroethene 127-18-4 8260B 5.6 1ug/L0.50 Toluene 108-88-3 8260B ND 1ug/L0.50 1,2,3-Trichlorobenzene 87-61-6 8260B ND 1ug/L0.50 1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L0.50 1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.50 1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.50 Trichloroethene 79-01-6 8260B 4.2 1ug/L0.50 Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.50 1,2,3-Trichloropropane 96-18-4 8260B ND 1ug/L0.50 1,2,4-Trimethylbenzene 95-63-6 8260B ND 1ug/L0.50 1,3,5-Trimethylbenzene 108-67-8 8260B ND 1ug/L0.50 Vinyl acetate 108-05-4 8260B ND 1ug/L1.0 Vinyl chloride 75-01-4 8260B 2.0 1ug/L0.50 m+p - Xylenes 179601-23-1 8260B ND 1ug/L0.50 o - Xylenes 95-47-6 8260B ND 1ug/L0.50 AcceptanceRun 1 Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 90 70-130 Bromofluorobenzene 87 70-130 Toluene-d8 91 70-130 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria_ H = Out of holding time Page: 13 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: GTA Associates, Inc. MW-13 QF02090-005 06/01/2015 1115 06/02/2015 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 06/04/2015 2253 PMM2 76590 AnalyticalCAS Parameter Number Method Result Q PQL Units Run Acetone 67-64-1 8260B ND 1ug/L10 Benzene 71-43-2 8260B 0.67 1ug/L0.50 Bromobenzene 108-86-1 8260B ND 1ug/L0.50 Bromochloromethane 74-97-5 8260B ND 1ug/L0.50 Bromodichloromethane 75-27-4 8260B ND 1ug/L0.50 Bromoform 75-25-2 8260B ND 1ug/L0.50 Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.50 2-Butanone (MEK)78-93-3 8260B ND 1ug/L5.0 n-Butylbenzene 104-51-8 8260B ND 1ug/L0.50 sec-Butylbenzene 135-98-8 8260B ND 1ug/L0.50 tert-Butylbenzene 98-06-6 8260B ND 1ug/L0.50 Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.50 Chlorobenzene 108-90-7 8260B ND 1ug/L0.50 Chloroethane 75-00-3 8260B ND 1ug/L0.50 Chloroform 67-66-3 8260B ND 1ug/L0.50 Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.50 2-Chlorotoluene 95-49-8 8260B ND 1ug/L0.50 4-Chlorotoluene 106-43-4 8260B ND 1ug/L0.50 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.50 Dibromochloromethane 124-48-1 8260B ND 1ug/L0.50 1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.50 Dibromomethane (Methylene bromide)74-95-3 8260B ND 1ug/L0.50 1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.50 1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L0.50 1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.50 Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L0.50 1,1-Dichloroethane 75-34-3 8260B 5.1 1ug/L0.50 1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.50 1,1-Dichloroethene 75-35-4 8260B 3.4 1ug/L0.50 cis-1,2-Dichloroethene 156-59-2 8260B 76 1ug/L0.50 trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.50 1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.50 1,3-Dichloropropane 142-28-9 8260B ND 1ug/L0.50 2,2-Dichloropropane 594-20-7 8260B ND 1ug/L0.50 1,1-Dichloropropene 563-58-6 8260B ND 1ug/L0.50 cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.50 trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.50 Diisopropyl ether (IPE)108-20-3 8260B ND 1ug/L0.50 Ethylbenzene 100-41-4 8260B ND 1ug/L0.50 Hexachlorobutadiene 87-68-3 8260B ND 1ug/L0.50 2-Hexanone 591-78-6 8260B ND 1ug/L5.0 Isopropylbenzene 98-82-8 8260B ND 1ug/L0.50 p-Isopropyltoluene 99-87-6 8260B ND 1ug/L0.50 Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L0.50 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria_ H = Out of holding time Page: 14 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: GTA Associates, Inc. MW-13 QF02090-005 06/01/2015 1115 06/02/2015 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 06/04/2015 2253 PMM2 76590 AnalyticalCAS Parameter Number Method Result Q PQL Units Run 4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L5.0 Methylene chloride 75-09-2 8260B ND 1ug/L0.50 Naphthalene 91-20-3 8260B ND 1ug/L0.50 n-Propylbenzene 103-65-1 8260B ND 1ug/L0.50 Styrene 100-42-5 8260B ND 1ug/L0.50 1,1,1,2-Tetrachloroethane 630-20-6 8260B ND 1ug/L0.50 1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.50 Tetrachloroethene 127-18-4 8260B 4.8 1ug/L0.50 Toluene 108-88-3 8260B ND 1ug/L0.50 1,2,3-Trichlorobenzene 87-61-6 8260B ND 1ug/L0.50 1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L0.50 1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.50 1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.50 Trichloroethene 79-01-6 8260B 2.2 1ug/L0.50 Trichlorofluoromethane 75-69-4 8260B 0.64 1ug/L0.50 1,2,3-Trichloropropane 96-18-4 8260B ND 1ug/L0.50 1,2,4-Trimethylbenzene 95-63-6 8260B ND 1ug/L0.50 1,3,5-Trimethylbenzene 108-67-8 8260B ND 1ug/L0.50 Vinyl acetate 108-05-4 8260B ND 1ug/L1.0 Vinyl chloride 75-01-4 8260B 0.81 1ug/L0.50 m+p - Xylenes 179601-23-1 8260B ND 1ug/L0.50 o - Xylenes 95-47-6 8260B ND 1ug/L0.50 AcceptanceRun 1 Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 90 70-130 Bromofluorobenzene 87 70-130 Toluene-d8 91 70-130 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria_ H = Out of holding time Page: 15 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: GTA Associates, Inc. MW-14A QF02090-006 06/01/2015 1355 06/02/2015 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 06/05/2015 1849 EH1 76638 AnalyticalCAS Parameter Number Method Result Q PQL Units Run Acetone 67-64-1 8260B ND 1ug/L10 Benzene 71-43-2 8260B 1.2 1ug/L0.50 Bromobenzene 108-86-1 8260B ND 1ug/L0.50 Bromochloromethane 74-97-5 8260B ND 1ug/L0.50 Bromodichloromethane 75-27-4 8260B ND 1ug/L0.50 Bromoform 75-25-2 8260B ND 1ug/L0.50 Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.50 2-Butanone (MEK)78-93-3 8260B ND 1ug/L5.0 n-Butylbenzene 104-51-8 8260B ND 1ug/L0.50 sec-Butylbenzene 135-98-8 8260B ND 1ug/L0.50 tert-Butylbenzene 98-06-6 8260B ND 1ug/L0.50 Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.50 Chlorobenzene 108-90-7 8260B ND 1ug/L0.50 Chloroethane 75-00-3 8260B ND 1ug/L0.50 Chloroform 67-66-3 8260B ND 1ug/L0.50 Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.50 2-Chlorotoluene 95-49-8 8260B ND 1ug/L0.50 4-Chlorotoluene 106-43-4 8260B ND 1ug/L0.50 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.50 Dibromochloromethane 124-48-1 8260B ND 1ug/L0.50 1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.50 Dibromomethane (Methylene bromide)74-95-3 8260B ND 1ug/L0.50 1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.50 1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L0.50 1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.50 Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L0.50 1,1-Dichloroethane 75-34-3 8260B 5.5 1ug/L0.50 1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.50 1,1-Dichloroethene 75-35-4 8260B 3.3 1ug/L0.50 cis-1,2-Dichloroethene 156-59-2 8260B 68 1ug/L0.50 trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.50 1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.50 1,3-Dichloropropane 142-28-9 8260B ND 1ug/L0.50 2,2-Dichloropropane 594-20-7 8260B ND 1ug/L0.50 1,1-Dichloropropene 563-58-6 8260B ND 1ug/L0.50 cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.50 trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.50 Diisopropyl ether (IPE)108-20-3 8260B ND 1ug/L0.50 Ethylbenzene 100-41-4 8260B ND 1ug/L0.50 Hexachlorobutadiene 87-68-3 8260B ND 1ug/L0.50 2-Hexanone 591-78-6 8260B ND 1ug/L5.0 Isopropylbenzene 98-82-8 8260B ND 1ug/L0.50 p-Isopropyltoluene 99-87-6 8260B ND 1ug/L0.50 Methyl tertiary butyl ether (MTBE)1634-04-4 8260B 0.62 1ug/L0.50 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria_ H = Out of holding time Page: 16 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: GTA Associates, Inc. MW-14A QF02090-006 06/01/2015 1355 06/02/2015 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 06/05/2015 1849 EH1 76638 AnalyticalCAS Parameter Number Method Result Q PQL Units Run 4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L5.0 Methylene chloride 75-09-2 8260B 0.52 1ug/L0.50 Naphthalene 91-20-3 8260B ND 1ug/L0.50 n-Propylbenzene 103-65-1 8260B ND 1ug/L0.50 Styrene 100-42-5 8260B ND 1ug/L0.50 1,1,1,2-Tetrachloroethane 630-20-6 8260B ND 1ug/L0.50 1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.50 Tetrachloroethene 127-18-4 8260B 5.1 1ug/L0.50 Toluene 108-88-3 8260B ND 1ug/L0.50 1,2,3-Trichlorobenzene 87-61-6 8260B ND 1ug/L0.50 1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L0.50 1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.50 1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.50 Trichloroethene 79-01-6 8260B 3.1 1ug/L0.50 Trichlorofluoromethane 75-69-4 8260B 0.58 1ug/L0.50 1,2,3-Trichloropropane 96-18-4 8260B ND 1ug/L0.50 1,2,4-Trimethylbenzene 95-63-6 8260B ND 1ug/L0.50 1,3,5-Trimethylbenzene 108-67-8 8260B ND 1ug/L0.50 Vinyl acetate 108-05-4 8260B ND 1ug/L1.0 Vinyl chloride 75-01-4 8260B 1.5 1ug/L0.50 m+p - Xylenes 179601-23-1 8260B ND 1ug/L0.50 o - Xylenes 95-47-6 8260B ND 1ug/L0.50 AcceptanceRun 1 Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 89 70-130 Bromofluorobenzene 87 70-130 Toluene-d8 89 70-130 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria_ H = Out of holding time Page: 17 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: GTA Associates, Inc. MW-15A QF02090-007 06/01/2015 1115 06/02/2015 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 06/05/2015 1913 EH1 76638 AnalyticalCAS Parameter Number Method Result Q PQL Units Run Acetone 67-64-1 8260B ND 1ug/L10 Benzene 71-43-2 8260B ND 1ug/L0.50 Bromobenzene 108-86-1 8260B ND 1ug/L0.50 Bromochloromethane 74-97-5 8260B ND 1ug/L0.50 Bromodichloromethane 75-27-4 8260B ND 1ug/L0.50 Bromoform 75-25-2 8260B ND 1ug/L0.50 Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.50 2-Butanone (MEK)78-93-3 8260B ND 1ug/L5.0 n-Butylbenzene 104-51-8 8260B ND 1ug/L0.50 sec-Butylbenzene 135-98-8 8260B ND 1ug/L0.50 tert-Butylbenzene 98-06-6 8260B ND 1ug/L0.50 Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.50 Chlorobenzene 108-90-7 8260B ND 1ug/L0.50 Chloroethane 75-00-3 8260B ND 1ug/L0.50 Chloroform 67-66-3 8260B ND 1ug/L0.50 Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.50 2-Chlorotoluene 95-49-8 8260B ND 1ug/L0.50 4-Chlorotoluene 106-43-4 8260B ND 1ug/L0.50 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.50 Dibromochloromethane 124-48-1 8260B ND 1ug/L0.50 1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.50 Dibromomethane (Methylene bromide)74-95-3 8260B ND 1ug/L0.50 1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.50 1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L0.50 1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.50 Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L0.50 1,1-Dichloroethane 75-34-3 8260B 2.6 1ug/L0.50 1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.50 1,1-Dichloroethene 75-35-4 8260B 0.83 1ug/L0.50 cis-1,2-Dichloroethene 156-59-2 8260B 30 1ug/L0.50 trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.50 1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.50 1,3-Dichloropropane 142-28-9 8260B ND 1ug/L0.50 2,2-Dichloropropane 594-20-7 8260B ND 1ug/L0.50 1,1-Dichloropropene 563-58-6 8260B ND 1ug/L0.50 cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.50 trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.50 Diisopropyl ether (IPE)108-20-3 8260B ND 1ug/L0.50 Ethylbenzene 100-41-4 8260B ND 1ug/L0.50 Hexachlorobutadiene 87-68-3 8260B ND 1ug/L0.50 2-Hexanone 591-78-6 8260B ND 1ug/L5.0 Isopropylbenzene 98-82-8 8260B ND 1ug/L0.50 p-Isopropyltoluene 99-87-6 8260B ND 1ug/L0.50 Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L0.50 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria_ H = Out of holding time Page: 18 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: GTA Associates, Inc. MW-15A QF02090-007 06/01/2015 1115 06/02/2015 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 06/05/2015 1913 EH1 76638 AnalyticalCAS Parameter Number Method Result Q PQL Units Run 4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L5.0 Methylene chloride 75-09-2 8260B ND 1ug/L0.50 Naphthalene 91-20-3 8260B ND 1ug/L0.50 n-Propylbenzene 103-65-1 8260B ND 1ug/L0.50 Styrene 100-42-5 8260B ND 1ug/L0.50 1,1,1,2-Tetrachloroethane 630-20-6 8260B ND 1ug/L0.50 1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.50 Tetrachloroethene 127-18-4 8260B 1.1 1ug/L0.50 Toluene 108-88-3 8260B 0.90 1ug/L0.50 1,2,3-Trichlorobenzene 87-61-6 8260B ND 1ug/L0.50 1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L0.50 1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.50 1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.50 Trichloroethene 79-01-6 8260B 0.65 1ug/L0.50 Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.50 1,2,3-Trichloropropane 96-18-4 8260B ND 1ug/L0.50 1,2,4-Trimethylbenzene 95-63-6 8260B ND 1ug/L0.50 1,3,5-Trimethylbenzene 108-67-8 8260B ND 1ug/L0.50 Vinyl acetate 108-05-4 8260B ND 1ug/L1.0 Vinyl chloride 75-01-4 8260B ND 1ug/L0.50 m+p - Xylenes 179601-23-1 8260B ND 1ug/L0.50 o - Xylenes 95-47-6 8260B ND 1ug/L0.50 AcceptanceRun 1 Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 92 70-130 Bromofluorobenzene 87 70-130 Toluene-d8 91 70-130 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria_ H = Out of holding time Page: 19 of 19 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1