17022_PSNC_MW Sampling_20080925

^miELD
ENGINEERING, INC.
September 25, 2008
PSNC Energy
800 Gaston Road
P.O.Box 1398
Gastonia, North Carolina 28053-1398
Attn: Mr. Darrell Shier
Subject: Report of Monitoring Well Sampling
Former Statesville Operations Center
433 Drake Street, Statesville, North Carolina
Shield Job No. 1080186
Dear Mr. Shier:
Shield Engineering, Inc. (Shield) appreciates the opportunity to provide this report of
monitoring well sampling for the Drake Street Facility. Our services were requested by PSNC
Energy.
Services Performed
Monitoring wells MW-1 through MW-15 andMW-16D were sampled on August 5,2008. The
wells were located on the subject site and north of the site across Connor Street. Other wells are
shown to be on the property north of the site on a site plan from a Limited Site Assessment
Report provided to us by TBE dated July 2006. However, we were not requested to sample
those wells.
Depths to groundwater were measured at the site monitoring wells prior to well purging and
sampling with an electronic water level indicator that was field decontaminated before each
measurement. Groundwater elevations at the wells were determined by subtracting the
measured groundwater depths from the top-bf-casing elevations provided to us from the TBE
Limited Site Assessment Report dated July 2006.
The wells were purged by removing three water column volumes from each well with new,
separate, factory cleaned disposable PVC bailers. Water samples were collected in laboratory
cleaned and laboratory furnished containers, preserved on ice, and delivered to Pace Analytical
Services, Inc., Huntersville, North Carolina (Pace). Chain-of-custody protocol was followed.
t301 Taggari Creek Road
Oharlotte, NC 28208
www.shieldengineering.com
Telephone [phone]
Fax [phone]
PSNC Energ)'
Report of Monitoring Well Sampling
Former Statesville Operations Center
Shield Job No. 1080186
September 25, 2008
Page 2
The samples were analyzed for volatile organic compounds using EPA Method 8260 and
Natural
Attenuation Parameters including iron, manganese, BOD, nitrate, COD and sulfate by various
EPA or Standard methods. Additional parameters pH, Oxidation Reduction Potential (ORP)
and Dissolved Oxygen (DO) were measured in the field with calibrated electronic meters.
Findings
Groundwater elevations determined at each monitoring well are listed in the attached Table 1.
Figure 1 illustrates a groundwater elevation contour map. Based on the elevation data,
groundwater flow is to the south.
Laboratory analytical results of the August 5, 2008 sampling event are summarized in the
attached Table 2. Volatile organic compounds (VOCs) were detected in the samples from
monitoring wells MW-3, MW-4, MW-5, MW-11, MW-12, MW-14, and MW-16D. The only
VOC detected that exceeds the 15 A NCAC 2L Groundwater Standards (2L Standards) was
tetrachloroethene (PCE) in monitoring wells MW-3, MW-4, MW-12, MW-14 and MW-16D.
The maximum detected concentration of PCE was in well MW-3 at a concentration of 7.7
micrograms per liter (ug/1) versus the 2L Standard of 0.7 ug/1. Based on the lateral extent of the
VOCs in groundwater and the groundwater flow direction, the source of the detected VOCs in
groundwater appears to be from offsite north of the subject property.
A summary of historical sampling results is provided as Table 3. The data indicate the detected
constituent concentrations are generally decreasing over time.
The Natural Attenuation parameters iron, manganese, BOD, nitrate, COD, sulfate, pH, ORP and
DO appear to represent natural concentrations measured in groundwater in this region. The
groundwater condition appears to be in an oxidizing state rather than reducing. Relatively low
concentration of degradation products of PCE such as cis-1,2 dichloroethene were present in the
latest sampling event, while the degradation product vinyl chloride has not been detected
historically. Based on the relatively low concentrations of VOCs detected in groundwater and
the overall trend of natural concentration reduction, monitored natural attenuation would be a
more feasible remedial approach at this time than an active remediation. Further evaluation
may be required to define the down gradient extent of PCE in groundwater as well as to the
north ofthe subject site.
PSNC Energy
Report of Monitoring Well Sanapling
Former Statesville Operations Center
Shield Job No. 1080186
September 25, 2008
Page 3
We appreciate the opportunity to provide our professional services to PSNC Energy on this
project and loolc forv/ard to providing further assistance. Please feel free to contact us ifyou
have any questions conceming this report.
Sincerely,
SHIELD ENGINEERING, INC.
Thomas W. Witner, P.G.
Senior Technical Specialist
Michael D. Arniour, P.G.
Principal
Attachment
H:\Projecls\2008\10S01S6 PSNC Slalesville\groiindwaler sampling report.doc
Table 1
Summary of Well Construction and Groundwater Elevation Data
PSNC Energy
Statesville, Iredell County, North Carolina
CASING DEPTH TO WATER WeU Screened
WELL DATE ELEV. WATER ELEV. Depth Interval
(Feet) (Feet) (Feet) (Feet) (Ft below grade)
MW-1 8/5/2008 75.00 19.61 55.39 25 15-25
MW-2 8/5/2008 75.78 18.72 57.06 25 15-25
MW-3 8/5/2008 75.25 16.77 58.48 25 15-25
MW-4 8/5/2008 73.4 18.88 54.52 25 15-25
MW-5 8/5/2008 71.71 20.04 51.67 25 15-30
MW-6 8/5/2008 73.93 19.21 54.72 30 15-30
MW-7 8/5/2008 70.87 14.35 56.52 30 15-30
MW-8 8/5/2008 73.8 12.93 60.87 30 15-30
MW-9 8/5/2008 84.32 26.54 57.78 35 15-35
MW-10 8/5/2008 81.53 22.62 58.91 40 15-40
MW-11 8/5/2008 74.73 15.01 59.72 30 15-30
MW-12 8/5/2008 73.98 18.87 55.11 25 15-25
MW-13 8/5/2008 69.13 20.01 49.12 25 15-25
MW-14 8/5/2008 70.5 21.44 49.06 25 15-25
MW-15 8/5/2008 71.52 20.42 51.10 25 15-25
MW-16D 8/5/2008 74.96 14.90 60.06 60 50-60
Notes:
Elevations referenced to an arbitrary site reference point (top of casing of MW-1 = 75.00 feet).
TOC Elevations, Screen Intervals and Total Well Depths based on TBE group LSA Report Dated July 2006
Table 2
Summary of Groundwater Sampling Results
PSNC Energy :
433 Drake Street
Statesville, Iredell County, North CaroUna {
Shield Project No. 1080186 '
Analytical Method EPA 8260 EPA 6010 EPA 6010 (Lab Filtered) SM 5210B1 EPA 353.2 SM 5220D ASTM D516-90 Held Parameters
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MW-1 8/5/2008 ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA 8.71
MW-2 8/5/2008 ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA 8.44
MW-3 8/5/2008 ND ND 7.7 1.6 12.9 ND 5.3 6 SS7 202 ND 159 ND 2.9 ND 66.5 ND ND ND 237 4.5 4.21
MW-4 8/5/2008 ND ND 4.3 1.9 ND ND 3.7 ND NA NA NA NA NA NA NA NA NA NA NA NA NA 7.87
MW-5 8/5/2008 ND 1.6 ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA 8.46
MW-6 8/5/2008 ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA 9.17
MW-7 8/5/2008 ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA 3.64
MW-8 8/5/2008 ND ND ND ND ND ND ND ND 2500 111 ND 76.1 ND 3.6 ND ND ND ND ND 225 J 4.85 2.75
MW-9 8/5/2008 ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA 8.61
MW-10 8/5/2008 ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA UA NA NA NA 8.56
MW-11 8/5/2008 ND ND ND ND 4.9 ND 1.5 15.5 633 36.4 ND 20.4 ND 1.6 ND 19.5 ND ND ND 212 5.04 5.8
MW-12 8/5/2008 ND ND 4.6 ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA 8.45
MW-13 8/5/2008 ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA 8.4
MW-14 8/5/2008 ND ND 2.9 ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA 7.24
MW-15 8/5/2008 ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA 5.22
MW-16D 8/5/2008 1.1 ND 3 ND ND ND ND 1.5 NA NA NA NA NA NA NA NA NA NA NA NA NA 5.85
units ug/L ug/L ug/L ug/L ugfl ug/L uga. ugflL n?/L upO. ufJL ugA. mf/L mg/L mRfL mg/L ug/l ug/1 ugrt mV — mg/L
2L Standard (ug/1) 2.8 200 0.7 NS 70 280 70 70 300 50 300 50 NS 10 NS 250 NS NS NS NS NS NS
Results in ug/L =micrograms per liter or mg/L miligrams per Uter
GCL =NCDENR gross contamination level
NCDENR 2L Standard= 15 A NCAC 2L Groundwater Standards
NA = Not Analyzed
NS = No Standard
ND= Not detected above the method detection limit specified in die laboratory report.
Bold type shows constituents above the 2L Standards
Bold italic type shows constituents above die GCL Standards
mV= miUivolts j
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Table 3
Summary of Historical Sampling Results
PSNC Energy
433 Drake Street
Statesville, Iredell County, North Carolina
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MW-1 11/7/2000 3.7 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 MW-1
9/21/2001 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-1
11/25/2002 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-1
7/12/2004 <3.0 2.8 3.3 <5.0 <1.0 <1.0 <1.0 <1.0
MW-1
2/28/2006 1.6 0.83 1.9 0.39 <1.0 <1.0 <1.0 <1.0
MW-1
8/5/2008 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0
MW-2 11/7/2000 <3.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 MW-2
9/21/2001 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-2
7/12/2004 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-2
2/28/2006 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-2
8/5/2008 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0
MW-3 11/7/2000 <3.0 7.3 NA 16 <1.0 16 40 74 MW-3
9/21/2001 <3.0 7.9 <1.0 32 <1.0 16 39 93
MW-3
11/25/2002 <3.0 5.1 <1.0 46 <1.0 13 25 56
MW-3
7/12/2004 <3.0 • 1.4 <1.0 18 <1.0 3.4 6.4 12
MW-3
2/28/2006 <3.0 1 <1.0 8.7 <1.0 1.8 5.9 11
MW-3
8/5/2008 <1.0 <1.0 <1.0 7.7 NA 1.6 5.3 12.9
MW-4 11/7/2000 <3.0 4.2 NA 14 <1.0 9.3 18 28 MW-4
9/21/2001 <3.0 4 <1.0 15 <1.0 11 22 39
MW-4
7/13/2004 <3.0 1.8 <1.0 7.4 <1.0 5.1 9.3 15
MW-4
2/28/2006 <3.0 1.5 <1.0 5.8 <1.0 4.1 6.7 9.1
MW-4
8/5/2008 <1.0 <1.0 <1.0 4.3 NA 1.9 3.7 7.5
MW-5 11/7/2000 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 MW-5
9/21/2001 <1.0 <1.0 17 <1.0 <1.0 <1.0 <1.0 <1.0
MW-5
11/25/2002 <1.0 <1.0 66 <1.0 <1.0 <1.0 <1.0 <1.0
MW-5
7/13/2004 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-5
2/28/2006 <1.0 <1.0 0.51 <1.0 <1.0 <1.0 <1.0 <1.0
MW-5
8/5/2008 1.6 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0
MW-6 9/21/2001 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 MW-6
7/13/2004 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-6
2/28/2006 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-6
8/5/2008 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0
MW-7 9/21/2001 <3.0 1.4 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 MW-7
11/25/2002 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-7
7/13/2004 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-7
2/28/2006 <3.0 0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-7
8/5/2008 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0
MW-8 9/21/2001 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 MW-8
11/25/2002 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-8
7/13/2004 <3.0 <1.0 <1.0 1.1 <1.0 <1.0 <1.0 <1.0
2LStar dard (ug/1) 1 530 2.8 200 0.7 0.269 7 70 70 1
Results in ug/L =micrograms per liter
NCDENR 2L Standard= 15 A NCAC 2L Groundwater Standards
NA = Not Analyzed
8/5/08 sampling event conducted by Shield Engineering. Sampled by others on otiier dates.
Bold type shows constituents above the 2L Standards
H:\Projects\2008\1080186 PSNC Statesville\TABLES\GWANAL
Table 3 (continued)
Summary of Historical Sampling Results
PSNC Statesville
433 Drake Street
Statesville, Iredell County, North Carolina
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MW-8 MW-8 2/28/2006 <3.0 <1.0 <1.0 1.3 <1.0 <1.0 <1.0 <1.0 MW-8
8/5/2008 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0
MW-9 9/21/2001 <3.0 <1.0 . <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 MW-9
7/13/2004 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-9
2/28/2006 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-9
8/5/2008 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0
MW-10 9/21/2001 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 MW-10
11/25/2002 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-10
7/13/2004 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-10
2/28/2006 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-10
8/5/2008 <1,0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0
MW-11 9/21/2001 <3.0 3.2 <1.0 8.6 <1.0 5.7 16 84 MW-11
11/25/2002 <3.0 1.9 <1.0 4 <1.0 2.3 8.6 30
MW-11
7/13/2004 <3.0 1.4 <1.0 5 <1.0 1.2 5 14
MW-11
2/28/2006 <3.0 1 <1.0 1.9 <1.0 0,86 2.6 5.6
MW-11
8/5/2008 <1.0 <1.0 <1.0 <1.0 NA <1.0 1.5 4.9
MW-12 11/25/2002 <3.0 <1.0 <1.0 7 <1.0 <1.0 . <1.0 <1.0 MW-12
7/13/2004 <3.0 <1.0 <1.0 5.4 <1.0 <1.0 <1.0 <1.0
MW-12
2/28/2006 <3.0 <1.0 <1.0 5.2 <1.0 <1.0 <1.0 <1.0
MW-12
8/5/2008 4.6 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0
MW-13 11/25/2002 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 MW-13
7/13/2004 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-13
3/1/2006 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-13
8/5/2008 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0
MW-14 11/25/2002 <3.0 <1.0 <1.0 1.6 <1.0 <1.0 <1.0 <1.0 MW-14
7/12/2004 <3.0 <1.0 <1.0 2.1 <1.0 <1.0 <1.0 <1.0
MW-14
2/28/2006 <3.0 <1.0 <1.0 1.7 <1.0 <1.0 <1.0 <1.0
MW-14
8/5/2008 <1.0 <1.0 <1.0 2.9 NA <1.0 <1.0 <1.0
MW-15 11/25/2002 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 MW-15
7/12/2004 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-15
2/28/2006 <3.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
MW-15
8/5/2008 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0
MW-16D 11/25/2002 <3.0 3.5 <1.0 1.8 4.4 <1.0 <1.0 <1.0 MW-16D
7/12/2004 <3.0 1.5 <1.0 1.1 1.8 <1.0 <1.0 <1.0
MW-16D
2/28/2006 <3.0 1.4 <1.0 2.8 0.87 <1.0 <1.0 <1.0
MW-16D
8/5/2008 <3.0 1.1 <1.0 <1.0 NA <1.0 <1.0 <1.0
2L Standard (ug/1) 530 2.8 200 0.7 0.269 7 70 70
Results in ug/L =micrograms per liter
NCDENR 2L Standard= 15 A NCAC 2L Groundwater Standards
NA = Not Analyzed
8/5/08 sampling event conducted by Shield Engineering. Sampled by odiers on other dates.
Bold type shows constituents above the 2L Standards
H:\Pro]ects\2008\1080186 PSNC Statesville\TABLES\GWANAL
lii
a
iZ
LO Q.
>o
00
i
o
00
s
CN
LEGEND
I — %—
(ft)
(55.39)
(Nl)
MONITORING WELL LOCATION BY OTHERS
MONITORING WELL LOCATION INSTALLED /SAMPLED BY TFI CONSULTANT
CHAIN LINK FENCE
CONCRETE AREAS
FEET
RELATIVE GROUNDWATER ELEVATION (ft)
RELATIVE GROUNDWATER ELEVATION CONTOUR LINE (ft)
RELATIVE GROUNDWATER FLOW DIRECTION
NOT INCLUDED
NOTES:
1. DEPTHS TO GROUNDWATER MEASURED ON 08/05/08.
2. CONTOUR INTERVALS = 1 FOOT.
3. SITE INFORMATION FROM TBE GROUP SITE PLAN 2 DATED JULY 2006.
4. ALL LOCATIONS ARE APPROXIMATE.
GROUNDWATER ELEVATION CONTOUR MAP
FORMER PSNC ENERGY FACILITY
433 DRAKE STREET
STATESVILLE, NORTH CAROLINA
SHIELD #1080186-01
DATE: 09/10/08
SCALE: AS SHOWN
DRAWN BY: RBS
FIGURE : 1
O
iZ
C3
I
u z
i
5
§
§
O
Ol D.
LEGEND
(ug/L)
(7.7)
(ND)
MONITORING WELL LOCATION BY OTHERS
MONITORING WELL LOCATION INSTALLED BY TFI CONSULTANT -NOT SAMPLED
DURING THIS SAMPLING EVENT
CHAIN LINK FENCE
CONCRETE AREAS
MICROGRAMS PER LITER
TETRACHLOROETHENE CONCENTRATION (ug/L)
TETRACHLOROETHENE ISOCONCENTRATION LINE (ug/L)
NOT DETECTED AT OR ABOVE UBORATORY TEXT METHOD DETECTION LIMIT
NOTES:
1. GROUNDWATER SAMPLES COLLECTED ON 08/05/08.
2. CONTOUR INTERVALS = AS SHOWN.
3. SITE INFORMATION FROM TBE GROUP SITE PL^N 2 DATED JULY 2006.
4. ALL LOCATIONS ARE APPROXIMATE.
TETRACHLOROETHENE
ISOCONCENTRATION MAP
FORMER PSNC ENERGY FACILITY
433 DRAKE STREET
STATESVILLE, NORTH CAROLINA
SHIELD #1080186-01
DATE 09/10/08
SCALE : AS SHOWN
DRAWN BY : RBS
FIGURE
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
August 19, 2008
Mr. Tom Witner
Shield Engineering
4301 Taggart Creek Road
Charlotte, NC 28208
RE: Project; PSNC 1080186-01
Pace Project No.: 9224817
Dear Mr. Witner:
Enclosed are the analytical results for sample(s) received by the laboratory on August 05, 2008. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body ofthe
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
k.?[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS Page 1 of 48
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without the written consent of Pace Analytical Services, Inc..
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[phone]
Pace Analytical Services, Inc.
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[phone]
CERTIFICATIONS
Project:
Pace Project No.:
PSNC 1080186-01
9224817
Charlotte Certification IDs
Connecticut Certification Number: PH-0104
Pennsylvania Certification Number: 68-00784
West Virginia Certification Number; 357
Virginia Certification Number: 00213
Tennessee Certification Number: 04010
South Carolina Bioassay Certification Number: 990060003
South Carolina Certification Number: 990060001
North Carolina Field Services Certification Number: 5342
North Carolina Wastewater Certification Number: 12
North Carolina Drinking Water Certification Number: 37706
Louislana/LELAP Certification Number; 04034
Kentucky UST Certification Number: 34
New/ Jersey Certification Number: NC012
Florida/NELAP Certification Number: E87627
Asheville Certification IDs
Connecticut Certification Number: PH-0106
Massachusetts Certification Number: M-NC030
West Virginia Certification Number: 356
Virginia Certification Number: 00072
Tennessee Certification Number: 2980
South Carolina Bioassay Certification Number: 99030002
South Carolina Certification Number: 99030001
Pennsylvania Certification Number; 68-03578
North Carolina Bioassay Certification Number: 9
North Carolina Wastew/ater Certification Number: 40
North Carolina Drinking Water Certification Number; 37712
Nev7 Jersey Certification Number: NC011
Louislana/LELAP Certification Number; 03095
Florida/NELAP Certification Number: E87648
Eden Certification IDs
Virginia Drinking Water Certification Number: 00424
North Carolina Wastevirater Certification Number; 633
North Carolina Drinking Water Certification Number: 37738
REPORT OF LABORATORY ANALYSIS Page 2 of 48
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[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-1
Parameters
Lab ID: 9224817001 Collected: 08/05/0811:55 Received: 08/05/08 13:25 (Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Brpmochloromethane
Bromodichloromethane
Bromofomi
Bromomethane
2-ButanQne (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1.2- Dichlorobenzene
1.3- Dichlorobenzene
1.4- Dichlorobenzene
Dichlorodifluoromethane
1.1- Dichloroethane
1.2- Dlchloroethane
1.1- Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dlchloroethene
1.2- Dichloropropane
1.3- Dichloropropane
2,2-Dichloropropane
1,1-Dlchloropropene
cis-1,3-Dichloropropene
lrans-1,3-Dichloropropene
Dllsopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-lsopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Date: 08/19/2008 08:25 AM
Analytical Method: EPA 8260
ND ug/L 25.0 1 08/09/08 06:45 67-64-1
ND ug/L 1.0 1 08/09/08 06:45 71-43-2
ND ug/L 1.0 1 08/09/08 06.45 108-86-1
ND ug/L 1.0 1 08/09/08 06:45 74-97-5
ND ug/L 1.0 1 08/09/08 06:45 75-27-4
ND ug/L 1.0 1 08/09/08 06:45 75-25-2
ND ug/L 5.0 1 08/09/08 06:45 74-83-9
ND ug/L 5.0 1 08/09/08 06:45 78-93-3
ND ug/L 1.0 1 08/09/08 06:45 56-23-5
ND ug/L 1.0 1 08/09/08 06:45 108-90-7
ND ug/L 1.0 1 08/09/08 06:45 75-00-3
ND ug/L 1.0 1 08/09/08 06:45 67-66-3
ND ug/L 1.0 1 08/09/08 06:45 74-87-3
ND ug/L 1.0 1 08/09/08 06:45 95-49-8
ND ug/L 1.0 1 08/09/08 06:45 106^3-4
ND ug/L 3.0 1 08/09/08 06:45 96-12-8
ND ug/L 1.0 1 08/09/08 06:45 124-48-1
ND ug/L 1.0 1 08/09/08 06:45 106-93-4
ND ug/L 1.0 1 08/09/08 06:45 74-95-3
ND ug/L 1.0 1 08/09/08 06:45 95-50-1
ND ug/L 1.0 1 08/09/08 06:45 541-73-1
ND ug/L 1.0 1 08/09/08 06:45 106-46-7
ND ug/L 1.0 1 08/09/08 06:45 75-71-8
ND ug/L 1.0 1 08/09/08 06:45 75-34-3
ND ug/L 1.0 1 08/09/08 06:45 107-06-2
ND ug/L 1.0 1 08/09/08 06:45 75-35-4
ND ug/L 1.0 1 08/09/08 06:45 156-59-2
ND ug/L 1.0 1 08/09/08 06:45 156-60-5
ND ug/L 1.0 1 08/09/08 06:45 78-87-5
ND ug/L 1.0 1 08/09/08 06:45 142-28-9
ND ug/L 1.0 1 08/09/08 06:45 594-20-7
ND ug/L 1.0 1 08/09/08 06:45 563-58-6
ND ug/L 1.0 1 08/09/08 06:45 10061-01-5
ND ug/L 1.0 1 08/09/08 06:45 10061-02-6
ND ug/L 1.0 1 08/09/08 06:45 108-20-3
ND ug/L 1.0 1 08/09/08 06.45 100-41-4
ND ug/L 1.0 1 08/09/08 06:45 87-68-3
ND ug/L 5.0 1 08/09/08 06:45 591-78-6
ND ug/L 1.0 1 08/09/08 06:45 99-87-6
ND ug/L 2.0 1 08/09/08 06:45 75-09-2
ND ug/L 5.0 1 08/09/08 06:45 108-10-1
ND ug/L 1.0 1 08/09/08 06:45 1634-04-4
ND ug/L 1.0 1 08/09/08 06:45 91-20-3
ND ug/L 1.0 1 08/09/08 06:45 100-42-5
ND ug/L 1.0 1 08/09/08 06:45 630-20-6
ND ug/L 1.0 1 08/09/08 06:45 79-34-5
ND ug/L 1.0 1 08/09/08 06:45 127-18-4
REPORT OF LABORATORY ANALYSIS Page 3 of 48
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
^ace Analytical
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Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-1
Parameters
Lab ID: 9224817001 Collected: 08/06/0811:55 Received: 08/05/08 13:25 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Levy Level Analytical Method: EPA 8260
Toluene ND ug/L 1.0 1 08/09/08 06:45 108-88-3
1,2,3-Trichlorobenzene ND ug/L 1.0 1 08/09/08 06:45 87-61-6
1,2,4-Trichlorobenzene ND ug/L 1.0 1 08/09/08 06:45 120-82-1
1,1,1-Trichloroethane ND ug/L 1.0 1 08/09/08 06:45 71-55-6
1,1,2-Trichloroethane ND ug/L 1.0 1 08/09/08 06:45 79-00-5
Trichloroethene ND ug/L 1.0 1 08/09/08 06:45 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 08/09/08 06:45 75-69-4
1,2,3-Trichloropropane ND ug/L 1.0 1 08/09/08 06:45 96-18-4
Vinyl acetate ND ug/L 2.0 1 08/09/08 06:45 108-05-4
Vinyl chloride ND ug/L 1.0 1 08/09/08 06:45 75-01-4
m&p-Xylene ND ug/L 2.0 1 08/09/08 06:45 1330-20-7
o-Xylene ND ug/L 1.0 1 08/09/08 06:45 95-47-6
4-Bromofluorobenzene (S) 99 % 87-109 1 08/09/08 06:45 460-00-4
Dlbromofluoromethane (S) 98 % 85-115 1 08/09/08 06:45 1868-53-7
1,2-Dichloroelhane-d4 (S) 98 % 79-120 1 08/09/08 06:45 17060-07-0
Toluene-d8 (S) 99 % 70-120 1 08/09/08 06:45 2037-26-5
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Sen/ices, Inc..
Page 4 of 48
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Pace Analytical Services, Inc.
2225 Riverside Dr.
Asiieville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-2 Lab ID: 9224817002 Collected: 08/05/08 11.45 Received: 08/05/08 13:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 25.0 1 08/09/08 07:08 67-64-1
Benzene ND ug/L 1.0 1 08/09/08 07:08 71-43-2
Bromobenzene . ND ug/L 1.0 1 08/09/08 07:08 108-86-1
Bromoctiloromettiane ND ug/L 1.0 1 08/09/08 07:08 74-97-5
Bromodichloromethane ND ug/L 1.0 1 08/09/08 07:08 75-27-4
Bromoform ND ug/L 1.0 1 08/09/08 07:08 75-25-2
Bromomethane ND ug/L 5.0 1 08/09/08 07:08 74-83-9
2-Butanone (MEK) ND ug/L 5.0 1 08/09/08 07:08 78-93-3
Carbon tetrachloride ND ug/L 1.0 1 08/09/08 07:08 56-23-5
Chlorobenzene ND ug/L 1.0 1 08/09/08 07:08 108-90-7
Chloroettiane ND ug/L 1.0 1 08/09/08 07:08 75-00-3
Chloroform ND ug/L 1.0 1 08/09/08 07:08 67-66-3
Chlorornethane ND ug/L 1.0 1 08/09/08 07:08 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 08/09/08 07:08 95-49-8
4-Chlorotoluene ND ug/L 1.0 1 08/09/08 07:08 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 3.0 1 08/09/08 07:08 96-12-8
Dibromochloromethane ND ug/L 1.0 1 08/09/08 07:08 124-48-1
1,2-Dlbromoethane (EDB) ND ug/L 1.0 1 08/09/08 07:08 106-93-4
Dibromomethane ND ug/L 1.0 1 08/09/08 07:08 74-95-3
1,2-Dichlorobenzene ND ug/L 1.0 1 08/09/08 07:08 95-50-1
1,3-Dlchlorobenzene ND ug/L 1.0 1 08/09/08 07:08 541-73-1
1,4-Dlchlorobenzene ND ug/L 1.0 1 08/09/08 07:08 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 08/09/08 07:08 75-71-8
1,1-Dichloroethane ND ug/L 1.0 1 08/09/08 07:08 75-34-3
1,2-Dichloroethane ND ug/L 1.0 1 08/09/08 07:08 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 08/09/08 07:08 75-35-4
cis-1,2-Dichloroelhene ND ug/L 1.0 1 08/09/08 07:08 156-59-2
trans-1,2-Dlchloroethene ND ug/L 1.0 1 08/09/08 07:08 156-60-5
1,2-Dlchloropropane ND ug/L 1.0 1 08/09/08 07:08 78-87-5
1,3-Dictiloropropane ND ug/L 1.0 1 08/09/08 07:08 142-28-9
2,2-Dichloropropane ND ug/L 1.0 1 08/09/08 07:08 594-20-7
1,1.-DichlproRropene ND ug/L 1.0 1 08/09/08 07:08 563-58-6
cis-1,3-Dichloropropene ND ug/L 1.0 1 08/09/08 07:08 10061-01-5
trans-1,3-Dichloropropene ND ug/L 1.0 1 08/09/08 07:08 10061-02-6
Dllsopropyl ether ND ug/L 1.0 1 08/09/08 07:08 108-20-3
Ethylbenzene ND ug/L 1.0 1 08/09/08 07:08 100-41-4
Hexachloro-1,3-butadiene ND ug/L 1.0 1 08/09/08 07:08 87-68-3
2-Hexanone ND ug/L 5.0 1 08/09/08 07:08 591-78-6
p-lsopropyltoluene ND ug/L 1.0 1 08/09/08 07:08 99-87-6
Methylene Chloride ND ug/L 2.0 1 08/09/08 07:08 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 08/09/08 07:08 108-10-1
Methyl-tert-butyl ether ND ug/L 1.0 1 08/09/08 07:08 1634-04-4
Naphthalene ND ug/L 1.0 1 08/09/08 07:08 91-20-3
Styrene ND ug/L 1.0 1 08/09/08 07:08 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 07:08 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 07:08 79-34-5
Tetrachloroethene ND ug/L 1.0 1 08/09/08 07:08 127-18-4
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc.
Page 5 of 4£
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Pace Analytical Services, Inc.
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Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project; PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-2
Parameters
8260 MSV Low Level
Lab ID: 9224817002 Collected: 08/05/08 11:45 Received: 08/05/08 13:25 Matrix; Water
Results Units Report Limit DF Prepared Analyzed CAS No.
Analytical Method; EPA 8260
Toluene ND ug/L 1.0 1 08/09/08 07:08 108-88-3
1,2,3-Trichlorobenzene ND ug/L 1.0 1 08/09/08 07:08 87-61-6
1,2,4-Trichlprobenzene ND ug/L 1.0 1 08/09/08 07:08 120-82-1
1,1,1-Trichloroelhane ND ug/L 1.0 1 08/09/08 07:08 71-55-6
1,1,2-Trichloroethane ND ug/L 1.0 1 08/09/08 07:08 79-00-5
Trichloroethene ND ug/L 1.0 1 08/09/08 07:08 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 08/09/08 07:08 75-69-4
1,2,3-Trichloropropane ND ug/L 1.0 1 08/09/08 07:08 96-18-4
Vinyl acetate ND ug/L 2.0 1 08/09/08 07:08 108-05-4
Vinyl chloride ND ug/L 1.0 1 08/09/08 07:08 75-01-4
m&p-Xylene ND ug/L 2.0 1 08/09/08 07:08 1330-20-7
o-Xylene ND ug/L 1.0 1 08/09/08 07:08 95-47-6
4-Bromofluorobenzene (S) 98 % 87-109 1 08/09/08 07:08 460-00-4
Dibromofluoromethane (S) 97 % 85-115 1 08/09/08 07:08 1868-53-7
1,2-Dichloroethane-d4 (S) 100 % 79-120 1 08/09/08 07:08 17060-07-0
Toluene-d8 (S) 99 % 70-120 1 08/09/08 07:08 2037-26-5
Qual
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written conisent of Pace Analytical Services, Inc..
Page 6 of 48
mAnalyticar
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Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-4 Lab ID: 9224817003 Collected: 08/05/0811:45 Received: 08/05/0813:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 25.0 1 08/09/08 07:32 67-64-1
Benzene ND ug/L 1.0 1 08/09/08 07:32 71-43-2
Brom6t)enzene ND ug/L 1.0 1 08/09/08 07:32 108-86-1
Bromochloromethane ND ug/L 1.0 1 08/09/08 07:32 74-97-5
Bromodichloromethane ND ug/L 1.0 1 08/09/08 07:32 75-27-4
Bromoform ND ug/L 1.0 1 08/09/08 07:32 75-25-2
Bromomethane ND ug/L 5.0 1 08/09/08 07:32 74-83-9
2-Butanone (MEK) ND ug/L 5.0 1 08/09/08 07:32 78-93-3
Carbon tetrachloride ND ug/L 1.0 1 08/09/08 07:32 56-23-5
Chlorobenzene ND ug/L 1.0 1 08/09/08 07:32 108-90-7
Chloroethane ND ug/L 1.0 1 08/09/08 07:32 75-00-3
Chloroform ND ug/L 1.0 1 08/09/08 07:32 67-66-3
Chloromethane ND ug/L 1.0 1 08/09/08 07:32 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 08/09/08 07:32 95-49-8
4-Chlorotoluene ND ug/L 1.0 1 08/09/08 07:32 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 3.0 1 08/09/08 07:32 96-12-8
Dibromochloromethane ND ug/L 1.0 1 08/09/08 07:32 124-48-1
1,2-Dibromoethane (EDB) ND ug/L 1.0 1 08/09/08 07:32 106-93-4
Dibromomethane ND ug/L 1.0 1 08/09/08 07:32 74-95-3
1,2-Dichlorobenzene ND ug/L 1.0 1 08/09/08 07:32 95-50-1
1,3-Dichlorobenzene ND ug/L 1.0 1 08/09/08 07:32 541-73-1
1,4-Dichlorobenzene ND ug/L 1.0 1 08/09/08 07:32 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 08/09/08 07:32 75-71-8
1,1-Dichloroethane 7.5 ug/L 1.0 1 08/09/08 07:32 75-34-3
1,2-Dichloroethane ND ug/L 1.0 1 08/09/08 07:32 107-06-2
1,1-Dichloroethene 1.9 ug/L 1.0 1 08/09/08 07:32 75-35-4
cls-1,2-Dichloroethene 3.7 ug/L 1.0 1 08/09/08 07:32 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.0 1 08/09/08 07:32 156-60-5
1,2-Dlchloropropane ND ug/L 1.0 1 08/09/08 07:32 78-87-5
1,3-Dichloropropane ND ug/L 1.0 1 08/09/08 07:32 142-28-9
2,2-Dlchloropropane ND ug/L 1.0 1 08/09/08 07:32 594-20-7
1,1-Dichloropropene ND ug/L 1.0 1 08/09/08 07:32 563-58-6
cis-1,3-Dichrorbpro|3ene ND ug/L 1.0 1 08/09/08 07:32 10061 -01 -5
trans-1,3-Dichloropropene ND ug/L 1.0 1 08/09/08 07:32 10061-02-6
Diisopropyl ether ND ug/L 1.0 1 08/09/08 07:32 108-20-3
Ethylbenzene ND ug/L 1.0 1 08/09/08 07:32 100-41-4
Hexachloro-1,3-butadiene ND ug/L 1.0 1 08/09/08 07:32 87-68-3
2-Hexanone ND ug/L 5.0 1 08/09/08 07:32 591-78-6
p-lsopropylloluene ND ug/L 1.0 1 08/09/08 07:32 99-87-6
Methylene Chloride ND ug/L 2.0 1 08/09/08 07:32 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 08/09/08 07:32 108-10-1
Methyl-tert-butyl ether ND ug/L 1.0 1 08/09/08 07:32 1634-04-4
Naphthalene ND ug/L 1.0 1 08/09/08 07:32 91-20-3
Styrene ND ug/L 1.0 1 08/09/08 07:32 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 07:32 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 07:32 79-34-5
Tetrachloroethene 4.3 ug/L 1.0 1 08/09/08 07:32 127-18-4
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 7 of 48
This report stiall not be reproduced, except In full,
witiiout ttie written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asiieville, NC 28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
^Analytical
www.pacelabsMn)
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheviiie, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-4 Lab ID: 9224817003 Collected: 08/05/08 11:45 Received: 08/05/08 13:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1.0 1 08/09/08 07:32 108-88-3
1,2,3-Trichlorobenzene ND ug/L 1.0 1 08/09/08 07:32 87-61-6
1,2,4-Trichlorobenzene ND ug/L 1.0 1 08/09/08 07:32 120-82-1
1,1,1-Trichloroethane ND ug/L 1.0 1 08/09/08 07:32 71-55-6
1,1,2-Trichloroethane ND ug/L 1.0 1 08/09/08 07:32 79-00-5
Trichloroethene ND ug/L 1.0 1 08/09/08 07:32 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 08/09/08 07:32 75-69-4
1,2,3-Trichloropropane ND ug/L 1.0 1 08/09/08 07:32 96-18-4
Vinyl acetate ND ug/L 2.0 1 08/09/08 07:32 108-05-4
Vinyl chloride ND ug/L 1.0 1 08/09/08 07:32 75-01-4
m&p-Xylene ND ug/L 2.0 1 08/09/08 07:32 1330720-7
o-Xylene ND ug/L 1.0 1 08/09/08 07:32 95-47-6
4-Bromofluorobenzene (S) 98 % 87-109 1 08/09/08 07:32 460-00-4
Dibromofluoromethane (S) 97 % 85-115 1 08/09/08 07:32 1868-53-7
1,2-Dichloroethane-d4 (S) 100 % 79-120 1 08/09/08 07:32 17060-07-0
Toluene-d8 (S) 99 % 70-120 1 08/09/08 07:32 2037-26-5
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 8 of 48
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc.,
mAnalytical
ivww.p8cete6s.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asiieviiie, NC 28804
[phone]
Pace Analytical Services, inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-S Lab ID: 9224817004 Collected: 08/05/0810:50 Received: 08/05/08 13:25 Matrix; Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method; EPA 8260
Acetone ND ug/L 25.0 1 08/09/08 07:56 67-64-1
Benzene ND ug/L 1.0 1 08/09/08 07:56 71-43-2
Bromobenzene ND ug/L 1.0 .1 08/09/08 07:56 108-86-1
BroTTiochloromethane ND ug/L 1.0 1 08/09/08 07:56 74-97-5
Brorfiodlchloromethane ND ug/L 1.0 1 08/09/08 07:56 75-27-4
Bromoform ND ug/L 1.0 1 08/09/08 07:56 75-25-2
Bromomethane ND ug/L 5.0 1 08/09/08 07:56 74-83-9
2-Butanone (MEK) ND ug/L 5.0 1 08/09/08 07:56 78-93-3
Carbon tetrachloride ND ug/L 1.0 1 08/09/08 07:56 56-23-5
Chlorobenzene ND ug/L 1.0 1 08/09/08 07:56 108-90-7
Chloroethane ND ug/L 1.0 1 08/09/08 07:56 75-00-3
Chloroform ND ug/L 1.0 1 08/09/08 07:56 67-66-3
Chloromethane ND ug/L 1.0 1 08/09/08 07:56 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 08/09/08 07:56 95-49-8
4-Chlorotoluene ND ug/L 1.0 1 08/09/08 07:56 106-43-4
1,2-Dlbromo-3-chloropropane ND ug/L 3.0 1 08/09/08 07:56 96-12-8
DIbromochJoromethane ND ug/L 1.0 1 08/09/08 07:56 124-48-1
1,2-Dibromoethane (EDB) ND ug/L 1.0 1 08/09/08 07:56 106-93-4
Dibromomethane ND ug/L 1.0 1 08/09/08 07:56 74-95-3
1,2-Dlchlorobenzene ND ug/L 1.0 1 08/09/08 07:56 95-50-1
1,3-Dlchlorobenzene ND ug/L 1.0 1 08/09/08 07:56 541-73-1
1,4-Dichlorobenzene ND ug/L 1.0 1 08/09/08 07:56 106^6-7
Dichlorodifluoromethane ND ug/L 1.0 1 08/09/08 07:56 75-71-8
1,1-Dichloroethane ND ug/L 1.0 1 08/09/08 07:56 75-34-3
1,2-Dlchloroethane ND ug/L 1.0 1 08/09/08 07:56 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 08/09/08 07:56 75-35-4
cis-1,2-Dichloroethene ND ug/L 1.0 1 08/09/08 07:56 156-59-2
trans-1,2-Dlchloroethene ND ug/L 1.0 1 08/09/08 07:56 156-60-5
1,2-Dlchloropropane ND ug/L 1.0 1 08/09/08 07:56 78-87-5
1,3-Dichloropropane ND ug/L 1.0 1 08/09/08 07:56 142-28-9
2,2-Dichloropropane ND ug/L 1.0 1 08/09/08 07:56 594-20-7
1,1-Dichloropropene ND ug/L 1.0 1 08/09/08 07:56 563-58-6
cis-1,3-Dlchloropropene ND ug/L 1.0 1 08/09/08 07:56 10061-01-5
trans-1,3-Dichloropropene ND ug/L 1.0 1 08/09/08 07:56 10061-02-6
Diisopropyl ether ND ug/L 1.0 1 08/09/08 07:56 108-20-3
Ethylbenzene ND ug/L 1.0 1 08/09/08 07:56 100-41-4
Hexachloro-1,3-butadiene ND ug/L 1.0 1 08/09/08 07:56 87-68-3
2-Hexanone ND ug/L 5.0 1 08/09/08 07:56 591-78-6
p-lsopropyltoluene ND ug/L 1.0 1 08/09/08 07:56 99-87-6
Methylene Chloride ND ug/L 2.0 1 08/09/08 07:56 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 08/09/08 07:56 108-10-1
Methyl-tert-butyl ether 1.6 ug/L 1.0 1 08/09/08 07:56 1634-04-4
Naphthalene ND ug/L 1.0 1 08/09/08 07:56 91-20-3
Styrene ND ug/L 1.0 1 08/09/08 07:56 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 07:56 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 07:56 79-34-5
Tetrachloroethene ND ug/L 1.0 1 08/09/08 07:56 127-18-4
Date; 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 9 of 48
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
'^ace Analytical
www.p»c9l$bs.eofH
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asiieville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-5 Lab ID: 9224817004 Collected: 08/05/08 10:50 Received: 08/05/08 13:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1.0 1 08/09/08 07:56 108-88-3
1,2,3-Trichlorobenzene ND ug/L 1.0 1 08/09/08 07:56 87-61-6
1,2,4-Trichlorobenzene ND ug/L 1.0 1 08/09/08 07:56 120-82-1
1,1,1-Trichloroethane ND ug/L 1.0 1 08/09/08 07:56 71-55-6
1,1,2-Trichloroethane ND ug/L 1.0 1 08/09/08 07:56 79-00-5
Trichloroethene ND ug/L 1.0 1 08/09/08 07:56 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 08/09/08 07:56 75-69-4
1,2,3-Trichloropropane ND ug/L 1.0 1 08/09/08 07:56 96-18-4
Vinyl acetate ND ug/L 2.0 1 08/09/08 07:56 108-05-4
Vinyl chloride ND ug/L 1.0 1 08/09/08 07:56 75-01-4
m&p-Xylene ND ug/L 2.0 1 08/09/08 07:56 1330-20-7
o-Xylene ND ug/L 1.0 1 08/09/08 07:56 95-47-6
4-Bromofluorobenzene (S) 98 % 87-109 1 08/09/08 07:56 460-00-4
Dibromofluoromethane (S) 97 % 85-115 1 08/09/08 07:56 1868-53-7
1,2-Dlchloroethane-d4 (S) 101 % 79-120 1 08/09/08 07:56 17060-07-0
Toluene-d8 (S) 99 % 70-120 1 08/09/08 07:56 2037-26-5
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
wilhout the written consent of Pace Analytical Services, inc..
Page 10 of 48
^ace Analytical
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Pace Analyticai Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No,: 9224817
Sample: MW-6
Parameters
Lab ID: 9224817005 Collected: 08/05/08 11:15
Results Units Report Limit DF
Received:
Prepared
08/05/08 13:25 Matrix: Water
Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 25.0 1 08/09/08 08:19 67-64-1
Benzene ND ug/L 1.0 1 08/09/08 08:19 71-43-2
Bromobenzene ND ug/L 1.0 1 08/09/08 08:19 108-86-1
Bromochloromethane ND ug/L 1.0 1 08/09/08 08:19 74-97-5
Bromodichloromethane ND ug/L 1.0 1 08/09/08 08:19 75-27-4
Bromoform ND ug/L 1.0 1 08/09/08 08:19 75-25-2
Bromomethane ND ug/L 5.0 1 08/09/08 08:19 74-83-9
2-Butanone (MEK) ND ug/L 5.0 1 08/09/08 08:19 78-93-3
Carbon tetrachloride ND ug/L 1.0 1 08/09/08 08:19 56-23-5
Chlorobenzene ND ug/L 1.0 1 08/09/08 08:19 108-90-7
Chloroethane ND ug/L 1.0 1 08/09/08 08:19 75-00-3
Chloroform ND ug/L 1.0 1 08/09/08 08:19 67-66-3
Chloromethane ND ug/L 1.0 1 08/09/08 08:19 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 08/09/08 08:19 95-49-8
4-Chlorotoluene ND ug/L 1.0 1 08/09/08 08:19 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 3.0 1 08/09/08 08:19 96-12-8
Dibromochloromethane ND ug/L 1.0 1 08/09/08 08:19 124-48-1
1,2-Dibromoethane (EDB) ND ug/L 1.0 1 08/09/08 08:19 106-93-4
Dibromomethane ND ug/L 1.0 1 08/09/08 08:19 74-95-3
1,2-Dlchlorobenzene ND ug/L 1.0 1 08/09/08 08:19 95-50-1
1,3-Dichlorobenzene ND ug/L 1.0 1 08/09/08 08:19 541-73-1
1,4-Dlchlorobenzene ND ug/L 1.0 1 08/09/08 08:19 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 08/09/08 08:19 75-71-8
1,1-Dichloroethane ND ug/L 1.0 1 08/09/08 08:19 75-34-3
1,2-Dlchloroethane ND ug/L 1.0 1 08/09/08 08:19 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 08/09/08 08:19 75-35-4
cls-1,2-Dlchloroethene ND ug/L 1.0 1 08/09/08 08:19 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.0 1 08/09/08 08:19 156-60-5
1,2-Dlchloropropane ND ug/L 1.0 1 08/09/08 08:19 78-87-5
1,3-Dichloropropane ND ug/L 1.0 1 08/09/08 08:19 142-28-9
2,2-Dichloropropane ND ug/L 1.0 1 08/09/08 08:19 594-20-7
1,1-Dlchloropropene ND ug/L 1.0 1 08/09/08 08:19 563-58-6
cis-1,3-Dlchloropropene ND ug/L 1.0 1 08/09/08 08:19 10061-01-5
tr3ns-1,3-Dlchloroprppene ND ug/L 1.0 1 08/09/08 08:19 10061-02-6
Diisopropyl ether ND ug/L 1.0 1 08/09/08 08:19 108-20-3
Ethylbenzene ND ug/L 1.0 1 08/09/08 08:19 100-41-4
Hexachloro-1,3-butadiene ND ug/L 1.0 1 08/09/08 08:19 87-68-3
2-Hexanone ND ug/L 5.0 1 08/09/08 08:19 591-78-6
p-lsopropyltoluene ND ug/L 1.0 1 08/09/08 08:19 99-87-6
Methylene Chloride ND ug/L 2.0 1 08/09/08 08:19 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 08/09/08 08:19 108-10-1
Methyl-tert-butyl ether ND ug/L 1.0 1 08/09/08 08:19 1634-04-4
Naphthalene ND ug/L 1.0 1 08/09/08 08:19 91-20-3
Styrene ND ug/L 1.0 1 08/09/08 08:19 100-42-5
1,1,1,2-Tetrachloroelhane ND ug/L 1.0 1 08/09/08 08:19 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 08:19 79-34-5
Tetrachloroethene ND ug/L 1.0 1 08/09/08 08:19 127-18-4
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 11 of 48
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
^Analytical
tww.pace/66s.(»m
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asiieville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-6 Lab ID: 9224817005 Collected: 08/05/08 11:15 Received: 08/05/08 13:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Metiiod: EPA 8260
Toluene ND ug/L 1.0 1 08/09/08 08:19 108-88-3
1,2,3-Triciilorobenzene ND ug/L 1.0 1 08/09/08 08:19 87-61-6
1,2,4-Trichlorobenzene ND ug/L 1.0 1 08/09/08 08:19 120-82-1
1,1,1-Triohloroethane ND ug/L 1.0 1 08/09/08 08:19 71-55-6
1,1,2-Trichloroethane ND ug/L 1.0 1 08/09/08 08:19 79-00-5
Trichloroethene ND ug/L 1.0 1 08/09/08 08:19 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 08/09/08 08:19 75-69-4
1,2,3-Trichloropropane ND ug/L 1.0 1 08/09/08 08:19 96-18-4
Vinyl acetate ND ug/L 2.0 1 08/09/08 08:19 108-05-4
Vinyl chloride ND ug/L 1.0 1 08/09/08 08:19 75-01-4
m&p-Xylene ND ug/L 2.0 1 08/09/08 08:19 1330-20-7
o-Xylene ND ug/L 1.0 1 08/09/08 08:19 95-47-6
4-Bromofluorobenzene (S) 98 % 87-109 1 08/09/08 08:19 460-00-4
Dibromofluoromethane (S) 97 % 85-115 1 08/09/08 08:19 1868-53-7
1,2-Dlchloroethane-d4 (S) 101 % 79-120 1 08/09/08 08:19 17060-07-0
Toluene-d8 (S) 99 % 70-120 1 08/09/08 08:19 2037-26-5
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
Ttiis report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 48
/^aceAnalytical
I iyvw.paC8te6s,com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asiieville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-7
Parameters
Lab ID: 9224817006 Collected: 08/05/08 09:55 Received: 08/05/08 13:25 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 25.0 1 08/09/08 08:43 67-64-1
Benzene ND ug/L 1.0 1 08/09/08 08:43 71-43-2
Bromotie nzene ND ug/L 1.0 1 08/09/08 08:43 108-86-1
Bromochlorometliane ND ug/L 1.0 1 08/09/08 08:43 74-97-5
Bromodichloromethane ND ug/L 1.0 1 08/09/08 08:43 75-27-4
Bromoform ND ug/L 1.0 1 08/09/08 08:43 75-25-2
Bromomethane ND ug/L 5.0 1 08/09/08 08.43 74-83-9
2-Butanone (MEK) ND ug/L 5.0 1 08/09/08 08:43 78-93-3
Carbon tetrachloride ND ug/L 1.0 1 08/09/08 08:43 56-23-5
Chlorobenzene ND ug/L 1.0 1 08/09/08 08:43 108-90-7
Chloroethane ND ug/L 1.0 1 08/09/08 08:43 75-00-3
Chloroform ND ug/L 1.0 1 08/09/08 08:43 67-66-3
Chloromethane ND ug/L 1.0 1 08/09/08 08:43 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 08/09/08 08:43 95-49-8
4-Chlorotoluene ND ug/L 1.0 1 08/09/08 08:43 106-43-4
1,2-Dlbromo-3-chloropropane ND ug/L 3.0 1 08/09/08 08:43 96-12-8
Dibromochloromethane ND ug/L 1.0 • 1 08/09/08 08:43 124.48-1
1,2-Dlbromoethane (EDB) ND ug/L 1.0 1 08/09/08 08:43 106-93-4
Dibromomethane ND ug/L 1.0 1 08/09/08 08:43 74-95-3
1,2-Dichlorobenzene ND ug/L 1.0 1 08/09/08 08:43 95-50-1
1,3-Dichlorobenzene ND ug/L 1.0 1 08/09/08 08:43 541-73-1
1,4-Dlchlorobenzene ND ug/L 1.0 1 08/09/08 08:43 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 08/09/08 08:43 75-71-8
1,1-Dichloroethane ND ug/L 1.0 1 08/09/08 08:43 75-34-3
1,2-Dlchloroethane ND ug/L 1.0 1 08/09/08 08:43 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 08/09/08 08:43 75-35-4
cis-1,2-Dlchloroethene ND ug/L 1.0 1 08/09/08 08:43 156-59-2
trans-1,2-Dlchloroethene ND ug/L 1.0 1 08/09/08 08:43 156-60-5
1,2-Dlchloropropane ND ug/L 1.0 1 08/09/08 08.43 78-87-5
1,3-Dichloropropane ND ug/L 1.0 1 08/09/08 08:43 142-28-9
2,2-Dichloropropane ND ug/L 1.0 1 08/09/08 08:43 594-20-7
1,1-Dlchloropropene ND ug/L 1.0 1 08/09/08 08:43 563-58-6
cls-1,3-Dlchloropropene ND ug/L 1.0 1 08/09/08 08:43 10061-01-5
.trans-1,3-Dlchloropropene ND ug/L 1.0 1 08/09/08 08:43 10061-02-6
Diisopropyl ether ND ug/L 1.0 1 08/09/08 08:43 108-20-3
Ethylbenzene ND uy/L 1.0 1 08/09/08 08:43 100-41-4
Hexachloro-1,3-butadlene ND ug/L 1.0 1 08/09/08 08:43 87-68-3
2-Hexanone ND ug/L 5.0 1 08/09/08 08:43 591-78-6
p-lsopropyltoluene ND ug/L 1.0 1 08/09/08 08:43 99-87-6
Methylene Chloride ND ug/L 2.0 1 08/09/08 08:43 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 08/09/08 08:43 108-10-1
Methyl-tert-butyl ether ND ug/L 1.0 1 08/09/08 08:43 1634-04-4
Naphthalene ND ug/L 1.0 1 08/09/08 08:43 91-20-3
Styrene ND ug/L 1.0 1 08/09/08 08:43 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 08:43 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 08:43 79-34-5
Tetrachloroethene ND ug/L 1.0 1 08/09/08 08:43 127-18-4
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 13 of 48
Tills report sfiall not be reproduced, except in full,
w^ittiout the written consent of Pace Analytical Services, Inc..
^Analytical
www.pace/siis.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asiieviiie, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-7 Lab ID: 9224817006 Collected: 08/05/08 09:55 Received: 08/05/0813:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No.
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1.0 1 08/09/08 08:43 108-88-3
1,2,3-Trictilorobenzene ND ug/L 1.0 1 08/09/08 08:43 87-61-6
1,2,4-Triciilorobenzene ND ug/L 1.0 1 08/09/08 08:43 120-82-1
1,1,1-Trichloroethane ND ug/L 1.0 1 08/09/08 08:43 71-55-6
1,1,2-Trichloroethane ND ug/L 1.0 1 08/09/08 08:43 79-00-5
Trichloroethene ND ug/L 1.0 1 08/09/08 08:43 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 08/09/08 08:43 75-69-4
1,2,3-Trichloropropane ND ug/L 1.0 1 08/09/08 08:43 96-18-4
Vinyl acetate ND ug/L 2.0 1 08/09/08 08:43 108-05-4
Vinyl chloride ND ug/L 1.0 1 08/09/08 08:43 75-01-4
m&p-Xylene ND ug/L 2.0 1 08/09/08 08:43 1330-20-7
o-Xylene ND ug/L 1.0 1 08/09/08 08:43 95-47-6
4-Bromofluorobenzene (S) 97 % 87-109 1 08/09/08 08:43 460-00-4
Dibromofluoromettiane (S) 97 % 85-115 1 08/09/08 08:43 1868-53-7
1,2-Dichloroethane-d4 (S) 101 % 79-120 1 08/09/08 08:43 17060-07-0
Toluene-d8 (S) 99 % 70-120 1 08/09/08 08:43 2037-26-5
Qual
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.,
Page 14 of 48
mAnalytical
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Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-9
Parameters
Lab ID: 9224817007 Collected: 08/05/08 08:40 Received: 08/05/08 13:25 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 25.0 1 08/09/08 09:07 67-64-1
Benzene ND ug/L 1.0 1 08/09/08 09:07 71-43-2
Bromobenzene ND ug/L 1.0 1 08/09/08 09:07 108-86-1
Bromocbloromethane ND ug/L 1.0 1 08/09/08 09:07 74-97-5
Bromodichiloromethane ND ug/L 1.0 1 08/09/08 09:07 75-27-4
Bromoform ND ug/L 1.0 1 08/09/08 09:07 75-25-2
Bromomethane ND ug/L 5.0 1 08/09/08 09:07 74-83-9
2-Butanone (MEK) ND ug/L 5.0 1 08/09/08 09:07 78-93-3
Carbon tetrachloride ND ug/L 1.0 1 08/09/08 09:07 56-23-5
Chlorobenzene ND ug/L 1.0 1 08/09/08 09:07 108-90-7
Chloroethane ND ug/L 1.0 1 08/09/08 09:07 75-00-3
Chloroform ND ug/L 1.0 1 08/09/08 09:07 67-66-3
Chloromethane ND ug/L 1.0 1 08/09/08 09:07 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 08/09/08 09:07 95-49-8
4-Chlorotoluene ND ug/L 1.0 1 08/09/08 09:07 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 3.0 1 08/09/08 09:07 96-12-8
Dibromochloromethane ND ug/L 1.0 1 08/09/08 09:07 124-48-1
1,2-Dlbromoethane (EDB) ND ug/L 1.0 1 08/09/08 09:07 106-93-4
Dibromomethane ND ug/L 1.0 1 08/09/08 09:07 74-95-3
1,2-Dlchlorobenzene ND ug/L 1.0 1 08/09/08 09:07 95-50-1
1,3-Dlchlorobenzene ND ug/L 1.0 1 08/09/08 09:07 541-73-1
1,4-Dlchlorobenzene ND ug/L 1.0 1 08/09/08 09:07 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 08/09/08 09:07 75-71-8
1,1-Dichloroethane ND ug/L 1.0 1 08/09/08 09:07 75-34-3
1,2-Dichloroethane ND ug/L 1.0 1 08/09/08 09:07 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 08/09/08 09:07 75-35-4
cls-1,2-Dlchloroethene ND ug/L 1.0 1 08/09/08 09:07 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.0 1 08/09/08 09:07 156-60-5
1,2-Dichloropropane ND ug/L 1.0 1 08/09/08 09:07 78-87-5
1,3-Dlchloropropane ND ug/L 1.0 1 08/09/08 09:07 142-28-9
2,2-Dichloropropane ND ug/L 1.0 1 08/09/08 09:07 594-20-7
1,1-Dlchloropropene ND ug/L 1.0 1 08/09/08 09:07 563-58-6
cls-l ,3-Dlchloropropene ND ug/L 1.0 1 08/09/08 09:07 10061-01-5
trans-1,3-Dichloropropene ND ug/L 'i.o 1 08/09/08 09:07 10061-02-6
Diisopropyl ether ND ug/L 1.0 1 08/09/08 09:07 108-20-3
Ethylbenzene ND ug/L 1.0 1 08/09/08 09:07 100-41-4
Hexachloro-1,3-butadiene ND ug/L 1.0 1 08/09/08 09:07 87-68-3
2-Hexanone ND ug/L 5.0 1 08/09/08 09:07 591-78-6
p-lsopropyltoluene ND ug/L 1.0 1 08/09/08 09:07 99-87-6
Methylene Chloride ND ug/L 2.0 1 08/09/08 09:07 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 08/09/08 09:07 108-10-1
Methyl-tert-butyl ether ND ug/L 1.0 1 08/09/08 09:07 1634-04-4
Naphthalene ND ug/L 1.0 1 08/09/08 09:07 91-20-3
Styrene ND ug/L 1.0 1 08/09/08 09:07 100-42-5
1,1,1,2-Tef rachloroethane ND ug/L 1.0 1 08/09/08 09:07 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 09:07 79-34-5
Tetrachloroethene ND ug/L 1.0 1 08/09/08 09:07 127-18-4
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 15 of 48
This report shall not be reproduced, except in full,
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mAnalytical
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Pace Analytical Services, Inc.
2225 Riverside Dr,
Asiieville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-9 Lab ID: 9224817007 Collected: 08/05/08 08:40 Received: 08/05/08 13:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1.0 1 08/09/08 09:07 108-88-3
1,2,3-Trlchlorobenzene ND ug/L 1.0 1 08/09/08 09:07 87-61-6
1,2,4-Trichlorobenzene ND ug/L 1.0 1 08/09/08 09:07 120-82-1
1,1,1-Trichloroethane ND ug/L 1.0 1 08/09/08 09:07 71-55-6
1,1,2-Trichlot^oethane ND ug/L 1.0 1 08/09/08 09:07 79-00-5
Trichloroethene ND ug/L 1.0 1 08/09/08 09:07 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 08/09/08 09:07 75-69-4
1,2,3-Trichloropropane ND ug/L 1.0 1 08/09/08 09:07 96-18-4
Vinyl acetate ND ug/L 2.0 1 08/09/08 09:07 108-05-4
Vinyl chloride ND ug/L 1.0 1 08/09/08 09:07 75-01-4
m&p-Xylene ND ug/L 2.0 1 08/09/08 09:07 1330-20-7
o-Xylene ND ug/L 1.0 1 08/09/08 09:07 95-47-6
4-Bromofluorobenzene (S) 98 % 87-109 1 08/09/08 09:07 460-00-4
Dibromofluoromethane (S) 97 % 85-115 1 08/09/08 09:07 1868-53-7
1,2-Dlchloroethane-d4 (S) 100 % 79-120 1 08/09/08 09:07 17060-07-0
Toluene-d8 (S) 99 % 70-120 1 08/09/08 09:07 2037-26-5
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
Tills report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 16 of 48
^Analytical
www.pacelabs.cofn
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asiieville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Prolect: PSNC 1080186-01
Pace Project No.; 9224817
Sample: MW-10
Parameters
Lab ID: 9224817008 Collected; 08/05/08 08:50 Received: 08/05/08 13:25 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 25.0 1 08/09/08 09:31 67-64-1
Benzene ND ug/L 1.0 1 08/09/08 09:31 71-43-2
Bromobenzene ND ug/L 1.0 1 08/09/08 09:31 108-86-1
Bromochlorometiiane ND ug/L 1.0 1 08/09/08 09:31 74-97-5
Bromodichloromethane ND ug/L 1.0 1 08/09/08 09:31 75-27-4
Bromoform ND ug/L 1.0 1 08/09/08 09:31 75-25-2
Bromomethane ND ug/L 5.0 1 . 08/09/08 09:31 74-83-9
2-Butanone (MEK) ND ug/L 5.0 1 08/09/08 09:31 78-93-3
Carbon tetrachloride ND ug/L 1.0 1 08/09/08 09:31 56-23-5
Chlorobenzene ND ug/L 1.0 1 08/09/08 09:31 108-90-7
Chloroethane ND ug/L 1.0 1 08/09/08 09:31 75-00-3
Chloroform ND ug/L 1.0 1 08/09/08 09:31 67-66-3
Chloromethane ND ug/L 1.0 1 08/09/08 09:31 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 08/09/08 09:31 95-49-8
4-Chlorotoluene ND ug/L 1.0 1 08/09/08 09:31 106-43-4
1,2-Dlbromo-3-chloropropane ND ug/L 3.0 1 08/09/08 09:31 96-12-8
Dibromochloromethane ND ug/L 1.0 1 08/09/08 09:31 124-48-1
1,2-Dibromoethane (EDB) ND ug/L 1.0 1 08/09/08 09:31 106-93-4
Dibromomethane ND ug/L 1.0 1 08/09/08 09:31 74-95-3
1,2-Dlchlorobenzene ND ug/L 1,0 1 08/09/08 09:31 95-50-1
1,3-Dichlorobenzene ND ug/L 1.0 1 08/09/08 09:31 541-73-1
1,4-Dlchlordbenzene ND ug/L 1.0 1 08/09/08 09:31 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 08/09/08 09:31 75-71-8
1,1-Dichloroethane ND ug/L 1.0 1 08/09/08 09:31 75-34-3
1,2-Dichloroethane ND ug/L 1.0 1 08/09/08 09:31 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 08/09/08 09:31 75-35-4
cIs-1,2-Dichloroetiiene ND ug/L 1.0 1 08/09/08 09:31 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.0 1 08/09/08 09:31 156-60-5
1,2-Dichloroprbpane ND ug/L 1.0 1 08/09/08 09:31 78-87-5
1,3-Dichloropropane ND ug/L 1.0 1 08/09/08 09:31 142-28-9
2,2-Dichloropropane ND ug/L 1.0 1 08/09/08 09:31 594-20-7
1,1-Dichloropropene ND ug/L 1.0 1 08/09/08 09:31 563-58-6
cis-1,3-Dlchloropropene ND ug/L 1.0 1 08/09/08 09:31 10061-01-5
trans-1,3-Dichloropropene ND ug/L 1.0 1 08/09/08 09:31 10061-02-6
Diisopropyl ether ND ug/L 1.0 1 08/09/08 09:31 108-20-3
Ethylbenzene ND ug/L 1.0 1 08/09/08 09:31 100-41-4
Hexachloro-1,3-butadiene ND ug/L 1.0 1 08/09/08 09:31 87-68-3
2-Hexanone ND ug/L 5.0 1 08/09/08 09:31 591-78-6
p-lsopropyltoluene ND ug/L 1.0 1 08/09/08 09:31 99-87-6
Methylene Chloride ND ug/L 2.0 1 08/09/08 09:31 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 08/09/08 09:31 108-10-1
Methyl-tert-butyl ether ND ug/L 1.0 1 08/09/08 09:31 1634-04-4
Naphthalene ND ug/L 1.0 1 08/09/08 09:31 91-20-3
Styrene ND ug/L 1.0 1 08/09/08 09:31 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 09:31 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 09:31 79-34-5
Tetrachloroethene ND ug/L 1.0 1 08/09/08 09:31 127-18-4
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS F
Tfiis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page 17 of 48
iceMyticaf
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-10 Lab ID: 9224817008 Collected: 08/05/08 08:50 Received: 08/05/0813:25 Matrix; Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low/ Level Analytical Method; EPA 8260
Toluene ND ug/L 1.0 1 08/09/08 09:31 108-88-3
1,2,3-Trichlorobenzene ND ug/L 1.0 1 08/09/08 09:31 87-61-6
1,2,4-Trich|probenzene ND ug/L 1.0 1 08/09/08 09:31 120-82-1
1,1,1-Trichloroethane ND ug/L 1.0 1 08/09/08 09:31 71-55-6
1,1,2-Trichloroethane ND ug/L 1.0 1 08/09/08 09:31 79-00-5
Trichloroethene ND ug/L 1.0 1 08/09/08 09:31 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 08/09/08 09:31 75-69-4
1,2,3-Trichloropropane ND ug/L 1.0 1 08/09/08 09:31 96-18-4
Vinyl acetate ND ug/L 2.0 1 08/09/08 09:31 108-05-4
Vinyl chloride ND ug/L 1.0 1 08/09/08 09:31 75-01-4
m&p-Xylene ND ug/L 2.0 1 08/09/08 09:31 1330-20-7
o-Xylene ND ug/L 1.0 1 08/09/08 09:31 95-47-6
4-Bromofluorobenzene (S) 98 % 87-109 1 08/09/08 09:31 460-00-4
Dibromofluoromethane (S) 100 % 85-115 1 08/09/08 09:31 1868-53-7
1,2-Dlchloroethane-d4 (S) 103 % 79-120 1 08/09/08 09:31 17060-07-0
Toluene-d8 (S) 99 % 70-120 1 08/09/08 09:31 2037-26-5
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2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asiieville, NC 28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Date; 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
Page 18 of 48
weAnalytical
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Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheviiie, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-12 Lab ID: 9224817009 Collected: 08/05/0811:35 Received: 08/05/08 13:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No.
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 25.0 1 08/09/08 09:54 67-64-1
Benzene ND ug/L 1.0 1 08/09/08 09:54 71-43-2
Bromobenzene ND ug/L 1.0 1 08/09/08 09:54 108-86-1
Bromociilorome thane ND ug/L 1.0 1 08/09/08 09:54 74-97-5
Bromodichloromethane ND ug/L 1.0 1 08/09/08 09:54 75-27-4
Bromofomn ND ug/L 1.0 1 08/09/08 09:54 75-25-2
Bromomethane ND ug/L 5.0 1 08/09/08 09:54 74-83-9
2-Butanone (MEK) ND ug/L 5.0 1 08/09/08 09:54 78-93-3
Carbon tetrachloride ND ug/L 1.0 1 08/09/08 09:54 56-23-5
Chlorobenzene ND ug/L 1.0 1 08/09/08 09:54 108-90-7
Chloroethane ND ug/L 1.0 1 08/09/08 09:54 75-00-3
Chloroform ND ug/L 1.0 1 08/09/08 09:54 67-66-3
Chloromethane ND ug/L 1.0 1 08/09/08 09:54 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 08/09/08 09:54 95-49-8
4-Chlorotoluene ND ug/L 1.0 1 08/09/08 09:54 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 3.0 1 08/09/08 09:54 96-12-8
Dibromochloromethane ND ug/L 1.0 1 08/09/08 09:54 124-48-1
1,2-Dlbromoethane (EDB) ND ug/L 1.0 1 08/09/08 09:54 106-93-4
Dibromomethane ND ug/L 1.0 1 08/09/08 09:54 74-95-3
1,2-Dichlorobenzene ND ug/L 1.0 1 08/09/08 09:54 95-50-1
1,3-Dichlorobenzene ND ug/L 1.0 1 08/09/08 09:54 541-73-1
1,4-Dlchlorobenzene ND ug/L 1.0 1 08/09/08 09:54 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 08/09/08 09:54 75-71-8
1,1-Dlchloroelhane ND ug/L 1.0 1 08/09/08 09:54 75-34-3
1,2-Dlchloroethane ND ug/L 1.0 1 08/09/08 09:54 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 08/09/08 09:54 75-35-4
cis-1,2-Dichloroethene ND ug/L 1.0 1 08/09/08 09:54 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.0 1 08/09/08 09:54 156-60-5
1,2-Dlchloropropane ND ug/L 1.0 1 08/09/08 09:54 78-87-5
1,3-Dichloropropane ND ug/L 1.0 1 08/09/08 09:54 142-28-9
2,2-Dichloropropane ND ug/L 1.0 1 08/09/08 09:54 594-20-7
1,1-pichloroprop.ene . ND ug/L 1.0 1 08/09/08 09:54 563-58-6
cis-1,3-Dichloropropene ND ug/L 1.0 1 08/09/08 09:54 1 0061-01-5
trans-1,3-Dichloropropene ND ug/L 1.0 1 08/09/08 09:54 10061-02-6
Dllsopropyl ether ND ug/L 1.0 1 08/09/08 09:54 108-20-3
Ethylbenzene ND ug/L 1.0 1 08/09/08 09:54 100-41-4
Hexachloro-1,3-butadlene ND ug/L 1.0 1 08/09/08 09:54 87-68-3
2-Hexanone ND ug/L 5.0 1 08/09/08 09:54 591-78-6
p-lsopropyltoluene ND ug/L 1.0 1 08/09/08 09:54 99-87-6
Methylene Chloride ND ug/L 2.0 1 08/09/08 09:54 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 08/09/08 09:54 108-10-1
Methyl-tert-butyl ether ND ug/L 1.0 1 08/09/08 09:54 1634-04-4
Naphthalene ND ug/L 1.0 1 08/09/08 09:54 91-20-3
Styrene ND ug/L 1.0 1 08/09/08 09:54 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 09:54 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 09:54 79-34-5
Tetrachloroethene 4.6 ug/L 1.0 1 08/09/08 09:54 127-18-4
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
P
Qual
Page 19 of 48
^Analytical
www.pecel6bs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asiieviiie, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviiie, NC 28078
[phone]
ANALYTICAL RESULTS
Project; PSNC 1080186-01
Pace Project No.; 9224817
Sample: MW-12
Parameters
8260 MSV Low Level
Lab ID: 9224817009 Collected; 08/05/08 11;35 Received; 08/05/0813;25 Matrix; Water
Results Units Report Limit DF Prepared Analyzed CAS No.
Analytical Method; EPA 8260
Toluene ND ug/L 1.0 1 08/09/08 09;54 108-88-3
1,2,3-Trichlorobenzene ND ug/L 1.0 1 08/09/08 09;54 87-61-6
1,2,4-Trichlorobenzene ND ug/L 1.0 1 08/09/08 09;54 120-82-1
1,1,1-Trichloroethane ND ug/L 1.0 1 08/09/08 09;54 71-55-6
1,1,2-Trichloroethane ND ug/L 1.0 1 08/09/08 09;54 79-00-5
Trichloroethene ND ug/L 1.0 1 08/09/08 09;54 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 08/09/08 09;54 75-69-4
1,2,3-Trichloropropane ND ug/L 1.0 1 08/09/08 09;54 96-18-4
Vinyl acetate ND ug/L 2.0 1 08/09/08 09;54 108-05-4
Vinyl chloride ND ug/L 1.0 1 08/09/08 09;54 75-01-4
m&p-Xylene ND ug/L 2.0 1 08/09/08 09;54 1330-20-7
o-Xylene ND ug/L 1.0 1 08/09/08 09:54 95-47-6
4-Bromofluorobenzene (S) 97 % 87-109 1 08/09/08 09:54 460-00-4
Dibromofluoromethane (S) 97 % 85-115 1 08/09/08 09:54 1868-53-7
1,2-Dichloroethane-d4 (S) 100 % 79-120 1 08/09/08 09:54 17060-07-0
Toluene-d8 (S) 99 % 70-120 1 08/09/08 09:54 2037-26-5
Qua!
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
Tills report stiall not be reproduced, except in full,
wittiout Itie written consent of Pace Analytical Services, Inc..
Page 20 of 48
^Analytical
mvw.pacste.bs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Paoe Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-13
Parameters
Lab ID: 9224817010 Collected: 08/05/08 10:35
Results Units Report Limit DF
Received:
Prepared
08/05/08 13:25 Matrix: Water
Analyzed CAS No.
8260 MSV Low Level Analytical Method: EPA8260
Acetone ND ug/L 25.0 1 08/09/08 10:18 67-64-1
Benzene ND ug/L 1.0 1 08/09/08 10:18 71-43-2
Bromobenzene ND ug/L 1.0 1 08/09/0810:18 108-86-1
Bromochlorometiiane ND ug/L 1.0 1 08/09/08 10:18 74-97-5
Bromodichloromethane ND ug/L 1.0 1 08/09/08 10:18 75-27-4
Bromoform ND ug/L 1.0 1 08/09/08 10:18 75-25-2
Bromomethane ND ug/L 5,0 1 08/09/0810:18 74-83-9
2-Butanone (MEK) ND ug/L 5.0 1 08/09/0810:18 78-93-3
Carbon tetrachloride ND ug/L 1.0 1 08/09/08 10:18 56-23-5
Chlorobenzene ND ug/L 1.0 1 08/09/0810:18 108-90-7
Chloroethane ND ug/L 1.0 1 08/09/08 10:18 75-00-3
Chloroform ND ug/L 1.0 1 08/09/0810:18 67-66-3
Chloromethane ND ug/L 1.0 1 08/09/0810:18 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 08/09/08 10:18 95-49-8
4-Chlorotoluene ND ug/L 1.0 1 08/09/08 10:18 106-43-4
1,2-Dlbromo-3-chloropropane ND ug/L 3.0 1 08/09/08 10:18 96-12-8
Dibromochloromethane ND ug/L 1.0 1 08/09/08 10:18 124-48-1
1,2-Dibromoethane (EDB) ND ug/L 1.0 1 08/09/0810:18 106-93-4
Dibromomethane ND ug/L 1.0 1 08/09/08 10:18 74-95-3
1,2-Dichlorobenzene ND ug/L 1.0 1 08/09/08 10:18 95-50-1
1,3-Dlchlorobenzene ND ug/L 1.0 1 08/09/0810:18 541-73-1
1,4-Dichlorobenzene ND ug/L 1.0 1 08/09/08 10:18 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 08/09/08 10:18 75-71-8
1,1-Dichloroethane ND ug/L 1.0 1 08/09/08 10:18 75-34-3
1,2-Dlchloroethane ND ug/L 1.0 1 08/09/08 10:18 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 08/09/08 10:18 75:35-4
cis-1,2-Dichloroethene ND ug/L 1.0 1 08/09/08 10:18 156-59-2
trans-1,2-Dlchlo,roethene ND ug/L 1.0 1 08/09/08 10:18 156-60-5
1,2-Dichloropropane ND ug/L 1.0 1 08/09/08 10:18 78-87-5
1,3-Dichloropropane ND ug/L 1.0 1 08/09/08 10:18 142-28-9
2,2-Dlchloropropane ND ug/L 1.0 1 08/09/08 1 0:18 594-20-7
1,1-Dlchloropropene ND ug/L 1.0 1 08/09/08 10:18 563-58-6
cis-1,3-Dichloropropene ND ug/L 1.0 1 08/09/0810:18 10061-01-5
trans-1,3-Dlchloropropene ND ug/L 1.0 1 08/09/08 10:18 10061-02-6
Diisopropyl ether ND ug/L 1.0 1 08/09/0810:18 108-20-3
Ethylbenzene ND ug/L 1.0 1 08/09/08 10:18 100-41-4
Hexachloro-1,3-butadiene ND ug/L 1.0 1 08/09/08 10:18 87-68-3
2-Hexanone ND ug/L 5.0 1 08/09/08 10:18 591-78-6
p-lsopropyltoluene ND ug/L 1.0 1 08/09/0810:18 99-87-6
Methylene Chloride ND ug/L 2.0 1 08/09/0810:18 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 08/09/08 10:18 108-10-1
Methyl-tert-butyl ether ND ug/L 1.0 1 08/09/08 10:18 1634-04^
Naphthalene ND ug/L 1.0 1 08/09/08 10:18 91-20-3
Styrene ND ug/L 1.0 1 08/09/08 10:18 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 10:18 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 08/09/0810:18 79-34-5
Tetrachloroethene ND ug/L 1.0 1 08/09/08 10:18 127-18-4
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 21 of 48
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
^aceAnalytical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-13 Lab ID: 9224817010 Collected: 08/05/08 10:35 Received; 08/05/08 13:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1.0 1 08/09/0810:18 108-88-3
1,2,3-Trichlorobenzene ND ug/L 1.0 1 08/09/0810:18 87-61-6
1,2,4-Trichlorobenzene ND ug/L 1.0 1 08/09/0810:18 120-82-1
1,1,1-Trichloroethane ND ug/L 1,0 1 08/09/08 10:18 71-55-6
1,1,2-Trichloroethane ND ug/L 1.0 1 08/09/0810:18 79-00-5
Trichloroethene ND ug/L 1.0 1 08/09/08 10:18 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 08/09/0810:18 75-69-4
1,2,3-Trichloropropane ND ug/L 1.0 1 08/09/08 10:18 96-18-4
Vinyl acetate ND ug/L 2.0 1 08/09/0810:18 108-05-4
Vinyl chloride ND ug/L 1.0 1 08/09/08 10:18 75-01-4
m&p-Xylene ND ug/L 2.0 1 08/09/0810:18 1330-20-7
o-Xylene ND ug/L 1.0 1 08/09/08 10:18 95-47-6
4-Bromofluorobenzene (S) 97 % 87-109 1 08/09/08 10:18 460-00-4
Dibromofluoromethane (S) 97 % 85-115 1 08/09/08 10:18 1868-53-7
1,2-Dichloroethane-d4 (S) 100 % 79-120 1 08/09/08 10:18 17060-07-0
Toluene-d8 (S) 99 % 70-120 1 08/09/08 10:18 2037-26-5
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
VKlthout the written consent of Pace Analytical Sen/ices, Inc.
Page 22 of 48
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ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-14 Lab ID: 9224817011 Collected: 08/05/0810:10 Received: 08/05/0813:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 25.0 1 08/09/0810:42 67-64-1
Benzene ND ug/L 1.0 1 08/09/0810:42 71-43;2
Bromobenzene ND ug/L 1.0 1 08/09/08 10:42 108-86-1
Bromoctiloromethane ND ug/L 1.0 1 08/09/0810:42 74-97-5
Bromodichloromethane ND ug/L 1.0 1 08/09/08 10:42 75-27-4-
Bromofomi ND ug/L 1.0 1 08/09/08 10:42 75-25-2
Bromomethane ND ug/L 5.0 1 08/09/0810:42 74-83-9
2-Butanone (MEK) ND ug/L 5.0 1 08/09/0810:42 78-93-3
Carbon tetrachloride ND ug/L 1.0 1 08/09/08.10:42 56-23-5
Chlorobenzene ND ug/L 1.0 1 08/09/08 10:42 108-90-7
Chloroethane ND ug/L 1.0 1 08/09/0810:42 75-00-3
Chlorofomi ND ug/L 1.0 1 08/09/0810:42 67-66-3
Chloromethane ND ug/L 1.0 1 08/09/08 10:42 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 08/09/08 10:42 95-49-8
4-Chlorotoluene ND ug/L 1.0 1 08/09/08 10:42 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 3.0 1 08/09/08 10:42 96-12-8
Dibromochloromethane ND ug/L 1.0 1 08/09/08 10:42 124-48-1
1,2-Dibromoethane (EDB) ND ug/L 1.0 1 08/09/08 10:42 106-93-4
Dibromomethane ND ug/L 1.0 1 08/09/08 10:42 74-95-3
1,2-Dichlorobenzene ND ug/L 1.0 1 08/09/08 10:42 95-50-1
1,3-Dichlorobenzene ND ug/L 1.0 1 08/09/0810:42 541-73-1
1,4-Dlchlorobenzene ND ug/L 1.0 1 08/09/08 10:42 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 08/09/08 10:42 75-71-8
1,1-Dichloroethane ND ug/L 1.0 1 08/09/08 10:42 75-34-3
1,2-Dichloroethane ND ug/L 1.0 1 08/09/08 10:42 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 08/09/08 10:42 75-35-4
cis-1,2-Dichloroethene ND ug/L 1.0 1 08/09/08 10:42 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.0 1 08/09/0810:42 156-60-5
1,2-Dichloropropane ND ug/L 1.0 1 08/09/08 10:42 78-87-5
1,3-Dichloropropane ND ug/L 1.0 1 08/09/08 10:42 142-28-9
2,2-Dichloropropane ND ug/L 1.0 1 08/09/08 1 0:42 594-20-7
1,1-Dichloropropene ND ug/L 1.0 1 08/09/08 10:42 563-58-6
cis-1,3-Dlchloropropene ND ug/L 1.0 1 08/09/08 10:42 10061-01-5
trans-1,3-Dichloropropene ND ug/L 1.0 1 08/09/08 10:42 10061-02-6
Dllsopropyl ether ND ug/L 1.0 1 08/09/08 10:42 108-20-3
Ethylbenzene ND ug/L 1.0 1 08/09/08 10:42 100-41-4
Hexachloro-1,3-butadiene ND ug/L 1.0 1 08/09/0810:42 87-68-3
2-Hexanone ND ug/L 5.0 1 08/09/08 10:42 591-78-6
p-lsopropyltoluene ND ug/L 1.0 1 08/09/08 10:42 99-87-6
Methylene Chloride ND ug/L 2.0 1 08/09/08 10:42 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 08/09/08 10:42 108-10-1
Methyl-tert-butyl ether ND ug/L 1.0 1 08/09/08 10:42 1634-04-4
Naphthalene ND ug/L 1.0 1 08/09/0810:42 91-20-3
Styrene ND ug/L 1.0 1 08/09/08 10:42 100^2-5
1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 10:42 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 1 0:42 79-34-5
Tetrachloroethene 2.9 ug/L 1.0 1 08/09/08 10:42 127-18-4
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 23 of 48
Tills report stiall not be reproduced, except In full,
wittiout ttie written consent of Pace Analytical Services, Inc.
'ace Analytical
mm.pBCal6bs.txim
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviiie, NC 28078
[phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-14 Lab ID: 9224817011 Collected: 08/05/08 10:10 Received: 08/05/0813:25 Matrix: Water ^
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Metiiod: EPA 8260
Toluene ND ug/L 1.0 1 08/09/0810:42 108-88-3
1,2,3-Trlchlorobenzene ND ug/L 1.0 1 08/09/0810:42 87-61-6
1,2,4-Trichlorobenzene ND ug/L 1.0 1 08/09/0810:42 120-82-1
1,1,1-Triciiloroethane ND ug/L 1.0 1 08/09/0810:42 71-55-6
1,1,2-trichroroethahe ND ug/L 1.0 1 08/09/0810:42 79-00-5
Trichloroethene . ND ug/L 1.0 1 08/09/0810:42 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 08/09/0810:42 75-69-4
1,2,3-Trichloropropane ND ug/L 1.0 1 08/09/0810:42 96-18-4
Vinyl acetate ND ug/L 2.0 1 08/09/0810:42 108-05-4
Vinyl chloride ND ug/L 1.0 1 08/09/0810:42 75-01-4
m&p-Xylene ND ug/L 2.0 1 08/09/08 10:42 1330-20-7
o-Xylene ND ug/L 1.0 1 08/09/0810:42 95-47-6
4-Bromofluorobenzene (S) 99 % 87-109 1 08/09/0810:42 460-00-4
Dibromofluoromethane (S) 97 % 85-115 1 08/09/08 10:42 1868-53-7
1,2-Dichloroethane-d4 (S) 99 % 79-120 1 08/09/0810:42 17060-07-0
Toluene-d8 (S) 99 % 70-120 1 08/09/0810:42 2037-26-5
mAnalytical
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2225 Riverside Dr.
Asiieville, NC 28804
[phone]
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 24 of 48
Ttiis report shall not be nepreiduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2226 i^iverside Dr 9800 Kincey Ave. Suite 100
Asiieviiie, NC 28804 Huntersviiie, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-1S Lab ID: 9224817012 Collected: 08/05/08 10:05 Received: 08/05/08 13:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 25.0 1 08/09/08 11:05 67-64-1
Benzene ND ug/L 1.0 1 08/09/0811:05 71-43-2
Bromobenzene ND ug/L 1.0 1 08/09/0811:05 108-86-1
Bromochloromethane ND ug/L 1.0 1 08/09/0811:05 74-97-5
Bromodichloromethane ND ug/L 1.0 1 08/09/08 11:05 75-27-4
Bromoform ND ug/L 1.0 1 08/09/08 11:05 75-25-2
Bromomethane ND ug/L 5.0 1 08/09/08 11.05 74-83-9
2-Butanone (MEK) ND ug/L 5.0 1 08/09/08 11:05 78-93-3
Carbon tetrachloride ND ug/L 1.0 1 08/09/0811:05 56-23-5
Chlorobenzene ND ug/L 1.0 1 08/09/0811:05 108-90-7
Chloroethane ND ug/L 1.0 1 08/09/08 11:05 75-00-3
Chlorofomi ND ug/L 1.0 1 08/09/0811:05 67-66-3
Chloromethane ND ug/L 1.0 1 08/09/0811:05 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 08/09/08 11:05 95-49-8
4-Ghlorotoluene ND ug/L 1.0 1 08/09/0811:05 106-43-4
1,2-Dlbromo-3-chloropropane ND ug/L 3.0 1 08/09/08 11:05 96-12-8
Dibromochloromethane ND ug/L 1.0 1 08/09/08 11:05 124-48-1
1,2-Dibromoethane (EDB) ND ug/L 1.0 1 08/09/08 11:05 106-93-4
Dibromomethane ND ug/L 1.0 1 08/09/0811:05 74-95-3
1,2-Dlchlorobenzene ND ug/L 1.0 1 08/09/08 11:05 95-50-1
1,3-Dlchlorobenzene ND ug/L 1.0 1 08/09/08 11:05 541-73-1
1,4-Dlchlorobenzene ND ug/L 1.0 1 08/09/0811:05 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 08/09/0811:05 75-71-8
1,1-Dichloroethane ND ug/L 1.0 1 08/09/0811:05 75-34-3
1,2-Dichloroethane ND ug/L 1.0 1 08/09/0811:05 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 08/09/0811:05 75-35-4
cis-1,2-Dlchloroethene ND ug/L 1.0 1 08/09/08 11:05 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.0 1 08/09/08 11:05 156-60-5
1,2-Dichloropropane ND ug/L 1.0 1 08/09/0811:05 78-87-5
1,3-Dichloropropane ND ug/L 1.0 1 08/09/08 11:05 142-28-9
2,2-Dlchloropropane ND ug/L 1.0 1 08/09/08 11:05 594-20-7
1,1-Dichloropropene ND ug/L 1.0 1 08/09/08 11:05 563-58-6
cis-1,3-Dichloropropene ND ug/L 1.0 1 08/09/08 11:05 10061-01-5
trans-1,3-Dlchloropropene ND ug/L 1.0 1 08/09/08 11:05 10061-02-6
Dllsopropyl ether ND ug/L 1.0 1 08/09/08 11:05 108-20-3
Ethylbenzene ND ug/L 1.0 1 08/09/0811:05 100-41-4
Hexachloro-1,3-butadiene ND ug/L 1.0 1 08/09/08 11:05 87-68-3
2-Hexanone ND ug/L 5.0 1 08/09/0811:05 591-78-6
p-lsopropyltoluene ND ug/L 1.0 1 08/09/0811:05 99-87-6
Methylene Chloride ND ug/L 2.0 1 08/09/0811:05 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 08/09/08 11:05 108-10-1
Methyl-tert-butyl ether ND ug/L 1.0 1 08/09/08 11:05 1634-04-4
Naphthalene ND ug/L 1.0 1 08/09/08 11:05 91-20-3
Styrene ND ug/L 1.0 1 08/09/0811:05 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 08/09/0811:05 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 11:05 79-34-5
Tetrachloroethene ND ug/L 1.0 1 08/09/0811:05 127-18-4
Date; 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page25of48
Ttiis report stiali not be reproduced, except in full,
without the written consent of Pace Anaiytical Services, Inc..
mAnalytical
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weAnalytical
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Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-15
Parameters
8260 MSV Low Level
Toluene
1.2.3- Trichlorobenzene
1.2.4- Trichlorobenzene
1.1.1- Trichloroethane
1.1.2- Trichloroethane
Trichloroethene
Trichlorofluoromethane
1.2.3- Trichloropropane
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Lab ID: 9224817012 Collected: 08/05/0810:05 Received: 08/05/0813:25 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No.
Analytical Method: EPA 8260
ND ug/L 1.0 1 08/09/0811:05 108-88-3
ND ug/L 1.0 1 08/09/0811:05 87-61-6
ND ug/L 1.0 1 08/09/0811:05 120-82-1
ND ug/L 1.0 1 08/09/0811:05 71-55-6
ND ug/L 1.0 1 08/09/0811:05 79-00-5
ND ug/L 1.0 1 08/09/0811:05 79-01-6
ND ug/L 1.0 1 08/09/0811:05 75-69-4
ND ug/L 1.0 1 08/09/0811:05 96-18-4
ND ug/L 2.0 1 08/09/0811:05 108-05-4
ND ug/L 1.0 1 08/09/0811:05 75-01-4
ND ug/L 2.0 1 08/09/0811:05 1330-20-7
ND ug/L 1.0 1 08/09/0811:05 95-47-6
98 % 87-109 1 08/09/0811:05 460-00-4
97 % 85-115 1 08/09/0811:05 1868-53-7
99 % 79-120 1 08/09/08 11:05 17060-07-0
100 % 70-120 1 08/09/0811:05 2037-26-5
Qual
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 26 of 48
This report shall not be reprciduced, except in full,
without the written consent of Pace Analytical Sen/ices, Inc..
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2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asiieviiie, NC 28804 Huntersviiie, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-16D Lab ID: 9224817013 Collected: 08/05/08 09:05 Received: 08/05/08 13:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 25.0 1 08/09/08 11:29 67-64-1
Benzene ND ug/L 1.0 1 08/09/08 11:29 71-43-2
Bromobenzene ND ug/L 1.0 1 08/09/08 11:29 108-86-1
Bromochloromethane ND ug/L 1.0 1 08/09/08 11:29 74-97-5
Brornodichloromethane ND ug/L 1.0 1 08/09/0811:29 75-27-4
Bromoform ND ug/L 1.0 1 08/09/0811:29 75-25-2
Bromomethane ND ug/L 5.0 1 08/09/08 11:29 74-83-9
2-Bulanone (MEK) ND ug/L 5.0 1 08/09/0811:29 78-93-3
Carbon tetrachloride ND ug/L 1.0 1 08/09/0811:29 56-23-5
Chlorobenzene ND ug/L 1.0 1 08/09/08 11:29 108-90-7
Chloroethane ND ug/L 1.0 1 08/09/0811:29 75-00-3
Chloroform 1.5 ug/L 1.0 1 08/09/0811:29 67-66-3
Chloromethane ND ug/L 1.0 1 08/09/0811:29 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 08/09/0811:29 95-49-8
4-Chlorotoluene ND ug/L 1.0 1 08/09/0811:29 106-43-4
1,2-Dlbromo-3-chloropropane ND ug/L' 3.0 1 08/09/0811:29 96-12-8
Dibromochloromethane ND ug/L 1.0 1 08/09/0811:29 124-48-1
1,2-Dibromoethane (EDB) ND ug/L 1.0 1 08/09/0811:29 106-93-4
Dibromomethane ND ug/L 1.0 1 08/09/0811:29 74-95-3
1,2-Dlchlorobenzene ND ug/L 1.0 1 08/09/08 11:29 95-50-1
1,3-Dichlorobenzene ND ug/L 1.0 1 08/09/0811:29 541-73-1
1,4-Dichlorobenzene ND ug/L 1.0 1 08/09/0811:29 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 08/09/0811:29 75-71-8
1,1-Dichloroethane ND ug/L 1.0 1 08/09/0811:29 75-34-3
1,2-Dichloroethane ND ug/L 1.0 1 08/09/0811:29 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 08/09/0811:29 75-35-4
cis-1,2-Dlchloroethene ND ug/L 1.0 1 08/09/08 11:29 156-59-2
trans-1,2-Dlchloroethene ND ug/L 1.0 1 08/09/0811:29 156-60-5
1,2-Dichloropropane ND ug/L 1.0 1 08/09/0811:29 78-87-5
1,3-Dlchloropropane ND ug/L 1.0 1 08/09/08 11:29 142-28-9
2,2-Dlchloropropane ND ug/L 1.0 1 08/09/08 11:29 594-20-7
1,1-Dichloropropene Nb ug/L 1.0 1 08/09/0811:29 563-58-6
cls-1,3-Dichloropropene ND ug/L 1.0 1 08/09/08 11:29 10061-01-5
trans-l ,3-Dlchloropropene ND ug/L 1.0 1 08/09/08 11:29 10061-02-6
Dllsopropyl ether ND ug/L 1.0 1 08/09/0811:29 108-20-3
Ethylbenzene ND ug/L 1.0 1 08/09/0811:29 100-41-4
Hexachloro-1,3-butadiene ND ug/L 1.0 1 08/09/08 11:29 87-68-3
2-Hexanone ND ug/L 5.0 1 08/09/08 11:29 591-78-6
p-lsopropyltoluene ND ug/L 1.0 1 08/09/0811:29 99-87-6
Methylene Chloride ND ug/L 2.0 1 08/09/0811:29 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 08/09/08 11:29 108-10-1
Methyl-tert-butyl ether ND ug/L 1.0 1 08/09/08 11:29 1634-04-4
Naphthalene ND ug/L 1.0 1 08/09/08 11:29 91-20-3
Styrene ND ug/L 1.0 1 08/09/0811:29 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 08/09/0811:29 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 11:29 79-34-5
Tetrachloroethene 3.0 ug/L 1.0 1 08/09/08 11:29 127-18-4
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page27of48
Tills report stiall not be reproduced, except in full,
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ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-16D Lab ID: 9224817013 Collected: 08/05/08 09:05 Received: 08/05/08 13:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1.0 1 08/09/08 11 29 108-88-3
1,2,3-Trictilorobenzene ND ug/L 1.0 1 08/09/08 11 29 87-61-6
1,2,4-Triciilorobenzene ND ug/L 1.0 1 08/09/08 11 29 120-82-1
1,1,1-Trichloroetiiane ND ug/L 1.0 1 08/09/08 11 29 71-55-6
1,1,2-Tcl chloroettiane ND ug/L 1.0 1 08/09/08 11 29 79-00-5
Trichloroethene 1.1 ug/L 1.0 1 08/09/08 11 29 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 08/09/08 11 29 75-69-4
1,2,3-Trichloropropane ND ug/L 1.0 1 08/09/08 11 29 96-18-4
Vinyl acetate ND ug/L 2.0 1 08/09/0811 29 108-05-4
Vinyl chloride ND ug/L 1.0 1 08/09/08 11 29 75-01-4
m&p-Xylene ND ug/L 2.0 1 08/09/08 11 29 1330-20-7
o-Xylene ND ug/L 1.0 1 08/09/08 11 29 95-47-6
4-Bromofluorobenzene (S) 98 % 87-109 1 08/09/08 11 29 460-00-4
Dibromofluoromethane (S) 97 % 85-115 1 08/09/08 11 29 1868-53-7
1,2-Dichloroethane-d4 (S) 100 % 79-120 1 08/09/08 11 29 17060-07-0
Toluene-d8 (S) 99 % 70-120 1 08/09/08 11 29 2037-26-5
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 28 of 48
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ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.; 9224817
Sample: MW-3
Parameters
Lab ID: 9224817014 Collected: 08/05/0811:10 Received: 08/05/08 13:25 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No.
6010 MET ICP Analytical Metiiod: EPA 6010 Preparation Method: EPA 3010
Iron 557 ug/L 50.0 1 08/06/08 14:40 08/12/08 15:14 7439-89-6
Manganese 202 ug/L , 5.0 1 08/06/08 14:40 08/12/0815:14 7439-96-5
6010 MET ICP, Lab Filtered Analytical Method: EPA 6010 Preparation Method: EPA 3010
Iron ND ug/L 50.0 1 08/12/08 14:46 08/13/08 20:04 7439-89-6
Manganese 159 ug/L 5.0 1 08/12/08 14:46 08/13/0820:04 7439-96-5
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 25.0 1 08/09/0811:53 67-64-1
Benzene ND ug/L 1.0 08/09/08 11:53 71-43-2
Bromobenzene ND ug/L 1.0 08/09/0811:53 108-86-1
Bromochloromethane ND ug/L 1.0 08/09/0811:53 74-97-5
Bromodichloromethane ND ug/L 1.0 08/09/08 11:53 75-27-4
Bromoform ND ug/L 1.0 08/09/0811:53 75-25-2
Bromomethane ND ug/L 5.0 08/09/0811:53 74-83-9
2-Butanone (MEK) ND ug/L 5.0 08/09/08 11:53 78-93-3
Carbon tetrachloride ND ug/L 1.0 08/09/08 11:53 56-23-5
Chlorobenzene ND ug/L 1.0 08/09/0811:53 108-90-7
Chloroethane ND ug/L 1.0 08/09/08 11:53 75-00-3
Chlorofomi 6.0 ug/L 1.0 08/09/08 11:53 67-66-3
Chloromethane ND ug/L 1.0 08/09/0811:53 74-87-3
2-Chlorotoluene ND ug/L 1.0 08/09/08 11:53 95-49-8
4-Chlorotoluene ND ug/L 1.0 08/09/0811:53 106-43-4
1,2-Dlbromo-3-chloropropane ND ug/L 3.0 08/09/08 11:53 96-12-8
Dibromochloromethane ND ug/L 1.0 08/09/08 11:53 124^8-1
1,2-Dibromoethane (EDB) ND ug/L 1.0 08/09/08 11:53 106-93-4
Dibromomethane ND ug/L 1.0 08/09/08 11:53 74-95-3
1,2-Dlchlorobenzene ND ug/L 1.0 08/09/08 11:53 95-50-1
1,3-Dlchlorobenzene ND ug/L 1.0 08/09/0811:53 541-73-1
1,4-Dlchlorobenzene ND ug/L 1.0 08/09/08 11:53 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 08/09/08 11:53 75-71-8
1,1-Dichloroethane 12.9 ug/L 1.0 08/09/08 11:53 75-34-3
1,2-Dlchlprpethane ND ug/L 1.0 08/09/08 11:53 107-06-2
1,1-Dichloroethene 1.6 ug/L 1.0 08/09/08 11:53 75-35-4
cis-1,2-Dichloroethene 5.3 ug/L 1.0 08/09/Cf) 11:53 156-59-2
trans-1,2-Dlchloroethene ND lig/L 1.0 08/09/08 11:53 156-60-5
1,2-Dichloropropane ND ug/L 1.0 08/09/08 11:53 78-87-5
1,3-Dlchloropropane ND ug/L 1.0 08/09/08 11:53 142-28-9
2,2-Dlchloropropane ND ug/L 1.0 08/09/08 11:53 594-20-7
1,1-Dichloropropene ND ug/L 1.0 08/09/08 11:53 563-58-6
cls-1,3-Dichloropropene ND ug/L 1.0 08/09/08 11:53 10061-01-5
trans-1,3-Dichloropropene ND ug/L 1.0 08/09/08 11:53 10061-02-6
Diisopropyl ether ND ug/L 1.0 08/09/08 11:53 108-20-3
Ethylbenzene ND ug/L 1.0 08/09/08 11:53 100-41-4
Hexachloro-1,3-butadiene ND ug/L 1.0 08/09/08 11:53 87-68-3
2-Hexanone ND ug/L 5.0 08/09/08 11:53 591-78-6
Qual
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 29 of 48
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample; MW-3
Parameters
8260 MSV Low Level
Lab ID: 9224817014 Collected; 08/05/08 11:10 Received; 08/05/0813:25 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Metiiod: EPA 8260
p-lsopropyltoluene ND ug/L 1.0 1 08/09/08 11:53 99-87-6
Mettiylene Chloride ND ug/L 2.0 1 08/09/0811:53 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 08/09/08 11:53 108-10-1
Methyl-tert-butyl ether ND ug/L 1.0 1 08/09/0811:53 1634-04-4
Naphthalene . ND ug/L 1.0 1 08/09/0811:53 91-20-3
Styrene ND ug/L 1.0 1 08/09/08 11:53 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 08/09/0811:53 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 08/09/0811:53 79-34-5
Tetrachloroethene 7.7 ug/L 1.0 1 08/09/0811:53 127-18-4
Toluene ND ug/L 1.0 1 08/09/0811:53 108-88-3
1,2,3-Trichlorobenzene ND ug/L 1.0 1 08/09/0811:53 87-61-6
1,2,4-Trichlorobenzene ND ug/L 1.0 1 08/09/0811:53 120-82-1
1,1,1-Trichloroethane ND ug/L 1.0 1 08/09/0811:53 71-55-6
1,1,2-Trichloroethane ND ug/L 1.0 1 08/09/08 11:53 79-00-5
Trichloroethene ND ug/L 1.0 1 08/09/08 11:53 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 08/09/0811:53 75-69-4
1,2,3-Trichloropropane ND ug/L 1.0 1 08/09/0811:53 96-18-4
Vinyl acetate ND ug/L 2.0 1 08/09/0811:53 108-05-4
Vinyl chloride ND ug/L 1.0 1 08/09/0811:53 75-01-4
m&p-Xylene ND ug/L 2.0 1 08/09/0811:53 1330-20-7
o-Xylene ND ug/L 1.0 1 08/09/0811:53 95-47-6
4-Bromofiuorobenzene (S) 98 % 87-109 1 08/09/0811:53 460-00-4
Dibromofluoromethane (S) 98 % 85-115 1 08/09/0811:53 1868-53-7
1,2-Dlchloroethane-d4 (S) 100 % 79-120 1 08/09/08 11:53 17060-07-0
Toluene-d8 (S) 99 % 70-120 1 08/09/0811:53 2037-26-5
521 OB BOD, Low Level Analytical Method: SM 521 OB
BOD, 5 day ND mg/L 2.0 1 08/06/0816.00 08/11/0816:10
353.2 Nitrogen, N02/N03 unpres Analytical Method: EPA 353.2
Nitrogen, Nitrate 2.9 mg/L 0.10 1 08/05/08 23:13
522PP COD Analytical Method: SM 5220D
Chemical Oxygen Demand ND mg/L 25.0 1 08/08/08 20:05
ASTM D516-90 Sulfate Water Analytical Method: ASTM D516-90
Sulfate 66.5 mg/L 10.0 2 08/07/08 18:14 14808-79-8
B2,B4
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page30of48
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ANALYTICAL RESULTS
Sample: MW-8 Lab ID: 9224817015 Collected: 08/05/08 09:35 Received: 08/05/0813:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Iron 2500 ug/L 50.0 1 08/06/08 14:40 08/13/08 20:57 7439-89-6
Manganese 111 ug/L 5.0 1 08/06/08 14:40 08/13/08 20:57 7439-96-5
6010 MET ICP, Lab Filtered Analytical Method: EPA 6010 Preparation Method: EPA 3010
Iron ND ug/L 50.0 1 08/12/08 14:46 08/13/08 20:11 7439-89-6
Manganese 76.1 ug/L 5.0 1 08/12/08 14:46 08/13/08 20:11 7439-96-5
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 25.0 1 08/09/08 12:16 67-64-1
Benzene ND ug/L 1.0 1 08/09/0812:16 71-43-2
Bromobenzene ND ug/L 1.0 1 08/09/08 12:16 108-86-1
Bromochloromethane ND ug/L 1.0 1 08/09/0812:16 74-97-5
Bromodichloromethane ND ug/L 1.0 1 08/09/0812:16 75-27-4
Bromoform ND ug/L 1.0 1 08/09/0812:16 75-25-2
Bromomethane ND ug/L 5.0 1 08/09/0812:16 74-83-9
2-Butanone (MEK) ND ug/L 5.0 1 08/09/08 12:16 78-93-3
Carbon tetrachloride ND ug/L 1.0 1 08/09/0812:16 56-23-5
Chlorobenzene ND ug/L 1.0 1 08/09/0812:16 108-90-7
Chloroethane ND ug/L 1.0 1 08/09/0812:16 75-00-3
Chloroform ND ug/L 1.0 1 08/09/08 12:16 67-66-3
Chloromethane ND ug/L 1.0 1 08/09/0812:16 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 08/09/0812:16 95-49-8
4-Chlorotoluene ND ug/L 1.0 1 08/09/0812:16 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 3.0 1 08/09/08 12:16 96-12-8
Dibromochloromethane ND ug/L 1.0 1 08/09/08 12:16 124-48-1
1,2-Dlbromoethane (EDB) ND ug/L 1.0 1 08/09/08 12:16 106-93-4
Dibromomethane ND ug/L 1.0 1 08/09/08 12:16 74-95-3
1,2-Dichlorobenzene ND ug/L 1.0 1 08/09/08 12:16 95-50-1
1,3-Dlchlorobenzene ND ug/L 1.0 1 08/09/0812:16 541-73-1
1,4-Dlchlorobenzene ND ug/L 1.0 1 08/09/0812:16 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 08/09/08 12:16 75-71-8
1,1-Dichloroethane ND ug/L 1.0 1 08/09/08 12:16 75-34-3
1,2-Dichloroethane ND ug/L 1.0 1 08/09/0812:16 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 08/09/0812:16 75-35^
cis-1,2-Dichloroethene ND ug/L 1.0 1 08/09/08 12:16 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.0 1 08/09/08 12:16 156-60-5
1,2-Dichloropropane ND ug/L 1.0 1 08/09/0812:16 78-87-5
1,3-Dichloropropane ND ug/L 1.0 1 08/09/0812:16 142-28-9
2,2-Dichloropropane ND ug/L 1.0 1 08/09/08 12:16 594-20-7
1,1-Dichloropropene ND ug/L 1.0 1 08/09/08 12:16 563-58-6
cis-1,3-Dichloropropene ND ug/L 1.0 1 08/09/08 12:16 10061-01-5
trans-1,3-Dichloropropene ND ug/L 1.0 1 08/09/08 12:16 10061-02-6
Diisopropyl ether ND ug/L 1.0 1 08/09/0812:16 108-20-3
Ethylbenzene ND ug/L 1.0 1 08/09/08 12:16 100-41-4
Hexachloro-1,3-butadiene ND ug/L 1.0 1 08/09/08 12:16 87-68-3
2-Hexanone ND ug/L 5.0 1 08/09/08 12:16 591-78-6
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 31 of 48
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9224817
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Pace Analytical Services, Inc.
2225 Riverside Dr.
Asiieviiie, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-8 Lab ID: 9224817015 Collected: 08/05/08 09:35 Received: 08/05/08 13:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No.
8260 MSV Low Level Analytical Method: EPA 8260
p-lsopropyltoluene ND ug/L 1.0 1 08/09/08 12:16 99-87-6
Methylene Chloride ND ug/L 2.0 1 08/09/08 12:16 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 08/09/08 12:16 108-10-1
Methyl-tert-butyl ether ND ug/L 1.0 1 08/09/08 12:16 1634-04-4
Naphthalene ND ug/L 1.0 1 08/09/08 12:16 91-20-3
Styrene ND ug/L 1.0 1 08/09/08 12:16 100^2-5
1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 12:16 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 08/09/08 12:16 79-34-5
Tetrachloroethene ND ug/L 1.0 1 08/09/0812:16 127-18-4
Toluene ND ug/L 1.0 1 08/09/0812:16 108-88-3
1,2,3-Trichlorobenzene ND ug/L 1.0 1 08/09/08 12:16 87-61-6
1,2,4-Trichlorobenzene ND ug/L 1.0 1 08/09/08 12:16 120-82-1
1,1,1-Trichloroethane ND ug/L 1.0 1 08/09/08 12:16 71-55-6
1,1,2-Trichloroethane ND ug/L 1.0 1 08/09/08 12:16 79-00-5
Trichloroethene ND ug/L 1.0 1 08/09/0812:16 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 08/09/08 12:16 75-69-4
1,2,3-Trichloropropane ND ug/L 1.0 1 08/09/08 12:16 96-18-4
Vinyl acetate ND ug/L 2.0 1 08/09/08 12:16 108-05-4
Vinyl chloride ND ug/L 1.0 1 08/09/08 12:16 75-01^
m&p-Xylene ND ug/L 2.0 1 08/09/08 12:16 1330-20-7
o-Xylene ND ug/L 1.0 1 08/09/0812:16 95-47-6
4-Bromofluorobenzene (S) 97 % 87-109 1 08/09/0812:16 460-00-4
Dibromofluoromethane (S) 97 % 85-115 1 08/09/08 12:16 1868-53-7
1,2-Dichloroethane-d4 (S) 101 % 79-120 1 08/09/08 12:16 17060-07-0
Toluene-d8 (S) 99 % 70-120 1 08/09/08 12:16 2037-26-5
5210B BOD, Low Level Analytical Method: SM 521 OB
BOD, 5 day ND mg/L 2.0 1 08/06/08 13:45 08/11/08 14:00
353.2 Nitrogen, N02/N03 unpres Analytical Method: EPA 353.2
Nitrogen, Nitrate 3.6 mg/L 0.10 1 08/05/0823:13
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand ND mg/L 25.0 1 08/08/08 20:05
ASTM D516-90 Sulfate Water Analytical Method: ASTM D516-90
Sulfate ND mg/L 5.0 1 08/07/08 17:55 14808-79-8
Qual
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 32 of 48
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without the written consent of Pace Analytical Services, Inc..
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2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asiieviiie, NC 28804 Huntersviiie, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Sample: MW-11 Lab ID: 9224817016 Collected: 08/05/08 09:25 Received: 08/05/08 13:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Metiiod: EPA6010 Preparation Method: EPA 3010
Iron 633 ug/L 50.0 1 08/06/08 14:40 08/13/08 21:01 7439-89-6
Manganese 36.4 ug/L 5.0 1 08/06/08 14:40 08/13/08 21:01 7439-96-5
60.10 MET ICP, Lab Filtered Analytical Method: EPA 6010 Preparation Method: EPA 3010
Iron ND ug/L 50.0 1 08/12/08 14:46 08/13/08 20:18 7439-89-6
Manganese 20.4 ug/L 5.0 1 08/12/0814:46 08/13/08 20:18 7439-96-5
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 25.0 1 08/09/08 12:40 67-64-1
Benzene ND ug/L 1.0 1 08/09/08 12:40 71-43-2
Bromobenzene ND ug/L 1.0 1 08/09/08 12:40 108-86-1
Bromochloromethane ND ug/L 1.0 1 08/09/08 12:40 74-97-5
Bromodichloromethane ND ug/L 1.0 1 08/09/08 12:40 75-27-4
Bromoform ND ug/L 1.0 1 08/09/08 12:40 75-25-2
Bromomethane ND ug/L 5.0 1 08/09/08 12:40 74-83-9
2-Butanone (MEK) ND ug/L , 5.0 1 08/09/08 12:40 78-93-3
Carbon tetrachloride ND ug/L 1.0 1 08/09/08 12:40 56-23-5
Chlorobenzene ND ug/L 1,0 1 08/09/08 12:40 108-90-7
Chloroethane ND ug/L 1.0 1 08/09/08 12:40 75-00-3
Chlorofonn 15.5 ug/L 1.0 1 08/09/08 12:40 67-66-3
Chloromethane ND ug/L 1.0 1 08/09/08 12:40 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 08/09/08 12:40 95-49-8
4-Chlorotoluene ND ug/L 1.0 1 08/09/08 12:40 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 3.0 1 08/09/08 12:40 96-12-8
Dibromochloromethane ND ug/L 1.0 1 08/09/08 12:40 124-48-1
1,2-Dibromoefhane (EDB) ND ug/L 1.0 1 08/09/08 12:40 106-93-4
Dibromomethane ND ug/L 1.0 1 08/09/08 12:40 74-95-3
1,2-Dichlorobenzene ND ug/L 1.0 1 08/09/08 12:40 95-50-1
1,3-Dichlorobenzene ND ug/L 1.0 1 08/09/08 12:40 541-73-1
1,4-Dichlorobenzene ND ug/L 1.0 1 08/09/08 12:40 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 08/09/08 12:40 75-71-8
1,1-Dichloroethane 4.9 ug/L 1.0 1 08/09/08 12:40 75-34-3
1,2-Dichloroethane ND ug/L 1.0 1 08/09/08 12:40 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 08/09/08 12:40 75-35-4
cis-1,2-Dichloroethene 1.5 ug/L 1.0 1 08/09/08 12:40 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.0 1 08/09/08 12:40 156-60-5
1,2-Dichloropropane ND ug/L 1.0 1 08/09/08 12:40 78-87-5
1,3-Dichloropropane ND ug/L 1.0 1 08/09/08 12:40 142-28-9
2,2-Dlchloropropane ND ug/L 1.0 1 08/09/08 12:40 594-20-7
1,1-Dlchloropropene ND ug/L 1.0 1 08/09/08 12:40 563-58-6
cis-1,3-Dichloropropene ND ug/L 1.0 1 08/09/08 12:40 10061-01-5
trans-1,3-Dichloropropene ND ug/L 1.0 1 08/09/08 12:40 10061-02-6
Diisopropyl ether ND ug/L 1.0 1 08/09/08 12:40 108-20-3
Ethylbenzene ND ug/L 1.0 1 08/09/08 12:40 100-41-4
Hexachloro-1,3-butadiene ND ug/L 1.0 1 08/09/08 12:40 87-68-3
2-Hexanone ND ug/L 5.0 1 08/09/08 12:40 591-78-6
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page33of48
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Project: PSNC 1080186-01
Pace Project No.: 9224817
This report shaii not be reproduced, except in fuii,
without the written consent of Pace Anaiytical Services, Inc..
mAnalytical
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Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: PSNC 1080186-01
Pace Project No.: 9224817
Sample: MW-11 Lab ID: 9224817016 Collected: 08/05/08 09:25 Received: 08/05/0813:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Metiiod: E'PA 8260
p-lsopropyltoluene ND ug/L 1.0 1 08/09/08 12:40 99-87-6
Mettiylene Ctiloride ND ug/L 2.0 1 08/09/08 12:40 75-09-2
4-Mettiyl-2-pentanone (MIBK) ND ug/L 5.0 1 08/09/0812:40 108-10-1
Metiiyl-tert-butyl ettier ND ug/L 1.0 1 08/09/08 12:40 1634-04-4
Naphtiialene ND ug/L 1.0 1 08/09/0812:40 91-20-3
Styrene ND ug/L 1.0 1 08/09/08 12:40 100-42-5
1,1,1,2-Tetrachloroettiane ND ug/L .1.0 1 08/09/0812:40 630-20-6
1,1,2,2-Tetractiloroethane ND ug/L 1.0 1 08/09/08 12:40 79-34-5
Tetractiloroetiiene ND ug/L 1.0 1 08/09/08 12:40 127-18-4
Toluene ND ug/L 1.0 1 08/09/08 12:40 108-88-3
1,2,3-Trictilorobenzene ND ug/L 1.0 1 08/09/0812:40 87-61-6
1,2,4-Trichlorobenzene ND ug/L 1.0 1 08/09/08 12:40 120-82-1
1,1,1-Trichloroethane ND ug/L 1.0 1 08/09/08 12:40 71-55-6
1,1,2-Trichloroethane ND ug/L 1.0 1 ' 08/09/08 12:40 79-00-5
Trichloroethene ND ug/L 1.0 1 08/09/08 12:40 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 08/09/08 12:40 75-69-4
1,2,3-Trichloropropane ND ug/L 1.0 1 08/09/08 12:40 96-18-4
Vinyl acetate ND ug/L 2.0 1 08/09/08 12:40 108-05-4
Vinyl chloride ND ug/L 1.0 1 08/09/0812:40 75-01-4
m&p-Xylene ND ug/L 2.0 1 08/09/08 12:40 1330-20-7
o-Xylene ND ug/L 1.0 1 08/09/08 12:40 95-47-6
4-Bromofluorobenzene (S) 99 % 87-109 1 08/09/08 12:40 460-00-4
Dibromofluoromethane (S) 100 % 85-115 1 08/09/08 12:40 1868-53-7
1,2-Dichloroethane-d4 (S) 102 % 79-120 1 08/09/08 12:40 17060-07-0
Toluene-d8 (S) 99 % 70-120 1 08/09/08 12:40 2037-26-5
521 OB BOD, Low Level Analytical Method: SM 521 OB
BOD, 5 day ND mg/L 2.0 1 08/06/08 07:00 08/11/08 09:00
353.2 Nitrogen, N02/N03 unpres Analytical Method: EPA 353.2
Nitrogen, Nitrate 1.6 mg/L 0.10 1 08/05/08 23:13
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand ND mg/L 25.0 1 08/08/08 20:05
ASTM D516-90 Sulfate Water Analytical Method: ASTM D516-90
Sulfate 19.5 mg/L 5.0 1 08/07/08 17:57 14808-79-8
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
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2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheviiie, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project; PSNC 1080186-01
Pace Project No.; 9224817
QCBatcti: WETA/3212 Analysis Metiiod; EPA 353.2
QC Batch Method; EPA 353.2 Analysis Description; 353.2 Nitrate -i- Nitrite, Unpres.
Associated Lab Samples; 9224817014, 9224817015, 9224817016
METHOD BLANK; 149236
Associated Lab Samples; 9224817014, 9224817015, 9224817016
Blank Reporting
Parameter Units Result Limit Qualifiers
Nitrogen, Nitrate mg/L ND 0.10
LABORATORY CONTROL SAMPLE;
Parameter
149237
Units
Spike LCS
Cone. Result
LCS
% Rec
% Rec
Limits Qualifiers
Nitrogen, Nitrate mg/L 5 5.2 103 90-110
MATRIX SPIKE SAMPLE;
Parameter
149238
Units
9224797002
Result
Spike
Cone.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Nitrogen, Nitrate mg/L 8.4 5 14.0 112 90-110 Ml
SAMPLE DUPLICATE; 149239
Parameter Units
9224831001
Result
Dup
Result RPD Qualifiers
Nitrogen, Nitrate mg/L 35.4 35.6 .7
mAnalytical
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Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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mAnalytical
wiw.pace/sbs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheviiie, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviiie, NC 28078
[phone]
QUALITY CONTROL DATA
Project: PSNC 1080186-01
Pace Project No.: 9224817
QC Batcii: WET/4949
QC Batcti Metiiod: SM 521 OB
Associated Lab Samples: 9224817016
Analysis Mettiod: SM 5210B
Analysis Description: 521 OB BOD, Low Level
METHOD BLANK: 149247
Associated Lab Samples: 9224817016
Parameter Units
BOD, 5 day mg/L
Blank Reporting
Result Limit Qualifiers
ND 2.0
LABORATORY CONTROL SAMPLE: 149248
Parameter Units
BOD, 5 day mg/L
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
198 196 99 84-115
SAMPLE DUPLICATE: 149249
Parameter
BOD, 5 day
Units
mg/L
9224736001 Dup
Result Result RPD Qualifiers
2.8 5.6 65 Rl
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 36 of 48
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Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheville, NC 28804 Huntersviiie, NC 28078
[phone] [phone]
DATA
QCBatcti: MPRP/2800 Analysis Method: EPA 6010
QC Batch Method: EPA 3010 ' Analysis Description: 6010 MET
Associated Lab Samples: 9224817014, 9224817015, 9224817016
METHOD BUNK: 149489
Associated Lab Samples: 9224817014, 9224817015, 9224817016
Blank Reporting
Parameter Units Result Limit Qualifiers
Iron
Manganese
ug/L
ug/L
ND
ND
50.0
5.0
UBORATORY CONTROL SAMPLE:
Parameter
149490
Units
Spike LCS
Cone. Result '
LCS
% Rec
% Rec
Limits Qualifiers
Iron
Manganese
ug/L
ug/L
5000
500
4690
476
94
95
80-120
80-120
MATRIX SPIKE SAMPLE:
Parameter
149491
Units
9224575003
Result
Spike
Cone.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Iron
Manganese
ug/L
ug/L
18400
250
5000
500
22100
683
74
87
75-125 M3
75-125
SAMPLE DUPLICATE: 149492
Parameter Units
9224575004
Result
Dup
Result RPD Qualifiers
Iron
Manganese
ug/L
ug/L
3800
69.6
3940
72.8
3
4
weAnalytical
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QUALITY CONTROL
Project: PSNC 1080186-01
Pace Project No.: 9224817
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent ot Pace Analytical Sen/ices, Inc..
Page 37 of 48
mAnalytical
wvm.pac^6bs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: PSNC 1080186-01
Pace Project No.: 9224817
QCBatcti: WET/4959
QC Batch IVIethod: SM 521 OB
Associated Lab Samples: 9224817015
METHOD BLANK: 149584
Associated Lab Samples: 9224817015
Blank Reporting
Parameter Units Result Limit Qualifiers
BOD, 5 day mg/L ND 2.0
Analysis Method: SM 5210B
Analysis Description: 521 OB BOD, Low Level
LABORATORY CONTROL SAM PLE: 149585
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
BOD, 5 day mg/L 198 202 102 84-115
SAMPLE DUPLICATE: 149586
9224817015 Dup
Parameter Units Result Result RPD Qualifiers
BOD, 5 day mg/L ND ND 0
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 38 of 48
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mAnalytical
WYm.p3Celabs.corn
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asiieviiie, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviiie, NC 28078
[phone]
QUALITY CONTROL DATA
Project: PSNC 1080186-01
Pace Project No.: 9224817
QC Batcii: WET/4962
QC Batcti IVIetiiod: SM5210B
Associated Lab Samples: 9224817014
Analysis Mettiod:
Analysis Description:
SM 521 OB
521 OB BOD, Low Level
METHOD BLANK: 149772
Associated Lab Samples: 9224817014
Parameter Units
BOD, 5 day mg/L
Blank Reporting
Result Limit Qualifiers
ND 2.0
LABORATORY CONTROL SAMPLE: 149773
Parameter Units
BOD, 5 day mg/L
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
198 255 129 84-115 B4
SAMPLE DUPLICATE: 149774
Parameter Units
9224805001
Result
Dup
Result RPD Qualifiers
BOD, 5 day mg/L 825 885 7 B4
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
Tills report stiall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
Page 39 of 48
mAnalytical
wvm.pBCelebs.com
Pace Anaiytical Services, Inc.
2225 Riverside Dr.
Astieviiie, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: PSNC 1080186-01
Pace Project No.: 9224817
QCBatcti: WETA/3222 Analysis Mettiod: ASTM D516-90
QC Batch Method: ASTM D516-90 Analysis Description: ASTM D516-90 Sulfate Water
Associated Lab Samples: 9224817014, 9224817015, 9224817016
METHOD BLANK: 150030
Associated Lab Samples: 9224817014, 9224817015, 9224817016
Blank Reporting
Parameter Units Result Limit Qualifiers
Sulfate mg/L ND 5.0
LABORATORY CONTROL SAMPLE: 150031
Parameter Units
Spike LCS
Cone. Result
LCS
% Rec
% Rec
Limits Qualifiers
Sulfate mg/L 20 19.0 95 90-110
MATRIX SPIKE SAMPLE: 150032
Parameter Units
9224836001 Spike
Result Cone.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Sulfate mg/L ND 20 19.7 90 75-125
SAMPLE DUPLICATE: 150033
Parameter Units
9224776003 Dup
Result Result RPD Qualifiers
Sulfate mg/L 11.9 12.0 .4
SAMPLE DUPLICATE: 150571
Parameter Units
9224928002 Dup
Result Result RPD Qualifiers
Sulfate mg/L 337 339 .7
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page 40 of 48
/^aceAnalytical
1" wm.T>a^Bbs.cm
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: PSNC 1080186-01
Pace Project No.: 9224817
QCBatcti: MSV/4216 Analysis Mettiod: EPA8260
QC Batcii Method: EPA 8260 Analysis Description; 8260 MSV Low Level
Associated Lab Samples' 9224817001, 9224817002, 9224817003, 9224817004, 9224817005, 9224817006, 9224817007, 9224817008,
9224817009, 9224817010,9224817011, 9224817012, 9224817013, 9224817014, 9224817015, 9224817016
METHOD BIJ^NK: 151298
Associated Lab Samples: 9224817001, 9224817002, 9224817003, 9224817004, 9224817005, 9224817006, 9224817007, 9224817008,
9224817009, 9224817010,9224817011, 9224817012, 9224817013, 9224817014,9224817015,9224817016
Blank Reporting
Parameter Units Result Limit Qualifiers
1,1,1,2-Tetrachloroethane ug/L ND 1.0
1,1,1-Trichloroethane ug/L ND 1.0
1,1,2,2-Tetrachloroethane ug/L ND 1.0
1,1,2-Trichloroethane ug/L ND 1.0
1,1-Dichloroethane ug/L ND 1.0
1,1-Dichloroethene ug/L ND 1.0
1,1-Dlchloropropene ug/L ND 1.0
1,2,3-Trichlorobenzene ug/L ND 1.0
1,2,3-Trichloropropane ug/L ND 1.0
1,2,4-Trichlorobenzene ug/L ND 1.0
1,2-Dibromo-3-chloropropane ug/L ND 3.0
1,2-Dibromoethane (EDB) ug/L ND 1.0
1,2-Dlchlorobenzene ug/L ND 1.0
1,2-Dlchloroethane ug/L ND 1.0
1,2-Dichloropropane ug/L ND 1.0
1,3-Dichlorobenzene ug/L " ND 1.0
1,3-Dlchloropropane ug/L ND 1.0
1,4-Dlchlorobenzene ug/L ND 1.0
2,2-Dlchloropropane ug/L ND 1.0
2-Butanone (MEK) ug/L ND 5.0
2-Chlorotoluene ug/L ND 1.0
2-Hexanone ug/L ND 5.0
4-Chlorotoluene ug/L ND 1.0
4-Methyl-2-pentanone (MIBK) ug/L ND 5.0
Acetone ug/L ND 25.0
Benzene ug/L ND 1.0
Bromobenzene ug/L ND 1.0
Bromochloromethane ug/L ND 1.0
Bromodichloromethane ug/L ND 1.0
Bromoform ug/L ND 1.0
Bromomethane ug/L ND 5.0
Carbon tetrachloride ug/L ND 1.0
Chlorobenzene ug/L ND 1.0
Chloroethane ug/L ND 1.0
Chloroform ug/L ND 1.0
Chloromethane ug/L ND 1.0
cis-1,2-Dichloroethene ug/L ND 1.0
cis-1,3-Dichloropropene ug/L ND 1.0
Dibromochloromethane ug/L ND 1.0
Dibromomethane ug/L ND 1.0
Dichlorodifluoromethane ug/L ND 1.0
Date; 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 41 of 48
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mAnalytical
www.paceltbs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asiieville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: PSNC 1080186-01
Pace Project No.: 9224817
METHOD BUWK: 151298
Associated Lab Samples: 9224817001, 9224817002, 9224817003, 9224817004, 9224817005, 9224817006, 9224817007, 9224817008,
9224817009, 9224817010, 9224817011, 9224817012, 9224817013, 9224817014, 9224817015, 9224817016
Blank Reporting
Parameter Units Result Limit
Diisopropyl ettier ug/L ND 1.0
Ettiylbenzene ug/L ND 1.0
Hexactiloro-1,3-butadiene ug/L ND 1.0
m&p-Xylene ug/L ND 2.0
Methyl-tert-butyl ether ug/L ND 1.0
Methylene Chloride ug/L ND 2.0
Naphthalene ug/L ND 1.0
o-Xylene ug/L ND 1.0
p-lsopropyltoluene ug/L ND 1.0
Styrene ug/L ND 1.0
Tetrachloroethene ug/L ND 1.0
Toluene ug/L ND 1.0
trans-1,2-Dichloroethene ug/L ND 1.0
trans-1,3-Dichloropropene ug/L ND 1.0
Trichloroethene ug/L ND 1.0
Trichlorofluoromethane ug/L ND 1.0
Vinyl acetate ug/L ND 2.0
Vinyl chloride ug/L ND 1.0
1,2-Dichloroethane-d4 (S) % 101 79-120
4-Bromofluorobenzene (S) % 97 87-109
Dibromofluoromethane (S) % 99 85-115
Toluene-d8 (S) % 99 70-120
LABORATORY CONTROL SAMPLE; 151299
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits
1,1,1,2-Tetrachloroethane ug/L 50 51.2 102 83-125
1,1,1-Trichloroethane ug/L 50 50.5 101 80-129
1,1,2,2-Tetrachloroethane ug/L 50 46.4 93 73-127
1,1,2-Trichloroethane ug/L 50 52.0 104 77-123
1,1-Dlchloroethane ug/L 50 51.4 103 76-129
1,1-Dichloroethene ug/L 50 51.8 104 78-146
1,1-Dlchloropropene ug/L 50 49.9 100 79-134
1,2,3-Trichlorobenzene ug/L 50 41.6 83 70-150
1,2,3-Trichloropropane ug/L 50 50.5 101 72-125
1,2,4-Trichlorobenzene ug/L 50 41.6 83 68-127
1,2-Dlbromo-3-chloropropane ug/L 50 48.3 97 65-128
1,2-Dibromoethane (EDB) ug/L 50 52.1 104 81-125
1,2-Dlchlorobenzene ug/L 50 51.8 104 82-126
1,2-Dichloroethane ug/L 50 50.7 101 72-126
1,2-Dlchloropropane ug/L 50 50.9 102 80-127
1,3-Dichlorobenzene ug/L 50 49.4 99 82-124
1,3-Dichloropropane ug/L 50 50.7 101 79-124
1,4-Dichlorobenzene ug/L 50 50.2 100 79-125
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 42 of 48
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mAnalytical
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Pace Analytical Services, Inc.
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project; PSNC 1080186-01
Pace Project No.; 9224817
lUBOfWORY CONTROL SAMPLE; 151299
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits
2,2-Dictiloropropane ug/L 50 51.8 104 58-140
2-Butanone (MEK) ug/L 100 106 106 50-134
2-Clilorotoluene ug/L 50 49.9 100 81-126
2-Hexanone ug/L 100 106 106 58-138
4-Chlorotoluene ug/L 50 52.0 104 82-126
4-Methyl-2-pentanone (MIBK) ug/L 100 107 107 70-131
Acetone ug/L 100 112 112 50-146
Benzene ug/L 50 49.4 99 78-128
Bromobenzene ug/L 50 49.5 99 81-127
Bromochloromethane ug/L 50 50.9 102 73-124
Bromodichloromethane ug/L 50 52.0 104 81-125
Brornoform ug/L 50 48.9 98 71-125
Bromomethane ug/L 50 46.0 92 50-150
Carbon tetrachloride ug/L 50 48.1 96 81-137
Chlorobenzene ug/L 50 50.1 100 82-126
Chloroethane ug/L 50 52.7 105 69-140
Chloroform ug/L 50 51.9 104 77-129
Chloromethane ug/L 50 46.4 93 54-139
cis-1,2-Dichloroethene ug/L 50 52.1 104 76-133
cis-1,3-pichloropropene ug/L 50 51.2 102 76-127
Dibromochloromethane ug/L 50 52.6 105 77-125
Dibromomethane ug/L 50 53.3 107 77-125
Dichlorodifluoromethane ug/L 50 47.9 • 96 50-150
Diisopropyl ether ug/L 50 49.3 99 74-131
Ethylbenzene ug/L 50 49.3 99 80-127
Hexachloro-1,3-butadiene ug/L 50 50.4 101 78-145
m&p-Xylene ug/L 100 86.3 86 82-127
Methyl-tert-butyl ether ug/L 50 50.6 101 71-130
Methylene Chloride ug/L 50 54.3 109 67-133
Naphthalene ug/L 50 54.9 110 52-136
o-Xylene ug/L 50 48.5 97 83-124
p-lsopropyltoluene ug/L 50 50.5 101 73-122
Styrene ug/L 50 53.1 106 80-130
Tetrachloroethene ug/L 50 49.0 98 78-128
Toluene ug/L 50 48.0 96 76-126
trans-1,2-Dichloroethene ug/L 50 50.8 102 78-134
trans-1,3-Dichloropropene ug/L 50 53.1 106 75-125
Trichloroethene ug/L 50 52.4 105 79-127
Trichlorofluoromethane ug/L 50 47.5 95 76-148
Vinyl acetate ug/L 100 68.9 69 50-150
Vinyl chloride ug/L 50 50.3 101 67-143
1,2-Dichloroethane-d4 (S) % 100 79-120
4-Bromofluorobenzene (S) % 99 87-109
Dibromofluoromethane (S) % 101 85-115
Toluene-d8 (S) % 100 70-120
Date; 08/19/2008 08;25AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 43 of 48
mAnalyticaf
www.p8celabs.ixM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheviiie, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviiie, NC 26078
[phone]
QUALITY CONTROL DATA
Project: PSNC 1080186-01
Pace Project No.: 9224817
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 151335 151336
Parameter Units
9224817004
Result
MS
Spike
Cone.
MSD
Spike
Cone.
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits RPD
1,1-Dichloroethene ug/L ND 50 50 53.2 49.5 106 99 60-150 7
Benzene ug/L ND 50 50 53.1 50.7 106 101 74-136 5
Chlorobenzene ug/L ND 50 50 52.4 50.6 105 101 79-135 3
Toluene ug/L ND 50 50 51.4 48.8 103 98 73-131 5
Trichloroethene ug/L ND 50 50 52.8 50.4 106 101 73-131 5
1,2-Dlchloroethane-d4 (S) % 98 100 79-120
4-Bromofiuorobenzene (S) % 98 99 87-109
Dibromofluoromethane (S) % 96 96 85-115
Toluene-d8 (S) % 99 99 70-120
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, inc.
Page 44 of 48
mAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheviiie, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviiie, NC 28078
[phone]
QUALITY CONTROL DATA
Project: PSNC 1080186-01
Pace Project No.: 9224817
QC Batcii: WETA/3236 Analysis IVIetliod: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 9224817014, 9224817015, 9224817016
METHOD BLANK: 151412
Associated Lab Samples: 9224817014, 9224817015, 9224817016
Blank Reporting
Parameter Units Result Limit Qualifiers
Chemical Oxygen Demand mg/L ND 25.0
UBORATORY CONTROL SAMPLE: 151413
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 758 101 90-110
MATRIX SPIKE SAMPLE: 151414
9224345001 Spike MS MS % Rec
Parameter Units Result Cone. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 129 750 853 97 75-125
MATRIX SPIKE SAMPLE: 151416
9224940001 Spike MS MS % Rec
Parameter Units Result Cone. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 8180 6000 13300 85 75-125
SAMPLE DUPLICATE: 151415
9224355001 Dup
Parameter Units Result Result RPD Qualifiers
Chemical Oxygen Demand mg/L ND ND
S/WIPLE DUPLICATE: 151417
9224942002 Dup
Parameter Units Result Result RPD Qualifiers
Chemical Oxygen Demand mg/L 375 364
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
Page 45 of 48
mAnalytical
v/nM.pacelabs.com
Pace Analytical Services, inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: PSNC 1080186-01
Pace Project No.: 9224817
QC Batcti: MPRP/2823 Analysis Mettiod: EPA 6010
QC Batcti Mettiod: EPA 3010 Analysis Description: 6010 MET Filtered
Associated Lab Samples: 9224817014, 9224817015, 9224817016
METHOD BLANK: 151636
Associated Lab Samples: 9224817014, 9224817015, 9224817016
Blank Reporting
Parameter Units Result Limit Qualifiers
Iron, Dissolved ug/L ND 50.0
Manganese, Dissolved ug/L ND 5.0
LABORATORY CONTROL SAMPLE: 151637
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Iron, Dissolved ug/L 5000 4390 88 80-120
Manganese, Dissolved ug/L 500 444 89 80-120
MATRIX SPIKE SAMPLE: 151638
9224817014 Spike MS MS % Rec
Parameter Units Result Cone. Result % Rec Limits Qualifiers
Iron, Dissolved ug/L ND 5000 4030 80 75-125
Manganese, Dissolved ug/L 159 500 543 77 75-125
SAMPLE DUPLICATE: 151639
9224817015 Dup
Parameter Units Result Result RPD Qualifiers
Iron, Dissolved ug/L ND 21.8J 77 R3
Manganese, Dissolved ug/L 76.1 76.9 1
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 46 of 48
mAnalytical'
wm/.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: PSNC 1080186-01
Pace Project No.: 9224817 ^
DEFINITIONS
DF - Dilution Factor, If reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
S - Sun^ogate
1,2-biphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the cun-ent list of accredited analytes.
ANALYTE QUALIFIERS
B2 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.
B4 The glucose/glutamic acid standard exceeded the range of 198 plus or minus 30.5 mg/L.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M3 Matrix spike recovery was outside laboratory control limits due to matrix interferences.
Rl RPD value was outside control limits.
R3 RPD value was outside control limits due to uncertainty of values at or near the PRL.
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page 47 of 48
This report shall not be repnaduced, except in full,
wilhout the written consent of Pace Analytical Services, Inc.
mAnalytical
wwi//.pace!abs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asiieville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: PSNC 1080186-01
Pace l^roject No.: 9224817
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
9224817014 MW-3 EPA 353.2 WETA/3212
9224817015 MW-8 EPA 353.2 WETA/3212
9224817016 MW-11 EPA 353.2 WETA/3212
9224817016 MW-11 SM 5210B WET/4949 SM5210B WET/5013
9224817014 MW-3 EPA 3010 MPRP/2800 EPA 6010 ICP/2659
9224817015 MW-8 EPA 3010 MPRP/280O EPA 6010 ICP/2659
9224817016 MW-11 EPA 3010 MPRP/2800 EPA 6010 ICP/2659
9224817015 MW-8 SM 5210B WET/4959 SM5210B WET/5017
9224817014 MW-3 SM 521 OB WET/4962 SM 5210B WET/4965
9224817014 MW-3 ASTM D516-90 WET/V3222
9224817015 MW-8 ASTM D516-90 WETA/3222
9224817016 MW-11 ASTM D516-90 WETA/3222
9224817001 MW-1 EPA 8260 MSV/4216
9224817002 MW-2 EPA 8260 MSV/4216
9224817003 MW-4 EPA 8260 MSV/4216
9224817004 MW-5 EPA 8260 MSV/4216
9224817005 MW-6 EPA 8260 MSV/4216
9224817006 MW-7 EPA 8260 MSV/4216
9224817007 MW-9 EPA 8260 MSV/4216
9224817008 MW-10 EPA 8260 MSV/4216
9224817009 MW-12 EPA 8260 MSV/4216
9224817010 MW-13 EPA 8260 MSV/4216
9224817011 MW-14 EPA 8260 MSV/4216
9224817012 MW-15 EPA 8260 MSV/4216
9224817013 MW-160 EPA 8260 MSV/4216
9224817014 MW-3 EPA 8260 MSV/4216
9224817015 MW-8 EPA 8260 MSV/4216
9224817016 MW-11 EPA 8260 MSV/4216
9224817014 MW-3 SM 5220D WETA/3236
9224817015 MW-8 SM 5220D WET/V3236
9224817016 MW-11 SM 5220D WETA/3236
9224817014 MW-3 EPA 3010 MPRP/2823 EPA 6010 ICP/2675
9224817015 MW-8 EPA 3010 MPRP/2823 EPA 6010 ICP/2675
922^-317016 MW-11 EPA 3010 MPRP/2823 EPA 6010 ICP/2675
Date: 08/19/2008 08:25 AM REPORT OF LABORATORY ANALYSIS Page48of48
Tills report stiall not be reproduced, except In full,
wilhout the written consent of Pace Analytical Services, Inc..
%ceAnalytical'
wm-HnMi-eMi
CHAIN-OF-CUSTODY/Analytical Request Document
The Chain-of-Custody is a LEGAL DOCUMENT. All relevant fields must t>e completed accurately.
Section A
Rtqulrad Client Information:
Section B
Rtqulred Project Information:
Section C
Invoice Information:
Report Toi^ > 1 A,ten«on:-j^^ ^^^^^
Copy To: company Name: ^^v^^ |
Address: r* ^
Purchase Order No.: Pace Quote '
RsfacBoce: ^
Pace Project
Manager
RequMtod Due Data/TAT: PrqjectNumber -<3) ( Pace Profile*: ^
of
1180676
GROUNDWATER F DRINKING WATER
RCRA r OTHER
Soctlon D
R«qulrad Client infbnnalion
SAMPLE ID
(A-Z,0-9/,-)
Sample IDs lulUST BE UNIQUE
Matrix Codas
MATRIX I CODE
Drinking Water DW
Water
Wastewater
Product
Soil/Solid
Oil
Wipe
Air
Tissue
Other
WT
WW
P
SL
OL
WP
AR
TS
OT
COLLECTED
COMPOSITE
START
DATE TIME
COWOSITE
END/GRAB
TIME
Preservatives
mm Pace Project No./Lab I.D.
OlO Ml
(JX
mi
X
JC
10
AOWnONAL C0llilE»ni3 mm SAMPLE CONDITIONS
ORIGINAL aamfiffinTWff'-^'iiiiiiTti'g?^ 1 itfririnfii'ii^f.,iTari„
PRINT N»n. of SAMPl£R: Ct^^j^UW jj^^ Rt\t ItK jU^lW
,«u.TUREC<"""^R:.^ 0*1-"'- 1?'^^!!?''
o ~
II ill il
'ace Analytical Client Name: Project #_2>>^^ir^
Courier: • Fed Ex • UPS • USP^^Q^nl • Commercial • Pace Other
Custody Seal on Cooler/Box Present: Dyes jQ-nT" Seals inlact: Dyes
Packing Material: • Bubble Wrap npHBgrTBags • None Dother
Thermometer Used f^^^ T Type of Ice^^^^^ Blue None
n ' Biological Tissue is Frozen: Yes i^o N/A
Optionaf
Pro; Due Date H!A
Pcoj^Na^me^flr/N/Xi:^
Cooler Temperature,
Temp should be above freezing to 6°C Comments:
Chain of Custody Present: ^r-STes DNO DN/A
Chain of Custody Filled Out: ^..^-gTe's DNO DN/A
Samples on ice, cooling process has begun
Date and inltia
contents:
2.
Chain of Custody Relinquished: lYes DNO DN/A
SamplerName & Signature on COC: ^ ONO DN/A
Samples Arrived within Hold Time: N/A
Short Hold Time Analysis (<72hr): JYes DNO DN/A
Rush Turn Around Tinne Requested: •Yes JSMS^DN/A
Sufficient Volume: feT DNO DN/A
Correct Containers Used:
-Pace Containers Used:
^^,.Bm DNO DN/A
^,^S7e% DNO- DN/A
9.
Containers Intact: fes DNO DN/A
Filtered volume received for Dissolved tests DYes (Bf^^^J^if^ T -0 \
Sample Labels match COC:
-Includes date/time/ID/Analysis
]Yes DNO DN/A 12.
Matrix:
All containers needing preservation have been checked.
All containers needing preservation are found to be in
compliance with EPA recommendation.
exceplions: VOA, collform. TOC. Q&G, WI-DRO (water)
^,0^ DNO ON/A
^^D^^^OHO DN/A
• Yes QNO
^>dYes
13.
Inilial when completed
Samples checked for dechlorination: •NO •N/A 14.
Headspace in VOA Vials ( >6mm):
Trip Blank Present:
•N/A 15.
Trip Blank Custody Seals Present
^ace Trip Blank Lot # (if purchased): N/A
• Yes GNO
• Yes QNO •NJ
I^lient Notification/ Resolution;
Person Contacted:
Comments/ Resolution:
J , rieia uai;
Date/Time:
Field Data Required? Y / N / N/A
X)errX ^<P^ c MO PiOW^JU^ec^ uf/J^^^
Project Manager Review:
oie: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
- erllfication Office (i.e out of hold, incorrect preservative, out of temp, incorrect containers)
Pace Analytical Services, Inc.
1700 Elm street
Minneapolis, MN 55414
[phone]
August 18, 2008
Client Servities
Pace Analytical Charlotte
9800 Kincey Ave.
Suite 100
Huntersville, NC 28078
RE; Project; 9224817 SHIELD
Pace Project No.: 1078310
Dear Client Services:
Enclosed are the analytical results for sample(s) received by the laboratory on August 05, 2008. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body ofthe
report.
Ifyou have any questions concerning this report, please feel free to contact me.
Sylvia Hunter
Sylvia.hunter(gpacelabs.com
Project Manager
Florida (Nelap) Certification #: E87605
Illinois Certlficati m #: 200011
Iowa Certification #: 368
Minnesota Certification #; 027-053-137
Wisconsin Certification #: 999407970
Enclosures
Sincerely,
REPORT OF LABORATORY ANALYSIS Page 1 of 5
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.,
mAnalytical
www.pBcelibs.com
Pace Analytical Services, Inc.
1700 Elm Street
Minneapolis, MN 55414
[phone]
ANALYTICAL RESULTS
Project: 9224817 SHIELD
Pace Project No.: 1078310
Sample: MW-3
Parameters
Lab ID: 9224817014 Collected: 08/05/08 11:10 Received: 08/05/08 13:25 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK175 AIR Headspace
Ethane
Ethene
Methane
Analytical Method: RSK 175
ND ug/L
ND ug/L
ND ug/L
20.0 1
20.0 1
10.0 1
08/15/08 11:45 74-84-0
08/15/08 11:45 74-85-1
08/15/08 11:45 74-82-8
Sample: MW-8
Parameters
Lab ID: 9224817015 Collected: 08/05/08 09:35 Received: 08/05/08 13:25 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace
Ethane
Ethene
Methane
Analytical Method: RSK 175
ND ug/L
ND ug/L
ND ug/L
20.0 1
20.0 1
10.0 1
08/15/08 12:10 74-84-0
08/15/08 12:10 74-85-1
08/15/08 12:10 74-82-8
Sample: MW-11 Lab ID: 9224817016 Collected: 08/05/08 09:25 Received: 08/05/0813:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace Analytical Method: RSK 175
Ethane ND ug/L 20.0 1 08/15/08 12:36 74-84-0
Ethene ND ug/L 20.0 1 08/15/08 12:36 74-85-1
Methane ND ug/L 10.0 1 08/15/08 12:36 74-82-8
Date: 08/18/2008 07:16 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fuii,
without the written consent of Pace Anaiyticai Sen/ices, inc..
Page 2 of 5
mAnalytical
www.pace!Bbi,com
Pace Analytical Services, Inc.
1700 Elm Street
Minneapolis, MN 55414
[phone]
QUALITY CONTROL DATA
Project: 9224817 SHIELD
Pace Project No.: 1078310
QC Batcti:
QC Batch Method:
AIR/7282
RSK 175
Analysis Method:
Analysis Description:
RSK 175
RSK 175 AIR HEADSPACE
Associated Lab Samples: 9224817014, 9224817015, 9224817016
METHOD BLANK: 512809
Associated Lab Samples: 9224817014, 9224817015, 9224817016
Blank
Parameter Units Result
Reporting
Limit Qualifiers
Ethane
Ethene
Methane
ug/L
ug/L
ug/L
ND
ND
ND
20.0
20.0
10.0
LABORATORY CONTROL SAMPLE & LCSD: 512810
Parameter Units
Spike
Cone.
512811
LCS LCSD
Result Result
LCS
% Rec
LCSD
% Rec
% Rec
Limits RPD
Max
RPD Qualiriers
Ethane ug/L 114 159 132 140 116 70-130 19 30 CU
Ethene ug/L 106 146 118 137 111 70-130 21 30 CU
Methane ug/L 60.7 78.7 65.2 130 107 70-130 19 30
Date: 08/18/2008 07:16 AM REPORT OF LABORATORY ANALYSIS
Ttils report shaii not be reproduced, except in fuil,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 5
Pace Analytical Services, Inc.
1700 Elm Street
Minneapolis, IVIN 55414
[phone]
QUALIFIERS
Project: 9224817 SHIELD
Pace Project No.: 1078310
DEFINITIONS
DF - Dilution Factor, If reported, represents ttie factor applied to ttie reported data due to ctianges in sample preparation, dilution of
ttie sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below/ the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
S - Surrogate
1,2-Dlphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC-Not Calculable.
Pace Analytical Is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
ANALYTE QUALIFIERS
CU The continuing calibration for this compound is outside of Pace Analytical acceptance limits. Analyte presence below
reporting limits in associated samples. Results unaffected by high bias.
weAnalytical
wm.pacelabs.coin
Date: 08/18/2008 07:16 AM REPORT OF LABORATORY ANALYSIS Page 4 of 5
Ttiis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, inc.
aceAnalytical
WMw.pacs/sbs.com
Pace Analytical Services, Ino.
1700 Elm Street
Minneapolis, MN 55414
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
9224817 SHIELD
1078310
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
9224817014
9224817015
9224817016
MW-3
MW-8
MW-11
RSK 175
RSK 175
RSK 175
AIR/7282
AIR/7282
AIR/7282
Date: 08/18/2008 07:16 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 5