U-3440_023 PSA_Baker Property-Bethpage Dump-

NC Department of Transportation – Preliminary Site Assessment
Jerry H Baker Property, Bethpage Dump
August 26, 2011

AMEC of North Carolina Inc
NCDOT State Project: U-3440, WBS Element: 39010.1.1
AMEC Project: 562113440

i

TABLE OF CONTENTS

1.0 INTRODUCTION ....................................................................................................... 1

1.1 Site Location and Vicinity ............................................................................ 1
1.2 Site Description and History ....................................................................... 2

2.0 GEOLOGY ................................................................................................................. 2

2.1 Regional Geology ......................................................................................... 2
2.2 Site Geology ................................................................................................. 2

3.0 FIELD ACTIVITIES .................................................................................................... 3

3.1 Site Reconnaissance ................................................................................... 3
3.2 Preliminary Activities ................................................................................... 3
3.3 Soil Sampling ................................................................................................ 4

4.0 SOIL SAMPLING RESULTS ..................................................................................... 5

5.0 CONCLUSIONS ......................................................................................................... 6

6.0 RECOMMENDATIONS .............................................................................................. 7
NC Department of Transportation – Preliminary Site Assessment
Jerry H Baker Property, Bethpage Dump
August 26, 2011

AMEC of North Carolina Inc
NCDOT State Project: U-3440, WBS Element: 39010.1.1
AMEC Project: 562113440

ii
TABLES
Table 1 PID Field Screening
Table 2 Soil Sampling Analytical Results

FIGURES
Figure 1 Vicinity Map
Figure 2 Site Map with Previous Assessment Locations
Figure 3 Site Map with Sampling Locations
Figure 4 Site Map with Analytical Detections (Shallow Samples)
Figure 5 Site Map with Analytical Detections (Deep Samples)
Figure 6 Site Map with Estimated Area of Contamination and Extent of Debris Field

APPENDICES
Appendix A Photo Log
Appendix B Excavation Logs
Appendix C Laboratory Analytical Data

NC Department of Transportation – Preliminary Site Assessment
Jerry H Baker Property, Bethpage Dump
August 26, 2011

AMEC of North Carolina Inc
NCDOT State Project: U-3440, WBS Element: 39010.1.1
AMEC Project: 562113440
1
1.0 INTRODUCTION

In accordance with the North Carolina Department of Transportation (NCDOT) Request for
Proposal, dated June 1, 2011, AMEC North Carolina Inc. (AMEC) has performed a
Preliminary Site Assessment (PSA) for the Jerry H Baker Property (the Site) to be effected
by a road improvement project along NC 3 (Mooresville Rd) in support of the proposed
West Side Bypass to SR 1691 (Loop Rd) project. The Site is located on the southwest
quadrant of the intersection of Mooresville Road and Bethpage Road in Kannapolis North
Carolina. According to the property owner, a construction contractor used this site as a
dump in the 1980s. The property owner stated that the dumped material consisted of tires,
general construction debris, and oil drums. The oil drums were sampled and removed in
2006. According to NCDENR’s Division of Waste management this site is not listed as an
active or inactive facility and is not listed on the “old non-permitted landfill inventory.”

NCDOT contracted AMEC to perform a PSA on the Jerry H Baker Property because
historically the site operated as an unregistered landfill. This PSA was performed to
identify the extent and depth of buried debris; determine whether contaminated soils are
present; determine contaminant nature of soil matrix within debris; and if applicable,
estimate the quantity and extent of impacted soil. The PSA activities took place along the
right of way (ROW) and to ten feet beyond the construction easement. This assessment
was conducted in accordance with AMEC’s Technical and Cost proposal dated June 20,
2011.

The following report presents the site history; field activities and methodologies; subsurface
lithology; extent and content of debris fill; soil sampling results; and an estimate of the
quantity of impacted soils. The report includes evaluation of the analytical data with
regards to the presence or absence of soil contamination within the NCDOT design area of
the Bethpage dump.

1.1 Site Location and Vicinity

The Jerry H Baker Property is located on the southwest quadrant of Mooresville Road and
Bethpage Road in Kannapolis, Cabarrus County, North Carolina, as shown in Figure 1.
The property to the north is agricultural. Walter M. Safrit Park is located south of the site.
The property to the east is residential with a single family home and the property to the
west is wooded.

NC Department of Transportation – Preliminary Site Assessment
Jerry H Baker Property, Bethpage Dump
August 26, 2011

AMEC of North Carolina Inc
NCDOT State Project: U-3440, WBS Element: 39010.1.1
AMEC Project: 562113440
2

1.2 Site Description and History

The Site is currently a vacant lot; however it historically operated as an unregistered dump
for construction debris. The proposed DOT project will involve an expanded ROW and
construction easement. The property owner stated that the dumped materials consisted of
tires, general construction debris, and oil drums. The oil drums were sampled and
removed in 2006. In May 2008, Environmental Services were performed for the property
owner Mr. Jerry Baker by CESI Land Development Services of Concord, North Carolina
(CESI). On May 5, 2008 a subcontractor to CESI excavated 23 test pits across the Site and
these former test pits are shown in Figure 2. Debris was noted in 21 of the 23 test pits.
Debris consisted of tree stumps, logs, concrete, brick, tires and household trash. CESI
indicated that the debris layer ranged from 4 to 18 feet in thickness. Two metal
underground storage tanks were excavated from the test pits. No staining or odors were
noted. Six storage tanks were observed on the ground surface. One of the six tanks had
signs of staining underneath. At that time a shovel was used to excavate the apparent spill.
Staining was not noted beyond six inches bgs and no sampling was conducted as part of
the activities.
During a June 2011 site visit, the site was observed to be quite overgrown with vegetation
except in the center of the property. Some debris piles were noted at ground surface in the
investigation area of the Site, predominantly along Mooresville Road. These piles were
overgrown with vegetation and not very distinguishable in extent or content. Appendix A
includes a photo log for the Site.

2.0 GEOLOGY

2.1 Regional Geology

The Jerry H. Baker Property is located within the Charlotte Belt of the Piedmont
Physiographic Province of south-central North Carolina. Near surface bedrock is
comprised of megacrystic to equigranular granitic rock.

2.2 Site Geology

Site geology was observed through the excavation of test pits in 11 trench lines. Test pits
ranged in depth from 10 to 21 feet bgs. Tan or red clayey sand or clayey silt fill exists at
the surface with a thickness range of 2 to 10 feet. A layer of debris fill is situated between
NC Department of Transportation – Preliminary Site Assessment
Jerry H Baker Property, Bethpage Dump
August 26, 2011

AMEC of North Carolina Inc
NCDOT State Project: U-3440, WBS Element: 39010.1.1
AMEC Project: 562113440
3
the fill and the underlying saprolite. The debris fill layer is typically comprised of varying
amounts of debris in a silty matrix. Debris items observed include wood (tree limbs, tree
trunks, and boards), metal (roofing, cable, fencing, pipe, wire, door), car and truck tires,
bricks, concrete, glass and plastic containers, and granitic rock. Wood was the most
common debris item observed. The debris fill layer had an average thickness of 6 feet and
varied in thickness from 1 foot at Test Pit 11, the southeastern most trench along Bethpage
Road, to 13 feet at Test Pit 8, near the intersection of Bethpage and Mooresville Roads. A
four foot thick layer of tires was observed in Test Pit 4. Approximately 30 tires were
excavated from Test Pit 4. Tires were not observed in the remaining test pits with an
exception for Test Pit 2, where a single automotive tire was observed.

The underlying saprolite was observed as light gray or tan sandy silt in the western portion
of the site and light gray or tan silty sand in the eastern portion of the site. Groundwater
was observed in the western test pits, which are nearest to Irish Buffalo Creek. Excavation
logs are presented in Appendix B.

3.0 FIELD ACTIVITIES

3.1 Site Reconnaissance

AMEC and NCDOT personnel completed site reconnaissance on June 6, 2011. During
reconnaissance, the area was visually examined for the presence of any UST or
areas/obstructions that could potentially affect the subsurface investigation. Strategy and
the number of trenching locations were discussed. AMEC personnel completed an
additional site reconnaissance on June 21, 2011 with EVO to further discuss strategy.
Trenching locations were marked on June 23, 2011 after clearing the vegetation.

3.2 Preliminary Activities

Prior to commencing field sampling activities at the site, several tasks were accomplished
in preparation for the subsurface investigation. The Health and Safety Plan (HSP) was
modified to include the site-specific health and safety information. On June 23, 2011 EVO
Environmental and Industrial Resources (EVO) of Winston Salem, North Carolina was
retained to bush hog the trench lines predetermined by AMEC and NCDOT personnel.
Due to the excessive vegetation a mini excavator was used to uncover and move debris in
order for the bush hog to operate safely. The mini excavator also cleared vegetation for the
NC Department of Transportation – Preliminary Site Assessment
Jerry H Baker Property, Bethpage Dump
August 26, 2011

AMEC of North Carolina Inc
NCDOT State Project: U-3440, WBS Element: 39010.1.1
AMEC Project: 562113440
4
utilities to be clearly located. On June 24, 2011 a private utility locating company, Priority
Underground Locating of Huntersville, North Carolina cleared the proposed trench lines
that had been marked in the field by AMEC personnel. North Carolina-1-Call was
contacted on June 29 to report the proposed trenching activities and subsequently notify all
affected utilities for the Property. EVO was also retained by AMEC to perform the
trenching. Pace Analytical of Huntersville, NC. was contacted for acquisition of sample
bottles. Eleven trenching locations were placed perpendicular to the road, across the
existing ROW, and extending to ten feet beyond the proposed construction easement. The
trenching locations were spaced roughly 50 foot apart along Mooresville and Bethpage
Road ROWs to maximize the likelihood of intercepting any potential soil contamination.

3.3 Soil Sampling

Trenching began on July 6, 2011 at the Bethpage Dump. Eleven trench lines were cleared
within the NCDOT design project area onsite. For Trench Line 1, three distinct test pits
(Test Pit 1a, Test Pit 1b, and Test Pit 1c) were dug in a staggered pattern. After conducting
the separate trench pit procedure for the first trench line AMEC personnel altered the
protocol for the remaining ten trench lines in order to improve safety adjacent to the
excavation and to improve the ability to log the subsurface to the maximum possible depth
of 20 feet bgs. For the next seven trench lines, one long test pit was excavated in two
sections (i.e. Test Pit Section a and Test Pit Section b). Starting at the stake closest to the
road, each excavation was first dug to the middle point of the trench line to a depth of
twenty feet bgs or until reaching native soil beneath debris. Test pit (a) was then logged
and sampled. Next, excavation continued from the middle point of the trench line toward
the property’s center, ending at the stake ten feet beyond the proposed construction
easement. Trench lines 9, 10, and 11 only had one test pit section excavation due to the
tree line which paralleled Bethpage Road and the limited amount of space to the proposed
construction easement. Excavation activities were monitored by David Treadway, who is a
North Carolina accredited Asbestos Inspector. Excavated materials were visually observed
for suspect asbestos containing materials (ACM). No suspect ACMs were observed;
therefore, no samples were collected for laboratory analysis.

From each trench line AMEC personnel targeted the upper 6 feet for the first laboratory
sample because that will be the potential shallow work zone for NCDOT employees during
the road widening project. Each of these samples was taken from the test pit closest to the
road and is identified with test pit number and an a. The second sample (sample b) was
deeper and targeted the soil matrix within the debris field, especially if there was evidence
NC Department of Transportation – Preliminary Site Assessment
Jerry H Baker Property, Bethpage Dump
August 26, 2011

AMEC of North Carolina Inc
NCDOT State Project: U-3440, WBS Element: 39010.1.1
AMEC Project: 562113440
5
of soil staining or PID readings. The sampling was accomplished by grabbing the soil with
nitrile gloved hands from the bucket of the excavator. Figure 3 presents the Site Map with
trench and sample locations. AMEC personnel use a photo ionized detector (PID) to screen
soils.

Soil samples were collected in accordance with EPA protocols in laboratory-supplied
containers. All samples were analyzed for the following: Total Petroleum Hydrocarbons
(TPH)-Gasoline Range Organics (GRO) and TPH-Diesel Range Organics (DRO) by EPA
method 8015B; Oil and Grease (O&G) by EPA method 9071A; Metals by EPA method
6010; Mercury by EPA method 7471; Volatile Organic Compounds (VOCs) by EPA method
8260; and, Semi Volatile Organic Compounds (SVOCs) by EPA method 8270. Once
placed in the containers, the samples were labeled with the sample number, time and date
of collection, name of the collector, and the requested analysis. The samples were packed
on ice, and then hand delivered to Pace Analytical a North Carolina Certified Laboratory
following proper chain-of-custody procedures.

4.0 SOIL SAMPLING RESULTS

AMEC conducted soil sampling at the Site on July 6 and July 7, 2011. The purpose of the
sampling was to determine the extent of the debris field within the proposed NCDOT
project area, evaluate if contaminated soils were present and, if so, estimate the quantity.

As excavation progressed AMEC personnel collected grab samples for PID screening and
these data are tabulated in Table 1. Low detections were found in trench lines 3 and 9 in
the upper 7 feet of soil (from 0.3 to 0.9 parts per million), while no detections were
measurable in the other trenches.

Twenty two samples were collected from the eleven trench lines and analyzed for a variety
of analytes. The analytical detections are presented in Table 2. These detections are also
presented in Figures 4 and 5 for shallow and deeper samples, respectively.

Of the 22 samples analyzed for GRO and DRO, none were reported with GRO detections.
DRO detections however, were measured in 18 of the 22 samples; 10 of which were
collected from the shallow soil from roughly 6 to 7 ft bgs. Most of the DRO concentrations
NC Department of Transportation – Preliminary Site Assessment
Jerry H Baker Property, Bethpage Dump
August 26, 2011

AMEC of North Carolina Inc
NCDOT State Project: U-3440, WBS Element: 39010.1.1
AMEC Project: 562113440
6
were low level with only four samples’ values exceeding the NCDENR non-UST TPH
Action level of 40 mg/kg. One of the four samples, Test Pit 3a, was a shallower sample
from 6 to 7 ft bgs with a DRO concentration of 64.3 mg/kg. The other three samples were
collected from deeper soil within the debris fill zones of Trenches 5, 6 and 8, with DRO
values ranging from 87.6 to 214 mg/kg.

The eight metals analyzed for in each sample include Arsenic, Barium, Cadmium, Total
Chromium, Lead, Selenium, Silver and Mercury. Most of these elements are also naturally
occurring in fill and saprolitic soil. Metals results for the 22 samples indicate natural, i.e.
background, levels as shown in Table 2. Although one arsenic concentration of 6.5 mg/kg
exceeds NCDENR Preliminary Soil Remediation Goals, its concentration fits within the
background range for the region and does not present as a contaminant of concern (COC).

Analytical detections for Oil and Grease were reported in 5 of the 22 samples. Only four
samples, Test Pit 4a (6-7’), Test Pit 5b (9-10’), Test Pit 7a (6-7’) and Test Pit-9a (15-16’)
indicated results above the Non-UST TPH Action Level of 250 mg/kg. These detections
ranged from 405 to 2570 mg/kg.

One soil sample Test Pit 2a (6-7) had SVOC detections for Fluoranthene and Pyrene. Both
analytes were below the Industrial Health Based Soil PRGs. VOCs indicated detections for
Acetone. Acetone is presumed a common laboratory contaminant.

Copies of the original laboratory report and chain-of-custody documentation are included as
Appendix D.

5.0 CONCLUSIONS

The following conclusions are based upon AMEC’s field evaluation and laboratory analyses
of samples collected from the Site on July 6 and 7, 2011.

• Eleven trench lines were conducted perpendicular to both Mooresville and
Bethpage Roads within the proposed expanded ROW and easement
corridor.
• The trenches ranged in depth from 10 to 21 feet bgs. A tan or red clayey
sand to clayey silt fill was noted from ground surface to an average depth of
7 feet bgs.

NC Department of Transportation – Preliminary Site Assessment
Jerry H Baker Property, Bethpage Dump
August 26, 2011

AMEC of North Carolina Inc
NCDOT State Project: U-3440, WBS Element: 39010.1.1
AMEC Project: 562113440
7
• Debris fill was identified at every trench location. Debris material observed
included wood, metal items, tires, bricks, concrete, glass and plastic
containers, and granitic rock. Wood was the most common debris item
observed.

• Debris fill thickness ranged from 1 to 13 feet, with an average of 6 feet.

• Twenty two samples were collected from the 11 trenches and analyzed for
TPH GRO and DRO, Metals, VOCs and SVOCs.

• Laboratory results indicated that the contaminants of concern (COC) include
TPH GRO and Oil & Grease, based on their reported concentrations above
the 40 and 250 mg/kg Action Standard for TPH at non-UST sites.

• The COC were identified only within the silty matrix of the debris fill, not in
the overlying suitable fill.

• The former approximate extent of the debris fill from the 2008 CESI field
activities is drawn in Figure 6. Their Test Pit 19 at the eastern side of the
site did not intercept debris hence their eastern boundary doesn’t include
that area. The approximate extent of the debris fill based on the July 2011
PSA activities and results, is shown in Figure 6 with a bold dark blue
dashed line. Due to the observation of debris in every trench the debris fill
boundary has now moved outward toward both Mooresville and Bethpage
Roads.

6.0 RECOMMENDATIONS

AMEC understands that at a future time the road improvements for Design Project U-3440
will impact this property along both Mooresville and Bethpage Roads. Buried debris fill has
been identified throughout the proposed expanded ROW and easement corridor. This
material is not suitable to underlay road construction or improvements, and therefore
should be removed and disposed of appropriately. All impacted soil exceeding an Action
Level was observed to be within the debris fill. Therefore the removal of debris fill will also
remove the TPH DRO and Oil & Grease impacted soil.

TABLES
Table 1
PID Field Screening
NCDOT - Bethpage Dump
Kannapolis, Cabarrus, North Carolina
P-1 7/6/2011 Test Pit 1a 3 0
P-2 7/6/2011 Test Pit 1a 6 0
P-3 7/6/2011 Test Pit 1a 8 0
P-4 7/6/2011 Test Pit 1a 10 0
P-5 7/6/2011 Test Pit 1a 12 0
P-6 7/6/2011 Test Pit 1b 2 0
P-7 7/6/2011 Test Pit 1b 4 0
P-8 7/6/2011 Test Pit 1b 6 0
P-9 7/6/2011 Test Pit 1b 8 0
P-10 7/6/2011 Test Pit 1b 10 0
P-11 7/6/2011 Test Pit 1b 12 0
P-12 7/6/2011 Test Pit 1c 4 0
P-13 7/6/2011 Test Pit 1c 6 0
P-14 7/6/2011 Test Pit 1c 8 0
P-15 7/6/2011 Test Pit 1c 10 0
P-16 7/6/2011 Test Pit 1c 12 0
P-17 7/6/2011 Test Pit 2a 2 0
P-18 7/6/2011 Test Pit 2a 4 0
P-19 7/6/2011 Test Pit 2a 6 0
P-20 7/6/2011 Test Pit 2a 8 0
P-21 7/6/2011 Test Pit 2a 10 0
P-22 7/6/2011 Test Pit 2a 12 0
P-23 7/6/2011 Test Pit 2b 2 0
P-24 7/6/2011 Test Pit 2b 4 0
P-25 7/6/2011 Test Pit 2b 6 0
P-26 7/6/2011 Test Pit 2b 8 0
P-27 7/6/2011 Test Pit 2b 10 0
P-28 7/6/2011 Test Pit 2b 12 0
P-29 7/6/2011 Test Pit 3a 4 0
P-30 7/6/2011 Test Pit 3a 6 0.4
P-31 7/6/2011 Test Pit 3a 7 0.3
P-32 7/6/2011 Test Pit 3a 8 0
P-33 7/6/2011 Test Pit 3a 10 0
P-34 7/6/2011 Test Pit 3a 12 0
P-35 7/6/2011 Test Pit 3b 4 0
P-36 7/6/2011 Test Pit 3b 6 0
P-37 7/6/2011 Test Pit 3b 8 0
P-38 7/6/2011 Test Pit 3b 10 0
P-39 7/6/2011 Test Pit 3b 12 0
Notes: PPM = Parts Per Million
SAMPLE ID Sample Date
Sample Depth
(feet bgs)
Field
Screening
(ppm)
Comments
Page 1 of 3
Table 1
PID Field Screening
NCDOT - Bethpage Dump
Kannapolis, Cabarrus, North Carolina
P-40 7/6/2011 Test Pit 4a 4 0
P-41 7/6/2011 Test Pit 4a 6 0
P-42 7/6/2011 Test Pit 4a 8 0
P-43 7/6/2011 Test Pit 4a 10 0
P-44 7/6/2011 Test Pit 4a 12 0
P-45 7/6/2011 Test Pit 4b 4 0
P-46 7/6/2011 Test Pit 4b 6 0
P-47 7/6/2011 Test Pit 4b 8 0
P-48 7/6/2011 Test Pit 4b 10 0
P-49 7/6/2011 Test Pit 4b 12 0
P-50 7/6/2011 Test Pit 4b 14 0
P-51 7/6/2011 Test Pit 5a 6 0
P-52 7/6/2011 Test Pit 5a 8 0
P-53 7/6/2011 Test Pit 5a 10 0
P-54 7/6/2011 Test Pit 5a 12 0
P-55 7/6/2011 Test Pit 5a 14 0
P-56 7/6/2011 Test Pit 5b 2 0
P-57 7/6/2011 Test Pit 5b 4 0
P-58 7/6/2011 Test Pit 5b 6 0
P-59 7/6/2011 Test Pit 5b 8 0
P-60 7/6/2011 Test Pit 5b 10 0
P-61 7/6/2011 Test Pit 5b 12 0
P-62 7/6/2011 Test Pit 6a 2 0
P-63 7/6/2011 Test Pit 6a 4 0
P-64 7/6/2011 Test Pit 6a 6 0
P-65 7/6/2011 Test Pit 6a 8 0
P-66 7/6/2011 Test Pit 6a 10 0
P-67 7/6/2011 Test Pit 6a 12 0
P-68 7/6/2011 Test Pit 6b 6 0
P-69 7/6/2011 Test Pit 6b 8 0
P-70 7/6/2011 Test Pit 6b 10 0
P-71 7/6/2011 Test Pit 6b 12 0
P-72 7/6/2011 Test Pit 7a 2 0
P-73 7/6/2011 Test Pit 7a 4 0
P-74 7/6/2011 Test Pit 7a 6 0
P-75 7/6/2011 Test Pit 7a 8 0
P-76 7/6/2011 Test Pit 7a 10 0
P-77 7/6/2011 Test Pit 7a 12 0
SAMPLE ID Sample Date Comments
Sample Depth
(feet bgs)
Field
Screening
(ppm)
Notes: PPM = Parts Per Million
Page 2 of 3
Table 1
PID Field Screening
NCDOT - Bethpage Dump
Kannapolis, Cabarrus, North Carolina
P-78 7/6/2011 Test Pit 7b 2 0
P-79 7/6/2011 Test Pit 7b 4 0
P-80 7/6/2011 Test Pit 7b 6 0
P-81 7/6/2011 Test Pit 7b 8 0
P-82 7/6/2011 Test Pit 7b 10 0
P-83 7/6/2011 Test Pit 7b 12 0
P-84 7/7/2011 Test Pit 8a 2 0
P-85 7/7/2011 Test Pit 8a 4 0
P-86 7/7/2011 Test Pit 8a 6 0
P-87 7/7/2011 Test Pit 8a 8 0
P-88 7/7/2011 Test Pit 8a 10 0
P-89 7/7/2011 Test Pit 8a 12 0
P-90 7/7/2011 Test Pit 8a 14 0
P-91 7/7/2011 Test Pit 8a 15 0
P-92 7/7/2011 Test Pit 8b 2 0
P-93 7/7/2011 Test Pit 8b 4 0
P-94 7/7/2011 Test Pit 8b 6 0
P-95 7/7/2011 Test Pit 8b 8 0
P-96 7/7/2011 Test Pit 8b 10 0
P-97 7/7/2011 Test Pit 8b 12 0
P-98 7/7/2011 Test Pit 8b 14 0
P-99 7/7/2011 Test Pit 8b 16 0
P-100 7/7/2011 Test Pit 8b 20 0
P-101 7/7/2011 Test Pit 9a 2 0
P-102 7/7/2011 Test Pit 9a 4 0.9
P-103 7/7/2011 Test Pit 9a 6 0
P-104 7/7/2011 Test Pit 9a 8 0
P-105 7/7/2011 Test Pit 9a 10 0
P-106 7/7/2011 Test Pit 9a 12 0
P-107 7/7/2011 Test Pit 9a 14 0
P-108 7/7/2011 Test Pit 9a 16 0
P-109 7/7/2011 Test Pit 9a 18 0
P-110 7/7/2011 Test Pit 10a 2 0
P-111 7/7/2011 Test Pit 10a 4 0
P-112 7/7/2011 Test Pit 10a 6 0
P-113 7/7/2011 Test Pit 10a 8 0
P-114 7/7/2011 Test Pit 10a 10 0
P-115 7/7/2011 Test Pit 10a 12 0
P-116 7/7/2011 Test Pit 10a 14 0
P-117 7/7/2011 Test Pit 11a 2 0
P-118 7/7/2011 Test Pit 11a 4 0
P-119 7/7/2011 Test Pit 11a 6 0
P-120 7/7/2011 Test Pit 11a 8 0
P-121 7/7/2011 Test Pit 11a 10 0
SAMPLE ID Sample Date Comments
Sample Depth
(feet bgs)
Field
Screening
(ppm)
Notes: PPM = Parts Per Million
Page 3 of 3
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FIGURES

APPENDIX A

PHOTO LOG
2801 Yorkmont RoadCharlotte, NC 28208
W.O. 562113440
PROCESSED TLH
DATE July 2011
PAGE
PHOTOGRAPHIC LOG
Preliminary Site Assessment
Bethpage Dump, Jerry Baker Property
Kannapolis, NC
Photo 1
Viewing northwest from
Bethpage Road site
entrance. The Photo shows
site prior to clearing
activities.
Photo 2
Viewing northwest from
Bethpage road. The photo
shows some of the utilities
that are present on this site.
1
2801 Yorkmont RoadCharlotte, NC 28208
W.O. 562113440
PROCESSED TLH
DATE July 2011
PAGE
PHOTOGRAPHIC LOG
Preliminary Site Assessment
Bethpage Dump, Jerry Baker Property
Kannapolis, NC
Photo 3
Viewing northeast from the
western portion of the site.
Photo is of EVO using the
Mini Excavator to move
debris before the bush hog
cuts this area.
Photo 4
Viewing north from central
portion of the site. Photo is
of exposed debris.
2
2801 Yorkmont RoadCharlotte, NC 28208
W.O. 562113440
PROCESSED TLH
DATE July 2011
PAGE
PHOTOGRAPHIC LOG
Preliminary Site Assessment
Bethpage Dump, Jerry Baker Property
Kannapolis, NC
Photo 5
Viewing west from eastern
portion of the site. Photo is
of EVO clearing site with
bush hog. This portion of the
site was used for staging
vehicles and earth moving
equipment.
Photo 6
Viewing east from central
portion of the site. Photo
shows site after bush hog
cut center area of site.
3
2801 Yorkmont RoadCharlotte, NC 28208
W.O. 562113440
PROCESSED TLH
DATE July 2011
PAGE
PHOTOGRAPHIC LOG
Preliminary Site Assessment
Bethpage Dump, Jerry Baker Property
Kannapolis, NC
Photo 7
Viewing north from central
portion of the site. Photo
shows area cleared for
digging test pits. Stake in
the foreground represents
the point ten feet beyond
proposed construction
easement.
Photo 8
Viewing south from northern
portion of the site. Photo
shows tires and other debris
in the test pit.
4
2801 Yorkmont RoadCharlotte, NC 28208
W.O. 562113440
PROCESSED TLH
DATE July 2011
PAGE
PHOTOGRAPHIC LOG
Preliminary Site Assessment
Bethpage Dump, Jerry Baker Property
Kannapolis, NC
Photo 9
Viewing north from central
portion of the site. Photo
shows tires being pulled from
the test pit.
Photo 10
Viewing north from eastern
portion of the site. Photo
shows construction debris.
5

APPENDIX B

BORING LOGS
Site Name: Jerry H Baker Property (Bethpage Dump)
Location: Kannapolis, NC
Excavation Method: Track Hoe
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0-5 Tan silty SAND; very fine grain; moist; no odor; fill
1-2' diameter granitic rocks were observed between the surface and
1' bgs
5-11 Debris Fill - observed concrete (4" thick by 1') and metal debris in light
gray clayey sandy silt matrix - Approximately 50% debris, 50% soil
Wet at 9'
11-13 Light gray sandy SILT; wet; no odor; Saprolite
AMEC Rep: David Treadway
Remarks:
Test Pit No.: TP-1a
Date: 07/06/11
Job No.: 562113440
Site Name: Jerry H Baker Property (Bethpage Dump)
Location: Kannapolis, NC
Excavation Method: Track Hoe
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0-5 Tan silty SAND; very fine grain; moist; no odor; fill
Several clay bricks were observed
5-10 Debris Fill - observed a tree stump, plastic flowers, concrete, and
wood in dark gray to black clayey sandy silt matrix - Approximately
50% debris, 50% soil
10-12 Light Gray Clayey SILT; wet; no odor; Saprolite
AMEC Rep: David Treadway
Remarks:
Test Pit No.: TP-1b
Date: 07/06/11
Job No.: 562113440
Site Name: Jerry H Baker Property (Bethpage Dump)
Location: Kannapolis, NC
Excavation Method: Track Hoe
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0-3 Tan silty SAND; very fine grain; moist; no odor; fill
3-10 Debris Fill - observed concrete (4" thick debris from building pad or
pavement), 3 tree stumps, plastic flowers, a 1' diameter tree
trunk, and tree limbs in dark gray clayey sandy silt matrix
Approximately 50% wood debris, 20% other debris, and 30% soil
Wet at 8'
10-13 Light gray clayey sandy SILT; moist; no odor; Saprolite
Test Pit No.: TP-1c
Date: 07/06/11
Job No.: 562113440
AMEC Rep: David Treadway
Remarks:
Site Name: Jerry H Baker Property (Bethpage Dump)
Location: Kannapolis, NC
Excavation Method: Track Hoe
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0-3 Red clayey sandy SILT; moist; no odor; fill
3-7 Tan silty SAND; very fine grain; moist; no odor; fill
7-12 Debris Fill - observed wood debris (1' diameter tree truck, power
pole, tree limbs), metal debris (including a metal door from a
transfer trailer), clay bricks, CMU blocks, plastic sheeting, and a tire
in light gray sandy silty matrix - Approximatley 50% wood debris,
20% other debris, and 30% soil
Wet at 8' - free water was observed in debris fill
12-13 Light gray clayey sandy SILT; wet; no odor; Saprolite; relict
structures visible
Test Pit No.: TP-2
Date: 07/06/11
Job No.: 562113440
AMEC Rep: David Treadway
Remarks:
Site Name: Jerry H Baker Property (Bethpage Dump)
Location: Kannapolis, NC
Excavation Method: Track Hoe
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0-2 Red sandy clayey SILT; moist; no odor; fill
2-4 Tan silty SAND; very fine grain; moist; no odor; fill
4-10 Debris Fill - observed metal wire fencing, metal roofing, wood debris,
and granitic rock debris (up to 4' wide by 8" thick)
Approximately 50% debris and 50% soil
Frequency of debris materials increases with depth
Wet at 8'
10-12 Tan sandy SILT; wet; no odor; Saprolite; relict structures visible
Test Pit No.: TP-3
Date: 07/06/11
Job No.: 562113440
AMEC Rep: David Treadway
Remarks:
Site Name: Jerry H Baker Property (Bethpage Dump)
Location: Kannapolis, NC
Excavation Method: Track Hoe
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0-5 Red clayey sandty SILT; moist; no odor
Tan below 4'
5-15** Debris Fill - observed a tree stump, 1" diameter metal cable,
concrete debris, wood debris (up to 1' diameter logs), and tires
Tires are stacked up to four feet thick at the bottom of the debris
fill layer. Approximately 30 tires were excavated from TP-4.
Above tire layer, debris fill is approximately 30% other debris and
70% gray sandy silt.
15-17** Tan sandy SILT; moist; no odor; Saprolite; relict structures visible
** On the north end of the test pit, the debris fill layer was
observed between 5 and 10'bgs
Test Pit No.: TP-4
Date: 07/06/11
Job No.: 562113440
AMEC Rep: David Treadway
Remarks:
observed between 5 and 10 bgs
Site Name: Jerry H Baker Property (Bethpage Dump)
Location: Kannapolis, NC
Excavation Method: Track Hoe
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0-3 Red clayey SILT; moist; no odor; fill
3-8 Tan silty SAND; very fine grain; moist; no odor; fill
Gray below 6'
8-15' Debris Fill - observed wood debris (tree stumps and limbs)
in gray silty sand matrix - Approximately 25% wood debris,
75% soil
Wet at 14'
15-16' Gray clayey sandy SILT; wet; no odor; Saprolite
Test Pit No.: TP-5
Date: 07/06/11
Job No.: 562113440
AMEC Rep: David Treadway
Remarks:
Site Name: Jerry H Baker Property (Bethpage Dump)
Location: Kannapolis, NC
Excavation Method: Track Hoe
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0-3 Red clayey SILT; moist; no odor; fill
3-5 Tan silty SAND; very fine grain; moist; no odor; fill
5-10 Debris Fill - observed clay tile pipe, wood debris, and rock debris
in gray sandy silt matrix - Approximately 10% debris, 90% soil
10-12 Gray clayey sandy SILT; moist; no odor; Saprolite
Test Pit No.: TP-6
Date: 07/06/11
Job No.: 562113440
AMEC Rep: David Treadway
Remarks:
Site Name: Jerry H Baker Property (Bethpage Dump)
Location: Kannapolis, NC
Excavation Method: Track Hoe
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0-6 Red clayey SILT; moist; no odor; fill
Observed 1' thick by 4' wide granitic rock layer at 5-6' on north
end of test pit
6-10 Light gray silty SAND; moist; no odor; Saprolite; relict structures
visible
Tree stump observed near center of test pit
Test Pit No.: TP-7
Date: 07/06/11
Job No.: 562113440
AMEC Rep: David Treadway
Remarks:
Site Name: Jerry H Baker Property (Bethpage Dump)
Location: Kannapolis, NC
Excavation Method: Track Hoe
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0-5 Tan and red sandy clayey SILT; moist; no odor; fill
5-7 Light gray silty SAND; moist; no odor; fill
Observed granitic rock debris (1'x0.75') at 2' BLS on west end of pit
7-20** Debris Fill - observed clay bricks, tree stump, wood boards, wood
tree limbs, metal debris (pipe, wire, rope, roofing), concrete debris
(3' x 0.5') in gray sandy silty matrix - Approximately 80% debris,
20% soil
20-21** Tan silty SAND; moist; no odor; Saprolite
**On the east end of the test pit, the debris fill layer was observed
between 7 and 13 feet BLS
Test Pit No.: TP-8
Date: 07/07/11
Job No.: 562113440
AMEC Rep: David Treadway
Remarks:
Site Name: Jerry H Baker Property (Bethpage Dump)
Location: Kannapolis, NC
Excavation Method: Track Hoe
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0-9 Tan clayey silty SAND; moist; no odor; fill
Red below 2'; light gray below 3'
9-17 Debris fill - observed wood boards, clay bricks, and metal roofing
Debris fill is approximately 5% sandy silt and 95% debris
17-18 Light gray silty SAND; wet; no odor; Saprolite; relict structures visible
Test Pit No.: TP-9
Date: 07/07/11
Job No.: 562113440
AMEC Rep: David Treadway
Remarks:
Site Name: Jerry H Baker Property (Bethpage Dump)
Location: Kannapolis, NC
Excavation Method: Track Hoe
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0-10 Tan clayey silty SAND; moist; no odor; fill
Red below 3', light gray below 4'
1' square by 5' long concrete debris near middle of pit at 3' BLS
10-14 Debris fill - observed wood debris and clay bricks in light gray
sandy silt matrix - Approximatley 80% wood debris, 10% other
debris, and 10% soil
14-15 Tan silty SAND; moist; no odor; Saprolite
Test Pit No.: TP-10
Date: 07/07/11
Job No.: 562113440
AMEC Rep: David Treadway
Remarks:
Site Name: Jerry H Baker Property (Bethpage Dump)
Location: Kannapolis, NC
Excavation Method: Track Hoe
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0-8 Tan clayey silty SAND; very fine grain; moist; no odor
Red below 3', light gray below 4'
8-9 Debris fill - observed aluminum and steel food cans, glass containers,
and clay bricks in black silty sand matrix
Approximately 90% debris, 10% soil
9-10 Tan silty SAND; moist; no odor; Saprolite
Test Pit No.: TP-11
Date: 07/07/11
Job No.: 562113440
AMEC Rep: David Treadway
Remarks:

APPENDIX C

LABORATORY ANALYTICAL RESULTS
July 19, 2011
LIMS USE: FR - CHEMICAL
LIMS OBJECT ID: 9297694
9297694
Project:
Pace Project No.:
RE:
Chemical Testing Engineer
NCDOT
Materials & Tests Unit
1801 Blueridge Road
Raleigh, NC 27607
JERRY BAKER PROPERTY 39010.1.1
Dear Chemical Engineer:
Enclosed are the analytical results for sample(s) received by the laboratory on July 07, 2011. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards, where applicable, unless otherwise narrated in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Erin Waters for
Kevin Herring
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078Louisiana/LELAP Certification #: 04034
New Jersey Certification #: NC012North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12Pennsylvania Certification #: 68-00784
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003Virginia Drinking Water Certification #: 00213
Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
Louisiana DHH Drinking Water # LA 100031West Virginia Certification #: 357
Virginia/VELAP Certification #: 460144
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804Connecticut Certification #: PH-0106Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030New Jersey Certification #: NC011
North Carolina Bioassay Certification #: 9North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40Pennsylvania Certification #: 68-03578South Carolina Bioassay Certification #: 99030002
South Carolina Certification #: 99030001Virginia Certification #: 00072
West Virginia Certification #: 356Virgina/VELAP Certification #: 460147
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
9297694001 TESTPIT 1A (6)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJMM
9297694002 TESTPIT 1B (8)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJMM
9297694003 TESTPIT 2A (6-7)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJMM
9297694004 TESTPIT 2B (8-9)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJMM
9297694005 TESTPIT 3A (6-7)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJMM
9297694006 TESTPIT 3B (8-9)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJMM
9297694007 TESTPIT 4A (6-7)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJMM
9297694008 TESTPIT 4B (9-10)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJMM
9297694009 TESTPIT 5A (6-7)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJMM
9297694010 TESTPIT 5B (9-10)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJMM
9297694011 TESTPIT 6A (6-7)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJMM
9297694012 TESTPIT 6B (9-10)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJMM
9297694013 TESTPIT 7A (6-7)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJMM
9297694014 TESTPIT 7B (9-10)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
ASTM D2974-87 1 PASI-CJMM
9297694015 TESTPIT 8A (6-7)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJMM
9297694016 TESTPIT 8B (13-14)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJEA
9297694017 TESTPIT 9A (4-6)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJEA
9297694018 TESTPIT 10A (6-7)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJEA
9297694019 TESTPIT 10A (9-10)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJEA
9297694020 TESTPIT 11A (6-7)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJEA
9297694021 TESTPIT 11A (8-9)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJEA
9297694022 TESTPIT 9A (15-16)EPA 8015 Modified 2 PASI-CCAH
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CKJM
EPA 6010 7 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJEA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
HITS ONLY
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
9297694001 TESTPIT 1A (6)
Diesel Components 20.2 mg/kg 07/12/11 01:366.0EPA 8015 Modified
Arsenic 2.1 mg/kg 07/13/11 15:010.54EPA 6010
Barium 91.8 mg/kg 07/13/11 15:010.54EPA 6010
Cadmium 0.40 mg/kg 07/13/11 15:010.11EPA 6010
Chromium 15.3 mg/kg 07/13/11 15:010.54EPA 6010
Lead 10.7 mg/kg 07/13/11 15:010.54EPA 6010
Selenium 3.0 mg/kg 07/13/11 15:011.1EPA 6010
Mercury 0.031 mg/kg 07/11/11 17:170.0049EPA 7471
Acetone 218 ug/kg 07/12/11 16:38 C994.4EPA 8260
Percent Moisture 17.0 %07/08/11 08:530.10ASTM D2974-87
9297694002 TESTPIT 1B (8)
Diesel Components 17.2 mg/kg 07/12/11 01:366.8EPA 8015 Modified
Arsenic 3.2 mg/kg 07/13/11 15:040.65EPA 6010
Barium 77.4 mg/kg 07/13/11 15:040.65EPA 6010
Chromium 12.8 mg/kg 07/13/11 15:040.65EPA 6010
Lead 20.4 mg/kg 07/13/11 15:040.65EPA 6010
Selenium 2.2 mg/kg 07/13/11 15:041.3EPA 6010
Mercury 0.012 mg/kg 07/11/11 17:220.0068EPA 7471
Acetone 168 ug/kg 07/12/11 16:58 C9103EPA 8260
Percent Moisture 26.4 %07/08/11 08:530.10ASTM D2974-87
9297694003 TESTPIT 2A (6-7)
Diesel Components 20.2 mg/kg 07/12/11 02:045.9EPA 8015 Modified
Arsenic 2.6 mg/kg 07/13/11 15:160.56EPA 6010
Barium 45.7 mg/kg 07/13/11 15:160.56EPA 6010
Chromium 5.7 mg/kg 07/13/11 15:160.56EPA 6010
Lead 18.2 mg/kg 07/13/11 15:160.56EPA 6010
Mercury 0.016 mg/kg 07/11/11 17:380.0057EPA 7471
Fluoranthene 464 ug/kg 07/14/11 17:16390EPA 8270
Pyrene 391 ug/kg 07/14/11 17:16390EPA 8270
Acetone 148 ug/kg 07/12/11 17:18 C989.1EPA 8260
Percent Moisture 15.6 %07/08/11 08:530.10ASTM D2974-87
9297694004 TESTPIT 2B (8-9)
Diesel Components 9.2 mg/kg 07/12/11 02:046.5EPA 8015 Modified
Arsenic 2.8 mg/kg 07/13/11 15:200.55EPA 6010
Barium 90.5 mg/kg 07/13/11 15:200.55EPA 6010
Chromium 4.8 mg/kg 07/13/11 15:200.55EPA 6010
Lead 26.0 mg/kg 07/13/11 15:200.55EPA 6010
Selenium 1.5 mg/kg 07/13/11 15:201.1EPA 6010
Mercury 0.021 mg/kg 07/11/11 17:430.0046EPA 7471
Acetone 104 ug/kg 07/12/11 17:39 C9101EPA 8260
Percent Moisture 23.0 %07/08/11 08:530.10ASTM D2974-87
9297694005 TESTPIT 3A (6-7)
Diesel Components 64.2 mg/kg 07/12/11 02:336.4EPA 8015 Modified
Arsenic 6.5 mg/kg 07/13/11 15:230.59EPA 6010
Barium 96.0 mg/kg 07/13/11 15:230.59EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
HITS ONLY
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
9297694005 TESTPIT 3A (6-7)
Cadmium 0.72 mg/kg 07/13/11 15:230.12EPA 6010
Chromium 12.4 mg/kg 07/13/11 15:230.59EPA 6010
Lead 85.8 mg/kg 07/13/11 15:230.59EPA 6010
Selenium 1.9 mg/kg 07/13/11 15:231.2EPA 6010
Mercury 0.028 mg/kg 07/11/11 17:490.0060EPA 7471
Percent Moisture 21.4 %07/08/11 08:530.10ASTM D2974-87
9297694006 TESTPIT 3B (8-9)
Diesel Components 18.7 mg/kg 07/12/11 02:336.2EPA 8015 Modified
Arsenic 2.8 mg/kg 07/13/11 15:310.48EPA 6010
Barium 71.1 mg/kg 07/13/11 15:310.48EPA 6010
Chromium 6.0 mg/kg 07/13/11 15:310.48EPA 6010
Lead 14.5 mg/kg 07/13/11 15:310.48EPA 6010
Selenium 1.2 mg/kg 07/13/11 15:310.96EPA 6010
Mercury 0.011 mg/kg 07/11/11 17:510.0040EPA 7471
Acetone 217 ug/kg 07/12/11 18:19 C992.6EPA 8260
Percent Moisture 18.8 %07/08/11 08:530.10ASTM D2974-87
9297694007 TESTPIT 4A (6-7)
Diesel Components 21.4 mg/kg 07/12/11 03:015.9EPA 8015 Modified
Oil and Grease 868 mg/kg 07/11/11 12:0582.19071B
Arsenic 3.2 mg/kg 07/13/11 15:340.51EPA 6010
Barium 61.1 mg/kg 07/13/11 15:340.51EPA 6010
Chromium 7.7 mg/kg 07/13/11 15:340.51EPA 6010
Lead 30.6 mg/kg 07/13/11 15:340.51EPA 6010
Selenium 1.4 mg/kg 07/13/11 15:341.0EPA 6010
Mercury 0.027 mg/kg 07/11/11 17:540.0050EPA 7471
Acetone 184 ug/kg 07/12/11 18:39 C989.9EPA 8260
Percent Moisture 14.7 %07/08/11 08:530.10ASTM D2974-87
9297694008 TESTPIT 4B (9-10)
Diesel Components 32.7 mg/kg 07/12/11 03:01 P331.0EPA 8015 Modified
Arsenic 1.8 mg/kg 07/13/11 15:370.50EPA 6010
Barium 61.7 mg/kg 07/13/11 15:370.50EPA 6010
Cadmium 0.26 mg/kg 07/13/11 15:370.10EPA 6010
Chromium 24.3 mg/kg 07/13/11 15:370.50EPA 6010
Lead 14.1 mg/kg 07/13/11 15:370.50EPA 6010
Selenium 2.5 mg/kg 07/13/11 15:371.0EPA 6010
Mercury 0.022 mg/kg 07/11/11 17:560.0053EPA 7471
Acetone 158 ug/kg 07/12/11 18:59 C996.2EPA 8260
Percent Moisture 19.3 %07/08/11 08:540.10ASTM D2974-87
9297694009 TESTPIT 5A (6-7)
Arsenic 2.8 mg/kg 07/13/11 15:400.48EPA 6010
Barium 107 mg/kg 07/13/11 15:400.48EPA 6010
Chromium 4.1 mg/kg 07/13/11 15:400.48EPA 6010
Lead 16.6 mg/kg 07/13/11 15:400.48EPA 6010
Selenium 1.8 mg/kg 07/13/11 15:400.96EPA 6010
Mercury 0.015 mg/kg 07/11/11 17:590.0046EPA 7471
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
HITS ONLY
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
9297694009 TESTPIT 5A (6-7)
Acetone 126 ug/kg 07/12/11 19:19 C996.7EPA 8260
Percent Moisture 17.7 %07/08/11 08:540.10ASTM D2974-87
9297694010 TESTPIT 5B (9-10)
Diesel Components 87.6 mg/kg 07/12/11 05:49 P333.3EPA 8015 Modified
Oil and Grease 2570 mg/kg 07/11/11 12:0593.39071B
Arsenic 3.6 mg/kg 07/13/11 15:440.63EPA 6010
Barium 120 mg/kg 07/13/11 15:440.63EPA 6010
Cadmium 0.47 mg/kg 07/13/11 15:440.13EPA 6010
Chromium 7.6 mg/kg 07/13/11 15:440.63EPA 6010
Lead 267 mg/kg 07/13/11 15:440.63EPA 6010
Mercury 0.038 mg/kg 07/11/11 18:020.0049EPA 7471
Acetone 117 ug/kg 07/12/11 19:39 C9110EPA 8260
Percent Moisture 25.0 %07/08/11 08:540.10ASTM D2974-87
9297694011 TESTPIT 6A (6-7)
Diesel Components 13.4 mg/kg 07/12/11 05:495.7EPA 8015 Modified
Arsenic 2.5 mg/kg 07/14/11 13:270.50EPA 6010
Barium 112 mg/kg 07/13/11 19:350.50EPA 6010
Chromium 3.3 mg/kg 07/13/11 19:350.50EPA 6010
Lead 23.3 mg/kg 07/13/11 19:350.50EPA 6010
Mercury 0.016 mg/kg 07/11/11 18:100.0045EPA 7471
Percent Moisture 12.7 %07/08/11 08:540.10ASTM D2974-87
9297694012 TESTPIT 6B (9-10)
Arsenic 2.2 mg/kg 07/14/11 14:310.49EPA 6010
Barium 50.0 mg/kg 07/13/11 19:520.49EPA 6010
Chromium 3.8 mg/kg 07/13/11 19:520.49EPA 6010
Lead 19.3 mg/kg 07/13/11 19:520.49EPA 6010
Mercury 0.027 mg/kg 07/11/11 18:120.0052EPA 7471
Acetone 135 ug/kg 07/12/11 20:19 C988.7EPA 8260
Percent Moisture 15.5 %07/08/11 08:540.10ASTM D2974-87
9297694013 TESTPIT 7A (6-7)
Diesel Components 9.4 mg/kg 07/12/11 06:465.4EPA 8015 Modified
Oil and Grease 405 mg/kg 07/11/11 12:0575.39071B
Arsenic 2.1 mg/kg 07/14/11 14:340.43EPA 6010
Barium 64.7 mg/kg 07/13/11 20:000.43EPA 6010
Chromium 2.6 mg/kg 07/13/11 20:000.43EPA 6010
Lead 12.0 mg/kg 07/13/11 20:000.43EPA 6010
Mercury 0.015 mg/kg 07/11/11 18:150.0045EPA 7471
Percent Moisture 7.1 %07/08/11 08:550.10ASTM D2974-87
9297694014 TESTPIT 7B (9-10)
Arsenic 3.0 mg/kg 07/14/11 14:390.56EPA 6010
Barium 82.3 mg/kg 07/13/11 20:030.56EPA 6010
Chromium 3.4 mg/kg 07/13/11 20:030.56EPA 6010
Lead 17.3 mg/kg 07/13/11 20:030.56EPA 6010
Selenium 1.2 mg/kg 07/13/11 20:031.1EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 10 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
HITS ONLY
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
9297694014 TESTPIT 7B (9-10)
Mercury 0.012 mg/kg 07/11/11 18:180.0051EPA 7471
Percent Moisture 15.7 %07/08/11 08:550.10ASTM D2974-87
9297694015 TESTPIT 8A (6-7)
Diesel Components 11.8 mg/kg 07/12/11 07:426.0EPA 8015 Modified
Arsenic 2.8 mg/kg 07/14/11 14:420.54EPA 6010
Barium 124 mg/kg 07/13/11 20:070.54EPA 6010
Chromium 3.7 mg/kg 07/13/11 20:070.54EPA 6010
Lead 17.6 mg/kg 07/13/11 20:070.54EPA 6010
Selenium 1.1 mg/kg 07/13/11 20:071.1EPA 6010
Mercury 0.021 mg/kg 07/11/11 18:200.0050EPA 7471
Percent Moisture 16.7 %07/08/11 08:550.10ASTM D2974-87
9297694016 TESTPIT 8B (13-14)
Diesel Components 105 mg/kg 07/12/11 08:106.1EPA 8015 Modified
Oil and Grease 174 mg/kg 07/11/11 12:0685.29071B
Arsenic 3.3 mg/kg 07/14/11 14:460.51EPA 6010
Barium 54.1 mg/kg 07/13/11 20:110.51EPA 6010
Chromium 4.8 mg/kg 07/13/11 20:110.51EPA 6010
Lead 94.6 mg/kg 07/13/11 20:110.51EPA 6010
Mercury 0.045 mg/kg 07/11/11 18:230.0055EPA 7471
Percent Moisture 17.8 %07/08/11 08:590.10ASTM D2974-87
9297694017 TESTPIT 9A (4-6)
Diesel Components 7.9 mg/kg 07/12/11 08:105.8EPA 8015 Modified
Arsenic 2.9 mg/kg 07/14/11 14:500.50EPA 6010
Barium 100 mg/kg 07/13/11 20:150.50EPA 6010
Chromium 3.3 mg/kg 07/13/11 20:150.50EPA 6010
Lead 15.1 mg/kg 07/13/11 20:150.50EPA 6010
Mercury 0.015 mg/kg 07/11/11 18:260.0050EPA 7471
Percent Moisture 13.9 %07/08/11 08:590.10ASTM D2974-87
9297694018 TESTPIT 10A (6-7)
Diesel Components 21.5 mg/kg 07/12/11 08:385.8EPA 8015 Modified
Arsenic 1.3 mg/kg 07/14/11 14:540.42EPA 6010
Barium 29.1 mg/kg 07/13/11 20:200.42EPA 6010
Chromium 1.5 mg/kg 07/13/11 20:200.42EPA 6010
Lead 15.2 mg/kg 07/13/11 20:200.42EPA 6010
Mercury 0.019 mg/kg 07/15/11 15:030.0049EPA 7471
Percent Moisture 13.1 %07/08/11 09:000.10ASTM D2974-87
9297694019 TESTPIT 10A (9-10)
Diesel Components 10 mg/kg 07/12/11 08:386.1EPA 8015 Modified
Arsenic 2.5 mg/kg 07/14/11 14:580.59EPA 6010
Barium 88.0 mg/kg 07/13/11 20:230.59EPA 6010
Chromium 3.5 mg/kg 07/13/11 20:230.59EPA 6010
Lead 13.8 mg/kg 07/13/11 20:230.59EPA 6010
Mercury 0.024 mg/kg 07/15/11 15:060.0048EPA 7471
Percent Moisture 17.5 %07/08/11 09:000.10ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 11 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
HITS ONLY
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
9297694020 TESTPIT 11A (6-7)
Diesel Components 5.9 mg/kg 07/12/11 09:075.7EPA 8015 Modified
Arsenic 1.9 mg/kg 07/13/11 20:370.54EPA 6010
Barium 39.2 mg/kg 07/13/11 20:370.54EPA 6010
Chromium 2.5 mg/kg 07/13/11 20:370.54EPA 6010
Lead 16.7 mg/kg 07/13/11 20:370.54EPA 6010
Mercury 0.021 mg/kg 07/15/11 15:080.0050EPA 7471
Percent Moisture 12.2 %07/08/11 09:000.10ASTM D2974-87
9297694021 TESTPIT 11A (8-9)
Arsenic 3.1 mg/kg 07/13/11 20:400.54EPA 6010
Barium 110 mg/kg 07/13/11 20:400.54EPA 6010
Chromium 6.8 mg/kg 07/13/11 20:400.54EPA 6010
Lead 11.6 mg/kg 07/13/11 20:400.54EPA 6010
Selenium 1.6 mg/kg 07/13/11 20:401.1EPA 6010
Mercury 0.030 mg/kg 07/15/11 15:110.0053EPA 7471
Percent Moisture 16.2 %07/08/11 09:010.10ASTM D2974-87
9297694022 TESTPIT 9A (15-16)
Diesel Components 214 mg/kg 07/12/11 09:35 P330.7EPA 8015 Modified
Oil and Grease 1110 mg/kg 07/14/11 11:2086.09071B
Arsenic 2.9 mg/kg 07/13/11 20:450.50EPA 6010
Barium 85.7 mg/kg 07/13/11 20:450.50EPA 6010
Chromium 14.8 mg/kg 07/13/11 20:450.50EPA 6010
Lead 28.4 mg/kg 07/13/11 20:450.50EPA 6010
Selenium 1.4 mg/kg 07/13/11 20:450.99EPA 6010
Mercury 0.063 mg/kg 07/15/11 15:190.0048EPA 7471
Percent Moisture 18.6 %07/08/11 09:010.10ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Method:
Client:NCDOT
EPA 8015 Modified
Date:July 19, 2011
Description:8015 GCS THC-Diesel
General Information:
22 samples were analyzed for EPA 8015 Modified. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3546 with any exceptions noted below.
QC Batch: OEXT/14158
P3: Sample extract could not be concentrated to the routine final volume, resulting in elevated reporting limits.
• TESTPIT 4B (9-10) (Lab ID: 9297694008)
QC Batch: OEXT/14160
P3: Sample extract could not be concentrated to the routine final volume, resulting in elevated reporting limits.
• TESTPIT 5B (9-10) (Lab ID: 9297694010)
• TESTPIT 9A (15-16) (Lab ID: 9297694022)
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: OEXT/14158
S4: Surrogate recovery not evaluated against control limits due to sample dilution.
• TESTPIT 4B (9-10) (Lab ID: 9297694008)
• n-Pentacosane (S)
QC Batch: OEXT/14160
S4: Surrogate recovery not evaluated against control limits due to sample dilution.
• TESTPIT 5B (9-10) (Lab ID: 9297694010)
• n-Pentacosane (S)
• TESTPIT 9A (15-16) (Lab ID: 9297694022)
• n-Pentacosane (S)
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 13 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Method:
Client:NCDOT
EPA 8015 Modified
Date:July 19, 2011
Description:8015 GCS THC-Diesel
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 14 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Method:
Client:NCDOT
9071B
Date:July 19, 2011
Description:9071 Oil and Grease
General Information:
22 samples were analyzed for 9071B. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with 9071B with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: GCSV/10103
A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 9297694005
M3: Matrix spike recovery was outside laboratory control limits due to matrix interferences.
• MS (Lab ID: 631934)
• Oil and Grease
• MSD (Lab ID: 631935)
• Oil and Grease
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 15 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Method:
Client:NCDOT
EPA 8015 Modified
Date:July 19, 2011
Description:Gasoline Range Organics
General Information:
22 samples were analyzed for EPA 8015 Modified. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 5035A/5030B with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 16 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Method:
Client:NCDOT
EPA 6010
Date:July 19, 2011
Description:6010 MET ICP
General Information:
22 samples were analyzed for EPA 6010. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3050 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MPRP/8714
A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 9297122001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 632217)
• Barium
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 17 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Method:
Client:NCDOT
EPA 7471
Date:July 19, 2011
Description:7471 Mercury
General Information:
22 samples were analyzed for EPA 7471. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 7471 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MERP/3599
A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 9297694001,9297694002
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 631151)
• Mercury
• MS (Lab ID: 631152)
• Mercury
QC Batch: MERP/3614
A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 9297452002,9297794001
M0: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
• MS (Lab ID: 633664)
• Mercury
• MS (Lab ID: 633666)
• Mercury
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 18 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Method:
Client:NCDOT
EPA 7471
Date:July 19, 2011
Description:7471 Mercury
QC Batch: MERP/3599
D6: The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 631154)
• Mercury
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 19 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Method:
Client:NCDOT
EPA 8270
Date:July 19, 2011
Description:8270 MSSV Microwave
General Information:
22 samples were analyzed for EPA 8270. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3546 with any exceptions noted below.
QC Batch: OEXT/14156
P3: Sample extract could not be concentrated to the routine final volume, resulting in elevated reporting limits.
• TESTPIT 2B (8-9) (Lab ID: 9297694004)
• TESTPIT 4A (6-7) (Lab ID: 9297694007)
• TESTPIT 5B (9-10) (Lab ID: 9297694010)
QC Batch: OEXT/14176
P3: Sample extract could not be concentrated to the routine final volume, resulting in elevated reporting limits.
• TESTPIT 9A (15-16) (Lab ID: 9297694022)
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: OEXT/14156
S4: Surrogate recovery not evaluated against control limits due to sample dilution.
• TESTPIT 4A (6-7) (Lab ID: 9297694007)
• Nitrobenzene-d5 (S)
• TESTPIT 5B (9-10) (Lab ID: 9297694010)
• Nitrobenzene-d5 (S)
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 20 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Method:
Client:NCDOT
EPA 8270
Date:July 19, 2011
Description:8270 MSSV Microwave
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: OEXT/14156
D3: Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.
• TESTPIT 4A (6-7) (Lab ID: 9297694007)
• Phenol
• TESTPIT 5B (9-10) (Lab ID: 9297694010)
• Phenol
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 21 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Method:
Client:NCDOT
EPA 8260
Date:July 19, 2011
Description:8260/5035A Volatile Organics
General Information:
22 samples were analyzed for EPA 8260. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: MSV/15970
1g: The internal standard response is below criteria. No hits associated with this internal standard. Results unaffected by high bias.
• TESTPIT 5B (9-10) (Lab ID: 9297694010)
• Dichlorodifluoromethane
C9: Common Laboratory Contaminant.
• TESTPIT 1A (6) (Lab ID: 9297694001)
• Acetone
• TESTPIT 1B (8) (Lab ID: 9297694002)
• Acetone
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 22 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Method:
Client:NCDOT
EPA 8260
Date:July 19, 2011
Description:8260/5035A Volatile Organics
Analyte Comments:
QC Batch: MSV/15970
C9: Common Laboratory Contaminant.
• TESTPIT 2A (6-7) (Lab ID: 9297694003)
• Acetone
• TESTPIT 2B (8-9) (Lab ID: 9297694004)
• Acetone
• TESTPIT 3B (8-9) (Lab ID: 9297694006)
• Acetone
• TESTPIT 4A (6-7) (Lab ID: 9297694007)
• Acetone
• TESTPIT 4B (9-10) (Lab ID: 9297694008)
• Acetone
• TESTPIT 5A (6-7) (Lab ID: 9297694009)
• Acetone
• TESTPIT 5B (9-10) (Lab ID: 9297694010)
• Acetone
• TESTPIT 6B (9-10) (Lab ID: 9297694012)
• Acetone
QC Batch: MSV/15994
1g: The internal standard response is below criteria. No hits associated with this internal standard. Results unaffected by high bias.
• TESTPIT 8B (13-14) (Lab ID: 9297694016)
• Dichlorodifluoromethane
C9: Common Laboratory Contaminant.
• DUP (Lab ID: 633652)
• Methylene Chloride
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 23 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 1A (6)Lab ID:9297694001 Collected:07/06/11 10:25 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 20.2 mg/kg 1 07/12/11 01:36 68334-30-507/07/11 15:356.0
n-Pentacosane (S)61 %1 07/12/11 01:36 629-99-207/07/11 15:3541-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease ND mg/kg 1 07/11/11 12:0507/11/11 11:1584.3
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/12/11 14:30 8006-61-907/12/11 10:346.7
4-Bromofluorobenzene (S)138 %1 07/12/11 14:30 460-00-407/12/11 10:3470-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 2.1 mg/kg 1 07/13/11 15:01 7440-38-207/12/11 11:400.54
Barium 91.8 mg/kg 1 07/13/11 15:01 7440-39-307/12/11 11:400.54
Cadmium 0.40 mg/kg 1 07/13/11 15:01 7440-43-907/12/11 11:400.11
Chromium 15.3 mg/kg 1 07/13/11 15:01 7440-47-307/12/11 11:400.54
Lead 10.7 mg/kg 1 07/13/11 15:01 7439-92-107/12/11 11:400.54
Selenium 3.0 mg/kg 1 07/13/11 15:01 7782-49-207/12/11 11:401.1
Silver ND mg/kg 1 07/13/11 15:01 7440-22-407/12/11 11:400.54
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.031 mg/kg 1 07/11/11 17:17 7439-97-607/08/11 15:100.0049
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/14/11 16:19 83-32-907/07/11 13:30399
Acenaphthylene ND ug/kg 1 07/14/11 16:19 208-96-807/07/11 13:30399
Aniline ND ug/kg 1 07/14/11 16:19 62-53-307/07/11 13:30399
Anthracene ND ug/kg 1 07/14/11 16:19 120-12-707/07/11 13:30399
Benzo(a)anthracene ND ug/kg 1 07/14/11 16:19 56-55-307/07/11 13:30399
Benzo(a)pyrene ND ug/kg 1 07/14/11 16:19 50-32-807/07/11 13:30399
Benzo(b)fluoranthene ND ug/kg 1 07/14/11 16:19 205-99-207/07/11 13:30399
Benzo(g,h,i)perylene ND ug/kg 1 07/14/11 16:19 191-24-207/07/11 13:30399
Benzo(k)fluoranthene ND ug/kg 1 07/14/11 16:19 207-08-907/07/11 13:30399
Benzoic Acid ND ug/kg 1 07/14/11 16:19 65-85-007/07/11 13:301990
Benzyl alcohol ND ug/kg 1 07/14/11 16:19 100-51-607/07/11 13:30798
4-Bromophenylphenyl ether ND ug/kg 1 07/14/11 16:19 101-55-307/07/11 13:30399
Butylbenzylphthalate ND ug/kg 1 07/14/11 16:19 85-68-707/07/11 13:30399
4-Chloro-3-methylphenol ND ug/kg 1 07/14/11 16:19 59-50-707/07/11 13:30798
4-Chloroaniline ND ug/kg 1 07/14/11 16:19 106-47-807/07/11 13:301990
bis(2-Chloroethoxy)methane ND ug/kg 1 07/14/11 16:19 111-91-107/07/11 13:30399
bis(2-Chloroethyl) ether ND ug/kg 1 07/14/11 16:19 111-44-407/07/11 13:30399
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/14/11 16:19 108-60-107/07/11 13:30399
2-Chloronaphthalene ND ug/kg 1 07/14/11 16:19 91-58-707/07/11 13:30399
2-Chlorophenol ND ug/kg 1 07/14/11 16:19 95-57-807/07/11 13:30399
4-Chlorophenylphenyl ether ND ug/kg 1 07/14/11 16:19 7005-72-307/07/11 13:30399
Chrysene ND ug/kg 1 07/14/11 16:19 218-01-907/07/11 13:30399
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 24 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 1A (6)Lab ID:9297694001 Collected:07/06/11 10:25 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/14/11 16:19 53-70-307/07/11 13:30399
Dibenzofuran ND ug/kg 1 07/14/11 16:19 132-64-907/07/11 13:30399
1,2-Dichlorobenzene ND ug/kg 1 07/14/11 16:19 95-50-107/07/11 13:30399
1,3-Dichlorobenzene ND ug/kg 1 07/14/11 16:19 541-73-107/07/11 13:30399
1,4-Dichlorobenzene ND ug/kg 1 07/14/11 16:19 106-46-707/07/11 13:30399
3,3'-Dichlorobenzidine ND ug/kg 1 07/14/11 16:19 91-94-107/07/11 13:301990
2,4-Dichlorophenol ND ug/kg 1 07/14/11 16:19 120-83-207/07/11 13:30399
Diethylphthalate ND ug/kg 1 07/14/11 16:19 84-66-207/07/11 13:30399
2,4-Dimethylphenol ND ug/kg 1 07/14/11 16:19 105-67-907/07/11 13:30399
Dimethylphthalate ND ug/kg 1 07/14/11 16:19 131-11-307/07/11 13:30399
Di-n-butylphthalate ND ug/kg 1 07/14/11 16:19 84-74-207/07/11 13:30399
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/14/11 16:19 534-52-107/07/11 13:30798
2,4-Dinitrophenol ND ug/kg 1 07/14/11 16:19 51-28-507/07/11 13:301990
2,4-Dinitrotoluene ND ug/kg 1 07/14/11 16:19 121-14-207/07/11 13:30399
2,6-Dinitrotoluene ND ug/kg 1 07/14/11 16:19 606-20-207/07/11 13:30399
Di-n-octylphthalate ND ug/kg 1 07/14/11 16:19 117-84-007/07/11 13:30399
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/14/11 16:19 117-81-707/07/11 13:30399
Fluoranthene ND ug/kg 1 07/14/11 16:19 206-44-007/07/11 13:30399
Fluorene ND ug/kg 1 07/14/11 16:19 86-73-707/07/11 13:30399
Hexachloro-1,3-butadiene ND ug/kg 1 07/14/11 16:19 87-68-307/07/11 13:30399
Hexachlorobenzene ND ug/kg 1 07/14/11 16:19 118-74-107/07/11 13:30399
Hexachlorocyclopentadiene ND ug/kg 1 07/14/11 16:19 77-47-407/07/11 13:30399
Hexachloroethane ND ug/kg 1 07/14/11 16:19 67-72-107/07/11 13:30399
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/14/11 16:19 193-39-507/07/11 13:30399
Isophorone ND ug/kg 1 07/14/11 16:19 78-59-107/07/11 13:30399
1-Methylnaphthalene ND ug/kg 1 07/14/11 16:19 90-12-007/07/11 13:30399
2-Methylnaphthalene ND ug/kg 1 07/14/11 16:19 91-57-607/07/11 13:30399
2-Methylphenol(o-Cresol)ND ug/kg 1 07/14/11 16:19 95-48-707/07/11 13:30399
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/14/11 16:1907/07/11 13:30399
Naphthalene ND ug/kg 1 07/14/11 16:19 91-20-307/07/11 13:30399
2-Nitroaniline ND ug/kg 1 07/14/11 16:19 88-74-407/07/11 13:301990
3-Nitroaniline ND ug/kg 1 07/14/11 16:19 99-09-207/07/11 13:301990
4-Nitroaniline ND ug/kg 1 07/14/11 16:19 100-01-607/07/11 13:30798
Nitrobenzene ND ug/kg 1 07/14/11 16:19 98-95-307/07/11 13:30399
2-Nitrophenol ND ug/kg 1 07/14/11 16:19 88-75-507/07/11 13:30399
4-Nitrophenol ND ug/kg 1 07/14/11 16:19 100-02-707/07/11 13:301990
N-Nitrosodimethylamine ND ug/kg 1 07/14/11 16:19 62-75-907/07/11 13:30399
N-Nitroso-di-n-propylamine ND ug/kg 1 07/14/11 16:19 621-64-707/07/11 13:30399
N-Nitrosodiphenylamine ND ug/kg 1 07/14/11 16:19 86-30-607/07/11 13:30399
Pentachlorophenol ND ug/kg 1 07/14/11 16:19 87-86-507/07/11 13:301990
Phenanthrene ND ug/kg 1 07/14/11 16:19 85-01-807/07/11 13:30399
Phenol ND ug/kg 1 07/14/11 16:19 108-95-207/07/11 13:30399
Pyrene ND ug/kg 1 07/14/11 16:19 129-00-007/07/11 13:30399
1,2,4-Trichlorobenzene ND ug/kg 1 07/14/11 16:19 120-82-107/07/11 13:30399
2,4,5-Trichlorophenol ND ug/kg 1 07/14/11 16:19 95-95-407/07/11 13:30399
2,4,6-Trichlorophenol ND ug/kg 1 07/14/11 16:19 88-06-207/07/11 13:30399
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 25 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 1A (6)Lab ID:9297694001 Collected:07/06/11 10:25 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)74 %1 07/14/11 16:19 4165-60-007/07/11 13:3023-110
2-Fluorobiphenyl (S)72 %1 07/14/11 16:19 321-60-807/07/11 13:3030-110
Terphenyl-d14 (S)71 %1 07/14/11 16:19 1718-51-007/07/11 13:3028-110
Phenol-d6 (S)48 %1 07/14/11 16:19 13127-88-307/07/11 13:3022-110
2-Fluorophenol (S)44 %1 07/14/11 16:19 367-12-407/07/11 13:3013-110
2,4,6-Tribromophenol (S)69 %1 07/14/11 16:19 118-79-607/07/11 13:3027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 218 ug/kg 1 07/12/11 16:38 67-64-1 C994.4
Benzene ND ug/kg 1 07/12/11 16:38 71-43-24.7
Bromobenzene ND ug/kg 1 07/12/11 16:38 108-86-14.7
Bromochloromethane ND ug/kg 1 07/12/11 16:38 74-97-54.7
Bromodichloromethane ND ug/kg 1 07/12/11 16:38 75-27-44.7
Bromoform ND ug/kg 1 07/12/11 16:38 75-25-24.7
Bromomethane ND ug/kg 1 07/12/11 16:38 74-83-99.4
2-Butanone (MEK)ND ug/kg 1 07/12/11 16:38 78-93-394.4
n-Butylbenzene ND ug/kg 1 07/12/11 16:38 104-51-84.7
sec-Butylbenzene ND ug/kg 1 07/12/11 16:38 135-98-84.7
tert-Butylbenzene ND ug/kg 1 07/12/11 16:38 98-06-64.7
Carbon tetrachloride ND ug/kg 1 07/12/11 16:38 56-23-54.7
Chlorobenzene ND ug/kg 1 07/12/11 16:38 108-90-74.7
Chloroethane ND ug/kg 1 07/12/11 16:38 75-00-39.4
Chloroform ND ug/kg 1 07/12/11 16:38 67-66-34.7
Chloromethane ND ug/kg 1 07/12/11 16:38 74-87-39.4
2-Chlorotoluene ND ug/kg 1 07/12/11 16:38 95-49-84.7
4-Chlorotoluene ND ug/kg 1 07/12/11 16:38 106-43-44.7
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/12/11 16:38 96-12-84.7
Dibromochloromethane ND ug/kg 1 07/12/11 16:38 124-48-14.7
1,2-Dibromoethane (EDB)ND ug/kg 1 07/12/11 16:38 106-93-44.7
Dibromomethane ND ug/kg 1 07/12/11 16:38 74-95-34.7
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 16:38 95-50-14.7
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 16:38 541-73-14.7
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 16:38 106-46-74.7
Dichlorodifluoromethane ND ug/kg 1 07/12/11 16:38 75-71-89.4
1,1-Dichloroethane ND ug/kg 1 07/12/11 16:38 75-34-34.7
1,2-Dichloroethane ND ug/kg 1 07/12/11 16:38 107-06-24.7
1,1-Dichloroethene ND ug/kg 1 07/12/11 16:38 75-35-44.7
cis-1,2-Dichloroethene ND ug/kg 1 07/12/11 16:38 156-59-24.7
trans-1,2-Dichloroethene ND ug/kg 1 07/12/11 16:38 156-60-54.7
1,2-Dichloropropane ND ug/kg 1 07/12/11 16:38 78-87-54.7
1,3-Dichloropropane ND ug/kg 1 07/12/11 16:38 142-28-94.7
2,2-Dichloropropane ND ug/kg 1 07/12/11 16:38 594-20-74.7
1,1-Dichloropropene ND ug/kg 1 07/12/11 16:38 563-58-64.7
cis-1,3-Dichloropropene ND ug/kg 1 07/12/11 16:38 10061-01-54.7
trans-1,3-Dichloropropene ND ug/kg 1 07/12/11 16:38 10061-02-64.7
Diisopropyl ether ND ug/kg 1 07/12/11 16:38 108-20-34.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 26 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 1A (6)Lab ID:9297694001 Collected:07/06/11 10:25 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/12/11 16:38 100-41-44.7
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 16:38 87-68-34.7
2-Hexanone ND ug/kg 1 07/12/11 16:38 591-78-647.2
Isopropylbenzene (Cumene)ND ug/kg 1 07/12/11 16:38 98-82-84.7
p-Isopropyltoluene ND ug/kg 1 07/12/11 16:38 99-87-64.7
Methylene Chloride ND ug/kg 1 07/12/11 16:38 75-09-218.9
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/12/11 16:38 108-10-147.2
Methyl-tert-butyl ether ND ug/kg 1 07/12/11 16:38 1634-04-44.7
Naphthalene ND ug/kg 1 07/12/11 16:38 91-20-34.7
n-Propylbenzene ND ug/kg 1 07/12/11 16:38 103-65-14.7
Styrene ND ug/kg 1 07/12/11 16:38 100-42-54.7
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/12/11 16:38 630-20-64.7
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/12/11 16:38 79-34-54.7
Tetrachloroethene ND ug/kg 1 07/12/11 16:38 127-18-44.7
Toluene ND ug/kg 1 07/12/11 16:38 108-88-34.7
1,2,3-Trichlorobenzene ND ug/kg 1 07/12/11 16:38 87-61-64.7
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 16:38 120-82-14.7
1,1,1-Trichloroethane ND ug/kg 1 07/12/11 16:38 71-55-64.7
1,1,2-Trichloroethane ND ug/kg 1 07/12/11 16:38 79-00-54.7
Trichloroethene ND ug/kg 1 07/12/11 16:38 79-01-64.7
Trichlorofluoromethane ND ug/kg 1 07/12/11 16:38 75-69-44.7
1,2,3-Trichloropropane ND ug/kg 1 07/12/11 16:38 96-18-44.7
1,2,4-Trimethylbenzene ND ug/kg 1 07/12/11 16:38 95-63-64.7
1,3,5-Trimethylbenzene ND ug/kg 1 07/12/11 16:38 108-67-84.7
Vinyl acetate ND ug/kg 1 07/12/11 16:38 108-05-447.2
Vinyl chloride ND ug/kg 1 07/12/11 16:38 75-01-49.4
Xylene (Total)ND ug/kg 1 07/12/11 16:38 1330-20-79.4
m&p-Xylene ND ug/kg 1 07/12/11 16:38 179601-23-19.4
o-Xylene ND ug/kg 1 07/12/11 16:38 95-47-64.7
Dibromofluoromethane (S)101 %1 07/12/11 16:38 1868-53-770-130
Toluene-d8 (S)105 %1 07/12/11 16:38 2037-26-570-130
4-Bromofluorobenzene (S)94 %1 07/12/11 16:38 460-00-470-130
1,2-Dichloroethane-d4 (S)90 %1 07/12/11 16:38 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 17.0 %1 07/08/11 08:530.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 27 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 1B (8)Lab ID:9297694002 Collected:07/06/11 10:40 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 17.2 mg/kg 1 07/12/11 01:36 68334-30-507/07/11 15:356.8
n-Pentacosane (S)46 %1 07/12/11 01:36 629-99-207/07/11 15:3541-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease ND mg/kg 1 07/11/11 12:0507/11/11 11:1595.1
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/12/11 14:55 8006-61-907/12/11 10:346.8
4-Bromofluorobenzene (S)145 %1 07/12/11 14:55 460-00-407/12/11 10:3470-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 3.2 mg/kg 1 07/13/11 15:04 7440-38-207/12/11 11:400.65
Barium 77.4 mg/kg 1 07/13/11 15:04 7440-39-307/12/11 11:400.65
Cadmium ND mg/kg 1 07/13/11 15:04 7440-43-907/12/11 11:400.13
Chromium 12.8 mg/kg 1 07/13/11 15:04 7440-47-307/12/11 11:400.65
Lead 20.4 mg/kg 1 07/13/11 15:04 7439-92-107/12/11 11:400.65
Selenium 2.2 mg/kg 1 07/13/11 15:04 7782-49-207/12/11 11:401.3
Silver ND mg/kg 1 07/13/11 15:04 7440-22-407/12/11 11:400.65
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.012 mg/kg 1 07/11/11 17:22 7439-97-607/08/11 15:100.0068
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/14/11 16:48 83-32-907/07/11 13:30447
Acenaphthylene ND ug/kg 1 07/14/11 16:48 208-96-807/07/11 13:30447
Aniline ND ug/kg 1 07/14/11 16:48 62-53-307/07/11 13:30447
Anthracene ND ug/kg 1 07/14/11 16:48 120-12-707/07/11 13:30447
Benzo(a)anthracene ND ug/kg 1 07/14/11 16:48 56-55-307/07/11 13:30447
Benzo(a)pyrene ND ug/kg 1 07/14/11 16:48 50-32-807/07/11 13:30447
Benzo(b)fluoranthene ND ug/kg 1 07/14/11 16:48 205-99-207/07/11 13:30447
Benzo(g,h,i)perylene ND ug/kg 1 07/14/11 16:48 191-24-207/07/11 13:30447
Benzo(k)fluoranthene ND ug/kg 1 07/14/11 16:48 207-08-907/07/11 13:30447
Benzoic Acid ND ug/kg 1 07/14/11 16:48 65-85-007/07/11 13:302230
Benzyl alcohol ND ug/kg 1 07/14/11 16:48 100-51-607/07/11 13:30893
4-Bromophenylphenyl ether ND ug/kg 1 07/14/11 16:48 101-55-307/07/11 13:30447
Butylbenzylphthalate ND ug/kg 1 07/14/11 16:48 85-68-707/07/11 13:30447
4-Chloro-3-methylphenol ND ug/kg 1 07/14/11 16:48 59-50-707/07/11 13:30893
4-Chloroaniline ND ug/kg 1 07/14/11 16:48 106-47-807/07/11 13:302230
bis(2-Chloroethoxy)methane ND ug/kg 1 07/14/11 16:48 111-91-107/07/11 13:30447
bis(2-Chloroethyl) ether ND ug/kg 1 07/14/11 16:48 111-44-407/07/11 13:30447
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/14/11 16:48 108-60-107/07/11 13:30447
2-Chloronaphthalene ND ug/kg 1 07/14/11 16:48 91-58-707/07/11 13:30447
2-Chlorophenol ND ug/kg 1 07/14/11 16:48 95-57-807/07/11 13:30447
4-Chlorophenylphenyl ether ND ug/kg 1 07/14/11 16:48 7005-72-307/07/11 13:30447
Chrysene ND ug/kg 1 07/14/11 16:48 218-01-907/07/11 13:30447
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 28 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 1B (8)Lab ID:9297694002 Collected:07/06/11 10:40 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/14/11 16:48 53-70-307/07/11 13:30447
Dibenzofuran ND ug/kg 1 07/14/11 16:48 132-64-907/07/11 13:30447
1,2-Dichlorobenzene ND ug/kg 1 07/14/11 16:48 95-50-107/07/11 13:30447
1,3-Dichlorobenzene ND ug/kg 1 07/14/11 16:48 541-73-107/07/11 13:30447
1,4-Dichlorobenzene ND ug/kg 1 07/14/11 16:48 106-46-707/07/11 13:30447
3,3'-Dichlorobenzidine ND ug/kg 1 07/14/11 16:48 91-94-107/07/11 13:302230
2,4-Dichlorophenol ND ug/kg 1 07/14/11 16:48 120-83-207/07/11 13:30447
Diethylphthalate ND ug/kg 1 07/14/11 16:48 84-66-207/07/11 13:30447
2,4-Dimethylphenol ND ug/kg 1 07/14/11 16:48 105-67-907/07/11 13:30447
Dimethylphthalate ND ug/kg 1 07/14/11 16:48 131-11-307/07/11 13:30447
Di-n-butylphthalate ND ug/kg 1 07/14/11 16:48 84-74-207/07/11 13:30447
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/14/11 16:48 534-52-107/07/11 13:30893
2,4-Dinitrophenol ND ug/kg 1 07/14/11 16:48 51-28-507/07/11 13:302230
2,4-Dinitrotoluene ND ug/kg 1 07/14/11 16:48 121-14-207/07/11 13:30447
2,6-Dinitrotoluene ND ug/kg 1 07/14/11 16:48 606-20-207/07/11 13:30447
Di-n-octylphthalate ND ug/kg 1 07/14/11 16:48 117-84-007/07/11 13:30447
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/14/11 16:48 117-81-707/07/11 13:30447
Fluoranthene ND ug/kg 1 07/14/11 16:48 206-44-007/07/11 13:30447
Fluorene ND ug/kg 1 07/14/11 16:48 86-73-707/07/11 13:30447
Hexachloro-1,3-butadiene ND ug/kg 1 07/14/11 16:48 87-68-307/07/11 13:30447
Hexachlorobenzene ND ug/kg 1 07/14/11 16:48 118-74-107/07/11 13:30447
Hexachlorocyclopentadiene ND ug/kg 1 07/14/11 16:48 77-47-407/07/11 13:30447
Hexachloroethane ND ug/kg 1 07/14/11 16:48 67-72-107/07/11 13:30447
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/14/11 16:48 193-39-507/07/11 13:30447
Isophorone ND ug/kg 1 07/14/11 16:48 78-59-107/07/11 13:30447
1-Methylnaphthalene ND ug/kg 1 07/14/11 16:48 90-12-007/07/11 13:30447
2-Methylnaphthalene ND ug/kg 1 07/14/11 16:48 91-57-607/07/11 13:30447
2-Methylphenol(o-Cresol)ND ug/kg 1 07/14/11 16:48 95-48-707/07/11 13:30447
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/14/11 16:4807/07/11 13:30447
Naphthalene ND ug/kg 1 07/14/11 16:48 91-20-307/07/11 13:30447
2-Nitroaniline ND ug/kg 1 07/14/11 16:48 88-74-407/07/11 13:302230
3-Nitroaniline ND ug/kg 1 07/14/11 16:48 99-09-207/07/11 13:302230
4-Nitroaniline ND ug/kg 1 07/14/11 16:48 100-01-607/07/11 13:30893
Nitrobenzene ND ug/kg 1 07/14/11 16:48 98-95-307/07/11 13:30447
2-Nitrophenol ND ug/kg 1 07/14/11 16:48 88-75-507/07/11 13:30447
4-Nitrophenol ND ug/kg 1 07/14/11 16:48 100-02-707/07/11 13:302230
N-Nitrosodimethylamine ND ug/kg 1 07/14/11 16:48 62-75-907/07/11 13:30447
N-Nitroso-di-n-propylamine ND ug/kg 1 07/14/11 16:48 621-64-707/07/11 13:30447
N-Nitrosodiphenylamine ND ug/kg 1 07/14/11 16:48 86-30-607/07/11 13:30447
Pentachlorophenol ND ug/kg 1 07/14/11 16:48 87-86-507/07/11 13:302230
Phenanthrene ND ug/kg 1 07/14/11 16:48 85-01-807/07/11 13:30447
Phenol ND ug/kg 1 07/14/11 16:48 108-95-207/07/11 13:30447
Pyrene ND ug/kg 1 07/14/11 16:48 129-00-007/07/11 13:30447
1,2,4-Trichlorobenzene ND ug/kg 1 07/14/11 16:48 120-82-107/07/11 13:30447
2,4,5-Trichlorophenol ND ug/kg 1 07/14/11 16:48 95-95-407/07/11 13:30447
2,4,6-Trichlorophenol ND ug/kg 1 07/14/11 16:48 88-06-207/07/11 13:30447
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 29 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 1B (8)Lab ID:9297694002 Collected:07/06/11 10:40 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)49 %1 07/14/11 16:48 4165-60-007/07/11 13:3023-110
2-Fluorobiphenyl (S)64 %1 07/14/11 16:48 321-60-807/07/11 13:3030-110
Terphenyl-d14 (S)61 %1 07/14/11 16:48 1718-51-007/07/11 13:3028-110
Phenol-d6 (S)54 %1 07/14/11 16:48 13127-88-307/07/11 13:3022-110
2-Fluorophenol (S)57 %1 07/14/11 16:48 367-12-407/07/11 13:3013-110
2,4,6-Tribromophenol (S)70 %1 07/14/11 16:48 118-79-607/07/11 13:3027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 168 ug/kg 1 07/12/11 16:58 67-64-1 C9103
Benzene ND ug/kg 1 07/12/11 16:58 71-43-25.2
Bromobenzene ND ug/kg 1 07/12/11 16:58 108-86-15.2
Bromochloromethane ND ug/kg 1 07/12/11 16:58 74-97-55.2
Bromodichloromethane ND ug/kg 1 07/12/11 16:58 75-27-45.2
Bromoform ND ug/kg 1 07/12/11 16:58 75-25-25.2
Bromomethane ND ug/kg 1 07/12/11 16:58 74-83-910.3
2-Butanone (MEK)ND ug/kg 1 07/12/11 16:58 78-93-3103
n-Butylbenzene ND ug/kg 1 07/12/11 16:58 104-51-85.2
sec-Butylbenzene ND ug/kg 1 07/12/11 16:58 135-98-85.2
tert-Butylbenzene ND ug/kg 1 07/12/11 16:58 98-06-65.2
Carbon tetrachloride ND ug/kg 1 07/12/11 16:58 56-23-55.2
Chlorobenzene ND ug/kg 1 07/12/11 16:58 108-90-75.2
Chloroethane ND ug/kg 1 07/12/11 16:58 75-00-310.3
Chloroform ND ug/kg 1 07/12/11 16:58 67-66-35.2
Chloromethane ND ug/kg 1 07/12/11 16:58 74-87-310.3
2-Chlorotoluene ND ug/kg 1 07/12/11 16:58 95-49-85.2
4-Chlorotoluene ND ug/kg 1 07/12/11 16:58 106-43-45.2
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/12/11 16:58 96-12-85.2
Dibromochloromethane ND ug/kg 1 07/12/11 16:58 124-48-15.2
1,2-Dibromoethane (EDB)ND ug/kg 1 07/12/11 16:58 106-93-45.2
Dibromomethane ND ug/kg 1 07/12/11 16:58 74-95-35.2
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 16:58 95-50-15.2
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 16:58 541-73-15.2
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 16:58 106-46-75.2
Dichlorodifluoromethane ND ug/kg 1 07/12/11 16:58 75-71-810.3
1,1-Dichloroethane ND ug/kg 1 07/12/11 16:58 75-34-35.2
1,2-Dichloroethane ND ug/kg 1 07/12/11 16:58 107-06-25.2
1,1-Dichloroethene ND ug/kg 1 07/12/11 16:58 75-35-45.2
cis-1,2-Dichloroethene ND ug/kg 1 07/12/11 16:58 156-59-25.2
trans-1,2-Dichloroethene ND ug/kg 1 07/12/11 16:58 156-60-55.2
1,2-Dichloropropane ND ug/kg 1 07/12/11 16:58 78-87-55.2
1,3-Dichloropropane ND ug/kg 1 07/12/11 16:58 142-28-95.2
2,2-Dichloropropane ND ug/kg 1 07/12/11 16:58 594-20-75.2
1,1-Dichloropropene ND ug/kg 1 07/12/11 16:58 563-58-65.2
cis-1,3-Dichloropropene ND ug/kg 1 07/12/11 16:58 10061-01-55.2
trans-1,3-Dichloropropene ND ug/kg 1 07/12/11 16:58 10061-02-65.2
Diisopropyl ether ND ug/kg 1 07/12/11 16:58 108-20-35.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 30 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 1B (8)Lab ID:9297694002 Collected:07/06/11 10:40 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/12/11 16:58 100-41-45.2
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 16:58 87-68-35.2
2-Hexanone ND ug/kg 1 07/12/11 16:58 591-78-651.7
Isopropylbenzene (Cumene)ND ug/kg 1 07/12/11 16:58 98-82-85.2
p-Isopropyltoluene ND ug/kg 1 07/12/11 16:58 99-87-65.2
Methylene Chloride ND ug/kg 1 07/12/11 16:58 75-09-220.7
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/12/11 16:58 108-10-151.7
Methyl-tert-butyl ether ND ug/kg 1 07/12/11 16:58 1634-04-45.2
Naphthalene ND ug/kg 1 07/12/11 16:58 91-20-35.2
n-Propylbenzene ND ug/kg 1 07/12/11 16:58 103-65-15.2
Styrene ND ug/kg 1 07/12/11 16:58 100-42-55.2
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/12/11 16:58 630-20-65.2
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/12/11 16:58 79-34-55.2
Tetrachloroethene ND ug/kg 1 07/12/11 16:58 127-18-45.2
Toluene ND ug/kg 1 07/12/11 16:58 108-88-35.2
1,2,3-Trichlorobenzene ND ug/kg 1 07/12/11 16:58 87-61-65.2
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 16:58 120-82-15.2
1,1,1-Trichloroethane ND ug/kg 1 07/12/11 16:58 71-55-65.2
1,1,2-Trichloroethane ND ug/kg 1 07/12/11 16:58 79-00-55.2
Trichloroethene ND ug/kg 1 07/12/11 16:58 79-01-65.2
Trichlorofluoromethane ND ug/kg 1 07/12/11 16:58 75-69-45.2
1,2,3-Trichloropropane ND ug/kg 1 07/12/11 16:58 96-18-45.2
1,2,4-Trimethylbenzene ND ug/kg 1 07/12/11 16:58 95-63-65.2
1,3,5-Trimethylbenzene ND ug/kg 1 07/12/11 16:58 108-67-85.2
Vinyl acetate ND ug/kg 1 07/12/11 16:58 108-05-451.7
Vinyl chloride ND ug/kg 1 07/12/11 16:58 75-01-410.3
Xylene (Total)ND ug/kg 1 07/12/11 16:58 1330-20-710.3
m&p-Xylene ND ug/kg 1 07/12/11 16:58 179601-23-110.3
o-Xylene ND ug/kg 1 07/12/11 16:58 95-47-65.2
Dibromofluoromethane (S)97 %1 07/12/11 16:58 1868-53-770-130
Toluene-d8 (S)100 %1 07/12/11 16:58 2037-26-570-130
4-Bromofluorobenzene (S)89 %1 07/12/11 16:58 460-00-470-130
1,2-Dichloroethane-d4 (S)88 %1 07/12/11 16:58 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 26.4 %1 07/08/11 08:530.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 31 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 2A (6-7)Lab ID:9297694003 Collected:07/06/11 11:05 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 20.2 mg/kg 1 07/12/11 02:04 68334-30-507/07/11 15:355.9
n-Pentacosane (S)48 %1 07/12/11 02:04 629-99-207/07/11 15:3541-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease ND mg/kg 1 07/11/11 12:0507/11/11 11:1682.9
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/12/11 15:20 8006-61-907/12/11 10:345.7
4-Bromofluorobenzene (S)141 %1 07/12/11 15:20 460-00-407/12/11 10:3470-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 2.6 mg/kg 1 07/13/11 15:16 7440-38-207/12/11 11:400.56
Barium 45.7 mg/kg 1 07/13/11 15:16 7440-39-307/12/11 11:400.56
Cadmium ND mg/kg 1 07/13/11 15:16 7440-43-907/12/11 11:400.11
Chromium 5.7 mg/kg 1 07/13/11 15:16 7440-47-307/12/11 11:400.56
Lead 18.2 mg/kg 1 07/13/11 15:16 7439-92-107/12/11 11:400.56
Selenium ND mg/kg 1 07/13/11 15:16 7782-49-207/12/11 11:401.1
Silver ND mg/kg 1 07/13/11 15:16 7440-22-407/12/11 11:400.56
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.016 mg/kg 1 07/11/11 17:38 7439-97-607/08/11 15:100.0057
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/14/11 17:16 83-32-907/07/11 13:30390
Acenaphthylene ND ug/kg 1 07/14/11 17:16 208-96-807/07/11 13:30390
Aniline ND ug/kg 1 07/14/11 17:16 62-53-307/07/11 13:30390
Anthracene ND ug/kg 1 07/14/11 17:16 120-12-707/07/11 13:30390
Benzo(a)anthracene ND ug/kg 1 07/14/11 17:16 56-55-307/07/11 13:30390
Benzo(a)pyrene ND ug/kg 1 07/14/11 17:16 50-32-807/07/11 13:30390
Benzo(b)fluoranthene ND ug/kg 1 07/14/11 17:16 205-99-207/07/11 13:30390
Benzo(g,h,i)perylene ND ug/kg 1 07/14/11 17:16 191-24-207/07/11 13:30390
Benzo(k)fluoranthene ND ug/kg 1 07/14/11 17:16 207-08-907/07/11 13:30390
Benzoic Acid ND ug/kg 1 07/14/11 17:16 65-85-007/07/11 13:301950
Benzyl alcohol ND ug/kg 1 07/14/11 17:16 100-51-607/07/11 13:30779
4-Bromophenylphenyl ether ND ug/kg 1 07/14/11 17:16 101-55-307/07/11 13:30390
Butylbenzylphthalate ND ug/kg 1 07/14/11 17:16 85-68-707/07/11 13:30390
4-Chloro-3-methylphenol ND ug/kg 1 07/14/11 17:16 59-50-707/07/11 13:30779
4-Chloroaniline ND ug/kg 1 07/14/11 17:16 106-47-807/07/11 13:301950
bis(2-Chloroethoxy)methane ND ug/kg 1 07/14/11 17:16 111-91-107/07/11 13:30390
bis(2-Chloroethyl) ether ND ug/kg 1 07/14/11 17:16 111-44-407/07/11 13:30390
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/14/11 17:16 108-60-107/07/11 13:30390
2-Chloronaphthalene ND ug/kg 1 07/14/11 17:16 91-58-707/07/11 13:30390
2-Chlorophenol ND ug/kg 1 07/14/11 17:16 95-57-807/07/11 13:30390
4-Chlorophenylphenyl ether ND ug/kg 1 07/14/11 17:16 7005-72-307/07/11 13:30390
Chrysene ND ug/kg 1 07/14/11 17:16 218-01-907/07/11 13:30390
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 32 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 2A (6-7)Lab ID:9297694003 Collected:07/06/11 11:05 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/14/11 17:16 53-70-307/07/11 13:30390
Dibenzofuran ND ug/kg 1 07/14/11 17:16 132-64-907/07/11 13:30390
1,2-Dichlorobenzene ND ug/kg 1 07/14/11 17:16 95-50-107/07/11 13:30390
1,3-Dichlorobenzene ND ug/kg 1 07/14/11 17:16 541-73-107/07/11 13:30390
1,4-Dichlorobenzene ND ug/kg 1 07/14/11 17:16 106-46-707/07/11 13:30390
3,3'-Dichlorobenzidine ND ug/kg 1 07/14/11 17:16 91-94-107/07/11 13:301950
2,4-Dichlorophenol ND ug/kg 1 07/14/11 17:16 120-83-207/07/11 13:30390
Diethylphthalate ND ug/kg 1 07/14/11 17:16 84-66-207/07/11 13:30390
2,4-Dimethylphenol ND ug/kg 1 07/14/11 17:16 105-67-907/07/11 13:30390
Dimethylphthalate ND ug/kg 1 07/14/11 17:16 131-11-307/07/11 13:30390
Di-n-butylphthalate ND ug/kg 1 07/14/11 17:16 84-74-207/07/11 13:30390
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/14/11 17:16 534-52-107/07/11 13:30779
2,4-Dinitrophenol ND ug/kg 1 07/14/11 17:16 51-28-507/07/11 13:301950
2,4-Dinitrotoluene ND ug/kg 1 07/14/11 17:16 121-14-207/07/11 13:30390
2,6-Dinitrotoluene ND ug/kg 1 07/14/11 17:16 606-20-207/07/11 13:30390
Di-n-octylphthalate ND ug/kg 1 07/14/11 17:16 117-84-007/07/11 13:30390
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/14/11 17:16 117-81-707/07/11 13:30390
Fluoranthene 464 ug/kg 1 07/14/11 17:16 206-44-007/07/11 13:30390
Fluorene ND ug/kg 1 07/14/11 17:16 86-73-707/07/11 13:30390
Hexachloro-1,3-butadiene ND ug/kg 1 07/14/11 17:16 87-68-307/07/11 13:30390
Hexachlorobenzene ND ug/kg 1 07/14/11 17:16 118-74-107/07/11 13:30390
Hexachlorocyclopentadiene ND ug/kg 1 07/14/11 17:16 77-47-407/07/11 13:30390
Hexachloroethane ND ug/kg 1 07/14/11 17:16 67-72-107/07/11 13:30390
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/14/11 17:16 193-39-507/07/11 13:30390
Isophorone ND ug/kg 1 07/14/11 17:16 78-59-107/07/11 13:30390
1-Methylnaphthalene ND ug/kg 1 07/14/11 17:16 90-12-007/07/11 13:30390
2-Methylnaphthalene ND ug/kg 1 07/14/11 17:16 91-57-607/07/11 13:30390
2-Methylphenol(o-Cresol)ND ug/kg 1 07/14/11 17:16 95-48-707/07/11 13:30390
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/14/11 17:1607/07/11 13:30390
Naphthalene ND ug/kg 1 07/14/11 17:16 91-20-307/07/11 13:30390
2-Nitroaniline ND ug/kg 1 07/14/11 17:16 88-74-407/07/11 13:301950
3-Nitroaniline ND ug/kg 1 07/14/11 17:16 99-09-207/07/11 13:301950
4-Nitroaniline ND ug/kg 1 07/14/11 17:16 100-01-607/07/11 13:30779
Nitrobenzene ND ug/kg 1 07/14/11 17:16 98-95-307/07/11 13:30390
2-Nitrophenol ND ug/kg 1 07/14/11 17:16 88-75-507/07/11 13:30390
4-Nitrophenol ND ug/kg 1 07/14/11 17:16 100-02-707/07/11 13:301950
N-Nitrosodimethylamine ND ug/kg 1 07/14/11 17:16 62-75-907/07/11 13:30390
N-Nitroso-di-n-propylamine ND ug/kg 1 07/14/11 17:16 621-64-707/07/11 13:30390
N-Nitrosodiphenylamine ND ug/kg 1 07/14/11 17:16 86-30-607/07/11 13:30390
Pentachlorophenol ND ug/kg 1 07/14/11 17:16 87-86-507/07/11 13:301950
Phenanthrene ND ug/kg 1 07/14/11 17:16 85-01-807/07/11 13:30390
Phenol ND ug/kg 1 07/14/11 17:16 108-95-207/07/11 13:30390
Pyrene 391 ug/kg 1 07/14/11 17:16 129-00-007/07/11 13:30390
1,2,4-Trichlorobenzene ND ug/kg 1 07/14/11 17:16 120-82-107/07/11 13:30390
2,4,5-Trichlorophenol ND ug/kg 1 07/14/11 17:16 95-95-407/07/11 13:30390
2,4,6-Trichlorophenol ND ug/kg 1 07/14/11 17:16 88-06-207/07/11 13:30390
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 33 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 2A (6-7)Lab ID:9297694003 Collected:07/06/11 11:05 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)86 %1 07/14/11 17:16 4165-60-007/07/11 13:3023-110
2-Fluorobiphenyl (S)82 %1 07/14/11 17:16 321-60-807/07/11 13:3030-110
Terphenyl-d14 (S)84 %1 07/14/11 17:16 1718-51-007/07/11 13:3028-110
Phenol-d6 (S)57 %1 07/14/11 17:16 13127-88-307/07/11 13:3022-110
2-Fluorophenol (S)53 %1 07/14/11 17:16 367-12-407/07/11 13:3013-110
2,4,6-Tribromophenol (S)77 %1 07/14/11 17:16 118-79-607/07/11 13:3027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 148 ug/kg 1 07/12/11 17:18 67-64-1 C989.1
Benzene ND ug/kg 1 07/12/11 17:18 71-43-24.5
Bromobenzene ND ug/kg 1 07/12/11 17:18 108-86-14.5
Bromochloromethane ND ug/kg 1 07/12/11 17:18 74-97-54.5
Bromodichloromethane ND ug/kg 1 07/12/11 17:18 75-27-44.5
Bromoform ND ug/kg 1 07/12/11 17:18 75-25-24.5
Bromomethane ND ug/kg 1 07/12/11 17:18 74-83-98.9
2-Butanone (MEK)ND ug/kg 1 07/12/11 17:18 78-93-389.1
n-Butylbenzene ND ug/kg 1 07/12/11 17:18 104-51-84.5
sec-Butylbenzene ND ug/kg 1 07/12/11 17:18 135-98-84.5
tert-Butylbenzene ND ug/kg 1 07/12/11 17:18 98-06-64.5
Carbon tetrachloride ND ug/kg 1 07/12/11 17:18 56-23-54.5
Chlorobenzene ND ug/kg 1 07/12/11 17:18 108-90-74.5
Chloroethane ND ug/kg 1 07/12/11 17:18 75-00-38.9
Chloroform ND ug/kg 1 07/12/11 17:18 67-66-34.5
Chloromethane ND ug/kg 1 07/12/11 17:18 74-87-38.9
2-Chlorotoluene ND ug/kg 1 07/12/11 17:18 95-49-84.5
4-Chlorotoluene ND ug/kg 1 07/12/11 17:18 106-43-44.5
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/12/11 17:18 96-12-84.5
Dibromochloromethane ND ug/kg 1 07/12/11 17:18 124-48-14.5
1,2-Dibromoethane (EDB)ND ug/kg 1 07/12/11 17:18 106-93-44.5
Dibromomethane ND ug/kg 1 07/12/11 17:18 74-95-34.5
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 17:18 95-50-14.5
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 17:18 541-73-14.5
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 17:18 106-46-74.5
Dichlorodifluoromethane ND ug/kg 1 07/12/11 17:18 75-71-88.9
1,1-Dichloroethane ND ug/kg 1 07/12/11 17:18 75-34-34.5
1,2-Dichloroethane ND ug/kg 1 07/12/11 17:18 107-06-24.5
1,1-Dichloroethene ND ug/kg 1 07/12/11 17:18 75-35-44.5
cis-1,2-Dichloroethene ND ug/kg 1 07/12/11 17:18 156-59-24.5
trans-1,2-Dichloroethene ND ug/kg 1 07/12/11 17:18 156-60-54.5
1,2-Dichloropropane ND ug/kg 1 07/12/11 17:18 78-87-54.5
1,3-Dichloropropane ND ug/kg 1 07/12/11 17:18 142-28-94.5
2,2-Dichloropropane ND ug/kg 1 07/12/11 17:18 594-20-74.5
1,1-Dichloropropene ND ug/kg 1 07/12/11 17:18 563-58-64.5
cis-1,3-Dichloropropene ND ug/kg 1 07/12/11 17:18 10061-01-54.5
trans-1,3-Dichloropropene ND ug/kg 1 07/12/11 17:18 10061-02-64.5
Diisopropyl ether ND ug/kg 1 07/12/11 17:18 108-20-34.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 34 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 2A (6-7)Lab ID:9297694003 Collected:07/06/11 11:05 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/12/11 17:18 100-41-44.5
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 17:18 87-68-34.5
2-Hexanone ND ug/kg 1 07/12/11 17:18 591-78-644.5
Isopropylbenzene (Cumene)ND ug/kg 1 07/12/11 17:18 98-82-84.5
p-Isopropyltoluene ND ug/kg 1 07/12/11 17:18 99-87-64.5
Methylene Chloride ND ug/kg 1 07/12/11 17:18 75-09-217.8
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/12/11 17:18 108-10-144.5
Methyl-tert-butyl ether ND ug/kg 1 07/12/11 17:18 1634-04-44.5
Naphthalene ND ug/kg 1 07/12/11 17:18 91-20-34.5
n-Propylbenzene ND ug/kg 1 07/12/11 17:18 103-65-14.5
Styrene ND ug/kg 1 07/12/11 17:18 100-42-54.5
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/12/11 17:18 630-20-64.5
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/12/11 17:18 79-34-54.5
Tetrachloroethene ND ug/kg 1 07/12/11 17:18 127-18-44.5
Toluene ND ug/kg 1 07/12/11 17:18 108-88-34.5
1,2,3-Trichlorobenzene ND ug/kg 1 07/12/11 17:18 87-61-64.5
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 17:18 120-82-14.5
1,1,1-Trichloroethane ND ug/kg 1 07/12/11 17:18 71-55-64.5
1,1,2-Trichloroethane ND ug/kg 1 07/12/11 17:18 79-00-54.5
Trichloroethene ND ug/kg 1 07/12/11 17:18 79-01-64.5
Trichlorofluoromethane ND ug/kg 1 07/12/11 17:18 75-69-44.5
1,2,3-Trichloropropane ND ug/kg 1 07/12/11 17:18 96-18-44.5
1,2,4-Trimethylbenzene ND ug/kg 1 07/12/11 17:18 95-63-64.5
1,3,5-Trimethylbenzene ND ug/kg 1 07/12/11 17:18 108-67-84.5
Vinyl acetate ND ug/kg 1 07/12/11 17:18 108-05-444.5
Vinyl chloride ND ug/kg 1 07/12/11 17:18 75-01-48.9
Xylene (Total)ND ug/kg 1 07/12/11 17:18 1330-20-78.9
m&p-Xylene ND ug/kg 1 07/12/11 17:18 179601-23-18.9
o-Xylene ND ug/kg 1 07/12/11 17:18 95-47-64.5
Dibromofluoromethane (S)100 %1 07/12/11 17:18 1868-53-770-130
Toluene-d8 (S)102 %1 07/12/11 17:18 2037-26-570-130
4-Bromofluorobenzene (S)89 %1 07/12/11 17:18 460-00-470-130
1,2-Dichloroethane-d4 (S)89 %1 07/12/11 17:18 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 15.6 %1 07/08/11 08:530.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 35 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 2B (8-9)Lab ID:9297694004 Collected:07/06/11 11:15 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 9.2 mg/kg 1 07/12/11 02:04 68334-30-507/07/11 15:356.5
n-Pentacosane (S)56 %1 07/12/11 02:04 629-99-207/07/11 15:3541-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease ND mg/kg 1 07/11/11 12:0507/11/11 11:1690.9
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/12/11 15:44 8006-61-907/12/11 10:346.2
4-Bromofluorobenzene (S)134 %1 07/12/11 15:44 460-00-407/12/11 10:3470-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 2.8 mg/kg 1 07/13/11 15:20 7440-38-207/12/11 11:400.55
Barium 90.5 mg/kg 1 07/13/11 15:20 7440-39-307/12/11 11:400.55
Cadmium ND mg/kg 1 07/13/11 15:20 7440-43-907/12/11 11:400.11
Chromium 4.8 mg/kg 1 07/13/11 15:20 7440-47-307/12/11 11:400.55
Lead 26.0 mg/kg 1 07/13/11 15:20 7439-92-107/12/11 11:400.55
Selenium 1.5 mg/kg 1 07/13/11 15:20 7782-49-207/12/11 11:401.1
Silver ND mg/kg 1 07/13/11 15:20 7440-22-407/12/11 11:400.55
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.021 mg/kg 1 07/11/11 17:43 7439-97-607/08/11 15:100.0046
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/15/11 13:48 83-32-907/07/11 13:302140
Acenaphthylene ND ug/kg 1 07/15/11 13:48 208-96-807/07/11 13:302140
Aniline ND ug/kg 1 07/15/11 13:48 62-53-307/07/11 13:302140
Anthracene ND ug/kg 1 07/15/11 13:48 120-12-707/07/11 13:302140
Benzo(a)anthracene ND ug/kg 1 07/15/11 13:48 56-55-307/07/11 13:302140
Benzo(a)pyrene ND ug/kg 1 07/15/11 13:48 50-32-807/07/11 13:302140
Benzo(b)fluoranthene ND ug/kg 1 07/15/11 13:48 205-99-207/07/11 13:302140
Benzo(g,h,i)perylene ND ug/kg 1 07/15/11 13:48 191-24-207/07/11 13:302140
Benzo(k)fluoranthene ND ug/kg 1 07/15/11 13:48 207-08-907/07/11 13:302140
Benzoic Acid ND ug/kg 1 07/15/11 13:48 65-85-007/07/11 13:3010700
Benzyl alcohol ND ug/kg 1 07/15/11 13:48 100-51-607/07/11 13:304290
4-Bromophenylphenyl ether ND ug/kg 1 07/15/11 13:48 101-55-307/07/11 13:302140
Butylbenzylphthalate ND ug/kg 1 07/15/11 13:48 85-68-707/07/11 13:302140
4-Chloro-3-methylphenol ND ug/kg 1 07/15/11 13:48 59-50-707/07/11 13:304290
4-Chloroaniline ND ug/kg 1 07/15/11 13:48 106-47-807/07/11 13:3010700
bis(2-Chloroethoxy)methane ND ug/kg 1 07/15/11 13:48 111-91-107/07/11 13:302140
bis(2-Chloroethyl) ether ND ug/kg 1 07/15/11 13:48 111-44-407/07/11 13:302140
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/15/11 13:48 108-60-107/07/11 13:302140
2-Chloronaphthalene ND ug/kg 1 07/15/11 13:48 91-58-707/07/11 13:302140
2-Chlorophenol ND ug/kg 1 07/15/11 13:48 95-57-807/07/11 13:302140
4-Chlorophenylphenyl ether ND ug/kg 1 07/15/11 13:48 7005-72-307/07/11 13:302140
Chrysene ND ug/kg 1 07/15/11 13:48 218-01-907/07/11 13:302140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 36 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 2B (8-9)Lab ID:9297694004 Collected:07/06/11 11:15 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/15/11 13:48 53-70-307/07/11 13:302140
Dibenzofuran ND ug/kg 1 07/15/11 13:48 132-64-907/07/11 13:302140
1,2-Dichlorobenzene ND ug/kg 1 07/15/11 13:48 95-50-107/07/11 13:302140
1,3-Dichlorobenzene ND ug/kg 1 07/15/11 13:48 541-73-107/07/11 13:302140
1,4-Dichlorobenzene ND ug/kg 1 07/15/11 13:48 106-46-707/07/11 13:302140
3,3'-Dichlorobenzidine ND ug/kg 1 07/15/11 13:48 91-94-107/07/11 13:3010700
2,4-Dichlorophenol ND ug/kg 1 07/15/11 13:48 120-83-207/07/11 13:302140
Diethylphthalate ND ug/kg 1 07/15/11 13:48 84-66-207/07/11 13:302140
2,4-Dimethylphenol ND ug/kg 1 07/15/11 13:48 105-67-907/07/11 13:302140
Dimethylphthalate ND ug/kg 1 07/15/11 13:48 131-11-307/07/11 13:302140
Di-n-butylphthalate ND ug/kg 1 07/15/11 13:48 84-74-207/07/11 13:302140
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/15/11 13:48 534-52-107/07/11 13:304290
2,4-Dinitrophenol ND ug/kg 1 07/15/11 13:48 51-28-507/07/11 13:3010700
2,4-Dinitrotoluene ND ug/kg 1 07/15/11 13:48 121-14-207/07/11 13:302140
2,6-Dinitrotoluene ND ug/kg 1 07/15/11 13:48 606-20-207/07/11 13:302140
Di-n-octylphthalate ND ug/kg 1 07/15/11 13:48 117-84-007/07/11 13:302140
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/15/11 13:48 117-81-707/07/11 13:302140
Fluoranthene ND ug/kg 1 07/15/11 13:48 206-44-007/07/11 13:302140
Fluorene ND ug/kg 1 07/15/11 13:48 86-73-707/07/11 13:302140
Hexachloro-1,3-butadiene ND ug/kg 1 07/15/11 13:48 87-68-307/07/11 13:302140
Hexachlorobenzene ND ug/kg 1 07/15/11 13:48 118-74-107/07/11 13:302140
Hexachlorocyclopentadiene ND ug/kg 1 07/15/11 13:48 77-47-407/07/11 13:302140
Hexachloroethane ND ug/kg 1 07/15/11 13:48 67-72-107/07/11 13:302140
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/15/11 13:48 193-39-507/07/11 13:302140
Isophorone ND ug/kg 1 07/15/11 13:48 78-59-107/07/11 13:302140
1-Methylnaphthalene ND ug/kg 1 07/15/11 13:48 90-12-007/07/11 13:302140
2-Methylnaphthalene ND ug/kg 1 07/15/11 13:48 91-57-607/07/11 13:302140
2-Methylphenol(o-Cresol)ND ug/kg 1 07/15/11 13:48 95-48-707/07/11 13:302140
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/15/11 13:4807/07/11 13:302140
Naphthalene ND ug/kg 1 07/15/11 13:48 91-20-307/07/11 13:302140
2-Nitroaniline ND ug/kg 1 07/15/11 13:48 88-74-407/07/11 13:3010700
3-Nitroaniline ND ug/kg 1 07/15/11 13:48 99-09-207/07/11 13:3010700
4-Nitroaniline ND ug/kg 1 07/15/11 13:48 100-01-607/07/11 13:304290
Nitrobenzene ND ug/kg 1 07/15/11 13:48 98-95-307/07/11 13:302140
2-Nitrophenol ND ug/kg 1 07/15/11 13:48 88-75-507/07/11 13:302140
4-Nitrophenol ND ug/kg 1 07/15/11 13:48 100-02-707/07/11 13:3010700
N-Nitrosodimethylamine ND ug/kg 1 07/15/11 13:48 62-75-907/07/11 13:302140
N-Nitroso-di-n-propylamine ND ug/kg 1 07/15/11 13:48 621-64-707/07/11 13:302140
N-Nitrosodiphenylamine ND ug/kg 1 07/15/11 13:48 86-30-607/07/11 13:302140
Pentachlorophenol ND ug/kg 1 07/15/11 13:48 87-86-507/07/11 13:3010700
Phenanthrene ND ug/kg 1 07/15/11 13:48 85-01-807/07/11 13:302140
Phenol ND ug/kg 1 07/15/11 13:48 108-95-2 P307/07/11 13:302140
Pyrene ND ug/kg 1 07/15/11 13:48 129-00-007/07/11 13:302140
1,2,4-Trichlorobenzene ND ug/kg 1 07/15/11 13:48 120-82-107/07/11 13:302140
2,4,5-Trichlorophenol ND ug/kg 1 07/15/11 13:48 95-95-407/07/11 13:302140
2,4,6-Trichlorophenol ND ug/kg 1 07/15/11 13:48 88-06-207/07/11 13:302140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 37 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 2B (8-9)Lab ID:9297694004 Collected:07/06/11 11:15 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)47 %1 07/15/11 13:48 4165-60-007/07/11 13:3023-110
2-Fluorobiphenyl (S)75 %1 07/15/11 13:48 321-60-807/07/11 13:3030-110
Terphenyl-d14 (S)79 %1 07/15/11 13:48 1718-51-007/07/11 13:3028-110
Phenol-d6 (S)58 %1 07/15/11 13:48 13127-88-307/07/11 13:3022-110
2-Fluorophenol (S)64 %1 07/15/11 13:48 367-12-407/07/11 13:3013-110
2,4,6-Tribromophenol (S)68 %1 07/15/11 13:48 118-79-607/07/11 13:3027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 104 ug/kg 1 07/12/11 17:39 67-64-1 C9101
Benzene ND ug/kg 1 07/12/11 17:39 71-43-25.1
Bromobenzene ND ug/kg 1 07/12/11 17:39 108-86-15.1
Bromochloromethane ND ug/kg 1 07/12/11 17:39 74-97-55.1
Bromodichloromethane ND ug/kg 1 07/12/11 17:39 75-27-45.1
Bromoform ND ug/kg 1 07/12/11 17:39 75-25-25.1
Bromomethane ND ug/kg 1 07/12/11 17:39 74-83-910.1
2-Butanone (MEK)ND ug/kg 1 07/12/11 17:39 78-93-3101
n-Butylbenzene ND ug/kg 1 07/12/11 17:39 104-51-85.1
sec-Butylbenzene ND ug/kg 1 07/12/11 17:39 135-98-85.1
tert-Butylbenzene ND ug/kg 1 07/12/11 17:39 98-06-65.1
Carbon tetrachloride ND ug/kg 1 07/12/11 17:39 56-23-55.1
Chlorobenzene ND ug/kg 1 07/12/11 17:39 108-90-75.1
Chloroethane ND ug/kg 1 07/12/11 17:39 75-00-310.1
Chloroform ND ug/kg 1 07/12/11 17:39 67-66-35.1
Chloromethane ND ug/kg 1 07/12/11 17:39 74-87-310.1
2-Chlorotoluene ND ug/kg 1 07/12/11 17:39 95-49-85.1
4-Chlorotoluene ND ug/kg 1 07/12/11 17:39 106-43-45.1
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/12/11 17:39 96-12-85.1
Dibromochloromethane ND ug/kg 1 07/12/11 17:39 124-48-15.1
1,2-Dibromoethane (EDB)ND ug/kg 1 07/12/11 17:39 106-93-45.1
Dibromomethane ND ug/kg 1 07/12/11 17:39 74-95-35.1
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 17:39 95-50-15.1
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 17:39 541-73-15.1
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 17:39 106-46-75.1
Dichlorodifluoromethane ND ug/kg 1 07/12/11 17:39 75-71-810.1
1,1-Dichloroethane ND ug/kg 1 07/12/11 17:39 75-34-35.1
1,2-Dichloroethane ND ug/kg 1 07/12/11 17:39 107-06-25.1
1,1-Dichloroethene ND ug/kg 1 07/12/11 17:39 75-35-45.1
cis-1,2-Dichloroethene ND ug/kg 1 07/12/11 17:39 156-59-25.1
trans-1,2-Dichloroethene ND ug/kg 1 07/12/11 17:39 156-60-55.1
1,2-Dichloropropane ND ug/kg 1 07/12/11 17:39 78-87-55.1
1,3-Dichloropropane ND ug/kg 1 07/12/11 17:39 142-28-95.1
2,2-Dichloropropane ND ug/kg 1 07/12/11 17:39 594-20-75.1
1,1-Dichloropropene ND ug/kg 1 07/12/11 17:39 563-58-65.1
cis-1,3-Dichloropropene ND ug/kg 1 07/12/11 17:39 10061-01-55.1
trans-1,3-Dichloropropene ND ug/kg 1 07/12/11 17:39 10061-02-65.1
Diisopropyl ether ND ug/kg 1 07/12/11 17:39 108-20-35.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 38 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 2B (8-9)Lab ID:9297694004 Collected:07/06/11 11:15 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/12/11 17:39 100-41-45.1
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 17:39 87-68-35.1
2-Hexanone ND ug/kg 1 07/12/11 17:39 591-78-650.6
Isopropylbenzene (Cumene)ND ug/kg 1 07/12/11 17:39 98-82-85.1
p-Isopropyltoluene ND ug/kg 1 07/12/11 17:39 99-87-65.1
Methylene Chloride ND ug/kg 1 07/12/11 17:39 75-09-220.3
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/12/11 17:39 108-10-150.6
Methyl-tert-butyl ether ND ug/kg 1 07/12/11 17:39 1634-04-45.1
Naphthalene ND ug/kg 1 07/12/11 17:39 91-20-35.1
n-Propylbenzene ND ug/kg 1 07/12/11 17:39 103-65-15.1
Styrene ND ug/kg 1 07/12/11 17:39 100-42-55.1
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/12/11 17:39 630-20-65.1
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/12/11 17:39 79-34-55.1
Tetrachloroethene ND ug/kg 1 07/12/11 17:39 127-18-45.1
Toluene ND ug/kg 1 07/12/11 17:39 108-88-35.1
1,2,3-Trichlorobenzene ND ug/kg 1 07/12/11 17:39 87-61-65.1
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 17:39 120-82-15.1
1,1,1-Trichloroethane ND ug/kg 1 07/12/11 17:39 71-55-65.1
1,1,2-Trichloroethane ND ug/kg 1 07/12/11 17:39 79-00-55.1
Trichloroethene ND ug/kg 1 07/12/11 17:39 79-01-65.1
Trichlorofluoromethane ND ug/kg 1 07/12/11 17:39 75-69-45.1
1,2,3-Trichloropropane ND ug/kg 1 07/12/11 17:39 96-18-45.1
1,2,4-Trimethylbenzene ND ug/kg 1 07/12/11 17:39 95-63-65.1
1,3,5-Trimethylbenzene ND ug/kg 1 07/12/11 17:39 108-67-85.1
Vinyl acetate ND ug/kg 1 07/12/11 17:39 108-05-450.6
Vinyl chloride ND ug/kg 1 07/12/11 17:39 75-01-410.1
Xylene (Total)ND ug/kg 1 07/12/11 17:39 1330-20-710.1
m&p-Xylene ND ug/kg 1 07/12/11 17:39 179601-23-110.1
o-Xylene ND ug/kg 1 07/12/11 17:39 95-47-65.1
Dibromofluoromethane (S)101 %1 07/12/11 17:39 1868-53-770-130
Toluene-d8 (S)104 %1 07/12/11 17:39 2037-26-570-130
4-Bromofluorobenzene (S)93 %1 07/12/11 17:39 460-00-470-130
1,2-Dichloroethane-d4 (S)85 %1 07/12/11 17:39 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 23.0 %1 07/08/11 08:530.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 39 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 3A (6-7)Lab ID:9297694005 Collected:07/06/11 11:45 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 64.2 mg/kg 1 07/12/11 02:33 68334-30-507/07/11 15:356.4
n-Pentacosane (S)78 %1 07/12/11 02:33 629-99-207/07/11 15:3541-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease ND mg/kg 1 07/11/11 12:0507/11/11 11:1689.0
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/12/11 16:09 8006-61-907/12/11 10:346.6
4-Bromofluorobenzene (S)151 %1 07/12/11 16:09 460-00-407/12/11 10:3470-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 6.5 mg/kg 1 07/13/11 15:23 7440-38-207/12/11 11:400.59
Barium 96.0 mg/kg 1 07/13/11 15:23 7440-39-307/12/11 11:400.59
Cadmium 0.72 mg/kg 1 07/13/11 15:23 7440-43-907/12/11 11:400.12
Chromium 12.4 mg/kg 1 07/13/11 15:23 7440-47-307/12/11 11:400.59
Lead 85.8 mg/kg 1 07/13/11 15:23 7439-92-107/12/11 11:400.59
Selenium 1.9 mg/kg 1 07/13/11 15:23 7782-49-207/12/11 11:401.2
Silver ND mg/kg 1 07/13/11 15:23 7440-22-407/12/11 11:400.59
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.028 mg/kg 1 07/11/11 17:49 7439-97-607/08/11 15:100.0060
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/14/11 17:45 83-32-907/07/11 13:30422
Acenaphthylene ND ug/kg 1 07/14/11 17:45 208-96-807/07/11 13:30422
Aniline ND ug/kg 1 07/14/11 17:45 62-53-307/07/11 13:30422
Anthracene ND ug/kg 1 07/14/11 17:45 120-12-707/07/11 13:30422
Benzo(a)anthracene ND ug/kg 1 07/14/11 17:45 56-55-307/07/11 13:30422
Benzo(a)pyrene ND ug/kg 1 07/14/11 17:45 50-32-807/07/11 13:30422
Benzo(b)fluoranthene ND ug/kg 1 07/14/11 17:45 205-99-207/07/11 13:30422
Benzo(g,h,i)perylene ND ug/kg 1 07/14/11 17:45 191-24-207/07/11 13:30422
Benzo(k)fluoranthene ND ug/kg 1 07/14/11 17:45 207-08-907/07/11 13:30422
Benzoic Acid ND ug/kg 1 07/14/11 17:45 65-85-007/07/11 13:302110
Benzyl alcohol ND ug/kg 1 07/14/11 17:45 100-51-607/07/11 13:30845
4-Bromophenylphenyl ether ND ug/kg 1 07/14/11 17:45 101-55-307/07/11 13:30422
Butylbenzylphthalate ND ug/kg 1 07/14/11 17:45 85-68-707/07/11 13:30422
4-Chloro-3-methylphenol ND ug/kg 1 07/14/11 17:45 59-50-707/07/11 13:30845
4-Chloroaniline ND ug/kg 1 07/14/11 17:45 106-47-807/07/11 13:302110
bis(2-Chloroethoxy)methane ND ug/kg 1 07/14/11 17:45 111-91-107/07/11 13:30422
bis(2-Chloroethyl) ether ND ug/kg 1 07/14/11 17:45 111-44-407/07/11 13:30422
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/14/11 17:45 108-60-107/07/11 13:30422
2-Chloronaphthalene ND ug/kg 1 07/14/11 17:45 91-58-707/07/11 13:30422
2-Chlorophenol ND ug/kg 1 07/14/11 17:45 95-57-807/07/11 13:30422
4-Chlorophenylphenyl ether ND ug/kg 1 07/14/11 17:45 7005-72-307/07/11 13:30422
Chrysene ND ug/kg 1 07/14/11 17:45 218-01-907/07/11 13:30422
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 40 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 3A (6-7)Lab ID:9297694005 Collected:07/06/11 11:45 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/14/11 17:45 53-70-307/07/11 13:30422
Dibenzofuran ND ug/kg 1 07/14/11 17:45 132-64-907/07/11 13:30422
1,2-Dichlorobenzene ND ug/kg 1 07/14/11 17:45 95-50-107/07/11 13:30422
1,3-Dichlorobenzene ND ug/kg 1 07/14/11 17:45 541-73-107/07/11 13:30422
1,4-Dichlorobenzene ND ug/kg 1 07/14/11 17:45 106-46-707/07/11 13:30422
3,3'-Dichlorobenzidine ND ug/kg 1 07/14/11 17:45 91-94-107/07/11 13:302110
2,4-Dichlorophenol ND ug/kg 1 07/14/11 17:45 120-83-207/07/11 13:30422
Diethylphthalate ND ug/kg 1 07/14/11 17:45 84-66-207/07/11 13:30422
2,4-Dimethylphenol ND ug/kg 1 07/14/11 17:45 105-67-907/07/11 13:30422
Dimethylphthalate ND ug/kg 1 07/14/11 17:45 131-11-307/07/11 13:30422
Di-n-butylphthalate ND ug/kg 1 07/14/11 17:45 84-74-207/07/11 13:30422
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/14/11 17:45 534-52-107/07/11 13:30845
2,4-Dinitrophenol ND ug/kg 1 07/14/11 17:45 51-28-507/07/11 13:302110
2,4-Dinitrotoluene ND ug/kg 1 07/14/11 17:45 121-14-207/07/11 13:30422
2,6-Dinitrotoluene ND ug/kg 1 07/14/11 17:45 606-20-207/07/11 13:30422
Di-n-octylphthalate ND ug/kg 1 07/14/11 17:45 117-84-007/07/11 13:30422
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/14/11 17:45 117-81-707/07/11 13:30422
Fluoranthene ND ug/kg 1 07/14/11 17:45 206-44-007/07/11 13:30422
Fluorene ND ug/kg 1 07/14/11 17:45 86-73-707/07/11 13:30422
Hexachloro-1,3-butadiene ND ug/kg 1 07/14/11 17:45 87-68-307/07/11 13:30422
Hexachlorobenzene ND ug/kg 1 07/14/11 17:45 118-74-107/07/11 13:30422
Hexachlorocyclopentadiene ND ug/kg 1 07/14/11 17:45 77-47-407/07/11 13:30422
Hexachloroethane ND ug/kg 1 07/14/11 17:45 67-72-107/07/11 13:30422
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/14/11 17:45 193-39-507/07/11 13:30422
Isophorone ND ug/kg 1 07/14/11 17:45 78-59-107/07/11 13:30422
1-Methylnaphthalene ND ug/kg 1 07/14/11 17:45 90-12-007/07/11 13:30422
2-Methylnaphthalene ND ug/kg 1 07/14/11 17:45 91-57-607/07/11 13:30422
2-Methylphenol(o-Cresol)ND ug/kg 1 07/14/11 17:45 95-48-707/07/11 13:30422
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/14/11 17:4507/07/11 13:30422
Naphthalene ND ug/kg 1 07/14/11 17:45 91-20-307/07/11 13:30422
2-Nitroaniline ND ug/kg 1 07/14/11 17:45 88-74-407/07/11 13:302110
3-Nitroaniline ND ug/kg 1 07/14/11 17:45 99-09-207/07/11 13:302110
4-Nitroaniline ND ug/kg 1 07/14/11 17:45 100-01-607/07/11 13:30845
Nitrobenzene ND ug/kg 1 07/14/11 17:45 98-95-307/07/11 13:30422
2-Nitrophenol ND ug/kg 1 07/14/11 17:45 88-75-507/07/11 13:30422
4-Nitrophenol ND ug/kg 1 07/14/11 17:45 100-02-707/07/11 13:302110
N-Nitrosodimethylamine ND ug/kg 1 07/14/11 17:45 62-75-907/07/11 13:30422
N-Nitroso-di-n-propylamine ND ug/kg 1 07/14/11 17:45 621-64-707/07/11 13:30422
N-Nitrosodiphenylamine ND ug/kg 1 07/14/11 17:45 86-30-607/07/11 13:30422
Pentachlorophenol ND ug/kg 1 07/14/11 17:45 87-86-507/07/11 13:302110
Phenanthrene ND ug/kg 1 07/14/11 17:45 85-01-807/07/11 13:30422
Phenol ND ug/kg 1 07/14/11 17:45 108-95-207/07/11 13:30422
Pyrene ND ug/kg 1 07/14/11 17:45 129-00-007/07/11 13:30422
1,2,4-Trichlorobenzene ND ug/kg 1 07/14/11 17:45 120-82-107/07/11 13:30422
2,4,5-Trichlorophenol ND ug/kg 1 07/14/11 17:45 95-95-407/07/11 13:30422
2,4,6-Trichlorophenol ND ug/kg 1 07/14/11 17:45 88-06-207/07/11 13:30422
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 41 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 3A (6-7)Lab ID:9297694005 Collected:07/06/11 11:45 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)69 %1 07/14/11 17:45 4165-60-007/07/11 13:3023-110
2-Fluorobiphenyl (S)73 %1 07/14/11 17:45 321-60-807/07/11 13:3030-110
Terphenyl-d14 (S)71 %1 07/14/11 17:45 1718-51-007/07/11 13:3028-110
Phenol-d6 (S)57 %1 07/14/11 17:45 13127-88-307/07/11 13:3022-110
2-Fluorophenol (S)55 %1 07/14/11 17:45 367-12-407/07/11 13:3013-110
2,4,6-Tribromophenol (S)81 %1 07/14/11 17:45 118-79-607/07/11 13:3027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/12/11 17:59 67-64-197.7
Benzene ND ug/kg 1 07/12/11 17:59 71-43-24.9
Bromobenzene ND ug/kg 1 07/12/11 17:59 108-86-14.9
Bromochloromethane ND ug/kg 1 07/12/11 17:59 74-97-54.9
Bromodichloromethane ND ug/kg 1 07/12/11 17:59 75-27-44.9
Bromoform ND ug/kg 1 07/12/11 17:59 75-25-24.9
Bromomethane ND ug/kg 1 07/12/11 17:59 74-83-99.8
2-Butanone (MEK)ND ug/kg 1 07/12/11 17:59 78-93-397.7
n-Butylbenzene ND ug/kg 1 07/12/11 17:59 104-51-84.9
sec-Butylbenzene ND ug/kg 1 07/12/11 17:59 135-98-84.9
tert-Butylbenzene ND ug/kg 1 07/12/11 17:59 98-06-64.9
Carbon tetrachloride ND ug/kg 1 07/12/11 17:59 56-23-54.9
Chlorobenzene ND ug/kg 1 07/12/11 17:59 108-90-74.9
Chloroethane ND ug/kg 1 07/12/11 17:59 75-00-39.8
Chloroform ND ug/kg 1 07/12/11 17:59 67-66-34.9
Chloromethane ND ug/kg 1 07/12/11 17:59 74-87-39.8
2-Chlorotoluene ND ug/kg 1 07/12/11 17:59 95-49-84.9
4-Chlorotoluene ND ug/kg 1 07/12/11 17:59 106-43-44.9
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/12/11 17:59 96-12-84.9
Dibromochloromethane ND ug/kg 1 07/12/11 17:59 124-48-14.9
1,2-Dibromoethane (EDB)ND ug/kg 1 07/12/11 17:59 106-93-44.9
Dibromomethane ND ug/kg 1 07/12/11 17:59 74-95-34.9
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 17:59 95-50-14.9
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 17:59 541-73-14.9
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 17:59 106-46-74.9
Dichlorodifluoromethane ND ug/kg 1 07/12/11 17:59 75-71-89.8
1,1-Dichloroethane ND ug/kg 1 07/12/11 17:59 75-34-34.9
1,2-Dichloroethane ND ug/kg 1 07/12/11 17:59 107-06-24.9
1,1-Dichloroethene ND ug/kg 1 07/12/11 17:59 75-35-44.9
cis-1,2-Dichloroethene ND ug/kg 1 07/12/11 17:59 156-59-24.9
trans-1,2-Dichloroethene ND ug/kg 1 07/12/11 17:59 156-60-54.9
1,2-Dichloropropane ND ug/kg 1 07/12/11 17:59 78-87-54.9
1,3-Dichloropropane ND ug/kg 1 07/12/11 17:59 142-28-94.9
2,2-Dichloropropane ND ug/kg 1 07/12/11 17:59 594-20-74.9
1,1-Dichloropropene ND ug/kg 1 07/12/11 17:59 563-58-64.9
cis-1,3-Dichloropropene ND ug/kg 1 07/12/11 17:59 10061-01-54.9
trans-1,3-Dichloropropene ND ug/kg 1 07/12/11 17:59 10061-02-64.9
Diisopropyl ether ND ug/kg 1 07/12/11 17:59 108-20-34.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 42 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 3A (6-7)Lab ID:9297694005 Collected:07/06/11 11:45 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/12/11 17:59 100-41-44.9
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 17:59 87-68-34.9
2-Hexanone ND ug/kg 1 07/12/11 17:59 591-78-648.8
Isopropylbenzene (Cumene)ND ug/kg 1 07/12/11 17:59 98-82-84.9
p-Isopropyltoluene ND ug/kg 1 07/12/11 17:59 99-87-64.9
Methylene Chloride ND ug/kg 1 07/12/11 17:59 75-09-219.5
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/12/11 17:59 108-10-148.8
Methyl-tert-butyl ether ND ug/kg 1 07/12/11 17:59 1634-04-44.9
Naphthalene ND ug/kg 1 07/12/11 17:59 91-20-34.9
n-Propylbenzene ND ug/kg 1 07/12/11 17:59 103-65-14.9
Styrene ND ug/kg 1 07/12/11 17:59 100-42-54.9
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/12/11 17:59 630-20-64.9
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/12/11 17:59 79-34-54.9
Tetrachloroethene ND ug/kg 1 07/12/11 17:59 127-18-44.9
Toluene ND ug/kg 1 07/12/11 17:59 108-88-34.9
1,2,3-Trichlorobenzene ND ug/kg 1 07/12/11 17:59 87-61-64.9
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 17:59 120-82-14.9
1,1,1-Trichloroethane ND ug/kg 1 07/12/11 17:59 71-55-64.9
1,1,2-Trichloroethane ND ug/kg 1 07/12/11 17:59 79-00-54.9
Trichloroethene ND ug/kg 1 07/12/11 17:59 79-01-64.9
Trichlorofluoromethane ND ug/kg 1 07/12/11 17:59 75-69-44.9
1,2,3-Trichloropropane ND ug/kg 1 07/12/11 17:59 96-18-44.9
1,2,4-Trimethylbenzene ND ug/kg 1 07/12/11 17:59 95-63-64.9
1,3,5-Trimethylbenzene ND ug/kg 1 07/12/11 17:59 108-67-84.9
Vinyl acetate ND ug/kg 1 07/12/11 17:59 108-05-448.8
Vinyl chloride ND ug/kg 1 07/12/11 17:59 75-01-49.8
Xylene (Total)ND ug/kg 1 07/12/11 17:59 1330-20-79.8
m&p-Xylene ND ug/kg 1 07/12/11 17:59 179601-23-19.8
o-Xylene ND ug/kg 1 07/12/11 17:59 95-47-64.9
Dibromofluoromethane (S)104 %1 07/12/11 17:59 1868-53-770-130
Toluene-d8 (S)101 %1 07/12/11 17:59 2037-26-570-130
4-Bromofluorobenzene (S)91 %1 07/12/11 17:59 460-00-470-130
1,2-Dichloroethane-d4 (S)92 %1 07/12/11 17:59 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 21.4 %1 07/08/11 08:530.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 43 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 3B (8-9)Lab ID:9297694006 Collected:07/06/11 12:00 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 18.7 mg/kg 1 07/12/11 02:33 68334-30-507/07/11 15:356.2
n-Pentacosane (S)65 %1 07/12/11 02:33 629-99-207/07/11 15:3541-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease ND mg/kg 1 07/11/11 12:0507/11/11 11:1786.3
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/12/11 16:34 8006-61-907/12/11 10:345.7
4-Bromofluorobenzene (S)146 %1 07/12/11 16:34 460-00-407/12/11 10:3470-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 2.8 mg/kg 1 07/13/11 15:31 7440-38-207/12/11 11:400.48
Barium 71.1 mg/kg 1 07/13/11 15:31 7440-39-307/12/11 11:400.48
Cadmium ND mg/kg 1 07/13/11 15:31 7440-43-907/12/11 11:400.096
Chromium 6.0 mg/kg 1 07/13/11 15:31 7440-47-307/12/11 11:400.48
Lead 14.5 mg/kg 1 07/13/11 15:31 7439-92-107/12/11 11:400.48
Selenium 1.2 mg/kg 1 07/13/11 15:31 7782-49-207/12/11 11:400.96
Silver ND mg/kg 1 07/13/11 15:31 7440-22-407/12/11 11:400.48
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.011 mg/kg 1 07/11/11 17:51 7439-97-607/08/11 15:100.0040
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/14/11 18:13 83-32-907/07/11 13:30408
Acenaphthylene ND ug/kg 1 07/14/11 18:13 208-96-807/07/11 13:30408
Aniline ND ug/kg 1 07/14/11 18:13 62-53-307/07/11 13:30408
Anthracene ND ug/kg 1 07/14/11 18:13 120-12-707/07/11 13:30408
Benzo(a)anthracene ND ug/kg 1 07/14/11 18:13 56-55-307/07/11 13:30408
Benzo(a)pyrene ND ug/kg 1 07/14/11 18:13 50-32-807/07/11 13:30408
Benzo(b)fluoranthene ND ug/kg 1 07/14/11 18:13 205-99-207/07/11 13:30408
Benzo(g,h,i)perylene ND ug/kg 1 07/14/11 18:13 191-24-207/07/11 13:30408
Benzo(k)fluoranthene ND ug/kg 1 07/14/11 18:13 207-08-907/07/11 13:30408
Benzoic Acid ND ug/kg 1 07/14/11 18:13 65-85-007/07/11 13:302040
Benzyl alcohol ND ug/kg 1 07/14/11 18:13 100-51-607/07/11 13:30816
4-Bromophenylphenyl ether ND ug/kg 1 07/14/11 18:13 101-55-307/07/11 13:30408
Butylbenzylphthalate ND ug/kg 1 07/14/11 18:13 85-68-707/07/11 13:30408
4-Chloro-3-methylphenol ND ug/kg 1 07/14/11 18:13 59-50-707/07/11 13:30816
4-Chloroaniline ND ug/kg 1 07/14/11 18:13 106-47-807/07/11 13:302040
bis(2-Chloroethoxy)methane ND ug/kg 1 07/14/11 18:13 111-91-107/07/11 13:30408
bis(2-Chloroethyl) ether ND ug/kg 1 07/14/11 18:13 111-44-407/07/11 13:30408
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/14/11 18:13 108-60-107/07/11 13:30408
2-Chloronaphthalene ND ug/kg 1 07/14/11 18:13 91-58-707/07/11 13:30408
2-Chlorophenol ND ug/kg 1 07/14/11 18:13 95-57-807/07/11 13:30408
4-Chlorophenylphenyl ether ND ug/kg 1 07/14/11 18:13 7005-72-307/07/11 13:30408
Chrysene ND ug/kg 1 07/14/11 18:13 218-01-907/07/11 13:30408
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 44 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 3B (8-9)Lab ID:9297694006 Collected:07/06/11 12:00 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/14/11 18:13 53-70-307/07/11 13:30408
Dibenzofuran ND ug/kg 1 07/14/11 18:13 132-64-907/07/11 13:30408
1,2-Dichlorobenzene ND ug/kg 1 07/14/11 18:13 95-50-107/07/11 13:30408
1,3-Dichlorobenzene ND ug/kg 1 07/14/11 18:13 541-73-107/07/11 13:30408
1,4-Dichlorobenzene ND ug/kg 1 07/14/11 18:13 106-46-707/07/11 13:30408
3,3'-Dichlorobenzidine ND ug/kg 1 07/14/11 18:13 91-94-107/07/11 13:302040
2,4-Dichlorophenol ND ug/kg 1 07/14/11 18:13 120-83-207/07/11 13:30408
Diethylphthalate ND ug/kg 1 07/14/11 18:13 84-66-207/07/11 13:30408
2,4-Dimethylphenol ND ug/kg 1 07/14/11 18:13 105-67-907/07/11 13:30408
Dimethylphthalate ND ug/kg 1 07/14/11 18:13 131-11-307/07/11 13:30408
Di-n-butylphthalate ND ug/kg 1 07/14/11 18:13 84-74-207/07/11 13:30408
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/14/11 18:13 534-52-107/07/11 13:30816
2,4-Dinitrophenol ND ug/kg 1 07/14/11 18:13 51-28-507/07/11 13:302040
2,4-Dinitrotoluene ND ug/kg 1 07/14/11 18:13 121-14-207/07/11 13:30408
2,6-Dinitrotoluene ND ug/kg 1 07/14/11 18:13 606-20-207/07/11 13:30408
Di-n-octylphthalate ND ug/kg 1 07/14/11 18:13 117-84-007/07/11 13:30408
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/14/11 18:13 117-81-707/07/11 13:30408
Fluoranthene ND ug/kg 1 07/14/11 18:13 206-44-007/07/11 13:30408
Fluorene ND ug/kg 1 07/14/11 18:13 86-73-707/07/11 13:30408
Hexachloro-1,3-butadiene ND ug/kg 1 07/14/11 18:13 87-68-307/07/11 13:30408
Hexachlorobenzene ND ug/kg 1 07/14/11 18:13 118-74-107/07/11 13:30408
Hexachlorocyclopentadiene ND ug/kg 1 07/14/11 18:13 77-47-407/07/11 13:30408
Hexachloroethane ND ug/kg 1 07/14/11 18:13 67-72-107/07/11 13:30408
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/14/11 18:13 193-39-507/07/11 13:30408
Isophorone ND ug/kg 1 07/14/11 18:13 78-59-107/07/11 13:30408
1-Methylnaphthalene ND ug/kg 1 07/14/11 18:13 90-12-007/07/11 13:30408
2-Methylnaphthalene ND ug/kg 1 07/14/11 18:13 91-57-607/07/11 13:30408
2-Methylphenol(o-Cresol)ND ug/kg 1 07/14/11 18:13 95-48-707/07/11 13:30408
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/14/11 18:1307/07/11 13:30408
Naphthalene ND ug/kg 1 07/14/11 18:13 91-20-307/07/11 13:30408
2-Nitroaniline ND ug/kg 1 07/14/11 18:13 88-74-407/07/11 13:302040
3-Nitroaniline ND ug/kg 1 07/14/11 18:13 99-09-207/07/11 13:302040
4-Nitroaniline ND ug/kg 1 07/14/11 18:13 100-01-607/07/11 13:30816
Nitrobenzene ND ug/kg 1 07/14/11 18:13 98-95-307/07/11 13:30408
2-Nitrophenol ND ug/kg 1 07/14/11 18:13 88-75-507/07/11 13:30408
4-Nitrophenol ND ug/kg 1 07/14/11 18:13 100-02-707/07/11 13:302040
N-Nitrosodimethylamine ND ug/kg 1 07/14/11 18:13 62-75-907/07/11 13:30408
N-Nitroso-di-n-propylamine ND ug/kg 1 07/14/11 18:13 621-64-707/07/11 13:30408
N-Nitrosodiphenylamine ND ug/kg 1 07/14/11 18:13 86-30-607/07/11 13:30408
Pentachlorophenol ND ug/kg 1 07/14/11 18:13 87-86-507/07/11 13:302040
Phenanthrene ND ug/kg 1 07/14/11 18:13 85-01-807/07/11 13:30408
Phenol ND ug/kg 1 07/14/11 18:13 108-95-207/07/11 13:30408
Pyrene ND ug/kg 1 07/14/11 18:13 129-00-007/07/11 13:30408
1,2,4-Trichlorobenzene ND ug/kg 1 07/14/11 18:13 120-82-107/07/11 13:30408
2,4,5-Trichlorophenol ND ug/kg 1 07/14/11 18:13 95-95-407/07/11 13:30408
2,4,6-Trichlorophenol ND ug/kg 1 07/14/11 18:13 88-06-207/07/11 13:30408
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 45 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 3B (8-9)Lab ID:9297694006 Collected:07/06/11 12:00 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)72 %1 07/14/11 18:13 4165-60-007/07/11 13:3023-110
2-Fluorobiphenyl (S)66 %1 07/14/11 18:13 321-60-807/07/11 13:3030-110
Terphenyl-d14 (S)70 %1 07/14/11 18:13 1718-51-007/07/11 13:3028-110
Phenol-d6 (S)57 %1 07/14/11 18:13 13127-88-307/07/11 13:3022-110
2-Fluorophenol (S)59 %1 07/14/11 18:13 367-12-407/07/11 13:3013-110
2,4,6-Tribromophenol (S)76 %1 07/14/11 18:13 118-79-607/07/11 13:3027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 217 ug/kg 1 07/12/11 18:19 67-64-1 C992.6
Benzene ND ug/kg 1 07/12/11 18:19 71-43-24.6
Bromobenzene ND ug/kg 1 07/12/11 18:19 108-86-14.6
Bromochloromethane ND ug/kg 1 07/12/11 18:19 74-97-54.6
Bromodichloromethane ND ug/kg 1 07/12/11 18:19 75-27-44.6
Bromoform ND ug/kg 1 07/12/11 18:19 75-25-24.6
Bromomethane ND ug/kg 1 07/12/11 18:19 74-83-99.3
2-Butanone (MEK)ND ug/kg 1 07/12/11 18:19 78-93-392.6
n-Butylbenzene ND ug/kg 1 07/12/11 18:19 104-51-84.6
sec-Butylbenzene ND ug/kg 1 07/12/11 18:19 135-98-84.6
tert-Butylbenzene ND ug/kg 1 07/12/11 18:19 98-06-64.6
Carbon tetrachloride ND ug/kg 1 07/12/11 18:19 56-23-54.6
Chlorobenzene ND ug/kg 1 07/12/11 18:19 108-90-74.6
Chloroethane ND ug/kg 1 07/12/11 18:19 75-00-39.3
Chloroform ND ug/kg 1 07/12/11 18:19 67-66-34.6
Chloromethane ND ug/kg 1 07/12/11 18:19 74-87-39.3
2-Chlorotoluene ND ug/kg 1 07/12/11 18:19 95-49-84.6
4-Chlorotoluene ND ug/kg 1 07/12/11 18:19 106-43-44.6
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/12/11 18:19 96-12-84.6
Dibromochloromethane ND ug/kg 1 07/12/11 18:19 124-48-14.6
1,2-Dibromoethane (EDB)ND ug/kg 1 07/12/11 18:19 106-93-44.6
Dibromomethane ND ug/kg 1 07/12/11 18:19 74-95-34.6
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 18:19 95-50-14.6
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 18:19 541-73-14.6
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 18:19 106-46-74.6
Dichlorodifluoromethane ND ug/kg 1 07/12/11 18:19 75-71-89.3
1,1-Dichloroethane ND ug/kg 1 07/12/11 18:19 75-34-34.6
1,2-Dichloroethane ND ug/kg 1 07/12/11 18:19 107-06-24.6
1,1-Dichloroethene ND ug/kg 1 07/12/11 18:19 75-35-44.6
cis-1,2-Dichloroethene ND ug/kg 1 07/12/11 18:19 156-59-24.6
trans-1,2-Dichloroethene ND ug/kg 1 07/12/11 18:19 156-60-54.6
1,2-Dichloropropane ND ug/kg 1 07/12/11 18:19 78-87-54.6
1,3-Dichloropropane ND ug/kg 1 07/12/11 18:19 142-28-94.6
2,2-Dichloropropane ND ug/kg 1 07/12/11 18:19 594-20-74.6
1,1-Dichloropropene ND ug/kg 1 07/12/11 18:19 563-58-64.6
cis-1,3-Dichloropropene ND ug/kg 1 07/12/11 18:19 10061-01-54.6
trans-1,3-Dichloropropene ND ug/kg 1 07/12/11 18:19 10061-02-64.6
Diisopropyl ether ND ug/kg 1 07/12/11 18:19 108-20-34.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 46 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 3B (8-9)Lab ID:9297694006 Collected:07/06/11 12:00 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/12/11 18:19 100-41-44.6
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 18:19 87-68-34.6
2-Hexanone ND ug/kg 1 07/12/11 18:19 591-78-646.3
Isopropylbenzene (Cumene)ND ug/kg 1 07/12/11 18:19 98-82-84.6
p-Isopropyltoluene ND ug/kg 1 07/12/11 18:19 99-87-64.6
Methylene Chloride ND ug/kg 1 07/12/11 18:19 75-09-218.5
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/12/11 18:19 108-10-146.3
Methyl-tert-butyl ether ND ug/kg 1 07/12/11 18:19 1634-04-44.6
Naphthalene ND ug/kg 1 07/12/11 18:19 91-20-34.6
n-Propylbenzene ND ug/kg 1 07/12/11 18:19 103-65-14.6
Styrene ND ug/kg 1 07/12/11 18:19 100-42-54.6
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/12/11 18:19 630-20-64.6
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/12/11 18:19 79-34-54.6
Tetrachloroethene ND ug/kg 1 07/12/11 18:19 127-18-44.6
Toluene ND ug/kg 1 07/12/11 18:19 108-88-34.6
1,2,3-Trichlorobenzene ND ug/kg 1 07/12/11 18:19 87-61-64.6
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 18:19 120-82-14.6
1,1,1-Trichloroethane ND ug/kg 1 07/12/11 18:19 71-55-64.6
1,1,2-Trichloroethane ND ug/kg 1 07/12/11 18:19 79-00-54.6
Trichloroethene ND ug/kg 1 07/12/11 18:19 79-01-64.6
Trichlorofluoromethane ND ug/kg 1 07/12/11 18:19 75-69-44.6
1,2,3-Trichloropropane ND ug/kg 1 07/12/11 18:19 96-18-44.6
1,2,4-Trimethylbenzene ND ug/kg 1 07/12/11 18:19 95-63-64.6
1,3,5-Trimethylbenzene ND ug/kg 1 07/12/11 18:19 108-67-84.6
Vinyl acetate ND ug/kg 1 07/12/11 18:19 108-05-446.3
Vinyl chloride ND ug/kg 1 07/12/11 18:19 75-01-49.3
Xylene (Total)ND ug/kg 1 07/12/11 18:19 1330-20-79.3
m&p-Xylene ND ug/kg 1 07/12/11 18:19 179601-23-19.3
o-Xylene ND ug/kg 1 07/12/11 18:19 95-47-64.6
Dibromofluoromethane (S)105 %1 07/12/11 18:19 1868-53-770-130
Toluene-d8 (S)99 %1 07/12/11 18:19 2037-26-570-130
4-Bromofluorobenzene (S)91 %1 07/12/11 18:19 460-00-470-130
1,2-Dichloroethane-d4 (S)90 %1 07/12/11 18:19 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 18.8 %1 07/08/11 08:530.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 47 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 4A (6-7)Lab ID:9297694007 Collected:07/06/11 13:10 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 21.4 mg/kg 1 07/12/11 03:01 68334-30-507/07/11 15:355.9
n-Pentacosane (S)49 %1 07/12/11 03:01 629-99-207/07/11 15:3541-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease 868 mg/kg 1 07/11/11 12:0507/11/11 11:1782.1
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/12/11 16:59 8006-61-907/12/11 10:345.8
4-Bromofluorobenzene (S)138 %1 07/12/11 16:59 460-00-407/12/11 10:3470-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 3.2 mg/kg 1 07/13/11 15:34 7440-38-207/12/11 11:400.51
Barium 61.1 mg/kg 1 07/13/11 15:34 7440-39-307/12/11 11:400.51
Cadmium ND mg/kg 1 07/13/11 15:34 7440-43-907/12/11 11:400.10
Chromium 7.7 mg/kg 1 07/13/11 15:34 7440-47-307/12/11 11:400.51
Lead 30.6 mg/kg 1 07/13/11 15:34 7439-92-107/12/11 11:400.51
Selenium 1.4 mg/kg 1 07/13/11 15:34 7782-49-207/12/11 11:401.0
Silver ND mg/kg 1 07/13/11 15:34 7440-22-407/12/11 11:400.51
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.027 mg/kg 1 07/11/11 17:54 7439-97-607/08/11 15:100.0050
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 10 07/15/11 14:16 83-32-907/07/11 13:3019300
Acenaphthylene ND ug/kg 10 07/15/11 14:16 208-96-807/07/11 13:3019300
Aniline ND ug/kg 10 07/15/11 14:16 62-53-307/07/11 13:3019300
Anthracene ND ug/kg 10 07/15/11 14:16 120-12-707/07/11 13:3019300
Benzo(a)anthracene ND ug/kg 10 07/15/11 14:16 56-55-307/07/11 13:3019300
Benzo(a)pyrene ND ug/kg 10 07/15/11 14:16 50-32-807/07/11 13:3019300
Benzo(b)fluoranthene ND ug/kg 10 07/15/11 14:16 205-99-207/07/11 13:3019300
Benzo(g,h,i)perylene ND ug/kg 10 07/15/11 14:16 191-24-207/07/11 13:3019300
Benzo(k)fluoranthene ND ug/kg 10 07/15/11 14:16 207-08-907/07/11 13:3019300
Benzoic Acid ND ug/kg 10 07/15/11 14:16 65-85-007/07/11 13:3096700
Benzyl alcohol ND ug/kg 10 07/15/11 14:16 100-51-607/07/11 13:3038700
4-Bromophenylphenyl ether ND ug/kg 10 07/15/11 14:16 101-55-307/07/11 13:3019300
Butylbenzylphthalate ND ug/kg 10 07/15/11 14:16 85-68-707/07/11 13:3019300
4-Chloro-3-methylphenol ND ug/kg 10 07/15/11 14:16 59-50-707/07/11 13:3038700
4-Chloroaniline ND ug/kg 10 07/15/11 14:16 106-47-807/07/11 13:3096700
bis(2-Chloroethoxy)methane ND ug/kg 10 07/15/11 14:16 111-91-107/07/11 13:3019300
bis(2-Chloroethyl) ether ND ug/kg 10 07/15/11 14:16 111-44-407/07/11 13:3019300
bis(2-Chloroisopropyl) ether ND ug/kg 10 07/15/11 14:16 108-60-107/07/11 13:3019300
2-Chloronaphthalene ND ug/kg 10 07/15/11 14:16 91-58-707/07/11 13:3019300
2-Chlorophenol ND ug/kg 10 07/15/11 14:16 95-57-807/07/11 13:3019300
4-Chlorophenylphenyl ether ND ug/kg 10 07/15/11 14:16 7005-72-307/07/11 13:3019300
Chrysene ND ug/kg 10 07/15/11 14:16 218-01-907/07/11 13:3019300
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 48 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 4A (6-7)Lab ID:9297694007 Collected:07/06/11 13:10 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 10 07/15/11 14:16 53-70-307/07/11 13:3019300
Dibenzofuran ND ug/kg 10 07/15/11 14:16 132-64-907/07/11 13:3019300
1,2-Dichlorobenzene ND ug/kg 10 07/15/11 14:16 95-50-107/07/11 13:3019300
1,3-Dichlorobenzene ND ug/kg 10 07/15/11 14:16 541-73-107/07/11 13:3019300
1,4-Dichlorobenzene ND ug/kg 10 07/15/11 14:16 106-46-707/07/11 13:3019300
3,3'-Dichlorobenzidine ND ug/kg 10 07/15/11 14:16 91-94-107/07/11 13:3096700
2,4-Dichlorophenol ND ug/kg 10 07/15/11 14:16 120-83-207/07/11 13:3019300
Diethylphthalate ND ug/kg 10 07/15/11 14:16 84-66-207/07/11 13:3019300
2,4-Dimethylphenol ND ug/kg 10 07/15/11 14:16 105-67-907/07/11 13:3019300
Dimethylphthalate ND ug/kg 10 07/15/11 14:16 131-11-307/07/11 13:3019300
Di-n-butylphthalate ND ug/kg 10 07/15/11 14:16 84-74-207/07/11 13:3019300
4,6-Dinitro-2-methylphenol ND ug/kg 10 07/15/11 14:16 534-52-107/07/11 13:3038700
2,4-Dinitrophenol ND ug/kg 10 07/15/11 14:16 51-28-507/07/11 13:3096700
2,4-Dinitrotoluene ND ug/kg 10 07/15/11 14:16 121-14-207/07/11 13:3019300
2,6-Dinitrotoluene ND ug/kg 10 07/15/11 14:16 606-20-207/07/11 13:3019300
Di-n-octylphthalate ND ug/kg 10 07/15/11 14:16 117-84-007/07/11 13:3019300
bis(2-Ethylhexyl)phthalate ND ug/kg 10 07/15/11 14:16 117-81-707/07/11 13:3019300
Fluoranthene ND ug/kg 10 07/15/11 14:16 206-44-007/07/11 13:3019300
Fluorene ND ug/kg 10 07/15/11 14:16 86-73-707/07/11 13:3019300
Hexachloro-1,3-butadiene ND ug/kg 10 07/15/11 14:16 87-68-307/07/11 13:3019300
Hexachlorobenzene ND ug/kg 10 07/15/11 14:16 118-74-107/07/11 13:3019300
Hexachlorocyclopentadiene ND ug/kg 10 07/15/11 14:16 77-47-407/07/11 13:3019300
Hexachloroethane ND ug/kg 10 07/15/11 14:16 67-72-107/07/11 13:3019300
Indeno(1,2,3-cd)pyrene ND ug/kg 10 07/15/11 14:16 193-39-507/07/11 13:3019300
Isophorone ND ug/kg 10 07/15/11 14:16 78-59-107/07/11 13:3019300
1-Methylnaphthalene ND ug/kg 10 07/15/11 14:16 90-12-007/07/11 13:3019300
2-Methylnaphthalene ND ug/kg 10 07/15/11 14:16 91-57-607/07/11 13:3019300
2-Methylphenol(o-Cresol)ND ug/kg 10 07/15/11 14:16 95-48-707/07/11 13:3019300
3&4-Methylphenol(m&p Cresol)ND ug/kg 10 07/15/11 14:1607/07/11 13:3019300
Naphthalene ND ug/kg 10 07/15/11 14:16 91-20-307/07/11 13:3019300
2-Nitroaniline ND ug/kg 10 07/15/11 14:16 88-74-407/07/11 13:3096700
3-Nitroaniline ND ug/kg 10 07/15/11 14:16 99-09-207/07/11 13:3096700
4-Nitroaniline ND ug/kg 10 07/15/11 14:16 100-01-607/07/11 13:3038700
Nitrobenzene ND ug/kg 10 07/15/11 14:16 98-95-307/07/11 13:3019300
2-Nitrophenol ND ug/kg 10 07/15/11 14:16 88-75-507/07/11 13:3019300
4-Nitrophenol ND ug/kg 10 07/15/11 14:16 100-02-707/07/11 13:3096700
N-Nitrosodimethylamine ND ug/kg 10 07/15/11 14:16 62-75-907/07/11 13:3019300
N-Nitroso-di-n-propylamine ND ug/kg 10 07/15/11 14:16 621-64-707/07/11 13:3019300
N-Nitrosodiphenylamine ND ug/kg 10 07/15/11 14:16 86-30-607/07/11 13:3019300
Pentachlorophenol ND ug/kg 10 07/15/11 14:16 87-86-507/07/11 13:3096700
Phenanthrene ND ug/kg 10 07/15/11 14:16 85-01-807/07/11 13:3019300
Phenol ND ug/kg 10 07/15/11 14:16 108-95-2 D3,P307/07/11 13:3019300
Pyrene ND ug/kg 10 07/15/11 14:16 129-00-007/07/11 13:3019300
1,2,4-Trichlorobenzene ND ug/kg 10 07/15/11 14:16 120-82-107/07/11 13:3019300
2,4,5-Trichlorophenol ND ug/kg 10 07/15/11 14:16 95-95-407/07/11 13:3019300
2,4,6-Trichlorophenol ND ug/kg 10 07/15/11 14:16 88-06-207/07/11 13:3019300
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 49 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 4A (6-7)Lab ID:9297694007 Collected:07/06/11 13:10 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)0 %10 07/15/11 14:16 4165-60-0 S407/07/11 13:3023-110
2-Fluorobiphenyl (S)0 %10 07/15/11 14:16 321-60-807/07/11 13:3030-110
Terphenyl-d14 (S)0 %10 07/15/11 14:16 1718-51-007/07/11 13:3028-110
Phenol-d6 (S)0 %10 07/15/11 14:16 13127-88-307/07/11 13:3022-110
2-Fluorophenol (S)0 %10 07/15/11 14:16 367-12-407/07/11 13:3013-110
2,4,6-Tribromophenol (S)0 %10 07/15/11 14:16 118-79-607/07/11 13:3027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 184 ug/kg 1 07/12/11 18:39 67-64-1 C989.9
Benzene ND ug/kg 1 07/12/11 18:39 71-43-24.5
Bromobenzene ND ug/kg 1 07/12/11 18:39 108-86-14.5
Bromochloromethane ND ug/kg 1 07/12/11 18:39 74-97-54.5
Bromodichloromethane ND ug/kg 1 07/12/11 18:39 75-27-44.5
Bromoform ND ug/kg 1 07/12/11 18:39 75-25-24.5
Bromomethane ND ug/kg 1 07/12/11 18:39 74-83-99.0
2-Butanone (MEK)ND ug/kg 1 07/12/11 18:39 78-93-389.9
n-Butylbenzene ND ug/kg 1 07/12/11 18:39 104-51-84.5
sec-Butylbenzene ND ug/kg 1 07/12/11 18:39 135-98-84.5
tert-Butylbenzene ND ug/kg 1 07/12/11 18:39 98-06-64.5
Carbon tetrachloride ND ug/kg 1 07/12/11 18:39 56-23-54.5
Chlorobenzene ND ug/kg 1 07/12/11 18:39 108-90-74.5
Chloroethane ND ug/kg 1 07/12/11 18:39 75-00-39.0
Chloroform ND ug/kg 1 07/12/11 18:39 67-66-34.5
Chloromethane ND ug/kg 1 07/12/11 18:39 74-87-39.0
2-Chlorotoluene ND ug/kg 1 07/12/11 18:39 95-49-84.5
4-Chlorotoluene ND ug/kg 1 07/12/11 18:39 106-43-44.5
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/12/11 18:39 96-12-84.5
Dibromochloromethane ND ug/kg 1 07/12/11 18:39 124-48-14.5
1,2-Dibromoethane (EDB)ND ug/kg 1 07/12/11 18:39 106-93-44.5
Dibromomethane ND ug/kg 1 07/12/11 18:39 74-95-34.5
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 18:39 95-50-14.5
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 18:39 541-73-14.5
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 18:39 106-46-74.5
Dichlorodifluoromethane ND ug/kg 1 07/12/11 18:39 75-71-89.0
1,1-Dichloroethane ND ug/kg 1 07/12/11 18:39 75-34-34.5
1,2-Dichloroethane ND ug/kg 1 07/12/11 18:39 107-06-24.5
1,1-Dichloroethene ND ug/kg 1 07/12/11 18:39 75-35-44.5
cis-1,2-Dichloroethene ND ug/kg 1 07/12/11 18:39 156-59-24.5
trans-1,2-Dichloroethene ND ug/kg 1 07/12/11 18:39 156-60-54.5
1,2-Dichloropropane ND ug/kg 1 07/12/11 18:39 78-87-54.5
1,3-Dichloropropane ND ug/kg 1 07/12/11 18:39 142-28-94.5
2,2-Dichloropropane ND ug/kg 1 07/12/11 18:39 594-20-74.5
1,1-Dichloropropene ND ug/kg 1 07/12/11 18:39 563-58-64.5
cis-1,3-Dichloropropene ND ug/kg 1 07/12/11 18:39 10061-01-54.5
trans-1,3-Dichloropropene ND ug/kg 1 07/12/11 18:39 10061-02-64.5
Diisopropyl ether ND ug/kg 1 07/12/11 18:39 108-20-34.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 50 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 4A (6-7)Lab ID:9297694007 Collected:07/06/11 13:10 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/12/11 18:39 100-41-44.5
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 18:39 87-68-34.5
2-Hexanone ND ug/kg 1 07/12/11 18:39 591-78-645.0
Isopropylbenzene (Cumene)ND ug/kg 1 07/12/11 18:39 98-82-84.5
p-Isopropyltoluene ND ug/kg 1 07/12/11 18:39 99-87-64.5
Methylene Chloride ND ug/kg 1 07/12/11 18:39 75-09-218.0
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/12/11 18:39 108-10-145.0
Methyl-tert-butyl ether ND ug/kg 1 07/12/11 18:39 1634-04-44.5
Naphthalene ND ug/kg 1 07/12/11 18:39 91-20-34.5
n-Propylbenzene ND ug/kg 1 07/12/11 18:39 103-65-14.5
Styrene ND ug/kg 1 07/12/11 18:39 100-42-54.5
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/12/11 18:39 630-20-64.5
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/12/11 18:39 79-34-54.5
Tetrachloroethene ND ug/kg 1 07/12/11 18:39 127-18-44.5
Toluene ND ug/kg 1 07/12/11 18:39 108-88-34.5
1,2,3-Trichlorobenzene ND ug/kg 1 07/12/11 18:39 87-61-64.5
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 18:39 120-82-14.5
1,1,1-Trichloroethane ND ug/kg 1 07/12/11 18:39 71-55-64.5
1,1,2-Trichloroethane ND ug/kg 1 07/12/11 18:39 79-00-54.5
Trichloroethene ND ug/kg 1 07/12/11 18:39 79-01-64.5
Trichlorofluoromethane ND ug/kg 1 07/12/11 18:39 75-69-44.5
1,2,3-Trichloropropane ND ug/kg 1 07/12/11 18:39 96-18-44.5
1,2,4-Trimethylbenzene ND ug/kg 1 07/12/11 18:39 95-63-64.5
1,3,5-Trimethylbenzene ND ug/kg 1 07/12/11 18:39 108-67-84.5
Vinyl acetate ND ug/kg 1 07/12/11 18:39 108-05-445.0
Vinyl chloride ND ug/kg 1 07/12/11 18:39 75-01-49.0
Xylene (Total)ND ug/kg 1 07/12/11 18:39 1330-20-79.0
m&p-Xylene ND ug/kg 1 07/12/11 18:39 179601-23-19.0
o-Xylene ND ug/kg 1 07/12/11 18:39 95-47-64.5
Dibromofluoromethane (S)102 %1 07/12/11 18:39 1868-53-770-130
Toluene-d8 (S)101 %1 07/12/11 18:39 2037-26-570-130
4-Bromofluorobenzene (S)90 %1 07/12/11 18:39 460-00-470-130
1,2-Dichloroethane-d4 (S)89 %1 07/12/11 18:39 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 14.7 %1 07/08/11 08:530.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 51 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 4B (9-10)Lab ID:9297694008 Collected:07/06/11 13:45 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 32.7 mg/kg 1 07/12/11 03:01 68334-30-5 P307/07/11 15:3531.0
n-Pentacosane (S)0 %1 07/12/11 03:01 629-99-2 S407/07/11 15:3541-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease ND mg/kg 1 07/11/11 12:0507/11/11 11:2086.8
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/12/11 17:24 8006-61-907/12/11 10:346.0
4-Bromofluorobenzene (S)148 %1 07/12/11 17:24 460-00-407/12/11 10:3470-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 1.8 mg/kg 1 07/13/11 15:37 7440-38-207/12/11 11:400.50
Barium 61.7 mg/kg 1 07/13/11 15:37 7440-39-307/12/11 11:400.50
Cadmium 0.26 mg/kg 1 07/13/11 15:37 7440-43-907/12/11 11:400.10
Chromium 24.3 mg/kg 1 07/13/11 15:37 7440-47-307/12/11 11:400.50
Lead 14.1 mg/kg 1 07/13/11 15:37 7439-92-107/12/11 11:400.50
Selenium 2.5 mg/kg 1 07/13/11 15:37 7782-49-207/12/11 11:401.0
Silver ND mg/kg 1 07/13/11 15:37 7440-22-407/12/11 11:400.50
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.022 mg/kg 1 07/11/11 17:56 7439-97-607/08/11 15:100.0053
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/14/11 18:41 83-32-907/07/11 13:30412
Acenaphthylene ND ug/kg 1 07/14/11 18:41 208-96-807/07/11 13:30412
Aniline ND ug/kg 1 07/14/11 18:41 62-53-307/07/11 13:30412
Anthracene ND ug/kg 1 07/14/11 18:41 120-12-707/07/11 13:30412
Benzo(a)anthracene ND ug/kg 1 07/14/11 18:41 56-55-307/07/11 13:30412
Benzo(a)pyrene ND ug/kg 1 07/14/11 18:41 50-32-807/07/11 13:30412
Benzo(b)fluoranthene ND ug/kg 1 07/14/11 18:41 205-99-207/07/11 13:30412
Benzo(g,h,i)perylene ND ug/kg 1 07/14/11 18:41 191-24-207/07/11 13:30412
Benzo(k)fluoranthene ND ug/kg 1 07/14/11 18:41 207-08-907/07/11 13:30412
Benzoic Acid ND ug/kg 1 07/14/11 18:41 65-85-007/07/11 13:302060
Benzyl alcohol ND ug/kg 1 07/14/11 18:41 100-51-607/07/11 13:30823
4-Bromophenylphenyl ether ND ug/kg 1 07/14/11 18:41 101-55-307/07/11 13:30412
Butylbenzylphthalate ND ug/kg 1 07/14/11 18:41 85-68-707/07/11 13:30412
4-Chloro-3-methylphenol ND ug/kg 1 07/14/11 18:41 59-50-707/07/11 13:30823
4-Chloroaniline ND ug/kg 1 07/14/11 18:41 106-47-807/07/11 13:302060
bis(2-Chloroethoxy)methane ND ug/kg 1 07/14/11 18:41 111-91-107/07/11 13:30412
bis(2-Chloroethyl) ether ND ug/kg 1 07/14/11 18:41 111-44-407/07/11 13:30412
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/14/11 18:41 108-60-107/07/11 13:30412
2-Chloronaphthalene ND ug/kg 1 07/14/11 18:41 91-58-707/07/11 13:30412
2-Chlorophenol ND ug/kg 1 07/14/11 18:41 95-57-807/07/11 13:30412
4-Chlorophenylphenyl ether ND ug/kg 1 07/14/11 18:41 7005-72-307/07/11 13:30412
Chrysene ND ug/kg 1 07/14/11 18:41 218-01-907/07/11 13:30412
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 52 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 4B (9-10)Lab ID:9297694008 Collected:07/06/11 13:45 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/14/11 18:41 53-70-307/07/11 13:30412
Dibenzofuran ND ug/kg 1 07/14/11 18:41 132-64-907/07/11 13:30412
1,2-Dichlorobenzene ND ug/kg 1 07/14/11 18:41 95-50-107/07/11 13:30412
1,3-Dichlorobenzene ND ug/kg 1 07/14/11 18:41 541-73-107/07/11 13:30412
1,4-Dichlorobenzene ND ug/kg 1 07/14/11 18:41 106-46-707/07/11 13:30412
3,3'-Dichlorobenzidine ND ug/kg 1 07/14/11 18:41 91-94-107/07/11 13:302060
2,4-Dichlorophenol ND ug/kg 1 07/14/11 18:41 120-83-207/07/11 13:30412
Diethylphthalate ND ug/kg 1 07/14/11 18:41 84-66-207/07/11 13:30412
2,4-Dimethylphenol ND ug/kg 1 07/14/11 18:41 105-67-907/07/11 13:30412
Dimethylphthalate ND ug/kg 1 07/14/11 18:41 131-11-307/07/11 13:30412
Di-n-butylphthalate ND ug/kg 1 07/14/11 18:41 84-74-207/07/11 13:30412
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/14/11 18:41 534-52-107/07/11 13:30823
2,4-Dinitrophenol ND ug/kg 1 07/14/11 18:41 51-28-507/07/11 13:302060
2,4-Dinitrotoluene ND ug/kg 1 07/14/11 18:41 121-14-207/07/11 13:30412
2,6-Dinitrotoluene ND ug/kg 1 07/14/11 18:41 606-20-207/07/11 13:30412
Di-n-octylphthalate ND ug/kg 1 07/14/11 18:41 117-84-007/07/11 13:30412
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/14/11 18:41 117-81-707/07/11 13:30412
Fluoranthene ND ug/kg 1 07/14/11 18:41 206-44-007/07/11 13:30412
Fluorene ND ug/kg 1 07/14/11 18:41 86-73-707/07/11 13:30412
Hexachloro-1,3-butadiene ND ug/kg 1 07/14/11 18:41 87-68-307/07/11 13:30412
Hexachlorobenzene ND ug/kg 1 07/14/11 18:41 118-74-107/07/11 13:30412
Hexachlorocyclopentadiene ND ug/kg 1 07/14/11 18:41 77-47-407/07/11 13:30412
Hexachloroethane ND ug/kg 1 07/14/11 18:41 67-72-107/07/11 13:30412
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/14/11 18:41 193-39-507/07/11 13:30412
Isophorone ND ug/kg 1 07/14/11 18:41 78-59-107/07/11 13:30412
1-Methylnaphthalene ND ug/kg 1 07/14/11 18:41 90-12-007/07/11 13:30412
2-Methylnaphthalene ND ug/kg 1 07/14/11 18:41 91-57-607/07/11 13:30412
2-Methylphenol(o-Cresol)ND ug/kg 1 07/14/11 18:41 95-48-707/07/11 13:30412
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/14/11 18:4107/07/11 13:30412
Naphthalene ND ug/kg 1 07/14/11 18:41 91-20-307/07/11 13:30412
2-Nitroaniline ND ug/kg 1 07/14/11 18:41 88-74-407/07/11 13:302060
3-Nitroaniline ND ug/kg 1 07/14/11 18:41 99-09-207/07/11 13:302060
4-Nitroaniline ND ug/kg 1 07/14/11 18:41 100-01-607/07/11 13:30823
Nitrobenzene ND ug/kg 1 07/14/11 18:41 98-95-307/07/11 13:30412
2-Nitrophenol ND ug/kg 1 07/14/11 18:41 88-75-507/07/11 13:30412
4-Nitrophenol ND ug/kg 1 07/14/11 18:41 100-02-707/07/11 13:302060
N-Nitrosodimethylamine ND ug/kg 1 07/14/11 18:41 62-75-907/07/11 13:30412
N-Nitroso-di-n-propylamine ND ug/kg 1 07/14/11 18:41 621-64-707/07/11 13:30412
N-Nitrosodiphenylamine ND ug/kg 1 07/14/11 18:41 86-30-607/07/11 13:30412
Pentachlorophenol ND ug/kg 1 07/14/11 18:41 87-86-507/07/11 13:302060
Phenanthrene ND ug/kg 1 07/14/11 18:41 85-01-807/07/11 13:30412
Phenol ND ug/kg 1 07/14/11 18:41 108-95-207/07/11 13:30412
Pyrene ND ug/kg 1 07/14/11 18:41 129-00-007/07/11 13:30412
1,2,4-Trichlorobenzene ND ug/kg 1 07/14/11 18:41 120-82-107/07/11 13:30412
2,4,5-Trichlorophenol ND ug/kg 1 07/14/11 18:41 95-95-407/07/11 13:30412
2,4,6-Trichlorophenol ND ug/kg 1 07/14/11 18:41 88-06-207/07/11 13:30412
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 53 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 4B (9-10)Lab ID:9297694008 Collected:07/06/11 13:45 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)26 %1 07/14/11 18:41 4165-60-007/07/11 13:3023-110
2-Fluorobiphenyl (S)54 %1 07/14/11 18:41 321-60-807/07/11 13:3030-110
Terphenyl-d14 (S)53 %1 07/14/11 18:41 1718-51-007/07/11 13:3028-110
Phenol-d6 (S)44 %1 07/14/11 18:41 13127-88-307/07/11 13:3022-110
2-Fluorophenol (S)48 %1 07/14/11 18:41 367-12-407/07/11 13:3013-110
2,4,6-Tribromophenol (S)62 %1 07/14/11 18:41 118-79-607/07/11 13:3027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 158 ug/kg 1 07/12/11 18:59 67-64-1 C996.2
Benzene ND ug/kg 1 07/12/11 18:59 71-43-24.8
Bromobenzene ND ug/kg 1 07/12/11 18:59 108-86-14.8
Bromochloromethane ND ug/kg 1 07/12/11 18:59 74-97-54.8
Bromodichloromethane ND ug/kg 1 07/12/11 18:59 75-27-44.8
Bromoform ND ug/kg 1 07/12/11 18:59 75-25-24.8
Bromomethane ND ug/kg 1 07/12/11 18:59 74-83-99.6
2-Butanone (MEK)ND ug/kg 1 07/12/11 18:59 78-93-396.2
n-Butylbenzene ND ug/kg 1 07/12/11 18:59 104-51-84.8
sec-Butylbenzene ND ug/kg 1 07/12/11 18:59 135-98-84.8
tert-Butylbenzene ND ug/kg 1 07/12/11 18:59 98-06-64.8
Carbon tetrachloride ND ug/kg 1 07/12/11 18:59 56-23-54.8
Chlorobenzene ND ug/kg 1 07/12/11 18:59 108-90-74.8
Chloroethane ND ug/kg 1 07/12/11 18:59 75-00-39.6
Chloroform ND ug/kg 1 07/12/11 18:59 67-66-34.8
Chloromethane ND ug/kg 1 07/12/11 18:59 74-87-39.6
2-Chlorotoluene ND ug/kg 1 07/12/11 18:59 95-49-84.8
4-Chlorotoluene ND ug/kg 1 07/12/11 18:59 106-43-44.8
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/12/11 18:59 96-12-84.8
Dibromochloromethane ND ug/kg 1 07/12/11 18:59 124-48-14.8
1,2-Dibromoethane (EDB)ND ug/kg 1 07/12/11 18:59 106-93-44.8
Dibromomethane ND ug/kg 1 07/12/11 18:59 74-95-34.8
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 18:59 95-50-14.8
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 18:59 541-73-14.8
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 18:59 106-46-74.8
Dichlorodifluoromethane ND ug/kg 1 07/12/11 18:59 75-71-89.6
1,1-Dichloroethane ND ug/kg 1 07/12/11 18:59 75-34-34.8
1,2-Dichloroethane ND ug/kg 1 07/12/11 18:59 107-06-24.8
1,1-Dichloroethene ND ug/kg 1 07/12/11 18:59 75-35-44.8
cis-1,2-Dichloroethene ND ug/kg 1 07/12/11 18:59 156-59-24.8
trans-1,2-Dichloroethene ND ug/kg 1 07/12/11 18:59 156-60-54.8
1,2-Dichloropropane ND ug/kg 1 07/12/11 18:59 78-87-54.8
1,3-Dichloropropane ND ug/kg 1 07/12/11 18:59 142-28-94.8
2,2-Dichloropropane ND ug/kg 1 07/12/11 18:59 594-20-74.8
1,1-Dichloropropene ND ug/kg 1 07/12/11 18:59 563-58-64.8
cis-1,3-Dichloropropene ND ug/kg 1 07/12/11 18:59 10061-01-54.8
trans-1,3-Dichloropropene ND ug/kg 1 07/12/11 18:59 10061-02-64.8
Diisopropyl ether ND ug/kg 1 07/12/11 18:59 108-20-34.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 54 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 4B (9-10)Lab ID:9297694008 Collected:07/06/11 13:45 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/12/11 18:59 100-41-44.8
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 18:59 87-68-34.8
2-Hexanone ND ug/kg 1 07/12/11 18:59 591-78-648.1
Isopropylbenzene (Cumene)ND ug/kg 1 07/12/11 18:59 98-82-84.8
p-Isopropyltoluene ND ug/kg 1 07/12/11 18:59 99-87-64.8
Methylene Chloride ND ug/kg 1 07/12/11 18:59 75-09-219.2
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/12/11 18:59 108-10-148.1
Methyl-tert-butyl ether ND ug/kg 1 07/12/11 18:59 1634-04-44.8
Naphthalene ND ug/kg 1 07/12/11 18:59 91-20-34.8
n-Propylbenzene ND ug/kg 1 07/12/11 18:59 103-65-14.8
Styrene ND ug/kg 1 07/12/11 18:59 100-42-54.8
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/12/11 18:59 630-20-64.8
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/12/11 18:59 79-34-54.8
Tetrachloroethene ND ug/kg 1 07/12/11 18:59 127-18-44.8
Toluene ND ug/kg 1 07/12/11 18:59 108-88-34.8
1,2,3-Trichlorobenzene ND ug/kg 1 07/12/11 18:59 87-61-64.8
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 18:59 120-82-14.8
1,1,1-Trichloroethane ND ug/kg 1 07/12/11 18:59 71-55-64.8
1,1,2-Trichloroethane ND ug/kg 1 07/12/11 18:59 79-00-54.8
Trichloroethene ND ug/kg 1 07/12/11 18:59 79-01-64.8
Trichlorofluoromethane ND ug/kg 1 07/12/11 18:59 75-69-44.8
1,2,3-Trichloropropane ND ug/kg 1 07/12/11 18:59 96-18-44.8
1,2,4-Trimethylbenzene ND ug/kg 1 07/12/11 18:59 95-63-64.8
1,3,5-Trimethylbenzene ND ug/kg 1 07/12/11 18:59 108-67-84.8
Vinyl acetate ND ug/kg 1 07/12/11 18:59 108-05-448.1
Vinyl chloride ND ug/kg 1 07/12/11 18:59 75-01-49.6
Xylene (Total)ND ug/kg 1 07/12/11 18:59 1330-20-79.6
m&p-Xylene ND ug/kg 1 07/12/11 18:59 179601-23-19.6
o-Xylene ND ug/kg 1 07/12/11 18:59 95-47-64.8
Dibromofluoromethane (S)108 %1 07/12/11 18:59 1868-53-770-130
Toluene-d8 (S)99 %1 07/12/11 18:59 2037-26-570-130
4-Bromofluorobenzene (S)89 %1 07/12/11 18:59 460-00-470-130
1,2-Dichloroethane-d4 (S)93 %1 07/12/11 18:59 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 19.3 %1 07/08/11 08:540.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 55 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 5A (6-7)Lab ID:9297694009 Collected:07/06/11 14:10 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components ND mg/kg 1 07/12/11 03:29 68334-30-507/07/11 15:356.1
n-Pentacosane (S)55 %1 07/12/11 03:29 629-99-207/07/11 15:3541-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease ND mg/kg 1 07/11/11 12:0507/11/11 11:2085.0
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/12/11 17:49 8006-61-907/12/11 10:346.3
4-Bromofluorobenzene (S)145 %1 07/12/11 17:49 460-00-407/12/11 10:3470-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 2.8 mg/kg 1 07/13/11 15:40 7440-38-207/12/11 11:400.48
Barium 107 mg/kg 1 07/13/11 15:40 7440-39-307/12/11 11:400.48
Cadmium ND mg/kg 1 07/13/11 15:40 7440-43-907/12/11 11:400.096
Chromium 4.1 mg/kg 1 07/13/11 15:40 7440-47-307/12/11 11:400.48
Lead 16.6 mg/kg 1 07/13/11 15:40 7439-92-107/12/11 11:400.48
Selenium 1.8 mg/kg 1 07/13/11 15:40 7782-49-207/12/11 11:400.96
Silver ND mg/kg 1 07/13/11 15:40 7440-22-407/12/11 11:400.48
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.015 mg/kg 1 07/11/11 17:59 7439-97-607/08/11 15:100.0046
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/15/11 13:20 83-32-907/07/11 13:30399
Acenaphthylene ND ug/kg 1 07/15/11 13:20 208-96-807/07/11 13:30399
Aniline ND ug/kg 1 07/15/11 13:20 62-53-307/07/11 13:30399
Anthracene ND ug/kg 1 07/15/11 13:20 120-12-707/07/11 13:30399
Benzo(a)anthracene ND ug/kg 1 07/15/11 13:20 56-55-307/07/11 13:30399
Benzo(a)pyrene ND ug/kg 1 07/15/11 13:20 50-32-807/07/11 13:30399
Benzo(b)fluoranthene ND ug/kg 1 07/15/11 13:20 205-99-207/07/11 13:30399
Benzo(g,h,i)perylene ND ug/kg 1 07/15/11 13:20 191-24-207/07/11 13:30399
Benzo(k)fluoranthene ND ug/kg 1 07/15/11 13:20 207-08-907/07/11 13:30399
Benzoic Acid ND ug/kg 1 07/15/11 13:20 65-85-007/07/11 13:302000
Benzyl alcohol ND ug/kg 1 07/15/11 13:20 100-51-607/07/11 13:30799
4-Bromophenylphenyl ether ND ug/kg 1 07/15/11 13:20 101-55-307/07/11 13:30399
Butylbenzylphthalate ND ug/kg 1 07/15/11 13:20 85-68-707/07/11 13:30399
4-Chloro-3-methylphenol ND ug/kg 1 07/15/11 13:20 59-50-707/07/11 13:30799
4-Chloroaniline ND ug/kg 1 07/15/11 13:20 106-47-807/07/11 13:302000
bis(2-Chloroethoxy)methane ND ug/kg 1 07/15/11 13:20 111-91-107/07/11 13:30399
bis(2-Chloroethyl) ether ND ug/kg 1 07/15/11 13:20 111-44-407/07/11 13:30399
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/15/11 13:20 108-60-107/07/11 13:30399
2-Chloronaphthalene ND ug/kg 1 07/15/11 13:20 91-58-707/07/11 13:30399
2-Chlorophenol ND ug/kg 1 07/15/11 13:20 95-57-807/07/11 13:30399
4-Chlorophenylphenyl ether ND ug/kg 1 07/15/11 13:20 7005-72-307/07/11 13:30399
Chrysene ND ug/kg 1 07/15/11 13:20 218-01-907/07/11 13:30399
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 56 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 5A (6-7)Lab ID:9297694009 Collected:07/06/11 14:10 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/15/11 13:20 53-70-307/07/11 13:30399
Dibenzofuran ND ug/kg 1 07/15/11 13:20 132-64-907/07/11 13:30399
1,2-Dichlorobenzene ND ug/kg 1 07/15/11 13:20 95-50-107/07/11 13:30399
1,3-Dichlorobenzene ND ug/kg 1 07/15/11 13:20 541-73-107/07/11 13:30399
1,4-Dichlorobenzene ND ug/kg 1 07/15/11 13:20 106-46-707/07/11 13:30399
3,3'-Dichlorobenzidine ND ug/kg 1 07/15/11 13:20 91-94-107/07/11 13:302000
2,4-Dichlorophenol ND ug/kg 1 07/15/11 13:20 120-83-207/07/11 13:30399
Diethylphthalate ND ug/kg 1 07/15/11 13:20 84-66-207/07/11 13:30399
2,4-Dimethylphenol ND ug/kg 1 07/15/11 13:20 105-67-907/07/11 13:30399
Dimethylphthalate ND ug/kg 1 07/15/11 13:20 131-11-307/07/11 13:30399
Di-n-butylphthalate ND ug/kg 1 07/15/11 13:20 84-74-207/07/11 13:30399
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/15/11 13:20 534-52-107/07/11 13:30799
2,4-Dinitrophenol ND ug/kg 1 07/15/11 13:20 51-28-507/07/11 13:302000
2,4-Dinitrotoluene ND ug/kg 1 07/15/11 13:20 121-14-207/07/11 13:30399
2,6-Dinitrotoluene ND ug/kg 1 07/15/11 13:20 606-20-207/07/11 13:30399
Di-n-octylphthalate ND ug/kg 1 07/15/11 13:20 117-84-007/07/11 13:30399
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/15/11 13:20 117-81-707/07/11 13:30399
Fluoranthene ND ug/kg 1 07/15/11 13:20 206-44-007/07/11 13:30399
Fluorene ND ug/kg 1 07/15/11 13:20 86-73-707/07/11 13:30399
Hexachloro-1,3-butadiene ND ug/kg 1 07/15/11 13:20 87-68-307/07/11 13:30399
Hexachlorobenzene ND ug/kg 1 07/15/11 13:20 118-74-107/07/11 13:30399
Hexachlorocyclopentadiene ND ug/kg 1 07/15/11 13:20 77-47-407/07/11 13:30399
Hexachloroethane ND ug/kg 1 07/15/11 13:20 67-72-107/07/11 13:30399
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/15/11 13:20 193-39-507/07/11 13:30399
Isophorone ND ug/kg 1 07/15/11 13:20 78-59-107/07/11 13:30399
1-Methylnaphthalene ND ug/kg 1 07/15/11 13:20 90-12-007/07/11 13:30399
2-Methylnaphthalene ND ug/kg 1 07/15/11 13:20 91-57-607/07/11 13:30399
2-Methylphenol(o-Cresol)ND ug/kg 1 07/15/11 13:20 95-48-707/07/11 13:30399
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/15/11 13:2007/07/11 13:30399
Naphthalene ND ug/kg 1 07/15/11 13:20 91-20-307/07/11 13:30399
2-Nitroaniline ND ug/kg 1 07/15/11 13:20 88-74-407/07/11 13:302000
3-Nitroaniline ND ug/kg 1 07/15/11 13:20 99-09-207/07/11 13:302000
4-Nitroaniline ND ug/kg 1 07/15/11 13:20 100-01-607/07/11 13:30799
Nitrobenzene ND ug/kg 1 07/15/11 13:20 98-95-307/07/11 13:30399
2-Nitrophenol ND ug/kg 1 07/15/11 13:20 88-75-507/07/11 13:30399
4-Nitrophenol ND ug/kg 1 07/15/11 13:20 100-02-707/07/11 13:302000
N-Nitrosodimethylamine ND ug/kg 1 07/15/11 13:20 62-75-907/07/11 13:30399
N-Nitroso-di-n-propylamine ND ug/kg 1 07/15/11 13:20 621-64-707/07/11 13:30399
N-Nitrosodiphenylamine ND ug/kg 1 07/15/11 13:20 86-30-607/07/11 13:30399
Pentachlorophenol ND ug/kg 1 07/15/11 13:20 87-86-507/07/11 13:302000
Phenanthrene ND ug/kg 1 07/15/11 13:20 85-01-807/07/11 13:30399
Phenol ND ug/kg 1 07/15/11 13:20 108-95-207/07/11 13:30399
Pyrene ND ug/kg 1 07/15/11 13:20 129-00-007/07/11 13:30399
1,2,4-Trichlorobenzene ND ug/kg 1 07/15/11 13:20 120-82-107/07/11 13:30399
2,4,5-Trichlorophenol ND ug/kg 1 07/15/11 13:20 95-95-407/07/11 13:30399
2,4,6-Trichlorophenol ND ug/kg 1 07/15/11 13:20 88-06-207/07/11 13:30399
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 57 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 5A (6-7)Lab ID:9297694009 Collected:07/06/11 14:10 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)80 %1 07/15/11 13:20 4165-60-007/07/11 13:3023-110
2-Fluorobiphenyl (S)77 %1 07/15/11 13:20 321-60-807/07/11 13:3030-110
Terphenyl-d14 (S)89 %1 07/15/11 13:20 1718-51-007/07/11 13:3028-110
Phenol-d6 (S)58 %1 07/15/11 13:20 13127-88-307/07/11 13:3022-110
2-Fluorophenol (S)60 %1 07/15/11 13:20 367-12-407/07/11 13:3013-110
2,4,6-Tribromophenol (S)81 %1 07/15/11 13:20 118-79-607/07/11 13:3027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 126 ug/kg 1 07/12/11 19:19 67-64-1 C996.7
Benzene ND ug/kg 1 07/12/11 19:19 71-43-24.8
Bromobenzene ND ug/kg 1 07/12/11 19:19 108-86-14.8
Bromochloromethane ND ug/kg 1 07/12/11 19:19 74-97-54.8
Bromodichloromethane ND ug/kg 1 07/12/11 19:19 75-27-44.8
Bromoform ND ug/kg 1 07/12/11 19:19 75-25-24.8
Bromomethane ND ug/kg 1 07/12/11 19:19 74-83-99.7
2-Butanone (MEK)ND ug/kg 1 07/12/11 19:19 78-93-396.7
n-Butylbenzene ND ug/kg 1 07/12/11 19:19 104-51-84.8
sec-Butylbenzene ND ug/kg 1 07/12/11 19:19 135-98-84.8
tert-Butylbenzene ND ug/kg 1 07/12/11 19:19 98-06-64.8
Carbon tetrachloride ND ug/kg 1 07/12/11 19:19 56-23-54.8
Chlorobenzene ND ug/kg 1 07/12/11 19:19 108-90-74.8
Chloroethane ND ug/kg 1 07/12/11 19:19 75-00-39.7
Chloroform ND ug/kg 1 07/12/11 19:19 67-66-34.8
Chloromethane ND ug/kg 1 07/12/11 19:19 74-87-39.7
2-Chlorotoluene ND ug/kg 1 07/12/11 19:19 95-49-84.8
4-Chlorotoluene ND ug/kg 1 07/12/11 19:19 106-43-44.8
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/12/11 19:19 96-12-84.8
Dibromochloromethane ND ug/kg 1 07/12/11 19:19 124-48-14.8
1,2-Dibromoethane (EDB)ND ug/kg 1 07/12/11 19:19 106-93-44.8
Dibromomethane ND ug/kg 1 07/12/11 19:19 74-95-34.8
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 19:19 95-50-14.8
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 19:19 541-73-14.8
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 19:19 106-46-74.8
Dichlorodifluoromethane ND ug/kg 1 07/12/11 19:19 75-71-89.7
1,1-Dichloroethane ND ug/kg 1 07/12/11 19:19 75-34-34.8
1,2-Dichloroethane ND ug/kg 1 07/12/11 19:19 107-06-24.8
1,1-Dichloroethene ND ug/kg 1 07/12/11 19:19 75-35-44.8
cis-1,2-Dichloroethene ND ug/kg 1 07/12/11 19:19 156-59-24.8
trans-1,2-Dichloroethene ND ug/kg 1 07/12/11 19:19 156-60-54.8
1,2-Dichloropropane ND ug/kg 1 07/12/11 19:19 78-87-54.8
1,3-Dichloropropane ND ug/kg 1 07/12/11 19:19 142-28-94.8
2,2-Dichloropropane ND ug/kg 1 07/12/11 19:19 594-20-74.8
1,1-Dichloropropene ND ug/kg 1 07/12/11 19:19 563-58-64.8
cis-1,3-Dichloropropene ND ug/kg 1 07/12/11 19:19 10061-01-54.8
trans-1,3-Dichloropropene ND ug/kg 1 07/12/11 19:19 10061-02-64.8
Diisopropyl ether ND ug/kg 1 07/12/11 19:19 108-20-34.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 58 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 5A (6-7)Lab ID:9297694009 Collected:07/06/11 14:10 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/12/11 19:19 100-41-44.8
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 19:19 87-68-34.8
2-Hexanone ND ug/kg 1 07/12/11 19:19 591-78-648.3
Isopropylbenzene (Cumene)ND ug/kg 1 07/12/11 19:19 98-82-84.8
p-Isopropyltoluene ND ug/kg 1 07/12/11 19:19 99-87-64.8
Methylene Chloride ND ug/kg 1 07/12/11 19:19 75-09-219.3
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/12/11 19:19 108-10-148.3
Methyl-tert-butyl ether ND ug/kg 1 07/12/11 19:19 1634-04-44.8
Naphthalene ND ug/kg 1 07/12/11 19:19 91-20-34.8
n-Propylbenzene ND ug/kg 1 07/12/11 19:19 103-65-14.8
Styrene ND ug/kg 1 07/12/11 19:19 100-42-54.8
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/12/11 19:19 630-20-64.8
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/12/11 19:19 79-34-54.8
Tetrachloroethene ND ug/kg 1 07/12/11 19:19 127-18-44.8
Toluene ND ug/kg 1 07/12/11 19:19 108-88-34.8
1,2,3-Trichlorobenzene ND ug/kg 1 07/12/11 19:19 87-61-64.8
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 19:19 120-82-14.8
1,1,1-Trichloroethane ND ug/kg 1 07/12/11 19:19 71-55-64.8
1,1,2-Trichloroethane ND ug/kg 1 07/12/11 19:19 79-00-54.8
Trichloroethene ND ug/kg 1 07/12/11 19:19 79-01-64.8
Trichlorofluoromethane ND ug/kg 1 07/12/11 19:19 75-69-44.8
1,2,3-Trichloropropane ND ug/kg 1 07/12/11 19:19 96-18-44.8
1,2,4-Trimethylbenzene ND ug/kg 1 07/12/11 19:19 95-63-64.8
1,3,5-Trimethylbenzene ND ug/kg 1 07/12/11 19:19 108-67-84.8
Vinyl acetate ND ug/kg 1 07/12/11 19:19 108-05-448.3
Vinyl chloride ND ug/kg 1 07/12/11 19:19 75-01-49.7
Xylene (Total)ND ug/kg 1 07/12/11 19:19 1330-20-79.7
m&p-Xylene ND ug/kg 1 07/12/11 19:19 179601-23-19.7
o-Xylene ND ug/kg 1 07/12/11 19:19 95-47-64.8
Dibromofluoromethane (S)99 %1 07/12/11 19:19 1868-53-770-130
Toluene-d8 (S)103 %1 07/12/11 19:19 2037-26-570-130
4-Bromofluorobenzene (S)94 %1 07/12/11 19:19 460-00-470-130
1,2-Dichloroethane-d4 (S)82 %1 07/12/11 19:19 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 17.7 %1 07/08/11 08:540.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 59 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 5B (9-10)Lab ID:9297694010 Collected:07/06/11 14:30 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 87.6 mg/kg 1 07/12/11 05:49 68334-30-5 P307/08/11 10:2733.3
n-Pentacosane (S)0 %1 07/12/11 05:49 629-99-2 S407/08/11 10:2741-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease 2570 mg/kg 1 07/11/11 12:0507/11/11 11:2093.3
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/12/11 18:14 8006-61-907/12/11 10:346.7
4-Bromofluorobenzene (S)145 %1 07/12/11 18:14 460-00-407/12/11 10:3470-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 3.6 mg/kg 1 07/13/11 15:44 7440-38-207/12/11 11:400.63
Barium 120 mg/kg 1 07/13/11 15:44 7440-39-307/12/11 11:400.63
Cadmium 0.47 mg/kg 1 07/13/11 15:44 7440-43-907/12/11 11:400.13
Chromium 7.6 mg/kg 1 07/13/11 15:44 7440-47-307/12/11 11:400.63
Lead 267 mg/kg 1 07/13/11 15:44 7439-92-107/12/11 11:400.63
Selenium ND mg/kg 1 07/13/11 15:44 7782-49-207/12/11 11:401.3
Silver ND mg/kg 1 07/13/11 15:44 7440-22-407/12/11 11:400.63
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.038 mg/kg 1 07/11/11 18:02 7439-97-607/08/11 15:100.0049
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 10 07/15/11 14:44 83-32-907/07/11 13:3021900
Acenaphthylene ND ug/kg 10 07/15/11 14:44 208-96-807/07/11 13:3021900
Aniline ND ug/kg 10 07/15/11 14:44 62-53-307/07/11 13:3021900
Anthracene ND ug/kg 10 07/15/11 14:44 120-12-707/07/11 13:3021900
Benzo(a)anthracene ND ug/kg 10 07/15/11 14:44 56-55-307/07/11 13:3021900
Benzo(a)pyrene ND ug/kg 10 07/15/11 14:44 50-32-807/07/11 13:3021900
Benzo(b)fluoranthene ND ug/kg 10 07/15/11 14:44 205-99-207/07/11 13:3021900
Benzo(g,h,i)perylene ND ug/kg 10 07/15/11 14:44 191-24-207/07/11 13:3021900
Benzo(k)fluoranthene ND ug/kg 10 07/15/11 14:44 207-08-907/07/11 13:3021900
Benzoic Acid ND ug/kg 10 07/15/11 14:44 65-85-007/07/11 13:30110000
Benzyl alcohol ND ug/kg 10 07/15/11 14:44 100-51-607/07/11 13:3043900
4-Bromophenylphenyl ether ND ug/kg 10 07/15/11 14:44 101-55-307/07/11 13:3021900
Butylbenzylphthalate ND ug/kg 10 07/15/11 14:44 85-68-707/07/11 13:3021900
4-Chloro-3-methylphenol ND ug/kg 10 07/15/11 14:44 59-50-707/07/11 13:3043900
4-Chloroaniline ND ug/kg 10 07/15/11 14:44 106-47-807/07/11 13:30110000
bis(2-Chloroethoxy)methane ND ug/kg 10 07/15/11 14:44 111-91-107/07/11 13:3021900
bis(2-Chloroethyl) ether ND ug/kg 10 07/15/11 14:44 111-44-407/07/11 13:3021900
bis(2-Chloroisopropyl) ether ND ug/kg 10 07/15/11 14:44 108-60-107/07/11 13:3021900
2-Chloronaphthalene ND ug/kg 10 07/15/11 14:44 91-58-707/07/11 13:3021900
2-Chlorophenol ND ug/kg 10 07/15/11 14:44 95-57-807/07/11 13:3021900
4-Chlorophenylphenyl ether ND ug/kg 10 07/15/11 14:44 7005-72-307/07/11 13:3021900
Chrysene ND ug/kg 10 07/15/11 14:44 218-01-907/07/11 13:3021900
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 60 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 5B (9-10)Lab ID:9297694010 Collected:07/06/11 14:30 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 10 07/15/11 14:44 53-70-307/07/11 13:3021900
Dibenzofuran ND ug/kg 10 07/15/11 14:44 132-64-907/07/11 13:3021900
1,2-Dichlorobenzene ND ug/kg 10 07/15/11 14:44 95-50-107/07/11 13:3021900
1,3-Dichlorobenzene ND ug/kg 10 07/15/11 14:44 541-73-107/07/11 13:3021900
1,4-Dichlorobenzene ND ug/kg 10 07/15/11 14:44 106-46-707/07/11 13:3021900
3,3'-Dichlorobenzidine ND ug/kg 10 07/15/11 14:44 91-94-107/07/11 13:30110000
2,4-Dichlorophenol ND ug/kg 10 07/15/11 14:44 120-83-207/07/11 13:3021900
Diethylphthalate ND ug/kg 10 07/15/11 14:44 84-66-207/07/11 13:3021900
2,4-Dimethylphenol ND ug/kg 10 07/15/11 14:44 105-67-907/07/11 13:3021900
Dimethylphthalate ND ug/kg 10 07/15/11 14:44 131-11-307/07/11 13:3021900
Di-n-butylphthalate ND ug/kg 10 07/15/11 14:44 84-74-207/07/11 13:3021900
4,6-Dinitro-2-methylphenol ND ug/kg 10 07/15/11 14:44 534-52-107/07/11 13:3043900
2,4-Dinitrophenol ND ug/kg 10 07/15/11 14:44 51-28-507/07/11 13:30110000
2,4-Dinitrotoluene ND ug/kg 10 07/15/11 14:44 121-14-207/07/11 13:3021900
2,6-Dinitrotoluene ND ug/kg 10 07/15/11 14:44 606-20-207/07/11 13:3021900
Di-n-octylphthalate ND ug/kg 10 07/15/11 14:44 117-84-007/07/11 13:3021900
bis(2-Ethylhexyl)phthalate ND ug/kg 10 07/15/11 14:44 117-81-707/07/11 13:3021900
Fluoranthene ND ug/kg 10 07/15/11 14:44 206-44-007/07/11 13:3021900
Fluorene ND ug/kg 10 07/15/11 14:44 86-73-707/07/11 13:3021900
Hexachloro-1,3-butadiene ND ug/kg 10 07/15/11 14:44 87-68-307/07/11 13:3021900
Hexachlorobenzene ND ug/kg 10 07/15/11 14:44 118-74-107/07/11 13:3021900
Hexachlorocyclopentadiene ND ug/kg 10 07/15/11 14:44 77-47-407/07/11 13:3021900
Hexachloroethane ND ug/kg 10 07/15/11 14:44 67-72-107/07/11 13:3021900
Indeno(1,2,3-cd)pyrene ND ug/kg 10 07/15/11 14:44 193-39-507/07/11 13:3021900
Isophorone ND ug/kg 10 07/15/11 14:44 78-59-107/07/11 13:3021900
1-Methylnaphthalene ND ug/kg 10 07/15/11 14:44 90-12-007/07/11 13:3021900
2-Methylnaphthalene ND ug/kg 10 07/15/11 14:44 91-57-607/07/11 13:3021900
2-Methylphenol(o-Cresol)ND ug/kg 10 07/15/11 14:44 95-48-707/07/11 13:3021900
3&4-Methylphenol(m&p Cresol)ND ug/kg 10 07/15/11 14:4407/07/11 13:3021900
Naphthalene ND ug/kg 10 07/15/11 14:44 91-20-307/07/11 13:3021900
2-Nitroaniline ND ug/kg 10 07/15/11 14:44 88-74-407/07/11 13:30110000
3-Nitroaniline ND ug/kg 10 07/15/11 14:44 99-09-207/07/11 13:30110000
4-Nitroaniline ND ug/kg 10 07/15/11 14:44 100-01-607/07/11 13:3043900
Nitrobenzene ND ug/kg 10 07/15/11 14:44 98-95-307/07/11 13:3021900
2-Nitrophenol ND ug/kg 10 07/15/11 14:44 88-75-507/07/11 13:3021900
4-Nitrophenol ND ug/kg 10 07/15/11 14:44 100-02-707/07/11 13:30110000
N-Nitrosodimethylamine ND ug/kg 10 07/15/11 14:44 62-75-907/07/11 13:3021900
N-Nitroso-di-n-propylamine ND ug/kg 10 07/15/11 14:44 621-64-707/07/11 13:3021900
N-Nitrosodiphenylamine ND ug/kg 10 07/15/11 14:44 86-30-607/07/11 13:3021900
Pentachlorophenol ND ug/kg 10 07/15/11 14:44 87-86-507/07/11 13:30110000
Phenanthrene ND ug/kg 10 07/15/11 14:44 85-01-807/07/11 13:3021900
Phenol ND ug/kg 10 07/15/11 14:44 108-95-2 D3,P307/07/11 13:3021900
Pyrene ND ug/kg 10 07/15/11 14:44 129-00-007/07/11 13:3021900
1,2,4-Trichlorobenzene ND ug/kg 10 07/15/11 14:44 120-82-107/07/11 13:3021900
2,4,5-Trichlorophenol ND ug/kg 10 07/15/11 14:44 95-95-407/07/11 13:3021900
2,4,6-Trichlorophenol ND ug/kg 10 07/15/11 14:44 88-06-207/07/11 13:3021900
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 61 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 5B (9-10)Lab ID:9297694010 Collected:07/06/11 14:30 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)0 %10 07/15/11 14:44 4165-60-0 S407/07/11 13:3023-110
2-Fluorobiphenyl (S)0 %10 07/15/11 14:44 321-60-807/07/11 13:3030-110
Terphenyl-d14 (S)0 %10 07/15/11 14:44 1718-51-007/07/11 13:3028-110
Phenol-d6 (S)0 %10 07/15/11 14:44 13127-88-307/07/11 13:3022-110
2-Fluorophenol (S)0 %10 07/15/11 14:44 367-12-407/07/11 13:3013-110
2,4,6-Tribromophenol (S)0 %10 07/15/11 14:44 118-79-607/07/11 13:3027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 117 ug/kg 1 07/12/11 19:39 67-64-1 C9110
Benzene ND ug/kg 1 07/12/11 19:39 71-43-25.5
Bromobenzene ND ug/kg 1 07/12/11 19:39 108-86-15.5
Bromochloromethane ND ug/kg 1 07/12/11 19:39 74-97-55.5
Bromodichloromethane ND ug/kg 1 07/12/11 19:39 75-27-45.5
Bromoform ND ug/kg 1 07/12/11 19:39 75-25-25.5
Bromomethane ND ug/kg 1 07/12/11 19:39 74-83-911.0
2-Butanone (MEK)ND ug/kg 1 07/12/11 19:39 78-93-3110
n-Butylbenzene ND ug/kg 1 07/12/11 19:39 104-51-85.5
sec-Butylbenzene ND ug/kg 1 07/12/11 19:39 135-98-85.5
tert-Butylbenzene ND ug/kg 1 07/12/11 19:39 98-06-65.5
Carbon tetrachloride ND ug/kg 1 07/12/11 19:39 56-23-55.5
Chlorobenzene ND ug/kg 1 07/12/11 19:39 108-90-75.5
Chloroethane ND ug/kg 1 07/12/11 19:39 75-00-311.0
Chloroform ND ug/kg 1 07/12/11 19:39 67-66-35.5
Chloromethane ND ug/kg 1 07/12/11 19:39 74-87-311.0
2-Chlorotoluene ND ug/kg 1 07/12/11 19:39 95-49-85.5
4-Chlorotoluene ND ug/kg 1 07/12/11 19:39 106-43-45.5
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/12/11 19:39 96-12-85.5
Dibromochloromethane ND ug/kg 1 07/12/11 19:39 124-48-15.5
1,2-Dibromoethane (EDB)ND ug/kg 1 07/12/11 19:39 106-93-45.5
Dibromomethane ND ug/kg 1 07/12/11 19:39 74-95-35.5
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 19:39 95-50-15.5
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 19:39 541-73-15.5
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 19:39 106-46-75.5
Dichlorodifluoromethane ND ug/kg 1 07/12/11 19:39 75-71-8 1g11.0
1,1-Dichloroethane ND ug/kg 1 07/12/11 19:39 75-34-35.5
1,2-Dichloroethane ND ug/kg 1 07/12/11 19:39 107-06-25.5
1,1-Dichloroethene ND ug/kg 1 07/12/11 19:39 75-35-45.5
cis-1,2-Dichloroethene ND ug/kg 1 07/12/11 19:39 156-59-25.5
trans-1,2-Dichloroethene ND ug/kg 1 07/12/11 19:39 156-60-55.5
1,2-Dichloropropane ND ug/kg 1 07/12/11 19:39 78-87-55.5
1,3-Dichloropropane ND ug/kg 1 07/12/11 19:39 142-28-95.5
2,2-Dichloropropane ND ug/kg 1 07/12/11 19:39 594-20-75.5
1,1-Dichloropropene ND ug/kg 1 07/12/11 19:39 563-58-65.5
cis-1,3-Dichloropropene ND ug/kg 1 07/12/11 19:39 10061-01-55.5
trans-1,3-Dichloropropene ND ug/kg 1 07/12/11 19:39 10061-02-65.5
Diisopropyl ether ND ug/kg 1 07/12/11 19:39 108-20-35.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 62 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 5B (9-10)Lab ID:9297694010 Collected:07/06/11 14:30 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/12/11 19:39 100-41-45.5
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 19:39 87-68-35.5
2-Hexanone ND ug/kg 1 07/12/11 19:39 591-78-654.8
Isopropylbenzene (Cumene)ND ug/kg 1 07/12/11 19:39 98-82-85.5
p-Isopropyltoluene ND ug/kg 1 07/12/11 19:39 99-87-65.5
Methylene Chloride ND ug/kg 1 07/12/11 19:39 75-09-221.9
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/12/11 19:39 108-10-154.8
Methyl-tert-butyl ether ND ug/kg 1 07/12/11 19:39 1634-04-45.5
Naphthalene ND ug/kg 1 07/12/11 19:39 91-20-35.5
n-Propylbenzene ND ug/kg 1 07/12/11 19:39 103-65-15.5
Styrene ND ug/kg 1 07/12/11 19:39 100-42-55.5
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/12/11 19:39 630-20-65.5
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/12/11 19:39 79-34-55.5
Tetrachloroethene ND ug/kg 1 07/12/11 19:39 127-18-45.5
Toluene ND ug/kg 1 07/12/11 19:39 108-88-35.5
1,2,3-Trichlorobenzene ND ug/kg 1 07/12/11 19:39 87-61-65.5
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 19:39 120-82-15.5
1,1,1-Trichloroethane ND ug/kg 1 07/12/11 19:39 71-55-65.5
1,1,2-Trichloroethane ND ug/kg 1 07/12/11 19:39 79-00-55.5
Trichloroethene ND ug/kg 1 07/12/11 19:39 79-01-65.5
Trichlorofluoromethane ND ug/kg 1 07/12/11 19:39 75-69-45.5
1,2,3-Trichloropropane ND ug/kg 1 07/12/11 19:39 96-18-45.5
1,2,4-Trimethylbenzene ND ug/kg 1 07/12/11 19:39 95-63-65.5
1,3,5-Trimethylbenzene ND ug/kg 1 07/12/11 19:39 108-67-85.5
Vinyl acetate ND ug/kg 1 07/12/11 19:39 108-05-454.8
Vinyl chloride ND ug/kg 1 07/12/11 19:39 75-01-411.0
Xylene (Total)ND ug/kg 1 07/12/11 19:39 1330-20-711.0
m&p-Xylene ND ug/kg 1 07/12/11 19:39 179601-23-111.0
o-Xylene ND ug/kg 1 07/12/11 19:39 95-47-65.5
Dibromofluoromethane (S)102 %1 07/12/11 19:39 1868-53-770-130
Toluene-d8 (S)97 %1 07/12/11 19:39 2037-26-570-130
4-Bromofluorobenzene (S)79 %1 07/12/11 19:39 460-00-470-130
1,2-Dichloroethane-d4 (S)93 %1 07/12/11 19:39 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 25.0 %1 07/08/11 08:540.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 63 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 6A (6-7)Lab ID:9297694011 Collected:07/06/11 14:50 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 13.4 mg/kg 1 07/12/11 05:49 68334-30-507/08/11 10:275.7
n-Pentacosane (S)72 %1 07/12/11 05:49 629-99-207/08/11 10:2741-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease ND mg/kg 1 07/11/11 12:0507/11/11 11:2180.2
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/12/11 23:12 8006-61-907/12/11 14:506.0
4-Bromofluorobenzene (S)146 %1 07/12/11 23:12 460-00-407/12/11 14:5070-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 2.5 mg/kg 1 07/14/11 13:27 7440-38-207/12/11 11:400.50
Barium 112 mg/kg 1 07/13/11 19:35 7440-39-307/12/11 11:400.50
Cadmium ND mg/kg 1 07/13/11 19:35 7440-43-907/12/11 11:400.10
Chromium 3.3 mg/kg 1 07/13/11 19:35 7440-47-307/12/11 11:400.50
Lead 23.3 mg/kg 1 07/13/11 19:35 7439-92-107/12/11 11:400.50
Selenium ND mg/kg 1 07/13/11 19:35 7782-49-207/12/11 11:401.0
Silver ND mg/kg 1 07/13/11 19:35 7440-22-407/12/11 11:400.50
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.016 mg/kg 1 07/11/11 18:10 7439-97-607/08/11 15:100.0045
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/13/11 11:01 83-32-907/08/11 11:00378
Acenaphthylene ND ug/kg 1 07/13/11 11:01 208-96-807/08/11 11:00378
Aniline ND ug/kg 1 07/13/11 11:01 62-53-307/08/11 11:00378
Anthracene ND ug/kg 1 07/13/11 11:01 120-12-707/08/11 11:00378
Benzo(a)anthracene ND ug/kg 1 07/13/11 11:01 56-55-307/08/11 11:00378
Benzo(a)pyrene ND ug/kg 1 07/13/11 11:01 50-32-807/08/11 11:00378
Benzo(b)fluoranthene ND ug/kg 1 07/13/11 11:01 205-99-207/08/11 11:00378
Benzo(g,h,i)perylene ND ug/kg 1 07/13/11 11:01 191-24-207/08/11 11:00378
Benzo(k)fluoranthene ND ug/kg 1 07/13/11 11:01 207-08-907/08/11 11:00378
Benzoic Acid ND ug/kg 1 07/13/11 11:01 65-85-007/08/11 11:001890
Benzyl alcohol ND ug/kg 1 07/13/11 11:01 100-51-607/08/11 11:00756
4-Bromophenylphenyl ether ND ug/kg 1 07/13/11 11:01 101-55-307/08/11 11:00378
Butylbenzylphthalate ND ug/kg 1 07/13/11 11:01 85-68-707/08/11 11:00378
4-Chloro-3-methylphenol ND ug/kg 1 07/13/11 11:01 59-50-707/08/11 11:00756
4-Chloroaniline ND ug/kg 1 07/13/11 11:01 106-47-807/08/11 11:001890
bis(2-Chloroethoxy)methane ND ug/kg 1 07/13/11 11:01 111-91-107/08/11 11:00378
bis(2-Chloroethyl) ether ND ug/kg 1 07/13/11 11:01 111-44-407/08/11 11:00378
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/13/11 11:01 108-60-107/08/11 11:00378
2-Chloronaphthalene ND ug/kg 1 07/13/11 11:01 91-58-707/08/11 11:00378
2-Chlorophenol ND ug/kg 1 07/13/11 11:01 95-57-807/08/11 11:00378
4-Chlorophenylphenyl ether ND ug/kg 1 07/13/11 11:01 7005-72-307/08/11 11:00378
Chrysene ND ug/kg 1 07/13/11 11:01 218-01-907/08/11 11:00378
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 64 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 6A (6-7)Lab ID:9297694011 Collected:07/06/11 14:50 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/13/11 11:01 53-70-307/08/11 11:00378
Dibenzofuran ND ug/kg 1 07/13/11 11:01 132-64-907/08/11 11:00378
1,2-Dichlorobenzene ND ug/kg 1 07/13/11 11:01 95-50-107/08/11 11:00378
1,3-Dichlorobenzene ND ug/kg 1 07/13/11 11:01 541-73-107/08/11 11:00378
1,4-Dichlorobenzene ND ug/kg 1 07/13/11 11:01 106-46-707/08/11 11:00378
3,3'-Dichlorobenzidine ND ug/kg 1 07/13/11 11:01 91-94-107/08/11 11:001890
2,4-Dichlorophenol ND ug/kg 1 07/13/11 11:01 120-83-207/08/11 11:00378
Diethylphthalate ND ug/kg 1 07/13/11 11:01 84-66-207/08/11 11:00378
2,4-Dimethylphenol ND ug/kg 1 07/13/11 11:01 105-67-907/08/11 11:00378
Dimethylphthalate ND ug/kg 1 07/13/11 11:01 131-11-307/08/11 11:00378
Di-n-butylphthalate ND ug/kg 1 07/13/11 11:01 84-74-207/08/11 11:00378
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/13/11 11:01 534-52-107/08/11 11:00756
2,4-Dinitrophenol ND ug/kg 1 07/13/11 11:01 51-28-507/08/11 11:001890
2,4-Dinitrotoluene ND ug/kg 1 07/13/11 11:01 121-14-207/08/11 11:00378
2,6-Dinitrotoluene ND ug/kg 1 07/13/11 11:01 606-20-207/08/11 11:00378
Di-n-octylphthalate ND ug/kg 1 07/13/11 11:01 117-84-007/08/11 11:00378
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/13/11 11:01 117-81-707/08/11 11:00378
Fluoranthene ND ug/kg 1 07/13/11 11:01 206-44-007/08/11 11:00378
Fluorene ND ug/kg 1 07/13/11 11:01 86-73-707/08/11 11:00378
Hexachloro-1,3-butadiene ND ug/kg 1 07/13/11 11:01 87-68-307/08/11 11:00378
Hexachlorobenzene ND ug/kg 1 07/13/11 11:01 118-74-107/08/11 11:00378
Hexachlorocyclopentadiene ND ug/kg 1 07/13/11 11:01 77-47-407/08/11 11:00378
Hexachloroethane ND ug/kg 1 07/13/11 11:01 67-72-107/08/11 11:00378
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/13/11 11:01 193-39-507/08/11 11:00378
Isophorone ND ug/kg 1 07/13/11 11:01 78-59-107/08/11 11:00378
1-Methylnaphthalene ND ug/kg 1 07/13/11 11:01 90-12-007/08/11 11:00378
2-Methylnaphthalene ND ug/kg 1 07/13/11 11:01 91-57-607/08/11 11:00378
2-Methylphenol(o-Cresol)ND ug/kg 1 07/13/11 11:01 95-48-707/08/11 11:00378
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/13/11 11:0107/08/11 11:00378
Naphthalene ND ug/kg 1 07/13/11 11:01 91-20-307/08/11 11:00378
2-Nitroaniline ND ug/kg 1 07/13/11 11:01 88-74-407/08/11 11:001890
3-Nitroaniline ND ug/kg 1 07/13/11 11:01 99-09-207/08/11 11:001890
4-Nitroaniline ND ug/kg 1 07/13/11 11:01 100-01-607/08/11 11:00756
Nitrobenzene ND ug/kg 1 07/13/11 11:01 98-95-307/08/11 11:00378
2-Nitrophenol ND ug/kg 1 07/13/11 11:01 88-75-507/08/11 11:00378
4-Nitrophenol ND ug/kg 1 07/13/11 11:01 100-02-707/08/11 11:001890
N-Nitrosodimethylamine ND ug/kg 1 07/13/11 11:01 62-75-907/08/11 11:00378
N-Nitroso-di-n-propylamine ND ug/kg 1 07/13/11 11:01 621-64-707/08/11 11:00378
N-Nitrosodiphenylamine ND ug/kg 1 07/13/11 11:01 86-30-607/08/11 11:00378
Pentachlorophenol ND ug/kg 1 07/13/11 11:01 87-86-507/08/11 11:001890
Phenanthrene ND ug/kg 1 07/13/11 11:01 85-01-807/08/11 11:00378
Phenol ND ug/kg 1 07/13/11 11:01 108-95-207/08/11 11:00378
Pyrene ND ug/kg 1 07/13/11 11:01 129-00-007/08/11 11:00378
1,2,4-Trichlorobenzene ND ug/kg 1 07/13/11 11:01 120-82-107/08/11 11:00378
2,4,5-Trichlorophenol ND ug/kg 1 07/13/11 11:01 95-95-407/08/11 11:00378
2,4,6-Trichlorophenol ND ug/kg 1 07/13/11 11:01 88-06-207/08/11 11:00378
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 65 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 6A (6-7)Lab ID:9297694011 Collected:07/06/11 14:50 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)69 %1 07/13/11 11:01 4165-60-007/08/11 11:0023-110
2-Fluorobiphenyl (S)69 %1 07/13/11 11:01 321-60-807/08/11 11:0030-110
Terphenyl-d14 (S)68 %1 07/13/11 11:01 1718-51-007/08/11 11:0028-110
Phenol-d6 (S)50 %1 07/13/11 11:01 13127-88-307/08/11 11:0022-110
2-Fluorophenol (S)49 %1 07/13/11 11:01 367-12-407/08/11 11:0013-110
2,4,6-Tribromophenol (S)65 %1 07/13/11 11:01 118-79-607/08/11 11:0027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/12/11 19:59 67-64-196.9
Benzene ND ug/kg 1 07/12/11 19:59 71-43-24.8
Bromobenzene ND ug/kg 1 07/12/11 19:59 108-86-14.8
Bromochloromethane ND ug/kg 1 07/12/11 19:59 74-97-54.8
Bromodichloromethane ND ug/kg 1 07/12/11 19:59 75-27-44.8
Bromoform ND ug/kg 1 07/12/11 19:59 75-25-24.8
Bromomethane ND ug/kg 1 07/12/11 19:59 74-83-99.7
2-Butanone (MEK)ND ug/kg 1 07/12/11 19:59 78-93-396.9
n-Butylbenzene ND ug/kg 1 07/12/11 19:59 104-51-84.8
sec-Butylbenzene ND ug/kg 1 07/12/11 19:59 135-98-84.8
tert-Butylbenzene ND ug/kg 1 07/12/11 19:59 98-06-64.8
Carbon tetrachloride ND ug/kg 1 07/12/11 19:59 56-23-54.8
Chlorobenzene ND ug/kg 1 07/12/11 19:59 108-90-74.8
Chloroethane ND ug/kg 1 07/12/11 19:59 75-00-39.7
Chloroform ND ug/kg 1 07/12/11 19:59 67-66-34.8
Chloromethane ND ug/kg 1 07/12/11 19:59 74-87-39.7
2-Chlorotoluene ND ug/kg 1 07/12/11 19:59 95-49-84.8
4-Chlorotoluene ND ug/kg 1 07/12/11 19:59 106-43-44.8
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/12/11 19:59 96-12-84.8
Dibromochloromethane ND ug/kg 1 07/12/11 19:59 124-48-14.8
1,2-Dibromoethane (EDB)ND ug/kg 1 07/12/11 19:59 106-93-44.8
Dibromomethane ND ug/kg 1 07/12/11 19:59 74-95-34.8
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 19:59 95-50-14.8
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 19:59 541-73-14.8
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 19:59 106-46-74.8
Dichlorodifluoromethane ND ug/kg 1 07/12/11 19:59 75-71-89.7
1,1-Dichloroethane ND ug/kg 1 07/12/11 19:59 75-34-34.8
1,2-Dichloroethane ND ug/kg 1 07/12/11 19:59 107-06-24.8
1,1-Dichloroethene ND ug/kg 1 07/12/11 19:59 75-35-44.8
cis-1,2-Dichloroethene ND ug/kg 1 07/12/11 19:59 156-59-24.8
trans-1,2-Dichloroethene ND ug/kg 1 07/12/11 19:59 156-60-54.8
1,2-Dichloropropane ND ug/kg 1 07/12/11 19:59 78-87-54.8
1,3-Dichloropropane ND ug/kg 1 07/12/11 19:59 142-28-94.8
2,2-Dichloropropane ND ug/kg 1 07/12/11 19:59 594-20-74.8
1,1-Dichloropropene ND ug/kg 1 07/12/11 19:59 563-58-64.8
cis-1,3-Dichloropropene ND ug/kg 1 07/12/11 19:59 10061-01-54.8
trans-1,3-Dichloropropene ND ug/kg 1 07/12/11 19:59 10061-02-64.8
Diisopropyl ether ND ug/kg 1 07/12/11 19:59 108-20-34.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 66 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 6A (6-7)Lab ID:9297694011 Collected:07/06/11 14:50 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/12/11 19:59 100-41-44.8
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 19:59 87-68-34.8
2-Hexanone ND ug/kg 1 07/12/11 19:59 591-78-648.5
Isopropylbenzene (Cumene)ND ug/kg 1 07/12/11 19:59 98-82-84.8
p-Isopropyltoluene ND ug/kg 1 07/12/11 19:59 99-87-64.8
Methylene Chloride ND ug/kg 1 07/12/11 19:59 75-09-219.4
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/12/11 19:59 108-10-148.5
Methyl-tert-butyl ether ND ug/kg 1 07/12/11 19:59 1634-04-44.8
Naphthalene ND ug/kg 1 07/12/11 19:59 91-20-34.8
n-Propylbenzene ND ug/kg 1 07/12/11 19:59 103-65-14.8
Styrene ND ug/kg 1 07/12/11 19:59 100-42-54.8
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/12/11 19:59 630-20-64.8
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/12/11 19:59 79-34-54.8
Tetrachloroethene ND ug/kg 1 07/12/11 19:59 127-18-44.8
Toluene ND ug/kg 1 07/12/11 19:59 108-88-34.8
1,2,3-Trichlorobenzene ND ug/kg 1 07/12/11 19:59 87-61-64.8
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 19:59 120-82-14.8
1,1,1-Trichloroethane ND ug/kg 1 07/12/11 19:59 71-55-64.8
1,1,2-Trichloroethane ND ug/kg 1 07/12/11 19:59 79-00-54.8
Trichloroethene ND ug/kg 1 07/12/11 19:59 79-01-64.8
Trichlorofluoromethane ND ug/kg 1 07/12/11 19:59 75-69-44.8
1,2,3-Trichloropropane ND ug/kg 1 07/12/11 19:59 96-18-44.8
1,2,4-Trimethylbenzene ND ug/kg 1 07/12/11 19:59 95-63-64.8
1,3,5-Trimethylbenzene ND ug/kg 1 07/12/11 19:59 108-67-84.8
Vinyl acetate ND ug/kg 1 07/12/11 19:59 108-05-448.5
Vinyl chloride ND ug/kg 1 07/12/11 19:59 75-01-49.7
Xylene (Total)ND ug/kg 1 07/12/11 19:59 1330-20-79.7
m&p-Xylene ND ug/kg 1 07/12/11 19:59 179601-23-19.7
o-Xylene ND ug/kg 1 07/12/11 19:59 95-47-64.8
Dibromofluoromethane (S)96 %1 07/12/11 19:59 1868-53-770-130
Toluene-d8 (S)102 %1 07/12/11 19:59 2037-26-570-130
4-Bromofluorobenzene (S)95 %1 07/12/11 19:59 460-00-470-130
1,2-Dichloroethane-d4 (S)84 %1 07/12/11 19:59 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 12.7 %1 07/08/11 08:540.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 67 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 6B (9-10)Lab ID:9297694012 Collected:07/06/11 15:15 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components ND mg/kg 1 07/12/11 06:46 68334-30-507/08/11 10:275.9
n-Pentacosane (S)70 %1 07/12/11 06:46 629-99-207/08/11 10:2741-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease ND mg/kg 1 07/11/11 12:0507/11/11 11:2182.8
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/12/11 23:37 8006-61-907/12/11 14:505.3
4-Bromofluorobenzene (S)129 %1 07/12/11 23:37 460-00-407/12/11 14:5070-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 2.2 mg/kg 1 07/14/11 14:31 7440-38-207/12/11 11:400.49
Barium 50.0 mg/kg 1 07/13/11 19:52 7440-39-307/12/11 11:400.49
Cadmium ND mg/kg 1 07/13/11 19:52 7440-43-907/12/11 11:400.099
Chromium 3.8 mg/kg 1 07/13/11 19:52 7440-47-307/12/11 11:400.49
Lead 19.3 mg/kg 1 07/13/11 19:52 7439-92-107/12/11 11:400.49
Selenium ND mg/kg 1 07/13/11 19:52 7782-49-207/12/11 11:400.99
Silver ND mg/kg 1 07/13/11 19:52 7440-22-407/12/11 11:400.49
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.027 mg/kg 1 07/11/11 18:12 7439-97-607/08/11 15:100.0052
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/12/11 00:19 83-32-907/08/11 11:00391
Acenaphthylene ND ug/kg 1 07/12/11 00:19 208-96-807/08/11 11:00391
Aniline ND ug/kg 1 07/12/11 00:19 62-53-307/08/11 11:00391
Anthracene ND ug/kg 1 07/12/11 00:19 120-12-707/08/11 11:00391
Benzo(a)anthracene ND ug/kg 1 07/12/11 00:19 56-55-307/08/11 11:00391
Benzo(a)pyrene ND ug/kg 1 07/12/11 00:19 50-32-807/08/11 11:00391
Benzo(b)fluoranthene ND ug/kg 1 07/12/11 00:19 205-99-207/08/11 11:00391
Benzo(g,h,i)perylene ND ug/kg 1 07/12/11 00:19 191-24-207/08/11 11:00391
Benzo(k)fluoranthene ND ug/kg 1 07/12/11 00:19 207-08-907/08/11 11:00391
Benzoic Acid ND ug/kg 1 07/12/11 00:19 65-85-007/08/11 11:001950
Benzyl alcohol ND ug/kg 1 07/12/11 00:19 100-51-607/08/11 11:00781
4-Bromophenylphenyl ether ND ug/kg 1 07/12/11 00:19 101-55-307/08/11 11:00391
Butylbenzylphthalate ND ug/kg 1 07/12/11 00:19 85-68-707/08/11 11:00391
4-Chloro-3-methylphenol ND ug/kg 1 07/12/11 00:19 59-50-707/08/11 11:00781
4-Chloroaniline ND ug/kg 1 07/12/11 00:19 106-47-807/08/11 11:001950
bis(2-Chloroethoxy)methane ND ug/kg 1 07/12/11 00:19 111-91-107/08/11 11:00391
bis(2-Chloroethyl) ether ND ug/kg 1 07/12/11 00:19 111-44-407/08/11 11:00391
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/12/11 00:19 108-60-107/08/11 11:00391
2-Chloronaphthalene ND ug/kg 1 07/12/11 00:19 91-58-707/08/11 11:00391
2-Chlorophenol ND ug/kg 1 07/12/11 00:19 95-57-807/08/11 11:00391
4-Chlorophenylphenyl ether ND ug/kg 1 07/12/11 00:19 7005-72-307/08/11 11:00391
Chrysene ND ug/kg 1 07/12/11 00:19 218-01-907/08/11 11:00391
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 68 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 6B (9-10)Lab ID:9297694012 Collected:07/06/11 15:15 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/12/11 00:19 53-70-307/08/11 11:00391
Dibenzofuran ND ug/kg 1 07/12/11 00:19 132-64-907/08/11 11:00391
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 00:19 95-50-107/08/11 11:00391
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 00:19 541-73-107/08/11 11:00391
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 00:19 106-46-707/08/11 11:00391
3,3'-Dichlorobenzidine ND ug/kg 1 07/12/11 00:19 91-94-107/08/11 11:001950
2,4-Dichlorophenol ND ug/kg 1 07/12/11 00:19 120-83-207/08/11 11:00391
Diethylphthalate ND ug/kg 1 07/12/11 00:19 84-66-207/08/11 11:00391
2,4-Dimethylphenol ND ug/kg 1 07/12/11 00:19 105-67-907/08/11 11:00391
Dimethylphthalate ND ug/kg 1 07/12/11 00:19 131-11-307/08/11 11:00391
Di-n-butylphthalate ND ug/kg 1 07/12/11 00:19 84-74-207/08/11 11:00391
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/12/11 00:19 534-52-107/08/11 11:00781
2,4-Dinitrophenol ND ug/kg 1 07/12/11 00:19 51-28-507/08/11 11:001950
2,4-Dinitrotoluene ND ug/kg 1 07/12/11 00:19 121-14-207/08/11 11:00391
2,6-Dinitrotoluene ND ug/kg 1 07/12/11 00:19 606-20-207/08/11 11:00391
Di-n-octylphthalate ND ug/kg 1 07/12/11 00:19 117-84-007/08/11 11:00391
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/12/11 00:19 117-81-707/08/11 11:00391
Fluoranthene ND ug/kg 1 07/12/11 00:19 206-44-007/08/11 11:00391
Fluorene ND ug/kg 1 07/12/11 00:19 86-73-707/08/11 11:00391
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 00:19 87-68-307/08/11 11:00391
Hexachlorobenzene ND ug/kg 1 07/12/11 00:19 118-74-107/08/11 11:00391
Hexachlorocyclopentadiene ND ug/kg 1 07/12/11 00:19 77-47-407/08/11 11:00391
Hexachloroethane ND ug/kg 1 07/12/11 00:19 67-72-107/08/11 11:00391
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/12/11 00:19 193-39-507/08/11 11:00391
Isophorone ND ug/kg 1 07/12/11 00:19 78-59-107/08/11 11:00391
1-Methylnaphthalene ND ug/kg 1 07/12/11 00:19 90-12-007/08/11 11:00391
2-Methylnaphthalene ND ug/kg 1 07/12/11 00:19 91-57-607/08/11 11:00391
2-Methylphenol(o-Cresol)ND ug/kg 1 07/12/11 00:19 95-48-707/08/11 11:00391
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/12/11 00:1907/08/11 11:00391
Naphthalene ND ug/kg 1 07/12/11 00:19 91-20-307/08/11 11:00391
2-Nitroaniline ND ug/kg 1 07/12/11 00:19 88-74-407/08/11 11:001950
3-Nitroaniline ND ug/kg 1 07/12/11 00:19 99-09-207/08/11 11:001950
4-Nitroaniline ND ug/kg 1 07/12/11 00:19 100-01-607/08/11 11:00781
Nitrobenzene ND ug/kg 1 07/12/11 00:19 98-95-307/08/11 11:00391
2-Nitrophenol ND ug/kg 1 07/12/11 00:19 88-75-507/08/11 11:00391
4-Nitrophenol ND ug/kg 1 07/12/11 00:19 100-02-707/08/11 11:001950
N-Nitrosodimethylamine ND ug/kg 1 07/12/11 00:19 62-75-907/08/11 11:00391
N-Nitroso-di-n-propylamine ND ug/kg 1 07/12/11 00:19 621-64-707/08/11 11:00391
N-Nitrosodiphenylamine ND ug/kg 1 07/12/11 00:19 86-30-607/08/11 11:00391
Pentachlorophenol ND ug/kg 1 07/12/11 00:19 87-86-507/08/11 11:001950
Phenanthrene ND ug/kg 1 07/12/11 00:19 85-01-807/08/11 11:00391
Phenol ND ug/kg 1 07/12/11 00:19 108-95-207/08/11 11:00391
Pyrene ND ug/kg 1 07/12/11 00:19 129-00-007/08/11 11:00391
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 00:19 120-82-107/08/11 11:00391
2,4,5-Trichlorophenol ND ug/kg 1 07/12/11 00:19 95-95-407/08/11 11:00391
2,4,6-Trichlorophenol ND ug/kg 1 07/12/11 00:19 88-06-207/08/11 11:00391
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 69 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 6B (9-10)Lab ID:9297694012 Collected:07/06/11 15:15 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)50 %1 07/12/11 00:19 4165-60-007/08/11 11:0023-110
2-Fluorobiphenyl (S)53 %1 07/12/11 00:19 321-60-807/08/11 11:0030-110
Terphenyl-d14 (S)64 %1 07/12/11 00:19 1718-51-007/08/11 11:0028-110
Phenol-d6 (S)42 %1 07/12/11 00:19 13127-88-307/08/11 11:0022-110
2-Fluorophenol (S)42 %1 07/12/11 00:19 367-12-407/08/11 11:0013-110
2,4,6-Tribromophenol (S)53 %1 07/12/11 00:19 118-79-607/08/11 11:0027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 135 ug/kg 1 07/12/11 20:19 67-64-1 C988.7
Benzene ND ug/kg 1 07/12/11 20:19 71-43-24.4
Bromobenzene ND ug/kg 1 07/12/11 20:19 108-86-14.4
Bromochloromethane ND ug/kg 1 07/12/11 20:19 74-97-54.4
Bromodichloromethane ND ug/kg 1 07/12/11 20:19 75-27-44.4
Bromoform ND ug/kg 1 07/12/11 20:19 75-25-24.4
Bromomethane ND ug/kg 1 07/12/11 20:19 74-83-98.9
2-Butanone (MEK)ND ug/kg 1 07/12/11 20:19 78-93-388.7
n-Butylbenzene ND ug/kg 1 07/12/11 20:19 104-51-84.4
sec-Butylbenzene ND ug/kg 1 07/12/11 20:19 135-98-84.4
tert-Butylbenzene ND ug/kg 1 07/12/11 20:19 98-06-64.4
Carbon tetrachloride ND ug/kg 1 07/12/11 20:19 56-23-54.4
Chlorobenzene ND ug/kg 1 07/12/11 20:19 108-90-74.4
Chloroethane ND ug/kg 1 07/12/11 20:19 75-00-38.9
Chloroform ND ug/kg 1 07/12/11 20:19 67-66-34.4
Chloromethane ND ug/kg 1 07/12/11 20:19 74-87-38.9
2-Chlorotoluene ND ug/kg 1 07/12/11 20:19 95-49-84.4
4-Chlorotoluene ND ug/kg 1 07/12/11 20:19 106-43-44.4
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/12/11 20:19 96-12-84.4
Dibromochloromethane ND ug/kg 1 07/12/11 20:19 124-48-14.4
1,2-Dibromoethane (EDB)ND ug/kg 1 07/12/11 20:19 106-93-44.4
Dibromomethane ND ug/kg 1 07/12/11 20:19 74-95-34.4
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 20:19 95-50-14.4
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 20:19 541-73-14.4
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 20:19 106-46-74.4
Dichlorodifluoromethane ND ug/kg 1 07/12/11 20:19 75-71-88.9
1,1-Dichloroethane ND ug/kg 1 07/12/11 20:19 75-34-34.4
1,2-Dichloroethane ND ug/kg 1 07/12/11 20:19 107-06-24.4
1,1-Dichloroethene ND ug/kg 1 07/12/11 20:19 75-35-44.4
cis-1,2-Dichloroethene ND ug/kg 1 07/12/11 20:19 156-59-24.4
trans-1,2-Dichloroethene ND ug/kg 1 07/12/11 20:19 156-60-54.4
1,2-Dichloropropane ND ug/kg 1 07/12/11 20:19 78-87-54.4
1,3-Dichloropropane ND ug/kg 1 07/12/11 20:19 142-28-94.4
2,2-Dichloropropane ND ug/kg 1 07/12/11 20:19 594-20-74.4
1,1-Dichloropropene ND ug/kg 1 07/12/11 20:19 563-58-64.4
cis-1,3-Dichloropropene ND ug/kg 1 07/12/11 20:19 10061-01-54.4
trans-1,3-Dichloropropene ND ug/kg 1 07/12/11 20:19 10061-02-64.4
Diisopropyl ether ND ug/kg 1 07/12/11 20:19 108-20-34.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 70 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 6B (9-10)Lab ID:9297694012 Collected:07/06/11 15:15 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/12/11 20:19 100-41-44.4
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 20:19 87-68-34.4
2-Hexanone ND ug/kg 1 07/12/11 20:19 591-78-644.4
Isopropylbenzene (Cumene)ND ug/kg 1 07/12/11 20:19 98-82-84.4
p-Isopropyltoluene ND ug/kg 1 07/12/11 20:19 99-87-64.4
Methylene Chloride ND ug/kg 1 07/12/11 20:19 75-09-217.7
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/12/11 20:19 108-10-144.4
Methyl-tert-butyl ether ND ug/kg 1 07/12/11 20:19 1634-04-44.4
Naphthalene ND ug/kg 1 07/12/11 20:19 91-20-34.4
n-Propylbenzene ND ug/kg 1 07/12/11 20:19 103-65-14.4
Styrene ND ug/kg 1 07/12/11 20:19 100-42-54.4
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/12/11 20:19 630-20-64.4
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/12/11 20:19 79-34-54.4
Tetrachloroethene ND ug/kg 1 07/12/11 20:19 127-18-44.4
Toluene ND ug/kg 1 07/12/11 20:19 108-88-34.4
1,2,3-Trichlorobenzene ND ug/kg 1 07/12/11 20:19 87-61-64.4
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 20:19 120-82-14.4
1,1,1-Trichloroethane ND ug/kg 1 07/12/11 20:19 71-55-64.4
1,1,2-Trichloroethane ND ug/kg 1 07/12/11 20:19 79-00-54.4
Trichloroethene ND ug/kg 1 07/12/11 20:19 79-01-64.4
Trichlorofluoromethane ND ug/kg 1 07/12/11 20:19 75-69-44.4
1,2,3-Trichloropropane ND ug/kg 1 07/12/11 20:19 96-18-44.4
1,2,4-Trimethylbenzene ND ug/kg 1 07/12/11 20:19 95-63-64.4
1,3,5-Trimethylbenzene ND ug/kg 1 07/12/11 20:19 108-67-84.4
Vinyl acetate ND ug/kg 1 07/12/11 20:19 108-05-444.4
Vinyl chloride ND ug/kg 1 07/12/11 20:19 75-01-48.9
Xylene (Total)ND ug/kg 1 07/12/11 20:19 1330-20-78.9
m&p-Xylene ND ug/kg 1 07/12/11 20:19 179601-23-18.9
o-Xylene ND ug/kg 1 07/12/11 20:19 95-47-64.4
Dibromofluoromethane (S)96 %1 07/12/11 20:19 1868-53-770-130
Toluene-d8 (S)100 %1 07/12/11 20:19 2037-26-570-130
4-Bromofluorobenzene (S)85 %1 07/12/11 20:19 460-00-470-130
1,2-Dichloroethane-d4 (S)83 %1 07/12/11 20:19 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 15.5 %1 07/08/11 08:540.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 71 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 7A (6-7)Lab ID:9297694013 Collected:07/06/11 15:40 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 9.4 mg/kg 1 07/12/11 06:46 68334-30-507/08/11 10:275.4
n-Pentacosane (S)66 %1 07/12/11 06:46 629-99-207/08/11 10:2741-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease 405 mg/kg 1 07/11/11 12:0507/11/11 11:2175.3
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/13/11 00:51 8006-61-907/12/11 14:505.4
4-Bromofluorobenzene (S)159 %1 07/13/11 00:51 460-00-407/12/11 14:5070-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 2.1 mg/kg 1 07/14/11 14:34 7440-38-207/12/11 11:400.43
Barium 64.7 mg/kg 1 07/13/11 20:00 7440-39-307/12/11 11:400.43
Cadmium ND mg/kg 1 07/13/11 20:00 7440-43-907/12/11 11:400.087
Chromium 2.6 mg/kg 1 07/13/11 20:00 7440-47-307/12/11 11:400.43
Lead 12.0 mg/kg 1 07/13/11 20:00 7439-92-107/12/11 11:400.43
Selenium ND mg/kg 1 07/13/11 20:00 7782-49-207/12/11 11:400.87
Silver ND mg/kg 1 07/13/11 20:00 7440-22-407/12/11 11:400.43
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.015 mg/kg 1 07/11/11 18:15 7439-97-607/08/11 15:100.0045
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/12/11 15:31 83-32-907/08/11 11:00355
Acenaphthylene ND ug/kg 1 07/12/11 15:31 208-96-807/08/11 11:00355
Aniline ND ug/kg 1 07/12/11 15:31 62-53-307/08/11 11:00355
Anthracene ND ug/kg 1 07/12/11 15:31 120-12-707/08/11 11:00355
Benzo(a)anthracene ND ug/kg 1 07/12/11 15:31 56-55-307/08/11 11:00355
Benzo(a)pyrene ND ug/kg 1 07/12/11 15:31 50-32-807/08/11 11:00355
Benzo(b)fluoranthene ND ug/kg 1 07/12/11 15:31 205-99-207/08/11 11:00355
Benzo(g,h,i)perylene ND ug/kg 1 07/12/11 15:31 191-24-207/08/11 11:00355
Benzo(k)fluoranthene ND ug/kg 1 07/12/11 15:31 207-08-907/08/11 11:00355
Benzoic Acid ND ug/kg 1 07/12/11 15:31 65-85-007/08/11 11:001780
Benzyl alcohol ND ug/kg 1 07/12/11 15:31 100-51-607/08/11 11:00710
4-Bromophenylphenyl ether ND ug/kg 1 07/12/11 15:31 101-55-307/08/11 11:00355
Butylbenzylphthalate ND ug/kg 1 07/12/11 15:31 85-68-707/08/11 11:00355
4-Chloro-3-methylphenol ND ug/kg 1 07/12/11 15:31 59-50-707/08/11 11:00710
4-Chloroaniline ND ug/kg 1 07/12/11 15:31 106-47-807/08/11 11:001780
bis(2-Chloroethoxy)methane ND ug/kg 1 07/12/11 15:31 111-91-107/08/11 11:00355
bis(2-Chloroethyl) ether ND ug/kg 1 07/12/11 15:31 111-44-407/08/11 11:00355
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/12/11 15:31 108-60-107/08/11 11:00355
2-Chloronaphthalene ND ug/kg 1 07/12/11 15:31 91-58-707/08/11 11:00355
2-Chlorophenol ND ug/kg 1 07/12/11 15:31 95-57-807/08/11 11:00355
4-Chlorophenylphenyl ether ND ug/kg 1 07/12/11 15:31 7005-72-307/08/11 11:00355
Chrysene ND ug/kg 1 07/12/11 15:31 218-01-907/08/11 11:00355
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 72 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 7A (6-7)Lab ID:9297694013 Collected:07/06/11 15:40 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/12/11 15:31 53-70-307/08/11 11:00355
Dibenzofuran ND ug/kg 1 07/12/11 15:31 132-64-907/08/11 11:00355
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 15:31 95-50-107/08/11 11:00355
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 15:31 541-73-107/08/11 11:00355
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 15:31 106-46-707/08/11 11:00355
3,3'-Dichlorobenzidine ND ug/kg 1 07/12/11 15:31 91-94-107/08/11 11:001780
2,4-Dichlorophenol ND ug/kg 1 07/12/11 15:31 120-83-207/08/11 11:00355
Diethylphthalate ND ug/kg 1 07/12/11 15:31 84-66-207/08/11 11:00355
2,4-Dimethylphenol ND ug/kg 1 07/12/11 15:31 105-67-907/08/11 11:00355
Dimethylphthalate ND ug/kg 1 07/12/11 15:31 131-11-307/08/11 11:00355
Di-n-butylphthalate ND ug/kg 1 07/12/11 15:31 84-74-207/08/11 11:00355
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/12/11 15:31 534-52-107/08/11 11:00710
2,4-Dinitrophenol ND ug/kg 1 07/12/11 15:31 51-28-507/08/11 11:001780
2,4-Dinitrotoluene ND ug/kg 1 07/12/11 15:31 121-14-207/08/11 11:00355
2,6-Dinitrotoluene ND ug/kg 1 07/12/11 15:31 606-20-207/08/11 11:00355
Di-n-octylphthalate ND ug/kg 1 07/12/11 15:31 117-84-007/08/11 11:00355
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/12/11 15:31 117-81-707/08/11 11:00355
Fluoranthene ND ug/kg 1 07/12/11 15:31 206-44-007/08/11 11:00355
Fluorene ND ug/kg 1 07/12/11 15:31 86-73-707/08/11 11:00355
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 15:31 87-68-307/08/11 11:00355
Hexachlorobenzene ND ug/kg 1 07/12/11 15:31 118-74-107/08/11 11:00355
Hexachlorocyclopentadiene ND ug/kg 1 07/12/11 15:31 77-47-407/08/11 11:00355
Hexachloroethane ND ug/kg 1 07/12/11 15:31 67-72-107/08/11 11:00355
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/12/11 15:31 193-39-507/08/11 11:00355
Isophorone ND ug/kg 1 07/12/11 15:31 78-59-107/08/11 11:00355
1-Methylnaphthalene ND ug/kg 1 07/12/11 15:31 90-12-007/08/11 11:00355
2-Methylnaphthalene ND ug/kg 1 07/12/11 15:31 91-57-607/08/11 11:00355
2-Methylphenol(o-Cresol)ND ug/kg 1 07/12/11 15:31 95-48-707/08/11 11:00355
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/12/11 15:3107/08/11 11:00355
Naphthalene ND ug/kg 1 07/12/11 15:31 91-20-307/08/11 11:00355
2-Nitroaniline ND ug/kg 1 07/12/11 15:31 88-74-407/08/11 11:001780
3-Nitroaniline ND ug/kg 1 07/12/11 15:31 99-09-207/08/11 11:001780
4-Nitroaniline ND ug/kg 1 07/12/11 15:31 100-01-607/08/11 11:00710
Nitrobenzene ND ug/kg 1 07/12/11 15:31 98-95-307/08/11 11:00355
2-Nitrophenol ND ug/kg 1 07/12/11 15:31 88-75-507/08/11 11:00355
4-Nitrophenol ND ug/kg 1 07/12/11 15:31 100-02-707/08/11 11:001780
N-Nitrosodimethylamine ND ug/kg 1 07/12/11 15:31 62-75-907/08/11 11:00355
N-Nitroso-di-n-propylamine ND ug/kg 1 07/12/11 15:31 621-64-707/08/11 11:00355
N-Nitrosodiphenylamine ND ug/kg 1 07/12/11 15:31 86-30-607/08/11 11:00355
Pentachlorophenol ND ug/kg 1 07/12/11 15:31 87-86-507/08/11 11:001780
Phenanthrene ND ug/kg 1 07/12/11 15:31 85-01-807/08/11 11:00355
Phenol ND ug/kg 1 07/12/11 15:31 108-95-207/08/11 11:00355
Pyrene ND ug/kg 1 07/12/11 15:31 129-00-007/08/11 11:00355
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 15:31 120-82-107/08/11 11:00355
2,4,5-Trichlorophenol ND ug/kg 1 07/12/11 15:31 95-95-407/08/11 11:00355
2,4,6-Trichlorophenol ND ug/kg 1 07/12/11 15:31 88-06-207/08/11 11:00355
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 73 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 7A (6-7)Lab ID:9297694013 Collected:07/06/11 15:40 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)72 %1 07/12/11 15:31 4165-60-007/08/11 11:0023-110
2-Fluorobiphenyl (S)72 %1 07/12/11 15:31 321-60-807/08/11 11:0030-110
Terphenyl-d14 (S)77 %1 07/12/11 15:31 1718-51-007/08/11 11:0028-110
Phenol-d6 (S)34 %1 07/12/11 15:31 13127-88-307/08/11 11:0022-110
2-Fluorophenol (S)30 %1 07/12/11 15:31 367-12-407/08/11 11:0013-110
2,4,6-Tribromophenol (S)50 %1 07/12/11 15:31 118-79-607/08/11 11:0027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/12/11 20:39 67-64-188.9
Benzene ND ug/kg 1 07/12/11 20:39 71-43-24.4
Bromobenzene ND ug/kg 1 07/12/11 20:39 108-86-14.4
Bromochloromethane ND ug/kg 1 07/12/11 20:39 74-97-54.4
Bromodichloromethane ND ug/kg 1 07/12/11 20:39 75-27-44.4
Bromoform ND ug/kg 1 07/12/11 20:39 75-25-24.4
Bromomethane ND ug/kg 1 07/12/11 20:39 74-83-98.9
2-Butanone (MEK)ND ug/kg 1 07/12/11 20:39 78-93-388.9
n-Butylbenzene ND ug/kg 1 07/12/11 20:39 104-51-84.4
sec-Butylbenzene ND ug/kg 1 07/12/11 20:39 135-98-84.4
tert-Butylbenzene ND ug/kg 1 07/12/11 20:39 98-06-64.4
Carbon tetrachloride ND ug/kg 1 07/12/11 20:39 56-23-54.4
Chlorobenzene ND ug/kg 1 07/12/11 20:39 108-90-74.4
Chloroethane ND ug/kg 1 07/12/11 20:39 75-00-38.9
Chloroform ND ug/kg 1 07/12/11 20:39 67-66-34.4
Chloromethane ND ug/kg 1 07/12/11 20:39 74-87-38.9
2-Chlorotoluene ND ug/kg 1 07/12/11 20:39 95-49-84.4
4-Chlorotoluene ND ug/kg 1 07/12/11 20:39 106-43-44.4
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/12/11 20:39 96-12-84.4
Dibromochloromethane ND ug/kg 1 07/12/11 20:39 124-48-14.4
1,2-Dibromoethane (EDB)ND ug/kg 1 07/12/11 20:39 106-93-44.4
Dibromomethane ND ug/kg 1 07/12/11 20:39 74-95-34.4
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 20:39 95-50-14.4
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 20:39 541-73-14.4
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 20:39 106-46-74.4
Dichlorodifluoromethane ND ug/kg 1 07/12/11 20:39 75-71-88.9
1,1-Dichloroethane ND ug/kg 1 07/12/11 20:39 75-34-34.4
1,2-Dichloroethane ND ug/kg 1 07/12/11 20:39 107-06-24.4
1,1-Dichloroethene ND ug/kg 1 07/12/11 20:39 75-35-44.4
cis-1,2-Dichloroethene ND ug/kg 1 07/12/11 20:39 156-59-24.4
trans-1,2-Dichloroethene ND ug/kg 1 07/12/11 20:39 156-60-54.4
1,2-Dichloropropane ND ug/kg 1 07/12/11 20:39 78-87-54.4
1,3-Dichloropropane ND ug/kg 1 07/12/11 20:39 142-28-94.4
2,2-Dichloropropane ND ug/kg 1 07/12/11 20:39 594-20-74.4
1,1-Dichloropropene ND ug/kg 1 07/12/11 20:39 563-58-64.4
cis-1,3-Dichloropropene ND ug/kg 1 07/12/11 20:39 10061-01-54.4
trans-1,3-Dichloropropene ND ug/kg 1 07/12/11 20:39 10061-02-64.4
Diisopropyl ether ND ug/kg 1 07/12/11 20:39 108-20-34.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 74 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 7A (6-7)Lab ID:9297694013 Collected:07/06/11 15:40 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/12/11 20:39 100-41-44.4
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 20:39 87-68-34.4
2-Hexanone ND ug/kg 1 07/12/11 20:39 591-78-644.5
Isopropylbenzene (Cumene)ND ug/kg 1 07/12/11 20:39 98-82-84.4
p-Isopropyltoluene ND ug/kg 1 07/12/11 20:39 99-87-64.4
Methylene Chloride ND ug/kg 1 07/12/11 20:39 75-09-217.8
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/12/11 20:39 108-10-144.5
Methyl-tert-butyl ether ND ug/kg 1 07/12/11 20:39 1634-04-44.4
Naphthalene ND ug/kg 1 07/12/11 20:39 91-20-34.4
n-Propylbenzene ND ug/kg 1 07/12/11 20:39 103-65-14.4
Styrene ND ug/kg 1 07/12/11 20:39 100-42-54.4
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/12/11 20:39 630-20-64.4
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/12/11 20:39 79-34-54.4
Tetrachloroethene ND ug/kg 1 07/12/11 20:39 127-18-44.4
Toluene ND ug/kg 1 07/12/11 20:39 108-88-34.4
1,2,3-Trichlorobenzene ND ug/kg 1 07/12/11 20:39 87-61-64.4
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 20:39 120-82-14.4
1,1,1-Trichloroethane ND ug/kg 1 07/12/11 20:39 71-55-64.4
1,1,2-Trichloroethane ND ug/kg 1 07/12/11 20:39 79-00-54.4
Trichloroethene ND ug/kg 1 07/12/11 20:39 79-01-64.4
Trichlorofluoromethane ND ug/kg 1 07/12/11 20:39 75-69-44.4
1,2,3-Trichloropropane ND ug/kg 1 07/12/11 20:39 96-18-44.4
1,2,4-Trimethylbenzene ND ug/kg 1 07/12/11 20:39 95-63-64.4
1,3,5-Trimethylbenzene ND ug/kg 1 07/12/11 20:39 108-67-84.4
Vinyl acetate ND ug/kg 1 07/12/11 20:39 108-05-444.5
Vinyl chloride ND ug/kg 1 07/12/11 20:39 75-01-48.9
Xylene (Total)ND ug/kg 1 07/12/11 20:39 1330-20-78.9
m&p-Xylene ND ug/kg 1 07/12/11 20:39 179601-23-18.9
o-Xylene ND ug/kg 1 07/12/11 20:39 95-47-64.4
Dibromofluoromethane (S)94 %1 07/12/11 20:39 1868-53-770-130
Toluene-d8 (S)102 %1 07/12/11 20:39 2037-26-570-130
4-Bromofluorobenzene (S)91 %1 07/12/11 20:39 460-00-470-130
1,2-Dichloroethane-d4 (S)84 %1 07/12/11 20:39 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 7.1 %1 07/08/11 08:550.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 75 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 7B (9-10)Lab ID:9297694014 Collected:07/06/11 15:50 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components ND mg/kg 1 07/12/11 07:42 68334-30-507/08/11 10:275.9
n-Pentacosane (S)62 %1 07/12/11 07:42 629-99-207/08/11 10:2741-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease ND mg/kg 1 07/11/11 12:0507/11/11 11:2283.0
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/13/11 01:16 8006-61-907/12/11 14:506.7
4-Bromofluorobenzene (S)140 %1 07/13/11 01:16 460-00-407/12/11 14:5070-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 3.0 mg/kg 1 07/14/11 14:39 7440-38-207/12/11 11:400.56
Barium 82.3 mg/kg 1 07/13/11 20:03 7440-39-307/12/11 11:400.56
Cadmium ND mg/kg 1 07/13/11 20:03 7440-43-907/12/11 11:400.11
Chromium 3.4 mg/kg 1 07/13/11 20:03 7440-47-307/12/11 11:400.56
Lead 17.3 mg/kg 1 07/13/11 20:03 7439-92-107/12/11 11:400.56
Selenium 1.2 mg/kg 1 07/13/11 20:03 7782-49-207/12/11 11:401.1
Silver ND mg/kg 1 07/13/11 20:03 7440-22-407/12/11 11:400.56
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.012 mg/kg 1 07/11/11 18:18 7439-97-607/08/11 15:100.0051
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/12/11 00:47 83-32-907/08/11 11:00392
Acenaphthylene ND ug/kg 1 07/12/11 00:47 208-96-807/08/11 11:00392
Aniline ND ug/kg 1 07/12/11 00:47 62-53-307/08/11 11:00392
Anthracene ND ug/kg 1 07/12/11 00:47 120-12-707/08/11 11:00392
Benzo(a)anthracene ND ug/kg 1 07/12/11 00:47 56-55-307/08/11 11:00392
Benzo(a)pyrene ND ug/kg 1 07/12/11 00:47 50-32-807/08/11 11:00392
Benzo(b)fluoranthene ND ug/kg 1 07/12/11 00:47 205-99-207/08/11 11:00392
Benzo(g,h,i)perylene ND ug/kg 1 07/12/11 00:47 191-24-207/08/11 11:00392
Benzo(k)fluoranthene ND ug/kg 1 07/12/11 00:47 207-08-907/08/11 11:00392
Benzoic Acid ND ug/kg 1 07/12/11 00:47 65-85-007/08/11 11:001960
Benzyl alcohol ND ug/kg 1 07/12/11 00:47 100-51-607/08/11 11:00783
4-Bromophenylphenyl ether ND ug/kg 1 07/12/11 00:47 101-55-307/08/11 11:00392
Butylbenzylphthalate ND ug/kg 1 07/12/11 00:47 85-68-707/08/11 11:00392
4-Chloro-3-methylphenol ND ug/kg 1 07/12/11 00:47 59-50-707/08/11 11:00783
4-Chloroaniline ND ug/kg 1 07/12/11 00:47 106-47-807/08/11 11:001960
bis(2-Chloroethoxy)methane ND ug/kg 1 07/12/11 00:47 111-91-107/08/11 11:00392
bis(2-Chloroethyl) ether ND ug/kg 1 07/12/11 00:47 111-44-407/08/11 11:00392
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/12/11 00:47 108-60-107/08/11 11:00392
2-Chloronaphthalene ND ug/kg 1 07/12/11 00:47 91-58-707/08/11 11:00392
2-Chlorophenol ND ug/kg 1 07/12/11 00:47 95-57-807/08/11 11:00392
4-Chlorophenylphenyl ether ND ug/kg 1 07/12/11 00:47 7005-72-307/08/11 11:00392
Chrysene ND ug/kg 1 07/12/11 00:47 218-01-907/08/11 11:00392
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 76 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 7B (9-10)Lab ID:9297694014 Collected:07/06/11 15:50 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/12/11 00:47 53-70-307/08/11 11:00392
Dibenzofuran ND ug/kg 1 07/12/11 00:47 132-64-907/08/11 11:00392
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 00:47 95-50-107/08/11 11:00392
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 00:47 541-73-107/08/11 11:00392
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 00:47 106-46-707/08/11 11:00392
3,3'-Dichlorobenzidine ND ug/kg 1 07/12/11 00:47 91-94-107/08/11 11:001960
2,4-Dichlorophenol ND ug/kg 1 07/12/11 00:47 120-83-207/08/11 11:00392
Diethylphthalate ND ug/kg 1 07/12/11 00:47 84-66-207/08/11 11:00392
2,4-Dimethylphenol ND ug/kg 1 07/12/11 00:47 105-67-907/08/11 11:00392
Dimethylphthalate ND ug/kg 1 07/12/11 00:47 131-11-307/08/11 11:00392
Di-n-butylphthalate ND ug/kg 1 07/12/11 00:47 84-74-207/08/11 11:00392
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/12/11 00:47 534-52-107/08/11 11:00783
2,4-Dinitrophenol ND ug/kg 1 07/12/11 00:47 51-28-507/08/11 11:001960
2,4-Dinitrotoluene ND ug/kg 1 07/12/11 00:47 121-14-207/08/11 11:00392
2,6-Dinitrotoluene ND ug/kg 1 07/12/11 00:47 606-20-207/08/11 11:00392
Di-n-octylphthalate ND ug/kg 1 07/12/11 00:47 117-84-007/08/11 11:00392
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/12/11 00:47 117-81-707/08/11 11:00392
Fluoranthene ND ug/kg 1 07/12/11 00:47 206-44-007/08/11 11:00392
Fluorene ND ug/kg 1 07/12/11 00:47 86-73-707/08/11 11:00392
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 00:47 87-68-307/08/11 11:00392
Hexachlorobenzene ND ug/kg 1 07/12/11 00:47 118-74-107/08/11 11:00392
Hexachlorocyclopentadiene ND ug/kg 1 07/12/11 00:47 77-47-407/08/11 11:00392
Hexachloroethane ND ug/kg 1 07/12/11 00:47 67-72-107/08/11 11:00392
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/12/11 00:47 193-39-507/08/11 11:00392
Isophorone ND ug/kg 1 07/12/11 00:47 78-59-107/08/11 11:00392
1-Methylnaphthalene ND ug/kg 1 07/12/11 00:47 90-12-007/08/11 11:00392
2-Methylnaphthalene ND ug/kg 1 07/12/11 00:47 91-57-607/08/11 11:00392
2-Methylphenol(o-Cresol)ND ug/kg 1 07/12/11 00:47 95-48-707/08/11 11:00392
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/12/11 00:4707/08/11 11:00392
Naphthalene ND ug/kg 1 07/12/11 00:47 91-20-307/08/11 11:00392
2-Nitroaniline ND ug/kg 1 07/12/11 00:47 88-74-407/08/11 11:001960
3-Nitroaniline ND ug/kg 1 07/12/11 00:47 99-09-207/08/11 11:001960
4-Nitroaniline ND ug/kg 1 07/12/11 00:47 100-01-607/08/11 11:00783
Nitrobenzene ND ug/kg 1 07/12/11 00:47 98-95-307/08/11 11:00392
2-Nitrophenol ND ug/kg 1 07/12/11 00:47 88-75-507/08/11 11:00392
4-Nitrophenol ND ug/kg 1 07/12/11 00:47 100-02-707/08/11 11:001960
N-Nitrosodimethylamine ND ug/kg 1 07/12/11 00:47 62-75-907/08/11 11:00392
N-Nitroso-di-n-propylamine ND ug/kg 1 07/12/11 00:47 621-64-707/08/11 11:00392
N-Nitrosodiphenylamine ND ug/kg 1 07/12/11 00:47 86-30-607/08/11 11:00392
Pentachlorophenol ND ug/kg 1 07/12/11 00:47 87-86-507/08/11 11:001960
Phenanthrene ND ug/kg 1 07/12/11 00:47 85-01-807/08/11 11:00392
Phenol ND ug/kg 1 07/12/11 00:47 108-95-207/08/11 11:00392
Pyrene ND ug/kg 1 07/12/11 00:47 129-00-007/08/11 11:00392
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 00:47 120-82-107/08/11 11:00392
2,4,5-Trichlorophenol ND ug/kg 1 07/12/11 00:47 95-95-407/08/11 11:00392
2,4,6-Trichlorophenol ND ug/kg 1 07/12/11 00:47 88-06-207/08/11 11:00392
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 77 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 7B (9-10)Lab ID:9297694014 Collected:07/06/11 15:50 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)77 %1 07/12/11 00:47 4165-60-007/08/11 11:0023-110
2-Fluorobiphenyl (S)77 %1 07/12/11 00:47 321-60-807/08/11 11:0030-110
Terphenyl-d14 (S)89 %1 07/12/11 00:47 1718-51-007/08/11 11:0028-110
Phenol-d6 (S)58 %1 07/12/11 00:47 13127-88-307/08/11 11:0022-110
2-Fluorophenol (S)63 %1 07/12/11 00:47 367-12-407/08/11 11:0013-110
2,4,6-Tribromophenol (S)71 %1 07/12/11 00:47 118-79-607/08/11 11:0027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/12/11 20:59 67-64-193.3
Benzene ND ug/kg 1 07/12/11 20:59 71-43-24.7
Bromobenzene ND ug/kg 1 07/12/11 20:59 108-86-14.7
Bromochloromethane ND ug/kg 1 07/12/11 20:59 74-97-54.7
Bromodichloromethane ND ug/kg 1 07/12/11 20:59 75-27-44.7
Bromoform ND ug/kg 1 07/12/11 20:59 75-25-24.7
Bromomethane ND ug/kg 1 07/12/11 20:59 74-83-99.3
2-Butanone (MEK)ND ug/kg 1 07/12/11 20:59 78-93-393.3
n-Butylbenzene ND ug/kg 1 07/12/11 20:59 104-51-84.7
sec-Butylbenzene ND ug/kg 1 07/12/11 20:59 135-98-84.7
tert-Butylbenzene ND ug/kg 1 07/12/11 20:59 98-06-64.7
Carbon tetrachloride ND ug/kg 1 07/12/11 20:59 56-23-54.7
Chlorobenzene ND ug/kg 1 07/12/11 20:59 108-90-74.7
Chloroethane ND ug/kg 1 07/12/11 20:59 75-00-39.3
Chloroform ND ug/kg 1 07/12/11 20:59 67-66-34.7
Chloromethane ND ug/kg 1 07/12/11 20:59 74-87-39.3
2-Chlorotoluene ND ug/kg 1 07/12/11 20:59 95-49-84.7
4-Chlorotoluene ND ug/kg 1 07/12/11 20:59 106-43-44.7
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/12/11 20:59 96-12-84.7
Dibromochloromethane ND ug/kg 1 07/12/11 20:59 124-48-14.7
1,2-Dibromoethane (EDB)ND ug/kg 1 07/12/11 20:59 106-93-44.7
Dibromomethane ND ug/kg 1 07/12/11 20:59 74-95-34.7
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 20:59 95-50-14.7
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 20:59 541-73-14.7
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 20:59 106-46-74.7
Dichlorodifluoromethane ND ug/kg 1 07/12/11 20:59 75-71-89.3
1,1-Dichloroethane ND ug/kg 1 07/12/11 20:59 75-34-34.7
1,2-Dichloroethane ND ug/kg 1 07/12/11 20:59 107-06-24.7
1,1-Dichloroethene ND ug/kg 1 07/12/11 20:59 75-35-44.7
cis-1,2-Dichloroethene ND ug/kg 1 07/12/11 20:59 156-59-24.7
trans-1,2-Dichloroethene ND ug/kg 1 07/12/11 20:59 156-60-54.7
1,2-Dichloropropane ND ug/kg 1 07/12/11 20:59 78-87-54.7
1,3-Dichloropropane ND ug/kg 1 07/12/11 20:59 142-28-94.7
2,2-Dichloropropane ND ug/kg 1 07/12/11 20:59 594-20-74.7
1,1-Dichloropropene ND ug/kg 1 07/12/11 20:59 563-58-64.7
cis-1,3-Dichloropropene ND ug/kg 1 07/12/11 20:59 10061-01-54.7
trans-1,3-Dichloropropene ND ug/kg 1 07/12/11 20:59 10061-02-64.7
Diisopropyl ether ND ug/kg 1 07/12/11 20:59 108-20-34.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 78 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 7B (9-10)Lab ID:9297694014 Collected:07/06/11 15:50 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/12/11 20:59 100-41-44.7
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 20:59 87-68-34.7
2-Hexanone ND ug/kg 1 07/12/11 20:59 591-78-646.6
Isopropylbenzene (Cumene)ND ug/kg 1 07/12/11 20:59 98-82-84.7
p-Isopropyltoluene ND ug/kg 1 07/12/11 20:59 99-87-64.7
Methylene Chloride ND ug/kg 1 07/12/11 20:59 75-09-218.7
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/12/11 20:59 108-10-146.6
Methyl-tert-butyl ether ND ug/kg 1 07/12/11 20:59 1634-04-44.7
Naphthalene ND ug/kg 1 07/12/11 20:59 91-20-34.7
n-Propylbenzene ND ug/kg 1 07/12/11 20:59 103-65-14.7
Styrene ND ug/kg 1 07/12/11 20:59 100-42-54.7
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/12/11 20:59 630-20-64.7
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/12/11 20:59 79-34-54.7
Tetrachloroethene ND ug/kg 1 07/12/11 20:59 127-18-44.7
Toluene ND ug/kg 1 07/12/11 20:59 108-88-34.7
1,2,3-Trichlorobenzene ND ug/kg 1 07/12/11 20:59 87-61-64.7
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 20:59 120-82-14.7
1,1,1-Trichloroethane ND ug/kg 1 07/12/11 20:59 71-55-64.7
1,1,2-Trichloroethane ND ug/kg 1 07/12/11 20:59 79-00-54.7
Trichloroethene ND ug/kg 1 07/12/11 20:59 79-01-64.7
Trichlorofluoromethane ND ug/kg 1 07/12/11 20:59 75-69-44.7
1,2,3-Trichloropropane ND ug/kg 1 07/12/11 20:59 96-18-44.7
1,2,4-Trimethylbenzene ND ug/kg 1 07/12/11 20:59 95-63-64.7
1,3,5-Trimethylbenzene ND ug/kg 1 07/12/11 20:59 108-67-84.7
Vinyl acetate ND ug/kg 1 07/12/11 20:59 108-05-446.6
Vinyl chloride ND ug/kg 1 07/12/11 20:59 75-01-49.3
Xylene (Total)ND ug/kg 1 07/12/11 20:59 1330-20-79.3
m&p-Xylene ND ug/kg 1 07/12/11 20:59 179601-23-19.3
o-Xylene ND ug/kg 1 07/12/11 20:59 95-47-64.7
Dibromofluoromethane (S)99 %1 07/12/11 20:59 1868-53-770-130
Toluene-d8 (S)101 %1 07/12/11 20:59 2037-26-570-130
4-Bromofluorobenzene (S)91 %1 07/12/11 20:59 460-00-470-130
1,2-Dichloroethane-d4 (S)81 %1 07/12/11 20:59 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 15.7 %1 07/08/11 08:550.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 79 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 8A (6-7)Lab ID:9297694015 Collected:07/07/11 08:40 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 11.8 mg/kg 1 07/12/11 07:42 68334-30-507/08/11 10:276.0
n-Pentacosane (S)69 %1 07/12/11 07:42 629-99-207/08/11 10:2741-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease ND mg/kg 1 07/11/11 12:0507/11/11 11:2284.1
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/13/11 01:41 8006-61-907/12/11 14:505.9
4-Bromofluorobenzene (S)135 %1 07/13/11 01:41 460-00-407/12/11 14:5070-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 2.8 mg/kg 1 07/14/11 14:42 7440-38-207/12/11 11:400.54
Barium 124 mg/kg 1 07/13/11 20:07 7440-39-307/12/11 11:400.54
Cadmium ND mg/kg 1 07/13/11 20:07 7440-43-907/12/11 11:400.11
Chromium 3.7 mg/kg 1 07/13/11 20:07 7440-47-307/12/11 11:400.54
Lead 17.6 mg/kg 1 07/13/11 20:07 7439-92-107/12/11 11:400.54
Selenium 1.1 mg/kg 1 07/13/11 20:07 7782-49-207/12/11 11:401.1
Silver ND mg/kg 1 07/13/11 20:07 7440-22-407/12/11 11:400.54
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.021 mg/kg 1 07/11/11 18:20 7439-97-607/08/11 15:100.0050
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/12/11 01:14 83-32-907/08/11 11:00396
Acenaphthylene ND ug/kg 1 07/12/11 01:14 208-96-807/08/11 11:00396
Aniline ND ug/kg 1 07/12/11 01:14 62-53-307/08/11 11:00396
Anthracene ND ug/kg 1 07/12/11 01:14 120-12-707/08/11 11:00396
Benzo(a)anthracene ND ug/kg 1 07/12/11 01:14 56-55-307/08/11 11:00396
Benzo(a)pyrene ND ug/kg 1 07/12/11 01:14 50-32-807/08/11 11:00396
Benzo(b)fluoranthene ND ug/kg 1 07/12/11 01:14 205-99-207/08/11 11:00396
Benzo(g,h,i)perylene ND ug/kg 1 07/12/11 01:14 191-24-207/08/11 11:00396
Benzo(k)fluoranthene ND ug/kg 1 07/12/11 01:14 207-08-907/08/11 11:00396
Benzoic Acid ND ug/kg 1 07/12/11 01:14 65-85-007/08/11 11:001980
Benzyl alcohol ND ug/kg 1 07/12/11 01:14 100-51-607/08/11 11:00792
4-Bromophenylphenyl ether ND ug/kg 1 07/12/11 01:14 101-55-307/08/11 11:00396
Butylbenzylphthalate ND ug/kg 1 07/12/11 01:14 85-68-707/08/11 11:00396
4-Chloro-3-methylphenol ND ug/kg 1 07/12/11 01:14 59-50-707/08/11 11:00792
4-Chloroaniline ND ug/kg 1 07/12/11 01:14 106-47-807/08/11 11:001980
bis(2-Chloroethoxy)methane ND ug/kg 1 07/12/11 01:14 111-91-107/08/11 11:00396
bis(2-Chloroethyl) ether ND ug/kg 1 07/12/11 01:14 111-44-407/08/11 11:00396
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/12/11 01:14 108-60-107/08/11 11:00396
2-Chloronaphthalene ND ug/kg 1 07/12/11 01:14 91-58-707/08/11 11:00396
2-Chlorophenol ND ug/kg 1 07/12/11 01:14 95-57-807/08/11 11:00396
4-Chlorophenylphenyl ether ND ug/kg 1 07/12/11 01:14 7005-72-307/08/11 11:00396
Chrysene ND ug/kg 1 07/12/11 01:14 218-01-907/08/11 11:00396
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 80 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 8A (6-7)Lab ID:9297694015 Collected:07/07/11 08:40 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/12/11 01:14 53-70-307/08/11 11:00396
Dibenzofuran ND ug/kg 1 07/12/11 01:14 132-64-907/08/11 11:00396
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 01:14 95-50-107/08/11 11:00396
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 01:14 541-73-107/08/11 11:00396
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 01:14 106-46-707/08/11 11:00396
3,3'-Dichlorobenzidine ND ug/kg 1 07/12/11 01:14 91-94-107/08/11 11:001980
2,4-Dichlorophenol ND ug/kg 1 07/12/11 01:14 120-83-207/08/11 11:00396
Diethylphthalate ND ug/kg 1 07/12/11 01:14 84-66-207/08/11 11:00396
2,4-Dimethylphenol ND ug/kg 1 07/12/11 01:14 105-67-907/08/11 11:00396
Dimethylphthalate ND ug/kg 1 07/12/11 01:14 131-11-307/08/11 11:00396
Di-n-butylphthalate ND ug/kg 1 07/12/11 01:14 84-74-207/08/11 11:00396
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/12/11 01:14 534-52-107/08/11 11:00792
2,4-Dinitrophenol ND ug/kg 1 07/12/11 01:14 51-28-507/08/11 11:001980
2,4-Dinitrotoluene ND ug/kg 1 07/12/11 01:14 121-14-207/08/11 11:00396
2,6-Dinitrotoluene ND ug/kg 1 07/12/11 01:14 606-20-207/08/11 11:00396
Di-n-octylphthalate ND ug/kg 1 07/12/11 01:14 117-84-007/08/11 11:00396
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/12/11 01:14 117-81-707/08/11 11:00396
Fluoranthene ND ug/kg 1 07/12/11 01:14 206-44-007/08/11 11:00396
Fluorene ND ug/kg 1 07/12/11 01:14 86-73-707/08/11 11:00396
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 01:14 87-68-307/08/11 11:00396
Hexachlorobenzene ND ug/kg 1 07/12/11 01:14 118-74-107/08/11 11:00396
Hexachlorocyclopentadiene ND ug/kg 1 07/12/11 01:14 77-47-407/08/11 11:00396
Hexachloroethane ND ug/kg 1 07/12/11 01:14 67-72-107/08/11 11:00396
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/12/11 01:14 193-39-507/08/11 11:00396
Isophorone ND ug/kg 1 07/12/11 01:14 78-59-107/08/11 11:00396
1-Methylnaphthalene ND ug/kg 1 07/12/11 01:14 90-12-007/08/11 11:00396
2-Methylnaphthalene ND ug/kg 1 07/12/11 01:14 91-57-607/08/11 11:00396
2-Methylphenol(o-Cresol)ND ug/kg 1 07/12/11 01:14 95-48-707/08/11 11:00396
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/12/11 01:1407/08/11 11:00396
Naphthalene ND ug/kg 1 07/12/11 01:14 91-20-307/08/11 11:00396
2-Nitroaniline ND ug/kg 1 07/12/11 01:14 88-74-407/08/11 11:001980
3-Nitroaniline ND ug/kg 1 07/12/11 01:14 99-09-207/08/11 11:001980
4-Nitroaniline ND ug/kg 1 07/12/11 01:14 100-01-607/08/11 11:00792
Nitrobenzene ND ug/kg 1 07/12/11 01:14 98-95-307/08/11 11:00396
2-Nitrophenol ND ug/kg 1 07/12/11 01:14 88-75-507/08/11 11:00396
4-Nitrophenol ND ug/kg 1 07/12/11 01:14 100-02-707/08/11 11:001980
N-Nitrosodimethylamine ND ug/kg 1 07/12/11 01:14 62-75-907/08/11 11:00396
N-Nitroso-di-n-propylamine ND ug/kg 1 07/12/11 01:14 621-64-707/08/11 11:00396
N-Nitrosodiphenylamine ND ug/kg 1 07/12/11 01:14 86-30-607/08/11 11:00396
Pentachlorophenol ND ug/kg 1 07/12/11 01:14 87-86-507/08/11 11:001980
Phenanthrene ND ug/kg 1 07/12/11 01:14 85-01-807/08/11 11:00396
Phenol ND ug/kg 1 07/12/11 01:14 108-95-207/08/11 11:00396
Pyrene ND ug/kg 1 07/12/11 01:14 129-00-007/08/11 11:00396
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 01:14 120-82-107/08/11 11:00396
2,4,5-Trichlorophenol ND ug/kg 1 07/12/11 01:14 95-95-407/08/11 11:00396
2,4,6-Trichlorophenol ND ug/kg 1 07/12/11 01:14 88-06-207/08/11 11:00396
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 81 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 8A (6-7)Lab ID:9297694015 Collected:07/07/11 08:40 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)64 %1 07/12/11 01:14 4165-60-007/08/11 11:0023-110
2-Fluorobiphenyl (S)70 %1 07/12/11 01:14 321-60-807/08/11 11:0030-110
Terphenyl-d14 (S)66 %1 07/12/11 01:14 1718-51-007/08/11 11:0028-110
Phenol-d6 (S)49 %1 07/12/11 01:14 13127-88-307/08/11 11:0022-110
2-Fluorophenol (S)52 %1 07/12/11 01:14 367-12-407/08/11 11:0013-110
2,4,6-Tribromophenol (S)62 %1 07/12/11 01:14 118-79-607/08/11 11:0027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/12/11 21:19 67-64-1114
Benzene ND ug/kg 1 07/12/11 21:19 71-43-25.7
Bromobenzene ND ug/kg 1 07/12/11 21:19 108-86-15.7
Bromochloromethane ND ug/kg 1 07/12/11 21:19 74-97-55.7
Bromodichloromethane ND ug/kg 1 07/12/11 21:19 75-27-45.7
Bromoform ND ug/kg 1 07/12/11 21:19 75-25-25.7
Bromomethane ND ug/kg 1 07/12/11 21:19 74-83-911.4
2-Butanone (MEK)ND ug/kg 1 07/12/11 21:19 78-93-3114
n-Butylbenzene ND ug/kg 1 07/12/11 21:19 104-51-85.7
sec-Butylbenzene ND ug/kg 1 07/12/11 21:19 135-98-85.7
tert-Butylbenzene ND ug/kg 1 07/12/11 21:19 98-06-65.7
Carbon tetrachloride ND ug/kg 1 07/12/11 21:19 56-23-55.7
Chlorobenzene ND ug/kg 1 07/12/11 21:19 108-90-75.7
Chloroethane ND ug/kg 1 07/12/11 21:19 75-00-311.4
Chloroform ND ug/kg 1 07/12/11 21:19 67-66-35.7
Chloromethane ND ug/kg 1 07/12/11 21:19 74-87-311.4
2-Chlorotoluene ND ug/kg 1 07/12/11 21:19 95-49-85.7
4-Chlorotoluene ND ug/kg 1 07/12/11 21:19 106-43-45.7
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/12/11 21:19 96-12-85.7
Dibromochloromethane ND ug/kg 1 07/12/11 21:19 124-48-15.7
1,2-Dibromoethane (EDB)ND ug/kg 1 07/12/11 21:19 106-93-45.7
Dibromomethane ND ug/kg 1 07/12/11 21:19 74-95-35.7
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 21:19 95-50-15.7
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 21:19 541-73-15.7
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 21:19 106-46-75.7
Dichlorodifluoromethane ND ug/kg 1 07/12/11 21:19 75-71-811.4
1,1-Dichloroethane ND ug/kg 1 07/12/11 21:19 75-34-35.7
1,2-Dichloroethane ND ug/kg 1 07/12/11 21:19 107-06-25.7
1,1-Dichloroethene ND ug/kg 1 07/12/11 21:19 75-35-45.7
cis-1,2-Dichloroethene ND ug/kg 1 07/12/11 21:19 156-59-25.7
trans-1,2-Dichloroethene ND ug/kg 1 07/12/11 21:19 156-60-55.7
1,2-Dichloropropane ND ug/kg 1 07/12/11 21:19 78-87-55.7
1,3-Dichloropropane ND ug/kg 1 07/12/11 21:19 142-28-95.7
2,2-Dichloropropane ND ug/kg 1 07/12/11 21:19 594-20-75.7
1,1-Dichloropropene ND ug/kg 1 07/12/11 21:19 563-58-65.7
cis-1,3-Dichloropropene ND ug/kg 1 07/12/11 21:19 10061-01-55.7
trans-1,3-Dichloropropene ND ug/kg 1 07/12/11 21:19 10061-02-65.7
Diisopropyl ether ND ug/kg 1 07/12/11 21:19 108-20-35.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 82 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 8A (6-7)Lab ID:9297694015 Collected:07/07/11 08:40 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/12/11 21:19 100-41-45.7
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 21:19 87-68-35.7
2-Hexanone ND ug/kg 1 07/12/11 21:19 591-78-657.1
Isopropylbenzene (Cumene)ND ug/kg 1 07/12/11 21:19 98-82-85.7
p-Isopropyltoluene ND ug/kg 1 07/12/11 21:19 99-87-65.7
Methylene Chloride ND ug/kg 1 07/12/11 21:19 75-09-222.8
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/12/11 21:19 108-10-157.1
Methyl-tert-butyl ether ND ug/kg 1 07/12/11 21:19 1634-04-45.7
Naphthalene ND ug/kg 1 07/12/11 21:19 91-20-35.7
n-Propylbenzene ND ug/kg 1 07/12/11 21:19 103-65-15.7
Styrene ND ug/kg 1 07/12/11 21:19 100-42-55.7
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/12/11 21:19 630-20-65.7
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/12/11 21:19 79-34-55.7
Tetrachloroethene ND ug/kg 1 07/12/11 21:19 127-18-45.7
Toluene ND ug/kg 1 07/12/11 21:19 108-88-35.7
1,2,3-Trichlorobenzene ND ug/kg 1 07/12/11 21:19 87-61-65.7
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 21:19 120-82-15.7
1,1,1-Trichloroethane ND ug/kg 1 07/12/11 21:19 71-55-65.7
1,1,2-Trichloroethane ND ug/kg 1 07/12/11 21:19 79-00-55.7
Trichloroethene ND ug/kg 1 07/12/11 21:19 79-01-65.7
Trichlorofluoromethane ND ug/kg 1 07/12/11 21:19 75-69-45.7
1,2,3-Trichloropropane ND ug/kg 1 07/12/11 21:19 96-18-45.7
1,2,4-Trimethylbenzene ND ug/kg 1 07/12/11 21:19 95-63-65.7
1,3,5-Trimethylbenzene ND ug/kg 1 07/12/11 21:19 108-67-85.7
Vinyl acetate ND ug/kg 1 07/12/11 21:19 108-05-457.1
Vinyl chloride ND ug/kg 1 07/12/11 21:19 75-01-411.4
Xylene (Total)ND ug/kg 1 07/12/11 21:19 1330-20-711.4
m&p-Xylene ND ug/kg 1 07/12/11 21:19 179601-23-111.4
o-Xylene ND ug/kg 1 07/12/11 21:19 95-47-65.7
Dibromofluoromethane (S)92 %1 07/12/11 21:19 1868-53-770-130
Toluene-d8 (S)99 %1 07/12/11 21:19 2037-26-570-130
4-Bromofluorobenzene (S)94 %1 07/12/11 21:19 460-00-470-130
1,2-Dichloroethane-d4 (S)85 %1 07/12/11 21:19 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 16.7 %1 07/08/11 08:550.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 83 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 8B (13-14)Lab ID:9297694016 Collected:07/07/11 09:00 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 105 mg/kg 1 07/12/11 08:10 68334-30-507/08/11 10:276.1
n-Pentacosane (S)78 %1 07/12/11 08:10 629-99-207/08/11 10:2741-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease 174 mg/kg 1 07/11/11 12:0607/11/11 11:2285.2
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/13/11 02:06 8006-61-907/12/11 14:505.2
4-Bromofluorobenzene (S)160 %1 07/13/11 02:06 460-00-407/12/11 14:5070-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 3.3 mg/kg 1 07/14/11 14:46 7440-38-207/12/11 11:400.51
Barium 54.1 mg/kg 1 07/13/11 20:11 7440-39-307/12/11 11:400.51
Cadmium ND mg/kg 1 07/13/11 20:11 7440-43-907/12/11 11:400.10
Chromium 4.8 mg/kg 1 07/13/11 20:11 7440-47-307/12/11 11:400.51
Lead 94.6 mg/kg 1 07/13/11 20:11 7439-92-107/12/11 11:400.51
Selenium ND mg/kg 1 07/13/11 20:11 7782-49-207/12/11 11:401.0
Silver ND mg/kg 1 07/13/11 20:11 7440-22-407/12/11 11:400.51
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.045 mg/kg 1 07/11/11 18:23 7439-97-607/08/11 15:100.0055
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/12/11 16:58 83-32-907/08/11 11:00402
Acenaphthylene ND ug/kg 1 07/12/11 16:58 208-96-807/08/11 11:00402
Aniline ND ug/kg 1 07/12/11 16:58 62-53-307/08/11 11:00402
Anthracene ND ug/kg 1 07/12/11 16:58 120-12-707/08/11 11:00402
Benzo(a)anthracene ND ug/kg 1 07/12/11 16:58 56-55-307/08/11 11:00402
Benzo(a)pyrene ND ug/kg 1 07/12/11 16:58 50-32-807/08/11 11:00402
Benzo(b)fluoranthene ND ug/kg 1 07/12/11 16:58 205-99-207/08/11 11:00402
Benzo(g,h,i)perylene ND ug/kg 1 07/12/11 16:58 191-24-207/08/11 11:00402
Benzo(k)fluoranthene ND ug/kg 1 07/12/11 16:58 207-08-907/08/11 11:00402
Benzoic Acid ND ug/kg 1 07/12/11 16:58 65-85-007/08/11 11:002010
Benzyl alcohol ND ug/kg 1 07/12/11 16:58 100-51-607/08/11 11:00803
4-Bromophenylphenyl ether ND ug/kg 1 07/12/11 16:58 101-55-307/08/11 11:00402
Butylbenzylphthalate ND ug/kg 1 07/12/11 16:58 85-68-707/08/11 11:00402
4-Chloro-3-methylphenol ND ug/kg 1 07/12/11 16:58 59-50-707/08/11 11:00803
4-Chloroaniline ND ug/kg 1 07/12/11 16:58 106-47-807/08/11 11:002010
bis(2-Chloroethoxy)methane ND ug/kg 1 07/12/11 16:58 111-91-107/08/11 11:00402
bis(2-Chloroethyl) ether ND ug/kg 1 07/12/11 16:58 111-44-407/08/11 11:00402
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/12/11 16:58 108-60-107/08/11 11:00402
2-Chloronaphthalene ND ug/kg 1 07/12/11 16:58 91-58-707/08/11 11:00402
2-Chlorophenol ND ug/kg 1 07/12/11 16:58 95-57-807/08/11 11:00402
4-Chlorophenylphenyl ether ND ug/kg 1 07/12/11 16:58 7005-72-307/08/11 11:00402
Chrysene ND ug/kg 1 07/12/11 16:58 218-01-907/08/11 11:00402
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 84 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 8B (13-14)Lab ID:9297694016 Collected:07/07/11 09:00 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/12/11 16:58 53-70-307/08/11 11:00402
Dibenzofuran ND ug/kg 1 07/12/11 16:58 132-64-907/08/11 11:00402
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 16:58 95-50-107/08/11 11:00402
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 16:58 541-73-107/08/11 11:00402
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 16:58 106-46-707/08/11 11:00402
3,3'-Dichlorobenzidine ND ug/kg 1 07/12/11 16:58 91-94-107/08/11 11:002010
2,4-Dichlorophenol ND ug/kg 1 07/12/11 16:58 120-83-207/08/11 11:00402
Diethylphthalate ND ug/kg 1 07/12/11 16:58 84-66-207/08/11 11:00402
2,4-Dimethylphenol ND ug/kg 1 07/12/11 16:58 105-67-907/08/11 11:00402
Dimethylphthalate ND ug/kg 1 07/12/11 16:58 131-11-307/08/11 11:00402
Di-n-butylphthalate ND ug/kg 1 07/12/11 16:58 84-74-207/08/11 11:00402
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/12/11 16:58 534-52-107/08/11 11:00803
2,4-Dinitrophenol ND ug/kg 1 07/12/11 16:58 51-28-507/08/11 11:002010
2,4-Dinitrotoluene ND ug/kg 1 07/12/11 16:58 121-14-207/08/11 11:00402
2,6-Dinitrotoluene ND ug/kg 1 07/12/11 16:58 606-20-207/08/11 11:00402
Di-n-octylphthalate ND ug/kg 1 07/12/11 16:58 117-84-007/08/11 11:00402
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/12/11 16:58 117-81-707/08/11 11:00402
Fluoranthene ND ug/kg 1 07/12/11 16:58 206-44-007/08/11 11:00402
Fluorene ND ug/kg 1 07/12/11 16:58 86-73-707/08/11 11:00402
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 16:58 87-68-307/08/11 11:00402
Hexachlorobenzene ND ug/kg 1 07/12/11 16:58 118-74-107/08/11 11:00402
Hexachlorocyclopentadiene ND ug/kg 1 07/12/11 16:58 77-47-407/08/11 11:00402
Hexachloroethane ND ug/kg 1 07/12/11 16:58 67-72-107/08/11 11:00402
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/12/11 16:58 193-39-507/08/11 11:00402
Isophorone ND ug/kg 1 07/12/11 16:58 78-59-107/08/11 11:00402
1-Methylnaphthalene ND ug/kg 1 07/12/11 16:58 90-12-007/08/11 11:00402
2-Methylnaphthalene ND ug/kg 1 07/12/11 16:58 91-57-607/08/11 11:00402
2-Methylphenol(o-Cresol)ND ug/kg 1 07/12/11 16:58 95-48-707/08/11 11:00402
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/12/11 16:5807/08/11 11:00402
Naphthalene ND ug/kg 1 07/12/11 16:58 91-20-307/08/11 11:00402
2-Nitroaniline ND ug/kg 1 07/12/11 16:58 88-74-407/08/11 11:002010
3-Nitroaniline ND ug/kg 1 07/12/11 16:58 99-09-207/08/11 11:002010
4-Nitroaniline ND ug/kg 1 07/12/11 16:58 100-01-607/08/11 11:00803
Nitrobenzene ND ug/kg 1 07/12/11 16:58 98-95-307/08/11 11:00402
2-Nitrophenol ND ug/kg 1 07/12/11 16:58 88-75-507/08/11 11:00402
4-Nitrophenol ND ug/kg 1 07/12/11 16:58 100-02-707/08/11 11:002010
N-Nitrosodimethylamine ND ug/kg 1 07/12/11 16:58 62-75-907/08/11 11:00402
N-Nitroso-di-n-propylamine ND ug/kg 1 07/12/11 16:58 621-64-707/08/11 11:00402
N-Nitrosodiphenylamine ND ug/kg 1 07/12/11 16:58 86-30-607/08/11 11:00402
Pentachlorophenol ND ug/kg 1 07/12/11 16:58 87-86-507/08/11 11:002010
Phenanthrene ND ug/kg 1 07/12/11 16:58 85-01-807/08/11 11:00402
Phenol ND ug/kg 1 07/12/11 16:58 108-95-207/08/11 11:00402
Pyrene ND ug/kg 1 07/12/11 16:58 129-00-007/08/11 11:00402
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 16:58 120-82-107/08/11 11:00402
2,4,5-Trichlorophenol ND ug/kg 1 07/12/11 16:58 95-95-407/08/11 11:00402
2,4,6-Trichlorophenol ND ug/kg 1 07/12/11 16:58 88-06-207/08/11 11:00402
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 85 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 8B (13-14)Lab ID:9297694016 Collected:07/07/11 09:00 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)38 %1 07/12/11 16:58 4165-60-007/08/11 11:0023-110
2-Fluorobiphenyl (S)67 %1 07/12/11 16:58 321-60-807/08/11 11:0030-110
Terphenyl-d14 (S)69 %1 07/12/11 16:58 1718-51-007/08/11 11:0028-110
Phenol-d6 (S)52 %1 07/12/11 16:58 13127-88-307/08/11 11:0022-110
2-Fluorophenol (S)56 %1 07/12/11 16:58 367-12-407/08/11 11:0013-110
2,4,6-Tribromophenol (S)74 %1 07/12/11 16:58 118-79-607/08/11 11:0027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/13/11 18:14 67-64-183.6
Benzene ND ug/kg 1 07/13/11 18:14 71-43-24.2
Bromobenzene ND ug/kg 1 07/13/11 18:14 108-86-14.2
Bromochloromethane ND ug/kg 1 07/13/11 18:14 74-97-54.2
Bromodichloromethane ND ug/kg 1 07/13/11 18:14 75-27-44.2
Bromoform ND ug/kg 1 07/13/11 18:14 75-25-24.2
Bromomethane ND ug/kg 1 07/13/11 18:14 74-83-98.4
2-Butanone (MEK)ND ug/kg 1 07/13/11 18:14 78-93-383.6
n-Butylbenzene ND ug/kg 1 07/13/11 18:14 104-51-84.2
sec-Butylbenzene ND ug/kg 1 07/13/11 18:14 135-98-84.2
tert-Butylbenzene ND ug/kg 1 07/13/11 18:14 98-06-64.2
Carbon tetrachloride ND ug/kg 1 07/13/11 18:14 56-23-54.2
Chlorobenzene ND ug/kg 1 07/13/11 18:14 108-90-74.2
Chloroethane ND ug/kg 1 07/13/11 18:14 75-00-38.4
Chloroform ND ug/kg 1 07/13/11 18:14 67-66-34.2
Chloromethane ND ug/kg 1 07/13/11 18:14 74-87-38.4
2-Chlorotoluene ND ug/kg 1 07/13/11 18:14 95-49-84.2
4-Chlorotoluene ND ug/kg 1 07/13/11 18:14 106-43-44.2
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/13/11 18:14 96-12-84.2
Dibromochloromethane ND ug/kg 1 07/13/11 18:14 124-48-14.2
1,2-Dibromoethane (EDB)ND ug/kg 1 07/13/11 18:14 106-93-44.2
Dibromomethane ND ug/kg 1 07/13/11 18:14 74-95-34.2
1,2-Dichlorobenzene ND ug/kg 1 07/13/11 18:14 95-50-14.2
1,3-Dichlorobenzene ND ug/kg 1 07/13/11 18:14 541-73-14.2
1,4-Dichlorobenzene ND ug/kg 1 07/13/11 18:14 106-46-74.2
Dichlorodifluoromethane ND ug/kg 1 07/13/11 18:14 75-71-8 1g8.4
1,1-Dichloroethane ND ug/kg 1 07/13/11 18:14 75-34-34.2
1,2-Dichloroethane ND ug/kg 1 07/13/11 18:14 107-06-24.2
1,1-Dichloroethene ND ug/kg 1 07/13/11 18:14 75-35-44.2
cis-1,2-Dichloroethene ND ug/kg 1 07/13/11 18:14 156-59-24.2
trans-1,2-Dichloroethene ND ug/kg 1 07/13/11 18:14 156-60-54.2
1,2-Dichloropropane ND ug/kg 1 07/13/11 18:14 78-87-54.2
1,3-Dichloropropane ND ug/kg 1 07/13/11 18:14 142-28-94.2
2,2-Dichloropropane ND ug/kg 1 07/13/11 18:14 594-20-74.2
1,1-Dichloropropene ND ug/kg 1 07/13/11 18:14 563-58-64.2
cis-1,3-Dichloropropene ND ug/kg 1 07/13/11 18:14 10061-01-54.2
trans-1,3-Dichloropropene ND ug/kg 1 07/13/11 18:14 10061-02-64.2
Diisopropyl ether ND ug/kg 1 07/13/11 18:14 108-20-34.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 86 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 8B (13-14)Lab ID:9297694016 Collected:07/07/11 09:00 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/13/11 18:14 100-41-44.2
Hexachloro-1,3-butadiene ND ug/kg 1 07/13/11 18:14 87-68-34.2
2-Hexanone ND ug/kg 1 07/13/11 18:14 591-78-641.8
Isopropylbenzene (Cumene)ND ug/kg 1 07/13/11 18:14 98-82-84.2
p-Isopropyltoluene ND ug/kg 1 07/13/11 18:14 99-87-64.2
Methylene Chloride ND ug/kg 1 07/13/11 18:14 75-09-216.7
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/13/11 18:14 108-10-141.8
Methyl-tert-butyl ether ND ug/kg 1 07/13/11 18:14 1634-04-44.2
Naphthalene ND ug/kg 1 07/13/11 18:14 91-20-34.2
n-Propylbenzene ND ug/kg 1 07/13/11 18:14 103-65-14.2
Styrene ND ug/kg 1 07/13/11 18:14 100-42-54.2
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/13/11 18:14 630-20-64.2
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/13/11 18:14 79-34-54.2
Tetrachloroethene ND ug/kg 1 07/13/11 18:14 127-18-44.2
Toluene ND ug/kg 1 07/13/11 18:14 108-88-34.2
1,2,3-Trichlorobenzene ND ug/kg 1 07/13/11 18:14 87-61-64.2
1,2,4-Trichlorobenzene ND ug/kg 1 07/13/11 18:14 120-82-14.2
1,1,1-Trichloroethane ND ug/kg 1 07/13/11 18:14 71-55-64.2
1,1,2-Trichloroethane ND ug/kg 1 07/13/11 18:14 79-00-54.2
Trichloroethene ND ug/kg 1 07/13/11 18:14 79-01-64.2
Trichlorofluoromethane ND ug/kg 1 07/13/11 18:14 75-69-44.2
1,2,3-Trichloropropane ND ug/kg 1 07/13/11 18:14 96-18-44.2
1,2,4-Trimethylbenzene ND ug/kg 1 07/13/11 18:14 95-63-64.2
1,3,5-Trimethylbenzene ND ug/kg 1 07/13/11 18:14 108-67-84.2
Vinyl acetate ND ug/kg 1 07/13/11 18:14 108-05-441.8
Vinyl chloride ND ug/kg 1 07/13/11 18:14 75-01-48.4
Xylene (Total)ND ug/kg 1 07/13/11 18:14 1330-20-78.4
m&p-Xylene ND ug/kg 1 07/13/11 18:14 179601-23-18.4
o-Xylene ND ug/kg 1 07/13/11 18:14 95-47-64.2
Dibromofluoromethane (S)99 %1 07/13/11 18:14 1868-53-770-130
Toluene-d8 (S)92 %1 07/13/11 18:14 2037-26-570-130
4-Bromofluorobenzene (S)91 %1 07/13/11 18:14 460-00-470-130
1,2-Dichloroethane-d4 (S)97 %1 07/13/11 18:14 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 17.8 %1 07/08/11 08:590.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 87 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 9A (4-6)Lab ID:9297694017 Collected:07/07/11 10:30 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 7.9 mg/kg 1 07/12/11 08:10 68334-30-507/08/11 10:275.8
n-Pentacosane (S)73 %1 07/12/11 08:10 629-99-207/08/11 10:2741-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease ND mg/kg 1 07/11/11 12:0607/11/11 11:2381.3
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/13/11 02:31 8006-61-907/12/11 14:505.9
4-Bromofluorobenzene (S)135 %1 07/13/11 02:31 460-00-407/12/11 14:5070-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 2.9 mg/kg 1 07/14/11 14:50 7440-38-207/12/11 11:400.50
Barium 100 mg/kg 1 07/13/11 20:15 7440-39-307/12/11 11:400.50
Cadmium ND mg/kg 1 07/13/11 20:15 7440-43-907/12/11 11:400.10
Chromium 3.3 mg/kg 1 07/13/11 20:15 7440-47-307/12/11 11:400.50
Lead 15.1 mg/kg 1 07/13/11 20:15 7439-92-107/12/11 11:400.50
Selenium ND mg/kg 1 07/13/11 20:15 7782-49-207/12/11 11:401.0
Silver ND mg/kg 1 07/13/11 20:15 7440-22-407/12/11 11:400.50
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.015 mg/kg 1 07/11/11 18:26 7439-97-607/08/11 15:100.0050
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/12/11 01:42 83-32-907/08/11 11:00383
Acenaphthylene ND ug/kg 1 07/12/11 01:42 208-96-807/08/11 11:00383
Aniline ND ug/kg 1 07/12/11 01:42 62-53-307/08/11 11:00383
Anthracene ND ug/kg 1 07/12/11 01:42 120-12-707/08/11 11:00383
Benzo(a)anthracene ND ug/kg 1 07/12/11 01:42 56-55-307/08/11 11:00383
Benzo(a)pyrene ND ug/kg 1 07/12/11 01:42 50-32-807/08/11 11:00383
Benzo(b)fluoranthene ND ug/kg 1 07/12/11 01:42 205-99-207/08/11 11:00383
Benzo(g,h,i)perylene ND ug/kg 1 07/12/11 01:42 191-24-207/08/11 11:00383
Benzo(k)fluoranthene ND ug/kg 1 07/12/11 01:42 207-08-907/08/11 11:00383
Benzoic Acid ND ug/kg 1 07/12/11 01:42 65-85-007/08/11 11:001920
Benzyl alcohol ND ug/kg 1 07/12/11 01:42 100-51-607/08/11 11:00766
4-Bromophenylphenyl ether ND ug/kg 1 07/12/11 01:42 101-55-307/08/11 11:00383
Butylbenzylphthalate ND ug/kg 1 07/12/11 01:42 85-68-707/08/11 11:00383
4-Chloro-3-methylphenol ND ug/kg 1 07/12/11 01:42 59-50-707/08/11 11:00766
4-Chloroaniline ND ug/kg 1 07/12/11 01:42 106-47-807/08/11 11:001920
bis(2-Chloroethoxy)methane ND ug/kg 1 07/12/11 01:42 111-91-107/08/11 11:00383
bis(2-Chloroethyl) ether ND ug/kg 1 07/12/11 01:42 111-44-407/08/11 11:00383
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/12/11 01:42 108-60-107/08/11 11:00383
2-Chloronaphthalene ND ug/kg 1 07/12/11 01:42 91-58-707/08/11 11:00383
2-Chlorophenol ND ug/kg 1 07/12/11 01:42 95-57-807/08/11 11:00383
4-Chlorophenylphenyl ether ND ug/kg 1 07/12/11 01:42 7005-72-307/08/11 11:00383
Chrysene ND ug/kg 1 07/12/11 01:42 218-01-907/08/11 11:00383
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 88 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 9A (4-6)Lab ID:9297694017 Collected:07/07/11 10:30 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/12/11 01:42 53-70-307/08/11 11:00383
Dibenzofuran ND ug/kg 1 07/12/11 01:42 132-64-907/08/11 11:00383
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 01:42 95-50-107/08/11 11:00383
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 01:42 541-73-107/08/11 11:00383
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 01:42 106-46-707/08/11 11:00383
3,3'-Dichlorobenzidine ND ug/kg 1 07/12/11 01:42 91-94-107/08/11 11:001920
2,4-Dichlorophenol ND ug/kg 1 07/12/11 01:42 120-83-207/08/11 11:00383
Diethylphthalate ND ug/kg 1 07/12/11 01:42 84-66-207/08/11 11:00383
2,4-Dimethylphenol ND ug/kg 1 07/12/11 01:42 105-67-907/08/11 11:00383
Dimethylphthalate ND ug/kg 1 07/12/11 01:42 131-11-307/08/11 11:00383
Di-n-butylphthalate ND ug/kg 1 07/12/11 01:42 84-74-207/08/11 11:00383
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/12/11 01:42 534-52-107/08/11 11:00766
2,4-Dinitrophenol ND ug/kg 1 07/12/11 01:42 51-28-507/08/11 11:001920
2,4-Dinitrotoluene ND ug/kg 1 07/12/11 01:42 121-14-207/08/11 11:00383
2,6-Dinitrotoluene ND ug/kg 1 07/12/11 01:42 606-20-207/08/11 11:00383
Di-n-octylphthalate ND ug/kg 1 07/12/11 01:42 117-84-007/08/11 11:00383
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/12/11 01:42 117-81-707/08/11 11:00383
Fluoranthene ND ug/kg 1 07/12/11 01:42 206-44-007/08/11 11:00383
Fluorene ND ug/kg 1 07/12/11 01:42 86-73-707/08/11 11:00383
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 01:42 87-68-307/08/11 11:00383
Hexachlorobenzene ND ug/kg 1 07/12/11 01:42 118-74-107/08/11 11:00383
Hexachlorocyclopentadiene ND ug/kg 1 07/12/11 01:42 77-47-407/08/11 11:00383
Hexachloroethane ND ug/kg 1 07/12/11 01:42 67-72-107/08/11 11:00383
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/12/11 01:42 193-39-507/08/11 11:00383
Isophorone ND ug/kg 1 07/12/11 01:42 78-59-107/08/11 11:00383
1-Methylnaphthalene ND ug/kg 1 07/12/11 01:42 90-12-007/08/11 11:00383
2-Methylnaphthalene ND ug/kg 1 07/12/11 01:42 91-57-607/08/11 11:00383
2-Methylphenol(o-Cresol)ND ug/kg 1 07/12/11 01:42 95-48-707/08/11 11:00383
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/12/11 01:4207/08/11 11:00383
Naphthalene ND ug/kg 1 07/12/11 01:42 91-20-307/08/11 11:00383
2-Nitroaniline ND ug/kg 1 07/12/11 01:42 88-74-407/08/11 11:001920
3-Nitroaniline ND ug/kg 1 07/12/11 01:42 99-09-207/08/11 11:001920
4-Nitroaniline ND ug/kg 1 07/12/11 01:42 100-01-607/08/11 11:00766
Nitrobenzene ND ug/kg 1 07/12/11 01:42 98-95-307/08/11 11:00383
2-Nitrophenol ND ug/kg 1 07/12/11 01:42 88-75-507/08/11 11:00383
4-Nitrophenol ND ug/kg 1 07/12/11 01:42 100-02-707/08/11 11:001920
N-Nitrosodimethylamine ND ug/kg 1 07/12/11 01:42 62-75-907/08/11 11:00383
N-Nitroso-di-n-propylamine ND ug/kg 1 07/12/11 01:42 621-64-707/08/11 11:00383
N-Nitrosodiphenylamine ND ug/kg 1 07/12/11 01:42 86-30-607/08/11 11:00383
Pentachlorophenol ND ug/kg 1 07/12/11 01:42 87-86-507/08/11 11:001920
Phenanthrene ND ug/kg 1 07/12/11 01:42 85-01-807/08/11 11:00383
Phenol ND ug/kg 1 07/12/11 01:42 108-95-207/08/11 11:00383
Pyrene ND ug/kg 1 07/12/11 01:42 129-00-007/08/11 11:00383
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 01:42 120-82-107/08/11 11:00383
2,4,5-Trichlorophenol ND ug/kg 1 07/12/11 01:42 95-95-407/08/11 11:00383
2,4,6-Trichlorophenol ND ug/kg 1 07/12/11 01:42 88-06-207/08/11 11:00383
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 89 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 9A (4-6)Lab ID:9297694017 Collected:07/07/11 10:30 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)70 %1 07/12/11 01:42 4165-60-007/08/11 11:0023-110
2-Fluorobiphenyl (S)71 %1 07/12/11 01:42 321-60-807/08/11 11:0030-110
Terphenyl-d14 (S)83 %1 07/12/11 01:42 1718-51-007/08/11 11:0028-110
Phenol-d6 (S)54 %1 07/12/11 01:42 13127-88-307/08/11 11:0022-110
2-Fluorophenol (S)56 %1 07/12/11 01:42 367-12-407/08/11 11:0013-110
2,4,6-Tribromophenol (S)69 %1 07/12/11 01:42 118-79-607/08/11 11:0027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/13/11 00:40 67-64-192.7
Benzene ND ug/kg 1 07/13/11 00:40 71-43-24.6
Bromobenzene ND ug/kg 1 07/13/11 00:40 108-86-14.6
Bromochloromethane ND ug/kg 1 07/13/11 00:40 74-97-54.6
Bromodichloromethane ND ug/kg 1 07/13/11 00:40 75-27-44.6
Bromoform ND ug/kg 1 07/13/11 00:40 75-25-24.6
Bromomethane ND ug/kg 1 07/13/11 00:40 74-83-99.3
2-Butanone (MEK)ND ug/kg 1 07/13/11 00:40 78-93-392.7
n-Butylbenzene ND ug/kg 1 07/13/11 00:40 104-51-84.6
sec-Butylbenzene ND ug/kg 1 07/13/11 00:40 135-98-84.6
tert-Butylbenzene ND ug/kg 1 07/13/11 00:40 98-06-64.6
Carbon tetrachloride ND ug/kg 1 07/13/11 00:40 56-23-54.6
Chlorobenzene ND ug/kg 1 07/13/11 00:40 108-90-74.6
Chloroethane ND ug/kg 1 07/13/11 00:40 75-00-39.3
Chloroform ND ug/kg 1 07/13/11 00:40 67-66-34.6
Chloromethane ND ug/kg 1 07/13/11 00:40 74-87-39.3
2-Chlorotoluene ND ug/kg 1 07/13/11 00:40 95-49-84.6
4-Chlorotoluene ND ug/kg 1 07/13/11 00:40 106-43-44.6
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/13/11 00:40 96-12-84.6
Dibromochloromethane ND ug/kg 1 07/13/11 00:40 124-48-14.6
1,2-Dibromoethane (EDB)ND ug/kg 1 07/13/11 00:40 106-93-44.6
Dibromomethane ND ug/kg 1 07/13/11 00:40 74-95-34.6
1,2-Dichlorobenzene ND ug/kg 1 07/13/11 00:40 95-50-14.6
1,3-Dichlorobenzene ND ug/kg 1 07/13/11 00:40 541-73-14.6
1,4-Dichlorobenzene ND ug/kg 1 07/13/11 00:40 106-46-74.6
Dichlorodifluoromethane ND ug/kg 1 07/13/11 00:40 75-71-89.3
1,1-Dichloroethane ND ug/kg 1 07/13/11 00:40 75-34-34.6
1,2-Dichloroethane ND ug/kg 1 07/13/11 00:40 107-06-24.6
1,1-Dichloroethene ND ug/kg 1 07/13/11 00:40 75-35-44.6
cis-1,2-Dichloroethene ND ug/kg 1 07/13/11 00:40 156-59-24.6
trans-1,2-Dichloroethene ND ug/kg 1 07/13/11 00:40 156-60-54.6
1,2-Dichloropropane ND ug/kg 1 07/13/11 00:40 78-87-54.6
1,3-Dichloropropane ND ug/kg 1 07/13/11 00:40 142-28-94.6
2,2-Dichloropropane ND ug/kg 1 07/13/11 00:40 594-20-74.6
1,1-Dichloropropene ND ug/kg 1 07/13/11 00:40 563-58-64.6
cis-1,3-Dichloropropene ND ug/kg 1 07/13/11 00:40 10061-01-54.6
trans-1,3-Dichloropropene ND ug/kg 1 07/13/11 00:40 10061-02-64.6
Diisopropyl ether ND ug/kg 1 07/13/11 00:40 108-20-34.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 90 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 9A (4-6)Lab ID:9297694017 Collected:07/07/11 10:30 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/13/11 00:40 100-41-44.6
Hexachloro-1,3-butadiene ND ug/kg 1 07/13/11 00:40 87-68-34.6
2-Hexanone ND ug/kg 1 07/13/11 00:40 591-78-646.4
Isopropylbenzene (Cumene)ND ug/kg 1 07/13/11 00:40 98-82-84.6
p-Isopropyltoluene ND ug/kg 1 07/13/11 00:40 99-87-64.6
Methylene Chloride ND ug/kg 1 07/13/11 00:40 75-09-218.5
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/13/11 00:40 108-10-146.4
Methyl-tert-butyl ether ND ug/kg 1 07/13/11 00:40 1634-04-44.6
Naphthalene ND ug/kg 1 07/13/11 00:40 91-20-34.6
n-Propylbenzene ND ug/kg 1 07/13/11 00:40 103-65-14.6
Styrene ND ug/kg 1 07/13/11 00:40 100-42-54.6
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/13/11 00:40 630-20-64.6
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/13/11 00:40 79-34-54.6
Tetrachloroethene ND ug/kg 1 07/13/11 00:40 127-18-44.6
Toluene ND ug/kg 1 07/13/11 00:40 108-88-34.6
1,2,3-Trichlorobenzene ND ug/kg 1 07/13/11 00:40 87-61-64.6
1,2,4-Trichlorobenzene ND ug/kg 1 07/13/11 00:40 120-82-14.6
1,1,1-Trichloroethane ND ug/kg 1 07/13/11 00:40 71-55-64.6
1,1,2-Trichloroethane ND ug/kg 1 07/13/11 00:40 79-00-54.6
Trichloroethene ND ug/kg 1 07/13/11 00:40 79-01-64.6
Trichlorofluoromethane ND ug/kg 1 07/13/11 00:40 75-69-44.6
1,2,3-Trichloropropane ND ug/kg 1 07/13/11 00:40 96-18-44.6
1,2,4-Trimethylbenzene ND ug/kg 1 07/13/11 00:40 95-63-64.6
1,3,5-Trimethylbenzene ND ug/kg 1 07/13/11 00:40 108-67-84.6
Vinyl acetate ND ug/kg 1 07/13/11 00:40 108-05-446.4
Vinyl chloride ND ug/kg 1 07/13/11 00:40 75-01-49.3
Xylene (Total)ND ug/kg 1 07/13/11 00:40 1330-20-79.3
m&p-Xylene ND ug/kg 1 07/13/11 00:40 179601-23-19.3
o-Xylene ND ug/kg 1 07/13/11 00:40 95-47-64.6
Dibromofluoromethane (S)98 %1 07/13/11 00:40 1868-53-770-130
Toluene-d8 (S)99 %1 07/13/11 00:40 2037-26-570-130
4-Bromofluorobenzene (S)93 %1 07/13/11 00:40 460-00-470-130
1,2-Dichloroethane-d4 (S)79 %1 07/13/11 00:40 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 13.9 %1 07/08/11 08:590.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 91 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 10A (6-7)Lab ID:9297694018 Collected:07/07/11 10:15 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 21.5 mg/kg 1 07/12/11 08:38 68334-30-507/08/11 10:275.8
n-Pentacosane (S)73 %1 07/12/11 08:38 629-99-207/08/11 10:2741-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease ND mg/kg 1 07/11/11 12:0607/11/11 11:2380.6
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/13/11 02:56 8006-61-907/12/11 14:505.8
4-Bromofluorobenzene (S)123 %1 07/13/11 02:56 460-00-407/12/11 14:5070-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 1.3 mg/kg 1 07/14/11 14:54 7440-38-207/12/11 11:400.42
Barium 29.1 mg/kg 1 07/13/11 20:20 7440-39-307/12/11 11:400.42
Cadmium ND mg/kg 1 07/13/11 20:20 7440-43-907/12/11 11:400.085
Chromium 1.5 mg/kg 1 07/13/11 20:20 7440-47-307/12/11 11:400.42
Lead 15.2 mg/kg 1 07/13/11 20:20 7439-92-107/12/11 11:400.42
Selenium ND mg/kg 1 07/13/11 20:20 7782-49-207/12/11 11:400.85
Silver ND mg/kg 1 07/13/11 20:20 7440-22-407/12/11 11:400.42
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.019 mg/kg 1 07/15/11 15:03 7439-97-607/14/11 15:100.0049
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/12/11 10:15 83-32-907/08/11 11:00380
Acenaphthylene ND ug/kg 1 07/12/11 10:15 208-96-807/08/11 11:00380
Aniline ND ug/kg 1 07/12/11 10:15 62-53-307/08/11 11:00380
Anthracene ND ug/kg 1 07/12/11 10:15 120-12-707/08/11 11:00380
Benzo(a)anthracene ND ug/kg 1 07/12/11 10:15 56-55-307/08/11 11:00380
Benzo(a)pyrene ND ug/kg 1 07/12/11 10:15 50-32-807/08/11 11:00380
Benzo(b)fluoranthene ND ug/kg 1 07/12/11 10:15 205-99-207/08/11 11:00380
Benzo(g,h,i)perylene ND ug/kg 1 07/12/11 10:15 191-24-207/08/11 11:00380
Benzo(k)fluoranthene ND ug/kg 1 07/12/11 10:15 207-08-907/08/11 11:00380
Benzoic Acid ND ug/kg 1 07/12/11 10:15 65-85-007/08/11 11:001900
Benzyl alcohol ND ug/kg 1 07/12/11 10:15 100-51-607/08/11 11:00760
4-Bromophenylphenyl ether ND ug/kg 1 07/12/11 10:15 101-55-307/08/11 11:00380
Butylbenzylphthalate ND ug/kg 1 07/12/11 10:15 85-68-707/08/11 11:00380
4-Chloro-3-methylphenol ND ug/kg 1 07/12/11 10:15 59-50-707/08/11 11:00760
4-Chloroaniline ND ug/kg 1 07/12/11 10:15 106-47-807/08/11 11:001900
bis(2-Chloroethoxy)methane ND ug/kg 1 07/12/11 10:15 111-91-107/08/11 11:00380
bis(2-Chloroethyl) ether ND ug/kg 1 07/12/11 10:15 111-44-407/08/11 11:00380
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/12/11 10:15 108-60-107/08/11 11:00380
2-Chloronaphthalene ND ug/kg 1 07/12/11 10:15 91-58-707/08/11 11:00380
2-Chlorophenol ND ug/kg 1 07/12/11 10:15 95-57-807/08/11 11:00380
4-Chlorophenylphenyl ether ND ug/kg 1 07/12/11 10:15 7005-72-307/08/11 11:00380
Chrysene ND ug/kg 1 07/12/11 10:15 218-01-907/08/11 11:00380
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 92 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 10A (6-7)Lab ID:9297694018 Collected:07/07/11 10:15 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/12/11 10:15 53-70-307/08/11 11:00380
Dibenzofuran ND ug/kg 1 07/12/11 10:15 132-64-907/08/11 11:00380
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 10:15 95-50-107/08/11 11:00380
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 10:15 541-73-107/08/11 11:00380
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 10:15 106-46-707/08/11 11:00380
3,3'-Dichlorobenzidine ND ug/kg 1 07/12/11 10:15 91-94-107/08/11 11:001900
2,4-Dichlorophenol ND ug/kg 1 07/12/11 10:15 120-83-207/08/11 11:00380
Diethylphthalate ND ug/kg 1 07/12/11 10:15 84-66-207/08/11 11:00380
2,4-Dimethylphenol ND ug/kg 1 07/12/11 10:15 105-67-907/08/11 11:00380
Dimethylphthalate ND ug/kg 1 07/12/11 10:15 131-11-307/08/11 11:00380
Di-n-butylphthalate ND ug/kg 1 07/12/11 10:15 84-74-207/08/11 11:00380
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/12/11 10:15 534-52-107/08/11 11:00760
2,4-Dinitrophenol ND ug/kg 1 07/12/11 10:15 51-28-507/08/11 11:001900
2,4-Dinitrotoluene ND ug/kg 1 07/12/11 10:15 121-14-207/08/11 11:00380
2,6-Dinitrotoluene ND ug/kg 1 07/12/11 10:15 606-20-207/08/11 11:00380
Di-n-octylphthalate ND ug/kg 1 07/12/11 10:15 117-84-007/08/11 11:00380
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/12/11 10:15 117-81-707/08/11 11:00380
Fluoranthene ND ug/kg 1 07/12/11 10:15 206-44-007/08/11 11:00380
Fluorene ND ug/kg 1 07/12/11 10:15 86-73-707/08/11 11:00380
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 10:15 87-68-307/08/11 11:00380
Hexachlorobenzene ND ug/kg 1 07/12/11 10:15 118-74-107/08/11 11:00380
Hexachlorocyclopentadiene ND ug/kg 1 07/12/11 10:15 77-47-407/08/11 11:00380
Hexachloroethane ND ug/kg 1 07/12/11 10:15 67-72-107/08/11 11:00380
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/12/11 10:15 193-39-507/08/11 11:00380
Isophorone ND ug/kg 1 07/12/11 10:15 78-59-107/08/11 11:00380
1-Methylnaphthalene ND ug/kg 1 07/12/11 10:15 90-12-007/08/11 11:00380
2-Methylnaphthalene ND ug/kg 1 07/12/11 10:15 91-57-607/08/11 11:00380
2-Methylphenol(o-Cresol)ND ug/kg 1 07/12/11 10:15 95-48-707/08/11 11:00380
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/12/11 10:1507/08/11 11:00380
Naphthalene ND ug/kg 1 07/12/11 10:15 91-20-307/08/11 11:00380
2-Nitroaniline ND ug/kg 1 07/12/11 10:15 88-74-407/08/11 11:001900
3-Nitroaniline ND ug/kg 1 07/12/11 10:15 99-09-207/08/11 11:001900
4-Nitroaniline ND ug/kg 1 07/12/11 10:15 100-01-607/08/11 11:00760
Nitrobenzene ND ug/kg 1 07/12/11 10:15 98-95-307/08/11 11:00380
2-Nitrophenol ND ug/kg 1 07/12/11 10:15 88-75-507/08/11 11:00380
4-Nitrophenol ND ug/kg 1 07/12/11 10:15 100-02-707/08/11 11:001900
N-Nitrosodimethylamine ND ug/kg 1 07/12/11 10:15 62-75-907/08/11 11:00380
N-Nitroso-di-n-propylamine ND ug/kg 1 07/12/11 10:15 621-64-707/08/11 11:00380
N-Nitrosodiphenylamine ND ug/kg 1 07/12/11 10:15 86-30-607/08/11 11:00380
Pentachlorophenol ND ug/kg 1 07/12/11 10:15 87-86-507/08/11 11:001900
Phenanthrene ND ug/kg 1 07/12/11 10:15 85-01-807/08/11 11:00380
Phenol ND ug/kg 1 07/12/11 10:15 108-95-207/08/11 11:00380
Pyrene ND ug/kg 1 07/12/11 10:15 129-00-007/08/11 11:00380
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 10:15 120-82-107/08/11 11:00380
2,4,5-Trichlorophenol ND ug/kg 1 07/12/11 10:15 95-95-407/08/11 11:00380
2,4,6-Trichlorophenol ND ug/kg 1 07/12/11 10:15 88-06-207/08/11 11:00380
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 93 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 10A (6-7)Lab ID:9297694018 Collected:07/07/11 10:15 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)63 %1 07/12/11 10:15 4165-60-007/08/11 11:0023-110
2-Fluorobiphenyl (S)68 %1 07/12/11 10:15 321-60-807/08/11 11:0030-110
Terphenyl-d14 (S)73 %1 07/12/11 10:15 1718-51-007/08/11 11:0028-110
Phenol-d6 (S)49 %1 07/12/11 10:15 13127-88-307/08/11 11:0022-110
2-Fluorophenol (S)51 %1 07/12/11 10:15 367-12-407/08/11 11:0013-110
2,4,6-Tribromophenol (S)70 %1 07/12/11 10:15 118-79-607/08/11 11:0027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/13/11 01:00 67-64-186.7
Benzene ND ug/kg 1 07/13/11 01:00 71-43-24.3
Bromobenzene ND ug/kg 1 07/13/11 01:00 108-86-14.3
Bromochloromethane ND ug/kg 1 07/13/11 01:00 74-97-54.3
Bromodichloromethane ND ug/kg 1 07/13/11 01:00 75-27-44.3
Bromoform ND ug/kg 1 07/13/11 01:00 75-25-24.3
Bromomethane ND ug/kg 1 07/13/11 01:00 74-83-98.7
2-Butanone (MEK)ND ug/kg 1 07/13/11 01:00 78-93-386.7
n-Butylbenzene ND ug/kg 1 07/13/11 01:00 104-51-84.3
sec-Butylbenzene ND ug/kg 1 07/13/11 01:00 135-98-84.3
tert-Butylbenzene ND ug/kg 1 07/13/11 01:00 98-06-64.3
Carbon tetrachloride ND ug/kg 1 07/13/11 01:00 56-23-54.3
Chlorobenzene ND ug/kg 1 07/13/11 01:00 108-90-74.3
Chloroethane ND ug/kg 1 07/13/11 01:00 75-00-38.7
Chloroform ND ug/kg 1 07/13/11 01:00 67-66-34.3
Chloromethane ND ug/kg 1 07/13/11 01:00 74-87-38.7
2-Chlorotoluene ND ug/kg 1 07/13/11 01:00 95-49-84.3
4-Chlorotoluene ND ug/kg 1 07/13/11 01:00 106-43-44.3
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/13/11 01:00 96-12-84.3
Dibromochloromethane ND ug/kg 1 07/13/11 01:00 124-48-14.3
1,2-Dibromoethane (EDB)ND ug/kg 1 07/13/11 01:00 106-93-44.3
Dibromomethane ND ug/kg 1 07/13/11 01:00 74-95-34.3
1,2-Dichlorobenzene ND ug/kg 1 07/13/11 01:00 95-50-14.3
1,3-Dichlorobenzene ND ug/kg 1 07/13/11 01:00 541-73-14.3
1,4-Dichlorobenzene ND ug/kg 1 07/13/11 01:00 106-46-74.3
Dichlorodifluoromethane ND ug/kg 1 07/13/11 01:00 75-71-88.7
1,1-Dichloroethane ND ug/kg 1 07/13/11 01:00 75-34-34.3
1,2-Dichloroethane ND ug/kg 1 07/13/11 01:00 107-06-24.3
1,1-Dichloroethene ND ug/kg 1 07/13/11 01:00 75-35-44.3
cis-1,2-Dichloroethene ND ug/kg 1 07/13/11 01:00 156-59-24.3
trans-1,2-Dichloroethene ND ug/kg 1 07/13/11 01:00 156-60-54.3
1,2-Dichloropropane ND ug/kg 1 07/13/11 01:00 78-87-54.3
1,3-Dichloropropane ND ug/kg 1 07/13/11 01:00 142-28-94.3
2,2-Dichloropropane ND ug/kg 1 07/13/11 01:00 594-20-74.3
1,1-Dichloropropene ND ug/kg 1 07/13/11 01:00 563-58-64.3
cis-1,3-Dichloropropene ND ug/kg 1 07/13/11 01:00 10061-01-54.3
trans-1,3-Dichloropropene ND ug/kg 1 07/13/11 01:00 10061-02-64.3
Diisopropyl ether ND ug/kg 1 07/13/11 01:00 108-20-34.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 94 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 10A (6-7)Lab ID:9297694018 Collected:07/07/11 10:15 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/13/11 01:00 100-41-44.3
Hexachloro-1,3-butadiene ND ug/kg 1 07/13/11 01:00 87-68-34.3
2-Hexanone ND ug/kg 1 07/13/11 01:00 591-78-643.3
Isopropylbenzene (Cumene)ND ug/kg 1 07/13/11 01:00 98-82-84.3
p-Isopropyltoluene ND ug/kg 1 07/13/11 01:00 99-87-64.3
Methylene Chloride ND ug/kg 1 07/13/11 01:00 75-09-217.3
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/13/11 01:00 108-10-143.3
Methyl-tert-butyl ether ND ug/kg 1 07/13/11 01:00 1634-04-44.3
Naphthalene ND ug/kg 1 07/13/11 01:00 91-20-34.3
n-Propylbenzene ND ug/kg 1 07/13/11 01:00 103-65-14.3
Styrene ND ug/kg 1 07/13/11 01:00 100-42-54.3
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/13/11 01:00 630-20-64.3
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/13/11 01:00 79-34-54.3
Tetrachloroethene ND ug/kg 1 07/13/11 01:00 127-18-44.3
Toluene ND ug/kg 1 07/13/11 01:00 108-88-34.3
1,2,3-Trichlorobenzene ND ug/kg 1 07/13/11 01:00 87-61-64.3
1,2,4-Trichlorobenzene ND ug/kg 1 07/13/11 01:00 120-82-14.3
1,1,1-Trichloroethane ND ug/kg 1 07/13/11 01:00 71-55-64.3
1,1,2-Trichloroethane ND ug/kg 1 07/13/11 01:00 79-00-54.3
Trichloroethene ND ug/kg 1 07/13/11 01:00 79-01-64.3
Trichlorofluoromethane ND ug/kg 1 07/13/11 01:00 75-69-44.3
1,2,3-Trichloropropane ND ug/kg 1 07/13/11 01:00 96-18-44.3
1,2,4-Trimethylbenzene ND ug/kg 1 07/13/11 01:00 95-63-64.3
1,3,5-Trimethylbenzene ND ug/kg 1 07/13/11 01:00 108-67-84.3
Vinyl acetate ND ug/kg 1 07/13/11 01:00 108-05-443.3
Vinyl chloride ND ug/kg 1 07/13/11 01:00 75-01-48.7
Xylene (Total)ND ug/kg 1 07/13/11 01:00 1330-20-78.7
m&p-Xylene ND ug/kg 1 07/13/11 01:00 179601-23-18.7
o-Xylene ND ug/kg 1 07/13/11 01:00 95-47-64.3
Dibromofluoromethane (S)93 %1 07/13/11 01:00 1868-53-770-130
Toluene-d8 (S)97 %1 07/13/11 01:00 2037-26-570-130
4-Bromofluorobenzene (S)86 %1 07/13/11 01:00 460-00-470-130
1,2-Dichloroethane-d4 (S)93 %1 07/13/11 01:00 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 13.1 %1 07/08/11 09:000.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 95 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 10A (9-10)Lab ID:9297694019 Collected:07/07/11 10:25 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 10 mg/kg 1 07/12/11 08:38 68334-30-507/08/11 10:276.1
n-Pentacosane (S)48 %1 07/12/11 08:38 629-99-207/08/11 10:2741-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease ND mg/kg 1 07/11/11 12:0607/11/11 11:2384.9
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/13/11 03:20 8006-61-907/12/11 14:506.1
4-Bromofluorobenzene (S)141 %1 07/13/11 03:20 460-00-407/12/11 14:5070-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 2.5 mg/kg 1 07/14/11 14:58 7440-38-207/12/11 11:400.59
Barium 88.0 mg/kg 1 07/13/11 20:23 7440-39-307/12/11 11:400.59
Cadmium ND mg/kg 1 07/13/11 20:23 7440-43-907/12/11 11:400.12
Chromium 3.5 mg/kg 1 07/13/11 20:23 7440-47-307/12/11 11:400.59
Lead 13.8 mg/kg 1 07/13/11 20:23 7439-92-107/12/11 11:400.59
Selenium ND mg/kg 1 07/13/11 20:23 7782-49-207/12/11 11:401.2
Silver ND mg/kg 1 07/13/11 20:23 7440-22-407/12/11 11:400.59
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.024 mg/kg 1 07/15/11 15:06 7439-97-607/14/11 15:100.0048
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/12/11 10:43 83-32-907/08/11 11:00400
Acenaphthylene ND ug/kg 1 07/12/11 10:43 208-96-807/08/11 11:00400
Aniline ND ug/kg 1 07/12/11 10:43 62-53-307/08/11 11:00400
Anthracene ND ug/kg 1 07/12/11 10:43 120-12-707/08/11 11:00400
Benzo(a)anthracene ND ug/kg 1 07/12/11 10:43 56-55-307/08/11 11:00400
Benzo(a)pyrene ND ug/kg 1 07/12/11 10:43 50-32-807/08/11 11:00400
Benzo(b)fluoranthene ND ug/kg 1 07/12/11 10:43 205-99-207/08/11 11:00400
Benzo(g,h,i)perylene ND ug/kg 1 07/12/11 10:43 191-24-207/08/11 11:00400
Benzo(k)fluoranthene ND ug/kg 1 07/12/11 10:43 207-08-907/08/11 11:00400
Benzoic Acid ND ug/kg 1 07/12/11 10:43 65-85-007/08/11 11:002000
Benzyl alcohol ND ug/kg 1 07/12/11 10:43 100-51-607/08/11 11:00800
4-Bromophenylphenyl ether ND ug/kg 1 07/12/11 10:43 101-55-307/08/11 11:00400
Butylbenzylphthalate ND ug/kg 1 07/12/11 10:43 85-68-707/08/11 11:00400
4-Chloro-3-methylphenol ND ug/kg 1 07/12/11 10:43 59-50-707/08/11 11:00800
4-Chloroaniline ND ug/kg 1 07/12/11 10:43 106-47-807/08/11 11:002000
bis(2-Chloroethoxy)methane ND ug/kg 1 07/12/11 10:43 111-91-107/08/11 11:00400
bis(2-Chloroethyl) ether ND ug/kg 1 07/12/11 10:43 111-44-407/08/11 11:00400
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/12/11 10:43 108-60-107/08/11 11:00400
2-Chloronaphthalene ND ug/kg 1 07/12/11 10:43 91-58-707/08/11 11:00400
2-Chlorophenol ND ug/kg 1 07/12/11 10:43 95-57-807/08/11 11:00400
4-Chlorophenylphenyl ether ND ug/kg 1 07/12/11 10:43 7005-72-307/08/11 11:00400
Chrysene ND ug/kg 1 07/12/11 10:43 218-01-907/08/11 11:00400
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 96 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 10A (9-10)Lab ID:9297694019 Collected:07/07/11 10:25 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/12/11 10:43 53-70-307/08/11 11:00400
Dibenzofuran ND ug/kg 1 07/12/11 10:43 132-64-907/08/11 11:00400
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 10:43 95-50-107/08/11 11:00400
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 10:43 541-73-107/08/11 11:00400
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 10:43 106-46-707/08/11 11:00400
3,3'-Dichlorobenzidine ND ug/kg 1 07/12/11 10:43 91-94-107/08/11 11:002000
2,4-Dichlorophenol ND ug/kg 1 07/12/11 10:43 120-83-207/08/11 11:00400
Diethylphthalate ND ug/kg 1 07/12/11 10:43 84-66-207/08/11 11:00400
2,4-Dimethylphenol ND ug/kg 1 07/12/11 10:43 105-67-907/08/11 11:00400
Dimethylphthalate ND ug/kg 1 07/12/11 10:43 131-11-307/08/11 11:00400
Di-n-butylphthalate ND ug/kg 1 07/12/11 10:43 84-74-207/08/11 11:00400
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/12/11 10:43 534-52-107/08/11 11:00800
2,4-Dinitrophenol ND ug/kg 1 07/12/11 10:43 51-28-507/08/11 11:002000
2,4-Dinitrotoluene ND ug/kg 1 07/12/11 10:43 121-14-207/08/11 11:00400
2,6-Dinitrotoluene ND ug/kg 1 07/12/11 10:43 606-20-207/08/11 11:00400
Di-n-octylphthalate ND ug/kg 1 07/12/11 10:43 117-84-007/08/11 11:00400
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/12/11 10:43 117-81-707/08/11 11:00400
Fluoranthene ND ug/kg 1 07/12/11 10:43 206-44-007/08/11 11:00400
Fluorene ND ug/kg 1 07/12/11 10:43 86-73-707/08/11 11:00400
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 10:43 87-68-307/08/11 11:00400
Hexachlorobenzene ND ug/kg 1 07/12/11 10:43 118-74-107/08/11 11:00400
Hexachlorocyclopentadiene ND ug/kg 1 07/12/11 10:43 77-47-407/08/11 11:00400
Hexachloroethane ND ug/kg 1 07/12/11 10:43 67-72-107/08/11 11:00400
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/12/11 10:43 193-39-507/08/11 11:00400
Isophorone ND ug/kg 1 07/12/11 10:43 78-59-107/08/11 11:00400
1-Methylnaphthalene ND ug/kg 1 07/12/11 10:43 90-12-007/08/11 11:00400
2-Methylnaphthalene ND ug/kg 1 07/12/11 10:43 91-57-607/08/11 11:00400
2-Methylphenol(o-Cresol)ND ug/kg 1 07/12/11 10:43 95-48-707/08/11 11:00400
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/12/11 10:4307/08/11 11:00400
Naphthalene ND ug/kg 1 07/12/11 10:43 91-20-307/08/11 11:00400
2-Nitroaniline ND ug/kg 1 07/12/11 10:43 88-74-407/08/11 11:002000
3-Nitroaniline ND ug/kg 1 07/12/11 10:43 99-09-207/08/11 11:002000
4-Nitroaniline ND ug/kg 1 07/12/11 10:43 100-01-607/08/11 11:00800
Nitrobenzene ND ug/kg 1 07/12/11 10:43 98-95-307/08/11 11:00400
2-Nitrophenol ND ug/kg 1 07/12/11 10:43 88-75-507/08/11 11:00400
4-Nitrophenol ND ug/kg 1 07/12/11 10:43 100-02-707/08/11 11:002000
N-Nitrosodimethylamine ND ug/kg 1 07/12/11 10:43 62-75-907/08/11 11:00400
N-Nitroso-di-n-propylamine ND ug/kg 1 07/12/11 10:43 621-64-707/08/11 11:00400
N-Nitrosodiphenylamine ND ug/kg 1 07/12/11 10:43 86-30-607/08/11 11:00400
Pentachlorophenol ND ug/kg 1 07/12/11 10:43 87-86-507/08/11 11:002000
Phenanthrene ND ug/kg 1 07/12/11 10:43 85-01-807/08/11 11:00400
Phenol ND ug/kg 1 07/12/11 10:43 108-95-207/08/11 11:00400
Pyrene ND ug/kg 1 07/12/11 10:43 129-00-007/08/11 11:00400
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 10:43 120-82-107/08/11 11:00400
2,4,5-Trichlorophenol ND ug/kg 1 07/12/11 10:43 95-95-407/08/11 11:00400
2,4,6-Trichlorophenol ND ug/kg 1 07/12/11 10:43 88-06-207/08/11 11:00400
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 97 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 10A (9-10)Lab ID:9297694019 Collected:07/07/11 10:25 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)78 %1 07/12/11 10:43 4165-60-007/08/11 11:0023-110
2-Fluorobiphenyl (S)77 %1 07/12/11 10:43 321-60-807/08/11 11:0030-110
Terphenyl-d14 (S)85 %1 07/12/11 10:43 1718-51-007/08/11 11:0028-110
Phenol-d6 (S)55 %1 07/12/11 10:43 13127-88-307/08/11 11:0022-110
2-Fluorophenol (S)60 %1 07/12/11 10:43 367-12-407/08/11 11:0013-110
2,4,6-Tribromophenol (S)76 %1 07/12/11 10:43 118-79-607/08/11 11:0027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/13/11 01:20 67-64-197.3
Benzene ND ug/kg 1 07/13/11 01:20 71-43-24.9
Bromobenzene ND ug/kg 1 07/13/11 01:20 108-86-14.9
Bromochloromethane ND ug/kg 1 07/13/11 01:20 74-97-54.9
Bromodichloromethane ND ug/kg 1 07/13/11 01:20 75-27-44.9
Bromoform ND ug/kg 1 07/13/11 01:20 75-25-24.9
Bromomethane ND ug/kg 1 07/13/11 01:20 74-83-99.7
2-Butanone (MEK)ND ug/kg 1 07/13/11 01:20 78-93-397.3
n-Butylbenzene ND ug/kg 1 07/13/11 01:20 104-51-84.9
sec-Butylbenzene ND ug/kg 1 07/13/11 01:20 135-98-84.9
tert-Butylbenzene ND ug/kg 1 07/13/11 01:20 98-06-64.9
Carbon tetrachloride ND ug/kg 1 07/13/11 01:20 56-23-54.9
Chlorobenzene ND ug/kg 1 07/13/11 01:20 108-90-74.9
Chloroethane ND ug/kg 1 07/13/11 01:20 75-00-39.7
Chloroform ND ug/kg 1 07/13/11 01:20 67-66-34.9
Chloromethane ND ug/kg 1 07/13/11 01:20 74-87-39.7
2-Chlorotoluene ND ug/kg 1 07/13/11 01:20 95-49-84.9
4-Chlorotoluene ND ug/kg 1 07/13/11 01:20 106-43-44.9
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/13/11 01:20 96-12-84.9
Dibromochloromethane ND ug/kg 1 07/13/11 01:20 124-48-14.9
1,2-Dibromoethane (EDB)ND ug/kg 1 07/13/11 01:20 106-93-44.9
Dibromomethane ND ug/kg 1 07/13/11 01:20 74-95-34.9
1,2-Dichlorobenzene ND ug/kg 1 07/13/11 01:20 95-50-14.9
1,3-Dichlorobenzene ND ug/kg 1 07/13/11 01:20 541-73-14.9
1,4-Dichlorobenzene ND ug/kg 1 07/13/11 01:20 106-46-74.9
Dichlorodifluoromethane ND ug/kg 1 07/13/11 01:20 75-71-89.7
1,1-Dichloroethane ND ug/kg 1 07/13/11 01:20 75-34-34.9
1,2-Dichloroethane ND ug/kg 1 07/13/11 01:20 107-06-24.9
1,1-Dichloroethene ND ug/kg 1 07/13/11 01:20 75-35-44.9
cis-1,2-Dichloroethene ND ug/kg 1 07/13/11 01:20 156-59-24.9
trans-1,2-Dichloroethene ND ug/kg 1 07/13/11 01:20 156-60-54.9
1,2-Dichloropropane ND ug/kg 1 07/13/11 01:20 78-87-54.9
1,3-Dichloropropane ND ug/kg 1 07/13/11 01:20 142-28-94.9
2,2-Dichloropropane ND ug/kg 1 07/13/11 01:20 594-20-74.9
1,1-Dichloropropene ND ug/kg 1 07/13/11 01:20 563-58-64.9
cis-1,3-Dichloropropene ND ug/kg 1 07/13/11 01:20 10061-01-54.9
trans-1,3-Dichloropropene ND ug/kg 1 07/13/11 01:20 10061-02-64.9
Diisopropyl ether ND ug/kg 1 07/13/11 01:20 108-20-34.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 98 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 10A (9-10)Lab ID:9297694019 Collected:07/07/11 10:25 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/13/11 01:20 100-41-44.9
Hexachloro-1,3-butadiene ND ug/kg 1 07/13/11 01:20 87-68-34.9
2-Hexanone ND ug/kg 1 07/13/11 01:20 591-78-648.7
Isopropylbenzene (Cumene)ND ug/kg 1 07/13/11 01:20 98-82-84.9
p-Isopropyltoluene ND ug/kg 1 07/13/11 01:20 99-87-64.9
Methylene Chloride ND ug/kg 1 07/13/11 01:20 75-09-219.5
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/13/11 01:20 108-10-148.7
Methyl-tert-butyl ether ND ug/kg 1 07/13/11 01:20 1634-04-44.9
Naphthalene ND ug/kg 1 07/13/11 01:20 91-20-34.9
n-Propylbenzene ND ug/kg 1 07/13/11 01:20 103-65-14.9
Styrene ND ug/kg 1 07/13/11 01:20 100-42-54.9
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/13/11 01:20 630-20-64.9
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/13/11 01:20 79-34-54.9
Tetrachloroethene ND ug/kg 1 07/13/11 01:20 127-18-44.9
Toluene ND ug/kg 1 07/13/11 01:20 108-88-34.9
1,2,3-Trichlorobenzene ND ug/kg 1 07/13/11 01:20 87-61-64.9
1,2,4-Trichlorobenzene ND ug/kg 1 07/13/11 01:20 120-82-14.9
1,1,1-Trichloroethane ND ug/kg 1 07/13/11 01:20 71-55-64.9
1,1,2-Trichloroethane ND ug/kg 1 07/13/11 01:20 79-00-54.9
Trichloroethene ND ug/kg 1 07/13/11 01:20 79-01-64.9
Trichlorofluoromethane ND ug/kg 1 07/13/11 01:20 75-69-44.9
1,2,3-Trichloropropane ND ug/kg 1 07/13/11 01:20 96-18-44.9
1,2,4-Trimethylbenzene ND ug/kg 1 07/13/11 01:20 95-63-64.9
1,3,5-Trimethylbenzene ND ug/kg 1 07/13/11 01:20 108-67-84.9
Vinyl acetate ND ug/kg 1 07/13/11 01:20 108-05-448.7
Vinyl chloride ND ug/kg 1 07/13/11 01:20 75-01-49.7
Xylene (Total)ND ug/kg 1 07/13/11 01:20 1330-20-79.7
m&p-Xylene ND ug/kg 1 07/13/11 01:20 179601-23-19.7
o-Xylene ND ug/kg 1 07/13/11 01:20 95-47-64.9
Dibromofluoromethane (S)88 %1 07/13/11 01:20 1868-53-770-130
Toluene-d8 (S)100 %1 07/13/11 01:20 2037-26-570-130
4-Bromofluorobenzene (S)93 %1 07/13/11 01:20 460-00-470-130
1,2-Dichloroethane-d4 (S)83 %1 07/13/11 01:20 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 17.5 %1 07/08/11 09:000.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 99 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 11A (6-7)Lab ID:9297694020 Collected:07/07/11 09:40 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 5.9 mg/kg 1 07/12/11 09:07 68334-30-507/08/11 10:275.7
n-Pentacosane (S)71 %1 07/12/11 09:07 629-99-207/08/11 10:2741-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease ND mg/kg 1 07/14/11 11:2007/14/11 10:4379.8
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/13/11 03:45 8006-61-907/12/11 14:505.8
4-Bromofluorobenzene (S)152 %1 07/13/11 03:45 460-00-407/12/11 14:5070-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 1.9 mg/kg 1 07/13/11 20:37 7440-38-207/12/11 11:400.54
Barium 39.2 mg/kg 1 07/13/11 20:37 7440-39-307/12/11 11:400.54
Cadmium ND mg/kg 1 07/13/11 20:37 7440-43-907/12/11 11:400.11
Chromium 2.5 mg/kg 1 07/13/11 20:37 7440-47-307/12/11 11:400.54
Lead 16.7 mg/kg 1 07/13/11 20:37 7439-92-107/12/11 11:400.54
Selenium ND mg/kg 1 07/13/11 20:37 7782-49-207/12/11 11:401.1
Silver ND mg/kg 1 07/13/11 20:37 7440-22-407/12/11 11:400.54
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.021 mg/kg 1 07/15/11 15:08 7439-97-607/14/11 15:100.0050
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/12/11 11:12 83-32-907/08/11 11:00376
Acenaphthylene ND ug/kg 1 07/12/11 11:12 208-96-807/08/11 11:00376
Aniline ND ug/kg 1 07/12/11 11:12 62-53-307/08/11 11:00376
Anthracene ND ug/kg 1 07/12/11 11:12 120-12-707/08/11 11:00376
Benzo(a)anthracene ND ug/kg 1 07/12/11 11:12 56-55-307/08/11 11:00376
Benzo(a)pyrene ND ug/kg 1 07/12/11 11:12 50-32-807/08/11 11:00376
Benzo(b)fluoranthene ND ug/kg 1 07/12/11 11:12 205-99-207/08/11 11:00376
Benzo(g,h,i)perylene ND ug/kg 1 07/12/11 11:12 191-24-207/08/11 11:00376
Benzo(k)fluoranthene ND ug/kg 1 07/12/11 11:12 207-08-907/08/11 11:00376
Benzoic Acid ND ug/kg 1 07/12/11 11:12 65-85-007/08/11 11:001880
Benzyl alcohol ND ug/kg 1 07/12/11 11:12 100-51-607/08/11 11:00752
4-Bromophenylphenyl ether ND ug/kg 1 07/12/11 11:12 101-55-307/08/11 11:00376
Butylbenzylphthalate ND ug/kg 1 07/12/11 11:12 85-68-707/08/11 11:00376
4-Chloro-3-methylphenol ND ug/kg 1 07/12/11 11:12 59-50-707/08/11 11:00752
4-Chloroaniline ND ug/kg 1 07/12/11 11:12 106-47-807/08/11 11:001880
bis(2-Chloroethoxy)methane ND ug/kg 1 07/12/11 11:12 111-91-107/08/11 11:00376
bis(2-Chloroethyl) ether ND ug/kg 1 07/12/11 11:12 111-44-407/08/11 11:00376
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/12/11 11:12 108-60-107/08/11 11:00376
2-Chloronaphthalene ND ug/kg 1 07/12/11 11:12 91-58-707/08/11 11:00376
2-Chlorophenol ND ug/kg 1 07/12/11 11:12 95-57-807/08/11 11:00376
4-Chlorophenylphenyl ether ND ug/kg 1 07/12/11 11:12 7005-72-307/08/11 11:00376
Chrysene ND ug/kg 1 07/12/11 11:12 218-01-907/08/11 11:00376
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 100 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 11A (6-7)Lab ID:9297694020 Collected:07/07/11 09:40 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/12/11 11:12 53-70-307/08/11 11:00376
Dibenzofuran ND ug/kg 1 07/12/11 11:12 132-64-907/08/11 11:00376
1,2-Dichlorobenzene ND ug/kg 1 07/12/11 11:12 95-50-107/08/11 11:00376
1,3-Dichlorobenzene ND ug/kg 1 07/12/11 11:12 541-73-107/08/11 11:00376
1,4-Dichlorobenzene ND ug/kg 1 07/12/11 11:12 106-46-707/08/11 11:00376
3,3'-Dichlorobenzidine ND ug/kg 1 07/12/11 11:12 91-94-107/08/11 11:001880
2,4-Dichlorophenol ND ug/kg 1 07/12/11 11:12 120-83-207/08/11 11:00376
Diethylphthalate ND ug/kg 1 07/12/11 11:12 84-66-207/08/11 11:00376
2,4-Dimethylphenol ND ug/kg 1 07/12/11 11:12 105-67-907/08/11 11:00376
Dimethylphthalate ND ug/kg 1 07/12/11 11:12 131-11-307/08/11 11:00376
Di-n-butylphthalate ND ug/kg 1 07/12/11 11:12 84-74-207/08/11 11:00376
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/12/11 11:12 534-52-107/08/11 11:00752
2,4-Dinitrophenol ND ug/kg 1 07/12/11 11:12 51-28-507/08/11 11:001880
2,4-Dinitrotoluene ND ug/kg 1 07/12/11 11:12 121-14-207/08/11 11:00376
2,6-Dinitrotoluene ND ug/kg 1 07/12/11 11:12 606-20-207/08/11 11:00376
Di-n-octylphthalate ND ug/kg 1 07/12/11 11:12 117-84-007/08/11 11:00376
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/12/11 11:12 117-81-707/08/11 11:00376
Fluoranthene ND ug/kg 1 07/12/11 11:12 206-44-007/08/11 11:00376
Fluorene ND ug/kg 1 07/12/11 11:12 86-73-707/08/11 11:00376
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/11 11:12 87-68-307/08/11 11:00376
Hexachlorobenzene ND ug/kg 1 07/12/11 11:12 118-74-107/08/11 11:00376
Hexachlorocyclopentadiene ND ug/kg 1 07/12/11 11:12 77-47-407/08/11 11:00376
Hexachloroethane ND ug/kg 1 07/12/11 11:12 67-72-107/08/11 11:00376
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/12/11 11:12 193-39-507/08/11 11:00376
Isophorone ND ug/kg 1 07/12/11 11:12 78-59-107/08/11 11:00376
1-Methylnaphthalene ND ug/kg 1 07/12/11 11:12 90-12-007/08/11 11:00376
2-Methylnaphthalene ND ug/kg 1 07/12/11 11:12 91-57-607/08/11 11:00376
2-Methylphenol(o-Cresol)ND ug/kg 1 07/12/11 11:12 95-48-707/08/11 11:00376
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/12/11 11:1207/08/11 11:00376
Naphthalene ND ug/kg 1 07/12/11 11:12 91-20-307/08/11 11:00376
2-Nitroaniline ND ug/kg 1 07/12/11 11:12 88-74-407/08/11 11:001880
3-Nitroaniline ND ug/kg 1 07/12/11 11:12 99-09-207/08/11 11:001880
4-Nitroaniline ND ug/kg 1 07/12/11 11:12 100-01-607/08/11 11:00752
Nitrobenzene ND ug/kg 1 07/12/11 11:12 98-95-307/08/11 11:00376
2-Nitrophenol ND ug/kg 1 07/12/11 11:12 88-75-507/08/11 11:00376
4-Nitrophenol ND ug/kg 1 07/12/11 11:12 100-02-707/08/11 11:001880
N-Nitrosodimethylamine ND ug/kg 1 07/12/11 11:12 62-75-907/08/11 11:00376
N-Nitroso-di-n-propylamine ND ug/kg 1 07/12/11 11:12 621-64-707/08/11 11:00376
N-Nitrosodiphenylamine ND ug/kg 1 07/12/11 11:12 86-30-607/08/11 11:00376
Pentachlorophenol ND ug/kg 1 07/12/11 11:12 87-86-507/08/11 11:001880
Phenanthrene ND ug/kg 1 07/12/11 11:12 85-01-807/08/11 11:00376
Phenol ND ug/kg 1 07/12/11 11:12 108-95-207/08/11 11:00376
Pyrene ND ug/kg 1 07/12/11 11:12 129-00-007/08/11 11:00376
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/11 11:12 120-82-107/08/11 11:00376
2,4,5-Trichlorophenol ND ug/kg 1 07/12/11 11:12 95-95-407/08/11 11:00376
2,4,6-Trichlorophenol ND ug/kg 1 07/12/11 11:12 88-06-207/08/11 11:00376
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 101 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 11A (6-7)Lab ID:9297694020 Collected:07/07/11 09:40 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)63 %1 07/12/11 11:12 4165-60-007/08/11 11:0023-110
2-Fluorobiphenyl (S)64 %1 07/12/11 11:12 321-60-807/08/11 11:0030-110
Terphenyl-d14 (S)78 %1 07/12/11 11:12 1718-51-007/08/11 11:0028-110
Phenol-d6 (S)50 %1 07/12/11 11:12 13127-88-307/08/11 11:0022-110
2-Fluorophenol (S)52 %1 07/12/11 11:12 367-12-407/08/11 11:0013-110
2,4,6-Tribromophenol (S)73 %1 07/12/11 11:12 118-79-607/08/11 11:0027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/13/11 01:40 67-64-179.6
Benzene ND ug/kg 1 07/13/11 01:40 71-43-24.0
Bromobenzene ND ug/kg 1 07/13/11 01:40 108-86-14.0
Bromochloromethane ND ug/kg 1 07/13/11 01:40 74-97-54.0
Bromodichloromethane ND ug/kg 1 07/13/11 01:40 75-27-44.0
Bromoform ND ug/kg 1 07/13/11 01:40 75-25-24.0
Bromomethane ND ug/kg 1 07/13/11 01:40 74-83-98.0
2-Butanone (MEK)ND ug/kg 1 07/13/11 01:40 78-93-379.6
n-Butylbenzene ND ug/kg 1 07/13/11 01:40 104-51-84.0
sec-Butylbenzene ND ug/kg 1 07/13/11 01:40 135-98-84.0
tert-Butylbenzene ND ug/kg 1 07/13/11 01:40 98-06-64.0
Carbon tetrachloride ND ug/kg 1 07/13/11 01:40 56-23-54.0
Chlorobenzene ND ug/kg 1 07/13/11 01:40 108-90-74.0
Chloroethane ND ug/kg 1 07/13/11 01:40 75-00-38.0
Chloroform ND ug/kg 1 07/13/11 01:40 67-66-34.0
Chloromethane ND ug/kg 1 07/13/11 01:40 74-87-38.0
2-Chlorotoluene ND ug/kg 1 07/13/11 01:40 95-49-84.0
4-Chlorotoluene ND ug/kg 1 07/13/11 01:40 106-43-44.0
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/13/11 01:40 96-12-84.0
Dibromochloromethane ND ug/kg 1 07/13/11 01:40 124-48-14.0
1,2-Dibromoethane (EDB)ND ug/kg 1 07/13/11 01:40 106-93-44.0
Dibromomethane ND ug/kg 1 07/13/11 01:40 74-95-34.0
1,2-Dichlorobenzene ND ug/kg 1 07/13/11 01:40 95-50-14.0
1,3-Dichlorobenzene ND ug/kg 1 07/13/11 01:40 541-73-14.0
1,4-Dichlorobenzene ND ug/kg 1 07/13/11 01:40 106-46-74.0
Dichlorodifluoromethane ND ug/kg 1 07/13/11 01:40 75-71-88.0
1,1-Dichloroethane ND ug/kg 1 07/13/11 01:40 75-34-34.0
1,2-Dichloroethane ND ug/kg 1 07/13/11 01:40 107-06-24.0
1,1-Dichloroethene ND ug/kg 1 07/13/11 01:40 75-35-44.0
cis-1,2-Dichloroethene ND ug/kg 1 07/13/11 01:40 156-59-24.0
trans-1,2-Dichloroethene ND ug/kg 1 07/13/11 01:40 156-60-54.0
1,2-Dichloropropane ND ug/kg 1 07/13/11 01:40 78-87-54.0
1,3-Dichloropropane ND ug/kg 1 07/13/11 01:40 142-28-94.0
2,2-Dichloropropane ND ug/kg 1 07/13/11 01:40 594-20-74.0
1,1-Dichloropropene ND ug/kg 1 07/13/11 01:40 563-58-64.0
cis-1,3-Dichloropropene ND ug/kg 1 07/13/11 01:40 10061-01-54.0
trans-1,3-Dichloropropene ND ug/kg 1 07/13/11 01:40 10061-02-64.0
Diisopropyl ether ND ug/kg 1 07/13/11 01:40 108-20-34.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 102 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 11A (6-7)Lab ID:9297694020 Collected:07/07/11 09:40 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/13/11 01:40 100-41-44.0
Hexachloro-1,3-butadiene ND ug/kg 1 07/13/11 01:40 87-68-34.0
2-Hexanone ND ug/kg 1 07/13/11 01:40 591-78-639.8
Isopropylbenzene (Cumene)ND ug/kg 1 07/13/11 01:40 98-82-84.0
p-Isopropyltoluene ND ug/kg 1 07/13/11 01:40 99-87-64.0
Methylene Chloride ND ug/kg 1 07/13/11 01:40 75-09-215.9
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/13/11 01:40 108-10-139.8
Methyl-tert-butyl ether ND ug/kg 1 07/13/11 01:40 1634-04-44.0
Naphthalene ND ug/kg 1 07/13/11 01:40 91-20-34.0
n-Propylbenzene ND ug/kg 1 07/13/11 01:40 103-65-14.0
Styrene ND ug/kg 1 07/13/11 01:40 100-42-54.0
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/13/11 01:40 630-20-64.0
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/13/11 01:40 79-34-54.0
Tetrachloroethene ND ug/kg 1 07/13/11 01:40 127-18-44.0
Toluene ND ug/kg 1 07/13/11 01:40 108-88-34.0
1,2,3-Trichlorobenzene ND ug/kg 1 07/13/11 01:40 87-61-64.0
1,2,4-Trichlorobenzene ND ug/kg 1 07/13/11 01:40 120-82-14.0
1,1,1-Trichloroethane ND ug/kg 1 07/13/11 01:40 71-55-64.0
1,1,2-Trichloroethane ND ug/kg 1 07/13/11 01:40 79-00-54.0
Trichloroethene ND ug/kg 1 07/13/11 01:40 79-01-64.0
Trichlorofluoromethane ND ug/kg 1 07/13/11 01:40 75-69-44.0
1,2,3-Trichloropropane ND ug/kg 1 07/13/11 01:40 96-18-44.0
1,2,4-Trimethylbenzene ND ug/kg 1 07/13/11 01:40 95-63-64.0
1,3,5-Trimethylbenzene ND ug/kg 1 07/13/11 01:40 108-67-84.0
Vinyl acetate ND ug/kg 1 07/13/11 01:40 108-05-439.8
Vinyl chloride ND ug/kg 1 07/13/11 01:40 75-01-48.0
Xylene (Total)ND ug/kg 1 07/13/11 01:40 1330-20-78.0
m&p-Xylene ND ug/kg 1 07/13/11 01:40 179601-23-18.0
o-Xylene ND ug/kg 1 07/13/11 01:40 95-47-64.0
Dibromofluoromethane (S)91 %1 07/13/11 01:40 1868-53-770-130
Toluene-d8 (S)99 %1 07/13/11 01:40 2037-26-570-130
4-Bromofluorobenzene (S)91 %1 07/13/11 01:40 460-00-470-130
1,2-Dichloroethane-d4 (S)84 %1 07/13/11 01:40 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 12.2 %1 07/08/11 09:000.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 103 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 11A (8-9)Lab ID:9297694021 Collected:07/07/11 09:50 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components ND mg/kg 1 07/12/11 09:07 68334-30-507/08/11 10:276.0
n-Pentacosane (S)72 %1 07/12/11 09:07 629-99-207/08/11 10:2741-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease ND mg/kg 1 07/14/11 11:2007/14/11 10:4483.5
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/13/11 04:10 8006-61-907/12/11 14:506.6
4-Bromofluorobenzene (S)126 %1 07/13/11 04:10 460-00-407/12/11 14:5070-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 3.1 mg/kg 1 07/13/11 20:40 7440-38-207/12/11 11:400.54
Barium 110 mg/kg 1 07/13/11 20:40 7440-39-307/12/11 11:400.54
Cadmium ND mg/kg 1 07/13/11 20:40 7440-43-907/12/11 11:400.11
Chromium 6.8 mg/kg 1 07/13/11 20:40 7440-47-307/12/11 11:400.54
Lead 11.6 mg/kg 1 07/13/11 20:40 7439-92-107/12/11 11:400.54
Selenium 1.6 mg/kg 1 07/13/11 20:40 7782-49-207/12/11 11:401.1
Silver ND mg/kg 1 07/13/11 20:40 7440-22-407/12/11 11:400.54
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.030 mg/kg 1 07/15/11 15:11 7439-97-607/14/11 15:100.0053
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/13/11 17:38 83-32-907/11/11 10:00394
Acenaphthylene ND ug/kg 1 07/13/11 17:38 208-96-807/11/11 10:00394
Aniline ND ug/kg 1 07/13/11 17:38 62-53-307/11/11 10:00394
Anthracene ND ug/kg 1 07/13/11 17:38 120-12-707/11/11 10:00394
Benzo(a)anthracene ND ug/kg 1 07/13/11 17:38 56-55-307/11/11 10:00394
Benzo(a)pyrene ND ug/kg 1 07/13/11 17:38 50-32-807/11/11 10:00394
Benzo(b)fluoranthene ND ug/kg 1 07/13/11 17:38 205-99-207/11/11 10:00394
Benzo(g,h,i)perylene ND ug/kg 1 07/13/11 17:38 191-24-207/11/11 10:00394
Benzo(k)fluoranthene ND ug/kg 1 07/13/11 17:38 207-08-907/11/11 10:00394
Benzoic Acid ND ug/kg 1 07/13/11 17:38 65-85-007/11/11 10:001970
Benzyl alcohol ND ug/kg 1 07/13/11 17:38 100-51-607/11/11 10:00788
4-Bromophenylphenyl ether ND ug/kg 1 07/13/11 17:38 101-55-307/11/11 10:00394
Butylbenzylphthalate ND ug/kg 1 07/13/11 17:38 85-68-707/11/11 10:00394
4-Chloro-3-methylphenol ND ug/kg 1 07/13/11 17:38 59-50-707/11/11 10:00788
4-Chloroaniline ND ug/kg 1 07/13/11 17:38 106-47-807/11/11 10:001970
bis(2-Chloroethoxy)methane ND ug/kg 1 07/13/11 17:38 111-91-107/11/11 10:00394
bis(2-Chloroethyl) ether ND ug/kg 1 07/13/11 17:38 111-44-407/11/11 10:00394
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/13/11 17:38 108-60-107/11/11 10:00394
2-Chloronaphthalene ND ug/kg 1 07/13/11 17:38 91-58-707/11/11 10:00394
2-Chlorophenol ND ug/kg 1 07/13/11 17:38 95-57-807/11/11 10:00394
4-Chlorophenylphenyl ether ND ug/kg 1 07/13/11 17:38 7005-72-307/11/11 10:00394
Chrysene ND ug/kg 1 07/13/11 17:38 218-01-907/11/11 10:00394
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 104 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 11A (8-9)Lab ID:9297694021 Collected:07/07/11 09:50 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/13/11 17:38 53-70-307/11/11 10:00394
Dibenzofuran ND ug/kg 1 07/13/11 17:38 132-64-907/11/11 10:00394
1,2-Dichlorobenzene ND ug/kg 1 07/13/11 17:38 95-50-107/11/11 10:00394
1,3-Dichlorobenzene ND ug/kg 1 07/13/11 17:38 541-73-107/11/11 10:00394
1,4-Dichlorobenzene ND ug/kg 1 07/13/11 17:38 106-46-707/11/11 10:00394
3,3'-Dichlorobenzidine ND ug/kg 1 07/13/11 17:38 91-94-107/11/11 10:001970
2,4-Dichlorophenol ND ug/kg 1 07/13/11 17:38 120-83-207/11/11 10:00394
Diethylphthalate ND ug/kg 1 07/13/11 17:38 84-66-207/11/11 10:00394
2,4-Dimethylphenol ND ug/kg 1 07/13/11 17:38 105-67-907/11/11 10:00394
Dimethylphthalate ND ug/kg 1 07/13/11 17:38 131-11-307/11/11 10:00394
Di-n-butylphthalate ND ug/kg 1 07/13/11 17:38 84-74-207/11/11 10:00394
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/13/11 17:38 534-52-107/11/11 10:00788
2,4-Dinitrophenol ND ug/kg 1 07/13/11 17:38 51-28-507/11/11 10:001970
2,4-Dinitrotoluene ND ug/kg 1 07/13/11 17:38 121-14-207/11/11 10:00394
2,6-Dinitrotoluene ND ug/kg 1 07/13/11 17:38 606-20-207/11/11 10:00394
Di-n-octylphthalate ND ug/kg 1 07/13/11 17:38 117-84-007/11/11 10:00394
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/13/11 17:38 117-81-707/11/11 10:00394
Fluoranthene ND ug/kg 1 07/13/11 17:38 206-44-007/11/11 10:00394
Fluorene ND ug/kg 1 07/13/11 17:38 86-73-707/11/11 10:00394
Hexachloro-1,3-butadiene ND ug/kg 1 07/13/11 17:38 87-68-307/11/11 10:00394
Hexachlorobenzene ND ug/kg 1 07/13/11 17:38 118-74-107/11/11 10:00394
Hexachlorocyclopentadiene ND ug/kg 1 07/13/11 17:38 77-47-407/11/11 10:00394
Hexachloroethane ND ug/kg 1 07/13/11 17:38 67-72-107/11/11 10:00394
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/13/11 17:38 193-39-507/11/11 10:00394
Isophorone ND ug/kg 1 07/13/11 17:38 78-59-107/11/11 10:00394
1-Methylnaphthalene ND ug/kg 1 07/13/11 17:38 90-12-007/11/11 10:00394
2-Methylnaphthalene ND ug/kg 1 07/13/11 17:38 91-57-607/11/11 10:00394
2-Methylphenol(o-Cresol)ND ug/kg 1 07/13/11 17:38 95-48-707/11/11 10:00394
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/13/11 17:3807/11/11 10:00394
Naphthalene ND ug/kg 1 07/13/11 17:38 91-20-307/11/11 10:00394
2-Nitroaniline ND ug/kg 1 07/13/11 17:38 88-74-407/11/11 10:001970
3-Nitroaniline ND ug/kg 1 07/13/11 17:38 99-09-207/11/11 10:001970
4-Nitroaniline ND ug/kg 1 07/13/11 17:38 100-01-607/11/11 10:00788
Nitrobenzene ND ug/kg 1 07/13/11 17:38 98-95-307/11/11 10:00394
2-Nitrophenol ND ug/kg 1 07/13/11 17:38 88-75-507/11/11 10:00394
4-Nitrophenol ND ug/kg 1 07/13/11 17:38 100-02-707/11/11 10:001970
N-Nitrosodimethylamine ND ug/kg 1 07/13/11 17:38 62-75-907/11/11 10:00394
N-Nitroso-di-n-propylamine ND ug/kg 1 07/13/11 17:38 621-64-707/11/11 10:00394
N-Nitrosodiphenylamine ND ug/kg 1 07/13/11 17:38 86-30-607/11/11 10:00394
Pentachlorophenol ND ug/kg 1 07/13/11 17:38 87-86-507/11/11 10:001970
Phenanthrene ND ug/kg 1 07/13/11 17:38 85-01-807/11/11 10:00394
Phenol ND ug/kg 1 07/13/11 17:38 108-95-207/11/11 10:00394
Pyrene ND ug/kg 1 07/13/11 17:38 129-00-007/11/11 10:00394
1,2,4-Trichlorobenzene ND ug/kg 1 07/13/11 17:38 120-82-107/11/11 10:00394
2,4,5-Trichlorophenol ND ug/kg 1 07/13/11 17:38 95-95-407/11/11 10:00394
2,4,6-Trichlorophenol ND ug/kg 1 07/13/11 17:38 88-06-207/11/11 10:00394
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 105 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 11A (8-9)Lab ID:9297694021 Collected:07/07/11 09:50 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)71 %1 07/13/11 17:38 4165-60-007/11/11 10:0023-110
2-Fluorobiphenyl (S)65 %1 07/13/11 17:38 321-60-807/11/11 10:0030-110
Terphenyl-d14 (S)89 %1 07/13/11 17:38 1718-51-007/11/11 10:0028-110
Phenol-d6 (S)53 %1 07/13/11 17:38 13127-88-307/11/11 10:0022-110
2-Fluorophenol (S)56 %1 07/13/11 17:38 367-12-407/11/11 10:0013-110
2,4,6-Tribromophenol (S)63 %1 07/13/11 17:38 118-79-607/11/11 10:0027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/13/11 02:00 67-64-1105
Benzene ND ug/kg 1 07/13/11 02:00 71-43-25.3
Bromobenzene ND ug/kg 1 07/13/11 02:00 108-86-15.3
Bromochloromethane ND ug/kg 1 07/13/11 02:00 74-97-55.3
Bromodichloromethane ND ug/kg 1 07/13/11 02:00 75-27-45.3
Bromoform ND ug/kg 1 07/13/11 02:00 75-25-25.3
Bromomethane ND ug/kg 1 07/13/11 02:00 74-83-910.5
2-Butanone (MEK)ND ug/kg 1 07/13/11 02:00 78-93-3105
n-Butylbenzene ND ug/kg 1 07/13/11 02:00 104-51-85.3
sec-Butylbenzene ND ug/kg 1 07/13/11 02:00 135-98-85.3
tert-Butylbenzene ND ug/kg 1 07/13/11 02:00 98-06-65.3
Carbon tetrachloride ND ug/kg 1 07/13/11 02:00 56-23-55.3
Chlorobenzene ND ug/kg 1 07/13/11 02:00 108-90-75.3
Chloroethane ND ug/kg 1 07/13/11 02:00 75-00-310.5
Chloroform ND ug/kg 1 07/13/11 02:00 67-66-35.3
Chloromethane ND ug/kg 1 07/13/11 02:00 74-87-310.5
2-Chlorotoluene ND ug/kg 1 07/13/11 02:00 95-49-85.3
4-Chlorotoluene ND ug/kg 1 07/13/11 02:00 106-43-45.3
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/13/11 02:00 96-12-85.3
Dibromochloromethane ND ug/kg 1 07/13/11 02:00 124-48-15.3
1,2-Dibromoethane (EDB)ND ug/kg 1 07/13/11 02:00 106-93-45.3
Dibromomethane ND ug/kg 1 07/13/11 02:00 74-95-35.3
1,2-Dichlorobenzene ND ug/kg 1 07/13/11 02:00 95-50-15.3
1,3-Dichlorobenzene ND ug/kg 1 07/13/11 02:00 541-73-15.3
1,4-Dichlorobenzene ND ug/kg 1 07/13/11 02:00 106-46-75.3
Dichlorodifluoromethane ND ug/kg 1 07/13/11 02:00 75-71-810.5
1,1-Dichloroethane ND ug/kg 1 07/13/11 02:00 75-34-35.3
1,2-Dichloroethane ND ug/kg 1 07/13/11 02:00 107-06-25.3
1,1-Dichloroethene ND ug/kg 1 07/13/11 02:00 75-35-45.3
cis-1,2-Dichloroethene ND ug/kg 1 07/13/11 02:00 156-59-25.3
trans-1,2-Dichloroethene ND ug/kg 1 07/13/11 02:00 156-60-55.3
1,2-Dichloropropane ND ug/kg 1 07/13/11 02:00 78-87-55.3
1,3-Dichloropropane ND ug/kg 1 07/13/11 02:00 142-28-95.3
2,2-Dichloropropane ND ug/kg 1 07/13/11 02:00 594-20-75.3
1,1-Dichloropropene ND ug/kg 1 07/13/11 02:00 563-58-65.3
cis-1,3-Dichloropropene ND ug/kg 1 07/13/11 02:00 10061-01-55.3
trans-1,3-Dichloropropene ND ug/kg 1 07/13/11 02:00 10061-02-65.3
Diisopropyl ether ND ug/kg 1 07/13/11 02:00 108-20-35.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 106 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 11A (8-9)Lab ID:9297694021 Collected:07/07/11 09:50 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/13/11 02:00 100-41-45.3
Hexachloro-1,3-butadiene ND ug/kg 1 07/13/11 02:00 87-68-35.3
2-Hexanone ND ug/kg 1 07/13/11 02:00 591-78-652.7
Isopropylbenzene (Cumene)ND ug/kg 1 07/13/11 02:00 98-82-85.3
p-Isopropyltoluene ND ug/kg 1 07/13/11 02:00 99-87-65.3
Methylene Chloride ND ug/kg 1 07/13/11 02:00 75-09-221.1
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/13/11 02:00 108-10-152.7
Methyl-tert-butyl ether ND ug/kg 1 07/13/11 02:00 1634-04-45.3
Naphthalene ND ug/kg 1 07/13/11 02:00 91-20-35.3
n-Propylbenzene ND ug/kg 1 07/13/11 02:00 103-65-15.3
Styrene ND ug/kg 1 07/13/11 02:00 100-42-55.3
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/13/11 02:00 630-20-65.3
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/13/11 02:00 79-34-55.3
Tetrachloroethene ND ug/kg 1 07/13/11 02:00 127-18-45.3
Toluene ND ug/kg 1 07/13/11 02:00 108-88-35.3
1,2,3-Trichlorobenzene ND ug/kg 1 07/13/11 02:00 87-61-65.3
1,2,4-Trichlorobenzene ND ug/kg 1 07/13/11 02:00 120-82-15.3
1,1,1-Trichloroethane ND ug/kg 1 07/13/11 02:00 71-55-65.3
1,1,2-Trichloroethane ND ug/kg 1 07/13/11 02:00 79-00-55.3
Trichloroethene ND ug/kg 1 07/13/11 02:00 79-01-65.3
Trichlorofluoromethane ND ug/kg 1 07/13/11 02:00 75-69-45.3
1,2,3-Trichloropropane ND ug/kg 1 07/13/11 02:00 96-18-45.3
1,2,4-Trimethylbenzene ND ug/kg 1 07/13/11 02:00 95-63-65.3
1,3,5-Trimethylbenzene ND ug/kg 1 07/13/11 02:00 108-67-85.3
Vinyl acetate ND ug/kg 1 07/13/11 02:00 108-05-452.7
Vinyl chloride ND ug/kg 1 07/13/11 02:00 75-01-410.5
Xylene (Total)ND ug/kg 1 07/13/11 02:00 1330-20-710.5
m&p-Xylene ND ug/kg 1 07/13/11 02:00 179601-23-110.5
o-Xylene ND ug/kg 1 07/13/11 02:00 95-47-65.3
Dibromofluoromethane (S)91 %1 07/13/11 02:00 1868-53-770-130
Toluene-d8 (S)99 %1 07/13/11 02:00 2037-26-570-130
4-Bromofluorobenzene (S)94 %1 07/13/11 02:00 460-00-470-130
1,2-Dichloroethane-d4 (S)82 %1 07/13/11 02:00 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 16.2 %1 07/08/11 09:010.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 107 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 9A (15-16)Lab ID:9297694022 Collected:07/07/11 10:45 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 214 mg/kg 1 07/12/11 09:35 68334-30-5 P307/08/11 10:2730.7
n-Pentacosane (S)0 %1 07/12/11 09:35 629-99-2 S407/08/11 10:2741-119
9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B
Oil and Grease 1110 mg/kg 1 07/14/11 11:2007/14/11 10:4586.0
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/13/11 04:35 8006-61-907/12/11 14:506.6
4-Bromofluorobenzene (S)159 %1 07/13/11 04:35 460-00-407/12/11 14:5070-167
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 2.9 mg/kg 1 07/13/11 20:45 7440-38-207/12/11 11:400.50
Barium 85.7 mg/kg 1 07/13/11 20:45 7440-39-307/12/11 11:400.50
Cadmium ND mg/kg 1 07/13/11 20:45 7440-43-907/12/11 11:400.099
Chromium 14.8 mg/kg 1 07/13/11 20:45 7440-47-307/12/11 11:400.50
Lead 28.4 mg/kg 1 07/13/11 20:45 7439-92-107/12/11 11:400.50
Selenium 1.4 mg/kg 1 07/13/11 20:45 7782-49-207/12/11 11:400.99
Silver ND mg/kg 1 07/13/11 20:45 7440-22-407/12/11 11:400.50
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.063 mg/kg 1 07/15/11 15:19 7439-97-607/14/11 15:100.0048
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/14/11 14:53 83-32-907/11/11 10:002030
Acenaphthylene ND ug/kg 1 07/14/11 14:53 208-96-807/11/11 10:002030
Aniline ND ug/kg 1 07/14/11 14:53 62-53-307/11/11 10:002030
Anthracene ND ug/kg 1 07/14/11 14:53 120-12-707/11/11 10:002030
Benzo(a)anthracene ND ug/kg 1 07/14/11 14:53 56-55-307/11/11 10:002030
Benzo(a)pyrene ND ug/kg 1 07/14/11 14:53 50-32-807/11/11 10:002030
Benzo(b)fluoranthene ND ug/kg 1 07/14/11 14:53 205-99-207/11/11 10:002030
Benzo(g,h,i)perylene ND ug/kg 1 07/14/11 14:53 191-24-207/11/11 10:002030
Benzo(k)fluoranthene ND ug/kg 1 07/14/11 14:53 207-08-907/11/11 10:002030
Benzoic Acid ND ug/kg 1 07/14/11 14:53 65-85-007/11/11 10:0010100
Benzyl alcohol ND ug/kg 1 07/14/11 14:53 100-51-607/11/11 10:004050
4-Bromophenylphenyl ether ND ug/kg 1 07/14/11 14:53 101-55-307/11/11 10:002030
Butylbenzylphthalate ND ug/kg 1 07/14/11 14:53 85-68-707/11/11 10:002030
4-Chloro-3-methylphenol ND ug/kg 1 07/14/11 14:53 59-50-707/11/11 10:004050
4-Chloroaniline ND ug/kg 1 07/14/11 14:53 106-47-807/11/11 10:0010100
bis(2-Chloroethoxy)methane ND ug/kg 1 07/14/11 14:53 111-91-107/11/11 10:002030
bis(2-Chloroethyl) ether ND ug/kg 1 07/14/11 14:53 111-44-407/11/11 10:002030
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/14/11 14:53 108-60-107/11/11 10:002030
2-Chloronaphthalene ND ug/kg 1 07/14/11 14:53 91-58-707/11/11 10:002030
2-Chlorophenol ND ug/kg 1 07/14/11 14:53 95-57-807/11/11 10:002030
4-Chlorophenylphenyl ether ND ug/kg 1 07/14/11 14:53 7005-72-307/11/11 10:002030
Chrysene ND ug/kg 1 07/14/11 14:53 218-01-907/11/11 10:002030
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 108 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 9A (15-16)Lab ID:9297694022 Collected:07/07/11 10:45 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dibenz(a,h)anthracene ND ug/kg 1 07/14/11 14:53 53-70-307/11/11 10:002030
Dibenzofuran ND ug/kg 1 07/14/11 14:53 132-64-907/11/11 10:002030
1,2-Dichlorobenzene ND ug/kg 1 07/14/11 14:53 95-50-107/11/11 10:002030
1,3-Dichlorobenzene ND ug/kg 1 07/14/11 14:53 541-73-107/11/11 10:002030
1,4-Dichlorobenzene ND ug/kg 1 07/14/11 14:53 106-46-707/11/11 10:002030
3,3'-Dichlorobenzidine ND ug/kg 1 07/14/11 14:53 91-94-107/11/11 10:0010100
2,4-Dichlorophenol ND ug/kg 1 07/14/11 14:53 120-83-207/11/11 10:002030
Diethylphthalate ND ug/kg 1 07/14/11 14:53 84-66-207/11/11 10:002030
2,4-Dimethylphenol ND ug/kg 1 07/14/11 14:53 105-67-907/11/11 10:002030
Dimethylphthalate ND ug/kg 1 07/14/11 14:53 131-11-307/11/11 10:002030
Di-n-butylphthalate ND ug/kg 1 07/14/11 14:53 84-74-207/11/11 10:002030
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/14/11 14:53 534-52-107/11/11 10:004050
2,4-Dinitrophenol ND ug/kg 1 07/14/11 14:53 51-28-507/11/11 10:0010100
2,4-Dinitrotoluene ND ug/kg 1 07/14/11 14:53 121-14-207/11/11 10:002030
2,6-Dinitrotoluene ND ug/kg 1 07/14/11 14:53 606-20-207/11/11 10:002030
Di-n-octylphthalate ND ug/kg 1 07/14/11 14:53 117-84-007/11/11 10:002030
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/14/11 14:53 117-81-707/11/11 10:002030
Fluoranthene ND ug/kg 1 07/14/11 14:53 206-44-007/11/11 10:002030
Fluorene ND ug/kg 1 07/14/11 14:53 86-73-707/11/11 10:002030
Hexachloro-1,3-butadiene ND ug/kg 1 07/14/11 14:53 87-68-307/11/11 10:002030
Hexachlorobenzene ND ug/kg 1 07/14/11 14:53 118-74-107/11/11 10:002030
Hexachlorocyclopentadiene ND ug/kg 1 07/14/11 14:53 77-47-407/11/11 10:002030
Hexachloroethane ND ug/kg 1 07/14/11 14:53 67-72-107/11/11 10:002030
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/14/11 14:53 193-39-507/11/11 10:002030
Isophorone ND ug/kg 1 07/14/11 14:53 78-59-107/11/11 10:002030
1-Methylnaphthalene ND ug/kg 1 07/14/11 14:53 90-12-007/11/11 10:002030
2-Methylnaphthalene ND ug/kg 1 07/14/11 14:53 91-57-607/11/11 10:002030
2-Methylphenol(o-Cresol)ND ug/kg 1 07/14/11 14:53 95-48-707/11/11 10:002030
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/14/11 14:5307/11/11 10:002030
Naphthalene ND ug/kg 1 07/14/11 14:53 91-20-307/11/11 10:002030
2-Nitroaniline ND ug/kg 1 07/14/11 14:53 88-74-407/11/11 10:0010100
3-Nitroaniline ND ug/kg 1 07/14/11 14:53 99-09-207/11/11 10:0010100
4-Nitroaniline ND ug/kg 1 07/14/11 14:53 100-01-607/11/11 10:004050
Nitrobenzene ND ug/kg 1 07/14/11 14:53 98-95-307/11/11 10:002030
2-Nitrophenol ND ug/kg 1 07/14/11 14:53 88-75-507/11/11 10:002030
4-Nitrophenol ND ug/kg 1 07/14/11 14:53 100-02-707/11/11 10:0010100
N-Nitrosodimethylamine ND ug/kg 1 07/14/11 14:53 62-75-907/11/11 10:002030
N-Nitroso-di-n-propylamine ND ug/kg 1 07/14/11 14:53 621-64-707/11/11 10:002030
N-Nitrosodiphenylamine ND ug/kg 1 07/14/11 14:53 86-30-607/11/11 10:002030
Pentachlorophenol ND ug/kg 1 07/14/11 14:53 87-86-507/11/11 10:0010100
Phenanthrene ND ug/kg 1 07/14/11 14:53 85-01-807/11/11 10:002030
Phenol ND ug/kg 1 07/14/11 14:53 108-95-2 P307/11/11 10:002030
Pyrene ND ug/kg 1 07/14/11 14:53 129-00-007/11/11 10:002030
1,2,4-Trichlorobenzene ND ug/kg 1 07/14/11 14:53 120-82-107/11/11 10:002030
2,4,5-Trichlorophenol ND ug/kg 1 07/14/11 14:53 95-95-407/11/11 10:002030
2,4,6-Trichlorophenol ND ug/kg 1 07/14/11 14:53 88-06-207/11/11 10:002030
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 109 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 9A (15-16)Lab ID:9297694022 Collected:07/07/11 10:45 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Nitrobenzene-d5 (S)42 %1 07/14/11 14:53 4165-60-007/11/11 10:0023-110
2-Fluorobiphenyl (S)64 %1 07/14/11 14:53 321-60-807/11/11 10:0030-110
Terphenyl-d14 (S)77 %1 07/14/11 14:53 1718-51-007/11/11 10:0028-110
Phenol-d6 (S)57 %1 07/14/11 14:53 13127-88-307/11/11 10:0022-110
2-Fluorophenol (S)66 %1 07/14/11 14:53 367-12-407/11/11 10:0013-110
2,4,6-Tribromophenol (S)66 %1 07/14/11 14:53 118-79-607/11/11 10:0027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/13/11 02:20 67-64-189.5
Benzene ND ug/kg 1 07/13/11 02:20 71-43-24.5
Bromobenzene ND ug/kg 1 07/13/11 02:20 108-86-14.5
Bromochloromethane ND ug/kg 1 07/13/11 02:20 74-97-54.5
Bromodichloromethane ND ug/kg 1 07/13/11 02:20 75-27-44.5
Bromoform ND ug/kg 1 07/13/11 02:20 75-25-24.5
Bromomethane ND ug/kg 1 07/13/11 02:20 74-83-99.0
2-Butanone (MEK)ND ug/kg 1 07/13/11 02:20 78-93-389.5
n-Butylbenzene ND ug/kg 1 07/13/11 02:20 104-51-84.5
sec-Butylbenzene ND ug/kg 1 07/13/11 02:20 135-98-84.5
tert-Butylbenzene ND ug/kg 1 07/13/11 02:20 98-06-64.5
Carbon tetrachloride ND ug/kg 1 07/13/11 02:20 56-23-54.5
Chlorobenzene ND ug/kg 1 07/13/11 02:20 108-90-74.5
Chloroethane ND ug/kg 1 07/13/11 02:20 75-00-39.0
Chloroform ND ug/kg 1 07/13/11 02:20 67-66-34.5
Chloromethane ND ug/kg 1 07/13/11 02:20 74-87-39.0
2-Chlorotoluene ND ug/kg 1 07/13/11 02:20 95-49-84.5
4-Chlorotoluene ND ug/kg 1 07/13/11 02:20 106-43-44.5
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/13/11 02:20 96-12-84.5
Dibromochloromethane ND ug/kg 1 07/13/11 02:20 124-48-14.5
1,2-Dibromoethane (EDB)ND ug/kg 1 07/13/11 02:20 106-93-44.5
Dibromomethane ND ug/kg 1 07/13/11 02:20 74-95-34.5
1,2-Dichlorobenzene ND ug/kg 1 07/13/11 02:20 95-50-14.5
1,3-Dichlorobenzene ND ug/kg 1 07/13/11 02:20 541-73-14.5
1,4-Dichlorobenzene ND ug/kg 1 07/13/11 02:20 106-46-74.5
Dichlorodifluoromethane ND ug/kg 1 07/13/11 02:20 75-71-89.0
1,1-Dichloroethane ND ug/kg 1 07/13/11 02:20 75-34-34.5
1,2-Dichloroethane ND ug/kg 1 07/13/11 02:20 107-06-24.5
1,1-Dichloroethene ND ug/kg 1 07/13/11 02:20 75-35-44.5
cis-1,2-Dichloroethene ND ug/kg 1 07/13/11 02:20 156-59-24.5
trans-1,2-Dichloroethene ND ug/kg 1 07/13/11 02:20 156-60-54.5
1,2-Dichloropropane ND ug/kg 1 07/13/11 02:20 78-87-54.5
1,3-Dichloropropane ND ug/kg 1 07/13/11 02:20 142-28-94.5
2,2-Dichloropropane ND ug/kg 1 07/13/11 02:20 594-20-74.5
1,1-Dichloropropene ND ug/kg 1 07/13/11 02:20 563-58-64.5
cis-1,3-Dichloropropene ND ug/kg 1 07/13/11 02:20 10061-01-54.5
trans-1,3-Dichloropropene ND ug/kg 1 07/13/11 02:20 10061-02-64.5
Diisopropyl ether ND ug/kg 1 07/13/11 02:20 108-20-34.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 110 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Sample:TESTPIT 9A (15-16)Lab ID:9297694022 Collected:07/07/11 10:45 Received:07/07/11 12:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/13/11 02:20 100-41-44.5
Hexachloro-1,3-butadiene ND ug/kg 1 07/13/11 02:20 87-68-34.5
2-Hexanone ND ug/kg 1 07/13/11 02:20 591-78-644.8
Isopropylbenzene (Cumene)ND ug/kg 1 07/13/11 02:20 98-82-84.5
p-Isopropyltoluene ND ug/kg 1 07/13/11 02:20 99-87-64.5
Methylene Chloride ND ug/kg 1 07/13/11 02:20 75-09-217.9
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/13/11 02:20 108-10-144.8
Methyl-tert-butyl ether ND ug/kg 1 07/13/11 02:20 1634-04-44.5
Naphthalene ND ug/kg 1 07/13/11 02:20 91-20-34.5
n-Propylbenzene ND ug/kg 1 07/13/11 02:20 103-65-14.5
Styrene ND ug/kg 1 07/13/11 02:20 100-42-54.5
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/13/11 02:20 630-20-64.5
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/13/11 02:20 79-34-54.5
Tetrachloroethene ND ug/kg 1 07/13/11 02:20 127-18-44.5
Toluene ND ug/kg 1 07/13/11 02:20 108-88-34.5
1,2,3-Trichlorobenzene ND ug/kg 1 07/13/11 02:20 87-61-64.5
1,2,4-Trichlorobenzene ND ug/kg 1 07/13/11 02:20 120-82-14.5
1,1,1-Trichloroethane ND ug/kg 1 07/13/11 02:20 71-55-64.5
1,1,2-Trichloroethane ND ug/kg 1 07/13/11 02:20 79-00-54.5
Trichloroethene ND ug/kg 1 07/13/11 02:20 79-01-64.5
Trichlorofluoromethane ND ug/kg 1 07/13/11 02:20 75-69-44.5
1,2,3-Trichloropropane ND ug/kg 1 07/13/11 02:20 96-18-44.5
1,2,4-Trimethylbenzene ND ug/kg 1 07/13/11 02:20 95-63-64.5
1,3,5-Trimethylbenzene ND ug/kg 1 07/13/11 02:20 108-67-84.5
Vinyl acetate ND ug/kg 1 07/13/11 02:20 108-05-444.8
Vinyl chloride ND ug/kg 1 07/13/11 02:20 75-01-49.0
Xylene (Total)ND ug/kg 1 07/13/11 02:20 1330-20-79.0
m&p-Xylene ND ug/kg 1 07/13/11 02:20 179601-23-19.0
o-Xylene ND ug/kg 1 07/13/11 02:20 95-47-64.5
Dibromofluoromethane (S)104 %1 07/13/11 02:20 1868-53-770-130
Toluene-d8 (S)96 %1 07/13/11 02:20 2037-26-570-130
4-Bromofluorobenzene (S)85 %1 07/13/11 02:20 460-00-470-130
1,2-Dichloroethane-d4 (S)89 %1 07/13/11 02:20 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 18.6 %1 07/08/11 09:010.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 111 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/14158
EPA 3546
EPA 8015 Modified
8015 Solid GCSV
Associated Lab Samples:9297694001, 9297694002, 9297694003, 9297694004, 9297694005, 9297694006, 9297694007, 9297694008,
9297694009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:630878
Associated Lab Samples:9297694001, 9297694002, 9297694003, 9297694004, 9297694005, 9297694006, 9297694007, 9297694008,
9297694009
Matrix:Solid
Analyzed
Diesel Components mg/kg ND 5.0 07/11/11 21:51
n-Pentacosane (S)%68 41-119 07/11/11 21:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
630879LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Components mg/kg 44.266.7 66 49-113
n-Pentacosane (S)%72 41-119
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
630880MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9297644016
630881
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Diesel Components mg/kg 90.3 50 10-14655 1090.36.4J 51.2 56.5
n-Pentacosane (S)%58 41-11962
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 112 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/14160
EPA 3546
EPA 8015 Modified
8015 Solid GCSV
Associated Lab Samples:9297694010, 9297694011, 9297694012, 9297694013, 9297694014, 9297694015, 9297694016, 9297694017,
9297694018, 9297694019, 9297694020, 9297694021, 9297694022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:631095
Associated Lab Samples:9297694010, 9297694011, 9297694012, 9297694013, 9297694014, 9297694015, 9297694016, 9297694017,
9297694018, 9297694019, 9297694020, 9297694021, 9297694022
Matrix:Solid
Analyzed
Diesel Components mg/kg ND 5.0 07/12/11 03:29
n-Pentacosane (S)%69 41-119 07/12/11 03:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
631096LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Components mg/kg 46.566.7 70 49-113
n-Pentacosane (S)%71 41-119
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
631097MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9297694011
631098
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Diesel Components mg/kg 76.4 58 10-14666 1076.413.4 57.8 63.7
n-Pentacosane (S)%67 41-11976
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 113 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCSV/10103
9071B
9071B
9071 Oil and Grease
Associated Lab Samples:9297694001, 9297694002, 9297694003, 9297694004, 9297694005, 9297694006, 9297694007, 9297694008,
9297694009, 9297694010, 9297694011, 9297694012, 9297694013, 9297694014, 9297694015, 9297694016,
9297694017, 9297694018, 9297694019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:631932
Associated Lab Samples:9297694001, 9297694002, 9297694003, 9297694004, 9297694005, 9297694006, 9297694007, 9297694008,
9297694009, 9297694010, 9297694011, 9297694012, 9297694013, 9297694014, 9297694015, 9297694016,
9297694017, 9297694018, 9297694019
Matrix:Solid
Analyzed
Oil and Grease mg/kg ND 70.0 07/11/11 12:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
631933LABORATORY CONTROL SAMPLE:
LCSSpike
Oil and Grease mg/kg 12701330 95 78-114
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
631934MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9297694005
631935
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Oil and Grease mg/kg M316906478-11457 111690ND11401020
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 114 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCSV/10118
9071B
9071B
9071 Oil and Grease
Associated Lab Samples:9297694020, 9297694021, 9297694022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:632742
Associated Lab Samples:9297694020, 9297694021, 9297694022
Matrix:Solid
Analyzed
Oil and Grease mg/kg ND 70.0 07/14/11 11:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
632743LABORATORY CONTROL SAMPLE:
LCSSpike
Oil and Grease mg/kg 12901330 97 78-114
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
632744MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9297694020
632745
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Oil and Grease mg/kg 1520 86 78-11493 81520ND13301450
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 115 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/5193
EPA 5035A/5030B
EPA 8015 Modified
Gasoline Range Organics
Associated Lab Samples:9297694001, 9297694002, 9297694003, 9297694004, 9297694005, 9297694006, 9297694007, 9297694008,
9297694009, 9297694010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:632283
Associated Lab Samples:9297694001, 9297694002, 9297694003, 9297694004, 9297694005, 9297694006, 9297694007, 9297694008,
9297694009, 9297694010
Matrix:Solid
Analyzed
Gasoline Range Organics mg/kg ND 6.0 07/12/11 11:10
4-Bromofluorobenzene (S)%143 70-167 07/12/11 11:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
632284LABORATORY CONTROL SAMPLE:
LCSSpike
Gasoline Range Organics mg/kg 25.825 103 70-165
4-Bromofluorobenzene (S)%95 70-167
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
632285MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9297667001
632286
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Gasoline Range Organics mg/kg 26.7 127 47-187121 426.7ND 36.7 35.2
4-Bromofluorobenzene (S)%97 70-167101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 116 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/5198
EPA 5035A/5030B
EPA 8015 Modified
Gasoline Range Organics
Associated Lab Samples:9297694011, 9297694012, 9297694013, 9297694014, 9297694015, 9297694016, 9297694017, 9297694018,
9297694019, 9297694020, 9297694021, 9297694022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:632483
Associated Lab Samples:9297694011, 9297694012, 9297694013, 9297694014, 9297694015, 9297694016, 9297694017, 9297694018,
9297694019, 9297694020, 9297694021, 9297694022
Matrix:Solid
Analyzed
Gasoline Range Organics mg/kg ND 6.0 07/12/11 22:47
4-Bromofluorobenzene (S)%151 70-167 07/12/11 22:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
632484LABORATORY CONTROL SAMPLE:
LCSSpike
Gasoline Range Organics mg/kg 23.325 93 70-165
4-Bromofluorobenzene (S)%90 70-167
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
632485MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9297694012
632486
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Gasoline Range Organics mg/kg 22.2 141 47-187122 1422.2ND 31.5 27.2
4-Bromofluorobenzene (S)%133 70-16792
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 117 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/8714
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:9297694001, 9297694002, 9297694003, 9297694004, 9297694005, 9297694006, 9297694007, 9297694008,
9297694009, 9297694010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:632215
Associated Lab Samples:9297694001, 9297694002, 9297694003, 9297694004, 9297694005, 9297694006, 9297694007, 9297694008,
9297694009, 9297694010
Matrix:Solid
Analyzed
Arsenic mg/kg ND 0.50 07/13/11 14:06
Barium mg/kg ND 0.50 07/13/11 14:06
Cadmium mg/kg ND 0.10 07/13/11 14:06
Chromium mg/kg ND 0.50 07/13/11 14:06
Lead mg/kg ND 0.50 07/13/11 14:06
Selenium mg/kg ND 1.0 07/13/11 14:06
Silver mg/kg ND 0.50 07/13/11 14:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
632216LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 47.450 95 80-120
Barium mg/kg 48.050 96 80-120
Cadmium mg/kg 49.650 99 80-120
Chromium mg/kg 50.250 100 80-120
Lead mg/kg 49.150 98 80-120
Selenium mg/kg 47.650 95 80-120
Silver mg/kg 24.625 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
632217MATRIX SPIKE SAMPLE:
MSSpike
Result
9297122001
Arsenic mg/kg 10891 102 75-12514.4
Barium mg/kg 1540 M19121475-1251350
Cadmium mg/kg 84.691 91 75-1252.2
Chromium mg/kg 11791 100 75-12526.1
Lead mg/kg 11091 85 75-12532.4
Selenium mg/kg 91.091 100 75-125ND
Silver mg/kg 45.745.4 98 75-1250.93
Parameter Units
Dup
Result QualifiersRPDResult
9297452002
632218SAMPLE DUPLICATE:
Arsenic mg/kg NDND
Barium mg/kg .17JND
Cadmium mg/kg NDND
Chromium mg/kg .062JND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 118 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
Dup
Result QualifiersRPDResult
9297452002
632218SAMPLE DUPLICATE:
Lead mg/kg NDND
Selenium mg/kg 1.0 21.0
Silver mg/kg .095JND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 119 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/8715
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:9297694011, 9297694012, 9297694013, 9297694014, 9297694015, 9297694016, 9297694017, 9297694018,
9297694019, 9297694020, 9297694021, 9297694022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:632219
Associated Lab Samples:9297694011, 9297694012, 9297694013, 9297694014, 9297694015, 9297694016, 9297694017, 9297694018,
9297694019, 9297694020, 9297694021, 9297694022
Matrix:Solid
Analyzed
Arsenic mg/kg ND 0.50 07/13/11 19:28
Barium mg/kg ND 0.50 07/13/11 19:28
Cadmium mg/kg ND 0.10 07/13/11 19:28
Chromium mg/kg ND 0.50 07/13/11 19:28
Lead mg/kg ND 0.50 07/13/11 19:28
Selenium mg/kg ND 1.0 07/13/11 19:28
Silver mg/kg ND 0.50 07/13/11 19:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
632220LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 46.350 93 80-120
Barium mg/kg 46.850 94 80-120
Cadmium mg/kg 48.150 96 80-120
Chromium mg/kg 48.950 98 80-120
Lead mg/kg 47.750 95 80-120
Selenium mg/kg 45.750 91 80-120
Silver mg/kg 24.125 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
632221MATRIX SPIKE SAMPLE:
MSSpike
Result
9297694011
Arsenic mg/kg 46.151.1 85 75-1252.5
Barium mg/kg 16551.1 103 75-125112
Cadmium mg/kg 47.151.1 92 75-125ND
Chromium mg/kg 52.551.1 96 75-1253.3
Lead mg/kg 72.051.1 95 75-12523.3
Selenium mg/kg 45.251.1 88 75-125ND
Silver mg/kg 24.725.6 96 75-125ND
Parameter Units
Dup
Result QualifiersRPDResult
9297694012
632222SAMPLE DUPLICATE:
Arsenic mg/kg 2.5 132.2
Barium mg/kg 46.4 750.0
Cadmium mg/kg NDND
Chromium mg/kg 3.6 63.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 120 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
Dup
Result QualifiersRPDResult
9297694012
632222SAMPLE DUPLICATE:
Lead mg/kg 16.3 1719.3
Selenium mg/kg 1.3ND
Silver mg/kg .076JND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 121 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/3599
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:9297694001, 9297694002, 9297694003, 9297694004, 9297694005, 9297694006, 9297694007, 9297694008,
9297694009, 9297694010, 9297694011, 9297694012, 9297694013, 9297694014, 9297694015, 9297694016,
9297694017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:631149
Associated Lab Samples:9297694001, 9297694002, 9297694003, 9297694004, 9297694005, 9297694006, 9297694007, 9297694008,
9297694009, 9297694010, 9297694011, 9297694012, 9297694013, 9297694014, 9297694015, 9297694016,
9297694017
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0050 07/11/11 17:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
631150LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.055.067 83 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
631151MATRIX SPIKE SAMPLE:
MSSpike
Result
9297694001
Mercury mg/kg 0.082 M1.081 64 75-1250.031
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
631152MATRIX SPIKE SAMPLE:
MSSpike
Result
9297694002
Mercury mg/kg 0.050 M1.069 55 75-1250.012
Parameter Units
Dup
Result QualifiersRPDResult
9297694003
631153SAMPLE DUPLICATE:
Mercury mg/kg 0.016 40.016
Parameter Units
Dup
Result QualifiersRPDResult
9297694004
631154SAMPLE DUPLICATE:
Mercury mg/kg 0.028 D6270.021
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 122 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/3614
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:9297694018, 9297694019, 9297694020, 9297694021, 9297694022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:633662
Associated Lab Samples:9297694018, 9297694019, 9297694020, 9297694021, 9297694022
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0050 07/15/11 14:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
633663LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.068.067 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
633664MATRIX SPIKE SAMPLE:
MSSpike
Result
9297452002
Mercury mg/kg 0.042 M0.057 70 75-125ND
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
633666MATRIX SPIKE SAMPLE:
MSSpike
Result
9297794001
Mercury mg/kg 0.18 M0.47 24 75-1250.0082 ug/g
Parameter Units
Dup
Result QualifiersRPDResult
9297452003
633665SAMPLE DUPLICATE:
Mercury mg/kg .00034JND
Parameter Units
Dup
Result QualifiersRPDResult
9297794002
633667SAMPLE DUPLICATE:
Mercury mg/kg 0.058 60.0065 ug/g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 123 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/14156
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:9297694001, 9297694002, 9297694003, 9297694004, 9297694005, 9297694006, 9297694007, 9297694008,
9297694009, 9297694010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:630845
Associated Lab Samples:9297694001, 9297694002, 9297694003, 9297694004, 9297694005, 9297694006, 9297694007, 9297694008,
9297694009, 9297694010
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 07/14/11 15:22
1,2-Dichlorobenzene ug/kg ND 330 07/14/11 15:22
1,3-Dichlorobenzene ug/kg ND 330 07/14/11 15:22
1,4-Dichlorobenzene ug/kg ND 330 07/14/11 15:22
1-Methylnaphthalene ug/kg ND 330 07/14/11 15:22
2,4,5-Trichlorophenol ug/kg ND 330 07/14/11 15:22
2,4,6-Trichlorophenol ug/kg ND 330 07/14/11 15:22
2,4-Dichlorophenol ug/kg ND 330 07/14/11 15:22
2,4-Dimethylphenol ug/kg ND 330 07/14/11 15:22
2,4-Dinitrophenol ug/kg ND 1650 07/14/11 15:22
2,4-Dinitrotoluene ug/kg ND 330 07/14/11 15:22
2,6-Dinitrotoluene ug/kg ND 330 07/14/11 15:22
2-Chloronaphthalene ug/kg ND 330 07/14/11 15:22
2-Chlorophenol ug/kg ND 330 07/14/11 15:22
2-Methylnaphthalene ug/kg ND 330 07/14/11 15:22
2-Methylphenol(o-Cresol)ug/kg ND 330 07/14/11 15:22
2-Nitroaniline ug/kg ND 1650 07/14/11 15:22
2-Nitrophenol ug/kg ND 330 07/14/11 15:22
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 07/14/11 15:22
3,3'-Dichlorobenzidine ug/kg ND 1650 07/14/11 15:22
3-Nitroaniline ug/kg ND 1650 07/14/11 15:22
4,6-Dinitro-2-methylphenol ug/kg ND 660 07/14/11 15:22
4-Bromophenylphenyl ether ug/kg ND 330 07/14/11 15:22
4-Chloro-3-methylphenol ug/kg ND 660 07/14/11 15:22
4-Chloroaniline ug/kg ND 1650 07/14/11 15:22
4-Chlorophenylphenyl ether ug/kg ND 330 07/14/11 15:22
4-Nitroaniline ug/kg ND 660 07/14/11 15:22
4-Nitrophenol ug/kg ND 1650 07/14/11 15:22
Acenaphthene ug/kg ND 330 07/14/11 15:22
Acenaphthylene ug/kg ND 330 07/14/11 15:22
Aniline ug/kg ND 330 07/14/11 15:22
Anthracene ug/kg ND 330 07/14/11 15:22
Benzo(a)anthracene ug/kg ND 330 07/14/11 15:22
Benzo(a)pyrene ug/kg ND 330 07/14/11 15:22
Benzo(b)fluoranthene ug/kg ND 330 07/14/11 15:22
Benzo(g,h,i)perylene ug/kg ND 330 07/14/11 15:22
Benzo(k)fluoranthene ug/kg ND 330 07/14/11 15:22
Benzoic Acid ug/kg ND 1650 07/14/11 15:22
Benzyl alcohol ug/kg ND 660 07/14/11 15:22
bis(2-Chloroethoxy)methane ug/kg ND 330 07/14/11 15:22
bis(2-Chloroethyl) ether ug/kg ND 330 07/14/11 15:22
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 124 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:630845
Associated Lab Samples:9297694001, 9297694002, 9297694003, 9297694004, 9297694005, 9297694006, 9297694007, 9297694008,
9297694009, 9297694010
Matrix:Solid
Analyzed
bis(2-Chloroisopropyl) ether ug/kg ND 330 07/14/11 15:22
bis(2-Ethylhexyl)phthalate ug/kg ND 330 07/14/11 15:22
Butylbenzylphthalate ug/kg ND 330 07/14/11 15:22
Chrysene ug/kg ND 330 07/14/11 15:22
Di-n-butylphthalate ug/kg ND 330 07/14/11 15:22
Di-n-octylphthalate ug/kg ND 330 07/14/11 15:22
Dibenz(a,h)anthracene ug/kg ND 330 07/14/11 15:22
Dibenzofuran ug/kg ND 330 07/14/11 15:22
Diethylphthalate ug/kg ND 330 07/14/11 15:22
Dimethylphthalate ug/kg ND 330 07/14/11 15:22
Fluoranthene ug/kg ND 330 07/14/11 15:22
Fluorene ug/kg ND 330 07/14/11 15:22
Hexachloro-1,3-butadiene ug/kg ND 330 07/14/11 15:22
Hexachlorobenzene ug/kg ND 330 07/14/11 15:22
Hexachlorocyclopentadiene ug/kg ND 330 07/14/11 15:22
Hexachloroethane ug/kg ND 330 07/14/11 15:22
Indeno(1,2,3-cd)pyrene ug/kg ND 330 07/14/11 15:22
Isophorone ug/kg ND 330 07/14/11 15:22
N-Nitroso-di-n-propylamine ug/kg ND 330 07/14/11 15:22
N-Nitrosodimethylamine ug/kg ND 330 07/14/11 15:22
N-Nitrosodiphenylamine ug/kg ND 330 07/14/11 15:22
Naphthalene ug/kg ND 330 07/14/11 15:22
Nitrobenzene ug/kg ND 330 07/14/11 15:22
Pentachlorophenol ug/kg ND 1650 07/14/11 15:22
Phenanthrene ug/kg ND 330 07/14/11 15:22
Phenol ug/kg ND 330 07/14/11 15:22
Pyrene ug/kg ND 330 07/14/11 15:22
2,4,6-Tribromophenol (S)%81 27-110 07/14/11 15:22
2-Fluorobiphenyl (S)%87 30-110 07/14/11 15:22
2-Fluorophenol (S)%72 13-110 07/14/11 15:22
Nitrobenzene-d5 (S)%95 23-110 07/14/11 15:22
Phenol-d6 (S)%74 22-110 07/14/11 15:22
Terphenyl-d14 (S)%94 28-110 07/14/11 15:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
630846LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 14701670 88 39-101
1,2-Dichlorobenzene ug/kg 13101670 79 36-110
1,3-Dichlorobenzene ug/kg 13001670 78 35-110
1,4-Dichlorobenzene ug/kg 13001670 78 35-110
1-Methylnaphthalene ug/kg 13601670 82 45-105
2,4,5-Trichlorophenol ug/kg 13901670 83 48-109
2,4,6-Trichlorophenol ug/kg 14501670 87 45-111
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 125 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
630846LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dichlorophenol ug/kg 14601670 88 51-116
2,4-Dimethylphenol ug/kg 13401670 80 42-103
2,4-Dinitrophenol ug/kg 49708330 60 28-103
2,4-Dinitrotoluene ug/kg 14401670 86 46-114
2,6-Dinitrotoluene ug/kg 14301670 86 48-112
2-Chloronaphthalene ug/kg 13801670 83 44-105
2-Chlorophenol ug/kg 12201670 73 36-110
2-Methylnaphthalene ug/kg 13201670 79 39-112
2-Methylphenol(o-Cresol)ug/kg 11701670 70 39-101
2-Nitroaniline ug/kg 30903330 93 44-111
2-Nitrophenol ug/kg 13001670 78 41-100
3&4-Methylphenol(m&p Cresol)ug/kg 11701670 70 43-103
3,3'-Dichlorobenzidine ug/kg 26003330 78 10-150
3-Nitroaniline ug/kg 24803330 74 35-110
4,6-Dinitro-2-methylphenol ug/kg 24403330 73 38-118
4-Bromophenylphenyl ether ug/kg 13701670 82 47-115
4-Chloro-3-methylphenol ug/kg 30003330 90 43-127
4-Chloroaniline ug/kg 23903330 72 34-109
4-Chlorophenylphenyl ether ug/kg 13901670 83 44-115
4-Nitroaniline ug/kg 25103330 75 37-111
4-Nitrophenol ug/kg 78208330 94 21-152
Acenaphthene ug/kg 14801670 89 38-117
Acenaphthylene ug/kg 13601670 81 46-107
Aniline ug/kg 11301670 68 29-110
Anthracene ug/kg 15001670 90 50-110
Benzo(a)anthracene ug/kg 13901670 83 47-116
Benzo(a)pyrene ug/kg 13001670 78 47-106
Benzo(b)fluoranthene ug/kg 13101670 79 47-109
Benzo(g,h,i)perylene ug/kg 14701670 88 39-115
Benzo(k)fluoranthene ug/kg 13801670 83 45-117
Benzoic Acid ug/kg 39308330 47 16-110
Benzyl alcohol ug/kg 25403330 76 38-105
bis(2-Chloroethoxy)methane ug/kg 12601670 75 39-110
bis(2-Chloroethyl) ether ug/kg 12501670 75 19-119
bis(2-Chloroisopropyl) ether ug/kg 11201670 67 21-110
bis(2-Ethylhexyl)phthalate ug/kg 14401670 86 35-116
Butylbenzylphthalate ug/kg 14601670 88 38-110
Chrysene ug/kg 14101670 85 49-110
Di-n-butylphthalate ug/kg 14201670 85 43-109
Di-n-octylphthalate ug/kg 13701670 82 37-109
Dibenz(a,h)anthracene ug/kg 14601670 88 43-116
Dibenzofuran ug/kg 14901670 89 45-106
Diethylphthalate ug/kg 14601670 87 41-114
Dimethylphthalate ug/kg 14001670 84 43-110
Fluoranthene ug/kg 14301670 86 50-114
Fluorene ug/kg 14901670 89 46-114
Hexachloro-1,3-butadiene ug/kg 15201670 91 28-111
Hexachlorobenzene ug/kg 15101670 90 46-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 126 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
630846LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorocyclopentadiene ug/kg 8231670 49 18-119
Hexachloroethane ug/kg 13101670 79 33-110
Indeno(1,2,3-cd)pyrene ug/kg 14701670 88 42-115
Isophorone ug/kg 14601670 88 44-109
N-Nitroso-di-n-propylamine ug/kg 13001670 78 43-104
N-Nitrosodimethylamine ug/kg 12501670 75 29-110
N-Nitrosodiphenylamine ug/kg 15301670 92 48-113
Naphthalene ug/kg 13401670 80 41-110
Nitrobenzene ug/kg 14401670 86 38-110
Pentachlorophenol ug/kg 21203330 64 32-128
Phenanthrene ug/kg 14601670 88 50-110
Phenol ug/kg 12501670 75 28-106
Pyrene ug/kg 15301670 92 45-114
2,4,6-Tribromophenol (S)%98 27-110
2-Fluorobiphenyl (S)%87 30-110
2-Fluorophenol (S)%76 13-110
Nitrobenzene-d5 (S)%90 23-110
Phenol-d6 (S)%71 22-110
Terphenyl-d14 (S)%92 28-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 127 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/14161
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:9297694011, 9297694012, 9297694013, 9297694014, 9297694015, 9297694016, 9297694017, 9297694018,
9297694019, 9297694020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:631099
Associated Lab Samples:9297694011, 9297694012, 9297694013, 9297694014, 9297694015, 9297694016, 9297694017, 9297694018,
9297694019, 9297694020
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 07/11/11 18:42
1,2-Dichlorobenzene ug/kg ND 330 07/11/11 18:42
1,3-Dichlorobenzene ug/kg ND 330 07/11/11 18:42
1,4-Dichlorobenzene ug/kg ND 330 07/11/11 18:42
1-Methylnaphthalene ug/kg ND 330 07/11/11 18:42
2,4,5-Trichlorophenol ug/kg ND 330 07/11/11 18:42
2,4,6-Trichlorophenol ug/kg ND 330 07/11/11 18:42
2,4-Dichlorophenol ug/kg ND 330 07/11/11 18:42
2,4-Dimethylphenol ug/kg ND 330 07/11/11 18:42
2,4-Dinitrophenol ug/kg ND 1650 07/11/11 18:42
2,4-Dinitrotoluene ug/kg ND 330 07/11/11 18:42
2,6-Dinitrotoluene ug/kg ND 330 07/11/11 18:42
2-Chloronaphthalene ug/kg ND 330 07/11/11 18:42
2-Chlorophenol ug/kg ND 330 07/11/11 18:42
2-Methylnaphthalene ug/kg ND 330 07/11/11 18:42
2-Methylphenol(o-Cresol)ug/kg ND 330 07/11/11 18:42
2-Nitroaniline ug/kg ND 1650 07/11/11 18:42
2-Nitrophenol ug/kg ND 330 07/11/11 18:42
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 07/11/11 18:42
3,3'-Dichlorobenzidine ug/kg ND 1650 07/11/11 18:42
3-Nitroaniline ug/kg ND 1650 07/11/11 18:42
4,6-Dinitro-2-methylphenol ug/kg ND 660 07/11/11 18:42
4-Bromophenylphenyl ether ug/kg ND 330 07/11/11 18:42
4-Chloro-3-methylphenol ug/kg ND 660 07/11/11 18:42
4-Chloroaniline ug/kg ND 1650 07/11/11 18:42
4-Chlorophenylphenyl ether ug/kg ND 330 07/11/11 18:42
4-Nitroaniline ug/kg ND 660 07/11/11 18:42
4-Nitrophenol ug/kg ND 1650 07/11/11 18:42
Acenaphthene ug/kg ND 330 07/11/11 18:42
Acenaphthylene ug/kg ND 330 07/11/11 18:42
Aniline ug/kg ND 330 07/11/11 18:42
Anthracene ug/kg ND 330 07/11/11 18:42
Benzo(a)anthracene ug/kg ND 330 07/11/11 18:42
Benzo(a)pyrene ug/kg ND 330 07/11/11 18:42
Benzo(b)fluoranthene ug/kg ND 330 07/11/11 18:42
Benzo(g,h,i)perylene ug/kg ND 330 07/11/11 18:42
Benzo(k)fluoranthene ug/kg ND 330 07/11/11 18:42
Benzoic Acid ug/kg ND 1650 07/11/11 18:42
Benzyl alcohol ug/kg ND 660 07/11/11 18:42
bis(2-Chloroethoxy)methane ug/kg ND 330 07/11/11 18:42
bis(2-Chloroethyl) ether ug/kg ND 330 07/11/11 18:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 128 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:631099
Associated Lab Samples:9297694011, 9297694012, 9297694013, 9297694014, 9297694015, 9297694016, 9297694017, 9297694018,
9297694019, 9297694020
Matrix:Solid
Analyzed
bis(2-Chloroisopropyl) ether ug/kg ND 330 07/11/11 18:42
bis(2-Ethylhexyl)phthalate ug/kg ND 330 07/11/11 18:42
Butylbenzylphthalate ug/kg ND 330 07/11/11 18:42
Chrysene ug/kg ND 330 07/11/11 18:42
Di-n-butylphthalate ug/kg ND 330 07/11/11 18:42
Di-n-octylphthalate ug/kg ND 330 07/11/11 18:42
Dibenz(a,h)anthracene ug/kg ND 330 07/11/11 18:42
Dibenzofuran ug/kg ND 330 07/11/11 18:42
Diethylphthalate ug/kg ND 330 07/11/11 18:42
Dimethylphthalate ug/kg ND 330 07/11/11 18:42
Fluoranthene ug/kg ND 330 07/11/11 18:42
Fluorene ug/kg ND 330 07/11/11 18:42
Hexachloro-1,3-butadiene ug/kg ND 330 07/11/11 18:42
Hexachlorobenzene ug/kg ND 330 07/11/11 18:42
Hexachlorocyclopentadiene ug/kg ND 330 07/11/11 18:42
Hexachloroethane ug/kg ND 330 07/11/11 18:42
Indeno(1,2,3-cd)pyrene ug/kg ND 330 07/11/11 18:42
Isophorone ug/kg ND 330 07/11/11 18:42
N-Nitroso-di-n-propylamine ug/kg ND 330 07/11/11 18:42
N-Nitrosodimethylamine ug/kg ND 330 07/11/11 18:42
N-Nitrosodiphenylamine ug/kg ND 330 07/11/11 18:42
Naphthalene ug/kg ND 330 07/11/11 18:42
Nitrobenzene ug/kg ND 330 07/11/11 18:42
Pentachlorophenol ug/kg ND 1650 07/11/11 18:42
Phenanthrene ug/kg ND 330 07/11/11 18:42
Phenol ug/kg ND 330 07/11/11 18:42
Pyrene ug/kg ND 330 07/11/11 18:42
2,4,6-Tribromophenol (S)%61 27-110 07/11/11 18:42
2-Fluorobiphenyl (S)%68 30-110 07/11/11 18:42
2-Fluorophenol (S)%57 13-110 07/11/11 18:42
Nitrobenzene-d5 (S)%69 23-110 07/11/11 18:42
Phenol-d6 (S)%51 22-110 07/11/11 18:42
Terphenyl-d14 (S)%83 28-110 07/11/11 18:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
631100LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 12801670 77 39-101
1,2-Dichlorobenzene ug/kg 11001670 66 36-110
1,3-Dichlorobenzene ug/kg 11201670 67 35-110
1,4-Dichlorobenzene ug/kg 11101670 67 35-110
1-Methylnaphthalene ug/kg 12701670 76 45-105
2,4,5-Trichlorophenol ug/kg 12501670 75 48-109
2,4,6-Trichlorophenol ug/kg 13801670 83 45-111
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 129 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
631100LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dichlorophenol ug/kg 13301670 80 51-116
2,4-Dimethylphenol ug/kg 12501670 75 42-103
2,4-Dinitrophenol ug/kg 45008330 54 28-103
2,4-Dinitrotoluene ug/kg 13101670 78 46-114
2,6-Dinitrotoluene ug/kg 13301670 80 48-112
2-Chloronaphthalene ug/kg 13401670 81 44-105
2-Chlorophenol ug/kg 9871670 59 36-110
2-Methylnaphthalene ug/kg 12201670 73 39-112
2-Methylphenol(o-Cresol)ug/kg 9801670 59 39-101
2-Nitroaniline ug/kg 29203330 88 44-111
2-Nitrophenol ug/kg 11701670 70 41-100
3&4-Methylphenol(m&p Cresol)ug/kg 10201670 61 43-103
3,3'-Dichlorobenzidine ug/kg 21803330 66 10-150
3-Nitroaniline ug/kg 22203330 67 35-110
4,6-Dinitro-2-methylphenol ug/kg 23103330 69 38-118
4-Bromophenylphenyl ether ug/kg 13601670 81 47-115
4-Chloro-3-methylphenol ug/kg 26903330 81 43-127
4-Chloroaniline ug/kg 22403330 67 34-109
4-Chlorophenylphenyl ether ug/kg 13001670 78 44-115
4-Nitroaniline ug/kg 21303330 64 37-111
4-Nitrophenol ug/kg 65408330 78 21-152
Acenaphthene ug/kg 14301670 86 38-117
Acenaphthylene ug/kg 13101670 78 46-107
Aniline ug/kg 9451670 57 29-110
Anthracene ug/kg 14401670 87 50-110
Benzo(a)anthracene ug/kg 13001670 78 47-116
Benzo(a)pyrene ug/kg 12901670 78 47-106
Benzo(b)fluoranthene ug/kg 13601670 81 47-109
Benzo(g,h,i)perylene ug/kg 12501670 75 39-115
Benzo(k)fluoranthene ug/kg 15101670 90 45-117
Benzoic Acid ug/kg 40808330 49 16-110
Benzyl alcohol ug/kg 22503330 68 38-105
bis(2-Chloroethoxy)methane ug/kg 12101670 73 39-110
bis(2-Chloroethyl) ether ug/kg 10601670 64 19-119
bis(2-Chloroisopropyl) ether ug/kg 9651670 58 21-110
bis(2-Ethylhexyl)phthalate ug/kg 13701670 82 35-116
Butylbenzylphthalate ug/kg 14001670 84 38-110
Chrysene ug/kg 13601670 81 49-110
Di-n-butylphthalate ug/kg 13201670 79 43-109
Di-n-octylphthalate ug/kg 11701670 70 37-109
Dibenz(a,h)anthracene ug/kg 12901670 78 43-116
Dibenzofuran ug/kg 13901670 84 45-106
Diethylphthalate ug/kg 13401670 80 41-114
Dimethylphthalate ug/kg 13101670 79 43-110
Fluoranthene ug/kg 13101670 79 50-114
Fluorene ug/kg 13801670 83 46-114
Hexachloro-1,3-butadiene ug/kg 13201670 79 28-111
Hexachlorobenzene ug/kg 14801670 89 46-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 130 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
631100LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorocyclopentadiene ug/kg 10601670 63 18-119
Hexachloroethane ug/kg 11301670 68 33-110
Indeno(1,2,3-cd)pyrene ug/kg 12801670 77 42-115
Isophorone ug/kg 14301670 86 44-109
N-Nitroso-di-n-propylamine ug/kg 11501670 69 43-104
N-Nitrosodimethylamine ug/kg 11101670 66 29-110
N-Nitrosodiphenylamine ug/kg 15101670 91 48-113
Naphthalene ug/kg 11901670 71 41-110
Nitrobenzene ug/kg 13201670 79 38-110
Pentachlorophenol ug/kg 18103330 54 32-128
Phenanthrene ug/kg 14201670 85 50-110
Phenol ug/kg 10401670 62 28-106
Pyrene ug/kg 15401670 92 45-114
2,4,6-Tribromophenol (S)%86 27-110
2-Fluorobiphenyl (S)%81 30-110
2-Fluorophenol (S)%61 13-110
Nitrobenzene-d5 (S)%79 23-110
Phenol-d6 (S)%58 22-110
Terphenyl-d14 (S)%90 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
631101MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9297694013
631102
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1800 74 18-11983 121800ND13201490
1,2-Dichlorobenzene ug/kg 1800 62 50-11073 171800ND11101310
1,3-Dichlorobenzene ug/kg 1800 62 27-11073 171800ND11201320
1,4-Dichlorobenzene ug/kg 1800 62 28-11073 171800ND11101310
1-Methylnaphthalene ug/kg 1800 71 24-11677 81800ND12801390
2,4,5-Trichlorophenol ug/kg 1800 66 28-11072 81800ND11901290
2,4,6-Trichlorophenol ug/kg 1800 65 17-11771 71800ND11701260
2,4-Dichlorophenol ug/kg 1800 65 21-12871 101800ND11601280
2,4-Dimethylphenol ug/kg 1800 16 10-120181800ND289J321J
2,4-Dinitrophenol ug/kg 8970 47 10-10753 128970ND42104750
2,4-Dinitrotoluene ug/kg 1800 71 36-10975 61800ND12601350
2,6-Dinitrotoluene ug/kg 1800 71 32-11077 71800ND12801380
2-Chloronaphthalene ug/kg 1800 76 30-10780 51800ND13601430
2-Chlorophenol ug/kg 1800 50 14-10658 151800ND9031050
2-Methylnaphthalene ug/kg 1800 69 10-13575 91800ND12401350
2-Methylphenol(o-Cresol)ug/kg 1800 26 10-12428 71800ND471504
2-Nitroaniline ug/kg 3580 76 26-11681 63580ND27402920
2-Nitrophenol ug/kg 1800 66 28-10374 111800ND11801320
3&4-Methylphenol(m&p
Cresol)ug/kg 1800 32 10-10934 81800ND569615
3,3'-Dichlorobenzidine ug/kg 3580 22 10-150283580ND784J1000J
3-Nitroaniline ug/kg 3580 57 22-11061 73580ND20402200
4,6-Dinitro-2-methylphenol ug/kg 3580 60 13-12169 133580ND21702480
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 131 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
631101MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9297694013
631102
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
4-Bromophenylphenyl ether ug/kg 1800 70 31-10976 81800ND12601370
4-Chloro-3-methylphenol ug/kg 3580 52 13-12860 143580ND18802160
4-Chloroaniline ug/kg 3580 48 18-102523580ND1710J1850
4-Chlorophenylphenyl ether ug/kg 1800 69 29-11274 71800ND12401320
4-Nitroaniline ug/kg 3580 58 16-11162 73580ND20902230
4-Nitrophenol ug/kg 8970 71 14-13579 118970ND63407100
Acenaphthene ug/kg 1800 78 26-11482 51800ND14001470
Acenaphthylene ug/kg 1800 71 32-10876 61800ND12801360
Aniline ug/kg 1800 16 10-107181800ND295J315J
Anthracene ug/kg 1800 74 32-11182 101800ND13301470
Benzo(a)anthracene ug/kg 1800 68 25-11776 101800ND12301360
Benzo(a)pyrene ug/kg 1800 66 25-10671 81800ND11801280
Benzo(b)fluoranthene ug/kg 1800 69 24-11071 31800ND12301270
Benzo(g,h,i)perylene ug/kg 1800 73 19-11282 121800ND13001470
Benzo(k)fluoranthene ug/kg 1800 65 24-11474 121800ND12101360
Benzoic Acid ug/kg 8970 19 10-110198970ND1730J1730J
Benzyl alcohol ug/kg 3580 64 24-10669 73580ND23002470
bis(2-Chloroethoxy)methane ug/kg 1800 66 13-11971 71800ND11901280
bis(2-Chloroethyl) ether ug/kg 1800 59 10-13468 141800ND10601220
bis(2-Chloroisopropyl) ether ug/kg 1800 55 10-11363 131800ND9911130
bis(2-Ethylhexyl)phthalate ug/kg 1800 70 10-12573 41800ND12601310
Butylbenzylphthalate ug/kg 1800 72 18-11073 11800ND13001310
Chrysene ug/kg 1800 71 30-11078 101800ND12801410
Di-n-butylphthalate ug/kg 1800 68 19-11277 121800ND12201380
Di-n-octylphthalate ug/kg 1800 67 17-10577 141800ND12001380
Dibenz(a,h)anthracene ug/kg 1800 71 23-11182 141800ND12801480
Dibenzofuran ug/kg 1800 76 35-10380 61800ND13601440
Diethylphthalate ug/kg 1800 71 27-11376 71800ND12701370
Dimethylphthalate ug/kg 1800 71 26-11176 61800ND12801360
Fluoranthene ug/kg 1800 70 33-10982 151800ND12601460
Fluorene ug/kg 1800 74 32-11380 71800ND13301430
Hexachloro-1,3-butadiene ug/kg 1800 76 16-11686 121800ND13601540
Hexachlorobenzene ug/kg 1800 76 27-12082 81800ND13601480
Hexachlorocyclopentadiene ug/kg 1800 40 10-10841 21800ND716730
Hexachloroethane ug/kg 1800 61 10-11772 171800ND11001290
Indeno(1,2,3-cd)pyrene ug/kg 1800 71 10-12281 131800ND12701440
Isophorone ug/kg 1800 76 28-11481 61800ND13601460
N-Nitroso-di-n-propylamine ug/kg 1800 66 27-11371 81800ND11801270
N-Nitrosodimethylamine ug/kg 1800 60 10-10969 151800ND10701240
N-Nitrosodiphenylamine ug/kg 1800 69 10-12875 81800ND12301340
Naphthalene ug/kg 1800 68 25-11075 111800ND12101350
Nitrobenzene ug/kg 1800 70 18-11480 131800ND12601430
Pentachlorophenol ug/kg 3580 48 10-122553580ND1710J1970
Phenanthrene ug/kg 1800 74 30-11481 91800ND13201450
Phenol ug/kg 1800 46 11-10252 111800ND832931
Pyrene ug/kg 1800 78 25-11675 41800ND14001350
2,4,6-Tribromophenol (S)%64 27-11071
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 132 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
631101MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9297694013
631102
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2-Fluorobiphenyl (S)%77 30-11080
2-Fluorophenol (S)%40 13-11046
Nitrobenzene-d5 (S)%71 23-11080
Phenol-d6 (S)%43 22-11049
Terphenyl-d14 (S)%73 28-11070
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 133 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/14176
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:9297694021, 9297694022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:631967
Associated Lab Samples:9297694021, 9297694022
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 07/12/11 17:57
1,2-Dichlorobenzene ug/kg ND 330 07/12/11 17:57
1,3-Dichlorobenzene ug/kg ND 330 07/12/11 17:57
1,4-Dichlorobenzene ug/kg ND 330 07/12/11 17:57
1-Methylnaphthalene ug/kg ND 330 07/12/11 17:57
2,4,5-Trichlorophenol ug/kg ND 330 07/12/11 17:57
2,4,6-Trichlorophenol ug/kg ND 330 07/12/11 17:57
2,4-Dichlorophenol ug/kg ND 330 07/12/11 17:57
2,4-Dimethylphenol ug/kg ND 330 07/12/11 17:57
2,4-Dinitrophenol ug/kg ND 1650 07/12/11 17:57
2,4-Dinitrotoluene ug/kg ND 330 07/12/11 17:57
2,6-Dinitrotoluene ug/kg ND 330 07/12/11 17:57
2-Chloronaphthalene ug/kg ND 330 07/12/11 17:57
2-Chlorophenol ug/kg ND 330 07/12/11 17:57
2-Methylnaphthalene ug/kg ND 330 07/12/11 17:57
2-Methylphenol(o-Cresol)ug/kg ND 330 07/12/11 17:57
2-Nitroaniline ug/kg ND 1650 07/12/11 17:57
2-Nitrophenol ug/kg ND 330 07/12/11 17:57
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 07/12/11 17:57
3,3'-Dichlorobenzidine ug/kg ND 1650 07/12/11 17:57
3-Nitroaniline ug/kg ND 1650 07/12/11 17:57
4,6-Dinitro-2-methylphenol ug/kg ND 660 07/12/11 17:57
4-Bromophenylphenyl ether ug/kg ND 330 07/12/11 17:57
4-Chloro-3-methylphenol ug/kg ND 660 07/12/11 17:57
4-Chloroaniline ug/kg ND 1650 07/12/11 17:57
4-Chlorophenylphenyl ether ug/kg ND 330 07/12/11 17:57
4-Nitroaniline ug/kg ND 660 07/12/11 17:57
4-Nitrophenol ug/kg ND 1650 07/12/11 17:57
Acenaphthene ug/kg ND 330 07/12/11 17:57
Acenaphthylene ug/kg ND 330 07/12/11 17:57
Aniline ug/kg ND 330 07/12/11 17:57
Anthracene ug/kg ND 330 07/12/11 17:57
Benzo(a)anthracene ug/kg ND 330 07/12/11 17:57
Benzo(a)pyrene ug/kg ND 330 07/12/11 17:57
Benzo(b)fluoranthene ug/kg ND 330 07/12/11 17:57
Benzo(g,h,i)perylene ug/kg ND 330 07/12/11 17:57
Benzo(k)fluoranthene ug/kg ND 330 07/12/11 17:57
Benzoic Acid ug/kg ND 1650 07/12/11 17:57
Benzyl alcohol ug/kg ND 660 07/12/11 17:57
bis(2-Chloroethoxy)methane ug/kg ND 330 07/12/11 17:57
bis(2-Chloroethyl) ether ug/kg ND 330 07/12/11 17:57
bis(2-Chloroisopropyl) ether ug/kg ND 330 07/12/11 17:57
bis(2-Ethylhexyl)phthalate ug/kg ND 330 07/12/11 17:57
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 134 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:631967
Associated Lab Samples:9297694021, 9297694022
Matrix:Solid
Analyzed
Butylbenzylphthalate ug/kg ND 330 07/12/11 17:57
Chrysene ug/kg ND 330 07/12/11 17:57
Di-n-butylphthalate ug/kg ND 330 07/12/11 17:57
Di-n-octylphthalate ug/kg ND 330 07/12/11 17:57
Dibenz(a,h)anthracene ug/kg ND 330 07/12/11 17:57
Dibenzofuran ug/kg ND 330 07/12/11 17:57
Diethylphthalate ug/kg ND 330 07/12/11 17:57
Dimethylphthalate ug/kg ND 330 07/12/11 17:57
Fluoranthene ug/kg ND 330 07/12/11 17:57
Fluorene ug/kg ND 330 07/12/11 17:57
Hexachloro-1,3-butadiene ug/kg ND 330 07/12/11 17:57
Hexachlorobenzene ug/kg ND 330 07/12/11 17:57
Hexachlorocyclopentadiene ug/kg ND 330 07/12/11 17:57
Hexachloroethane ug/kg ND 330 07/12/11 17:57
Indeno(1,2,3-cd)pyrene ug/kg ND 330 07/12/11 17:57
Isophorone ug/kg ND 330 07/12/11 17:57
N-Nitroso-di-n-propylamine ug/kg ND 330 07/12/11 17:57
N-Nitrosodimethylamine ug/kg ND 330 07/12/11 17:57
N-Nitrosodiphenylamine ug/kg ND 330 07/12/11 17:57
Naphthalene ug/kg ND 330 07/12/11 17:57
Nitrobenzene ug/kg ND 330 07/12/11 17:57
Pentachlorophenol ug/kg ND 1650 07/12/11 17:57
Phenanthrene ug/kg ND 330 07/12/11 17:57
Phenol ug/kg ND 330 07/12/11 17:57
Pyrene ug/kg ND 330 07/12/11 17:57
2,4,6-Tribromophenol (S)%67 27-110 07/12/11 17:57
2-Fluorobiphenyl (S)%67 30-110 07/12/11 17:57
2-Fluorophenol (S)%55 13-110 07/12/11 17:57
Nitrobenzene-d5 (S)%70 23-110 07/12/11 17:57
Phenol-d6 (S)%55 22-110 07/12/11 17:57
Terphenyl-d14 (S)%83 28-110 07/12/11 17:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
631968LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 15401670 93 39-101
1,2-Dichlorobenzene ug/kg 13301670 80 36-110
1,3-Dichlorobenzene ug/kg 13401670 81 35-110
1,4-Dichlorobenzene ug/kg 13401670 80 35-110
1-Methylnaphthalene ug/kg 13701670 82 45-105
2,4,5-Trichlorophenol ug/kg 13001670 78 48-109
2,4,6-Trichlorophenol ug/kg 14301670 86 45-111
2,4-Dichlorophenol ug/kg 14701670 88 51-116
2,4-Dimethylphenol ug/kg 13501670 81 42-103
2,4-Dinitrophenol ug/kg 35508330 43 28-103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 135 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
631968LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dinitrotoluene ug/kg 13201670 79 46-114
2,6-Dinitrotoluene ug/kg 13601670 81 48-112
2-Chloronaphthalene ug/kg 14201670 85 44-105
2-Chlorophenol ug/kg 12401670 74 36-110
2-Methylnaphthalene ug/kg 13301670 80 39-112
2-Methylphenol(o-Cresol)ug/kg 11701670 70 39-101
2-Nitroaniline ug/kg 28603330 86 44-111
2-Nitrophenol ug/kg 13601670 82 41-100
3&4-Methylphenol(m&p Cresol)ug/kg 11501670 69 43-103
3,3'-Dichlorobenzidine ug/kg 24603330 74 10-150
3-Nitroaniline ug/kg 21503330 65 35-110
4,6-Dinitro-2-methylphenol ug/kg 19403330 58 38-118
4-Bromophenylphenyl ether ug/kg 13501670 81 47-115
4-Chloro-3-methylphenol ug/kg 27403330 82 43-127
4-Chloroaniline ug/kg 22603330 68 34-109
4-Chlorophenylphenyl ether ug/kg 13201670 79 44-115
4-Nitroaniline ug/kg 21403330 64 37-111
4-Nitrophenol ug/kg 64808330 78 21-152
Acenaphthene ug/kg 14501670 87 38-117
Acenaphthylene ug/kg 13301670 80 46-107
Aniline ug/kg 11001670 66 29-110
Anthracene ug/kg 14301670 86 50-110
Benzo(a)anthracene ug/kg 13301670 80 47-116
Benzo(a)pyrene ug/kg 12301670 74 47-106
Benzo(b)fluoranthene ug/kg 12401670 75 47-109
Benzo(g,h,i)perylene ug/kg 13801670 83 39-115
Benzo(k)fluoranthene ug/kg 13401670 81 45-117
Benzoic Acid ug/kg 40508330 49 16-110
Benzyl alcohol ug/kg 25103330 75 38-105
bis(2-Chloroethoxy)methane ug/kg 13001670 78 39-110
bis(2-Chloroethyl) ether ug/kg 12601670 76 19-119
bis(2-Chloroisopropyl) ether ug/kg 11301670 68 21-110
bis(2-Ethylhexyl)phthalate ug/kg 14001670 84 35-116
Butylbenzylphthalate ug/kg 14001670 84 38-110
Chrysene ug/kg 13601670 82 49-110
Di-n-butylphthalate ug/kg 13301670 80 43-109
Di-n-octylphthalate ug/kg 13201670 79 37-109
Dibenz(a,h)anthracene ug/kg 13601670 82 43-116
Dibenzofuran ug/kg 14001670 84 45-106
Diethylphthalate ug/kg 13301670 80 41-114
Dimethylphthalate ug/kg 13401670 80 43-110
Fluoranthene ug/kg 13201670 79 50-114
Fluorene ug/kg 14001670 84 46-114
Hexachloro-1,3-butadiene ug/kg 15901670 95 28-111
Hexachlorobenzene ug/kg 14701670 88 46-120
Hexachlorocyclopentadiene ug/kg 6151670 37 18-119
Hexachloroethane ug/kg 12901670 77 33-110
Indeno(1,2,3-cd)pyrene ug/kg 13801670 83 42-115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 136 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
631968LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/kg 14501670 87 44-109
N-Nitroso-di-n-propylamine ug/kg 12401670 74 43-104
N-Nitrosodimethylamine ug/kg 12701670 76 29-110
N-Nitrosodiphenylamine ug/kg 15001670 90 48-113
Naphthalene ug/kg 13801670 83 41-110
Nitrobenzene ug/kg 15001670 90 38-110
Pentachlorophenol ug/kg 17903330 54 32-128
Phenanthrene ug/kg 14001670 84 50-110
Phenol ug/kg 12201670 73 28-106
Pyrene ug/kg 14901670 90 45-114
2,4,6-Tribromophenol (S)%91 27-110
2-Fluorobiphenyl (S)%89 30-110
2-Fluorophenol (S)%76 13-110
Nitrobenzene-d5 (S)%93 23-110
Phenol-d6 (S)%70 22-110
Terphenyl-d14 (S)%90 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
631969MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9297694021
631970
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1990 79 18-11975 51990ND15801490
1,2-Dichlorobenzene ug/kg 1990 72 50-11067 71990ND14301340
1,3-Dichlorobenzene ug/kg 1990 71 27-11067 51990ND14101340
1,4-Dichlorobenzene ug/kg 1990 71 28-11067 61990ND14101330
1-Methylnaphthalene ug/kg 1990 75 24-11672 41990ND14901430
2,4,5-Trichlorophenol ug/kg 1990 76 28-11070 71990ND15101400
2,4,6-Trichlorophenol ug/kg 1990 83 17-11776 81990ND16501510
2,4-Dichlorophenol ug/kg 1990 82 21-12876 81990ND16401520
2,4-Dimethylphenol ug/kg 1990 78 10-12072 81990ND15501430
2,4-Dinitrophenol ug/kg 9940 61 10-10753 149940ND60505250
2,4-Dinitrotoluene ug/kg 1990 79 36-10976 41990ND15801510
2,6-Dinitrotoluene ug/kg 1990 79 32-11076 41990ND15701500
2-Chloronaphthalene ug/kg 1990 77 30-10770 81990ND15201400
2-Chlorophenol ug/kg 1990 70 14-10664 101990ND14001260
2-Methylnaphthalene ug/kg 1990 72 10-13569 51990ND14401380
2-Methylphenol(o-Cresol)ug/kg 1990 70 10-12463 121990ND14001240
2-Nitroaniline ug/kg 3970 88 26-11683 63970ND34903300
2-Nitrophenol ug/kg 1990 75 28-10370 81990ND14901380
3&4-Methylphenol(m&p
Cresol)ug/kg 1990 71 10-10963 131990ND14201250
3,3'-Dichlorobenzidine ug/kg 3970 67 10-15068 03970ND26802690
3-Nitroaniline ug/kg 3970 69 22-11068 23970ND27602690
4,6-Dinitro-2-methylphenol ug/kg 3970 76 13-12166 143970ND30102620
4-Bromophenylphenyl ether ug/kg 1990 69 31-10968 21990ND13701340
4-Chloro-3-methylphenol ug/kg 3970 83 13-12880 43970ND33203190
4-Chloroaniline ug/kg 3970 69 18-10266 53970ND27402610
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 137 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
631969MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9297694021
631970
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
4-Chlorophenylphenyl ether ug/kg 1990 70 29-11267 41990ND13901340
4-Nitroaniline ug/kg 3970 70 16-11167 33970ND27702680
4-Nitrophenol ug/kg 9940 88 14-13581 89940ND87808080
Acenaphthene ug/kg 1990 80 26-11476 51990ND15901510
Acenaphthylene ug/kg 1990 74 32-10870 61990ND14701380
Aniline ug/kg 1990 63 10-10756 111990ND12501110
Anthracene ug/kg 1990 77 32-11176 21990ND15401510
Benzo(a)anthracene ug/kg 1990 70 25-11770 11990ND13901380
Benzo(a)pyrene ug/kg 1990 68 25-10664 61990ND13501280
Benzo(b)fluoranthene ug/kg 1990 70 24-11065 71990ND13801290
Benzo(g,h,i)perylene ug/kg 1990 70 19-11270 11990ND14001380
Benzo(k)fluoranthene ug/kg 1990 76 24-11473 41990ND15101450
Benzoic Acid ug/kg 9940 17 10-110129940ND1740J1200J
Benzyl alcohol ug/kg 3970 76 24-10667 123970ND30302680
bis(2-Chloroethoxy)methane ug/kg 1990 73 13-11969 61990ND14501380
bis(2-Chloroethyl) ether ug/kg 1990 73 10-13468 81990ND14601340
bis(2-Chloroisopropyl) ether ug/kg 1990 67 10-11362 71990ND13201230
bis(2-Ethylhexyl)phthalate ug/kg 1990 66 10-12568 31990ND13201350
Butylbenzylphthalate ug/kg 1990 69 18-11072 51990ND13601440
Chrysene ug/kg 1990 72 30-11073 11990ND14301450
Di-n-butylphthalate ug/kg 1990 69 19-11269 01990ND13701370
Di-n-octylphthalate ug/kg 1990 59 17-10559 11990ND11601170
Dibenz(a,h)anthracene ug/kg 1990 74 23-11171 31990ND14701420
Dibenzofuran ug/kg 1990 79 35-10375 51990ND15701500
Diethylphthalate ug/kg 1990 78 27-11375 41990ND15501490
Dimethylphthalate ug/kg 1990 78 26-11174 51990ND15501480
Fluoranthene ug/kg 1990 78 33-10972 91990ND15601430
Fluorene ug/kg 1990 77 32-11375 41990ND15401480
Hexachloro-1,3-butadiene ug/kg 1990 75 16-11673 31990ND14901440
Hexachlorobenzene ug/kg 1990 77 27-12074 41990ND15301460
Hexachlorocyclopentadiene ug/kg 1990 54 10-10845 171990ND1070902
Hexachloroethane ug/kg 1990 70 10-11766 61990ND14001320
Indeno(1,2,3-cd)pyrene ug/kg 1990 70 10-12270 11990ND14001390
Isophorone ug/kg 1990 84 28-11481 41990ND16801610
N-Nitroso-di-n-propylamine ug/kg 1990 81 27-11371 121990ND16001420
N-Nitrosodimethylamine ug/kg 1990 70 10-10966 61990ND13901300
N-Nitrosodiphenylamine ug/kg 1990 83 10-12880 41990ND16601590
Naphthalene ug/kg 1990 74 25-11070 61990ND14801390
Nitrobenzene ug/kg 1990 83 18-11477 71990ND16401540
Pentachlorophenol ug/kg 3970 61 10-12253 133970ND24102110
Phenanthrene ug/kg 1990 80 30-11475 71990ND15901490
Phenol ug/kg 1990 74 11-10264 141990ND14601280
Pyrene ug/kg 1990 80 25-11680 11990ND15801600
2,4,6-Tribromophenol (S)%90 27-11080
2-Fluorobiphenyl (S)%77 30-11069
2-Fluorophenol (S)%71 13-11063
Nitrobenzene-d5 (S)%85 23-11078
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 138 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
631969MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9297694021
631970
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenol-d6 (S)%70 22-11060
Terphenyl-d14 (S)%79 28-11078
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 139 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/15970
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:9297694001, 9297694002, 9297694003, 9297694004, 9297694005, 9297694006, 9297694007, 9297694008,
9297694009, 9297694010, 9297694011, 9297694012, 9297694013, 9297694014, 9297694015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:631958
Associated Lab Samples:9297694001, 9297694002, 9297694003, 9297694004, 9297694005, 9297694006, 9297694007, 9297694008,
9297694009, 9297694010, 9297694011, 9297694012, 9297694013, 9297694014, 9297694015
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/12/11 13:37
1,1,1-Trichloroethane ug/kg ND 5.0 07/12/11 13:37
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/12/11 13:37
1,1,2-Trichloroethane ug/kg ND 5.0 07/12/11 13:37
1,1-Dichloroethane ug/kg ND 5.0 07/12/11 13:37
1,1-Dichloroethene ug/kg ND 5.0 07/12/11 13:37
1,1-Dichloropropene ug/kg ND 5.0 07/12/11 13:37
1,2,3-Trichlorobenzene ug/kg ND 5.0 07/12/11 13:37
1,2,3-Trichloropropane ug/kg ND 5.0 07/12/11 13:37
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/12/11 13:37
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/12/11 13:37
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 07/12/11 13:37
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/12/11 13:37
1,2-Dichlorobenzene ug/kg ND 5.0 07/12/11 13:37
1,2-Dichloroethane ug/kg ND 5.0 07/12/11 13:37
1,2-Dichloropropane ug/kg ND 5.0 07/12/11 13:37
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/12/11 13:37
1,3-Dichlorobenzene ug/kg ND 5.0 07/12/11 13:37
1,3-Dichloropropane ug/kg ND 5.0 07/12/11 13:37
1,4-Dichlorobenzene ug/kg ND 5.0 07/12/11 13:37
2,2-Dichloropropane ug/kg ND 5.0 07/12/11 13:37
2-Butanone (MEK)ug/kg ND 100 07/12/11 13:37
2-Chlorotoluene ug/kg ND 5.0 07/12/11 13:37
2-Hexanone ug/kg ND 50.0 07/12/11 13:37
4-Chlorotoluene ug/kg ND 5.0 07/12/11 13:37
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/12/11 13:37
Acetone ug/kg ND 100 07/12/11 13:37
Benzene ug/kg ND 5.0 07/12/11 13:37
Bromobenzene ug/kg ND 5.0 07/12/11 13:37
Bromochloromethane ug/kg ND 5.0 07/12/11 13:37
Bromodichloromethane ug/kg ND 5.0 07/12/11 13:37
Bromoform ug/kg ND 5.0 07/12/11 13:37
Bromomethane ug/kg ND 10.0 07/12/11 13:37
Carbon tetrachloride ug/kg ND 5.0 07/12/11 13:37
Chlorobenzene ug/kg ND 5.0 07/12/11 13:37
Chloroethane ug/kg ND 10.0 07/12/11 13:37
Chloroform ug/kg ND 5.0 07/12/11 13:37
Chloromethane ug/kg ND 10.0 07/12/11 13:37
cis-1,2-Dichloroethene ug/kg ND 5.0 07/12/11 13:37
cis-1,3-Dichloropropene ug/kg ND 5.0 07/12/11 13:37
Dibromochloromethane ug/kg ND 5.0 07/12/11 13:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 140 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:631958
Associated Lab Samples:9297694001, 9297694002, 9297694003, 9297694004, 9297694005, 9297694006, 9297694007, 9297694008,
9297694009, 9297694010, 9297694011, 9297694012, 9297694013, 9297694014, 9297694015
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 5.0 07/12/11 13:37
Dichlorodifluoromethane ug/kg ND 10.0 07/12/11 13:37
Diisopropyl ether ug/kg ND 5.0 07/12/11 13:37
Ethylbenzene ug/kg ND 5.0 07/12/11 13:37
Hexachloro-1,3-butadiene ug/kg ND 5.0 07/12/11 13:37
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/12/11 13:37
m&p-Xylene ug/kg ND 10.0 07/12/11 13:37
Methyl-tert-butyl ether ug/kg ND 5.0 07/12/11 13:37
Methylene Chloride ug/kg ND 20.0 07/12/11 13:37
n-Butylbenzene ug/kg ND 5.0 07/12/11 13:37
n-Propylbenzene ug/kg ND 5.0 07/12/11 13:37
Naphthalene ug/kg ND 5.0 07/12/11 13:37
o-Xylene ug/kg ND 5.0 07/12/11 13:37
p-Isopropyltoluene ug/kg ND 5.0 07/12/11 13:37
sec-Butylbenzene ug/kg ND 5.0 07/12/11 13:37
Styrene ug/kg ND 5.0 07/12/11 13:37
tert-Butylbenzene ug/kg ND 5.0 07/12/11 13:37
Tetrachloroethene ug/kg ND 5.0 07/12/11 13:37
Toluene ug/kg ND 5.0 07/12/11 13:37
trans-1,2-Dichloroethene ug/kg ND 5.0 07/12/11 13:37
trans-1,3-Dichloropropene ug/kg ND 5.0 07/12/11 13:37
Trichloroethene ug/kg ND 5.0 07/12/11 13:37
Trichlorofluoromethane ug/kg ND 5.0 07/12/11 13:37
Vinyl acetate ug/kg ND 50.0 07/12/11 13:37
Vinyl chloride ug/kg ND 10.0 07/12/11 13:37
Xylene (Total)ug/kg ND 10.0 07/12/11 13:37
1,2-Dichloroethane-d4 (S)%95 70-132 07/12/11 13:37
4-Bromofluorobenzene (S)%97 70-130 07/12/11 13:37
Dibromofluoromethane (S)%97 70-130 07/12/11 13:37
Toluene-d8 (S)%104 70-130 07/12/11 13:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
631959LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 51.850 104 70-131
1,1,1-Trichloroethane ug/kg 50.550 101 70-141
1,1,2,2-Tetrachloroethane ug/kg 50.550 101 70-130
1,1,2-Trichloroethane ug/kg 50.050 100 70-132
1,1-Dichloroethane ug/kg 49.150 98 70-143
1,1-Dichloroethene ug/kg 47.950 96 70-137
1,1-Dichloropropene ug/kg 46.350 93 70-135
1,2,3-Trichlorobenzene ug/kg 49.550 99 69-153
1,2,3-Trichloropropane ug/kg 49.450 99 70-130
1,2,4-Trichlorobenzene ug/kg 45.950 92 55-171
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 141 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
631959LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 48.350 97 70-149
1,2-Dibromo-3-chloropropane ug/kg 49.650 99 68-141
1,2-Dibromoethane (EDB)ug/kg 48.650 97 70-130
1,2-Dichlorobenzene ug/kg 51.250 102 70-140
1,2-Dichloroethane ug/kg 49.250 98 70-137
1,2-Dichloropropane ug/kg 50.550 101 70-133
1,3,5-Trimethylbenzene ug/kg 48.350 97 70-143
1,3-Dichlorobenzene ug/kg 48.250 96 70-144
1,3-Dichloropropane ug/kg 50.150 100 70-132
1,4-Dichlorobenzene ug/kg 46.950 94 70-142
2,2-Dichloropropane ug/kg 47.650 95 68-152
2-Butanone (MEK)ug/kg 98J100 98 70-149
2-Chlorotoluene ug/kg 49.750 99 70-141
2-Hexanone ug/kg 99.2100 99 70-149
4-Chlorotoluene ug/kg 50.950 102 70-149
4-Methyl-2-pentanone (MIBK)ug/kg 96.7100 97 70-153
Acetone ug/kg 108100 108 70-157
Benzene ug/kg 46.850 94 70-130
Bromobenzene ug/kg 48.850 98 70-141
Bromochloromethane ug/kg 48.250 96 70-149
Bromodichloromethane ug/kg 52.450 105 70-130
Bromoform ug/kg 48.050 96 70-131
Bromomethane ug/kg 50.950 102 64-136
Carbon tetrachloride ug/kg 50.950 102 70-154
Chlorobenzene ug/kg 50.550 101 70-135
Chloroethane ug/kg 56.150 112 68-151
Chloroform ug/kg 52.050 104 70-130
Chloromethane ug/kg 43.850 88 70-132
cis-1,2-Dichloroethene ug/kg 48.550 97 70-140
cis-1,3-Dichloropropene ug/kg 51.750 103 70-137
Dibromochloromethane ug/kg 50.650 101 70-130
Dibromomethane ug/kg 49.250 98 70-136
Dichlorodifluoromethane ug/kg 44.650 89 36-148
Diisopropyl ether ug/kg 50.350 101 70-139
Ethylbenzene ug/kg 47.750 95 70-137
Hexachloro-1,3-butadiene ug/kg 48.350 97 70-145
Isopropylbenzene (Cumene)ug/kg 49.850 100 70-141
m&p-Xylene ug/kg 99.0100 99 70-140
Methyl-tert-butyl ether ug/kg 47.550 95 45-150
Methylene Chloride ug/kg 46.950 94 70-133
n-Butylbenzene ug/kg 48.150 96 65-155
n-Propylbenzene ug/kg 49.250 98 70-148
Naphthalene ug/kg 52.450 105 70-148
o-Xylene ug/kg 49.750 99 70-141
p-Isopropyltoluene ug/kg 48.950 98 70-148
sec-Butylbenzene ug/kg 49.050 98 70-145
Styrene ug/kg 52.450 105 70-138
tert-Butylbenzene ug/kg 50.450 101 70-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 142 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
631959LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 47.850 96 70-140
Toluene ug/kg 50.150 100 70-130
trans-1,2-Dichloroethene ug/kg 47.050 94 70-136
trans-1,3-Dichloropropene ug/kg 51.550 103 70-138
Trichloroethene ug/kg 50.850 102 70-132
Trichlorofluoromethane ug/kg 45.350 91 69-134
Vinyl acetate ug/kg 75.4100 75 24-161
Vinyl chloride ug/kg 47.150 94 55-140
Xylene (Total)ug/kg 149150 99 70-141
1,2-Dichloroethane-d4 (S)%86 70-132
4-Bromofluorobenzene (S)%100 70-130
Dibromofluoromethane (S)%96 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
632751MATRIX SPIKE SAMPLE:
MSSpike
Result
9297694002
1,1-Dichloroethene ug/kg 49.955.3 90 49-180ND
Benzene ug/kg 51.655.3 93 50-166ND
Chlorobenzene ug/kg 41.755.3 75 43-169ND
Toluene ug/kg 48.755.3 88 52-163ND
Trichloroethene ug/kg 50.655.3 92 49-167ND
1,2-Dichloroethane-d4 (S)%83 70-132
4-Bromofluorobenzene (S)%83 70-130
Dibromofluoromethane (S)%90 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result QualifiersRPDResult
9297661003
632750SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 143 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
Dup
Result QualifiersRPDResult
9297661003
632750SAMPLE DUPLICATE:
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg 141ND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg 1.3JND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 144 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
Dup
Result QualifiersRPDResult
9297661003
632750SAMPLE DUPLICATE:
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%90 187
4-Bromofluorobenzene (S)%96 496
Dibromofluoromethane (S)%93 997
Toluene-d8 (S)%101 7103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 145 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/15983
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:9297694017, 9297694018, 9297694019, 9297694020, 9297694021, 9297694022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:632338
Associated Lab Samples:9297694017, 9297694018, 9297694019, 9297694020, 9297694021, 9297694022
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/13/11 00:20
1,1,1-Trichloroethane ug/kg ND 5.0 07/13/11 00:20
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/13/11 00:20
1,1,2-Trichloroethane ug/kg ND 5.0 07/13/11 00:20
1,1-Dichloroethane ug/kg ND 5.0 07/13/11 00:20
1,1-Dichloroethene ug/kg ND 5.0 07/13/11 00:20
1,1-Dichloropropene ug/kg ND 5.0 07/13/11 00:20
1,2,3-Trichlorobenzene ug/kg ND 5.0 07/13/11 00:20
1,2,3-Trichloropropane ug/kg ND 5.0 07/13/11 00:20
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/13/11 00:20
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/13/11 00:20
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 07/13/11 00:20
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/13/11 00:20
1,2-Dichlorobenzene ug/kg ND 5.0 07/13/11 00:20
1,2-Dichloroethane ug/kg ND 5.0 07/13/11 00:20
1,2-Dichloropropane ug/kg ND 5.0 07/13/11 00:20
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/13/11 00:20
1,3-Dichlorobenzene ug/kg ND 5.0 07/13/11 00:20
1,3-Dichloropropane ug/kg ND 5.0 07/13/11 00:20
1,4-Dichlorobenzene ug/kg ND 5.0 07/13/11 00:20
2,2-Dichloropropane ug/kg ND 5.0 07/13/11 00:20
2-Butanone (MEK)ug/kg ND 100 07/13/11 00:20
2-Chlorotoluene ug/kg ND 5.0 07/13/11 00:20
2-Hexanone ug/kg ND 50.0 07/13/11 00:20
4-Chlorotoluene ug/kg ND 5.0 07/13/11 00:20
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/13/11 00:20
Acetone ug/kg ND 100 07/13/11 00:20
Benzene ug/kg ND 5.0 07/13/11 00:20
Bromobenzene ug/kg ND 5.0 07/13/11 00:20
Bromochloromethane ug/kg ND 5.0 07/13/11 00:20
Bromodichloromethane ug/kg ND 5.0 07/13/11 00:20
Bromoform ug/kg ND 5.0 07/13/11 00:20
Bromomethane ug/kg ND 10.0 07/13/11 00:20
Carbon tetrachloride ug/kg ND 5.0 07/13/11 00:20
Chlorobenzene ug/kg ND 5.0 07/13/11 00:20
Chloroethane ug/kg ND 10.0 07/13/11 00:20
Chloroform ug/kg ND 5.0 07/13/11 00:20
Chloromethane ug/kg ND 10.0 07/13/11 00:20
cis-1,2-Dichloroethene ug/kg ND 5.0 07/13/11 00:20
cis-1,3-Dichloropropene ug/kg ND 5.0 07/13/11 00:20
Dibromochloromethane ug/kg ND 5.0 07/13/11 00:20
Dibromomethane ug/kg ND 5.0 07/13/11 00:20
Dichlorodifluoromethane ug/kg ND 10.0 07/13/11 00:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 146 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:632338
Associated Lab Samples:9297694017, 9297694018, 9297694019, 9297694020, 9297694021, 9297694022
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.0 07/13/11 00:20
Ethylbenzene ug/kg ND 5.0 07/13/11 00:20
Hexachloro-1,3-butadiene ug/kg ND 5.0 07/13/11 00:20
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/13/11 00:20
m&p-Xylene ug/kg ND 10.0 07/13/11 00:20
Methyl-tert-butyl ether ug/kg ND 5.0 07/13/11 00:20
Methylene Chloride ug/kg ND 20.0 07/13/11 00:20
n-Butylbenzene ug/kg ND 5.0 07/13/11 00:20
n-Propylbenzene ug/kg ND 5.0 07/13/11 00:20
Naphthalene ug/kg ND 5.0 07/13/11 00:20
o-Xylene ug/kg ND 5.0 07/13/11 00:20
p-Isopropyltoluene ug/kg ND 5.0 07/13/11 00:20
sec-Butylbenzene ug/kg ND 5.0 07/13/11 00:20
Styrene ug/kg ND 5.0 07/13/11 00:20
tert-Butylbenzene ug/kg ND 5.0 07/13/11 00:20
Tetrachloroethene ug/kg ND 5.0 07/13/11 00:20
Toluene ug/kg ND 5.0 07/13/11 00:20
trans-1,2-Dichloroethene ug/kg ND 5.0 07/13/11 00:20
trans-1,3-Dichloropropene ug/kg ND 5.0 07/13/11 00:20
Trichloroethene ug/kg ND 5.0 07/13/11 00:20
Trichlorofluoromethane ug/kg ND 5.0 07/13/11 00:20
Vinyl acetate ug/kg ND 50.0 07/13/11 00:20
Vinyl chloride ug/kg ND 10.0 07/13/11 00:20
Xylene (Total)ug/kg ND 10.0 07/13/11 00:20
1,2-Dichloroethane-d4 (S)%94 70-132 07/13/11 00:20
4-Bromofluorobenzene (S)%99 70-130 07/13/11 00:20
Dibromofluoromethane (S)%99 70-130 07/13/11 00:20
Toluene-d8 (S)%101 70-130 07/13/11 00:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
632339LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 48.450 97 70-131
1,1,1-Trichloroethane ug/kg 44.550 89 70-141
1,1,2,2-Tetrachloroethane ug/kg 46.550 93 70-130
1,1,2-Trichloroethane ug/kg 47.450 95 70-132
1,1-Dichloroethane ug/kg 44.050 88 70-143
1,1-Dichloroethene ug/kg 41.550 83 70-137
1,1-Dichloropropene ug/kg 40.350 81 70-135
1,2,3-Trichlorobenzene ug/kg 40.650 81 69-153
1,2,3-Trichloropropane ug/kg 44.050 88 70-130
1,2,4-Trichlorobenzene ug/kg 38.650 77 55-171
1,2,4-Trimethylbenzene ug/kg 43.550 87 70-149
1,2-Dibromo-3-chloropropane ug/kg 44.650 89 68-141
1,2-Dibromoethane (EDB)ug/kg 43.750 87 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 147 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
632339LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 44.150 88 70-140
1,2-Dichloroethane ug/kg 42.950 86 70-137
1,2-Dichloropropane ug/kg 47.250 94 70-133
1,3,5-Trimethylbenzene ug/kg 43.650 87 70-143
1,3-Dichlorobenzene ug/kg 43.250 86 70-144
1,3-Dichloropropane ug/kg 46.550 93 70-132
1,4-Dichlorobenzene ug/kg 42.450 85 70-142
2,2-Dichloropropane ug/kg 37.950 76 68-152
2-Butanone (MEK)ug/kg 87J100 87 70-149
2-Chlorotoluene ug/kg 43.350 87 70-141
2-Hexanone ug/kg 85.1100 85 70-149
4-Chlorotoluene ug/kg 44.350 89 70-149
4-Methyl-2-pentanone (MIBK)ug/kg 87.6100 88 70-153
Acetone ug/kg 87.8J100 88 70-157
Benzene ug/kg 42.850 86 70-130
Bromobenzene ug/kg 42.850 86 70-141
Bromochloromethane ug/kg 42.550 85 70-149
Bromodichloromethane ug/kg 46.350 93 70-130
Bromoform ug/kg 42.950 86 70-131
Bromomethane ug/kg 42.650 85 64-136
Carbon tetrachloride ug/kg 44.850 90 70-154
Chlorobenzene ug/kg 46.550 93 70-135
Chloroethane ug/kg 48.650 97 68-151
Chloroform ug/kg 45.950 92 70-130
Chloromethane ug/kg 38.450 77 70-132
cis-1,2-Dichloroethene ug/kg 42.550 85 70-140
cis-1,3-Dichloropropene ug/kg 44.450 89 70-137
Dibromochloromethane ug/kg 45.950 92 70-130
Dibromomethane ug/kg 46.350 93 70-136
Dichlorodifluoromethane ug/kg 35.650 71 36-148
Diisopropyl ether ug/kg 43.550 87 70-139
Ethylbenzene ug/kg 44.050 88 70-137
Hexachloro-1,3-butadiene ug/kg 43.750 87 70-145
Isopropylbenzene (Cumene)ug/kg 45.350 91 70-141
m&p-Xylene ug/kg 89.1100 89 70-140
Methyl-tert-butyl ether ug/kg 42.350 85 45-150
Methylene Chloride ug/kg 37.750 75 70-133
n-Butylbenzene ug/kg 43.450 87 65-155
n-Propylbenzene ug/kg 44.250 88 70-148
Naphthalene ug/kg 44.050 88 70-148
o-Xylene ug/kg 44.550 89 70-141
p-Isopropyltoluene ug/kg 44.250 88 70-148
sec-Butylbenzene ug/kg 44.950 90 70-145
Styrene ug/kg 47.650 95 70-138
tert-Butylbenzene ug/kg 45.750 91 70-143
Tetrachloroethene ug/kg 45.050 90 70-140
Toluene ug/kg 45.450 91 70-130
trans-1,2-Dichloroethene ug/kg 41.250 82 70-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 148 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
632339LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 43.650 87 70-138
Trichloroethene ug/kg 45.250 90 70-132
Trichlorofluoromethane ug/kg 39.950 80 69-134
Vinyl acetate ug/kg 24.5J100 25 24-161
Vinyl chloride ug/kg 41.650 83 55-140
Xylene (Total)ug/kg 134150 89 70-141
1,2-Dichloroethane-d4 (S)%98 70-132
4-Bromofluorobenzene (S)%100 70-130
Dibromofluoromethane (S)%95 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
632822MATRIX SPIKE SAMPLE:
MSSpike
Result
9297783001
1,1-Dichloroethene ug/kg 60.761.2 99 49-180ND
Benzene ug/kg 64.861.2 106 50-166ND
Chlorobenzene ug/kg 64.961.2 106 43-169ND
Toluene ug/kg 68.461.2 112 52-163ND
Trichloroethene ug/kg 67.361.2 110 49-167ND
1,2-Dichloroethane-d4 (S)%87 70-132
4-Bromofluorobenzene (S)%95 70-130
Dibromofluoromethane (S)%94 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result QualifiersRPDResult
9297694017
632821SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 149 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
Dup
Result QualifiersRPDResult
9297694017
632821SAMPLE DUPLICATE:
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg 19.1JND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 150 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
Dup
Result QualifiersRPDResult
9297694017
632821SAMPLE DUPLICATE:
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%84 1279
4-Bromofluorobenzene (S)%92 593
Dibromofluoromethane (S)%95 398
Toluene-d8 (S)%104 1199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 151 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/15994
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:9297694016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:632992
Associated Lab Samples:9297694016
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/13/11 13:32
1,1,1-Trichloroethane ug/kg ND 5.0 07/13/11 13:32
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/13/11 13:32
1,1,2-Trichloroethane ug/kg ND 5.0 07/13/11 13:32
1,1-Dichloroethane ug/kg ND 5.0 07/13/11 13:32
1,1-Dichloroethene ug/kg ND 5.0 07/13/11 13:32
1,1-Dichloropropene ug/kg ND 5.0 07/13/11 13:32
1,2,3-Trichlorobenzene ug/kg ND 5.0 07/13/11 13:32
1,2,3-Trichloropropane ug/kg ND 5.0 07/13/11 13:32
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/13/11 13:32
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/13/11 13:32
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 07/13/11 13:32
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/13/11 13:32
1,2-Dichlorobenzene ug/kg ND 5.0 07/13/11 13:32
1,2-Dichloroethane ug/kg ND 5.0 07/13/11 13:32
1,2-Dichloropropane ug/kg ND 5.0 07/13/11 13:32
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/13/11 13:32
1,3-Dichlorobenzene ug/kg ND 5.0 07/13/11 13:32
1,3-Dichloropropane ug/kg ND 5.0 07/13/11 13:32
1,4-Dichlorobenzene ug/kg ND 5.0 07/13/11 13:32
2,2-Dichloropropane ug/kg ND 5.0 07/13/11 13:32
2-Butanone (MEK)ug/kg ND 100 07/13/11 13:32
2-Chlorotoluene ug/kg ND 5.0 07/13/11 13:32
2-Hexanone ug/kg ND 50.0 07/13/11 13:32
4-Chlorotoluene ug/kg ND 5.0 07/13/11 13:32
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/13/11 13:32
Acetone ug/kg ND 100 07/13/11 13:32
Benzene ug/kg ND 5.0 07/13/11 13:32
Bromobenzene ug/kg ND 5.0 07/13/11 13:32
Bromochloromethane ug/kg ND 5.0 07/13/11 13:32
Bromodichloromethane ug/kg ND 5.0 07/13/11 13:32
Bromoform ug/kg ND 5.0 07/13/11 13:32
Bromomethane ug/kg ND 10.0 07/13/11 13:32
Carbon tetrachloride ug/kg ND 5.0 07/13/11 13:32
Chlorobenzene ug/kg ND 5.0 07/13/11 13:32
Chloroethane ug/kg ND 10.0 07/13/11 13:32
Chloroform ug/kg ND 5.0 07/13/11 13:32
Chloromethane ug/kg ND 10.0 07/13/11 13:32
cis-1,2-Dichloroethene ug/kg ND 5.0 07/13/11 13:32
cis-1,3-Dichloropropene ug/kg ND 5.0 07/13/11 13:32
Dibromochloromethane ug/kg ND 5.0 07/13/11 13:32
Dibromomethane ug/kg ND 5.0 07/13/11 13:32
Dichlorodifluoromethane ug/kg ND 10.0 07/13/11 13:32
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 152 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:632992
Associated Lab Samples:9297694016
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.0 07/13/11 13:32
Ethylbenzene ug/kg ND 5.0 07/13/11 13:32
Hexachloro-1,3-butadiene ug/kg ND 5.0 07/13/11 13:32
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/13/11 13:32
m&p-Xylene ug/kg ND 10.0 07/13/11 13:32
Methyl-tert-butyl ether ug/kg ND 5.0 07/13/11 13:32
Methylene Chloride ug/kg ND 20.0 07/13/11 13:32
n-Butylbenzene ug/kg ND 5.0 07/13/11 13:32
n-Propylbenzene ug/kg ND 5.0 07/13/11 13:32
Naphthalene ug/kg ND 5.0 07/13/11 13:32
o-Xylene ug/kg ND 5.0 07/13/11 13:32
p-Isopropyltoluene ug/kg ND 5.0 07/13/11 13:32
sec-Butylbenzene ug/kg ND 5.0 07/13/11 13:32
Styrene ug/kg ND 5.0 07/13/11 13:32
tert-Butylbenzene ug/kg ND 5.0 07/13/11 13:32
Tetrachloroethene ug/kg ND 5.0 07/13/11 13:32
Toluene ug/kg ND 5.0 07/13/11 13:32
trans-1,2-Dichloroethene ug/kg ND 5.0 07/13/11 13:32
trans-1,3-Dichloropropene ug/kg ND 5.0 07/13/11 13:32
Trichloroethene ug/kg ND 5.0 07/13/11 13:32
Trichlorofluoromethane ug/kg ND 5.0 07/13/11 13:32
Vinyl acetate ug/kg ND 50.0 07/13/11 13:32
Vinyl chloride ug/kg ND 10.0 07/13/11 13:32
Xylene (Total)ug/kg ND 10.0 07/13/11 13:32
1,2-Dichloroethane-d4 (S)%91 70-132 07/13/11 13:32
4-Bromofluorobenzene (S)%98 70-130 07/13/11 13:32
Dibromofluoromethane (S)%92 70-130 07/13/11 13:32
Toluene-d8 (S)%103 70-130 07/13/11 13:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
632993LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 51.750 103 70-131
1,1,1-Trichloroethane ug/kg 48.250 96 70-141
1,1,2,2-Tetrachloroethane ug/kg 52.250 104 70-130
1,1,2-Trichloroethane ug/kg 50.050 100 70-132
1,1-Dichloroethane ug/kg 46.450 93 70-143
1,1-Dichloroethene ug/kg 47.050 94 70-137
1,1-Dichloropropene ug/kg 46.450 93 70-135
1,2,3-Trichlorobenzene ug/kg 51.450 103 69-153
1,2,3-Trichloropropane ug/kg 48.750 97 70-130
1,2,4-Trichlorobenzene ug/kg 51.750 103 55-171
1,2,4-Trimethylbenzene ug/kg 52.150 104 70-149
1,2-Dibromo-3-chloropropane ug/kg 49.950 100 68-141
1,2-Dibromoethane (EDB)ug/kg 50.650 101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 153 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
632993LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 51.850 104 70-140
1,2-Dichloroethane ug/kg 44.950 90 70-137
1,2-Dichloropropane ug/kg 49.950 100 70-133
1,3,5-Trimethylbenzene ug/kg 51.950 104 70-143
1,3-Dichlorobenzene ug/kg 51.950 104 70-144
1,3-Dichloropropane ug/kg 50.450 101 70-132
1,4-Dichlorobenzene ug/kg 50.450 101 70-142
2,2-Dichloropropane ug/kg 46.850 94 68-152
2-Butanone (MEK)ug/kg 92.4J100 92 70-149
2-Chlorotoluene ug/kg 51.650 103 70-141
2-Hexanone ug/kg 97.0100 97 70-149
4-Chlorotoluene ug/kg 53.450 107 70-149
4-Methyl-2-pentanone (MIBK)ug/kg 98.8100 99 70-153
Acetone ug/kg 87.7J100 88 70-157
Benzene ug/kg 46.750 93 70-130
Bromobenzene ug/kg 49.250 98 70-141
Bromochloromethane ug/kg 46.550 93 70-149
Bromodichloromethane ug/kg 50.850 102 70-130
Bromoform ug/kg 46.850 94 70-131
Bromomethane ug/kg 41.750 83 64-136
Carbon tetrachloride ug/kg 49.050 98 70-154
Chlorobenzene ug/kg 52.850 106 70-135
Chloroethane ug/kg 55.850 112 68-151
Chloroform ug/kg 49.050 98 70-130
Chloromethane ug/kg 44.350 89 70-132
cis-1,2-Dichloroethene ug/kg 46.150 92 70-140
cis-1,3-Dichloropropene ug/kg 50.550 101 70-137
Dibromochloromethane ug/kg 50.850 102 70-130
Dibromomethane ug/kg 49.750 99 70-136
Dichlorodifluoromethane ug/kg 48.250 96 36-148
Diisopropyl ether ug/kg 46.350 93 70-139
Ethylbenzene ug/kg 50.650 101 70-137
Hexachloro-1,3-butadiene ug/kg 52.750 105 70-145
Isopropylbenzene (Cumene)ug/kg 52.750 105 70-141
m&p-Xylene ug/kg 104100 104 70-140
Methyl-tert-butyl ether ug/kg 46.150 92 45-150
Methylene Chloride ug/kg 41.350 83 70-133
n-Butylbenzene ug/kg 55.650 111 65-155
n-Propylbenzene ug/kg 53.050 106 70-148
Naphthalene ug/kg 53.950 108 70-148
o-Xylene ug/kg 52.550 105 70-141
p-Isopropyltoluene ug/kg 53.650 107 70-148
sec-Butylbenzene ug/kg 53.150 106 70-145
Styrene ug/kg 54.650 109 70-138
tert-Butylbenzene ug/kg 52.450 105 70-143
Tetrachloroethene ug/kg 52.550 105 70-140
Toluene ug/kg 50.350 101 70-130
trans-1,2-Dichloroethene ug/kg 45.750 91 70-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 154 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
632993LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 48.650 97 70-138
Trichloroethene ug/kg 50.950 102 70-132
Trichlorofluoromethane ug/kg 45.250 90 69-134
Vinyl acetate ug/kg 109100 109 24-161
Vinyl chloride ug/kg 47.850 96 55-140
Xylene (Total)ug/kg 157150 104 70-141
1,2-Dichloroethane-d4 (S)%86 70-132
4-Bromofluorobenzene (S)%103 70-130
Dibromofluoromethane (S)%92 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
633653MATRIX SPIKE SAMPLE:
MSSpike
Result
9297809008
1,1-Dichloroethene ug/kg 42.046 91 49-180ND
Benzene ug/kg 43.946 95 50-166ND
Chlorobenzene ug/kg 45.046 98 43-169ND
Toluene ug/kg 46.746 99 52-163ND
Trichloroethene ug/kg 45.646 99 49-167ND
1,2-Dichloroethane-d4 (S)%84 70-132
4-Bromofluorobenzene (S)%97 70-130
Dibromofluoromethane (S)%91 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result QualifiersRPDResult
9297809004
633652SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 155 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
Dup
Result QualifiersRPDResult
9297809004
633652SAMPLE DUPLICATE:
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg ND10.4J
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg 3.2J3.1J
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg 157 0158
Methylene Chloride ug/kg 21.6 C98.5J
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg 3.1JND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 156 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Parameter Units
Dup
Result QualifiersRPDResult
9297809004
633652SAMPLE DUPLICATE:
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%86 285
4-Bromofluorobenzene (S)%96 593
Dibromofluoromethane (S)%89 191
Toluene-d8 (S)%102 3100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 157 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/4042
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:9297694001, 9297694002, 9297694003, 9297694004, 9297694005, 9297694006, 9297694007, 9297694008,
9297694009, 9297694010, 9297694011, 9297694012, 9297694013, 9297694014, 9297694015
Parameter Units
Dup
Result QualifiersRPDResult
9297667002
630763SAMPLE DUPLICATE:
Percent Moisture %18.2 619.4
Parameter Units
Dup
Result QualifiersRPDResult
9297694015
630764SAMPLE DUPLICATE:
Percent Moisture %15.8 616.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 158 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/4043
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:9297694016, 9297694017, 9297694018, 9297694019, 9297694020, 9297694021, 9297694022
Parameter Units
Dup
Result QualifiersRPDResult
9297590001
630796SAMPLE DUPLICATE:
Percent Moisture %10.3 79.6
Parameter Units
Dup
Result QualifiersRPDResult
9297577011
630797SAMPLE DUPLICATE:
Percent Moisture %19.3 418.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 159 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The internal standard response is below criteria. No hits associated with this internal standard. Results unaffected by
high bias.1g
Common Laboratory Contaminant.C9
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.D6
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery was outside laboratory control limits due to matrix interferences.M3
Sample extract could not be concentrated to the routine final volume, resulting in elevated reporting limits.P3
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 160 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
9297694001 OEXT/14158 GCSV/10105TESTPIT 1A (6)EPA 3546 EPA 8015 Modified
9297694002 OEXT/14158 GCSV/10105TESTPIT 1B (8)EPA 3546 EPA 8015 Modified
9297694003 OEXT/14158 GCSV/10105TESTPIT 2A (6-7)EPA 3546 EPA 8015 Modified
9297694004 OEXT/14158 GCSV/10105TESTPIT 2B (8-9)EPA 3546 EPA 8015 Modified
9297694005 OEXT/14158 GCSV/10105TESTPIT 3A (6-7)EPA 3546 EPA 8015 Modified
9297694006 OEXT/14158 GCSV/10105TESTPIT 3B (8-9)EPA 3546 EPA 8015 Modified
9297694007 OEXT/14158 GCSV/10105TESTPIT 4A (6-7)EPA 3546 EPA 8015 Modified
9297694008 OEXT/14158 GCSV/10105TESTPIT 4B (9-10)EPA 3546 EPA 8015 Modified
9297694009 OEXT/14158 GCSV/10105TESTPIT 5A (6-7)EPA 3546 EPA 8015 Modified
9297694010 OEXT/14160 GCSV/10110TESTPIT 5B (9-10)EPA 3546 EPA 8015 Modified
9297694011 OEXT/14160 GCSV/10110TESTPIT 6A (6-7)EPA 3546 EPA 8015 Modified
9297694012 OEXT/14160 GCSV/10110TESTPIT 6B (9-10)EPA 3546 EPA 8015 Modified
9297694013 OEXT/14160 GCSV/10110TESTPIT 7A (6-7)EPA 3546 EPA 8015 Modified
9297694014 OEXT/14160 GCSV/10110TESTPIT 7B (9-10)EPA 3546 EPA 8015 Modified
9297694015 OEXT/14160 GCSV/10110TESTPIT 8A (6-7)EPA 3546 EPA 8015 Modified
9297694016 OEXT/14160 GCSV/10110TESTPIT 8B (13-14)EPA 3546 EPA 8015 Modified
9297694017 OEXT/14160 GCSV/10110TESTPIT 9A (4-6)EPA 3546 EPA 8015 Modified
9297694018 OEXT/14160 GCSV/10110TESTPIT 10A (6-7)EPA 3546 EPA 8015 Modified
9297694019 OEXT/14160 GCSV/10110TESTPIT 10A (9-10)EPA 3546 EPA 8015 Modified
9297694020 OEXT/14160 GCSV/10110TESTPIT 11A (6-7)EPA 3546 EPA 8015 Modified
9297694021 OEXT/14160 GCSV/10110TESTPIT 11A (8-9)EPA 3546 EPA 8015 Modified
9297694022 OEXT/14160 GCSV/10110TESTPIT 9A (15-16)EPA 3546 EPA 8015 Modified
9297694001 GCSV/10103 GCSV/10107TESTPIT 1A (6)9071B 9071B
9297694002 GCSV/10103 GCSV/10107TESTPIT 1B (8)9071B 9071B
9297694003 GCSV/10103 GCSV/10107TESTPIT 2A (6-7)9071B 9071B
9297694004 GCSV/10103 GCSV/10107TESTPIT 2B (8-9)9071B 9071B
9297694005 GCSV/10103 GCSV/10107TESTPIT 3A (6-7)9071B 9071B
9297694006 GCSV/10103 GCSV/10107TESTPIT 3B (8-9)9071B 9071B
9297694007 GCSV/10103 GCSV/10107TESTPIT 4A (6-7)9071B 9071B
9297694008 GCSV/10103 GCSV/10107TESTPIT 4B (9-10)9071B 9071B
9297694009 GCSV/10103 GCSV/10107TESTPIT 5A (6-7)9071B 9071B
9297694010 GCSV/10103 GCSV/10107TESTPIT 5B (9-10)9071B 9071B
9297694011 GCSV/10103 GCSV/10107TESTPIT 6A (6-7)9071B 9071B
9297694012 GCSV/10103 GCSV/10107TESTPIT 6B (9-10)9071B 9071B
9297694013 GCSV/10103 GCSV/10107TESTPIT 7A (6-7)9071B 9071B
9297694014 GCSV/10103 GCSV/10107TESTPIT 7B (9-10)9071B 9071B
9297694015 GCSV/10103 GCSV/10107TESTPIT 8A (6-7)9071B 9071B
9297694016 GCSV/10103 GCSV/10107TESTPIT 8B (13-14)9071B 9071B
9297694017 GCSV/10103 GCSV/10107TESTPIT 9A (4-6)9071B 9071B
9297694018 GCSV/10103 GCSV/10107TESTPIT 10A (6-7)9071B 9071B
9297694019 GCSV/10103 GCSV/10107TESTPIT 10A (9-10)9071B 9071B
9297694020 GCSV/10118 GCSV/10123TESTPIT 11A (6-7)9071B 9071B
9297694021 GCSV/10118 GCSV/10123TESTPIT 11A (8-9)9071B 9071B
9297694022 GCSV/10118 GCSV/10123TESTPIT 9A (15-16)9071B 9071B
9297694001 GCV/5193 GCV/5194TESTPIT 1A (6)EPA 5035A/5030B EPA 8015 Modified
9297694002 GCV/5193 GCV/5194TESTPIT 1B (8)EPA 5035A/5030B EPA 8015 Modified
9297694003 GCV/5193 GCV/5194TESTPIT 2A (6-7)EPA 5035A/5030B EPA 8015 Modified
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 161 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
9297694004 GCV/5193 GCV/5194TESTPIT 2B (8-9)EPA 5035A/5030B EPA 8015 Modified
9297694005 GCV/5193 GCV/5194TESTPIT 3A (6-7)EPA 5035A/5030B EPA 8015 Modified
9297694006 GCV/5193 GCV/5194TESTPIT 3B (8-9)EPA 5035A/5030B EPA 8015 Modified
9297694007 GCV/5193 GCV/5194TESTPIT 4A (6-7)EPA 5035A/5030B EPA 8015 Modified
9297694008 GCV/5193 GCV/5194TESTPIT 4B (9-10)EPA 5035A/5030B EPA 8015 Modified
9297694009 GCV/5193 GCV/5194TESTPIT 5A (6-7)EPA 5035A/5030B EPA 8015 Modified
9297694010 GCV/5193 GCV/5194TESTPIT 5B (9-10)EPA 5035A/5030B EPA 8015 Modified
9297694011 GCV/5198 GCV/5199TESTPIT 6A (6-7)EPA 5035A/5030B EPA 8015 Modified
9297694012 GCV/5198 GCV/5199TESTPIT 6B (9-10)EPA 5035A/5030B EPA 8015 Modified
9297694013 GCV/5198 GCV/5199TESTPIT 7A (6-7)EPA 5035A/5030B EPA 8015 Modified
9297694014 GCV/5198 GCV/5199TESTPIT 7B (9-10)EPA 5035A/5030B EPA 8015 Modified
9297694015 GCV/5198 GCV/5199TESTPIT 8A (6-7)EPA 5035A/5030B EPA 8015 Modified
9297694016 GCV/5198 GCV/5199TESTPIT 8B (13-14)EPA 5035A/5030B EPA 8015 Modified
9297694017 GCV/5198 GCV/5199TESTPIT 9A (4-6)EPA 5035A/5030B EPA 8015 Modified
9297694018 GCV/5198 GCV/5199TESTPIT 10A (6-7)EPA 5035A/5030B EPA 8015 Modified
9297694019 GCV/5198 GCV/5199TESTPIT 10A (9-10)EPA 5035A/5030B EPA 8015 Modified
9297694020 GCV/5198 GCV/5199TESTPIT 11A (6-7)EPA 5035A/5030B EPA 8015 Modified
9297694021 GCV/5198 GCV/5199TESTPIT 11A (8-9)EPA 5035A/5030B EPA 8015 Modified
9297694022 GCV/5198 GCV/5199TESTPIT 9A (15-16)EPA 5035A/5030B EPA 8015 Modified
9297694001 MPRP/8714 ICP/8050TESTPIT 1A (6)EPA 3050 EPA 6010
9297694002 MPRP/8714 ICP/8050TESTPIT 1B (8)EPA 3050 EPA 6010
9297694003 MPRP/8714 ICP/8050TESTPIT 2A (6-7)EPA 3050 EPA 6010
9297694004 MPRP/8714 ICP/8050TESTPIT 2B (8-9)EPA 3050 EPA 6010
9297694005 MPRP/8714 ICP/8050TESTPIT 3A (6-7)EPA 3050 EPA 6010
9297694006 MPRP/8714 ICP/8050TESTPIT 3B (8-9)EPA 3050 EPA 6010
9297694007 MPRP/8714 ICP/8050TESTPIT 4A (6-7)EPA 3050 EPA 6010
9297694008 MPRP/8714 ICP/8050TESTPIT 4B (9-10)EPA 3050 EPA 6010
9297694009 MPRP/8714 ICP/8050TESTPIT 5A (6-7)EPA 3050 EPA 6010
9297694010 MPRP/8714 ICP/8050TESTPIT 5B (9-10)EPA 3050 EPA 6010
9297694011 MPRP/8715 ICP/8051TESTPIT 6A (6-7)EPA 3050 EPA 6010
9297694012 MPRP/8715 ICP/8051TESTPIT 6B (9-10)EPA 3050 EPA 6010
9297694013 MPRP/8715 ICP/8051TESTPIT 7A (6-7)EPA 3050 EPA 6010
9297694014 MPRP/8715 ICP/8051TESTPIT 7B (9-10)EPA 3050 EPA 6010
9297694015 MPRP/8715 ICP/8051TESTPIT 8A (6-7)EPA 3050 EPA 6010
9297694016 MPRP/8715 ICP/8051TESTPIT 8B (13-14)EPA 3050 EPA 6010
9297694017 MPRP/8715 ICP/8051TESTPIT 9A (4-6)EPA 3050 EPA 6010
9297694018 MPRP/8715 ICP/8051TESTPIT 10A (6-7)EPA 3050 EPA 6010
9297694019 MPRP/8715 ICP/8051TESTPIT 10A (9-10)EPA 3050 EPA 6010
9297694020 MPRP/8715 ICP/8051TESTPIT 11A (6-7)EPA 3050 EPA 6010
9297694021 MPRP/8715 ICP/8051TESTPIT 11A (8-9)EPA 3050 EPA 6010
9297694022 MPRP/8715 ICP/8051TESTPIT 9A (15-16)EPA 3050 EPA 6010
9297694001 MERP/3599 MERC/3549TESTPIT 1A (6)EPA 7471 EPA 7471
9297694002 MERP/3599 MERC/3549TESTPIT 1B (8)EPA 7471 EPA 7471
9297694003 MERP/3599 MERC/3549TESTPIT 2A (6-7)EPA 7471 EPA 7471
9297694004 MERP/3599 MERC/3549TESTPIT 2B (8-9)EPA 7471 EPA 7471
9297694005 MERP/3599 MERC/3549TESTPIT 3A (6-7)EPA 7471 EPA 7471
9297694006 MERP/3599 MERC/3549TESTPIT 3B (8-9)EPA 7471 EPA 7471
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 162 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
9297694007 MERP/3599 MERC/3549TESTPIT 4A (6-7)EPA 7471 EPA 7471
9297694008 MERP/3599 MERC/3549TESTPIT 4B (9-10)EPA 7471 EPA 7471
9297694009 MERP/3599 MERC/3549TESTPIT 5A (6-7)EPA 7471 EPA 7471
9297694010 MERP/3599 MERC/3549TESTPIT 5B (9-10)EPA 7471 EPA 7471
9297694011 MERP/3599 MERC/3549TESTPIT 6A (6-7)EPA 7471 EPA 7471
9297694012 MERP/3599 MERC/3549TESTPIT 6B (9-10)EPA 7471 EPA 7471
9297694013 MERP/3599 MERC/3549TESTPIT 7A (6-7)EPA 7471 EPA 7471
9297694014 MERP/3599 MERC/3549TESTPIT 7B (9-10)EPA 7471 EPA 7471
9297694015 MERP/3599 MERC/3549TESTPIT 8A (6-7)EPA 7471 EPA 7471
9297694016 MERP/3599 MERC/3549TESTPIT 8B (13-14)EPA 7471 EPA 7471
9297694017 MERP/3599 MERC/3549TESTPIT 9A (4-6)EPA 7471 EPA 7471
9297694018 MERP/3614 MERC/3562TESTPIT 10A (6-7)EPA 7471 EPA 7471
9297694019 MERP/3614 MERC/3562TESTPIT 10A (9-10)EPA 7471 EPA 7471
9297694020 MERP/3614 MERC/3562TESTPIT 11A (6-7)EPA 7471 EPA 7471
9297694021 MERP/3614 MERC/3562TESTPIT 11A (8-9)EPA 7471 EPA 7471
9297694022 MERP/3614 MERC/3562TESTPIT 9A (15-16)EPA 7471 EPA 7471
9297694001 OEXT/14156 MSSV/5146TESTPIT 1A (6)EPA 3546 EPA 8270
9297694002 OEXT/14156 MSSV/5146TESTPIT 1B (8)EPA 3546 EPA 8270
9297694003 OEXT/14156 MSSV/5146TESTPIT 2A (6-7)EPA 3546 EPA 8270
9297694004 OEXT/14156 MSSV/5146TESTPIT 2B (8-9)EPA 3546 EPA 8270
9297694005 OEXT/14156 MSSV/5146TESTPIT 3A (6-7)EPA 3546 EPA 8270
9297694006 OEXT/14156 MSSV/5146TESTPIT 3B (8-9)EPA 3546 EPA 8270
9297694007 OEXT/14156 MSSV/5146TESTPIT 4A (6-7)EPA 3546 EPA 8270
9297694008 OEXT/14156 MSSV/5146TESTPIT 4B (9-10)EPA 3546 EPA 8270
9297694009 OEXT/14156 MSSV/5146TESTPIT 5A (6-7)EPA 3546 EPA 8270
9297694010 OEXT/14156 MSSV/5146TESTPIT 5B (9-10)EPA 3546 EPA 8270
9297694011 OEXT/14161 MSSV/5135TESTPIT 6A (6-7)EPA 3546 EPA 8270
9297694012 OEXT/14161 MSSV/5135TESTPIT 6B (9-10)EPA 3546 EPA 8270
9297694013 OEXT/14161 MSSV/5135TESTPIT 7A (6-7)EPA 3546 EPA 8270
9297694014 OEXT/14161 MSSV/5135TESTPIT 7B (9-10)EPA 3546 EPA 8270
9297694015 OEXT/14161 MSSV/5135TESTPIT 8A (6-7)EPA 3546 EPA 8270
9297694016 OEXT/14161 MSSV/5135TESTPIT 8B (13-14)EPA 3546 EPA 8270
9297694017 OEXT/14161 MSSV/5135TESTPIT 9A (4-6)EPA 3546 EPA 8270
9297694018 OEXT/14161 MSSV/5135TESTPIT 10A (6-7)EPA 3546 EPA 8270
9297694019 OEXT/14161 MSSV/5135TESTPIT 10A (9-10)EPA 3546 EPA 8270
9297694020 OEXT/14161 MSSV/5135TESTPIT 11A (6-7)EPA 3546 EPA 8270
9297694021 OEXT/14176 MSSV/5139TESTPIT 11A (8-9)EPA 3546 EPA 8270
9297694022 OEXT/14176 MSSV/5139TESTPIT 9A (15-16)EPA 3546 EPA 8270
9297694001 MSV/15970TESTPIT 1A (6)EPA 8260
9297694002 MSV/15970TESTPIT 1B (8)EPA 8260
9297694003 MSV/15970TESTPIT 2A (6-7)EPA 8260
9297694004 MSV/15970TESTPIT 2B (8-9)EPA 8260
9297694005 MSV/15970TESTPIT 3A (6-7)EPA 8260
9297694006 MSV/15970TESTPIT 3B (8-9)EPA 8260
9297694007 MSV/15970TESTPIT 4A (6-7)EPA 8260
9297694008 MSV/15970TESTPIT 4B (9-10)EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 163 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
9297694
JERRY BAKER PROPERTY 39010.1.1
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
9297694009 MSV/15970TESTPIT 5A (6-7)EPA 8260
9297694010 MSV/15970TESTPIT 5B (9-10)EPA 8260
9297694011 MSV/15970TESTPIT 6A (6-7)EPA 8260
9297694012 MSV/15970TESTPIT 6B (9-10)EPA 8260
9297694013 MSV/15970TESTPIT 7A (6-7)EPA 8260
9297694014 MSV/15970TESTPIT 7B (9-10)EPA 8260
9297694015 MSV/15970TESTPIT 8A (6-7)EPA 8260
9297694016 MSV/15994TESTPIT 8B (13-14)EPA 8260
9297694017 MSV/15983TESTPIT 9A (4-6)EPA 8260
9297694018 MSV/15983TESTPIT 10A (6-7)EPA 8260
9297694019 MSV/15983TESTPIT 10A (9-10)EPA 8260
9297694020 MSV/15983TESTPIT 11A (6-7)EPA 8260
9297694021 MSV/15983TESTPIT 11A (8-9)EPA 8260
9297694022 MSV/15983TESTPIT 9A (15-16)EPA 8260
9297694001 PMST/4042TESTPIT 1A (6)ASTM D2974-87
9297694002 PMST/4042TESTPIT 1B (8)ASTM D2974-87
9297694003 PMST/4042TESTPIT 2A (6-7)ASTM D2974-87
9297694004 PMST/4042TESTPIT 2B (8-9)ASTM D2974-87
9297694005 PMST/4042TESTPIT 3A (6-7)ASTM D2974-87
9297694006 PMST/4042TESTPIT 3B (8-9)ASTM D2974-87
9297694007 PMST/4042TESTPIT 4A (6-7)ASTM D2974-87
9297694008 PMST/4042TESTPIT 4B (9-10)ASTM D2974-87
9297694009 PMST/4042TESTPIT 5A (6-7)ASTM D2974-87
9297694010 PMST/4042TESTPIT 5B (9-10)ASTM D2974-87
9297694011 PMST/4042TESTPIT 6A (6-7)ASTM D2974-87
9297694012 PMST/4042TESTPIT 6B (9-10)ASTM D2974-87
9297694013 PMST/4042TESTPIT 7A (6-7)ASTM D2974-87
9297694014 PMST/4042TESTPIT 7B (9-10)ASTM D2974-87
9297694015 PMST/4042TESTPIT 8A (6-7)ASTM D2974-87
9297694016 PMST/4043TESTPIT 8B (13-14)ASTM D2974-87
9297694017 PMST/4043TESTPIT 9A (4-6)ASTM D2974-87
9297694018 PMST/4043TESTPIT 10A (6-7)ASTM D2974-87
9297694019 PMST/4043TESTPIT 10A (9-10)ASTM D2974-87
9297694020 PMST/4043TESTPIT 11A (6-7)ASTM D2974-87
9297694021 PMST/4043TESTPIT 11A (8-9)ASTM D2974-87
9297694022 PMST/4043TESTPIT 9A (15-16)ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/19/2011 09:24 AM Page 164 of 164
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]