18056_Dillon Station_USTClosures 1-3_20170207

February 7, 2017 Mr. James Rudder North Carolina Department of Environmental Quality Division of Waste Management NC Brownfields Program 1601 Mail Service Center Raleigh, North Carolina 27699-1601 Subject: Underground Storage Tank Closures Dillon Station Redevelopment Project - Raleigh, North Carolina NCDEQ Brownfields Project #18056-14-092 HES Project #306007 Dear Mr. Rudder: On behalf of our client, Dillon Station, LLC, Highlands Environmental Solutions, Inc. (HES) is submitting this correspondence regarding the removal of underground storage tanks (USTs) at the above-referenced site. As you are aware, this site is being redeveloped under a Brownfields Agreement with the North Carolina Department of Environmental Quality (NCDEQ). Site Characteristics
The Dillon Station, LLC site (The Dillon) is located at 406 West Hargett Street; in Raleigh, Wake County, North Carolina. The approximate location of the site is graphically presented on Figure 1 (included in Attachment A), and is situated at approximate coordinates UST #1 and UST#2: 35.778123 N and – 78.645935 W; UST #3: 35.777490 N and –78.645255 W. A topographic map of the area is included as Figure 2.
The site is located in the Warehouse District of downtown Raleigh, North Carolina. The land use of surrounding properties consists primarily of commercial and municipal land uses. Historically, the property was utilized for industrial land uses.
The site is located in central Wake County, which is situated in the Piedmont Physiographic Province (Piedmont) of North Carolina. The Piedmont is characterized by gently rolling topography and deeply
weathered bedrock. Dendritic surface drainage patterns generally allow for good drainage within this region. The region is characterized by a soil veneer derived from weathered rock, or saprolite, which overlies bedrock. The thickness of the saprolitic soil varies considerably between locations, however, it is generally thicker in areas where topographic slope is small, and infiltration from precipitation is abundant.
A variety of igneous and metamorphic rocks make up the Piedmont bedrock, which occurs at varying depths, and is typically fractured by jointing and faulting. Joints are most abundant at shallow depths in
the bedrock where overburden pressures are minimal; whereas faults commonly extend to considerable depths.
8410-D Falls of Neuse Road; Raleigh, NC 27615 Phone: [phone] / Fax: [phone] / www.HESfast.com
Mr. James Rudder February 7, 2017 Underground Storage Tank Closures – Dillon Station Development Site; Raleigh, NC Page 2
Geologically, the Piedmont is divided into a series of northeast-southwest trending “belts” which are generally defined as “…areas of regionally metamorphosed rocks delineated and characterized on the basis of their metamorphism.” (Metamorphism typically refers to a broad re-crystallization of igneous rocks under various levels or “grades” of intense heat and pressure). Based on a review of the Geologic Map of North Carolina (1985), the site is located in the Raleigh Belt, which is underlain by igneous and metamorphic rock assemblages. Although not determined during this assessment, the depth to bedrock in the immediate area typically ranges from approximately 20 and 35 feet below grade. Groundwater occurs within two distinct water-bearing units in the subsurface in the vicinity of the site. The initial water-bearing unit is the surficial aquifer. Within the surficial aquifer, groundwater movement is facilitated through pore spaces between soil particles. The direction of groundwater movement typically mirrors surface topography, as flow is generally in response to gravity. The second water-bearing unit is the bedrock aquifer. In the bedrock aquifer, groundwater may be found in bedrock fractures and/or cavities. Groundwater movement in the bedrock unit is controlled by fracture orientation and connectivity, and is not necessarily controlled by gravity. The two aquifers may or may not be locally interconnected depending on local conditions. Discharge of stored groundwater occurs primarily as baseflow to surface water bodies, and/or discharge from “springs.” Hydraulic conductivity values for the surficial aquifer range from less than one to several feet per day, while values for fractured rock vary greatly. The depth to groundwater in the surficial aquifer beneath the site was determined during previous environmental assessment activities performed at the site, and is approximately 16 feet below grade. UST Information
Tank Number Install Date Capacity Dimensions Contents Date Removed
#1 Unknown 8,000-gallon 6’x18’ Fuel Oil (assumed) May 10, 2016
#2 Unknown 8,000-gallon 6’x18’ Fuel Oil (assumed) May 10, 2016
#3 Unknown 3,000-gallon 6’x7’ Fuel Oil (assumed) July 20, 2016
UST Closure Procedures The subject USTs were orphaned USTs, and were identified during an environmental assessment that
was conducted at the site. During both UST removal activities’ (May 10 and July 20, 2016) the following activities were initiated and completed. HES inspected the site, and coordinated UST removal activities (including the location of subsurface utilities, securing a permit from the Raleigh Fire Department, etc.). HES also prepared a site-specific health and safety plan (HASP) to ensure personnel safety while onsite; and completed and submitted a UST-3 Form (Notice of Intent: UST Permanent Closure or Change in Service) to the North Carolina Department of Environmental Quality (NCDEQ) Copies of the UST-3 Form
and the Fire Permit form are included in Attachment B. The location of the former USTs are depicted on Figure 3.
Personnel from HES and EHG, LLC (EHG) mobilized to the site to remove residual sludge and liquids from the USTs using a vacuum truck (May 10 and July 20, 2016). The waste material was removed and transported to A&D Environmental Services, Inc. (A&D) in Archdale, NC for disposal. Copies of the waste disposal documentation are included in Attachment C. Personnel from HES and EHG continued UST removal activities at the site on May 10 and July 20, 2016. EHG provided equipment and labor for soil excavation and tank removal. The excavation areas were originally covered with asphalt and concrete, which was removed prior to UST removal. During UST closure, overburden soil was removed from the top and sides of the USTs. The depth to the top of the tanks was approximately three feet below grade. Random soil samples were
Mr. James Rudder February 7, 2017 Underground Storage Tank Closures – Dillon Station Development Site; Raleigh, NC Page 3
collected during soil excavation and field screened for organic vapors using a photoionization detector (PID). All excavated soil remained at the site. As noted earlier, random soil samples were collected during excavation activities. Native soil primarily consisted of reddish brown silty clay and some reddish brown-orange sand from 0 to approximately 11 feet below grade. During overburden removal, the soil was evaluated for evidence of petroleum impacts (i.e., staining, etc.). Evidence of petroleum impact was not observed in the soil around the former fill port and of the USTs. The random soil samples were collected and field screened. To field screen the soil samples, an aliquot of soil was placed in a clean, labeled, zip-lock bag and allowed to volatilize in direct sunlight for approximately 10 minutes. At the end of the volatilization period, the headspace in the sample bags was sampled for total volatiles using the PID, which was calibrated to a 100 ppm Isobutylene standard. After the top of the former USTs were exposed, the condition of the tank atmospheres was verified using a MultiRAE four gas meter. After removal, the USTs were examined and found to be in good condition. Only slight pitting was observed on the bottom of the USTs. No obvious holes were observed in the former USTs. Following removal of the USTs, the USTs were transported to A&D in Archdale, NC for disposal. Neither product lines nor fuel dispensers were located at the site. Select photographs of site activities and tank conditions are included in Attachment D. Groundwater was not encountered in the UST basins. Following removal of the tanks, soil samples were collected from the UST excavations. Upon collection, the samples were split into two aliquots. The first aliquot was placed in clean, labeled, laboratory-supplied containers, maintained on ice, and transported to SGS Accutest for laboratory analysis of volatile organic compounds (VOCs) by Method 8260, and semi-volatile organic compounds (SVOCs) by Method 8270. The UST information and the UST owner/operator information are included in Table 1 and Table 2, respectively; in Attachment E. Laboratory analytical and field screening data are summarized on Table 3a and Table 3b. A copy of the complete laboratory analytical data report is included in Attachment F. Sample collection locations are depicted on Figure 4a and Figure 4b. Conclusions and Recommendations
On May 10, 2016, two, orphaned, 8,000-gallon USTs were closed by removal at the Dillon Station Site, in Raleigh, North Carolina. On July 20, 2016, one, orphaned, 3,000-gallon UST was closed by removal at Dillon Station Site, in Raleigh, North Carolina. The subject site is part of The Dillon development site. The subject site is being redeveloped under a Brownfields Agreement with the NCDEQ. The former USTs were described as being in good condition, with no corrosion-related holes being observed. A UST-2 (Site Investigation Report) for the UST closure is included in Attachment G.
May 2016 Findings (UST #1 and UST#2 Closures) Petroleum-impacted soil was not observed within the excavated material from the USTs (UST #1 and UST#2). Based on analytical data for soil samples collected following UST closures, petroleum impacts
were identified. Naphthalene was detected in sample UST-4 at a concentration of 6 mg/kg (NCDEQ soil-to-water MSCC: 0.160 mg/kg). This sample is located within the center of the excavation on the eastern
most side wall at a depth of 8 feet below grade. Other constituents were detected at the site; however, the concentrations of these compounds were less than their respective Soil to Water Maximum Soil Contaminant Concentrations (MSCCs).
July 2016 Findings (UST #3 Closures) Petroleum-impacted soil was not observed within the excavated material from the UST. Based on
analytical data for soil samples collected following UST closures, petroleum impacts were identified. In soil sample UST-9 concentrations of benzo(a)anthracene, benzo(a)pyrene, and benzo(b)flouranthene
Mr. James Rudder February 7, 2017 Underground Storage Tank Closures – Dillon Station Development Site; Raleigh, NC Page 4
were detected above the NCDEQ soil-to-water MSCCs. This sample is located within the center of the excavation on the western most side wall at a depth of 8 feet below grade. Other constituents were detected at the site; however, the concentrations of these compounds were less than their respective Soil to Water Maximum Soil Contaminant Concentrations (MSCCs). Based on the results of this investigation, HES concludes that a release of petroleum did occur from the former UST system (UST#1, UST#2, and UST#3); however, the site is currently in the brownfields program and as such, no additional environmental assessment and/or remediation are recommended at the subject site. Certification and Limitations Highlands Environmental Solutions, Inc. (HES) has performed the investigation documented in this report in a professional manner using generally accepted environmental practices. This report shall not be construed to create any warranty regarding the property on which the investigation was conducted. This report is a representation and presentation of the findings and conclusions of HES based upon observations made at the time of site reconnaissance visits; personal interviews; research of available documents (records, maps, etc.) held by the appropriate government and private agencies; and and/or analytical data for samples collected during the course of the investigation. This report is subject to the limitation of historical documentation, and the availability and accuracy of pertinent records. HES shall not be responsible for conditions, or consequences, arising from relevant facts that were concealed, withheld or not fully disclosed to HES at the time the investigation was performed. This report is intended solely for the use of Dillon Station, LLC; their subsidiaries; their agents; and consultants, and the North Carolina Department of Environmental Quality. The information provided in this report is relevant to the dates of our site and research activities, and should not be relied upon to represent conditions at future dates. With reference to the applicable technical requirements of 15 NCAC 2L .0115, and pursuant to 15A NCAC 2L .0103(e), I certify that the work described herein has been performed in accordance with industry standards and practices by me, or under my direct supervision. On behalf of our client, Highlands Environmental Solutions, Inc. respectfully requests that this matter be closed. If there are any questions regarding this correspondence, or the project in general, please contact me at [phone]. Sincerely,
Highlands Environmental Solutions, Inc. Bill Frederick Senior Environmental Scientist Bobby J. Beaman, P.G., RSM Principal Geologist NC Licensed Geologist #1468 Attachments cc: Mr. Greg Kuruc – Dillon Station, LLC Mr. John Gallagher – Aptus Management File
Attachment A

Project Name
Client
Project # Drawn by
Fig. # Scale Date
N
Property Location Diagram Base diagram from MicroSoft Streets and Trips Plus.
UST Closure Dillon Supply Property
Dillon Station, LLC
306007 BF
None August 2016 1
Approximate Site Location

Project Name
Client
Project # Drawn by
Fig. # Scale Date
N
Topographic Location Diagram Base diagram USGS 7.5 Minute Topographic Map; Raleigh West; 2002
UST Closure Dillon Supply Property
Dillon Station, LLC
306007 BF
None August 2016 2
Approximate Site Location

Attachment B

Attachment C

Attachment D

Photograph Number 1: Looking south across area of UST location (excavation open).
Photograph Number 2: Looking southwest area of UST location (excavation open).

Photograph Number 3: Removal of UST from excavation area (typical).
Photograph Number 4: Removal of UST from excavation area (typical).

Photograph Number 5: Excavation area after UST removal looking south.
Photograph Number 6: Excavation area after UST removal looking north.

Photograph Number 7: Former UST area with excavated material placed back and surfaces
secured.
Photograph Number 8: Former UST area with excavated material placed back and surfaces
secured.

Photograph Number 9: Looking south across area of UST location (excavation open).
Photograph Number 10: Looking north across area of UST location (excavation open).

Photograph Number 11: Removal of UST from excavation area (typical).
Photograph Number 12: Removal of UST from excavation area (typical).

Photograph Number 13: Excavation area after UST removal looking south.
Photograph Number 14: Excavation area after UST removal looking north.

Photograph Number 15: Former UST area with excavated material placed back and additional flowable fill and surfaces secured.
Attachment E
Attachment F
Report Number:31600936
Client Project:Dillon Station
Laboratory Report of Analysis
Joe Beaman
HIGHLANDS ENVIRONMENTAL SERVICES
8410-D Falls of Neuse Road
RALEIGH, NC 27615
US
To:
Dear Joe Beaman,
Enclosed are the results of the analytical services performed under the referenced project for the received
samples and associated QC as applicable. The samples analyzed at the SGS Wilmington location are certified to
meet the requirements of the National Environmental Laboratory Accreditation Conference Standards, unless
otherwise noted. Copies of this report and supporting data will be retained in our files for a period of five years in
the event they are required for future reference. All results are intended to be used in their entirety and SGS is not
responsible for use of less than the complete report. Any samples submitted to our laboratory will be retained for a
maximum of thirty (30) days from the date of this report unless other arrangements are requested.
If there are any questions about the report or services performed during this project, please call Michael D. Page
at [phone]. We will be happy to answer any questions or concerns which you may have.
Thank you for using SGS North America Inc. for your analytical services. We look forward to working with you
again on any additional analytical needs.
Sincerely,
SGS North America Inc.
__________________________________________________________________
Michael D. Page Date
Project Manager
[e-mail]
Print Date: 05/23/2016 N.C. Certification # 481
Terms and Conditions:
All services are rendered in accordance with the applicable SGS General Conditions of Service accessible via:
http://www.sgs.com/terms_and_conditions.htm
Page 1 of 62
Laboratory Qualifiers
Report Definitions
DL Method, Instrument, or Estimated Detection Limit per Analytical Method
CL Control Limits for the recovery result of a parameter
LOQ Reporting Limit
DF Dilution Factor
RPD Relative Percent Difference
LCS(D)Laboratory Control Spike (Duplicate)
MS(D)Matrix Spike (Duplicate)
MB Method Blank
Qualifier Definitions
*Recovery or RPD outside of control limits
B Analyte was detected in the Lab Method Blank at a level above the LOQ
U Undetected (Reported as ND or < DL)
J Estimated Concentration.
E Amount detected is greater than the Upper Calibration Limit
TIC Tentatively Identified Compound
ND Not Detected
P RPD > 40% between results of dual columns
D Spike or surrogate was diluted out in order to achieve a parameter result within instrument calibration
range
Samples requiring manual integrations for various congeners and/or standards are marked and dated by the analyst. A
code definition is provided below:
M1 Mis-identified peak
M2 Software did not integrate peak
M3 Incorrect baseline construction (i.e. not all of peak included; two peaks integrated as one)
M4 Pattern integration required (i.e. DRO, GRO, PCB, Toxaphene and Technical Chlordane)
M5 Other - Explained in case narrative
Note Results pages that include a value for "Solids (%)" have been adjusted for moisture content.
Print Date: 05/23/2016 N.C. Certification # 481
Page 2 of 62
Sample Summary
Client Sample ID Lab Sample ID Collected Received Matrix
UST-1 31600936001 05/10/2016 16:30 05/12/2016 09:52 Soil-Solid as dry weight
UST-2 31600936002 05/10/2016 16:35 05/12/2016 09:52 Soil-Solid as dry weight
UST-3 31600936003 05/10/2016 16:40 05/12/2016 09:52 Soil-Solid as dry weight
UST-4 31600936004 05/10/2016 16:45 05/12/2016 09:52 Soil-Solid as dry weight
UST-5 31600936005 05/10/2016 16:50 05/12/2016 09:52 Soil-Solid as dry weight
Print Date: 05/23/2016 N.C. Certification # 481
Page 3 of 62
Case Narrative
UST-3
8260B - The recovery of surrogate 4­Bromofluorobenzene was above the QC control limits due to matrix interferences. Confirmed
by duplicate analysis.

Print Date: 05/23/2016 N.C. Certification # 481
Page 4 of 62
Detectable Results Summary
Client Sample ID: UST-2
Lab Sample ID: 31600936002-A UnitsParameterResult
Acetone ug/KgSW-846 8260B 71.3
Client Sample ID: UST-3
Lab Sample ID: 31600936003-B UnitsParameterResult
Acetone ug/KgSW-846 8260B 60.6
Phenanthrene ug/KgSW-846 8270D 3000
Client Sample ID: UST-4
Lab Sample ID: 31600936004-A UnitsParameterResult
n-Butylbenzene ug/KgSW-846 8260B 400
Naphthalene ug/Kg6050
Client Sample ID: UST-5
Lab Sample ID: 31600936005-A UnitsParameterResult
Chlorodibromomethane ug/KgSW-846 8260B 208
Print Date: 05/23/2016 N.C. Certification # 481
Page 5 of 62
Client Sample ID: UST-1
Client Project ID: Dillon Station
Lab Sample ID: 31600936001-A
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:30
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 75.80
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-1
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/Kg 15.04 05/17/2016 14:20
1,1,1-Trichloroethane ND ug/Kg 15.04 05/17/2016 14:20
1,1,2,2-Tetrachloroethane ND ug/Kg 15.04 05/17/2016 14:20
1,1,2-Trichloroethane ND ug/Kg 15.04 05/17/2016 14:20
1,1-Dichloroethane ND ug/Kg 15.04 05/17/2016 14:20
1,1-Dichloroethene ND ug/Kg 15.04 05/17/2016 14:20
1,1-Dichloropropene ND ug/Kg 15.04 05/17/2016 14:20
1,2,3-Trichlorobenzene ND ug/Kg 15.04 05/17/2016 14:20
1,2,3-Trichloropropane ND ug/Kg 15.04 05/17/2016 14:20
1,2,4-Trichlorobenzene ND ug/Kg 15.04 05/17/2016 14:20
1,2,4-Trimethylbenzene ND ug/Kg 15.04 05/17/2016 14:20
1,2-Dibromo-3-chloropropane ND ug/Kg 130.2 05/17/2016 14:20
1,2-Dibromoethane ND ug/Kg 15.04 05/17/2016 14:20
1,2-Dichlorobenzene ND ug/Kg 15.04 05/17/2016 14:20
1,2-Dichloroethane ND ug/Kg 15.04 05/17/2016 14:20
1,2-Dichloropropane ND ug/Kg 15.04 05/17/2016 14:20
1,3,5-Trimethylbenzene ND ug/Kg 15.04 05/17/2016 14:20
1,3-Dichlorobenzene ND ug/Kg 15.04 05/17/2016 14:20
1,3-Dichloropropane ND ug/Kg 15.04 05/17/2016 14:20
1,4-Dichlorobenzene ND ug/Kg 15.04 05/17/2016 14:20
2,2-Dichloropropane ND ug/Kg 15.04 05/17/2016 14:20
2-Butanone ND ug/Kg 125.2 05/17/2016 14:20
2-Chlorotoluene ND ug/Kg 15.04 05/17/2016 14:20
2-Hexanone ND ug/Kg 112.6 05/17/2016 14:20
4-Chlorotoluene ND ug/Kg 15.04 05/17/2016 14:20
4-Isopropyltoluene ND ug/Kg 15.04 05/17/2016 14:20
4-Methyl-2-pentanone ND ug/Kg 112.6 05/17/2016 14:20
Acetone ND ug/Kg 150.4 05/17/2016 14:20
Benzene ND ug/Kg 15.04 05/17/2016 14:20
Bromobenzene ND ug/Kg 15.04 05/17/2016 14:20
Bromochloromethane ND ug/Kg 15.04 05/17/2016 14:20
Bromoform ND ug/Kg 15.04 05/17/2016 14:20
Bromomethane ND ug/Kg 15.04 05/17/2016 14:20
n-Butylbenzene ND ug/Kg 15.04 05/17/2016 14:20
Carbon disulfide ND ug/Kg 15.04 05/17/2016 14:20
Carbon tetrachloride ND ug/Kg 15.04 05/17/2016 14:20
Chlorobenzene ND ug/Kg 15.04 05/17/2016 14:20
Chlorodibromomethane ND ug/Kg 15.04 05/17/2016 14:20
Chloroethane ND ug/Kg 15.04 05/17/2016 14:20
Chloroform ND ug/Kg 15.04 05/17/2016 14:20
Chloromethane ND ug/Kg 15.04 05/17/2016 14:20
Dibromomethane ND ug/Kg 15.04 05/17/2016 14:20
Print Date: 05/23/2016 N.C. Certification # 481
Page 6 of 62
Client Sample ID: UST-1
Client Project ID: Dillon Station
Lab Sample ID: 31600936001-A
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:30
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 75.80
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-1
Date Analyzed
Dichlorobromomethane ND ug/Kg 15.04 05/17/2016 14:20
Dichlorodifluoromethane ND ug/Kg 15.04 05/17/2016 14:20
cis-1,3-Dichloropropene ND ug/Kg 15.04 05/17/2016 14:20
trans-1,3-Dichloropropene ND ug/Kg 15.04 05/17/2016 14:20
Diisopropyl Ether ND ug/Kg 15.04 05/17/2016 14:20
Ethyl Benzene ND ug/Kg 15.04 05/17/2016 14:20
Hexachlorobutadiene ND ug/Kg 15.04 05/17/2016 14:20
Isopropylbenzene (Cumene)ND ug/Kg 15.04 05/17/2016 14:20
Methyl iodide ND ug/Kg 15.04 05/17/2016 14:20
Methylene chloride ND ug/Kg 120.2 05/17/2016 14:20
Naphthalene ND ug/Kg 15.04 05/17/2016 14:20
Styrene ND ug/Kg 15.04 05/17/2016 14:20
Tetrachloroethene ND ug/Kg 15.04 05/17/2016 14:20
Toluene ND ug/Kg 15.04 05/17/2016 14:20
Trichloroethene ND ug/Kg 15.04 05/17/2016 14:20
Trichlorofluoromethane ND ug/Kg 15.04 05/17/2016 14:20
Vinyl chloride ND ug/Kg 15.04 05/17/2016 14:20
Xylene (total)ND ug/Kg 110.1 05/17/2016 14:20
cis-1,2-Dichloroethene ND ug/Kg 15.04 05/17/2016 14:20
m,p-Xylene ND ug/Kg 110.1 05/17/2016 14:20
n-Propylbenzene ND ug/Kg 15.04 05/17/2016 14:20
o-Xylene ND ug/Kg 15.04 05/17/2016 14:20
sec-Butylbenzene ND ug/Kg 15.04 05/17/2016 14:20
tert-Butyl methyl ether (MTBE)ND ug/Kg 15.04 05/17/2016 14:20
tert-Butylbenzene ND ug/Kg 15.04 05/17/2016 14:20
trans-1,2-Dichloroethene ND ug/Kg 15.04 05/17/2016 14:20
trans-1,4-Dichloro-2-butene ND ug/Kg 125.2 05/17/2016 14:20
Surrogates
1,2-Dichloroethane-d4 107 %155.0-173 05/17/2016 14:20
4-Bromofluorobenzene 111 %123.0-141 05/17/2016 14:20
Toluene d8 105 %157.0-134 05/17/2016 14:20
Batch Information
Prep Batch: VXX6487
Prep Method: SW-846 5035 SL
Prep Date/Time: 05/12/2016 12:12
Prep Initial Wt./Vol.: 6.55 g
Prep Extract Vol: 5 mL
Analytical Batch: VMS3992
Analytical Method: SW-846 8260B
Instrument: MSD4
Analyst: JHL
Print Date: 05/23/2016 N.C. Certification # 481
Page 7 of 62
Client Sample ID: UST-1
Client Project ID: Dillon Station
Lab Sample ID: 31600936001-G
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:30
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 75.80
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-1
Date Analyzed
1,2,4-Trichlorobenzene ND ug/Kg 1405 05/18/2016 15:25
1,2-Dichlorobenzene ND ug/Kg 1405 05/18/2016 15:25
1,3-Dichlorobenzene ND ug/Kg 1405 05/18/2016 15:25
1,4-Dichlorobenzene ND ug/Kg 1405 05/18/2016 15:25
2,4,5-Trichlorophenol ND ug/Kg 1405 05/18/2016 15:25
2,4,6-Trichlorophenol ND ug/Kg 1405 05/18/2016 15:25
2,4-Dichlorophenol ND ug/Kg 1405 05/18/2016 15:25
2,4-Dinitrophenol ND ug/Kg 12030 05/18/2016 15:25
2,4-Dinitrotoluene ND ug/Kg 1405 05/18/2016 15:25
2,6-Dinitrotoluene ND ug/Kg 1405 05/18/2016 15:25
2-Chloronaphthalene ND ug/Kg 1405 05/18/2016 15:25
2-Chlorophenol ND ug/Kg 1405 05/18/2016 15:25
2-Methylnaphthalene ND ug/Kg 1405 05/18/2016 15:25
2-Methylphenol ND ug/Kg 1405 05/18/2016 15:25
2-Nitroaniline ND ug/Kg 1405 05/18/2016 15:25
2-Nitrophenol ND ug/Kg 1405 05/18/2016 15:25
3 and/or 4-Methylphenol ND ug/Kg 1405 05/18/2016 15:25
3,3'-Dichlorobenzidine ND ug/Kg 1963 05/20/2016 22:20
3-Nitroaniline ND ug/Kg 12410 05/20/2016 22:20
4,6-Dinitro-2-methylphenol ND ug/Kg 12030 05/18/2016 15:25
4-Chloro-3-methylphenol ND ug/Kg 1405 05/18/2016 15:25
4-Chloroaniline ND ug/Kg 1405 05/18/2016 15:25
4-Chlorophenyl phenyl ether ND ug/Kg 1405 05/18/2016 15:25
Acenaphthene ND ug/Kg 1405 05/18/2016 15:25
Acenaphthylene ND ug/Kg 1405 05/18/2016 15:25
Anthracene ND ug/Kg 1405 05/18/2016 15:25
Benzo(a)anthracene ND ug/Kg 1405 05/18/2016 15:25
Benzo(a)pyrene ND ug/Kg 1405 05/18/2016 15:25
Benzo(b)fluoranthene ND ug/Kg 1405 05/18/2016 15:25
Benzo(g,h,i)perylene ND ug/Kg 1405 05/18/2016 15:25
Benzo(k)fluoranthene ND ug/Kg 1405 05/18/2016 15:25
Benzoic acid ND ug/Kg 12030 05/18/2016 15:25
Bis(2-Chloroethoxy)methane ND ug/Kg 1405 05/18/2016 15:25
Bis(2-Chloroethyl)ether ND ug/Kg 1405 05/18/2016 15:25
Bis(2-Chloroisopropyl)ether ND ug/Kg 1405 05/18/2016 15:25
Bis(2-Ethylhexyl)phthalate ND ug/Kg 1405 05/18/2016 15:25
4-Bromophenyl phenyl ether ND ug/Kg 1405 05/18/2016 15:25
Butyl benzyl phthalate ND ug/Kg 1405 05/18/2016 15:25
Chrysene ND ug/Kg 1405 05/18/2016 15:25
Di-n-butyl phthalate ND ug/Kg 1405 05/18/2016 15:25
Di-n-octyl phthalate ND ug/Kg 1405 05/18/2016 15:25
Dibenz(a,h)anthracene ND ug/Kg 1405 05/18/2016 15:25
Print Date: 05/23/2016 N.C. Certification # 481
Page 8 of 62
Client Sample ID: UST-1
Client Project ID: Dillon Station
Lab Sample ID: 31600936001-G
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:30
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 75.80
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-1
Date Analyzed
Dibenzofuran ND ug/Kg 1405 05/18/2016 15:25
Diethyl phthalate ND ug/Kg 1405 05/18/2016 15:25
Dimethyl phthalate ND ug/Kg 1405 05/18/2016 15:25
2,4-Dimethylphenol ND ug/Kg 1405 05/18/2016 15:25
Diphenylamine ND ug/Kg 1405 05/18/2016 15:25
Fluoranthene ND ug/Kg 1405 05/18/2016 15:25
Fluorene ND ug/Kg 1405 05/18/2016 15:25
Hexachlorobenzene ND ug/Kg 12030 05/18/2016 15:25
Hexachlorobutadiene ND ug/Kg 1405 05/18/2016 15:25
Hexachlorocyclopentadiene ND ug/Kg 1810 05/18/2016 15:25
Hexachloroethane ND ug/Kg 1405 05/18/2016 15:25
Indeno(1,2,3-cd)pyrene ND ug/Kg 1405 05/18/2016 15:25
Isophorone ND ug/Kg 1405 05/18/2016 15:25
Naphthalene ND ug/Kg 1405 05/18/2016 15:25
4-Nitroaniline ND ug/Kg 12030 05/18/2016 15:25
Nitrobenzene ND ug/Kg 1405 05/18/2016 15:25
4-Nitrophenol ND ug/Kg 12030 05/18/2016 15:25
Pentachlorophenol ND ug/Kg 12030 05/18/2016 15:25
Phenanthrene ND ug/Kg 1405 05/18/2016 15:25
Phenol ND ug/Kg 1405 05/18/2016 15:25
Pyrene ND ug/Kg 1405 05/18/2016 15:25
n-Nitrosodi-n-propylamine ND ug/Kg 1405 05/18/2016 15:25
Surrogates
2,4,6-Tribromophenol 99.0 %141.0-129 05/18/2016 15:25
2-Fluorobiphenyl 101 %148.0-123 05/18/2016 15:25
2-Fluorophenol 114 %142.0-123 05/18/2016 15:25
Nitrobenzene-d5 105 %146.0-117 05/18/2016 15:25
Phenol-d6 113 %148.0-125 05/18/2016 15:25
Terphenyl-d14 99.0 %144.0-140 05/18/2016 15:25
Print Date: 05/23/2016 N.C. Certification # 481
Page 9 of 62
Client Sample ID: UST-1
Client Project ID: Dillon Station
Lab Sample ID: 31600936001-G
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:30
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 75.80
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-1
Date Analyzed
Batch Information
Prep Batch: XXX5737
Prep Method: SW-846 3541
Prep Date/Time: 05/12/2016 15:06
Prep Initial Wt./Vol.: 32.64 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2629
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX5757
Prep Method: SW-846 3541
Prep Date/Time: 05/19/2016 16:04
Prep Initial Wt./Vol.: 27.45 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2632
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 05/23/2016 N.C. Certification # 481
Page 10 of 62
Client Sample ID: UST-2
Client Project ID: Dillon Station
Lab Sample ID: 31600936002-A
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:35
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 68.70
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-2
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/Kg 16.51 05/17/2016 14:48
1,1,1-Trichloroethane ND ug/Kg 16.51 05/17/2016 14:48
1,1,2,2-Tetrachloroethane ND ug/Kg 16.51 05/17/2016 14:48
1,1,2-Trichloroethane ND ug/Kg 16.51 05/17/2016 14:48
1,1-Dichloroethane ND ug/Kg 16.51 05/17/2016 14:48
1,1-Dichloroethene ND ug/Kg 16.51 05/17/2016 14:48
1,1-Dichloropropene ND ug/Kg 16.51 05/17/2016 14:48
1,2,3-Trichlorobenzene ND ug/Kg 16.51 05/17/2016 14:48
1,2,3-Trichloropropane ND ug/Kg 16.51 05/17/2016 14:48
1,2,4-Trichlorobenzene ND ug/Kg 16.51 05/17/2016 14:48
1,2,4-Trimethylbenzene ND ug/Kg 16.51 05/17/2016 14:48
1,2-Dibromo-3-chloropropane ND ug/Kg 139.1 05/17/2016 14:48
1,2-Dibromoethane ND ug/Kg 16.51 05/17/2016 14:48
1,2-Dichlorobenzene ND ug/Kg 16.51 05/17/2016 14:48
1,2-Dichloroethane ND ug/Kg 16.51 05/17/2016 14:48
1,2-Dichloropropane ND ug/Kg 16.51 05/17/2016 14:48
1,3,5-Trimethylbenzene ND ug/Kg 16.51 05/17/2016 14:48
1,3-Dichlorobenzene ND ug/Kg 16.51 05/17/2016 14:48
1,3-Dichloropropane ND ug/Kg 16.51 05/17/2016 14:48
1,4-Dichlorobenzene ND ug/Kg 16.51 05/17/2016 14:48
2,2-Dichloropropane ND ug/Kg 16.51 05/17/2016 14:48
2-Butanone ND ug/Kg 132.6 05/17/2016 14:48
2-Chlorotoluene ND ug/Kg 16.51 05/17/2016 14:48
2-Hexanone ND ug/Kg 116.3 05/17/2016 14:48
4-Chlorotoluene ND ug/Kg 16.51 05/17/2016 14:48
4-Isopropyltoluene ND ug/Kg 16.51 05/17/2016 14:48
4-Methyl-2-pentanone ND ug/Kg 116.3 05/17/2016 14:48
Acetone 71.3 ug/Kg 165.1 05/17/2016 14:48
Benzene ND ug/Kg 16.51 05/17/2016 14:48
Bromobenzene ND ug/Kg 16.51 05/17/2016 14:48
Bromochloromethane ND ug/Kg 16.51 05/17/2016 14:48
Bromoform ND ug/Kg 16.51 05/17/2016 14:48
Bromomethane ND ug/Kg 16.51 05/17/2016 14:48
n-Butylbenzene ND ug/Kg 16.51 05/17/2016 14:48
Carbon disulfide ND ug/Kg 16.51 05/17/2016 14:48
Carbon tetrachloride ND ug/Kg 16.51 05/17/2016 14:48
Chlorobenzene ND ug/Kg 16.51 05/17/2016 14:48
Chlorodibromomethane ND ug/Kg 16.51 05/17/2016 14:48
Chloroethane ND ug/Kg 16.51 05/17/2016 14:48
Chloroform ND ug/Kg 16.51 05/17/2016 14:48
Chloromethane ND ug/Kg 16.51 05/17/2016 14:48
Dibromomethane ND ug/Kg 16.51 05/17/2016 14:48
Print Date: 05/23/2016 N.C. Certification # 481
Page 11 of 62
Client Sample ID: UST-2
Client Project ID: Dillon Station
Lab Sample ID: 31600936002-A
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:35
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 68.70
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-2
Date Analyzed
Dichlorobromomethane ND ug/Kg 16.51 05/17/2016 14:48
Dichlorodifluoromethane ND ug/Kg 16.51 05/17/2016 14:48
cis-1,3-Dichloropropene ND ug/Kg 16.51 05/17/2016 14:48
trans-1,3-Dichloropropene ND ug/Kg 16.51 05/17/2016 14:48
Diisopropyl Ether ND ug/Kg 16.51 05/17/2016 14:48
Ethyl Benzene ND ug/Kg 16.51 05/17/2016 14:48
Hexachlorobutadiene ND ug/Kg 16.51 05/17/2016 14:48
Isopropylbenzene (Cumene)ND ug/Kg 16.51 05/17/2016 14:48
Methyl iodide ND ug/Kg 16.51 05/17/2016 14:48
Methylene chloride ND ug/Kg 126.0 05/17/2016 14:48
Naphthalene ND ug/Kg 16.51 05/17/2016 14:48
Styrene ND ug/Kg 16.51 05/17/2016 14:48
Tetrachloroethene ND ug/Kg 16.51 05/17/2016 14:48
Toluene ND ug/Kg 16.51 05/17/2016 14:48
Trichloroethene ND ug/Kg 16.51 05/17/2016 14:48
Trichlorofluoromethane ND ug/Kg 16.51 05/17/2016 14:48
Vinyl chloride ND ug/Kg 16.51 05/17/2016 14:48
Xylene (total)ND ug/Kg 113.0 05/17/2016 14:48
cis-1,2-Dichloroethene ND ug/Kg 16.51 05/17/2016 14:48
m,p-Xylene ND ug/Kg 113.0 05/17/2016 14:48
n-Propylbenzene ND ug/Kg 16.51 05/17/2016 14:48
o-Xylene ND ug/Kg 16.51 05/17/2016 14:48
sec-Butylbenzene ND ug/Kg 16.51 05/17/2016 14:48
tert-Butyl methyl ether (MTBE)ND ug/Kg 16.51 05/17/2016 14:48
tert-Butylbenzene ND ug/Kg 16.51 05/17/2016 14:48
trans-1,2-Dichloroethene ND ug/Kg 16.51 05/17/2016 14:48
trans-1,4-Dichloro-2-butene ND ug/Kg 132.6 05/17/2016 14:48
Surrogates
1,2-Dichloroethane-d4 106 %155.0-173 05/17/2016 14:48
4-Bromofluorobenzene 113 %123.0-141 05/17/2016 14:48
Toluene d8 103 %157.0-134 05/17/2016 14:48
Batch Information
Prep Batch: VXX6487
Prep Method: SW-846 5035 SL
Prep Date/Time: 05/12/2016 12:16
Prep Initial Wt./Vol.: 5.59 g
Prep Extract Vol: 5 mL
Analytical Batch: VMS3992
Analytical Method: SW-846 8260B
Instrument: MSD4
Analyst: JHL
Print Date: 05/23/2016 N.C. Certification # 481
Page 12 of 62
Client Sample ID: UST-2
Client Project ID: Dillon Station
Lab Sample ID: 31600936002-G
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:35
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 68.70
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-2
Date Analyzed
1,2,4-Trichlorobenzene ND ug/Kg 1444 05/18/2016 16:30
1,2-Dichlorobenzene ND ug/Kg 1444 05/18/2016 16:30
1,3-Dichlorobenzene ND ug/Kg 1444 05/18/2016 16:30
1,4-Dichlorobenzene ND ug/Kg 1444 05/18/2016 16:30
2,4,5-Trichlorophenol ND ug/Kg 1444 05/18/2016 16:30
2,4,6-Trichlorophenol ND ug/Kg 1444 05/18/2016 16:30
2,4-Dichlorophenol ND ug/Kg 1444 05/18/2016 16:30
2,4-Dinitrophenol ND ug/Kg 12220 05/18/2016 16:30
2,4-Dinitrotoluene ND ug/Kg 1444 05/18/2016 16:30
2,6-Dinitrotoluene ND ug/Kg 1444 05/18/2016 16:30
2-Chloronaphthalene ND ug/Kg 1444 05/18/2016 16:30
2-Chlorophenol ND ug/Kg 1444 05/18/2016 16:30
2-Methylnaphthalene ND ug/Kg 1444 05/18/2016 16:30
2-Methylphenol ND ug/Kg 1444 05/18/2016 16:30
2-Nitroaniline ND ug/Kg 1444 05/18/2016 16:30
2-Nitrophenol ND ug/Kg 1444 05/18/2016 16:30
3 and/or 4-Methylphenol ND ug/Kg 1444 05/18/2016 16:30
3,3'-Dichlorobenzidine ND ug/Kg 1899 05/20/2016 22:41
3-Nitroaniline ND ug/Kg 12250 05/20/2016 22:41
4,6-Dinitro-2-methylphenol ND ug/Kg 12220 05/18/2016 16:30
4-Chloro-3-methylphenol ND ug/Kg 1444 05/18/2016 16:30
4-Chloroaniline ND ug/Kg 1444 05/18/2016 16:30
4-Chlorophenyl phenyl ether ND ug/Kg 1444 05/18/2016 16:30
Acenaphthene ND ug/Kg 1444 05/18/2016 16:30
Acenaphthylene ND ug/Kg 1444 05/18/2016 16:30
Anthracene ND ug/Kg 1444 05/18/2016 16:30
Benzo(a)anthracene ND ug/Kg 1444 05/18/2016 16:30
Benzo(a)pyrene ND ug/Kg 1444 05/18/2016 16:30
Benzo(b)fluoranthene ND ug/Kg 1444 05/18/2016 16:30
Benzo(g,h,i)perylene ND ug/Kg 1444 05/18/2016 16:30
Benzo(k)fluoranthene ND ug/Kg 1444 05/18/2016 16:30
Benzoic acid ND ug/Kg 12220 05/18/2016 16:30
Bis(2-Chloroethoxy)methane ND ug/Kg 1444 05/18/2016 16:30
Bis(2-Chloroethyl)ether ND ug/Kg 1444 05/18/2016 16:30
Bis(2-Chloroisopropyl)ether ND ug/Kg 1444 05/18/2016 16:30
Bis(2-Ethylhexyl)phthalate ND ug/Kg 1444 05/18/2016 16:30
4-Bromophenyl phenyl ether ND ug/Kg 1444 05/18/2016 16:30
Butyl benzyl phthalate ND ug/Kg 1444 05/18/2016 16:30
Chrysene ND ug/Kg 1444 05/18/2016 16:30
Di-n-butyl phthalate ND ug/Kg 1444 05/18/2016 16:30
Di-n-octyl phthalate ND ug/Kg 1444 05/18/2016 16:30
Dibenz(a,h)anthracene ND ug/Kg 1444 05/18/2016 16:30
Print Date: 05/23/2016 N.C. Certification # 481
Page 13 of 62
Client Sample ID: UST-2
Client Project ID: Dillon Station
Lab Sample ID: 31600936002-G
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:35
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 68.70
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-2
Date Analyzed
Dibenzofuran ND ug/Kg 1444 05/18/2016 16:30
Diethyl phthalate ND ug/Kg 1444 05/18/2016 16:30
Dimethyl phthalate ND ug/Kg 1444 05/18/2016 16:30
2,4-Dimethylphenol ND ug/Kg 1444 05/18/2016 16:30
Diphenylamine ND ug/Kg 1444 05/18/2016 16:30
Fluoranthene ND ug/Kg 1444 05/18/2016 16:30
Fluorene ND ug/Kg 1444 05/18/2016 16:30
Hexachlorobenzene ND ug/Kg 12220 05/18/2016 16:30
Hexachlorobutadiene ND ug/Kg 1444 05/18/2016 16:30
Hexachlorocyclopentadiene ND ug/Kg 1889 05/18/2016 16:30
Hexachloroethane ND ug/Kg 1444 05/18/2016 16:30
Indeno(1,2,3-cd)pyrene ND ug/Kg 1444 05/18/2016 16:30
Isophorone ND ug/Kg 1444 05/18/2016 16:30
Naphthalene ND ug/Kg 1444 05/18/2016 16:30
4-Nitroaniline ND ug/Kg 12220 05/18/2016 16:30
Nitrobenzene ND ug/Kg 1444 05/18/2016 16:30
4-Nitrophenol ND ug/Kg 12220 05/18/2016 16:30
Pentachlorophenol ND ug/Kg 12220 05/18/2016 16:30
Phenanthrene ND ug/Kg 1444 05/18/2016 16:30
Phenol ND ug/Kg 1444 05/18/2016 16:30
Pyrene ND ug/Kg 1444 05/18/2016 16:30
n-Nitrosodi-n-propylamine ND ug/Kg 1444 05/18/2016 16:30
Surrogates
2,4,6-Tribromophenol 100 %141.0-129 05/18/2016 16:30
2-Fluorobiphenyl 94.0 %148.0-123 05/18/2016 16:30
2-Fluorophenol 103 %142.0-123 05/18/2016 16:30
Nitrobenzene-d5 98.0 %146.0-117 05/18/2016 16:30
Phenol-d6 108 %148.0-125 05/18/2016 16:30
Terphenyl-d14 96.0 %144.0-140 05/18/2016 16:30
Print Date: 05/23/2016 N.C. Certification # 481
Page 14 of 62
Client Sample ID: UST-2
Client Project ID: Dillon Station
Lab Sample ID: 31600936002-G
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:35
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 68.70
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-2
Date Analyzed
Batch Information
Prep Batch: XXX5737
Prep Method: SW-846 3541
Prep Date/Time: 05/12/2016 15:06
Prep Initial Wt./Vol.: 32.82 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2629
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX5757
Prep Method: SW-846 3541
Prep Date/Time: 05/19/2016 16:04
Prep Initial Wt./Vol.: 32.44 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2632
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 05/23/2016 N.C. Certification # 481
Page 15 of 62
Client Sample ID: UST-3
Client Project ID: Dillon Station
Lab Sample ID: 31600936003-B
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:40
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 65.50
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-3
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/Kg 15.85 05/17/2016 19:55
1,1,1-Trichloroethane ND ug/Kg 15.85 05/17/2016 19:55
1,1,2,2-Tetrachloroethane ND ug/Kg 15.85 05/17/2016 19:55
1,1,2-Trichloroethane ND ug/Kg 15.85 05/17/2016 19:55
1,1-Dichloroethane ND ug/Kg 15.85 05/17/2016 19:55
1,1-Dichloroethene ND ug/Kg 15.85 05/17/2016 19:55
1,1-Dichloropropene ND ug/Kg 15.85 05/17/2016 19:55
1,2,3-Trichlorobenzene ND ug/Kg 15.85 05/17/2016 19:55
1,2,3-Trichloropropane ND ug/Kg 15.85 05/17/2016 19:55
1,2,4-Trichlorobenzene ND ug/Kg 15.85 05/17/2016 19:55
1,2,4-Trimethylbenzene ND ug/Kg 15.85 05/17/2016 19:55
1,2-Dibromo-3-chloropropane ND ug/Kg 135.1 05/17/2016 19:55
1,2-Dibromoethane ND ug/Kg 15.85 05/17/2016 19:55
1,2-Dichlorobenzene ND ug/Kg 15.85 05/17/2016 19:55
1,2-Dichloroethane ND ug/Kg 15.85 05/17/2016 19:55
1,2-Dichloropropane ND ug/Kg 15.85 05/17/2016 19:55
1,3,5-Trimethylbenzene ND ug/Kg 15.85 05/17/2016 19:55
1,3-Dichlorobenzene ND ug/Kg 15.85 05/17/2016 19:55
1,3-Dichloropropane ND ug/Kg 15.85 05/17/2016 19:55
1,4-Dichlorobenzene ND ug/Kg 15.85 05/17/2016 19:55
2,2-Dichloropropane ND ug/Kg 15.85 05/17/2016 19:55
2-Butanone ND ug/Kg 129.2 05/17/2016 19:55
2-Chlorotoluene ND ug/Kg 15.85 05/17/2016 19:55
2-Hexanone ND ug/Kg 114.6 05/17/2016 19:55
4-Chlorotoluene ND ug/Kg 15.85 05/17/2016 19:55
4-Isopropyltoluene ND ug/Kg 15.85 05/17/2016 19:55
4-Methyl-2-pentanone ND ug/Kg 114.6 05/17/2016 19:55
Acetone 60.6 ug/Kg 158.5 05/17/2016 19:55
Benzene ND ug/Kg 15.85 05/17/2016 19:55
Bromobenzene ND ug/Kg 15.85 05/17/2016 19:55
Bromochloromethane ND ug/Kg 15.85 05/17/2016 19:55
Bromoform ND ug/Kg 15.85 05/17/2016 19:55
Bromomethane ND ug/Kg 15.85 05/17/2016 19:55
n-Butylbenzene ND ug/Kg 15.85 05/17/2016 19:55
Carbon disulfide ND ug/Kg 15.85 05/17/2016 19:55
Carbon tetrachloride ND ug/Kg 15.85 05/17/2016 19:55
Chlorobenzene ND ug/Kg 15.85 05/17/2016 19:55
Chlorodibromomethane ND ug/Kg 15.85 05/17/2016 19:55
Chloroethane ND ug/Kg 15.85 05/17/2016 19:55
Chloroform ND ug/Kg 15.85 05/17/2016 19:55
Chloromethane ND ug/Kg 15.85 05/17/2016 19:55
Dibromomethane ND ug/Kg 15.85 05/17/2016 19:55
Print Date: 05/23/2016 N.C. Certification # 481
Page 16 of 62
Client Sample ID: UST-3
Client Project ID: Dillon Station
Lab Sample ID: 31600936003-B
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:40
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 65.50
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-3
Date Analyzed
Dichlorobromomethane ND ug/Kg 15.85 05/17/2016 19:55
Dichlorodifluoromethane ND ug/Kg 15.85 05/17/2016 19:55
cis-1,3-Dichloropropene ND ug/Kg 15.85 05/17/2016 19:55
trans-1,3-Dichloropropene ND ug/Kg 15.85 05/17/2016 19:55
Diisopropyl Ether ND ug/Kg 15.85 05/17/2016 19:55
Ethyl Benzene ND ug/Kg 15.85 05/17/2016 19:55
Hexachlorobutadiene ND ug/Kg 15.85 05/17/2016 19:55
Isopropylbenzene (Cumene)ND ug/Kg 15.85 05/17/2016 19:55
Methyl iodide ND ug/Kg 15.85 05/17/2016 19:55
Methylene chloride ND ug/Kg 123.4 05/17/2016 19:55
Naphthalene ND ug/Kg 15.85 05/17/2016 19:55
Styrene ND ug/Kg 15.85 05/17/2016 19:55
Tetrachloroethene ND ug/Kg 15.85 05/17/2016 19:55
Toluene ND ug/Kg 15.85 05/17/2016 19:55
Trichloroethene ND ug/Kg 15.85 05/17/2016 19:55
Trichlorofluoromethane ND ug/Kg 15.85 05/17/2016 19:55
Vinyl chloride ND ug/Kg 15.85 05/17/2016 19:55
Xylene (total)ND ug/Kg 111.7 05/17/2016 19:55
cis-1,2-Dichloroethene ND ug/Kg 15.85 05/17/2016 19:55
m,p-Xylene ND ug/Kg 111.7 05/17/2016 19:55
n-Propylbenzene ND ug/Kg 15.85 05/17/2016 19:55
o-Xylene ND ug/Kg 15.85 05/17/2016 19:55
sec-Butylbenzene ND ug/Kg 15.85 05/17/2016 19:55
tert-Butyl methyl ether (MTBE)ND ug/Kg 15.85 05/17/2016 19:55
tert-Butylbenzene ND ug/Kg 15.85 05/17/2016 19:55
trans-1,2-Dichloroethene ND ug/Kg 15.85 05/17/2016 19:55
trans-1,4-Dichloro-2-butene ND ug/Kg 129.2 05/17/2016 19:55
Surrogates
1,2-Dichloroethane-d4 103 %155.0-173 05/17/2016 19:55
4-Bromofluorobenzene 160*%123.0-141 05/17/2016 19:55
Toluene d8 104 %157.0-134 05/17/2016 19:55
Batch Information
Prep Batch: VXX6487
Prep Method: SW-846 5035 SL
Prep Date/Time: 05/12/2016 12:18
Prep Initial Wt./Vol.: 6.53 g
Prep Extract Vol: 5 mL
Analytical Batch: VMS3992
Analytical Method: SW-846 8260B
Instrument: MSD4
Analyst: JHL
Print Date: 05/23/2016 N.C. Certification # 481
Page 17 of 62
Client Sample ID: UST-3
Client Project ID: Dillon Station
Lab Sample ID: 31600936003-G
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:40
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 65.50
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-3
Date Analyzed
1,2,4-Trichlorobenzene ND ug/Kg 1467 05/18/2016 16:51
1,2-Dichlorobenzene ND ug/Kg 1467 05/18/2016 16:51
1,3-Dichlorobenzene ND ug/Kg 1467 05/18/2016 16:51
1,4-Dichlorobenzene ND ug/Kg 1467 05/18/2016 16:51
2,4,5-Trichlorophenol ND ug/Kg 1467 05/18/2016 16:51
2,4,6-Trichlorophenol ND ug/Kg 1467 05/18/2016 16:51
2,4-Dichlorophenol ND ug/Kg 1467 05/18/2016 16:51
2,4-Dinitrophenol ND ug/Kg 12330 05/18/2016 16:51
2,4-Dinitrotoluene ND ug/Kg 1467 05/18/2016 16:51
2,6-Dinitrotoluene ND ug/Kg 1467 05/18/2016 16:51
2-Chloronaphthalene ND ug/Kg 1467 05/18/2016 16:51
2-Chlorophenol ND ug/Kg 1467 05/18/2016 16:51
2-Methylnaphthalene ND ug/Kg 1467 05/18/2016 16:51
2-Methylphenol ND ug/Kg 1467 05/18/2016 16:51
2-Nitroaniline ND ug/Kg 1467 05/18/2016 16:51
2-Nitrophenol ND ug/Kg 1467 05/18/2016 16:51
3 and/or 4-Methylphenol ND ug/Kg 1467 05/18/2016 16:51
3,3'-Dichlorobenzidine ND ug/Kg 1932 05/20/2016 23:47
3-Nitroaniline ND ug/Kg 12330 05/20/2016 23:47
4,6-Dinitro-2-methylphenol ND ug/Kg 12330 05/18/2016 16:51
4-Chloro-3-methylphenol ND ug/Kg 1467 05/18/2016 16:51
4-Chloroaniline ND ug/Kg 1467 05/18/2016 16:51
4-Chlorophenyl phenyl ether ND ug/Kg 1467 05/18/2016 16:51
Acenaphthene ND ug/Kg 1467 05/18/2016 16:51
Acenaphthylene ND ug/Kg 1467 05/18/2016 16:51
Anthracene ND ug/Kg 1467 05/18/2016 16:51
Benzo(a)anthracene ND ug/Kg 1467 05/18/2016 16:51
Benzo(a)pyrene ND ug/Kg 1467 05/18/2016 16:51
Benzo(b)fluoranthene ND ug/Kg 1467 05/18/2016 16:51
Benzo(g,h,i)perylene ND ug/Kg 1467 05/18/2016 16:51
Benzo(k)fluoranthene ND ug/Kg 1467 05/18/2016 16:51
Benzoic acid ND ug/Kg 12330 05/18/2016 16:51
Bis(2-Chloroethoxy)methane ND ug/Kg 1467 05/18/2016 16:51
Bis(2-Chloroethyl)ether ND ug/Kg 1467 05/18/2016 16:51
Bis(2-Chloroisopropyl)ether ND ug/Kg 1467 05/18/2016 16:51
Bis(2-Ethylhexyl)phthalate ND ug/Kg 1467 05/18/2016 16:51
4-Bromophenyl phenyl ether ND ug/Kg 1467 05/18/2016 16:51
Butyl benzyl phthalate ND ug/Kg 1467 05/18/2016 16:51
Chrysene ND ug/Kg 1467 05/18/2016 16:51
Di-n-butyl phthalate ND ug/Kg 1467 05/18/2016 16:51
Di-n-octyl phthalate ND ug/Kg 1467 05/18/2016 16:51
Dibenz(a,h)anthracene ND ug/Kg 1467 05/18/2016 16:51
Print Date: 05/23/2016 N.C. Certification # 481
Page 18 of 62
Client Sample ID: UST-3
Client Project ID: Dillon Station
Lab Sample ID: 31600936003-G
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:40
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 65.50
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-3
Date Analyzed
Dibenzofuran ND ug/Kg 1467 05/18/2016 16:51
Diethyl phthalate ND ug/Kg 1467 05/18/2016 16:51
Dimethyl phthalate ND ug/Kg 1467 05/18/2016 16:51
2,4-Dimethylphenol ND ug/Kg 1467 05/18/2016 16:51
Diphenylamine ND ug/Kg 1467 05/18/2016 16:51
Fluoranthene ND ug/Kg 1467 05/18/2016 16:51
Fluorene ND ug/Kg 1467 05/18/2016 16:51
Hexachlorobenzene ND ug/Kg 12330 05/18/2016 16:51
Hexachlorobutadiene ND ug/Kg 1467 05/18/2016 16:51
Hexachlorocyclopentadiene ND ug/Kg 1933 05/18/2016 16:51
Hexachloroethane ND ug/Kg 1467 05/18/2016 16:51
Indeno(1,2,3-cd)pyrene ND ug/Kg 1467 05/18/2016 16:51
Isophorone ND ug/Kg 1467 05/18/2016 16:51
Naphthalene ND ug/Kg 1467 05/18/2016 16:51
4-Nitroaniline ND ug/Kg 12330 05/18/2016 16:51
Nitrobenzene ND ug/Kg 1467 05/18/2016 16:51
4-Nitrophenol ND ug/Kg 12330 05/18/2016 16:51
Pentachlorophenol ND ug/Kg 12330 05/18/2016 16:51
Phenanthrene 3000 ug/Kg 1467 05/18/2016 16:51
Phenol ND ug/Kg 1467 05/18/2016 16:51
Pyrene ND ug/Kg 1467 05/18/2016 16:51
n-Nitrosodi-n-propylamine ND ug/Kg 1467 05/18/2016 16:51
Surrogates
2,4,6-Tribromophenol 127 %141.0-129 05/18/2016 16:51
2-Fluorobiphenyl 118 %148.0-123 05/18/2016 16:51
2-Fluorophenol 102 %142.0-123 05/18/2016 16:51
Nitrobenzene-d5 112 %146.0-117 05/18/2016 16:51
Phenol-d6 105 %148.0-125 05/18/2016 16:51
Terphenyl-d14 90.0 %144.0-140 05/18/2016 16:51
Print Date: 05/23/2016 N.C. Certification # 481
Page 19 of 62
Client Sample ID: UST-3
Client Project ID: Dillon Station
Lab Sample ID: 31600936003-G
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:40
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 65.50
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-3
Date Analyzed
Batch Information
Prep Batch: XXX5737
Prep Method: SW-846 3541
Prep Date/Time: 05/12/2016 15:06
Prep Initial Wt./Vol.: 32.79 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2629
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX5757
Prep Method: SW-846 3541
Prep Date/Time: 05/19/2016 16:04
Prep Initial Wt./Vol.: 32.83 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2632
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 05/23/2016 N.C. Certification # 481
Page 20 of 62
Client Sample ID: UST-4
Client Project ID: Dillon Station
Lab Sample ID: 31600936004-A
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:45
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 69.00
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-4
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/Kg 250290 05/19/2016 15:31
1,1,1-Trichloroethane ND ug/Kg 250290 05/19/2016 15:31
1,1,2,2-Tetrachloroethane ND ug/Kg 250290 05/19/2016 15:31
1,1,2-Trichloroethane ND ug/Kg 250290 05/19/2016 15:31
1,1-Dichloroethane ND ug/Kg 250290 05/19/2016 15:31
1,1-Dichloroethene ND ug/Kg 250290 05/19/2016 15:31
1,1-Dichloropropene ND ug/Kg 250290 05/19/2016 15:31
1,2,3-Trichlorobenzene ND ug/Kg 250290 05/19/2016 15:31
1,2,3-Trichloropropane ND ug/Kg 250290 05/19/2016 15:31
1,2,4-Trichlorobenzene ND ug/Kg 250290 05/19/2016 15:31
1,2,4-Trimethylbenzene ND ug/Kg 250290 05/19/2016 15:31
1,2-Dibromo-3-chloropropane ND ug/Kg 2501450 05/19/2016 15:31
1,2-Dibromoethane ND ug/Kg 250290 05/19/2016 15:31
1,2-Dichlorobenzene ND ug/Kg 250290 05/19/2016 15:31
1,2-Dichloroethane ND ug/Kg 250290 05/19/2016 15:31
1,2-Dichloropropane ND ug/Kg 250290 05/19/2016 15:31
1,3,5-Trimethylbenzene ND ug/Kg 250290 05/19/2016 15:31
1,3-Dichlorobenzene ND ug/Kg 250290 05/19/2016 15:31
1,3-Dichloropropane ND ug/Kg 250290 05/19/2016 15:31
1,4-Dichlorobenzene ND ug/Kg 250290 05/19/2016 15:31
2,2-Dichloropropane ND ug/Kg 250290 05/19/2016 15:31
2-Butanone ND ug/Kg 2507250 05/19/2016 15:31
2-Chlorotoluene ND ug/Kg 250290 05/19/2016 15:31
2-Hexanone ND ug/Kg 2501450 05/19/2016 15:31
4-Chlorotoluene ND ug/Kg 250290 05/19/2016 15:31
4-Isopropyltoluene ND ug/Kg 250290 05/19/2016 15:31
4-Methyl-2-pentanone ND ug/Kg 2501450 05/19/2016 15:31
Acetone ND ug/Kg 2507250 05/19/2016 15:31
Benzene ND ug/Kg 250290 05/19/2016 15:31
Bromobenzene ND ug/Kg 250290 05/19/2016 15:31
Bromochloromethane ND ug/Kg 250290 05/19/2016 15:31
Bromoform ND ug/Kg 250290 05/19/2016 15:31
Bromomethane ND ug/Kg 250290 05/19/2016 15:31
n-Butylbenzene 400 ug/Kg 250290 05/19/2016 15:31
Carbon disulfide ND ug/Kg 250290 05/19/2016 15:31
Carbon tetrachloride ND ug/Kg 250290 05/19/2016 15:31
Chlorobenzene ND ug/Kg 250290 05/19/2016 15:31
Chlorodibromomethane ND ug/Kg 250290 05/19/2016 15:31
Chloroethane ND ug/Kg 250290 05/19/2016 15:31
Chloroform ND ug/Kg 250290 05/19/2016 15:31
Chloromethane ND ug/Kg 250290 05/19/2016 15:31
Dibromomethane ND ug/Kg 250290 05/19/2016 15:31
Print Date: 05/23/2016 N.C. Certification # 481
Page 21 of 62
Client Sample ID: UST-4
Client Project ID: Dillon Station
Lab Sample ID: 31600936004-A
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:45
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 69.00
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-4
Date Analyzed
Dichlorobromomethane ND ug/Kg 250290 05/19/2016 15:31
Dichlorodifluoromethane ND ug/Kg 2501450 05/19/2016 15:31
cis-1,3-Dichloropropene ND ug/Kg 250290 05/19/2016 15:31
trans-1,3-Dichloropropene ND ug/Kg 250290 05/19/2016 15:31
Diisopropyl Ether ND ug/Kg 250290 05/19/2016 15:31
Ethyl Benzene ND ug/Kg 250290 05/19/2016 15:31
Hexachlorobutadiene ND ug/Kg 250290 05/19/2016 15:31
Isopropylbenzene (Cumene)ND ug/Kg 250290 05/19/2016 15:31
Methyl iodide ND ug/Kg 250290 05/19/2016 15:31
Methylene chloride ND ug/Kg 2501450 05/19/2016 15:31
Naphthalene 6050 ug/Kg 250290 05/19/2016 15:31
Styrene ND ug/Kg 250290 05/19/2016 15:31
Tetrachloroethene ND ug/Kg 250290 05/19/2016 15:31
Toluene ND ug/Kg 250290 05/19/2016 15:31
Trichloroethene ND ug/Kg 250290 05/19/2016 15:31
Trichlorofluoromethane ND ug/Kg 250290 05/19/2016 15:31
Vinyl chloride ND ug/Kg 250290 05/19/2016 15:31
Xylene (total)ND ug/Kg 250580 05/19/2016 15:31
cis-1,2-Dichloroethene ND ug/Kg 250290 05/19/2016 15:31
m,p-Xylene ND ug/Kg 250580 05/19/2016 15:31
n-Propylbenzene ND ug/Kg 250290 05/19/2016 15:31
o-Xylene ND ug/Kg 250290 05/19/2016 15:31
sec-Butylbenzene ND ug/Kg 250290 05/19/2016 15:31
tert-Butyl methyl ether (MTBE)ND ug/Kg 250290 05/19/2016 15:31
tert-Butylbenzene ND ug/Kg 250290 05/19/2016 15:31
trans-1,2-Dichloroethene ND ug/Kg 250290 05/19/2016 15:31
trans-1,4-Dichloro-2-butene ND ug/Kg 2501450 05/19/2016 15:31
Surrogates
1,2-Dichloroethane-d4 105 %25055.0-173 05/19/2016 15:31
4-Bromofluorobenzene 102 %25023.0-141 05/19/2016 15:31
Toluene d8 107 %25057.0-134 05/19/2016 15:31
Batch Information
Prep Batch: VXX6491
Prep Method: SW-846 5035 SM
Prep Date/Time: 05/19/2016 15:34
Prep Initial Wt./Vol.: 6.25 g
Prep Extract Vol: 5 mL
Analytical Batch: VMS3995
Analytical Method: SW-846 8260B
Instrument: MSD9
Analyst: JHL
Print Date: 05/23/2016 N.C. Certification # 481
Page 22 of 62
Client Sample ID: UST-4
Client Project ID: Dillon Station
Lab Sample ID: 31600936004-G
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:45
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 69.00
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-4
Date Analyzed
1,2,4-Trichlorobenzene ND ug/Kg 1452 05/21/2016 0:09
1,2-Dichlorobenzene ND ug/Kg 1452 05/21/2016 0:09
1,3-Dichlorobenzene ND ug/Kg 1452 05/21/2016 0:09
1,4-Dichlorobenzene ND ug/Kg 1452 05/21/2016 0:09
2,4,5-Trichlorophenol ND ug/Kg 1452 05/21/2016 0:09
2,4,6-Trichlorophenol ND ug/Kg 1452 05/21/2016 0:09
2,4-Dichlorophenol ND ug/Kg 1452 05/21/2016 0:09
2,4-Dinitrophenol ND ug/Kg 12260 05/21/2016 0:09
2,4-Dinitrotoluene ND ug/Kg 1452 05/21/2016 0:09
2,6-Dinitrotoluene ND ug/Kg 1452 05/21/2016 0:09
2-Chloronaphthalene ND ug/Kg 1452 05/21/2016 0:09
2-Chlorophenol ND ug/Kg 1452 05/21/2016 0:09
2-Methylnaphthalene ND ug/Kg 1452 05/21/2016 0:09
2-Methylphenol ND ug/Kg 1452 05/21/2016 0:09
2-Nitroaniline ND ug/Kg 1452 05/21/2016 0:09
2-Nitrophenol ND ug/Kg 1452 05/21/2016 0:09
3 and/or 4-Methylphenol ND ug/Kg 1452 05/21/2016 0:09
3,3'-Dichlorobenzidine ND ug/Kg 1903 05/21/2016 0:09
3-Nitroaniline ND ug/Kg 12260 05/21/2016 0:09
4,6-Dinitro-2-methylphenol ND ug/Kg 12260 05/21/2016 0:09
4-Chloro-3-methylphenol ND ug/Kg 1452 05/21/2016 0:09
4-Chloroaniline ND ug/Kg 1452 05/21/2016 0:09
4-Chlorophenyl phenyl ether ND ug/Kg 1452 05/21/2016 0:09
Acenaphthene ND ug/Kg 1452 05/21/2016 0:09
Acenaphthylene ND ug/Kg 1452 05/21/2016 0:09
Anthracene ND ug/Kg 1452 05/21/2016 0:09
Benzo(a)anthracene ND ug/Kg 1452 05/21/2016 0:09
Benzo(a)pyrene ND ug/Kg 1452 05/21/2016 0:09
Benzo(b)fluoranthene ND ug/Kg 1452 05/21/2016 0:09
Benzo(g,h,i)perylene ND ug/Kg 1452 05/21/2016 0:09
Benzo(k)fluoranthene ND ug/Kg 1452 05/21/2016 0:09
Benzoic acid ND ug/Kg 12260 05/21/2016 0:09
Bis(2-Chloroethoxy)methane ND ug/Kg 1452 05/21/2016 0:09
Bis(2-Chloroethyl)ether ND ug/Kg 1452 05/21/2016 0:09
Bis(2-Chloroisopropyl)ether ND ug/Kg 1452 05/21/2016 0:09
Bis(2-Ethylhexyl)phthalate ND ug/Kg 1452 05/21/2016 0:09
4-Bromophenyl phenyl ether ND ug/Kg 1452 05/21/2016 0:09
Butyl benzyl phthalate ND ug/Kg 1452 05/21/2016 0:09
Chrysene ND ug/Kg 1452 05/21/2016 0:09
Di-n-butyl phthalate ND ug/Kg 1452 05/21/2016 0:09
Di-n-octyl phthalate ND ug/Kg 1452 05/21/2016 0:09
Dibenz(a,h)anthracene ND ug/Kg 1452 05/21/2016 0:09
Print Date: 05/23/2016 N.C. Certification # 481
Page 23 of 62
Client Sample ID: UST-4
Client Project ID: Dillon Station
Lab Sample ID: 31600936004-G
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:45
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 69.00
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-4
Date Analyzed
Dibenzofuran ND ug/Kg 1452 05/21/2016 0:09
Diethyl phthalate ND ug/Kg 1452 05/21/2016 0:09
Dimethyl phthalate ND ug/Kg 1452 05/21/2016 0:09
2,4-Dimethylphenol ND ug/Kg 1452 05/21/2016 0:09
Diphenylamine ND ug/Kg 1452 05/21/2016 0:09
Fluoranthene ND ug/Kg 1452 05/21/2016 0:09
Fluorene ND ug/Kg 1452 05/21/2016 0:09
Hexachlorobenzene ND ug/Kg 12260 05/21/2016 0:09
Hexachlorobutadiene ND ug/Kg 1452 05/21/2016 0:09
Hexachlorocyclopentadiene ND ug/Kg 1903 05/21/2016 0:09
Hexachloroethane ND ug/Kg 1452 05/21/2016 0:09
Indeno(1,2,3-cd)pyrene ND ug/Kg 1452 05/21/2016 0:09
Isophorone ND ug/Kg 1452 05/21/2016 0:09
Naphthalene ND ug/Kg 1452 05/21/2016 0:09
4-Nitroaniline ND ug/Kg 12260 05/21/2016 0:09
Nitrobenzene ND ug/Kg 1452 05/21/2016 0:09
4-Nitrophenol ND ug/Kg 12260 05/21/2016 0:09
Pentachlorophenol ND ug/Kg 12260 05/21/2016 0:09
Phenanthrene ND ug/Kg 1452 05/21/2016 0:09
Phenol ND ug/Kg 1452 05/21/2016 0:09
Pyrene ND ug/Kg 1452 05/21/2016 0:09
n-Nitrosodi-n-propylamine ND ug/Kg 1452 05/21/2016 0:09
Surrogates
2,4,6-Tribromophenol 82.0 %141.0-129 05/21/2016 0:09
2-Fluorobiphenyl 85.0 %148.0-123 05/21/2016 0:09
2-Fluorophenol 98.0 %142.0-123 05/21/2016 0:09
Nitrobenzene-d5 90.0 %146.0-117 05/21/2016 0:09
Phenol-d6 101 %148.0-125 05/21/2016 0:09
Terphenyl-d14 84.0 %144.0-140 05/21/2016 0:09
Batch Information
Prep Batch: XXX5757
Prep Method: SW-846 3541
Prep Date/Time: 05/19/2016 16:04
Prep Initial Wt./Vol.: 32.15 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2632
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 05/23/2016 N.C. Certification # 481
Page 24 of 62
Client Sample ID: UST-5
Client Project ID: Dillon Station
Lab Sample ID: 31600936005-A
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:50
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 72.80
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-5
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/Kg 5067.9 05/19/2016 15:57
1,1,1-Trichloroethane ND ug/Kg 5067.9 05/19/2016 15:57
1,1,2,2-Tetrachloroethane ND ug/Kg 5067.9 05/19/2016 15:57
1,1,2-Trichloroethane ND ug/Kg 5067.9 05/19/2016 15:57
1,1-Dichloroethane ND ug/Kg 5067.9 05/19/2016 15:57
1,1-Dichloroethene ND ug/Kg 5067.9 05/19/2016 15:57
1,1-Dichloropropene ND ug/Kg 5067.9 05/19/2016 15:57
1,2,3-Trichlorobenzene ND ug/Kg 5067.9 05/19/2016 15:57
1,2,3-Trichloropropane ND ug/Kg 5067.9 05/19/2016 15:57
1,2,4-Trichlorobenzene ND ug/Kg 5067.9 05/19/2016 15:57
1,2,4-Trimethylbenzene ND ug/Kg 5067.9 05/19/2016 15:57
1,2-Dibromo-3-chloropropane ND ug/Kg 50339 05/19/2016 15:57
1,2-Dibromoethane ND ug/Kg 5067.9 05/19/2016 15:57
1,2-Dichlorobenzene ND ug/Kg 5067.9 05/19/2016 15:57
1,2-Dichloroethane ND ug/Kg 5067.9 05/19/2016 15:57
1,2-Dichloropropane ND ug/Kg 5067.9 05/19/2016 15:57
1,3,5-Trimethylbenzene ND ug/Kg 5067.9 05/19/2016 15:57
1,3-Dichlorobenzene ND ug/Kg 5067.9 05/19/2016 15:57
1,3-Dichloropropane ND ug/Kg 5067.9 05/19/2016 15:57
1,4-Dichlorobenzene ND ug/Kg 5067.9 05/19/2016 15:57
2,2-Dichloropropane ND ug/Kg 5067.9 05/19/2016 15:57
2-Butanone ND ug/Kg 501700 05/19/2016 15:57
2-Chlorotoluene ND ug/Kg 5067.9 05/19/2016 15:57
2-Hexanone ND ug/Kg 50339 05/19/2016 15:57
4-Chlorotoluene ND ug/Kg 5067.9 05/19/2016 15:57
4-Isopropyltoluene ND ug/Kg 5067.9 05/19/2016 15:57
4-Methyl-2-pentanone ND ug/Kg 50339 05/19/2016 15:57
Acetone ND ug/Kg 501700 05/19/2016 15:57
Benzene ND ug/Kg 5067.9 05/19/2016 15:57
Bromobenzene ND ug/Kg 5067.9 05/19/2016 15:57
Bromochloromethane ND ug/Kg 5067.9 05/19/2016 15:57
Bromoform ND ug/Kg 5067.9 05/19/2016 15:57
Bromomethane ND ug/Kg 5067.9 05/19/2016 15:57
n-Butylbenzene ND ug/Kg 5067.9 05/19/2016 15:57
Carbon disulfide ND ug/Kg 5067.9 05/19/2016 15:57
Carbon tetrachloride ND ug/Kg 5067.9 05/19/2016 15:57
Chlorobenzene ND ug/Kg 5067.9 05/19/2016 15:57
Chlorodibromomethane 208 ug/Kg 5067.9 05/19/2016 15:57
Chloroethane ND ug/Kg 5067.9 05/19/2016 15:57
Chloroform ND ug/Kg 5067.9 05/19/2016 15:57
Chloromethane ND ug/Kg 5067.9 05/19/2016 15:57
Dibromomethane ND ug/Kg 5067.9 05/19/2016 15:57
Print Date: 05/23/2016 N.C. Certification # 481
Page 25 of 62
Client Sample ID: UST-5
Client Project ID: Dillon Station
Lab Sample ID: 31600936005-A
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:50
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 72.80
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-5
Date Analyzed
Dichlorobromomethane ND ug/Kg 5067.9 05/19/2016 15:57
Dichlorodifluoromethane ND ug/Kg 50339 05/19/2016 15:57
cis-1,3-Dichloropropene ND ug/Kg 5067.9 05/19/2016 15:57
trans-1,3-Dichloropropene ND ug/Kg 5067.9 05/19/2016 15:57
Diisopropyl Ether ND ug/Kg 5067.9 05/19/2016 15:57
Ethyl Benzene ND ug/Kg 5067.9 05/19/2016 15:57
Hexachlorobutadiene ND ug/Kg 5067.9 05/19/2016 15:57
Isopropylbenzene (Cumene)ND ug/Kg 5067.9 05/19/2016 15:57
Methyl iodide ND ug/Kg 5067.9 05/19/2016 15:57
Methylene chloride ND ug/Kg 50339 05/19/2016 15:57
Naphthalene ND ug/Kg 5067.9 05/19/2016 15:57
Styrene ND ug/Kg 5067.9 05/19/2016 15:57
Tetrachloroethene ND ug/Kg 5067.9 05/19/2016 15:57
Toluene ND ug/Kg 5067.9 05/19/2016 15:57
Trichloroethene ND ug/Kg 5067.9 05/19/2016 15:57
Trichlorofluoromethane ND ug/Kg 5067.9 05/19/2016 15:57
Vinyl chloride ND ug/Kg 5067.9 05/19/2016 15:57
Xylene (total)ND ug/Kg 50136 05/19/2016 15:57
cis-1,2-Dichloroethene ND ug/Kg 5067.9 05/19/2016 15:57
m,p-Xylene ND ug/Kg 50136 05/19/2016 15:57
n-Propylbenzene ND ug/Kg 5067.9 05/19/2016 15:57
o-Xylene ND ug/Kg 5067.9 05/19/2016 15:57
sec-Butylbenzene ND ug/Kg 5067.9 05/19/2016 15:57
tert-Butyl methyl ether (MTBE)ND ug/Kg 5067.9 05/19/2016 15:57
tert-Butylbenzene ND ug/Kg 5067.9 05/19/2016 15:57
trans-1,2-Dichloroethene ND ug/Kg 5067.9 05/19/2016 15:57
trans-1,4-Dichloro-2-butene ND ug/Kg 50339 05/19/2016 15:57
Surrogates
1,2-Dichloroethane-d4 102 %5055.0-173 05/19/2016 15:57
4-Bromofluorobenzene 103 %5023.0-141 05/19/2016 15:57
Toluene d8 110 %5057.0-134 05/19/2016 15:57
Batch Information
Prep Batch: VXX6491
Prep Method: SW-846 5035 SM
Prep Date/Time: 05/19/2016 15:34
Prep Initial Wt./Vol.: 5.06 g
Prep Extract Vol: 5 mL
Analytical Batch: VMS3995
Analytical Method: SW-846 8260B
Instrument: MSD9
Analyst: JHL
Print Date: 05/23/2016 N.C. Certification # 481
Page 26 of 62
Client Sample ID: UST-5
Client Project ID: Dillon Station
Lab Sample ID: 31600936005-G
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:50
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 72.80
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-5
Date Analyzed
1,2,4-Trichlorobenzene ND ug/Kg 1424 05/18/2016 17:35
1,2-Dichlorobenzene ND ug/Kg 1424 05/18/2016 17:35
1,3-Dichlorobenzene ND ug/Kg 1424 05/18/2016 17:35
1,4-Dichlorobenzene ND ug/Kg 1424 05/18/2016 17:35
2,4,5-Trichlorophenol ND ug/Kg 1424 05/18/2016 17:35
2,4,6-Trichlorophenol ND ug/Kg 1424 05/18/2016 17:35
2,4-Dichlorophenol ND ug/Kg 1424 05/18/2016 17:35
2,4-Dinitrophenol ND ug/Kg 12120 05/18/2016 17:35
2,4-Dinitrotoluene ND ug/Kg 1424 05/18/2016 17:35
2,6-Dinitrotoluene ND ug/Kg 1424 05/18/2016 17:35
2-Chloronaphthalene ND ug/Kg 1424 05/18/2016 17:35
2-Chlorophenol ND ug/Kg 1424 05/18/2016 17:35
2-Methylnaphthalene ND ug/Kg 1424 05/18/2016 17:35
2-Methylphenol ND ug/Kg 1424 05/18/2016 17:35
2-Nitroaniline ND ug/Kg 1424 05/18/2016 17:35
2-Nitrophenol ND ug/Kg 1424 05/18/2016 17:35
3 and/or 4-Methylphenol ND ug/Kg 1424 05/18/2016 17:35
3,3'-Dichlorobenzidine ND ug/Kg 1845 05/21/2016 0:53
3-Nitroaniline ND ug/Kg 12110 05/21/2016 0:53
4,6-Dinitro-2-methylphenol ND ug/Kg 12120 05/18/2016 17:35
4-Chloro-3-methylphenol ND ug/Kg 1424 05/18/2016 17:35
4-Chloroaniline ND ug/Kg 1424 05/18/2016 17:35
4-Chlorophenyl phenyl ether ND ug/Kg 1424 05/18/2016 17:35
Acenaphthene ND ug/Kg 1424 05/18/2016 17:35
Acenaphthylene ND ug/Kg 1424 05/18/2016 17:35
Anthracene ND ug/Kg 1424 05/18/2016 17:35
Benzo(a)anthracene ND ug/Kg 1424 05/18/2016 17:35
Benzo(a)pyrene ND ug/Kg 1424 05/18/2016 17:35
Benzo(b)fluoranthene ND ug/Kg 1424 05/18/2016 17:35
Benzo(g,h,i)perylene ND ug/Kg 1424 05/18/2016 17:35
Benzo(k)fluoranthene ND ug/Kg 1424 05/18/2016 17:35
Benzoic acid ND ug/Kg 12120 05/18/2016 17:35
Bis(2-Chloroethoxy)methane ND ug/Kg 1424 05/18/2016 17:35
Bis(2-Chloroethyl)ether ND ug/Kg 1424 05/18/2016 17:35
Bis(2-Chloroisopropyl)ether ND ug/Kg 1424 05/18/2016 17:35
Bis(2-Ethylhexyl)phthalate ND ug/Kg 1424 05/18/2016 17:35
4-Bromophenyl phenyl ether ND ug/Kg 1424 05/18/2016 17:35
Butyl benzyl phthalate ND ug/Kg 1424 05/18/2016 17:35
Chrysene ND ug/Kg 1424 05/18/2016 17:35
Di-n-butyl phthalate ND ug/Kg 1424 05/18/2016 17:35
Di-n-octyl phthalate ND ug/Kg 1424 05/18/2016 17:35
Dibenz(a,h)anthracene ND ug/Kg 1424 05/18/2016 17:35
Print Date: 05/23/2016 N.C. Certification # 481
Page 27 of 62
Client Sample ID: UST-5
Client Project ID: Dillon Station
Lab Sample ID: 31600936005-G
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:50
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 72.80
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-5
Date Analyzed
Dibenzofuran ND ug/Kg 1424 05/18/2016 17:35
Diethyl phthalate ND ug/Kg 1424 05/18/2016 17:35
Dimethyl phthalate ND ug/Kg 1424 05/18/2016 17:35
2,4-Dimethylphenol ND ug/Kg 1424 05/18/2016 17:35
Diphenylamine ND ug/Kg 1424 05/18/2016 17:35
Fluoranthene ND ug/Kg 1424 05/18/2016 17:35
Fluorene ND ug/Kg 1424 05/18/2016 17:35
Hexachlorobenzene ND ug/Kg 12120 05/18/2016 17:35
Hexachlorobutadiene ND ug/Kg 1424 05/18/2016 17:35
Hexachlorocyclopentadiene ND ug/Kg 1848 05/18/2016 17:35
Hexachloroethane ND ug/Kg 1424 05/18/2016 17:35
Indeno(1,2,3-cd)pyrene ND ug/Kg 1424 05/18/2016 17:35
Isophorone ND ug/Kg 1424 05/18/2016 17:35
Naphthalene ND ug/Kg 1424 05/18/2016 17:35
4-Nitroaniline ND ug/Kg 12120 05/18/2016 17:35
Nitrobenzene ND ug/Kg 1424 05/18/2016 17:35
4-Nitrophenol ND ug/Kg 12120 05/18/2016 17:35
Pentachlorophenol ND ug/Kg 12120 05/18/2016 17:35
Phenanthrene ND ug/Kg 1424 05/18/2016 17:35
Phenol ND ug/Kg 1424 05/18/2016 17:35
Pyrene ND ug/Kg 1424 05/18/2016 17:35
n-Nitrosodi-n-propylamine ND ug/Kg 1424 05/18/2016 17:35
Surrogates
2,4,6-Tribromophenol 104 %141.0-129 05/18/2016 17:35
2-Fluorobiphenyl 100 %148.0-123 05/18/2016 17:35
2-Fluorophenol 110 %142.0-123 05/18/2016 17:35
Nitrobenzene-d5 101 %146.0-117 05/18/2016 17:35
Phenol-d6 109 %148.0-125 05/18/2016 17:35
Terphenyl-d14 99.0 %144.0-140 05/18/2016 17:35
Print Date: 05/23/2016 N.C. Certification # 481
Page 28 of 62
Client Sample ID: UST-5
Client Project ID: Dillon Station
Lab Sample ID: 31600936005-G
Lab Project ID: 31600936
Collection Date: 05/10/2016 16:50
Received Date: 05/12/2016 09:52
Matrix: Soil-Solid as dry weight
Solids (%): 72.80
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-5
Date Analyzed
Batch Information
Prep Batch: XXX5737
Prep Method: SW-846 3541
Prep Date/Time: 05/12/2016 15:06
Prep Initial Wt./Vol.: 32.44 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2629
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX5757
Prep Method: SW-846 3541
Prep Date/Time: 05/19/2016 16:04
Prep Initial Wt./Vol.: 32.56 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2632
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 05/23/2016 N.C. Certification # 481
Page 29 of 62
Batch Summary
SW-846 8260B SW-846 5035 SLAnalytical Method:Prep Method:
VXX6487
05/17/2016 15:54
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
LCS-S for HBN 115267 [VXX/6487 05/17/2016 12:07 MSD4 JHL200832VMS3992
LCSD-S for HBN 115267 [VXX/648 05/17/2016 12:35 MSD4 JHL200833VMS3992
MB-S for HBN 115267 [VXX/6487]05/17/2016 13:52 MSD4 JHL200834VMS3992
Floor (4-5ft)(200477DUP)05/17/2016 18:59 MSD4 JHL200835VMS3992
West Wall (0-5ft)(200476MS)05/17/2016 19:27 MSD4 JHL200836VMS3992
UST-1 05/17/2016 14:20 MSD4 JHL31600936001VMS3992
UST-2 05/17/2016 14:48 MSD4 JHL31600936002VMS3992
UST-3 05/17/2016 19:55 MSD4 JHL31600936003VMS3992
Print Date: 05/23/2016 N.C. Certification # 481
Page 30 of 62
Blank ID: MB-S for HBN 115267 [VXX/6487]
Blank Lab ID: 200834
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31600936001, 31600936002, 31600936003
Dichlorodifluoromethane ND 5.00 ug/Kg 1
Chloromethane ND 5.00 ug/Kg 1
Vinyl chloride ND 5.00 ug/Kg 1
Bromomethane ND 5.00 ug/Kg 1
Chloroethane ND 5.00 ug/Kg 1
Trichlorofluoromethane ND 5.00 ug/Kg 1
1,1-Dichloroethene ND 5.00 ug/Kg 1
Acetone ND 50.0 ug/Kg 1
Methylene chloride ND 20.0 ug/Kg 1
trans-1,2-Dichloroethene ND 5.00 ug/Kg 1
tert-Butyl methyl ether (MTBE)ND 5.00 ug/Kg 1
1,1-Dichloroethane ND 5.00 ug/Kg 1
Diisopropyl Ether ND 5.00 ug/Kg 1
2,2-Dichloropropane ND 5.00 ug/Kg 1
cis-1,2-Dichloroethene ND 5.00 ug/Kg 1
2-Butanone ND 25.0 ug/Kg 1
Bromochloromethane ND 5.00 ug/Kg 1
Chloroform ND 5.00 ug/Kg 1
1,1,1-Trichloroethane ND 5.00 ug/Kg 1
Carbon tetrachloride ND 5.00 ug/Kg 1
1,1-Dichloropropene ND 5.00 ug/Kg 1
Benzene ND 5.00 ug/Kg 1
1,2-Dichloroethane ND 5.00 ug/Kg 1
Trichloroethene ND 5.00 ug/Kg 1
1,2-Dichloropropane ND 5.00 ug/Kg 1
Dibromomethane ND 5.00 ug/Kg 1
Dichlorobromomethane ND 5.00 ug/Kg 1
cis-1,3-Dichloropropene ND 5.00 ug/Kg 1
4-Methyl-2-pentanone ND 12.5 ug/Kg 1
Toluene ND 5.00 ug/Kg 1
Methyl iodide ND 5.00 ug/Kg 1
trans-1,3-Dichloropropene ND 5.00 ug/Kg 1
Carbon disulfide ND 5.00 ug/Kg 1
1,1,2-Trichloroethane ND 5.00 ug/Kg 1
Tetrachloroethene ND 5.00 ug/Kg 1
1,3-Dichloropropane ND 5.00 ug/Kg 1
2-Hexanone ND 12.5 ug/Kg 1
Chlorodibromomethane ND 5.00 ug/Kg 1
1,2-Dibromoethane ND 5.00 ug/Kg 1
Chlorobenzene ND 5.00 ug/Kg 1
1,1,1,2-Tetrachloroethane ND 5.00 ug/Kg 1
Print Date: 05/23/2016 N.C. Certification # 481
Page 31 of 62
Blank ID: MB-S for HBN 115267 [VXX/6487]
Blank Lab ID: 200834
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31600936001, 31600936002, 31600936003
Bromoform ND 5.00 ug/Kg 1
Bromobenzene ND 5.00 ug/Kg 1
1,1,2,2-Tetrachloroethane ND 5.00 ug/Kg 1
1,2,3-Trichloropropane ND 5.00 ug/Kg 1
Ethyl Benzene ND 5.00 ug/Kg 1
m,p-Xylene ND 10.0 ug/Kg 1
Styrene ND 5.00 ug/Kg 1
o-Xylene ND 5.00 ug/Kg 1
Xylene (total)ND 10.0 ug/Kg 1
Isopropylbenzene (Cumene)ND 5.00 ug/Kg 1
n-Propylbenzene ND 5.00 ug/Kg 1
2-Chlorotoluene ND 5.00 ug/Kg 1
4-Chlorotoluene ND 5.00 ug/Kg 1
1,3,5-Trimethylbenzene ND 5.00 ug/Kg 1
tert-Butylbenzene ND 5.00 ug/Kg 1
1,2,4-Trimethylbenzene ND 5.00 ug/Kg 1
sec-Butylbenzene ND 5.00 ug/Kg 1
1,3-Dichlorobenzene ND 5.00 ug/Kg 1
4-Isopropyltoluene ND 5.00 ug/Kg 1
1,4-Dichlorobenzene ND 5.00 ug/Kg 1
1,2-Dichlorobenzene ND 5.00 ug/Kg 1
n-Butylbenzene ND 5.00 ug/Kg 1
1,2-Dibromo-3-chloropropane ND 30.0 ug/Kg 1
1,2,4-Trichlorobenzene ND 5.00 ug/Kg 1
Hexachlorobutadiene ND 5.00 ug/Kg 1
Naphthalene ND 5.00 ug/Kg 1
trans-1,4-Dichloro-2-butene ND 25.0 ug/Kg 1
1,2,3-Trichlorobenzene ND 5.00 ug/Kg 1
Surrogates
1,2-Dichloroethane-d4 103 55.0-173 %1
Toluene d8 103 57.0-134 %1
4-Bromofluorobenzene 108 23.0-141 %1
Batch Information
Prep Batch: VXX6487
Prep Method: SW-846 5035 SL
Prep Date/Time: 5/17/2016 3:55:17PM
Prep Initial Wt./Vol.: 5 g
Prep Extract Vol: 5 mL
Analytical Batch: VMS3992
Analytical Method: SW-846 8260B
Instrument: MSD4
Analyst: JHL
Print Date: 05/23/2016 N.C. Certification # 481
Page 32 of 62
Blank Spike ID: LCS-S for HBN 115267 [VXX/6487
Blank Spike Lab ID: 200832
Date Analyzed: 05/17/2016 12:07
Spike Duplicate ID: LCSD-S for HBN 115267 [VXX/648
Spike Duplicate Lab ID: 200833
Date Analyzed: 05/17/2016 12:35
Results by SW-846 8260B
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/Kg)
RPD CL
Spike Duplicate (ug/Kg)
31600936001, 31600936002, 31600936003QC for Samples:
Dichlorodifluoromethane 30.0 27.1 1.59030.0 26.7 89 21.3-143 30.00
Chloromethane 30.0 28.5 0.709530.0 28.3 94 53.5-124 30.00
Vinyl chloride 30.0 30.8 0.3310330.0 30.7 102 62.4-123 30.00
Bromomethane 30.0 32.5 0.9310830.0 32.2 107 43.9-141 30.00
Chloroethane 30.0 31.4 0.6410530.0 31.2 104 59.7-133 30.00
Trichlorofluoromethane 30.0 32.2 2.810730.0 31.3 104 58.1-131 30.00
1,1-Dichloroethene 30.0 32.2 0.9310730.0 32.5 108 69.1-121 30.00
Acetone 75.0 81.2 1010875.0 89.9 120 38.3-190 30.00
Methylene chloride 30.0 31.3 1.610430.0 31.8 106 73.0-121 30.00
trans-1,2-Dichloroethene 30.0 32.6 0.9210930.0 32.9 110 72.0-121 30.00
tert-Butyl methyl ether (MTBE)30.0 32.3 2.110830.0 33.0 110 74.4-127 30.00
1,1-Dichloroethane 30.0 32.5 0.9210830.0 32.8 109 72.0-126 30.00
Diisopropyl Ether 30.0 32.5 1.810830.0 33.1 110 73.0-126 30.00
2,2-Dichloropropane 30.0 37.8 0.26126*30.0 37.7 126*73.7-124 30.00
cis-1,2-Dichloroethene 30.0 34.3 1.211430.0 34.7 116 73.9-124 30.00
2-Butanone 75.0 84.4 8.611375.0 92.0 123 57.7-161 30.00
Bromochloromethane 30.0 33.8 1.511330.0 34.3 114 78.9-126 30.00
Chloroform 30.0 34.5 0.8711530.0 34.8 116 75.8-124 30.00
1,1,1-Trichloroethane 30.0 34.8 0.5711630.0 35.0 117 73.4-123 30.00
Carbon tetrachloride 30.0 35.9 0.2812030.0 36.0 120 72.2-123 30.00
1,1-Dichloropropene 30.0 34.2 1.511430.0 34.7 116 70.8-125 30.00
Benzene 30.0 34.1 1.511430.0 34.6 115 76.1-122 30.00
1,2-Dichloroethane 30.0 33.5 2.411230.0 34.3 114 79.7-123 30.00
Trichloroethene 30.0 33.5 1.511230.0 34.0 113 73.0-124 30.00
1,2-Dichloropropane 30.0 34.2 1.711430.0 34.8 116 78.1-122 30.00
Dibromomethane 30.0 33.9 2.911330.0 34.9 116 77.1-129 30.00
Dichlorobromomethane 30.0 35.5 0.8411830.0 35.8 119 77.7-123 30.00
cis-1,3-Dichloropropene 30.0 36.8 2.412330.0 37.7 126 78.9-126 30.00
4-Methyl-2-pentanone 75.0 84.3 6.211275.0 89.7 120 68.1-145 30.00
Toluene 30.0 34.6 0.8611530.0 34.9 116 74.6-125 30.00
Methyl iodide 30.0 33.5 0.9011230.0 33.2 111 63.8-133 30.00
trans-1,3-Dichloropropene 30.0 36.8 2.412330.0 37.7 126 80.0-127 30.00
Print Date: 05/23/2016 N.C. Certification # 481
Page 33 of 62
Blank Spike ID: LCS-S for HBN 115267 [VXX/6487
Blank Spike Lab ID: 200832
Date Analyzed: 05/17/2016 12:07
Spike Duplicate ID: LCSD-S for HBN 115267 [VXX/648
Spike Duplicate Lab ID: 200833
Date Analyzed: 05/17/2016 12:35
Results by SW-846 8260B
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/Kg)
RPD CL
Spike Duplicate (ug/Kg)
31600936001, 31600936002, 31600936003QC for Samples:
Carbon disulfide 30.0 32.4 0.3110830.0 32.5 108 61.5-131 30.00
1,1,2-Trichloroethane 30.0 31.1 4.410430.0 32.5 108 81.5-119 30.00
Tetrachloroethene 30.0 31.3 2.210430.0 32.0 107 75.2-117 30.00
1,3-Dichloropropane 30.0 31.4 3.410530.0 32.5 108 80.4-119 30.00
2-Hexanone 75.0 83.6 5.011175.0 87.9 117 67.0-143 30.00
Chlorodibromomethane 30.0 33.1 2.711030.0 34.0 113 78.0-120 30.00
1,2-Dibromoethane 30.0 31.3 4.710430.0 32.8 109 79.4-122 30.00
Chlorobenzene 30.0 31.9 1.210630.0 32.3 108 79.0-116 30.00
1,1,1,2-Tetrachloroethane 30.0 32.6 1.810930.0 33.2 111 78.7-117 30.00
Bromoform 30.0 33.7 4.411230.0 35.2 117 70.3-132 30.00
Bromobenzene 30.0 31.5 2.210530.0 32.2 107 81.3-116 30.00
1,1,2,2-Tetrachloroethane 30.0 31.9 6.110630.0 33.9 113 74.5-135 30.00
1,2,3-Trichloropropane 30.0 30.9 6.910330.0 33.1 110 74.8-133 30.00
Ethyl Benzene 30.0 29.9 0.6710030.0 29.7 99 70.9-118 30.00
m,p-Xylene 60.0 61.3 0.1610260.0 61.2 102 71.8-120 30.00
Styrene 30.0 30.4 0.6610130.0 30.2 101 72.8-119 30.00
o-Xylene 30.0 29.9 0.3410030.0 29.8 99 71.9-118 30.00
Isopropylbenzene (Cumene)30.0 30.2 0.6610130.0 30.4 101 70.1-121 30.00
n-Propylbenzene 30.0 30.9 0.010330.0 30.9 103 71.1-122 30.00
2-Chlorotoluene 30.0 29.6 0.679930.0 29.8 99 73.4-117 30.00
4-Chlorotoluene 30.0 30.2 1.010130.0 29.9 100 74.5-118 30.00
1,3,5-Trimethylbenzene 30.0 30.8 1.310330.0 30.4 101 72.5-120 30.00
tert-Butylbenzene 30.0 30.0 0.6610030.0 30.2 101 70.9-119 30.00
1,2,4-Trimethylbenzene 30.0 30.3 0.3310130.0 30.2 101 74.1-120 30.00
sec-Butylbenzene 30.0 30.4 0.010130.0 30.4 101 71.6-121 30.00
1,3-Dichlorobenzene 30.0 29.8 0.349930.0 29.9 100 77.3-118 30.00
4-Isopropyltoluene 30.0 30.4 0.010130.0 30.4 101 72.3-121 30.00
1,4-Dichlorobenzene 30.0 29.9 0.010030.0 29.9 100 78.6-118 30.00
1,2-Dichlorobenzene 30.0 29.5 1.09830.0 29.8 99 80.5-116 30.00
n-Butylbenzene 30.0 30.9 0.3210330.0 31.0 103 72.6-122 30.00
1,2-Dibromo-3-chloropropane 180 174 7.29618018710468.6-135 30.00
1,2,4-Trichlorobenzene 30.0 29.0 0.699730.0 29.2 97 79.7-120 30.00
Print Date: 05/23/2016 N.C. Certification # 481
Page 34 of 62
Blank Spike ID: LCS-S for HBN 115267 [VXX/6487
Blank Spike Lab ID: 200832
Date Analyzed: 05/17/2016 12:07
Spike Duplicate ID: LCSD-S for HBN 115267 [VXX/648
Spike Duplicate Lab ID: 200833
Date Analyzed: 05/17/2016 12:35
Results by SW-846 8260B
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/Kg)
RPD CL
Spike Duplicate (ug/Kg)
31600936001, 31600936002, 31600936003QC for Samples:
Hexachlorobutadiene 30.0 28.1 1.19430.0 27.8 93 69.6-119 30.00
Naphthalene 30.0 28.5 3.89530.0 29.6 99 75.8-126 30.00
trans-1,4-Dichloro-2-butene 150 161 4.810815016911373.5-133 30.00
1,2,3-Trichlorobenzene 30.0 27.9 2.19330.0 28.5 95 80.6-118 30.00
Surrogates
1,2-Dichloroethane-d4 98 98 55.0-173
Toluene d8 102 102 57.0-134
4-Bromofluorobenzene 106 107 23.0-141
Batch Information
Analytical Batch: VMS3992
Analytical Method: SW-846 8260B
Instrument: MSD4
Analyst: JHL
Prep Batch: VXX6487
Prep Method: SW-846 5035 SL
Prep Date/Time: 05/17/2016 15:54
Spike Init Wt./Vol.: 5 g Extract Vol: 5 mL
Dupe Init Wt./Vol.: 5 g Extract Vol: 5 mL
Print Date: 05/23/2016 N.C. Certification # 481
Page 35 of 62
Batch Summary
SW-846 8260B SW-846 5035 SMAnalytical Method:Prep Method:
VXX6491
05/19/2016 15:34
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
MB-S for HBN 115456 [VXX/6491]05/19/2016 14:46 MSD9 JHL201014VMS3995
LCS-S for HBN 115456 [VXX/6491 05/19/2016 12:02 MSD9 JHL201015VMS3995
LCSD-S for HBN 115456 [VXX/649 05/19/2016 12:28 MSD9 JHL201016VMS3995
UST-5(200542MS)05/19/2016 16:54 MSD9 JHL201041VMS3995
UST-5(200542MSD)05/19/2016 17:20 MSD9 JHL201042VMS3995
UST-4 05/19/2016 15:31 MSD9 JHL31600936004VMS3995
UST-5 05/19/2016 15:57 MSD9 JHL31600936005VMS3995
Print Date: 05/23/2016 N.C. Certification # 481
Page 36 of 62
Blank ID: MB-S for HBN 115456 [VXX/6491]
Blank Lab ID: 201014
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31600936004, 31600936005
Dichlorodifluoromethane ND 5.00 ug/Kg 1
Chloromethane ND 1.00 ug/Kg 1
Vinyl chloride ND 1.00 ug/Kg 1
Bromomethane ND 1.00 ug/Kg 1
Chloroethane ND 1.00 ug/Kg 1
Trichlorofluoromethane ND 1.00 ug/Kg 1
1,1-Dichloroethene ND 1.00 ug/Kg 1
Acetone ND 25.0 ug/Kg 1
Methylene chloride ND 5.00 ug/Kg 1
trans-1,2-Dichloroethene ND 1.00 ug/Kg 1
tert-Butyl methyl ether (MTBE)ND 1.00 ug/Kg 1
1,1-Dichloroethane ND 1.00 ug/Kg 1
Diisopropyl Ether ND 1.00 ug/Kg 1
2,2-Dichloropropane ND 1.00 ug/Kg 1
cis-1,2-Dichloroethene ND 1.00 ug/Kg 1
2-Butanone ND 25.0 ug/Kg 1
Bromochloromethane ND 1.00 ug/Kg 1
Chloroform ND 1.00 ug/Kg 1
1,1,1-Trichloroethane ND 1.00 ug/Kg 1
Carbon tetrachloride ND 1.00 ug/Kg 1
1,1-Dichloropropene ND 1.00 ug/Kg 1
Benzene ND 1.00 ug/Kg 1
1,2-Dichloroethane ND 1.00 ug/Kg 1
Trichloroethene ND 1.00 ug/Kg 1
1,2-Dichloropropane ND 1.00 ug/Kg 1
Dibromomethane ND 1.00 ug/Kg 1
Dichlorobromomethane ND 1.00 ug/Kg 1
cis-1,3-Dichloropropene ND 1.00 ug/Kg 1
4-Methyl-2-pentanone ND 5.00 ug/Kg 1
Toluene ND 1.00 ug/Kg 1
Methyl iodide ND 1.00 ug/Kg 1
trans-1,3-Dichloropropene ND 1.00 ug/Kg 1
Carbon disulfide ND 1.00 ug/Kg 1
1,1,2-Trichloroethane ND 1.00 ug/Kg 1
Tetrachloroethene ND 1.00 ug/Kg 1
1,3-Dichloropropane ND 1.00 ug/Kg 1
2-Hexanone ND 5.00 ug/Kg 1
Chlorodibromomethane ND 1.00 ug/Kg 1
1,2-Dibromoethane ND 1.00 ug/Kg 1
Chlorobenzene ND 1.00 ug/Kg 1
1,1,1,2-Tetrachloroethane ND 1.00 ug/Kg 1
Print Date: 05/23/2016 N.C. Certification # 481
Page 37 of 62
Blank ID: MB-S for HBN 115456 [VXX/6491]
Blank Lab ID: 201014
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31600936004, 31600936005
Bromoform ND 1.00 ug/Kg 1
Bromobenzene ND 1.00 ug/Kg 1
1,1,2,2-Tetrachloroethane ND 1.00 ug/Kg 1
1,2,3-Trichloropropane ND 1.00 ug/Kg 1
Ethyl Benzene ND 1.00 ug/Kg 1
m,p-Xylene ND 2.00 ug/Kg 1
Styrene ND 1.00 ug/Kg 1
o-Xylene ND 1.00 ug/Kg 1
Xylene (total)ND 2.00 ug/Kg 1
Isopropylbenzene (Cumene)ND 1.00 ug/Kg 1
n-Propylbenzene ND 1.00 ug/Kg 1
2-Chlorotoluene ND 1.00 ug/Kg 1
4-Chlorotoluene ND 1.00 ug/Kg 1
1,3,5-Trimethylbenzene ND 1.00 ug/Kg 1
tert-Butylbenzene ND 1.00 ug/Kg 1
1,2,4-Trimethylbenzene ND 1.00 ug/Kg 1
sec-Butylbenzene ND 1.00 ug/Kg 1
1,3-Dichlorobenzene ND 1.00 ug/Kg 1
4-Isopropyltoluene ND 1.00 ug/Kg 1
1,4-Dichlorobenzene ND 1.00 ug/Kg 1
1,2-Dichlorobenzene ND 1.00 ug/Kg 1
n-Butylbenzene ND 1.00 ug/Kg 1
1,2-Dibromo-3-chloropropane ND 5.00 ug/Kg 1
1,2,4-Trichlorobenzene ND 1.00 ug/Kg 1
Hexachlorobutadiene ND 1.00 ug/Kg 1
Naphthalene ND 1.00 ug/Kg 1
trans-1,4-Dichloro-2-butene ND 5.00 ug/Kg 1
1,2,3-Trichlorobenzene ND 1.00 ug/Kg 1
Surrogates
1,2-Dichloroethane-d4 106 55.0-173 %1
Toluene d8 108 57.0-134 %1
4-Bromofluorobenzene 95.0 23.0-141 %1
Batch Information
Prep Batch: VXX6491
Prep Method: SW-846 5035 SM
Prep Date/Time: 5/19/2016 3:34:31PM
Prep Initial Wt./Vol.: 5 g
Prep Extract Vol: 5 mL
Analytical Batch: VMS3995
Analytical Method: SW-846 8260B
Instrument: MSD9
Analyst: JHL
Print Date: 05/23/2016 N.C. Certification # 481
Page 38 of 62
Blank Spike ID: LCS-S for HBN 115456 [VXX/6491
Blank Spike Lab ID: 201015
Date Analyzed: 05/19/2016 12:02
Spike Duplicate ID: LCSD-S for HBN 115456 [VXX/649
Spike Duplicate Lab ID: 201016
Date Analyzed: 05/19/2016 12:28
Results by SW-846 8260B
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/Kg)
RPD CL
Spike Duplicate (ug/Kg)
31600936004, 31600936005QC for Samples:
Dichlorodifluoromethane 5.00 6.98 1.2140*5.00 6.90 138*70.0-130 30.00
Chloromethane 5.00 5.70 5.01145.00 5.99 120 70.0-130 30.00
Vinyl chloride 5.00 7.18 5.6144*5.00 6.79 136*70.0-130 30.00
Bromomethane 5.00 4.46 5.3895.00 4.23 85 70.0-130 30.00
Chloroethane 5.00 7.72 2.7154*5.00 7.93 159*70.0-130 30.00
Trichlorofluoromethane 5.00 8.30 2.2166*5.00 8.12 162*70.0-130 30.00
1,1-Dichloroethene 5.00 6.26 2.81255.00 6.09 122 70.0-130 30.00
Acetone 25.0 27.0 1410825.0 ND 94 70.0-130 30.00
Methylene chloride 5.00 5.63 3.11135.00 5.46 109 70.0-130 30.00
trans-1,2-Dichloroethene 5.00 5.39 3.21085.00 5.22 104 70.0-130 30.00
tert-Butyl methyl ether (MTBE)5.00 4.61 6.5925.00 4.32 86 70.0-130 30.00
1,1-Dichloroethane 5.00 5.24 1.51055.00 5.16 103 70.0-130 30.00
Diisopropyl Ether 5.00 4.50 5.5905.00 4.26 85 70.0-130 30.00
2,2-Dichloropropane 5.00 4.66 7.1935.00 4.34 87 70.0-130 30.00
cis-1,2-Dichloroethene 5.00 5.41 4.71085.00 5.16 103 70.0-130 30.00
2-Butanone 25.0 ND 9.49725.0 ND 89 70.0-130 30.00
Bromochloromethane 5.00 6.23 5.61255.00 5.89 118 70.0-130 30.00
Chloroform 5.00 5.51 3.31105.00 5.33 107 70.0-130 30.00
1,1,1-Trichloroethane 5.00 5.10 1.81025.00 5.01 100 70.0-130 30.00
Carbon tetrachloride 5.00 4.47 6.7895.00 4.18 84 70.0-130 30.00
1,1-Dichloropropene 5.00 5.08 5.31025.00 4.82 96 70.0-130 30.00
Benzene 5.00 5.36 3.41075.00 5.18 104 70.0-130 30.00
1,2-Dichloroethane 5.00 5.30 1.71065.00 5.21 104 70.0-130 30.00
Trichloroethene 5.00 5.50 5.21105.00 5.22 104 70.0-130 30.00
1,2-Dichloropropane 5.00 5.17 3.71035.00 4.98 100 70.0-130 30.00
Dibromomethane 5.00 5.47 3.91095.00 5.26 105 70.0-130 30.00
Dichlorobromomethane 5.00 5.06 8.01015.00 4.67 93 70.0-130 30.00
cis-1,3-Dichloropropene 5.00 4.98 5.41005.00 4.72 94 70.0-130 30.00
4-Methyl-2-pentanone 25.0 22.8 8.79125.0 20.9 84 70.0-130 30.00
Toluene 5.00 5.50 5.01105.00 5.23 105 70.0-130 30.00
Methyl iodide 5.00 3.59 0.83725.00 3.62 72 70.0-130 30.00
trans-1,3-Dichloropropene 5.00 4.64 7.8935.00 4.29 86 70.0-130 30.00
Print Date: 05/23/2016 N.C. Certification # 481
Page 39 of 62
Blank Spike ID: LCS-S for HBN 115456 [VXX/6491
Blank Spike Lab ID: 201015
Date Analyzed: 05/19/2016 12:02
Spike Duplicate ID: LCSD-S for HBN 115456 [VXX/649
Spike Duplicate Lab ID: 201016
Date Analyzed: 05/19/2016 12:28
Results by SW-846 8260B
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/Kg)
RPD CL
Spike Duplicate (ug/Kg)
31600936004, 31600936005QC for Samples:
Carbon disulfide 5.00 5.34 3.61075.00 5.15 103 70.0-130 30.00
1,1,2-Trichloroethane 5.00 5.04 2.81015.00 4.90 98 70.0-130 30.00
Tetrachloroethene 5.00 5.24 1.21055.00 5.18 104 70.0-130 30.00
1,3-Dichloropropane 5.00 4.74 4.3955.00 4.54 91 70.0-130 30.00
2-Hexanone 25.0 19.1 6.57625.0 17.9 72 70.0-130 30.00
Chlorodibromomethane 5.00 4.16 2.9835.00 4.04 81 70.0-130 30.00
1,2-Dibromoethane 5.00 4.82 2.1965.00 4.72 94 70.0-130 30.00
Chlorobenzene 5.00 5.08 2.01025.00 4.98 100 70.0-130 30.00
1,1,1,2-Tetrachloroethane 5.00 4.26 3.1855.00 4.13 83 70.0-130 30.00
Bromoform 5.00 3.73 2.7755.00 3.63 73 70.0-130 30.00
Bromobenzene 5.00 5.17 2.01035.00 5.07 101 70.0-130 30.00
1,1,2,2-Tetrachloroethane 5.00 5.12 6.21025.00 4.81 96 70.0-130 30.00
1,2,3-Trichloropropane 5.00 5.09 2.01025.00 4.99 100 70.0-130 30.00
Ethyl Benzene 5.00 4.16 1.7835.00 4.09 82 70.0-130 30.00
m,p-Xylene 10.0 8.75 3.38810.0 8.47 85 70.0-130 30.00
Styrene 5.00 4.14 5.7835.00 3.91 78 70.0-130 30.00
o-Xylene 5.00 4.08 3.2825.00 3.95 79 70.0-130 30.00
Isopropylbenzene (Cumene)5.00 4.25 5.1855.00 4.04 81 70.0-130 30.00
n-Propylbenzene 5.00 4.30 3.3865.00 4.16 83 70.0-130 30.00
2-Chlorotoluene 5.00 4.44 2.7895.00 4.32 86 70.0-130 30.00
4-Chlorotoluene 5.00 4.41 3.9885.00 4.24 85 70.0-130 30.00
1,3,5-Trimethylbenzene 5.00 4.13 3.4835.00 3.99 80 70.0-130 30.00
tert-Butylbenzene 5.00 4.23 3.1855.00 4.10 82 70.0-130 30.00
1,2,4-Trimethylbenzene 5.00 4.26 2.4855.00 4.16 83 70.0-130 30.00
sec-Butylbenzene 5.00 4.26 3.1855.00 4.13 83 70.0-130 30.00
1,3-Dichlorobenzene 5.00 4.54 1.6915.00 4.47 89 70.0-130 30.00
4-Isopropyltoluene 5.00 4.20 3.4845.00 4.06 81 70.0-130 30.00
1,4-Dichlorobenzene 5.00 4.54 1.3915.00 4.48 90 70.0-130 30.00
1,2-Dichlorobenzene 5.00 4.77 3.4955.00 4.61 92 70.0-130 30.00
n-Butylbenzene 5.00 4.06 4.3815.00 3.89 78 70.0-130 30.00
1,2-Dibromo-3-chloropropane 30.0 23.0 8.67730.0 21.1 70 70.0-130 30.00
1,2,4-Trichlorobenzene 5.00 4.45 4.4895.00 4.26 85 70.0-130 30.00
Print Date: 05/23/2016 N.C. Certification # 481
Page 40 of 62
Blank Spike ID: LCS-S for HBN 115456 [VXX/6491
Blank Spike Lab ID: 201015
Date Analyzed: 05/19/2016 12:02
Spike Duplicate ID: LCSD-S for HBN 115456 [VXX/649
Spike Duplicate Lab ID: 201016
Date Analyzed: 05/19/2016 12:28
Results by SW-846 8260B
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/Kg)
RPD CL
Spike Duplicate (ug/Kg)
31600936004, 31600936005QC for Samples:
Hexachlorobutadiene 5.00 4.80 6.9965.00 4.48 90 70.0-130 30.00
Naphthalene 5.00 4.07 6.1815.00 3.83 77 70.0-130 30.00
trans-1,4-Dichloro-2-butene 25.0 20.4 6.68225.0 19.1 76 70.0-130 30.00
1,2,3-Trichlorobenzene 5.00 4.53 3.4915.00 4.38 88 70.0-130 30.00
Surrogates
1,2-Dichloroethane-d4 104 101 55.0-173
Toluene d8 110 110 57.0-134
4-Bromofluorobenzene 98 98 23.0-141
Batch Information
Analytical Batch: VMS3995
Analytical Method: SW-846 8260B
Instrument: MSD9
Analyst: JHL
Prep Batch: VXX6491
Prep Method: SW-846 5035 SM
Prep Date/Time: 05/19/2016 15:34
Spike Init Wt./Vol.: 5 g Extract Vol: 5 mL
Dupe Init Wt./Vol.: 5 g Extract Vol: 5 mL
Print Date: 05/23/2016 N.C. Certification # 481
Page 41 of 62
Original Sample ID: 31600936005 (UST-5)
MS Sample ID: 201041
MSD Sample ID: 201042
Analysis Date: 05/19/2016 15:57
Analysis Date: 05/19/2016 16:54
Analysis Date: 05/19/2016 17:20
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (ug/Kg)Spike Duplicate (ug/Kg)
CL RPD CL
QC for Samples:31600936004, 31600936005
1,1,1,2-Tetrachloroethane ND 339 276 339 267 79 3.081 30.0069.0-120
1,1,1-Trichloroethane ND 339 330 339 339 100 2.997 30.0078.0-121
1,1,2,2-Tetrachloroethane ND 339 343 339 348 103 1.2101 30.0076.0-136
1,1,2-Trichloroethane ND 339 355 339 364 107 2.7105 30.0065.0-128
1,1-Dichloroethane ND 339 346 339 363 107 5.0102 30.0072.0-139
1,1-Dichloroethene ND 339 405 339 408 120 1.0119 30.0072.0-135
1,1-Dichloropropene ND 339 348 339 363 107 4.3103 30.0069.0-137
1,2,3-Trichlorobenzene ND 339 327 339 344 101 4.996 30.0061.0-126
1,2,3-Trichloropropane ND 339 357 339 375 110 4.9105 30.0010.0-218
1,2,4-Trichlorobenzene ND 339 321 339 339 100 5.495 30.0061.0-125
1,2,4-Trimethylbenzene ND 339 313 339 322 95 3.092 30.0031.0-172
1,2-Dibromo-3-chloropropane ND 2033 1270 2033 1350 66 6.163 30.0043.0-229
1,2-Dibromoethane ND 339 343 339 354 104 2.8101 30.0078.0-148
1,2-Dichlorobenzene ND 339 323 339 335 99 3.895 30.0058.0-148
1,2-Dichloroethane ND 339 358 339 366 108 1.9106 30.0073.0-146
1,2-Dichloropropane ND 339 341 339 361 106 5.5101 30.0076.0-136
1,3,5-Trimethylbenzene ND 339 319 339 324 95 1.794 30.0068.0-132
1,3-Dichlorobenzene ND 339 329 339 342 101 4.197 30.0055.0-145
1,3-Dichloropropane ND 339 335 339 349 103 4.099 30.0033.0-137
1,4-Dichlorobenzene ND 339 328 339 335 99 2.197 30.0053.0-146
2,2-Dichloropropane ND 339 341 339 353 104 3.2101 30.0058.0-150
2-Butanone ND 1703 3880 1703 4030 238 3.8228 30.0041.0-256
2-Chlorotoluene ND 339 312 339 324 95 3.992 30.0060.0-144
2-Hexanone ND 1703 3350 1703 3310 195 *1.2197 * 30.0042.0-111
4-Chlorotoluene ND 339 329 339 348 102 5.397 30.0059.0-141
4-Isopropyltoluene ND 339 318 339 320 94 0.8694 30.0075.0-122
4-Methyl-2-pentanone ND 1703 3320 1703 3470 205 *4.4196 * 30.006.90-166
Acetone ND 1703 4650 1703 4630 273 0.30274 30.006.80-355
Benzene ND 339 367 339 377 111 3.0108 30.0075.0-133
Bromobenzene ND 339 569 339 409 120 33*168 * 30.0066.0-140
Bromochloromethane ND 339 389 339 405 119 4.2115 30.0085.0-136
Bromoform ND 339 214 339 202 59 *5.963 * 30.0075.0-151
Bromomethane ND 339 185 339 203 60 9.255 30.0030.0-127
n-Butylbenzene ND 339 310 339 313 92 1.391 30.0041.0-147
Carbon disulfide ND 339 329 339 331 98 0.8397 30.0064.0-145
Carbon tetrachloride ND 339 257 339 256 75 0.5476 30.0064.0-142
Print Date: 05/23/2016 N.C. Certification # 481
Page 42 of 62
Original Sample ID: 31600936005 (UST-5)
MS Sample ID: 201041
MSD Sample ID: 201042
Analysis Date: 05/19/2016 15:57
Analysis Date: 05/19/2016 16:54
Analysis Date: 05/19/2016 17:20
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (ug/Kg)Spike Duplicate (ug/Kg)
CL RPD CL
QC for Samples:31600936004, 31600936005
Chlorobenzene ND 339 359 339 368 108 2.6106 30.0066.0-135
Chlorodibromomethane 208 339 249 339 233 7.4 *6.912 * 30.0078.0-141
Chloroethane ND 339 115 339 130 38 1334 30.0021.0-182
Chloroform ND 339 353 339 366 108 3.4104 30.0071.0-143
Chloromethane ND 339 350 339 361 106 3.1103 30.0069.0-138
Dibromomethane ND 339 371 339 384 113 3.3109 30.0080.0-150
Dichlorobromomethane ND 339 287 339 288 85 0.085 30.0077.0-140
Dichlorodifluoromethane ND 339 424 339 428 126 0.97125 30.0082.0-130
cis-1,3-Dichloropropene ND 339 314 339 329 97 4.793 30.0072.0-146
trans-1,3-Dichloropropene ND 339 315 339 329 97 4.393 30.0045.0-144
Diisopropyl Ether ND 339 305 339 315 93 3.190 30.0079.0-122
Ethyl Benzene ND 339 304 339 321 95 5.790 30.0074.0-126
Hexachlorobutadiene ND 339 333 339 349 103 4.498 30.0052.0-134
Isopropylbenzene (Cumene)ND 339 319 339 341 100 6.794 30.0074.0-123
Methyl iodide ND 339 201 339 208 61 3.459 30.0041.0-126
Methylene chloride ND 339 383 339 396 117 3.5113 30.0049.0-155
Naphthalene ND 339 316 339 330 97 4.393 30.0055.0-140
Styrene ND 339 316 339 313 92 0.8793 30.0073.0-123
Tetrachloroethene ND 339 369 339 375 111 1.8109 30.0046.0-153
Toluene ND 339 384 339 401 118 4.6113 30.0066.0-128
Trichloroethene ND 339 360 339 371 109 3.0106 30.0085.0-136
Trichlorofluoromethane ND 339 102 339 100 30 *1.430 * 30.0077.0-132
Vinyl chloride ND 339 399 339 403 119 0.68118 30.0068.0-137
cis-1,2-Dichloroethene ND 339 369 339 390 115 5.4109 30.0077.0-134
m,p-Xylene ND 679 645 679 667 98 3.695 30.0080.0-118
n-Propylbenzene ND 339 318 339 329 97 3.894 30.0072.0-128
o-Xylene ND 339 319 339 320 94 0.4394 30.0080.0-121
sec-Butylbenzene ND 339 310 339 319 94 3.191 30.0057.0-138
tert-Butyl methyl ether (MTBE)ND 339 316 339 330 97 4.393 30.0067.0-135
tert-Butylbenzene ND 339 315 339 325 96 3.493 30.0061.0-142
trans-1,2-Dichloroethene ND 339 368 339 379 112 2.9108 30.0072.0-135
trans-1,4-Dichloro-2-butene ND 1703 1370 1703 1400 83 2.181 30.0049.0-211
Surrogates
1,2-Dichloroethane-d4 9998 55.0-173
4-Bromofluorobenzene 101103 23.0-141
Toluene d8 108107 57.0-134
Print Date: 05/23/2016 N.C. Certification # 481
Page 43 of 62
Original Sample ID: 31600936005 (UST-5)
MS Sample ID: 201041
MSD Sample ID: 201042
Analysis Date: 05/19/2016 15:57
Analysis Date: 05/19/2016 16:54
Analysis Date: 05/19/2016 17:20
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (%)Spike Duplicate (%)
CL RPD CL
QC for Samples:31600936004, 31600936005
Batch Information
Analytical Batch: VMS3995
Analytical Method: SW-846 8260B
Instrument: MSD9
Analyst: JHL
Prep Batch: VXX6491
Prep Method: SW-846 5035 SM
Prep Date/Time: 05/19/2016 15:34
MS Init Wt./Vol.: 5.06 g Extract Vol.: 5 mL
MSD Init Wt./Vol.: 5.06 g Extract Vol.: 5 mL
Print Date: 05/23/2016 N.C. Certification # 481
Page 44 of 62
Batch Summary
SW-846 8270D SW-846 3541Analytical Method:Prep Method:
XXX5737
05/12/2016 15:06
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
MB for HBN 115051 [XXX/5737]05/18/2016 11:41 MSD10 DTF200558XMS2629
LCS for HBN 115051 [XXX/5737]05/18/2016 12:02 MSD10 DTF200559XMS2629
VST-1(200538MS)05/18/2016 15:46 MSD10 DTF200560XMS2629
VST-1(200538MSD)05/18/2016 16:08 MSD10 DTF200561XMS2629
UST-1 05/18/2016 15:25 MSD10 DTF31600936001XMS2629
UST-2 05/18/2016 16:30 MSD10 DTF31600936002XMS2629
UST-3 05/18/2016 16:51 MSD10 DTF31600936003XMS2629
UST-5 05/18/2016 17:35 MSD10 DTF31600936005XMS2629
Print Date: 05/23/2016 N.C. Certification # 481
Page 45 of 62
Blank ID: MB for HBN 115051 [XXX/5737]
Blank Lab ID: 200558
Matrix: Soil-Solid as dry weight
Results by SW-846 8270D
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31600936001, 31600936002, 31600936003, 31600936005
Phenol ND 313 ug/Kg 1
Bis(2-Chloroethyl)ether ND 313 ug/Kg 1
2-Chlorophenol ND 313 ug/Kg 1
1,3-Dichlorobenzene ND 313 ug/Kg 1
1,4-Dichlorobenzene ND 313 ug/Kg 1
1,2-Dichlorobenzene ND 313 ug/Kg 1
2-Methylphenol ND 313 ug/Kg 1
3 and/or 4-Methylphenol ND 313 ug/Kg 1
Bis(2-Chloroisopropyl)ether ND 313 ug/Kg 1
n-Nitrosodi-n-propylamine ND 313 ug/Kg 1
Hexachloroethane ND 313 ug/Kg 1
Nitrobenzene ND 313 ug/Kg 1
Isophorone ND 313 ug/Kg 1
2-Nitrophenol ND 313 ug/Kg 1
2,4-Dimethylphenol ND 313 ug/Kg 1
Bis(2-Chloroethoxy)methane ND 313 ug/Kg 1
2,4-Dichlorophenol ND 313 ug/Kg 1
1,2,4-Trichlorobenzene ND 313 ug/Kg 1
Naphthalene ND 313 ug/Kg 1
4-Chloroaniline ND 313 ug/Kg 1
Hexachlorobutadiene ND 313 ug/Kg 1
4-Chloro-3-methylphenol ND 313 ug/Kg 1
2-Methylnaphthalene ND 313 ug/Kg 1
Hexachlorocyclopentadiene ND 626 ug/Kg 1
2,4,5-Trichlorophenol ND 313 ug/Kg 1
2,4,6-Trichlorophenol ND 313 ug/Kg 1
2-Chloronaphthalene ND 313 ug/Kg 1
2-Nitroaniline ND 313 ug/Kg 1
Dimethyl phthalate ND 313 ug/Kg 1
2,6-Dinitrotoluene ND 313 ug/Kg 1
Acenaphthene ND 313 ug/Kg 1
2,4-Dinitrophenol ND 1570 ug/Kg 1
4-Nitrophenol ND 1570 ug/Kg 1
Dibenzofuran ND 313 ug/Kg 1
2,4-Dinitrotoluene ND 313 ug/Kg 1
Fluorene ND 313 ug/Kg 1
Diethyl phthalate ND 313 ug/Kg 1
4-Chlorophenyl phenyl ether ND 313 ug/Kg 1
4-Nitroaniline ND 1570 ug/Kg 1
4,6-Dinitro-2-methylphenol ND 1570 ug/Kg 1
Diphenylamine ND 313 ug/Kg 1
Print Date: 05/23/2016 N.C. Certification # 481
Page 46 of 62
Blank ID: MB for HBN 115051 [XXX/5737]
Blank Lab ID: 200558
Matrix: Soil-Solid as dry weight
Results by SW-846 8270D
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31600936001, 31600936002, 31600936003, 31600936005
4-Bromophenyl phenyl ether ND 313 ug/Kg 1
Hexachlorobenzene ND 1570 ug/Kg 1
Pentachlorophenol ND 1570 ug/Kg 1
Phenanthrene ND 313 ug/Kg 1
Anthracene ND 313 ug/Kg 1
Di-n-butyl phthalate ND 313 ug/Kg 1
Fluoranthene ND 313 ug/Kg 1
Pyrene ND 313 ug/Kg 1
Butyl benzyl phthalate ND 313 ug/Kg 1
Benzo(a)anthracene ND 313 ug/Kg 1
Chrysene ND 313 ug/Kg 1
Bis(2-Ethylhexyl)phthalate ND 313 ug/Kg 1
Di-n-octyl phthalate ND 313 ug/Kg 1
Benzo(b)fluoranthene ND 313 ug/Kg 1
Benzo(k)fluoranthene ND 313 ug/Kg 1
Benzo(a)pyrene ND 313 ug/Kg 1
Indeno(1,2,3-cd)pyrene ND 313 ug/Kg 1
Dibenz(a,h)anthracene ND 313 ug/Kg 1
Benzo(g,h,i)perylene ND 313 ug/Kg 1
Benzoic acid ND 1570 ug/Kg 1
Acenaphthylene ND 313 ug/Kg 1
Surrogates
2-Fluorophenol 113 42.0-123 %1
Phenol-d6 119 48.0-125 %1
Nitrobenzene-d5 119*46.0-117 %1
2-Fluorobiphenyl 112 48.0-123 %1
2,4,6-Tribromophenol 57.0 41.0-129 %1
Terphenyl-d14 109 44.0-140 %1
Batch Information
Prep Batch: XXX5737
Prep Method: SW-846 3541
Prep Date/Time: 5/12/2016 3:06:00PM
Prep Initial Wt./Vol.: 32 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2629
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 05/23/2016 N.C. Certification # 481
Page 47 of 62
Blank Spike ID: LCS for HBN 115051 [XXX/5737]
Blank Spike Lab ID: 200559
Date Analyzed: 05/18/2016 12:02
Results by SW-846 8270D
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)CL
Blank Spike (ug/Kg)
31600936001, 31600936002, 31600936003, 31600936005QC for Samples:
Phenol 3130 3430 110 69.0-116
Bis(2-Chloroethyl)ether 3130 3820 122 58.0-127
2-Chlorophenol 3130 3270 105 70.0-115
1,3-Dichlorobenzene 3130 3170 101 63.0-119
1,4-Dichlorobenzene 3130 3180 102 65.0-119
1,2-Dichlorobenzene 3130 3200 102 66.0-119
2-Methylphenol 3130 3550 114 69.0-118
3 and/or 4-Methylphenol 6250 7070 113 71.0-124
Bis(2-Chloroisopropyl)ether 3130 3260 104 65.0-112
n-Nitrosodi-n-propylamine 3130 3500 112 70.0-112
Hexachloroethane 3130 3210 103 64.0-118
Nitrobenzene 3130 3460 111 70.0-116
Isophorone 3130 3530 113 75.0-118
2-Nitrophenol 3130 3230 103 71.0-116
2,4-Dimethylphenol 3130 3410 109 53.0-122
Bis(2-Chloroethoxy)methane 3130 3610 115 72.0-119
Benzoic acid 3130 ND 33 0.00-114
2,4-Dichlorophenol 3130 3310 106 73.0-120
1,2,4-Trichlorobenzene 3130 3250 104 73.0-124
Naphthalene 3130 3190 102 72.0-116
4-Chloroaniline 3130 446 14 7.00-126
Hexachlorobutadiene 3130 3210 103 70.0-121
4-Chloro-3-methylphenol 3130 3190 102 72.0-121
2-Methylnaphthalene 3130 3240 104 75.0-120
Hexachlorocyclopentadiene 3130 5280 169*71.0-130
2,4,5-Trichlorophenol 3130 3230 103 76.0-128
2,4,6-Trichlorophenol 3130 3310 106 68.0-119
2-Chloronaphthalene 3130 2870 92 66.0-110
2-Nitroaniline 3130 2690 86 60.0-103
Dimethyl phthalate 3130 3220 103 73.0-121
2,6-Dinitrotoluene 3130 3220 103 74.0-121
Acenaphthene 3130 3210 103 74.0-118
Print Date: 05/23/2016 N.C. Certification # 481
Page 48 of 62
Blank Spike ID: LCS for HBN 115051 [XXX/5737]
Blank Spike Lab ID: 200559
Date Analyzed: 05/18/2016 12:02
Results by SW-846 8270D
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)CL
Blank Spike (ug/Kg)
31600936001, 31600936002, 31600936003, 31600936005QC for Samples:
2,4-Dinitrophenol 3130 2180 70 17.0-125
4-Nitrophenol 3130 3150 101 56.0-133
Dibenzofuran 3130 3260 104 75.0-120
2,4-Dinitrotoluene 3130 3270 105 76.0-122
Fluorene 3130 3290 105 77.0-123
Diethyl phthalate 3130 3180 102 74.0-120
4-Chlorophenyl phenyl ether 3130 3320 106 76.0-125
4-Nitroaniline 3130 2040 65 61.0-112
4,6-Dinitro-2-methylphenol 3130 3000 96 50.0-143
Diphenylamine 3130 2680 86 72.0-124
4-Bromophenyl phenyl ether 3130 3300 106 71.0-130
Hexachlorobenzene 3130 3190 102 71.0-123
Pentachlorophenol 3130 3480 111 32.0-140
Phenanthrene 3130 3210 103 74.0-128
Anthracene 3130 3240 104 73.0-128
Di-n-butyl phthalate 3130 3260 104 75.0-129
Fluoranthene 3130 3240 104 74.0-130
Pyrene 3130 3110 99 74.0-121
Butyl benzyl phthalate 3130 3260 104 73.0-118
Benzo(a)anthracene 3130 3160 101 72.0-123
Chrysene 3130 3230 103 72.0-128
Bis(2-Ethylhexyl)phthalate 3130 3200 102 69.0-125
Di-n-octyl phthalate 3130 3500 112 71.0-121
Benzo(b)fluoranthene 3130 3400 109 63.0-116
Benzo(k)fluoranthene 3130 3750 120 74.0-125
Benzo(a)pyrene 3130 3410 109 71.0-126
Indeno(1,2,3-cd)pyrene 3130 3700 118 76.0-137
Dibenz(a,h)anthracene 3130 3700 118 73.0-138
Benzo(g,h,i)perylene 3130 3750 120 77.0-143
Acenaphthylene 3130 3330 107 75.0-122
Surrogates
2-Fluorophenol 122 42.0-123
Print Date: 05/23/2016 N.C. Certification # 481
Page 49 of 62
Blank Spike ID: LCS for HBN 115051 [XXX/5737]
Blank Spike Lab ID: 200559
Date Analyzed: 05/18/2016 12:02
Results by SW-846 8270D
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)CL
Blank Spike (%)
31600936001, 31600936002, 31600936003, 31600936005QC for Samples:
Phenol-d6 124 48.0-125
Nitrobenzene-d5 124*46.0-117
2-Fluorobiphenyl 118 48.0-123
2,4,6-Tribromophenol 121 41.0-129
Terphenyl-d14 119 44.0-140
Batch Information
Analytical Batch: XMS2629
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX5737
Prep Method: SW-846 3541
Prep Date/Time: 05/12/2016 15:06
Spike Init Wt./Vol.: 32 g Extract Vol: 10 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 05/23/2016 N.C. Certification # 481
Page 50 of 62
Original Sample ID: 31600936001 (UST-1)
MS Sample ID: 200560
MSD Sample ID: 200561
Analysis Date: 05/18/2016 15:25
Analysis Date: 05/18/2016 15:46
Analysis Date: 05/18/2016 16:08
Matrix: Soil-Solid as dry weight
Results by SW-846 8270D
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (ug/Kg)Spike Duplicate (ug/Kg)
CL RPD CL
QC for Samples:31600936001, 31600936002, 31600936003, 31600936005
1,2,4-Trichlorobenzene ND 4116 3530 4116 3800 92 7.286 30.0068.9-119
1,2-Dichlorobenzene ND 4116 3520 4116 3780 92 7.285 30.0073.3-121
1,3-Dichlorobenzene ND 4116 3470 4116 3730 91 7.384 30.0069.7-119
1,4-Dichlorobenzene ND 4116 3530 4116 3780 92 6.886 30.0070.6-117
2,4,5-Trichlorophenol ND 4116 3660 4116 3950 96 8.089 30.0072.4-118
2,4,6-Trichlorophenol ND 4116 3620 4116 3820 93 5.788 30.0067.9-116
2,4-Dichlorophenol ND 4116 3760 4116 4070 99 8.191 30.0074.5-115
2,4-Dinitrophenol ND 4116 2060 4116 3790 92 59*50 30.0020.4-130
2,4-Dinitrotoluene ND 4116 3730 4116 4020 98 7.591 30.0067.6-136
2,6-Dinitrotoluene ND 4116 3620 4116 3910 95 7.488 30.0069.3-131
2-Chloronaphthalene ND 4116 3140 4116 3350 81 6.576 30.0070.3-124
2-Chlorophenol ND 4116 3790 4116 4040 98 6.492 30.0077.1-111
2-Methylnaphthalene ND 4116 3490 4116 3750 91 7.385 30.0074.1-111
2-Methylphenol ND 4116 3740 4116 4120 100 9.491 30.0078.7-116
2-Nitroaniline ND 4116 3270 4116 3570 87 8.979 30.0070.0-129
2-Nitrophenol ND 4116 3660 4116 3910 95 6.689 30.0063.3-112
3 and/or 4-Methylphenol ND 8232 7880 8232 8570 104 *8.596 30.0071.2-101
4,6-Dinitro-2-methylphenol ND 4116 3220 4116 3940 96 2078 30.0039.4-126
4-Chloro-3-methylphenol ND 4116 3540 4116 3830 93 7.986 30.0080.0-115
4-Chloroaniline ND 4116 666 4116 897 22 *3016 * 30.0025.1-237
4-Chlorophenyl phenyl ether ND 4116 3690 4116 3920 95 6.389 30.0072.8-125
Acenaphthene ND 4116 3550 4116 3770 91 6.186 30.0071.0-125
Acenaphthylene ND 4116 3670 4116 3950 96 7.689 30.0073.0-140
Anthracene ND 4116 3520 4116 3860 94 9.385 30.0066.9-119
Benzo(a)anthracene ND 4116 3360 4116 3630 88 7.582 30.0051.8-127
Benzo(a)pyrene ND 4116 3640 4116 4050 98 1188 30.0078.5-137
Benzo(b)fluoranthene ND 4116 3490 4116 3820 93 8.785 30.0062.3-134
Benzo(g,h,i)perylene ND 4116 3900 4116 4250 103 8.495 30.0056.2-149
Benzo(k)fluoranthene ND 4116 4000 4116 4330 105 7.997 30.0079.7-133
Benzoic acid ND 4116 ND 4116 2660 652.1 30.001.00-140
Bis(2-Chloroethoxy)methane ND 4116 3770 4116 4060 99 7.891 30.0071.4-123
Bis(2-Chloroethyl)ether ND 4116 3870 4116 4460 108 1494 30.0064.0-120
Bis(2-Chloroisopropyl)ether ND 4116 3630 4116 3920 95 7.788 30.0060.5-123
Bis(2-Ethylhexyl)phthalate ND 4116 3480 4116 3820 93 9.085 30.0068.5-134
4-Bromophenyl phenyl ether ND 4116 3520 4116 3860 94 9.385 30.0065.2-127
Butyl benzyl phthalate ND 4116 3480 4116 3780 92 8.484 30.0064.4-133
Print Date: 05/23/2016 N.C. Certification # 481
Page 51 of 62
Original Sample ID: 31600936001 (UST-1)
MS Sample ID: 200560
MSD Sample ID: 200561
Analysis Date: 05/18/2016 15:25
Analysis Date: 05/18/2016 15:46
Analysis Date: 05/18/2016 16:08
Matrix: Soil-Solid as dry weight
Results by SW-846 8270D
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (ug/Kg)Spike Duplicate (ug/Kg)
CL RPD CL
QC for Samples:31600936001, 31600936002, 31600936003, 31600936005
Chrysene ND 4116 3490 4116 3870 94 1085 30.0072.7-124
Di-n-butyl phthalate ND 4116 3480 4116 3810 92 9.184 30.0067.9-125
Di-n-octyl phthalate ND 4116 3670 4116 4000 97 8.689 30.0048.9-162
Dibenz(a,h)anthracene ND 4116 3840 4116 4160 101 8.293 30.0058.6-146
Dibenzofuran ND 4116 3560 4116 3860 94 7.886 30.0070.6-115
Diethyl phthalate ND 4116 3500 4116 3790 92 8.085 30.0070.8-127
Dimethyl phthalate ND 4116 3580 4116 3850 93 7.587 30.0068.5-122
2,4-Dimethylphenol ND 4116 3480 4116 3670 89 5.285 * 30.0085.4-138
Diphenylamine ND 4116 3180 4116 3440 84 8.077 30.0073.6-208
Fluoranthene ND 4116 3500 4116 3800 92 8.385 30.0064.6-129
Fluorene ND 4116 3630 4116 3930 95 8.088 30.0072.4-128
Hexachlorobenzene ND 4116 3430 4116 3710 90 7.883 30.0062.9-124
Hexachlorobutadiene ND 4116 3540 4116 3770 91 6.186 30.0069.1-118
Hexachlorocyclopentadiene ND 4116 5870 4116 6370 155 8.2142 30.001.00-176
Hexachloroethane ND 4116 3400 4116 3640 88 7.182 30.0068.0-122
Indeno(1,2,3-cd)pyrene ND 4116 3830 4116 4210 102 9.593 30.0029.1-157
Isophorone ND 4116 3620 4116 3930 95 8.488 30.0065.2-143
Naphthalene ND 4116 3500 4116 3800 92 7.985 30.0049.9-137
4-Nitroaniline ND 4116 3300 4116 3630 88 9.580 30.0050.8-178
Nitrobenzene ND 4116 3570 4116 3910 95 9.287 30.0071.4-122
4-Nitrophenol ND 4116 3600 4116 4080 99 1287 30.0056.8-133
Pentachlorophenol ND 4116 3620 4116 4140 101 1488 30.0029.2-108
Phenanthrene ND 4116 3420 4116 3780 92 9.983 30.0055.8-128
Phenol ND 4116 3870 4116 4140 100 6.394 30.0071.2-120
Pyrene ND 4116 3400 4116 3680 89 7.583 30.0068.5-140
n-Nitrosodi-n-propylamine ND 4116 3650 4116 3970 96 8.389 30.0074.3-133
Surrogates
2,4,6-Tribromophenol 110104 41.0-129
2-Fluorobiphenyl 10396 48.0-123
2-Fluorophenol 113108 42.0-123
Nitrobenzene-d5 10798 46.0-117
Phenol-d6 117108 48.0-125
Terphenyl-d14 10295 44.0-140
Print Date: 05/23/2016 N.C. Certification # 481
Page 52 of 62
Original Sample ID: 31600936001 (UST-1)
MS Sample ID: 200560
MSD Sample ID: 200561
Analysis Date: 05/18/2016 15:25
Analysis Date: 05/18/2016 15:46
Analysis Date: 05/18/2016 16:08
Matrix: Soil-Solid as dry weight
Results by SW-846 8270D
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (%)Spike Duplicate (%)
CL RPD CL
QC for Samples:31600936001, 31600936002, 31600936003, 31600936005
Batch Information
Analytical Batch: XMS2629
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX5737
Prep Method: SW-846 3541
Prep Date/Time: 05/12/2016 15:06
MS Init Wt./Vol.: 32.05 g Extract Vol.: 10 mL
MSD Init Wt./Vol.: 32.03 g Extract Vol.: 10 mL
Print Date: 05/23/2016 N.C. Certification # 481
Page 53 of 62
Batch Summary
SW-846 8270D SW-846 3541Analytical Method:Prep Method:
XXX5757
05/19/2016 16:04
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
MB for HBN 115463 [XXX/5757]05/20/2016 16:28 MSD10 DTF201035XMS2632
LCS for HBN 115463 [XXX/5757]05/20/2016 16:50 MSD10 DTF201036XMS2632
UST-2(200539MS)05/20/2016 23:03 MSD10 DTF201037XMS2632
UST-2(200539MSD)05/20/2016 23:25 MSD10 DTF201038XMS2632
UST-1 05/20/2016 22:20 MSD10 DTF31600936001XMS2632
UST-2 05/20/2016 22:41 MSD10 DTF31600936002XMS2632
UST-3 05/20/2016 23:47 MSD10 DTF31600936003XMS2632
UST-4 05/21/2016 00:09 MSD10 DTF31600936004XMS2632
UST-5 05/21/2016 00:53 MSD10 DTF31600936005XMS2632
Print Date: 05/23/2016 N.C. Certification # 481
Page 54 of 62
Blank ID: MB for HBN 115463 [XXX/5757]
Blank Lab ID: 201035
Matrix: Soil-Solid as dry weight
Results by SW-846 8270D
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31600936001, 31600936002, 31600936003, 31600936004, 31600936005
Phenol ND 313 ug/Kg 1
Bis(2-Chloroethyl)ether ND 313 ug/Kg 1
2-Chlorophenol ND 313 ug/Kg 1
1,3-Dichlorobenzene ND 313 ug/Kg 1
1,4-Dichlorobenzene ND 313 ug/Kg 1
1,2-Dichlorobenzene ND 313 ug/Kg 1
2-Methylphenol ND 313 ug/Kg 1
3 and/or 4-Methylphenol ND 313 ug/Kg 1
Bis(2-Chloroisopropyl)ether ND 313 ug/Kg 1
n-Nitrosodi-n-propylamine ND 313 ug/Kg 1
Hexachloroethane ND 313 ug/Kg 1
Nitrobenzene ND 313 ug/Kg 1
Isophorone ND 313 ug/Kg 1
2-Nitrophenol ND 313 ug/Kg 1
2,4-Dimethylphenol ND 313 ug/Kg 1
Bis(2-Chloroethoxy)methane ND 313 ug/Kg 1
2,4-Dichlorophenol ND 313 ug/Kg 1
1,2,4-Trichlorobenzene ND 313 ug/Kg 1
Naphthalene ND 313 ug/Kg 1
4-Chloroaniline ND 313 ug/Kg 1
Hexachlorobutadiene ND 313 ug/Kg 1
4-Chloro-3-methylphenol ND 313 ug/Kg 1
2-Methylnaphthalene ND 313 ug/Kg 1
Hexachlorocyclopentadiene ND 626 ug/Kg 1
2,4,5-Trichlorophenol ND 313 ug/Kg 1
2,4,6-Trichlorophenol ND 313 ug/Kg 1
2-Chloronaphthalene ND 313 ug/Kg 1
2-Nitroaniline ND 313 ug/Kg 1
3-Nitroaniline ND 1570 ug/Kg 1
Dimethyl phthalate ND 313 ug/Kg 1
2,6-Dinitrotoluene ND 313 ug/Kg 1
Acenaphthene ND 313 ug/Kg 1
2,4-Dinitrophenol ND 1570 ug/Kg 1
4-Nitrophenol ND 1570 ug/Kg 1
Dibenzofuran ND 313 ug/Kg 1
2,4-Dinitrotoluene ND 313 ug/Kg 1
Fluorene ND 313 ug/Kg 1
Diethyl phthalate ND 313 ug/Kg 1
4-Chlorophenyl phenyl ether ND 313 ug/Kg 1
4-Nitroaniline ND 1570 ug/Kg 1
4,6-Dinitro-2-methylphenol ND 1570 ug/Kg 1
Print Date: 05/23/2016 N.C. Certification # 481
Page 55 of 62
Blank ID: MB for HBN 115463 [XXX/5757]
Blank Lab ID: 201035
Matrix: Soil-Solid as dry weight
Results by SW-846 8270D
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31600936001, 31600936002, 31600936003, 31600936004, 31600936005
Diphenylamine ND 313 ug/Kg 1
4-Bromophenyl phenyl ether ND 313 ug/Kg 1
Hexachlorobenzene ND 1570 ug/Kg 1
Pentachlorophenol ND 1570 ug/Kg 1
Phenanthrene ND 313 ug/Kg 1
Anthracene ND 313 ug/Kg 1
Di-n-butyl phthalate ND 313 ug/Kg 1
Fluoranthene ND 313 ug/Kg 1
Pyrene ND 313 ug/Kg 1
Butyl benzyl phthalate ND 313 ug/Kg 1
Benzo(a)anthracene ND 313 ug/Kg 1
3,3'-Dichlorobenzidine ND 626 ug/Kg 1
Chrysene ND 313 ug/Kg 1
Bis(2-Ethylhexyl)phthalate ND 313 ug/Kg 1
Di-n-octyl phthalate ND 313 ug/Kg 1
Benzo(b)fluoranthene ND 313 ug/Kg 1
Benzo(k)fluoranthene ND 313 ug/Kg 1
Benzo(a)pyrene ND 313 ug/Kg 1
Indeno(1,2,3-cd)pyrene ND 313 ug/Kg 1
Dibenz(a,h)anthracene ND 313 ug/Kg 1
Benzo(g,h,i)perylene ND 313 ug/Kg 1
Benzoic acid ND 1570 ug/Kg 1
Acenaphthylene ND 313 ug/Kg 1
Surrogates
2-Fluorophenol 94.0 42.0-123 %1
Phenol-d6 98.0 48.0-125 %1
Nitrobenzene-d5 95.0 46.0-117 %1
2-Fluorobiphenyl 81.0 48.0-123 %1
2,4,6-Tribromophenol 49.0 41.0-129 %1
Terphenyl-d14 84.0 44.0-140 %1
Batch Information
Prep Batch: XXX5757
Prep Method: SW-846 3541
Prep Date/Time: 5/19/2016 4:04:00PM
Prep Initial Wt./Vol.: 32 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2632
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 05/23/2016 N.C. Certification # 481
Page 56 of 62
Blank Spike ID: LCS for HBN 115463 [XXX/5757]
Blank Spike Lab ID: 201036
Date Analyzed: 05/20/2016 16:50
Results by SW-846 8270D
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)CL
Blank Spike (ug/Kg)
31600936001, 31600936002, 31600936003, 31600936004, 31600936005QC for Samples:
Phenol 3130 3500 112 69.0-116
Bis(2-Chloroethyl)ether 3130 3620 116 58.0-127
2-Chlorophenol 3130 3090 99 70.0-115
1,3-Dichlorobenzene 3130 3020 97 63.0-119
1,4-Dichlorobenzene 3130 3030 97 65.0-119
1,2-Dichlorobenzene 3130 3030 97 66.0-119
2-Methylphenol 3130 3360 108 69.0-118
3 and/or 4-Methylphenol 6250 6920 111 71.0-124
Bis(2-Chloroisopropyl)ether 3130 3060 98 65.0-112
n-Nitrosodi-n-propylamine 3130 3470 111 70.0-112
Hexachloroethane 3130 3090 99 64.0-118
Nitrobenzene 3130 3580 115 70.0-116
Isophorone 3130 3550 114 75.0-118
2-Nitrophenol 3130 3180 102 71.0-116
2,4-Dimethylphenol 3130 3100 99 53.0-122
Bis(2-Chloroethoxy)methane 3130 3530 113 72.0-119
Benzoic acid 3130 ND 42 0.00-114
2,4-Dichlorophenol 3130 3160 101 73.0-120
1,2,4-Trichlorobenzene 3130 3490 112 73.0-124
Naphthalene 3130 3240 104 72.0-116
4-Chloroaniline 3130 2510 80 7.00-126
Hexachlorobutadiene 3130 3100 99 70.0-121
4-Chloro-3-methylphenol 3130 3110 100 72.0-121
2-Methylnaphthalene 3130 3100 99 75.0-120
Hexachlorocyclopentadiene 3130 4870 156*71.0-130
2,4,5-Trichlorophenol 3130 3110 99 76.0-128
2,4,6-Trichlorophenol 3130 3020 97 68.0-119
2-Chloronaphthalene 3130 2670 85 66.0-110
2-Nitroaniline 3130 2600 83 60.0-103
3-Nitroaniline 3130 2390 77 29.0-124
Dimethyl phthalate 3130 2970 95 73.0-121
2,6-Dinitrotoluene 3130 2930 94 74.0-121
Print Date: 05/23/2016 N.C. Certification # 481
Page 57 of 62
Blank Spike ID: LCS for HBN 115463 [XXX/5757]
Blank Spike Lab ID: 201036
Date Analyzed: 05/20/2016 16:50
Results by SW-846 8270D
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)CL
Blank Spike (ug/Kg)
31600936001, 31600936002, 31600936003, 31600936004, 31600936005QC for Samples:
Acenaphthene 3130 2980 95 74.0-118
2,4-Dinitrophenol 3130 1710 55 17.0-125
4-Nitrophenol 3130 3130 100 56.0-133
Dibenzofuran 3130 3000 96 75.0-120
2,4-Dinitrotoluene 3130 3070 98 76.0-122
Fluorene 3130 2960 95 77.0-123
Diethyl phthalate 3130 2930 94 74.0-120
4-Chlorophenyl phenyl ether 3130 3010 96 76.0-125
4-Nitroaniline 3130 2850 91 61.0-112
4,6-Dinitro-2-methylphenol 3130 2430 78 50.0-143
Diphenylamine 3130 3020 97 72.0-124
4-Bromophenyl phenyl ether 3130 3070 98 71.0-130
Hexachlorobenzene 3130 2970 95 71.0-123
Pentachlorophenol 3130 3190 102 32.0-140
Phenanthrene 3130 2970 95 74.0-128
Anthracene 3130 3060 98 73.0-128
Di-n-butyl phthalate 3130 3020 97 75.0-129
Fluoranthene 3130 3020 97 74.0-130
Pyrene 3130 2880 92 74.0-121
Butyl benzyl phthalate 3130 3050 98 73.0-118
Benzo(a)anthracene 3130 2870 92 72.0-123
3,3'-Dichlorobenzidine 3130 2670 86 8.00-158
Chrysene 3130 2920 94 72.0-128
Bis(2-Ethylhexyl)phthalate 3130 2880 92 69.0-125
Di-n-octyl phthalate 3130 3210 103 71.0-121
Benzo(b)fluoranthene 3130 2990 96 63.0-116
Benzo(k)fluoranthene 3130 3410 109 74.0-125
Benzo(a)pyrene 3130 3180 102 71.0-126
Indeno(1,2,3-cd)pyrene 3130 3300 106 76.0-137
Dibenz(a,h)anthracene 3130 3310 106 73.0-138
Benzo(g,h,i)perylene 3130 3330 107 77.0-143
Acenaphthylene 3130 3070 98 75.0-122
Print Date: 05/23/2016 N.C. Certification # 481
Page 58 of 62
Blank Spike ID: LCS for HBN 115463 [XXX/5757]
Blank Spike Lab ID: 201036
Date Analyzed: 05/20/2016 16:50
Results by SW-846 8270D
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)CL
Blank Spike (%)
31600936001, 31600936002, 31600936003, 31600936004, 31600936005QC for Samples:
Surrogates
2-Fluorophenol 114 42.0-123
Phenol-d6 116 48.0-125
Nitrobenzene-d5 122*46.0-117
2-Fluorobiphenyl 103 48.0-123
2,4,6-Tribromophenol 106 41.0-129
Terphenyl-d14 101 44.0-140
Batch Information
Analytical Batch: XMS2632
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX5757
Prep Method: SW-846 3541
Prep Date/Time: 05/19/2016 16:04
Spike Init Wt./Vol.: 32 g Extract Vol: 10 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 05/23/2016 N.C. Certification # 481
Page 59 of 62
Original Sample ID: 31600936002 (UST-2)
MS Sample ID: 201037
MSD Sample ID: 201038
Analysis Date: 05/20/2016 22:41
Analysis Date: 05/20/2016 23:03
Analysis Date: 05/20/2016 23:25
Matrix: Soil-Solid as dry weight
Results by SW-846 8270D
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (ug/Kg)Spike Duplicate (ug/Kg)
CL RPD CL
QC for Samples:31600936001, 31600936002, 31600936003, 31600936004, 31600936005
3,3'-Dichlorobenzidine ND 4425 3590 4469 3510 79 2.181 30.0014.2-302
3-Nitroaniline ND 4425 3840 4469 3770 84 1.987 30.0076.6-356
Batch Information
Analytical Batch: XMS2632
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX5757
Prep Method: SW-846 3541
Prep Date/Time: 05/19/2016 16:04
MS Init Wt./Vol.: 32.88 g Extract Vol.: 10 mL
MSD Init Wt./Vol.: 32.62 g Extract Vol.: 10 mL
Print Date: 05/23/2016 N.C. Certification # 481
Page 60 of 62
Page 61 of 62
Page 62 of 62
Report Number:31601445
Client Project:306007
Laboratory Report of Analysis
Bill Frederick
Highlands Environmental Services
8410 Falls of the Neuse Rd
Raleigh, NC 27615
To:
Dear Bill Frederick,
Enclosed are the results of the analytical services performed under the referenced project for the received
samples and associated QC as applicable. The samples analyzed at the SGS Wilmington location are certified to
meet the requirements of the National Environmental Laboratory Accreditation Conference Standards, unless
otherwise noted. Copies of this report and supporting data will be retained in our files for a period of five years in
the event they are required for future reference. All results are intended to be used in their entirety and SGS is not
responsible for use of less than the complete report. Any samples submitted to our laboratory will be retained for a
maximum of thirty (30) days from the date of this report unless other arrangements are requested.
If there are any questions about the report or services performed during this project, please call Michael D. Page
at [phone]. We will be happy to answer any questions or concerns which you may have.
Thank you for using SGS North America Inc. for your analytical services. We look forward to working with you
again on any additional analytical needs.
Sincerely,
SGS North America Inc.
__________________________________________________________________
Michael D. Page Date
Project Manager
[e-mail]
Print Date: 08/03/2016 N.C. Certification # 481
Terms and Conditions:
All services are rendered in accordance with the applicable SGS General Conditions of Service accessible via:
http://www.sgs.com/terms_and_conditions.htm
Page 1 of 59
Laboratory Qualifiers
Report Definitions
DL Method, Instrument, or Estimated Detection Limit per Analytical Method
CL Control Limits for the recovery result of a parameter
LOQ Reporting Limit
DF Dilution Factor
RPD Relative Percent Difference
LCS(D)Laboratory Control Spike (Duplicate)
MS(D)Matrix Spike (Duplicate)
MB Method Blank
Qualifier Definitions
*Recovery or RPD outside of control limits
B Analyte was detected in the Lab Method Blank at a level above the LOQ
U Undetected (Reported as ND or < DL)
J Estimated Concentration.
E Amount detected is greater than the Upper Calibration Limit
TIC Tentatively Identified Compound
ND Not Detected
P RPD > 40% between results of dual columns
D Spike or surrogate was diluted out in order to achieve a parameter result within instrument calibration
range
Samples requiring manual integrations for various congeners and/or standards are marked and dated by the analyst. A
code definition is provided below:
M1 Mis-identified peak
M2 Software did not integrate peak
M3 Incorrect baseline construction (i.e. not all of peak included; two peaks integrated as one)
M4 Pattern integration required (i.e. DRO, GRO, PCB, Toxaphene and Technical Chlordane)
M5 Other - Explained in case narrative
Note Results pages that include a value for "Solids (%)" have been adjusted for moisture content.
Print Date: 08/03/2016 N.C. Certification # 481
Page 2 of 59
Sample Summary
Client Sample ID Lab Sample ID Collected Received Matrix
UST-7 31601445001 07/20/2016 11:00 07/21/2016 09:50 Soil-Solid as dry weight
UST-8 31601445002 07/20/2016 11:10 07/21/2016 09:50 Soil-Solid as dry weight
UST-9 31601445003 07/20/2016 11:15 07/21/2016 09:50 Soil-Solid as dry weight
UST-10 31601445004 07/20/2016 11:20 07/21/2016 09:50 Soil-Solid as dry weight
UST-11 31601445005 07/20/2016 11:30 07/21/2016 09:50 Soil-Solid as dry weight
Trip Blank 31601445006 07/21/2016 09:50 Soil-Solid as received
Print Date: 08/03/2016 N.C. Certification # 481
Page 3 of 59
Case Narrative
UST-11
8270D: Sample diluted for non-target interference
8260B - VMS4083: Surrogate failures due to sample matrix interactions confirmed by duplicate analysis.
Print Date: 08/03/2016 N.C. Certification # 481
Page 4 of 59
Detectable Results Summary
Client Sample ID: UST-8
Lab Sample ID: 31601445002-A UnitsParameterResult
2-Butanone ug/KgSW-846 8260B 31.5
Acetone ug/Kg99.0
Client Sample ID: UST-9
Lab Sample ID: 31601445003-D UnitsParameterResult
Anthracene ug/KgSW-846 8270D 660
Benzo(a)anthracene ug/Kg2460
Benzo(a)pyrene ug/Kg2090
Benzo(b)fluoranthene ug/Kg3130
Benzo(g,h,i)perylene ug/Kg1100
Benzo(k)fluoranthene ug/Kg1220
Chrysene ug/Kg2880
Fluoranthene ug/Kg5330
Indeno(1,2,3-cd)pyrene ug/Kg1060
Phenanthrene ug/Kg4950
Pyrene ug/Kg4230
Client Sample ID: UST-10
Lab Sample ID: 31601445004-D UnitsParameterResult
Fluoranthene ug/KgSW-846 8270D 735
Pyrene ug/Kg638
Client Sample ID: UST-11
Lab Sample ID: 31601445005-A UnitsParameterResult
1,2,4-Trimethylbenzene ug/KgSW-846 8260B 15.0
4-Isopropyltoluene ug/Kg5.90
Naphthalene ug/Kg60.6
sec-Butylbenzene ug/Kg7.19
Print Date: 08/03/2016 N.C. Certification # 481
Page 5 of 59
Client Sample ID: UST-7
Client Project ID: 306007
Lab Sample ID: 31601445001-A
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:00
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 71.70
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-7
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/Kg 15.23 08/1/2016 18:20
1,1,1-Trichloroethane ND ug/Kg 15.23 08/1/2016 18:20
1,1,2,2-Tetrachloroethane ND ug/Kg 15.23 08/1/2016 18:20
1,1,2-Trichloroethane ND ug/Kg 15.23 08/1/2016 18:20
1,1-Dichloroethane ND ug/Kg 15.23 08/1/2016 18:20
1,1-Dichloroethene ND ug/Kg 15.23 08/1/2016 18:20
1,1-Dichloropropene ND ug/Kg 15.23 08/1/2016 18:20
1,2,3-Trichlorobenzene ND ug/Kg 15.23 08/1/2016 18:20
1,2,3-Trichloropropane ND ug/Kg 15.23 08/1/2016 18:20
1,2,4-Trichlorobenzene ND ug/Kg 15.23 08/1/2016 18:20
1,2,4-Trimethylbenzene ND ug/Kg 15.23 08/1/2016 18:20
1,2-Dibromo-3-chloropropane ND ug/Kg 131.4 08/1/2016 18:20
1,2-Dibromoethane ND ug/Kg 15.23 08/1/2016 18:20
1,2-Dichlorobenzene ND ug/Kg 15.23 08/1/2016 18:20
1,2-Dichloroethane ND ug/Kg 15.23 08/1/2016 18:20
1,2-Dichloropropane ND ug/Kg 15.23 08/1/2016 18:20
1,3,5-Trimethylbenzene ND ug/Kg 15.23 08/1/2016 18:20
1,3-Dichlorobenzene ND ug/Kg 15.23 08/1/2016 18:20
1,3-Dichloropropane ND ug/Kg 15.23 08/1/2016 18:20
1,4-Dichlorobenzene ND ug/Kg 15.23 08/1/2016 18:20
2,2-Dichloropropane ND ug/Kg 15.23 08/1/2016 18:20
2-Butanone ND ug/Kg 126.2 08/1/2016 18:20
2-Chlorotoluene ND ug/Kg 15.23 08/1/2016 18:20
2-Hexanone ND ug/Kg 113.1 08/1/2016 18:20
4-Chlorotoluene ND ug/Kg 15.23 08/1/2016 18:20
4-Isopropyltoluene ND ug/Kg 15.23 08/1/2016 18:20
4-Methyl-2-pentanone ND ug/Kg 113.1 08/1/2016 18:20
Acetone ND ug/Kg 152.3 08/1/2016 18:20
Benzene ND ug/Kg 15.23 08/1/2016 18:20
Bromobenzene ND ug/Kg 15.23 08/1/2016 18:20
Bromochloromethane ND ug/Kg 15.23 08/1/2016 18:20
Bromoform ND ug/Kg 15.23 08/1/2016 18:20
Bromomethane ND ug/Kg 15.23 08/1/2016 18:20
n-Butylbenzene ND ug/Kg 15.23 08/1/2016 18:20
Carbon disulfide ND ug/Kg 15.23 08/1/2016 18:20
Carbon tetrachloride ND ug/Kg 15.23 08/1/2016 18:20
Chlorobenzene ND ug/Kg 15.23 08/1/2016 18:20
Chlorodibromomethane ND ug/Kg 15.23 08/1/2016 18:20
Chloroethane ND ug/Kg 15.23 08/1/2016 18:20
Chloroform ND ug/Kg 15.23 08/1/2016 18:20
Chloromethane ND ug/Kg 15.23 08/1/2016 18:20
Dibromomethane ND ug/Kg 15.23 08/1/2016 18:20
Print Date: 08/03/2016 N.C. Certification # 481
Page 6 of 59
Client Sample ID: UST-7
Client Project ID: 306007
Lab Sample ID: 31601445001-A
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:00
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 71.70
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-7
Date Analyzed
Dichlorobromomethane ND ug/Kg 15.23 08/1/2016 18:20
Dichlorodifluoromethane ND ug/Kg 15.23 08/1/2016 18:20
cis-1,3-Dichloropropene ND ug/Kg 15.23 08/1/2016 18:20
trans-1,3-Dichloropropene ND ug/Kg 15.23 08/1/2016 18:20
Diisopropyl Ether ND ug/Kg 15.23 08/1/2016 18:20
Ethyl Benzene ND ug/Kg 15.23 08/1/2016 18:20
Hexachlorobutadiene ND ug/Kg 15.23 08/1/2016 18:20
Isopropylbenzene (Cumene)ND ug/Kg 15.23 08/1/2016 18:20
Methyl iodide ND ug/Kg 15.23 08/1/2016 18:20
Methylene chloride ND ug/Kg 120.9 08/1/2016 18:20
Naphthalene ND ug/Kg 15.23 08/1/2016 18:20
Styrene ND ug/Kg 15.23 08/1/2016 18:20
Tetrachloroethene ND ug/Kg 15.23 08/1/2016 18:20
Toluene ND ug/Kg 15.23 08/1/2016 18:20
Trichloroethene ND ug/Kg 15.23 08/1/2016 18:20
Trichlorofluoromethane ND ug/Kg 15.23 08/1/2016 18:20
Vinyl chloride ND ug/Kg 15.23 08/1/2016 18:20
Xylene (total)ND ug/Kg 110.5 08/1/2016 18:20
cis-1,2-Dichloroethene ND ug/Kg 15.23 08/1/2016 18:20
m,p-Xylene ND ug/Kg 110.5 08/1/2016 18:20
n-Propylbenzene ND ug/Kg 15.23 08/1/2016 18:20
o-Xylene ND ug/Kg 15.23 08/1/2016 18:20
sec-Butylbenzene ND ug/Kg 15.23 08/1/2016 18:20
tert-Butyl methyl ether (MTBE)ND ug/Kg 15.23 08/1/2016 18:20
tert-Butylbenzene ND ug/Kg 15.23 08/1/2016 18:20
trans-1,2-Dichloroethene ND ug/Kg 15.23 08/1/2016 18:20
trans-1,4-Dichloro-2-butene ND ug/Kg 126.2 08/1/2016 18:20
Surrogates
1,2-Dichloroethane-d4 109 %190.9-137 08/1/2016 18:20
4-Bromofluorobenzene 106 %174.6-125 08/1/2016 18:20
Toluene d8 96.0 %188.8-113 08/1/2016 18:20
Batch Information
Prep Batch: VXX6687
Prep Method: SW-846 5035 SL
Prep Date/Time: 07/21/2016 13:00
Prep Initial Wt./Vol.: 6.66 g
Prep Extract Vol: 5 mL
Analytical Batch: VMS4083
Analytical Method: SW-846 8260B
Instrument: MSD4
Analyst: JHL
Print Date: 08/03/2016 N.C. Certification # 481
Page 7 of 59
Client Sample ID: UST-7
Client Project ID: 306007
Lab Sample ID: 31601445001-D
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:00
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 71.70
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-7
Date Analyzed
1,2,4-Trichlorobenzene ND ug/Kg 1430 07/25/2016 15:39
1,2-Dichlorobenzene ND ug/Kg 1430 07/25/2016 15:39
1,3-Dichlorobenzene ND ug/Kg 1430 07/25/2016 15:39
1,4-Dichlorobenzene ND ug/Kg 1430 07/25/2016 15:39
2,4,5-Trichlorophenol ND ug/Kg 1430 07/25/2016 15:39
2,4,6-Trichlorophenol ND ug/Kg 1430 07/25/2016 15:39
2,4-Dichlorophenol ND ug/Kg 1430 07/25/2016 15:39
2,4-Dinitrophenol ND ug/Kg 12150 07/25/2016 15:39
2,4-Dinitrotoluene ND ug/Kg 1430 07/25/2016 15:39
2,6-Dinitrotoluene ND ug/Kg 1430 07/25/2016 15:39
2-Chloronaphthalene ND ug/Kg 1430 07/25/2016 15:39
2-Chlorophenol ND ug/Kg 1430 07/25/2016 15:39
2-Methylnaphthalene ND ug/Kg 1430 07/25/2016 15:39
2-Methylphenol ND ug/Kg 1430 07/25/2016 15:39
2-Nitroaniline ND ug/Kg 1430 07/25/2016 15:39
2-Nitrophenol ND ug/Kg 1430 07/25/2016 15:39
3 and/or 4-Methylphenol ND ug/Kg 1430 07/25/2016 15:39
3,3'-Dichlorobenzidine ND ug/Kg 1857 08/1/2016 16:09
3-Nitroaniline ND ug/Kg 12150 07/25/2016 15:39
4,6-Dinitro-2-methylphenol ND ug/Kg 12150 07/25/2016 15:39
4-Chloro-3-methylphenol ND ug/Kg 1430 07/25/2016 15:39
4-Chloroaniline ND ug/Kg 1430 07/25/2016 15:39
4-Chlorophenyl phenyl ether ND ug/Kg 1430 07/25/2016 15:39
Acenaphthene ND ug/Kg 1430 07/25/2016 15:39
Acenaphthylene ND ug/Kg 1430 07/25/2016 15:39
Anthracene ND ug/Kg 1430 07/25/2016 15:39
Benzo(a)anthracene ND ug/Kg 1430 07/25/2016 15:39
Benzo(a)pyrene ND ug/Kg 1430 07/25/2016 15:39
Benzo(b)fluoranthene ND ug/Kg 1430 07/25/2016 15:39
Benzo(g,h,i)perylene ND ug/Kg 1430 07/25/2016 15:39
Benzo(k)fluoranthene ND ug/Kg 1430 07/25/2016 15:39
Benzoic acid ND ug/Kg 12150 07/25/2016 15:39
Bis(2-Chloroethoxy)methane ND ug/Kg 1430 07/25/2016 15:39
Bis(2-Chloroethyl)ether ND ug/Kg 1430 07/25/2016 15:39
Bis(2-Chloroisopropyl)ether ND ug/Kg 1430 07/25/2016 15:39
Bis(2-Ethylhexyl)phthalate ND ug/Kg 1430 07/25/2016 15:39
4-Bromophenyl phenyl ether ND ug/Kg 1430 07/25/2016 15:39
Butyl benzyl phthalate ND ug/Kg 1430 07/25/2016 15:39
Chrysene ND ug/Kg 1430 07/25/2016 15:39
Di-n-butyl phthalate ND ug/Kg 1430 07/25/2016 15:39
Di-n-octyl phthalate ND ug/Kg 1430 07/25/2016 15:39
Dibenz(a,h)anthracene ND ug/Kg 1430 07/25/2016 15:39
Print Date: 08/03/2016 N.C. Certification # 481
Page 8 of 59
Client Sample ID: UST-7
Client Project ID: 306007
Lab Sample ID: 31601445001-D
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:00
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 71.70
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-7
Date Analyzed
Dibenzofuran ND ug/Kg 1430 07/25/2016 15:39
Diethyl phthalate ND ug/Kg 1430 07/25/2016 15:39
Dimethyl phthalate ND ug/Kg 1430 07/25/2016 15:39
2,4-Dimethylphenol ND ug/Kg 1430 07/25/2016 15:39
Diphenylamine ND ug/Kg 1430 07/25/2016 15:39
Fluoranthene ND ug/Kg 1430 07/25/2016 15:39
Fluorene ND ug/Kg 1430 07/25/2016 15:39
Hexachlorobenzene ND ug/Kg 12150 07/25/2016 15:39
Hexachlorobutadiene ND ug/Kg 1430 07/25/2016 15:39
Hexachlorocyclopentadiene ND ug/Kg 1860 07/25/2016 15:39
Hexachloroethane ND ug/Kg 1430 07/25/2016 15:39
Indeno(1,2,3-cd)pyrene ND ug/Kg 1430 07/25/2016 15:39
Isophorone ND ug/Kg 1430 07/25/2016 15:39
Naphthalene ND ug/Kg 1430 07/25/2016 15:39
4-Nitroaniline ND ug/Kg 12150 07/25/2016 15:39
Nitrobenzene ND ug/Kg 1430 07/25/2016 15:39
4-Nitrophenol ND ug/Kg 12150 07/25/2016 15:39
Pentachlorophenol ND ug/Kg 12150 07/25/2016 15:39
Phenanthrene ND ug/Kg 1430 07/25/2016 15:39
Phenol ND ug/Kg 1430 07/25/2016 15:39
Pyrene ND ug/Kg 1430 07/25/2016 15:39
n-Nitrosodi-n-propylamine ND ug/Kg 1430 07/25/2016 15:39
Surrogates
2,4,6-Tribromophenol 73.0 %141.0-129 07/25/2016 15:39
2-Fluorobiphenyl 75.0 %148.0-123 07/25/2016 15:39
2-Fluorophenol 84.0 %142.0-123 07/25/2016 15:39
Nitrobenzene-d5 77.0 %146.0-117 07/25/2016 15:39
Phenol-d6 86.0 %148.0-125 07/25/2016 15:39
Terphenyl-d14 75.0 %144.0-140 07/25/2016 15:39
Print Date: 08/03/2016 N.C. Certification # 481
Page 9 of 59
Client Sample ID: UST-7
Client Project ID: 306007
Lab Sample ID: 31601445001-D
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:00
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 71.70
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-7
Date Analyzed
Batch Information
Prep Batch: XXX5904
Prep Method: SW-846 3541
Prep Date/Time: 07/21/2016 16:30
Prep Initial Wt./Vol.: 32.47 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2678
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX5925
Prep Method: SW-846 3541
Prep Date/Time: 08/01/2016 12:40
Prep Initial Wt./Vol.: 32.6 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2680
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 08/03/2016 N.C. Certification # 481
Page 10 of 59
Client Sample ID: UST-8
Client Project ID: 306007
Lab Sample ID: 31601445002-A
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:10
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 72.80
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-8
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/Kg 15.67 08/1/2016 17:51
1,1,1-Trichloroethane ND ug/Kg 15.67 08/1/2016 17:51
1,1,2,2-Tetrachloroethane ND ug/Kg 15.67 08/1/2016 17:51
1,1,2-Trichloroethane ND ug/Kg 15.67 08/1/2016 17:51
1,1-Dichloroethane ND ug/Kg 15.67 08/1/2016 17:51
1,1-Dichloroethene ND ug/Kg 15.67 08/1/2016 17:51
1,1-Dichloropropene ND ug/Kg 15.67 08/1/2016 17:51
1,2,3-Trichlorobenzene ND ug/Kg 15.67 08/1/2016 17:51
1,2,3-Trichloropropane ND ug/Kg 15.67 08/1/2016 17:51
1,2,4-Trichlorobenzene ND ug/Kg 15.67 08/1/2016 17:51
1,2,4-Trimethylbenzene ND ug/Kg 15.67 08/1/2016 17:51
1,2-Dibromo-3-chloropropane ND ug/Kg 134.0 08/1/2016 17:51
1,2-Dibromoethane ND ug/Kg 15.67 08/1/2016 17:51
1,2-Dichlorobenzene ND ug/Kg 15.67 08/1/2016 17:51
1,2-Dichloroethane ND ug/Kg 15.67 08/1/2016 17:51
1,2-Dichloropropane ND ug/Kg 15.67 08/1/2016 17:51
1,3,5-Trimethylbenzene ND ug/Kg 15.67 08/1/2016 17:51
1,3-Dichlorobenzene ND ug/Kg 15.67 08/1/2016 17:51
1,3-Dichloropropane ND ug/Kg 15.67 08/1/2016 17:51
1,4-Dichlorobenzene ND ug/Kg 15.67 08/1/2016 17:51
2,2-Dichloropropane ND ug/Kg 15.67 08/1/2016 17:51
2-Butanone 31.5 ug/Kg 128.4 08/1/2016 17:51
2-Chlorotoluene ND ug/Kg 15.67 08/1/2016 17:51
2-Hexanone ND ug/Kg 114.2 08/1/2016 17:51
4-Chlorotoluene ND ug/Kg 15.67 08/1/2016 17:51
4-Isopropyltoluene ND ug/Kg 15.67 08/1/2016 17:51
4-Methyl-2-pentanone ND ug/Kg 114.2 08/1/2016 17:51
Acetone 99.0 ug/Kg 156.7 08/1/2016 17:51
Benzene ND ug/Kg 15.67 08/1/2016 17:51
Bromobenzene ND ug/Kg 15.67 08/1/2016 17:51
Bromochloromethane ND ug/Kg 15.67 08/1/2016 17:51
Bromoform ND ug/Kg 15.67 08/1/2016 17:51
Bromomethane ND ug/Kg 15.67 08/1/2016 17:51
n-Butylbenzene ND ug/Kg 15.67 08/1/2016 17:51
Carbon disulfide ND ug/Kg 15.67 08/1/2016 17:51
Carbon tetrachloride ND ug/Kg 15.67 08/1/2016 17:51
Chlorobenzene ND ug/Kg 15.67 08/1/2016 17:51
Chlorodibromomethane ND ug/Kg 15.67 08/1/2016 17:51
Chloroethane ND ug/Kg 15.67 08/1/2016 17:51
Chloroform ND ug/Kg 15.67 08/1/2016 17:51
Chloromethane ND ug/Kg 15.67 08/1/2016 17:51
Dibromomethane ND ug/Kg 15.67 08/1/2016 17:51
Print Date: 08/03/2016 N.C. Certification # 481
Page 11 of 59
Client Sample ID: UST-8
Client Project ID: 306007
Lab Sample ID: 31601445002-A
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:10
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 72.80
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-8
Date Analyzed
Dichlorobromomethane ND ug/Kg 15.67 08/1/2016 17:51
Dichlorodifluoromethane ND ug/Kg 15.67 08/1/2016 17:51
cis-1,3-Dichloropropene ND ug/Kg 15.67 08/1/2016 17:51
trans-1,3-Dichloropropene ND ug/Kg 15.67 08/1/2016 17:51
Diisopropyl Ether ND ug/Kg 15.67 08/1/2016 17:51
Ethyl Benzene ND ug/Kg 15.67 08/1/2016 17:51
Hexachlorobutadiene ND ug/Kg 15.67 08/1/2016 17:51
Isopropylbenzene (Cumene)ND ug/Kg 15.67 08/1/2016 17:51
Methyl iodide ND ug/Kg 15.67 08/1/2016 17:51
Methylene chloride ND ug/Kg 122.7 08/1/2016 17:51
Naphthalene ND ug/Kg 15.67 08/1/2016 17:51
Styrene ND ug/Kg 15.67 08/1/2016 17:51
Tetrachloroethene ND ug/Kg 15.67 08/1/2016 17:51
Toluene ND ug/Kg 15.67 08/1/2016 17:51
Trichloroethene ND ug/Kg 15.67 08/1/2016 17:51
Trichlorofluoromethane ND ug/Kg 15.67 08/1/2016 17:51
Vinyl chloride ND ug/Kg 15.67 08/1/2016 17:51
Xylene (total)ND ug/Kg 111.3 08/1/2016 17:51
cis-1,2-Dichloroethene ND ug/Kg 15.67 08/1/2016 17:51
m,p-Xylene ND ug/Kg 111.3 08/1/2016 17:51
n-Propylbenzene ND ug/Kg 15.67 08/1/2016 17:51
o-Xylene ND ug/Kg 15.67 08/1/2016 17:51
sec-Butylbenzene ND ug/Kg 15.67 08/1/2016 17:51
tert-Butyl methyl ether (MTBE)ND ug/Kg 15.67 08/1/2016 17:51
tert-Butylbenzene ND ug/Kg 15.67 08/1/2016 17:51
trans-1,2-Dichloroethene ND ug/Kg 15.67 08/1/2016 17:51
trans-1,4-Dichloro-2-butene ND ug/Kg 128.4 08/1/2016 17:51
Surrogates
1,2-Dichloroethane-d4 107 %190.9-137 08/1/2016 17:51
4-Bromofluorobenzene 104 %174.6-125 08/1/2016 17:51
Toluene d8 95.0 %188.8-113 08/1/2016 17:51
Batch Information
Prep Batch: VXX6687
Prep Method: SW-846 5035 SL
Prep Date/Time: 07/21/2016 13:00
Prep Initial Wt./Vol.: 6.05 g
Prep Extract Vol: 5 mL
Analytical Batch: VMS4083
Analytical Method: SW-846 8260B
Instrument: MSD4
Analyst: JHL
Print Date: 08/03/2016 N.C. Certification # 481
Page 12 of 59
Client Sample ID: UST-8
Client Project ID: 306007
Lab Sample ID: 31601445002-D
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:10
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 72.80
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-8
Date Analyzed
1,2,4-Trichlorobenzene ND ug/Kg 1421 07/25/2016 16:44
1,2-Dichlorobenzene ND ug/Kg 1421 07/25/2016 16:44
1,3-Dichlorobenzene ND ug/Kg 1421 07/25/2016 16:44
1,4-Dichlorobenzene ND ug/Kg 1421 07/25/2016 16:44
2,4,5-Trichlorophenol ND ug/Kg 1421 07/25/2016 16:44
2,4,6-Trichlorophenol ND ug/Kg 1421 07/25/2016 16:44
2,4-Dichlorophenol ND ug/Kg 1421 07/25/2016 16:44
2,4-Dinitrophenol ND ug/Kg 12100 07/25/2016 16:44
2,4-Dinitrotoluene ND ug/Kg 1421 07/25/2016 16:44
2,6-Dinitrotoluene ND ug/Kg 1421 07/25/2016 16:44
2-Chloronaphthalene ND ug/Kg 1421 07/25/2016 16:44
2-Chlorophenol ND ug/Kg 1421 07/25/2016 16:44
2-Methylnaphthalene ND ug/Kg 1421 07/25/2016 16:44
2-Methylphenol ND ug/Kg 1421 07/25/2016 16:44
2-Nitroaniline ND ug/Kg 1421 07/25/2016 16:44
2-Nitrophenol ND ug/Kg 1421 07/25/2016 16:44
3 and/or 4-Methylphenol ND ug/Kg 1421 07/25/2016 16:44
3,3'-Dichlorobenzidine ND ug/Kg 1824 08/1/2016 16:31
3-Nitroaniline ND ug/Kg 12100 07/25/2016 16:44
4,6-Dinitro-2-methylphenol ND ug/Kg 12100 07/25/2016 16:44
4-Chloro-3-methylphenol ND ug/Kg 1421 07/25/2016 16:44
4-Chloroaniline ND ug/Kg 1421 07/25/2016 16:44
4-Chlorophenyl phenyl ether ND ug/Kg 1421 07/25/2016 16:44
Acenaphthene ND ug/Kg 1421 07/25/2016 16:44
Acenaphthylene ND ug/Kg 1421 07/25/2016 16:44
Anthracene ND ug/Kg 1421 07/25/2016 16:44
Benzo(a)anthracene ND ug/Kg 1421 07/25/2016 16:44
Benzo(a)pyrene ND ug/Kg 1421 07/25/2016 16:44
Benzo(b)fluoranthene ND ug/Kg 1421 07/25/2016 16:44
Benzo(g,h,i)perylene ND ug/Kg 1421 07/25/2016 16:44
Benzo(k)fluoranthene ND ug/Kg 1421 07/25/2016 16:44
Benzoic acid ND ug/Kg 12100 07/25/2016 16:44
Bis(2-Chloroethoxy)methane ND ug/Kg 1421 07/25/2016 16:44
Bis(2-Chloroethyl)ether ND ug/Kg 1421 07/25/2016 16:44
Bis(2-Chloroisopropyl)ether ND ug/Kg 1421 07/25/2016 16:44
Bis(2-Ethylhexyl)phthalate ND ug/Kg 1421 07/25/2016 16:44
4-Bromophenyl phenyl ether ND ug/Kg 1421 07/25/2016 16:44
Butyl benzyl phthalate ND ug/Kg 1421 07/25/2016 16:44
Chrysene ND ug/Kg 1421 07/25/2016 16:44
Di-n-butyl phthalate ND ug/Kg 1421 07/25/2016 16:44
Di-n-octyl phthalate ND ug/Kg 1421 07/25/2016 16:44
Dibenz(a,h)anthracene ND ug/Kg 1421 07/25/2016 16:44
Print Date: 08/03/2016 N.C. Certification # 481
Page 13 of 59
Client Sample ID: UST-8
Client Project ID: 306007
Lab Sample ID: 31601445002-D
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:10
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 72.80
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-8
Date Analyzed
Dibenzofuran ND ug/Kg 1421 07/25/2016 16:44
Diethyl phthalate ND ug/Kg 1421 07/25/2016 16:44
Dimethyl phthalate ND ug/Kg 1421 07/25/2016 16:44
2,4-Dimethylphenol ND ug/Kg 1421 07/25/2016 16:44
Diphenylamine ND ug/Kg 1421 07/25/2016 16:44
Fluoranthene ND ug/Kg 1421 07/25/2016 16:44
Fluorene ND ug/Kg 1421 07/25/2016 16:44
Hexachlorobenzene ND ug/Kg 12100 07/25/2016 16:44
Hexachlorobutadiene ND ug/Kg 1421 07/25/2016 16:44
Hexachlorocyclopentadiene ND ug/Kg 1842 07/25/2016 16:44
Hexachloroethane ND ug/Kg 1421 07/25/2016 16:44
Indeno(1,2,3-cd)pyrene ND ug/Kg 1421 07/25/2016 16:44
Isophorone ND ug/Kg 1421 07/25/2016 16:44
Naphthalene ND ug/Kg 1421 07/25/2016 16:44
4-Nitroaniline ND ug/Kg 12100 07/25/2016 16:44
Nitrobenzene ND ug/Kg 1421 07/25/2016 16:44
4-Nitrophenol ND ug/Kg 12100 07/25/2016 16:44
Pentachlorophenol ND ug/Kg 12100 07/25/2016 16:44
Phenanthrene ND ug/Kg 1421 07/25/2016 16:44
Phenol ND ug/Kg 1421 07/25/2016 16:44
Pyrene ND ug/Kg 1421 07/25/2016 16:44
n-Nitrosodi-n-propylamine ND ug/Kg 1421 07/25/2016 16:44
Surrogates
2,4,6-Tribromophenol 76.0 %141.0-129 07/25/2016 16:44
2-Fluorobiphenyl 74.0 %148.0-123 07/25/2016 16:44
2-Fluorophenol 81.0 %142.0-123 07/25/2016 16:44
Nitrobenzene-d5 74.0 %146.0-117 07/25/2016 16:44
Phenol-d6 84.0 %148.0-125 07/25/2016 16:44
Terphenyl-d14 74.0 %144.0-140 07/25/2016 16:44
Print Date: 08/03/2016 N.C. Certification # 481
Page 14 of 59
Client Sample ID: UST-8
Client Project ID: 306007
Lab Sample ID: 31601445002-D
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:10
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 72.80
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-8
Date Analyzed
Batch Information
Prep Batch: XXX5904
Prep Method: SW-846 3541
Prep Date/Time: 07/21/2016 16:30
Prep Initial Wt./Vol.: 32.67 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2678
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX5925
Prep Method: SW-846 3541
Prep Date/Time: 08/01/2016 12:40
Prep Initial Wt./Vol.: 33.37 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2680
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 08/03/2016 N.C. Certification # 481
Page 15 of 59
Client Sample ID: UST-9
Client Project ID: 306007
Lab Sample ID: 31601445003-A
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:15
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 76.20
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-9
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/Kg 16.45 08/1/2016 17:23
1,1,1-Trichloroethane ND ug/Kg 16.45 08/1/2016 17:23
1,1,2,2-Tetrachloroethane ND ug/Kg 16.45 08/1/2016 17:23
1,1,2-Trichloroethane ND ug/Kg 16.45 08/1/2016 17:23
1,1-Dichloroethane ND ug/Kg 16.45 08/1/2016 17:23
1,1-Dichloroethene ND ug/Kg 16.45 08/1/2016 17:23
1,1-Dichloropropene ND ug/Kg 16.45 08/1/2016 17:23
1,2,3-Trichlorobenzene ND ug/Kg 16.45 08/1/2016 17:23
1,2,3-Trichloropropane ND ug/Kg 16.45 08/1/2016 17:23
1,2,4-Trichlorobenzene ND ug/Kg 16.45 08/1/2016 17:23
1,2,4-Trimethylbenzene ND ug/Kg 16.45 08/1/2016 17:23
1,2-Dibromo-3-chloropropane ND ug/Kg 138.7 08/1/2016 17:23
1,2-Dibromoethane ND ug/Kg 16.45 08/1/2016 17:23
1,2-Dichlorobenzene ND ug/Kg 16.45 08/1/2016 17:23
1,2-Dichloroethane ND ug/Kg 16.45 08/1/2016 17:23
1,2-Dichloropropane ND ug/Kg 16.45 08/1/2016 17:23
1,3,5-Trimethylbenzene ND ug/Kg 16.45 08/1/2016 17:23
1,3-Dichlorobenzene ND ug/Kg 16.45 08/1/2016 17:23
1,3-Dichloropropane ND ug/Kg 16.45 08/1/2016 17:23
1,4-Dichlorobenzene ND ug/Kg 16.45 08/1/2016 17:23
2,2-Dichloropropane ND ug/Kg 16.45 08/1/2016 17:23
2-Butanone ND ug/Kg 132.2 08/1/2016 17:23
2-Chlorotoluene ND ug/Kg 16.45 08/1/2016 17:23
2-Hexanone ND ug/Kg 116.1 08/1/2016 17:23
4-Chlorotoluene ND ug/Kg 16.45 08/1/2016 17:23
4-Isopropyltoluene ND ug/Kg 16.45 08/1/2016 17:23
4-Methyl-2-pentanone ND ug/Kg 116.1 08/1/2016 17:23
Acetone ND ug/Kg 164.5 08/1/2016 17:23
Benzene ND ug/Kg 16.45 08/1/2016 17:23
Bromobenzene ND ug/Kg 16.45 08/1/2016 17:23
Bromochloromethane ND ug/Kg 16.45 08/1/2016 17:23
Bromoform ND ug/Kg 16.45 08/1/2016 17:23
Bromomethane ND ug/Kg 16.45 08/1/2016 17:23
n-Butylbenzene ND ug/Kg 16.45 08/1/2016 17:23
Carbon disulfide ND ug/Kg 16.45 08/1/2016 17:23
Carbon tetrachloride ND ug/Kg 16.45 08/1/2016 17:23
Chlorobenzene ND ug/Kg 16.45 08/1/2016 17:23
Chlorodibromomethane ND ug/Kg 16.45 08/1/2016 17:23
Chloroethane ND ug/Kg 16.45 08/1/2016 17:23
Chloroform ND ug/Kg 16.45 08/1/2016 17:23
Chloromethane ND ug/Kg 16.45 08/1/2016 17:23
Dibromomethane ND ug/Kg 16.45 08/1/2016 17:23
Print Date: 08/03/2016 N.C. Certification # 481
Page 16 of 59
Client Sample ID: UST-9
Client Project ID: 306007
Lab Sample ID: 31601445003-A
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:15
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 76.20
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-9
Date Analyzed
Dichlorobromomethane ND ug/Kg 16.45 08/1/2016 17:23
Dichlorodifluoromethane ND ug/Kg 16.45 08/1/2016 17:23
cis-1,3-Dichloropropene ND ug/Kg 16.45 08/1/2016 17:23
trans-1,3-Dichloropropene ND ug/Kg 16.45 08/1/2016 17:23
Diisopropyl Ether ND ug/Kg 16.45 08/1/2016 17:23
Ethyl Benzene ND ug/Kg 16.45 08/1/2016 17:23
Hexachlorobutadiene ND ug/Kg 16.45 08/1/2016 17:23
Isopropylbenzene (Cumene)ND ug/Kg 16.45 08/1/2016 17:23
Methyl iodide ND ug/Kg 16.45 08/1/2016 17:23
Methylene chloride ND ug/Kg 125.8 08/1/2016 17:23
Naphthalene ND ug/Kg 16.45 08/1/2016 17:23
Styrene ND ug/Kg 16.45 08/1/2016 17:23
Tetrachloroethene ND ug/Kg 16.45 08/1/2016 17:23
Toluene ND ug/Kg 16.45 08/1/2016 17:23
Trichloroethene ND ug/Kg 16.45 08/1/2016 17:23
Trichlorofluoromethane ND ug/Kg 16.45 08/1/2016 17:23
Vinyl chloride ND ug/Kg 16.45 08/1/2016 17:23
Xylene (total)ND ug/Kg 112.9 08/1/2016 17:23
cis-1,2-Dichloroethene ND ug/Kg 16.45 08/1/2016 17:23
m,p-Xylene ND ug/Kg 112.9 08/1/2016 17:23
n-Propylbenzene ND ug/Kg 16.45 08/1/2016 17:23
o-Xylene ND ug/Kg 16.45 08/1/2016 17:23
sec-Butylbenzene ND ug/Kg 16.45 08/1/2016 17:23
tert-Butyl methyl ether (MTBE)ND ug/Kg 16.45 08/1/2016 17:23
tert-Butylbenzene ND ug/Kg 16.45 08/1/2016 17:23
trans-1,2-Dichloroethene ND ug/Kg 16.45 08/1/2016 17:23
trans-1,4-Dichloro-2-butene ND ug/Kg 132.2 08/1/2016 17:23
Surrogates
1,2-Dichloroethane-d4 107 %190.9-137 08/1/2016 17:23
4-Bromofluorobenzene 106 %174.6-125 08/1/2016 17:23
Toluene d8 96.0 %188.8-113 08/1/2016 17:23
Batch Information
Prep Batch: VXX6687
Prep Method: SW-846 5035 SL
Prep Date/Time: 07/21/2016 13:00
Prep Initial Wt./Vol.: 5.09 g
Prep Extract Vol: 5 mL
Analytical Batch: VMS4083
Analytical Method: SW-846 8260B
Instrument: MSD4
Analyst: JHL
Print Date: 08/03/2016 N.C. Certification # 481
Page 17 of 59
Client Sample ID: UST-9
Client Project ID: 306007
Lab Sample ID: 31601445003-D
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:15
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 76.20
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-9
Date Analyzed
1,2,4-Trichlorobenzene ND ug/Kg 1403 07/25/2016 17:06
1,2-Dichlorobenzene ND ug/Kg 1403 07/25/2016 17:06
1,3-Dichlorobenzene ND ug/Kg 1403 07/25/2016 17:06
1,4-Dichlorobenzene ND ug/Kg 1403 07/25/2016 17:06
2,4,5-Trichlorophenol ND ug/Kg 1403 07/25/2016 17:06
2,4,6-Trichlorophenol ND ug/Kg 1403 07/25/2016 17:06
2,4-Dichlorophenol ND ug/Kg 1403 07/25/2016 17:06
2,4-Dinitrophenol ND ug/Kg 12020 07/25/2016 17:06
2,4-Dinitrotoluene ND ug/Kg 1403 07/25/2016 17:06
2,6-Dinitrotoluene ND ug/Kg 1403 07/25/2016 17:06
2-Chloronaphthalene ND ug/Kg 1403 07/25/2016 17:06
2-Chlorophenol ND ug/Kg 1403 07/25/2016 17:06
2-Methylnaphthalene ND ug/Kg 1403 07/25/2016 17:06
2-Methylphenol ND ug/Kg 1403 07/25/2016 17:06
2-Nitroaniline ND ug/Kg 1403 07/25/2016 17:06
2-Nitrophenol ND ug/Kg 1403 07/25/2016 17:06
3 and/or 4-Methylphenol ND ug/Kg 1403 07/25/2016 17:06
3,3'-Dichlorobenzidine ND ug/Kg 1819 08/1/2016 16:53
3-Nitroaniline ND ug/Kg 12020 07/25/2016 17:06
4,6-Dinitro-2-methylphenol ND ug/Kg 12020 07/25/2016 17:06
4-Chloro-3-methylphenol ND ug/Kg 1403 07/25/2016 17:06
4-Chloroaniline ND ug/Kg 1403 07/25/2016 17:06
4-Chlorophenyl phenyl ether ND ug/Kg 1403 07/25/2016 17:06
Acenaphthene ND ug/Kg 1403 07/25/2016 17:06
Acenaphthylene ND ug/Kg 1403 07/25/2016 17:06
Anthracene 660 ug/Kg 1403 07/25/2016 17:06
Benzo(a)anthracene 2460 ug/Kg 1403 07/25/2016 17:06
Benzo(a)pyrene 2090 ug/Kg 1403 07/25/2016 17:06
Benzo(b)fluoranthene 3130 ug/Kg 1403 07/25/2016 17:06
Benzo(g,h,i)perylene 1100 ug/Kg 1403 07/25/2016 17:06
Benzo(k)fluoranthene 1220 ug/Kg 1403 07/25/2016 17:06
Benzoic acid ND ug/Kg 12020 07/25/2016 17:06
Bis(2-Chloroethoxy)methane ND ug/Kg 1403 07/25/2016 17:06
Bis(2-Chloroethyl)ether ND ug/Kg 1403 07/25/2016 17:06
Bis(2-Chloroisopropyl)ether ND ug/Kg 1403 07/25/2016 17:06
Bis(2-Ethylhexyl)phthalate ND ug/Kg 1403 07/25/2016 17:06
4-Bromophenyl phenyl ether ND ug/Kg 1403 07/25/2016 17:06
Butyl benzyl phthalate ND ug/Kg 1403 07/25/2016 17:06
Chrysene 2880 ug/Kg 1403 07/25/2016 17:06
Di-n-butyl phthalate ND ug/Kg 1403 07/25/2016 17:06
Di-n-octyl phthalate ND ug/Kg 1403 07/25/2016 17:06
Dibenz(a,h)anthracene ND ug/Kg 1403 07/25/2016 17:06
Print Date: 08/03/2016 N.C. Certification # 481
Page 18 of 59
Client Sample ID: UST-9
Client Project ID: 306007
Lab Sample ID: 31601445003-D
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:15
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 76.20
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-9
Date Analyzed
Dibenzofuran ND ug/Kg 1403 07/25/2016 17:06
Diethyl phthalate ND ug/Kg 1403 07/25/2016 17:06
Dimethyl phthalate ND ug/Kg 1403 07/25/2016 17:06
2,4-Dimethylphenol ND ug/Kg 1403 07/25/2016 17:06
Diphenylamine ND ug/Kg 1403 07/25/2016 17:06
Fluoranthene 5330 ug/Kg 1403 07/25/2016 17:06
Fluorene ND ug/Kg 1403 07/25/2016 17:06
Hexachlorobenzene ND ug/Kg 12020 07/25/2016 17:06
Hexachlorobutadiene ND ug/Kg 1403 07/25/2016 17:06
Hexachlorocyclopentadiene ND ug/Kg 1807 07/25/2016 17:06
Hexachloroethane ND ug/Kg 1403 07/25/2016 17:06
Indeno(1,2,3-cd)pyrene 1060 ug/Kg 1403 07/25/2016 17:06
Isophorone ND ug/Kg 1403 07/25/2016 17:06
Naphthalene ND ug/Kg 1403 07/25/2016 17:06
4-Nitroaniline ND ug/Kg 12020 07/25/2016 17:06
Nitrobenzene ND ug/Kg 1403 07/25/2016 17:06
4-Nitrophenol ND ug/Kg 12020 07/25/2016 17:06
Pentachlorophenol ND ug/Kg 12020 07/25/2016 17:06
Phenanthrene 4950 ug/Kg 1403 07/25/2016 17:06
Phenol ND ug/Kg 1403 07/25/2016 17:06
Pyrene 4230 ug/Kg 1403 07/25/2016 17:06
n-Nitrosodi-n-propylamine ND ug/Kg 1403 07/25/2016 17:06
Surrogates
2,4,6-Tribromophenol 93.0 %141.0-129 07/25/2016 17:06
2-Fluorobiphenyl 84.0 %148.0-123 07/25/2016 17:06
2-Fluorophenol 85.0 %142.0-123 07/25/2016 17:06
Nitrobenzene-d5 86.0 %146.0-117 07/25/2016 17:06
Phenol-d6 93.0 %148.0-125 07/25/2016 17:06
Terphenyl-d14 81.0 %144.0-140 07/25/2016 17:06
Print Date: 08/03/2016 N.C. Certification # 481
Page 19 of 59
Client Sample ID: UST-9
Client Project ID: 306007
Lab Sample ID: 31601445003-D
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:15
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 76.20
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-9
Date Analyzed
Batch Information
Prep Batch: XXX5904
Prep Method: SW-846 3541
Prep Date/Time: 07/21/2016 16:30
Prep Initial Wt./Vol.: 32.59 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2678
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX5925
Prep Method: SW-846 3541
Prep Date/Time: 08/01/2016 12:40
Prep Initial Wt./Vol.: 32.11 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2680
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 08/03/2016 N.C. Certification # 481
Page 20 of 59
Client Sample ID: UST-10
Client Project ID: 306007
Lab Sample ID: 31601445004-A
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:20
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 75.70
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-10
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/Kg 15.34 08/1/2016 16:55
1,1,1-Trichloroethane ND ug/Kg 15.34 08/1/2016 16:55
1,1,2,2-Tetrachloroethane ND ug/Kg 15.34 08/1/2016 16:55
1,1,2-Trichloroethane ND ug/Kg 15.34 08/1/2016 16:55
1,1-Dichloroethane ND ug/Kg 15.34 08/1/2016 16:55
1,1-Dichloroethene ND ug/Kg 15.34 08/1/2016 16:55
1,1-Dichloropropene ND ug/Kg 15.34 08/1/2016 16:55
1,2,3-Trichlorobenzene ND ug/Kg 15.34 08/1/2016 16:55
1,2,3-Trichloropropane ND ug/Kg 15.34 08/1/2016 16:55
1,2,4-Trichlorobenzene ND ug/Kg 15.34 08/1/2016 16:55
1,2,4-Trimethylbenzene ND ug/Kg 15.34 08/1/2016 16:55
1,2-Dibromo-3-chloropropane ND ug/Kg 132.0 08/1/2016 16:55
1,2-Dibromoethane ND ug/Kg 15.34 08/1/2016 16:55
1,2-Dichlorobenzene ND ug/Kg 15.34 08/1/2016 16:55
1,2-Dichloroethane ND ug/Kg 15.34 08/1/2016 16:55
1,2-Dichloropropane ND ug/Kg 15.34 08/1/2016 16:55
1,3,5-Trimethylbenzene ND ug/Kg 15.34 08/1/2016 16:55
1,3-Dichlorobenzene ND ug/Kg 15.34 08/1/2016 16:55
1,3-Dichloropropane ND ug/Kg 15.34 08/1/2016 16:55
1,4-Dichlorobenzene ND ug/Kg 15.34 08/1/2016 16:55
2,2-Dichloropropane ND ug/Kg 15.34 08/1/2016 16:55
2-Butanone ND ug/Kg 126.7 08/1/2016 16:55
2-Chlorotoluene ND ug/Kg 15.34 08/1/2016 16:55
2-Hexanone ND ug/Kg 113.4 08/1/2016 16:55
4-Chlorotoluene ND ug/Kg 15.34 08/1/2016 16:55
4-Isopropyltoluene ND ug/Kg 15.34 08/1/2016 16:55
4-Methyl-2-pentanone ND ug/Kg 113.4 08/1/2016 16:55
Acetone ND ug/Kg 153.4 08/1/2016 16:55
Benzene ND ug/Kg 15.34 08/1/2016 16:55
Bromobenzene ND ug/Kg 15.34 08/1/2016 16:55
Bromochloromethane ND ug/Kg 15.34 08/1/2016 16:55
Bromoform ND ug/Kg 15.34 08/1/2016 16:55
Bromomethane ND ug/Kg 15.34 08/1/2016 16:55
n-Butylbenzene ND ug/Kg 15.34 08/1/2016 16:55
Carbon disulfide ND ug/Kg 15.34 08/1/2016 16:55
Carbon tetrachloride ND ug/Kg 15.34 08/1/2016 16:55
Chlorobenzene ND ug/Kg 15.34 08/1/2016 16:55
Chlorodibromomethane ND ug/Kg 15.34 08/1/2016 16:55
Chloroethane ND ug/Kg 15.34 08/1/2016 16:55
Chloroform ND ug/Kg 15.34 08/1/2016 16:55
Chloromethane ND ug/Kg 15.34 08/1/2016 16:55
Dibromomethane ND ug/Kg 15.34 08/1/2016 16:55
Print Date: 08/03/2016 N.C. Certification # 481
Page 21 of 59
Client Sample ID: UST-10
Client Project ID: 306007
Lab Sample ID: 31601445004-A
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:20
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 75.70
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-10
Date Analyzed
Dichlorobromomethane ND ug/Kg 15.34 08/1/2016 16:55
Dichlorodifluoromethane ND ug/Kg 15.34 08/1/2016 16:55
cis-1,3-Dichloropropene ND ug/Kg 15.34 08/1/2016 16:55
trans-1,3-Dichloropropene ND ug/Kg 15.34 08/1/2016 16:55
Diisopropyl Ether ND ug/Kg 15.34 08/1/2016 16:55
Ethyl Benzene ND ug/Kg 15.34 08/1/2016 16:55
Hexachlorobutadiene ND ug/Kg 15.34 08/1/2016 16:55
Isopropylbenzene (Cumene)ND ug/Kg 15.34 08/1/2016 16:55
Methyl iodide ND ug/Kg 15.34 08/1/2016 16:55
Methylene chloride ND ug/Kg 121.4 08/1/2016 16:55
Naphthalene ND ug/Kg 15.34 08/1/2016 16:55
Styrene ND ug/Kg 15.34 08/1/2016 16:55
Tetrachloroethene ND ug/Kg 15.34 08/1/2016 16:55
Toluene ND ug/Kg 15.34 08/1/2016 16:55
Trichloroethene ND ug/Kg 15.34 08/1/2016 16:55
Trichlorofluoromethane ND ug/Kg 15.34 08/1/2016 16:55
Vinyl chloride ND ug/Kg 15.34 08/1/2016 16:55
Xylene (total)ND ug/Kg 110.7 08/1/2016 16:55
cis-1,2-Dichloroethene ND ug/Kg 15.34 08/1/2016 16:55
m,p-Xylene ND ug/Kg 110.7 08/1/2016 16:55
n-Propylbenzene ND ug/Kg 15.34 08/1/2016 16:55
o-Xylene ND ug/Kg 15.34 08/1/2016 16:55
sec-Butylbenzene ND ug/Kg 15.34 08/1/2016 16:55
tert-Butyl methyl ether (MTBE)ND ug/Kg 15.34 08/1/2016 16:55
tert-Butylbenzene ND ug/Kg 15.34 08/1/2016 16:55
trans-1,2-Dichloroethene ND ug/Kg 15.34 08/1/2016 16:55
trans-1,4-Dichloro-2-butene ND ug/Kg 126.7 08/1/2016 16:55
Surrogates
1,2-Dichloroethane-d4 109 %190.9-137 08/1/2016 16:55
4-Bromofluorobenzene 105 %174.6-125 08/1/2016 16:55
Toluene d8 96.0 %188.8-113 08/1/2016 16:55
Batch Information
Prep Batch: VXX6687
Prep Method: SW-846 5035 SL
Prep Date/Time: 07/21/2016 13:00
Prep Initial Wt./Vol.: 6.18 g
Prep Extract Vol: 5 mL
Analytical Batch: VMS4083
Analytical Method: SW-846 8260B
Instrument: MSD4
Analyst: JHL
Print Date: 08/03/2016 N.C. Certification # 481
Page 22 of 59
Client Sample ID: UST-10
Client Project ID: 306007
Lab Sample ID: 31601445004-D
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:20
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 75.70
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-10
Date Analyzed
1,2,4-Trichlorobenzene ND ug/Kg 1405 07/25/2016 17:28
1,2-Dichlorobenzene ND ug/Kg 1405 07/25/2016 17:28
1,3-Dichlorobenzene ND ug/Kg 1405 07/25/2016 17:28
1,4-Dichlorobenzene ND ug/Kg 1405 07/25/2016 17:28
2,4,5-Trichlorophenol ND ug/Kg 1405 07/25/2016 17:28
2,4,6-Trichlorophenol ND ug/Kg 1405 07/25/2016 17:28
2,4-Dichlorophenol ND ug/Kg 1405 07/25/2016 17:28
2,4-Dinitrophenol ND ug/Kg 12020 07/25/2016 17:28
2,4-Dinitrotoluene ND ug/Kg 1405 07/25/2016 17:28
2,6-Dinitrotoluene ND ug/Kg 1405 07/25/2016 17:28
2-Chloronaphthalene ND ug/Kg 1405 07/25/2016 17:28
2-Chlorophenol ND ug/Kg 1405 07/25/2016 17:28
2-Methylnaphthalene ND ug/Kg 1405 07/25/2016 17:28
2-Methylphenol ND ug/Kg 1405 07/25/2016 17:28
2-Nitroaniline ND ug/Kg 1405 07/25/2016 17:28
2-Nitrophenol ND ug/Kg 1405 07/25/2016 17:28
3 and/or 4-Methylphenol ND ug/Kg 1405 07/25/2016 17:28
3,3'-Dichlorobenzidine ND ug/Kg 1802 08/1/2016 17:14
3-Nitroaniline ND ug/Kg 12020 07/25/2016 17:28
4,6-Dinitro-2-methylphenol ND ug/Kg 12020 07/25/2016 17:28
4-Chloro-3-methylphenol ND ug/Kg 1405 07/25/2016 17:28
4-Chloroaniline ND ug/Kg 1405 07/25/2016 17:28
4-Chlorophenyl phenyl ether ND ug/Kg 1405 07/25/2016 17:28
Acenaphthene ND ug/Kg 1405 07/25/2016 17:28
Acenaphthylene ND ug/Kg 1405 07/25/2016 17:28
Anthracene ND ug/Kg 1405 07/25/2016 17:28
Benzo(a)anthracene ND ug/Kg 1405 07/25/2016 17:28
Benzo(a)pyrene ND ug/Kg 1405 07/25/2016 17:28
Benzo(b)fluoranthene ND ug/Kg 1405 07/25/2016 17:28
Benzo(g,h,i)perylene ND ug/Kg 1405 07/25/2016 17:28
Benzo(k)fluoranthene ND ug/Kg 1405 07/25/2016 17:28
Benzoic acid ND ug/Kg 12020 07/25/2016 17:28
Bis(2-Chloroethoxy)methane ND ug/Kg 1405 07/25/2016 17:28
Bis(2-Chloroethyl)ether ND ug/Kg 1405 07/25/2016 17:28
Bis(2-Chloroisopropyl)ether ND ug/Kg 1405 07/25/2016 17:28
Bis(2-Ethylhexyl)phthalate ND ug/Kg 1405 07/25/2016 17:28
4-Bromophenyl phenyl ether ND ug/Kg 1405 07/25/2016 17:28
Butyl benzyl phthalate ND ug/Kg 1405 07/25/2016 17:28
Chrysene ND ug/Kg 1405 07/25/2016 17:28
Di-n-butyl phthalate ND ug/Kg 1405 07/25/2016 17:28
Di-n-octyl phthalate ND ug/Kg 1405 07/25/2016 17:28
Dibenz(a,h)anthracene ND ug/Kg 1405 07/25/2016 17:28
Print Date: 08/03/2016 N.C. Certification # 481
Page 23 of 59
Client Sample ID: UST-10
Client Project ID: 306007
Lab Sample ID: 31601445004-D
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:20
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 75.70
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-10
Date Analyzed
Dibenzofuran ND ug/Kg 1405 07/25/2016 17:28
Diethyl phthalate ND ug/Kg 1405 07/25/2016 17:28
Dimethyl phthalate ND ug/Kg 1405 07/25/2016 17:28
2,4-Dimethylphenol ND ug/Kg 1405 07/25/2016 17:28
Diphenylamine ND ug/Kg 1405 07/25/2016 17:28
Fluoranthene 735 ug/Kg 1405 07/25/2016 17:28
Fluorene ND ug/Kg 1405 07/25/2016 17:28
Hexachlorobenzene ND ug/Kg 12020 07/25/2016 17:28
Hexachlorobutadiene ND ug/Kg 1405 07/25/2016 17:28
Hexachlorocyclopentadiene ND ug/Kg 1810 07/25/2016 17:28
Hexachloroethane ND ug/Kg 1405 07/25/2016 17:28
Indeno(1,2,3-cd)pyrene ND ug/Kg 1405 07/25/2016 17:28
Isophorone ND ug/Kg 1405 07/25/2016 17:28
Naphthalene ND ug/Kg 1405 07/25/2016 17:28
4-Nitroaniline ND ug/Kg 12020 07/25/2016 17:28
Nitrobenzene ND ug/Kg 1405 07/25/2016 17:28
4-Nitrophenol ND ug/Kg 12020 07/25/2016 17:28
Pentachlorophenol ND ug/Kg 12020 07/25/2016 17:28
Phenanthrene ND ug/Kg 1405 07/25/2016 17:28
Phenol ND ug/Kg 1405 07/25/2016 17:28
Pyrene 638 ug/Kg 1405 07/25/2016 17:28
n-Nitrosodi-n-propylamine ND ug/Kg 1405 07/25/2016 17:28
Surrogates
2,4,6-Tribromophenol 91.0 %141.0-129 07/25/2016 17:28
2-Fluorobiphenyl 83.0 %148.0-123 07/25/2016 17:28
2-Fluorophenol 85.0 %142.0-123 07/25/2016 17:28
Nitrobenzene-d5 81.0 %146.0-117 07/25/2016 17:28
Phenol-d6 87.0 %148.0-125 07/25/2016 17:28
Terphenyl-d14 80.0 %144.0-140 07/25/2016 17:28
Print Date: 08/03/2016 N.C. Certification # 481
Page 24 of 59
Client Sample ID: UST-10
Client Project ID: 306007
Lab Sample ID: 31601445004-D
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:20
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 75.70
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-10
Date Analyzed
Batch Information
Prep Batch: XXX5904
Prep Method: SW-846 3541
Prep Date/Time: 07/21/2016 16:30
Prep Initial Wt./Vol.: 32.66 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2678
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX5925
Prep Method: SW-846 3541
Prep Date/Time: 08/01/2016 12:40
Prep Initial Wt./Vol.: 32.98 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2680
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 08/03/2016 N.C. Certification # 481
Page 25 of 59
Client Sample ID: UST-11
Client Project ID: 306007
Lab Sample ID: 31601445005-A
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:30
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 73.00
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-11
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/Kg 15.66 08/1/2016 16:26
1,1,1-Trichloroethane ND ug/Kg 15.66 08/1/2016 16:26
1,1,2,2-Tetrachloroethane ND ug/Kg 15.66 08/1/2016 16:26
1,1,2-Trichloroethane ND ug/Kg 15.66 08/1/2016 16:26
1,1-Dichloroethane ND ug/Kg 15.66 08/1/2016 16:26
1,1-Dichloroethene ND ug/Kg 15.66 08/1/2016 16:26
1,1-Dichloropropene ND ug/Kg 15.66 08/1/2016 16:26
1,2,3-Trichlorobenzene ND ug/Kg 15.66 08/1/2016 16:26
1,2,3-Trichloropropane ND ug/Kg 15.66 08/1/2016 16:26
1,2,4-Trichlorobenzene ND ug/Kg 15.66 08/1/2016 16:26
1,2,4-Trimethylbenzene 15.0 ug/Kg 15.66 08/1/2016 16:26
1,2-Dibromo-3-chloropropane ND ug/Kg 134.0 08/1/2016 16:26
1,2-Dibromoethane ND ug/Kg 15.66 08/1/2016 16:26
1,2-Dichlorobenzene ND ug/Kg 15.66 08/1/2016 16:26
1,2-Dichloroethane ND ug/Kg 15.66 08/1/2016 16:26
1,2-Dichloropropane ND ug/Kg 15.66 08/1/2016 16:26
1,3,5-Trimethylbenzene ND ug/Kg 15.66 08/1/2016 16:26
1,3-Dichlorobenzene ND ug/Kg 15.66 08/1/2016 16:26
1,3-Dichloropropane ND ug/Kg 15.66 08/1/2016 16:26
1,4-Dichlorobenzene ND ug/Kg 15.66 08/1/2016 16:26
2,2-Dichloropropane ND ug/Kg 15.66 08/1/2016 16:26
2-Butanone ND ug/Kg 128.3 08/1/2016 16:26
2-Chlorotoluene ND ug/Kg 15.66 08/1/2016 16:26
2-Hexanone ND ug/Kg 114.2 08/1/2016 16:26
4-Chlorotoluene ND ug/Kg 15.66 08/1/2016 16:26
4-Isopropyltoluene 5.90 ug/Kg 15.66 08/1/2016 16:26
4-Methyl-2-pentanone ND ug/Kg 114.2 08/1/2016 16:26
Acetone ND ug/Kg 156.6 08/1/2016 16:26
Benzene ND ug/Kg 15.66 08/1/2016 16:26
Bromobenzene ND ug/Kg 15.66 08/1/2016 16:26
Bromochloromethane ND ug/Kg 15.66 08/1/2016 16:26
Bromoform ND ug/Kg 15.66 08/1/2016 16:26
Bromomethane ND ug/Kg 15.66 08/1/2016 16:26
n-Butylbenzene ND ug/Kg 15.66 08/1/2016 16:26
Carbon disulfide ND ug/Kg 15.66 08/1/2016 16:26
Carbon tetrachloride ND ug/Kg 15.66 08/1/2016 16:26
Chlorobenzene ND ug/Kg 15.66 08/1/2016 16:26
Chlorodibromomethane ND ug/Kg 15.66 08/1/2016 16:26
Chloroethane ND ug/Kg 15.66 08/1/2016 16:26
Chloroform ND ug/Kg 15.66 08/1/2016 16:26
Chloromethane ND ug/Kg 15.66 08/1/2016 16:26
Dibromomethane ND ug/Kg 15.66 08/1/2016 16:26
Print Date: 08/03/2016 N.C. Certification # 481
Page 26 of 59
Client Sample ID: UST-11
Client Project ID: 306007
Lab Sample ID: 31601445005-A
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:30
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 73.00
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of UST-11
Date Analyzed
Dichlorobromomethane ND ug/Kg 15.66 08/1/2016 16:26
Dichlorodifluoromethane ND ug/Kg 15.66 08/1/2016 16:26
cis-1,3-Dichloropropene ND ug/Kg 15.66 08/1/2016 16:26
trans-1,3-Dichloropropene ND ug/Kg 15.66 08/1/2016 16:26
Diisopropyl Ether ND ug/Kg 15.66 08/1/2016 16:26
Ethyl Benzene ND ug/Kg 15.66 08/1/2016 16:26
Hexachlorobutadiene ND ug/Kg 15.66 08/1/2016 16:26
Isopropylbenzene (Cumene)ND ug/Kg 15.66 08/1/2016 16:26
Methyl iodide ND ug/Kg 15.66 08/1/2016 16:26
Methylene chloride ND ug/Kg 122.7 08/1/2016 16:26
Naphthalene 60.6 ug/Kg 15.66 08/1/2016 16:26
Styrene ND ug/Kg 15.66 08/1/2016 16:26
Tetrachloroethene ND ug/Kg 15.66 08/1/2016 16:26
Toluene ND ug/Kg 15.66 08/1/2016 16:26
Trichloroethene ND ug/Kg 15.66 08/1/2016 16:26
Trichlorofluoromethane ND ug/Kg 15.66 08/1/2016 16:26
Vinyl chloride ND ug/Kg 15.66 08/1/2016 16:26
Xylene (total)ND ug/Kg 111.3 08/1/2016 16:26
cis-1,2-Dichloroethene ND ug/Kg 15.66 08/1/2016 16:26
m,p-Xylene ND ug/Kg 111.3 08/1/2016 16:26
n-Propylbenzene ND ug/Kg 15.66 08/1/2016 16:26
o-Xylene ND ug/Kg 15.66 08/1/2016 16:26
sec-Butylbenzene 7.19 ug/Kg 15.66 08/1/2016 16:26
tert-Butyl methyl ether (MTBE)ND ug/Kg 15.66 08/1/2016 16:26
tert-Butylbenzene ND ug/Kg 15.66 08/1/2016 16:26
trans-1,2-Dichloroethene ND ug/Kg 15.66 08/1/2016 16:26
trans-1,4-Dichloro-2-butene ND ug/Kg 128.3 08/1/2016 16:26
Surrogates
1,2-Dichloroethane-d4 118 %190.9-137 08/1/2016 16:26
4-Bromofluorobenzene 160*%174.6-125 08/1/2016 16:26
Toluene d8 85.0*%188.8-113 08/1/2016 16:26
Batch Information
Prep Batch: VXX6687
Prep Method: SW-846 5035 SL
Prep Date/Time: 07/21/2016 13:01
Prep Initial Wt./Vol.: 6.05 g
Prep Extract Vol: 5 mL
Analytical Batch: VMS4083
Analytical Method: SW-846 8260B
Instrument: MSD4
Analyst: JHL
Print Date: 08/03/2016 N.C. Certification # 481
Page 27 of 59
Client Sample ID: UST-11
Client Project ID: 306007
Lab Sample ID: 31601445005-D
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:30
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 73.00
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-11
Date Analyzed
1,2,4-Trichlorobenzene ND ug/Kg 104220 07/27/2016 12:33
1,2-Dichlorobenzene ND ug/Kg 104220 07/27/2016 12:33
1,3-Dichlorobenzene ND ug/Kg 104220 07/27/2016 12:33
1,4-Dichlorobenzene ND ug/Kg 104220 07/27/2016 12:33
2,4,5-Trichlorophenol ND ug/Kg 104220 07/27/2016 12:33
2,4,6-Trichlorophenol ND ug/Kg 104220 07/27/2016 12:33
2,4-Dichlorophenol ND ug/Kg 104220 07/27/2016 12:33
2,4-Dinitrophenol ND ug/Kg 1021100 07/27/2016 12:33
2,4-Dinitrotoluene ND ug/Kg 104220 07/27/2016 12:33
2,6-Dinitrotoluene ND ug/Kg 104220 07/27/2016 12:33
2-Chloronaphthalene ND ug/Kg 104220 07/27/2016 12:33
2-Chlorophenol ND ug/Kg 104220 07/27/2016 12:33
2-Methylnaphthalene ND ug/Kg 104220 07/27/2016 12:33
2-Methylphenol ND ug/Kg 104220 07/27/2016 12:33
2-Nitroaniline ND ug/Kg 104220 07/27/2016 12:33
2-Nitrophenol ND ug/Kg 104220 07/27/2016 12:33
3 and/or 4-Methylphenol ND ug/Kg 104220 07/27/2016 12:33
3,3'-Dichlorobenzidine ND ug/Kg 108550 08/1/2016 18:20
3-Nitroaniline ND ug/Kg 1021100 07/27/2016 12:33
4,6-Dinitro-2-methylphenol ND ug/Kg 1021100 07/27/2016 12:33
4-Chloro-3-methylphenol ND ug/Kg 104220 07/27/2016 12:33
4-Chloroaniline ND ug/Kg 104220 07/27/2016 12:33
4-Chlorophenyl phenyl ether ND ug/Kg 104220 07/27/2016 12:33
Acenaphthene ND ug/Kg 104220 07/27/2016 12:33
Acenaphthylene ND ug/Kg 104220 07/27/2016 12:33
Anthracene ND ug/Kg 104220 07/27/2016 12:33
Benzo(a)anthracene ND ug/Kg 104220 07/27/2016 12:33
Benzo(a)pyrene ND ug/Kg 104220 07/27/2016 12:33
Benzo(b)fluoranthene ND ug/Kg 104220 07/27/2016 12:33
Benzo(g,h,i)perylene ND ug/Kg 104220 07/27/2016 12:33
Benzo(k)fluoranthene ND ug/Kg 104220 07/27/2016 12:33
Benzoic acid ND ug/Kg 1021100 07/27/2016 12:33
Bis(2-Chloroethoxy)methane ND ug/Kg 104220 07/27/2016 12:33
Bis(2-Chloroethyl)ether ND ug/Kg 104220 07/27/2016 12:33
Bis(2-Chloroisopropyl)ether ND ug/Kg 104220 07/27/2016 12:33
Bis(2-Ethylhexyl)phthalate ND ug/Kg 104220 07/27/2016 12:33
4-Bromophenyl phenyl ether ND ug/Kg 104220 07/27/2016 12:33
Butyl benzyl phthalate ND ug/Kg 104220 07/27/2016 12:33
Chrysene ND ug/Kg 104220 07/27/2016 12:33
Di-n-butyl phthalate ND ug/Kg 104220 07/27/2016 12:33
Di-n-octyl phthalate ND ug/Kg 104220 07/27/2016 12:33
Dibenz(a,h)anthracene ND ug/Kg 104220 07/27/2016 12:33
Print Date: 08/03/2016 N.C. Certification # 481
Page 28 of 59
Client Sample ID: UST-11
Client Project ID: 306007
Lab Sample ID: 31601445005-D
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:30
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 73.00
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-11
Date Analyzed
Dibenzofuran ND ug/Kg 104220 07/27/2016 12:33
Diethyl phthalate ND ug/Kg 104220 07/27/2016 12:33
Dimethyl phthalate ND ug/Kg 104220 07/27/2016 12:33
2,4-Dimethylphenol ND ug/Kg 104220 07/27/2016 12:33
Diphenylamine ND ug/Kg 104220 07/27/2016 12:33
Fluoranthene ND ug/Kg 104220 07/27/2016 12:33
Fluorene ND ug/Kg 104220 07/27/2016 12:33
Hexachlorobenzene ND ug/Kg 1021100 07/27/2016 12:33
Hexachlorobutadiene ND ug/Kg 104220 07/27/2016 12:33
Hexachlorocyclopentadiene ND ug/Kg 108440 07/27/2016 12:33
Hexachloroethane ND ug/Kg 104220 07/27/2016 12:33
Indeno(1,2,3-cd)pyrene ND ug/Kg 104220 07/27/2016 12:33
Isophorone ND ug/Kg 104220 07/27/2016 12:33
Naphthalene ND ug/Kg 104220 07/27/2016 12:33
4-Nitroaniline ND ug/Kg 1021100 07/27/2016 12:33
Nitrobenzene ND ug/Kg 104220 07/27/2016 12:33
4-Nitrophenol ND ug/Kg 1021100 07/27/2016 12:33
Pentachlorophenol ND ug/Kg 1021100 07/27/2016 12:33
Phenanthrene ND ug/Kg 104220 07/27/2016 12:33
Phenol ND ug/Kg 104220 07/27/2016 12:33
Pyrene ND ug/Kg 104220 07/27/2016 12:33
n-Nitrosodi-n-propylamine ND ug/Kg 104220 07/27/2016 12:33
Surrogates
2,4,6-Tribromophenol NA %10D41.0-129 07/27/2016 12:33
2-Fluorobiphenyl NA %10D48.0-123 07/27/2016 12:33
2-Fluorophenol NA %10D42.0-123 07/27/2016 12:33
Nitrobenzene-d5 NA %10D46.0-117 07/27/2016 12:33
Phenol-d6 NA %10D48.0-125 07/27/2016 12:33
Terphenyl-d14 NA %10D44.0-140 07/27/2016 12:33
Print Date: 08/03/2016 N.C. Certification # 481
Page 29 of 59
Client Sample ID: UST-11
Client Project ID: 306007
Lab Sample ID: 31601445005-D
Lab Project ID: 31601445
Collection Date: 07/20/2016 11:30
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as dry weight
Solids (%): 73.00
LOQ/CLResultQual Units DFParameter
Results by SW-846 8270D
Results of UST-11
Date Analyzed
Batch Information
Prep Batch: XXX5904
Prep Method: SW-846 3541
Prep Date/Time: 07/21/2016 16:30
Prep Initial Wt./Vol.: 32.53 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2679
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX5925
Prep Method: SW-846 3541
Prep Date/Time: 08/01/2016 12:40
Prep Initial Wt./Vol.: 32.12 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2680
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 08/03/2016 N.C. Certification # 481
Page 30 of 59
Client Sample ID: Trip Blank
Client Project ID: 306007
Lab Sample ID: 31601445006-A
Lab Project ID: 31601445
Collection Date:
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as received
Solids (%):
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of Trip Blank
Date Analyzed
1,1,1,2-Tetrachloroethane ND ug/Kg 15.00 08/1/2016 15:58
1,1,1-Trichloroethane ND ug/Kg 15.00 08/1/2016 15:58
1,1,2,2-Tetrachloroethane ND ug/Kg 15.00 08/1/2016 15:58
1,1,2-Trichloroethane ND ug/Kg 15.00 08/1/2016 15:58
1,1-Dichloroethane ND ug/Kg 15.00 08/1/2016 15:58
1,1-Dichloroethene ND ug/Kg 15.00 08/1/2016 15:58
1,1-Dichloropropene ND ug/Kg 15.00 08/1/2016 15:58
1,2,3-Trichlorobenzene ND ug/Kg 15.00 08/1/2016 15:58
1,2,3-Trichloropropane ND ug/Kg 15.00 08/1/2016 15:58
1,2,4-Trichlorobenzene ND ug/Kg 15.00 08/1/2016 15:58
1,2,4-Trimethylbenzene ND ug/Kg 15.00 08/1/2016 15:58
1,2-Dibromo-3-chloropropane ND ug/Kg 130.0 08/1/2016 15:58
1,2-Dibromoethane ND ug/Kg 15.00 08/1/2016 15:58
1,2-Dichlorobenzene ND ug/Kg 15.00 08/1/2016 15:58
1,2-Dichloroethane ND ug/Kg 15.00 08/1/2016 15:58
1,2-Dichloropropane ND ug/Kg 15.00 08/1/2016 15:58
1,3,5-Trimethylbenzene ND ug/Kg 15.00 08/1/2016 15:58
1,3-Dichlorobenzene ND ug/Kg 15.00 08/1/2016 15:58
1,3-Dichloropropane ND ug/Kg 15.00 08/1/2016 15:58
1,4-Dichlorobenzene ND ug/Kg 15.00 08/1/2016 15:58
2,2-Dichloropropane ND ug/Kg 15.00 08/1/2016 15:58
2-Butanone ND ug/Kg 125.0 08/1/2016 15:58
2-Chlorotoluene ND ug/Kg 15.00 08/1/2016 15:58
2-Hexanone ND ug/Kg 112.5 08/1/2016 15:58
4-Chlorotoluene ND ug/Kg 15.00 08/1/2016 15:58
4-Isopropyltoluene ND ug/Kg 15.00 08/1/2016 15:58
4-Methyl-2-pentanone ND ug/Kg 112.5 08/1/2016 15:58
Acetone ND ug/Kg 150.0 08/1/2016 15:58
Benzene ND ug/Kg 15.00 08/1/2016 15:58
Bromobenzene ND ug/Kg 15.00 08/1/2016 15:58
Bromochloromethane ND ug/Kg 15.00 08/1/2016 15:58
Bromoform ND ug/Kg 15.00 08/1/2016 15:58
Bromomethane ND ug/Kg 15.00 08/1/2016 15:58
n-Butylbenzene ND ug/Kg 15.00 08/1/2016 15:58
Carbon disulfide ND ug/Kg 15.00 08/1/2016 15:58
Carbon tetrachloride ND ug/Kg 15.00 08/1/2016 15:58
Chlorobenzene ND ug/Kg 15.00 08/1/2016 15:58
Chlorodibromomethane ND ug/Kg 15.00 08/1/2016 15:58
Chloroethane ND ug/Kg 15.00 08/1/2016 15:58
Chloroform ND ug/Kg 15.00 08/1/2016 15:58
Chloromethane ND ug/Kg 15.00 08/1/2016 15:58
Dibromomethane ND ug/Kg 15.00 08/1/2016 15:58
Print Date: 08/03/2016 N.C. Certification # 481
Page 31 of 59
Client Sample ID: Trip Blank
Client Project ID: 306007
Lab Sample ID: 31601445006-A
Lab Project ID: 31601445
Collection Date:
Received Date: 07/21/2016 09:50
Matrix: Soil-Solid as received
Solids (%):
LOQ/CLResultQual Units DFParameter
Results by SW-846 8260B
Results of Trip Blank
Date Analyzed
Dichlorobromomethane ND ug/Kg 15.00 08/1/2016 15:58
Dichlorodifluoromethane ND ug/Kg 15.00 08/1/2016 15:58
cis-1,3-Dichloropropene ND ug/Kg 15.00 08/1/2016 15:58
trans-1,3-Dichloropropene ND ug/Kg 15.00 08/1/2016 15:58
Diisopropyl Ether ND ug/Kg 15.00 08/1/2016 15:58
Ethyl Benzene ND ug/Kg 15.00 08/1/2016 15:58
Hexachlorobutadiene ND ug/Kg 15.00 08/1/2016 15:58
Isopropylbenzene (Cumene)ND ug/Kg 15.00 08/1/2016 15:58
Methyl iodide ND ug/Kg 15.00 08/1/2016 15:58
Methylene chloride ND ug/Kg 120.0 08/1/2016 15:58
Naphthalene ND ug/Kg 15.00 08/1/2016 15:58
Styrene ND ug/Kg 15.00 08/1/2016 15:58
Tetrachloroethene ND ug/Kg 15.00 08/1/2016 15:58
Toluene ND ug/Kg 15.00 08/1/2016 15:58
Trichloroethene ND ug/Kg 15.00 08/1/2016 15:58
Trichlorofluoromethane ND ug/Kg 15.00 08/1/2016 15:58
Vinyl chloride ND ug/Kg 15.00 08/1/2016 15:58
Xylene (total)ND ug/Kg 110.0 08/1/2016 15:58
cis-1,2-Dichloroethene ND ug/Kg 15.00 08/1/2016 15:58
m,p-Xylene ND ug/Kg 110.0 08/1/2016 15:58
n-Propylbenzene ND ug/Kg 15.00 08/1/2016 15:58
o-Xylene ND ug/Kg 15.00 08/1/2016 15:58
sec-Butylbenzene ND ug/Kg 15.00 08/1/2016 15:58
tert-Butyl methyl ether (MTBE)ND ug/Kg 15.00 08/1/2016 15:58
tert-Butylbenzene ND ug/Kg 15.00 08/1/2016 15:58
trans-1,2-Dichloroethene ND ug/Kg 15.00 08/1/2016 15:58
trans-1,4-Dichloro-2-butene ND ug/Kg 125.0 08/1/2016 15:58
Surrogates
1,2-Dichloroethane-d4 108 %190.9-137 08/1/2016 15:58
4-Bromofluorobenzene 104 %174.6-125 08/1/2016 15:58
Toluene d8 94.0 %188.8-113 08/1/2016 15:58
Batch Information
Prep Batch: VXX6687
Prep Method: SW-846 5035 SL
Prep Date/Time: 07/21/2016 13:02
Prep Initial Wt./Vol.: 5 g
Prep Extract Vol: 5 mL
Analytical Batch: VMS4083
Analytical Method: SW-846 8260B
Instrument: MSD4
Analyst: JHL
Print Date: 08/03/2016 N.C. Certification # 481
Page 32 of 59
Batch Summary
SW-846 8260B SW-846 5035 SLAnalytical Method:Prep Method:
VXX6687
08/01/2016 16:27
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
LCS-S for HBN 122763 [VXX/6687 08/01/2016 12:57 MSD4 JHL206041VMS4083
LCSD-S for HBN 122763 [VXX/668 08/01/2016 13:25 MSD4 JHL206042VMS4083
MB-S for HBN 122763 [VXX/6687]08/01/2016 14:21 MSD4 JHL206043VMS4083
UST-7(205263DUP)08/01/2016 18:48 MSD4 JHL206044VMS4083
UST-8(205264MS)08/01/2016 19:16 MSD4 JHL206045VMS4083
UST-7 08/01/2016 18:20 MSD4 JHL31601445001VMS4083
UST-8 08/01/2016 17:51 MSD4 JHL31601445002VMS4083
UST-9 08/01/2016 17:23 MSD4 JHL31601445003VMS4083
UST-10 08/01/2016 16:55 MSD4 JHL31601445004VMS4083
UST-11 08/01/2016 16:26 MSD4 JHL31601445005VMS4083
Trip Blank 08/01/2016 15:58 MSD4 JHL31601445006VMS4083
Print Date: 08/03/2016 N.C. Certification # 481
Page 33 of 59
Blank ID: MB-S for HBN 122763 [VXX/6687]
Blank Lab ID: 206043
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31601445001, 31601445002, 31601445003, 31601445004, 31601445005, 31601445006
1,1,1,2-Tetrachloroethane ND 5.00 ug/Kg 1
1,1,1-Trichloroethane ND 5.00 ug/Kg 1
1,1,2,2-Tetrachloroethane ND 5.00 ug/Kg 1
1,1,2-Trichloroethane ND 5.00 ug/Kg 1
1,1-Dichloroethane ND 5.00 ug/Kg 1
1,1-Dichloroethene ND 5.00 ug/Kg 1
1,1-Dichloropropene ND 5.00 ug/Kg 1
1,2,3-Trichlorobenzene ND 5.00 ug/Kg 1
1,2,3-Trichloropropane ND 5.00 ug/Kg 1
1,2,4-Trichlorobenzene ND 5.00 ug/Kg 1
1,2,4-Trimethylbenzene ND 5.00 ug/Kg 1
1,2-Dibromo-3-chloropropane ND 30.0 ug/Kg 1
1,2-Dibromoethane ND 5.00 ug/Kg 1
1,2-Dichlorobenzene ND 5.00 ug/Kg 1
1,2-Dichloroethane ND 5.00 ug/Kg 1
1,2-Dichloropropane ND 5.00 ug/Kg 1
1,3,5-Trimethylbenzene ND 5.00 ug/Kg 1
1,3-Dichlorobenzene ND 5.00 ug/Kg 1
1,3-Dichloropropane ND 5.00 ug/Kg 1
1,4-Dichlorobenzene ND 5.00 ug/Kg 1
2,2-Dichloropropane ND 5.00 ug/Kg 1
2-Butanone ND 25.0 ug/Kg 1
2-Chlorotoluene ND 5.00 ug/Kg 1
2-Hexanone ND 12.5 ug/Kg 1
4-Chlorotoluene ND 5.00 ug/Kg 1
4-Isopropyltoluene ND 5.00 ug/Kg 1
4-Methyl-2-pentanone ND 12.5 ug/Kg 1
Acetone ND 50.0 ug/Kg 1
Benzene ND 5.00 ug/Kg 1
Bromobenzene ND 5.00 ug/Kg 1
Bromochloromethane ND 5.00 ug/Kg 1
Bromoform ND 5.00 ug/Kg 1
Bromomethane ND 5.00 ug/Kg 1
Carbon disulfide ND 5.00 ug/Kg 1
Carbon tetrachloride ND 5.00 ug/Kg 1
Chlorobenzene ND 5.00 ug/Kg 1
Chlorodibromomethane ND 5.00 ug/Kg 1
Chloroethane ND 5.00 ug/Kg 1
Chloroform ND 5.00 ug/Kg 1
Chloromethane ND 5.00 ug/Kg 1
cis-1,2-Dichloroethene ND 5.00 ug/Kg 1
Print Date: 08/03/2016 N.C. Certification # 481
Page 34 of 59
Blank ID: MB-S for HBN 122763 [VXX/6687]
Blank Lab ID: 206043
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31601445001, 31601445002, 31601445003, 31601445004, 31601445005, 31601445006
cis-1,3-Dichloropropene ND 5.00 ug/Kg 1
Dibromomethane ND 5.00 ug/Kg 1
Dichlorobromomethane ND 5.00 ug/Kg 1
Dichlorodifluoromethane ND 5.00 ug/Kg 1
Diisopropyl Ether ND 5.00 ug/Kg 1
Ethyl Benzene ND 5.00 ug/Kg 1
Hexachlorobutadiene ND 5.00 ug/Kg 1
Isopropylbenzene (Cumene)ND 5.00 ug/Kg 1
m,p-Xylene ND 10.0 ug/Kg 1
Methyl iodide ND 5.00 ug/Kg 1
Methylene chloride ND 20.0 ug/Kg 1
Naphthalene ND 5.00 ug/Kg 1
n-Butylbenzene ND 5.00 ug/Kg 1
n-Propylbenzene ND 5.00 ug/Kg 1
o-Xylene ND 5.00 ug/Kg 1
sec-Butylbenzene ND 5.00 ug/Kg 1
Styrene ND 5.00 ug/Kg 1
tert-Butyl methyl ether (MTBE)ND 5.00 ug/Kg 1
tert-Butylbenzene ND 5.00 ug/Kg 1
Tetrachloroethene ND 5.00 ug/Kg 1
Toluene ND 5.00 ug/Kg 1
trans-1,2-Dichloroethene ND 5.00 ug/Kg 1
trans-1,3-Dichloropropene ND 5.00 ug/Kg 1
trans-1,4-Dichloro-2-butene ND 25.0 ug/Kg 1
Trichloroethene ND 5.00 ug/Kg 1
Trichlorofluoromethane ND 5.00 ug/Kg 1
Vinyl chloride ND 5.00 ug/Kg 1
Xylene (total)ND 10.0 ug/Kg 1
Surrogates
1,2-Dichloroethane-d4 107 90.9-137 %1
4-Bromofluorobenzene 102 74.6-125 %1
Toluene d8 94.0 88.8-113 %1
Batch Information
Prep Batch: VXX6687
Prep Method: SW-846 5035 SL
Prep Date/Time: 8/1/2016 4:27:50PM
Prep Initial Wt./Vol.: 5 g
Prep Extract Vol: 5 mL
Analytical Batch: VMS4083
Analytical Method: SW-846 8260B
Instrument: MSD4
Analyst: JHL
Print Date: 08/03/2016 N.C. Certification # 481
Page 35 of 59
Blank Spike ID: LCS-S for HBN 122763 [VXX/6687
Blank Spike Lab ID: 206041
Date Analyzed: 08/01/2016 12:57
Spike Duplicate ID: LCSD-S for HBN 122763 [VXX/668
Spike Duplicate Lab ID: 206042
Date Analyzed: 08/01/2016 13:25
Results by SW-846 8260B
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/Kg)
RPD CL
Spike Duplicate (ug/Kg)
31601445001, 31601445002, 31601445003, 31601445004, 31601445005, 31601445006QC for Samples:
1,1,1,2-Tetrachloroethane 30.0 31.0 2.210330.0 31.7 106 78.7-117 30.00
1,1,1-Trichloroethane 30.0 30.1 2.310030.0 30.8 103 73.4-123 30.00
1,1,2,2-Tetrachloroethane 30.0 31.9 1010630.0 35.4 118 74.5-135 30.00
1,1,2-Trichloroethane 30.0 30.6 6.010230.0 32.5 108 81.5-119 30.00
1,1-Dichloroethane 30.0 30.4 2.610130.0 31.2 104 72.0-126 30.00
1,1-Dichloroethene 30.0 32.1 0.9310730.0 32.4 108 69.1-121 30.00
1,1-Dichloropropene 30.0 30.2 2.310130.0 30.9 103 70.8-125 30.00
1,2,3-Trichlorobenzene 30.0 28.9 4.49630.0 30.2 101 80.6-118 30.00
1,2,3-Trichloropropane 30.0 30.9 1110330.0 34.5 115 74.8-133 30.00
1,2,4-Trichlorobenzene 30.0 29.6 3.39930.0 30.6 102 79.7-120 30.00
1,2,4-Trimethylbenzene 30.0 33.2 1.211130.0 32.8 109 74.1-120 30.00
1,2-Dibromo-3-chloropropane 180 208 1411518024013368.6-135 30.00
1,2-Dibromoethane 30.0 30.1 8.010030.0 32.6 109 79.4-122 30.00
1,2-Dichlorobenzene 30.0 30.9 2.210330.0 31.6 105 80.5-116 30.00
1,2-Dichloroethane 30.0 29.7 5.29930.0 31.3 104 79.7-123 30.00
1,2-Dichloropropane 30.0 29.4 3.09830.0 30.3 101 78.1-122 30.00
1,3,5-Trimethylbenzene 30.0 33.6 1.811230.0 33.0 110 72.5-120 30.00
1,3-Dichlorobenzene 30.0 30.8 1.910330.0 31.4 105 77.3-118 30.00
1,3-Dichloropropane 30.0 31.3 5.910430.0 33.2 111 80.4-119 30.00
1,4-Dichlorobenzene 30.0 30.7 0.9710230.0 31.0 103 78.6-118 30.00
2,2-Dichloropropane 30.0 29.7 1.39930.0 30.1 100 73.7-124 30.00
2-Butanone 75.0 69.9 189375.0 83.7 112 57.7-161 30.00
2-Chlorotoluene 30.0 31.2 0.010430.0 31.2 104 73.4-117 30.00
2-Hexanone 75.0 83.0 1511175.0 96.4 129 67.0-143 30.00
4-Chlorotoluene 30.0 31.1 0.6410430.0 31.3 104 74.5-118 30.00
4-Isopropyltoluene 30.0 32.5 0.010830.0 32.5 108 72.3-121 30.00
4-Methyl-2-pentanone 75.0 75.8 1610175.0 89.1 119 68.1-145 30.00
Acetone 75.0 70.8 169475.0 83.1 111 38.3-190 30.00
Benzene 30.0 29.1 3.09730.0 30.0 100 76.1-122 30.00
Bromobenzene 30.0 28.6 3.89530.0 29.7 99 81.3-116 30.00
Bromochloromethane 30.0 27.1 5.09030.0 28.5 95 78.9-126 30.00
Bromoform 30.0 32.9 7.911030.0 35.6 119 70.3-132 30.00
Print Date: 08/03/2016 N.C. Certification # 481
Page 36 of 59
Blank Spike ID: LCS-S for HBN 122763 [VXX/6687
Blank Spike Lab ID: 206041
Date Analyzed: 08/01/2016 12:57
Spike Duplicate ID: LCSD-S for HBN 122763 [VXX/668
Spike Duplicate Lab ID: 206042
Date Analyzed: 08/01/2016 13:25
Results by SW-846 8260B
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/Kg)
RPD CL
Spike Duplicate (ug/Kg)
31601445001, 31601445002, 31601445003, 31601445004, 31601445005, 31601445006QC for Samples:
Bromomethane 30.0 33.0 2.111030.0 33.7 112 43.9-141 30.00
Carbon disulfide 30.0 45.3 0.66151*30.0 45.0 150*61.5-131 30.00
Carbon tetrachloride 30.0 31.3 0.9510430.0 31.6 105 72.2-123 30.00
Chlorobenzene 30.0 29.9 3.010030.0 30.8 103 79.0-116 30.00
Chlorodibromomethane 30.0 32.4 3.910830.0 33.7 112 78.0-120 30.00
Chloroethane 30.0 28.2 139430.0 32.2 107 59.7-133 30.00
Chloroform 30.0 29.3 2.49830.0 30.0 100 75.8-124 30.00
Chloromethane 30.0 29.6 2.09930.0 30.2 101 53.5-124 30.00
cis-1,2-Dichloroethene 30.0 28.4 2.19530.0 29.0 97 73.9-124 30.00
cis-1,3-Dichloropropene 30.0 31.0 5.310330.0 32.7 109 78.9-126 30.00
Dibromomethane 30.0 27.8 5.99330.0 29.5 98 77.1-129 30.00
Dichlorobromomethane 30.0 30.9 2.910330.0 31.8 106 77.7-123 30.00
Dichlorodifluoromethane 30.0 29.4 0.349830.0 29.5 98 21.3-143 30.00
Diisopropyl Ether 30.0 31.0 4.110330.0 32.3 108 73.0-126 30.00
Ethyl Benzene 30.0 32.5 0.6210830.0 32.3 108 70.9-118 30.00
Hexachlorobutadiene 30.0 29.0 3.49730.0 30.0 100 69.6-119 30.00
Isopropylbenzene (Cumene)30.0 33.0 0.3011030.0 33.1 110 70.1-121 30.00
m,p-Xylene 60.0 65.5 0.4610960.0 65.8 110 71.8-120 30.00
Methyl iodide 30.0 37.5 1.112530.0 37.9 126 63.8-133 30.00
Methylene chloride 30.0 28.1 3.89430.0 29.2 97 73.0-121 30.00
Naphthalene 30.0 30.1 8.610030.0 32.8 109 75.8-126 30.00
n-Butylbenzene 30.0 34.5 0.5811530.0 34.3 114 72.6-122 30.00
n-Propylbenzene 30.0 33.9 0.011330.0 33.9 113 71.1-122 30.00
o-Xylene 30.0 31.8 0.010630.0 31.8 106 71.9-118 30.00
sec-Butylbenzene 30.0 33.0 0.3011030.0 32.9 110 71.6-121 30.00
Styrene 30.0 32.4 1.510830.0 32.9 110 72.8-119 30.00
tert-Butyl methyl ether (MTBE)30.0 30.0 6.510030.0 32.0 107 74.4-127 30.00
tert-Butylbenzene 30.0 31.9 0.6310630.0 32.1 107 70.9-119 30.00
Tetrachloroethene 30.0 28.2 1.89430.0 28.7 96 75.2-117 30.00
Toluene 30.0 28.6 2.49530.0 29.3 98 74.6-125 30.00
trans-1,2-Dichloroethene 30.0 29.7 2.09930.0 30.3 101 72.0-121 30.00
trans-1,3-Dichloropropene 30.0 31.0 5.310330.0 32.7 109 80.0-127 30.00
Print Date: 08/03/2016 N.C. Certification # 481
Page 37 of 59
Blank Spike ID: LCS-S for HBN 122763 [VXX/6687
Blank Spike Lab ID: 206041
Date Analyzed: 08/01/2016 12:57
Spike Duplicate ID: LCSD-S for HBN 122763 [VXX/668
Spike Duplicate Lab ID: 206042
Date Analyzed: 08/01/2016 13:25
Results by SW-846 8260B
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)Spike Result Rec (%)RPD (%)CL
Blank Spike (ug/Kg)
RPD CL
Spike Duplicate (ug/Kg)
31601445001, 31601445002, 31601445003, 31601445004, 31601445005, 31601445006QC for Samples:
trans-1,4-Dichloro-2-butene 150 190 10127150210140*73.5-133 30.00
Trichloroethene 30.0 28.0 2.89330.0 28.8 96 73.0-124 30.00
Trichlorofluoromethane 30.0 32.1 5.810730.0 30.3 101 58.1-131 30.00
Vinyl chloride 30.0 31.3 1.910430.0 31.9 106 62.4-123 30.00
Surrogates
1,2-Dichloroethane-d4 102 103 90.9-137
4-Bromofluorobenzene 99 101 74.6-125
Toluene d8 93 93 88.8-113
Batch Information
Analytical Batch: VMS4083
Analytical Method: SW-846 8260B
Instrument: MSD4
Analyst: JHL
Prep Batch: VXX6687
Prep Method: SW-846 5035 SL
Prep Date/Time: 08/01/2016 16:27
Spike Init Wt./Vol.: 5 g Extract Vol: 5 mL
Dupe Init Wt./Vol.: 5 g Extract Vol: 5 mL
Print Date: 08/03/2016 N.C. Certification # 481
Page 38 of 59
Original Sample ID: 31601445002 (UST-8)
MS Sample ID: 206045
MSD Sample ID:
Analysis Date: 08/01/2016 17:51
Analysis Date: 08/01/2016 19:16
Analysis Date:
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (ug/Kg)Spike Duplicate (ug/Kg)
CL RPD CL
QC for Samples:31601445001, 31601445002, 31601445003, 31601445004, 31601445005, 31601445006
1,1,1,2-Tetrachloroethane ND 41.2 25.6 62 *69.0-120
1,1,1-Trichloroethane ND 41.2 28.4 69 *78.0-121
1,1,2,2-Tetrachloroethane ND 41.2 32.8 80 76.0-136
1,1,2-Trichloroethane ND 41.2 31.7 77 65.0-128
1,1-Dichloroethane ND 41.2 32.0 78 72.0-139
1,1-Dichloroethene ND 41.2 33.6 81 72.0-135
1,1-Dichloropropene ND 41.2 27.2 66 *69.0-137
1,2,3-Trichlorobenzene ND 41.2 9.13 22 *61.0-126
1,2,3-Trichloropropane ND 41.2 33.3 81 10.0-218
1,2,4-Trichlorobenzene ND 41.2 9.53 23 *61.0-125
1,2,4-Trimethylbenzene ND 41.2 17.3 42 31.0-172
1,2-Dibromo-3-chloropropane ND 247 210 85 43.0-229
1,2-Dibromoethane ND 41.2 31.2 76 *78.0-148
1,2-Dichlorobenzene ND 41.2 17.5 43 *58.0-148
1,2-Dichloroethane ND 41.2 31.2 76 73.0-146
1,2-Dichloropropane ND 41.2 29.6 72 *76.0-136
1,3,5-Trimethylbenzene ND 41.2 17.1 42 *68.0-132
1,3-Dichlorobenzene ND 41.2 16.8 41 *55.0-145
1,3-Dichloropropane ND 41.2 31.9 78 33.0-137
1,4-Dichlorobenzene ND 41.2 17.2 42 *53.0-146
2,2-Dichloropropane ND 41.2 26.7 65 58.0-150
2-Butanone 31.5 103 109 75 41.0-256
2-Chlorotoluene ND 41.2 19.0 46 *60.0-144
2-Hexanone ND 103 103 100 42.0-111
4-Chlorotoluene ND 41.2 18.8 46 *59.0-141
4-Isopropyltoluene ND 41.2 13.1 32 *75.0-122
4-Methyl-2-pentanone ND 103 99.4 97 6.90-166
Acetone 99.0 103 165 64 6.80-355
Benzene ND 41.2 29.8 72 *75.0-133
Bromobenzene ND 41.2 21.0 51 *66.0-140
Bromochloromethane ND 41.2 29.0 70 *85.0-136
Bromoform ND 41.2 29.7 72 *75.0-151
Bromomethane ND 41.2 36.5 89 30.0-127
n-Butylbenzene ND 41.2 11.8 29 *41.0-147
Carbon disulfide ND 41.2 45.0 109 64.0-145
Carbon tetrachloride ND 41.2 26.0 63 *64.0-142
Print Date: 08/03/2016 N.C. Certification # 481
Page 39 of 59
Original Sample ID: 31601445002 (UST-8)
MS Sample ID: 206045
MSD Sample ID:
Analysis Date: 08/01/2016 17:51
Analysis Date: 08/01/2016 19:16
Analysis Date:
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (ug/Kg)Spike Duplicate (ug/Kg)
CL RPD CL
QC for Samples:31601445001, 31601445002, 31601445003, 31601445004, 31601445005, 31601445006
Chlorobenzene ND 41.2 24.3 59 *66.0-135
Chlorodibromomethane ND 41.2 29.8 72 *78.0-141
Chloroethane ND 41.2 30.3 74 21.0-182
Chloroform ND 41.2 30.2 73 71.0-143
Chloromethane ND 41.2 32.8 80 69.0-138
Dibromomethane ND 41.2 29.7 72 *80.0-150
Dichlorobromomethane ND 41.2 30.0 73 *77.0-140
Dichlorodifluoromethane ND 41.2 29.9 73 *82.0-130
cis-1,3-Dichloropropene ND 41.2 29.3 71 *72.0-146
trans-1,3-Dichloropropene ND 41.2 29.3 71 45.0-144
Diisopropyl Ether ND 41.2 32.3 78 *79.0-122
Ethyl Benzene ND 41.2 23.1 56 *74.0-126
Hexachlorobutadiene ND 41.2 ND 13 *52.0-134
Isopropylbenzene (Cumene)ND 41.2 19.1 46 *74.0-123
Methyl iodide ND 41.2 43.4 105 41.0-126
Methylene chloride ND 41.2 31.0 75 49.0-155
Naphthalene ND 41.2 15.7 38 *55.0-140
Styrene ND 41.2 16.8 41 *73.0-123
Tetrachloroethene ND 41.2 19.2 47 46.0-153
Toluene ND 41.2 26.0 63 *66.0-128
Trichloroethene ND 41.2 25.2 61 35.0-136
Trichlorofluoromethane ND 41.2 32.8 80 77.0-132
Vinyl chloride ND 41.2 34.7 84 68.0-137
cis-1,2-Dichloroethene ND 41.2 29.3 71 *77.0-134
m,p-Xylene ND 82.4 46.4 56 *80.0-118
n-Propylbenzene ND 41.2 17.8 43 *72.0-128
o-Xylene ND 41.2 23.3 57 *80.0-121
sec-Butylbenzene ND 41.2 13.4 32 *57.0-138
tert-Butyl methyl ether (MTBE)ND 41.2 32.1 78 67.0-135
tert-Butylbenzene ND 41.2 15.0 36 *61.0-142
trans-1,2-Dichloroethene ND 41.2 30.9 75 72.0-135
trans-1,4-Dichloro-2-butene ND 206 203 99 49.0-211
Surrogates
1,2-Dichloroethane-d4 106 90.9-137
4-Bromofluorobenzene 102 74.6-125
Toluene d8 96 88.8-113
Print Date: 08/03/2016 N.C. Certification # 481
Page 40 of 59
Original Sample ID: 31601445002 (UST-8)
MS Sample ID: 206045
MSD Sample ID:
Analysis Date: 08/01/2016 17:51
Analysis Date: 08/01/2016 19:16
Analysis Date:
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (%)Spike Duplicate (%)
CL RPD CL
QC for Samples:31601445001, 31601445002, 31601445003, 31601445004, 31601445005, 31601445006
Batch Information
Analytical Batch: VMS4083
Analytical Method: SW-846 8260B
Instrument: MSD4
Analyst: JHL
Prep Batch: VXX6687
Prep Method: SW-846 5035 SL
Prep Date/Time: 07/21/2016 13:00
MS Init Wt./Vol.: 5 g Extract Vol.: 5 mL
MSD Init Wt./Vol.: Extract Vol.:
Print Date: 08/03/2016 N.C. Certification # 481
Page 41 of 59
Original Sample ID: 31601445001-A
Duplicate Sample ID: 206044
Analysis Date: 08/01/2016 18:20
Analysis Date: 08/01/2016 18:48
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Duplicate Sample Summary
PARAMETER Original (ug/Kg)Duplicate (ug/Kg)RPD (%)RPD CL
QC for Samples:31601445001, 31601445002, 31601445003, 31601445004, 31601445005, 31601445006
Qual Qual
1,1,1,2-Tetrachloroethane ND ND 30.00
1,1,1-Trichloroethane ND ND 30.00
1,1,2,2-Tetrachloroethane ND ND 30.00
1,1,2-Trichloroethane ND ND 30.00
1,1-Dichloroethane ND ND 30.00
1,1-Dichloroethene ND ND 30.00
1,1-Dichloropropene ND ND 30.00
1,2,3-Trichlorobenzene ND ND 30.00
1,2,3-Trichloropropane ND ND 30.00
1,2,4-Trichlorobenzene ND ND 30.00
1,2,4-Trimethylbenzene ND ND 30.00
1,2-Dibromo-3-chloropropane ND ND 30.00
1,2-Dibromoethane ND ND 30.00
1,2-Dichlorobenzene ND ND 30.00
1,2-Dichloroethane ND ND 30.00
1,2-Dichloropropane ND ND 30.00
1,3,5-Trimethylbenzene ND ND 30.00
1,3-Dichlorobenzene ND ND 30.00
1,3-Dichloropropane ND ND 30.00
1,4-Dichlorobenzene ND ND 30.00
2,2-Dichloropropane ND ND 30.00
2-Butanone ND ND 30.00
2-Chlorotoluene ND ND 30.00
2-Hexanone ND ND 30.00
4-Chlorotoluene ND ND 30.00
4-Isopropyltoluene ND ND 30.00
4-Methyl-2-pentanone ND ND 30.00
Print Date: 08/03/2016 N.C. Certification # 481
Page 42 of 59
Original Sample ID: 31601445001-A
Duplicate Sample ID: 206044
Analysis Date: 08/01/2016 18:20
Analysis Date: 08/01/2016 18:48
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Duplicate Sample Summary
PARAMETER Original (ug/Kg)Duplicate (ug/Kg)RPD (%)RPD CL
QC for Samples:31601445001, 31601445002, 31601445003, 31601445004, 31601445005, 31601445006
Qual Qual
Acetone ND ND 30.00
Benzene ND ND 30.00
Bromobenzene ND ND 30.00
Bromochloromethane ND ND 30.00
Bromoform ND ND 30.00
Bromomethane ND ND 30.00
Carbon disulfide ND ND 30.00
Carbon tetrachloride ND ND 30.00
Chlorobenzene ND ND 30.00
Chlorodibromomethane ND ND 30.00
Chloroethane ND ND 30.00
Chloroform ND ND 30.00
Chloromethane ND ND 30.00
cis-1,2-Dichloroethene ND ND 30.00
cis-1,3-Dichloropropene ND ND 30.00
Dibromomethane ND ND 30.00
Dichlorobromomethane ND ND 30.00
Dichlorodifluoromethane ND ND 30.00
Diisopropyl Ether ND ND 30.00
Ethyl Benzene ND ND 30.00
Hexachlorobutadiene ND ND 30.00
Isopropylbenzene (Cumene)ND ND 30.00
m,p-Xylene ND ND 30.00
Methyl iodide ND ND 30.00
Methylene chloride ND ND 30.00
Naphthalene ND ND 30.00
n-Butylbenzene ND ND 30.00
Print Date: 08/03/2016 N.C. Certification # 481
Page 43 of 59
Original Sample ID: 31601445001-A
Duplicate Sample ID: 206044
Analysis Date: 08/01/2016 18:20
Analysis Date: 08/01/2016 18:48
Matrix: Soil-Solid as dry weight
Results by SW-846 8260B
Duplicate Sample Summary
PARAMETER Original (ug/Kg)Duplicate (ug/Kg)RPD (%)RPD CL
QC for Samples:31601445001, 31601445002, 31601445003, 31601445004, 31601445005, 31601445006
Qual Qual
n-Propylbenzene ND ND 30.00
o-Xylene ND ND 30.00
sec-Butylbenzene ND ND 30.00
Styrene ND ND 30.00
tert-Butyl methyl ether (MTBE)ND ND 30.00
tert-Butylbenzene ND ND 30.00
Tetrachloroethene ND ND 30.00
Toluene ND ND 30.00
trans-1,2-Dichloroethene ND ND 30.00
trans-1,3-Dichloropropene ND ND 30.00
trans-1,4-Dichloro-2-butene ND ND 30.00
Trichloroethene ND ND 30.00
Trichlorofluoromethane ND ND 30.00
Vinyl chloride ND ND 30.00
Xylene (total)ND ND
Surrogates
1,2-Dichloroethane-d4 109 107 27
4-Bromofluorobenzene 106 106 28
Toluene d8 96.0 96.0 28
Analytical Batch: VMS4083
Analytical Method: SW-846 8260B
Instrument: MSD4
Analyst: JHL
Prep Batch: VXX6687
Prep Method: SW-846 5035 SL
Prep Date/Time: 07/21/2016 13:00
Batch Information
Print Date: 08/03/2016 N.C. Certification # 481
Page 44 of 59
Batch Summary
SW-846 8270D SW-846 3541Analytical Method:Prep Method:
XXX5904
07/21/2016 16:30
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
MB for HBN 121814 [XXX/5904]07/25/2016 12:44 MSD10 DTF205338XMS2678
LCS for HBN 121814 [XXX/5904]07/25/2016 13:06 MSD10 DTF205339XMS2678
UST-7(205263MS)07/25/2016 16:01 MSD10 DTF205340XMS2678
UST-7(205263MSD)07/25/2016 16:23 MSD10 DTF205341XMS2678
UST-7 07/25/2016 15:39 MSD10 DTF31601445001XMS2678
UST-8 07/25/2016 16:44 MSD10 DTF31601445002XMS2678
UST-9 07/25/2016 17:06 MSD10 DTF31601445003XMS2678
UST-10 07/25/2016 17:28 MSD10 DTF31601445004XMS2678
UST-11 07/27/2016 12:33 MSD10 DTF31601445005XMS2679
Print Date: 08/03/2016 N.C. Certification # 481
Page 45 of 59
Blank ID: MB for HBN 121814 [XXX/5904]
Blank Lab ID: 205338
Matrix: Soil-Solid as dry weight
Results by SW-846 8270D
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31601445001, 31601445002, 31601445003, 31601445004, 31601445005
1,2,4-Trichlorobenzene ND 313 ug/Kg 1
1,2-Dichlorobenzene ND 313 ug/Kg 1
1,3-Dichlorobenzene ND 313 ug/Kg 1
1,4-Dichlorobenzene ND 313 ug/Kg 1
2,4,5-Trichlorophenol ND 313 ug/Kg 1
2,4,6-Trichlorophenol ND 313 ug/Kg 1
2,4-Dichlorophenol ND 313 ug/Kg 1
2,4-Dimethylphenol ND 313 ug/Kg 1
2,4-Dinitrophenol ND 1570 ug/Kg 1
2,4-Dinitrotoluene ND 313 ug/Kg 1
2,6-Dinitrotoluene ND 313 ug/Kg 1
2-Chloronaphthalene ND 313 ug/Kg 1
2-Chlorophenol ND 313 ug/Kg 1
2-Methylnaphthalene ND 313 ug/Kg 1
2-Methylphenol ND 313 ug/Kg 1
2-Nitroaniline ND 313 ug/Kg 1
2-Nitrophenol ND 313 ug/Kg 1
3 and/or 4-Methylphenol ND 313 ug/Kg 1
3-Nitroaniline ND 1570 ug/Kg 1
4,6-Dinitro-2-methylphenol ND 1570 ug/Kg 1
4-Bromophenyl phenyl ether ND 313 ug/Kg 1
4-Chloro-3-methylphenol ND 313 ug/Kg 1
4-Chloroaniline ND 313 ug/Kg 1
4-Chlorophenyl phenyl ether ND 313 ug/Kg 1
4-Nitroaniline ND 1570 ug/Kg 1
4-Nitrophenol ND 1570 ug/Kg 1
Acenaphthene ND 313 ug/Kg 1
Acenaphthylene ND 313 ug/Kg 1
Anthracene ND 313 ug/Kg 1
Benzo(a)anthracene ND 313 ug/Kg 1
Benzo(a)pyrene ND 313 ug/Kg 1
Benzo(b)fluoranthene ND 313 ug/Kg 1
Benzo(g,h,i)perylene ND 313 ug/Kg 1
Benzo(k)fluoranthene ND 313 ug/Kg 1
Benzoic acid ND 1570 ug/Kg 1
Bis(2-Chloroethoxy)methane ND 313 ug/Kg 1
Bis(2-Chloroethyl)ether ND 313 ug/Kg 1
Bis(2-Chloroisopropyl)ether ND 313 ug/Kg 1
Bis(2-Ethylhexyl)phthalate ND 313 ug/Kg 1
Butyl benzyl phthalate ND 313 ug/Kg 1
Chrysene ND 313 ug/Kg 1
Print Date: 08/03/2016 N.C. Certification # 481
Page 46 of 59
Blank ID: MB for HBN 121814 [XXX/5904]
Blank Lab ID: 205338
Matrix: Soil-Solid as dry weight
Results by SW-846 8270D
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31601445001, 31601445002, 31601445003, 31601445004, 31601445005
Dibenz(a,h)anthracene ND 313 ug/Kg 1
Dibenzofuran ND 313 ug/Kg 1
Diethyl phthalate ND 313 ug/Kg 1
Dimethyl phthalate ND 313 ug/Kg 1
Di-n-butyl phthalate ND 313 ug/Kg 1
Di-n-octyl phthalate ND 313 ug/Kg 1
Diphenylamine ND 313 ug/Kg 1
Fluoranthene ND 313 ug/Kg 1
Fluorene ND 313 ug/Kg 1
Hexachlorobenzene ND 1570 ug/Kg 1
Hexachlorobutadiene ND 313 ug/Kg 1
Hexachlorocyclopentadiene ND 626 ug/Kg 1
Hexachloroethane ND 313 ug/Kg 1
Indeno(1,2,3-cd)pyrene ND 313 ug/Kg 1
Isophorone ND 313 ug/Kg 1
Naphthalene ND 313 ug/Kg 1
Nitrobenzene ND 313 ug/Kg 1
n-Nitrosodi-n-propylamine ND 313 ug/Kg 1
Pentachlorophenol ND 1570 ug/Kg 1
Phenanthrene ND 313 ug/Kg 1
Phenol ND 313 ug/Kg 1
Pyrene ND 313 ug/Kg 1
Surrogates
2,4,6-Tribromophenol 32.0*41.0-129 %1
2-Fluorobiphenyl 85.0 48.0-123 %1
2-Fluorophenol 59.0 42.0-123 %1
Nitrobenzene-d5 91.0 46.0-117 %1
Phenol-d6 75.0 48.0-125 %1
Terphenyl-d14 80.0 44.0-140 %1
Batch Information
Prep Batch: XXX5904
Prep Method: SW-846 3541
Prep Date/Time: 7/21/2016 4:30:00PM
Prep Initial Wt./Vol.: 32 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2678
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 08/03/2016 N.C. Certification # 481
Page 47 of 59
Blank Spike ID: LCS for HBN 121814 [XXX/5904]
Blank Spike Lab ID: 205339
Date Analyzed: 07/25/2016 13:06
Results by SW-846 8270D
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)CL
Blank Spike (ug/Kg)
31601445001, 31601445002, 31601445003, 31601445004, 31601445005QC for Samples:
1,2,4-Trichlorobenzene 3130 2690 86 73.0-124
1,2-Dichlorobenzene 3130 2470 79 66.0-119
1,3-Dichlorobenzene 3130 2500 80 63.0-119
1,4-Dichlorobenzene 3130 2490 80 65.0-119
2,4,5-Trichlorophenol 3130 2380 76 76.0-128
2,4,6-Trichlorophenol 3130 2400 77 68.0-119
2,4-Dichlorophenol 3130 2530 81 73.0-120
2,4-Dimethylphenol 3130 2460 79 53.0-122
2,4-Dinitrophenol 3130 ND 26 17.0-125
2,4-Dinitrotoluene 3130 2630 84 76.0-122
2,6-Dinitrotoluene 3130 2640 85 74.0-121
2-Chloronaphthalene 3130 2460 79 66.0-110
2-Chlorophenol 3130 2440 78 70.0-115
2-Methylnaphthalene 3130 2750 88 75.0-120
2-Methylphenol 3130 2480 79 69.0-118
2-Nitroaniline 3130 2260 72 60.0-103
2-Nitrophenol 3130 2510 80 71.0-116
3 and/or 4-Methylphenol 6250 5200 83 71.0-124
3-Nitroaniline 3130 ND 41 29.0-124
4,6-Dinitro-2-methylphenol 3130 2000 64 50.0-143
4-Bromophenyl phenyl ether 3130 2610 83 71.0-130
4-Chloro-3-methylphenol 3130 2470 79 72.0-121
4-Chloroaniline 3130 515 16 7.00-126
4-Chlorophenyl phenyl ether 3130 2800 90 76.0-125
4-Nitroaniline 3130 2200 70 61.0-112
4-Nitrophenol 3130 2020 65 56.0-133
Acenaphthene 3130 2610 83 74.0-118
Acenaphthylene 3130 2730 87 75.0-122
Anthracene 3130 2550 82 73.0-128
Benzo(a)anthracene 3130 2510 80 72.0-123
Benzo(a)pyrene 3130 2850 91 71.0-126
Benzo(b)fluoranthene 3130 3290 105 63.0-116
Print Date: 08/03/2016 N.C. Certification # 481
Page 48 of 59
Blank Spike ID: LCS for HBN 121814 [XXX/5904]
Blank Spike Lab ID: 205339
Date Analyzed: 07/25/2016 13:06
Results by SW-846 8270D
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)CL
Blank Spike (ug/Kg)
31601445001, 31601445002, 31601445003, 31601445004, 31601445005QC for Samples:
Benzo(g,h,i)perylene 3130 3390 108 77.0-143
Benzo(k)fluoranthene 3130 3410 109 74.0-125
Benzoic acid 3130 ND 0 0.00-114
Bis(2-Chloroethoxy)methane 3130 2720 87 72.0-119
Bis(2-Chloroethyl)ether 3130 3130 100 58.0-127
Bis(2-Chloroisopropyl)ether 3130 2620 84 65.0-112
Bis(2-Ethylhexyl)phthalate 3130 2520 81 69.0-125
Butyl benzyl phthalate 3130 2580 82 73.0-118
Chrysene 3130 2570 82 72.0-128
Dibenz(a,h)anthracene 3130 3350 107 73.0-138
Dibenzofuran 3130 2670 85 75.0-120
Diethyl phthalate 3130 2670 85 74.0-120
Dimethyl phthalate 3130 2620 84 73.0-121
Di-n-butyl phthalate 3130 2600 83 75.0-129
Di-n-octyl phthalate 3130 3260 104 71.0-121
Diphenylamine 3130 2430 78 72.0-124
Fluoranthene 3130 2630 84 74.0-130
Fluorene 3130 2780 89 77.0-123
Hexachlorobenzene 3130 2580 82 71.0-123
Hexachlorobutadiene 3130 2720 87 70.0-121
Hexachlorocyclopentadiene 3130 2970 95 71.0-130
Hexachloroethane 3130 2440 78 64.0-118
Indeno(1,2,3-cd)pyrene 3130 3360 108 76.0-137
Isophorone 3130 2750 88 75.0-118
Naphthalene 3130 2650 85 72.0-116
Nitrobenzene 3130 2860 91 70.0-116
n-Nitrosodi-n-propylamine 3130 2530 81 70.0-112
Pentachlorophenol 3130 2050 66 32.0-140
Phenanthrene 3130 2590 83 74.0-128
Phenol 3130 2460 79 69.0-116
Pyrene 3130 2600 83 74.0-121
Surrogates
Print Date: 08/03/2016 N.C. Certification # 481
Page 49 of 59
Blank Spike ID: LCS for HBN 121814 [XXX/5904]
Blank Spike Lab ID: 205339
Date Analyzed: 07/25/2016 13:06
Results by SW-846 8270D
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)CL
Blank Spike (%)
31601445001, 31601445002, 31601445003, 31601445004, 31601445005QC for Samples:
2,4,6-Tribromophenol 85 41.0-129
2-Fluorobiphenyl 88 48.0-123
2-Fluorophenol 79 42.0-123
Nitrobenzene-d5 93 46.0-117
Phenol-d6 83 48.0-125
Terphenyl-d14 88 44.0-140
Batch Information
Analytical Batch: XMS2678
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX5904
Prep Method: SW-846 3541
Prep Date/Time: 07/21/2016 16:30
Spike Init Wt./Vol.: 32 g Extract Vol: 10 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 08/03/2016 N.C. Certification # 481
Page 50 of 59
Original Sample ID: 31601445001 (UST-7)
MS Sample ID: 205340
MSD Sample ID: 205341
Analysis Date: 07/25/2016 15:39
Analysis Date: 07/25/2016 16:01
Analysis Date: 07/25/2016 16:23
Matrix: Soil-Solid as dry weight
Results by SW-846 8270D
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (ug/Kg)Spike Duplicate (ug/Kg)
CL RPD CL
QC for Samples:31601445001, 31601445002, 31601445003, 31601445004, 31601445005
1,2,4-Trichlorobenzene ND 4324 3300 4351 3520 81 7.076 30.0068.9-119
1,2-Dichlorobenzene ND 4324 3330 4351 3450 79 3.377 30.0073.3-121
1,3-Dichlorobenzene ND 4324 3310 4351 3440 79 4.177 30.0069.7-119
1,4-Dichlorobenzene ND 4324 3330 4351 3470 80 4.177 30.0070.6-117
2,4,5-Trichlorophenol ND 4324 3350 4351 3750 86 1177 30.0072.4-118
2,4,6-Trichlorophenol ND 4324 3380 4351 3700 85 9.478 30.0067.9-116
2,4-Dichlorophenol ND 4324 3430 4351 3720 86 8.279 30.0074.5-115
2,4-Dinitrophenol ND 4324 2530 4351 2720 63 7.458 30.0020.4-130
2,4-Dinitrotoluene ND 4324 3370 4351 3630 84 7.678 30.0067.6-136
2,6-Dinitrotoluene ND 4324 3330 4351 3560 82 6.577 30.0069.3-131
2-Chloronaphthalene ND 4324 3110 4351 3300 76 6.172 30.0070.3-124
2-Chlorophenol ND 4324 3600 4351 3770 87 4.583 30.0077.1-111
2-Methylnaphthalene ND 4324 3390 4351 3590 82 5.678 30.0074.1-111
2-Methylphenol ND 4324 3580 4351 3670 84 2.383 30.0078.7-116
2-Nitroaniline ND 4324 3290 4351 3250 75 1.376 30.0070.0-129
2-Nitrophenol ND 4324 3440 4351 3730 86 7.880 30.0063.3-112
3 and/or 4-Methylphenol ND 8647 7720 8703 7800 90 0.9089 30.0071.2-101
3-Nitroaniline ND 4324 2210 4351 2880 66 *2651 * 30.0076.6-356
4,6-Dinitro-2-methylphenol ND 4324 3670 4351 3520 81 3.985 30.0039.4-126
4-Chloro-3-methylphenol ND 4324 3430 4351 3540 81 3.279 * 30.0080.0-115
4-Chloroaniline ND 4324 3210 4351 1520 35 71*74 30.0025.1-237
4-Chlorophenyl phenyl ether ND 4324 3460 4351 3790 87 9.280 30.0072.8-125
Acenaphthene ND 4324 3340 4351 3480 80 3.777 30.0071.0-125
Acenaphthylene ND 4324 3460 4351 3600 83 4.080 30.0073.0-140
Anthracene ND 4324 3260 4351 3440 79 5.475 30.0066.9-119
Benzo(a)anthracene ND 4324 3270 4351 3480 80 5.876 30.0051.8-127
Benzo(a)pyrene ND 4324 3490 4351 3760 86 7.381 30.0078.5-137
Benzo(b)fluoranthene ND 4324 3320 4351 3710 85 1177 30.0062.3-134
Benzo(g,h,i)perylene ND 4324 3670 4351 4060 93 1085 30.0056.2-149
Benzo(k)fluoranthene ND 4324 3510 4351 3790 87 7.681 30.0079.7-133
Benzoic acid ND 4324 ND 4351 ND 3.12.7 30.001.00-140
Bis(2-Chloroethoxy)methane ND 4324 3430 4351 3660 84 6.779 30.0071.4-123
Bis(2-Chloroethyl)ether ND 4324 4540 4351 4290 99 5.7105 30.0064.0-120
Bis(2-Chloroisopropyl)ether ND 4324 3490 4351 3670 84 5.181 30.0060.5-123
Bis(2-Ethylhexyl)phthalate ND 4324 3240 4351 3450 79 5.875 30.0068.5-134
4-Bromophenyl phenyl ether ND 4324 3130 4351 3530 81 1272 30.0065.2-127
Print Date: 08/03/2016 N.C. Certification # 481
Page 51 of 59
Original Sample ID: 31601445001 (UST-7)
MS Sample ID: 205340
MSD Sample ID: 205341
Analysis Date: 07/25/2016 15:39
Analysis Date: 07/25/2016 16:01
Analysis Date: 07/25/2016 16:23
Matrix: Soil-Solid as dry weight
Results by SW-846 8270D
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (ug/Kg)Spike Duplicate (ug/Kg)
CL RPD CL
QC for Samples:31601445001, 31601445002, 31601445003, 31601445004, 31601445005
Butyl benzyl phthalate ND 4324 3330 4351 3540 81 6.177 30.0064.4-133
Chrysene ND 4324 3300 4351 3570 82 7.776 30.0072.7-124
Di-n-butyl phthalate ND 4324 3290 4351 3520 81 6.676 30.0067.9-125
Di-n-octyl phthalate ND 4324 3510 4351 3820 88 8.481 30.0048.9-162
Dibenz(a,h)anthracene ND 4324 3510 4351 3850 88 9.181 30.0058.6-146
Dibenzofuran ND 4324 3350 4351 3570 82 6.577 30.0070.6-115
Diethyl phthalate ND 4324 3300 4351 3500 81 6.276 30.0070.8-127
Dimethyl phthalate ND 4324 3320 4351 3540 81 6.577 30.0068.5-122
2,4-Dimethylphenol ND 4324 3230 4351 3510 81 *8.775 * 30.0085.4-138
Diphenylamine ND 4324 3100 4351 3340 77 7.872 * 30.0073.6-208
Fluoranthene ND 4324 3350 4351 3530 81 5.777 30.0064.6-129
Fluorene ND 4324 3490 4351 3700 85 6.281 30.0072.4-128
Hexachlorobenzene ND 4324 3210 4351 3460 80 7.574 30.0062.9-124
Hexachlorobutadiene ND 4324 3190 4351 3620 83 1374 30.0069.1-118
Hexachlorocyclopentadiene ND 4324 3350 4351 3690 85 9.978 30.001.00-176
Hexachloroethane ND 4324 3340 4351 3450 79 3.377 30.0068.0-122
Indeno(1,2,3-cd)pyrene ND 4324 3590 4351 3960 91 1083 30.0029.1-157
Isophorone ND 4324 3340 4351 3550 82 6.177 30.0065.2-143
Naphthalene ND 4324 3400 4351 3510 81 3.279 30.0049.9-137
4-Nitroaniline ND 4324 3230 4351 3570 82 9.875 30.0050.8-178
Nitrobenzene ND 4324 3320 4351 3550 82 6.577 30.0071.4-122
4-Nitrophenol ND 4324 3490 4351 3870 89 1081 30.0056.8-133
Pentachlorophenol ND 4324 3350 4351 3730 86 1178 30.0029.2-108
Phenanthrene ND 4324 3320 4351 3550 82 6.977 30.0055.8-128
Phenol ND 4324 3680 4351 4030 93 9.085 30.0071.2-120
Pyrene ND 4324 3380 4351 3630 84 7.678 30.0068.5-140
n-Nitrosodi-n-propylamine ND 4324 3630 4351 3620 83 0.3884 30.0074.3-133
Surrogates
2,4,6-Tribromophenol 8675 41.0-129
2-Fluorobiphenyl 7976 48.0-123
2-Fluorophenol 8384 42.0-123
Nitrobenzene-d5 8076 46.0-117
Phenol-d6 8785 48.0-125
Terphenyl-d14 8277 44.0-140
Print Date: 08/03/2016 N.C. Certification # 481
Page 52 of 59
Original Sample ID: 31601445001 (UST-7)
MS Sample ID: 205340
MSD Sample ID: 205341
Analysis Date: 07/25/2016 15:39
Analysis Date: 07/25/2016 16:01
Analysis Date: 07/25/2016 16:23
Matrix: Soil-Solid as dry weight
Results by SW-846 8270D
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (%)Spike Duplicate (%)
CL RPD CL
QC for Samples:31601445001, 31601445002, 31601445003, 31601445004, 31601445005
Batch Information
Analytical Batch: XMS2678
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX5904
Prep Method: SW-846 3541
Prep Date/Time: 07/21/2016 16:30
MS Init Wt./Vol.: 32.24 g Extract Vol.: 10 mL
MSD Init Wt./Vol.: 32.07 g Extract Vol.: 10 mL
Print Date: 08/03/2016 N.C. Certification # 481
Page 53 of 59
Batch Summary
SW-846 8270D SW-846 3541Analytical Method:Prep Method:
XXX5925
08/01/2016 12:40
Prep Batch:
Prep Date:
Client Sample ID Analysis Date Instrument AnalystLab Sample ID Analytical Batch
MB for HBN 122751 [XXX/5925]08/01/2016 15:25 MSD10 DTF206004XMS2680
LCS for HBN 122751 [XXX/5925]08/01/2016 15:47 MSD10 DTF206005XMS2680
UST-10(205266MS)08/01/2016 17:36 MSD10 DTF206006XMS2680
UST-10(205266MSD)08/01/2016 17:58 MSD10 DTF206007XMS2680
UST-7 08/01/2016 16:09 MSD10 DTF31601445001XMS2680
UST-8 08/01/2016 16:31 MSD10 DTF31601445002XMS2680
UST-9 08/01/2016 16:53 MSD10 DTF31601445003XMS2680
UST-10 08/01/2016 17:14 MSD10 DTF31601445004XMS2680
UST-11 08/01/2016 18:20 MSD10 DTF31601445005XMS2680
Print Date: 08/03/2016 N.C. Certification # 481
Page 54 of 59
Blank ID: MB for HBN 122751 [XXX/5925]
Blank Lab ID: 206004
Matrix: Soil-Solid as dry weight
Results by SW-846 8270D
Method Blank
Parameter Result LOQ/CL Units DFQual
QC for Samples:
31601445001, 31601445002, 31601445003, 31601445004, 31601445005
3,3'-Dichlorobenzidine ND 626 ug/Kg 1
Batch Information
Prep Batch: XXX5925
Prep Method: SW-846 3541
Prep Date/Time: 8/1/2016 12:40:55PM
Prep Initial Wt./Vol.: 32 g
Prep Extract Vol: 10 mL
Analytical Batch: XMS2680
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Print Date: 08/03/2016 N.C. Certification # 481
Page 55 of 59
Blank Spike ID: LCS for HBN 122751 [XXX/5925]
Blank Spike Lab ID: 206005
Date Analyzed: 08/01/2016 15:47
Results by SW-846 8270D
Blank Spike Summary
Matrix: Soil-Solid as dry weight
Parameter Spike Result Rec (%)CL
Blank Spike (ug/Kg)
31601445001, 31601445002, 31601445003, 31601445004, 31601445005QC for Samples:
3,3'-Dichlorobenzidine 3130 2450 79 8.00-158
Batch Information
Analytical Batch: XMS2680
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX5925
Prep Method: SW-846 3541
Prep Date/Time: 08/01/2016 12:40
Spike Init Wt./Vol.: 32 g Extract Vol: 10 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 08/03/2016 N.C. Certification # 481
Page 56 of 59
Original Sample ID: 31601445004 (UST-10)
MS Sample ID: 206006
MSD Sample ID: 206007
Analysis Date: 08/01/2016 17:14
Analysis Date: 08/01/2016 17:36
Analysis Date: 08/01/2016 17:58
Matrix: Soil-Solid as dry weight
Results by SW-846 8270D
Matrix Spike Summary
Parameter Sample Spike Result Rec (%)Spike Result Rec (%)RPD (%)
Matrix Spike (ug/Kg)Spike Duplicate (ug/Kg)
CL RPD CL
QC for Samples:31601445001, 31601445002, 31601445003, 31601445004, 31601445005
3,3'-Dichlorobenzidine ND 4122 2840 4082 1750 43 47*69 30.0014.2-302
Batch Information
Analytical Batch: XMS2680
Analytical Method: SW-846 8270D
Instrument: MSD10
Analyst: DTF
Prep Batch: XXX5925
Prep Method: SW-846 3541
Prep Date/Time: 08/01/2016 12:40
MS Init Wt./Vol.: 32.08 g Extract Vol.: 10 mL
MSD Init Wt./Vol.: 32.4 g Extract Vol.: 10 mL
Print Date: 08/03/2016 N.C. Certification # 481
Page 57 of 59
Page 58 of 59
Page 59 of 59
Attachment G