16039_Revolution_Mill_Two_Year_Rpt_20161130

APPENDIX A 
Republic Services, Inc.
18500 N. Allied Way, Phoenix, AZ 85054
SPECIAL WASTE DEPARTMENT DECISION
Waste Profile #
3041161011
Expiration Date
1/18/2017
I. Decision Request:Initial Recertification Change
Disposal Facility:3041 - Uwharrie Environmental Regional MSW Landfill
Generator Name:Historic Revolution LLC
Generator Site Address:1200 N. Revolution Mill Drive
City:Greensboro County:State:NC Zip:
Name of Waste:Excavated Soil
Estimated Annual Volume:200 Cubic Yards
II. Special Waste Department Decision:
Approved Rejected
Management Method(s):
Landfill Solidification Bioremediation Transfer Facility
Problematic Special Waste according to Republic?Yes No
If yes, which one?
Approved by Special Waste Review Committee?Yes No Not Applicable
Precautions, Conditions or Limitations on Approval


Special Waste Analyst Signature:____________________________Name (Printed):KEITH DIAMANTI
Date: 1/20/2016
III. Facility Decision:Approved Rejected
Precautions, Conditions or Limitations on Approval

By signing below, the General Manager or Designee agrees that a fully executed Special Waste Service Agreement is on file for this profile and that the
special waste file is complete.
General Manager or Designee:_____________________________Name (Printed):_____________________________
Date: 1/20/2016
X
Joe Reynolds, Site Manager
SPECIAL WASTE PROFILE
pril3
I. Generator Information
II. Billing Information
III. Waste Stream Information
ONGOING
IV. Representative Sample Certification

e Date
Sample ID Numbers:
3041 Uwharrie Environmental LF NC
Historic Revolution LLC
1200 N. Revolution Mill Drive, Greensboro, NC
Greensboro Guilford North Carolina 27405
N/A N/A N/A
✔301 W. Main Street
Durham Durham North Carolina 27701
Paul Brown [e-mail]
[phone] None
CT Wilson Construction Company Kate White
PO Box 2011 [e-mail]
Durham NC 27702 [phone]
Excavated Soil
Soil excavated from the Revolution Mill brownfields site for sewer line construction that did not meet compaction
standards and has to be disposed off-site.
✔
✔
✔
200 Cubic Yards
✔
✔
✔
1/13/2016
✔✔
SP-1A, SP-1B, SP-2A, SP-2B - grab samples tested for VOCs.
SP-1 and SP-2 - composite samples; each had four aliquots collected from separate locations within
approximately half of the 200 cubic yard stockpile. These composite samples were tested for RCRA
metals (total and TCLP), SVOCs, total sulfur and total sulfate.
3041161011
512
3041161011

April 2013

THIRD PARTY SIGNATURE AUTHORIZATION
for Special Waste Disposal

Date:
This Authorization is only valid for 3 years
from the above date.

To Whom It May Concern:

Please be advised that the following company/individual has been appointed to work as our
agent for purposes of managing waste materials that we may generate.

Name of Authorized Agent Title

Name of Company Telephone Number

The above broker/individual is authorized to act as our authorized agent for the following
purposes:

Complete and sign Special Waste Profile.

Complete and sign Special Waste Profile-Recertification.

Authorize amendments to Special Waste Profile.

Sign contracts to dispose and/or transport material.

Sign certifications necessary to comply with landfill requirements.

Sign manifests to initiate shipment to disposal facilities.

Our authorized agent will notify us prior to any action stated above, and will provide us with
copies of any documents bearing our name.

Name of Company Mailing Address

Generator Contact (Print Name) Title

Signature Telephone Number

01/13/2016
Billy Carden, Josh Parsley, Chris Greenway Superintendent, Assist. Superintendent, Assist. PM
CT Wilson Construction 336-285-8801
n
n
n
Historic Revolution, LLC 301 W. Main Street, Durham, NC 27701
Paul Brown Construction Services Director
919 956 4475
Acetone 0.0152 J 0.0383 J BDL BDL
Naphthalene BDL BDL 4.35 0.587
Tetrachloroethene 0.00154 0.00104 J BDL BDL
Toluene BDL BDL BDL 0.0271 J
1,2,4-Trimethylbenzene BDL BDL 0.0143 J 0.0185 J
1,2,3- Trimethylbenzene BDL BDL 0.00999 J 0.0118 J
1,2,5-Trimethylbenzene BDL BDL 0.00697 J BDL
Xylenes, Total BDL BDL BDL 0.0486 J
Acenaphthene 0.280 0.143
Acenaphthylene 0.0794 J 0.0388 J
Anthracene 0.683 0.235
Benzo(a) anthracene 1.92 0.626
Benzo(b) fluoranthene 1.89 0.785
Benzo(k) fluoranthene 0.805 0.264
Benzo(g,h,i) perylene 1.03 0.19
Benzo(a) pyrene 1.56 0.542
Chrysene 183 0 608
Not Tested
Grab Samples Composite Samples
SP-1 SP-2
Volatile Organic Compounds - EPA 8260 (mg/kg)
Semivolatile Organic Compounds - EPA 8270 (mg/kg)
Table 1
Soil Laboratory Test Results: Revolution Mill Stockpile
Greensboro. North Carolina
Not Tested
Analyte
Sample Identification
SP-1A SP-1B SP-2A SP-2B
Chrysene 1.83 0.608
Dibenz(a,h)anthracene 0.310 0.073
Fluoranthene 4.14 1.31
Fluorene 0.256 0.125
Indeno(1,2,3-cd) pyrene 0.979 0.219
Naphthalene 0.0917 J 0.290
Phenanthrene 2.62 0.827
Pyrene 3.20 0.966
Total Sulfur 95.6 J 112 J
Total Sulfate 153 99.1
Notes:
All samples were collected on January 12, 2015
bold font
Laboratory Qualifiers
Not Tested
Result exceeds reported detetion limit
J - estimated concentration for test results above the method detection limit but below the reported detection limit
< # - analyte not detected at a concentration that exceeds the minimum detection limit shown
BDL - Below Detection Limit
Sulfur/Sulfate - EPA 9056/6010 (mg/kg)
All results in mg/kg, equivalent to parts per million.
* No metals exceeded the reported detection limit for TCLP testing; total values available in lab report
P:\Self-Help Ventures Fund\Revolution Mill - 201234\Soil Testing\Soil Disposal - 2016\2016-01-13 Stockpile Page 1 of 1
ANALYTICAL REPORT
January 18, 2016
Duncklee and Dunham
Sample Delivery Group:L811879
Samples Received:01/14/2016
Project Number:201234
Description:Revolution Mills
Report To:Daphne Jones
PO Box 639
Cary, NC 27512
Entire Report Reviewed By:
January 18, 2016
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com
January 18, 2016
Jimmy Hunt
Technical Service Representative
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
¹Cp: Cover Page 1
²Tc: Table of Contents 2
³Ss: Sample Summary 3
⁴Cn: Case Narrative 5
⁵Sr: Sample Results 6
SP-1A L811879-01 6
SP-1B L811879-02 8
SP-1 L811879-03 10
SP-1 L811879-04 12
SP-2A L811879-05 13
SP-2B L811879-06 15
SP-2 L811879-07 17
SP-2 L811879-08 19
⁶Qc: Quality Control Summary 20
Total Solids by Method 2540 G-2011 20
Wet Chemistry by Method 9056A 22
Mercury by Method 7470A 23
Mercury by Method 7471A 24
Metals (ICP) by Method 6010C 25
Volatile Organic Compounds (GC/MS) by Method 8260B 28
Semi Volatile Organic Compounds (GC/MS) by Method 8270D 44
⁷Gl: Glossary of Terms 48
⁸Al: Accreditations & Locations 49
⁹Sc: Chain of Custody 50
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SP-1A L811879-01 Solid Daphne Jones 01/13/16 11:45 01/14/16 07:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG842357 1 01/14/16 13:58 01/15/16 08:41 KDW
Volatile Organic Compounds (GC/MS) by Method 8260B WG843034 1.04 01/17/16 18:42 01/17/16 23:50 ACG
Volatile Organic Compounds (GC/MS) by Method 8260B WG843055 1 01/18/16 13:00 01/18/16 13:32 ACG
Collected by Collected date/time Received date/time
SP-1B L811879-02 Solid Daphne Jones 01/13/16 11:45 01/14/16 07:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG842357 1 01/14/16 13:58 01/15/16 08:42 KDW
Volatile Organic Compounds (GC/MS) by Method 8260B WG843055 1 01/18/16 13:00 01/18/16 13:49 ACG
Collected by Collected date/time Received date/time
SP-1 L811879-03 Solid Daphne Jones 01/13/16 11:45 01/14/16 07:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG842440 1 01/15/16 15:56 01/16/16 09:27 TRB
Metals (ICP) by Method 6010C WG842325 1 01/14/16 12:14 01/14/16 15:19 RDS
Metals (ICP) by Method 6010C WG842325 1 01/14/16 12:14 01/15/16 02:12 RDS
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG842447 5 01/15/16 03:38 01/18/16 15:10 ADF
Total Solids by Method 2540 G-2011 WG842357 1 01/14/16 13:58 01/15/16 08:42 KDW
Wet Chemistry by Method 9056A WG842373 1 01/15/16 08:49 01/15/16 20:22 DJD
Collected by Collected date/time Received date/time
SP-1 L811879-04 Waste Daphne Jones 01/13/16 11:45 01/14/16 07:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG842626 1 01/15/16 11:45 01/16/16 09:31 TRB
Metals (ICP) by Method 6010C WG842596 1 01/15/16 08:55 01/15/16 18:56 WBD
Preparation by Method 1311 WG842345 1 01/14/16 12:34 01/14/16 12:35 CHM
Collected by Collected date/time Received date/time
SP-2A L811879-05 Solid Daphne Jones 01/13/16 12:50 01/14/16 07:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG842357 1 01/14/16 13:58 01/15/16 08:42 KDW
Volatile Organic Compounds (GC/MS) by Method 8260B WG842549 19.5 01/15/16 05:00 01/15/16 15:47 BMB
Collected by Collected date/time Received date/time
SP-2B L811879-06 Solid Daphne Jones 01/13/16 12:50 01/14/16 07:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG842437 1 01/14/16 16:26 01/15/16 09:30 KDW
Volatile Organic Compounds (GC/MS) by Method 8260B WG842549 24.25 01/15/16 05:00 01/15/16 16:08 BMB
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SP-2 L811879-07 Solid Daphne Jones 01/13/16 12:50 01/14/16 07:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG842440 1 01/15/16 15:56 01/16/16 09:30 TRB
Metals (ICP) by Method 6010C WG842325 1 01/14/16 12:14 01/14/16 15:22 RDS
Metals (ICP) by Method 6010C WG842325 1 01/14/16 12:14 01/15/16 02:15 RDS
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG842447 1 01/15/16 03:38 01/15/16 16:11 ADF
Total Solids by Method 2540 G-2011 WG842437 1 01/14/16 16:26 01/15/16 09:31 KDW
Wet Chemistry by Method 9056A WG842373 1 01/15/16 08:49 01/15/16 20:45 DJD
Collected by Collected date/time Received date/time
SP-2 L811879-08 Waste Daphne Jones 01/13/16 12:50 01/14/16 07:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG842626 1 01/15/16 11:45 01/16/16 09:43 TRB
Metals (ICP) by Method 6010C WG842596 1 01/15/16 08:55 01/15/16 19:08 WBD
Preparation by Method 1311 WG842345 1 01/14/16 12:34 01/14/16 12:35 CHM
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ)
values reported for environmental samples have been corrected for the dilution factor used in the
analysis. All Method and Batch Quality Control are within established criteria except where addressed
in this case narrative, a non-conformance form or properly qualified within the sample results. By my
digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the
laboratory as having the potential to affect the quality of the data have been identified by the
laboratory, and no information or data have been knowingly withheld that would affect the quality of the
data.
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Jimmy Hunt
Technical Service Representative
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L811879
SP-1A
Collected date/time: 01/13/16 11:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 81.2 1 01/15/2016 08:41 WG842357
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0152 J 0.0104 0.0640 1.04 01/17/2016 23:50 WG843034
Acrylonitrile U 0.00186 0.0128 1.04 01/17/2016 23:50 WG843034
Benzene U 0.000281 0.00128 1.04 01/17/2016 23:50 WG843034
Bromobenzene U 0.000295 0.00128 1.04 01/17/2016 23:50 WG843034
Bromodichloromethane U 0.000264 0.00128 1.04 01/17/2016 23:50 WG843034
Bromoform U 0.000441 0.00128 1.04 01/17/2016 23:50 WG843034
Bromomethane U 0.00139 0.00640 1.04 01/17/2016 23:50 WG843034
n-Butylbenzene U 0.000268 0.00128 1.04 01/17/2016 23:50 WG843034
sec-Butylbenzene U 0.000209 0.00128 1.04 01/17/2016 23:50 WG843034
tert-Butylbenzene U 0.000214 0.00128 1.04 01/17/2016 23:50 WG843034
Carbon tetrachloride U 0.000341 0.00128 1.04 01/17/2016 23:50 WG843034
Chlorobenzene U 0.000220 0.00128 1.04 01/17/2016 23:50 WG843034
Chlorodibromomethane U 0.000388 0.00128 1.04 01/17/2016 23:50 WG843034
Chloroethane U 0.000984 0.00640 1.04 01/17/2016 23:50 WG843034
2-Chloroethyl vinyl ether U 0.00243 0.0640 1.04 01/17/2016 23:50 WG843034
Chloroform U 0.000238 0.00640 1.04 01/17/2016 23:50 WG843034
Chloromethane U 0.000375 0.00308 1 01/18/2016 13:32 WG843055
2-Chlorotoluene U 0.000313 0.00128 1.04 01/17/2016 23:50 WG843034
4-Chlorotoluene U 0.000250 0.00128 1.04 01/17/2016 23:50 WG843034
1,2-Dibromo-3-Chloropropane U 0.00109 0.00640 1.04 01/17/2016 23:50 WG843034
1,2-Dibromoethane U 0.000357 0.00128 1.04 01/17/2016 23:50 WG843034
Dibromomethane U 0.000397 0.00128 1.04 01/17/2016 23:50 WG843034
1,2-Dichlorobenzene U 0.000317 0.00128 1.04 01/17/2016 23:50 WG843034
1,3-Dichlorobenzene U 0.000248 0.00128 1.04 01/17/2016 23:50 WG843034
1,4-Dichlorobenzene U 0.000235 0.00128 1.04 01/17/2016 23:50 WG843034
Dichlorodifluoromethane U 0.000742 0.00640 1.04 01/17/2016 23:50 WG843034
1,1-Dichloroethane U 0.000207 0.00128 1.04 01/17/2016 23:50 WG843034
1,2-Dichloroethane U 0.000276 0.00128 1.04 01/17/2016 23:50 WG843034
1,1-Dichloroethene U 0.000315 0.00128 1.04 01/17/2016 23:50 WG843034
cis-1,2-Dichloroethene U 0.000244 0.00128 1.04 01/17/2016 23:50 WG843034
trans-1,2-Dichloroethene U 0.000274 0.00128 1.04 01/17/2016 23:50 WG843034
1,2-Dichloropropane U 0.000372 0.00128 1.04 01/17/2016 23:50 WG843034
1,1-Dichloropropene U 0.000330 0.00128 1.04 01/17/2016 23:50 WG843034
1,3-Dichloropropane U 0.000215 0.00128 1.04 01/17/2016 23:50 WG843034
cis-1,3-Dichloropropene U 0.000272 0.00128 1.04 01/17/2016 23:50 WG843034
trans-1,3-Dichloropropene U J4 0.000278 0.00128 1.04 01/17/2016 23:50 WG843034
2,2-Dichloropropane U 0.000290 0.00128 1.04 01/17/2016 23:50 WG843034
Di-isopropyl ether U 0.000258 0.00128 1.04 01/17/2016 23:50 WG843034
Ethylbenzene U 0.000309 0.00128 1.04 01/17/2016 23:50 WG843034
Hexachloro-1,3-butadiene U 0.000356 0.00128 1.04 01/17/2016 23:50 WG843034
Isopropylbenzene U 0.000253 0.00128 1.04 01/17/2016 23:50 WG843034
p-Isopropyltoluene U 0.000212 0.00128 1.04 01/17/2016 23:50 WG843034
2-Butanone (MEK)U 0.00487 0.0128 1.04 01/17/2016 23:50 WG843034
Methylene Chloride U 0.00104 0.00640 1.04 01/17/2016 23:50 WG843034
4-Methyl-2-pentanone (MIBK)U J4 0.00196 0.0128 1.04 01/17/2016 23:50 WG843034
Methyl tert-butyl ether U 0.000220 0.00128 1.04 01/17/2016 23:50 WG843034
Naphthalene U 0.00104 0.00640 1.04 01/17/2016 23:50 WG843034
n-Propylbenzene U 0.000214 0.00128 1.04 01/17/2016 23:50 WG843034
Styrene U 0.000243 0.00128 1.04 01/17/2016 23:50 WG843034
1,1,1,2-Tetrachloroethane U 0.000274 0.00128 1.04 01/17/2016 23:50 WG843034
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L811879
SP-1A
Collected date/time: 01/13/16 11:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2,2-Tetrachloroethane U 0.000380 0.00128 1.04 01/17/2016 23:50 WG843034
1,1,2-Trichlorotrifluoroethane U 0.000380 0.00128 1.04 01/17/2016 23:50 WG843034
Tetrachloroethene 0.00154 0.000287 0.00128 1.04 01/17/2016 23:50 WG843034
Toluene U 0.000451 0.00640 1.04 01/17/2016 23:50 WG843034
1,2,3-Trichlorobenzene U 0.000318 0.00128 1.04 01/17/2016 23:50 WG843034
1,2,4-Trichlorobenzene U 0.000404 0.00128 1.04 01/17/2016 23:50 WG843034
1,1,1-Trichloroethane U 0.000297 0.00128 1.04 01/17/2016 23:50 WG843034
1,1,2-Trichloroethane U 0.000288 0.00128 1.04 01/17/2016 23:50 WG843034
Trichloroethene U 0.000290 0.00128 1.04 01/17/2016 23:50 WG843034
Trichlorofluoromethane U 0.000397 0.00640 1.04 01/17/2016 23:50 WG843034
1,2,3-Trichloropropane U 0.000771 0.00320 1.04 01/17/2016 23:50 WG843034
1,2,4-Trimethylbenzene U 0.000219 0.00128 1.04 01/17/2016 23:50 WG843034
1,2,3-Trimethylbenzene U 0.000298 0.00128 1.04 01/17/2016 23:50 WG843034
1,3,5-Trimethylbenzene U 0.000277 0.00128 1.04 01/17/2016 23:50 WG843034
Vinyl chloride U 0.000303 0.00128 1.04 01/17/2016 23:50 WG843034
Xylenes, Total U 0.000726 0.00384 1.04 01/17/2016 23:50 WG843034
(S) Toluene-d8 104 88.7-115 01/17/2016 23:50 WG843034
(S) Dibromofluoromethane 101 76.3-123 01/17/2016 23:50 WG843034
(S) 4-Bromofluorobenzene 98.9 69.7-129 01/17/2016 23:50 WG843034
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L811879
SP-1B
Collected date/time: 01/13/16 11:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 83.1 1 01/15/2016 08:42 WG842357
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0383 J 0.0100 0.0601 1 01/18/2016 13:49 WG843055
Acrylonitrile U 0.00179 0.0120 1 01/18/2016 13:49 WG843055
Benzene U 0.000270 0.00120 1 01/18/2016 13:49 WG843055
Bromobenzene U 0.000284 0.00120 1 01/18/2016 13:49 WG843055
Bromodichloromethane U 0.000254 0.00120 1 01/18/2016 13:49 WG843055
Bromoform U 0.000424 0.00120 1 01/18/2016 13:49 WG843055
Bromomethane U 0.00134 0.00601 1 01/18/2016 13:49 WG843055
n-Butylbenzene U 0.000258 0.00120 1 01/18/2016 13:49 WG843055
sec-Butylbenzene U 0.000201 0.00120 1 01/18/2016 13:49 WG843055
tert-Butylbenzene U 0.000206 0.00120 1 01/18/2016 13:49 WG843055
Carbon tetrachloride U 0.000328 0.00120 1 01/18/2016 13:49 WG843055
Chlorobenzene U 0.000212 0.00120 1 01/18/2016 13:49 WG843055
Chlorodibromomethane U 0.000373 0.00120 1 01/18/2016 13:49 WG843055
Chloroethane U 0.000946 0.00601 1 01/18/2016 13:49 WG843055
2-Chloroethyl vinyl ether U 0.00234 0.0601 1 01/18/2016 13:49 WG843055
Chloroform U 0.000229 0.00601 1 01/18/2016 13:49 WG843055
Chloromethane U 0.000375 0.00301 1 01/18/2016 13:49 WG843055
2-Chlorotoluene U J4 0.000301 0.00120 1 01/18/2016 13:49 WG843055
4-Chlorotoluene U 0.000240 0.00120 1 01/18/2016 13:49 WG843055
1,2-Dibromo-3-Chloropropane U 0.00105 0.00601 1 01/18/2016 13:49 WG843055
1,2-Dibromoethane U 0.000343 0.00120 1 01/18/2016 13:49 WG843055
Dibromomethane U 0.000382 0.00120 1 01/18/2016 13:49 WG843055
1,2-Dichlorobenzene U 0.000305 0.00120 1 01/18/2016 13:49 WG843055
1,3-Dichlorobenzene U 0.000239 0.00120 1 01/18/2016 13:49 WG843055
1,4-Dichlorobenzene U 0.000226 0.00120 1 01/18/2016 13:49 WG843055
Dichlorodifluoromethane U 0.000713 0.00601 1 01/18/2016 13:49 WG843055
1,1-Dichloroethane U 0.000199 0.00120 1 01/18/2016 13:49 WG843055
1,2-Dichloroethane U 0.000265 0.00120 1 01/18/2016 13:49 WG843055
1,1-Dichloroethene U 0.000303 0.00120 1 01/18/2016 13:49 WG843055
cis-1,2-Dichloroethene U 0.000235 0.00120 1 01/18/2016 13:49 WG843055
trans-1,2-Dichloroethene U 0.000264 0.00120 1 01/18/2016 13:49 WG843055
1,2-Dichloropropane U 0.000358 0.00120 1 01/18/2016 13:49 WG843055
1,1-Dichloropropene U 0.000317 0.00120 1 01/18/2016 13:49 WG843055
1,3-Dichloropropane U 0.000207 0.00120 1 01/18/2016 13:49 WG843055
cis-1,3-Dichloropropene U 0.000262 0.00120 1 01/18/2016 13:49 WG843055
trans-1,3-Dichloropropene U 0.000267 0.00120 1 01/18/2016 13:49 WG843055
2,2-Dichloropropane U 0.000279 0.00120 1 01/18/2016 13:49 WG843055
Di-isopropyl ether U 0.000248 0.00120 1 01/18/2016 13:49 WG843055
Ethylbenzene U 0.000297 0.00120 1 01/18/2016 13:49 WG843055
Hexachloro-1,3-butadiene U 0.000342 0.00120 1 01/18/2016 13:49 WG843055
Isopropylbenzene U 0.000243 0.00120 1 01/18/2016 13:49 WG843055
p-Isopropyltoluene U 0.000204 0.00120 1 01/18/2016 13:49 WG843055
2-Butanone (MEK)U 0.00468 0.0120 1 01/18/2016 13:49 WG843055
Methylene Chloride U 0.00100 0.00601 1 01/18/2016 13:49 WG843055
4-Methyl-2-pentanone (MIBK)U 0.00188 0.0120 1 01/18/2016 13:49 WG843055
Methyl tert-butyl ether U 0.000212 0.00120 1 01/18/2016 13:49 WG843055
Naphthalene U 0.00100 0.00601 1 01/18/2016 13:49 WG843055
n-Propylbenzene U 0.000206 0.00120 1 01/18/2016 13:49 WG843055
Styrene U 0.000234 0.00120 1 01/18/2016 13:49 WG843055
1,1,1,2-Tetrachloroethane U 0.000264 0.00120 1 01/18/2016 13:49 WG843055
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 16:11 8 of 50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 17:00 8 of 50
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L811879
SP-1B
Collected date/time: 01/13/16 11:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2,2-Tetrachloroethane U 0.000365 0.00120 1 01/18/2016 13:49 WG843055
1,1,2-Trichlorotrifluoroethane U 0.000365 0.00120 1 01/18/2016 13:49 WG843055
Tetrachloroethene 0.00104 J 0.000276 0.00120 1 01/18/2016 13:49 WG843055
Toluene U 0.000434 0.00601 1 01/18/2016 13:49 WG843055
1,2,3-Trichlorobenzene U 0.000306 0.00120 1 01/18/2016 13:49 WG843055
1,2,4-Trichlorobenzene U 0.000388 0.00120 1 01/18/2016 13:49 WG843055
1,1,1-Trichloroethane U 0.000286 0.00120 1 01/18/2016 13:49 WG843055
1,1,2-Trichloroethane U 0.000277 0.00120 1 01/18/2016 13:49 WG843055
Trichloroethene U 0.000279 0.00120 1 01/18/2016 13:49 WG843055
Trichlorofluoromethane U 0.000382 0.00601 1 01/18/2016 13:49 WG843055
1,2,3-Trichloropropane U 0.000741 0.00301 1 01/18/2016 13:49 WG843055
1,2,4-Trimethylbenzene U 0.000211 0.00120 1 01/18/2016 13:49 WG843055
1,2,3-Trimethylbenzene U 0.000287 0.00120 1 01/18/2016 13:49 WG843055
1,3,5-Trimethylbenzene U 0.000266 0.00120 1 01/18/2016 13:49 WG843055
Vinyl chloride U 0.000291 0.00120 1 01/18/2016 13:49 WG843055
Xylenes, Total U 0.000698 0.00361 1 01/18/2016 13:49 WG843055
(S) Toluene-d8 101 88.7-115 01/18/2016 13:49 WG843055
(S) Dibromofluoromethane 109 76.3-123 01/18/2016 13:49 WG843055
(S) 4-Bromofluorobenzene 97.3 69.7-129 01/18/2016 13:49 WG843055
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 16:11 9 of 50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 17:00 9 of 50
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L811879
SP-1
Collected date/time: 01/13/16 11:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 80.6 1 01/15/2016 08:42 WG842357
Wet Chemistry by Method 9056A
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Sulfate 153 0.570 62.0 1 01/15/2016 20:22 WG842373
Mercury by Method 7471A
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0654 0.00280 0.0248 1 01/16/2016 09:27 WG842440
Metals (ICP) by Method 6010C
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 0.814 J 0.650 2.48 1 01/15/2016 02:12 WG842325
Barium 105 0.170 0.620 1 01/14/2016 15:19 WG842325
Cadmium 0.546 J 0.0700 0.620 1 01/14/2016 15:19 WG842325
Chromium 11.0 0.140 1.24 1 01/14/2016 15:19 WG842325
Lead 34.9 0.190 0.620 1 01/14/2016 15:19 WG842325
Selenium U 0.740 2.48 1 01/14/2016 15:19 WG842325
Silver U 0.280 1.24 1 01/15/2016 02:12 WG842325
Sulfur 95.6 J 22.0 124 1 01/14/2016 15:19 WG842325
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.280 0.0321 0.205 5 01/18/2016 15:10 WG842447
Acenaphthylene 0.0794 J 0.0336 0.205 5 01/18/2016 15:10 WG842447
Anthracene 0.683 0.0316 0.205 5 01/18/2016 15:10 WG842447
Benzidine U 0.318 2.07 5 01/18/2016 15:10 WG842447
Benzo(a)anthracene 1.92 0.0214 0.205 5 01/18/2016 15:10 WG842447
Benzo(b)fluoranthene 1.89 0.0348 0.205 5 01/18/2016 15:10 WG842447
Benzo(k)fluoranthene 0.805 0.0291 0.205 5 01/18/2016 15:10 WG842447
Benzo(g,h,i)perylene 1.03 0.0360 0.205 5 01/18/2016 15:10 WG842447
Benzo(a)pyrene 1.56 0.0274 0.205 5 01/18/2016 15:10 WG842447
Bis(2-chlorethoxy)methane U 0.0385 2.07 5 01/18/2016 15:10 WG842447
Bis(2-chloroethyl)ether U 0.0448 2.07 5 01/18/2016 15:10 WG842447
Bis(2-chloroisopropyl)ether U 0.0380 2.07 5 01/18/2016 15:10 WG842447
4-Bromophenyl-phenylether U 0.0570 2.07 5 01/18/2016 15:10 WG842447
2-Chloronaphthalene U 0.0320 0.205 5 01/18/2016 15:10 WG842447
4-Chlorophenyl-phenylether U 0.0314 2.07 5 01/18/2016 15:10 WG842447
Chrysene 1.83 0.0278 0.205 5 01/18/2016 15:10 WG842447
Dibenz(a,h)anthracene 0.310 0.0410 0.205 5 01/18/2016 15:10 WG842447
3,3-Dichlorobenzidine U 0.397 2.07 5 01/18/2016 15:10 WG842447
2,4-Dinitrotoluene U 0.0304 2.07 5 01/18/2016 15:10 WG842447
2,6-Dinitrotoluene U 0.0368 2.07 5 01/18/2016 15:10 WG842447
Fluoranthene 4.14 0.0248 0.205 5 01/18/2016 15:10 WG842447
Fluorene 0.256 0.0341 0.205 5 01/18/2016 15:10 WG842447
Hexachlorobenzene U 0.0428 2.07 5 01/18/2016 15:10 WG842447
Hexachloro-1,3-butadiene U 0.0500 2.07 5 01/18/2016 15:10 WG842447
Hexachlorocyclopentadiene U 0.294 2.07 5 01/18/2016 15:10 WG842447
Hexachloroethane U 0.0670 2.07 5 01/18/2016 15:10 WG842447
Indeno(1,2,3-cd)pyrene 0.979 0.0386 0.205 5 01/18/2016 15:10 WG842447
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 16:11 10 of 50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 17:00 10 of 50
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L811879
SP-1
Collected date/time: 01/13/16 11:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Isophorone U 0.0261 2.07 5 01/18/2016 15:10 WG842447
Naphthalene 0.0917 J 0.0444 0.205 5 01/18/2016 15:10 WG842447
Nitrobenzene U 0.0348 2.07 5 01/18/2016 15:10 WG842447
n-Nitrosodimethylamine U 0.324 2.07 5 01/18/2016 15:10 WG842447
n-Nitrosodiphenylamine U 0.0297 2.07 5 01/18/2016 15:10 WG842447
n-Nitrosodi-n-propylamine U 0.0453 2.07 5 01/18/2016 15:10 WG842447
Phenanthrene 2.62 0.0264 0.205 5 01/18/2016 15:10 WG842447
Benzylbutyl phthalate U 0.0515 2.07 5 01/18/2016 15:10 WG842447
Bis(2-ethylhexyl)phthalate U 0.0600 2.07 5 01/18/2016 15:10 WG842447
Di-n-butyl phthalate U 0.0545 2.07 5 01/18/2016 15:10 WG842447
Diethyl phthalate U 0.0346 2.07 5 01/18/2016 15:10 WG842447
Dimethyl phthalate U 0.0270 2.07 5 01/18/2016 15:10 WG842447
Di-n-octyl phthalate U 0.0454 2.07 5 01/18/2016 15:10 WG842447
Pyrene 3.20 0.0615 0.205 5 01/18/2016 15:10 WG842447
1,2,4-Trichlorobenzene U 0.0438 2.07 5 01/18/2016 15:10 WG842447
4-Chloro-3-methylphenol U 0.0238 2.07 5 01/18/2016 15:10 WG842447
2-Chlorophenol U 0.0416 2.07 5 01/18/2016 15:10 WG842447
2,4-Dichlorophenol U 0.0373 2.07 5 01/18/2016 15:10 WG842447
2,4-Dimethylphenol U 0.236 2.07 5 01/18/2016 15:10 WG842447
4,6-Dinitro-2-methylphenol U 0.620 2.07 5 01/18/2016 15:10 WG842447
2,4-Dinitrophenol U 0.490 2.07 5 01/18/2016 15:10 WG842447
2-Nitrophenol U 0.0650 2.07 5 01/18/2016 15:10 WG842447
4-Nitrophenol U 0.262 2.07 5 01/18/2016 15:10 WG842447
Pentachlorophenol U 0.240 2.07 5 01/18/2016 15:10 WG842447
Phenol U 0.0348 2.07 5 01/18/2016 15:10 WG842447
2,4,6-Trichlorophenol U 0.0390 2.07 5 01/18/2016 15:10 WG842447
(S) 2-Fluorophenol 71.9 21.1-116 01/18/2016 15:10 WG842447
(S) Phenol-d5 76.7 26.3-121 01/18/2016 15:10 WG842447
(S) Nitrobenzene-d5 80.7 21.9-129 01/18/2016 15:10 WG842447
(S) 2-Fluorobiphenyl 77.4 34.9-129 01/18/2016 15:10 WG842447
(S) 2,4,6-Tribromophenol 78.0 21.6-142 01/18/2016 15:10 WG842447
(S) p-Terphenyl-d14 83.1 21.5-128 01/18/2016 15:10 WG842447
Sample Narrative:
8270D L811879-03 WG842447: Dilution due to matrix
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 16:11 11 of 50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 17:00 11 of 50
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L811879
SP-1
Collected date/time: 01/13/16 11:45
Preparation by Method 1311
Result Qualifier Prep Batch
Analyte date / time
TCLP Extraction -1/14/2016 12:34:31 PM WG842345
Mercury by Method 7470A
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
Mercury ND 0.0100 0.20 1 01/16/2016 09:31 WG842626
Metals (ICP) by Method 6010C
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
Arsenic ND 0.450 5 1 01/15/2016 18:56 WG842596
Barium ND 1.35 100 1 01/15/2016 18:56 WG842596
Cadmium ND 0.450 1 1 01/15/2016 18:56 WG842596
Chromium ND 0.450 5 1 01/15/2016 18:56 WG842596
Lead ND 0.450 5 1 01/15/2016 18:56 WG842596
Selenium ND 0.450 1 1 01/15/2016 18:56 WG842596
Silver ND 0.450 5 1 01/15/2016 18:56 WG842596
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 16:11 12 of 50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 17:00 12 of 50
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L811879
SP-2A
Collected date/time: 01/13/16 12:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.6 1 01/15/2016 08:42 WG842357
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.195 1.23 19.5 01/15/2016 15:47 WG842549
Acrylonitrile U 0.0349 0.245 19.5 01/15/2016 15:47 WG842549
Benzene U 0.00526 0.0245 19.5 01/15/2016 15:47 WG842549
Bromobenzene U 0.00554 0.0245 19.5 01/15/2016 15:47 WG842549
Bromodichloromethane U 0.00495 0.0245 19.5 01/15/2016 15:47 WG842549
Bromoform U 0.00827 0.0245 19.5 01/15/2016 15:47 WG842549
Bromomethane U 0.0261 0.123 19.5 01/15/2016 15:47 WG842549
n-Butylbenzene U 0.00503 0.0245 19.5 01/15/2016 15:47 WG842549
sec-Butylbenzene U 0.00392 0.0245 19.5 01/15/2016 15:47 WG842549
tert-Butylbenzene U 0.00402 0.0245 19.5 01/15/2016 15:47 WG842549
Carbon tetrachloride U 0.00640 0.0245 19.5 01/15/2016 15:47 WG842549
Chlorobenzene U 0.00413 0.0245 19.5 01/15/2016 15:47 WG842549
Chlorodibromomethane U 0.00727 0.0245 19.5 01/15/2016 15:47 WG842549
Chloroethane U 0.0184 0.123 19.5 01/15/2016 15:47 WG842549
2-Chloroethyl vinyl ether U 0.0456 1.23 19.5 01/15/2016 15:47 WG842549
Chloroform U 0.00446 0.123 19.5 01/15/2016 15:47 WG842549
Chloromethane U 0.00731 0.0613 19.5 01/15/2016 15:47 WG842549
2-Chlorotoluene U 0.00587 0.0245 19.5 01/15/2016 15:47 WG842549
4-Chlorotoluene U 0.00468 0.0245 19.5 01/15/2016 15:47 WG842549
1,2-Dibromo-3-Chloropropane U 0.0205 0.123 19.5 01/15/2016 15:47 WG842549
1,2-Dibromoethane U 0.00669 0.0245 19.5 01/15/2016 15:47 WG842549
Dibromomethane U 0.00745 0.0245 19.5 01/15/2016 15:47 WG842549
1,2-Dichlorobenzene U 0.00595 0.0245 19.5 01/15/2016 15:47 WG842549
1,3-Dichlorobenzene U 0.00466 0.0245 19.5 01/15/2016 15:47 WG842549
1,4-Dichlorobenzene U 0.00441 0.0245 19.5 01/15/2016 15:47 WG842549
Dichlorodifluoromethane U 0.0139 0.123 19.5 01/15/2016 15:47 WG842549
1,1-Dichloroethane U 0.00388 0.0245 19.5 01/15/2016 15:47 WG842549
1,2-Dichloroethane U 0.00517 0.0245 19.5 01/15/2016 15:47 WG842549
1,1-Dichloroethene U 0.00591 0.0245 19.5 01/15/2016 15:47 WG842549
cis-1,2-Dichloroethene U 0.00458 0.0245 19.5 01/15/2016 15:47 WG842549
trans-1,2-Dichloroethene U 0.00515 0.0245 19.5 01/15/2016 15:47 WG842549
1,2-Dichloropropane U 0.00698 0.0245 19.5 01/15/2016 15:47 WG842549
1,1-Dichloropropene U 0.00618 0.0245 19.5 01/15/2016 15:47 WG842549
1,3-Dichloropropane U 0.00404 0.0245 19.5 01/15/2016 15:47 WG842549
cis-1,3-Dichloropropene U 0.00511 0.0245 19.5 01/15/2016 15:47 WG842549
trans-1,3-Dichloropropene U 0.00521 0.0245 19.5 01/15/2016 15:47 WG842549
2,2-Dichloropropane U 0.00544 0.0245 19.5 01/15/2016 15:47 WG842549
Di-isopropyl ether U 0.00484 0.0245 19.5 01/15/2016 15:47 WG842549
Ethylbenzene U 0.00579 0.0245 19.5 01/15/2016 15:47 WG842549
Hexachloro-1,3-butadiene U 0.00667 0.0245 19.5 01/15/2016 15:47 WG842549
Isopropylbenzene U 0.00474 0.0245 19.5 01/15/2016 15:47 WG842549
p-Isopropyltoluene U 0.00398 0.0245 19.5 01/15/2016 15:47 WG842549
2-Butanone (MEK)U 0.0913 0.245 19.5 01/15/2016 15:47 WG842549
Methylene Chloride U 0.0195 0.123 19.5 01/15/2016 15:47 WG842549
4-Methyl-2-pentanone (MIBK)U 0.0367 0.245 19.5 01/15/2016 15:47 WG842549
Methyl tert-butyl ether U 0.00413 0.0245 19.5 01/15/2016 15:47 WG842549
Naphthalene 4.35 0.0195 0.123 19.5 01/15/2016 15:47 WG842549
n-Propylbenzene U 0.00402 0.0245 19.5 01/15/2016 15:47 WG842549
Styrene U 0.00456 0.0245 19.5 01/15/2016 15:47 WG842549
1,1,1,2-Tetrachloroethane U 0.00515 0.0245 19.5 01/15/2016 15:47 WG842549
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 16:11 13 of 50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 17:00 13 of 50
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L811879
SP-2A
Collected date/time: 01/13/16 12:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2,2-Tetrachloroethane U 0.00712 0.0245 19.5 01/15/2016 15:47 WG842549
1,1,2-Trichlorotrifluoroethane U 0.00712 0.0245 19.5 01/15/2016 15:47 WG842549
Tetrachloroethene U 0.00538 0.0245 19.5 01/15/2016 15:47 WG842549
Toluene U 0.00846 0.123 19.5 01/15/2016 15:47 WG842549
1,2,3-Trichlorobenzene U 0.00597 0.0245 19.5 01/15/2016 15:47 WG842549
1,2,4-Trichlorobenzene U 0.00757 0.0245 19.5 01/15/2016 15:47 WG842549
1,1,1-Trichloroethane U 0.00558 0.0245 19.5 01/15/2016 15:47 WG842549
1,1,2-Trichloroethane U 0.00540 0.0245 19.5 01/15/2016 15:47 WG842549
Trichloroethene U 0.00544 0.0245 19.5 01/15/2016 15:47 WG842549
Trichlorofluoromethane U 0.00745 0.123 19.5 01/15/2016 15:47 WG842549
1,2,3-Trichloropropane U 0.0144 0.0613 19.5 01/15/2016 15:47 WG842549
1,2,4-Trimethylbenzene 0.0143 J 0.00411 0.0245 19.5 01/15/2016 15:47 WG842549
1,2,3-Trimethylbenzene 0.00999 J 0.00560 0.0245 19.5 01/15/2016 15:47 WG842549
1,3,5-Trimethylbenzene 0.00697 J 0.00519 0.0245 19.5 01/15/2016 15:47 WG842549
Vinyl chloride U 0.00567 0.0245 19.5 01/15/2016 15:47 WG842549
Xylenes, Total U 0.0136 0.0735 19.5 01/15/2016 15:47 WG842549
(S) Toluene-d8 105 88.7-115 01/15/2016 15:47 WG842549
(S) Dibromofluoromethane 94.3 76.3-123 01/15/2016 15:47 WG842549
(S) 4-Bromofluorobenzene 114 69.7-129 01/15/2016 15:47 WG842549
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 17:00 14 of 50
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L811879
SP-2B
Collected date/time: 01/13/16 12:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.6 1 01/15/2016 09:30 WG842437
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.242 1.52 24.25 01/15/2016 16:08 WG842549
Acrylonitrile U 0.0434 0.305 24.25 01/15/2016 16:08 WG842549
Benzene U 0.00655 0.0305 24.25 01/15/2016 16:08 WG842549
Bromobenzene U 0.00689 0.0305 24.25 01/15/2016 16:08 WG842549
Bromodichloromethane U 0.00616 0.0305 24.25 01/15/2016 16:08 WG842549
Bromoform U 0.0103 0.0305 24.25 01/15/2016 16:08 WG842549
Bromomethane U 0.0325 0.152 24.25 01/15/2016 16:08 WG842549
n-Butylbenzene U 0.00626 0.0305 24.25 01/15/2016 16:08 WG842549
sec-Butylbenzene U 0.00487 0.0305 24.25 01/15/2016 16:08 WG842549
tert-Butylbenzene U 0.00500 0.0305 24.25 01/15/2016 16:08 WG842549
Carbon tetrachloride U 0.00795 0.0305 24.25 01/15/2016 16:08 WG842549
Chlorobenzene U 0.00514 0.0305 24.25 01/15/2016 16:08 WG842549
Chlorodibromomethane U 0.00904 0.0305 24.25 01/15/2016 16:08 WG842549
Chloroethane U 0.0229 0.152 24.25 01/15/2016 16:08 WG842549
2-Chloroethyl vinyl ether U 0.0567 1.52 24.25 01/15/2016 16:08 WG842549
Chloroform U 0.00555 0.152 24.25 01/15/2016 16:08 WG842549
Chloromethane U 0.00909 0.0761 24.25 01/15/2016 16:08 WG842549
2-Chlorotoluene U 0.00730 0.0305 24.25 01/15/2016 16:08 WG842549
4-Chlorotoluene U 0.00582 0.0305 24.25 01/15/2016 16:08 WG842549
1,2-Dibromo-3-Chloropropane U 0.0255 0.152 24.25 01/15/2016 16:08 WG842549
1,2-Dibromoethane U 0.00832 0.0305 24.25 01/15/2016 16:08 WG842549
Dibromomethane U 0.00926 0.0305 24.25 01/15/2016 16:08 WG842549
1,2-Dichlorobenzene U 0.00740 0.0305 24.25 01/15/2016 16:08 WG842549
1,3-Dichlorobenzene U 0.00580 0.0305 24.25 01/15/2016 16:08 WG842549
1,4-Dichlorobenzene U 0.00548 0.0305 24.25 01/15/2016 16:08 WG842549
Dichlorodifluoromethane U 0.0173 0.152 24.25 01/15/2016 16:08 WG842549
1,1-Dichloroethane U 0.00482 0.0305 24.25 01/15/2016 16:08 WG842549
1,2-Dichloroethane U 0.00643 0.0305 24.25 01/15/2016 16:08 WG842549
1,1-Dichloroethene U 0.00735 0.0305 24.25 01/15/2016 16:08 WG842549
cis-1,2-Dichloroethene U 0.00570 0.0305 24.25 01/15/2016 16:08 WG842549
trans-1,2-Dichloroethene U 0.00640 0.0305 24.25 01/15/2016 16:08 WG842549
1,2-Dichloropropane U 0.00868 0.0305 24.25 01/15/2016 16:08 WG842549
1,1-Dichloropropene U 0.00769 0.0305 24.25 01/15/2016 16:08 WG842549
1,3-Dichloropropane U 0.00502 0.0305 24.25 01/15/2016 16:08 WG842549
cis-1,3-Dichloropropene U 0.00635 0.0305 24.25 01/15/2016 16:08 WG842549
trans-1,3-Dichloropropene U 0.00647 0.0305 24.25 01/15/2016 16:08 WG842549
2,2-Dichloropropane U 0.00676 0.0305 24.25 01/15/2016 16:08 WG842549
Di-isopropyl ether U 0.00601 0.0305 24.25 01/15/2016 16:08 WG842549
Ethylbenzene U 0.00720 0.0305 24.25 01/15/2016 16:08 WG842549
Hexachloro-1,3-butadiene U 0.00829 0.0305 24.25 01/15/2016 16:08 WG842549
Isopropylbenzene U 0.00589 0.0305 24.25 01/15/2016 16:08 WG842549
p-Isopropyltoluene U 0.00495 0.0305 24.25 01/15/2016 16:08 WG842549
2-Butanone (MEK)U 0.113 0.305 24.25 01/15/2016 16:08 WG842549
Methylene Chloride U 0.0242 0.152 24.25 01/15/2016 16:08 WG842549
4-Methyl-2-pentanone (MIBK)U 0.0456 0.305 24.25 01/15/2016 16:08 WG842549
Methyl tert-butyl ether U 0.00514 0.0305 24.25 01/15/2016 16:08 WG842549
Naphthalene 0.587 0.0242 0.152 24.25 01/15/2016 16:08 WG842549
n-Propylbenzene U 0.00500 0.0305 24.25 01/15/2016 16:08 WG842549
Styrene U 0.00567 0.0305 24.25 01/15/2016 16:08 WG842549
1,1,1,2-Tetrachloroethane U 0.00640 0.0305 24.25 01/15/2016 16:08 WG842549
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 17:00 15 of 50
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L811879
SP-2B
Collected date/time: 01/13/16 12:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2,2-Tetrachloroethane U 0.00885 0.0305 24.25 01/15/2016 16:08 WG842549
1,1,2-Trichlorotrifluoroethane U 0.00885 0.0305 24.25 01/15/2016 16:08 WG842549
Tetrachloroethene U 0.00669 0.0305 24.25 01/15/2016 16:08 WG842549
Toluene 0.0271 J 0.0105 0.152 24.25 01/15/2016 16:08 WG842549
1,2,3-Trichlorobenzene U 0.00742 0.0305 24.25 01/15/2016 16:08 WG842549
1,2,4-Trichlorobenzene U 0.00941 0.0305 24.25 01/15/2016 16:08 WG842549
1,1,1-Trichloroethane U 0.00694 0.0305 24.25 01/15/2016 16:08 WG842549
1,1,2-Trichloroethane U 0.00672 0.0305 24.25 01/15/2016 16:08 WG842549
Trichloroethene U 0.00676 0.0305 24.25 01/15/2016 16:08 WG842549
Trichlorofluoromethane U 0.00926 0.152 24.25 01/15/2016 16:08 WG842549
1,2,3-Trichloropropane U 0.0180 0.0761 24.25 01/15/2016 16:08 WG842549
1,2,4-Trimethylbenzene 0.0185 J 0.00512 0.0305 24.25 01/15/2016 16:08 WG842549
1,2,3-Trimethylbenzene 0.0118 J 0.00696 0.0305 24.25 01/15/2016 16:08 WG842549
1,3,5-Trimethylbenzene U 0.00645 0.0305 24.25 01/15/2016 16:08 WG842549
Vinyl chloride U 0.00706 0.0305 24.25 01/15/2016 16:08 WG842549
Xylenes, Total 0.0486 J 0.0169 0.0914 24.25 01/15/2016 16:08 WG842549
(S) Toluene-d8 106 88.7-115 01/15/2016 16:08 WG842549
(S) Dibromofluoromethane 90.3 76.3-123 01/15/2016 16:08 WG842549
(S) 4-Bromofluorobenzene 111 69.7-129 01/15/2016 16:08 WG842549
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 16:11 16 of 50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 17:00 16 of 50
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L811879
SP-2
Collected date/time: 01/13/16 12:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.0 1 01/15/2016 09:31 WG842437
Wet Chemistry by Method 9056A
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Sulfate 99.1 0.570 63.3 1 01/15/2016 20:45 WG842373
Mercury by Method 7471A
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0768 0.00280 0.0253 1 01/16/2016 09:30 WG842440
Metals (ICP) by Method 6010C
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic U 0.650 2.53 1 01/15/2016 02:15 WG842325
Barium 124 0.170 0.633 1 01/14/2016 15:22 WG842325
Cadmium 0.506 J 0.0700 0.633 1 01/14/2016 15:22 WG842325
Chromium 19.0 0.140 1.27 1 01/14/2016 15:22 WG842325
Lead 47.9 0.190 0.633 1 01/14/2016 15:22 WG842325
Selenium U 0.740 2.53 1 01/14/2016 15:22 WG842325
Silver U 0.280 1.27 1 01/15/2016 02:15 WG842325
Sulfur 112 J 22.0 127 1 01/14/2016 15:22 WG842325
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.143 0.00642 0.0418 1 01/15/2016 16:11 WG842447
Acenaphthylene 0.0388 J 0.00671 0.0418 1 01/15/2016 16:11 WG842447
Anthracene 0.235 0.00632 0.0418 1 01/15/2016 16:11 WG842447
Benzidine U 0.0637 0.421 1 01/15/2016 16:11 WG842447
Benzo(a)anthracene 0.626 0.00428 0.0418 1 01/15/2016 16:11 WG842447
Benzo(b)fluoranthene 0.785 0.00695 0.0418 1 01/15/2016 16:11 WG842447
Benzo(k)fluoranthene 0.264 0.00582 0.0418 1 01/15/2016 16:11 WG842447
Benzo(g,h,i)perylene 0.190 0.00721 0.0418 1 01/15/2016 16:11 WG842447
Benzo(a)pyrene 0.542 0.00548 0.0418 1 01/15/2016 16:11 WG842447
Bis(2-chlorethoxy)methane U 0.00770 0.421 1 01/15/2016 16:11 WG842447
Bis(2-chloroethyl)ether U 0.00896 0.421 1 01/15/2016 16:11 WG842447
Bis(2-chloroisopropyl)ether U 0.00760 0.421 1 01/15/2016 16:11 WG842447
4-Bromophenyl-phenylether U 0.0114 0.421 1 01/15/2016 16:11 WG842447
2-Chloronaphthalene U 0.00639 0.0418 1 01/15/2016 16:11 WG842447
4-Chlorophenyl-phenylether U 0.00627 0.421 1 01/15/2016 16:11 WG842447
Chrysene 0.608 0.00555 0.0418 1 01/15/2016 16:11 WG842447
Dibenz(a,h)anthracene 0.0732 0.00821 0.0418 1 01/15/2016 16:11 WG842447
3,3-Dichlorobenzidine U 0.0794 0.421 1 01/15/2016 16:11 WG842447
2,4-Dinitrotoluene U 0.00607 0.421 1 01/15/2016 16:11 WG842447
2,6-Dinitrotoluene U 0.00737 0.421 1 01/15/2016 16:11 WG842447
Fluoranthene 1.31 0.00496 0.0418 1 01/15/2016 16:11 WG842447
Fluorene 0.125 0.00682 0.0418 1 01/15/2016 16:11 WG842447
Hexachlorobenzene U 0.00856 0.421 1 01/15/2016 16:11 WG842447
Hexachloro-1,3-butadiene U 0.0100 0.421 1 01/15/2016 16:11 WG842447
Hexachlorocyclopentadiene U 0.0587 0.421 1 01/15/2016 16:11 WG842447
Hexachloroethane U 0.0134 0.421 1 01/15/2016 16:11 WG842447
Indeno(1,2,3-cd)pyrene 0.219 0.00772 0.0418 1 01/15/2016 16:11 WG842447
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 16:11 17 of 50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L811879
SP-2
Collected date/time: 01/13/16 12:50
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Isophorone U 0.00522 0.421 1 01/15/2016 16:11 WG842447
Naphthalene 0.290 0.00889 0.0418 1 01/15/2016 16:11 WG842447
Nitrobenzene U 0.00695 0.421 1 01/15/2016 16:11 WG842447
n-Nitrosodimethylamine U 0.0647 0.421 1 01/15/2016 16:11 WG842447
n-Nitrosodiphenylamine U 0.00594 0.421 1 01/15/2016 16:11 WG842447
n-Nitrosodi-n-propylamine U 0.00906 0.421 1 01/15/2016 16:11 WG842447
Phenanthrene 0.827 0.00528 0.0418 1 01/15/2016 16:11 WG842447
Benzylbutyl phthalate U 0.0103 0.421 1 01/15/2016 16:11 WG842447
Bis(2-ethylhexyl)phthalate U 0.0120 0.421 1 01/15/2016 16:11 WG842447
Di-n-butyl phthalate U 0.0109 0.421 1 01/15/2016 16:11 WG842447
Diethyl phthalate U 0.00691 0.421 1 01/15/2016 16:11 WG842447
Dimethyl phthalate U 0.00540 0.421 1 01/15/2016 16:11 WG842447
Di-n-octyl phthalate U 0.00907 0.421 1 01/15/2016 16:11 WG842447
Pyrene 0.966 0.0123 0.0418 1 01/15/2016 16:11 WG842447
1,2,4-Trichlorobenzene U 0.00876 0.421 1 01/15/2016 16:11 WG842447
4-Chloro-3-methylphenol U 0.00477 0.421 1 01/15/2016 16:11 WG842447
2-Chlorophenol U 0.00831 0.421 1 01/15/2016 16:11 WG842447
2,4-Dichlorophenol U 0.00746 0.421 1 01/15/2016 16:11 WG842447
2,4-Dimethylphenol U 0.0471 0.421 1 01/15/2016 16:11 WG842447
4,6-Dinitro-2-methylphenol U 0.124 0.421 1 01/15/2016 16:11 WG842447
2,4-Dinitrophenol U 0.0980 0.421 1 01/15/2016 16:11 WG842447
2-Nitrophenol U 0.0130 0.421 1 01/15/2016 16:11 WG842447
4-Nitrophenol U 0.0525 0.421 1 01/15/2016 16:11 WG842447
Pentachlorophenol U 0.0480 0.421 1 01/15/2016 16:11 WG842447
Phenol U 0.00695 0.421 1 01/15/2016 16:11 WG842447
2,4,6-Trichlorophenol U 0.00779 0.421 1 01/15/2016 16:11 WG842447
(S) 2-Fluorophenol 68.1 21.1-116 01/15/2016 16:11 WG842447
(S) Phenol-d5 71.4 26.3-121 01/15/2016 16:11 WG842447
(S) Nitrobenzene-d5 77.6 21.9-129 01/15/2016 16:11 WG842447
(S) 2-Fluorobiphenyl 74.7 34.9-129 01/15/2016 16:11 WG842447
(S) 2,4,6-Tribromophenol 93.0 21.6-142 01/15/2016 16:11 WG842447
(S) p-Terphenyl-d14 74.2 21.5-128 01/15/2016 16:11 WG842447
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 16:11 18 of 50
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 17:00 18 of 50
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L811879
SP-2
Collected date/time: 01/13/16 12:50
Preparation by Method 1311
Result Qualifier Prep Batch
Analyte date / time
TCLP Extraction -1/14/2016 12:34:31 PM WG842345
Mercury by Method 7470A
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
Mercury ND 0.0100 0.20 1 01/16/2016 09:43 WG842626
Metals (ICP) by Method 6010C
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
Arsenic ND 0.450 5 1 01/15/2016 19:08 WG842596
Barium ND 1.35 100 1 01/15/2016 19:08 WG842596
Cadmium ND 0.450 1 1 01/15/2016 19:08 WG842596
Chromium ND 0.450 5 1 01/15/2016 19:08 WG842596
Lead ND 0.450 5 1 01/15/2016 19:08 WG842596
Selenium ND 0.450 1 1 01/15/2016 19:08 WG842596
Silver ND 0.450 5 1 01/15/2016 19:08 WG842596
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG842357
Total Solids by Method 2540 G-2011 L811879-01,02,03,05
Method Blank (MB)
(MB) 01/15/16 08:41
MB Result MB Qualifier MB RDL
Analyte %%
Total Solids 0.000900
L811908-03 Original Sample (OS) • Duplicate (DUP)
(OS) 01/15/16 08:43 • (DUP) 01/15/16 08:44
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte %% % %
Total Solids 91.7 92.0 1 0.409 5
Laboratory Control Sample (LCS)
(LCS) 01/15/16 08:41
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 99.9 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 17:00 20 of 50
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG842437
Total Solids by Method 2540 G-2011 L811879-06,07
Method Blank (MB)
(MB) 01/15/16 09:29
MB Result MB Qualifier MB RDL
Analyte %%
Total Solids 0.000800
L810990-01 Original Sample (OS) • Duplicate (DUP)
(OS) 01/15/16 09:29 • (DUP) 01/15/16 09:30
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte %% % %
Total Solids 78.4 78.1 1 0.401 5
Laboratory Control Sample (LCS)
(LCS) 01/15/16 09:29
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG842373
Wet Chemistry by Method 9056A L811879-03,07
Method Blank (MB)
(MB) 01/15/16 12:44
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Sulfate U 0.57 50.0
L812119-01 Original Sample (OS) • Duplicate (DUP)
(OS) 01/15/16 14:39 • (DUP) 01/15/16 15:01
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/kg mg/kg % %
Sulfate 26.3 26.1 1 0 15
L812119-05 Original Sample (OS) • Duplicate (DUP)
(OS) 01/15/16 21:31 • (DUP) 01/15/16 21:54
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/kg mg/kg % %
Sulfate 60.6 60.4 1 0 15
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 01/15/16 13:07 • (LCSD) 01/15/16 13:30
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Sulfate 200 204 204 102 102 80-120 0 15
L812119-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 01/15/16 15:24 • (MS) 01/15/16 15:47 • (MSD) 01/15/16 16:10
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Sulfate 500 9.08 524 525 103 103 1 80-120 0 15
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 17:00 22 of 50
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG842626
Mercury by Method 7470A L811879-04,08
Method Blank (MB)
(MB) 01/16/16 09:05
MB Result MB Qualifier MB RDL
Analyte mg/l mg/l
Mercury ND 0.0100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 01/16/16 09:08 • (LCSD) 01/16/16 09:11
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Mercury 0.0300 0.0313 0.0344 104 115 80-120 9 20
L811585-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 01/16/16 09:14 • (MS) 01/16/16 09:17 • (MSD) 01/16/16 09:20
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Mercury 0.0300 ND 0.0326 0.0286 109 95 1 75-125 13 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG842440
Mercury by Method 7471A L811879-03,07
Method Blank (MB)
(MB) 01/16/16 08:56
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0028 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 01/16/16 08:59 • (LCSD) 01/16/16 09:02
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Mercury 0.300 0.252 0.265 84 88 80-120 5 20
L811941-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 01/16/16 09:04 • (MS) 01/16/16 09:07 • (MSD) 01/16/16 09:09
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.300 0.00851 0.261 0.291 84 94 1 75-125 11 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG842325
Metals (ICP) by Method 6010C L811879-03,07
Method Blank (MB)
(MB) 01/14/16 14:30
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Arsenic U 0.65 2.00
Barium U 0.17 0.500
Cadmium U 0.07 0.500
Chromium U 0.14 1.00
Lead U 0.19 0.500
Selenium U 0.74 2.00
Silver U 0.28 1.00
Sulfur U 22 100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 01/14/16 14:33 • (LCSD) 01/14/16 14:36
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Arsenic 100 93.8 88.5 94 88 80-120 6 20
Barium 100 95.8 89.6 96 90 80-120 7 20
Cadmium 100 96.1 90.3 96 90 80-120 6 20
Chromium 100 95.0 88.3 95 88 80-120 7 20
Lead 100 95.3 89.1 95 89 80-120 7 20
Selenium 100 96.8 91.3 97 91 80-120 6 20
Silver 100 94.5 89.0 94 89 80-120 6 20
Sulfur 1000 913 858 91 86 80-120 6 20
L811908-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 01/14/16 14:39 • (MS) 01/14/16 14:48 • (MSD) 01/14/16 14:52
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Barium 100 32.2 123 121 91 89 1 75-125 2 20
Cadmium 100 0.526 107 109 107 108 1 75-125 1 20
Chromium 100 2.68 91.7 91.6 89 89 1 75-125 0 20
Lead 100 5.01 103 103 98 98 1 75-125 1 20
Selenium 100 0.670 105 108 105 107 1 75-125 2 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG842325
Metals (ICP) by Method 6010C L811879-03,07
L811908-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 01/15/16 01:56 • (MS) 01/15/16 02:05 • (MSD) 01/15/16 02:09
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Arsenic 100 2.71 110 111 107 108 1 75-125 1 20
Silver 100 0.104 112 114 112 114 1 75-125 2 20
Sulfur 1000 556 1610 1680 106 112 1 75-125 4 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG842596
Metals (ICP) by Method 6010C L811879-04,08
Method Blank (MB)
(MB) 01/15/16 18:47
MB Result MB Qualifier MB RDL
Analyte mg/l mg/l
Arsenic ND 0.450
Barium ND 1.35
Cadmium ND 0.450
Chromium ND 0.450
Lead ND 0.450
Selenium ND 0.450
Silver ND 0.450
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 01/15/16 18:50 • (LCSD) 01/15/16 18:53
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Arsenic 10.0 9.10 9.06 91 91 80-120 0 20
Barium 10.0 9.06 9.03 91 90 80-120 0 20
Cadmium 10.0 9.18 9.16 92 92 80-120 0 20
Chromium 10.0 8.77 8.79 88 88 80-120 0 20
Lead 10.0 8.93 8.90 89 89 80-120 0 20
Selenium 10.0 9.12 9.18 91 92 80-120 1 20
Silver 10.0 8.95 8.91 89 89 80-120 0 20
L811879-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 01/15/16 18:56 • (MS) 01/15/16 19:02 • (MSD) 01/15/16 19:05
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Arsenic 10.0 0.0500 9.30 9.34 92 93 1 75-125 0 20
Barium 10.0 1.00 9.77 9.81 88 88 1 75-125 0 20
Cadmium 10.0 0.00156 9.25 9.32 92 93 1 75-125 1 20
Chromium 10.0 0.00412 8.70 8.73 87 87 1 75-125 0 20
Lead 10.0 0.0125 8.93 8.94 89 89 1 75-125 0 20
Selenium 10.0 0.0251 9.46 9.54 94 95 1 75-125 1 20
Silver 10.0 0.00343 9.06 9.10 91 91 1 75-125 0 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG842549
Volatile Organic Compounds (GC/MS) by Method 8260B L811879-05,06
Method Blank (MB)
(MB) 01/15/16 06:43
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0100 0.0500
Acrylonitrile U 0.00179 0.0100
Benzene U 0.000270 0.00100
Bromobenzene U 0.000284 0.00100
Bromodichloromethane U 0.000254 0.00100
Bromoform U 0.000424 0.00100
Bromomethane U 0.00134 0.00500
n-Butylbenzene U 0.000258 0.00100
sec-Butylbenzene U 0.000201 0.00100
tert-Butylbenzene U 0.000206 0.00100
Carbon tetrachloride U 0.000328 0.00100
Chlorobenzene U 0.000212 0.00100
Chlorodibromomethane U 0.000373 0.00100
Chloroethane U 0.000946 0.00500
2-Chloroethyl vinyl ether U 0.00234 0.0500
Chloroform U 0.000229 0.00500
Chloromethane U 0.000375 0.00250
2-Chlorotoluene U 0.000301 0.00100
4-Chlorotoluene U 0.000240 0.00100
1,2-Dibromo-3-Chloropropane U 0.00105 0.00500
1,2-Dibromoethane U 0.000343 0.00100
Dibromomethane U 0.000382 0.00100
1,2-Dichlorobenzene U 0.000305 0.00100
1,3-Dichlorobenzene U 0.000239 0.00100
1,4-Dichlorobenzene U 0.000226 0.00100
Dichlorodifluoromethane U 0.000713 0.00500
1,1-Dichloroethane U 0.000199 0.00100
1,2-Dichloroethane U 0.000265 0.00100
1,1-Dichloroethene U 0.000303 0.00100
cis-1,2-Dichloroethene U 0.000235 0.00100
trans-1,2-Dichloroethene U 0.000264 0.00100
1,2-Dichloropropane U 0.000358 0.00100
1,1-Dichloropropene U 0.000317 0.00100
1,3-Dichloropropane U 0.000207 0.00100
cis-1,3-Dichloropropene U 0.000262 0.00100
trans-1,3-Dichloropropene U 0.000267 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG842549
Volatile Organic Compounds (GC/MS) by Method 8260B L811879-05,06
Method Blank (MB)
(MB) 01/15/16 06:43
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
2,2-Dichloropropane U 0.000279 0.00100
Di-isopropyl ether U 0.000248 0.00100
Ethylbenzene U 0.000297 0.00100
Hexachloro-1,3-butadiene U 0.000342 0.00100
Isopropylbenzene U 0.000243 0.00100
p-Isopropyltoluene U 0.000204 0.00100
2-Butanone (MEK)U 0.00468 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK)U 0.00188 0.0100
Methyl tert-butyl ether U 0.000212 0.00100
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.000206 0.00100
Styrene U 0.000234 0.00100
1,1,1,2-Tetrachloroethane U 0.000264 0.00100
1,1,2,2-Tetrachloroethane U 0.000365 0.00100
Tetrachloroethene U 0.000276 0.00100
Toluene U 0.000434 0.00500
1,1,2-Trichlorotrifluoroethane U 0.000365 0.00100
1,2,3-Trichlorobenzene U 0.000306 0.00100
1,2,4-Trichlorobenzene U 0.000388 0.00100
1,1,1-Trichloroethane U 0.000286 0.00100
1,1,2-Trichloroethane U 0.000277 0.00100
Trichloroethene U 0.000279 0.00100
Trichlorofluoromethane U 0.000382 0.00500
1,2,3-Trichloropropane U 0.000741 0.00250
1,2,3-Trimethylbenzene U 0.000287 0.00100
1,2,4-Trimethylbenzene U 0.000211 0.00100
1,3,5-Trimethylbenzene U 0.000266 0.00100
Vinyl chloride U 0.000291 0.00100
Xylenes, Total U 0.000698 0.00300
(S) Toluene-d8 106 88.7-115
(S) Dibromofluoromethane 97.8 76.3-123
(S) 4-Bromofluorobenzene 105 69.7-129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG842549
Volatile Organic Compounds (GC/MS) by Method 8260B L811879-05,06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 01/15/16 04:55 • (LCSD) 01/15/16 05:17
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.125 0.112 0.118 89.4 94.4 25.3-178 5.40 22.9
Acrylonitrile 0.125 0.116 0.116 93.0 92.8 57.8-143 0.230 20
Benzene 0.0250 0.0246 0.0244 98.4 97.4 72.6-120 0.980 20
Bromobenzene 0.0250 0.0228 0.0231 91.1 92.2 80.3-115 1.21 20
Bromodichloromethane 0.0250 0.0248 0.0242 99.4 96.9 75.3-119 2.52 20
Bromoform 0.0250 0.0226 0.0229 90.3 91.6 69.1-135 1.38 20
Bromomethane 0.0250 0.0241 0.0240 96.6 96.0 23.0-191 0.600 20
n-Butylbenzene 0.0250 0.0234 0.0238 93.7 95.3 74.2-134 1.71 20
sec-Butylbenzene 0.0250 0.0235 0.0238 94.0 95.3 77.8-129 1.40 20
tert-Butylbenzene 0.0250 0.0237 0.0241 95.0 96.4 77.2-129 1.47 20
Carbon tetrachloride 0.0250 0.0236 0.0227 94.5 90.9 69.4-129 3.89 20
Chlorobenzene 0.0250 0.0243 0.0240 97.1 96.2 78.9-122 0.930 20
Chlorodibromomethane 0.0250 0.0239 0.0232 95.7 92.9 76.4-126 2.94 20
Chloroethane 0.0250 0.0229 0.0242 91.5 96.9 47.2-147 5.65 20
2-Chloroethyl vinyl ether 0.125 0.122 0.122 97.4 97.5 16.7-162 0.110 23.7
Chloroform 0.0250 0.0246 0.0245 98.5 98.0 73.3-122 0.470 20
Chloromethane 0.0250 0.0260 0.0252 104 101 53.1-135 2.93 20
2-Chlorotoluene 0.0250 0.0228 0.0227 91.0 90.7 74.6-127 0.410 20
4-Chlorotoluene 0.0250 0.0242 0.0244 96.7 97.4 79.5-123 0.810 20
1,2-Dibromo-3-Chloropropane 0.0250 0.0202 0.0203 80.8 81.1 64.9-131 0.360 20
1,2-Dibromoethane 0.0250 0.0236 0.0236 94.4 94.4 78.7-123 0.0200 20
Dibromomethane 0.0250 0.0234 0.0244 93.5 97.7 78.5-117 4.38 20
1,2-Dichlorobenzene 0.0250 0.0234 0.0228 93.4 91.2 83.6-119 2.37 20
1,3-Dichlorobenzene 0.0250 0.0228 0.0231 91.0 92.4 75.9-129 1.47 20
1,4-Dichlorobenzene 0.0250 0.0224 0.0224 89.5 89.6 81.0-115 0.0700 20
Dichlorodifluoromethane 0.0250 0.0260 0.0256 104 103 50.9-139 1.23 20
1,1-Dichloroethane 0.0250 0.0250 0.0242 99.8 97.0 71.7-125 2.89 20
1,2-Dichloroethane 0.0250 0.0242 0.0242 97.0 96.8 67.2-121 0.150 20
1,1-Dichloroethene 0.0250 0.0243 0.0236 97.1 94.5 60.6-133 2.73 20
cis-1,2-Dichloroethene 0.0250 0.0237 0.0240 94.8 96.1 76.1-121 1.35 20
trans-1,2-Dichloroethene 0.0250 0.0239 0.0233 95.8 93.2 70.7-124 2.70 20
1,2-Dichloropropane 0.0250 0.0250 0.0251 100 100 76.9-123 0.0400 20
1,1-Dichloropropene 0.0250 0.0265 0.0261 106 104 71.2-126 1.67 20
1,3-Dichloropropane 0.0250 0.0246 0.0251 98.3 100 80.3-114 2.00 20
cis-1,3-Dichloropropene 0.0250 0.0262 0.0262 105 105 77.3-123 0.0400 20
trans-1,3-Dichloropropene 0.0250 0.0255 0.0260 102 104 73.0-127 1.87 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG842549
Volatile Organic Compounds (GC/MS) by Method 8260B L811879-05,06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 01/15/16 04:55 • (LCSD) 01/15/16 05:17
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
2,2-Dichloropropane 0.0250 0.0229 0.0219 91.7 87.7 61.9-132 4.51 20
Di-isopropyl ether 0.0250 0.0239 0.0232 95.6 92.6 67.2-131 3.12 20
Ethylbenzene 0.0250 0.0244 0.0240 97.7 96.1 78.6-124 1.70 20
Hexachloro-1,3-butadiene 0.0250 0.0222 0.0232 88.7 92.7 69.2-136 4.35 20
Isopropylbenzene 0.0250 0.0241 0.0238 96.4 95.2 79.4-126 1.26 20
p-Isopropyltoluene 0.0250 0.0235 0.0248 94.1 99.1 75.4-132 5.17 20
2-Butanone (MEK)0.125 0.126 0.130 101 104 44.5-154 3.48 21.3
Methylene Chloride 0.0250 0.0223 0.0216 89.4 86.4 68.2-119 3.37 20
4-Methyl-2-pentanone (MIBK)0.125 0.119 0.119 95.5 95.1 61.1-138 0.470 20
Methyl tert-butyl ether 0.0250 0.0238 0.0233 95.2 93.3 70.2-122 1.99 20
Naphthalene 0.0250 0.0216 0.0214 86.4 85.8 69.9-132 0.780 20
n-Propylbenzene 0.0250 0.0237 0.0238 94.8 95.1 80.2-124 0.300 20
Styrene 0.0250 0.0254 0.0255 102 102 79.4-124 0.420 20
1,1,1,2-Tetrachloroethane 0.0250 0.0238 0.0230 95.2 92.0 76.7-127 3.40 20
1,1,2,2-Tetrachloroethane 0.0250 0.0219 0.0214 87.4 85.8 78.8-124 1.89 20
Tetrachloroethene 0.0250 0.0245 0.0245 97.9 98.0 71.1-133 0.0800 20
Toluene 0.0250 0.0237 0.0234 94.8 93.8 76.7-116 1.12 20
1,1,2-Trichlorotrifluoroethane 0.0250 0.0196 0.0176 78.4 70.3 62.6-138 10.8 20
1,2,3-Trichlorobenzene 0.0250 0.0212 0.0215 84.8 85.9 72.5-137 1.35 20
1,2,4-Trichlorobenzene 0.0250 0.0225 0.0229 89.8 91.5 74.0-137 1.87 20
1,1,1-Trichloroethane 0.0250 0.0244 0.0241 97.5 96.5 69.9-127 0.970 20
1,1,2-Trichloroethane 0.0250 0.0240 0.0237 96.1 94.6 81.9-119 1.52 20
Trichloroethene 0.0250 0.0241 0.0237 96.4 94.9 77.2-122 1.57 20
Trichlorofluoromethane 0.0250 0.0238 0.0226 95.0 90.3 51.5-151 5.08 20
1,2,3-Trichloropropane 0.0250 0.0220 0.0215 87.9 85.8 74.0-124 2.38 20
1,2,3-Trimethylbenzene 0.0250 0.0228 0.0229 91.3 91.8 79.4-118 0.480 20
1,2,4-Trimethylbenzene 0.0250 0.0227 0.0229 90.8 91.5 77.1-124 0.770 20
1,3,5-Trimethylbenzene 0.0250 0.0231 0.0229 92.5 91.8 79.0-125 0.840 20
Vinyl chloride 0.0250 0.0250 0.0247 100 98.8 58.4-134 1.33 20
Xylenes, Total 0.0750 0.0729 0.0716 97.2 95.5 78.1-123 1.76 20
(S) Toluene-d8 105 103 88.7-115
(S) Dibromofluoromethane 100 98.6 76.3-123
(S) 4-Bromofluorobenzene 104 103 69.7-129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG842549
Volatile Organic Compounds (GC/MS) by Method 8260B L811879-05,06
L811786-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 01/15/16 12:30 • (MS) 01/15/16 07:52 • (MSD) 01/15/16 08:14
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 0.125 0.00392 0.646 0.603 103 95.8 5 10.0-130 6.92 31.5
Acrylonitrile 0.125 ND 0.610 0.596 97.6 95.4 5 39.3-152 2.24 27.2
Benzene 0.0250 ND 0.120 0.124 96.3 99.1 5 47.8-131 2.78 22.8
Bromobenzene 0.0250 ND 0.113 0.116 90.2 93.0 5 40.0-130 3.09 27.4
Bromodichloromethane 0.0250 ND 0.118 0.124 94.7 99.1 5 50.6-128 4.55 22.8
Bromoform 0.0250 ND 0.111 0.115 88.7 91.9 5 43.3-139 3.59 25.9
Bromomethane 0.0250 ND 0.110 0.124 87.7 99.1 5 5.00-189 12.2 26.7
n-Butylbenzene 0.0250 ND 0.124 0.115 99.2 92.4 5 23.6-146 7.10 39.2
sec-Butylbenzene 0.0250 ND 0.120 0.119 96.0 95.3 5 31.0-142 0.690 34.7
tert-Butylbenzene 0.0250 ND 0.120 0.124 96.1 99.0 5 36.9-142 2.92 31.7
Carbon tetrachloride 0.0250 ND 0.0946 0.104 75.7 83.2 5 46.0-140 9.43 27.2
Chlorobenzene 0.0250 ND 0.119 0.122 95.5 97.5 5 44.1-134 2.11 25.7
Chlorodibromomethane 0.0250 ND 0.117 0.119 93.4 95.0 5 49.7-134 1.68 24
Chloroethane 0.0250 ND 0.108 0.117 86.4 93.2 5 5.00-164 7.67 28.4
2-Chloroethyl vinyl ether 0.125 ND 0.607 0.619 97.1 99.1 5 5.00-159 2.06 40
Chloroform 0.0250 ND 0.118 0.124 94.5 99.4 5 51.2-133 5.02 22.8
Chloromethane 0.0250 ND 0.122 0.131 97.8 105 5 31.4-141 6.65 24.6
2-Chlorotoluene 0.0250 ND 0.113 0.114 90.5 90.9 5 36.1-137 0.400 28.9
4-Chlorotoluene 0.0250 ND 0.120 0.123 96.4 98.3 5 35.4-137 2.00 29.8
1,2-Dibromo-3-Chloropropane 0.0250 ND 0.106 0.103 84.5 82.4 5 40.4-138 2.52 30.8
1,2-Dibromoethane 0.0250 ND 0.116 0.123 93.0 98.5 5 50.2-133 5.74 23.6
Dibromomethane 0.0250 ND 0.116 0.123 92.8 98.5 5 52.4-128 5.91 23
1,2-Dichlorobenzene 0.0250 ND 0.114 0.111 91.0 88.7 5 34.6-139 2.55 29.9
1,3-Dichlorobenzene 0.0250 ND 0.115 0.116 91.7 92.8 5 28.4-142 1.25 31.2
1,4-Dichlorobenzene 0.0250 ND 0.111 0.110 88.7 87.6 5 35.0-133 1.21 31.1
Dichlorodifluoromethane 0.0250 ND 0.127 0.129 102 103 5 31.2-144 1.78 30.2
1,1-Dichloroethane 0.0250 ND 0.118 0.124 94.7 99.6 5 49.1-136 4.95 22.9
1,2-Dichloroethane 0.0250 ND 0.117 0.122 93.9 97.8 5 47.1-129 4.01 22.7
1,1-Dichloroethene 0.0250 ND 0.114 0.124 91.5 99.2 5 36.1-142 8.18 25.6
cis-1,2-Dichloroethene 0.0250 ND 0.115 0.123 92.1 98.4 5 50.6-133 6.58 23
trans-1,2-Dichloroethene 0.0250 ND 0.115 0.120 91.6 96.3 5 43.8-135 4.90 24.8
1,2-Dichloropropane 0.0250 ND 0.127 0.127 102 102 5 50.3-134 0.300 22.7
1,1-Dichloropropene 0.0250 ND 0.130 0.133 104 106 5 43.0-137 2.27 26.4
1,3-Dichloropropane 0.0250 ND 0.122 0.125 98.0 99.8 5 51.4-127 1.87 23.1
cis-1,3-Dichloropropene 0.0250 ND 0.129 0.134 104 107 5 48.4-134 3.13 23.6
trans-1,3-Dichloropropene 0.0250 ND 0.127 0.133 102 106 5 46.6-135 4.06 25.3
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 17:00 32 of 50
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG842549
Volatile Organic Compounds (GC/MS) by Method 8260B L811879-05,06
L811786-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 01/15/16 12:30 • (MS) 01/15/16 07:52 • (MSD) 01/15/16 08:14
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
2,2-Dichloropropane 0.0250 ND 0.116 0.121 92.7 96.5 5 45.2-141 4.06 26.6
Di-isopropyl ether 0.0250 ND 0.114 0.121 91.6 97.0 5 46.7-140 5.74 23.5
Ethylbenzene 0.0250 ND 0.122 0.123 97.5 98.6 5 44.8-135 1.12 26.9
Hexachloro-1,3-butadiene 0.0250 ND 0.122 0.105 98.0 84.4 5 10.0-149 14.9 40
Isopropylbenzene 0.0250 ND 0.121 0.124 96.8 99.2 5 41.9-139 2.47 29.3
p-Isopropyltoluene 0.0250 ND 0.121 0.121 96.8 96.7 5 27.3-146 0.0800 35.1
2-Butanone (MEK)0.125 ND 0.660 0.661 106 106 5 23.9-170 0.230 28.3
Methylene Chloride 0.0250 ND 0.106 0.112 85.1 89.9 5 46.7-125 5.47 22.2
4-Methyl-2-pentanone (MIBK)0.125 ND 0.588 0.617 94.0 98.7 5 42.4-146 4.82 26.7
Methyl tert-butyl ether 0.0250 ND 0.113 0.117 90.4 93.3 5 50.4-131 3.24 24.8
Naphthalene 0.0250 0.000571 0.111 0.107 88.5 85.4 5 18.4-145 3.57 34
n-Propylbenzene 0.0250 ND 0.118 0.119 94.7 95.5 5 35.2-139 0.810 31.9
Styrene 0.0250 ND 0.127 0.128 102 103 5 39.7-137 0.800 28.2
1,1,1,2-Tetrachloroethane 0.0250 ND 0.116 0.120 92.6 96.3 5 48.8-136 3.84 25.5
1,1,2,2-Tetrachloroethane 0.0250 ND 0.108 0.114 86.0 91.0 5 45.7-140 5.61 26.4
Tetrachloroethene 0.0250 ND 0.124 0.124 99.0 98.8 5 37.7-140 0.200 29.2
Toluene 0.0250 0.000208 0.118 0.120 93.9 95.8 5 47.8-127 2.05 24.3
1,1,2-Trichlorotrifluoroethane 0.0250 ND 0.0919 0.0965 73.5 77.2 5 35.7-146 4.84 28.8
1,2,3-Trichlorobenzene 0.0250 ND 0.112 0.102 89.9 81.5 5 10.0-150 9.86 38.5
1,2,4-Trichlorobenzene 0.0250 ND 0.120 0.106 95.9 84.4 5 10.0-153 12.8 39.3
1,1,1-Trichloroethane 0.0250 ND 0.122 0.127 97.9 102 5 49.0-138 3.82 25.3
1,1,2-Trichloroethane 0.0250 ND 0.120 0.121 96.4 96.6 5 52.3-132 0.220 23.4
Trichloroethene 0.0250 ND 0.116 0.120 92.8 96.4 5 48.0-132 3.75 24.8
Trichlorofluoromethane 0.0250 ND 0.107 0.124 85.9 99.5 5 12.8-169 14.7 29.7
1,2,3-Trichloropropane 0.0250 ND 0.110 0.117 87.8 94.0 5 44.4-138 6.79 26.3
1,2,3-Trimethylbenzene 0.0250 ND 0.115 0.112 92.3 89.7 5 41.0-133 2.87 27.6
1,2,4-Trimethylbenzene 0.0250 0.000139 0.115 0.117 91.7 93.3 5 32.9-139 1.77 30.6
1,3,5-Trimethylbenzene 0.0250 ND 0.116 0.116 92.5 93.2 5 37.1-138 0.690 30.6
Vinyl chloride 0.0250 ND 0.121 0.127 96.5 102 5 32.0-146 5.49 26.3
Xylenes, Total 0.0750 ND 0.361 0.367 96.4 97.8 5 42.7-135 1.47 26.6
(S) Toluene-d8 105 106 88.7-115
(S) Dibromofluoromethane 97.1 99.8 76.3-123
(S) 4-Bromofluorobenzene 103 106 69.7-129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG843034
Volatile Organic Compounds (GC/MS) by Method 8260B L811879-01
Method Blank (MB)
(MB) 01/17/16 19:18
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0100 0.0500
Acrylonitrile U 0.00179 0.0100
Benzene U 0.000270 0.00100
Bromobenzene U 0.000284 0.00100
Bromodichloromethane U 0.000254 0.00100
Bromoform U 0.000424 0.00100
Bromomethane U 0.00134 0.00500
n-Butylbenzene U 0.000258 0.00100
sec-Butylbenzene U 0.000201 0.00100
tert-Butylbenzene U 0.000206 0.00100
Carbon tetrachloride U 0.000328 0.00100
Chlorobenzene U 0.000212 0.00100
Chlorodibromomethane U 0.000373 0.00100
Chloroethane U 0.000946 0.00500
2-Chloroethyl vinyl ether U 0.00234 0.0500
Chloroform U 0.000229 0.00500
2-Chlorotoluene U 0.000301 0.00100
4-Chlorotoluene U 0.000240 0.00100
1,2-Dibromo-3-Chloropropane U 0.00105 0.00500
1,2-Dibromoethane U 0.000343 0.00100
Dibromomethane U 0.000382 0.00100
1,2-Dichlorobenzene U 0.000305 0.00100
1,3-Dichlorobenzene U 0.000239 0.00100
1,4-Dichlorobenzene U 0.000226 0.00100
Dichlorodifluoromethane U 0.000713 0.00500
1,1-Dichloroethane U 0.000199 0.00100
1,2-Dichloroethane U 0.000265 0.00100
1,1-Dichloroethene U 0.000303 0.00100
cis-1,2-Dichloroethene U 0.000235 0.00100
trans-1,2-Dichloroethene U 0.000264 0.00100
1,2-Dichloropropane U 0.000358 0.00100
1,1-Dichloropropene U 0.000317 0.00100
1,3-Dichloropropane U 0.000207 0.00100
cis-1,3-Dichloropropene U 0.000262 0.00100
trans-1,3-Dichloropropene U 0.000267 0.00100
2,2-Dichloropropane U 0.000279 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 17:00 34 of 50
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG843034
Volatile Organic Compounds (GC/MS) by Method 8260B L811879-01
Method Blank (MB)
(MB) 01/17/16 19:18
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Di-isopropyl ether U 0.000248 0.00100
Ethylbenzene U 0.000297 0.00100
Hexachloro-1,3-butadiene U 0.000342 0.00100
Isopropylbenzene U 0.000243 0.00100
p-Isopropyltoluene U 0.000204 0.00100
2-Butanone (MEK)U 0.00468 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK)U 0.00188 0.0100
Methyl tert-butyl ether U 0.000212 0.00100
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.000206 0.00100
Styrene U 0.000234 0.00100
1,1,1,2-Tetrachloroethane U 0.000264 0.00100
1,1,2,2-Tetrachloroethane U 0.000365 0.00100
Tetrachloroethene U 0.000276 0.00100
Toluene U 0.000434 0.00500
1,1,2-Trichlorotrifluoroethane U 0.000365 0.00100
1,2,3-Trichlorobenzene U 0.000306 0.00100
1,2,4-Trichlorobenzene U 0.000388 0.00100
1,1,1-Trichloroethane U 0.000286 0.00100
1,1,2-Trichloroethane U 0.000277 0.00100
Trichloroethene U 0.000279 0.00100
Trichlorofluoromethane U 0.000382 0.00500
1,2,3-Trichloropropane U 0.000741 0.00250
1,2,3-Trimethylbenzene U 0.000287 0.00100
1,2,4-Trimethylbenzene U 0.000211 0.00100
1,3,5-Trimethylbenzene U 0.000266 0.00100
Vinyl chloride U 0.000291 0.00100
Xylenes, Total U 0.000698 0.00300
(S) Toluene-d8 105 88.7-115
(S) Dibromofluoromethane 98.3 76.3-123
(S) 4-Bromofluorobenzene 101 69.7-129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Duncklee and Dunham 201234 L811879 01/18/16 17:00 35 of 50
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG843034
Volatile Organic Compounds (GC/MS) by Method 8260B L811879-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 01/17/16 17:41 • (LCSD) 01/17/16 18:00
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.125 0.140 0.148 112 118 25.3-178 5.45 22.9
Acrylonitrile 0.125 0.142 0.157 114 126 57.8-143 9.99 20
Benzene 0.0250 0.0248 0.0246 99.4 98.2 72.6-120 1.17 20
Bromobenzene 0.0250 0.0281 0.0251 112 100 80.3-115 11.2 20
Bromodichloromethane 0.0250 0.0293 0.0283 117 113 75.3-119 3.45 20
Bromoform 0.0250 0.0309 0.0270 123 108 69.1-135 13.5 20
Bromomethane 0.0250 0.0408 0.0420 163 168 23.0-191 2.87 20
n-Butylbenzene 0.0250 0.0287 0.0263 115 105 74.2-134 8.78 20
sec-Butylbenzene 0.0250 0.0237 0.0216 94.8 86.5 77.8-129 9.26 20
tert-Butylbenzene 0.0250 0.0251 0.0238 101 95.3 77.2-129 5.35 20
Carbon tetrachloride 0.0250 0.0280 0.0257 112 103 69.4-129 8.59 20
Chlorobenzene 0.0250 0.0249 0.0233 99.5 93.2 78.9-122 6.63 20
Chlorodibromomethane 0.0250 0.0289 0.0272 116 109 76.4-126 6.10 20
Chloroethane 0.0250 0.0309 0.0317 124 127 47.2-147 2.45 20
2-Chloroethyl vinyl ether 0.125 0.149 0.150 119 120 16.7-162 0.970 23.7
Chloroform 0.0250 0.0271 0.0266 108 106 73.3-122 1.85 20
2-Chlorotoluene 0.0250 0.0245 0.0226 98.0 90.4 74.6-127 8.11 20
4-Chlorotoluene 0.0250 0.0274 0.0251 110 100 79.5-123 8.83 20
1,2-Dibromo-3-Chloropropane 0.0250 0.0308 0.0273 123 109 64.9-131 12.2 20
1,2-Dibromoethane 0.0250 0.0241 0.0231 96.6 92.5 78.7-123 4.29 20
Dibromomethane 0.0250 0.0293 0.0284 117 114 78.5-117 3.12 20
1,2-Dichlorobenzene 0.0250 0.0276 0.0237 111 94.9 83.6-119 15.3 20
1,3-Dichlorobenzene 0.0250 0.0253 0.0207 101 82.9 75.9-129 19.8 20
1,4-Dichlorobenzene 0.0250 0.0268 0.0237 107 95.0 81.0-115 12.2 20
Dichlorodifluoromethane 0.0250 0.0256 0.0254 102 102 50.9-139 0.700 20
1,1-Dichloroethane 0.0250 0.0262 0.0287 105 115 71.7-125 9.14 20
1,2-Dichloroethane 0.0250 0.0297 0.0292 119 117 67.2-121 1.57 20
1,1-Dichloroethene 0.0250 0.0267 0.0282 107 113 60.6-133 5.61 20
cis-1,2-Dichloroethene 0.0250 0.0224 0.0238 89.6 95.2 76.1-121 6.08 20
trans-1,2-Dichloroethene 0.0250 0.0231 0.0249 92.3 99.6 70.7-124 7.65 20
1,2-Dichloropropane 0.0250 0.0296 0.0284 118 113 76.9-123 4.17 20
1,1-Dichloropropene 0.0250 0.0276 0.0265 110 106 71.2-126 4.24 20
1,3-Dichloropropane 0.0250 0.0273 0.0267 109 107 80.3-114 2.35 20
cis-1,3-Dichloropropene 0.0250 0.0278 0.0281 111 112 77.3-123 1.05 20
trans-1,3-Dichloropropene 0.0250 0.0319 0.0294 128 118 73.0-127 J4 8.13 20
2,2-Dichloropropane 0.0250 0.0257 0.0276 103 110 61.9-132 6.98 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Duncklee and Dunham 201234 L811879 01/18/16 17:00 36 of 50
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG843034
Volatile Organic Compounds (GC/MS) by Method 8260B L811879-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 01/17/16 17:41 • (LCSD) 01/17/16 18:00
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Di-isopropyl ether 0.0250 0.0297 0.0319 119 128 67.2-131 7.19 20
Ethylbenzene 0.0250 0.0247 0.0236 98.9 94.4 78.6-124 4.68 20
Hexachloro-1,3-butadiene 0.0250 0.0273 0.0256 109 102 69.2-136 6.63 20
Isopropylbenzene 0.0250 0.0238 0.0240 95.2 95.9 79.4-126 0.800 20
p-Isopropyltoluene 0.0250 0.0246 0.0217 98.3 86.8 75.4-132 12.4 20
2-Butanone (MEK)0.125 0.163 0.149 131 119 44.5-154 9.13 21.3
Methylene Chloride 0.0250 0.0209 0.0229 83.5 91.8 68.2-119 9.42 20
4-Methyl-2-pentanone (MIBK)0.125 0.203 0.171 162 137 61.1-138 J4 17.0 20
Methyl tert-butyl ether 0.0250 0.0249 0.0279 99.5 112 70.2-122 11.5 20
Naphthalene 0.0250 0.0252 0.0240 101 96.2 69.9-132 4.60 20
n-Propylbenzene 0.0250 0.0266 0.0247 106 98.8 80.2-124 7.24 20
Styrene 0.0250 0.0259 0.0246 104 98.3 79.4-124 5.40 20
1,1,1,2-Tetrachloroethane 0.0250 0.0289 0.0258 115 103 76.7-127 11.1 20
1,1,2,2-Tetrachloroethane 0.0250 0.0310 0.0261 124 104 78.8-124 17.5 20
Tetrachloroethene 0.0250 0.0241 0.0232 96.3 92.8 71.1-133 3.72 20
Toluene 0.0250 0.0249 0.0261 99.8 104 76.7-116 4.50 20
1,1,2-Trichlorotrifluoroethane 0.0250 0.0232 0.0249 92.6 99.7 62.6-138 7.31 20
1,2,3-Trichlorobenzene 0.0250 0.0247 0.0236 98.7 94.5 72.5-137 4.27 20
1,2,4-Trichlorobenzene 0.0250 0.0270 0.0249 108 99.5 74.0-137 8.06 20
1,1,1-Trichloroethane 0.0250 0.0272 0.0270 109 108 69.9-127 0.820 20
1,1,2-Trichloroethane 0.0250 0.0254 0.0244 102 97.5 81.9-119 4.20 20
Trichloroethene 0.0250 0.0255 0.0245 102 97.8 77.2-122 4.33 20
Trichlorofluoromethane 0.0250 0.0275 0.0280 110 112 51.5-151 1.56 20
1,2,3-Trichloropropane 0.0250 0.0303 0.0266 121 106 74.0-124 12.9 20
1,2,3-Trimethylbenzene 0.0250 0.0276 0.0255 111 102 79.4-118 8.12 20
1,2,4-Trimethylbenzene 0.0250 0.0245 0.0247 97.9 98.8 77.1-124 0.920 20
1,3,5-Trimethylbenzene 0.0250 0.0254 0.0236 102 94.5 79.0-125 7.46 20
Vinyl chloride 0.0250 0.0252 0.0258 101 103 58.4-134 2.36 20
Xylenes, Total 0.0750 0.0730 0.0694 97.3 92.6 78.1-123 5.03 20
(S) Toluene-d8 100 105 88.7-115
(S) Dibromofluoromethane 97.5 94.3 76.3-123
(S) 4-Bromofluorobenzene 99.1 100 69.7-129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 17:00 37 of 50
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG843034
Volatile Organic Compounds (GC/MS) by Method 8260B L811879-01
L811934-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 01/17/16 20:55 • (MS) 01/17/16 19:57 • (MSD) 01/17/16 20:16
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 0.125 0.540 19.5 21.2 101 110 150 10.0-130 8.62 31.5
Acrylonitrile 0.125 0.341 22.5 25.5 118 134 150 39.3-152 12.7 27.2
Benzene 0.0250 0.260 3.64 3.86 90.1 95.9 150 47.8-131 5.81 22.8
Bromobenzene 0.0250 0.0962 3.81 3.83 99.1 99.5 150 40.0-130 0.400 27.4
Bromodichloromethane 0.0250 0.0446 4.02 4.18 106 110 150 50.6-128 3.94 22.8
Bromoform 0.0250 ND 3.59 3.72 95.6 99.1 150 43.3-139 3.57 25.9
Bromomethane 0.0250 0.757 5.89 6.06 137 141 150 5.00-189 2.85 26.7
n-Butylbenzene 0.0250 0.285 4.40 4.69 110 117 150 23.6-146 6.46 39.2
sec-Butylbenzene 0.0250 0.128 3.68 3.90 94.7 101 150 31.0-142 5.91 34.7
tert-Butylbenzene 0.0250 0.0127 3.60 3.85 95.6 102 150 36.9-142 6.68 31.7
Carbon tetrachloride 0.0250 0.0148 3.81 4.20 101 111 150 46.0-140 9.54 27.2
Chlorobenzene 0.0250 0.00571 3.43 3.62 91.4 96.4 150 44.1-134 5.23 25.7
Chlorodibromomethane 0.0250 ND 3.71 3.80 98.9 101 150 49.7-134 2.39 24
Chloroethane 0.0250 0.0293 3.66 3.82 96.8 101 150 5.00-164 4.41 28.4
2-Chloroethyl vinyl ether 0.125 ND 23.4 24.9 125 133 150 5.00-159 6.15 40
Chloroform 0.0250 0.0479 4.07 4.38 107 115 150 51.2-133 7.24 22.8
2-Chlorotoluene 0.0250 0.0166 3.33 3.46 88.4 91.8 150 36.1-137 3.72 28.9
4-Chlorotoluene 0.0250 0.00715 3.72 3.86 98.9 103 150 35.4-137 3.87 29.8
1,2-Dibromo-3-Chloropropane 0.0250 ND 3.75 4.05 100 108 150 40.4-138 7.60 30.8
1,2-Dibromoethane 0.0250 ND 3.42 3.54 91.1 94.5 150 50.2-133 3.61 23.6
Dibromomethane 0.0250 ND 3.96 4.13 106 110 150 52.4-128 4.26 23
1,2-Dichlorobenzene 0.0250 0.0149 3.56 3.73 94.6 99.1 150 34.6-139 4.66 29.9
1,3-Dichlorobenzene 0.0250 ND 3.39 3.43 90.3 91.5 150 28.4-142 1.30 31.2
1,4-Dichlorobenzene 0.0250 0.0169 3.64 3.72 96.7 98.8 150 35.0-133 2.05 31.1
Dichlorodifluoromethane 0.0250 ND 3.74 3.97 99.6 106 150 31.2-144 5.96 30.2
1,1-Dichloroethane 0.0250 0.0125 3.89 4.19 103 111 150 49.1-136 7.37 22.9
1,2-Dichloroethane 0.0250 ND 4.06 4.25 108 113 150 47.1-129 4.53 22.7
1,1-Dichloroethene 0.0250 ND 3.67 3.97 98.0 106 150 36.1-142 7.73 25.6
cis-1,2-Dichloroethene 0.0250 ND 3.40 3.60 90.8 95.9 150 50.6-133 5.50 23
trans-1,2-Dichloroethene 0.0250 ND 3.20 3.45 85.4 92.1 150 43.8-135 7.56 24.8
1,2-Dichloropropane 0.0250 0.332 4.10 4.33 100 107 150 50.3-134 5.49 22.7
1,1-Dichloropropene 0.0250 ND 3.86 4.20 103 112 150 43.0-137 8.29 26.4
1,3-Dichloropropane 0.0250 ND 3.65 3.67 97.2 97.9 150 51.4-127 0.670 23.1
cis-1,3-Dichloropropene 0.0250 ND 4.07 4.14 108 110 150 48.4-134 1.74 23.6
trans-1,3-Dichloropropene 0.0250 0.140 4.29 4.31 111 111 150 46.6-135 0.360 25.3
2,2-Dichloropropane 0.0250 0.0149 3.91 4.30 104 114 150 45.2-141 9.59 26.6
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG843034
Volatile Organic Compounds (GC/MS) by Method 8260B L811879-01
L811934-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 01/17/16 20:55 • (MS) 01/17/16 19:57 • (MSD) 01/17/16 20:16
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Di-isopropyl ether 0.0250 ND 4.39 4.53 117 121 150 46.7-140 3.18 23.5
Ethylbenzene 0.0250 2.64 5.80 6.20 84.2 94.7 150 44.8-135 6.56 26.9
Hexachloro-1,3-butadiene 0.0250 ND 4.04 4.26 108 114 150 10.0-149 5.22 40
Isopropylbenzene 0.0250 0.236 3.78 4.00 94.5 100 150 41.9-139 5.70 29.3
p-Isopropyltoluene 0.0250 0.266 3.93 4.17 97.6 104 150 27.3-146 5.87 35.1
2-Butanone (MEK)0.125 0.589 21.8 24.2 113 126 150 23.9-170 10.3 28.3
Methylene Chloride 0.0250 0.0685 2.89 3.08 75.2 80.4 150 46.7-125 6.53 22.2
4-Methyl-2-pentanone (MIBK)0.125 0.386 27.1 29.3 142 154 150 42.4-146 J5 8.07 26.7
Methyl tert-butyl ether 0.0250 ND 3.63 3.80 96.9 101 150 50.4-131 4.50 24.8
Naphthalene 0.0250 1.06 4.43 4.67 89.7 96.2 150 18.4-145 5.38 34
n-Propylbenzene 0.0250 0.787 4.43 4.54 97.2 100 150 35.2-139 2.42 31.9
Styrene 0.0250 0.164 3.79 3.66 96.8 93.2 150 39.7-137 3.55 28.2
1,1,1,2-Tetrachloroethane 0.0250 ND 3.79 3.86 101 103 150 48.8-136 1.77 25.5
1,1,2,2-Tetrachloroethane 0.0250 ND 3.79 3.82 101 102 150 45.7-140 0.970 26.4
Tetrachloroethene 0.0250 ND 3.42 3.58 91.3 95.4 150 37.7-140 4.37 29.2
Toluene 0.0250 1.28 4.88 5.15 96.2 103 150 47.8-127 5.27 24.3
1,1,2-Trichlorotrifluoroethane 0.0250 ND 3.55 3.73 94.7 99.4 150 35.7-146 4.82 28.8
1,2,3-Trichlorobenzene 0.0250 0.0379 3.31 3.40 87.3 89.7 150 10.0-150 2.69 38.5
1,2,4-Trichlorobenzene 0.0250 0.0266 3.64 3.76 96.2 99.5 150 10.0-153 3.29 39.3
1,1,1-Trichloroethane 0.0250 ND 4.04 4.34 108 116 150 49.0-138 7.24 25.3
1,1,2-Trichloroethane 0.0250 0.0665 3.48 3.63 91.0 95.1 150 52.3-132 4.37 23.4
Trichloroethene 0.0250 ND 3.61 3.83 96.2 102 150 48.0-132 6.05 24.8
Trichlorofluoromethane 0.0250 ND 4.05 4.42 108 118 150 12.8-169 8.89 29.7
1,2,3-Trichloropropane 0.0250 0.0596 3.85 3.98 101 104 150 44.4-138 3.37 26.3
1,2,3-Trimethylbenzene 0.0250 2.39 5.92 6.21 94.2 102 150 41.0-133 4.72 27.6
1,2,4-Trimethylbenzene 0.0250 8.77 11.3 12.0 68.9 86.5 150 32.9-139 5.65 30.6
1,3,5-Trimethylbenzene 0.0250 2.87 6.14 6.36 87.2 93.1 150 37.1-138 3.53 30.6
Vinyl chloride 0.0250 ND 3.36 3.58 89.7 95.5 150 32.0-146 6.32 26.3
Xylenes, Total 0.0750 23.2 30.6 32.5 66.6 83.1 150 42.7-135 5.88 26.6
(S) Toluene-d8 104 105 88.7-115
(S) Dibromofluoromethane 96.5 97.9 76.3-123
(S) 4-Bromofluorobenzene 98.5 97.4 69.7-129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG843055
Volatile Organic Compounds (GC/MS) by Method 8260B L811879-01,02
Method Blank (MB)
(MB) 01/18/16 09:20
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0100 0.0500
Acrylonitrile U 0.00179 0.0100
Benzene U 0.000270 0.00100
Bromobenzene U 0.000284 0.00100
Bromodichloromethane U 0.000254 0.00100
Bromoform U 0.000424 0.00100
Bromomethane U 0.00134 0.00500
n-Butylbenzene U 0.000258 0.00100
sec-Butylbenzene U 0.000201 0.00100
tert-Butylbenzene U 0.000206 0.00100
Carbon tetrachloride U 0.000328 0.00100
Chlorobenzene U 0.000212 0.00100
Chlorodibromomethane U 0.000373 0.00100
Chloroethane U 0.000946 0.00500
2-Chloroethyl vinyl ether U 0.00234 0.0500
Chloroform U 0.000229 0.00500
Chloromethane U 0.000375 0.00250
2-Chlorotoluene U 0.000301 0.00100
4-Chlorotoluene U 0.000240 0.00100
1,2-Dibromo-3-Chloropropane U 0.00105 0.00500
1,2-Dibromoethane U 0.000343 0.00100
Dibromomethane U 0.000382 0.00100
1,2-Dichlorobenzene U 0.000305 0.00100
1,3-Dichlorobenzene U 0.000239 0.00100
1,4-Dichlorobenzene U 0.000226 0.00100
Dichlorodifluoromethane U 0.000713 0.00500
1,1-Dichloroethane U 0.000199 0.00100
1,2-Dichloroethane U 0.000265 0.00100
1,1-Dichloroethene U 0.000303 0.00100
cis-1,2-Dichloroethene U 0.000235 0.00100
trans-1,2-Dichloroethene U 0.000264 0.00100
1,2-Dichloropropane U 0.000358 0.00100
1,1-Dichloropropene U 0.000317 0.00100
1,3-Dichloropropane U 0.000207 0.00100
cis-1,3-Dichloropropene U 0.000262 0.00100
trans-1,3-Dichloropropene U 0.000267 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG843055
Volatile Organic Compounds (GC/MS) by Method 8260B L811879-01,02
Method Blank (MB)
(MB) 01/18/16 09:20
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
2,2-Dichloropropane U 0.000279 0.00100
Di-isopropyl ether U 0.000248 0.00100
Ethylbenzene U 0.000297 0.00100
Hexachloro-1,3-butadiene U 0.000342 0.00100
Isopropylbenzene U 0.000243 0.00100
p-Isopropyltoluene U 0.000204 0.00100
2-Butanone (MEK)U 0.00468 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK)U 0.00188 0.0100
Methyl tert-butyl ether U 0.000212 0.00100
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.000206 0.00100
Styrene U 0.000234 0.00100
1,1,1,2-Tetrachloroethane U 0.000264 0.00100
1,1,2,2-Tetrachloroethane U 0.000365 0.00100
Tetrachloroethene U 0.000276 0.00100
Toluene U 0.000434 0.00500
1,1,2-Trichlorotrifluoroethane U 0.000365 0.00100
1,2,3-Trichlorobenzene U 0.000306 0.00100
1,2,4-Trichlorobenzene U 0.000388 0.00100
1,1,1-Trichloroethane U 0.000286 0.00100
1,1,2-Trichloroethane U 0.000277 0.00100
Trichloroethene U 0.000279 0.00100
Trichlorofluoromethane U 0.000382 0.00500
1,2,3-Trichloropropane U 0.000741 0.00250
1,2,3-Trimethylbenzene U 0.000287 0.00100
1,2,4-Trimethylbenzene U 0.000211 0.00100
1,3,5-Trimethylbenzene U 0.000266 0.00100
Vinyl chloride U 0.000291 0.00100
Xylenes, Total U 0.000698 0.00300
(S) Toluene-d8 102 88.7-115
(S) Dibromofluoromethane 99.0 76.3-123
(S) 4-Bromofluorobenzene 103 69.7-129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG843055
Volatile Organic Compounds (GC/MS) by Method 8260B L811879-01,02
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 01/18/16 08:15 • (LCSD) 01/18/16 11:27
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.125 0.178 0.204 142 163 25.3-178 13.7 22.9
Acrylonitrile 0.125 0.130 0.131 104 105 57.8-143 0.720 20
Benzene 0.0250 0.0260 0.0269 104 108 72.6-120 3.44 20
Bromobenzene 0.0250 0.0268 0.0252 107 101 80.3-115 6.11 20
Bromodichloromethane 0.0250 0.0284 0.0275 114 110 75.3-119 3.31 20
Bromoform 0.0250 0.0292 0.0274 117 110 69.1-135 6.30 20
Bromomethane 0.0250 0.0258 0.0287 103 115 23.0-191 10.9 20
n-Butylbenzene 0.0250 0.0270 0.0270 108 108 74.2-134 0.0100 20
sec-Butylbenzene 0.0250 0.0266 0.0253 107 101 77.8-129 5.00 20
tert-Butylbenzene 0.0250 0.0268 0.0258 107 103 77.2-129 4.11 20
Carbon tetrachloride 0.0250 0.0250 0.0261 99.9 104 69.4-129 4.24 20
Chlorobenzene 0.0250 0.0269 0.0256 108 102 78.9-122 4.98 20
Chlorodibromomethane 0.0250 0.0296 0.0276 118 110 76.4-126 7.07 20
Chloroethane 0.0250 0.0248 0.0273 99.3 109 47.2-147 9.59 20
2-Chloroethyl vinyl ether 0.125 0.152 0.152 121 122 16.7-162 0.460 23.7
Chloroform 0.0250 0.0274 0.0274 110 109 73.3-122 0.120 20
Chloromethane 0.0250 0.0219 0.0254 87.7 102 53.1-135 14.6 20
2-Chlorotoluene 0.0250 0.0193 0.0173 77.3 69.4 74.6-127 J4 10.8 20
4-Chlorotoluene 0.0250 0.0275 0.0258 110 103 79.5-123 6.45 20
1,2-Dibromo-3-Chloropropane 0.0250 0.0283 0.0283 113 113 64.9-131 0.0800 20
1,2-Dibromoethane 0.0250 0.0270 0.0262 108 105 78.7-123 3.35 20
Dibromomethane 0.0250 0.0277 0.0270 111 108 78.5-117 2.44 20
1,2-Dichlorobenzene 0.0250 0.0277 0.0266 111 107 83.6-119 4.11 20
1,3-Dichlorobenzene 0.0250 0.0269 0.0244 107 97.6 75.9-129 9.61 20
1,4-Dichlorobenzene 0.0250 0.0271 0.0262 108 105 81.0-115 3.42 20
Dichlorodifluoromethane 0.0250 0.0218 0.0250 87.1 99.9 50.9-139 13.6 20
1,1-Dichloroethane 0.0250 0.0267 0.0272 107 109 71.7-125 1.75 20
1,2-Dichloroethane 0.0250 0.0276 0.0279 110 111 67.2-121 0.940 20
1,1-Dichloroethene 0.0250 0.0255 0.0277 102 111 60.6-133 8.25 20
cis-1,2-Dichloroethene 0.0250 0.0282 0.0280 113 112 76.1-121 0.630 20
trans-1,2-Dichloroethene 0.0250 0.0255 0.0273 102 109 70.7-124 6.89 20
1,2-Dichloropropane 0.0250 0.0275 0.0274 110 110 76.9-123 0.150 20
1,1-Dichloropropene 0.0250 0.0258 0.0282 103 113 71.2-126 8.85 20
1,3-Dichloropropane 0.0250 0.0271 0.0259 108 104 80.3-114 4.43 20
cis-1,3-Dichloropropene 0.0250 0.0288 0.0289 115 115 77.3-123 0.340 20
trans-1,3-Dichloropropene 0.0250 0.0278 0.0279 111 112 73.0-127 0.330 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG843055
Volatile Organic Compounds (GC/MS) by Method 8260B L811879-01,02
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 01/18/16 08:15 • (LCSD) 01/18/16 11:27
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
2,2-Dichloropropane 0.0250 0.0272 0.0271 109 109 61.9-132 0.230 20
Di-isopropyl ether 0.0250 0.0274 0.0274 110 110 67.2-131 0.0900 20
Ethylbenzene 0.0250 0.0266 0.0258 106 103 78.6-124 2.78 20
Hexachloro-1,3-butadiene 0.0250 0.0269 0.0260 107 104 69.2-136 3.09 20
Isopropylbenzene 0.0250 0.0264 0.0257 106 103 79.4-126 2.93 20
p-Isopropyltoluene 0.0250 0.0279 0.0263 112 105 75.4-132 5.87 20
2-Butanone (MEK)0.125 0.123 0.136 98.4 109 44.5-154 9.93 21.3
Methylene Chloride 0.0250 0.0267 0.0269 107 108 68.2-119 0.890 20
4-Methyl-2-pentanone (MIBK)0.125 0.136 0.136 109 109 61.1-138 0.0600 20
Methyl tert-butyl ether 0.0250 0.0272 0.0264 109 106 70.2-122 2.81 20
Naphthalene 0.0250 0.0273 0.0271 109 108 69.9-132 0.850 20
n-Propylbenzene 0.0250 0.0267 0.0258 107 103 80.2-124 3.18 20
Styrene 0.0250 0.0279 0.0261 111 104 79.4-124 6.45 20
1,1,1,2-Tetrachloroethane 0.0250 0.0284 0.0266 114 106 76.7-127 6.84 20
1,1,2,2-Tetrachloroethane 0.0250 0.0270 0.0247 108 98.8 78.8-124 8.78 20
Tetrachloroethene 0.0250 0.0255 0.0254 102 102 71.1-133 0.470 20
Toluene 0.0250 0.0271 0.0273 109 109 76.7-116 0.730 20
1,1,2-Trichlorotrifluoroethane 0.0250 0.0261 0.0273 104 109 62.6-138 4.38 20
1,2,3-Trichlorobenzene 0.0250 0.0276 0.0264 110 105 72.5-137 4.50 20
1,2,4-Trichlorobenzene 0.0250 0.0291 0.0277 117 111 74.0-137 5.14 20
1,1,1-Trichloroethane 0.0250 0.0266 0.0274 107 110 69.9-127 2.95 20
1,1,2-Trichloroethane 0.0250 0.0271 0.0258 109 103 81.9-119 5.16 20
Trichloroethene 0.0250 0.0260 0.0265 104 106 77.2-122 1.87 20
Trichlorofluoromethane 0.0250 0.0244 0.0266 97.5 106 51.5-151 8.77 20
1,2,3-Trichloropropane 0.0250 0.0280 0.0260 112 104 74.0-124 7.47 20
1,2,3-Trimethylbenzene 0.0250 0.0260 0.0260 104 104 79.4-118 0.0700 20
1,2,4-Trimethylbenzene 0.0250 0.0275 0.0258 110 103 77.1-124 6.41 20
1,3,5-Trimethylbenzene 0.0250 0.0271 0.0257 108 103 79.0-125 5.14 20
Vinyl chloride 0.0250 0.0232 0.0262 92.7 105 58.4-134 12.3 20
Xylenes, Total 0.0750 0.0799 0.0775 107 103 78.1-123 2.99 20
(S) Toluene-d8 103 102 88.7-115
(S) Dibromofluoromethane 101 102 76.3-123
(S) 4-Bromofluorobenzene 99.6 96.2 69.7-129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG842447
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L811879-03,07
Method Blank (MB)
(MB) 01/15/16 15:01
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00642 0.0330
Acenaphthylene U 0.00671 0.0330
Anthracene U 0.00632 0.0330
Benzidine U 0.0637 0.333
Benzo(a)anthracene U 0.00428 0.0330
Benzo(b)fluoranthene U 0.00695 0.0330
Benzo(k)fluoranthene U 0.00582 0.0330
Benzo(g,h,i)perylene U 0.00721 0.0330
Benzo(a)pyrene U 0.00548 0.0330
Bis(2-chlorethoxy)methane U 0.00770 0.333
Bis(2-chloroethyl)ether U 0.00896 0.333
Bis(2-chloroisopropyl)ether U 0.00760 0.333
4-Bromophenyl-phenylether U 0.0114 0.333
2-Chloronaphthalene U 0.00639 0.0330
4-Chlorophenyl-phenylether U 0.00627 0.333
Chrysene U 0.00555 0.0330
Dibenz(a,h)anthracene U 0.00821 0.0330
3,3-Dichlorobenzidine U 0.0794 0.333
2,4-Dinitrotoluene U 0.00607 0.333
2,6-Dinitrotoluene U 0.00737 0.333
Fluoranthene U 0.00496 0.0330
Fluorene U 0.00682 0.0330
Hexachlorobenzene U 0.00856 0.333
Hexachloro-1,3-butadiene U 0.0100 0.333
Hexachlorocyclopentadiene U 0.0587 0.333
Hexachloroethane U 0.0134 0.333
Indeno(1,2,3-cd)pyrene U 0.00772 0.0330
Isophorone U 0.00522 0.333
Naphthalene U 0.00889 0.0330
Nitrobenzene U 0.00695 0.333
n-Nitrosodimethylamine U 0.0647 0.333
n-Nitrosodiphenylamine U 0.00594 0.333
n-Nitrosodi-n-propylamine U 0.00906 0.333
Phenanthrene U 0.00528 0.0330
Benzylbutyl phthalate U 0.0103 0.333
Bis(2-ethylhexyl)phthalate U 0.0120 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG842447
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L811879-03,07
Method Blank (MB)
(MB) 01/15/16 15:01
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Di-n-butyl phthalate U 0.0109 0.333
Diethyl phthalate U 0.00691 0.333
Dimethyl phthalate U 0.00540 0.333
Di-n-octyl phthalate U 0.00907 0.333
Pyrene U 0.0123 0.0330
1,2,4-Trichlorobenzene U 0.00876 0.333
4-Chloro-3-methylphenol U 0.00477 0.333
2-Chlorophenol U 0.00831 0.333
2,4-Dichlorophenol U 0.00746 0.333
2,4-Dimethylphenol U 0.0471 0.333
4,6-Dinitro-2-methylphenol U 0.124 0.333
2,4-Dinitrophenol U 0.0980 0.333
2-Nitrophenol U 0.0130 0.333
4-Nitrophenol U 0.0525 0.333
Pentachlorophenol U 0.0480 0.333
Phenol U 0.00695 0.333
2,4,6-Trichlorophenol U 0.00779 0.333
(S) Nitrobenzene-d5 79.9 21.9-129
(S) 2-Fluorobiphenyl 73.3 34.9-129
(S) p-Terphenyl-d14 86.7 21.5-128
(S) Phenol-d5 78.0 26.3-121
(S) 2-Fluorophenol 75.2 21.1-116
(S) 2,4,6-Tribromophenol 79.9 21.6-142
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 01/15/16 14:14 • (LCSD) 01/15/16 14:37
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.667 0.560 0.533 84.0 80.0 48.9-107 4.95 20
Acenaphthylene 0.667 0.560 0.532 84.0 79.8 49.2-111 5.08 20
Anthracene 0.667 0.571 0.549 85.6 82.4 52.0-112 3.81 20
Benzidine 0.667 ND ND 5.09 4.12 0.000-48.0 20.9 40
Benzo(a)anthracene 0.667 0.553 0.544 83.0 81.5 52.3-106 1.76 20
Benzo(b)fluoranthene 0.667 0.555 0.518 83.2 77.6 51.3-106 6.98 20
Benzo(k)fluoranthene 0.667 0.564 0.551 84.6 82.7 52.9-107 2.32 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG842447
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L811879-03,07
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 01/15/16 14:14 • (LCSD) 01/15/16 14:37
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Benzo(g,h,i)perylene 0.667 0.573 0.560 85.9 84.0 45.8-108 2.23 20
Benzo(a)pyrene 0.667 0.566 0.556 84.8 83.3 51.9-106 1.72 20
Bis(2-chlorethoxy)methane 0.667 0.521 0.516 78.2 77.3 44.9-108 1.12 20
Bis(2-chloroethyl)ether 0.667 0.524 0.505 78.6 75.7 32.5-112 3.73 26
Bis(2-chloroisopropyl)ether 0.667 0.521 0.500 78.0 75.0 40.4-99.0 4.03 20.7
4-Bromophenyl-phenylether 0.667 0.534 0.521 80.1 78.1 51.4-110 2.56 20
2-Chloronaphthalene 0.667 0.537 0.510 80.4 76.4 47.1-105 5.15 20
4-Chlorophenyl-phenylether 0.667 0.549 0.519 82.3 77.8 48.1-108 5.58 20
Chrysene 0.667 0.547 0.548 82.0 82.2 54.4-110 0.280 20
Dibenz(a,h)anthracene 0.667 0.569 0.559 85.3 83.8 45.7-111 1.85 20
3,3-Dichlorobenzidine 0.667 0.503 0.479 75.4 71.8 21.0-101 4.83 22
2,4-Dinitrotoluene 0.667 0.635 0.607 95.2 91.0 53.0-112 4.52 20
2,6-Dinitrotoluene 0.667 0.585 0.570 87.7 85.4 51.6-110 2.64 20
Fluoranthene 0.667 0.564 0.554 84.6 83.0 53.7-110 1.89 20
Fluorene 0.667 0.564 0.532 84.6 79.7 51.1-109 5.91 20
Hexachlorobenzene 0.667 0.536 0.528 80.3 79.1 43.2-104 1.51 20.1
Hexachloro-1,3-butadiene 0.667 0.498 0.480 74.7 71.9 41.5-112 3.78 20
Hexachlorocyclopentadiene 0.667 0.345 0.337 51.7 50.5 13.5-123 2.34 20.7
Hexachloroethane 0.667 0.523 0.511 78.4 76.6 36.2-103 2.34 22.7
Indeno(1,2,3-cd)pyrene 0.667 0.580 0.565 87.0 84.8 47.5-109 2.54 20
Isophorone 0.667 0.600 0.576 89.9 86.3 28.8-104 4.06 20
Naphthalene 0.667 0.496 0.481 74.4 72.2 43.4-103 3.01 20
Nitrobenzene 0.667 0.580 0.563 87.0 84.4 40.7-109 3.07 21
n-Nitrosodimethylamine 0.667 0.508 0.492 76.1 73.7 18.1-122 3.23 23.5
n-Nitrosodiphenylamine 0.667 0.535 0.520 80.3 77.9 48.8-107 2.95 20
n-Nitrosodi-n-propylamine 0.667 0.553 0.537 82.9 80.4 43.3-109 3.03 20
Phenanthrene 0.667 0.546 0.528 81.8 79.1 51.6-107 3.33 20
Benzylbutyl phthalate 0.667 0.621 0.622 93.2 93.2 47.5-115 0.0400 20
Bis(2-ethylhexyl)phthalate 0.667 0.635 0.629 95.2 94.2 48.1-116 1.02 20.5
Di-n-butyl phthalate 0.667 0.612 0.594 91.8 89.1 49.7-113 3.02 20
Diethyl phthalate 0.667 0.640 0.604 95.9 90.5 52.0-112 5.84 20
Dimethyl phthalate 0.667 0.566 0.544 84.9 81.6 51.4-108 3.99 20
Di-n-octyl phthalate 0.667 0.629 0.619 94.3 92.8 49.6-112 1.67 22
Pyrene 0.667 0.551 0.552 82.6 82.7 47.1-108 0.100 20
1,2,4-Trichlorobenzene 0.667 0.477 0.463 71.5 69.4 39.8-100 2.98 20
4-Chloro-3-methylphenol 0.667 0.603 0.587 90.4 88.0 51.1-113 2.67 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG842447
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L811879-03,07
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 01/15/16 14:14 • (LCSD) 01/15/16 14:37
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
2-Chlorophenol 0.667 0.491 0.480 73.7 72.0 40.8-103 2.28 20
2,4-Dichlorophenol 0.667 0.534 0.521 80.0 78.1 46.2-109 2.38 20
2,4-Dimethylphenol 0.667 0.564 0.537 84.6 80.5 42.2-110 4.96 20
4,6-Dinitro-2-methylphenol 0.667 0.656 0.652 98.4 97.7 23.1-119 0.690 23.7
2,4-Dinitrophenol 0.667 0.435 0.421 65.2 63.1 10.0-105 3.28 36.5
2-Nitrophenol 0.667 0.624 0.611 93.5 91.5 44.2-113 2.10 20.9
4-Nitrophenol 0.667 0.639 0.600 95.8 90.0 34.8-109 6.27 20
Pentachlorophenol 0.667 0.669 0.646 100 96.9 16.2-102 3.48 22.9
Phenol 0.667 0.522 0.497 78.2 74.6 41.5-106 4.74 20
2,4,6-Trichlorophenol 0.667 0.574 0.531 86.1 79.5 44.4-108 7.89 20
(S) Nitrobenzene-d5 83.0 80.8 21.9-129
(S) 2-Fluorobiphenyl 74.9 71.8 34.9-129
(S) p-Terphenyl-d14 82.8 83.0 21.5-128
(S) Phenol-d5 77.2 74.8 26.3-121
(S) 2-Fluorophenol 78.6 74.9 21.1-116
(S) 2,4,6-Tribromophenol 92.6 90.7 21.6-142
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 17:00 47 of 50
ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Abbreviations and Definitions
SDG Sample Delivery Group.
MDL Method Detection Limit.
RDL Reported Detection Limit.
ND,U Not detected at the Reporting Limit (or MDL where applicable).
RPD Relative Percent Difference.
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry
report basis for soils].
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.Recovery.
SDL Sample Detection Limit.
MQL Method Quantitation Limit.
Unadj. MQL Unadjusted Method Quantitation Limit.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is
high.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please
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1461.02A2LA – ISO 170255
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Duncklee and Dunham 201234 L811879 01/18/16 17:00 49 of 50
DIVIDER PAGE
Republic Services, Inc.
18500 N. Allied Way, Phoenix, AZ 85054
SPECIAL WASTE DEPARTMENT DECISION
Waste Profile #3041164111 Expiration Date9/16/2016
I. Decision Request:Initial Recertification Change
Disposal Facility:3041 - Uwharrie Environmental Regional MSW Landfill
Generator Name:Historic Revolution LLC
Generator Site Address:1200 N. Revolution Mill Drive, Greensboro, NC
City:Greensboro County:State:NC Zip:
Name of Waste:Excavated sediment
Estimated Annual Volume:260 Cubic Yards
II. Special Waste Department Decision: Approved Rejected
Management Method(s):Landfill Solidification Bioremediation Transfer Facility
Problematic Special Waste according to Republic?Yes No
If yes, which one?
Approved by Special Waste Review Committee?Yes No Not Applicable
Precautions, Conditions or Limitations on Approval


Special Waste Analyst Signature:____________________________Name (Printed):Holly Bradley
Date: 3/16/2016
III. Facility Decision:Approved Rejected
Precautions, Conditions or Limitations on Approval

By signing below, the General Manager or Designee agrees that a fully executed Special Waste Service Agreement is on file for this profile and that the
special waste file is complete.
General Manager or Designee:_____________________________Name (Printed):_____________________________
Date: 3/16/2016
X
Joe Reynolds, Site Manager
SPECIAL WASTE PROFILE 3DJHRI
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5HTXHVWHG'LVSRVDO)DFLOLW\



6DYHDEOHILOOLQIRUP5HVWULFWHGSULQWLQJXQWLODOOUHTXLUHG\HOORZILHOGVDUHFRPSOHWHG
:DVWH3URILOH


I. Generator Information 6DOHV5HS
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II. Billing Information
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III. Waste Stream Information
1DPHRI:DVWH
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7\SHRI:DVWH,1'8675,$/352&(66:$67(32//87,21&21752/:$67(
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IV. Representative Sample Certification 126$03/(7$.(1
,VWKHUHSUHVHQWDWLYHVDPSOHFROOHFWHGWRSUHSDUHWKLVSURILOHDQGODERUDWRU\DQDO\VLV
FROOHFWHGLQDFFRUGDQFHZLWK86(3$&)5FJXLGHOLQHVRUHTXLYDOHQWUXOHV"<(6RU12
7\SHRI6DPSOH &20326,7(6$03/(*5$%6$03/(
6DPSOe Date
Sample ID Numbers:
3041 Uwharrie Environmental LF NC
Historic Revolution LLC
1200 N. Revolution Mill Drive
Greensboro Guilford North Carolina 27405
N/A N/A
✔301 W. Main Street
Durham Durham North Carolina 27701
Paul Brown [e-mail]
[phone]
CT Wilson Construction Company Kate White
P.O. Box 2011 [e-mail]
Durham NC 27702 [phone]
Excavated Sediment
Runoff from soil on site into concrete-lined reservoir that was once used as the fire water source when Revolution Mill
operated. Owner recently drained reservoir to clean out sediment on concrete base so they could tie new stormwater
system into reservoir.
✔
✔
✔
260 Cubic Yards
✔
✔
✔
2/19/2016
✔✔
PS-1A, PS-1B- two grab samples tested for VOCs;
PS-1 composite sample with four aliquots; two aliquots from the VOC grab locations and two
addtiional locations from sediment in base of reservoir. This composite sample was tested for RCRA
metals (total), ran lead after total results for TCLP lead, SVOCs, total sulfur and total sulfate. See
attached table and lab report.
Lab report revised to include missing parameters (creosols, 1,4-dichlorobenzene, pyridine, and
2,4,5-trichlorophenol). 1,4-dichlorobenzene included in 8260 VOC analysis.
3041164111
512
3041164111

April 2013

THIRD PARTY SIGNATURE AUTHORIZATION
for Special Waste Disposal

Date:
This Authorization is only valid for 3 years
from the above date.

To Whom It May Concern:

Please be advised that the following company/individual has been appointed to work as our
agent for purposes of managing waste materials that we may generate.

Name of Authorized Agent Title

Name of Company Telephone Number

The above broker/individual is authorized to act as our authorized agent for the following
purposes:

Complete and sign Special Waste Profile.

Complete and sign Special Waste Profile-Recertification.

Authorize amendments to Special Waste Profile.

Sign contracts to dispose and/or transport material.

Sign certifications necessary to comply with landfill requirements.

Sign manifests to initiate shipment to disposal facilities.

Our authorized agent will notify us prior to any action stated above, and will provide us with
copies of any documents bearing our name.

Name of Company Mailing Address

Generator Contact (Print Name) Title

Signature Telephone Number

February 22, 2016
Daphne Jones/Sean Jarvah Sr. Geologist/Field Ops Mgr.
Solutions-IES Inc. [phone] x139/x122
n
n
n
n
Historic Revolution LLC 301 W. Main Street, Durham, NC 27701
Paul Brown Construction Services Director
919-956-4475
Composite
Sample
Acetone 0.441 0.662
2-Butanone 0.113 0.0856
Acenaphthene 0.162
Acenaphthylene 0.0198 J
Anthracene 0.372
Benzo(a) anthracene 1.55
Benzo(b) fluoranthene 2.09
Benzo(k) fluoranthene 0.697
Benzo(g,h,i) perylene 0.582
Benzo(a) pyrene 1.32
Chrysene 1.62
Dibenz(a,h)anthracene 0.180
Fluoranthene 3.27
Fluorene 0.124
Indeno(1,2,3-cd) pyrene 0.577
Naphthalene 0.0347 J
Phenanthrene 1.96
Pyrene 2.85
Arsenic 3.41 J
Barium 133
Cadmium 0.724 J
Chromium 16.2
Lead 433
Lead, TCLP 0.771 mg/L
Mercury 0.0899
Total Sulfur 860
Total Sulfate 30.6 J
Notes:
All results in mg/kg except TCLP lead result in mg/L, equivalent to parts per million.
bold font
Laboratory Qualifiers

Table 1
Sediment Laboratory Test Results: Revolution Mill Reservoir
Greensboro. North Carolina
Not Tested
PS-1
Samples collected on 2/19/2016. The composite sample for PS-1 includes four aliquots, two
from the location of the VOC grab sample locations and two additional samples collected at
random locations between 4 and 12 inches below the top of the accumulated sediment on top of
the concrete base of the reservoir.. Sediment very thin (less than 2 inches thick) in central
portion of reservoir.
Volatile Organic Compounds - EPA 8260 (mg/kg)
Semivolatile Organic Compounds - EPA 8270 (mg/kg)
Not Tested
Not Tested
Grab Samples
Analyte
Sample Identification
PS-1A PS-1B
J - estimated concentration for test results that exceed the method detection limit but are
below the reported detection limit
< # - analyte not detected at a concentration that exceeds the minimum detection limit shown
BDL - Below Detection Limit
Metals/Sulfur/Sulfate - EPA 6010/7471/9056 (mg/kg except as noted)
Result exceeds reported detetion
limit
T:\Project Files\Self-Help\Revolution Mill\7. Working Documents\Soil Testing\Sediment Testing - Feb 2016\2016-03-01 Sediment Page 1 of 1
ANALYTICAL REPORT
March 03, 2016
Solutions-IES
Sample Delivery Group:L819039
Samples Received:02/20/2016
Project Number:16018
Description:Revolution Mill
Report To:Daphne Jones
1101 Nowell Road
Raleigh, NC 27607
Entire Report Reviewed By:
March 03, 2016
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com
March 03, 2016
Jimmy Hunt
Technical Service Representative
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
¹Cp: Cover Page 1
²Tc: Table of Contents 2
³Ss: Sample Summary 3
⁴Cn: Case Narrative 4
⁵Sr: Sample Results 5
PS-1A 8IN L819039-01 5
PS-1B 14IN L819039-02 7
PS-1 12-4IN L819039-03 9
PS-1 12-4IN L819039-04 11
⁶Qc: Quality Control Summary 12
Total Solids by Method 2540 G-2011 12
Wet Chemistry by Method 9056A 13
Mercury by Method 7471A 14
Metals (ICP) by Method 6010C 15
Volatile Organic Compounds (GC/MS) by Method 8260B 17
Semi Volatile Organic Compounds (GC/MS) by Method 8270D 23
⁷Gl: Glossary of Terms 29
⁸Al: Accreditations & Locations 30
⁹Sc: Chain of Custody 31
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Solutions-IES 16018 L819039 03/03/16 14:10 2 of 32
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
PS-1A 8IN L819039-01 Solid 02/19/16 09:15 02/20/16 07:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG851398 1 02/23/16 09:29 02/23/16 09:41 KDW
Volatile Organic Compounds (GC/MS) by Method 8260B WG851267 1 02/28/16 11:50 02/28/16 21:32 ACG
Collected by Collected date/time Received date/time
PS-1B 14IN L819039-02 Solid 02/19/16 09:25 02/20/16 07:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG851398 1 02/23/16 09:29 02/23/16 09:41 KDW
Volatile Organic Compounds (GC/MS) by Method 8260B WG851267 1 02/28/16 11:50 02/28/16 21:52 ACG
Collected by Collected date/time Received date/time
PS-1 12-4IN L819039-03 Solid 02/19/16 09:40 02/20/16 07:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG851139 1 02/23/16 15:13 02/24/16 10:07 BRJ
Metals (ICP) by Method 6010C WG851082 1 02/23/16 08:38 02/23/16 17:58 CCE
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG851554 1 02/23/16 16:47 02/24/16 17:24 JF
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG851554 5 02/23/16 16:47 02/25/16 22:32 JF
Total Solids by Method 2540 G-2011 WG851398 1 02/23/16 09:29 02/23/16 09:41 KDW
Wet Chemistry by Method 9056A WG851727 1 02/24/16 20:55 02/25/16 01:00 DJD
Collected by Collected date/time Received date/time
PS-1 12-4IN L819039-04 Waste 02/19/16 09:40 02/20/16 07:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Metals (ICP) by Method 6010C WG853598 1 03/03/16 09:51 03/03/16 11:30 LTB
Preparation by Method 1311 WG853340 1 03/02/16 11:29 03/02/16 11:30 BG
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Solutions-IES 16018 L819039 03/03/16 13:50 3 of 32
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Solutions-IES 16018 L819039 03/03/16 14:10 3 of 32
ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ)
values reported for environmental samples have been corrected for the dilution factor used in the
analysis. All Method and Batch Quality Control are within established criteria except where addressed
in this case narrative, a non-conformance form or properly qualified within the sample results. By my
digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the
laboratory as having the potential to affect the quality of the data have been identified by the
laboratory, and no information or data have been knowingly withheld that would affect the quality of the
data.
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Solutions-IES 16018 L819039 03/03/16 13:50 4 of 32
Jimmy Hunt
Technical Service Representative
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Solutions-IES 16018 L819039 03/03/16 14:10 4 of 32
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L819039
PS-1A 8IN
Collected date/time: 02/19/16 09:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 25.2 1 02/23/2016 09:41 WG851398
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.441 0.0100 0.198 1 02/28/2016 21:32 WG851267
Acrylonitrile U 0.00179 0.0397 1 02/28/2016 21:32 WG851267
Benzene U 0.000270 0.00397 1 02/28/2016 21:32 WG851267
Bromobenzene U 0.000284 0.00397 1 02/28/2016 21:32 WG851267
Bromodichloromethane U 0.000254 0.00397 1 02/28/2016 21:32 WG851267
Bromoform U 0.000424 0.00397 1 02/28/2016 21:32 WG851267
Bromomethane U 0.00134 0.0198 1 02/28/2016 21:32 WG851267
n-Butylbenzene U 0.000258 0.00397 1 02/28/2016 21:32 WG851267
sec-Butylbenzene U 0.000201 0.00397 1 02/28/2016 21:32 WG851267
tert-Butylbenzene U 0.000206 0.00397 1 02/28/2016 21:32 WG851267
Carbon tetrachloride U 0.000328 0.00397 1 02/28/2016 21:32 WG851267
Chlorobenzene U 0.000212 0.00397 1 02/28/2016 21:32 WG851267
Chlorodibromomethane U 0.000373 0.00397 1 02/28/2016 21:32 WG851267
Chloroethane U 0.000946 0.0198 1 02/28/2016 21:32 WG851267
2-Chloroethyl vinyl ether U 0.00234 0.198 1 02/28/2016 21:32 WG851267
Chloroform U 0.000229 0.0198 1 02/28/2016 21:32 WG851267
Chloromethane U 0.000375 0.00992 1 02/28/2016 21:32 WG851267
2-Chlorotoluene U 0.000301 0.00397 1 02/28/2016 21:32 WG851267
4-Chlorotoluene U 0.000240 0.00397 1 02/28/2016 21:32 WG851267
1,2-Dibromo-3-Chloropropane U J4 0.00105 0.0198 1 02/28/2016 21:32 WG851267
1,2-Dibromoethane U 0.000343 0.00397 1 02/28/2016 21:32 WG851267
Dibromomethane U 0.000382 0.00397 1 02/28/2016 21:32 WG851267
1,2-Dichlorobenzene U 0.000305 0.00397 1 02/28/2016 21:32 WG851267
1,3-Dichlorobenzene U 0.000239 0.00397 1 02/28/2016 21:32 WG851267
1,4-Dichlorobenzene U 0.000226 0.00397 1 02/28/2016 21:32 WG851267
Dichlorodifluoromethane U J4 0.000713 0.0198 1 02/28/2016 21:32 WG851267
1,1-Dichloroethane U 0.000199 0.00397 1 02/28/2016 21:32 WG851267
1,2-Dichloroethane U 0.000265 0.00397 1 02/28/2016 21:32 WG851267
1,1-Dichloroethene U 0.000303 0.00397 1 02/28/2016 21:32 WG851267
cis-1,2-Dichloroethene U 0.000235 0.00397 1 02/28/2016 21:32 WG851267
trans-1,2-Dichloroethene U 0.000264 0.00397 1 02/28/2016 21:32 WG851267
1,2-Dichloropropane U 0.000358 0.00397 1 02/28/2016 21:32 WG851267
1,1-Dichloropropene U 0.000317 0.00397 1 02/28/2016 21:32 WG851267
1,3-Dichloropropane U 0.000207 0.00397 1 02/28/2016 21:32 WG851267
cis-1,3-Dichloropropene U 0.000262 0.00397 1 02/28/2016 21:32 WG851267
trans-1,3-Dichloropropene U 0.000267 0.00397 1 02/28/2016 21:32 WG851267
2,2-Dichloropropane U 0.000279 0.00397 1 02/28/2016 21:32 WG851267
Di-isopropyl ether U 0.000248 0.00397 1 02/28/2016 21:32 WG851267
Ethylbenzene U 0.000297 0.00397 1 02/28/2016 21:32 WG851267
Hexachloro-1,3-butadiene U 0.000342 0.00397 1 02/28/2016 21:32 WG851267
Isopropylbenzene U 0.000243 0.00397 1 02/28/2016 21:32 WG851267
p-Isopropyltoluene U 0.000204 0.00397 1 02/28/2016 21:32 WG851267
2-Butanone (MEK)0.113 0.00468 0.0397 1 02/28/2016 21:32 WG851267
Methylene Chloride U 0.00100 0.0198 1 02/28/2016 21:32 WG851267
4-Methyl-2-pentanone (MIBK)U 0.00188 0.0397 1 02/28/2016 21:32 WG851267
Methyl tert-butyl ether U 0.000212 0.00397 1 02/28/2016 21:32 WG851267
Naphthalene U 0.00100 0.0198 1 02/28/2016 21:32 WG851267
n-Propylbenzene U 0.000206 0.00397 1 02/28/2016 21:32 WG851267
Styrene U 0.000234 0.00397 1 02/28/2016 21:32 WG851267
1,1,1,2-Tetrachloroethane U 0.000264 0.00397 1 02/28/2016 21:32 WG851267
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L819039
PS-1A 8IN
Collected date/time: 02/19/16 09:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2,2-Tetrachloroethane U 0.000365 0.00397 1 02/28/2016 21:32 WG851267
1,1,2-Trichlorotrifluoroethane U 0.000365 0.00397 1 02/28/2016 21:32 WG851267
Tetrachloroethene U 0.000276 0.00397 1 02/28/2016 21:32 WG851267
Toluene U 0.000434 0.0198 1 02/28/2016 21:32 WG851267
1,2,3-Trichlorobenzene U 0.000306 0.00397 1 02/28/2016 21:32 WG851267
1,2,4-Trichlorobenzene U 0.000388 0.00397 1 02/28/2016 21:32 WG851267
1,1,1-Trichloroethane U 0.000286 0.00397 1 02/28/2016 21:32 WG851267
1,1,2-Trichloroethane U 0.000277 0.00397 1 02/28/2016 21:32 WG851267
Trichloroethene U 0.000279 0.00397 1 02/28/2016 21:32 WG851267
Trichlorofluoromethane U 0.000382 0.0198 1 02/28/2016 21:32 WG851267
1,2,3-Trichloropropane U 0.000741 0.00992 1 02/28/2016 21:32 WG851267
1,2,4-Trimethylbenzene U 0.000211 0.00397 1 02/28/2016 21:32 WG851267
1,2,3-Trimethylbenzene U 0.000287 0.00397 1 02/28/2016 21:32 WG851267
1,3,5-Trimethylbenzene U 0.000266 0.00397 1 02/28/2016 21:32 WG851267
Vinyl chloride U 0.000291 0.00397 1 02/28/2016 21:32 WG851267
Xylenes, Total U 0.000698 0.0119 1 02/28/2016 21:32 WG851267
(S) Toluene-d8 104 88.7-115 02/28/2016 21:32 WG851267
(S) Dibromofluoromethane 53.6 J2 76.3-123 02/28/2016 21:32 WG851267
(S) 4-Bromofluorobenzene 90.0 69.7-129 02/28/2016 21:32 WG851267
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L819039
PS-1B 14IN
Collected date/time: 02/19/16 09:25
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 45.3 1 02/23/2016 09:41 WG851398
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.662 0.0100 0.110 1 02/28/2016 21:52 WG851267
Acrylonitrile U 0.00179 0.0221 1 02/28/2016 21:52 WG851267
Benzene U 0.000270 0.00221 1 02/28/2016 21:52 WG851267
Bromobenzene U 0.000284 0.00221 1 02/28/2016 21:52 WG851267
Bromodichloromethane U 0.000254 0.00221 1 02/28/2016 21:52 WG851267
Bromoform U 0.000424 0.00221 1 02/28/2016 21:52 WG851267
Bromomethane U 0.00134 0.0110 1 02/28/2016 21:52 WG851267
n-Butylbenzene U 0.000258 0.00221 1 02/28/2016 21:52 WG851267
sec-Butylbenzene U 0.000201 0.00221 1 02/28/2016 21:52 WG851267
tert-Butylbenzene U 0.000206 0.00221 1 02/28/2016 21:52 WG851267
Carbon tetrachloride U 0.000328 0.00221 1 02/28/2016 21:52 WG851267
Chlorobenzene U 0.000212 0.00221 1 02/28/2016 21:52 WG851267
Chlorodibromomethane U 0.000373 0.00221 1 02/28/2016 21:52 WG851267
Chloroethane U 0.000946 0.0110 1 02/28/2016 21:52 WG851267
2-Chloroethyl vinyl ether U 0.00234 0.110 1 02/28/2016 21:52 WG851267
Chloroform U 0.000229 0.0110 1 02/28/2016 21:52 WG851267
Chloromethane U 0.000375 0.00551 1 02/28/2016 21:52 WG851267
2-Chlorotoluene U 0.000301 0.00221 1 02/28/2016 21:52 WG851267
4-Chlorotoluene U 0.000240 0.00221 1 02/28/2016 21:52 WG851267
1,2-Dibromo-3-Chloropropane U J4 0.00105 0.0110 1 02/28/2016 21:52 WG851267
1,2-Dibromoethane U 0.000343 0.00221 1 02/28/2016 21:52 WG851267
Dibromomethane U 0.000382 0.00221 1 02/28/2016 21:52 WG851267
1,2-Dichlorobenzene U 0.000305 0.00221 1 02/28/2016 21:52 WG851267
1,3-Dichlorobenzene U 0.000239 0.00221 1 02/28/2016 21:52 WG851267
1,4-Dichlorobenzene U 0.000226 0.00221 1 02/28/2016 21:52 WG851267
Dichlorodifluoromethane U J4 0.000713 0.0110 1 02/28/2016 21:52 WG851267
1,1-Dichloroethane U 0.000199 0.00221 1 02/28/2016 21:52 WG851267
1,2-Dichloroethane U 0.000265 0.00221 1 02/28/2016 21:52 WG851267
1,1-Dichloroethene U 0.000303 0.00221 1 02/28/2016 21:52 WG851267
cis-1,2-Dichloroethene U 0.000235 0.00221 1 02/28/2016 21:52 WG851267
trans-1,2-Dichloroethene U 0.000264 0.00221 1 02/28/2016 21:52 WG851267
1,2-Dichloropropane U 0.000358 0.00221 1 02/28/2016 21:52 WG851267
1,1-Dichloropropene U 0.000317 0.00221 1 02/28/2016 21:52 WG851267
1,3-Dichloropropane U 0.000207 0.00221 1 02/28/2016 21:52 WG851267
cis-1,3-Dichloropropene U 0.000262 0.00221 1 02/28/2016 21:52 WG851267
trans-1,3-Dichloropropene U 0.000267 0.00221 1 02/28/2016 21:52 WG851267
2,2-Dichloropropane U 0.000279 0.00221 1 02/28/2016 21:52 WG851267
Di-isopropyl ether U 0.000248 0.00221 1 02/28/2016 21:52 WG851267
Ethylbenzene U 0.000297 0.00221 1 02/28/2016 21:52 WG851267
Hexachloro-1,3-butadiene U 0.000342 0.00221 1 02/28/2016 21:52 WG851267
Isopropylbenzene U 0.000243 0.00221 1 02/28/2016 21:52 WG851267
p-Isopropyltoluene U 0.000204 0.00221 1 02/28/2016 21:52 WG851267
2-Butanone (MEK)0.0856 0.00468 0.0221 1 02/28/2016 21:52 WG851267
Methylene Chloride U 0.00100 0.0110 1 02/28/2016 21:52 WG851267
4-Methyl-2-pentanone (MIBK)U 0.00188 0.0221 1 02/28/2016 21:52 WG851267
Methyl tert-butyl ether U 0.000212 0.00221 1 02/28/2016 21:52 WG851267
Naphthalene U 0.00100 0.0110 1 02/28/2016 21:52 WG851267
n-Propylbenzene U 0.000206 0.00221 1 02/28/2016 21:52 WG851267
Styrene U 0.000234 0.00221 1 02/28/2016 21:52 WG851267
1,1,1,2-Tetrachloroethane U 0.000264 0.00221 1 02/28/2016 21:52 WG851267
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L819039
PS-1B 14IN
Collected date/time: 02/19/16 09:25
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2,2-Tetrachloroethane U 0.000365 0.00221 1 02/28/2016 21:52 WG851267
1,1,2-Trichlorotrifluoroethane U 0.000365 0.00221 1 02/28/2016 21:52 WG851267
Tetrachloroethene U 0.000276 0.00221 1 02/28/2016 21:52 WG851267
Toluene U 0.000434 0.0110 1 02/28/2016 21:52 WG851267
1,2,3-Trichlorobenzene U 0.000306 0.00221 1 02/28/2016 21:52 WG851267
1,2,4-Trichlorobenzene U 0.000388 0.00221 1 02/28/2016 21:52 WG851267
1,1,1-Trichloroethane U 0.000286 0.00221 1 02/28/2016 21:52 WG851267
1,1,2-Trichloroethane U 0.000277 0.00221 1 02/28/2016 21:52 WG851267
Trichloroethene U 0.000279 0.00221 1 02/28/2016 21:52 WG851267
Trichlorofluoromethane U 0.000382 0.0110 1 02/28/2016 21:52 WG851267
1,2,3-Trichloropropane U 0.000741 0.00551 1 02/28/2016 21:52 WG851267
1,2,4-Trimethylbenzene U 0.000211 0.00221 1 02/28/2016 21:52 WG851267
1,2,3-Trimethylbenzene U 0.000287 0.00221 1 02/28/2016 21:52 WG851267
1,3,5-Trimethylbenzene U 0.000266 0.00221 1 02/28/2016 21:52 WG851267
Vinyl chloride U 0.000291 0.00221 1 02/28/2016 21:52 WG851267
Xylenes, Total U 0.000698 0.00662 1 02/28/2016 21:52 WG851267
(S) Toluene-d8 103 88.7-115 02/28/2016 21:52 WG851267
(S) Dibromofluoromethane 63.0 J2 76.3-123 02/28/2016 21:52 WG851267
(S) 4-Bromofluorobenzene 91.6 69.7-129 02/28/2016 21:52 WG851267
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L819039
PS-1 12-4IN
Collected date/time: 02/19/16 09:40
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 40.0 1 02/23/2016 09:41 WG851398
Wet Chemistry by Method 9056A
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Sulfate 30.6 J 0.570 125 1 02/25/2016 01:00 WG851727
Mercury by Method 7471A
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0899 0.00280 0.0499 1 02/24/2016 10:07 WG851139
Metals (ICP) by Method 6010C
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 3.41 J 0.650 4.99 1 02/23/2016 17:58 WG851082
Barium 133 0.170 1.25 1 02/23/2016 17:58 WG851082
Cadmium 0.724 J 0.0700 1.25 1 02/23/2016 17:58 WG851082
Chromium 16.2 0.140 2.50 1 02/23/2016 17:58 WG851082
Lead 433 0.190 1.25 1 02/23/2016 17:58 WG851082
Selenium U 0.740 4.99 1 02/23/2016 17:58 WG851082
Silver U 0.280 2.50 1 02/23/2016 17:58 WG851082
Sulfur 860 22.0 250 1 02/23/2016 17:58 WG851082
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.162 0.00642 0.0824 1 02/24/2016 17:24 WG851554
Acenaphthylene 0.0198 J 0.00671 0.0824 1 02/24/2016 17:24 WG851554
Anthracene 0.372 0.00632 0.0824 1 02/24/2016 17:24 WG851554
Benzidine U 0.0637 0.831 1 02/24/2016 17:24 WG851554
Benzo(a)anthracene 1.55 0.00428 0.0824 1 02/24/2016 17:24 WG851554
Benzo(b)fluoranthene 2.09 0.00695 0.0824 1 02/24/2016 17:24 WG851554
Benzo(k)fluoranthene 0.697 0.00582 0.0824 1 02/24/2016 17:24 WG851554
Benzo(g,h,i)perylene 0.582 0.00721 0.0824 1 02/24/2016 17:24 WG851554
Benzo(a)pyrene 1.32 0.00548 0.0824 1 02/24/2016 17:24 WG851554
Bis(2-chlorethoxy)methane U 0.00770 0.831 1 02/24/2016 17:24 WG851554
Bis(2-chloroethyl)ether U 0.00896 0.831 1 02/24/2016 17:24 WG851554
Bis(2-chloroisopropyl)ether U 0.00760 0.831 1 02/24/2016 17:24 WG851554
4-Bromophenyl-phenylether U 0.0114 0.831 1 02/24/2016 17:24 WG851554
2-Chloronaphthalene U 0.00639 0.0824 1 02/24/2016 17:24 WG851554
4-Chlorophenyl-phenylether U 0.00627 0.831 1 02/24/2016 17:24 WG851554
Chrysene 1.62 0.00555 0.0824 1 02/24/2016 17:24 WG851554
Dibenz(a,h)anthracene 0.180 0.00821 0.0824 1 02/24/2016 17:24 WG851554
3,3-Dichlorobenzidine U 0.0794 0.831 1 02/24/2016 17:24 WG851554
2,4-Dinitrotoluene U 0.00607 0.831 1 02/24/2016 17:24 WG851554
2,6-Dinitrotoluene U 0.00737 0.831 1 02/24/2016 17:24 WG851554
Fluoranthene 3.27 0.0248 0.412 5 02/25/2016 22:32 WG851554
Fluorene 0.124 0.00682 0.0824 1 02/24/2016 17:24 WG851554
Hexachlorobenzene U 0.00856 0.831 1 02/24/2016 17:24 WG851554
Hexachloro-1,3-butadiene U 0.0100 0.831 1 02/24/2016 17:24 WG851554
Hexachlorocyclopentadiene U 0.0587 0.831 1 02/24/2016 17:24 WG851554
Hexachloroethane U 0.0134 0.831 1 02/24/2016 17:24 WG851554
Indeno(1,2,3-cd)pyrene 0.577 0.00772 0.0824 1 02/24/2016 17:24 WG851554
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L819039
PS-1 12-4IN
Collected date/time: 02/19/16 09:40
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Isophorone U 0.00522 0.831 1 02/24/2016 17:24 WG851554
Naphthalene 0.0347 J 0.00889 0.0824 1 02/24/2016 17:24 WG851554
Nitrobenzene U 0.00695 0.831 1 02/24/2016 17:24 WG851554
n-Nitrosodimethylamine U 0.0647 0.831 1 02/24/2016 17:24 WG851554
n-Nitrosodiphenylamine U 0.00594 0.831 1 02/24/2016 17:24 WG851554
n-Nitrosodi-n-propylamine U 0.00906 0.831 1 02/24/2016 17:24 WG851554
Phenanthrene 1.96 0.00528 0.0824 1 02/24/2016 17:24 WG851554
Benzylbutyl phthalate U 0.0103 0.831 1 02/24/2016 17:24 WG851554
Bis(2-ethylhexyl)phthalate U 0.0120 0.831 1 02/24/2016 17:24 WG851554
Di-n-butyl phthalate U 0.0109 0.831 1 02/24/2016 17:24 WG851554
Diethyl phthalate U 0.00691 0.831 1 02/24/2016 17:24 WG851554
Dimethyl phthalate U 0.00540 0.831 1 02/24/2016 17:24 WG851554
Di-n-octyl phthalate U 0.00907 0.831 1 02/24/2016 17:24 WG851554
Pyrene 2.85 0.0123 0.0824 1 02/24/2016 17:24 WG851554
1,2,4-Trichlorobenzene U 0.00876 0.831 1 02/24/2016 17:24 WG851554
4-Chloro-3-methylphenol U 0.00477 0.831 1 02/24/2016 17:24 WG851554
2-Chlorophenol U 0.00831 0.831 1 02/24/2016 17:24 WG851554
2,4-Dichlorophenol U 0.00746 0.831 1 02/24/2016 17:24 WG851554
2,4-Dimethylphenol U 0.0471 0.831 1 02/24/2016 17:24 WG851554
4,6-Dinitro-2-methylphenol U 0.124 0.831 1 02/24/2016 17:24 WG851554
2,4-Dinitrophenol U 0.0980 0.831 1 02/24/2016 17:24 WG851554
2-Nitrophenol U 0.0130 0.831 1 02/24/2016 17:24 WG851554
4-Nitrophenol U 0.0525 0.831 1 02/24/2016 17:24 WG851554
Pentachlorophenol U 0.0480 0.831 1 02/24/2016 17:24 WG851554
Phenol U 0.00695 0.831 1 02/24/2016 17:24 WG851554
2,4,6-Trichlorophenol U 0.00779 0.831 1 02/24/2016 17:24 WG851554
(S) 2-Fluorophenol 70.2 21.1-116 02/24/2016 17:24 WG851554
(S) Phenol-d5 59.8 26.3-121 02/24/2016 17:24 WG851554
(S) Nitrobenzene-d5 67.1 21.9-129 02/24/2016 17:24 WG851554
(S) 2-Fluorobiphenyl 68.5 34.9-129 02/24/2016 17:24 WG851554
(S) 2,4,6-Tribromophenol 93.7 21.6-142 02/24/2016 17:24 WG851554
(S) p-Terphenyl-d14 53.1 21.5-128 02/24/2016 17:24 WG851554
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L819039
PS-1 12-4IN
Collected date/time: 02/19/16 09:40
Preparation by Method 1311
Result Qualifier Prep Batch
Analyte date / time
TCLP Extraction -3/2/2016 11:29:59 AM WG853340
Metals (ICP) by Method 6010C
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
Lead 0.771 0.450 5 1 03/03/2016 11:30 WG853598
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG851398
Total Solids by Method 2540 G-2011 L819039-01,02,03
Method Blank (MB)
(MB) 02/23/16 09:41
MB Result MB Qualifier MB RDL
Analyte %%
Total Solids 0.000400
L819044-01 Original Sample (OS) • Duplicate (DUP)
(OS) 02/23/16 09:41 • (DUP) 02/23/16 09:41
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte %% % %
Total Solids 91.2 91.7 1 0.558 5
Laboratory Control Sample (LCS)
(LCS) 02/23/16 09:41
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG851727
Wet Chemistry by Method 9056A L819039-03
Method Blank (MB)
(MB) 02/24/16 23:06
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Sulfate U 0.57 50.0
L819039-03 Original Sample (OS) • Duplicate (DUP)
(OS) 02/25/16 01:00 • (DUP) 02/25/16 01:23
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/kg mg/kg % %
Sulfate 12.3 10.9 1 12 J 15
L819628-02 Original Sample (OS) • Duplicate (DUP)
(OS) 02/25/16 06:44 • (DUP) 02/25/16 07:07
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/kg mg/kg % %
Sulfate 35.5 36.1 1 2 J 15
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 02/24/16 23:28 • (LCSD) 02/24/16 23:51
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Sulfate 200 217 220 108 110 80-120 1 15
L819628-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 02/25/16 04:49 • (MS) 02/25/16 05:12 • (MSD) 02/25/16 05:35
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Sulfate 500 28.9 557 547 106 104 1 80-120 2 15
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG851139
Mercury by Method 7471A L819039-03
Method Blank (MB)
(MB) 02/24/16 09:08
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0028 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 02/24/16 09:11 • (LCSD) 02/24/16 09:14
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Mercury 0.300 0.289 0.295 96 98 80-120 2 20
L819175-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 02/24/16 09:17 • (MS) 02/24/16 09:20 • (MSD) 02/24/16 09:29
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.300 0.0122 0.293 0.297 94 95 1 75-125 1 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG851082
Metals (ICP) by Method 6010C L819039-03
Method Blank (MB)
(MB) 02/23/16 17:08
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Arsenic U 0.65 2.00
Barium U 0.17 0.500
Cadmium U 0.07 0.500
Chromium U 0.14 1.00
Lead 1.13 0.19 0.500
Selenium U 0.74 2.00
Silver U 0.28 1.00
Sulfur U 22 100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 02/23/16 17:11 • (LCSD) 02/23/16 17:14
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Arsenic 100 94.1 102 94 102 80-120 8 20
Barium 100 96.1 104 96 104 80-120 8 20
Cadmium 100 94.1 102 94 102 80-120 8 20
Chromium 100 95.6 103 96 103 80-120 8 20
Lead 100 95.9 104 96 104 80-120 8 20
Selenium 100 95.8 104 96 104 80-120 8 20
Silver 100 91.5 99.0 91 99 80-120 8 20
Sulfur 1000 880 950 88 95 80-120 8 20
L818950-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 02/23/16 17:17 • (MS) 02/23/16 17:26 • (MSD) 02/23/16 17:28
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Arsenic 100 5.18 101 98.2 96 93 1 75-125 3 20
Barium 100 41.2 133 137 92 96 1 75-125 3 20
Cadmium 100 0.305 96.5 94.0 96 94 1 75-125 3 20
Chromium 100 15.2 110 108 95 93 1 75-125 1 20
Lead 100 21.1 119 117 98 96 1 75-125 2 20
Selenium 100 0.666 96.9 94.7 96 94 1 75-125 2 20
Silver 100 ND 94.5 91.4 95 91 1 75-125 3 20
Sulfur 1000 56.3 968 930 91 87 1 75-125 4 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG853598
Metals (ICP) by Method 6010C L819039-04
Method Blank (MB)
(MB) 03/03/16 11:22
MB Result MB Qualifier MB RDL
Analyte mg/l mg/l
Lead ND 0.450
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 03/03/16 11:25 • (LCSD) 03/03/16 11:27
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Lead 10.0 10.2 10.2 102 102 80-120 0 20
L819039-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 03/03/16 11:30 • (MS) 03/03/16 11:37 • (MSD) 03/03/16 11:39
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Lead 10.0 0.771 11.1 10.9 103 101 1 75-125 2 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG851267
Volatile Organic Compounds (GC/MS) by Method 8260B L819039-01,02
Method Blank (MB)
(MB) 02/28/16 15:47
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0100 0.0500
Acrylonitrile U 0.00179 0.0100
Benzene U 0.000270 0.00100
Bromobenzene U 0.000284 0.00100
Bromodichloromethane U 0.000254 0.00100
Bromoform U 0.000424 0.00100
Bromomethane U 0.00134 0.00500
n-Butylbenzene U 0.000258 0.00100
sec-Butylbenzene U 0.000201 0.00100
tert-Butylbenzene U 0.000206 0.00100
Carbon tetrachloride U 0.000328 0.00100
Chlorobenzene U 0.000212 0.00100
Chlorodibromomethane U 0.000373 0.00100
Chloroethane U 0.000946 0.00500
2-Chloroethyl vinyl ether U 0.00234 0.0500
Chloroform U 0.000229 0.00500
Chloromethane U 0.000375 0.00250
2-Chlorotoluene U 0.000301 0.00100
4-Chlorotoluene U 0.000240 0.00100
1,2-Dibromo-3-Chloropropane U 0.00105 0.00500
1,2-Dibromoethane U 0.000343 0.00100
Dibromomethane U 0.000382 0.00100
1,2-Dichlorobenzene U 0.000305 0.00100
1,3-Dichlorobenzene U 0.000239 0.00100
1,4-Dichlorobenzene U 0.000226 0.00100
Dichlorodifluoromethane U 0.000713 0.00500
1,1-Dichloroethane U 0.000199 0.00100
1,2-Dichloroethane U 0.000265 0.00100
1,1-Dichloroethene U 0.000303 0.00100
cis-1,2-Dichloroethene U 0.000235 0.00100
trans-1,2-Dichloroethene U 0.000264 0.00100
1,2-Dichloropropane U 0.000358 0.00100
1,1-Dichloropropene U 0.000317 0.00100
1,3-Dichloropropane U 0.000207 0.00100
cis-1,3-Dichloropropene U 0.000262 0.00100
trans-1,3-Dichloropropene U 0.000267 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG851267
Volatile Organic Compounds (GC/MS) by Method 8260B L819039-01,02
Method Blank (MB)
(MB) 02/28/16 15:47
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
2,2-Dichloropropane U 0.000279 0.00100
Di-isopropyl ether U 0.000248 0.00100
Ethylbenzene U 0.000297 0.00100
Hexachloro-1,3-butadiene U 0.000342 0.00100
Isopropylbenzene U 0.000243 0.00100
p-Isopropyltoluene U 0.000204 0.00100
2-Butanone (MEK)U 0.00468 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK)U 0.00188 0.0100
Methyl tert-butyl ether U 0.000212 0.00100
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.000206 0.00100
Styrene U 0.000234 0.00100
1,1,1,2-Tetrachloroethane U 0.000264 0.00100
1,1,2,2-Tetrachloroethane U 0.000365 0.00100
Tetrachloroethene U 0.000276 0.00100
Toluene U 0.000434 0.00500
1,1,2-Trichlorotrifluoroethane U 0.000365 0.00100
1,2,3-Trichlorobenzene U 0.000306 0.00100
1,2,4-Trichlorobenzene U 0.000388 0.00100
1,1,1-Trichloroethane U 0.000286 0.00100
1,1,2-Trichloroethane U 0.000277 0.00100
Trichloroethene U 0.000279 0.00100
Trichlorofluoromethane U 0.000382 0.00500
1,2,3-Trichloropropane U 0.000741 0.00250
1,2,3-Trimethylbenzene U 0.000287 0.00100
1,2,4-Trimethylbenzene U 0.000211 0.00100
1,3,5-Trimethylbenzene U 0.000266 0.00100
Vinyl chloride U 0.000291 0.00100
Xylenes, Total U 0.000698 0.00300
(S) Toluene-d8 104 88.7-115
(S) Dibromofluoromethane 109 76.3-123
(S) 4-Bromofluorobenzene 100 69.7-129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG851267
Volatile Organic Compounds (GC/MS) by Method 8260B L819039-01,02
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 02/28/16 14:06 • (LCSD) 02/28/16 14:26
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.125 0.173 0.162 138 130 25.3-178 6.39 22.9
Acrylonitrile 0.125 0.145 0.140 116 112 57.8-143 3.60 20
Benzene 0.0250 0.0269 0.0264 108 106 72.6-120 1.81 20
Bromobenzene 0.0250 0.0274 0.0255 110 102 80.3-115 7.43 20
Bromodichloromethane 0.0250 0.0278 0.0267 111 107 75.3-119 3.88 20
Bromoform 0.0250 0.0303 0.0281 121 112 69.1-135 7.64 20
Bromomethane 0.0250 0.0313 0.0313 125 125 23.0-191 0.160 20
n-Butylbenzene 0.0250 0.0302 0.0282 121 113 74.2-134 7.03 20
sec-Butylbenzene 0.0250 0.0265 0.0248 106 99.1 77.8-129 6.69 20
tert-Butylbenzene 0.0250 0.0269 0.0247 107 98.9 77.2-129 8.26 20
Carbon tetrachloride 0.0250 0.0269 0.0254 108 102 69.4-129 5.73 20
Chlorobenzene 0.0250 0.0251 0.0240 101 96.0 78.9-122 4.62 20
Chlorodibromomethane 0.0250 0.0278 0.0257 111 103 76.4-126 8.08 20
Chloroethane 0.0250 0.0296 0.0292 118 117 47.2-147 1.26 20
2-Chloroethyl vinyl ether 0.125 0.155 0.144 124 115 16.7-162 7.66 23.7
Chloroform 0.0250 0.0278 0.0273 111 109 73.3-122 1.76 20
Chloromethane 0.0250 0.0308 0.0304 123 122 53.1-135 1.25 20
2-Chlorotoluene 0.0250 0.0258 0.0237 103 94.7 74.6-127 8.66 20
4-Chlorotoluene 0.0250 0.0276 0.0259 110 104 79.5-123 6.26 20
1,2-Dibromo-3-Chloropropane 0.0250 0.0343 0.0318 137 127 64.9-131 J4 7.30 20
1,2-Dibromoethane 0.0250 0.0257 0.0238 103 95.4 78.7-123 7.68 20
Dibromomethane 0.0250 0.0272 0.0262 109 105 78.5-117 4.02 20
1,2-Dichlorobenzene 0.0250 0.0295 0.0280 118 112 83.6-119 5.33 20
1,3-Dichlorobenzene 0.0250 0.0272 0.0253 109 101 75.9-129 7.17 20
1,4-Dichlorobenzene 0.0250 0.0276 0.0255 110 102 81.0-115 7.71 20
Dichlorodifluoromethane 0.0250 0.0352 0.0339 141 135 50.9-139 J4 3.74 20
1,1-Dichloroethane 0.0250 0.0289 0.0285 116 114 71.7-125 1.63 20
1,2-Dichloroethane 0.0250 0.0279 0.0270 112 108 67.2-121 3.33 20
1,1-Dichloroethene 0.0250 0.0294 0.0284 118 114 60.6-133 3.43 20
cis-1,2-Dichloroethene 0.0250 0.0283 0.0276 113 110 76.1-121 2.49 20
trans-1,2-Dichloroethene 0.0250 0.0270 0.0268 108 107 70.7-124 0.890 20
1,2-Dichloropropane 0.0250 0.0267 0.0264 107 106 76.9-123 0.960 20
1,1-Dichloropropene 0.0250 0.0287 0.0282 115 113 71.2-126 1.55 20
1,3-Dichloropropane 0.0250 0.0260 0.0250 104 99.9 80.3-114 4.05 20
cis-1,3-Dichloropropene 0.0250 0.0274 0.0261 110 104 77.3-123 5.08 20
trans-1,3-Dichloropropene 0.0250 0.0298 0.0288 119 115 73.0-127 3.42 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG851267
Volatile Organic Compounds (GC/MS) by Method 8260B L819039-01,02
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 02/28/16 14:06 • (LCSD) 02/28/16 14:26
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
2,2-Dichloropropane 0.0250 0.0271 0.0272 109 109 61.9-132 0.350 20
Di-isopropyl ether 0.0250 0.0284 0.0280 114 112 67.2-131 1.35 20
Ethylbenzene 0.0250 0.0246 0.0242 98.5 97.0 78.6-124 1.57 20
Hexachloro-1,3-butadiene 0.0250 0.0293 0.0279 117 112 69.2-136 4.77 20
Isopropylbenzene 0.0250 0.0255 0.0240 102 96.1 79.4-126 6.01 20
p-Isopropyltoluene 0.0250 0.0280 0.0259 112 103 75.4-132 7.96 20
2-Butanone (MEK)0.125 0.167 0.150 134 120 44.5-154 10.9 21.3
Methylene Chloride 0.0250 0.0273 0.0272 109 109 68.2-119 0.0700 20
4-Methyl-2-pentanone (MIBK)0.125 0.163 0.144 131 115 61.1-138 12.8 20
Methyl tert-butyl ether 0.0250 0.0271 0.0264 108 105 70.2-122 2.84 20
Naphthalene 0.0250 0.0326 0.0311 130 124 69.9-132 4.60 20
n-Propylbenzene 0.0250 0.0269 0.0251 108 100 80.2-124 7.06 20
Styrene 0.0250 0.0277 0.0256 111 102 79.4-124 7.89 20
1,1,1,2-Tetrachloroethane 0.0250 0.0261 0.0240 104 96.0 76.7-127 8.37 20
1,1,2,2-Tetrachloroethane 0.0250 0.0301 0.0275 120 110 78.8-124 9.12 20
Tetrachloroethene 0.0250 0.0229 0.0230 91.6 92.0 71.1-133 0.520 20
Toluene 0.0250 0.0244 0.0241 97.6 96.4 76.7-116 1.26 20
1,1,2-Trichlorotrifluoroethane 0.0250 0.0279 0.0270 112 108 62.6-138 3.20 20
1,2,3-Trichlorobenzene 0.0250 0.0309 0.0294 124 118 72.5-137 5.03 20
1,2,4-Trichlorobenzene 0.0250 0.0324 0.0297 130 119 74.0-137 8.68 20
1,1,1-Trichloroethane 0.0250 0.0268 0.0268 107 107 69.9-127 0.0900 20
1,1,2-Trichloroethane 0.0250 0.0259 0.0235 103 94.0 81.9-119 9.58 20
Trichloroethene 0.0250 0.0251 0.0246 100 98.5 77.2-122 1.73 20
Trichlorofluoromethane 0.0250 0.0271 0.0270 108 108 51.5-151 0.130 20
1,2,3-Trichloropropane 0.0250 0.0278 0.0253 111 101 74.0-124 9.40 20
1,2,3-Trimethylbenzene 0.0250 0.0282 0.0264 113 106 79.4-118 6.51 20
1,2,4-Trimethylbenzene 0.0250 0.0263 0.0245 105 97.9 77.1-124 7.13 20
1,3,5-Trimethylbenzene 0.0250 0.0261 0.0243 104 97.0 79.0-125 7.19 20
Vinyl chloride 0.0250 0.0306 0.0299 122 120 58.4-134 2.15 20
Xylenes, Total 0.0750 0.0736 0.0702 98.1 93.5 78.1-123 4.77 20
(S) Toluene-d8 102 101 88.7-115
(S) Dibromofluoromethane 108 107 76.3-123
(S) 4-Bromofluorobenzene 98.7 97.4 69.7-129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG851267
Volatile Organic Compounds (GC/MS) by Method 8260B L819039-01,02
L818928-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 02/28/16 19:12 • (MS) 02/28/16 17:11 • (MSD) 02/28/16 17:31
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 0.125 0.00729 0.891 0.781 141 124 5 10.0-130 J5 13.1 31.5
Acrylonitrile 0.125 ND 0.763 0.692 122 111 5 39.3-152 9.71 27.2
Benzene 0.0250 0.000398 0.138 0.126 110 100 5 47.8-131 8.86 22.8
Bromobenzene 0.0250 ND 0.124 0.113 99.4 90.7 5 40.0-130 9.09 27.4
Bromodichloromethane 0.0250 ND 0.138 0.125 110 100 5 50.6-128 9.52 22.8
Bromoform 0.0250 ND 0.136 0.122 109 97.4 5 43.3-139 11.2 25.9
Bromomethane 0.0250 ND 0.148 0.142 118 114 5 5.00-189 3.85 26.7
n-Butylbenzene 0.0250 ND 0.132 0.113 106 90.3 5 23.6-146 15.8 39.2
sec-Butylbenzene 0.0250 ND 0.123 0.108 98.6 86.6 5 31.0-142 12.9 34.7
tert-Butylbenzene 0.0250 ND 0.125 0.112 100 89.2 5 36.9-142 11.8 31.7
Carbon tetrachloride 0.0250 ND 0.136 0.126 109 100 5 46.0-140 8.04 27.2
Chlorobenzene 0.0250 ND 0.124 0.113 99.1 90.2 5 44.1-134 9.37 25.7
Chlorodibromomethane 0.0250 ND 0.132 0.121 105 96.5 5 49.7-134 8.69 24
Chloroethane 0.0250 ND 0.148 0.137 119 109 5 5.00-164 8.09 28.4
2-Chloroethyl vinyl ether 0.125 ND 0.758 0.705 121 113 5 5.00-159 7.26 40
Chloroform 0.0250 ND 0.141 0.130 113 104 5 51.2-133 8.35 22.8
Chloromethane 0.0250 ND 0.142 0.132 114 105 5 31.4-141 7.38 24.6
2-Chlorotoluene 0.0250 ND 0.122 0.111 97.5 88.7 5 36.1-137 9.47 28.9
4-Chlorotoluene 0.0250 ND 0.128 0.116 102 92.8 5 35.4-137 9.83 29.8
1,2-Dibromo-3-Chloropropane 0.0250 ND 0.145 0.132 116 106 5 40.4-138 9.13 30.8
1,2-Dibromoethane 0.0250 ND 0.124 0.116 98.9 92.8 5 50.2-133 6.33 23.6
Dibromomethane 0.0250 ND 0.134 0.127 107 101 5 52.4-128 5.82 23
1,2-Dichlorobenzene 0.0250 ND 0.128 0.115 102 92.0 5 34.6-139 10.6 29.9
1,3-Dichlorobenzene 0.0250 ND 0.119 0.107 95.2 85.7 5 28.4-142 10.6 31.2
1,4-Dichlorobenzene 0.0250 ND 0.123 0.108 98.0 86.6 5 35.0-133 12.4 31.1
Dichlorodifluoromethane 0.0250 ND 0.151 0.136 121 109 5 31.2-144 10.4 30.2
1,1-Dichloroethane 0.0250 ND 0.150 0.134 120 107 5 49.1-136 11.1 22.9
1,2-Dichloroethane 0.0250 ND 0.141 0.128 112 102 5 47.1-129 9.48 22.7
1,1-Dichloroethene 0.0250 ND 0.147 0.134 117 108 5 36.1-142 8.77 25.6
cis-1,2-Dichloroethene 0.0250 ND 0.142 0.129 114 103 5 50.6-133 9.58 23
trans-1,2-Dichloroethene 0.0250 ND 0.137 0.127 109 102 5 43.8-135 6.92 24.8
1,2-Dichloropropane 0.0250 ND 0.135 0.126 108 101 5 50.3-134 6.58 22.7
1,1-Dichloropropene 0.0250 ND 0.144 0.131 115 104 5 43.0-137 9.90 26.4
1,3-Dichloropropane 0.0250 ND 0.129 0.118 103 94.5 5 51.4-127 8.58 23.1
cis-1,3-Dichloropropene 0.0250 ND 0.138 0.127 110 102 5 48.4-134 8.14 23.6
trans-1,3-Dichloropropene 0.0250 ND 0.147 0.131 117 105 5 46.6-135 11.3 25.3
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG851267
Volatile Organic Compounds (GC/MS) by Method 8260B L819039-01,02
L818928-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 02/28/16 19:12 • (MS) 02/28/16 17:11 • (MSD) 02/28/16 17:31
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
2,2-Dichloropropane 0.0250 ND 0.147 0.137 117 109 5 45.2-141 7.03 26.6
Di-isopropyl ether 0.0250 ND 0.144 0.132 115 106 5 46.7-140 8.20 23.5
Ethylbenzene 0.0250 ND 0.123 0.113 98.8 90.7 5 44.8-135 8.55 26.9
Hexachloro-1,3-butadiene 0.0250 ND 0.113 0.0950 90.7 76.0 5 10.0-149 17.7 40
Isopropylbenzene 0.0250 ND 0.125 0.112 99.7 89.7 5 41.9-139 10.5 29.3
p-Isopropyltoluene 0.0250 ND 0.127 0.111 101 88.9 5 27.3-146 13.2 35.1
2-Butanone (MEK)0.125 ND 0.816 0.763 131 122 5 23.9-170 6.67 28.3
Methylene Chloride 0.0250 ND 0.139 0.127 111 101 5 46.7-125 9.22 22.2
4-Methyl-2-pentanone (MIBK)0.125 ND 0.748 0.686 120 110 5 42.4-146 8.56 26.7
Methyl tert-butyl ether 0.0250 ND 0.141 0.129 113 103 5 50.4-131 8.37 24.8
Naphthalene 0.0250 ND 0.133 0.120 106 95.9 5 18.4-145 10.2 34
n-Propylbenzene 0.0250 ND 0.128 0.114 103 91.1 5 35.2-139 11.9 31.9
Styrene 0.0250 ND 0.129 0.119 104 95.2 5 39.7-137 8.37 28.2
1,1,1,2-Tetrachloroethane 0.0250 ND 0.127 0.114 101 91.6 5 48.8-136 10.2 25.5
1,1,2,2-Tetrachloroethane 0.0250 ND 0.129 0.115 103 92.3 5 45.7-140 11.2 26.4
Tetrachloroethene 0.0250 ND 0.118 0.103 94.3 82.2 5 37.7-140 13.7 29.2
Toluene 0.0250 0.00105 0.125 0.115 99.3 91.4 5 47.8-127 8.22 24.3
1,1,2-Trichlorotrifluoroethane 0.0250 ND 0.139 0.124 111 99.4 5 35.7-146 11.0 28.8
1,2,3-Trichlorobenzene 0.0250 ND 0.122 0.110 97.8 87.9 5 10.0-150 10.6 38.5
1,2,4-Trichlorobenzene 0.0250 ND 0.127 0.112 102 90.0 5 10.0-153 12.3 39.3
1,1,1-Trichloroethane 0.0250 ND 0.142 0.132 113 105 5 49.0-138 7.19 25.3
1,1,2-Trichloroethane 0.0250 ND 0.122 0.113 97.9 90.1 5 52.3-132 8.25 23.4
Trichloroethene 0.0250 ND 0.126 0.119 101 95.2 5 48.0-132 6.09 24.8
Trichlorofluoromethane 0.0250 ND 0.145 0.139 116 111 5 12.8-169 4.33 29.7
1,2,3-Trichloropropane 0.0250 ND 0.120 0.115 95.9 91.7 5 44.4-138 4.46 26.3
1,2,3-Trimethylbenzene 0.0250 ND 0.131 0.116 105 92.6 5 41.0-133 12.3 27.6
1,2,4-Trimethylbenzene 0.0250 0.000230 0.121 0.109 96.4 87.0 5 32.9-139 10.3 30.6
1,3,5-Trimethylbenzene 0.0250 ND 0.125 0.110 100 87.9 5 37.1-138 13.2 30.6
Vinyl chloride 0.0250 ND 0.149 0.138 119 110 5 32.0-146 7.85 26.3
Xylenes, Total 0.0750 0.000253 0.361 0.328 96.2 87.5 5 42.7-135 9.50 26.6
(S) Toluene-d8 102 102 88.7-115
(S) Dibromofluoromethane 109 107 76.3-123
(S) 4-Bromofluorobenzene 97.1 95.8 69.7-129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG851554
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L819039-03
Method Blank (MB)
(MB) 02/24/16 09:02
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00642 0.0330
Acenaphthylene U 0.00671 0.0330
Anthracene U 0.00632 0.0330
Benzidine U 0.0637 0.333
Benzo(a)anthracene U 0.00428 0.0330
Benzo(b)fluoranthene U 0.00695 0.0330
Benzo(k)fluoranthene U 0.00582 0.0330
Benzo(g,h,i)perylene U 0.00721 0.0330
Benzo(a)pyrene U 0.00548 0.0330
Bis(2-chlorethoxy)methane U 0.00770 0.333
Bis(2-chloroethyl)ether U 0.00896 0.333
Bis(2-chloroisopropyl)ether U 0.00760 0.333
4-Bromophenyl-phenylether U 0.0114 0.333
2-Chloronaphthalene U 0.00639 0.0330
4-Chlorophenyl-phenylether U 0.00627 0.333
Chrysene U 0.00555 0.0330
Dibenz(a,h)anthracene U 0.00821 0.0330
3,3-Dichlorobenzidine U 0.0794 0.333
2,4-Dinitrotoluene U 0.00607 0.333
2,6-Dinitrotoluene U 0.00737 0.333
Fluoranthene U 0.00496 0.0330
Fluorene U 0.00682 0.0330
Hexachlorobenzene U 0.00856 0.333
Hexachloro-1,3-butadiene U 0.0100 0.333
Hexachlorocyclopentadiene U 0.0587 0.333
Hexachloroethane U 0.0134 0.333
Indeno(1,2,3-cd)pyrene U 0.00772 0.0330
Isophorone U 0.00522 0.333
Naphthalene U 0.00889 0.0330
Nitrobenzene U 0.00695 0.333
n-Nitrosodimethylamine U 0.0647 0.333
n-Nitrosodiphenylamine U 0.00594 0.333
n-Nitrosodi-n-propylamine U 0.00906 0.333
Phenanthrene U 0.00528 0.0330
Benzylbutyl phthalate U 0.0103 0.333
Bis(2-ethylhexyl)phthalate U 0.0120 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG851554
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L819039-03
Method Blank (MB)
(MB) 02/24/16 09:02
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Di-n-butyl phthalate U 0.0109 0.333
Diethyl phthalate U 0.00691 0.333
Dimethyl phthalate U 0.00540 0.333
Di-n-octyl phthalate U 0.00907 0.333
Pyrene U 0.0123 0.0330
1,2,4-Trichlorobenzene U 0.00876 0.333
4-Chloro-3-methylphenol U 0.00477 0.333
2-Chlorophenol U 0.00831 0.333
2,4-Dichlorophenol U 0.00746 0.333
2,4-Dimethylphenol U 0.0471 0.333
4,6-Dinitro-2-methylphenol U 0.124 0.333
2,4-Dinitrophenol U 0.0980 0.333
2-Nitrophenol U 0.0130 0.333
4-Nitrophenol U 0.0525 0.333
Pentachlorophenol U 0.0480 0.333
Phenol U 0.00695 0.333
2,4,6-Trichlorophenol U 0.00779 0.333
(S) Nitrobenzene-d5 76.9 21.9-129
(S) 2-Fluorobiphenyl 84.5 34.9-129
(S) p-Terphenyl-d14 88.1 21.5-128
(S) Phenol-d5 71.4 26.3-121
(S) 2-Fluorophenol 78.0 21.1-116
(S) 2,4,6-Tribromophenol 91.5 21.6-142
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 02/24/16 08:14 • (LCSD) 02/24/16 08:38
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.667 0.550 0.548 82.5 82.1 48.9-107 0.480 20
Acenaphthylene 0.667 0.582 0.576 87.3 86.4 49.2-111 1.00 20
Anthracene 0.667 0.568 0.548 85.2 82.2 52.0-112 3.66 20
Benzidine 0.667 0.0897 0.0809 13.5 12.1 0.000-48.0 10.3 40
Benzo(a)anthracene 0.667 0.569 0.561 85.3 84.1 52.3-106 1.43 20
Benzo(b)fluoranthene 0.667 0.552 0.543 82.8 81.4 51.3-106 1.70 20
Benzo(k)fluoranthene 0.667 0.577 0.559 86.5 83.7 52.9-107 3.22 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG851554
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L819039-03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 02/24/16 08:14 • (LCSD) 02/24/16 08:38
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Benzo(g,h,i)perylene 0.667 0.620 0.608 92.9 91.2 45.8-108 1.86 20
Benzo(a)pyrene 0.667 0.583 0.559 87.4 83.8 51.9-106 4.20 20
Bis(2-chlorethoxy)methane 0.667 0.473 0.452 71.0 67.8 44.9-108 4.59 20
Bis(2-chloroethyl)ether 0.667 0.428 0.384 64.2 57.5 32.5-112 11.1 26
Bis(2-chloroisopropyl)ether 0.667 0.497 0.463 74.4 69.5 40.4-99.0 6.93 20.7
4-Bromophenyl-phenylether 0.667 0.606 0.601 90.9 90.1 51.4-110 0.890 20
2-Chloronaphthalene 0.667 0.574 0.569 86.1 85.3 47.1-105 0.900 20
4-Chlorophenyl-phenylether 0.667 0.577 0.566 86.6 84.9 48.1-108 1.99 20
Chrysene 0.667 0.547 0.554 82.1 83.1 54.4-110 1.28 20
Dibenz(a,h)anthracene 0.667 0.609 0.590 91.2 88.5 45.7-111 3.04 20
3,3-Dichlorobenzidine 0.667 0.421 0.401 63.2 60.2 21.0-101 4.89 22
2,4-Dinitrotoluene 0.667 0.630 0.620 94.5 92.9 53.0-112 1.68 20
2,6-Dinitrotoluene 0.667 0.638 0.641 95.6 96.1 51.6-110 0.560 20
Fluoranthene 0.667 0.593 0.585 88.9 87.7 53.7-110 1.40 20
Fluorene 0.667 0.566 0.554 84.8 83.1 51.1-109 2.08 20
Hexachlorobenzene 0.667 0.614 0.597 92.0 89.5 43.2-104 2.78 20.1
Hexachloro-1,3-butadiene 0.667 0.617 0.583 92.5 87.4 41.5-112 5.71 20
Hexachlorocyclopentadiene 0.667 0.416 0.409 62.4 61.3 13.5-123 1.87 20.7
Hexachloroethane 0.667 0.513 0.462 76.9 69.3 36.2-103 10.4 22.7
Indeno(1,2,3-cd)pyrene 0.667 0.632 0.617 94.7 92.5 47.5-109 2.39 20
Isophorone 0.667 0.538 0.524 80.7 78.5 28.8-104 2.78 20
Naphthalene 0.667 0.510 0.479 76.5 71.8 43.4-103 6.41 20
Nitrobenzene 0.667 0.525 0.488 78.7 73.2 40.7-109 7.29 21
n-Nitrosodimethylamine 0.667 0.487 0.446 73.0 66.9 18.1-122 8.75 23.5
n-Nitrosodiphenylamine 0.667 0.542 0.525 81.2 78.6 48.8-107 3.20 20
n-Nitrosodi-n-propylamine 0.667 0.456 0.430 68.4 64.5 43.3-109 5.81 20
Phenanthrene 0.667 0.553 0.535 82.9 80.2 51.6-107 3.32 20
Benzylbutyl phthalate 0.667 0.578 0.566 86.6 84.9 47.5-115 2.06 20
Bis(2-ethylhexyl)phthalate 0.667 0.584 0.589 87.6 88.3 48.1-116 0.760 20.5
Di-n-butyl phthalate 0.667 0.587 0.589 88.0 88.3 49.7-113 0.330 20
Diethyl phthalate 0.667 0.618 0.604 92.7 90.5 52.0-112 2.38 20
Dimethyl phthalate 0.667 0.607 0.602 91.0 90.2 51.4-108 0.890 20
Di-n-octyl phthalate 0.667 0.551 0.566 82.5 84.8 49.6-112 2.69 22
Pyrene 0.667 0.558 0.543 83.7 81.4 47.1-108 2.80 20
1,2,4-Trichlorobenzene 0.667 0.557 0.531 83.5 79.7 39.8-100 4.70 20
4-Chloro-3-methylphenol 0.667 0.556 0.536 83.3 80.4 51.1-113 3.60 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG851554
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L819039-03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 02/24/16 08:14 • (LCSD) 02/24/16 08:38
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
2-Chlorophenol 0.667 0.509 0.458 76.3 68.7 40.8-103 10.5 20
2,4-Dichlorophenol 0.667 0.586 0.568 87.9 85.2 46.2-109 3.10 20
2,4-Dimethylphenol 0.667 0.535 0.501 80.2 75.1 42.2-110 6.58 20
4,6-Dinitro-2-methylphenol 0.667 0.578 0.548 86.6 82.2 23.1-119 5.22 23.7
2,4-Dinitrophenol 0.667 0.357 0.325 53.5 48.8 10.0-105 9.32 36.5
2-Nitrophenol 0.667 0.610 0.572 91.4 85.8 44.2-113 6.37 20.9
4-Nitrophenol 0.667 0.587 0.590 88.1 88.4 34.8-109 0.400 20
Pentachlorophenol 0.667 0.623 0.599 93.5 89.8 16.2-102 3.97 22.9
Phenol 0.667 0.474 0.442 71.1 66.2 41.5-106 7.08 20
2,4,6-Trichlorophenol 0.667 0.620 0.603 93.0 90.4 44.4-108 2.78 20
(S) Nitrobenzene-d5 72.9 71.8 21.9-129
(S) 2-Fluorobiphenyl 83.5 80.5 34.9-129
(S) p-Terphenyl-d14 92.4 83.7 21.5-128
(S) Phenol-d5 73.3 68.5 26.3-121
(S) 2-Fluorophenol 79.6 71.1 21.1-116
(S) 2,4,6-Tribromophenol 103 98.1 21.6-142
L818928-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 02/24/16 12:11 • (MS) 02/24/16 12:35 • (MSD) 02/24/16 12:59
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.667 ND 0.417 0.472 62.5 70.7 1 32.2-134 12.4 27.3
Acenaphthylene 0.667 ND 0.438 0.510 65.6 76.4 1 38.7-129 15.1 25.9
Anthracene 0.667 ND 0.403 0.468 60.5 70.1 1 32.3-137 14.7 28.4
Benzidine 0.667 ND 0.0922 0.0865 13.8 13.0 1 0.000-49.9 6.45 40
Benzo(a)anthracene 0.667 ND 0.409 0.451 61.4 67.7 1 33.3-124 9.79 29
Benzo(b)fluoranthene 0.667 ND 0.397 0.432 59.4 64.7 1 23.3-133 8.47 30.3
Benzo(k)fluoranthene 0.667 ND 0.382 0.450 57.2 67.5 1 31.0-129 16.5 26.7
Benzo(g,h,i)perylene 0.667 ND 0.433 0.450 64.9 67.5 1 10.0-127 3.91 31.9
Benzo(a)pyrene 0.667 ND 0.402 0.452 60.3 67.8 1 28.2-128 11.7 28.4
Bis(2-chlorethoxy)methane 0.667 ND 0.351 0.404 52.7 60.6 1 35.0-132 14.0 26.1
Bis(2-chloroethyl)ether 0.667 ND 0.318 0.362 47.7 54.3 1 28.8-128 12.9 33.6
Bis(2-chloroisopropyl)ether 0.667 ND 0.378 0.437 56.6 65.5 1 31.8-118 14.5 31.7
4-Bromophenyl-phenylether 0.667 ND 0.428 0.491 64.1 73.6 1 39.0-130 13.8 26
2-Chloronaphthalene 0.667 ND 0.436 0.503 65.4 75.5 1 37.5-123 14.2 26.5
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG851554
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L819039-03
L818928-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 02/24/16 12:11 • (MS) 02/24/16 12:35 • (MSD) 02/24/16 12:59
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
4-Chlorophenyl-phenylether 0.667 ND 0.417 0.485 62.5 72.7 1 37.9-123 15.0 25.9
Chrysene 0.667 ND 0.410 0.451 61.5 67.7 1 36.3-129 9.55 28
Dibenz(a,h)anthracene 0.667 ND 0.436 0.464 65.4 69.5 1 10.5-128 6.13 29.5
3,3-Dichlorobenzidine 0.667 ND 0.283 0.327 42.4 49.0 1 10.0-129 14.4 40
2,4-Dinitrotoluene 0.667 ND 0.488 0.570 73.2 85.5 1 27.8-147 15.5 29.7
2,6-Dinitrotoluene 0.667 ND 0.493 0.573 74.0 85.9 1 36.5-137 14.9 29.7
Fluoranthene 0.667 ND 0.418 0.489 62.7 73.3 1 27.9-138 15.5 26.9
Fluorene 0.667 ND 0.423 0.481 63.4 72.1 1 34.0-133 12.9 27.1
Hexachlorobenzene 0.667 ND 0.450 0.514 67.5 77.1 1 34.4-116 13.3 25.4
Hexachloro-1,3-butadiene 0.667 ND 0.479 0.533 71.8 80.0 1 36.5-125 10.8 29.7
Hexachlorocyclopentadiene 0.667 ND 0.235 0.278 35.3 41.6 1 10.0-124 16.4 37.5
Hexachloroethane 0.667 ND 0.405 0.446 60.7 66.9 1 11.3-143 9.74 31.9
Indeno(1,2,3-cd)pyrene 0.667 ND 0.434 0.464 65.0 69.5 1 10.0-128 6.70 31.5
Isophorone 0.667 ND 0.394 0.460 59.1 69.0 1 25.7-116 15.5 27.7
Naphthalene 0.667 ND 0.393 0.446 58.9 66.8 1 36.4-121 12.6 27.2
Nitrobenzene 0.667 ND 0.392 0.448 58.8 67.2 1 30.9-134 13.3 27.8
n-Nitrosodimethylamine 0.667 ND 0.369 0.410 55.3 61.5 1 19.2-127 10.6 32
n-Nitrosodiphenylamine 0.667 ND 0.393 0.436 58.9 65.4 1 26.8-133 10.5 25.9
n-Nitrosodi-n-propylamine 0.667 ND 0.338 0.386 50.7 57.8 1 33.0-134 13.2 28.2
Phenanthrene 0.667 ND 0.395 0.452 59.1 67.8 1 30.8-137 13.6 26.5
Benzylbutyl phthalate 0.667 ND 0.390 0.432 58.5 64.7 1 33.4-128 10.2 28.5
Bis(2-ethylhexyl)phthalate 0.667 ND 0.395 0.434 59.2 65.0 1 21.8-141 9.40 35.2
Di-n-butyl phthalate 0.667 ND 0.401 0.454 60.2 68.1 1 32.2-133 12.3 25.9
Diethyl phthalate 0.667 ND 0.466 0.548 69.9 82.1 1 39.4-136 16.1 25.5
Dimethyl phthalate 0.667 ND 0.474 0.555 71.1 83.2 1 35.8-137 15.7 25.4
Di-n-octyl phthalate 0.667 ND 0.378 0.419 56.7 62.8 1 28.5-128 10.2 32.5
Pyrene 0.667 ND 0.404 0.425 60.6 63.7 1 24.1-130 5.06 29.9
1,2,4-Trichlorobenzene 0.667 ND 0.447 0.494 67.1 74.0 1 36.5-114 9.85 28.4
4-Chloro-3-methylphenol 0.667 ND 0.419 0.494 62.9 74.0 1 27.0-154 16.3 26.6
2-Chlorophenol 0.667 ND 0.389 0.447 58.4 67.0 1 33.2-121 13.7 29.3
2,4-Dichlorophenol 0.667 ND 0.449 0.532 67.4 79.7 1 34.8-134 16.7 27.3
2,4-Dimethylphenol 0.667 ND 0.386 0.456 57.9 68.4 1 12.3-149 16.6 32.3
4,6-Dinitro-2-methylphenol 0.667 ND 0.384 0.457 57.5 68.6 1 10.0-144 17.5 32.7
2,4-Dinitrophenol 0.667 ND 0.232 0.259 34.7 38.8 1 10.0-121 11.2 39.4
2-Nitrophenol 0.667 ND 0.470 0.531 70.4 79.6 1 29.5-144 12.2 29.9
4-Nitrophenol 0.667 ND 0.427 0.514 64.0 77.0 1 20.0-133 18.5 30.2
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG851554
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L819039-03
L818928-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 02/24/16 12:11 • (MS) 02/24/16 12:35 • (MSD) 02/24/16 12:59
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Pentachlorophenol 0.667 ND 0.466 0.532 69.9 79.8 1 10.0-139 13.3 28.3
Phenol 0.667 ND 0.351 0.410 52.6 61.5 1 25.1-130 15.6 29.6
2,4,6-Trichlorophenol 0.667 ND 0.486 0.560 72.9 84.0 1 33.8-133 14.1 28.1
(S) Nitrobenzene-d5 57.9 64.8 21.9-129
(S) 2-Fluorobiphenyl 63.0 73.3 34.9-129
(S) p-Terphenyl-d14 61.6 71.2 21.5-128
(S) Phenol-d5 52.8 62.9 26.3-121
(S) 2-Fluorophenol 61.2 68.5 21.1-116
(S) 2,4,6-Tribromophenol 81.8 92.0 21.6-142
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Abbreviations and Definitions
SDG Sample Delivery Group.
MDL Method Detection Limit.
RDL Reported Detection Limit.
ND,U Not detected at the Reporting Limit (or MDL where applicable).
RPD Relative Percent Difference.
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry
report basis for soils].
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.Recovery.
SDL Sample Detection Limit.
MQL Method Quantitation Limit.
Unadj. MQL Unadjusted Method Quantitation Limit.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is
high.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Solutions-IES 16018 L819039 03/03/16 13:50 30 of 32
Our Locations
Alabama 40660
Alaska UST-080
Arizona AZ0612
Arkansas 88-0469
California 01157CA
Colorado TN00003
Conneticut PH-0197
Florida E87487
Georgia NELAP
Georgia 1 923
Idaho TN00003
Illinois 200008
Indiana C-TN-01
Iowa 364
Kansas E-10277
Kentucky 1 90010
Kentucky 2 16
Louisiana AI30792
Maine TN0002
Maryland 324
Massachusetts M-TN003
Michigan 9958
Minnesota 047-999-395
Mississippi TN00003
Missouri 340
Montana CERT0086
Nebraska NE-OS-15-05
Nevada TN-03-2002-34
New Hampshire 2975
New Jersey–NELAP TN002
New Mexico TN00003
New York 11742
North Carolina Env375
North Carolina 1 DW21704
North Carolina 2 41
North Dakota R-140
Ohio–VAP CL0069
Oklahoma 9915
Oregon TN200002
Pennsylvania 68-02979
Rhode Island 221
South Carolina 84004
South Dakota n/a
Tennessee 1 4 2006
Texas T 104704245-07-TX
Texas 5 LAB0152
Utah 6157585858
Vermont VT2006
Virginia 109
Washington C1915
West Virginia 233
Wisconsin 9980939910
Wyoming A2LA
A2LA – ISO 17025 1461.01
Canada 1461.01
EPA–Crypto TN00003
AIHA 100789
DOD 1461.01
USDA S-67674
State Accreditations
Third Party & Federal Accreditations
ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other
lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the
network laboratories in our industry. The most significant benefit to our “one location” design is the design of our laboratory campus. The model is conducive to accelerated productivity,
decreasing turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please
contact our main office. ESC Lab Sciences performs all testing at our central laboratory.
1. Drinking Water 2. Underground Storage Tanks 3. Aquatic Toxicity 4. Chemical/Microbiological 5. Mold n/a Accreditation not applicable
1461.02A2LA – ISO 170255
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Solutions-IES 16018 L819039 03/03/16 14:10 30 of 32
DIVIDER PAGE
Republic Services, Inc.
18500 N. Allied Way, Phoenix, AZ 85054
SPECIAL WASTE DEPARTMENT DECISION
Waste Profile #
3041161011
Expiration Date
1/18/2017
I. Decision Request:Initial Recertification Change
Disposal Facility:3041 - Uwharrie Environmental Regional MSW Landfill
Generator Name:Historic Revolution LLC
Generator Site Address:1200 N. Revolution Mill Drive
City:Greensboro County:State:NC Zip:
Name of Waste:Excavated Soil
Estimated Annual Volume:340 Cubic Yards
II. Special Waste Department Decision:
Approved Rejected
Management Method(s):
Landfill Solidification Bioremediation Transfer Facility
Problematic Special Waste according to Republic?Yes No
If yes, which one?
Approved by Special Waste Review Committee?Yes No Not Applicable
Precautions, Conditions or Limitations on Approval


The analytical data (Sample # SP-3A, SP-3B, SP-3) has been received and reviewed. The additional 140 cubic yards of
excavated soil represented by this analysis is acceptable for disposal.
Special Waste Analyst Signature:____________________________Name (Printed):KEITH DIAMANTI
Date: 3/30/2016
III. Facility Decision:Approved Rejected
Precautions, Conditions or Limitations on Approval

By signing below, the General Manager or Designee agrees that a fully executed Special Waste Service Agreement is on file for this profile and that the
special waste file is complete.
General Manager or Designee:_____________________________Name (Printed):_____________________________
Date: 3/30/2016
X
Joe Reynold, Site Manager
Composite
Sample
Acetone 0.0448 J 0.0289 J
Benzene 0.000415 J <0.000270
4-Methyl-2-pentanone (MIBK)0.00837 J <0.00188
Naphthalene 0.0103 <0.00100
Acenaphthene 0.269 J
Anthracene 0.641
Benzo(a) anthracene 1.77
Benzo(b) fluoranthene 1.73
Benzo(k) fluoranthene 0.537
Benzo(g,h,i) perylene 0.989
Benzo(a) pyrene 1.41
Chrysene 1.51
Dibenz(a,h)anthracene 0.269 J
Fluoranthene 3.24
Fluorene 0.237 J
Indeno(1,2,3-cd) pyrene 0.882
Naphthalene 0.115 J
Phenanthrene 2.23
Pyrene 2.97
Barium 211
Cadmium 0.581 J
Chromium 32.0
Lead 56.9
Mercury 0.0280
Selenium 2.41 J
Total Sulfur 161
Total Sulfate 153
Notes:
Samples collected March 10, 2016 bold font
Laboratory Qualifiers
J - estimated concentration for test results above the method detection limit but below the
reported detection limit
< # - analyte not detected at a concentration that exceeds the minimum detection limit shown
BDL - Below Detection Limit
Metals/Sulfur/Sulfate - EPA 9056/6010 (mg/kg) *
All results in mg/kg, equivalent to parts per million.
Result exceeds reported detetion
limit
Not Tested
SP-3
* No total metal results exceeded 20x the TCLP regulatory levels, so TCLP
extraction /testing not necessary.
Volatile Organic Compounds - EPA 8260 (mg/kg)
Semivolatile Organic Compounds - EPA 8270 (mg/kg)
Not Tested
Not Tested
Grab Samples
Analyte
Sample Identification
SP-3A SP-3B
Table 1
Soil Laboratory Test Results: Revolution Mill Stockpiles
Greensboro. North Carolina
T:\Project Files\Self-Help\2016-0022.SELF - Revolution Mill\7. Working Documents\Soil Testing\Soil Testing - March 2016\2016-03-10 Stockpiles and bad soil Page 1 of 1
ANALYTICAL REPORT
March 16, 2016
Solutions-IES
Sample Delivery Group:L823060
Samples Received:03/11/2016
Project Number:2016.0022.SELF
Description:Revolution Mill
Report To:Daphne Jones
1101 Nowell Road
Raleigh, NC 27607
Entire Report Reviewed By:
March 16, 2016
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com
March 17, 2016
Jimmy Hunt
Technical Service Representative
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
¹Cp: Cover Page 1
²Tc: Table of Contents 2
³Ss: Sample Summary 3
⁴Cn: Case Narrative 4
⁵Sr: Sample Results 5
SP-3A L823060-01 5
SP-3B L823060-02 7
SP-3 L823060-03 9
⁶Qc: Quality Control Summary 11
Total Solids by Method 2540 G-2011 11
Wet Chemistry by Method 9056A 12
Mercury by Method 7471A 13
Metals (ICP) by Method 6010C 14
Volatile Organic Compounds (GC/MS) by Method 8260B 15
Semi Volatile Organic Compounds (GC/MS) by Method 8270D 19
⁷Gl: Glossary of Terms 23
⁸Al: Accreditations & Locations 24
⁹Sc: Chain of Custody 25
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SP-3A L823060-01 Solid Sean Jarvah 03/10/16 09:00 03/11/16 16:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG855891 1 03/12/16 11:38 03/12/16 11:50 KDW
Volatile Organic Compounds (GC/MS) by Method 8260B WG856331 1 03/15/16 09:00 03/15/16 09:07 JHH
Collected by Collected date/time Received date/time
SP-3B L823060-02 Solid Sean Jarvah 03/10/16 09:23 03/11/16 16:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG855891 1 03/12/16 11:38 03/12/16 11:50 KDW
Volatile Organic Compounds (GC/MS) by Method 8260B WG856331 1 03/15/16 09:00 03/15/16 09:25 JHH
Collected by Collected date/time Received date/time
SP-3 L823060-03 Solid Sean Jarvah 03/10/16 09:32 03/11/16 16:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG855803 1 03/12/16 10:45 03/15/16 08:37 BRJ
Metals (ICP) by Method 6010C WG855946 1 03/13/16 13:03 03/13/16 19:01 CCE
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG856576 10 03/16/16 11:25 03/16/16 17:41 ADF
Total Solids by Method 2540 G-2011 WG855891 1 03/12/16 11:38 03/12/16 11:50 KDW
Wet Chemistry by Method 9056A WG855610 1 03/14/16 21:45 03/15/16 01:46 DJD
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ)
values reported for environmental samples have been corrected for the dilution factor used in the
analysis. All Method and Batch Quality Control are within established criteria except where addressed
in this case narrative, a non-conformance form or properly qualified within the sample results. By my
digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the
laboratory as having the potential to affect the quality of the data have been identified by the
laboratory, and no information or data have been knowingly withheld that would affect the quality of the
data.
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Jimmy Hunt
Technical Service Representative
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L823060
SP-3A
Collected date/time: 03/10/16 09:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.9 1 03/12/2016 11:50 WG855891
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0448 J 0.0100 0.0625 1 03/15/2016 09:07 WG856331
Acrylonitrile U 0.00179 0.0125 1 03/15/2016 09:07 WG856331
Benzene 0.000415 J 0.000270 0.00125 1 03/15/2016 09:07 WG856331
Bromobenzene U 0.000284 0.00125 1 03/15/2016 09:07 WG856331
Bromodichloromethane U 0.000254 0.00125 1 03/15/2016 09:07 WG856331
Bromoform U 0.000424 0.00125 1 03/15/2016 09:07 WG856331
Bromomethane U 0.00134 0.00625 1 03/15/2016 09:07 WG856331
n-Butylbenzene U 0.000258 0.00125 1 03/15/2016 09:07 WG856331
sec-Butylbenzene U 0.000201 0.00125 1 03/15/2016 09:07 WG856331
tert-Butylbenzene U 0.000206 0.00125 1 03/15/2016 09:07 WG856331
Carbon tetrachloride U 0.000328 0.00125 1 03/15/2016 09:07 WG856331
Chlorobenzene U 0.000212 0.00125 1 03/15/2016 09:07 WG856331
Chlorodibromomethane U 0.000373 0.00125 1 03/15/2016 09:07 WG856331
Chloroethane U 0.000946 0.00625 1 03/15/2016 09:07 WG856331
2-Chloroethyl vinyl ether U J4 0.00234 0.0625 1 03/15/2016 09:07 WG856331
Chloroform U 0.000229 0.00625 1 03/15/2016 09:07 WG856331
Chloromethane U 0.000375 0.00313 1 03/15/2016 09:07 WG856331
2-Chlorotoluene U 0.000301 0.00125 1 03/15/2016 09:07 WG856331
4-Chlorotoluene U 0.000240 0.00125 1 03/15/2016 09:07 WG856331
1,2-Dibromo-3-Chloropropane U 0.00105 0.00625 1 03/15/2016 09:07 WG856331
1,2-Dibromoethane U 0.000343 0.00125 1 03/15/2016 09:07 WG856331
Dibromomethane U 0.000382 0.00125 1 03/15/2016 09:07 WG856331
1,2-Dichlorobenzene U 0.000305 0.00125 1 03/15/2016 09:07 WG856331
1,3-Dichlorobenzene U 0.000239 0.00125 1 03/15/2016 09:07 WG856331
1,4-Dichlorobenzene U 0.000226 0.00125 1 03/15/2016 09:07 WG856331
Dichlorodifluoromethane U 0.000713 0.00625 1 03/15/2016 09:07 WG856331
1,1-Dichloroethane U 0.000199 0.00125 1 03/15/2016 09:07 WG856331
1,2-Dichloroethane U 0.000265 0.00125 1 03/15/2016 09:07 WG856331
1,1-Dichloroethene U 0.000303 0.00125 1 03/15/2016 09:07 WG856331
cis-1,2-Dichloroethene U 0.000235 0.00125 1 03/15/2016 09:07 WG856331
trans-1,2-Dichloroethene U 0.000264 0.00125 1 03/15/2016 09:07 WG856331
1,2-Dichloropropane U 0.000358 0.00125 1 03/15/2016 09:07 WG856331
1,1-Dichloropropene U 0.000317 0.00125 1 03/15/2016 09:07 WG856331
1,3-Dichloropropane U 0.000207 0.00125 1 03/15/2016 09:07 WG856331
cis-1,3-Dichloropropene U 0.000262 0.00125 1 03/15/2016 09:07 WG856331
trans-1,3-Dichloropropene U 0.000267 0.00125 1 03/15/2016 09:07 WG856331
2,2-Dichloropropane U 0.000279 0.00125 1 03/15/2016 09:07 WG856331
Di-isopropyl ether U 0.000248 0.00125 1 03/15/2016 09:07 WG856331
Ethylbenzene U 0.000297 0.00125 1 03/15/2016 09:07 WG856331
Hexachloro-1,3-butadiene U 0.000342 0.00125 1 03/15/2016 09:07 WG856331
Isopropylbenzene U 0.000243 0.00125 1 03/15/2016 09:07 WG856331
p-Isopropyltoluene U 0.000204 0.00125 1 03/15/2016 09:07 WG856331
2-Butanone (MEK)U 0.00468 0.0125 1 03/15/2016 09:07 WG856331
Methylene Chloride U 0.00100 0.00625 1 03/15/2016 09:07 WG856331
4-Methyl-2-pentanone (MIBK)0.00837 J 0.00188 0.0125 1 03/15/2016 09:07 WG856331
Methyl tert-butyl ether U 0.000212 0.00125 1 03/15/2016 09:07 WG856331
Naphthalene 0.0103 0.00100 0.00625 1 03/15/2016 09:07 WG856331
n-Propylbenzene U 0.000206 0.00125 1 03/15/2016 09:07 WG856331
Styrene U 0.000234 0.00125 1 03/15/2016 09:07 WG856331
1,1,1,2-Tetrachloroethane U 0.000264 0.00125 1 03/15/2016 09:07 WG856331
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L823060
SP-3A
Collected date/time: 03/10/16 09:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2,2-Tetrachloroethane U 0.000365 0.00125 1 03/15/2016 09:07 WG856331
1,1,2-Trichlorotrifluoroethane U 0.000365 0.00125 1 03/15/2016 09:07 WG856331
Tetrachloroethene U 0.000276 0.00125 1 03/15/2016 09:07 WG856331
Toluene U 0.000434 0.00625 1 03/15/2016 09:07 WG856331
1,2,3-Trichlorobenzene U 0.000306 0.00125 1 03/15/2016 09:07 WG856331
1,2,4-Trichlorobenzene U 0.000388 0.00125 1 03/15/2016 09:07 WG856331
1,1,1-Trichloroethane U 0.000286 0.00125 1 03/15/2016 09:07 WG856331
1,1,2-Trichloroethane U 0.000277 0.00125 1 03/15/2016 09:07 WG856331
Trichloroethene U 0.000279 0.00125 1 03/15/2016 09:07 WG856331
Trichlorofluoromethane U 0.000382 0.00625 1 03/15/2016 09:07 WG856331
1,2,3-Trichloropropane U 0.000741 0.00313 1 03/15/2016 09:07 WG856331
1,2,4-Trimethylbenzene U 0.000211 0.00125 1 03/15/2016 09:07 WG856331
1,2,3-Trimethylbenzene U 0.000287 0.00125 1 03/15/2016 09:07 WG856331
1,3,5-Trimethylbenzene U 0.000266 0.00125 1 03/15/2016 09:07 WG856331
Vinyl chloride U 0.000291 0.00125 1 03/15/2016 09:07 WG856331
Xylenes, Total U 0.000698 0.00375 1 03/15/2016 09:07 WG856331
(S) Toluene-d8 102 88.7-115 03/15/2016 09:07 WG856331
(S) Dibromofluoromethane 111 76.3-123 03/15/2016 09:07 WG856331
(S) 4-Bromofluorobenzene 81.2 69.7-129 03/15/2016 09:07 WG856331
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L823060
SP-3B
Collected date/time: 03/10/16 09:23
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 74.0 1 03/12/2016 11:50 WG855891
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0289 J 0.0100 0.0676 1 03/15/2016 09:25 WG856331
Acrylonitrile U 0.00179 0.0135 1 03/15/2016 09:25 WG856331
Benzene U 0.000270 0.00135 1 03/15/2016 09:25 WG856331
Bromobenzene U 0.000284 0.00135 1 03/15/2016 09:25 WG856331
Bromodichloromethane U 0.000254 0.00135 1 03/15/2016 09:25 WG856331
Bromoform U 0.000424 0.00135 1 03/15/2016 09:25 WG856331
Bromomethane U 0.00134 0.00676 1 03/15/2016 09:25 WG856331
n-Butylbenzene U 0.000258 0.00135 1 03/15/2016 09:25 WG856331
sec-Butylbenzene U 0.000201 0.00135 1 03/15/2016 09:25 WG856331
tert-Butylbenzene U 0.000206 0.00135 1 03/15/2016 09:25 WG856331
Carbon tetrachloride U 0.000328 0.00135 1 03/15/2016 09:25 WG856331
Chlorobenzene U 0.000212 0.00135 1 03/15/2016 09:25 WG856331
Chlorodibromomethane U 0.000373 0.00135 1 03/15/2016 09:25 WG856331
Chloroethane U 0.000946 0.00676 1 03/15/2016 09:25 WG856331
2-Chloroethyl vinyl ether U J4 0.00234 0.0676 1 03/15/2016 09:25 WG856331
Chloroform U 0.000229 0.00676 1 03/15/2016 09:25 WG856331
Chloromethane U 0.000375 0.00338 1 03/15/2016 09:25 WG856331
2-Chlorotoluene U 0.000301 0.00135 1 03/15/2016 09:25 WG856331
4-Chlorotoluene U 0.000240 0.00135 1 03/15/2016 09:25 WG856331
1,2-Dibromo-3-Chloropropane U 0.00105 0.00676 1 03/15/2016 09:25 WG856331
1,2-Dibromoethane U 0.000343 0.00135 1 03/15/2016 09:25 WG856331
Dibromomethane U 0.000382 0.00135 1 03/15/2016 09:25 WG856331
1,2-Dichlorobenzene U 0.000305 0.00135 1 03/15/2016 09:25 WG856331
1,3-Dichlorobenzene U 0.000239 0.00135 1 03/15/2016 09:25 WG856331
1,4-Dichlorobenzene U 0.000226 0.00135 1 03/15/2016 09:25 WG856331
Dichlorodifluoromethane U 0.000713 0.00676 1 03/15/2016 09:25 WG856331
1,1-Dichloroethane U 0.000199 0.00135 1 03/15/2016 09:25 WG856331
1,2-Dichloroethane U 0.000265 0.00135 1 03/15/2016 09:25 WG856331
1,1-Dichloroethene U 0.000303 0.00135 1 03/15/2016 09:25 WG856331
cis-1,2-Dichloroethene U 0.000235 0.00135 1 03/15/2016 09:25 WG856331
trans-1,2-Dichloroethene U 0.000264 0.00135 1 03/15/2016 09:25 WG856331
1,2-Dichloropropane U 0.000358 0.00135 1 03/15/2016 09:25 WG856331
1,1-Dichloropropene U 0.000317 0.00135 1 03/15/2016 09:25 WG856331
1,3-Dichloropropane U 0.000207 0.00135 1 03/15/2016 09:25 WG856331
cis-1,3-Dichloropropene U 0.000262 0.00135 1 03/15/2016 09:25 WG856331
trans-1,3-Dichloropropene U 0.000267 0.00135 1 03/15/2016 09:25 WG856331
2,2-Dichloropropane U 0.000279 0.00135 1 03/15/2016 09:25 WG856331
Di-isopropyl ether U 0.000248 0.00135 1 03/15/2016 09:25 WG856331
Ethylbenzene U 0.000297 0.00135 1 03/15/2016 09:25 WG856331
Hexachloro-1,3-butadiene U 0.000342 0.00135 1 03/15/2016 09:25 WG856331
Isopropylbenzene U 0.000243 0.00135 1 03/15/2016 09:25 WG856331
p-Isopropyltoluene U 0.000204 0.00135 1 03/15/2016 09:25 WG856331
2-Butanone (MEK)U 0.00468 0.0135 1 03/15/2016 09:25 WG856331
Methylene Chloride U 0.00100 0.00676 1 03/15/2016 09:25 WG856331
4-Methyl-2-pentanone (MIBK)U 0.00188 0.0135 1 03/15/2016 09:25 WG856331
Methyl tert-butyl ether U 0.000212 0.00135 1 03/15/2016 09:25 WG856331
Naphthalene U 0.00100 0.00676 1 03/15/2016 09:25 WG856331
n-Propylbenzene U 0.000206 0.00135 1 03/15/2016 09:25 WG856331
Styrene U 0.000234 0.00135 1 03/15/2016 09:25 WG856331
1,1,1,2-Tetrachloroethane U 0.000264 0.00135 1 03/15/2016 09:25 WG856331
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L823060
SP-3B
Collected date/time: 03/10/16 09:23
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2,2-Tetrachloroethane U 0.000365 0.00135 1 03/15/2016 09:25 WG856331
1,1,2-Trichlorotrifluoroethane U 0.000365 0.00135 1 03/15/2016 09:25 WG856331
Tetrachloroethene U 0.000276 0.00135 1 03/15/2016 09:25 WG856331
Toluene U 0.000434 0.00676 1 03/15/2016 09:25 WG856331
1,2,3-Trichlorobenzene U 0.000306 0.00135 1 03/15/2016 09:25 WG856331
1,2,4-Trichlorobenzene U 0.000388 0.00135 1 03/15/2016 09:25 WG856331
1,1,1-Trichloroethane U 0.000286 0.00135 1 03/15/2016 09:25 WG856331
1,1,2-Trichloroethane U 0.000277 0.00135 1 03/15/2016 09:25 WG856331
Trichloroethene U 0.000279 0.00135 1 03/15/2016 09:25 WG856331
Trichlorofluoromethane U 0.000382 0.00676 1 03/15/2016 09:25 WG856331
1,2,3-Trichloropropane U 0.000741 0.00338 1 03/15/2016 09:25 WG856331
1,2,4-Trimethylbenzene U 0.000211 0.00135 1 03/15/2016 09:25 WG856331
1,2,3-Trimethylbenzene U 0.000287 0.00135 1 03/15/2016 09:25 WG856331
1,3,5-Trimethylbenzene U 0.000266 0.00135 1 03/15/2016 09:25 WG856331
Vinyl chloride U 0.000291 0.00135 1 03/15/2016 09:25 WG856331
Xylenes, Total U 0.000698 0.00406 1 03/15/2016 09:25 WG856331
(S) Toluene-d8 103 88.7-115 03/15/2016 09:25 WG856331
(S) Dibromofluoromethane 108 76.3-123 03/15/2016 09:25 WG856331
(S) 4-Bromofluorobenzene 86.4 69.7-129 03/15/2016 09:25 WG856331
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L823060
SP-3
Collected date/time: 03/10/16 09:32
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 82.5 1 03/12/2016 11:50 WG855891
Wet Chemistry by Method 9056A
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Sulfate 153 0.570 60.6 1 03/15/2016 01:46 WG855610
Mercury by Method 7471A
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0280 0.00280 0.0242 1 03/15/2016 08:37 WG855803
Metals (ICP) by Method 6010C
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic U 0.650 2.42 1 03/13/2016 19:01 WG855946
Barium 211 0.170 0.606 1 03/13/2016 19:01 WG855946
Cadmium 0.581 J 0.0700 0.606 1 03/13/2016 19:01 WG855946
Chromium 32.0 0.140 1.21 1 03/13/2016 19:01 WG855946
Lead 56.9 0.190 0.606 1 03/13/2016 19:01 WG855946
Selenium 2.41 J 0.740 2.42 1 03/13/2016 19:01 WG855946
Silver U 0.280 1.21 1 03/13/2016 19:01 WG855946
Sulfur 161 22.0 121 1 03/13/2016 19:01 WG855946
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.269 J 0.0642 0.400 10 03/16/2016 17:41 WG856576
Acenaphthylene U 0.0671 0.400 10 03/16/2016 17:41 WG856576
Anthracene 0.641 0.0632 0.400 10 03/16/2016 17:41 WG856576
Benzidine U 0.637 4.03 10 03/16/2016 17:41 WG856576
Benzo(a)anthracene 1.77 0.0428 0.400 10 03/16/2016 17:41 WG856576
Benzo(b)fluoranthene 1.73 0.0695 0.400 10 03/16/2016 17:41 WG856576
Benzo(k)fluoranthene 0.537 0.0582 0.400 10 03/16/2016 17:41 WG856576
Benzo(g,h,i)perylene 0.989 0.0721 0.400 10 03/16/2016 17:41 WG856576
Benzo(a)pyrene 1.41 0.0548 0.400 10 03/16/2016 17:41 WG856576
Bis(2-chlorethoxy)methane U 0.0770 4.03 10 03/16/2016 17:41 WG856576
Bis(2-chloroethyl)ether U 0.0896 4.03 10 03/16/2016 17:41 WG856576
Bis(2-chloroisopropyl)ether U 0.0760 4.03 10 03/16/2016 17:41 WG856576
4-Bromophenyl-phenylether U 0.114 4.03 10 03/16/2016 17:41 WG856576
2-Chloronaphthalene U 0.0639 0.400 10 03/16/2016 17:41 WG856576
4-Chlorophenyl-phenylether U 0.0627 4.03 10 03/16/2016 17:41 WG856576
Chrysene 1.52 0.0555 0.400 10 03/16/2016 17:41 WG856576
Dibenz(a,h)anthracene 0.269 J 0.0821 0.400 10 03/16/2016 17:41 WG856576
1,4-Dichlorobenzene U J3 0.109 4.03 10 03/16/2016 17:41 WG856576
3,3-Dichlorobenzidine U 0.794 4.03 10 03/16/2016 17:41 WG856576
2,4-Dinitrotoluene U J4 0.0607 4.03 10 03/16/2016 17:41 WG856576
2,6-Dinitrotoluene U 0.0737 4.03 10 03/16/2016 17:41 WG856576
Fluoranthene 3.24 0.0496 0.400 10 03/16/2016 17:41 WG856576
Fluorene 0.237 J 0.0682 0.400 10 03/16/2016 17:41 WG856576
Hexachlorobenzene U 0.0856 4.03 10 03/16/2016 17:41 WG856576
Hexachloro-1,3-butadiene U 0.100 4.03 10 03/16/2016 17:41 WG856576
Hexachlorocyclopentadiene U 0.587 4.03 10 03/16/2016 17:41 WG856576
Hexachloroethane U 0.134 4.03 10 03/16/2016 17:41 WG856576
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L823060
SP-3
Collected date/time: 03/10/16 09:32
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry)Qualifier MDL RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Indeno(1,2,3-cd)pyrene 0.882 0.0772 0.400 10 03/16/2016 17:41 WG856576
Isophorone U J4 0.0522 4.03 10 03/16/2016 17:41 WG856576
2-Methylphenol U 0.0986 4.03 10 03/16/2016 17:41 WG856576
3&4-Methyl Phenol U 0.0783 4.03 10 03/16/2016 17:41 WG856576
Naphthalene 0.115 J 0.0889 0.400 10 03/16/2016 17:41 WG856576
Nitrobenzene U 0.0695 4.03 10 03/16/2016 17:41 WG856576
n-Nitrosodimethylamine U 0.647 4.03 10 03/16/2016 17:41 WG856576
n-Nitrosodiphenylamine U 0.0594 4.03 10 03/16/2016 17:41 WG856576
n-Nitrosodi-n-propylamine U 0.0906 4.03 10 03/16/2016 17:41 WG856576
Phenanthrene 2.23 0.0528 0.400 10 03/16/2016 17:41 WG856576
Benzylbutyl phthalate U J4 0.103 4.03 10 03/16/2016 17:41 WG856576
Bis(2-ethylhexyl)phthalate U J4 0.120 4.03 10 03/16/2016 17:41 WG856576
Di-n-butyl phthalate U 0.109 4.03 10 03/16/2016 17:41 WG856576
Diethyl phthalate U J4 0.0691 4.03 10 03/16/2016 17:41 WG856576
Dimethyl phthalate U 0.0540 4.03 10 03/16/2016 17:41 WG856576
Di-n-octyl phthalate U J4 0.0907 4.03 10 03/16/2016 17:41 WG856576
Pyrene 2.97 0.123 0.400 10 03/16/2016 17:41 WG856576
1,2,4-Trichlorobenzene U 0.0876 4.03 10 03/16/2016 17:41 WG856576
4-Chloro-3-methylphenol U 0.0477 4.03 10 03/16/2016 17:41 WG856576
2-Chlorophenol U 0.0831 4.03 10 03/16/2016 17:41 WG856576
2,4-Dichlorophenol U 0.0746 4.03 10 03/16/2016 17:41 WG856576
2,4-Dimethylphenol U 0.471 4.03 10 03/16/2016 17:41 WG856576
4,6-Dinitro-2-methylphenol U 1.24 4.03 10 03/16/2016 17:41 WG856576
2,4-Dinitrophenol U 0.980 4.03 10 03/16/2016 17:41 WG856576
2-Nitrophenol U 0.130 4.03 10 03/16/2016 17:41 WG856576
4-Nitrophenol U J4 0.525 4.03 10 03/16/2016 17:41 WG856576
Pentachlorophenol U 0.480 4.03 10 03/16/2016 17:41 WG856576
Phenol U 0.0695 4.03 10 03/16/2016 17:41 WG856576
Pyridine U 0.628 4.03 10 03/16/2016 17:41 WG856576
2,4,5-Trichlorophenol U 0.104 4.03 10 03/16/2016 17:41 WG856576
2,4,6-Trichlorophenol U 0.0779 4.03 10 03/16/2016 17:41 WG856576
(S) 2-Fluorophenol 63.3 21.1-116 03/16/2016 17:41 WG856576
(S) Phenol-d5 64.2 26.3-121 03/16/2016 17:41 WG856576
(S) Nitrobenzene-d5 73.2 21.9-129 03/16/2016 17:41 WG856576
(S) 2-Fluorobiphenyl 73.1 34.9-129 03/16/2016 17:41 WG856576
(S) 2,4,6-Tribromophenol 53.9 21.6-142 03/16/2016 17:41 WG856576
(S) p-Terphenyl-d14 74.7 21.5-128 03/16/2016 17:41 WG856576
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG855891
Total Solids by Method 2540 G-2011 L823060-01,02,03
Method Blank (MB)
(MB) 03/12/16 11:50
MB Result MB Qualifier MB RDL
Analyte %%
Total Solids 0.000500
L823060-01 Original Sample (OS) • Duplicate (DUP)
(OS) 03/12/16 11:50 • (DUP) 03/12/16 11:50
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte %% % %
Total Solids 79.9 78.6 1 1.70 5
Laboratory Control Sample (LCS)
(LCS) 03/12/16 11:50
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG855610
Wet Chemistry by Method 9056A L823060-03
Method Blank (MB)
(MB) 03/14/16 23:46
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Sulfate U 0.57 50.0
L822572-02 Original Sample (OS) • Duplicate (DUP)
(OS) 03/15/16 02:58 • (DUP) 03/15/16 03:22
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/kg mg/kg % %
Sulfate 99.3 108 1 8 15
L822711-58 Original Sample (OS) • Duplicate (DUP)
(OS) 03/15/16 12:32 • (DUP) 03/15/16 12:56
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/kg mg/kg % %
Sulfate 3.92 3.77 1 4 J 15
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 03/15/16 00:10 • (LCSD) 03/15/16 00:34
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Sulfate 200 207 208 103 104 80-120 0 15
L822711-56 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 03/15/16 03:45 • (MS) 03/15/16 04:09 • (MSD) 03/15/16 04:33
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Sulfate 500 4.80 513 515 102 102 1 80-120 J J 0 15
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG855803
Mercury by Method 7471A L823060-03
Method Blank (MB)
(MB) 03/15/16 07:34
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0028 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 03/15/16 07:36 • (LCSD) 03/15/16 07:39
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Mercury 0.300 0.268 0.282 89 94 80-120 5 20
L822841-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 03/15/16 07:42 • (MS) 03/15/16 07:44 • (MSD) 03/15/16 07:47
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.300 0.000668 0.244 0.244 81 81 1 75-125 0 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG855946
Metals (ICP) by Method 6010C L823060-03
Method Blank (MB)
(MB) 03/13/16 18:37
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Arsenic U 0.65 2.00
Barium U 0.17 0.500
Cadmium U 0.07 0.500
Chromium U 0.14 1.00
Lead U 0.19 0.500
Selenium U 0.74 2.00
Silver U 0.28 1.00
Sulfur U 22 100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 03/13/16 18:40 • (LCSD) 03/13/16 18:43
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Arsenic 100 94.4 99.2 94 99 80-120 5 20
Barium 100 97.3 102 97 102 80-120 5 20
Cadmium 100 96.5 101 97 101 80-120 5 20
Chromium 100 94.1 98.5 94 99 80-120 5 20
Lead 100 98.8 103 99 103 80-120 5 20
Selenium 100 94.2 98.6 94 99 80-120 4 20
Silver 100 90.9 95.1 91 95 80-120 4 20
Sulfur 1000 876 920 88 92 80-120 5 20
L822912-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 03/13/16 18:46 • (MS) 03/13/16 18:55 • (MSD) 03/13/16 18:58
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Arsenic 100 4.03 98.5 94.5 94 90 1 75-125 4 20
Barium 100 8.55 107 104 99 95 1 75-125 3 20
Cadmium 100 0.0685 100 97.3 100 97 1 75-125 3 20
Chromium 100 17.5 112 108 95 91 1 75-125 3 20
Lead 100 6.74 110 106 103 99 1 75-125 4 20
Selenium 100 1.26 94.1 90.4 93 89 1 75-125 4 20
Silver 100 ND 94.4 92.1 94 92 1 75-125 2 20
Sulfur 1000 155 1080 1020 93 86 1 75-125 6 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG856331
Volatile Organic Compounds (GC/MS) by Method 8260B L823060-01,02
Method Blank (MB)
(MB) 03/15/16 07:41
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0100 0.0500
Acrylonitrile U 0.00179 0.0100
Benzene U 0.000270 0.00100
Bromobenzene U 0.000284 0.00100
Bromodichloromethane U 0.000254 0.00100
Bromoform U 0.000424 0.00100
Bromomethane U 0.00134 0.00500
n-Butylbenzene U 0.000258 0.00100
sec-Butylbenzene U 0.000201 0.00100
tert-Butylbenzene U 0.000206 0.00100
Carbon tetrachloride U 0.000328 0.00100
Chlorobenzene U 0.000212 0.00100
Chlorodibromomethane U 0.000373 0.00100
Chloroethane U 0.000946 0.00500
2-Chloroethyl vinyl ether U 0.00234 0.0500
Chloroform U 0.000229 0.00500
Chloromethane U 0.000375 0.00250
2-Chlorotoluene U 0.000301 0.00100
4-Chlorotoluene U 0.000240 0.00100
1,2-Dibromo-3-Chloropropane U 0.00105 0.00500
1,2-Dibromoethane U 0.000343 0.00100
Dibromomethane U 0.000382 0.00100
1,2-Dichlorobenzene U 0.000305 0.00100
1,3-Dichlorobenzene U 0.000239 0.00100
1,4-Dichlorobenzene U 0.000226 0.00100
Dichlorodifluoromethane U 0.000713 0.00500
1,1-Dichloroethane U 0.000199 0.00100
1,2-Dichloroethane U 0.000265 0.00100
1,1-Dichloroethene U 0.000303 0.00100
cis-1,2-Dichloroethene U 0.000235 0.00100
trans-1,2-Dichloroethene U 0.000264 0.00100
1,2-Dichloropropane U 0.000358 0.00100
1,1-Dichloropropene U 0.000317 0.00100
1,3-Dichloropropane U 0.000207 0.00100
cis-1,3-Dichloropropene U 0.000262 0.00100
trans-1,3-Dichloropropene U 0.000267 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG856331
Volatile Organic Compounds (GC/MS) by Method 8260B L823060-01,02
Method Blank (MB)
(MB) 03/15/16 07:41
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
2,2-Dichloropropane U 0.000279 0.00100
Di-isopropyl ether U 0.000248 0.00100
Ethylbenzene U 0.000297 0.00100
Hexachloro-1,3-butadiene U 0.000342 0.00100
Isopropylbenzene U 0.000243 0.00100
p-Isopropyltoluene U 0.000204 0.00100
2-Butanone (MEK)U 0.00468 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK)U 0.00188 0.0100
Methyl tert-butyl ether U 0.000212 0.00100
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.000206 0.00100
Styrene U 0.000234 0.00100
1,1,1,2-Tetrachloroethane U 0.000264 0.00100
1,1,2,2-Tetrachloroethane U 0.000365 0.00100
Tetrachloroethene U 0.000276 0.00100
Toluene U 0.000434 0.00500
1,1,2-Trichlorotrifluoroethane U 0.000365 0.00100
1,2,3-Trichlorobenzene U 0.000306 0.00100
1,2,4-Trichlorobenzene U 0.000388 0.00100
1,1,1-Trichloroethane U 0.000286 0.00100
1,1,2-Trichloroethane U 0.000277 0.00100
Trichloroethene U 0.000279 0.00100
Trichlorofluoromethane U 0.000382 0.00500
1,2,3-Trichloropropane U 0.000741 0.00250
1,2,3-Trimethylbenzene U 0.000287 0.00100
1,2,4-Trimethylbenzene U 0.000211 0.00100
1,3,5-Trimethylbenzene U 0.000266 0.00100
Vinyl chloride U 0.000291 0.00100
Xylenes, Total U 0.000698 0.00300
(S) Toluene-d8 103 88.7-115
(S) Dibromofluoromethane 103 76.3-123
(S) 4-Bromofluorobenzene 88.8 69.7-129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG856331
Volatile Organic Compounds (GC/MS) by Method 8260B L823060-01,02
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 03/15/16 06:29 • (LCSD) 03/15/16 06:47
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.125 0.0951 0.101 76.1 81.0 25.3-178 6.29 22.9
Acrylonitrile 0.125 0.134 0.147 107 118 57.8-143 9.49 20
Benzene 0.0250 0.0263 0.0266 105 106 72.6-120 1.16 20
Bromobenzene 0.0250 0.0231 0.0242 92.6 96.9 80.3-115 4.53 20
Bromodichloromethane 0.0250 0.0242 0.0245 96.8 98.1 75.3-119 1.29 20
Bromoform 0.0250 0.0220 0.0234 88.2 93.6 69.1-135 5.98 20
Bromomethane 0.0250 0.0269 0.0283 108 113 23.0-191 5.27 20
n-Butylbenzene 0.0250 0.0256 0.0257 103 103 74.2-134 0.260 20
sec-Butylbenzene 0.0250 0.0224 0.0236 89.7 94.4 77.8-129 5.10 20
tert-Butylbenzene 0.0250 0.0227 0.0239 90.7 95.7 77.2-129 5.32 20
Carbon tetrachloride 0.0250 0.0230 0.0233 92.0 93.1 69.4-129 1.22 20
Chlorobenzene 0.0250 0.0240 0.0251 96.0 100 78.9-122 4.51 20
Chlorodibromomethane 0.0250 0.0233 0.0239 93.4 95.5 76.4-126 2.28 20
Chloroethane 0.0250 0.0274 0.0283 109 113 47.2-147 3.24 20
2-Chloroethyl vinyl ether 0.125 0.201 0.212 161 169 16.7-162 J4 5.40 23.7
Chloroform 0.0250 0.0244 0.0248 97.7 99.2 73.3-122 1.50 20
Chloromethane 0.0250 0.0282 0.0288 113 115 53.1-135 2.03 20
2-Chlorotoluene 0.0250 0.0236 0.0248 94.5 99.1 74.6-127 4.82 20
4-Chlorotoluene 0.0250 0.0237 0.0246 94.7 98.4 79.5-123 3.76 20
1,2-Dibromo-3-Chloropropane 0.0250 0.0231 0.0239 92.4 95.5 64.9-131 3.36 20
1,2-Dibromoethane 0.0250 0.0229 0.0237 91.8 94.9 78.7-123 3.37 20
Dibromomethane 0.0250 0.0240 0.0244 96.1 97.6 78.5-117 1.61 20
1,2-Dichlorobenzene 0.0250 0.0242 0.0245 97.0 97.9 83.6-119 0.940 20
1,3-Dichlorobenzene 0.0250 0.0228 0.0240 91.4 96.0 75.9-129 4.88 20
1,4-Dichlorobenzene 0.0250 0.0245 0.0245 97.8 97.8 81.0-115 0.0200 20
Dichlorodifluoromethane 0.0250 0.0279 0.0267 112 107 50.9-139 4.28 20
1,1-Dichloroethane 0.0250 0.0266 0.0266 106 106 71.7-125 0.0500 20
1,2-Dichloroethane 0.0250 0.0245 0.0246 98.2 98.5 67.2-121 0.340 20
1,1-Dichloroethene 0.0250 0.0253 0.0252 101 101 60.6-133 0.280 20
cis-1,2-Dichloroethene 0.0250 0.0254 0.0253 101 101 76.1-121 0.250 20
trans-1,2-Dichloroethene 0.0250 0.0251 0.0250 100 100 70.7-124 0.0900 20
1,2-Dichloropropane 0.0250 0.0264 0.0266 106 106 76.9-123 0.640 20
1,1-Dichloropropene 0.0250 0.0266 0.0265 106 106 71.2-126 0.390 20
1,3-Dichloropropane 0.0250 0.0251 0.0261 100 104 80.3-114 3.86 20
cis-1,3-Dichloropropene 0.0250 0.0263 0.0264 105 106 77.3-123 0.460 20
trans-1,3-Dichloropropene 0.0250 0.0259 0.0275 104 110 73.0-127 5.81 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG856331
Volatile Organic Compounds (GC/MS) by Method 8260B L823060-01,02
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 03/15/16 06:29 • (LCSD) 03/15/16 06:47
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
2,2-Dichloropropane 0.0250 0.0210 0.0218 83.8 87.2 61.9-132 3.97 20
Di-isopropyl ether 0.0250 0.0265 0.0270 106 108 67.2-131 1.82 20
Ethylbenzene 0.0250 0.0235 0.0246 94.2 98.2 78.6-124 4.20 20
Hexachloro-1,3-butadiene 0.0250 0.0236 0.0239 94.4 95.7 69.2-136 1.43 20
Isopropylbenzene 0.0250 0.0216 0.0225 86.6 90.0 79.4-126 3.94 20
p-Isopropyltoluene 0.0250 0.0232 0.0244 92.6 97.6 75.4-132 5.27 20
2-Butanone (MEK)0.125 0.108 0.116 86.5 92.8 44.5-154 7.12 21.3
Methylene Chloride 0.0250 0.0252 0.0258 101 103 68.2-119 2.34 20
4-Methyl-2-pentanone (MIBK)0.125 0.123 0.131 98.4 105 61.1-138 6.63 20
Methyl tert-butyl ether 0.0250 0.0236 0.0243 94.3 97.0 70.2-122 2.86 20
Naphthalene 0.0250 0.0226 0.0239 90.3 95.7 69.9-132 5.78 20
n-Propylbenzene 0.0250 0.0228 0.0238 91.1 95.1 80.2-124 4.21 20
Styrene 0.0250 0.0241 0.0252 96.2 101 79.4-124 4.67 20
1,1,1,2-Tetrachloroethane 0.0250 0.0228 0.0238 91.3 95.2 76.7-127 4.13 20
1,1,2,2-Tetrachloroethane 0.0250 0.0220 0.0237 87.9 94.9 78.8-124 7.62 20
Tetrachloroethene 0.0250 0.0228 0.0243 91.3 97.2 71.1-133 6.24 20
Toluene 0.0250 0.0250 0.0251 99.8 100 76.7-116 0.670 20
1,1,2-Trichlorotrifluoroethane 0.0250 0.0259 0.0256 104 102 62.6-138 1.04 20
1,2,3-Trichlorobenzene 0.0250 0.0239 0.0251 95.6 100 72.5-137 4.69 20
1,2,4-Trichlorobenzene 0.0250 0.0251 0.0258 100 103 74.0-137 2.73 20
1,1,1-Trichloroethane 0.0250 0.0239 0.0240 95.6 95.9 69.9-127 0.320 20
1,1,2-Trichloroethane 0.0250 0.0235 0.0244 94.2 97.7 81.9-119 3.66 20
Trichloroethene 0.0250 0.0251 0.0253 101 101 77.2-122 0.710 20
Trichlorofluoromethane 0.0250 0.0223 0.0223 89.1 89.4 51.5-151 0.360 20
1,2,3-Trichloropropane 0.0250 0.0213 0.0243 85.3 97.1 74.0-124 13.0 20
1,2,3-Trimethylbenzene 0.0250 0.0237 0.0237 94.9 95.0 79.4-118 0.110 20
1,2,4-Trimethylbenzene 0.0250 0.0224 0.0234 89.8 93.6 77.1-124 4.15 20
1,3,5-Trimethylbenzene 0.0250 0.0220 0.0230 88.0 92.0 79.0-125 4.42 20
Vinyl chloride 0.0250 0.0281 0.0282 112 113 58.4-134 0.520 20
Xylenes, Total 0.0750 0.0702 0.0720 93.6 96.0 78.1-123 2.60 20
(S) Toluene-d8 102 101 88.7-115
(S) Dibromofluoromethane 102 102 76.3-123
(S) 4-Bromofluorobenzene 89.2 93.2 69.7-129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG856576
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L823060-03
Method Blank (MB)
(MB) 03/16/16 17:16
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00642 0.0330
Acenaphthylene U 0.00671 0.0330
Anthracene U 0.00632 0.0330
Benzidine U 0.0637 0.333
Benzo(a)anthracene U 0.00428 0.0330
Benzo(b)fluoranthene U 0.00695 0.0330
Benzo(k)fluoranthene U 0.00582 0.0330
Benzo(g,h,i)perylene U 0.00721 0.0330
Benzo(a)pyrene U 0.00548 0.0330
Bis(2-chlorethoxy)methane U 0.00770 0.333
Bis(2-chloroethyl)ether U 0.00896 0.333
Bis(2-chloroisopropyl)ether U 0.00760 0.333
4-Bromophenyl-phenylether U 0.0114 0.333
2-Chloronaphthalene U 0.00639 0.0330
4-Chlorophenyl-phenylether U 0.00627 0.333
Chrysene U 0.00555 0.0330
Dibenz(a,h)anthracene U 0.00821 0.0330
1,4-Dichlorobenzene U 0.0109 0.333
3,3-Dichlorobenzidine U 0.0794 0.333
2,4-Dinitrotoluene U 0.00607 0.333
2,6-Dinitrotoluene U 0.00737 0.333
Fluoranthene U 0.00496 0.0330
Fluorene U 0.00682 0.0330
Hexachlorobenzene U 0.00856 0.333
Hexachloro-1,3-butadiene U 0.0100 0.333
Hexachlorocyclopentadiene U 0.0587 0.333
Hexachloroethane U 0.0134 0.333
Indeno(1,2,3-cd)pyrene U 0.00772 0.0330
Isophorone U 0.00522 0.333
Naphthalene U 0.00889 0.0330
Nitrobenzene U 0.00695 0.333
n-Nitrosodimethylamine U 0.0647 0.333
n-Nitrosodiphenylamine U 0.00594 0.333
n-Nitrosodi-n-propylamine U 0.00906 0.333
Phenanthrene U 0.00528 0.0330
Benzylbutyl phthalate U 0.0103 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG856576
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L823060-03
Method Blank (MB)
(MB) 03/16/16 17:16
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Bis(2-ethylhexyl)phthalate U 0.0120 0.333
Di-n-butyl phthalate U 0.0109 0.333
Diethyl phthalate U 0.00691 0.333
Dimethyl phthalate U 0.00540 0.333
Di-n-octyl phthalate U 0.00907 0.333
Pyrene U 0.0123 0.0330
Pyridine U 0.0628 0.333
1,2,4-Trichlorobenzene U 0.00876 0.333
4-Chloro-3-methylphenol U 0.00477 0.333
2-Chlorophenol U 0.00831 0.333
2-Methylphenol U 0.00986 0.333
3&4-Methyl Phenol U 0.00783 0.333
2,4-Dichlorophenol U 0.00746 0.333
2,4-Dimethylphenol U 0.0471 0.333
4,6-Dinitro-2-methylphenol U 0.124 0.333
2,4-Dinitrophenol U 0.0980 0.333
2-Nitrophenol U 0.0130 0.333
4-Nitrophenol U 0.0525 0.333
Pentachlorophenol U 0.0480 0.333
Phenol U 0.00695 0.333
2,4,5-Trichlorophenol U 0.0104 0.333
2,4,6-Trichlorophenol U 0.00779 0.333
(S) Nitrobenzene-d5 77.9 21.9-129
(S) 2-Fluorobiphenyl 78.2 34.9-129
(S) p-Terphenyl-d14 86.2 21.5-128
(S) Phenol-d5 76.6 26.3-121
(S) 2-Fluorophenol 75.9 21.1-116
(S) 2,4,6-Tribromophenol 72.4 21.6-142
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 03/16/16 16:26 • (LCSD) 03/16/16 16:51
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.667 0.540 0.621 81.0 93.1 48.9-107 13.9 20
Acenaphthylene 0.667 0.588 0.655 88.2 98.2 49.2-111 10.7 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG856576
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L823060-03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 03/16/16 16:26 • (LCSD) 03/16/16 16:51
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Anthracene 0.667 0.557 0.633 83.5 94.9 52.0-112 12.7 20
Benzidine 0.667 0.162 0.164 24.3 24.6 0.000-48.0 0.880 40
Benzo(a)anthracene 0.667 0.545 0.623 81.7 93.4 52.3-106 13.5 20
Benzo(b)fluoranthene 0.667 0.528 0.603 79.2 90.4 51.3-106 13.2 20
Benzo(k)fluoranthene 0.667 0.562 0.642 84.3 96.2 52.9-107 13.3 20
Benzo(g,h,i)perylene 0.667 0.606 0.682 90.8 102 45.8-108 11.9 20
Benzo(a)pyrene 0.667 0.571 0.634 85.6 95.0 51.9-106 10.4 20
Bis(2-chlorethoxy)methane 0.667 0.534 0.584 80.1 87.6 44.9-108 9.02 20
Bis(2-chloroethyl)ether 0.667 0.481 0.540 72.1 81.0 32.5-112 11.6 26
Bis(2-chloroisopropyl)ether 0.667 0.497 0.561 74.4 84.1 40.4-99.0 12.2 20.7
4-Bromophenyl-phenylether 0.667 0.522 0.606 78.3 90.9 51.4-110 15.0 20
1,4-Dichlorobenzene 0.667 0.390 0.480 58.5 72.0 36.5-97.0 J3 20.6 20
2-Chloronaphthalene 0.667 0.581 0.629 87.1 94.2 47.1-105 7.83 20
4-Chlorophenyl-phenylether 0.667 0.521 0.592 78.0 88.7 48.1-108 12.8 20
Chrysene 0.667 0.545 0.606 81.6 90.9 54.4-110 10.7 20
Dibenz(a,h)anthracene 0.667 0.601 0.679 90.1 102 45.7-111 12.2 20
3,3-Dichlorobenzidine 0.667 0.520 0.612 77.9 91.8 21.0-101 16.4 22
2,4-Dinitrotoluene 0.667 0.660 0.763 99.0 114 53.0-112 J4 14.5 20
2,6-Dinitrotoluene 0.667 0.614 0.690 92.1 103 51.6-110 11.6 20
Fluoranthene 0.667 0.523 0.600 78.4 90.0 53.7-110 13.7 20
Fluorene 0.667 0.545 0.613 81.8 91.9 51.1-109 11.7 20
Hexachlorobenzene 0.667 0.521 0.590 78.0 88.4 43.2-104 12.5 20.1
Hexachloro-1,3-butadiene 0.667 0.504 0.563 75.5 84.4 41.5-112 11.1 20
Hexachlorocyclopentadiene 0.667 0.477 0.521 71.6 78.2 13.5-123 8.81 20.7
Hexachloroethane 0.667 0.462 0.556 69.3 83.4 36.2-103 18.5 22.7
Indeno(1,2,3-cd)pyrene 0.667 0.615 0.685 92.1 103 47.5-109 10.8 20
Isophorone 0.667 0.635 0.705 95.2 106 28.8-104 J4 10.6 20
Naphthalene 0.667 0.483 0.539 72.4 80.8 43.4-103 11.0 20
Nitrobenzene 0.667 0.589 0.656 88.3 98.3 40.7-109 10.7 21
n-Nitrosodimethylamine 0.667 0.395 0.460 59.2 68.9 18.1-122 15.3 23.5
n-Nitrosodiphenylamine 0.667 0.555 0.642 83.3 96.3 48.8-107 14.5 20
n-Nitrosodi-n-propylamine 0.667 0.597 0.649 89.5 97.4 43.3-109 8.38 20
Pyridine 0.667 0.166 0.198 24.8 29.7 10.0-90.0 17.9 38.3
Phenanthrene 0.667 0.538 0.607 80.6 91.0 51.6-107 12.1 20
Benzylbutyl phthalate 0.667 0.732 0.830 110 124 47.5-115 J4 12.5 20
Bis(2-ethylhexyl)phthalate 0.667 0.713 0.818 107 123 48.1-116 J4 13.6 20.5
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG856576
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L823060-03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 03/16/16 16:26 • (LCSD) 03/16/16 16:51
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Di-n-butyl phthalate 0.667 0.643 0.735 96.4 110 49.7-113 13.3 20
Diethyl phthalate 0.667 0.678 0.773 102 116 52.0-112 J4 13.1 20
Dimethyl phthalate 0.667 0.641 0.717 96.1 107 51.4-108 11.1 20
Di-n-octyl phthalate 0.667 0.733 0.827 110 124 49.6-112 J4 12.1 22
2-Methylphenol 0.667 0.506 0.568 75.9 85.2 42.4-100 11.6 20
3&4-Methyl Phenol 0.667 0.602 0.659 90.2 98.7 50.5-115 8.99 20
Pyrene 0.667 0.551 0.632 82.6 94.7 47.1-108 13.7 20
1,2,4-Trichlorobenzene 0.667 0.452 0.513 67.8 77.0 39.8-100 12.6 20
4-Chloro-3-methylphenol 0.667 0.642 0.709 96.3 106 51.1-113 9.88 20
2-Chlorophenol 0.667 0.490 0.566 73.5 84.9 40.8-103 14.3 20
2,4-Dichlorophenol 0.667 0.545 0.592 81.7 88.8 46.2-109 8.37 20
2,4,5-Trichlorophenol 0.667 0.573 0.628 85.9 94.1 43.3-110 9.10 20
2,4-Dimethylphenol 0.667 0.590 0.662 88.5 99.3 42.2-110 11.5 20
4,6-Dinitro-2-methylphenol 0.667 0.582 0.640 87.3 96.0 23.1-119 9.49 23.7
2,4-Dinitrophenol 0.667 0.293 0.300 44.0 45.0 10.0-105 2.30 36.5
2-Nitrophenol 0.667 0.625 0.676 93.7 101 44.2-113 7.83 20.9
4-Nitrophenol 0.667 0.676 0.748 101 112 34.8-109 J4 10.1 20
Pentachlorophenol 0.667 0.516 0.547 77.4 82.0 16.2-102 5.78 22.9
Phenol 0.667 0.542 0.589 81.3 88.3 41.5-106 8.22 20
2,4,6-Trichlorophenol 0.667 0.604 0.657 90.6 98.5 44.4-108 8.38 20
(S) Nitrobenzene-d5 86.2 92.3 21.9-129
(S) 2-Fluorobiphenyl 81.9 87.2 34.9-129
(S) p-Terphenyl-d14 83.2 95.1 21.5-128
(S) Phenol-d5 82.8 89.0 26.3-121
(S) 2-Fluorophenol 72.2 83.4 21.1-116
(S) 2,4,6-Tribromophenol 81.5 94.4 21.6-142
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Abbreviations and Definitions
SDG Sample Delivery Group.
MDL Method Detection Limit.
RDL Reported Detection Limit.
ND,U Not detected at the Reporting Limit (or MDL where applicable).
RPD Relative Percent Difference.
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry
report basis for soils].
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.Recovery.
SDL Sample Detection Limit.
MQL Method Quantitation Limit.
Unadj. MQL Unadjusted Method Quantitation Limit.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Our Locations
Alabama 40660
Alaska UST-080
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California 01157CA
Colorado TN00003
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Florida E87487
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Georgia 1 923
Idaho TN00003
Illinois 200008
Indiana C-TN-01
Iowa 364
Kansas E-10277
Kentucky 1 90010
Kentucky 2 16
Louisiana AI30792
Maine TN0002
Maryland 324
Massachusetts M-TN003
Michigan 9958
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Mississippi TN00003
Missouri 340
Montana CERT0086
Nebraska NE-OS-15-05
Nevada TN-03-2002-34
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New York 11742
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North Carolina 2 41
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Pennsylvania 68-02979
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A2LA – ISO 17025 1461.01
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EPA–Crypto TN00003
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DOD 1461.01
USDA S-67674
State Accreditations
Third Party & Federal Accreditations
ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other
lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the
network laboratories in our industry. The most significant benefit to our “one location” design is the design of our laboratory campus. The model is conducive to accelerated productivity,
decreasing turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please
contact our main office. ESC Lab Sciences performs all testing at our central laboratory.
1. Drinking Water 2. Underground Storage Tanks 3. Aquatic Toxicity 4. Chemical/Microbiological 5. Mold n/a Accreditation not applicable
1461.02A2LA – ISO 170255
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
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Contract Number:
Landfill :
Sales Rep
Bill To:
Acct #:Transporter Information:
Same
Generator Name:
Origin:Additional Notes:
Waste Name:
Trux Waste Code
Inbound Rate:29.00$UOM:Tons
Minimum:Fee/Taxes
(ERF/FRF/Admin/Local)
Other Charges:
(Trans, Backfill, App, etc.)
Historic Revolution
Guilford
(This should be set up at the Account level w/ Division)
Name:
Address
Address
Phone
Special Waste Summary Report
Cont. Soil-VG
CT Wilson Construction
333354
HR Uwharrie Env
3041161011
Excavated soil
Lucas Norris
ADDITIONALLY APPROVED BY:_____________________________ DATE:______________
ENTERED BY: ______________________________________ DATE:______________
APPENDIX B 
APPENDIX C 
DIVIDER PAGE
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