11045_Charlotte_Chemical_Revised_SMP_opt 4-10-12

REVISED
SOIL MANAGEMENT PLAN for
GRADING and SITE DEVELOPMENT ACTIVITIES
1200 SOUTH BOULEVARD APARTMENTS
FORMER SIMPSON’S LIGHTING PROPERTY
(CHARLOTTE CHEMICAL LABORATORY SITE)
1200 SOUTH BOULEVARD
CHARLOTTE, NORTH CAROLINA
PREPARED FOR:
1200 SOUTH BOULEVARD PARTNERS, LLC
4550 POST OAK PLACE,STE 225
HOUSTON, TEXAS 77027
PREPARED BY:
AMEC ENVIRONMENT & INFRASTRUCTURE, INC.
2801 YORKMONT AVE
CHARLOTTE, NORTH CAROLINA 28208
APRIL 10, 2012
AMEC PROJECT 6228-11-5486
Revised Soil Management Plan April 10, 2012
Charlotte Chemical Laboratory SiteAMEC Project 6228-11-5486
i
TABLE OF CONTENTS
Page
1.0INTRODUCTION .......................................................................................................................1
2.0PLANNED SITE DEVELOPMENT .........................................................................................1
3.0PREVIOUS ENVIRONMENTAL ASSESSMENT RESULTS...............................................2
3.1 2007 and 2008 Assessment Activities ...................................................................................3
3.2 2011 Assessment Activities...................................................................................................43.3 Environmental Assessment Conclusions...............................................................................5
4.0SOIL MANAGEMENT PROCEDURES AND CONSIDERATIONS...................................6
4.1 Environmental Goals and Criteria .........................................................................................64.2 Discovery of Environmental Conditions ...............................................................................74.3 Soil Management Procedures ................................................................................................8
4.4 Communications Procedures ...............................................................................................124.5 Health and Safety Considerations........................................................................................13
5.0REPORTING.............................................................................................................................14
Tables
Table 1: Summary of Soil Analytical Results-Metals
Table 2: Summary of Soil Analytical Results-VOCs
Table 3: Summary of Soil Analytical Results-SVOCs
Table 4: Summary of Groundwater Analytical Results
Table 5: Summary of Sump TCLP Metal Analytical Results
Figures
Figure 1: Site Location
Figure 2: Site Plan and Sample Location Plan
Appendices
Appendix A: Proposed Cut and Fill Plan
Appendix B: 2007 and 2008 Environmental Results
Appendix C: 2011 Laboratory Analytical Reports
Appendix D: 2011 Geophysical Survey Report
Revised Soil Management Plan April 10, 2012
Charlotte Chemical Laboratory SiteAMEC Project 6228-11-5486
1
1.0 INTRODUCTION
The Charlotte Chemical Laboratory (Former Simpson’s Lighting property) is a Brownfield Site with an
existing Brownfield Agreement (BFA) with the North Carolina Department of Environment and Natural
Resources (NCDENR) located at 1200 South Boulevard in Charlotte, Mecklenburg County, North
Carolina (Figure 1). The Notice of Brownfield Property (NBP) was made effective November 23, 2010
with the Prospective Developer, 1200 South Boulevard, LLC, who is also the current owner of the
property. The property is currently being evaluated for purchase by 1200 South Boulevard Partners, LLC.
The current owner is presently removing water mains and other utilities beneath Palmer Avenue at the site
and realigning the utilities to run across the northwest corner of the property and parallel to Carson Blvd.
Figure 2 provides a Site Plan of the property. This water-line realignment is being conducted under a
separate Soil Management Plan (SMP) prepared by others dated December 15, 2011 and approved by
NCDENR on December 21, 2011.
This SMP has been developed to address the site grading and subsequent development activities planned
by the current purchaser of the property should the property transaction be completed. In accordance with
the BFA, this SMP describes the responsibility of Contractors and Subcontractors in the event that
potentially-contaminated soil/materials are encountered during grading and site development activities. A
goal of describing this responsibility is to instill environmental awareness so that Site contractors and
subcontractors will recognize potential environmental concerns, immediately notify the appropriate
specified party, and manage impacted soils/environmental conditions using approved procedures
contained in this plan.
After reviewing the general site development plan and previous environmental assessment results, this
SMP presents procedures to follow during site grading and development activities.
2.0 PLANNED SITE DEVELOPMENT
1200 South Boulevard Partners, LLC is considering the purchase and redevelopment of the approximately
3-acre former Charlotte Chemical Laboratory property. Figure 2 provides a proposed site plan overlaid
with the current aerial photograph of the property and environmental sampling locations. As depicted on
Figure 2, the final site footprint is expected to cover the majority of the Property. The strip of land
extending 35-feet from the Charlotte Area Transit System (“CATS”) light rail center line is planned to be
deeded to CATS prior to acquisition of the remainder of the Property by 1200 South Boulevard Partners,
LLC. As described further below, aside from possible construction of a portion of a fire lane, 1200 South
Revised Soil Management Plan April 10, 2012
Charlotte Chemical Laboratory SiteAMEC Project 6228-11-5486
Page 2
Boulevard Partners is not planning any development activities on the 35-feet strip that will be owned by
CATS. The Site is proposed to be evenly graded by generally cutting soils from the northeastern and
southwestern portion of the property to fill the remaining portion of the Site (Appendix A provides the
currently proposed cut and fill plan for the site development). Following the site grading, a six story
structure is planned to include a two-story, open-air podium garage with four stories of apartments on top
of the garage. The 35-foot strip of land between the building and the CATS rail line is planned to be
covered with a roadway and landscaping that provides for emergency vehicle access to the property as
well as connect with the existing pedestrian walkway in this area. In addition, a hardscaped pedestrian
plaza for civic use is planned in the northwest corner of the Site near the intersection of the light rail line
and Carson Blvd. The plaza will provide open access to the public and supports the pedestrian friendly
nature of the area. The plaza will include a drinking water and pet fountain as well as a splash pad, all
supplied with City water.The splash pad is designed to drain towards the center of the pad where the
water will be collected into a vault and re-circulate until discharged to the building sewer system.The
area will cover the realigned water main in the northwest corner of the Site, will be paved with an
impervious surface, and will include landscaped planters and benches for public enjoyment.
The first floor of the parking garage will likely be cut approximately 10 feet into grade at the northeast
corner of the property and otherwise be level with the graded surface. A subterranean parking level will
be cut beneath the first floor garage to accommodate additional parking spaces. The subterranean parking
is planned in the west-northwestern portion of the Site as noted on Figure 2. During grading activities,
general soil disturbance will occur associated with removing remnant underground utilities then cutting
soils along the northern portion of the property and for the subsurface garage. The cut soils will be used
to balance the elevation across the property including raising the basement below the current Simpson’s
Lighting building to the planned final grade. Following grading, installation of building footings will also
cause soil disturbance.
3.0 PREVIOUS ENVIRONMENTAL ASSESSMENT RESULTS
Previous environmental and engineering studies have been performed at the property (described below)
associated with site redevelopment planning and associated due diligence activities. Environmental
assessments were conducted in 2007, 2008, and 2011.
Revised Soil Management Plan April 10, 2012
Charlotte Chemical Laboratory SiteAMEC Project 6228-11-5486
Page 3
3.1 2007 and 2008 Assessment Activities
In 2007 and 2008 the current owner of the property conducted site assessment activities as part of their
due diligence activities (2007) and subsequently as part of entering the NCDENR Brownfield Program
(2008). The analytical results from the 2007 and 2008 sampling activities are presented in Appendix B.
During these activities, the following environmental concerns were identified and evaluated:
Former Filling Station located in the front parking lot of the Simpson’s Lighting building along
South Boulevard;
Former Oil Storage Warehouses located beneath the southwest corner of the property and near the
central portion of the site (beneath the southwestern corner of the Simpson’s Lighting building);
Former Charlotte Chemical Test Laboratory located in the central and western portions of the
property;
Former Dye House located in the northwestern portion of the property; and
Historical underground storage tanks that were removed in 1999.
These areas of environmental concern were initially evaluated in 2007 when soil and groundwater
sampling activities were implemented by the current property owner. Soil impacts slightly exceeding
screening levels were identified at the former oil warehouses (polycyclic aromatic hydrocarbons (PAHs)
and oil and grease) and in the vicinity of the Former Chemical Lab (chlorobenzene and 1,4-
dichlorobenzene). Groundwater impacts slightly exceeding NCDENR 2L Groundwater standards were
detected beneath the Former Chemical Lab (1,2-, and 1,4-dichlorobenzene), the former Dye House
(diisopropyl ether), and the former oil house in the southern portion of the property (benzene and
naphthalene).
The current owner conducted additional environmental assessment activities in 2008 to further evaluate
the noted areas of concern and in support of entering NCDENR Brownfield Program. The assessment
activities focused on the former Dye House and Chemical Laboratory areas and additional areas along the
CATS right of way, the geothermal system at the property (geothermal wells and discharge sumps), and
adjacent to an electrical substation in the northern portion of the property. Sampling results identified soil
concentrations above applicable screening criteria primarily within the former Dye House and Chemical
Laboratory Areas in the southern and western portion of the property. The primary constituents of
concern in these areas include PAHs and metals. The groundwater sample results indicated non-detected
levels of constituents or concentrations below NCDENR 2L Groundwater Standards except for
bromodichloromethane that was detected in two of the geothermal wells. Note that the geothermal wells
Revised Soil Management Plan April 10, 2012
Charlotte Chemical Laboratory SiteAMEC Project 6228-11-5486
Page 4
are installed at depths ranging from 312 to 560 feet below grade and are generally cased with less than 90
feet of casing at the base of the well. The wells are planned to be properly abandoned in accordance with
NCDENR and Mecklenburg County requirements.
Samples from a thin layer of crusted mossy material were collected that had grown on the base of the two
geothermal sumps located beneath the loading docks on the western and southern portions of the
Simpson’s Lighting building. Results of these samples indicated elevated concentrations of metals.
However, the crusty material was subsequently eroded down the sumps by the geothermal system
discharge or otherwise eroding away, as explained in correspondence from the owners environmental
consultant to NCDENR dated September 12, 2011.
3.2 2011 Assessment Activities
In July 2011 the current purchaser of the property contracted AMEC to conduct additional environmental
investigation that included twenty-nine soil borings installed via direct push technology across the site
(Figure 2). The borings were installed at the former Charlotte Chemical Laboratory, Dye House and
Storage Area; the former Gasoline Station; the former Oil Storage Building and UST; as well as the
Parcel between E. Carson Boulevard and E. Palmer Street. AMEC sampled the borings for volatile
organic compounds (VOCs), semi-volatile compounds (SVOCs) and metals, based upon the results of
field screening with a photo-ionization detector (PID) and previous site history. AMEC sampled the
groundwater out of temporary wells installed in soil borings SB-17, SB-18 and SB-23 to SB-27 for
VOCs. AMEC also sampled the concrete base of the two geothermal sumps and sediment from a third
sediment trap identified during the 2011 sampling activities. The samples from the sumps were prepared
using the toxicity characteristic leaching procedure (TCLP) and the leachate was subsequently analyzed
for selected metals. The sampling activities were described in the scope of work provided to NCDENR
dated July 22, 2011 and approved on July 25, 2011.
Finally, a geophysical survey was conducted in selected areas of the site to evaluate the potential presence
of USTs in suspected areas (i.e., the former filling station and around the former residential structure at
the southeast corner of the site along South Boulevard). In addition, a geophysical survey was conducted
at the parcel between Palmer Ave. and Carson Blvd. to evaluate the potential presence of USTs because
of the planned grading that will cut soil from this area for use along the southern portion of the property.
Revised Soil Management Plan April 10, 2012
Charlotte Chemical Laboratory SiteAMEC Project 6228-11-5486
Page 5
Results of the environmental investigation are consistent with the findings of the previous assessment
activities and generally indicate that contamination is present in the site soils mainly south of Palmer
Avenue (Table 1, 2 & 3) in the vicinity of the former Chemical Laboratory and Dye House. The primary
constituents of concerns include metals and PAHs. Groundwater sampling results indicate VOCs are not
present above the NCDENR 2L Groundwater Standards in the recently sampled borings (Table 4).
Results of the sump sampling indicate that metal compounds in exceedance of regulatory levels are not
present and therefore do not require management as hazardous waste based on these results (Table 5).
The laboratory analytical reports from the recent sampling activities are provided in Appendix C.
The geophysical survey did not identify potential USTs at the site. However, a second concrete pad was
indicated beneath the existing parking area in the vicinity of the former filling station, and the survey was
not able to scan below the second concrete pad. This represents a limited portion of the site and gross
impacts are not anticipated based on the existing data from multiple borings in and around this area. The
scope and results of the geophysical survey are provided in Appendix D.
3.3 Environmental Assessment Conclusions
Based on the results of the environmental assessment activities, the following conclusions are made
related to the requirements of this SMP:
Soils in the northern portion of the Site, between Palmer Ave. and Carson Blvd., are not expected
to exhibit impacts from VOCs, SVOCs, or metals requiring additional action. Historical
information, soil analytical results, and the geophysical survey did not indicate the presence of
environmental concerns in this area. Therefore, soils from this portion of the site appear suitable
to use as fill across the balance of the property without limitation during the site grading
activities.
Soils south of Palmer Ave. generally indicated the presence of PAHs and metals that will require
active management in accordance using the procedures specified in Section 4.0 below. Site
contractors will potentially encounter these soils and associated impacts during removal of
remnant utilities, installation of building footings, or should additional cutting below grade be
required.
Revised Soil Management Plan April 10, 2012
Charlotte Chemical Laboratory SiteAMEC Project 6228-11-5486
Page 6
Groundwater has generally been encountered between 10 and 25 feet below grade at the Site and
is expected to flow generally south-southwest direction beneath the property. Minor impacts to
groundwater were identified in the southern and central portions of the property with both VOCs
and PAHs. Therefore, it is anticipated that groundwater management will be required should
groundwater be encountered during grading or site development activities in these areas. Should
groundwater be encountered that causes an exposure risk to onsite workers, existing groundwater
data will be evaluated to assess these potential risks. If removal of groundwater is required to
accommodate site development, the groundwater will be properly managed in accordance with
NCDENR requirements for appropriate offsite disposal or subsequent discharge.
Various fill material including bricks, wood, gravel, remnant building materials, etc was
encountered at the property during the 2011 assessment activities. Although not necessarily an
environmental concern, this material may require segregation for subsequent offsite disposal to
facilitate site development activities in accordance with procedures noted below and disposal
facility requirements.
4.0 SOIL MANAGEMENT PROCEDURES AND CONSIDERATIONS
In accordance with the BFA, this SMP addresses actions to be taken in the event that potential
environmental conditions are encountered at the project Site during grading activities. The following
sections present the environmental goals and criteria, discovery of environmental conditions, soil
management provisions, sampling methods and protocols, communication procedures, and health and
safety considerations.
4.1 Environmental Goals and Criteria
The procedures described in this SMP are designed to protect Site workers and future residents from the
following concerns:
Exposure to contaminated soil; and
Exposure to contaminated groundwater.
Potential exposure routes include contact with impacted soil and groundwater, inadvertent ingestion of
impacted soil and groundwater, inhalation of impacted dust, and inhalation of impacted vapors.
Revised Soil Management Plan April 10, 2012
Charlotte Chemical Laboratory SiteAMEC Project 6228-11-5486
Page 7
To achieve these goals, this plan specifies the following criteria:
Soils with contaminant concentrations exceeding Residential Health-Based Soil Remediation
Goals (SRGs) will not be exposed to residential users at the Site. The soils will either be placed
beneath the footprint of the planned building, hardscape features, or covered with a minimum two
feet of clean soil. A post grading sampling plan will be implemented, with NCDENR approval,
to evaluate surface soil concentrations in areas that will be exposed after development is
completed.The sampling will be conducted to confirm that the exposed soils meet Residential
Health-Based SRGs.If soils are identified that exceed Residential Health-Based SRGs, these
soils will be moved to an area planned to be beneath the building footprint or hardscape features
and confirmation samples will be collected.The post grading sampling plan will be submitted to
NCDENR review and approval prior to implementing the associated sampling field work.
Groundwater with contaminant concentrations exceeding NCDENR 2L Groundwater Standards
will not be exposed to residential users at the site. Groundwater use is restricted at the Site;
therefore, residential users are not expected to be exposed to site groundwater. However, if
groundwater is encountered during site grading or development activities precautions will be
taken to protect site workers from the exposure risks noted above.
4.2 Discovery of Environmental Conditions
Contractors and Subcontractors shall be constantly aware of the possible discovery of potentially-
contaminated soil (through the observation of unusual odors, staining, suspect pooled liquids,
underground structures or tanks, etc.) during grading and site development activities at the Site regardless
of whether the environmental consultant is present at the time of discovery. It is expected that the
environmental consultant will be present on site when site grading and/or development activities are
planned in known impacted areas to conduct field screening and document field observations. Therefore,
if an unexpected environmental condition is encountered or suspected while the environmental consultant
is not present, the Contractor or Subcontractor shall temporarily suspend work in that area, isolate the area
(i.e., restrict access to the area), and immediately inform the responsible persons listed in the
Communication Procedures section below.
As described previously, extensive site data, including historical site use information, soil and
groundwater assessment data, and geophysical survey data, has been collected across the site in support of
Revised Soil Management Plan April 10, 2012
Charlotte Chemical Laboratory SiteAMEC Project 6228-11-5486
Page 8
planning the site redevelopment activities. The data indicates that soils in the northern portion of the
property between Palmer Ave. and Carson Blvd. are expected to be suitable for use as fill across the Site.
Soils south of Palmer Ave. generally exhibit impacts that are expected to require management during site
preparation, grading, development, and post-development. As such, the soil management procedures
below generally recommend managing impacted soil to minimize worker exposure while ensuring that
the soil is deployed beneath an impervious surface.
4.3 Soil Management Procedures
The following procedures will be followed to meet the environmental goals and associated criteria
described above during site preparation, site grading, site development, and post development.
Site Preparation
In preparing the site for subsequent grading and development, it is anticipated that remnant
utilities, separate from the water main relocation project the current owner is implementing, may
be removed from the property. These include former storm drains, pipe chases associated with
the geothermal well system, and other similar utilities serving the Former Simpson’s Lighting
building.
Because the utilities are generally located in areas of known impacted soil south of Palmer Ave.,
the environmental consultant will be present during removal to properly document field
observations.
Fluids identified in the remnant utilities that must be removed to access the utilities will be
segregated into 55-gallon drum(s) and characterized for proper disposal.
Soils disturbed during the utility removal will be visually inspected and field observations will be
documented. The soils will be placed back within the utility excavation when such excavation is
known to be below the footprint of the building. Attempts will be made to replace soils in the
order they were excavated so that soils removed last will be the first placed back in the
excavation. If impacted soils are identified outside the footprint of the building, these soils will
placed beneath the building footprint, hardscape, or two feet of known clean fill to prevent future
exposure.
Site preparation activities also involve demolishing the Simpson’s Lighting building in
accordance with applicable Mecklenburg County rules and procedures. Recent environmental
data and information indicates that sumps associated with the geothermal system are no longer an
Revised Soil Management Plan April 10, 2012
Charlotte Chemical Laboratory SiteAMEC Project 6228-11-5486
Page 9
environmental concern. The data indicate these sumps do not require special waste disposal
consideration and can be managed with the other demolition debris. Following removal, piping
associated with the sumps will be visually inspected for sediments. If sediments are detected, the
piping will be rinsed to remove sediment by pressure washing the piping. The rinse water will be
collected for subsequent characterization and disposal.
The potential exists to encounter USTs beneath the concrete parking area in the vicinity of the
former filling station should the observed slabs be removed during site development. Previous
sampling activities do indicate a release downgradient of the filling station; however, an
estimated concentration of benzene orders of magnitude below the health-based screening level
was observed in boring SB-18 in this area. If encountered, USTs in this area will be isolated and
managed in accordance with NCDENR’s UST Section guidelines and in coordination with the
NCDENR Brownfield program. The contractor will not remove or otherwise disturb observed
USTs until proper safety precautions and associated planning have been implemented.
Site Grading
Soils are generally planned to be cut from the northeast and west-northwest portion of the Site
and used to balance the remaining portion of the property (Appendix A). Previous environmental
data indicates soils in the northeastern portion of the Site are not impacted. Therefore, the
environmental consultant will not be present at the site during grading of this area, but will be on-
call should an unexpected environmental condition be encountered. These soils will be placed in
the southern portion of the property to balance the elevation of the Site. However, since soils in
the west-northwest portion of the Site may be impacted with PAHs and metals based on previous
sampling, additional measures will be undertaken to address them. Grab samples collected
during the 2008 sampling activities and composite samples collected during the July 2011
sampling activities in the west-northwestern portion of the site indicate relatively low metal
concentrations only slightly above residential screening criteria except for the sample from
location SB-9 in 2008 (see attached Tables). Soils cut from the west-northwest portion of the Site
are planned to be placed within the basement beneath the Simpson’s Lighting Building. During
cutting, these soils will be screened by the environmental consultant with a mercury vapor meter
and an organic vapor analyzer and their placement within the Simpson’s Lighting basement or
other NCDENR-approved designated area beneath the footprint of the proposed building will be
documented.
Revised Soil Management Plan April 10, 2012
Charlotte Chemical Laboratory SiteAMEC Project 6228-11-5486
Page 10
Soils disturbed during the Site grading will be visually inspected and field observations
documented. Soils from known impacted areas will be placed below the building footprint,
hardscape, or two feet of known clean fill to prevent exposure.
Fill and other materials (i.e., bricks, concrete, wood, etc.) encountered during site grading will be
left in place if supported by the development activities. Otherwise the material segregated for
offsite disposal or recycling.
The balance of the site is planned to be filled using onsite soils. Therefore, the Contractor is not
expected to encounter environmental conditions on the southern portion of the property during
placement of the fill.
Should additional fill be required from an offsite source, it will be tested as agreed with
NCDENR to confirm it is below Residential Health-Based SRGs prior to accepting the fill on
site. The source of fill will be tested prior to bringing the fill to the site and samples will be
analyzed for VOCs, SVOCs, and HSL Metals. The sample results will be compared to
Residential Health-Based SRGs as well as commonly accepted background concentrations for
metals. The fill will be considered clean if it is below these screening criteria and suitable for use
on site without limitation.
Dust generation will be monitored visually during site grading and subsequent development
activities and control measures will be implemented as necessary to control excessive dust. In
particular, the grading contractor will wet soils during grading activities, as necessary, to prevent
excessive dust generation at the site.
Post grading sampling will be conducted upon completion of the grading activities and prior to
developing the site to assess soils within two feet of the ground surface that will be exposed; i.e.,
not covered with the building footprint or hardscape. The sampling will be confirmed with
NCDENR prior to implementing and will consist of collected soil samples from agreed upon
locations for VOC, PAH, and metals analysis. The results will be screened against Residential
Health-Based SRGs and commonly accepted background concentrations for this area. With
approval from NCDENR, soils exceeding the screening criteria will be placed beneath a barrier;
such as, the planned building footprint, hardscape, or two feet of clean fill. Otherwise the
material will be properly disposed offsite.
Revised Soil Management Plan April 10, 2012
Charlotte Chemical Laboratory SiteAMEC Project 6228-11-5486
Page 11
Site Development
Site development activities include preparing the site to accommodate the planned parking garage
and installing building foundations and utilities. Site development activities south of Palmer Ave.
are expected to encounter impacted soils based on existing site environmental data.
The parking garage is planned to be cut approximately 10 feet into the graded soils in the
northeast corner of the Site (near the corner of South Blvd. and Carson Blvd). Based on previous
site history and environmental data, environmental impacts are not anticipated in this area.
Should impacts be discovered, the soils will be placed beneath the building footprint, hardscape,
or two feet of known clean fill.
Subterranean parking is planned beneath the parking garage (see Figure 2).The subterranean
garage will provide additional parking spaces as required for the Site development. Site soils will
be cut in the planned area and there is the potential environmental impacts will be encountered.
Impacted soils will be placed in the basement beneath the existing Simpson’s Lighting building or
other designated area beneath the building footprint or hardscape to the extent practical. The
environmental consultant will be present during cutting soils from the west-northwest portion of
the site and will monitor the activities with a mercury vapor meter and an organic vapor analyzer.
If soils are encountered that are grossly contaminated based on field observations or otherwise
require off-site disposal, they will be staged in the northern corner of the site as described further
below for proper characterization and subsequent disposal with approval from NCDENR.
Building footings will be installed across the site based on the final structural and geotechnical
design. The footings are anticipated to encounter impacted soils on the southern portion of the
property that will require management. To the extent practical, soils exhibiting impacts as will be
placed beneath the building footprint, hardscape, or two feet of known clean fill.
Excess soil generated during site development activities and not required to balance the site
elevation will be stockpiled and covered with secured plastic sheeting to prevent erosion pending
their final disposition. The material will be appropriately tested based on its final disposition; i.e.,
use as fill at another off-site construction site, disposed at a permitted facility, etc. These excess
soils will be staged on plastic sheeting in the northern corner of the site where the proposed water
main is planned to cut across the site from Palmer Avenue to Carson Blvd.
Demolition debris and other building materials; such as, bricks, concrete, and wood, encountered
during site grading will be left in place if supported by the development activities. Otherwise the
material will be segregated for offsite disposal or recycling. These materials will be staged in the
Revised Soil Management Plan April 10, 2012
Charlotte Chemical Laboratory SiteAMEC Project 6228-11-5486
Page 12
northern corner of the site where the proposed water main is planned to cut across the site from
Palmer Avenue to Carson Blvd.
Surface water or groundwater encountered during site development will be allowed to reinfiltrate
into the ground to the extent practical. The contractor will also attempt to minimize potential
contact with groundwater during site development activities. Should groundwater be encountered
that causes an exposure risk to onsite workers, existing groundwater data will be evaluated to
assess potential risks. If removal of groundwater is required to accommodate site development,
the groundwater will be properly managed in accordance with NCDENR requirements for
appropriate offsite disposal or subsequent discharge.
4.4 Communications Procedures
In the event that obvious or suspected contaminated soil is identified during work activities when the
environmental consultant is not present, the Contractor or its Subcontractor should immediately contact
the appropriate individual(s) as identified below. The designated environmental consultant (i.e., AMEC
Environment & Infrastructure, Inc.) will mobilize to the site and assist with managing the identified
environmental condition.
Emergencies
Fire/Police/Ambulance 911
North Carolina Department of Environment and Natural ResourcesPrimary Contact Ms. Carolyn Minnich [phone] (office)
AMEC Environment and Infrastructure, Inc.
Primary Contact:Mr. Andrew Frantz [phone] (office)
[phone] (mobile)
Secondary Contact:Mr. Andy Clark [phone] (office)
[phone] (mobile)
South Boulevard Partners, LLC
Primary Contact:Mr. David Smelley [phone] (office)[phone] (mobile)
Secondary Contact:Mr. Turner Inscoe [phone] (mobile)
If any situation which arises is immediately dangerous to human health and/or the environment, the
Contractor and/or environmental consultant shall immediately evacuate the area, as appropriate to prevent
injury, and immediately notify the appropriate emergency response agency by dialing 911. The
Revised Soil Management Plan April 10, 2012
Charlotte Chemical Laboratory SiteAMEC Project 6228-11-5486
Page 13
Contractor shall then follow the above path of communication if the environmental consultant is not
present.
4.5 Health and Safety Considerations
Any Site contractor performing land disturbance activities in an area of known or suspected contaminated
materials is responsible for developing a Health and Safety Plan (HASP) to address the protection of its
workers who may be exposed to such impacted material. This requirement is in addition to any other
construction-related safety requirements applicable to the Contractor’s work (i.e., other OSHA
requirements, municipal requirements, etc.) The HASP must consider potential exposure to the impacted
material through inhalation of vapors and/or dust, dermal contact, and incidental ingestion. The
environmental consultant will also be responsible for developing its own HASP to address potential risks
associated with the site grading and development activities. The environmental consultant will develop
its HASP when the property transaction is completed and site development details and associated
schedule are finalized with the selected development Contractor. The environmental consultant’s HASP
will be made available to the contractor as an example for their consideration. This SMP specifies the
following considerations to be included in a HASP:
The Contractor’s site superintendent (or appropriate on-site designee) will have completed
OSHA’s 40-hour hazardous waste operations training and associated annual refreshers, as
required. This individual will be present on site at all times during the site grading and
development activities.
The Consultant’s site representatives will also have completed OSHA’s 40-hour hazardous waste
operations training and associated annual refreshers.
Contractor will be aware of potential environmental hazards and prepared to address such hazards
during site grading and development activities.
Contractor will conduct daily safety briefings regarding potential site hazards associated with the
planned activities.
Contractor will provide appropriate personal protective equipment (PPE) for its employees and
require such PPE of its subcontractors to protect against exposure to contaminants at the Site.
Provisions will be made to conduct field screening for vapors when cutting or otherwise exposing
soils known or suspected to be impacted with volatile organic compounds.
Revised Soil Management Plan April 10, 2012
Charlotte Chemical Laboratory SiteAMEC Project 6228-11-5486
Page 14
The HASP will include a description of the scope of work, potential safety hazards, and measures
to protect against the identified hazards.
Provisions will also be made to mitigate exposure to dust generated in known or suspected
impacted areas during site grading and development activities.
The HASP will also include clear directions to the nearest hospital emergency room and note
emergency contact numbers for easy reference.
5.0 REPORTING
Within 15 business days of receipt of contaminated soil waste disposal manifests and/or associated
laboratory analytical reports or completion of site activities, a written report regarding this plan’s
implementation will be submitted to NCDENR. The report will include activities related to this SMP
performed during site grading and development activities. The report will contain a description of the
field screening activities and results, soil sampling activities, and a description of the contaminated soil
management. The report will also describe if newly discovered areas of impacted soil or other
environmental conditions were encountered and how the soils/conditions were managed. Documentation
of impacted soil that was originally outside of the building footprint and subsequently moved beneath the
footprint will be documented with field notes, photographs, and noted on a site figure.
TABLES
TABLE 1
SUMMARY OF SOIL ANALYTICAL RESULTS - METALS
1200 SOUTH BOULEVARD
AMEC PROJECT: 6228-11-5486
Sample ID Date Sampled Depth Sampled Antimony Arsenic Beryllium Cadmium Copper Lead Manganese Mercury Nickel Selenium Silver Thallium Zinc Total
Chromium1
Hexavalent
Chromium
Trivalent
Chromium
COMP 1 7/27/2011 1-2 4.2 34.3 0.27 30.1 191 389 253 5.8 10.0 1.7 <0.54 <1.1 3,320 30.1 <1.9 30.1
SB-1*7/27/2011 1-2 4.7 52.2 0.34 2.3 69.1 334 300 0.94 11.4 1.3 0.43J 0.52J 614 25.2 ----
SB-2*7/27/2011 1-2 2.3 30.8 0.3 1.4 47 201 283 2.1 9.1 1.2 0.42J <1.1 228 19.2 ----
SB-3*7/27/2011 1-2 11.8 19.6 0.22 58.5 376 591 301 1.5 11.8 4.4 1.3 0.40J 7,430 20.6 ----
SB-4*7/27/2011 1-2 0.75 3.3 0.4 1.8 41.2 58.9 183 0.93 4 1.2 0.25J <1.1 65 20.8 ----
SB-5*7/27/2011 1-2 3.1 18 0.31 2 56.7 254 345 0.72 10.3 1.4 0.46J 0.315 320 27.1 ----
COMP 2 7/27/2011 3-5 1.9 30.9 0.26 2.6 91.6 192 191 10.1 5.8 <1.0 <0.52 <1.0 985 34.3 <1.7 34.3
COMP 3 7/27/2011 1-2 0.96 3.3 0.21 1.1 24.8 59.1 85.4 0.65 3.3 <0.93 <0.46 <0.93 97.7 20.9 <1.5 20.9
COMP 4 7/27/2011 3-5 0.59 6.1 0.28 0.51 29.3 150 111 4.2 4.0 <1.1 <0.57 <1.1 139 29.7 <2.2 29.7
COMP 5 7/27/2011 1-2 1.3 4.4 0.25 2.7 87.4 156 237 1.0 5.6 <1.2 <0.58 <1.2 1,400 14.3 <2.4 14.3
COMP 6 7/27/2011 3-5 0.58 3.2 0.33 1.1 35.8 58.7 305 1.6 3.8 <1.2 <0.58 <1.2 196 37.3 <2.3 37.3
SB-16 7/27/2011 3-4 1.6 6.3 0.29 4.8 115 232 151 0.8 5 <1.1 <0.55 <1.1 2,160 16.1 <2.4 16.1
SB-17 7/27/2011 13-14 <0.58 <0.58 0.3 3.9 73.6 10.6 52.2 0.037 2.8 1.6 <0.58 <1.2 20.7 35 <2.3 35
SB-18 7/27/2011 5-6 <0.58 1.1 0.58 3.1 48.8 18.3 532 0.078 13 <1.2 <0.58 <1.2 36.8 45.2 <2.6 45.2
SB-19 7/27/2011 1-2 <0.50 0.88 0.41 0.96 29.4 15 298 0.016 11.9 <0.99 <0.50 <0.99 37.7 24.2 <2.3 24.2
SB-20 7/27/2011 1-2 <0.52 3.7 0.84 1.6 30.7 9.3 328 0.012 12.2 <1.0 <0.52 <1.0 39 21 <2.4 21
SB-21 7/27/2011 1-2 <0.60 2.1 0.28 0.46 20.6 95.2 203 0.08 11.7 <1.2 <0.60 <1.2 111 34.4 <3.2 34.4
SB-22 7/27/2011 1-2 <0.55 0.65 <0.11 0.28 6.7 7.2 36.5 0.028 <0.55 <1.1 <0.55 <1.1 3.6 11.7 <2.8 11.7
SB-23 7/28/2011 12-13 <0.70 <0.70 0.58 2.2 50.3 5.3 178 0.019 10.0 <1.4 <0.70 <1.4 45.8 30.2 <2.8 30.2
SB-24 7/28/2011 6-7 <0.47 0.66 0.19 1.7 27.7 7.7 116 0.014 0.99 1.1 <0.47 <0.94 9.7 8.4 <2.4 8.4
SB-25 7/28/2011 12-13 <0.65 <0.65 <0.13 0.44 19.4 4.8 11.8 0.096 1.1 <1.3 <0.65 <1.3 6.5 17.7 <2.6 17.7
SB-26 7/28/2011 9-10 <0.48 <0.48 0.42 5.5 13.4 14 20.8 0.033 3.6 1.9 0.48 0.96 420 18.5 <2.1 18.5
SB-27 7/28/2011 12-13 <0.51 1.3 0.16 <0.10 31.5 10.7 210 0.038 2.4 <1.0 <0.51 <1.0 13 16 <2.2 16
SB-28 7/28/2011 1-2 <0.65 <0.65 0.20 1.6 36.4 9.9 36.1 0.13 1.6 1.8 <0.65 <1.3 14.5 21.7 <2.9 21.7
SB-29 7/28/2011 1-2 <0.62 1.3 0.13 <0.12 13.1 18.6 73.3 0.16 4.4 <1.2 <0.62 <1.2 23.2 8.9 <0.88 8.9
6.2 0.39 32 14 620 400 360 4.6 300 78 78 0.16 4,600 24,000 0.29 24,000
0.9 5.8 63 3.0 700 270 65 1.0 130 2.1 3.4 0.28 1,200 360,000 3.8 360,000
Notes:
1. The data indicates that total chromium at the site consists of trivalent chromium. Therefore, the remediation goals for trivalent chromium are used for total chromium.
SRGs = Inactive Hazardous Sites Branch, Preliminary Soil Remediation Goals, February 2012 Prepared By/Date:AJF 10/17/11
Bold values exceed the Residential Health-Based SRGs Checked By/Date:AMC 4/10/12
Concentrations shown in mg/kg (ppm)
Depths shown in feet below ground surface (bgs)
* Samples SB-1 - SB-5 comprise composite sample COMP-1
Residential Health-Based SRGs
Protection of Groundwater SRGs
Page 1 of 1
TABLE 2
SUMMARY OF SOIL ANALYTICAL RESULTS - VOCs
1200 SOUTH BOULEVARD
AMEC PROJECT: 6228-11-5486
Sample ID Date Sampled Depth Sampled Acetone Benzene 2-Butanone (MEK)tert-Butyl-benzene
SB-4 7/27/2011 1-2 39.3J <4.7 <94.8 <4.7
SB-10 7/27/2011 1-2 <89.8 <4.5 <89.8 <4.5
SB-13 7/27/2011 1-2 <90.7 <4.5 <90.7 <4.5
SB-16 7/27/2011 3-4 120 <4.4 5.7J <4.4
SB-17 7/27/2011 13-14 <109 <5.5 <109 <5.5
SB-18 7/27/2011 5-6 <90.8 3.9J <90.8 9.9
SB-19 7/27/2011 1-2 9.9J <4.1 <82.6 <4.1
SB-20 7/27/2011 1-2 29.8J <5.0 <100 <5.0
SB-21 7/27/2011 1-2 62.2J <4.1 <81.9 <4.1
SB-22 7/27/2011 1-2 <85.0 <4.3 <85.0 <4.3
SB-23 7/28/2011 12-13 <130 <6.5 <130 <6.5
SB-24 7/28/2011 6-7 <97.7 <4.9 <97.7 <4.9
SB-25 7/28/2011 12-13 <96.0 <4.8 <96.0 <4.8
SB-26 7/28/2011 9-10 <84.7 <4.2 <84.7 <4.2
SB-27 7/28/2011 12-13 <83.2 <4.2 <83.2 <4.2
SB-28 7/28/2011 1-2 <105 <5.3 <105 <5.3
SB-29 7/28/2011 1-2 <95.7 <4.8 <95.7 <4.8
12,000,000 1,100 5,600,000 NSL
24,000 7.3 16,000 1,700
Notes:
SRGs = Inactive Hazardous Sites Branch, Preliminary Soil Remediation Goals, February 2012 Prepared By/Date:AJF 10/17/11
Bold values exceed Residential Health-Based SRGs Checked By/Date:AMC 4/10/12
NSL = No standard listed
Concentrations shown in µg/kg (ppb)
Depths shown in feet below gound surface (bgs)
Residential Health-Based SRGs
Protection of Groundwater SRGs
Page 1 of 1
TABLE 3
SUMMARY OF SOIL ANALYTICAL RESULTS - SVOCs
1200 SOUTH BOULEVARD
AMEC PROJECT: 6228-11-5486
Sample ID Date Sampled Depth Sampled Anthracene Benzo(a)-
anthracene
Benzo(a)-
pyrene
Benzo(b)-
fluoranthene
Benzo(g,h,i)-
perylene
Benzo(k)-
fluoranthene
Butylbenzyl-
phthalate Chrysene Dibenz(a,h)-
anthracene
bis(2-
Ethylhexyl)-
phthalate
Fluoranthene Indeno(1,2,3-cd)-
pyrene 4-Nitrophenol Pentachloro-
phenol Phenanthrene Pyrene
COMP 1 7/27/2011 1-2 2,380J 12,800 9,960 9,420 3,850 9,470 <3,620 13,200 2,230J <3,620 20,300 3,990 <18,100 <18,100 3,780 17,200
SB-1*7/27/2011 1-2 258J 592 671 734 470 522 <379 740 1,925 <379 1,250 407 <1890 <1,890 935 987
SB-2*7/27/2011 1-2 <18,900 <18,900 <18,900 <18,900 <18,900 <18,900 <18,900 <18,900 <18,900 <18,900 <18,900 <18,900 <94,600 <94,600 <18,900 <18,900
SB-3*7/27/2011 1-2 <18,900 <18,900 <18,900 <18,900 <18,900 <18,900 <18,900 <18,900 <18,900 <18,900 <18,900 <18,900 <94,500 <94,500 <18,900 <18,900
SB-4*7/27/2011 1-2 <17,800 4,570J 5,920J 6,020J <17,800 6,720J <17,800 7,410J <17,800 <17,800 22,800 3,790J <17,800 <88,900 22,000 12,600J
SB-5*7/27/2011 1-2 <18,600 <18,600 <18,600 <18,600 <18,600 <18,600 <18,600 <18,600 <18,600 <18,600 <18,600 <18,600 <92,800 <92,800 <18,600 <18,600
COMP 2 7/27/2011 3-5 <3,830 3,190J 1,870J 1,690J <3,830 1,960J <3,830 3,390J <3,830 <3,830 1,630J <3,830 <19,100 <19,100 <3,830 2,250J
COMP 3 7/27/2011 1-2 <373 123J 89.4J 99.7J <373 77.0J 112J 139J <373 105J 132J <373 245J 92.4J 89.8J 141J
COMP 4 7/27/2011 3-5 <390 201J 201J 238J 172J 204J <390 271J <390 284J 473 155J 200J 80.4J 307J 387J
COMP 5 7/27/2011 1-2 <388 169J 158J 163J 131J 143J <388 213J <388 <388 313J 108J 79.3J <1,940 205J 259J
COMP 6 7/27/2011 3-5 <19,100 <19,100 <19,100 <19,100 <19,100 <19,100 <19,100 <19,100 <19,100 <19,100 <19,100 <19,100 <95,600 <95,600 <19,100 <19,100
SB-16 7/27/2011 3-4 <19,100 <19,100 <19,100 <19,100 <19,100 <19,100 <19,100 <19,100 <19,100 <19,100 <19,100 <19,100 <95,500 <95,500 <19,100 <19,100
SB-17 7/27/2011 13-14 <455 <455 <455 <455 <455 <455 <455 <455 <455 <455 <455 <455 <2,280 <2,280 <455 <455
SB-18 7/27/2011 5-6 <416 <416 <416 <416 <416 <416 <416 <416 <416 <416 <416 <416 <2,080 <2,080 <416 <416
SB-19 7/27/2011 1-2 <341 <341 <341 <341 <341 <341 <341 <341 <341 <341 <341 <341 <1,700 <1,700 <341 <341
SB-20 7/27/2011 1-2 <369 <369 92.3J 85.4J <369 98.4J <369 79.0J <369 <369 <369 <369 95.3J <1,840 <369 <369
SB-21 7/27/2011 1-2 <403 <403 <403 76.4J <403 <403 <403 68.3J <403 <403 89.0J <403 <2,020 <2,020 <403 78.8J
SB-22 7/27/2011 1-2 <370 <370 <370 <370 <370 <370 <370 <370 <370 <370 <370 <370 <1,850 <1,850 <370 <370
SB-23 7/28/2011 12-13 <498 <498 <498 <498 <498 <498 <498 <498 <498 <498 <498 <498 <2,490 <2,490 <498 <498
SB-24 7/28/2011 6-7 <432 <432 <432 <432 <432 <432 <432 <432 <432 <432 <432 <432 <2,160 <2,160 <432 <432
SB-25 7/28/2011 12-13 <455 <455 <455 <455 <455 <455 <455 <455 <455 <455 <455 <455 <2,270 <2,270 <455 <455
SB-26 7/28/2011 9-10 <398 <398 <398 <398 <398 <398 <398 <398 <398 <398 <398 <398 <1,990 <1,990 <398 <398
SB-27 7/28/2011 12-13 <374 <374 <374 <374 <374 <374 <374 <374 <374 <374 <374 <374 <1,870 <1,870 <374 <374
SB-28 7/28/2011 1-2 <443 <443 <443 <443 <443 <443 <443 <443 <443 <443 <443 <443 <2,210 <2,210 <443 <443
SB-29 7/28/2011 1-2 <419 <419 <419 <419 <419 <419 <419 <419 <419 <419 <419 <419 <2,100 <2,100 <419 <419
3,400,000 150 15 150 NSL 1,500 NSL 15,000 15 35,000 460,000 150 NSL 890 NSL 340,000660,000 180 59 600 7,800,000 5,900 NSL 18,000 190 7,200 330,000 2,000 NSL 31 68,000 220,000
Notes:
SRGs = Inactive Hazardous Sites Branch, Preliminary Soil Remediation Goals, February 2012 Prepared By/Date:AJF 10/17/11
Bold values exceed Residential Health-Based SRGs Checked By/Date:AMC 10/18/11
NSL = No standard listed
Concentrations shown in µg/kg (ppb)
Depths shown in feet below gound surface (bgs)
* Samples SB-1 - SB-5 comprise composite sample COMP-1
Residential Health-Based SRGsProtection of Groundwater SRGs
Page 1 of 1
TABLE 4
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
1200 SOUTH BOULEVARD
AMEC PROJECT: 6228-11-5486
Sample ID Date Sampled Acetone Chloroform
SB-17 7/28/2011 <25.0 <1.0
SB-18 7/29/2011 30.7 <1.0
SB-23 7/28/2011 <25.0 5.7
SB-24 7/28/2011 <25.0 12.6
SB-25 7/28/2011 <25.0 2.1
SB-26 7/28/2011 <25.0 <1.0
SB-27 7/28/2011 <25.0 <1.0
6,000 70
Notes:
Prepared By/Date:AJF 10/17/11
January 2010 Checked By/Date:AMC 10/18/11
2. Bold values exceed the 15A NCAC 2L Standards
3. Concentrations shown in µg/L (ppb)
15A NCAC 2L Standards
1. 15A NCAC 2L Standards = Title 15A of the
North Carolina Administartive Code Subchapter
2L Groundwater Quality Stadards
Page 1 of 1
TALBE 5
SUMMARY OF TCLP ANALYTICAL RESULTS
1200 SOUTH BOULEVARD
AMEC PROJECT: 6228-11-5486
Sample ID Date Sampled Barium Chromium
SUMP 1 7/29/2011 <0.50 0.13
SUMP 2 7/29/2011 0.85 <0.025
SUMP 3 7/29/2011 <0.50 0.038
100 5.0
Notes:
Concentrations shown in mg/L (ppm)Prepared By/Date:AJF 10/17/11
Checked By/Date:AMC 10/18/11
Regulatory Level
Page 1 of 1
FIGURES
PREPAREDBY DATE CHECKEDBY DATE JOB NUMBER FIGURE 16228-11-5486
Site Location
SITE LOCATION1200 SOUTH BOULEVARDCHARLOTTE, NORTH CAROLINA
0 1,000 2,000500Feet
p
§¨¦77
§¨¦85
§¨¦277
§¨¦77
£¤29
£¤74
£¤74£¤29
PROJECT VICINITY
Charlotte
Source: http://goto/arcgisonline.com/maps/World_Topo_Map, accessed 1/17/2012.
SJM AMC1/18/12 1/19/12
PREPAREDBY DATE CHECKEDBY DATE JOB NUMBER FIGURE 26228-11-5486
Source: Mecklenburg County Aerial Photography, dated 2009.
!U
!U
!U
!U
!U
!U !U
!U !U
!U
!U
!U
!U
!U
!U
!U
!U
!U
!U
!U
!U
!U
!U!U
!U
!U
!U
!U !U
!U
!U!U
!P
!P
!P!A
!A!@
!P
!P
"S
")
!@
!P
!@
"S
!@ !@
!P
!P
"S
!P
Property Boundary Line
35' from centerline ofrail alignment is anticipatedto be deeded to CATS.
Approximate locationof subgrade ramp and parking area
E Palmer St
S o u t h B v
Arlin
gton
A
v
S C o l l e g e S t
Lexin
gton
Av
E Carson Bv
SB-3
SB-16
SB-6
SB-5
SB-4
SB-1 SB-2 SB-8 SB-10
SB-9
SB-7
SB-12
SB-14
SB-13
SB-15
SB-11
SB-17
SB-18
SB-22
SB-21
SB-20
SB-19
SB-23SB-30
SB-24
SB-28
SB-26
SB-27 SB-29
SB-32
SB-31SB-25
SB-13
SB-8
SB-9
TMW-7
TMW-5GTW-1
SB-10 SB-4
ST-2/SUMP 3
DRAINAGE WELL
GTW-5
SM-3/TMW-3
GTW-2
ST-1/SUMP1
GTW-3 GTW-4
SB-2/TMW-2SB-1
SUMP2
SB-6/TMW-6
SITE LAYOUT AND SAMPLE LOCATION PLAN1200 SOUTH BOULEVARDCHARLOTTE, NORTH CAROLINAp
0 60 12030Feet
!U Sample Locations
!U COMP 1/2 !U COMP 3/4
!U COMP 5/6 ")Drainage Well
!@ Groundwater Extraction Well
"S Sediment Vault/Trap
2008 Sample Locations
!P Soil Boring and/or Temporary Groundwater Sampling Point
!A Temporary Groundwater Sampling Point
SJM AMC3/23/12 3/23/12
APPENDIX A
PLANNED CUT AND FILL
Job: AGTEK BLOCK GARAGE LOWER
Units: Ft-CYThu Mar 29, 2012 16:07:00 Page 1

Volume Report Subgrade vs. Stripped

Area Volume Comp/Ratio Compact Export Change Total Cut Fill OnGrade Cut Fill Cut Fill Cut Fill -Import Per .1 Ft
BUILDING 76,336 14,267 59,318 2,751 1,516 8,153 1.00 1.15 1,516 9,376 -7,860 325
GARAGE 17,043 17,042 1 0 1,923 0 1.00 1.15 1,923 0 1,923 73

RAMP 5,748 958 4,709 81 46 191 1.00 1.15 46 220 -174 24
Regions Total 99,127 32,267 64,028 2,832 3,485 8,344 3,485 9,596 -6,111 422
Unspecified 41,782 873 39,821 1,088 60 2,310 1.00 1.15 60 2,656 -2,596 178

Job Total 140,909 33,140 103,849 3,920 3,545 10,654 3,545 12,252 -8,707 600

Plane Slope
Stripping Qtys Area Area Depth Volume
STRIPPINGS 140,909 141,836 0.500 2,627

Plane Slope
Sectional Qtys Area Area Depth Volume
BUILDING 76,336 76,337 1.000 2,827

GARAGE 17,043 17,044 10.000 6,313

RAMP 5,748 5,748 5.000 1,064

Sectional Total 99,127 99,129 10,204
0 48.9 97.8
1200 SOUTH AGTEK GARAGE RAMP 03-29-12
APPENDIX B
2007 AND 2008 ENVIRONMENTAL RESULTS
APPENDIX C
2011 LABORATORY ANALYTICAL REPORTS
August 18, 2011
LIMS USE: FR - ANDREW FRANTZ
LIMS OBJECT ID: 9299254
9299254
Project:
Pace Project No.:
RE:
Mr. Andrew Frantz
AMEC-Charlotte
2801 Yorkmont Road
Suite 100
Charlotte, NC 28208
1200 SOUTH BOULEVARD
Dear Mr. Frantz:
Enclosed are the analytical results for sample(s) received by the laboratory on July 28, 2011. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards, where applicable, unless otherwise narrated in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001South Carolina Drinking Water Cert. #: 99006003Virginia Drinking Water Certification #: 00213
Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031West Virginia Certification #: 357Virginia/VELAP Certification #: 460144
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030North Carolina Bioassay Certification #: 9
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001Virginia Certification #: 00072West Virginia Certification #: 356
Virgina/VELAP Certification #: 460147
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE SUMMARY
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Lab ID Sample ID Matrix Date Collected Date Received
9299254001 SB-1 Solid 07/27/11 09:15 07/28/11 14:15
9299254002 SB-2 Solid 07/27/11 09:20 07/28/11 14:15
9299254003 SB-3 Solid 07/27/11 09:25 07/28/11 14:15
9299254004 SB-5 Solid 07/27/11 09:35 07/28/11 14:15
9299254013 SB-4 Solid 07/27/11 09:30 07/28/11 14:15
9299254014 SB-10 Solid 07/27/11 10:25 07/28/11 14:15
9299254015 SB-13 Solid 07/27/11 11:10 07/28/11 14:15
9299254016 SB-16 Solid 07/27/11 12:10 07/28/11 14:15
9299254017 SB-17 Solid 07/27/11 13:55 07/28/11 14:15
9299254018 SB-18 Solid 07/27/11 14:05 07/28/11 14:15
9299254019 SB-19 Solid 07/27/11 14:40 07/28/11 14:15
9299254020 SB-20 Solid 07/27/11 14:50 07/28/11 14:15
9299254021 SB-21 Solid 07/27/11 15:00 07/28/11 14:15
9299254022 SB-22 Solid 07/27/11 15:10 07/28/11 14:15
9299254023 COMP 1 Solid 07/27/11 09:40 07/28/11 14:15
9299254024 COMP 2 Solid 07/27/11 09:45 07/28/11 14:15
9299254025 COMP 3 Solid 07/27/11 10:30 07/28/11 14:15
9299254026 COMP 4 Solid 07/27/11 10:35 07/28/11 14:15
9299254027 COMP 5 Solid 07/27/11 11:35 07/28/11 14:15
9299254028 COMP 6 Solid 07/27/11 11:40 07/28/11 14:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
9299254001 SB-1 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CRRH
ASTM D2974-87 1 PASI-CKDF
9299254002 SB-2 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CRRH
ASTM D2974-87 1 PASI-CKDF
9299254003 SB-3 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CRRH
ASTM D2974-87 1 PASI-CKDF
9299254004 SB-5 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
ASTM D2974-87 1 PASI-CKDF
9299254013 SB-4 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CBPJ
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
9299254014 SB-10 EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
9299254015 SB-13 EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
9299254016 SB-16 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
9299254017 SB-17 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
9299254018 SB-18 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
9299254019 SB-19 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
9299254020 SB-20 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
9299254021 SB-21 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
9299254022 SB-22 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
9299254023 COMP 1 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
9299254024 COMP 2 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
9299254025 COMP 3 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
9299254026 COMP 4 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
9299254027 COMP 5 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
9299254028 COMP 6 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-1 Lab ID:9299254001 Collected:07/27/11 09:15 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 4.7 mg/kg 1 08/16/11 18:39 7440-36-008/15/11 12:400.57 0.32
Arsenic 52.2 mg/kg 1 08/16/11 18:39 7440-38-208/15/11 12:400.57 0.37
Beryllium 0.34 mg/kg 1 08/16/11 18:39 7440-41-708/15/11 12:400.11 0.023
Cadmium 2.3 mg/kg 1 08/16/11 18:39 7440-43-908/15/11 12:400.11 0.069
Chromium 25.2 mg/kg 1 08/16/11 18:39 7440-47-308/15/11 12:400.57 0.034
Copper 69.1 mg/kg 1 08/16/11 18:39 7440-50-808/15/11 12:400.57 0.046
Lead 334 mg/kg 1 08/16/11 18:39 7439-92-108/15/11 12:400.57 0.55
Manganese 300 mg/kg 1 08/16/11 18:39 7439-96-508/15/11 12:400.57 0.034
Nickel 11.4 mg/kg 1 08/16/11 18:39 7440-02-008/15/11 12:400.57 0.21
Selenium 1.3 mg/kg 1 08/16/11 18:39 7782-49-208/15/11 12:401.1 0.44
Silver 0.43J mg/kg 1 08/16/11 18:39 7440-22-408/15/11 12:400.57 0.034
Thallium 0.52J mg/kg 1 08/16/11 18:39 7440-28-008/15/11 12:401.1 0.30
Zinc 614 mg/kg 1 08/16/11 18:39 7440-66-608/15/11 12:401.1 0.30
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.94 mg/kg 20 08/12/11 14:14 7439-97-608/10/11 18:000.10 0.0021
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 08/14/11 12:57 83-32-908/10/11 11:5037987.2
Acenaphthylene 136J ug/kg 1 08/14/11 12:57 208-96-808/10/11 11:5037989.5
Aniline ND ug/kg 1 08/14/11 12:57 62-53-308/10/11 11:50379102
Anthracene 258J ug/kg 1 08/14/11 12:57 120-12-708/10/11 11:5037984.9
Benzo(a)anthracene 592 ug/kg 1 08/14/11 12:57 56-55-308/10/11 11:5037970.0
Benzo(a)pyrene 671 ug/kg 1 08/14/11 12:57 50-32-808/10/11 11:5037972.3
Benzo(b)fluoranthene 734 ug/kg 1 08/14/11 12:57 205-99-208/10/11 11:5037965.4
Benzo(g,h,i)perylene 470 ug/kg 1 08/14/11 12:57 191-24-208/10/11 11:5037996.4
Benzo(k)fluoranthene 522 ug/kg 1 08/14/11 12:57 207-08-908/10/11 11:5037974.6
Benzoic Acid ND ug/kg 1 08/14/11 12:57 65-85-008/10/11 11:50189068.8
Benzyl alcohol ND ug/kg 1 08/14/11 12:57 100-51-608/10/11 11:5075775.7
4-Bromophenylphenyl ether ND ug/kg 1 08/14/11 12:57 101-55-308/10/11 11:5037968.8
Butylbenzylphthalate ND ug/kg 1 08/14/11 12:57 85-68-708/10/11 11:5037980.3
4-Chloro-3-methylphenol ND ug/kg 1 08/14/11 12:57 59-50-708/10/11 11:5075778.0
4-Chloroaniline ND ug/kg 1 08/14/11 12:57 106-47-808/10/11 11:501890106
bis(2-Chloroethoxy)methane ND ug/kg 1 08/14/11 12:57 111-91-108/10/11 11:5037988.3
bis(2-Chloroethyl) ether ND ug/kg 1 08/14/11 12:57 111-44-408/10/11 11:5037996.4
bis(2-Chloroisopropyl) ether ND ug/kg 1 08/14/11 12:57 108-60-108/10/11 11:50379101
2-Chloronaphthalene ND ug/kg 1 08/14/11 12:57 91-58-708/10/11 11:5037974.6
2-Chlorophenol ND ug/kg 1 08/14/11 12:57 95-57-808/10/11 11:50379103
4-Chlorophenylphenyl ether ND ug/kg 1 08/14/11 12:57 7005-72-308/10/11 11:5037978.0
Chrysene 740 ug/kg 1 08/14/11 12:57 218-01-908/10/11 11:5037950.5
Dibenz(a,h)anthracene 192J ug/kg 1 08/14/11 12:57 53-70-308/10/11 11:5037980.3
Dibenzofuran 110J ug/kg 1 08/14/11 12:57 132-64-908/10/11 11:5037962.0
1,2-Dichlorobenzene ND ug/kg 1 08/14/11 12:57 95-50-108/10/11 11:50379101
1,3-Dichlorobenzene ND ug/kg 1 08/14/11 12:57 541-73-108/10/11 11:5037986.0
1,4-Dichlorobenzene ND ug/kg 1 08/14/11 12:57 106-46-708/10/11 11:50379107
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 7 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-1 Lab ID:9299254001 Collected:07/27/11 09:15 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3,3'-Dichlorobenzidine ND ug/kg 1 08/14/11 12:57 91-94-108/10/11 11:50189082.6
2,4-Dichlorophenol ND ug/kg 1 08/14/11 12:57 120-83-208/10/11 11:5037982.6
Diethylphthalate ND ug/kg 1 08/14/11 12:57 84-66-208/10/11 11:5037958.5
2,4-Dimethylphenol ND ug/kg 1 08/14/11 12:57 105-67-908/10/11 11:50379149
Dimethylphthalate ND ug/kg 1 08/14/11 12:57 131-11-308/10/11 11:5037976.9
Di-n-butylphthalate ND ug/kg 1 08/14/11 12:57 84-74-208/10/11 11:5037962.0
4,6-Dinitro-2-methylphenol ND ug/kg 1 08/14/11 12:57 534-52-108/10/11 11:5075775.7
2,4-Dinitrophenol ND ug/kg 1 08/14/11 12:57 51-28-508/10/11 11:50189062.0
2,4-Dinitrotoluene ND ug/kg 1 08/14/11 12:57 121-14-208/10/11 11:5037971.1
2,6-Dinitrotoluene ND ug/kg 1 08/14/11 12:57 606-20-208/10/11 11:5037979.2
Di-n-octylphthalate ND ug/kg 1 08/14/11 12:57 117-84-008/10/11 11:5037979.2
bis(2-Ethylhexyl)phthalate ND ug/kg 1 08/14/11 12:57 117-81-708/10/11 11:50379103
Fluoranthene 1250 ug/kg 1 08/14/11 12:57 206-44-008/10/11 11:5037955.1
Fluorene ND ug/kg 1 08/14/11 12:57 86-73-708/10/11 11:5037978.0
Hexachloro-1,3-butadiene ND ug/kg 1 08/14/11 12:57 87-68-308/10/11 11:5037965.4
Hexachlorobenzene ND ug/kg 1 08/14/11 12:57 118-74-108/10/11 11:5037948.2
Hexachlorocyclopentadiene ND ug/kg 1 08/14/11 12:57 77-47-408/10/11 11:5037970.0
Hexachloroethane ND ug/kg 1 08/14/11 12:57 67-72-108/10/11 11:5037999.8
Indeno(1,2,3-cd)pyrene 407 ug/kg 1 08/14/11 12:57 193-39-508/10/11 11:5037978.0
Isophorone ND ug/kg 1 08/14/11 12:57 78-59-108/10/11 11:5037984.9
1-Methylnaphthalene 249J ug/kg 1 08/14/11 12:57 90-12-008/10/11 11:5037998.7
2-Methylnaphthalene 325J ug/kg 1 08/14/11 12:57 91-57-608/10/11 11:5037981.5
2-Methylphenol(o-Cresol)ND ug/kg 1 08/14/11 12:57 95-48-708/10/11 11:50379115
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 08/14/11 12:5708/10/11 11:50379149
Naphthalene 228J ug/kg 1 08/14/11 12:57 91-20-308/10/11 11:5037992.9
2-Nitroaniline ND ug/kg 1 08/14/11 12:57 88-74-408/10/11 11:501890117
3-Nitroaniline ND ug/kg 1 08/14/11 12:57 99-09-208/10/11 11:501890103
4-Nitroaniline ND ug/kg 1 08/14/11 12:57 100-01-608/10/11 11:50757107
Nitrobenzene ND ug/kg 1 08/14/11 12:57 98-95-308/10/11 11:50379103
2-Nitrophenol ND ug/kg 1 08/14/11 12:57 88-75-508/10/11 11:5037991.8
4-Nitrophenol ND ug/kg 1 08/14/11 12:57 100-02-708/10/11 11:50189067.7
N-Nitrosodimethylamine ND ug/kg 1 08/14/11 12:57 62-75-908/10/11 11:50379123
N-Nitroso-di-n-propylamine ND ug/kg 1 08/14/11 12:57 621-64-708/10/11 11:5037972.3
N-Nitrosodiphenylamine ND ug/kg 1 08/14/11 12:57 86-30-608/10/11 11:50379112
Pentachlorophenol ND ug/kg 1 08/14/11 12:57 87-86-508/10/11 11:50189068.8
Phenanthrene 935 ug/kg 1 08/14/11 12:57 85-01-808/10/11 11:5037963.1
Phenol ND ug/kg 1 08/14/11 12:57 108-95-208/10/11 11:50379114
Pyrene 987 ug/kg 1 08/14/11 12:57 129-00-008/10/11 11:5037964.2
1,2,4-Trichlorobenzene ND ug/kg 1 08/14/11 12:57 120-82-108/10/11 11:5037973.4
2,4,5-Trichlorophenol ND ug/kg 1 08/14/11 12:57 95-95-408/10/11 11:50379117
2,4,6-Trichlorophenol ND ug/kg 1 08/14/11 12:57 88-06-208/10/11 11:5037983.8
Nitrobenzene-d5 (S)39 %1 08/14/11 12:57 4165-60-008/10/11 11:5023-110
2-Fluorobiphenyl (S)45 %1 08/14/11 12:57 321-60-808/10/11 11:5030-110
Terphenyl-d14 (S)43 %1 08/14/11 12:57 1718-51-008/10/11 11:5028-110
Phenol-d6 (S)39 %1 08/14/11 12:57 13127-88-308/10/11 11:5022-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 8 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-1 Lab ID:9299254001 Collected:07/27/11 09:15 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Fluorophenol (S)34 %1 08/14/11 12:57 367-12-408/10/11 11:5013-110
2,4,6-Tribromophenol (S)38 %1 08/14/11 12:57 118-79-608/10/11 11:5027-110
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 12.8 %1 07/29/11 14:460.10 0.10
Sample:SB-2 Lab ID:9299254002 Collected:07/27/11 09:20 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 2.3 mg/kg 1 08/16/11 18:47 7440-36-008/15/11 12:400.56 0.31
Arsenic 30.8 mg/kg 1 08/16/11 18:47 7440-38-208/15/11 12:400.56 0.36
Beryllium 0.30 mg/kg 1 08/16/11 18:47 7440-41-708/15/11 12:400.11 0.022
Cadmium 1.4 mg/kg 1 08/16/11 18:47 7440-43-908/15/11 12:400.11 0.067
Chromium 19.2 mg/kg 1 08/16/11 18:47 7440-47-308/15/11 12:400.56 0.034
Copper 47.0 mg/kg 1 08/16/11 18:47 7440-50-808/15/11 12:400.56 0.045
Lead 201 mg/kg 1 08/16/11 18:47 7439-92-108/15/11 12:400.56 0.54
Manganese 283 mg/kg 1 08/16/11 18:47 7439-96-508/15/11 12:400.56 0.034
Nickel 9.1 mg/kg 1 08/16/11 18:47 7440-02-008/15/11 12:400.56 0.20
Selenium 1.2 mg/kg 1 08/16/11 18:47 7782-49-208/15/11 12:401.1 0.43
Silver 0.42J mg/kg 1 08/16/11 18:47 7440-22-408/15/11 12:400.56 0.034
Thallium ND mg/kg 1 08/16/11 18:47 7440-28-008/15/11 12:401.1 0.29
Zinc 298 mg/kg 1 08/16/11 18:47 7440-66-608/15/11 12:401.1 0.29
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 2.1 mg/kg 50 08/12/11 14:19 7439-97-608/10/11 18:000.28 0.0056
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 10 08/14/11 13:25 83-32-908/10/11 11:50189004360
Acenaphthylene ND ug/kg 10 08/14/11 13:25 208-96-808/10/11 11:50189004470
Aniline ND ug/kg 10 08/14/11 13:25 62-53-308/10/11 11:50189005110
Anthracene ND ug/kg 10 08/14/11 13:25 120-12-708/10/11 11:50189004240
Benzo(a)anthracene ND ug/kg 10 08/14/11 13:25 56-55-308/10/11 11:50189003500
Benzo(a)pyrene ND ug/kg 10 08/14/11 13:25 50-32-808/10/11 11:50189003610
Benzo(b)fluoranthene ND ug/kg 10 08/14/11 13:25 205-99-208/10/11 11:50189003270
Benzo(g,h,i)perylene ND ug/kg 10 08/14/11 13:25 191-24-208/10/11 11:50189004820
Benzo(k)fluoranthene ND ug/kg 10 08/14/11 13:25 207-08-908/10/11 11:50189003730
Benzoic Acid ND ug/kg 10 08/14/11 13:25 65-85-008/10/11 11:50946003440
Benzyl alcohol ND ug/kg 10 08/14/11 13:25 100-51-608/10/11 11:50379003790
4-Bromophenylphenyl ether ND ug/kg 10 08/14/11 13:25 101-55-308/10/11 11:50189003440
Butylbenzylphthalate ND ug/kg 10 08/14/11 13:25 85-68-708/10/11 11:50189004020
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 9 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-2 Lab ID:9299254002 Collected:07/27/11 09:20 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
4-Chloro-3-methylphenol ND ug/kg 10 08/14/11 13:25 59-50-708/10/11 11:50379003900
4-Chloroaniline ND ug/kg 10 08/14/11 13:25 106-47-808/10/11 11:50946005280
bis(2-Chloroethoxy)methane ND ug/kg 10 08/14/11 13:25 111-91-108/10/11 11:50189004420
bis(2-Chloroethyl) ether ND ug/kg 10 08/14/11 13:25 111-44-408/10/11 11:50189004820
bis(2-Chloroisopropyl) ether ND ug/kg 10 08/14/11 13:25 108-60-108/10/11 11:50189005050
2-Chloronaphthalene ND ug/kg 10 08/14/11 13:25 91-58-708/10/11 11:50189003730
2-Chlorophenol ND ug/kg 10 08/14/11 13:25 95-57-808/10/11 11:50189005160
4-Chlorophenylphenyl ether ND ug/kg 10 08/14/11 13:25 7005-72-308/10/11 11:50189003900
Chrysene ND ug/kg 10 08/14/11 13:25 218-01-908/10/11 11:50189002520
Dibenz(a,h)anthracene ND ug/kg 10 08/14/11 13:25 53-70-308/10/11 11:50189004020
Dibenzofuran ND ug/kg 10 08/14/11 13:25 132-64-908/10/11 11:50189003100
1,2-Dichlorobenzene ND ug/kg 10 08/14/11 13:25 95-50-108/10/11 11:50189005050
1,3-Dichlorobenzene ND ug/kg 10 08/14/11 13:25 541-73-108/10/11 11:50189004300
1,4-Dichlorobenzene ND ug/kg 10 08/14/11 13:25 106-46-708/10/11 11:50189005330
3,3'-Dichlorobenzidine ND ug/kg 10 08/14/11 13:25 91-94-108/10/11 11:50946004130
2,4-Dichlorophenol ND ug/kg 10 08/14/11 13:25 120-83-208/10/11 11:50189004130
Diethylphthalate ND ug/kg 10 08/14/11 13:25 84-66-208/10/11 11:50189002930
2,4-Dimethylphenol ND ug/kg 10 08/14/11 13:25 105-67-908/10/11 11:50189007460
Dimethylphthalate ND ug/kg 10 08/14/11 13:25 131-11-308/10/11 11:50189003840
Di-n-butylphthalate ND ug/kg 10 08/14/11 13:25 84-74-208/10/11 11:50189003100
4,6-Dinitro-2-methylphenol ND ug/kg 10 08/14/11 13:25 534-52-108/10/11 11:50379003790
2,4-Dinitrophenol ND ug/kg 10 08/14/11 13:25 51-28-508/10/11 11:50946003100
2,4-Dinitrotoluene ND ug/kg 10 08/14/11 13:25 121-14-208/10/11 11:50189003560
2,6-Dinitrotoluene ND ug/kg 10 08/14/11 13:25 606-20-208/10/11 11:50189003960
Di-n-octylphthalate ND ug/kg 10 08/14/11 13:25 117-84-008/10/11 11:50189003960
bis(2-Ethylhexyl)phthalate ND ug/kg 10 08/14/11 13:25 117-81-708/10/11 11:50189005160
Fluoranthene ND ug/kg 10 08/14/11 13:25 206-44-008/10/11 11:50189002750
Fluorene ND ug/kg 10 08/14/11 13:25 86-73-708/10/11 11:50189003900
Hexachloro-1,3-butadiene ND ug/kg 10 08/14/11 13:25 87-68-308/10/11 11:50189003270
Hexachlorobenzene ND ug/kg 10 08/14/11 13:25 118-74-108/10/11 11:50189002410
Hexachlorocyclopentadiene ND ug/kg 10 08/14/11 13:25 77-47-408/10/11 11:50189003500
Hexachloroethane ND ug/kg 10 08/14/11 13:25 67-72-108/10/11 11:50189004990
Indeno(1,2,3-cd)pyrene ND ug/kg 10 08/14/11 13:25 193-39-508/10/11 11:50189003900
Isophorone ND ug/kg 10 08/14/11 13:25 78-59-108/10/11 11:50189004240
1-Methylnaphthalene ND ug/kg 10 08/14/11 13:25 90-12-008/10/11 11:50189004930
2-Methylnaphthalene ND ug/kg 10 08/14/11 13:25 91-57-608/10/11 11:50189004070
2-Methylphenol(o-Cresol)ND ug/kg 10 08/14/11 13:25 95-48-708/10/11 11:50189005740
3&4-Methylphenol(m&p Cresol)ND ug/kg 10 08/14/11 13:2508/10/11 11:50189007460
Naphthalene ND ug/kg 10 08/14/11 13:25 91-20-308/10/11 11:50189004650
2-Nitroaniline ND ug/kg 10 08/14/11 13:25 88-74-408/10/11 11:50946005850
3-Nitroaniline ND ug/kg 10 08/14/11 13:25 99-09-208/10/11 11:50946005160
4-Nitroaniline ND ug/kg 10 08/14/11 13:25 100-01-608/10/11 11:50379005330
Nitrobenzene ND ug/kg 10 08/14/11 13:25 98-95-308/10/11 11:50189005160
2-Nitrophenol ND ug/kg 10 08/14/11 13:25 88-75-508/10/11 11:50189004590
4-Nitrophenol ND ug/kg 10 08/14/11 13:25 100-02-708/10/11 11:50946003380
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 10 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-2 Lab ID:9299254002 Collected:07/27/11 09:20 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
N-Nitrosodimethylamine ND ug/kg 10 08/14/11 13:25 62-75-908/10/11 11:50189006140
N-Nitroso-di-n-propylamine ND ug/kg 10 08/14/11 13:25 621-64-708/10/11 11:50189003610
N-Nitrosodiphenylamine ND ug/kg 10 08/14/11 13:25 86-30-608/10/11 11:50189005620
Pentachlorophenol ND ug/kg 10 08/14/11 13:25 87-86-508/10/11 11:50946003440
Phenanthrene ND ug/kg 10 08/14/11 13:25 85-01-808/10/11 11:50189003150
Phenol ND ug/kg 10 08/14/11 13:25 108-95-2 D3,P308/10/11 11:50189005680
Pyrene ND ug/kg 10 08/14/11 13:25 129-00-008/10/11 11:50189003210
1,2,4-Trichlorobenzene ND ug/kg 10 08/14/11 13:25 120-82-108/10/11 11:50189003670
2,4,5-Trichlorophenol ND ug/kg 10 08/14/11 13:25 95-95-408/10/11 11:50189005850
2,4,6-Trichlorophenol ND ug/kg 10 08/14/11 13:25 88-06-208/10/11 11:50189004190
Nitrobenzene-d5 (S)0 %10 08/14/11 13:25 4165-60-0 S408/10/11 11:5023-110
2-Fluorobiphenyl (S)0 %10 08/14/11 13:25 321-60-808/10/11 11:5030-110
Terphenyl-d14 (S)0 %10 08/14/11 13:25 1718-51-008/10/11 11:5028-110
Phenol-d6 (S)0 %10 08/14/11 13:25 13127-88-308/10/11 11:5022-110
2-Fluorophenol (S)0 %10 08/14/11 13:25 367-12-408/10/11 11:5013-110
2,4,6-Tribromophenol (S)0 %10 08/14/11 13:25 118-79-608/10/11 11:5027-110
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 12.8 %1 07/29/11 14:460.10 0.10
Sample:SB-3 Lab ID:9299254003 Collected:07/27/11 09:25 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 11.8 mg/kg 1 08/16/11 18:56 7440-36-008/15/11 12:400.55 0.31
Arsenic 19.6 mg/kg 1 08/16/11 18:56 7440-38-208/15/11 12:400.55 0.35
Beryllium 0.22 mg/kg 1 08/16/11 18:56 7440-41-708/15/11 12:400.11 0.022
Cadmium 58.5 mg/kg 1 08/16/11 18:56 7440-43-908/15/11 12:400.11 0.066
Chromium 20.6 mg/kg 1 08/16/11 18:56 7440-47-308/15/11 12:400.55 0.033
Copper 376 mg/kg 1 08/16/11 18:56 7440-50-808/15/11 12:400.55 0.044
Lead 591 mg/kg 1 08/16/11 18:56 7439-92-108/15/11 12:400.55 0.53
Manganese 301 mg/kg 1 08/16/11 18:56 7439-96-508/15/11 12:400.55 0.033
Nickel 11.8 mg/kg 1 08/16/11 18:56 7440-02-008/15/11 12:400.55 0.20
Selenium 4.4 mg/kg 1 08/16/11 18:56 7782-49-208/15/11 12:401.1 0.42
Silver 1.3 mg/kg 1 08/16/11 18:56 7440-22-408/15/11 12:400.55 0.033
Thallium 0.40J mg/kg 1 08/16/11 18:56 7440-28-008/15/11 12:401.1 0.29
Zinc 7430 mg/kg 10 08/17/11 12:58 7440-66-608/15/11 12:4011.0 2.9
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 1.5 mg/kg 50 08/12/11 14:24 7439-97-608/10/11 18:000.20 0.0041
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 11 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-3 Lab ID:9299254003 Collected:07/27/11 09:25 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 10 08/14/11 13:52 83-32-908/10/11 11:50189004350
Acenaphthylene ND ug/kg 10 08/14/11 13:52 208-96-808/10/11 11:50189004470
Aniline ND ug/kg 10 08/14/11 13:52 62-53-308/10/11 11:50189005100
Anthracene ND ug/kg 10 08/14/11 13:52 120-12-708/10/11 11:50189004240
Benzo(a)anthracene ND ug/kg 10 08/14/11 13:52 56-55-308/10/11 11:50189003490
Benzo(a)pyrene ND ug/kg 10 08/14/11 13:52 50-32-808/10/11 11:50189003610
Benzo(b)fluoranthene ND ug/kg 10 08/14/11 13:52 205-99-208/10/11 11:50189003260
Benzo(g,h,i)perylene ND ug/kg 10 08/14/11 13:52 191-24-208/10/11 11:50189004810
Benzo(k)fluoranthene ND ug/kg 10 08/14/11 13:52 207-08-908/10/11 11:50189003720
Benzoic Acid ND ug/kg 10 08/14/11 13:52 65-85-008/10/11 11:50945003440
Benzyl alcohol ND ug/kg 10 08/14/11 13:52 100-51-608/10/11 11:50378003780
4-Bromophenylphenyl ether ND ug/kg 10 08/14/11 13:52 101-55-308/10/11 11:50189003440
Butylbenzylphthalate ND ug/kg 10 08/14/11 13:52 85-68-708/10/11 11:50189004010
4-Chloro-3-methylphenol ND ug/kg 10 08/14/11 13:52 59-50-708/10/11 11:50378003890
4-Chloroaniline ND ug/kg 10 08/14/11 13:52 106-47-808/10/11 11:50945005270
bis(2-Chloroethoxy)methane ND ug/kg 10 08/14/11 13:52 111-91-108/10/11 11:50189004410
bis(2-Chloroethyl) ether ND ug/kg 10 08/14/11 13:52 111-44-408/10/11 11:50189004810
bis(2-Chloroisopropyl) ether ND ug/kg 10 08/14/11 13:52 108-60-108/10/11 11:50189005040
2-Chloronaphthalene ND ug/kg 10 08/14/11 13:52 91-58-708/10/11 11:50189003720
2-Chlorophenol ND ug/kg 10 08/14/11 13:52 95-57-808/10/11 11:50189005150
4-Chlorophenylphenyl ether ND ug/kg 10 08/14/11 13:52 7005-72-308/10/11 11:50189003890
Chrysene ND ug/kg 10 08/14/11 13:52 218-01-908/10/11 11:50189002520
Dibenz(a,h)anthracene ND ug/kg 10 08/14/11 13:52 53-70-308/10/11 11:50189004010
Dibenzofuran ND ug/kg 10 08/14/11 13:52 132-64-908/10/11 11:50189003090
1,2-Dichlorobenzene ND ug/kg 10 08/14/11 13:52 95-50-108/10/11 11:50189005040
1,3-Dichlorobenzene ND ug/kg 10 08/14/11 13:52 541-73-108/10/11 11:50189004290
1,4-Dichlorobenzene ND ug/kg 10 08/14/11 13:52 106-46-708/10/11 11:50189005320
3,3'-Dichlorobenzidine ND ug/kg 10 08/14/11 13:52 91-94-108/10/11 11:50945004120
2,4-Dichlorophenol ND ug/kg 10 08/14/11 13:52 120-83-208/10/11 11:50189004120
Diethylphthalate ND ug/kg 10 08/14/11 13:52 84-66-208/10/11 11:50189002920
2,4-Dimethylphenol ND ug/kg 10 08/14/11 13:52 105-67-908/10/11 11:50189007440
Dimethylphthalate ND ug/kg 10 08/14/11 13:52 131-11-308/10/11 11:50189003840
Di-n-butylphthalate ND ug/kg 10 08/14/11 13:52 84-74-208/10/11 11:50189003090
4,6-Dinitro-2-methylphenol ND ug/kg 10 08/14/11 13:52 534-52-108/10/11 11:50378003780
2,4-Dinitrophenol ND ug/kg 10 08/14/11 13:52 51-28-508/10/11 11:50945003090
2,4-Dinitrotoluene ND ug/kg 10 08/14/11 13:52 121-14-208/10/11 11:50189003550
2,6-Dinitrotoluene ND ug/kg 10 08/14/11 13:52 606-20-208/10/11 11:50189003950
Di-n-octylphthalate ND ug/kg 10 08/14/11 13:52 117-84-008/10/11 11:50189003950
bis(2-Ethylhexyl)phthalate ND ug/kg 10 08/14/11 13:52 117-81-708/10/11 11:50189005150
Fluoranthene ND ug/kg 10 08/14/11 13:52 206-44-008/10/11 11:50189002750
Fluorene ND ug/kg 10 08/14/11 13:52 86-73-708/10/11 11:50189003890
Hexachloro-1,3-butadiene ND ug/kg 10 08/14/11 13:52 87-68-308/10/11 11:50189003260
Hexachlorobenzene ND ug/kg 10 08/14/11 13:52 118-74-108/10/11 11:50189002400
Hexachlorocyclopentadiene ND ug/kg 10 08/14/11 13:52 77-47-408/10/11 11:50189003490
Hexachloroethane ND ug/kg 10 08/14/11 13:52 67-72-108/10/11 11:50189004980
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 12 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-3 Lab ID:9299254003 Collected:07/27/11 09:25 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Indeno(1,2,3-cd)pyrene ND ug/kg 10 08/14/11 13:52 193-39-508/10/11 11:50189003890
Isophorone ND ug/kg 10 08/14/11 13:52 78-59-108/10/11 11:50189004240
1-Methylnaphthalene ND ug/kg 10 08/14/11 13:52 90-12-008/10/11 11:50189004920
2-Methylnaphthalene ND ug/kg 10 08/14/11 13:52 91-57-608/10/11 11:50189004060
2-Methylphenol(o-Cresol)ND ug/kg 10 08/14/11 13:52 95-48-708/10/11 11:50189005730
3&4-Methylphenol(m&p Cresol)ND ug/kg 10 08/14/11 13:5208/10/11 11:50189007440
Naphthalene ND ug/kg 10 08/14/11 13:52 91-20-308/10/11 11:50189004640
2-Nitroaniline ND ug/kg 10 08/14/11 13:52 88-74-408/10/11 11:50945005840
3-Nitroaniline ND ug/kg 10 08/14/11 13:52 99-09-208/10/11 11:50945005150
4-Nitroaniline ND ug/kg 10 08/14/11 13:52 100-01-608/10/11 11:50378005320
Nitrobenzene ND ug/kg 10 08/14/11 13:52 98-95-308/10/11 11:50189005150
2-Nitrophenol ND ug/kg 10 08/14/11 13:52 88-75-508/10/11 11:50189004580
4-Nitrophenol ND ug/kg 10 08/14/11 13:52 100-02-708/10/11 11:50945003380
N-Nitrosodimethylamine ND ug/kg 10 08/14/11 13:52 62-75-908/10/11 11:50189006130
N-Nitroso-di-n-propylamine ND ug/kg 10 08/14/11 13:52 621-64-708/10/11 11:50189003610
N-Nitrosodiphenylamine ND ug/kg 10 08/14/11 13:52 86-30-608/10/11 11:50189005610
Pentachlorophenol ND ug/kg 10 08/14/11 13:52 87-86-508/10/11 11:50945003440
Phenanthrene ND ug/kg 10 08/14/11 13:52 85-01-808/10/11 11:50189003150
Phenol ND ug/kg 10 08/14/11 13:52 108-95-2 D3,P308/10/11 11:50189005670
Pyrene ND ug/kg 10 08/14/11 13:52 129-00-008/10/11 11:50189003210
1,2,4-Trichlorobenzene ND ug/kg 10 08/14/11 13:52 120-82-108/10/11 11:50189003660
2,4,5-Trichlorophenol ND ug/kg 10 08/14/11 13:52 95-95-408/10/11 11:50189005840
2,4,6-Trichlorophenol ND ug/kg 10 08/14/11 13:52 88-06-208/10/11 11:50189004180
Nitrobenzene-d5 (S)0 %10 08/14/11 13:52 4165-60-0 S408/10/11 11:5023-110
2-Fluorobiphenyl (S)0 %10 08/14/11 13:52 321-60-808/10/11 11:5030-110
Terphenyl-d14 (S)0 %10 08/14/11 13:52 1718-51-008/10/11 11:5028-110
Phenol-d6 (S)0 %10 08/14/11 13:52 13127-88-308/10/11 11:5022-110
2-Fluorophenol (S)0 %10 08/14/11 13:52 367-12-408/10/11 11:5013-110
2,4,6-Tribromophenol (S)0 %10 08/14/11 13:52 118-79-608/10/11 11:5027-110
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 12.7 %1 07/29/11 14:470.10 0.10
Sample:SB-5 Lab ID:9299254004 Collected:07/27/11 09:35 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 3.1 mg/kg 1 08/16/11 19:00 7440-36-008/15/11 12:400.55 0.31
Arsenic 18.0 mg/kg 1 08/16/11 19:00 7440-38-208/15/11 12:400.55 0.35
Beryllium 0.31 mg/kg 1 08/16/11 19:00 7440-41-708/15/11 12:400.11 0.022
Cadmium 2.0 mg/kg 1 08/16/11 19:00 7440-43-908/15/11 12:400.11 0.066
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 13 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-5 Lab ID:9299254004 Collected:07/27/11 09:35 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Chromium 27.1 mg/kg 1 08/16/11 19:00 7440-47-308/15/11 12:400.55 0.033
Copper 56.7 mg/kg 1 08/16/11 19:00 7440-50-808/15/11 12:400.55 0.044
Lead 254 mg/kg 1 08/16/11 19:00 7439-92-108/15/11 12:400.55 0.53
Manganese 345 mg/kg 1 08/16/11 19:00 7439-96-508/15/11 12:400.55 0.033
Nickel 10.3 mg/kg 1 08/16/11 19:00 7440-02-008/15/11 12:400.55 0.20
Selenium 1.4 mg/kg 1 08/16/11 19:00 7782-49-208/15/11 12:401.1 0.42
Silver 0.46J mg/kg 1 08/16/11 19:00 7440-22-408/15/11 12:400.55 0.033
Thallium 0.31J mg/kg 1 08/16/11 19:00 7440-28-008/15/11 12:401.1 0.29
Zinc 320 mg/kg 1 08/16/11 19:00 7440-66-608/15/11 12:401.1 0.29
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.72 mg/kg 10 08/12/11 14:27 7439-97-608/10/11 18:000.050 0.00099
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 10 08/15/11 11:34 83-32-908/10/11 11:50186004270
Acenaphthylene ND ug/kg 10 08/15/11 11:34 208-96-808/10/11 11:50186004390
Aniline ND ug/kg 10 08/15/11 11:34 62-53-308/10/11 11:50186005010
Anthracene ND ug/kg 10 08/15/11 11:34 120-12-708/10/11 11:50186004160
Benzo(a)anthracene ND ug/kg 10 08/15/11 11:34 56-55-308/10/11 11:50186003430
Benzo(a)pyrene ND ug/kg 10 08/15/11 11:34 50-32-808/10/11 11:50186003540
Benzo(b)fluoranthene ND ug/kg 10 08/15/11 11:34 205-99-208/10/11 11:50186003210
Benzo(g,h,i)perylene ND ug/kg 10 08/15/11 11:34 191-24-208/10/11 11:50186004720
Benzo(k)fluoranthene ND ug/kg 10 08/15/11 11:34 207-08-908/10/11 11:50186003660
Benzoic Acid ND ug/kg 10 08/15/11 11:34 65-85-008/10/11 11:50928003370
Benzyl alcohol ND ug/kg 10 08/15/11 11:34 100-51-608/10/11 11:50371003710
4-Bromophenylphenyl ether ND ug/kg 10 08/15/11 11:34 101-55-308/10/11 11:50186003370
Butylbenzylphthalate ND ug/kg 10 08/15/11 11:34 85-68-708/10/11 11:50186003940
4-Chloro-3-methylphenol ND ug/kg 10 08/15/11 11:34 59-50-708/10/11 11:50371003820
4-Chloroaniline ND ug/kg 10 08/15/11 11:34 106-47-808/10/11 11:50928005170
bis(2-Chloroethoxy)methane ND ug/kg 10 08/15/11 11:34 111-91-108/10/11 11:50186004330
bis(2-Chloroethyl) ether ND ug/kg 10 08/15/11 11:34 111-44-408/10/11 11:50186004720
bis(2-Chloroisopropyl) ether ND ug/kg 10 08/15/11 11:34 108-60-108/10/11 11:50186004950
2-Chloronaphthalene ND ug/kg 10 08/15/11 11:34 91-58-708/10/11 11:50186003660
2-Chlorophenol ND ug/kg 10 08/15/11 11:34 95-57-808/10/11 11:50186005060
4-Chlorophenylphenyl ether ND ug/kg 10 08/15/11 11:34 7005-72-308/10/11 11:50186003820
Chrysene ND ug/kg 10 08/15/11 11:34 218-01-908/10/11 11:50186002470
Dibenz(a,h)anthracene ND ug/kg 10 08/15/11 11:34 53-70-308/10/11 11:50186003940
Dibenzofuran ND ug/kg 10 08/15/11 11:34 132-64-908/10/11 11:50186003040
1,2-Dichlorobenzene ND ug/kg 10 08/15/11 11:34 95-50-108/10/11 11:50186004950
1,3-Dichlorobenzene ND ug/kg 10 08/15/11 11:34 541-73-108/10/11 11:50186004220
1,4-Dichlorobenzene ND ug/kg 10 08/15/11 11:34 106-46-708/10/11 11:50186005230
3,3'-Dichlorobenzidine ND ug/kg 10 08/15/11 11:34 91-94-108/10/11 11:50928004050
2,4-Dichlorophenol ND ug/kg 10 08/15/11 11:34 120-83-208/10/11 11:50186004050
Diethylphthalate ND ug/kg 10 08/15/11 11:34 84-66-208/10/11 11:50186002870
2,4-Dimethylphenol ND ug/kg 10 08/15/11 11:34 105-67-908/10/11 11:50186007310
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 14 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-5 Lab ID:9299254004 Collected:07/27/11 09:35 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Dimethylphthalate ND ug/kg 10 08/15/11 11:34 131-11-308/10/11 11:50186003770
Di-n-butylphthalate ND ug/kg 10 08/15/11 11:34 84-74-208/10/11 11:50186003040
4,6-Dinitro-2-methylphenol ND ug/kg 10 08/15/11 11:34 534-52-108/10/11 11:50371003710
2,4-Dinitrophenol ND ug/kg 10 08/15/11 11:34 51-28-508/10/11 11:50928003040
2,4-Dinitrotoluene ND ug/kg 10 08/15/11 11:34 121-14-208/10/11 11:50186003490
2,6-Dinitrotoluene ND ug/kg 10 08/15/11 11:34 606-20-208/10/11 11:50186003880
Di-n-octylphthalate ND ug/kg 10 08/15/11 11:34 117-84-008/10/11 11:50186003880
bis(2-Ethylhexyl)phthalate ND ug/kg 10 08/15/11 11:34 117-81-708/10/11 11:50186005060
Fluoranthene ND ug/kg 10 08/15/11 11:34 206-44-008/10/11 11:50186002700
Fluorene ND ug/kg 10 08/15/11 11:34 86-73-708/10/11 11:50186003820
Hexachloro-1,3-butadiene ND ug/kg 10 08/15/11 11:34 87-68-308/10/11 11:50186003210
Hexachlorobenzene ND ug/kg 10 08/15/11 11:34 118-74-108/10/11 11:50186002360
Hexachlorocyclopentadiene ND ug/kg 10 08/15/11 11:34 77-47-408/10/11 11:50186003430
Hexachloroethane ND ug/kg 10 08/15/11 11:34 67-72-108/10/11 11:50186004890
Indeno(1,2,3-cd)pyrene ND ug/kg 10 08/15/11 11:34 193-39-508/10/11 11:50186003820
Isophorone ND ug/kg 10 08/15/11 11:34 78-59-108/10/11 11:50186004160
1-Methylnaphthalene ND ug/kg 10 08/15/11 11:34 90-12-008/10/11 11:50186004840
2-Methylnaphthalene ND ug/kg 10 08/15/11 11:34 91-57-608/10/11 11:50186003990
2-Methylphenol(o-Cresol)ND ug/kg 10 08/15/11 11:34 95-48-708/10/11 11:50186005620
3&4-Methylphenol(m&p Cresol)ND ug/kg 10 08/15/11 11:3408/10/11 11:50186007310
Naphthalene ND ug/kg 10 08/15/11 11:34 91-20-308/10/11 11:50186004560
2-Nitroaniline ND ug/kg 10 08/15/11 11:34 88-74-408/10/11 11:50928005740
3-Nitroaniline ND ug/kg 10 08/15/11 11:34 99-09-208/10/11 11:50928005060
4-Nitroaniline ND ug/kg 10 08/15/11 11:34 100-01-608/10/11 11:50371005230
Nitrobenzene ND ug/kg 10 08/15/11 11:34 98-95-308/10/11 11:50186005060
2-Nitrophenol ND ug/kg 10 08/15/11 11:34 88-75-508/10/11 11:50186004500
4-Nitrophenol ND ug/kg 10 08/15/11 11:34 100-02-708/10/11 11:50928003320
N-Nitrosodimethylamine ND ug/kg 10 08/15/11 11:34 62-75-908/10/11 11:50186006020
N-Nitroso-di-n-propylamine ND ug/kg 10 08/15/11 11:34 621-64-708/10/11 11:50186003540
N-Nitrosodiphenylamine ND ug/kg 10 08/15/11 11:34 86-30-608/10/11 11:50186005510
Pentachlorophenol ND ug/kg 10 08/15/11 11:34 87-86-508/10/11 11:50928003370
Phenanthrene ND ug/kg 10 08/15/11 11:34 85-01-808/10/11 11:50186003090
Phenol ND ug/kg 10 08/15/11 11:34 108-95-2 D3,P308/10/11 11:50186005570
Pyrene ND ug/kg 10 08/15/11 11:34 129-00-008/10/11 11:50186003150
1,2,4-Trichlorobenzene ND ug/kg 10 08/15/11 11:34 120-82-108/10/11 11:50186003600
2,4,5-Trichlorophenol ND ug/kg 10 08/15/11 11:34 95-95-408/10/11 11:50186005740
2,4,6-Trichlorophenol ND ug/kg 10 08/15/11 11:34 88-06-208/10/11 11:50186004110
Nitrobenzene-d5 (S)0 %10 08/15/11 11:34 4165-60-0 S408/10/11 11:5023-110
2-Fluorobiphenyl (S)0 %10 08/15/11 11:34 321-60-808/10/11 11:5030-110
Terphenyl-d14 (S)0 %10 08/15/11 11:34 1718-51-008/10/11 11:5028-110
Phenol-d6 (S)0 %10 08/15/11 11:34 13127-88-308/10/11 11:5022-110
2-Fluorophenol (S)0 %10 08/15/11 11:34 367-12-408/10/11 11:5013-110
2,4,6-Tribromophenol (S)0 %10 08/15/11 11:34 118-79-608/10/11 11:5027-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 15 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-5 Lab ID:9299254004 Collected:07/27/11 09:35 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 11.1 %1 07/29/11 14:490.10 0.10
Sample:SB-4 Lab ID:9299254013 Collected:07/27/11 09:30 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 0.75 mg/kg 1 08/16/11 19:04 7440-36-008/15/11 12:400.54 0.30
Arsenic 3.3 mg/kg 1 08/16/11 19:04 7440-38-208/15/11 12:400.54 0.34
Beryllium 0.40 mg/kg 1 08/16/11 19:04 7440-41-708/15/11 12:400.11 0.022
Cadmium 1.8 mg/kg 1 08/16/11 19:04 7440-43-908/15/11 12:400.11 0.065
Chromium 20.8 mg/kg 1 08/16/11 19:04 7440-47-308/15/11 12:400.54 0.032
Copper 41.2 mg/kg 1 08/16/11 19:04 7440-50-808/15/11 12:400.54 0.043
Lead 58.9 mg/kg 1 08/16/11 19:04 7439-92-108/15/11 12:400.54 0.52
Manganese 183 mg/kg 1 08/16/11 19:04 7439-96-508/15/11 12:400.54 0.032
Nickel 4.0 mg/kg 1 08/16/11 19:04 7440-02-008/15/11 12:400.54 0.19
Selenium 1.2 mg/kg 1 08/16/11 19:04 7782-49-208/15/11 12:401.1 0.41
Silver 0.25J mg/kg 1 08/16/11 19:04 7440-22-408/15/11 12:400.54 0.032
Thallium ND mg/kg 1 08/16/11 19:04 7440-28-008/15/11 12:401.1 0.28
Zinc 65.4 mg/kg 1 08/16/11 19:04 7440-66-608/15/11 12:401.1 0.28
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.93 mg/kg 20 08/12/11 14:30 7439-97-608/10/11 18:000.10 0.0020
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 10 08/14/11 19:46 83-32-908/10/11 14:24178004090
Acenaphthylene ND ug/kg 10 08/14/11 19:46 208-96-808/10/11 14:24178004200
Aniline ND ug/kg 10 08/14/11 19:46 62-53-308/10/11 14:24178004790
Anthracene ND ug/kg 10 08/14/11 19:46 120-12-708/10/11 14:24178003990
Benzo(a)anthracene 4570J ug/kg 10 08/14/11 19:46 56-55-308/10/11 14:24178003290
Benzo(a)pyrene 5920J ug/kg 10 08/14/11 19:46 50-32-808/10/11 14:24178003390
Benzo(b)fluoranthene 6020J ug/kg 10 08/14/11 19:46 205-99-208/10/11 14:24178003070
Benzo(g,h,i)perylene ND ug/kg 10 08/14/11 19:46 191-24-208/10/11 14:24178004520
Benzo(k)fluoranthene 6720J ug/kg 10 08/14/11 19:46 207-08-908/10/11 14:24178003500
Benzoic Acid ND ug/kg 10 08/14/11 19:46 65-85-008/10/11 14:24889003230
Benzyl alcohol ND ug/kg 10 08/14/11 19:46 100-51-608/10/11 14:24356003560
4-Bromophenylphenyl ether ND ug/kg 10 08/14/11 19:46 101-55-308/10/11 14:24178003230
Butylbenzylphthalate ND ug/kg 10 08/14/11 19:46 85-68-708/10/11 14:24178003770
4-Chloro-3-methylphenol ND ug/kg 10 08/14/11 19:46 59-50-708/10/11 14:24356003660
4-Chloroaniline ND ug/kg 10 08/14/11 19:46 106-47-808/10/11 14:24889004960
bis(2-Chloroethoxy)methane ND ug/kg 10 08/14/11 19:46 111-91-108/10/11 14:24178004150
bis(2-Chloroethyl) ether ND ug/kg 10 08/14/11 19:46 111-44-408/10/11 14:24178004520
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 16 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-4 Lab ID:9299254013 Collected:07/27/11 09:30 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
bis(2-Chloroisopropyl) ether ND ug/kg 10 08/14/11 19:46 108-60-108/10/11 14:24178004740
2-Chloronaphthalene ND ug/kg 10 08/14/11 19:46 91-58-708/10/11 14:24178003500
2-Chlorophenol ND ug/kg 10 08/14/11 19:46 95-57-808/10/11 14:24178004850
4-Chlorophenylphenyl ether ND ug/kg 10 08/14/11 19:46 7005-72-308/10/11 14:24178003660
Chrysene 7410J ug/kg 10 08/14/11 19:46 218-01-908/10/11 14:24178002370
Dibenz(a,h)anthracene ND ug/kg 10 08/14/11 19:46 53-70-308/10/11 14:24178003770
Dibenzofuran ND ug/kg 10 08/14/11 19:46 132-64-908/10/11 14:24178002910
1,2-Dichlorobenzene ND ug/kg 10 08/14/11 19:46 95-50-108/10/11 14:24178004740
1,3-Dichlorobenzene ND ug/kg 10 08/14/11 19:46 541-73-108/10/11 14:24178004040
1,4-Dichlorobenzene ND ug/kg 10 08/14/11 19:46 106-46-708/10/11 14:24178005010
3,3'-Dichlorobenzidine ND ug/kg 10 08/14/11 19:46 91-94-108/10/11 14:24889003880
2,4-Dichlorophenol ND ug/kg 10 08/14/11 19:46 120-83-208/10/11 14:24178003880
Diethylphthalate ND ug/kg 10 08/14/11 19:46 84-66-208/10/11 14:24178002750
2,4-Dimethylphenol ND ug/kg 10 08/14/11 19:46 105-67-908/10/11 14:24178007000
Dimethylphthalate ND ug/kg 10 08/14/11 19:46 131-11-308/10/11 14:24178003610
Di-n-butylphthalate ND ug/kg 10 08/14/11 19:46 84-74-208/10/11 14:24178002910
4,6-Dinitro-2-methylphenol ND ug/kg 10 08/14/11 19:46 534-52-108/10/11 14:24356003560
2,4-Dinitrophenol ND ug/kg 10 08/14/11 19:46 51-28-508/10/11 14:24889002910
2,4-Dinitrotoluene ND ug/kg 10 08/14/11 19:46 121-14-208/10/11 14:24178003340
2,6-Dinitrotoluene ND ug/kg 10 08/14/11 19:46 606-20-208/10/11 14:24178003720
Di-n-octylphthalate ND ug/kg 10 08/14/11 19:46 117-84-008/10/11 14:24178003720
bis(2-Ethylhexyl)phthalate ND ug/kg 10 08/14/11 19:46 117-81-708/10/11 14:24178004850
Fluoranthene 22800 ug/kg 10 08/14/11 19:46 206-44-008/10/11 14:24178002590
Fluorene ND ug/kg 10 08/14/11 19:46 86-73-708/10/11 14:24178003660
Hexachloro-1,3-butadiene ND ug/kg 10 08/14/11 19:46 87-68-308/10/11 14:24178003070
Hexachlorobenzene ND ug/kg 10 08/14/11 19:46 118-74-108/10/11 14:24178002260
Hexachlorocyclopentadiene ND ug/kg 10 08/14/11 19:46 77-47-408/10/11 14:24178003290
Hexachloroethane ND ug/kg 10 08/14/11 19:46 67-72-108/10/11 14:24178004690
Indeno(1,2,3-cd)pyrene 3790J ug/kg 10 08/14/11 19:46 193-39-508/10/11 14:24178003660
Isophorone ND ug/kg 10 08/14/11 19:46 78-59-108/10/11 14:24178003990
1-Methylnaphthalene ND ug/kg 10 08/14/11 19:46 90-12-008/10/11 14:24178004630
2-Methylnaphthalene ND ug/kg 10 08/14/11 19:46 91-57-608/10/11 14:24178003820
2-Methylphenol(o-Cresol)ND ug/kg 10 08/14/11 19:46 95-48-708/10/11 14:24178005390
3&4-Methylphenol(m&p Cresol)ND ug/kg 10 08/14/11 19:4608/10/11 14:24178007000
Naphthalene 5960J ug/kg 10 08/14/11 19:46 91-20-308/10/11 14:24178004360
2-Nitroaniline ND ug/kg 10 08/14/11 19:46 88-74-408/10/11 14:24889005490
3-Nitroaniline ND ug/kg 10 08/14/11 19:46 99-09-208/10/11 14:24889004850
4-Nitroaniline ND ug/kg 10 08/14/11 19:46 100-01-608/10/11 14:24356005010
Nitrobenzene ND ug/kg 10 08/14/11 19:46 98-95-308/10/11 14:24178004850
2-Nitrophenol ND ug/kg 10 08/14/11 19:46 88-75-508/10/11 14:24178004310
4-Nitrophenol ND ug/kg 10 08/14/11 19:46 100-02-708/10/11 14:24889003180
N-Nitrosodimethylamine ND ug/kg 10 08/14/11 19:46 62-75-908/10/11 14:24178005760
N-Nitroso-di-n-propylamine ND ug/kg 10 08/14/11 19:46 621-64-708/10/11 14:24178003390
N-Nitrosodiphenylamine ND ug/kg 10 08/14/11 19:46 86-30-608/10/11 14:24178005280
Pentachlorophenol ND ug/kg 10 08/14/11 19:46 87-86-508/10/11 14:24889003230
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 17 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-4 Lab ID:9299254013 Collected:07/27/11 09:30 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Phenanthrene 22000 ug/kg 10 08/14/11 19:46 85-01-808/10/11 14:24178002960
Phenol ND ug/kg 10 08/14/11 19:46 108-95-2 D3,P308/10/11 14:24178005330
Pyrene 12600J ug/kg 10 08/14/11 19:46 129-00-008/10/11 14:24178003020
1,2,4-Trichlorobenzene ND ug/kg 10 08/14/11 19:46 120-82-108/10/11 14:24178003450
2,4,5-Trichlorophenol ND ug/kg 10 08/14/11 19:46 95-95-408/10/11 14:24178005490
2,4,6-Trichlorophenol ND ug/kg 10 08/14/11 19:46 88-06-208/10/11 14:24178003930
Nitrobenzene-d5 (S)0 %10 08/14/11 19:46 4165-60-0 S408/10/11 14:2423-110
2-Fluorobiphenyl (S)0 %10 08/14/11 19:46 321-60-808/10/11 14:2430-110
Terphenyl-d14 (S)0 %10 08/14/11 19:46 1718-51-008/10/11 14:2428-110
Phenol-d6 (S)0 %10 08/14/11 19:46 13127-88-308/10/11 14:2422-110
2-Fluorophenol (S)0 %10 08/14/11 19:46 367-12-408/10/11 14:2413-110
2,4,6-Tribromophenol (S)0 %10 08/14/11 19:46 118-79-608/10/11 14:2427-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 39.3J ug/kg 1 07/31/11 14:13 67-64-194.8 9.5
Benzene ND ug/kg 1 07/31/11 14:13 71-43-24.7 1.5
Bromobenzene ND ug/kg 1 07/31/11 14:13 108-86-14.7 1.9
Bromochloromethane ND ug/kg 1 07/31/11 14:13 74-97-54.7 1.6
Bromodichloromethane ND ug/kg 1 07/31/11 14:13 75-27-44.7 1.8
Bromoform ND ug/kg 1 07/31/11 14:13 75-25-24.7 2.2
Bromomethane ND ug/kg 1 07/31/11 14:13 74-83-99.5 2.4
2-Butanone (MEK)ND ug/kg 1 07/31/11 14:13 78-93-394.8 2.8
n-Butylbenzene ND ug/kg 1 07/31/11 14:13 104-51-84.7 1.7
sec-Butylbenzene ND ug/kg 1 07/31/11 14:13 135-98-84.7 1.5
tert-Butylbenzene ND ug/kg 1 07/31/11 14:13 98-06-64.7 1.9
Carbon tetrachloride ND ug/kg 1 07/31/11 14:13 56-23-54.7 2.5
Chlorobenzene ND ug/kg 1 07/31/11 14:13 108-90-74.7 1.8
Chloroethane ND ug/kg 1 07/31/11 14:13 75-00-39.5 2.3
Chloroform ND ug/kg 1 07/31/11 14:13 67-66-34.7 1.5
Chloromethane ND ug/kg 1 07/31/11 14:13 74-87-39.5 2.3
2-Chlorotoluene ND ug/kg 1 07/31/11 14:13 95-49-84.7 1.6
4-Chlorotoluene ND ug/kg 1 07/31/11 14:13 106-43-44.7 1.7
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/31/11 14:13 96-12-84.7 3.4
Dibromochloromethane ND ug/kg 1 07/31/11 14:13 124-48-14.7 1.7
1,2-Dibromoethane (EDB)ND ug/kg 1 07/31/11 14:13 106-93-44.7 1.7
Dibromomethane ND ug/kg 1 07/31/11 14:13 74-95-34.7 2.4
1,2-Dichlorobenzene ND ug/kg 1 07/31/11 14:13 95-50-14.7 1.8
1,3-Dichlorobenzene ND ug/kg 1 07/31/11 14:13 541-73-14.7 1.9
1,4-Dichlorobenzene ND ug/kg 1 07/31/11 14:13 106-46-74.7 1.6
Dichlorodifluoromethane ND ug/kg 1 07/31/11 14:13 75-71-8 IO9.5 3.4
1,1-Dichloroethane ND ug/kg 1 07/31/11 14:13 75-34-34.7 1.4
1,2-Dichloroethane ND ug/kg 1 07/31/11 14:13 107-06-24.7 2.1
1,1-Dichloroethene ND ug/kg 1 07/31/11 14:13 75-35-44.7 1.7
cis-1,2-Dichloroethene ND ug/kg 1 07/31/11 14:13 156-59-24.7 1.3
trans-1,2-Dichloroethene ND ug/kg 1 07/31/11 14:13 156-60-54.7 1.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 18 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-4 Lab ID:9299254013 Collected:07/27/11 09:30 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dichloropropane ND ug/kg 1 07/31/11 14:13 78-87-54.7 1.6
1,3-Dichloropropane ND ug/kg 1 07/31/11 14:13 142-28-94.7 1.8
2,2-Dichloropropane ND ug/kg 1 07/31/11 14:13 594-20-74.7 1.6
1,1-Dichloropropene ND ug/kg 1 07/31/11 14:13 563-58-64.7 1.4
cis-1,3-Dichloropropene ND ug/kg 1 07/31/11 14:13 10061-01-54.7 1.7
trans-1,3-Dichloropropene ND ug/kg 1 07/31/11 14:13 10061-02-64.7 1.4
Diisopropyl ether ND ug/kg 1 07/31/11 14:13 108-20-34.7 1.6
Ethylbenzene ND ug/kg 1 07/31/11 14:13 100-41-44.7 1.7
Hexachloro-1,3-butadiene ND ug/kg 1 07/31/11 14:13 87-68-34.7 1.9
2-Hexanone ND ug/kg 1 07/31/11 14:13 591-78-647.4 3.7
Isopropylbenzene (Cumene)ND ug/kg 1 07/31/11 14:13 98-82-84.7 1.8
p-Isopropyltoluene ND ug/kg 1 07/31/11 14:13 99-87-64.7 1.6
Methylene Chloride ND ug/kg 1 07/31/11 14:13 75-09-219.0 2.8
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/31/11 14:13 108-10-147.4 3.5
Methyl-tert-butyl ether ND ug/kg 1 07/31/11 14:13 1634-04-44.7 1.4
Naphthalene ND ug/kg 1 07/31/11 14:13 91-20-34.7 1.1
n-Propylbenzene ND ug/kg 1 07/31/11 14:13 103-65-14.7 1.6
Styrene ND ug/kg 1 07/31/11 14:13 100-42-54.7 1.7
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/31/11 14:13 630-20-64.7 2.0
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/31/11 14:13 79-34-54.7 1.8
Tetrachloroethene ND ug/kg 1 07/31/11 14:13 127-18-44.7 1.6
Toluene ND ug/kg 1 07/31/11 14:13 108-88-34.7 1.7
1,2,3-Trichlorobenzene ND ug/kg 1 07/31/11 14:13 87-61-64.7 2.1
1,2,4-Trichlorobenzene ND ug/kg 1 07/31/11 14:13 120-82-14.7 1.5
1,1,1-Trichloroethane ND ug/kg 1 07/31/11 14:13 71-55-64.7 1.7
1,1,2-Trichloroethane ND ug/kg 1 07/31/11 14:13 79-00-54.7 2.0
Trichloroethene ND ug/kg 1 07/31/11 14:13 79-01-64.7 2.0
Trichlorofluoromethane ND ug/kg 1 07/31/11 14:13 75-69-44.7 2.1
1,2,3-Trichloropropane ND ug/kg 1 07/31/11 14:13 96-18-44.7 1.5
1,2,4-Trimethylbenzene ND ug/kg 1 07/31/11 14:13 95-63-64.7 1.9
1,3,5-Trimethylbenzene ND ug/kg 1 07/31/11 14:13 108-67-84.7 1.7
Vinyl acetate ND ug/kg 1 07/31/11 14:13 108-05-447.4 8.3
Vinyl chloride ND ug/kg 1 07/31/11 14:13 75-01-49.5 1.7
Xylene (Total)ND ug/kg 1 07/31/11 14:13 1330-20-79.5 3.4
m&p-Xylene ND ug/kg 1 07/31/11 14:13 179601-23-19.5 3.4
o-Xylene ND ug/kg 1 07/31/11 14:13 95-47-64.7 1.8
Dibromofluoromethane (S)103 %1 07/31/11 14:13 1868-53-770-130
Toluene-d8 (S)102 %1 07/31/11 14:13 2037-26-570-130
4-Bromofluorobenzene (S)81 %1 07/31/11 14:13 460-00-470-130
1,2-Dichloroethane-d4 (S)93 %1 07/31/11 14:13 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 7.2 %1 07/29/11 14:520.10 0.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 19 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-10 Lab ID:9299254014 Collected:07/27/11 10:25 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/29/11 18:44 67-64-189.8 9.0
Benzene ND ug/kg 1 07/29/11 18:44 71-43-24.5 1.4
Bromobenzene ND ug/kg 1 07/29/11 18:44 108-86-14.5 1.8
Bromochloromethane ND ug/kg 1 07/29/11 18:44 74-97-54.5 1.5
Bromodichloromethane ND ug/kg 1 07/29/11 18:44 75-27-44.5 1.7
Bromoform ND ug/kg 1 07/29/11 18:44 75-25-24.5 2.1
Bromomethane ND ug/kg 1 07/29/11 18:44 74-83-99.0 2.2
2-Butanone (MEK)ND ug/kg 1 07/29/11 18:44 78-93-389.8 2.6
n-Butylbenzene ND ug/kg 1 07/29/11 18:44 104-51-84.5 1.6
sec-Butylbenzene ND ug/kg 1 07/29/11 18:44 135-98-84.5 1.4
tert-Butylbenzene ND ug/kg 1 07/29/11 18:44 98-06-64.5 1.8
Carbon tetrachloride ND ug/kg 1 07/29/11 18:44 56-23-54.5 2.3
Chlorobenzene ND ug/kg 1 07/29/11 18:44 108-90-74.5 1.7
Chloroethane ND ug/kg 1 07/29/11 18:44 75-00-39.0 2.2
Chloroform ND ug/kg 1 07/29/11 18:44 67-66-34.5 1.4
Chloromethane ND ug/kg 1 07/29/11 18:44 74-87-39.0 2.2
2-Chlorotoluene ND ug/kg 1 07/29/11 18:44 95-49-84.5 1.5
4-Chlorotoluene ND ug/kg 1 07/29/11 18:44 106-43-44.5 1.6
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/29/11 18:44 96-12-84.5 3.2
Dibromochloromethane ND ug/kg 1 07/29/11 18:44 124-48-14.5 1.6
1,2-Dibromoethane (EDB)ND ug/kg 1 07/29/11 18:44 106-93-44.5 1.6
Dibromomethane ND ug/kg 1 07/29/11 18:44 74-95-34.5 2.2
1,2-Dichlorobenzene ND ug/kg 1 07/29/11 18:44 95-50-14.5 1.7
1,3-Dichlorobenzene ND ug/kg 1 07/29/11 18:44 541-73-14.5 1.8
1,4-Dichlorobenzene ND ug/kg 1 07/29/11 18:44 106-46-74.5 1.5
Dichlorodifluoromethane ND ug/kg 1 07/29/11 18:44 75-71-89.0 3.2
1,1-Dichloroethane ND ug/kg 1 07/29/11 18:44 75-34-34.5 1.3
1,2-Dichloroethane ND ug/kg 1 07/29/11 18:44 107-06-24.5 2.0
1,1-Dichloroethene ND ug/kg 1 07/29/11 18:44 75-35-44.5 1.6
cis-1,2-Dichloroethene ND ug/kg 1 07/29/11 18:44 156-59-24.5 1.3
trans-1,2-Dichloroethene ND ug/kg 1 07/29/11 18:44 156-60-54.5 1.7
1,2-Dichloropropane ND ug/kg 1 07/29/11 18:44 78-87-54.5 1.5
1,3-Dichloropropane ND ug/kg 1 07/29/11 18:44 142-28-94.5 1.7
2,2-Dichloropropane ND ug/kg 1 07/29/11 18:44 594-20-74.5 1.5
1,1-Dichloropropene ND ug/kg 1 07/29/11 18:44 563-58-64.5 1.3
cis-1,3-Dichloropropene ND ug/kg 1 07/29/11 18:44 10061-01-54.5 1.6
trans-1,3-Dichloropropene ND ug/kg 1 07/29/11 18:44 10061-02-64.5 1.3
Diisopropyl ether ND ug/kg 1 07/29/11 18:44 108-20-34.5 1.5
Ethylbenzene ND ug/kg 1 07/29/11 18:44 100-41-44.5 1.6
Hexachloro-1,3-butadiene ND ug/kg 1 07/29/11 18:44 87-68-34.5 1.8
2-Hexanone ND ug/kg 1 07/29/11 18:44 591-78-644.9 3.5
Isopropylbenzene (Cumene)ND ug/kg 1 07/29/11 18:44 98-82-84.5 1.7
p-Isopropyltoluene ND ug/kg 1 07/29/11 18:44 99-87-64.5 1.5
Methylene Chloride ND ug/kg 1 07/29/11 18:44 75-09-218.0 2.7
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/29/11 18:44 108-10-144.9 3.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 20 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-10 Lab ID:9299254014 Collected:07/27/11 10:25 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
Methyl-tert-butyl ether ND ug/kg 1 07/29/11 18:44 1634-04-44.5 1.3
Naphthalene ND ug/kg 1 07/29/11 18:44 91-20-34.5 1.1
n-Propylbenzene ND ug/kg 1 07/29/11 18:44 103-65-14.5 1.5
Styrene ND ug/kg 1 07/29/11 18:44 100-42-54.5 1.6
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/29/11 18:44 630-20-64.5 1.9
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/29/11 18:44 79-34-54.5 1.7
Tetrachloroethene ND ug/kg 1 07/29/11 18:44 127-18-44.5 1.5
Toluene ND ug/kg 1 07/29/11 18:44 108-88-34.5 1.6
1,2,3-Trichlorobenzene ND ug/kg 1 07/29/11 18:44 87-61-64.5 2.0
1,2,4-Trichlorobenzene ND ug/kg 1 07/29/11 18:44 120-82-14.5 1.4
1,1,1-Trichloroethane ND ug/kg 1 07/29/11 18:44 71-55-64.5 1.6
1,1,2-Trichloroethane ND ug/kg 1 07/29/11 18:44 79-00-54.5 1.9
Trichloroethene ND ug/kg 1 07/29/11 18:44 79-01-64.5 1.9
Trichlorofluoromethane ND ug/kg 1 07/29/11 18:44 75-69-44.5 2.0
1,2,3-Trichloropropane ND ug/kg 1 07/29/11 18:44 96-18-44.5 1.4
1,2,4-Trimethylbenzene ND ug/kg 1 07/29/11 18:44 95-63-64.5 1.8
1,3,5-Trimethylbenzene ND ug/kg 1 07/29/11 18:44 108-67-84.5 1.6
Vinyl acetate ND ug/kg 1 07/29/11 18:44 108-05-444.9 7.9
Vinyl chloride ND ug/kg 1 07/29/11 18:44 75-01-49.0 1.6
Xylene (Total)ND ug/kg 1 07/29/11 18:44 1330-20-79.0 3.2
m&p-Xylene ND ug/kg 1 07/29/11 18:44 179601-23-19.0 3.2
o-Xylene ND ug/kg 1 07/29/11 18:44 95-47-64.5 1.7
Dibromofluoromethane (S)104 %1 07/29/11 18:44 1868-53-770-130
Toluene-d8 (S)104 %1 07/29/11 18:44 2037-26-570-130
4-Bromofluorobenzene (S)95 %1 07/29/11 18:44 460-00-470-130
1,2-Dichloroethane-d4 (S)97 %1 07/29/11 18:44 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 15.3 %1 07/29/11 14:520.10 0.10
Sample:SB-13 Lab ID:9299254015 Collected:07/27/11 11:10 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/31/11 14:34 67-64-190.7 9.1
Benzene ND ug/kg 1 07/31/11 14:34 71-43-24.5 1.5
Bromobenzene ND ug/kg 1 07/31/11 14:34 108-86-14.5 1.8
Bromochloromethane ND ug/kg 1 07/31/11 14:34 74-97-54.5 1.5
Bromodichloromethane ND ug/kg 1 07/31/11 14:34 75-27-44.5 1.7
Bromoform ND ug/kg 1 07/31/11 14:34 75-25-24.5 2.1
Bromomethane ND ug/kg 1 07/31/11 14:34 74-83-99.1 2.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 21 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-13 Lab ID:9299254015 Collected:07/27/11 11:10 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
2-Butanone (MEK)ND ug/kg 1 07/31/11 14:34 78-93-390.7 2.6
n-Butylbenzene ND ug/kg 1 07/31/11 14:34 104-51-84.5 1.6
sec-Butylbenzene ND ug/kg 1 07/31/11 14:34 135-98-84.5 1.5
tert-Butylbenzene ND ug/kg 1 07/31/11 14:34 98-06-64.5 1.8
Carbon tetrachloride ND ug/kg 1 07/31/11 14:34 56-23-54.5 2.4
Chlorobenzene ND ug/kg 1 07/31/11 14:34 108-90-74.5 1.7
Chloroethane ND ug/kg 1 07/31/11 14:34 75-00-39.1 2.2
Chloroform ND ug/kg 1 07/31/11 14:34 67-66-34.5 1.5
Chloromethane ND ug/kg 1 07/31/11 14:34 74-87-39.1 2.2
2-Chlorotoluene ND ug/kg 1 07/31/11 14:34 95-49-84.5 1.5
4-Chlorotoluene ND ug/kg 1 07/31/11 14:34 106-43-44.5 1.6
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/31/11 14:34 96-12-84.5 3.3
Dibromochloromethane ND ug/kg 1 07/31/11 14:34 124-48-14.5 1.6
1,2-Dibromoethane (EDB)ND ug/kg 1 07/31/11 14:34 106-93-44.5 1.6
Dibromomethane ND ug/kg 1 07/31/11 14:34 74-95-34.5 2.3
1,2-Dichlorobenzene ND ug/kg 1 07/31/11 14:34 95-50-14.5 1.7
1,3-Dichlorobenzene ND ug/kg 1 07/31/11 14:34 541-73-14.5 1.8
1,4-Dichlorobenzene ND ug/kg 1 07/31/11 14:34 106-46-74.5 1.5
Dichlorodifluoromethane ND ug/kg 1 07/31/11 14:34 75-71-89.1 3.3
1,1-Dichloroethane ND ug/kg 1 07/31/11 14:34 75-34-34.5 1.4
1,2-Dichloroethane ND ug/kg 1 07/31/11 14:34 107-06-24.5 2.0
1,1-Dichloroethene ND ug/kg 1 07/31/11 14:34 75-35-44.5 1.6
cis-1,2-Dichloroethene ND ug/kg 1 07/31/11 14:34 156-59-24.5 1.3
trans-1,2-Dichloroethene ND ug/kg 1 07/31/11 14:34 156-60-54.5 1.7
1,2-Dichloropropane ND ug/kg 1 07/31/11 14:34 78-87-54.5 1.5
1,3-Dichloropropane ND ug/kg 1 07/31/11 14:34 142-28-94.5 1.7
2,2-Dichloropropane ND ug/kg 1 07/31/11 14:34 594-20-74.5 1.5
1,1-Dichloropropene ND ug/kg 1 07/31/11 14:34 563-58-64.5 1.4
cis-1,3-Dichloropropene ND ug/kg 1 07/31/11 14:34 10061-01-54.5 1.6
trans-1,3-Dichloropropene ND ug/kg 1 07/31/11 14:34 10061-02-64.5 1.4
Diisopropyl ether ND ug/kg 1 07/31/11 14:34 108-20-34.5 1.5
Ethylbenzene ND ug/kg 1 07/31/11 14:34 100-41-44.5 1.6
Hexachloro-1,3-butadiene ND ug/kg 1 07/31/11 14:34 87-68-34.5 1.8
2-Hexanone ND ug/kg 1 07/31/11 14:34 591-78-645.4 3.5
Isopropylbenzene (Cumene)ND ug/kg 1 07/31/11 14:34 98-82-84.5 1.7
p-Isopropyltoluene ND ug/kg 1 07/31/11 14:34 99-87-64.5 1.5
Methylene Chloride ND ug/kg 1 07/31/11 14:34 75-09-218.1 2.7
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/31/11 14:34 108-10-145.4 3.4
Methyl-tert-butyl ether ND ug/kg 1 07/31/11 14:34 1634-04-44.5 1.4
Naphthalene ND ug/kg 1 07/31/11 14:34 91-20-34.5 1.1
n-Propylbenzene ND ug/kg 1 07/31/11 14:34 103-65-14.5 1.5
Styrene ND ug/kg 1 07/31/11 14:34 100-42-54.5 1.6
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/31/11 14:34 630-20-64.5 1.9
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/31/11 14:34 79-34-54.5 1.7
Tetrachloroethene ND ug/kg 1 07/31/11 14:34 127-18-44.5 1.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 22 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-13 Lab ID:9299254015 Collected:07/27/11 11:10 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
Toluene ND ug/kg 1 07/31/11 14:34 108-88-34.5 1.6
1,2,3-Trichlorobenzene ND ug/kg 1 07/31/11 14:34 87-61-64.5 2.0
1,2,4-Trichlorobenzene ND ug/kg 1 07/31/11 14:34 120-82-14.5 1.5
1,1,1-Trichloroethane ND ug/kg 1 07/31/11 14:34 71-55-64.5 1.6
1,1,2-Trichloroethane ND ug/kg 1 07/31/11 14:34 79-00-54.5 1.9
Trichloroethene ND ug/kg 1 07/31/11 14:34 79-01-64.5 1.9
Trichlorofluoromethane ND ug/kg 1 07/31/11 14:34 75-69-44.5 2.0
1,2,3-Trichloropropane ND ug/kg 1 07/31/11 14:34 96-18-44.5 1.5
1,2,4-Trimethylbenzene ND ug/kg 1 07/31/11 14:34 95-63-64.5 1.8
1,3,5-Trimethylbenzene ND ug/kg 1 07/31/11 14:34 108-67-84.5 1.6
Vinyl acetate ND ug/kg 1 07/31/11 14:34 108-05-445.4 8.0
Vinyl chloride ND ug/kg 1 07/31/11 14:34 75-01-49.1 1.6
Xylene (Total)ND ug/kg 1 07/31/11 14:34 1330-20-79.1 3.3
m&p-Xylene ND ug/kg 1 07/31/11 14:34 179601-23-19.1 3.3
o-Xylene ND ug/kg 1 07/31/11 14:34 95-47-64.5 1.7
Dibromofluoromethane (S)103 %1 07/31/11 14:34 1868-53-770-130
Toluene-d8 (S)101 %1 07/31/11 14:34 2037-26-570-130
4-Bromofluorobenzene (S)87 %1 07/31/11 14:34 460-00-470-130
1,2-Dichloroethane-d4 (S)101 %1 07/31/11 14:34 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 7.4 %1 07/29/11 14:520.10 0.10
Sample:SB-16 Lab ID:9299254016 Collected:07/27/11 12:10 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 1.6 mg/kg 1 08/02/11 18:11 7440-36-008/02/11 09:000.55 0.31
Arsenic 6.3 mg/kg 1 08/02/11 18:11 7440-38-208/02/11 09:000.55 0.35
Beryllium 0.29 mg/kg 1 08/02/11 18:11 7440-41-708/02/11 09:000.11 0.022
Cadmium 4.8 mg/kg 1 08/02/11 18:11 7440-43-908/02/11 09:000.11 0.066
Chromium 16.1 mg/kg 1 08/02/11 18:11 7440-47-308/02/11 09:000.55 0.033
Copper 115 mg/kg 1 08/02/11 18:11 7440-50-808/02/11 09:000.55 0.044
Lead 232 mg/kg 1 08/02/11 18:11 7439-92-108/02/11 09:000.55 0.52
Manganese 151 mg/kg 1 08/02/11 18:11 7439-96-508/02/11 09:000.55 0.033
Nickel 5.0 mg/kg 1 08/02/11 18:11 7440-02-008/02/11 09:000.55 0.20
Selenium 0.99J mg/kg 1 08/02/11 18:11 7782-49-208/02/11 09:001.1 0.42
Silver 0.18J mg/kg 1 08/02/11 18:11 7440-22-408/02/11 09:000.55 0.033
Thallium ND mg/kg 1 08/02/11 18:11 7440-28-008/02/11 09:001.1 0.28
Zinc 2160 mg/kg 10 08/03/11 20:00 7440-66-608/02/11 09:0010.9 2.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 23 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-16 Lab ID:9299254016 Collected:07/27/11 12:10 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.80 mg/kg 10 08/03/11 11:56 7439-97-608/01/11 14:150.046 0.00091
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 10 08/03/11 10:04 83-32-907/29/11 08:30191004400
Acenaphthylene ND ug/kg 10 08/03/11 10:04 208-96-807/29/11 08:30191004520
Aniline ND ug/kg 10 08/03/11 10:04 62-53-307/29/11 08:30191005150
Anthracene ND ug/kg 10 08/03/11 10:04 120-12-707/29/11 08:30191004280
Benzo(a)anthracene ND ug/kg 10 08/03/11 10:04 56-55-307/29/11 08:30191003530
Benzo(a)pyrene ND ug/kg 10 08/03/11 10:04 50-32-807/29/11 08:30191003650
Benzo(b)fluoranthene ND ug/kg 10 08/03/11 10:04 205-99-207/29/11 08:30191003300
Benzo(g,h,i)perylene ND ug/kg 10 08/03/11 10:04 191-24-207/29/11 08:30191004860
Benzo(k)fluoranthene ND ug/kg 10 08/03/11 10:04 207-08-907/29/11 08:30191003760
Benzoic Acid ND ug/kg 10 08/03/11 10:04 65-85-007/29/11 08:30955003470
Benzyl alcohol ND ug/kg 10 08/03/11 10:04 100-51-607/29/11 08:30382003820
4-Bromophenylphenyl ether ND ug/kg 10 08/03/11 10:04 101-55-307/29/11 08:30191003470
Butylbenzylphthalate ND ug/kg 10 08/03/11 10:04 85-68-707/29/11 08:30191004050
4-Chloro-3-methylphenol ND ug/kg 10 08/03/11 10:04 59-50-707/29/11 08:30382003940
4-Chloroaniline ND ug/kg 10 08/03/11 10:04 106-47-807/29/11 08:30955005330
bis(2-Chloroethoxy)methane ND ug/kg 10 08/03/11 10:04 111-91-107/29/11 08:30191004460
bis(2-Chloroethyl) ether ND ug/kg 10 08/03/11 10:04 111-44-407/29/11 08:30191004860
bis(2-Chloroisopropyl) ether ND ug/kg 10 08/03/11 10:04 108-60-107/29/11 08:30191005100
2-Chloronaphthalene ND ug/kg 10 08/03/11 10:04 91-58-707/29/11 08:30191003760
2-Chlorophenol ND ug/kg 10 08/03/11 10:04 95-57-807/29/11 08:30191005210
4-Chlorophenylphenyl ether ND ug/kg 10 08/03/11 10:04 7005-72-307/29/11 08:30191003940
Chrysene ND ug/kg 10 08/03/11 10:04 218-01-907/29/11 08:30191002550
Dibenz(a,h)anthracene ND ug/kg 10 08/03/11 10:04 53-70-307/29/11 08:30191004050
Dibenzofuran ND ug/kg 10 08/03/11 10:04 132-64-907/29/11 08:30191003130
1,2-Dichlorobenzene ND ug/kg 10 08/03/11 10:04 95-50-107/29/11 08:30191005100
1,3-Dichlorobenzene ND ug/kg 10 08/03/11 10:04 541-73-107/29/11 08:30191004340
1,4-Dichlorobenzene ND ug/kg 10 08/03/11 10:04 106-46-707/29/11 08:30191005380
3,3'-Dichlorobenzidine ND ug/kg 10 08/03/11 10:04 91-94-107/29/11 08:30955004170
2,4-Dichlorophenol ND ug/kg 10 08/03/11 10:04 120-83-207/29/11 08:30191004170
Diethylphthalate ND ug/kg 10 08/03/11 10:04 84-66-207/29/11 08:30191002950
2,4-Dimethylphenol ND ug/kg 10 08/03/11 10:04 105-67-907/29/11 08:30191007530
Dimethylphthalate ND ug/kg 10 08/03/11 10:04 131-11-307/29/11 08:30191003880
Di-n-butylphthalate ND ug/kg 10 08/03/11 10:04 84-74-207/29/11 08:30191003130
4,6-Dinitro-2-methylphenol ND ug/kg 10 08/03/11 10:04 534-52-107/29/11 08:30382003820
2,4-Dinitrophenol ND ug/kg 10 08/03/11 10:04 51-28-507/29/11 08:30955003130
2,4-Dinitrotoluene ND ug/kg 10 08/03/11 10:04 121-14-207/29/11 08:30191003590
2,6-Dinitrotoluene ND ug/kg 10 08/03/11 10:04 606-20-207/29/11 08:30191004000
Di-n-octylphthalate ND ug/kg 10 08/03/11 10:04 117-84-007/29/11 08:30191004000
bis(2-Ethylhexyl)phthalate ND ug/kg 10 08/03/11 10:04 117-81-707/29/11 08:30191005210
Fluoranthene ND ug/kg 10 08/03/11 10:04 206-44-007/29/11 08:30191002780
Fluorene ND ug/kg 10 08/03/11 10:04 86-73-707/29/11 08:30191003940
Hexachloro-1,3-butadiene ND ug/kg 10 08/03/11 10:04 87-68-307/29/11 08:30191003300
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 24 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-16 Lab ID:9299254016 Collected:07/27/11 12:10 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Hexachlorobenzene ND ug/kg 10 08/03/11 10:04 118-74-107/29/11 08:30191002430
Hexachlorocyclopentadiene ND ug/kg 10 08/03/11 10:04 77-47-407/29/11 08:30191003530
Hexachloroethane ND ug/kg 10 08/03/11 10:04 67-72-107/29/11 08:30191005040
Indeno(1,2,3-cd)pyrene ND ug/kg 10 08/03/11 10:04 193-39-507/29/11 08:30191003940
Isophorone ND ug/kg 10 08/03/11 10:04 78-59-107/29/11 08:30191004280
1-Methylnaphthalene ND ug/kg 10 08/03/11 10:04 90-12-007/29/11 08:30191004980
2-Methylnaphthalene ND ug/kg 10 08/03/11 10:04 91-57-607/29/11 08:30191004110
2-Methylphenol(o-Cresol)ND ug/kg 10 08/03/11 10:04 95-48-707/29/11 08:30191005790
3&4-Methylphenol(m&p Cresol)ND ug/kg 10 08/03/11 10:0407/29/11 08:30191007530
Naphthalene ND ug/kg 10 08/03/11 10:04 91-20-307/29/11 08:30191004690
2-Nitroaniline ND ug/kg 10 08/03/11 10:04 88-74-407/29/11 08:30955005910
3-Nitroaniline ND ug/kg 10 08/03/11 10:04 99-09-207/29/11 08:30955005210
4-Nitroaniline ND ug/kg 10 08/03/11 10:04 100-01-607/29/11 08:30382005380
Nitrobenzene ND ug/kg 10 08/03/11 10:04 98-95-307/29/11 08:30191005210
2-Nitrophenol ND ug/kg 10 08/03/11 10:04 88-75-507/29/11 08:30191004630
4-Nitrophenol ND ug/kg 10 08/03/11 10:04 100-02-707/29/11 08:30955003420
N-Nitrosodimethylamine ND ug/kg 10 08/03/11 10:04 62-75-907/29/11 08:30191006200
N-Nitroso-di-n-propylamine ND ug/kg 10 08/03/11 10:04 621-64-707/29/11 08:30191003650
N-Nitrosodiphenylamine ND ug/kg 10 08/03/11 10:04 86-30-607/29/11 08:30191005670
Pentachlorophenol ND ug/kg 10 08/03/11 10:04 87-86-507/29/11 08:30955003470
Phenanthrene ND ug/kg 10 08/03/11 10:04 85-01-807/29/11 08:30191003180
Phenol ND ug/kg 10 08/03/11 10:04 108-95-2 D3,P307/29/11 08:30191005730
Pyrene ND ug/kg 10 08/03/11 10:04 129-00-007/29/11 08:30191003240
1,2,4-Trichlorobenzene ND ug/kg 10 08/03/11 10:04 120-82-107/29/11 08:30191003710
2,4,5-Trichlorophenol ND ug/kg 10 08/03/11 10:04 95-95-407/29/11 08:30191005910
2,4,6-Trichlorophenol ND ug/kg 10 08/03/11 10:04 88-06-207/29/11 08:30191004230
Nitrobenzene-d5 (S)0 %10 08/03/11 10:04 4165-60-0 S407/29/11 08:3023-110
2-Fluorobiphenyl (S)0 %10 08/03/11 10:04 321-60-807/29/11 08:3030-110
Terphenyl-d14 (S)0 %10 08/03/11 10:04 1718-51-007/29/11 08:3028-110
Phenol-d6 (S)0 %10 08/03/11 10:04 13127-88-307/29/11 08:3022-110
2-Fluorophenol (S)0 %10 08/03/11 10:04 367-12-407/29/11 08:3013-110
2,4,6-Tribromophenol (S)0 %10 08/03/11 10:04 118-79-607/29/11 08:3027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 120 ug/kg 1 07/31/11 14:54 67-64-1 C988.7 8.9
Benzene ND ug/kg 1 07/31/11 14:54 71-43-24.4 1.4
Bromobenzene ND ug/kg 1 07/31/11 14:54 108-86-14.4 1.8
Bromochloromethane ND ug/kg 1 07/31/11 14:54 74-97-54.4 1.5
Bromodichloromethane ND ug/kg 1 07/31/11 14:54 75-27-44.4 1.7
Bromoform ND ug/kg 1 07/31/11 14:54 75-25-24.4 2.0
Bromomethane ND ug/kg 1 07/31/11 14:54 74-83-98.9 2.2
2-Butanone (MEK)5.7J ug/kg 1 07/31/11 14:54 78-93-388.7 2.6
n-Butylbenzene ND ug/kg 1 07/31/11 14:54 104-51-84.4 1.6
sec-Butylbenzene ND ug/kg 1 07/31/11 14:54 135-98-84.4 1.4
tert-Butylbenzene ND ug/kg 1 07/31/11 14:54 98-06-64.4 1.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 25 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-16 Lab ID:9299254016 Collected:07/27/11 12:10 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
Carbon tetrachloride ND ug/kg 1 07/31/11 14:54 56-23-54.4 2.3
Chlorobenzene ND ug/kg 1 07/31/11 14:54 108-90-74.4 1.7
Chloroethane ND ug/kg 1 07/31/11 14:54 75-00-38.9 2.1
Chloroform ND ug/kg 1 07/31/11 14:54 67-66-34.4 1.4
Chloromethane ND ug/kg 1 07/31/11 14:54 74-87-38.9 2.1
2-Chlorotoluene ND ug/kg 1 07/31/11 14:54 95-49-84.4 1.5
4-Chlorotoluene ND ug/kg 1 07/31/11 14:54 106-43-44.4 1.6
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/31/11 14:54 96-12-84.4 3.2
Dibromochloromethane ND ug/kg 1 07/31/11 14:54 124-48-14.4 1.6
1,2-Dibromoethane (EDB)ND ug/kg 1 07/31/11 14:54 106-93-44.4 1.6
Dibromomethane ND ug/kg 1 07/31/11 14:54 74-95-34.4 2.2
1,2-Dichlorobenzene ND ug/kg 1 07/31/11 14:54 95-50-14.4 1.7
1,3-Dichlorobenzene ND ug/kg 1 07/31/11 14:54 541-73-14.4 1.8
1,4-Dichlorobenzene ND ug/kg 1 07/31/11 14:54 106-46-74.4 1.5
Dichlorodifluoromethane ND ug/kg 1 07/31/11 14:54 75-71-8 IO8.9 3.2
1,1-Dichloroethane ND ug/kg 1 07/31/11 14:54 75-34-34.4 1.3
1,2-Dichloroethane ND ug/kg 1 07/31/11 14:54 107-06-24.4 2.0
1,1-Dichloroethene ND ug/kg 1 07/31/11 14:54 75-35-44.4 1.6
cis-1,2-Dichloroethene ND ug/kg 1 07/31/11 14:54 156-59-24.4 1.2
trans-1,2-Dichloroethene ND ug/kg 1 07/31/11 14:54 156-60-54.4 1.7
1,2-Dichloropropane ND ug/kg 1 07/31/11 14:54 78-87-54.4 1.5
1,3-Dichloropropane ND ug/kg 1 07/31/11 14:54 142-28-94.4 1.7
2,2-Dichloropropane ND ug/kg 1 07/31/11 14:54 594-20-74.4 1.5
1,1-Dichloropropene ND ug/kg 1 07/31/11 14:54 563-58-64.4 1.3
cis-1,3-Dichloropropene ND ug/kg 1 07/31/11 14:54 10061-01-54.4 1.6
trans-1,3-Dichloropropene ND ug/kg 1 07/31/11 14:54 10061-02-64.4 1.3
Diisopropyl ether ND ug/kg 1 07/31/11 14:54 108-20-34.4 1.5
Ethylbenzene ND ug/kg 1 07/31/11 14:54 100-41-44.4 1.6
Hexachloro-1,3-butadiene ND ug/kg 1 07/31/11 14:54 87-68-34.4 1.8
2-Hexanone ND ug/kg 1 07/31/11 14:54 591-78-644.3 3.5
Isopropylbenzene (Cumene)ND ug/kg 1 07/31/11 14:54 98-82-84.4 1.7
p-Isopropyltoluene ND ug/kg 1 07/31/11 14:54 99-87-64.4 1.5
Methylene Chloride ND ug/kg 1 07/31/11 14:54 75-09-217.7 2.7
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/31/11 14:54 108-10-144.3 3.3
Methyl-tert-butyl ether ND ug/kg 1 07/31/11 14:54 1634-04-44.4 1.3
Naphthalene ND ug/kg 1 07/31/11 14:54 91-20-34.4 1.1
n-Propylbenzene ND ug/kg 1 07/31/11 14:54 103-65-14.4 1.5
Styrene ND ug/kg 1 07/31/11 14:54 100-42-54.4 1.6
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/31/11 14:54 630-20-64.4 1.9
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/31/11 14:54 79-34-54.4 1.7
Tetrachloroethene ND ug/kg 1 07/31/11 14:54 127-18-44.4 1.5
Toluene ND ug/kg 1 07/31/11 14:54 108-88-34.4 1.6
1,2,3-Trichlorobenzene ND ug/kg 1 07/31/11 14:54 87-61-64.4 2.0
1,2,4-Trichlorobenzene ND ug/kg 1 07/31/11 14:54 120-82-14.4 1.4
1,1,1-Trichloroethane ND ug/kg 1 07/31/11 14:54 71-55-64.4 1.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 26 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-16 Lab ID:9299254016 Collected:07/27/11 12:10 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,2-Trichloroethane ND ug/kg 1 07/31/11 14:54 79-00-54.4 1.9
Trichloroethene ND ug/kg 1 07/31/11 14:54 79-01-64.4 1.9
Trichlorofluoromethane ND ug/kg 1 07/31/11 14:54 75-69-44.4 2.0
1,2,3-Trichloropropane ND ug/kg 1 07/31/11 14:54 96-18-44.4 1.4
1,2,4-Trimethylbenzene ND ug/kg 1 07/31/11 14:54 95-63-64.4 1.8
1,3,5-Trimethylbenzene ND ug/kg 1 07/31/11 14:54 108-67-84.4 1.6
Vinyl acetate ND ug/kg 1 07/31/11 14:54 108-05-444.3 7.8
Vinyl chloride ND ug/kg 1 07/31/11 14:54 75-01-48.9 1.6
Xylene (Total)ND ug/kg 1 07/31/11 14:54 1330-20-78.9 3.2
m&p-Xylene ND ug/kg 1 07/31/11 14:54 179601-23-18.9 3.2
o-Xylene ND ug/kg 1 07/31/11 14:54 95-47-64.4 1.7
Dibromofluoromethane (S)116 %1 07/31/11 14:54 1868-53-770-130
Toluene-d8 (S)89 %1 07/31/11 14:54 2037-26-570-130
4-Bromofluorobenzene (S)63 %1 07/31/11 14:54 460-00-4 S270-130
1,2-Dichloroethane-d4 (S)113 %1 07/31/11 14:54 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 13.6 %1 07/29/11 14:530.10 0.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 16.1 mg/kg 1 08/04/11 15:44 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent 0.28J mg/kg 1 08/02/11 16:24 18540-29-9 N208/02/11 12:402.4 0.24
Sample:SB-17 Lab ID:9299254017 Collected:07/27/11 13:55 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 08/02/11 18:14 7440-36-008/02/11 09:000.58 0.32
Arsenic ND mg/kg 1 08/02/11 18:14 7440-38-208/02/11 09:000.58 0.37
Beryllium 0.30 mg/kg 1 08/02/11 18:14 7440-41-708/02/11 09:000.12 0.023
Cadmium 3.9 mg/kg 1 08/02/11 18:14 7440-43-908/02/11 09:000.12 0.069
Chromium 35.0 mg/kg 1 08/02/11 18:14 7440-47-308/02/11 09:000.58 0.035
Copper 73.6 mg/kg 1 08/02/11 18:14 7440-50-808/02/11 09:000.58 0.046
Lead 10.6 mg/kg 1 08/02/11 18:14 7439-92-108/02/11 09:000.58 0.55
Manganese 52.2 mg/kg 1 08/02/11 18:14 7439-96-508/02/11 09:000.58 0.035
Nickel 2.8 mg/kg 1 08/02/11 18:14 7440-02-008/02/11 09:000.58 0.21
Selenium 1.6 mg/kg 1 08/02/11 18:14 7782-49-208/02/11 09:001.2 0.44
Silver ND mg/kg 1 08/02/11 18:14 7440-22-408/02/11 09:000.58 0.035
Thallium 0.53J mg/kg 1 08/02/11 18:14 7440-28-008/02/11 09:001.2 0.30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 27 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-17 Lab ID:9299254017 Collected:07/27/11 13:55 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Zinc 20.7 mg/kg 1 08/02/11 18:14 7440-66-608/02/11 09:001.2 0.30
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.037 mg/kg 1 08/02/11 15:14 7439-97-608/01/11 14:150.0054 0.00011
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 08/02/11 19:06 83-32-907/29/11 08:30455105
Acenaphthylene ND ug/kg 1 08/02/11 19:06 208-96-807/29/11 08:30455108
Aniline ND ug/kg 1 08/02/11 19:06 62-53-307/29/11 08:30455123
Anthracene ND ug/kg 1 08/02/11 19:06 120-12-707/29/11 08:30455102
Benzo(a)anthracene ND ug/kg 1 08/02/11 19:06 56-55-307/29/11 08:3045584.2
Benzo(a)pyrene ND ug/kg 1 08/02/11 19:06 50-32-807/29/11 08:3045586.9
Benzo(b)fluoranthene ND ug/kg 1 08/02/11 19:06 205-99-207/29/11 08:3045578.7
Benzo(g,h,i)perylene ND ug/kg 1 08/02/11 19:06 191-24-207/29/11 08:30455116
Benzo(k)fluoranthene ND ug/kg 1 08/02/11 19:06 207-08-907/29/11 08:3045589.7
Benzoic Acid ND ug/kg 1 08/02/11 19:06 65-85-007/29/11 08:30228082.8
Benzyl alcohol ND ug/kg 1 08/02/11 19:06 100-51-607/29/11 08:3091191.1
4-Bromophenylphenyl ether ND ug/kg 1 08/02/11 19:06 101-55-307/29/11 08:3045582.8
Butylbenzylphthalate ND ug/kg 1 08/02/11 19:06 85-68-707/29/11 08:3045596.6
4-Chloro-3-methylphenol ND ug/kg 1 08/02/11 19:06 59-50-707/29/11 08:3091193.8
4-Chloroaniline ND ug/kg 1 08/02/11 19:06 106-47-807/29/11 08:302280127
bis(2-Chloroethoxy)methane ND ug/kg 1 08/02/11 19:06 111-91-107/29/11 08:30455106
bis(2-Chloroethyl) ether ND ug/kg 1 08/02/11 19:06 111-44-407/29/11 08:30455116
bis(2-Chloroisopropyl) ether ND ug/kg 1 08/02/11 19:06 108-60-107/29/11 08:30455121
2-Chloronaphthalene ND ug/kg 1 08/02/11 19:06 91-58-707/29/11 08:3045589.7
2-Chlorophenol ND ug/kg 1 08/02/11 19:06 95-57-807/29/11 08:30455124
4-Chlorophenylphenyl ether ND ug/kg 1 08/02/11 19:06 7005-72-307/29/11 08:3045593.8
Chrysene ND ug/kg 1 08/02/11 19:06 218-01-907/29/11 08:3045560.7
Dibenz(a,h)anthracene ND ug/kg 1 08/02/11 19:06 53-70-307/29/11 08:3045596.6
Dibenzofuran ND ug/kg 1 08/02/11 19:06 132-64-907/29/11 08:3045574.5
1,2-Dichlorobenzene ND ug/kg 1 08/02/11 19:06 95-50-107/29/11 08:30455121
1,3-Dichlorobenzene ND ug/kg 1 08/02/11 19:06 541-73-107/29/11 08:30455104
1,4-Dichlorobenzene ND ug/kg 1 08/02/11 19:06 106-46-707/29/11 08:30455128
3,3'-Dichlorobenzidine ND ug/kg 1 08/02/11 19:06 91-94-107/29/11 08:30228099.4
2,4-Dichlorophenol ND ug/kg 1 08/02/11 19:06 120-83-207/29/11 08:3045599.4
Diethylphthalate ND ug/kg 1 08/02/11 19:06 84-66-207/29/11 08:3045570.4
2,4-Dimethylphenol ND ug/kg 1 08/02/11 19:06 105-67-907/29/11 08:30455179
Dimethylphthalate ND ug/kg 1 08/02/11 19:06 131-11-307/29/11 08:3045592.5
Di-n-butylphthalate ND ug/kg 1 08/02/11 19:06 84-74-207/29/11 08:3045574.5
4,6-Dinitro-2-methylphenol ND ug/kg 1 08/02/11 19:06 534-52-107/29/11 08:3091191.1
2,4-Dinitrophenol ND ug/kg 1 08/02/11 19:06 51-28-507/29/11 08:30228074.5
2,4-Dinitrotoluene ND ug/kg 1 08/02/11 19:06 121-14-207/29/11 08:3045585.6
2,6-Dinitrotoluene ND ug/kg 1 08/02/11 19:06 606-20-207/29/11 08:3045595.2
Di-n-octylphthalate ND ug/kg 1 08/02/11 19:06 117-84-007/29/11 08:3045595.2
bis(2-Ethylhexyl)phthalate ND ug/kg 1 08/02/11 19:06 117-81-707/29/11 08:30455124
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 28 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-17 Lab ID:9299254017 Collected:07/27/11 13:55 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Fluoranthene ND ug/kg 1 08/02/11 19:06 206-44-007/29/11 08:3045566.2
Fluorene ND ug/kg 1 08/02/11 19:06 86-73-707/29/11 08:3045593.8
Hexachloro-1,3-butadiene ND ug/kg 1 08/02/11 19:06 87-68-307/29/11 08:3045578.7
Hexachlorobenzene ND ug/kg 1 08/02/11 19:06 118-74-107/29/11 08:3045558.0
Hexachlorocyclopentadiene ND ug/kg 1 08/02/11 19:06 77-47-407/29/11 08:3045584.2
Hexachloroethane ND ug/kg 1 08/02/11 19:06 67-72-107/29/11 08:30455120
Indeno(1,2,3-cd)pyrene ND ug/kg 1 08/02/11 19:06 193-39-507/29/11 08:3045593.8
Isophorone ND ug/kg 1 08/02/11 19:06 78-59-107/29/11 08:30455102
1-Methylnaphthalene ND ug/kg 1 08/02/11 19:06 90-12-007/29/11 08:30455119
2-Methylnaphthalene ND ug/kg 1 08/02/11 19:06 91-57-607/29/11 08:3045598.0
2-Methylphenol(o-Cresol)ND ug/kg 1 08/02/11 19:06 95-48-707/29/11 08:30455138
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 08/02/11 19:0607/29/11 08:30455179
Naphthalene ND ug/kg 1 08/02/11 19:06 91-20-307/29/11 08:30455112
2-Nitroaniline ND ug/kg 1 08/02/11 19:06 88-74-407/29/11 08:302280141
3-Nitroaniline ND ug/kg 1 08/02/11 19:06 99-09-207/29/11 08:302280124
4-Nitroaniline ND ug/kg 1 08/02/11 19:06 100-01-607/29/11 08:30911128
Nitrobenzene ND ug/kg 1 08/02/11 19:06 98-95-307/29/11 08:30455124
2-Nitrophenol ND ug/kg 1 08/02/11 19:06 88-75-507/29/11 08:30455110
4-Nitrophenol ND ug/kg 1 08/02/11 19:06 100-02-707/29/11 08:30228081.4
N-Nitrosodimethylamine ND ug/kg 1 08/02/11 19:06 62-75-907/29/11 08:30455148
N-Nitroso-di-n-propylamine ND ug/kg 1 08/02/11 19:06 621-64-707/29/11 08:3045586.9
N-Nitrosodiphenylamine ND ug/kg 1 08/02/11 19:06 86-30-607/29/11 08:30455135
Pentachlorophenol ND ug/kg 1 08/02/11 19:06 87-86-507/29/11 08:30228082.8
Phenanthrene ND ug/kg 1 08/02/11 19:06 85-01-807/29/11 08:3045575.9
Phenol ND ug/kg 1 08/02/11 19:06 108-95-207/29/11 08:30455137
Pyrene ND ug/kg 1 08/02/11 19:06 129-00-007/29/11 08:3045577.3
1,2,4-Trichlorobenzene ND ug/kg 1 08/02/11 19:06 120-82-107/29/11 08:3045588.3
2,4,5-Trichlorophenol ND ug/kg 1 08/02/11 19:06 95-95-407/29/11 08:30455141
2,4,6-Trichlorophenol ND ug/kg 1 08/02/11 19:06 88-06-207/29/11 08:30455101
Nitrobenzene-d5 (S)52 %1 08/02/11 19:06 4165-60-007/29/11 08:3023-110
2-Fluorobiphenyl (S)55 %1 08/02/11 19:06 321-60-807/29/11 08:3030-110
Terphenyl-d14 (S)59 %1 08/02/11 19:06 1718-51-007/29/11 08:3028-110
Phenol-d6 (S)50 %1 08/02/11 19:06 13127-88-307/29/11 08:3022-110
2-Fluorophenol (S)52 %1 08/02/11 19:06 367-12-407/29/11 08:3013-110
2,4,6-Tribromophenol (S)67 %1 08/02/11 19:06 118-79-607/29/11 08:3027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/29/11 19:44 67-64-110910.9
Benzene ND ug/kg 1 07/29/11 19:44 71-43-25.5 1.7
Bromobenzene ND ug/kg 1 07/29/11 19:44 108-86-15.5 2.2
Bromochloromethane ND ug/kg 1 07/29/11 19:44 74-97-55.5 1.9
Bromodichloromethane ND ug/kg 1 07/29/11 19:44 75-27-45.5 2.1
Bromoform ND ug/kg 1 07/29/11 19:44 75-25-25.5 2.5
Bromomethane ND ug/kg 1 07/29/11 19:44 74-83-910.9 2.7
2-Butanone (MEK)ND ug/kg 1 07/29/11 19:44 78-93-31093.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 29 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-17 Lab ID:9299254017 Collected:07/27/11 13:55 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
n-Butylbenzene ND ug/kg 1 07/29/11 19:44 104-51-85.5 2.0
sec-Butylbenzene ND ug/kg 1 07/29/11 19:44 135-98-85.5 1.7
tert-Butylbenzene ND ug/kg 1 07/29/11 19:44 98-06-65.5 2.2
Carbon tetrachloride ND ug/kg 1 07/29/11 19:44 56-23-55.5 2.8
Chlorobenzene ND ug/kg 1 07/29/11 19:44 108-90-75.5 2.1
Chloroethane ND ug/kg 1 07/29/11 19:44 75-00-310.9 2.6
Chloroform ND ug/kg 1 07/29/11 19:44 67-66-35.5 1.7
Chloromethane ND ug/kg 1 07/29/11 19:44 74-87-310.9 2.6
2-Chlorotoluene ND ug/kg 1 07/29/11 19:44 95-49-85.5 1.9
4-Chlorotoluene ND ug/kg 1 07/29/11 19:44 106-43-45.5 2.0
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/29/11 19:44 96-12-85.5 3.9
Dibromochloromethane ND ug/kg 1 07/29/11 19:44 124-48-15.5 2.0
1,2-Dibromoethane (EDB)ND ug/kg 1 07/29/11 19:44 106-93-45.5 2.0
Dibromomethane ND ug/kg 1 07/29/11 19:44 74-95-35.5 2.7
1,2-Dichlorobenzene ND ug/kg 1 07/29/11 19:44 95-50-15.5 2.1
1,3-Dichlorobenzene ND ug/kg 1 07/29/11 19:44 541-73-15.5 2.2
1,4-Dichlorobenzene ND ug/kg 1 07/29/11 19:44 106-46-75.5 1.9
Dichlorodifluoromethane ND ug/kg 1 07/29/11 19:44 75-71-810.9 3.9
1,1-Dichloroethane ND ug/kg 1 07/29/11 19:44 75-34-35.5 1.6
1,2-Dichloroethane ND ug/kg 1 07/29/11 19:44 107-06-25.5 2.4
1,1-Dichloroethene ND ug/kg 1 07/29/11 19:44 75-35-45.5 2.0
cis-1,2-Dichloroethene ND ug/kg 1 07/29/11 19:44 156-59-25.5 1.5
trans-1,2-Dichloroethene ND ug/kg 1 07/29/11 19:44 156-60-55.5 2.1
1,2-Dichloropropane ND ug/kg 1 07/29/11 19:44 78-87-55.5 1.9
1,3-Dichloropropane ND ug/kg 1 07/29/11 19:44 142-28-95.5 2.1
2,2-Dichloropropane ND ug/kg 1 07/29/11 19:44 594-20-75.5 1.9
1,1-Dichloropropene ND ug/kg 1 07/29/11 19:44 563-58-65.5 1.6
cis-1,3-Dichloropropene ND ug/kg 1 07/29/11 19:44 10061-01-55.5 2.0
trans-1,3-Dichloropropene ND ug/kg 1 07/29/11 19:44 10061-02-65.5 1.6
Diisopropyl ether ND ug/kg 1 07/29/11 19:44 108-20-35.5 1.9
Ethylbenzene ND ug/kg 1 07/29/11 19:44 100-41-45.5 2.0
Hexachloro-1,3-butadiene ND ug/kg 1 07/29/11 19:44 87-68-35.5 2.2
2-Hexanone ND ug/kg 1 07/29/11 19:44 591-78-654.7 4.3
Isopropylbenzene (Cumene)ND ug/kg 1 07/29/11 19:44 98-82-85.5 2.1
p-Isopropyltoluene ND ug/kg 1 07/29/11 19:44 99-87-65.5 1.9
Methylene Chloride ND ug/kg 1 07/29/11 19:44 75-09-221.9 3.3
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/29/11 19:44 108-10-154.7 4.0
Methyl-tert-butyl ether ND ug/kg 1 07/29/11 19:44 1634-04-45.5 1.6
Naphthalene ND ug/kg 1 07/29/11 19:44 91-20-35.5 1.3
n-Propylbenzene ND ug/kg 1 07/29/11 19:44 103-65-15.5 1.9
Styrene ND ug/kg 1 07/29/11 19:44 100-42-55.5 2.0
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/29/11 19:44 630-20-65.5 2.3
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/29/11 19:44 79-34-55.5 2.1
Tetrachloroethene ND ug/kg 1 07/29/11 19:44 127-18-45.5 1.9
Toluene ND ug/kg 1 07/29/11 19:44 108-88-35.5 2.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 30 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-17 Lab ID:9299254017 Collected:07/27/11 13:55 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2,3-Trichlorobenzene ND ug/kg 1 07/29/11 19:44 87-61-65.5 2.4
1,2,4-Trichlorobenzene ND ug/kg 1 07/29/11 19:44 120-82-15.5 1.7
1,1,1-Trichloroethane ND ug/kg 1 07/29/11 19:44 71-55-65.5 2.0
1,1,2-Trichloroethane ND ug/kg 1 07/29/11 19:44 79-00-55.5 2.3
Trichloroethene ND ug/kg 1 07/29/11 19:44 79-01-65.5 2.3
Trichlorofluoromethane ND ug/kg 1 07/29/11 19:44 75-69-45.5 2.4
1,2,3-Trichloropropane ND ug/kg 1 07/29/11 19:44 96-18-45.5 1.7
1,2,4-Trimethylbenzene ND ug/kg 1 07/29/11 19:44 95-63-65.5 2.2
1,3,5-Trimethylbenzene ND ug/kg 1 07/29/11 19:44 108-67-85.5 2.0
Vinyl acetate ND ug/kg 1 07/29/11 19:44 108-05-454.7 9.6
Vinyl chloride ND ug/kg 1 07/29/11 19:44 75-01-410.9 2.0
Xylene (Total)ND ug/kg 1 07/29/11 19:44 1330-20-710.9 3.9
m&p-Xylene ND ug/kg 1 07/29/11 19:44 179601-23-110.9 3.9
o-Xylene ND ug/kg 1 07/29/11 19:44 95-47-65.5 2.1
Dibromofluoromethane (S)104 %1 07/29/11 19:44 1868-53-770-130
Toluene-d8 (S)104 %1 07/29/11 19:44 2037-26-570-130
4-Bromofluorobenzene (S)90 %1 07/29/11 19:44 460-00-470-130
1,2-Dichloroethane-d4 (S)93 %1 07/29/11 19:44 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 27.5 %1 07/29/11 14:530.10 0.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 35.0 mg/kg 1 08/04/11 15:44 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/02/11 16:24 18540-29-9 N208/02/11 12:402.3 0.23
Sample:SB-18 Lab ID:9299254018 Collected:07/27/11 14:05 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 08/02/11 18:19 7440-36-008/02/11 09:000.58 0.33
Arsenic 1.1 mg/kg 1 08/02/11 18:19 7440-38-208/02/11 09:000.58 0.37
Beryllium 0.58 mg/kg 1 08/02/11 18:19 7440-41-708/02/11 09:000.12 0.023
Cadmium 3.1 mg/kg 1 08/02/11 18:19 7440-43-908/02/11 09:000.12 0.070
Chromium 45.2 mg/kg 1 08/02/11 18:19 7440-47-308/02/11 09:000.58 0.035
Copper 48.8 mg/kg 1 08/02/11 18:19 7440-50-808/02/11 09:000.58 0.047
Lead 18.3 mg/kg 1 08/02/11 18:19 7439-92-108/02/11 09:000.58 0.56
Manganese 532 mg/kg 1 08/02/11 18:19 7439-96-508/02/11 09:000.58 0.035
Nickel 13.0 mg/kg 1 08/02/11 18:19 7440-02-008/02/11 09:000.58 0.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 31 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-18 Lab ID:9299254018 Collected:07/27/11 14:05 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Selenium 0.98J mg/kg 1 08/02/11 18:19 7782-49-208/02/11 09:001.2 0.44
Silver 0.092J mg/kg 1 08/02/11 18:19 7440-22-408/02/11 09:000.58 0.035
Thallium ND mg/kg 1 08/02/11 18:19 7440-28-008/02/11 09:001.2 0.30
Zinc 36.8 mg/kg 1 08/02/11 18:19 7440-66-608/02/11 09:001.2 0.30
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.078 mg/kg 1 08/02/11 15:16 7439-97-608/01/11 14:150.0061 0.00012
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 08/02/11 19:34 83-32-907/29/11 08:3041695.9
Acenaphthylene ND ug/kg 1 08/02/11 19:34 208-96-807/29/11 08:3041698.4
Aniline ND ug/kg 1 08/02/11 19:34 62-53-307/29/11 08:30416112
Anthracene ND ug/kg 1 08/02/11 19:34 120-12-707/29/11 08:3041693.4
Benzo(a)anthracene ND ug/kg 1 08/02/11 19:34 56-55-307/29/11 08:3041677.0
Benzo(a)pyrene ND ug/kg 1 08/02/11 19:34 50-32-807/29/11 08:3041679.5
Benzo(b)fluoranthene ND ug/kg 1 08/02/11 19:34 205-99-207/29/11 08:3041671.9
Benzo(g,h,i)perylene ND ug/kg 1 08/02/11 19:34 191-24-207/29/11 08:30416106
Benzo(k)fluoranthene ND ug/kg 1 08/02/11 19:34 207-08-907/29/11 08:3041682.0
Benzoic Acid ND ug/kg 1 08/02/11 19:34 65-85-007/29/11 08:30208075.7
Benzyl alcohol ND ug/kg 1 08/02/11 19:34 100-51-607/29/11 08:3083383.3
4-Bromophenylphenyl ether ND ug/kg 1 08/02/11 19:34 101-55-307/29/11 08:3041675.7
Butylbenzylphthalate ND ug/kg 1 08/02/11 19:34 85-68-707/29/11 08:3041688.3
4-Chloro-3-methylphenol ND ug/kg 1 08/02/11 19:34 59-50-707/29/11 08:3083385.8
4-Chloroaniline ND ug/kg 1 08/02/11 19:34 106-47-807/29/11 08:302080116
bis(2-Chloroethoxy)methane ND ug/kg 1 08/02/11 19:34 111-91-107/29/11 08:3041697.2
bis(2-Chloroethyl) ether ND ug/kg 1 08/02/11 19:34 111-44-407/29/11 08:30416106
bis(2-Chloroisopropyl) ether ND ug/kg 1 08/02/11 19:34 108-60-107/29/11 08:30416111
2-Chloronaphthalene ND ug/kg 1 08/02/11 19:34 91-58-707/29/11 08:3041682.0
2-Chlorophenol ND ug/kg 1 08/02/11 19:34 95-57-807/29/11 08:30416114
4-Chlorophenylphenyl ether ND ug/kg 1 08/02/11 19:34 7005-72-307/29/11 08:3041685.8
Chrysene ND ug/kg 1 08/02/11 19:34 218-01-907/29/11 08:3041655.5
Dibenz(a,h)anthracene ND ug/kg 1 08/02/11 19:34 53-70-307/29/11 08:3041688.3
Dibenzofuran ND ug/kg 1 08/02/11 19:34 132-64-907/29/11 08:3041668.1
1,2-Dichlorobenzene ND ug/kg 1 08/02/11 19:34 95-50-107/29/11 08:30416111
1,3-Dichlorobenzene ND ug/kg 1 08/02/11 19:34 541-73-107/29/11 08:3041694.6
1,4-Dichlorobenzene ND ug/kg 1 08/02/11 19:34 106-46-707/29/11 08:30416117
3,3'-Dichlorobenzidine ND ug/kg 1 08/02/11 19:34 91-94-107/29/11 08:30208090.9
2,4-Dichlorophenol ND ug/kg 1 08/02/11 19:34 120-83-207/29/11 08:3041690.9
Diethylphthalate ND ug/kg 1 08/02/11 19:34 84-66-207/29/11 08:3041664.4
2,4-Dimethylphenol ND ug/kg 1 08/02/11 19:34 105-67-907/29/11 08:30416164
Dimethylphthalate ND ug/kg 1 08/02/11 19:34 131-11-307/29/11 08:3041684.6
Di-n-butylphthalate ND ug/kg 1 08/02/11 19:34 84-74-207/29/11 08:3041668.1
4,6-Dinitro-2-methylphenol ND ug/kg 1 08/02/11 19:34 534-52-107/29/11 08:3083383.3
2,4-Dinitrophenol ND ug/kg 1 08/02/11 19:34 51-28-507/29/11 08:30208068.1
2,4-Dinitrotoluene ND ug/kg 1 08/02/11 19:34 121-14-207/29/11 08:3041678.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 32 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-18 Lab ID:9299254018 Collected:07/27/11 14:05 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,6-Dinitrotoluene ND ug/kg 1 08/02/11 19:34 606-20-207/29/11 08:3041687.1
Di-n-octylphthalate ND ug/kg 1 08/02/11 19:34 117-84-007/29/11 08:3041687.1
bis(2-Ethylhexyl)phthalate ND ug/kg 1 08/02/11 19:34 117-81-707/29/11 08:30416114
Fluoranthene ND ug/kg 1 08/02/11 19:34 206-44-007/29/11 08:3041660.6
Fluorene ND ug/kg 1 08/02/11 19:34 86-73-707/29/11 08:3041685.8
Hexachloro-1,3-butadiene ND ug/kg 1 08/02/11 19:34 87-68-307/29/11 08:3041671.9
Hexachlorobenzene ND ug/kg 1 08/02/11 19:34 118-74-107/29/11 08:3041653.0
Hexachlorocyclopentadiene ND ug/kg 1 08/02/11 19:34 77-47-407/29/11 08:3041677.0
Hexachloroethane ND ug/kg 1 08/02/11 19:34 67-72-107/29/11 08:30416110
Indeno(1,2,3-cd)pyrene ND ug/kg 1 08/02/11 19:34 193-39-507/29/11 08:3041685.8
Isophorone ND ug/kg 1 08/02/11 19:34 78-59-107/29/11 08:3041693.4
1-Methylnaphthalene ND ug/kg 1 08/02/11 19:34 90-12-007/29/11 08:30416109
2-Methylnaphthalene ND ug/kg 1 08/02/11 19:34 91-57-607/29/11 08:3041689.6
2-Methylphenol(o-Cresol)ND ug/kg 1 08/02/11 19:34 95-48-707/29/11 08:30416126
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 08/02/11 19:3407/29/11 08:30416164
Naphthalene ND ug/kg 1 08/02/11 19:34 91-20-307/29/11 08:30416102
2-Nitroaniline ND ug/kg 1 08/02/11 19:34 88-74-407/29/11 08:302080129
3-Nitroaniline ND ug/kg 1 08/02/11 19:34 99-09-207/29/11 08:302080114
4-Nitroaniline ND ug/kg 1 08/02/11 19:34 100-01-607/29/11 08:30833117
Nitrobenzene ND ug/kg 1 08/02/11 19:34 98-95-307/29/11 08:30416114
2-Nitrophenol ND ug/kg 1 08/02/11 19:34 88-75-507/29/11 08:30416101
4-Nitrophenol ND ug/kg 1 08/02/11 19:34 100-02-707/29/11 08:30208074.5
N-Nitrosodimethylamine ND ug/kg 1 08/02/11 19:34 62-75-907/29/11 08:30416135
N-Nitroso-di-n-propylamine ND ug/kg 1 08/02/11 19:34 621-64-707/29/11 08:3041679.5
N-Nitrosodiphenylamine ND ug/kg 1 08/02/11 19:34 86-30-607/29/11 08:30416124
Pentachlorophenol ND ug/kg 1 08/02/11 19:34 87-86-507/29/11 08:30208075.7
Phenanthrene ND ug/kg 1 08/02/11 19:34 85-01-807/29/11 08:3041669.4
Phenol ND ug/kg 1 08/02/11 19:34 108-95-207/29/11 08:30416125
Pyrene ND ug/kg 1 08/02/11 19:34 129-00-007/29/11 08:3041670.7
1,2,4-Trichlorobenzene ND ug/kg 1 08/02/11 19:34 120-82-107/29/11 08:3041680.8
2,4,5-Trichlorophenol ND ug/kg 1 08/02/11 19:34 95-95-407/29/11 08:30416129
2,4,6-Trichlorophenol ND ug/kg 1 08/02/11 19:34 88-06-207/29/11 08:3041692.1
Nitrobenzene-d5 (S)40 %1 08/02/11 19:34 4165-60-007/29/11 08:3023-110
2-Fluorobiphenyl (S)49 %1 08/02/11 19:34 321-60-807/29/11 08:3030-110
Terphenyl-d14 (S)60 %1 08/02/11 19:34 1718-51-007/29/11 08:3028-110
Phenol-d6 (S)47 %1 08/02/11 19:34 13127-88-307/29/11 08:3022-110
2-Fluorophenol (S)43 %1 08/02/11 19:34 367-12-407/29/11 08:3013-110
2,4,6-Tribromophenol (S)62 %1 08/02/11 19:34 118-79-607/29/11 08:3027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/29/11 20:04 67-64-190.8 9.1
Benzene 3.9J ug/kg 1 07/29/11 20:04 71-43-24.5 1.5
Bromobenzene ND ug/kg 1 07/29/11 20:04 108-86-14.5 1.8
Bromochloromethane ND ug/kg 1 07/29/11 20:04 74-97-54.5 1.5
Bromodichloromethane ND ug/kg 1 07/29/11 20:04 75-27-44.5 1.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 33 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-18 Lab ID:9299254018 Collected:07/27/11 14:05 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromoform ND ug/kg 1 07/29/11 20:04 75-25-24.5 2.1
Bromomethane ND ug/kg 1 07/29/11 20:04 74-83-99.1 2.3
2-Butanone (MEK)ND ug/kg 1 07/29/11 20:04 78-93-390.8 2.6
n-Butylbenzene ND ug/kg 1 07/29/11 20:04 104-51-84.5 1.6
sec-Butylbenzene ND ug/kg 1 07/29/11 20:04 135-98-84.5 1.5
tert-Butylbenzene 9.9 ug/kg 1 07/29/11 20:04 98-06-64.5 1.8
Carbon tetrachloride ND ug/kg 1 07/29/11 20:04 56-23-54.5 2.4
Chlorobenzene ND ug/kg 1 07/29/11 20:04 108-90-74.5 1.7
Chloroethane ND ug/kg 1 07/29/11 20:04 75-00-39.1 2.2
Chloroform ND ug/kg 1 07/29/11 20:04 67-66-34.5 1.5
Chloromethane ND ug/kg 1 07/29/11 20:04 74-87-39.1 2.2
2-Chlorotoluene ND ug/kg 1 07/29/11 20:04 95-49-84.5 1.5
4-Chlorotoluene ND ug/kg 1 07/29/11 20:04 106-43-44.5 1.6
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/29/11 20:04 96-12-84.5 3.3
Dibromochloromethane ND ug/kg 1 07/29/11 20:04 124-48-14.5 1.6
1,2-Dibromoethane (EDB)ND ug/kg 1 07/29/11 20:04 106-93-44.5 1.6
Dibromomethane ND ug/kg 1 07/29/11 20:04 74-95-34.5 2.3
1,2-Dichlorobenzene ND ug/kg 1 07/29/11 20:04 95-50-14.5 1.7
1,3-Dichlorobenzene ND ug/kg 1 07/29/11 20:04 541-73-14.5 1.8
1,4-Dichlorobenzene ND ug/kg 1 07/29/11 20:04 106-46-74.5 1.5
Dichlorodifluoromethane ND ug/kg 1 07/29/11 20:04 75-71-89.1 3.3
1,1-Dichloroethane ND ug/kg 1 07/29/11 20:04 75-34-34.5 1.4
1,2-Dichloroethane ND ug/kg 1 07/29/11 20:04 107-06-24.5 2.0
1,1-Dichloroethene ND ug/kg 1 07/29/11 20:04 75-35-44.5 1.6
cis-1,2-Dichloroethene ND ug/kg 1 07/29/11 20:04 156-59-24.5 1.3
trans-1,2-Dichloroethene ND ug/kg 1 07/29/11 20:04 156-60-54.5 1.7
1,2-Dichloropropane ND ug/kg 1 07/29/11 20:04 78-87-54.5 1.5
1,3-Dichloropropane ND ug/kg 1 07/29/11 20:04 142-28-94.5 1.7
2,2-Dichloropropane ND ug/kg 1 07/29/11 20:04 594-20-74.5 1.5
1,1-Dichloropropene ND ug/kg 1 07/29/11 20:04 563-58-64.5 1.4
cis-1,3-Dichloropropene ND ug/kg 1 07/29/11 20:04 10061-01-54.5 1.6
trans-1,3-Dichloropropene ND ug/kg 1 07/29/11 20:04 10061-02-64.5 1.4
Diisopropyl ether ND ug/kg 1 07/29/11 20:04 108-20-34.5 1.5
Ethylbenzene ND ug/kg 1 07/29/11 20:04 100-41-44.5 1.6
Hexachloro-1,3-butadiene ND ug/kg 1 07/29/11 20:04 87-68-34.5 1.8
2-Hexanone ND ug/kg 1 07/29/11 20:04 591-78-645.4 3.5
Isopropylbenzene (Cumene)ND ug/kg 1 07/29/11 20:04 98-82-84.5 1.7
p-Isopropyltoluene ND ug/kg 1 07/29/11 20:04 99-87-64.5 1.5
Methylene Chloride ND ug/kg 1 07/29/11 20:04 75-09-218.2 2.7
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/29/11 20:04 108-10-145.4 3.4
Methyl-tert-butyl ether ND ug/kg 1 07/29/11 20:04 1634-04-44.5 1.4
Naphthalene ND ug/kg 1 07/29/11 20:04 91-20-34.5 1.1
n-Propylbenzene ND ug/kg 1 07/29/11 20:04 103-65-14.5 1.5
Styrene ND ug/kg 1 07/29/11 20:04 100-42-54.5 1.6
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/29/11 20:04 630-20-64.5 1.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 34 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-18 Lab ID:9299254018 Collected:07/27/11 14:05 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/29/11 20:04 79-34-54.5 1.7
Tetrachloroethene ND ug/kg 1 07/29/11 20:04 127-18-44.5 1.5
Toluene ND ug/kg 1 07/29/11 20:04 108-88-34.5 1.6
1,2,3-Trichlorobenzene ND ug/kg 1 07/29/11 20:04 87-61-64.5 2.0
1,2,4-Trichlorobenzene ND ug/kg 1 07/29/11 20:04 120-82-14.5 1.5
1,1,1-Trichloroethane ND ug/kg 1 07/29/11 20:04 71-55-64.5 1.6
1,1,2-Trichloroethane ND ug/kg 1 07/29/11 20:04 79-00-54.5 1.9
Trichloroethene ND ug/kg 1 07/29/11 20:04 79-01-64.5 1.9
Trichlorofluoromethane ND ug/kg 1 07/29/11 20:04 75-69-44.5 2.0
1,2,3-Trichloropropane ND ug/kg 1 07/29/11 20:04 96-18-44.5 1.5
1,2,4-Trimethylbenzene ND ug/kg 1 07/29/11 20:04 95-63-64.5 1.8
1,3,5-Trimethylbenzene ND ug/kg 1 07/29/11 20:04 108-67-84.5 1.6
Vinyl acetate ND ug/kg 1 07/29/11 20:04 108-05-445.4 8.0
Vinyl chloride ND ug/kg 1 07/29/11 20:04 75-01-49.1 1.6
Xylene (Total)ND ug/kg 1 07/29/11 20:04 1330-20-79.1 3.3
m&p-Xylene ND ug/kg 1 07/29/11 20:04 179601-23-19.1 3.3
o-Xylene ND ug/kg 1 07/29/11 20:04 95-47-64.5 1.7
Dibromofluoromethane (S)106 %1 07/29/11 20:04 1868-53-770-130
Toluene-d8 (S)109 %1 07/29/11 20:04 2037-26-570-130
4-Bromofluorobenzene (S)92 %1 07/29/11 20:04 460-00-470-130
1,2-Dichloroethane-d4 (S)103 %1 07/29/11 20:04 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 20.8 %1 07/29/11 14:530.10 0.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 45.2 mg/kg 1 08/04/11 15:44 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/02/11 16:24 18540-29-9 N208/02/11 12:402.6 0.26
Sample:SB-19 Lab ID:9299254019 Collected:07/27/11 14:40 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 08/02/11 18:23 7440-36-008/02/11 09:000.50 0.28
Arsenic 0.88 mg/kg 1 08/02/11 18:23 7440-38-208/02/11 09:000.50 0.32
Beryllium 0.41 mg/kg 1 08/02/11 18:23 7440-41-708/02/11 09:000.099 0.020
Cadmium 0.96 mg/kg 1 08/02/11 18:23 7440-43-908/02/11 09:000.099 0.060
Chromium 24.2 mg/kg 1 08/02/11 18:23 7440-47-308/02/11 09:000.50 0.030
Copper 29.4 mg/kg 1 08/02/11 18:23 7440-50-808/02/11 09:000.50 0.040
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 35 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-19 Lab ID:9299254019 Collected:07/27/11 14:40 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Lead 15.0 mg/kg 1 08/02/11 18:23 7439-92-108/02/11 09:000.50 0.48
Manganese 298 mg/kg 1 08/02/11 18:23 7439-96-508/02/11 09:000.50 0.030
Nickel 11.9 mg/kg 1 08/02/11 18:23 7440-02-008/02/11 09:000.50 0.18
Selenium ND mg/kg 1 08/02/11 18:23 7782-49-208/02/11 09:000.99 0.38
Silver ND mg/kg 1 08/02/11 18:23 7440-22-408/02/11 09:000.50 0.030
Thallium 0.40J mg/kg 1 08/02/11 18:23 7440-28-008/02/11 09:000.99 0.26
Zinc 37.7 mg/kg 1 08/02/11 18:23 7440-66-608/02/11 09:000.99 0.26
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.016 mg/kg 1 08/02/11 15:19 7439-97-608/01/11 14:150.0043 0.000086
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 08/02/11 20:01 83-32-907/29/11 08:3034178.4
Acenaphthylene ND ug/kg 1 08/02/11 20:01 208-96-807/29/11 08:3034180.5
Aniline ND ug/kg 1 08/02/11 20:01 62-53-307/29/11 08:3034191.8
Anthracene ND ug/kg 1 08/02/11 20:01 120-12-707/29/11 08:3034176.4
Benzo(a)anthracene ND ug/kg 1 08/02/11 20:01 56-55-307/29/11 08:3034163.0
Benzo(a)pyrene ND ug/kg 1 08/02/11 20:01 50-32-807/29/11 08:3034165.0
Benzo(b)fluoranthene ND ug/kg 1 08/02/11 20:01 205-99-207/29/11 08:3034158.8
Benzo(g,h,i)perylene ND ug/kg 1 08/02/11 20:01 191-24-207/29/11 08:3034186.7
Benzo(k)fluoranthene ND ug/kg 1 08/02/11 20:01 207-08-907/29/11 08:3034167.1
Benzoic Acid ND ug/kg 1 08/02/11 20:01 65-85-007/29/11 08:30170061.9
Benzyl alcohol ND ug/kg 1 08/02/11 20:01 100-51-607/29/11 08:3068168.1
4-Bromophenylphenyl ether ND ug/kg 1 08/02/11 20:01 101-55-307/29/11 08:3034161.9
Butylbenzylphthalate ND ug/kg 1 08/02/11 20:01 85-68-707/29/11 08:3034172.2
4-Chloro-3-methylphenol ND ug/kg 1 08/02/11 20:01 59-50-707/29/11 08:3068170.2
4-Chloroaniline ND ug/kg 1 08/02/11 20:01 106-47-807/29/11 08:30170094.9
bis(2-Chloroethoxy)methane ND ug/kg 1 08/02/11 20:01 111-91-107/29/11 08:3034179.5
bis(2-Chloroethyl) ether ND ug/kg 1 08/02/11 20:01 111-44-407/29/11 08:3034186.7
bis(2-Chloroisopropyl) ether ND ug/kg 1 08/02/11 20:01 108-60-107/29/11 08:3034190.8
2-Chloronaphthalene ND ug/kg 1 08/02/11 20:01 91-58-707/29/11 08:3034167.1
2-Chlorophenol ND ug/kg 1 08/02/11 20:01 95-57-807/29/11 08:3034192.9
4-Chlorophenylphenyl ether ND ug/kg 1 08/02/11 20:01 7005-72-307/29/11 08:3034170.2
Chrysene ND ug/kg 1 08/02/11 20:01 218-01-907/29/11 08:3034145.4
Dibenz(a,h)anthracene ND ug/kg 1 08/02/11 20:01 53-70-307/29/11 08:3034172.2
Dibenzofuran ND ug/kg 1 08/02/11 20:01 132-64-907/29/11 08:3034155.7
1,2-Dichlorobenzene ND ug/kg 1 08/02/11 20:01 95-50-107/29/11 08:3034190.8
1,3-Dichlorobenzene ND ug/kg 1 08/02/11 20:01 541-73-107/29/11 08:3034177.4
1,4-Dichlorobenzene ND ug/kg 1 08/02/11 20:01 106-46-707/29/11 08:3034196.0
3,3'-Dichlorobenzidine ND ug/kg 1 08/02/11 20:01 91-94-107/29/11 08:30170074.3
2,4-Dichlorophenol ND ug/kg 1 08/02/11 20:01 120-83-207/29/11 08:3034174.3
Diethylphthalate ND ug/kg 1 08/02/11 20:01 84-66-207/29/11 08:3034152.6
2,4-Dimethylphenol ND ug/kg 1 08/02/11 20:01 105-67-907/29/11 08:30341134
Dimethylphthalate ND ug/kg 1 08/02/11 20:01 131-11-307/29/11 08:3034169.1
Di-n-butylphthalate ND ug/kg 1 08/02/11 20:01 84-74-207/29/11 08:3034155.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 36 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-19 Lab ID:9299254019 Collected:07/27/11 14:40 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
4,6-Dinitro-2-methylphenol ND ug/kg 1 08/02/11 20:01 534-52-107/29/11 08:3068168.1
2,4-Dinitrophenol ND ug/kg 1 08/02/11 20:01 51-28-507/29/11 08:30170055.7
2,4-Dinitrotoluene ND ug/kg 1 08/02/11 20:01 121-14-207/29/11 08:3034164.0
2,6-Dinitrotoluene ND ug/kg 1 08/02/11 20:01 606-20-207/29/11 08:3034171.2
Di-n-octylphthalate ND ug/kg 1 08/02/11 20:01 117-84-007/29/11 08:3034171.2
bis(2-Ethylhexyl)phthalate ND ug/kg 1 08/02/11 20:01 117-81-707/29/11 08:3034192.9
Fluoranthene ND ug/kg 1 08/02/11 20:01 206-44-007/29/11 08:3034149.5
Fluorene ND ug/kg 1 08/02/11 20:01 86-73-707/29/11 08:3034170.2
Hexachloro-1,3-butadiene ND ug/kg 1 08/02/11 20:01 87-68-307/29/11 08:3034158.8
Hexachlorobenzene ND ug/kg 1 08/02/11 20:01 118-74-107/29/11 08:3034143.3
Hexachlorocyclopentadiene ND ug/kg 1 08/02/11 20:01 77-47-407/29/11 08:3034163.0
Hexachloroethane ND ug/kg 1 08/02/11 20:01 67-72-107/29/11 08:3034189.8
Indeno(1,2,3-cd)pyrene ND ug/kg 1 08/02/11 20:01 193-39-507/29/11 08:3034170.2
Isophorone ND ug/kg 1 08/02/11 20:01 78-59-107/29/11 08:3034176.4
1-Methylnaphthalene ND ug/kg 1 08/02/11 20:01 90-12-007/29/11 08:3034188.8
2-Methylnaphthalene ND ug/kg 1 08/02/11 20:01 91-57-607/29/11 08:3034173.3
2-Methylphenol(o-Cresol)ND ug/kg 1 08/02/11 20:01 95-48-707/29/11 08:30341103
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 08/02/11 20:0107/29/11 08:30341134
Naphthalene ND ug/kg 1 08/02/11 20:01 91-20-307/29/11 08:3034183.6
2-Nitroaniline ND ug/kg 1 08/02/11 20:01 88-74-407/29/11 08:301700105
3-Nitroaniline ND ug/kg 1 08/02/11 20:01 99-09-207/29/11 08:30170092.9
4-Nitroaniline ND ug/kg 1 08/02/11 20:01 100-01-607/29/11 08:3068196.0
Nitrobenzene ND ug/kg 1 08/02/11 20:01 98-95-307/29/11 08:3034192.9
2-Nitrophenol ND ug/kg 1 08/02/11 20:01 88-75-507/29/11 08:3034182.6
4-Nitrophenol ND ug/kg 1 08/02/11 20:01 100-02-707/29/11 08:30170060.9
N-Nitrosodimethylamine ND ug/kg 1 08/02/11 20:01 62-75-907/29/11 08:30341110
N-Nitroso-di-n-propylamine ND ug/kg 1 08/02/11 20:01 621-64-707/29/11 08:3034165.0
N-Nitrosodiphenylamine ND ug/kg 1 08/02/11 20:01 86-30-607/29/11 08:30341101
Pentachlorophenol ND ug/kg 1 08/02/11 20:01 87-86-507/29/11 08:30170061.9
Phenanthrene ND ug/kg 1 08/02/11 20:01 85-01-807/29/11 08:3034156.8
Phenol ND ug/kg 1 08/02/11 20:01 108-95-207/29/11 08:30341102
Pyrene ND ug/kg 1 08/02/11 20:01 129-00-007/29/11 08:3034157.8
1,2,4-Trichlorobenzene ND ug/kg 1 08/02/11 20:01 120-82-107/29/11 08:3034166.0
2,4,5-Trichlorophenol ND ug/kg 1 08/02/11 20:01 95-95-407/29/11 08:30341105
2,4,6-Trichlorophenol ND ug/kg 1 08/02/11 20:01 88-06-207/29/11 08:3034175.3
Nitrobenzene-d5 (S)18 %1 08/02/11 20:01 4165-60-0 3g07/29/11 08:3023-110
2-Fluorobiphenyl (S)22 %1 08/02/11 20:01 321-60-8 3g07/29/11 08:3030-110
Terphenyl-d14 (S)26 %1 08/02/11 20:01 1718-51-0 3g07/29/11 08:3028-110
Phenol-d6 (S)18 %1 08/02/11 20:01 13127-88-3 3g07/29/11 08:3022-110
2-Fluorophenol (S)16 %1 08/02/11 20:01 367-12-407/29/11 08:3013-110
2,4,6-Tribromophenol (S)21 %1 08/02/11 20:01 118-79-6 3g07/29/11 08:3027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 9.9J ug/kg 1 07/29/11 20:24 67-64-182.6 8.3
Benzene ND ug/kg 1 07/29/11 20:24 71-43-24.1 1.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 37 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-19 Lab ID:9299254019 Collected:07/27/11 14:40 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene ND ug/kg 1 07/29/11 20:24 108-86-14.1 1.7
Bromochloromethane ND ug/kg 1 07/29/11 20:24 74-97-54.1 1.4
Bromodichloromethane ND ug/kg 1 07/29/11 20:24 75-27-44.1 1.6
Bromoform ND ug/kg 1 07/29/11 20:24 75-25-24.1 1.9
Bromomethane ND ug/kg 1 07/29/11 20:24 74-83-98.3 2.1
2-Butanone (MEK)ND ug/kg 1 07/29/11 20:24 78-93-382.6 2.4
n-Butylbenzene ND ug/kg 1 07/29/11 20:24 104-51-84.1 1.5
sec-Butylbenzene ND ug/kg 1 07/29/11 20:24 135-98-84.1 1.3
tert-Butylbenzene ND ug/kg 1 07/29/11 20:24 98-06-64.1 1.7
Carbon tetrachloride ND ug/kg 1 07/29/11 20:24 56-23-54.1 2.1
Chlorobenzene ND ug/kg 1 07/29/11 20:24 108-90-74.1 1.6
Chloroethane ND ug/kg 1 07/29/11 20:24 75-00-38.3 2.0
Chloroform ND ug/kg 1 07/29/11 20:24 67-66-34.1 1.3
Chloromethane ND ug/kg 1 07/29/11 20:24 74-87-38.3 2.0
2-Chlorotoluene ND ug/kg 1 07/29/11 20:24 95-49-84.1 1.4
4-Chlorotoluene ND ug/kg 1 07/29/11 20:24 106-43-44.1 1.5
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/29/11 20:24 96-12-84.1 3.0
Dibromochloromethane ND ug/kg 1 07/29/11 20:24 124-48-14.1 1.5
1,2-Dibromoethane (EDB)ND ug/kg 1 07/29/11 20:24 106-93-44.1 1.5
Dibromomethane ND ug/kg 1 07/29/11 20:24 74-95-34.1 2.1
1,2-Dichlorobenzene ND ug/kg 1 07/29/11 20:24 95-50-14.1 1.6
1,3-Dichlorobenzene ND ug/kg 1 07/29/11 20:24 541-73-14.1 1.7
1,4-Dichlorobenzene ND ug/kg 1 07/29/11 20:24 106-46-74.1 1.4
Dichlorodifluoromethane ND ug/kg 1 07/29/11 20:24 75-71-88.3 3.0
1,1-Dichloroethane ND ug/kg 1 07/29/11 20:24 75-34-34.1 1.2
1,2-Dichloroethane ND ug/kg 1 07/29/11 20:24 107-06-24.1 1.8
1,1-Dichloroethene ND ug/kg 1 07/29/11 20:24 75-35-44.1 1.5
cis-1,2-Dichloroethene ND ug/kg 1 07/29/11 20:24 156-59-24.1 1.2
trans-1,2-Dichloroethene ND ug/kg 1 07/29/11 20:24 156-60-54.1 1.6
1,2-Dichloropropane ND ug/kg 1 07/29/11 20:24 78-87-54.1 1.4
1,3-Dichloropropane ND ug/kg 1 07/29/11 20:24 142-28-94.1 1.6
2,2-Dichloropropane ND ug/kg 1 07/29/11 20:24 594-20-74.1 1.4
1,1-Dichloropropene ND ug/kg 1 07/29/11 20:24 563-58-64.1 1.2
cis-1,3-Dichloropropene ND ug/kg 1 07/29/11 20:24 10061-01-54.1 1.5
trans-1,3-Dichloropropene ND ug/kg 1 07/29/11 20:24 10061-02-64.1 1.2
Diisopropyl ether ND ug/kg 1 07/29/11 20:24 108-20-34.1 1.4
Ethylbenzene ND ug/kg 1 07/29/11 20:24 100-41-44.1 1.5
Hexachloro-1,3-butadiene ND ug/kg 1 07/29/11 20:24 87-68-34.1 1.7
2-Hexanone ND ug/kg 1 07/29/11 20:24 591-78-641.3 3.2
Isopropylbenzene (Cumene)ND ug/kg 1 07/29/11 20:24 98-82-84.1 1.6
p-Isopropyltoluene ND ug/kg 1 07/29/11 20:24 99-87-64.1 1.4
Methylene Chloride ND ug/kg 1 07/29/11 20:24 75-09-216.5 2.5
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/29/11 20:24 108-10-141.3 3.1
Methyl-tert-butyl ether ND ug/kg 1 07/29/11 20:24 1634-04-44.1 1.2
Naphthalene ND ug/kg 1 07/29/11 20:24 91-20-34.1 0.99
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 38 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-19 Lab ID:9299254019 Collected:07/27/11 14:40 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
n-Propylbenzene ND ug/kg 1 07/29/11 20:24 103-65-14.1 1.4
Styrene ND ug/kg 1 07/29/11 20:24 100-42-54.1 1.5
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/29/11 20:24 630-20-64.1 1.7
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/29/11 20:24 79-34-54.1 1.6
Tetrachloroethene ND ug/kg 1 07/29/11 20:24 127-18-44.1 1.4
Toluene ND ug/kg 1 07/29/11 20:24 108-88-34.1 1.5
1,2,3-Trichlorobenzene ND ug/kg 1 07/29/11 20:24 87-61-64.1 1.8
1,2,4-Trichlorobenzene ND ug/kg 1 07/29/11 20:24 120-82-14.1 1.3
1,1,1-Trichloroethane ND ug/kg 1 07/29/11 20:24 71-55-64.1 1.5
1,1,2-Trichloroethane ND ug/kg 1 07/29/11 20:24 79-00-54.1 1.7
Trichloroethene ND ug/kg 1 07/29/11 20:24 79-01-64.1 1.7
Trichlorofluoromethane ND ug/kg 1 07/29/11 20:24 75-69-44.1 1.8
1,2,3-Trichloropropane ND ug/kg 1 07/29/11 20:24 96-18-44.1 1.3
1,2,4-Trimethylbenzene ND ug/kg 1 07/29/11 20:24 95-63-64.1 1.7
1,3,5-Trimethylbenzene ND ug/kg 1 07/29/11 20:24 108-67-84.1 1.5
Vinyl acetate ND ug/kg 1 07/29/11 20:24 108-05-441.3 7.3
Vinyl chloride ND ug/kg 1 07/29/11 20:24 75-01-48.3 1.5
Xylene (Total)ND ug/kg 1 07/29/11 20:24 1330-20-78.3 3.0
m&p-Xylene ND ug/kg 1 07/29/11 20:24 179601-23-18.3 3.0
o-Xylene ND ug/kg 1 07/29/11 20:24 95-47-64.1 1.6
Dibromofluoromethane (S)102 %1 07/29/11 20:24 1868-53-770-130
Toluene-d8 (S)104 %1 07/29/11 20:24 2037-26-570-130
4-Bromofluorobenzene (S)93 %1 07/29/11 20:24 460-00-470-130
1,2-Dichloroethane-d4 (S)94 %1 07/29/11 20:24 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 3.1 %1 07/29/11 14:530.10 0.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 24.2 mg/kg 1 08/04/11 15:44 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/02/11 16:24 18540-29-9 N208/02/11 12:402.3 0.23
Sample:SB-20 Lab ID:9299254020 Collected:07/27/11 14:50 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 08/02/11 18:27 7440-36-008/02/11 09:000.52 0.29
Arsenic 3.7 mg/kg 1 08/02/11 18:27 7440-38-208/02/11 09:000.52 0.33
Beryllium 0.84 mg/kg 1 08/02/11 18:27 7440-41-708/02/11 09:000.10 0.021
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 39 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-20 Lab ID:9299254020 Collected:07/27/11 14:50 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Cadmium 1.6 mg/kg 1 08/02/11 18:27 7440-43-908/02/11 09:000.10 0.062
Chromium 21.0 mg/kg 1 08/02/11 18:27 7440-47-308/02/11 09:000.52 0.031
Copper 30.7 mg/kg 1 08/02/11 18:27 7440-50-808/02/11 09:000.52 0.041
Lead 9.3 mg/kg 1 08/02/11 18:27 7439-92-108/02/11 09:000.52 0.50
Manganese 328 mg/kg 1 08/02/11 18:27 7439-96-508/02/11 09:000.52 0.031
Nickel 12.2 mg/kg 1 08/02/11 18:27 7440-02-008/02/11 09:000.52 0.19
Selenium 0.51J mg/kg 1 08/02/11 18:27 7782-49-208/02/11 09:001.0 0.39
Silver ND mg/kg 1 08/02/11 18:27 7440-22-408/02/11 09:000.52 0.031
Thallium ND mg/kg 1 08/02/11 18:27 7440-28-008/02/11 09:001.0 0.27
Zinc 39.0 mg/kg 1 08/02/11 18:27 7440-66-608/02/11 09:001.0 0.27
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.012 mg/kg 1 08/02/11 15:21 7439-97-608/01/11 14:150.0040 0.000080
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 08/04/11 15:45 83-32-908/03/11 11:2636985.0
Acenaphthylene ND ug/kg 1 08/04/11 15:45 208-96-808/03/11 11:2636987.2
Aniline ND ug/kg 1 08/04/11 15:45 62-53-308/03/11 11:2636999.5
Anthracene ND ug/kg 1 08/04/11 15:45 120-12-708/03/11 11:2636982.7
Benzo(a)anthracene ND ug/kg 1 08/04/11 15:45 56-55-308/03/11 11:2636968.2
Benzo(a)pyrene 92.3J ug/kg 1 08/04/11 15:45 50-32-808/03/11 11:2636970.4
Benzo(b)fluoranthene 85.4J ug/kg 1 08/04/11 15:45 205-99-208/03/11 11:2636963.7
Benzo(g,h,i)perylene ND ug/kg 1 08/04/11 15:45 191-24-208/03/11 11:2636993.9
Benzo(k)fluoranthene 98.4J ug/kg 1 08/04/11 15:45 207-08-908/03/11 11:2636972.7
Benzoic Acid ND ug/kg 1 08/04/11 15:45 65-85-008/03/11 11:26184067.1
Benzyl alcohol ND ug/kg 1 08/04/11 15:45 100-51-608/03/11 11:2673873.8
4-Bromophenylphenyl ether ND ug/kg 1 08/04/11 15:45 101-55-308/03/11 11:2636967.1
Butylbenzylphthalate ND ug/kg 1 08/04/11 15:45 85-68-708/03/11 11:2636978.2
4-Chloro-3-methylphenol ND ug/kg 1 08/04/11 15:45 59-50-708/03/11 11:2673876.0
4-Chloroaniline ND ug/kg 1 08/04/11 15:45 106-47-808/03/11 11:261840103
bis(2-Chloroethoxy)methane ND ug/kg 1 08/04/11 15:45 111-91-108/03/11 11:2636986.1
bis(2-Chloroethyl) ether ND ug/kg 1 08/04/11 15:45 111-44-408/03/11 11:2636993.9
bis(2-Chloroisopropyl) ether ND ug/kg 1 08/04/11 15:45 108-60-108/03/11 11:2636998.4
2-Chloronaphthalene ND ug/kg 1 08/04/11 15:45 91-58-708/03/11 11:2636972.7
2-Chlorophenol ND ug/kg 1 08/04/11 15:45 95-57-808/03/11 11:26369101
4-Chlorophenylphenyl ether ND ug/kg 1 08/04/11 15:45 7005-72-308/03/11 11:2636976.0
Chrysene 79.0J ug/kg 1 08/04/11 15:45 218-01-908/03/11 11:2636949.2
Dibenz(a,h)anthracene ND ug/kg 1 08/04/11 15:45 53-70-308/03/11 11:2636978.2
Dibenzofuran ND ug/kg 1 08/04/11 15:45 132-64-908/03/11 11:2636960.4
1,2-Dichlorobenzene ND ug/kg 1 08/04/11 15:45 95-50-108/03/11 11:2636998.4
1,3-Dichlorobenzene ND ug/kg 1 08/04/11 15:45 541-73-108/03/11 11:2636983.8
1,4-Dichlorobenzene ND ug/kg 1 08/04/11 15:45 106-46-708/03/11 11:26369104
3,3'-Dichlorobenzidine ND ug/kg 1 08/04/11 15:45 91-94-108/03/11 11:26184080.5
2,4-Dichlorophenol ND ug/kg 1 08/04/11 15:45 120-83-208/03/11 11:2636980.5
Diethylphthalate ND ug/kg 1 08/04/11 15:45 84-66-208/03/11 11:2636957.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 40 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-20 Lab ID:9299254020 Collected:07/27/11 14:50 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dimethylphenol ND ug/kg 1 08/04/11 15:45 105-67-908/03/11 11:26369145
Dimethylphthalate ND ug/kg 1 08/04/11 15:45 131-11-308/03/11 11:2636974.9
Di-n-butylphthalate ND ug/kg 1 08/04/11 15:45 84-74-208/03/11 11:2636960.4
4,6-Dinitro-2-methylphenol ND ug/kg 1 08/04/11 15:45 534-52-108/03/11 11:2673873.8
2,4-Dinitrophenol ND ug/kg 1 08/04/11 15:45 51-28-508/03/11 11:26184060.4
2,4-Dinitrotoluene ND ug/kg 1 08/04/11 15:45 121-14-208/03/11 11:2636969.3
2,6-Dinitrotoluene ND ug/kg 1 08/04/11 15:45 606-20-208/03/11 11:2636977.1
Di-n-octylphthalate ND ug/kg 1 08/04/11 15:45 117-84-008/03/11 11:2636977.1
bis(2-Ethylhexyl)phthalate ND ug/kg 1 08/04/11 15:45 117-81-708/03/11 11:26369101
Fluoranthene ND ug/kg 1 08/04/11 15:45 206-44-008/03/11 11:2636953.7
Fluorene ND ug/kg 1 08/04/11 15:45 86-73-708/03/11 11:2636976.0
Hexachloro-1,3-butadiene ND ug/kg 1 08/04/11 15:45 87-68-308/03/11 11:2636963.7
Hexachlorobenzene ND ug/kg 1 08/04/11 15:45 118-74-108/03/11 11:2636946.9
Hexachlorocyclopentadiene ND ug/kg 1 08/04/11 15:45 77-47-408/03/11 11:2636968.2
Hexachloroethane ND ug/kg 1 08/04/11 15:45 67-72-108/03/11 11:2636997.3
Indeno(1,2,3-cd)pyrene ND ug/kg 1 08/04/11 15:45 193-39-508/03/11 11:2636976.0
Isophorone ND ug/kg 1 08/04/11 15:45 78-59-108/03/11 11:2636982.7
1-Methylnaphthalene ND ug/kg 1 08/04/11 15:45 90-12-008/03/11 11:2636996.1
2-Methylnaphthalene ND ug/kg 1 08/04/11 15:45 91-57-608/03/11 11:2636979.4
2-Methylphenol(o-Cresol)ND ug/kg 1 08/04/11 15:45 95-48-708/03/11 11:26369112
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 08/04/11 15:4508/03/11 11:26369145
Naphthalene ND ug/kg 1 08/04/11 15:45 91-20-308/03/11 11:2636990.5
2-Nitroaniline ND ug/kg 1 08/04/11 15:45 88-74-408/03/11 11:261840114
3-Nitroaniline ND ug/kg 1 08/04/11 15:45 99-09-208/03/11 11:261840101
4-Nitroaniline ND ug/kg 1 08/04/11 15:45 100-01-608/03/11 11:26738104
Nitrobenzene ND ug/kg 1 08/04/11 15:45 98-95-308/03/11 11:26369101
2-Nitrophenol ND ug/kg 1 08/04/11 15:45 88-75-508/03/11 11:2636989.4
4-Nitrophenol 95.3J ug/kg 1 08/04/11 15:45 100-02-708/03/11 11:26184066.0
N-Nitrosodimethylamine ND ug/kg 1 08/04/11 15:45 62-75-908/03/11 11:26369120
N-Nitroso-di-n-propylamine ND ug/kg 1 08/04/11 15:45 621-64-708/03/11 11:2636970.4
N-Nitrosodiphenylamine ND ug/kg 1 08/04/11 15:45 86-30-608/03/11 11:26369110
Pentachlorophenol ND ug/kg 1 08/04/11 15:45 87-86-508/03/11 11:26184067.1
Phenanthrene ND ug/kg 1 08/04/11 15:45 85-01-808/03/11 11:2636961.5
Phenol ND ug/kg 1 08/04/11 15:45 108-95-208/03/11 11:26369111
Pyrene ND ug/kg 1 08/04/11 15:45 129-00-008/03/11 11:2636962.6
1,2,4-Trichlorobenzene ND ug/kg 1 08/04/11 15:45 120-82-108/03/11 11:2636971.5
2,4,5-Trichlorophenol ND ug/kg 1 08/04/11 15:45 95-95-408/03/11 11:26369114
2,4,6-Trichlorophenol ND ug/kg 1 08/04/11 15:45 88-06-208/03/11 11:2636981.6
Nitrobenzene-d5 (S)33 %1 08/04/11 15:45 4165-60-008/03/11 11:2623-110
2-Fluorobiphenyl (S)32 %1 08/04/11 15:45 321-60-808/03/11 11:2630-110
Terphenyl-d14 (S)38 %1 08/04/11 15:45 1718-51-008/03/11 11:2628-110
Phenol-d6 (S)38 %1 08/04/11 15:45 13127-88-308/03/11 11:2622-110
2-Fluorophenol (S)35 %1 08/04/11 15:45 367-12-408/03/11 11:2613-110
2,4,6-Tribromophenol (S)30 %1 08/04/11 15:45 118-79-608/03/11 11:2627-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 41 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-20 Lab ID:9299254020 Collected:07/27/11 14:50 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 29.8J ug/kg 1 07/29/11 20:44 67-64-110010.0
Benzene ND ug/kg 1 07/29/11 20:44 71-43-25.0 1.6
Bromobenzene ND ug/kg 1 07/29/11 20:44 108-86-15.0 2.0
Bromochloromethane ND ug/kg 1 07/29/11 20:44 74-97-55.0 1.7
Bromodichloromethane ND ug/kg 1 07/29/11 20:44 75-27-45.0 1.9
Bromoform ND ug/kg 1 07/29/11 20:44 75-25-25.0 2.3
Bromomethane ND ug/kg 1 07/29/11 20:44 74-83-910.0 2.5
2-Butanone (MEK)ND ug/kg 1 07/29/11 20:44 78-93-31002.9
n-Butylbenzene ND ug/kg 1 07/29/11 20:44 104-51-85.0 1.8
sec-Butylbenzene ND ug/kg 1 07/29/11 20:44 135-98-85.0 1.6
tert-Butylbenzene ND ug/kg 1 07/29/11 20:44 98-06-65.0 2.0
Carbon tetrachloride ND ug/kg 1 07/29/11 20:44 56-23-55.0 2.6
Chlorobenzene ND ug/kg 1 07/29/11 20:44 108-90-75.0 1.9
Chloroethane ND ug/kg 1 07/29/11 20:44 75-00-310.0 2.4
Chloroform ND ug/kg 1 07/29/11 20:44 67-66-35.0 1.6
Chloromethane ND ug/kg 1 07/29/11 20:44 74-87-310.0 2.4
2-Chlorotoluene ND ug/kg 1 07/29/11 20:44 95-49-85.0 1.7
4-Chlorotoluene ND ug/kg 1 07/29/11 20:44 106-43-45.0 1.8
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/29/11 20:44 96-12-85.0 3.6
Dibromochloromethane ND ug/kg 1 07/29/11 20:44 124-48-15.0 1.8
1,2-Dibromoethane (EDB)ND ug/kg 1 07/29/11 20:44 106-93-45.0 1.8
Dibromomethane ND ug/kg 1 07/29/11 20:44 74-95-35.0 2.5
1,2-Dichlorobenzene ND ug/kg 1 07/29/11 20:44 95-50-15.0 1.9
1,3-Dichlorobenzene ND ug/kg 1 07/29/11 20:44 541-73-15.0 2.0
1,4-Dichlorobenzene ND ug/kg 1 07/29/11 20:44 106-46-75.0 1.7
Dichlorodifluoromethane ND ug/kg 1 07/29/11 20:44 75-71-810.0 3.6
1,1-Dichloroethane ND ug/kg 1 07/29/11 20:44 75-34-35.0 1.5
1,2-Dichloroethane ND ug/kg 1 07/29/11 20:44 107-06-25.0 2.2
1,1-Dichloroethene ND ug/kg 1 07/29/11 20:44 75-35-45.0 1.8
cis-1,2-Dichloroethene ND ug/kg 1 07/29/11 20:44 156-59-25.0 1.4
trans-1,2-Dichloroethene ND ug/kg 1 07/29/11 20:44 156-60-55.0 1.9
1,2-Dichloropropane ND ug/kg 1 07/29/11 20:44 78-87-55.0 1.7
1,3-Dichloropropane ND ug/kg 1 07/29/11 20:44 142-28-95.0 1.9
2,2-Dichloropropane ND ug/kg 1 07/29/11 20:44 594-20-75.0 1.7
1,1-Dichloropropene ND ug/kg 1 07/29/11 20:44 563-58-65.0 1.5
cis-1,3-Dichloropropene ND ug/kg 1 07/29/11 20:44 10061-01-55.0 1.8
trans-1,3-Dichloropropene ND ug/kg 1 07/29/11 20:44 10061-02-65.0 1.5
Diisopropyl ether ND ug/kg 1 07/29/11 20:44 108-20-35.0 1.7
Ethylbenzene ND ug/kg 1 07/29/11 20:44 100-41-45.0 1.8
Hexachloro-1,3-butadiene ND ug/kg 1 07/29/11 20:44 87-68-35.0 2.0
2-Hexanone ND ug/kg 1 07/29/11 20:44 591-78-650.1 3.9
Isopropylbenzene (Cumene)ND ug/kg 1 07/29/11 20:44 98-82-85.0 1.9
p-Isopropyltoluene ND ug/kg 1 07/29/11 20:44 99-87-65.0 1.7
Methylene Chloride ND ug/kg 1 07/29/11 20:44 75-09-220.0 3.0
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/29/11 20:44 108-10-150.1 3.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 42 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-20 Lab ID:9299254020 Collected:07/27/11 14:50 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
Methyl-tert-butyl ether ND ug/kg 1 07/29/11 20:44 1634-04-45.0 1.5
Naphthalene ND ug/kg 1 07/29/11 20:44 91-20-35.0 1.2
n-Propylbenzene ND ug/kg 1 07/29/11 20:44 103-65-15.0 1.7
Styrene ND ug/kg 1 07/29/11 20:44 100-42-55.0 1.8
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/29/11 20:44 630-20-65.0 2.1
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/29/11 20:44 79-34-55.0 1.9
Tetrachloroethene ND ug/kg 1 07/29/11 20:44 127-18-45.0 1.7
Toluene ND ug/kg 1 07/29/11 20:44 108-88-35.0 1.8
1,2,3-Trichlorobenzene ND ug/kg 1 07/29/11 20:44 87-61-65.0 2.2
1,2,4-Trichlorobenzene ND ug/kg 1 07/29/11 20:44 120-82-15.0 1.6
1,1,1-Trichloroethane ND ug/kg 1 07/29/11 20:44 71-55-65.0 1.8
1,1,2-Trichloroethane ND ug/kg 1 07/29/11 20:44 79-00-55.0 2.1
Trichloroethene ND ug/kg 1 07/29/11 20:44 79-01-65.0 2.1
Trichlorofluoromethane ND ug/kg 1 07/29/11 20:44 75-69-45.0 2.2
1,2,3-Trichloropropane ND ug/kg 1 07/29/11 20:44 96-18-45.0 1.6
1,2,4-Trimethylbenzene ND ug/kg 1 07/29/11 20:44 95-63-65.0 2.0
1,3,5-Trimethylbenzene ND ug/kg 1 07/29/11 20:44 108-67-85.0 1.8
Vinyl acetate ND ug/kg 1 07/29/11 20:44 108-05-450.1 8.8
Vinyl chloride ND ug/kg 1 07/29/11 20:44 75-01-410.0 1.8
Xylene (Total)ND ug/kg 1 07/29/11 20:44 1330-20-710.0 3.6
m&p-Xylene ND ug/kg 1 07/29/11 20:44 179601-23-110.0 3.6
o-Xylene ND ug/kg 1 07/29/11 20:44 95-47-65.0 1.9
Dibromofluoromethane (S)107 %1 07/29/11 20:44 1868-53-770-130
Toluene-d8 (S)104 %1 07/29/11 20:44 2037-26-570-130
4-Bromofluorobenzene (S)93 %1 07/29/11 20:44 460-00-470-130
1,2-Dichloroethane-d4 (S)96 %1 07/29/11 20:44 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 10.5 %1 07/29/11 14:530.10 0.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 21.0 mg/kg 1 08/04/11 15:44 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/02/11 16:24 18540-29-9 N208/02/11 12:402.4 0.24
Sample:SB-21 Lab ID:9299254021 Collected:07/27/11 15:00 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 08/02/11 18:31 7440-36-008/02/11 09:000.60 0.34
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 43 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-21 Lab ID:9299254021 Collected:07/27/11 15:00 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic 2.1 mg/kg 1 08/02/11 18:31 7440-38-208/02/11 09:000.60 0.38
Beryllium 0.28 mg/kg 1 08/02/11 18:31 7440-41-708/02/11 09:000.12 0.024
Cadmium 0.46 mg/kg 1 08/02/11 18:31 7440-43-908/02/11 09:000.12 0.072
Chromium 34.4 mg/kg 1 08/02/11 18:31 7440-47-308/02/11 09:000.60 0.036
Copper 20.6 mg/kg 1 08/02/11 18:31 7440-50-808/02/11 09:000.60 0.048
Lead 95.2 mg/kg 1 08/02/11 18:31 7439-92-108/02/11 09:000.60 0.58
Manganese 203 mg/kg 1 08/02/11 18:31 7439-96-508/02/11 09:000.60 0.036
Nickel 11.7 mg/kg 1 08/02/11 18:31 7440-02-008/02/11 09:000.60 0.22
Selenium ND mg/kg 1 08/02/11 18:31 7782-49-208/02/11 09:001.2 0.46
Silver ND mg/kg 1 08/02/11 18:31 7440-22-408/02/11 09:000.60 0.036
Thallium ND mg/kg 1 08/02/11 18:31 7440-28-008/02/11 09:001.2 0.31
Zinc 111 mg/kg 1 08/02/11 18:31 7440-66-608/02/11 09:001.2 0.31
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.080 mg/kg 1 08/02/11 15:24 7439-97-608/01/11 14:150.0056 0.00011
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 08/02/11 21:51 83-32-907/29/11 08:3040392.9
Acenaphthylene ND ug/kg 1 08/02/11 21:51 208-96-807/29/11 08:3040395.4
Aniline ND ug/kg 1 08/02/11 21:51 62-53-307/29/11 08:30403109
Anthracene ND ug/kg 1 08/02/11 21:51 120-12-707/29/11 08:3040390.5
Benzo(a)anthracene ND ug/kg 1 08/02/11 21:51 56-55-307/29/11 08:3040374.6
Benzo(a)pyrene ND ug/kg 1 08/02/11 21:51 50-32-807/29/11 08:3040377.0
Benzo(b)fluoranthene 76.4J ug/kg 1 08/02/11 21:51 205-99-207/29/11 08:3040369.7
Benzo(g,h,i)perylene ND ug/kg 1 08/02/11 21:51 191-24-207/29/11 08:30403103
Benzo(k)fluoranthene ND ug/kg 1 08/02/11 21:51 207-08-907/29/11 08:3040379.5
Benzoic Acid ND ug/kg 1 08/02/11 21:51 65-85-007/29/11 08:30202073.4
Benzyl alcohol ND ug/kg 1 08/02/11 21:51 100-51-607/29/11 08:3080780.7
4-Bromophenylphenyl ether ND ug/kg 1 08/02/11 21:51 101-55-307/29/11 08:3040373.4
Butylbenzylphthalate ND ug/kg 1 08/02/11 21:51 85-68-707/29/11 08:3040385.6
4-Chloro-3-methylphenol ND ug/kg 1 08/02/11 21:51 59-50-707/29/11 08:3080783.1
4-Chloroaniline ND ug/kg 1 08/02/11 21:51 106-47-807/29/11 08:302020112
bis(2-Chloroethoxy)methane ND ug/kg 1 08/02/11 21:51 111-91-107/29/11 08:3040394.1
bis(2-Chloroethyl) ether ND ug/kg 1 08/02/11 21:51 111-44-407/29/11 08:30403103
bis(2-Chloroisopropyl) ether ND ug/kg 1 08/02/11 21:51 108-60-107/29/11 08:30403108
2-Chloronaphthalene ND ug/kg 1 08/02/11 21:51 91-58-707/29/11 08:3040379.5
2-Chlorophenol ND ug/kg 1 08/02/11 21:51 95-57-807/29/11 08:30403110
4-Chlorophenylphenyl ether ND ug/kg 1 08/02/11 21:51 7005-72-307/29/11 08:3040383.1
Chrysene 68.3J ug/kg 1 08/02/11 21:51 218-01-907/29/11 08:3040353.8
Dibenz(a,h)anthracene ND ug/kg 1 08/02/11 21:51 53-70-307/29/11 08:3040385.6
Dibenzofuran ND ug/kg 1 08/02/11 21:51 132-64-907/29/11 08:3040366.0
1,2-Dichlorobenzene ND ug/kg 1 08/02/11 21:51 95-50-107/29/11 08:30403108
1,3-Dichlorobenzene ND ug/kg 1 08/02/11 21:51 541-73-107/29/11 08:3040391.7
1,4-Dichlorobenzene ND ug/kg 1 08/02/11 21:51 106-46-707/29/11 08:30403114
3,3'-Dichlorobenzidine ND ug/kg 1 08/02/11 21:51 91-94-107/29/11 08:30202088.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 44 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-21 Lab ID:9299254021 Collected:07/27/11 15:00 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dichlorophenol ND ug/kg 1 08/02/11 21:51 120-83-207/29/11 08:3040388.0
Diethylphthalate ND ug/kg 1 08/02/11 21:51 84-66-207/29/11 08:3040362.4
2,4-Dimethylphenol ND ug/kg 1 08/02/11 21:51 105-67-907/29/11 08:30403159
Dimethylphthalate ND ug/kg 1 08/02/11 21:51 131-11-307/29/11 08:3040381.9
Di-n-butylphthalate ND ug/kg 1 08/02/11 21:51 84-74-207/29/11 08:3040366.0
4,6-Dinitro-2-methylphenol ND ug/kg 1 08/02/11 21:51 534-52-107/29/11 08:3080780.7
2,4-Dinitrophenol ND ug/kg 1 08/02/11 21:51 51-28-507/29/11 08:30202066.0
2,4-Dinitrotoluene ND ug/kg 1 08/02/11 21:51 121-14-207/29/11 08:3040375.8
2,6-Dinitrotoluene ND ug/kg 1 08/02/11 21:51 606-20-207/29/11 08:3040384.4
Di-n-octylphthalate ND ug/kg 1 08/02/11 21:51 117-84-007/29/11 08:3040384.4
bis(2-Ethylhexyl)phthalate ND ug/kg 1 08/02/11 21:51 117-81-707/29/11 08:30403110
Fluoranthene 89.0J ug/kg 1 08/02/11 21:51 206-44-007/29/11 08:3040358.7
Fluorene ND ug/kg 1 08/02/11 21:51 86-73-707/29/11 08:3040383.1
Hexachloro-1,3-butadiene ND ug/kg 1 08/02/11 21:51 87-68-307/29/11 08:3040369.7
Hexachlorobenzene ND ug/kg 1 08/02/11 21:51 118-74-107/29/11 08:3040351.4
Hexachlorocyclopentadiene ND ug/kg 1 08/02/11 21:51 77-47-407/29/11 08:3040374.6
Hexachloroethane ND ug/kg 1 08/02/11 21:51 67-72-107/29/11 08:30403106
Indeno(1,2,3-cd)pyrene ND ug/kg 1 08/02/11 21:51 193-39-507/29/11 08:3040383.1
Isophorone ND ug/kg 1 08/02/11 21:51 78-59-107/29/11 08:3040390.5
1-Methylnaphthalene ND ug/kg 1 08/02/11 21:51 90-12-007/29/11 08:30403105
2-Methylnaphthalene ND ug/kg 1 08/02/11 21:51 91-57-607/29/11 08:3040386.8
2-Methylphenol(o-Cresol)ND ug/kg 1 08/02/11 21:51 95-48-707/29/11 08:30403122
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 08/02/11 21:5107/29/11 08:30403159
Naphthalene ND ug/kg 1 08/02/11 21:51 91-20-307/29/11 08:3040399.0
2-Nitroaniline ND ug/kg 1 08/02/11 21:51 88-74-407/29/11 08:302020125
3-Nitroaniline ND ug/kg 1 08/02/11 21:51 99-09-207/29/11 08:302020110
4-Nitroaniline ND ug/kg 1 08/02/11 21:51 100-01-607/29/11 08:30807114
Nitrobenzene ND ug/kg 1 08/02/11 21:51 98-95-307/29/11 08:30403110
2-Nitrophenol ND ug/kg 1 08/02/11 21:51 88-75-507/29/11 08:3040397.8
4-Nitrophenol ND ug/kg 1 08/02/11 21:51 100-02-707/29/11 08:30202072.1
N-Nitrosodimethylamine ND ug/kg 1 08/02/11 21:51 62-75-907/29/11 08:30403131
N-Nitroso-di-n-propylamine ND ug/kg 1 08/02/11 21:51 621-64-707/29/11 08:3040377.0
N-Nitrosodiphenylamine ND ug/kg 1 08/02/11 21:51 86-30-607/29/11 08:30403120
Pentachlorophenol ND ug/kg 1 08/02/11 21:51 87-86-507/29/11 08:30202073.4
Phenanthrene ND ug/kg 1 08/02/11 21:51 85-01-807/29/11 08:3040367.2
Phenol ND ug/kg 1 08/02/11 21:51 108-95-207/29/11 08:30403121
Pyrene 78.8J ug/kg 1 08/02/11 21:51 129-00-007/29/11 08:3040368.5
1,2,4-Trichlorobenzene ND ug/kg 1 08/02/11 21:51 120-82-107/29/11 08:3040378.2
2,4,5-Trichlorophenol ND ug/kg 1 08/02/11 21:51 95-95-407/29/11 08:30403125
2,4,6-Trichlorophenol ND ug/kg 1 08/02/11 21:51 88-06-207/29/11 08:3040389.3
Nitrobenzene-d5 (S)27 %1 08/02/11 21:51 4165-60-007/29/11 08:3023-110
2-Fluorobiphenyl (S)29 %1 08/02/11 21:51 321-60-8 S007/29/11 08:3030-110
Terphenyl-d14 (S)36 %1 08/02/11 21:51 1718-51-007/29/11 08:3028-110
Phenol-d6 (S)25 %1 08/02/11 21:51 13127-88-307/29/11 08:3022-110
2-Fluorophenol (S)24 %1 08/02/11 21:51 367-12-407/29/11 08:3013-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 45 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-21 Lab ID:9299254021 Collected:07/27/11 15:00 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4,6-Tribromophenol (S)33 %1 08/02/11 21:51 118-79-607/29/11 08:3027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 62.2J ug/kg 1 07/29/11 21:04 67-64-181.9 8.2
Benzene ND ug/kg 1 07/29/11 21:04 71-43-24.1 1.3
Bromobenzene ND ug/kg 1 07/29/11 21:04 108-86-14.1 1.6
Bromochloromethane ND ug/kg 1 07/29/11 21:04 74-97-54.1 1.4
Bromodichloromethane ND ug/kg 1 07/29/11 21:04 75-27-44.1 1.6
Bromoform ND ug/kg 1 07/29/11 21:04 75-25-24.1 1.9
Bromomethane ND ug/kg 1 07/29/11 21:04 74-83-98.2 2.0
2-Butanone (MEK)ND ug/kg 1 07/29/11 21:04 78-93-381.9 2.4
n-Butylbenzene ND ug/kg 1 07/29/11 21:04 104-51-84.1 1.5
sec-Butylbenzene ND ug/kg 1 07/29/11 21:04 135-98-84.1 1.3
tert-Butylbenzene ND ug/kg 1 07/29/11 21:04 98-06-64.1 1.6
Carbon tetrachloride ND ug/kg 1 07/29/11 21:04 56-23-54.1 2.1
Chlorobenzene ND ug/kg 1 07/29/11 21:04 108-90-74.1 1.6
Chloroethane ND ug/kg 1 07/29/11 21:04 75-00-38.2 2.0
Chloroform ND ug/kg 1 07/29/11 21:04 67-66-34.1 1.3
Chloromethane ND ug/kg 1 07/29/11 21:04 74-87-38.2 2.0
2-Chlorotoluene ND ug/kg 1 07/29/11 21:04 95-49-84.1 1.4
4-Chlorotoluene ND ug/kg 1 07/29/11 21:04 106-43-44.1 1.5
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/29/11 21:04 96-12-84.1 3.0
Dibromochloromethane ND ug/kg 1 07/29/11 21:04 124-48-14.1 1.5
1,2-Dibromoethane (EDB)ND ug/kg 1 07/29/11 21:04 106-93-44.1 1.5
Dibromomethane ND ug/kg 1 07/29/11 21:04 74-95-34.1 2.0
1,2-Dichlorobenzene ND ug/kg 1 07/29/11 21:04 95-50-14.1 1.6
1,3-Dichlorobenzene ND ug/kg 1 07/29/11 21:04 541-73-14.1 1.6
1,4-Dichlorobenzene ND ug/kg 1 07/29/11 21:04 106-46-74.1 1.4
Dichlorodifluoromethane ND ug/kg 1 07/29/11 21:04 75-71-88.2 3.0
1,1-Dichloroethane ND ug/kg 1 07/29/11 21:04 75-34-34.1 1.2
1,2-Dichloroethane ND ug/kg 1 07/29/11 21:04 107-06-24.1 1.8
1,1-Dichloroethene ND ug/kg 1 07/29/11 21:04 75-35-44.1 1.5
cis-1,2-Dichloroethene ND ug/kg 1 07/29/11 21:04 156-59-24.1 1.1
trans-1,2-Dichloroethene ND ug/kg 1 07/29/11 21:04 156-60-54.1 1.6
1,2-Dichloropropane ND ug/kg 1 07/29/11 21:04 78-87-54.1 1.4
1,3-Dichloropropane ND ug/kg 1 07/29/11 21:04 142-28-94.1 1.6
2,2-Dichloropropane ND ug/kg 1 07/29/11 21:04 594-20-74.1 1.4
1,1-Dichloropropene ND ug/kg 1 07/29/11 21:04 563-58-64.1 1.2
cis-1,3-Dichloropropene ND ug/kg 1 07/29/11 21:04 10061-01-54.1 1.5
trans-1,3-Dichloropropene ND ug/kg 1 07/29/11 21:04 10061-02-64.1 1.2
Diisopropyl ether ND ug/kg 1 07/29/11 21:04 108-20-34.1 1.4
Ethylbenzene ND ug/kg 1 07/29/11 21:04 100-41-44.1 1.5
Hexachloro-1,3-butadiene ND ug/kg 1 07/29/11 21:04 87-68-34.1 1.6
2-Hexanone ND ug/kg 1 07/29/11 21:04 591-78-641.0 3.2
Isopropylbenzene (Cumene)ND ug/kg 1 07/29/11 21:04 98-82-84.1 1.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 46 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-21 Lab ID:9299254021 Collected:07/27/11 15:00 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
p-Isopropyltoluene ND ug/kg 1 07/29/11 21:04 99-87-64.1 1.4
Methylene Chloride ND ug/kg 1 07/29/11 21:04 75-09-216.4 2.5
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/29/11 21:04 108-10-141.0 3.0
Methyl-tert-butyl ether ND ug/kg 1 07/29/11 21:04 1634-04-44.1 1.2
Naphthalene ND ug/kg 1 07/29/11 21:04 91-20-34.1 0.98
n-Propylbenzene ND ug/kg 1 07/29/11 21:04 103-65-14.1 1.4
Styrene ND ug/kg 1 07/29/11 21:04 100-42-54.1 1.5
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/29/11 21:04 630-20-64.1 1.7
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/29/11 21:04 79-34-54.1 1.6
Tetrachloroethene ND ug/kg 1 07/29/11 21:04 127-18-44.1 1.4
Toluene ND ug/kg 1 07/29/11 21:04 108-88-34.1 1.5
1,2,3-Trichlorobenzene ND ug/kg 1 07/29/11 21:04 87-61-64.1 1.8
1,2,4-Trichlorobenzene ND ug/kg 1 07/29/11 21:04 120-82-14.1 1.3
1,1,1-Trichloroethane ND ug/kg 1 07/29/11 21:04 71-55-64.1 1.5
1,1,2-Trichloroethane ND ug/kg 1 07/29/11 21:04 79-00-54.1 1.7
Trichloroethene ND ug/kg 1 07/29/11 21:04 79-01-64.1 1.7
Trichlorofluoromethane ND ug/kg 1 07/29/11 21:04 75-69-44.1 1.8
1,2,3-Trichloropropane ND ug/kg 1 07/29/11 21:04 96-18-44.1 1.3
1,2,4-Trimethylbenzene ND ug/kg 1 07/29/11 21:04 95-63-64.1 1.6
1,3,5-Trimethylbenzene ND ug/kg 1 07/29/11 21:04 108-67-84.1 1.5
Vinyl acetate ND ug/kg 1 07/29/11 21:04 108-05-441.0 7.2
Vinyl chloride ND ug/kg 1 07/29/11 21:04 75-01-48.2 1.5
Xylene (Total)ND ug/kg 1 07/29/11 21:04 1330-20-78.2 3.0
m&p-Xylene ND ug/kg 1 07/29/11 21:04 179601-23-18.2 3.0
o-Xylene ND ug/kg 1 07/29/11 21:04 95-47-64.1 1.6
Dibromofluoromethane (S)104 %1 07/29/11 21:04 1868-53-770-130
Toluene-d8 (S)105 %1 07/29/11 21:04 2037-26-570-130
4-Bromofluorobenzene (S)91 %1 07/29/11 21:04 460-00-470-130
1,2-Dichloroethane-d4 (S)101 %1 07/29/11 21:04 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 18.2 %1 07/29/11 14:530.10 0.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 34.4 mg/kg 1 08/04/11 15:44 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/04/11 13:17 18540-29-9 N208/04/11 10:433.2 0.32
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 47 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-22 Lab ID:9299254022 Collected:07/27/11 15:10 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 08/02/11 18:34 7440-36-008/02/11 09:000.55 0.31
Arsenic 0.65 mg/kg 1 08/02/11 18:34 7440-38-208/02/11 09:000.55 0.35
Beryllium 0.074J mg/kg 1 08/02/11 18:34 7440-41-708/02/11 09:000.11 0.022
Cadmium 0.28 mg/kg 1 08/02/11 18:34 7440-43-908/02/11 09:000.11 0.066
Chromium 11.7 mg/kg 1 08/02/11 18:34 7440-47-308/02/11 09:000.55 0.033
Copper 6.7 mg/kg 1 08/02/11 18:34 7440-50-808/02/11 09:000.55 0.044
Lead 7.2 mg/kg 1 08/02/11 18:34 7439-92-108/02/11 09:000.55 0.53
Manganese 36.5 mg/kg 1 08/02/11 18:34 7439-96-508/02/11 09:000.55 0.033
Nickel 0.49J mg/kg 1 08/02/11 18:34 7440-02-008/02/11 09:000.55 0.20
Selenium ND mg/kg 1 08/02/11 18:34 7782-49-208/02/11 09:001.1 0.42
Silver ND mg/kg 1 08/02/11 18:34 7440-22-408/02/11 09:000.55 0.033
Thallium ND mg/kg 1 08/02/11 18:34 7440-28-008/02/11 09:001.1 0.29
Zinc 3.6 mg/kg 1 08/02/11 18:34 7440-66-608/02/11 09:001.1 0.29
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.028 mg/kg 1 08/02/11 15:27 7439-97-608/01/11 14:150.0034 0.000067
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 08/02/11 22:19 83-32-907/29/11 08:3037085.3
Acenaphthylene ND ug/kg 1 08/02/11 22:19 208-96-807/29/11 08:3037087.6
Aniline ND ug/kg 1 08/02/11 22:19 62-53-307/29/11 08:3037099.9
Anthracene ND ug/kg 1 08/02/11 22:19 120-12-707/29/11 08:3037083.1
Benzo(a)anthracene ND ug/kg 1 08/02/11 22:19 56-55-307/29/11 08:3037068.5
Benzo(a)pyrene ND ug/kg 1 08/02/11 22:19 50-32-807/29/11 08:3037070.7
Benzo(b)fluoranthene ND ug/kg 1 08/02/11 22:19 205-99-207/29/11 08:3037064.0
Benzo(g,h,i)perylene ND ug/kg 1 08/02/11 22:19 191-24-207/29/11 08:3037094.3
Benzo(k)fluoranthene ND ug/kg 1 08/02/11 22:19 207-08-907/29/11 08:3037073.0
Benzoic Acid ND ug/kg 1 08/02/11 22:19 65-85-007/29/11 08:30185067.4
Benzyl alcohol ND ug/kg 1 08/02/11 22:19 100-51-607/29/11 08:3074174.1
4-Bromophenylphenyl ether ND ug/kg 1 08/02/11 22:19 101-55-307/29/11 08:3037067.4
Butylbenzylphthalate ND ug/kg 1 08/02/11 22:19 85-68-707/29/11 08:3037078.6
4-Chloro-3-methylphenol ND ug/kg 1 08/02/11 22:19 59-50-707/29/11 08:3074176.3
4-Chloroaniline ND ug/kg 1 08/02/11 22:19 106-47-807/29/11 08:301850103
bis(2-Chloroethoxy)methane ND ug/kg 1 08/02/11 22:19 111-91-107/29/11 08:3037086.4
bis(2-Chloroethyl) ether ND ug/kg 1 08/02/11 22:19 111-44-407/29/11 08:3037094.3
bis(2-Chloroisopropyl) ether ND ug/kg 1 08/02/11 22:19 108-60-107/29/11 08:3037098.8
2-Chloronaphthalene ND ug/kg 1 08/02/11 22:19 91-58-707/29/11 08:3037073.0
2-Chlorophenol ND ug/kg 1 08/02/11 22:19 95-57-807/29/11 08:30370101
4-Chlorophenylphenyl ether ND ug/kg 1 08/02/11 22:19 7005-72-307/29/11 08:3037076.3
Chrysene ND ug/kg 1 08/02/11 22:19 218-01-907/29/11 08:3037049.4
Dibenz(a,h)anthracene ND ug/kg 1 08/02/11 22:19 53-70-307/29/11 08:3037078.6
Dibenzofuran ND ug/kg 1 08/02/11 22:19 132-64-907/29/11 08:3037060.6
1,2-Dichlorobenzene ND ug/kg 1 08/02/11 22:19 95-50-107/29/11 08:3037098.8
1,3-Dichlorobenzene ND ug/kg 1 08/02/11 22:19 541-73-107/29/11 08:3037084.2
1,4-Dichlorobenzene ND ug/kg 1 08/02/11 22:19 106-46-707/29/11 08:30370104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 48 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-22 Lab ID:9299254022 Collected:07/27/11 15:10 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3,3'-Dichlorobenzidine ND ug/kg 1 08/02/11 22:19 91-94-107/29/11 08:30185080.8
2,4-Dichlorophenol ND ug/kg 1 08/02/11 22:19 120-83-207/29/11 08:3037080.8
Diethylphthalate ND ug/kg 1 08/02/11 22:19 84-66-207/29/11 08:3037057.3
2,4-Dimethylphenol ND ug/kg 1 08/02/11 22:19 105-67-907/29/11 08:30370146
Dimethylphthalate ND ug/kg 1 08/02/11 22:19 131-11-307/29/11 08:3037075.2
Di-n-butylphthalate ND ug/kg 1 08/02/11 22:19 84-74-207/29/11 08:3037060.6
4,6-Dinitro-2-methylphenol ND ug/kg 1 08/02/11 22:19 534-52-107/29/11 08:3074174.1
2,4-Dinitrophenol ND ug/kg 1 08/02/11 22:19 51-28-507/29/11 08:30185060.6
2,4-Dinitrotoluene ND ug/kg 1 08/02/11 22:19 121-14-207/29/11 08:3037069.6
2,6-Dinitrotoluene ND ug/kg 1 08/02/11 22:19 606-20-207/29/11 08:3037077.5
Di-n-octylphthalate ND ug/kg 1 08/02/11 22:19 117-84-007/29/11 08:3037077.5
bis(2-Ethylhexyl)phthalate ND ug/kg 1 08/02/11 22:19 117-81-707/29/11 08:30370101
Fluoranthene ND ug/kg 1 08/02/11 22:19 206-44-007/29/11 08:3037053.9
Fluorene ND ug/kg 1 08/02/11 22:19 86-73-707/29/11 08:3037076.3
Hexachloro-1,3-butadiene ND ug/kg 1 08/02/11 22:19 87-68-307/29/11 08:3037064.0
Hexachlorobenzene ND ug/kg 1 08/02/11 22:19 118-74-107/29/11 08:3037047.1
Hexachlorocyclopentadiene ND ug/kg 1 08/02/11 22:19 77-47-407/29/11 08:3037068.5
Hexachloroethane ND ug/kg 1 08/02/11 22:19 67-72-107/29/11 08:3037097.7
Indeno(1,2,3-cd)pyrene ND ug/kg 1 08/02/11 22:19 193-39-507/29/11 08:3037076.3
Isophorone ND ug/kg 1 08/02/11 22:19 78-59-107/29/11 08:3037083.1
1-Methylnaphthalene ND ug/kg 1 08/02/11 22:19 90-12-007/29/11 08:3037096.5
2-Methylnaphthalene ND ug/kg 1 08/02/11 22:19 91-57-607/29/11 08:3037079.7
2-Methylphenol(o-Cresol)ND ug/kg 1 08/02/11 22:19 95-48-707/29/11 08:30370112
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 08/02/11 22:1907/29/11 08:30370146
Naphthalene ND ug/kg 1 08/02/11 22:19 91-20-307/29/11 08:3037090.9
2-Nitroaniline ND ug/kg 1 08/02/11 22:19 88-74-407/29/11 08:301850115
3-Nitroaniline ND ug/kg 1 08/02/11 22:19 99-09-207/29/11 08:301850101
4-Nitroaniline ND ug/kg 1 08/02/11 22:19 100-01-607/29/11 08:30741104
Nitrobenzene ND ug/kg 1 08/02/11 22:19 98-95-307/29/11 08:30370101
2-Nitrophenol ND ug/kg 1 08/02/11 22:19 88-75-507/29/11 08:3037089.8
4-Nitrophenol ND ug/kg 1 08/02/11 22:19 100-02-707/29/11 08:30185066.2
N-Nitrosodimethylamine ND ug/kg 1 08/02/11 22:19 62-75-907/29/11 08:30370120
N-Nitroso-di-n-propylamine ND ug/kg 1 08/02/11 22:19 621-64-707/29/11 08:3037070.7
N-Nitrosodiphenylamine ND ug/kg 1 08/02/11 22:19 86-30-607/29/11 08:30370110
Pentachlorophenol ND ug/kg 1 08/02/11 22:19 87-86-507/29/11 08:30185067.4
Phenanthrene ND ug/kg 1 08/02/11 22:19 85-01-807/29/11 08:3037061.7
Phenol ND ug/kg 1 08/02/11 22:19 108-95-207/29/11 08:30370111
Pyrene ND ug/kg 1 08/02/11 22:19 129-00-007/29/11 08:3037062.9
1,2,4-Trichlorobenzene ND ug/kg 1 08/02/11 22:19 120-82-107/29/11 08:3037071.8
2,4,5-Trichlorophenol ND ug/kg 1 08/02/11 22:19 95-95-407/29/11 08:30370115
2,4,6-Trichlorophenol ND ug/kg 1 08/02/11 22:19 88-06-207/29/11 08:3037081.9
Nitrobenzene-d5 (S)31 %1 08/02/11 22:19 4165-60-007/29/11 08:3023-110
2-Fluorobiphenyl (S)34 %1 08/02/11 22:19 321-60-807/29/11 08:3030-110
Terphenyl-d14 (S)41 %1 08/02/11 22:19 1718-51-007/29/11 08:3028-110
Phenol-d6 (S)35 %1 08/02/11 22:19 13127-88-307/29/11 08:3022-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 49 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-22 Lab ID:9299254022 Collected:07/27/11 15:10 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Fluorophenol (S)33 %1 08/02/11 22:19 367-12-407/29/11 08:3013-110
2,4,6-Tribromophenol (S)44 %1 08/02/11 22:19 118-79-607/29/11 08:3027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/29/11 21:24 67-64-185.0 8.5
Benzene ND ug/kg 1 07/29/11 21:24 71-43-24.3 1.4
Bromobenzene ND ug/kg 1 07/29/11 21:24 108-86-14.3 1.7
Bromochloromethane ND ug/kg 1 07/29/11 21:24 74-97-54.3 1.4
Bromodichloromethane ND ug/kg 1 07/29/11 21:24 75-27-44.3 1.6
Bromoform ND ug/kg 1 07/29/11 21:24 75-25-24.3 2.0
Bromomethane ND ug/kg 1 07/29/11 21:24 74-83-98.5 2.1
2-Butanone (MEK)ND ug/kg 1 07/29/11 21:24 78-93-385.0 2.5
n-Butylbenzene ND ug/kg 1 07/29/11 21:24 104-51-84.3 1.5
sec-Butylbenzene ND ug/kg 1 07/29/11 21:24 135-98-84.3 1.4
tert-Butylbenzene ND ug/kg 1 07/29/11 21:24 98-06-64.3 1.7
Carbon tetrachloride ND ug/kg 1 07/29/11 21:24 56-23-54.3 2.2
Chlorobenzene ND ug/kg 1 07/29/11 21:24 108-90-74.3 1.6
Chloroethane ND ug/kg 1 07/29/11 21:24 75-00-38.5 2.0
Chloroform ND ug/kg 1 07/29/11 21:24 67-66-34.3 1.4
Chloromethane ND ug/kg 1 07/29/11 21:24 74-87-38.5 2.0
2-Chlorotoluene ND ug/kg 1 07/29/11 21:24 95-49-84.3 1.4
4-Chlorotoluene ND ug/kg 1 07/29/11 21:24 106-43-44.3 1.5
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/29/11 21:24 96-12-84.3 3.1
Dibromochloromethane ND ug/kg 1 07/29/11 21:24 124-48-14.3 1.5
1,2-Dibromoethane (EDB)ND ug/kg 1 07/29/11 21:24 106-93-44.3 1.5
Dibromomethane ND ug/kg 1 07/29/11 21:24 74-95-34.3 2.1
1,2-Dichlorobenzene ND ug/kg 1 07/29/11 21:24 95-50-14.3 1.6
1,3-Dichlorobenzene ND ug/kg 1 07/29/11 21:24 541-73-14.3 1.7
1,4-Dichlorobenzene ND ug/kg 1 07/29/11 21:24 106-46-74.3 1.4
Dichlorodifluoromethane ND ug/kg 1 07/29/11 21:24 75-71-88.5 3.1
1,1-Dichloroethane ND ug/kg 1 07/29/11 21:24 75-34-34.3 1.3
1,2-Dichloroethane ND ug/kg 1 07/29/11 21:24 107-06-24.3 1.9
1,1-Dichloroethene ND ug/kg 1 07/29/11 21:24 75-35-44.3 1.5
cis-1,2-Dichloroethene ND ug/kg 1 07/29/11 21:24 156-59-24.3 1.2
trans-1,2-Dichloroethene ND ug/kg 1 07/29/11 21:24 156-60-54.3 1.6
1,2-Dichloropropane ND ug/kg 1 07/29/11 21:24 78-87-54.3 1.4
1,3-Dichloropropane ND ug/kg 1 07/29/11 21:24 142-28-94.3 1.6
2,2-Dichloropropane ND ug/kg 1 07/29/11 21:24 594-20-74.3 1.4
1,1-Dichloropropene ND ug/kg 1 07/29/11 21:24 563-58-64.3 1.3
cis-1,3-Dichloropropene ND ug/kg 1 07/29/11 21:24 10061-01-54.3 1.5
trans-1,3-Dichloropropene ND ug/kg 1 07/29/11 21:24 10061-02-64.3 1.3
Diisopropyl ether ND ug/kg 1 07/29/11 21:24 108-20-34.3 1.4
Ethylbenzene ND ug/kg 1 07/29/11 21:24 100-41-44.3 1.5
Hexachloro-1,3-butadiene ND ug/kg 1 07/29/11 21:24 87-68-34.3 1.7
2-Hexanone ND ug/kg 1 07/29/11 21:24 591-78-642.5 3.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 50 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:SB-22 Lab ID:9299254022 Collected:07/27/11 15:10 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
Isopropylbenzene (Cumene)ND ug/kg 1 07/29/11 21:24 98-82-84.3 1.6
p-Isopropyltoluene ND ug/kg 1 07/29/11 21:24 99-87-64.3 1.4
Methylene Chloride ND ug/kg 1 07/29/11 21:24 75-09-217.0 2.6
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/29/11 21:24 108-10-142.5 3.1
Methyl-tert-butyl ether ND ug/kg 1 07/29/11 21:24 1634-04-44.3 1.3
Naphthalene ND ug/kg 1 07/29/11 21:24 91-20-34.3 1.0
n-Propylbenzene ND ug/kg 1 07/29/11 21:24 103-65-14.3 1.4
Styrene ND ug/kg 1 07/29/11 21:24 100-42-54.3 1.5
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/29/11 21:24 630-20-64.3 1.8
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/29/11 21:24 79-34-54.3 1.6
Tetrachloroethene ND ug/kg 1 07/29/11 21:24 127-18-44.3 1.4
Toluene ND ug/kg 1 07/29/11 21:24 108-88-34.3 1.5
1,2,3-Trichlorobenzene ND ug/kg 1 07/29/11 21:24 87-61-64.3 1.9
1,2,4-Trichlorobenzene ND ug/kg 1 07/29/11 21:24 120-82-14.3 1.4
1,1,1-Trichloroethane ND ug/kg 1 07/29/11 21:24 71-55-64.3 1.5
1,1,2-Trichloroethane ND ug/kg 1 07/29/11 21:24 79-00-54.3 1.8
Trichloroethene ND ug/kg 1 07/29/11 21:24 79-01-64.3 1.8
Trichlorofluoromethane ND ug/kg 1 07/29/11 21:24 75-69-44.3 1.9
1,2,3-Trichloropropane ND ug/kg 1 07/29/11 21:24 96-18-44.3 1.4
1,2,4-Trimethylbenzene ND ug/kg 1 07/29/11 21:24 95-63-64.3 1.7
1,3,5-Trimethylbenzene ND ug/kg 1 07/29/11 21:24 108-67-84.3 1.5
Vinyl acetate ND ug/kg 1 07/29/11 21:24 108-05-442.5 7.5
Vinyl chloride ND ug/kg 1 07/29/11 21:24 75-01-48.5 1.5
Xylene (Total)ND ug/kg 1 07/29/11 21:24 1330-20-78.5 3.1
m&p-Xylene ND ug/kg 1 07/29/11 21:24 179601-23-18.5 3.1
o-Xylene ND ug/kg 1 07/29/11 21:24 95-47-64.3 1.6
Dibromofluoromethane (S)101 %1 07/29/11 21:24 1868-53-770-130
Toluene-d8 (S)102 %1 07/29/11 21:24 2037-26-570-130
4-Bromofluorobenzene (S)93 %1 07/29/11 21:24 460-00-470-130
1,2-Dichloroethane-d4 (S)99 %1 07/29/11 21:24 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 10.9 %1 07/29/11 14:530.10 0.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 11.7 mg/kg 1 08/04/11 15:44 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/04/11 13:17 18540-29-9 M0,N208/04/11 10:432.8 0.28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 51 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:COMP 1 Lab ID:9299254023 Collected:07/27/11 09:40 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 4.2 mg/kg 1 08/02/11 14:32 7440-36-008/02/11 09:000.54 0.30
Arsenic 34.3 mg/kg 1 08/02/11 14:32 7440-38-208/02/11 09:000.54 0.34
Beryllium 0.27 mg/kg 1 08/02/11 14:32 7440-41-708/02/11 09:000.11 0.021
Cadmium 17.8 mg/kg 1 08/02/11 14:32 7440-43-908/02/11 09:000.11 0.064
Chromium 30.1 mg/kg 1 08/02/11 14:32 7440-47-308/02/11 09:000.54 0.032
Copper 191 mg/kg 1 08/02/11 14:32 7440-50-808/02/11 09:000.54 0.043
Lead 389 mg/kg 1 08/02/11 14:32 7439-92-108/02/11 09:000.54 0.52
Manganese 253 mg/kg 1 08/02/11 14:32 7439-96-508/02/11 09:000.54 0.032
Nickel 10 mg/kg 1 08/02/11 14:32 7440-02-008/02/11 09:000.54 0.19
Selenium 1.7 mg/kg 1 08/02/11 14:32 7782-49-208/02/11 09:001.1 0.41
Silver 0.42J mg/kg 1 08/02/11 14:32 7440-22-408/02/11 09:000.54 0.032
Thallium ND mg/kg 1 08/02/11 14:32 7440-28-008/02/11 09:001.1 0.28
Zinc 3320 mg/kg 10 08/03/11 16:17 7440-66-608/02/11 09:0010.7 2.8
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 5.8 mg/kg 200 08/03/11 11:58 7439-97-608/01/11 14:150.73 0.015
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 10 08/04/11 13:19 83-32-907/29/11 13:043620833
Acenaphthylene ND ug/kg 10 08/04/11 13:19 208-96-807/29/11 13:043620855
Aniline ND ug/kg 10 08/04/11 13:19 62-53-307/29/11 13:043620976
Anthracene 2380J ug/kg 10 08/04/11 13:19 120-12-707/29/11 13:043620811
Benzo(a)anthracene 12800 ug/kg 10 08/04/11 13:19 56-55-307/29/11 13:043620669
Benzo(a)pyrene 9960 ug/kg 10 08/04/11 13:19 50-32-8 IO07/29/11 13:043620691
Benzo(b)fluoranthene 9420 ug/kg 10 08/04/11 13:19 205-99-2 IO07/29/11 13:043620625
Benzo(g,h,i)perylene 3850 ug/kg 10 08/04/11 13:19 191-24-2 IO07/29/11 13:043620921
Benzo(k)fluoranthene 9470 ug/kg 10 08/04/11 13:19 207-08-9 IO07/29/11 13:043620713
Benzoic Acid ND ug/kg 10 08/04/11 13:19 65-85-007/29/11 13:0418100658
Benzyl alcohol ND ug/kg 10 08/04/11 13:19 100-51-607/29/11 13:047240724
4-Bromophenylphenyl ether ND ug/kg 10 08/04/11 13:19 101-55-307/29/11 13:043620658
Butylbenzylphthalate ND ug/kg 10 08/04/11 13:19 85-68-707/29/11 13:043620767
4-Chloro-3-methylphenol ND ug/kg 10 08/04/11 13:19 59-50-707/29/11 13:047240745
4-Chloroaniline ND ug/kg 10 08/04/11 13:19 106-47-807/29/11 13:04181001010
bis(2-Chloroethoxy)methane ND ug/kg 10 08/04/11 13:19 111-91-107/29/11 13:043620844
bis(2-Chloroethyl) ether ND ug/kg 10 08/04/11 13:19 111-44-407/29/11 13:043620921
bis(2-Chloroisopropyl) ether ND ug/kg 10 08/04/11 13:19 108-60-107/29/11 13:043620965
2-Chloronaphthalene ND ug/kg 10 08/04/11 13:19 91-58-707/29/11 13:043620713
2-Chlorophenol ND ug/kg 10 08/04/11 13:19 95-57-807/29/11 13:043620987
4-Chlorophenylphenyl ether ND ug/kg 10 08/04/11 13:19 7005-72-307/29/11 13:043620745
Chrysene 13200 ug/kg 10 08/04/11 13:19 218-01-907/29/11 13:043620482
Dibenz(a,h)anthracene 2230J ug/kg 10 08/04/11 13:19 53-70-3 IO07/29/11 13:043620767
Dibenzofuran ND ug/kg 10 08/04/11 13:19 132-64-907/29/11 13:043620592
1,2-Dichlorobenzene ND ug/kg 10 08/04/11 13:19 95-50-107/29/11 13:043620965
1,3-Dichlorobenzene ND ug/kg 10 08/04/11 13:19 541-73-107/29/11 13:043620822
1,4-Dichlorobenzene ND ug/kg 10 08/04/11 13:19 106-46-707/29/11 13:0436201020
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 52 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:COMP 1 Lab ID:9299254023 Collected:07/27/11 09:40 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3,3'-Dichlorobenzidine ND ug/kg 10 08/04/11 13:19 91-94-107/29/11 13:0418100789
2,4-Dichlorophenol ND ug/kg 10 08/04/11 13:19 120-83-207/29/11 13:043620789
Diethylphthalate ND ug/kg 10 08/04/11 13:19 84-66-207/29/11 13:043620559
2,4-Dimethylphenol ND ug/kg 10 08/04/11 13:19 105-67-907/29/11 13:0436201430
Dimethylphthalate ND ug/kg 10 08/04/11 13:19 131-11-307/29/11 13:043620735
Di-n-butylphthalate ND ug/kg 10 08/04/11 13:19 84-74-207/29/11 13:043620592
4,6-Dinitro-2-methylphenol ND ug/kg 10 08/04/11 13:19 534-52-107/29/11 13:047240724
2,4-Dinitrophenol ND ug/kg 10 08/04/11 13:19 51-28-507/29/11 13:0418100592
2,4-Dinitrotoluene ND ug/kg 10 08/04/11 13:19 121-14-207/29/11 13:043620680
2,6-Dinitrotoluene ND ug/kg 10 08/04/11 13:19 606-20-207/29/11 13:043620756
Di-n-octylphthalate ND ug/kg 10 08/04/11 13:19 117-84-007/29/11 13:043620756
bis(2-Ethylhexyl)phthalate ND ug/kg 10 08/04/11 13:19 117-81-707/29/11 13:043620987
Fluoranthene 20300 ug/kg 10 08/04/11 13:19 206-44-007/29/11 13:043620526
Fluorene ND ug/kg 10 08/04/11 13:19 86-73-707/29/11 13:043620745
Hexachloro-1,3-butadiene ND ug/kg 10 08/04/11 13:19 87-68-307/29/11 13:043620625
Hexachlorobenzene ND ug/kg 10 08/04/11 13:19 118-74-107/29/11 13:043620460
Hexachlorocyclopentadiene ND ug/kg 10 08/04/11 13:19 77-47-407/29/11 13:043620669
Hexachloroethane ND ug/kg 10 08/04/11 13:19 67-72-107/29/11 13:043620954
Indeno(1,2,3-cd)pyrene 3990 ug/kg 10 08/04/11 13:19 193-39-5 IO07/29/11 13:043620745
Isophorone ND ug/kg 10 08/04/11 13:19 78-59-107/29/11 13:043620811
1-Methylnaphthalene ND ug/kg 10 08/04/11 13:19 90-12-007/29/11 13:043620943
2-Methylnaphthalene ND ug/kg 10 08/04/11 13:19 91-57-607/29/11 13:043620778
2-Methylphenol(o-Cresol)ND ug/kg 10 08/04/11 13:19 95-48-707/29/11 13:0436201100
3&4-Methylphenol(m&p Cresol)ND ug/kg 10 08/04/11 13:1907/29/11 13:0436201430
Naphthalene ND ug/kg 10 08/04/11 13:19 91-20-307/29/11 13:043620888
2-Nitroaniline ND ug/kg 10 08/04/11 13:19 88-74-407/29/11 13:04181001120
3-Nitroaniline ND ug/kg 10 08/04/11 13:19 99-09-207/29/11 13:0418100987
4-Nitroaniline ND ug/kg 10 08/04/11 13:19 100-01-607/29/11 13:0472401020
Nitrobenzene ND ug/kg 10 08/04/11 13:19 98-95-307/29/11 13:043620987
2-Nitrophenol ND ug/kg 10 08/04/11 13:19 88-75-507/29/11 13:043620877
4-Nitrophenol ND ug/kg 10 08/04/11 13:19 100-02-707/29/11 13:0418100647
N-Nitrosodimethylamine ND ug/kg 10 08/04/11 13:19 62-75-907/29/11 13:0436201170
N-Nitroso-di-n-propylamine ND ug/kg 10 08/04/11 13:19 621-64-707/29/11 13:043620691
N-Nitrosodiphenylamine ND ug/kg 10 08/04/11 13:19 86-30-607/29/11 13:0436201070
Pentachlorophenol ND ug/kg 10 08/04/11 13:19 87-86-507/29/11 13:0418100658
Phenanthrene 3780 ug/kg 10 08/04/11 13:19 85-01-807/29/11 13:043620603
Phenol ND ug/kg 10 08/04/11 13:19 108-95-2 D307/29/11 13:0436201090
Pyrene 17200 ug/kg 10 08/04/11 13:19 129-00-007/29/11 13:043620614
1,2,4-Trichlorobenzene ND ug/kg 10 08/04/11 13:19 120-82-107/29/11 13:043620702
2,4,5-Trichlorophenol ND ug/kg 10 08/04/11 13:19 95-95-407/29/11 13:0436201120
2,4,6-Trichlorophenol ND ug/kg 10 08/04/11 13:19 88-06-207/29/11 13:043620800
Nitrobenzene-d5 (S)0 %10 08/04/11 13:19 4165-60-0 S407/29/11 13:0423-110
2-Fluorobiphenyl (S)0 %10 08/04/11 13:19 321-60-807/29/11 13:0430-110
Terphenyl-d14 (S)0 %10 08/04/11 13:19 1718-51-007/29/11 13:0428-110
Phenol-d6 (S)0 %10 08/04/11 13:19 13127-88-307/29/11 13:0422-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 53 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:COMP 1 Lab ID:9299254023 Collected:07/27/11 09:40 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Fluorophenol (S)0 %10 08/04/11 13:19 367-12-407/29/11 13:0413-110
2,4,6-Tribromophenol (S)0 %10 08/04/11 13:19 118-79-607/29/11 13:0427-110
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 8.8 %1 07/29/11 14:530.10 0.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 30.1 mg/kg 1 08/04/11 15:44 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/04/11 13:17 18540-29-9 N208/04/11 10:431.9 0.19
Sample:COMP 2 Lab ID:9299254024 Collected:07/27/11 09:45 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 1.9 mg/kg 1 08/02/11 15:10 7440-36-008/02/11 09:000.52 0.29
Arsenic 30.9 mg/kg 1 08/02/11 15:10 7440-38-208/02/11 09:000.52 0.33
Beryllium 0.26 mg/kg 1 08/02/11 15:10 7440-41-708/02/11 09:000.10 0.021
Cadmium 2.6 mg/kg 1 08/02/11 15:10 7440-43-908/02/11 09:000.10 0.062
Chromium 34.3 mg/kg 1 08/02/11 15:10 7440-47-308/02/11 09:000.52 0.031
Copper 91.6 mg/kg 1 08/02/11 15:10 7440-50-808/02/11 09:000.52 0.041
Lead 192 mg/kg 1 08/02/11 15:10 7439-92-108/02/11 09:000.52 0.50
Manganese 191 mg/kg 1 08/02/11 15:10 7439-96-508/02/11 09:000.52 0.031
Nickel 5.8 mg/kg 1 08/02/11 15:10 7440-02-008/02/11 09:000.52 0.19
Selenium 0.47J mg/kg 1 08/02/11 15:10 7782-49-208/02/11 09:001.0 0.39
Silver 0.11J mg/kg 1 08/02/11 15:10 7440-22-408/02/11 09:000.52 0.031
Thallium ND mg/kg 1 08/02/11 15:10 7440-28-008/02/11 09:001.0 0.27
Zinc 985 mg/kg 1 08/02/11 15:10 7440-66-608/02/11 09:001.0 0.27
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 10.1 mg/kg 200 08/03/11 12:01 7439-97-608/01/11 14:151.1 0.022
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 10 08/04/11 11:55 83-32-907/29/11 13:043830882
Acenaphthylene ND ug/kg 10 08/04/11 11:55 208-96-807/29/11 13:043830905
Aniline ND ug/kg 10 08/04/11 11:55 62-53-307/29/11 13:0438301030
Anthracene ND ug/kg 10 08/04/11 11:55 120-12-707/29/11 13:043830859
Benzo(a)anthracene 3190J ug/kg 10 08/04/11 11:55 56-55-307/29/11 13:043830708
Benzo(a)pyrene 1870J ug/kg 10 08/04/11 11:55 50-32-807/29/11 13:043830731
Benzo(b)fluoranthene 1690J ug/kg 10 08/04/11 11:55 205-99-207/29/11 13:043830661
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 54 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:COMP 2 Lab ID:9299254024 Collected:07/27/11 09:45 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Benzo(g,h,i)perylene ND ug/kg 10 08/04/11 11:55 191-24-207/29/11 13:043830975
Benzo(k)fluoranthene 1960J ug/kg 10 08/04/11 11:55 207-08-907/29/11 13:043830754
Benzoic Acid ND ug/kg 10 08/04/11 11:55 65-85-007/29/11 13:0419100696
Benzyl alcohol ND ug/kg 10 08/04/11 11:55 100-51-607/29/11 13:047660766
4-Bromophenylphenyl ether ND ug/kg 10 08/04/11 11:55 101-55-307/29/11 13:043830696
Butylbenzylphthalate ND ug/kg 10 08/04/11 11:55 85-68-707/29/11 13:043830812
4-Chloro-3-methylphenol ND ug/kg 10 08/04/11 11:55 59-50-707/29/11 13:047660789
4-Chloroaniline ND ug/kg 10 08/04/11 11:55 106-47-807/29/11 13:04191001070
bis(2-Chloroethoxy)methane ND ug/kg 10 08/04/11 11:55 111-91-107/29/11 13:043830893
bis(2-Chloroethyl) ether ND ug/kg 10 08/04/11 11:55 111-44-407/29/11 13:043830975
bis(2-Chloroisopropyl) ether ND ug/kg 10 08/04/11 11:55 108-60-107/29/11 13:0438301020
2-Chloronaphthalene ND ug/kg 10 08/04/11 11:55 91-58-707/29/11 13:043830754
2-Chlorophenol ND ug/kg 10 08/04/11 11:55 95-57-807/29/11 13:0438301040
4-Chlorophenylphenyl ether ND ug/kg 10 08/04/11 11:55 7005-72-307/29/11 13:043830789
Chrysene 3390J ug/kg 10 08/04/11 11:55 218-01-907/29/11 13:043830510
Dibenz(a,h)anthracene ND ug/kg 10 08/04/11 11:55 53-70-307/29/11 13:043830812
Dibenzofuran ND ug/kg 10 08/04/11 11:55 132-64-907/29/11 13:043830627
1,2-Dichlorobenzene ND ug/kg 10 08/04/11 11:55 95-50-107/29/11 13:0438301020
1,3-Dichlorobenzene ND ug/kg 10 08/04/11 11:55 541-73-107/29/11 13:043830870
1,4-Dichlorobenzene ND ug/kg 10 08/04/11 11:55 106-46-707/29/11 13:0438301080
3,3'-Dichlorobenzidine ND ug/kg 10 08/04/11 11:55 91-94-107/29/11 13:0419100835
2,4-Dichlorophenol ND ug/kg 10 08/04/11 11:55 120-83-207/29/11 13:043830835
Diethylphthalate ND ug/kg 10 08/04/11 11:55 84-66-207/29/11 13:043830592
2,4-Dimethylphenol ND ug/kg 10 08/04/11 11:55 105-67-907/29/11 13:0438301510
Dimethylphthalate ND ug/kg 10 08/04/11 11:55 131-11-307/29/11 13:043830777
Di-n-butylphthalate ND ug/kg 10 08/04/11 11:55 84-74-207/29/11 13:043830627
4,6-Dinitro-2-methylphenol ND ug/kg 10 08/04/11 11:55 534-52-107/29/11 13:047660766
2,4-Dinitrophenol ND ug/kg 10 08/04/11 11:55 51-28-507/29/11 13:0419100627
2,4-Dinitrotoluene ND ug/kg 10 08/04/11 11:55 121-14-207/29/11 13:043830719
2,6-Dinitrotoluene ND ug/kg 10 08/04/11 11:55 606-20-207/29/11 13:043830801
Di-n-octylphthalate ND ug/kg 10 08/04/11 11:55 117-84-007/29/11 13:043830801
bis(2-Ethylhexyl)phthalate ND ug/kg 10 08/04/11 11:55 117-81-707/29/11 13:0438301040
Fluoranthene 1630J ug/kg 10 08/04/11 11:55 206-44-007/29/11 13:043830557
Fluorene ND ug/kg 10 08/04/11 11:55 86-73-707/29/11 13:043830789
Hexachloro-1,3-butadiene ND ug/kg 10 08/04/11 11:55 87-68-307/29/11 13:043830661
Hexachlorobenzene ND ug/kg 10 08/04/11 11:55 118-74-107/29/11 13:043830487
Hexachlorocyclopentadiene ND ug/kg 10 08/04/11 11:55 77-47-407/29/11 13:043830708
Hexachloroethane ND ug/kg 10 08/04/11 11:55 67-72-107/29/11 13:0438301010
Indeno(1,2,3-cd)pyrene ND ug/kg 10 08/04/11 11:55 193-39-507/29/11 13:043830789
Isophorone ND ug/kg 10 08/04/11 11:55 78-59-107/29/11 13:043830859
1-Methylnaphthalene ND ug/kg 10 08/04/11 11:55 90-12-007/29/11 13:043830998
2-Methylnaphthalene ND ug/kg 10 08/04/11 11:55 91-57-607/29/11 13:043830824
2-Methylphenol(o-Cresol)ND ug/kg 10 08/04/11 11:55 95-48-707/29/11 13:0438301160
3&4-Methylphenol(m&p Cresol)ND ug/kg 10 08/04/11 11:5507/29/11 13:0438301510
Naphthalene ND ug/kg 10 08/04/11 11:55 91-20-307/29/11 13:043830940
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 55 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:COMP 2 Lab ID:9299254024 Collected:07/27/11 09:45 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Nitroaniline ND ug/kg 10 08/04/11 11:55 88-74-407/29/11 13:04191001180
3-Nitroaniline ND ug/kg 10 08/04/11 11:55 99-09-207/29/11 13:04191001040
4-Nitroaniline ND ug/kg 10 08/04/11 11:55 100-01-607/29/11 13:0476601080
Nitrobenzene ND ug/kg 10 08/04/11 11:55 98-95-307/29/11 13:0438301040
2-Nitrophenol ND ug/kg 10 08/04/11 11:55 88-75-507/29/11 13:043830928
4-Nitrophenol ND ug/kg 10 08/04/11 11:55 100-02-707/29/11 13:0419100685
N-Nitrosodimethylamine ND ug/kg 10 08/04/11 11:55 62-75-907/29/11 13:0438301240
N-Nitroso-di-n-propylamine ND ug/kg 10 08/04/11 11:55 621-64-707/29/11 13:043830731
N-Nitrosodiphenylamine ND ug/kg 10 08/04/11 11:55 86-30-607/29/11 13:0438301140
Pentachlorophenol ND ug/kg 10 08/04/11 11:55 87-86-507/29/11 13:0419100696
Phenanthrene ND ug/kg 10 08/04/11 11:55 85-01-807/29/11 13:043830638
Phenol ND ug/kg 10 08/04/11 11:55 108-95-2 D307/29/11 13:0438301150
Pyrene 2250J ug/kg 10 08/04/11 11:55 129-00-007/29/11 13:043830650
1,2,4-Trichlorobenzene ND ug/kg 10 08/04/11 11:55 120-82-107/29/11 13:043830743
2,4,5-Trichlorophenol ND ug/kg 10 08/04/11 11:55 95-95-407/29/11 13:0438301180
2,4,6-Trichlorophenol ND ug/kg 10 08/04/11 11:55 88-06-207/29/11 13:043830847
Nitrobenzene-d5 (S)0 %10 08/04/11 11:55 4165-60-0 S407/29/11 13:0423-110
2-Fluorobiphenyl (S)0 %10 08/04/11 11:55 321-60-807/29/11 13:0430-110
Terphenyl-d14 (S)0 %10 08/04/11 11:55 1718-51-007/29/11 13:0428-110
Phenol-d6 (S)0 %10 08/04/11 11:55 13127-88-307/29/11 13:0422-110
2-Fluorophenol (S)0 %10 08/04/11 11:55 367-12-407/29/11 13:0413-110
2,4,6-Tribromophenol (S)0 %10 08/04/11 11:55 118-79-607/29/11 13:0427-110
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 13.8 %1 08/01/11 09:020.10 0.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 34.3 mg/kg 1 08/04/11 15:44 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/04/11 13:17 18540-29-9 N208/04/11 10:431.7 0.17
Sample:COMP 3 Lab ID:9299254025 Collected:07/27/11 10:30 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 0.96 mg/kg 1 08/02/11 15:18 7440-36-008/02/11 09:000.46 0.26
Arsenic 3.3 mg/kg 1 08/02/11 15:18 7440-38-208/02/11 09:000.46 0.30
Beryllium 0.21 mg/kg 1 08/02/11 15:18 7440-41-708/02/11 09:000.093 0.019
Cadmium 1.1 mg/kg 1 08/02/11 15:18 7440-43-908/02/11 09:000.093 0.056
Chromium 20.9 mg/kg 1 08/02/11 15:18 7440-47-308/02/11 09:000.46 0.028
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 56 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:COMP 3 Lab ID:9299254025 Collected:07/27/11 10:30 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Copper 24.8 mg/kg 1 08/02/11 15:18 7440-50-808/02/11 09:000.46 0.037
Lead 59.1 mg/kg 1 08/02/11 15:18 7439-92-108/02/11 09:000.46 0.45
Manganese 85.4 mg/kg 1 08/02/11 15:18 7439-96-508/02/11 09:000.46 0.028
Nickel 3.3 mg/kg 1 08/02/11 15:18 7440-02-008/02/11 09:000.46 0.17
Selenium 0.42J mg/kg 1 08/02/11 15:18 7782-49-208/02/11 09:000.93 0.35
Silver 0.039J mg/kg 1 08/02/11 15:18 7440-22-408/02/11 09:000.46 0.028
Thallium ND mg/kg 1 08/02/11 15:18 7440-28-008/02/11 09:000.93 0.24
Zinc 97.7 mg/kg 1 08/02/11 15:18 7440-66-608/02/11 09:000.93 0.24
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.65 mg/kg 20 08/03/11 12:03 7439-97-608/01/11 14:150.083 0.0017
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 08/04/11 09:17 83-32-907/29/11 13:0437386.0
Acenaphthylene ND ug/kg 1 08/04/11 09:17 208-96-807/29/11 13:0437388.2
Aniline ND ug/kg 1 08/04/11 09:17 62-53-307/29/11 13:04373101
Anthracene ND ug/kg 1 08/04/11 09:17 120-12-707/29/11 13:0437383.7
Benzo(a)anthracene 123J ug/kg 1 08/04/11 09:17 56-55-307/29/11 13:0437369.0
Benzo(a)pyrene 89.4J ug/kg 1 08/04/11 09:17 50-32-807/29/11 13:0437371.3
Benzo(b)fluoranthene 99.7J ug/kg 1 08/04/11 09:17 205-99-207/29/11 13:0437364.5
Benzo(g,h,i)perylene ND ug/kg 1 08/04/11 09:17 191-24-207/29/11 13:0437395.0
Benzo(k)fluoranthene 77.0J ug/kg 1 08/04/11 09:17 207-08-907/29/11 13:0437373.5
Benzoic Acid ND ug/kg 1 08/04/11 09:17 65-85-007/29/11 13:04187067.9
Benzyl alcohol ND ug/kg 1 08/04/11 09:17 100-51-607/29/11 13:0474774.7
4-Bromophenylphenyl ether ND ug/kg 1 08/04/11 09:17 101-55-307/29/11 13:0437367.9
Butylbenzylphthalate 112J ug/kg 1 08/04/11 09:17 85-68-707/29/11 13:0437379.2
4-Chloro-3-methylphenol ND ug/kg 1 08/04/11 09:17 59-50-707/29/11 13:0474776.9
4-Chloroaniline ND ug/kg 1 08/04/11 09:17 106-47-807/29/11 13:041870104
bis(2-Chloroethoxy)methane ND ug/kg 1 08/04/11 09:17 111-91-107/29/11 13:0437387.1
bis(2-Chloroethyl) ether ND ug/kg 1 08/04/11 09:17 111-44-407/29/11 13:0437395.0
bis(2-Chloroisopropyl) ether ND ug/kg 1 08/04/11 09:17 108-60-107/29/11 13:0437399.5
2-Chloronaphthalene ND ug/kg 1 08/04/11 09:17 91-58-707/29/11 13:0437373.5
2-Chlorophenol ND ug/kg 1 08/04/11 09:17 95-57-807/29/11 13:04373102
4-Chlorophenylphenyl ether ND ug/kg 1 08/04/11 09:17 7005-72-307/29/11 13:0437376.9
Chrysene 139J ug/kg 1 08/04/11 09:17 218-01-907/29/11 13:0437349.8
Dibenz(a,h)anthracene ND ug/kg 1 08/04/11 09:17 53-70-307/29/11 13:0437379.2
Dibenzofuran ND ug/kg 1 08/04/11 09:17 132-64-907/29/11 13:0437361.1
1,2-Dichlorobenzene ND ug/kg 1 08/04/11 09:17 95-50-107/29/11 13:0437399.5
1,3-Dichlorobenzene ND ug/kg 1 08/04/11 09:17 541-73-107/29/11 13:0437384.8
1,4-Dichlorobenzene ND ug/kg 1 08/04/11 09:17 106-46-707/29/11 13:04373105
3,3'-Dichlorobenzidine ND ug/kg 1 08/04/11 09:17 91-94-107/29/11 13:04187081.4
2,4-Dichlorophenol ND ug/kg 1 08/04/11 09:17 120-83-207/29/11 13:0437381.4
Diethylphthalate ND ug/kg 1 08/04/11 09:17 84-66-207/29/11 13:0437357.7
2,4-Dimethylphenol ND ug/kg 1 08/04/11 09:17 105-67-907/29/11 13:04373147
Dimethylphthalate ND ug/kg 1 08/04/11 09:17 131-11-307/29/11 13:0437375.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 57 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:COMP 3 Lab ID:9299254025 Collected:07/27/11 10:30 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Di-n-butylphthalate ND ug/kg 1 08/04/11 09:17 84-74-207/29/11 13:0437361.1
4,6-Dinitro-2-methylphenol ND ug/kg 1 08/04/11 09:17 534-52-107/29/11 13:0474774.7
2,4-Dinitrophenol ND ug/kg 1 08/04/11 09:17 51-28-507/29/11 13:04187061.1
2,4-Dinitrotoluene ND ug/kg 1 08/04/11 09:17 121-14-207/29/11 13:0437370.1
2,6-Dinitrotoluene ND ug/kg 1 08/04/11 09:17 606-20-207/29/11 13:0437378.0
Di-n-octylphthalate ND ug/kg 1 08/04/11 09:17 117-84-007/29/11 13:0437378.0
bis(2-Ethylhexyl)phthalate 105J ug/kg 1 08/04/11 09:17 117-81-707/29/11 13:04373102
Fluoranthene 132J ug/kg 1 08/04/11 09:17 206-44-007/29/11 13:0437354.3
Fluorene ND ug/kg 1 08/04/11 09:17 86-73-707/29/11 13:0437376.9
Hexachloro-1,3-butadiene ND ug/kg 1 08/04/11 09:17 87-68-307/29/11 13:0437364.5
Hexachlorobenzene ND ug/kg 1 08/04/11 09:17 118-74-107/29/11 13:0437347.5
Hexachlorocyclopentadiene ND ug/kg 1 08/04/11 09:17 77-47-407/29/11 13:0437369.0
Hexachloroethane ND ug/kg 1 08/04/11 09:17 67-72-107/29/11 13:0437398.4
Indeno(1,2,3-cd)pyrene ND ug/kg 1 08/04/11 09:17 193-39-507/29/11 13:0437376.9
Isophorone ND ug/kg 1 08/04/11 09:17 78-59-107/29/11 13:0437383.7
1-Methylnaphthalene ND ug/kg 1 08/04/11 09:17 90-12-007/29/11 13:0437397.3
2-Methylnaphthalene ND ug/kg 1 08/04/11 09:17 91-57-607/29/11 13:0437380.3
2-Methylphenol(o-Cresol)ND ug/kg 1 08/04/11 09:17 95-48-707/29/11 13:04373113
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 08/04/11 09:1707/29/11 13:04373147
Naphthalene ND ug/kg 1 08/04/11 09:17 91-20-307/29/11 13:0437391.6
2-Nitroaniline ND ug/kg 1 08/04/11 09:17 88-74-407/29/11 13:041870115
3-Nitroaniline ND ug/kg 1 08/04/11 09:17 99-09-207/29/11 13:041870102
4-Nitroaniline ND ug/kg 1 08/04/11 09:17 100-01-607/29/11 13:04747105
Nitrobenzene ND ug/kg 1 08/04/11 09:17 98-95-307/29/11 13:04373102
2-Nitrophenol ND ug/kg 1 08/04/11 09:17 88-75-507/29/11 13:0437390.5
4-Nitrophenol 246J ug/kg 1 08/04/11 09:17 100-02-707/29/11 13:04187066.7
N-Nitrosodimethylamine ND ug/kg 1 08/04/11 09:17 62-75-907/29/11 13:04373121
N-Nitroso-di-n-propylamine ND ug/kg 1 08/04/11 09:17 621-64-707/29/11 13:0437371.3
N-Nitrosodiphenylamine ND ug/kg 1 08/04/11 09:17 86-30-607/29/11 13:04373111
Pentachlorophenol 92.4J ug/kg 1 08/04/11 09:17 87-86-507/29/11 13:04187067.9
Phenanthrene 89.8J ug/kg 1 08/04/11 09:17 85-01-807/29/11 13:0437362.2
Phenol ND ug/kg 1 08/04/11 09:17 108-95-207/29/11 13:04373112
Pyrene 141J ug/kg 1 08/04/11 09:17 129-00-007/29/11 13:0437363.3
1,2,4-Trichlorobenzene ND ug/kg 1 08/04/11 09:17 120-82-107/29/11 13:0437372.4
2,4,5-Trichlorophenol ND ug/kg 1 08/04/11 09:17 95-95-407/29/11 13:04373115
2,4,6-Trichlorophenol ND ug/kg 1 08/04/11 09:17 88-06-207/29/11 13:0437382.6
Nitrobenzene-d5 (S)25 %1 08/04/11 09:17 4165-60-007/29/11 13:0423-110
2-Fluorobiphenyl (S)27 %1 08/04/11 09:17 321-60-8 S007/29/11 13:0430-110
Terphenyl-d14 (S)33 %1 08/04/11 09:17 1718-51-007/29/11 13:0428-110
Phenol-d6 (S)25 %1 08/04/11 09:17 13127-88-307/29/11 13:0422-110
2-Fluorophenol (S)22 %1 08/04/11 09:17 367-12-407/29/11 13:0413-110
2,4,6-Tribromophenol (S)24 %1 08/04/11 09:17 118-79-6 S007/29/11 13:0427-110
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 11.6 %1 08/01/11 09:020.10 0.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 58 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:COMP 3 Lab ID:9299254025 Collected:07/27/11 10:30 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 20.9 mg/kg 1 08/04/11 15:44 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/04/11 13:23 18540-29-9 N208/04/11 10:431.5 0.15
Sample:COMP 4 Lab ID:9299254026 Collected:07/27/11 10:35 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 0.59 mg/kg 1 08/02/11 15:22 7440-36-008/02/11 09:000.57 0.32
Arsenic 6.1 mg/kg 1 08/02/11 15:22 7440-38-208/02/11 09:000.57 0.36
Beryllium 0.28 mg/kg 1 08/02/11 15:22 7440-41-708/02/11 09:000.11 0.023
Cadmium 0.51 mg/kg 1 08/02/11 15:22 7440-43-908/02/11 09:000.11 0.068
Chromium 29.7 mg/kg 1 08/02/11 15:22 7440-47-308/02/11 09:000.57 0.034
Copper 29.3 mg/kg 1 08/02/11 15:22 7440-50-808/02/11 09:000.57 0.045
Lead 150 mg/kg 1 08/02/11 15:22 7439-92-108/02/11 09:000.57 0.54
Manganese 111 mg/kg 1 08/02/11 15:22 7439-96-508/02/11 09:000.57 0.034
Nickel 4.0 mg/kg 1 08/02/11 15:22 7440-02-008/02/11 09:000.57 0.20
Selenium ND mg/kg 1 08/02/11 15:22 7782-49-208/02/11 09:001.1 0.43
Silver ND mg/kg 1 08/02/11 15:22 7440-22-408/02/11 09:000.57 0.034
Thallium ND mg/kg 1 08/02/11 15:22 7440-28-008/02/11 09:001.1 0.30
Zinc 139 mg/kg 1 08/02/11 15:22 7440-66-608/02/11 09:001.1 0.30
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 4.2 mg/kg 100 08/03/11 13:50 7439-97-608/01/11 14:150.57 0.011
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 08/04/11 09:44 83-32-907/29/11 13:0439089.7
Acenaphthylene ND ug/kg 1 08/04/11 09:44 208-96-807/29/11 13:0439092.1
Aniline ND ug/kg 1 08/04/11 09:44 62-53-307/29/11 13:04390105
Anthracene ND ug/kg 1 08/04/11 09:44 120-12-707/29/11 13:0439087.4
Benzo(a)anthracene 201J ug/kg 1 08/04/11 09:44 56-55-307/29/11 13:0439072.0
Benzo(a)pyrene 201J ug/kg 1 08/04/11 09:44 50-32-807/29/11 13:0439074.4
Benzo(b)fluoranthene 238J ug/kg 1 08/04/11 09:44 205-99-207/29/11 13:0439067.3
Benzo(g,h,i)perylene 172J ug/kg 1 08/04/11 09:44 191-24-207/29/11 13:0439099.2
Benzo(k)fluoranthene 204J ug/kg 1 08/04/11 09:44 207-08-907/29/11 13:0439076.8
Benzoic Acid ND ug/kg 1 08/04/11 09:44 65-85-007/29/11 13:04195070.8
Benzyl alcohol ND ug/kg 1 08/04/11 09:44 100-51-607/29/11 13:0477977.9
4-Bromophenylphenyl ether ND ug/kg 1 08/04/11 09:44 101-55-307/29/11 13:0439070.8
Butylbenzylphthalate ND ug/kg 1 08/04/11 09:44 85-68-707/29/11 13:0439082.7
4-Chloro-3-methylphenol ND ug/kg 1 08/04/11 09:44 59-50-707/29/11 13:0477980.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 59 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:COMP 4 Lab ID:9299254026 Collected:07/27/11 10:35 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
4-Chloroaniline ND ug/kg 1 08/04/11 09:44 106-47-807/29/11 13:041950109
bis(2-Chloroethoxy)methane ND ug/kg 1 08/04/11 09:44 111-91-107/29/11 13:0439090.9
bis(2-Chloroethyl) ether ND ug/kg 1 08/04/11 09:44 111-44-407/29/11 13:0439099.2
bis(2-Chloroisopropyl) ether ND ug/kg 1 08/04/11 09:44 108-60-107/29/11 13:04390104
2-Chloronaphthalene ND ug/kg 1 08/04/11 09:44 91-58-707/29/11 13:0439076.8
2-Chlorophenol ND ug/kg 1 08/04/11 09:44 95-57-807/29/11 13:04390106
4-Chlorophenylphenyl ether ND ug/kg 1 08/04/11 09:44 7005-72-307/29/11 13:0439080.3
Chrysene 271J ug/kg 1 08/04/11 09:44 218-01-907/29/11 13:0439052.0
Dibenz(a,h)anthracene ND ug/kg 1 08/04/11 09:44 53-70-307/29/11 13:0439082.7
Dibenzofuran ND ug/kg 1 08/04/11 09:44 132-64-907/29/11 13:0439063.8
1,2-Dichlorobenzene ND ug/kg 1 08/04/11 09:44 95-50-107/29/11 13:04390104
1,3-Dichlorobenzene ND ug/kg 1 08/04/11 09:44 541-73-107/29/11 13:0439088.6
1,4-Dichlorobenzene ND ug/kg 1 08/04/11 09:44 106-46-707/29/11 13:04390110
3,3'-Dichlorobenzidine ND ug/kg 1 08/04/11 09:44 91-94-107/29/11 13:04195085.0
2,4-Dichlorophenol ND ug/kg 1 08/04/11 09:44 120-83-207/29/11 13:0439085.0
Diethylphthalate ND ug/kg 1 08/04/11 09:44 84-66-207/29/11 13:0439060.2
2,4-Dimethylphenol ND ug/kg 1 08/04/11 09:44 105-67-907/29/11 13:04390154
Dimethylphthalate ND ug/kg 1 08/04/11 09:44 131-11-307/29/11 13:0439079.1
Di-n-butylphthalate ND ug/kg 1 08/04/11 09:44 84-74-207/29/11 13:0439063.8
4,6-Dinitro-2-methylphenol ND ug/kg 1 08/04/11 09:44 534-52-107/29/11 13:0477977.9
2,4-Dinitrophenol ND ug/kg 1 08/04/11 09:44 51-28-507/29/11 13:04195063.8
2,4-Dinitrotoluene ND ug/kg 1 08/04/11 09:44 121-14-207/29/11 13:0439073.2
2,6-Dinitrotoluene ND ug/kg 1 08/04/11 09:44 606-20-207/29/11 13:0439081.5
Di-n-octylphthalate ND ug/kg 1 08/04/11 09:44 117-84-007/29/11 13:0439081.5
bis(2-Ethylhexyl)phthalate 284J ug/kg 1 08/04/11 09:44 117-81-707/29/11 13:04390106
Fluoranthene 473 ug/kg 1 08/04/11 09:44 206-44-007/29/11 13:0439056.7
Fluorene ND ug/kg 1 08/04/11 09:44 86-73-707/29/11 13:0439080.3
Hexachloro-1,3-butadiene ND ug/kg 1 08/04/11 09:44 87-68-307/29/11 13:0439067.3
Hexachlorobenzene ND ug/kg 1 08/04/11 09:44 118-74-107/29/11 13:0439049.6
Hexachlorocyclopentadiene ND ug/kg 1 08/04/11 09:44 77-47-407/29/11 13:0439072.0
Hexachloroethane ND ug/kg 1 08/04/11 09:44 67-72-107/29/11 13:04390103
Indeno(1,2,3-cd)pyrene 155J ug/kg 1 08/04/11 09:44 193-39-507/29/11 13:0439080.3
Isophorone ND ug/kg 1 08/04/11 09:44 78-59-107/29/11 13:0439087.4
1-Methylnaphthalene ND ug/kg 1 08/04/11 09:44 90-12-007/29/11 13:04390102
2-Methylnaphthalene ND ug/kg 1 08/04/11 09:44 91-57-607/29/11 13:0439083.8
2-Methylphenol(o-Cresol)ND ug/kg 1 08/04/11 09:44 95-48-707/29/11 13:04390118
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 08/04/11 09:4407/29/11 13:04390154
Naphthalene ND ug/kg 1 08/04/11 09:44 91-20-307/29/11 13:0439095.6
2-Nitroaniline ND ug/kg 1 08/04/11 09:44 88-74-407/29/11 13:041950120
3-Nitroaniline ND ug/kg 1 08/04/11 09:44 99-09-207/29/11 13:041950106
4-Nitroaniline ND ug/kg 1 08/04/11 09:44 100-01-607/29/11 13:04779110
Nitrobenzene ND ug/kg 1 08/04/11 09:44 98-95-307/29/11 13:04390106
2-Nitrophenol ND ug/kg 1 08/04/11 09:44 88-75-507/29/11 13:0439094.5
4-Nitrophenol 200J ug/kg 1 08/04/11 09:44 100-02-707/29/11 13:04195069.7
N-Nitrosodimethylamine ND ug/kg 1 08/04/11 09:44 62-75-907/29/11 13:04390126
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 60 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:COMP 4 Lab ID:9299254026 Collected:07/27/11 10:35 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
N-Nitroso-di-n-propylamine ND ug/kg 1 08/04/11 09:44 621-64-707/29/11 13:0439074.4
N-Nitrosodiphenylamine ND ug/kg 1 08/04/11 09:44 86-30-607/29/11 13:04390116
Pentachlorophenol 80.4J ug/kg 1 08/04/11 09:44 87-86-507/29/11 13:04195070.8
Phenanthrene 307J ug/kg 1 08/04/11 09:44 85-01-807/29/11 13:0439064.9
Phenol ND ug/kg 1 08/04/11 09:44 108-95-2 1g07/29/11 13:04390117
Pyrene 387J ug/kg 1 08/04/11 09:44 129-00-007/29/11 13:0439066.1
1,2,4-Trichlorobenzene ND ug/kg 1 08/04/11 09:44 120-82-107/29/11 13:0439075.6
2,4,5-Trichlorophenol ND ug/kg 1 08/04/11 09:44 95-95-407/29/11 13:04390120
2,4,6-Trichlorophenol ND ug/kg 1 08/04/11 09:44 88-06-207/29/11 13:0439086.2
Nitrobenzene-d5 (S)5 %1 08/04/11 09:44 4165-60-0 2g07/29/11 13:0423-110
2-Fluorobiphenyl (S)8 %1 08/04/11 09:44 321-60-8 2g07/29/11 13:0430-110
Terphenyl-d14 (S)15 %1 08/04/11 09:44 1718-51-0 2g07/29/11 13:0428-110
Phenol-d6 (S)7 %1 08/04/11 09:44 13127-88-3 2g07/29/11 13:0422-110
2-Fluorophenol (S)2 %1 08/04/11 09:44 367-12-4 2g07/29/11 13:0413-110
2,4,6-Tribromophenol (S)5 %1 08/04/11 09:44 118-79-6 2g07/29/11 13:0427-110
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 15.3 %1 08/01/11 09:020.10 0.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 29.7 mg/kg 1 08/04/11 15:44 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/04/11 13:23 18540-29-9 N208/04/11 10:432.2 0.22
Sample:COMP 5 Lab ID:9299254027 Collected:07/27/11 11:35 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 1.3 mg/kg 1 08/02/11 15:25 7440-36-008/02/11 09:000.58 0.32
Arsenic 4.4 mg/kg 1 08/02/11 15:25 7440-38-208/02/11 09:000.58 0.37
Beryllium 0.25 mg/kg 1 08/02/11 15:25 7440-41-708/02/11 09:000.12 0.023
Cadmium 2.7 mg/kg 1 08/02/11 15:25 7440-43-908/02/11 09:000.12 0.069
Chromium 14.3 mg/kg 1 08/02/11 15:25 7440-47-308/02/11 09:000.58 0.035
Copper 87.4 mg/kg 1 08/02/11 15:25 7440-50-808/02/11 09:000.58 0.046
Lead 156 mg/kg 1 08/02/11 15:25 7439-92-108/02/11 09:000.58 0.55
Manganese 237 mg/kg 1 08/02/11 15:25 7439-96-508/02/11 09:000.58 0.035
Nickel 5.6 mg/kg 1 08/02/11 15:25 7440-02-008/02/11 09:000.58 0.21
Selenium 0.61J mg/kg 1 08/02/11 15:25 7782-49-208/02/11 09:001.2 0.44
Silver 0.23J mg/kg 1 08/02/11 15:25 7440-22-408/02/11 09:000.58 0.035
Thallium ND mg/kg 1 08/02/11 15:25 7440-28-008/02/11 09:001.2 0.30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 61 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:COMP 5 Lab ID:9299254027 Collected:07/27/11 11:35 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Zinc 1400 mg/kg 10 08/03/11 16:20 7440-66-608/02/11 09:0011.5 3.0
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 1.0 mg/kg 20 08/03/11 12:17 7439-97-608/01/11 14:150.11 0.0021
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 08/04/11 10:12 83-32-907/29/11 13:0438889.3
Acenaphthylene ND ug/kg 1 08/04/11 10:12 208-96-807/29/11 13:0438891.7
Aniline ND ug/kg 1 08/04/11 10:12 62-53-307/29/11 13:04388105
Anthracene ND ug/kg 1 08/04/11 10:12 120-12-707/29/11 13:0438887.0
Benzo(a)anthracene 169J ug/kg 1 08/04/11 10:12 56-55-307/29/11 13:0438871.7
Benzo(a)pyrene 158J ug/kg 1 08/04/11 10:12 50-32-807/29/11 13:0438874.0
Benzo(b)fluoranthene 163J ug/kg 1 08/04/11 10:12 205-99-207/29/11 13:0438867.0
Benzo(g,h,i)perylene 131J ug/kg 1 08/04/11 10:12 191-24-207/29/11 13:0438898.7
Benzo(k)fluoranthene 143J ug/kg 1 08/04/11 10:12 207-08-907/29/11 13:0438876.4
Benzoic Acid ND ug/kg 1 08/04/11 10:12 65-85-007/29/11 13:04194070.5
Benzyl alcohol ND ug/kg 1 08/04/11 10:12 100-51-607/29/11 13:0477677.6
4-Bromophenylphenyl ether ND ug/kg 1 08/04/11 10:12 101-55-307/29/11 13:0438870.5
Butylbenzylphthalate ND ug/kg 1 08/04/11 10:12 85-68-707/29/11 13:0438882.3
4-Chloro-3-methylphenol ND ug/kg 1 08/04/11 10:12 59-50-707/29/11 13:0477679.9
4-Chloroaniline ND ug/kg 1 08/04/11 10:12 106-47-807/29/11 13:041940108
bis(2-Chloroethoxy)methane ND ug/kg 1 08/04/11 10:12 111-91-107/29/11 13:0438890.5
bis(2-Chloroethyl) ether ND ug/kg 1 08/04/11 10:12 111-44-407/29/11 13:0438898.7
bis(2-Chloroisopropyl) ether ND ug/kg 1 08/04/11 10:12 108-60-107/29/11 13:04388103
2-Chloronaphthalene ND ug/kg 1 08/04/11 10:12 91-58-707/29/11 13:0438876.4
2-Chlorophenol ND ug/kg 1 08/04/11 10:12 95-57-807/29/11 13:04388106
4-Chlorophenylphenyl ether ND ug/kg 1 08/04/11 10:12 7005-72-307/29/11 13:0438879.9
Chrysene 213J ug/kg 1 08/04/11 10:12 218-01-907/29/11 13:0438851.7
Dibenz(a,h)anthracene ND ug/kg 1 08/04/11 10:12 53-70-307/29/11 13:0438882.3
Dibenzofuran ND ug/kg 1 08/04/11 10:12 132-64-907/29/11 13:0438863.5
1,2-Dichlorobenzene ND ug/kg 1 08/04/11 10:12 95-50-107/29/11 13:04388103
1,3-Dichlorobenzene ND ug/kg 1 08/04/11 10:12 541-73-107/29/11 13:0438888.1
1,4-Dichlorobenzene ND ug/kg 1 08/04/11 10:12 106-46-707/29/11 13:04388109
3,3'-Dichlorobenzidine ND ug/kg 1 08/04/11 10:12 91-94-107/29/11 13:04194084.6
2,4-Dichlorophenol ND ug/kg 1 08/04/11 10:12 120-83-207/29/11 13:0438884.6
Diethylphthalate ND ug/kg 1 08/04/11 10:12 84-66-207/29/11 13:0438859.9
2,4-Dimethylphenol ND ug/kg 1 08/04/11 10:12 105-67-907/29/11 13:04388153
Dimethylphthalate ND ug/kg 1 08/04/11 10:12 131-11-307/29/11 13:0438878.7
Di-n-butylphthalate ND ug/kg 1 08/04/11 10:12 84-74-207/29/11 13:0438863.5
4,6-Dinitro-2-methylphenol ND ug/kg 1 08/04/11 10:12 534-52-107/29/11 13:0477677.6
2,4-Dinitrophenol ND ug/kg 1 08/04/11 10:12 51-28-507/29/11 13:04194063.5
2,4-Dinitrotoluene ND ug/kg 1 08/04/11 10:12 121-14-207/29/11 13:0438872.9
2,6-Dinitrotoluene ND ug/kg 1 08/04/11 10:12 606-20-207/29/11 13:0438881.1
Di-n-octylphthalate ND ug/kg 1 08/04/11 10:12 117-84-007/29/11 13:0438881.1
bis(2-Ethylhexyl)phthalate ND ug/kg 1 08/04/11 10:12 117-81-707/29/11 13:04388106
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 62 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:COMP 5 Lab ID:9299254027 Collected:07/27/11 11:35 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Fluoranthene 313J ug/kg 1 08/04/11 10:12 206-44-007/29/11 13:0438856.4
Fluorene ND ug/kg 1 08/04/11 10:12 86-73-707/29/11 13:0438879.9
Hexachloro-1,3-butadiene ND ug/kg 1 08/04/11 10:12 87-68-307/29/11 13:0438867.0
Hexachlorobenzene ND ug/kg 1 08/04/11 10:12 118-74-107/29/11 13:0438849.4
Hexachlorocyclopentadiene ND ug/kg 1 08/04/11 10:12 77-47-407/29/11 13:0438871.7
Hexachloroethane ND ug/kg 1 08/04/11 10:12 67-72-107/29/11 13:04388102
Indeno(1,2,3-cd)pyrene 108J ug/kg 1 08/04/11 10:12 193-39-507/29/11 13:0438879.9
Isophorone ND ug/kg 1 08/04/11 10:12 78-59-107/29/11 13:0438887.0
1-Methylnaphthalene ND ug/kg 1 08/04/11 10:12 90-12-007/29/11 13:04388101
2-Methylnaphthalene ND ug/kg 1 08/04/11 10:12 91-57-607/29/11 13:0438883.4
2-Methylphenol(o-Cresol)ND ug/kg 1 08/04/11 10:12 95-48-707/29/11 13:04388118
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 08/04/11 10:1207/29/11 13:04388153
Naphthalene ND ug/kg 1 08/04/11 10:12 91-20-307/29/11 13:0438895.2
2-Nitroaniline ND ug/kg 1 08/04/11 10:12 88-74-407/29/11 13:041940120
3-Nitroaniline ND ug/kg 1 08/04/11 10:12 99-09-207/29/11 13:041940106
4-Nitroaniline ND ug/kg 1 08/04/11 10:12 100-01-607/29/11 13:04776109
Nitrobenzene ND ug/kg 1 08/04/11 10:12 98-95-307/29/11 13:04388106
2-Nitrophenol ND ug/kg 1 08/04/11 10:12 88-75-507/29/11 13:0438894.0
4-Nitrophenol 79.3J ug/kg 1 08/04/11 10:12 100-02-707/29/11 13:04194069.3
N-Nitrosodimethylamine ND ug/kg 1 08/04/11 10:12 62-75-907/29/11 13:04388126
N-Nitroso-di-n-propylamine ND ug/kg 1 08/04/11 10:12 621-64-707/29/11 13:0438874.0
N-Nitrosodiphenylamine ND ug/kg 1 08/04/11 10:12 86-30-607/29/11 13:04388115
Pentachlorophenol ND ug/kg 1 08/04/11 10:12 87-86-507/29/11 13:04194070.5
Phenanthrene 205J ug/kg 1 08/04/11 10:12 85-01-807/29/11 13:0438864.6
Phenol ND ug/kg 1 08/04/11 10:12 108-95-207/29/11 13:04388116
Pyrene 259J ug/kg 1 08/04/11 10:12 129-00-007/29/11 13:0438865.8
1,2,4-Trichlorobenzene ND ug/kg 1 08/04/11 10:12 120-82-107/29/11 13:0438875.2
2,4,5-Trichlorophenol ND ug/kg 1 08/04/11 10:12 95-95-407/29/11 13:04388120
2,4,6-Trichlorophenol ND ug/kg 1 08/04/11 10:12 88-06-207/29/11 13:0438885.8
Nitrobenzene-d5 (S)55 %1 08/04/11 10:12 4165-60-007/29/11 13:0423-110
2-Fluorobiphenyl (S)56 %1 08/04/11 10:12 321-60-807/29/11 13:0430-110
Terphenyl-d14 (S)56 %1 08/04/11 10:12 1718-51-007/29/11 13:0428-110
Phenol-d6 (S)60 %1 08/04/11 10:12 13127-88-307/29/11 13:0422-110
2-Fluorophenol (S)53 %1 08/04/11 10:12 367-12-407/29/11 13:0413-110
2,4,6-Tribromophenol (S)49 %1 08/04/11 10:12 118-79-607/29/11 13:0427-110
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 14.9 %1 08/01/11 09:020.10 0.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 14.3 mg/kg 1 08/04/11 15:44 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/04/11 13:23 18540-29-9 N208/04/11 10:432.4 0.24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 63 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:COMP 6 Lab ID:9299254028 Collected:07/27/11 11:40 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 0.58 mg/kg 1 08/02/11 15:29 7440-36-008/02/11 09:000.58 0.32
Arsenic 3.2 mg/kg 1 08/02/11 15:29 7440-38-208/02/11 09:000.58 0.37
Beryllium 0.33 mg/kg 1 08/02/11 15:29 7440-41-708/02/11 09:000.12 0.023
Cadmium 1.1 mg/kg 1 08/02/11 15:29 7440-43-908/02/11 09:000.12 0.069
Chromium 37.3 mg/kg 1 08/02/11 15:29 7440-47-308/02/11 09:000.58 0.035
Copper 35.8 mg/kg 1 08/02/11 15:29 7440-50-808/02/11 09:000.58 0.046
Lead 58.7 mg/kg 1 08/02/11 15:29 7439-92-108/02/11 09:000.58 0.56
Manganese 305 mg/kg 1 08/02/11 15:29 7439-96-508/02/11 09:000.58 0.035
Nickel 3.8 mg/kg 1 08/02/11 15:29 7440-02-008/02/11 09:000.58 0.21
Selenium 0.92J mg/kg 1 08/02/11 15:29 7782-49-208/02/11 09:001.2 0.44
Silver ND mg/kg 1 08/02/11 15:29 7440-22-408/02/11 09:000.58 0.035
Thallium ND mg/kg 1 08/02/11 15:29 7440-28-008/02/11 09:001.2 0.30
Zinc 196 mg/kg 1 08/02/11 15:29 7440-66-608/02/11 09:001.2 0.30
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 1.6 mg/kg 20 08/03/11 12:19 7439-97-608/01/11 14:150.099 0.0020
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 10 08/04/11 10:39 83-32-907/29/11 13:04191004400
Acenaphthylene ND ug/kg 10 08/04/11 10:39 208-96-807/29/11 13:04191004520
Aniline ND ug/kg 10 08/04/11 10:39 62-53-307/29/11 13:04191005150
Anthracene ND ug/kg 10 08/04/11 10:39 120-12-707/29/11 13:04191004290
Benzo(a)anthracene ND ug/kg 10 08/04/11 10:39 56-55-307/29/11 13:04191003530
Benzo(a)pyrene ND ug/kg 10 08/04/11 10:39 50-32-807/29/11 13:04191003650
Benzo(b)fluoranthene ND ug/kg 10 08/04/11 10:39 205-99-207/29/11 13:04191003300
Benzo(g,h,i)perylene ND ug/kg 10 08/04/11 10:39 191-24-207/29/11 13:04191004860
Benzo(k)fluoranthene ND ug/kg 10 08/04/11 10:39 207-08-907/29/11 13:04191003760
Benzoic Acid ND ug/kg 10 08/04/11 10:39 65-85-007/29/11 13:04956003470
Benzyl alcohol ND ug/kg 10 08/04/11 10:39 100-51-607/29/11 13:04382003820
4-Bromophenylphenyl ether ND ug/kg 10 08/04/11 10:39 101-55-307/29/11 13:04191003470
Butylbenzylphthalate ND ug/kg 10 08/04/11 10:39 85-68-707/29/11 13:04191004050
4-Chloro-3-methylphenol ND ug/kg 10 08/04/11 10:39 59-50-707/29/11 13:04382003940
4-Chloroaniline ND ug/kg 10 08/04/11 10:39 106-47-807/29/11 13:04956005330
bis(2-Chloroethoxy)methane ND ug/kg 10 08/04/11 10:39 111-91-107/29/11 13:04191004460
bis(2-Chloroethyl) ether ND ug/kg 10 08/04/11 10:39 111-44-407/29/11 13:04191004860
bis(2-Chloroisopropyl) ether ND ug/kg 10 08/04/11 10:39 108-60-107/29/11 13:04191005100
2-Chloronaphthalene ND ug/kg 10 08/04/11 10:39 91-58-707/29/11 13:04191003760
2-Chlorophenol ND ug/kg 10 08/04/11 10:39 95-57-807/29/11 13:04191005210
4-Chlorophenylphenyl ether ND ug/kg 10 08/04/11 10:39 7005-72-307/29/11 13:04191003940
Chrysene ND ug/kg 10 08/04/11 10:39 218-01-907/29/11 13:04191002550
Dibenz(a,h)anthracene ND ug/kg 10 08/04/11 10:39 53-70-307/29/11 13:04191004050
Dibenzofuran ND ug/kg 10 08/04/11 10:39 132-64-907/29/11 13:04191003130
1,2-Dichlorobenzene ND ug/kg 10 08/04/11 10:39 95-50-107/29/11 13:04191005100
1,3-Dichlorobenzene ND ug/kg 10 08/04/11 10:39 541-73-107/29/11 13:04191004340
1,4-Dichlorobenzene ND ug/kg 10 08/04/11 10:39 106-46-707/29/11 13:04191005390
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 64 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:COMP 6 Lab ID:9299254028 Collected:07/27/11 11:40 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3,3'-Dichlorobenzidine ND ug/kg 10 08/04/11 10:39 91-94-107/29/11 13:04956004170
2,4-Dichlorophenol ND ug/kg 10 08/04/11 10:39 120-83-207/29/11 13:04191004170
Diethylphthalate ND ug/kg 10 08/04/11 10:39 84-66-207/29/11 13:04191002950
2,4-Dimethylphenol ND ug/kg 10 08/04/11 10:39 105-67-907/29/11 13:04191007530
Dimethylphthalate ND ug/kg 10 08/04/11 10:39 131-11-307/29/11 13:04191003880
Di-n-butylphthalate ND ug/kg 10 08/04/11 10:39 84-74-207/29/11 13:04191003130
4,6-Dinitro-2-methylphenol ND ug/kg 10 08/04/11 10:39 534-52-107/29/11 13:04382003820
2,4-Dinitrophenol ND ug/kg 10 08/04/11 10:39 51-28-507/29/11 13:04956003130
2,4-Dinitrotoluene ND ug/kg 10 08/04/11 10:39 121-14-207/29/11 13:04191003590
2,6-Dinitrotoluene ND ug/kg 10 08/04/11 10:39 606-20-207/29/11 13:04191004000
Di-n-octylphthalate ND ug/kg 10 08/04/11 10:39 117-84-007/29/11 13:04191004000
bis(2-Ethylhexyl)phthalate ND ug/kg 10 08/04/11 10:39 117-81-707/29/11 13:04191005210
Fluoranthene ND ug/kg 10 08/04/11 10:39 206-44-007/29/11 13:04191002780
Fluorene ND ug/kg 10 08/04/11 10:39 86-73-707/29/11 13:04191003940
Hexachloro-1,3-butadiene ND ug/kg 10 08/04/11 10:39 87-68-307/29/11 13:04191003300
Hexachlorobenzene ND ug/kg 10 08/04/11 10:39 118-74-107/29/11 13:04191002430
Hexachlorocyclopentadiene ND ug/kg 10 08/04/11 10:39 77-47-407/29/11 13:04191003530
Hexachloroethane ND ug/kg 10 08/04/11 10:39 67-72-107/29/11 13:04191005040
Indeno(1,2,3-cd)pyrene ND ug/kg 10 08/04/11 10:39 193-39-507/29/11 13:04191003940
Isophorone ND ug/kg 10 08/04/11 10:39 78-59-107/29/11 13:04191004290
1-Methylnaphthalene ND ug/kg 10 08/04/11 10:39 90-12-007/29/11 13:04191004980
2-Methylnaphthalene ND ug/kg 10 08/04/11 10:39 91-57-607/29/11 13:04191004110
2-Methylphenol(o-Cresol)ND ug/kg 10 08/04/11 10:39 95-48-707/29/11 13:04191005790
3&4-Methylphenol(m&p Cresol)ND ug/kg 10 08/04/11 10:3907/29/11 13:04191007530
Naphthalene ND ug/kg 10 08/04/11 10:39 91-20-307/29/11 13:04191004690
2-Nitroaniline ND ug/kg 10 08/04/11 10:39 88-74-407/29/11 13:04956005910
3-Nitroaniline ND ug/kg 10 08/04/11 10:39 99-09-207/29/11 13:04956005210
4-Nitroaniline ND ug/kg 10 08/04/11 10:39 100-01-607/29/11 13:04382005390
Nitrobenzene ND ug/kg 10 08/04/11 10:39 98-95-307/29/11 13:04191005210
2-Nitrophenol ND ug/kg 10 08/04/11 10:39 88-75-507/29/11 13:04191004630
4-Nitrophenol ND ug/kg 10 08/04/11 10:39 100-02-707/29/11 13:04956003420
N-Nitrosodimethylamine ND ug/kg 10 08/04/11 10:39 62-75-907/29/11 13:04191006200
N-Nitroso-di-n-propylamine ND ug/kg 10 08/04/11 10:39 621-64-707/29/11 13:04191003650
N-Nitrosodiphenylamine ND ug/kg 10 08/04/11 10:39 86-30-607/29/11 13:04191005680
Pentachlorophenol ND ug/kg 10 08/04/11 10:39 87-86-507/29/11 13:04956003470
Phenanthrene ND ug/kg 10 08/04/11 10:39 85-01-807/29/11 13:04191003190
Phenol ND ug/kg 10 08/04/11 10:39 108-95-2 D3,P307/29/11 13:04191005730
Pyrene ND ug/kg 10 08/04/11 10:39 129-00-007/29/11 13:04191003240
1,2,4-Trichlorobenzene ND ug/kg 10 08/04/11 10:39 120-82-107/29/11 13:04191003710
2,4,5-Trichlorophenol ND ug/kg 10 08/04/11 10:39 95-95-407/29/11 13:04191005910
2,4,6-Trichlorophenol ND ug/kg 10 08/04/11 10:39 88-06-207/29/11 13:04191004230
Nitrobenzene-d5 (S)0 %10 08/04/11 10:39 4165-60-0 S407/29/11 13:0423-110
2-Fluorobiphenyl (S)0 %10 08/04/11 10:39 321-60-807/29/11 13:0430-110
Terphenyl-d14 (S)0 %10 08/04/11 10:39 1718-51-007/29/11 13:0428-110
Phenol-d6 (S)0 %10 08/04/11 10:39 13127-88-307/29/11 13:0422-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 65 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Sample:COMP 6 Lab ID:9299254028 Collected:07/27/11 11:40 Received:07/28/11 14:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Fluorophenol (S)0 %10 08/04/11 10:39 367-12-407/29/11 13:0413-110
2,4,6-Tribromophenol (S)0 %10 08/04/11 10:39 118-79-607/29/11 13:0427-110
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 13.7 %1 08/01/11 09:030.10 0.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 37.3 mg/kg 1 08/04/11 15:44 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/04/11 13:23 18540-29-9 N208/04/11 10:432.3 0.23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 66 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/8819
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:9299254016, 9299254017, 9299254018, 9299254019, 9299254020, 9299254021, 9299254022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:641212
Associated Lab Samples:9299254016, 9299254017, 9299254018, 9299254019, 9299254020, 9299254021, 9299254022
Matrix:Solid
Analyzed
Antimony mg/kg ND 0.50 08/02/11 16:46
Arsenic mg/kg ND 0.50 08/02/11 16:46
Beryllium mg/kg ND 0.10 08/02/11 16:46
Cadmium mg/kg ND 0.10 08/02/11 16:46
Chromium mg/kg 0.065J 0.50 08/02/11 16:46
Copper mg/kg ND 0.50 08/02/11 16:46
Lead mg/kg ND 0.50 08/02/11 16:46
Manganese mg/kg 0.12J 0.50 08/02/11 16:46
Nickel mg/kg ND 0.50 08/02/11 16:46
Selenium mg/kg ND 1.0 08/02/11 16:46
Silver mg/kg ND 0.50 08/02/11 16:46
Thallium mg/kg ND 1.0 08/02/11 16:46
Zinc mg/kg ND 1.0 08/02/11 16:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
641213LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony mg/kg 48.050 96 80-120
Arsenic mg/kg 48.450 97 80-120
Beryllium mg/kg 50.450 101 80-120
Cadmium mg/kg 49.050 98 80-120
Chromium mg/kg 49.850 100 80-120
Copper mg/kg 49.750 99 80-120
Lead mg/kg 49.850 100 80-120
Manganese mg/kg 49.550 99 80-120
Nickel mg/kg 49.650 99 80-120
Selenium mg/kg 48.750 97 80-120
Silver mg/kg 24.725 99 80-120
Thallium mg/kg 48.650 97 80-120
Zinc mg/kg 49.150 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
641214MATRIX SPIKE SAMPLE:
MSSpike
Result
9298895001
Antimony mg/kg 67.172.6 92 75-125ND
Arsenic mg/kg 72.272.6 97 75-1251.9
Beryllium mg/kg 71.972.6 99 75-125ND
Cadmium mg/kg 68.172.6 94 75-125ND
Chromium mg/kg 76.572.6 96 75-1257.1
Copper mg/kg 139 M172.6 71 75-12587.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 67 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
641214MATRIX SPIKE SAMPLE:
MSSpike
Result
9298895001
Lead mg/kg 77.772.6 93 75-12510.5
Manganese mg/kg 94.572.6 106 75-12517.9
Nickel mg/kg 71.372.6 96 75-1251.8
Selenium mg/kg 72.072.6 99 75-125ND
Silver mg/kg 35.336.4 97 75-125ND
Thallium mg/kg 65.472.6 89 75-1250.39J
Zinc mg/kg 78.972.6 101 75-1255.6
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9298895002
641215SAMPLE DUPLICATE:
Antimony mg/kg ND 20ND
Arsenic mg/kg 2.3 D668201.1
Beryllium mg/kg ND 20ND
Cadmium mg/kg ND 20ND
Chromium mg/kg 8.8 D6312012.0
Copper mg/kg 74.7 12 2066.1
Lead mg/kg 15.6 D6392010.5
Manganese mg/kg 33.7 D6822014.2
Nickel mg/kg 2.5 D679205.8
Selenium mg/kg ND 20ND
Silver mg/kg ND 20ND
Thallium mg/kg ND 20ND
Zinc mg/kg 9.2 14 2010.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 68 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/8820
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:9299254023, 9299254024, 9299254025, 9299254026, 9299254027, 9299254028
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:641217
Associated Lab Samples:9299254023, 9299254024, 9299254025, 9299254026, 9299254027, 9299254028
Matrix:Solid
Analyzed
Antimony mg/kg ND 0.50 08/02/11 14:20
Arsenic mg/kg ND 0.50 08/02/11 14:20
Beryllium mg/kg ND 0.10 08/02/11 14:20
Cadmium mg/kg ND 0.10 08/02/11 14:20
Chromium mg/kg 0.045J 0.50 08/02/11 14:20
Copper mg/kg ND 0.50 08/02/11 14:20
Lead mg/kg ND 0.50 08/02/11 14:20
Manganese mg/kg 0.078J 0.50 08/02/11 14:20
Nickel mg/kg ND 0.50 08/02/11 14:20
Selenium mg/kg ND 1.0 08/02/11 14:20
Silver mg/kg ND 0.50 08/02/11 14:20
Thallium mg/kg ND 1.0 08/02/11 14:20
Zinc mg/kg ND 1.0 08/02/11 14:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
641218LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony mg/kg 48.850 98 80-120
Arsenic mg/kg 49.450 99 80-120
Beryllium mg/kg 50.950 102 80-120
Cadmium mg/kg 49.950 100 80-120
Chromium mg/kg 50.850 102 80-120
Copper mg/kg 50.250 100 80-120
Lead mg/kg 50.850 102 80-120
Manganese mg/kg 50.350 101 80-120
Nickel mg/kg 50.250 100 80-120
Selenium mg/kg 49.550 99 80-120
Silver mg/kg 25.025 100 80-120
Thallium mg/kg 49.250 98 80-120
Zinc mg/kg 50.850 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
641219MATRIX SPIKE SAMPLE:
MSSpike
Result
9299254023
Antimony mg/kg 42.648.9 78 75-1254.2
Arsenic mg/kg 156 M148.9 249 75-12534.3
Beryllium mg/kg 44.348.9 90 75-1250.27
Cadmium mg/kg 54.948.9 76 75-12517.8
Chromium mg/kg 82.848.9 108 75-12530.1
Copper mg/kg 214 M148.9 47 75-125191
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 69 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
641219MATRIX SPIKE SAMPLE:
MSSpike
Result
9299254023
Lead mg/kg 324 M148.9 -134 75-125389
Manganese mg/kg 365 M148.9 229 75-125253
Nickel mg/kg 51.848.9 85 75-12510
Selenium mg/kg 44.248.9 87 75-1251.7
Silver mg/kg 24.424.4 98 75-1250.42J
Thallium mg/kg 36.1 M148.9 74 75-125ND
Zinc mg/kg 2600 M648.9 -1468 75-1253320
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9299254024
641220SAMPLE DUPLICATE:
Antimony mg/kg 2.1 14 201.9
Arsenic mg/kg 50.1 D6482030.9
Beryllium mg/kg 0.34 D628200.26
Cadmium mg/kg 4.5 D656202.6
Chromium mg/kg 44.9 D6272034.3
Copper mg/kg 135 D6382091.6
Lead mg/kg 242 D62320192
Manganese mg/kg 215 12 20191
Nickel mg/kg 8.7 D640205.8
Selenium mg/kg ND 200.47J
Silver mg/kg 0.23J 200.11J
Thallium mg/kg ND 20ND
Zinc mg/kg 1520 D64320985
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 70 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/8901
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:9299254001, 9299254002, 9299254003, 9299254004, 9299254013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:647562
Associated Lab Samples:9299254001, 9299254002, 9299254003, 9299254004, 9299254013
Matrix:Solid
Analyzed
Antimony mg/kg ND 0.50 08/16/11 18:32
Arsenic mg/kg ND 0.50 08/16/11 18:32
Beryllium mg/kg ND 0.10 08/16/11 18:32
Cadmium mg/kg ND 0.10 08/16/11 18:32
Chromium mg/kg 0.080J 0.50 08/16/11 18:32
Copper mg/kg ND 0.50 08/16/11 18:32
Lead mg/kg ND 0.50 08/16/11 18:32
Manganese mg/kg 0.072J 0.50 08/16/11 18:32
Nickel mg/kg ND 0.50 08/16/11 18:32
Selenium mg/kg ND 1.0 08/16/11 18:32
Silver mg/kg ND 0.50 08/16/11 18:32
Thallium mg/kg 0.32J 1.0 08/16/11 18:32
Zinc mg/kg ND 1.0 08/16/11 18:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
647563LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony mg/kg 50.050 100 80-120
Arsenic mg/kg 51.150 102 80-120
Beryllium mg/kg 53.850 108 80-120
Cadmium mg/kg 52.150 104 80-120
Chromium mg/kg 53.050 106 80-120
Copper mg/kg 50.550 101 80-120
Lead mg/kg 52.450 105 80-120
Manganese mg/kg 51.450 103 80-120
Nickel mg/kg 52.450 105 80-120
Selenium mg/kg 52.650 105 80-120
Silver mg/kg 25.725 103 80-120
Thallium mg/kg 50.650 101 80-120
Zinc mg/kg 52.850 106 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
647564MATRIX SPIKE SAMPLE:
MSSpike
Result
9299254001
Antimony mg/kg 55.754.2 94 75-1254.7
Arsenic mg/kg 11354.2 112 75-12552.2
Beryllium mg/kg 53.754.2 99 75-1250.34
Cadmium mg/kg 52.954.2 93 75-1252.3
Chromium mg/kg 80.654.2 102 75-12525.2
Copper mg/kg 13454.2 121 75-12569.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 71 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
647564MATRIX SPIKE SAMPLE:
MSSpike
Result
9299254001
Lead mg/kg 539 M154.2 380 75-125334
Manganese mg/kg 406 M154.2 195 75-125300
Nickel mg/kg 61.754.2 93 75-12511.4
Selenium mg/kg 51.554.2 93 75-1251.3
Silver mg/kg 27.927.1 102 75-1250.43J
Thallium mg/kg 42.954.2 78 75-1250.52J
Zinc mg/kg 710 M154.2 177 75-125614
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9299254002
647565SAMPLE DUPLICATE:
Antimony mg/kg 3.2 D633202.3
Arsenic mg/kg 41.4 D6292030.8
Beryllium mg/kg 0.35 18 200.30
Cadmium mg/kg 2.0 D637201.4
Chromium mg/kg 28.6 D6392019.2
Copper mg/kg 61.2 D6262047.0
Lead mg/kg 249 D62120201
Manganese mg/kg 300 6 20283
Nickel mg/kg 11.9 D626209.1
Selenium mg/kg 1.6 D630201.2
Silver mg/kg 0.67 200.42J
Thallium mg/kg ND 20ND
Zinc mg/kg 405 D63020298
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 72 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/3648
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:9299254016, 9299254017, 9299254018, 9299254019, 9299254020, 9299254021, 9299254022, 9299254023,
9299254024, 9299254025, 9299254026, 9299254027, 9299254028
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:641149
Associated Lab Samples:9299254016, 9299254017, 9299254018, 9299254019, 9299254020, 9299254021, 9299254022, 9299254023,
9299254024, 9299254025, 9299254026, 9299254027, 9299254028
Matrix:Solid
Analyzed
Mercury mg/kg 0.00037J 0.0050 08/02/11 14:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
641150LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.057.067 85 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
641151MATRIX SPIKE SAMPLE:
MSSpike
Result
9299190005
Mercury mg/kg 0.063.06 89 75-1250.010
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
641153MATRIX SPIKE SAMPLE:
MSSpike
Result
9299254024
Mercury mg/kg 7.4 M6.075 -3565 75-12510.1
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9299190006
641152SAMPLE DUPLICATE:
Mercury mg/kg 0.0018J 200.0017J
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9299254025
641154SAMPLE DUPLICATE:
Mercury mg/kg 0.60 9 200.65
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 73 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/3677
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:9299254001, 9299254002, 9299254003, 9299254004, 9299254013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:645884
Associated Lab Samples:9299254001, 9299254002, 9299254003, 9299254004, 9299254013
Matrix:Solid
Analyzed
Mercury mg/kg 0.00016J 0.0050 08/12/11 11:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
645885LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.058.067 87 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
645886MATRIX SPIKE SAMPLE:
MSSpike
Result
9299254001
Mercury mg/kg 1.1 M6.07 192 75-1250.94
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
645888MATRIX SPIKE SAMPLE:
MSSpike
Result
9299890004
Mercury mg/kg 0.065.067 88 75-1250.0064
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9299254002
645887SAMPLE DUPLICATE:
Mercury mg/kg 1.4 D641202.1
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9299890005
645889SAMPLE DUPLICATE:
Mercury mg/kg 0.029 D637200.041
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 74 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/14354
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:9299254016, 9299254017, 9299254018, 9299254019, 9299254021, 9299254022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:640140
Associated Lab Samples:9299254016, 9299254017, 9299254018, 9299254021, 9299254022
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 08/02/11 12:34
1,2-Dichlorobenzene ug/kg ND 330 08/02/11 12:34
1,3-Dichlorobenzene ug/kg ND 330 08/02/11 12:34
1,4-Dichlorobenzene ug/kg ND 330 08/02/11 12:34
1-Methylnaphthalene ug/kg ND 330 08/02/11 12:34
2,4,5-Trichlorophenol ug/kg ND 330 08/02/11 12:34
2,4,6-Trichlorophenol ug/kg ND 330 08/02/11 12:34
2,4-Dichlorophenol ug/kg ND 330 08/02/11 12:34
2,4-Dimethylphenol ug/kg ND 330 08/02/11 12:34
2,4-Dinitrophenol ug/kg ND 1650 08/02/11 12:34
2,4-Dinitrotoluene ug/kg ND 330 08/02/11 12:34
2,6-Dinitrotoluene ug/kg ND 330 08/02/11 12:34
2-Chloronaphthalene ug/kg ND 330 08/02/11 12:34
2-Chlorophenol ug/kg ND 330 08/02/11 12:34
2-Methylnaphthalene ug/kg ND 330 08/02/11 12:34
2-Methylphenol(o-Cresol)ug/kg ND 330 08/02/11 12:34
2-Nitroaniline ug/kg ND 1650 08/02/11 12:34
2-Nitrophenol ug/kg ND 330 08/02/11 12:34
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 08/02/11 12:34
3,3'-Dichlorobenzidine ug/kg 78.2J 1650 08/02/11 12:34
3-Nitroaniline ug/kg ND 1650 08/02/11 12:34
4,6-Dinitro-2-methylphenol ug/kg ND 660 08/02/11 12:34
4-Bromophenylphenyl ether ug/kg ND 330 08/02/11 12:34
4-Chloro-3-methylphenol ug/kg ND 660 08/02/11 12:34
4-Chloroaniline ug/kg ND 1650 08/02/11 12:34
4-Chlorophenylphenyl ether ug/kg ND 330 08/02/11 12:34
4-Nitroaniline ug/kg ND 660 08/02/11 12:34
4-Nitrophenol ug/kg 99.5J 1650 08/02/11 12:34
Acenaphthene ug/kg ND 330 08/02/11 12:34
Acenaphthylene ug/kg ND 330 08/02/11 12:34
Aniline ug/kg ND 330 08/02/11 12:34
Anthracene ug/kg ND 330 08/02/11 12:34
Benzo(a)anthracene ug/kg ND 330 08/02/11 12:34
Benzo(a)pyrene ug/kg ND 330 08/02/11 12:34
Benzo(b)fluoranthene ug/kg ND 330 08/02/11 12:34
Benzo(g,h,i)perylene ug/kg ND 330 08/02/11 12:34
Benzo(k)fluoranthene ug/kg ND 330 08/02/11 12:34
Benzoic Acid ug/kg ND 1650 08/02/11 12:34
Benzyl alcohol ug/kg ND 660 08/02/11 12:34
bis(2-Chloroethoxy)methane ug/kg ND 330 08/02/11 12:34
bis(2-Chloroethyl) ether ug/kg ND 330 08/02/11 12:34
bis(2-Chloroisopropyl) ether ug/kg ND 330 08/02/11 12:34
bis(2-Ethylhexyl)phthalate ug/kg ND 330 08/02/11 12:34
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 75 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:640140
Associated Lab Samples:9299254016, 9299254017, 9299254018, 9299254021, 9299254022
Matrix:Solid
Analyzed
Butylbenzylphthalate ug/kg ND 330 08/02/11 12:34
Chrysene ug/kg ND 330 08/02/11 12:34
Di-n-butylphthalate ug/kg ND 330 08/02/11 12:34
Di-n-octylphthalate ug/kg ND 330 08/02/11 12:34
Dibenz(a,h)anthracene ug/kg ND 330 08/02/11 12:34
Dibenzofuran ug/kg ND 330 08/02/11 12:34
Diethylphthalate ug/kg ND 330 08/02/11 12:34
Dimethylphthalate ug/kg ND 330 08/02/11 12:34
Fluoranthene ug/kg ND 330 08/02/11 12:34
Fluorene ug/kg ND 330 08/02/11 12:34
Hexachloro-1,3-butadiene ug/kg ND 330 08/02/11 12:34
Hexachlorobenzene ug/kg ND 330 08/02/11 12:34
Hexachlorocyclopentadiene ug/kg ND 330 08/02/11 12:34
Hexachloroethane ug/kg ND 330 08/02/11 12:34
Indeno(1,2,3-cd)pyrene ug/kg ND 330 08/02/11 12:34
Isophorone ug/kg ND 330 08/02/11 12:34
N-Nitroso-di-n-propylamine ug/kg ND 330 08/02/11 12:34
N-Nitrosodimethylamine ug/kg ND 330 08/02/11 12:34
N-Nitrosodiphenylamine ug/kg ND 330 08/02/11 12:34
Naphthalene ug/kg ND 330 08/02/11 12:34
Nitrobenzene ug/kg ND 330 08/02/11 12:34
Pentachlorophenol ug/kg ND 1650 08/02/11 12:34
Phenanthrene ug/kg ND 330 08/02/11 12:34
Phenol ug/kg ND 330 08/02/11 12:34
Pyrene ug/kg ND 330 08/02/11 12:34
2,4,6-Tribromophenol (S)%70 27-110 08/02/11 12:34
2-Fluorobiphenyl (S)%54 30-110 08/02/11 12:34
2-Fluorophenol (S)%52 13-110 08/02/11 12:34
Nitrobenzene-d5 (S)%51 23-110 08/02/11 12:34
Phenol-d6 (S)%52 22-110 08/02/11 12:34
Terphenyl-d14 (S)%72 28-110 08/02/11 12:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640141LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 10001670 60 39-101
1,2-Dichlorobenzene ug/kg 9411670 56 36-110
1,3-Dichlorobenzene ug/kg 9221670 55 35-110
1,4-Dichlorobenzene ug/kg 9561670 57 35-110
1-Methylnaphthalene ug/kg 10301670 62 45-105
2,4,5-Trichlorophenol ug/kg 10601670 64 48-109
2,4,6-Trichlorophenol ug/kg 12001670 72 45-111
2,4-Dichlorophenol ug/kg 10701670 64 51-116
2,4-Dimethylphenol ug/kg 10501670 63 42-103
2,4-Dinitrophenol ug/kg 63308330 76 28-103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 76 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640141LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dinitrotoluene ug/kg 12401670 75 46-114
2,6-Dinitrotoluene ug/kg 12301670 74 48-112
2-Chloronaphthalene ug/kg 10501670 63 44-105
2-Chlorophenol ug/kg 9671670 58 36-110
2-Methylnaphthalene ug/kg 10401670 62 39-112
2-Methylphenol(o-Cresol)ug/kg 8941670 54 39-101
2-Nitroaniline ug/kg 22303330 67 44-111
2-Nitrophenol ug/kg 10301670 62 41-100
3&4-Methylphenol(m&p Cresol)ug/kg 9251670 56 43-103
3,3'-Dichlorobenzidine ug/kg 21403330 64 10-150
3-Nitroaniline ug/kg 23603330 71 35-110
4,6-Dinitro-2-methylphenol ug/kg 27003330 81 38-118
4-Bromophenylphenyl ether ug/kg 11701670 70 47-115
4-Chloro-3-methylphenol ug/kg 23303330 70 43-127
4-Chloroaniline ug/kg 22303330 67 34-109
4-Chlorophenylphenyl ether ug/kg 11801670 71 44-115
4-Nitroaniline ug/kg 25303330 76 37-111
4-Nitrophenol ug/kg 60508330 73 21-152
Acenaphthene ug/kg 11101670 66 38-117
Acenaphthylene ug/kg 10701670 64 46-107
Aniline ug/kg 8651670 52 29-110
Anthracene ug/kg 11301670 68 50-110
Benzo(a)anthracene ug/kg 11201670 67 47-116
Benzo(a)pyrene ug/kg 10801670 65 47-106
Benzo(b)fluoranthene ug/kg 11001670 66 47-109
Benzo(g,h,i)perylene ug/kg 11101670 66 39-115
Benzo(k)fluoranthene ug/kg 10701670 64 45-117
Benzoic Acid ug/kg 41208330 49 16-110
Benzyl alcohol ug/kg 20603330 62 38-105
bis(2-Chloroethoxy)methane ug/kg 9441670 57 39-110
bis(2-Chloroethyl) ether ug/kg 8771670 53 19-119
bis(2-Chloroisopropyl) ether ug/kg 7901670 47 21-110
bis(2-Ethylhexyl)phthalate ug/kg 11201670 67 35-116
Butylbenzylphthalate ug/kg 10901670 65 38-110
Chrysene ug/kg 11201670 67 49-110
Di-n-butylphthalate ug/kg 11401670 68 43-109
Di-n-octylphthalate ug/kg 11101670 67 37-109
Dibenz(a,h)anthracene ug/kg 11301670 68 43-116
Dibenzofuran ug/kg 11501670 69 45-106
Diethylphthalate ug/kg 11601670 69 41-114
Dimethylphthalate ug/kg 11301670 68 43-110
Fluoranthene ug/kg 11901670 72 50-114
Fluorene ug/kg 11401670 69 46-114
Hexachloro-1,3-butadiene ug/kg 9481670 57 28-111
Hexachlorobenzene ug/kg 11701670 70 46-120
Hexachlorocyclopentadiene ug/kg 10901670 66 18-119
Hexachloroethane ug/kg 8821670 53 33-110
Indeno(1,2,3-cd)pyrene ug/kg 11301670 68 42-115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 77 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640141LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/kg 10901670 65 44-109
N-Nitroso-di-n-propylamine ug/kg 9701670 58 43-104
N-Nitrosodimethylamine ug/kg 8811670 53 29-110
N-Nitrosodiphenylamine ug/kg 11401670 68 48-113
Naphthalene ug/kg 9381670 56 41-110
Nitrobenzene ug/kg 8971670 54 38-110
Pentachlorophenol ug/kg 28303330 85 32-128
Phenanthrene ug/kg 11001670 66 50-110
Phenol ug/kg 9631670 58 28-106
Pyrene ug/kg 10701670 64 45-114
2,4,6-Tribromophenol (S)%81 27-110
2-Fluorobiphenyl (S)%62 30-110
2-Fluorophenol (S)%57 13-110
Nitrobenzene-d5 (S)%55 23-110
Phenol-d6 (S)%58 22-110
Terphenyl-d14 (S)%69 28-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 78 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/14362
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:9299254023, 9299254024, 9299254025, 9299254026, 9299254027, 9299254028
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:640690
Associated Lab Samples:9299254023, 9299254024, 9299254025, 9299254026, 9299254027, 9299254028
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 08/03/11 10:59
1,2-Dichlorobenzene ug/kg ND 330 08/03/11 10:59
1,3-Dichlorobenzene ug/kg ND 330 08/03/11 10:59
1,4-Dichlorobenzene ug/kg ND 330 08/03/11 10:59
1-Methylnaphthalene ug/kg ND 330 08/03/11 10:59
2,4,5-Trichlorophenol ug/kg ND 330 08/03/11 10:59
2,4,6-Trichlorophenol ug/kg ND 330 08/03/11 10:59
2,4-Dichlorophenol ug/kg ND 330 08/03/11 10:59
2,4-Dimethylphenol ug/kg ND 330 08/03/11 10:59
2,4-Dinitrophenol ug/kg ND 1650 08/03/11 10:59
2,4-Dinitrotoluene ug/kg ND 330 08/03/11 10:59
2,6-Dinitrotoluene ug/kg ND 330 08/03/11 10:59
2-Chloronaphthalene ug/kg ND 330 08/03/11 10:59
2-Chlorophenol ug/kg ND 330 08/03/11 10:59
2-Methylnaphthalene ug/kg ND 330 08/03/11 10:59
2-Methylphenol(o-Cresol)ug/kg ND 330 08/03/11 10:59
2-Nitroaniline ug/kg ND 1650 08/03/11 10:59
2-Nitrophenol ug/kg ND 330 08/03/11 10:59
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 08/03/11 10:59
3,3'-Dichlorobenzidine ug/kg ND 1650 08/03/11 10:59
3-Nitroaniline ug/kg ND 1650 08/03/11 10:59
4,6-Dinitro-2-methylphenol ug/kg ND 660 08/03/11 10:59
4-Bromophenylphenyl ether ug/kg ND 330 08/03/11 10:59
4-Chloro-3-methylphenol ug/kg ND 660 08/03/11 10:59
4-Chloroaniline ug/kg ND 1650 08/03/11 10:59
4-Chlorophenylphenyl ether ug/kg ND 330 08/03/11 10:59
4-Nitroaniline ug/kg ND 660 08/03/11 10:59
4-Nitrophenol ug/kg ND 1650 08/03/11 10:59
Acenaphthene ug/kg ND 330 08/03/11 10:59
Acenaphthylene ug/kg ND 330 08/03/11 10:59
Aniline ug/kg ND 330 08/03/11 10:59
Anthracene ug/kg ND 330 08/03/11 10:59
Benzo(a)anthracene ug/kg ND 330 08/03/11 10:59
Benzo(a)pyrene ug/kg ND 330 08/03/11 10:59
Benzo(b)fluoranthene ug/kg ND 330 08/03/11 10:59
Benzo(g,h,i)perylene ug/kg ND 330 08/03/11 10:59
Benzo(k)fluoranthene ug/kg ND 330 08/03/11 10:59
Benzoic Acid ug/kg ND 1650 08/03/11 10:59
Benzyl alcohol ug/kg ND 660 08/03/11 10:59
bis(2-Chloroethoxy)methane ug/kg ND 330 08/03/11 10:59
bis(2-Chloroethyl) ether ug/kg ND 330 08/03/11 10:59
bis(2-Chloroisopropyl) ether ug/kg ND 330 08/03/11 10:59
bis(2-Ethylhexyl)phthalate ug/kg ND 330 08/03/11 10:59
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 79 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:640690
Associated Lab Samples:9299254023, 9299254024, 9299254025, 9299254026, 9299254027, 9299254028
Matrix:Solid
Analyzed
Butylbenzylphthalate ug/kg ND 330 08/03/11 10:59
Chrysene ug/kg ND 330 08/03/11 10:59
Di-n-butylphthalate ug/kg ND 330 08/03/11 10:59
Di-n-octylphthalate ug/kg ND 330 08/03/11 10:59
Dibenz(a,h)anthracene ug/kg ND 330 08/03/11 10:59
Dibenzofuran ug/kg ND 330 08/03/11 10:59
Diethylphthalate ug/kg ND 330 08/03/11 10:59
Dimethylphthalate ug/kg ND 330 08/03/11 10:59
Fluoranthene ug/kg ND 330 08/03/11 10:59
Fluorene ug/kg ND 330 08/03/11 10:59
Hexachloro-1,3-butadiene ug/kg ND 330 08/03/11 10:59
Hexachlorobenzene ug/kg ND 330 08/03/11 10:59
Hexachlorocyclopentadiene ug/kg ND 330 08/03/11 10:59
Hexachloroethane ug/kg ND 330 08/03/11 10:59
Indeno(1,2,3-cd)pyrene ug/kg ND 330 08/03/11 10:59
Isophorone ug/kg ND 330 08/03/11 10:59
N-Nitroso-di-n-propylamine ug/kg ND 330 08/03/11 10:59
N-Nitrosodimethylamine ug/kg ND 330 08/03/11 10:59
N-Nitrosodiphenylamine ug/kg ND 330 08/03/11 10:59
Naphthalene ug/kg ND 330 08/03/11 10:59
Nitrobenzene ug/kg ND 330 08/03/11 10:59
Pentachlorophenol ug/kg ND 1650 08/03/11 10:59
Phenanthrene ug/kg ND 330 08/03/11 10:59
Phenol ug/kg ND 330 08/03/11 10:59
Pyrene ug/kg ND 330 08/03/11 10:59
2,4,6-Tribromophenol (S)%57 27-110 08/03/11 10:59
2-Fluorobiphenyl (S)%59 30-110 08/03/11 10:59
2-Fluorophenol (S)%61 13-110 08/03/11 10:59
Nitrobenzene-d5 (S)%62 23-110 08/03/11 10:59
Phenol-d6 (S)%66 22-110 08/03/11 10:59
Terphenyl-d14 (S)%72 28-110 08/03/11 10:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640691LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 10601670 64 39-101
1,2-Dichlorobenzene ug/kg 11801670 71 36-110
1,3-Dichlorobenzene ug/kg 11601670 70 35-110
1,4-Dichlorobenzene ug/kg 11501670 69 35-110
1-Methylnaphthalene ug/kg 11901670 71 45-105
2,4,5-Trichlorophenol ug/kg 10901670 65 48-109
2,4,6-Trichlorophenol ug/kg 12701670 76 45-111
2,4-Dichlorophenol ug/kg 12301670 74 51-116
2,4-Dimethylphenol ug/kg 13301670 80 42-103
2,4-Dinitrophenol ug/kg 58208330 70 28-103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 80 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640691LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dinitrotoluene ug/kg 13801670 83 46-114
2,6-Dinitrotoluene ug/kg 13401670 81 48-112
2-Chloronaphthalene ug/kg 12201670 73 44-105
2-Chlorophenol ug/kg 12701670 76 36-110
2-Methylnaphthalene ug/kg 12101670 72 39-112
2-Methylphenol(o-Cresol)ug/kg 12301670 74 39-101
2-Nitroaniline ug/kg 30803330 92 44-111
2-Nitrophenol ug/kg 12501670 75 41-100
3&4-Methylphenol(m&p Cresol)ug/kg 12801670 77 43-103
3,3'-Dichlorobenzidine ug/kg 22503330 67 10-150
3-Nitroaniline ug/kg 27803330 84 35-110
4,6-Dinitro-2-methylphenol ug/kg 26603330 80 38-118
4-Bromophenylphenyl ether ug/kg 11001670 66 47-115
4-Chloro-3-methylphenol ug/kg 28203330 85 43-127
4-Chloroaniline ug/kg 25603330 77 34-109
4-Chlorophenylphenyl ether ug/kg 11901670 71 44-115
4-Nitroaniline ug/kg 29903330 90 37-111
4-Nitrophenol ug/kg 72508330 87 21-152
Acenaphthene ug/kg 12901670 77 38-117
Acenaphthylene ug/kg 12701670 76 46-107
Aniline ug/kg 11801670 71 29-110
Anthracene ug/kg 13701670 82 50-110
Benzo(a)anthracene ug/kg 13101670 79 47-116
Benzo(a)pyrene ug/kg 12901670 77 47-106
Benzo(b)fluoranthene ug/kg 12401670 75 47-109
Benzo(g,h,i)perylene ug/kg 11401670 69 39-115
Benzo(k)fluoranthene ug/kg 13201670 79 45-117
Benzoic Acid ug/kg 47308330 57 16-110
Benzyl alcohol ug/kg 27603330 83 38-105
bis(2-Chloroethoxy)methane ug/kg 12301670 74 39-110
bis(2-Chloroethyl) ether ug/kg 12201670 73 19-119
bis(2-Chloroisopropyl) ether ug/kg 12701670 76 21-110
bis(2-Ethylhexyl)phthalate ug/kg 16001670 96 35-116
Butylbenzylphthalate ug/kg 15801670 95 38-110
Chrysene ug/kg 13201670 79 49-110
Di-n-butylphthalate ug/kg 14501670 87 43-109
Di-n-octylphthalate ug/kg 15901670 95 37-109
Dibenz(a,h)anthracene ug/kg 11401670 69 43-116
Dibenzofuran ug/kg 12801670 77 45-106
Diethylphthalate ug/kg 13101670 79 41-114
Dimethylphthalate ug/kg 12301670 74 43-110
Fluoranthene ug/kg 13301670 80 50-114
Fluorene ug/kg 12601670 75 46-114
Hexachloro-1,3-butadiene ug/kg 9541670 57 28-111
Hexachlorobenzene ug/kg 10101670 60 46-120
Hexachlorocyclopentadiene ug/kg 10801670 65 18-119
Hexachloroethane ug/kg 11601670 70 33-110
Indeno(1,2,3-cd)pyrene ug/kg 11701670 70 42-115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 81 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640691LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/kg 13701670 82 44-109
N-Nitroso-di-n-propylamine ug/kg 13501670 81 43-104
N-Nitrosodimethylamine ug/kg 11901670 71 29-110
N-Nitrosodiphenylamine ug/kg 13201670 79 48-113
Naphthalene ug/kg 11601670 70 41-110
Nitrobenzene ug/kg 11901670 71 38-110
Pentachlorophenol ug/kg 25603330 77 32-128
Phenanthrene ug/kg 13001670 78 50-110
Phenol ug/kg 13301670 80 28-106
Pyrene ug/kg 13301670 80 45-114
2,4,6-Tribromophenol (S)%66 27-110
2-Fluorobiphenyl (S)%69 30-110
2-Fluorophenol (S)%74 13-110
Nitrobenzene-d5 (S)%70 23-110
Phenol-d6 (S)%82 22-110
Terphenyl-d14 (S)%76 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
640692MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299306001
640693
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1950 53 18-11962 16 301950ND10301210
1,2-Dichlorobenzene ug/kg 1950 57 50-11068 17 301950ND11201330
1,3-Dichlorobenzene ug/kg 1950 57 27-11068 17 301950ND11101320
1,4-Dichlorobenzene ug/kg 1950 57 28-11067 17 301950ND11101310
1-Methylnaphthalene ug/kg 1950 60 24-11667 11 301950ND11601300
2,4,5-Trichlorophenol ug/kg 1950 55 28-11062 12 301950ND10601200
2,4,6-Trichlorophenol ug/kg 1950 62 17-11768 10 301950ND12101330
2,4-Dichlorophenol ug/kg 1950 62 21-12870 13 301950ND12001370
2,4-Dimethylphenol ug/kg 1950 65 10-12075 14 301950ND12701460
2,4-Dinitrophenol ug/kg 9720 48 10-10753 9 309720ND47105160
2,4-Dinitrotoluene ug/kg 1950 71 36-10978 10 301950ND13801530
2,6-Dinitrotoluene ug/kg 1950 69 32-11076 10 301950ND13401470
2-Chloronaphthalene ug/kg 1950 61 30-10769 12 301950ND11901350
2-Chlorophenol ug/kg 1950 61 14-10673 18 301950ND11801420
2-Methylnaphthalene ug/kg 1950 61 10-13568 11 301950ND11801320
2-Methylphenol(o-Cresol)ug/kg 1950 58 10-12468 16 301950ND11201330
2-Nitroaniline ug/kg 3890 78 26-11688 12 303890ND30303420
2-Nitrophenol ug/kg 1950 57 28-10369 20 301950ND11101350
3&4-Methylphenol(m&p
Cresol)ug/kg 1950 62 10-10972 16 301950ND12001410
3,3'-Dichlorobenzidine ug/kg 3890 60 10-15066 9 303890ND23302560
3-Nitroaniline ug/kg 3890 71 22-11078 9 303890ND27603020
4,6-Dinitro-2-methylphenol ug/kg 3890 67 13-12174 10 303890ND25902870
4-Bromophenylphenyl ether ug/kg 1950 55 31-10961 11 301950ND10701190
4-Chloro-3-methylphenol ug/kg 3890 70 13-12879 12 303890ND27203060
4-Chloroaniline ug/kg 3890 63 18-10270 11 303890ND24602740
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 82 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
640692MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299306001
640693
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
4-Chlorophenylphenyl ether ug/kg 1950 60 29-11266 10 301950ND11601290
4-Nitroaniline ug/kg 3890 79 16-11186 7 303890ND30903330
4-Nitrophenol ug/kg 9720 76 14-13581 7 309720ND73907920
Acenaphthene ug/kg 1950 65 26-11471 8 301950ND12701380
Acenaphthylene ug/kg 1950 64 32-10871 10 301950ND12501380
Aniline ug/kg 1950 52 10-10764 20 301950ND10201250
Anthracene ug/kg 1950 71 32-11175 5 301950ND13901470
Benzo(a)anthracene ug/kg 1950 64 25-11770 9 301950ND12501370
Benzo(a)pyrene ug/kg 1950 61 25-10668 11 301950ND11901330
Benzo(b)fluoranthene ug/kg 1950 61 24-11070 14 301950ND11801360
Benzo(g,h,i)perylene ug/kg 1950 55 19-11263 13 301950ND10701220
Benzo(k)fluoranthene ug/kg 1950 61 24-11468 10 301950ND12001320
Benzoic Acid ug/kg M0,M19720910-11010 309720ND894J968J
Benzyl alcohol ug/kg 3890 65 24-10677 17 303890ND25302990
bis(2-Chloroethoxy)methane ug/kg 1950 59 13-11968 14 301950ND11401320
bis(2-Chloroethyl) ether ug/kg 1950 59 10-13469 16 301950ND11401330
bis(2-Chloroisopropyl) ether ug/kg 1950 61 10-11374 19 301950ND11801430
bis(2-Ethylhexyl)phthalate ug/kg 1950 74 10-12584 13 301950ND14301640
Butylbenzylphthalate ug/kg 1950 75 18-11085 12 301950ND14601650
Chrysene ug/kg 1950 65 30-11071 8 301950ND12701380
Di-n-butylphthalate ug/kg 1950 75 19-11281 8 301950ND14501580
Di-n-octylphthalate ug/kg 1950 74 17-10583 12 301950ND14301620
Dibenz(a,h)anthracene ug/kg 1950 55 23-11163 12 301950ND10801220
Dibenzofuran ug/kg 1950 65 35-10371 8 301950ND12701380
Diethylphthalate ug/kg 1950 67 27-11374 11 301950ND13001450
Dimethylphthalate ug/kg 1950 63 26-11169 10 301950ND12201340
Fluoranthene ug/kg 1950 71 33-10974 3 301950ND13901440
Fluorene ug/kg 1950 66 32-11369 5 301950ND12801350
Hexachloro-1,3-butadiene ug/kg 1950 47 16-11657 20 301950ND9081110
Hexachlorobenzene ug/kg 1950 51 27-12056 8 301950ND9961080
Hexachlorocyclopentadiene ug/kg 1950 49 10-10861 21 301950ND9621180
Hexachloroethane ug/kg 1950 57 10-11767 17 301950ND11001310
Indeno(1,2,3-cd)pyrene ug/kg 1950 55 10-12263 13 301950ND10701220
Isophorone ug/kg 1950 67 28-11476 12 301950ND13101470
N-Nitroso-di-n-propylamine ug/kg 1950 62 27-11374 18 301950ND12101450
N-Nitrosodimethylamine ug/kg 1950 58 10-10970 20 301950ND11201370
N-Nitrosodiphenylamine ug/kg 1950 68 10-12874 9 301950ND13201450
Naphthalene ug/kg 1950 57 25-11066 14 301950ND11101290
Nitrobenzene ug/kg 1950 58 18-11468 17 301950ND11201330
Pentachlorophenol ug/kg 3890 65 10-12269 7 303890ND25102690
Phenanthrene ug/kg 1950 68 30-11472 5 301950ND13301390
Phenol ug/kg 1950 61 11-10276 21 301950ND11901470
Pyrene ug/kg 1950 66 25-11672 10 301950ND12801400
2,4,6-Tribromophenol (S)%57 27-11062
2-Fluorobiphenyl (S)%57 30-11066
2-Fluorophenol (S)%59 13-11070
Nitrobenzene-d5 (S)%58 23-11068
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 83 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
640692MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299306001
640693
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol-d6 (S)%63 22-11075
Terphenyl-d14 (S)%62 28-11077
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 84 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/14405
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:9299254020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:642226
Associated Lab Samples:9299254020
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 08/05/11 10:23
1,2-Dichlorobenzene ug/kg ND 330 08/05/11 10:23
1,3-Dichlorobenzene ug/kg ND 330 08/05/11 10:23
1,4-Dichlorobenzene ug/kg ND 330 08/05/11 10:23
1-Methylnaphthalene ug/kg ND 330 08/05/11 10:23
2,4,5-Trichlorophenol ug/kg ND 330 08/05/11 10:23
2,4,6-Trichlorophenol ug/kg ND 330 08/05/11 10:23
2,4-Dichlorophenol ug/kg ND 330 08/05/11 10:23
2,4-Dimethylphenol ug/kg ND 330 08/05/11 10:23
2,4-Dinitrophenol ug/kg ND 1650 08/05/11 10:23
2,4-Dinitrotoluene ug/kg ND 330 08/05/11 10:23
2,6-Dinitrotoluene ug/kg ND 330 08/05/11 10:23
2-Chloronaphthalene ug/kg ND 330 08/05/11 10:23
2-Chlorophenol ug/kg ND 330 08/05/11 10:23
2-Methylnaphthalene ug/kg ND 330 08/05/11 10:23
2-Methylphenol(o-Cresol)ug/kg ND 330 08/05/11 10:23
2-Nitroaniline ug/kg ND 1650 08/05/11 10:23
2-Nitrophenol ug/kg ND 330 08/05/11 10:23
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 08/05/11 10:23
3,3'-Dichlorobenzidine ug/kg ND 1650 08/05/11 10:23
3-Nitroaniline ug/kg ND 1650 08/05/11 10:23
4,6-Dinitro-2-methylphenol ug/kg ND 660 08/05/11 10:23
4-Bromophenylphenyl ether ug/kg ND 330 08/05/11 10:23
4-Chloro-3-methylphenol ug/kg ND 660 08/05/11 10:23
4-Chloroaniline ug/kg ND 1650 08/05/11 10:23
4-Chlorophenylphenyl ether ug/kg ND 330 08/05/11 10:23
4-Nitroaniline ug/kg ND 660 08/05/11 10:23
4-Nitrophenol ug/kg ND 1650 08/05/11 10:23
Acenaphthene ug/kg ND 330 08/05/11 10:23
Acenaphthylene ug/kg ND 330 08/05/11 10:23
Aniline ug/kg ND 330 08/05/11 10:23
Anthracene ug/kg ND 330 08/05/11 10:23
Benzo(a)anthracene ug/kg ND 330 08/05/11 10:23
Benzo(a)pyrene ug/kg ND 330 08/05/11 10:23
Benzo(b)fluoranthene ug/kg ND 330 08/05/11 10:23
Benzo(g,h,i)perylene ug/kg ND 330 08/05/11 10:23
Benzo(k)fluoranthene ug/kg ND 330 08/05/11 10:23
Benzoic Acid ug/kg ND 1650 08/05/11 10:23
Benzyl alcohol ug/kg ND 660 08/05/11 10:23
bis(2-Chloroethoxy)methane ug/kg ND 330 08/05/11 10:23
bis(2-Chloroethyl) ether ug/kg ND 330 08/05/11 10:23
bis(2-Chloroisopropyl) ether ug/kg ND 330 08/05/11 10:23
bis(2-Ethylhexyl)phthalate ug/kg ND 330 08/05/11 10:23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 85 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:642226
Associated Lab Samples:9299254020
Matrix:Solid
Analyzed
Butylbenzylphthalate ug/kg ND 330 08/05/11 10:23
Chrysene ug/kg ND 330 08/05/11 10:23
Di-n-butylphthalate ug/kg ND 330 08/05/11 10:23
Di-n-octylphthalate ug/kg ND 330 08/05/11 10:23
Dibenz(a,h)anthracene ug/kg ND 330 08/05/11 10:23
Dibenzofuran ug/kg ND 330 08/05/11 10:23
Diethylphthalate ug/kg ND 330 08/05/11 10:23
Dimethylphthalate ug/kg ND 330 08/05/11 10:23
Fluoranthene ug/kg ND 330 08/05/11 10:23
Fluorene ug/kg ND 330 08/05/11 10:23
Hexachloro-1,3-butadiene ug/kg ND 330 08/05/11 10:23
Hexachlorobenzene ug/kg ND 330 08/05/11 10:23
Hexachlorocyclopentadiene ug/kg ND 330 08/05/11 10:23
Hexachloroethane ug/kg ND 330 08/05/11 10:23
Indeno(1,2,3-cd)pyrene ug/kg ND 330 08/05/11 10:23
Isophorone ug/kg ND 330 08/05/11 10:23
N-Nitroso-di-n-propylamine ug/kg ND 330 08/05/11 10:23
N-Nitrosodimethylamine ug/kg ND 330 08/05/11 10:23
N-Nitrosodiphenylamine ug/kg ND 330 08/05/11 10:23
Naphthalene ug/kg ND 330 08/05/11 10:23
Nitrobenzene ug/kg ND 330 08/05/11 10:23
Pentachlorophenol ug/kg ND 1650 08/05/11 10:23
Phenanthrene ug/kg ND 330 08/05/11 10:23
Phenol ug/kg ND 330 08/05/11 10:23
Pyrene ug/kg ND 330 08/05/11 10:23
2,4,6-Tribromophenol (S)%51 27-110 08/05/11 10:23
2-Fluorobiphenyl (S)%50 30-110 08/05/11 10:23
2-Fluorophenol (S)%56 13-110 08/05/11 10:23
Nitrobenzene-d5 (S)%55 23-110 08/05/11 10:23
Phenol-d6 (S)%57 22-110 08/05/11 10:23
Terphenyl-d14 (S)%66 28-110 08/05/11 10:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
642227LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 11401670 68 39-101
1,2-Dichlorobenzene ug/kg 12701670 76 36-110
1,3-Dichlorobenzene ug/kg 12701670 76 35-110
1,4-Dichlorobenzene ug/kg 12601670 76 35-110
1-Methylnaphthalene ug/kg 12701670 76 45-105
2,4,5-Trichlorophenol ug/kg 11601670 70 48-109
2,4,6-Trichlorophenol ug/kg 13201670 79 45-111
2,4-Dichlorophenol ug/kg 13301670 80 51-116
2,4-Dimethylphenol ug/kg 13901670 83 42-103
2,4-Dinitrophenol ug/kg 43708330 52 28-103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 86 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
642227LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dinitrotoluene ug/kg 14201670 85 46-114
2,6-Dinitrotoluene ug/kg 14001670 84 48-112
2-Chloronaphthalene ug/kg 12901670 77 44-105
2-Chlorophenol ug/kg 13801670 83 36-110
2-Methylnaphthalene ug/kg 12601670 76 39-112
2-Methylphenol(o-Cresol)ug/kg 13301670 80 39-101
2-Nitroaniline ug/kg 31203330 94 44-111
2-Nitrophenol ug/kg 13001670 78 41-100
3&4-Methylphenol(m&p Cresol)ug/kg 14001670 84 43-103
3,3'-Dichlorobenzidine ug/kg 23703330 71 10-150
3-Nitroaniline ug/kg 25803330 78 35-110
4,6-Dinitro-2-methylphenol ug/kg 18803330 56 38-118
4-Bromophenylphenyl ether ug/kg 10901670 66 47-115
4-Chloro-3-methylphenol ug/kg 29203330 88 43-127
4-Chloroaniline ug/kg 24603330 74 34-109
4-Chlorophenylphenyl ether ug/kg 12201670 73 44-115
4-Nitroaniline ug/kg 28003330 84 37-111
4-Nitrophenol ug/kg 75608330 91 21-152
Acenaphthene ug/kg 13001670 78 38-117
Acenaphthylene ug/kg 13001670 78 46-107
Aniline ug/kg 12201670 73 29-110
Anthracene ug/kg 13801670 83 50-110
Benzo(a)anthracene ug/kg 13201670 79 47-116
Benzo(a)pyrene ug/kg 12701670 76 47-106
Benzo(b)fluoranthene ug/kg 12401670 74 47-109
Benzo(g,h,i)perylene ug/kg 11801670 71 39-115
Benzo(k)fluoranthene ug/kg 12701670 76 45-117
Benzoic Acid ug/kg 59608330 72 16-110
Benzyl alcohol ug/kg 29703330 89 38-105
bis(2-Chloroethoxy)methane ug/kg 12701670 76 39-110
bis(2-Chloroethyl) ether ug/kg 12801670 77 19-119
bis(2-Chloroisopropyl) ether ug/kg 13801670 83 21-110
bis(2-Ethylhexyl)phthalate ug/kg 15601670 94 35-116
Butylbenzylphthalate ug/kg 15201670 91 38-110
Chrysene ug/kg 13401670 80 49-110
Di-n-butylphthalate ug/kg 14801670 89 43-109
Di-n-octylphthalate ug/kg 16101670 97 37-109
Dibenz(a,h)anthracene ug/kg 11801670 71 43-116
Dibenzofuran ug/kg 13101670 78 45-106
Diethylphthalate ug/kg 13601670 82 41-114
Dimethylphthalate ug/kg 12801670 77 43-110
Fluoranthene ug/kg 14201670 85 50-114
Fluorene ug/kg 12801670 77 46-114
Hexachloro-1,3-butadiene ug/kg 10301670 62 28-111
Hexachlorobenzene ug/kg 9931670 60 46-120
Hexachlorocyclopentadiene ug/kg 8951670 54 18-119
Hexachloroethane ug/kg 12201670 73 33-110
Indeno(1,2,3-cd)pyrene ug/kg 11901670 71 42-115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 87 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
642227LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/kg 14301670 86 44-109
N-Nitroso-di-n-propylamine ug/kg 14201670 85 43-104
N-Nitrosodimethylamine ug/kg 12901670 77 29-110
N-Nitrosodiphenylamine ug/kg 13201670 79 48-113
Naphthalene ug/kg 12301670 74 41-110
Nitrobenzene ug/kg 12501670 75 38-110
Pentachlorophenol ug/kg 26903330 81 32-128
Phenanthrene ug/kg 12901670 77 50-110
Phenol ug/kg 14101670 85 28-106
Pyrene ug/kg 12601670 76 45-114
2,4,6-Tribromophenol (S)%66 27-110
2-Fluorobiphenyl (S)%72 30-110
2-Fluorophenol (S)%81 13-110
Nitrobenzene-d5 (S)%75 23-110
Phenol-d6 (S)%88 22-110
Terphenyl-d14 (S)%71 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
642228MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299537001
642229
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1720 61 18-11952 16 301720ND1040888
1,2-Dichlorobenzene ug/kg 1720 60 50-11051 16 301720ND1030881
1,3-Dichlorobenzene ug/kg 1720 59 27-11050 17 301720ND1010853
1,4-Dichlorobenzene ug/kg 1720 60 28-11052 15 301720ND1030889
1-Methylnaphthalene ug/kg 1720 65 24-11650 26 301720ND1120863
2,4,5-Trichlorophenol ug/kg 1720 58 28-11047 22 301720ND999798
2,4,6-Trichlorophenol ug/kg 1720 67 17-11754 21 301720ND1140919
2,4-Dichlorophenol ug/kg 1720 66 21-12851 27 301720ND1130866
2,4-Dimethylphenol ug/kg 1720 60 10-12047 23 301720ND1020809
2,4-Dinitrophenol ug/kg R185605510-10738 36 308560ND46903250
2,4-Dinitrotoluene ug/kg 1720 86 36-10965 29 301720ND14801110
2,6-Dinitrotoluene ug/kg 1720 67 32-11054 21 301720ND1140926
2-Chloronaphthalene ug/kg 1720 69 30-10758 16 301720ND11801000
2-Chlorophenol ug/kg 1720 63 14-10653 16 301720ND1070911
2-Methylnaphthalene ug/kg 1720 66 10-13551 26 301720ND1140874
2-Methylphenol(o-Cresol)ug/kg 1720 58 10-12448 19 301720ND998823
2-Nitroaniline ug/kg 3420 80 26-11664 23 303420ND27402180
2-Nitrophenol ug/kg 1720 62 28-10352 17 301720ND1060895
3&4-Methylphenol(m&p
Cresol)ug/kg 1720 56 10-10945 23 301720ND963764
3,3'-Dichlorobenzidine ug/kg 3420 57 10-15046 303420ND19601570J
3-Nitroaniline ug/kg 3420 75 22-11057 27 303420ND25801960
4,6-Dinitro-2-methylphenol ug/kg R134205713-12141 32 303420ND19501410
4-Bromophenylphenyl ether ug/kg 1720 55 31-10947 15 301720ND940807
4-Chloro-3-methylphenol ug/kg R134207313-12851 35 303420ND25101750
4-Chloroaniline ug/kg 3420 64 18-10249 303420ND21801660J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 88 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
642228MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299537001
642229
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
4-Chlorophenylphenyl ether ug/kg 1720 67 29-11255 19 301720ND1140946
4-Nitroaniline ug/kg R134209916-11171 34 303420ND34002420
4-Nitrophenol ug/kg R1856011114-13578 35 308560ND95006690
Acenaphthene ug/kg 1720 68 26-11456 20 301720ND1170959
Acenaphthylene ug/kg 1720 66 32-10855 20 301720ND1140935
Aniline ug/kg 1720 44 10-10735 22 301720ND752603
Anthracene ug/kg 1720 69 32-11156 22 301720ND1180951
Benzo(a)anthracene ug/kg 1720 65 25-11752 22 301720ND1110897
Benzo(a)pyrene ug/kg 1720 60 25-10649 20 301720ND1020835
Benzo(b)fluoranthene ug/kg 1720 58 24-11048 19 301720ND995820
Benzo(g,h,i)perylene ug/kg 1720 69 19-11257 20 301720ND1190972
Benzo(k)fluoranthene ug/kg 1720 64 24-11450 25 301720ND1090852
Benzoic Acid ug/kg 8560 23 10-11030 26 308560ND19902590
Benzyl alcohol ug/kg 3420 65 24-10653 20 303420ND22101820
bis(2-Chloroethoxy)methane ug/kg 1720 66 13-11956 16 301720ND1140967
bis(2-Chloroethyl) ether ug/kg 1720 69 10-13459 15 301720ND11901020
bis(2-Chloroisopropyl) ether ug/kg 1720 66 10-11356 17 301720ND1130955
bis(2-Ethylhexyl)phthalate ug/kg 1720 66 10-12552 25 301720ND1130885
Butylbenzylphthalate ug/kg 1720 65 18-11053 21 301720ND1110902
Chrysene ug/kg 1720 67 30-11055 19 301720ND1150944
Di-n-butylphthalate ug/kg 1720 75 19-11258 25 301720ND1280995
Di-n-octylphthalate ug/kg 1720 58 17-10544 27 301720ND997757
Dibenz(a,h)anthracene ug/kg 1720 63 23-11150 23 301720ND1070850
Dibenzofuran ug/kg 1720 70 35-10357 20 301720ND1200983
Diethylphthalate ug/kg 1720 79 27-11361 25 301720ND13501050
Dimethylphthalate ug/kg 1720 67 26-11155 20 301720ND1150940
Fluoranthene ug/kg 1720 72 33-10955 26 301720ND1230941
Fluorene ug/kg 1720 72 32-11358 22 301720ND1240986
Hexachloro-1,3-butadiene ug/kg 1720 57 16-11649 16 301720ND981835
Hexachlorobenzene ug/kg 1720 62 27-12051 19 301720ND1050873
Hexachlorocyclopentadiene ug/kg 1720 45 10-10836 22 301720ND769619
Hexachloroethane ug/kg 1720 62 10-11753 16 301720ND1070907
Indeno(1,2,3-cd)pyrene ug/kg 1720 65 10-12252 22 301720ND1110890
Isophorone ug/kg 1720 75 28-11459 23 301720ND12801020
N-Nitroso-di-n-propylamine ug/kg 1720 63 27-11351 21 301720ND1090876
N-Nitrosodimethylamine ug/kg 1720 61 10-10951 18 301720ND1040866
N-Nitrosodiphenylamine ug/kg 1720 58 10-12849 16 301720ND995845
Naphthalene ug/kg 1720 63 25-11053 17 301720ND1080912
Nitrobenzene ug/kg 1720 69 18-11458 17 301720ND1180993
Pentachlorophenol ug/kg 3420 63 10-12248 303420ND21601630J
Phenanthrene ug/kg 1720 68 30-11455 21 301720ND1160943
Phenol ug/kg 1720 67 11-10255 19 301720ND1160950
Pyrene ug/kg 1720 65 25-11654 19 301720ND1110922
2,4,6-Tribromophenol (S)%57 27-11048
2-Fluorobiphenyl (S)%61 30-11055
2-Fluorophenol (S)%54 13-11047
Nitrobenzene-d5 (S)%60 23-11054
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 89 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
642228MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299537001
642229
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol-d6 (S)%59 22-11052
Terphenyl-d14 (S)%58 28-11051
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 90 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/14477
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:9299254001, 9299254002, 9299254003, 9299254004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:645596
Associated Lab Samples:9299254001, 9299254002, 9299254003, 9299254004
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 08/14/11 12:03
1,2-Dichlorobenzene ug/kg ND 330 08/14/11 12:03
1,3-Dichlorobenzene ug/kg ND 330 08/14/11 12:03
1,4-Dichlorobenzene ug/kg ND 330 08/14/11 12:03
1-Methylnaphthalene ug/kg ND 330 08/14/11 12:03
2,4,5-Trichlorophenol ug/kg ND 330 08/14/11 12:03
2,4,6-Trichlorophenol ug/kg ND 330 08/14/11 12:03
2,4-Dichlorophenol ug/kg ND 330 08/14/11 12:03
2,4-Dimethylphenol ug/kg ND 330 08/14/11 12:03
2,4-Dinitrophenol ug/kg ND 1650 08/14/11 12:03
2,4-Dinitrotoluene ug/kg ND 330 08/14/11 12:03
2,6-Dinitrotoluene ug/kg ND 330 08/14/11 12:03
2-Chloronaphthalene ug/kg ND 330 08/14/11 12:03
2-Chlorophenol ug/kg ND 330 08/14/11 12:03
2-Methylnaphthalene ug/kg ND 330 08/14/11 12:03
2-Methylphenol(o-Cresol)ug/kg ND 330 08/14/11 12:03
2-Nitroaniline ug/kg ND 1650 08/14/11 12:03
2-Nitrophenol ug/kg ND 330 08/14/11 12:03
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 08/14/11 12:03
3,3'-Dichlorobenzidine ug/kg ND 1650 08/14/11 12:03
3-Nitroaniline ug/kg ND 1650 08/14/11 12:03
4,6-Dinitro-2-methylphenol ug/kg ND 660 08/14/11 12:03
4-Bromophenylphenyl ether ug/kg ND 330 08/14/11 12:03
4-Chloro-3-methylphenol ug/kg ND 660 08/14/11 12:03
4-Chloroaniline ug/kg ND 1650 08/14/11 12:03
4-Chlorophenylphenyl ether ug/kg ND 330 08/14/11 12:03
4-Nitroaniline ug/kg ND 660 08/14/11 12:03
4-Nitrophenol ug/kg ND 1650 08/14/11 12:03
Acenaphthene ug/kg ND 330 08/14/11 12:03
Acenaphthylene ug/kg ND 330 08/14/11 12:03
Aniline ug/kg ND 330 08/14/11 12:03
Anthracene ug/kg ND 330 08/14/11 12:03
Benzo(a)anthracene ug/kg ND 330 08/14/11 12:03
Benzo(a)pyrene ug/kg ND 330 08/14/11 12:03
Benzo(b)fluoranthene ug/kg ND 330 08/14/11 12:03
Benzo(g,h,i)perylene ug/kg ND 330 08/14/11 12:03
Benzo(k)fluoranthene ug/kg ND 330 08/14/11 12:03
Benzoic Acid ug/kg ND 1650 08/14/11 12:03
Benzyl alcohol ug/kg ND 660 08/14/11 12:03
bis(2-Chloroethoxy)methane ug/kg ND 330 08/14/11 12:03
bis(2-Chloroethyl) ether ug/kg ND 330 08/14/11 12:03
bis(2-Chloroisopropyl) ether ug/kg ND 330 08/14/11 12:03
bis(2-Ethylhexyl)phthalate ug/kg ND 330 08/14/11 12:03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 91 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:645596
Associated Lab Samples:9299254001, 9299254002, 9299254003, 9299254004
Matrix:Solid
Analyzed
Butylbenzylphthalate ug/kg ND 330 08/14/11 12:03
Chrysene ug/kg ND 330 08/14/11 12:03
Di-n-butylphthalate ug/kg ND 330 08/14/11 12:03
Di-n-octylphthalate ug/kg ND 330 08/14/11 12:03
Dibenz(a,h)anthracene ug/kg ND 330 08/14/11 12:03
Dibenzofuran ug/kg ND 330 08/14/11 12:03
Diethylphthalate ug/kg ND 330 08/14/11 12:03
Dimethylphthalate ug/kg ND 330 08/14/11 12:03
Fluoranthene ug/kg ND 330 08/14/11 12:03
Fluorene ug/kg ND 330 08/14/11 12:03
Hexachloro-1,3-butadiene ug/kg ND 330 08/14/11 12:03
Hexachlorobenzene ug/kg ND 330 08/14/11 12:03
Hexachlorocyclopentadiene ug/kg ND 330 08/14/11 12:03
Hexachloroethane ug/kg ND 330 08/14/11 12:03
Indeno(1,2,3-cd)pyrene ug/kg ND 330 08/14/11 12:03
Isophorone ug/kg ND 330 08/14/11 12:03
N-Nitroso-di-n-propylamine ug/kg ND 330 08/14/11 12:03
N-Nitrosodimethylamine ug/kg ND 330 08/14/11 12:03
N-Nitrosodiphenylamine ug/kg ND 330 08/14/11 12:03
Naphthalene ug/kg ND 330 08/14/11 12:03
Nitrobenzene ug/kg ND 330 08/14/11 12:03
Pentachlorophenol ug/kg ND 1650 08/14/11 12:03
Phenanthrene ug/kg ND 330 08/14/11 12:03
Phenol ug/kg ND 330 08/14/11 12:03
Pyrene ug/kg ND 330 08/14/11 12:03
2,4,6-Tribromophenol (S)%66 27-110 08/14/11 12:03
2-Fluorobiphenyl (S)%66 30-110 08/14/11 12:03
2-Fluorophenol (S)%71 13-110 08/14/11 12:03
Nitrobenzene-d5 (S)%69 23-110 08/14/11 12:03
Phenol-d6 (S)%76 22-110 08/14/11 12:03
Terphenyl-d14 (S)%77 28-110 08/14/11 12:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
645597LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 11001670 66 39-101
1,2-Dichlorobenzene ug/kg 12801670 77 36-110
1,3-Dichlorobenzene ug/kg 12601670 75 35-110
1,4-Dichlorobenzene ug/kg 12701670 76 35-110
1-Methylnaphthalene ug/kg 13801670 83 45-105
2,4,5-Trichlorophenol ug/kg 11401670 68 48-109
2,4,6-Trichlorophenol ug/kg 13101670 78 45-111
2,4-Dichlorophenol ug/kg 13101670 79 51-116
2,4-Dimethylphenol ug/kg 13601670 82 42-103
2,4-Dinitrophenol ug/kg 69008330 83 28-103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 92 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
645597LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dinitrotoluene ug/kg 13501670 81 46-114
2,6-Dinitrotoluene ug/kg 13801670 83 48-112
2-Chloronaphthalene ug/kg 12901670 77 44-105
2-Chlorophenol ug/kg 13301670 80 36-110
2-Methylnaphthalene ug/kg 13701670 82 39-112
2-Methylphenol(o-Cresol)ug/kg 14201670 85 39-101
2-Nitroaniline ug/kg 30903330 93 44-111
2-Nitrophenol ug/kg 12301670 74 41-100
3&4-Methylphenol(m&p Cresol)ug/kg 15401670 92 43-103
3,3'-Dichlorobenzidine ug/kg 23303330 70 10-150
3-Nitroaniline ug/kg 27703330 83 35-110
4,6-Dinitro-2-methylphenol ug/kg 30303330 91 38-118
4-Bromophenylphenyl ether ug/kg 12401670 74 47-115
4-Chloro-3-methylphenol ug/kg 32203330 97 43-127
4-Chloroaniline ug/kg 28503330 86 34-109
4-Chlorophenylphenyl ether ug/kg 12601670 76 44-115
4-Nitroaniline ug/kg 28803330 86 37-111
4-Nitrophenol ug/kg 71108330 85 21-152
Acenaphthene ug/kg 13401670 80 38-117
Acenaphthylene ug/kg 13101670 79 46-107
Aniline ug/kg 13101670 79 29-110
Anthracene ug/kg 14301670 86 50-110
Benzo(a)anthracene ug/kg 13501670 81 47-116
Benzo(a)pyrene ug/kg 13101670 79 47-106
Benzo(b)fluoranthene ug/kg 13101670 78 47-109
Benzo(g,h,i)perylene ug/kg 12901670 78 39-115
Benzo(k)fluoranthene ug/kg 13201670 79 45-117
Benzoic Acid ug/kg 69908330 84 16-110
Benzyl alcohol ug/kg 32703330 98 38-105
bis(2-Chloroethoxy)methane ug/kg 12801670 77 39-110
bis(2-Chloroethyl) ether ug/kg 12501670 75 19-119
bis(2-Chloroisopropyl) ether ug/kg 13901670 83 21-110
bis(2-Ethylhexyl)phthalate ug/kg 15801670 95 35-116
Butylbenzylphthalate ug/kg 15801670 95 38-110
Chrysene ug/kg 13601670 82 49-110
Di-n-butylphthalate ug/kg 15001670 90 43-109
Di-n-octylphthalate ug/kg 15201670 91 37-109
Dibenz(a,h)anthracene ug/kg 12601670 76 43-116
Dibenzofuran ug/kg 13401670 80 45-106
Diethylphthalate ug/kg 13501670 81 41-114
Dimethylphthalate ug/kg 13101670 78 43-110
Fluoranthene ug/kg 13501670 81 50-114
Fluorene ug/kg 12901670 78 46-114
Hexachloro-1,3-butadiene ug/kg 10201670 61 28-111
Hexachlorobenzene ug/kg 11201670 67 46-120
Hexachlorocyclopentadiene ug/kg 11101670 67 18-119
Hexachloroethane ug/kg 12601670 76 33-110
Indeno(1,2,3-cd)pyrene ug/kg 12801670 77 42-115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 93 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
645597LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/kg 15501670 93 44-109
N-Nitroso-di-n-propylamine ug/kg 16701670 100 43-104
N-Nitrosodimethylamine ug/kg 11701670 70 29-110
N-Nitrosodiphenylamine ug/kg 14301670 86 48-113
Naphthalene ug/kg 12101670 73 41-110
Nitrobenzene ug/kg 11601670 70 38-110
Pentachlorophenol ug/kg 27103330 81 32-128
Phenanthrene ug/kg 13701670 82 50-110
Phenol ug/kg 14401670 86 28-106
Pyrene ug/kg 14001670 84 45-114
2,4,6-Tribromophenol (S)%72 27-110
2-Fluorobiphenyl (S)%74 30-110
2-Fluorophenol (S)%75 13-110
Nitrobenzene-d5 (S)%69 23-110
Phenol-d6 (S)%85 22-110
Terphenyl-d14 (S)%79 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
645598MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299783001
645599
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 2090 65 18-11966 2 302090ND13601380
1,2-Dichlorobenzene ug/kg 2090 71 50-11071 1 302090ND14801470
1,3-Dichlorobenzene ug/kg 2090 73 27-11069 6 302090ND15201430
1,4-Dichlorobenzene ug/kg 2090 71 28-11069 3 302090ND14901440
1-Methylnaphthalene ug/kg 2090 66 24-11673 10 302090ND13701510
2,4,5-Trichlorophenol ug/kg 2090 63 28-11066 5 302090ND13101370
2,4,6-Trichlorophenol ug/kg 2090 72 17-11777 7 302090ND14901600
2,4-Dichlorophenol ug/kg 2090 74 21-12877 5 302090ND15301610
2,4-Dimethylphenol ug/kg 2090 76 10-12081 7 302090ND15701690
2,4-Dinitrophenol ug/kg 10400 49 10-10761 22 3010400ND50906350
2,4-Dinitrotoluene ug/kg 2090 76 36-10982 7 302090ND15901710
2,6-Dinitrotoluene ug/kg 2090 73 32-11082 11 302090ND15201700
2-Chloronaphthalene ug/kg 2090 68 30-10772 5 302090ND14201490
2-Chlorophenol ug/kg 2090 76 14-10676 1 302090ND15801570
2-Methylnaphthalene ug/kg 2090 67 10-13573 9 302090ND13901530
2-Methylphenol(o-Cresol)ug/kg 2090 70 10-12473 4 302090ND14701520
2-Nitroaniline ug/kg 4160 85 26-11688 4 304160ND35403680
2-Nitrophenol ug/kg 2090 73 28-10376 4 302090ND15201570
3&4-Methylphenol(m&p
Cresol)ug/kg 2090 73 10-10975 4 302090ND15101570
3,3'-Dichlorobenzidine ug/kg 4160 55 10-15075 30 304160ND22903110
3-Nitroaniline ug/kg 4160 83 22-11084 2 304160ND34503510
4,6-Dinitro-2-methylphenol ug/kg 4160 56 13-12171 24 304160ND23202940
4-Bromophenylphenyl ether ug/kg 2090 62 31-10970 13 302090ND12801450
4-Chloro-3-methylphenol ug/kg 4160 78 13-12888 12 304160ND32703670
4-Chloroaniline ug/kg 4160 69 18-10272 4 304160ND28802990
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 94 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
645598MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299783001
645599
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
4-Chlorophenylphenyl ether ug/kg 2090 68 29-11274 9 302090ND14101540
4-Nitroaniline ug/kg 4160 89 16-11187 2 304160ND37103620
4-Nitrophenol ug/kg 10400 89 14-13586 4 3010400ND93008960
Acenaphthene ug/kg 2090 70 26-11478 11 302090ND14601630
Acenaphthylene ug/kg 2090 68 32-10876 11 302090ND14201580
Aniline ug/kg 2090 47 10-10754 14 302090ND9721120
Anthracene ug/kg 2090 74 32-11182 11 302090ND15301710
Benzo(a)anthracene ug/kg 2090 68 25-11777 13 302090ND14101610
Benzo(a)pyrene ug/kg 2090 64 25-10673 13 302090ND13401520
Benzo(b)fluoranthene ug/kg 2090 62 24-11073 16 302090ND12901520
Benzo(g,h,i)perylene ug/kg 2090 68 19-11272 6 302090ND14101500
Benzo(k)fluoranthene ug/kg 2090 59 24-11470 17 302090ND12301460
Benzoic Acid ug/kg 10400 37 10-11045 22 3010400ND38004720
Benzyl alcohol ug/kg 4160 77 24-10681 6 304160ND32003390
bis(2-Chloroethoxy)methane ug/kg 2090 67 13-11972 6 302090ND14001490
bis(2-Chloroethyl) ether ug/kg 2090 69 10-13467 2 302090ND14301400
bis(2-Chloroisopropyl) ether ug/kg 2090 68 10-11370 3 302090ND14201460
bis(2-Ethylhexyl)phthalate ug/kg 2090 75 10-12587 14 302090ND16001840
Butylbenzylphthalate ug/kg 2090 75 18-11087 15 302090ND15701820
Chrysene ug/kg 2090 68 30-11078 13 302090ND14201630
Di-n-butylphthalate ug/kg 2090 77 19-11288 13 302090ND16001820
Di-n-octylphthalate ug/kg 2090 82 17-10598 17 302090ND17202040
Dibenz(a,h)anthracene ug/kg 2090 67 23-11171 7 302090ND13901490
Dibenzofuran ug/kg 2090 71 35-10378 8 302090ND14801620
Diethylphthalate ug/kg 2090 73 27-11381 10 302090ND15201680
Dimethylphthalate ug/kg 2090 71 26-11176 7 302090ND14801590
Fluoranthene ug/kg 2090 69 33-10979 13 302090ND14401650
Fluorene ug/kg 2090 71 32-11377 9 302090ND14701600
Hexachloro-1,3-butadiene ug/kg 2090 61 16-11662 1 302090ND12701290
Hexachlorobenzene ug/kg 2090 57 27-12064 12 302090ND11801330
Hexachlorocyclopentadiene ug/kg 2090 30 10-10837 20 302090ND632773
Hexachloroethane ug/kg 2090 72 10-11768 5 302090ND15001430
Indeno(1,2,3-cd)pyrene ug/kg 2090 68 10-12273 7 302090ND14101510
Isophorone ug/kg 2090 76 28-11480 5 302090ND15701660
N-Nitroso-di-n-propylamine ug/kg 2090 67 27-11374 9 302090ND14001540
N-Nitrosodimethylamine ug/kg 2090 66 10-10955 17 302090ND13601150
N-Nitrosodiphenylamine ug/kg R120905810-12880 33 302090ND12001670
Naphthalene ug/kg 2090 67 25-11070 4 302090ND14001460
Nitrobenzene ug/kg 2090 69 18-11470 2 302090ND14401460
Pentachlorophenol ug/kg 4160 71 10-12285 17 304160ND29603520
Phenanthrene ug/kg 2090 70 30-11478 11 302090ND14601630
Phenol ug/kg 2090 71 11-10275 5 302090ND14801560
Pyrene ug/kg 2090 65 25-11677 17 302090ND13401600
2,4,6-Tribromophenol (S)%64 27-11071
2-Fluorobiphenyl (S)%61 30-11067
2-Fluorophenol (S)%73 13-11065
Nitrobenzene-d5 (S)%69 23-11069
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 95 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
645598MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299783001
645599
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol-d6 (S)%72 22-11075
Terphenyl-d14 (S)%60 28-11072
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 96 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/14483
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:9299254013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:645774
Associated Lab Samples:9299254013
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 08/14/11 19:17
1,2-Dichlorobenzene ug/kg ND 330 08/14/11 19:17
1,3-Dichlorobenzene ug/kg ND 330 08/14/11 19:17
1,4-Dichlorobenzene ug/kg ND 330 08/14/11 19:17
1-Methylnaphthalene ug/kg ND 330 08/14/11 19:17
2,4,5-Trichlorophenol ug/kg ND 330 08/14/11 19:17
2,4,6-Trichlorophenol ug/kg ND 330 08/14/11 19:17
2,4-Dichlorophenol ug/kg ND 330 08/14/11 19:17
2,4-Dimethylphenol ug/kg ND 330 08/14/11 19:17
2,4-Dinitrophenol ug/kg ND 1650 08/14/11 19:17
2,4-Dinitrotoluene ug/kg ND 330 08/14/11 19:17
2,6-Dinitrotoluene ug/kg ND 330 08/14/11 19:17
2-Chloronaphthalene ug/kg ND 330 08/14/11 19:17
2-Chlorophenol ug/kg ND 330 08/14/11 19:17
2-Methylnaphthalene ug/kg ND 330 08/14/11 19:17
2-Methylphenol(o-Cresol)ug/kg ND 330 08/14/11 19:17
2-Nitroaniline ug/kg ND 1650 08/14/11 19:17
2-Nitrophenol ug/kg ND 330 08/14/11 19:17
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 08/14/11 19:17
3,3'-Dichlorobenzidine ug/kg ND 1650 08/14/11 19:17
3-Nitroaniline ug/kg ND 1650 08/14/11 19:17
4,6-Dinitro-2-methylphenol ug/kg ND 660 08/14/11 19:17
4-Bromophenylphenyl ether ug/kg ND 330 08/14/11 19:17
4-Chloro-3-methylphenol ug/kg ND 660 08/14/11 19:17
4-Chloroaniline ug/kg ND 1650 08/14/11 19:17
4-Chlorophenylphenyl ether ug/kg ND 330 08/14/11 19:17
4-Nitroaniline ug/kg ND 660 08/14/11 19:17
4-Nitrophenol ug/kg ND 1650 08/14/11 19:17
Acenaphthene ug/kg ND 330 08/14/11 19:17
Acenaphthylene ug/kg ND 330 08/14/11 19:17
Aniline ug/kg ND 330 08/14/11 19:17
Anthracene ug/kg ND 330 08/14/11 19:17
Benzo(a)anthracene ug/kg ND 330 08/14/11 19:17
Benzo(a)pyrene ug/kg ND 330 08/14/11 19:17
Benzo(b)fluoranthene ug/kg ND 330 08/14/11 19:17
Benzo(g,h,i)perylene ug/kg ND 330 08/14/11 19:17
Benzo(k)fluoranthene ug/kg ND 330 08/14/11 19:17
Benzoic Acid ug/kg ND 1650 08/14/11 19:17
Benzyl alcohol ug/kg ND 660 08/14/11 19:17
bis(2-Chloroethoxy)methane ug/kg ND 330 08/14/11 19:17
bis(2-Chloroethyl) ether ug/kg ND 330 08/14/11 19:17
bis(2-Chloroisopropyl) ether ug/kg ND 330 08/14/11 19:17
bis(2-Ethylhexyl)phthalate ug/kg ND 330 08/14/11 19:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 97 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:645774
Associated Lab Samples:9299254013
Matrix:Solid
Analyzed
Butylbenzylphthalate ug/kg ND 330 08/14/11 19:17
Chrysene ug/kg ND 330 08/14/11 19:17
Di-n-butylphthalate ug/kg ND 330 08/14/11 19:17
Di-n-octylphthalate ug/kg ND 330 08/14/11 19:17
Dibenz(a,h)anthracene ug/kg ND 330 08/14/11 19:17
Dibenzofuran ug/kg ND 330 08/14/11 19:17
Diethylphthalate ug/kg ND 330 08/14/11 19:17
Dimethylphthalate ug/kg ND 330 08/14/11 19:17
Fluoranthene ug/kg ND 330 08/14/11 19:17
Fluorene ug/kg ND 330 08/14/11 19:17
Hexachloro-1,3-butadiene ug/kg ND 330 08/14/11 19:17
Hexachlorobenzene ug/kg ND 330 08/14/11 19:17
Hexachlorocyclopentadiene ug/kg ND 330 08/14/11 19:17
Hexachloroethane ug/kg ND 330 08/14/11 19:17
Indeno(1,2,3-cd)pyrene ug/kg ND 330 08/14/11 19:17
Isophorone ug/kg ND 330 08/14/11 19:17
N-Nitroso-di-n-propylamine ug/kg ND 330 08/14/11 19:17
N-Nitrosodimethylamine ug/kg ND 330 08/14/11 19:17
N-Nitrosodiphenylamine ug/kg ND 330 08/14/11 19:17
Naphthalene ug/kg ND 330 08/14/11 19:17
Nitrobenzene ug/kg ND 330 08/14/11 19:17
Pentachlorophenol ug/kg ND 1650 08/14/11 19:17
Phenanthrene ug/kg ND 330 08/14/11 19:17
Phenol ug/kg ND 330 08/14/11 19:17
Pyrene ug/kg ND 330 08/14/11 19:17
2,4,6-Tribromophenol (S)%62 27-110 08/14/11 19:17
2-Fluorobiphenyl (S)%54 30-110 08/14/11 19:17
2-Fluorophenol (S)%64 13-110 08/14/11 19:17
Nitrobenzene-d5 (S)%60 23-110 08/14/11 19:17
Phenol-d6 (S)%51 22-110 08/14/11 19:17
Terphenyl-d14 (S)%63 28-110 08/14/11 19:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
645775LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 11801670 71 39-101
1,2-Dichlorobenzene ug/kg 11901670 72 36-110
1,3-Dichlorobenzene ug/kg 12201670 73 35-110
1,4-Dichlorobenzene ug/kg 12301670 74 35-110
1-Methylnaphthalene ug/kg 11701670 70 45-105
2,4,5-Trichlorophenol ug/kg 12001670 72 48-109
2,4,6-Trichlorophenol ug/kg 13101670 79 45-111
2,4-Dichlorophenol ug/kg 12301670 74 51-116
2,4-Dimethylphenol ug/kg 12101670 73 42-103
2,4-Dinitrophenol ug/kg 41608330 50 28-103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 98 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
645775LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dinitrotoluene ug/kg 13901670 83 46-114
2,6-Dinitrotoluene ug/kg 13601670 82 48-112
2-Chloronaphthalene ug/kg 12101670 73 44-105
2-Chlorophenol ug/kg 12301670 74 36-110
2-Methylnaphthalene ug/kg 11801670 71 39-112
2-Methylphenol(o-Cresol)ug/kg 9781670 59 39-101
2-Nitroaniline ug/kg 30303330 91 44-111
2-Nitrophenol ug/kg 12301670 74 41-100
3&4-Methylphenol(m&p Cresol)ug/kg 9841670 59 43-103
3,3'-Dichlorobenzidine ug/kg 26203330 79 10-150
3-Nitroaniline ug/kg 26903330 81 35-110
4,6-Dinitro-2-methylphenol ug/kg 18803330 56 38-118
4-Bromophenylphenyl ether ug/kg 11901670 72 47-115
4-Chloro-3-methylphenol ug/kg 27203330 82 43-127
4-Chloroaniline ug/kg 22603330 68 34-109
4-Chlorophenylphenyl ether ug/kg 12701670 76 44-115
4-Nitroaniline ug/kg 31003330 93 37-111
4-Nitrophenol ug/kg 87508330 105 21-152
Acenaphthene ug/kg 12401670 75 38-117
Acenaphthylene ug/kg 12201670 73 46-107
Aniline ug/kg 9341670 56 29-110
Anthracene ug/kg 12701670 76 50-110
Benzo(a)anthracene ug/kg 12401670 74 47-116
Benzo(a)pyrene ug/kg 12101670 72 47-106
Benzo(b)fluoranthene ug/kg 11301670 68 47-109
Benzo(g,h,i)perylene ug/kg 12501670 75 39-115
Benzo(k)fluoranthene ug/kg 11501670 69 45-117
Benzoic Acid ug/kg 52508330 63 16-110
Benzyl alcohol ug/kg 21203330 64 38-105
bis(2-Chloroethoxy)methane ug/kg 10901670 65 39-110
bis(2-Chloroethyl) ether ug/kg 11601670 69 19-119
bis(2-Chloroisopropyl) ether ug/kg 10201670 61 21-110
bis(2-Ethylhexyl)phthalate ug/kg 10501670 63 35-116
Butylbenzylphthalate ug/kg 10601670 64 38-110
Chrysene ug/kg 12101670 73 49-110
Di-n-butylphthalate ug/kg 11501670 69 43-109
Di-n-octylphthalate ug/kg 10601670 64 37-109
Dibenz(a,h)anthracene ug/kg 12401670 74 43-116
Dibenzofuran ug/kg 13101670 79 45-106
Diethylphthalate ug/kg 12101670 72 41-114
Dimethylphthalate ug/kg 11901670 71 43-110
Fluoranthene ug/kg 13601670 82 50-114
Fluorene ug/kg 12701670 76 46-114
Hexachloro-1,3-butadiene ug/kg 11501670 69 28-111
Hexachlorobenzene ug/kg 11701670 70 46-120
Hexachlorocyclopentadiene ug/kg 6681670 40 18-119
Hexachloroethane ug/kg 11101670 67 33-110
Indeno(1,2,3-cd)pyrene ug/kg 12701670 76 42-115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 99 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
645775LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/kg 12001670 72 44-109
N-Nitroso-di-n-propylamine ug/kg 9541670 57 43-104
N-Nitrosodimethylamine ug/kg 12601670 75 29-110
N-Nitrosodiphenylamine ug/kg 12201670 73 48-113
Naphthalene ug/kg 12001670 72 41-110
Nitrobenzene ug/kg 12301670 74 38-110
Pentachlorophenol ug/kg 35703330 107 32-128
Phenanthrene ug/kg 11801670 71 50-110
Phenol ug/kg 11301670 68 28-106
Pyrene ug/kg 10701670 64 45-114
2,4,6-Tribromophenol (S)%88 27-110
2-Fluorobiphenyl (S)%66 30-110
2-Fluorophenol (S)%80 13-110
Nitrobenzene-d5 (S)%74 23-110
Phenol-d6 (S)%68 22-110
Terphenyl-d14 (S)%63 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
645776MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299900002
645777
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 2320 62 18-11958 6 302320ND14401350
1,2-Dichlorobenzene ug/kg 2320 65 50-11057 12 302320ND15001330
1,3-Dichlorobenzene ug/kg 2320 66 27-11060 9 302320ND15301390
1,4-Dichlorobenzene ug/kg 2320 66 28-11061 9 302320ND15401400
1-Methylnaphthalene ug/kg 2320 60 24-11653 12 302320ND13801230
2,4,5-Trichlorophenol ug/kg 2320 60 28-11059 0 302320ND13801380
2,4,6-Trichlorophenol ug/kg 2320 62 17-11764 3 302320ND14201470
2,4-Dichlorophenol ug/kg 2320 64 21-12859 9 302320ND14801360
2,4-Dimethylphenol ug/kg 2320 61 10-12055 10 302320ND14101280
2,4-Dinitrophenol ug/kg 11600 60 10-10754 11 3011600ND69706220
2,4-Dinitrotoluene ug/kg 2320 69 36-10977 11 302320ND15901770
2,6-Dinitrotoluene ug/kg 2320 67 32-11071 5 302320ND15501630
2-Chloronaphthalene ug/kg 2320 56 30-10759 6 302320ND12801360
2-Chlorophenol ug/kg 2320 65 14-10657 14 302320ND15001310
2-Methylnaphthalene ug/kg 2320 60 10-13554 11 302320ND13901240
2-Methylphenol(o-Cresol)ug/kg 2320 52 10-12443 19 302320ND1190988
2-Nitroaniline ug/kg 4620 71 26-11671 1 304620ND32703300
2-Nitrophenol ug/kg 2320 63 28-10360 6 302320ND14601380
3&4-Methylphenol(m&p
Cresol)ug/kg 2320 54 10-10943 22 302320ND1250999
3,3'-Dichlorobenzidine ug/kg 4620 29 10-15043 304620ND1360J1990J
3-Nitroaniline ug/kg 4620 65 22-11071 8 304620ND30103280
4,6-Dinitro-2-methylphenol ug/kg 4620 56 13-12153 6 304620ND26102450
4-Bromophenylphenyl ether ug/kg 2320 56 31-10959 4 302320ND13001360
4-Chloro-3-methylphenol ug/kg 4620 72 13-12859 19 304620ND33202740
4-Chloroaniline ug/kg 4620 62 18-10251 20 304620ND28702340
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 100 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
645776MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299900002
645777
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
4-Chlorophenylphenyl ether ug/kg 2320 64 29-11267 4 302320ND14801540
4-Nitroaniline ug/kg 4620 69 16-11178 12 304620ND32103620
4-Nitrophenol ug/kg 11600 78 14-13580 2 3011600ND90009220
Acenaphthene ug/kg 2320 58 26-11461 5 302320ND13401410
Acenaphthylene ug/kg 2320 56 32-10858 4 302320ND13001350
Aniline ug/kg R123202810-10720 35 302320ND656463
Anthracene ug/kg 2320 56 32-11160 7 302320ND13001390
Benzo(a)anthracene ug/kg 2320 54 25-11759 10 302320ND12401360
Benzo(a)pyrene ug/kg 2320 48 25-10654 11 302320ND11601300
Benzo(b)fluoranthene ug/kg 2320 47 24-11055 16 302320ND10901270
Benzo(g,h,i)perylene ug/kg 2320 54 19-11263 16 302320ND12401450
Benzo(k)fluoranthene ug/kg 2320 47 24-11451 8 302320ND10901180
Benzoic Acid ug/kg 11600 33 10-11020 3011600ND38502260J
Benzyl alcohol ug/kg 4620 57 24-10646 20 304620ND26302150
bis(2-Chloroethoxy)methane ug/kg 2320 51 13-11948 7 302320ND11801100
bis(2-Chloroethyl) ether ug/kg 2320 63 10-13452 19 302320ND14501200
bis(2-Chloroisopropyl) ether ug/kg 2320 55 10-11348 13 302320ND12801120
bis(2-Ethylhexyl)phthalate ug/kg 2320 56 10-12561 8 302320ND13001410
Butylbenzylphthalate ug/kg 2320 52 18-11059 13 302320ND12001370
Chrysene ug/kg 2320 53 30-11059 12 302320ND12201370
Di-n-butylphthalate ug/kg 2320 55 19-11261 11 302320ND12701410
Di-n-octylphthalate ug/kg 2320 59 17-10565 10 302320ND13601510
Dibenz(a,h)anthracene ug/kg 2320 56 23-11164 13 302320ND12901470
Dibenzofuran ug/kg 2320 61 35-10365 5 302320ND14201500
Diethylphthalate ug/kg 2320 62 27-11370 12 302320ND14401630
Dimethylphthalate ug/kg 2320 60 26-11164 6 302320ND13901470
Fluoranthene ug/kg 2320 57 33-10962 9 302320ND13201440
Fluorene ug/kg 2320 63 32-11367 6 302320ND14501540
Hexachloro-1,3-butadiene ug/kg 2320 62 16-11658 6 302320ND14201350
Hexachlorobenzene ug/kg 2320 56 27-12059 5 302320ND13001380
Hexachlorocyclopentadiene ug/kg 2320 29 10-10828 6 302320ND677639
Hexachloroethane ug/kg 2320 61 10-11754 12 302320ND14201260
Indeno(1,2,3-cd)pyrene ug/kg 2320 55 10-12263 14 302320ND12701460
Isophorone ug/kg 2320 64 28-11460 6 302320ND14701380
N-Nitroso-di-n-propylamine ug/kg 2320 54 27-11342 24 302320ND1250983
N-Nitrosodimethylamine ug/kg 2320 58 10-10953 8 302320ND13301230
N-Nitrosodiphenylamine ug/kg 2320 40 10-12837 6 302320ND920865
Naphthalene ug/kg 2320 58 25-11055 5 302320ND13401270
Nitrobenzene ug/kg 2320 59 18-11455 7 302320ND13701280
Pentachlorophenol ug/kg 4620 77 10-12276 1 304620ND35503530
Phenanthrene ug/kg 2320 53 30-11457 7 302320ND12301320
Phenol ug/kg 2320 52 11-10245 15 302320ND12001030
Pyrene ug/kg 2320 51 25-11656 9 302320ND11901300
2,4,6-Tribromophenol (S)%70 27-11070
2-Fluorobiphenyl (S)%49 30-11054
2-Fluorophenol (S)%70 13-11062
Nitrobenzene-d5 (S)%59 23-11056
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 101 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
645776MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299900002
645777
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol-d6 (S)%54 22-11046
Terphenyl-d14 (S)%49 28-11051
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 102 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/16149
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:9299254014, 9299254017, 9299254018, 9299254019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:640268
Associated Lab Samples:9299254014, 9299254017, 9299254018, 9299254019
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/29/11 13:02
1,1,1-Trichloroethane ug/kg ND 5.0 07/29/11 13:02
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/29/11 13:02
1,1,2-Trichloroethane ug/kg ND 5.0 07/29/11 13:02
1,1-Dichloroethane ug/kg ND 5.0 07/29/11 13:02
1,1-Dichloroethene ug/kg ND 5.0 07/29/11 13:02
1,1-Dichloropropene ug/kg ND 5.0 07/29/11 13:02
1,2,3-Trichlorobenzene ug/kg ND 5.0 07/29/11 13:02
1,2,3-Trichloropropane ug/kg ND 5.0 07/29/11 13:02
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/29/11 13:02
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/29/11 13:02
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 07/29/11 13:02
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/29/11 13:02
1,2-Dichlorobenzene ug/kg ND 5.0 07/29/11 13:02
1,2-Dichloroethane ug/kg ND 5.0 07/29/11 13:02
1,2-Dichloropropane ug/kg ND 5.0 07/29/11 13:02
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/29/11 13:02
1,3-Dichlorobenzene ug/kg ND 5.0 07/29/11 13:02
1,3-Dichloropropane ug/kg ND 5.0 07/29/11 13:02
1,4-Dichlorobenzene ug/kg ND 5.0 07/29/11 13:02
2,2-Dichloropropane ug/kg ND 5.0 07/29/11 13:02
2-Butanone (MEK)ug/kg ND 100 07/29/11 13:02
2-Chlorotoluene ug/kg ND 5.0 07/29/11 13:02
2-Hexanone ug/kg ND 50.0 07/29/11 13:02
4-Chlorotoluene ug/kg ND 5.0 07/29/11 13:02
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/29/11 13:02
Acetone ug/kg ND 100 07/29/11 13:02
Benzene ug/kg ND 5.0 07/29/11 13:02
Bromobenzene ug/kg ND 5.0 07/29/11 13:02
Bromochloromethane ug/kg ND 5.0 07/29/11 13:02
Bromodichloromethane ug/kg ND 5.0 07/29/11 13:02
Bromoform ug/kg ND 5.0 07/29/11 13:02
Bromomethane ug/kg ND 10.0 07/29/11 13:02
Carbon tetrachloride ug/kg ND 5.0 07/29/11 13:02
Chlorobenzene ug/kg ND 5.0 07/29/11 13:02
Chloroethane ug/kg ND 10.0 07/29/11 13:02
Chloroform ug/kg ND 5.0 07/29/11 13:02
Chloromethane ug/kg ND 10.0 07/29/11 13:02
cis-1,2-Dichloroethene ug/kg ND 5.0 07/29/11 13:02
cis-1,3-Dichloropropene ug/kg ND 5.0 07/29/11 13:02
Dibromochloromethane ug/kg ND 5.0 07/29/11 13:02
Dibromomethane ug/kg ND 5.0 07/29/11 13:02
Dichlorodifluoromethane ug/kg ND 10.0 07/29/11 13:02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 103 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:640268
Associated Lab Samples:9299254014, 9299254017, 9299254018, 9299254019
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.0 07/29/11 13:02
Ethylbenzene ug/kg ND 5.0 07/29/11 13:02
Hexachloro-1,3-butadiene ug/kg ND 5.0 07/29/11 13:02
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/29/11 13:02
m&p-Xylene ug/kg ND 10.0 07/29/11 13:02
Methyl-tert-butyl ether ug/kg ND 5.0 07/29/11 13:02
Methylene Chloride ug/kg ND 20.0 07/29/11 13:02
n-Butylbenzene ug/kg ND 5.0 07/29/11 13:02
n-Propylbenzene ug/kg ND 5.0 07/29/11 13:02
Naphthalene ug/kg ND 5.0 07/29/11 13:02
o-Xylene ug/kg ND 5.0 07/29/11 13:02
p-Isopropyltoluene ug/kg ND 5.0 07/29/11 13:02
sec-Butylbenzene ug/kg ND 5.0 07/29/11 13:02
Styrene ug/kg ND 5.0 07/29/11 13:02
tert-Butylbenzene ug/kg ND 5.0 07/29/11 13:02
Tetrachloroethene ug/kg ND 5.0 07/29/11 13:02
Toluene ug/kg ND 5.0 07/29/11 13:02
trans-1,2-Dichloroethene ug/kg ND 5.0 07/29/11 13:02
trans-1,3-Dichloropropene ug/kg ND 5.0 07/29/11 13:02
Trichloroethene ug/kg ND 5.0 07/29/11 13:02
Trichlorofluoromethane ug/kg ND 5.0 07/29/11 13:02
Vinyl acetate ug/kg ND 50.0 07/29/11 13:02
Vinyl chloride ug/kg ND 10.0 07/29/11 13:02
Xylene (Total)ug/kg ND 10.0 07/29/11 13:02
1,2-Dichloroethane-d4 (S)%91 70-132 07/29/11 13:02
4-Bromofluorobenzene (S)%94 70-130 07/29/11 13:02
Dibromofluoromethane (S)%93 70-130 07/29/11 13:02
Toluene-d8 (S)%104 70-130 07/29/11 13:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640269LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 46.550 93 70-131
1,1,1-Trichloroethane ug/kg 42.950 86 70-141
1,1,2,2-Tetrachloroethane ug/kg 43.250 86 70-130
1,1,2-Trichloroethane ug/kg 43.150 86 70-132
1,1-Dichloroethane ug/kg 42.650 85 70-143
1,1-Dichloroethene ug/kg 41.250 82 70-137
1,1-Dichloropropene ug/kg 40.650 81 70-135
1,2,3-Trichlorobenzene ug/kg 42.450 85 69-153
1,2,3-Trichloropropane ug/kg 41.450 83 70-130
1,2,4-Trichlorobenzene ug/kg 45.550 91 55-171
1,2,4-Trimethylbenzene ug/kg 46.250 92 70-149
1,2-Dibromo-3-chloropropane ug/kg 42.050 84 68-141
1,2-Dibromoethane (EDB)ug/kg 42.950 86 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 104 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640269LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 44.750 89 70-140
1,2-Dichloroethane ug/kg 40.650 81 70-137
1,2-Dichloropropane ug/kg 43.850 88 70-133
1,3,5-Trimethylbenzene ug/kg 45.050 90 70-143
1,3-Dichlorobenzene ug/kg 43.950 88 70-144
1,3-Dichloropropane ug/kg 43.650 87 70-132
1,4-Dichlorobenzene ug/kg 43.650 87 70-142
2,2-Dichloropropane ug/kg 43.150 86 68-152
2-Butanone (MEK)ug/kg 74.1J100 74 70-149
2-Chlorotoluene ug/kg 44.550 89 70-141
2-Hexanone ug/kg 86.4100 86 70-149
4-Chlorotoluene ug/kg 46.750 93 70-149
4-Methyl-2-pentanone (MIBK)ug/kg 84.9100 85 70-153
Acetone ug/kg 81.1J100 81 70-157
Benzene ug/kg 41.350 83 70-130
Bromobenzene ug/kg 42.850 86 70-141
Bromochloromethane ug/kg 40.950 82 70-149
Bromodichloromethane ug/kg 44.950 90 70-130
Bromoform ug/kg 42.250 84 70-131
Bromomethane ug/kg 45.850 92 64-136
Carbon tetrachloride ug/kg 43.150 86 70-154
Chlorobenzene ug/kg 44.550 89 70-135
Chloroethane ug/kg 47.750 95 68-151
Chloroform ug/kg 44.250 88 70-130
Chloromethane ug/kg 43.850 88 70-132
cis-1,2-Dichloroethene ug/kg 41.650 83 70-140
cis-1,3-Dichloropropene ug/kg 47.050 94 70-137
Dibromochloromethane ug/kg 45.250 90 70-130
Dibromomethane ug/kg 41.850 84 70-136
Dichlorodifluoromethane ug/kg 44.750 89 36-148
Diisopropyl ether ug/kg 44.250 88 70-139
Ethylbenzene ug/kg 44.250 88 70-137
Hexachloro-1,3-butadiene ug/kg 43.350 87 70-145
Isopropylbenzene (Cumene)ug/kg 46.550 93 70-141
m&p-Xylene ug/kg 89.2100 89 70-140
Methyl-tert-butyl ether ug/kg 43.650 87 45-150
Methylene Chloride ug/kg 38.850 78 70-133
n-Butylbenzene ug/kg 47.650 95 65-155
n-Propylbenzene ug/kg 45.750 91 70-148
Naphthalene ug/kg 48.750 97 70-148
o-Xylene ug/kg 45.850 92 70-141
p-Isopropyltoluene ug/kg 46.950 94 70-148
sec-Butylbenzene ug/kg 46.650 93 70-145
Styrene ug/kg 47.350 95 70-138
tert-Butylbenzene ug/kg 46.450 93 70-143
Tetrachloroethene ug/kg 44.250 88 70-140
Toluene ug/kg 41.550 83 70-130
trans-1,2-Dichloroethene ug/kg 41.050 82 70-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 105 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640269LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 44.350 89 70-138
Trichloroethene ug/kg 43.350 87 70-132
Trichlorofluoromethane ug/kg 44.050 88 69-134
Vinyl acetate ug/kg 97.7100 98 24-161
Vinyl chloride ug/kg 45.450 91 55-140
Xylene (Total)ug/kg 135150 90 70-141
1,2-Dichloroethane-d4 (S)%85 70-132
4-Bromofluorobenzene (S)%102 70-130
Dibromofluoromethane (S)%96 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
640986MATRIX SPIKE SAMPLE:
MSSpike
Result
9299254014
1,1-Dichloroethene ug/kg 38.041.3 92 49-180ND
Benzene ug/kg 35.841.3 87 50-166ND
Chlorobenzene ug/kg 41.241.3 100 43-169ND
Toluene ug/kg 41.041.3 99 52-163ND
Trichloroethene ug/kg 38.741.3 94 49-167ND
1,2-Dichloroethane-d4 (S)%96 70-132
4-Bromofluorobenzene (S)%91 70-130
Dibromofluoromethane (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9299171005
640985SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 106 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9299171005
640985SAMPLE DUPLICATE:
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg 75.1J 30111J
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 107 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9299171005
640985SAMPLE DUPLICATE:
Xylene (Total)ug/kg ND
1,2-Dichloroethane-d4 (S)%108 13100
4-Bromofluorobenzene (S)%85 2185
Dibromofluoromethane (S)%107 17103
Toluene-d8 (S)%99 21100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 108 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/16150
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:9299254020, 9299254021, 9299254022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:640273
Associated Lab Samples:9299254020, 9299254021, 9299254022
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/29/11 12:42
1,1,1-Trichloroethane ug/kg ND 5.0 07/29/11 12:42
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/29/11 12:42
1,1,2-Trichloroethane ug/kg ND 5.0 07/29/11 12:42
1,1-Dichloroethane ug/kg ND 5.0 07/29/11 12:42
1,1-Dichloroethene ug/kg ND 5.0 07/29/11 12:42
1,1-Dichloropropene ug/kg ND 5.0 07/29/11 12:42
1,2,3-Trichlorobenzene ug/kg ND 5.0 07/29/11 12:42
1,2,3-Trichloropropane ug/kg ND 5.0 07/29/11 12:42
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/29/11 12:42
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/29/11 12:42
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 07/29/11 12:42
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/29/11 12:42
1,2-Dichlorobenzene ug/kg ND 5.0 07/29/11 12:42
1,2-Dichloroethane ug/kg ND 5.0 07/29/11 12:42
1,2-Dichloropropane ug/kg ND 5.0 07/29/11 12:42
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/29/11 12:42
1,3-Dichlorobenzene ug/kg ND 5.0 07/29/11 12:42
1,3-Dichloropropane ug/kg ND 5.0 07/29/11 12:42
1,4-Dichlorobenzene ug/kg ND 5.0 07/29/11 12:42
2,2-Dichloropropane ug/kg ND 5.0 07/29/11 12:42
2-Butanone (MEK)ug/kg ND 100 07/29/11 12:42
2-Chlorotoluene ug/kg ND 5.0 07/29/11 12:42
2-Hexanone ug/kg ND 50.0 07/29/11 12:42
4-Chlorotoluene ug/kg ND 5.0 07/29/11 12:42
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/29/11 12:42
Acetone ug/kg ND 100 07/29/11 12:42
Benzene ug/kg ND 5.0 07/29/11 12:42
Bromobenzene ug/kg ND 5.0 07/29/11 12:42
Bromochloromethane ug/kg ND 5.0 07/29/11 12:42
Bromodichloromethane ug/kg ND 5.0 07/29/11 12:42
Bromoform ug/kg ND 5.0 07/29/11 12:42
Bromomethane ug/kg ND 10.0 07/29/11 12:42
Carbon tetrachloride ug/kg ND 5.0 07/29/11 12:42
Chlorobenzene ug/kg ND 5.0 07/29/11 12:42
Chloroethane ug/kg ND 10.0 07/29/11 12:42
Chloroform ug/kg ND 5.0 07/29/11 12:42
Chloromethane ug/kg ND 10.0 07/29/11 12:42
cis-1,2-Dichloroethene ug/kg ND 5.0 07/29/11 12:42
cis-1,3-Dichloropropene ug/kg ND 5.0 07/29/11 12:42
Dibromochloromethane ug/kg ND 5.0 07/29/11 12:42
Dibromomethane ug/kg ND 5.0 07/29/11 12:42
Dichlorodifluoromethane ug/kg ND 10.0 07/29/11 12:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 109 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:640273
Associated Lab Samples:9299254020, 9299254021, 9299254022
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.0 07/29/11 12:42
Ethylbenzene ug/kg ND 5.0 07/29/11 12:42
Hexachloro-1,3-butadiene ug/kg ND 5.0 07/29/11 12:42
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/29/11 12:42
m&p-Xylene ug/kg ND 10.0 07/29/11 12:42
Methyl-tert-butyl ether ug/kg ND 5.0 07/29/11 12:42
Methylene Chloride ug/kg ND 20.0 07/29/11 12:42
n-Butylbenzene ug/kg ND 5.0 07/29/11 12:42
n-Propylbenzene ug/kg ND 5.0 07/29/11 12:42
Naphthalene ug/kg 1.4J 5.0 07/29/11 12:42
o-Xylene ug/kg ND 5.0 07/29/11 12:42
p-Isopropyltoluene ug/kg ND 5.0 07/29/11 12:42
sec-Butylbenzene ug/kg ND 5.0 07/29/11 12:42
Styrene ug/kg ND 5.0 07/29/11 12:42
tert-Butylbenzene ug/kg ND 5.0 07/29/11 12:42
Tetrachloroethene ug/kg ND 5.0 07/29/11 12:42
Toluene ug/kg ND 5.0 07/29/11 12:42
trans-1,2-Dichloroethene ug/kg ND 5.0 07/29/11 12:42
trans-1,3-Dichloropropene ug/kg ND 5.0 07/29/11 12:42
Trichloroethene ug/kg ND 5.0 07/29/11 12:42
Trichlorofluoromethane ug/kg ND 5.0 07/29/11 12:42
Vinyl acetate ug/kg ND 50.0 07/29/11 12:42
Vinyl chloride ug/kg ND 10.0 07/29/11 12:42
Xylene (Total)ug/kg ND 10.0 07/29/11 12:42
1,2-Dichloroethane-d4 (S)%94 70-132 07/29/11 12:42
4-Bromofluorobenzene (S)%93 70-130 07/29/11 12:42
Dibromofluoromethane (S)%99 70-130 07/29/11 12:42
Toluene-d8 (S)%100 70-130 07/29/11 12:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640274LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 45.050 90 70-131
1,1,1-Trichloroethane ug/kg 42.150 84 70-141
1,1,2,2-Tetrachloroethane ug/kg 45.550 91 70-130
1,1,2-Trichloroethane ug/kg 43.150 86 70-132
1,1-Dichloroethane ug/kg 41.150 82 70-143
1,1-Dichloroethene ug/kg 40.350 81 70-137
1,1-Dichloropropene ug/kg 40.050 80 70-135
1,2,3-Trichlorobenzene ug/kg 46.650 93 69-153
1,2,3-Trichloropropane ug/kg 42.150 84 70-130
1,2,4-Trichlorobenzene ug/kg 46.850 94 55-171
1,2,4-Trimethylbenzene ug/kg 45.150 90 70-149
1,2-Dibromo-3-chloropropane ug/kg 46.150 92 68-141
1,2-Dibromoethane (EDB)ug/kg 41.950 84 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 110 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640274LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 45.250 90 70-140
1,2-Dichloroethane ug/kg 40.750 81 70-137
1,2-Dichloropropane ug/kg 42.150 84 70-133
1,3,5-Trimethylbenzene ug/kg 44.550 89 70-143
1,3-Dichlorobenzene ug/kg 43.750 87 70-144
1,3-Dichloropropane ug/kg 42.250 84 70-132
1,4-Dichlorobenzene ug/kg 43.750 87 70-142
2,2-Dichloropropane ug/kg 41.250 82 68-152
2-Butanone (MEK)ug/kg 78.5J100 78 70-149
2-Chlorotoluene ug/kg 43.650 87 70-141
2-Hexanone ug/kg 90.9100 91 70-149
4-Chlorotoluene ug/kg 45.850 92 70-149
4-Methyl-2-pentanone (MIBK)ug/kg 87.9100 88 70-153
Acetone ug/kg 82.6J100 83 70-157
Benzene ug/kg 39.850 80 70-130
Bromobenzene ug/kg 42.250 84 70-141
Bromochloromethane ug/kg 39.550 79 70-149
Bromodichloromethane ug/kg 43.050 86 70-130
Bromoform ug/kg 42.450 85 70-131
Bromomethane ug/kg 42.850 86 64-136
Carbon tetrachloride ug/kg 42.550 85 70-154
Chlorobenzene ug/kg 41.950 84 70-135
Chloroethane ug/kg 46.550 93 68-151
Chloroform ug/kg 43.450 87 70-130
Chloromethane ug/kg 41.450 83 70-132
cis-1,2-Dichloroethene ug/kg 41.050 82 70-140
cis-1,3-Dichloropropene ug/kg 45.050 90 70-137
Dibromochloromethane ug/kg 44.150 88 70-130
Dibromomethane ug/kg 40.650 81 70-136
Dichlorodifluoromethane ug/kg 43.350 87 36-148
Diisopropyl ether ug/kg 42.250 84 70-139
Ethylbenzene ug/kg 42.050 84 70-137
Hexachloro-1,3-butadiene ug/kg 44.750 89 70-145
Isopropylbenzene (Cumene)ug/kg 45.050 90 70-141
m&p-Xylene ug/kg 84.5100 85 70-140
Methyl-tert-butyl ether ug/kg 41.950 84 45-150
Methylene Chloride ug/kg 37.750 75 70-133
n-Butylbenzene ug/kg 46.750 93 65-155
n-Propylbenzene ug/kg 44.750 89 70-148
Naphthalene ug/kg 52.650 105 70-148
o-Xylene ug/kg 43.950 88 70-141
p-Isopropyltoluene ug/kg 46.450 93 70-148
sec-Butylbenzene ug/kg 45.250 90 70-145
Styrene ug/kg 45.450 91 70-138
tert-Butylbenzene ug/kg 46.150 92 70-143
Tetrachloroethene ug/kg 41.650 83 70-140
Toluene ug/kg 40.750 81 70-130
trans-1,2-Dichloroethene ug/kg 39.850 80 70-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 111 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640274LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 43.350 87 70-138
Trichloroethene ug/kg 41.350 83 70-132
Trichlorofluoromethane ug/kg 42.250 84 69-134
Vinyl acetate ug/kg 90.3100 90 24-161
Vinyl chloride ug/kg 45.050 90 55-140
Xylene (Total)ug/kg 128150 86 70-141
1,2-Dichloroethane-d4 (S)%91 70-132
4-Bromofluorobenzene (S)%97 70-130
Dibromofluoromethane (S)%97 70-130
Toluene-d8 (S)%103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 112 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/16161
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:9299254013, 9299254015, 9299254016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:640989
Associated Lab Samples:9299254013, 9299254015, 9299254016
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/31/11 11:33
1,1,1-Trichloroethane ug/kg ND 5.0 07/31/11 11:33
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/31/11 11:33
1,1,2-Trichloroethane ug/kg ND 5.0 07/31/11 11:33
1,1-Dichloroethane ug/kg ND 5.0 07/31/11 11:33
1,1-Dichloroethene ug/kg ND 5.0 07/31/11 11:33
1,1-Dichloropropene ug/kg ND 5.0 07/31/11 11:33
1,2,3-Trichlorobenzene ug/kg ND 5.0 07/31/11 11:33
1,2,3-Trichloropropane ug/kg ND 5.0 07/31/11 11:33
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/31/11 11:33
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/31/11 11:33
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 07/31/11 11:33
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/31/11 11:33
1,2-Dichlorobenzene ug/kg ND 5.0 07/31/11 11:33
1,2-Dichloroethane ug/kg ND 5.0 07/31/11 11:33
1,2-Dichloropropane ug/kg ND 5.0 07/31/11 11:33
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/31/11 11:33
1,3-Dichlorobenzene ug/kg ND 5.0 07/31/11 11:33
1,3-Dichloropropane ug/kg ND 5.0 07/31/11 11:33
1,4-Dichlorobenzene ug/kg ND 5.0 07/31/11 11:33
2,2-Dichloropropane ug/kg ND 5.0 07/31/11 11:33
2-Butanone (MEK)ug/kg ND 100 07/31/11 11:33
2-Chlorotoluene ug/kg ND 5.0 07/31/11 11:33
2-Hexanone ug/kg ND 50.0 07/31/11 11:33
4-Chlorotoluene ug/kg ND 5.0 07/31/11 11:33
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/31/11 11:33
Acetone ug/kg ND 100 07/31/11 11:33
Benzene ug/kg ND 5.0 07/31/11 11:33
Bromobenzene ug/kg ND 5.0 07/31/11 11:33
Bromochloromethane ug/kg ND 5.0 07/31/11 11:33
Bromodichloromethane ug/kg ND 5.0 07/31/11 11:33
Bromoform ug/kg ND 5.0 07/31/11 11:33
Bromomethane ug/kg ND 10.0 07/31/11 11:33
Carbon tetrachloride ug/kg ND 5.0 07/31/11 11:33
Chlorobenzene ug/kg ND 5.0 07/31/11 11:33
Chloroethane ug/kg ND 10.0 07/31/11 11:33
Chloroform ug/kg ND 5.0 07/31/11 11:33
Chloromethane ug/kg ND 10.0 07/31/11 11:33
cis-1,2-Dichloroethene ug/kg ND 5.0 07/31/11 11:33
cis-1,3-Dichloropropene ug/kg ND 5.0 07/31/11 11:33
Dibromochloromethane ug/kg ND 5.0 07/31/11 11:33
Dibromomethane ug/kg ND 5.0 07/31/11 11:33
Dichlorodifluoromethane ug/kg ND 10.0 07/31/11 11:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 113 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:640989
Associated Lab Samples:9299254013, 9299254015, 9299254016
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.0 07/31/11 11:33
Ethylbenzene ug/kg ND 5.0 07/31/11 11:33
Hexachloro-1,3-butadiene ug/kg ND 5.0 07/31/11 11:33
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/31/11 11:33
m&p-Xylene ug/kg ND 10.0 07/31/11 11:33
Methyl-tert-butyl ether ug/kg ND 5.0 07/31/11 11:33
Methylene Chloride ug/kg ND 20.0 07/31/11 11:33
n-Butylbenzene ug/kg ND 5.0 07/31/11 11:33
n-Propylbenzene ug/kg ND 5.0 07/31/11 11:33
Naphthalene ug/kg ND 5.0 07/31/11 11:33
o-Xylene ug/kg ND 5.0 07/31/11 11:33
p-Isopropyltoluene ug/kg ND 5.0 07/31/11 11:33
sec-Butylbenzene ug/kg ND 5.0 07/31/11 11:33
Styrene ug/kg ND 5.0 07/31/11 11:33
tert-Butylbenzene ug/kg ND 5.0 07/31/11 11:33
Tetrachloroethene ug/kg ND 5.0 07/31/11 11:33
Toluene ug/kg ND 5.0 07/31/11 11:33
trans-1,2-Dichloroethene ug/kg ND 5.0 07/31/11 11:33
trans-1,3-Dichloropropene ug/kg ND 5.0 07/31/11 11:33
Trichloroethene ug/kg ND 5.0 07/31/11 11:33
Trichlorofluoromethane ug/kg ND 5.0 07/31/11 11:33
Vinyl acetate ug/kg ND 50.0 07/31/11 11:33
Vinyl chloride ug/kg ND 10.0 07/31/11 11:33
Xylene (Total)ug/kg ND 10.0 07/31/11 11:33
1,2-Dichloroethane-d4 (S)%93 70-132 07/31/11 11:33
4-Bromofluorobenzene (S)%96 70-130 07/31/11 11:33
Dibromofluoromethane (S)%99 70-130 07/31/11 11:33
Toluene-d8 (S)%106 70-130 07/31/11 11:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640990LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 50.550 101 70-131
1,1,1-Trichloroethane ug/kg 45.550 91 70-141
1,1,2,2-Tetrachloroethane ug/kg 45.550 91 70-130
1,1,2-Trichloroethane ug/kg 47.150 94 70-132
1,1-Dichloroethane ug/kg 44.850 90 70-143
1,1-Dichloroethene ug/kg 43.450 87 70-137
1,1-Dichloropropene ug/kg 42.350 85 70-135
1,2,3-Trichlorobenzene ug/kg 46.550 93 69-153
1,2,3-Trichloropropane ug/kg 41.250 82 70-130
1,2,4-Trichlorobenzene ug/kg 48.650 97 55-171
1,2,4-Trimethylbenzene ug/kg 48.150 96 70-149
1,2-Dibromo-3-chloropropane ug/kg 43.750 87 68-141
1,2-Dibromoethane (EDB)ug/kg 43.850 88 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 114 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640990LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 46.950 94 70-140
1,2-Dichloroethane ug/kg 43.350 87 70-137
1,2-Dichloropropane ug/kg 46.750 93 70-133
1,3,5-Trimethylbenzene ug/kg 48.550 97 70-143
1,3-Dichlorobenzene ug/kg 47.950 96 70-144
1,3-Dichloropropane ug/kg 44.950 90 70-132
1,4-Dichlorobenzene ug/kg 46.450 93 70-142
2,2-Dichloropropane ug/kg 47.650 95 68-152
2-Butanone (MEK)ug/kg 81.1J100 81 70-149
2-Chlorotoluene ug/kg 47.750 95 70-141
2-Hexanone ug/kg 80.3100 80 70-149
4-Chlorotoluene ug/kg 49.050 98 70-149
4-Methyl-2-pentanone (MIBK)ug/kg 87.2100 87 70-153
Acetone ug/kg 93.5J100 94 70-157
Benzene ug/kg 44.150 88 70-130
Bromobenzene ug/kg 44.550 89 70-141
Bromochloromethane ug/kg 43.050 86 70-149
Bromodichloromethane ug/kg 48.050 96 70-130
Bromoform ug/kg 44.250 88 70-131
Bromomethane ug/kg 47.750 95 64-136
Carbon tetrachloride ug/kg 45.550 91 70-154
Chlorobenzene ug/kg 48.150 96 70-135
Chloroethane ug/kg 48.450 97 68-151
Chloroform ug/kg 46.750 93 70-130
Chloromethane ug/kg 43.750 87 70-132
cis-1,2-Dichloroethene ug/kg 43.250 86 70-140
cis-1,3-Dichloropropene ug/kg 48.650 97 70-137
Dibromochloromethane ug/kg 47.550 95 70-130
Dibromomethane ug/kg 44.450 89 70-136
Dichlorodifluoromethane ug/kg 42.850 86 36-148
Diisopropyl ether ug/kg 45.450 91 70-139
Ethylbenzene ug/kg 46.550 93 70-137
Hexachloro-1,3-butadiene ug/kg 45.650 91 70-145
Isopropylbenzene (Cumene)ug/kg 49.550 99 70-141
m&p-Xylene ug/kg 94.0100 94 70-140
Methyl-tert-butyl ether ug/kg 44.050 88 45-150
Methylene Chloride ug/kg 46.050 92 70-133
n-Butylbenzene ug/kg 49.850 100 65-155
n-Propylbenzene ug/kg 48.050 96 70-148
Naphthalene ug/kg 48.850 98 70-148
o-Xylene ug/kg 50.450 101 70-141
p-Isopropyltoluene ug/kg 49.650 99 70-148
sec-Butylbenzene ug/kg 48.850 98 70-145
Styrene ug/kg 50.650 101 70-138
tert-Butylbenzene ug/kg 48.950 98 70-143
Tetrachloroethene ug/kg 47.650 95 70-140
Toluene ug/kg 45.250 90 70-130
trans-1,2-Dichloroethene ug/kg 43.850 88 70-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 115 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640990LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 48.150 96 70-138
Trichloroethene ug/kg 46.850 94 70-132
Trichlorofluoromethane ug/kg 46.150 92 69-134
Vinyl acetate ug/kg 130100 130 24-161
Vinyl chloride ug/kg 47.950 96 55-140
Xylene (Total)ug/kg 144150 96 70-141
1,2-Dichloroethane-d4 (S)%86 70-132
4-Bromofluorobenzene (S)%102 70-130
Dibromofluoromethane (S)%93 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
641010MATRIX SPIKE SAMPLE:
MSSpike
Result
9298927006
1,1-Dichloroethene ug/kg 60.872.7 84 49-180ND
Benzene ug/kg 60.872.7 84 50-166ND
Chlorobenzene ug/kg 72.372.7 99 43-169ND
Toluene ug/kg 72.072.7 99 52-163ND
Trichloroethene ug/kg 69.172.7 95 49-167ND
1,2-Dichloroethane-d4 (S)%94 70-132
4-Bromofluorobenzene (S)%92 70-130
Dibromofluoromethane (S)%93 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9298927005
641009SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 116 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9298927005
641009SAMPLE DUPLICATE:
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 117 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9298927005
641009SAMPLE DUPLICATE:
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%91 4186
4-Bromofluorobenzene (S)%94 3495
Dibromofluoromethane (S)%94 3593
Toluene-d8 (S)%102 35103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 118 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/4083
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:9299254001, 9299254002, 9299254003
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9298829001
640126SAMPLE DUPLICATE:
Percent Moisture %10.7 9 259.8
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9299254003
640127SAMPLE DUPLICATE:
Percent Moisture %13.4 5 2512.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 119 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/4084
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:9299254004, 9299254013, 9299254014, 9299254015, 9299254016, 9299254017, 9299254018, 9299254019,
9299254020, 9299254021, 9299254022, 9299254023
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9299254004
640199SAMPLE DUPLICATE:
Percent Moisture %12.7 13 2511.1
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9299254023
640200SAMPLE DUPLICATE:
Percent Moisture %9.1 4 258.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 120 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/4086
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:9299254024, 9299254025, 9299254026, 9299254027, 9299254028
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9299111001
640864SAMPLE DUPLICATE:
Percent Moisture %26.1 15 2522.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9299303001
640865SAMPLE DUPLICATE:
Percent Moisture %13.1 10 2511.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 121 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/10234
EPA 7196
EPA 7196
7196 Chromium, Hexavalent
Associated Lab Samples:9299254016, 9299254017, 9299254018, 9299254019, 9299254020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:641350
Associated Lab Samples:9299254016, 9299254017, 9299254018, 9299254019, 9299254020
Matrix:Solid
Analyzed
Chromium, Hexavalent mg/kg 1.0J 5.0 N208/02/11 17:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
641351LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 54.9 N25011090-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
641352MATRIX SPIKE SAMPLE:
MSSpike
Result
9299172041
Chromium, Hexavalent mg/kg 13.2 N215.3 82 75-1250.51J
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
641356MATRIX SPIKE SAMPLE:
MSSpike
Result
9299172042
Chromium, Hexavalent mg/kg 15.3 M0,N227.2 54 75-1250.65J
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9299172043
641357SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND N2200.27J
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9299172044
641358SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 0.63J N2200.45J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 122 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/10250
EPA 7196
EPA 7196
7196 Chromium, Hexavalent
Associated Lab Samples:9299254021, 9299254022, 9299254023, 9299254024, 9299254025, 9299254026, 9299254027, 9299254028
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:642188
Associated Lab Samples:9299254021, 9299254022, 9299254023, 9299254024, 9299254025, 9299254026, 9299254027, 9299254028
Matrix:Solid
Analyzed
Chromium, Hexavalent mg/kg 1.9J 5.0 N208/04/11 13:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
642189LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 48.7 N2509790-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
642190MATRIX SPIKE SAMPLE:
MSSpike
Result
9299254021
Chromium, Hexavalent mg/kg 21.2 N224.2 87 75-125ND
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
642194MATRIX SPIKE SAMPLE:
MSSpike
Result
9299254022
Chromium, Hexavalent mg/kg 9.3 M0,N2214575-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9299254023
642195SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND N220ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9299254024
642196SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND N220ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 123 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Project No.:
Project:
9299254
1200 SOUTH BOULEVARD
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Sample went dry during microwave extraction twice.1g
Surrogate recovery outside control limits due to matrix interferences (confirmed by re-analysis).2g
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-extraction and re-analysis).3g
Common Laboratory Contaminant.C9
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.D6
The internal standard response was outside the laboratory acceptance limits confirmed by reanalysis. The results
reported are from the most QC compliant analysis.IO
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
The lab does not hold TNI accreditation for this parameter.N2
Sample extract could not be concentrated to the routine final volume, resulting in elevated reporting limits.P3
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/18/2011 04:58 PM Page 124 of 124
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
August 08, 2011
LIMS USE: FR - ANDREW FRANTZ
LIMS OBJECT ID: 9299302
9299302
Project:
Pace Project No.:
RE:
Mr. Andrew Frantz
AMEC-Charlotte
2801 Yorkmont Road
Suite 100
Charlotte, NC 28208
1200 South Blvd 6228-11-5486
Dear Mr. Frantz:
Enclosed are the analytical results for sample(s) received by the laboratory on July 29, 2011. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards, where applicable, unless otherwise narrated in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001South Carolina Drinking Water Cert. #: 99006003Virginia Drinking Water Certification #: 00213
Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031West Virginia Certification #: 357Virginia/VELAP Certification #: 460144
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030North Carolina Bioassay Certification #: 9
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001Virginia Certification #: 00072West Virginia Certification #: 356
Virgina/VELAP Certification #: 460147
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
9299302001 SB-23 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
9299302002 SB-24 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
9299302003 SB-25 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
9299302004 SB-26 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
9299302005 SB-27 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
9299302006 SB-28 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
9299302007 SB-29 EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-AJMW
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
Trivalent Chromium Calculation 1 PASI-AEWS
EPA 7196 1 PASI-ALEP
9299302008 SB-23 EPA 8270 74 PASI-CBPJ
EPA 8260 64 PASI-CMCK
9299302009 SB-24 EPA 8270 74 PASI-CBPJ
EPA 8260 64 PASI-CMCK
9299302010 SB-25 EPA 8270 74 PASI-CBPJ
EPA 8260 64 PASI-CMCK
9299302011 SB-26 EPA 8270 74 PASI-CPPM
EPA 8260 64 PASI-CMCK
9299302012 SB-27 EPA 8270 74 PASI-CPPM
EPA 8260 64 PASI-CMCK
9299302015 SB-17 EPA 8270 74 PASI-CPPM
EPA 8260 64 PASI-CMCK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-23 Lab ID:9299302001 Collected:07/28/11 08:45 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 08/02/11 16:00 7440-36-008/02/11 09:000.70
Arsenic ND mg/kg 1 08/03/11 18:15 7440-38-208/02/11 09:000.70
Beryllium 0.58 mg/kg 1 08/02/11 16:00 7440-41-708/02/11 09:000.14
Cadmium 2.2 mg/kg 1 08/02/11 16:00 7440-43-908/02/11 09:000.14
Chromium 30.2 mg/kg 1 08/02/11 16:00 7440-47-308/02/11 09:000.70
Copper 50.3 mg/kg 1 08/02/11 16:00 7440-50-808/02/11 09:000.70
Lead 5.3 mg/kg 1 08/02/11 16:00 7439-92-108/02/11 09:000.70
Manganese 178 mg/kg 1 08/02/11 16:00 7439-96-508/02/11 09:000.70
Nickel 10.0 mg/kg 1 08/02/11 16:00 7440-02-008/02/11 09:000.70
Selenium ND mg/kg 1 08/02/11 16:00 7782-49-208/02/11 09:001.4
Silver ND mg/kg 1 08/02/11 16:00 7440-22-408/02/11 09:000.70
Thallium ND mg/kg 1 08/02/11 16:00 7440-28-008/02/11 09:001.4
Zinc 45.8 mg/kg 1 08/02/11 16:00 7440-66-608/02/11 09:001.4
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.019 mg/kg 1 08/03/11 12:27 7439-97-608/01/11 14:150.0063
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 08/03/11 16:31 83-32-907/29/11 13:04498
Acenaphthylene ND ug/kg 1 08/03/11 16:31 208-96-807/29/11 13:04498
Aniline ND ug/kg 1 08/03/11 16:31 62-53-307/29/11 13:04498
Anthracene ND ug/kg 1 08/03/11 16:31 120-12-707/29/11 13:04498
Benzo(a)anthracene ND ug/kg 1 08/03/11 16:31 56-55-307/29/11 13:04498
Benzo(a)pyrene ND ug/kg 1 08/03/11 16:31 50-32-807/29/11 13:04498
Benzo(b)fluoranthene ND ug/kg 1 08/03/11 16:31 205-99-207/29/11 13:04498
Benzo(g,h,i)perylene ND ug/kg 1 08/03/11 16:31 191-24-207/29/11 13:04498
Benzo(k)fluoranthene ND ug/kg 1 08/03/11 16:31 207-08-907/29/11 13:04498
Benzoic Acid ND ug/kg 1 08/03/11 16:31 65-85-007/29/11 13:042490
Benzyl alcohol ND ug/kg 1 08/03/11 16:31 100-51-607/29/11 13:04996
4-Bromophenylphenyl ether ND ug/kg 1 08/03/11 16:31 101-55-307/29/11 13:04498
Butylbenzylphthalate ND ug/kg 1 08/03/11 16:31 85-68-707/29/11 13:04498
4-Chloro-3-methylphenol ND ug/kg 1 08/03/11 16:31 59-50-707/29/11 13:04996
4-Chloroaniline ND ug/kg 1 08/03/11 16:31 106-47-807/29/11 13:042490
bis(2-Chloroethoxy)methane ND ug/kg 1 08/03/11 16:31 111-91-107/29/11 13:04498
bis(2-Chloroethyl) ether ND ug/kg 1 08/03/11 16:31 111-44-407/29/11 13:04498
bis(2-Chloroisopropyl) ether ND ug/kg 1 08/03/11 16:31 108-60-107/29/11 13:04498
2-Chloronaphthalene ND ug/kg 1 08/03/11 16:31 91-58-707/29/11 13:04498
2-Chlorophenol ND ug/kg 1 08/03/11 16:31 95-57-807/29/11 13:04498
4-Chlorophenylphenyl ether ND ug/kg 1 08/03/11 16:31 7005-72-307/29/11 13:04498
Chrysene ND ug/kg 1 08/03/11 16:31 218-01-907/29/11 13:04498
Dibenz(a,h)anthracene ND ug/kg 1 08/03/11 16:31 53-70-307/29/11 13:04498
Dibenzofuran ND ug/kg 1 08/03/11 16:31 132-64-907/29/11 13:04498
1,2-Dichlorobenzene ND ug/kg 1 08/03/11 16:31 95-50-107/29/11 13:04498
1,3-Dichlorobenzene ND ug/kg 1 08/03/11 16:31 541-73-107/29/11 13:04498
1,4-Dichlorobenzene ND ug/kg 1 08/03/11 16:31 106-46-707/29/11 13:04498
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 5 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-23 Lab ID:9299302001 Collected:07/28/11 08:45 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3,3'-Dichlorobenzidine ND ug/kg 1 08/03/11 16:31 91-94-107/29/11 13:042490
2,4-Dichlorophenol ND ug/kg 1 08/03/11 16:31 120-83-207/29/11 13:04498
Diethylphthalate ND ug/kg 1 08/03/11 16:31 84-66-207/29/11 13:04498
2,4-Dimethylphenol ND ug/kg 1 08/03/11 16:31 105-67-907/29/11 13:04498
Dimethylphthalate ND ug/kg 1 08/03/11 16:31 131-11-307/29/11 13:04498
Di-n-butylphthalate ND ug/kg 1 08/03/11 16:31 84-74-207/29/11 13:04498
4,6-Dinitro-2-methylphenol ND ug/kg 1 08/03/11 16:31 534-52-107/29/11 13:04996
2,4-Dinitrophenol ND ug/kg 1 08/03/11 16:31 51-28-507/29/11 13:042490
2,4-Dinitrotoluene ND ug/kg 1 08/03/11 16:31 121-14-207/29/11 13:04498
2,6-Dinitrotoluene ND ug/kg 1 08/03/11 16:31 606-20-207/29/11 13:04498
Di-n-octylphthalate ND ug/kg 1 08/03/11 16:31 117-84-007/29/11 13:04498
bis(2-Ethylhexyl)phthalate ND ug/kg 1 08/03/11 16:31 117-81-707/29/11 13:04498
Fluoranthene ND ug/kg 1 08/03/11 16:31 206-44-007/29/11 13:04498
Fluorene ND ug/kg 1 08/03/11 16:31 86-73-707/29/11 13:04498
Hexachloro-1,3-butadiene ND ug/kg 1 08/03/11 16:31 87-68-307/29/11 13:04498
Hexachlorobenzene ND ug/kg 1 08/03/11 16:31 118-74-107/29/11 13:04498
Hexachlorocyclopentadiene ND ug/kg 1 08/03/11 16:31 77-47-407/29/11 13:04498
Hexachloroethane ND ug/kg 1 08/03/11 16:31 67-72-107/29/11 13:04498
Indeno(1,2,3-cd)pyrene ND ug/kg 1 08/03/11 16:31 193-39-507/29/11 13:04498
Isophorone ND ug/kg 1 08/03/11 16:31 78-59-107/29/11 13:04498
1-Methylnaphthalene ND ug/kg 1 08/03/11 16:31 90-12-007/29/11 13:04498
2-Methylnaphthalene ND ug/kg 1 08/03/11 16:31 91-57-607/29/11 13:04498
2-Methylphenol(o-Cresol)ND ug/kg 1 08/03/11 16:31 95-48-707/29/11 13:04498
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 08/03/11 16:3107/29/11 13:04498
Naphthalene ND ug/kg 1 08/03/11 16:31 91-20-307/29/11 13:04498
2-Nitroaniline ND ug/kg 1 08/03/11 16:31 88-74-407/29/11 13:042490
3-Nitroaniline ND ug/kg 1 08/03/11 16:31 99-09-207/29/11 13:042490
4-Nitroaniline ND ug/kg 1 08/03/11 16:31 100-01-607/29/11 13:04996
Nitrobenzene ND ug/kg 1 08/03/11 16:31 98-95-307/29/11 13:04498
2-Nitrophenol ND ug/kg 1 08/03/11 16:31 88-75-507/29/11 13:04498
4-Nitrophenol ND ug/kg 1 08/03/11 16:31 100-02-707/29/11 13:042490
N-Nitrosodimethylamine ND ug/kg 1 08/03/11 16:31 62-75-907/29/11 13:04498
N-Nitroso-di-n-propylamine ND ug/kg 1 08/03/11 16:31 621-64-707/29/11 13:04498
N-Nitrosodiphenylamine ND ug/kg 1 08/03/11 16:31 86-30-607/29/11 13:04498
Pentachlorophenol ND ug/kg 1 08/03/11 16:31 87-86-507/29/11 13:042490
Phenanthrene ND ug/kg 1 08/03/11 16:31 85-01-807/29/11 13:04498
Phenol ND ug/kg 1 08/03/11 16:31 108-95-207/29/11 13:04498
Pyrene ND ug/kg 1 08/03/11 16:31 129-00-007/29/11 13:04498
1,2,4-Trichlorobenzene ND ug/kg 1 08/03/11 16:31 120-82-107/29/11 13:04498
2,4,5-Trichlorophenol ND ug/kg 1 08/03/11 16:31 95-95-407/29/11 13:04498
2,4,6-Trichlorophenol ND ug/kg 1 08/03/11 16:31 88-06-207/29/11 13:04498
Nitrobenzene-d5 (S)51 %1 08/03/11 16:31 4165-60-007/29/11 13:0423-110
2-Fluorobiphenyl (S)49 %1 08/03/11 16:31 321-60-807/29/11 13:0430-110
Terphenyl-d14 (S)48 %1 08/03/11 16:31 1718-51-007/29/11 13:0428-110
Phenol-d6 (S)48 %1 08/03/11 16:31 13127-88-307/29/11 13:0422-110
2-Fluorophenol (S)50 %1 08/03/11 16:31 367-12-407/29/11 13:0413-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 6 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-23 Lab ID:9299302001 Collected:07/28/11 08:45 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4,6-Tribromophenol (S)42 %1 08/03/11 16:31 118-79-607/29/11 13:0427-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/30/11 04:27 67-64-1130
Benzene ND ug/kg 1 07/30/11 04:27 71-43-26.5
Bromobenzene ND ug/kg 1 07/30/11 04:27 108-86-16.5
Bromochloromethane ND ug/kg 1 07/30/11 04:27 74-97-56.5
Bromodichloromethane ND ug/kg 1 07/30/11 04:27 75-27-46.5
Bromoform ND ug/kg 1 07/30/11 04:27 75-25-26.5
Bromomethane ND ug/kg 1 07/30/11 04:27 74-83-913.0
2-Butanone (MEK)ND ug/kg 1 07/30/11 04:27 78-93-3130
n-Butylbenzene ND ug/kg 1 07/30/11 04:27 104-51-86.5
sec-Butylbenzene ND ug/kg 1 07/30/11 04:27 135-98-86.5
tert-Butylbenzene ND ug/kg 1 07/30/11 04:27 98-06-66.5
Carbon tetrachloride ND ug/kg 1 07/30/11 04:27 56-23-56.5
Chlorobenzene ND ug/kg 1 07/30/11 04:27 108-90-76.5
Chloroethane ND ug/kg 1 07/30/11 04:27 75-00-313.0
Chloroform ND ug/kg 1 07/30/11 04:27 67-66-36.5
Chloromethane ND ug/kg 1 07/30/11 04:27 74-87-313.0
2-Chlorotoluene ND ug/kg 1 07/30/11 04:27 95-49-86.5
4-Chlorotoluene ND ug/kg 1 07/30/11 04:27 106-43-46.5
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/30/11 04:27 96-12-86.5
Dibromochloromethane ND ug/kg 1 07/30/11 04:27 124-48-16.5
1,2-Dibromoethane (EDB)ND ug/kg 1 07/30/11 04:27 106-93-46.5
Dibromomethane ND ug/kg 1 07/30/11 04:27 74-95-36.5
1,2-Dichlorobenzene ND ug/kg 1 07/30/11 04:27 95-50-16.5
1,3-Dichlorobenzene ND ug/kg 1 07/30/11 04:27 541-73-16.5
1,4-Dichlorobenzene ND ug/kg 1 07/30/11 04:27 106-46-76.5
Dichlorodifluoromethane ND ug/kg 1 07/30/11 04:27 75-71-813.0
1,1-Dichloroethane ND ug/kg 1 07/30/11 04:27 75-34-36.5
1,2-Dichloroethane ND ug/kg 1 07/30/11 04:27 107-06-26.5
1,1-Dichloroethene ND ug/kg 1 07/30/11 04:27 75-35-46.5
cis-1,2-Dichloroethene ND ug/kg 1 07/30/11 04:27 156-59-26.5
trans-1,2-Dichloroethene ND ug/kg 1 07/30/11 04:27 156-60-56.5
1,2-Dichloropropane ND ug/kg 1 07/30/11 04:27 78-87-56.5
1,3-Dichloropropane ND ug/kg 1 07/30/11 04:27 142-28-96.5
2,2-Dichloropropane ND ug/kg 1 07/30/11 04:27 594-20-76.5
1,1-Dichloropropene ND ug/kg 1 07/30/11 04:27 563-58-66.5
cis-1,3-Dichloropropene ND ug/kg 1 07/30/11 04:27 10061-01-56.5
trans-1,3-Dichloropropene ND ug/kg 1 07/30/11 04:27 10061-02-66.5
Diisopropyl ether ND ug/kg 1 07/30/11 04:27 108-20-36.5
Ethylbenzene ND ug/kg 1 07/30/11 04:27 100-41-46.5
Hexachloro-1,3-butadiene ND ug/kg 1 07/30/11 04:27 87-68-36.5
2-Hexanone ND ug/kg 1 07/30/11 04:27 591-78-665.1
Isopropylbenzene (Cumene)ND ug/kg 1 07/30/11 04:27 98-82-86.5
p-Isopropyltoluene ND ug/kg 1 07/30/11 04:27 99-87-66.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 7 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-23 Lab ID:9299302001 Collected:07/28/11 08:45 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Methylene Chloride ND ug/kg 1 07/30/11 04:27 75-09-226.0
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/30/11 04:27 108-10-165.1
Methyl-tert-butyl ether ND ug/kg 1 07/30/11 04:27 1634-04-46.5
Naphthalene ND ug/kg 1 07/30/11 04:27 91-20-36.5
n-Propylbenzene ND ug/kg 1 07/30/11 04:27 103-65-16.5
Styrene ND ug/kg 1 07/30/11 04:27 100-42-56.5
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/30/11 04:27 630-20-66.5
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/30/11 04:27 79-34-56.5
Tetrachloroethene ND ug/kg 1 07/30/11 04:27 127-18-46.5
Toluene ND ug/kg 1 07/30/11 04:27 108-88-36.5
1,2,3-Trichlorobenzene ND ug/kg 1 07/30/11 04:27 87-61-66.5
1,2,4-Trichlorobenzene ND ug/kg 1 07/30/11 04:27 120-82-16.5
1,1,1-Trichloroethane ND ug/kg 1 07/30/11 04:27 71-55-66.5
1,1,2-Trichloroethane ND ug/kg 1 07/30/11 04:27 79-00-56.5
Trichloroethene ND ug/kg 1 07/30/11 04:27 79-01-66.5
Trichlorofluoromethane ND ug/kg 1 07/30/11 04:27 75-69-46.5
1,2,3-Trichloropropane ND ug/kg 1 07/30/11 04:27 96-18-46.5
1,2,4-Trimethylbenzene ND ug/kg 1 07/30/11 04:27 95-63-66.5
1,3,5-Trimethylbenzene ND ug/kg 1 07/30/11 04:27 108-67-86.5
Vinyl acetate ND ug/kg 1 07/30/11 04:27 108-05-465.1
Vinyl chloride ND ug/kg 1 07/30/11 04:27 75-01-413.0
Xylene (Total)ND ug/kg 1 07/30/11 04:27 1330-20-713.0
m&p-Xylene ND ug/kg 1 07/30/11 04:27 179601-23-113.0
o-Xylene ND ug/kg 1 07/30/11 04:27 95-47-66.5
Dibromofluoromethane (S)104 %1 07/30/11 04:27 1868-53-770-130
Toluene-d8 (S)103 %1 07/30/11 04:27 2037-26-570-130
4-Bromofluorobenzene (S)91 %1 07/30/11 04:27 460-00-470-130
1,2-Dichloroethane-d4 (S)94 %1 07/30/11 04:27 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 33.8 %1 08/01/11 09:040.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 30.2 mg/kg 1 08/05/11 16:42 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/04/11 13:23 18540-29-9 N208/04/11 10:432.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 8 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-24 Lab ID:9299302002 Collected:07/28/11 09:45 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 08/02/11 16:03 7440-36-008/02/11 09:000.47
Arsenic 0.66 mg/kg 1 08/03/11 17:13 7440-38-208/02/11 09:000.47
Beryllium 0.19 mg/kg 1 08/02/11 16:03 7440-41-708/02/11 09:000.094
Cadmium 1.7 mg/kg 1 08/02/11 16:03 7440-43-908/02/11 09:000.094
Chromium 8.4 mg/kg 1 08/02/11 16:03 7440-47-308/02/11 09:000.47
Copper 27.7 mg/kg 1 08/02/11 16:03 7440-50-808/02/11 09:000.47
Lead 7.7 mg/kg 1 08/02/11 16:03 7439-92-108/02/11 09:000.47
Manganese 116 mg/kg 1 08/02/11 16:03 7439-96-508/02/11 09:000.47
Nickel 0.99 mg/kg 1 08/02/11 16:03 7440-02-008/02/11 09:000.47
Selenium 1.1 mg/kg 1 08/02/11 16:03 7782-49-208/02/11 09:000.94
Silver ND mg/kg 1 08/02/11 16:03 7440-22-408/02/11 09:000.47
Thallium ND mg/kg 1 08/02/11 16:03 7440-28-008/02/11 09:000.94
Zinc 9.7 mg/kg 1 08/02/11 16:03 7440-66-608/02/11 09:000.94
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.014 mg/kg 1 08/03/11 12:33 7439-97-608/01/11 14:150.0060
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 08/03/11 16:59 83-32-907/29/11 13:04432
Acenaphthylene ND ug/kg 1 08/03/11 16:59 208-96-807/29/11 13:04432
Aniline ND ug/kg 1 08/03/11 16:59 62-53-307/29/11 13:04432
Anthracene ND ug/kg 1 08/03/11 16:59 120-12-707/29/11 13:04432
Benzo(a)anthracene ND ug/kg 1 08/03/11 16:59 56-55-307/29/11 13:04432
Benzo(a)pyrene ND ug/kg 1 08/03/11 16:59 50-32-807/29/11 13:04432
Benzo(b)fluoranthene ND ug/kg 1 08/03/11 16:59 205-99-207/29/11 13:04432
Benzo(g,h,i)perylene ND ug/kg 1 08/03/11 16:59 191-24-207/29/11 13:04432
Benzo(k)fluoranthene ND ug/kg 1 08/03/11 16:59 207-08-907/29/11 13:04432
Benzoic Acid ND ug/kg 1 08/03/11 16:59 65-85-007/29/11 13:042160
Benzyl alcohol ND ug/kg 1 08/03/11 16:59 100-51-607/29/11 13:04864
4-Bromophenylphenyl ether ND ug/kg 1 08/03/11 16:59 101-55-307/29/11 13:04432
Butylbenzylphthalate ND ug/kg 1 08/03/11 16:59 85-68-707/29/11 13:04432
4-Chloro-3-methylphenol ND ug/kg 1 08/03/11 16:59 59-50-707/29/11 13:04864
4-Chloroaniline ND ug/kg 1 08/03/11 16:59 106-47-807/29/11 13:042160
bis(2-Chloroethoxy)methane ND ug/kg 1 08/03/11 16:59 111-91-107/29/11 13:04432
bis(2-Chloroethyl) ether ND ug/kg 1 08/03/11 16:59 111-44-407/29/11 13:04432
bis(2-Chloroisopropyl) ether ND ug/kg 1 08/03/11 16:59 108-60-107/29/11 13:04432
2-Chloronaphthalene ND ug/kg 1 08/03/11 16:59 91-58-707/29/11 13:04432
2-Chlorophenol ND ug/kg 1 08/03/11 16:59 95-57-807/29/11 13:04432
4-Chlorophenylphenyl ether ND ug/kg 1 08/03/11 16:59 7005-72-307/29/11 13:04432
Chrysene ND ug/kg 1 08/03/11 16:59 218-01-907/29/11 13:04432
Dibenz(a,h)anthracene ND ug/kg 1 08/03/11 16:59 53-70-307/29/11 13:04432
Dibenzofuran ND ug/kg 1 08/03/11 16:59 132-64-907/29/11 13:04432
1,2-Dichlorobenzene ND ug/kg 1 08/03/11 16:59 95-50-107/29/11 13:04432
1,3-Dichlorobenzene ND ug/kg 1 08/03/11 16:59 541-73-107/29/11 13:04432
1,4-Dichlorobenzene ND ug/kg 1 08/03/11 16:59 106-46-707/29/11 13:04432
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 9 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-24 Lab ID:9299302002 Collected:07/28/11 09:45 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3,3'-Dichlorobenzidine ND ug/kg 1 08/03/11 16:59 91-94-107/29/11 13:042160
2,4-Dichlorophenol ND ug/kg 1 08/03/11 16:59 120-83-207/29/11 13:04432
Diethylphthalate ND ug/kg 1 08/03/11 16:59 84-66-207/29/11 13:04432
2,4-Dimethylphenol ND ug/kg 1 08/03/11 16:59 105-67-907/29/11 13:04432
Dimethylphthalate ND ug/kg 1 08/03/11 16:59 131-11-307/29/11 13:04432
Di-n-butylphthalate ND ug/kg 1 08/03/11 16:59 84-74-207/29/11 13:04432
4,6-Dinitro-2-methylphenol ND ug/kg 1 08/03/11 16:59 534-52-107/29/11 13:04864
2,4-Dinitrophenol ND ug/kg 1 08/03/11 16:59 51-28-507/29/11 13:042160
2,4-Dinitrotoluene ND ug/kg 1 08/03/11 16:59 121-14-207/29/11 13:04432
2,6-Dinitrotoluene ND ug/kg 1 08/03/11 16:59 606-20-207/29/11 13:04432
Di-n-octylphthalate ND ug/kg 1 08/03/11 16:59 117-84-007/29/11 13:04432
bis(2-Ethylhexyl)phthalate ND ug/kg 1 08/03/11 16:59 117-81-707/29/11 13:04432
Fluoranthene ND ug/kg 1 08/03/11 16:59 206-44-007/29/11 13:04432
Fluorene ND ug/kg 1 08/03/11 16:59 86-73-707/29/11 13:04432
Hexachloro-1,3-butadiene ND ug/kg 1 08/03/11 16:59 87-68-307/29/11 13:04432
Hexachlorobenzene ND ug/kg 1 08/03/11 16:59 118-74-107/29/11 13:04432
Hexachlorocyclopentadiene ND ug/kg 1 08/03/11 16:59 77-47-407/29/11 13:04432
Hexachloroethane ND ug/kg 1 08/03/11 16:59 67-72-107/29/11 13:04432
Indeno(1,2,3-cd)pyrene ND ug/kg 1 08/03/11 16:59 193-39-507/29/11 13:04432
Isophorone ND ug/kg 1 08/03/11 16:59 78-59-107/29/11 13:04432
1-Methylnaphthalene ND ug/kg 1 08/03/11 16:59 90-12-007/29/11 13:04432
2-Methylnaphthalene ND ug/kg 1 08/03/11 16:59 91-57-607/29/11 13:04432
2-Methylphenol(o-Cresol)ND ug/kg 1 08/03/11 16:59 95-48-707/29/11 13:04432
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 08/03/11 16:5907/29/11 13:04432
Naphthalene ND ug/kg 1 08/03/11 16:59 91-20-307/29/11 13:04432
2-Nitroaniline ND ug/kg 1 08/03/11 16:59 88-74-407/29/11 13:042160
3-Nitroaniline ND ug/kg 1 08/03/11 16:59 99-09-207/29/11 13:042160
4-Nitroaniline ND ug/kg 1 08/03/11 16:59 100-01-607/29/11 13:04864
Nitrobenzene ND ug/kg 1 08/03/11 16:59 98-95-307/29/11 13:04432
2-Nitrophenol ND ug/kg 1 08/03/11 16:59 88-75-507/29/11 13:04432
4-Nitrophenol ND ug/kg 1 08/03/11 16:59 100-02-707/29/11 13:042160
N-Nitrosodimethylamine ND ug/kg 1 08/03/11 16:59 62-75-907/29/11 13:04432
N-Nitroso-di-n-propylamine ND ug/kg 1 08/03/11 16:59 621-64-707/29/11 13:04432
N-Nitrosodiphenylamine ND ug/kg 1 08/03/11 16:59 86-30-607/29/11 13:04432
Pentachlorophenol ND ug/kg 1 08/03/11 16:59 87-86-507/29/11 13:042160
Phenanthrene ND ug/kg 1 08/03/11 16:59 85-01-807/29/11 13:04432
Phenol ND ug/kg 1 08/03/11 16:59 108-95-207/29/11 13:04432
Pyrene ND ug/kg 1 08/03/11 16:59 129-00-007/29/11 13:04432
1,2,4-Trichlorobenzene ND ug/kg 1 08/03/11 16:59 120-82-107/29/11 13:04432
2,4,5-Trichlorophenol ND ug/kg 1 08/03/11 16:59 95-95-407/29/11 13:04432
2,4,6-Trichlorophenol ND ug/kg 1 08/03/11 16:59 88-06-207/29/11 13:04432
Nitrobenzene-d5 (S)45 %1 08/03/11 16:59 4165-60-007/29/11 13:0423-110
2-Fluorobiphenyl (S)40 %1 08/03/11 16:59 321-60-807/29/11 13:0430-110
Terphenyl-d14 (S)44 %1 08/03/11 16:59 1718-51-007/29/11 13:0428-110
Phenol-d6 (S)46 %1 08/03/11 16:59 13127-88-307/29/11 13:0422-110
2-Fluorophenol (S)45 %1 08/03/11 16:59 367-12-407/29/11 13:0413-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 10 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-24 Lab ID:9299302002 Collected:07/28/11 09:45 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4,6-Tribromophenol (S)38 %1 08/03/11 16:59 118-79-607/29/11 13:0427-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/30/11 04:47 67-64-197.7
Benzene ND ug/kg 1 07/30/11 04:47 71-43-24.9
Bromobenzene ND ug/kg 1 07/30/11 04:47 108-86-14.9
Bromochloromethane ND ug/kg 1 07/30/11 04:47 74-97-54.9
Bromodichloromethane ND ug/kg 1 07/30/11 04:47 75-27-44.9
Bromoform ND ug/kg 1 07/30/11 04:47 75-25-24.9
Bromomethane ND ug/kg 1 07/30/11 04:47 74-83-99.8
2-Butanone (MEK)ND ug/kg 1 07/30/11 04:47 78-93-397.7
n-Butylbenzene ND ug/kg 1 07/30/11 04:47 104-51-84.9
sec-Butylbenzene ND ug/kg 1 07/30/11 04:47 135-98-84.9
tert-Butylbenzene ND ug/kg 1 07/30/11 04:47 98-06-64.9
Carbon tetrachloride ND ug/kg 1 07/30/11 04:47 56-23-54.9
Chlorobenzene ND ug/kg 1 07/30/11 04:47 108-90-74.9
Chloroethane ND ug/kg 1 07/30/11 04:47 75-00-39.8
Chloroform ND ug/kg 1 07/30/11 04:47 67-66-34.9
Chloromethane ND ug/kg 1 07/30/11 04:47 74-87-39.8
2-Chlorotoluene ND ug/kg 1 07/30/11 04:47 95-49-84.9
4-Chlorotoluene ND ug/kg 1 07/30/11 04:47 106-43-44.9
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/30/11 04:47 96-12-84.9
Dibromochloromethane ND ug/kg 1 07/30/11 04:47 124-48-14.9
1,2-Dibromoethane (EDB)ND ug/kg 1 07/30/11 04:47 106-93-44.9
Dibromomethane ND ug/kg 1 07/30/11 04:47 74-95-34.9
1,2-Dichlorobenzene ND ug/kg 1 07/30/11 04:47 95-50-14.9
1,3-Dichlorobenzene ND ug/kg 1 07/30/11 04:47 541-73-14.9
1,4-Dichlorobenzene ND ug/kg 1 07/30/11 04:47 106-46-74.9
Dichlorodifluoromethane ND ug/kg 1 07/30/11 04:47 75-71-89.8
1,1-Dichloroethane ND ug/kg 1 07/30/11 04:47 75-34-34.9
1,2-Dichloroethane ND ug/kg 1 07/30/11 04:47 107-06-24.9
1,1-Dichloroethene ND ug/kg 1 07/30/11 04:47 75-35-44.9
cis-1,2-Dichloroethene ND ug/kg 1 07/30/11 04:47 156-59-24.9
trans-1,2-Dichloroethene ND ug/kg 1 07/30/11 04:47 156-60-54.9
1,2-Dichloropropane ND ug/kg 1 07/30/11 04:47 78-87-54.9
1,3-Dichloropropane ND ug/kg 1 07/30/11 04:47 142-28-94.9
2,2-Dichloropropane ND ug/kg 1 07/30/11 04:47 594-20-74.9
1,1-Dichloropropene ND ug/kg 1 07/30/11 04:47 563-58-64.9
cis-1,3-Dichloropropene ND ug/kg 1 07/30/11 04:47 10061-01-54.9
trans-1,3-Dichloropropene ND ug/kg 1 07/30/11 04:47 10061-02-64.9
Diisopropyl ether ND ug/kg 1 07/30/11 04:47 108-20-34.9
Ethylbenzene ND ug/kg 1 07/30/11 04:47 100-41-44.9
Hexachloro-1,3-butadiene ND ug/kg 1 07/30/11 04:47 87-68-34.9
2-Hexanone ND ug/kg 1 07/30/11 04:47 591-78-648.9
Isopropylbenzene (Cumene)ND ug/kg 1 07/30/11 04:47 98-82-84.9
p-Isopropyltoluene ND ug/kg 1 07/30/11 04:47 99-87-64.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 11 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-24 Lab ID:9299302002 Collected:07/28/11 09:45 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Methylene Chloride ND ug/kg 1 07/30/11 04:47 75-09-219.5
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/30/11 04:47 108-10-148.9
Methyl-tert-butyl ether ND ug/kg 1 07/30/11 04:47 1634-04-44.9
Naphthalene ND ug/kg 1 07/30/11 04:47 91-20-34.9
n-Propylbenzene ND ug/kg 1 07/30/11 04:47 103-65-14.9
Styrene ND ug/kg 1 07/30/11 04:47 100-42-54.9
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/30/11 04:47 630-20-64.9
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/30/11 04:47 79-34-54.9
Tetrachloroethene ND ug/kg 1 07/30/11 04:47 127-18-44.9
Toluene ND ug/kg 1 07/30/11 04:47 108-88-34.9
1,2,3-Trichlorobenzene ND ug/kg 1 07/30/11 04:47 87-61-64.9
1,2,4-Trichlorobenzene ND ug/kg 1 07/30/11 04:47 120-82-14.9
1,1,1-Trichloroethane ND ug/kg 1 07/30/11 04:47 71-55-64.9
1,1,2-Trichloroethane ND ug/kg 1 07/30/11 04:47 79-00-54.9
Trichloroethene ND ug/kg 1 07/30/11 04:47 79-01-64.9
Trichlorofluoromethane ND ug/kg 1 07/30/11 04:47 75-69-44.9
1,2,3-Trichloropropane ND ug/kg 1 07/30/11 04:47 96-18-44.9
1,2,4-Trimethylbenzene ND ug/kg 1 07/30/11 04:47 95-63-64.9
1,3,5-Trimethylbenzene ND ug/kg 1 07/30/11 04:47 108-67-84.9
Vinyl acetate ND ug/kg 1 07/30/11 04:47 108-05-448.9
Vinyl chloride ND ug/kg 1 07/30/11 04:47 75-01-49.8
Xylene (Total)ND ug/kg 1 07/30/11 04:47 1330-20-79.8
m&p-Xylene ND ug/kg 1 07/30/11 04:47 179601-23-19.8
o-Xylene ND ug/kg 1 07/30/11 04:47 95-47-64.9
Dibromofluoromethane (S)98 %1 07/30/11 04:47 1868-53-770-130
Toluene-d8 (S)105 %1 07/30/11 04:47 2037-26-570-130
4-Bromofluorobenzene (S)92 %1 07/30/11 04:47 460-00-470-130
1,2-Dichloroethane-d4 (S)93 %1 07/30/11 04:47 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 23.6 %1 08/01/11 09:040.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 8.4 mg/kg 1 08/05/11 16:42 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/04/11 13:23 18540-29-9 N208/04/11 10:432.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 12 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-25 Lab ID:9299302003 Collected:07/28/11 14:15 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 08/02/11 16:07 7440-36-008/02/11 09:000.65
Arsenic ND mg/kg 1 08/03/11 17:27 7440-38-208/02/11 09:000.65
Beryllium ND mg/kg 1 08/02/11 16:07 7440-41-708/02/11 09:000.13
Cadmium 0.44 mg/kg 1 08/02/11 16:07 7440-43-908/02/11 09:000.13
Chromium 17.7 mg/kg 1 08/02/11 16:07 7440-47-308/02/11 09:000.65
Copper 19.4 mg/kg 1 08/02/11 16:07 7440-50-808/02/11 09:000.65
Lead 4.8 mg/kg 1 08/02/11 16:07 7439-92-108/02/11 09:000.65
Manganese 11.8 mg/kg 1 08/02/11 16:07 7439-96-508/02/11 09:000.65
Nickel 1.1 mg/kg 1 08/02/11 16:07 7440-02-008/02/11 09:000.65
Selenium ND mg/kg 1 08/02/11 16:07 7782-49-208/02/11 09:001.3
Silver ND mg/kg 1 08/02/11 16:07 7440-22-408/02/11 09:000.65
Thallium ND mg/kg 1 08/02/11 16:07 7440-28-008/02/11 09:001.3
Zinc 6.5 mg/kg 1 08/02/11 16:07 7440-66-608/02/11 09:001.3
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.096 mg/kg 1 08/03/11 12:38 7439-97-608/01/11 14:150.0052
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 08/03/11 17:27 83-32-907/29/11 13:04455
Acenaphthylene ND ug/kg 1 08/03/11 17:27 208-96-807/29/11 13:04455
Aniline ND ug/kg 1 08/03/11 17:27 62-53-307/29/11 13:04455
Anthracene ND ug/kg 1 08/03/11 17:27 120-12-707/29/11 13:04455
Benzo(a)anthracene ND ug/kg 1 08/03/11 17:27 56-55-307/29/11 13:04455
Benzo(a)pyrene ND ug/kg 1 08/03/11 17:27 50-32-807/29/11 13:04455
Benzo(b)fluoranthene ND ug/kg 1 08/03/11 17:27 205-99-207/29/11 13:04455
Benzo(g,h,i)perylene ND ug/kg 1 08/03/11 17:27 191-24-207/29/11 13:04455
Benzo(k)fluoranthene ND ug/kg 1 08/03/11 17:27 207-08-907/29/11 13:04455
Benzoic Acid ND ug/kg 1 08/03/11 17:27 65-85-007/29/11 13:042270
Benzyl alcohol ND ug/kg 1 08/03/11 17:27 100-51-607/29/11 13:04910
4-Bromophenylphenyl ether ND ug/kg 1 08/03/11 17:27 101-55-307/29/11 13:04455
Butylbenzylphthalate ND ug/kg 1 08/03/11 17:27 85-68-707/29/11 13:04455
4-Chloro-3-methylphenol ND ug/kg 1 08/03/11 17:27 59-50-707/29/11 13:04910
4-Chloroaniline ND ug/kg 1 08/03/11 17:27 106-47-807/29/11 13:042270
bis(2-Chloroethoxy)methane ND ug/kg 1 08/03/11 17:27 111-91-107/29/11 13:04455
bis(2-Chloroethyl) ether ND ug/kg 1 08/03/11 17:27 111-44-407/29/11 13:04455
bis(2-Chloroisopropyl) ether ND ug/kg 1 08/03/11 17:27 108-60-107/29/11 13:04455
2-Chloronaphthalene ND ug/kg 1 08/03/11 17:27 91-58-707/29/11 13:04455
2-Chlorophenol ND ug/kg 1 08/03/11 17:27 95-57-807/29/11 13:04455
4-Chlorophenylphenyl ether ND ug/kg 1 08/03/11 17:27 7005-72-307/29/11 13:04455
Chrysene ND ug/kg 1 08/03/11 17:27 218-01-907/29/11 13:04455
Dibenz(a,h)anthracene ND ug/kg 1 08/03/11 17:27 53-70-307/29/11 13:04455
Dibenzofuran ND ug/kg 1 08/03/11 17:27 132-64-907/29/11 13:04455
1,2-Dichlorobenzene ND ug/kg 1 08/03/11 17:27 95-50-107/29/11 13:04455
1,3-Dichlorobenzene ND ug/kg 1 08/03/11 17:27 541-73-107/29/11 13:04455
1,4-Dichlorobenzene ND ug/kg 1 08/03/11 17:27 106-46-707/29/11 13:04455
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 13 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-25 Lab ID:9299302003 Collected:07/28/11 14:15 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3,3'-Dichlorobenzidine ND ug/kg 1 08/03/11 17:27 91-94-107/29/11 13:042270
2,4-Dichlorophenol ND ug/kg 1 08/03/11 17:27 120-83-207/29/11 13:04455
Diethylphthalate ND ug/kg 1 08/03/11 17:27 84-66-207/29/11 13:04455
2,4-Dimethylphenol ND ug/kg 1 08/03/11 17:27 105-67-907/29/11 13:04455
Dimethylphthalate ND ug/kg 1 08/03/11 17:27 131-11-307/29/11 13:04455
Di-n-butylphthalate ND ug/kg 1 08/03/11 17:27 84-74-207/29/11 13:04455
4,6-Dinitro-2-methylphenol ND ug/kg 1 08/03/11 17:27 534-52-107/29/11 13:04910
2,4-Dinitrophenol ND ug/kg 1 08/03/11 17:27 51-28-507/29/11 13:042270
2,4-Dinitrotoluene ND ug/kg 1 08/03/11 17:27 121-14-207/29/11 13:04455
2,6-Dinitrotoluene ND ug/kg 1 08/03/11 17:27 606-20-207/29/11 13:04455
Di-n-octylphthalate ND ug/kg 1 08/03/11 17:27 117-84-007/29/11 13:04455
bis(2-Ethylhexyl)phthalate ND ug/kg 1 08/03/11 17:27 117-81-707/29/11 13:04455
Fluoranthene ND ug/kg 1 08/03/11 17:27 206-44-007/29/11 13:04455
Fluorene ND ug/kg 1 08/03/11 17:27 86-73-707/29/11 13:04455
Hexachloro-1,3-butadiene ND ug/kg 1 08/03/11 17:27 87-68-307/29/11 13:04455
Hexachlorobenzene ND ug/kg 1 08/03/11 17:27 118-74-107/29/11 13:04455
Hexachlorocyclopentadiene ND ug/kg 1 08/03/11 17:27 77-47-407/29/11 13:04455
Hexachloroethane ND ug/kg 1 08/03/11 17:27 67-72-107/29/11 13:04455
Indeno(1,2,3-cd)pyrene ND ug/kg 1 08/03/11 17:27 193-39-507/29/11 13:04455
Isophorone ND ug/kg 1 08/03/11 17:27 78-59-107/29/11 13:04455
1-Methylnaphthalene ND ug/kg 1 08/03/11 17:27 90-12-007/29/11 13:04455
2-Methylnaphthalene ND ug/kg 1 08/03/11 17:27 91-57-607/29/11 13:04455
2-Methylphenol(o-Cresol)ND ug/kg 1 08/03/11 17:27 95-48-707/29/11 13:04455
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 08/03/11 17:2707/29/11 13:04455
Naphthalene ND ug/kg 1 08/03/11 17:27 91-20-307/29/11 13:04455
2-Nitroaniline ND ug/kg 1 08/03/11 17:27 88-74-407/29/11 13:042270
3-Nitroaniline ND ug/kg 1 08/03/11 17:27 99-09-207/29/11 13:042270
4-Nitroaniline ND ug/kg 1 08/03/11 17:27 100-01-607/29/11 13:04910
Nitrobenzene ND ug/kg 1 08/03/11 17:27 98-95-307/29/11 13:04455
2-Nitrophenol ND ug/kg 1 08/03/11 17:27 88-75-507/29/11 13:04455
4-Nitrophenol ND ug/kg 1 08/03/11 17:27 100-02-707/29/11 13:042270
N-Nitrosodimethylamine ND ug/kg 1 08/03/11 17:27 62-75-907/29/11 13:04455
N-Nitroso-di-n-propylamine ND ug/kg 1 08/03/11 17:27 621-64-707/29/11 13:04455
N-Nitrosodiphenylamine ND ug/kg 1 08/03/11 17:27 86-30-607/29/11 13:04455
Pentachlorophenol ND ug/kg 1 08/03/11 17:27 87-86-507/29/11 13:042270
Phenanthrene ND ug/kg 1 08/03/11 17:27 85-01-807/29/11 13:04455
Phenol ND ug/kg 1 08/03/11 17:27 108-95-207/29/11 13:04455
Pyrene ND ug/kg 1 08/03/11 17:27 129-00-007/29/11 13:04455
1,2,4-Trichlorobenzene ND ug/kg 1 08/03/11 17:27 120-82-107/29/11 13:04455
2,4,5-Trichlorophenol ND ug/kg 1 08/03/11 17:27 95-95-407/29/11 13:04455
2,4,6-Trichlorophenol ND ug/kg 1 08/03/11 17:27 88-06-207/29/11 13:04455
Nitrobenzene-d5 (S)51 %1 08/03/11 17:27 4165-60-007/29/11 13:0423-110
2-Fluorobiphenyl (S)48 %1 08/03/11 17:27 321-60-807/29/11 13:0430-110
Terphenyl-d14 (S)58 %1 08/03/11 17:27 1718-51-007/29/11 13:0428-110
Phenol-d6 (S)52 %1 08/03/11 17:27 13127-88-307/29/11 13:0422-110
2-Fluorophenol (S)50 %1 08/03/11 17:27 367-12-407/29/11 13:0413-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 14 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-25 Lab ID:9299302003 Collected:07/28/11 14:15 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4,6-Tribromophenol (S)46 %1 08/03/11 17:27 118-79-607/29/11 13:0427-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/30/11 05:07 67-64-196.0
Benzene ND ug/kg 1 07/30/11 05:07 71-43-24.8
Bromobenzene ND ug/kg 1 07/30/11 05:07 108-86-14.8
Bromochloromethane ND ug/kg 1 07/30/11 05:07 74-97-54.8
Bromodichloromethane ND ug/kg 1 07/30/11 05:07 75-27-44.8
Bromoform ND ug/kg 1 07/30/11 05:07 75-25-24.8
Bromomethane ND ug/kg 1 07/30/11 05:07 74-83-99.6
2-Butanone (MEK)ND ug/kg 1 07/30/11 05:07 78-93-396.0
n-Butylbenzene ND ug/kg 1 07/30/11 05:07 104-51-84.8
sec-Butylbenzene ND ug/kg 1 07/30/11 05:07 135-98-84.8
tert-Butylbenzene ND ug/kg 1 07/30/11 05:07 98-06-64.8
Carbon tetrachloride ND ug/kg 1 07/30/11 05:07 56-23-54.8
Chlorobenzene ND ug/kg 1 07/30/11 05:07 108-90-74.8
Chloroethane ND ug/kg 1 07/30/11 05:07 75-00-39.6
Chloroform ND ug/kg 1 07/30/11 05:07 67-66-34.8
Chloromethane ND ug/kg 1 07/30/11 05:07 74-87-39.6
2-Chlorotoluene ND ug/kg 1 07/30/11 05:07 95-49-84.8
4-Chlorotoluene ND ug/kg 1 07/30/11 05:07 106-43-44.8
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/30/11 05:07 96-12-84.8
Dibromochloromethane ND ug/kg 1 07/30/11 05:07 124-48-14.8
1,2-Dibromoethane (EDB)ND ug/kg 1 07/30/11 05:07 106-93-44.8
Dibromomethane ND ug/kg 1 07/30/11 05:07 74-95-34.8
1,2-Dichlorobenzene ND ug/kg 1 07/30/11 05:07 95-50-14.8
1,3-Dichlorobenzene ND ug/kg 1 07/30/11 05:07 541-73-14.8
1,4-Dichlorobenzene ND ug/kg 1 07/30/11 05:07 106-46-74.8
Dichlorodifluoromethane ND ug/kg 1 07/30/11 05:07 75-71-89.6
1,1-Dichloroethane ND ug/kg 1 07/30/11 05:07 75-34-34.8
1,2-Dichloroethane ND ug/kg 1 07/30/11 05:07 107-06-24.8
1,1-Dichloroethene ND ug/kg 1 07/30/11 05:07 75-35-44.8
cis-1,2-Dichloroethene ND ug/kg 1 07/30/11 05:07 156-59-24.8
trans-1,2-Dichloroethene ND ug/kg 1 07/30/11 05:07 156-60-54.8
1,2-Dichloropropane ND ug/kg 1 07/30/11 05:07 78-87-54.8
1,3-Dichloropropane ND ug/kg 1 07/30/11 05:07 142-28-94.8
2,2-Dichloropropane ND ug/kg 1 07/30/11 05:07 594-20-74.8
1,1-Dichloropropene ND ug/kg 1 07/30/11 05:07 563-58-64.8
cis-1,3-Dichloropropene ND ug/kg 1 07/30/11 05:07 10061-01-54.8
trans-1,3-Dichloropropene ND ug/kg 1 07/30/11 05:07 10061-02-64.8
Diisopropyl ether ND ug/kg 1 07/30/11 05:07 108-20-34.8
Ethylbenzene ND ug/kg 1 07/30/11 05:07 100-41-44.8
Hexachloro-1,3-butadiene ND ug/kg 1 07/30/11 05:07 87-68-34.8
2-Hexanone ND ug/kg 1 07/30/11 05:07 591-78-648.0
Isopropylbenzene (Cumene)ND ug/kg 1 07/30/11 05:07 98-82-84.8
p-Isopropyltoluene ND ug/kg 1 07/30/11 05:07 99-87-64.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 15 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-25 Lab ID:9299302003 Collected:07/28/11 14:15 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Methylene Chloride ND ug/kg 1 07/30/11 05:07 75-09-219.2
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/30/11 05:07 108-10-148.0
Methyl-tert-butyl ether ND ug/kg 1 07/30/11 05:07 1634-04-44.8
Naphthalene ND ug/kg 1 07/30/11 05:07 91-20-34.8
n-Propylbenzene ND ug/kg 1 07/30/11 05:07 103-65-14.8
Styrene ND ug/kg 1 07/30/11 05:07 100-42-54.8
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/30/11 05:07 630-20-64.8
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/30/11 05:07 79-34-54.8
Tetrachloroethene ND ug/kg 1 07/30/11 05:07 127-18-44.8
Toluene ND ug/kg 1 07/30/11 05:07 108-88-34.8
1,2,3-Trichlorobenzene ND ug/kg 1 07/30/11 05:07 87-61-64.8
1,2,4-Trichlorobenzene ND ug/kg 1 07/30/11 05:07 120-82-14.8
1,1,1-Trichloroethane ND ug/kg 1 07/30/11 05:07 71-55-64.8
1,1,2-Trichloroethane ND ug/kg 1 07/30/11 05:07 79-00-54.8
Trichloroethene ND ug/kg 1 07/30/11 05:07 79-01-64.8
Trichlorofluoromethane ND ug/kg 1 07/30/11 05:07 75-69-44.8
1,2,3-Trichloropropane ND ug/kg 1 07/30/11 05:07 96-18-44.8
1,2,4-Trimethylbenzene ND ug/kg 1 07/30/11 05:07 95-63-64.8
1,3,5-Trimethylbenzene ND ug/kg 1 07/30/11 05:07 108-67-84.8
Vinyl acetate ND ug/kg 1 07/30/11 05:07 108-05-448.0
Vinyl chloride ND ug/kg 1 07/30/11 05:07 75-01-49.6
Xylene (Total)ND ug/kg 1 07/30/11 05:07 1330-20-79.6
m&p-Xylene ND ug/kg 1 07/30/11 05:07 179601-23-19.6
o-Xylene ND ug/kg 1 07/30/11 05:07 95-47-64.8
Dibromofluoromethane (S)103 %1 07/30/11 05:07 1868-53-770-130
Toluene-d8 (S)103 %1 07/30/11 05:07 2037-26-570-130
4-Bromofluorobenzene (S)95 %1 07/30/11 05:07 460-00-470-130
1,2-Dichloroethane-d4 (S)97 %1 07/30/11 05:07 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 27.5 %1 08/01/11 09:040.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 17.7 mg/kg 1 08/05/11 16:46 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/04/11 13:23 18540-29-9 N208/04/11 10:432.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 16 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-26 Lab ID:9299302004 Collected:07/28/11 10:45 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 08/02/11 16:11 7440-36-008/02/11 09:000.48
Arsenic ND mg/kg 1 08/03/11 17:31 7440-38-208/02/11 09:000.48
Beryllium 0.42 mg/kg 1 08/02/11 16:11 7440-41-708/02/11 09:000.096
Cadmium 5.5 mg/kg 1 08/02/11 16:11 7440-43-908/02/11 09:000.096
Chromium 18.5 mg/kg 1 08/02/11 16:11 7440-47-308/02/11 09:000.48
Copper 13.4 mg/kg 1 08/02/11 16:11 7440-50-808/02/11 09:000.48
Lead 14.0 mg/kg 1 08/02/11 16:11 7439-92-108/02/11 09:000.48
Manganese 20.8 mg/kg 1 08/02/11 16:11 7439-96-508/02/11 09:000.48
Nickel 3.6 mg/kg 1 08/02/11 16:11 7440-02-008/02/11 09:000.48
Selenium 1.9 mg/kg 1 08/02/11 16:11 7782-49-208/02/11 09:000.96
Silver ND mg/kg 1 08/02/11 16:11 7440-22-408/02/11 09:000.48
Thallium ND mg/kg 1 08/02/11 16:11 7440-28-008/02/11 09:000.96
Zinc 420 mg/kg 1 08/02/11 16:11 7440-66-608/02/11 09:000.96
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.033 mg/kg 1 08/03/11 12:46 7439-97-608/01/11 14:150.0055
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 08/03/11 17:54 83-32-907/29/11 13:04398
Acenaphthylene ND ug/kg 1 08/03/11 17:54 208-96-807/29/11 13:04398
Aniline ND ug/kg 1 08/03/11 17:54 62-53-307/29/11 13:04398
Anthracene ND ug/kg 1 08/03/11 17:54 120-12-707/29/11 13:04398
Benzo(a)anthracene ND ug/kg 1 08/03/11 17:54 56-55-307/29/11 13:04398
Benzo(a)pyrene ND ug/kg 1 08/03/11 17:54 50-32-807/29/11 13:04398
Benzo(b)fluoranthene ND ug/kg 1 08/03/11 17:54 205-99-207/29/11 13:04398
Benzo(g,h,i)perylene ND ug/kg 1 08/03/11 17:54 191-24-207/29/11 13:04398
Benzo(k)fluoranthene ND ug/kg 1 08/03/11 17:54 207-08-907/29/11 13:04398
Benzoic Acid ND ug/kg 1 08/03/11 17:54 65-85-007/29/11 13:041990
Benzyl alcohol ND ug/kg 1 08/03/11 17:54 100-51-607/29/11 13:04796
4-Bromophenylphenyl ether ND ug/kg 1 08/03/11 17:54 101-55-307/29/11 13:04398
Butylbenzylphthalate ND ug/kg 1 08/03/11 17:54 85-68-707/29/11 13:04398
4-Chloro-3-methylphenol ND ug/kg 1 08/03/11 17:54 59-50-707/29/11 13:04796
4-Chloroaniline ND ug/kg 1 08/03/11 17:54 106-47-807/29/11 13:041990
bis(2-Chloroethoxy)methane ND ug/kg 1 08/03/11 17:54 111-91-107/29/11 13:04398
bis(2-Chloroethyl) ether ND ug/kg 1 08/03/11 17:54 111-44-407/29/11 13:04398
bis(2-Chloroisopropyl) ether ND ug/kg 1 08/03/11 17:54 108-60-107/29/11 13:04398
2-Chloronaphthalene ND ug/kg 1 08/03/11 17:54 91-58-707/29/11 13:04398
2-Chlorophenol ND ug/kg 1 08/03/11 17:54 95-57-807/29/11 13:04398
4-Chlorophenylphenyl ether ND ug/kg 1 08/03/11 17:54 7005-72-307/29/11 13:04398
Chrysene ND ug/kg 1 08/03/11 17:54 218-01-907/29/11 13:04398
Dibenz(a,h)anthracene ND ug/kg 1 08/03/11 17:54 53-70-307/29/11 13:04398
Dibenzofuran ND ug/kg 1 08/03/11 17:54 132-64-907/29/11 13:04398
1,2-Dichlorobenzene ND ug/kg 1 08/03/11 17:54 95-50-107/29/11 13:04398
1,3-Dichlorobenzene ND ug/kg 1 08/03/11 17:54 541-73-107/29/11 13:04398
1,4-Dichlorobenzene ND ug/kg 1 08/03/11 17:54 106-46-707/29/11 13:04398
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 17 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-26 Lab ID:9299302004 Collected:07/28/11 10:45 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3,3'-Dichlorobenzidine ND ug/kg 1 08/03/11 17:54 91-94-107/29/11 13:041990
2,4-Dichlorophenol ND ug/kg 1 08/03/11 17:54 120-83-207/29/11 13:04398
Diethylphthalate ND ug/kg 1 08/03/11 17:54 84-66-207/29/11 13:04398
2,4-Dimethylphenol ND ug/kg 1 08/03/11 17:54 105-67-907/29/11 13:04398
Dimethylphthalate ND ug/kg 1 08/03/11 17:54 131-11-307/29/11 13:04398
Di-n-butylphthalate ND ug/kg 1 08/03/11 17:54 84-74-207/29/11 13:04398
4,6-Dinitro-2-methylphenol ND ug/kg 1 08/03/11 17:54 534-52-107/29/11 13:04796
2,4-Dinitrophenol ND ug/kg 1 08/03/11 17:54 51-28-507/29/11 13:041990
2,4-Dinitrotoluene ND ug/kg 1 08/03/11 17:54 121-14-207/29/11 13:04398
2,6-Dinitrotoluene ND ug/kg 1 08/03/11 17:54 606-20-207/29/11 13:04398
Di-n-octylphthalate ND ug/kg 1 08/03/11 17:54 117-84-007/29/11 13:04398
bis(2-Ethylhexyl)phthalate ND ug/kg 1 08/03/11 17:54 117-81-707/29/11 13:04398
Fluoranthene ND ug/kg 1 08/03/11 17:54 206-44-007/29/11 13:04398
Fluorene ND ug/kg 1 08/03/11 17:54 86-73-707/29/11 13:04398
Hexachloro-1,3-butadiene ND ug/kg 1 08/03/11 17:54 87-68-307/29/11 13:04398
Hexachlorobenzene ND ug/kg 1 08/03/11 17:54 118-74-107/29/11 13:04398
Hexachlorocyclopentadiene ND ug/kg 1 08/03/11 17:54 77-47-407/29/11 13:04398
Hexachloroethane ND ug/kg 1 08/03/11 17:54 67-72-107/29/11 13:04398
Indeno(1,2,3-cd)pyrene ND ug/kg 1 08/03/11 17:54 193-39-507/29/11 13:04398
Isophorone ND ug/kg 1 08/03/11 17:54 78-59-107/29/11 13:04398
1-Methylnaphthalene ND ug/kg 1 08/03/11 17:54 90-12-007/29/11 13:04398
2-Methylnaphthalene ND ug/kg 1 08/03/11 17:54 91-57-607/29/11 13:04398
2-Methylphenol(o-Cresol)ND ug/kg 1 08/03/11 17:54 95-48-707/29/11 13:04398
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 08/03/11 17:5407/29/11 13:04398
Naphthalene ND ug/kg 1 08/03/11 17:54 91-20-307/29/11 13:04398
2-Nitroaniline ND ug/kg 1 08/03/11 17:54 88-74-407/29/11 13:041990
3-Nitroaniline ND ug/kg 1 08/03/11 17:54 99-09-207/29/11 13:041990
4-Nitroaniline ND ug/kg 1 08/03/11 17:54 100-01-607/29/11 13:04796
Nitrobenzene ND ug/kg 1 08/03/11 17:54 98-95-307/29/11 13:04398
2-Nitrophenol ND ug/kg 1 08/03/11 17:54 88-75-507/29/11 13:04398
4-Nitrophenol ND ug/kg 1 08/03/11 17:54 100-02-707/29/11 13:041990
N-Nitrosodimethylamine ND ug/kg 1 08/03/11 17:54 62-75-907/29/11 13:04398
N-Nitroso-di-n-propylamine ND ug/kg 1 08/03/11 17:54 621-64-707/29/11 13:04398
N-Nitrosodiphenylamine ND ug/kg 1 08/03/11 17:54 86-30-607/29/11 13:04398
Pentachlorophenol ND ug/kg 1 08/03/11 17:54 87-86-507/29/11 13:041990
Phenanthrene ND ug/kg 1 08/03/11 17:54 85-01-807/29/11 13:04398
Phenol ND ug/kg 1 08/03/11 17:54 108-95-207/29/11 13:04398
Pyrene ND ug/kg 1 08/03/11 17:54 129-00-007/29/11 13:04398
1,2,4-Trichlorobenzene ND ug/kg 1 08/03/11 17:54 120-82-107/29/11 13:04398
2,4,5-Trichlorophenol ND ug/kg 1 08/03/11 17:54 95-95-407/29/11 13:04398
2,4,6-Trichlorophenol ND ug/kg 1 08/03/11 17:54 88-06-207/29/11 13:04398
Nitrobenzene-d5 (S)59 %1 08/03/11 17:54 4165-60-007/29/11 13:0423-110
2-Fluorobiphenyl (S)56 %1 08/03/11 17:54 321-60-807/29/11 13:0430-110
Terphenyl-d14 (S)71 %1 08/03/11 17:54 1718-51-007/29/11 13:0428-110
Phenol-d6 (S)59 %1 08/03/11 17:54 13127-88-307/29/11 13:0422-110
2-Fluorophenol (S)55 %1 08/03/11 17:54 367-12-407/29/11 13:0413-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 18 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-26 Lab ID:9299302004 Collected:07/28/11 10:45 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4,6-Tribromophenol (S)56 %1 08/03/11 17:54 118-79-607/29/11 13:0427-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/30/11 05:27 67-64-184.7
Benzene ND ug/kg 1 07/30/11 05:27 71-43-24.2
Bromobenzene ND ug/kg 1 07/30/11 05:27 108-86-14.2
Bromochloromethane ND ug/kg 1 07/30/11 05:27 74-97-54.2
Bromodichloromethane ND ug/kg 1 07/30/11 05:27 75-27-44.2
Bromoform ND ug/kg 1 07/30/11 05:27 75-25-24.2
Bromomethane ND ug/kg 1 07/30/11 05:27 74-83-98.5
2-Butanone (MEK)ND ug/kg 1 07/30/11 05:27 78-93-384.7
n-Butylbenzene ND ug/kg 1 07/30/11 05:27 104-51-84.2
sec-Butylbenzene ND ug/kg 1 07/30/11 05:27 135-98-84.2
tert-Butylbenzene ND ug/kg 1 07/30/11 05:27 98-06-64.2
Carbon tetrachloride ND ug/kg 1 07/30/11 05:27 56-23-54.2
Chlorobenzene ND ug/kg 1 07/30/11 05:27 108-90-74.2
Chloroethane ND ug/kg 1 07/30/11 05:27 75-00-38.5
Chloroform ND ug/kg 1 07/30/11 05:27 67-66-34.2
Chloromethane ND ug/kg 1 07/30/11 05:27 74-87-38.5
2-Chlorotoluene ND ug/kg 1 07/30/11 05:27 95-49-84.2
4-Chlorotoluene ND ug/kg 1 07/30/11 05:27 106-43-44.2
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/30/11 05:27 96-12-84.2
Dibromochloromethane ND ug/kg 1 07/30/11 05:27 124-48-14.2
1,2-Dibromoethane (EDB)ND ug/kg 1 07/30/11 05:27 106-93-44.2
Dibromomethane ND ug/kg 1 07/30/11 05:27 74-95-34.2
1,2-Dichlorobenzene ND ug/kg 1 07/30/11 05:27 95-50-14.2
1,3-Dichlorobenzene ND ug/kg 1 07/30/11 05:27 541-73-14.2
1,4-Dichlorobenzene ND ug/kg 1 07/30/11 05:27 106-46-74.2
Dichlorodifluoromethane ND ug/kg 1 07/30/11 05:27 75-71-88.5
1,1-Dichloroethane ND ug/kg 1 07/30/11 05:27 75-34-34.2
1,2-Dichloroethane ND ug/kg 1 07/30/11 05:27 107-06-24.2
1,1-Dichloroethene ND ug/kg 1 07/30/11 05:27 75-35-44.2
cis-1,2-Dichloroethene ND ug/kg 1 07/30/11 05:27 156-59-24.2
trans-1,2-Dichloroethene ND ug/kg 1 07/30/11 05:27 156-60-54.2
1,2-Dichloropropane ND ug/kg 1 07/30/11 05:27 78-87-54.2
1,3-Dichloropropane ND ug/kg 1 07/30/11 05:27 142-28-94.2
2,2-Dichloropropane ND ug/kg 1 07/30/11 05:27 594-20-74.2
1,1-Dichloropropene ND ug/kg 1 07/30/11 05:27 563-58-64.2
cis-1,3-Dichloropropene ND ug/kg 1 07/30/11 05:27 10061-01-54.2
trans-1,3-Dichloropropene ND ug/kg 1 07/30/11 05:27 10061-02-64.2
Diisopropyl ether ND ug/kg 1 07/30/11 05:27 108-20-34.2
Ethylbenzene ND ug/kg 1 07/30/11 05:27 100-41-44.2
Hexachloro-1,3-butadiene ND ug/kg 1 07/30/11 05:27 87-68-34.2
2-Hexanone ND ug/kg 1 07/30/11 05:27 591-78-642.3
Isopropylbenzene (Cumene)ND ug/kg 1 07/30/11 05:27 98-82-84.2
p-Isopropyltoluene ND ug/kg 1 07/30/11 05:27 99-87-64.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 19 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-26 Lab ID:9299302004 Collected:07/28/11 10:45 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Methylene Chloride ND ug/kg 1 07/30/11 05:27 75-09-216.9
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/30/11 05:27 108-10-142.3
Methyl-tert-butyl ether ND ug/kg 1 07/30/11 05:27 1634-04-44.2
Naphthalene ND ug/kg 1 07/30/11 05:27 91-20-34.2
n-Propylbenzene ND ug/kg 1 07/30/11 05:27 103-65-14.2
Styrene ND ug/kg 1 07/30/11 05:27 100-42-54.2
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/30/11 05:27 630-20-64.2
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/30/11 05:27 79-34-54.2
Tetrachloroethene ND ug/kg 1 07/30/11 05:27 127-18-44.2
Toluene ND ug/kg 1 07/30/11 05:27 108-88-34.2
1,2,3-Trichlorobenzene ND ug/kg 1 07/30/11 05:27 87-61-64.2
1,2,4-Trichlorobenzene ND ug/kg 1 07/30/11 05:27 120-82-14.2
1,1,1-Trichloroethane ND ug/kg 1 07/30/11 05:27 71-55-64.2
1,1,2-Trichloroethane ND ug/kg 1 07/30/11 05:27 79-00-54.2
Trichloroethene ND ug/kg 1 07/30/11 05:27 79-01-64.2
Trichlorofluoromethane ND ug/kg 1 07/30/11 05:27 75-69-44.2
1,2,3-Trichloropropane ND ug/kg 1 07/30/11 05:27 96-18-44.2
1,2,4-Trimethylbenzene ND ug/kg 1 07/30/11 05:27 95-63-64.2
1,3,5-Trimethylbenzene ND ug/kg 1 07/30/11 05:27 108-67-84.2
Vinyl acetate ND ug/kg 1 07/30/11 05:27 108-05-442.3
Vinyl chloride ND ug/kg 1 07/30/11 05:27 75-01-48.5
Xylene (Total)ND ug/kg 1 07/30/11 05:27 1330-20-78.5
m&p-Xylene ND ug/kg 1 07/30/11 05:27 179601-23-18.5
o-Xylene ND ug/kg 1 07/30/11 05:27 95-47-64.2
Dibromofluoromethane (S)101 %1 07/30/11 05:27 1868-53-770-130
Toluene-d8 (S)105 %1 07/30/11 05:27 2037-26-570-130
4-Bromofluorobenzene (S)92 %1 07/30/11 05:27 460-00-470-130
1,2-Dichloroethane-d4 (S)95 %1 07/30/11 05:27 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 17.0 %1 08/01/11 09:040.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 18.5 mg/kg 1 08/05/11 16:42 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/04/11 13:23 18540-29-9 N208/04/11 10:432.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 20 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-27 Lab ID:9299302005 Collected:07/28/11 11:45 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 08/02/11 16:15 7440-36-008/02/11 09:000.51
Arsenic 1.3 mg/kg 1 08/03/11 17:36 7440-38-208/02/11 09:000.51
Beryllium 0.16 mg/kg 1 08/02/11 16:15 7440-41-708/02/11 09:000.10
Cadmium ND mg/kg 1 08/02/11 16:15 7440-43-908/02/11 09:000.10
Chromium 16.0 mg/kg 1 08/02/11 16:15 7440-47-308/02/11 09:000.51
Copper 31.5 mg/kg 1 08/02/11 16:15 7440-50-808/02/11 09:000.51
Lead 10.7 mg/kg 1 08/02/11 16:15 7439-92-108/02/11 09:000.51
Manganese 210 mg/kg 1 08/02/11 16:15 7439-96-508/02/11 09:000.51
Nickel 2.4 mg/kg 1 08/02/11 16:15 7440-02-008/02/11 09:000.51
Selenium ND mg/kg 1 08/02/11 16:15 7782-49-208/02/11 09:001.0
Silver ND mg/kg 1 08/02/11 16:15 7440-22-408/02/11 09:000.51
Thallium ND mg/kg 1 08/02/11 16:15 7440-28-008/02/11 09:001.0
Zinc 13.0 mg/kg 1 08/02/11 16:15 7440-66-608/02/11 09:001.0
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.038 mg/kg 1 08/03/11 12:49 7439-97-608/01/11 14:150.0050
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 08/03/11 18:22 83-32-907/29/11 13:04374
Acenaphthylene ND ug/kg 1 08/03/11 18:22 208-96-807/29/11 13:04374
Aniline ND ug/kg 1 08/03/11 18:22 62-53-307/29/11 13:04374
Anthracene ND ug/kg 1 08/03/11 18:22 120-12-707/29/11 13:04374
Benzo(a)anthracene ND ug/kg 1 08/03/11 18:22 56-55-307/29/11 13:04374
Benzo(a)pyrene ND ug/kg 1 08/03/11 18:22 50-32-807/29/11 13:04374
Benzo(b)fluoranthene ND ug/kg 1 08/03/11 18:22 205-99-207/29/11 13:04374
Benzo(g,h,i)perylene ND ug/kg 1 08/03/11 18:22 191-24-207/29/11 13:04374
Benzo(k)fluoranthene ND ug/kg 1 08/03/11 18:22 207-08-907/29/11 13:04374
Benzoic Acid ND ug/kg 1 08/03/11 18:22 65-85-007/29/11 13:041870
Benzyl alcohol ND ug/kg 1 08/03/11 18:22 100-51-607/29/11 13:04749
4-Bromophenylphenyl ether ND ug/kg 1 08/03/11 18:22 101-55-307/29/11 13:04374
Butylbenzylphthalate ND ug/kg 1 08/03/11 18:22 85-68-707/29/11 13:04374
4-Chloro-3-methylphenol ND ug/kg 1 08/03/11 18:22 59-50-707/29/11 13:04749
4-Chloroaniline ND ug/kg 1 08/03/11 18:22 106-47-807/29/11 13:041870
bis(2-Chloroethoxy)methane ND ug/kg 1 08/03/11 18:22 111-91-107/29/11 13:04374
bis(2-Chloroethyl) ether ND ug/kg 1 08/03/11 18:22 111-44-407/29/11 13:04374
bis(2-Chloroisopropyl) ether ND ug/kg 1 08/03/11 18:22 108-60-107/29/11 13:04374
2-Chloronaphthalene ND ug/kg 1 08/03/11 18:22 91-58-707/29/11 13:04374
2-Chlorophenol ND ug/kg 1 08/03/11 18:22 95-57-807/29/11 13:04374
4-Chlorophenylphenyl ether ND ug/kg 1 08/03/11 18:22 7005-72-307/29/11 13:04374
Chrysene ND ug/kg 1 08/03/11 18:22 218-01-907/29/11 13:04374
Dibenz(a,h)anthracene ND ug/kg 1 08/03/11 18:22 53-70-307/29/11 13:04374
Dibenzofuran ND ug/kg 1 08/03/11 18:22 132-64-907/29/11 13:04374
1,2-Dichlorobenzene ND ug/kg 1 08/03/11 18:22 95-50-107/29/11 13:04374
1,3-Dichlorobenzene ND ug/kg 1 08/03/11 18:22 541-73-107/29/11 13:04374
1,4-Dichlorobenzene ND ug/kg 1 08/03/11 18:22 106-46-707/29/11 13:04374
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 21 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-27 Lab ID:9299302005 Collected:07/28/11 11:45 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3,3'-Dichlorobenzidine ND ug/kg 1 08/03/11 18:22 91-94-107/29/11 13:041870
2,4-Dichlorophenol ND ug/kg 1 08/03/11 18:22 120-83-207/29/11 13:04374
Diethylphthalate ND ug/kg 1 08/03/11 18:22 84-66-207/29/11 13:04374
2,4-Dimethylphenol ND ug/kg 1 08/03/11 18:22 105-67-907/29/11 13:04374
Dimethylphthalate ND ug/kg 1 08/03/11 18:22 131-11-307/29/11 13:04374
Di-n-butylphthalate ND ug/kg 1 08/03/11 18:22 84-74-207/29/11 13:04374
4,6-Dinitro-2-methylphenol ND ug/kg 1 08/03/11 18:22 534-52-107/29/11 13:04749
2,4-Dinitrophenol ND ug/kg 1 08/03/11 18:22 51-28-507/29/11 13:041870
2,4-Dinitrotoluene ND ug/kg 1 08/03/11 18:22 121-14-207/29/11 13:04374
2,6-Dinitrotoluene ND ug/kg 1 08/03/11 18:22 606-20-207/29/11 13:04374
Di-n-octylphthalate ND ug/kg 1 08/03/11 18:22 117-84-007/29/11 13:04374
bis(2-Ethylhexyl)phthalate ND ug/kg 1 08/03/11 18:22 117-81-707/29/11 13:04374
Fluoranthene ND ug/kg 1 08/03/11 18:22 206-44-007/29/11 13:04374
Fluorene ND ug/kg 1 08/03/11 18:22 86-73-707/29/11 13:04374
Hexachloro-1,3-butadiene ND ug/kg 1 08/03/11 18:22 87-68-307/29/11 13:04374
Hexachlorobenzene ND ug/kg 1 08/03/11 18:22 118-74-107/29/11 13:04374
Hexachlorocyclopentadiene ND ug/kg 1 08/03/11 18:22 77-47-407/29/11 13:04374
Hexachloroethane ND ug/kg 1 08/03/11 18:22 67-72-107/29/11 13:04374
Indeno(1,2,3-cd)pyrene ND ug/kg 1 08/03/11 18:22 193-39-507/29/11 13:04374
Isophorone ND ug/kg 1 08/03/11 18:22 78-59-107/29/11 13:04374
1-Methylnaphthalene ND ug/kg 1 08/03/11 18:22 90-12-007/29/11 13:04374
2-Methylnaphthalene ND ug/kg 1 08/03/11 18:22 91-57-607/29/11 13:04374
2-Methylphenol(o-Cresol)ND ug/kg 1 08/03/11 18:22 95-48-707/29/11 13:04374
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 08/03/11 18:2207/29/11 13:04374
Naphthalene ND ug/kg 1 08/03/11 18:22 91-20-307/29/11 13:04374
2-Nitroaniline ND ug/kg 1 08/03/11 18:22 88-74-407/29/11 13:041870
3-Nitroaniline ND ug/kg 1 08/03/11 18:22 99-09-207/29/11 13:041870
4-Nitroaniline ND ug/kg 1 08/03/11 18:22 100-01-607/29/11 13:04749
Nitrobenzene ND ug/kg 1 08/03/11 18:22 98-95-307/29/11 13:04374
2-Nitrophenol ND ug/kg 1 08/03/11 18:22 88-75-507/29/11 13:04374
4-Nitrophenol ND ug/kg 1 08/03/11 18:22 100-02-707/29/11 13:041870
N-Nitrosodimethylamine ND ug/kg 1 08/03/11 18:22 62-75-907/29/11 13:04374
N-Nitroso-di-n-propylamine ND ug/kg 1 08/03/11 18:22 621-64-707/29/11 13:04374
N-Nitrosodiphenylamine ND ug/kg 1 08/03/11 18:22 86-30-607/29/11 13:04374
Pentachlorophenol ND ug/kg 1 08/03/11 18:22 87-86-507/29/11 13:041870
Phenanthrene ND ug/kg 1 08/03/11 18:22 85-01-807/29/11 13:04374
Phenol ND ug/kg 1 08/03/11 18:22 108-95-207/29/11 13:04374
Pyrene ND ug/kg 1 08/03/11 18:22 129-00-007/29/11 13:04374
1,2,4-Trichlorobenzene ND ug/kg 1 08/03/11 18:22 120-82-107/29/11 13:04374
2,4,5-Trichlorophenol ND ug/kg 1 08/03/11 18:22 95-95-407/29/11 13:04374
2,4,6-Trichlorophenol ND ug/kg 1 08/03/11 18:22 88-06-207/29/11 13:04374
Nitrobenzene-d5 (S)51 %1 08/03/11 18:22 4165-60-007/29/11 13:0423-110
2-Fluorobiphenyl (S)51 %1 08/03/11 18:22 321-60-807/29/11 13:0430-110
Terphenyl-d14 (S)64 %1 08/03/11 18:22 1718-51-007/29/11 13:0428-110
Phenol-d6 (S)51 %1 08/03/11 18:22 13127-88-307/29/11 13:0422-110
2-Fluorophenol (S)46 %1 08/03/11 18:22 367-12-407/29/11 13:0413-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 22 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-27 Lab ID:9299302005 Collected:07/28/11 11:45 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4,6-Tribromophenol (S)55 %1 08/03/11 18:22 118-79-607/29/11 13:0427-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/31/11 21:14 67-64-183.2
Benzene ND ug/kg 1 07/31/11 21:14 71-43-24.2
Bromobenzene ND ug/kg 1 07/31/11 21:14 108-86-14.2
Bromochloromethane ND ug/kg 1 07/31/11 21:14 74-97-54.2
Bromodichloromethane ND ug/kg 1 07/31/11 21:14 75-27-44.2
Bromoform ND ug/kg 1 07/31/11 21:14 75-25-24.2
Bromomethane ND ug/kg 1 07/31/11 21:14 74-83-98.3
2-Butanone (MEK)ND ug/kg 1 07/31/11 21:14 78-93-383.2
n-Butylbenzene ND ug/kg 1 07/31/11 21:14 104-51-84.2
sec-Butylbenzene ND ug/kg 1 07/31/11 21:14 135-98-84.2
tert-Butylbenzene ND ug/kg 1 07/31/11 21:14 98-06-64.2
Carbon tetrachloride ND ug/kg 1 07/31/11 21:14 56-23-54.2
Chlorobenzene ND ug/kg 1 07/31/11 21:14 108-90-74.2
Chloroethane ND ug/kg 1 07/31/11 21:14 75-00-38.3
Chloroform ND ug/kg 1 07/31/11 21:14 67-66-34.2
Chloromethane ND ug/kg 1 07/31/11 21:14 74-87-38.3
2-Chlorotoluene ND ug/kg 1 07/31/11 21:14 95-49-84.2
4-Chlorotoluene ND ug/kg 1 07/31/11 21:14 106-43-44.2
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/31/11 21:14 96-12-84.2
Dibromochloromethane ND ug/kg 1 07/31/11 21:14 124-48-14.2
1,2-Dibromoethane (EDB)ND ug/kg 1 07/31/11 21:14 106-93-44.2
Dibromomethane ND ug/kg 1 07/31/11 21:14 74-95-34.2
1,2-Dichlorobenzene ND ug/kg 1 07/31/11 21:14 95-50-14.2
1,3-Dichlorobenzene ND ug/kg 1 07/31/11 21:14 541-73-14.2
1,4-Dichlorobenzene ND ug/kg 1 07/31/11 21:14 106-46-74.2
Dichlorodifluoromethane ND ug/kg 1 07/31/11 21:14 75-71-88.3
1,1-Dichloroethane ND ug/kg 1 07/31/11 21:14 75-34-34.2
1,2-Dichloroethane ND ug/kg 1 07/31/11 21:14 107-06-24.2
1,1-Dichloroethene ND ug/kg 1 07/31/11 21:14 75-35-44.2
cis-1,2-Dichloroethene ND ug/kg 1 07/31/11 21:14 156-59-24.2
trans-1,2-Dichloroethene ND ug/kg 1 07/31/11 21:14 156-60-54.2
1,2-Dichloropropane ND ug/kg 1 07/31/11 21:14 78-87-54.2
1,3-Dichloropropane ND ug/kg 1 07/31/11 21:14 142-28-94.2
2,2-Dichloropropane ND ug/kg 1 07/31/11 21:14 594-20-74.2
1,1-Dichloropropene ND ug/kg 1 07/31/11 21:14 563-58-64.2
cis-1,3-Dichloropropene ND ug/kg 1 07/31/11 21:14 10061-01-54.2
trans-1,3-Dichloropropene ND ug/kg 1 07/31/11 21:14 10061-02-64.2
Diisopropyl ether ND ug/kg 1 07/31/11 21:14 108-20-34.2
Ethylbenzene ND ug/kg 1 07/31/11 21:14 100-41-44.2
Hexachloro-1,3-butadiene ND ug/kg 1 07/31/11 21:14 87-68-34.2
2-Hexanone ND ug/kg 1 07/31/11 21:14 591-78-641.6
Isopropylbenzene (Cumene)ND ug/kg 1 07/31/11 21:14 98-82-84.2
p-Isopropyltoluene ND ug/kg 1 07/31/11 21:14 99-87-64.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 23 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-27 Lab ID:9299302005 Collected:07/28/11 11:45 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Methylene Chloride ND ug/kg 1 07/31/11 21:14 75-09-216.6
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/31/11 21:14 108-10-141.6
Methyl-tert-butyl ether ND ug/kg 1 07/31/11 21:14 1634-04-44.2
Naphthalene ND ug/kg 1 07/31/11 21:14 91-20-34.2
n-Propylbenzene ND ug/kg 1 07/31/11 21:14 103-65-14.2
Styrene ND ug/kg 1 07/31/11 21:14 100-42-54.2
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/31/11 21:14 630-20-64.2
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/31/11 21:14 79-34-54.2
Tetrachloroethene ND ug/kg 1 07/31/11 21:14 127-18-44.2
Toluene ND ug/kg 1 07/31/11 21:14 108-88-34.2
1,2,3-Trichlorobenzene ND ug/kg 1 07/31/11 21:14 87-61-64.2
1,2,4-Trichlorobenzene ND ug/kg 1 07/31/11 21:14 120-82-14.2
1,1,1-Trichloroethane ND ug/kg 1 07/31/11 21:14 71-55-64.2
1,1,2-Trichloroethane ND ug/kg 1 07/31/11 21:14 79-00-54.2
Trichloroethene ND ug/kg 1 07/31/11 21:14 79-01-64.2
Trichlorofluoromethane ND ug/kg 1 07/31/11 21:14 75-69-44.2
1,2,3-Trichloropropane ND ug/kg 1 07/31/11 21:14 96-18-44.2
1,2,4-Trimethylbenzene ND ug/kg 1 07/31/11 21:14 95-63-64.2
1,3,5-Trimethylbenzene ND ug/kg 1 07/31/11 21:14 108-67-84.2
Vinyl acetate ND ug/kg 1 07/31/11 21:14 108-05-441.6
Vinyl chloride ND ug/kg 1 07/31/11 21:14 75-01-48.3
Xylene (Total)ND ug/kg 1 07/31/11 21:14 1330-20-78.3
m&p-Xylene ND ug/kg 1 07/31/11 21:14 179601-23-18.3
o-Xylene ND ug/kg 1 07/31/11 21:14 95-47-64.2
Dibromofluoromethane (S)97 %1 07/31/11 21:14 1868-53-770-130
Toluene-d8 (S)103 %1 07/31/11 21:14 2037-26-570-130
4-Bromofluorobenzene (S)93 %1 07/31/11 21:14 460-00-470-130
1,2-Dichloroethane-d4 (S)91 %1 07/31/11 21:14 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 11.9 %1 08/01/11 09:040.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 16.0 mg/kg 1 08/05/11 16:46 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/04/11 13:23 18540-29-9 N208/04/11 10:432.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 24 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-28 Lab ID:9299302006 Collected:07/28/11 14:50 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 08/02/11 16:28 7440-36-008/02/11 09:000.65
Arsenic ND mg/kg 1 08/03/11 17:40 7440-38-208/02/11 09:000.65
Beryllium 0.20 mg/kg 1 08/02/11 16:28 7440-41-708/02/11 09:000.13
Cadmium 1.6 mg/kg 1 08/02/11 16:28 7440-43-908/02/11 09:000.13
Chromium 21.7 mg/kg 1 08/02/11 16:28 7440-47-308/02/11 09:000.65
Copper 36.4 mg/kg 1 08/02/11 16:28 7440-50-808/02/11 09:000.65
Lead 9.9 mg/kg 1 08/02/11 16:28 7439-92-108/02/11 09:000.65
Manganese 36.1 mg/kg 1 08/02/11 16:28 7439-96-508/02/11 09:000.65
Nickel 1.6 mg/kg 1 08/02/11 16:28 7440-02-008/02/11 09:000.65
Selenium 1.8 mg/kg 1 08/02/11 16:28 7782-49-208/02/11 09:001.3
Silver ND mg/kg 1 08/02/11 16:28 7440-22-408/02/11 09:000.65
Thallium ND mg/kg 1 08/02/11 16:28 7440-28-008/02/11 09:001.3
Zinc 14.5 mg/kg 1 08/02/11 16:28 7440-66-608/02/11 09:001.3
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.13 mg/kg 1 08/03/11 12:51 7439-97-608/01/11 14:150.0058
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 08/03/11 18:49 83-32-907/29/11 13:04443
Acenaphthylene ND ug/kg 1 08/03/11 18:49 208-96-807/29/11 13:04443
Aniline ND ug/kg 1 08/03/11 18:49 62-53-307/29/11 13:04443
Anthracene ND ug/kg 1 08/03/11 18:49 120-12-707/29/11 13:04443
Benzo(a)anthracene ND ug/kg 1 08/03/11 18:49 56-55-307/29/11 13:04443
Benzo(a)pyrene ND ug/kg 1 08/03/11 18:49 50-32-807/29/11 13:04443
Benzo(b)fluoranthene ND ug/kg 1 08/03/11 18:49 205-99-207/29/11 13:04443
Benzo(g,h,i)perylene ND ug/kg 1 08/03/11 18:49 191-24-207/29/11 13:04443
Benzo(k)fluoranthene ND ug/kg 1 08/03/11 18:49 207-08-907/29/11 13:04443
Benzoic Acid ND ug/kg 1 08/03/11 18:49 65-85-007/29/11 13:042210
Benzyl alcohol ND ug/kg 1 08/03/11 18:49 100-51-607/29/11 13:04886
4-Bromophenylphenyl ether ND ug/kg 1 08/03/11 18:49 101-55-307/29/11 13:04443
Butylbenzylphthalate ND ug/kg 1 08/03/11 18:49 85-68-707/29/11 13:04443
4-Chloro-3-methylphenol ND ug/kg 1 08/03/11 18:49 59-50-707/29/11 13:04886
4-Chloroaniline ND ug/kg 1 08/03/11 18:49 106-47-807/29/11 13:042210
bis(2-Chloroethoxy)methane ND ug/kg 1 08/03/11 18:49 111-91-107/29/11 13:04443
bis(2-Chloroethyl) ether ND ug/kg 1 08/03/11 18:49 111-44-407/29/11 13:04443
bis(2-Chloroisopropyl) ether ND ug/kg 1 08/03/11 18:49 108-60-107/29/11 13:04443
2-Chloronaphthalene ND ug/kg 1 08/03/11 18:49 91-58-707/29/11 13:04443
2-Chlorophenol ND ug/kg 1 08/03/11 18:49 95-57-807/29/11 13:04443
4-Chlorophenylphenyl ether ND ug/kg 1 08/03/11 18:49 7005-72-307/29/11 13:04443
Chrysene ND ug/kg 1 08/03/11 18:49 218-01-907/29/11 13:04443
Dibenz(a,h)anthracene ND ug/kg 1 08/03/11 18:49 53-70-307/29/11 13:04443
Dibenzofuran ND ug/kg 1 08/03/11 18:49 132-64-907/29/11 13:04443
1,2-Dichlorobenzene ND ug/kg 1 08/03/11 18:49 95-50-107/29/11 13:04443
1,3-Dichlorobenzene ND ug/kg 1 08/03/11 18:49 541-73-107/29/11 13:04443
1,4-Dichlorobenzene ND ug/kg 1 08/03/11 18:49 106-46-707/29/11 13:04443
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 25 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-28 Lab ID:9299302006 Collected:07/28/11 14:50 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3,3'-Dichlorobenzidine ND ug/kg 1 08/03/11 18:49 91-94-107/29/11 13:042210
2,4-Dichlorophenol ND ug/kg 1 08/03/11 18:49 120-83-207/29/11 13:04443
Diethylphthalate ND ug/kg 1 08/03/11 18:49 84-66-207/29/11 13:04443
2,4-Dimethylphenol ND ug/kg 1 08/03/11 18:49 105-67-907/29/11 13:04443
Dimethylphthalate ND ug/kg 1 08/03/11 18:49 131-11-307/29/11 13:04443
Di-n-butylphthalate ND ug/kg 1 08/03/11 18:49 84-74-207/29/11 13:04443
4,6-Dinitro-2-methylphenol ND ug/kg 1 08/03/11 18:49 534-52-107/29/11 13:04886
2,4-Dinitrophenol ND ug/kg 1 08/03/11 18:49 51-28-507/29/11 13:042210
2,4-Dinitrotoluene ND ug/kg 1 08/03/11 18:49 121-14-207/29/11 13:04443
2,6-Dinitrotoluene ND ug/kg 1 08/03/11 18:49 606-20-207/29/11 13:04443
Di-n-octylphthalate ND ug/kg 1 08/03/11 18:49 117-84-007/29/11 13:04443
bis(2-Ethylhexyl)phthalate ND ug/kg 1 08/03/11 18:49 117-81-707/29/11 13:04443
Fluoranthene ND ug/kg 1 08/03/11 18:49 206-44-007/29/11 13:04443
Fluorene ND ug/kg 1 08/03/11 18:49 86-73-707/29/11 13:04443
Hexachloro-1,3-butadiene ND ug/kg 1 08/03/11 18:49 87-68-307/29/11 13:04443
Hexachlorobenzene ND ug/kg 1 08/03/11 18:49 118-74-107/29/11 13:04443
Hexachlorocyclopentadiene ND ug/kg 1 08/03/11 18:49 77-47-407/29/11 13:04443
Hexachloroethane ND ug/kg 1 08/03/11 18:49 67-72-107/29/11 13:04443
Indeno(1,2,3-cd)pyrene ND ug/kg 1 08/03/11 18:49 193-39-507/29/11 13:04443
Isophorone ND ug/kg 1 08/03/11 18:49 78-59-107/29/11 13:04443
1-Methylnaphthalene ND ug/kg 1 08/03/11 18:49 90-12-007/29/11 13:04443
2-Methylnaphthalene ND ug/kg 1 08/03/11 18:49 91-57-607/29/11 13:04443
2-Methylphenol(o-Cresol)ND ug/kg 1 08/03/11 18:49 95-48-707/29/11 13:04443
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 08/03/11 18:4907/29/11 13:04443
Naphthalene ND ug/kg 1 08/03/11 18:49 91-20-307/29/11 13:04443
2-Nitroaniline ND ug/kg 1 08/03/11 18:49 88-74-407/29/11 13:042210
3-Nitroaniline ND ug/kg 1 08/03/11 18:49 99-09-207/29/11 13:042210
4-Nitroaniline ND ug/kg 1 08/03/11 18:49 100-01-607/29/11 13:04886
Nitrobenzene ND ug/kg 1 08/03/11 18:49 98-95-307/29/11 13:04443
2-Nitrophenol ND ug/kg 1 08/03/11 18:49 88-75-507/29/11 13:04443
4-Nitrophenol ND ug/kg 1 08/03/11 18:49 100-02-707/29/11 13:042210
N-Nitrosodimethylamine ND ug/kg 1 08/03/11 18:49 62-75-907/29/11 13:04443
N-Nitroso-di-n-propylamine ND ug/kg 1 08/03/11 18:49 621-64-707/29/11 13:04443
N-Nitrosodiphenylamine ND ug/kg 1 08/03/11 18:49 86-30-607/29/11 13:04443
Pentachlorophenol ND ug/kg 1 08/03/11 18:49 87-86-507/29/11 13:042210
Phenanthrene ND ug/kg 1 08/03/11 18:49 85-01-807/29/11 13:04443
Phenol ND ug/kg 1 08/03/11 18:49 108-95-207/29/11 13:04443
Pyrene ND ug/kg 1 08/03/11 18:49 129-00-007/29/11 13:04443
1,2,4-Trichlorobenzene ND ug/kg 1 08/03/11 18:49 120-82-107/29/11 13:04443
2,4,5-Trichlorophenol ND ug/kg 1 08/03/11 18:49 95-95-407/29/11 13:04443
2,4,6-Trichlorophenol ND ug/kg 1 08/03/11 18:49 88-06-207/29/11 13:04443
Nitrobenzene-d5 (S)67 %1 08/03/11 18:49 4165-60-007/29/11 13:0423-110
2-Fluorobiphenyl (S)61 %1 08/03/11 18:49 321-60-807/29/11 13:0430-110
Terphenyl-d14 (S)64 %1 08/03/11 18:49 1718-51-007/29/11 13:0428-110
Phenol-d6 (S)68 %1 08/03/11 18:49 13127-88-307/29/11 13:0422-110
2-Fluorophenol (S)65 %1 08/03/11 18:49 367-12-407/29/11 13:0413-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 26 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-28 Lab ID:9299302006 Collected:07/28/11 14:50 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4,6-Tribromophenol (S)58 %1 08/03/11 18:49 118-79-607/29/11 13:0427-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 08/01/11 14:09 67-64-1105
Benzene ND ug/kg 1 08/01/11 14:09 71-43-25.3
Bromobenzene ND ug/kg 1 08/01/11 14:09 108-86-15.3
Bromochloromethane ND ug/kg 1 08/01/11 14:09 74-97-55.3
Bromodichloromethane ND ug/kg 1 08/01/11 14:09 75-27-45.3
Bromoform ND ug/kg 1 08/01/11 14:09 75-25-25.3
Bromomethane ND ug/kg 1 08/01/11 14:09 74-83-910.5
2-Butanone (MEK)ND ug/kg 1 08/01/11 14:09 78-93-3105
n-Butylbenzene ND ug/kg 1 08/01/11 14:09 104-51-85.3
sec-Butylbenzene ND ug/kg 1 08/01/11 14:09 135-98-85.3
tert-Butylbenzene ND ug/kg 1 08/01/11 14:09 98-06-65.3
Carbon tetrachloride ND ug/kg 1 08/01/11 14:09 56-23-55.3
Chlorobenzene ND ug/kg 1 08/01/11 14:09 108-90-75.3
Chloroethane ND ug/kg 1 08/01/11 14:09 75-00-310.5
Chloroform ND ug/kg 1 08/01/11 14:09 67-66-35.3
Chloromethane ND ug/kg 1 08/01/11 14:09 74-87-310.5
2-Chlorotoluene ND ug/kg 1 08/01/11 14:09 95-49-85.3
4-Chlorotoluene ND ug/kg 1 08/01/11 14:09 106-43-45.3
1,2-Dibromo-3-chloropropane ND ug/kg 1 08/01/11 14:09 96-12-85.3
Dibromochloromethane ND ug/kg 1 08/01/11 14:09 124-48-15.3
1,2-Dibromoethane (EDB)ND ug/kg 1 08/01/11 14:09 106-93-45.3
Dibromomethane ND ug/kg 1 08/01/11 14:09 74-95-35.3
1,2-Dichlorobenzene ND ug/kg 1 08/01/11 14:09 95-50-15.3
1,3-Dichlorobenzene ND ug/kg 1 08/01/11 14:09 541-73-15.3
1,4-Dichlorobenzene ND ug/kg 1 08/01/11 14:09 106-46-75.3
Dichlorodifluoromethane ND ug/kg 1 08/01/11 14:09 75-71-810.5
1,1-Dichloroethane ND ug/kg 1 08/01/11 14:09 75-34-35.3
1,2-Dichloroethane ND ug/kg 1 08/01/11 14:09 107-06-25.3
1,1-Dichloroethene ND ug/kg 1 08/01/11 14:09 75-35-45.3
cis-1,2-Dichloroethene ND ug/kg 1 08/01/11 14:09 156-59-25.3
trans-1,2-Dichloroethene ND ug/kg 1 08/01/11 14:09 156-60-55.3
1,2-Dichloropropane ND ug/kg 1 08/01/11 14:09 78-87-55.3
1,3-Dichloropropane ND ug/kg 1 08/01/11 14:09 142-28-95.3
2,2-Dichloropropane ND ug/kg 1 08/01/11 14:09 594-20-75.3
1,1-Dichloropropene ND ug/kg 1 08/01/11 14:09 563-58-65.3
cis-1,3-Dichloropropene ND ug/kg 1 08/01/11 14:09 10061-01-55.3
trans-1,3-Dichloropropene ND ug/kg 1 08/01/11 14:09 10061-02-65.3
Diisopropyl ether ND ug/kg 1 08/01/11 14:09 108-20-35.3
Ethylbenzene ND ug/kg 1 08/01/11 14:09 100-41-45.3
Hexachloro-1,3-butadiene ND ug/kg 1 08/01/11 14:09 87-68-35.3
2-Hexanone ND ug/kg 1 08/01/11 14:09 591-78-652.7
Isopropylbenzene (Cumene)ND ug/kg 1 08/01/11 14:09 98-82-85.3
p-Isopropyltoluene ND ug/kg 1 08/01/11 14:09 99-87-65.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 27 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-28 Lab ID:9299302006 Collected:07/28/11 14:50 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Methylene Chloride ND ug/kg 1 08/01/11 14:09 75-09-221.1
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 08/01/11 14:09 108-10-152.7
Methyl-tert-butyl ether ND ug/kg 1 08/01/11 14:09 1634-04-45.3
Naphthalene ND ug/kg 1 08/01/11 14:09 91-20-35.3
n-Propylbenzene ND ug/kg 1 08/01/11 14:09 103-65-15.3
Styrene ND ug/kg 1 08/01/11 14:09 100-42-55.3
1,1,1,2-Tetrachloroethane ND ug/kg 1 08/01/11 14:09 630-20-65.3
1,1,2,2-Tetrachloroethane ND ug/kg 1 08/01/11 14:09 79-34-55.3
Tetrachloroethene ND ug/kg 1 08/01/11 14:09 127-18-45.3
Toluene ND ug/kg 1 08/01/11 14:09 108-88-35.3
1,2,3-Trichlorobenzene ND ug/kg 1 08/01/11 14:09 87-61-65.3
1,2,4-Trichlorobenzene ND ug/kg 1 08/01/11 14:09 120-82-15.3
1,1,1-Trichloroethane ND ug/kg 1 08/01/11 14:09 71-55-65.3
1,1,2-Trichloroethane ND ug/kg 1 08/01/11 14:09 79-00-55.3
Trichloroethene ND ug/kg 1 08/01/11 14:09 79-01-65.3
Trichlorofluoromethane ND ug/kg 1 08/01/11 14:09 75-69-45.3
1,2,3-Trichloropropane ND ug/kg 1 08/01/11 14:09 96-18-45.3
1,2,4-Trimethylbenzene ND ug/kg 1 08/01/11 14:09 95-63-65.3
1,3,5-Trimethylbenzene ND ug/kg 1 08/01/11 14:09 108-67-85.3
Vinyl acetate ND ug/kg 1 08/01/11 14:09 108-05-452.7
Vinyl chloride ND ug/kg 1 08/01/11 14:09 75-01-410.5
Xylene (Total)ND ug/kg 1 08/01/11 14:09 1330-20-710.5
m&p-Xylene ND ug/kg 1 08/01/11 14:09 179601-23-110.5
o-Xylene ND ug/kg 1 08/01/11 14:09 95-47-65.3
Dibromofluoromethane (S)95 %1 08/01/11 14:09 1868-53-770-130
Toluene-d8 (S)106 %1 08/01/11 14:09 2037-26-570-130
4-Bromofluorobenzene (S)94 %1 08/01/11 14:09 460-00-470-130
1,2-Dichloroethane-d4 (S)93 %1 08/01/11 14:09 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 25.5 %1 08/01/11 09:050.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 21.7 mg/kg 1 08/05/11 16:46 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/04/11 13:23 18540-29-9 N208/04/11 10:432.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 28 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-29 Lab ID:9299302007 Collected:07/28/11 15:15 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 08/02/11 16:32 7440-36-008/02/11 09:000.62
Arsenic 1.3 mg/kg 1 08/03/11 17:45 7440-38-208/02/11 09:000.62
Beryllium 0.13 mg/kg 1 08/02/11 16:32 7440-41-708/02/11 09:000.12
Cadmium ND mg/kg 1 08/02/11 16:32 7440-43-908/02/11 09:000.12
Chromium 8.9 mg/kg 1 08/02/11 16:32 7440-47-308/02/11 09:000.62
Copper 13.1 mg/kg 1 08/02/11 16:32 7440-50-808/02/11 09:000.62
Lead 18.6 mg/kg 1 08/02/11 16:32 7439-92-108/02/11 09:000.62
Manganese 73.3 mg/kg 1 08/02/11 16:32 7439-96-508/02/11 09:000.62
Nickel 4.4 mg/kg 1 08/02/11 16:32 7440-02-008/02/11 09:000.62
Selenium ND mg/kg 1 08/02/11 16:32 7782-49-208/02/11 09:001.2
Silver ND mg/kg 1 08/02/11 16:32 7440-22-408/02/11 09:000.62
Thallium ND mg/kg 1 08/02/11 16:32 7440-28-008/02/11 09:001.2
Zinc 23.2 mg/kg 1 08/02/11 16:32 7440-66-608/02/11 09:001.2
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.16 mg/kg 5 08/03/11 13:53 7439-97-608/01/11 14:150.023
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 08/03/11 20:39 83-32-907/29/11 13:04419
Acenaphthylene ND ug/kg 1 08/03/11 20:39 208-96-807/29/11 13:04419
Aniline ND ug/kg 1 08/03/11 20:39 62-53-307/29/11 13:04419
Anthracene ND ug/kg 1 08/03/11 20:39 120-12-707/29/11 13:04419
Benzo(a)anthracene ND ug/kg 1 08/03/11 20:39 56-55-307/29/11 13:04419
Benzo(a)pyrene ND ug/kg 1 08/03/11 20:39 50-32-807/29/11 13:04419
Benzo(b)fluoranthene ND ug/kg 1 08/03/11 20:39 205-99-207/29/11 13:04419
Benzo(g,h,i)perylene ND ug/kg 1 08/03/11 20:39 191-24-207/29/11 13:04419
Benzo(k)fluoranthene ND ug/kg 1 08/03/11 20:39 207-08-907/29/11 13:04419
Benzoic Acid ND ug/kg 1 08/03/11 20:39 65-85-007/29/11 13:042100
Benzyl alcohol ND ug/kg 1 08/03/11 20:39 100-51-607/29/11 13:04839
4-Bromophenylphenyl ether ND ug/kg 1 08/03/11 20:39 101-55-307/29/11 13:04419
Butylbenzylphthalate ND ug/kg 1 08/03/11 20:39 85-68-707/29/11 13:04419
4-Chloro-3-methylphenol ND ug/kg 1 08/03/11 20:39 59-50-707/29/11 13:04839
4-Chloroaniline ND ug/kg 1 08/03/11 20:39 106-47-807/29/11 13:042100
bis(2-Chloroethoxy)methane ND ug/kg 1 08/03/11 20:39 111-91-107/29/11 13:04419
bis(2-Chloroethyl) ether ND ug/kg 1 08/03/11 20:39 111-44-407/29/11 13:04419
bis(2-Chloroisopropyl) ether ND ug/kg 1 08/03/11 20:39 108-60-107/29/11 13:04419
2-Chloronaphthalene ND ug/kg 1 08/03/11 20:39 91-58-707/29/11 13:04419
2-Chlorophenol ND ug/kg 1 08/03/11 20:39 95-57-807/29/11 13:04419
4-Chlorophenylphenyl ether ND ug/kg 1 08/03/11 20:39 7005-72-307/29/11 13:04419
Chrysene ND ug/kg 1 08/03/11 20:39 218-01-907/29/11 13:04419
Dibenz(a,h)anthracene ND ug/kg 1 08/03/11 20:39 53-70-307/29/11 13:04419
Dibenzofuran ND ug/kg 1 08/03/11 20:39 132-64-907/29/11 13:04419
1,2-Dichlorobenzene ND ug/kg 1 08/03/11 20:39 95-50-107/29/11 13:04419
1,3-Dichlorobenzene ND ug/kg 1 08/03/11 20:39 541-73-107/29/11 13:04419
1,4-Dichlorobenzene ND ug/kg 1 08/03/11 20:39 106-46-707/29/11 13:04419
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 29 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-29 Lab ID:9299302007 Collected:07/28/11 15:15 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3,3'-Dichlorobenzidine ND ug/kg 1 08/03/11 20:39 91-94-107/29/11 13:042100
2,4-Dichlorophenol ND ug/kg 1 08/03/11 20:39 120-83-207/29/11 13:04419
Diethylphthalate ND ug/kg 1 08/03/11 20:39 84-66-207/29/11 13:04419
2,4-Dimethylphenol ND ug/kg 1 08/03/11 20:39 105-67-907/29/11 13:04419
Dimethylphthalate ND ug/kg 1 08/03/11 20:39 131-11-307/29/11 13:04419
Di-n-butylphthalate ND ug/kg 1 08/03/11 20:39 84-74-207/29/11 13:04419
4,6-Dinitro-2-methylphenol ND ug/kg 1 08/03/11 20:39 534-52-107/29/11 13:04839
2,4-Dinitrophenol ND ug/kg 1 08/03/11 20:39 51-28-507/29/11 13:042100
2,4-Dinitrotoluene ND ug/kg 1 08/03/11 20:39 121-14-207/29/11 13:04419
2,6-Dinitrotoluene ND ug/kg 1 08/03/11 20:39 606-20-207/29/11 13:04419
Di-n-octylphthalate ND ug/kg 1 08/03/11 20:39 117-84-007/29/11 13:04419
bis(2-Ethylhexyl)phthalate ND ug/kg 1 08/03/11 20:39 117-81-707/29/11 13:04419
Fluoranthene ND ug/kg 1 08/03/11 20:39 206-44-007/29/11 13:04419
Fluorene ND ug/kg 1 08/03/11 20:39 86-73-707/29/11 13:04419
Hexachloro-1,3-butadiene ND ug/kg 1 08/03/11 20:39 87-68-307/29/11 13:04419
Hexachlorobenzene ND ug/kg 1 08/03/11 20:39 118-74-107/29/11 13:04419
Hexachlorocyclopentadiene ND ug/kg 1 08/03/11 20:39 77-47-407/29/11 13:04419
Hexachloroethane ND ug/kg 1 08/03/11 20:39 67-72-107/29/11 13:04419
Indeno(1,2,3-cd)pyrene ND ug/kg 1 08/03/11 20:39 193-39-507/29/11 13:04419
Isophorone ND ug/kg 1 08/03/11 20:39 78-59-107/29/11 13:04419
1-Methylnaphthalene ND ug/kg 1 08/03/11 20:39 90-12-007/29/11 13:04419
2-Methylnaphthalene ND ug/kg 1 08/03/11 20:39 91-57-607/29/11 13:04419
2-Methylphenol(o-Cresol)ND ug/kg 1 08/03/11 20:39 95-48-707/29/11 13:04419
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 08/03/11 20:3907/29/11 13:04419
Naphthalene ND ug/kg 1 08/03/11 20:39 91-20-307/29/11 13:04419
2-Nitroaniline ND ug/kg 1 08/03/11 20:39 88-74-407/29/11 13:042100
3-Nitroaniline ND ug/kg 1 08/03/11 20:39 99-09-207/29/11 13:042100
4-Nitroaniline ND ug/kg 1 08/03/11 20:39 100-01-607/29/11 13:04839
Nitrobenzene ND ug/kg 1 08/03/11 20:39 98-95-307/29/11 13:04419
2-Nitrophenol ND ug/kg 1 08/03/11 20:39 88-75-507/29/11 13:04419
4-Nitrophenol ND ug/kg 1 08/03/11 20:39 100-02-707/29/11 13:042100
N-Nitrosodimethylamine ND ug/kg 1 08/03/11 20:39 62-75-907/29/11 13:04419
N-Nitroso-di-n-propylamine ND ug/kg 1 08/03/11 20:39 621-64-707/29/11 13:04419
N-Nitrosodiphenylamine ND ug/kg 1 08/03/11 20:39 86-30-607/29/11 13:04419
Pentachlorophenol ND ug/kg 1 08/03/11 20:39 87-86-507/29/11 13:042100
Phenanthrene ND ug/kg 1 08/03/11 20:39 85-01-807/29/11 13:04419
Phenol ND ug/kg 1 08/03/11 20:39 108-95-207/29/11 13:04419
Pyrene ND ug/kg 1 08/03/11 20:39 129-00-007/29/11 13:04419
1,2,4-Trichlorobenzene ND ug/kg 1 08/03/11 20:39 120-82-107/29/11 13:04419
2,4,5-Trichlorophenol ND ug/kg 1 08/03/11 20:39 95-95-407/29/11 13:04419
2,4,6-Trichlorophenol ND ug/kg 1 08/03/11 20:39 88-06-207/29/11 13:04419
Nitrobenzene-d5 (S)50 %1 08/03/11 20:39 4165-60-007/29/11 13:0423-110
2-Fluorobiphenyl (S)53 %1 08/03/11 20:39 321-60-807/29/11 13:0430-110
Terphenyl-d14 (S)56 %1 08/03/11 20:39 1718-51-007/29/11 13:0428-110
Phenol-d6 (S)46 %1 08/03/11 20:39 13127-88-307/29/11 13:0422-110
2-Fluorophenol (S)38 %1 08/03/11 20:39 367-12-407/29/11 13:0413-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 30 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-29 Lab ID:9299302007 Collected:07/28/11 15:15 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4,6-Tribromophenol (S)49 %1 08/03/11 20:39 118-79-607/29/11 13:0427-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/31/11 21:54 67-64-195.7
Benzene ND ug/kg 1 07/31/11 21:54 71-43-24.8
Bromobenzene ND ug/kg 1 07/31/11 21:54 108-86-14.8
Bromochloromethane ND ug/kg 1 07/31/11 21:54 74-97-54.8
Bromodichloromethane ND ug/kg 1 07/31/11 21:54 75-27-44.8
Bromoform ND ug/kg 1 07/31/11 21:54 75-25-24.8
Bromomethane ND ug/kg 1 07/31/11 21:54 74-83-99.6
2-Butanone (MEK)ND ug/kg 1 07/31/11 21:54 78-93-395.7
n-Butylbenzene ND ug/kg 1 07/31/11 21:54 104-51-84.8
sec-Butylbenzene ND ug/kg 1 07/31/11 21:54 135-98-84.8
tert-Butylbenzene ND ug/kg 1 07/31/11 21:54 98-06-64.8
Carbon tetrachloride ND ug/kg 1 07/31/11 21:54 56-23-54.8
Chlorobenzene ND ug/kg 1 07/31/11 21:54 108-90-74.8
Chloroethane ND ug/kg 1 07/31/11 21:54 75-00-39.6
Chloroform ND ug/kg 1 07/31/11 21:54 67-66-34.8
Chloromethane ND ug/kg 1 07/31/11 21:54 74-87-39.6
2-Chlorotoluene ND ug/kg 1 07/31/11 21:54 95-49-84.8
4-Chlorotoluene ND ug/kg 1 07/31/11 21:54 106-43-44.8
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/31/11 21:54 96-12-84.8
Dibromochloromethane ND ug/kg 1 07/31/11 21:54 124-48-14.8
1,2-Dibromoethane (EDB)ND ug/kg 1 07/31/11 21:54 106-93-44.8
Dibromomethane ND ug/kg 1 07/31/11 21:54 74-95-34.8
1,2-Dichlorobenzene ND ug/kg 1 07/31/11 21:54 95-50-14.8
1,3-Dichlorobenzene ND ug/kg 1 07/31/11 21:54 541-73-14.8
1,4-Dichlorobenzene ND ug/kg 1 07/31/11 21:54 106-46-74.8
Dichlorodifluoromethane ND ug/kg 1 07/31/11 21:54 75-71-89.6
1,1-Dichloroethane ND ug/kg 1 07/31/11 21:54 75-34-34.8
1,2-Dichloroethane ND ug/kg 1 07/31/11 21:54 107-06-24.8
1,1-Dichloroethene ND ug/kg 1 07/31/11 21:54 75-35-44.8
cis-1,2-Dichloroethene ND ug/kg 1 07/31/11 21:54 156-59-24.8
trans-1,2-Dichloroethene ND ug/kg 1 07/31/11 21:54 156-60-54.8
1,2-Dichloropropane ND ug/kg 1 07/31/11 21:54 78-87-54.8
1,3-Dichloropropane ND ug/kg 1 07/31/11 21:54 142-28-94.8
2,2-Dichloropropane ND ug/kg 1 07/31/11 21:54 594-20-74.8
1,1-Dichloropropene ND ug/kg 1 07/31/11 21:54 563-58-64.8
cis-1,3-Dichloropropene ND ug/kg 1 07/31/11 21:54 10061-01-54.8
trans-1,3-Dichloropropene ND ug/kg 1 07/31/11 21:54 10061-02-64.8
Diisopropyl ether ND ug/kg 1 07/31/11 21:54 108-20-34.8
Ethylbenzene ND ug/kg 1 07/31/11 21:54 100-41-44.8
Hexachloro-1,3-butadiene ND ug/kg 1 07/31/11 21:54 87-68-34.8
2-Hexanone ND ug/kg 1 07/31/11 21:54 591-78-647.8
Isopropylbenzene (Cumene)ND ug/kg 1 07/31/11 21:54 98-82-84.8
p-Isopropyltoluene ND ug/kg 1 07/31/11 21:54 99-87-64.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 31 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-29 Lab ID:9299302007 Collected:07/28/11 15:15 Received:07/29/11 10:30 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Methylene Chloride ND ug/kg 1 07/31/11 21:54 75-09-219.1
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/31/11 21:54 108-10-147.8
Methyl-tert-butyl ether ND ug/kg 1 07/31/11 21:54 1634-04-44.8
Naphthalene ND ug/kg 1 07/31/11 21:54 91-20-34.8
n-Propylbenzene ND ug/kg 1 07/31/11 21:54 103-65-14.8
Styrene ND ug/kg 1 07/31/11 21:54 100-42-54.8
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/31/11 21:54 630-20-64.8
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/31/11 21:54 79-34-54.8
Tetrachloroethene ND ug/kg 1 07/31/11 21:54 127-18-44.8
Toluene ND ug/kg 1 07/31/11 21:54 108-88-34.8
1,2,3-Trichlorobenzene ND ug/kg 1 07/31/11 21:54 87-61-64.8
1,2,4-Trichlorobenzene ND ug/kg 1 07/31/11 21:54 120-82-14.8
1,1,1-Trichloroethane ND ug/kg 1 07/31/11 21:54 71-55-64.8
1,1,2-Trichloroethane ND ug/kg 1 07/31/11 21:54 79-00-54.8
Trichloroethene ND ug/kg 1 07/31/11 21:54 79-01-64.8
Trichlorofluoromethane ND ug/kg 1 07/31/11 21:54 75-69-44.8
1,2,3-Trichloropropane ND ug/kg 1 07/31/11 21:54 96-18-44.8
1,2,4-Trimethylbenzene ND ug/kg 1 07/31/11 21:54 95-63-64.8
1,3,5-Trimethylbenzene ND ug/kg 1 07/31/11 21:54 108-67-84.8
Vinyl acetate ND ug/kg 1 07/31/11 21:54 108-05-447.8
Vinyl chloride ND ug/kg 1 07/31/11 21:54 75-01-49.6
Xylene (Total)ND ug/kg 1 07/31/11 21:54 1330-20-79.6
m&p-Xylene ND ug/kg 1 07/31/11 21:54 179601-23-19.6
o-Xylene ND ug/kg 1 07/31/11 21:54 95-47-64.8
Dibromofluoromethane (S)98 %1 07/31/11 21:54 1868-53-770-130
Toluene-d8 (S)103 %1 07/31/11 21:54 2037-26-570-130
4-Bromofluorobenzene (S)90 %1 07/31/11 21:54 460-00-470-130
1,2-Dichloroethane-d4 (S)86 %1 07/31/11 21:54 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 21.3 %1 08/01/11 09:050.10
Trivalent Chromium Calculation Analytical Method: Trivalent Chromium Calculation
Chromium, Trivalent 8.9 mg/kg 1 08/05/11 16:46 16065-83-15.0
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 08/04/11 13:28 18540-29-9 N208/04/11 10:430.88
Sample:SB-23 Lab ID:9299302008 Collected:07/28/11 08:45 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 08/05/11 10:42 83-32-908/01/11 15:0010.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 32 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-23 Lab ID:9299302008 Collected:07/28/11 08:45 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthylene ND ug/L 1 08/05/11 10:42 208-96-808/01/11 15:0010.0
Aniline ND ug/L 1 08/05/11 10:42 62-53-308/01/11 15:0010.0
Anthracene ND ug/L 1 08/05/11 10:42 120-12-708/01/11 15:0010.0
Benzo(a)anthracene ND ug/L 1 08/05/11 10:42 56-55-308/01/11 15:0010.0
Benzo(a)pyrene ND ug/L 1 08/05/11 10:42 50-32-808/01/11 15:0010.0
Benzo(b)fluoranthene ND ug/L 1 08/05/11 10:42 205-99-208/01/11 15:0010.0
Benzo(g,h,i)perylene ND ug/L 1 08/05/11 10:42 191-24-208/01/11 15:0010.0
Benzo(k)fluoranthene ND ug/L 1 08/05/11 10:42 207-08-908/01/11 15:0010.0
Benzoic Acid ND ug/L 1 08/05/11 10:42 65-85-008/01/11 15:0050.0
Benzyl alcohol ND ug/L 1 08/05/11 10:42 100-51-608/01/11 15:0020.0
4-Bromophenylphenyl ether ND ug/L 1 08/05/11 10:42 101-55-308/01/11 15:0010.0
Butylbenzylphthalate ND ug/L 1 08/05/11 10:42 85-68-708/01/11 15:0010.0
4-Chloro-3-methylphenol ND ug/L 1 08/05/11 10:42 59-50-708/01/11 15:0020.0
4-Chloroaniline ND ug/L 1 08/05/11 10:42 106-47-808/01/11 15:0020.0
bis(2-Chloroethoxy)methane ND ug/L 1 08/05/11 10:42 111-91-108/01/11 15:0010.0
bis(2-Chloroethyl) ether ND ug/L 1 08/05/11 10:42 111-44-408/01/11 15:0010.0
bis(2-Chloroisopropyl) ether ND ug/L 1 08/05/11 10:42 108-60-108/01/11 15:0010.0
2-Chloronaphthalene ND ug/L 1 08/05/11 10:42 91-58-708/01/11 15:0010.0
2-Chlorophenol ND ug/L 1 08/05/11 10:42 95-57-808/01/11 15:0010.0
4-Chlorophenylphenyl ether ND ug/L 1 08/05/11 10:42 7005-72-308/01/11 15:0010.0
Chrysene ND ug/L 1 08/05/11 10:42 218-01-908/01/11 15:0010.0
Dibenz(a,h)anthracene ND ug/L 1 08/05/11 10:42 53-70-308/01/11 15:0010.0
Dibenzofuran ND ug/L 1 08/05/11 10:42 132-64-908/01/11 15:0010.0
1,2-Dichlorobenzene ND ug/L 1 08/05/11 10:42 95-50-108/01/11 15:0010.0
1,3-Dichlorobenzene ND ug/L 1 08/05/11 10:42 541-73-108/01/11 15:0010.0
1,4-Dichlorobenzene ND ug/L 1 08/05/11 10:42 106-46-708/01/11 15:0010.0
3,3'-Dichlorobenzidine ND ug/L 1 08/05/11 10:42 91-94-108/01/11 15:0020.0
2,4-Dichlorophenol ND ug/L 1 08/05/11 10:42 120-83-208/01/11 15:0010.0
Diethylphthalate ND ug/L 1 08/05/11 10:42 84-66-208/01/11 15:0010.0
2,4-Dimethylphenol ND ug/L 1 08/05/11 10:42 105-67-908/01/11 15:0010.0
Dimethylphthalate ND ug/L 1 08/05/11 10:42 131-11-308/01/11 15:0010.0
Di-n-butylphthalate ND ug/L 1 08/05/11 10:42 84-74-208/01/11 15:0010.0
4,6-Dinitro-2-methylphenol ND ug/L 1 08/05/11 10:42 534-52-108/01/11 15:0020.0
2,4-Dinitrophenol ND ug/L 1 08/05/11 10:42 51-28-508/01/11 15:0050.0
2,4-Dinitrotoluene ND ug/L 1 08/05/11 10:42 121-14-208/01/11 15:0010.0
2,6-Dinitrotoluene ND ug/L 1 08/05/11 10:42 606-20-208/01/11 15:0010.0
Di-n-octylphthalate ND ug/L 1 08/05/11 10:42 117-84-008/01/11 15:0010.0
bis(2-Ethylhexyl)phthalate ND ug/L 1 08/05/11 10:42 117-81-708/01/11 15:006.0
Fluoranthene ND ug/L 1 08/05/11 10:42 206-44-008/01/11 15:0010.0
Fluorene ND ug/L 1 08/05/11 10:42 86-73-708/01/11 15:0010.0
Hexachloro-1,3-butadiene ND ug/L 1 08/05/11 10:42 87-68-308/01/11 15:0010.0
Hexachlorobenzene ND ug/L 1 08/05/11 10:42 118-74-108/01/11 15:0010.0
Hexachlorocyclopentadiene ND ug/L 1 08/05/11 10:42 77-47-408/01/11 15:0010.0
Hexachloroethane ND ug/L 1 08/05/11 10:42 67-72-108/01/11 15:0010.0
Indeno(1,2,3-cd)pyrene ND ug/L 1 08/05/11 10:42 193-39-508/01/11 15:0010.0
Isophorone ND ug/L 1 08/05/11 10:42 78-59-108/01/11 15:0010.0
1-Methylnaphthalene ND ug/L 1 08/05/11 10:42 90-12-008/01/11 15:0010.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 33 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-23 Lab ID:9299302008 Collected:07/28/11 08:45 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
2-Methylnaphthalene ND ug/L 1 08/05/11 10:42 91-57-608/01/11 15:0010.0
2-Methylphenol(o-Cresol)ND ug/L 1 08/05/11 10:42 95-48-708/01/11 15:0010.0
3&4-Methylphenol(m&p Cresol)ND ug/L 1 08/05/11 10:4208/01/11 15:0010.0
Naphthalene ND ug/L 1 08/05/11 10:42 91-20-308/01/11 15:0010.0
2-Nitroaniline ND ug/L 1 08/05/11 10:42 88-74-408/01/11 15:0050.0
3-Nitroaniline ND ug/L 1 08/05/11 10:42 99-09-208/01/11 15:0050.0
4-Nitroaniline ND ug/L 1 08/05/11 10:42 100-01-608/01/11 15:0020.0
Nitrobenzene ND ug/L 1 08/05/11 10:42 98-95-308/01/11 15:0010.0
2-Nitrophenol ND ug/L 1 08/05/11 10:42 88-75-508/01/11 15:0010.0
4-Nitrophenol ND ug/L 1 08/05/11 10:42 100-02-708/01/11 15:0050.0
N-Nitrosodimethylamine ND ug/L 1 08/05/11 10:42 62-75-908/01/11 15:0010.0
N-Nitroso-di-n-propylamine ND ug/L 1 08/05/11 10:42 621-64-708/01/11 15:0010.0
N-Nitrosodiphenylamine ND ug/L 1 08/05/11 10:42 86-30-608/01/11 15:0010.0
Pentachlorophenol ND ug/L 1 08/05/11 10:42 87-86-508/01/11 15:0025.0
Phenanthrene ND ug/L 1 08/05/11 10:42 85-01-808/01/11 15:0010.0
Phenol ND ug/L 1 08/05/11 10:42 108-95-208/01/11 15:0010.0
Pyrene ND ug/L 1 08/05/11 10:42 129-00-008/01/11 15:0010.0
1,2,4-Trichlorobenzene ND ug/L 1 08/05/11 10:42 120-82-108/01/11 15:0010.0
2,4,5-Trichlorophenol ND ug/L 1 08/05/11 10:42 95-95-408/01/11 15:0010.0
2,4,6-Trichlorophenol ND ug/L 1 08/05/11 10:42 88-06-208/01/11 15:0010.0
Nitrobenzene-d5 (S)67 %1 08/05/11 10:42 4165-60-008/01/11 15:0021-110
2-Fluorobiphenyl (S)66 %1 08/05/11 10:42 321-60-808/01/11 15:0027-110
Terphenyl-d14 (S)77 %1 08/05/11 10:42 1718-51-008/01/11 15:0031-107
Phenol-d6 (S)47 %1 08/05/11 10:42 13127-88-308/01/11 15:0010-110
2-Fluorophenol (S)49 %1 08/05/11 10:42 367-12-408/01/11 15:0012-110
2,4,6-Tribromophenol (S)84 %1 08/05/11 10:42 118-79-608/01/11 15:0027-110
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 08/02/11 21:24 67-64-125.0
Benzene ND ug/L 1 08/02/11 21:24 71-43-21.0
Bromobenzene ND ug/L 1 08/02/11 21:24 108-86-11.0
Bromochloromethane ND ug/L 1 08/02/11 21:24 74-97-51.0
Bromodichloromethane ND ug/L 1 08/02/11 21:24 75-27-41.0
Bromoform ND ug/L 1 08/02/11 21:24 75-25-21.0
Bromomethane ND ug/L 1 08/02/11 21:24 74-83-92.0
2-Butanone (MEK)ND ug/L 1 08/02/11 21:24 78-93-35.0
Carbon tetrachloride ND ug/L 1 08/02/11 21:24 56-23-51.0
Chlorobenzene ND ug/L 1 08/02/11 21:24 108-90-71.0
Chloroethane ND ug/L 1 08/02/11 21:24 75-00-31.0
Chloroform 5.7 ug/L 1 08/02/11 21:24 67-66-31.0
Chloromethane ND ug/L 1 08/02/11 21:24 74-87-31.0
2-Chlorotoluene ND ug/L 1 08/02/11 21:24 95-49-81.0
4-Chlorotoluene ND ug/L 1 08/02/11 21:24 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 08/02/11 21:24 96-12-85.0
Dibromochloromethane ND ug/L 1 08/02/11 21:24 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 08/02/11 21:24 106-93-41.0
Dibromomethane ND ug/L 1 08/02/11 21:24 74-95-31.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 34 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-23 Lab ID:9299302008 Collected:07/28/11 08:45 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
1,2-Dichlorobenzene ND ug/L 1 08/02/11 21:24 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 08/02/11 21:24 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 08/02/11 21:24 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 08/02/11 21:24 75-71-81.0
1,1-Dichloroethane ND ug/L 1 08/02/11 21:24 75-34-31.0
1,2-Dichloroethane ND ug/L 1 08/02/11 21:24 107-06-21.0
1,1-Dichloroethene ND ug/L 1 08/02/11 21:24 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 08/02/11 21:24 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 08/02/11 21:24 156-60-51.0
1,2-Dichloropropane ND ug/L 1 08/02/11 21:24 78-87-51.0
1,3-Dichloropropane ND ug/L 1 08/02/11 21:24 142-28-91.0
2,2-Dichloropropane ND ug/L 1 08/02/11 21:24 594-20-71.0
1,1-Dichloropropene ND ug/L 1 08/02/11 21:24 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 08/02/11 21:24 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 08/02/11 21:24 10061-02-61.0
Diisopropyl ether ND ug/L 1 08/02/11 21:24 108-20-31.0
Ethylbenzene ND ug/L 1 08/02/11 21:24 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 08/02/11 21:24 87-68-31.0
2-Hexanone ND ug/L 1 08/02/11 21:24 591-78-65.0
p-Isopropyltoluene ND ug/L 1 08/02/11 21:24 99-87-61.0
Methylene Chloride ND ug/L 1 08/02/11 21:24 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 08/02/11 21:24 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 08/02/11 21:24 1634-04-41.0
Naphthalene ND ug/L 1 08/02/11 21:24 91-20-31.0
Styrene ND ug/L 1 08/02/11 21:24 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 08/02/11 21:24 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 08/02/11 21:24 79-34-51.0
Tetrachloroethene ND ug/L 1 08/02/11 21:24 127-18-41.0
Toluene ND ug/L 1 08/02/11 21:24 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 08/02/11 21:24 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 08/02/11 21:24 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 08/02/11 21:24 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 08/02/11 21:24 79-00-51.0
Trichloroethene ND ug/L 1 08/02/11 21:24 79-01-61.0
Trichlorofluoromethane ND ug/L 1 08/02/11 21:24 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 08/02/11 21:24 96-18-41.0
Vinyl acetate ND ug/L 1 08/02/11 21:24 108-05-42.0
Vinyl chloride ND ug/L 1 08/02/11 21:24 75-01-41.0
Xylene (Total)ND ug/L 1 08/02/11 21:24 1330-20-72.0
m&p-Xylene ND ug/L 1 08/02/11 21:24 179601-23-12.0
o-Xylene ND ug/L 1 08/02/11 21:24 95-47-61.0
4-Bromofluorobenzene (S)98 %1 08/02/11 21:24 460-00-470-130
Dibromofluoromethane (S)105 %1 08/02/11 21:24 1868-53-770-130
1,2-Dichloroethane-d4 (S)107 %1 08/02/11 21:24 17060-07-070-130
Toluene-d8 (S)102 %1 08/02/11 21:24 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 35 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-24 Lab ID:9299302009 Collected:07/28/11 09:45 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 08/05/11 11:10 83-32-908/01/11 15:0010.0
Acenaphthylene ND ug/L 1 08/05/11 11:10 208-96-808/01/11 15:0010.0
Aniline ND ug/L 1 08/05/11 11:10 62-53-308/01/11 15:0010.0
Anthracene ND ug/L 1 08/05/11 11:10 120-12-708/01/11 15:0010.0
Benzo(a)anthracene ND ug/L 1 08/05/11 11:10 56-55-308/01/11 15:0010.0
Benzo(a)pyrene ND ug/L 1 08/05/11 11:10 50-32-808/01/11 15:0010.0
Benzo(b)fluoranthene ND ug/L 1 08/05/11 11:10 205-99-208/01/11 15:0010.0
Benzo(g,h,i)perylene ND ug/L 1 08/05/11 11:10 191-24-208/01/11 15:0010.0
Benzo(k)fluoranthene ND ug/L 1 08/05/11 11:10 207-08-908/01/11 15:0010.0
Benzoic Acid ND ug/L 1 08/05/11 11:10 65-85-008/01/11 15:0050.0
Benzyl alcohol ND ug/L 1 08/05/11 11:10 100-51-608/01/11 15:0020.0
4-Bromophenylphenyl ether ND ug/L 1 08/05/11 11:10 101-55-308/01/11 15:0010.0
Butylbenzylphthalate ND ug/L 1 08/05/11 11:10 85-68-708/01/11 15:0010.0
4-Chloro-3-methylphenol ND ug/L 1 08/05/11 11:10 59-50-708/01/11 15:0020.0
4-Chloroaniline ND ug/L 1 08/05/11 11:10 106-47-808/01/11 15:0020.0
bis(2-Chloroethoxy)methane ND ug/L 1 08/05/11 11:10 111-91-108/01/11 15:0010.0
bis(2-Chloroethyl) ether ND ug/L 1 08/05/11 11:10 111-44-408/01/11 15:0010.0
bis(2-Chloroisopropyl) ether ND ug/L 1 08/05/11 11:10 108-60-108/01/11 15:0010.0
2-Chloronaphthalene ND ug/L 1 08/05/11 11:10 91-58-708/01/11 15:0010.0
2-Chlorophenol ND ug/L 1 08/05/11 11:10 95-57-808/01/11 15:0010.0
4-Chlorophenylphenyl ether ND ug/L 1 08/05/11 11:10 7005-72-308/01/11 15:0010.0
Chrysene ND ug/L 1 08/05/11 11:10 218-01-908/01/11 15:0010.0
Dibenz(a,h)anthracene ND ug/L 1 08/05/11 11:10 53-70-308/01/11 15:0010.0
Dibenzofuran ND ug/L 1 08/05/11 11:10 132-64-908/01/11 15:0010.0
1,2-Dichlorobenzene ND ug/L 1 08/05/11 11:10 95-50-108/01/11 15:0010.0
1,3-Dichlorobenzene ND ug/L 1 08/05/11 11:10 541-73-108/01/11 15:0010.0
1,4-Dichlorobenzene ND ug/L 1 08/05/11 11:10 106-46-708/01/11 15:0010.0
3,3'-Dichlorobenzidine ND ug/L 1 08/05/11 11:10 91-94-108/01/11 15:0020.0
2,4-Dichlorophenol ND ug/L 1 08/05/11 11:10 120-83-208/01/11 15:0010.0
Diethylphthalate ND ug/L 1 08/05/11 11:10 84-66-208/01/11 15:0010.0
2,4-Dimethylphenol ND ug/L 1 08/05/11 11:10 105-67-908/01/11 15:0010.0
Dimethylphthalate ND ug/L 1 08/05/11 11:10 131-11-308/01/11 15:0010.0
Di-n-butylphthalate ND ug/L 1 08/05/11 11:10 84-74-208/01/11 15:0010.0
4,6-Dinitro-2-methylphenol ND ug/L 1 08/05/11 11:10 534-52-108/01/11 15:0020.0
2,4-Dinitrophenol ND ug/L 1 08/05/11 11:10 51-28-508/01/11 15:0050.0
2,4-Dinitrotoluene ND ug/L 1 08/05/11 11:10 121-14-208/01/11 15:0010.0
2,6-Dinitrotoluene ND ug/L 1 08/05/11 11:10 606-20-208/01/11 15:0010.0
Di-n-octylphthalate ND ug/L 1 08/05/11 11:10 117-84-008/01/11 15:0010.0
bis(2-Ethylhexyl)phthalate ND ug/L 1 08/05/11 11:10 117-81-708/01/11 15:006.0
Fluoranthene ND ug/L 1 08/05/11 11:10 206-44-008/01/11 15:0010.0
Fluorene ND ug/L 1 08/05/11 11:10 86-73-708/01/11 15:0010.0
Hexachloro-1,3-butadiene ND ug/L 1 08/05/11 11:10 87-68-308/01/11 15:0010.0
Hexachlorobenzene ND ug/L 1 08/05/11 11:10 118-74-108/01/11 15:0010.0
Hexachlorocyclopentadiene ND ug/L 1 08/05/11 11:10 77-47-408/01/11 15:0010.0
Hexachloroethane ND ug/L 1 08/05/11 11:10 67-72-108/01/11 15:0010.0
Indeno(1,2,3-cd)pyrene ND ug/L 1 08/05/11 11:10 193-39-508/01/11 15:0010.0
Isophorone ND ug/L 1 08/05/11 11:10 78-59-108/01/11 15:0010.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 36 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-24 Lab ID:9299302009 Collected:07/28/11 09:45 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
1-Methylnaphthalene ND ug/L 1 08/05/11 11:10 90-12-008/01/11 15:0010.0
2-Methylnaphthalene ND ug/L 1 08/05/11 11:10 91-57-608/01/11 15:0010.0
2-Methylphenol(o-Cresol)ND ug/L 1 08/05/11 11:10 95-48-708/01/11 15:0010.0
3&4-Methylphenol(m&p Cresol)ND ug/L 1 08/05/11 11:1008/01/11 15:0010.0
Naphthalene ND ug/L 1 08/05/11 11:10 91-20-308/01/11 15:0010.0
2-Nitroaniline ND ug/L 1 08/05/11 11:10 88-74-408/01/11 15:0050.0
3-Nitroaniline ND ug/L 1 08/05/11 11:10 99-09-208/01/11 15:0050.0
4-Nitroaniline ND ug/L 1 08/05/11 11:10 100-01-608/01/11 15:0020.0
Nitrobenzene ND ug/L 1 08/05/11 11:10 98-95-308/01/11 15:0010.0
2-Nitrophenol ND ug/L 1 08/05/11 11:10 88-75-508/01/11 15:0010.0
4-Nitrophenol ND ug/L 1 08/05/11 11:10 100-02-708/01/11 15:0050.0
N-Nitrosodimethylamine ND ug/L 1 08/05/11 11:10 62-75-908/01/11 15:0010.0
N-Nitroso-di-n-propylamine ND ug/L 1 08/05/11 11:10 621-64-708/01/11 15:0010.0
N-Nitrosodiphenylamine ND ug/L 1 08/05/11 11:10 86-30-608/01/11 15:0010.0
Pentachlorophenol ND ug/L 1 08/05/11 11:10 87-86-508/01/11 15:0025.0
Phenanthrene ND ug/L 1 08/05/11 11:10 85-01-808/01/11 15:0010.0
Phenol ND ug/L 1 08/05/11 11:10 108-95-208/01/11 15:0010.0
Pyrene ND ug/L 1 08/05/11 11:10 129-00-008/01/11 15:0010.0
1,2,4-Trichlorobenzene ND ug/L 1 08/05/11 11:10 120-82-108/01/11 15:0010.0
2,4,5-Trichlorophenol ND ug/L 1 08/05/11 11:10 95-95-408/01/11 15:0010.0
2,4,6-Trichlorophenol ND ug/L 1 08/05/11 11:10 88-06-208/01/11 15:0010.0
Nitrobenzene-d5 (S)51 %1 08/05/11 11:10 4165-60-008/01/11 15:0021-110
2-Fluorobiphenyl (S)61 %1 08/05/11 11:10 321-60-808/01/11 15:0027-110
Terphenyl-d14 (S)78 %1 08/05/11 11:10 1718-51-008/01/11 15:0031-107
Phenol-d6 (S)52 %1 08/05/11 11:10 13127-88-308/01/11 15:0010-110
2-Fluorophenol (S)44 %1 08/05/11 11:10 367-12-408/01/11 15:0012-110
2,4,6-Tribromophenol (S)81 %1 08/05/11 11:10 118-79-608/01/11 15:0027-110
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 08/02/11 21:49 67-64-125.0
Benzene ND ug/L 1 08/02/11 21:49 71-43-21.0
Bromobenzene ND ug/L 1 08/02/11 21:49 108-86-11.0
Bromochloromethane ND ug/L 1 08/02/11 21:49 74-97-51.0
Bromodichloromethane ND ug/L 1 08/02/11 21:49 75-27-41.0
Bromoform ND ug/L 1 08/02/11 21:49 75-25-21.0
Bromomethane ND ug/L 1 08/02/11 21:49 74-83-92.0
2-Butanone (MEK)ND ug/L 1 08/02/11 21:49 78-93-35.0
Carbon tetrachloride ND ug/L 1 08/02/11 21:49 56-23-51.0
Chlorobenzene ND ug/L 1 08/02/11 21:49 108-90-71.0
Chloroethane ND ug/L 1 08/02/11 21:49 75-00-31.0
Chloroform 12.6 ug/L 1 08/02/11 21:49 67-66-31.0
Chloromethane ND ug/L 1 08/02/11 21:49 74-87-31.0
2-Chlorotoluene ND ug/L 1 08/02/11 21:49 95-49-81.0
4-Chlorotoluene ND ug/L 1 08/02/11 21:49 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 08/02/11 21:49 96-12-85.0
Dibromochloromethane ND ug/L 1 08/02/11 21:49 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 08/02/11 21:49 106-93-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 37 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-24 Lab ID:9299302009 Collected:07/28/11 09:45 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Dibromomethane ND ug/L 1 08/02/11 21:49 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 08/02/11 21:49 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 08/02/11 21:49 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 08/02/11 21:49 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 08/02/11 21:49 75-71-81.0
1,1-Dichloroethane ND ug/L 1 08/02/11 21:49 75-34-31.0
1,2-Dichloroethane ND ug/L 1 08/02/11 21:49 107-06-21.0
1,1-Dichloroethene ND ug/L 1 08/02/11 21:49 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 08/02/11 21:49 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 08/02/11 21:49 156-60-51.0
1,2-Dichloropropane ND ug/L 1 08/02/11 21:49 78-87-51.0
1,3-Dichloropropane ND ug/L 1 08/02/11 21:49 142-28-91.0
2,2-Dichloropropane ND ug/L 1 08/02/11 21:49 594-20-71.0
1,1-Dichloropropene ND ug/L 1 08/02/11 21:49 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 08/02/11 21:49 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 08/02/11 21:49 10061-02-61.0
Diisopropyl ether ND ug/L 1 08/02/11 21:49 108-20-31.0
Ethylbenzene ND ug/L 1 08/02/11 21:49 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 08/02/11 21:49 87-68-31.0
2-Hexanone ND ug/L 1 08/02/11 21:49 591-78-65.0
p-Isopropyltoluene ND ug/L 1 08/02/11 21:49 99-87-61.0
Methylene Chloride ND ug/L 1 08/02/11 21:49 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 08/02/11 21:49 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 08/02/11 21:49 1634-04-41.0
Naphthalene ND ug/L 1 08/02/11 21:49 91-20-31.0
Styrene ND ug/L 1 08/02/11 21:49 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 08/02/11 21:49 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 08/02/11 21:49 79-34-51.0
Tetrachloroethene ND ug/L 1 08/02/11 21:49 127-18-41.0
Toluene ND ug/L 1 08/02/11 21:49 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 08/02/11 21:49 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 08/02/11 21:49 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 08/02/11 21:49 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 08/02/11 21:49 79-00-51.0
Trichloroethene ND ug/L 1 08/02/11 21:49 79-01-61.0
Trichlorofluoromethane ND ug/L 1 08/02/11 21:49 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 08/02/11 21:49 96-18-41.0
Vinyl acetate ND ug/L 1 08/02/11 21:49 108-05-42.0
Vinyl chloride ND ug/L 1 08/02/11 21:49 75-01-41.0
Xylene (Total)ND ug/L 1 08/02/11 21:49 1330-20-72.0
m&p-Xylene ND ug/L 1 08/02/11 21:49 179601-23-12.0
o-Xylene ND ug/L 1 08/02/11 21:49 95-47-61.0
4-Bromofluorobenzene (S)99 %1 08/02/11 21:49 460-00-470-130
Dibromofluoromethane (S)104 %1 08/02/11 21:49 1868-53-770-130
1,2-Dichloroethane-d4 (S)106 %1 08/02/11 21:49 17060-07-070-130
Toluene-d8 (S)100 %1 08/02/11 21:49 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 38 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-25 Lab ID:9299302010 Collected:07/28/11 14:15 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 08/05/11 11:39 83-32-908/01/11 15:0010.0
Acenaphthylene ND ug/L 1 08/05/11 11:39 208-96-808/01/11 15:0010.0
Aniline ND ug/L 1 08/05/11 11:39 62-53-308/01/11 15:0010.0
Anthracene ND ug/L 1 08/05/11 11:39 120-12-708/01/11 15:0010.0
Benzo(a)anthracene ND ug/L 1 08/05/11 11:39 56-55-308/01/11 15:0010.0
Benzo(a)pyrene ND ug/L 1 08/05/11 11:39 50-32-808/01/11 15:0010.0
Benzo(b)fluoranthene ND ug/L 1 08/05/11 11:39 205-99-208/01/11 15:0010.0
Benzo(g,h,i)perylene ND ug/L 1 08/05/11 11:39 191-24-208/01/11 15:0010.0
Benzo(k)fluoranthene ND ug/L 1 08/05/11 11:39 207-08-908/01/11 15:0010.0
Benzoic Acid ND ug/L 1 08/05/11 11:39 65-85-008/01/11 15:0050.0
Benzyl alcohol ND ug/L 1 08/05/11 11:39 100-51-608/01/11 15:0020.0
4-Bromophenylphenyl ether ND ug/L 1 08/05/11 11:39 101-55-308/01/11 15:0010.0
Butylbenzylphthalate ND ug/L 1 08/05/11 11:39 85-68-708/01/11 15:0010.0
4-Chloro-3-methylphenol ND ug/L 1 08/05/11 11:39 59-50-708/01/11 15:0020.0
4-Chloroaniline ND ug/L 1 08/05/11 11:39 106-47-808/01/11 15:0020.0
bis(2-Chloroethoxy)methane ND ug/L 1 08/05/11 11:39 111-91-108/01/11 15:0010.0
bis(2-Chloroethyl) ether ND ug/L 1 08/05/11 11:39 111-44-408/01/11 15:0010.0
bis(2-Chloroisopropyl) ether ND ug/L 1 08/05/11 11:39 108-60-108/01/11 15:0010.0
2-Chloronaphthalene ND ug/L 1 08/05/11 11:39 91-58-708/01/11 15:0010.0
2-Chlorophenol ND ug/L 1 08/05/11 11:39 95-57-808/01/11 15:0010.0
4-Chlorophenylphenyl ether ND ug/L 1 08/05/11 11:39 7005-72-308/01/11 15:0010.0
Chrysene ND ug/L 1 08/05/11 11:39 218-01-908/01/11 15:0010.0
Dibenz(a,h)anthracene ND ug/L 1 08/05/11 11:39 53-70-308/01/11 15:0010.0
Dibenzofuran ND ug/L 1 08/05/11 11:39 132-64-908/01/11 15:0010.0
1,2-Dichlorobenzene ND ug/L 1 08/05/11 11:39 95-50-108/01/11 15:0010.0
1,3-Dichlorobenzene ND ug/L 1 08/05/11 11:39 541-73-108/01/11 15:0010.0
1,4-Dichlorobenzene ND ug/L 1 08/05/11 11:39 106-46-708/01/11 15:0010.0
3,3'-Dichlorobenzidine ND ug/L 1 08/05/11 11:39 91-94-108/01/11 15:0020.0
2,4-Dichlorophenol ND ug/L 1 08/05/11 11:39 120-83-208/01/11 15:0010.0
Diethylphthalate ND ug/L 1 08/05/11 11:39 84-66-208/01/11 15:0010.0
2,4-Dimethylphenol ND ug/L 1 08/05/11 11:39 105-67-908/01/11 15:0010.0
Dimethylphthalate ND ug/L 1 08/05/11 11:39 131-11-308/01/11 15:0010.0
Di-n-butylphthalate ND ug/L 1 08/05/11 11:39 84-74-208/01/11 15:0010.0
4,6-Dinitro-2-methylphenol ND ug/L 1 08/05/11 11:39 534-52-108/01/11 15:0020.0
2,4-Dinitrophenol ND ug/L 1 08/05/11 11:39 51-28-508/01/11 15:0050.0
2,4-Dinitrotoluene ND ug/L 1 08/05/11 11:39 121-14-208/01/11 15:0010.0
2,6-Dinitrotoluene ND ug/L 1 08/05/11 11:39 606-20-208/01/11 15:0010.0
Di-n-octylphthalate ND ug/L 1 08/05/11 11:39 117-84-008/01/11 15:0010.0
bis(2-Ethylhexyl)phthalate ND ug/L 1 08/05/11 11:39 117-81-708/01/11 15:006.0
Fluoranthene ND ug/L 1 08/05/11 11:39 206-44-008/01/11 15:0010.0
Fluorene ND ug/L 1 08/05/11 11:39 86-73-708/01/11 15:0010.0
Hexachloro-1,3-butadiene ND ug/L 1 08/05/11 11:39 87-68-308/01/11 15:0010.0
Hexachlorobenzene ND ug/L 1 08/05/11 11:39 118-74-108/01/11 15:0010.0
Hexachlorocyclopentadiene ND ug/L 1 08/05/11 11:39 77-47-408/01/11 15:0010.0
Hexachloroethane ND ug/L 1 08/05/11 11:39 67-72-108/01/11 15:0010.0
Indeno(1,2,3-cd)pyrene ND ug/L 1 08/05/11 11:39 193-39-508/01/11 15:0010.0
Isophorone ND ug/L 1 08/05/11 11:39 78-59-108/01/11 15:0010.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 39 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-25 Lab ID:9299302010 Collected:07/28/11 14:15 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
1-Methylnaphthalene ND ug/L 1 08/05/11 11:39 90-12-008/01/11 15:0010.0
2-Methylnaphthalene ND ug/L 1 08/05/11 11:39 91-57-608/01/11 15:0010.0
2-Methylphenol(o-Cresol)ND ug/L 1 08/05/11 11:39 95-48-708/01/11 15:0010.0
3&4-Methylphenol(m&p Cresol)ND ug/L 1 08/05/11 11:3908/01/11 15:0010.0
Naphthalene ND ug/L 1 08/05/11 11:39 91-20-308/01/11 15:0010.0
2-Nitroaniline ND ug/L 1 08/05/11 11:39 88-74-408/01/11 15:0050.0
3-Nitroaniline ND ug/L 1 08/05/11 11:39 99-09-208/01/11 15:0050.0
4-Nitroaniline ND ug/L 1 08/05/11 11:39 100-01-608/01/11 15:0020.0
Nitrobenzene ND ug/L 1 08/05/11 11:39 98-95-308/01/11 15:0010.0
2-Nitrophenol ND ug/L 1 08/05/11 11:39 88-75-508/01/11 15:0010.0
4-Nitrophenol ND ug/L 1 08/05/11 11:39 100-02-708/01/11 15:0050.0
N-Nitrosodimethylamine ND ug/L 1 08/05/11 11:39 62-75-908/01/11 15:0010.0
N-Nitroso-di-n-propylamine ND ug/L 1 08/05/11 11:39 621-64-708/01/11 15:0010.0
N-Nitrosodiphenylamine ND ug/L 1 08/05/11 11:39 86-30-608/01/11 15:0010.0
Pentachlorophenol ND ug/L 1 08/05/11 11:39 87-86-508/01/11 15:0025.0
Phenanthrene ND ug/L 1 08/05/11 11:39 85-01-808/01/11 15:0010.0
Phenol ND ug/L 1 08/05/11 11:39 108-95-208/01/11 15:0010.0
Pyrene ND ug/L 1 08/05/11 11:39 129-00-008/01/11 15:0010.0
1,2,4-Trichlorobenzene ND ug/L 1 08/05/11 11:39 120-82-108/01/11 15:0010.0
2,4,5-Trichlorophenol ND ug/L 1 08/05/11 11:39 95-95-408/01/11 15:0010.0
2,4,6-Trichlorophenol ND ug/L 1 08/05/11 11:39 88-06-208/01/11 15:0010.0
Nitrobenzene-d5 (S)63 %1 08/05/11 11:39 4165-60-008/01/11 15:0021-110
2-Fluorobiphenyl (S)60 %1 08/05/11 11:39 321-60-808/01/11 15:0027-110
Terphenyl-d14 (S)77 %1 08/05/11 11:39 1718-51-008/01/11 15:0031-107
Phenol-d6 (S)49 %1 08/05/11 11:39 13127-88-308/01/11 15:0010-110
2-Fluorophenol (S)52 %1 08/05/11 11:39 367-12-408/01/11 15:0012-110
2,4,6-Tribromophenol (S)83 %1 08/05/11 11:39 118-79-608/01/11 15:0027-110
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 08/02/11 22:13 67-64-125.0
Benzene ND ug/L 1 08/02/11 22:13 71-43-21.0
Bromobenzene ND ug/L 1 08/02/11 22:13 108-86-11.0
Bromochloromethane ND ug/L 1 08/02/11 22:13 74-97-51.0
Bromodichloromethane ND ug/L 1 08/02/11 22:13 75-27-41.0
Bromoform ND ug/L 1 08/02/11 22:13 75-25-21.0
Bromomethane ND ug/L 1 08/02/11 22:13 74-83-92.0
2-Butanone (MEK)ND ug/L 1 08/02/11 22:13 78-93-35.0
Carbon tetrachloride ND ug/L 1 08/02/11 22:13 56-23-51.0
Chlorobenzene ND ug/L 1 08/02/11 22:13 108-90-71.0
Chloroethane ND ug/L 1 08/02/11 22:13 75-00-31.0
Chloroform 2.1 ug/L 1 08/02/11 22:13 67-66-31.0
Chloromethane ND ug/L 1 08/02/11 22:13 74-87-31.0
2-Chlorotoluene ND ug/L 1 08/02/11 22:13 95-49-81.0
4-Chlorotoluene ND ug/L 1 08/02/11 22:13 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 08/02/11 22:13 96-12-85.0
Dibromochloromethane ND ug/L 1 08/02/11 22:13 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 08/02/11 22:13 106-93-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 40 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-25 Lab ID:9299302010 Collected:07/28/11 14:15 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Dibromomethane ND ug/L 1 08/02/11 22:13 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 08/02/11 22:13 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 08/02/11 22:13 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 08/02/11 22:13 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 08/02/11 22:13 75-71-81.0
1,1-Dichloroethane ND ug/L 1 08/02/11 22:13 75-34-31.0
1,2-Dichloroethane ND ug/L 1 08/02/11 22:13 107-06-21.0
1,1-Dichloroethene ND ug/L 1 08/02/11 22:13 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 08/02/11 22:13 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 08/02/11 22:13 156-60-51.0
1,2-Dichloropropane ND ug/L 1 08/02/11 22:13 78-87-51.0
1,3-Dichloropropane ND ug/L 1 08/02/11 22:13 142-28-91.0
2,2-Dichloropropane ND ug/L 1 08/02/11 22:13 594-20-71.0
1,1-Dichloropropene ND ug/L 1 08/02/11 22:13 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 08/02/11 22:13 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 08/02/11 22:13 10061-02-61.0
Diisopropyl ether ND ug/L 1 08/02/11 22:13 108-20-31.0
Ethylbenzene ND ug/L 1 08/02/11 22:13 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 08/02/11 22:13 87-68-31.0
2-Hexanone ND ug/L 1 08/02/11 22:13 591-78-65.0
p-Isopropyltoluene ND ug/L 1 08/02/11 22:13 99-87-61.0
Methylene Chloride ND ug/L 1 08/02/11 22:13 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 08/02/11 22:13 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 08/02/11 22:13 1634-04-41.0
Naphthalene ND ug/L 1 08/02/11 22:13 91-20-31.0
Styrene ND ug/L 1 08/02/11 22:13 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 08/02/11 22:13 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 08/02/11 22:13 79-34-51.0
Tetrachloroethene ND ug/L 1 08/02/11 22:13 127-18-41.0
Toluene ND ug/L 1 08/02/11 22:13 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 08/02/11 22:13 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 08/02/11 22:13 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 08/02/11 22:13 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 08/02/11 22:13 79-00-51.0
Trichloroethene ND ug/L 1 08/02/11 22:13 79-01-61.0
Trichlorofluoromethane ND ug/L 1 08/02/11 22:13 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 08/02/11 22:13 96-18-41.0
Vinyl acetate ND ug/L 1 08/02/11 22:13 108-05-42.0
Vinyl chloride ND ug/L 1 08/02/11 22:13 75-01-41.0
Xylene (Total)ND ug/L 1 08/02/11 22:13 1330-20-72.0
m&p-Xylene ND ug/L 1 08/02/11 22:13 179601-23-12.0
o-Xylene ND ug/L 1 08/02/11 22:13 95-47-61.0
4-Bromofluorobenzene (S)96 %1 08/02/11 22:13 460-00-470-130
Dibromofluoromethane (S)108 %1 08/02/11 22:13 1868-53-770-130
1,2-Dichloroethane-d4 (S)110 %1 08/02/11 22:13 17060-07-070-130
Toluene-d8 (S)101 %1 08/02/11 22:13 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 41 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-26 Lab ID:9299302011 Collected:07/28/11 10:45 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 08/05/11 14:55 83-32-908/01/11 15:0010.0
Acenaphthylene ND ug/L 1 08/05/11 14:55 208-96-808/01/11 15:0010.0
Aniline ND ug/L 1 08/05/11 14:55 62-53-308/01/11 15:0010.0
Anthracene ND ug/L 1 08/05/11 14:55 120-12-708/01/11 15:0010.0
Benzo(a)anthracene ND ug/L 1 08/05/11 14:55 56-55-308/01/11 15:0010.0
Benzo(a)pyrene ND ug/L 1 08/05/11 14:55 50-32-808/01/11 15:0010.0
Benzo(b)fluoranthene ND ug/L 1 08/05/11 14:55 205-99-208/01/11 15:0010.0
Benzo(g,h,i)perylene ND ug/L 1 08/05/11 14:55 191-24-208/01/11 15:0010.0
Benzo(k)fluoranthene ND ug/L 1 08/05/11 14:55 207-08-908/01/11 15:0010.0
Benzoic Acid ND ug/L 1 08/05/11 14:55 65-85-008/01/11 15:0050.0
Benzyl alcohol ND ug/L 1 08/05/11 14:55 100-51-608/01/11 15:0020.0
4-Bromophenylphenyl ether ND ug/L 1 08/05/11 14:55 101-55-308/01/11 15:0010.0
Butylbenzylphthalate ND ug/L 1 08/05/11 14:55 85-68-708/01/11 15:0010.0
4-Chloro-3-methylphenol ND ug/L 1 08/05/11 14:55 59-50-708/01/11 15:0020.0
4-Chloroaniline ND ug/L 1 08/05/11 14:55 106-47-808/01/11 15:0020.0
bis(2-Chloroethoxy)methane ND ug/L 1 08/05/11 14:55 111-91-108/01/11 15:0010.0
bis(2-Chloroethyl) ether ND ug/L 1 08/05/11 14:55 111-44-408/01/11 15:0010.0
bis(2-Chloroisopropyl) ether ND ug/L 1 08/05/11 14:55 108-60-108/01/11 15:0010.0
2-Chloronaphthalene ND ug/L 1 08/05/11 14:55 91-58-708/01/11 15:0010.0
2-Chlorophenol ND ug/L 1 08/05/11 14:55 95-57-808/01/11 15:0010.0
4-Chlorophenylphenyl ether ND ug/L 1 08/05/11 14:55 7005-72-308/01/11 15:0010.0
Chrysene ND ug/L 1 08/05/11 14:55 218-01-908/01/11 15:0010.0
Dibenz(a,h)anthracene ND ug/L 1 08/05/11 14:55 53-70-308/01/11 15:0010.0
Dibenzofuran ND ug/L 1 08/05/11 14:55 132-64-908/01/11 15:0010.0
1,2-Dichlorobenzene ND ug/L 1 08/05/11 14:55 95-50-108/01/11 15:0010.0
1,3-Dichlorobenzene ND ug/L 1 08/05/11 14:55 541-73-108/01/11 15:0010.0
1,4-Dichlorobenzene ND ug/L 1 08/05/11 14:55 106-46-708/01/11 15:0010.0
3,3'-Dichlorobenzidine ND ug/L 1 08/05/11 14:55 91-94-108/01/11 15:0020.0
2,4-Dichlorophenol ND ug/L 1 08/05/11 14:55 120-83-208/01/11 15:0010.0
Diethylphthalate ND ug/L 1 08/05/11 14:55 84-66-208/01/11 15:0010.0
2,4-Dimethylphenol ND ug/L 1 08/05/11 14:55 105-67-908/01/11 15:0010.0
Dimethylphthalate ND ug/L 1 08/05/11 14:55 131-11-308/01/11 15:0010.0
Di-n-butylphthalate ND ug/L 1 08/05/11 14:55 84-74-208/01/11 15:0010.0
4,6-Dinitro-2-methylphenol ND ug/L 1 08/05/11 14:55 534-52-108/01/11 15:0020.0
2,4-Dinitrophenol ND ug/L 1 08/05/11 14:55 51-28-508/01/11 15:0050.0
2,4-Dinitrotoluene ND ug/L 1 08/05/11 14:55 121-14-208/01/11 15:0010.0
2,6-Dinitrotoluene ND ug/L 1 08/05/11 14:55 606-20-208/01/11 15:0010.0
Di-n-octylphthalate ND ug/L 1 08/05/11 14:55 117-84-008/01/11 15:0010.0
bis(2-Ethylhexyl)phthalate ND ug/L 1 08/05/11 14:55 117-81-708/01/11 15:006.0
Fluoranthene ND ug/L 1 08/05/11 14:55 206-44-008/01/11 15:0010.0
Fluorene ND ug/L 1 08/05/11 14:55 86-73-708/01/11 15:0010.0
Hexachloro-1,3-butadiene ND ug/L 1 08/05/11 14:55 87-68-308/01/11 15:0010.0
Hexachlorobenzene ND ug/L 1 08/05/11 14:55 118-74-108/01/11 15:0010.0
Hexachlorocyclopentadiene ND ug/L 1 08/05/11 14:55 77-47-408/01/11 15:0010.0
Hexachloroethane ND ug/L 1 08/05/11 14:55 67-72-108/01/11 15:0010.0
Indeno(1,2,3-cd)pyrene ND ug/L 1 08/05/11 14:55 193-39-508/01/11 15:0010.0
Isophorone ND ug/L 1 08/05/11 14:55 78-59-108/01/11 15:0010.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 42 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-26 Lab ID:9299302011 Collected:07/28/11 10:45 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
1-Methylnaphthalene ND ug/L 1 08/05/11 14:55 90-12-008/01/11 15:0010.0
2-Methylnaphthalene ND ug/L 1 08/05/11 14:55 91-57-608/01/11 15:0010.0
2-Methylphenol(o-Cresol)ND ug/L 1 08/05/11 14:55 95-48-708/01/11 15:0010.0
3&4-Methylphenol(m&p Cresol)ND ug/L 1 08/05/11 14:5508/01/11 15:0010.0
Naphthalene ND ug/L 1 08/05/11 14:55 91-20-308/01/11 15:0010.0
2-Nitroaniline ND ug/L 1 08/05/11 14:55 88-74-408/01/11 15:0050.0
3-Nitroaniline ND ug/L 1 08/05/11 14:55 99-09-208/01/11 15:0050.0
4-Nitroaniline ND ug/L 1 08/05/11 14:55 100-01-608/01/11 15:0020.0
Nitrobenzene ND ug/L 1 08/05/11 14:55 98-95-308/01/11 15:0010.0
2-Nitrophenol ND ug/L 1 08/05/11 14:55 88-75-508/01/11 15:0010.0
4-Nitrophenol ND ug/L 1 08/05/11 14:55 100-02-708/01/11 15:0050.0
N-Nitrosodimethylamine ND ug/L 1 08/05/11 14:55 62-75-908/01/11 15:0010.0
N-Nitroso-di-n-propylamine ND ug/L 1 08/05/11 14:55 621-64-708/01/11 15:0010.0
N-Nitrosodiphenylamine ND ug/L 1 08/05/11 14:55 86-30-608/01/11 15:0010.0
Pentachlorophenol ND ug/L 1 08/05/11 14:55 87-86-508/01/11 15:0025.0
Phenanthrene ND ug/L 1 08/05/11 14:55 85-01-808/01/11 15:0010.0
Phenol ND ug/L 1 08/05/11 14:55 108-95-208/01/11 15:0010.0
Pyrene ND ug/L 1 08/05/11 14:55 129-00-008/01/11 15:0010.0
1,2,4-Trichlorobenzene ND ug/L 1 08/05/11 14:55 120-82-108/01/11 15:0010.0
2,4,5-Trichlorophenol ND ug/L 1 08/05/11 14:55 95-95-408/01/11 15:0010.0
2,4,6-Trichlorophenol ND ug/L 1 08/05/11 14:55 88-06-208/01/11 15:0010.0
Nitrobenzene-d5 (S)63 %1 08/05/11 14:55 4165-60-008/01/11 15:0021-110
2-Fluorobiphenyl (S)65 %1 08/05/11 14:55 321-60-808/01/11 15:0027-110
Terphenyl-d14 (S)69 %1 08/05/11 14:55 1718-51-008/01/11 15:0031-107
Phenol-d6 (S)39 %1 08/05/11 14:55 13127-88-308/01/11 15:0010-110
2-Fluorophenol (S)48 %1 08/05/11 14:55 367-12-408/01/11 15:0012-110
2,4,6-Tribromophenol (S)65 %1 08/05/11 14:55 118-79-608/01/11 15:0027-110
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 08/02/11 22:38 67-64-125.0
Benzene ND ug/L 1 08/02/11 22:38 71-43-21.0
Bromobenzene ND ug/L 1 08/02/11 22:38 108-86-11.0
Bromochloromethane ND ug/L 1 08/02/11 22:38 74-97-51.0
Bromodichloromethane ND ug/L 1 08/02/11 22:38 75-27-41.0
Bromoform ND ug/L 1 08/02/11 22:38 75-25-21.0
Bromomethane ND ug/L 1 08/02/11 22:38 74-83-92.0
2-Butanone (MEK)ND ug/L 1 08/02/11 22:38 78-93-35.0
Carbon tetrachloride ND ug/L 1 08/02/11 22:38 56-23-51.0
Chlorobenzene ND ug/L 1 08/02/11 22:38 108-90-71.0
Chloroethane ND ug/L 1 08/02/11 22:38 75-00-31.0
Chloroform ND ug/L 1 08/02/11 22:38 67-66-31.0
Chloromethane ND ug/L 1 08/02/11 22:38 74-87-31.0
2-Chlorotoluene ND ug/L 1 08/02/11 22:38 95-49-81.0
4-Chlorotoluene ND ug/L 1 08/02/11 22:38 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 08/02/11 22:38 96-12-85.0
Dibromochloromethane ND ug/L 1 08/02/11 22:38 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 08/02/11 22:38 106-93-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 43 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-26 Lab ID:9299302011 Collected:07/28/11 10:45 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Dibromomethane ND ug/L 1 08/02/11 22:38 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 08/02/11 22:38 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 08/02/11 22:38 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 08/02/11 22:38 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 08/02/11 22:38 75-71-81.0
1,1-Dichloroethane ND ug/L 1 08/02/11 22:38 75-34-31.0
1,2-Dichloroethane ND ug/L 1 08/02/11 22:38 107-06-21.0
1,1-Dichloroethene ND ug/L 1 08/02/11 22:38 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 08/02/11 22:38 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 08/02/11 22:38 156-60-51.0
1,2-Dichloropropane ND ug/L 1 08/02/11 22:38 78-87-51.0
1,3-Dichloropropane ND ug/L 1 08/02/11 22:38 142-28-91.0
2,2-Dichloropropane ND ug/L 1 08/02/11 22:38 594-20-71.0
1,1-Dichloropropene ND ug/L 1 08/02/11 22:38 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 08/02/11 22:38 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 08/02/11 22:38 10061-02-61.0
Diisopropyl ether ND ug/L 1 08/02/11 22:38 108-20-31.0
Ethylbenzene ND ug/L 1 08/02/11 22:38 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 08/02/11 22:38 87-68-31.0
2-Hexanone ND ug/L 1 08/02/11 22:38 591-78-65.0
p-Isopropyltoluene ND ug/L 1 08/02/11 22:38 99-87-61.0
Methylene Chloride ND ug/L 1 08/02/11 22:38 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 08/02/11 22:38 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 08/02/11 22:38 1634-04-41.0
Naphthalene ND ug/L 1 08/02/11 22:38 91-20-31.0
Styrene ND ug/L 1 08/02/11 22:38 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 08/02/11 22:38 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 08/02/11 22:38 79-34-51.0
Tetrachloroethene ND ug/L 1 08/02/11 22:38 127-18-41.0
Toluene ND ug/L 1 08/02/11 22:38 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 08/02/11 22:38 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 08/02/11 22:38 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 08/02/11 22:38 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 08/02/11 22:38 79-00-51.0
Trichloroethene ND ug/L 1 08/02/11 22:38 79-01-61.0
Trichlorofluoromethane ND ug/L 1 08/02/11 22:38 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 08/02/11 22:38 96-18-41.0
Vinyl acetate ND ug/L 1 08/02/11 22:38 108-05-42.0
Vinyl chloride ND ug/L 1 08/02/11 22:38 75-01-41.0
Xylene (Total)ND ug/L 1 08/02/11 22:38 1330-20-72.0
m&p-Xylene ND ug/L 1 08/02/11 22:38 179601-23-12.0
o-Xylene ND ug/L 1 08/02/11 22:38 95-47-61.0
4-Bromofluorobenzene (S)96 %1 08/02/11 22:38 460-00-470-130
Dibromofluoromethane (S)106 %1 08/02/11 22:38 1868-53-770-130
1,2-Dichloroethane-d4 (S)107 %1 08/02/11 22:38 17060-07-070-130
Toluene-d8 (S)100 %1 08/02/11 22:38 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 44 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-27 Lab ID:9299302012 Collected:07/28/11 11:45 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 08/05/11 15:22 83-32-908/01/11 15:0010.0
Acenaphthylene ND ug/L 1 08/05/11 15:22 208-96-808/01/11 15:0010.0
Aniline ND ug/L 1 08/05/11 15:22 62-53-308/01/11 15:0010.0
Anthracene ND ug/L 1 08/05/11 15:22 120-12-708/01/11 15:0010.0
Benzo(a)anthracene ND ug/L 1 08/05/11 15:22 56-55-308/01/11 15:0010.0
Benzo(a)pyrene ND ug/L 1 08/05/11 15:22 50-32-808/01/11 15:0010.0
Benzo(b)fluoranthene ND ug/L 1 08/05/11 15:22 205-99-208/01/11 15:0010.0
Benzo(g,h,i)perylene ND ug/L 1 08/05/11 15:22 191-24-208/01/11 15:0010.0
Benzo(k)fluoranthene ND ug/L 1 08/05/11 15:22 207-08-908/01/11 15:0010.0
Benzoic Acid ND ug/L 1 08/05/11 15:22 65-85-008/01/11 15:0050.0
Benzyl alcohol ND ug/L 1 08/05/11 15:22 100-51-608/01/11 15:0020.0
4-Bromophenylphenyl ether ND ug/L 1 08/05/11 15:22 101-55-308/01/11 15:0010.0
Butylbenzylphthalate ND ug/L 1 08/05/11 15:22 85-68-708/01/11 15:0010.0
4-Chloro-3-methylphenol ND ug/L 1 08/05/11 15:22 59-50-708/01/11 15:0020.0
4-Chloroaniline ND ug/L 1 08/05/11 15:22 106-47-808/01/11 15:0020.0
bis(2-Chloroethoxy)methane ND ug/L 1 08/05/11 15:22 111-91-108/01/11 15:0010.0
bis(2-Chloroethyl) ether ND ug/L 1 08/05/11 15:22 111-44-408/01/11 15:0010.0
bis(2-Chloroisopropyl) ether ND ug/L 1 08/05/11 15:22 108-60-108/01/11 15:0010.0
2-Chloronaphthalene ND ug/L 1 08/05/11 15:22 91-58-708/01/11 15:0010.0
2-Chlorophenol ND ug/L 1 08/05/11 15:22 95-57-808/01/11 15:0010.0
4-Chlorophenylphenyl ether ND ug/L 1 08/05/11 15:22 7005-72-308/01/11 15:0010.0
Chrysene ND ug/L 1 08/05/11 15:22 218-01-908/01/11 15:0010.0
Dibenz(a,h)anthracene ND ug/L 1 08/05/11 15:22 53-70-308/01/11 15:0010.0
Dibenzofuran ND ug/L 1 08/05/11 15:22 132-64-908/01/11 15:0010.0
1,2-Dichlorobenzene ND ug/L 1 08/05/11 15:22 95-50-108/01/11 15:0010.0
1,3-Dichlorobenzene ND ug/L 1 08/05/11 15:22 541-73-108/01/11 15:0010.0
1,4-Dichlorobenzene ND ug/L 1 08/05/11 15:22 106-46-708/01/11 15:0010.0
3,3'-Dichlorobenzidine ND ug/L 1 08/05/11 15:22 91-94-108/01/11 15:0020.0
2,4-Dichlorophenol ND ug/L 1 08/05/11 15:22 120-83-208/01/11 15:0010.0
Diethylphthalate ND ug/L 1 08/05/11 15:22 84-66-208/01/11 15:0010.0
2,4-Dimethylphenol ND ug/L 1 08/05/11 15:22 105-67-908/01/11 15:0010.0
Dimethylphthalate ND ug/L 1 08/05/11 15:22 131-11-308/01/11 15:0010.0
Di-n-butylphthalate ND ug/L 1 08/05/11 15:22 84-74-208/01/11 15:0010.0
4,6-Dinitro-2-methylphenol ND ug/L 1 08/05/11 15:22 534-52-108/01/11 15:0020.0
2,4-Dinitrophenol ND ug/L 1 08/05/11 15:22 51-28-508/01/11 15:0050.0
2,4-Dinitrotoluene ND ug/L 1 08/05/11 15:22 121-14-208/01/11 15:0010.0
2,6-Dinitrotoluene ND ug/L 1 08/05/11 15:22 606-20-208/01/11 15:0010.0
Di-n-octylphthalate ND ug/L 1 08/05/11 15:22 117-84-008/01/11 15:0010.0
bis(2-Ethylhexyl)phthalate ND ug/L 1 08/05/11 15:22 117-81-708/01/11 15:006.0
Fluoranthene ND ug/L 1 08/05/11 15:22 206-44-008/01/11 15:0010.0
Fluorene ND ug/L 1 08/05/11 15:22 86-73-708/01/11 15:0010.0
Hexachloro-1,3-butadiene ND ug/L 1 08/05/11 15:22 87-68-308/01/11 15:0010.0
Hexachlorobenzene ND ug/L 1 08/05/11 15:22 118-74-108/01/11 15:0010.0
Hexachlorocyclopentadiene ND ug/L 1 08/05/11 15:22 77-47-408/01/11 15:0010.0
Hexachloroethane ND ug/L 1 08/05/11 15:22 67-72-108/01/11 15:0010.0
Indeno(1,2,3-cd)pyrene ND ug/L 1 08/05/11 15:22 193-39-508/01/11 15:0010.0
Isophorone ND ug/L 1 08/05/11 15:22 78-59-108/01/11 15:0010.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 45 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-27 Lab ID:9299302012 Collected:07/28/11 11:45 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
1-Methylnaphthalene ND ug/L 1 08/05/11 15:22 90-12-008/01/11 15:0010.0
2-Methylnaphthalene ND ug/L 1 08/05/11 15:22 91-57-608/01/11 15:0010.0
2-Methylphenol(o-Cresol)ND ug/L 1 08/05/11 15:22 95-48-708/01/11 15:0010.0
3&4-Methylphenol(m&p Cresol)ND ug/L 1 08/05/11 15:2208/01/11 15:0010.0
Naphthalene ND ug/L 1 08/05/11 15:22 91-20-308/01/11 15:0010.0
2-Nitroaniline ND ug/L 1 08/05/11 15:22 88-74-408/01/11 15:0050.0
3-Nitroaniline ND ug/L 1 08/05/11 15:22 99-09-208/01/11 15:0050.0
4-Nitroaniline ND ug/L 1 08/05/11 15:22 100-01-608/01/11 15:0020.0
Nitrobenzene ND ug/L 1 08/05/11 15:22 98-95-308/01/11 15:0010.0
2-Nitrophenol ND ug/L 1 08/05/11 15:22 88-75-508/01/11 15:0010.0
4-Nitrophenol ND ug/L 1 08/05/11 15:22 100-02-708/01/11 15:0050.0
N-Nitrosodimethylamine ND ug/L 1 08/05/11 15:22 62-75-908/01/11 15:0010.0
N-Nitroso-di-n-propylamine ND ug/L 1 08/05/11 15:22 621-64-708/01/11 15:0010.0
N-Nitrosodiphenylamine ND ug/L 1 08/05/11 15:22 86-30-608/01/11 15:0010.0
Pentachlorophenol ND ug/L 1 08/05/11 15:22 87-86-508/01/11 15:0025.0
Phenanthrene ND ug/L 1 08/05/11 15:22 85-01-808/01/11 15:0010.0
Phenol ND ug/L 1 08/05/11 15:22 108-95-208/01/11 15:0010.0
Pyrene ND ug/L 1 08/05/11 15:22 129-00-008/01/11 15:0010.0
1,2,4-Trichlorobenzene ND ug/L 1 08/05/11 15:22 120-82-108/01/11 15:0010.0
2,4,5-Trichlorophenol ND ug/L 1 08/05/11 15:22 95-95-408/01/11 15:0010.0
2,4,6-Trichlorophenol ND ug/L 1 08/05/11 15:22 88-06-208/01/11 15:0010.0
Nitrobenzene-d5 (S)59 %1 08/05/11 15:22 4165-60-008/01/11 15:0021-110
2-Fluorobiphenyl (S)60 %1 08/05/11 15:22 321-60-808/01/11 15:0027-110
Terphenyl-d14 (S)73 %1 08/05/11 15:22 1718-51-008/01/11 15:0031-107
Phenol-d6 (S)42 %1 08/05/11 15:22 13127-88-308/01/11 15:0010-110
2-Fluorophenol (S)46 %1 08/05/11 15:22 367-12-408/01/11 15:0012-110
2,4,6-Tribromophenol (S)60 %1 08/05/11 15:22 118-79-608/01/11 15:0027-110
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 08/02/11 23:02 67-64-125.0
Benzene ND ug/L 1 08/02/11 23:02 71-43-21.0
Bromobenzene ND ug/L 1 08/02/11 23:02 108-86-11.0
Bromochloromethane ND ug/L 1 08/02/11 23:02 74-97-51.0
Bromodichloromethane ND ug/L 1 08/02/11 23:02 75-27-41.0
Bromoform ND ug/L 1 08/02/11 23:02 75-25-21.0
Bromomethane ND ug/L 1 08/02/11 23:02 74-83-92.0
2-Butanone (MEK)ND ug/L 1 08/02/11 23:02 78-93-35.0
Carbon tetrachloride ND ug/L 1 08/02/11 23:02 56-23-51.0
Chlorobenzene ND ug/L 1 08/02/11 23:02 108-90-71.0
Chloroethane ND ug/L 1 08/02/11 23:02 75-00-31.0
Chloroform ND ug/L 1 08/02/11 23:02 67-66-31.0
Chloromethane ND ug/L 1 08/02/11 23:02 74-87-31.0
2-Chlorotoluene ND ug/L 1 08/02/11 23:02 95-49-81.0
4-Chlorotoluene ND ug/L 1 08/02/11 23:02 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 08/02/11 23:02 96-12-85.0
Dibromochloromethane ND ug/L 1 08/02/11 23:02 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 08/02/11 23:02 106-93-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 46 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-27 Lab ID:9299302012 Collected:07/28/11 11:45 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Dibromomethane ND ug/L 1 08/02/11 23:02 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 08/02/11 23:02 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 08/02/11 23:02 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 08/02/11 23:02 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 08/02/11 23:02 75-71-81.0
1,1-Dichloroethane ND ug/L 1 08/02/11 23:02 75-34-31.0
1,2-Dichloroethane ND ug/L 1 08/02/11 23:02 107-06-21.0
1,1-Dichloroethene ND ug/L 1 08/02/11 23:02 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 08/02/11 23:02 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 08/02/11 23:02 156-60-51.0
1,2-Dichloropropane ND ug/L 1 08/02/11 23:02 78-87-51.0
1,3-Dichloropropane ND ug/L 1 08/02/11 23:02 142-28-91.0
2,2-Dichloropropane ND ug/L 1 08/02/11 23:02 594-20-71.0
1,1-Dichloropropene ND ug/L 1 08/02/11 23:02 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 08/02/11 23:02 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 08/02/11 23:02 10061-02-61.0
Diisopropyl ether ND ug/L 1 08/02/11 23:02 108-20-31.0
Ethylbenzene ND ug/L 1 08/02/11 23:02 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 08/02/11 23:02 87-68-31.0
2-Hexanone ND ug/L 1 08/02/11 23:02 591-78-65.0
p-Isopropyltoluene ND ug/L 1 08/02/11 23:02 99-87-61.0
Methylene Chloride ND ug/L 1 08/02/11 23:02 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 08/02/11 23:02 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 08/02/11 23:02 1634-04-41.0
Naphthalene ND ug/L 1 08/02/11 23:02 91-20-31.0
Styrene ND ug/L 1 08/02/11 23:02 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 08/02/11 23:02 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 08/02/11 23:02 79-34-51.0
Tetrachloroethene ND ug/L 1 08/02/11 23:02 127-18-41.0
Toluene ND ug/L 1 08/02/11 23:02 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 08/02/11 23:02 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 08/02/11 23:02 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 08/02/11 23:02 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 08/02/11 23:02 79-00-51.0
Trichloroethene ND ug/L 1 08/02/11 23:02 79-01-61.0
Trichlorofluoromethane ND ug/L 1 08/02/11 23:02 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 08/02/11 23:02 96-18-41.0
Vinyl acetate ND ug/L 1 08/02/11 23:02 108-05-42.0
Vinyl chloride ND ug/L 1 08/02/11 23:02 75-01-41.0
Xylene (Total)ND ug/L 1 08/02/11 23:02 1330-20-72.0
m&p-Xylene ND ug/L 1 08/02/11 23:02 179601-23-12.0
o-Xylene ND ug/L 1 08/02/11 23:02 95-47-61.0
4-Bromofluorobenzene (S)95 %1 08/02/11 23:02 460-00-470-130
Dibromofluoromethane (S)103 %1 08/02/11 23:02 1868-53-770-130
1,2-Dichloroethane-d4 (S)105 %1 08/02/11 23:02 17060-07-070-130
Toluene-d8 (S)101 %1 08/02/11 23:02 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 47 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-17 Lab ID:9299302015 Collected:07/28/11 15:45 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 08/05/11 15:49 83-32-908/01/11 15:0010.0
Acenaphthylene ND ug/L 1 08/05/11 15:49 208-96-808/01/11 15:0010.0
Aniline ND ug/L 1 08/05/11 15:49 62-53-308/01/11 15:0010.0
Anthracene ND ug/L 1 08/05/11 15:49 120-12-708/01/11 15:0010.0
Benzo(a)anthracene ND ug/L 1 08/05/11 15:49 56-55-308/01/11 15:0010.0
Benzo(a)pyrene ND ug/L 1 08/05/11 15:49 50-32-808/01/11 15:0010.0
Benzo(b)fluoranthene ND ug/L 1 08/05/11 15:49 205-99-208/01/11 15:0010.0
Benzo(g,h,i)perylene ND ug/L 1 08/05/11 15:49 191-24-208/01/11 15:0010.0
Benzo(k)fluoranthene ND ug/L 1 08/05/11 15:49 207-08-908/01/11 15:0010.0
Benzoic Acid ND ug/L 1 08/05/11 15:49 65-85-008/01/11 15:0050.0
Benzyl alcohol ND ug/L 1 08/05/11 15:49 100-51-608/01/11 15:0020.0
4-Bromophenylphenyl ether ND ug/L 1 08/05/11 15:49 101-55-308/01/11 15:0010.0
Butylbenzylphthalate ND ug/L 1 08/05/11 15:49 85-68-708/01/11 15:0010.0
4-Chloro-3-methylphenol ND ug/L 1 08/05/11 15:49 59-50-708/01/11 15:0020.0
4-Chloroaniline ND ug/L 1 08/05/11 15:49 106-47-808/01/11 15:0020.0
bis(2-Chloroethoxy)methane ND ug/L 1 08/05/11 15:49 111-91-108/01/11 15:0010.0
bis(2-Chloroethyl) ether ND ug/L 1 08/05/11 15:49 111-44-408/01/11 15:0010.0
bis(2-Chloroisopropyl) ether ND ug/L 1 08/05/11 15:49 108-60-108/01/11 15:0010.0
2-Chloronaphthalene ND ug/L 1 08/05/11 15:49 91-58-708/01/11 15:0010.0
2-Chlorophenol ND ug/L 1 08/05/11 15:49 95-57-808/01/11 15:0010.0
4-Chlorophenylphenyl ether ND ug/L 1 08/05/11 15:49 7005-72-308/01/11 15:0010.0
Chrysene ND ug/L 1 08/05/11 15:49 218-01-908/01/11 15:0010.0
Dibenz(a,h)anthracene ND ug/L 1 08/05/11 15:49 53-70-308/01/11 15:0010.0
Dibenzofuran ND ug/L 1 08/05/11 15:49 132-64-908/01/11 15:0010.0
1,2-Dichlorobenzene ND ug/L 1 08/05/11 15:49 95-50-108/01/11 15:0010.0
1,3-Dichlorobenzene ND ug/L 1 08/05/11 15:49 541-73-108/01/11 15:0010.0
1,4-Dichlorobenzene ND ug/L 1 08/05/11 15:49 106-46-708/01/11 15:0010.0
3,3'-Dichlorobenzidine ND ug/L 1 08/05/11 15:49 91-94-108/01/11 15:0020.0
2,4-Dichlorophenol ND ug/L 1 08/05/11 15:49 120-83-208/01/11 15:0010.0
Diethylphthalate ND ug/L 1 08/05/11 15:49 84-66-208/01/11 15:0010.0
2,4-Dimethylphenol ND ug/L 1 08/05/11 15:49 105-67-908/01/11 15:0010.0
Dimethylphthalate ND ug/L 1 08/05/11 15:49 131-11-308/01/11 15:0010.0
Di-n-butylphthalate ND ug/L 1 08/05/11 15:49 84-74-208/01/11 15:0010.0
4,6-Dinitro-2-methylphenol ND ug/L 1 08/05/11 15:49 534-52-108/01/11 15:0020.0
2,4-Dinitrophenol ND ug/L 1 08/05/11 15:49 51-28-508/01/11 15:0050.0
2,4-Dinitrotoluene ND ug/L 1 08/05/11 15:49 121-14-208/01/11 15:0010.0
2,6-Dinitrotoluene ND ug/L 1 08/05/11 15:49 606-20-208/01/11 15:0010.0
Di-n-octylphthalate ND ug/L 1 08/05/11 15:49 117-84-008/01/11 15:0010.0
bis(2-Ethylhexyl)phthalate ND ug/L 1 08/05/11 15:49 117-81-708/01/11 15:006.0
Fluoranthene ND ug/L 1 08/05/11 15:49 206-44-008/01/11 15:0010.0
Fluorene ND ug/L 1 08/05/11 15:49 86-73-708/01/11 15:0010.0
Hexachloro-1,3-butadiene ND ug/L 1 08/05/11 15:49 87-68-308/01/11 15:0010.0
Hexachlorobenzene ND ug/L 1 08/05/11 15:49 118-74-108/01/11 15:0010.0
Hexachlorocyclopentadiene ND ug/L 1 08/05/11 15:49 77-47-408/01/11 15:0010.0
Hexachloroethane ND ug/L 1 08/05/11 15:49 67-72-108/01/11 15:0010.0
Indeno(1,2,3-cd)pyrene ND ug/L 1 08/05/11 15:49 193-39-508/01/11 15:0010.0
Isophorone ND ug/L 1 08/05/11 15:49 78-59-108/01/11 15:0010.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 48 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-17 Lab ID:9299302015 Collected:07/28/11 15:45 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
1-Methylnaphthalene ND ug/L 1 08/05/11 15:49 90-12-008/01/11 15:0010.0
2-Methylnaphthalene ND ug/L 1 08/05/11 15:49 91-57-608/01/11 15:0010.0
2-Methylphenol(o-Cresol)ND ug/L 1 08/05/11 15:49 95-48-708/01/11 15:0010.0
3&4-Methylphenol(m&p Cresol)ND ug/L 1 08/05/11 15:4908/01/11 15:0010.0
Naphthalene ND ug/L 1 08/05/11 15:49 91-20-308/01/11 15:0010.0
2-Nitroaniline ND ug/L 1 08/05/11 15:49 88-74-408/01/11 15:0050.0
3-Nitroaniline ND ug/L 1 08/05/11 15:49 99-09-208/01/11 15:0050.0
4-Nitroaniline ND ug/L 1 08/05/11 15:49 100-01-608/01/11 15:0020.0
Nitrobenzene ND ug/L 1 08/05/11 15:49 98-95-308/01/11 15:0010.0
2-Nitrophenol ND ug/L 1 08/05/11 15:49 88-75-508/01/11 15:0010.0
4-Nitrophenol ND ug/L 1 08/05/11 15:49 100-02-708/01/11 15:0050.0
N-Nitrosodimethylamine ND ug/L 1 08/05/11 15:49 62-75-908/01/11 15:0010.0
N-Nitroso-di-n-propylamine ND ug/L 1 08/05/11 15:49 621-64-708/01/11 15:0010.0
N-Nitrosodiphenylamine ND ug/L 1 08/05/11 15:49 86-30-608/01/11 15:0010.0
Pentachlorophenol ND ug/L 1 08/05/11 15:49 87-86-508/01/11 15:0025.0
Phenanthrene ND ug/L 1 08/05/11 15:49 85-01-808/01/11 15:0010.0
Phenol ND ug/L 1 08/05/11 15:49 108-95-208/01/11 15:0010.0
Pyrene ND ug/L 1 08/05/11 15:49 129-00-008/01/11 15:0010.0
1,2,4-Trichlorobenzene ND ug/L 1 08/05/11 15:49 120-82-108/01/11 15:0010.0
2,4,5-Trichlorophenol ND ug/L 1 08/05/11 15:49 95-95-408/01/11 15:0010.0
2,4,6-Trichlorophenol ND ug/L 1 08/05/11 15:49 88-06-208/01/11 15:0010.0
Nitrobenzene-d5 (S)56 %1 08/05/11 15:49 4165-60-008/01/11 15:0021-110
2-Fluorobiphenyl (S)54 %1 08/05/11 15:49 321-60-808/01/11 15:0027-110
Terphenyl-d14 (S)73 %1 08/05/11 15:49 1718-51-008/01/11 15:0031-107
Phenol-d6 (S)34 %1 08/05/11 15:49 13127-88-308/01/11 15:0010-110
2-Fluorophenol (S)43 %1 08/05/11 15:49 367-12-408/01/11 15:0012-110
2,4,6-Tribromophenol (S)61 %1 08/05/11 15:49 118-79-608/01/11 15:0027-110
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 08/02/11 23:27 67-64-125.0
Benzene ND ug/L 1 08/02/11 23:27 71-43-21.0
Bromobenzene ND ug/L 1 08/02/11 23:27 108-86-11.0
Bromochloromethane ND ug/L 1 08/02/11 23:27 74-97-51.0
Bromodichloromethane ND ug/L 1 08/02/11 23:27 75-27-41.0
Bromoform ND ug/L 1 08/02/11 23:27 75-25-21.0
Bromomethane ND ug/L 1 08/02/11 23:27 74-83-92.0
2-Butanone (MEK)ND ug/L 1 08/02/11 23:27 78-93-35.0
Carbon tetrachloride ND ug/L 1 08/02/11 23:27 56-23-51.0
Chlorobenzene ND ug/L 1 08/02/11 23:27 108-90-71.0
Chloroethane ND ug/L 1 08/02/11 23:27 75-00-31.0
Chloroform ND ug/L 1 08/02/11 23:27 67-66-31.0
Chloromethane ND ug/L 1 08/02/11 23:27 74-87-31.0
2-Chlorotoluene ND ug/L 1 08/02/11 23:27 95-49-81.0
4-Chlorotoluene ND ug/L 1 08/02/11 23:27 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 08/02/11 23:27 96-12-85.0
Dibromochloromethane ND ug/L 1 08/02/11 23:27 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 08/02/11 23:27 106-93-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 49 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Sample:SB-17 Lab ID:9299302015 Collected:07/28/11 15:45 Received:07/29/11 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Dibromomethane ND ug/L 1 08/02/11 23:27 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 08/02/11 23:27 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 08/02/11 23:27 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 08/02/11 23:27 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 08/02/11 23:27 75-71-81.0
1,1-Dichloroethane ND ug/L 1 08/02/11 23:27 75-34-31.0
1,2-Dichloroethane ND ug/L 1 08/02/11 23:27 107-06-21.0
1,1-Dichloroethene ND ug/L 1 08/02/11 23:27 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 08/02/11 23:27 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 08/02/11 23:27 156-60-51.0
1,2-Dichloropropane ND ug/L 1 08/02/11 23:27 78-87-51.0
1,3-Dichloropropane ND ug/L 1 08/02/11 23:27 142-28-91.0
2,2-Dichloropropane ND ug/L 1 08/02/11 23:27 594-20-71.0
1,1-Dichloropropene ND ug/L 1 08/02/11 23:27 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 08/02/11 23:27 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 08/02/11 23:27 10061-02-61.0
Diisopropyl ether ND ug/L 1 08/02/11 23:27 108-20-31.0
Ethylbenzene ND ug/L 1 08/02/11 23:27 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 08/02/11 23:27 87-68-31.0
2-Hexanone ND ug/L 1 08/02/11 23:27 591-78-65.0
p-Isopropyltoluene ND ug/L 1 08/02/11 23:27 99-87-61.0
Methylene Chloride ND ug/L 1 08/02/11 23:27 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 08/02/11 23:27 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 08/02/11 23:27 1634-04-41.0
Naphthalene ND ug/L 1 08/02/11 23:27 91-20-31.0
Styrene ND ug/L 1 08/02/11 23:27 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 08/02/11 23:27 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 08/02/11 23:27 79-34-51.0
Tetrachloroethene ND ug/L 1 08/02/11 23:27 127-18-41.0
Toluene ND ug/L 1 08/02/11 23:27 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 08/02/11 23:27 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 08/02/11 23:27 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 08/02/11 23:27 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 08/02/11 23:27 79-00-51.0
Trichloroethene ND ug/L 1 08/02/11 23:27 79-01-61.0
Trichlorofluoromethane ND ug/L 1 08/02/11 23:27 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 08/02/11 23:27 96-18-41.0
Vinyl acetate ND ug/L 1 08/02/11 23:27 108-05-42.0
Vinyl chloride ND ug/L 1 08/02/11 23:27 75-01-41.0
Xylene (Total)ND ug/L 1 08/02/11 23:27 1330-20-72.0
m&p-Xylene ND ug/L 1 08/02/11 23:27 179601-23-12.0
o-Xylene ND ug/L 1 08/02/11 23:27 95-47-61.0
4-Bromofluorobenzene (S)96 %1 08/02/11 23:27 460-00-470-130
Dibromofluoromethane (S)107 %1 08/02/11 23:27 1868-53-770-130
1,2-Dichloroethane-d4 (S)106 %1 08/02/11 23:27 17060-07-070-130
Toluene-d8 (S)101 %1 08/02/11 23:27 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 50 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/8820
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:9299302001, 9299302002, 9299302003, 9299302004, 9299302005, 9299302006, 9299302007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:641217
Associated Lab Samples:9299302001, 9299302002, 9299302003, 9299302004, 9299302005, 9299302006, 9299302007
Matrix:Solid
Analyzed
Antimony mg/kg ND 0.50 08/02/11 14:20
Arsenic mg/kg ND 0.50 08/02/11 14:20
Beryllium mg/kg ND 0.10 08/02/11 14:20
Cadmium mg/kg ND 0.10 08/02/11 14:20
Chromium mg/kg ND 0.50 08/02/11 14:20
Copper mg/kg ND 0.50 08/02/11 14:20
Lead mg/kg ND 0.50 08/02/11 14:20
Manganese mg/kg ND 0.50 08/02/11 14:20
Nickel mg/kg ND 0.50 08/02/11 14:20
Selenium mg/kg ND 1.0 08/02/11 14:20
Silver mg/kg ND 0.50 08/02/11 14:20
Thallium mg/kg ND 1.0 08/02/11 14:20
Zinc mg/kg ND 1.0 08/02/11 14:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
641218LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony mg/kg 48.850 98 80-120
Arsenic mg/kg 49.450 99 80-120
Beryllium mg/kg 50.950 102 80-120
Cadmium mg/kg 49.950 100 80-120
Chromium mg/kg 50.850 102 80-120
Copper mg/kg 50.250 100 80-120
Lead mg/kg 50.850 102 80-120
Manganese mg/kg 50.350 101 80-120
Nickel mg/kg 50.250 100 80-120
Selenium mg/kg 49.550 99 80-120
Silver mg/kg 25.025 100 80-120
Thallium mg/kg 49.250 98 80-120
Zinc mg/kg 50.850 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
641219MATRIX SPIKE SAMPLE:
MSSpike
Result
9299254023
Antimony mg/kg 42.648.9 78 75-1254.2
Arsenic mg/kg 156 M148.9 249 75-12534.3
Beryllium mg/kg 44.348.9 90 75-1250.27
Cadmium mg/kg 54.948.9 76 75-12517.8
Chromium mg/kg 82.848.9 108 75-12530.1
Copper mg/kg 214 M148.9 47 75-125191
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 51 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
641219MATRIX SPIKE SAMPLE:
MSSpike
Result
9299254023
Lead mg/kg 324 M148.9 -134 75-125389
Manganese mg/kg 365 M148.9 229 75-125253
Nickel mg/kg 51.848.9 85 75-12510
Selenium mg/kg 44.248.9 87 75-1251.7
Silver mg/kg 24.424.4 98 75-125ND
Thallium mg/kg 36.1 M148.9 74 75-125ND
Zinc mg/kg 2600 M648.9 -1468 75-1253320
Parameter Units
Dup
Result QualifiersRPDResult
9299254024
641220SAMPLE DUPLICATE:
Antimony mg/kg 2.1 141.9
Arsenic mg/kg 50.1 D64830.9
Beryllium mg/kg 0.34 D6280.26
Cadmium mg/kg 4.5 D6562.6
Chromium mg/kg 44.9 D62734.3
Copper mg/kg 135 D63891.6
Lead mg/kg 242 D623192
Manganese mg/kg 215 12191
Nickel mg/kg 8.7 D6405.8
Selenium mg/kg NDND
Silver mg/kg .23JND
Thallium mg/kg NDND
Zinc mg/kg 1520 D643985
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 52 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/3649
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:9299302001, 9299302002, 9299302003, 9299302004, 9299302005, 9299302006, 9299302007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:641155
Associated Lab Samples:9299302001, 9299302002, 9299302003, 9299302004, 9299302005, 9299302006, 9299302007
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0050 08/03/11 12:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
641156LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.062.067 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
641157MATRIX SPIKE SAMPLE:
MSSpike
Result
9299302001
Mercury mg/kg 0.071 M1.077 67 75-1250.019
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
641159MATRIX SPIKE SAMPLE:
MSSpike
Result
9299306004
Mercury mg/kg 0.014 M1.079 2 75-1250.012
Parameter Units
Dup
Result QualifiersRPDResult
9299302002
641158SAMPLE DUPLICATE:
Mercury mg/kg 0.0074 D6650.014
Parameter Units
Dup
Result QualifiersRPDResult
9299306005
641160SAMPLE DUPLICATE:
Mercury mg/kg .0039J0.011
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 53 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/14362
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:9299302001, 9299302002, 9299302003, 9299302004, 9299302005, 9299302006, 9299302007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:640690
Associated Lab Samples:9299302001, 9299302002, 9299302003, 9299302004, 9299302005, 9299302006, 9299302007
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 08/03/11 10:59
1,2-Dichlorobenzene ug/kg ND 330 08/03/11 10:59
1,3-Dichlorobenzene ug/kg ND 330 08/03/11 10:59
1,4-Dichlorobenzene ug/kg ND 330 08/03/11 10:59
1-Methylnaphthalene ug/kg ND 330 08/03/11 10:59
2,4,5-Trichlorophenol ug/kg ND 330 08/03/11 10:59
2,4,6-Trichlorophenol ug/kg ND 330 08/03/11 10:59
2,4-Dichlorophenol ug/kg ND 330 08/03/11 10:59
2,4-Dimethylphenol ug/kg ND 330 08/03/11 10:59
2,4-Dinitrophenol ug/kg ND 1650 08/03/11 10:59
2,4-Dinitrotoluene ug/kg ND 330 08/03/11 10:59
2,6-Dinitrotoluene ug/kg ND 330 08/03/11 10:59
2-Chloronaphthalene ug/kg ND 330 08/03/11 10:59
2-Chlorophenol ug/kg ND 330 08/03/11 10:59
2-Methylnaphthalene ug/kg ND 330 08/03/11 10:59
2-Methylphenol(o-Cresol)ug/kg ND 330 08/03/11 10:59
2-Nitroaniline ug/kg ND 1650 08/03/11 10:59
2-Nitrophenol ug/kg ND 330 08/03/11 10:59
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 08/03/11 10:59
3,3'-Dichlorobenzidine ug/kg ND 1650 08/03/11 10:59
3-Nitroaniline ug/kg ND 1650 08/03/11 10:59
4,6-Dinitro-2-methylphenol ug/kg ND 660 08/03/11 10:59
4-Bromophenylphenyl ether ug/kg ND 330 08/03/11 10:59
4-Chloro-3-methylphenol ug/kg ND 660 08/03/11 10:59
4-Chloroaniline ug/kg ND 1650 08/03/11 10:59
4-Chlorophenylphenyl ether ug/kg ND 330 08/03/11 10:59
4-Nitroaniline ug/kg ND 660 08/03/11 10:59
4-Nitrophenol ug/kg ND 1650 08/03/11 10:59
Acenaphthene ug/kg ND 330 08/03/11 10:59
Acenaphthylene ug/kg ND 330 08/03/11 10:59
Aniline ug/kg ND 330 08/03/11 10:59
Anthracene ug/kg ND 330 08/03/11 10:59
Benzo(a)anthracene ug/kg ND 330 08/03/11 10:59
Benzo(a)pyrene ug/kg ND 330 08/03/11 10:59
Benzo(b)fluoranthene ug/kg ND 330 08/03/11 10:59
Benzo(g,h,i)perylene ug/kg ND 330 08/03/11 10:59
Benzo(k)fluoranthene ug/kg ND 330 08/03/11 10:59
Benzoic Acid ug/kg ND 1650 08/03/11 10:59
Benzyl alcohol ug/kg ND 660 08/03/11 10:59
bis(2-Chloroethoxy)methane ug/kg ND 330 08/03/11 10:59
bis(2-Chloroethyl) ether ug/kg ND 330 08/03/11 10:59
bis(2-Chloroisopropyl) ether ug/kg ND 330 08/03/11 10:59
bis(2-Ethylhexyl)phthalate ug/kg ND 330 08/03/11 10:59
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 54 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:640690
Associated Lab Samples:9299302001, 9299302002, 9299302003, 9299302004, 9299302005, 9299302006, 9299302007
Matrix:Solid
Analyzed
Butylbenzylphthalate ug/kg ND 330 08/03/11 10:59
Chrysene ug/kg ND 330 08/03/11 10:59
Di-n-butylphthalate ug/kg ND 330 08/03/11 10:59
Di-n-octylphthalate ug/kg ND 330 08/03/11 10:59
Dibenz(a,h)anthracene ug/kg ND 330 08/03/11 10:59
Dibenzofuran ug/kg ND 330 08/03/11 10:59
Diethylphthalate ug/kg ND 330 08/03/11 10:59
Dimethylphthalate ug/kg ND 330 08/03/11 10:59
Fluoranthene ug/kg ND 330 08/03/11 10:59
Fluorene ug/kg ND 330 08/03/11 10:59
Hexachloro-1,3-butadiene ug/kg ND 330 08/03/11 10:59
Hexachlorobenzene ug/kg ND 330 08/03/11 10:59
Hexachlorocyclopentadiene ug/kg ND 330 08/03/11 10:59
Hexachloroethane ug/kg ND 330 08/03/11 10:59
Indeno(1,2,3-cd)pyrene ug/kg ND 330 08/03/11 10:59
Isophorone ug/kg ND 330 08/03/11 10:59
N-Nitroso-di-n-propylamine ug/kg ND 330 08/03/11 10:59
N-Nitrosodimethylamine ug/kg ND 330 08/03/11 10:59
N-Nitrosodiphenylamine ug/kg ND 330 08/03/11 10:59
Naphthalene ug/kg ND 330 08/03/11 10:59
Nitrobenzene ug/kg ND 330 08/03/11 10:59
Pentachlorophenol ug/kg ND 1650 08/03/11 10:59
Phenanthrene ug/kg ND 330 08/03/11 10:59
Phenol ug/kg ND 330 08/03/11 10:59
Pyrene ug/kg ND 330 08/03/11 10:59
2,4,6-Tribromophenol (S)%57 27-110 08/03/11 10:59
2-Fluorobiphenyl (S)%59 30-110 08/03/11 10:59
2-Fluorophenol (S)%61 13-110 08/03/11 10:59
Nitrobenzene-d5 (S)%62 23-110 08/03/11 10:59
Phenol-d6 (S)%66 22-110 08/03/11 10:59
Terphenyl-d14 (S)%72 28-110 08/03/11 10:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640691LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 10601670 64 39-101
1,2-Dichlorobenzene ug/kg 11801670 71 36-110
1,3-Dichlorobenzene ug/kg 11601670 70 35-110
1,4-Dichlorobenzene ug/kg 11501670 69 35-110
1-Methylnaphthalene ug/kg 11901670 71 45-105
2,4,5-Trichlorophenol ug/kg 10901670 65 48-109
2,4,6-Trichlorophenol ug/kg 12701670 76 45-111
2,4-Dichlorophenol ug/kg 12301670 74 51-116
2,4-Dimethylphenol ug/kg 13301670 80 42-103
2,4-Dinitrophenol ug/kg 58208330 70 28-103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 55 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640691LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dinitrotoluene ug/kg 13801670 83 46-114
2,6-Dinitrotoluene ug/kg 13401670 81 48-112
2-Chloronaphthalene ug/kg 12201670 73 44-105
2-Chlorophenol ug/kg 12701670 76 36-110
2-Methylnaphthalene ug/kg 12101670 72 39-112
2-Methylphenol(o-Cresol)ug/kg 12301670 74 39-101
2-Nitroaniline ug/kg 30803330 92 44-111
2-Nitrophenol ug/kg 12501670 75 41-100
3&4-Methylphenol(m&p Cresol)ug/kg 12801670 77 43-103
3,3'-Dichlorobenzidine ug/kg 22503330 67 10-150
3-Nitroaniline ug/kg 27803330 84 35-110
4,6-Dinitro-2-methylphenol ug/kg 26603330 80 38-118
4-Bromophenylphenyl ether ug/kg 11001670 66 47-115
4-Chloro-3-methylphenol ug/kg 28203330 85 43-127
4-Chloroaniline ug/kg 25603330 77 34-109
4-Chlorophenylphenyl ether ug/kg 11901670 71 44-115
4-Nitroaniline ug/kg 29903330 90 37-111
4-Nitrophenol ug/kg 72508330 87 21-152
Acenaphthene ug/kg 12901670 77 38-117
Acenaphthylene ug/kg 12701670 76 46-107
Aniline ug/kg 11801670 71 29-110
Anthracene ug/kg 13701670 82 50-110
Benzo(a)anthracene ug/kg 13101670 79 47-116
Benzo(a)pyrene ug/kg 12901670 77 47-106
Benzo(b)fluoranthene ug/kg 12401670 75 47-109
Benzo(g,h,i)perylene ug/kg 11401670 69 39-115
Benzo(k)fluoranthene ug/kg 13201670 79 45-117
Benzoic Acid ug/kg 47308330 57 16-110
Benzyl alcohol ug/kg 27603330 83 38-105
bis(2-Chloroethoxy)methane ug/kg 12301670 74 39-110
bis(2-Chloroethyl) ether ug/kg 12201670 73 19-119
bis(2-Chloroisopropyl) ether ug/kg 12701670 76 21-110
bis(2-Ethylhexyl)phthalate ug/kg 16001670 96 35-116
Butylbenzylphthalate ug/kg 15801670 95 38-110
Chrysene ug/kg 13201670 79 49-110
Di-n-butylphthalate ug/kg 14501670 87 43-109
Di-n-octylphthalate ug/kg 15901670 95 37-109
Dibenz(a,h)anthracene ug/kg 11401670 69 43-116
Dibenzofuran ug/kg 12801670 77 45-106
Diethylphthalate ug/kg 13101670 79 41-114
Dimethylphthalate ug/kg 12301670 74 43-110
Fluoranthene ug/kg 13301670 80 50-114
Fluorene ug/kg 12601670 75 46-114
Hexachloro-1,3-butadiene ug/kg 9541670 57 28-111
Hexachlorobenzene ug/kg 10101670 60 46-120
Hexachlorocyclopentadiene ug/kg 10801670 65 18-119
Hexachloroethane ug/kg 11601670 70 33-110
Indeno(1,2,3-cd)pyrene ug/kg 11701670 70 42-115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 56 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640691LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/kg 13701670 82 44-109
N-Nitroso-di-n-propylamine ug/kg 13501670 81 43-104
N-Nitrosodimethylamine ug/kg 11901670 71 29-110
N-Nitrosodiphenylamine ug/kg 13201670 79 48-113
Naphthalene ug/kg 11601670 70 41-110
Nitrobenzene ug/kg 11901670 71 38-110
Pentachlorophenol ug/kg 25603330 77 32-128
Phenanthrene ug/kg 13001670 78 50-110
Phenol ug/kg 13301670 80 28-106
Pyrene ug/kg 13301670 80 45-114
2,4,6-Tribromophenol (S)%66 27-110
2-Fluorobiphenyl (S)%69 30-110
2-Fluorophenol (S)%74 13-110
Nitrobenzene-d5 (S)%70 23-110
Phenol-d6 (S)%82 22-110
Terphenyl-d14 (S)%76 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
640692MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299306001
640693
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1950 53 18-11962 161950ND10301210
1,2-Dichlorobenzene ug/kg 1950 57 50-11068 171950ND11201330
1,3-Dichlorobenzene ug/kg 1950 57 27-11068 171950ND11101320
1,4-Dichlorobenzene ug/kg 1950 57 28-11067 171950ND11101310
1-Methylnaphthalene ug/kg 1950 60 24-11667 111950ND11601300
2,4,5-Trichlorophenol ug/kg 1950 55 28-11062 121950ND10601200
2,4,6-Trichlorophenol ug/kg 1950 62 17-11768 101950ND12101330
2,4-Dichlorophenol ug/kg 1950 62 21-12870 131950ND12001370
2,4-Dimethylphenol ug/kg 1950 65 10-12075 141950ND12701460
2,4-Dinitrophenol ug/kg 9720 48 10-10753 99720ND47105160
2,4-Dinitrotoluene ug/kg 1950 71 36-10978 101950ND13801530
2,6-Dinitrotoluene ug/kg 1950 69 32-11076 101950ND13401470
2-Chloronaphthalene ug/kg 1950 61 30-10769 121950ND11901350
2-Chlorophenol ug/kg 1950 61 14-10673 181950ND11801420
2-Methylnaphthalene ug/kg 1950 61 10-13568 111950ND11801320
2-Methylphenol(o-Cresol)ug/kg 1950 58 10-12468 161950ND11201330
2-Nitroaniline ug/kg 3890 78 26-11688 123890ND30303420
2-Nitrophenol ug/kg 1950 57 28-10369 201950ND11101350
3&4-Methylphenol(m&p
Cresol)ug/kg 1950 62 10-10972 161950ND12001410
3,3'-Dichlorobenzidine ug/kg 3890 60 10-15066 93890ND23302560
3-Nitroaniline ug/kg 3890 71 22-11078 93890ND27603020
4,6-Dinitro-2-methylphenol ug/kg 3890 67 13-12174 103890ND25902870
4-Bromophenylphenyl ether ug/kg 1950 55 31-10961 111950ND10701190
4-Chloro-3-methylphenol ug/kg 3890 70 13-12879 123890ND27203060
4-Chloroaniline ug/kg 3890 63 18-10270 113890ND24602740
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 57 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
640692MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299306001
640693
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
4-Chlorophenylphenyl ether ug/kg 1950 60 29-11266 101950ND11601290
4-Nitroaniline ug/kg 3890 79 16-11186 73890ND30903330
4-Nitrophenol ug/kg 9720 76 14-13581 79720ND73907920
Acenaphthene ug/kg 1950 65 26-11471 81950ND12701380
Acenaphthylene ug/kg 1950 64 32-10871 101950ND12501380
Aniline ug/kg 1950 52 10-10764 201950ND10201250
Anthracene ug/kg 1950 71 32-11175 51950ND13901470
Benzo(a)anthracene ug/kg 1950 64 25-11770 91950ND12501370
Benzo(a)pyrene ug/kg 1950 61 25-10668 111950ND11901330
Benzo(b)fluoranthene ug/kg 1950 61 24-11070 141950ND11801360
Benzo(g,h,i)perylene ug/kg 1950 55 19-11263 131950ND10701220
Benzo(k)fluoranthene ug/kg 1950 61 24-11468 101950ND12001320
Benzoic Acid ug/kg M0,M19720910-110109720ND894J968J
Benzyl alcohol ug/kg 3890 65 24-10677 173890ND25302990
bis(2-Chloroethoxy)methane ug/kg 1950 59 13-11968 141950ND11401320
bis(2-Chloroethyl) ether ug/kg 1950 59 10-13469 161950ND11401330
bis(2-Chloroisopropyl) ether ug/kg 1950 61 10-11374 191950ND11801430
bis(2-Ethylhexyl)phthalate ug/kg 1950 74 10-12584 131950ND14301640
Butylbenzylphthalate ug/kg 1950 75 18-11085 121950ND14601650
Chrysene ug/kg 1950 65 30-11071 81950ND12701380
Di-n-butylphthalate ug/kg 1950 75 19-11281 81950ND14501580
Di-n-octylphthalate ug/kg 1950 74 17-10583 121950ND14301620
Dibenz(a,h)anthracene ug/kg 1950 55 23-11163 121950ND10801220
Dibenzofuran ug/kg 1950 65 35-10371 81950ND12701380
Diethylphthalate ug/kg 1950 67 27-11374 111950ND13001450
Dimethylphthalate ug/kg 1950 63 26-11169 101950ND12201340
Fluoranthene ug/kg 1950 71 33-10974 31950ND13901440
Fluorene ug/kg 1950 66 32-11369 51950ND12801350
Hexachloro-1,3-butadiene ug/kg 1950 47 16-11657 201950ND9081110
Hexachlorobenzene ug/kg 1950 51 27-12056 81950ND9961080
Hexachlorocyclopentadiene ug/kg 1950 49 10-10861 211950ND9621180
Hexachloroethane ug/kg 1950 57 10-11767 171950ND11001310
Indeno(1,2,3-cd)pyrene ug/kg 1950 55 10-12263 131950ND10701220
Isophorone ug/kg 1950 67 28-11476 121950ND13101470
N-Nitroso-di-n-propylamine ug/kg 1950 62 27-11374 181950ND12101450
N-Nitrosodimethylamine ug/kg 1950 58 10-10970 201950ND11201370
N-Nitrosodiphenylamine ug/kg 1950 68 10-12874 91950ND13201450
Naphthalene ug/kg 1950 57 25-11066 141950ND11101290
Nitrobenzene ug/kg 1950 58 18-11468 171950ND11201330
Pentachlorophenol ug/kg 3890 65 10-12269 73890ND25102690
Phenanthrene ug/kg 1950 68 30-11472 51950ND13301390
Phenol ug/kg 1950 61 11-10276 211950ND11901470
Pyrene ug/kg 1950 66 25-11672 101950ND12801400
2,4,6-Tribromophenol (S)%57 27-11062
2-Fluorobiphenyl (S)%57 30-11066
2-Fluorophenol (S)%59 13-11070
Nitrobenzene-d5 (S)%58 23-11068
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 58 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
640692MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299306001
640693
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenol-d6 (S)%63 22-11075
Terphenyl-d14 (S)%62 28-11077
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 59 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/14374
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:9299302008, 9299302009, 9299302010, 9299302011, 9299302012, 9299302015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:641270
Associated Lab Samples:9299302008, 9299302009, 9299302010, 9299302011, 9299302012, 9299302015
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 08/05/11 13:33
1,2-Dichlorobenzene ug/L ND 10.0 08/05/11 13:33
1,3-Dichlorobenzene ug/L ND 10.0 08/05/11 13:33
1,4-Dichlorobenzene ug/L ND 10.0 08/05/11 13:33
1-Methylnaphthalene ug/L ND 10.0 08/05/11 13:33
2,4,5-Trichlorophenol ug/L ND 10.0 08/05/11 13:33
2,4,6-Trichlorophenol ug/L ND 10.0 08/05/11 13:33
2,4-Dichlorophenol ug/L ND 10.0 08/05/11 13:33
2,4-Dimethylphenol ug/L ND 10.0 08/05/11 13:33
2,4-Dinitrophenol ug/L ND 50.0 08/05/11 13:33
2,4-Dinitrotoluene ug/L ND 10.0 08/05/11 13:33
2,6-Dinitrotoluene ug/L ND 10.0 08/05/11 13:33
2-Chloronaphthalene ug/L ND 10.0 08/05/11 13:33
2-Chlorophenol ug/L ND 10.0 08/05/11 13:33
2-Methylnaphthalene ug/L ND 10.0 08/05/11 13:33
2-Methylphenol(o-Cresol)ug/L ND 10.0 08/05/11 13:33
2-Nitroaniline ug/L ND 50.0 08/05/11 13:33
2-Nitrophenol ug/L ND 10.0 08/05/11 13:33
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 08/05/11 13:33
3,3'-Dichlorobenzidine ug/L ND 20.0 08/05/11 13:33
3-Nitroaniline ug/L ND 50.0 08/05/11 13:33
4,6-Dinitro-2-methylphenol ug/L ND 20.0 08/05/11 13:33
4-Bromophenylphenyl ether ug/L ND 10.0 08/05/11 13:33
4-Chloro-3-methylphenol ug/L ND 20.0 08/05/11 13:33
4-Chloroaniline ug/L ND 20.0 08/05/11 13:33
4-Chlorophenylphenyl ether ug/L ND 10.0 08/05/11 13:33
4-Nitroaniline ug/L ND 20.0 08/05/11 13:33
4-Nitrophenol ug/L ND 50.0 08/05/11 13:33
Acenaphthene ug/L ND 10.0 08/05/11 13:33
Acenaphthylene ug/L ND 10.0 08/05/11 13:33
Aniline ug/L ND 10.0 08/05/11 13:33
Anthracene ug/L ND 10.0 08/05/11 13:33
Benzo(a)anthracene ug/L ND 10.0 08/05/11 13:33
Benzo(a)pyrene ug/L ND 10.0 08/05/11 13:33
Benzo(b)fluoranthene ug/L ND 10.0 08/05/11 13:33
Benzo(g,h,i)perylene ug/L ND 10.0 08/05/11 13:33
Benzo(k)fluoranthene ug/L ND 10.0 08/05/11 13:33
Benzoic Acid ug/L ND 50.0 08/05/11 13:33
Benzyl alcohol ug/L ND 20.0 08/05/11 13:33
bis(2-Chloroethoxy)methane ug/L ND 10.0 08/05/11 13:33
bis(2-Chloroethyl) ether ug/L ND 10.0 08/05/11 13:33
bis(2-Chloroisopropyl) ether ug/L ND 10.0 08/05/11 13:33
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 08/05/11 13:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 60 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:641270
Associated Lab Samples:9299302008, 9299302009, 9299302010, 9299302011, 9299302012, 9299302015
Matrix:Water
Analyzed
Butylbenzylphthalate ug/L ND 10.0 08/05/11 13:33
Chrysene ug/L ND 10.0 08/05/11 13:33
Di-n-butylphthalate ug/L ND 10.0 08/05/11 13:33
Di-n-octylphthalate ug/L ND 10.0 08/05/11 13:33
Dibenz(a,h)anthracene ug/L ND 10.0 08/05/11 13:33
Dibenzofuran ug/L ND 10.0 08/05/11 13:33
Diethylphthalate ug/L ND 10.0 08/05/11 13:33
Dimethylphthalate ug/L ND 10.0 08/05/11 13:33
Fluoranthene ug/L ND 10.0 08/05/11 13:33
Fluorene ug/L ND 10.0 08/05/11 13:33
Hexachloro-1,3-butadiene ug/L ND 10.0 08/05/11 13:33
Hexachlorobenzene ug/L ND 10.0 08/05/11 13:33
Hexachlorocyclopentadiene ug/L ND 10.0 08/05/11 13:33
Hexachloroethane ug/L ND 10.0 08/05/11 13:33
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 08/05/11 13:33
Isophorone ug/L ND 10.0 08/05/11 13:33
N-Nitroso-di-n-propylamine ug/L ND 10.0 08/05/11 13:33
N-Nitrosodimethylamine ug/L ND 10.0 08/05/11 13:33
N-Nitrosodiphenylamine ug/L ND 10.0 08/05/11 13:33
Naphthalene ug/L ND 10.0 08/05/11 13:33
Nitrobenzene ug/L ND 10.0 08/05/11 13:33
Pentachlorophenol ug/L ND 25.0 08/05/11 13:33
Phenanthrene ug/L ND 10.0 08/05/11 13:33
Phenol ug/L ND 10.0 08/05/11 13:33
Pyrene ug/L ND 10.0 08/05/11 13:33
2,4,6-Tribromophenol (S)%63 27-110 08/05/11 13:33
2-Fluorobiphenyl (S)%65 27-110 08/05/11 13:33
2-Fluorophenol (S)%46 12-110 08/05/11 13:33
Nitrobenzene-d5 (S)%69 21-110 08/05/11 13:33
Phenol-d6 (S)%32 10-110 08/05/11 13:33
Terphenyl-d14 (S)%81 31-107 08/05/11 13:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
641271LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 27.350 55 10-110
1,2-Dichlorobenzene ug/L 28.150 56 10-110
1,3-Dichlorobenzene ug/L 25.450 51 10-110
1,4-Dichlorobenzene ug/L 26.250 52 10-110
1-Methylnaphthalene ug/L 34.250 68 21-110
2,4,5-Trichlorophenol ug/L 34.050 68 23-116
2,4,6-Trichlorophenol ug/L 40.150 80 21-114
2,4-Dichlorophenol ug/L 36.550 73 22-120
2,4-Dimethylphenol ug/L 31.150 62 15-109
2,4-Dinitrophenol ug/L 183250 73 10-103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 61 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
641271LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dinitrotoluene ug/L 38.250 76 24-119
2,6-Dinitrotoluene ug/L 38.750 77 25-116
2-Chloronaphthalene ug/L 37.450 75 18-110
2-Chlorophenol ug/L 38.150 76 10-104
2-Methylnaphthalene ug/L 34.150 68 16-110
2-Methylphenol(o-Cresol)ug/L 39.050 78 13-110
2-Nitroaniline ug/L 85.0100 85 20-117
2-Nitrophenol ug/L 37.850 76 16-108
3&4-Methylphenol(m&p Cresol)ug/L 39.250 78 14-110
3,3'-Dichlorobenzidine ug/L 61.6100 62 13-131
3-Nitroaniline ug/L 71.4100 71 15-117
4,6-Dinitro-2-methylphenol ug/L 81.8100 82 13-119
4-Bromophenylphenyl ether ug/L 39.050 78 23-120
4-Chloro-3-methylphenol ug/L 80.1100 80 21-119
4-Chloroaniline ug/L 74.4100 74 10-122
4-Chlorophenylphenyl ether ug/L 36.750 73 22-112
4-Nitroaniline ug/L 65.4100 65 14-118
4-Nitrophenol ug/L 106250 42 10-110
Acenaphthene ug/L 37.750 75 20-105
Acenaphthylene ug/L 36.550 73 23-106
Aniline ug/L 36.150 72 10-110
Anthracene ug/L 38.450 77 25-120
Benzo(a)anthracene ug/L 38.850 78 21-128
Benzo(a)pyrene ug/L 36.450 73 25-116
Benzo(b)fluoranthene ug/L 37.450 75 23-117
Benzo(g,h,i)perylene ug/L 35.850 72 17-128
Benzo(k)fluoranthene ug/L 36.850 74 25-127
Benzoic Acid ug/L 107250 43 10-110
Benzyl alcohol ug/L 91.6100 92 10-101
bis(2-Chloroethoxy)methane ug/L 38.250 76 19-107
bis(2-Chloroethyl) ether ug/L 41.650 83 10-108
bis(2-Chloroisopropyl) ether ug/L 40.850 82 10-108
bis(2-Ethylhexyl)phthalate ug/L 41.050 82 16-123
Butylbenzylphthalate ug/L 40.650 81 20-118
Chrysene ug/L 38.850 78 24-125
Di-n-butylphthalate ug/L 39.950 80 23-115
Di-n-octylphthalate ug/L 37.250 74 20-115
Dibenz(a,h)anthracene ug/L 34.550 69 18-131
Dibenzofuran ug/L 38.250 76 23-106
Diethylphthalate ug/L 38.250 76 24-115
Dimethylphthalate ug/L 38.250 76 22-113
Fluoranthene ug/L 36.550 73 24-125
Fluorene ug/L 36.950 74 24-114
Hexachloro-1,3-butadiene ug/L 22.150 44 10-110
Hexachlorobenzene ug/L 39.150 78 22-127
Hexachlorocyclopentadiene ug/L 34.350 69 10-110
Hexachloroethane ug/L 25.350 51 10-110
Indeno(1,2,3-cd)pyrene ug/L 35.050 70 18-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 62 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
641271LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/L 42.650 85 23-114
N-Nitroso-di-n-propylamine ug/L 48.050 96 21-114
N-Nitrosodimethylamine ug/L 26.850 54 10-110
N-Nitrosodiphenylamine ug/L 39.250 78 24-123
Naphthalene ug/L 31.650 63 14-110
Nitrobenzene ug/L 38.150 76 16-106
Pentachlorophenol ug/L 77.6100 78 10-123
Phenanthrene ug/L 38.150 76 25-119
Phenol ug/L 26.450 53 10-110
Pyrene ug/L 39.250 78 22-127
2,4,6-Tribromophenol (S)%90 27-110
2-Fluorobiphenyl (S)%74 27-110
2-Fluorophenol (S)%50 12-110
Nitrobenzene-d5 (S)%71 21-110
Phenol-d6 (S)%47 10-110
Terphenyl-d14 (S)%78 31-107
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
641272MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299262008
641273
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 100 55 10-11062 11100ND55.4 61.8
1,2-Dichlorobenzene ug/L 100 58 10-11063 7100ND58.2 62.7
1,3-Dichlorobenzene ug/L 100 56 10-11062 10100ND55.8 61.6
1,4-Dichlorobenzene ug/L 100 58 10-11063 8100ND57.8 62.6
1-Methylnaphthalene ug/L 100 61 14-11070 13100ND61.2 69.9
2,4,5-Trichlorophenol ug/L 100 60 19-10567 12100ND59.9 67.3
2,4,6-Trichlorophenol ug/L 100 70 13-10877 9100ND69.9 76.8
2,4-Dichlorophenol ug/L 100 64 29-11174 13100ND64.3 73.6
2,4-Dimethylphenol ug/L 100 60 21-10364 6100ND60.1 63.9
2,4-Dinitrophenol ug/L 500 60 10-10966 10500ND300332
2,4-Dinitrotoluene ug/L 100 90 27-10492 2100ND89.8 91.5
2,6-Dinitrotoluene ug/L 100 79 28-10187 9100ND79.3 87.1
2-Chloronaphthalene ug/L 100 67 14-10272 7100ND67.5 72.1
2-Chlorophenol ug/L 100 68 16-11072 6100ND67.8 72.1
2-Methylnaphthalene ug/L 100 62 13-11070 13100ND61.6 70.1
2-Methylphenol(o-Cresol)ug/L 100 59 19-11064 8100ND58.8 63.8
2-Nitroaniline ug/L 200 90 26-103101 11200ND180202
2-Nitrophenol ug/L 100 65 20-11074 12100ND65.1 73.8
3&4-Methylphenol(m&p
Cresol)ug/L 100 54 20-11060 11100ND53.8 60.0
3,3'-Dichlorobenzidine ug/L 200 66 25-11254 20200ND133109
3-Nitroaniline ug/L 200 83 29-11084 1200ND167168
4,6-Dinitro-2-methylphenol ug/L 200 71 10-11771 1200ND143142
4-Bromophenylphenyl ether ug/L 100 67 20-10576 13100ND67.1 76.4
4-Chloro-3-methylphenol ug/L 200 73 22-11090 21200ND146181
4-Chloroaniline ug/L 200 68 20-10071 4200ND136142
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 63 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
641272MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299262008
641273
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
4-Chlorophenylphenyl ether ug/L 100 72 19-10281 12100ND72.2 81.2
4-Nitroaniline ug/L 200 98 29-11088 11200ND196176
4-Nitrophenol ug/L 500 61 10-11066 7500ND307331
Acenaphthene ug/L 100 71 17-10079 10100ND71.5 79.2
Acenaphthylene ug/L 100 68 21-10075 11100ND67.9 75.5
Aniline ug/L R11006110-11041 38100ND60.8 41.4
Anthracene ug/L 100 79 24-10981 3100ND78.7 80.9
Benzo(a)anthracene ug/L 100 73 22-11776 4100ND72.9 75.9
Benzo(a)pyrene ug/L 100 69 23-10474 6100ND69.4 73.7
Benzo(b)fluoranthene ug/L 100 69 23-10374 7100ND68.7 73.9
Benzo(g,h,i)perylene ug/L 100 70 18-11173 4100ND70.0 72.7
Benzo(k)fluoranthene ug/L 100 73 22-11379 7100ND73.3 78.8
Benzoic Acid ug/L 500 17 10-11055500ND86.2J 277
Benzyl alcohol ug/L 200 67 19-10176 12200ND135151
bis(2-Chloroethoxy)methane ug/L 100 71 22-11081 13100ND70.7 80.6
bis(2-Chloroethyl) ether ug/L 100 76 16-11077 2100ND76.1 77.5
bis(2-Chloroisopropyl) ether ug/L 100 70 14-11075 8100ND69.9 75.3
bis(2-Ethylhexyl)phthalate ug/L 100 74 23-10279 6100ND74.1 78.7
Butylbenzylphthalate ug/L 100 72 25-11080 11100ND72.2 80.3
Chrysene ug/L 100 75 23-11579 5100ND74.8 78.6
Di-n-butylphthalate ug/L 100 93 26-11087 7100ND93.3 87.1
Di-n-octylphthalate ug/L 100 63 22-11063 0100ND63.1 63.4
Dibenz(a,h)anthracene ug/L 100 66 21-11268 3100ND65.6 67.6
Dibenzofuran ug/L 100 74 19-10282 10100ND74.4 81.9
Diethylphthalate ug/L 100 92 29-11092 1100ND91.7 92.4
Dimethylphthalate ug/L 100 84 27-11088 5100ND83.6 88.0
Fluoranthene ug/L 100 89 23-11277 15100ND89.1 76.7
Fluorene ug/L 100 75 22-10482 10100ND74.7 82.4
Hexachloro-1,3-butadiene ug/L 100 47 10-11054 14100ND47.2 54.4
Hexachlorobenzene ug/L 100 72 21-11677 7100ND71.5 76.6
Hexachlorocyclopentadiene ug/L 100 56 10-11055 1100ND55.6 54.9
Hexachloroethane ug/L 100 56 10-11061 9100ND55.5 61.0
Indeno(1,2,3-cd)pyrene ug/L 100 67 20-11370 3100ND67.2 69.6
Isophorone ug/L 100 77 50-15094 20100ND77.2 94.4
N-Nitroso-di-n-propylamine ug/L 100 67 21-10576 13100ND66.8 76.1
N-Nitrosodimethylamine ug/L 100 59 10-11069 15100ND59.4 69.2
N-Nitrosodiphenylamine ug/L 100 73 23-10780 9100ND73.2 80.4
Naphthalene ug/L 100 62 10-11069 10100ND62.0 68.6
Nitrobenzene ug/L 100 72 20-11080 11100ND71.7 80.3
Pentachlorophenol ug/L 200 68 10-11868 1200ND137135
Phenanthrene ug/L 100 77 24-10679 3100ND77.0 79.2
Phenol ug/L 100 46 12-11051 11100ND45.7 51.1
Pyrene ug/L 100 67 24-11481 19100ND66.9 81.3
2,4,6-Tribromophenol (S)%75 27-11082
2-Fluorobiphenyl (S)%66 27-11068
2-Fluorophenol (S)%50 12-11058
Nitrobenzene-d5 (S)%69 21-11075
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 64 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
641272MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299262008
641273
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenol-d6 (S)%40 10-11046
Terphenyl-d14 (S)%68 31-10780
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 65 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/16181
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:9299302008, 9299302009, 9299302010, 9299302011, 9299302012, 9299302015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:641590
Associated Lab Samples:9299302008, 9299302009, 9299302010, 9299302011, 9299302012, 9299302015
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/02/11 15:09
1,1,1-Trichloroethane ug/L ND 1.0 08/02/11 15:09
1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/02/11 15:09
1,1,2-Trichloroethane ug/L ND 1.0 08/02/11 15:09
1,1-Dichloroethane ug/L ND 1.0 08/02/11 15:09
1,1-Dichloroethene ug/L ND 1.0 08/02/11 15:09
1,1-Dichloropropene ug/L ND 1.0 08/02/11 15:09
1,2,3-Trichlorobenzene ug/L ND 1.0 08/02/11 15:09
1,2,3-Trichloropropane ug/L ND 1.0 08/02/11 15:09
1,2,4-Trichlorobenzene ug/L ND 1.0 08/02/11 15:09
1,2-Dibromo-3-chloropropane ug/L ND 5.0 08/02/11 15:09
1,2-Dibromoethane (EDB)ug/L ND 1.0 08/02/11 15:09
1,2-Dichlorobenzene ug/L ND 1.0 08/02/11 15:09
1,2-Dichloroethane ug/L ND 1.0 08/02/11 15:09
1,2-Dichloropropane ug/L ND 1.0 08/02/11 15:09
1,3-Dichlorobenzene ug/L ND 1.0 08/02/11 15:09
1,3-Dichloropropane ug/L ND 1.0 08/02/11 15:09
1,4-Dichlorobenzene ug/L ND 1.0 08/02/11 15:09
2,2-Dichloropropane ug/L ND 1.0 08/02/11 15:09
2-Butanone (MEK)ug/L ND 5.0 08/02/11 15:09
2-Chlorotoluene ug/L ND 1.0 08/02/11 15:09
2-Hexanone ug/L ND 5.0 08/02/11 15:09
4-Chlorotoluene ug/L ND 1.0 08/02/11 15:09
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 08/02/11 15:09
Acetone ug/L ND 25.0 08/02/11 15:09
Benzene ug/L ND 1.0 08/02/11 15:09
Bromobenzene ug/L ND 1.0 08/02/11 15:09
Bromochloromethane ug/L ND 1.0 08/02/11 15:09
Bromodichloromethane ug/L ND 1.0 08/02/11 15:09
Bromoform ug/L ND 1.0 08/02/11 15:09
Bromomethane ug/L ND 2.0 08/02/11 15:09
Carbon tetrachloride ug/L ND 1.0 08/02/11 15:09
Chlorobenzene ug/L ND 1.0 08/02/11 15:09
Chloroethane ug/L ND 1.0 08/02/11 15:09
Chloroform ug/L ND 1.0 08/02/11 15:09
Chloromethane ug/L ND 1.0 08/02/11 15:09
cis-1,2-Dichloroethene ug/L ND 1.0 08/02/11 15:09
cis-1,3-Dichloropropene ug/L ND 1.0 08/02/11 15:09
Dibromochloromethane ug/L ND 1.0 08/02/11 15:09
Dibromomethane ug/L ND 1.0 08/02/11 15:09
Dichlorodifluoromethane ug/L ND 1.0 08/02/11 15:09
Diisopropyl ether ug/L ND 1.0 08/02/11 15:09
Ethylbenzene ug/L ND 1.0 08/02/11 15:09
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 66 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:641590
Associated Lab Samples:9299302008, 9299302009, 9299302010, 9299302011, 9299302012, 9299302015
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 1.0 08/02/11 15:09
m&p-Xylene ug/L ND 2.0 08/02/11 15:09
Methyl-tert-butyl ether ug/L ND 1.0 08/02/11 15:09
Methylene Chloride ug/L ND 2.0 08/02/11 15:09
Naphthalene ug/L ND 1.0 08/02/11 15:09
o-Xylene ug/L ND 1.0 08/02/11 15:09
p-Isopropyltoluene ug/L ND 1.0 08/02/11 15:09
Styrene ug/L ND 1.0 08/02/11 15:09
Tetrachloroethene ug/L ND 1.0 08/02/11 15:09
Toluene ug/L ND 1.0 08/02/11 15:09
trans-1,2-Dichloroethene ug/L ND 1.0 08/02/11 15:09
trans-1,3-Dichloropropene ug/L ND 1.0 08/02/11 15:09
Trichloroethene ug/L ND 1.0 08/02/11 15:09
Trichlorofluoromethane ug/L ND 1.0 08/02/11 15:09
Vinyl acetate ug/L ND 2.0 08/02/11 15:09
Vinyl chloride ug/L ND 1.0 08/02/11 15:09
Xylene (Total)ug/L ND 2.0 08/02/11 15:09
1,2-Dichloroethane-d4 (S)%105 70-130 08/02/11 15:09
4-Bromofluorobenzene (S)%95 70-130 08/02/11 15:09
Dibromofluoromethane (S)%103 70-130 08/02/11 15:09
Toluene-d8 (S)%100 70-130 08/02/11 15:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
641591LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.750 105 70-130
1,1,1-Trichloroethane ug/L 46.850 94 70-130
1,1,2,2-Tetrachloroethane ug/L 52.550 105 70-130
1,1,2-Trichloroethane ug/L 50.950 102 70-130
1,1-Dichloroethane ug/L 45.250 90 70-130
1,1-Dichloroethene ug/L 42.550 85 70-132
1,1-Dichloropropene ug/L 44.550 89 70-130
1,2,3-Trichlorobenzene ug/L 51.250 102 70-135
1,2,3-Trichloropropane ug/L 50.950 102 70-130
1,2,4-Trichlorobenzene ug/L 50.150 100 70-134
1,2-Dibromo-3-chloropropane ug/L 52.650 105 70-130
1,2-Dibromoethane (EDB)ug/L 51.250 102 70-130
1,2-Dichlorobenzene ug/L 49.850 100 70-130
1,2-Dichloroethane ug/L 45.650 91 70-130
1,2-Dichloropropane ug/L 46.850 94 70-130
1,3-Dichlorobenzene ug/L 49.550 99 70-130
1,3-Dichloropropane ug/L 50.750 101 70-130
1,4-Dichlorobenzene ug/L 48.850 98 70-130
2,2-Dichloropropane ug/L 45.550 91 58-145
2-Butanone (MEK)ug/L 103100 103 70-145
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 67 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
641591LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorotoluene ug/L 49.050 98 70-130
2-Hexanone ug/L 110100 110 70-144
4-Chlorotoluene ug/L 52.050 104 70-130
4-Methyl-2-pentanone (MIBK)ug/L 101100 101 70-140
Acetone ug/L 100100 100 50-175
Benzene ug/L 44.150 88 70-130
Bromobenzene ug/L 48.250 96 70-130
Bromochloromethane ug/L 46.850 94 70-130
Bromodichloromethane ug/L 49.850 100 70-130
Bromoform ug/L 52.450 105 70-130
Bromomethane ug/L 44.750 89 54-130
Carbon tetrachloride ug/L 48.350 97 70-132
Chlorobenzene ug/L 49.950 100 70-130
Chloroethane ug/L 41.950 84 64-134
Chloroform ug/L 47.950 96 70-130
Chloromethane ug/L 43.050 86 64-130
cis-1,2-Dichloroethene ug/L 44.750 89 70-131
cis-1,3-Dichloropropene ug/L 50.650 101 70-130
Dibromochloromethane ug/L 52.050 104 70-130
Dibromomethane ug/L 48.850 98 70-131
Dichlorodifluoromethane ug/L 43.850 88 56-130
Diisopropyl ether ug/L 44.550 89 70-130
Ethylbenzene ug/L 49.050 98 70-130
Hexachloro-1,3-butadiene ug/L 50.950 102 70-130
m&p-Xylene ug/L 99.0100 99 70-130
Methyl-tert-butyl ether ug/L 46.950 94 70-130
Methylene Chloride ug/L 43.250 86 63-130
Naphthalene ug/L 55.950 112 70-138
o-Xylene ug/L 51.850 104 70-130
p-Isopropyltoluene ug/L 52.450 105 70-130
Styrene ug/L 53.950 108 70-130
Tetrachloroethene ug/L 51.150 102 70-130
Toluene ug/L 45.550 91 70-130
trans-1,2-Dichloroethene ug/L 43.750 87 70-130
trans-1,3-Dichloropropene ug/L 50.650 101 70-132
Trichloroethene ug/L 47.550 95 70-130
Trichlorofluoromethane ug/L 43.750 87 62-133
Vinyl acetate ug/L 116100 116 66-157
Vinyl chloride ug/L 47.950 96 69-130
Xylene (Total)ug/L 151150 101 70-130
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%100 70-130
Dibromofluoromethane (S)%98 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 68 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
641592MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299331001
641593
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 50 118 70-166105 1250ND59.2 52.3
Benzene ug/L 50 106 70-14892 1450ND52.9 46.2
Chlorobenzene ug/L 50 126 70-146112 1250ND63.0 56.1
Toluene ug/L 50 124 70-155109 1350ND61.9 54.4
Trichloroethene ug/L 50 124 69-151109 1350ND62.1 54.5
1,2-Dichloroethane-d4 (S)%102 70-130103
4-Bromofluorobenzene (S)%95 70-13096
Dibromofluoromethane (S)%100 70-130102
Toluene-d8 (S)%98 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 69 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/16155
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:9299302001, 9299302002, 9299302003, 9299302004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:640648
Associated Lab Samples:9299302001, 9299302002, 9299302003, 9299302004
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/29/11 23:25
1,1,1-Trichloroethane ug/kg ND 5.0 07/29/11 23:25
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/29/11 23:25
1,1,2-Trichloroethane ug/kg ND 5.0 07/29/11 23:25
1,1-Dichloroethane ug/kg ND 5.0 07/29/11 23:25
1,1-Dichloroethene ug/kg ND 5.0 07/29/11 23:25
1,1-Dichloropropene ug/kg ND 5.0 07/29/11 23:25
1,2,3-Trichlorobenzene ug/kg ND 5.0 07/29/11 23:25
1,2,3-Trichloropropane ug/kg ND 5.0 07/29/11 23:25
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/29/11 23:25
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/29/11 23:25
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 07/29/11 23:25
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/29/11 23:25
1,2-Dichlorobenzene ug/kg ND 5.0 07/29/11 23:25
1,2-Dichloroethane ug/kg ND 5.0 07/29/11 23:25
1,2-Dichloropropane ug/kg ND 5.0 07/29/11 23:25
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/29/11 23:25
1,3-Dichlorobenzene ug/kg ND 5.0 07/29/11 23:25
1,3-Dichloropropane ug/kg ND 5.0 07/29/11 23:25
1,4-Dichlorobenzene ug/kg ND 5.0 07/29/11 23:25
2,2-Dichloropropane ug/kg ND 5.0 07/29/11 23:25
2-Butanone (MEK)ug/kg ND 100 07/29/11 23:25
2-Chlorotoluene ug/kg ND 5.0 07/29/11 23:25
2-Hexanone ug/kg ND 50.0 07/29/11 23:25
4-Chlorotoluene ug/kg ND 5.0 07/29/11 23:25
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/29/11 23:25
Acetone ug/kg ND 100 07/29/11 23:25
Benzene ug/kg ND 5.0 07/29/11 23:25
Bromobenzene ug/kg ND 5.0 07/29/11 23:25
Bromochloromethane ug/kg ND 5.0 07/29/11 23:25
Bromodichloromethane ug/kg ND 5.0 07/29/11 23:25
Bromoform ug/kg ND 5.0 07/29/11 23:25
Bromomethane ug/kg ND 10.0 07/29/11 23:25
Carbon tetrachloride ug/kg ND 5.0 07/29/11 23:25
Chlorobenzene ug/kg ND 5.0 07/29/11 23:25
Chloroethane ug/kg ND 10.0 07/29/11 23:25
Chloroform ug/kg ND 5.0 07/29/11 23:25
Chloromethane ug/kg ND 10.0 07/29/11 23:25
cis-1,2-Dichloroethene ug/kg ND 5.0 07/29/11 23:25
cis-1,3-Dichloropropene ug/kg ND 5.0 07/29/11 23:25
Dibromochloromethane ug/kg ND 5.0 07/29/11 23:25
Dibromomethane ug/kg ND 5.0 07/29/11 23:25
Dichlorodifluoromethane ug/kg ND 10.0 07/29/11 23:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 70 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:640648
Associated Lab Samples:9299302001, 9299302002, 9299302003, 9299302004
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.0 07/29/11 23:25
Ethylbenzene ug/kg ND 5.0 07/29/11 23:25
Hexachloro-1,3-butadiene ug/kg ND 5.0 07/29/11 23:25
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/29/11 23:25
m&p-Xylene ug/kg ND 10.0 07/29/11 23:25
Methyl-tert-butyl ether ug/kg ND 5.0 07/29/11 23:25
Methylene Chloride ug/kg ND 20.0 07/29/11 23:25
n-Butylbenzene ug/kg ND 5.0 07/29/11 23:25
n-Propylbenzene ug/kg ND 5.0 07/29/11 23:25
Naphthalene ug/kg ND 5.0 07/29/11 23:25
o-Xylene ug/kg ND 5.0 07/29/11 23:25
p-Isopropyltoluene ug/kg ND 5.0 07/29/11 23:25
sec-Butylbenzene ug/kg ND 5.0 07/29/11 23:25
Styrene ug/kg ND 5.0 07/29/11 23:25
tert-Butylbenzene ug/kg ND 5.0 07/29/11 23:25
Tetrachloroethene ug/kg ND 5.0 07/29/11 23:25
Toluene ug/kg ND 5.0 07/29/11 23:25
trans-1,2-Dichloroethene ug/kg ND 5.0 07/29/11 23:25
trans-1,3-Dichloropropene ug/kg ND 5.0 07/29/11 23:25
Trichloroethene ug/kg ND 5.0 07/29/11 23:25
Trichlorofluoromethane ug/kg ND 5.0 07/29/11 23:25
Vinyl acetate ug/kg ND 50.0 07/29/11 23:25
Vinyl chloride ug/kg ND 10.0 07/29/11 23:25
Xylene (Total)ug/kg ND 10.0 07/29/11 23:25
1,2-Dichloroethane-d4 (S)%95 70-132 07/29/11 23:25
4-Bromofluorobenzene (S)%94 70-130 07/29/11 23:25
Dibromofluoromethane (S)%101 70-130 07/29/11 23:25
Toluene-d8 (S)%103 70-130 07/29/11 23:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640649LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 48.250 96 70-131
1,1,1-Trichloroethane ug/kg 41.850 84 70-141
1,1,2,2-Tetrachloroethane ug/kg 44.250 88 70-130
1,1,2-Trichloroethane ug/kg 44.950 90 70-132
1,1-Dichloroethane ug/kg 40.850 82 70-143
1,1-Dichloroethene ug/kg 39.050 78 70-137
1,1-Dichloropropene ug/kg 37.750 75 70-135
1,2,3-Trichlorobenzene ug/kg 38.850 78 69-153
1,2,3-Trichloropropane ug/kg 40.750 81 70-130
1,2,4-Trichlorobenzene ug/kg 37.750 75 55-171
1,2,4-Trimethylbenzene ug/kg 42.950 86 70-149
1,2-Dibromo-3-chloropropane ug/kg 38.450 77 68-141
1,2-Dibromoethane (EDB)ug/kg 42.950 86 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 71 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640649LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 43.250 86 70-140
1,2-Dichloroethane ug/kg 41.050 82 70-137
1,2-Dichloropropane ug/kg 44.050 88 70-133
1,3,5-Trimethylbenzene ug/kg 42.050 84 70-143
1,3-Dichlorobenzene ug/kg 41.150 82 70-144
1,3-Dichloropropane ug/kg 42.450 85 70-132
1,4-Dichlorobenzene ug/kg 39.450 79 70-142
2,2-Dichloropropane ug/kg 36.150 72 68-152
2-Butanone (MEK)ug/kg 73.5J100 74 70-149
2-Chlorotoluene ug/kg 42.350 85 70-141
2-Hexanone ug/kg 76.3100 76 70-149
4-Chlorotoluene ug/kg 42.250 84 70-149
4-Methyl-2-pentanone (MIBK)ug/kg 78.6100 79 70-153
Acetone ug/kg 78.9J100 79 70-157
Benzene ug/kg 40.750 81 70-130
Bromobenzene ug/kg 40.750 81 70-141
Bromochloromethane ug/kg 40.550 81 70-149
Bromodichloromethane ug/kg 45.250 90 70-130
Bromoform ug/kg 41.350 83 70-131
Bromomethane ug/kg 43.350 87 64-136
Carbon tetrachloride ug/kg 41.150 82 70-154
Chlorobenzene ug/kg 44.050 88 70-135
Chloroethane ug/kg 44.350 89 68-151
Chloroform ug/kg 43.350 87 70-130
Chloromethane ug/kg 40.950 82 70-132
cis-1,2-Dichloroethene ug/kg 39.250 78 70-140
cis-1,3-Dichloropropene ug/kg 44.050 88 70-137
Dibromochloromethane ug/kg 45.850 92 70-130
Dibromomethane ug/kg 42.450 85 70-136
Dichlorodifluoromethane ug/kg 41.150 82 36-148
Diisopropyl ether ug/kg 41.250 82 70-139
Ethylbenzene ug/kg 42.050 84 70-137
Hexachloro-1,3-butadiene ug/kg 39.050 78 70-145
Isopropylbenzene (Cumene)ug/kg 43.850 88 70-141
m&p-Xylene ug/kg 83.9100 84 70-140
Methyl-tert-butyl ether ug/kg 41.550 83 45-150
Methylene Chloride ug/kg 36.750 73 70-133
n-Butylbenzene ug/kg 40.050 80 65-155
n-Propylbenzene ug/kg 42.250 84 70-148
Naphthalene ug/kg 43.950 88 70-148
o-Xylene ug/kg 44.050 88 70-141
p-Isopropyltoluene ug/kg 41.850 84 70-148
sec-Butylbenzene ug/kg 42.450 85 70-145
Styrene ug/kg 46.150 92 70-138
tert-Butylbenzene ug/kg 44.250 88 70-143
Tetrachloroethene ug/kg 41.750 83 70-140
Toluene ug/kg 41.150 82 70-130
trans-1,2-Dichloroethene ug/kg 38.650 77 70-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 72 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640649LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 42.250 84 70-138
Trichloroethene ug/kg 43.550 87 70-132
Trichlorofluoromethane ug/kg 41.650 83 69-134
Vinyl acetate ug/kg 38.7J100 39 24-161
Vinyl chloride ug/kg 43.650 87 55-140
Xylene (Total)ug/kg 128150 85 70-141
1,2-Dichloroethane-d4 (S)%97 70-132
4-Bromofluorobenzene (S)%99 70-130
Dibromofluoromethane (S)%94 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
640988MATRIX SPIKE SAMPLE:
MSSpike
Result
9299304001
1,1-Dichloroethene ug/kg 38.943.4 90 49-180ND
Benzene ug/kg 35.443.4 82 50-166ND
Chlorobenzene ug/kg 41.543.4 96 43-169ND
Toluene ug/kg 40.943.4 94 52-163ND
Trichloroethene ug/kg 41.843.4 96 49-167ND
1,2-Dichloroethane-d4 (S)%87 70-132
4-Bromofluorobenzene (S)%92 70-130
Dibromofluoromethane (S)%95 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result QualifiersRPDResult
9299182004
640987SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 73 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
Dup
Result QualifiersRPDResult
9299182004
640987SAMPLE DUPLICATE:
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg 147 C915126
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg 3JND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 74 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
Dup
Result QualifiersRPDResult
9299182004
640987SAMPLE DUPLICATE:
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%85 284
4-Bromofluorobenzene (S)%95 394
Dibromofluoromethane (S)%98 198
Toluene-d8 (S)%104 2103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 75 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/16162
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:9299302005, 9299302007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:640991
Associated Lab Samples:9299302005, 9299302007
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/31/11 11:14
1,1,1-Trichloroethane ug/kg ND 5.0 07/31/11 11:14
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/31/11 11:14
1,1,2-Trichloroethane ug/kg ND 5.0 07/31/11 11:14
1,1-Dichloroethane ug/kg ND 5.0 07/31/11 11:14
1,1-Dichloroethene ug/kg ND 5.0 07/31/11 11:14
1,1-Dichloropropene ug/kg ND 5.0 07/31/11 11:14
1,2,3-Trichlorobenzene ug/kg ND 5.0 07/31/11 11:14
1,2,3-Trichloropropane ug/kg ND 5.0 07/31/11 11:14
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/31/11 11:14
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/31/11 11:14
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 07/31/11 11:14
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/31/11 11:14
1,2-Dichlorobenzene ug/kg ND 5.0 07/31/11 11:14
1,2-Dichloroethane ug/kg ND 5.0 07/31/11 11:14
1,2-Dichloropropane ug/kg ND 5.0 07/31/11 11:14
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/31/11 11:14
1,3-Dichlorobenzene ug/kg ND 5.0 07/31/11 11:14
1,3-Dichloropropane ug/kg ND 5.0 07/31/11 11:14
1,4-Dichlorobenzene ug/kg ND 5.0 07/31/11 11:14
2,2-Dichloropropane ug/kg ND 5.0 07/31/11 11:14
2-Butanone (MEK)ug/kg ND 100 07/31/11 11:14
2-Chlorotoluene ug/kg ND 5.0 07/31/11 11:14
2-Hexanone ug/kg ND 50.0 07/31/11 11:14
4-Chlorotoluene ug/kg ND 5.0 07/31/11 11:14
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/31/11 11:14
Acetone ug/kg ND 100 07/31/11 11:14
Benzene ug/kg ND 5.0 07/31/11 11:14
Bromobenzene ug/kg ND 5.0 07/31/11 11:14
Bromochloromethane ug/kg ND 5.0 07/31/11 11:14
Bromodichloromethane ug/kg ND 5.0 07/31/11 11:14
Bromoform ug/kg ND 5.0 07/31/11 11:14
Bromomethane ug/kg ND 10.0 07/31/11 11:14
Carbon tetrachloride ug/kg ND 5.0 07/31/11 11:14
Chlorobenzene ug/kg ND 5.0 07/31/11 11:14
Chloroethane ug/kg ND 10.0 07/31/11 11:14
Chloroform ug/kg ND 5.0 07/31/11 11:14
Chloromethane ug/kg ND 10.0 07/31/11 11:14
cis-1,2-Dichloroethene ug/kg ND 5.0 07/31/11 11:14
cis-1,3-Dichloropropene ug/kg ND 5.0 07/31/11 11:14
Dibromochloromethane ug/kg ND 5.0 07/31/11 11:14
Dibromomethane ug/kg ND 5.0 07/31/11 11:14
Dichlorodifluoromethane ug/kg ND 10.0 07/31/11 11:14
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 76 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:640991
Associated Lab Samples:9299302005, 9299302007
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.0 07/31/11 11:14
Ethylbenzene ug/kg ND 5.0 07/31/11 11:14
Hexachloro-1,3-butadiene ug/kg ND 5.0 07/31/11 11:14
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/31/11 11:14
m&p-Xylene ug/kg ND 10.0 07/31/11 11:14
Methyl-tert-butyl ether ug/kg ND 5.0 07/31/11 11:14
Methylene Chloride ug/kg ND 20.0 07/31/11 11:14
n-Butylbenzene ug/kg ND 5.0 07/31/11 11:14
n-Propylbenzene ug/kg ND 5.0 07/31/11 11:14
Naphthalene ug/kg ND 5.0 07/31/11 11:14
o-Xylene ug/kg ND 5.0 07/31/11 11:14
p-Isopropyltoluene ug/kg ND 5.0 07/31/11 11:14
sec-Butylbenzene ug/kg ND 5.0 07/31/11 11:14
Styrene ug/kg ND 5.0 07/31/11 11:14
tert-Butylbenzene ug/kg ND 5.0 07/31/11 11:14
Tetrachloroethene ug/kg ND 5.0 07/31/11 11:14
Toluene ug/kg ND 5.0 07/31/11 11:14
trans-1,2-Dichloroethene ug/kg ND 5.0 07/31/11 11:14
trans-1,3-Dichloropropene ug/kg ND 5.0 07/31/11 11:14
Trichloroethene ug/kg ND 5.0 07/31/11 11:14
Trichlorofluoromethane ug/kg ND 5.0 07/31/11 11:14
Vinyl acetate ug/kg ND 50.0 07/31/11 11:14
Vinyl chloride ug/kg ND 10.0 07/31/11 11:14
Xylene (Total)ug/kg ND 10.0 07/31/11 11:14
1,2-Dichloroethane-d4 (S)%88 70-132 07/31/11 11:14
4-Bromofluorobenzene (S)%95 70-130 07/31/11 11:14
Dibromofluoromethane (S)%94 70-130 07/31/11 11:14
Toluene-d8 (S)%103 70-130 07/31/11 11:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640992LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 49.050 98 70-131
1,1,1-Trichloroethane ug/kg 45.850 92 70-141
1,1,2,2-Tetrachloroethane ug/kg 44.450 89 70-130
1,1,2-Trichloroethane ug/kg 45.950 92 70-132
1,1-Dichloroethane ug/kg 44.350 89 70-143
1,1-Dichloroethene ug/kg 42.850 86 70-137
1,1-Dichloropropene ug/kg 42.450 85 70-135
1,2,3-Trichlorobenzene ug/kg 46.750 93 69-153
1,2,3-Trichloropropane ug/kg 41.950 84 70-130
1,2,4-Trichlorobenzene ug/kg 49.750 99 55-171
1,2,4-Trimethylbenzene ug/kg 48.750 97 70-149
1,2-Dibromo-3-chloropropane ug/kg 42.350 85 68-141
1,2-Dibromoethane (EDB)ug/kg 43.350 87 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 77 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640992LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 46.550 93 70-140
1,2-Dichloroethane ug/kg 44.450 89 70-137
1,2-Dichloropropane ug/kg 45.650 91 70-133
1,3,5-Trimethylbenzene ug/kg 47.750 95 70-143
1,3-Dichlorobenzene ug/kg 47.650 95 70-144
1,3-Dichloropropane ug/kg 43.150 86 70-132
1,4-Dichlorobenzene ug/kg 46.350 93 70-142
2,2-Dichloropropane ug/kg 48.450 97 68-152
2-Butanone (MEK)ug/kg 81.2J100 81 70-149
2-Chlorotoluene ug/kg 46.850 94 70-141
2-Hexanone ug/kg 78.6100 79 70-149
4-Chlorotoluene ug/kg 48.750 97 70-149
4-Methyl-2-pentanone (MIBK)ug/kg 83.3100 83 70-153
Acetone ug/kg 89.5J100 90 70-157
Benzene ug/kg 43.950 88 70-130
Bromobenzene ug/kg 43.850 88 70-141
Bromochloromethane ug/kg 44.250 88 70-149
Bromodichloromethane ug/kg 48.350 97 70-130
Bromoform ug/kg 43.550 87 70-131
Bromomethane ug/kg 45.750 91 64-136
Carbon tetrachloride ug/kg 46.950 94 70-154
Chlorobenzene ug/kg 46.750 93 70-135
Chloroethane ug/kg 48.350 97 68-151
Chloroform ug/kg 46.750 93 70-130
Chloromethane ug/kg 43.350 87 70-132
cis-1,2-Dichloroethene ug/kg 42.550 85 70-140
cis-1,3-Dichloropropene ug/kg 49.550 99 70-137
Dibromochloromethane ug/kg 46.350 93 70-130
Dibromomethane ug/kg 45.150 90 70-136
Dichlorodifluoromethane ug/kg 43.250 86 36-148
Diisopropyl ether ug/kg 44.750 89 70-139
Ethylbenzene ug/kg 46.150 92 70-137
Hexachloro-1,3-butadiene ug/kg 45.950 92 70-145
Isopropylbenzene (Cumene)ug/kg 49.350 99 70-141
m&p-Xylene ug/kg 94.4100 94 70-140
Methyl-tert-butyl ether ug/kg 43.350 87 45-150
Methylene Chloride ug/kg 44.550 89 70-133
n-Butylbenzene ug/kg 49.950 100 65-155
n-Propylbenzene ug/kg 48.350 97 70-148
Naphthalene ug/kg 48.250 96 70-148
o-Xylene ug/kg 49.550 99 70-141
p-Isopropyltoluene ug/kg 49.350 99 70-148
sec-Butylbenzene ug/kg 49.050 98 70-145
Styrene ug/kg 50.050 100 70-138
tert-Butylbenzene ug/kg 48.350 97 70-143
Tetrachloroethene ug/kg 47.450 95 70-140
Toluene ug/kg 45.150 90 70-130
trans-1,2-Dichloroethene ug/kg 43.050 86 70-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 78 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
640992LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 48.150 96 70-138
Trichloroethene ug/kg 47.750 95 70-132
Trichlorofluoromethane ug/kg 46.250 92 69-134
Vinyl acetate ug/kg 137100 137 24-161
Vinyl chloride ug/kg 47.250 94 55-140
Xylene (Total)ug/kg 144150 96 70-141
1,2-Dichloroethane-d4 (S)%88 70-132
4-Bromofluorobenzene (S)%97 70-130
Dibromofluoromethane (S)%93 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
641015MATRIX SPIKE SAMPLE:
MSSpike
Result
9299302007
1,1-Dichloroethene ug/kg 35.446.6 76 49-180ND
Benzene ug/kg 33.746.6 72 50-166ND
Chlorobenzene ug/kg 34.246.6 73 43-169ND
Toluene ug/kg 35.946.6 77 52-163ND
Trichloroethene ug/kg 36.546.6 78 49-167ND
1,2-Dichloroethane-d4 (S)%88 70-132
4-Bromofluorobenzene (S)%84 70-130
Dibromofluoromethane (S)%93 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
Dup
Result QualifiersRPDResult
9299296002
641014SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 79 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
Dup
Result QualifiersRPDResult
9299296002
641014SAMPLE DUPLICATE:
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg 241 C9ND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 80 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
Dup
Result QualifiersRPDResult
9299296002
641014SAMPLE DUPLICATE:
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%94 5292
4-Bromofluorobenzene (S)%89 4694
Dibromofluoromethane (S)%100 50101
Toluene-d8 (S)%104 52102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 81 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/16166
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:9299302006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:641118
Associated Lab Samples:9299302006
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 08/01/11 12:08
1,1,1-Trichloroethane ug/kg ND 5.0 08/01/11 12:08
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 08/01/11 12:08
1,1,2-Trichloroethane ug/kg ND 5.0 08/01/11 12:08
1,1-Dichloroethane ug/kg ND 5.0 08/01/11 12:08
1,1-Dichloroethene ug/kg ND 5.0 08/01/11 12:08
1,1-Dichloropropene ug/kg ND 5.0 08/01/11 12:08
1,2,3-Trichlorobenzene ug/kg ND 5.0 08/01/11 12:08
1,2,3-Trichloropropane ug/kg ND 5.0 08/01/11 12:08
1,2,4-Trichlorobenzene ug/kg ND 5.0 08/01/11 12:08
1,2,4-Trimethylbenzene ug/kg ND 5.0 08/01/11 12:08
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 08/01/11 12:08
1,2-Dibromoethane (EDB)ug/kg ND 5.0 08/01/11 12:08
1,2-Dichlorobenzene ug/kg ND 5.0 08/01/11 12:08
1,2-Dichloroethane ug/kg ND 5.0 08/01/11 12:08
1,2-Dichloropropane ug/kg ND 5.0 08/01/11 12:08
1,3,5-Trimethylbenzene ug/kg ND 5.0 08/01/11 12:08
1,3-Dichlorobenzene ug/kg ND 5.0 08/01/11 12:08
1,3-Dichloropropane ug/kg ND 5.0 08/01/11 12:08
1,4-Dichlorobenzene ug/kg ND 5.0 08/01/11 12:08
2,2-Dichloropropane ug/kg ND 5.0 08/01/11 12:08
2-Butanone (MEK)ug/kg ND 100 08/01/11 12:08
2-Chlorotoluene ug/kg ND 5.0 08/01/11 12:08
2-Hexanone ug/kg ND 50.0 08/01/11 12:08
4-Chlorotoluene ug/kg ND 5.0 08/01/11 12:08
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 08/01/11 12:08
Acetone ug/kg ND 100 08/01/11 12:08
Benzene ug/kg ND 5.0 08/01/11 12:08
Bromobenzene ug/kg ND 5.0 08/01/11 12:08
Bromochloromethane ug/kg ND 5.0 08/01/11 12:08
Bromodichloromethane ug/kg ND 5.0 08/01/11 12:08
Bromoform ug/kg ND 5.0 08/01/11 12:08
Bromomethane ug/kg ND 10.0 08/01/11 12:08
Carbon tetrachloride ug/kg ND 5.0 08/01/11 12:08
Chlorobenzene ug/kg ND 5.0 08/01/11 12:08
Chloroethane ug/kg ND 10.0 08/01/11 12:08
Chloroform ug/kg ND 5.0 08/01/11 12:08
Chloromethane ug/kg ND 10.0 08/01/11 12:08
cis-1,2-Dichloroethene ug/kg ND 5.0 08/01/11 12:08
cis-1,3-Dichloropropene ug/kg ND 5.0 08/01/11 12:08
Dibromochloromethane ug/kg ND 5.0 08/01/11 12:08
Dibromomethane ug/kg ND 5.0 08/01/11 12:08
Dichlorodifluoromethane ug/kg ND 10.0 08/01/11 12:08
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 82 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:641118
Associated Lab Samples:9299302006
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.0 08/01/11 12:08
Ethylbenzene ug/kg ND 5.0 08/01/11 12:08
Hexachloro-1,3-butadiene ug/kg ND 5.0 08/01/11 12:08
Isopropylbenzene (Cumene)ug/kg ND 5.0 08/01/11 12:08
m&p-Xylene ug/kg ND 10.0 08/01/11 12:08
Methyl-tert-butyl ether ug/kg ND 5.0 08/01/11 12:08
Methylene Chloride ug/kg ND 20.0 08/01/11 12:08
n-Butylbenzene ug/kg ND 5.0 08/01/11 12:08
n-Propylbenzene ug/kg ND 5.0 08/01/11 12:08
Naphthalene ug/kg ND 5.0 08/01/11 12:08
o-Xylene ug/kg ND 5.0 08/01/11 12:08
p-Isopropyltoluene ug/kg ND 5.0 08/01/11 12:08
sec-Butylbenzene ug/kg ND 5.0 08/01/11 12:08
Styrene ug/kg ND 5.0 08/01/11 12:08
tert-Butylbenzene ug/kg ND 5.0 08/01/11 12:08
Tetrachloroethene ug/kg ND 5.0 08/01/11 12:08
Toluene ug/kg ND 5.0 08/01/11 12:08
trans-1,2-Dichloroethene ug/kg ND 5.0 08/01/11 12:08
trans-1,3-Dichloropropene ug/kg ND 5.0 08/01/11 12:08
Trichloroethene ug/kg ND 5.0 08/01/11 12:08
Trichlorofluoromethane ug/kg ND 5.0 08/01/11 12:08
Vinyl acetate ug/kg ND 50.0 08/01/11 12:08
Vinyl chloride ug/kg ND 10.0 08/01/11 12:08
Xylene (Total)ug/kg ND 10.0 08/01/11 12:08
1,2-Dichloroethane-d4 (S)%91 70-132 08/01/11 12:08
4-Bromofluorobenzene (S)%97 70-130 08/01/11 12:08
Dibromofluoromethane (S)%97 70-130 08/01/11 12:08
Toluene-d8 (S)%103 70-130 08/01/11 12:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
641119LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 50.350 101 70-131
1,1,1-Trichloroethane ug/kg 47.250 94 70-141
1,1,2,2-Tetrachloroethane ug/kg 48.050 96 70-130
1,1,2-Trichloroethane ug/kg 49.150 98 70-132
1,1-Dichloroethane ug/kg 45.350 91 70-143
1,1-Dichloroethene ug/kg 43.450 87 70-137
1,1-Dichloropropene ug/kg 44.850 90 70-135
1,2,3-Trichlorobenzene ug/kg 48.950 98 69-153
1,2,3-Trichloropropane ug/kg 44.350 89 70-130
1,2,4-Trichlorobenzene ug/kg 50.650 101 55-171
1,2,4-Trimethylbenzene ug/kg 50.650 101 70-149
1,2-Dibromo-3-chloropropane ug/kg 48.750 97 68-141
1,2-Dibromoethane (EDB)ug/kg 46.350 93 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 83 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
641119LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 48.950 98 70-140
1,2-Dichloroethane ug/kg 43.950 88 70-137
1,2-Dichloropropane ug/kg 47.150 94 70-133
1,3,5-Trimethylbenzene ug/kg 49.950 100 70-143
1,3-Dichlorobenzene ug/kg 48.850 98 70-144
1,3-Dichloropropane ug/kg 46.550 93 70-132
1,4-Dichlorobenzene ug/kg 48.250 96 70-142
2,2-Dichloropropane ug/kg 47.750 95 68-152
2-Butanone (MEK)ug/kg 88.5J100 89 70-149
2-Chlorotoluene ug/kg 48.950 98 70-141
2-Hexanone ug/kg 88.4100 88 70-149
4-Chlorotoluene ug/kg 51.750 103 70-149
4-Methyl-2-pentanone (MIBK)ug/kg 93.2100 93 70-153
Acetone ug/kg 88.3J100 88 70-157
Benzene ug/kg 45.250 90 70-130
Bromobenzene ug/kg 47.050 94 70-141
Bromochloromethane ug/kg 44.550 89 70-149
Bromodichloromethane ug/kg 49.450 99 70-130
Bromoform ug/kg 46.050 92 70-131
Bromomethane ug/kg 44.950 90 64-136
Carbon tetrachloride ug/kg 47.250 94 70-154
Chlorobenzene ug/kg 49.550 99 70-135
Chloroethane ug/kg 47.650 95 68-151
Chloroform ug/kg 47.550 95 70-130
Chloromethane ug/kg 44.650 89 70-132
cis-1,2-Dichloroethene ug/kg 44.050 88 70-140
cis-1,3-Dichloropropene ug/kg 50.450 101 70-137
Dibromochloromethane ug/kg 49.050 98 70-130
Dibromomethane ug/kg 46.150 92 70-136
Dichlorodifluoromethane ug/kg 42.750 85 36-148
Diisopropyl ether ug/kg 45.850 92 70-139
Ethylbenzene ug/kg 47.950 96 70-137
Hexachloro-1,3-butadiene ug/kg 46.150 92 70-145
Isopropylbenzene (Cumene)ug/kg 50.950 102 70-141
m&p-Xylene ug/kg 97.9100 98 70-140
Methyl-tert-butyl ether ug/kg 45.450 91 45-150
Methylene Chloride ug/kg 43.250 86 70-133
n-Butylbenzene ug/kg 51.450 103 65-155
n-Propylbenzene ug/kg 50.150 100 70-148
Naphthalene ug/kg 51.650 103 70-148
o-Xylene ug/kg 49.850 100 70-141
p-Isopropyltoluene ug/kg 51.850 104 70-148
sec-Butylbenzene ug/kg 51.150 102 70-145
Styrene ug/kg 52.350 105 70-138
tert-Butylbenzene ug/kg 50.750 101 70-143
Tetrachloroethene ug/kg 49.850 100 70-140
Toluene ug/kg 45.750 91 70-130
trans-1,2-Dichloroethene ug/kg 43.050 86 70-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 84 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
641119LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 46.850 94 70-138
Trichloroethene ug/kg 48.250 96 70-132
Trichlorofluoromethane ug/kg 46.550 93 69-134
Vinyl acetate ug/kg 132100 132 24-161
Vinyl chloride ug/kg 46.950 94 55-140
Xylene (Total)ug/kg 148150 98 70-141
1,2-Dichloroethane-d4 (S)%87 70-132
4-Bromofluorobenzene (S)%105 70-130
Dibromofluoromethane (S)%94 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
641416MATRIX SPIKE SAMPLE:
MSSpike
Result
9299248001
1,1-Dichloroethene ug/kg 49.854.2 92 49-180ND
Benzene ug/kg 41.554.2 77 50-166ND
Chlorobenzene ug/kg 51.554.2 95 43-169ND
Toluene ug/kg 50.554.2 93 52-163ND
Trichloroethene ug/kg 48.054.2 89 49-167ND
1,2-Dichloroethane-d4 (S)%102 70-132
4-Bromofluorobenzene (S)%90 70-130
Dibromofluoromethane (S)%106 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result QualifiersRPDResult
9299303002
641417SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 85 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
Dup
Result QualifiersRPDResult
9299303002
641417SAMPLE DUPLICATE:
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg 74.8J56.1J
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 86 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
Parameter Units
Dup
Result QualifiersRPDResult
9299303002
641417SAMPLE DUPLICATE:
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%114 2094
4-Bromofluorobenzene (S)%87 187
Dibromofluoromethane (S)%114 1798
Toluene-d8 (S)%102 1104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 87 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/4086
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:9299302001, 9299302002, 9299302003, 9299302004, 9299302005, 9299302006, 9299302007
Parameter Units
Dup
Result QualifiersRPDResult
9299111001
640864SAMPLE DUPLICATE:
Percent Moisture %26.1 1522.4
Parameter Units
Dup
Result QualifiersRPDResult
9299303001
640865SAMPLE DUPLICATE:
Percent Moisture %13.1 1011.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 88 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/10250
EPA 7196
EPA 7196
7196 Chromium, Hexavalent
Associated Lab Samples:9299302001, 9299302002, 9299302003, 9299302004, 9299302005, 9299302006, 9299302007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:642188
Associated Lab Samples:9299302001, 9299302002, 9299302003, 9299302004, 9299302005, 9299302006, 9299302007
Matrix:Solid
Analyzed
Chromium, Hexavalent mg/kg ND 5.0 N208/04/11 13:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
642189LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 48.7 N2509790-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
642190MATRIX SPIKE SAMPLE:
MSSpike
Result
9299254021
Chromium, Hexavalent mg/kg 21.2 N224.2 87 75-125ND
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
642194MATRIX SPIKE SAMPLE:
MSSpike
Result
9299254022
Chromium, Hexavalent mg/kg 9.3 M0,N2214575-125ND
Parameter Units
Dup
Result QualifiersRPDResult
9299254023
642195SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND N2ND
Parameter Units
Dup
Result QualifiersRPDResult
9299254024
642196SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND N2ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 89 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Project No.:
Project:
9299302
1200 South Blvd 6228-11-5486
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.D6
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
The lab does not hold TNI accreditation for this parameter.N2
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:33 PM Page 90 of 90
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
August 08, 2011
LIMS USE: FR - ANDREW FRANTZ
LIMS OBJECT ID: 9299334
9299334
Project:
Pace Project No.:
RE:
Mr. Andrew Frantz
AMEC-Charlotte
2801 Yorkmont Road
Suite 100
Charlotte, NC 28208
1200 SOUTH BOULEVARD
Dear Mr. Frantz:
Enclosed are the analytical results for sample(s) received by the laboratory on July 29, 2011. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards, where applicable, unless otherwise narrated in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001South Carolina Drinking Water Cert. #: 99006003Virginia Drinking Water Certification #: 00213
Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031West Virginia Certification #: 357Virginia/VELAP Certification #: 460144
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030North Carolina Bioassay Certification #: 9
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001Virginia Certification #: 00072West Virginia Certification #: 356
Virgina/VELAP Certification #: 460147
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
9299334001 SB-18 EPA 8270 74 PASI-CBPJ
EPA 8260 64 PASI-CMCK
9299334003 SUMP 1 EPA 6010 7 PASI-ASHB
EPA 7470 1 PASI-AJMW
9299334004 SUMP 2 EPA 6010 7 PASI-ASHB
EPA 7470 1 PASI-AJMW
9299334005 SUMP 3 EPA 6010 7 PASI-ASHB
EPA 7470 1 PASI-AJMW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
Sample:SB-18 Lab ID:9299334001 Collected:07/29/11 09:00 Received:07/29/11 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 08/06/11 14:47 83-32-908/01/11 15:0010.0
Acenaphthylene ND ug/L 1 08/06/11 14:47 208-96-808/01/11 15:0010.0
Aniline ND ug/L 1 08/06/11 14:47 62-53-308/01/11 15:0010.0
Anthracene ND ug/L 1 08/06/11 14:47 120-12-708/01/11 15:0010.0
Benzo(a)anthracene ND ug/L 1 08/06/11 14:47 56-55-308/01/11 15:0010.0
Benzo(a)pyrene ND ug/L 1 08/06/11 14:47 50-32-808/01/11 15:0010.0
Benzo(b)fluoranthene ND ug/L 1 08/06/11 14:47 205-99-208/01/11 15:0010.0
Benzo(g,h,i)perylene ND ug/L 1 08/06/11 14:47 191-24-208/01/11 15:0010.0
Benzo(k)fluoranthene ND ug/L 1 08/06/11 14:47 207-08-908/01/11 15:0010.0
Benzoic Acid ND ug/L 1 08/06/11 14:47 65-85-008/01/11 15:0050.0
Benzyl alcohol ND ug/L 1 08/06/11 14:47 100-51-608/01/11 15:0020.0
4-Bromophenylphenyl ether ND ug/L 1 08/06/11 14:47 101-55-308/01/11 15:0010.0
Butylbenzylphthalate ND ug/L 1 08/06/11 14:47 85-68-708/01/11 15:0010.0
4-Chloro-3-methylphenol ND ug/L 1 08/06/11 14:47 59-50-708/01/11 15:0020.0
4-Chloroaniline ND ug/L 1 08/06/11 14:47 106-47-808/01/11 15:0020.0
bis(2-Chloroethoxy)methane ND ug/L 1 08/06/11 14:47 111-91-108/01/11 15:0010.0
bis(2-Chloroethyl) ether ND ug/L 1 08/06/11 14:47 111-44-408/01/11 15:0010.0
bis(2-Chloroisopropyl) ether ND ug/L 1 08/06/11 14:47 108-60-108/01/11 15:0010.0
2-Chloronaphthalene ND ug/L 1 08/06/11 14:47 91-58-708/01/11 15:0010.0
2-Chlorophenol ND ug/L 1 08/06/11 14:47 95-57-808/01/11 15:0010.0
4-Chlorophenylphenyl ether ND ug/L 1 08/06/11 14:47 7005-72-308/01/11 15:0010.0
Chrysene ND ug/L 1 08/06/11 14:47 218-01-908/01/11 15:0010.0
Dibenz(a,h)anthracene ND ug/L 1 08/06/11 14:47 53-70-308/01/11 15:0010.0
Dibenzofuran ND ug/L 1 08/06/11 14:47 132-64-908/01/11 15:0010.0
1,2-Dichlorobenzene ND ug/L 1 08/06/11 14:47 95-50-108/01/11 15:0010.0
1,3-Dichlorobenzene ND ug/L 1 08/06/11 14:47 541-73-108/01/11 15:0010.0
1,4-Dichlorobenzene ND ug/L 1 08/06/11 14:47 106-46-708/01/11 15:0010.0
3,3'-Dichlorobenzidine ND ug/L 1 08/06/11 14:47 91-94-108/01/11 15:0020.0
2,4-Dichlorophenol ND ug/L 1 08/06/11 14:47 120-83-208/01/11 15:0010.0
Diethylphthalate ND ug/L 1 08/06/11 14:47 84-66-208/01/11 15:0010.0
2,4-Dimethylphenol ND ug/L 1 08/06/11 14:47 105-67-908/01/11 15:0010.0
Dimethylphthalate ND ug/L 1 08/06/11 14:47 131-11-308/01/11 15:0010.0
Di-n-butylphthalate ND ug/L 1 08/06/11 14:47 84-74-208/01/11 15:0010.0
4,6-Dinitro-2-methylphenol ND ug/L 1 08/06/11 14:47 534-52-108/01/11 15:0020.0
2,4-Dinitrophenol ND ug/L 1 08/06/11 14:47 51-28-508/01/11 15:0050.0
2,4-Dinitrotoluene ND ug/L 1 08/06/11 14:47 121-14-208/01/11 15:0010.0
2,6-Dinitrotoluene ND ug/L 1 08/06/11 14:47 606-20-208/01/11 15:0010.0
Di-n-octylphthalate ND ug/L 1 08/06/11 14:47 117-84-008/01/11 15:0010.0
bis(2-Ethylhexyl)phthalate ND ug/L 1 08/06/11 14:47 117-81-708/01/11 15:006.0
Fluoranthene ND ug/L 1 08/06/11 14:47 206-44-008/01/11 15:0010.0
Fluorene ND ug/L 1 08/06/11 14:47 86-73-708/01/11 15:0010.0
Hexachloro-1,3-butadiene ND ug/L 1 08/06/11 14:47 87-68-308/01/11 15:0010.0
Hexachlorobenzene ND ug/L 1 08/06/11 14:47 118-74-108/01/11 15:0010.0
Hexachlorocyclopentadiene ND ug/L 1 08/06/11 14:47 77-47-408/01/11 15:0010.0
Hexachloroethane ND ug/L 1 08/06/11 14:47 67-72-108/01/11 15:0010.0
Indeno(1,2,3-cd)pyrene ND ug/L 1 08/06/11 14:47 193-39-508/01/11 15:0010.0
Isophorone ND ug/L 1 08/06/11 14:47 78-59-108/01/11 15:0010.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 4 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
Sample:SB-18 Lab ID:9299334001 Collected:07/29/11 09:00 Received:07/29/11 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
1-Methylnaphthalene ND ug/L 1 08/06/11 14:47 90-12-008/01/11 15:0010.0
2-Methylnaphthalene ND ug/L 1 08/06/11 14:47 91-57-608/01/11 15:0010.0
2-Methylphenol(o-Cresol)ND ug/L 1 08/06/11 14:47 95-48-708/01/11 15:0010.0
3&4-Methylphenol(m&p Cresol)ND ug/L 1 08/06/11 14:4708/01/11 15:0010.0
Naphthalene ND ug/L 1 08/06/11 14:47 91-20-308/01/11 15:0010.0
2-Nitroaniline ND ug/L 1 08/06/11 14:47 88-74-408/01/11 15:0050.0
3-Nitroaniline ND ug/L 1 08/06/11 14:47 99-09-208/01/11 15:0050.0
4-Nitroaniline ND ug/L 1 08/06/11 14:47 100-01-608/01/11 15:0020.0
Nitrobenzene ND ug/L 1 08/06/11 14:47 98-95-308/01/11 15:0010.0
2-Nitrophenol ND ug/L 1 08/06/11 14:47 88-75-508/01/11 15:0010.0
4-Nitrophenol ND ug/L 1 08/06/11 14:47 100-02-708/01/11 15:0050.0
N-Nitrosodimethylamine ND ug/L 1 08/06/11 14:47 62-75-908/01/11 15:0010.0
N-Nitroso-di-n-propylamine ND ug/L 1 08/06/11 14:47 621-64-708/01/11 15:0010.0
N-Nitrosodiphenylamine ND ug/L 1 08/06/11 14:47 86-30-608/01/11 15:0010.0
Pentachlorophenol ND ug/L 1 08/06/11 14:47 87-86-508/01/11 15:0025.0
Phenanthrene ND ug/L 1 08/06/11 14:47 85-01-808/01/11 15:0010.0
Phenol ND ug/L 1 08/06/11 14:47 108-95-208/01/11 15:0010.0
Pyrene ND ug/L 1 08/06/11 14:47 129-00-008/01/11 15:0010.0
1,2,4-Trichlorobenzene ND ug/L 1 08/06/11 14:47 120-82-108/01/11 15:0010.0
2,4,5-Trichlorophenol ND ug/L 1 08/06/11 14:47 95-95-408/01/11 15:0010.0
2,4,6-Trichlorophenol ND ug/L 1 08/06/11 14:47 88-06-208/01/11 15:0010.0
Nitrobenzene-d5 (S)56 %1 08/06/11 14:47 4165-60-008/01/11 15:0021-110
2-Fluorobiphenyl (S)62 %1 08/06/11 14:47 321-60-808/01/11 15:0027-110
Terphenyl-d14 (S)79 %1 08/06/11 14:47 1718-51-008/01/11 15:0031-107
Phenol-d6 (S)21 %1 08/06/11 14:47 13127-88-308/01/11 15:0010-110
2-Fluorophenol (S)32 %1 08/06/11 14:47 367-12-408/01/11 15:0012-110
2,4,6-Tribromophenol (S)71 %1 08/06/11 14:47 118-79-608/01/11 15:0027-110
8260 MSV Low Level Analytical Method: EPA 8260
Acetone 30.7 ug/L 1 08/04/11 04:08 67-64-125.0
Benzene ND ug/L 1 08/04/11 04:08 71-43-21.0
Bromobenzene ND ug/L 1 08/04/11 04:08 108-86-11.0
Bromochloromethane ND ug/L 1 08/04/11 04:08 74-97-51.0
Bromodichloromethane ND ug/L 1 08/04/11 04:08 75-27-41.0
Bromoform ND ug/L 1 08/04/11 04:08 75-25-21.0
Bromomethane ND ug/L 1 08/04/11 04:08 74-83-92.0
2-Butanone (MEK)ND ug/L 1 08/04/11 04:08 78-93-35.0
Carbon tetrachloride ND ug/L 1 08/04/11 04:08 56-23-51.0
Chlorobenzene ND ug/L 1 08/04/11 04:08 108-90-71.0
Chloroethane ND ug/L 1 08/04/11 04:08 75-00-31.0
Chloroform ND ug/L 1 08/04/11 04:08 67-66-31.0
Chloromethane ND ug/L 1 08/04/11 04:08 74-87-31.0
2-Chlorotoluene ND ug/L 1 08/04/11 04:08 95-49-81.0
4-Chlorotoluene ND ug/L 1 08/04/11 04:08 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 08/04/11 04:08 96-12-85.0
Dibromochloromethane ND ug/L 1 08/04/11 04:08 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 08/04/11 04:08 106-93-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 5 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
Sample:SB-18 Lab ID:9299334001 Collected:07/29/11 09:00 Received:07/29/11 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Dibromomethane ND ug/L 1 08/04/11 04:08 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 08/04/11 04:08 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 08/04/11 04:08 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 08/04/11 04:08 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 08/04/11 04:08 75-71-81.0
1,1-Dichloroethane ND ug/L 1 08/04/11 04:08 75-34-31.0
1,2-Dichloroethane ND ug/L 1 08/04/11 04:08 107-06-21.0
1,1-Dichloroethene ND ug/L 1 08/04/11 04:08 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 08/04/11 04:08 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 08/04/11 04:08 156-60-51.0
1,2-Dichloropropane ND ug/L 1 08/04/11 04:08 78-87-51.0
1,3-Dichloropropane ND ug/L 1 08/04/11 04:08 142-28-91.0
2,2-Dichloropropane ND ug/L 1 08/04/11 04:08 594-20-71.0
1,1-Dichloropropene ND ug/L 1 08/04/11 04:08 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 08/04/11 04:08 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 08/04/11 04:08 10061-02-61.0
Diisopropyl ether ND ug/L 1 08/04/11 04:08 108-20-31.0
Ethylbenzene ND ug/L 1 08/04/11 04:08 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 08/04/11 04:08 87-68-31.0
2-Hexanone ND ug/L 1 08/04/11 04:08 591-78-65.0
p-Isopropyltoluene ND ug/L 1 08/04/11 04:08 99-87-61.0
Methylene Chloride ND ug/L 1 08/04/11 04:08 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 08/04/11 04:08 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 08/04/11 04:08 1634-04-41.0
Naphthalene ND ug/L 1 08/04/11 04:08 91-20-31.0
Styrene ND ug/L 1 08/04/11 04:08 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 08/04/11 04:08 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 08/04/11 04:08 79-34-51.0
Tetrachloroethene ND ug/L 1 08/04/11 04:08 127-18-41.0
Toluene ND ug/L 1 08/04/11 04:08 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 08/04/11 04:08 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 08/04/11 04:08 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 08/04/11 04:08 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 08/04/11 04:08 79-00-51.0
Trichloroethene ND ug/L 1 08/04/11 04:08 79-01-61.0
Trichlorofluoromethane ND ug/L 1 08/04/11 04:08 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 08/04/11 04:08 96-18-41.0
Vinyl acetate ND ug/L 1 08/04/11 04:08 108-05-42.0
Vinyl chloride ND ug/L 1 08/04/11 04:08 75-01-41.0
Xylene (Total)ND ug/L 1 08/04/11 04:08 1330-20-72.0
m&p-Xylene ND ug/L 1 08/04/11 04:08 179601-23-12.0
o-Xylene ND ug/L 1 08/04/11 04:08 95-47-61.0
4-Bromofluorobenzene (S)93 %1 08/04/11 04:08 460-00-470-130
Dibromofluoromethane (S)105 %1 08/04/11 04:08 1868-53-770-130
1,2-Dichloroethane-d4 (S)112 %1 08/04/11 04:08 17060-07-070-130
Toluene-d8 (S)99 %1 08/04/11 04:08 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 6 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
Sample:SUMP 1 Lab ID:9299334003 Collected:07/29/11 12:00 Received:07/29/11 15:30 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 08/02/11 16:00
Arsenic ND mg/L 1 08/04/11 12:07 7440-38-208/03/11 15:050.025
Barium ND mg/L 1 08/04/11 12:07 7440-39-308/03/11 15:050.50
Cadmium ND mg/L 1 08/04/11 12:07 7440-43-908/03/11 15:050.0050
Chromium 0.13 mg/L 1 08/04/11 12:07 7440-47-308/03/11 15:050.025
Lead ND mg/L 1 08/04/11 12:07 7439-92-108/03/11 15:050.025
Selenium ND mg/L 1 08/04/11 12:07 7782-49-208/03/11 15:050.10
Silver ND mg/L 1 08/04/11 12:07 7440-22-408/03/11 15:050.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 08/02/11 16:00
Mercury ND ug/L 1 08/04/11 13:18 7439-97-608/03/11 14:200.20
Sample:SUMP 2 Lab ID:9299334004 Collected:07/29/11 13:00 Received:07/29/11 15:30 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 08/02/11 16:00
Arsenic ND mg/L 1 08/04/11 12:10 7440-38-208/03/11 15:050.025
Barium 0.85 mg/L 1 08/04/11 12:10 7440-39-308/03/11 15:050.50
Cadmium ND mg/L 1 08/04/11 12:10 7440-43-908/03/11 15:050.0050
Chromium ND mg/L 1 08/04/11 12:10 7440-47-308/03/11 15:050.025
Lead ND mg/L 1 08/04/11 12:10 7439-92-108/03/11 15:050.025
Selenium ND mg/L 1 08/04/11 12:10 7782-49-208/03/11 15:050.10
Silver ND mg/L 1 08/04/11 12:10 7440-22-408/03/11 15:050.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 08/02/11 16:00
Mercury ND ug/L 1 08/04/11 13:21 7439-97-608/03/11 14:200.20
Sample:SUMP 3 Lab ID:9299334005 Collected:07/29/11 13:30 Received:07/29/11 15:30 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 08/02/11 16:00
Arsenic ND mg/L 1 08/04/11 12:15 7440-38-208/03/11 15:050.025
Barium ND mg/L 1 08/04/11 12:15 7440-39-308/03/11 15:050.50
Cadmium ND mg/L 1 08/04/11 12:15 7440-43-908/03/11 15:050.0050
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 7 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
Sample:SUMP 3 Lab ID:9299334005 Collected:07/29/11 13:30 Received:07/29/11 15:30 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 08/02/11 16:00
Chromium 0.038 mg/L 1 08/04/11 12:15 7440-47-308/03/11 15:050.025
Lead ND mg/L 1 08/04/11 12:15 7439-92-108/03/11 15:050.025
Selenium ND mg/L 1 08/04/11 12:15 7782-49-208/03/11 15:050.10
Silver ND mg/L 1 08/04/11 12:15 7440-22-408/03/11 15:050.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 08/02/11 16:00
Mercury ND ug/L 1 08/04/11 13:23 7439-97-608/03/11 14:200.20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 8 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/8832
EPA 3010
EPA 6010
6010 MET TCLP
Associated Lab Samples:9299334003, 9299334004, 9299334005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:642482
Associated Lab Samples:9299334003, 9299334004, 9299334005
Matrix:Water
Analyzed
Arsenic mg/L ND 0.025 08/04/11 11:09
Barium mg/L ND 0.50 08/04/11 11:09
Cadmium mg/L ND 0.0050 08/04/11 11:09
Chromium mg/L ND 0.025 08/04/11 11:09
Lead mg/L ND 0.025 08/04/11 11:09
Selenium mg/L ND 0.10 08/04/11 11:09
Silver mg/L ND 0.025 08/04/11 11:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
642483LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/L 2.72.5 108 80-120
Barium mg/L 2.52.5 102 80-120
Cadmium mg/L 2.42.5 96 80-120
Chromium mg/L 2.42.5 96 80-120
Lead mg/L 2.22.5 90 80-120
Selenium mg/L 2.82.5 110 80-120
Silver mg/L 1.41.2 110 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
642484MATRIX SPIKE SAMPLE:
MSSpike
Result
9298752002
Arsenic mg/L 2.72.5 108 75-125<0.014
Barium mg/L 3.12.5 93 75-1250.76
Cadmium mg/L 2.42.5 96 75-125<0.0025
Chromium mg/L 2.42.5 96 75-125<0.0020
Lead mg/L 3.62.5 87 75-1251.4
Selenium mg/L 2.72.5 108 75-125<0.019
Silver mg/L 1.41.2 109 75-1250.0020J
Parameter Units
Dup
Result QualifiersRPDResult
9298917001
642485SAMPLE DUPLICATE:
Arsenic mg/L NDND
Barium mg/L 0.92 20.90
Cadmium mg/L NDND
Chromium mg/L NDND
Lead mg/L 0.28 00.28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 9 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
Parameter Units
Dup
Result QualifiersRPDResult
9298917001
642485SAMPLE DUPLICATE:
Selenium mg/L .031JND
Silver mg/L .0006JND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 10 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/3656
EPA 7470
EPA 7470
7470 Mercury TCLP
Associated Lab Samples:9299334003, 9299334004, 9299334005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:642463
Associated Lab Samples:9299334003, 9299334004, 9299334005
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 08/04/11 12:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
642464LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
642465MATRIX SPIKE SAMPLE:
MSSpike
Result
9298917001
Mercury ug/L 2.42.5 94 75-125ND
Parameter Units
Dup
Result QualifiersRPDResult
9298917002
642466SAMPLE DUPLICATE:
Mercury ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 11 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/14374
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:9299334001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:641270
Associated Lab Samples:9299334001
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 08/05/11 13:33
1,2-Dichlorobenzene ug/L ND 10.0 08/05/11 13:33
1,3-Dichlorobenzene ug/L ND 10.0 08/05/11 13:33
1,4-Dichlorobenzene ug/L ND 10.0 08/05/11 13:33
1-Methylnaphthalene ug/L ND 10.0 08/05/11 13:33
2,4,5-Trichlorophenol ug/L ND 10.0 08/05/11 13:33
2,4,6-Trichlorophenol ug/L ND 10.0 08/05/11 13:33
2,4-Dichlorophenol ug/L ND 10.0 08/05/11 13:33
2,4-Dimethylphenol ug/L ND 10.0 08/05/11 13:33
2,4-Dinitrophenol ug/L ND 50.0 08/05/11 13:33
2,4-Dinitrotoluene ug/L ND 10.0 08/05/11 13:33
2,6-Dinitrotoluene ug/L ND 10.0 08/05/11 13:33
2-Chloronaphthalene ug/L ND 10.0 08/05/11 13:33
2-Chlorophenol ug/L ND 10.0 08/05/11 13:33
2-Methylnaphthalene ug/L ND 10.0 08/05/11 13:33
2-Methylphenol(o-Cresol)ug/L ND 10.0 08/05/11 13:33
2-Nitroaniline ug/L ND 50.0 08/05/11 13:33
2-Nitrophenol ug/L ND 10.0 08/05/11 13:33
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 08/05/11 13:33
3,3'-Dichlorobenzidine ug/L ND 20.0 08/05/11 13:33
3-Nitroaniline ug/L ND 50.0 08/05/11 13:33
4,6-Dinitro-2-methylphenol ug/L ND 20.0 08/05/11 13:33
4-Bromophenylphenyl ether ug/L ND 10.0 08/05/11 13:33
4-Chloro-3-methylphenol ug/L ND 20.0 08/05/11 13:33
4-Chloroaniline ug/L ND 20.0 08/05/11 13:33
4-Chlorophenylphenyl ether ug/L ND 10.0 08/05/11 13:33
4-Nitroaniline ug/L ND 20.0 08/05/11 13:33
4-Nitrophenol ug/L ND 50.0 08/05/11 13:33
Acenaphthene ug/L ND 10.0 08/05/11 13:33
Acenaphthylene ug/L ND 10.0 08/05/11 13:33
Aniline ug/L ND 10.0 08/05/11 13:33
Anthracene ug/L ND 10.0 08/05/11 13:33
Benzo(a)anthracene ug/L ND 10.0 08/05/11 13:33
Benzo(a)pyrene ug/L ND 10.0 08/05/11 13:33
Benzo(b)fluoranthene ug/L ND 10.0 08/05/11 13:33
Benzo(g,h,i)perylene ug/L ND 10.0 08/05/11 13:33
Benzo(k)fluoranthene ug/L ND 10.0 08/05/11 13:33
Benzoic Acid ug/L ND 50.0 08/05/11 13:33
Benzyl alcohol ug/L ND 20.0 08/05/11 13:33
bis(2-Chloroethoxy)methane ug/L ND 10.0 08/05/11 13:33
bis(2-Chloroethyl) ether ug/L ND 10.0 08/05/11 13:33
bis(2-Chloroisopropyl) ether ug/L ND 10.0 08/05/11 13:33
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 08/05/11 13:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 12 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:641270
Associated Lab Samples:9299334001
Matrix:Water
Analyzed
Butylbenzylphthalate ug/L ND 10.0 08/05/11 13:33
Chrysene ug/L ND 10.0 08/05/11 13:33
Di-n-butylphthalate ug/L ND 10.0 08/05/11 13:33
Di-n-octylphthalate ug/L ND 10.0 08/05/11 13:33
Dibenz(a,h)anthracene ug/L ND 10.0 08/05/11 13:33
Dibenzofuran ug/L ND 10.0 08/05/11 13:33
Diethylphthalate ug/L ND 10.0 08/05/11 13:33
Dimethylphthalate ug/L ND 10.0 08/05/11 13:33
Fluoranthene ug/L ND 10.0 08/05/11 13:33
Fluorene ug/L ND 10.0 08/05/11 13:33
Hexachloro-1,3-butadiene ug/L ND 10.0 08/05/11 13:33
Hexachlorobenzene ug/L ND 10.0 08/05/11 13:33
Hexachlorocyclopentadiene ug/L ND 10.0 08/05/11 13:33
Hexachloroethane ug/L ND 10.0 08/05/11 13:33
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 08/05/11 13:33
Isophorone ug/L ND 10.0 08/05/11 13:33
N-Nitroso-di-n-propylamine ug/L ND 10.0 08/05/11 13:33
N-Nitrosodimethylamine ug/L ND 10.0 08/05/11 13:33
N-Nitrosodiphenylamine ug/L ND 10.0 08/05/11 13:33
Naphthalene ug/L ND 10.0 08/05/11 13:33
Nitrobenzene ug/L ND 10.0 08/05/11 13:33
Pentachlorophenol ug/L ND 25.0 08/05/11 13:33
Phenanthrene ug/L ND 10.0 08/05/11 13:33
Phenol ug/L ND 10.0 08/05/11 13:33
Pyrene ug/L ND 10.0 08/05/11 13:33
2,4,6-Tribromophenol (S)%63 27-110 08/05/11 13:33
2-Fluorobiphenyl (S)%65 27-110 08/05/11 13:33
2-Fluorophenol (S)%46 12-110 08/05/11 13:33
Nitrobenzene-d5 (S)%69 21-110 08/05/11 13:33
Phenol-d6 (S)%32 10-110 08/05/11 13:33
Terphenyl-d14 (S)%81 31-107 08/05/11 13:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
641271LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 27.350 55 10-110
1,2-Dichlorobenzene ug/L 28.150 56 10-110
1,3-Dichlorobenzene ug/L 25.450 51 10-110
1,4-Dichlorobenzene ug/L 26.250 52 10-110
1-Methylnaphthalene ug/L 34.250 68 21-110
2,4,5-Trichlorophenol ug/L 34.050 68 23-116
2,4,6-Trichlorophenol ug/L 40.150 80 21-114
2,4-Dichlorophenol ug/L 36.550 73 22-120
2,4-Dimethylphenol ug/L 31.150 62 15-109
2,4-Dinitrophenol ug/L 183250 73 10-103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 13 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
641271LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dinitrotoluene ug/L 38.250 76 24-119
2,6-Dinitrotoluene ug/L 38.750 77 25-116
2-Chloronaphthalene ug/L 37.450 75 18-110
2-Chlorophenol ug/L 38.150 76 10-104
2-Methylnaphthalene ug/L 34.150 68 16-110
2-Methylphenol(o-Cresol)ug/L 39.050 78 13-110
2-Nitroaniline ug/L 85.0100 85 20-117
2-Nitrophenol ug/L 37.850 76 16-108
3&4-Methylphenol(m&p Cresol)ug/L 39.250 78 14-110
3,3'-Dichlorobenzidine ug/L 61.6100 62 13-131
3-Nitroaniline ug/L 71.4100 71 15-117
4,6-Dinitro-2-methylphenol ug/L 81.8100 82 13-119
4-Bromophenylphenyl ether ug/L 39.050 78 23-120
4-Chloro-3-methylphenol ug/L 80.1100 80 21-119
4-Chloroaniline ug/L 74.4100 74 10-122
4-Chlorophenylphenyl ether ug/L 36.750 73 22-112
4-Nitroaniline ug/L 65.4100 65 14-118
4-Nitrophenol ug/L 106250 42 10-110
Acenaphthene ug/L 37.750 75 20-105
Acenaphthylene ug/L 36.550 73 23-106
Aniline ug/L 36.150 72 10-110
Anthracene ug/L 38.450 77 25-120
Benzo(a)anthracene ug/L 38.850 78 21-128
Benzo(a)pyrene ug/L 36.450 73 25-116
Benzo(b)fluoranthene ug/L 37.450 75 23-117
Benzo(g,h,i)perylene ug/L 35.850 72 17-128
Benzo(k)fluoranthene ug/L 36.850 74 25-127
Benzoic Acid ug/L 107250 43 10-110
Benzyl alcohol ug/L 91.6100 92 10-101
bis(2-Chloroethoxy)methane ug/L 38.250 76 19-107
bis(2-Chloroethyl) ether ug/L 41.650 83 10-108
bis(2-Chloroisopropyl) ether ug/L 40.850 82 10-108
bis(2-Ethylhexyl)phthalate ug/L 41.050 82 16-123
Butylbenzylphthalate ug/L 40.650 81 20-118
Chrysene ug/L 38.850 78 24-125
Di-n-butylphthalate ug/L 39.950 80 23-115
Di-n-octylphthalate ug/L 37.250 74 20-115
Dibenz(a,h)anthracene ug/L 34.550 69 18-131
Dibenzofuran ug/L 38.250 76 23-106
Diethylphthalate ug/L 38.250 76 24-115
Dimethylphthalate ug/L 38.250 76 22-113
Fluoranthene ug/L 36.550 73 24-125
Fluorene ug/L 36.950 74 24-114
Hexachloro-1,3-butadiene ug/L 22.150 44 10-110
Hexachlorobenzene ug/L 39.150 78 22-127
Hexachlorocyclopentadiene ug/L 34.350 69 10-110
Hexachloroethane ug/L 25.350 51 10-110
Indeno(1,2,3-cd)pyrene ug/L 35.050 70 18-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 14 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
641271LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/L 42.650 85 23-114
N-Nitroso-di-n-propylamine ug/L 48.050 96 21-114
N-Nitrosodimethylamine ug/L 26.850 54 10-110
N-Nitrosodiphenylamine ug/L 39.250 78 24-123
Naphthalene ug/L 31.650 63 14-110
Nitrobenzene ug/L 38.150 76 16-106
Pentachlorophenol ug/L 77.6100 78 10-123
Phenanthrene ug/L 38.150 76 25-119
Phenol ug/L 26.450 53 10-110
Pyrene ug/L 39.250 78 22-127
2,4,6-Tribromophenol (S)%90 27-110
2-Fluorobiphenyl (S)%74 27-110
2-Fluorophenol (S)%50 12-110
Nitrobenzene-d5 (S)%71 21-110
Phenol-d6 (S)%47 10-110
Terphenyl-d14 (S)%78 31-107
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
641272MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299262008
641273
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 100 55 10-11062 11100ND55.4 61.8
1,2-Dichlorobenzene ug/L 100 58 10-11063 7100ND58.2 62.7
1,3-Dichlorobenzene ug/L 100 56 10-11062 10100ND55.8 61.6
1,4-Dichlorobenzene ug/L 100 58 10-11063 8100ND57.8 62.6
1-Methylnaphthalene ug/L 100 61 14-11070 13100ND61.2 69.9
2,4,5-Trichlorophenol ug/L 100 60 19-10567 12100ND59.9 67.3
2,4,6-Trichlorophenol ug/L 100 70 13-10877 9100ND69.9 76.8
2,4-Dichlorophenol ug/L 100 64 29-11174 13100ND64.3 73.6
2,4-Dimethylphenol ug/L 100 60 21-10364 6100ND60.1 63.9
2,4-Dinitrophenol ug/L 500 60 10-10966 10500ND300332
2,4-Dinitrotoluene ug/L 100 90 27-10492 2100ND89.8 91.5
2,6-Dinitrotoluene ug/L 100 79 28-10187 9100ND79.3 87.1
2-Chloronaphthalene ug/L 100 67 14-10272 7100ND67.5 72.1
2-Chlorophenol ug/L 100 68 16-11072 6100ND67.8 72.1
2-Methylnaphthalene ug/L 100 62 13-11070 13100ND61.6 70.1
2-Methylphenol(o-Cresol)ug/L 100 59 19-11064 8100ND58.8 63.8
2-Nitroaniline ug/L 200 90 26-103101 11200ND180202
2-Nitrophenol ug/L 100 65 20-11074 12100ND65.1 73.8
3&4-Methylphenol(m&p
Cresol)ug/L 100 54 20-11060 11100ND53.8 60.0
3,3'-Dichlorobenzidine ug/L 200 66 25-11254 20200ND133109
3-Nitroaniline ug/L 200 83 29-11084 1200ND167168
4,6-Dinitro-2-methylphenol ug/L 200 71 10-11771 1200ND143142
4-Bromophenylphenyl ether ug/L 100 67 20-10576 13100ND67.1 76.4
4-Chloro-3-methylphenol ug/L 200 73 22-11090 21200ND146181
4-Chloroaniline ug/L 200 68 20-10071 4200ND136142
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 15 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
641272MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299262008
641273
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
4-Chlorophenylphenyl ether ug/L 100 72 19-10281 12100ND72.2 81.2
4-Nitroaniline ug/L 200 98 29-11088 11200ND196176
4-Nitrophenol ug/L 500 61 10-11066 7500ND307331
Acenaphthene ug/L 100 71 17-10079 10100ND71.5 79.2
Acenaphthylene ug/L 100 68 21-10075 11100ND67.9 75.5
Aniline ug/L R11006110-11041 38100ND60.8 41.4
Anthracene ug/L 100 79 24-10981 3100ND78.7 80.9
Benzo(a)anthracene ug/L 100 73 22-11776 4100ND72.9 75.9
Benzo(a)pyrene ug/L 100 69 23-10474 6100ND69.4 73.7
Benzo(b)fluoranthene ug/L 100 69 23-10374 7100ND68.7 73.9
Benzo(g,h,i)perylene ug/L 100 70 18-11173 4100ND70.0 72.7
Benzo(k)fluoranthene ug/L 100 73 22-11379 7100ND73.3 78.8
Benzoic Acid ug/L 500 17 10-11055500ND86.2J 277
Benzyl alcohol ug/L 200 67 19-10176 12200ND135151
bis(2-Chloroethoxy)methane ug/L 100 71 22-11081 13100ND70.7 80.6
bis(2-Chloroethyl) ether ug/L 100 76 16-11077 2100ND76.1 77.5
bis(2-Chloroisopropyl) ether ug/L 100 70 14-11075 8100ND69.9 75.3
bis(2-Ethylhexyl)phthalate ug/L 100 74 23-10279 6100ND74.1 78.7
Butylbenzylphthalate ug/L 100 72 25-11080 11100ND72.2 80.3
Chrysene ug/L 100 75 23-11579 5100ND74.8 78.6
Di-n-butylphthalate ug/L 100 93 26-11087 7100ND93.3 87.1
Di-n-octylphthalate ug/L 100 63 22-11063 0100ND63.1 63.4
Dibenz(a,h)anthracene ug/L 100 66 21-11268 3100ND65.6 67.6
Dibenzofuran ug/L 100 74 19-10282 10100ND74.4 81.9
Diethylphthalate ug/L 100 92 29-11092 1100ND91.7 92.4
Dimethylphthalate ug/L 100 84 27-11088 5100ND83.6 88.0
Fluoranthene ug/L 100 89 23-11277 15100ND89.1 76.7
Fluorene ug/L 100 75 22-10482 10100ND74.7 82.4
Hexachloro-1,3-butadiene ug/L 100 47 10-11054 14100ND47.2 54.4
Hexachlorobenzene ug/L 100 72 21-11677 7100ND71.5 76.6
Hexachlorocyclopentadiene ug/L 100 56 10-11055 1100ND55.6 54.9
Hexachloroethane ug/L 100 56 10-11061 9100ND55.5 61.0
Indeno(1,2,3-cd)pyrene ug/L 100 67 20-11370 3100ND67.2 69.6
Isophorone ug/L 100 77 50-15094 20100ND77.2 94.4
N-Nitroso-di-n-propylamine ug/L 100 67 21-10576 13100ND66.8 76.1
N-Nitrosodimethylamine ug/L 100 59 10-11069 15100ND59.4 69.2
N-Nitrosodiphenylamine ug/L 100 73 23-10780 9100ND73.2 80.4
Naphthalene ug/L 100 62 10-11069 10100ND62.0 68.6
Nitrobenzene ug/L 100 72 20-11080 11100ND71.7 80.3
Pentachlorophenol ug/L 200 68 10-11868 1200ND137135
Phenanthrene ug/L 100 77 24-10679 3100ND77.0 79.2
Phenol ug/L 100 46 12-11051 11100ND45.7 51.1
Pyrene ug/L 100 67 24-11481 19100ND66.9 81.3
2,4,6-Tribromophenol (S)%75 27-11082
2-Fluorobiphenyl (S)%66 27-11068
2-Fluorophenol (S)%50 12-11058
Nitrobenzene-d5 (S)%69 21-11075
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 16 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
641272MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299262008
641273
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenol-d6 (S)%40 10-11046
Terphenyl-d14 (S)%68 31-10780
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 17 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/16190
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:9299334001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:642253
Associated Lab Samples:9299334001
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/04/11 01:36
1,1,1-Trichloroethane ug/L ND 1.0 08/04/11 01:36
1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/04/11 01:36
1,1,2-Trichloroethane ug/L ND 1.0 08/04/11 01:36
1,1-Dichloroethane ug/L ND 1.0 08/04/11 01:36
1,1-Dichloroethene ug/L ND 1.0 08/04/11 01:36
1,1-Dichloropropene ug/L ND 1.0 08/04/11 01:36
1,2,3-Trichlorobenzene ug/L ND 1.0 08/04/11 01:36
1,2,3-Trichloropropane ug/L ND 1.0 08/04/11 01:36
1,2,4-Trichlorobenzene ug/L ND 1.0 08/04/11 01:36
1,2-Dibromo-3-chloropropane ug/L ND 5.0 08/04/11 01:36
1,2-Dibromoethane (EDB)ug/L ND 1.0 08/04/11 01:36
1,2-Dichlorobenzene ug/L ND 1.0 08/04/11 01:36
1,2-Dichloroethane ug/L ND 1.0 08/04/11 01:36
1,2-Dichloropropane ug/L ND 1.0 08/04/11 01:36
1,3-Dichlorobenzene ug/L ND 1.0 08/04/11 01:36
1,3-Dichloropropane ug/L ND 1.0 08/04/11 01:36
1,4-Dichlorobenzene ug/L ND 1.0 08/04/11 01:36
2,2-Dichloropropane ug/L ND 1.0 08/04/11 01:36
2-Butanone (MEK)ug/L ND 5.0 08/04/11 01:36
2-Chlorotoluene ug/L ND 1.0 08/04/11 01:36
2-Hexanone ug/L ND 5.0 08/04/11 01:36
4-Chlorotoluene ug/L ND 1.0 08/04/11 01:36
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 08/04/11 01:36
Acetone ug/L ND 25.0 08/04/11 01:36
Benzene ug/L ND 1.0 08/04/11 01:36
Bromobenzene ug/L ND 1.0 08/04/11 01:36
Bromochloromethane ug/L ND 1.0 08/04/11 01:36
Bromodichloromethane ug/L ND 1.0 08/04/11 01:36
Bromoform ug/L ND 1.0 08/04/11 01:36
Bromomethane ug/L ND 2.0 08/04/11 01:36
Carbon tetrachloride ug/L ND 1.0 08/04/11 01:36
Chlorobenzene ug/L ND 1.0 08/04/11 01:36
Chloroethane ug/L ND 1.0 08/04/11 01:36
Chloroform ug/L ND 1.0 08/04/11 01:36
Chloromethane ug/L ND 1.0 08/04/11 01:36
cis-1,2-Dichloroethene ug/L ND 1.0 08/04/11 01:36
cis-1,3-Dichloropropene ug/L ND 1.0 08/04/11 01:36
Dibromochloromethane ug/L ND 1.0 08/04/11 01:36
Dibromomethane ug/L ND 1.0 08/04/11 01:36
Dichlorodifluoromethane ug/L ND 1.0 08/04/11 01:36
Diisopropyl ether ug/L ND 1.0 08/04/11 01:36
Ethylbenzene ug/L ND 1.0 08/04/11 01:36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 18 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:642253
Associated Lab Samples:9299334001
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 1.0 08/04/11 01:36
m&p-Xylene ug/L ND 2.0 08/04/11 01:36
Methyl-tert-butyl ether ug/L ND 1.0 08/04/11 01:36
Methylene Chloride ug/L ND 2.0 08/04/11 01:36
Naphthalene ug/L ND 1.0 08/04/11 01:36
o-Xylene ug/L ND 1.0 08/04/11 01:36
p-Isopropyltoluene ug/L ND 1.0 08/04/11 01:36
Styrene ug/L ND 1.0 08/04/11 01:36
Tetrachloroethene ug/L ND 1.0 08/04/11 01:36
Toluene ug/L ND 1.0 08/04/11 01:36
trans-1,2-Dichloroethene ug/L ND 1.0 08/04/11 01:36
trans-1,3-Dichloropropene ug/L ND 1.0 08/04/11 01:36
Trichloroethene ug/L ND 1.0 08/04/11 01:36
Trichlorofluoromethane ug/L ND 1.0 08/04/11 01:36
Vinyl acetate ug/L ND 2.0 08/04/11 01:36
Vinyl chloride ug/L ND 1.0 08/04/11 01:36
Xylene (Total)ug/L ND 2.0 08/04/11 01:36
1,2-Dichloroethane-d4 (S)%108 70-130 08/04/11 01:36
4-Bromofluorobenzene (S)%94 70-130 08/04/11 01:36
Dibromofluoromethane (S)%105 70-130 08/04/11 01:36
Toluene-d8 (S)%99 70-130 08/04/11 01:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
642254LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.550 103 70-130
1,1,1-Trichloroethane ug/L 53.350 107 70-130
1,1,2,2-Tetrachloroethane ug/L 52.550 105 70-130
1,1,2-Trichloroethane ug/L 52.750 105 70-130
1,1-Dichloroethane ug/L 52.650 105 70-130
1,1-Dichloroethene ug/L 51.450 103 70-132
1,1-Dichloropropene ug/L 48.650 97 70-130
1,2,3-Trichlorobenzene ug/L 53.850 108 70-135
1,2,3-Trichloropropane ug/L 48.450 97 70-130
1,2,4-Trichlorobenzene ug/L 53.050 106 70-134
1,2-Dibromo-3-chloropropane ug/L 49.750 99 70-130
1,2-Dibromoethane (EDB)ug/L 52.350 105 70-130
1,2-Dichlorobenzene ug/L 53.550 107 70-130
1,2-Dichloroethane ug/L 53.350 107 70-130
1,2-Dichloropropane ug/L 52.950 106 70-130
1,3-Dichlorobenzene ug/L 50.750 101 70-130
1,3-Dichloropropane ug/L 50.650 101 70-130
1,4-Dichlorobenzene ug/L 50.050 100 70-130
2,2-Dichloropropane ug/L 51.450 103 58-145
2-Butanone (MEK)ug/L 103100 103 70-145
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 19 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
642254LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorotoluene ug/L 53.050 106 70-130
2-Hexanone ug/L 103100 103 70-144
4-Chlorotoluene ug/L 52.850 106 70-130
4-Methyl-2-pentanone (MIBK)ug/L 110100 110 70-140
Acetone ug/L 103100 103 50-175
Benzene ug/L 48.650 97 70-130
Bromobenzene ug/L 50.250 100 70-130
Bromochloromethane ug/L 53.050 106 70-130
Bromodichloromethane ug/L 53.950 108 70-130
Bromoform ug/L 52.750 105 70-130
Bromomethane ug/L 62.150 124 54-130
Carbon tetrachloride ug/L 54.850 110 70-132
Chlorobenzene ug/L 51.650 103 70-130
Chloroethane ug/L 60.350 121 64-134
Chloroform ug/L 54.450 109 70-130
Chloromethane ug/L 54.950 110 64-130
cis-1,2-Dichloroethene ug/L 51.650 103 70-131
cis-1,3-Dichloropropene ug/L 55.550 111 70-130
Dibromochloromethane ug/L 51.550 103 70-130
Dibromomethane ug/L 51.550 103 70-131
Dichlorodifluoromethane ug/L 94.0 F3,L35018856-130
Diisopropyl ether ug/L 53.250 106 70-130
Ethylbenzene ug/L 49.850 100 70-130
Hexachloro-1,3-butadiene ug/L 51.150 102 70-130
m&p-Xylene ug/L 102100 102 70-130
Methyl-tert-butyl ether ug/L 56.750 113 70-130
Methylene Chloride ug/L 53.550 107 63-130
Naphthalene ug/L 53.950 108 70-138
o-Xylene ug/L 52.750 105 70-130
p-Isopropyltoluene ug/L 51.950 104 70-130
Styrene ug/L 54.150 108 70-130
Tetrachloroethene ug/L 49.350 99 70-130
Toluene ug/L 49.450 99 70-130
trans-1,2-Dichloroethene ug/L 51.750 103 70-130
trans-1,3-Dichloropropene ug/L 56.750 113 70-132
Trichloroethene ug/L 52.050 104 70-130
Trichlorofluoromethane ug/L 53.650 107 62-133
Vinyl acetate ug/L 116100 116 66-157
Vinyl chloride ug/L 64.050 128 69-130
Xylene (Total)ug/L 155150 103 70-130
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%96 70-130
Dibromofluoromethane (S)%104 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 20 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
642255MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9299255001
642256
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 50 100 70-166100 050ND49.8 49.9
Benzene ug/L 50 100 70-14899 150ND49.8 49.3
Chlorobenzene ug/L 50 118 70-146117 150ND59.0 58.4
Toluene ug/L 50 114 70-155112 250ND56.8 55.9
Trichloroethene ug/L 50 115 69-151113 250ND57.6 56.5
1,2-Dichloroethane-d4 (S)%112 70-130115
4-Bromofluorobenzene (S)%90 70-13089
Dibromofluoromethane (S)%105 70-130107
Toluene-d8 (S)%96 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 21 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Project No.:
Project:
9299334
1200 SOUTH BOULEVARD
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 08/08/2011 03:46 PM Page 22 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
APPENDIX D
2011 GEOPHYSICAL SURVEY REPORT

September 13, 2011

Mr. Andy Clark
AMEC
2801 Yorkmont Road, Suite 100
Charlotte, North Carolina 28208

Re: Geophysical Investigation of Potential Underground Storage Tanks, 1200 South
Boulevard, Charlotte, NC

Dear Mr. Clark:

Geo Solutions Limited, Inc. (Geo Solutions) is pleased to submit this report of findings for a
geophysical survey completed on September 2, 2011 at 1200 South Boulevard, Charlotte, NC.

Aerial photograph of site illustrating the survey boundary and buildings, 1200 South Blvd,
Charlotte, NC
Background

AMEC is currently conducting an Environmental Assessment at three combined site located at
1200 South Boulevard, Charlotte, NC. AMEC has been informed that a portion of the property
may contain former underground storage tanks (USTs). Geo Solutions was asked to complete a
two phase geophysical evaluation using a full site multifrequency electromagnetic detector (EM)
and ground-penetrating radar (GPR).

Field Activities
Geo Solutions completed two types of geophysical surveys as part of the investigation:

1. Geo Solutions completed an initial EM survey over the paved and grassy surfaces
surrounding the building. . The detailed EM evaluation (survey lines spaced at
approximately 3 to 5-ft and data points every 0.5 feet along each profile line). These data
were collected utilizing a Geophex Model GEM-2. The location of the data points were
measured utilizing a CSI GPS that directly records the location of each EM data point.
From these data, Geo Solutions prepared a site map illustrating the distribution of in-
phase (metal detection mode) and quadrature (apparent conductivity) values (Figures 1
and 2, respectively).

2. Geo Solutions also completed a limited Ground-penetrating radar (GPR) evaluation of
portions of the site where anomalous EM results indicated potential buried debris or other
anomalous subsurface conditions.

Results

EM Evaluation

The EM results are presented in Figures 1, and 2.

Figure 1 illustrates the results of the 53370 Hz in-phase data. This information is generally used
to indicate the location of buried metal material. This would include but not limited to: buried
concrete with metal reinforcement, buried underground storage tanks (USTs), septic tanks, and
utilities.

Geo Solutions identified several anomalous features that corresponded to observed surface
features, and several apparent subsurface utility features (as shown on Figures 1 and 2). The
presence of a reinforced concrete pad located in the parking lot of the existing building shows a
strong in-phase signal

Figure 2 illustrates the sum/average of all computed electrical conductivity values collected at
the site. Electrical conductivity data conforms to similar anomalies identified in Figure 1 (in-
phase data) with the exception of the suspected. The presence of a reinforced concrete pad
located in the parking lot of the existing building shows a strong electrical conductivity signal.
Typical of UST features, the in-phase anomaly is generally strong (red) and the quadrature
values weak or not present.
GPR Evaluation

Geo Solutions completed GPR evaluations over the area of the property that may have an UST.
As such, the only area extensively evaluated included the steel reinforced concrete pad located in
the parking lot of the existing building. Here the presence of metal reinforcement prohibited the
detection of the UST using the EM unit. Geo Solutions completed a cross-grid survey over the
entire concrete pad. Here we discovered a shallow reflective surface located approximately 2 ft.
beneath the existing concrete surface. We suspect this may be a former land surface and may
represent a former drive surface. The maximum detection depth at this site is 4-ft bls. As a
result, given the typical UST setting depth for the area is 2 to 3 feet, it may not be possible to
detect UST at great depth at the portion of the site.

Conclusions and Recommendations

Based on the results of the expanded EM evaluation, Geo Solutions did not recognize the
presence of any USTs at this site. However, Geo Solutions was not able to fully evaluate, at
depth great enough to rule out the presence of USTs beneath the reinforced concrete pad at the
existing building. As such, USTs greater than 4 to 5 feet in depth may not have been detected.

Geo Solutions is pleased to have been provided this opportunity to be of assistance, please give
me a call should you have questions concerning the above.

Very truly yours,

GEO SOLUTIONS LIMITED, INC.

Ronald A. Crowson
Geophysicist

Figures 1 through 2