10042_Southside_Prpty_Phase_II_Soil_Mgmt_Plan

Phase II Soil Management Plan
Carolina Metals Site

2208-2222 South Blvd.
Charlotte, North Carolina

Brownfields Project No. 10042-06-60

H&H Job No. SLS-001
February 26, 2013
i

S:\AAA-Master Projects\Stiles - SLS\SLS-001 South Blvd\SMP\Soil Mgmt Plan Phase II.doc
Phase II Soil Management Plan
Carolina Metals Site
2208-2222 South Blvd.
Charlotte, North Carolina
H&H Job No. SLS-001

Table of Contents
Section Page
1.0 Introduction ................................................................................................................ 1 
2.0 February 2013 Soil Assessment ................................................................................ 4 
2.1 Sampling Methodology ............................................................................................ 4 
2.2 Soil Analytical Results ............................................................................................. 5 

3.0 Proposed Environmental Action .............................................................................. 6 

List of Tables

Table 1 Summary of Soil Analytical Data

List of Figures

Figure 1 Site Location Map
Figure 2 Approved Fill Soil for Use at Southline Site – Phase I SMP
Figure 3 Soil Sample Locations and Phase II SMP

List of Appendices

Appendix A Boring Logs
Appendix B Laboratory Analytical Report

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Phase II Soil Management Plan
Carolina Metals Site
2208-2222 South Blvd.
Charlotte, North Carolina
H&H Job No. SLS-001

1.0 Introduction

Hart & Hickman, PC has prepared this Phase II Soil Management Plan (SMP) for the
Carolina Metals Brownfields site located at 2208-2222 South Blvd. in Charlotte
(Brownfields Project ID 10042-06-60). A site location map is presented as Figure 1. The
purpose of the SMP is to present measures to address soil that will be excavated during
redevelopment of the site.

The subject property is 4.16 acres in area and contains an approximate 16,000 sq ft
commercial building located in the northeastern portion of the site. Four other buildings
were previously located at the site but have been demolished, although their foundations
remain. The site is bordered to the west by the Charlotte light rail line with residences
located beyond, to the south by vacant land (which is part of the Southline Brownfields
project which is to be redeveloped as apartments by Camden), to the north by the
Atherton Lofts live/work condominiums and a bank, and the east by South Blvd. with a
Lowe’s Home Improvement Center located beyond.

The redevelopment plans for the site include demolition of the existing structure and
foundations and construction of a large commercial building that will be used for retail
purposes by several tenants. The remainder of the property will primarily be paved
access areas, although there will be some landscape strips. A two-level subterranean
parking structure will underlie the commercial building, with 1.5 levels below ground
that will be mechanically vented per code.

The grading plan calls for net export of approximately 38,800 cubic yards of soil from the
site. A grading plan with anticipated cut and fill depths and areas is provided as Figure 2.
Cut areas and depths are shown in red, and fill areas and depths are shown in green. Cut

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depths generally range from 10 to 23 ft from current grade in the central and eastern
portions of the site to less than 1 to 3 ft below current grade in the northern portion of the
site. Fill depths are primarily in the west-central and southern portions of the site and
range from less than 1 ft to approximately 11 ft from current grade.

In November 2012, H&H evaluated previous soil assessment data to determine what
areas of the cut soils had been previously sampled and to propose a plan to manage these
soils. The results of the evaluation were presented in a Phase I SMP dated November 19,
2012 that included the following:

 Cut soil from 0 to 5 ft in southern portion of the site (enclosed in dashed red lines
on Figure 2), and soil from 0 to 3 ft in the northwestern portion of the site
(enclosed in dashed purple lines on Figure 2) will be transported to the adjacent
Southline Brownfields project located at 2300 and 2316 South Blvd (which is
located south of the Carolina Metals site) and used for fill. The volume of this
soil is approximately 8,900 cubic yards.

 Because of the presence of several polynuclear aromatic hydrocarbons (PAHs) in
the GP-15 soil sample above North Carolina Department of Environment and
Natural Resources (DENR) Inactive Hazardous Sites Branch Soil Remediation
Goals (SRGs), cut soil in the area of previous sample location GP-15 as depicted
on Figure 2 will be used for on-site fill either in the southern portion of the site or
in the adjacent fill area to the east of sample GP-15. Both of these areas will be
covered with pavement after completion of the site construction activities.

The Phase I SMP was approved by the North Carolina Department of Environment and
Natural Resources (DENR) in a letter dated January 24, 2013. As part of the approval
letter DENR specified the following conditions:

 Soil excavated must be moved directly to the adjacent Southline Brownfields site
and must not be taken on any roads.

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 DENR must be notified of any unusual conditions within 24 hours.
 DENR must be notified of placement of soil and the Brownfields plat must be
updated accordingly.

As part of the Phase I SMP, H&H proposed that additional soil samples be collected at
locations and depths of the proposed cut soil not included in the Phase I SMP so that
appropriate management of that soil could be determined. H&H conducted the additional
soil assessment in February 2013. The methods and results of the soil sampling activities
and a plan for management of the remaining areas of cut fill are summarized in the
following sections.

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2.0 February 2013 Soil Assessment

2.1 Sampling Methodology

On February 6, 2013, five soil borings were advanced to characterize cut soil at the site
which has not been previously sampled. H&H utilized Probe Technology, Inc. of
Concord, North Carolina to advance the soil borings using Geoprobe® direct-push
technology (DPT) equipment. Soil cores were continuously retrieved within acetate
sleeves for visual characterization and soil vapor screening using a photo-ionization
detector (PID). Boring logs including PID readings are provided in Appendix A. One or
two 4 ft long samples were collected from each soil boring for laboratory analysis.

The locations of the proposed soil borings are indicated on Figure 3 and are described
below:

 Soil borings SB-A and SB-B were advanced in areas where shallow soils had
been previously assessed to a depth of 4 ft and cut depths are approximately 11 ft.
Therefore, a soil sample from each of these borings was collected from 6 to 10 ft
below ground surface (bgs).

 Soil borings SB-C and SB-E were advanced in areas where previous samples had
not been collected and where excavation depths up to approximately 23 ft below
current grade are planned. Soil samples were collected from these borings at
depths of 6 to 10 ft bgs and 16 to 20 ft bgs.

 Soil boring SB-D was advanced in an area where previous samples had not been
collected and where excavation depths are up to approximately 16 ft below
current grade. Soil samples were collected from this boring at depths of 4 to 8 ft
bgs and 12 to 16 ft bgs.

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All eight of the soil samples were analyzed for volatile organic compounds (VOCs) by
EPA Method 8260, PAHs by EPA Method 8270, and the following nine metals: arsenic,
cadmium, total chromium, hexavalent chromium, lead, mercury, nickel, selenium, and
thallium by EPA Method 6010/7471/7196A. The samples were submitted to
TestAmerica, Inc., a North Carolina-certified laboratory. Dedicated laboratory-supplied
sample kits and bottles were used for sample collection. The samples were placed in an
iced cooler after collection. A chain-of-custody record was completed for the samples
collected and included the sample description, date collected, time collected, matrix,
sample container information, and analyses required. The chain-of-custody was signed
by H&H prior to placement in the iced sample cooler for delivery to the laboratory.
2.2 Soil Analytical Results

The results of the soil sample analyses are summarized in Table 1, and the laboratory
analytical report is provided in Appendix B.

The results indicate that VOCs and PAHs were not detected above the laboratory
reporting limits in any of the eight soil samples. Several metals including chromium,
lead, nickel, and selenium were detected in the soil samples; however, the detected
concentrations are well below the DENR Inactive Hazardous Sites Branch (IHSB)
Residential and Commercial/Industrial SRGs and are consistent with typical background
levels. Results of the chromium speciation indicated that hexavalent chromium was not
detected above the laboratory reporting limits in any of the samples; therefore, the
detected chromium concentrations (13.7 mg/kg to 65.0 mg/kg) are comprised of trivalent
chromium. The detected trivalent concentrations are well below the SRG for trivalent
chromium.

The results of analysis of the additional soil samples did not indicate the presence of soil
impacts that would warrant special management of the soil.

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3.0 Proposed Environmental Action

Based upon the existing soil analytical data, shallow and deeper soil at the site is not
impacted above Residential or Commercial/Industrial SRGs, except for an isolated area
near sample GP-15 in the west-central portion of the site.

H&H has developed a Phase II SMP based upon the soil analytical data for the site. Soil
in the following areas will be managed as described below:

1. As approved in the Phase I SMP, cut soil in the area of previous sample location
GP-15 (enclosed in dashed blue lines on Figure 3) will be used for on-site fill
either in the southern portion of the site or in the adjacent fill area to the east of
sample GP-15. As mentioned in Section 2.0, both of these areas will be covered
with pavement after completion of the site construction activities. DENR will be
notified of the location of these soils, and the Brownfields plat will be updated as
needed. The total volume of this soil is approximately 3,200 cubic yards (based
on an average cut depth of 10 ft) as indicated on Figure 3.

2. Up to approximately 22,000 cubic yards of cut soil in the area enclosed in dashed
red lines on Figure 3 will be excavated during site redevelopment and transported
to the adjacent Southline Brownfields project located at 2300 and 2316 South
Blvd and used for fill. The soil will be transported directly across the property
boundary and will not be taken on any roads.

3. The cut soil that is not used as fill at the Southline Brownfields project
(approximately 16,800 cubic yards) will be transported off-site for use as fill or to
a permitted landfill. At this time, the Developer (South End Partners, LLC) is
evaluating options for off-site placement of the cut soil not taken to the adjacent
Southline Brownfields site. DENR will be notified of the off-site proposed fill
placement location(s) for review and approval prior to transporting the cut soil
off-site.
Table 1 (Page 1 of 1)
Summary of Soil Analytical Data
Carolina Metals Site2208-2222 South Blvd.
Charlotte, North Carolina
H&H Job No. SLS-001
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2/22/2013
Table 1 (Page 1 of 1)
Hart & Hickman, PC
Sample ID GP-4 GP-5 GP-6 GP-7 GP-8 GP-9 GP-10 GP-11 GP-12 GP-13 GP-14 GP-15 SB-A SB-B
Depth (ft bgs)0-4 0-4 0-4 0-4 0-4 0-4 0-4 0-4 0-4 4-8 0-4 4-8 0-4 0-4 0-4 0-4 6-8 6-8 6-10 6-10 6-10 16-20 4-8 12-16 6-10 16-20
Sample Date 7/17/2000 7/18/2000 7/17/2000 7/19/2000 7/17/2000 7/17/2000 7/17/2000 7/17/2000 7/17/2000 7/18/2000 7/18/2000 7/18/2000 7/18/2000 3/11/2008 7/18/2000 3/11/2008 7/20/2006 3/11/2008 2/6/2013 2/6/2013 2/6/2013 2/6/2013 2/6/2013 2/6/2013 2/6/2013 2/6/2013
Units (mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)
VOCs (8260B)All ND All ND All ND All ND All ND All ND All ND All ND All ND All ND All ND All ND All ND NA All ND NA NA NA All ND All ND All ND All ND All ND All ND All ND All ND NA NA
SVOCs (8270C)
Fluoranthene <0.42 <0.45 <0.48 <0.47 <0.43 <0.44 <0.44 <0.48 <0.42 <0.44 <0.44 0.85 <0.43 NA <0.44 NA NA NA <0.0979 <0.101 <0.0858 <0.00275 <0.0843 <0.0942 <0.0905 <0.0890 460 4,400
Phenanthrene <0.42 <0.45 <0.48 <0.47 <0.43 <0.44 <0.44 <0.48 <0.42 <0.44 0.80 0.49 <0.43 NA <0.44 NA NA NA <0.0979 <0.101 <0.0858 <0.00275 <0.0843 <0.0942 <0.0905 <0.0890 NE NE
Pyrene <0.42 <0.45 <0.48 <0.47 <0.43 <0.44 <0.44 <0.48 <0.42 <0.44 <0.44 1.0 <0.43 NA <0.44 NA NA NA <0.0979 <0.101 <0.0858 <0.00275 <0.0843 <0.0942 <0.0905 <0.0890 340 3,400
Chrysene <0.42 <0.45 <0.48 <0.47 <0.43 <0.44 <0.44 <0.48 <0.42 <0.44 0.56 0.53 <0.43 NA <0.44 NA NA NA <0.0979 <0.101 <0.0858 <0.00275 <0.0843 <0.0942 <0.0905 <0.0890 15 210
Fluorene <0.42 <0.45 <0.48 <0.47 <0.43 <0.44 <0.44 <0.48 <0.42 <0.44 0.63 <0.35 <0.43 NA <0.44 NA NA NA <0.0979 <0.101 <0.0858 <0.00275 <0.0843 <0.0942 <0.0905 <0.0890 460 4,400
Benzo(a)anthracene <0.42 <0.45 <0.48 <0.47 <0.43 <0.44 <0.44 <0.48 <0.42 <0.44 <0.44 0.49 <0.43 NA <0.44 NA NA NA <0.0979 <0.101 <0.0858 <0.00275 <0.0843 <0.0942 <0.0905 <0.0890 0.15 2.1
Benzo(b)fluoranthene <0.42 <0.45 <0.48 <0.47 <0.43 <0.44 <0.44 <0.48 <0.42 <0.44 <0.44 0.56 <0.43 NA <0.44 NA NA NA <0.0979 <0.101 <0.0858 <0.00275 <0.0843 <0.0942 <0.0905 <0.0890 0.15 2.1
Benzo(a)pyrene <0.42 <0.45 <0.48 <0.47 <0.43 <0.44 <0.44 <0.48 <0.42 <0.44 <0.44 0.48 <0.43 NA <0.44 NA NA NA <0.0979 <0.101 <0.0858 <0.00275 <0.0843 <0.0942 <0.0905 <0.0890 0.015 0.21
Metals (6010/7471A/7196)
Arsenic <0.32 <0.34 <0.37 <0.36 <0.33 <0.34 <0.34 <0.36 <0.32 <0.33 <0.33 <0.27 <0.33 NA <0.33 NA <0.130 NA <1.52 <3.05 <2.51 <2.90 <2.47 <2.87 <2.66 <1.35 0.39 1.6
Barium 43 35 58 40 7.2 70 16 17 20 36 50 94 250 NA 190 NA NA NA NA NA NA NA NA NA NA NA 3,000 38,000
Cadmium 1 2.1 1.6 2.5 0.67 1.5 1.1 4 1.5 2.4 2.7 1.2 1.4 NA 1 NA NA NA <1.52 <3.05 <2.51 <2.90 <2.47 <2.87 <2.66 <1.35 14 160
Total Chromium 4.1 16 25.0 37.0 29.0 2.2 18 23 13 41 40 17 47 124 90 59.8 44.5 11.8 25.7 65.0 39.8 38.9 25.8 28.7 34.9 13.7 NE NE
Hexavalent Chromium NA NA NA NA NA NA NA NA NA NA NA NA NA <2.56 NA <2.57 NA <2.41 <7.54 <7.56 <6.59 <7.27 <6.48 <7.20 <6.94 <6.81 0.29 5.6
Trivalent Chromium NA NA NA NA NA NA NA NA NA NA NA NA NA 124 NA 59.8 NA 11.8 25.7 65.0 39.8 38.9 25.8 28.7 34.9 13.7 24,000 100,000
Lead 14 12 14 10 2.3 2.2 4.1 12 7.3 10 14 28 1.5 NA 0.79 NA NA NA 7.30 15.1 9.74 24.3 9.84 5.62 13.9 3.68 400 800
Mercury <0.025 <0.027 0.039 0.031 <0.026 0.046 0.034 0.034 0.036 0.28 0.29 0.078 <0.026 NA 0.036 NA NA NA <0.152 <0.146 <0.127 <0.141 <0.126 <0.143 <0.138 <0.136 2 3.1
Nickel NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 11.4 15.7 8.84 9.97 7.42 10.1 8.77 7.06 300 4,000
Selenium 1.1 2.2 1.8 2.7 <0.33 1.5 0.71 4 1.6 3 3 1.7 1.5 NA 0.99 NA NA NA 4.44 <6.10 5.88 6.49 5.29 <5.73 <5.31 3.43 78 1,000
Silver <0.13 <0.14 <0.15 <0.14 <0.13 <0.14 <0.14 <0.14 <0.13 <0.13 <0.13 <0.11 <0.13 NA <0.13 NA NA NA NA NA NA NA NA NA NA NA 78 1,000
Notes:Yellow highlighting indicates samples collected in February 2013.Green highlighting indicates concentration exceeds Residential SRGOrange highlighting indicates concentration exceeds Commercial/Industrial SRGSoil Remediation Goals (SRGs) from North Carolina Department of Environment and Natural Resources (DENR) Inactive Hazardous Sites Branch (IHSB) Preliminary SRG Table dated July 2012. Only those organic compounds detected in at least one sample shown above
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compoundsNE = not established; NA = not analyzed/not applicable; ND = not detectedmg/kg = milligrams per kilogram
DENR IHSB
Residential Use SRG
DENR IHSB
Industrial Use SRG
GP-17/HA-1 GP-18/HA-2 SB-EBG-2/HA-3 SB-C SB-D
TITLE
PROJECT
SITE LOCATION MAP
CAROLINA METALS SITE
2208-2222 SOUTH BOULEVARD
CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE NO:
2-21-13 0
1SLS-001
0 2000 4000
APPROXIMATE
SCALE IN FEETN
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
CHARLOTTE EAST, NC 1993
CHARLOTTE WEST, NC 1993
SITE
Figure 2 –Approved Fill Soil for Use at Southline Site –Phase I SMP
Figure 3 –Soil Sample Locations and Phase II SMP
Notes:
1.Green numbers are
depth of fill
2.Red numbers are
cut thickness
SB-A
SB-B
SB-C
SB-D
SB-E
GP-15 Cut Area (soil to remain on-site)
February 2013 Soil
Boring Location
Legend:
General Cut Areas (soil to be moved off-site)

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Appendix A

Boring Logs
BORING STARTED:2/6/13
DRAWN BY:RJC
BORING COMPLETED:2/6/13
DRILLING CONTRACTOR:Probe Technology Remarks:
DRILL RIG/ METHOD:6620DT / DPT
0
Soil sample collected from 6 to 10 ft bgs
0
LOGGED BY:RJC
TOTAL DEPTH:10 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
SAMPLING METHOD:Macrocore Sampler
2.1
1.7
2.4
0 1.7
Concrete
Slightly moist, medium stiff, red, clayey SILT
Dry, medium stiff, red and orange, fine sandy SILT
Bottom of borehole at 10.0 feet.
0
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1.3
Sheet 1 of 1
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PROJECT:Carolina Metals Site
LOCATION:Charlotte, North Carolina
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2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
JOB NUMBER:SLS-001
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BORING NUMBER SB-A
BORING DIAGRAM
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TOP OF CASING ELEV:
DRAWN BY:RJC
BORING COMPLETED:2/6/13
DRILLING CONTRACTOR:Probe Technology Remarks:
DRILL RIG/ METHOD:6620DT / DPT
SAMPLING METHOD:Macrocore Sampler Soil sample collected from 6 to 10 ft bgs
BORING STARTED:2/6/13
TOTAL DEPTH:10 ft.
0
DEPTH TO WATER:
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LOGGED BY:RJC
Slightly moist, medium stiff, red/orange/tan, fine sandy SILT
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Moist, medium stiff, brown/tan/orange, clayey SILT w/ fine sand
Bottom of borehole at 10.0 feet.
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BORING NUMBER SB-B
PROJECT:Carolina Metals Site
JOB NUMBER:SLS-001
Sheet 1 of 1
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2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)LOCATION:Charlotte, North Carolina
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Remarks:
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DRAWN BY:RJC
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DRILLING CONTRACTOR:Probe Technology
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DRILL RIG/ METHOD:6620DT / DPT
SAMPLING METHOD:Macrocore Sampler Soil samples collected from 6 to 10 ft and
16 to 20 ft bgs
BORING STARTED:2/6/13
LOGGED BY:RJC
TOTAL DEPTH:20 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
BORING COMPLETED:2/6/13
2.2
0.6
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0.7
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2.10
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Slightly moist, stiff, orangish red, silty CLAY
Dry, medium stiff, orange and brown, clayey SILT
Bottom of borehole at 20.0 feet.
0
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LOCATION:Charlotte, North Carolina
Sheet 1 of 1
BORING NUMBER SB-C
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JOB NUMBER:SLS-001
BORING DIAGRAM
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2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
PROJECT:Carolina Metals Site
DE
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MATERIAL DESCRIPTIONOV
A

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0
5
10
15
20
0
5
10
15
20
DRILLING CONTRACTOR:Probe Technology
0.3
0
0.3
0.1
0.5
0.7
0.7
BORING COMPLETED:2/6/13
Remarks:
DRILL RIG/ METHOD:6620DT / DPT
SAMPLING METHOD:Macrocore Sampler Soil samples collected from 4 to 8 ft and
12 to 16 ft bgs
BORING STARTED:2/6/13
LOGGED BY:RJC
TOTAL DEPTH:16 ft.
DEPTH TO WATER:DRAWN BY:RJC
0.7
0.2
0.3
0
0.3
0.2
0.5
0.7
Concrete
Dry, medium dense, brown, silty fine SAND
Slightly moist, stiff, red, silty CLAY
Moist, medium stiff, red, clayey SILT
Bottom of borehole at 16.0 feet.
0.7
LOCATION:Charlotte, North Carolina
TOP OF CASING ELEV:
Sheet 1 of 1
BORING NUMBER SB-D
JOB NUMBER:SLS-001
BORING DIAGRAM
BO
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2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
PROJECT:Carolina Metals Site
LI
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L
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G
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MATERIAL DESCRIPTION
RE
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(
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)
BK
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.
0
5
10
15
0
5
10
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BORING COMPLETED:2/6/13
0
0
0
0
0
0
0.2
0.4
0.5
DRAWN BY:RJC
DRILLING CONTRACTOR:Probe Technology Remarks:
DRILL RIG/ METHOD:6620DT / DPT
SAMPLING METHOD:Macrocore Sampler Soil samples collected from 6 to 10 ft and
16 to 20 ft bgs
BORING STARTED:2/6/13
LOGGED BY:RJC TOP OF CASING ELEV:
0.6
0
0
0
0.5
0.4
0
0.6
0.5
1
Slightly moist, medium stiff, brownish red, silty CLAY
Slightly moist, medium stiff, tan and orange, SILT
Moist, stiff, red/orange/tan, SILT
Moist, soft, tan and light brown, fine sandy SILT
Bottom of borehole at 20.0 feet.
DEPTH TO WATER:
0.4
JOB NUMBER:SLS-001
BORING DIAGRAM
TOTAL DEPTH:20 ft.
Sheet 1 of 1
BORING NUMBER SB-E
SA
M
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NU
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PROJECT:Carolina Metals Site
LOCATION:Charlotte, North Carolina
BO
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2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
DE
P
T
H
(f
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)
DE
P
T
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MATERIAL DESCRIPTION
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20

S:\AAA-Master Projects\Stiles - SLS\SLS-001 South Blvd\SMP\Soil Mgmt Plan Phase II.doc
Appendix B

Laboratory Analytical Report
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-18944-1
TestAmerica Sample Delivery Group: SLS-001
Client Project/Site: Carolina Metals Site
For:
Hart & Hickman, PC
2923 S Tryon Street
Suite 100
Charlotte, North Carolina 28203
Attn: Steve Hart
Authorized for release by:
2/14/2013 11:41:17 AM
Ken Hayes
Project Manager I
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Hart & Hickman, PC
Project/Site: Carolina Metals Site
TestAmerica Job ID: 490-18944-1
SDG: SLS-001
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Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .51
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .55
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .56
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .57
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59
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Sample Summary
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-18944-1 SB-A (6-10')Solid 02/06/13 12:05 02/07/13 08:20
490-18944-2 SB-B (6-10')Solid 02/06/13 12:15 02/07/13 08:20
490-18944-3 SB-C (6-10')Solid 02/06/13 10:15 02/07/13 08:20
490-18944-4 SB-C (16-20')Solid 02/06/13 10:20 02/07/13 08:20
490-18944-5 SB-D (4-8')Solid 02/06/13 11:25 02/07/13 08:20
490-18944-6 SB-D (12-16')Solid 02/06/13 11:30 02/07/13 08:20
490-18944-7 SB-E (6-10')Solid 02/06/13 10:50 02/07/13 08:20
490-18944-8 SB-E (16-20')Solid 02/06/13 11:00 02/07/13 08:20
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Definitions/Glossary
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Qualifiers
GC/MS VOA
Qualifier Description
*LCS or LCSD exceeds the control limits
Qualifier
GC/MS Semi VOA
Qualifier Description
X Surrogate is outside control limits
Qualifier
Metals
Qualifier Description
L A negative instrument reading had an absolute value greater than the reporting limit
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
☼Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
EDL Estimated Detection Limit
EPA United States Environmental Protection Agency
MDA Minimum detectable activity
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-1Client Sample ID: SB-A (6-10')
Matrix: SolidDate Collected: 02/06/13 12:05
Percent Solids: 66.3Date Received: 02/07/13 08:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0733 mg/Kg ☼02/08/13 10:02 02/11/13 18:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Benzene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Bromobenzene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Bromochloromethane ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Bromodichloromethane ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Bromoform ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Bromomethane ND
0.0733 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼2-Butanone (MEK)ND *
0.00733 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Carbon disulfide ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Carbon tetrachloride ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Chlorobenzene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Chlorodibromomethane ND
0.00733 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Chloroethane ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Chloroform ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Chloromethane ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼2-Chlorotoluene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼4-Chlorotoluene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼cis-1,2-Dichloroethene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼cis-1,3-Dichloropropene ND
0.00733 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,2-Dibromo-3-Chloropropane ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,2-Dibromoethane (EDB)ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Dibromomethane ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,2-Dichlorobenzene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,3-Dichlorobenzene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,4-Dichlorobenzene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Dichlorodifluoromethane ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,1-Dichloroethane ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,2-Dichloroethane ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,1-Dichloroethene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,2-Dichloroethene, Total ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,2-Dichloropropane ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,3-Dichloropropane ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼2,2-Dichloropropane ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,1-Dichloropropene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Ethylbenzene ND
0.00733 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Hexachlorobutadiene ND
0.0733 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼2-Hexanone ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Isopropylbenzene ND
0.0147 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Methylene Chloride ND
0.0733 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼4-Methyl-2-pentanone (MIBK)ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Methyl tert-butyl ether ND
0.00733 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Naphthalene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼n-Butylbenzene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼N-Propylbenzene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼p-Isopropyltoluene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼sec-Butylbenzene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Styrene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼tert-Butylbenzene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,1,1,2-Tetrachloroethane ND
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-1Client Sample ID: SB-A (6-10')
Matrix: SolidDate Collected: 02/06/13 12:05
Percent Solids: 66.3Date Received: 02/07/13 08:20
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,2,2-Tetrachloroethane ND 0.00293 mg/Kg ☼02/08/13 10:02 02/11/13 18:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Tetrachloroethene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Toluene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼trans-1,2-Dichloroethene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼trans-1,3-Dichloropropene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,2,3-Trichlorobenzene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,2,4-Trichlorobenzene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,1,1-Trichloroethane ND
0.00733 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,1,2-Trichloroethane ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Trichloroethene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Trichlorofluoromethane ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,2,3-Trichloropropane ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,2,4-Trimethylbenzene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼1,3,5-Trimethylbenzene ND
0.00293 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Vinyl chloride ND
0.00733 mg/Kg 02/08/13 10:02 02/11/13 18:48 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)95 70-130 02/08/13 10:02 02/11/13 18:48 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)100 02/08/13 10:02 02/11/13 18:48 170-130
1,2-Dichloroethane-d4 (Surr)101 02/08/13 10:02 02/11/13 18:48 170-130
Toluene-d8 (Surr)95 02/08/13 10:02 02/11/13 18:48 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0979 mg/Kg ☼02/08/13 10:48 02/10/13 00:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0979 mg/Kg 02/08/13 10:48 02/10/13 00:46 1☼Acenaphthylene ND
0.0979 mg/Kg 02/08/13 10:48 02/10/13 00:46 1☼Anthracene ND
0.0979 mg/Kg 02/08/13 10:48 02/10/13 00:46 1☼Benzo[a]anthracene ND
0.0979 mg/Kg 02/08/13 10:48 02/10/13 00:46 1☼Benzo[a]pyrene ND
0.0979 mg/Kg 02/08/13 10:48 02/10/13 00:46 1☼Benzo[b]fluoranthene ND
0.0979 mg/Kg 02/08/13 10:48 02/10/13 00:46 1☼Benzo[g,h,i]perylene ND
0.0979 mg/Kg 02/08/13 10:48 02/10/13 00:46 1☼Benzo[k]fluoranthene ND
0.0979 mg/Kg 02/08/13 10:48 02/10/13 00:46 1☼Chrysene ND
0.0979 mg/Kg 02/08/13 10:48 02/10/13 00:46 1☼Dibenz(a,h)anthracene ND
0.0979 mg/Kg 02/08/13 10:48 02/10/13 00:46 1☼Fluoranthene ND
0.0979 mg/Kg 02/08/13 10:48 02/10/13 00:46 1☼Fluorene ND
0.0979 mg/Kg 02/08/13 10:48 02/10/13 00:46 1☼Indeno[1,2,3-cd]pyrene ND
0.0979 mg/Kg 02/08/13 10:48 02/10/13 00:46 1☼Naphthalene ND
0.0979 mg/Kg 02/08/13 10:48 02/10/13 00:46 1☼Phenanthrene ND
0.0979 mg/Kg 02/08/13 10:48 02/10/13 00:46 1☼Pyrene ND
2-Fluorobiphenyl (Surr)69 29-120 02/08/13 10:48 02/10/13 00:46 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)63 02/08/13 10:48 02/10/13 00:46 127-120
Terphenyl-d14 (Surr)88 02/08/13 10:48 02/10/13 00:46 113-120
Method: 6010C - Metals (ICP)
RL MDL
Arsenic ND 1.52 mg/Kg ☼02/09/13 10:48 02/12/13 10:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-1Client Sample ID: SB-A (6-10')
Matrix: SolidDate Collected: 02/06/13 12:05
Percent Solids: 66.3Date Received: 02/07/13 08:20
Method: 6010C - Metals (ICP) (Continued)
RL MDL
Cadmium ND L 1.52 mg/Kg ☼02/09/13 10:48 02/12/13 10:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.52 mg/Kg 02/09/13 10:48 02/12/13 10:06 1☼Chromium 25.7
1.52 mg/Kg 02/09/13 10:48 02/12/13 10:06 1☼Lead 7.30
3.04 mg/Kg 02/09/13 10:48 02/12/13 10:06 1☼Nickel 11.4
3.04 mg/Kg 02/09/13 10:48 02/12/13 10:06 1☼Selenium 4.44
3.04 mg/Kg 02/09/13 10:48 02/12/13 10:06 1☼Thallium ND
Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique)
RL MDL
Mercury ND 0.152 mg/Kg ☼02/12/13 14:01 02/13/13 08:57 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chromium, hex ND 7.54 mg/Kg ☼02/08/13 15:46 02/13/13 15:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
RL RL
Percent Solids 66 0.10 %02/08/13 08:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-2Client Sample ID: SB-B (6-10')
Matrix: SolidDate Collected: 02/06/13 12:15
Percent Solids: 66.1Date Received: 02/07/13 08:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0630 mg/Kg ☼02/08/13 10:02 02/11/13 19:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Benzene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Bromobenzene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Bromochloromethane ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Bromodichloromethane ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Bromoform ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Bromomethane ND
0.0630 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼2-Butanone (MEK)ND *
0.00630 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Carbon disulfide ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Carbon tetrachloride ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Chlorobenzene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Chlorodibromomethane ND
0.00630 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Chloroethane ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Chloroform ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Chloromethane ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼2-Chlorotoluene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼4-Chlorotoluene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼cis-1,2-Dichloroethene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼cis-1,3-Dichloropropene ND
0.00630 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,2-Dibromo-3-Chloropropane ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,2-Dibromoethane (EDB)ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Dibromomethane ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,2-Dichlorobenzene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,3-Dichlorobenzene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,4-Dichlorobenzene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Dichlorodifluoromethane ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,1-Dichloroethane ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,2-Dichloroethane ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,1-Dichloroethene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,2-Dichloroethene, Total ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,2-Dichloropropane ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,3-Dichloropropane ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼2,2-Dichloropropane ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,1-Dichloropropene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Ethylbenzene ND
0.00630 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Hexachlorobutadiene ND
0.0630 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼2-Hexanone ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Isopropylbenzene ND
0.0126 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Methylene Chloride ND
0.0630 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼4-Methyl-2-pentanone (MIBK)ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Methyl tert-butyl ether ND
0.00630 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Naphthalene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼n-Butylbenzene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼N-Propylbenzene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼p-Isopropyltoluene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼sec-Butylbenzene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Styrene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼tert-Butylbenzene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,1,1,2-Tetrachloroethane ND
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-2Client Sample ID: SB-B (6-10')
Matrix: SolidDate Collected: 02/06/13 12:15
Percent Solids: 66.1Date Received: 02/07/13 08:20
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,2,2-Tetrachloroethane ND 0.00252 mg/Kg ☼02/08/13 10:02 02/11/13 19:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Tetrachloroethene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Toluene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼trans-1,2-Dichloroethene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼trans-1,3-Dichloropropene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,2,3-Trichlorobenzene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,2,4-Trichlorobenzene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,1,1-Trichloroethane ND
0.00630 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,1,2-Trichloroethane ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Trichloroethene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Trichlorofluoromethane ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,2,3-Trichloropropane ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,2,4-Trimethylbenzene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼1,3,5-Trimethylbenzene ND
0.00252 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Vinyl chloride ND
0.00630 mg/Kg 02/08/13 10:02 02/11/13 19:19 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)94 70-130 02/08/13 10:02 02/11/13 19:19 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)100 02/08/13 10:02 02/11/13 19:19 170-130
1,2-Dichloroethane-d4 (Surr)102 02/08/13 10:02 02/11/13 19:19 170-130
Toluene-d8 (Surr)94 02/08/13 10:02 02/11/13 19:19 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.101 mg/Kg ☼02/08/13 10:48 02/10/13 01:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.101 mg/Kg 02/08/13 10:48 02/10/13 01:11 1☼Acenaphthylene ND
0.101 mg/Kg 02/08/13 10:48 02/10/13 01:11 1☼Anthracene ND
0.101 mg/Kg 02/08/13 10:48 02/10/13 01:11 1☼Benzo[a]anthracene ND
0.101 mg/Kg 02/08/13 10:48 02/10/13 01:11 1☼Benzo[a]pyrene ND
0.101 mg/Kg 02/08/13 10:48 02/10/13 01:11 1☼Benzo[b]fluoranthene ND
0.101 mg/Kg 02/08/13 10:48 02/10/13 01:11 1☼Benzo[g,h,i]perylene ND
0.101 mg/Kg 02/08/13 10:48 02/10/13 01:11 1☼Benzo[k]fluoranthene ND
0.101 mg/Kg 02/08/13 10:48 02/10/13 01:11 1☼Chrysene ND
0.101 mg/Kg 02/08/13 10:48 02/10/13 01:11 1☼Dibenz(a,h)anthracene ND
0.101 mg/Kg 02/08/13 10:48 02/10/13 01:11 1☼Fluoranthene ND
0.101 mg/Kg 02/08/13 10:48 02/10/13 01:11 1☼Fluorene ND
0.101 mg/Kg 02/08/13 10:48 02/10/13 01:11 1☼Indeno[1,2,3-cd]pyrene ND
0.101 mg/Kg 02/08/13 10:48 02/10/13 01:11 1☼Naphthalene ND
0.101 mg/Kg 02/08/13 10:48 02/10/13 01:11 1☼Phenanthrene ND
0.101 mg/Kg 02/08/13 10:48 02/10/13 01:11 1☼Pyrene ND
2-Fluorobiphenyl (Surr)59 29-120 02/08/13 10:48 02/10/13 01:11 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)49 02/08/13 10:48 02/10/13 01:11 127-120
Terphenyl-d14 (Surr)69 02/08/13 10:48 02/10/13 01:11 113-120
Method: 6010C - Metals (ICP)
RL MDL
Arsenic ND 3.05 mg/Kg ☼02/09/13 10:48 02/12/13 11:17 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-2Client Sample ID: SB-B (6-10')
Matrix: SolidDate Collected: 02/06/13 12:15
Percent Solids: 66.1Date Received: 02/07/13 08:20
Method: 6010C - Metals (ICP) (Continued)
RL MDL
Cadmium ND 3.05 mg/Kg ☼02/09/13 10:48 02/12/13 11:17 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.05 mg/Kg 02/09/13 10:48 02/12/13 11:17 2☼Chromium 65.0
3.05 mg/Kg 02/09/13 10:48 02/12/13 11:17 2☼Lead 15.1
6.10 mg/Kg 02/09/13 10:48 02/12/13 11:17 2☼Nickel 15.7
6.10 mg/Kg 02/09/13 10:48 02/12/13 11:17 2☼Selenium ND
6.10 mg/Kg 02/09/13 10:48 02/12/13 11:17 2☼Thallium ND
Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique)
RL MDL
Mercury ND 0.146 mg/Kg ☼02/12/13 14:01 02/13/13 09:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chromium, hex ND 7.56 mg/Kg ☼02/08/13 15:46 02/13/13 15:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
RL RL
Percent Solids 66 0.10 %02/08/13 08:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-3Client Sample ID: SB-C (6-10')
Matrix: SolidDate Collected: 02/06/13 10:15
Percent Solids: 75.9Date Received: 02/07/13 08:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0647 mg/Kg ☼02/08/13 10:02 02/11/13 19:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Benzene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Bromobenzene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Bromochloromethane ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Bromodichloromethane ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Bromoform ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Bromomethane ND
0.0647 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼2-Butanone (MEK)ND *
0.00647 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Carbon disulfide ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Carbon tetrachloride ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Chlorobenzene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Chlorodibromomethane ND
0.00647 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Chloroethane ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Chloroform ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Chloromethane ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼2-Chlorotoluene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼4-Chlorotoluene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼cis-1,2-Dichloroethene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼cis-1,3-Dichloropropene ND
0.00647 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,2-Dibromo-3-Chloropropane ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,2-Dibromoethane (EDB)ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Dibromomethane ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,2-Dichlorobenzene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,3-Dichlorobenzene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,4-Dichlorobenzene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Dichlorodifluoromethane ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,1-Dichloroethane ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,2-Dichloroethane ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,1-Dichloroethene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,2-Dichloroethene, Total ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,2-Dichloropropane ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,3-Dichloropropane ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼2,2-Dichloropropane ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,1-Dichloropropene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Ethylbenzene ND
0.00647 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Hexachlorobutadiene ND
0.0647 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼2-Hexanone ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Isopropylbenzene ND
0.0129 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Methylene Chloride ND
0.0647 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼4-Methyl-2-pentanone (MIBK)ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Methyl tert-butyl ether ND
0.00647 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Naphthalene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼n-Butylbenzene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼N-Propylbenzene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼p-Isopropyltoluene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼sec-Butylbenzene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Styrene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼tert-Butylbenzene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,1,1,2-Tetrachloroethane ND
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-3Client Sample ID: SB-C (6-10')
Matrix: SolidDate Collected: 02/06/13 10:15
Percent Solids: 75.9Date Received: 02/07/13 08:20
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,2,2-Tetrachloroethane ND 0.00259 mg/Kg ☼02/08/13 10:02 02/11/13 19:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Tetrachloroethene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Toluene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼trans-1,2-Dichloroethene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼trans-1,3-Dichloropropene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,2,3-Trichlorobenzene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,2,4-Trichlorobenzene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,1,1-Trichloroethane ND
0.00647 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,1,2-Trichloroethane ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Trichloroethene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Trichlorofluoromethane ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,2,3-Trichloropropane ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,2,4-Trimethylbenzene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼1,3,5-Trimethylbenzene ND
0.00259 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Vinyl chloride ND
0.00647 mg/Kg 02/08/13 10:02 02/11/13 19:50 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)97 70-130 02/08/13 10:02 02/11/13 19:50 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)102 02/08/13 10:02 02/11/13 19:50 170-130
1,2-Dichloroethane-d4 (Surr)103 02/08/13 10:02 02/11/13 19:50 170-130
Toluene-d8 (Surr)94 02/08/13 10:02 02/11/13 19:50 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0858 mg/Kg ☼02/08/13 10:48 02/10/13 01:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0858 mg/Kg 02/08/13 10:48 02/10/13 01:36 1☼Acenaphthylene ND
0.0858 mg/Kg 02/08/13 10:48 02/10/13 01:36 1☼Anthracene ND
0.0858 mg/Kg 02/08/13 10:48 02/10/13 01:36 1☼Benzo[a]anthracene ND
0.0858 mg/Kg 02/08/13 10:48 02/10/13 01:36 1☼Benzo[a]pyrene ND
0.0858 mg/Kg 02/08/13 10:48 02/10/13 01:36 1☼Benzo[b]fluoranthene ND
0.0858 mg/Kg 02/08/13 10:48 02/10/13 01:36 1☼Benzo[g,h,i]perylene ND
0.0858 mg/Kg 02/08/13 10:48 02/10/13 01:36 1☼Benzo[k]fluoranthene ND
0.0858 mg/Kg 02/08/13 10:48 02/10/13 01:36 1☼Chrysene ND
0.0858 mg/Kg 02/08/13 10:48 02/10/13 01:36 1☼Dibenz(a,h)anthracene ND
0.0858 mg/Kg 02/08/13 10:48 02/10/13 01:36 1☼Fluoranthene ND
0.0858 mg/Kg 02/08/13 10:48 02/10/13 01:36 1☼Fluorene ND
0.0858 mg/Kg 02/08/13 10:48 02/10/13 01:36 1☼Indeno[1,2,3-cd]pyrene ND
0.0858 mg/Kg 02/08/13 10:48 02/10/13 01:36 1☼Naphthalene ND
0.0858 mg/Kg 02/08/13 10:48 02/10/13 01:36 1☼Phenanthrene ND
0.0858 mg/Kg 02/08/13 10:48 02/10/13 01:36 1☼Pyrene ND
2-Fluorobiphenyl (Surr)59 29-120 02/08/13 10:48 02/10/13 01:36 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)52 02/08/13 10:48 02/10/13 01:36 127-120
Terphenyl-d14 (Surr)78 02/08/13 10:48 02/10/13 01:36 113-120
Method: 6010C - Metals (ICP)
RL MDL
Arsenic ND 2.51 mg/Kg ☼02/09/13 10:48 02/12/13 11:20 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-3Client Sample ID: SB-C (6-10')
Matrix: SolidDate Collected: 02/06/13 10:15
Percent Solids: 75.9Date Received: 02/07/13 08:20
Method: 6010C - Metals (ICP) (Continued)
RL MDL
Cadmium ND 2.51 mg/Kg ☼02/09/13 10:48 02/12/13 11:20 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.51 mg/Kg 02/09/13 10:48 02/12/13 11:20 2☼Chromium 39.8
2.51 mg/Kg 02/09/13 10:48 02/12/13 11:20 2☼Lead 9.74
5.02 mg/Kg 02/09/13 10:48 02/12/13 11:20 2☼Nickel 8.84
5.02 mg/Kg 02/09/13 10:48 02/12/13 11:20 2☼Selenium 5.88
5.02 mg/Kg 02/09/13 10:48 02/12/13 11:20 2☼Thallium ND
Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique)
RL MDL
Mercury ND 0.127 mg/Kg ☼02/12/13 14:01 02/13/13 09:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chromium, hex ND 6.59 mg/Kg ☼02/08/13 15:46 02/13/13 15:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
RL RL
Percent Solids 76 0.10 %02/08/13 08:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-4Client Sample ID: SB-C (16-20')
Matrix: SolidDate Collected: 02/06/13 10:20
Percent Solids: 68.7Date Received: 02/07/13 08:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0688 mg/Kg ☼02/08/13 10:02 02/11/13 20:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Benzene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Bromobenzene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Bromochloromethane ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Bromodichloromethane ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Bromoform ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Bromomethane ND
0.0688 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼2-Butanone (MEK)ND *
0.00688 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Carbon disulfide ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Carbon tetrachloride ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Chlorobenzene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Chlorodibromomethane ND
0.00688 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Chloroethane ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Chloroform ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Chloromethane ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼2-Chlorotoluene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼4-Chlorotoluene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼cis-1,2-Dichloroethene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼cis-1,3-Dichloropropene ND
0.00688 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,2-Dibromo-3-Chloropropane ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,2-Dibromoethane (EDB)ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Dibromomethane ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,2-Dichlorobenzene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,3-Dichlorobenzene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,4-Dichlorobenzene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Dichlorodifluoromethane ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,1-Dichloroethane ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,2-Dichloroethane ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,1-Dichloroethene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,2-Dichloroethene, Total ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,2-Dichloropropane ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,3-Dichloropropane ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼2,2-Dichloropropane ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,1-Dichloropropene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Ethylbenzene ND
0.00688 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Hexachlorobutadiene ND
0.0688 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼2-Hexanone ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Isopropylbenzene ND
0.0138 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Methylene Chloride ND
0.0688 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼4-Methyl-2-pentanone (MIBK)ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Methyl tert-butyl ether ND
0.00688 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Naphthalene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼n-Butylbenzene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼N-Propylbenzene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼p-Isopropyltoluene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼sec-Butylbenzene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Styrene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼tert-Butylbenzene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,1,1,2-Tetrachloroethane ND
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-4Client Sample ID: SB-C (16-20')
Matrix: SolidDate Collected: 02/06/13 10:20
Percent Solids: 68.7Date Received: 02/07/13 08:20
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,2,2-Tetrachloroethane ND 0.00275 mg/Kg ☼02/08/13 10:02 02/11/13 20:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Tetrachloroethene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Toluene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼trans-1,2-Dichloroethene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼trans-1,3-Dichloropropene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,2,3-Trichlorobenzene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,2,4-Trichlorobenzene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,1,1-Trichloroethane ND
0.00688 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,1,2-Trichloroethane ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Trichloroethene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Trichlorofluoromethane ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,2,3-Trichloropropane ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,2,4-Trimethylbenzene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼1,3,5-Trimethylbenzene ND
0.00275 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Vinyl chloride ND
0.00688 mg/Kg 02/08/13 10:02 02/11/13 20:21 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)94 70-130 02/08/13 10:02 02/11/13 20:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)100 02/08/13 10:02 02/11/13 20:21 170-130
1,2-Dichloroethane-d4 (Surr)100 02/08/13 10:02 02/11/13 20:21 170-130
Toluene-d8 (Surr)94 02/08/13 10:02 02/11/13 20:21 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0970 mg/Kg ☼02/08/13 10:48 02/10/13 00:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0970 mg/Kg 02/08/13 10:48 02/10/13 00:21 1☼Acenaphthylene ND
0.0970 mg/Kg 02/08/13 10:48 02/10/13 00:21 1☼Anthracene ND
0.0970 mg/Kg 02/08/13 10:48 02/10/13 00:21 1☼Benzo[a]anthracene ND
0.0970 mg/Kg 02/08/13 10:48 02/10/13 00:21 1☼Benzo[a]pyrene ND
0.0970 mg/Kg 02/08/13 10:48 02/10/13 00:21 1☼Benzo[b]fluoranthene ND
0.0970 mg/Kg 02/08/13 10:48 02/10/13 00:21 1☼Benzo[g,h,i]perylene ND
0.0970 mg/Kg 02/08/13 10:48 02/10/13 00:21 1☼Benzo[k]fluoranthene ND
0.0970 mg/Kg 02/08/13 10:48 02/10/13 00:21 1☼Chrysene ND
0.0970 mg/Kg 02/08/13 10:48 02/10/13 00:21 1☼Dibenz(a,h)anthracene ND
0.0970 mg/Kg 02/08/13 10:48 02/10/13 00:21 1☼Fluoranthene ND
0.0970 mg/Kg 02/08/13 10:48 02/10/13 00:21 1☼Fluorene ND
0.0970 mg/Kg 02/08/13 10:48 02/10/13 00:21 1☼Indeno[1,2,3-cd]pyrene ND
0.0970 mg/Kg 02/08/13 10:48 02/10/13 00:21 1☼Naphthalene ND
0.0970 mg/Kg 02/08/13 10:48 02/10/13 00:21 1☼Phenanthrene ND
0.0970 mg/Kg 02/08/13 10:48 02/10/13 00:21 1☼Pyrene ND
2-Fluorobiphenyl (Surr)69 29-120 02/08/13 10:48 02/10/13 00:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)58 02/08/13 10:48 02/10/13 00:21 127-120
Terphenyl-d14 (Surr)83 02/08/13 10:48 02/10/13 00:21 113-120
Method: 6010C - Metals (ICP)
RL MDL
Arsenic ND 2.90 mg/Kg ☼02/09/13 10:48 02/12/13 11:24 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-4Client Sample ID: SB-C (16-20')
Matrix: SolidDate Collected: 02/06/13 10:20
Percent Solids: 68.7Date Received: 02/07/13 08:20
Method: 6010C - Metals (ICP) (Continued)
RL MDL
Cadmium ND 2.90 mg/Kg ☼02/09/13 10:48 02/12/13 11:24 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.90 mg/Kg 02/09/13 10:48 02/12/13 11:24 2☼Chromium 38.9
2.90 mg/Kg 02/09/13 10:48 02/12/13 11:24 2☼Lead 24.3
5.80 mg/Kg 02/09/13 10:48 02/12/13 11:24 2☼Nickel 9.97
5.80 mg/Kg 02/09/13 10:48 02/12/13 11:24 2☼Selenium 6.49
5.80 mg/Kg 02/09/13 10:48 02/12/13 11:24 2☼Thallium ND
Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique)
RL MDL
Mercury ND 0.141 mg/Kg ☼02/12/13 14:01 02/13/13 09:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chromium, hex ND 7.27 mg/Kg ☼02/08/13 15:46 02/13/13 15:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
RL RL
Percent Solids 69 0.10 %02/08/13 08:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-5Client Sample ID: SB-D (4-8')
Matrix: SolidDate Collected: 02/06/13 11:25
Percent Solids: 77.2Date Received: 02/07/13 08:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0600 mg/Kg ☼02/08/13 10:02 02/11/13 20:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Benzene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Bromobenzene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Bromochloromethane ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Bromodichloromethane ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Bromoform ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Bromomethane ND
0.0600 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼2-Butanone (MEK)ND *
0.00600 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Carbon disulfide ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Carbon tetrachloride ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Chlorobenzene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Chlorodibromomethane ND
0.00600 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Chloroethane ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Chloroform ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Chloromethane ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼2-Chlorotoluene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼4-Chlorotoluene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼cis-1,2-Dichloroethene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼cis-1,3-Dichloropropene ND
0.00600 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,2-Dibromo-3-Chloropropane ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,2-Dibromoethane (EDB)ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Dibromomethane ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,2-Dichlorobenzene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,3-Dichlorobenzene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,4-Dichlorobenzene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Dichlorodifluoromethane ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,1-Dichloroethane ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,2-Dichloroethane ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,1-Dichloroethene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,2-Dichloroethene, Total ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,2-Dichloropropane ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,3-Dichloropropane ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼2,2-Dichloropropane ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,1-Dichloropropene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Ethylbenzene ND
0.00600 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Hexachlorobutadiene ND
0.0600 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼2-Hexanone ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Isopropylbenzene ND
0.0120 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Methylene Chloride ND
0.0600 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼4-Methyl-2-pentanone (MIBK)ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Methyl tert-butyl ether ND
0.00600 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Naphthalene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼n-Butylbenzene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼N-Propylbenzene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼p-Isopropyltoluene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼sec-Butylbenzene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Styrene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼tert-Butylbenzene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,1,1,2-Tetrachloroethane ND
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-5Client Sample ID: SB-D (4-8')
Matrix: SolidDate Collected: 02/06/13 11:25
Percent Solids: 77.2Date Received: 02/07/13 08:20
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,2,2-Tetrachloroethane ND 0.00240 mg/Kg ☼02/08/13 10:02 02/11/13 20:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Tetrachloroethene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Toluene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼trans-1,2-Dichloroethene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼trans-1,3-Dichloropropene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,2,3-Trichlorobenzene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,2,4-Trichlorobenzene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,1,1-Trichloroethane ND
0.00600 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,1,2-Trichloroethane ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Trichloroethene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Trichlorofluoromethane ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,2,3-Trichloropropane ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,2,4-Trimethylbenzene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼1,3,5-Trimethylbenzene ND
0.00240 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Vinyl chloride ND
0.00600 mg/Kg 02/08/13 10:02 02/11/13 20:52 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)95 70-130 02/08/13 10:02 02/11/13 20:52 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)100 02/08/13 10:02 02/11/13 20:52 170-130
1,2-Dichloroethane-d4 (Surr)98 02/08/13 10:02 02/11/13 20:52 170-130
Toluene-d8 (Surr)95 02/08/13 10:02 02/11/13 20:52 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0843 mg/Kg ☼02/08/13 10:48 02/10/13 02:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0843 mg/Kg 02/08/13 10:48 02/10/13 02:01 1☼Acenaphthylene ND
0.0843 mg/Kg 02/08/13 10:48 02/10/13 02:01 1☼Anthracene ND
0.0843 mg/Kg 02/08/13 10:48 02/10/13 02:01 1☼Benzo[a]anthracene ND
0.0843 mg/Kg 02/08/13 10:48 02/10/13 02:01 1☼Benzo[a]pyrene ND
0.0843 mg/Kg 02/08/13 10:48 02/10/13 02:01 1☼Benzo[b]fluoranthene ND
0.0843 mg/Kg 02/08/13 10:48 02/10/13 02:01 1☼Benzo[g,h,i]perylene ND
0.0843 mg/Kg 02/08/13 10:48 02/10/13 02:01 1☼Benzo[k]fluoranthene ND
0.0843 mg/Kg 02/08/13 10:48 02/10/13 02:01 1☼Chrysene ND
0.0843 mg/Kg 02/08/13 10:48 02/10/13 02:01 1☼Dibenz(a,h)anthracene ND
0.0843 mg/Kg 02/08/13 10:48 02/10/13 02:01 1☼Fluoranthene ND
0.0843 mg/Kg 02/08/13 10:48 02/10/13 02:01 1☼Fluorene ND
0.0843 mg/Kg 02/08/13 10:48 02/10/13 02:01 1☼Indeno[1,2,3-cd]pyrene ND
0.0843 mg/Kg 02/08/13 10:48 02/10/13 02:01 1☼Naphthalene ND
0.0843 mg/Kg 02/08/13 10:48 02/10/13 02:01 1☼Phenanthrene ND
0.0843 mg/Kg 02/08/13 10:48 02/10/13 02:01 1☼Pyrene ND
2-Fluorobiphenyl (Surr)63 29-120 02/08/13 10:48 02/10/13 02:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)53 02/08/13 10:48 02/10/13 02:01 127-120
Terphenyl-d14 (Surr)76 02/08/13 10:48 02/10/13 02:01 113-120
Method: 6010C - Metals (ICP)
RL MDL
Arsenic ND 2.47 mg/Kg ☼02/09/13 10:48 02/12/13 11:39 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-5Client Sample ID: SB-D (4-8')
Matrix: SolidDate Collected: 02/06/13 11:25
Percent Solids: 77.2Date Received: 02/07/13 08:20
Method: 6010C - Metals (ICP) (Continued)
RL MDL
Cadmium ND 2.47 mg/Kg ☼02/09/13 10:48 02/12/13 11:39 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.47 mg/Kg 02/09/13 10:48 02/12/13 11:39 2☼Chromium 25.8
2.47 mg/Kg 02/09/13 10:48 02/12/13 11:39 2☼Lead 9.84
4.94 mg/Kg 02/09/13 10:48 02/12/13 11:39 2☼Nickel 7.42
4.94 mg/Kg 02/09/13 10:48 02/12/13 11:39 2☼Selenium 5.29
4.94 mg/Kg 02/09/13 10:48 02/12/13 11:39 2☼Thallium ND
Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique)
RL MDL
Mercury ND 0.126 mg/Kg ☼02/12/13 14:01 02/13/13 09:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chromium, hex ND 6.48 mg/Kg ☼02/08/13 15:46 02/13/13 15:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
RL RL
Percent Solids 77 0.10 %02/08/13 08:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-6Client Sample ID: SB-D (12-16')
Matrix: SolidDate Collected: 02/06/13 11:30
Percent Solids: 69.5Date Received: 02/07/13 08:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0660 mg/Kg ☼02/08/13 10:02 02/11/13 21:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Benzene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Bromobenzene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Bromochloromethane ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Bromodichloromethane ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Bromoform ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Bromomethane ND
0.0660 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼2-Butanone (MEK)ND *
0.00660 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Carbon disulfide ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Carbon tetrachloride ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Chlorobenzene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Chlorodibromomethane ND
0.00660 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Chloroethane ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Chloroform ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Chloromethane ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼2-Chlorotoluene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼4-Chlorotoluene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼cis-1,2-Dichloroethene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼cis-1,3-Dichloropropene ND
0.00660 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,2-Dibromo-3-Chloropropane ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,2-Dibromoethane (EDB)ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Dibromomethane ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,2-Dichlorobenzene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,3-Dichlorobenzene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,4-Dichlorobenzene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Dichlorodifluoromethane ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,1-Dichloroethane ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,2-Dichloroethane ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,1-Dichloroethene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,2-Dichloroethene, Total ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,2-Dichloropropane ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,3-Dichloropropane ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼2,2-Dichloropropane ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,1-Dichloropropene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Ethylbenzene ND
0.00660 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Hexachlorobutadiene ND
0.0660 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼2-Hexanone ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Isopropylbenzene ND
0.0132 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Methylene Chloride ND
0.0660 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼4-Methyl-2-pentanone (MIBK)ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Methyl tert-butyl ether ND
0.00660 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Naphthalene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼n-Butylbenzene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼N-Propylbenzene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼p-Isopropyltoluene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼sec-Butylbenzene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Styrene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼tert-Butylbenzene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,1,1,2-Tetrachloroethane ND
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-6Client Sample ID: SB-D (12-16')
Matrix: SolidDate Collected: 02/06/13 11:30
Percent Solids: 69.5Date Received: 02/07/13 08:20
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,2,2-Tetrachloroethane ND 0.00264 mg/Kg ☼02/08/13 10:02 02/11/13 21:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Tetrachloroethene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Toluene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼trans-1,2-Dichloroethene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼trans-1,3-Dichloropropene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,2,3-Trichlorobenzene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,2,4-Trichlorobenzene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,1,1-Trichloroethane ND
0.00660 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,1,2-Trichloroethane ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Trichloroethene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Trichlorofluoromethane ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,2,3-Trichloropropane ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,2,4-Trimethylbenzene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼1,3,5-Trimethylbenzene ND
0.00264 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Vinyl chloride ND
0.00660 mg/Kg 02/08/13 10:02 02/11/13 21:23 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)94 70-130 02/08/13 10:02 02/11/13 21:23 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)100 02/08/13 10:02 02/11/13 21:23 170-130
1,2-Dichloroethane-d4 (Surr)100 02/08/13 10:02 02/11/13 21:23 170-130
Toluene-d8 (Surr)95 02/08/13 10:02 02/11/13 21:23 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0942 mg/Kg ☼02/08/13 10:48 02/11/13 16:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0942 mg/Kg 02/08/13 10:48 02/11/13 16:45 1☼Acenaphthylene ND
0.0942 mg/Kg 02/08/13 10:48 02/11/13 16:45 1☼Anthracene ND
0.0942 mg/Kg 02/08/13 10:48 02/11/13 16:45 1☼Benzo[a]anthracene ND
0.0942 mg/Kg 02/08/13 10:48 02/11/13 16:45 1☼Benzo[a]pyrene ND
0.0942 mg/Kg 02/08/13 10:48 02/11/13 16:45 1☼Benzo[b]fluoranthene ND
0.0942 mg/Kg 02/08/13 10:48 02/11/13 16:45 1☼Benzo[g,h,i]perylene ND
0.0942 mg/Kg 02/08/13 10:48 02/11/13 16:45 1☼Benzo[k]fluoranthene ND
0.0942 mg/Kg 02/08/13 10:48 02/11/13 16:45 1☼Chrysene ND
0.0942 mg/Kg 02/08/13 10:48 02/11/13 16:45 1☼Dibenz(a,h)anthracene ND
0.0942 mg/Kg 02/08/13 10:48 02/11/13 16:45 1☼Fluoranthene ND
0.0942 mg/Kg 02/08/13 10:48 02/11/13 16:45 1☼Fluorene ND
0.0942 mg/Kg 02/08/13 10:48 02/11/13 16:45 1☼Indeno[1,2,3-cd]pyrene ND
0.0942 mg/Kg 02/08/13 10:48 02/11/13 16:45 1☼Naphthalene ND
0.0942 mg/Kg 02/08/13 10:48 02/11/13 16:45 1☼Phenanthrene ND
0.0942 mg/Kg 02/08/13 10:48 02/11/13 16:45 1☼Pyrene ND
2-Fluorobiphenyl (Surr)65 29-120 02/08/13 10:48 02/11/13 16:45 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)55 02/08/13 10:48 02/11/13 16:45 127-120
Terphenyl-d14 (Surr)75 02/08/13 10:48 02/11/13 16:45 113-120
Method: 6010C - Metals (ICP)
RL MDL
Arsenic ND 2.87 mg/Kg ☼02/09/13 10:48 02/12/13 11:43 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-6Client Sample ID: SB-D (12-16')
Matrix: SolidDate Collected: 02/06/13 11:30
Percent Solids: 69.5Date Received: 02/07/13 08:20
Method: 6010C - Metals (ICP) (Continued)
RL MDL
Cadmium ND 2.87 mg/Kg ☼02/09/13 10:48 02/12/13 11:43 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.87 mg/Kg 02/09/13 10:48 02/12/13 11:43 2☼Chromium 28.7
2.87 mg/Kg 02/09/13 10:48 02/12/13 11:43 2☼Lead 5.62
5.73 mg/Kg 02/09/13 10:48 02/12/13 11:43 2☼Nickel 10.1
5.73 mg/Kg 02/09/13 10:48 02/12/13 11:43 2☼Selenium ND
5.73 mg/Kg 02/09/13 10:48 02/12/13 11:43 2☼Thallium ND
Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique)
RL MDL
Mercury ND 0.143 mg/Kg ☼02/12/13 14:01 02/13/13 09:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chromium, hex ND 7.20 mg/Kg ☼02/08/13 15:46 02/13/13 15:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
RL RL
Percent Solids 69 0.10 %02/08/13 08:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-7Client Sample ID: SB-E (6-10')
Matrix: SolidDate Collected: 02/06/13 10:50
Percent Solids: 72.1Date Received: 02/07/13 08:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0698 mg/Kg ☼02/08/13 10:02 02/11/13 21:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Benzene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Bromobenzene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Bromochloromethane ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Bromodichloromethane ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Bromoform ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Bromomethane ND
0.0698 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼2-Butanone (MEK)ND *
0.00698 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Carbon disulfide ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Carbon tetrachloride ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Chlorobenzene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Chlorodibromomethane ND
0.00698 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Chloroethane ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Chloroform ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Chloromethane ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼2-Chlorotoluene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼4-Chlorotoluene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼cis-1,2-Dichloroethene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼cis-1,3-Dichloropropene ND
0.00698 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,2-Dibromo-3-Chloropropane ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,2-Dibromoethane (EDB)ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Dibromomethane ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,2-Dichlorobenzene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,3-Dichlorobenzene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,4-Dichlorobenzene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Dichlorodifluoromethane ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,1-Dichloroethane ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,2-Dichloroethane ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,1-Dichloroethene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,2-Dichloroethene, Total ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,2-Dichloropropane ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,3-Dichloropropane ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼2,2-Dichloropropane ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,1-Dichloropropene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Ethylbenzene ND
0.00698 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Hexachlorobutadiene ND
0.0698 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼2-Hexanone ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Isopropylbenzene ND
0.0140 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Methylene Chloride ND
0.0698 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼4-Methyl-2-pentanone (MIBK)ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Methyl tert-butyl ether ND
0.00698 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Naphthalene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼n-Butylbenzene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼N-Propylbenzene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼p-Isopropyltoluene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼sec-Butylbenzene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Styrene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼tert-Butylbenzene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,1,1,2-Tetrachloroethane ND
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-7Client Sample ID: SB-E (6-10')
Matrix: SolidDate Collected: 02/06/13 10:50
Percent Solids: 72.1Date Received: 02/07/13 08:20
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,2,2-Tetrachloroethane ND 0.00279 mg/Kg ☼02/08/13 10:02 02/11/13 21:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Tetrachloroethene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Toluene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼trans-1,2-Dichloroethene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼trans-1,3-Dichloropropene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,2,3-Trichlorobenzene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,2,4-Trichlorobenzene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,1,1-Trichloroethane ND
0.00698 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,1,2-Trichloroethane ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Trichloroethene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Trichlorofluoromethane ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,2,3-Trichloropropane ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,2,4-Trimethylbenzene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼1,3,5-Trimethylbenzene ND
0.00279 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Vinyl chloride ND
0.00698 mg/Kg 02/08/13 10:02 02/11/13 21:55 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)94 70-130 02/08/13 10:02 02/11/13 21:55 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)100 02/08/13 10:02 02/11/13 21:55 170-130
1,2-Dichloroethane-d4 (Surr)100 02/08/13 10:02 02/11/13 21:55 170-130
Toluene-d8 (Surr)96 02/08/13 10:02 02/11/13 21:55 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0905 mg/Kg ☼02/08/13 10:48 02/11/13 17:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0905 mg/Kg 02/08/13 10:48 02/11/13 17:11 1☼Acenaphthylene ND
0.0905 mg/Kg 02/08/13 10:48 02/11/13 17:11 1☼Anthracene ND
0.0905 mg/Kg 02/08/13 10:48 02/11/13 17:11 1☼Benzo[a]anthracene ND
0.0905 mg/Kg 02/08/13 10:48 02/11/13 17:11 1☼Benzo[a]pyrene ND
0.0905 mg/Kg 02/08/13 10:48 02/11/13 17:11 1☼Benzo[b]fluoranthene ND
0.0905 mg/Kg 02/08/13 10:48 02/11/13 17:11 1☼Benzo[g,h,i]perylene ND
0.0905 mg/Kg 02/08/13 10:48 02/11/13 17:11 1☼Benzo[k]fluoranthene ND
0.0905 mg/Kg 02/08/13 10:48 02/11/13 17:11 1☼Chrysene ND
0.0905 mg/Kg 02/08/13 10:48 02/11/13 17:11 1☼Dibenz(a,h)anthracene ND
0.0905 mg/Kg 02/08/13 10:48 02/11/13 17:11 1☼Fluoranthene ND
0.0905 mg/Kg 02/08/13 10:48 02/11/13 17:11 1☼Fluorene ND
0.0905 mg/Kg 02/08/13 10:48 02/11/13 17:11 1☼Indeno[1,2,3-cd]pyrene ND
0.0905 mg/Kg 02/08/13 10:48 02/11/13 17:11 1☼Naphthalene ND
0.0905 mg/Kg 02/08/13 10:48 02/11/13 17:11 1☼Phenanthrene ND
0.0905 mg/Kg 02/08/13 10:48 02/11/13 17:11 1☼Pyrene ND
2-Fluorobiphenyl (Surr)51 29-120 02/08/13 10:48 02/11/13 17:11 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)46 02/08/13 10:48 02/11/13 17:11 127-120
Terphenyl-d14 (Surr)57 02/08/13 10:48 02/11/13 17:11 113-120
Method: 6010C - Metals (ICP)
RL MDL
Arsenic ND 2.66 mg/Kg ☼02/09/13 10:48 02/12/13 11:46 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-7Client Sample ID: SB-E (6-10')
Matrix: SolidDate Collected: 02/06/13 10:50
Percent Solids: 72.1Date Received: 02/07/13 08:20
Method: 6010C - Metals (ICP) (Continued)
RL MDL
Cadmium ND 2.66 mg/Kg ☼02/09/13 10:48 02/12/13 11:46 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.66 mg/Kg 02/09/13 10:48 02/12/13 11:46 2☼Chromium 34.9
2.66 mg/Kg 02/09/13 10:48 02/12/13 11:46 2☼Lead 13.9
5.31 mg/Kg 02/09/13 10:48 02/12/13 11:46 2☼Nickel 8.77
5.31 mg/Kg 02/09/13 10:48 02/12/13 11:46 2☼Selenium ND
5.31 mg/Kg 02/09/13 10:48 02/12/13 11:46 2☼Thallium ND
Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique)
RL MDL
Mercury ND 0.138 mg/Kg ☼02/12/13 14:01 02/13/13 09:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chromium, hex ND 6.94 mg/Kg ☼02/08/13 15:46 02/13/13 15:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
RL RL
Percent Solids 72 0.10 %02/08/13 08:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-8Client Sample ID: SB-E (16-20')
Matrix: SolidDate Collected: 02/06/13 11:00
Percent Solids: 73.4Date Received: 02/07/13 08:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0585 mg/Kg ☼02/08/13 10:02 02/12/13 10:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Benzene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Bromobenzene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Bromochloromethane ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Bromodichloromethane ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Bromoform ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Bromomethane ND
0.0585 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼2-Butanone (MEK)ND
0.00585 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Carbon disulfide ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Carbon tetrachloride ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Chlorobenzene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Chlorodibromomethane ND
0.00585 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Chloroethane ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Chloroform ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Chloromethane ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼2-Chlorotoluene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼4-Chlorotoluene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼cis-1,2-Dichloroethene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼cis-1,3-Dichloropropene ND
0.00585 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,2-Dibromo-3-Chloropropane ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,2-Dibromoethane (EDB)ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Dibromomethane ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,2-Dichlorobenzene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,3-Dichlorobenzene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,4-Dichlorobenzene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Dichlorodifluoromethane ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,1-Dichloroethane ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,2-Dichloroethane ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,1-Dichloroethene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,2-Dichloroethene, Total ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,2-Dichloropropane ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,3-Dichloropropane ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼2,2-Dichloropropane ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,1-Dichloropropene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Ethylbenzene ND
0.00585 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Hexachlorobutadiene ND
0.0585 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼2-Hexanone ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Isopropylbenzene ND
0.0117 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Methylene Chloride ND
0.0585 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼4-Methyl-2-pentanone (MIBK)ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Methyl tert-butyl ether ND
0.00585 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Naphthalene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼n-Butylbenzene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼N-Propylbenzene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼p-Isopropyltoluene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼sec-Butylbenzene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Styrene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼tert-Butylbenzene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,1,1,2-Tetrachloroethane ND
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-8Client Sample ID: SB-E (16-20')
Matrix: SolidDate Collected: 02/06/13 11:00
Percent Solids: 73.4Date Received: 02/07/13 08:20
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,2,2-Tetrachloroethane ND 0.00234 mg/Kg ☼02/08/13 10:02 02/12/13 10:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Tetrachloroethene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Toluene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼trans-1,2-Dichloroethene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼trans-1,3-Dichloropropene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,2,3-Trichlorobenzene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,2,4-Trichlorobenzene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,1,1-Trichloroethane ND
0.00585 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,1,2-Trichloroethane ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Trichloroethene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Trichlorofluoromethane ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,2,3-Trichloropropane ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,2,4-Trimethylbenzene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼1,3,5-Trimethylbenzene ND
0.00234 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Vinyl chloride ND
0.00585 mg/Kg 02/08/13 10:02 02/12/13 10:18 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)95 70-130 02/08/13 10:02 02/12/13 10:18 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)102 02/08/13 10:02 02/12/13 10:18 170-130
1,2-Dichloroethane-d4 (Surr)101 02/08/13 10:02 02/12/13 10:18 170-130
Toluene-d8 (Surr)98 02/08/13 10:02 02/12/13 10:18 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0890 mg/Kg ☼02/08/13 10:48 02/11/13 17:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0890 mg/Kg 02/08/13 10:48 02/11/13 17:38 1☼Acenaphthylene ND
0.0890 mg/Kg 02/08/13 10:48 02/11/13 17:38 1☼Anthracene ND
0.0890 mg/Kg 02/08/13 10:48 02/11/13 17:38 1☼Benzo[a]anthracene ND
0.0890 mg/Kg 02/08/13 10:48 02/11/13 17:38 1☼Benzo[a]pyrene ND
0.0890 mg/Kg 02/08/13 10:48 02/11/13 17:38 1☼Benzo[b]fluoranthene ND
0.0890 mg/Kg 02/08/13 10:48 02/11/13 17:38 1☼Benzo[g,h,i]perylene ND
0.0890 mg/Kg 02/08/13 10:48 02/11/13 17:38 1☼Benzo[k]fluoranthene ND
0.0890 mg/Kg 02/08/13 10:48 02/11/13 17:38 1☼Chrysene ND
0.0890 mg/Kg 02/08/13 10:48 02/11/13 17:38 1☼Dibenz(a,h)anthracene ND
0.0890 mg/Kg 02/08/13 10:48 02/11/13 17:38 1☼Fluoranthene ND
0.0890 mg/Kg 02/08/13 10:48 02/11/13 17:38 1☼Fluorene ND
0.0890 mg/Kg 02/08/13 10:48 02/11/13 17:38 1☼Indeno[1,2,3-cd]pyrene ND
0.0890 mg/Kg 02/08/13 10:48 02/11/13 17:38 1☼Naphthalene ND
0.0890 mg/Kg 02/08/13 10:48 02/11/13 17:38 1☼Phenanthrene ND
0.0890 mg/Kg 02/08/13 10:48 02/11/13 17:38 1☼Pyrene ND
2-Fluorobiphenyl (Surr)67 29-120 02/08/13 10:48 02/11/13 17:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)54 02/08/13 10:48 02/11/13 17:38 127-120
Terphenyl-d14 (Surr)83 02/08/13 10:48 02/11/13 17:38 113-120
Method: 6010C - Metals (ICP)
RL MDL
Arsenic ND 1.35 mg/Kg ☼02/09/13 10:48 02/12/13 10:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Lab Sample ID: 490-18944-8Client Sample ID: SB-E (16-20')
Matrix: SolidDate Collected: 02/06/13 11:00
Percent Solids: 73.4Date Received: 02/07/13 08:20
Method: 6010C - Metals (ICP) (Continued)
RL MDL
Cadmium ND 1.35 mg/Kg ☼02/09/13 10:48 02/12/13 10:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.35 mg/Kg 02/09/13 10:48 02/12/13 10:31 1☼Chromium 13.7
1.35 mg/Kg 02/09/13 10:48 02/12/13 10:31 1☼Lead 3.68
2.70 mg/Kg 02/09/13 10:48 02/12/13 10:31 1☼Nickel 7.06
2.70 mg/Kg 02/09/13 10:48 02/12/13 10:31 1☼Selenium 3.43
2.70 mg/Kg 02/09/13 10:48 02/12/13 10:31 1☼Thallium ND
Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique)
RL MDL
Mercury ND 0.136 mg/Kg ☼02/12/13 14:01 02/13/13 09:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chromium, hex ND 6.81 mg/Kg ☼02/08/13 15:48 02/13/13 15:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
RL RL
Percent Solids 73 0.10 %02/08/13 08:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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QC Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Matrix SpikeLab Sample ID: 490-19164-B-3-D MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57636 Prep Batch: 57544
Acetone ND 0.204 0.2414 mg/Kg 96 19 -175
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Benzene ND 0.0407 0.03910 mg/Kg 96 31 -143
Bromobenzene ND 0.0407 0.03355 mg/Kg 82 12 -157
Bromochloromethane ND 0.0407 0.04303 mg/Kg 106 31 -141
Bromodichloromethane ND 0.0407 0.03861 mg/Kg 95 19 -148
Bromoform ND 0.0407 0.03205 mg/Kg 79 10 -165
Bromomethane ND 0.0407 0.04135 mg/Kg 102 10 -164
2-Butanone (MEK)ND *0.204 0.2135 mg/Kg 101 18 -153
Carbon disulfide ND 0.0407 0.03216 mg/Kg 79 32 -144
Carbon tetrachloride ND 0.0407 0.04023 mg/Kg 99 31 -149
Chlorobenzene ND 0.0407 0.03698 mg/Kg 91 25 -152
Chlorodibromomethane ND 0.0407 0.03575 mg/Kg 88 14 -146
Chloroethane ND 0.0407 0.03206 mg/Kg 79 10 -151
Chloroform ND 0.0407 0.03980 mg/Kg 98 34 -160
Chloromethane ND 0.0407 0.01851 mg/Kg 45 10 -156
2-Chlorotoluene ND 0.0407 0.03480 mg/Kg 85 20 -156
4-Chlorotoluene ND 0.0407 0.03434 mg/Kg 84 17 -159
cis-1,2-Dichloroethene ND 0.0407 0.03705 mg/Kg 91 36 -139
cis-1,3-Dichloropropene ND 0.0407 0.03570 mg/Kg 88 15 -166
1,2-Dibromo-3-Chloropropane ND 0.0407 0.02987 mg/Kg 73 10 -147
1,2-Dibromoethane (EDB)ND 0.0407 0.03969 mg/Kg 97 18 -156
Dibromomethane ND 0.0407 0.03998 mg/Kg 98 20 -146
1,2-Dichlorobenzene ND 0.0407 0.03365 mg/Kg 83 10 -160
1,3-Dichlorobenzene ND 0.0407 0.03489 mg/Kg 86 10 -162
1,4-Dichlorobenzene ND 0.0407 0.03454 mg/Kg 85 11 -159
Dichlorodifluoromethane ND 0.0407 0.01392 mg/Kg 34 10 -143
1,1-Dichloroethane ND 0.0407 0.03910 mg/Kg 96 42 -136
1,2-Dichloroethane ND 0.0407 0.03968 mg/Kg 97 28 -138
1,1-Dichloroethene ND 0.0407 0.04364 mg/Kg 107 41 -143
1,2-Dichloroethene, Total ND 0.0814 0.07672 mg/Kg 94 36 -140
1,2-Dichloropropane ND 0.0407 0.03549 mg/Kg 87 20 -146
1,3-Dichloropropane ND 0.0407 0.03622 mg/Kg 89 22 -148
2,2-Dichloropropane ND 0.0407 0.03784 mg/Kg 93 33 -148
1,1-Dichloropropene ND 0.0407 0.03964 mg/Kg 97 38 -145
Ethylbenzene ND 0.0407 0.03783 mg/Kg 93 23 -161
Hexachlorobutadiene ND 0.0407 0.02612 mg/Kg 64 10 -171
2-Hexanone ND 0.204 0.1708 mg/Kg 84 10 -169
Isopropylbenzene ND 0.0407 0.03765 mg/Kg 92 23 -181
Methylene Chloride ND 0.0407 0.04167 mg/Kg 102 24 -182
4-Methyl-2-pentanone (MIBK)ND 0.204 0.2031 mg/Kg 100 10 -168
Methyl tert-butyl ether ND 0.0407 0.03845 mg/Kg 94 28 -141
Naphthalene ND 0.0407 0.02456 mg/Kg 55 10 -176
n-Butylbenzene ND 0.0407 0.03248 mg/Kg 80 10 -175
N-Propylbenzene ND 0.0407 0.03642 mg/Kg 89 19 -162
p-Isopropyltoluene ND 0.0407 0.03371 mg/Kg 83 12 -168
sec-Butylbenzene ND 0.0407 0.03464 mg/Kg 85 12 -170
Styrene ND 0.0407 0.02826 mg/Kg 69 10 -165
tert-Butylbenzene ND 0.0407 0.03543 mg/Kg 87 20 -164
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QC Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-19164-B-3-D MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57636 Prep Batch: 57544
1,1,1,2-Tetrachloroethane ND 0.0407 0.03708 mg/Kg 91 19 -158
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,1,2,2-Tetrachloroethane ND 0.0407 0.03450 mg/Kg 85 10 -162
Tetrachloroethene ND 0.0407 0.04469 mg/Kg 110 33 -161
Toluene ND 0.0407 0.03877 mg/Kg 95 30 -155
trans-1,2-Dichloroethene ND 0.0407 0.03967 mg/Kg 97 39 -140
trans-1,3-Dichloropropene ND 0.0407 0.03138 mg/Kg 77 10 -157
1,2,3-Trichlorobenzene ND 0.0407 0.02456 mg/Kg 60 10 -157
1,2,4-Trichlorobenzene ND 0.0407 0.02761 mg/Kg 68 10 -167
1,1,1-Trichloroethane ND 0.0407 0.04173 mg/Kg 102 35 -149
1,1,2-Trichloroethane ND 0.0407 0.03877 mg/Kg 95 19 -157
Trichloroethene ND 0.0407 0.04349 mg/Kg 107 27 -153
Trichlorofluoromethane ND 0.0407 0.03377 mg/Kg 83 25 -140
1,2,3-Trichloropropane ND 0.0407 0.03328 mg/Kg 82 10 -157
1,2,4-Trimethylbenzene ND 0.0407 0.03546 mg/Kg 87 14 -165
1,3,5-Trimethylbenzene ND 0.0407 0.03618 mg/Kg 89 18 -164
Vinyl chloride ND 0.0407 0.02531 mg/Kg 62 20 -141
Xylenes, Total ND 0.122 0.1122 mg/Kg 92 25 -162
4-Bromofluorobenzene (Surr)70 -130
Surrogate
97
MS MS
Qualifier Limits%Recovery
103Dibromofluoromethane (Surr)70 -130
1011,2-Dichloroethane-d4 (Surr)70 -130
95Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-19164-B-3-E MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57636 Prep Batch: 57544
Acetone ND 0.198 0.2536 mg/Kg 104 19 -175 5 50
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Benzene ND 0.0396 0.03871 mg/Kg 98 31 -143 1 50
Bromobenzene ND 0.0396 0.03522 mg/Kg 89 12 -157 5 50
Bromochloromethane ND 0.0396 0.04264 mg/Kg 108 31 -141 1 50
Bromodichloromethane ND 0.0396 0.03859 mg/Kg 97 19 -148 0 50
Bromoform ND 0.0396 0.03244 mg/Kg 82 10 -165 1 50
Bromomethane ND 0.0396 0.04056 mg/Kg 102 10 -164 2 50
2-Butanone (MEK)ND *0.198 0.2214 mg/Kg 107 18 -153 4 50
Carbon disulfide ND 0.0396 0.03175 mg/Kg 80 32 -144 1 50
Carbon tetrachloride ND 0.0396 0.03984 mg/Kg 101 31 -149 1 50
Chlorobenzene ND 0.0396 0.03600 mg/Kg 91 25 -152 3 50
Chlorodibromomethane ND 0.0396 0.03629 mg/Kg 92 14 -146 2 50
Chloroethane ND 0.0396 0.03223 mg/Kg 81 10 -151 1 50
Chloroform ND 0.0396 0.03957 mg/Kg 100 34 -160 1 49
Chloromethane ND 0.0396 0.01771 mg/Kg 45 10 -156 4 50
2-Chlorotoluene ND 0.0396 0.03488 mg/Kg 88 20 -156 0 50
4-Chlorotoluene ND 0.0396 0.03454 mg/Kg 87 17 -159 1 50
cis-1,2-Dichloroethene ND 0.0396 0.03675 mg/Kg 93 36 -139 1 50
cis-1,3-Dichloropropene ND 0.0396 0.03602 mg/Kg 91 15 -166 1 50
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QC Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-19164-B-3-E MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57636 Prep Batch: 57544
1,2-Dibromo-3-Chloropropane ND 0.0396 0.03172 mg/Kg 80 10 -147 6 50
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
1,2-Dibromoethane (EDB)ND 0.0396 0.04015 mg/Kg 101 18 -156 1 50
Dibromomethane ND 0.0396 0.04006 mg/Kg 101 20 -146 0 50
1,2-Dichlorobenzene ND 0.0396 0.03220 mg/Kg 81 10 -160 4 50
1,3-Dichlorobenzene ND 0.0396 0.03355 mg/Kg 85 10 -162 4 50
1,4-Dichlorobenzene ND 0.0396 0.03345 mg/Kg 84 11 -159 3 50
Dichlorodifluoromethane ND 0.0396 0.01376 mg/Kg 35 10 -143 1 50
1,1-Dichloroethane ND 0.0396 0.03855 mg/Kg 97 42 -136 1 50
1,2-Dichloroethane ND 0.0396 0.03919 mg/Kg 99 28 -138 1 50
1,1-Dichloroethene ND 0.0396 0.04274 mg/Kg 108 41 -143 2 50
1,2-Dichloroethene, Total ND 0.0792 0.07570 mg/Kg 96 36 -140 1 41
1,2-Dichloropropane ND 0.0396 0.03524 mg/Kg 89 20 -146 1 50
1,3-Dichloropropane ND 0.0396 0.03642 mg/Kg 92 22 -148 1 42
2,2-Dichloropropane ND 0.0396 0.03721 mg/Kg 94 33 -148 2 50
1,1-Dichloropropene ND 0.0396 0.03911 mg/Kg 99 38 -145 1 50
Ethylbenzene ND 0.0396 0.03636 mg/Kg 92 23 -161 4 50
Hexachlorobutadiene ND 0.0396 0.01968 mg/Kg 50 10 -171 28 50
2-Hexanone ND 0.198 0.1784 mg/Kg 90 10 -169 4 50
Isopropylbenzene ND 0.0396 0.03490 mg/Kg 88 23 -181 8 50
Methylene Chloride ND 0.0396 0.04085 mg/Kg 103 24 -182 2 50
4-Methyl-2-pentanone (MIBK)ND 0.198 0.2104 mg/Kg 106 10 -168 4 50
Methyl tert-butyl ether ND 0.0396 0.03810 mg/Kg 96 28 -141 1 50
Naphthalene ND 0.0396 0.02685 mg/Kg 62 10 -176 9 50
n-Butylbenzene ND 0.0396 0.02850 mg/Kg 72 10 -175 13 50
N-Propylbenzene ND 0.0396 0.03554 mg/Kg 90 19 -162 2 50
p-Isopropyltoluene ND 0.0396 0.03089 mg/Kg 78 12 -168 9 50
sec-Butylbenzene ND 0.0396 0.03196 mg/Kg 81 12 -170 8 50
Styrene ND 0.0396 0.02646 mg/Kg 67 10 -165 7 50
tert-Butylbenzene ND 0.0396 0.03421 mg/Kg 86 20 -164 3 50
1,1,1,2-Tetrachloroethane ND 0.0396 0.03689 mg/Kg 93 19 -158 1 50
1,1,2,2-Tetrachloroethane ND 0.0396 0.03742 mg/Kg 94 10 -162 8 50
Tetrachloroethene ND 0.0396 0.04333 mg/Kg 109 33 -161 3 50
Toluene ND 0.0396 0.03864 mg/Kg 98 30 -155 0 50
trans-1,2-Dichloroethene ND 0.0396 0.03895 mg/Kg 98 39 -140 2 50
trans-1,3-Dichloropropene ND 0.0396 0.03154 mg/Kg 80 10 -157 1 50
1,2,3-Trichlorobenzene ND 0.0396 0.02047 mg/Kg 52 10 -157 18 50
1,2,4-Trichlorobenzene ND 0.0396 0.02291 mg/Kg 58 10 -167 19 50
1,1,1-Trichloroethane ND 0.0396 0.04108 mg/Kg 104 35 -149 2 50
1,1,2-Trichloroethane ND 0.0396 0.03889 mg/Kg 98 19 -157 0 50
Trichloroethene ND 0.0396 0.04272 mg/Kg 108 27 -153 2 50
Trichlorofluoromethane ND 0.0396 0.03370 mg/Kg 85 25 -140 0 50
1,2,3-Trichloropropane ND 0.0396 0.03609 mg/Kg 91 10 -157 8 50
1,2,4-Trimethylbenzene ND 0.0396 0.03444 mg/Kg 87 14 -165 3 50
1,3,5-Trimethylbenzene ND 0.0396 0.03459 mg/Kg 87 18 -164 4 50
Vinyl chloride ND 0.0396 0.02432 mg/Kg 61 20 -141 4 50
Xylenes, Total ND 0.119 0.1074 mg/Kg 90 25 -162 4 50
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QC Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-19164-B-3-E MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57636 Prep Batch: 57544
4-Bromofluorobenzene (Surr)70 -130
Surrogate
103
MSD MSD
Qualifier Limits%Recovery
103Dibromofluoromethane (Surr)70 -130
1001,2-Dichloroethane-d4 (Surr)70 -130
95Toluene-d8 (Surr)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 490-57636/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57636
RL MDL
Acetone ND 0.0500 mg/Kg 02/11/13 13:05 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00200 mg/Kg 02/11/13 13:05 1Benzene
ND 0.00200 mg/Kg 02/11/13 13:05 1Bromobenzene
ND 0.00200 mg/Kg 02/11/13 13:05 1Bromochloromethane
ND 0.00200 mg/Kg 02/11/13 13:05 1Bromodichloromethane
ND 0.00200 mg/Kg 02/11/13 13:05 1Bromoform
ND 0.00200 mg/Kg 02/11/13 13:05 1Bromomethane
ND 0.0500 mg/Kg 02/11/13 13:05 12-Butanone (MEK)
ND 0.00500 mg/Kg 02/11/13 13:05 1Carbon disulfide
ND 0.00200 mg/Kg 02/11/13 13:05 1Carbon tetrachloride
ND 0.00200 mg/Kg 02/11/13 13:05 1Chlorobenzene
ND 0.00200 mg/Kg 02/11/13 13:05 1Chlorodibromomethane
ND 0.00500 mg/Kg 02/11/13 13:05 1Chloroethane
ND 0.00200 mg/Kg 02/11/13 13:05 1Chloroform
ND 0.00200 mg/Kg 02/11/13 13:05 1Chloromethane
ND 0.00200 mg/Kg 02/11/13 13:05 12-Chlorotoluene
ND 0.00200 mg/Kg 02/11/13 13:05 14-Chlorotoluene
ND 0.00200 mg/Kg 02/11/13 13:05 1cis-1,2-Dichloroethene
ND 0.00200 mg/Kg 02/11/13 13:05 1cis-1,3-Dichloropropene
ND 0.00500 mg/Kg 02/11/13 13:05 11,2-Dibromo-3-Chloropropane
ND 0.00200 mg/Kg 02/11/13 13:05 11,2-Dibromoethane (EDB)
ND 0.00200 mg/Kg 02/11/13 13:05 1Dibromomethane
ND 0.00200 mg/Kg 02/11/13 13:05 11,2-Dichlorobenzene
ND 0.00200 mg/Kg 02/11/13 13:05 11,3-Dichlorobenzene
ND 0.00200 mg/Kg 02/11/13 13:05 11,4-Dichlorobenzene
ND 0.00200 mg/Kg 02/11/13 13:05 1Dichlorodifluoromethane
ND 0.00200 mg/Kg 02/11/13 13:05 11,1-Dichloroethane
ND 0.00200 mg/Kg 02/11/13 13:05 11,2-Dichloroethane
ND 0.00200 mg/Kg 02/11/13 13:05 11,1-Dichloroethene
ND 0.00200 mg/Kg 02/11/13 13:05 11,2-Dichloroethene, Total
ND 0.00200 mg/Kg 02/11/13 13:05 11,2-Dichloropropane
ND 0.00200 mg/Kg 02/11/13 13:05 11,3-Dichloropropane
ND 0.00200 mg/Kg 02/11/13 13:05 12,2-Dichloropropane
ND 0.00200 mg/Kg 02/11/13 13:05 11,1-Dichloropropene
ND 0.00200 mg/Kg 02/11/13 13:05 1Ethylbenzene
ND 0.00500 mg/Kg 02/11/13 13:05 1Hexachlorobutadiene
ND 0.0500 mg/Kg 02/11/13 13:05 12-Hexanone
ND 0.00200 mg/Kg 02/11/13 13:05 1Isopropylbenzene
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QC Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-57636/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57636
RL MDL
Methylene Chloride ND 0.0100 mg/Kg 02/11/13 13:05 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0500 mg/Kg 02/11/13 13:05 14-Methyl-2-pentanone (MIBK)
ND 0.00200 mg/Kg 02/11/13 13:05 1Methyl tert-butyl ether
ND 0.00500 mg/Kg 02/11/13 13:05 1Naphthalene
ND 0.00200 mg/Kg 02/11/13 13:05 1n-Butylbenzene
ND 0.00200 mg/Kg 02/11/13 13:05 1N-Propylbenzene
ND 0.00200 mg/Kg 02/11/13 13:05 1p-Isopropyltoluene
ND 0.00200 mg/Kg 02/11/13 13:05 1sec-Butylbenzene
ND 0.00200 mg/Kg 02/11/13 13:05 1Styrene
ND 0.00200 mg/Kg 02/11/13 13:05 1tert-Butylbenzene
ND 0.00200 mg/Kg 02/11/13 13:05 11,1,1,2-Tetrachloroethane
ND 0.00200 mg/Kg 02/11/13 13:05 11,1,2,2-Tetrachloroethane
ND 0.00200 mg/Kg 02/11/13 13:05 1Tetrachloroethene
ND 0.00200 mg/Kg 02/11/13 13:05 1Toluene
ND 0.00200 mg/Kg 02/11/13 13:05 1trans-1,2-Dichloroethene
ND 0.00200 mg/Kg 02/11/13 13:05 1trans-1,3-Dichloropropene
ND 0.00200 mg/Kg 02/11/13 13:05 11,2,3-Trichlorobenzene
ND 0.00200 mg/Kg 02/11/13 13:05 11,2,4-Trichlorobenzene
ND 0.00200 mg/Kg 02/11/13 13:05 11,1,1-Trichloroethane
ND 0.00500 mg/Kg 02/11/13 13:05 11,1,2-Trichloroethane
ND 0.00200 mg/Kg 02/11/13 13:05 1Trichloroethene
ND 0.00200 mg/Kg 02/11/13 13:05 1Trichlorofluoromethane
ND 0.00200 mg/Kg 02/11/13 13:05 11,2,3-Trichloropropane
ND 0.00200 mg/Kg 02/11/13 13:05 11,2,4-Trimethylbenzene
ND 0.00200 mg/Kg 02/11/13 13:05 11,3,5-Trimethylbenzene
ND 0.00200 mg/Kg 02/11/13 13:05 1Vinyl chloride
ND 0.00500 mg/Kg 02/11/13 13:05 1Xylenes, Total
4-Bromofluorobenzene (Surr)97 70-130 02/11/13 13:05 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
99 02/11/13 13:05 1Dibromofluoromethane (Surr)70-130
98 02/11/13 13:05 11,2-Dichloroethane-d4 (Surr)70-130
94 02/11/13 13:05 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-57636/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57636
Acetone 0.250 0.2789 mg/Kg 112 51 -149
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 0.0500 0.05144 mg/Kg 103 75 -127
Bromobenzene 0.0500 0.04764 mg/Kg 95 75 -130
Bromochloromethane 0.0500 0.05663 mg/Kg 113 70 -132
Bromodichloromethane 0.0500 0.05155 mg/Kg 103 68 -135
Bromoform 0.0500 0.04864 mg/Kg 97 36 -150
Bromomethane 0.0500 0.05774 mg/Kg 115 43 -142
2-Butanone (MEK)0.250 0.3120 mg/Kg 125 61 -132
Carbon disulfide 0.0500 0.04285 mg/Kg 86 74 -135
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QC Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-57636/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57636
Carbon tetrachloride 0.0500 0.05335 mg/Kg 107 70 -141
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Chlorobenzene 0.0500 0.05129 mg/Kg 103 84 -125
Chlorodibromomethane 0.0500 0.05000 mg/Kg 100 66 -134
Chloroethane 0.0500 0.04815 mg/Kg 96 53 -144
Chloroform 0.0500 0.05219 mg/Kg 104 76 -130
Chloromethane 0.0500 0.03392 mg/Kg 68 23 -150
2-Chlorotoluene 0.0500 0.04751 mg/Kg 95 78 -132
4-Chlorotoluene 0.0500 0.04830 mg/Kg 97 77 -138
cis-1,2-Dichloroethene 0.0500 0.04963 mg/Kg 99 75 -125
cis-1,3-Dichloropropene 0.0500 0.04870 mg/Kg 97 73 -148
1,2-Dibromo-3-Chloropropane 0.0500 0.05531 mg/Kg 111 49 -142
1,2-Dibromoethane (EDB)0.0500 0.05520 mg/Kg 110 80 -135
Dibromomethane 0.0500 0.05379 mg/Kg 108 71 -130
1,2-Dichlorobenzene 0.0500 0.05283 mg/Kg 106 80 -134
1,3-Dichlorobenzene 0.0500 0.05289 mg/Kg 106 79 -137
1,4-Dichlorobenzene 0.0500 0.05226 mg/Kg 105 77 -139
Dichlorodifluoromethane 0.0500 0.03790 mg/Kg 76 12 -144
1,1-Dichloroethane 0.0500 0.05210 mg/Kg 104 75 -124
1,2-Dichloroethane 0.0500 0.05285 mg/Kg 106 65 -134
1,1-Dichloroethene 0.0500 0.06074 mg/Kg 121 75 -131
1,2-Dichloroethene, Total 0.100 0.1030 mg/Kg 103 75 -128
1,2-Dichloropropane 0.0500 0.04649 mg/Kg 93 69 -120
1,3-Dichloropropane 0.0500 0.04942 mg/Kg 99 78 -126
2,2-Dichloropropane 0.0500 0.05059 mg/Kg 101 68 -145
1,1-Dichloropropene 0.0500 0.05194 mg/Kg 104 79 -127
Ethylbenzene 0.0500 0.05054 mg/Kg 101 80 -134
Hexachlorobutadiene 0.0500 0.06062 mg/Kg 121 65 -148
2-Hexanone 0.250 0.2792 mg/Kg 112 57 -148
Isopropylbenzene 0.0500 0.05215 mg/Kg 104 80 -150
Methylene Chloride 0.0500 0.05368 mg/Kg 107 68 -144
4-Methyl-2-pentanone (MIBK)0.250 0.2862 mg/Kg 114 59 -138
Methyl tert-butyl ether 0.0500 0.05264 mg/Kg 105 70 -136
Naphthalene 0.0500 0.05856 mg/Kg 117 69 -150
n-Butylbenzene 0.0500 0.05136 mg/Kg 103 72 -152
N-Propylbenzene 0.0500 0.04845 mg/Kg 97 75 -137
p-Isopropyltoluene 0.0500 0.04963 mg/Kg 99 77 -141
sec-Butylbenzene 0.0500 0.05029 mg/Kg 101 79 -141
Styrene 0.0500 0.05293 mg/Kg 106 82 -137
tert-Butylbenzene 0.0500 0.05002 mg/Kg 100 80 -132
1,1,1,2-Tetrachloroethane 0.0500 0.05153 mg/Kg 103 80 -136
1,1,2,2-Tetrachloroethane 0.0500 0.05082 mg/Kg 102 66 -134
Tetrachloroethene 0.0500 0.05905 mg/Kg 118 78 -140
Toluene 0.0500 0.05134 mg/Kg 103 80 -132
trans-1,2-Dichloroethene 0.0500 0.05340 mg/Kg 107 76 -128
trans-1,3-Dichloropropene 0.0500 0.04532 mg/Kg 91 62 -139
1,2,3-Trichlorobenzene 0.0500 0.06196 mg/Kg 124 70 -150
1,2,4-Trichlorobenzene 0.0500 0.06290 mg/Kg 126 62 -150
1,1,1-Trichloroethane 0.0500 0.05533 mg/Kg 111 72 -140
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QC Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-57636/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57636
1,1,2-Trichloroethane 0.0500 0.05134 mg/Kg 103 78 -128
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Trichloroethene 0.0500 0.05720 mg/Kg 114 77 -127
Trichlorofluoromethane 0.0500 0.04811 mg/Kg 96 50 -140
1,2,3-Trichloropropane 0.0500 0.04865 mg/Kg 97 65 -139
1,2,4-Trimethylbenzene 0.0500 0.04899 mg/Kg 98 77 -139
1,3,5-Trimethylbenzene 0.0500 0.04998 mg/Kg 100 78 -138
Vinyl chloride 0.0500 0.04223 mg/Kg 84 47 -136
Xylenes, Total 0.150 0.1527 mg/Kg 102 80 -137
4-Bromofluorobenzene (Surr)70 -130
Surrogate
92
LCS LCS
Qualifier Limits%Recovery
100Dibromofluoromethane (Surr)70 -130
971,2-Dichloroethane-d4 (Surr)70 -130
97Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-57636/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57636
Acetone 0.250 0.3010 mg/Kg 120 51 -149 8 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 0.0500 0.05184 mg/Kg 104 75 -127 1 50
Bromobenzene 0.0500 0.04763 mg/Kg 95 75 -130 0 50
Bromochloromethane 0.0500 0.05796 mg/Kg 116 70 -132 2 50
Bromodichloromethane 0.0500 0.05246 mg/Kg 105 68 -135 2 50
Bromoform 0.0500 0.05124 mg/Kg 102 36 -150 5 50
Bromomethane 0.0500 0.06027 mg/Kg 121 43 -142 4 50
2-Butanone (MEK)0.250 0.3324 *mg/Kg 133 61 -132 6 50
Carbon disulfide 0.0500 0.04292 mg/Kg 86 74 -135 0 50
Carbon tetrachloride 0.0500 0.05387 mg/Kg 108 70 -141 1 50
Chlorobenzene 0.0500 0.05184 mg/Kg 104 84 -125 1 50
Chlorodibromomethane 0.0500 0.05143 mg/Kg 103 66 -134 3 50
Chloroethane 0.0500 0.04785 mg/Kg 96 53 -144 1 50
Chloroform 0.0500 0.05289 mg/Kg 106 76 -130 1 49
Chloromethane 0.0500 0.03441 mg/Kg 69 23 -150 1 50
2-Chlorotoluene 0.0500 0.04693 mg/Kg 94 78 -132 1 50
4-Chlorotoluene 0.0500 0.04747 mg/Kg 95 77 -138 2 50
cis-1,2-Dichloroethene 0.0500 0.04967 mg/Kg 99 75 -125 0 50
cis-1,3-Dichloropropene 0.0500 0.04943 mg/Kg 99 73 -148 2 50
1,2-Dibromo-3-Chloropropane 0.0500 0.05782 mg/Kg 116 49 -142 4 50
1,2-Dibromoethane (EDB)0.0500 0.05660 mg/Kg 113 80 -135 2 50
Dibromomethane 0.0500 0.05531 mg/Kg 111 71 -130 3 50
1,2-Dichlorobenzene 0.0500 0.05274 mg/Kg 105 80 -134 0 50
1,3-Dichlorobenzene 0.0500 0.05230 mg/Kg 105 79 -137 1 50
1,4-Dichlorobenzene 0.0500 0.05162 mg/Kg 103 77 -139 1 50
Dichlorodifluoromethane 0.0500 0.03732 mg/Kg 75 12 -144 2 50
1,1-Dichloroethane 0.0500 0.05239 mg/Kg 105 75 -124 1 50
1,2-Dichloroethane 0.0500 0.05418 mg/Kg 108 65 -134 2 50
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Page 35 of 59 2/14/2013
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QC Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-57636/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57636
1,1-Dichloroethene 0.0500 0.06065 mg/Kg 121 75 -131 0 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,2-Dichloroethene, Total 0.100 0.1033 mg/Kg 103 75 -128 0 41
1,2-Dichloropropane 0.0500 0.04733 mg/Kg 95 69 -120 2 50
1,3-Dichloropropane 0.0500 0.05060 mg/Kg 101 78 -126 2 42
2,2-Dichloropropane 0.0500 0.05095 mg/Kg 102 68 -145 1 50
1,1-Dichloropropene 0.0500 0.05212 mg/Kg 104 79 -127 0 50
Ethylbenzene 0.0500 0.05107 mg/Kg 102 80 -134 1 50
Hexachlorobutadiene 0.0500 0.05941 mg/Kg 119 65 -148 2 50
2-Hexanone 0.250 0.2958 mg/Kg 118 57 -148 6 50
Isopropylbenzene 0.0500 0.05238 mg/Kg 105 80 -150 0 50
Methylene Chloride 0.0500 0.05427 mg/Kg 109 68 -144 1 50
4-Methyl-2-pentanone (MIBK)0.250 0.3043 mg/Kg 122 59 -138 6 50
Methyl tert-butyl ether 0.0500 0.05375 mg/Kg 107 70 -136 2 50
Naphthalene 0.0500 0.05955 mg/Kg 119 69 -150 2 50
n-Butylbenzene 0.0500 0.05016 mg/Kg 100 72 -152 2 50
N-Propylbenzene 0.0500 0.04791 mg/Kg 96 75 -137 1 50
p-Isopropyltoluene 0.0500 0.04850 mg/Kg 97 77 -141 2 50
sec-Butylbenzene 0.0500 0.04912 mg/Kg 98 79 -141 2 50
Styrene 0.0500 0.05303 mg/Kg 106 82 -137 0 50
tert-Butylbenzene 0.0500 0.04866 mg/Kg 97 80 -132 3 50
1,1,1,2-Tetrachloroethane 0.0500 0.05265 mg/Kg 105 80 -136 2 50
1,1,2,2-Tetrachloroethane 0.0500 0.05015 mg/Kg 100 66 -134 1 50
Tetrachloroethene 0.0500 0.05967 mg/Kg 119 78 -140 1 50
Toluene 0.0500 0.05185 mg/Kg 104 80 -132 1 50
trans-1,2-Dichloroethene 0.0500 0.05366 mg/Kg 107 76 -128 0 50
trans-1,3-Dichloropropene 0.0500 0.04613 mg/Kg 92 62 -139 2 50
1,2,3-Trichlorobenzene 0.0500 0.06156 mg/Kg 123 70 -150 1 50
1,2,4-Trichlorobenzene 0.0500 0.06250 mg/Kg 125 62 -150 1 50
1,1,1-Trichloroethane 0.0500 0.05534 mg/Kg 111 72 -140 0 50
1,1,2-Trichloroethane 0.0500 0.05288 mg/Kg 106 78 -128 3 50
Trichloroethene 0.0500 0.05756 mg/Kg 115 77 -127 1 50
Trichlorofluoromethane 0.0500 0.04758 mg/Kg 95 50 -140 1 50
1,2,3-Trichloropropane 0.0500 0.04979 mg/Kg 100 65 -139 2 50
1,2,4-Trimethylbenzene 0.0500 0.04881 mg/Kg 98 77 -139 0 50
1,3,5-Trimethylbenzene 0.0500 0.04922 mg/Kg 98 78 -138 2 50
Vinyl chloride 0.0500 0.04160 mg/Kg 83 47 -136 2 50
Xylenes, Total 0.150 0.1536 mg/Kg 102 80 -137 1 50
4-Bromofluorobenzene (Surr)70 -130
Surrogate
92
LCSD LCSD
Qualifier Limits%Recovery
102Dibromofluoromethane (Surr)70 -130
991,2-Dichloroethane-d4 (Surr)70 -130
95Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-57826/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57826
RL MDL
Acetone ND 0.0500 mg/Kg 02/12/13 08:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00200 mg/Kg 02/12/13 08:59 1Benzene
ND 0.00200 mg/Kg 02/12/13 08:59 1Bromobenzene
ND 0.00200 mg/Kg 02/12/13 08:59 1Bromochloromethane
ND 0.00200 mg/Kg 02/12/13 08:59 1Bromodichloromethane
ND 0.00200 mg/Kg 02/12/13 08:59 1Bromoform
ND 0.00200 mg/Kg 02/12/13 08:59 1Bromomethane
ND 0.0500 mg/Kg 02/12/13 08:59 12-Butanone (MEK)
ND 0.00500 mg/Kg 02/12/13 08:59 1Carbon disulfide
ND 0.00200 mg/Kg 02/12/13 08:59 1Carbon tetrachloride
ND 0.00200 mg/Kg 02/12/13 08:59 1Chlorobenzene
ND 0.00200 mg/Kg 02/12/13 08:59 1Chlorodibromomethane
ND 0.00500 mg/Kg 02/12/13 08:59 1Chloroethane
ND 0.00200 mg/Kg 02/12/13 08:59 1Chloroform
ND 0.00200 mg/Kg 02/12/13 08:59 1Chloromethane
ND 0.00200 mg/Kg 02/12/13 08:59 12-Chlorotoluene
ND 0.00200 mg/Kg 02/12/13 08:59 14-Chlorotoluene
ND 0.00200 mg/Kg 02/12/13 08:59 1cis-1,2-Dichloroethene
ND 0.00200 mg/Kg 02/12/13 08:59 1cis-1,3-Dichloropropene
ND 0.00500 mg/Kg 02/12/13 08:59 11,2-Dibromo-3-Chloropropane
ND 0.00200 mg/Kg 02/12/13 08:59 11,2-Dibromoethane (EDB)
ND 0.00200 mg/Kg 02/12/13 08:59 1Dibromomethane
ND 0.00200 mg/Kg 02/12/13 08:59 11,2-Dichlorobenzene
ND 0.00200 mg/Kg 02/12/13 08:59 11,3-Dichlorobenzene
ND 0.00200 mg/Kg 02/12/13 08:59 11,4-Dichlorobenzene
ND 0.00200 mg/Kg 02/12/13 08:59 1Dichlorodifluoromethane
ND 0.00200 mg/Kg 02/12/13 08:59 11,1-Dichloroethane
ND 0.00200 mg/Kg 02/12/13 08:59 11,2-Dichloroethane
ND 0.00200 mg/Kg 02/12/13 08:59 11,1-Dichloroethene
ND 0.00200 mg/Kg 02/12/13 08:59 11,2-Dichloroethene, Total
ND 0.00200 mg/Kg 02/12/13 08:59 11,2-Dichloropropane
ND 0.00200 mg/Kg 02/12/13 08:59 11,3-Dichloropropane
ND 0.00200 mg/Kg 02/12/13 08:59 12,2-Dichloropropane
ND 0.00200 mg/Kg 02/12/13 08:59 11,1-Dichloropropene
ND 0.00200 mg/Kg 02/12/13 08:59 1Ethylbenzene
ND 0.00500 mg/Kg 02/12/13 08:59 1Hexachlorobutadiene
ND 0.0500 mg/Kg 02/12/13 08:59 12-Hexanone
ND 0.00200 mg/Kg 02/12/13 08:59 1Isopropylbenzene
ND 0.0100 mg/Kg 02/12/13 08:59 1Methylene Chloride
ND 0.0500 mg/Kg 02/12/13 08:59 14-Methyl-2-pentanone (MIBK)
ND 0.00200 mg/Kg 02/12/13 08:59 1Methyl tert-butyl ether
ND 0.00500 mg/Kg 02/12/13 08:59 1Naphthalene
ND 0.00200 mg/Kg 02/12/13 08:59 1n-Butylbenzene
ND 0.00200 mg/Kg 02/12/13 08:59 1N-Propylbenzene
ND 0.00200 mg/Kg 02/12/13 08:59 1p-Isopropyltoluene
ND 0.00200 mg/Kg 02/12/13 08:59 1sec-Butylbenzene
ND 0.00200 mg/Kg 02/12/13 08:59 1Styrene
ND 0.00200 mg/Kg 02/12/13 08:59 1tert-Butylbenzene
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QC Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-57826/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57826
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00200 mg/Kg 02/12/13 08:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00200 mg/Kg 02/12/13 08:59 11,1,2,2-Tetrachloroethane
ND 0.00200 mg/Kg 02/12/13 08:59 1Tetrachloroethene
ND 0.00200 mg/Kg 02/12/13 08:59 1Toluene
ND 0.00200 mg/Kg 02/12/13 08:59 1trans-1,2-Dichloroethene
ND 0.00200 mg/Kg 02/12/13 08:59 1trans-1,3-Dichloropropene
ND 0.00200 mg/Kg 02/12/13 08:59 11,2,3-Trichlorobenzene
ND 0.00200 mg/Kg 02/12/13 08:59 11,2,4-Trichlorobenzene
ND 0.00200 mg/Kg 02/12/13 08:59 11,1,1-Trichloroethane
ND 0.00500 mg/Kg 02/12/13 08:59 11,1,2-Trichloroethane
ND 0.00200 mg/Kg 02/12/13 08:59 1Trichloroethene
ND 0.00200 mg/Kg 02/12/13 08:59 1Trichlorofluoromethane
ND 0.00200 mg/Kg 02/12/13 08:59 11,2,3-Trichloropropane
ND 0.00200 mg/Kg 02/12/13 08:59 11,2,4-Trimethylbenzene
ND 0.00200 mg/Kg 02/12/13 08:59 11,3,5-Trimethylbenzene
ND 0.00200 mg/Kg 02/12/13 08:59 1Vinyl chloride
ND 0.00500 mg/Kg 02/12/13 08:59 1Xylenes, Total
4-Bromofluorobenzene (Surr)96 70-130 02/12/13 08:59 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
100 02/12/13 08:59 1Dibromofluoromethane (Surr)70-130
98 02/12/13 08:59 11,2-Dichloroethane-d4 (Surr)70-130
96 02/12/13 08:59 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-57826/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57826
Acetone 0.250 0.2658 mg/Kg 106 51 -149
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 0.0500 0.04682 mg/Kg 94 75 -127
Bromobenzene 0.0500 0.04295 mg/Kg 86 75 -130
Bromochloromethane 0.0500 0.04945 mg/Kg 99 70 -132
Bromodichloromethane 0.0500 0.04361 mg/Kg 87 68 -135
Bromoform 0.0500 0.03980 mg/Kg 80 36 -150
Bromomethane 0.0500 0.05463 mg/Kg 109 43 -142
2-Butanone (MEK)0.250 0.2921 mg/Kg 117 61 -132
Carbon disulfide 0.0500 0.04011 mg/Kg 80 74 -135
Carbon tetrachloride 0.0500 0.04853 mg/Kg 97 70 -141
Chlorobenzene 0.0500 0.04686 mg/Kg 94 84 -125
Chlorodibromomethane 0.0500 0.04172 mg/Kg 83 66 -134
Chloroethane 0.0500 0.04456 mg/Kg 89 53 -144
Chloroform 0.0500 0.04664 mg/Kg 93 76 -130
Chloromethane 0.0500 0.03190 mg/Kg 64 23 -150
2-Chlorotoluene 0.0500 0.04505 mg/Kg 90 78 -132
4-Chlorotoluene 0.0500 0.04564 mg/Kg 91 77 -138
cis-1,2-Dichloroethene 0.0500 0.04452 mg/Kg 89 75 -125
cis-1,3-Dichloropropene 0.0500 0.04352 mg/Kg 87 73 -148
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QC Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-57826/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57826
1,2-Dibromo-3-Chloropropane 0.0500 0.04829 mg/Kg 97 49 -142
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dibromoethane (EDB)0.0500 0.04669 mg/Kg 93 80 -135
Dibromomethane 0.0500 0.04545 mg/Kg 91 71 -130
1,2-Dichlorobenzene 0.0500 0.04831 mg/Kg 97 80 -134
1,3-Dichlorobenzene 0.0500 0.05003 mg/Kg 100 79 -137
1,4-Dichlorobenzene 0.0500 0.04974 mg/Kg 99 77 -139
Dichlorodifluoromethane 0.0500 0.03451 mg/Kg 69 12 -144
1,1-Dichloroethane 0.0500 0.04656 mg/Kg 93 75 -124
1,2-Dichloroethane 0.0500 0.04548 mg/Kg 91 65 -134
1,1-Dichloroethene 0.0500 0.05547 mg/Kg 111 75 -131
1,2-Dichloroethene, Total 0.100 0.09404 mg/Kg 94 75 -128
1,2-Dichloropropane 0.0500 0.04123 mg/Kg 82 69 -120
1,3-Dichloropropane 0.0500 0.04236 mg/Kg 85 78 -126
2,2-Dichloropropane 0.0500 0.04553 mg/Kg 91 68 -145
1,1-Dichloropropene 0.0500 0.04891 mg/Kg 98 79 -127
Ethylbenzene 0.0500 0.04698 mg/Kg 94 80 -134
Hexachlorobutadiene 0.0500 0.05664 mg/Kg 113 65 -148
2-Hexanone 0.250 0.2473 mg/Kg 99 57 -148
Isopropylbenzene 0.0500 0.04801 mg/Kg 96 80 -150
Methylene Chloride 0.0500 0.04845 mg/Kg 97 68 -144
4-Methyl-2-pentanone (MIBK)0.250 0.2547 mg/Kg 102 59 -138
Methyl tert-butyl ether 0.0500 0.04241 mg/Kg 85 70 -136
Naphthalene 0.0500 0.05074 mg/Kg 101 69 -150
n-Butylbenzene 0.0500 0.04957 mg/Kg 99 72 -152
N-Propylbenzene 0.0500 0.04676 mg/Kg 94 75 -137
p-Isopropyltoluene 0.0500 0.04763 mg/Kg 95 77 -141
sec-Butylbenzene 0.0500 0.04790 mg/Kg 96 79 -141
Styrene 0.0500 0.04710 mg/Kg 94 82 -137
tert-Butylbenzene 0.0500 0.04652 mg/Kg 93 80 -132
1,1,1,2-Tetrachloroethane 0.0500 0.04489 mg/Kg 90 80 -136
1,1,2,2-Tetrachloroethane 0.0500 0.04348 mg/Kg 87 66 -134
Tetrachloroethene 0.0500 0.05664 mg/Kg 113 78 -140
Toluene 0.0500 0.04722 mg/Kg 94 80 -132
trans-1,2-Dichloroethene 0.0500 0.04952 mg/Kg 99 76 -128
trans-1,3-Dichloropropene 0.0500 0.03809 mg/Kg 76 62 -139
1,2,3-Trichlorobenzene 0.0500 0.05672 mg/Kg 113 70 -150
1,2,4-Trichlorobenzene 0.0500 0.05952 mg/Kg 119 62 -150
1,1,1-Trichloroethane 0.0500 0.04958 mg/Kg 99 72 -140
1,1,2-Trichloroethane 0.0500 0.04423 mg/Kg 88 78 -128
Trichloroethene 0.0500 0.05292 mg/Kg 106 77 -127
Trichlorofluoromethane 0.0500 0.04561 mg/Kg 91 50 -140
1,2,3-Trichloropropane 0.0500 0.04236 mg/Kg 85 65 -139
1,2,4-Trimethylbenzene 0.0500 0.04647 mg/Kg 93 77 -139
1,3,5-Trimethylbenzene 0.0500 0.04707 mg/Kg 94 78 -138
Vinyl chloride 0.0500 0.03930 mg/Kg 79 47 -136
Xylenes, Total 0.150 0.1408 mg/Kg 94 80 -137
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QC Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-57826/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57826
4-Bromofluorobenzene (Surr)70 -130
Surrogate
94
LCS LCS
Qualifier Limits%Recovery
100Dibromofluoromethane (Surr)70 -130
971,2-Dichloroethane-d4 (Surr)70 -130
94Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-57826/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57826
Acetone 0.250 0.2869 mg/Kg 115 51 -149 8 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 0.0500 0.05256 mg/Kg 105 75 -127 12 50
Bromobenzene 0.0500 0.04813 mg/Kg 96 75 -130 11 50
Bromochloromethane 0.0500 0.05614 mg/Kg 112 70 -132 13 50
Bromodichloromethane 0.0500 0.05037 mg/Kg 101 68 -135 14 50
Bromoform 0.0500 0.04669 mg/Kg 93 36 -150 16 50
Bromomethane 0.0500 0.06220 mg/Kg 124 43 -142 13 50
2-Butanone (MEK)0.250 0.3221 mg/Kg 129 61 -132 10 50
Carbon disulfide 0.0500 0.04458 mg/Kg 89 74 -135 11 50
Carbon tetrachloride 0.0500 0.05513 mg/Kg 110 70 -141 13 50
Chlorobenzene 0.0500 0.05269 mg/Kg 105 84 -125 12 50
Chlorodibromomethane 0.0500 0.04824 mg/Kg 96 66 -134 14 50
Chloroethane 0.0500 0.04898 mg/Kg 98 53 -144 9 50
Chloroform 0.0500 0.05251 mg/Kg 105 76 -130 12 49
Chloromethane 0.0500 0.03494 mg/Kg 70 23 -150 9 50
2-Chlorotoluene 0.0500 0.04935 mg/Kg 99 78 -132 9 50
4-Chlorotoluene 0.0500 0.05055 mg/Kg 101 77 -138 10 50
cis-1,2-Dichloroethene 0.0500 0.04995 mg/Kg 100 75 -125 12 50
cis-1,3-Dichloropropene 0.0500 0.04930 mg/Kg 99 73 -148 12 50
1,2-Dibromo-3-Chloropropane 0.0500 0.05483 mg/Kg 110 49 -142 13 50
1,2-Dibromoethane (EDB)0.0500 0.05305 mg/Kg 106 80 -135 13 50
Dibromomethane 0.0500 0.05184 mg/Kg 104 71 -130 13 50
1,2-Dichlorobenzene 0.0500 0.05372 mg/Kg 107 80 -134 11 50
1,3-Dichlorobenzene 0.0500 0.05603 mg/Kg 112 79 -137 11 50
1,4-Dichlorobenzene 0.0500 0.05458 mg/Kg 109 77 -139 9 50
Dichlorodifluoromethane 0.0500 0.03764 mg/Kg 75 12 -144 9 50
1,1-Dichloroethane 0.0500 0.05242 mg/Kg 105 75 -124 12 50
1,2-Dichloroethane 0.0500 0.05107 mg/Kg 102 65 -134 12 50
1,1-Dichloroethene 0.0500 0.06246 mg/Kg 125 75 -131 12 50
1,2-Dichloroethene, Total 0.100 0.1048 mg/Kg 105 75 -128 11 41
1,2-Dichloropropane 0.0500 0.04683 mg/Kg 94 69 -120 13 50
1,3-Dichloropropane 0.0500 0.04794 mg/Kg 96 78 -126 12 42
2,2-Dichloropropane 0.0500 0.05221 mg/Kg 104 68 -145 14 50
1,1-Dichloropropene 0.0500 0.05434 mg/Kg 109 79 -127 11 50
Ethylbenzene 0.0500 0.05294 mg/Kg 106 80 -134 12 50
Hexachlorobutadiene 0.0500 0.06350 mg/Kg 127 65 -148 11 50
2-Hexanone 0.250 0.2746 mg/Kg 110 57 -148 10 50
Isopropylbenzene 0.0500 0.05431 mg/Kg 109 80 -150 12 50
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QC Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-57826/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57826
Methylene Chloride 0.0500 0.05446 mg/Kg 109 68 -144 12 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
4-Methyl-2-pentanone (MIBK)0.250 0.2836 mg/Kg 113 59 -138 11 50
Methyl tert-butyl ether 0.0500 0.04867 mg/Kg 97 70 -136 14 50
Naphthalene 0.0500 0.05694 mg/Kg 114 69 -150 12 50
n-Butylbenzene 0.0500 0.05533 mg/Kg 111 72 -152 11 50
N-Propylbenzene 0.0500 0.05187 mg/Kg 104 75 -137 10 50
p-Isopropyltoluene 0.0500 0.05324 mg/Kg 106 77 -141 11 50
sec-Butylbenzene 0.0500 0.05321 mg/Kg 106 79 -141 11 50
Styrene 0.0500 0.05332 mg/Kg 107 82 -137 12 50
tert-Butylbenzene 0.0500 0.05191 mg/Kg 104 80 -132 11 50
1,1,1,2-Tetrachloroethane 0.0500 0.05181 mg/Kg 104 80 -136 14 50
1,1,2,2-Tetrachloroethane 0.0500 0.04776 mg/Kg 96 66 -134 9 50
Tetrachloroethene 0.0500 0.06388 mg/Kg 128 78 -140 12 50
Toluene 0.0500 0.05329 mg/Kg 107 80 -132 12 50
trans-1,2-Dichloroethene 0.0500 0.05481 mg/Kg 110 76 -128 10 50
trans-1,3-Dichloropropene 0.0500 0.04337 mg/Kg 87 62 -139 13 50
1,2,3-Trichlorobenzene 0.0500 0.06373 mg/Kg 127 70 -150 12 50
1,2,4-Trichlorobenzene 0.0500 0.06643 mg/Kg 133 62 -150 11 50
1,1,1-Trichloroethane 0.0500 0.05598 mg/Kg 112 72 -140 12 50
1,1,2-Trichloroethane 0.0500 0.05034 mg/Kg 101 78 -128 13 50
Trichloroethene 0.0500 0.05905 mg/Kg 118 77 -127 11 50
Trichlorofluoromethane 0.0500 0.04982 mg/Kg 100 50 -140 9 50
1,2,3-Trichloropropane 0.0500 0.04721 mg/Kg 94 65 -139 11 50
1,2,4-Trimethylbenzene 0.0500 0.05092 mg/Kg 102 77 -139 9 50
1,3,5-Trimethylbenzene 0.0500 0.05262 mg/Kg 105 78 -138 11 50
Vinyl chloride 0.0500 0.04277 mg/Kg 86 47 -136 8 50
Xylenes, Total 0.150 0.1590 mg/Kg 106 80 -137 12 50
4-Bromofluorobenzene (Surr)70 -130
Surrogate
93
LCSD LCSD
Qualifier Limits%Recovery
100Dibromofluoromethane (Surr)70 -130
951,2-Dichloroethane-d4 (Surr)70 -130
94Toluene-d8 (Surr)70 -130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-57063/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57450 Prep Batch: 57063
RL MDL
Acenaphthene ND 0.0670 mg/Kg 02/08/13 06:25 02/09/13 19:20 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0670 mg/Kg 02/08/13 06:25 02/09/13 19:20 1Acenaphthylene
ND 0.0670 mg/Kg 02/08/13 06:25 02/09/13 19:20 1Anthracene
ND 0.0670 mg/Kg 02/08/13 06:25 02/09/13 19:20 1Benzo[a]anthracene
ND 0.0670 mg/Kg 02/08/13 06:25 02/09/13 19:20 1Benzo[a]pyrene
ND 0.0670 mg/Kg 02/08/13 06:25 02/09/13 19:20 1Benzo[b]fluoranthene
ND 0.0670 mg/Kg 02/08/13 06:25 02/09/13 19:20 1Benzo[g,h,i]perylene
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QC Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-57063/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57450 Prep Batch: 57063
RL MDL
Benzo[k]fluoranthene ND 0.0670 mg/Kg 02/08/13 06:25 02/09/13 19:20 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0670 mg/Kg 02/08/13 06:25 02/09/13 19:20 1Chrysene
ND 0.0670 mg/Kg 02/08/13 06:25 02/09/13 19:20 1Dibenz(a,h)anthracene
ND 0.0670 mg/Kg 02/08/13 06:25 02/09/13 19:20 1Fluoranthene
ND 0.0670 mg/Kg 02/08/13 06:25 02/09/13 19:20 1Fluorene
ND 0.0670 mg/Kg 02/08/13 06:25 02/09/13 19:20 1Indeno[1,2,3-cd]pyrene
ND 0.0670 mg/Kg 02/08/13 06:25 02/09/13 19:20 1Naphthalene
ND 0.0670 mg/Kg 02/08/13 06:25 02/09/13 19:20 1Phenanthrene
ND 0.0670 mg/Kg 02/08/13 06:25 02/09/13 19:20 1Pyrene
2-Fluorobiphenyl (Surr)20 X 29-120 02/09/13 19:20 1
MB MB
Surrogate
02/08/13 06:25
Dil FacPreparedAnalyzedQualifierLimits%Recovery
17 X 02/08/13 06:25 02/09/13 19:20 1Nitrobenzene-d5 (Surr)27-120
24 02/08/13 06:25 02/09/13 19:20 1Terphenyl-d14 (Surr)13-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-57063/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57450 Prep Batch: 57063
Acenaphthene 1.67 1.323 mg/Kg 79 36 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 1.67 1.351 mg/Kg 81 38 -120
Anthracene 1.67 1.341 mg/Kg 80 46 -124
Benzo[a]anthracene 1.67 1.280 mg/Kg 77 45 -120
Benzo[a]pyrene 1.67 1.227 mg/Kg 74 45 -120
Benzo[b]fluoranthene 1.67 1.168 mg/Kg 70 42 -120
Benzo[g,h,i]perylene 1.67 1.249 mg/Kg 75 38 -120
Benzo[k]fluoranthene 1.67 1.367 mg/Kg 82 42 -120
Chrysene 1.67 1.297 mg/Kg 78 43 -120
Dibenz(a,h)anthracene 1.67 1.226 mg/Kg 74 32 -128
Fluoranthene 1.67 1.355 mg/Kg 81 46 -120
Fluorene 1.67 1.449 mg/Kg 87 42 -120
Indeno[1,2,3-cd]pyrene 1.67 1.225 mg/Kg 74 41 -121
Naphthalene 1.67 1.169 mg/Kg 70 32 -120
Phenanthrene 1.67 1.444 mg/Kg 87 45 -120
Pyrene 1.67 1.233 mg/Kg 74 43 -120
2-Fluorobiphenyl (Surr)29 -120
Surrogate
72
LCS LCS
Qualifier Limits%Recovery
53Nitrobenzene-d5 (Surr)27 -120
81Terphenyl-d14 (Surr)13 -120
Client Sample ID: Matrix SpikeLab Sample ID: 490-18906-A-1-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57450 Prep Batch: 57063
Acenaphthene ND 1.93 1.319 mg/Kg 68 19 -120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-18906-A-1-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57450 Prep Batch: 57063
Acenaphthylene ND 1.93 1.373 mg/Kg 71 25 -120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Anthracene ND 1.93 1.438 mg/Kg 74 28 -125☼
Benzo[a]anthracene ND 1.93 1.421 mg/Kg 74 23 -120☼
Benzo[a]pyrene ND 1.93 1.387 mg/Kg 68 15 -128☼
Benzo[b]fluoranthene ND 1.93 1.487 mg/Kg 75 12 -133☼
Benzo[g,h,i]perylene ND 1.93 1.464 mg/Kg 76 22 -120☼
Benzo[k]fluoranthene ND 1.93 1.496 mg/Kg 76 28 -120☼
Chrysene ND 1.93 1.543 mg/Kg 78 20 -120☼
Dibenz(a,h)anthracene ND 1.93 1.423 mg/Kg 74 12 -128☼
Fluoranthene ND 1.93 1.507 mg/Kg 78 10 -143☼
Fluorene ND 1.93 1.319 mg/Kg 68 20 -120☼
Indeno[1,2,3-cd]pyrene ND 1.93 1.431 mg/Kg 74 22 -121☼
Naphthalene ND 1.93 1.177 mg/Kg 61 10 -120☼
Phenanthrene ND 1.93 1.564 mg/Kg 81 21 -122☼
Pyrene ND 1.93 1.463 mg/Kg 76 20 -123☼
2-Fluorobiphenyl (Surr)29 -120
Surrogate
57
MS MS
Qualifier Limits%Recovery
46Nitrobenzene-d5 (Surr)27 -120
75Terphenyl-d14 (Surr)13 -120
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-18906-A-1-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57450 Prep Batch: 57063
Acenaphthene ND 1.93 1.389 mg/Kg 72 19 -120 5 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acenaphthylene ND 1.93 1.447 mg/Kg 75 25 -120 5 50☼
Anthracene ND 1.93 1.457 mg/Kg 75 28 -125 1 49☼
Benzo[a]anthracene ND 1.93 1.841 mg/Kg 95 23 -120 26 50☼
Benzo[a]pyrene ND 1.93 1.593 mg/Kg 79 15 -128 14 50☼
Benzo[b]fluoranthene ND 1.93 1.734 mg/Kg 87 12 -133 15 50☼
Benzo[g,h,i]perylene ND 1.93 1.477 mg/Kg 76 22 -120 1 50☼
Benzo[k]fluoranthene ND 1.93 1.733 mg/Kg 88 28 -120 15 45☼
Chrysene ND 1.93 1.837 mg/Kg 93 20 -120 17 49☼
Dibenz(a,h)anthracene ND 1.93 1.433 mg/Kg 74 12 -128 1 50☼
Fluoranthene ND 1.93 2.105 mg/Kg 109 10 -143 33 50☼
Fluorene ND 1.93 1.440 mg/Kg 74 20 -120 9 50☼
Indeno[1,2,3-cd]pyrene ND 1.93 1.474 mg/Kg 76 22 -121 3 50☼
Naphthalene ND 1.93 1.344 mg/Kg 69 10 -120 13 50☼
Phenanthrene ND 1.93 1.746 mg/Kg 90 21 -122 11 50☼
Pyrene ND 1.93 2.088 mg/Kg 108 20 -123 35 50☼
2-Fluorobiphenyl (Surr)29 -120
Surrogate
63
MSD MSD
Qualifier Limits%Recovery
52Nitrobenzene-d5 (Surr)27 -120
73Terphenyl-d14 (Surr)13 -120
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QC Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method: 6010C - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-57413/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 58025 Prep Batch: 57413
RL MDL
Arsenic ND 0.978 mg/Kg 02/09/13 10:48 02/12/13 09:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.978 mg/Kg 02/09/13 10:48 02/12/13 09:16 1Cadmium
ND 0.978 mg/Kg 02/09/13 10:48 02/12/13 09:16 1Chromium
ND 0.978 mg/Kg 02/09/13 10:48 02/12/13 09:16 1Lead
ND 1.96 mg/Kg 02/09/13 10:48 02/12/13 09:16 1Nickel
ND 1.96 mg/Kg 02/09/13 10:48 02/12/13 09:16 1Selenium
ND 1.96 mg/Kg 02/09/13 10:48 02/12/13 09:16 1Thallium
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-57413/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 58025 Prep Batch: 57413
Arsenic 19.2 16.39 mg/Kg 85 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Cadmium 19.2 18.39 mg/Kg 96 80 -120
Chromium 76.8 70.63 mg/Kg 92 80 -120
Lead 19.2 18.45 mg/Kg 96 80 -120
Nickel 192 187.4 mg/Kg 98 80 -120
Selenium 19.2 18.41 mg/Kg 96 80 -120
Thallium 19.2 18.04 mg/Kg 94 80 -120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-57413/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 58025 Prep Batch: 57413
Arsenic 20.2 16.67 mg/Kg 83 80 -120 2 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Cadmium 20.2 19.21 mg/Kg 95 80 -120 4 20
Chromium 80.8 75.01 mg/Kg 93 80 -120 6 20
Lead 20.2 19.13 mg/Kg 95 80 -120 4 20
Nickel 202 195.9 mg/Kg 97 80 -120 4 20
Selenium 20.2 18.93 mg/Kg 94 80 -120 3 20
Thallium 20.2 18.24 mg/Kg 90 80 -120 1 20
Client Sample ID: Matrix SpikeLab Sample ID: 490-18823-C-1-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 58025 Prep Batch: 57413
Arsenic ND 25.5 22.59 mg/Kg 89 75 -125☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Cadmium ND 25.5 23.73 mg/Kg 93 75 -125☼
Chromium 5.23 102 102.6 mg/Kg 96 75 -125☼
Lead 4.14 25.5 30.38 mg/Kg 103 75 -125☼
Nickel 4.98 255 262.5 mg/Kg 101 75 -125☼
Selenium ND 25.5 23.35 mg/Kg 92 75 -125☼
Thallium ND 25.5 24.32 mg/Kg 95 75 -125☼
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QC Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method: 6010C - Metals (ICP) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-18823-C-1-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 58025 Prep Batch: 57413
Arsenic ND 25.1 22.23 mg/Kg 89 75 -125 2 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Cadmium ND 25.1 23.13 mg/Kg 92 75 -125 3 20☼
Chromium 5.23 100 99.37 mg/Kg 94 75 -125 3 20☼
Lead 4.14 25.1 29.52 mg/Kg 101 75 -125 3 20☼
Nickel 4.98 251 255.1 mg/Kg 100 75 -125 3 20☼
Selenium ND 25.1 23.23 mg/Kg 93 75 -125 1 20☼
Thallium ND 25.1 22.86 mg/Kg 91 75 -125 6 20☼
Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique)
Client Sample ID: Method BlankLab Sample ID: MB 490-58046/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 58205 Prep Batch: 58046
RL MDL
Mercury ND 0.0990 mg/Kg 02/12/13 14:01 02/13/13 08:53 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-58046/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 58205 Prep Batch: 58046
Mercury 0.165 0.1576 mg/Kg 96 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: SB-A (6-10')Lab Sample ID: 490-18944-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 58205 Prep Batch: 58046
Mercury ND 0.242 0.2765 mg/Kg 114 80 -120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: SB-A (6-10')Lab Sample ID: 490-18944-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 58205 Prep Batch: 58046
Mercury ND 0.241 0.2701 mg/Kg 112 80 -120 2 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: 7196A - Chromium, Hexavalent
Client Sample ID: Method BlankLab Sample ID: MB 490-57299/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 58389 Prep Batch: 57299
RL MDL
Chromium, hex ND 5.00 mg/Kg 02/08/13 15:46 02/13/13 15:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
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QC Sample Results
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method: 7196A - Chromium, Hexavalent (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-57299/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 58389 Prep Batch: 57299
Chromium, hex 40.0 38.60 mg/Kg 97 85 -115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCSS 490-57299/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 58389 Prep Batch: 57299
Chromium, hex 40.0 39.80 mg/Kg 100 85 -115
Analyte
LCSS LCSS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: SB-A (6-10')Lab Sample ID: 490-18944-1 MSS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 58389 Prep Batch: 57299
Chromium, hex ND 60.3 57.90 mg/Kg 96 75 -125☼
Analyte
MSS MSS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: SB-A (6-10')Lab Sample ID: 490-18944-1 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 58389 Prep Batch: 57299
Chromium, hex ND ND mg/Kg NC 20☼
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-58389/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 58389
Chromium, hex 0.100 0.1030 mg/Kg 103 85 -115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Method: Moisture - Percent Moisture
Client Sample ID: SB-A (6-10')Lab Sample ID: 490-18944-1 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 57103
Percent Solids 66 66 %0.5 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
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QC Association Summary
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
GC/MS VOA
Prep Batch: 57147
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035490-18944-1 SB-A (6-10')Total/NA
Solid 5035490-18944-2 SB-B (6-10')Total/NA
Solid 5035490-18944-3 SB-C (6-10')Total/NA
Solid 5035490-18944-4 SB-C (16-20')Total/NA
Solid 5035490-18944-5 SB-D (4-8')Total/NA
Solid 5035490-18944-6 SB-D (12-16')Total/NA
Solid 5035490-18944-7 SB-E (6-10')Total/NA
Solid 5035490-18944-8 SB-E (16-20')Total/NA
Prep Batch: 57544
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035490-19164-B-3-D MS Matrix Spike Total/NA
Solid 5035490-19164-B-3-E MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 57636
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B 57147490-18944-1 SB-A (6-10')Total/NA
Solid 8260B 57147490-18944-2 SB-B (6-10')Total/NA
Solid 8260B 57147490-18944-3 SB-C (6-10')Total/NA
Solid 8260B 57147490-18944-4 SB-C (16-20')Total/NA
Solid 8260B 57147490-18944-5 SB-D (4-8')Total/NA
Solid 8260B 57147490-18944-6 SB-D (12-16')Total/NA
Solid 8260B 57147490-18944-7 SB-E (6-10')Total/NA
Solid 8260B 57544490-19164-B-3-D MS Matrix Spike Total/NA
Solid 8260B 57544490-19164-B-3-E MSD Matrix Spike Duplicate Total/NA
Solid 8260BLCS 490-57636/3 Lab Control Sample Total/NA
Solid 8260BLCSD 490-57636/4 Lab Control Sample Dup Total/NA
Solid 8260BMB 490-57636/6 Method Blank Total/NA
Analysis Batch: 57826
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B 57147490-18944-8 SB-E (16-20')Total/NA
Solid 8260BLCS 490-57826/3 Lab Control Sample Total/NA
Solid 8260BLCSD 490-57826/4 Lab Control Sample Dup Total/NA
Solid 8260BMB 490-57826/6 Method Blank Total/NA
GC/MS Semi VOA
Prep Batch: 57063
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3550C490-18906-A-1-B MS Matrix Spike Total/NA
Solid 3550C490-18906-A-1-C MSD Matrix Spike Duplicate Total/NA
Solid 3550C490-18944-1 SB-A (6-10')Total/NA
Solid 3550C490-18944-2 SB-B (6-10')Total/NA
Solid 3550C490-18944-3 SB-C (6-10')Total/NA
Solid 3550C490-18944-4 SB-C (16-20')Total/NA
Solid 3550C490-18944-5 SB-D (4-8')Total/NA
Solid 3550C490-18944-6 SB-D (12-16')Total/NA
Solid 3550C490-18944-7 SB-E (6-10')Total/NA
Solid 3550C490-18944-8 SB-E (16-20')Total/NA
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QC Association Summary
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
GC/MS Semi VOA (Continued)
Prep Batch: 57063 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3550CLCS 490-57063/2-A Lab Control Sample Total/NA
Solid 3550CMB 490-57063/1-A Method Blank Total/NA
Analysis Batch: 57450
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 57063490-18906-A-1-B MS Matrix Spike Total/NA
Solid 8270D 57063490-18906-A-1-C MSD Matrix Spike Duplicate Total/NA
Solid 8270D 57063490-18944-1 SB-A (6-10')Total/NA
Solid 8270D 57063490-18944-2 SB-B (6-10')Total/NA
Solid 8270D 57063490-18944-3 SB-C (6-10')Total/NA
Solid 8270D 57063490-18944-4 SB-C (16-20')Total/NA
Solid 8270D 57063490-18944-5 SB-D (4-8')Total/NA
Solid 8270D 57063LCS 490-57063/2-A Lab Control Sample Total/NA
Solid 8270D 57063MB 490-57063/1-A Method Blank Total/NA
Analysis Batch: 57588
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 57063490-18944-6 SB-D (12-16')Total/NA
Solid 8270D 57063490-18944-7 SB-E (6-10')Total/NA
Solid 8270D 57063490-18944-8 SB-E (16-20')Total/NA
Metals
Prep Batch: 57413
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3051A490-18823-C-1-B MS Matrix Spike Total/NA
Solid 3051A490-18823-C-1-C MSD Matrix Spike Duplicate Total/NA
Solid 3051A490-18944-1 SB-A (6-10')Total/NA
Solid 3051A490-18944-2 SB-B (6-10')Total/NA
Solid 3051A490-18944-3 SB-C (6-10')Total/NA
Solid 3051A490-18944-4 SB-C (16-20')Total/NA
Solid 3051A490-18944-5 SB-D (4-8')Total/NA
Solid 3051A490-18944-6 SB-D (12-16')Total/NA
Solid 3051A490-18944-7 SB-E (6-10')Total/NA
Solid 3051A490-18944-8 SB-E (16-20')Total/NA
Solid 3051ALCS 490-57413/2-A Lab Control Sample Total/NA
Solid 3051ALCSD 490-57413/3-A Lab Control Sample Dup Total/NA
Solid 3051AMB 490-57413/1-A Method Blank Total/NA
Analysis Batch: 58025
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010C 57413490-18823-C-1-B MS Matrix Spike Total/NA
Solid 6010C 57413490-18823-C-1-C MSD Matrix Spike Duplicate Total/NA
Solid 6010C 57413490-18944-1 SB-A (6-10')Total/NA
Solid 6010C 57413490-18944-2 SB-B (6-10')Total/NA
Solid 6010C 57413490-18944-3 SB-C (6-10')Total/NA
Solid 6010C 57413490-18944-4 SB-C (16-20')Total/NA
Solid 6010C 57413490-18944-5 SB-D (4-8')Total/NA
Solid 6010C 57413490-18944-6 SB-D (12-16')Total/NA
Solid 6010C 57413490-18944-7 SB-E (6-10')Total/NA
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QC Association Summary
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Metals (Continued)
Analysis Batch: 58025 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010C 57413490-18944-8 SB-E (16-20')Total/NA
Solid 6010C 57413LCS 490-57413/2-A Lab Control Sample Total/NA
Solid 6010C 57413LCSD 490-57413/3-A Lab Control Sample Dup Total/NA
Solid 6010C 57413MB 490-57413/1-A Method Blank Total/NA
Prep Batch: 58046
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471B490-18944-1 SB-A (6-10')Total/NA
Solid 7471B490-18944-1 MS SB-A (6-10')Total/NA
Solid 7471B490-18944-1 MSD SB-A (6-10')Total/NA
Solid 7471B490-18944-2 SB-B (6-10')Total/NA
Solid 7471B490-18944-3 SB-C (6-10')Total/NA
Solid 7471B490-18944-4 SB-C (16-20')Total/NA
Solid 7471B490-18944-5 SB-D (4-8')Total/NA
Solid 7471B490-18944-6 SB-D (12-16')Total/NA
Solid 7471B490-18944-7 SB-E (6-10')Total/NA
Solid 7471B490-18944-8 SB-E (16-20')Total/NA
Solid 7471BLCS 490-58046/2-A Lab Control Sample Total/NA
Solid 7471BMB 490-58046/1-A Method Blank Total/NA
Analysis Batch: 58205
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471B 58046490-18944-1 SB-A (6-10')Total/NA
Solid 7471B 58046490-18944-1 MS SB-A (6-10')Total/NA
Solid 7471B 58046490-18944-1 MSD SB-A (6-10')Total/NA
Solid 7471B 58046490-18944-2 SB-B (6-10')Total/NA
Solid 7471B 58046490-18944-3 SB-C (6-10')Total/NA
Solid 7471B 58046490-18944-4 SB-C (16-20')Total/NA
Solid 7471B 58046490-18944-5 SB-D (4-8')Total/NA
Solid 7471B 58046490-18944-6 SB-D (12-16')Total/NA
Solid 7471B 58046490-18944-7 SB-E (6-10')Total/NA
Solid 7471B 58046490-18944-8 SB-E (16-20')Total/NA
Solid 7471B 58046LCS 490-58046/2-A Lab Control Sample Total/NA
Solid 7471B 58046MB 490-58046/1-A Method Blank Total/NA
General Chemistry
Analysis Batch: 57103
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture490-18944-1 SB-A (6-10')Total/NA
Solid Moisture490-18944-1 DU SB-A (6-10')Total/NA
Solid Moisture490-18944-2 SB-B (6-10')Total/NA
Solid Moisture490-18944-3 SB-C (6-10')Total/NA
Solid Moisture490-18944-4 SB-C (16-20')Total/NA
Solid Moisture490-18944-5 SB-D (4-8')Total/NA
Solid Moisture490-18944-6 SB-D (12-16')Total/NA
Solid Moisture490-18944-7 SB-E (6-10')Total/NA
Solid Moisture490-18944-8 SB-E (16-20')Total/NA
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QC Association Summary
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
General Chemistry (Continued)
Prep Batch: 57299
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3060A490-18944-1 SB-A (6-10')Total/NA
Solid 3060A490-18944-1 DU SB-A (6-10')Total/NA
Solid 3060A490-18944-1 MSI SB-A (6-10')Total/NA
Solid 3060A490-18944-1 MSS SB-A (6-10')Total/NA
Solid 3060A490-18944-2 SB-B (6-10')Total/NA
Solid 3060A490-18944-3 SB-C (6-10')Total/NA
Solid 3060A490-18944-4 SB-C (16-20')Total/NA
Solid 3060A490-18944-5 SB-D (4-8')Total/NA
Solid 3060A490-18944-6 SB-D (12-16')Total/NA
Solid 3060A490-18944-7 SB-E (6-10')Total/NA
Solid 3060A490-18944-8 SB-E (16-20')Total/NA
Solid 3060ALCS 490-57299/2-A Lab Control Sample Total/NA
Solid 3060ALCSI 490-57299/4-A Lab Control Sample Total/NA
Solid 3060ALCSS 490-57299/3-A Lab Control Sample Total/NA
Solid 3060AMB 490-57299/1-A Method Blank Total/NA
Analysis Batch: 58389
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7196A 57299490-18944-1 SB-A (6-10')Total/NA
Solid 7196A 57299490-18944-1 DU SB-A (6-10')Total/NA
Solid 7196A 57299490-18944-1 MSI SB-A (6-10')Total/NA
Solid 7196A 57299490-18944-1 MSS SB-A (6-10')Total/NA
Solid 7196A 57299490-18944-2 SB-B (6-10')Total/NA
Solid 7196A 57299490-18944-3 SB-C (6-10')Total/NA
Solid 7196A 57299490-18944-4 SB-C (16-20')Total/NA
Solid 7196A 57299490-18944-5 SB-D (4-8')Total/NA
Solid 7196A 57299490-18944-6 SB-D (12-16')Total/NA
Solid 7196A 57299490-18944-7 SB-E (6-10')Total/NA
Solid 7196A 57299490-18944-8 SB-E (16-20')Total/NA
Solid 7196A 57299LCS 490-57299/2-A Lab Control Sample Total/NA
Solid 7196ALCS 490-58389/3 Lab Control Sample Total/NA
Solid 7196A 57299LCSI 490-57299/4-A Lab Control Sample Total/NA
Solid 7196A 57299LCSS 490-57299/3-A Lab Control Sample Total/NA
Solid 7196A 57299MB 490-57299/1-A Method Blank Total/NA
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-18944-1
Project/Site: Carolina Metals Site SDG: SLS-001
Client Sample ID: SB-A (6-10')Lab Sample ID: 490-18944-1
Matrix: SolidDate Collected: 02/06/13 12:05
Percent Solids: 66.3Date Received: 02/07/13 08:20
Prep 5035 02/08/13 10:02 ML57147 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8260B 1 57636 02/11/13 18:48 KK TAL NSHTotal/NA
Prep 3550C 57063 02/08/13 10:48 AK TAL NSHTotal/NA
Analysis 8270D 1 57450 02/10/13 00:46 BS TAL NSHTotal/NA
Prep 3051A 57413 02/09/13 10:48 SR TAL NSHTotal/NA
Analysis 6010C 1 58025 02/12/13 10:06 BB TAL NSHTotal/NA
Prep 7471B 58046 02/12/13 14:01 LB TAL NSHTotal/NA
Analysis 7471B 1 58205 02/13/13 08:57 LB TAL NSHTotal/NA
Analysis Moisture 1 57103 02/08/13 08:15 RS TAL NSHTotal/NA
Prep 3060A 57299 02/08/13 15:46 AB TAL NSHTotal/NA
Analysis 7196A 1 58389 02/13/13 15:17 AB TAL NSHTotal/NA
Client Sample ID: SB-B (6-10')Lab Sample ID: 490-18944-2
Matrix: SolidDate Collected: 02/06/13 12:15
Percent Solids: 66.1Date Received: 02/07/13 08:20
Prep 5035 02/08/13 10:02 ML57147 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8260B 1 57636 02/11/13 19:19 KK TAL NSHTotal/NA
Prep 3550C 57063 02/08/13 10:48 AK TAL NSHTotal/NA
Analysis 8270D 1 57450 02/10/13 01:11 BS TAL NSHTotal/NA
Prep 3051A 57413 02/09/13 10:48 SR TAL NSHTotal/NA
Analysis 6010C 2 58025 02/12/13 11:17 BB TAL NSHTotal/NA
Prep 7471B 58046 02/12/13 14:01 LB TAL NSHTotal/NA
Analysis 7471B 1 58205 02/13/13 09:03 LB TAL NSHTotal/NA
Analysis Moisture 1 57103 02/08/13 08:15 RS TAL NSHTotal/NA
Prep 3060A 57299 02/08/13 15:46 AB TAL NSHTotal/NA
Analysis 7196A 1 58389 02/13/13 15:17 AB TAL NSHTotal/NA
Client Sample ID: SB-C (6-10')Lab Sample ID: 490-18944-3
Matrix: SolidDate Collected: 02/06/13 10:15
Percent Solids: 75.9Date Received: 02/07/13 08:20
Prep 5035 02/08/13 10:02 ML57147 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8260B 1 57636 02/11/13 19:50 KK TAL NSHTotal/NA
Prep 3550C 57063 02/08/13 10:48 AK TAL NSHTotal/NA
Analysis 8270D 1 57450 02/10/13 01:36 BS TAL NSHTotal/NA
Prep 3051A 57413 02/09/13 10:48 SR TAL NSHTotal/NA
Analysis 6010C 2 58025 02/12/13 11:20 BB TAL NSHTotal/NA
Prep 7471B 58046 02/12/13 14:01 LB TAL NSHTotal/NA
Analysis 7471B 1 58205 02/13/13 09:06 LB TAL NSHTotal/NA
Analysis Moisture 1 57103 02/08/13 08:15 RS TAL NSHTotal/NA
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-18944-1
Project/Site: Carolina Metals Site SDG: SLS-001
Client Sample ID: SB-C (6-10')Lab Sample ID: 490-18944-3
Matrix: SolidDate Collected: 02/06/13 10:15
Percent Solids: 75.9Date Received: 02/07/13 08:20
Prep 3060A 02/08/13 15:46 AB57299 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 7196A 1 58389 02/13/13 15:17 AB TAL NSHTotal/NA
Client Sample ID: SB-C (16-20')Lab Sample ID: 490-18944-4
Matrix: SolidDate Collected: 02/06/13 10:20
Percent Solids: 68.7Date Received: 02/07/13 08:20
Prep 5035 02/08/13 10:02 ML57147 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8260B 1 57636 02/11/13 20:21 KK TAL NSHTotal/NA
Prep 3550C 57063 02/08/13 10:48 AK TAL NSHTotal/NA
Analysis 8270D 1 57450 02/10/13 00:21 BS TAL NSHTotal/NA
Prep 3051A 57413 02/09/13 10:48 SR TAL NSHTotal/NA
Analysis 6010C 2 58025 02/12/13 11:24 BB TAL NSHTotal/NA
Prep 7471B 58046 02/12/13 14:01 LB TAL NSHTotal/NA
Analysis 7471B 1 58205 02/13/13 09:08 LB TAL NSHTotal/NA
Analysis Moisture 1 57103 02/08/13 08:15 RS TAL NSHTotal/NA
Prep 3060A 57299 02/08/13 15:46 AB TAL NSHTotal/NA
Analysis 7196A 1 58389 02/13/13 15:17 AB TAL NSHTotal/NA
Client Sample ID: SB-D (4-8')Lab Sample ID: 490-18944-5
Matrix: SolidDate Collected: 02/06/13 11:25
Percent Solids: 77.2Date Received: 02/07/13 08:20
Prep 5035 02/08/13 10:02 ML57147 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8260B 1 57636 02/11/13 20:52 KK TAL NSHTotal/NA
Prep 3550C 57063 02/08/13 10:48 AK TAL NSHTotal/NA
Analysis 8270D 1 57450 02/10/13 02:01 BS TAL NSHTotal/NA
Prep 3051A 57413 02/09/13 10:48 SR TAL NSHTotal/NA
Analysis 6010C 2 58025 02/12/13 11:39 BB TAL NSHTotal/NA
Prep 7471B 58046 02/12/13 14:01 LB TAL NSHTotal/NA
Analysis 7471B 1 58205 02/13/13 09:10 LB TAL NSHTotal/NA
Analysis Moisture 1 57103 02/08/13 08:15 RS TAL NSHTotal/NA
Prep 3060A 57299 02/08/13 15:46 AB TAL NSHTotal/NA
Analysis 7196A 1 58389 02/13/13 15:17 AB TAL NSHTotal/NA
Client Sample ID: SB-D (12-16')Lab Sample ID: 490-18944-6
Matrix: SolidDate Collected: 02/06/13 11:30
Percent Solids: 69.5Date Received: 02/07/13 08:20
Prep 5035 02/08/13 10:02 ML57147 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
TestAmerica Nashville
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-18944-1
Project/Site: Carolina Metals Site SDG: SLS-001
Client Sample ID: SB-D (12-16')Lab Sample ID: 490-18944-6
Matrix: SolidDate Collected: 02/06/13 11:30
Percent Solids: 69.5Date Received: 02/07/13 08:20
Analysis 8260B 02/11/13 21:23 KK157636 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3550C 57063 02/08/13 10:48 AK TAL NSHTotal/NA
Analysis 8270D 1 57588 02/11/13 16:45 BS TAL NSHTotal/NA
Prep 3051A 57413 02/09/13 10:48 SR TAL NSHTotal/NA
Analysis 6010C 2 58025 02/12/13 11:43 BB TAL NSHTotal/NA
Prep 7471B 58046 02/12/13 14:01 LB TAL NSHTotal/NA
Analysis 7471B 1 58205 02/13/13 09:12 LB TAL NSHTotal/NA
Analysis Moisture 1 57103 02/08/13 08:15 RS TAL NSHTotal/NA
Prep 3060A 57299 02/08/13 15:46 AB TAL NSHTotal/NA
Analysis 7196A 1 58389 02/13/13 15:17 AB TAL NSHTotal/NA
Client Sample ID: SB-E (6-10')Lab Sample ID: 490-18944-7
Matrix: SolidDate Collected: 02/06/13 10:50
Percent Solids: 72.1Date Received: 02/07/13 08:20
Prep 5035 02/08/13 10:02 ML57147 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8260B 1 57636 02/11/13 21:55 KK TAL NSHTotal/NA
Prep 3550C 57063 02/08/13 10:48 AK TAL NSHTotal/NA
Analysis 8270D 1 57588 02/11/13 17:11 BS TAL NSHTotal/NA
Prep 3051A 57413 02/09/13 10:48 SR TAL NSHTotal/NA
Analysis 6010C 2 58025 02/12/13 11:46 BB TAL NSHTotal/NA
Prep 7471B 58046 02/12/13 14:01 LB TAL NSHTotal/NA
Analysis 7471B 1 58205 02/13/13 09:18 LB TAL NSHTotal/NA
Analysis Moisture 1 57103 02/08/13 08:15 RS TAL NSHTotal/NA
Prep 3060A 57299 02/08/13 15:46 AB TAL NSHTotal/NA
Analysis 7196A 1 58389 02/13/13 15:17 AB TAL NSHTotal/NA
Client Sample ID: SB-E (16-20')Lab Sample ID: 490-18944-8
Matrix: SolidDate Collected: 02/06/13 11:00
Percent Solids: 73.4Date Received: 02/07/13 08:20
Prep 5035 02/08/13 10:02 ML57147 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8260B 1 57826 02/12/13 10:18 KK TAL NSHTotal/NA
Prep 3550C 57063 02/08/13 10:48 AK TAL NSHTotal/NA
Analysis 8270D 1 57588 02/11/13 17:38 BS TAL NSHTotal/NA
Prep 3051A 57413 02/09/13 10:48 SR TAL NSHTotal/NA
Analysis 6010C 1 58025 02/12/13 10:31 BB TAL NSHTotal/NA
Prep 7471B 58046 02/12/13 14:01 LB TAL NSHTotal/NA
Analysis 7471B 1 58205 02/13/13 09:20 LB TAL NSHTotal/NA
Analysis Moisture 1 57103 02/08/13 08:15 RS TAL NSHTotal/NA
Prep 3060A 57299 02/08/13 15:48 AB TAL NSHTotal/NA
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-18944-1
Project/Site: Carolina Metals Site SDG: SLS-001
Client Sample ID: SB-E (16-20')Lab Sample ID: 490-18944-8
Matrix: SolidDate Collected: 02/06/13 11:00
Percent Solids: 73.4Date Received: 02/07/13 08:20
Analysis 7196A 02/13/13 15:17 AB158389 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Method Summary
TestAmerica Job ID: 490-18944-1Client: Hart & Hickman, PC
SDG: SLS-001Project/Site: Carolina Metals Site
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8468270DSemivolatile Organic Compounds (GC/MS)TAL NSH
SW8466010CMetals (ICP)TAL NSH
SW8467471BMercury in Solid or Semisolid Waste (Manual Cold Vapor Technique)TAL NSH
SW8467196AChromium, Hexavalent TAL NSH
EPAMoisturePercent Moisture TAL NSH
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Certification Summary
Client: Hart & Hickman, PC TestAmerica Job ID: 490-18944-1
Project/Site: Carolina Metals Site SDG: SLS-001
Laboratory: TestAmerica Nashville
All certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
10-30-13393ACIL
A2LA ISO/IEC 17025 0453.07 12-31-13
Alabama State Program 4 41150 05-31-13
Alaska (UST)State Program 10 UST-087 07-24-13
Arizona State Program 9 AZ0473 05-05-13
Arkansas DEQ State Program 6 88-0737 04-25-13
California NELAP 9 1168CA 10-31-13
Canadian Assoc Lab Accred (CALA)Canada 3744 03-08-14
Colorado State Program 8 N/A 02-28-13
Connecticut State Program 1 PH-0220 12-31-13
Florida NELAP 4 E87358 06-30-13
Illinois NELAP 5 200010 12-09-13
Iowa State Program 7 131 05-01-14
Kansas NELAP 7 E-10229 10-31-13
Kentucky (UST)State Program 4 19 09-15-13
Louisiana NELAP 6 30613 06-30-13
Maryland State Program 3 316 03-31-13
Massachusetts State Program 1 M-TN032 06-30-13
Minnesota NELAP 5 047-999-345 12-31-13
Mississippi State Program 4 N/A 06-30-13
Montana (UST)State Program 8 NA 01-01-15
Nevada State Program 9 TN00032 07-31-13
New Hampshire NELAP 1 2963 10-09-13
New Jersey NELAP 2 TN965 06-30-13
New York NELAP 2 11342 04-01-13
North Carolina DENR State Program 4 387 12-31-13
North Dakota State Program 8 R-146 06-30-13
Ohio VAP State Program 5 CL0033 01-19-14
Oklahoma State Program 6 9412 08-31-13
Oregon NELAP 10 TN200001 04-30-13
Pennsylvania NELAP 3 68-00585 06-30-13
Rhode Island State Program 1 LAO00268 12-30-13
South Carolina State Program 4 84009 [phone]
South Carolina State Program 4 84009 [phone]
Tennessee State Program 4 2008 02-23-14
Texas NELAP 6 T104704077-09-TX 08-31-13
USDA Federal S-48469 11-02-13
Utah NELAP 8 TAN 06-30-13
Virginia NELAP 3 460152 06-14-13
Washington State Program 10 C789 07-19-13
West Virginia DEP State Program 3 219 02-28-13
Wisconsin State Program 5 998020430 08-31-13
Wyoming (UST)A2LA 8 453.07 12-31-13
TestAmerica Nashville
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Login Sample Receipt Checklist
Client: Hart & Hickman, PC Job Number: 490-18944-1
SDG Number: SLS-001
Login Number: 18944
Question Answer Comment
Creator: Ford, Easton
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a
survey meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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