Charlotte Chemical_Soil Mgmt Rpt

BROWNFIELD SOIL MANAGEMENT
REPORT

CHARLOTTE CHEMICAL
1100 SOUTH BOULEVARD
CHARLOTTE, NC

Prepared for:

North Carolina Department of Environmental
Quality
217 W Jones Street
Raleigh, NC 27603

Prepared By:

EFI Global, Inc.
9307 Monroe Road, Suite M
Charlotte, NC 28270

EFI Project No. 94705-07722
February 2, 2016

Charlotte Chemical 1 February 2, 2016
Charlotte, NC Project Number 94705-07722
9307 Monroe Road
Suite M
Charlotte, NC 28270
Tel: [phone]
TF: 866-964-6334
Fax: [phone]
www.efiglobal.com
Project No. 94705-07722
February 2, 2016

Ms. Carolyn Minnich
Brownfields Project Manager
NC Department of Environmental Quality
217 W Jones Street
Raleigh, NC 27603

Re: Brownfield Soil Management Report
Charlotte Chemical
1100 South Boulevard
Charlotte, NC
Former EFI Project # 98411-09470

Dear Ms. Minnich:

EFI Global, Inc. (EFI) is presenting the documentation for a Brownfield Soil Management Report
performed at Charlotte Chemical, Simpson Lighting, 1100 South Boulevard, Charlotte, North
Carolina (Site), as required by the Soil Management Plan respecting the Site (described in
greater detail below). The report is being performed to provide documentation on the outcomes
of discovered underground storage tanks (USTs), drum oil house excavation (storm water vault)
and disposal of impacted soil related to undiscovered soil conditions at the Site.

PURPOSE

The purpose of this report is to provide the environmental status of the discovered USTs, storm
water vault excavation, and impacted soil associated with excavation completed at the Site.
The information provided in this report describes the scope of work performed during the
investigation and provides documentation of the factual findings of the investigation.

BACKGROUND INFORMATION

The Former Simpson Lighting Property (Charlotte Chemical Laboratory) is a Brownfield site with
an existing Brownfield Agreement with the North Carolina Department of Environmental Quality
(NCDEQ). Maps illustrating the topography, tank locations, and boring locations are provided in
Appendix 1. The Notice of Brownfield Property (NBP) was made effective November 23, 2010
with the Prospective Developer, 1200 South Boulevard, LLC. The current owner and
redeveloper of the Site is TP 1100 South Blvd, LLC.

Charlotte Chemical 2 February 2, 2016
Charlotte, NC Project Number 94705-07722
Previous environmental and engineering studies were performed at the Site by others
associated with previous site redevelopment due diligence activities. Areas of environmental
concern were previously identified at the Site associated with the historical site uses, including
the former Charlotte Chemical Laboratory, dye house operations, oil storage, gasoline and
diesel underground storage tanks, a former gasoline station, and sumps associated with water
discharge from a geothermal well system. Planned redevelopment activities included balancing
the site elevation by cutting soil from the northern portion of the Site to fill the southern portion of
the Site. Following the grading activities, a six-story structure was constructed over the majority
of the Site. The structure has an open air, two-story podium parking garage topped with four
stories of apartments.

The redevelopment activities were planned in accordance with the Brownfields Agreement that
specifies, among other things specified that a Soil Management Plan (SMP) be prepared,
approved by NCDEQ, and implemented during site development. TP 1100 South Boulevard
Partners, LLC conducted additional assessment activities to evaluate environmental conditions
at the Site and in support of preparing the SMP. The SMP was submitted to NCDEQ on January
27, 2012 for their review and the Report of Environmental Assessment was prepared to
document the sampling activities conducted in 2011. A copy of the SMP is provided as
Appendix 2.

Assessment activities by AMEC concluded that soil in the northern portion of the Site, between
Palmer Avenue and Carson Boulevard, did not exhibit impacts from volatile organic compounds
(VOCs), semi-volatile organic compounds (SVOCs), or metals requiring additional action.
Historical information, soil analytical results, and a geophysical survey did not indicate the
presence of environmental concerns in this area. Soil located south of Palmer Avenue,
generally indicated the presence of PAHs and metals consistent with historical results.

Groundwater was previously encountered between 20 and 25 feet below grade level and was
determined to flow south to southwest. Minor impacts (VOCs and PAHs) were noted in the
southern and central portions of the Site based on previous assessments. Recent groundwater
assessment results from the northern portion of the Site did not indicate environmental impacts
associated with historical activities. No USTs were identified in the areas survey, although a
small area could not be scanned in the vicinity of the former gasoline service stations. AMEC’s
report also indicated that bricks and other debris were noted during assessment activities. The
debris was not to be considered environmentally impacted but could provide complications for
development.

Charlotte Chemical 3 February 2, 2016
Charlotte, NC Project Number 94705-07722
HEALTH AND SAFETY PLAN

EFI developed a Health and Safety Plan that was specific to the Site. The development of this
plan is required by the Occupational Safety and Health Administration (OSHA) under Hazardous
Waste Operations & Emergency Response 29 CFR 1910.120. The Health and Safety Plan was
designed to reduce the risk of physical or chemical exposures that may affect on-site workers in
the proposed work area. The Health and Safety Plan includes information about chemicals
expected on the Site, health and safety procedures, and emergency response procedures. The
Health and Safety Plan is attached in Appendix 3.

SUBSURFACE INVESTIGATION

Field Activities Borings and Dry Wells

EFI conducted a preliminary field investigation by completing six borings at the Site. The Limited
Subsurface Investigation was conducted on October 25, 2013. During the investigation, nine
soil borings (EFI-1 through EFI-9) were advanced at the Site by Probe Technology with a
Geoprobe drilling rig. The borings were completed around the Site to evaluate potential gaps in
the previous data. The soil boring locations completed by EFI and others are illustrated in
Appendix 1. The AMEC report provides some back up on the other soil borings completed at the
Site.

Soil Sampling

Soil samples were continuously collected from borings EFI-1 through EFI-9 with a four-foot long
stainless-steel macro core and disposable acetate sleeves to various terminal depth. The soil
samples collected from each boring were field screened with a photo-ionization detector (PID) to
determine if volatile organic vapors were present. There were no field screening readings,
olfactory or visual indications of contamination detected in any of the soil samples. Based upon
the PID results and field observations, soil samples were collected for chemical analysis from
borings EFI-1 at 13 feet, EFI-2 at 7 feet, 13 feet, and 17 feet, EFI-3 at 8 feet and 14 feet, EFI-6
at 8 feet and 14 feet, and EFI-7 at 8 feet and 18 feet.

Soil borings EFI-8 and EFI-9 were completed to evaluate evidence of odor or staining only as no
soil samples were collected from these borings. EFI-8 was associated with potential dispensers
and EFI-9 was completed near a former UST location.

Soil encountered at the Site consisted mainly of light brown to red to beige silty clay with some
rubble debris present at depths.

Charlotte Chemical 4 February 2, 2016
Charlotte, NC Project Number 94705-07722
Ground Water Sampling

Ground water was not encountered in the borings and no groundwater samples were collected.

Laboratory Analytical Results

The soil samples were transported under chain of custody to Pace Analytical Services (Pace) of
Huntersville, North Carolina. Pace is a North Carolina certified laboratory. Eleven soil samples
were submitted to Pace. The samples were analyzed for volatile organic compounds (VOCs) by
EPA Method 8260 and poly-nuclear aromatic hydrocarbons (PAHs) by EPA Method 8270, for
total petroleum hydrocarbons (TPH), and metals.

According to the laboratory analytical report, PAHs, TPH, and metals were detected in several
of the samples, however the concentrations were less than the residential standards. The soil
analytical results are summarized in Table 1. The laboratory analytical report and chain-of-
custody forms are included as Appendix 4.

RESULTS OF SOIL MANAGEMENT ACTIVITIES

Five USTs and a water tank were discovered at the Site before and during development
activities. UST-1 and petroleum-impacted soil were discovered during assessment activities;
UST-2, UST-3, UST-4, UST-5 and petroleum-impacted soil were discovered during grading
activities; UST-7 and petroleum-impacted soil were discovered during vibro-pier installation;
petroleum-impacted soil was discovered during the construction of a storm water vault; and
water tank 6 was discovered during grading activities. Brownfields personnel were notified via
email regarding the discovery of the USTs and impacted soil. A summary of each incident is
described below:

UST-1

A 3,000-gallon UST (UST-1) was discovered at the Site in October 2013. Because the UST was
likely last used prior to redevelopment of the Site with Simpson Lighting or the Charlotte
Chemical building, the UST was considered to be an orphan tank, and TP 1100 South
Boulevard Partners, LLC is not the responsible party. On November 8, 2013, the Brownfields
Program project manager was notified by email regarding the discovery of UST-1. Fuel oil and
water were removed from the UST prior to removal and petroleum-impacted soil was identified
in the area of the UST. After the UST was excavated, the bottom and sidewalls of the tank basin
were sampled and the samples were analyzed in accordance with Brownfields Program
requirements. After the soil sampling and additional excavation activities were completed, it was
determined that the petroleum impact was removed from the former UST basin and the soil at

Charlotte Chemical 5 February 2, 2016
Charlotte, NC Project Number 94705-07722
the bottom of the former UST basin was below residential standards. A UST Management Letter
with correspondence to and from NCDEQ, dated January 14, 2014 is attached as Appendix 5,
along with email to and from NCDEQ, and information associated with UST-1, UST-2, and UST-
3 (discussed below). Brownfields personnel concluded that no additional information was
required and that it was not necessary to add data concerning UST-1 to the plat. The disposal
manifests for impacted soil and water/sludge removed from the tank, and the analytical results,
are provided in Appendix 6.

Additionally, EFI completed a test pit near the edge of the UST basin. It was determined that
total petroleum hydrocarbons were present in the upper overburden of the UST and vault area.
Copies of the disposal manifests are included in Appendix 5. The soil analytical results are
summarized in Table 2. The laboratory analytical report and chain-of-custody forms are
included as Appendix 7. Photographic documentation is included in Appendix 8.

STORM WATER VAULT

After the removal of UST-1, excavation began on a storm water vault which included the area of
UST-1. Petroleum-impacted soil and other debris identified in this area were excavated and
removed from the Site. The storm water vault excavation was approximately 132 feet long by
96 feet wide by 20 feet deep. Approximately 6,505 tons of soil were removed from this area,
including 2,725 tons of petroleum-impacted soil. The soil disposal manifests are presented in
Appendix 9. Included with the manifest are the profiles sheets highlighted with the laboratory
sample IDs. Photo documentation is included in Appendix 10. The laboratory analytical report
and chain-of-custody forms are included with the documents associated with UST-1.

UST-2, UST-3, AND UST-4

UST-2, UST-3, and UST-4s were discovered during the grading activities and were believed to
have been associated with a former filling station. Sand was discovered in the USTs, therefore
it was determined that the USTs had been previously abandoned in place. The USTs were
likely last used in the 1960s, so TP 1100 South Boulevard Partners, LLC is neither the owner
nor the operator of the USTs, and there is no known responsible party for the USTs. The UST
Management Report summarizes the activities associated with UST-2, UST-3, and UST-4 is
provided in Appendix 5.

On December 3, 2013, the Brownfields Program project manager was notified via email
regarding the discovery of UST-2. On December 11, 2013, the Brownfields Program project
manager was notified via email regarding the discovery of UST-3 and UST-4. The project
manager was also notified that the developer was planning to place excavated soil back in to
the tank basins if impact was not present at elevated concentrations. Brownfields personnel

Charlotte Chemical 6 February 2, 2016
Charlotte, NC Project Number 94705-07722
indicated via email dated December 17, 2013 that it assuming the soil would be within
acceptable risk levels for the property, placing overburden soil back into the original hole was
acceptable. As documented in the UST Management Report, the overburden soil did not reveal
any evidence of impacts exceeding detection limits. The USTs were removed and the sidewalls
and bottoms were sampled in accordance with Brownfields requirements.

Based on the analytical report, the contaminant concentrations in soil at the bottom of the
former UST basin were below residential standards. Approximately 800 tons of petroleum-
impacted soil were excavated and transported to an off-site disposal facility. In the email dated
February 18, 2014, Brownfields personnel indicated that no additional assessment was
necessary in the vicinity of UST-2, UST-3, and UST-4, and that soil that exceeded the IHSB
Residential Preliminary Soil Remediation Goals (PRSG) were removed from the Property in
these areas, therefore no changes were necessary to the Brownfields Plat Map.

Certificates of disposal are attached in Appendix 11. The soil analytical results are summarized
in Table 3. The laboratory analytical report and chain-of-custody forms are included as
Appendix 12. Appendix 13 provides photographic documentation of the UST removal.

WATER TANK 6

During grading, a steel tank believed to be a boiler tank or water tank for a boiler system was
discovered near the storm water catch basin. The water tank was not a UST, therefore TP 1100
South Boulevard Partners, LLC was not legally responsible for water tank 6. However, soil
samples were collected in accordance with Brownfields requirements. No contaminants were
detected in the soil samples that were collected from the bottom and sidewalls of the tank basin.
Photo-documentation of the tank is presented in Appendix 14. The water tank was removed
with UST-5 (see below). Copies of the disposal manifests are provided in Appendix 15. The
laboratory analytical report and chain-of-custody forms are included as Appendix 16.

UST-5 AND UST-7

Two orphan tanks (UST-5 and UST-7) were found during grading and vibro-pier installation
activities. Petroleum-impacted soil was found at the bottom of UST-5 and at the bottom and
sidewalls of UST-7. Due to the age of the USTs, TP 1100 South Boulevard Partners, LLC is not
the responsible party.

The former tank basins were sampled in accordance with Brownfields requirements. According
to the laboratory analytical report for UST-5, diesel range organics and poly-nuclear aromatic
hydrocarbons were detected in one bottom sample at concentrations exceeding the residential
standards. The impacted soil was removed and the area was resampled. The second round of

Charlotte Chemical 7 February 2, 2016
Charlotte, NC Project Number 94705-07722
sampling indicated no contaminants were detected at concentrations exceeding the residential
standards. Additionally, the bottom and sidewalls were sampled at UST-7. Impact was noted on
both end sidewalls and one bottom sample at concentrations exceeding residential standards.
Therefore, additional soil was excavated from the impacted sidewalls and bottom. Initially,
approximately 150 tons of soil were excavated, and the Brownfields program was notified in the
email dated March 12, 2014. Additional soil was excavated from the UST-7 area after sampling
results determined that more impacted soil was present. Approximately 347 tons of petroleum-
impacted soil were eventually excavated and removed from the Site. This total included a small
about of soil from vibro-pier 159 (see below). A report that provides details about USTs 5 and 7
is provided in Appendix 17. Included in the report are disposal manifests, laboratory reports, and
photographs. Additionally, Table 4 provides the analytical results for UST-5 and Table 5
provides the analytical results for UST-7.

After receiving the report, the Brownfields Program indicated in the email dated March 13, 2014,
that based on the soil samples and information submitted to NC Brownfields Program, no
additional assessment was necessary in the vicinity of UST-5 or UST-7. Additionally, based on
the reports provided to the Brownfields Program, soil that exceeded the IHSB Residential
Preliminary Soil Remediation Goals (PRSG) was removed from the property in these areas,
therefore no changes were necessary to the Brownfields Plat Map. A copy of the email is
provided in Appendix 17.

VIBRO-PIER SOIL CUTTINGS

Vibro-piers were installed on Pads 1, 2, and 3 to increase bearing pressure and mitigate
settlement for future construction. In one area (Pier 159), heavily-stained soil and petroleum
odor were observed. The impacted soil was transported to an off-site disposal facility. In an
email dated July 20, 2014, the Brownfields Program was notified about the impacted soil, and
was informed that the soil generated during the installation of the surrounding piers was clean
and that some overexcavation had occurred at Pier 159, however collecting confirmation
samples was difficult due to space constraints in the excavation. In the email dated September
23, 2014, the Brownfields Program indicated that no additional informational data needed to
added to the Brownfields Plat map at this time. The soil analytical results from Pad 1 and Pad 2
are summarized in Table 6. The September 23, 2014 email, the laboratory analytical report, and
chain-of-custody forms are included as Appendix 18.

At one location a concrete storm line was encountered and had to be excavated. Most of the
soil excavated was placed back into the excavation, however unsuitable material was stockpiled
with soil cuttings from Pad 1 and 2. Additionally, the soil cuttings from all vibro-piers were
eventually stockpiled on Pad 3. The soil analytical results from Pad 3 are summarized in Table
7. The laboratory analytical report and chain-of-custody forms are included as Appendix 19.

Charlotte Chemical 8 February 2, 2016
Charlotte, NC Project Number 94705-07722
In addition, some soil cuttings from the vibro-piers from Pad 3 were stockpiled on Pad 1, and
were sampled for chemical analysis to facilitate their disposition. The laboratory results
indicated elevated concentrations of mercury in the soil samples. EFI understands additional
samples were analyzed for metal by the TCLP procedure, and that this soil was accepted by an
approved landfill. The laboratory reports are included in Appendix 19.

OVER EXCAVATION

EFI observed several areas on Pad 3 being over excavated to evaluate the refusal encountered
during vibro-pier installation. Debris such as bricks, wood, metal beams, corroded pipes and fly
wheel and leather products were noticed in the debris. After the obstructions were removed, the
areas were backfilled with the excavated soil up to five feet, then geo-fabric was placed over the
compacted fill and clean fill from the Carson Street side of the Site was used to bring the
remainder of the footage to grade. It was estimated that 380 tons of this soil were stockpiled on
Pad 1 with other soil cuttings. The soil stockpile on Pad 1 was transported to an off-site disposal
facility. The manifests are attached in Appendix 20.

The Brownfields Program was informed about the removal of the impacted soil, and about a
plan to place approximately 250 cubic yards of “clean” excavated soil (Stockpile 10) at a
location that would be beneath a ramp that would connect levels of the subsurface parking on
the Site. In the email dated May 12, 2014 (see Appendix 18), Brownfields personnel indicated
the developer may do the following with the approval of the NC Brownfields Program: 1) move
the Stockpile 10 soils as proposed and (2) does not need to add data regarding the Stockpile 10
soils to the Brownfields plat.

IMPORTED SOIL

In the email dated March 27, 2015, NCDEQ was provided a laboratory report of organic soil that
was to be imported to the Site to amend soil in the tree pits. Arsenic was detected at a
concentration exceeding the residential standard in the sample, however the concentration was
consistent with naturally-occurring background levels at the Site. A copy of the laboratory report
and the email are provided in Appendix 21.

RELIANCE

The use of and reliance on this report are strictly limited. This report is the intellectual property
of EFI, protected by copyright law and other laws, and has been prepared solely for the use and
benefit of USAA. Unless authorized in writing by EFI, reliance on or use (collectively, “Use”) of
this report by additional parties is strictly prohibited and shall be at the sole risk of the user,
without rights of recourse or recovery from or against EFI. Any such unauthorized user shall be

Charlotte Chemical 9 February 2, 2016
Charlotte, NC Project Number 94705-07722
responsible to protect, indemnify and hold EFI, USAA and their respective officers, employees,
vendors, successors and assigns harmless from any and all claims, damages, losses, liabilities,
expenses (including reasonable attorneys’ fees) and costs attributable to such Use. The
unauthorized use of this report shall constitute acceptance of and commitment to these
responsibilities, which shall be irrevocable and shall apply regardless of the cause of action or
legal theory pled or asserted. Additional legal penalties may apply.

SUMMARY

Underground storage tanks, a water tank, and soil that was impacted with petroleum
compounds and metals were discovered at the Site during redevelopment. The USTs, water
tank, and the impacted soil were excavated and transported to off-site facilities for disposal.
The sampling indicated that the impacted soil was successfully removed from the Site.

Sincerely,

EFI GLOBAL, INC.

John Burkart Mandeep Sandhu
Field Professional Director of Assessment Services, East Region
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D
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N
D

N
D

N
D

N
D

1
4
0
NE 430
te
r
t

b
u
t
y
l

b
e
n
z
e
n
e

N
A

N
A

N
D
ND

N
D

0
.
0
0
5
9

N
D

N
D

N
D
ND

N
D

N
D

N
D

N
D

1
6
0
0
1.7

2
0
0
0
0
2-
m
e
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e

N
A

N
A

2
.
1
8
24
.
3

N
D

N
D

N
D

N
D

N
D
ND

N
D

N
D

N
D

N
D
46 1.6 370
Flu
o
r
e
n
e
NA

N
A

N
D
1.1
9

N
D

0
.
4
0
7

N
D

N
D

N
D
ND

N
D

N
D

N
D

N
D

4
6
0
56

4
4
0
0
1-
M
e
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e

N
A

N
A

1
.
3
4
13
.
2

N
D

N
D

N
D

N
D

N
D
ND

N
D

N
D

N
D

N
D
16 0.055

5
3
Ph
e
n
a
n
t
h
r
e
n
e
NA

N
A

0
.
3
4
9
2,4
7

N
D

0
.
9
4
6

N
D

N
D

N
D
ND

N
D

N
D

N
D

N
D

N
E
68 NE
P-
I
s
o
p
r
o
p
y
t
o
l
u
e
n
e

N
A

N
A

N
D
ND

N
D

0
.
2
2
2

N
D

N
D

N
D
ND

N
D

N
D

N
D

N
D

N
E
NE NE
Ac
e
n
a
p
h
t
h
a
l
e
n
e
NA

N
A

N
D
0.
6
3
2

0
.
3
4
3

0
.
3
4
3

N
D

N
D

N
D
ND

N
D

N
D

N
D

N
D

6
8
0
8.4

6
,
6
6
0
An
t
h
r
a
c
e
n
e
NA

N
A

N
D
0.
4
0
3

N
D

N
D

N
D

N
D

N
D
ND

N
D

N
D

N
D

N
D

3
4
0
0

6
6
0

6
,
6
0
0
Flu
o
r
a
n
t
h
e
n
e
NA

N
A

N
D
ND

N
D

0
.
3
7
4

N
D

N
D

N
D
ND

N
D

N
D

N
D

N
D

4
6
0
330

4
4
0
0
Py
r
e
n
e
NA

N
A

N
D
ND

N
D

0
.
3
3
8

N
D

N
D

N
D
ND

N
D

N
D

N
D

N
D

3
4
0
220

3
4
0
0
se
c
-
b
u
t
y
l
b
e
n
z
e
n
e
NA

N
A

N
D
ND

0
.
2
0
4

0
.
2
0
4

N
D

N
D

N
D
ND

N
D

N
D

N
D

N
D

1
6
0
0

2
.
2
0

2
0
0
0
0
TP
H

D
R
O
26
7
0
29
.
3
16
3
63
3

6
7
.
7

2
4
1
0
ND
57
.
2
8.
2
43
.
2

2
6
3
ND

N
D

N
A

1
0
*
TP
H

G
R
O
10
7
ND
27
7
69
.
3
ND
42
.
9
ND
ND

N
D
ND

N
D

N
D

N
D

N
A

1
0
*
* P
e
t
r
o
l
e
u
m

A
c
t
i
o
n

L
e
v
e
l
Co
n
c
e
n
t
r
a
t
i
o
n
s

r
e
p
o
r
t
e
d

i
n

m
i
l
l
i
g
r
a
m
s

p
e
r

k
i
l
o
g
r
a
m

(
m
g
/
k
g
)
PS
R
G

-

P
r
e
l
i
m
i
n
a
r
y

S
o
i
l

R
e
m
e
d
i
a
t
i
o
n

G
o
a
l

(
I
n
a
c
t
i
v
e

H
a
z
a
r
d
o
u
s

S
i
t
e

B
r
a
n
c
h
)
ND

-

N
o
t

D
e
t
e
c
t
e
d
NA

-

N
o
t

A
n
a
l
y
z
e
d
NE

-

C
r
i
t
e
r
i
a

n
o
t

e
s
t
a
b
l
i
s
h
e
d
BO
L
D
c
o
n
c
e
n
t
r
a
t
i
o
n
s

e
x
c
e
e
d

t
h
e

G
r
o
u
n
d
w
a
t
e
r

P
r
o
t
e
c
t
i
o
n

L
e
v
e
l
s

o
r

S
o
i
l

t
o

G
r
o
u
n
d
w
a
t
e
r

L
e
v
e
l
s
TA
B
L
E

4
Su
m
m
a
r
y

o
f

S
o
i
l

A
n
a
l
y
t
i
c
a
l

R
e
s
u
l
t
s
US
T

5

20
1
3
-
2
0
1
4

S
a
m
p
l
i
n
g

E
v
e
n
t
So
u
t
h

B
o
u
l
e
v
a
r
d
,

N
o
r
t
h

C
a
r
o
l
i
n
a
Sa
m
p
l
e

I
D
US
T
-
5

S
-
1

U
S
T
-
5

S
-
2

U
S
T
-
5

S
1
A

S
i
d
e
w
a
l
l

N
o
r
t
h

S
i
d
e
w
a
l
l

S
o
u
t
h

S
i
d
e
w
a
l
l

E
a
s
t

S
i
d
e
w
a
l
l

W
e
s
t
NC
D
E
N
R

N
C
D
E
N
R

N
C
D
E
N
R

Sa
m
p
l
e

D
e
p
t
h
11
5
1
1
1
1
PS
R
G

P
S
R
G

P
S
R
G
Sa
m
p
l
e

D
a
t
e

1
2
/
1
9
/
1
3

1
2
/
1
9
/
1
3

1
/
1
2
/
1
4

1
/
2
1
/
1
4

1
/
2
1
/
1
4

1
/
2
1
/
1
4

1
/
2
1
/
1
4

R
e
s
i
d
e
n
t
i
a
l

G
W

P
r
o
t
e
c
t
i
o
n

I
n
d
u
s
t
r
i
a
l
Be
n
z
e
n
e
ND

N
D

N
D

N
D

N
D

N
D

N
D

1
.
1

0
.
0
0
7
3

5
.
4
n-
b
u
t
l
y
b
e
n
z
e
n
e
0.
2
1

N
D

N
D

N
D

N
D

N
D

N
D

1
1
0

2
.
4

1
1
0
Eth
y
l
b
e
n
z
e
n
e
ND

N
D

N
D

N
D

N
D

N
D

N
D

5
.
4

8
.
1

2
7
Na
p
h
t
h
a
l
e
n
e
7.
4
5
0.
9
0

N
D

N
D

N
D

N
D

N
D

3
.
6

1
.
6

3
7
0
n-
p
r
o
p
y
l
b
e
n
z
e
n
e

N
D

N
D

N
D

N
D

N
D

N
D

N
D

2
6
0

1
.
5

2
6
0
To
l
u
e
n
e

N
D

N
D

N
D

N
D

N
D

N
D

N
D

8
2
0

5
.
5

8
2
0
1,
2
,
4

t
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e

0
.
8
2

1
.
0
4

N
D

N
D

N
D

N
D

N
D

1
2

6
.
7

5
2
1,
3
,
5

t
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e

0
.
3
7
1

0
.
3
6
2

N
D

N
D

N
D

N
D

N
D

1
6
0

6
.
7

1
8
0
xy
l
e
n
e
s

N
D

0
.
8
3
2

N
D

N
D

N
D

N
D

N
D

1
3
0

5
.
8

2
6
0
m+
p

x
y
l
e
n
e
s

N
D

0
.
5
5
9

N
D

N
D

N
D

N
D

N
D

1
2
0

N
E

2
6
0
o-
x
y
l
e
n
e

N
D

0
.
2
7
2

N
D

N
D

N
D

N
D

N
D

1
4
0

N
E

4
3
0
te
r
t

b
u
t
y
l

b
e
n
z
e
n
e

N
D

N
D

N
D

N
D

N
D

N
D

N
D

1
6
0
0

1
.
7

2
0
0
0
0
2-
m
e
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e

3
1
.
7

4
.
1
5

N
D

N
D

N
D

N
D

N
D

4
6

1
.
6

3
7
0
Fl
u
o
r
e
n
e

3
.
5
2

0
.
3
6
8

N
D

N
D

N
D

N
D

N
D

4
6
0

5
6

4
4
0
0
1-
M
e
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e
20
.
7
2.
8

N
D

N
D

N
D

N
D

N
D

1
6

0
.
0
5
5

5
3
Ph
e
n
a
n
t
h
r
e
n
e

5
.
5
4

0
.
4
4
5

N
D

N
D

N
D

N
D

N
D

N
E

6
8

N
E
P-
I
s
o
p
r
o
p
y
t
o
l
u
e
n
e

N
D

0
.
2
5
1

N
D

N
D

N
D

N
D

N
D

N
E

N
E

N
E
Co
n
c
e
n
t
r
a
t
i
o
n
s

r
e
p
o
r
t
e
d

i
n

m
i
l
l
i
g
r
a
m
s

p
e
r

k
i
l
o
g
r
a
m

(
m
g
/
k
g
)
ND

-

N
o
t

D
e
t
e
c
t
e
d
PS
R
G

-

P
r
e
l
i
m
i
n
a
r
y

S
o
i
l

R
e
m
e
d
i
a
t
i
o
n

G
o
a
l

(
I
n
a
c
t
i
v
e

H
a
z
a
r
d
o
u
s

S
i
t
e

B
r
a
n
c
h
)
NE

-

C
r
i
t
e
r
i
a

n
o
t

e
s
t
a
b
l
i
s
h
e
d
BO
L
D
c
o
n
c
e
n
t
r
a
t
i
o
n
s

e
x
c
e
e
d

t
h
e

G
r
o
u
n
d
w
a
t
e
r

P
r
o
t
e
c
t
i
o
n

L
e
v
e
l
s

o
r

S
o
i
l

t
o

G
r
o
u
n
d
w
a
t
e
r

L
e
v
e
l
s
TA
B
L
E

5
Su
m
m
a
r
y

o
f

S
o
i
l

A
n
a
l
y
t
i
c
a
l

R
e
s
u
l
t
s
US
T

7

20
1
4

S
a
m
p
l
i
n
g

E
v
e
n
t
So
u
t
h

B
o
u
l
e
v
a
r
d
,

N
o
r
t
h

C
a
r
o
l
i
n
a
Sa
m
p
l
e

I
D
US
T
-
7

B
-
1
US
T
-
7

Sid
e
w
a
l
l
1
US
T
-
7

S
i
d
e
w
a
l
l

2
US
T
-
7

S
i
d
e
w
a
l
l

3
US
T
-
7

S
i
d
e
w
a
l
l

4
US
T
-
7

B
o
t
t
o
m

5
US
T
-
7

B
o
t
t
o
m

6
Si
d
w
e
a
l
l

1

U
S
T
-
7
1
A
Sid
e
w
a
l
l

4

U
S
T
-
7
4
A
US
T
-
7

B
o
t
t
o
m

1A
NC
D
E
N
R

N
C
D
E
N
R

N
C
D
E
N
R

Sa
m
p
l
e

D
e
p
t
h

1
5

1
2

1
2

1
3
.
0
0

1
2
.
0
0

1
5

1
5

1
2

1
2

1
6

P
S
R
G

P
S
R
G

P
S
R
G
Sa
m
p
l
e

D
a
t
e

2
/
1
8
/
1
4

2
/
1
8
/
1
4

2
/
1
8
/
1
4

4
1
6
8
8
.
0
0

4
1
6
8
8
.
0
0

2
/
1
8
/
1
4

2
/
1
8
/
1
4

2
/
2
2
/
1
4

2
/
2
2
/
1
4

2
/
2
2
/
1
4

R
e
s
i
d
e
n
t
i
a
l

G
W

P
r
o
t
e
c
t
i
o
n

I
n
d
u
s
t
r
i
a
l
Be
n
z
e
n
e
ND

N
D

N
D

N
D

N
D

N
D

N
D

N
D

N
D

N
D

1
.
1

0
.
0
0
7
3

5
.
4
n-
b
u
t
l
y
b
e
n
z
e
n
e
10
.
4
0

8
.
2
8

N
D

N
D

N
D

N
D

N
D

N
D

N
D

N
D

1
1
0

2
.
4

1
1
0
Et
h
y
l
b
e
n
z
e
n
e
ND

N
D

N
D

N
D

N
D

N
D

N
D

N
D

N
D

N
D

5
.
4

8
.
1

2
7
Na
p
h
t
h
a
l
e
n
e
7.
4
5

2
5
.
5
0
ND

2
.
2
6
6.
9
3
ND

N
D

0
.
0
2

N
D

N
D

3
.
6

1
.
6

3
7
0
n-
p
r
o
p
y
l
b
e
n
z
e
n
e

3
.
1
8

2
7
,
2

N
D

N
D

N
D

N
D

N
D

N
D

N
D

N
D

2
6
0

1
.
5

2
6
0
To
l
u
e
n
e

N
D

N
D

N
D

N
D

N
D

N
D

N
D

N
D

N
D

N
D

8
2
0

5
.
5

8
2
0
1,
2
,
4

t
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e

0
.
8
2

2
8
.
2

N
D

0
.
0
1

N
D

N
D

N
D

N
D

N
D

N
D

1
2

6
.
7

5
2
1,
3
,
5

t
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e

9
.
8
1

8
.
4
7

N
D

N
D

N
D

N
D

N
D

0
.
0
2

N
D

N
D

1
6
0

6
.
7

1
8
0
xy
l
e
n
e
s

1
2
.
5
6

7
.
6
7

N
D

N
D

N
D

N
D

N
D

0
.
0
1

N
D

N
D

1
3
0

5
.
8

2
6
0
m+
p

x
y
l
e
n
e
s

9
.
6
7

7
.
6
7

N
D

N
D

N
D

N
D

N
D

N
D

N
D

N
D

1
2
0

N
E

2
6
0
o-
x
y
l
e
n
e

2
.
8
9

N
D

N
D

N
D

N
D

N
D

N
D

N
D

N
D

N
D

1
4
0

N
E

4
3
0
te
r
t

b
u
t
y
l

b
e
n
z
e
n
e

N
D

N
D

N
D

N
D

N
D

N
D

N
D

N
D

N
D

N
D

1
6
0
0

1
.
7

2
0
0
0
0
2-
m
e
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e

3
1
4

4
.
1
5

N
D

2
0
.
2
0
77
.
4
0
ND

N
D

N
D

N
D

N
D

4
6

1
.
6

3
7
0
Flu
o
r
e
n
e

3
.
5
2

0
.
3
6
8

N
D

1
.
1
3

3
.
3
4

N
D

N
D

N
D

N
D

N
D

4
6
0

5
6

4
4
0
0
1-
M
e
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e
16
0

1
3
6
ND

1
1
.
7
0
43
.
6
0
ND

N
D

N
D

N
D

N
D

1
6

0
.
0
5
5

5
3
Ph
e
n
a
n
t
h
r
e
n
e

5
.
5
4

3
0
.
6

N
D

2
.
5
1

9
.
0
1

0
.
5
3

N
D

N
D

N
D

N
D

N
E

6
8

N
E
P-
I
s
o
p
r
o
p
y
t
o
l
u
e
n
e

N
D

4
.
4
7

N
D

N
D

N
D

N
D

N
D

N
D

N
D

N
D

N
E

N
E

N
E
Ac
e
t
o
n
e

N
D

N
D

N
D

N
D

N
D

N
D

N
D

0
.
2
1

0
.
1
4

0
.
1
8

1
2
0
0
0

2
4
.
0
0

1
0
0
0
0
0
Ac
e
n
a
p
h
t
h
a
l
e
n
e

N
D

N
D

N
D

N
D

2
.
4
0

N
D

N
D

N
D

N
D

N
D

N
A

2
1
.
0
0

N
A
An
t
h
a
c
e
n
e

N
D

N
D

N
D

N
D

0
.
9
9

N
D

N
D

N
D

N
D

N
D

3
4
0
0

6
6
0
.
0
0

3
4
0
0
0
Co
n
c
e
n
t
r
a
t
i
o
n
s

r
e
p
o
r
t
e
d

i
n

m
i
l
l
i
g
r
a
m
s

p
e
r

k
i
l
o
g
r
a
m

(
m
g
/
k
g
)
ND

-

N
o
t

D
e
t
e
c
t
e
d
PS
R
G

-

P
r
e
l
i
m
i
n
a
r
y

S
o
i
l

R
e
m
e
d
i
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t
i
o
n

G
o
a
l

(
I
n
a
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H
a
z
a
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S
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e

B
r
a
n
c
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)
NE

-

C
r
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r
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a

n
o
t

e
s
t
a
b
l
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d
BO
L
D
c
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r
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s

e
x
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d

t
h
e

G
r
o
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n
d
w
a
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r

P
r
o
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c
t
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n

L
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v
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s

o
r

S
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t
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G
r
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w
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L
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B
L
E

6
Su
m
m
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y

o
f

S
o
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l

A
n
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R
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s
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s
Pa
d

1

S
o
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C
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P
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a
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V
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-
P
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r

1
5
9

S
o
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20
1
4

S
a
m
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g

E
v
e
n
t
So
u
t
h

B
o
u
l
e
v
a
r
d
,

N
o
r
t
h

C
a
r
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l
i
n
a
a
Sa
m
p
l
e

I
D
So
i
l

C
u
t

P
a
d

1

Sto
c
k

1
So
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l

C
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t

P
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d

1

Sto
c
k

2
So
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l

C
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t

P
a
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1

St
o
c
k

3
So
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l

C
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t

P
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1
S
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c
k

4
So
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l

C
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P
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d

1
S
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c
k

5
So
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l

C
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t

P
a
d

1
S
t
o
c
k
6

So
i
l

C
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t

P
a
d

1

St
o
c
k

7

S
o
i
l

C
u
t

1
5
9
So
i
l

C
u
t

1
5
9

Du
p
l
i
c
a
t
e
NC
D
E
N
R

N
C
D
E
N
R

N
C
D
E
N
R

Sa
m
p
l
e

D
e
p
t
h
Co
m
p
o
s
i
t
e

C
o
m
p
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s
i
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e

C
o
m
p
o
s
i
t
e

C
o
m
p
o
s
i
t
e

C
o
m
p
o
s
i
t
e

C
o
m
p
o
s
i
t
e

C
o
m
p
o
s
i
t
e

G
r
a
b
Gr
a
b

P
S
R
G

P
S
R
G

P
S
R
G
Sa
m
p
l
e

D
a
t
e
2/
2
0
/
1
4

2
/
2
0
/
1
4

2
/
2
0
/
1
4

2
/
2
0
/
1
4

2
/
2
0
/
1
4

2
/
2
0
/
1
4

2
/
2
0
/
1
4

2
/
2
2
/
1
4
2/2
2
/
1
4

R
e
s
i
d
e
n
t
i
a
l

G
W

P
r
o
t
e
c
t
i
o
n

I
n
d
u
s
t
r
i
a
l
Be
n
z
e
n
e
ND

N
D

N
D

N
D

N
D

N
D
ND

N
D
8.
1
6
1.
1

0
.
0
0
7
3

5
.
4
n-
b
u
t
l
y
b
e
n
z
e
n
e
ND

N
D

N
D

N
D

N
D

N
D
ND
3.
4
4

1
1
.
1
11
0

2
.
4

1
1
0
se
c
-
b
u
t
y
l
b
e
n
z
e
n
e
ND

N
D

N
D

N
D

N
D

N
D
ND
ND

1
0
.
5
15
0

2
.
2

1
5
0
Eth
y
l
b
e
n
z
e
n
e
ND

N
D

N
D

N
D

N
D

N
D
ND
8.
9
9

6
9
.
0
5.
4

8
.
1

2
7
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
ND

N
D

N
D

N
D

N
D

N
D
ND
3.
4
4

2
3
.
2
NE

N
E

N
E
Na
p
h
t
h
a
l
e
n
e
ND
ND

N
D

N
D

N
D

N
D
ND
48
.
7

8
7
.
8
3.
6

1
.
6

3
7
0
n-
p
r
o
p
y
l
b
e
n
z
e
n
e
ND

N
D

N
D

N
D

N
D

N
D
ND
4.
2
4

2
7
.
0
26
0

1
.
5

2
6
0
To
l
u
e
n
e
ND

N
D

N
D

N
D

N
D

N
D
ND
13
.
6

1
4
1
.
0
82
0

5
.
5

8
2
0
1,
2
,
4

t
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
ND

N
D

N
D

N
D

N
D

N
D
ND
22
.
3

1
7
1
.
0
12

6
.
7

5
2
1,
3
,
5

t
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
ND

N
D

N
D

N
D

N
D

N
D
ND
8.
8

6
1
.
6
16
0

6
.
7

1
8
0
xy
l
e
n
e
s
ND

N
D

N
D

N
D

N
D

N
D
ND
38
.
9

3
0
8
.
0
13
0

5
.
8

2
6
0
m+
p

x
y
l
e
n
e
s

ND

N
D

N
D

N
D

N
D

N
D
ND

2
8
.
1

2
2
0
.
0

1
2
0

N
E

2
6
0
o-
x
y
l
e
n
e
ND

N
D

N
D

N
D

N
D

N
D
ND

1
0
.
8

8
7
.
6

1
4
0

N
E

4
3
0
te
r
t

b
u
t
y
l

b
e
n
z
e
n
e
ND

N
D

N
D

N
D

N
D

N
D
ND

N
D

N
D

1
6
0
0

1
.
7

2
0
0
0
0
2-
m
e
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e
ND

N
D

N
D

N
D

N
D

N
D
ND

N
D

N
D

4
6

1
.
6

3
7
0
Fl
u
o
r
e
n
e
ND

N
D

N
D

N
D

N
D

N
D
ND

N
D

N
D

4
6
0

5
6

4
4
0
0
1-
M
e
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e
ND

N
D

N
D

N
D

N
D

N
D
ND

N
D

N
D

1
6

0
.
0
5
5

5
3
Ph
e
n
a
n
t
h
r
e
n
e
ND

N
D

N
D

N
D

N
D

N
D
ND

N
D

N
D

N
E

6
8

N
E
P-
I
s
o
p
r
o
p
y
t
o
l
u
e
n
e
ND
ND
ND
ND

N
D

N
D
ND
3.
2
8
22
.
0
NE
NE NE
Ac
e
n
a
p
h
t
h
a
l
e
n
e
ND
ND
ND
ND

N
D

N
D
ND
ND
ND
68
0
8.4 6,660
An
t
h
r
a
c
e
n
e
ND
ND
ND
ND

N
D

N
D
ND
ND
ND
34
0
0
660 6,600
Fl
u
o
r
a
n
t
h
e
n
e
ND
ND
ND
ND

N
D

N
D
ND
ND
ND
46
0
330 4400
Py
r
e
n
e
ND
ND
ND
ND

N
D

N
D
ND
ND
ND
34
0
220 3400
se
c
-
b
u
t
y
l
b
e
n
z
e
n
e
ND
ND
ND
ND

N
D

N
D
ND
ND
10
.
5
16
0
0
2.20 20000
TP
H

D
R
O
7.
6
16
7
ND
ND
ND
7.
2
ND
47
3
0
27
5
0
10
*
TP
H

G
R
O
ND
ND
ND
ND

N
D

N
D
ND
19
1
0
34
.
7
10
*
Ac
e
t
o
n
e
ND

0
.
2
0
9

N
D
ND

N
D

0
.
1
0
9
ND
ND
ND
12
0
0
0
24 100000
Ar
s
e
n
i
c
ND
ND
ND
ND

N
D

N
D
ND
ND
0.
9
6
0.6
1
5.80 2.40
Ba
r
i
u
m
88
95
.
5

2
0
4

*
*

7
2
.
2
*
*

9
4
.
1

1
4
2
*
*
47
.
1
6.
7
12
.
1
30
0
0
580 44000
Ca
d
m
i
u
m
0.
1
1
ND
0.
1
7

0
.
1
7

N
D

0
.
1
2
ND
ND
ND
14
400 63
Ch
r
o
m
i
u
m
30
.
5
17
21
.
4

1
3
.
3

5
27
.
2
18
.
7
1.
4
2.9
24
0
0
360000 100000
Le
a
d
15
.
5

1
6
.
7

2
5
.
9
*
*

5
.
4
*
*

4
.
3

8
.
1
4.8
10
.
8
25
.
1
40
0
270 800
Se
l
e
n
i
u
m
ND
ND
ND
ND

N
D

N
D
ND
ND
ND
78
2.1 1000
Sil
v
e
r
ND
ND
ND
ND

N
D

N
D
ND
ND
ND
78
NE 1000
Me
c
u
r
y
0.0
4
8

0
.
0
5
2

0
.
1
6

0
.
0
2
3

0
.
0
0
9

0
.
0
2
8
0.0
0
7
7

N
D
0.
0
1
9
2.
0
1.0 3.1
**

I
n
d
i
c
a
t
e
s

s
a
m
p
l
e

w
a
s

a
n
a
l
y
z
e
d

f
o
r

T
C
L
P

m
e
t
a
l
s

a
n
d

r
e
s
u
l
t
s

i
n
d
i
c
a
t
e
d

i
t

l
e
a
c
h
e
d

b
u
t

b
e
l
o
w

s
t
a
n
d
a
r
d
s

*
P
e
t
r
o
l
e
u
m

A
c
t
i
o
n

L
e
v
e
l
Co
n
c
e
n
t
r
a
t
i
o
n
s

r
e
p
o
r
t
e
d

i
n

m
i
l
l
i
g
r
a
m
s

p
e
r

k
i
l
o
g
r
a
m

(
m
g
/
k
g
)
ND

-

N
o
t

D
e
t
e
c
t
e
d
PS
R
G

-

P
r
e
l
i
m
i
n
a
r
y

S
o
i
l

R
e
m
e
d
i
a
t
i
o
n

G
o
a
l

(
I
n
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TABLE 7
Summary of Soil Analytical Results
Vibro-Pier and Pad 3 Soil Cutting Pile
2014 Sampling Event
South Boulevard, North Carolina
Sample ID
Stock Soil Pad
3 #1
Stock Soil Pad
3 #2
Stock Soil
Pad 3 #3
Stock Soil
Pad 3 #4
Stock Soil
Pat 3 #5
Stock Soil
Pad 3 #6 NCDENR NCDENR NCDENR
Sample Depth Composite Composite Composite Composite Composite Composite PSRG PSRG PSRG
Sample Date 3/5/14 3/5/14 3/5/14 3/5/14 3/5/14 3/5/14 Residential GW Protection Industrial
Benzene ND ND ND ND ND ND 1.1 0.0073 5.4
n-butlybenzene ND ND ND ND ND ND 110 2.4 110
sec-butylbenzene ND ND ND ND ND ND 150 2.2 150
Ethylbenzene ND ND ND ND ND ND 5.4 8.1 27
Isopropylbenzene ND ND ND ND ND ND NE NE NE
Naphthalene ND ND ND ND ND ND 3.6 1.6 370
n-propylbenzene ND ND ND ND ND ND 260 1.5 260
Toluene ND ND ND ND ND ND 820 5.5 820
1,2,4 trimethylbenzene ND ND ND ND 0.0049 ND 12 6.7 52
1,3,5 trimethylbenzene ND ND ND ND ND ND 160 6.7 180
xylenes ND ND ND ND ND ND 130 5.8 260
m+p xylenes ND ND ND ND ND ND 120 NE 260
o-xylene ND ND ND ND ND ND 140 NE 430
tert butyl benzene ND ND ND ND ND ND 1600 1.7 20000
2-methylnaphthalene ND ND ND ND ND ND 46 1.6 370
Fluorene ND ND ND 5.31 ND ND 460 56 4400
1-Methylnaphthalene ND ND ND ND ND ND 16 0.055 53
Phenanthrene ND ND 3.68 24.7 ND ND NE 68 NE
P-Isopropytoluene ND ND ND ND 0.0119 ND NE NE NE
Acenaphthalene ND ND ND ND ND ND 680 8.4 6,660
Anthracene ND ND ND 5.2 ND ND 3400 660 6,600
Benzo(a)anthracene ND ND ND 6.66 ND ND NE NE NE
Benzo(a)pyrene ND ND ND 5.55 ND ND NE NE NE
Benzo(b)fluoranthene ND ND ND 5.34 ND ND NE NE NE
Benzo(g,h,i)perylene ND ND ND 3.44 ND ND NE NE NE
Benzo(k)fluoranthene ND ND ND 4.66 ND ND NE NE NE
Chrysene ND ND ND 6.78 ND ND NE NE NE
Fluoranthene ND ND 5.12 25.3 4.07 ND 460 330 4400
Pyrene ND ND ND 11.9 ND ND 340 220 3400
sec-butylbenzene ND ND ND ND ND ND 1600 2.20 20000
TPH DRO 110 179 110 165 267 140 10*
TPH GRO ND ND ND ND ND ND 10*
Acetone 92.9 ND ND ND 98.8 ND 12000 24 100000
Arsenic 5.9 11.7 5.3 4.1 6.5 1.5 0.61 5.80 2.40
Barium 114 147 121 115 134 82.8 3000 580 44000
Cadmium 0.64 1.0 0.5 0.47 0.68 0.21 14 400 63
Chromium 36.8 51 37.4 28.2 38.5 26.1 2400 360000 100000
Lead 230 225 140 128 218 75 400 270 800
Selenium ND ND ND ND ND ND 78 2.1 1000
Silver ND 0.35 ND ND ND ND 78 NE 1000
Mecury 17.0 0.052 0.16 13.3 27.6 24.8 2.0 1.0 3.1
* Petroleum Action Level
Concentrations reported in milligrams per kilogram (mg/kg)
ND - Not Detected
PSRG - Preliminary Soil Remediation Goal (Inactive Hazardous Site Branch)
NE - Criteria not established
BOLD concentrations exceed the Groundwater Protection Levels or Soil to Groundwater Levels

APPENDIX 1

TOPOGRAPHIC MAP, TANK LOCATION MAPS, AND BORING
LOCATION MAPS

Site Topographic Map
Former Charlotte Chemical
1100 South Boulevard
Charlotte, North Carolina

APPENDIX 2

SOIL MANAGEMENT PLAN

APPENDIX 3

HEALTH & SAFETY PLAN

APPENDIX 4

LABORATORY ANALYTICAL REPORT
EFI-1 THROUGH EFI-9

APPENDIX 5

UST MANAGEMENT LETTER AND CORRESPONDENCE

CH-3199293 v 1
9307 Monroe Road
Suite M
Charlotte, NC 28270
Tel: [phone]
TF: 866.390.3274
Fax: [phone]
www.efiglobal.com

Project No. 94705- 05034
January 13, 2014

Ms, Carolyn Minnich Brownfields Project Manager
NCDENR-DWM
217 W Jones Street Raleigh, NC 27603

RE: UST SOIL MANAGEMENT LETTER
CHARLOTTE CHEMICAL LABORATORY SITE
1100 SOUTH BOULEVARD
CHARLOTTE, MECKLENBURG COUNTY
BROWNFIELDS PROJECT NUMBER 11045-07-060
Dear Ms. Minnich:

EFI Global (EFI) is presenting this letter concerning soil excavation and disposal from UST Area
1 at the former drum oil house and UST-2, UST-3 and UST-4 from the former gasoline service
station along South Boulevard.

PROJECT INFORMATION

EFI understands a storm water vault will be installed on the property; a portion of the vault will
be installed over the location of the former drum oil house UST-1. The vault will be concrete
bottom, side walls and top and connected to a 24 inch storm line. EFI understands the vault
bottom is approximately 19.5 feet below grade level and 72 feet long by 30 feet wide. EFI has
proposed to over excavate the bottom of the UST excavation area by three feet in order to
create a compacted buffer between the vault bottom and the impacted soil. In addition, the
buffer will assist to control exposure to the construction workers. The impacted soil will be
disposed at a secure landfill. Currently, cost and paperwork for disposal are being worked out
by all parties involved. EFI will provide a letter following the excavation and removal of the
impacted soil.

As the developer’s counsel, David Franchina, described to the Brownfields Program in a
November 8, 2013 email (copy enclosed), UST-1 was buried beneath 12 feet of compacted soil.
Soils that were removed from the UST-1 excavation during tank removal have been removed

-2-

from the property and disposed at a licensed off-site facility. Documentation of proper disposal
of these soils will be submitted to the Brownfields Program under separate cover.

Per the request of the Brownfields Program, sampling has been performed at UST-1 to
establish the conditions of the excavation bottom and sidewalls using EPA Methods 8260 and
8270. Samples were taken by EFI at locations that correspond with the proposed bottom of the
excavation as well as the anticipated sidewalls (the developer might excavate beyond these
points if necessary for geotechnical purposes in connection with construction). These results
are summarized in attached Table; laboratory data is enclosed as well.

Only one exceedence of either residential or industrial PSRGs for contaminants analyzed using
EPA Method 8260 and 8270 was detected. Naphthalene was detected at 5.32 mg/kg in bottom
sample S-1, which exceeds the residential PSRG of 3.6 mg/kg. The concentration detected
does not exceed the industrial PSRG. All soils above the proposed bottom of the excavation
and within the sidewalls will be disposed at an off-site secure landfill. Documentation of proper
disposal of these soils will be submitted to the Brownfields Program under separate cover. The
general contractor is on a critical path where the soil from the storm water vault must begin to
be excavated as soon as possible to begin construction of the vault. All parties involved would
appreciate confirmation from Brownfields that it is acceptable to begin construction on the storm
water vault in the vicinity of UST-1 (the developer is likely to begin work on the remainder of the
vault pursuant to the Soil Management Plan for the property in the coming days).

A second UST, followed by a third and fourth UST was discovered at the property. They were
discovered in the vicinity of the gasoline filling station that was present on the property along
South Blvd (see enclosed map). The USTs were all in the same grave. This this portion of the
property was a gasoline filling station from the 1940s through the 1960s. In the 1970s a new
slab was installed over the old one, and the new slab served as the parking lot for Simpson's
Lighting, which never used the USTs.

Thus, the UST is likely to have been last used in the 1960s, so the developer is neither the
owner nor the operator of the UST, and there is no known responsible party for the UST.

On December 9, EFI removed the remaining liquids from the USTs, excavated around the
USTs, removed the USTs from the ground, and disposed of the USTs off site. It was
determined that the USTs had been closed in-place by a slurry sand mixture. The USTs were
transported by GARCO to their Asheboro facility for proper disposal of the sand and metal.

-3-

GARCO will be providing a certificate of disposal soon. Documentation of proper disposal will
be submitted to the Brownfields Program under separate cover.

The excavated overburden was stockpiled and sampled as labeled Bottom EX which is the
grade level of the sub-base for the parking podium. Per Carolyn Minnich’s December 17,
2013 email to David Franchina (copy enclosed), these soils can be placed back into the tank
grave as the soil test results indicate non-detect in the upper soil removed. No bottom soils
were removed to excavate the tanks from the ground.

This portion of the property will lie beneath the building's podium parking structure. The
samples DENR requested for the first tank removed from the property (8260/8270 in the base
of the excavation and the overburden). These samples are summarized in attached tables.
Samples that are representative of sidewall conditions will be collected in the next few days.
The results will be provided to Brownfields so it review same and approve commencement of
construction in this portion of the property.

Sample results for the bottoms of UST-2, UST-3 and UST-4 were received on evening
December 12, 2013. No exceedances of residential or industrial PSRGs for contaminants
analyzed using EPA Method 8260 and 8270 were detected, however, UST-2 Bottom S-1 was
determined by Pace Analytical to have an exceedence of a soil-to-groundwater value for
benzene (.724 mg/kg vs. 0.01 mg/kg) Clean fill will be placed over the excavation as indicated
by sample UST Bottom Elevation (EX) which indicated no detected petroleum constituents in
the volatile organic range and the polynuclear aromatic hydrocarbon range by EPA Methods
8260 and 8270.

Please see the attached Table for a summary of the results of UST 2, 3, and 4.

Please review the attached data and if you have any questions please call EFI representative
John Burkart at 704-241-3302.

Sincerely,

EFI Global, Inc.

-4-

John Burkart Robert Hird , PG, C.P.G.
Environmental Manager Director of Assessment Services

CORRESPONDENCE

1905 Certified Sanborn Map
A3
B
7
-
4
C
1
3
-
8
E
7
9
Order Date:EDR Inquiry:
Client:
Site Name:
Address:
City, ST, ZIP:
Certification #
Copyright:1905
6/5/2013 4:16:59 PM3627597.3
EFI- Eng. & Fire Investigations
Simpsons Lighting
1112 & 1200 South Boulevard
Charlotte NC 28203
A3B7-4C13-8E79
This Certified Sanborn Map combines the following sheets.Outlined areas indicate map sheets within the collection.
Volume 1, Sheet 24
Volume 1, Sheet 25
Volume 1, Sheet 26
Volume 1, Sheet 27
0 Feet 150 300 600
3627597 - 3 page 11
INQUIRY #:
YEAR:
3627597.5
1983
= 500'

APPENDIX 6

DISPOSAL MANIFESTS AND LABORATORY ANALYTICAL
REPORT
UST-1

APPENDIX 7

LABORATORY ANALYTICAL REPORT
TEST PIT

APPENDIX 8

UST-1 PHOTOGRAPHS

APPENDIX 9

SOIL DISPOSAL MANIFESTS
UST-1

APPENDIX 10

STORMWATER VAULT PHOTOGRAPHS

APPENDIX 11

CERTIFICATES OF DISPOSAL
UST-2, UST-3, AND UST-4

APPENDIX 12

LABORATORY ANALYTICAL REPORT
UST-2, UST-3, AND UST-4

APPENDIX 13

UST-2, UST-3, AND UST-4 PHOTOGRAPHS

APPENDIX 14

WATER TANK 6 PHOTOGRAPHS

APPENDIX 15

WATER TANK 6 AND UST-5 DISPOSAL CERTIFICATES

APPENDIX 16

LABORATORY ANAYTICAL REPORT
WATER TANK

APPENDIX 17

UST-5 AND UST-7 REPORT
DISPOSAL MANIFESTS (UST-7 AND SOIL CUTTINGS)
LABORATORY ANAYTICAL REPORT AND EMAIL

9307 Monroe Road
Suite M
Charlotte, NC 28270
Tel: [phone]
TF: 866.390.3274
Fax: [phone]
www.efiglobal.com

Project No. 94705- 05034
March 5, 2014

Ms, Carolyn Minnich Brownfields Project Manager
NCDENR-DWM
217 W Jones Street Raleigh, NC 27603

RE: UST 5 AND UST-7
CHARLOTTE CHEMICAL LABORATORY SITE
1100 SOUTH BOULEVARD
CHARLOTTE, MECKLENBURG COUNTY
BROWNFIELDS PROJECT NUMBER 11045-07-060

Dear Ms. Minnich:
EFI Global (EFI) is presenting sampling results concerning two recently discovered
Underground Storage Tanks: UST-5 at a location just off former Palmer Street and UST-7
under the footer of the old Simpson Light building. (An additional suspected UST, which was
temporarily called UST-6, was also discovered on the referenced site. Further investigation by
EFI revealed it was not a UST, so we will not be reporting on it.) The attached Figure 1
provides the location of the discovered UST-5 and UST-7.

UST–5 AND UST-7 INFORMATION

UST-5 was discovered during routine grading at the site. UST-7 was discovered during vibro-
pier installation. The developer was not aware of the existence of either UST prior to discovery.

Based on historical research, it appears that UST-5 was last used sometime before 1983. See
attached Figures 2 through 6, which are Sanborn Maps from 1953 and 1969 and aerial
photographs from 1968, 1973, and 1983. The 1953 and 1969 Sanborn Maps (Figures 2 and 3)
show a large building in the immediate vicinity of UST -5. The maps contain an "S" denoting a
store. Aerial photographs from 1968 (Figure 4) and 1973 (Figure 5) show this building, but a
1983 aerial photograph (Figure 6) reveals that the structure has been demolished. Thus, the
tank was last used in 1983 at the latest.

Based on historical research, it appears that UST-7 was installed before the former Simpson's
Lighting was built. During the excavation activities in which UST-7 was discovered, the tank was

-2-

observed to be under the footer of the old Simpson’s Lighting Building. Terracotta sewer lines
traversed the top of the UST.UST-7 was apparently never used by Simpson’s Lighting, as no
lines were observed running from the UST toward the building. Thus, UST-7 must last have
been used sometime before the 1970s, when Simpson's was built.

Since the developer was not aware of either UST prior to their discovery, it could not have
operated either tank. Further, since each tank was last operated in 1983 or earlier, the
developer is not the owner of either tank (the owner would be the person who owned the tanks
immediately before the discontinuation of their use). Thus, UST-5 and UST-7 are orphan tanks
with no responsible party, and the developer bears no regulatory responsibility for them.
However, the developer does plan to address this tank in accordance with the requirements of
the Brownfields Program.

Both tanks were empty upon discovery. UST-5 was approximately 10 feet long by 3 feet in
diameter. UST-7 was approximately 20 feet long by 5 feet in diameter. It appears both USTs
have been used as fuel oil tanks to support on-site heating. Photographic documentation is
provided in the attachments. EFI has also attached data confirming that the bottom of the
excavation and the overburden were sampled using EPA Methods 8260 and 8270. Table 1
provides UST-5 data and UST-7 data are provided in Table 2. Minor impact was detected in
one or more of the bottom sample and sidewall samples where contaminates were above the
residential standards established for this project. EFI returned to each UST site to obtain
additional sidewall and bottom samples which are representative of the anticipated boundaries
of the UST excavation . The results of the second round of sampling indicated no impact above
residential standards. . Please see the attached figure and tables that depict the location and
summarizes the lab results. The USTs were hauled by Garco which has provided a disposal
certificate. Impacted soils from the USTs have been removed from the site and disposed in
licensed landfills. EFI will present the disposal certificates in a final report. The UST excavations
have been refilled, and EFI believes both areas are now closed.

Thus, since the bottom and sidewalls of UST-5 and UST-7 meet residential standards, we
believe that development can proceed in this area of the Brownfields Property. We also believe
that no data regarding UST-5 and UST-7 needs to be added to the Brownfields Plat. Please
confirm this at your first convenience so that development can proceed in this area.

If you have any questions please call EFI representative John Burkart at 704-241-3302.

-3-

Sincerely,

EFI Global, Inc.

John Burkart Robert Hird , PG, C.P.G.
Environmental Manager Director of Assessment Services

TABLE 1
Summary of Soil Analytical Results
UST 5
2013-2014 Sampling Event
South Bolevard, North Carolina
Sample ID UST-5 S-1 UST-5 S-2 UST-5 S1A Sidewall North Sidewall South Sidewall East Sidewall West NCDENR NCDENR NCDENR
Sample Depth 1 1 5 1 1 1 1 PSRG PSRG PSRG
Sample Date 12/19/13 12/19/13 1/12/14 1/21/14 1/21/14 1/21/14 1/21/14 Residential GW Protection Industrial
Benzene ND ND ND ND ND ND ND 1.1 0.0073 5.4
n-butlybenzene 0.21 ND ND ND ND ND ND 110 2.4 110
Ethylbenzene ND ND ND ND ND ND ND 5.4 8.1 27
Naphthalene 7.45 0.90 ND ND ND ND ND 3.6 1.6 370
n-propylbenzene ND ND ND ND ND ND ND 260 1.5 260
Toluene ND ND ND ND ND ND ND 820 5.5 820
1,2,4 trimethylbenzene 0.82 1.04 ND ND ND ND ND 12 6.7 52
1,3,5 trimethylbenzene 0.371 0.362 ND ND ND ND ND 160 6.7 180
xylenes ND 0.832 ND ND ND ND ND 130 5.8 260
m+p xylenes ND 0.559 ND ND ND ND ND 120 NE 260
o-xylene ND 0.272 ND ND ND ND ND 140 NE 430
tert butyl benzene ND ND ND ND ND ND ND 1600 1.7 20000
2-methylnaphthalene 31.7 4.15 ND ND ND ND ND 46 1.6 370
Fluorene 3.52 0.368 ND ND ND ND ND 460 56 4400
1-Methylnaphthalene 20.7 2.8 ND ND ND ND ND 16 0.055 53
Phenanthrene 5.54 0.445 ND ND ND ND ND NE 68 NE
P-Isopropytoluene ND 0.251 ND ND ND ND ND NE NE NE
Concentrations reported in milligrams per kilogram (mg/kg)
ND - Not Detected
PSRG - Preliminary Soil Remediation Goal (Inactive Hazardous Site Branch)
NE - Criteria not established
BOLD concentrations exceed the Groundwater Protection Levels or Soil to Groundwater Levels
TABLE 2
Summary of Soil Analytical Results
UST 7
2014 Sampling Event
South Bolevard, North Carolina
Sample ID UST-7 B-1
UST-7
Sidewall1
UST-7
Sidewall 2
UST-7
Sidewall 3
UST-7
Sidewall 4
UST-7 Bottom
5
UST-7 Bottom
6
Sidweall 1
UST-7 1A
Sidewall 4
UST-7 4A
UST-7 Bottom
1A NCDENR NCDENR NCDENR
Sample Depth 15 12 12 13.00 12.00 15 15 12 12 16 PSRG PSRG PSRG
Sample Date 2/18/14 2/18/14 2/18/14 41688.00 41688.00 2/18/14 2/18/14 2/22/14 2/22/14 2/22/14 Residential GW Protection Industrial
Benzene ND ND ND ND ND ND ND ND ND ND 1.1 0.0073 5.4
n-butlybenzene 10.40 8.28 ND ND ND ND ND ND ND ND 110 2.4 110
Ethylbenzene ND ND ND ND ND ND ND ND ND ND 5.4 8.1 27
Naphthalene 7.45 25.50 ND 2.26 6.93 ND ND 0.02 ND ND 3.6 1.6 370
n-propylbenzene 3.18 27,2 ND ND ND ND ND ND ND ND 260 1.5 260
Toluene ND ND ND ND ND ND ND ND ND ND 820 5.5 820
1,2,4 trimethylbenzene 0.82 28.2 ND 0.01 ND ND ND ND ND ND 12 6.7 52
1,3,5 trimethylbenzene 9.81 8.47 ND ND ND ND ND 0.02 ND ND 160 6.7 180
xylenes 12.56 7.67 ND ND ND ND ND 0.01 ND ND 130 5.8 260
m+p xylenes 9.67 7.67 ND ND ND ND ND ND ND ND 120 NE 260
o-xylene 2.89 ND ND ND ND ND ND ND ND ND 140 NE 430
tert butyl benzene ND ND ND ND ND ND ND ND ND ND 1600 1.7 20000
2-methylnaphthalene 314 4.15 ND 20.20 77.40 ND ND ND ND ND 46 1.6 370
Fluorene 3.52 0.368 ND 1.13 3.34 ND ND ND ND ND 460 56 4400
1-Methylnaphthalene 160 136 ND 11.70 43.60 ND ND ND ND ND 16 0.055 53
Phenanthrene 5.54 30.6 ND 2.51 9.01 0.53 ND ND ND ND NE 68 NE
P-Isopropytoluene ND 4.47 ND ND ND ND ND ND ND ND NE NE NE
Acetone ND ND ND ND ND ND ND 0.21 0.14 0.18 12000 24.00 100000
Acenaphthalene ND ND ND ND 2.40 ND ND ND ND ND NA 21.00 NA
Anthacene ND ND ND ND 0.99 ND ND ND ND ND 3400 660.00 34000
Concentrations reported in milligrams per kilogram (mg/kg)
ND - Not Detected
PSRG - Preliminary Soil Remediation Goal (Inactive Hazardous Site Branch)
NE - Criteria not establishedBOLD concentrations exceed the Groundwater Protection Levels or Soil to Groundwater Levels

FIGURE

From: Franchina, Dave
Sent: Thursday, March 13, 2014 3:16 PM
To: Minnich, Carolyn
Subject: RE: Charlotte Chemical Lab, 1100 South Boulevard, Charlotte -- Report regarding UST-5 and
UST-7

Thanks, Carolyn. I appreciate the prompt turnaround on our request.

Regards,
Dave

David A. Franchina
K&L Gates LLP
214 North Tryon Street
47th Floor
Charlotte, NC 28202
Phone: [phone]
Fax: [phone]
[e-mail]
www.klgates.com

From: Minnich, Carolyn [mailto:[e-mail]]
Sent: Thursday, March 13, 2014 2:53 PM
To: Franchina, Dave
Subject: RE: Charlotte Chemical Lab, 1100 South Boulevard, Charlotte -- Report regarding UST-5 and
UST-7

Dave:

Based on the soil samples and information submitted to NC Brownfields Program, no additional
assessment is necessary in the vicinity of UST-5 or UST-7. Based on the reports, soils that exceed the
IHSB Residential Preliminary Soil Remediation Goals (PRSG) were removed from the property in these
areas, therefore no changes are necessary to the Brownfields Plat Map. Once you have the final reports
for soil disposal, please forward them to my attention. I will send one final letter with addressing all the
UST removals and remaining soils. If you have any questions or comments, please contact me.

Carolyn Minnich
------------------------------------------------------
Brownfields Project Manager
NCDENR-DWM
704/661-0330
www.ncbrownfields.org
Come Clean Up With Us!
------------------------------------------------------
Email correspondence to and from this address is subject to the North Carolina Public Records Law and
may be disclosed to third parties unless the content is exempt by statute or other regulation.
From: Franchina, Dave
Sent: Wednesday, March 12, 2014 11:34 AM
To: Minnich, Carolyn
Subject: RE: Charlotte Chemical Lab, 1100 South Boulevard, Charlotte -- Report regarding UST-5 and
UST-7

Carolyn,

Thanks for the follow up question.

As I understand things, there was very little impacted soil from UST-5 -- only 3 or so drums that were
generated as the developer over-excavated the UST bottom sample in the vicinity of UST-5 S-1 to get to
a clean (that is, below Residential PSRGs) bottom. Those soils went to BFI/Republic Landfill, Concord,
along with about 3,000 tons of soil from the property.

There was a greater amount of impacted soil from UST-7 -- about 150 tons. It went to Lattimore.

EFI will include precise amounts of disposed soil, manifests, and sampling data to confirm that the
landfills can accept these (and other) soils when it puts together its final report on soil management.

Please contact me if you have questions.

Regards,
Dave

David A. Franchina
K&L Gates LLP
214 North Tryon Street
47th Floor
Charlotte, NC 28202
Phone: [phone]
Fax: [phone]
[e-mail]
www.klgates.com

From: Minnich, Carolyn [mailto:[e-mail]]
Sent: Monday, March 10, 2014 9:54 AM
To: Franchina, Dave
Subject: RE: Charlotte Chemical Lab, 1100 South Boulevard, Charlotte -- Report regarding UST-5 and
UST-7

Dave:

I am reviewing the report now. One question not address was how much soil was excavated and where
was it taken to?

CFM

Carolyn Minnich
------------------------------------------------------
Brownfields Project Manager
NCDENR-DWM
704/661-0330
www.ncbrownfields.org
Come Clean Up With Us!
------------------------------------------------------
Email correspondence to and from this address is subject to the North Carolina Public Records Law and
may be disclosed to third parties unless the content is exempt by statute or other regulation.

From: Franchina, Dave [mailto:[e-mail]]
Sent: Thursday, March 06, 2014 5:34 PM
To: Minnich, Carolyn
Subject: Charlotte Chemical Lab, 1100 South Boulevard, Charlotte -- Report regarding UST-5 and UST-7

Carolyn,

As we’ve discussed, the developer of the referenced property has discovered two additional petroleum
USTs during development. They’ve been designated UST-5 and UST-7. (We found something we
thought was UST-6, but it wasn’t, so that will be a gap in our numbering.) The enclosed letter, prepared
by John Burkart at EFI, describes the tanks and how they’ve been handled. It also describes the
confirmation sampling taken around the tanks.

Please review the enclosed and confirm that (1) developer can move forward with construction in the
vicinity of UST-5 and UST-7 and (2) since no soils exceeding residential standards remain in either tank
excavation, no new data points need to be added to the Brownfields plat.

Thanks,
Dave
#=CL#
March 04, 2014
LIMS USE: FR - JOHN BURKART
LIMS OBJECT ID: 92190644
92190644
Project:
Pace Project No.:
RE:
Mr. John Burkart
EFI Global
9307 Monroe Road
Suite M
Charlotte, NC 28270
CHARLOTTE CHEMICAL
Dear Mr. Burkart:
Enclosed are the analytical results for sample(s) received by the laboratory on February 21, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 42
#=CL#
March 04, 2014
Page 2
LIMS USE: FR - JOHN BURKART
LIMS OBJECT ID: 92190644
cc:Accounts Payable, EFI Global
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 2 of 42
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 42
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92190644001 SOIL CUTTING PAD 1 STOCK 1 EPA 8015 Modified 2 PASI-CNU1
EPA 6010 7 PASI-AJMW
EPA 7471 1 PASI-AMTS
EPA 8270 21 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CLLW
92190644002 SOIL CUTTING PAD 1 STOCK 2 EPA 8015 Modified 2 PASI-CNU1
EPA 6010 7 PASI-AJMW
EPA 7471 1 PASI-AMTS
EPA 8270 21 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CLLW
92190644003 SOIL CUTTING PAD 1 STOCK 3 EPA 8015 Modified 2 PASI-CNU1
EPA 6010 7 PASI-AJMW
EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASH1
EPA 7471 1 PASI-AMTS
EPA 8270 21 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CLLW
92190644004 SOIL CUTTING PAD 1 STOCK 4 EPA 8015 Modified 2 PASI-CNU1
EPA 6010 7 PASI-AJMW
EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASH1
EPA 7471 1 PASI-AMTS
EPA 8270 21 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CLLW
92190644005 SOIL CUTTING PAD 1 STOCK 5 EPA 8015 Modified 2 PASI-CNU1
EPA 6010 7 PASI-AJMW
EPA 7471 1 PASI-AMTS
EPA 8270 21 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CLLW
92190644006 SOIL CUTTING PAD 1 STOCK 6 EPA 8015 Modified 2 PASI-CNU1
EPA 6010 7 PASI-AJMW
EPA 6010 7 PASI-AJMW
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
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Page 4 of 42
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7470 1 PASI-ASH1
EPA 7471 1 PASI-AMTS
EPA 8270 21 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CLLW
92190644007 SOIL CUTTING PAD 1 STOCK 7 EPA 8015 Modified 2 PASI-CNU1
EPA 6010 7 PASI-AJMW
EPA 7471 1 PASI-AMTS
EPA 8270 21 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CLLW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 1
Lab ID:92190644001 Collected:02/20/14 11:30 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 7.6 mg/kg 02/24/14 10:07 68334-30-502/21/14 14:585.0 1
Surrogates
n-Pentacosane (S)83 %02/24/14 10:07 629-99-202/21/14 14:5841-119 1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 02/25/14 14:18 7440-38-202/25/14 10:250.98 1
Barium 88.0 mg/kg 02/25/14 14:18 7440-39-302/25/14 10:250.49 1
Cadmium 0.11 mg/kg 02/25/14 14:18 7440-43-902/25/14 10:250.098 1
Chromium 30.5 mg/kg 02/25/14 14:18 7440-47-302/25/14 10:250.49 1
Lead 15.5 mg/kg 02/25/14 14:18 7439-92-102/25/14 10:250.49 1
Selenium ND mg/kg 02/25/14 14:18 7782-49-202/25/14 10:250.98 1
Silver ND mg/kg 02/25/14 14:18 7440-22-402/25/14 10:250.49 1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.048 mg/kg 02/25/14 14:57 7439-97-6 M1,R102/24/14 22:450.0036 1
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 02/24/14 11:05 83-32-902/21/14 14:263301
Acenaphthylene ND ug/kg 02/24/14 11:05 208-96-802/21/14 14:263301
Anthracene ND ug/kg 02/24/14 11:05 120-12-702/21/14 14:263301
Benzo(a)anthracene ND ug/kg 02/24/14 11:05 56-55-302/21/14 14:263301
Benzo(a)pyrene ND ug/kg 02/24/14 11:05 50-32-802/21/14 14:263301
Benzo(b)fluoranthene ND ug/kg 02/24/14 11:05 205-99-202/21/14 14:263301
Benzo(g,h,i)perylene ND ug/kg 02/24/14 11:05 191-24-202/21/14 14:263301
Benzo(k)fluoranthene ND ug/kg 02/24/14 11:05 207-08-902/21/14 14:263301
Chrysene ND ug/kg 02/24/14 11:05 218-01-902/21/14 14:263301
Dibenz(a,h)anthracene ND ug/kg 02/24/14 11:05 53-70-302/21/14 14:263301
Fluoranthene ND ug/kg 02/24/14 11:05 206-44-002/21/14 14:263301
Fluorene ND ug/kg 02/24/14 11:05 86-73-702/21/14 14:263301
Indeno(1,2,3-cd)pyrene ND ug/kg 02/24/14 11:05 193-39-502/21/14 14:263301
1-Methylnaphthalene ND ug/kg 02/24/14 11:05 90-12-002/21/14 14:263301
2-Methylnaphthalene ND ug/kg 02/24/14 11:05 91-57-602/21/14 14:263301
Naphthalene ND ug/kg 02/24/14 11:05 91-20-302/21/14 14:263301
Phenanthrene ND ug/kg 02/24/14 11:05 85-01-802/21/14 14:263301
Pyrene ND ug/kg 02/24/14 11:05 129-00-002/21/14 14:263301
Surrogates
Nitrobenzene-d5 (S)69 %02/24/14 11:05 4165-60-002/21/14 14:2623-110 1
2-Fluorobiphenyl (S)69 %02/24/14 11:05 321-60-802/21/14 14:2630-110 1
Terphenyl-d14 (S)81 %02/24/14 11:05 1718-51-002/21/14 14:2628-110 1
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 02/24/14 14:54 67-64-11081
Benzene ND ug/kg 02/24/14 14:54 71-43-25.4 1
Bromobenzene ND ug/kg 02/24/14 14:54 108-86-15.4 1
Bromochloromethane ND ug/kg 02/24/14 14:54 74-97-55.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 1
Lab ID:92190644001 Collected:02/20/14 11:30 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromodichloromethane ND ug/kg 02/24/14 14:54 75-27-45.4 1
Bromoform ND ug/kg 02/24/14 14:54 75-25-25.4 1
Bromomethane ND ug/kg 02/24/14 14:54 74-83-910.8 1
2-Butanone (MEK)ND ug/kg 02/24/14 14:54 78-93-31081
n-Butylbenzene ND ug/kg 02/24/14 14:54 104-51-85.4 1
sec-Butylbenzene ND ug/kg 02/24/14 14:54 135-98-85.4 1
tert-Butylbenzene ND ug/kg 02/24/14 14:54 98-06-65.4 1
Carbon tetrachloride ND ug/kg 02/24/14 14:54 56-23-55.4 1
Chlorobenzene ND ug/kg 02/24/14 14:54 108-90-75.4 1
Chloroethane ND ug/kg 02/24/14 14:54 75-00-310.8 1
Chloroform ND ug/kg 02/24/14 14:54 67-66-35.4 1
Chloromethane ND ug/kg 02/24/14 14:54 74-87-310.8 1
2-Chlorotoluene ND ug/kg 02/24/14 14:54 95-49-85.4 1
4-Chlorotoluene ND ug/kg 02/24/14 14:54 106-43-45.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/24/14 14:54 96-12-85.4 1
Dibromochloromethane ND ug/kg 02/24/14 14:54 124-48-15.4 1
1,2-Dibromoethane (EDB)ND ug/kg 02/24/14 14:54 106-93-45.4 1
Dibromomethane ND ug/kg 02/24/14 14:54 74-95-35.4 1
1,2-Dichlorobenzene ND ug/kg 02/24/14 14:54 95-50-15.4 1
1,3-Dichlorobenzene ND ug/kg 02/24/14 14:54 541-73-15.4 1
1,4-Dichlorobenzene ND ug/kg 02/24/14 14:54 106-46-75.4 1
Dichlorodifluoromethane ND ug/kg 02/24/14 14:54 75-71-810.8 1
1,1-Dichloroethane ND ug/kg 02/24/14 14:54 75-34-35.4 1
1,2-Dichloroethane ND ug/kg 02/24/14 14:54 107-06-25.4 1
1,1-Dichloroethene ND ug/kg 02/24/14 14:54 75-35-45.4 1
cis-1,2-Dichloroethene ND ug/kg 02/24/14 14:54 156-59-25.4 1
trans-1,2-Dichloroethene ND ug/kg 02/24/14 14:54 156-60-55.4 1
1,2-Dichloropropane ND ug/kg 02/24/14 14:54 78-87-55.4 1
1,3-Dichloropropane ND ug/kg 02/24/14 14:54 142-28-95.4 1
2,2-Dichloropropane ND ug/kg 02/24/14 14:54 594-20-75.4 1
1,1-Dichloropropene ND ug/kg 02/24/14 14:54 563-58-65.4 1
cis-1,3-Dichloropropene ND ug/kg 02/24/14 14:54 10061-01-55.4 1
trans-1,3-Dichloropropene ND ug/kg 02/24/14 14:54 10061-02-65.4 1
Diisopropyl ether ND ug/kg 02/24/14 14:54 108-20-35.4 1
Ethylbenzene ND ug/kg 02/24/14 14:54 100-41-45.4 1
Hexachloro-1,3-butadiene ND ug/kg 02/24/14 14:54 87-68-35.4 1
2-Hexanone ND ug/kg 02/24/14 14:54 591-78-654.2 1
Isopropylbenzene (Cumene)ND ug/kg 02/24/14 14:54 98-82-85.4 1
p-Isopropyltoluene ND ug/kg 02/24/14 14:54 99-87-65.4 1
Methylene Chloride ND ug/kg 02/24/14 14:54 75-09-221.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/24/14 14:54 108-10-154.2 1
Methyl-tert-butyl ether ND ug/kg 02/24/14 14:54 1634-04-45.4 1
Naphthalene ND ug/kg 02/24/14 14:54 91-20-35.4 1
n-Propylbenzene ND ug/kg 02/24/14 14:54 103-65-15.4 1
Styrene ND ug/kg 02/24/14 14:54 100-42-55.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 1
Lab ID:92190644001 Collected:02/20/14 11:30 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 02/24/14 14:54 630-20-65.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/24/14 14:54 79-34-55.4 1
Tetrachloroethene ND ug/kg 02/24/14 14:54 127-18-45.4 1
Toluene ND ug/kg 02/24/14 14:54 108-88-35.4 1
1,2,3-Trichlorobenzene ND ug/kg 02/24/14 14:54 87-61-65.4 1
1,2,4-Trichlorobenzene ND ug/kg 02/24/14 14:54 120-82-15.4 1
1,1,1-Trichloroethane ND ug/kg 02/24/14 14:54 71-55-65.4 1
1,1,2-Trichloroethane ND ug/kg 02/24/14 14:54 79-00-55.4 1
Trichloroethene ND ug/kg 02/24/14 14:54 79-01-65.4 1
Trichlorofluoromethane ND ug/kg 02/24/14 14:54 75-69-45.4 1
1,2,3-Trichloropropane ND ug/kg 02/24/14 14:54 96-18-45.4 1
1,2,4-Trimethylbenzene ND ug/kg 02/24/14 14:54 95-63-65.4 1
1,3,5-Trimethylbenzene ND ug/kg 02/24/14 14:54 108-67-85.4 1
Vinyl acetate ND ug/kg 02/24/14 14:54 108-05-454.2 1
Vinyl chloride ND ug/kg 02/24/14 14:54 75-01-410.8 1
Xylene (Total)ND ug/kg 02/24/14 14:54 1330-20-710.8 1
m&p-Xylene ND ug/kg 02/24/14 14:54 179601-23-110.8 1
o-Xylene ND ug/kg 02/24/14 14:54 95-47-65.4 1
Surrogates
Toluene-d8 (S)109 %02/24/14 14:54 2037-26-570-130 1
4-Bromofluorobenzene (S)94 %02/24/14 14:54 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %02/24/14 14:54 17060-07-070-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 20.9 %02/24/14 16:110.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 2
Lab ID:92190644002 Collected:02/20/14 11:35 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 167 mg/kg 02/22/14 15:33 68334-30-502/21/14 14:585.0 1
Surrogates
n-Pentacosane (S)79 %02/22/14 15:33 629-99-202/21/14 14:5841-119 1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 02/25/14 14:27 7440-38-202/25/14 10:250.76 1
Barium 95.5 mg/kg 02/25/14 14:27 7440-39-302/25/14 10:250.38 1
Cadmium ND mg/kg 02/25/14 14:27 7440-43-902/25/14 10:250.076 1
Chromium 17.0 mg/kg 02/25/14 14:27 7440-47-302/25/14 10:250.38 1
Lead 16.7 mg/kg 02/25/14 14:27 7439-92-102/25/14 10:250.38 1
Selenium ND mg/kg 02/25/14 14:27 7782-49-202/25/14 10:250.76 1
Silver ND mg/kg 02/25/14 14:27 7440-22-402/25/14 10:250.38 1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.052 mg/kg 02/25/14 15:10 7439-97-602/24/14 22:450.0042 1
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 02/24/14 11:36 83-32-902/21/14 14:263301
Acenaphthylene ND ug/kg 02/24/14 11:36 208-96-802/21/14 14:263301
Anthracene ND ug/kg 02/24/14 11:36 120-12-702/21/14 14:263301
Benzo(a)anthracene ND ug/kg 02/24/14 11:36 56-55-302/21/14 14:263301
Benzo(a)pyrene ND ug/kg 02/24/14 11:36 50-32-802/21/14 14:263301
Benzo(b)fluoranthene ND ug/kg 02/24/14 11:36 205-99-202/21/14 14:263301
Benzo(g,h,i)perylene ND ug/kg 02/24/14 11:36 191-24-202/21/14 14:263301
Benzo(k)fluoranthene ND ug/kg 02/24/14 11:36 207-08-902/21/14 14:263301
Chrysene ND ug/kg 02/24/14 11:36 218-01-902/21/14 14:263301
Dibenz(a,h)anthracene ND ug/kg 02/24/14 11:36 53-70-302/21/14 14:263301
Fluoranthene ND ug/kg 02/24/14 11:36 206-44-002/21/14 14:263301
Fluorene ND ug/kg 02/24/14 11:36 86-73-702/21/14 14:263301
Indeno(1,2,3-cd)pyrene ND ug/kg 02/24/14 11:36 193-39-502/21/14 14:263301
1-Methylnaphthalene ND ug/kg 02/24/14 11:36 90-12-002/21/14 14:263301
2-Methylnaphthalene ND ug/kg 02/24/14 11:36 91-57-602/21/14 14:263301
Naphthalene ND ug/kg 02/24/14 11:36 91-20-302/21/14 14:263301
Phenanthrene ND ug/kg 02/24/14 11:36 85-01-802/21/14 14:263301
Pyrene ND ug/kg 02/24/14 11:36 129-00-002/21/14 14:263301
Surrogates
Nitrobenzene-d5 (S)70 %02/24/14 11:36 4165-60-002/21/14 14:2623-110 1
2-Fluorobiphenyl (S)75 %02/24/14 11:36 321-60-802/21/14 14:2630-110 1
Terphenyl-d14 (S)89 %02/24/14 11:36 1718-51-002/21/14 14:2628-110 1
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 209 ug/kg 02/24/14 15:14 67-64-1 A+95.2 1
Benzene ND ug/kg 02/24/14 15:14 71-43-24.8 1
Bromobenzene ND ug/kg 02/24/14 15:14 108-86-14.8 1
Bromochloromethane ND ug/kg 02/24/14 15:14 74-97-54.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 2
Lab ID:92190644002 Collected:02/20/14 11:35 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromodichloromethane ND ug/kg 02/24/14 15:14 75-27-44.8 1
Bromoform ND ug/kg 02/24/14 15:14 75-25-24.8 1
Bromomethane ND ug/kg 02/24/14 15:14 74-83-99.5 1
2-Butanone (MEK)ND ug/kg 02/24/14 15:14 78-93-395.2 1
n-Butylbenzene ND ug/kg 02/24/14 15:14 104-51-84.8 1
sec-Butylbenzene ND ug/kg 02/24/14 15:14 135-98-84.8 1
tert-Butylbenzene ND ug/kg 02/24/14 15:14 98-06-64.8 1
Carbon tetrachloride ND ug/kg 02/24/14 15:14 56-23-54.8 1
Chlorobenzene ND ug/kg 02/24/14 15:14 108-90-74.8 1
Chloroethane ND ug/kg 02/24/14 15:14 75-00-39.5 1
Chloroform ND ug/kg 02/24/14 15:14 67-66-34.8 1
Chloromethane ND ug/kg 02/24/14 15:14 74-87-39.5 1
2-Chlorotoluene ND ug/kg 02/24/14 15:14 95-49-84.8 1
4-Chlorotoluene ND ug/kg 02/24/14 15:14 106-43-44.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/24/14 15:14 96-12-84.8 1
Dibromochloromethane ND ug/kg 02/24/14 15:14 124-48-14.8 1
1,2-Dibromoethane (EDB)ND ug/kg 02/24/14 15:14 106-93-44.8 1
Dibromomethane ND ug/kg 02/24/14 15:14 74-95-34.8 1
1,2-Dichlorobenzene ND ug/kg 02/24/14 15:14 95-50-14.8 1
1,3-Dichlorobenzene ND ug/kg 02/24/14 15:14 541-73-14.8 1
1,4-Dichlorobenzene ND ug/kg 02/24/14 15:14 106-46-74.8 1
Dichlorodifluoromethane ND ug/kg 02/24/14 15:14 75-71-89.5 1
1,1-Dichloroethane ND ug/kg 02/24/14 15:14 75-34-34.8 1
1,2-Dichloroethane ND ug/kg 02/24/14 15:14 107-06-24.8 1
1,1-Dichloroethene ND ug/kg 02/24/14 15:14 75-35-44.8 1
cis-1,2-Dichloroethene ND ug/kg 02/24/14 15:14 156-59-24.8 1
trans-1,2-Dichloroethene ND ug/kg 02/24/14 15:14 156-60-54.8 1
1,2-Dichloropropane ND ug/kg 02/24/14 15:14 78-87-54.8 1
1,3-Dichloropropane ND ug/kg 02/24/14 15:14 142-28-94.8 1
2,2-Dichloropropane ND ug/kg 02/24/14 15:14 594-20-74.8 1
1,1-Dichloropropene ND ug/kg 02/24/14 15:14 563-58-64.8 1
cis-1,3-Dichloropropene ND ug/kg 02/24/14 15:14 10061-01-54.8 1
trans-1,3-Dichloropropene ND ug/kg 02/24/14 15:14 10061-02-64.8 1
Diisopropyl ether ND ug/kg 02/24/14 15:14 108-20-34.8 1
Ethylbenzene ND ug/kg 02/24/14 15:14 100-41-44.8 1
Hexachloro-1,3-butadiene ND ug/kg 02/24/14 15:14 87-68-34.8 1
2-Hexanone ND ug/kg 02/24/14 15:14 591-78-647.6 1
Isopropylbenzene (Cumene)ND ug/kg 02/24/14 15:14 98-82-84.8 1
p-Isopropyltoluene ND ug/kg 02/24/14 15:14 99-87-64.8 1
Methylene Chloride ND ug/kg 02/24/14 15:14 75-09-219.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/24/14 15:14 108-10-147.6 1
Methyl-tert-butyl ether ND ug/kg 02/24/14 15:14 1634-04-44.8 1
Naphthalene ND ug/kg 02/24/14 15:14 91-20-34.8 1
n-Propylbenzene ND ug/kg 02/24/14 15:14 103-65-14.8 1
Styrene ND ug/kg 02/24/14 15:14 100-42-54.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 2
Lab ID:92190644002 Collected:02/20/14 11:35 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 02/24/14 15:14 630-20-64.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/24/14 15:14 79-34-54.8 1
Tetrachloroethene ND ug/kg 02/24/14 15:14 127-18-44.8 1
Toluene ND ug/kg 02/24/14 15:14 108-88-34.8 1
1,2,3-Trichlorobenzene ND ug/kg 02/24/14 15:14 87-61-64.8 1
1,2,4-Trichlorobenzene ND ug/kg 02/24/14 15:14 120-82-14.8 1
1,1,1-Trichloroethane ND ug/kg 02/24/14 15:14 71-55-64.8 1
1,1,2-Trichloroethane ND ug/kg 02/24/14 15:14 79-00-54.8 1
Trichloroethene ND ug/kg 02/24/14 15:14 79-01-64.8 1
Trichlorofluoromethane ND ug/kg 02/24/14 15:14 75-69-44.8 1
1,2,3-Trichloropropane ND ug/kg 02/24/14 15:14 96-18-44.8 1
1,2,4-Trimethylbenzene ND ug/kg 02/24/14 15:14 95-63-64.8 1
1,3,5-Trimethylbenzene ND ug/kg 02/24/14 15:14 108-67-84.8 1
Vinyl acetate ND ug/kg 02/24/14 15:14 108-05-447.6 1
Vinyl chloride ND ug/kg 02/24/14 15:14 75-01-49.5 1
Xylene (Total)ND ug/kg 02/24/14 15:14 1330-20-79.5 1
m&p-Xylene ND ug/kg 02/24/14 15:14 179601-23-19.5 1
o-Xylene ND ug/kg 02/24/14 15:14 95-47-64.8 1
Surrogates
Toluene-d8 (S)112 %02/24/14 15:14 2037-26-570-130 1
4-Bromofluorobenzene (S)93 %02/24/14 15:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %02/24/14 15:14 17060-07-070-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 15.8 %02/24/14 16:110.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 3
Lab ID:92190644003 Collected:02/20/14 11:40 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 13.7 mg/kg 02/22/14 15:33 68334-30-502/21/14 14:585.0 1
Surrogates
n-Pentacosane (S)93 %02/22/14 15:33 629-99-202/21/14 14:5841-119 1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 02/25/14 14:30 7440-38-202/25/14 10:250.78 1
Barium 204 mg/kg 02/25/14 14:30 7440-39-302/25/14 10:250.39 1
Cadmium 0.17 mg/kg 02/25/14 14:30 7440-43-902/25/14 10:250.078 1
Chromium 21.4 mg/kg 02/25/14 14:30 7440-47-302/25/14 10:250.39 1
Lead 25.9 mg/kg 02/25/14 14:30 7439-92-102/25/14 10:250.39 1
Selenium ND mg/kg 02/25/14 14:30 7782-49-202/25/14 10:250.78 1
Silver ND mg/kg 02/25/14 14:30 7440-22-402/25/14 10:250.39 1
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 02/28/14 20:10
Arsenic ND mg/L 03/04/14 14:21 7440-38-203/03/14 17:100.050 1
Barium 0.82 mg/L 03/04/14 14:21 7440-39-303/03/14 17:100.25 1
Cadmium ND mg/L 03/04/14 14:21 7440-43-903/03/14 17:100.0050 1
Chromium ND mg/L 03/04/14 14:21 7440-47-303/03/14 17:100.025 1
Lead 0.064 mg/L 03/04/14 14:21 7439-92-103/03/14 17:100.025 1
Selenium ND mg/L 03/04/14 14:21 7782-49-203/03/14 17:100.10 1
Silver ND mg/L 03/04/14 14:21 7440-22-403/03/14 17:100.025 1
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 02/28/14 20:10
Mercury ND ug/L 03/04/14 13:41 7439-97-6 M1,R103/03/14 18:000.20 1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.16 mg/kg 02/25/14 15:18 7439-97-602/24/14 22:450.018 5
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 02/24/14 12:07 83-32-902/21/14 14:263301
Acenaphthylene ND ug/kg 02/24/14 12:07 208-96-802/21/14 14:263301
Anthracene ND ug/kg 02/24/14 12:07 120-12-702/21/14 14:263301
Benzo(a)anthracene ND ug/kg 02/24/14 12:07 56-55-302/21/14 14:263301
Benzo(a)pyrene ND ug/kg 02/24/14 12:07 50-32-802/21/14 14:263301
Benzo(b)fluoranthene ND ug/kg 02/24/14 12:07 205-99-202/21/14 14:263301
Benzo(g,h,i)perylene ND ug/kg 02/24/14 12:07 191-24-202/21/14 14:263301
Benzo(k)fluoranthene ND ug/kg 02/24/14 12:07 207-08-902/21/14 14:263301
Chrysene ND ug/kg 02/24/14 12:07 218-01-902/21/14 14:263301
Dibenz(a,h)anthracene ND ug/kg 02/24/14 12:07 53-70-302/21/14 14:263301
Fluoranthene ND ug/kg 02/24/14 12:07 206-44-002/21/14 14:263301
Fluorene ND ug/kg 02/24/14 12:07 86-73-702/21/14 14:263301
Indeno(1,2,3-cd)pyrene ND ug/kg 02/24/14 12:07 193-39-502/21/14 14:263301
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 3
Lab ID:92190644003 Collected:02/20/14 11:40 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
1-Methylnaphthalene ND ug/kg 02/24/14 12:07 90-12-002/21/14 14:263301
2-Methylnaphthalene ND ug/kg 02/24/14 12:07 91-57-602/21/14 14:263301
Naphthalene ND ug/kg 02/24/14 12:07 91-20-302/21/14 14:263301
Phenanthrene ND ug/kg 02/24/14 12:07 85-01-802/21/14 14:263301
Pyrene ND ug/kg 02/24/14 12:07 129-00-002/21/14 14:263301
Surrogates
Nitrobenzene-d5 (S)59 %02/24/14 12:07 4165-60-002/21/14 14:2623-110 1
2-Fluorobiphenyl (S)61 %02/24/14 12:07 321-60-802/21/14 14:2630-110 1
Terphenyl-d14 (S)69 %02/24/14 12:07 1718-51-002/21/14 14:2628-110 1
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 02/24/14 15:34 67-64-170.4 1
Benzene ND ug/kg 02/24/14 15:34 71-43-23.5 1
Bromobenzene ND ug/kg 02/24/14 15:34 108-86-13.5 1
Bromochloromethane ND ug/kg 02/24/14 15:34 74-97-53.5 1
Bromodichloromethane ND ug/kg 02/24/14 15:34 75-27-43.5 1
Bromoform ND ug/kg 02/24/14 15:34 75-25-23.5 1
Bromomethane ND ug/kg 02/24/14 15:34 74-83-97.0 1
2-Butanone (MEK)ND ug/kg 02/24/14 15:34 78-93-370.4 1
n-Butylbenzene ND ug/kg 02/24/14 15:34 104-51-83.5 1
sec-Butylbenzene ND ug/kg 02/24/14 15:34 135-98-83.5 1
tert-Butylbenzene ND ug/kg 02/24/14 15:34 98-06-63.5 1
Carbon tetrachloride ND ug/kg 02/24/14 15:34 56-23-53.5 1
Chlorobenzene ND ug/kg 02/24/14 15:34 108-90-73.5 1
Chloroethane ND ug/kg 02/24/14 15:34 75-00-37.0 1
Chloroform ND ug/kg 02/24/14 15:34 67-66-33.5 1
Chloromethane ND ug/kg 02/24/14 15:34 74-87-37.0 1
2-Chlorotoluene ND ug/kg 02/24/14 15:34 95-49-83.5 1
4-Chlorotoluene ND ug/kg 02/24/14 15:34 106-43-43.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/24/14 15:34 96-12-83.5 1
Dibromochloromethane ND ug/kg 02/24/14 15:34 124-48-13.5 1
1,2-Dibromoethane (EDB)ND ug/kg 02/24/14 15:34 106-93-43.5 1
Dibromomethane ND ug/kg 02/24/14 15:34 74-95-33.5 1
1,2-Dichlorobenzene ND ug/kg 02/24/14 15:34 95-50-13.5 1
1,3-Dichlorobenzene ND ug/kg 02/24/14 15:34 541-73-13.5 1
1,4-Dichlorobenzene ND ug/kg 02/24/14 15:34 106-46-73.5 1
Dichlorodifluoromethane ND ug/kg 02/24/14 15:34 75-71-87.0 1
1,1-Dichloroethane ND ug/kg 02/24/14 15:34 75-34-33.5 1
1,2-Dichloroethane ND ug/kg 02/24/14 15:34 107-06-23.5 1
1,1-Dichloroethene ND ug/kg 02/24/14 15:34 75-35-43.5 1
cis-1,2-Dichloroethene ND ug/kg 02/24/14 15:34 156-59-23.5 1
trans-1,2-Dichloroethene ND ug/kg 02/24/14 15:34 156-60-53.5 1
1,2-Dichloropropane ND ug/kg 02/24/14 15:34 78-87-53.5 1
1,3-Dichloropropane ND ug/kg 02/24/14 15:34 142-28-93.5 1
2,2-Dichloropropane ND ug/kg 02/24/14 15:34 594-20-73.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 3
Lab ID:92190644003 Collected:02/20/14 11:40 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/kg 02/24/14 15:34 563-58-63.5 1
cis-1,3-Dichloropropene ND ug/kg 02/24/14 15:34 10061-01-53.5 1
trans-1,3-Dichloropropene ND ug/kg 02/24/14 15:34 10061-02-63.5 1
Diisopropyl ether ND ug/kg 02/24/14 15:34 108-20-33.5 1
Ethylbenzene ND ug/kg 02/24/14 15:34 100-41-43.5 1
Hexachloro-1,3-butadiene ND ug/kg 02/24/14 15:34 87-68-33.5 1
2-Hexanone ND ug/kg 02/24/14 15:34 591-78-635.2 1
Isopropylbenzene (Cumene)ND ug/kg 02/24/14 15:34 98-82-83.5 1
p-Isopropyltoluene ND ug/kg 02/24/14 15:34 99-87-63.5 1
Methylene Chloride ND ug/kg 02/24/14 15:34 75-09-214.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/24/14 15:34 108-10-135.2 1
Methyl-tert-butyl ether ND ug/kg 02/24/14 15:34 1634-04-43.5 1
Naphthalene ND ug/kg 02/24/14 15:34 91-20-33.5 1
n-Propylbenzene ND ug/kg 02/24/14 15:34 103-65-13.5 1
Styrene ND ug/kg 02/24/14 15:34 100-42-53.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/24/14 15:34 630-20-63.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/24/14 15:34 79-34-53.5 1
Tetrachloroethene ND ug/kg 02/24/14 15:34 127-18-43.5 1
Toluene ND ug/kg 02/24/14 15:34 108-88-33.5 1
1,2,3-Trichlorobenzene ND ug/kg 02/24/14 15:34 87-61-63.5 1
1,2,4-Trichlorobenzene ND ug/kg 02/24/14 15:34 120-82-13.5 1
1,1,1-Trichloroethane ND ug/kg 02/24/14 15:34 71-55-63.5 1
1,1,2-Trichloroethane ND ug/kg 02/24/14 15:34 79-00-53.5 1
Trichloroethene ND ug/kg 02/24/14 15:34 79-01-63.5 1
Trichlorofluoromethane ND ug/kg 02/24/14 15:34 75-69-43.5 1
1,2,3-Trichloropropane ND ug/kg 02/24/14 15:34 96-18-43.5 1
1,2,4-Trimethylbenzene ND ug/kg 02/24/14 15:34 95-63-63.5 1
1,3,5-Trimethylbenzene ND ug/kg 02/24/14 15:34 108-67-83.5 1
Vinyl acetate ND ug/kg 02/24/14 15:34 108-05-435.2 1
Vinyl chloride ND ug/kg 02/24/14 15:34 75-01-47.0 1
Xylene (Total)ND ug/kg 02/24/14 15:34 1330-20-77.0 1
m&p-Xylene ND ug/kg 02/24/14 15:34 179601-23-17.0 1
o-Xylene ND ug/kg 02/24/14 15:34 95-47-63.5 1
Surrogates
Toluene-d8 (S)121 %02/24/14 15:34 2037-26-570-130 1
4-Bromofluorobenzene (S)84 %02/24/14 15:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)77 %02/24/14 15:34 17060-07-070-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 18.4 %02/24/14 16:110.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 4
Lab ID:92190644004 Collected:02/20/14 11:45 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components ND mg/kg 02/22/14 15:56 68334-30-502/21/14 14:585.0 1
Surrogates
n-Pentacosane (S)67 %02/22/14 15:56 629-99-202/21/14 14:5841-119 1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 02/25/14 14:33 7440-38-202/25/14 10:250.82 1
Barium 72.2 mg/kg 02/25/14 14:33 7440-39-302/25/14 10:250.41 1
Cadmium 0.17 mg/kg 02/25/14 14:33 7440-43-902/25/14 10:250.082 1
Chromium 13.3 mg/kg 02/25/14 14:33 7440-47-302/25/14 10:250.41 1
Lead 5.4 mg/kg 02/25/14 14:33 7439-92-102/25/14 10:250.41 1
Selenium ND mg/kg 02/25/14 14:33 7782-49-202/25/14 10:250.82 1
Silver ND mg/kg 02/25/14 14:33 7440-22-402/25/14 10:250.41 1
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 02/28/14 20:10
Arsenic ND mg/L 03/04/14 14:36 7440-38-203/03/14 17:100.050 1
Barium 0.39 mg/L 03/04/14 14:36 7440-39-303/03/14 17:100.25 1
Cadmium ND mg/L 03/04/14 14:36 7440-43-903/03/14 17:100.0050 1
Chromium ND mg/L 03/04/14 14:36 7440-47-303/03/14 17:100.025 1
Lead 0.029 mg/L 03/04/14 14:36 7439-92-103/03/14 17:100.025 1
Selenium ND mg/L 03/04/14 14:36 7782-49-203/03/14 17:100.10 1
Silver ND mg/L 03/04/14 14:36 7440-22-403/03/14 17:100.025 1
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 02/28/14 20:10
Mercury ND ug/L 03/04/14 13:49 7439-97-603/03/14 18:000.20 1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.023 mg/kg 02/25/14 15:21 7439-97-602/24/14 22:450.0039 1
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 02/24/14 12:37 83-32-902/21/14 14:263301
Acenaphthylene ND ug/kg 02/24/14 12:37 208-96-802/21/14 14:263301
Anthracene ND ug/kg 02/24/14 12:37 120-12-702/21/14 14:263301
Benzo(a)anthracene ND ug/kg 02/24/14 12:37 56-55-302/21/14 14:263301
Benzo(a)pyrene ND ug/kg 02/24/14 12:37 50-32-802/21/14 14:263301
Benzo(b)fluoranthene ND ug/kg 02/24/14 12:37 205-99-202/21/14 14:263301
Benzo(g,h,i)perylene ND ug/kg 02/24/14 12:37 191-24-202/21/14 14:263301
Benzo(k)fluoranthene ND ug/kg 02/24/14 12:37 207-08-902/21/14 14:263301
Chrysene ND ug/kg 02/24/14 12:37 218-01-902/21/14 14:263301
Dibenz(a,h)anthracene ND ug/kg 02/24/14 12:37 53-70-302/21/14 14:263301
Fluoranthene ND ug/kg 02/24/14 12:37 206-44-002/21/14 14:263301
Fluorene ND ug/kg 02/24/14 12:37 86-73-702/21/14 14:263301
Indeno(1,2,3-cd)pyrene ND ug/kg 02/24/14 12:37 193-39-502/21/14 14:263301
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 4
Lab ID:92190644004 Collected:02/20/14 11:45 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
1-Methylnaphthalene ND ug/kg 02/24/14 12:37 90-12-002/21/14 14:263301
2-Methylnaphthalene ND ug/kg 02/24/14 12:37 91-57-602/21/14 14:263301
Naphthalene ND ug/kg 02/24/14 12:37 91-20-302/21/14 14:263301
Phenanthrene ND ug/kg 02/24/14 12:37 85-01-802/21/14 14:263301
Pyrene ND ug/kg 02/24/14 12:37 129-00-002/21/14 14:263301
Surrogates
Nitrobenzene-d5 (S)57 %02/24/14 12:37 4165-60-002/21/14 14:2623-110 1
2-Fluorobiphenyl (S)60 %02/24/14 12:37 321-60-802/21/14 14:2630-110 1
Terphenyl-d14 (S)67 %02/24/14 12:37 1718-51-002/21/14 14:2628-110 1
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 02/24/14 15:54 67-64-179.9 1
Benzene ND ug/kg 02/24/14 15:54 71-43-24.0 1
Bromobenzene ND ug/kg 02/24/14 15:54 108-86-14.0 1
Bromochloromethane ND ug/kg 02/24/14 15:54 74-97-54.0 1
Bromodichloromethane ND ug/kg 02/24/14 15:54 75-27-44.0 1
Bromoform ND ug/kg 02/24/14 15:54 75-25-24.0 1
Bromomethane ND ug/kg 02/24/14 15:54 74-83-98.0 1
2-Butanone (MEK)ND ug/kg 02/24/14 15:54 78-93-379.9 1
n-Butylbenzene ND ug/kg 02/24/14 15:54 104-51-84.0 1
sec-Butylbenzene ND ug/kg 02/24/14 15:54 135-98-84.0 1
tert-Butylbenzene ND ug/kg 02/24/14 15:54 98-06-64.0 1
Carbon tetrachloride ND ug/kg 02/24/14 15:54 56-23-54.0 1
Chlorobenzene ND ug/kg 02/24/14 15:54 108-90-74.0 1
Chloroethane ND ug/kg 02/24/14 15:54 75-00-38.0 1
Chloroform ND ug/kg 02/24/14 15:54 67-66-34.0 1
Chloromethane ND ug/kg 02/24/14 15:54 74-87-38.0 1
2-Chlorotoluene ND ug/kg 02/24/14 15:54 95-49-84.0 1
4-Chlorotoluene ND ug/kg 02/24/14 15:54 106-43-44.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/24/14 15:54 96-12-84.0 1
Dibromochloromethane ND ug/kg 02/24/14 15:54 124-48-14.0 1
1,2-Dibromoethane (EDB)ND ug/kg 02/24/14 15:54 106-93-44.0 1
Dibromomethane ND ug/kg 02/24/14 15:54 74-95-34.0 1
1,2-Dichlorobenzene ND ug/kg 02/24/14 15:54 95-50-14.0 1
1,3-Dichlorobenzene ND ug/kg 02/24/14 15:54 541-73-14.0 1
1,4-Dichlorobenzene ND ug/kg 02/24/14 15:54 106-46-74.0 1
Dichlorodifluoromethane ND ug/kg 02/24/14 15:54 75-71-88.0 1
1,1-Dichloroethane ND ug/kg 02/24/14 15:54 75-34-34.0 1
1,2-Dichloroethane ND ug/kg 02/24/14 15:54 107-06-24.0 1
1,1-Dichloroethene ND ug/kg 02/24/14 15:54 75-35-44.0 1
cis-1,2-Dichloroethene ND ug/kg 02/24/14 15:54 156-59-24.0 1
trans-1,2-Dichloroethene ND ug/kg 02/24/14 15:54 156-60-54.0 1
1,2-Dichloropropane ND ug/kg 02/24/14 15:54 78-87-54.0 1
1,3-Dichloropropane ND ug/kg 02/24/14 15:54 142-28-94.0 1
2,2-Dichloropropane ND ug/kg 02/24/14 15:54 594-20-74.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 4
Lab ID:92190644004 Collected:02/20/14 11:45 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/kg 02/24/14 15:54 563-58-64.0 1
cis-1,3-Dichloropropene ND ug/kg 02/24/14 15:54 10061-01-54.0 1
trans-1,3-Dichloropropene ND ug/kg 02/24/14 15:54 10061-02-64.0 1
Diisopropyl ether ND ug/kg 02/24/14 15:54 108-20-34.0 1
Ethylbenzene ND ug/kg 02/24/14 15:54 100-41-44.0 1
Hexachloro-1,3-butadiene ND ug/kg 02/24/14 15:54 87-68-34.0 1
2-Hexanone ND ug/kg 02/24/14 15:54 591-78-639.9 1
Isopropylbenzene (Cumene)ND ug/kg 02/24/14 15:54 98-82-84.0 1
p-Isopropyltoluene ND ug/kg 02/24/14 15:54 99-87-64.0 1
Methylene Chloride ND ug/kg 02/24/14 15:54 75-09-216.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/24/14 15:54 108-10-139.9 1
Methyl-tert-butyl ether ND ug/kg 02/24/14 15:54 1634-04-44.0 1
Naphthalene ND ug/kg 02/24/14 15:54 91-20-34.0 1
n-Propylbenzene ND ug/kg 02/24/14 15:54 103-65-14.0 1
Styrene ND ug/kg 02/24/14 15:54 100-42-54.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/24/14 15:54 630-20-64.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/24/14 15:54 79-34-54.0 1
Tetrachloroethene ND ug/kg 02/24/14 15:54 127-18-44.0 1
Toluene ND ug/kg 02/24/14 15:54 108-88-34.0 1
1,2,3-Trichlorobenzene ND ug/kg 02/24/14 15:54 87-61-64.0 1
1,2,4-Trichlorobenzene ND ug/kg 02/24/14 15:54 120-82-14.0 1
1,1,1-Trichloroethane ND ug/kg 02/24/14 15:54 71-55-64.0 1
1,1,2-Trichloroethane ND ug/kg 02/24/14 15:54 79-00-54.0 1
Trichloroethene ND ug/kg 02/24/14 15:54 79-01-64.0 1
Trichlorofluoromethane ND ug/kg 02/24/14 15:54 75-69-44.0 1
1,2,3-Trichloropropane ND ug/kg 02/24/14 15:54 96-18-44.0 1
1,2,4-Trimethylbenzene ND ug/kg 02/24/14 15:54 95-63-64.0 1
1,3,5-Trimethylbenzene ND ug/kg 02/24/14 15:54 108-67-84.0 1
Vinyl acetate ND ug/kg 02/24/14 15:54 108-05-439.9 1
Vinyl chloride ND ug/kg 02/24/14 15:54 75-01-48.0 1
Xylene (Total)ND ug/kg 02/24/14 15:54 1330-20-78.0 1
m&p-Xylene ND ug/kg 02/24/14 15:54 179601-23-18.0 1
o-Xylene ND ug/kg 02/24/14 15:54 95-47-64.0 1
Surrogates
Toluene-d8 (S)111 %02/24/14 15:54 2037-26-570-130 1
4-Bromofluorobenzene (S)95 %02/24/14 15:54 460-00-470-130 1
1,2-Dichloroethane-d4 (S)84 %02/24/14 15:54 17060-07-070-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 32.8 %02/24/14 16:110.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 5
Lab ID:92190644005 Collected:02/20/14 11:47 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components ND mg/kg 02/22/14 15:56 68334-30-502/21/14 14:585.0 1
Surrogates
n-Pentacosane (S)77 %02/22/14 15:56 629-99-202/21/14 14:5841-119 1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 02/25/14 14:37 7440-38-202/25/14 10:250.70 1
Barium 94.1 mg/kg 02/25/14 14:37 7440-39-302/25/14 10:250.35 1
Cadmium ND mg/kg 02/25/14 14:37 7440-43-902/25/14 10:250.070 1
Chromium 5.0 mg/kg 02/25/14 14:37 7440-47-302/25/14 10:250.35 1
Lead 4.3 mg/kg 02/25/14 14:37 7439-92-102/25/14 10:250.35 1
Selenium ND mg/kg 02/25/14 14:37 7782-49-202/25/14 10:250.70 1
Silver ND mg/kg 02/25/14 14:37 7440-22-402/25/14 10:250.35 1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.0090 mg/kg 02/25/14 15:29 7439-97-602/24/14 22:450.0031 1
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 02/24/14 13:08 83-32-902/21/14 14:263301
Acenaphthylene ND ug/kg 02/24/14 13:08 208-96-802/21/14 14:263301
Anthracene ND ug/kg 02/24/14 13:08 120-12-702/21/14 14:263301
Benzo(a)anthracene ND ug/kg 02/24/14 13:08 56-55-302/21/14 14:263301
Benzo(a)pyrene ND ug/kg 02/24/14 13:08 50-32-802/21/14 14:263301
Benzo(b)fluoranthene ND ug/kg 02/24/14 13:08 205-99-202/21/14 14:263301
Benzo(g,h,i)perylene ND ug/kg 02/24/14 13:08 191-24-202/21/14 14:263301
Benzo(k)fluoranthene ND ug/kg 02/24/14 13:08 207-08-902/21/14 14:263301
Chrysene ND ug/kg 02/24/14 13:08 218-01-902/21/14 14:263301
Dibenz(a,h)anthracene ND ug/kg 02/24/14 13:08 53-70-302/21/14 14:263301
Fluoranthene ND ug/kg 02/24/14 13:08 206-44-002/21/14 14:263301
Fluorene ND ug/kg 02/24/14 13:08 86-73-702/21/14 14:263301
Indeno(1,2,3-cd)pyrene ND ug/kg 02/24/14 13:08 193-39-502/21/14 14:263301
1-Methylnaphthalene ND ug/kg 02/24/14 13:08 90-12-002/21/14 14:263301
2-Methylnaphthalene ND ug/kg 02/24/14 13:08 91-57-602/21/14 14:263301
Naphthalene ND ug/kg 02/24/14 13:08 91-20-302/21/14 14:263301
Phenanthrene ND ug/kg 02/24/14 13:08 85-01-802/21/14 14:263301
Pyrene ND ug/kg 02/24/14 13:08 129-00-002/21/14 14:263301
Surrogates
Nitrobenzene-d5 (S)67 %02/24/14 13:08 4165-60-002/21/14 14:2623-110 1
2-Fluorobiphenyl (S)72 %02/24/14 13:08 321-60-802/21/14 14:2630-110 1
Terphenyl-d14 (S)72 %02/24/14 13:08 1718-51-002/21/14 14:2628-110 1
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 02/24/14 16:14 67-64-198.2 1
Benzene ND ug/kg 02/24/14 16:14 71-43-24.9 1
Bromobenzene ND ug/kg 02/24/14 16:14 108-86-14.9 1
Bromochloromethane ND ug/kg 02/24/14 16:14 74-97-54.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 5
Lab ID:92190644005 Collected:02/20/14 11:47 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromodichloromethane ND ug/kg 02/24/14 16:14 75-27-44.9 1
Bromoform ND ug/kg 02/24/14 16:14 75-25-24.9 1
Bromomethane ND ug/kg 02/24/14 16:14 74-83-99.8 1
2-Butanone (MEK)ND ug/kg 02/24/14 16:14 78-93-398.2 1
n-Butylbenzene ND ug/kg 02/24/14 16:14 104-51-84.9 1
sec-Butylbenzene ND ug/kg 02/24/14 16:14 135-98-84.9 1
tert-Butylbenzene ND ug/kg 02/24/14 16:14 98-06-64.9 1
Carbon tetrachloride ND ug/kg 02/24/14 16:14 56-23-54.9 1
Chlorobenzene ND ug/kg 02/24/14 16:14 108-90-74.9 1
Chloroethane ND ug/kg 02/24/14 16:14 75-00-39.8 1
Chloroform ND ug/kg 02/24/14 16:14 67-66-34.9 1
Chloromethane ND ug/kg 02/24/14 16:14 74-87-39.8 1
2-Chlorotoluene ND ug/kg 02/24/14 16:14 95-49-84.9 1
4-Chlorotoluene ND ug/kg 02/24/14 16:14 106-43-44.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/24/14 16:14 96-12-84.9 1
Dibromochloromethane ND ug/kg 02/24/14 16:14 124-48-14.9 1
1,2-Dibromoethane (EDB)ND ug/kg 02/24/14 16:14 106-93-44.9 1
Dibromomethane ND ug/kg 02/24/14 16:14 74-95-34.9 1
1,2-Dichlorobenzene ND ug/kg 02/24/14 16:14 95-50-14.9 1
1,3-Dichlorobenzene ND ug/kg 02/24/14 16:14 541-73-14.9 1
1,4-Dichlorobenzene ND ug/kg 02/24/14 16:14 106-46-74.9 1
Dichlorodifluoromethane ND ug/kg 02/24/14 16:14 75-71-89.8 1
1,1-Dichloroethane ND ug/kg 02/24/14 16:14 75-34-34.9 1
1,2-Dichloroethane ND ug/kg 02/24/14 16:14 107-06-24.9 1
1,1-Dichloroethene ND ug/kg 02/24/14 16:14 75-35-44.9 1
cis-1,2-Dichloroethene ND ug/kg 02/24/14 16:14 156-59-24.9 1
trans-1,2-Dichloroethene ND ug/kg 02/24/14 16:14 156-60-54.9 1
1,2-Dichloropropane ND ug/kg 02/24/14 16:14 78-87-54.9 1
1,3-Dichloropropane ND ug/kg 02/24/14 16:14 142-28-94.9 1
2,2-Dichloropropane ND ug/kg 02/24/14 16:14 594-20-74.9 1
1,1-Dichloropropene ND ug/kg 02/24/14 16:14 563-58-64.9 1
cis-1,3-Dichloropropene ND ug/kg 02/24/14 16:14 10061-01-54.9 1
trans-1,3-Dichloropropene ND ug/kg 02/24/14 16:14 10061-02-64.9 1
Diisopropyl ether ND ug/kg 02/24/14 16:14 108-20-34.9 1
Ethylbenzene ND ug/kg 02/24/14 16:14 100-41-44.9 1
Hexachloro-1,3-butadiene ND ug/kg 02/24/14 16:14 87-68-34.9 1
2-Hexanone ND ug/kg 02/24/14 16:14 591-78-649.1 1
Isopropylbenzene (Cumene)ND ug/kg 02/24/14 16:14 98-82-84.9 1
p-Isopropyltoluene ND ug/kg 02/24/14 16:14 99-87-64.9 1
Methylene Chloride ND ug/kg 02/24/14 16:14 75-09-219.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/24/14 16:14 108-10-149.1 1
Methyl-tert-butyl ether ND ug/kg 02/24/14 16:14 1634-04-44.9 1
Naphthalene ND ug/kg 02/24/14 16:14 91-20-34.9 1
n-Propylbenzene ND ug/kg 02/24/14 16:14 103-65-14.9 1
Styrene ND ug/kg 02/24/14 16:14 100-42-54.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 5
Lab ID:92190644005 Collected:02/20/14 11:47 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 02/24/14 16:14 630-20-64.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/24/14 16:14 79-34-54.9 1
Tetrachloroethene ND ug/kg 02/24/14 16:14 127-18-44.9 1
Toluene ND ug/kg 02/24/14 16:14 108-88-34.9 1
1,2,3-Trichlorobenzene ND ug/kg 02/24/14 16:14 87-61-64.9 1
1,2,4-Trichlorobenzene ND ug/kg 02/24/14 16:14 120-82-14.9 1
1,1,1-Trichloroethane ND ug/kg 02/24/14 16:14 71-55-64.9 1
1,1,2-Trichloroethane ND ug/kg 02/24/14 16:14 79-00-54.9 1
Trichloroethene ND ug/kg 02/24/14 16:14 79-01-64.9 1
Trichlorofluoromethane ND ug/kg 02/24/14 16:14 75-69-44.9 1
1,2,3-Trichloropropane ND ug/kg 02/24/14 16:14 96-18-44.9 1
1,2,4-Trimethylbenzene ND ug/kg 02/24/14 16:14 95-63-64.9 1
1,3,5-Trimethylbenzene ND ug/kg 02/24/14 16:14 108-67-84.9 1
Vinyl acetate ND ug/kg 02/24/14 16:14 108-05-449.1 1
Vinyl chloride ND ug/kg 02/24/14 16:14 75-01-49.8 1
Xylene (Total)ND ug/kg 02/24/14 16:14 1330-20-79.8 1
m&p-Xylene ND ug/kg 02/24/14 16:14 179601-23-19.8 1
o-Xylene ND ug/kg 02/24/14 16:14 95-47-64.9 1
Surrogates
Toluene-d8 (S)109 %02/24/14 16:14 2037-26-570-130 1
4-Bromofluorobenzene (S)99 %02/24/14 16:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %02/24/14 16:14 17060-07-070-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 38.8 %02/24/14 16:110.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 6
Lab ID:92190644006 Collected:02/20/14 11:55 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 7.2 mg/kg 02/22/14 16:20 68334-30-502/21/14 14:585.0 1
Surrogates
n-Pentacosane (S)73 %02/22/14 16:20 629-99-202/21/14 14:5841-119 1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 02/25/14 14:40 7440-38-202/25/14 10:250.89 1
Barium 142 mg/kg 02/25/14 14:40 7440-39-302/25/14 10:250.45 1
Cadmium 0.12 mg/kg 02/25/14 14:40 7440-43-902/25/14 10:250.089 1
Chromium 27.2 mg/kg 02/25/14 14:40 7440-47-302/25/14 10:250.45 1
Lead 8.1 mg/kg 02/25/14 14:40 7439-92-102/25/14 10:250.45 1
Selenium ND mg/kg 02/25/14 14:40 7782-49-202/25/14 10:250.89 1
Silver ND mg/kg 02/25/14 14:40 7440-22-402/25/14 10:250.45 1
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 02/28/14 20:10
Arsenic ND mg/L 03/04/14 14:42 7440-38-203/03/14 17:100.050 1
Barium 0.92 mg/L 03/04/14 14:42 7440-39-303/03/14 17:100.25 1
Cadmium ND mg/L 03/04/14 14:42 7440-43-903/03/14 17:100.0050 1
Chromium ND mg/L 03/04/14 14:42 7440-47-303/03/14 17:100.025 1
Lead ND mg/L 03/04/14 14:42 7439-92-103/03/14 17:100.025 1
Selenium ND mg/L 03/04/14 14:42 7782-49-203/03/14 17:100.10 1
Silver ND mg/L 03/04/14 14:42 7440-22-403/03/14 17:100.025 1
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 02/28/14 20:10
Mercury ND ug/L 03/04/14 13:51 7439-97-603/03/14 18:000.20 1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.028 mg/kg 02/25/14 15:32 7439-97-602/24/14 22:450.0037 1
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 02/24/14 13:38 83-32-902/21/14 14:263301
Acenaphthylene ND ug/kg 02/24/14 13:38 208-96-802/21/14 14:263301
Anthracene ND ug/kg 02/24/14 13:38 120-12-702/21/14 14:263301
Benzo(a)anthracene ND ug/kg 02/24/14 13:38 56-55-302/21/14 14:263301
Benzo(a)pyrene ND ug/kg 02/24/14 13:38 50-32-802/21/14 14:263301
Benzo(b)fluoranthene ND ug/kg 02/24/14 13:38 205-99-202/21/14 14:263301
Benzo(g,h,i)perylene ND ug/kg 02/24/14 13:38 191-24-202/21/14 14:263301
Benzo(k)fluoranthene ND ug/kg 02/24/14 13:38 207-08-902/21/14 14:263301
Chrysene ND ug/kg 02/24/14 13:38 218-01-902/21/14 14:263301
Dibenz(a,h)anthracene ND ug/kg 02/24/14 13:38 53-70-302/21/14 14:263301
Fluoranthene ND ug/kg 02/24/14 13:38 206-44-002/21/14 14:263301
Fluorene ND ug/kg 02/24/14 13:38 86-73-702/21/14 14:263301
Indeno(1,2,3-cd)pyrene ND ug/kg 02/24/14 13:38 193-39-502/21/14 14:263301
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 6
Lab ID:92190644006 Collected:02/20/14 11:55 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
1-Methylnaphthalene ND ug/kg 02/24/14 13:38 90-12-002/21/14 14:263301
2-Methylnaphthalene ND ug/kg 02/24/14 13:38 91-57-602/21/14 14:263301
Naphthalene ND ug/kg 02/24/14 13:38 91-20-302/21/14 14:263301
Phenanthrene ND ug/kg 02/24/14 13:38 85-01-802/21/14 14:263301
Pyrene ND ug/kg 02/24/14 13:38 129-00-002/21/14 14:263301
Surrogates
Nitrobenzene-d5 (S)67 %02/24/14 13:38 4165-60-002/21/14 14:2623-110 1
2-Fluorobiphenyl (S)65 %02/24/14 13:38 321-60-802/21/14 14:2630-110 1
Terphenyl-d14 (S)69 %02/24/14 13:38 1718-51-002/21/14 14:2628-110 1
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 109 ug/kg 02/24/14 16:33 67-64-1 A+80.4 1
Benzene ND ug/kg 02/24/14 16:33 71-43-24.0 1
Bromobenzene ND ug/kg 02/24/14 16:33 108-86-14.0 1
Bromochloromethane ND ug/kg 02/24/14 16:33 74-97-54.0 1
Bromodichloromethane ND ug/kg 02/24/14 16:33 75-27-44.0 1
Bromoform ND ug/kg 02/24/14 16:33 75-25-24.0 1
Bromomethane ND ug/kg 02/24/14 16:33 74-83-98.0 1
2-Butanone (MEK)ND ug/kg 02/24/14 16:33 78-93-380.4 1
n-Butylbenzene ND ug/kg 02/24/14 16:33 104-51-84.0 1
sec-Butylbenzene ND ug/kg 02/24/14 16:33 135-98-84.0 1
tert-Butylbenzene ND ug/kg 02/24/14 16:33 98-06-64.0 1
Carbon tetrachloride ND ug/kg 02/24/14 16:33 56-23-54.0 1
Chlorobenzene ND ug/kg 02/24/14 16:33 108-90-74.0 1
Chloroethane ND ug/kg 02/24/14 16:33 75-00-38.0 1
Chloroform ND ug/kg 02/24/14 16:33 67-66-34.0 1
Chloromethane ND ug/kg 02/24/14 16:33 74-87-38.0 1
2-Chlorotoluene ND ug/kg 02/24/14 16:33 95-49-84.0 1
4-Chlorotoluene ND ug/kg 02/24/14 16:33 106-43-44.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/24/14 16:33 96-12-84.0 1
Dibromochloromethane ND ug/kg 02/24/14 16:33 124-48-14.0 1
1,2-Dibromoethane (EDB)ND ug/kg 02/24/14 16:33 106-93-44.0 1
Dibromomethane ND ug/kg 02/24/14 16:33 74-95-34.0 1
1,2-Dichlorobenzene ND ug/kg 02/24/14 16:33 95-50-14.0 1
1,3-Dichlorobenzene ND ug/kg 02/24/14 16:33 541-73-14.0 1
1,4-Dichlorobenzene ND ug/kg 02/24/14 16:33 106-46-74.0 1
Dichlorodifluoromethane ND ug/kg 02/24/14 16:33 75-71-88.0 1
1,1-Dichloroethane ND ug/kg 02/24/14 16:33 75-34-34.0 1
1,2-Dichloroethane ND ug/kg 02/24/14 16:33 107-06-24.0 1
1,1-Dichloroethene ND ug/kg 02/24/14 16:33 75-35-44.0 1
cis-1,2-Dichloroethene ND ug/kg 02/24/14 16:33 156-59-24.0 1
trans-1,2-Dichloroethene ND ug/kg 02/24/14 16:33 156-60-54.0 1
1,2-Dichloropropane ND ug/kg 02/24/14 16:33 78-87-54.0 1
1,3-Dichloropropane ND ug/kg 02/24/14 16:33 142-28-94.0 1
2,2-Dichloropropane ND ug/kg 02/24/14 16:33 594-20-74.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 6
Lab ID:92190644006 Collected:02/20/14 11:55 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/kg 02/24/14 16:33 563-58-64.0 1
cis-1,3-Dichloropropene ND ug/kg 02/24/14 16:33 10061-01-54.0 1
trans-1,3-Dichloropropene ND ug/kg 02/24/14 16:33 10061-02-64.0 1
Diisopropyl ether ND ug/kg 02/24/14 16:33 108-20-34.0 1
Ethylbenzene ND ug/kg 02/24/14 16:33 100-41-44.0 1
Hexachloro-1,3-butadiene ND ug/kg 02/24/14 16:33 87-68-34.0 1
2-Hexanone ND ug/kg 02/24/14 16:33 591-78-640.2 1
Isopropylbenzene (Cumene)ND ug/kg 02/24/14 16:33 98-82-84.0 1
p-Isopropyltoluene ND ug/kg 02/24/14 16:33 99-87-64.0 1
Methylene Chloride ND ug/kg 02/24/14 16:33 75-09-216.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/24/14 16:33 108-10-140.2 1
Methyl-tert-butyl ether ND ug/kg 02/24/14 16:33 1634-04-44.0 1
Naphthalene ND ug/kg 02/24/14 16:33 91-20-34.0 1
n-Propylbenzene ND ug/kg 02/24/14 16:33 103-65-14.0 1
Styrene ND ug/kg 02/24/14 16:33 100-42-54.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/24/14 16:33 630-20-64.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/24/14 16:33 79-34-54.0 1
Tetrachloroethene ND ug/kg 02/24/14 16:33 127-18-44.0 1
Toluene ND ug/kg 02/24/14 16:33 108-88-34.0 1
1,2,3-Trichlorobenzene ND ug/kg 02/24/14 16:33 87-61-64.0 1
1,2,4-Trichlorobenzene ND ug/kg 02/24/14 16:33 120-82-14.0 1
1,1,1-Trichloroethane ND ug/kg 02/24/14 16:33 71-55-64.0 1
1,1,2-Trichloroethane ND ug/kg 02/24/14 16:33 79-00-54.0 1
Trichloroethene ND ug/kg 02/24/14 16:33 79-01-64.0 1
Trichlorofluoromethane ND ug/kg 02/24/14 16:33 75-69-44.0 1
1,2,3-Trichloropropane ND ug/kg 02/24/14 16:33 96-18-44.0 1
1,2,4-Trimethylbenzene ND ug/kg 02/24/14 16:33 95-63-64.0 1
1,3,5-Trimethylbenzene ND ug/kg 02/24/14 16:33 108-67-84.0 1
Vinyl acetate ND ug/kg 02/24/14 16:33 108-05-440.2 1
Vinyl chloride ND ug/kg 02/24/14 16:33 75-01-48.0 1
Xylene (Total)ND ug/kg 02/24/14 16:33 1330-20-78.0 1
m&p-Xylene ND ug/kg 02/24/14 16:33 179601-23-18.0 1
o-Xylene ND ug/kg 02/24/14 16:33 95-47-64.0 1
Surrogates
Toluene-d8 (S)113 %02/24/14 16:33 2037-26-570-130 1
4-Bromofluorobenzene (S)90 %02/24/14 16:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %02/24/14 16:33 17060-07-070-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 27.0 %02/24/14 16:120.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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Page 23 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 7
Lab ID:92190644007 Collected:02/20/14 11:50 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components ND mg/kg 02/22/14 16:20 68334-30-502/21/14 14:585.0 1
Surrogates
n-Pentacosane (S)87 %02/22/14 16:20 629-99-202/21/14 14:5841-119 1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 02/25/14 14:56 7440-38-202/25/14 10:250.98 1
Barium 47.1 mg/kg 02/25/14 14:56 7440-39-302/25/14 10:250.49 1
Cadmium ND mg/kg 02/25/14 14:56 7440-43-902/25/14 10:250.098 1
Chromium 18.7 mg/kg 02/25/14 14:56 7440-47-302/25/14 10:250.49 1
Lead 4.8 mg/kg 02/25/14 14:56 7439-92-102/25/14 10:250.49 1
Selenium ND mg/kg 02/25/14 14:56 7782-49-202/25/14 10:250.98 1
Silver ND mg/kg 02/25/14 14:56 7440-22-402/25/14 10:250.49 1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.0077 mg/kg 02/25/14 15:34 7439-97-602/24/14 22:450.0033 1
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 02/24/14 14:09 83-32-902/21/14 14:263301
Acenaphthylene ND ug/kg 02/24/14 14:09 208-96-802/21/14 14:263301
Anthracene ND ug/kg 02/24/14 14:09 120-12-702/21/14 14:263301
Benzo(a)anthracene ND ug/kg 02/24/14 14:09 56-55-302/21/14 14:263301
Benzo(a)pyrene ND ug/kg 02/24/14 14:09 50-32-802/21/14 14:263301
Benzo(b)fluoranthene ND ug/kg 02/24/14 14:09 205-99-202/21/14 14:263301
Benzo(g,h,i)perylene ND ug/kg 02/24/14 14:09 191-24-202/21/14 14:263301
Benzo(k)fluoranthene ND ug/kg 02/24/14 14:09 207-08-902/21/14 14:263301
Chrysene ND ug/kg 02/24/14 14:09 218-01-902/21/14 14:263301
Dibenz(a,h)anthracene ND ug/kg 02/24/14 14:09 53-70-302/21/14 14:263301
Fluoranthene ND ug/kg 02/24/14 14:09 206-44-002/21/14 14:263301
Fluorene ND ug/kg 02/24/14 14:09 86-73-702/21/14 14:263301
Indeno(1,2,3-cd)pyrene ND ug/kg 02/24/14 14:09 193-39-502/21/14 14:263301
1-Methylnaphthalene ND ug/kg 02/24/14 14:09 90-12-002/21/14 14:263301
2-Methylnaphthalene ND ug/kg 02/24/14 14:09 91-57-602/21/14 14:263301
Naphthalene ND ug/kg 02/24/14 14:09 91-20-302/21/14 14:263301
Phenanthrene ND ug/kg 02/24/14 14:09 85-01-802/21/14 14:263301
Pyrene ND ug/kg 02/24/14 14:09 129-00-002/21/14 14:263301
Surrogates
Nitrobenzene-d5 (S)57 %02/24/14 14:09 4165-60-002/21/14 14:2623-110 1
2-Fluorobiphenyl (S)60 %02/24/14 14:09 321-60-802/21/14 14:2630-110 1
Terphenyl-d14 (S)63 %02/24/14 14:09 1718-51-002/21/14 14:2628-110 1
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 02/24/14 16:53 67-64-186.4 1
Benzene ND ug/kg 02/24/14 16:53 71-43-24.3 1
Bromobenzene ND ug/kg 02/24/14 16:53 108-86-14.3 1
Bromochloromethane ND ug/kg 02/24/14 16:53 74-97-54.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 7
Lab ID:92190644007 Collected:02/20/14 11:50 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromodichloromethane ND ug/kg 02/24/14 16:53 75-27-44.3 1
Bromoform ND ug/kg 02/24/14 16:53 75-25-24.3 1
Bromomethane ND ug/kg 02/24/14 16:53 74-83-98.6 1
2-Butanone (MEK)ND ug/kg 02/24/14 16:53 78-93-386.4 1
n-Butylbenzene ND ug/kg 02/24/14 16:53 104-51-84.3 1
sec-Butylbenzene ND ug/kg 02/24/14 16:53 135-98-84.3 1
tert-Butylbenzene ND ug/kg 02/24/14 16:53 98-06-64.3 1
Carbon tetrachloride ND ug/kg 02/24/14 16:53 56-23-54.3 1
Chlorobenzene ND ug/kg 02/24/14 16:53 108-90-74.3 1
Chloroethane ND ug/kg 02/24/14 16:53 75-00-38.6 1
Chloroform ND ug/kg 02/24/14 16:53 67-66-34.3 1
Chloromethane ND ug/kg 02/24/14 16:53 74-87-38.6 1
2-Chlorotoluene ND ug/kg 02/24/14 16:53 95-49-84.3 1
4-Chlorotoluene ND ug/kg 02/24/14 16:53 106-43-44.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/24/14 16:53 96-12-84.3 1
Dibromochloromethane ND ug/kg 02/24/14 16:53 124-48-14.3 1
1,2-Dibromoethane (EDB)ND ug/kg 02/24/14 16:53 106-93-44.3 1
Dibromomethane ND ug/kg 02/24/14 16:53 74-95-34.3 1
1,2-Dichlorobenzene ND ug/kg 02/24/14 16:53 95-50-14.3 1
1,3-Dichlorobenzene ND ug/kg 02/24/14 16:53 541-73-14.3 1
1,4-Dichlorobenzene ND ug/kg 02/24/14 16:53 106-46-74.3 1
Dichlorodifluoromethane ND ug/kg 02/24/14 16:53 75-71-88.6 1
1,1-Dichloroethane ND ug/kg 02/24/14 16:53 75-34-34.3 1
1,2-Dichloroethane ND ug/kg 02/24/14 16:53 107-06-24.3 1
1,1-Dichloroethene ND ug/kg 02/24/14 16:53 75-35-44.3 1
cis-1,2-Dichloroethene ND ug/kg 02/24/14 16:53 156-59-24.3 1
trans-1,2-Dichloroethene ND ug/kg 02/24/14 16:53 156-60-54.3 1
1,2-Dichloropropane ND ug/kg 02/24/14 16:53 78-87-54.3 1
1,3-Dichloropropane ND ug/kg 02/24/14 16:53 142-28-94.3 1
2,2-Dichloropropane ND ug/kg 02/24/14 16:53 594-20-74.3 1
1,1-Dichloropropene ND ug/kg 02/24/14 16:53 563-58-64.3 1
cis-1,3-Dichloropropene ND ug/kg 02/24/14 16:53 10061-01-54.3 1
trans-1,3-Dichloropropene ND ug/kg 02/24/14 16:53 10061-02-64.3 1
Diisopropyl ether ND ug/kg 02/24/14 16:53 108-20-34.3 1
Ethylbenzene ND ug/kg 02/24/14 16:53 100-41-44.3 1
Hexachloro-1,3-butadiene ND ug/kg 02/24/14 16:53 87-68-34.3 1
2-Hexanone ND ug/kg 02/24/14 16:53 591-78-643.2 1
Isopropylbenzene (Cumene)ND ug/kg 02/24/14 16:53 98-82-84.3 1
p-Isopropyltoluene ND ug/kg 02/24/14 16:53 99-87-64.3 1
Methylene Chloride ND ug/kg 02/24/14 16:53 75-09-217.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/24/14 16:53 108-10-143.2 1
Methyl-tert-butyl ether ND ug/kg 02/24/14 16:53 1634-04-44.3 1
Naphthalene ND ug/kg 02/24/14 16:53 91-20-34.3 1
n-Propylbenzene ND ug/kg 02/24/14 16:53 103-65-14.3 1
Styrene ND ug/kg 02/24/14 16:53 100-42-54.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 7
Lab ID:92190644007 Collected:02/20/14 11:50 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 02/24/14 16:53 630-20-64.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/24/14 16:53 79-34-54.3 1
Tetrachloroethene ND ug/kg 02/24/14 16:53 127-18-44.3 1
Toluene ND ug/kg 02/24/14 16:53 108-88-34.3 1
1,2,3-Trichlorobenzene ND ug/kg 02/24/14 16:53 87-61-64.3 1
1,2,4-Trichlorobenzene ND ug/kg 02/24/14 16:53 120-82-14.3 1
1,1,1-Trichloroethane ND ug/kg 02/24/14 16:53 71-55-64.3 1
1,1,2-Trichloroethane ND ug/kg 02/24/14 16:53 79-00-54.3 1
Trichloroethene ND ug/kg 02/24/14 16:53 79-01-64.3 1
Trichlorofluoromethane ND ug/kg 02/24/14 16:53 75-69-44.3 1
1,2,3-Trichloropropane ND ug/kg 02/24/14 16:53 96-18-44.3 1
1,2,4-Trimethylbenzene ND ug/kg 02/24/14 16:53 95-63-64.3 1
1,3,5-Trimethylbenzene ND ug/kg 02/24/14 16:53 108-67-84.3 1
Vinyl acetate ND ug/kg 02/24/14 16:53 108-05-443.2 1
Vinyl chloride ND ug/kg 02/24/14 16:53 75-01-48.6 1
Xylene (Total)ND ug/kg 02/24/14 16:53 1330-20-78.6 1
m&p-Xylene ND ug/kg 02/24/14 16:53 179601-23-18.6 1
o-Xylene ND ug/kg 02/24/14 16:53 95-47-64.3 1
Surrogates
Toluene-d8 (S)106 %02/24/14 16:53 2037-26-570-130 1
4-Bromofluorobenzene (S)98 %02/24/14 16:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %02/24/14 16:53 17060-07-070-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 24.3 %02/24/14 16:120.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/6263
EPA 7470
EPA 7470
7470 Mercury TCLP
Associated Lab Samples:92190644003, 92190644004, 92190644006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1149126
Associated Lab Samples:92190644003, 92190644004, 92190644006
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 03/04/14 13:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1149127LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.82.5 110 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1149128MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190644003
1149129
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L M1,R12.5 200 75-125112 552.5ND 5.1 2.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/6223
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1144175
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0050 02/25/14 14:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1144176LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.068.067 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1144177MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190644001
1144178
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/kg M1,R1.056 47 75-125281 82.0530.048 0.087 0.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/15295
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1143290
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Matrix:Solid
Analyzed
Arsenic mg/kg ND 1.0 02/25/14 14:12
Cadmium mg/kg ND 0.10 02/25/14 14:12
Chromium mg/kg ND 0.50 02/25/14 14:12
Lead mg/kg ND 0.50 02/25/14 14:12
Selenium mg/kg ND 1.0 02/25/14 14:12
Silver mg/kg ND 0.50 02/25/14 14:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1143291LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 50.150 100 80-120
Cadmium mg/kg 51.350 103 80-120
Chromium mg/kg 50.750 101 80-120
Lead mg/kg 51.050 102 80-120
Selenium mg/kg 51.050 102 80-120
Silver mg/kg 25.225 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1143292MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190644001
1143293
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic mg/kg 57.6 86 75-12587 760.8ND 49.8 53.2
Cadmium mg/kg 57.6 96 75-12597 660.80.11 55.3 58.8
Chromium mg/kg 57.6 103 75-12588 660.830.5 97.6 92.4
Lead mg/kg 57.6 89 75-12594 860.815.5 70.5 76.8
Selenium mg/kg 57.6 76 75-12578 860.8ND 43.8 47.7
Silver mg/kg 28.7 96 75-12596 530.4ND 27.8 29.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 29 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/15350
EPA 3010
EPA 6010
6010 MET TCLP
Associated Lab Samples:92190644003, 92190644004, 92190644006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1149132
Associated Lab Samples:92190644003, 92190644004, 92190644006
Matrix:Water
Analyzed
Arsenic mg/L ND 0.050 03/04/14 14:01
Barium mg/L ND 0.25 03/04/14 14:01
Cadmium mg/L ND 0.0050 03/04/14 14:01
Chromium mg/L ND 0.025 03/04/14 14:01
Lead mg/L ND 0.025 03/04/14 14:01
Selenium mg/L ND 0.10 03/04/14 14:01
Silver mg/L ND 0.025 03/04/14 14:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1149133LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/L 2.62.5 106 80-120
Barium mg/L 2.22.5 90 80-120
Cadmium mg/L 2.42.5 96 80-120
Chromium mg/L 2.52.5 98 80-120
Lead mg/L 2.32.5 93 80-120
Selenium mg/L 2.72.5 108 80-120
Silver mg/L 1.31.2 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1149134MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190644003
1149135
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic mg/L 2.5 108 75-125104 42.5ND 2.7 2.6
Barium mg/L 2.5 92 75-12588 32.50.82 3.1 3.0
Cadmium mg/L 2.5 98 75-12595 42.5ND 2.4 2.4
Chromium mg/L 2.5 100 75-12596 42.5ND 2.5 2.4
Lead mg/L 2.5 95 75-12592 42.50.064 2.4 2.4
Selenium mg/L 2.5 109 75-125106 32.5ND 2.7 2.7
Silver mg/L 1.2 102 75-125100 21.2ND 1.3 1.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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Page 30 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/25876
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1143872
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.2 02/24/14 14:34
1,1,1-Trichloroethane ug/kg ND 5.2 02/24/14 14:34
1,1,2,2-Tetrachloroethane ug/kg ND 5.2 02/24/14 14:34
1,1,2-Trichloroethane ug/kg ND 5.2 02/24/14 14:34
1,1-Dichloroethane ug/kg ND 5.2 02/24/14 14:34
1,1-Dichloroethene ug/kg ND 5.2 02/24/14 14:34
1,1-Dichloropropene ug/kg ND 5.2 02/24/14 14:34
1,2,3-Trichlorobenzene ug/kg ND 5.2 02/24/14 14:34
1,2,3-Trichloropropane ug/kg ND 5.2 02/24/14 14:34
1,2,4-Trichlorobenzene ug/kg ND 5.2 02/24/14 14:34
1,2,4-Trimethylbenzene ug/kg ND 5.2 02/24/14 14:34
1,2-Dibromo-3-chloropropane ug/kg ND 5.2 02/24/14 14:34
1,2-Dibromoethane (EDB)ug/kg ND 5.2 02/24/14 14:34
1,2-Dichlorobenzene ug/kg ND 5.2 02/24/14 14:34
1,2-Dichloroethane ug/kg ND 5.2 02/24/14 14:34
1,2-Dichloropropane ug/kg ND 5.2 02/24/14 14:34
1,3,5-Trimethylbenzene ug/kg ND 5.2 02/24/14 14:34
1,3-Dichlorobenzene ug/kg ND 5.2 02/24/14 14:34
1,3-Dichloropropane ug/kg ND 5.2 02/24/14 14:34
1,4-Dichlorobenzene ug/kg ND 5.2 02/24/14 14:34
2,2-Dichloropropane ug/kg ND 5.2 02/24/14 14:34
2-Butanone (MEK)ug/kg ND 104 02/24/14 14:34
2-Chlorotoluene ug/kg ND 5.2 02/24/14 14:34
2-Hexanone ug/kg ND 51.9 02/24/14 14:34
4-Chlorotoluene ug/kg ND 5.2 02/24/14 14:34
4-Methyl-2-pentanone (MIBK)ug/kg ND 51.9 02/24/14 14:34
Acetone ug/kg ND 104 02/24/14 14:34
Benzene ug/kg ND 5.2 02/24/14 14:34
Bromobenzene ug/kg ND 5.2 02/24/14 14:34
Bromochloromethane ug/kg ND 5.2 02/24/14 14:34
Bromodichloromethane ug/kg ND 5.2 02/24/14 14:34
Bromoform ug/kg ND 5.2 02/24/14 14:34
Bromomethane ug/kg ND 10.4 02/24/14 14:34
Carbon tetrachloride ug/kg ND 5.2 02/24/14 14:34
Chlorobenzene ug/kg ND 5.2 02/24/14 14:34
Chloroethane ug/kg ND 10.4 02/24/14 14:34
Chloroform ug/kg ND 5.2 02/24/14 14:34
Chloromethane ug/kg ND 10.4 02/24/14 14:34
cis-1,2-Dichloroethene ug/kg ND 5.2 02/24/14 14:34
cis-1,3-Dichloropropene ug/kg ND 5.2 02/24/14 14:34
Dibromochloromethane ug/kg ND 5.2 02/24/14 14:34
Dibromomethane ug/kg ND 5.2 02/24/14 14:34
Dichlorodifluoromethane ug/kg ND 10.4 02/24/14 14:34
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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Page 31 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1143872
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.2 02/24/14 14:34
Ethylbenzene ug/kg ND 5.2 02/24/14 14:34
Hexachloro-1,3-butadiene ug/kg ND 5.2 02/24/14 14:34
Isopropylbenzene (Cumene)ug/kg ND 5.2 02/24/14 14:34
m&p-Xylene ug/kg ND 10.4 02/24/14 14:34
Methyl-tert-butyl ether ug/kg ND 5.2 02/24/14 14:34
Methylene Chloride ug/kg ND 20.7 02/24/14 14:34
n-Butylbenzene ug/kg ND 5.2 02/24/14 14:34
n-Propylbenzene ug/kg ND 5.2 02/24/14 14:34
Naphthalene ug/kg ND 5.2 02/24/14 14:34
o-Xylene ug/kg ND 5.2 02/24/14 14:34
p-Isopropyltoluene ug/kg ND 5.2 02/24/14 14:34
sec-Butylbenzene ug/kg ND 5.2 02/24/14 14:34
Styrene ug/kg ND 5.2 02/24/14 14:34
tert-Butylbenzene ug/kg ND 5.2 02/24/14 14:34
Tetrachloroethene ug/kg ND 5.2 02/24/14 14:34
Toluene ug/kg ND 5.2 02/24/14 14:34
trans-1,2-Dichloroethene ug/kg ND 5.2 02/24/14 14:34
trans-1,3-Dichloropropene ug/kg ND 5.2 02/24/14 14:34
Trichloroethene ug/kg ND 5.2 02/24/14 14:34
Trichlorofluoromethane ug/kg ND 5.2 02/24/14 14:34
Vinyl acetate ug/kg ND 51.9 02/24/14 14:34
Vinyl chloride ug/kg ND 10.4 02/24/14 14:34
Xylene (Total)ug/kg ND 10.4 02/24/14 14:34
1,2-Dichloroethane-d4 (S)%91 70-132 02/24/14 14:34
4-Bromofluorobenzene (S)%96 70-130 02/24/14 14:34
Toluene-d8 (S)%111 70-130 02/24/14 14:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1143873LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 51.649.7 104 70-131
1,1,1-Trichloroethane ug/kg 61.049.7 123 70-141
1,1,2,2-Tetrachloroethane ug/kg 45.249.7 91 70-130
1,1,2-Trichloroethane ug/kg 57.549.7 116 70-132
1,1-Dichloroethane ug/kg 59.049.7 119 70-143
1,1-Dichloroethene ug/kg 61.049.7 123 70-137
1,1-Dichloropropene ug/kg 57.249.7 115 70-135
1,2,3-Trichlorobenzene ug/kg 51.949.7 104 69-153
1,2,3-Trichloropropane ug/kg 48.549.7 98 70-130
1,2,4-Trichlorobenzene ug/kg 46.849.7 94 55-171
1,2,4-Trimethylbenzene ug/kg 47.449.7 95 70-149
1,2-Dibromo-3-chloropropane ug/kg 51.749.7 104 68-141
1,2-Dibromoethane (EDB)ug/kg 53.049.7 107 70-130
1,2-Dichlorobenzene ug/kg 49.949.7 100 70-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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Page 32 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1143873LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane ug/kg 59.749.7 120 70-137
1,2-Dichloropropane ug/kg 55.249.7 111 70-133
1,3,5-Trimethylbenzene ug/kg 47.749.7 96 70-143
1,3-Dichlorobenzene ug/kg 47.349.7 95 70-144
1,3-Dichloropropane ug/kg 52.449.7 106 70-132
1,4-Dichlorobenzene ug/kg 48.649.7 98 70-142
2,2-Dichloropropane ug/kg 58.549.7 118 68-152
2-Butanone (MEK)ug/kg 11599.4 116 70-149
2-Chlorotoluene ug/kg 48.349.7 97 70-141
2-Hexanone ug/kg 93.299.4 94 70-149
4-Chlorotoluene ug/kg 49.549.7 100 70-149
4-Methyl-2-pentanone (MIBK)ug/kg 99.199.4 100 70-153
Acetone ug/kg 12399.4 124 70-157
Benzene ug/kg 56.149.7 113 70-130
Bromobenzene ug/kg 49.449.7 99 70-141
Bromochloromethane ug/kg 63.349.7 127 70-149
Bromodichloromethane ug/kg 55.749.7 112 70-130
Bromoform ug/kg 45.549.7 92 70-131
Bromomethane ug/kg 78.8 L349.7 159 64-136
Carbon tetrachloride ug/kg 52.849.7 106 70-154
Chlorobenzene ug/kg 48.849.7 98 70-135
Chloroethane ug/kg 62.749.7 126 68-151
Chloroform ug/kg 60.449.7 122 70-130
Chloromethane ug/kg 56.849.7 114 70-132
cis-1,2-Dichloroethene ug/kg 60.149.7 121 70-140
cis-1,3-Dichloropropene ug/kg 54.049.7 109 70-137
Dibromochloromethane ug/kg 47.849.7 96 70-130
Dibromomethane ug/kg 55.049.7 111 70-136
Dichlorodifluoromethane ug/kg 55.349.7 111 36-148
Diisopropyl ether ug/kg 56.549.7 114 70-139
Ethylbenzene ug/kg 48.849.7 98 70-137
Hexachloro-1,3-butadiene ug/kg 50.949.7 102 70-145
Isopropylbenzene (Cumene)ug/kg 50.749.7 102 70-141
m&p-Xylene ug/kg 99.699.4 100 70-140
Methyl-tert-butyl ether ug/kg 66.149.7 133 45-150
Methylene Chloride ug/kg 58.649.7 118 70-133
n-Butylbenzene ug/kg 47.049.7 95 65-155
n-Propylbenzene ug/kg 51.249.7 103 70-148
Naphthalene ug/kg 52.149.7 105 70-148
o-Xylene ug/kg 50.349.7 101 70-141
p-Isopropyltoluene ug/kg 49.749.7 100 70-148
sec-Butylbenzene ug/kg 51.049.7 103 70-145
Styrene ug/kg 51.249.7 103 70-138
tert-Butylbenzene ug/kg 52.249.7 105 70-143
Tetrachloroethene ug/kg 47.749.7 96 70-140
Toluene ug/kg 52.349.7 105 70-130
trans-1,2-Dichloroethene ug/kg 59.449.7 119 70-136
trans-1,3-Dichloropropene ug/kg 53.249.7 107 70-138
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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[phone]
Page 33 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1143873LABORATORY CONTROL SAMPLE:
LCSSpike
Trichloroethene ug/kg 55.249.7 111 70-132
Trichlorofluoromethane ug/kg 64.749.7 130 69-134
Vinyl acetate ug/kg 92.8 F399.4 93 24-161
Vinyl chloride ug/kg 61.349.7 123 55-140
Xylene (Total)ug/kg 150149 101 70-141
1,2-Dichloroethane-d4 (S)%115 70-132
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 34 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/26043
EPA 3546
EPA 8015 Modified
8015 Solid GCSV
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1142830
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Matrix:Solid
Analyzed
Diesel Components mg/kg ND 5.0 02/22/14 14:47
n-Pentacosane (S)%78 41-119 02/22/14 14:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1142831LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1142833
Diesel Components mg/kg 51.666.7 77 49-1137952.6 2 30
n-Pentacosane (S)%88 41-11973
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1143312MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190639002
1143313
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Diesel Components mg/kg 73.9 85 10-14647 2073.990.5 153 125
n-Pentacosane (S)%72 41-11961
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/26042
EPA 3546
EPA 8270
8270 Solid MSSV Microwave PAH
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1142828
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Matrix:Solid
Analyzed
1-Methylnaphthalene ug/kg ND 330 02/24/14 10:04
2-Methylnaphthalene ug/kg ND 330 02/24/14 10:04
Acenaphthene ug/kg ND 330 02/24/14 10:04
Acenaphthylene ug/kg ND 330 02/24/14 10:04
Anthracene ug/kg ND 330 02/24/14 10:04
Benzo(a)anthracene ug/kg ND 330 02/24/14 10:04
Benzo(a)pyrene ug/kg ND 330 02/24/14 10:04
Benzo(b)fluoranthene ug/kg ND 330 02/24/14 10:04
Benzo(g,h,i)perylene ug/kg ND 330 02/24/14 10:04
Benzo(k)fluoranthene ug/kg ND 330 02/24/14 10:04
Chrysene ug/kg ND 330 02/24/14 10:04
Dibenz(a,h)anthracene ug/kg ND 330 02/24/14 10:04
Fluoranthene ug/kg ND 330 02/24/14 10:04
Fluorene ug/kg ND 330 02/24/14 10:04
Indeno(1,2,3-cd)pyrene ug/kg ND 330 02/24/14 10:04
Naphthalene ug/kg ND 330 02/24/14 10:04
Phenanthrene ug/kg ND 330 02/24/14 10:04
Pyrene ug/kg ND 330 02/24/14 10:04
2-Fluorobiphenyl (S)%83 30-110 02/24/14 10:04
Nitrobenzene-d5 (S)%76 23-110 02/24/14 10:04
Terphenyl-d14 (S)%96 28-110 02/24/14 10:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1142829LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/kg 14501670 87 45-105
2-Methylnaphthalene ug/kg 15401670 92 39-112
Acenaphthene ug/kg 13201670 79 38-117
Acenaphthylene ug/kg 14001670 84 46-107
Anthracene ug/kg 14701670 88 50-110
Benzo(a)anthracene ug/kg 14001670 84 47-116
Benzo(a)pyrene ug/kg 15801670 95 47-106
Benzo(b)fluoranthene ug/kg 14201670 85 47-109
Benzo(g,h,i)perylene ug/kg 15501670 93 39-115
Benzo(k)fluoranthene ug/kg 13801670 83 45-117
Chrysene ug/kg 14901670 90 49-110
Dibenz(a,h)anthracene ug/kg 15901670 95 43-116
Fluoranthene ug/kg 15501670 93 50-114
Fluorene ug/kg 14001670 84 46-114
Indeno(1,2,3-cd)pyrene ug/kg 16101670 97 42-115
Naphthalene ug/kg 14101670 85 41-110
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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Page 36 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1142829LABORATORY CONTROL SAMPLE:
LCSSpike
Phenanthrene ug/kg 14301670 86 50-110
Pyrene ug/kg 14501670 87 45-114
2-Fluorobiphenyl (S)%83 30-110
Nitrobenzene-d5 (S)%79 23-110
Terphenyl-d14 (S)%94 28-110
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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[phone]
Page 37 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/6265
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Parameter Units
Dup
Result QualifiersRPDResult
92190479001
1143347SAMPLE DUPLICATE:
Percent Moisture %19.8 420.6
Parameter Units
Dup
Result QualifiersRPDResult
92190644009
1143348SAMPLE DUPLICATE:
Percent Moisture %32.2 131.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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[phone]
Page 38 of 42
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The reaction of the soil preservative, sodium bisulfate, is known to react with humic acid in soils to produce ketones.
Based upon method blank results, the laboratory feels the ketones in this sample are a result of that reaction.A+
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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[phone]
Page 39 of 42
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92190644001 OEXT/26043 GCSV/16735SOIL CUTTING PAD 1 STOCK 1 EPA 3546 EPA 8015 Modified
92190644002 OEXT/26043 GCSV/16735SOIL CUTTING PAD 1 STOCK 2 EPA 3546 EPA 8015 Modified
92190644003 OEXT/26043 GCSV/16735SOIL CUTTING PAD 1 STOCK 3 EPA 3546 EPA 8015 Modified
92190644004 OEXT/26043 GCSV/16735SOIL CUTTING PAD 1 STOCK 4 EPA 3546 EPA 8015 Modified
92190644005 OEXT/26043 GCSV/16735SOIL CUTTING PAD 1 STOCK 5 EPA 3546 EPA 8015 Modified
92190644006 OEXT/26043 GCSV/16735SOIL CUTTING PAD 1 STOCK 6 EPA 3546 EPA 8015 Modified
92190644007 OEXT/26043 GCSV/16735SOIL CUTTING PAD 1 STOCK 7 EPA 3546 EPA 8015 Modified
92190644001 MPRP/15295 ICP/13878SOIL CUTTING PAD 1 STOCK 1 EPA 3050 EPA 6010
92190644002 MPRP/15295 ICP/13878SOIL CUTTING PAD 1 STOCK 2 EPA 3050 EPA 6010
92190644003 MPRP/15295 ICP/13878SOIL CUTTING PAD 1 STOCK 3 EPA 3050 EPA 6010
92190644004 MPRP/15295 ICP/13878SOIL CUTTING PAD 1 STOCK 4 EPA 3050 EPA 6010
92190644005 MPRP/15295 ICP/13878SOIL CUTTING PAD 1 STOCK 5 EPA 3050 EPA 6010
92190644006 MPRP/15295 ICP/13878SOIL CUTTING PAD 1 STOCK 6 EPA 3050 EPA 6010
92190644007 MPRP/15295 ICP/13878SOIL CUTTING PAD 1 STOCK 7 EPA 3050 EPA 6010
92190644003 MPRP/15350 ICP/13923SOIL CUTTING PAD 1 STOCK 3 EPA 3010 EPA 6010
92190644004 MPRP/15350 ICP/13923SOIL CUTTING PAD 1 STOCK 4 EPA 3010 EPA 6010
92190644006 MPRP/15350 ICP/13923SOIL CUTTING PAD 1 STOCK 6 EPA 3010 EPA 6010
92190644003 MERP/6263 MERC/6038SOIL CUTTING PAD 1 STOCK 3 EPA 7470 EPA 7470
92190644004 MERP/6263 MERC/6038SOIL CUTTING PAD 1 STOCK 4 EPA 7470 EPA 7470
92190644006 MERP/6263 MERC/6038SOIL CUTTING PAD 1 STOCK 6 EPA 7470 EPA 7470
92190644001 MERP/6223 MERC/6000SOIL CUTTING PAD 1 STOCK 1 EPA 7471 EPA 7471
92190644002 MERP/6223 MERC/6000SOIL CUTTING PAD 1 STOCK 2 EPA 7471 EPA 7471
92190644003 MERP/6223 MERC/6000SOIL CUTTING PAD 1 STOCK 3 EPA 7471 EPA 7471
92190644004 MERP/6223 MERC/6000SOIL CUTTING PAD 1 STOCK 4 EPA 7471 EPA 7471
92190644005 MERP/6223 MERC/6000SOIL CUTTING PAD 1 STOCK 5 EPA 7471 EPA 7471
92190644006 MERP/6223 MERC/6000SOIL CUTTING PAD 1 STOCK 6 EPA 7471 EPA 7471
92190644007 MERP/6223 MERC/6000SOIL CUTTING PAD 1 STOCK 7 EPA 7471 EPA 7471
92190644001 OEXT/26042 MSSV/8774SOIL CUTTING PAD 1 STOCK 1 EPA 3546 EPA 8270
92190644002 OEXT/26042 MSSV/8774SOIL CUTTING PAD 1 STOCK 2 EPA 3546 EPA 8270
92190644003 OEXT/26042 MSSV/8774SOIL CUTTING PAD 1 STOCK 3 EPA 3546 EPA 8270
92190644004 OEXT/26042 MSSV/8774SOIL CUTTING PAD 1 STOCK 4 EPA 3546 EPA 8270
92190644005 OEXT/26042 MSSV/8774SOIL CUTTING PAD 1 STOCK 5 EPA 3546 EPA 8270
92190644006 OEXT/26042 MSSV/8774SOIL CUTTING PAD 1 STOCK 6 EPA 3546 EPA 8270
92190644007 OEXT/26042 MSSV/8774SOIL CUTTING PAD 1 STOCK 7 EPA 3546 EPA 8270
92190644001 MSV/25876SOIL CUTTING PAD 1 STOCK 1 EPA 8260
92190644002 MSV/25876SOIL CUTTING PAD 1 STOCK 2 EPA 8260
92190644003 MSV/25876SOIL CUTTING PAD 1 STOCK 3 EPA 8260
92190644004 MSV/25876SOIL CUTTING PAD 1 STOCK 4 EPA 8260
92190644005 MSV/25876SOIL CUTTING PAD 1 STOCK 5 EPA 8260
92190644006 MSV/25876SOIL CUTTING PAD 1 STOCK 6 EPA 8260
92190644007 MSV/25876SOIL CUTTING PAD 1 STOCK 7 EPA 8260
92190644001 PMST/6265SOIL CUTTING PAD 1 STOCK 1 ASTM D2974-87
92190644002 PMST/6265SOIL CUTTING PAD 1 STOCK 2 ASTM D2974-87
92190644003 PMST/6265SOIL CUTTING PAD 1 STOCK 3 ASTM D2974-87
92190644004 PMST/6265SOIL CUTTING PAD 1 STOCK 4 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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Page 40 of 42
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92190644005 PMST/6265SOIL CUTTING PAD 1 STOCK 5 ASTM D2974-87
92190644006 PMST/6265SOIL CUTTING PAD 1 STOCK 6 ASTM D2974-87
92190644007 PMST/6265SOIL CUTTING PAD 1 STOCK 7 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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Page 41 of 42
Page 42 of 42

APPENDIX 18

SOIL CUTTING STOCKPILE (PAD 1) LABORATORY REPORT
EMAIL
SOIL CUTTING STOCKPILE (VIBRO-PIER 159) LABORATORY
REPORT
#=CL#
March 04, 2014
LIMS USE: FR - JOHN BURKART
LIMS OBJECT ID: 92190644
92190644
Project:
Pace Project No.:
RE:
Mr. John Burkart
EFI Global
9307 Monroe Road
Suite M
Charlotte, NC 28270
CHARLOTTE CHEMICAL
Dear Mr. Burkart:
Enclosed are the analytical results for sample(s) received by the laboratory on February 21, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 1 of 42
#=CL#
March 04, 2014
Page 2
LIMS USE: FR - JOHN BURKART
LIMS OBJECT ID: 92190644
cc:Accounts Payable, EFI Global
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
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Page 2 of 42
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 3 of 42
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92190644001 SOIL CUTTING PAD 1 STOCK 1 EPA 8015 Modified 2 PASI-CNU1
EPA 6010 7 PASI-AJMW
EPA 7471 1 PASI-AMTS
EPA 8270 21 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CLLW
92190644002 SOIL CUTTING PAD 1 STOCK 2 EPA 8015 Modified 2 PASI-CNU1
EPA 6010 7 PASI-AJMW
EPA 7471 1 PASI-AMTS
EPA 8270 21 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CLLW
92190644003 SOIL CUTTING PAD 1 STOCK 3 EPA 8015 Modified 2 PASI-CNU1
EPA 6010 7 PASI-AJMW
EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASH1
EPA 7471 1 PASI-AMTS
EPA 8270 21 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CLLW
92190644004 SOIL CUTTING PAD 1 STOCK 4 EPA 8015 Modified 2 PASI-CNU1
EPA 6010 7 PASI-AJMW
EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASH1
EPA 7471 1 PASI-AMTS
EPA 8270 21 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CLLW
92190644005 SOIL CUTTING PAD 1 STOCK 5 EPA 8015 Modified 2 PASI-CNU1
EPA 6010 7 PASI-AJMW
EPA 7471 1 PASI-AMTS
EPA 8270 21 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CLLW
92190644006 SOIL CUTTING PAD 1 STOCK 6 EPA 8015 Modified 2 PASI-CNU1
EPA 6010 7 PASI-AJMW
EPA 6010 7 PASI-AJMW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Page 4 of 42
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7470 1 PASI-ASH1
EPA 7471 1 PASI-AMTS
EPA 8270 21 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CLLW
92190644007 SOIL CUTTING PAD 1 STOCK 7 EPA 8015 Modified 2 PASI-CNU1
EPA 6010 7 PASI-AJMW
EPA 7471 1 PASI-AMTS
EPA 8270 21 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CLLW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Page 5 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 1
Lab ID:92190644001 Collected:02/20/14 11:30 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 7.6 mg/kg 02/24/14 10:07 68334-30-502/21/14 14:585.0 1
Surrogates
n-Pentacosane (S)83 %02/24/14 10:07 629-99-202/21/14 14:5841-119 1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 02/25/14 14:18 7440-38-202/25/14 10:250.98 1
Barium 88.0 mg/kg 02/25/14 14:18 7440-39-302/25/14 10:250.49 1
Cadmium 0.11 mg/kg 02/25/14 14:18 7440-43-902/25/14 10:250.098 1
Chromium 30.5 mg/kg 02/25/14 14:18 7440-47-302/25/14 10:250.49 1
Lead 15.5 mg/kg 02/25/14 14:18 7439-92-102/25/14 10:250.49 1
Selenium ND mg/kg 02/25/14 14:18 7782-49-202/25/14 10:250.98 1
Silver ND mg/kg 02/25/14 14:18 7440-22-402/25/14 10:250.49 1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.048 mg/kg 02/25/14 14:57 7439-97-6 M1,R102/24/14 22:450.0036 1
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 02/24/14 11:05 83-32-902/21/14 14:263301
Acenaphthylene ND ug/kg 02/24/14 11:05 208-96-802/21/14 14:263301
Anthracene ND ug/kg 02/24/14 11:05 120-12-702/21/14 14:263301
Benzo(a)anthracene ND ug/kg 02/24/14 11:05 56-55-302/21/14 14:263301
Benzo(a)pyrene ND ug/kg 02/24/14 11:05 50-32-802/21/14 14:263301
Benzo(b)fluoranthene ND ug/kg 02/24/14 11:05 205-99-202/21/14 14:263301
Benzo(g,h,i)perylene ND ug/kg 02/24/14 11:05 191-24-202/21/14 14:263301
Benzo(k)fluoranthene ND ug/kg 02/24/14 11:05 207-08-902/21/14 14:263301
Chrysene ND ug/kg 02/24/14 11:05 218-01-902/21/14 14:263301
Dibenz(a,h)anthracene ND ug/kg 02/24/14 11:05 53-70-302/21/14 14:263301
Fluoranthene ND ug/kg 02/24/14 11:05 206-44-002/21/14 14:263301
Fluorene ND ug/kg 02/24/14 11:05 86-73-702/21/14 14:263301
Indeno(1,2,3-cd)pyrene ND ug/kg 02/24/14 11:05 193-39-502/21/14 14:263301
1-Methylnaphthalene ND ug/kg 02/24/14 11:05 90-12-002/21/14 14:263301
2-Methylnaphthalene ND ug/kg 02/24/14 11:05 91-57-602/21/14 14:263301
Naphthalene ND ug/kg 02/24/14 11:05 91-20-302/21/14 14:263301
Phenanthrene ND ug/kg 02/24/14 11:05 85-01-802/21/14 14:263301
Pyrene ND ug/kg 02/24/14 11:05 129-00-002/21/14 14:263301
Surrogates
Nitrobenzene-d5 (S)69 %02/24/14 11:05 4165-60-002/21/14 14:2623-110 1
2-Fluorobiphenyl (S)69 %02/24/14 11:05 321-60-802/21/14 14:2630-110 1
Terphenyl-d14 (S)81 %02/24/14 11:05 1718-51-002/21/14 14:2628-110 1
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 02/24/14 14:54 67-64-11081
Benzene ND ug/kg 02/24/14 14:54 71-43-25.4 1
Bromobenzene ND ug/kg 02/24/14 14:54 108-86-15.4 1
Bromochloromethane ND ug/kg 02/24/14 14:54 74-97-55.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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Huntersville, NC 28078
[phone]
Page 6 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 1
Lab ID:92190644001 Collected:02/20/14 11:30 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromodichloromethane ND ug/kg 02/24/14 14:54 75-27-45.4 1
Bromoform ND ug/kg 02/24/14 14:54 75-25-25.4 1
Bromomethane ND ug/kg 02/24/14 14:54 74-83-910.8 1
2-Butanone (MEK)ND ug/kg 02/24/14 14:54 78-93-31081
n-Butylbenzene ND ug/kg 02/24/14 14:54 104-51-85.4 1
sec-Butylbenzene ND ug/kg 02/24/14 14:54 135-98-85.4 1
tert-Butylbenzene ND ug/kg 02/24/14 14:54 98-06-65.4 1
Carbon tetrachloride ND ug/kg 02/24/14 14:54 56-23-55.4 1
Chlorobenzene ND ug/kg 02/24/14 14:54 108-90-75.4 1
Chloroethane ND ug/kg 02/24/14 14:54 75-00-310.8 1
Chloroform ND ug/kg 02/24/14 14:54 67-66-35.4 1
Chloromethane ND ug/kg 02/24/14 14:54 74-87-310.8 1
2-Chlorotoluene ND ug/kg 02/24/14 14:54 95-49-85.4 1
4-Chlorotoluene ND ug/kg 02/24/14 14:54 106-43-45.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/24/14 14:54 96-12-85.4 1
Dibromochloromethane ND ug/kg 02/24/14 14:54 124-48-15.4 1
1,2-Dibromoethane (EDB)ND ug/kg 02/24/14 14:54 106-93-45.4 1
Dibromomethane ND ug/kg 02/24/14 14:54 74-95-35.4 1
1,2-Dichlorobenzene ND ug/kg 02/24/14 14:54 95-50-15.4 1
1,3-Dichlorobenzene ND ug/kg 02/24/14 14:54 541-73-15.4 1
1,4-Dichlorobenzene ND ug/kg 02/24/14 14:54 106-46-75.4 1
Dichlorodifluoromethane ND ug/kg 02/24/14 14:54 75-71-810.8 1
1,1-Dichloroethane ND ug/kg 02/24/14 14:54 75-34-35.4 1
1,2-Dichloroethane ND ug/kg 02/24/14 14:54 107-06-25.4 1
1,1-Dichloroethene ND ug/kg 02/24/14 14:54 75-35-45.4 1
cis-1,2-Dichloroethene ND ug/kg 02/24/14 14:54 156-59-25.4 1
trans-1,2-Dichloroethene ND ug/kg 02/24/14 14:54 156-60-55.4 1
1,2-Dichloropropane ND ug/kg 02/24/14 14:54 78-87-55.4 1
1,3-Dichloropropane ND ug/kg 02/24/14 14:54 142-28-95.4 1
2,2-Dichloropropane ND ug/kg 02/24/14 14:54 594-20-75.4 1
1,1-Dichloropropene ND ug/kg 02/24/14 14:54 563-58-65.4 1
cis-1,3-Dichloropropene ND ug/kg 02/24/14 14:54 10061-01-55.4 1
trans-1,3-Dichloropropene ND ug/kg 02/24/14 14:54 10061-02-65.4 1
Diisopropyl ether ND ug/kg 02/24/14 14:54 108-20-35.4 1
Ethylbenzene ND ug/kg 02/24/14 14:54 100-41-45.4 1
Hexachloro-1,3-butadiene ND ug/kg 02/24/14 14:54 87-68-35.4 1
2-Hexanone ND ug/kg 02/24/14 14:54 591-78-654.2 1
Isopropylbenzene (Cumene)ND ug/kg 02/24/14 14:54 98-82-85.4 1
p-Isopropyltoluene ND ug/kg 02/24/14 14:54 99-87-65.4 1
Methylene Chloride ND ug/kg 02/24/14 14:54 75-09-221.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/24/14 14:54 108-10-154.2 1
Methyl-tert-butyl ether ND ug/kg 02/24/14 14:54 1634-04-45.4 1
Naphthalene ND ug/kg 02/24/14 14:54 91-20-35.4 1
n-Propylbenzene ND ug/kg 02/24/14 14:54 103-65-15.4 1
Styrene ND ug/kg 02/24/14 14:54 100-42-55.4 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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Page 7 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 1
Lab ID:92190644001 Collected:02/20/14 11:30 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 02/24/14 14:54 630-20-65.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/24/14 14:54 79-34-55.4 1
Tetrachloroethene ND ug/kg 02/24/14 14:54 127-18-45.4 1
Toluene ND ug/kg 02/24/14 14:54 108-88-35.4 1
1,2,3-Trichlorobenzene ND ug/kg 02/24/14 14:54 87-61-65.4 1
1,2,4-Trichlorobenzene ND ug/kg 02/24/14 14:54 120-82-15.4 1
1,1,1-Trichloroethane ND ug/kg 02/24/14 14:54 71-55-65.4 1
1,1,2-Trichloroethane ND ug/kg 02/24/14 14:54 79-00-55.4 1
Trichloroethene ND ug/kg 02/24/14 14:54 79-01-65.4 1
Trichlorofluoromethane ND ug/kg 02/24/14 14:54 75-69-45.4 1
1,2,3-Trichloropropane ND ug/kg 02/24/14 14:54 96-18-45.4 1
1,2,4-Trimethylbenzene ND ug/kg 02/24/14 14:54 95-63-65.4 1
1,3,5-Trimethylbenzene ND ug/kg 02/24/14 14:54 108-67-85.4 1
Vinyl acetate ND ug/kg 02/24/14 14:54 108-05-454.2 1
Vinyl chloride ND ug/kg 02/24/14 14:54 75-01-410.8 1
Xylene (Total)ND ug/kg 02/24/14 14:54 1330-20-710.8 1
m&p-Xylene ND ug/kg 02/24/14 14:54 179601-23-110.8 1
o-Xylene ND ug/kg 02/24/14 14:54 95-47-65.4 1
Surrogates
Toluene-d8 (S)109 %02/24/14 14:54 2037-26-570-130 1
4-Bromofluorobenzene (S)94 %02/24/14 14:54 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %02/24/14 14:54 17060-07-070-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 20.9 %02/24/14 16:110.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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Page 8 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 2
Lab ID:92190644002 Collected:02/20/14 11:35 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 167 mg/kg 02/22/14 15:33 68334-30-502/21/14 14:585.0 1
Surrogates
n-Pentacosane (S)79 %02/22/14 15:33 629-99-202/21/14 14:5841-119 1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 02/25/14 14:27 7440-38-202/25/14 10:250.76 1
Barium 95.5 mg/kg 02/25/14 14:27 7440-39-302/25/14 10:250.38 1
Cadmium ND mg/kg 02/25/14 14:27 7440-43-902/25/14 10:250.076 1
Chromium 17.0 mg/kg 02/25/14 14:27 7440-47-302/25/14 10:250.38 1
Lead 16.7 mg/kg 02/25/14 14:27 7439-92-102/25/14 10:250.38 1
Selenium ND mg/kg 02/25/14 14:27 7782-49-202/25/14 10:250.76 1
Silver ND mg/kg 02/25/14 14:27 7440-22-402/25/14 10:250.38 1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.052 mg/kg 02/25/14 15:10 7439-97-602/24/14 22:450.0042 1
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 02/24/14 11:36 83-32-902/21/14 14:263301
Acenaphthylene ND ug/kg 02/24/14 11:36 208-96-802/21/14 14:263301
Anthracene ND ug/kg 02/24/14 11:36 120-12-702/21/14 14:263301
Benzo(a)anthracene ND ug/kg 02/24/14 11:36 56-55-302/21/14 14:263301
Benzo(a)pyrene ND ug/kg 02/24/14 11:36 50-32-802/21/14 14:263301
Benzo(b)fluoranthene ND ug/kg 02/24/14 11:36 205-99-202/21/14 14:263301
Benzo(g,h,i)perylene ND ug/kg 02/24/14 11:36 191-24-202/21/14 14:263301
Benzo(k)fluoranthene ND ug/kg 02/24/14 11:36 207-08-902/21/14 14:263301
Chrysene ND ug/kg 02/24/14 11:36 218-01-902/21/14 14:263301
Dibenz(a,h)anthracene ND ug/kg 02/24/14 11:36 53-70-302/21/14 14:263301
Fluoranthene ND ug/kg 02/24/14 11:36 206-44-002/21/14 14:263301
Fluorene ND ug/kg 02/24/14 11:36 86-73-702/21/14 14:263301
Indeno(1,2,3-cd)pyrene ND ug/kg 02/24/14 11:36 193-39-502/21/14 14:263301
1-Methylnaphthalene ND ug/kg 02/24/14 11:36 90-12-002/21/14 14:263301
2-Methylnaphthalene ND ug/kg 02/24/14 11:36 91-57-602/21/14 14:263301
Naphthalene ND ug/kg 02/24/14 11:36 91-20-302/21/14 14:263301
Phenanthrene ND ug/kg 02/24/14 11:36 85-01-802/21/14 14:263301
Pyrene ND ug/kg 02/24/14 11:36 129-00-002/21/14 14:263301
Surrogates
Nitrobenzene-d5 (S)70 %02/24/14 11:36 4165-60-002/21/14 14:2623-110 1
2-Fluorobiphenyl (S)75 %02/24/14 11:36 321-60-802/21/14 14:2630-110 1
Terphenyl-d14 (S)89 %02/24/14 11:36 1718-51-002/21/14 14:2628-110 1
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 209 ug/kg 02/24/14 15:14 67-64-1 A+95.2 1
Benzene ND ug/kg 02/24/14 15:14 71-43-24.8 1
Bromobenzene ND ug/kg 02/24/14 15:14 108-86-14.8 1
Bromochloromethane ND ug/kg 02/24/14 15:14 74-97-54.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 2
Lab ID:92190644002 Collected:02/20/14 11:35 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromodichloromethane ND ug/kg 02/24/14 15:14 75-27-44.8 1
Bromoform ND ug/kg 02/24/14 15:14 75-25-24.8 1
Bromomethane ND ug/kg 02/24/14 15:14 74-83-99.5 1
2-Butanone (MEK)ND ug/kg 02/24/14 15:14 78-93-395.2 1
n-Butylbenzene ND ug/kg 02/24/14 15:14 104-51-84.8 1
sec-Butylbenzene ND ug/kg 02/24/14 15:14 135-98-84.8 1
tert-Butylbenzene ND ug/kg 02/24/14 15:14 98-06-64.8 1
Carbon tetrachloride ND ug/kg 02/24/14 15:14 56-23-54.8 1
Chlorobenzene ND ug/kg 02/24/14 15:14 108-90-74.8 1
Chloroethane ND ug/kg 02/24/14 15:14 75-00-39.5 1
Chloroform ND ug/kg 02/24/14 15:14 67-66-34.8 1
Chloromethane ND ug/kg 02/24/14 15:14 74-87-39.5 1
2-Chlorotoluene ND ug/kg 02/24/14 15:14 95-49-84.8 1
4-Chlorotoluene ND ug/kg 02/24/14 15:14 106-43-44.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/24/14 15:14 96-12-84.8 1
Dibromochloromethane ND ug/kg 02/24/14 15:14 124-48-14.8 1
1,2-Dibromoethane (EDB)ND ug/kg 02/24/14 15:14 106-93-44.8 1
Dibromomethane ND ug/kg 02/24/14 15:14 74-95-34.8 1
1,2-Dichlorobenzene ND ug/kg 02/24/14 15:14 95-50-14.8 1
1,3-Dichlorobenzene ND ug/kg 02/24/14 15:14 541-73-14.8 1
1,4-Dichlorobenzene ND ug/kg 02/24/14 15:14 106-46-74.8 1
Dichlorodifluoromethane ND ug/kg 02/24/14 15:14 75-71-89.5 1
1,1-Dichloroethane ND ug/kg 02/24/14 15:14 75-34-34.8 1
1,2-Dichloroethane ND ug/kg 02/24/14 15:14 107-06-24.8 1
1,1-Dichloroethene ND ug/kg 02/24/14 15:14 75-35-44.8 1
cis-1,2-Dichloroethene ND ug/kg 02/24/14 15:14 156-59-24.8 1
trans-1,2-Dichloroethene ND ug/kg 02/24/14 15:14 156-60-54.8 1
1,2-Dichloropropane ND ug/kg 02/24/14 15:14 78-87-54.8 1
1,3-Dichloropropane ND ug/kg 02/24/14 15:14 142-28-94.8 1
2,2-Dichloropropane ND ug/kg 02/24/14 15:14 594-20-74.8 1
1,1-Dichloropropene ND ug/kg 02/24/14 15:14 563-58-64.8 1
cis-1,3-Dichloropropene ND ug/kg 02/24/14 15:14 10061-01-54.8 1
trans-1,3-Dichloropropene ND ug/kg 02/24/14 15:14 10061-02-64.8 1
Diisopropyl ether ND ug/kg 02/24/14 15:14 108-20-34.8 1
Ethylbenzene ND ug/kg 02/24/14 15:14 100-41-44.8 1
Hexachloro-1,3-butadiene ND ug/kg 02/24/14 15:14 87-68-34.8 1
2-Hexanone ND ug/kg 02/24/14 15:14 591-78-647.6 1
Isopropylbenzene (Cumene)ND ug/kg 02/24/14 15:14 98-82-84.8 1
p-Isopropyltoluene ND ug/kg 02/24/14 15:14 99-87-64.8 1
Methylene Chloride ND ug/kg 02/24/14 15:14 75-09-219.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/24/14 15:14 108-10-147.6 1
Methyl-tert-butyl ether ND ug/kg 02/24/14 15:14 1634-04-44.8 1
Naphthalene ND ug/kg 02/24/14 15:14 91-20-34.8 1
n-Propylbenzene ND ug/kg 02/24/14 15:14 103-65-14.8 1
Styrene ND ug/kg 02/24/14 15:14 100-42-54.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 2
Lab ID:92190644002 Collected:02/20/14 11:35 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 02/24/14 15:14 630-20-64.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/24/14 15:14 79-34-54.8 1
Tetrachloroethene ND ug/kg 02/24/14 15:14 127-18-44.8 1
Toluene ND ug/kg 02/24/14 15:14 108-88-34.8 1
1,2,3-Trichlorobenzene ND ug/kg 02/24/14 15:14 87-61-64.8 1
1,2,4-Trichlorobenzene ND ug/kg 02/24/14 15:14 120-82-14.8 1
1,1,1-Trichloroethane ND ug/kg 02/24/14 15:14 71-55-64.8 1
1,1,2-Trichloroethane ND ug/kg 02/24/14 15:14 79-00-54.8 1
Trichloroethene ND ug/kg 02/24/14 15:14 79-01-64.8 1
Trichlorofluoromethane ND ug/kg 02/24/14 15:14 75-69-44.8 1
1,2,3-Trichloropropane ND ug/kg 02/24/14 15:14 96-18-44.8 1
1,2,4-Trimethylbenzene ND ug/kg 02/24/14 15:14 95-63-64.8 1
1,3,5-Trimethylbenzene ND ug/kg 02/24/14 15:14 108-67-84.8 1
Vinyl acetate ND ug/kg 02/24/14 15:14 108-05-447.6 1
Vinyl chloride ND ug/kg 02/24/14 15:14 75-01-49.5 1
Xylene (Total)ND ug/kg 02/24/14 15:14 1330-20-79.5 1
m&p-Xylene ND ug/kg 02/24/14 15:14 179601-23-19.5 1
o-Xylene ND ug/kg 02/24/14 15:14 95-47-64.8 1
Surrogates
Toluene-d8 (S)112 %02/24/14 15:14 2037-26-570-130 1
4-Bromofluorobenzene (S)93 %02/24/14 15:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %02/24/14 15:14 17060-07-070-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 15.8 %02/24/14 16:110.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 3
Lab ID:92190644003 Collected:02/20/14 11:40 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 13.7 mg/kg 02/22/14 15:33 68334-30-502/21/14 14:585.0 1
Surrogates
n-Pentacosane (S)93 %02/22/14 15:33 629-99-202/21/14 14:5841-119 1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 02/25/14 14:30 7440-38-202/25/14 10:250.78 1
Barium 204 mg/kg 02/25/14 14:30 7440-39-302/25/14 10:250.39 1
Cadmium 0.17 mg/kg 02/25/14 14:30 7440-43-902/25/14 10:250.078 1
Chromium 21.4 mg/kg 02/25/14 14:30 7440-47-302/25/14 10:250.39 1
Lead 25.9 mg/kg 02/25/14 14:30 7439-92-102/25/14 10:250.39 1
Selenium ND mg/kg 02/25/14 14:30 7782-49-202/25/14 10:250.78 1
Silver ND mg/kg 02/25/14 14:30 7440-22-402/25/14 10:250.39 1
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 02/28/14 20:10
Arsenic ND mg/L 03/04/14 14:21 7440-38-203/03/14 17:100.050 1
Barium 0.82 mg/L 03/04/14 14:21 7440-39-303/03/14 17:100.25 1
Cadmium ND mg/L 03/04/14 14:21 7440-43-903/03/14 17:100.0050 1
Chromium ND mg/L 03/04/14 14:21 7440-47-303/03/14 17:100.025 1
Lead 0.064 mg/L 03/04/14 14:21 7439-92-103/03/14 17:100.025 1
Selenium ND mg/L 03/04/14 14:21 7782-49-203/03/14 17:100.10 1
Silver ND mg/L 03/04/14 14:21 7440-22-403/03/14 17:100.025 1
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 02/28/14 20:10
Mercury ND ug/L 03/04/14 13:41 7439-97-6 M1,R103/03/14 18:000.20 1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.16 mg/kg 02/25/14 15:18 7439-97-602/24/14 22:450.018 5
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 02/24/14 12:07 83-32-902/21/14 14:263301
Acenaphthylene ND ug/kg 02/24/14 12:07 208-96-802/21/14 14:263301
Anthracene ND ug/kg 02/24/14 12:07 120-12-702/21/14 14:263301
Benzo(a)anthracene ND ug/kg 02/24/14 12:07 56-55-302/21/14 14:263301
Benzo(a)pyrene ND ug/kg 02/24/14 12:07 50-32-802/21/14 14:263301
Benzo(b)fluoranthene ND ug/kg 02/24/14 12:07 205-99-202/21/14 14:263301
Benzo(g,h,i)perylene ND ug/kg 02/24/14 12:07 191-24-202/21/14 14:263301
Benzo(k)fluoranthene ND ug/kg 02/24/14 12:07 207-08-902/21/14 14:263301
Chrysene ND ug/kg 02/24/14 12:07 218-01-902/21/14 14:263301
Dibenz(a,h)anthracene ND ug/kg 02/24/14 12:07 53-70-302/21/14 14:263301
Fluoranthene ND ug/kg 02/24/14 12:07 206-44-002/21/14 14:263301
Fluorene ND ug/kg 02/24/14 12:07 86-73-702/21/14 14:263301
Indeno(1,2,3-cd)pyrene ND ug/kg 02/24/14 12:07 193-39-502/21/14 14:263301
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 3
Lab ID:92190644003 Collected:02/20/14 11:40 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
1-Methylnaphthalene ND ug/kg 02/24/14 12:07 90-12-002/21/14 14:263301
2-Methylnaphthalene ND ug/kg 02/24/14 12:07 91-57-602/21/14 14:263301
Naphthalene ND ug/kg 02/24/14 12:07 91-20-302/21/14 14:263301
Phenanthrene ND ug/kg 02/24/14 12:07 85-01-802/21/14 14:263301
Pyrene ND ug/kg 02/24/14 12:07 129-00-002/21/14 14:263301
Surrogates
Nitrobenzene-d5 (S)59 %02/24/14 12:07 4165-60-002/21/14 14:2623-110 1
2-Fluorobiphenyl (S)61 %02/24/14 12:07 321-60-802/21/14 14:2630-110 1
Terphenyl-d14 (S)69 %02/24/14 12:07 1718-51-002/21/14 14:2628-110 1
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 02/24/14 15:34 67-64-170.4 1
Benzene ND ug/kg 02/24/14 15:34 71-43-23.5 1
Bromobenzene ND ug/kg 02/24/14 15:34 108-86-13.5 1
Bromochloromethane ND ug/kg 02/24/14 15:34 74-97-53.5 1
Bromodichloromethane ND ug/kg 02/24/14 15:34 75-27-43.5 1
Bromoform ND ug/kg 02/24/14 15:34 75-25-23.5 1
Bromomethane ND ug/kg 02/24/14 15:34 74-83-97.0 1
2-Butanone (MEK)ND ug/kg 02/24/14 15:34 78-93-370.4 1
n-Butylbenzene ND ug/kg 02/24/14 15:34 104-51-83.5 1
sec-Butylbenzene ND ug/kg 02/24/14 15:34 135-98-83.5 1
tert-Butylbenzene ND ug/kg 02/24/14 15:34 98-06-63.5 1
Carbon tetrachloride ND ug/kg 02/24/14 15:34 56-23-53.5 1
Chlorobenzene ND ug/kg 02/24/14 15:34 108-90-73.5 1
Chloroethane ND ug/kg 02/24/14 15:34 75-00-37.0 1
Chloroform ND ug/kg 02/24/14 15:34 67-66-33.5 1
Chloromethane ND ug/kg 02/24/14 15:34 74-87-37.0 1
2-Chlorotoluene ND ug/kg 02/24/14 15:34 95-49-83.5 1
4-Chlorotoluene ND ug/kg 02/24/14 15:34 106-43-43.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/24/14 15:34 96-12-83.5 1
Dibromochloromethane ND ug/kg 02/24/14 15:34 124-48-13.5 1
1,2-Dibromoethane (EDB)ND ug/kg 02/24/14 15:34 106-93-43.5 1
Dibromomethane ND ug/kg 02/24/14 15:34 74-95-33.5 1
1,2-Dichlorobenzene ND ug/kg 02/24/14 15:34 95-50-13.5 1
1,3-Dichlorobenzene ND ug/kg 02/24/14 15:34 541-73-13.5 1
1,4-Dichlorobenzene ND ug/kg 02/24/14 15:34 106-46-73.5 1
Dichlorodifluoromethane ND ug/kg 02/24/14 15:34 75-71-87.0 1
1,1-Dichloroethane ND ug/kg 02/24/14 15:34 75-34-33.5 1
1,2-Dichloroethane ND ug/kg 02/24/14 15:34 107-06-23.5 1
1,1-Dichloroethene ND ug/kg 02/24/14 15:34 75-35-43.5 1
cis-1,2-Dichloroethene ND ug/kg 02/24/14 15:34 156-59-23.5 1
trans-1,2-Dichloroethene ND ug/kg 02/24/14 15:34 156-60-53.5 1
1,2-Dichloropropane ND ug/kg 02/24/14 15:34 78-87-53.5 1
1,3-Dichloropropane ND ug/kg 02/24/14 15:34 142-28-93.5 1
2,2-Dichloropropane ND ug/kg 02/24/14 15:34 594-20-73.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 3
Lab ID:92190644003 Collected:02/20/14 11:40 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/kg 02/24/14 15:34 563-58-63.5 1
cis-1,3-Dichloropropene ND ug/kg 02/24/14 15:34 10061-01-53.5 1
trans-1,3-Dichloropropene ND ug/kg 02/24/14 15:34 10061-02-63.5 1
Diisopropyl ether ND ug/kg 02/24/14 15:34 108-20-33.5 1
Ethylbenzene ND ug/kg 02/24/14 15:34 100-41-43.5 1
Hexachloro-1,3-butadiene ND ug/kg 02/24/14 15:34 87-68-33.5 1
2-Hexanone ND ug/kg 02/24/14 15:34 591-78-635.2 1
Isopropylbenzene (Cumene)ND ug/kg 02/24/14 15:34 98-82-83.5 1
p-Isopropyltoluene ND ug/kg 02/24/14 15:34 99-87-63.5 1
Methylene Chloride ND ug/kg 02/24/14 15:34 75-09-214.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/24/14 15:34 108-10-135.2 1
Methyl-tert-butyl ether ND ug/kg 02/24/14 15:34 1634-04-43.5 1
Naphthalene ND ug/kg 02/24/14 15:34 91-20-33.5 1
n-Propylbenzene ND ug/kg 02/24/14 15:34 103-65-13.5 1
Styrene ND ug/kg 02/24/14 15:34 100-42-53.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/24/14 15:34 630-20-63.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/24/14 15:34 79-34-53.5 1
Tetrachloroethene ND ug/kg 02/24/14 15:34 127-18-43.5 1
Toluene ND ug/kg 02/24/14 15:34 108-88-33.5 1
1,2,3-Trichlorobenzene ND ug/kg 02/24/14 15:34 87-61-63.5 1
1,2,4-Trichlorobenzene ND ug/kg 02/24/14 15:34 120-82-13.5 1
1,1,1-Trichloroethane ND ug/kg 02/24/14 15:34 71-55-63.5 1
1,1,2-Trichloroethane ND ug/kg 02/24/14 15:34 79-00-53.5 1
Trichloroethene ND ug/kg 02/24/14 15:34 79-01-63.5 1
Trichlorofluoromethane ND ug/kg 02/24/14 15:34 75-69-43.5 1
1,2,3-Trichloropropane ND ug/kg 02/24/14 15:34 96-18-43.5 1
1,2,4-Trimethylbenzene ND ug/kg 02/24/14 15:34 95-63-63.5 1
1,3,5-Trimethylbenzene ND ug/kg 02/24/14 15:34 108-67-83.5 1
Vinyl acetate ND ug/kg 02/24/14 15:34 108-05-435.2 1
Vinyl chloride ND ug/kg 02/24/14 15:34 75-01-47.0 1
Xylene (Total)ND ug/kg 02/24/14 15:34 1330-20-77.0 1
m&p-Xylene ND ug/kg 02/24/14 15:34 179601-23-17.0 1
o-Xylene ND ug/kg 02/24/14 15:34 95-47-63.5 1
Surrogates
Toluene-d8 (S)121 %02/24/14 15:34 2037-26-570-130 1
4-Bromofluorobenzene (S)84 %02/24/14 15:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)77 %02/24/14 15:34 17060-07-070-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 18.4 %02/24/14 16:110.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 4
Lab ID:92190644004 Collected:02/20/14 11:45 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components ND mg/kg 02/22/14 15:56 68334-30-502/21/14 14:585.0 1
Surrogates
n-Pentacosane (S)67 %02/22/14 15:56 629-99-202/21/14 14:5841-119 1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 02/25/14 14:33 7440-38-202/25/14 10:250.82 1
Barium 72.2 mg/kg 02/25/14 14:33 7440-39-302/25/14 10:250.41 1
Cadmium 0.17 mg/kg 02/25/14 14:33 7440-43-902/25/14 10:250.082 1
Chromium 13.3 mg/kg 02/25/14 14:33 7440-47-302/25/14 10:250.41 1
Lead 5.4 mg/kg 02/25/14 14:33 7439-92-102/25/14 10:250.41 1
Selenium ND mg/kg 02/25/14 14:33 7782-49-202/25/14 10:250.82 1
Silver ND mg/kg 02/25/14 14:33 7440-22-402/25/14 10:250.41 1
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 02/28/14 20:10
Arsenic ND mg/L 03/04/14 14:36 7440-38-203/03/14 17:100.050 1
Barium 0.39 mg/L 03/04/14 14:36 7440-39-303/03/14 17:100.25 1
Cadmium ND mg/L 03/04/14 14:36 7440-43-903/03/14 17:100.0050 1
Chromium ND mg/L 03/04/14 14:36 7440-47-303/03/14 17:100.025 1
Lead 0.029 mg/L 03/04/14 14:36 7439-92-103/03/14 17:100.025 1
Selenium ND mg/L 03/04/14 14:36 7782-49-203/03/14 17:100.10 1
Silver ND mg/L 03/04/14 14:36 7440-22-403/03/14 17:100.025 1
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 02/28/14 20:10
Mercury ND ug/L 03/04/14 13:49 7439-97-603/03/14 18:000.20 1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.023 mg/kg 02/25/14 15:21 7439-97-602/24/14 22:450.0039 1
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 02/24/14 12:37 83-32-902/21/14 14:263301
Acenaphthylene ND ug/kg 02/24/14 12:37 208-96-802/21/14 14:263301
Anthracene ND ug/kg 02/24/14 12:37 120-12-702/21/14 14:263301
Benzo(a)anthracene ND ug/kg 02/24/14 12:37 56-55-302/21/14 14:263301
Benzo(a)pyrene ND ug/kg 02/24/14 12:37 50-32-802/21/14 14:263301
Benzo(b)fluoranthene ND ug/kg 02/24/14 12:37 205-99-202/21/14 14:263301
Benzo(g,h,i)perylene ND ug/kg 02/24/14 12:37 191-24-202/21/14 14:263301
Benzo(k)fluoranthene ND ug/kg 02/24/14 12:37 207-08-902/21/14 14:263301
Chrysene ND ug/kg 02/24/14 12:37 218-01-902/21/14 14:263301
Dibenz(a,h)anthracene ND ug/kg 02/24/14 12:37 53-70-302/21/14 14:263301
Fluoranthene ND ug/kg 02/24/14 12:37 206-44-002/21/14 14:263301
Fluorene ND ug/kg 02/24/14 12:37 86-73-702/21/14 14:263301
Indeno(1,2,3-cd)pyrene ND ug/kg 02/24/14 12:37 193-39-502/21/14 14:263301
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 4
Lab ID:92190644004 Collected:02/20/14 11:45 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
1-Methylnaphthalene ND ug/kg 02/24/14 12:37 90-12-002/21/14 14:263301
2-Methylnaphthalene ND ug/kg 02/24/14 12:37 91-57-602/21/14 14:263301
Naphthalene ND ug/kg 02/24/14 12:37 91-20-302/21/14 14:263301
Phenanthrene ND ug/kg 02/24/14 12:37 85-01-802/21/14 14:263301
Pyrene ND ug/kg 02/24/14 12:37 129-00-002/21/14 14:263301
Surrogates
Nitrobenzene-d5 (S)57 %02/24/14 12:37 4165-60-002/21/14 14:2623-110 1
2-Fluorobiphenyl (S)60 %02/24/14 12:37 321-60-802/21/14 14:2630-110 1
Terphenyl-d14 (S)67 %02/24/14 12:37 1718-51-002/21/14 14:2628-110 1
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 02/24/14 15:54 67-64-179.9 1
Benzene ND ug/kg 02/24/14 15:54 71-43-24.0 1
Bromobenzene ND ug/kg 02/24/14 15:54 108-86-14.0 1
Bromochloromethane ND ug/kg 02/24/14 15:54 74-97-54.0 1
Bromodichloromethane ND ug/kg 02/24/14 15:54 75-27-44.0 1
Bromoform ND ug/kg 02/24/14 15:54 75-25-24.0 1
Bromomethane ND ug/kg 02/24/14 15:54 74-83-98.0 1
2-Butanone (MEK)ND ug/kg 02/24/14 15:54 78-93-379.9 1
n-Butylbenzene ND ug/kg 02/24/14 15:54 104-51-84.0 1
sec-Butylbenzene ND ug/kg 02/24/14 15:54 135-98-84.0 1
tert-Butylbenzene ND ug/kg 02/24/14 15:54 98-06-64.0 1
Carbon tetrachloride ND ug/kg 02/24/14 15:54 56-23-54.0 1
Chlorobenzene ND ug/kg 02/24/14 15:54 108-90-74.0 1
Chloroethane ND ug/kg 02/24/14 15:54 75-00-38.0 1
Chloroform ND ug/kg 02/24/14 15:54 67-66-34.0 1
Chloromethane ND ug/kg 02/24/14 15:54 74-87-38.0 1
2-Chlorotoluene ND ug/kg 02/24/14 15:54 95-49-84.0 1
4-Chlorotoluene ND ug/kg 02/24/14 15:54 106-43-44.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/24/14 15:54 96-12-84.0 1
Dibromochloromethane ND ug/kg 02/24/14 15:54 124-48-14.0 1
1,2-Dibromoethane (EDB)ND ug/kg 02/24/14 15:54 106-93-44.0 1
Dibromomethane ND ug/kg 02/24/14 15:54 74-95-34.0 1
1,2-Dichlorobenzene ND ug/kg 02/24/14 15:54 95-50-14.0 1
1,3-Dichlorobenzene ND ug/kg 02/24/14 15:54 541-73-14.0 1
1,4-Dichlorobenzene ND ug/kg 02/24/14 15:54 106-46-74.0 1
Dichlorodifluoromethane ND ug/kg 02/24/14 15:54 75-71-88.0 1
1,1-Dichloroethane ND ug/kg 02/24/14 15:54 75-34-34.0 1
1,2-Dichloroethane ND ug/kg 02/24/14 15:54 107-06-24.0 1
1,1-Dichloroethene ND ug/kg 02/24/14 15:54 75-35-44.0 1
cis-1,2-Dichloroethene ND ug/kg 02/24/14 15:54 156-59-24.0 1
trans-1,2-Dichloroethene ND ug/kg 02/24/14 15:54 156-60-54.0 1
1,2-Dichloropropane ND ug/kg 02/24/14 15:54 78-87-54.0 1
1,3-Dichloropropane ND ug/kg 02/24/14 15:54 142-28-94.0 1
2,2-Dichloropropane ND ug/kg 02/24/14 15:54 594-20-74.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 4
Lab ID:92190644004 Collected:02/20/14 11:45 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/kg 02/24/14 15:54 563-58-64.0 1
cis-1,3-Dichloropropene ND ug/kg 02/24/14 15:54 10061-01-54.0 1
trans-1,3-Dichloropropene ND ug/kg 02/24/14 15:54 10061-02-64.0 1
Diisopropyl ether ND ug/kg 02/24/14 15:54 108-20-34.0 1
Ethylbenzene ND ug/kg 02/24/14 15:54 100-41-44.0 1
Hexachloro-1,3-butadiene ND ug/kg 02/24/14 15:54 87-68-34.0 1
2-Hexanone ND ug/kg 02/24/14 15:54 591-78-639.9 1
Isopropylbenzene (Cumene)ND ug/kg 02/24/14 15:54 98-82-84.0 1
p-Isopropyltoluene ND ug/kg 02/24/14 15:54 99-87-64.0 1
Methylene Chloride ND ug/kg 02/24/14 15:54 75-09-216.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/24/14 15:54 108-10-139.9 1
Methyl-tert-butyl ether ND ug/kg 02/24/14 15:54 1634-04-44.0 1
Naphthalene ND ug/kg 02/24/14 15:54 91-20-34.0 1
n-Propylbenzene ND ug/kg 02/24/14 15:54 103-65-14.0 1
Styrene ND ug/kg 02/24/14 15:54 100-42-54.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/24/14 15:54 630-20-64.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/24/14 15:54 79-34-54.0 1
Tetrachloroethene ND ug/kg 02/24/14 15:54 127-18-44.0 1
Toluene ND ug/kg 02/24/14 15:54 108-88-34.0 1
1,2,3-Trichlorobenzene ND ug/kg 02/24/14 15:54 87-61-64.0 1
1,2,4-Trichlorobenzene ND ug/kg 02/24/14 15:54 120-82-14.0 1
1,1,1-Trichloroethane ND ug/kg 02/24/14 15:54 71-55-64.0 1
1,1,2-Trichloroethane ND ug/kg 02/24/14 15:54 79-00-54.0 1
Trichloroethene ND ug/kg 02/24/14 15:54 79-01-64.0 1
Trichlorofluoromethane ND ug/kg 02/24/14 15:54 75-69-44.0 1
1,2,3-Trichloropropane ND ug/kg 02/24/14 15:54 96-18-44.0 1
1,2,4-Trimethylbenzene ND ug/kg 02/24/14 15:54 95-63-64.0 1
1,3,5-Trimethylbenzene ND ug/kg 02/24/14 15:54 108-67-84.0 1
Vinyl acetate ND ug/kg 02/24/14 15:54 108-05-439.9 1
Vinyl chloride ND ug/kg 02/24/14 15:54 75-01-48.0 1
Xylene (Total)ND ug/kg 02/24/14 15:54 1330-20-78.0 1
m&p-Xylene ND ug/kg 02/24/14 15:54 179601-23-18.0 1
o-Xylene ND ug/kg 02/24/14 15:54 95-47-64.0 1
Surrogates
Toluene-d8 (S)111 %02/24/14 15:54 2037-26-570-130 1
4-Bromofluorobenzene (S)95 %02/24/14 15:54 460-00-470-130 1
1,2-Dichloroethane-d4 (S)84 %02/24/14 15:54 17060-07-070-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 32.8 %02/24/14 16:110.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 5
Lab ID:92190644005 Collected:02/20/14 11:47 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components ND mg/kg 02/22/14 15:56 68334-30-502/21/14 14:585.0 1
Surrogates
n-Pentacosane (S)77 %02/22/14 15:56 629-99-202/21/14 14:5841-119 1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 02/25/14 14:37 7440-38-202/25/14 10:250.70 1
Barium 94.1 mg/kg 02/25/14 14:37 7440-39-302/25/14 10:250.35 1
Cadmium ND mg/kg 02/25/14 14:37 7440-43-902/25/14 10:250.070 1
Chromium 5.0 mg/kg 02/25/14 14:37 7440-47-302/25/14 10:250.35 1
Lead 4.3 mg/kg 02/25/14 14:37 7439-92-102/25/14 10:250.35 1
Selenium ND mg/kg 02/25/14 14:37 7782-49-202/25/14 10:250.70 1
Silver ND mg/kg 02/25/14 14:37 7440-22-402/25/14 10:250.35 1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.0090 mg/kg 02/25/14 15:29 7439-97-602/24/14 22:450.0031 1
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 02/24/14 13:08 83-32-902/21/14 14:263301
Acenaphthylene ND ug/kg 02/24/14 13:08 208-96-802/21/14 14:263301
Anthracene ND ug/kg 02/24/14 13:08 120-12-702/21/14 14:263301
Benzo(a)anthracene ND ug/kg 02/24/14 13:08 56-55-302/21/14 14:263301
Benzo(a)pyrene ND ug/kg 02/24/14 13:08 50-32-802/21/14 14:263301
Benzo(b)fluoranthene ND ug/kg 02/24/14 13:08 205-99-202/21/14 14:263301
Benzo(g,h,i)perylene ND ug/kg 02/24/14 13:08 191-24-202/21/14 14:263301
Benzo(k)fluoranthene ND ug/kg 02/24/14 13:08 207-08-902/21/14 14:263301
Chrysene ND ug/kg 02/24/14 13:08 218-01-902/21/14 14:263301
Dibenz(a,h)anthracene ND ug/kg 02/24/14 13:08 53-70-302/21/14 14:263301
Fluoranthene ND ug/kg 02/24/14 13:08 206-44-002/21/14 14:263301
Fluorene ND ug/kg 02/24/14 13:08 86-73-702/21/14 14:263301
Indeno(1,2,3-cd)pyrene ND ug/kg 02/24/14 13:08 193-39-502/21/14 14:263301
1-Methylnaphthalene ND ug/kg 02/24/14 13:08 90-12-002/21/14 14:263301
2-Methylnaphthalene ND ug/kg 02/24/14 13:08 91-57-602/21/14 14:263301
Naphthalene ND ug/kg 02/24/14 13:08 91-20-302/21/14 14:263301
Phenanthrene ND ug/kg 02/24/14 13:08 85-01-802/21/14 14:263301
Pyrene ND ug/kg 02/24/14 13:08 129-00-002/21/14 14:263301
Surrogates
Nitrobenzene-d5 (S)67 %02/24/14 13:08 4165-60-002/21/14 14:2623-110 1
2-Fluorobiphenyl (S)72 %02/24/14 13:08 321-60-802/21/14 14:2630-110 1
Terphenyl-d14 (S)72 %02/24/14 13:08 1718-51-002/21/14 14:2628-110 1
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 02/24/14 16:14 67-64-198.2 1
Benzene ND ug/kg 02/24/14 16:14 71-43-24.9 1
Bromobenzene ND ug/kg 02/24/14 16:14 108-86-14.9 1
Bromochloromethane ND ug/kg 02/24/14 16:14 74-97-54.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 5
Lab ID:92190644005 Collected:02/20/14 11:47 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromodichloromethane ND ug/kg 02/24/14 16:14 75-27-44.9 1
Bromoform ND ug/kg 02/24/14 16:14 75-25-24.9 1
Bromomethane ND ug/kg 02/24/14 16:14 74-83-99.8 1
2-Butanone (MEK)ND ug/kg 02/24/14 16:14 78-93-398.2 1
n-Butylbenzene ND ug/kg 02/24/14 16:14 104-51-84.9 1
sec-Butylbenzene ND ug/kg 02/24/14 16:14 135-98-84.9 1
tert-Butylbenzene ND ug/kg 02/24/14 16:14 98-06-64.9 1
Carbon tetrachloride ND ug/kg 02/24/14 16:14 56-23-54.9 1
Chlorobenzene ND ug/kg 02/24/14 16:14 108-90-74.9 1
Chloroethane ND ug/kg 02/24/14 16:14 75-00-39.8 1
Chloroform ND ug/kg 02/24/14 16:14 67-66-34.9 1
Chloromethane ND ug/kg 02/24/14 16:14 74-87-39.8 1
2-Chlorotoluene ND ug/kg 02/24/14 16:14 95-49-84.9 1
4-Chlorotoluene ND ug/kg 02/24/14 16:14 106-43-44.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/24/14 16:14 96-12-84.9 1
Dibromochloromethane ND ug/kg 02/24/14 16:14 124-48-14.9 1
1,2-Dibromoethane (EDB)ND ug/kg 02/24/14 16:14 106-93-44.9 1
Dibromomethane ND ug/kg 02/24/14 16:14 74-95-34.9 1
1,2-Dichlorobenzene ND ug/kg 02/24/14 16:14 95-50-14.9 1
1,3-Dichlorobenzene ND ug/kg 02/24/14 16:14 541-73-14.9 1
1,4-Dichlorobenzene ND ug/kg 02/24/14 16:14 106-46-74.9 1
Dichlorodifluoromethane ND ug/kg 02/24/14 16:14 75-71-89.8 1
1,1-Dichloroethane ND ug/kg 02/24/14 16:14 75-34-34.9 1
1,2-Dichloroethane ND ug/kg 02/24/14 16:14 107-06-24.9 1
1,1-Dichloroethene ND ug/kg 02/24/14 16:14 75-35-44.9 1
cis-1,2-Dichloroethene ND ug/kg 02/24/14 16:14 156-59-24.9 1
trans-1,2-Dichloroethene ND ug/kg 02/24/14 16:14 156-60-54.9 1
1,2-Dichloropropane ND ug/kg 02/24/14 16:14 78-87-54.9 1
1,3-Dichloropropane ND ug/kg 02/24/14 16:14 142-28-94.9 1
2,2-Dichloropropane ND ug/kg 02/24/14 16:14 594-20-74.9 1
1,1-Dichloropropene ND ug/kg 02/24/14 16:14 563-58-64.9 1
cis-1,3-Dichloropropene ND ug/kg 02/24/14 16:14 10061-01-54.9 1
trans-1,3-Dichloropropene ND ug/kg 02/24/14 16:14 10061-02-64.9 1
Diisopropyl ether ND ug/kg 02/24/14 16:14 108-20-34.9 1
Ethylbenzene ND ug/kg 02/24/14 16:14 100-41-44.9 1
Hexachloro-1,3-butadiene ND ug/kg 02/24/14 16:14 87-68-34.9 1
2-Hexanone ND ug/kg 02/24/14 16:14 591-78-649.1 1
Isopropylbenzene (Cumene)ND ug/kg 02/24/14 16:14 98-82-84.9 1
p-Isopropyltoluene ND ug/kg 02/24/14 16:14 99-87-64.9 1
Methylene Chloride ND ug/kg 02/24/14 16:14 75-09-219.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/24/14 16:14 108-10-149.1 1
Methyl-tert-butyl ether ND ug/kg 02/24/14 16:14 1634-04-44.9 1
Naphthalene ND ug/kg 02/24/14 16:14 91-20-34.9 1
n-Propylbenzene ND ug/kg 02/24/14 16:14 103-65-14.9 1
Styrene ND ug/kg 02/24/14 16:14 100-42-54.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 5
Lab ID:92190644005 Collected:02/20/14 11:47 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 02/24/14 16:14 630-20-64.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/24/14 16:14 79-34-54.9 1
Tetrachloroethene ND ug/kg 02/24/14 16:14 127-18-44.9 1
Toluene ND ug/kg 02/24/14 16:14 108-88-34.9 1
1,2,3-Trichlorobenzene ND ug/kg 02/24/14 16:14 87-61-64.9 1
1,2,4-Trichlorobenzene ND ug/kg 02/24/14 16:14 120-82-14.9 1
1,1,1-Trichloroethane ND ug/kg 02/24/14 16:14 71-55-64.9 1
1,1,2-Trichloroethane ND ug/kg 02/24/14 16:14 79-00-54.9 1
Trichloroethene ND ug/kg 02/24/14 16:14 79-01-64.9 1
Trichlorofluoromethane ND ug/kg 02/24/14 16:14 75-69-44.9 1
1,2,3-Trichloropropane ND ug/kg 02/24/14 16:14 96-18-44.9 1
1,2,4-Trimethylbenzene ND ug/kg 02/24/14 16:14 95-63-64.9 1
1,3,5-Trimethylbenzene ND ug/kg 02/24/14 16:14 108-67-84.9 1
Vinyl acetate ND ug/kg 02/24/14 16:14 108-05-449.1 1
Vinyl chloride ND ug/kg 02/24/14 16:14 75-01-49.8 1
Xylene (Total)ND ug/kg 02/24/14 16:14 1330-20-79.8 1
m&p-Xylene ND ug/kg 02/24/14 16:14 179601-23-19.8 1
o-Xylene ND ug/kg 02/24/14 16:14 95-47-64.9 1
Surrogates
Toluene-d8 (S)109 %02/24/14 16:14 2037-26-570-130 1
4-Bromofluorobenzene (S)99 %02/24/14 16:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %02/24/14 16:14 17060-07-070-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 38.8 %02/24/14 16:110.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 6
Lab ID:92190644006 Collected:02/20/14 11:55 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 7.2 mg/kg 02/22/14 16:20 68334-30-502/21/14 14:585.0 1
Surrogates
n-Pentacosane (S)73 %02/22/14 16:20 629-99-202/21/14 14:5841-119 1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 02/25/14 14:40 7440-38-202/25/14 10:250.89 1
Barium 142 mg/kg 02/25/14 14:40 7440-39-302/25/14 10:250.45 1
Cadmium 0.12 mg/kg 02/25/14 14:40 7440-43-902/25/14 10:250.089 1
Chromium 27.2 mg/kg 02/25/14 14:40 7440-47-302/25/14 10:250.45 1
Lead 8.1 mg/kg 02/25/14 14:40 7439-92-102/25/14 10:250.45 1
Selenium ND mg/kg 02/25/14 14:40 7782-49-202/25/14 10:250.89 1
Silver ND mg/kg 02/25/14 14:40 7440-22-402/25/14 10:250.45 1
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 02/28/14 20:10
Arsenic ND mg/L 03/04/14 14:42 7440-38-203/03/14 17:100.050 1
Barium 0.92 mg/L 03/04/14 14:42 7440-39-303/03/14 17:100.25 1
Cadmium ND mg/L 03/04/14 14:42 7440-43-903/03/14 17:100.0050 1
Chromium ND mg/L 03/04/14 14:42 7440-47-303/03/14 17:100.025 1
Lead ND mg/L 03/04/14 14:42 7439-92-103/03/14 17:100.025 1
Selenium ND mg/L 03/04/14 14:42 7782-49-203/03/14 17:100.10 1
Silver ND mg/L 03/04/14 14:42 7440-22-403/03/14 17:100.025 1
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 02/28/14 20:10
Mercury ND ug/L 03/04/14 13:51 7439-97-603/03/14 18:000.20 1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.028 mg/kg 02/25/14 15:32 7439-97-602/24/14 22:450.0037 1
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 02/24/14 13:38 83-32-902/21/14 14:263301
Acenaphthylene ND ug/kg 02/24/14 13:38 208-96-802/21/14 14:263301
Anthracene ND ug/kg 02/24/14 13:38 120-12-702/21/14 14:263301
Benzo(a)anthracene ND ug/kg 02/24/14 13:38 56-55-302/21/14 14:263301
Benzo(a)pyrene ND ug/kg 02/24/14 13:38 50-32-802/21/14 14:263301
Benzo(b)fluoranthene ND ug/kg 02/24/14 13:38 205-99-202/21/14 14:263301
Benzo(g,h,i)perylene ND ug/kg 02/24/14 13:38 191-24-202/21/14 14:263301
Benzo(k)fluoranthene ND ug/kg 02/24/14 13:38 207-08-902/21/14 14:263301
Chrysene ND ug/kg 02/24/14 13:38 218-01-902/21/14 14:263301
Dibenz(a,h)anthracene ND ug/kg 02/24/14 13:38 53-70-302/21/14 14:263301
Fluoranthene ND ug/kg 02/24/14 13:38 206-44-002/21/14 14:263301
Fluorene ND ug/kg 02/24/14 13:38 86-73-702/21/14 14:263301
Indeno(1,2,3-cd)pyrene ND ug/kg 02/24/14 13:38 193-39-502/21/14 14:263301
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 6
Lab ID:92190644006 Collected:02/20/14 11:55 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
1-Methylnaphthalene ND ug/kg 02/24/14 13:38 90-12-002/21/14 14:263301
2-Methylnaphthalene ND ug/kg 02/24/14 13:38 91-57-602/21/14 14:263301
Naphthalene ND ug/kg 02/24/14 13:38 91-20-302/21/14 14:263301
Phenanthrene ND ug/kg 02/24/14 13:38 85-01-802/21/14 14:263301
Pyrene ND ug/kg 02/24/14 13:38 129-00-002/21/14 14:263301
Surrogates
Nitrobenzene-d5 (S)67 %02/24/14 13:38 4165-60-002/21/14 14:2623-110 1
2-Fluorobiphenyl (S)65 %02/24/14 13:38 321-60-802/21/14 14:2630-110 1
Terphenyl-d14 (S)69 %02/24/14 13:38 1718-51-002/21/14 14:2628-110 1
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 109 ug/kg 02/24/14 16:33 67-64-1 A+80.4 1
Benzene ND ug/kg 02/24/14 16:33 71-43-24.0 1
Bromobenzene ND ug/kg 02/24/14 16:33 108-86-14.0 1
Bromochloromethane ND ug/kg 02/24/14 16:33 74-97-54.0 1
Bromodichloromethane ND ug/kg 02/24/14 16:33 75-27-44.0 1
Bromoform ND ug/kg 02/24/14 16:33 75-25-24.0 1
Bromomethane ND ug/kg 02/24/14 16:33 74-83-98.0 1
2-Butanone (MEK)ND ug/kg 02/24/14 16:33 78-93-380.4 1
n-Butylbenzene ND ug/kg 02/24/14 16:33 104-51-84.0 1
sec-Butylbenzene ND ug/kg 02/24/14 16:33 135-98-84.0 1
tert-Butylbenzene ND ug/kg 02/24/14 16:33 98-06-64.0 1
Carbon tetrachloride ND ug/kg 02/24/14 16:33 56-23-54.0 1
Chlorobenzene ND ug/kg 02/24/14 16:33 108-90-74.0 1
Chloroethane ND ug/kg 02/24/14 16:33 75-00-38.0 1
Chloroform ND ug/kg 02/24/14 16:33 67-66-34.0 1
Chloromethane ND ug/kg 02/24/14 16:33 74-87-38.0 1
2-Chlorotoluene ND ug/kg 02/24/14 16:33 95-49-84.0 1
4-Chlorotoluene ND ug/kg 02/24/14 16:33 106-43-44.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/24/14 16:33 96-12-84.0 1
Dibromochloromethane ND ug/kg 02/24/14 16:33 124-48-14.0 1
1,2-Dibromoethane (EDB)ND ug/kg 02/24/14 16:33 106-93-44.0 1
Dibromomethane ND ug/kg 02/24/14 16:33 74-95-34.0 1
1,2-Dichlorobenzene ND ug/kg 02/24/14 16:33 95-50-14.0 1
1,3-Dichlorobenzene ND ug/kg 02/24/14 16:33 541-73-14.0 1
1,4-Dichlorobenzene ND ug/kg 02/24/14 16:33 106-46-74.0 1
Dichlorodifluoromethane ND ug/kg 02/24/14 16:33 75-71-88.0 1
1,1-Dichloroethane ND ug/kg 02/24/14 16:33 75-34-34.0 1
1,2-Dichloroethane ND ug/kg 02/24/14 16:33 107-06-24.0 1
1,1-Dichloroethene ND ug/kg 02/24/14 16:33 75-35-44.0 1
cis-1,2-Dichloroethene ND ug/kg 02/24/14 16:33 156-59-24.0 1
trans-1,2-Dichloroethene ND ug/kg 02/24/14 16:33 156-60-54.0 1
1,2-Dichloropropane ND ug/kg 02/24/14 16:33 78-87-54.0 1
1,3-Dichloropropane ND ug/kg 02/24/14 16:33 142-28-94.0 1
2,2-Dichloropropane ND ug/kg 02/24/14 16:33 594-20-74.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 6
Lab ID:92190644006 Collected:02/20/14 11:55 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/kg 02/24/14 16:33 563-58-64.0 1
cis-1,3-Dichloropropene ND ug/kg 02/24/14 16:33 10061-01-54.0 1
trans-1,3-Dichloropropene ND ug/kg 02/24/14 16:33 10061-02-64.0 1
Diisopropyl ether ND ug/kg 02/24/14 16:33 108-20-34.0 1
Ethylbenzene ND ug/kg 02/24/14 16:33 100-41-44.0 1
Hexachloro-1,3-butadiene ND ug/kg 02/24/14 16:33 87-68-34.0 1
2-Hexanone ND ug/kg 02/24/14 16:33 591-78-640.2 1
Isopropylbenzene (Cumene)ND ug/kg 02/24/14 16:33 98-82-84.0 1
p-Isopropyltoluene ND ug/kg 02/24/14 16:33 99-87-64.0 1
Methylene Chloride ND ug/kg 02/24/14 16:33 75-09-216.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/24/14 16:33 108-10-140.2 1
Methyl-tert-butyl ether ND ug/kg 02/24/14 16:33 1634-04-44.0 1
Naphthalene ND ug/kg 02/24/14 16:33 91-20-34.0 1
n-Propylbenzene ND ug/kg 02/24/14 16:33 103-65-14.0 1
Styrene ND ug/kg 02/24/14 16:33 100-42-54.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/24/14 16:33 630-20-64.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/24/14 16:33 79-34-54.0 1
Tetrachloroethene ND ug/kg 02/24/14 16:33 127-18-44.0 1
Toluene ND ug/kg 02/24/14 16:33 108-88-34.0 1
1,2,3-Trichlorobenzene ND ug/kg 02/24/14 16:33 87-61-64.0 1
1,2,4-Trichlorobenzene ND ug/kg 02/24/14 16:33 120-82-14.0 1
1,1,1-Trichloroethane ND ug/kg 02/24/14 16:33 71-55-64.0 1
1,1,2-Trichloroethane ND ug/kg 02/24/14 16:33 79-00-54.0 1
Trichloroethene ND ug/kg 02/24/14 16:33 79-01-64.0 1
Trichlorofluoromethane ND ug/kg 02/24/14 16:33 75-69-44.0 1
1,2,3-Trichloropropane ND ug/kg 02/24/14 16:33 96-18-44.0 1
1,2,4-Trimethylbenzene ND ug/kg 02/24/14 16:33 95-63-64.0 1
1,3,5-Trimethylbenzene ND ug/kg 02/24/14 16:33 108-67-84.0 1
Vinyl acetate ND ug/kg 02/24/14 16:33 108-05-440.2 1
Vinyl chloride ND ug/kg 02/24/14 16:33 75-01-48.0 1
Xylene (Total)ND ug/kg 02/24/14 16:33 1330-20-78.0 1
m&p-Xylene ND ug/kg 02/24/14 16:33 179601-23-18.0 1
o-Xylene ND ug/kg 02/24/14 16:33 95-47-64.0 1
Surrogates
Toluene-d8 (S)113 %02/24/14 16:33 2037-26-570-130 1
4-Bromofluorobenzene (S)90 %02/24/14 16:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %02/24/14 16:33 17060-07-070-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 27.0 %02/24/14 16:120.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 7
Lab ID:92190644007 Collected:02/20/14 11:50 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components ND mg/kg 02/22/14 16:20 68334-30-502/21/14 14:585.0 1
Surrogates
n-Pentacosane (S)87 %02/22/14 16:20 629-99-202/21/14 14:5841-119 1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 02/25/14 14:56 7440-38-202/25/14 10:250.98 1
Barium 47.1 mg/kg 02/25/14 14:56 7440-39-302/25/14 10:250.49 1
Cadmium ND mg/kg 02/25/14 14:56 7440-43-902/25/14 10:250.098 1
Chromium 18.7 mg/kg 02/25/14 14:56 7440-47-302/25/14 10:250.49 1
Lead 4.8 mg/kg 02/25/14 14:56 7439-92-102/25/14 10:250.49 1
Selenium ND mg/kg 02/25/14 14:56 7782-49-202/25/14 10:250.98 1
Silver ND mg/kg 02/25/14 14:56 7440-22-402/25/14 10:250.49 1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.0077 mg/kg 02/25/14 15:34 7439-97-602/24/14 22:450.0033 1
8270 MSSV PAH Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 02/24/14 14:09 83-32-902/21/14 14:263301
Acenaphthylene ND ug/kg 02/24/14 14:09 208-96-802/21/14 14:263301
Anthracene ND ug/kg 02/24/14 14:09 120-12-702/21/14 14:263301
Benzo(a)anthracene ND ug/kg 02/24/14 14:09 56-55-302/21/14 14:263301
Benzo(a)pyrene ND ug/kg 02/24/14 14:09 50-32-802/21/14 14:263301
Benzo(b)fluoranthene ND ug/kg 02/24/14 14:09 205-99-202/21/14 14:263301
Benzo(g,h,i)perylene ND ug/kg 02/24/14 14:09 191-24-202/21/14 14:263301
Benzo(k)fluoranthene ND ug/kg 02/24/14 14:09 207-08-902/21/14 14:263301
Chrysene ND ug/kg 02/24/14 14:09 218-01-902/21/14 14:263301
Dibenz(a,h)anthracene ND ug/kg 02/24/14 14:09 53-70-302/21/14 14:263301
Fluoranthene ND ug/kg 02/24/14 14:09 206-44-002/21/14 14:263301
Fluorene ND ug/kg 02/24/14 14:09 86-73-702/21/14 14:263301
Indeno(1,2,3-cd)pyrene ND ug/kg 02/24/14 14:09 193-39-502/21/14 14:263301
1-Methylnaphthalene ND ug/kg 02/24/14 14:09 90-12-002/21/14 14:263301
2-Methylnaphthalene ND ug/kg 02/24/14 14:09 91-57-602/21/14 14:263301
Naphthalene ND ug/kg 02/24/14 14:09 91-20-302/21/14 14:263301
Phenanthrene ND ug/kg 02/24/14 14:09 85-01-802/21/14 14:263301
Pyrene ND ug/kg 02/24/14 14:09 129-00-002/21/14 14:263301
Surrogates
Nitrobenzene-d5 (S)57 %02/24/14 14:09 4165-60-002/21/14 14:2623-110 1
2-Fluorobiphenyl (S)60 %02/24/14 14:09 321-60-802/21/14 14:2630-110 1
Terphenyl-d14 (S)63 %02/24/14 14:09 1718-51-002/21/14 14:2628-110 1
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 02/24/14 16:53 67-64-186.4 1
Benzene ND ug/kg 02/24/14 16:53 71-43-24.3 1
Bromobenzene ND ug/kg 02/24/14 16:53 108-86-14.3 1
Bromochloromethane ND ug/kg 02/24/14 16:53 74-97-54.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 7
Lab ID:92190644007 Collected:02/20/14 11:50 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromodichloromethane ND ug/kg 02/24/14 16:53 75-27-44.3 1
Bromoform ND ug/kg 02/24/14 16:53 75-25-24.3 1
Bromomethane ND ug/kg 02/24/14 16:53 74-83-98.6 1
2-Butanone (MEK)ND ug/kg 02/24/14 16:53 78-93-386.4 1
n-Butylbenzene ND ug/kg 02/24/14 16:53 104-51-84.3 1
sec-Butylbenzene ND ug/kg 02/24/14 16:53 135-98-84.3 1
tert-Butylbenzene ND ug/kg 02/24/14 16:53 98-06-64.3 1
Carbon tetrachloride ND ug/kg 02/24/14 16:53 56-23-54.3 1
Chlorobenzene ND ug/kg 02/24/14 16:53 108-90-74.3 1
Chloroethane ND ug/kg 02/24/14 16:53 75-00-38.6 1
Chloroform ND ug/kg 02/24/14 16:53 67-66-34.3 1
Chloromethane ND ug/kg 02/24/14 16:53 74-87-38.6 1
2-Chlorotoluene ND ug/kg 02/24/14 16:53 95-49-84.3 1
4-Chlorotoluene ND ug/kg 02/24/14 16:53 106-43-44.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/24/14 16:53 96-12-84.3 1
Dibromochloromethane ND ug/kg 02/24/14 16:53 124-48-14.3 1
1,2-Dibromoethane (EDB)ND ug/kg 02/24/14 16:53 106-93-44.3 1
Dibromomethane ND ug/kg 02/24/14 16:53 74-95-34.3 1
1,2-Dichlorobenzene ND ug/kg 02/24/14 16:53 95-50-14.3 1
1,3-Dichlorobenzene ND ug/kg 02/24/14 16:53 541-73-14.3 1
1,4-Dichlorobenzene ND ug/kg 02/24/14 16:53 106-46-74.3 1
Dichlorodifluoromethane ND ug/kg 02/24/14 16:53 75-71-88.6 1
1,1-Dichloroethane ND ug/kg 02/24/14 16:53 75-34-34.3 1
1,2-Dichloroethane ND ug/kg 02/24/14 16:53 107-06-24.3 1
1,1-Dichloroethene ND ug/kg 02/24/14 16:53 75-35-44.3 1
cis-1,2-Dichloroethene ND ug/kg 02/24/14 16:53 156-59-24.3 1
trans-1,2-Dichloroethene ND ug/kg 02/24/14 16:53 156-60-54.3 1
1,2-Dichloropropane ND ug/kg 02/24/14 16:53 78-87-54.3 1
1,3-Dichloropropane ND ug/kg 02/24/14 16:53 142-28-94.3 1
2,2-Dichloropropane ND ug/kg 02/24/14 16:53 594-20-74.3 1
1,1-Dichloropropene ND ug/kg 02/24/14 16:53 563-58-64.3 1
cis-1,3-Dichloropropene ND ug/kg 02/24/14 16:53 10061-01-54.3 1
trans-1,3-Dichloropropene ND ug/kg 02/24/14 16:53 10061-02-64.3 1
Diisopropyl ether ND ug/kg 02/24/14 16:53 108-20-34.3 1
Ethylbenzene ND ug/kg 02/24/14 16:53 100-41-44.3 1
Hexachloro-1,3-butadiene ND ug/kg 02/24/14 16:53 87-68-34.3 1
2-Hexanone ND ug/kg 02/24/14 16:53 591-78-643.2 1
Isopropylbenzene (Cumene)ND ug/kg 02/24/14 16:53 98-82-84.3 1
p-Isopropyltoluene ND ug/kg 02/24/14 16:53 99-87-64.3 1
Methylene Chloride ND ug/kg 02/24/14 16:53 75-09-217.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/24/14 16:53 108-10-143.2 1
Methyl-tert-butyl ether ND ug/kg 02/24/14 16:53 1634-04-44.3 1
Naphthalene ND ug/kg 02/24/14 16:53 91-20-34.3 1
n-Propylbenzene ND ug/kg 02/24/14 16:53 103-65-14.3 1
Styrene ND ug/kg 02/24/14 16:53 100-42-54.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Sample:SOIL CUTTING PAD 1
STOCK 7
Lab ID:92190644007 Collected:02/20/14 11:50 Received:02/21/14 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 02/24/14 16:53 630-20-64.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/24/14 16:53 79-34-54.3 1
Tetrachloroethene ND ug/kg 02/24/14 16:53 127-18-44.3 1
Toluene ND ug/kg 02/24/14 16:53 108-88-34.3 1
1,2,3-Trichlorobenzene ND ug/kg 02/24/14 16:53 87-61-64.3 1
1,2,4-Trichlorobenzene ND ug/kg 02/24/14 16:53 120-82-14.3 1
1,1,1-Trichloroethane ND ug/kg 02/24/14 16:53 71-55-64.3 1
1,1,2-Trichloroethane ND ug/kg 02/24/14 16:53 79-00-54.3 1
Trichloroethene ND ug/kg 02/24/14 16:53 79-01-64.3 1
Trichlorofluoromethane ND ug/kg 02/24/14 16:53 75-69-44.3 1
1,2,3-Trichloropropane ND ug/kg 02/24/14 16:53 96-18-44.3 1
1,2,4-Trimethylbenzene ND ug/kg 02/24/14 16:53 95-63-64.3 1
1,3,5-Trimethylbenzene ND ug/kg 02/24/14 16:53 108-67-84.3 1
Vinyl acetate ND ug/kg 02/24/14 16:53 108-05-443.2 1
Vinyl chloride ND ug/kg 02/24/14 16:53 75-01-48.6 1
Xylene (Total)ND ug/kg 02/24/14 16:53 1330-20-78.6 1
m&p-Xylene ND ug/kg 02/24/14 16:53 179601-23-18.6 1
o-Xylene ND ug/kg 02/24/14 16:53 95-47-64.3 1
Surrogates
Toluene-d8 (S)106 %02/24/14 16:53 2037-26-570-130 1
4-Bromofluorobenzene (S)98 %02/24/14 16:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %02/24/14 16:53 17060-07-070-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 24.3 %02/24/14 16:120.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/6263
EPA 7470
EPA 7470
7470 Mercury TCLP
Associated Lab Samples:92190644003, 92190644004, 92190644006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1149126
Associated Lab Samples:92190644003, 92190644004, 92190644006
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 03/04/14 13:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1149127LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.82.5 110 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1149128MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190644003
1149129
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L M1,R12.5 200 75-125112 552.5ND 5.1 2.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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9800 Kincey Ave. Suite 100
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Page 27 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/6223
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1144175
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0050 02/25/14 14:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1144176LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.068.067 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1144177MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190644001
1144178
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/kg M1,R1.056 47 75-125281 82.0530.048 0.087 0.21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/15295
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1143290
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Matrix:Solid
Analyzed
Arsenic mg/kg ND 1.0 02/25/14 14:12
Cadmium mg/kg ND 0.10 02/25/14 14:12
Chromium mg/kg ND 0.50 02/25/14 14:12
Lead mg/kg ND 0.50 02/25/14 14:12
Selenium mg/kg ND 1.0 02/25/14 14:12
Silver mg/kg ND 0.50 02/25/14 14:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1143291LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 50.150 100 80-120
Cadmium mg/kg 51.350 103 80-120
Chromium mg/kg 50.750 101 80-120
Lead mg/kg 51.050 102 80-120
Selenium mg/kg 51.050 102 80-120
Silver mg/kg 25.225 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1143292MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190644001
1143293
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic mg/kg 57.6 86 75-12587 760.8ND 49.8 53.2
Cadmium mg/kg 57.6 96 75-12597 660.80.11 55.3 58.8
Chromium mg/kg 57.6 103 75-12588 660.830.5 97.6 92.4
Lead mg/kg 57.6 89 75-12594 860.815.5 70.5 76.8
Selenium mg/kg 57.6 76 75-12578 860.8ND 43.8 47.7
Silver mg/kg 28.7 96 75-12596 530.4ND 27.8 29.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 29 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/15350
EPA 3010
EPA 6010
6010 MET TCLP
Associated Lab Samples:92190644003, 92190644004, 92190644006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1149132
Associated Lab Samples:92190644003, 92190644004, 92190644006
Matrix:Water
Analyzed
Arsenic mg/L ND 0.050 03/04/14 14:01
Barium mg/L ND 0.25 03/04/14 14:01
Cadmium mg/L ND 0.0050 03/04/14 14:01
Chromium mg/L ND 0.025 03/04/14 14:01
Lead mg/L ND 0.025 03/04/14 14:01
Selenium mg/L ND 0.10 03/04/14 14:01
Silver mg/L ND 0.025 03/04/14 14:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1149133LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/L 2.62.5 106 80-120
Barium mg/L 2.22.5 90 80-120
Cadmium mg/L 2.42.5 96 80-120
Chromium mg/L 2.52.5 98 80-120
Lead mg/L 2.32.5 93 80-120
Selenium mg/L 2.72.5 108 80-120
Silver mg/L 1.31.2 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1149134MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190644003
1149135
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic mg/L 2.5 108 75-125104 42.5ND 2.7 2.6
Barium mg/L 2.5 92 75-12588 32.50.82 3.1 3.0
Cadmium mg/L 2.5 98 75-12595 42.5ND 2.4 2.4
Chromium mg/L 2.5 100 75-12596 42.5ND 2.5 2.4
Lead mg/L 2.5 95 75-12592 42.50.064 2.4 2.4
Selenium mg/L 2.5 109 75-125106 32.5ND 2.7 2.7
Silver mg/L 1.2 102 75-125100 21.2ND 1.3 1.2
REPORT OF LABORATORY ANALYSIS
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Page 30 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/25876
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1143872
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.2 02/24/14 14:34
1,1,1-Trichloroethane ug/kg ND 5.2 02/24/14 14:34
1,1,2,2-Tetrachloroethane ug/kg ND 5.2 02/24/14 14:34
1,1,2-Trichloroethane ug/kg ND 5.2 02/24/14 14:34
1,1-Dichloroethane ug/kg ND 5.2 02/24/14 14:34
1,1-Dichloroethene ug/kg ND 5.2 02/24/14 14:34
1,1-Dichloropropene ug/kg ND 5.2 02/24/14 14:34
1,2,3-Trichlorobenzene ug/kg ND 5.2 02/24/14 14:34
1,2,3-Trichloropropane ug/kg ND 5.2 02/24/14 14:34
1,2,4-Trichlorobenzene ug/kg ND 5.2 02/24/14 14:34
1,2,4-Trimethylbenzene ug/kg ND 5.2 02/24/14 14:34
1,2-Dibromo-3-chloropropane ug/kg ND 5.2 02/24/14 14:34
1,2-Dibromoethane (EDB)ug/kg ND 5.2 02/24/14 14:34
1,2-Dichlorobenzene ug/kg ND 5.2 02/24/14 14:34
1,2-Dichloroethane ug/kg ND 5.2 02/24/14 14:34
1,2-Dichloropropane ug/kg ND 5.2 02/24/14 14:34
1,3,5-Trimethylbenzene ug/kg ND 5.2 02/24/14 14:34
1,3-Dichlorobenzene ug/kg ND 5.2 02/24/14 14:34
1,3-Dichloropropane ug/kg ND 5.2 02/24/14 14:34
1,4-Dichlorobenzene ug/kg ND 5.2 02/24/14 14:34
2,2-Dichloropropane ug/kg ND 5.2 02/24/14 14:34
2-Butanone (MEK)ug/kg ND 104 02/24/14 14:34
2-Chlorotoluene ug/kg ND 5.2 02/24/14 14:34
2-Hexanone ug/kg ND 51.9 02/24/14 14:34
4-Chlorotoluene ug/kg ND 5.2 02/24/14 14:34
4-Methyl-2-pentanone (MIBK)ug/kg ND 51.9 02/24/14 14:34
Acetone ug/kg ND 104 02/24/14 14:34
Benzene ug/kg ND 5.2 02/24/14 14:34
Bromobenzene ug/kg ND 5.2 02/24/14 14:34
Bromochloromethane ug/kg ND 5.2 02/24/14 14:34
Bromodichloromethane ug/kg ND 5.2 02/24/14 14:34
Bromoform ug/kg ND 5.2 02/24/14 14:34
Bromomethane ug/kg ND 10.4 02/24/14 14:34
Carbon tetrachloride ug/kg ND 5.2 02/24/14 14:34
Chlorobenzene ug/kg ND 5.2 02/24/14 14:34
Chloroethane ug/kg ND 10.4 02/24/14 14:34
Chloroform ug/kg ND 5.2 02/24/14 14:34
Chloromethane ug/kg ND 10.4 02/24/14 14:34
cis-1,2-Dichloroethene ug/kg ND 5.2 02/24/14 14:34
cis-1,3-Dichloropropene ug/kg ND 5.2 02/24/14 14:34
Dibromochloromethane ug/kg ND 5.2 02/24/14 14:34
Dibromomethane ug/kg ND 5.2 02/24/14 14:34
Dichlorodifluoromethane ug/kg ND 10.4 02/24/14 14:34
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 31 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1143872
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.2 02/24/14 14:34
Ethylbenzene ug/kg ND 5.2 02/24/14 14:34
Hexachloro-1,3-butadiene ug/kg ND 5.2 02/24/14 14:34
Isopropylbenzene (Cumene)ug/kg ND 5.2 02/24/14 14:34
m&p-Xylene ug/kg ND 10.4 02/24/14 14:34
Methyl-tert-butyl ether ug/kg ND 5.2 02/24/14 14:34
Methylene Chloride ug/kg ND 20.7 02/24/14 14:34
n-Butylbenzene ug/kg ND 5.2 02/24/14 14:34
n-Propylbenzene ug/kg ND 5.2 02/24/14 14:34
Naphthalene ug/kg ND 5.2 02/24/14 14:34
o-Xylene ug/kg ND 5.2 02/24/14 14:34
p-Isopropyltoluene ug/kg ND 5.2 02/24/14 14:34
sec-Butylbenzene ug/kg ND 5.2 02/24/14 14:34
Styrene ug/kg ND 5.2 02/24/14 14:34
tert-Butylbenzene ug/kg ND 5.2 02/24/14 14:34
Tetrachloroethene ug/kg ND 5.2 02/24/14 14:34
Toluene ug/kg ND 5.2 02/24/14 14:34
trans-1,2-Dichloroethene ug/kg ND 5.2 02/24/14 14:34
trans-1,3-Dichloropropene ug/kg ND 5.2 02/24/14 14:34
Trichloroethene ug/kg ND 5.2 02/24/14 14:34
Trichlorofluoromethane ug/kg ND 5.2 02/24/14 14:34
Vinyl acetate ug/kg ND 51.9 02/24/14 14:34
Vinyl chloride ug/kg ND 10.4 02/24/14 14:34
Xylene (Total)ug/kg ND 10.4 02/24/14 14:34
1,2-Dichloroethane-d4 (S)%91 70-132 02/24/14 14:34
4-Bromofluorobenzene (S)%96 70-130 02/24/14 14:34
Toluene-d8 (S)%111 70-130 02/24/14 14:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1143873LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 51.649.7 104 70-131
1,1,1-Trichloroethane ug/kg 61.049.7 123 70-141
1,1,2,2-Tetrachloroethane ug/kg 45.249.7 91 70-130
1,1,2-Trichloroethane ug/kg 57.549.7 116 70-132
1,1-Dichloroethane ug/kg 59.049.7 119 70-143
1,1-Dichloroethene ug/kg 61.049.7 123 70-137
1,1-Dichloropropene ug/kg 57.249.7 115 70-135
1,2,3-Trichlorobenzene ug/kg 51.949.7 104 69-153
1,2,3-Trichloropropane ug/kg 48.549.7 98 70-130
1,2,4-Trichlorobenzene ug/kg 46.849.7 94 55-171
1,2,4-Trimethylbenzene ug/kg 47.449.7 95 70-149
1,2-Dibromo-3-chloropropane ug/kg 51.749.7 104 68-141
1,2-Dibromoethane (EDB)ug/kg 53.049.7 107 70-130
1,2-Dichlorobenzene ug/kg 49.949.7 100 70-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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Huntersville, NC 28078
[phone]
Page 32 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1143873LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane ug/kg 59.749.7 120 70-137
1,2-Dichloropropane ug/kg 55.249.7 111 70-133
1,3,5-Trimethylbenzene ug/kg 47.749.7 96 70-143
1,3-Dichlorobenzene ug/kg 47.349.7 95 70-144
1,3-Dichloropropane ug/kg 52.449.7 106 70-132
1,4-Dichlorobenzene ug/kg 48.649.7 98 70-142
2,2-Dichloropropane ug/kg 58.549.7 118 68-152
2-Butanone (MEK)ug/kg 11599.4 116 70-149
2-Chlorotoluene ug/kg 48.349.7 97 70-141
2-Hexanone ug/kg 93.299.4 94 70-149
4-Chlorotoluene ug/kg 49.549.7 100 70-149
4-Methyl-2-pentanone (MIBK)ug/kg 99.199.4 100 70-153
Acetone ug/kg 12399.4 124 70-157
Benzene ug/kg 56.149.7 113 70-130
Bromobenzene ug/kg 49.449.7 99 70-141
Bromochloromethane ug/kg 63.349.7 127 70-149
Bromodichloromethane ug/kg 55.749.7 112 70-130
Bromoform ug/kg 45.549.7 92 70-131
Bromomethane ug/kg 78.8 L349.7 159 64-136
Carbon tetrachloride ug/kg 52.849.7 106 70-154
Chlorobenzene ug/kg 48.849.7 98 70-135
Chloroethane ug/kg 62.749.7 126 68-151
Chloroform ug/kg 60.449.7 122 70-130
Chloromethane ug/kg 56.849.7 114 70-132
cis-1,2-Dichloroethene ug/kg 60.149.7 121 70-140
cis-1,3-Dichloropropene ug/kg 54.049.7 109 70-137
Dibromochloromethane ug/kg 47.849.7 96 70-130
Dibromomethane ug/kg 55.049.7 111 70-136
Dichlorodifluoromethane ug/kg 55.349.7 111 36-148
Diisopropyl ether ug/kg 56.549.7 114 70-139
Ethylbenzene ug/kg 48.849.7 98 70-137
Hexachloro-1,3-butadiene ug/kg 50.949.7 102 70-145
Isopropylbenzene (Cumene)ug/kg 50.749.7 102 70-141
m&p-Xylene ug/kg 99.699.4 100 70-140
Methyl-tert-butyl ether ug/kg 66.149.7 133 45-150
Methylene Chloride ug/kg 58.649.7 118 70-133
n-Butylbenzene ug/kg 47.049.7 95 65-155
n-Propylbenzene ug/kg 51.249.7 103 70-148
Naphthalene ug/kg 52.149.7 105 70-148
o-Xylene ug/kg 50.349.7 101 70-141
p-Isopropyltoluene ug/kg 49.749.7 100 70-148
sec-Butylbenzene ug/kg 51.049.7 103 70-145
Styrene ug/kg 51.249.7 103 70-138
tert-Butylbenzene ug/kg 52.249.7 105 70-143
Tetrachloroethene ug/kg 47.749.7 96 70-140
Toluene ug/kg 52.349.7 105 70-130
trans-1,2-Dichloroethene ug/kg 59.449.7 119 70-136
trans-1,3-Dichloropropene ug/kg 53.249.7 107 70-138
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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[phone]
Page 33 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1143873LABORATORY CONTROL SAMPLE:
LCSSpike
Trichloroethene ug/kg 55.249.7 111 70-132
Trichlorofluoromethane ug/kg 64.749.7 130 69-134
Vinyl acetate ug/kg 92.8 F399.4 93 24-161
Vinyl chloride ug/kg 61.349.7 123 55-140
Xylene (Total)ug/kg 150149 101 70-141
1,2-Dichloroethane-d4 (S)%115 70-132
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
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Page 34 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/26043
EPA 3546
EPA 8015 Modified
8015 Solid GCSV
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1142830
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Matrix:Solid
Analyzed
Diesel Components mg/kg ND 5.0 02/22/14 14:47
n-Pentacosane (S)%78 41-119 02/22/14 14:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1142831LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1142833
Diesel Components mg/kg 51.666.7 77 49-1137952.6 2 30
n-Pentacosane (S)%88 41-11973
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1143312MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92190639002
1143313
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Diesel Components mg/kg 73.9 85 10-14647 2073.990.5 153 125
n-Pentacosane (S)%72 41-11961
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/26042
EPA 3546
EPA 8270
8270 Solid MSSV Microwave PAH
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1142828
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Matrix:Solid
Analyzed
1-Methylnaphthalene ug/kg ND 330 02/24/14 10:04
2-Methylnaphthalene ug/kg ND 330 02/24/14 10:04
Acenaphthene ug/kg ND 330 02/24/14 10:04
Acenaphthylene ug/kg ND 330 02/24/14 10:04
Anthracene ug/kg ND 330 02/24/14 10:04
Benzo(a)anthracene ug/kg ND 330 02/24/14 10:04
Benzo(a)pyrene ug/kg ND 330 02/24/14 10:04
Benzo(b)fluoranthene ug/kg ND 330 02/24/14 10:04
Benzo(g,h,i)perylene ug/kg ND 330 02/24/14 10:04
Benzo(k)fluoranthene ug/kg ND 330 02/24/14 10:04
Chrysene ug/kg ND 330 02/24/14 10:04
Dibenz(a,h)anthracene ug/kg ND 330 02/24/14 10:04
Fluoranthene ug/kg ND 330 02/24/14 10:04
Fluorene ug/kg ND 330 02/24/14 10:04
Indeno(1,2,3-cd)pyrene ug/kg ND 330 02/24/14 10:04
Naphthalene ug/kg ND 330 02/24/14 10:04
Phenanthrene ug/kg ND 330 02/24/14 10:04
Pyrene ug/kg ND 330 02/24/14 10:04
2-Fluorobiphenyl (S)%83 30-110 02/24/14 10:04
Nitrobenzene-d5 (S)%76 23-110 02/24/14 10:04
Terphenyl-d14 (S)%96 28-110 02/24/14 10:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1142829LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/kg 14501670 87 45-105
2-Methylnaphthalene ug/kg 15401670 92 39-112
Acenaphthene ug/kg 13201670 79 38-117
Acenaphthylene ug/kg 14001670 84 46-107
Anthracene ug/kg 14701670 88 50-110
Benzo(a)anthracene ug/kg 14001670 84 47-116
Benzo(a)pyrene ug/kg 15801670 95 47-106
Benzo(b)fluoranthene ug/kg 14201670 85 47-109
Benzo(g,h,i)perylene ug/kg 15501670 93 39-115
Benzo(k)fluoranthene ug/kg 13801670 83 45-117
Chrysene ug/kg 14901670 90 49-110
Dibenz(a,h)anthracene ug/kg 15901670 95 43-116
Fluoranthene ug/kg 15501670 93 50-114
Fluorene ug/kg 14001670 84 46-114
Indeno(1,2,3-cd)pyrene ug/kg 16101670 97 42-115
Naphthalene ug/kg 14101670 85 41-110
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
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[phone]
Page 36 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1142829LABORATORY CONTROL SAMPLE:
LCSSpike
Phenanthrene ug/kg 14301670 86 50-110
Pyrene ug/kg 14501670 87 45-114
2-Fluorobiphenyl (S)%83 30-110
Nitrobenzene-d5 (S)%79 23-110
Terphenyl-d14 (S)%94 28-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/6265
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92190644001, 92190644002, 92190644003, 92190644004, 92190644005, 92190644006, 92190644007
Parameter Units
Dup
Result QualifiersRPDResult
92190479001
1143347SAMPLE DUPLICATE:
Percent Moisture %19.8 420.6
Parameter Units
Dup
Result QualifiersRPDResult
92190644009
1143348SAMPLE DUPLICATE:
Percent Moisture %32.2 131.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 42
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The reaction of the soil preservative, sodium bisulfate, is known to react with humic acid in soils to produce ketones.
Based upon method blank results, the laboratory feels the ketones in this sample are a result of that reaction.A+
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 42
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92190644001 OEXT/26043 GCSV/16735SOIL CUTTING PAD 1 STOCK 1 EPA 3546 EPA 8015 Modified
92190644002 OEXT/26043 GCSV/16735SOIL CUTTING PAD 1 STOCK 2 EPA 3546 EPA 8015 Modified
92190644003 OEXT/26043 GCSV/16735SOIL CUTTING PAD 1 STOCK 3 EPA 3546 EPA 8015 Modified
92190644004 OEXT/26043 GCSV/16735SOIL CUTTING PAD 1 STOCK 4 EPA 3546 EPA 8015 Modified
92190644005 OEXT/26043 GCSV/16735SOIL CUTTING PAD 1 STOCK 5 EPA 3546 EPA 8015 Modified
92190644006 OEXT/26043 GCSV/16735SOIL CUTTING PAD 1 STOCK 6 EPA 3546 EPA 8015 Modified
92190644007 OEXT/26043 GCSV/16735SOIL CUTTING PAD 1 STOCK 7 EPA 3546 EPA 8015 Modified
92190644001 MPRP/15295 ICP/13878SOIL CUTTING PAD 1 STOCK 1 EPA 3050 EPA 6010
92190644002 MPRP/15295 ICP/13878SOIL CUTTING PAD 1 STOCK 2 EPA 3050 EPA 6010
92190644003 MPRP/15295 ICP/13878SOIL CUTTING PAD 1 STOCK 3 EPA 3050 EPA 6010
92190644004 MPRP/15295 ICP/13878SOIL CUTTING PAD 1 STOCK 4 EPA 3050 EPA 6010
92190644005 MPRP/15295 ICP/13878SOIL CUTTING PAD 1 STOCK 5 EPA 3050 EPA 6010
92190644006 MPRP/15295 ICP/13878SOIL CUTTING PAD 1 STOCK 6 EPA 3050 EPA 6010
92190644007 MPRP/15295 ICP/13878SOIL CUTTING PAD 1 STOCK 7 EPA 3050 EPA 6010
92190644003 MPRP/15350 ICP/13923SOIL CUTTING PAD 1 STOCK 3 EPA 3010 EPA 6010
92190644004 MPRP/15350 ICP/13923SOIL CUTTING PAD 1 STOCK 4 EPA 3010 EPA 6010
92190644006 MPRP/15350 ICP/13923SOIL CUTTING PAD 1 STOCK 6 EPA 3010 EPA 6010
92190644003 MERP/6263 MERC/6038SOIL CUTTING PAD 1 STOCK 3 EPA 7470 EPA 7470
92190644004 MERP/6263 MERC/6038SOIL CUTTING PAD 1 STOCK 4 EPA 7470 EPA 7470
92190644006 MERP/6263 MERC/6038SOIL CUTTING PAD 1 STOCK 6 EPA 7470 EPA 7470
92190644001 MERP/6223 MERC/6000SOIL CUTTING PAD 1 STOCK 1 EPA 7471 EPA 7471
92190644002 MERP/6223 MERC/6000SOIL CUTTING PAD 1 STOCK 2 EPA 7471 EPA 7471
92190644003 MERP/6223 MERC/6000SOIL CUTTING PAD 1 STOCK 3 EPA 7471 EPA 7471
92190644004 MERP/6223 MERC/6000SOIL CUTTING PAD 1 STOCK 4 EPA 7471 EPA 7471
92190644005 MERP/6223 MERC/6000SOIL CUTTING PAD 1 STOCK 5 EPA 7471 EPA 7471
92190644006 MERP/6223 MERC/6000SOIL CUTTING PAD 1 STOCK 6 EPA 7471 EPA 7471
92190644007 MERP/6223 MERC/6000SOIL CUTTING PAD 1 STOCK 7 EPA 7471 EPA 7471
92190644001 OEXT/26042 MSSV/8774SOIL CUTTING PAD 1 STOCK 1 EPA 3546 EPA 8270
92190644002 OEXT/26042 MSSV/8774SOIL CUTTING PAD 1 STOCK 2 EPA 3546 EPA 8270
92190644003 OEXT/26042 MSSV/8774SOIL CUTTING PAD 1 STOCK 3 EPA 3546 EPA 8270
92190644004 OEXT/26042 MSSV/8774SOIL CUTTING PAD 1 STOCK 4 EPA 3546 EPA 8270
92190644005 OEXT/26042 MSSV/8774SOIL CUTTING PAD 1 STOCK 5 EPA 3546 EPA 8270
92190644006 OEXT/26042 MSSV/8774SOIL CUTTING PAD 1 STOCK 6 EPA 3546 EPA 8270
92190644007 OEXT/26042 MSSV/8774SOIL CUTTING PAD 1 STOCK 7 EPA 3546 EPA 8270
92190644001 MSV/25876SOIL CUTTING PAD 1 STOCK 1 EPA 8260
92190644002 MSV/25876SOIL CUTTING PAD 1 STOCK 2 EPA 8260
92190644003 MSV/25876SOIL CUTTING PAD 1 STOCK 3 EPA 8260
92190644004 MSV/25876SOIL CUTTING PAD 1 STOCK 4 EPA 8260
92190644005 MSV/25876SOIL CUTTING PAD 1 STOCK 5 EPA 8260
92190644006 MSV/25876SOIL CUTTING PAD 1 STOCK 6 EPA 8260
92190644007 MSV/25876SOIL CUTTING PAD 1 STOCK 7 EPA 8260
92190644001 PMST/6265SOIL CUTTING PAD 1 STOCK 1 ASTM D2974-87
92190644002 PMST/6265SOIL CUTTING PAD 1 STOCK 2 ASTM D2974-87
92190644003 PMST/6265SOIL CUTTING PAD 1 STOCK 3 ASTM D2974-87
92190644004 PMST/6265SOIL CUTTING PAD 1 STOCK 4 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 42
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92190644
CHARLOTTE CHEMICAL
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92190644005 PMST/6265SOIL CUTTING PAD 1 STOCK 5 ASTM D2974-87
92190644006 PMST/6265SOIL CUTTING PAD 1 STOCK 6 ASTM D2974-87
92190644007 PMST/6265SOIL CUTTING PAD 1 STOCK 7 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2014 04:46 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 42
Page 42 of 42
From: Franchina, Dave
Sent: Monday, May 12, 2014 10:25 AM
To: Minnich, Carolyn
Subject: RE: Charlotte Chemical Laboratories/1100 South Blvd, Charlotte, NC -- Soil Management
Question

Thanks very much, Carolyn. I really appreciate the prompt turn.

Regards,
Dave

David A. Franchina
K&L Gates LLP
214 North Tryon Street
47th Floor
Charlotte, NC 28202
Phone: [phone]
Fax: [phone]
[e-mail]
www.klgates.com

From: Minnich, Carolyn [mailto:[e-mail]]
Sent: Monday, May 12, 2014 10:13 AM
To: Franchina, Dave
Subject: RE: Charlotte Chemical Laboratories/1100 South Blvd, Charlotte, NC -- Soil Management
Question

Dave:

Based on the information presented below, our telephone call, and analytical data provided, the
developer may do the following with the approval of the NC Brownfields Program: 1) move the Stockpile
10 soils as proposed and (2) does not need to add data regarding the Stockpile 10 soils to the
Brownfields plat. If you have any questions or comments, please contact me.

Carolyn Minnich
------------------------------------------------------
Brownfields Project Manager
NCDENR-DWM
704/661-0330
www.ncbrownfields.org
Come Clean Up With Us!
------------------------------------------------------
Email correspondence to and from this address is subject to the North Carolina Public Records Law and
may be disclosed to third parties unless the content is exempt by statute or other regulation.

From: Franchina, Dave [mailto:[e-mail]]
Sent: Monday, May 12, 2014 10:03 AM
To: Minnich, Carolyn
Subject: Charlotte Chemical Laboratories/1100 South Blvd, Charlotte, NC -- Soil Management Question

Carolyn,

Hope you enjoyed the weekend. Following up on our conversation last week, the developer would like
to get confirmation that it can take certain potentially impacted soils from the west-northwest portion
of the property that are generated through the development of geopiers, test them to confirm they
meet residential standards (or, as noted below, naturally occurring concentrations), and if they do,
move them to a nearby portion of the site for reuse.

Over the weekend, we received the enclosed sampling results. Stock-8 is a sample taken from Stockpile
8, a stockpile that contains less than 250 cubic yards of soil. Stock 10-A and 10-B come from Stockpile
10, a stockpile that contains less than 500 cubic yards of soil. (During our call, we mentioned 1500 cubic
yards of soil; there are in fact 1500 cubic yards of soil for the developer to manage, but the remainder is
either documented clean from a presumed clean portion of the property (and so will be reused on site)
or dirty (and so will be thrown out), so no need to discuss them here.)

Stock-8 has mercury exceeding residential standards. The developer’s current plan is to dispose of them
offsite in an appropriately permitted facility.

Stock-10A and 10B are non-detect or below residential standards for VOCs and SVOCs. All metals are
below all residential standards, except for arsenic. Arsenic, however, is present in concentrations that
are entirely consistent with naturally occurring concentrations in the Piedmont (0.97 mg/kg in 10A, and
3.9 mg/kg in 10B), and, as you’ll recall, arsenic is not a contaminant of concern at the site. Thus, we do
not view the soils as “contaminated” for purposes of adding data regarding them to the Brownfields
plat.

As we mentioned last week, the developer’s plan is to use the Stockpile 10 soils beneath a ramp that will
connect levels of the subsurface parking on the property (in other words, they will remain under a paved
surface). According to the SMP, because of the initial location of these soils, moving them to a different
portion on the property requires Brownfields OK. And, as you’ll recall, the developer would like to
ensure that if it reuses the Stockpile 10 soils, it will not need to add any additional data to the
Brownfields plat.

Can you please confirm that (1) developer can move the Stockpile 10 soils as proposed and (2)
developer does not need to add data regarding the Stockpile 10 soils to the Brownfields plat? An email
response will suffice.
By the way, we will memorialize all soil management and disposal in a report to be provided to
Brownfields in the future.
Please contact me with questions, and thanks.
Regards,
Dave

David A. Franchina
K&L Gates LLP
214 North Tryon Street
47th Floor
Charlotte, NC 28202
Phone: [phone]
Fax: [phone]
[e-mail]
www.klgates.com

From: Franchina, Dave
Sent: Tuesday, September 23, 2014 3:12 PM
To: Minnich, Carolyn
Subject: RE: Charlotte Chemical Laboratory/1100 South Boulevard, Charlotte -- Impacts Detected in One
Geopier Boring

Thanks very much, Carolyn, for the prompt response.

Regards,
Dave

David A. Franchina
K&L Gates LLP
214 North Tryon Street
47th Floor
Charlotte, NC 28202
Phone: [phone]
Fax: [phone]
[e-mail]
www.klgates.com

From: Minnich, Carolyn [mailto:[e-mail]]
Sent: Tuesday, September 23, 2014 2:32 PM
To: Franchina, Dave
Subject: RE: Charlotte Chemical Laboratory/1100 South Boulevard, Charlotte -- Impacts Detected in One
Geopier Boring

Dave:

Thank you for the follow up data. No additional informational data needs to added to the Brownfields
Plat map at this time.

Thank you.
CFM

Carolyn Minnich, Brownfields Project Manager www.ncbrownfields.org 704/661-0330
___________________________________________________________________________________________________________________________________________________________________________________________
__________________ Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be
disclosed to third parties unless the content is exempt by statute or other regulation.

From: Franchina, Dave [mailto:[e-mail]]
Sent: Sunday, September 21, 2014 11:13 PM
To: Minnich, Carolyn
Subject: RE: Charlotte Chemical Laboratory/1100 South Boulevard, Charlotte -- Impacts Detected in One
Geopier Boring

Carolyn,

I wanted to follow up on the email below and our subsequent conversation on it.

We’ve followed up to determine whether screening was performed as digging in the excavation at issue
proceeded. Due to safety concerns, EFI was not able to take a sample or otherwise access the
excavation itself as soils were removed. However, it was able to confirm that the open area around the
excavation showed no indication of impacts through soil screening with a photoionization
detector. There was also no visual evidence of an impact.

When you combine these results with the prior analysis we provided (namely, that the developer
excavated out to points on the property where prior sampling had confirmed that soils were clean), it’s
our sense that impacted soils in this area were fully excavated, and no additional data needs to be
added to the Brownfields plat. Can you please let us know if you agree?

Thanks,
Dave

David A. Franchina
K&L Gates LLP
214 North Tryon Street
47th Floor
Charlotte, NC 28202
Phone: [phone]
Fax: [phone]
[e-mail]
www.klgates.com

From: Franchina, Dave
Sent: Friday, August 15, 2014 2:34 PM
To: 'Minnich, Carolyn'
Subject: RE: Charlotte Chemical Laboratory/1100 South Boulevard, Charlotte -- Impacts Detected in One
Geopier Boring

Thanks for getting back to me, Carolyn. Since we’re in good shape so far (thanks for confirming that), I
think we can wait until we’re done with the additional soil work, and we submit a follow up report,
before we request a final note from you on this aspect of soil management. I expect an email will be
fine when the time comes.

In the meantime, can you please confirm whether the scope of work we’ve done to excavate the
impacted soils (digging out to the property boundary and to former borings that have been documented
as clean, and not seeing any additional impacts) is sufficient to avoid the addition of a note to the
plat? As you know, this developer has been working hard to avoid any additional plat notations, so if
you could confirm we’re OK on this point, it would be helpful.

Hope you have a great weekend.

Regards,
Dave

David A. Franchina
K&L Gates LLP
214 North Tryon Street
47th Floor
Charlotte, NC 28202
Phone: [phone]
Fax: [phone]
[e-mail]
www.klgates.com

From: Minnich, Carolyn [mailto:[e-mail]]
Sent: Friday, August 15, 2014 2:11 PM
To: Franchina, Dave
Subject: RE: Charlotte Chemical Laboratory/1100 South Boulevard, Charlotte -- Impacts Detected in One
Geopier Boring

Thanks for sending again and prompting me. The documents are in order and all appears well. What
do you want from me an email or letter? Want to wait until you get the other additional soil
information to me and I’ll send one letter. Please advise.

Carolyn Minnich
------------------------------------------------------
Brownfields Project Manager
NCDENR-DWM
704/661-0330
www.ncbrownfields.org
Come Clean Up With Us!
------------------------------------------------------
Email correspondence to and from this address is subject to the North Carolina Public Records Law and
may be disclosed to third parties unless the content is exempt by statute or other regulation.

From: Franchina, Dave [mailto:[e-mail]]
Sent: Wednesday, August 06, 2014 11:56 PM
To: Minnich, Carolyn
Subject: RE: Charlotte Chemical Laboratory/1100 South Boulevard, Charlotte -- Impacts Detected in One
Geopier Boring

Carolyn,

As requested, the developer has put together a report regarding the impacts detected in, and removed
from, a geopier boring. A copy is enclosed.

While the report was being put together, additional impacted soils in close proximity to the initial
geopier boring were detected. The enclosed report discusses those soils as well, though it currently
lacks information that we recognize Brownfields will need before closing out this second impact, such as
soil disposal documentation. We will expedite the processing of that documentation.

Please contact me if you have questions regarding the enclosed materials.

Regards,
Dave

David A. Franchina
K&L Gates LLP
214 North Tryon Street
47th Floor
Charlotte, NC 28202
Phone: [phone]
Fax: [phone]
[e-mail]
www.klgates.com

From: Franchina, Dave
Sent: Monday, July 21, 2014 10:02 AM
To: 'Minnich, Carolyn'
Subject: RE: Charlotte Chemical Laboratory/1100 South Boulevard, Charlotte -- Impacts Detected in One
Geopier Boring

Carolyn,

Thanks for the prompt feedback. I believe the answers to your questions are: (1) soils in the
surrounding piers were clean; (2) some overexcavation of the affected boring (#159) did occur; and (3)
the affected soils have been disposed off-site already. We will expedite a report to you that confirms
the answers to the foregoing questions, and that includes the other information you’ve requested.

Regards,
Dave

David A. Franchina
K&L Gates LLP
214 North Tryon Street
47th Floor
Charlotte, NC 28202
Phone: [phone]
Fax: [phone]
[e-mail]
www.klgates.com

From: Minnich, Carolyn [mailto:[e-mail]]
Sent: Monday, July 21, 2014 9:57 AM
To: Franchina, Dave
Subject: RE: Charlotte Chemical Laboratory/1100 South Boulevard, Charlotte -- Impacts Detected in One
Geopier Boring

Dave:

Thank you for the update. What was the condition of the soils in the surrounding piers? Did you over
excavate or just the amount needed for the pier? Based on the email below, it sounds like the soils have
since been removed and disposed of. Please expedite a summary letter similar to the one below with
lab data, disposal records, and final estimated removed for the project file.

Thank you.

Carolyn Minnich
------------------------------------------------------
Brownfields Project Manager
NCDENR-DWM
704/661-0330
www.ncbrownfields.org
Come Clean Up With Us!
------------------------------------------------------
Email correspondence to and from this address is subject to the North Carolina Public Records Law and
may be disclosed to third parties unless the content is exempt by statute or other regulation.

From: Franchina, Dave [mailto:[e-mail]]
Sent: Sunday, July 20, 2014 1:00 PM
To: Minnich, Carolyn
Subject: Charlotte Chemical Laboratory/1100 South Boulevard, Charlotte -- Impacts Detected in One
Geopier Boring

Carolyn,

I wanted to let you know about a small area of impacted soils at the referenced Brownfields site that
was detected several months ago, and due to an oversight Brownfields was not notified of the situation
promptly.

In February, during the installation of pier 159 (see enclosed figure for approximate location on site),
odors and discolored soils were detected, as well as debris. Excavated materials, about a dump truck
load, were stockpiled and placed under plastic sheeting. Sampling revealed petroleum
contamination. A copy of the sampling report from the stockpiled soils is enclosed.

The area of contamination appears to be extremely limited. As reflected on the enclosed figure, the
area of boring 159 is very close to former sample location SB-12, which as noted in the SMP, was pretty
much clean. (Copy of SMP enclosed for ease of reference.) So too were all adjacent borings.

Based on historical records, the source of this limited contamination is not clear. Our review of relevant
Sanborn maps (copy enclosed), suggests that boring 159 was located behind the former Charlotte
Chemical Laboratory or behind a former textile operation. The contamination does not appear to be
associated with an underground storage tank, either based upon field observations or based upon the
Sanborns (which do not indicate tanks are present in this vicinity).

As part of its ongoing effort to avoid adding additional data points to the Brownfields plat, the developer
will not use any of these soils on-site. They all have been disposed off-site at a licensed disposal facility.

We will provide further detail on this matter, including manifests associated with soil disposal, in the
developer’s final report on soil management. Please let us know if you have questions in the meantime.

Regards,
Dave

David A. Franchina
K&L Gates LLP
214 North Tryon Street
47th Floor
Charlotte, NC 28202
Phone: [phone]
Fax: [phone]
[e-mail]
www.klgates.com

APPENDIX 19

VIBRO-PIER / PAD 3 LABORATORY REPORT

APPENDIX 20

SOIL DISPOSAL MANIFESTS

Activity by Customer and Contract
Date Range: 2/16/2015 to 2/16/2015
Customer Range: 100608 to 100608
All Contracts
Both Intercompany and 3rd Party
Details
Tracking
QtyTonsVehicleDateTicket
In/
OutMaterial
Wt
Out Pounds
U
O
MOrigin
Wt
In
Reference/
BOL
7 0.00 125.93 100608 J. O. FLOWE GRADING
Ticket Count
Contract - 5010149672-1 7 0.00 125.93Ticket Count
2/16/15 17.03 0.00 1113419 DT341 ISW-CONT SOIL 60,740 26,680 34,060 YDMECKLENBURG2187611
2/16/15 17.94 0.00 1113431 dt585 ISW-CONT SOIL 65,420 29,540 35,880 YDMECKLENBURG2187610
2/16/15 18.73 0.00 1113461 DT329 ISW-CONT SOIL 64,100 26,640 37,460 YDMECKLENBURG2187609
2/16/15 17.78 0.00 1113505 DT341 ISW-CONT SOIL 62,240 26,680 35,560 YDMECKLENBURG2187582
2/16/15 19.39 0.00 1113542 dt585 ISW-CONT SOIL 68,320 29,540 38,780 YDMECKLENBURG2187608
2/16/15 16.93 0.00 1113565 DT329 ISW-CONT SOIL 60,500 26,640 33,860 YDMECKLENBURG2187607
2/16/15 18.13 0.00 1113588 DT341 ISW-CONT SOIL 62,940 26,680 36,260 YDMECKLENBURG2187606
125.93 7 Grand TotalsGrand Total Ticket Count
3/19/2015 9:46:52AM Page 1 of 1BFI/CMS LANDFILL - 5010
All Ticket Types All Facilities
Detail Customer Activity Report
March 01, 2015 to March 31, 2015
Specific Customer: 100608History and Waiting
100608- J. O. FLOWE GRADING
Ticket
Date
Facility & Ticket
Number MaterialContractTruck #
Billing
QuantityContainer
1126114 5010154432 DT34103/26/2015 16.78 TNSW-CONT SOILI Y6
1126187 5010154432 DT34103/26/2015 17.86 TNSW-CONT SOILI Y6
1126212 5010154432 DT33103/26/2015 11.84 TNSW-CONT SOILI Y6
Customer Totals: Tickets Reported: 3 Items Reported: 3
Weight Volume Count
Inbound Outbound Inbound Outbound Inbound Outbound
Material Summary Billing
Quantity
TN 0.00 46.48 0.00 0.00 0.00 0.00 YD 46.48 TNVG - SW-CONT SOIL
3Tickets Reported:Items Reported: 3
eurydo 04/22/2015 2:59 PM BFI/CMS LANDFILL - 5010 Page 1 of 1
All Ticket Types All Facilities
Detail Customer Activity Report
April 01, 2015 to April 21, 2015
Specific Customer: 100608History and Waiting
100608- J. O. FLOWE GRADING
Ticket
Date
Facility & Ticket
Number MaterialContractTruck #
Billing
QuantityContainer
1129563 5010154432 DT32904/07/2015 17.24 TNSW-CONT SOILIY6
1129605 5010154432 DT34104/07/2015 17.92 TNSW-CONT SOILIY6
1129766 5010154432 DT32904/07/2015 18.65 TNSW-CONT SOILI Y6
1129805 5010154432 DT34104/07/2015 20.88 TNSW-CONT SOILI Y6
1131298 5010154432 dt58504/13/2015 20.87 TNSW-CONT SOILI Y6
1131402 5010154432 dt58504/13/2015 22.86 TNSW-CONT SOILI Y6
1131490 5010154432 dt58504/13/2015 22.43 TNSW-CONT SOILI Y6
1131570 5010154432 dt58504/13/2015 23.67 TNSW-CONT SOILI Y6
1132206 5010154432 DT33104/15/2015 14.42 TNSW-CONT SOILI Y6
1132216 5010154432 DT34104/15/2015 20.06 TNSW-CONT SOILI Y6
1132238 5010154432 dt58504/15/2015 19.55 TNSW-CONT SOILI Y6
1132254 5010154432 dt75504/15/2015 20.42 TNSW-CONT SOILI Y6
1133892 5010154432 dt58504/21/2015 21.68 TNSW-CONT SOILI Y6
Customer Totals: Tickets Reported: 13 Items Reported: 13
Weight Volume Count
Inbound Outbound Inbound Outbound Inbound Outbound
Material Summary Billing
Quantity
TN 0.00 260.65 0.00 0.00 0.00 0.00 YD 260.65 TNVG - SW-CONT SOIL
13Tickets Reported:Items Reported: 13
eurydo 04/22/2015 2:39 PM BFI/CMS LANDFILL - 5010 Page 1 of 1
All Ticket Types All Facilities
Detail Contract Activity Report
April 01, 2015 to May 14, 2015
Specific Contract: 5010154432History and Waiting
5010154432
Ticket
Date
Facility &
Ticket Number MaterialCustomer
Billing
QuantityTruck
1129563 04/07/2015 17.24 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 DT329
1129605 04/07/2015 17.92 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 DT341
1129766 04/07/2015 18.65 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 DT329
1129805 04/07/2015 20.88 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 DT341
1131298 04/13/2015 20.87 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 dt585
1131402 04/13/2015 22.86 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 dt585
1131490 04/13/2015 22.43 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 dt585
1131570 04/13/2015 23.67 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 dt585
1132206 04/15/2015 14.42 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 DT331
1132216 04/15/2015 20.06 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 DT341
1132238 04/15/2015 19.55 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 dt585
1132254 04/15/2015 20.42 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 dt755
1133892 04/21/2015 21.68 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 dt585
1136518 04/28/2015 19.48 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 dt587
1139124 05/05/2015 22.91 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 dt755
1139591 05/06/2015 15.45 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 DT787
1139760 05/07/2015 20.76 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 DT699
1139885 05/07/2015 19.73 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 DT699
1140263 05/08/2015 22.37 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 dt585
1140345 05/08/2015 22.87 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 dt585
1140423 05/08/2015 21.72 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 dt585
1140486 05/08/2015 19.64 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 dt585
1140511 05/08/2015 12.65 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 dt228
1141058 05/11/2015 19.87 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 DT329
1141133 05/11/2015 22.10 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 DT329
1141186 05/12/2015 15.06 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 DT331
1141483 05/12/2015 13.64 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 DT331
1141559 05/12/2015 12.49 TNSW-CONT SOILI100608 - J. O. FLOWE GRADINGY6 DT331
Items Reported: 28Tickets Reported: 28
Weight Volume Count
Inbound Outbound Inbound Outbound Inbound Outbound
Material Summary Billing
Quantity
TN 0.00 541.39 0.00 0.00 0.00 0.00 YD 541.39 TNVG - SW-CONT SOIL
eurydo 05/15/2015 1:08 PM BFI/CMS LANDFILL - 5010 Page 1 of 2
All Ticket Types All Facilities
Detail Contract Activity Report
April 01, 2015 to May 14, 2015
Specific Contract: 5010154432History and Waiting
28Tickets Reported:Items Reported: 28
eurydo 05/15/2015 1:08 PM BFI/CMS LANDFILL - 5010 Page 2 of 2
All Ticket Types All Facilities
Detail Customer Activity Report
May 01, 2015 to May 27, 2015
Specific Customer: 100608History and Waiting
100608- J. O. FLOWE GRADING
Ticket
Date
Facility & Ticket
Number MaterialContractTruck #
Billing
QuantityContainer
1139124 5010154432 dt75505/05/2015 22.91 TNSW-CONT SOILI Y6
1139591 5010154432 DT78705/06/2015 15.45 TNSW-CONT SOILI Y6
1139760 5010154432 DT69905/07/2015 20.76 TNSW-CONT SOILI Y6
1139885 5010154432 DT69905/07/2015 19.73 TNSW-CONT SOILI Y6
1140263 5010154432 dt58505/08/2015 22.37 TNSW-CONT SOILI Y6
1140345 5010154432 dt58505/08/2015 22.87 TNSW-CONT SOILI Y6
1140423 5010154432 dt58505/08/2015 21.72 TNSW-CONT SOILI Y6
1140486 5010154432 dt58505/08/2015 19.64 TNSW-CONT SOILI Y6
1140511 5010154432 dt22805/08/2015 12.65 TNSW-CONT SOILI Y6
1141058 5010154432 DT32905/11/2015 19.87 TNSW-CONT SOILI Y6
1141133 5010154432 DT32905/11/2015 22.10 TNSW-CONT SOILI Y6
1141186 5010154432 DT33105/12/2015 15.06 TNSW-CONT SOILI Y6
1141483 5010154432 DT33105/12/2015 13.64 TNSW-CONT SOILI Y6
1141559 5010154432 DT33105/12/2015 12.49 TNSW-CONT SOILI Y6
1142629 5010154432 DT34105/14/2015 18.67 TNSW-CONT SOILI Y6
1142823 5010154432 DT34105/15/2015 18.79 TNSW-CONT SOILI Y6
1143395 5010154432 DT33105/18/2015 14.66 TNSW-CONT SOILI Y6
1143539 5010154432 DT33105/18/2015 16.46 TNSW-CONT SOILI Y6
1143635 5010154432 DT33105/18/2015 13.00 TNSW-CONT SOILI Y6
1144722 5010154432 DT34105/21/2015 19.10 TNSW-CONT SOILI Y6
1144735 5010154432 dt58505/21/2015 22.17 TNSW-CONT SOILI Y6
1144745 5010154432 dt58705/21/2015 22.12 TNSW-CONT SOILI Y6
1144759 5010154432 DT33105/21/2015 17.14 TNSW-CONT SOILI Y6
1144767 5010154432 dt75605/21/2015 20.26 TNSW-CONT SOILI Y6
1144769 5010154432 DT32905/21/2015 20.17 TNSW-CONT SOILI Y6
1144779 5010154432 dt22805/21/2015 14.57 TNSW-CONT SOILI Y6
1144788 5010154432 dt75505/21/2015 19.34 TNSW-CONT SOILI Y6
1144813 5010154432 DT34105/21/2015 20.92 TNSW-CONT SOILI Y6
1144832 5010154432 dt58505/21/2015 19.29 TNSW-CONT SOILI Y6
1144860 5010154432 dt58705/21/2015 24.70 TNSW-CONT SOILI Y6
1144873 5010154432 DT33105/21/2015 15.41 TNSW-CONT SOILI Y6
1144884 5010154432 dt22805/21/2015 15.16 TNSW-CONT SOILI Y6
1144899 5010154432 dt75605/21/2015 21.02 TNSW-CONT SOILI Y6
1144958 5010154432 DT32905/21/2015 13.53 TNSW-CONT SOILI Y6
1145067 5010154432 DT32905/21/2015 12.08 TNSW-CONT SOILI Y6
Customer Totals: Tickets Reported: 35 Items Reported: 35
eurydo 05/27/2015 2:06 PM BFI/CMS LANDFILL - 5010 Page 1 of 2
All Ticket Types All Facilities
Detail Customer Activity Report
May 01, 2015 to May 27, 2015
Specific Customer: 100608History and Waiting
Weight Volume Count
Inbound Outbound Inbound Outbound Inbound Outbound
Material Summary Billing
Quantity
TN 0.00 639.82 0.00 0.00 0.00 0.00 YD 639.82 TNVG - SW-CONT SOIL
35Tickets Reported:Items Reported: 35
eurydo 05/27/2015 2:06 PM BFI/CMS LANDFILL - 5010 Page 2 of 2

APPENDIX 21

EMAIL AND LABORATORY REPORT FOR IMPORTED SOIL

-----Original Message-----
From: Minnich, Carolyn [mailto:[e-mail]]
Sent: Tuesday, March 31, 2015 4:25 PM
To: Randy Martin
Cc: Franchina, Dave
Subject: Re: Charlotte Chemical (Pace Project # 92241627)

Sorry for delay. The soil is acceptable.
Call me if you want to discuss.

Sent from my iPhone

-----Original Message-----
From: Randy Martin [mailto:[e-mail]]
Sent: Friday, March 27, 2015 5:02 PM
To: [e-mail]
Cc: Franchina, Dave
Subject: Charlotte Chemical (Pace Project # 92241627)

Hi Carolyn,
We are dangerously close to finishing our site work at 1100 South Blvd! We have moved towards
landscaping the front of the site and need to import amended soil in our tree pits to ensure adequate
tree growth. The attached lab data represents a sample of the organic soil we will be importing. My
understanding is this sample shows arsenic above residential standards but is consistent with naturally
occurring background levels. I wanted to make sure you are comfortable with this import before we turn
the landscaping contractor loose.

I originally had 10 days to work through this approval but we are changing our sequence and would like
to move on this asap (Monday/Tuesday next week).
I realize this leave little time for your review so I'm apologizing in advance.

I've copied Dave Franchina on this email in case you have questions or if Dave feels I've left something
out.

As always, thank you for your time on this. We do appreciate your continued efforts and support on this
project.

Randy Martin, PE
Cambridge Development Group
711 Central Avenue
Charlotte, NC 28204
O 704.909.2477
C 704.719.6993

#=CL#
March 20, 2015
LIMS USE: FR - JOHN BURKART
LIMS OBJECT ID: 92241627
92241627
Project:
Pace Project No.:
RE:
Mr. John Burkart
EFI Global
9307 Monroe Road
Suite M
Charlotte, NC 28270
Charlotte Chemical
Dear Mr. Burkart:
Enclosed are the analytical results for sample(s) received by the laboratory on March 17, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
HORIZON Database Administrator
Enclosures
cc:Accounts Payable, EFI Global
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 22
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92241627
Charlotte Chemical
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 22
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92241627
Charlotte Chemical
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92241627001 Tree Soil EPA 6010 7 PASI-AJMW
EPA 7471 1 PASI-AHVK
EPA 8270 21 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CEJK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241627
Charlotte Chemical
Sample:Tree Soil Lab ID:92241627001 Collected:03/16/15 12:00 Received:03/17/15 17:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Arsenic 1.3 mg/kg 03/19/15 14:41 7440-38-203/19/15 11:110.98 1
Barium 63.8 mg/kg 03/19/15 14:41 7440-39-303/19/15 11:110.49 1
Cadmium 0.14 mg/kg 03/19/15 14:41 7440-43-903/19/15 11:110.098 1
Chromium 24.1 mg/kg 03/19/15 14:41 7440-47-303/19/15 11:110.49 1
Lead 14.0 mg/kg 03/19/15 14:41 7439-92-103/19/15 11:110.49 1
Selenium 2.7 mg/kg 03/19/15 14:41 7782-49-203/19/15 11:110.98 1
Silver ND mg/kg 03/19/15 14:41 7440-22-403/19/15 11:110.49 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.010 mg/kg 03/19/15 13:18 7439-97-6 M1,R103/19/15 11:250.0035 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV PAH Microwave
Acenaphthene ND ug/kg 03/19/15 11:54 83-32-903/18/15 14:204951
Acenaphthylene ND ug/kg 03/19/15 11:54 208-96-803/18/15 14:204951
Anthracene ND ug/kg 03/19/15 11:54 120-12-703/18/15 14:204951
Benzo(a)anthracene ND ug/kg 03/19/15 11:54 56-55-303/18/15 14:204951
Benzo(a)pyrene ND ug/kg 03/19/15 11:54 50-32-803/18/15 14:204951
Benzo(b)fluoranthene ND ug/kg 03/19/15 11:54 205-99-203/18/15 14:204951
Benzo(g,h,i)perylene ND ug/kg 03/19/15 11:54 191-24-203/18/15 14:204951
Benzo(k)fluoranthene ND ug/kg 03/19/15 11:54 207-08-903/18/15 14:204951
Chrysene ND ug/kg 03/19/15 11:54 218-01-903/18/15 14:204951
Dibenz(a,h)anthracene ND ug/kg 03/19/15 11:54 53-70-303/18/15 14:204951
Fluoranthene ND ug/kg 03/19/15 11:54 206-44-003/18/15 14:204951
Fluorene ND ug/kg 03/19/15 11:54 86-73-703/18/15 14:204951
Indeno(1,2,3-cd)pyrene ND ug/kg 03/19/15 11:54 193-39-503/18/15 14:204951
1-Methylnaphthalene ND ug/kg 03/19/15 11:54 90-12-003/18/15 14:204951
2-Methylnaphthalene ND ug/kg 03/19/15 11:54 91-57-603/18/15 14:204951
Naphthalene ND ug/kg 03/19/15 11:54 91-20-303/18/15 14:204951
Phenanthrene ND ug/kg 03/19/15 11:54 85-01-803/18/15 14:204951
Pyrene ND ug/kg 03/19/15 11:54 129-00-003/18/15 14:204951
Surrogates
Nitrobenzene-d5 (S)30 %03/19/15 11:54 4165-60-003/18/15 14:2023-110 1
2-Fluorobiphenyl (S)38 %03/19/15 11:54 321-60-803/18/15 14:2030-110 1
Terphenyl-d14 (S)40 %03/19/15 11:54 1718-51-003/18/15 14:2028-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/18/15 14:08 67-64-11871
Benzene ND ug/kg 03/18/15 14:08 71-43-29.4 1
Bromobenzene ND ug/kg 03/18/15 14:08 108-86-19.4 1
Bromochloromethane ND ug/kg 03/18/15 14:08 74-97-59.4 1
Bromodichloromethane ND ug/kg 03/18/15 14:08 75-27-49.4 1
Bromoform ND ug/kg 03/18/15 14:08 75-25-29.4 1
Bromomethane ND ug/kg 03/18/15 14:08 74-83-918.7 1
2-Butanone (MEK)ND ug/kg 03/18/15 14:08 78-93-31871
n-Butylbenzene ND ug/kg 03/18/15 14:08 104-51-89.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/20/2015 03:43 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241627
Charlotte Chemical
Sample:Tree Soil Lab ID:92241627001 Collected:03/16/15 12:00 Received:03/17/15 17:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
sec-Butylbenzene ND ug/kg 03/18/15 14:08 135-98-89.4 1
tert-Butylbenzene ND ug/kg 03/18/15 14:08 98-06-69.4 1
Carbon tetrachloride ND ug/kg 03/18/15 14:08 56-23-59.4 1
Chlorobenzene ND ug/kg 03/18/15 14:08 108-90-79.4 1
Chloroethane ND ug/kg 03/18/15 14:08 75-00-318.7 1
Chloroform ND ug/kg 03/18/15 14:08 67-66-39.4 1
Chloromethane ND ug/kg 03/18/15 14:08 74-87-318.7 1
2-Chlorotoluene ND ug/kg 03/18/15 14:08 95-49-89.4 1
4-Chlorotoluene ND ug/kg 03/18/15 14:08 106-43-49.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/18/15 14:08 96-12-89.4 1
Dibromochloromethane ND ug/kg 03/18/15 14:08 124-48-19.4 1
1,2-Dibromoethane (EDB)ND ug/kg 03/18/15 14:08 106-93-49.4 1
Dibromomethane ND ug/kg 03/18/15 14:08 74-95-39.4 1
1,2-Dichlorobenzene ND ug/kg 03/18/15 14:08 95-50-19.4 1
1,3-Dichlorobenzene ND ug/kg 03/18/15 14:08 541-73-19.4 1
1,4-Dichlorobenzene ND ug/kg 03/18/15 14:08 106-46-79.4 1
Dichlorodifluoromethane ND ug/kg 03/18/15 14:08 75-71-818.7 1
1,1-Dichloroethane ND ug/kg 03/18/15 14:08 75-34-39.4 1
1,2-Dichloroethane ND ug/kg 03/18/15 14:08 107-06-29.4 1
1,1-Dichloroethene ND ug/kg 03/18/15 14:08 75-35-49.4 1
cis-1,2-Dichloroethene ND ug/kg 03/18/15 14:08 156-59-29.4 1
trans-1,2-Dichloroethene ND ug/kg 03/18/15 14:08 156-60-59.4 1
1,2-Dichloropropane ND ug/kg 03/18/15 14:08 78-87-59.4 1
1,3-Dichloropropane ND ug/kg 03/18/15 14:08 142-28-99.4 1
2,2-Dichloropropane ND ug/kg 03/18/15 14:08 594-20-79.4 1
1,1-Dichloropropene ND ug/kg 03/18/15 14:08 563-58-69.4 1
cis-1,3-Dichloropropene ND ug/kg 03/18/15 14:08 10061-01-59.4 1
trans-1,3-Dichloropropene ND ug/kg 03/18/15 14:08 10061-02-69.4 1
Diisopropyl ether ND ug/kg 03/18/15 14:08 108-20-39.4 1
Ethylbenzene ND ug/kg 03/18/15 14:08 100-41-49.4 1
Hexachloro-1,3-butadiene ND ug/kg 03/18/15 14:08 87-68-39.4 1
2-Hexanone ND ug/kg 03/18/15 14:08 591-78-693.6 1
Isopropylbenzene (Cumene)ND ug/kg 03/18/15 14:08 98-82-89.4 1
p-Isopropyltoluene ND ug/kg 03/18/15 14:08 99-87-69.4 1
Methylene Chloride ND ug/kg 03/18/15 14:08 75-09-237.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/18/15 14:08 108-10-193.6 1
Methyl-tert-butyl ether ND ug/kg 03/18/15 14:08 1634-04-49.4 1
Naphthalene ND ug/kg 03/18/15 14:08 91-20-39.4 1
n-Propylbenzene ND ug/kg 03/18/15 14:08 103-65-19.4 1
Styrene ND ug/kg 03/18/15 14:08 100-42-59.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/18/15 14:08 630-20-69.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/18/15 14:08 79-34-59.4 1
Tetrachloroethene ND ug/kg 03/18/15 14:08 127-18-49.4 1
Toluene ND ug/kg 03/18/15 14:08 108-88-39.4 1
1,2,3-Trichlorobenzene ND ug/kg 03/18/15 14:08 87-61-69.4 1
1,2,4-Trichlorobenzene ND ug/kg 03/18/15 14:08 120-82-19.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/20/2015 03:43 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241627
Charlotte Chemical
Sample:Tree Soil Lab ID:92241627001 Collected:03/16/15 12:00 Received:03/17/15 17:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
1,1,1-Trichloroethane ND ug/kg 03/18/15 14:08 71-55-69.4 1
1,1,2-Trichloroethane ND ug/kg 03/18/15 14:08 79-00-59.4 1
Trichloroethene ND ug/kg 03/18/15 14:08 79-01-69.4 1
Trichlorofluoromethane ND ug/kg 03/18/15 14:08 75-69-49.4 1
1,2,3-Trichloropropane ND ug/kg 03/18/15 14:08 96-18-49.4 1
1,2,4-Trimethylbenzene ND ug/kg 03/18/15 14:08 95-63-69.4 1
1,3,5-Trimethylbenzene ND ug/kg 03/18/15 14:08 108-67-89.4 1
Vinyl acetate ND ug/kg 03/18/15 14:08 108-05-493.6 1
Vinyl chloride ND ug/kg 03/18/15 14:08 75-01-418.7 1
Xylene (Total)ND ug/kg 03/18/15 14:08 1330-20-718.7 1
m&p-Xylene ND ug/kg 03/18/15 14:08 179601-23-118.7 1
o-Xylene ND ug/kg 03/18/15 14:08 95-47-69.4 1
Surrogates
Toluene-d8 (S)96 %03/18/15 14:08 2037-26-5 1g70-130 1
4-Bromofluorobenzene (S)85 %03/18/15 14:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)119 %03/18/15 14:08 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 25.3 %03/18/15 14:330.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/20/2015 03:43 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241627
Charlotte Chemical
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/7677
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:92241627001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1414628
Associated Lab Samples:92241627001
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0050 03/19/15 13:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1414629LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.070.067 106 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1414630MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92241627001
1414631
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/kg M1,R1.06 80 75-12557 23.0630.010 0.062 0.050
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/20/2015 03:43 PM
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Page 7 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241627
Charlotte Chemical
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/18098
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:92241627001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1414632
Associated Lab Samples:92241627001
Matrix:Solid
Analyzed
Arsenic mg/kg ND 1.0 03/19/15 14:35
Barium mg/kg ND 0.50 03/19/15 14:35
Cadmium mg/kg ND 0.10 03/19/15 14:35
Chromium mg/kg ND 0.50 03/19/15 14:35
Lead mg/kg ND 0.50 03/19/15 14:35
Selenium mg/kg ND 1.0 03/19/15 14:35
Silver mg/kg ND 0.50 03/19/15 14:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1414633LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 49.950 100 80-120
Barium mg/kg 49.150 98 80-120
Cadmium mg/kg 49.950 100 80-120
Chromium mg/kg 49.250 98 80-120
Lead mg/kg 50.050 100 80-120
Selenium mg/kg 50.650 101 80-120
Silver mg/kg 25.625 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1414634MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92241627001
1414635
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic mg/kg 66.9 95 75-12594 166.91.3 65.5 64.7
Barium mg/kg 66.9 111 75-125115 166.963.8 160 162
Cadmium mg/kg 66.9 100 75-12599 166.90.14 67.4 66.6
Chromium mg/kg 66.9 97 75-12598 166.924.1 97.4 98.0
Lead mg/kg 66.9 85 75-12584 166.914.0 75.8 74.7
Selenium mg/kg 66.9 100 75-12599 166.92.7 70.5 69.9
Silver mg/kg 33.5 100 75-12599 133.5ND 34.0 33.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/20/2015 03:43 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241627
Charlotte Chemical
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30784
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92241627001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1413556
Associated Lab Samples:92241627001
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 4.8 03/18/15 12:48
1,1,1-Trichloroethane ug/kg ND 4.8 03/18/15 12:48
1,1,2,2-Tetrachloroethane ug/kg ND 4.8 03/18/15 12:48
1,1,2-Trichloroethane ug/kg ND 4.8 03/18/15 12:48
1,1-Dichloroethane ug/kg ND 4.8 03/18/15 12:48
1,1-Dichloroethene ug/kg ND 4.8 03/18/15 12:48
1,1-Dichloropropene ug/kg ND 4.8 03/18/15 12:48
1,2,3-Trichlorobenzene ug/kg ND 4.8 03/18/15 12:48
1,2,3-Trichloropropane ug/kg ND 4.8 03/18/15 12:48
1,2,4-Trichlorobenzene ug/kg ND 4.8 03/18/15 12:48
1,2,4-Trimethylbenzene ug/kg ND 4.8 03/18/15 12:48
1,2-Dibromo-3-chloropropane ug/kg ND 4.8 03/18/15 12:48
1,2-Dibromoethane (EDB)ug/kg ND 4.8 03/18/15 12:48
1,2-Dichlorobenzene ug/kg ND 4.8 03/18/15 12:48
1,2-Dichloroethane ug/kg ND 4.8 03/18/15 12:48
1,2-Dichloropropane ug/kg ND 4.8 03/18/15 12:48
1,3,5-Trimethylbenzene ug/kg ND 4.8 03/18/15 12:48
1,3-Dichlorobenzene ug/kg ND 4.8 03/18/15 12:48
1,3-Dichloropropane ug/kg ND 4.8 03/18/15 12:48
1,4-Dichlorobenzene ug/kg ND 4.8 03/18/15 12:48
2,2-Dichloropropane ug/kg ND 4.8 03/18/15 12:48
2-Butanone (MEK)ug/kg ND 95.1 03/18/15 12:48
2-Chlorotoluene ug/kg ND 4.8 03/18/15 12:48
2-Hexanone ug/kg ND 47.5 03/18/15 12:48
4-Chlorotoluene ug/kg ND 4.8 03/18/15 12:48
4-Methyl-2-pentanone (MIBK)ug/kg ND 47.5 03/18/15 12:48
Acetone ug/kg ND 95.1 03/18/15 12:48
Benzene ug/kg ND 4.8 03/18/15 12:48
Bromobenzene ug/kg ND 4.8 03/18/15 12:48
Bromochloromethane ug/kg ND 4.8 03/18/15 12:48
Bromodichloromethane ug/kg ND 4.8 03/18/15 12:48
Bromoform ug/kg ND 4.8 03/18/15 12:48
Bromomethane ug/kg ND 9.5 03/18/15 12:48
Carbon tetrachloride ug/kg ND 4.8 03/18/15 12:48
Chlorobenzene ug/kg ND 4.8 03/18/15 12:48
Chloroethane ug/kg ND 9.5 03/18/15 12:48
Chloroform ug/kg ND 4.8 03/18/15 12:48
Chloromethane ug/kg ND 9.5 03/18/15 12:48
cis-1,2-Dichloroethene ug/kg ND 4.8 03/18/15 12:48
cis-1,3-Dichloropropene ug/kg ND 4.8 03/18/15 12:48
Dibromochloromethane ug/kg ND 4.8 03/18/15 12:48
REPORT OF LABORATORY ANALYSIS
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Page 9 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241627
Charlotte Chemical
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1413556
Associated Lab Samples:92241627001
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 4.8 03/18/15 12:48
Dichlorodifluoromethane ug/kg ND 9.5 03/18/15 12:48
Diisopropyl ether ug/kg ND 4.8 03/18/15 12:48
Ethylbenzene ug/kg ND 4.8 03/18/15 12:48
Hexachloro-1,3-butadiene ug/kg ND 4.8 03/18/15 12:48
Isopropylbenzene (Cumene)ug/kg ND 4.8 03/18/15 12:48
m&p-Xylene ug/kg ND 9.5 03/18/15 12:48
Methyl-tert-butyl ether ug/kg ND 4.8 03/18/15 12:48
Methylene Chloride ug/kg ND 19.0 03/18/15 12:48
n-Butylbenzene ug/kg ND 4.8 03/18/15 12:48
n-Propylbenzene ug/kg ND 4.8 03/18/15 12:48
Naphthalene ug/kg ND 4.8 03/18/15 12:48
o-Xylene ug/kg ND 4.8 03/18/15 12:48
p-Isopropyltoluene ug/kg ND 4.8 03/18/15 12:48
sec-Butylbenzene ug/kg ND 4.8 03/18/15 12:48
Styrene ug/kg ND 4.8 03/18/15 12:48
tert-Butylbenzene ug/kg ND 4.8 03/18/15 12:48
Tetrachloroethene ug/kg ND 4.8 03/18/15 12:48
Toluene ug/kg ND 4.8 03/18/15 12:48
trans-1,2-Dichloroethene ug/kg ND 4.8 03/18/15 12:48
trans-1,3-Dichloropropene ug/kg ND 4.8 03/18/15 12:48
Trichloroethene ug/kg ND 4.8 03/18/15 12:48
Trichlorofluoromethane ug/kg ND 4.8 03/18/15 12:48
Vinyl acetate ug/kg ND 47.5 03/18/15 12:48
Vinyl chloride ug/kg ND 9.5 03/18/15 12:48
Xylene (Total)ug/kg ND 9.5 03/18/15 12:48
1,2-Dichloroethane-d4 (S)%99 70-132 03/18/15 12:48
4-Bromofluorobenzene (S)%98 70-130 03/18/15 12:48
Toluene-d8 (S)%103 70-130 03/18/15 12:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1413557LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 49.347.2 104 74-137
1,1,1-Trichloroethane ug/kg 48.647.2 103 67-140
1,1,2,2-Tetrachloroethane ug/kg 46.847.2 99 72-141
1,1,2-Trichloroethane ug/kg 49.747.2 105 78-138
1,1-Dichloroethane ug/kg 50.347.2 107 69-134
1,1-Dichloroethene ug/kg 49.347.2 104 67-138
1,1-Dichloropropene ug/kg 50.447.2 107 69-139
1,2,3-Trichlorobenzene ug/kg 52.847.2 112 70-146
1,2,3-Trichloropropane ug/kg 44.747.2 95 69-144
1,2,4-Trichlorobenzene ug/kg 51.947.2 110 68-148
1,2,4-Trimethylbenzene ug/kg 51.047.2 108 74-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/20/2015 03:43 PM
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Huntersville, NC 28078
[phone]
Page 10 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241627
Charlotte Chemical
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1413557LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 45.447.2 96 65-140
1,2-Dibromoethane (EDB)ug/kg 50.147.2 106 77-135
1,2-Dichlorobenzene ug/kg 49.947.2 106 77-141
1,2-Dichloroethane ug/kg 50.047.2 106 65-137
1,2-Dichloropropane ug/kg 51.047.2 108 72-136
1,3,5-Trimethylbenzene ug/kg 50.947.2 108 76-133
1,3-Dichlorobenzene ug/kg 49.447.2 105 74-138
1,3-Dichloropropane ug/kg 49.247.2 104 71-139
1,4-Dichlorobenzene ug/kg 50.847.2 108 76-138
2,2-Dichloropropane ug/kg 49.047.2 104 68-137
2-Butanone (MEK)ug/kg 89.8J94.3 95 58-147
2-Chlorotoluene ug/kg 50.547.2 107 73-139
2-Hexanone ug/kg 88.494.3 94 62-145
4-Chlorotoluene ug/kg 49.647.2 105 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 10194.3 107 64-149
Acetone ug/kg 86.1J94.3 91 53-153
Benzene ug/kg 53.347.2 113 73-135
Bromobenzene ug/kg 49.847.2 106 75-133
Bromochloromethane ug/kg 46.647.2 99 73-134
Bromodichloromethane ug/kg 48.647.2 103 71-135
Bromoform ug/kg 45.147.2 96 66-141
Bromomethane ug/kg 49.247.2 104 53-160
Carbon tetrachloride ug/kg 51.447.2 109 60-145
Chlorobenzene ug/kg 49.147.2 104 78-130
Chloroethane ug/kg 49.547.2 105 64-149
Chloroform ug/kg 45.947.2 97 70-134
Chloromethane ug/kg 44.947.2 95 52-150
cis-1,2-Dichloroethene ug/kg 51.747.2 110 70-133
cis-1,3-Dichloropropene ug/kg 50.647.2 107 68-134
Dibromochloromethane ug/kg 44.547.2 94 71-138
Dibromomethane ug/kg 52.447.2 111 74-130
Dichlorodifluoromethane ug/kg 41.147.2 87 40-160
Diisopropyl ether ug/kg 49.447.2 105 69-141
Ethylbenzene ug/kg 49.447.2 105 75-133
Hexachloro-1,3-butadiene ug/kg 50.947.2 108 68-143
Isopropylbenzene (Cumene)ug/kg 49.447.2 105 76-143
m&p-Xylene ug/kg 99.594.3 106 75-136
Methyl-tert-butyl ether ug/kg 45.147.2 96 68-144
Methylene Chloride ug/kg 48.247.2 102 45-154
n-Butylbenzene ug/kg 50.447.2 107 72-137
n-Propylbenzene ug/kg 49.147.2 104 76-136
Naphthalene ug/kg 50.947.2 108 68-151
o-Xylene ug/kg 49.747.2 105 76-141
p-Isopropyltoluene ug/kg 49.347.2 104 76-140
sec-Butylbenzene ug/kg 48.747.2 103 79-139
Styrene ug/kg 50.147.2 106 79-137
tert-Butylbenzene ug/kg 48.147.2 102 74-143
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/20/2015 03:43 PM
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Page 11 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241627
Charlotte Chemical
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1413557LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 48.347.2 102 71-138
Toluene ug/kg 51.847.2 110 74-131
trans-1,2-Dichloroethene ug/kg 50.347.2 107 67-135
trans-1,3-Dichloropropene ug/kg 54.247.2 115 65-146
Trichloroethene ug/kg 51.347.2 109 67-135
Trichlorofluoromethane ug/kg 47.047.2 100 59-144
Vinyl acetate ug/kg 73.7 F394.3 78 40-160
Vinyl chloride ug/kg 43.647.2 93 56-141
Xylene (Total)ug/kg 149142 105 76-137
1,2-Dichloroethane-d4 (S)%95 70-132
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1414461MATRIX SPIKE SAMPLE:
MSSpike
Result
92241589003
1,1,1,2-Tetrachloroethane ug/kg 27.722.8 122 70-130ND
1,1,1-Trichloroethane ug/kg 25.522.8 112 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 35.6 M122.8 156 70-130ND
1,1,2-Trichloroethane ug/kg 34.1 M122.8 149 70-130ND
1,1-Dichloroethane ug/kg 26.422.8 116 70-130ND
1,1-Dichloroethene ug/kg 24.722.8 108 49-180ND
1,1-Dichloropropene ug/kg 26.722.8 117 70-130ND
1,2,3-Trichlorobenzene ug/kg 25.722.8 113 70-130ND
1,2,3-Trichloropropane ug/kg 35.5 M122.8 156 70-130ND
1,2,4-Trichlorobenzene ug/kg 24.122.8 106 70-130ND
1,2,4-Trimethylbenzene ug/kg 25.422.8 100 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 34.8 M122.8 153 70-130ND
1,2-Dibromoethane (EDB)ug/kg 33.9 M122.8 149 70-130ND
1,2-Dichlorobenzene ug/kg 27.122.8 119 70-130ND
1,2-Dichloroethane ug/kg 31.5 M122.8 138 70-130ND
1,2-Dichloropropane ug/kg 28.522.8 125 70-130ND
1,3,5-Trimethylbenzene ug/kg 24.022.8 102 70-130ND
1,3-Dichlorobenzene ug/kg 24.922.8 109 70-130ND
1,3-Dichloropropane ug/kg 31.5 M122.8 138 70-130ND
1,4-Dichlorobenzene ug/kg 26.222.8 115 70-130ND
2,2-Dichloropropane ug/kg 25.222.8 110 70-130ND
2-Butanone (MEK)ug/kg 68.8J M145.6 151 70-130ND
2-Chlorotoluene ug/kg 24.622.8 108 70-130ND
2-Hexanone ug/kg 78.4 M145.6 172 70-130ND
4-Chlorotoluene ug/kg 25.222.8 110 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 85.4 M145.6 187 70-130ND
Acetone ug/kg 72.6J M145.6 159 70-130ND
Benzene ug/kg 28.422.8 125 50-166ND
Bromobenzene ug/kg 28.022.8 123 70-130ND
REPORT OF LABORATORY ANALYSIS
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Page 12 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241627
Charlotte Chemical
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1414461MATRIX SPIKE SAMPLE:
MSSpike
Result
92241589003
Bromochloromethane ug/kg 30.5 M122.8 134 70-130ND
Bromodichloromethane ug/kg 27.922.8 123 70-130ND
Bromoform ug/kg 31.3 M122.8 137 70-130ND
Bromomethane ug/kg 25.522.8 112 70-130ND
Carbon tetrachloride ug/kg 26.222.8 115 70-130ND
Chlorobenzene ug/kg 28.022.8 123 43-169ND
Chloroethane ug/kg 24.122.8 106 70-130ND
Chloroform ug/kg 25.422.8 112 70-130ND
Chloromethane ug/kg 24.322.8 106 70-130ND
cis-1,2-Dichloroethene ug/kg 27.922.8 122 70-130ND
cis-1,3-Dichloropropene ug/kg 30.1 M122.8 132 70-130ND
Dibromochloromethane ug/kg 28.022.8 123 70-130ND
Dibromomethane ug/kg 31.2 M122.8 137 70-130ND
Dichlorodifluoromethane ug/kg 18.122.8 79 70-130ND
Diisopropyl ether ug/kg 29.9 M122.8 131 70-130ND
Ethylbenzene ug/kg 27.322.8 118 70-130ND
Hexachloro-1,3-butadiene ug/kg 15.7 M122.8 69 70-130ND
Isopropylbenzene (Cumene)ug/kg 25.422.8 111 70-130ND
m&p-Xylene ug/kg 54.345.6 112 70-130ND
Methyl-tert-butyl ether ug/kg 30.9 M122.8 136 70-130ND
Methylene Chloride ug/kg 24.422.8 107 70-130ND
n-Butylbenzene ug/kg 21.922.8 95 70-130ND
n-Propylbenzene ug/kg 23.722.8 102 70-130ND
Naphthalene ug/kg 31.8 M122.8 136 70-130ND
o-Xylene ug/kg 26.922.8 112 70-130ND
p-Isopropyltoluene ug/kg 22.122.8 97 70-130ND
sec-Butylbenzene ug/kg 22.222.8 97 70-130ND
Styrene ug/kg 28.722.8 126 70-130ND
tert-Butylbenzene ug/kg 22.722.8 99 70-130ND
Tetrachloroethene ug/kg 23.822.8 104 70-130ND
Toluene ug/kg 28.522.8 122 52-163ND
trans-1,2-Dichloroethene ug/kg 25.622.8 112 70-130ND
trans-1,3-Dichloropropene ug/kg 32.7 M122.8 143 70-130ND
Trichloroethene ug/kg 26.122.8 114 49-167ND
Trichlorofluoromethane ug/kg 22.522.8 98 70-130ND
Vinyl acetate ug/kg 57.145.6 125 70-130ND
Vinyl chloride ug/kg 20.422.8 89 70-130ND
1,2-Dichloroethane-d4 (S)%109 70-132
4-Bromofluorobenzene (S)%108 70-130
Toluene-d8 (S)%104 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92241317003
1414460SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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Page 13 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241627
Charlotte Chemical
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92241317003
1414460SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg 16.3J279
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/20/2015 03:43 PM
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Page 14 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241627
Charlotte Chemical
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92241317003
1414460SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%110 35113
4-Bromofluorobenzene (S)%106 4696
Toluene-d8 (S)%104 36105
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/20/2015 03:43 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241627
Charlotte Chemical
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/33655
EPA 3546
EPA 8270
8270 Solid MSSV Microwave PAH
Associated Lab Samples:92241627001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1413817
Associated Lab Samples:92241627001
Matrix:Solid
Analyzed
1-Methylnaphthalene ug/kg ND 330 03/19/15 10:59
2-Methylnaphthalene ug/kg ND 330 03/19/15 10:59
Acenaphthene ug/kg ND 330 03/19/15 10:59
Acenaphthylene ug/kg ND 330 03/19/15 10:59
Anthracene ug/kg ND 330 03/19/15 10:59
Benzo(a)anthracene ug/kg ND 330 03/19/15 10:59
Benzo(a)pyrene ug/kg ND 330 03/19/15 10:59
Benzo(b)fluoranthene ug/kg ND 330 03/19/15 10:59
Benzo(g,h,i)perylene ug/kg ND 330 03/19/15 10:59
Benzo(k)fluoranthene ug/kg ND 330 03/19/15 10:59
Chrysene ug/kg ND 330 03/19/15 10:59
Dibenz(a,h)anthracene ug/kg ND 330 03/19/15 10:59
Fluoranthene ug/kg ND 330 03/19/15 10:59
Fluorene ug/kg ND 330 03/19/15 10:59
Indeno(1,2,3-cd)pyrene ug/kg ND 330 03/19/15 10:59
Naphthalene ug/kg ND 330 03/19/15 10:59
Phenanthrene ug/kg ND 330 03/19/15 10:59
Pyrene ug/kg ND 330 03/19/15 10:59
2-Fluorobiphenyl (S)%76 30-110 03/19/15 10:59
Nitrobenzene-d5 (S)%70 23-110 03/19/15 10:59
Terphenyl-d14 (S)%88 28-110 03/19/15 10:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1413818LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/kg 13801670 83 40-120
2-Methylnaphthalene ug/kg 12801670 77 26-120
Acenaphthene ug/kg 13101670 78 46-120
Acenaphthylene ug/kg 12801670 77 46-120
Anthracene ug/kg 14201670 85 63-120
Benzo(a)anthracene ug/kg 15501670 93 61-120
Benzo(a)pyrene ug/kg 15501670 93 59-120
Benzo(b)fluoranthene ug/kg 16201670 97 55-120
Benzo(g,h,i)perylene ug/kg 15301670 92 57-120
Benzo(k)fluoranthene ug/kg 15101670 90 56-120
Chrysene ug/kg 15901670 96 64-120
Dibenz(a,h)anthracene ug/kg 15801670 95 56-120
Fluoranthene ug/kg 15401670 92 61-120
Fluorene ug/kg 14201670 85 51-120
Indeno(1,2,3-cd)pyrene ug/kg 16101670 97 58-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/20/2015 03:43 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241627
Charlotte Chemical
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1413818LABORATORY CONTROL SAMPLE:
LCSSpike
Naphthalene ug/kg 13001670 78 38-120
Phenanthrene ug/kg 14101670 84 62-120
Pyrene ug/kg 14101670 84 63-120
2-Fluorobiphenyl (S)%74 30-110
Nitrobenzene-d5 (S)%68 23-110
Terphenyl-d14 (S)%91 28-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/20/2015 03:43 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241627
Charlotte Chemical
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/7630
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92241627001
Parameter Units
Dup
Result QualifiersRPDResult
92241616001
1413432SAMPLE DUPLICATE:
Percent Moisture %20.7 120.5
Parameter Units
Dup
Result QualifiersRPDResult
92241627001
1413433SAMPLE DUPLICATE:
Percent Moisture %23.0 925.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/20/2015 03:43 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 22
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92241627
Charlotte Chemical
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The internal standard response is below criteria. No hits associated with this internal standard. Results unaffected by
high bias.1g
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/20/2015 03:43 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 22
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92241627
Charlotte Chemical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92241627001 MPRP/18098 ICP/16268Tree Soil EPA 3050 EPA 6010
92241627001 MERP/7677 MERC/7361Tree Soil EPA 7471 EPA 7471
92241627001 OEXT/33655 MSSV/10431Tree Soil EPA 3546 EPA 8270
92241627001 MSV/30784Tree Soil EPA 8260
92241627001 PMST/7630Tree Soil ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/20/2015 03:43 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 22
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