19040_Atando Ave_LSI 20151218

LIMITED SITE
INVESTIGATION REPORT
Atando Avenue Brownfields Site
527 Atando Avenue
Charlotte, Mecklenburg County, North Carolina
December 18, 2015
Terracon Project No. 71157718
Prepared for:
Gould Family Properties II, LLC
Prepared by:
Terracon Consultants, Inc.
Charlotte, North Carolina
TABLE OF CONTENTS
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1.0 SITE DESCRIPTION ....................................................................................................... 1
1.1 Occurrence of Chlorinated Volatile Organic Compounds (CVOCs) at the Site ..... 1
1.2 Underground Storage Tank (UST) History ........................................................... 3
2.0 SCOPE OF SERVICES ................................................................................................... 4
2.1 Standard of Care.................................................................................................. 4
2.2 Additional Scope Limitations ................................................................................ 5
2.3 Reliance ............................................................................................................... 5
3.0 FIELD INVESTIGATION METHODS ............................................................................... 5
3.1 Monitoring Well Installation .................................................................................. 5
3.2 Groundwater Sampling ........................................................................................ 6
3.3 Soil Sampling ....................................................................................................... 7
3.4 Soil Vapor Sample Point Installation .................................................................... 8
3.5 Soil Vapor Sampling ............................................................................................ 8
3.6 Indoor and Outdoor Air Sampling ......................................................................... 9
3.7 GPR Survey ....................................................................................................... 10
3.8 Plat Survey ........................................................................................................ 10
4.0 INVESTIGATIVE DERIVED WASTE ............................................................................. 10
5.0 RESULTS ..................................................................................................................... 11
5.1 Site Hydrogeology .............................................................................................. 11
5.2 Groundwater Sample Results ............................................................................ 11
Non-Chlorinated VOCs ...................................................................................... 11
CVOCs .............................................................................................................. 12
5.3 Soil Sample Results ........................................................................................... 13
VOCs ................................................................................................................. 13
SVOCs ............................................................................................................... 14
5.4 Soil Vapor Sample Results ................................................................................ 14
5.5 Indoor and Outdoor Air Sample Results ............................................................. 15
6.0 SUMMARY .................................................................................................................... 16
7.0 CONCLUSIONS AND RECOMMENDATIONS ............................................................. 17
Tables
Table 1 – Sampling and Analysis Plan
Table 2 – Well Construction and Groundwater Elevations (October 2015)
Table 3 – Groundwater Analytical Results (August/October 2015)
Table 4 – Soil Analytical Results (August/November 2015)
Table 5 – Air and Soil Vapor Analytical Results (November 2015)
Figures
Figure 1 – Site Location Map
Figure 2 – Site Layout Map
Figure 3 – Groundwater Elevation Map (October 2105)
Figure 4 – Groundwater Results and CVOC Isoconcentration Map
Figure 5 – Soil Boring Location Map
Figure 6 – Soil Boring Analytical Results Map
Figure 7 – Sub-Slab Soil Vapor and Air Sample Location Map
Figure 8 – Sub-Slab Soil Vapor and Air Sample Results Map
TABLE OF CONTENTS (CONTINUED)
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Appendices
APPENDIX A – WELL CONSTRUCTION RECORD
APPENDIX B – FIELD FORMS AND SAMPLE SHEETS
Groundwater Sample Collection Records
Sub-Slab Soil Vapor Sample Record
Indoor and Outdoor Air Sample Record
Indoor Air Building Survey Form
Indoor Air Sampling Instructions for Occupants
APPENDIX C – GPR INVESTIGATION REPORT
APPENDIX D – SURVEY PLAT
APPENDIX E – IDW WASTE MANIFEST
APPENDIX F – ANALYTICAL REPORTS AND CHAINS OF CUSTODY
Groundwater Sample Analytical Reports – Pace Analytical
Soil Sample Analytical Reports – Pace Analytical
Gas Sample Analytical Report – Eurofins AirToxics
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LIMITED SITE INVESTIGATION
ATANDO AVENUE BROWNFIELDS SITE
527 ATANDO AVENUE
CHARLOTTE, NORTH CAROLINA
Terracon Project No. 71157718
December 18, 2015
1.0 SITE DESCRIPTION
The site is located at 527 Atando Avenue in Charlotte, North Carolina and consists of an
approximate 4-acre developed parcel in a predominantly industrialized area (Mecklenburg County
Tax Parcel ID 08505412). The single-story commercial building at the site includes a 7,546
square foot (sq. ft.) office area and two warehouse/manufacturing areas totaling approximately
97,211 sq. ft. The site is bound to the southwest by railroad tracks, to the northwest and southeast
by adjacent industrial facilities, and to the northeast by Atando Avenue. Current and historical
occupants of the on-site building have been suppliers of steel bar stock. As a result of documented
contaminants at the site and planned improvements, the property has been accepted into the
North Carolina Brownfields Program. A topographic map showing the site location is included as
Figure 1 and a site layout map with general site features is included as Figure 2.
Eleven active groundwater monitoring wells (ten shallow aquifer wells and one deep well) are
currently located at the site to assess the extent of impact from releases associated with on-site
underground petroleum storage tanks and chlorinated compounds from an off-site up-gradient
source. The groundwater flow direction at the site is towards the south-southeast. The locations
of on-site monitoring wells and other site features are shown on Figure 2. Water supply wells
have not been reported within 1,500 feet of the site. The nearest surface water feature is an
intermittent stream/drainage ditch located approximately 500 feet to the southwest of the site.
Based on local topography, water from the drainage feature discharges into Little Sugar Creek.
1.1 Occurrence of Chlorinated Volatile Organic Compounds (CVOCs) at the Site
The vapor intrusion concerns addressed in this report are in direct response to the presence of
chlorinated compounds that have been detected in the groundwater at the site. The source of
these CVOCs is separate from and not related to the on-site USTs. The releases associated with
the USTs are being assessed by others.
Historically, groundwater samples obtained from on-site monitoring well MW-5 have shown the
highest concentrations of CVOCs in any other on-site groundwater monitoring well. The detected
concentrations for most of the CVOC constituents exceeded the North Carolina Administrative
Code (NCAC) 2L Groundwater Standards. Well MW-5 is located in the northwestern portion of
the site, up-gradient of the on-site buildings and most operations conducted on the property.
Based on the CVOC levels detected in well MW-5 and health and safety concerns for personnel
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December 18, 2015 ■ Terracon Project No. 71157718
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on the site and nearby properties, the North Carolina Department of Environmental Quality
(NCDEQ), Division of Waste Management (DWM), Inactive Hazardous Sites Branch (IHSB)
opened Incident No. NONCD0001992 for the site in 2014. Based on preliminary assessment
activities conducted at the site, the IHSB recommended additional assessment to identify the on-
site source of the CVOCs.
In response to the recommendations of the IHSB, Terracon installed monitoring wells MW-9 and
MW-10 in August 2015 at locations up-gradient of well MW-5 along the northwestern property
boundary in an effort to disprove IHSB’s claim of an on-site source. Terracon also collected
groundwater samples from remaining monitoring wells MW-2 through MW-8 and DW-1 in October
2015 to evaluate current constituent levels in the groundwater at the site. As a result of our most
recent sampling event, detected CVOCs were highest in the sample from well MW-9 which is
located near the property boundary directly up-gradient of well MW-5. Monitoring well MW-5
generally exhibited CVOC concentrations lower than well MW-9 but higher than the remaining on-
site monitoring wells. CVOCs were also detected in wells MW-8 and MW-10 located in the
northwestern portion of the site at concentrations several orders of magnitude lower than wells
MW-5 and MW-9. Certain CVOC constituents were also detected in deep monitoring well DW-1
which is located down-gradient of wells MW-5 and MW-9 at concentrations above the 2L
Groundwater Standards while the sample from adjacent shallow well MW-4 did not contain CVOC
constituents above laboratory reporting limits. The August/October 2015 well installation and
sampling activities are discussed in detail in the field methods and results sections of this report.
Based on the groundwater sampling results from August and October 2015, the following activities
were conducted at the site.
§Preliminary groundwater to indoor air off-gassing calculations (submitted to the IHSB and
the NC Brownfields program on October 27, 2015) indicated a vapor intrusion concern
exists for personnel working inside the warehouse and office areas at the on-site facility.
§After reviewing the preliminary off-gassing calculations, Mr. Miguel Alvalle of the IHSB
requested additional unsaturated zone soil samples be collected near wells MW-5 and
MW-9 to confirm the absence of impacted soils that could be an on-site source of CVOCs.
§Evaluate the presence of a third UST located in the northwestern portion of the site based
on NCDEQ regulatory file information that could be a potential source of the CVOC
constituents in the groundwater. Two known petroleum USTs were removed from this
portion of the site in the past. The results of a ground penetrating radar (GPR) survey are
provided in Section 3.7.
§Ms. Carolyn Minnich of the NC Brownfields Program requested sub-slab soil vapor
samples be collected inside the office area and the warehouse to evaluate VOC
concentrations beneath the building slab and determine if the constituent concentrations
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December 18, 2015 ■ Terracon Project No. 71157718
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are hazardous to the occupants of the site. The soil and soil vapor/air sampling activities
and results are discussed in this report.
A previously completed Phase I ESA conducted for the site in 2013 identified the adjacent Dy-
Dee Service, as an industrial laundry business formerly located on the property to the north and
up-gradient of the site. An approximate 1,500-gallon aboveground storage tank (AST) in poor
overall condition was reported as a Recognized Environmental Condition (REC) located at the
rear exterior of the Dy-Dee Service building. Terracon confirmed the presence of the AST in
August, October, and November 2015 and also observed several rusted 55-gallon drums stored
at the rear of the Dy-Dee Service building near the AST. Based on the groundwater flow direction
towards the south, a release from the AST, drums or former operations at the Dy-Dee Service
facility could potentially impact the groundwater quality at 527 Atando Avenue. A secondary
potential source for groundwater contamination is a former automotive repair shop that was
reportedly located in a building located at the rear of the Dy-Dee Service building (on the same
parcel). Terracon could not obtain information regarding the car repair business.
1.2 Underground Storage Tank (UST) History
Below is a summary of assessment and remediation activities related to the on-site and out of
service USTs. The UST release incidents are not related to the CVOC contamination but are
summarized below.
Two 6,000-gallon diesel USTs located near the northwestern property corner, just north of the on-
site manufacturing area were reportedly excavated in April 1990. Impacted soils located near the
USTs were reportedly removed at the time of the excavation activities. Confirmation testing
indicated petroleum impacted soils remained in the former tank basin; thus, additional soils were
removed in May 1990. A No Further Action Letter was issued by the NCDEQ in November 1990.
A GPR investigation performed by Terracon in 2015 confirmed the absence of the USTs in the
area of the former tank basin. The GPR survey and associated results are discussed in this report.
Two 6,000-gallon heating oil USTs (an earlier Phase I ESA identified one of the USTs as being
12,000 gallons) were located beneath the concrete slab in the warehouse area, south of the office
space in 2003. Five shallow monitoring wells (MW-1 through MW-5) and one deep monitoring
well (DW-1) were installed to assess groundwater quality. The UST located near well MW-1 was
removed in 2004 and the second UST, located near well MW-2, was abandoned in place. An
aggressive fluid vapor recovery (AFVR) event and impacted soil removal activities were
performed at the time of removal of the heating oil tank in an attempt to remove the contaminant
source. Free product has been observed in monitoring well MW-1 since the excavation and AFVR
event. The release of heating oil from the two USTs is maintained by a separate LUST incident.
The approximate locations of the four former on-site USTs are depicted on Figure 2.
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December 18, 2015 ■ Terracon Project No. 71157718
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During a 2013 Limited Phase II Environmental Assessment conducted by HRP Associates, Inc.,
three additional monitoring wells (MW-6, MW-7 and MW-8) were installed at the site to further
define the groundwater contaminant plume. Wells MW-7 and MW-8 were installed near the
northern and western facility corners, respectively, to assess potential up-gradient and off-site
sources that could impact the groundwater quality at the site.
2.0 SCOPE OF SERVICES
Terracon’s Limited Site Investigation was performed in general agreement with Terracon’s
Proposal P71157E009 dated January 20, 2015. The scope of services included:
§Installation of two new groundwater monitoring wells (MW-9 and MW-10);
§Groundwater sample collection from the 11 on-site monitoring wells;
§Collection of unsaturated zone soil samples from the borings for wells MW-9 and MW-10,
as well as three additional soil borings near well MW-5;
§Collection of shallow soil samples near existing groundwater monitoring wells MW-5 and
MW-9;
§Collection of four sub-slab soil vapor samples, 1 outdoor ambient air sample and 1 indoor
ambient air sample;
§A ground penetrating radar (GPR) survey to assess the presence of USTs in specific areas
of the site; and,
§A land survey by a NC licensed surveyor to obtain a plat survey (including monitoring
wells) that satisfies the requirements of the NC Brownfields Program.
The survey was conducted to obtain top of casing elevations and coordinates for the monitoring
wells, a requirement to accurately determine groundwater elevations and flow direction on the
site. The survey plat was also designed to meet the requirements as specified by the NC
Brownfields Program. Soil sampling activities and the GPR survey were performed in response
to a request by the IHSB as discussed in Section 1.1 of this report. The vapor intrusion
investigation was conducted to address a request by the NC Brownfields Program as outlined in
Section 1.1. Our scope of services was not intended to identify every chemical possibly
associated with the site. Similarly, the proposed scope was not intended to determine the extent
or magnitude of any existing contamination.
2.1 Standard of Care
Terracon’s services were performed in a manner consistent with generally accepted practices of
the profession undertaken in similar studies in the same geographical area during the same time.
Terracon makes no warranties, either expressed or implied, regarding the findings, conclusions,
or recommendations. Please note that Terracon does not warrant the work of laboratories,
regulatory agencies, or other third parties supplying information used in the preparation of the
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report. The services were performed in accordance with the scope of work authorized by our
client, as reflected in our proposal and were not conducted in accordance with ASTM E1903-11.
2.2 Additional Scope Limitations
Findings, conclusions, and recommendations resulting from these services are based upon
information derived from the on-site activities and other services performed under this scope of
work; such information is subject to change over time. Certain indicators of the presence of
hazardous substances, petroleum products, or other constituents may have been latent,
inaccessible, unobservable, non-detectable, or not present during these services. We cannot
represent that the site contains no hazardous substances, toxic materials, petroleum products, or
other latent conditions beyond those identified during this investigation. Subsurface conditions
may vary from those encountered at specific borings or wells or during other surveys, tests,
assessments, investigations, or exploratory services. The data, interpretations, findings, and our
recommendations are based solely upon data obtained at the time and within the scope of these
services.
2.3 Reliance
This report has been prepared for the exclusive use of Gould Family Properties II, LLC. Any
authorization for use or reliance by another party (except a governmental entity having jurisdiction
over the site) is prohibited without the expressed written authorization of Gould Family Properties
II, LLC and Terracon. Any unauthorized distribution or reuse is at Gould Family Properties II,
LLC’s sole risk. Reliance by authorized parties will be subject to the terms, conditions, and
limitations stated in the proposal, report, and Terracon’s Agreement for Services. The limitation
of liability defined in the terms and conditions is the aggregate limit of Terracon’s liability to Gould
Family Properties II, LLC and all relying parties unless otherwise agreed in writing.
3.0 FIELD INVESTIGATION METHODS
Terracon conducted the field work under a health and safety plan developed for this project. Work
was performed using United States Environmental Protection Agency (USEPA) Level D work
attire consisting of hard hats, safety glasses, protective gloves, and protective boots.
3.1 Monitoring Well Installation
Terracon mobilized to the site on August 26, 2015 to install groundwater monitoring wells MW-9
and MW-10 along the northern property boundary (Figure 2). Prior to intrusive activities, Terracon
submitted a locate request to the public utility locator [NC 811] to arrange for location of
underground public utilities from the street to the utility meter. As an added measure of safety,
Terracon subcontracted Priority Locating of Huntersville, North Carolina, a private utility locator,
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December 18, 2015 ■ Terracon Project No. 71157718
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to locate and mark public utilities beyond the meter as well as additional site utilities identified
near the proposed well locations.
The boreholes were drilled by Environmental Drilling & Probing Services using 8.25-inch inner
diameter hollow stem augers. Boreholes for both wells were advanced to 25 feet below ground
surface (bgs) and constructed with a 2-inch diameter PVC riser and a 15-foot, 10-slot PVC screen.
A sand filter pack was placed in the annulus, extending from the bottom of the well screen to one
foot above the top of the well screen. Hydrated bentonite was then used to create a 2-foot thick
seal above the filter pack and the remainder of the borehole was filled with cement grout. Wells
were completed with flush-mount manhole covers and 2 by 2 foot concrete well pads. A lockable
expansion plug was installed to provide a watertight seal. The driller’s well construction records
for wells MW-9 and MW-10 are included as Appendix A.
3.2 Groundwater Sampling
Terracon mobilized to the site to conduct groundwater sampling as requested by the NCDEQ.
Groundwater samples were collected from the following wells as shown in Table 1.
§Wells MW-2 through MW-8 and DW-1 on October 8, 2015
§Wells MW-9 and MW-10 on August 27, 2015
Prior to sample collection, Terracon gauged the groundwater elevations in the monitoring wells.
Sufficient time was allowed for the water level in each well to equilibrate to atmospheric pressure.
Since monitoring well MW-1 contained free product, no groundwater elevation was obtained and
no sampling was conducted at the well. Groundwater elevation measurements and monitoring
well construction information are provided in Table 2. The surveyed locations of the 11 on-site
wells are shown on Figure 2.
Prior to sampling, the wells were purged a minimum of three well volumes using a new disposable
bailer. Water quality parameters pH, specific conductance, oxidation-reduction potential,
dissolved oxygen and temperature were measured and recorded after purging each well volume.
The wells were allowed to recharge to a minimum of 90 percent of the original water level volume
before samples were collected. Purge water was temporarily contained in 5-gallon buckets and
then transferred to 55 gallon drums. The drums containing purge water were properly labeled and
transported to an off-site disposal facility on October 26, 2015. Groundwater sampling records
are included in Appendix B of this report.
The groundwater samples were placed in laboratory-supplied glassware, labeled and stored in
an ice-packed cooler. The samples, along with chain-of-custody documentation, were delivered
to Pace Analytical Services, Inc. in Huntersville, North Carolina for analysis of volatile organic
compounds (VOCs) by EPA Method 8260 SIM, including 1,4-dioxane. For quality assurance and
quality control purposes (QA/QC), one duplicate sample was collected from well DW-1 and one
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December 18, 2015 ■ Terracon Project No. 71157718
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equipment blank sample was collected from rinsing a new, clean disposable bailer that was later
used to purge well MW-2.
3.3 Soil Sampling
Prior to intrusive activities, Terracon submitted a locate request to the public utility locator [NC
811] to arrange for location of underground public utilities from the street to the utility meter. As
an added measure of safety, Terracon subcontracted Priority Locating of Huntersville, NC, a
private utility locator, in an attempt to locate and mark public utilities beyond the meter as well as
any additional site utilities identified near the proposed soil boring locations. The soil boring
locations are shown on Figure 5.
On August 26, 2015, three soil borings (SB-1, SB-2 and SB-3) were advanced near and up-
gradient of well MW-5. Borings were advanced to 10 feet bgs using direct-push technology and
screened for volatiles using a photo ionization detector (PID). One sample was collected and
submitted for laboratory analysis from the interval with the highest PID reading for each boring.
The borings were located in an area containing an asphalt ground cover while the underlying soils
consisted predominantly of red and tan clayey silts. Petroleum odors were detected by Terracon
while screening the soil cores with a PID. The boreholes were abandoned using hydrated
bentonite and an asphalt patch after the sampling activities were completed.
During the advancement of the borings for wells MW-9 and MW-10, also on August 26, 2015,
continuous soil cores were extracted from the boreholes for characterization of the soils. Soil
samples (MW-9 10’-15’ and MW-10 15’-18’) were collected from each boring at intervals with the
highest PID reading and submitted for laboratory analysis. Soils from both borings consisted
predominantly of brown and tan clayey silt. Upon completion of sampling, monitoring wells MW-
9 and MW-10 were installed in the borings.
On November 11, 2015 at the request of the IHSB, an additional shallow soil sample, SB-04(1-
2), was collected approximately seven feet east of well MW-9 in a grassed area along the northern
property boundary. The soil boring was advanced to a depth of about 2 feet bgs using a hand
auger that was decontaminated using a Liquinox® and water mixture prior to advancing the boring.
The sample was collected from 1-2 feet bgs and screened for volatiles using a PID. At boring
SB-04, the 0-0.5 ft. interval consisted of topsoil with high organic matter. The 0.5-2 ft. interval
consisted of brown silty clay with minor amounts of fine sand. PID screening results of the soil
sample showed readings of 0.0-0.2 parts per million (ppm).
Terracon attempted to collect a shallow soil sample near well MW-5 but could not advance the
hand auger through an asphalt and gravel surface layer.
Soil samples were collected in laboratory provided containers, labeled and placed on ice
immediately after sample collection. The soil samples were submitted for analysis of VOCs via
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EPA Method 8260. Terracon staff delivered the soil samples and a completed chain-of-custody
form to Pace Analytical Labs in Huntersville, NC, a North Carolina certified analytical lab.
3.4 Soil Vapor Sample Point Installation
Before any intrusive work inside the warehouse and office areas commenced, Terracon personnel
visited the site on November 3, 2015 to meet with Mr. Jerry Webb, the General Manager of
Sunbelt-Turret, the current building tenant. Mr. Webb approved our locations for each proposed
sub-slab soil vapor sample.
Terracon then submitted a locate request to the public utility locator [NC 811] and subcontracted
Priority Locating to locate and mark public utilities beyond the meter as well as any additional site
utilities identified near the proposed sub-slab soil vapor sample locations. The private utility
locating activities were performed on November 11, 2015. Two unidentified utility lines were
found near proposed boring location SV-01 so Terracon staff decided, upon Mr. Webb’s approval,
to move the boring to the north by approximately 3 feet.
Technical approaches and methods outlined in this soil vapor investigation report are in general
accordance with the Interstate Technical and Regulatory Council’s Vapor Intrusion: A Practical
Guideline (2007) and Vapor Intrusion Pathway: Investigative Approaches for Typical Scenarios
(2007), as well as the NCDEQ DWM’s Vapor Intrusion Guidance (2014).
On November 11, 2015, three temporary sub-slab soil vapor (SV) sampling points were installed
inside the office area and one SV point was installed in the manufacturing area near well MW-5
(Figure 7). Each temporary SV sampling point was installed by drilling a 5/8-inch diameter hole
through the floor slab to a depth of approximately 1 to 2 inches into the underlying soils. The
concrete slab in the office area (points SV-01 through SV-03) was approximately 5 inches thick
while the floor slab in the manufacturing area was roughly 8 inches thick (SV-04). The existence
of a vapor barrier underneath the building slab could not be verified by Terracon. The SV
sampling points were completed with a Vapor Pin™ assembly consisting of a brass barb fitting
with a silicone sleeve to seal the 5/8-inch diameter hole. A silicone cap was placed over the vapor
pin to keep it sealed and the sample points were allowed to equilibrate overnight prior to sampling.
Details regarding sample IDs and analytical methods for the SV samples are provided in Table
1.
3.5 Soil Vapor Sampling
Terracon mobilized to the site on November 12, 2015 to collect the four sub-slab soil vapor
samples. In order to test the integrity of the sampling point seal, both a shut-in test and a helium
tracer test were conducted at each sample point. A MGD-2000 helium detector was used to verify
the presence and concentration of tracer gas.
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The protocol for using a tracer gas is to enclose the sample manifold, tubing and ground interface
with a shroud and enrich the shroud atmosphere with helium. Prior to sample collection, at least
three volumes of the vapor point annulus and attached Teflon® lined tubing and sample train were
purged using a vacuum canister. Purge samples were then screened for helium to assess the
presence of leaks in the well seal and fittings and with a PID to assess for the presence of VOCs.
Sample collection was started if the tracer testing indicated the helium concentration in the vapor
point was less than 10 percent of the helium concentration in the shroud, indicating an
appropriately sealed vapor point annulus.
Samples were collected with 1.0-liter Summa® canisters equipped with 170 ml/min flow controllers
for analysis of VOCs per EPA Method TO-15. The reporting list was restricted to the CVOC
compounds detected in the groundwater at the site and their daughter products. In addition to the
tracer test performed in the field, one sample was analyzed for helium by Method ASTM-1946 to
quantify leakage. A helium analysis was performed on a sample that exhibited leakage during
field leak testing. The vacuum pressure of the sample canisters was monitored and recorded at
regular intervals throughout the sampling period. After completion of soil vapor sampling activities,
the vapor sample points were abandoned by removal of the vapor pin and silicone sleeve and
filling the borehole with neat cement grout to the slab surface.
Following completion of the field activities, the Summa canisters (5 samples), along with chain-
of-custody documentation, were shipped to Eurofins AirToxics in Folsom, California for laboratory
analysis of volatile organic compounds (VOCs) by United States Environmental Protection
Agency (EPA) Method TO-15 and ASTM-1946 (1 sample only).
3.6 Indoor and Outdoor Air Sampling
Prior to indoor and outdoor air sampling, Terracon completed a building survey form (Appendix
B) by interviewing Mr. Webb on November 3, 2015. Terracon also provided Mr. Webb a summary
sheet with information on indoor/outdoor air sampling for the on-site workers. A copy of the
summary sheet is included in Appendix B.
One indoor air (IA-01) and one outdoor air (OA-01) sample were collected concurrently with the
sub-slab soil vapor samples to assess the presence of VOCs in ambient air. The indoor air sample
canister was located approximately five feet from sub-slab soil vapor sample location SV-02. The
canister was located so that it did not interfere with routine business activities and the sample
intake was at a normal breathing height, approximately 5 feet above ground surface.
The outdoor air sample was collected upwind of the soil gas sample points and the sample intake
was located approximately 5 feet above ground surface. Both air samples were collected in
laboratory supplied 6-liter Summa canisters attached to a flow controller set for 8 hours and
analyzed for TO-15 Low Level. The laboratory reporting list was limited to compounds detected
in groundwater at the site.
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Following completion of the field activities, the Summa canisters (2 samples), along with chain-
of-custody documentation, were shipped to Eurofins AirToxics in Folsom, California for laboratory
analysis of volatile organic compounds (VOCs) by EPA Method TO-15-SIM.
3.7 GPR Survey
Terracon subcontracted Probe Utility Locating (PUL) to perform a ground penetrating radar (GPR)
survey of the area north of the manufacturing area. The GPR survey was performed on
September 10, 2015 to assess the presence of USTs that could have been a source of the
contaminants detected on the site. According to records from the NCDEQ, two documented tanks
and one potential UST were formerly located in the northern portion of the site. Since two USTs
had been removed from the northern site area, the regulatory records were unclear whether a
third tank remained at the site.
The GPR survey identified an area where the subsurface profile was indicative of an excavation
and backfilled by soils. The area coincided with the assumed locations of the two former USTs as
shown on Figure 2. No evidence of additional USTs was found during the GPR survey. A letter
from PUL stating the results is included as Appendix C.
3.8 Plat Survey
Terracon subcontracted Dewberry, Inc. of Charlotte, NC, to perform a land survey of the on-site
parcel. The survey was performed on November 12, 2015 while Terracon was conducting
sampling activities on the property. Dewberry used a combination of GPS devices, equipped with
the North Carolina Continuously Operating Reference Station (CORS) Network of Global
Navigation Satellite System (GNSS) base stations, and traditional laser-based total stations to
survey site features. In addition to the features required for a plat survey under the NC
Brownfields Program, Dewberry also surveyed the vertical top of casing elevation and the northing
and easting of each on-site monitoring well. The survey plat is included as Appendix D.
4.0 INVESTIGATIVE DERIVED WASTE
Investigative derived waste (IDW) from well installation activities and groundwater sampling
activities was contained in 55-gallon steel drums at the site. Drilling activities for monitoring wells
MW-6 through MW-10 and soil sampling activities created six drums of solid drill cuttings.
Groundwater sampling and well development activities created two drums of purge water. The
drums were properly labeled with “on hold pending analysis” labels. Concord Industrial Service of
Harrisburg, NC, transported the eight drums to an off-site facility for non-hazardous disposal. The
signed waste manifest is included as Appendix E.
Limited Site Investigation
Atando Avenue Brownfields Site ■ Charlotte, NC
December 18, 2015 ■ Terracon Project No. 71157718
Responsive ■Resourceful ■Reliable 11
5.0 RESULTS
The laboratory analytical reports and chain-of-custody record are attached in Appendix F. The
following sections describe the results of the testing.
5.1 Site Hydrogeology
Groundwater levels measured in the eleven on-site monitoring wells ranged from 11.26 ft bgs
(MW-8) to 19.29 ft. bgs (MW-2) on October 8, 2015. Groundwater elevations were calculated
using the field measurements and the updated top of casing elevation data from the land survey
conducted in November 2015. The elevation of the water table was not be determined in well
MW-1 due to the presence of free product. Groundwater depths and elevations are reported in
Table 2. A groundwater elevation contour map is provided as Figure 3.
Groundwater in the shallow aquifer zone appears to be flowing towards the south/southeast at
the site. The horizontal hydraulic gradient is approximately 0.007 ft/ft (MW-7 to MW-6) in the
eastern portion of the site and somewhat steeper at 0.013 ft/ft (MW-8 to MW-4) in the western
portion of the site. The gradient also appears to be elevated near wells MW-9 and MW-10 along
the northern property boundary. Only one well, DW-1, is screened in the deeper aquifer zone;
thus, horizontal gradients could not be determined for that zone. An upward vertical hydraulic
gradient of -0.015 ft/ft was calculated for well cluster MW-4/DW-1 assuming a screened interval
of 10 ft for both wells (well construction information is not available).
5.2 Groundwater Sample Results
For the purpose of the discussion of groundwater sample analytical results, CVOCs are discussed
separately from non-chlorinated VOCs detected in the samples. The reason for segregating the
analytical results is based on the lateral distribution of the VOC concentrations suggesting
different sources for CVOCs and non-chlorinated VOCs. Groundwater sample analytical results
are summarized in Table 3. The laboratory analytical reports included in Appendix F.
Non-Chlorinated VOCs
The following non-chlorinated VOCs were detected during the August and October 2015
groundwater sampling events.
§Benzene was detected in wells MW-2 (58.2 micrograms per liter [µg/L]) and MW-3 (1.6
µg/L) at levels that exceed the 2L Standard of 1 µg/L. Benzene was not detected in the
other samples.
§Naphthalene was detected in well MW-2 (87.9 µg/L) at a concentration above the 2L
Standard of 6 µg/L. Naphthalene was also detected below the 2L Standard in well MW-
3.
Limited Site Investigation
Atando Avenue Brownfields Site ■ Charlotte, NC
December 18, 2015 ■ Terracon Project No. 71157718
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§Ethylbenzene, p-isopropyltoluene, and xylenes were detected at concentrations below
their respective 2L Standards in well MW-2.
§Non-chlorinated VOCs were not detected above laboratory reporting limits in wells MW-4
through MW-10 and DW-1.
CVOCs
The following CVOCs were detected during the August and October 2015 groundwater sampling
events.
§Tetrachloroethylene (PCE) in wells MW-5 (2,790 µg/L), MW-8 (163 µg/L), MW-9 (4,460
µg/L), MW-10 (2.7 µg/L), and DW-1 (148 µg/L) at concentrations above its 2L Standard of
0.7 µg/L. PCE was not detected above laboratory reporting limits in the other samples.
§Trichloroethene (TCE) was detected in wells MW-5 (1,870 µg/L), MW-8 (25.5 µg/L), MW-
9 (2,880 µg/L), MW-10 (3.3 µg/L), and DW-1 (78.2 µg/L) at levels exceeding its 2L
Standard of 3 µg/L. TCE was not detected above laboratory reporting limits in the other
samples.
§cis-1,2-Dichloroethene (cis-1,2-DCE) was detected in wells MW-5 (1,000 µg/L) and MW-
9 (5,500 µg/L) exceeding its 2L Standard of 70 µg/L. cis-1,2-DCE was also detected in
wells MW-8, MW10, and DW-1 at concentrations below the 2L Standard.
§1,1-Dichloroethene (1,1-DCE) was detected in wells MW-9 and DW-1 at levels below the
2L Standard. 1,1-DCE was not detected above laboratory reporting limits in the other
samples.
§Vinyl chloride was detected in wells MW-5 (41.3 µg/L) and MW-9 (6.5 µg/L) above its 2L
Standard of 0.03 µg/L. Vinyl chloride was not detected above laboratory reporting limits
in the other samples.
§The following VOCs were detected at concentrations below their respective 2L Standards:
trans-1,2-dichloroethene (MW-5 and MW-9), 1,2-dichloroethane (MW-9), and chloroform
(MW-6).
§CVOCs were not detected above laboratory reporting limits in wells MW-2, MW-3, MW-4,
and MW-7.
§Total CVOC concentrations were highest in wells MW-9 (12,957 µg/L) and MW-5 (5,714
µg/L) located near the northern property boundary. In these wells, CVOCs were detected
at concentrations up to two orders of magnitude higher than the highest non-chlorinated
VOC concentrations at the site.
§Deep well DW-1 exhibited a significant total CVOC concentration (271 µg/L) when
compared to nearby shallow wells MW-2, MW-3, and MW-4 which did not contain CVOCs
above laboratory reporting limits.
In addition to the primary samples, QA/QC samples were also evaluated. DUP-01-10082015
(collected from well DW-1) had analytical results comparable to the primary DW-1 sample. The
equipment blank sample, EB-01-10082015, as well as the trip blank did not contain VOCs above
Limited Site Investigation
Atando Avenue Brownfields Site ■ Charlotte, NC
December 18, 2015 ■ Terracon Project No. 71157718
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laboratory reporting limits. Samples were received by the laboratory within the optimal
temperature range specified for EPA Method 8260.
5.3 Soil Sample Results
A total of six soil samples were collected near the northern site boundary in August and October
2015. Due to the number of compounds detected, laboratory results are summarized by sample
below. VOC soil sample results are discussed separately from semi-volatile organic compound
(SVOC) results. Results were compared to the NCDEQ IHSB Industrial Health Based Preliminary
Soil Remediation Goals (Industrial PSRGs), the NCDEQ IHSB Residential Health Based
Preliminary Soil Remediation Goal (Residential PSRGs), and the NCDEQ IHSB Protection of
Groundwater Preliminary Soil Remediation Goals (PoG PSRGs), updated September 2015. Soil
sample analytical results are summarized in Table 4 and the laboratory analytical reports are
included in Appendix F. Analytical results are shown on Figure 6.
VOCs
Volatile organic compounds were not detected in the six soil samples at concentrations that
exceed the Residential or Industrial PSRGs.
MW-9 10’-15’
§Exceed PoG PSRG; PCE, TCE
§Below regulatory standards; acetone (estimated), cis-1,2-DCE
MW-10 15’-18’
§Below regulatory standards; acetone (estimated), methylene chloride (estimated)
SB-01 5’-7’:
§Exceed PoG PSRG; p-isopropyltoluene, naphthalene, n-propylbenzene
§Below regulatory standards; toluene, ethylbenzene, n-butylbenzene, sec-butylbenzene,
tert-butylbenzene, isopropylbenzene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene
(estimated), and total xylenes (estimated)
SB-02 5’-7’
§Below regulatory standards; n-butylbenzene, sec-butylbenzene, cis-1,2-DCE,
naphthalene (estimated), n-propylbenzene (estimated), and vinyl chloride (estimated)
SB-03 5’-7’
§Exceed PoG PSRG; naphthalene
§Below regulatory standards; methylene chloride (estimated), n-butylbenzene (estimated),
sec-butylbenzene (estimated), isopropylbenzene (estimated), n-propylbenzene, 1,2,4-
trimethylbenzene (estimated)
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Atando Avenue Brownfields Site ■ Charlotte, NC
December 18, 2015 ■ Terracon Project No. 71157718
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SB-04 (1-2 ft)
§Exceed PoG PSRG; PCE
It should be noted that sample MW-9 10'-15' was the only soil sample that contained PCE and
TCE above the laboratory reporting limit and the PoG PSRG. The soil sample from boring MW-
9 also contained the highest concentration of PCE/TCE degradation product cis-1,2-DCE.
SVOCs
Samples MW-9 10’-15’, MW-10 15’-18’, and SB-04(1-2) contained no SVOCs above laboratory
reporting limits. SVOC results for the remaining samples are discussed below.
SB-01 5’-7’:
§Exceed Industrial PSRG; benzo(a)pyrene
§Exceed Residential PSRG; benzo(a)anthracene and benzo(b)fluoranthene
§Exceed PoG PSRG; 1-methylnaphthalene, 2-methylnaphthalene and naphthalene
§Below regulatory standards; anthracene (estimated), benzo(g,h,i)perylene (estimated),
benzo(k)fluoranthene (estimated), chrysene, fluorene (estimated), dibenz(a,h)anthracene
(estimated), fluoranthene, indeno(1,2,3-cd)perylene (estimated), n-nitrosidophenylamine
(estimated), phenanthrene, and pyrene
SB-02 5’-7’
§Below regulatory standards (estimated); benzo(a)anthracene, benzo(a)pyrene,
benzo(b)fluoranthene, chrysene, fluoranthene, phenanthrene, and pyrene
SB-03 5’-7’
§Exceed Industrial PSRG; benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene,
benzo(g,h,i)perylene, benzo(k)fluoranthene, and indeno(1,2,3-cd)pyrene
§Below regulatory standards; acenaphthene (estimated), anthracene (estimated),
chrysene, dinbenz(a,h)anthracene (estimated), dibenzofuran (estimated), fluoranthene,
fluorene (estimated), phenanthrene, and pyrene
Sample SB-03 5’-7’ exhibited the highest SVOC concentrations.
5.4 Soil Vapor Sample Results
No leaks were detected in the sample manifolds during the initial dead-head or shut-in tests. After
purging, the purge tubing was screened for helium and VOCs. VOCs were not detected within
the purge tubing for each of the four soil vapor samples. During purging, helium was not detected
in the tubing for samples SV-01 and SV-04 but was detected at low concentrations in the sample
manifolds for samples SV-02 and SV-03. The helium concentrations detected in samples SV-02
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Atando Avenue Brownfields Site ■ Charlotte, NC
December 18, 2015 ■ Terracon Project No. 71157718
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and SV-03 during field screening correspond to leaks less than 0.2%; thus, the leaks did not pose
a concern for sample collection.
As described in Table 1, sample SV-03 was also analyzed for helium by the analytical lab to
obtain a more reliable leak quantification. Based on the laboratory analytical result for sample
SV-03 helium was not detected in the sample (<0.13%). A hypothetical worst-case scenario
concentration of 0.13% helium in sample SV-03 would correspond to a 1.5% leak, considering a
time-weighted average helium concentration of 8.9% inside the sampling shroud during sampling.
A 1.5% leak is well below the 10% leak threshold specified in the NCDEQ Vapor Intrusion
Guidance (2014); therefore, the QA/QC helium sample supports the integrity of the soil vapor
sample results.
Laboratory analytical results for the soil vapor samples were compared to the NCDEQ Soil Gas
Screening Concentrations (SGSL) for residential and non-residential exposure scenarios,
updated September 2015.
§Sample SV-01 (office area) contained m,p-xylene and o-xylene above laboratory reporting
limits but below the SGSLs. No other constituents were detected above laboratory
reporting limits.
§Sample SV-02 (safe room) contained naphthalene (43 µg/m3) which exceeded its
residential SGSL of 20.9 µg/m3. No other compounds were detected above the residential
or industrial SGSLs. Ethylbenzene, m,p-xylene, and o-xylene were detected at
concentrations higher than the laboratory reporting limits but lower than regulatory
standards.
§Sample SV-03 (locker room) contained PCE at a concentration above laboratory reporting
limits but PCE did not exceed the residential or industrial SGSLs. Helium analysis on
sample SV-03 yielded a non-detect (<0.13%) result. No other constituents were detected
in the sample above laboratory reporting limits.
§Sample SV-04 (warehouse) contained PCE (4,100 µg/m3) which exceeds its industrial
(3,500 µg/m3) and residential (278 µg/m3) SGSLs. TCE (31 µg/m3) was found above its
residential PSRG of 13.9 µg/m3. Ethylbenzene, m,p-xylene and o-xylene were also
detected above laboratory reporting limits but below their respective SGSLs.
Soil vapor sample results are shown on Figure 8 and summarized on Table 5. The laboratory
analytical report is included in Appendix F.
5.5 Indoor and Outdoor Air Sample Results
PID and helium detector measurements at sample locations IA-01 and OA-01 were non-detect
(0.0 ppm). Laboratory analytical results for the indoor and outdoor air samples were compared
to the NCDEQ Indoor Air and Crawlspace Screening Concentrations (IASL) for residential and
Limited Site Investigation
Atando Avenue Brownfields Site ■ Charlotte, NC
December 18, 2015 ■ Terracon Project No. 71157718
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non-residential exposure scenarios, updated September 2015. The values assuming a target
carcinogenic risk of 1.0E-06 and a target hazard quotient of 0.2 (i.e., the IASL(A) values on the
screening tables) were used for this assessment.
§Indoor air sample IA-01 contained naphthalene (0.61µg/m3) which exceeds the non-
residential IASL of 0.361µg/m3. Additionally, benzene (0.75 µg/m3) and chloroform (0.29
µg/m3) were detected at concentrations exceeding their respective residential IASL. PCE,
ethylbenzene, m,p- and o-xylene were detected above laboratory reporting limits but
below their residential and non-residential IASLs.
§The outdoor/background air sample, OA-1, contained benzene above the residential IASL.
Laboratory results also indicate m,p-xylene, and o-xylene at concentrations below the
residential and non-residential IASLs. No other VOCs were detected above laboratory
reporting limits in sample OA-1.
Air sample results are shown on Figure 8 and summarized on Table 5. The laboratory analytical
report is included in Appendix F.
6.0 SUMMARY
Terracon performed activities at the site in August, October and November 2015. A brief summary
of these activities and associated results is provided below.
§A GPR survey was performed to determine the presence of reportedly abandoned USTs
in the northern portion of the site. The GPR survey identified two former UST locations
where the subsurface profile was indicative of backfilled soils but no other USTs or former
UST locations were identified in the northern portion of the site.
§A land survey was performed at the site to obtain a survey plat that will be part of the
Brownfields Agreement. Northing, easting and elevation measurements for each of the
on-site monitoring wells were also surveyed.
§Shallow monitoring wells MW-9 and MW-10 were installed near the northern property
boundary to evaluate impacts from potential up-gradient sources.
§Groundwater samples were collected from 10 on-site monitoring wells. A sample was not
collected from well MW-1 due to the presence of free product in the well.
o Groundwater levels were measured between 11.26 and 19.29 ft bgs in the on-site
monitoring wells.
o Groundwater flow direction at the site is towards the south/southeast.
o CVOCs were detected above the 2L Standards in wells MW-5, MW-8, MW-9, MW-
10, and deep well DW-1.
o CVOC concentrations were highest in groundwater samples from wells MW-9 and
MW-5.
Limited Site Investigation
Atando Avenue Brownfields Site ■ Charlotte, NC
December 18, 2015 ■ Terracon Project No. 71157718
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o CVOCs were detected at concentrations up to two orders of magnitude higher than
the highest non-chlorinated compounds in the groundwater.
o Non-chlorinated VOCs were detected above the 2L Standards in wells MW-2 and
MW-3.
§Six soil samples were collected in the vicinity of wells MW-5 and MW-9 at sample depths
ranging from 2-18 ft bgs.
o VOCs were not detected at concentrations exceeding the residential and industrial
PSRGs; however, four of the six samples had VOC detections exceeding the PoG
PSRG.
o SVOCs were detected at concentrations exceeding industrial and residential
PSRGs in two of the six samples. The remaining four samples did not contain
SVOCs above regulatory standards.
§Four sub-slab soil vapor samples were collected in the office and manufacturing ares of
the on-site facility. Additionally, one indoor air and one outdoor air sample were collected
concurrently with the soil vapor samples.
o PCE was detected at a concentration exceeding the industrial SGSL in SV-04
(warehouse area). No other compounds were detected exceeding the industrial
SGSL in the sub-slab vapor samples.
o VOCs were detected at levels exceeding the residential SGSL in samples SV-02
and SV-04.
o VOCs were not detected above regulatory standards in samples SV-01 (office
area) and SV-03 (locker room).
o The indoor air sample contained naphthalene at a concentration exceeding the
non-residential (and residential) IASL. It also contained benzene and chloroform
above residential IASLs. No other compounds were detected above regulatory
standards.
o The outdoor air sample contained benzene above residential IASLs. No other
compounds were detected above regulatory standards.
7.0 CONCLUSIONS AND RECOMMENDATIONS
Based on the scope of services described in this report and subject to the limitations described
herein, Terracon provides the following conclusions.
§Groundwater results indicate that CVOCs are present at concentrations exceeding
regulatory standards near the north-central property boundary at the site. CVOC
concentrations were highest in well MW-9, which is located at the northern property
boundary. The shallow and narrow lateral occurrence of CVOCs at wells MW-9 and MW-
5 suggests that a surface or near-surface off-site CVOC source is relatively close to the
northern property boundary.
Limited Site Investigation
Atando Avenue Brownfields Site ■ Charlotte, NC
December 18, 2015 ■ Terracon Project No. 71157718
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§The presence of CVOCs in deep well DW-1 but not in the surrounding shallow wells
indicates that the high density chlorinated compounds have migrated to a deeper, down-
gradient zone in the aquifer. CVOCs were not detected in shallow down-gradient wells at
the site.
§The potential off-site CVOC source is believed to be located on the adjacent parcel to the
north of the site where the Dy-Dee Diaper business formerly operated and where several
rusted 55-gallon drums and ASTs were observed by Terracon and others.
§Terracon concludes that there is sufficient evidence that the property owner is not
responsible or liable for the CVOC contamination in the northern portion of the site.
§Non-chlorinated VOCs such as benzene and naphthalene were detected in monitoring
wells MW-2 and MW-3 above regulatory standards. Terracon concludes that these results
are consistent with historical groundwater results and are likely associated with the on-
site UST releases that are subject of a separate investigation (IHSB Incident No.
NONCD0001992).
§Both chlorinated and non-chlorinated VOCs, as well as SVOCs were detected above
regulatory standards in six soil samples that were advanced in the vicinity of wells MW-5
and MW-9.
§Detections of PCE in near-surface soil sample SB-04 (1-2) are believed to be the result of
the following processes:
o SB-04 is located directly down-gradient of the off-site ASTs and rusted drums
located on the adjacent Dy-Dee Diaper property to the north. Additionally, boring
SB-04 is located in a topographic low spot that appears to be an east-west trending
drainage ditch to direct stormwater flow during storm events. This suggests that
an offsite spill/source product on the adjacent property to the north would likely be
washed towards the area where boring SB-04 was advanced.
o During installation of well MW-9, soil cuttings were temporarily staged in the area
where SB-04 (1-2) was collected. The soil cuttings from well MW-9 are known to
be impacted by PCE (see sample results for MW-9 10'-15’). It is possible that
residual amounts of the temporarily staged soil cuttings from well MW-9 were not
removed and placed into 55-gallon IDW drums; thus, PCE from the remaining
impacted soil could have leached into the ground at boring SB-04. Terracon
attempted to collect a shallow soil sample on the opposite side of well MW-9 but
could not advance the hand auger due to an asphalt ground cover.
§Sub-slab soil vapor conclusions:
o PCE was detected exceeding the industrial SGSL in sample SV-04 (manufacturing
area). Additionally, TCE was detected above its residential PSRG in sample SV-
04. The presence of these two CVOCs in the sub-slab sample located near well
MW-5 is thought to be due to off-gassing from impacted groundwater originating
from the suspected off-site source. Although screening levels were exceeded, it
should be considered that the concrete floor slab in the manufacturing area is
relatively thick (8 inches were measured at SV-04 and the tenant reported slab
Limited Site Investigation
Atando Avenue Brownfields Site ■ Charlotte, NC
December 18, 2015 ■ Terracon Project No. 71157718
Responsive ■Resourceful ■Reliable 19
thicknesses up to 13 inches) and may perform better than average in restricting
vapor intrusion. The warehouse also has large bay doors at the eastern and
western ends of the building for truck deliveries and pickups. The doors appear to
be open during work hours. The increased slab thickness suggests a lower risk
for vapor intrusion and the increased ventilation in the warehouse area suggests
that indoor air is unlikely to have high concentrations of VOCs. Terracon
recommends collecting an indoor air sample in the warehouse area to verify indoor
air concentrations are below standards.
o Sample SV-02 (safe room) contained naphthalene exceeding its residential SGSL.
The area where sample SV-02 was collected is near the break room and is not
continuously occupied. Though the source of the naphthalene is unknown, it is
thought to be related to the UST incident at the site. No industrial SGSLs were
exceeded in the locker room/safe room/office area samples. In addition, no SGSLs
were exceeded in the office (and locker room) area where workers are more likely
to spend an extended period of time. This suggests that workers at the site are
not immediately endangered by vapor intrusion in these areas.
§The presence of CVOCs (in groundwater, smear zone soil, and soil vapor) in the northern
portion of the property appears to be related to an up-gradient off-site source.
Remediation would presumably be the responsibility of the adjoining landowner; however,
the contamination on the subject property may be addressed within the Brownfields
Program.
APPENDIX A – WELL CONSTRUCTION RECORD
Sources: Esri, HERE, DeLorme, Intermap, increment P Corp., GEBCO, USGS, FAO, NPS, NRCAN,GeoBase, IGN, Kadaster NL, Ordnance Survey, Esri Japan, METI, Esri China (Hong Kong), swisstopo,MapmyIndia, © OpenStreetMap contributors, and the GIS User Community
PH. [phone] terracon.com
2020 STARITA RD, SUITE E CHARLOTTE, NC
FIGURE
1
SITE LOCATION MAP
ATANDO AVENUE BROWNFIELDS SITE527 ATANDO AVE.CHARLOTTE, NC
71157718
CZ
CLC
11/18/2015
Project No.:
Drawn By:
Checked By:
Date:
N :\P r o j e c t s \2 0 1 5 \7 1 1 5 7 7 1 8 \F i g u r e s \M X D \1 _S i t e L o c .m x d
³
0 2,000 4,0001,000 Feet1 inch = 2,000 feet
Legend
Site Parcel Boundary
1:24,000
Site
@A
@A
@A
@A
@A
@A
@A
ED@A
@A
@A
O f f i c e A r e a
W a r e h o u s e A r e a
M e t a l C u t t i n g / P r o d u c t i o n W a r e h o u s e
F o r m e r L a u n d r y / D r y C l e a n i n g F a c i l i t y
F o r m e r
C a r
R e p a i r
Atando Avenue
Railroad Tracks
L e o t a D r i v e
SV-4
MW-9
MW-1
MW-4DW-1 MW-2
MW-3
MW-6
MW-7
MW-5
MW-8
MW-10
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AEX,Getmapping, Aerogrid, IGN, IGP, swisstopo, and the GIS User Community
PH. [phone] terracon.com
2020 STARITA RD, SUITE E CHARLOTTE, NC
FIGURE
2
SITE LAYOUT MAP
ATANDO AVENUE BROWNFIELDS SITE527 ATANDO AVE.CHARLOTTE, NC
71157718
CZ
CLC
11/18/2015
Project No.:
Drawn By:
Checked By:
Date:
N :\P r o j e c t s \2 0 1 5 \7 1 1 5 7 7 1 8 \F i g u r e s \M X D \2 _S i t e M a p .m x d
³
0 60 12030Feet1 inch = 60 feet
Notes:- Locations of building footprint and site features are approximate.- Parcel data taken from Mecklenburg County GIS website.- Monitoring well locations are based on November 2015 survey.- Sample location will be adjusted based on field conditions.
Legend
ED Deep Monitoring Well
@A Shallow Monitoring Well
Potential Off-Site Source Areas
Site Parcel Boundary
Parcel Boundaries
Former UST
@A
@A
@A
@A
@A
@A
@A
ED@A
@A
@A
O f f i c e A r e a
W a r e h o u s e A r e a
M e t a l C u t t i n g / P r o d u c t i o n W a r e h o u s e
F o r m e r L a u n d r y / D r y C l e a n i n g F a c i l i t y
F o r m e r
C a r
R e p a i r
Atando Avenue
Railroad Tracks
L e o t a D r i v e
MW-1NA
MW-6(725.62)
MW-7(727.66)
MW-5(727.99)
MW-8(728.65)
MW-9(729.41)
MW-10(729.21)
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AEX,Getmapping, Aerogrid, IGN, IGP, swisstopo, and the GIS User Community
PH. [phone] terracon.com
2020 STARITA RD, SUITE E CHARLOTTE, NC
FIGURE
3
GW ELEVATION - SHALLOW WELLSOCTOBER 2015
ATANDO AVENUE BROWNFIELDS SITE527 ATANDO AVE.CHARLOTTE, NC
71157718
CZ
CLC
11/18/2015
Project No.:
Drawn By:
Checked By:
Date:
N :\P r o j e c t s \2 0 1 5 \7 1 1 5 7 7 1 8 \F i g u r e s \M X D \3 _G W _C o n t o u r s .m x d
³
0 60 12030Feet1 inch = 60 feet
Notes:- Wells were gauged on 10/8/2015 and reported in ft msl.- ft msl = feet above mean sea level- NA - MW-1 was not included in calculating contours due to free product.- Deep well DW-1 not included.- Locations of building footprint and site features are approximate.- Parcel data taken from Mecklenburg County GIS website.- Monitoring well locations and elevations are based on November 2015 survey.
Legend
ED Deep Monitoring Well
@A Shallow Monitoring Well
Groundwater Elev. Contour (Dashed where Inferred)
Potential Off-Site Source Areas
Site Parcel Boundary
Parcel Boundaries
Former UST
7 2 7 f t m s l
7 2 6 f t m s l
7 2 8 f t m s l
7 2 5 f t m s l
7 2 9 f t m s l
MW-3(724.36)
MW-4(724.57)
DW-1 MW-2(725.36)(724.44)
@A
@A
@A
@A
@A
@A
@A
ED@A
@A
@A
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AEX,Getmapping, Aerogrid, IGN, IGP, swisstopo, and the GIS User Community
PH. [phone] terracon.com
2020 STARITA RD, SUITE E CHARLOTTE, NC
FIGURE
4
TOTAL CVOC CONCENTRATIONSHALLOW WELLS - AUGUST/OCTOBER 2015
ATANDO AVENUE BROWNFIELDS SITE527 ATANDO AVE.CHARLOTTE, NC
71157718
CZ
CLC
10/24/2015
Project No.:
Drawn By:
Checked By:
Date:
N :\P r o j e c t s \2 0 1 5 \7 1 1 5 7 7 1 8 \F i g u r e s \M X D \4 _C V O C _C o n c .m x d
³
0 60 12030Feet1 inch = 60 feet
Notes:- Wells were sampled on 10/8/2015.- All concentrations in ug/L.- CVOCs = Chlorinated volatile organic compounds.- NCAC 2L GWQS - North Carolina Administrative Code Subchapter 2L Groundwater Quality Standards 4/2013.- Detections highlighted in grey exceed their respective NCAC 2L GWQS.- J indicates an estimated concentration above the method detection limit but below the laboratory reporting limit.- CVOC totals include tetrachloroethene, trichloroethene, cis- and trans-1,2-dichloroethene, 1,1-dichloroethene, 1,2-dichloroethane, and vinyl chloride.- Deep well DW-1 not used for contouring.- Locations of building footprint and site features are approximate.- Parcel data taken from Mecklenburg County GIS website.- Monitoring well locations are based on the November 2015 survey.
Legend
ED Deep Monitoring Well
@A Shallow Monitoring Well
Total CVOC Concentration1-10 ug/L
10-100 ug/L
100-1,000 ug/L
1,000-10,000 ug/L
>10,000 ug/LFormer USTParcel BoundariesPotential Off-Site Source AreasSite Parcel Boundary
O f f i c e A r e a
W a r e h o u s e A r e a
M e t a l C u t t i n g / P r o d u c t i o n W a r e h o u s e
F o r m e r L a u n d r y /
D r y C l e a n i n g F a c i l i t y
F o r m e r
C a r
R e p a i r
Atando Avenue
Railroad Tracks
L e o t a D r i v e
MW-2 10/08/15Benzene58.2Ethylbenzene4.5p-Isopropyltoluene 3.6Naphthalene87.9Xylenes (total)3.0o-Xylene 3.0
MW-3 10/08/15Benzene1.6Naphthalene4.0
MW-5 10/08/15cis-1,2-Dichloroethene 1,000trans-1,2-Dichloroethene 12.2Tetrachloroethylene2,790Trichloroethene1,870Vinyl chloride 41.3
MW-8 10/08/15cis-1,2-Dichloroethene 19.8Tetrachloroethylene163Trichloroethene25.5
MW-9 08/27/15cis-1,2-Dichloroethene 5,550trans-1,2-Dichloroethene 48.51,1-Dichloroethene 11.51,2-Dichloroethane 0.34 JTetrachloroethylene4,460Trichloroethene2,880Vinyl chloride 6.5
MW-10 08/27/15cis-1,2-Dichloroethene 1.6Tetrachloroethylene2.7Trichloroethene3.3
MW-6 10/08/15Chloroform7.4
MW-1 10/08/15No sample was collected due to presence of free product in well.
MW-4 10/08/15No compounds detected above laboratory reporting limits
MW-7 10/08/15No compounds detected above laboratory reporting limits
DW-1 10/08/15cis-1,2-Dichloroethene 42.3Tetrachloroethylene148Trichloroethene78.2
@A
@A
@A
!(
!(
!(
!(
M e t a l C u t t i n g / P r o d u c t i o n W a r e h o u s e
F o r m e r L a u n d r y / D r y C l e a n i n g F a c i l i t y
SB-1
SB-3
SB-2
SB-4
MW-9
MW-5
MW-10
PH. [phone] terracon.com
2020 STARITA RD, SUITE E CHARLOTTE, NC
FIGURESOIL BORING LOCATION MAP
ATANDO AVENUE BROWNFIELDS SITE527 ATANDO AVE.CHARLOTTE, NC
71157718
CZ
CLC
11/24/2015
Project No.:
Drawn By:
Checked By:
Date:
N :\P r o j e c t s \2 0 1 5 \7 1 1 5 7 7 1 8 \F i g u r e s \M X D \5 _S o i l B o r i n g L o c .m x d
³
0 10 205Feet1 inch = 15 feet
Notes:- Locations of building footprint and site features are approximate.- Parcel data taken from Mecklenburg County GIS website.- Monitoring well locations are based on November 2015 survey.- SB locations are approximate and based on field measurements.
Legend
!(Soil Boring Location
ED Deep Monitoring Well
@A Shallow Monitoring Well
Site Parcel Boundary
Parcel Boundaries
Former UST
5
@A
@A
@A
!(
!(
!(
!(
M e t a l C u t t i n g / P r o d u c t i o n W a r e h o u s e
F o r m e r L a u n d r y / D r y C l e a n i n g F a c i l i t y
PH. [phone] terracon.com
2020 STARITA RD, SUITE E CHARLOTTE, NC
FIGURESOIL BORING RESULTS MAP
ATANDO AVENUE BROWNFIELDS SITE527 ATANDO AVE.CHARLOTTE, NC
71157718
CZ
CLC
12/03/2015
Project No.:
Drawn By:
Checked By:
Date:
N :\P r o j e c t s \2 0 1 5 \7 1 1 5 7 7 1 8 \F i g u r e s \M X D \6 _S o i l B o r i n g R e s u l t s .m x d
³
0 10 205Feet 1 inch = 15 feet
Notes:- Only detected compounds are shown.- Concentrations are reported in micrograms per kilogram (μg/kg)- "J" indicates an estimated concentration above the method detection limit but below the laboratory reporting limit.- ft bgs - feet below ground surface- PoG - Protection of Groundwater- PSRG - NCDEQ Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals, updated September 2015.- SVOCs - Semi-Volatile Organic Compounds- VOCs - Volatile Organic Compounds- Concentrations highlighted in grey exceed their respective PoG PSRG.- Concentrations highlighted in yellow exceed their respective PoG and residential health based PSRG.- Concentrations highlighted in orange exceed their respective PoG, residential, and industrial health based PSRG.- Locations of building footprint and site features are approximate.- Parcel data taken from Mecklenburg County GIS website.- Monitoring well locations are based on November 2015 survey.- SB locations are approximate and based on field measurements.
Legend
!(Soil Boring Location
ED Deep Monitoring Well
@A Shallow Monitoring Well
Site Parcel Boundary
Parcel Boundaries
Former UST 6
SB-04(1-2)11/11/15
V O C s Tetrachloroethene 40.2
S V O C s Sample was not analyzed for SVOCs.
SB-03 5'-7'08/26/15n-Butylbenzene 160 Jsec-Butylbenzene 176 JIsopropylbenzene115 JMethylene Chloride 220 JNaphthalene612n-Propylbenzene 3261,2,4-Trimethylbenzene 181 JAcenaphthene1580 JAnthracene2970 JBenzo(a)anthracene 9720Benzo(a)pyrene 8830Benzo(b)fluoranthene 13300Benzo(g,h,i)perylene 5820Benzo(k)fluoranthene 7200Chrysene9410Dibenz(a,h)anthracene 1770 JDibenzofuran782 JFluoranthene22400Fluorene 1590 JIndeno(1,2,3-cd)pyrene 5310Phenanthrene13300Pyrene16200
V O C s
S V O C s
SB-02 5'-7'08/26/15n-Butylbenzene 5.8sec-Butylbenzene 6.3cis-1,2-Dichloroethene 15.3Naphthalene5.0 Jn-Propylbenzene 2.9 JVinyl Chloride 2.2 JBenzo(a)anthracene 109 JBenzo(a)pyrene 91.2 JBenzo(b)fluoranthene 159 JChrysene109 JFluoranthene241 JPhenanthrene115 JPyrene175 J
S V O C s
V O C s
V O C s
S V O C s
MW-10 15'-18'08/26/15Acetone15.6 JMethylene Chloride 5.2 J
S V O C s Not detected above laboratory reporting limits.
V O C s
MW-9 10'-15'08/26/15Acetone27.3 Jcis-1,2-Dichloroethene 68.1Tetrachloroethene201Trichloroethene449VOCs
Not detected above laboratory reporting limits.S V O C s
@A
@A
@A
@A
@A
&(
&(
%2
%2
%2
%2SV-4
SV-1
SV-3
SV-2
IA-1
OA-1
MW-9
MW-1
MW-5
MW-10
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AEX,Getmapping, Aerogrid, IGN, IGP, swisstopo, and the GIS User Community
PH. [phone] terracon.com
2020 STARITA RD, SUITE E CHARLOTTE, NC
FIGURE
7
SUB-SLAB SOIL VAPOR ANDAIR SAMPLE LOCATIONS
ATANDO AVENUE BROWNFIELDS SITE527 ATANDO AVENUECHARLOTTE, NC
71157718
CZ
CLC
11/25/2015
Project No.:
Drawn By:
Checked By:
Date:
N :\P r o j e c t s \2 0 1 5 \7 1 1 5 7 7 1 8 \F i g u r e s \M X D \7 _S V _L o c a t i o n s .m x d
³
0 25 5012.5 Feet1 inch = 25 feet
Notes:- Locations of building footprint and site features are approximate.- Locations of interior walls and sample locations are approximate and based on a figure provided by Sunbelt-Turret and site observations and measurements by Terracon.- Parcel data obtained from the Mecklenburg County GIS website.
W o r k s h o p A r e a
Main Entrance
Metal Cutting / Production Warehouse
WarehouseArea
Parking Lot
Legend
&(Indoor Air Sample Location
&(Outdoor Air Sample Location
%2 Sub-Slab Soil Vapor Sample Location
@A Shallow Monitoring Well
Office Area
Metal Cutting / Production Area
Warehouse Area
Building Walls
Former USTSite Parcel
L o c k e r R o o m
L o c k e r R o o m
B r e a k R o o m
S a f e
R o o m
C o n f e r e n c e
R o o m
O f f i c e
S t o r a g e
S t o r a g e
S t o r a g e
B a t h r o o m
B a t h r o o m
O f f i c e
O f f i c e
O f f i c eOffice
O f f i c e
O f f i c e
W o r k
S t a t i o n s
W o r k
S t a t i o n
W o r k
S t a t i o n
F r o n t
D e s k
@A
@A
@A
@A
@A
&(
&(
%2
%2
%2
%2
MW-9
MW-1
MW-5
MW-10
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AEX,Getmapping, Aerogrid, IGN, IGP, swisstopo, and the GIS User Community
PH. [phone] terracon.com
2020 STARITA RD, SUITE E CHARLOTTE, NC
FIGURE
8
SUB-SLAB SOIL VAPOR ANDAIR SAMPLE RESULTS
ATANDO AVENUE BROWNFIELDS SITE527 ATANDO AVENUECHARLOTTE, NC
71157718
CZ
CLC
12/03/2015
Project No.:
Drawn By:
Checked By:
Date:
N :\P r o j e c t s \2 0 1 5 \7 1 1 5 7 7 1 8 \F i g u r e s \M X D \8 _S V _R e s u l t s .m x d
³
0 25 5012.5 Feet1 inch = 25 feet
Notes:- Only detected compounds are shown.- Concentrations are reported in micrograms per cubic meter (μg/m3).- DWM - North Carolina Department of Environmental Quality, Division of Waste Management- IASL - DWM Indoor Air and Crawlspace Screening Concentration, updated September 2015- SGSL - DWM Sub-slab and Exterior Soil Gas Screening Level, updated September 2015- Concentrations highlighted in yellow exceed their respective residential SGSL or IASL (whichever is applicable).- Concentrations highlighted in orange exceed their respective non-residential SGSL or IASL (whichever is applicable).- A target carcinogenic risk of 1.0E-06 and target hazard quotient of 0.2 was assumed for the IASL (i.e., IASL(A) on DWM's screening levels table).- Locations of building footprint and site features are approximate.- Locations of interior walls and sample locations are approximate and based on a figure provided by Sunbelt-Turret and site observations and measurements by Terracon.- Parcel data obtained from the Mecklenburg County GIS website.
W o r k s h o p A r e a
Main Entrance
Metal Cutting / Production Warehouse
WarehouseArea
Parking Lot
Legend
&(Indoor Air Sample Location
&(Outdoor Air Sample Location
%2 Sub-Slab Soil Vapor Sample Location
@A Shallow Monitoring Well
Office Area
Metal Cutting / Production Area
Warehouse Area
Building WallsFormer UST
Site Parcel
L o c k e r R o o m
L o c k e r R o o m
B r e a k R o o m
S a f e
R o o m
C o n f e r e n c e
R o o m
O f f i c e
S t o r a g e
S t o r a g e
S t o r a g e
B a t h r o o m
B a t h r o o m
O f f i c e
O f f i c e
O f f i c eOffice
O f f i c e
O f f i c e
W o r k
S t a t i o n s
W o r k
S t a t i o n
W o r k
S t a t i o n
F r o n t
D e s k
IA-01 11/12/15Benzene0.75Chloroform0.29Ethylbenzene1.1Naphthalene0.61Tetrachloroethylene1.1m,p-Xylene 3.1o-Xylene 1.2
SV-02 11/12/15Ethylbenzene33Naphthalene43m,p-Xylene 250o-Xylene 140
SV-01 11/12/15m,p-Xylene 21o-Xylene 18
SV-03 11/12/15Tetrachloroethene29
SV-04 11/12/15Tetrachloroethene4,100Trichloroethene31Ethylbenzene33m,p-Xylene 140o-Xylene 38
Table 1
Sampling and Analysis Plan
Atando Avenue Brownfields Site
527 Atando Ave
Charlotte, Mecklenburg Couny, NC
Terracon Project No. 71157718
SAMPLE ID SAMPLE DATE SAMPLE MEDIUM SAMPLE INTERVAL ANALYTICAL METHOD
MW-2 10/08/15 Groundwater ? - 34 ft bgs 8260; 1,4-Dioxane
MW-3 10/08/15 Groundwater ? - 33 ft bgs 8260; 1,4-Dioxane
MW-4 10/08/15 Groundwater ? - 32 ft bgs 8260; 1,4-Dioxane
MW-5 10/08/15 Groundwater ? - 30 ft bgs 8260; 1,4-Dioxane
MW-6 10/08/15 Groundwater 20 - 30 ft bgs 8260; 1,4-Dioxane
MW-7 10/08/15 Groundwater 18 - 28 ft bgs 8260; 1,4-Dioxane
MW-8 10/08/15 Groundwater 24 - 34 ft bgs 8260; 1,4-Dioxane
MW-9 08/27/15 Groundwater 10 - 25 ft bgs 8260; 1,4-Dioxane
MW-10 08/27/15 Groundwater 10 - 25 ft bgs 8260; 1,4-Dioxane
DW-1 10/08/15 Groundwater ? - 86 ft bgs 8260; 1,4-Dioxane
MW-9 10'-15'08/26/15 Soil 10-15 ft bgs 8260; 8270
MW-10 15'-18'08/26/15 Soil 15-18 ft bgs 8260; 8270
SB-01 5'-7'08/26/15 Soil 5-7 ft bgs 8260; 8270
SB-02 5'-7'08/26/15 Soil 5-7 ft bgs 8260; 8270
SB-03 5'-7'08/26/15 Soil 5-7 ft bgs 8260; 8270
SB-04(1-2)11/11/15 Soil 1-2 ft bgs 8260
IA-01 11/12/15 Indoor Air (Gas)5 ft ags TO-15 Low Level*
OA-01 11/12/15 Outdoor Air (Gas)5 ft ags T0-15 Low Level*
SV-01 11/12/15 Soil Vapor (Gas)Sub-Slab TO-15*
SV-02 11/12/15 Soil Vapor (Gas)Sub-Slab TO-15*
SV-03 11/12/15 Soil Vapor (Gas)Sub-Slab TO-15*; Helium
SV-04 11/12/15 Soil Vapor (Gas)Sub-Slab TO-15*
Notes:
ft bgs - feet below ground surface
ft als - feet above ground surface
? - indicates that the depth to the top of the screened interval is unknown
* - reported compounds for TO-15 and TO-15 SIM are limited to compounds detected in site groundwater and include:
tetrachloroethylene, trichloroethene, cis-1,2-dichloroethene, trans-1,2-dichloroethene, 1,1-dichloroethene, 1,2-dichloroethane, vinyl chloride, benzenen chloroform, ethylbenzene,
naphthalene, total xyelnes, o-xylene
Table 2
Well Construction and Groundwater Elevations (October 2015)
Atando Avenue Brownfields Site
527 Atando Ave
Charlotte, Mecklenburg Couny, NC
Terracon Project No. 71157718
WELL I.D.DATE
MEASURED
SCREEN INTERVAL
(ft bls )
TOP OF CASING
ELEVATION
(ft msl)
DEPTH TO WATER
(ft BTOC)
GROUNDWATER
ELEVATION
(ft msl)
SHALLOW MONITORING WELLS
MW-1 10/08/15 ? - 34 743.39 18.15*NA
MW-2 10/08/15 ? - 34 743.73 19.29 724.44
MW-3 10/08/15 ? - 33 738.79 14.43 724.36
MW-4 10/08/15 ? - 32 739.04 14.47 724.57
MW-5 10/08/15 ? - 30 740.75 12.76 727.99
MW-6 10/08/15 20 - 30 742.90 17.28 725.62
MW-7 10/08/15 18 - 28 743.93 16.27 727.66
MW-8 10/08/15 24 - 34 739.91 11.26 728.65
MW-9 10/08/15 10 - 25 741.16 11.75 729.41
MW-10 10/08/15 10 - 25 741.79 12.58 729.21
DW-1 10/08/15 ? - 86 739.14 13.78 725.36
Notes:
ft bls - feet below land surface
ft BTOC - feet below top of casing
NM - Not measured
NA - Not applicable
ft msl - feet above mean sea level
* Depth to water
Well construction data obtained from HRP report and Terracon's field measurements.
No well construction information available for wells MW-1 through MW-5 and DW-1.
Well top of casing elevations based on November 2015 survey by Dewberry.
DEEP MONITORING WELLS
Table 3
Groundwater Analytical Results (August/October 2015)
Atando Avenue Brownfields Site
527 Atando Ave
Charlotte, Mecklenburg Couny, NC
Terracon Project No. 71157718
Sample ID:
Sample Date:
Screen Interval
(ft bls):
Chlorinated Volatile Organic Compounds (EPA Method 8260)
Tetrachloroethylene 0.7 5.0 <1.0 <1.0 <1.0 2,790 <1.0 <1.0 163 4,460 2.7 148
Trichloroethene 3 5 <1.0 <1.0 <1.0 1,870 <1.0 <1.0 25.5 2,880 3.3 78.2
cis-1,2-Dichloroethene 70 70 <1.0 <1.0 <1.0 1,000 <1.0 <1.0 19.8 5,550 1.6 42.3
trans-1,2-Dichloroethene 100 100 <1.0 <1.0 <1.0 12.2 <1.0 <1.0 <1.0 48.5 <0.50 <1.0
1,1-Dichloroethene 7 7 <1.0 <1.0 <1.0 <10 <1.0 <1.0 <1.0 11.5 <0.50 2.5
1,2-Dichloroethane 0.4 5 <1.0 <1.0 <1.0 <10 <1.0 <1.0 <1.0 0.34 J <0.50 <1.0
Vinyl chloride 0.03 2 <1.0 <1.0 <1.0 41.3 <1.0 <1.0 <1.0 6.5 <1.0 <1.0
Chloroform 70 NS <1.0 <1.0 <1.0 <10 7.4 <1.0 <1.0 <0.50 <0.50 <1.0
Total CVOCs <1.0 <1.0 <1.0 5,714 7.4 <1.0 208 12,957 7.6 271
Non-Chlorinated Volatile Organic Compounds (EPA Method 8260)
Benzene 1 5 58.2 1.6 <1.0 <10 <1.0 <1.0 <1.0 <0.50 <0.50 <1.0
Ethylbenzene 600 700 4.5 <1.0 <1.0 <10 <1.0 <1.0 <1.0 <0.50 <0.50 <1.0
p-Isopropyltoluene 70 NS 3.6 <1.0 <1.0 <10 <1.0 <1.0 <1.0 <0.50 <0.50 <1.0
Naphthalene 6 NS 87.9 4.0 <1.0 <10 <1.0 <1.0 <1.0 <2.0 <2.0 <1.0
Xylenes (total)500 10,000 3.0 <2.0 <2.0 <20 <2.0 <2.0 <2.0 <1.0 <1.0 <2.0
o-Xylene 500 NS 3.0 <1.0 <1.0 <10 <1.0 <1.0 <1.0 <0.5 <0.5 <1.0
Notes:
Only detected compounds are shown.
Concentrations are reported in micrograms per liter (μg/L)
NCAC 2L GWQS - North Carolina Administrative Code Subchapter 2L Groundwater Quality Standards (April 1, 2013).
Concentrations highlighted in grey exceed their respective NCAC 2L GWQS.
"J" indicates an estimated concentration above the method detection limit but below the laboratory reporting limit.
NS - no standard
Well MW-1 not sampled due to presence of free product.
?-86
10/08/15
?-34 ?-33 ?-32 ?-30 20-30 18-28 24-34 10-25 10-25
DW-1
10/08/15 10/08/15 10/08/15 10/08/15 10/08/15 10/08/15 10/08/15 08/27/15 08/27/15
MW-5 MW-6 MW-7 MW-8 MW-9 MW-10MW-4
Analyte NCAC 2L
GWQS EPA MCLs
MW-2 MW-3
Table 4
Soil Analytical Results (August/November 2015)
Atando Avenue Brownfields Site
527 Atando Ave
Charlotte, Mecklenburg Couny, NC
Terracon Project No. 71157718
Sample ID:
Sample Date:
Sample
Interval (ft
bgs):
Volatile Organic Compounds (EPA Method 8260)
Acetone 24,000 12,000,000 100,000,000 27.3 J 15.6 J <123 <114 <5740 <6.1
n-Butylbenzene 2,400 110,000 110,000 <4.1 <4.4 1520 5.8 160 J <6.1
sec-Butylbenzene 2,200 150,000 150,000 <4.1 <4.4 827 6.3 176 J <6.1
tert-Butylbenzene 1,700 180,000 180,000 <4.1 <4.4 208 <5.7 <287 <6.1
cis-1,2-Dichloroethene 360 32,000 460,000 68.1 <4.4 <123 15.3 <287 <6.1
Ethylbenzene 8,100 5,800 25,000 <4.1 <4.4 465 <5.7 <287 <6.1
Isopropylbenzene NS NS NS <4.1 <4.4 2520 <5.7 115 J <6.1
p-Isopropyltoluene 680 NS NS <4.1 <4.4 1120 <5.7 <287 <6.1
Methylene Chloride 23 57,000 640,000 <4.1 5.2J <491 <22.8 220 J <6.1
Naphthalene 210 3,800 17,000 <4.1 <4.4 2760 5.0J 612 <6.1
n-Propylbenzene 1,500 260,000 260,000 <4.1 <4.4 6360 2.9J 326 <6.1
Tetrachloroethene 5 16,000 78,000 201 <4.4 <123 <5.7 <287 40.2
Trichloroethene 18 820 3,800 449 <4.4 <123 <5.7 <287 <6.1
Toluene 5,500 820,000 820,000 <4.1 <4.4 139 <5.7 <287 <6.1
1,2,4-Trimethylbenzene 6,700 11,600 48,000 <4.1 <4.4 187 <5.7 181 J <6.1
1,3,5-Trimethylbenzene 6,700 156,000 182,000 <4.1 <4.4 65.4 J <5.7 <287 <6.1
Vinyl Chloride 0.19 59 1,700 <8.1 <8.9 <246 2.2J <574 <12.1
Total Xylenes 6,000 130,000 258,000 <8.1 <8.9 1010 <11.4 <574 <12.1
m&p-Xylene NS 110,000 388,000 <8.1 <8.9 1010 <11.4 <574 <12.1
o-Xylene NS 130,000 434,000 <4.1 <4.4 96.1 J <5.7 <287 <6.1
Semi-Volatile Organic Compounds (EPA Method 8270)
Acenaphthene 8,400 720,000 9,000,000 <402 <391 <388 <406 1580 J NA
Anthracene 660,000 3,600,000 46,000,000 <402 <391 128 J <406 2970 J NA
Benzo(a)anthracene 180 160 2,900 <402 <391 461 109 J 9720 NA
Benzo(a)pyrene 59 16 290 <402 <391 401 91.2 J 8830 NA
Benzo(b)fluoranthene NS 420 1,800 <402 <391 638 159 J 13300 NA
Benzo(g,h,i)perylene 59 16 290 <402 <391 263 J <406 5820 NA
Benzo(k)fluoranthene 600 160 2,900 <402 <391 286 J <406 7200 NA
Chrysene 18,000 16,000 290,000 <402 <391 450 109 J 9410 NA
Dibenz(a,h)anthracene 190 16 290 <402 <391 85J <406 1770 J NA
Dibenzofuran 5,200 15,000 200,000 <402 <391 <388 <406 782 J NA
Fluoranthene 330,000 480,000 6,000,000 <402 <391 1020 241 J 22400 NA
Fluorene 56,000 480,000 6,000,000 <402 <391 181 J <406 1590 J NA
Indeno(1,2,3-cd)pyrene 2,000 160 2,900 <402 <391 230 J <406 5310 NA
1-Methylnaphthalene 55 18,000 73,000 <402 <391 1090 <406 <4520 NA
2-Methylnaphthalene 1,600 48,000 600,000 <402 <391 1620 <406 <4520 NA
Naphthalene 210 3,800 17,000 <402 <391 1350 <406 <4520 NA
N-Nitrosodiphenylamine NS 110,000 470,000 <402 <391 372 J <406 <4520 NA
Phenanthrene 68,000 NS NS <402 <391 569 115 J 13300 NA
Pyrene 220,000 360,000 4,600,000 <402 <391 741 175 J 16200 NA
Notes:
Only detected compounds are shown.
Concentrations are reported in micrograms per kilogram (μg/kg)
"J" indicates an estimated concentration above the method detection limit but below the laboratory reporting limit.
ft bgs - feet below ground surface
NA - not analyzed
NS - no standard
PoG - Protection of Groundwater
PSRG - NCDEQ Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals, updated September 2015.
Concentrations highlighted in grey exceed their respective protection of groundwater PSRG.
Concentrations highlighted in yellow exceed their respective protection of groundwater and residential health based PSRG.
Concentrations highlighted in orange exceed their respective protection of groundwater, residential, and industrial health based PSRG.
SB-02 5'-7' SB-03 5'-7' SB-04(1-2)
Analyte PoG PSRG Residential
PSRG
MW-9 10'-
15'
MW-10 15'-
18'SB-01 5'-7'
Industrial
PSRG
5-7
08/26/15 08/26/15 08/26/15 08/26/15 08/26/15 11/11/15
10-15 15-18 5-7 5-7 5-7
Table 5
Air and Soil Vapor Sample Results (November 2015)
Atando Avenue Brownfields Site
527 Atando Ave
Charlotte, Mecklenburg Couny, NC
Terracon Project No. 71157718
Sample ID:
Sample Date:
Type:
SGSL IASL SGSL IASL Location:
Chlorinated Volatile Organic Compounds (EPA Method TO-15)
Tetrachloroethylene 278 8.34 3,500 35.0 <8.9 <8.8 29 4,100 <0.25 1.1
Trichloroethene 13.9 0.417 175 1.75 <7.0 <7.0 <6.8 31 <0.20 <0.20
cis-1,2-Dichloroethene NS NS NS NS <5.2 <5.1 <5.0 <7.3 <0.14 <0.14
trans-1,2-Dichloroethene NS NS NS NS <5.2 <5.1 <5.0 <7.3 <0.72 <0.72
1,1-Dichloroethene 1390 41.7 17,500 175 <5.2 <5.1 <5.0 <7.3 <0.072 <0.072
1,2-Dichloroethane 36.0 0.108 472 0.472 <5.3 <5.2 <5.1 <7.5 <0.15 <0.15
Vinyl chloride 55.9 0.168 2,790 2.79 <3.3 <3.3 <3.2 <4.7 <0.046 <0.047
Chloroform 40.7 0.122 533 0.533 <6.4 <6.3 <6.2 <9.0 <0.18 0.29
Non-Chlorinated Volatile Organic Compounds (EPA Method TO-15)
Benzene 120 0.360 1,570 1.57 <4.2 <4.1 <4.0 <5.9 0.42 0.75
Ethylbenzene 374 1.12 4,910 4.91 <5.7 33 <5.5 33 <0.16 1.1
Naphthalene 20.9 0.0826 263 0.361 <14 43 <13 <19 <0.48 0.61
m,p-Xylene 695 20.9 8,760 87.6 21 250 <5.5 140 0.45 3.1
o-Xylene 695 20.9 8,760 87.6 18 140 <5.5 38 0.16 1.2
Helium NS NS NS NS NA NA <0.13 %NA NA NA
Notes:
Concentrations are reported in micrograms per cubic meter (μg/m3) unless otherwise noted.
Only compounds that were detected in groundwater are shown.
ft ags - feet above ground surface
NA - not analyzed
NS - no standard
DWM - North Carolina Department of Environmental Quality, Division of Waste Management
IASL - DWM Indoor Air and Crawlspace Screening Concentration, updated September 2015
SGSL - DWM Sub-slab and Exterior Soil Gas Screening Level, updated September 2015
Concentrations highlighted in yellow exceed their respective residential SGSL or IASL (whichever is applicable).
Concentrations highlighted in orange exceed their respective non-residential SGSL or IASL (whichever is applicable).
A target carcinogenic risk of 1.0E-06 and target hazard quotient of 0.2 was assumed for the IASL (i.e., IASL(A) on DWM's screening levels table).
Office Area Safe Room Locker Room Warehouse
Sub-SlabSub-Slab Sub-Slab Sub-Slab
11/12/15 11/12/15 11/12/15
SV-02 SV-03 SV-04
Other Compounds (QA/QC)
Analyte
OA-01 IA-01
Outdoor Air Indoor Air
11/12/15 11/12/15
SE of Office Area Safe Room
SV-01Non-Residential
Screening LevelsScreening Levels
Residential
11/12/15
APPENDIX A – WELL CONSTRUCTION RECORD
APPENDIX B – FIELD FORMS AND SAMPLE SHEETS
Groundwater Sample Collection Records
Soil Vapor Sample Collection Records
Indoor/Outdoor Air Sample Collection Records
Indoor Air Building Survey Form
Indoor Air Sampling Instructions for Occupants

Typical air sampling
equipment
Instructions for Occupants
Indoor Air Sampling Events

In order to collect an indoor air sample in your structure that is both representative of indoor
conditions and avoids the common sources of background air contamination associated with household activities and consumer products, the Division of Waste Management (DWM) requests
your assistance.

To the extent possible, please follow the instructions below starting at least 48 hours prior to and
during the indoor air sampling event:
 Operate your heating and/or whole-house air conditioner as appropriate for the current weather
conditions
 Do not use wood stoves, fireplaces or auxiliary heating equipment
 Do not open windows or keep doors open
 Avoid using window air conditioners, fans or vents
 Do not smoke in the building
 Do not use air fresheners or odor eliminators
 Do not use paints or varnishes (up to a week in advance, if possible)
 Do not use cleaning products (e.g., bathroom cleaners, furniture polish, appliance cleaners, all-purpose cleaners, floor cleaners)
 Do not use cosmetics, including hair spray, nail polish remover, perfume, etc.
 Avoid bringing freshly dry-cleaned clothes into the building
 Do not engage in indoor hobbies involving the use of solvents
 Do not apply pesticides
 Do not store containers of gasoline, oil or petroleum-based or other solvents within the
building or attached garages (exception: fuel oil tanks)
 Do not operate or store automobiles in an attached garage
 Do not operate gasoline-powered equipment within the building, attached garage or around the
immediate perimeter of the building You will be asked a series of questions about the structure, consumer
products you store in your building, and household activities typically
occurring in the building. These questions are designed to identify “background” sources of indoor air contamination. While this investigation is
looking for a select number of chemicals related to the subsurface
contamination, the laboratory may be analyzing the indoor air samples for a
wide variety of chemicals. Thus, tetrachloroethene used in dry cleaning or
acetone found in nail polish remover might be found in your sample results.
Your cooperation is greatly appreciated.
If you have any questions about these instructions, please feel free to contact:

______________________________________________________________
______________________________________________________________

(Adapted from NJDEP Vapor Intrusion Guidance, October 2005)
APPENDIX C – GPR INVESTIGATION REPORT
Probe Utility Locating, L.L.C.
4185 Barrier Road
Concord, NC 29025
704-363-8663
704-784-2934 Fax
Chris L.Corbitt, PG
Senior Project Manager
Terracon Consultants
Reference:
527 Atando Ave.
Charlotte, NC
The following report details the findings of the utility locating services performed on September 10, 2015.
Based on the direction of Terracon’s Chris Corbitt and Megan Sears, an area on the north side of the building
was identified as the location of a possible underground storage tank (UST) and two removed UST’s.
Probe Utility Locating, Inc, Pat Tynan then used Ground-Penetrating Radar (GPR) measures to evaluate the
locations.
During this service, the area was scanned for the presence of underground storage tanks (UST). It appeared
that the locations where known UST’s had been removed, there was evidence of excavation, thus confirming
the removal. There was no evidence of tanks were found in the adjacent area where indicated by Mr. Corbitt.
Please feel free to contact me with any further questions or concerns.
Sincerely,
Patrick J. Tynan
Probe Utility Locating, L.L.C.
980-722-4290
[e-mail]
APPENDIX D – SURVEY PLAT
APPENDIX E – IDW WASTE MANIFEST
APPENDIX F – ANALYTICAL REPORTS AND CHAINS OF
CUSTODY
Groundwater Sample Analytical Reports – Pace Analytical
Soil Sample Analytical Reports – Pace Analytical
Gas Sample Analytical Report – Eurofins AirToxics
#=CL#
September 25, 2015
LIMS USE: FR - CHRIS CORBITT
LIMS OBJECT ID: 92265344
92265344
Project:
Pace Project No.:
RE:
Mr. Chris Corbitt
Terracon
2020 E-Starita Road
Charlotte, NC 28206
Atando Brownfields 71157718
Dear Mr. Corbitt:
Enclosed are the analytical results for sample(s) received by the laboratory on August 27, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 22
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 22
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
Lab ID Sample ID Matrix Date Collected Date Received
92265344001 MW-9 Water 08/27/15 14:25 08/27/15 16:10
92265344002 MW-10 Water 08/27/15 14:45 08/27/15 16:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 22
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92265344001 MW-9 SM 6200B 63 PASI-CCAH
92265344002 MW-10 SM 6200B 63 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
Sample:MW-9 Lab ID:92265344001 Collected:08/27/15 14:25 Received:08/27/15 16:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 08/29/15 06:08 71-43-20.50 0.25 1
Bromobenzene ND ug/L 08/29/15 06:08 108-86-10.50 0.25 1
Bromochloromethane ND ug/L 08/29/15 06:08 74-97-50.50 0.25 1
Bromodichloromethane ND ug/L 08/29/15 06:08 75-27-40.50 0.25 1
Bromoform ND ug/L 08/29/15 06:08 75-25-20.50 0.25 1
Bromomethane ND ug/L 08/29/15 06:08 74-83-95.0 0.50 1
n-Butylbenzene ND ug/L 08/29/15 06:08 104-51-80.50 0.25 1
sec-Butylbenzene ND ug/L 08/29/15 06:08 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 08/29/15 06:08 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 08/29/15 06:08 56-23-50.50 0.25 1
Chlorobenzene ND ug/L 08/29/15 06:08 108-90-70.50 0.25 1
Chloroethane ND ug/L 08/29/15 06:08 75-00-31.0 0.50 1
Chloroform ND ug/L 08/29/15 06:08 67-66-30.50 0.25 1
Chloromethane ND ug/L 08/29/15 06:08 74-87-31.0 0.50 1
2-Chlorotoluene ND ug/L 08/29/15 06:08 95-49-80.50 0.25 1
4-Chlorotoluene ND ug/L 08/29/15 06:08 106-43-40.50 0.25 1
1,2-Dibromo-3-chloropropane ND ug/L 08/29/15 06:08 96-12-81.0 0.50 1
Dibromochloromethane ND ug/L 08/29/15 06:08 124-48-10.50 0.25 1
1,2-Dibromoethane (EDB)ND ug/L 08/29/15 06:08 106-93-40.50 0.25 1
Dibromomethane ND ug/L 08/29/15 06:08 74-95-30.50 0.25 1
1,2-Dichlorobenzene ND ug/L 08/29/15 06:08 95-50-10.50 0.25 1
1,3-Dichlorobenzene ND ug/L 08/29/15 06:08 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 08/29/15 06:08 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 08/29/15 06:08 75-71-80.50 0.25 1
1,1-Dichloroethane ND ug/L 08/29/15 06:08 75-34-30.50 0.25 1
1,2-Dichloroethane 0.34J ug/L 08/29/15 06:08 107-06-20.50 0.25 1
1,1-Dichloroethene 11.5 ug/L 08/29/15 06:08 75-35-40.50 0.25 1
cis-1,2-Dichloroethene 5550 ug/L 08/31/15 13:29 156-59-250.0 25.0 100
trans-1,2-Dichloroethene 48.5 ug/L 08/29/15 06:08 156-60-50.50 0.25 1
1,2-Dichloropropane ND ug/L 08/29/15 06:08 78-87-50.50 0.25 1
1,3-Dichloropropane ND ug/L 08/29/15 06:08 142-28-90.50 0.25 1
2,2-Dichloropropane ND ug/L 08/29/15 06:08 594-20-70.50 0.25 1
1,1-Dichloropropene ND ug/L 08/29/15 06:08 563-58-60.50 0.25 1
cis-1,3-Dichloropropene ND ug/L 08/29/15 06:08 10061-01-50.50 0.25 1
trans-1,3-Dichloropropene ND ug/L 08/29/15 06:08 10061-02-60.50 0.25 1
Diisopropyl ether ND ug/L 08/29/15 06:08 108-20-30.50 0.25 1
Ethylbenzene ND ug/L 08/29/15 06:08 100-41-40.50 0.25 1
Hexachloro-1,3-butadiene ND ug/L 08/29/15 06:08 87-68-32.0 1.0 1
Isopropylbenzene (Cumene)ND ug/L 08/29/15 06:08 98-82-80.50 0.25 1
Methylene Chloride ND ug/L 08/29/15 06:08 75-09-22.0 1.0 1
Methyl-tert-butyl ether ND ug/L 08/29/15 06:08 1634-04-40.50 0.25 1
Naphthalene ND ug/L 08/29/15 06:08 91-20-32.0 1.0 1
n-Propylbenzene ND ug/L 08/29/15 06:08 103-65-10.50 0.25 1
Styrene ND ug/L 08/29/15 06:08 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane ND ug/L 08/29/15 06:08 630-20-60.50 0.25 1
1,1,2,2-Tetrachloroethane ND ug/L 08/29/15 06:08 79-34-50.50 0.25 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/25/2015 01:12 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
Sample:MW-9 Lab ID:92265344001 Collected:08/27/15 14:25 Received:08/27/15 16:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene 4460 ug/L 08/31/15 13:29 127-18-450.0 25.0 100
Toluene ND ug/L 08/29/15 06:08 108-88-30.50 0.25 1
1,2,3-Trichlorobenzene ND ug/L 08/29/15 06:08 87-61-62.0 1.0 1
1,2,4-Trichlorobenzene ND ug/L 08/29/15 06:08 120-82-12.0 1.0 1
1,1,1-Trichloroethane ND ug/L 08/29/15 06:08 71-55-60.50 0.25 1
1,1,2-Trichloroethane ND ug/L 08/29/15 06:08 79-00-50.50 0.25 1
Trichloroethene 2880 ug/L 08/31/15 13:29 79-01-650.0 25.0 100
Trichlorofluoromethane ND ug/L 08/29/15 06:08 75-69-41.0 0.50 1
1,2,3-Trichloropropane ND ug/L 08/29/15 06:08 96-18-40.50 0.25 1
1,2,4-Trimethylbenzene ND ug/L 08/29/15 06:08 95-63-60.50 0.25 1
1,3,5-Trimethylbenzene ND ug/L 08/29/15 06:08 108-67-80.50 0.25 1
Vinyl chloride 6.5 ug/L 08/29/15 06:08 75-01-41.0 0.25 1
m&p-Xylene ND ug/L 08/29/15 06:08 179601-23-11.0 0.50 1
o-Xylene ND ug/L 08/29/15 06:08 95-47-60.50 0.25 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %08/29/15 06:08 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %08/29/15 06:08 460-00-470-130 1
Toluene-d8 (S)98 %08/29/15 06:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/25/2015 01:12 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
Sample:MW-10 Lab ID:92265344002 Collected:08/27/15 14:45 Received:08/27/15 16:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 08/30/15 15:39 71-43-20.50 0.25 1
Bromobenzene ND ug/L 08/30/15 15:39 108-86-10.50 0.25 1
Bromochloromethane ND ug/L 08/30/15 15:39 74-97-50.50 0.25 1
Bromodichloromethane ND ug/L 08/30/15 15:39 75-27-40.50 0.25 1
Bromoform ND ug/L 08/30/15 15:39 75-25-20.50 0.25 1
Bromomethane ND ug/L 08/30/15 15:39 74-83-95.0 0.50 1
n-Butylbenzene ND ug/L 08/30/15 15:39 104-51-80.50 0.25 1
sec-Butylbenzene ND ug/L 08/30/15 15:39 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 08/30/15 15:39 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 08/30/15 15:39 56-23-50.50 0.25 1
Chlorobenzene ND ug/L 08/30/15 15:39 108-90-70.50 0.25 1
Chloroethane ND ug/L 08/30/15 15:39 75-00-31.0 0.50 1
Chloroform ND ug/L 08/30/15 15:39 67-66-30.50 0.25 1
Chloromethane ND ug/L 08/30/15 15:39 74-87-31.0 0.50 1
2-Chlorotoluene ND ug/L 08/30/15 15:39 95-49-80.50 0.25 1
4-Chlorotoluene ND ug/L 08/30/15 15:39 106-43-40.50 0.25 1
1,2-Dibromo-3-chloropropane ND ug/L 08/30/15 15:39 96-12-81.0 0.50 1
Dibromochloromethane ND ug/L 08/30/15 15:39 124-48-10.50 0.25 1
1,2-Dibromoethane (EDB)ND ug/L 08/30/15 15:39 106-93-40.50 0.25 1
Dibromomethane ND ug/L 08/30/15 15:39 74-95-30.50 0.25 1
1,2-Dichlorobenzene ND ug/L 08/30/15 15:39 95-50-10.50 0.25 1
1,3-Dichlorobenzene ND ug/L 08/30/15 15:39 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 08/30/15 15:39 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 08/30/15 15:39 75-71-80.50 0.25 1
1,1-Dichloroethane ND ug/L 08/30/15 15:39 75-34-30.50 0.25 1
1,2-Dichloroethane ND ug/L 08/30/15 15:39 107-06-20.50 0.25 1
1,1-Dichloroethene ND ug/L 08/30/15 15:39 75-35-40.50 0.25 1
cis-1,2-Dichloroethene 1.6 ug/L 08/30/15 15:39 156-59-20.50 0.25 1
trans-1,2-Dichloroethene ND ug/L 08/30/15 15:39 156-60-50.50 0.25 1
1,2-Dichloropropane ND ug/L 08/30/15 15:39 78-87-50.50 0.25 1
1,3-Dichloropropane ND ug/L 08/30/15 15:39 142-28-90.50 0.25 1
2,2-Dichloropropane ND ug/L 08/30/15 15:39 594-20-70.50 0.25 1
1,1-Dichloropropene ND ug/L 08/30/15 15:39 563-58-60.50 0.25 1
cis-1,3-Dichloropropene ND ug/L 08/30/15 15:39 10061-01-50.50 0.25 1
trans-1,3-Dichloropropene ND ug/L 08/30/15 15:39 10061-02-60.50 0.25 1
Diisopropyl ether ND ug/L 08/30/15 15:39 108-20-30.50 0.25 1
Ethylbenzene ND ug/L 08/30/15 15:39 100-41-40.50 0.25 1
Hexachloro-1,3-butadiene ND ug/L 08/30/15 15:39 87-68-32.0 1.0 1
Isopropylbenzene (Cumene)ND ug/L 08/30/15 15:39 98-82-80.50 0.25 1
Methylene Chloride ND ug/L 08/30/15 15:39 75-09-22.0 1.0 1
Methyl-tert-butyl ether ND ug/L 08/30/15 15:39 1634-04-40.50 0.25 1
Naphthalene ND ug/L 08/30/15 15:39 91-20-32.0 1.0 1
n-Propylbenzene ND ug/L 08/30/15 15:39 103-65-10.50 0.25 1
Styrene ND ug/L 08/30/15 15:39 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane ND ug/L 08/30/15 15:39 630-20-60.50 0.25 1
1,1,2,2-Tetrachloroethane ND ug/L 08/30/15 15:39 79-34-50.50 0.25 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/25/2015 01:12 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
Sample:MW-10 Lab ID:92265344002 Collected:08/27/15 14:45 Received:08/27/15 16:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene 2.7 ug/L 08/30/15 15:39 127-18-40.50 0.25 1
Toluene ND ug/L 08/30/15 15:39 108-88-30.50 0.25 1
1,2,3-Trichlorobenzene ND ug/L 08/30/15 15:39 87-61-62.0 1.0 1
1,2,4-Trichlorobenzene ND ug/L 08/30/15 15:39 120-82-12.0 1.0 1
1,1,1-Trichloroethane ND ug/L 08/30/15 15:39 71-55-60.50 0.25 1
1,1,2-Trichloroethane ND ug/L 08/30/15 15:39 79-00-50.50 0.25 1
Trichloroethene 3.3 ug/L 08/30/15 15:39 79-01-60.50 0.25 1
Trichlorofluoromethane ND ug/L 08/30/15 15:39 75-69-41.0 0.50 1
1,2,3-Trichloropropane ND ug/L 08/30/15 15:39 96-18-40.50 0.25 1
1,2,4-Trimethylbenzene ND ug/L 08/30/15 15:39 95-63-60.50 0.25 1
1,3,5-Trimethylbenzene ND ug/L 08/30/15 15:39 108-67-80.50 0.25 1
Vinyl chloride ND ug/L 08/30/15 15:39 75-01-41.0 0.25 1
m&p-Xylene ND ug/L 08/30/15 15:39 179601-23-11.0 0.50 1
o-Xylene ND ug/L 08/30/15 15:39 95-47-60.50 0.25 1
Surrogates
1,2-Dichloroethane-d4 (S)108 %08/30/15 15:39 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %08/30/15 15:39 460-00-470-130 1
Toluene-d8 (S)101 %08/30/15 15:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/25/2015 01:12 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/33169
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92265344001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1544250
Associated Lab Samples:92265344001
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 08/29/15 00:52
1,1,1-Trichloroethane ug/L ND 0.50 08/29/15 00:52
1,1,2,2-Tetrachloroethane ug/L ND 0.50 08/29/15 00:52
1,1,2-Trichloroethane ug/L ND 0.50 08/29/15 00:52
1,1-Dichloroethane ug/L ND 0.50 08/29/15 00:52
1,1-Dichloroethene ug/L ND 0.50 08/29/15 00:52
1,1-Dichloropropene ug/L ND 0.50 08/29/15 00:52
1,2,3-Trichlorobenzene ug/L ND 2.0 08/29/15 00:52
1,2,3-Trichloropropane ug/L ND 0.50 08/29/15 00:52
1,2,4-Trichlorobenzene ug/L ND 2.0 08/29/15 00:52
1,2,4-Trimethylbenzene ug/L ND 0.50 08/29/15 00:52
1,2-Dibromo-3-chloropropane ug/L ND 1.0 08/29/15 00:52
1,2-Dibromoethane (EDB)ug/L ND 0.50 08/29/15 00:52
1,2-Dichlorobenzene ug/L ND 0.50 08/29/15 00:52
1,2-Dichloroethane ug/L ND 0.50 08/29/15 00:52
1,2-Dichloropropane ug/L ND 0.50 08/29/15 00:52
1,3,5-Trimethylbenzene ug/L ND 0.50 08/29/15 00:52
1,3-Dichlorobenzene ug/L ND 0.50 08/29/15 00:52
1,3-Dichloropropane ug/L ND 0.50 08/29/15 00:52
1,4-Dichlorobenzene ug/L ND 0.50 08/29/15 00:52
2,2-Dichloropropane ug/L ND 0.50 08/29/15 00:52
2-Chlorotoluene ug/L ND 0.50 08/29/15 00:52
4-Chlorotoluene ug/L ND 0.50 08/29/15 00:52
Benzene ug/L ND 0.50 08/29/15 00:52
Bromobenzene ug/L ND 0.50 08/29/15 00:52
Bromochloromethane ug/L ND 0.50 08/29/15 00:52
Bromodichloromethane ug/L ND 0.50 08/29/15 00:52
Bromoform ug/L ND 0.50 08/29/15 00:52
Bromomethane ug/L ND 5.0 08/29/15 00:52
Carbon tetrachloride ug/L ND 0.50 08/29/15 00:52
Chlorobenzene ug/L ND 0.50 08/29/15 00:52
Chloroethane ug/L ND 1.0 08/29/15 00:52
Chloroform ug/L ND 0.50 08/29/15 00:52
Chloromethane ug/L ND 1.0 08/29/15 00:52
cis-1,2-Dichloroethene ug/L ND 0.50 08/29/15 00:52
cis-1,3-Dichloropropene ug/L ND 0.50 08/29/15 00:52
Dibromochloromethane ug/L ND 0.50 08/29/15 00:52
Dibromomethane ug/L ND 0.50 08/29/15 00:52
Dichlorodifluoromethane ug/L ND 0.50 08/29/15 00:52
Diisopropyl ether ug/L ND 0.50 08/29/15 00:52
Ethylbenzene ug/L ND 0.50 08/29/15 00:52
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/25/2015 01:12 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1544250
Associated Lab Samples:92265344001
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 08/29/15 00:52
Isopropylbenzene (Cumene)ug/L ND 0.50 08/29/15 00:52
m&p-Xylene ug/L ND 1.0 08/29/15 00:52
Methyl-tert-butyl ether ug/L ND 0.50 08/29/15 00:52
Methylene Chloride ug/L 1.9J 2.0 08/29/15 00:52
n-Butylbenzene ug/L ND 0.50 08/29/15 00:52
n-Propylbenzene ug/L ND 0.50 08/29/15 00:52
Naphthalene ug/L ND 2.0 08/29/15 00:52
o-Xylene ug/L ND 0.50 08/29/15 00:52
sec-Butylbenzene ug/L ND 0.50 08/29/15 00:52
Styrene ug/L ND 0.50 08/29/15 00:52
tert-Butylbenzene ug/L ND 0.50 08/29/15 00:52
Tetrachloroethene ug/L ND 0.50 08/29/15 00:52
Toluene ug/L ND 0.50 08/29/15 00:52
trans-1,2-Dichloroethene ug/L ND 0.50 08/29/15 00:52
trans-1,3-Dichloropropene ug/L ND 0.50 08/29/15 00:52
Trichloroethene ug/L ND 0.50 08/29/15 00:52
Trichlorofluoromethane ug/L ND 1.0 08/29/15 00:52
Vinyl chloride ug/L ND 1.0 08/29/15 00:52
1,2-Dichloroethane-d4 (S)%101 70-130 08/29/15 00:52
4-Bromofluorobenzene (S)%98 70-130 08/29/15 00:52
Toluene-d8 (S)%100 70-130 08/29/15 00:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1544251LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.550 101 60-140
1,1,1-Trichloroethane ug/L 49.550 99 60-140
1,1,2,2-Tetrachloroethane ug/L 48.950 98 60-140
1,1,2-Trichloroethane ug/L 49.150 98 60-140
1,1-Dichloroethane ug/L 47.650 95 60-140
1,1-Dichloroethene ug/L 49.050 98 60-140
1,1-Dichloropropene ug/L 51.050 102 60-140
1,2,3-Trichlorobenzene ug/L 53.750 107 60-140
1,2,3-Trichloropropane ug/L 46.350 93 60-140
1,2,4-Trichlorobenzene ug/L 53.250 106 60-140
1,2,4-Trimethylbenzene ug/L 51.350 103 60-140
1,2-Dibromo-3-chloropropane ug/L 54.350 109 60-140
1,2-Dibromoethane (EDB)ug/L 50.950 102 60-140
1,2-Dichlorobenzene ug/L 50.750 101 60-140
1,2-Dichloroethane ug/L 45.750 91 60-140
1,2-Dichloropropane ug/L 48.550 97 60-140
1,3,5-Trimethylbenzene ug/L 50.050 100 60-140
1,3-Dichlorobenzene ug/L 51.350 103 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/25/2015 01:12 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1544251LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 48.950 98 60-140
1,4-Dichlorobenzene ug/L 49.050 98 60-140
2,2-Dichloropropane ug/L 45.250 90 60-140
2-Chlorotoluene ug/L 48.350 97 60-140
4-Chlorotoluene ug/L 49.150 98 60-140
Benzene ug/L 50.950 102 60-140
Bromobenzene ug/L 47.750 95 60-140
Bromochloromethane ug/L 51.750 103 60-140
Bromodichloromethane ug/L 51.950 104 60-140
Bromoform ug/L 51.450 103 60-140
Bromomethane ug/L 51.050 102 60-140
Carbon tetrachloride ug/L 52.150 104 60-140
Chlorobenzene ug/L 48.850 98 60-140
Chloroethane ug/L 44.850 90 60-140
Chloroform ug/L 47.850 96 60-140
Chloromethane ug/L 37.050 74 60-140
cis-1,2-Dichloroethene ug/L 49.250 98 60-140
cis-1,3-Dichloropropene ug/L 50.750 101 60-140
Dibromochloromethane ug/L 51.350 103 60-140
Dibromomethane ug/L 52.550 105 60-140
Dichlorodifluoromethane ug/L 41.550 83 60-140
Diisopropyl ether ug/L 50.050 100 60-140
Ethylbenzene ug/L 47.550 95 60-140
Hexachloro-1,3-butadiene ug/L 59.950 120 60-140
Isopropylbenzene (Cumene)ug/L 52.750 105 60-140
m&p-Xylene ug/L 96.8100 97 60-140
Methyl-tert-butyl ether ug/L 49.250 98 60-140
Methylene Chloride ug/L 49.650 99 60-140
n-Butylbenzene ug/L 50.650 101 60-140
n-Propylbenzene ug/L 48.650 97 60-140
Naphthalene ug/L 56.150 112 60-140
o-Xylene ug/L 50.350 101 60-140
sec-Butylbenzene ug/L 52.250 104 60-140
Styrene ug/L 52.450 105 60-140
tert-Butylbenzene ug/L 43.650 87 60-140
Tetrachloroethene ug/L 47.750 95 60-140
Toluene ug/L 49.050 98 60-140
trans-1,2-Dichloroethene ug/L 50.650 101 60-140
trans-1,3-Dichloropropene ug/L 51.750 103 60-140
Trichloroethene ug/L 47.050 94 60-140
Trichlorofluoromethane ug/L 43.650 87 60-140
Vinyl chloride ug/L 45.250 90 60-140
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/25/2015 01:12 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1544252MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92264538002
1544253
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 105 60-140110 4 3020ND21.1 22.0
1,1,1-Trichloroethane ug/L 20 112 60-140115 3 3020ND22.4 23.0
1,1,2,2-Tetrachloroethane ug/L 20 106 60-140107 1 3020ND21.2 21.4
1,1,2-Trichloroethane ug/L 20 101 60-140103 2 3020ND20.3 20.7
1,1-Dichloroethane ug/L 20 105 60-140107 3 3020ND20.9 21.5
1,1-Dichloroethene ug/L 20 114 60-140119 5 3020ND22.8 23.9
1,1-Dichloropropene ug/L 20 116 60-140120 4 3020ND23.2 24.1
1,2,3-Trichlorobenzene ug/L 20 94 60-140101 7 3020ND18.9 20.2
1,2,3-Trichloropropane ug/L 20 99 60-140102 3 3020ND19.7 20.4
1,2,4-Trichlorobenzene ug/L 20 95 60-140104 9 3020ND19.1 20.8
1,2,4-Trimethylbenzene ug/L 20 105 60-140113 7 3020ND21.1 22.5
1,2-Dibromo-3-
chloropropane ug/L 20 106 60-140118 11 3020ND21.2 23.6
1,2-Dibromoethane (EDB)ug/L 20 109 60-140112 3 3020ND21.8 22.5
1,2-Dichlorobenzene ug/L 20 105 60-140114 8 3020ND21.0 22.7
1,2-Dichloroethane ug/L 20 96 60-140100 4 3020ND19.4 20.2
1,2-Dichloropropane ug/L 20 105 60-140107 2 3020ND21.0 21.5
1,3,5-Trimethylbenzene ug/L 20 106 60-140115 8 3020ND21.3 23.0
1,3-Dichlorobenzene ug/L 20 107 60-140113 6 3020ND21.3 22.6
1,3-Dichloropropane ug/L 20 105 60-140109 4 3020ND20.9 21.7
1,4-Dichlorobenzene ug/L 20 100 60-140109 8 3020ND20.2 21.8
2,2-Dichloropropane ug/L 20 92 60-14094 3 3020ND18.4 18.9
2-Chlorotoluene ug/L 20 103 60-140113 10 3020ND20.5 22.6
4-Chlorotoluene ug/L 20 106 60-140112 6 3020ND21.2 22.5
Benzene ug/L 20 110 60-140112 2 3020ND22.1 22.5
Bromobenzene ug/L 20 102 60-140111 8 3020ND20.5 22.2
Bromochloromethane ug/L 20 111 60-140113 2 3020ND22.3 22.7
Bromodichloromethane ug/L 20 107 60-140108 1 3020ND21.4 21.6
Bromoform ug/L 20 96 60-14097 1 3020ND19.2 19.4
Bromomethane ug/L 20 91 60-14099 9 3020ND18.1 19.8
Carbon tetrachloride ug/L 20 114 60-140117 2 3020ND22.9 23.4
Chlorobenzene ug/L 20 107 60-140110 3 3020ND21.4 21.9
Chloroethane ug/L 20 101 60-140102 1 3020ND20.1 20.4
Chloroform ug/L 20 109 60-140110 1 3020ND21.7 22.0
Chloromethane ug/L 20 93 60-14096 3 3020ND18.8 19.5
cis-1,2-Dichloroethene ug/L 20 116 60-140114 2 3020ND23.2 22.8
cis-1,3-Dichloropropene ug/L 20 100 60-140102 2 3020ND19.9 20.4
Dibromochloromethane ug/L 20 101 60-140101 1 3020ND20.1 20.2
Dibromomethane ug/L 20 107 60-140111 3 3020ND21.5 22.1
Dichlorodifluoromethane ug/L 20 100 60-140101 1 3020ND20.0 20.2
Diisopropyl ether ug/L 20 106 60-140108 1 3020ND21.3 21.5
Ethylbenzene ug/L 20 104 60-140108 4 3020ND20.8 21.5
Hexachloro-1,3-butadiene ug/L 20 116 60-140135 15 3020ND23.2 26.9
Isopropylbenzene (Cumene)ug/L 20 115 60-140118 3 3020ND23.0 23.6
m&p-Xylene ug/L 40 106 60-140109 2 3040ND42.4 43.4
Methyl-tert-butyl ether ug/L 20 104 60-140106 1 3020ND20.9 21.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/25/2015 01:12 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1544252MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92264538002
1544253
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methylene Chloride ug/L 20 103 60-140106 3 3020ND20.6 21.3
n-Butylbenzene ug/L 20 100 60-140106 6 3020ND20.1 21.3
n-Propylbenzene ug/L 20 105 60-140111 5 3020ND21.1 22.2
Naphthalene ug/L 20 98 60-140107 8 3020ND19.6 21.4
o-Xylene ug/L 20 108 60-140110 2 3020ND21.6 22.0
sec-Butylbenzene ug/L 20 110 60-140115 4 3020ND22.1 23.1
Styrene ug/L 20 109 60-140114 5 3020ND21.7 22.8
tert-Butylbenzene ug/L 20 92 60-14099 7 3020ND18.5 19.7
Tetrachloroethene ug/L 20 110 60-140110 0 3020ND21.9 21.9
Toluene ug/L 20 104 60-140109 5 3020ND20.7 21.8
trans-1,2-Dichloroethene ug/L 20 115 60-140118 2 3020ND23.0 23.5
trans-1,3-Dichloropropene ug/L 20 100 60-140104 4 3020ND19.9 20.8
Trichloroethene ug/L 20 105 60-140105 1 3020ND20.9 21.1
Trichlorofluoromethane ug/L 20 104 60-140107 3 3020ND20.7 21.3
Vinyl chloride ug/L 20 107 60-140109 2 3020ND21.4 21.9
1,2-Dichloroethane-d4 (S)%96 70-13095
4-Bromofluorobenzene (S)%102 70-13098
Toluene-d8 (S)%99 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/25/2015 01:12 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/33173
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92265344002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1544680
Associated Lab Samples:92265344002
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 08/30/15 14:16
1,1,1-Trichloroethane ug/L ND 0.50 08/30/15 14:16
1,1,2,2-Tetrachloroethane ug/L ND 0.50 08/30/15 14:16
1,1,2-Trichloroethane ug/L ND 0.50 08/30/15 14:16
1,1-Dichloroethane ug/L ND 0.50 08/30/15 14:16
1,1-Dichloroethene ug/L ND 0.50 08/30/15 14:16
1,1-Dichloropropene ug/L ND 0.50 08/30/15 14:16
1,2,3-Trichlorobenzene ug/L ND 2.0 08/30/15 14:16
1,2,3-Trichloropropane ug/L ND 0.50 08/30/15 14:16
1,2,4-Trichlorobenzene ug/L ND 2.0 08/30/15 14:16
1,2,4-Trimethylbenzene ug/L ND 0.50 08/30/15 14:16
1,2-Dibromo-3-chloropropane ug/L ND 1.0 08/30/15 14:16
1,2-Dibromoethane (EDB)ug/L ND 0.50 08/30/15 14:16
1,2-Dichlorobenzene ug/L ND 0.50 08/30/15 14:16
1,2-Dichloroethane ug/L ND 0.50 08/30/15 14:16
1,2-Dichloropropane ug/L ND 0.50 08/30/15 14:16
1,3,5-Trimethylbenzene ug/L ND 0.50 08/30/15 14:16
1,3-Dichlorobenzene ug/L ND 0.50 08/30/15 14:16
1,3-Dichloropropane ug/L ND 0.50 08/30/15 14:16
1,4-Dichlorobenzene ug/L ND 0.50 08/30/15 14:16
2,2-Dichloropropane ug/L ND 0.50 08/30/15 14:16
2-Chlorotoluene ug/L ND 0.50 08/30/15 14:16
4-Chlorotoluene ug/L ND 0.50 08/30/15 14:16
Benzene ug/L ND 0.50 08/30/15 14:16
Bromobenzene ug/L ND 0.50 08/30/15 14:16
Bromochloromethane ug/L ND 0.50 08/30/15 14:16
Bromodichloromethane ug/L ND 0.50 08/30/15 14:16
Bromoform ug/L ND 0.50 08/30/15 14:16
Bromomethane ug/L ND 5.0 08/30/15 14:16
Carbon tetrachloride ug/L ND 0.50 08/30/15 14:16
Chlorobenzene ug/L ND 0.50 08/30/15 14:16
Chloroethane ug/L ND 1.0 08/30/15 14:16
Chloroform ug/L ND 0.50 08/30/15 14:16
Chloromethane ug/L ND 1.0 08/30/15 14:16
cis-1,2-Dichloroethene ug/L ND 0.50 08/30/15 14:16
cis-1,3-Dichloropropene ug/L ND 0.50 08/30/15 14:16
Dibromochloromethane ug/L ND 0.50 08/30/15 14:16
Dibromomethane ug/L ND 0.50 08/30/15 14:16
Dichlorodifluoromethane ug/L ND 0.50 08/30/15 14:16
Diisopropyl ether ug/L ND 0.50 08/30/15 14:16
Ethylbenzene ug/L ND 0.50 08/30/15 14:16
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/25/2015 01:12 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1544680
Associated Lab Samples:92265344002
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 08/30/15 14:16
Isopropylbenzene (Cumene)ug/L ND 0.50 08/30/15 14:16
m&p-Xylene ug/L ND 1.0 08/30/15 14:16
Methyl-tert-butyl ether ug/L ND 0.50 08/30/15 14:16
Methylene Chloride ug/L ND 2.0 08/30/15 14:16
n-Butylbenzene ug/L ND 0.50 08/30/15 14:16
n-Propylbenzene ug/L ND 0.50 08/30/15 14:16
Naphthalene ug/L ND 2.0 08/30/15 14:16
o-Xylene ug/L ND 0.50 08/30/15 14:16
sec-Butylbenzene ug/L ND 0.50 08/30/15 14:16
Styrene ug/L ND 0.50 08/30/15 14:16
tert-Butylbenzene ug/L ND 0.50 08/30/15 14:16
Tetrachloroethene ug/L ND 0.50 08/30/15 14:16
Toluene ug/L ND 0.50 08/30/15 14:16
trans-1,2-Dichloroethene ug/L ND 0.50 08/30/15 14:16
trans-1,3-Dichloropropene ug/L ND 0.50 08/30/15 14:16
Trichloroethene ug/L ND 0.50 08/30/15 14:16
Trichlorofluoromethane ug/L ND 1.0 08/30/15 14:16
Vinyl chloride ug/L ND 1.0 08/30/15 14:16
1,2-Dichloroethane-d4 (S)%98 70-130 08/30/15 14:16
4-Bromofluorobenzene (S)%95 70-130 08/30/15 14:16
Toluene-d8 (S)%102 70-130 08/30/15 14:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1544681LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.950 110 60-140
1,1,1-Trichloroethane ug/L 52.350 105 60-140
1,1,2,2-Tetrachloroethane ug/L 53.950 108 60-140
1,1,2-Trichloroethane ug/L 50.750 101 60-140
1,1-Dichloroethane ug/L 48.050 96 60-140
1,1-Dichloroethene ug/L 51.350 103 60-140
1,1-Dichloropropene ug/L 52.950 106 60-140
1,2,3-Trichlorobenzene ug/L 56.950 114 60-140
1,2,3-Trichloropropane ug/L 50.350 101 60-140
1,2,4-Trichlorobenzene ug/L 57.750 115 60-140
1,2,4-Trimethylbenzene ug/L 54.650 109 60-140
1,2-Dibromo-3-chloropropane ug/L 60.650 121 60-140
1,2-Dibromoethane (EDB)ug/L 53.550 107 60-140
1,2-Dichlorobenzene ug/L 55.150 110 60-140
1,2-Dichloroethane ug/L 46.450 93 60-140
1,2-Dichloropropane ug/L 48.150 96 60-140
1,3,5-Trimethylbenzene ug/L 54.250 108 60-140
1,3-Dichlorobenzene ug/L 55.250 110 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/25/2015 01:12 PM
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Page 15 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1544681LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 50.750 101 60-140
1,4-Dichlorobenzene ug/L 51.750 103 60-140
2,2-Dichloropropane ug/L 53.350 107 60-140
2-Chlorotoluene ug/L 52.250 104 60-140
4-Chlorotoluene ug/L 52.750 105 60-140
Benzene ug/L 51.450 103 60-140
Bromobenzene ug/L 51.650 103 60-140
Bromochloromethane ug/L 54.250 108 60-140
Bromodichloromethane ug/L 55.450 111 60-140
Bromoform ug/L 59.650 119 60-140
Bromomethane ug/L 56.850 114 60-140
Carbon tetrachloride ug/L 56.050 112 60-140
Chlorobenzene ug/L 51.450 103 60-140
Chloroethane ug/L 48.550 97 60-140
Chloroform ug/L 51.150 102 60-140
Chloromethane ug/L 46.850 94 60-140
cis-1,2-Dichloroethene ug/L 49.950 100 60-140
cis-1,3-Dichloropropene ug/L 54.250 108 60-140
Dibromochloromethane ug/L 56.750 113 60-140
Dibromomethane ug/L 52.750 105 60-140
Dichlorodifluoromethane ug/L 51.750 103 60-140
Diisopropyl ether ug/L 48.150 96 60-140
Ethylbenzene ug/L 50.550 101 60-140
Hexachloro-1,3-butadiene ug/L 62.750 125 60-140
Isopropylbenzene (Cumene)ug/L 57.050 114 60-140
m&p-Xylene ug/L 103100 103 60-140
Methyl-tert-butyl ether ug/L 49.550 99 60-140
Methylene Chloride ug/L 47.150 94 60-140
n-Butylbenzene ug/L 56.450 113 60-140
n-Propylbenzene ug/L 52.450 105 60-140
Naphthalene ug/L 59.750 119 60-140
o-Xylene ug/L 52.750 105 60-140
sec-Butylbenzene ug/L 56.650 113 60-140
Styrene ug/L 55.750 111 60-140
tert-Butylbenzene ug/L 46.450 93 60-140
Tetrachloroethene ug/L 50.450 101 60-140
Toluene ug/L 50.750 101 60-140
trans-1,2-Dichloroethene ug/L 52.350 105 60-140
trans-1,3-Dichloropropene ug/L 55.150 110 60-140
Trichloroethene ug/L 47.950 96 60-140
Trichlorofluoromethane ug/L 48.450 97 60-140
Vinyl chloride ug/L 50.150 100 60-140
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/25/2015 01:12 PM
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Huntersville, NC 28078
[phone]
Page 16 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1544682MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92265352006
1544683
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 112 60-140116 4 3020ND22.3 23.2
1,1,1-Trichloroethane ug/L 20 122 60-140121 1 3020ND24.5 24.2
1,1,2,2-Tetrachloroethane ug/L 20 112 60-140115 3 3020ND22.4 23.0
1,1,2-Trichloroethane ug/L 20 109 60-140108 1 3020ND21.8 21.7
1,1-Dichloroethane ug/L 20 112 60-140111 0 3020ND22.4 22.3
1,1-Dichloroethene ug/L 20 121 60-140124 2 3020ND24.2 24.8
1,1-Dichloropropene ug/L 20 125 60-140126 0 3020ND25.1 25.2
1,2,3-Trichlorobenzene ug/L 20 115 60-140118 3 3020ND23.0 23.7
1,2,3-Trichloropropane ug/L 20 105 60-140108 3 3020ND20.9 21.6
1,2,4-Trichlorobenzene ug/L 20 116 60-140115 1 3020ND23.3 23.1
1,2,4-Trimethylbenzene ug/L 20 118 60-140116 2 3020ND23.5 23.1
1,2-Dibromo-3-
chloropropane ug/L 20 117 60-140126 7 3020ND23.3 25.1
1,2-Dibromoethane (EDB)ug/L 20 112 60-140113 1 3020ND22.5 22.7
1,2-Dichlorobenzene ug/L 20 115 60-140116 1 3020ND23.0 23.2
1,2-Dichloroethane ug/L 20 105 60-140107 3 3020ND20.9 21.4
1,2-Dichloropropane ug/L 20 108 60-140106 1 3020ND21.5 21.3
1,3,5-Trimethylbenzene ug/L 20 119 60-140114 4 3020ND23.7 22.9
1,3-Dichlorobenzene ug/L 20 117 60-140114 3 3020ND23.5 22.8
1,3-Dichloropropane ug/L 20 109 60-140109 1 3020ND21.9 21.7
1,4-Dichlorobenzene ug/L 20 110 60-140112 2 3020ND22.0 22.4
2,2-Dichloropropane ug/L 20 109 60-140114 4 3020ND21.7 22.7
2-Chlorotoluene ug/L 20 114 60-140111 3 3020ND22.8 22.1
4-Chlorotoluene ug/L 20 116 60-140111 4 3020ND23.2 22.3
Benzene ug/L 20 116 60-140114 1 3020ND23.1 22.8
Bromobenzene ug/L 20 112 60-140107 4 3020ND22.4 21.4
Bromochloromethane ug/L 20 122 60-140121 1 3020ND24.5 24.2
Bromodichloromethane ug/L 20 116 60-140114 2 3020ND23.3 22.9
Bromoform ug/L 20 105 60-140111 6 3020ND20.9 22.1
Bromomethane ug/L 20 74 60-14085 15 3020ND14.7 17.0
Carbon tetrachloride ug/L 20 120 60-140120 0 3020ND24.0 24.0
Chlorobenzene ug/L 20 113 60-140111 2 3020ND22.6 22.3
Chloroethane ug/L 20 105 60-140115 9 3020ND21.0 23.0
Chloroform ug/L 20 113 60-140115 2 3020ND22.5 23.0
Chloromethane ug/L 20 99 60-140108 8 3020ND19.9 21.6
cis-1,2-Dichloroethene ug/L 20 115 60-140115 0 3020ND23.0 23.0
cis-1,3-Dichloropropene ug/L 20 106 60-140109 2 3020ND21.3 21.8
Dibromochloromethane ug/L 20 110 60-140111 1 3020ND22.0 22.2
Dibromomethane ug/L 20 110 60-140111 1 3020ND22.1 22.3
Dichlorodifluoromethane ug/L 20 125 60-140124 0 3020ND24.9 24.9
Diisopropyl ether ug/L 20 108 60-140110 2 3020ND21.6 22.0
Ethylbenzene ug/L 20 111 60-140111 0 3020ND22.2 22.1
Hexachloro-1,3-butadiene ug/L 20 135 60-140137 2 3020ND27.1 27.5
Isopropylbenzene (Cumene)ug/L 20 124 60-140124 0 3020ND24.7 24.8
m&p-Xylene ug/L 40 113 60-140112 2 3040ND45.3 44.6
Methyl-tert-butyl ether ug/L 20 108 60-140111 3 3020ND21.7 22.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/25/2015 01:12 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1544682MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92265352006
1544683
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methylene Chloride ug/L 20 106 60-140106 1 3020ND21.1 21.3
n-Butylbenzene ug/L 20 117 60-140117 0 3020ND23.4 23.4
n-Propylbenzene ug/L 20 117 60-140114 2 3020ND23.4 22.8
Naphthalene ug/L 20 123 60-140122 1 3020ND24.6 24.3
o-Xylene ug/L 20 114 60-140113 1 3020ND22.8 22.6
sec-Butylbenzene ug/L 20 123 60-140121 2 3020ND24.7 24.2
Styrene ug/L 20 118 60-140117 0 3020ND23.6 23.5
tert-Butylbenzene ug/L 20 99 60-14099 0 3020ND19.9 19.9
Tetrachloroethene ug/L 20 111 60-140110 1 3020ND22.2 22.0
Toluene ug/L 20 111 60-140110 1 3020ND22.2 22.0
trans-1,2-Dichloroethene ug/L 20 119 60-140121 2 3020ND23.9 24.3
trans-1,3-Dichloropropene ug/L 20 109 60-140111 2 3020ND21.7 22.2
Trichloroethene ug/L 20 109 60-140107 2 3020ND21.8 21.4
Trichlorofluoromethane ug/L 20 115 60-140114 1 3020ND23.0 22.8
Vinyl chloride ug/L 20 117 60-140119 1 3020ND23.5 23.7
1,2-Dichloroethane-d4 (S)%99 70-130100
4-Bromofluorobenzene (S)%100 70-130101
Toluene-d8 (S)%100 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/25/2015 01:12 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 22
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/25/2015 01:12 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 22
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92265344
Atando Brownfields 71157718
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92265344001 MSV/33169MW-9 SM 6200B
92265344002 MSV/33173MW-10 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/25/2015 01:12 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 22
Page 21 of 22
Page 22 of 22
#=CL#
October 16, 2015
LIMS USE: FR - CARLO ZANON
LIMS OBJECT ID: 92271206
92271206
Project:
Pace Project No.:
RE:
Carlo Zanon
Terracon
2020 Starita Rd
Suite E
,
SUNBELT TURRENT 71157718
Dear Carlo Zanon:
Enclosed are the analytical results for sample(s) received by the laboratory on October 09, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 47
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Sample:MW-4 Lab ID:92271206001 Collected:10/08/15 13:30 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 10/15/15 04:34 67-64-125.0 1
Benzene ND ug/L 10/15/15 04:34 71-43-21.0 1
Bromobenzene ND ug/L 10/15/15 04:34 108-86-11.0 1
Bromochloromethane ND ug/L 10/15/15 04:34 74-97-51.0 1
Bromodichloromethane ND ug/L 10/15/15 04:34 75-27-41.0 1
Bromoform ND ug/L 10/15/15 04:34 75-25-21.0 1
Bromomethane ND ug/L 10/15/15 04:34 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/15/15 04:34 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/15/15 04:34 56-23-51.0 1
Chlorobenzene ND ug/L 10/15/15 04:34 108-90-71.0 1
Chloroethane ND ug/L 10/15/15 04:34 75-00-31.0 1
Chloroform ND ug/L 10/15/15 04:34 67-66-31.0 1
Chloromethane ND ug/L 10/15/15 04:34 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/15/15 04:34 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/15/15 04:34 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/15/15 04:34 96-12-82.0 1
Dibromochloromethane ND ug/L 10/15/15 04:34 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/15/15 04:34 106-93-41.0 1
Dibromomethane ND ug/L 10/15/15 04:34 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/15/15 04:34 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/15/15 04:34 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/15/15 04:34 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/15/15 04:34 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/15/15 04:34 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/15/15 04:34 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/15/15 04:34 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/15/15 04:34 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/15/15 04:34 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/15/15 04:34 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/15/15 04:34 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/15/15 04:34 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/15/15 04:34 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/15/15 04:34 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/15/15 04:34 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/15/15 04:34 108-20-31.0 1
Ethylbenzene ND ug/L 10/15/15 04:34 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/15/15 04:34 87-68-31.0 1
2-Hexanone ND ug/L 10/15/15 04:34 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/15/15 04:34 99-87-61.0 1
Methylene Chloride ND ug/L 10/15/15 04:34 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/15/15 04:34 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/15/15 04:34 1634-04-41.0 1
Naphthalene ND ug/L 10/15/15 04:34 91-20-31.0 1
Styrene ND ug/L 10/15/15 04:34 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/15/15 04:34 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/15/15 04:34 79-34-51.0 1
Tetrachloroethene ND ug/L 10/15/15 04:34 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 3 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Sample:MW-4 Lab ID:92271206001 Collected:10/08/15 13:30 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Toluene ND ug/L 10/15/15 04:34 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/15/15 04:34 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/15/15 04:34 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/15/15 04:34 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/15/15 04:34 79-00-51.0 1
Trichloroethene ND ug/L 10/15/15 04:34 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/15/15 04:34 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/15/15 04:34 96-18-41.0 1
Vinyl acetate ND ug/L 10/15/15 04:34 108-05-42.0 1
Vinyl chloride ND ug/L 10/15/15 04:34 75-01-41.0 1
Xylene (Total)ND ug/L 10/15/15 04:34 1330-20-72.0 1
m&p-Xylene ND ug/L 10/15/15 04:34 179601-23-12.0 1
o-Xylene ND ug/L 10/15/15 04:34 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %10/15/15 04:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)112 %10/15/15 04:34 17060-07-070-130 1
Toluene-d8 (S)101 %10/15/15 04:34 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/15 14:45 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)109 %10/12/15 14:45 17060-07-050-150 1
Toluene-d8 (S)125 %10/12/15 14:45 2037-26-550-150 1
Sample:MW-2 Lab ID:92271206002 Collected:10/08/15 14:35 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 10/15/15 04:51 67-64-125.0 1
Benzene 58.2 ug/L 10/15/15 04:51 71-43-21.0 1
Bromobenzene ND ug/L 10/15/15 04:51 108-86-11.0 1
Bromochloromethane ND ug/L 10/15/15 04:51 74-97-51.0 1
Bromodichloromethane ND ug/L 10/15/15 04:51 75-27-41.0 1
Bromoform ND ug/L 10/15/15 04:51 75-25-21.0 1
Bromomethane ND ug/L 10/15/15 04:51 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/15/15 04:51 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/15/15 04:51 56-23-51.0 1
Chlorobenzene ND ug/L 10/15/15 04:51 108-90-71.0 1
Chloroethane ND ug/L 10/15/15 04:51 75-00-31.0 1
Chloroform ND ug/L 10/15/15 04:51 67-66-31.0 1
Chloromethane ND ug/L 10/15/15 04:51 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/15/15 04:51 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/15/15 04:51 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/15/15 04:51 96-12-82.0 1
Dibromochloromethane ND ug/L 10/15/15 04:51 124-48-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
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Huntersville, NC 28078
[phone]
Page 4 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Sample:MW-2 Lab ID:92271206002 Collected:10/08/15 14:35 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 10/15/15 04:51 106-93-41.0 1
Dibromomethane ND ug/L 10/15/15 04:51 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/15/15 04:51 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/15/15 04:51 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/15/15 04:51 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/15/15 04:51 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/15/15 04:51 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/15/15 04:51 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/15/15 04:51 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/15/15 04:51 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/15/15 04:51 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/15/15 04:51 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/15/15 04:51 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/15/15 04:51 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/15/15 04:51 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/15/15 04:51 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/15/15 04:51 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/15/15 04:51 108-20-31.0 1
Ethylbenzene 4.5 ug/L 10/15/15 04:51 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/15/15 04:51 87-68-31.0 1
2-Hexanone ND ug/L 10/15/15 04:51 591-78-65.0 1
p-Isopropyltoluene 3.6 ug/L 10/15/15 04:51 99-87-61.0 1
Methylene Chloride ND ug/L 10/15/15 04:51 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/15/15 04:51 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/15/15 04:51 1634-04-41.0 1
Naphthalene 87.9 ug/L 10/15/15 04:51 91-20-31.0 1
Styrene ND ug/L 10/15/15 04:51 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/15/15 04:51 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/15/15 04:51 79-34-51.0 1
Tetrachloroethene ND ug/L 10/15/15 04:51 127-18-41.0 1
Toluene ND ug/L 10/15/15 04:51 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/15/15 04:51 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/15/15 04:51 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/15/15 04:51 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/15/15 04:51 79-00-51.0 1
Trichloroethene ND ug/L 10/15/15 04:51 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/15/15 04:51 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/15/15 04:51 96-18-41.0 1
Vinyl acetate ND ug/L 10/15/15 04:51 108-05-42.0 1
Vinyl chloride ND ug/L 10/15/15 04:51 75-01-41.0 1
Xylene (Total)3.0 ug/L 10/15/15 04:51 1330-20-72.0 1
m&p-Xylene ND ug/L 10/15/15 04:51 179601-23-12.0 1
o-Xylene 3.0 ug/L 10/15/15 04:51 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)105 %10/15/15 04:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %10/15/15 04:51 17060-07-070-130 1
Toluene-d8 (S)100 %10/15/15 04:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Sample:MW-2 Lab ID:92271206002 Collected:10/08/15 14:35 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/15 15:05 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)111 %10/12/15 15:05 17060-07-050-150 1
Toluene-d8 (S)124 %10/12/15 15:05 2037-26-550-150 1
Sample:MW-3 Lab ID:92271206003 Collected:10/08/15 15:55 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 10/15/15 05:09 67-64-125.0 1
Benzene 1.6 ug/L 10/15/15 05:09 71-43-21.0 1
Bromobenzene ND ug/L 10/15/15 05:09 108-86-11.0 1
Bromochloromethane ND ug/L 10/15/15 05:09 74-97-51.0 1
Bromodichloromethane ND ug/L 10/15/15 05:09 75-27-41.0 1
Bromoform ND ug/L 10/15/15 05:09 75-25-21.0 1
Bromomethane ND ug/L 10/15/15 05:09 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/15/15 05:09 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/15/15 05:09 56-23-51.0 1
Chlorobenzene ND ug/L 10/15/15 05:09 108-90-71.0 1
Chloroethane ND ug/L 10/15/15 05:09 75-00-31.0 1
Chloroform ND ug/L 10/15/15 05:09 67-66-31.0 1
Chloromethane ND ug/L 10/15/15 05:09 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/15/15 05:09 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/15/15 05:09 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/15/15 05:09 96-12-82.0 1
Dibromochloromethane ND ug/L 10/15/15 05:09 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/15/15 05:09 106-93-41.0 1
Dibromomethane ND ug/L 10/15/15 05:09 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/15/15 05:09 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/15/15 05:09 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/15/15 05:09 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/15/15 05:09 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/15/15 05:09 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/15/15 05:09 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/15/15 05:09 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/15/15 05:09 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/15/15 05:09 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/15/15 05:09 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/15/15 05:09 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/15/15 05:09 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/15/15 05:09 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/15/15 05:09 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/15/15 05:09 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/15/15 05:09 108-20-31.0 1
Ethylbenzene ND ug/L 10/15/15 05:09 100-41-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Sample:MW-3 Lab ID:92271206003 Collected:10/08/15 15:55 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Hexachloro-1,3-butadiene ND ug/L 10/15/15 05:09 87-68-31.0 1
2-Hexanone ND ug/L 10/15/15 05:09 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/15/15 05:09 99-87-61.0 1
Methylene Chloride ND ug/L 10/15/15 05:09 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/15/15 05:09 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/15/15 05:09 1634-04-41.0 1
Naphthalene 4.0 ug/L 10/15/15 05:09 91-20-31.0 1
Styrene ND ug/L 10/15/15 05:09 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/15/15 05:09 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/15/15 05:09 79-34-51.0 1
Tetrachloroethene ND ug/L 10/15/15 05:09 127-18-41.0 1
Toluene ND ug/L 10/15/15 05:09 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/15/15 05:09 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/15/15 05:09 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/15/15 05:09 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/15/15 05:09 79-00-51.0 1
Trichloroethene ND ug/L 10/15/15 05:09 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/15/15 05:09 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/15/15 05:09 96-18-41.0 1
Vinyl acetate ND ug/L 10/15/15 05:09 108-05-42.0 1
Vinyl chloride ND ug/L 10/15/15 05:09 75-01-41.0 1
Xylene (Total)ND ug/L 10/15/15 05:09 1330-20-72.0 1
m&p-Xylene ND ug/L 10/15/15 05:09 179601-23-12.0 1
o-Xylene ND ug/L 10/15/15 05:09 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %10/15/15 05:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %10/15/15 05:09 17060-07-070-130 1
Toluene-d8 (S)100 %10/15/15 05:09 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/15 15:26 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %10/12/15 15:26 17060-07-050-150 1
Toluene-d8 (S)123 %10/12/15 15:26 2037-26-550-150 1
Sample:MW-5 Lab ID:92271206004 Collected:10/08/15 10:35 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 10/14/15 08:44 67-64-125010
Benzene ND ug/L 10/14/15 08:44 71-43-210.0 10
Bromobenzene ND ug/L 10/14/15 08:44 108-86-110.0 10
Bromochloromethane ND ug/L 10/14/15 08:44 74-97-510.0 10
Bromodichloromethane ND ug/L 10/14/15 08:44 75-27-410.0 10
Bromoform ND ug/L 10/14/15 08:44 75-25-210.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Sample:MW-5 Lab ID:92271206004 Collected:10/08/15 10:35 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Bromomethane ND ug/L 10/14/15 08:44 74-83-920.0 10
2-Butanone (MEK)ND ug/L 10/14/15 08:44 78-93-350.0 10
Carbon tetrachloride ND ug/L 10/14/15 08:44 56-23-510.0 10
Chlorobenzene ND ug/L 10/14/15 08:44 108-90-710.0 10
Chloroethane ND ug/L 10/14/15 08:44 75-00-310.0 10
Chloroform ND ug/L 10/14/15 08:44 67-66-310.0 10
Chloromethane ND ug/L 10/14/15 08:44 74-87-310.0 10
2-Chlorotoluene ND ug/L 10/14/15 08:44 95-49-810.0 10
4-Chlorotoluene ND ug/L 10/14/15 08:44 106-43-410.0 10
1,2-Dibromo-3-chloropropane ND ug/L 10/14/15 08:44 96-12-820.0 10
Dibromochloromethane ND ug/L 10/14/15 08:44 124-48-110.0 10
1,2-Dibromoethane (EDB)ND ug/L 10/14/15 08:44 106-93-410.0 10
Dibromomethane ND ug/L 10/14/15 08:44 74-95-310.0 10
1,2-Dichlorobenzene ND ug/L 10/14/15 08:44 95-50-110.0 10
1,3-Dichlorobenzene ND ug/L 10/14/15 08:44 541-73-110.0 10
1,4-Dichlorobenzene ND ug/L 10/14/15 08:44 106-46-710.0 10
Dichlorodifluoromethane ND ug/L 10/14/15 08:44 75-71-810.0 10
1,1-Dichloroethane ND ug/L 10/14/15 08:44 75-34-310.0 10
1,2-Dichloroethane ND ug/L 10/14/15 08:44 107-06-210.0 10
1,1-Dichloroethene ND ug/L 10/14/15 08:44 75-35-410.0 10
cis-1,2-Dichloroethene 1000 ug/L 10/14/15 08:44 156-59-210.0 10
trans-1,2-Dichloroethene 12.2 ug/L 10/14/15 08:44 156-60-510.0 10
1,2-Dichloropropane ND ug/L 10/14/15 08:44 78-87-510.0 10
1,3-Dichloropropane ND ug/L 10/14/15 08:44 142-28-910.0 10
2,2-Dichloropropane ND ug/L 10/14/15 08:44 594-20-710.0 10
1,1-Dichloropropene ND ug/L 10/14/15 08:44 563-58-610.0 10
cis-1,3-Dichloropropene ND ug/L 10/14/15 08:44 10061-01-510.0 10
trans-1,3-Dichloropropene ND ug/L 10/14/15 08:44 10061-02-610.0 10
Diisopropyl ether ND ug/L 10/14/15 08:44 108-20-310.0 10
Ethylbenzene ND ug/L 10/14/15 08:44 100-41-410.0 10
Hexachloro-1,3-butadiene ND ug/L 10/14/15 08:44 87-68-310.0 10
2-Hexanone ND ug/L 10/14/15 08:44 591-78-650.0 10
p-Isopropyltoluene ND ug/L 10/14/15 08:44 99-87-610.0 10
Methylene Chloride ND ug/L 10/14/15 08:44 75-09-220.0 10
4-Methyl-2-pentanone (MIBK)ND ug/L 10/14/15 08:44 108-10-150.0 10
Methyl-tert-butyl ether ND ug/L 10/14/15 08:44 1634-04-410.0 10
Naphthalene ND ug/L 10/14/15 08:44 91-20-310.0 10
Styrene ND ug/L 10/14/15 08:44 100-42-510.0 10
1,1,1,2-Tetrachloroethane ND ug/L 10/14/15 08:44 630-20-610.0 10
1,1,2,2-Tetrachloroethane ND ug/L 10/14/15 08:44 79-34-510.0 10
Tetrachloroethene 2790 ug/L 10/14/15 21:46 127-18-425.0 25
Toluene ND ug/L 10/14/15 08:44 108-88-310.0 10
1,2,3-Trichlorobenzene ND ug/L 10/14/15 08:44 87-61-610.0 10
1,2,4-Trichlorobenzene ND ug/L 10/14/15 08:44 120-82-110.0 10
1,1,1-Trichloroethane ND ug/L 10/14/15 08:44 71-55-610.0 10
1,1,2-Trichloroethane ND ug/L 10/14/15 08:44 79-00-510.0 10
Trichloroethene 1870 ug/L 10/14/15 08:44 79-01-610.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Sample:MW-5 Lab ID:92271206004 Collected:10/08/15 10:35 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Trichlorofluoromethane ND ug/L 10/14/15 08:44 75-69-410.0 10
1,2,3-Trichloropropane ND ug/L 10/14/15 08:44 96-18-410.0 10
Vinyl acetate ND ug/L 10/14/15 08:44 108-05-420.0 10
Vinyl chloride 41.3 ug/L 10/14/15 08:44 75-01-410.0 10
Xylene (Total)ND ug/L 10/14/15 08:44 1330-20-720.0 10
m&p-Xylene ND ug/L 10/14/15 08:44 179601-23-120.0 10
o-Xylene ND ug/L 10/14/15 08:44 95-47-610.0 10
Surrogates
4-Bromofluorobenzene (S)104 %10/14/15 08:44 460-00-470-130 10
1,2-Dichloroethane-d4 (S)105 %10/14/15 08:44 17060-07-070-130 10
Toluene-d8 (S)97 %10/14/15 08:44 2037-26-570-130 10
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/15 15:46 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %10/12/15 15:46 17060-07-050-150 1
Toluene-d8 (S)125 %10/12/15 15:46 2037-26-550-150 1
Sample:MW-6 Lab ID:92271206005 Collected:10/08/15 16:20 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 10/14/15 07:36 67-64-125.0 1
Benzene ND ug/L 10/14/15 07:36 71-43-21.0 1
Bromobenzene ND ug/L 10/14/15 07:36 108-86-11.0 1
Bromochloromethane ND ug/L 10/14/15 07:36 74-97-51.0 1
Bromodichloromethane ND ug/L 10/14/15 07:36 75-27-41.0 1
Bromoform ND ug/L 10/14/15 07:36 75-25-21.0 1
Bromomethane ND ug/L 10/14/15 07:36 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/14/15 07:36 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/14/15 07:36 56-23-51.0 1
Chlorobenzene ND ug/L 10/14/15 07:36 108-90-71.0 1
Chloroethane ND ug/L 10/14/15 07:36 75-00-31.0 1
Chloroform 7.4 ug/L 10/14/15 07:36 67-66-31.0 1
Chloromethane ND ug/L 10/14/15 07:36 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/14/15 07:36 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/14/15 07:36 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/14/15 07:36 96-12-82.0 1
Dibromochloromethane ND ug/L 10/14/15 07:36 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/14/15 07:36 106-93-41.0 1
Dibromomethane ND ug/L 10/14/15 07:36 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/14/15 07:36 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/14/15 07:36 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/14/15 07:36 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/14/15 07:36 75-71-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Sample:MW-6 Lab ID:92271206005 Collected:10/08/15 16:20 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,1-Dichloroethane ND ug/L 10/14/15 07:36 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/14/15 07:36 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/14/15 07:36 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/14/15 07:36 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/14/15 07:36 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/14/15 07:36 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/14/15 07:36 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/14/15 07:36 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/14/15 07:36 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/14/15 07:36 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/14/15 07:36 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/14/15 07:36 108-20-31.0 1
Ethylbenzene ND ug/L 10/14/15 07:36 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/14/15 07:36 87-68-31.0 1
2-Hexanone ND ug/L 10/14/15 07:36 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/14/15 07:36 99-87-61.0 1
Methylene Chloride ND ug/L 10/14/15 07:36 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/14/15 07:36 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/14/15 07:36 1634-04-41.0 1
Naphthalene ND ug/L 10/14/15 07:36 91-20-31.0 1
Styrene ND ug/L 10/14/15 07:36 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/14/15 07:36 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/14/15 07:36 79-34-51.0 1
Tetrachloroethene ND ug/L 10/14/15 07:36 127-18-41.0 1
Toluene ND ug/L 10/14/15 07:36 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/14/15 07:36 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/14/15 07:36 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/14/15 07:36 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/14/15 07:36 79-00-51.0 1
Trichloroethene ND ug/L 10/14/15 07:36 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/14/15 07:36 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/14/15 07:36 96-18-41.0 1
Vinyl acetate ND ug/L 10/14/15 07:36 108-05-42.0 1
Vinyl chloride ND ug/L 10/14/15 07:36 75-01-41.0 1
Xylene (Total)ND ug/L 10/14/15 07:36 1330-20-72.0 1
m&p-Xylene ND ug/L 10/14/15 07:36 179601-23-12.0 1
o-Xylene ND ug/L 10/14/15 07:36 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %10/14/15 07:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %10/14/15 07:36 17060-07-070-130 1
Toluene-d8 (S)100 %10/14/15 07:36 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/15 16:06 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %10/12/15 16:06 17060-07-050-150 1
Toluene-d8 (S)125 %10/12/15 16:06 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Sample:MW-7 Lab ID:92271206006 Collected:10/08/15 11:05 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 10/14/15 07:53 67-64-125.0 1
Benzene ND ug/L 10/14/15 07:53 71-43-21.0 1
Bromobenzene ND ug/L 10/14/15 07:53 108-86-11.0 1
Bromochloromethane ND ug/L 10/14/15 07:53 74-97-51.0 1
Bromodichloromethane ND ug/L 10/14/15 07:53 75-27-41.0 1
Bromoform ND ug/L 10/14/15 07:53 75-25-21.0 1
Bromomethane ND ug/L 10/14/15 07:53 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/14/15 07:53 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/14/15 07:53 56-23-51.0 1
Chlorobenzene ND ug/L 10/14/15 07:53 108-90-71.0 1
Chloroethane ND ug/L 10/14/15 07:53 75-00-31.0 1
Chloroform ND ug/L 10/14/15 07:53 67-66-31.0 1
Chloromethane ND ug/L 10/14/15 07:53 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/14/15 07:53 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/14/15 07:53 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/14/15 07:53 96-12-82.0 1
Dibromochloromethane ND ug/L 10/14/15 07:53 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/14/15 07:53 106-93-41.0 1
Dibromomethane ND ug/L 10/14/15 07:53 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/14/15 07:53 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/14/15 07:53 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/14/15 07:53 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/14/15 07:53 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/14/15 07:53 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/14/15 07:53 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/14/15 07:53 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/14/15 07:53 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/14/15 07:53 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/14/15 07:53 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/14/15 07:53 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/14/15 07:53 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/14/15 07:53 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/14/15 07:53 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/14/15 07:53 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/14/15 07:53 108-20-31.0 1
Ethylbenzene ND ug/L 10/14/15 07:53 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/14/15 07:53 87-68-31.0 1
2-Hexanone ND ug/L 10/14/15 07:53 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/14/15 07:53 99-87-61.0 1
Methylene Chloride ND ug/L 10/14/15 07:53 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/14/15 07:53 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/14/15 07:53 1634-04-41.0 1
Naphthalene ND ug/L 10/14/15 07:53 91-20-31.0 1
Styrene ND ug/L 10/14/15 07:53 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/14/15 07:53 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/14/15 07:53 79-34-51.0 1
Tetrachloroethene ND ug/L 10/14/15 07:53 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Sample:MW-7 Lab ID:92271206006 Collected:10/08/15 11:05 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Toluene ND ug/L 10/14/15 07:53 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/14/15 07:53 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/14/15 07:53 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/14/15 07:53 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/14/15 07:53 79-00-51.0 1
Trichloroethene ND ug/L 10/14/15 07:53 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/14/15 07:53 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/14/15 07:53 96-18-41.0 1
Vinyl acetate ND ug/L 10/14/15 07:53 108-05-42.0 1
Vinyl chloride ND ug/L 10/14/15 07:53 75-01-41.0 1
Xylene (Total)ND ug/L 10/14/15 07:53 1330-20-72.0 1
m&p-Xylene ND ug/L 10/14/15 07:53 179601-23-12.0 1
o-Xylene ND ug/L 10/14/15 07:53 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %10/14/15 07:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %10/14/15 07:53 17060-07-070-130 1
Toluene-d8 (S)100 %10/14/15 07:53 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/15 17:07 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)105 %10/12/15 17:07 17060-07-050-150 1
Toluene-d8 (S)123 %10/12/15 17:07 2037-26-550-150 1
Sample:MW-8 Lab ID:92271206007 Collected:10/08/15 11:55 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 10/14/15 08:10 67-64-125.0 1
Benzene ND ug/L 10/14/15 08:10 71-43-21.0 1
Bromobenzene ND ug/L 10/14/15 08:10 108-86-11.0 1
Bromochloromethane ND ug/L 10/14/15 08:10 74-97-51.0 1
Bromodichloromethane ND ug/L 10/14/15 08:10 75-27-41.0 1
Bromoform ND ug/L 10/14/15 08:10 75-25-21.0 1
Bromomethane ND ug/L 10/14/15 08:10 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/14/15 08:10 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/14/15 08:10 56-23-51.0 1
Chlorobenzene ND ug/L 10/14/15 08:10 108-90-71.0 1
Chloroethane ND ug/L 10/14/15 08:10 75-00-31.0 1
Chloroform ND ug/L 10/14/15 08:10 67-66-31.0 1
Chloromethane ND ug/L 10/14/15 08:10 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/14/15 08:10 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/14/15 08:10 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/14/15 08:10 96-12-82.0 1
Dibromochloromethane ND ug/L 10/14/15 08:10 124-48-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Sample:MW-8 Lab ID:92271206007 Collected:10/08/15 11:55 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 10/14/15 08:10 106-93-41.0 1
Dibromomethane ND ug/L 10/14/15 08:10 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/14/15 08:10 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/14/15 08:10 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/14/15 08:10 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/14/15 08:10 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/14/15 08:10 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/14/15 08:10 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/14/15 08:10 75-35-41.0 1
cis-1,2-Dichloroethene 19.8 ug/L 10/14/15 08:10 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/14/15 08:10 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/14/15 08:10 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/14/15 08:10 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/14/15 08:10 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/14/15 08:10 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/14/15 08:10 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/14/15 08:10 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/14/15 08:10 108-20-31.0 1
Ethylbenzene ND ug/L 10/14/15 08:10 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/14/15 08:10 87-68-31.0 1
2-Hexanone ND ug/L 10/14/15 08:10 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/14/15 08:10 99-87-61.0 1
Methylene Chloride ND ug/L 10/14/15 08:10 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/14/15 08:10 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/14/15 08:10 1634-04-41.0 1
Naphthalene ND ug/L 10/14/15 08:10 91-20-31.0 1
Styrene ND ug/L 10/14/15 08:10 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/14/15 08:10 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/14/15 08:10 79-34-51.0 1
Tetrachloroethene 163 ug/L 10/14/15 08:10 127-18-41.0 1
Toluene ND ug/L 10/14/15 08:10 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/14/15 08:10 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/14/15 08:10 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/14/15 08:10 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/14/15 08:10 79-00-51.0 1
Trichloroethene 25.5 ug/L 10/14/15 08:10 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/14/15 08:10 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/14/15 08:10 96-18-41.0 1
Vinyl acetate ND ug/L 10/14/15 08:10 108-05-42.0 1
Vinyl chloride ND ug/L 10/14/15 08:10 75-01-41.0 1
Xylene (Total)ND ug/L 10/14/15 08:10 1330-20-72.0 1
m&p-Xylene ND ug/L 10/14/15 08:10 179601-23-12.0 1
o-Xylene ND ug/L 10/14/15 08:10 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %10/14/15 08:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %10/14/15 08:10 17060-07-070-130 1
Toluene-d8 (S)98 %10/14/15 08:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Sample:MW-8 Lab ID:92271206007 Collected:10/08/15 11:55 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/15 17:27 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %10/12/15 17:27 17060-07-050-150 1
Toluene-d8 (S)122 %10/12/15 17:27 2037-26-550-150 1
Sample:DW-1 Lab ID:92271206008 Collected:10/08/15 12:40 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 10/15/15 05:26 67-64-125.0 1
Benzene ND ug/L 10/15/15 05:26 71-43-21.0 1
Bromobenzene ND ug/L 10/15/15 05:26 108-86-11.0 1
Bromochloromethane ND ug/L 10/15/15 05:26 74-97-51.0 1
Bromodichloromethane ND ug/L 10/15/15 05:26 75-27-41.0 1
Bromoform ND ug/L 10/15/15 05:26 75-25-21.0 1
Bromomethane ND ug/L 10/15/15 05:26 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/15/15 05:26 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/15/15 05:26 56-23-51.0 1
Chlorobenzene ND ug/L 10/15/15 05:26 108-90-71.0 1
Chloroethane ND ug/L 10/15/15 05:26 75-00-31.0 1
Chloroform ND ug/L 10/15/15 05:26 67-66-31.0 1
Chloromethane ND ug/L 10/15/15 05:26 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/15/15 05:26 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/15/15 05:26 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/15/15 05:26 96-12-82.0 1
Dibromochloromethane ND ug/L 10/15/15 05:26 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/15/15 05:26 106-93-41.0 1
Dibromomethane ND ug/L 10/15/15 05:26 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/15/15 05:26 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/15/15 05:26 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/15/15 05:26 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/15/15 05:26 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/15/15 05:26 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/15/15 05:26 107-06-21.0 1
1,1-Dichloroethene 2.5 ug/L 10/15/15 05:26 75-35-41.0 1
cis-1,2-Dichloroethene 42.3 ug/L 10/15/15 05:26 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/15/15 05:26 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/15/15 05:26 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/15/15 05:26 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/15/15 05:26 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/15/15 05:26 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/15/15 05:26 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/15/15 05:26 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/15/15 05:26 108-20-31.0 1
Ethylbenzene ND ug/L 10/15/15 05:26 100-41-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Sample:DW-1 Lab ID:92271206008 Collected:10/08/15 12:40 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Hexachloro-1,3-butadiene ND ug/L 10/15/15 05:26 87-68-31.0 1
2-Hexanone ND ug/L 10/15/15 05:26 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/15/15 05:26 99-87-61.0 1
Methylene Chloride ND ug/L 10/15/15 05:26 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/15/15 05:26 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/15/15 05:26 1634-04-41.0 1
Naphthalene ND ug/L 10/15/15 05:26 91-20-31.0 1
Styrene ND ug/L 10/15/15 05:26 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/15/15 05:26 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/15/15 05:26 79-34-51.0 1
Tetrachloroethene 148 ug/L 10/15/15 05:26 127-18-41.0 1
Toluene ND ug/L 10/15/15 05:26 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/15/15 05:26 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/15/15 05:26 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/15/15 05:26 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/15/15 05:26 79-00-51.0 1
Trichloroethene 78.2 ug/L 10/15/15 05:26 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/15/15 05:26 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/15/15 05:26 96-18-41.0 1
Vinyl acetate ND ug/L 10/15/15 05:26 108-05-42.0 1
Vinyl chloride ND ug/L 10/15/15 05:26 75-01-41.0 1
Xylene (Total)ND ug/L 10/15/15 05:26 1330-20-72.0 1
m&p-Xylene ND ug/L 10/15/15 05:26 179601-23-12.0 1
o-Xylene ND ug/L 10/15/15 05:26 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %10/15/15 05:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %10/15/15 05:26 17060-07-070-130 1
Toluene-d8 (S)97 %10/15/15 05:26 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/15 17:47 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)106 %10/12/15 17:47 17060-07-050-150 1
Toluene-d8 (S)123 %10/12/15 17:47 2037-26-550-150 1
Sample:DUP-01-1008 2015 Lab ID:92271206009 Collected:10/08/15 00:00 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 10/15/15 22:12 67-64-125.0 1
Benzene ND ug/L 10/15/15 22:12 71-43-21.0 1
Bromobenzene ND ug/L 10/15/15 22:12 108-86-11.0 1
Bromochloromethane ND ug/L 10/15/15 22:12 74-97-51.0 1
Bromodichloromethane ND ug/L 10/15/15 22:12 75-27-41.0 1
Bromoform ND ug/L 10/15/15 22:12 75-25-2 M11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Sample:DUP-01-1008 2015 Lab ID:92271206009 Collected:10/08/15 00:00 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Bromomethane ND ug/L 10/15/15 22:12 74-83-9 M12.0 1
2-Butanone (MEK)ND ug/L 10/15/15 22:12 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/15/15 22:12 56-23-51.0 1
Chlorobenzene ND ug/L 10/15/15 22:12 108-90-71.0 1
Chloroethane ND ug/L 10/15/15 22:12 75-00-31.0 1
Chloroform ND ug/L 10/15/15 22:12 67-66-31.0 1
Chloromethane ND ug/L 10/15/15 22:12 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/15/15 22:12 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/15/15 22:12 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/15/15 22:12 96-12-82.0 1
Dibromochloromethane ND ug/L 10/15/15 22:12 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/15/15 22:12 106-93-41.0 1
Dibromomethane ND ug/L 10/15/15 22:12 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/15/15 22:12 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/15/15 22:12 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/15/15 22:12 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/15/15 22:12 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/15/15 22:12 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/15/15 22:12 107-06-21.0 1
1,1-Dichloroethene 2.3 ug/L 10/15/15 22:12 75-35-41.0 1
cis-1,2-Dichloroethene 38.1 ug/L 10/15/15 22:12 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/15/15 22:12 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/15/15 22:12 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/15/15 22:12 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/15/15 22:12 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/15/15 22:12 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/15/15 22:12 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/15/15 22:12 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/15/15 22:12 108-20-31.0 1
Ethylbenzene ND ug/L 10/15/15 22:12 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/15/15 22:12 87-68-31.0 1
2-Hexanone ND ug/L 10/15/15 22:12 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/15/15 22:12 99-87-61.0 1
Methylene Chloride ND ug/L 10/15/15 22:12 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/15/15 22:12 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/15/15 22:12 1634-04-41.0 1
Naphthalene ND ug/L 10/15/15 22:12 91-20-31.0 1
Styrene ND ug/L 10/15/15 22:12 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/15/15 22:12 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/15/15 22:12 79-34-51.0 1
Tetrachloroethene 166 ug/L 10/15/15 22:12 127-18-41.0 1
Toluene ND ug/L 10/15/15 22:12 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/15/15 22:12 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/15/15 22:12 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/15/15 22:12 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/15/15 22:12 79-00-51.0 1
Trichloroethene 77.5 ug/L 10/15/15 22:12 79-01-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Sample:DUP-01-1008 2015 Lab ID:92271206009 Collected:10/08/15 00:00 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Trichlorofluoromethane ND ug/L 10/15/15 22:12 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/15/15 22:12 96-18-41.0 1
Vinyl acetate ND ug/L 10/15/15 22:12 108-05-42.0 1
Vinyl chloride ND ug/L 10/15/15 22:12 75-01-41.0 1
Xylene (Total)ND ug/L 10/15/15 22:12 1330-20-72.0 1
m&p-Xylene ND ug/L 10/15/15 22:12 179601-23-12.0 1
o-Xylene ND ug/L 10/15/15 22:12 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %10/15/15 22:12 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %10/15/15 22:12 17060-07-070-130 1
Toluene-d8 (S)97 %10/15/15 22:12 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/15 18:08 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)106 %10/12/15 18:08 17060-07-050-150 1
Toluene-d8 (S)123 %10/12/15 18:08 2037-26-550-150 1
Sample:EB-01-1008 2016 Lab ID:92271206010 Collected:10/08/15 13:45 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 10/12/15 14:20 67-64-125.0 1
Benzene ND ug/L 10/12/15 14:20 71-43-21.0 1
Bromobenzene ND ug/L 10/12/15 14:20 108-86-11.0 1
Bromochloromethane ND ug/L 10/12/15 14:20 74-97-51.0 1
Bromodichloromethane ND ug/L 10/12/15 14:20 75-27-41.0 1
Bromoform ND ug/L 10/12/15 14:20 75-25-21.0 1
Bromomethane ND ug/L 10/12/15 14:20 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/12/15 14:20 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/12/15 14:20 56-23-51.0 1
Chlorobenzene ND ug/L 10/12/15 14:20 108-90-71.0 1
Chloroethane ND ug/L 10/12/15 14:20 75-00-31.0 1
Chloroform ND ug/L 10/12/15 14:20 67-66-31.0 1
Chloromethane ND ug/L 10/12/15 14:20 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/12/15 14:20 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/12/15 14:20 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/15 14:20 96-12-82.0 1
Dibromochloromethane ND ug/L 10/12/15 14:20 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/15 14:20 106-93-41.0 1
Dibromomethane ND ug/L 10/12/15 14:20 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/12/15 14:20 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/12/15 14:20 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/12/15 14:20 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/12/15 14:20 75-71-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
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Page 17 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Sample:EB-01-1008 2016 Lab ID:92271206010 Collected:10/08/15 13:45 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,1-Dichloroethane ND ug/L 10/12/15 14:20 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/12/15 14:20 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/12/15 14:20 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/12/15 14:20 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/12/15 14:20 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/12/15 14:20 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/12/15 14:20 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/12/15 14:20 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/12/15 14:20 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/12/15 14:20 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/12/15 14:20 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/12/15 14:20 108-20-31.0 1
Ethylbenzene ND ug/L 10/12/15 14:20 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/12/15 14:20 87-68-31.0 1
2-Hexanone ND ug/L 10/12/15 14:20 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/12/15 14:20 99-87-61.0 1
Methylene Chloride ND ug/L 10/12/15 14:20 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/15 14:20 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/12/15 14:20 1634-04-41.0 1
Naphthalene ND ug/L 10/12/15 14:20 91-20-31.0 1
Styrene ND ug/L 10/12/15 14:20 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/15 14:20 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/15 14:20 79-34-51.0 1
Tetrachloroethene ND ug/L 10/12/15 14:20 127-18-41.0 1
Toluene ND ug/L 10/12/15 14:20 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/12/15 14:20 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/12/15 14:20 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/12/15 14:20 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/12/15 14:20 79-00-51.0 1
Trichloroethene ND ug/L 10/12/15 14:20 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/12/15 14:20 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/12/15 14:20 96-18-41.0 1
Vinyl acetate ND ug/L 10/12/15 14:20 108-05-42.0 1
Vinyl chloride ND ug/L 10/12/15 14:20 75-01-41.0 1
Xylene (Total)ND ug/L 10/12/15 14:20 1330-20-72.0 1
m&p-Xylene ND ug/L 10/12/15 14:20 179601-23-12.0 1
o-Xylene ND ug/L 10/12/15 14:20 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %10/12/15 14:20 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %10/12/15 14:20 17060-07-070-130 1
Toluene-d8 (S)100 %10/12/15 14:20 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/15 18:28 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)107 %10/12/15 18:28 17060-07-050-150 1
Toluene-d8 (S)125 %10/12/15 18:28 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Sample:Trip Blank Lab ID:92271206011 Collected:10/08/15 00:00 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 10/12/15 13:28 67-64-125.0 1
Benzene ND ug/L 10/12/15 13:28 71-43-21.0 1
Bromobenzene ND ug/L 10/12/15 13:28 108-86-11.0 1
Bromochloromethane ND ug/L 10/12/15 13:28 74-97-51.0 1
Bromodichloromethane ND ug/L 10/12/15 13:28 75-27-41.0 1
Bromoform ND ug/L 10/12/15 13:28 75-25-21.0 1
Bromomethane ND ug/L 10/12/15 13:28 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/12/15 13:28 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/12/15 13:28 56-23-51.0 1
Chlorobenzene ND ug/L 10/12/15 13:28 108-90-71.0 1
Chloroethane ND ug/L 10/12/15 13:28 75-00-31.0 1
Chloroform ND ug/L 10/12/15 13:28 67-66-31.0 1
Chloromethane ND ug/L 10/12/15 13:28 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/12/15 13:28 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/12/15 13:28 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/15 13:28 96-12-82.0 1
Dibromochloromethane ND ug/L 10/12/15 13:28 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/15 13:28 106-93-41.0 1
Dibromomethane ND ug/L 10/12/15 13:28 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/12/15 13:28 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/12/15 13:28 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/12/15 13:28 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/12/15 13:28 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/12/15 13:28 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/12/15 13:28 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/12/15 13:28 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/12/15 13:28 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/12/15 13:28 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/12/15 13:28 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/12/15 13:28 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/12/15 13:28 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/12/15 13:28 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/12/15 13:28 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/12/15 13:28 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/12/15 13:28 108-20-31.0 1
Ethylbenzene ND ug/L 10/12/15 13:28 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/12/15 13:28 87-68-31.0 1
2-Hexanone ND ug/L 10/12/15 13:28 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/12/15 13:28 99-87-61.0 1
Methylene Chloride ND ug/L 10/12/15 13:28 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/15 13:28 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/12/15 13:28 1634-04-41.0 1
Naphthalene ND ug/L 10/12/15 13:28 91-20-31.0 1
Styrene ND ug/L 10/12/15 13:28 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/15 13:28 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/15 13:28 79-34-51.0 1
Tetrachloroethene ND ug/L 10/12/15 13:28 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Sample:Trip Blank Lab ID:92271206011 Collected:10/08/15 00:00 Received:10/09/15 09:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Toluene ND ug/L 10/12/15 13:28 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/12/15 13:28 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/12/15 13:28 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/12/15 13:28 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/12/15 13:28 79-00-51.0 1
Trichloroethene ND ug/L 10/12/15 13:28 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/12/15 13:28 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/12/15 13:28 96-18-41.0 1
Vinyl acetate ND ug/L 10/12/15 13:28 108-05-42.0 1
Vinyl chloride ND ug/L 10/12/15 13:28 75-01-41.0 1
Xylene (Total)ND ug/L 10/12/15 13:28 1330-20-72.0 1
m&p-Xylene ND ug/L 10/12/15 13:28 179601-23-12.0 1
o-Xylene ND ug/L 10/12/15 13:28 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)104 %10/12/15 13:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %10/12/15 13:28 17060-07-070-130 1
Toluene-d8 (S)98 %10/12/15 13:28 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/15 18:48 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)106 %10/12/15 18:48 17060-07-050-150 1
Toluene-d8 (S)121 %10/12/15 18:48 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/33753
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92271206010, 92271206011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1580439
Associated Lab Samples:92271206010, 92271206011
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/12/15 13:11
1,1,1-Trichloroethane ug/L ND 1.0 10/12/15 13:11
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/12/15 13:11
1,1,2-Trichloroethane ug/L ND 1.0 10/12/15 13:11
1,1-Dichloroethane ug/L ND 1.0 10/12/15 13:11
1,1-Dichloroethene ug/L ND 1.0 10/12/15 13:11
1,1-Dichloropropene ug/L ND 1.0 10/12/15 13:11
1,2,3-Trichlorobenzene ug/L ND 1.0 10/12/15 13:11
1,2,3-Trichloropropane ug/L ND 1.0 10/12/15 13:11
1,2,4-Trichlorobenzene ug/L ND 1.0 10/12/15 13:11
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/12/15 13:11
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/12/15 13:11
1,2-Dichlorobenzene ug/L ND 1.0 10/12/15 13:11
1,2-Dichloroethane ug/L ND 1.0 10/12/15 13:11
1,2-Dichloropropane ug/L ND 1.0 10/12/15 13:11
1,3-Dichlorobenzene ug/L ND 1.0 10/12/15 13:11
1,3-Dichloropropane ug/L ND 1.0 10/12/15 13:11
1,4-Dichlorobenzene ug/L ND 1.0 10/12/15 13:11
2,2-Dichloropropane ug/L ND 1.0 10/12/15 13:11
2-Butanone (MEK)ug/L ND 5.0 10/12/15 13:11
2-Chlorotoluene ug/L ND 1.0 10/12/15 13:11
2-Hexanone ug/L ND 5.0 10/12/15 13:11
4-Chlorotoluene ug/L ND 1.0 10/12/15 13:11
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/12/15 13:11
Acetone ug/L ND 25.0 10/12/15 13:11
Benzene ug/L ND 1.0 10/12/15 13:11
Bromobenzene ug/L ND 1.0 10/12/15 13:11
Bromochloromethane ug/L ND 1.0 10/12/15 13:11
Bromodichloromethane ug/L ND 1.0 10/12/15 13:11
Bromoform ug/L ND 1.0 10/12/15 13:11
Bromomethane ug/L ND 2.0 10/12/15 13:11
Carbon tetrachloride ug/L ND 1.0 10/12/15 13:11
Chlorobenzene ug/L ND 1.0 10/12/15 13:11
Chloroethane ug/L ND 1.0 10/12/15 13:11
Chloroform ug/L ND 1.0 10/12/15 13:11
Chloromethane ug/L ND 1.0 10/12/15 13:11
cis-1,2-Dichloroethene ug/L ND 1.0 10/12/15 13:11
cis-1,3-Dichloropropene ug/L ND 1.0 10/12/15 13:11
Dibromochloromethane ug/L ND 1.0 10/12/15 13:11
Dibromomethane ug/L ND 1.0 10/12/15 13:11
Dichlorodifluoromethane ug/L ND 1.0 10/12/15 13:11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1580439
Associated Lab Samples:92271206010, 92271206011
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 1.0 10/12/15 13:11
Ethylbenzene ug/L ND 1.0 10/12/15 13:11
Hexachloro-1,3-butadiene ug/L ND 1.0 10/12/15 13:11
m&p-Xylene ug/L ND 2.0 10/12/15 13:11
Methyl-tert-butyl ether ug/L ND 1.0 10/12/15 13:11
Methylene Chloride ug/L ND 2.0 10/12/15 13:11
Naphthalene ug/L ND 1.0 10/12/15 13:11
o-Xylene ug/L ND 1.0 10/12/15 13:11
p-Isopropyltoluene ug/L ND 1.0 10/12/15 13:11
Styrene ug/L ND 1.0 10/12/15 13:11
Tetrachloroethene ug/L ND 1.0 10/12/15 13:11
Toluene ug/L ND 1.0 10/12/15 13:11
trans-1,2-Dichloroethene ug/L ND 1.0 10/12/15 13:11
trans-1,3-Dichloropropene ug/L ND 1.0 10/12/15 13:11
Trichloroethene ug/L ND 1.0 10/12/15 13:11
Trichlorofluoromethane ug/L ND 1.0 10/12/15 13:11
Vinyl acetate ug/L ND 2.0 10/12/15 13:11
Vinyl chloride ug/L ND 1.0 10/12/15 13:11
Xylene (Total)ug/L ND 2.0 10/12/15 13:11
1,2-Dichloroethane-d4 (S)%105 70-130 10/12/15 13:11
4-Bromofluorobenzene (S)%103 70-130 10/12/15 13:11
Toluene-d8 (S)%99 70-130 10/12/15 13:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1580440LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 45.750 91 70-130
1,1,1-Trichloroethane ug/L 51.850 104 70-130
1,1,2,2-Tetrachloroethane ug/L 46.450 93 70-130
1,1,2-Trichloroethane ug/L 47.750 95 70-130
1,1-Dichloroethane ug/L 50.150 100 70-130
1,1-Dichloroethene ug/L 52.750 105 70-132
1,1-Dichloropropene ug/L 50.650 101 70-130
1,2,3-Trichlorobenzene ug/L 47.050 94 70-135
1,2,3-Trichloropropane ug/L 47.650 95 70-130
1,2,4-Trichlorobenzene ug/L 48.250 96 70-134
1,2-Dibromo-3-chloropropane ug/L 42.350 85 70-130
1,2-Dibromoethane (EDB)ug/L 48.550 97 70-130
1,2-Dichlorobenzene ug/L 47.350 95 70-130
1,2-Dichloroethane ug/L 49.350 99 70-130
1,2-Dichloropropane ug/L 46.850 94 70-130
1,3-Dichlorobenzene ug/L 48.650 97 70-130
1,3-Dichloropropane ug/L 46.850 94 70-130
1,4-Dichlorobenzene ug/L 47.850 96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1580440LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 52.150 104 58-145
2-Butanone (MEK)ug/L 103100 103 70-145
2-Chlorotoluene ug/L 43.950 88 70-130
2-Hexanone ug/L 93.7100 94 70-144
4-Chlorotoluene ug/L 45.050 90 70-130
4-Methyl-2-pentanone (MIBK)ug/L 102100 102 70-140
Acetone ug/L 117100 117 50-175
Benzene ug/L 48.850 98 70-130
Bromobenzene ug/L 45.850 92 70-130
Bromochloromethane ug/L 53.350 107 70-130
Bromodichloromethane ug/L 46.950 94 70-130
Bromoform ug/L 40.350 81 70-130
Bromomethane ug/L 47.550 95 54-130
Carbon tetrachloride ug/L 49.350 99 70-132
Chlorobenzene ug/L 47.150 94 70-130
Chloroethane ug/L 40.750 81 64-134
Chloroform ug/L 50.450 101 70-130
Chloromethane ug/L 46.250 92 64-130
cis-1,2-Dichloroethene ug/L 49.650 99 70-131
cis-1,3-Dichloropropene ug/L 47.750 95 70-130
Dibromochloromethane ug/L 44.350 89 70-130
Dibromomethane ug/L 51.850 104 70-131
Dichlorodifluoromethane ug/L 50.450 101 56-130
Diisopropyl ether ug/L 53.750 107 70-130
Ethylbenzene ug/L 46.950 94 70-130
Hexachloro-1,3-butadiene ug/L 57.250 114 70-130
m&p-Xylene ug/L 92.8100 93 70-130
Methyl-tert-butyl ether ug/L 53.050 106 70-130
Methylene Chloride ug/L 57.350 115 63-130
Naphthalene ug/L 45.350 91 70-138
o-Xylene ug/L 46.650 93 70-130
p-Isopropyltoluene ug/L 47.950 96 70-130
Styrene ug/L 46.050 92 70-130
Tetrachloroethene ug/L 46.250 92 70-130
Toluene ug/L 48.950 98 70-130
trans-1,2-Dichloroethene ug/L 50.050 100 70-130
trans-1,3-Dichloropropene ug/L 48.150 96 70-132
Trichloroethene ug/L 48.150 96 70-130
Trichlorofluoromethane ug/L 55.250 110 62-133
Vinyl acetate ug/L 105100 105 66-157
Vinyl chloride ug/L 54.250 108 50-150
Xylene (Total)ug/L 139150 93 70-130
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%109 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 23 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1580442MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92271213002
1580443
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 95 70-130100 520ND19.0 20.0
1,1,1-Trichloroethane ug/L 20 120 70-130125 420ND24.0 25.0
1,1,2,2-Tetrachloroethane ug/L 20 95 70-13099 520ND18.9 19.8
1,1,2-Trichloroethane ug/L 20 103 70-130110 620ND20.6 22.0
1,1-Dichloroethane ug/L 20 115 70-130120 520ND22.9 24.0
1,1-Dichloroethene ug/L 20 120 70-166125 420ND24.1 25.0
1,1-Dichloropropene ug/L 20 115 70-130123 620ND23.0 24.5
1,2,3-Trichlorobenzene ug/L 20 93 70-13094 220ND18.6 18.8
1,2,3-Trichloropropane ug/L 20 98 70-13099 120ND19.6 19.8
1,2,4-Trichlorobenzene ug/L 20 95 70-13099 320ND19.1 19.8
1,2-Dibromo-3-chloropropane ug/L 20 76 70-13078 320ND15.1 15.6
1,2-Dibromoethane (EDB)ug/L 20 101 70-130105 420ND20.3 21.0
1,2-Dichlorobenzene ug/L 20 100 70-130105 520ND19.9 21.0
1,2-Dichloroethane ug/L 20 109 70-130113 420ND21.9 22.8
1,2-Dichloropropane ug/L 20 105 70-130111 520ND20.9 22.1
1,3-Dichlorobenzene ug/L 20 103 70-130109 520ND20.7 21.9
1,3-Dichloropropane ug/L 20 101 70-130103 220ND20.1 20.5
1,4-Dichlorobenzene ug/L 20 101 70-130106 520ND20.2 21.2
2,2-Dichloropropane ug/L 20 108 70-130112 420ND21.6 22.5
2-Butanone (MEK)ug/L 40 101 70-130107 540ND40.5 42.8
2-Chlorotoluene ug/L 20 93 70-13099 520ND18.7 19.7
2-Hexanone ug/L 40 91 70-13094 440ND36.3 37.6
4-Chlorotoluene ug/L 20 99 70-130105 520ND19.9 20.9
4-Methyl-2-pentanone (MIBK)ug/L 40 104 70-130109 540ND41.7 43.6
Acetone ug/L 40 98 70-130106 840ND39.4 42.6
Benzene ug/L 20 112 70-148118 520ND22.5 23.6
Bromobenzene ug/L 20 101 70-130106 520ND20.1 21.2
Bromochloromethane ug/L 20 115 70-130123 620ND23.1 24.5
Bromodichloromethane ug/L 20 100 70-130102 220ND20.0 20.3
Bromoform ug/L 20 72 70-13075 320ND14.4 14.9
Bromomethane ug/L 20 96 70-130114 1720ND19.2 22.8
Carbon tetrachloride ug/L 20 112 70-130115 220ND22.5 23.1
Chlorobenzene ug/L 20 103 70-146107 320ND20.7 21.4
Chloroethane ug/L 20 104 70-130109 420ND20.8 21.7
Chloroform ug/L 20 112 70-130121 720ND22.5 24.1
Chloromethane ug/L M12014170-130128 1020ND28.3 25.5
cis-1,2-Dichloroethene ug/L M1,R12040970-130209 442028.1 110 70.0
cis-1,3-Dichloropropene ug/L 20 96 70-130102 720ND19.1 20.4
Dibromochloromethane ug/L 20 87 70-13090 420ND17.3 18.0
Dibromomethane ug/L 20 109 70-130114 420ND21.9 22.8
Dichlorodifluoromethane ug/L 20 117 70-130125 620ND23.4 24.9
Diisopropyl ether ug/L 20 118 70-130124 520ND23.5 24.8
Ethylbenzene ug/L 20 103 70-130108 520ND20.7 21.6
Hexachloro-1,3-butadiene ug/L 20 110 70-130121 1020ND22.0 24.2
m&p-Xylene ug/L 40 101 70-130107 640ND40.5 43.0
Methyl-tert-butyl ether ug/L 20 111 70-130116 520ND22.2 23.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1580442MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92271213002
1580443
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Methylene Chloride ug/L 20 116 70-130122 520ND23.3 24.3
Naphthalene ug/L 20 88 70-13093 520ND17.8 18.8
o-Xylene ug/L 20 101 70-130106 520ND20.2 21.1
p-Isopropyltoluene ug/L 20 100 70-130104 520ND19.9 20.9
Styrene ug/L 20 97 70-130101 420ND19.4 20.2
Tetrachloroethene ug/L 20 104 70-130107 2205.3 26.2 26.6
Toluene ug/L 20 112 70-155114 220ND22.8 23.2
trans-1,2-Dichloroethene ug/L 20 115 70-130120 520ND22.9 24.0
trans-1,3-Dichloropropene ug/L 20 97 70-130102 520ND19.3 20.3
Trichloroethene ug/L 20 117 69-151123 22041.5 64.9 66.1
Trichlorofluoromethane ug/L M12013570-130142 520ND27.1 28.4
Vinyl acetate ug/L 40 101 70-130101 040ND40.5 40.4
Vinyl chloride ug/L M12014170-130130 820ND28.7 26.5
1,2-Dichloroethane-d4 (S)%104 70-130105
4-Bromofluorobenzene (S)%104 70-130106
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/33783
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92271206004, 92271206005, 92271206006, 92271206007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1581737
Associated Lab Samples:92271206004, 92271206005, 92271206006, 92271206007
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/14/15 01:55
1,1,1-Trichloroethane ug/L ND 1.0 10/14/15 01:55
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/14/15 01:55
1,1,2-Trichloroethane ug/L ND 1.0 10/14/15 01:55
1,1-Dichloroethane ug/L ND 1.0 10/14/15 01:55
1,1-Dichloroethene ug/L ND 1.0 10/14/15 01:55
1,1-Dichloropropene ug/L ND 1.0 10/14/15 01:55
1,2,3-Trichlorobenzene ug/L ND 1.0 10/14/15 01:55
1,2,3-Trichloropropane ug/L ND 1.0 10/14/15 01:55
1,2,4-Trichlorobenzene ug/L ND 1.0 10/14/15 01:55
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/14/15 01:55
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/14/15 01:55
1,2-Dichlorobenzene ug/L ND 1.0 10/14/15 01:55
1,2-Dichloroethane ug/L ND 1.0 10/14/15 01:55
1,2-Dichloropropane ug/L ND 1.0 10/14/15 01:55
1,3-Dichlorobenzene ug/L ND 1.0 10/14/15 01:55
1,3-Dichloropropane ug/L ND 1.0 10/14/15 01:55
1,4-Dichlorobenzene ug/L ND 1.0 10/14/15 01:55
2,2-Dichloropropane ug/L ND 1.0 10/14/15 01:55
2-Butanone (MEK)ug/L ND 5.0 10/14/15 01:55
2-Chlorotoluene ug/L ND 1.0 10/14/15 01:55
2-Hexanone ug/L ND 5.0 10/14/15 01:55
4-Chlorotoluene ug/L ND 1.0 10/14/15 01:55
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/14/15 01:55
Acetone ug/L ND 25.0 10/14/15 01:55
Benzene ug/L ND 1.0 10/14/15 01:55
Bromobenzene ug/L ND 1.0 10/14/15 01:55
Bromochloromethane ug/L ND 1.0 10/14/15 01:55
Bromodichloromethane ug/L ND 1.0 10/14/15 01:55
Bromoform ug/L ND 1.0 10/14/15 01:55
Bromomethane ug/L ND 2.0 10/14/15 01:55
Carbon tetrachloride ug/L ND 1.0 10/14/15 01:55
Chlorobenzene ug/L ND 1.0 10/14/15 01:55
Chloroethane ug/L ND 1.0 10/14/15 01:55
Chloroform ug/L ND 1.0 10/14/15 01:55
Chloromethane ug/L ND 1.0 10/14/15 01:55
cis-1,2-Dichloroethene ug/L ND 1.0 10/14/15 01:55
cis-1,3-Dichloropropene ug/L ND 1.0 10/14/15 01:55
Dibromochloromethane ug/L ND 1.0 10/14/15 01:55
Dibromomethane ug/L ND 1.0 10/14/15 01:55
Dichlorodifluoromethane ug/L ND 1.0 10/14/15 01:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1581737
Associated Lab Samples:92271206004, 92271206005, 92271206006, 92271206007
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 1.0 10/14/15 01:55
Ethylbenzene ug/L ND 1.0 10/14/15 01:55
Hexachloro-1,3-butadiene ug/L ND 1.0 10/14/15 01:55
m&p-Xylene ug/L ND 2.0 10/14/15 01:55
Methyl-tert-butyl ether ug/L ND 1.0 10/14/15 01:55
Methylene Chloride ug/L ND 2.0 10/14/15 01:55
Naphthalene ug/L ND 1.0 10/14/15 01:55
o-Xylene ug/L ND 1.0 10/14/15 01:55
p-Isopropyltoluene ug/L ND 1.0 10/14/15 01:55
Styrene ug/L ND 1.0 10/14/15 01:55
Tetrachloroethene ug/L ND 1.0 10/14/15 01:55
Toluene ug/L ND 1.0 10/14/15 01:55
trans-1,2-Dichloroethene ug/L ND 1.0 10/14/15 01:55
trans-1,3-Dichloropropene ug/L ND 1.0 10/14/15 01:55
Trichloroethene ug/L ND 1.0 10/14/15 01:55
Trichlorofluoromethane ug/L ND 1.0 10/14/15 01:55
Vinyl acetate ug/L ND 2.0 10/14/15 01:55
Vinyl chloride ug/L ND 1.0 10/14/15 01:55
Xylene (Total)ug/L ND 2.0 10/14/15 01:55
1,2-Dichloroethane-d4 (S)%105 70-130 10/14/15 01:55
4-Bromofluorobenzene (S)%104 70-130 10/14/15 01:55
Toluene-d8 (S)%99 70-130 10/14/15 01:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1581738LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.050 92 70-130
1,1,1-Trichloroethane ug/L 53.250 106 70-130
1,1,2,2-Tetrachloroethane ug/L 47.850 96 70-130
1,1,2-Trichloroethane ug/L 50.550 101 70-130
1,1-Dichloroethane ug/L 52.950 106 70-130
1,1-Dichloroethene ug/L 54.250 108 70-132
1,1-Dichloropropene ug/L 52.050 104 70-130
1,2,3-Trichlorobenzene ug/L 44.950 90 70-135
1,2,3-Trichloropropane ug/L 48.050 96 70-130
1,2,4-Trichlorobenzene ug/L 46.550 93 70-134
1,2-Dibromo-3-chloropropane ug/L 40.050 80 70-130
1,2-Dibromoethane (EDB)ug/L 49.150 98 70-130
1,2-Dichlorobenzene ug/L 47.250 94 70-130
1,2-Dichloroethane ug/L 51.650 103 70-130
1,2-Dichloropropane ug/L 49.550 99 70-130
1,3-Dichlorobenzene ug/L 48.450 97 70-130
1,3-Dichloropropane ug/L 47.450 95 70-130
1,4-Dichlorobenzene ug/L 47.750 95 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1581738LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 49.650 99 58-145
2-Butanone (MEK)ug/L 106100 106 70-145
2-Chlorotoluene ug/L 44.850 90 70-130
2-Hexanone ug/L 93.9100 94 70-144
4-Chlorotoluene ug/L 45.250 90 70-130
4-Methyl-2-pentanone (MIBK)ug/L 108100 108 70-140
Acetone ug/L 124100 124 50-175
Benzene ug/L 52.550 105 70-130
Bromobenzene ug/L 46.850 94 70-130
Bromochloromethane ug/L 56.450 113 70-130
Bromodichloromethane ug/L 48.450 97 70-130
Bromoform ug/L 37.950 76 70-130
Bromomethane ug/L 49.050 98 54-130
Carbon tetrachloride ug/L 48.650 97 70-132
Chlorobenzene ug/L 47.750 95 70-130
Chloroethane ug/L 43.250 86 64-134
Chloroform ug/L 53.650 107 70-130
Chloromethane ug/L 51.250 102 64-130
cis-1,2-Dichloroethene ug/L 52.750 105 70-131
cis-1,3-Dichloropropene ug/L 49.450 99 70-130
Dibromochloromethane ug/L 42.950 86 70-130
Dibromomethane ug/L 54.050 108 70-131
Dichlorodifluoromethane ug/L 50.550 101 56-130
Diisopropyl ether ug/L 58.050 116 70-130
Ethylbenzene ug/L 47.250 94 70-130
Hexachloro-1,3-butadiene ug/L 55.050 110 70-130
m&p-Xylene ug/L 94.3100 94 70-130
Methyl-tert-butyl ether ug/L 55.650 111 70-130
Methylene Chloride ug/L 64.850 130 63-130
Naphthalene ug/L 45.250 90 70-138
o-Xylene ug/L 47.650 95 70-130
p-Isopropyltoluene ug/L 46.650 93 70-130
Styrene ug/L 47.150 94 70-130
Tetrachloroethene ug/L 45.550 91 70-130
Toluene ug/L 52.350 105 70-130
trans-1,2-Dichloroethene ug/L 52.950 106 70-130
trans-1,3-Dichloropropene ug/L 49.250 98 70-132
Trichloroethene ug/L 49.650 99 70-130
Trichlorofluoromethane ug/L 55.650 111 62-133
Vinyl acetate ug/L 111100 111 66-157
Vinyl chloride ug/L 55.850 112 50-150
Xylene (Total)ug/L 142150 95 70-130
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%107 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1581740MATRIX SPIKE SAMPLE:
MSSpike
Result
92271252002
1,1,1,2-Tetrachloroethane ug/L 19.120 95 70-130ND
1,1,1-Trichloroethane ug/L 24.220 121 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.920 99 70-130ND
1,1,2-Trichloroethane ug/L 21.520 107 70-130ND
1,1-Dichloroethane ug/L 25.620 119 70-1301.9
1,1-Dichloroethene ug/L 24.820 123 70-166ND
1,1-Dichloropropene ug/L 24.220 121 70-130ND
1,2,3-Trichlorobenzene ug/L 19.820 99 70-130ND
1,2,3-Trichloropropane ug/L 19.620 98 70-130ND
1,2,4-Trichlorobenzene ug/L 19.620 98 70-130ND
1,2-Dibromo-3-chloropropane ug/L 15.720 79 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.720 104 70-130ND
1,2-Dichlorobenzene ug/L 20.620 103 70-130ND
1,2-Dichloroethane ug/L 22.220 110 70-130ND
1,2-Dichloropropane ug/L 21.920 109 70-130ND
1,3-Dichlorobenzene ug/L 21.220 106 70-130ND
1,3-Dichloropropane ug/L 20.520 102 70-130ND
1,4-Dichlorobenzene ug/L 20.920 105 70-130ND
2,2-Dichloropropane ug/L 22.120 110 70-130ND
2-Butanone (MEK)ug/L 44.440 111 70-130ND
2-Chlorotoluene ug/L 19.520 98 70-130ND
2-Hexanone ug/L 38.340 96 70-130ND
4-Chlorotoluene ug/L 20.720 104 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 44.240 110 70-130ND
Acetone ug/L 43.940 110 70-130ND
Benzene ug/L 23.320 117 70-148ND
Bromobenzene ug/L 20.720 103 70-130ND
Bromochloromethane ug/L 24.220 121 70-130ND
Bromodichloromethane ug/L 19.720 99 70-130ND
Bromoform ug/L 13.7 M1206970-130ND
Bromomethane ug/L 24.820 124 70-130ND
Carbon tetrachloride ug/L 21.820 109 70-130ND
Chlorobenzene ug/L 21.020 105 70-146ND
Chloroethane ug/L 20.720 104 70-130ND
Chloroform ug/L 23.620 118 70-130ND
Chloromethane ug/L 23.920 119 70-130ND
cis-1,2-Dichloroethene ug/L 23.220 115 70-130ND
cis-1,3-Dichloropropene ug/L 20.420 102 70-130ND
Dibromochloromethane ug/L 16.720 83 70-130ND
Dibromomethane ug/L 22.920 115 70-130ND
Dichlorodifluoromethane ug/L 24.720 123 70-130ND
Diisopropyl ether ug/L 24.820 124 70-130ND
Ethylbenzene ug/L 21.220 106 70-130ND
Hexachloro-1,3-butadiene ug/L 25.920 130 70-130ND
m&p-Xylene ug/L 41.440 104 70-130ND
Methyl-tert-butyl ether ug/L 23.520 118 70-130ND
Methylene Chloride ug/L 24.420 122 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1581740MATRIX SPIKE SAMPLE:
MSSpike
Result
92271252002
Naphthalene ug/L 19.220 96 70-130ND
o-Xylene ug/L 20.720 104 70-130ND
p-Isopropyltoluene ug/L 21.220 106 70-130ND
Styrene ug/L 20.020 100 70-130ND
Tetrachloroethene ug/L 21.020 105 70-130ND
Toluene ug/L 23.220 116 70-155ND
trans-1,2-Dichloroethene ug/L 23.820 119 70-130ND
trans-1,3-Dichloropropene ug/L 19.820 99 70-130ND
Trichloroethene ug/L 22.920 115 69-151ND
Trichlorofluoromethane ug/L 26.7 M12013370-130ND
Vinyl acetate ug/L 40.940 102 70-130ND
Vinyl chloride ug/L 25.620 128 70-130ND
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%105 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92271254013
1581739SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Chlorotoluene ug/L NDND
2-Hexanone ug/L NDND
4-Chlorotoluene ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Benzene ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
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Huntersville, NC 28078
[phone]
Page 30 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92271254013
1581739SAMPLE DUPLICATE:
Bromobenzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Diisopropyl ether ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
m&p-Xylene ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylene Chloride ug/L NDND
Naphthalene ug/L NDND
o-Xylene ug/L NDND
p-Isopropyltoluene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%106 0106
4-Bromofluorobenzene (S)%103 2105
Toluene-d8 (S)%100 0100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/33803
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92271206001, 92271206002, 92271206003, 92271206008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1582957
Associated Lab Samples:92271206001, 92271206002, 92271206003, 92271206008
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/15/15 02:52
1,1,1-Trichloroethane ug/L ND 1.0 10/15/15 02:52
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/15/15 02:52
1,1,2-Trichloroethane ug/L ND 1.0 10/15/15 02:52
1,1-Dichloroethane ug/L ND 1.0 10/15/15 02:52
1,1-Dichloroethene ug/L ND 1.0 10/15/15 02:52
1,1-Dichloropropene ug/L ND 1.0 10/15/15 02:52
1,2,3-Trichlorobenzene ug/L ND 1.0 10/15/15 02:52
1,2,3-Trichloropropane ug/L ND 1.0 10/15/15 02:52
1,2,4-Trichlorobenzene ug/L ND 1.0 10/15/15 02:52
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/15/15 02:52
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/15/15 02:52
1,2-Dichlorobenzene ug/L ND 1.0 10/15/15 02:52
1,2-Dichloroethane ug/L ND 1.0 10/15/15 02:52
1,2-Dichloropropane ug/L ND 1.0 10/15/15 02:52
1,3-Dichlorobenzene ug/L ND 1.0 10/15/15 02:52
1,3-Dichloropropane ug/L ND 1.0 10/15/15 02:52
1,4-Dichlorobenzene ug/L ND 1.0 10/15/15 02:52
2,2-Dichloropropane ug/L ND 1.0 10/15/15 02:52
2-Butanone (MEK)ug/L ND 5.0 10/15/15 02:52
2-Chlorotoluene ug/L ND 1.0 10/15/15 02:52
2-Hexanone ug/L ND 5.0 10/15/15 02:52
4-Chlorotoluene ug/L ND 1.0 10/15/15 02:52
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/15/15 02:52
Acetone ug/L ND 25.0 10/15/15 02:52
Benzene ug/L ND 1.0 10/15/15 02:52
Bromobenzene ug/L ND 1.0 10/15/15 02:52
Bromochloromethane ug/L ND 1.0 10/15/15 02:52
Bromodichloromethane ug/L ND 1.0 10/15/15 02:52
Bromoform ug/L ND 1.0 10/15/15 02:52
Bromomethane ug/L ND 2.0 10/15/15 02:52
Carbon tetrachloride ug/L ND 1.0 10/15/15 02:52
Chlorobenzene ug/L ND 1.0 10/15/15 02:52
Chloroethane ug/L ND 1.0 10/15/15 02:52
Chloroform ug/L ND 1.0 10/15/15 02:52
Chloromethane ug/L ND 1.0 10/15/15 02:52
cis-1,2-Dichloroethene ug/L ND 1.0 10/15/15 02:52
cis-1,3-Dichloropropene ug/L ND 1.0 10/15/15 02:52
Dibromochloromethane ug/L ND 1.0 10/15/15 02:52
Dibromomethane ug/L ND 1.0 10/15/15 02:52
Dichlorodifluoromethane ug/L ND 1.0 10/15/15 02:52
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1582957
Associated Lab Samples:92271206001, 92271206002, 92271206003, 92271206008
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 1.0 10/15/15 02:52
Ethylbenzene ug/L ND 1.0 10/15/15 02:52
Hexachloro-1,3-butadiene ug/L ND 1.0 10/15/15 02:52
m&p-Xylene ug/L ND 2.0 10/15/15 02:52
Methyl-tert-butyl ether ug/L ND 1.0 10/15/15 02:52
Methylene Chloride ug/L ND 2.0 10/15/15 02:52
Naphthalene ug/L ND 1.0 10/15/15 02:52
o-Xylene ug/L ND 1.0 10/15/15 02:52
p-Isopropyltoluene ug/L ND 1.0 10/15/15 02:52
Styrene ug/L ND 1.0 10/15/15 02:52
Tetrachloroethene ug/L ND 1.0 10/15/15 02:52
Toluene ug/L ND 1.0 10/15/15 02:52
trans-1,2-Dichloroethene ug/L ND 1.0 10/15/15 02:52
trans-1,3-Dichloropropene ug/L ND 1.0 10/15/15 02:52
Trichloroethene ug/L ND 1.0 10/15/15 02:52
Trichlorofluoromethane ug/L ND 1.0 10/15/15 02:52
Vinyl acetate ug/L ND 2.0 10/15/15 02:52
Vinyl chloride ug/L ND 1.0 10/15/15 02:52
Xylene (Total)ug/L ND 2.0 10/15/15 02:52
1,2-Dichloroethane-d4 (S)%107 70-130 10/15/15 02:52
4-Bromofluorobenzene (S)%103 70-130 10/15/15 02:52
Toluene-d8 (S)%100 70-130 10/15/15 02:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1582958LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 45.950 92 70-130
1,1,1-Trichloroethane ug/L 55.850 112 70-130
1,1,2,2-Tetrachloroethane ug/L 47.450 95 70-130
1,1,2-Trichloroethane ug/L 50.650 101 70-130
1,1-Dichloroethane ug/L 54.050 108 70-130
1,1-Dichloroethene ug/L 55.250 110 70-132
1,1-Dichloropropene ug/L 54.350 109 70-130
1,2,3-Trichlorobenzene ug/L 46.550 93 70-135
1,2,3-Trichloropropane ug/L 49.050 98 70-130
1,2,4-Trichlorobenzene ug/L 47.250 94 70-134
1,2-Dibromo-3-chloropropane ug/L 39.850 80 70-130
1,2-Dibromoethane (EDB)ug/L 49.250 98 70-130
1,2-Dichlorobenzene ug/L 47.250 94 70-130
1,2-Dichloroethane ug/L 52.750 105 70-130
1,2-Dichloropropane ug/L 49.550 99 70-130
1,3-Dichlorobenzene ug/L 49.250 98 70-130
1,3-Dichloropropane ug/L 47.750 95 70-130
1,4-Dichlorobenzene ug/L 48.250 96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1582958LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 49.850 100 58-145
2-Butanone (MEK)ug/L 109100 109 70-145
2-Chlorotoluene ug/L 44.650 89 70-130
2-Hexanone ug/L 94.5100 95 70-144
4-Chlorotoluene ug/L 47.350 95 70-130
4-Methyl-2-pentanone (MIBK)ug/L 110100 110 70-140
Acetone ug/L 126100 126 50-175
Benzene ug/L 51.950 104 70-130
Bromobenzene ug/L 47.450 95 70-130
Bromochloromethane ug/L 56.450 113 70-130
Bromodichloromethane ug/L 48.350 97 70-130
Bromoform ug/L 37.150 74 70-130
Bromomethane ug/L 53.150 106 54-130
Carbon tetrachloride ug/L 50.150 100 70-132
Chlorobenzene ug/L 48.150 96 70-130
Chloroethane ug/L 42.850 86 64-134
Chloroform ug/L 54.450 109 70-130
Chloromethane ug/L 50.750 101 64-130
cis-1,2-Dichloroethene ug/L 53.150 106 70-131
cis-1,3-Dichloropropene ug/L 48.450 97 70-130
Dibromochloromethane ug/L 42.850 86 70-130
Dibromomethane ug/L 53.150 106 70-131
Dichlorodifluoromethane ug/L 49.650 99 56-130
Diisopropyl ether ug/L 58.850 118 70-130
Ethylbenzene ug/L 48.850 98 70-130
Hexachloro-1,3-butadiene ug/L 54.750 109 70-130
m&p-Xylene ug/L 95.6100 96 70-130
Methyl-tert-butyl ether ug/L 54.950 110 70-130
Methylene Chloride ug/L 62.950 126 63-130
Naphthalene ug/L 46.650 93 70-138
o-Xylene ug/L 47.850 96 70-130
p-Isopropyltoluene ug/L 47.750 95 70-130
Styrene ug/L 46.650 93 70-130
Tetrachloroethene ug/L 46.450 93 70-130
Toluene ug/L 51.650 103 70-130
trans-1,2-Dichloroethene ug/L 53.450 107 70-130
trans-1,3-Dichloropropene ug/L 47.950 96 70-132
Trichloroethene ug/L 51.150 102 70-130
Trichlorofluoromethane ug/L 60.150 120 62-133
Vinyl acetate ug/L 113100 113 66-157
Vinyl chloride ug/L 51.950 104 50-150
Xylene (Total)ug/L 143150 96 70-130
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%106 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1582959MATRIX SPIKE SAMPLE:
MSSpike
Result
92271232011
1,1,1,2-Tetrachloroethane ug/L 18.320 92 70-130ND
1,1,1-Trichloroethane ug/L 24.220 121 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.020 95 70-130ND
1,1,2-Trichloroethane ug/L 21.620 108 70-130ND
1,1-Dichloroethane ug/L 23.420 117 70-130ND
1,1-Dichloroethene ug/L 24.720 124 70-166ND
1,1-Dichloropropene ug/L 23.920 120 70-130ND
1,2,3-Trichlorobenzene ug/L 18.820 94 70-130ND
1,2,3-Trichloropropane ug/L 19.820 99 70-130ND
1,2,4-Trichlorobenzene ug/L 19.420 97 70-130ND
1,2-Dibromo-3-chloropropane ug/L 14.120 70 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.920 99 70-130ND
1,2-Dichlorobenzene ug/L 19.420 97 70-130ND
1,2-Dichloroethane ug/L 22.620 112 70-130ND
1,2-Dichloropropane ug/L 21.120 105 70-130ND
1,3-Dichlorobenzene ug/L 20.320 102 70-130ND
1,3-Dichloropropane ug/L 20.020 100 70-130ND
1,4-Dichlorobenzene ug/L 20.020 100 70-130ND
2,2-Dichloropropane ug/L 21.820 109 70-130ND
2-Butanone (MEK)ug/L 53.540 115 70-1307.6
2-Chlorotoluene ug/L 18.320 92 70-130ND
2-Hexanone ug/L 37.840 94 70-130ND
4-Chlorotoluene ug/L 19.620 98 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 44.140 110 70-130ND
Acetone ug/L 93.5 M14014870-13034.5
Benzene ug/L 28.220 113 70-1485.6
Bromobenzene ug/L 20.120 101 70-130ND
Bromochloromethane ug/L 24.020 120 70-130ND
Bromodichloromethane ug/L 19.220 96 70-130ND
Bromoform ug/L 13.4 M1206770-130ND
Bromomethane ug/L 23.220 116 70-130ND
Carbon tetrachloride ug/L 21.320 106 70-130ND
Chlorobenzene ug/L 20.420 102 70-146ND
Chloroethane ug/L 20.520 103 70-130ND
Chloroform ug/L 23.620 118 70-130ND
Chloromethane ug/L 22.620 111 70-130ND
cis-1,2-Dichloroethene ug/L 23.220 116 70-130ND
cis-1,3-Dichloropropene ug/L 19.720 98 70-130ND
Dibromochloromethane ug/L 15.720 79 70-130ND
Dibromomethane ug/L 22.420 112 70-130ND
Dichlorodifluoromethane ug/L 22.120 111 70-130ND
Diisopropyl ether ug/L 35.420 126 70-13010.3
Ethylbenzene ug/L 20.620 103 70-130ND
Hexachloro-1,3-butadiene ug/L 24.620 123 70-130ND
m&p-Xylene ug/L 40.640 101 70-130ND
Methyl-tert-butyl ether ug/L 25.920 117 70-1302.5
Methylene Chloride ug/L 24.120 121 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 35 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1582959MATRIX SPIKE SAMPLE:
MSSpike
Result
92271232011
Naphthalene ug/L 18.820 94 70-130ND
o-Xylene ug/L 20.120 101 70-130ND
p-Isopropyltoluene ug/L 71.920 105 70-13051.0
Styrene ug/L 19.620 98 70-130ND
Tetrachloroethene ug/L 19.820 99 70-130ND
Toluene ug/L 22.620 112 70-155ND
trans-1,2-Dichloroethene ug/L 23.720 118 70-130ND
trans-1,3-Dichloropropene ug/L 19.020 95 70-130ND
Trichloroethene ug/L 22.420 112 69-151ND
Trichlorofluoromethane ug/L 26.6 M12013370-130ND
Vinyl acetate ug/L 40.940 102 70-130ND
Vinyl chloride ug/L 23.620 118 70-130ND
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%105 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92271276001
1582960SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Chlorotoluene ug/L NDND
2-Hexanone ug/L NDND
4-Chlorotoluene ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Benzene ug/L NDND
REPORT OF LABORATORY ANALYSIS
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Page 36 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92271276001
1582960SAMPLE DUPLICATE:
Bromobenzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L .29JND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Diisopropyl ether ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
m&p-Xylene ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylene Chloride ug/L NDND
Naphthalene ug/L NDND
o-Xylene ug/L NDND
p-Isopropyltoluene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%111 0111
4-Bromofluorobenzene (S)%105 0105
Toluene-d8 (S)%100 0100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
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Page 37 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/33823
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92271206009
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1583833LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.450 93 70-130
1,1,1-Trichloroethane ug/L 48.750 97 70-130
1,1,2,2-Tetrachloroethane ug/L 48.150 96 70-130
1,1,2-Trichloroethane ug/L 46.750 93 70-130
1,1-Dichloroethane ug/L 47.650 95 70-130
1,1-Dichloroethene ug/L 49.550 99 70-132
1,1-Dichloropropene ug/L 48.250 96 70-130
1,2,3-Trichlorobenzene ug/L 48.950 98 70-135
1,2,3-Trichloropropane ug/L 48.550 97 70-130
1,2,4-Trichlorobenzene ug/L 49.950 100 70-134
1,2-Dibromo-3-chloropropane ug/L 41.950 84 70-130
1,2-Dibromoethane (EDB)ug/L 49.750 99 70-130
1,2-Dichlorobenzene ug/L 50.750 101 70-130
1,2-Dichloroethane ug/L 46.550 93 70-130
1,2-Dichloropropane ug/L 46.050 92 70-130
1,3-Dichlorobenzene ug/L 51.750 103 70-130
1,3-Dichloropropane ug/L 48.050 96 70-130
1,4-Dichlorobenzene ug/L 51.350 103 70-130
2,2-Dichloropropane ug/L 49.250 98 58-145
2-Butanone (MEK)ug/L 96.8100 97 70-145
2-Chlorotoluene ug/L 48.650 97 70-130
2-Hexanone ug/L 97.2100 97 70-144
4-Chlorotoluene ug/L 49.350 99 70-130
4-Methyl-2-pentanone (MIBK)ug/L 103100 103 70-140
Acetone ug/L 111100 111 50-175
Benzene ug/L 48.850 98 70-130
Bromobenzene ug/L 49.450 99 70-130
Bromochloromethane ug/L 48.550 97 70-130
Bromodichloromethane ug/L 44.950 90 70-130
Bromoform ug/L 37.150 74 70-130
Bromomethane ug/L 48.450 97 54-130
Carbon tetrachloride ug/L 47.950 96 70-132
Chlorobenzene ug/L 48.650 97 70-130
Chloroethane ug/L 38.250 76 64-134
Chloroform ug/L 47.850 96 70-130
Chloromethane ug/L 46.250 92 64-130
cis-1,2-Dichloroethene ug/L 46.950 94 70-131
cis-1,3-Dichloropropene ug/L 46.150 92 70-130
Dibromochloromethane ug/L 42.950 86 70-130
Dibromomethane ug/L 49.950 100 70-131
Dichlorodifluoromethane ug/L 44.650 89 56-130
Diisopropyl ether ug/L 53.150 106 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
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Page 38 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1583833LABORATORY CONTROL SAMPLE:
LCSSpike
Ethylbenzene ug/L 49.250 98 70-130
Hexachloro-1,3-butadiene ug/L 58.750 117 70-130
m&p-Xylene ug/L 97.2100 97 70-130
Methyl-tert-butyl ether ug/L 49.650 99 70-130
Methylene Chloride ug/L 54.750 109 63-130
Naphthalene ug/L 48.250 96 70-138
o-Xylene ug/L 48.750 97 70-130
p-Isopropyltoluene ug/L 52.050 104 70-130
Styrene ug/L 47.650 95 70-130
Tetrachloroethene ug/L 47.150 94 70-130
Toluene ug/L 48.650 97 70-130
trans-1,2-Dichloroethene ug/L 47.450 95 70-130
trans-1,3-Dichloropropene ug/L 45.350 91 70-132
Trichloroethene ug/L 48.050 96 70-130
Trichlorofluoromethane ug/L 53.650 107 62-133
Vinyl acetate ug/L 101100 101 66-157
Vinyl chloride ug/L 47.950 96 50-150
Xylene (Total)ug/L 146150 97 70-130
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1583834MATRIX SPIKE SAMPLE:
MSSpike
Result
92271206009
1,1,1,2-Tetrachloroethane ug/L 17.920 90 70-130ND
1,1,1-Trichloroethane ug/L 20.920 104 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.320 97 70-130ND
1,1,2-Trichloroethane ug/L 19.020 95 70-130ND
1,1-Dichloroethane ug/L 20.720 104 70-130ND
1,1-Dichloroethene ug/L 23.720 107 70-1662.3
1,1-Dichloropropene ug/L 20.420 102 70-130ND
1,2,3-Trichlorobenzene ug/L 15.620 78 70-130ND
1,2,3-Trichloropropane ug/L 20.620 103 70-130ND
1,2,4-Trichlorobenzene ug/L 16.020 80 70-130ND
1,2-Dibromo-3-chloropropane ug/L 14.020 70 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.720 103 70-130ND
1,2-Dichlorobenzene ug/L 19.720 98 70-130ND
1,2-Dichloroethane ug/L 20.620 99 70-130ND
1,2-Dichloropropane ug/L 19.120 95 70-130ND
1,3-Dichlorobenzene ug/L 20.320 101 70-130ND
1,3-Dichloropropane ug/L 20.020 100 70-130ND
1,4-Dichlorobenzene ug/L 20.320 102 70-130ND
2,2-Dichloropropane ug/L 18.220 91 70-130ND
2-Butanone (MEK)ug/L 37.940 95 70-130ND
REPORT OF LABORATORY ANALYSIS
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Page 39 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1583834MATRIX SPIKE SAMPLE:
MSSpike
Result
92271206009
2-Chlorotoluene ug/L 20.720 104 70-130ND
2-Hexanone ug/L 38.340 96 70-130ND
4-Chlorotoluene ug/L 20.120 101 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 40.840 102 70-130ND
Acetone ug/L 37.440 93 70-130ND
Benzene ug/L 20.620 103 70-148ND
Bromobenzene ug/L 20.320 102 70-130ND
Bromochloromethane ug/L 20.920 105 70-130ND
Bromodichloromethane ug/L 17.120 86 70-130ND
Bromoform ug/L 11.9 M1206070-130ND
Bromomethane ug/L 13.6 M1206870-130ND
Carbon tetrachloride ug/L 18.520 92 70-130ND
Chlorobenzene ug/L 21.020 105 70-146ND
Chloroethane ug/L 17.520 88 70-130ND
Chloroform ug/L 21.320 103 70-130ND
Chloromethane ug/L 19.220 96 70-130ND
cis-1,2-Dichloroethene ug/L 58.120 100 70-13038.1
cis-1,3-Dichloropropene ug/L 16.520 83 70-130ND
Dibromochloromethane ug/L 15.020 75 70-130ND
Dibromomethane ug/L 19.920 99 70-130ND
Dichlorodifluoromethane ug/L 20.320 101 70-130ND
Diisopropyl ether ug/L 21.920 109 70-130ND
Ethylbenzene ug/L 20.720 103 70-130ND
Hexachloro-1,3-butadiene ug/L 17.820 89 70-130ND
m&p-Xylene ug/L 40.940 102 70-130ND
Methyl-tert-butyl ether ug/L 20.120 100 70-130ND
Methylene Chloride ug/L 20.620 103 70-130ND
Naphthalene ug/L 16.820 83 70-130ND
o-Xylene ug/L 19.920 100 70-130ND
p-Isopropyltoluene ug/L 18.220 91 70-130ND
Styrene ug/L 18.420 92 70-130ND
Tetrachloroethene ug/L 18720 102 70-130166
Toluene ug/L 20.420 102 70-155ND
trans-1,2-Dichloroethene ug/L 20.520 101 70-130ND
trans-1,3-Dichloropropene ug/L 16.520 83 70-130ND
Trichloroethene ug/L 97.420 100 69-15177.5
Trichlorofluoromethane ug/L 24.320 122 70-130ND
Vinyl acetate ug/L 35.340 88 70-130ND
Vinyl chloride ug/L 20.120 100 70-130ND
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
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[phone]
Page 40 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92271232018
1583835SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Chlorotoluene ug/L NDND
2-Hexanone ug/L NDND
4-Chlorotoluene ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Benzene ug/L NDND
Bromobenzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Diisopropyl ether ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
m&p-Xylene ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylene Chloride ug/L NDND
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 41 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92271232018
1583835SAMPLE DUPLICATE:
Naphthalene ug/L NDND
o-Xylene ug/L NDND
p-Isopropyltoluene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%107 1106
4-Bromofluorobenzene (S)%100 0101
Toluene-d8 (S)%97 097
REPORT OF LABORATORY ANALYSIS
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Page 42 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/33754
EPA 8260B Mod.
EPA 8260B Mod.
8260 MSV SIM
Associated Lab Samples:92271206001, 92271206002, 92271206003, 92271206004, 92271206005, 92271206006, 92271206007,
92271206008, 92271206009, 92271206010, 92271206011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1580447
Associated Lab Samples:92271206001, 92271206002, 92271206003, 92271206004, 92271206005, 92271206006, 92271206007,
92271206008, 92271206009, 92271206010, 92271206011
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 10/12/15 13:44
1,2-Dichloroethane-d4 (S)%109 50-150 10/12/15 13:44
Toluene-d8 (S)%126 50-150 10/12/15 13:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1580448LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 24.120 120 71-125
1,2-Dichloroethane-d4 (S)%105 50-150
Toluene-d8 (S)%126 50-150
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1580449MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92271206005
1580450
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 112 50-150120 720ND22.4 24.0
1,2-Dichloroethane-d4 (S)%105 50-150103
Toluene-d8 (S)%123 50-150123
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
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Page 43 of 47
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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Page 44 of 47
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92271206
SUNBELT TURRENT 71157718
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92271206001 MSV/33803MW-4 EPA 8260
92271206002 MSV/33803MW-2 EPA 8260
92271206003 MSV/33803MW-3 EPA 8260
92271206004 MSV/33783MW-5 EPA 8260
92271206005 MSV/33783MW-6 EPA 8260
92271206006 MSV/33783MW-7 EPA 8260
92271206007 MSV/33783MW-8 EPA 8260
92271206008 MSV/33803DW-1 EPA 8260
92271206009 MSV/33823DUP-01-1008 2015 EPA 8260
92271206010 MSV/33753EB-01-1008 2016 EPA 8260
92271206011 MSV/33753Trip Blank EPA 8260
92271206001 MSV/33754MW-4 EPA 8260B Mod.
92271206002 MSV/33754MW-2 EPA 8260B Mod.
92271206003 MSV/33754MW-3 EPA 8260B Mod.
92271206004 MSV/33754MW-5 EPA 8260B Mod.
92271206005 MSV/33754MW-6 EPA 8260B Mod.
92271206006 MSV/33754MW-7 EPA 8260B Mod.
92271206007 MSV/33754MW-8 EPA 8260B Mod.
92271206008 MSV/33754DW-1 EPA 8260B Mod.
92271206009 MSV/33754DUP-01-1008 2015 EPA 8260B Mod.
92271206010 MSV/33754EB-01-1008 2016 EPA 8260B Mod.
92271206011 MSV/33754Trip Blank EPA 8260B Mod.
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/16/2015 04:30 PM
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Page 45 of 47
Page 46 of 47
Page 47 of 47
#=CL#
September 03, 2015
LIMS USE: FR - ANALEE FARRELL
LIMS OBJECT ID: 92265398
92265398
Project:
Pace Project No.:
RE:
Analee Farrell
Terracon
2020 Starita Rd
Suite E
Charlotte, NC 28206
Atando Ave 71157718
Dear Analee Farrell:
Enclosed are the analytical results for sample(s) received by the laboratory on August 27, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 1 of 46
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 2 of 46
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Lab ID Sample ID Matrix Date Collected Date Received
92265398001 MW-9 10'-15'Solid 08/26/15 11:35 08/27/15 12:49
92265398002 MW-10 15'-18'Solid 08/26/15 12:45 08/27/15 12:49
92265398003 SB-1 5'-7'Solid 08/26/15 16:20 08/27/15 12:49
92265398004 SB-2 5'-7'Solid 08/26/15 16:30 08/27/15 12:49
92265398005 SB-3 5'-7'Solid 08/26/15 16:35 08/27/15 12:49
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 46
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92265398001 MW-9 10'-15'EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92265398002 MW-10 15'-18'EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92265398003 SB-1 5'-7'EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92265398004 SB-2 5'-7'EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92265398005 SB-3 5'-7'EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 46
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92265398001 MW-9 10'-15'
Acetone 27.3J ug/kg 08/31/15 21:5381.1EPA 8260
cis-1,2-Dichloroethene 68.1 ug/kg 08/31/15 21:534.1EPA 8260
Methylene Chloride 7.0J ug/kg 08/31/15 21:53 B16.2EPA 8260
Tetrachloroethene 201 ug/kg 09/01/15 15:04120EPA 8260
Trichloroethene 449 ug/kg 09/01/15 15:04120EPA 8260
Percent Moisture 17.8 %08/28/15 19:380.10ASTM D2974-87
92265398002 MW-10 15'-18'
Acetone 15.6J ug/kg 08/31/15 22:1388.7EPA 8260
Methylene Chloride 5.2J ug/kg 08/31/15 22:13 B17.7EPA 8260
Percent Moisture 15.7 %08/28/15 19:380.10ASTM D2974-87
92265398003 SB-1 5'-7'
Anthracene 128J ug/kg 09/02/15 20:07388EPA 8270
Benzo(a)anthracene 461 ug/kg 09/02/15 20:07388EPA 8270
Benzo(a)pyrene 401 ug/kg 09/02/15 20:07388EPA 8270
Benzo(b)fluoranthene 638 ug/kg 09/02/15 20:07388EPA 8270
Benzo(g,h,i)perylene 263J ug/kg 09/02/15 20:07388EPA 8270
Benzo(k)fluoranthene 286J ug/kg 09/02/15 20:07388EPA 8270
Chrysene 450 ug/kg 09/02/15 20:07 B388EPA 8270
Dibenz(a,h)anthracene 85.0J ug/kg 09/02/15 20:07388EPA 8270
Fluoranthene 1020 ug/kg 09/02/15 20:07388EPA 8270
Fluorene 181J ug/kg 09/02/15 20:07388EPA 8270
Indeno(1,2,3-cd)pyrene 230J ug/kg 09/02/15 20:07388EPA 8270
1-Methylnaphthalene 1090 ug/kg 09/02/15 20:07388EPA 8270
2-Methylnaphthalene 1620 ug/kg 09/02/15 20:07388EPA 8270
Naphthalene 1350 ug/kg 09/02/15 20:07388EPA 8270
N-Nitrosodiphenylamine 372J ug/kg 09/02/15 20:07388EPA 8270
Phenanthrene 569 ug/kg 09/02/15 20:07388EPA 8270
Pyrene 741 ug/kg 09/02/15 20:07388EPA 8270
n-Butylbenzene 1520 ug/kg 08/31/15 22:33123EPA 8260
sec-Butylbenzene 827 ug/kg 08/31/15 22:33123EPA 8260
tert-Butylbenzene 208 ug/kg 08/31/15 22:33123EPA 8260
Ethylbenzene 465 ug/kg 08/31/15 22:33123EPA 8260
Isopropylbenzene (Cumene)2520 ug/kg 08/31/15 22:33123EPA 8260
p-Isopropyltoluene 1120 ug/kg 08/31/15 22:33123EPA 8260
Naphthalene 2760 ug/kg 08/31/15 22:33123EPA 8260
n-Propylbenzene 6360 ug/kg 09/02/15 12:57246EPA 8260
Toluene 139 ug/kg 08/31/15 22:33123EPA 8260
1,2,4-Trimethylbenzene 187 ug/kg 08/31/15 22:33123EPA 8260
1,3,5-Trimethylbenzene 65.4J ug/kg 08/31/15 22:33123EPA 8260
Xylene (Total)1010 ug/kg 08/31/15 22:33246EPA 8260
m&p-Xylene 1010 ug/kg 08/31/15 22:33246EPA 8260
o-Xylene 96.1J ug/kg 08/31/15 22:33123EPA 8260
Percent Moisture 14.9 %08/28/15 19:380.10ASTM D2974-87
92265398004 SB-2 5'-7'
Benzo(a)anthracene 109J ug/kg 09/02/15 20:35406EPA 8270
Benzo(a)pyrene 91.2J ug/kg 09/02/15 20:35406EPA 8270
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 46
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92265398004 SB-2 5'-7'
Benzo(b)fluoranthene 159J ug/kg 09/02/15 20:35406EPA 8270
Chrysene 109J ug/kg 09/02/15 20:35 B406EPA 8270
Fluoranthene 241J ug/kg 09/02/15 20:35406EPA 8270
Phenanthrene 115J ug/kg 09/02/15 20:35406EPA 8270
Pyrene 175J ug/kg 09/02/15 20:35406EPA 8270
n-Butylbenzene 5.8 ug/kg 08/31/15 22:525.7EPA 8260
sec-Butylbenzene 6.3 ug/kg 08/31/15 22:525.7EPA 8260
cis-1,2-Dichloroethene 15.3 ug/kg 08/31/15 22:525.7EPA 8260
Naphthalene 5.0J ug/kg 08/31/15 22:52 B5.7EPA 8260
n-Propylbenzene 2.9J ug/kg 08/31/15 22:525.7EPA 8260
Vinyl chloride 2.2J ug/kg 08/31/15 22:5211.4EPA 8260
Percent Moisture 18.8 %08/28/15 19:380.10ASTM D2974-87
92265398005 SB-3 5'-7'
Acenaphthene 1580J ug/kg 09/03/15 14:384520EPA 8270
Anthracene 2970J ug/kg 09/03/15 14:384520EPA 8270
Benzo(a)anthracene 9720 ug/kg 09/03/15 14:384520EPA 8270
Benzo(a)pyrene 8830 ug/kg 09/03/15 14:384520EPA 8270
Benzo(b)fluoranthene 13300 ug/kg 09/03/15 14:384520EPA 8270
Benzo(g,h,i)perylene 5820 ug/kg 09/03/15 14:384520EPA 8270
Benzo(k)fluoranthene 7200 ug/kg 09/03/15 14:384520EPA 8270
Chrysene 9410 ug/kg 09/03/15 14:384520EPA 8270
Dibenz(a,h)anthracene 1770J ug/kg 09/03/15 14:384520EPA 8270
Dibenzofuran 782J ug/kg 09/03/15 14:384520EPA 8270
Fluoranthene 22400 ug/kg 09/03/15 14:384520EPA 8270
Fluorene 1590J ug/kg 09/03/15 14:384520EPA 8270
Indeno(1,2,3-cd)pyrene 5310 ug/kg 09/03/15 14:384520EPA 8270
Phenanthrene 13300 ug/kg 09/03/15 14:384520EPA 8270
Pyrene 16200 ug/kg 09/03/15 14:384520EPA 8270
n-Butylbenzene 160J ug/kg 08/31/15 23:12287EPA 8260
sec-Butylbenzene 176J ug/kg 08/31/15 23:12287EPA 8260
Isopropylbenzene (Cumene)115J ug/kg 08/31/15 23:12287EPA 8260
Methylene Chloride 220J ug/kg 08/31/15 23:12 B1150EPA 8260
Naphthalene 612 ug/kg 08/31/15 23:12 B287EPA 8260
n-Propylbenzene 326 ug/kg 08/31/15 23:12287EPA 8260
1,2,4-Trimethylbenzene 181J ug/kg 08/31/15 23:12287EPA 8260
Percent Moisture 26.9 %08/28/15 19:390.10ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 46
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Method:
Client:Terracon NC
EPA 8270
Date:September 03, 2015
Description:8270 MSSV Microwave
General Information:
5 samples were analyzed for EPA 8270. All samples were received in acceptable condition with any exceptions noted below or on the
chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3546 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: OEXT/37442
S4: Surrogate recovery not evaluated against control limits due to sample dilution.
• SB-3 5'-7' (Lab ID: 92265398005)
• 2,4,6-Tribromophenol (S)
• 2-Fluorobiphenyl (S)
• 2-Fluorophenol (S)
• Nitrobenzene-d5 (S)
• Phenol-d6 (S)
• Terphenyl-d14 (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
QC Batch: OEXT/37442
B: Analyte was detected in the associated method blank.
• BLANK for HBN 279032 [OEXT/374 (Lab ID: 1545554)
• Chrysene
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 46
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Method:
Client:Terracon NC
EPA 8270
Date:September 03, 2015
Description:8270 MSSV Microwave
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: OEXT/37442
D3: Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.
• SB-3 5'-7' (Lab ID: 92265398005)
• Nitrobenzene-d5 (S)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 46
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Method:
Client:Terracon NC
EPA 8260
Date:September 03, 2015
Description:8260/5035A Volatile Organics
General Information:
5 samples were analyzed for EPA 8260. All samples were received in acceptable condition with any exceptions noted below or on the
chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: MSV/33184
S2: Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample re-
analysis).
• SB-1 5'-7' (Lab ID: 92265398003)
• 1,2-Dichloroethane-d4 (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
QC Batch: MSV/33184
B: Analyte was detected in the associated method blank.
• BLANK for HBN 278958 [MSV/3318 (Lab ID: 1545121)
• Methylene Chloride
• Naphthalene
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 46
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Method:
Client:Terracon NC
EPA 8260
Date:September 03, 2015
Description:8260/5035A Volatile Organics
Analyte Comments:
QC Batch: MSV/33184
D3: Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.
• SB-3 5'-7' (Lab ID: 92265398005)
• Toluene-d8 (S)
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:MW-9 10'-15'Lab ID:92265398001 Collected:08/26/15 11:35 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 09/02/15 19:12 83-32-908/31/15 17:3040292.5 1
Acenaphthylene ND ug/kg 09/02/15 19:12 208-96-808/31/15 17:3040294.9 1
Aniline ND ug/kg 09/02/15 19:12 62-53-308/31/15 17:304021081
Anthracene ND ug/kg 09/02/15 19:12 120-12-708/31/15 17:3040290.0 1
Benzo(a)anthracene ND ug/kg 09/02/15 19:12 56-55-308/31/15 17:3040274.2 1
Benzo(a)pyrene ND ug/kg 09/02/15 19:12 50-32-808/31/15 17:3040276.7 1
Benzo(b)fluoranthene ND ug/kg 09/02/15 19:12 205-99-208/31/15 17:3040269.4 1
Benzo(g,h,i)perylene ND ug/kg 09/02/15 19:12 191-24-208/31/15 17:304021021
Benzo(k)fluoranthene ND ug/kg 09/02/15 19:12 207-08-908/31/15 17:3040279.1 1
Benzoic Acid ND ug/kg 09/02/15 19:12 65-85-008/31/15 17:30201073.0 1
Benzyl alcohol ND ug/kg 09/02/15 19:12 100-51-608/31/15 17:3080380.3 1
4-Bromophenylphenyl ether ND ug/kg 09/02/15 19:12 101-55-308/31/15 17:3040273.0 1
Butylbenzylphthalate ND ug/kg 09/02/15 19:12 85-68-708/31/15 17:3040285.2 1
4-Chloro-3-methylphenol ND ug/kg 09/02/15 19:12 59-50-708/31/15 17:3080382.7 1
4-Chloroaniline ND ug/kg 09/02/15 19:12 106-47-808/31/15 17:3020101121
bis(2-Chloroethoxy)methane ND ug/kg 09/02/15 19:12 111-91-108/31/15 17:3040293.7 1
bis(2-Chloroethyl) ether ND ug/kg 09/02/15 19:12 111-44-408/31/15 17:304021021
bis(2-Chloroisopropyl) ether ND ug/kg 09/02/15 19:12 108-60-108/31/15 17:304021071
2-Chloronaphthalene ND ug/kg 09/02/15 19:12 91-58-708/31/15 17:3040279.1 1
2-Chlorophenol ND ug/kg 09/02/15 19:12 95-57-808/31/15 17:304021101
4-Chlorophenylphenyl ether ND ug/kg 09/02/15 19:12 7005-72-308/31/15 17:3040282.7 1
Chrysene ND ug/kg 09/02/15 19:12 218-01-908/31/15 17:3040253.5 1
Dibenz(a,h)anthracene ND ug/kg 09/02/15 19:12 53-70-308/31/15 17:3040285.2 1
Dibenzofuran ND ug/kg 09/02/15 19:12 132-64-908/31/15 17:3040265.7 1
1,2-Dichlorobenzene ND ug/kg 09/02/15 19:12 95-50-108/31/15 17:304021071
1,3-Dichlorobenzene ND ug/kg 09/02/15 19:12 541-73-108/31/15 17:3040291.3 1
1,4-Dichlorobenzene ND ug/kg 09/02/15 19:12 106-46-708/31/15 17:304021131
3,3'-Dichlorobenzidine ND ug/kg 09/02/15 19:12 91-94-108/31/15 17:30201087.6 1
2,4-Dichlorophenol ND ug/kg 09/02/15 19:12 120-83-208/31/15 17:3040287.6 1
Diethylphthalate ND ug/kg 09/02/15 19:12 84-66-208/31/15 17:3040262.1 1
2,4-Dimethylphenol ND ug/kg 09/02/15 19:12 105-67-908/31/15 17:304021581
Dimethylphthalate ND ug/kg 09/02/15 19:12 131-11-308/31/15 17:3040281.5 1
Di-n-butylphthalate ND ug/kg 09/02/15 19:12 84-74-208/31/15 17:3040265.7 1
4,6-Dinitro-2-methylphenol ND ug/kg 09/02/15 19:12 534-52-108/31/15 17:3080380.3 1
2,4-Dinitrophenol ND ug/kg 09/02/15 19:12 51-28-508/31/15 17:30201065.7 1
2,4-Dinitrotoluene ND ug/kg 09/02/15 19:12 121-14-208/31/15 17:3040275.4 1
2,6-Dinitrotoluene ND ug/kg 09/02/15 19:12 606-20-208/31/15 17:3040284.0 1
Di-n-octylphthalate ND ug/kg 09/02/15 19:12 117-84-008/31/15 17:3040284.0 1
bis(2-Ethylhexyl)phthalate ND ug/kg 09/02/15 19:12 117-81-708/31/15 17:304021101
Fluoranthene ND ug/kg 09/02/15 19:12 206-44-008/31/15 17:3040258.4 1
Fluorene ND ug/kg 09/02/15 19:12 86-73-708/31/15 17:3040282.7 1
Hexachloro-1,3-butadiene ND ug/kg 09/02/15 19:12 87-68-308/31/15 17:3040269.4 1
Hexachlorobenzene ND ug/kg 09/02/15 19:12 118-74-108/31/15 17:3040251.1 1
Hexachlorocyclopentadiene ND ug/kg 09/02/15 19:12 77-47-408/31/15 17:3040274.2 1
Hexachloroethane ND ug/kg 09/02/15 19:12 67-72-108/31/15 17:304021061
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:MW-9 10'-15'Lab ID:92265398001 Collected:08/26/15 11:35 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Indeno(1,2,3-cd)pyrene ND ug/kg 09/02/15 19:12 193-39-508/31/15 17:3040282.7 1
Isophorone ND ug/kg 09/02/15 19:12 78-59-108/31/15 17:3040290.0 1
1-Methylnaphthalene ND ug/kg 09/02/15 19:12 90-12-008/31/15 17:304021051
2-Methylnaphthalene ND ug/kg 09/02/15 19:12 91-57-608/31/15 17:3040286.4 1
2-Methylphenol(o-Cresol)ND ug/kg 09/02/15 19:12 95-48-708/31/15 17:304021221
3&4-Methylphenol(m&p Cresol)ND ug/kg 09/02/15 19:1208/31/15 17:304021581
Naphthalene ND ug/kg 09/02/15 19:12 91-20-308/31/15 17:3040298.6 1
2-Nitroaniline ND ug/kg 09/02/15 19:12 88-74-408/31/15 17:3020101241
3-Nitroaniline ND ug/kg 09/02/15 19:12 99-09-208/31/15 17:3020101101
4-Nitroaniline ND ug/kg 09/02/15 19:12 100-01-608/31/15 17:308031131
Nitrobenzene ND ug/kg 09/02/15 19:12 98-95-308/31/15 17:304021101
2-Nitrophenol ND ug/kg 09/02/15 19:12 88-75-508/31/15 17:3040297.3 1
4-Nitrophenol ND ug/kg 09/02/15 19:12 100-02-708/31/15 17:30201071.8 1
N-Nitrosodimethylamine ND ug/kg 09/02/15 19:12 62-75-908/31/15 17:304021301
N-Nitroso-di-n-propylamine ND ug/kg 09/02/15 19:12 621-64-708/31/15 17:3040276.7 1
N-Nitrosodiphenylamine ND ug/kg 09/02/15 19:12 86-30-608/31/15 17:304021191
Pentachlorophenol ND ug/kg 09/02/15 19:12 87-86-508/31/15 17:30201073.0 1
Phenanthrene ND ug/kg 09/02/15 19:12 85-01-808/31/15 17:3040266.9 1
Phenol ND ug/kg 09/02/15 19:12 108-95-208/31/15 17:304021201
Pyrene ND ug/kg 09/02/15 19:12 129-00-008/31/15 17:3040268.1 1
1,2,4-Trichlorobenzene ND ug/kg 09/02/15 19:12 120-82-108/31/15 17:3040277.9 1
2,4,5-Trichlorophenol ND ug/kg 09/02/15 19:12 95-95-408/31/15 17:304021241
2,4,6-Trichlorophenol ND ug/kg 09/02/15 19:12 88-06-208/31/15 17:3040288.8 1
Surrogates
Nitrobenzene-d5 (S)43 %09/02/15 19:12 4165-60-008/31/15 17:3023-110 1
2-Fluorobiphenyl (S)49 %09/02/15 19:12 321-60-808/31/15 17:3030-110 1
Terphenyl-d14 (S)77 %09/02/15 19:12 1718-51-008/31/15 17:3028-110 1
Phenol-d6 (S)59 %09/02/15 19:12 13127-88-308/31/15 17:3022-110 1
2-Fluorophenol (S)56 %09/02/15 19:12 367-12-408/31/15 17:3013-110 1
2,4,6-Tribromophenol (S)73 %09/02/15 19:12 118-79-608/31/15 17:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 27.3J ug/kg 08/31/15 21:53 67-64-181.1 8.1 1
Benzene ND ug/kg 08/31/15 21:53 71-43-24.1 1.3 1
Bromobenzene ND ug/kg 08/31/15 21:53 108-86-14.1 1.6 1
Bromochloromethane ND ug/kg 08/31/15 21:53 74-97-54.1 1.4 1
Bromodichloromethane ND ug/kg 08/31/15 21:53 75-27-44.1 1.5 1
Bromoform ND ug/kg 08/31/15 21:53 75-25-24.1 1.9 1
Bromomethane ND ug/kg 08/31/15 21:53 74-83-98.1 2.0 1
2-Butanone (MEK)ND ug/kg 08/31/15 21:53 78-93-381.1 2.4 1
n-Butylbenzene ND ug/kg 08/31/15 21:53 104-51-84.1 1.5 1
sec-Butylbenzene ND ug/kg 08/31/15 21:53 135-98-84.1 1.3 1
tert-Butylbenzene ND ug/kg 08/31/15 21:53 98-06-64.1 1.6 1
Carbon tetrachloride ND ug/kg 08/31/15 21:53 56-23-54.1 2.1 1
Chlorobenzene ND ug/kg 08/31/15 21:53 108-90-74.1 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:MW-9 10'-15'Lab ID:92265398001 Collected:08/26/15 11:35 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloroethane ND ug/kg 08/31/15 21:53 75-00-38.1 1.9 1
Chloroform ND ug/kg 08/31/15 21:53 67-66-34.1 1.3 1
Chloromethane ND ug/kg 08/31/15 21:53 74-87-38.1 1.9 1
2-Chlorotoluene ND ug/kg 08/31/15 21:53 95-49-84.1 1.4 1
4-Chlorotoluene ND ug/kg 08/31/15 21:53 106-43-44.1 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/31/15 21:53 96-12-84.1 2.9 1
Dibromochloromethane ND ug/kg 08/31/15 21:53 124-48-14.1 1.5 1
1,2-Dibromoethane (EDB)ND ug/kg 08/31/15 21:53 106-93-44.1 1.5 1
Dibromomethane ND ug/kg 08/31/15 21:53 74-95-34.1 2.0 1
1,2-Dichlorobenzene ND ug/kg 08/31/15 21:53 95-50-14.1 1.5 1
1,3-Dichlorobenzene ND ug/kg 08/31/15 21:53 541-73-14.1 1.6 1
1,4-Dichlorobenzene ND ug/kg 08/31/15 21:53 106-46-74.1 1.4 1
Dichlorodifluoromethane ND ug/kg 08/31/15 21:53 75-71-88.1 2.9 1
1,1-Dichloroethane ND ug/kg 08/31/15 21:53 75-34-34.1 1.2 1
1,2-Dichloroethane ND ug/kg 08/31/15 21:53 107-06-24.1 1.8 1
1,1-Dichloroethene ND ug/kg 08/31/15 21:53 75-35-44.1 1.5 1
cis-1,2-Dichloroethene 68.1 ug/kg 08/31/15 21:53 156-59-24.1 1.1 1
trans-1,2-Dichloroethene ND ug/kg 08/31/15 21:53 156-60-54.1 1.5 1
1,2-Dichloropropane ND ug/kg 08/31/15 21:53 78-87-54.1 1.4 1
1,3-Dichloropropane ND ug/kg 08/31/15 21:53 142-28-94.1 1.5 1
2,2-Dichloropropane ND ug/kg 08/31/15 21:53 594-20-74.1 1.4 1
1,1-Dichloropropene ND ug/kg 08/31/15 21:53 563-58-64.1 1.2 1
cis-1,3-Dichloropropene ND ug/kg 08/31/15 21:53 10061-01-54.1 1.5 1
trans-1,3-Dichloropropene ND ug/kg 08/31/15 21:53 10061-02-64.1 1.2 1
Diisopropyl ether ND ug/kg 08/31/15 21:53 108-20-34.1 1.4 1
Ethylbenzene ND ug/kg 08/31/15 21:53 100-41-44.1 1.5 1
Hexachloro-1,3-butadiene ND ug/kg 08/31/15 21:53 87-68-34.1 1.6 1
2-Hexanone ND ug/kg 08/31/15 21:53 591-78-640.6 3.2 1
Isopropylbenzene (Cumene)ND ug/kg 08/31/15 21:53 98-82-84.1 1.5 1
p-Isopropyltoluene ND ug/kg 08/31/15 21:53 99-87-64.1 1.4 1
Methylene Chloride 7.0J ug/kg 08/31/15 21:53 75-09-2 B16.2 2.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/31/15 21:53 108-10-140.6 3.0 1
Methyl-tert-butyl ether ND ug/kg 08/31/15 21:53 1634-04-44.1 1.2 1
Naphthalene ND ug/kg 08/31/15 21:53 91-20-34.1 0.97 1
n-Propylbenzene ND ug/kg 08/31/15 21:53 103-65-14.1 1.4 1
Styrene ND ug/kg 08/31/15 21:53 100-42-54.1 1.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/31/15 21:53 630-20-64.1 1.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/31/15 21:53 79-34-54.1 1.5 1
Tetrachloroethene 201 ug/kg 09/01/15 15:04 127-18-412040.7 25
Toluene ND ug/kg 08/31/15 21:53 108-88-34.1 1.5 1
1,2,3-Trichlorobenzene ND ug/kg 08/31/15 21:53 87-61-64.1 1.8 1
1,2,4-Trichlorobenzene ND ug/kg 08/31/15 21:53 120-82-14.1 1.3 1
1,1,1-Trichloroethane ND ug/kg 08/31/15 21:53 71-55-64.1 1.5 1
1,1,2-Trichloroethane ND ug/kg 08/31/15 21:53 79-00-54.1 1.7 1
Trichloroethene 449 ug/kg 09/01/15 15:04 79-01-612050.3 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:MW-9 10'-15'Lab ID:92265398001 Collected:08/26/15 11:35 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 08/31/15 21:53 75-69-44.1 1.8 1
1,2,3-Trichloropropane ND ug/kg 08/31/15 21:53 96-18-44.1 1.3 1
1,2,4-Trimethylbenzene ND ug/kg 08/31/15 21:53 95-63-64.1 1.6 1
1,3,5-Trimethylbenzene ND ug/kg 08/31/15 21:53 108-67-84.1 1.5 1
Vinyl acetate ND ug/kg 08/31/15 21:53 108-05-440.6 7.1 1
Vinyl chloride ND ug/kg 08/31/15 21:53 75-01-48.1 1.5 1
Xylene (Total)ND ug/kg 08/31/15 21:53 1330-20-78.1 2.9 1
m&p-Xylene ND ug/kg 08/31/15 21:53 179601-23-18.1 2.9 1
o-Xylene ND ug/kg 08/31/15 21:53 95-47-64.1 1.5 1
Surrogates
Toluene-d8 (S)98 %08/31/15 21:53 2037-26-570-130 1
4-Bromofluorobenzene (S)96 %08/31/15 21:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %08/31/15 21:53 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.8 %08/28/15 19:380.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:MW-10 15'-18'Lab ID:92265398002 Collected:08/26/15 12:45 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 09/02/15 19:40 83-32-908/31/15 17:3039190.1 1
Acenaphthylene ND ug/kg 09/02/15 19:40 208-96-808/31/15 17:3039192.5 1
Aniline ND ug/kg 09/02/15 19:40 62-53-308/31/15 17:303911061
Anthracene ND ug/kg 09/02/15 19:40 120-12-708/31/15 17:3039187.7 1
Benzo(a)anthracene ND ug/kg 09/02/15 19:40 56-55-308/31/15 17:3039172.3 1
Benzo(a)pyrene ND ug/kg 09/02/15 19:40 50-32-808/31/15 17:3039174.7 1
Benzo(b)fluoranthene ND ug/kg 09/02/15 19:40 205-99-208/31/15 17:3039167.6 1
Benzo(g,h,i)perylene ND ug/kg 09/02/15 19:40 191-24-208/31/15 17:3039199.6 1
Benzo(k)fluoranthene ND ug/kg 09/02/15 19:40 207-08-908/31/15 17:3039177.1 1
Benzoic Acid ND ug/kg 09/02/15 19:40 65-85-008/31/15 17:30196071.1 1
Benzyl alcohol ND ug/kg 09/02/15 19:40 100-51-608/31/15 17:3078278.2 1
4-Bromophenylphenyl ether ND ug/kg 09/02/15 19:40 101-55-308/31/15 17:3039171.1 1
Butylbenzylphthalate ND ug/kg 09/02/15 19:40 85-68-708/31/15 17:3039183.0 1
4-Chloro-3-methylphenol ND ug/kg 09/02/15 19:40 59-50-708/31/15 17:3078280.6 1
4-Chloroaniline ND ug/kg 09/02/15 19:40 106-47-808/31/15 17:3019601091
bis(2-Chloroethoxy)methane ND ug/kg 09/02/15 19:40 111-91-108/31/15 17:3039191.3 1
bis(2-Chloroethyl) ether ND ug/kg 09/02/15 19:40 111-44-408/31/15 17:3039199.6 1
bis(2-Chloroisopropyl) ether ND ug/kg 09/02/15 19:40 108-60-108/31/15 17:303911041
2-Chloronaphthalene ND ug/kg 09/02/15 19:40 91-58-708/31/15 17:3039177.1 1
2-Chlorophenol ND ug/kg 09/02/15 19:40 95-57-808/31/15 17:303911071
4-Chlorophenylphenyl ether ND ug/kg 09/02/15 19:40 7005-72-308/31/15 17:3039180.6 1
Chrysene ND ug/kg 09/02/15 19:40 218-01-908/31/15 17:3039152.2 1
Dibenz(a,h)anthracene ND ug/kg 09/02/15 19:40 53-70-308/31/15 17:3039183.0 1
Dibenzofuran ND ug/kg 09/02/15 19:40 132-64-908/31/15 17:3039164.0 1
1,2-Dichlorobenzene ND ug/kg 09/02/15 19:40 95-50-108/31/15 17:303911041
1,3-Dichlorobenzene ND ug/kg 09/02/15 19:40 541-73-108/31/15 17:3039188.9 1
1,4-Dichlorobenzene ND ug/kg 09/02/15 19:40 106-46-708/31/15 17:303911101
3,3'-Dichlorobenzidine ND ug/kg 09/02/15 19:40 91-94-108/31/15 17:30196085.4 1
2,4-Dichlorophenol ND ug/kg 09/02/15 19:40 120-83-208/31/15 17:3039185.4 1
Diethylphthalate ND ug/kg 09/02/15 19:40 84-66-208/31/15 17:3039160.5 1
2,4-Dimethylphenol ND ug/kg 09/02/15 19:40 105-67-908/31/15 17:303911541
Dimethylphthalate ND ug/kg 09/02/15 19:40 131-11-308/31/15 17:3039179.4 1
Di-n-butylphthalate ND ug/kg 09/02/15 19:40 84-74-208/31/15 17:3039164.0 1
4,6-Dinitro-2-methylphenol ND ug/kg 09/02/15 19:40 534-52-108/31/15 17:3078278.2 1
2,4-Dinitrophenol ND ug/kg 09/02/15 19:40 51-28-508/31/15 17:30196064.0 1
2,4-Dinitrotoluene ND ug/kg 09/02/15 19:40 121-14-208/31/15 17:3039173.5 1
2,6-Dinitrotoluene ND ug/kg 09/02/15 19:40 606-20-208/31/15 17:3039181.8 1
Di-n-octylphthalate ND ug/kg 09/02/15 19:40 117-84-008/31/15 17:3039181.8 1
bis(2-Ethylhexyl)phthalate ND ug/kg 09/02/15 19:40 117-81-708/31/15 17:303911071
Fluoranthene ND ug/kg 09/02/15 19:40 206-44-008/31/15 17:3039156.9 1
Fluorene ND ug/kg 09/02/15 19:40 86-73-708/31/15 17:3039180.6 1
Hexachloro-1,3-butadiene ND ug/kg 09/02/15 19:40 87-68-308/31/15 17:3039167.6 1
Hexachlorobenzene ND ug/kg 09/02/15 19:40 118-74-108/31/15 17:3039149.8 1
Hexachlorocyclopentadiene ND ug/kg 09/02/15 19:40 77-47-408/31/15 17:3039172.3 1
Hexachloroethane ND ug/kg 09/02/15 19:40 67-72-108/31/15 17:303911031
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:MW-10 15'-18'Lab ID:92265398002 Collected:08/26/15 12:45 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Indeno(1,2,3-cd)pyrene ND ug/kg 09/02/15 19:40 193-39-508/31/15 17:3039180.6 1
Isophorone ND ug/kg 09/02/15 19:40 78-59-108/31/15 17:3039187.7 1
1-Methylnaphthalene ND ug/kg 09/02/15 19:40 90-12-008/31/15 17:303911021
2-Methylnaphthalene ND ug/kg 09/02/15 19:40 91-57-608/31/15 17:3039184.2 1
2-Methylphenol(o-Cresol)ND ug/kg 09/02/15 19:40 95-48-708/31/15 17:303911191
3&4-Methylphenol(m&p Cresol)ND ug/kg 09/02/15 19:4008/31/15 17:303911541
Naphthalene ND ug/kg 09/02/15 19:40 91-20-308/31/15 17:3039196.0 1
2-Nitroaniline ND ug/kg 09/02/15 19:40 88-74-408/31/15 17:3019601211
3-Nitroaniline ND ug/kg 09/02/15 19:40 99-09-208/31/15 17:3019601071
4-Nitroaniline ND ug/kg 09/02/15 19:40 100-01-608/31/15 17:307821101
Nitrobenzene ND ug/kg 09/02/15 19:40 98-95-308/31/15 17:303911071
2-Nitrophenol ND ug/kg 09/02/15 19:40 88-75-508/31/15 17:3039194.8 1
4-Nitrophenol ND ug/kg 09/02/15 19:40 100-02-708/31/15 17:30196070.0 1
N-Nitrosodimethylamine ND ug/kg 09/02/15 19:40 62-75-908/31/15 17:303911271
N-Nitroso-di-n-propylamine ND ug/kg 09/02/15 19:40 621-64-708/31/15 17:3039174.7 1
N-Nitrosodiphenylamine ND ug/kg 09/02/15 19:40 86-30-608/31/15 17:303911161
Pentachlorophenol ND ug/kg 09/02/15 19:40 87-86-508/31/15 17:30196071.1 1
Phenanthrene ND ug/kg 09/02/15 19:40 85-01-808/31/15 17:3039165.2 1
Phenol ND ug/kg 09/02/15 19:40 108-95-208/31/15 17:303911171
Pyrene ND ug/kg 09/02/15 19:40 129-00-008/31/15 17:3039166.4 1
1,2,4-Trichlorobenzene ND ug/kg 09/02/15 19:40 120-82-108/31/15 17:3039175.9 1
2,4,5-Trichlorophenol ND ug/kg 09/02/15 19:40 95-95-408/31/15 17:303911211
2,4,6-Trichlorophenol ND ug/kg 09/02/15 19:40 88-06-208/31/15 17:3039186.5 1
Surrogates
Nitrobenzene-d5 (S)61 %09/02/15 19:40 4165-60-008/31/15 17:3023-110 1
2-Fluorobiphenyl (S)62 %09/02/15 19:40 321-60-808/31/15 17:3030-110 1
Terphenyl-d14 (S)80 %09/02/15 19:40 1718-51-008/31/15 17:3028-110 1
Phenol-d6 (S)60 %09/02/15 19:40 13127-88-308/31/15 17:3022-110 1
2-Fluorophenol (S)63 %09/02/15 19:40 367-12-408/31/15 17:3013-110 1
2,4,6-Tribromophenol (S)80 %09/02/15 19:40 118-79-608/31/15 17:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 15.6J ug/kg 08/31/15 22:13 67-64-188.7 8.9 1
Benzene ND ug/kg 08/31/15 22:13 71-43-24.4 1.4 1
Bromobenzene ND ug/kg 08/31/15 22:13 108-86-14.4 1.8 1
Bromochloromethane ND ug/kg 08/31/15 22:13 74-97-54.4 1.5 1
Bromodichloromethane ND ug/kg 08/31/15 22:13 75-27-44.4 1.7 1
Bromoform ND ug/kg 08/31/15 22:13 75-25-24.4 2.0 1
Bromomethane ND ug/kg 08/31/15 22:13 74-83-98.9 2.2 1
2-Butanone (MEK)ND ug/kg 08/31/15 22:13 78-93-388.7 2.6 1
n-Butylbenzene ND ug/kg 08/31/15 22:13 104-51-84.4 1.6 1
sec-Butylbenzene ND ug/kg 08/31/15 22:13 135-98-84.4 1.4 1
tert-Butylbenzene ND ug/kg 08/31/15 22:13 98-06-64.4 1.8 1
Carbon tetrachloride ND ug/kg 08/31/15 22:13 56-23-54.4 2.3 1
Chlorobenzene ND ug/kg 08/31/15 22:13 108-90-74.4 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:MW-10 15'-18'Lab ID:92265398002 Collected:08/26/15 12:45 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloroethane ND ug/kg 08/31/15 22:13 75-00-38.9 2.1 1
Chloroform ND ug/kg 08/31/15 22:13 67-66-34.4 1.4 1
Chloromethane ND ug/kg 08/31/15 22:13 74-87-38.9 2.1 1
2-Chlorotoluene ND ug/kg 08/31/15 22:13 95-49-84.4 1.5 1
4-Chlorotoluene ND ug/kg 08/31/15 22:13 106-43-44.4 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/31/15 22:13 96-12-84.4 3.2 1
Dibromochloromethane ND ug/kg 08/31/15 22:13 124-48-14.4 1.6 1
1,2-Dibromoethane (EDB)ND ug/kg 08/31/15 22:13 106-93-44.4 1.6 1
Dibromomethane ND ug/kg 08/31/15 22:13 74-95-34.4 2.2 1
1,2-Dichlorobenzene ND ug/kg 08/31/15 22:13 95-50-14.4 1.7 1
1,3-Dichlorobenzene ND ug/kg 08/31/15 22:13 541-73-14.4 1.8 1
1,4-Dichlorobenzene ND ug/kg 08/31/15 22:13 106-46-74.4 1.5 1
Dichlorodifluoromethane ND ug/kg 08/31/15 22:13 75-71-88.9 3.2 1
1,1-Dichloroethane ND ug/kg 08/31/15 22:13 75-34-34.4 1.3 1
1,2-Dichloroethane ND ug/kg 08/31/15 22:13 107-06-24.4 2.0 1
1,1-Dichloroethene ND ug/kg 08/31/15 22:13 75-35-44.4 1.6 1
cis-1,2-Dichloroethene ND ug/kg 08/31/15 22:13 156-59-24.4 1.2 1
trans-1,2-Dichloroethene ND ug/kg 08/31/15 22:13 156-60-54.4 1.7 1
1,2-Dichloropropane ND ug/kg 08/31/15 22:13 78-87-54.4 1.5 1
1,3-Dichloropropane ND ug/kg 08/31/15 22:13 142-28-94.4 1.7 1
2,2-Dichloropropane ND ug/kg 08/31/15 22:13 594-20-74.4 1.5 1
1,1-Dichloropropene ND ug/kg 08/31/15 22:13 563-58-64.4 1.3 1
cis-1,3-Dichloropropene ND ug/kg 08/31/15 22:13 10061-01-54.4 1.6 1
trans-1,3-Dichloropropene ND ug/kg 08/31/15 22:13 10061-02-64.4 1.3 1
Diisopropyl ether ND ug/kg 08/31/15 22:13 108-20-34.4 1.5 1
Ethylbenzene ND ug/kg 08/31/15 22:13 100-41-44.4 1.6 1
Hexachloro-1,3-butadiene ND ug/kg 08/31/15 22:13 87-68-34.4 1.8 1
2-Hexanone ND ug/kg 08/31/15 22:13 591-78-644.4 3.5 1
Isopropylbenzene (Cumene)ND ug/kg 08/31/15 22:13 98-82-84.4 1.7 1
p-Isopropyltoluene ND ug/kg 08/31/15 22:13 99-87-64.4 1.5 1
Methylene Chloride 5.2J ug/kg 08/31/15 22:13 75-09-2 B17.7 2.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/31/15 22:13 108-10-144.4 3.3 1
Methyl-tert-butyl ether ND ug/kg 08/31/15 22:13 1634-04-44.4 1.3 1
Naphthalene ND ug/kg 08/31/15 22:13 91-20-34.4 1.1 1
n-Propylbenzene ND ug/kg 08/31/15 22:13 103-65-14.4 1.5 1
Styrene ND ug/kg 08/31/15 22:13 100-42-54.4 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/31/15 22:13 630-20-64.4 1.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/31/15 22:13 79-34-54.4 1.7 1
Tetrachloroethene ND ug/kg 08/31/15 22:13 127-18-44.4 1.5 1
Toluene ND ug/kg 08/31/15 22:13 108-88-34.4 1.6 1
1,2,3-Trichlorobenzene ND ug/kg 08/31/15 22:13 87-61-64.4 2.0 1
1,2,4-Trichlorobenzene ND ug/kg 08/31/15 22:13 120-82-14.4 1.4 1
1,1,1-Trichloroethane ND ug/kg 08/31/15 22:13 71-55-64.4 1.6 1
1,1,2-Trichloroethane ND ug/kg 08/31/15 22:13 79-00-54.4 1.9 1
Trichloroethene ND ug/kg 08/31/15 22:13 79-01-64.4 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:MW-10 15'-18'Lab ID:92265398002 Collected:08/26/15 12:45 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 08/31/15 22:13 75-69-44.4 2.0 1
1,2,3-Trichloropropane ND ug/kg 08/31/15 22:13 96-18-44.4 1.4 1
1,2,4-Trimethylbenzene ND ug/kg 08/31/15 22:13 95-63-64.4 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 08/31/15 22:13 108-67-84.4 1.6 1
Vinyl acetate ND ug/kg 08/31/15 22:13 108-05-444.4 7.8 1
Vinyl chloride ND ug/kg 08/31/15 22:13 75-01-48.9 1.6 1
Xylene (Total)ND ug/kg 08/31/15 22:13 1330-20-78.9 3.2 1
m&p-Xylene ND ug/kg 08/31/15 22:13 179601-23-18.9 3.2 1
o-Xylene ND ug/kg 08/31/15 22:13 95-47-64.4 1.7 1
Surrogates
Toluene-d8 (S)103 %08/31/15 22:13 2037-26-570-130 1
4-Bromofluorobenzene (S)91 %08/31/15 22:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %08/31/15 22:13 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.7 %08/28/15 19:380.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:SB-1 5'-7'Lab ID:92265398003 Collected:08/26/15 16:20 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 09/02/15 20:07 83-32-908/31/15 17:3038889.3 1
Acenaphthylene ND ug/kg 09/02/15 20:07 208-96-808/31/15 17:3038891.6 1
Aniline ND ug/kg 09/02/15 20:07 62-53-308/31/15 17:303881051
Anthracene 128J ug/kg 09/02/15 20:07 120-12-708/31/15 17:3038886.9 1
Benzo(a)anthracene 461 ug/kg 09/02/15 20:07 56-55-308/31/15 17:3038871.7 1
Benzo(a)pyrene 401 ug/kg 09/02/15 20:07 50-32-808/31/15 17:3038874.0 1
Benzo(b)fluoranthene 638 ug/kg 09/02/15 20:07 205-99-208/31/15 17:3038867.0 1
Benzo(g,h,i)perylene 263J ug/kg 09/02/15 20:07 191-24-208/31/15 17:3038898.7 1
Benzo(k)fluoranthene 286J ug/kg 09/02/15 20:07 207-08-908/31/15 17:3038876.4 1
Benzoic Acid ND ug/kg 09/02/15 20:07 65-85-008/31/15 17:30194070.5 1
Benzyl alcohol ND ug/kg 09/02/15 20:07 100-51-608/31/15 17:3077577.5 1
4-Bromophenylphenyl ether ND ug/kg 09/02/15 20:07 101-55-308/31/15 17:3038870.5 1
Butylbenzylphthalate ND ug/kg 09/02/15 20:07 85-68-708/31/15 17:3038882.2 1
4-Chloro-3-methylphenol ND ug/kg 09/02/15 20:07 59-50-708/31/15 17:3077579.9 1
4-Chloroaniline ND ug/kg 09/02/15 20:07 106-47-808/31/15 17:3019401081
bis(2-Chloroethoxy)methane ND ug/kg 09/02/15 20:07 111-91-108/31/15 17:3038890.5 1
bis(2-Chloroethyl) ether ND ug/kg 09/02/15 20:07 111-44-408/31/15 17:3038898.7 1
bis(2-Chloroisopropyl) ether ND ug/kg 09/02/15 20:07 108-60-108/31/15 17:303881031
2-Chloronaphthalene ND ug/kg 09/02/15 20:07 91-58-708/31/15 17:3038876.4 1
2-Chlorophenol ND ug/kg 09/02/15 20:07 95-57-808/31/15 17:303881061
4-Chlorophenylphenyl ether ND ug/kg 09/02/15 20:07 7005-72-308/31/15 17:3038879.9 1
Chrysene 450 ug/kg 09/02/15 20:07 218-01-9 B08/31/15 17:3038851.7 1
Dibenz(a,h)anthracene 85.0J ug/kg 09/02/15 20:07 53-70-308/31/15 17:3038882.2 1
Dibenzofuran ND ug/kg 09/02/15 20:07 132-64-908/31/15 17:3038863.4 1
1,2-Dichlorobenzene ND ug/kg 09/02/15 20:07 95-50-108/31/15 17:303881031
1,3-Dichlorobenzene ND ug/kg 09/02/15 20:07 541-73-108/31/15 17:3038888.1 1
1,4-Dichlorobenzene ND ug/kg 09/02/15 20:07 106-46-708/31/15 17:303881091
3,3'-Dichlorobenzidine ND ug/kg 09/02/15 20:07 91-94-108/31/15 17:30194084.6 1
2,4-Dichlorophenol ND ug/kg 09/02/15 20:07 120-83-208/31/15 17:3038884.6 1
Diethylphthalate ND ug/kg 09/02/15 20:07 84-66-208/31/15 17:3038859.9 1
2,4-Dimethylphenol ND ug/kg 09/02/15 20:07 105-67-908/31/15 17:303881531
Dimethylphthalate ND ug/kg 09/02/15 20:07 131-11-308/31/15 17:3038878.7 1
Di-n-butylphthalate ND ug/kg 09/02/15 20:07 84-74-208/31/15 17:3038863.4 1
4,6-Dinitro-2-methylphenol ND ug/kg 09/02/15 20:07 534-52-108/31/15 17:3077577.5 1
2,4-Dinitrophenol ND ug/kg 09/02/15 20:07 51-28-508/31/15 17:30194063.4 1
2,4-Dinitrotoluene ND ug/kg 09/02/15 20:07 121-14-208/31/15 17:3038872.8 1
2,6-Dinitrotoluene ND ug/kg 09/02/15 20:07 606-20-208/31/15 17:3038881.1 1
Di-n-octylphthalate ND ug/kg 09/02/15 20:07 117-84-008/31/15 17:3038881.1 1
bis(2-Ethylhexyl)phthalate ND ug/kg 09/02/15 20:07 117-81-708/31/15 17:303881061
Fluoranthene 1020 ug/kg 09/02/15 20:07 206-44-008/31/15 17:3038856.4 1
Fluorene 181J ug/kg 09/02/15 20:07 86-73-708/31/15 17:3038879.9 1
Hexachloro-1,3-butadiene ND ug/kg 09/02/15 20:07 87-68-308/31/15 17:3038867.0 1
Hexachlorobenzene ND ug/kg 09/02/15 20:07 118-74-108/31/15 17:3038849.3 1
Hexachlorocyclopentadiene ND ug/kg 09/02/15 20:07 77-47-408/31/15 17:3038871.7 1
Hexachloroethane ND ug/kg 09/02/15 20:07 67-72-108/31/15 17:303881021
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:SB-1 5'-7'Lab ID:92265398003 Collected:08/26/15 16:20 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Indeno(1,2,3-cd)pyrene 230J ug/kg 09/02/15 20:07 193-39-508/31/15 17:3038879.9 1
Isophorone ND ug/kg 09/02/15 20:07 78-59-108/31/15 17:3038886.9 1
1-Methylnaphthalene 1090 ug/kg 09/02/15 20:07 90-12-008/31/15 17:303881011
2-Methylnaphthalene 1620 ug/kg 09/02/15 20:07 91-57-608/31/15 17:3038883.4 1
2-Methylphenol(o-Cresol)ND ug/kg 09/02/15 20:07 95-48-708/31/15 17:303881171
3&4-Methylphenol(m&p Cresol)ND ug/kg 09/02/15 20:0708/31/15 17:303881531
Naphthalene 1350 ug/kg 09/02/15 20:07 91-20-308/31/15 17:3038895.2 1
2-Nitroaniline ND ug/kg 09/02/15 20:07 88-74-408/31/15 17:3019401201
3-Nitroaniline ND ug/kg 09/02/15 20:07 99-09-208/31/15 17:3019401061
4-Nitroaniline ND ug/kg 09/02/15 20:07 100-01-608/31/15 17:307751091
Nitrobenzene ND ug/kg 09/02/15 20:07 98-95-308/31/15 17:303881061
2-Nitrophenol ND ug/kg 09/02/15 20:07 88-75-508/31/15 17:3038894.0 1
4-Nitrophenol ND ug/kg 09/02/15 20:07 100-02-708/31/15 17:30194069.3 1
N-Nitrosodimethylamine ND ug/kg 09/02/15 20:07 62-75-908/31/15 17:303881261
N-Nitroso-di-n-propylamine ND ug/kg 09/02/15 20:07 621-64-708/31/15 17:3038874.0 1
N-Nitrosodiphenylamine 372J ug/kg 09/02/15 20:07 86-30-608/31/15 17:303881151
Pentachlorophenol ND ug/kg 09/02/15 20:07 87-86-508/31/15 17:30194070.5 1
Phenanthrene 569 ug/kg 09/02/15 20:07 85-01-808/31/15 17:3038864.6 1
Phenol ND ug/kg 09/02/15 20:07 108-95-208/31/15 17:303881161
Pyrene 741 ug/kg 09/02/15 20:07 129-00-008/31/15 17:3038865.8 1
1,2,4-Trichlorobenzene ND ug/kg 09/02/15 20:07 120-82-108/31/15 17:3038875.2 1
2,4,5-Trichlorophenol ND ug/kg 09/02/15 20:07 95-95-408/31/15 17:303881201
2,4,6-Trichlorophenol ND ug/kg 09/02/15 20:07 88-06-208/31/15 17:3038885.8 1
Surrogates
Nitrobenzene-d5 (S)42 %09/02/15 20:07 4165-60-008/31/15 17:3023-110 1
2-Fluorobiphenyl (S)50 %09/02/15 20:07 321-60-808/31/15 17:3030-110 1
Terphenyl-d14 (S)74 %09/02/15 20:07 1718-51-008/31/15 17:3028-110 1
Phenol-d6 (S)51 %09/02/15 20:07 13127-88-308/31/15 17:3022-110 1
2-Fluorophenol (S)49 %09/02/15 20:07 367-12-408/31/15 17:3013-110 1
2,4,6-Tribromophenol (S)76 %09/02/15 20:07 118-79-608/31/15 17:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 08/31/15 22:33 67-64-1246024625
Benzene ND ug/kg 08/31/15 22:33 71-43-212339.3 25
Bromobenzene ND ug/kg 08/31/15 22:33 108-86-112349.1 25
Bromochloromethane ND ug/kg 08/31/15 22:33 74-97-512341.7 25
Bromodichloromethane ND ug/kg 08/31/15 22:33 75-27-412346.7 25
Bromoform ND ug/kg 08/31/15 22:33 75-25-212356.5 25
Bromomethane ND ug/kg 08/31/15 22:33 74-83-924661.4 25
2-Butanone (MEK)ND ug/kg 08/31/15 22:33 78-93-3246071.2 25
n-Butylbenzene 1520 ug/kg 08/31/15 22:33 104-51-812344.2 25
sec-Butylbenzene 827 ug/kg 08/31/15 22:33 135-98-812339.3 25
tert-Butylbenzene 208 ug/kg 08/31/15 22:33 98-06-612349.1 25
Carbon tetrachloride ND ug/kg 08/31/15 22:33 56-23-512363.9 25
Chlorobenzene ND ug/kg 08/31/15 22:33 108-90-712346.7 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:SB-1 5'-7'Lab ID:92265398003 Collected:08/26/15 16:20 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloroethane ND ug/kg 08/31/15 22:33 75-00-324658.9 25
Chloroform ND ug/kg 08/31/15 22:33 67-66-312339.3 25
Chloromethane ND ug/kg 08/31/15 22:33 74-87-324658.9 25
2-Chlorotoluene ND ug/kg 08/31/15 22:33 95-49-812341.7 25
4-Chlorotoluene ND ug/kg 08/31/15 22:33 106-43-412344.2 25
1,2-Dibromo-3-chloropropane ND ug/kg 08/31/15 22:33 96-12-812388.4 25
Dibromochloromethane ND ug/kg 08/31/15 22:33 124-48-112344.2 25
1,2-Dibromoethane (EDB)ND ug/kg 08/31/15 22:33 106-93-412344.2 25
Dibromomethane ND ug/kg 08/31/15 22:33 74-95-312361.4 25
1,2-Dichlorobenzene ND ug/kg 08/31/15 22:33 95-50-112346.7 25
1,3-Dichlorobenzene ND ug/kg 08/31/15 22:33 541-73-112349.1 25
1,4-Dichlorobenzene ND ug/kg 08/31/15 22:33 106-46-712341.7 25
Dichlorodifluoromethane ND ug/kg 08/31/15 22:33 75-71-824688.4 25
1,1-Dichloroethane ND ug/kg 08/31/15 22:33 75-34-312336.8 25
1,2-Dichloroethane ND ug/kg 08/31/15 22:33 107-06-212354.0 25
1,1-Dichloroethene ND ug/kg 08/31/15 22:33 75-35-412344.2 25
cis-1,2-Dichloroethene ND ug/kg 08/31/15 22:33 156-59-212334.4 25
trans-1,2-Dichloroethene ND ug/kg 08/31/15 22:33 156-60-512346.7 25
1,2-Dichloropropane ND ug/kg 08/31/15 22:33 78-87-512341.7 25
1,3-Dichloropropane ND ug/kg 08/31/15 22:33 142-28-912346.7 25
2,2-Dichloropropane ND ug/kg 08/31/15 22:33 594-20-712341.7 25
1,1-Dichloropropene ND ug/kg 08/31/15 22:33 563-58-612336.8 25
cis-1,3-Dichloropropene ND ug/kg 08/31/15 22:33 10061-01-512344.2 25
trans-1,3-Dichloropropene ND ug/kg 08/31/15 22:33 10061-02-612336.8 25
Diisopropyl ether ND ug/kg 08/31/15 22:33 108-20-312341.7 25
Ethylbenzene 465 ug/kg 08/31/15 22:33 100-41-412344.2 25
Hexachloro-1,3-butadiene ND ug/kg 08/31/15 22:33 87-68-312349.1 25
2-Hexanone ND ug/kg 08/31/15 22:33 591-78-6123095.8 25
Isopropylbenzene (Cumene)2520 ug/kg 08/31/15 22:33 98-82-812346.7 25
p-Isopropyltoluene 1120 ug/kg 08/31/15 22:33 99-87-612341.7 25
Methylene Chloride ND ug/kg 08/31/15 22:33 75-09-249173.7 25
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/31/15 22:33 108-10-1123090.9 25
Methyl-tert-butyl ether ND ug/kg 08/31/15 22:33 1634-04-412336.8 25
Naphthalene 2760 ug/kg 08/31/15 22:33 91-20-312329.5 25
n-Propylbenzene 6360 ug/kg 09/02/15 12:57 103-65-124683.5 50
Styrene ND ug/kg 08/31/15 22:33 100-42-512344.2 25
1,1,1,2-Tetrachloroethane ND ug/kg 08/31/15 22:33 630-20-612351.6 25
1,1,2,2-Tetrachloroethane ND ug/kg 08/31/15 22:33 79-34-512346.7 25
Tetrachloroethene ND ug/kg 08/31/15 22:33 127-18-412341.7 25
Toluene 139 ug/kg 08/31/15 22:33 108-88-312344.2 25
1,2,3-Trichlorobenzene ND ug/kg 08/31/15 22:33 87-61-612354.0 25
1,2,4-Trichlorobenzene ND ug/kg 08/31/15 22:33 120-82-112339.3 25
1,1,1-Trichloroethane ND ug/kg 08/31/15 22:33 71-55-612344.2 25
1,1,2-Trichloroethane ND ug/kg 08/31/15 22:33 79-00-512351.6 25
Trichloroethene ND ug/kg 08/31/15 22:33 79-01-612351.6 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:SB-1 5'-7'Lab ID:92265398003 Collected:08/26/15 16:20 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 08/31/15 22:33 75-69-412354.0 25
1,2,3-Trichloropropane ND ug/kg 08/31/15 22:33 96-18-412339.3 25
1,2,4-Trimethylbenzene 187 ug/kg 08/31/15 22:33 95-63-612349.1 25
1,3,5-Trimethylbenzene 65.4J ug/kg 08/31/15 22:33 108-67-812344.2 25
Vinyl acetate ND ug/kg 08/31/15 22:33 108-05-4123021625
Vinyl chloride ND ug/kg 08/31/15 22:33 75-01-424644.2 25
Xylene (Total)1010 ug/kg 08/31/15 22:33 1330-20-724688.4 25
m&p-Xylene 1010 ug/kg 08/31/15 22:33 179601-23-124688.4 25
o-Xylene 96.1J ug/kg 08/31/15 22:33 95-47-612346.7 25
Surrogates
Toluene-d8 (S)97 %08/31/15 22:33 2037-26-570-130 25
4-Bromofluorobenzene (S)96 %08/31/15 22:33 460-00-470-130 25
1,2-Dichloroethane-d4 (S)278 %08/31/15 22:33 17060-07-0 S270-132 25
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.9 %08/28/15 19:380.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:SB-2 5'-7'Lab ID:92265398004 Collected:08/26/15 16:30 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 09/02/15 20:35 83-32-908/31/15 17:3040693.6 1
Acenaphthylene ND ug/kg 09/02/15 20:35 208-96-808/31/15 17:3040696.1 1
Aniline ND ug/kg 09/02/15 20:35 62-53-308/31/15 17:304061101
Anthracene ND ug/kg 09/02/15 20:35 120-12-708/31/15 17:3040691.1 1
Benzo(a)anthracene 109J ug/kg 09/02/15 20:35 56-55-308/31/15 17:3040675.1 1
Benzo(a)pyrene 91.2J ug/kg 09/02/15 20:35 50-32-808/31/15 17:3040677.6 1
Benzo(b)fluoranthene 159J ug/kg 09/02/15 20:35 205-99-208/31/15 17:3040670.2 1
Benzo(g,h,i)perylene ND ug/kg 09/02/15 20:35 191-24-208/31/15 17:304061031
Benzo(k)fluoranthene ND ug/kg 09/02/15 20:35 207-08-908/31/15 17:3040680.1 1
Benzoic Acid ND ug/kg 09/02/15 20:35 65-85-008/31/15 17:30203073.9 1
Benzyl alcohol ND ug/kg 09/02/15 20:35 100-51-608/31/15 17:3081381.3 1
4-Bromophenylphenyl ether ND ug/kg 09/02/15 20:35 101-55-308/31/15 17:3040673.9 1
Butylbenzylphthalate ND ug/kg 09/02/15 20:35 85-68-708/31/15 17:3040686.2 1
4-Chloro-3-methylphenol ND ug/kg 09/02/15 20:35 59-50-708/31/15 17:3081383.8 1
4-Chloroaniline ND ug/kg 09/02/15 20:35 106-47-808/31/15 17:3020301131
bis(2-Chloroethoxy)methane ND ug/kg 09/02/15 20:35 111-91-108/31/15 17:3040694.8 1
bis(2-Chloroethyl) ether ND ug/kg 09/02/15 20:35 111-44-408/31/15 17:304061031
bis(2-Chloroisopropyl) ether ND ug/kg 09/02/15 20:35 108-60-108/31/15 17:304061081
2-Chloronaphthalene ND ug/kg 09/02/15 20:35 91-58-708/31/15 17:3040680.1 1
2-Chlorophenol ND ug/kg 09/02/15 20:35 95-57-808/31/15 17:304061111
4-Chlorophenylphenyl ether ND ug/kg 09/02/15 20:35 7005-72-308/31/15 17:3040683.8 1
Chrysene 109J ug/kg 09/02/15 20:35 218-01-9 B08/31/15 17:3040654.2 1
Dibenz(a,h)anthracene ND ug/kg 09/02/15 20:35 53-70-308/31/15 17:3040686.2 1
Dibenzofuran ND ug/kg 09/02/15 20:35 132-64-908/31/15 17:3040666.5 1
1,2-Dichlorobenzene ND ug/kg 09/02/15 20:35 95-50-108/31/15 17:304061081
1,3-Dichlorobenzene ND ug/kg 09/02/15 20:35 541-73-108/31/15 17:3040692.4 1
1,4-Dichlorobenzene ND ug/kg 09/02/15 20:35 106-46-708/31/15 17:304061151
3,3'-Dichlorobenzidine ND ug/kg 09/02/15 20:35 91-94-108/31/15 17:30203088.7 1
2,4-Dichlorophenol ND ug/kg 09/02/15 20:35 120-83-208/31/15 17:3040688.7 1
Diethylphthalate ND ug/kg 09/02/15 20:35 84-66-208/31/15 17:3040662.8 1
2,4-Dimethylphenol ND ug/kg 09/02/15 20:35 105-67-908/31/15 17:304061601
Dimethylphthalate ND ug/kg 09/02/15 20:35 131-11-308/31/15 17:3040682.5 1
Di-n-butylphthalate ND ug/kg 09/02/15 20:35 84-74-208/31/15 17:3040666.5 1
4,6-Dinitro-2-methylphenol ND ug/kg 09/02/15 20:35 534-52-108/31/15 17:3081381.3 1
2,4-Dinitrophenol ND ug/kg 09/02/15 20:35 51-28-508/31/15 17:30203066.5 1
2,4-Dinitrotoluene ND ug/kg 09/02/15 20:35 121-14-208/31/15 17:3040676.4 1
2,6-Dinitrotoluene ND ug/kg 09/02/15 20:35 606-20-208/31/15 17:3040685.0 1
Di-n-octylphthalate ND ug/kg 09/02/15 20:35 117-84-008/31/15 17:3040685.0 1
bis(2-Ethylhexyl)phthalate ND ug/kg 09/02/15 20:35 117-81-708/31/15 17:304061111
Fluoranthene 241J ug/kg 09/02/15 20:35 206-44-008/31/15 17:3040659.1 1
Fluorene ND ug/kg 09/02/15 20:35 86-73-708/31/15 17:3040683.8 1
Hexachloro-1,3-butadiene ND ug/kg 09/02/15 20:35 87-68-308/31/15 17:3040670.2 1
Hexachlorobenzene ND ug/kg 09/02/15 20:35 118-74-108/31/15 17:3040651.7 1
Hexachlorocyclopentadiene ND ug/kg 09/02/15 20:35 77-47-408/31/15 17:3040675.1 1
Hexachloroethane ND ug/kg 09/02/15 20:35 67-72-108/31/15 17:304061071
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:SB-2 5'-7'Lab ID:92265398004 Collected:08/26/15 16:30 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Indeno(1,2,3-cd)pyrene ND ug/kg 09/02/15 20:35 193-39-508/31/15 17:3040683.8 1
Isophorone ND ug/kg 09/02/15 20:35 78-59-108/31/15 17:3040691.1 1
1-Methylnaphthalene ND ug/kg 09/02/15 20:35 90-12-008/31/15 17:304061061
2-Methylnaphthalene ND ug/kg 09/02/15 20:35 91-57-608/31/15 17:3040687.5 1
2-Methylphenol(o-Cresol)ND ug/kg 09/02/15 20:35 95-48-708/31/15 17:304061231
3&4-Methylphenol(m&p Cresol)ND ug/kg 09/02/15 20:3508/31/15 17:304061601
Naphthalene ND ug/kg 09/02/15 20:35 91-20-308/31/15 17:3040699.8 1
2-Nitroaniline ND ug/kg 09/02/15 20:35 88-74-408/31/15 17:3020301261
3-Nitroaniline ND ug/kg 09/02/15 20:35 99-09-208/31/15 17:3020301111
4-Nitroaniline ND ug/kg 09/02/15 20:35 100-01-608/31/15 17:308131151
Nitrobenzene ND ug/kg 09/02/15 20:35 98-95-308/31/15 17:304061111
2-Nitrophenol ND ug/kg 09/02/15 20:35 88-75-508/31/15 17:3040698.5 1
4-Nitrophenol ND ug/kg 09/02/15 20:35 100-02-708/31/15 17:30203072.7 1
N-Nitrosodimethylamine ND ug/kg 09/02/15 20:35 62-75-908/31/15 17:304061321
N-Nitroso-di-n-propylamine ND ug/kg 09/02/15 20:35 621-64-708/31/15 17:3040677.6 1
N-Nitrosodiphenylamine ND ug/kg 09/02/15 20:35 86-30-608/31/15 17:304061211
Pentachlorophenol ND ug/kg 09/02/15 20:35 87-86-508/31/15 17:30203073.9 1
Phenanthrene 115J ug/kg 09/02/15 20:35 85-01-808/31/15 17:3040667.7 1
Phenol ND ug/kg 09/02/15 20:35 108-95-208/31/15 17:304061221
Pyrene 175J ug/kg 09/02/15 20:35 129-00-008/31/15 17:3040669.0 1
1,2,4-Trichlorobenzene ND ug/kg 09/02/15 20:35 120-82-108/31/15 17:3040678.8 1
2,4,5-Trichlorophenol ND ug/kg 09/02/15 20:35 95-95-408/31/15 17:304061261
2,4,6-Trichlorophenol ND ug/kg 09/02/15 20:35 88-06-208/31/15 17:3040689.9 1
Surrogates
Nitrobenzene-d5 (S)46 %09/02/15 20:35 4165-60-008/31/15 17:3023-110 1
2-Fluorobiphenyl (S)53 %09/02/15 20:35 321-60-808/31/15 17:3030-110 1
Terphenyl-d14 (S)75 %09/02/15 20:35 1718-51-008/31/15 17:3028-110 1
Phenol-d6 (S)60 %09/02/15 20:35 13127-88-308/31/15 17:3022-110 1
2-Fluorophenol (S)62 %09/02/15 20:35 367-12-408/31/15 17:3013-110 1
2,4,6-Tribromophenol (S)81 %09/02/15 20:35 118-79-608/31/15 17:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 08/31/15 22:52 67-64-111411.4 1
Benzene ND ug/kg 08/31/15 22:52 71-43-25.7 1.8 1
Bromobenzene ND ug/kg 08/31/15 22:52 108-86-15.7 2.3 1
Bromochloromethane ND ug/kg 08/31/15 22:52 74-97-55.7 1.9 1
Bromodichloromethane ND ug/kg 08/31/15 22:52 75-27-45.7 2.2 1
Bromoform ND ug/kg 08/31/15 22:52 75-25-25.7 2.6 1
Bromomethane ND ug/kg 08/31/15 22:52 74-83-911.4 2.9 1
2-Butanone (MEK)ND ug/kg 08/31/15 22:52 78-93-31143.3 1
n-Butylbenzene 5.8 ug/kg 08/31/15 22:52 104-51-85.7 2.1 1
sec-Butylbenzene 6.3 ug/kg 08/31/15 22:52 135-98-85.7 1.8 1
tert-Butylbenzene ND ug/kg 08/31/15 22:52 98-06-65.7 2.3 1
Carbon tetrachloride ND ug/kg 08/31/15 22:52 56-23-55.7 3.0 1
Chlorobenzene ND ug/kg 08/31/15 22:52 108-90-75.7 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:SB-2 5'-7'Lab ID:92265398004 Collected:08/26/15 16:30 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloroethane ND ug/kg 08/31/15 22:52 75-00-311.4 2.7 1
Chloroform ND ug/kg 08/31/15 22:52 67-66-35.7 1.8 1
Chloromethane ND ug/kg 08/31/15 22:52 74-87-311.4 2.7 1
2-Chlorotoluene ND ug/kg 08/31/15 22:52 95-49-85.7 1.9 1
4-Chlorotoluene ND ug/kg 08/31/15 22:52 106-43-45.7 2.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/31/15 22:52 96-12-85.7 4.1 1
Dibromochloromethane ND ug/kg 08/31/15 22:52 124-48-15.7 2.1 1
1,2-Dibromoethane (EDB)ND ug/kg 08/31/15 22:52 106-93-45.7 2.1 1
Dibromomethane ND ug/kg 08/31/15 22:52 74-95-35.7 2.9 1
1,2-Dichlorobenzene ND ug/kg 08/31/15 22:52 95-50-15.7 2.2 1
1,3-Dichlorobenzene ND ug/kg 08/31/15 22:52 541-73-15.7 2.3 1
1,4-Dichlorobenzene ND ug/kg 08/31/15 22:52 106-46-75.7 1.9 1
Dichlorodifluoromethane ND ug/kg 08/31/15 22:52 75-71-811.4 4.1 1
1,1-Dichloroethane ND ug/kg 08/31/15 22:52 75-34-35.7 1.7 1
1,2-Dichloroethane ND ug/kg 08/31/15 22:52 107-06-25.7 2.5 1
1,1-Dichloroethene ND ug/kg 08/31/15 22:52 75-35-45.7 2.1 1
cis-1,2-Dichloroethene 15.3 ug/kg 08/31/15 22:52 156-59-25.7 1.6 1
trans-1,2-Dichloroethene ND ug/kg 08/31/15 22:52 156-60-55.7 2.2 1
1,2-Dichloropropane ND ug/kg 08/31/15 22:52 78-87-55.7 1.9 1
1,3-Dichloropropane ND ug/kg 08/31/15 22:52 142-28-95.7 2.2 1
2,2-Dichloropropane ND ug/kg 08/31/15 22:52 594-20-75.7 1.9 1
1,1-Dichloropropene ND ug/kg 08/31/15 22:52 563-58-65.7 1.7 1
cis-1,3-Dichloropropene ND ug/kg 08/31/15 22:52 10061-01-55.7 2.1 1
trans-1,3-Dichloropropene ND ug/kg 08/31/15 22:52 10061-02-65.7 1.7 1
Diisopropyl ether ND ug/kg 08/31/15 22:52 108-20-35.7 1.9 1
Ethylbenzene ND ug/kg 08/31/15 22:52 100-41-45.7 2.1 1
Hexachloro-1,3-butadiene ND ug/kg 08/31/15 22:52 87-68-35.7 2.3 1
2-Hexanone ND ug/kg 08/31/15 22:52 591-78-657.0 4.4 1
Isopropylbenzene (Cumene)ND ug/kg 08/31/15 22:52 98-82-85.7 2.2 1
p-Isopropyltoluene ND ug/kg 08/31/15 22:52 99-87-65.7 1.9 1
Methylene Chloride ND ug/kg 08/31/15 22:52 75-09-222.8 3.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/31/15 22:52 108-10-157.0 4.2 1
Methyl-tert-butyl ether ND ug/kg 08/31/15 22:52 1634-04-45.7 1.7 1
Naphthalene 5.0J ug/kg 08/31/15 22:52 91-20-3 B5.7 1.4 1
n-Propylbenzene 2.9J ug/kg 08/31/15 22:52 103-65-15.7 1.9 1
Styrene ND ug/kg 08/31/15 22:52 100-42-55.7 2.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/31/15 22:52 630-20-65.7 2.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/31/15 22:52 79-34-55.7 2.2 1
Tetrachloroethene ND ug/kg 08/31/15 22:52 127-18-45.7 1.9 1
Toluene ND ug/kg 08/31/15 22:52 108-88-35.7 2.1 1
1,2,3-Trichlorobenzene ND ug/kg 08/31/15 22:52 87-61-65.7 2.5 1
1,2,4-Trichlorobenzene ND ug/kg 08/31/15 22:52 120-82-15.7 1.8 1
1,1,1-Trichloroethane ND ug/kg 08/31/15 22:52 71-55-65.7 2.1 1
1,1,2-Trichloroethane ND ug/kg 08/31/15 22:52 79-00-55.7 2.4 1
Trichloroethene ND ug/kg 08/31/15 22:52 79-01-65.7 2.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:SB-2 5'-7'Lab ID:92265398004 Collected:08/26/15 16:30 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 08/31/15 22:52 75-69-45.7 2.5 1
1,2,3-Trichloropropane ND ug/kg 08/31/15 22:52 96-18-45.7 1.8 1
1,2,4-Trimethylbenzene ND ug/kg 08/31/15 22:52 95-63-65.7 2.3 1
1,3,5-Trimethylbenzene ND ug/kg 08/31/15 22:52 108-67-85.7 2.1 1
Vinyl acetate ND ug/kg 08/31/15 22:52 108-05-457.0 10.0 1
Vinyl chloride 2.2J ug/kg 08/31/15 22:52 75-01-411.4 2.1 1
Xylene (Total)ND ug/kg 08/31/15 22:52 1330-20-711.4 4.1 1
m&p-Xylene ND ug/kg 08/31/15 22:52 179601-23-111.4 4.1 1
o-Xylene ND ug/kg 08/31/15 22:52 95-47-65.7 2.2 1
Surrogates
Toluene-d8 (S)101 %08/31/15 22:52 2037-26-570-130 1
4-Bromofluorobenzene (S)93 %08/31/15 22:52 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %08/31/15 22:52 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.8 %08/28/15 19:380.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:SB-3 5'-7'Lab ID:92265398005 Collected:08/26/15 16:35 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene 1580J ug/kg 09/03/15 14:38 83-32-908/31/15 17:304520104010
Acenaphthylene ND ug/kg 09/03/15 14:38 208-96-808/31/15 17:304520107010
Aniline ND ug/kg 09/03/15 14:38 62-53-308/31/15 17:304520122010
Anthracene 2970J ug/kg 09/03/15 14:38 120-12-708/31/15 17:304520101010
Benzo(a)anthracene 9720 ug/kg 09/03/15 14:38 56-55-308/31/15 17:30452083510
Benzo(a)pyrene 8830 ug/kg 09/03/15 14:38 50-32-808/31/15 17:30452086210
Benzo(b)fluoranthene 13300 ug/kg 09/03/15 14:38 205-99-208/31/15 17:30452078010
Benzo(g,h,i)perylene 5820 ug/kg 09/03/15 14:38 191-24-208/31/15 17:304520115010
Benzo(k)fluoranthene 7200 ug/kg 09/03/15 14:38 207-08-908/31/15 17:30452089010
Benzoic Acid ND ug/kg 09/03/15 14:38 65-85-008/31/15 17:302260082110
Benzyl alcohol ND ug/kg 09/03/15 14:38 100-51-608/31/15 17:30903090310
4-Bromophenylphenyl ether ND ug/kg 09/03/15 14:38 101-55-308/31/15 17:30452082110
Butylbenzylphthalate ND ug/kg 09/03/15 14:38 85-68-708/31/15 17:30452095810
4-Chloro-3-methylphenol ND ug/kg 09/03/15 14:38 59-50-708/31/15 17:30903093110
4-Chloroaniline ND ug/kg 09/03/15 14:38 106-47-808/31/15 17:3022600126010
bis(2-Chloroethoxy)methane ND ug/kg 09/03/15 14:38 111-91-108/31/15 17:304520105010
bis(2-Chloroethyl) ether ND ug/kg 09/03/15 14:38 111-44-408/31/15 17:304520115010
bis(2-Chloroisopropyl) ether ND ug/kg 09/03/15 14:38 108-60-108/31/15 17:304520120010
2-Chloronaphthalene ND ug/kg 09/03/15 14:38 91-58-708/31/15 17:30452089010
2-Chlorophenol ND ug/kg 09/03/15 14:38 95-57-808/31/15 17:304520123010
4-Chlorophenylphenyl ether ND ug/kg 09/03/15 14:38 7005-72-308/31/15 17:30452093110
Chrysene 9410 ug/kg 09/03/15 14:38 218-01-908/31/15 17:30452060210
Dibenz(a,h)anthracene 1770J ug/kg 09/03/15 14:38 53-70-308/31/15 17:30452095810
Dibenzofuran 782J ug/kg 09/03/15 14:38 132-64-908/31/15 17:30452073910
1,2-Dichlorobenzene ND ug/kg 09/03/15 14:38 95-50-108/31/15 17:304520120010
1,3-Dichlorobenzene ND ug/kg 09/03/15 14:38 541-73-108/31/15 17:304520103010
1,4-Dichlorobenzene ND ug/kg 09/03/15 14:38 106-46-708/31/15 17:304520127010
3,3'-Dichlorobenzidine ND ug/kg 09/03/15 14:38 91-94-108/31/15 17:302260098510
2,4-Dichlorophenol ND ug/kg 09/03/15 14:38 120-83-208/31/15 17:30452098510
Diethylphthalate ND ug/kg 09/03/15 14:38 84-66-208/31/15 17:30452069810
2,4-Dimethylphenol ND ug/kg 09/03/15 14:38 105-67-908/31/15 17:304520178010
Dimethylphthalate ND ug/kg 09/03/15 14:38 131-11-308/31/15 17:30452091710
Di-n-butylphthalate ND ug/kg 09/03/15 14:38 84-74-208/31/15 17:30452073910
4,6-Dinitro-2-methylphenol ND ug/kg 09/03/15 14:38 534-52-108/31/15 17:30903090310
2,4-Dinitrophenol ND ug/kg 09/03/15 14:38 51-28-508/31/15 17:302260073910
2,4-Dinitrotoluene ND ug/kg 09/03/15 14:38 121-14-208/31/15 17:30452084810
2,6-Dinitrotoluene ND ug/kg 09/03/15 14:38 606-20-208/31/15 17:30452094410
Di-n-octylphthalate ND ug/kg 09/03/15 14:38 117-84-008/31/15 17:30452094410
bis(2-Ethylhexyl)phthalate ND ug/kg 09/03/15 14:38 117-81-708/31/15 17:304520123010
Fluoranthene 22400 ug/kg 09/03/15 14:38 206-44-008/31/15 17:30452065710
Fluorene 1590J ug/kg 09/03/15 14:38 86-73-708/31/15 17:30452093110
Hexachloro-1,3-butadiene ND ug/kg 09/03/15 14:38 87-68-308/31/15 17:30452078010
Hexachlorobenzene ND ug/kg 09/03/15 14:38 118-74-108/31/15 17:30452057510
Hexachlorocyclopentadiene ND ug/kg 09/03/15 14:38 77-47-408/31/15 17:30452083510
Hexachloroethane ND ug/kg 09/03/15 14:38 67-72-108/31/15 17:304520119010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:SB-3 5'-7'Lab ID:92265398005 Collected:08/26/15 16:35 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Indeno(1,2,3-cd)pyrene 5310 ug/kg 09/03/15 14:38 193-39-508/31/15 17:30452093110
Isophorone ND ug/kg 09/03/15 14:38 78-59-108/31/15 17:304520101010
1-Methylnaphthalene ND ug/kg 09/03/15 14:38 90-12-008/31/15 17:304520118010
2-Methylnaphthalene ND ug/kg 09/03/15 14:38 91-57-608/31/15 17:30452097210
2-Methylphenol(o-Cresol)ND ug/kg 09/03/15 14:38 95-48-708/31/15 17:304520137010
3&4-Methylphenol(m&p Cresol)ND ug/kg 09/03/15 14:3808/31/15 17:304520178010
Naphthalene ND ug/kg 09/03/15 14:38 91-20-308/31/15 17:304520111010
2-Nitroaniline ND ug/kg 09/03/15 14:38 88-74-408/31/15 17:3022600140010
3-Nitroaniline ND ug/kg 09/03/15 14:38 99-09-208/31/15 17:3022600123010
4-Nitroaniline ND ug/kg 09/03/15 14:38 100-01-608/31/15 17:309030127010
Nitrobenzene ND ug/kg 09/03/15 14:38 98-95-308/31/15 17:304520123010
2-Nitrophenol ND ug/kg 09/03/15 14:38 88-75-508/31/15 17:304520109010
4-Nitrophenol ND ug/kg 09/03/15 14:38 100-02-708/31/15 17:302260080710
N-Nitrosodimethylamine ND ug/kg 09/03/15 14:38 62-75-908/31/15 17:304520146010
N-Nitroso-di-n-propylamine ND ug/kg 09/03/15 14:38 621-64-708/31/15 17:30452086210
N-Nitrosodiphenylamine ND ug/kg 09/03/15 14:38 86-30-608/31/15 17:304520134010
Pentachlorophenol ND ug/kg 09/03/15 14:38 87-86-508/31/15 17:302260082110
Phenanthrene 13300 ug/kg 09/03/15 14:38 85-01-808/31/15 17:30452075310
Phenol ND ug/kg 09/03/15 14:38 108-95-208/31/15 17:304520135010
Pyrene 16200 ug/kg 09/03/15 14:38 129-00-008/31/15 17:30452076610
1,2,4-Trichlorobenzene ND ug/kg 09/03/15 14:38 120-82-108/31/15 17:30452087610
2,4,5-Trichlorophenol ND ug/kg 09/03/15 14:38 95-95-408/31/15 17:304520140010
2,4,6-Trichlorophenol ND ug/kg 09/03/15 14:38 88-06-208/31/15 17:30452099910
Surrogates
Nitrobenzene-d5 (S)0 %09/03/15 14:38 4165-60-0 D3,S408/31/15 17:3023-110 10
2-Fluorobiphenyl (S)0 %09/03/15 14:38 321-60-8 S408/31/15 17:3030-110 10
Terphenyl-d14 (S)0 %09/03/15 14:38 1718-51-0 S408/31/15 17:3028-110 10
Phenol-d6 (S)0 %09/03/15 14:38 13127-88-3 S408/31/15 17:3022-110 10
2-Fluorophenol (S)0 %09/03/15 14:38 367-12-4 S408/31/15 17:3013-110 10
2,4,6-Tribromophenol (S)0 %09/03/15 14:38 118-79-6 S408/31/15 17:3027-110 10
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 08/31/15 23:12 67-64-1574057450
Benzene ND ug/kg 08/31/15 23:12 71-43-228791.8 50
Bromobenzene ND ug/kg 08/31/15 23:12 108-86-128711550
Bromochloromethane ND ug/kg 08/31/15 23:12 74-97-528797.6 50
Bromodichloromethane ND ug/kg 08/31/15 23:12 75-27-428710950
Bromoform ND ug/kg 08/31/15 23:12 75-25-228713250
Bromomethane ND ug/kg 08/31/15 23:12 74-83-957414450
2-Butanone (MEK)ND ug/kg 08/31/15 23:12 78-93-3574016650
n-Butylbenzene 160J ug/kg 08/31/15 23:12 104-51-828710350
sec-Butylbenzene 176J ug/kg 08/31/15 23:12 135-98-828791.8 50
tert-Butylbenzene ND ug/kg 08/31/15 23:12 98-06-628711550
Carbon tetrachloride ND ug/kg 08/31/15 23:12 56-23-528714950
Chlorobenzene ND ug/kg 08/31/15 23:12 108-90-728710950
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
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Huntersville, NC 28078
[phone]
Page 28 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:SB-3 5'-7'Lab ID:92265398005 Collected:08/26/15 16:35 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloroethane ND ug/kg 08/31/15 23:12 75-00-357413850
Chloroform ND ug/kg 08/31/15 23:12 67-66-328791.8 50
Chloromethane ND ug/kg 08/31/15 23:12 74-87-357413850
2-Chlorotoluene ND ug/kg 08/31/15 23:12 95-49-828797.6 50
4-Chlorotoluene ND ug/kg 08/31/15 23:12 106-43-428710350
1,2-Dibromo-3-chloropropane ND ug/kg 08/31/15 23:12 96-12-828720750
Dibromochloromethane ND ug/kg 08/31/15 23:12 124-48-128710350
1,2-Dibromoethane (EDB)ND ug/kg 08/31/15 23:12 106-93-428710350
Dibromomethane ND ug/kg 08/31/15 23:12 74-95-328714450
1,2-Dichlorobenzene ND ug/kg 08/31/15 23:12 95-50-128710950
1,3-Dichlorobenzene ND ug/kg 08/31/15 23:12 541-73-128711550
1,4-Dichlorobenzene ND ug/kg 08/31/15 23:12 106-46-728797.6 50
Dichlorodifluoromethane ND ug/kg 08/31/15 23:12 75-71-857420750
1,1-Dichloroethane ND ug/kg 08/31/15 23:12 75-34-328786.1 50
1,2-Dichloroethane ND ug/kg 08/31/15 23:12 107-06-228712650
1,1-Dichloroethene ND ug/kg 08/31/15 23:12 75-35-428710350
cis-1,2-Dichloroethene ND ug/kg 08/31/15 23:12 156-59-228780.4 50
trans-1,2-Dichloroethene ND ug/kg 08/31/15 23:12 156-60-528710950
1,2-Dichloropropane ND ug/kg 08/31/15 23:12 78-87-528797.6 50
1,3-Dichloropropane ND ug/kg 08/31/15 23:12 142-28-928710950
2,2-Dichloropropane ND ug/kg 08/31/15 23:12 594-20-728797.6 50
1,1-Dichloropropene ND ug/kg 08/31/15 23:12 563-58-628786.1 50
cis-1,3-Dichloropropene ND ug/kg 08/31/15 23:12 10061-01-528710350
trans-1,3-Dichloropropene ND ug/kg 08/31/15 23:12 10061-02-628786.1 50
Diisopropyl ether ND ug/kg 08/31/15 23:12 108-20-328797.6 50
Ethylbenzene ND ug/kg 08/31/15 23:12 100-41-428710350
Hexachloro-1,3-butadiene ND ug/kg 08/31/15 23:12 87-68-328711550
2-Hexanone ND ug/kg 08/31/15 23:12 591-78-6287022450
Isopropylbenzene (Cumene)115J ug/kg 08/31/15 23:12 98-82-828710950
p-Isopropyltoluene ND ug/kg 08/31/15 23:12 99-87-628797.6 50
Methylene Chloride 220J ug/kg 08/31/15 23:12 75-09-2 B115017250
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/31/15 23:12 108-10-1287021250
Methyl-tert-butyl ether ND ug/kg 08/31/15 23:12 1634-04-428786.1 50
Naphthalene 612 ug/kg 08/31/15 23:12 91-20-3 B28768.9 50
n-Propylbenzene 326 ug/kg 08/31/15 23:12 103-65-128797.6 50
Styrene ND ug/kg 08/31/15 23:12 100-42-528710350
1,1,1,2-Tetrachloroethane ND ug/kg 08/31/15 23:12 630-20-628712150
1,1,2,2-Tetrachloroethane ND ug/kg 08/31/15 23:12 79-34-528710950
Tetrachloroethene ND ug/kg 08/31/15 23:12 127-18-428797.6 50
Toluene ND ug/kg 08/31/15 23:12 108-88-328710350
1,2,3-Trichlorobenzene ND ug/kg 08/31/15 23:12 87-61-628712650
1,2,4-Trichlorobenzene ND ug/kg 08/31/15 23:12 120-82-128791.8 50
1,1,1-Trichloroethane ND ug/kg 08/31/15 23:12 71-55-628710350
1,1,2-Trichloroethane ND ug/kg 08/31/15 23:12 79-00-528712150
Trichloroethene ND ug/kg 08/31/15 23:12 79-01-628712150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Sample:SB-3 5'-7'Lab ID:92265398005 Collected:08/26/15 16:35 Received:08/27/15 12:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 08/31/15 23:12 75-69-428712650
1,2,3-Trichloropropane ND ug/kg 08/31/15 23:12 96-18-428791.8 50
1,2,4-Trimethylbenzene 181J ug/kg 08/31/15 23:12 95-63-628711550
1,3,5-Trimethylbenzene ND ug/kg 08/31/15 23:12 108-67-828710350
Vinyl acetate ND ug/kg 08/31/15 23:12 108-05-4287050550
Vinyl chloride ND ug/kg 08/31/15 23:12 75-01-457410350
Xylene (Total)ND ug/kg 08/31/15 23:12 1330-20-757420750
m&p-Xylene ND ug/kg 08/31/15 23:12 179601-23-157420750
o-Xylene ND ug/kg 08/31/15 23:12 95-47-628710950
Surrogates
Toluene-d8 (S)100 %08/31/15 23:12 2037-26-5 D370-130 50
4-Bromofluorobenzene (S)93 %08/31/15 23:12 460-00-470-130 50
1,2-Dichloroethane-d4 (S)91 %08/31/15 23:12 17060-07-070-132 50
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 26.9 %08/28/15 19:390.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/33184
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92265398001, 92265398002, 92265398003, 92265398004, 92265398005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1545121
Associated Lab Samples:92265398001, 92265398002, 92265398003, 92265398004, 92265398005
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.4 08/31/15 12:14
1,1,1-Trichloroethane ug/kg ND 5.4 08/31/15 12:14
1,1,2,2-Tetrachloroethane ug/kg ND 5.4 08/31/15 12:14
1,1,2-Trichloroethane ug/kg ND 5.4 08/31/15 12:14
1,1-Dichloroethane ug/kg ND 5.4 08/31/15 12:14
1,1-Dichloroethene ug/kg ND 5.4 08/31/15 12:14
1,1-Dichloropropene ug/kg ND 5.4 08/31/15 12:14
1,2,3-Trichlorobenzene ug/kg ND 5.4 08/31/15 12:14
1,2,3-Trichloropropane ug/kg ND 5.4 08/31/15 12:14
1,2,4-Trichlorobenzene ug/kg ND 5.4 08/31/15 12:14
1,2,4-Trimethylbenzene ug/kg ND 5.4 08/31/15 12:14
1,2-Dibromo-3-chloropropane ug/kg ND 5.4 08/31/15 12:14
1,2-Dibromoethane (EDB)ug/kg ND 5.4 08/31/15 12:14
1,2-Dichlorobenzene ug/kg ND 5.4 08/31/15 12:14
1,2-Dichloroethane ug/kg ND 5.4 08/31/15 12:14
1,2-Dichloropropane ug/kg ND 5.4 08/31/15 12:14
1,3,5-Trimethylbenzene ug/kg ND 5.4 08/31/15 12:14
1,3-Dichlorobenzene ug/kg ND 5.4 08/31/15 12:14
1,3-Dichloropropane ug/kg ND 5.4 08/31/15 12:14
1,4-Dichlorobenzene ug/kg ND 5.4 08/31/15 12:14
2,2-Dichloropropane ug/kg ND 5.4 08/31/15 12:14
2-Butanone (MEK)ug/kg ND 108 08/31/15 12:14
2-Chlorotoluene ug/kg ND 5.4 08/31/15 12:14
2-Hexanone ug/kg ND 54.0 08/31/15 12:14
4-Chlorotoluene ug/kg ND 5.4 08/31/15 12:14
4-Methyl-2-pentanone (MIBK)ug/kg ND 54.0 08/31/15 12:14
Acetone ug/kg ND 108 08/31/15 12:14
Benzene ug/kg ND 5.4 08/31/15 12:14
Bromobenzene ug/kg ND 5.4 08/31/15 12:14
Bromochloromethane ug/kg ND 5.4 08/31/15 12:14
Bromodichloromethane ug/kg ND 5.4 08/31/15 12:14
Bromoform ug/kg ND 5.4 08/31/15 12:14
Bromomethane ug/kg ND 10.8 08/31/15 12:14
Carbon tetrachloride ug/kg ND 5.4 08/31/15 12:14
Chlorobenzene ug/kg ND 5.4 08/31/15 12:14
Chloroethane ug/kg ND 10.8 08/31/15 12:14
Chloroform ug/kg ND 5.4 08/31/15 12:14
Chloromethane ug/kg ND 10.8 08/31/15 12:14
cis-1,2-Dichloroethene ug/kg ND 5.4 08/31/15 12:14
cis-1,3-Dichloropropene ug/kg ND 5.4 08/31/15 12:14
Dibromochloromethane ug/kg ND 5.4 08/31/15 12:14
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1545121
Associated Lab Samples:92265398001, 92265398002, 92265398003, 92265398004, 92265398005
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 5.4 08/31/15 12:14
Dichlorodifluoromethane ug/kg ND 10.8 08/31/15 12:14
Diisopropyl ether ug/kg ND 5.4 08/31/15 12:14
Ethylbenzene ug/kg ND 5.4 08/31/15 12:14
Hexachloro-1,3-butadiene ug/kg ND 5.4 08/31/15 12:14
Isopropylbenzene (Cumene)ug/kg ND 5.4 08/31/15 12:14
m&p-Xylene ug/kg ND 10.8 08/31/15 12:14
Methyl-tert-butyl ether ug/kg ND 5.4 08/31/15 12:14
Methylene Chloride ug/kg 4.5J 21.6 08/31/15 12:14
n-Butylbenzene ug/kg ND 5.4 08/31/15 12:14
n-Propylbenzene ug/kg ND 5.4 08/31/15 12:14
Naphthalene ug/kg 2.2J 5.4 08/31/15 12:14
o-Xylene ug/kg ND 5.4 08/31/15 12:14
p-Isopropyltoluene ug/kg ND 5.4 08/31/15 12:14
sec-Butylbenzene ug/kg ND 5.4 08/31/15 12:14
Styrene ug/kg ND 5.4 08/31/15 12:14
tert-Butylbenzene ug/kg ND 5.4 08/31/15 12:14
Tetrachloroethene ug/kg ND 5.4 08/31/15 12:14
Toluene ug/kg ND 5.4 08/31/15 12:14
trans-1,2-Dichloroethene ug/kg ND 5.4 08/31/15 12:14
trans-1,3-Dichloropropene ug/kg ND 5.4 08/31/15 12:14
Trichloroethene ug/kg ND 5.4 08/31/15 12:14
Trichlorofluoromethane ug/kg ND 5.4 08/31/15 12:14
Vinyl acetate ug/kg ND 54.0 08/31/15 12:14
Vinyl chloride ug/kg ND 10.8 08/31/15 12:14
Xylene (Total)ug/kg ND 10.8 08/31/15 12:14
1,2-Dichloroethane-d4 (S)%94 70-132 08/31/15 12:14
4-Bromofluorobenzene (S)%94 70-130 08/31/15 12:14
Toluene-d8 (S)%101 70-130 08/31/15 12:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1545122LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 59.962.3 96 74-137
1,1,1-Trichloroethane ug/kg 59.962.3 96 67-140
1,1,2,2-Tetrachloroethane ug/kg 58.362.3 94 72-141
1,1,2-Trichloroethane ug/kg 62.962.3 101 78-138
1,1-Dichloroethane ug/kg 60.862.3 98 69-134
1,1-Dichloroethene ug/kg 73.562.3 118 67-138
1,1-Dichloropropene ug/kg 67.162.3 108 69-139
1,2,3-Trichlorobenzene ug/kg 67.562.3 108 70-146
1,2,3-Trichloropropane ug/kg 58.262.3 93 69-144
1,2,4-Trichlorobenzene ug/kg 66.762.3 107 68-148
1,2,4-Trimethylbenzene ug/kg 67.462.3 108 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1545122LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 63.662.3 102 65-140
1,2-Dibromoethane (EDB)ug/kg 61.262.3 98 77-135
1,2-Dichlorobenzene ug/kg 67.462.3 108 77-141
1,2-Dichloroethane ug/kg 55.362.3 89 65-137
1,2-Dichloropropane ug/kg 66.162.3 106 72-136
1,3,5-Trimethylbenzene ug/kg 67.962.3 109 76-133
1,3-Dichlorobenzene ug/kg 69.462.3 111 74-138
1,3-Dichloropropane ug/kg 61.562.3 99 71-139
1,4-Dichlorobenzene ug/kg 66.662.3 107 76-138
2,2-Dichloropropane ug/kg 60.562.3 97 68-137
2-Butanone (MEK)ug/kg 128125 102 58-147
2-Chlorotoluene ug/kg 71.362.3 114 73-139
2-Hexanone ug/kg 131125 105 62-145
4-Chlorotoluene ug/kg 67.662.3 108 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 137125 110 64-149
Acetone ug/kg 119J125 95 53-153
Benzene ug/kg 67.462.3 108 73-135
Bromobenzene ug/kg 70.062.3 112 75-133
Bromochloromethane ug/kg 64.262.3 103 73-134
Bromodichloromethane ug/kg 61.262.3 98 71-135
Bromoform ug/kg 55.262.3 88 66-141
Bromomethane ug/kg 80.162.3 128 53-160
Carbon tetrachloride ug/kg 59.462.3 95 60-145
Chlorobenzene ug/kg 62.562.3 100 78-130
Chloroethane ug/kg 68.862.3 110 64-149
Chloroform ug/kg 60.862.3 98 70-134
Chloromethane ug/kg 66.262.3 106 52-150
cis-1,2-Dichloroethene ug/kg 63.562.3 102 70-133
cis-1,3-Dichloropropene ug/kg 64.262.3 103 68-134
Dibromochloromethane ug/kg 59.962.3 96 71-138
Dibromomethane ug/kg 57.862.3 93 74-130
Dichlorodifluoromethane ug/kg 56.062.3 90 40-160
Diisopropyl ether ug/kg 64.962.3 104 69-141
Ethylbenzene ug/kg 61.962.3 99 75-133
Hexachloro-1,3-butadiene ug/kg 64.362.3 103 68-143
Isopropylbenzene (Cumene)ug/kg 67.062.3 107 76-143
m&p-Xylene ug/kg 122125 98 75-136
Methyl-tert-butyl ether ug/kg 60.362.3 97 68-144
Methylene Chloride ug/kg 65.362.3 105 45-154
n-Butylbenzene ug/kg 68.862.3 110 72-137
n-Propylbenzene ug/kg 67.462.3 108 76-136
Naphthalene ug/kg 70.062.3 112 68-151
o-Xylene ug/kg 63.162.3 101 76-141
p-Isopropyltoluene ug/kg 67.862.3 109 76-140
sec-Butylbenzene ug/kg 71.162.3 114 79-139
Styrene ug/kg 65.162.3 104 79-137
tert-Butylbenzene ug/kg 60.662.3 97 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1545122LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 55.262.3 89 71-138
Toluene ug/kg 64.262.3 103 74-131
trans-1,2-Dichloroethene ug/kg 67.062.3 108 67-135
trans-1,3-Dichloropropene ug/kg 62.462.3 100 65-146
Trichloroethene ug/kg 62.162.3 100 67-135
Trichlorofluoromethane ug/kg 59.262.3 95 59-144
Vinyl acetate ug/kg 91.6 F31257340-160
Vinyl chloride ug/kg 70.262.3 113 56-141
Xylene (Total)ug/kg 185187 99 76-137
1,2-Dichloroethane-d4 (S)%90 70-132
4-Bromofluorobenzene (S)%92 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/37442
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:92265398001, 92265398002, 92265398003, 92265398004, 92265398005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1545554
Associated Lab Samples:92265398001, 92265398002, 92265398003, 92265398004, 92265398005
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 09/02/15 09:31
1,2-Dichlorobenzene ug/kg ND 330 09/02/15 09:31
1,3-Dichlorobenzene ug/kg ND 330 09/02/15 09:31
1,4-Dichlorobenzene ug/kg ND 330 09/02/15 09:31
1-Methylnaphthalene ug/kg ND 330 09/02/15 09:31
2,4,5-Trichlorophenol ug/kg ND 330 09/02/15 09:31
2,4,6-Trichlorophenol ug/kg ND 330 09/02/15 09:31
2,4-Dichlorophenol ug/kg ND 330 09/02/15 09:31
2,4-Dimethylphenol ug/kg ND 330 09/02/15 09:31
2,4-Dinitrophenol ug/kg ND 1650 09/02/15 09:31
2,4-Dinitrotoluene ug/kg ND 330 09/02/15 09:31
2,6-Dinitrotoluene ug/kg ND 330 09/02/15 09:31
2-Chloronaphthalene ug/kg ND 330 09/02/15 09:31
2-Chlorophenol ug/kg ND 330 09/02/15 09:31
2-Methylnaphthalene ug/kg ND 330 09/02/15 09:31
2-Methylphenol(o-Cresol)ug/kg ND 330 09/02/15 09:31
2-Nitroaniline ug/kg ND 1650 09/02/15 09:31
2-Nitrophenol ug/kg ND 330 09/02/15 09:31
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 09/02/15 09:31
3,3'-Dichlorobenzidine ug/kg ND 1650 09/02/15 09:31
3-Nitroaniline ug/kg ND 1650 09/02/15 09:31
4,6-Dinitro-2-methylphenol ug/kg ND 660 09/02/15 09:31
4-Bromophenylphenyl ether ug/kg ND 330 09/02/15 09:31
4-Chloro-3-methylphenol ug/kg ND 660 09/02/15 09:31
4-Chloroaniline ug/kg ND 1650 09/02/15 09:31
4-Chlorophenylphenyl ether ug/kg ND 330 09/02/15 09:31
4-Nitroaniline ug/kg ND 660 09/02/15 09:31
4-Nitrophenol ug/kg 127J 1650 09/02/15 09:31
Acenaphthene ug/kg ND 330 09/02/15 09:31
Acenaphthylene ug/kg ND 330 09/02/15 09:31
Aniline ug/kg ND 330 09/02/15 09:31
Anthracene ug/kg ND 330 09/02/15 09:31
Benzo(a)anthracene ug/kg ND 330 09/02/15 09:31
Benzo(a)pyrene ug/kg ND 330 09/02/15 09:31
Benzo(b)fluoranthene ug/kg ND 330 09/02/15 09:31
Benzo(g,h,i)perylene ug/kg ND 330 09/02/15 09:31
Benzo(k)fluoranthene ug/kg ND 330 09/02/15 09:31
Benzoic Acid ug/kg ND 1650 09/02/15 09:31
Benzyl alcohol ug/kg ND 660 09/02/15 09:31
bis(2-Chloroethoxy)methane ug/kg ND 330 09/02/15 09:31
bis(2-Chloroethyl) ether ug/kg ND 330 09/02/15 09:31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1545554
Associated Lab Samples:92265398001, 92265398002, 92265398003, 92265398004, 92265398005
Matrix:Solid
Analyzed
bis(2-Chloroisopropyl) ether ug/kg ND 330 09/02/15 09:31
bis(2-Ethylhexyl)phthalate ug/kg ND 330 09/02/15 09:31
Butylbenzylphthalate ug/kg ND 330 09/02/15 09:31
Chrysene ug/kg 57.8J 330 09/02/15 09:31
Di-n-butylphthalate ug/kg ND 330 09/02/15 09:31
Di-n-octylphthalate ug/kg ND 330 09/02/15 09:31
Dibenz(a,h)anthracene ug/kg ND 330 09/02/15 09:31
Dibenzofuran ug/kg ND 330 09/02/15 09:31
Diethylphthalate ug/kg ND 330 09/02/15 09:31
Dimethylphthalate ug/kg ND 330 09/02/15 09:31
Fluoranthene ug/kg ND 330 09/02/15 09:31
Fluorene ug/kg ND 330 09/02/15 09:31
Hexachloro-1,3-butadiene ug/kg ND 330 09/02/15 09:31
Hexachlorobenzene ug/kg ND 330 09/02/15 09:31
Hexachlorocyclopentadiene ug/kg ND 330 09/02/15 09:31
Hexachloroethane ug/kg ND 330 09/02/15 09:31
Indeno(1,2,3-cd)pyrene ug/kg ND 330 09/02/15 09:31
Isophorone ug/kg ND 330 09/02/15 09:31
N-Nitroso-di-n-propylamine ug/kg ND 330 09/02/15 09:31
N-Nitrosodimethylamine ug/kg ND 330 09/02/15 09:31
N-Nitrosodiphenylamine ug/kg ND 330 09/02/15 09:31
Naphthalene ug/kg ND 330 09/02/15 09:31
Nitrobenzene ug/kg ND 330 09/02/15 09:31
Pentachlorophenol ug/kg ND 1650 09/02/15 09:31
Phenanthrene ug/kg ND 330 09/02/15 09:31
Phenol ug/kg ND 330 09/02/15 09:31
Pyrene ug/kg ND 330 09/02/15 09:31
2,4,6-Tribromophenol (S)%94 27-110 09/02/15 09:31
2-Fluorobiphenyl (S)%75 30-110 09/02/15 09:31
2-Fluorophenol (S)%76 13-110 09/02/15 09:31
Nitrobenzene-d5 (S)%79 23-110 09/02/15 09:31
Phenol-d6 (S)%76 22-110 09/02/15 09:31
Terphenyl-d14 (S)%101 28-110 09/02/15 09:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1545555LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 14901670 89 36-120
1,2-Dichlorobenzene ug/kg 13501670 81 41-120
1,3-Dichlorobenzene ug/kg 12901670 77 66-120
1,4-Dichlorobenzene ug/kg 12901670 78 42-120
1-Methylnaphthalene ug/kg 14501670 87 40-120
2,4,5-Trichlorophenol ug/kg 13401670 81 37-120
2,4,6-Trichlorophenol ug/kg 14801670 89 40-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1545555LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dichlorophenol ug/kg 15201670 91 33-120
2,4-Dimethylphenol ug/kg 14501670 87 36-120
2,4-Dinitrophenol ug/kg 76108330 91 22-121
2,4-Dinitrotoluene ug/kg 15901670 95 60-120
2,6-Dinitrotoluene ug/kg 15101670 91 54-120
2-Chloronaphthalene ug/kg 13501670 81 41-120
2-Chlorophenol ug/kg 13301670 80 39-120
2-Methylnaphthalene ug/kg 14001670 84 26-120
2-Methylphenol(o-Cresol)ug/kg 12201670 73 41-120
2-Nitroaniline ug/kg 24103330 72 45-120
2-Nitrophenol ug/kg 14801670 89 35-120
3&4-Methylphenol(m&p Cresol)ug/kg 11801670 71 35-120
3,3'-Dichlorobenzidine ug/kg 28503330 85 16-125
3-Nitroaniline ug/kg 28003330 84 45-120
4,6-Dinitro-2-methylphenol ug/kg 33003330 99 46-120
4-Bromophenylphenyl ether ug/kg 14701670 88 36-120
4-Chloro-3-methylphenol ug/kg 30303330 91 37-120
4-Chloroaniline ug/kg 25003330 75 35-120
4-Chlorophenylphenyl ether ug/kg 14801670 89 30-120
4-Nitroaniline ug/kg 30303330 91 48-120
4-Nitrophenol ug/kg 80508330 97 43-120
Acenaphthene ug/kg 13401670 81 46-120
Acenaphthylene ug/kg 14001670 84 46-120
Aniline ug/kg 10601670 64 33-120
Anthracene ug/kg 14901670 90 63-120
Benzo(a)anthracene ug/kg 14901670 90 61-120
Benzo(a)pyrene ug/kg 16001670 96 59-120
Benzo(b)fluoranthene ug/kg 16201670 97 55-120
Benzo(g,h,i)perylene ug/kg 14701670 88 57-120
Benzo(k)fluoranthene ug/kg 19101670 115 56-120
Benzoic Acid ug/kg 52508330 63 13-120
Benzyl alcohol ug/kg 25003330 75 34-120
bis(2-Chloroethoxy)methane ug/kg 12901670 77 21-120
bis(2-Chloroethyl) ether ug/kg 10601670 64 25-120
bis(2-Chloroisopropyl) ether ug/kg 10201670 61 13-120
bis(2-Ethylhexyl)phthalate ug/kg 15501670 93 56-123
Butylbenzylphthalate ug/kg 15401670 93 57-120
Chrysene ug/kg 14101670 85 64-120
Di-n-butylphthalate ug/kg 16501670 99 58-120
Di-n-octylphthalate ug/kg 14101670 85 47-121
Dibenz(a,h)anthracene ug/kg 15901670 95 56-120
Dibenzofuran ug/kg 14201670 85 43-120
Diethylphthalate ug/kg 15601670 94 55-120
Dimethylphthalate ug/kg 14701670 88 54-120
Fluoranthene ug/kg 16601670 100 61-120
Fluorene ug/kg 14901670 90 51-120
Hexachloro-1,3-butadiene ug/kg 15501670 93 22-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
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[phone]
Page 37 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1545555LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 16901670 102 53-120
Hexachlorocyclopentadiene ug/kg 13801670 83 18-150
Hexachloroethane ug/kg 13201670 79 39-120
Indeno(1,2,3-cd)pyrene ug/kg 15601670 94 58-120
Isophorone ug/kg 12301670 74 38-120
N-Nitroso-di-n-propylamine ug/kg 11601670 70 30-120
N-Nitrosodimethylamine ug/kg 11101670 67 32-120
N-Nitrosodiphenylamine ug/kg 13401670 80 50-120
Naphthalene ug/kg 13501670 81 38-120
Nitrobenzene ug/kg 12501670 75 37-120
Pentachlorophenol ug/kg 31303330 94 10-120
Phenanthrene ug/kg 14001670 84 62-120
Phenol ug/kg 13901670 83 37-120
Pyrene ug/kg 14901670 89 63-120
2,4,6-Tribromophenol (S)%98 27-110
2-Fluorobiphenyl (S)%77 30-110
2-Fluorophenol (S)%84 13-110
Nitrobenzene-d5 (S)%83 23-110
Phenol-d6 (S)%80 22-110
Terphenyl-d14 (S)%95 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1545556MATRIX SPIKE SAMPLE:
MSSpike
Result
92265315005
1,2,4-Trichlorobenzene ug/kg 13801880 74 18-119ND
1,2-Dichlorobenzene ug/kg 12401880 66 50-110ND
1,3-Dichlorobenzene ug/kg 12001880 64 27-110ND
1,4-Dichlorobenzene ug/kg 12201880 65 28-110ND
1-Methylnaphthalene ug/kg 14901880 80 24-116ND
2,4,5-Trichlorophenol ug/kg 13301880 71 28-110ND
2,4,6-Trichlorophenol ug/kg 13101880 70 17-117ND
2,4-Dichlorophenol ug/kg 13001880 69 21-128ND
2,4-Dimethylphenol ug/kg 5551880 30 10-120ND
2,4-Dinitrophenol ug/kg 82509360 88 10-107ND
2,4-Dinitrotoluene ug/kg 16001880 85 36-109ND
2,6-Dinitrotoluene ug/kg 15101880 80 32-110ND
2-Chloronaphthalene ug/kg 12801880 68 30-107ND
2-Chlorophenol ug/kg 11601880 62 14-106ND
2-Methylnaphthalene ug/kg 14501880 77 10-135ND
2-Methylphenol(o-Cresol)ug/kg 7781880 42 10-124ND
2-Nitroaniline ug/kg 23603740 63 26-116ND
2-Nitrophenol ug/kg 13401880 71 28-103ND
3&4-Methylphenol(m&p Cresol)ug/kg 8431880 45 10-109ND
3,3'-Dichlorobenzidine ug/kg 385J3740 10 10-150ND
3-Nitroaniline ug/kg 24903740 67 22-110ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1545556MATRIX SPIKE SAMPLE:
MSSpike
Result
92265315005
4,6-Dinitro-2-methylphenol ug/kg 33303740 89 13-121ND
4-Bromophenylphenyl ether ug/kg 14701880 78 31-109ND
4-Chloro-3-methylphenol ug/kg 27403740 73 13-128ND
4-Chloroaniline ug/kg 1550J3740 41 18-102ND
4-Chlorophenylphenyl ether ug/kg 14901880 80 29-112ND
4-Nitroaniline ug/kg 26103740 67 16-111ND
4-Nitrophenol ug/kg 76309360 79 14-135ND
Acenaphthene ug/kg 13201880 70 26-114ND
Acenaphthylene ug/kg 13401880 72 32-108ND
Aniline ug/kg 225J1880 12 10-107ND
Anthracene ug/kg 14501880 77 32-111ND
Benzo(a)anthracene ug/kg 14701880 74 25-117ND
Benzo(a)pyrene ug/kg 15101880 78 25-106ND
Benzo(b)fluoranthene ug/kg 16101880 86 24-110ND
Benzo(g,h,i)perylene ug/kg 13901880 74 19-112ND
Benzo(k)fluoranthene ug/kg 18601880 99 24-114ND
Benzoic Acid ug/kg 56909360 61 10-110ND
Benzyl alcohol ug/kg 23003740 61 24-106ND
bis(2-Chloroethoxy)methane ug/kg 12201880 65 13-119ND
bis(2-Chloroethyl) ether ug/kg 225J1880 12 10-134ND
bis(2-Chloroisopropyl) ether ug/kg 9521880 51 10-113ND
bis(2-Ethylhexyl)phthalate ug/kg 15301880 78 10-125ND
Butylbenzylphthalate ug/kg 15701880 80 18-110ND
Chrysene ug/kg 14201880 71 30-110ND
Di-n-butylphthalate ug/kg 15401880 79 19-112ND
Di-n-octylphthalate ug/kg 14801880 79 17-105ND
Dibenz(a,h)anthracene ug/kg 14301880 76 23-111ND
Dibenzofuran ug/kg 14201880 76 35-103ND
Diethylphthalate ug/kg 15401880 82 27-113ND
Dimethylphthalate ug/kg 14501880 77 26-111ND
Fluoranthene ug/kg 15701880 79 33-109ND
Fluorene ug/kg 15001880 80 32-113ND
Hexachloro-1,3-butadiene ug/kg 14701880 78 16-116ND
Hexachlorobenzene ug/kg 16701880 89 27-120ND
Hexachlorocyclopentadiene ug/kg 11901880 64 10-108ND
Hexachloroethane ug/kg 12501880 67 10-117ND
Indeno(1,2,3-cd)pyrene ug/kg 14701880 78 10-122ND
Isophorone ug/kg 12001880 64 28-114ND
N-Nitroso-di-n-propylamine ug/kg 11101880 59 27-113ND
N-Nitrosodimethylamine ug/kg 9291880 50 10-109ND
N-Nitrosodiphenylamine ug/kg 9491880 51 10-128ND
Naphthalene ug/kg 13201880 71 25-110ND
Nitrobenzene ug/kg 11501880 61 18-114ND
Pentachlorophenol ug/kg 30803740 80 10-122ND
Phenanthrene ug/kg 14001880 73 30-114ND
Phenol ug/kg 10401880 56 11-102ND
Pyrene ug/kg 14401880 72 25-116ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1545556MATRIX SPIKE SAMPLE:
MSSpike
Result
92265315005
2,4,6-Tribromophenol (S)%74 27-110
2-Fluorobiphenyl (S)%63 30-110
2-Fluorophenol (S)%54 13-110
Nitrobenzene-d5 (S)%65 23-110
Phenol-d6 (S)%56 22-110
Terphenyl-d14 (S)%80 28-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92265315008
1545557SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg 69.3J 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92265315008
1545557SAMPLE DUPLICATE:
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Chloroisopropyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg 57.0J 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2,4,6-Tribromophenol (S)%64 1876
2-Fluorobiphenyl (S)%61 1571
2-Fluorophenol (S)%41 2352
Nitrobenzene-d5 (S)%61 1370
Phenol-d6 (S)%46 2861
Terphenyl-d14 (S)%78 1288
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 41 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/8302
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92265398001, 92265398002, 92265398003, 92265398004, 92265398005
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92265369001
1544275SAMPLE DUPLICATE:
Percent Moisture %79.7 0 2579.6
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92265335002
1544276SAMPLE DUPLICATE:
Percent Moisture %7.7 9 258.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 46
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92265398
Atando Ave 71157718
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
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Huntersville, NC 28078
[phone]
Page 43 of 46
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92265398
Atando Ave 71157718
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92265398001 OEXT/37442 MSSV/11169MW-9 10'-15'EPA 3546 EPA 8270
92265398002 OEXT/37442 MSSV/11169MW-10 15'-18'EPA 3546 EPA 8270
92265398003 OEXT/37442 MSSV/11169SB-1 5'-7'EPA 3546 EPA 8270
92265398004 OEXT/37442 MSSV/11169SB-2 5'-7'EPA 3546 EPA 8270
92265398005 OEXT/37442 MSSV/11169SB-3 5'-7'EPA 3546 EPA 8270
92265398001 MSV/33184MW-9 10'-15'EPA 8260
92265398002 MSV/33184MW-10 15'-18'EPA 8260
92265398003 MSV/33184SB-1 5'-7'EPA 8260
92265398004 MSV/33184SB-2 5'-7'EPA 8260
92265398005 MSV/33184SB-3 5'-7'EPA 8260
92265398001 PMST/8302MW-9 10'-15'ASTM D2974-87
92265398002 PMST/8302MW-10 15'-18'ASTM D2974-87
92265398003 PMST/8302SB-1 5'-7'ASTM D2974-87
92265398004 PMST/8302SB-2 5'-7'ASTM D2974-87
92265398005 PMST/8302SB-3 5'-7'ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/03/2015 03:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 46
Page 45 of 46
Page 46 of 46
#=CL#
November 19, 2015
LIMS USE: FR - CARLO ZANON
LIMS OBJECT ID: 92276028
92276028
Project:
Pace Project No.:
RE:
Carlo Zanon
Terracon
2020 Starita Rd Suite E
Suite E
Charlotte, NC 28206
Attando Avenue Brownfields
Dear Carlo Zanon:
Enclosed are the analytical results for sample(s) received by the laboratory on November 13, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Huntersville, NC 28078
[phone]
Page 1 of 23
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Sample:SB-04 (1-2)Lab ID:92276028001 Collected:11/11/15 15:15 Received:11/13/15 08:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 11/16/15 18:10 67-64-11211
Benzene ND ug/kg 11/16/15 18:10 71-43-26.1 1
Bromobenzene ND ug/kg 11/16/15 18:10 108-86-16.1 1
Bromochloromethane ND ug/kg 11/16/15 18:10 74-97-56.1 1
Bromodichloromethane ND ug/kg 11/16/15 18:10 75-27-46.1 1
Bromoform ND ug/kg 11/16/15 18:10 75-25-26.1 1
Bromomethane ND ug/kg 11/16/15 18:10 74-83-912.1 1
2-Butanone (MEK)ND ug/kg 11/16/15 18:10 78-93-31211
n-Butylbenzene ND ug/kg 11/16/15 18:10 104-51-86.1 1
sec-Butylbenzene ND ug/kg 11/16/15 18:10 135-98-8 M16.1 1
tert-Butylbenzene ND ug/kg 11/16/15 18:10 98-06-66.1 1
Carbon tetrachloride ND ug/kg 11/16/15 18:10 56-23-56.1 1
Chlorobenzene ND ug/kg 11/16/15 18:10 108-90-76.1 1
Chloroethane ND ug/kg 11/16/15 18:10 75-00-312.1 1
Chloroform ND ug/kg 11/16/15 18:10 67-66-36.1 1
Chloromethane ND ug/kg 11/16/15 18:10 74-87-312.1 1
2-Chlorotoluene ND ug/kg 11/16/15 18:10 95-49-86.1 1
4-Chlorotoluene ND ug/kg 11/16/15 18:10 106-43-46.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 11/16/15 18:10 96-12-86.1 1
Dibromochloromethane ND ug/kg 11/16/15 18:10 124-48-16.1 1
1,2-Dibromoethane (EDB)ND ug/kg 11/16/15 18:10 106-93-46.1 1
Dibromomethane ND ug/kg 11/16/15 18:10 74-95-36.1 1
1,2-Dichlorobenzene ND ug/kg 11/16/15 18:10 95-50-16.1 1
1,3-Dichlorobenzene ND ug/kg 11/16/15 18:10 541-73-16.1 1
1,4-Dichlorobenzene ND ug/kg 11/16/15 18:10 106-46-76.1 1
Dichlorodifluoromethane ND ug/kg 11/16/15 18:10 75-71-812.1 1
1,1-Dichloroethane ND ug/kg 11/16/15 18:10 75-34-36.1 1
1,2-Dichloroethane ND ug/kg 11/16/15 18:10 107-06-26.1 1
1,1-Dichloroethene ND ug/kg 11/16/15 18:10 75-35-46.1 1
cis-1,2-Dichloroethene ND ug/kg 11/16/15 18:10 156-59-26.1 1
trans-1,2-Dichloroethene ND ug/kg 11/16/15 18:10 156-60-56.1 1
1,2-Dichloropropane ND ug/kg 11/16/15 18:10 78-87-56.1 1
1,3-Dichloropropane ND ug/kg 11/16/15 18:10 142-28-96.1 1
2,2-Dichloropropane ND ug/kg 11/16/15 18:10 594-20-76.1 1
1,1-Dichloropropene ND ug/kg 11/16/15 18:10 563-58-66.1 1
cis-1,3-Dichloropropene ND ug/kg 11/16/15 18:10 10061-01-56.1 1
trans-1,3-Dichloropropene ND ug/kg 11/16/15 18:10 10061-02-66.1 1
Diisopropyl ether ND ug/kg 11/16/15 18:10 108-20-36.1 1
Ethylbenzene ND ug/kg 11/16/15 18:10 100-41-46.1 1
Hexachloro-1,3-butadiene ND ug/kg 11/16/15 18:10 87-68-36.1 1
2-Hexanone ND ug/kg 11/16/15 18:10 591-78-660.5 1
Isopropylbenzene (Cumene)ND ug/kg 11/16/15 18:10 98-82-86.1 1
p-Isopropyltoluene ND ug/kg 11/16/15 18:10 99-87-66.1 1
Methylene Chloride ND ug/kg 11/16/15 18:10 75-09-224.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 11/16/15 18:10 108-10-160.5 1
Methyl-tert-butyl ether ND ug/kg 11/16/15 18:10 1634-04-46.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Sample:SB-04 (1-2)Lab ID:92276028001 Collected:11/11/15 15:15 Received:11/13/15 08:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Naphthalene ND ug/kg 11/16/15 18:10 91-20-36.1 1
n-Propylbenzene ND ug/kg 11/16/15 18:10 103-65-16.1 1
Styrene ND ug/kg 11/16/15 18:10 100-42-56.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 11/16/15 18:10 630-20-66.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 11/16/15 18:10 79-34-56.1 1
Tetrachloroethene 40.2 ug/kg 11/16/15 18:10 127-18-46.1 1
Toluene ND ug/kg 11/16/15 18:10 108-88-36.1 1
1,2,3-Trichlorobenzene ND ug/kg 11/16/15 18:10 87-61-6 M16.1 1
1,2,4-Trichlorobenzene ND ug/kg 11/16/15 18:10 120-82-1 M16.1 1
1,1,1-Trichloroethane ND ug/kg 11/16/15 18:10 71-55-66.1 1
1,1,2-Trichloroethane ND ug/kg 11/16/15 18:10 79-00-56.1 1
Trichloroethene ND ug/kg 11/16/15 18:10 79-01-66.1 1
Trichlorofluoromethane ND ug/kg 11/16/15 18:10 75-69-46.1 1
1,2,3-Trichloropropane ND ug/kg 11/16/15 18:10 96-18-46.1 1
1,2,4-Trimethylbenzene ND ug/kg 11/16/15 18:10 95-63-66.1 1
1,3,5-Trimethylbenzene ND ug/kg 11/16/15 18:10 108-67-86.1 1
Vinyl acetate ND ug/kg 11/16/15 18:10 108-05-4 M160.5 1
Vinyl chloride ND ug/kg 11/16/15 18:10 75-01-412.1 1
Xylene (Total)ND ug/kg 11/16/15 18:10 1330-20-712.1 1
m&p-Xylene ND ug/kg 11/16/15 18:10 179601-23-112.1 1
o-Xylene ND ug/kg 11/16/15 18:10 95-47-66.1 1
Surrogates
Toluene-d8 (S)98 %11/16/15 18:10 2037-26-570-130 1
4-Bromofluorobenzene (S)100 %11/16/15 18:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %11/16/15 18:10 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.5 %11/13/15 19:320.10 1
Sample:TRIP BLANK Lab ID:92276028002 Collected:11/11/15 00:00 Received:11/13/15 08:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 11/15/15 13:41 67-64-125.0 1
Benzene ND ug/L 11/15/15 13:41 71-43-21.0 1
Bromobenzene ND ug/L 11/15/15 13:41 108-86-11.0 1
Bromochloromethane ND ug/L 11/15/15 13:41 74-97-51.0 1
Bromodichloromethane ND ug/L 11/15/15 13:41 75-27-41.0 1
Bromoform ND ug/L 11/15/15 13:41 75-25-21.0 1
Bromomethane ND ug/L 11/15/15 13:41 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/15/15 13:41 78-93-35.0 1
Carbon tetrachloride ND ug/L 11/15/15 13:41 56-23-51.0 1
Chlorobenzene ND ug/L 11/15/15 13:41 108-90-71.0 1
Chloroethane ND ug/L 11/15/15 13:41 75-00-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Sample:TRIP BLANK Lab ID:92276028002 Collected:11/11/15 00:00 Received:11/13/15 08:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Chloroform ND ug/L 11/15/15 13:41 67-66-31.0 1
Chloromethane ND ug/L 11/15/15 13:41 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/15/15 13:41 95-49-81.0 1
4-Chlorotoluene ND ug/L 11/15/15 13:41 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/15/15 13:41 96-12-82.0 1
Dibromochloromethane ND ug/L 11/15/15 13:41 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/15/15 13:41 106-93-41.0 1
Dibromomethane ND ug/L 11/15/15 13:41 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/15/15 13:41 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/15/15 13:41 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/15/15 13:41 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 11/15/15 13:41 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/15/15 13:41 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/15/15 13:41 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/15/15 13:41 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/15/15 13:41 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/15/15 13:41 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/15/15 13:41 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/15/15 13:41 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/15/15 13:41 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/15/15 13:41 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/15/15 13:41 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/15/15 13:41 10061-02-61.0 1
Diisopropyl ether ND ug/L 11/15/15 13:41 108-20-31.0 1
Ethylbenzene ND ug/L 11/15/15 13:41 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 11/15/15 13:41 87-68-3 L31.0 1
2-Hexanone ND ug/L 11/15/15 13:41 591-78-65.0 1
p-Isopropyltoluene ND ug/L 11/15/15 13:41 99-87-61.0 1
Methylene Chloride ND ug/L 11/15/15 13:41 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/15/15 13:41 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 11/15/15 13:41 1634-04-41.0 1
Naphthalene ND ug/L 11/15/15 13:41 91-20-31.0 1
Styrene ND ug/L 11/15/15 13:41 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/15/15 13:41 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/15/15 13:41 79-34-51.0 1
Tetrachloroethene ND ug/L 11/15/15 13:41 127-18-41.0 1
Toluene ND ug/L 11/15/15 13:41 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 11/15/15 13:41 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 11/15/15 13:41 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/15/15 13:41 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/15/15 13:41 79-00-51.0 1
Trichloroethene ND ug/L 11/15/15 13:41 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/15/15 13:41 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/15/15 13:41 96-18-41.0 1
Vinyl acetate ND ug/L 11/15/15 13:41 108-05-42.0 1
Vinyl chloride ND ug/L 11/15/15 13:41 75-01-41.0 1
Xylene (Total)ND ug/L 11/15/15 13:41 1330-20-72.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Sample:TRIP BLANK Lab ID:92276028002 Collected:11/11/15 00:00 Received:11/13/15 08:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
m&p-Xylene ND ug/L 11/15/15 13:41 179601-23-12.0 1
o-Xylene ND ug/L 11/15/15 13:41 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)104 %11/15/15 13:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %11/15/15 13:41 17060-07-070-130 1
Toluene-d8 (S)102 %11/15/15 13:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34299
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92276028002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1607155
Associated Lab Samples:92276028002
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/15/15 13:06
1,1,1-Trichloroethane ug/L ND 1.0 11/15/15 13:06
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/15/15 13:06
1,1,2-Trichloroethane ug/L ND 1.0 11/15/15 13:06
1,1-Dichloroethane ug/L ND 1.0 11/15/15 13:06
1,1-Dichloroethene ug/L ND 1.0 11/15/15 13:06
1,1-Dichloropropene ug/L ND 1.0 11/15/15 13:06
1,2,3-Trichlorobenzene ug/L ND 1.0 11/15/15 13:06
1,2,3-Trichloropropane ug/L ND 1.0 11/15/15 13:06
1,2,4-Trichlorobenzene ug/L ND 1.0 11/15/15 13:06
1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/15/15 13:06
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/15/15 13:06
1,2-Dichlorobenzene ug/L ND 1.0 11/15/15 13:06
1,2-Dichloroethane ug/L ND 1.0 11/15/15 13:06
1,2-Dichloropropane ug/L ND 1.0 11/15/15 13:06
1,3-Dichlorobenzene ug/L ND 1.0 11/15/15 13:06
1,3-Dichloropropane ug/L ND 1.0 11/15/15 13:06
1,4-Dichlorobenzene ug/L ND 1.0 11/15/15 13:06
2,2-Dichloropropane ug/L ND 1.0 11/15/15 13:06
2-Butanone (MEK)ug/L ND 5.0 11/15/15 13:06
2-Chlorotoluene ug/L ND 1.0 11/15/15 13:06
2-Hexanone ug/L ND 5.0 11/15/15 13:06
4-Chlorotoluene ug/L ND 1.0 11/15/15 13:06
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/15/15 13:06
Acetone ug/L ND 25.0 11/15/15 13:06
Benzene ug/L ND 1.0 11/15/15 13:06
Bromobenzene ug/L ND 1.0 11/15/15 13:06
Bromochloromethane ug/L ND 1.0 11/15/15 13:06
Bromodichloromethane ug/L ND 1.0 11/15/15 13:06
Bromoform ug/L ND 1.0 11/15/15 13:06
Bromomethane ug/L ND 2.0 11/15/15 13:06
Carbon tetrachloride ug/L ND 1.0 11/15/15 13:06
Chlorobenzene ug/L ND 1.0 11/15/15 13:06
Chloroethane ug/L ND 1.0 11/15/15 13:06
Chloroform ug/L ND 1.0 11/15/15 13:06
Chloromethane ug/L ND 1.0 11/15/15 13:06
cis-1,2-Dichloroethene ug/L ND 1.0 11/15/15 13:06
cis-1,3-Dichloropropene ug/L ND 1.0 11/15/15 13:06
Dibromochloromethane ug/L ND 1.0 11/15/15 13:06
Dibromomethane ug/L ND 1.0 11/15/15 13:06
Dichlorodifluoromethane ug/L ND 1.0 11/15/15 13:06
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1607155
Associated Lab Samples:92276028002
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 1.0 11/15/15 13:06
Ethylbenzene ug/L ND 1.0 11/15/15 13:06
Hexachloro-1,3-butadiene ug/L ND 1.0 11/15/15 13:06
m&p-Xylene ug/L ND 2.0 11/15/15 13:06
Methyl-tert-butyl ether ug/L ND 1.0 11/15/15 13:06
Methylene Chloride ug/L ND 2.0 11/15/15 13:06
Naphthalene ug/L ND 1.0 11/15/15 13:06
o-Xylene ug/L ND 1.0 11/15/15 13:06
p-Isopropyltoluene ug/L ND 1.0 11/15/15 13:06
Styrene ug/L ND 1.0 11/15/15 13:06
Tetrachloroethene ug/L ND 1.0 11/15/15 13:06
Toluene ug/L ND 1.0 11/15/15 13:06
trans-1,2-Dichloroethene ug/L ND 1.0 11/15/15 13:06
trans-1,3-Dichloropropene ug/L ND 1.0 11/15/15 13:06
Trichloroethene ug/L ND 1.0 11/15/15 13:06
Trichlorofluoromethane ug/L ND 1.0 11/15/15 13:06
Vinyl acetate ug/L ND 2.0 11/15/15 13:06
Vinyl chloride ug/L ND 1.0 11/15/15 13:06
Xylene (Total)ug/L ND 2.0 11/15/15 13:06
1,2-Dichloroethane-d4 (S)%107 70-130 11/15/15 13:06
4-Bromofluorobenzene (S)%103 70-130 11/15/15 13:06
Toluene-d8 (S)%101 70-130 11/15/15 13:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1607156LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.250 96 70-130
1,1,1-Trichloroethane ug/L 53.550 107 70-130
1,1,2,2-Tetrachloroethane ug/L 53.050 106 70-130
1,1,2-Trichloroethane ug/L 51.150 102 70-130
1,1-Dichloroethane ug/L 55.250 110 70-130
1,1-Dichloroethene ug/L 58.350 117 70-132
1,1-Dichloropropene ug/L 54.150 108 70-130
1,2,3-Trichlorobenzene ug/L 54.850 110 70-135
1,2,3-Trichloropropane ug/L 55.250 110 70-130
1,2,4-Trichlorobenzene ug/L 51.550 103 70-134
1,2-Dibromo-3-chloropropane ug/L 47.950 96 70-130
1,2-Dibromoethane (EDB)ug/L 52.550 105 70-130
1,2-Dichlorobenzene ug/L 53.450 107 70-130
1,2-Dichloroethane ug/L 50.750 101 70-130
1,2-Dichloropropane ug/L 54.150 108 70-130
1,3-Dichlorobenzene ug/L 55.050 110 70-130
1,3-Dichloropropane ug/L 53.950 108 70-130
1,4-Dichlorobenzene ug/L 53.650 107 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1607156LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 55.550 111 58-145
2-Butanone (MEK)ug/L 117100 117 70-145
2-Chlorotoluene ug/L 57.450 115 70-130
2-Hexanone ug/L 112100 112 70-144
4-Chlorotoluene ug/L 54.650 109 70-130
4-Methyl-2-pentanone (MIBK)ug/L 111100 111 70-140
Acetone ug/L 117100 117 50-175
Benzene ug/L 56.250 112 70-130
Bromobenzene ug/L 54.150 108 70-130
Bromochloromethane ug/L 56.950 114 70-130
Bromodichloromethane ug/L 50.850 102 70-130
Bromoform ug/L 42.850 86 70-130
Bromomethane ug/L 49.650 99 54-130
Carbon tetrachloride ug/L 51.850 104 70-132
Chlorobenzene ug/L 52.750 105 70-130
Chloroethane ug/L 56.650 113 64-134
Chloroform ug/L 55.350 111 70-130
Chloromethane ug/L 64.350 129 64-130
cis-1,2-Dichloroethene ug/L 55.950 112 70-131
cis-1,3-Dichloropropene ug/L 52.050 104 70-130
Dibromochloromethane ug/L 47.250 94 70-130
Dibromomethane ug/L 50.350 101 70-131
Dichlorodifluoromethane ug/L 56.050 112 56-130
Diisopropyl ether ug/L 59.250 118 70-130
Ethylbenzene ug/L 54.850 110 70-130
Hexachloro-1,3-butadiene ug/L 67.6 L05013570-130
m&p-Xylene ug/L 111100 111 70-130
Methyl-tert-butyl ether ug/L 59.450 119 70-130
Methylene Chloride ug/L 53.250 106 63-130
Naphthalene ug/L 53.850 108 70-138
o-Xylene ug/L 51.350 103 70-130
p-Isopropyltoluene ug/L 53.450 107 70-130
Styrene ug/L 51.350 103 70-130
Tetrachloroethene ug/L 53.250 106 70-130
Toluene ug/L 55.750 111 70-130
trans-1,2-Dichloroethene ug/L 57.850 116 70-130
trans-1,3-Dichloropropene ug/L 50.450 101 70-132
Trichloroethene ug/L 53.550 107 70-130
Trichlorofluoromethane ug/L 54.550 109 62-133
Vinyl acetate ug/L 113100 113 66-157
Vinyl chloride ug/L 57.050 114 50-150
Xylene (Total)ug/L 162150 108 70-130
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%105 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1607157MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276008041
1607158
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 102 70-130106 420ND20.4 21.2
1,1,1-Trichloroethane ug/L 20 126 70-130125 120ND25.2 25.0
1,1,2,2-Tetrachloroethane ug/L 20 111 70-130115 420ND22.2 23.0
1,1,2-Trichloroethane ug/L 20 114 70-130116 220ND22.8 23.2
1,1-Dichloroethane ug/L M12013070-130133 220ND26.1 26.7
1,1-Dichloroethene ug/L 20 143 70-166140 220ND28.6 28.0
1,1-Dichloropropene ug/L 20 123 70-130122 120ND24.6 24.4
1,2,3-Trichlorobenzene ug/L 20 103 70-130105 220ND20.6 20.9
1,2,3-Trichloropropane ug/L 20 111 70-130117 520ND22.3 23.4
1,2,4-Trichlorobenzene ug/L 20 97 70-130100 220ND19.4 19.9
1,2-Dibromo-3-chloropropane ug/L 20 99 70-130107 820ND19.7 21.4
1,2-Dibromoethane (EDB)ug/L 20 110 70-130114 320ND22.1 22.8
1,2-Dichlorobenzene ug/L 20 109 70-130109 020ND21.8 21.7
1,2-Dichloroethane ug/L 20 117 70-130120 220ND23.4 24.0
1,2-Dichloropropane ug/L 20 120 70-130121 120ND24.0 24.3
1,3-Dichlorobenzene ug/L 20 115 70-130114 120ND23.0 22.8
1,3-Dichloropropane ug/L 20 114 70-130118 420ND22.7 23.6
1,4-Dichlorobenzene ug/L 20 113 70-130109 320ND22.6 21.9
2,2-Dichloropropane ug/L 20 113 70-130115 220ND22.5 22.9
2-Butanone (MEK)ug/L M14012970-130133 340ND51.4 53.2
2-Chlorotoluene ug/L 20 111 70-130111 120ND22.1 22.3
2-Hexanone ug/L 40 111 70-130119 840ND44.2 47.7
4-Chlorotoluene ug/L 20 117 70-130116 120ND23.4 23.1
4-Methyl-2-pentanone (MIBK)ug/L 40 118 70-130124 540ND47.2 49.6
Acetone ug/L M14013470-130138 340ND53.4 55.1
Benzene ug/L 20 124 70-148125 120ND24.8 25.1
Bromobenzene ug/L 20 116 70-130115 020ND23.1 23.1
Bromochloromethane ug/L 20 126 70-130129 320ND25.1 25.8
Bromodichloromethane ug/L 20 110 70-130114 320ND22.1 22.8
Bromoform ug/L 20 94 70-13096 220ND18.8 19.2
Bromomethane ug/L 20 100 70-130113 1220ND20.0 22.6
Carbon tetrachloride ug/L 20 117 70-130115 220ND23.3 23.0
Chlorobenzene ug/L 20 115 70-146113 220ND23.0 22.5
Chloroethane ug/L M12013470-130135 120ND26.9 27.1
Chloroform ug/L M12012770-130131 320ND25.3 26.1
Chloromethane ug/L M12015270-130150 220ND30.4 29.9
cis-1,2-Dichloroethene ug/L 20 125 70-130128 220ND25.0 25.6
cis-1,3-Dichloropropene ug/L 20 102 70-130104 320ND20.3 20.9
Dibromochloromethane ug/L 20 98 70-130100 120ND19.7 19.9
Dibromomethane ug/L 20 112 70-130115 320ND22.4 23.0
Dichlorodifluoromethane ug/L 20 127 70-130120 620ND25.4 24.1
Diisopropyl ether ug/L M12012770-130134 520ND25.4 26.7
Ethylbenzene ug/L 20 118 70-130114 420ND23.7 22.7
Hexachloro-1,3-butadiene ug/L M02013470-130138 320ND26.8 27.6
m&p-Xylene ug/L 40 118 70-130115 240ND47.1 46.2
Methyl-tert-butyl ether ug/L M12012770-130133 520ND25.3 26.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1607157MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92276008041
1607158
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Methylene Chloride ug/L 20 122 70-130123 120ND24.4 24.6
Naphthalene ug/L 20 105 70-130110 520ND21.0 22.1
o-Xylene ug/L 20 108 70-130105 220ND21.5 21.1
p-Isopropyltoluene ug/L 20 110 70-130111 120ND21.9 22.1
Styrene ug/L 20 107 70-130105 220ND21.3 20.9
Tetrachloroethene ug/L 20 111 70-130107 420ND22.1 21.4
Toluene ug/L 20 125 70-155122 220ND25.0 24.4
trans-1,2-Dichloroethene ug/L M12013470-130132 120ND26.8 26.5
trans-1,3-Dichloropropene ug/L 20 106 70-130110 420ND21.1 22.0
Trichloroethene ug/L 20 120 69-151116 420ND24.0 23.2
Trichlorofluoromethane ug/L M12013470-130128 520ND26.8 25.5
Vinyl acetate ug/L 40 107 70-130116 940ND42.7 46.5
Vinyl chloride ug/L M12013870-130139 120ND27.6 27.9
1,2-Dichloroethane-d4 (S)%103 70-130103
4-Bromofluorobenzene (S)%102 70-130103
Toluene-d8 (S)%100 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34305
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92276028001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1607357
Associated Lab Samples:92276028001
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.4 11/16/15 11:32
1,1,1-Trichloroethane ug/kg ND 5.4 11/16/15 11:32
1,1,2,2-Tetrachloroethane ug/kg ND 5.4 11/16/15 11:32
1,1,2-Trichloroethane ug/kg ND 5.4 11/16/15 11:32
1,1-Dichloroethane ug/kg ND 5.4 11/16/15 11:32
1,1-Dichloroethene ug/kg ND 5.4 11/16/15 11:32
1,1-Dichloropropene ug/kg ND 5.4 11/16/15 11:32
1,2,3-Trichlorobenzene ug/kg ND 5.4 11/16/15 11:32
1,2,3-Trichloropropane ug/kg ND 5.4 11/16/15 11:32
1,2,4-Trichlorobenzene ug/kg ND 5.4 11/16/15 11:32
1,2,4-Trimethylbenzene ug/kg ND 5.4 11/16/15 11:32
1,2-Dibromo-3-chloropropane ug/kg ND 5.4 11/16/15 11:32
1,2-Dibromoethane (EDB)ug/kg ND 5.4 11/16/15 11:32
1,2-Dichlorobenzene ug/kg ND 5.4 11/16/15 11:32
1,2-Dichloroethane ug/kg ND 5.4 11/16/15 11:32
1,2-Dichloropropane ug/kg ND 5.4 11/16/15 11:32
1,3,5-Trimethylbenzene ug/kg ND 5.4 11/16/15 11:32
1,3-Dichlorobenzene ug/kg ND 5.4 11/16/15 11:32
1,3-Dichloropropane ug/kg ND 5.4 11/16/15 11:32
1,4-Dichlorobenzene ug/kg ND 5.4 11/16/15 11:32
2,2-Dichloropropane ug/kg ND 5.4 11/16/15 11:32
2-Butanone (MEK)ug/kg ND 108 11/16/15 11:32
2-Chlorotoluene ug/kg ND 5.4 11/16/15 11:32
2-Hexanone ug/kg ND 53.8 11/16/15 11:32
4-Chlorotoluene ug/kg ND 5.4 11/16/15 11:32
4-Methyl-2-pentanone (MIBK)ug/kg ND 53.8 11/16/15 11:32
Acetone ug/kg ND 108 11/16/15 11:32
Benzene ug/kg ND 5.4 11/16/15 11:32
Bromobenzene ug/kg ND 5.4 11/16/15 11:32
Bromochloromethane ug/kg ND 5.4 11/16/15 11:32
Bromodichloromethane ug/kg ND 5.4 11/16/15 11:32
Bromoform ug/kg ND 5.4 11/16/15 11:32
Bromomethane ug/kg ND 10.8 11/16/15 11:32
Carbon tetrachloride ug/kg ND 5.4 11/16/15 11:32
Chlorobenzene ug/kg ND 5.4 11/16/15 11:32
Chloroethane ug/kg ND 10.8 11/16/15 11:32
Chloroform ug/kg ND 5.4 11/16/15 11:32
Chloromethane ug/kg ND 10.8 11/16/15 11:32
cis-1,2-Dichloroethene ug/kg ND 5.4 11/16/15 11:32
cis-1,3-Dichloropropene ug/kg ND 5.4 11/16/15 11:32
Dibromochloromethane ug/kg ND 5.4 11/16/15 11:32
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1607357
Associated Lab Samples:92276028001
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 5.4 11/16/15 11:32
Dichlorodifluoromethane ug/kg ND 10.8 11/16/15 11:32
Diisopropyl ether ug/kg ND 5.4 11/16/15 11:32
Ethylbenzene ug/kg ND 5.4 11/16/15 11:32
Hexachloro-1,3-butadiene ug/kg ND 5.4 11/16/15 11:32
Isopropylbenzene (Cumene)ug/kg ND 5.4 11/16/15 11:32
m&p-Xylene ug/kg ND 10.8 11/16/15 11:32
Methyl-tert-butyl ether ug/kg ND 5.4 11/16/15 11:32
Methylene Chloride ug/kg ND 21.5 11/16/15 11:32
n-Butylbenzene ug/kg ND 5.4 11/16/15 11:32
n-Propylbenzene ug/kg ND 5.4 11/16/15 11:32
Naphthalene ug/kg ND 5.4 11/16/15 11:32
o-Xylene ug/kg ND 5.4 11/16/15 11:32
p-Isopropyltoluene ug/kg ND 5.4 11/16/15 11:32
sec-Butylbenzene ug/kg ND 5.4 11/16/15 11:32
Styrene ug/kg ND 5.4 11/16/15 11:32
tert-Butylbenzene ug/kg ND 5.4 11/16/15 11:32
Tetrachloroethene ug/kg ND 5.4 11/16/15 11:32
Toluene ug/kg ND 5.4 11/16/15 11:32
trans-1,2-Dichloroethene ug/kg ND 5.4 11/16/15 11:32
trans-1,3-Dichloropropene ug/kg ND 5.4 11/16/15 11:32
Trichloroethene ug/kg ND 5.4 11/16/15 11:32
Trichlorofluoromethane ug/kg ND 5.4 11/16/15 11:32
Vinyl acetate ug/kg ND 53.8 11/16/15 11:32
Vinyl chloride ug/kg ND 10.8 11/16/15 11:32
Xylene (Total)ug/kg ND 10.8 11/16/15 11:32
1,2-Dichloroethane-d4 (S)%91 70-132 11/16/15 11:32
4-Bromofluorobenzene (S)%102 70-130 11/16/15 11:32
Toluene-d8 (S)%100 70-130 11/16/15 11:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1607358LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 79.068.9 115 74-137
1,1,1-Trichloroethane ug/kg 73.268.9 106 67-140
1,1,2,2-Tetrachloroethane ug/kg 68.268.9 99 72-141
1,1,2-Trichloroethane ug/kg 69.668.9 101 78-138
1,1-Dichloroethane ug/kg 67.268.9 98 69-134
1,1-Dichloroethene ug/kg 73.468.9 107 67-138
1,1-Dichloropropene ug/kg 71.668.9 104 69-139
1,2,3-Trichlorobenzene ug/kg 67.068.9 97 70-146
1,2,3-Trichloropropane ug/kg 73.168.9 106 69-144
1,2,4-Trichlorobenzene ug/kg 70.968.9 103 68-148
1,2,4-Trimethylbenzene ug/kg 73.068.9 106 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1607358LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 70.968.9 103 65-140
1,2-Dibromoethane (EDB)ug/kg 74.968.9 109 77-135
1,2-Dichlorobenzene ug/kg 73.968.9 107 77-141
1,2-Dichloroethane ug/kg 63.068.9 91 65-137
1,2-Dichloropropane ug/kg 66.568.9 97 72-136
1,3,5-Trimethylbenzene ug/kg 73.568.9 107 76-133
1,3-Dichlorobenzene ug/kg 76.168.9 110 74-138
1,3-Dichloropropane ug/kg 67.768.9 98 71-139
1,4-Dichlorobenzene ug/kg 72.268.9 105 76-138
2,2-Dichloropropane ug/kg 77.468.9 112 68-137
2-Butanone (MEK)ug/kg 110J138 80 58-147
2-Chlorotoluene ug/kg 71.568.9 104 73-139
2-Hexanone ug/kg 120138 87 62-145
4-Chlorotoluene ug/kg 71.668.9 104 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 132138 96 64-149
Acetone ug/kg 104J138 76 53-153
Benzene ug/kg 73.668.9 107 73-135
Bromobenzene ug/kg 67.868.9 98 75-133
Bromochloromethane ug/kg 71.768.9 104 73-134
Bromodichloromethane ug/kg 75.368.9 109 71-135
Bromoform ug/kg 79.268.9 115 66-141
Bromomethane ug/kg 97.068.9 141 53-160
Carbon tetrachloride ug/kg 83.968.9 122 60-145
Chlorobenzene ug/kg 72.868.9 106 78-130
Chloroethane ug/kg 77.368.9 112 64-149
Chloroform ug/kg 69.468.9 101 70-134
Chloromethane ug/kg 75.468.9 109 52-150
cis-1,2-Dichloroethene ug/kg 66.868.9 97 70-133
cis-1,3-Dichloropropene ug/kg 73.768.9 107 68-134
Dibromochloromethane ug/kg 78.468.9 114 71-138
Dibromomethane ug/kg 71.768.9 104 74-130
Dichlorodifluoromethane ug/kg 66.268.9 96 40-160
Diisopropyl ether ug/kg 60.868.9 88 69-141
Ethylbenzene ug/kg 72.568.9 105 75-133
Hexachloro-1,3-butadiene ug/kg 77.368.9 112 68-143
Isopropylbenzene (Cumene)ug/kg 81.368.9 118 76-143
m&p-Xylene ug/kg 148138 107 75-136
Methyl-tert-butyl ether ug/kg 67.168.9 97 68-144
Methylene Chloride ug/kg 63.168.9 92 45-154
n-Butylbenzene ug/kg 73.068.9 106 72-137
n-Propylbenzene ug/kg 71.568.9 104 76-136
Naphthalene ug/kg 64.568.9 94 68-151
o-Xylene ug/kg 73.368.9 106 76-141
p-Isopropyltoluene ug/kg 74.468.9 108 76-140
sec-Butylbenzene ug/kg 75.368.9 109 79-139
Styrene ug/kg 75.568.9 110 79-137
tert-Butylbenzene ug/kg 67.568.9 98 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1607358LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 67.468.9 98 71-138
Toluene ug/kg 73.868.9 107 74-131
trans-1,2-Dichloroethene ug/kg 70.768.9 103 67-135
trans-1,3-Dichloropropene ug/kg 77.068.9 112 65-146
Trichloroethene ug/kg 76.968.9 112 67-135
Trichlorofluoromethane ug/kg 75.168.9 109 59-144
Vinyl acetate ug/kg 128 F31389340-160
Vinyl chloride ug/kg 76.768.9 111 56-141
Xylene (Total)ug/kg 221207 107 76-137
1,2-Dichloroethane-d4 (S)%91 70-132
4-Bromofluorobenzene (S)%107 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1608080MATRIX SPIKE SAMPLE:
MSSpike
Result
92276028001
1,1,1,2-Tetrachloroethane ug/kg 25.723.1 111 70-130ND
1,1,1-Trichloroethane ug/kg 25.623.1 111 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 25.023.1 108 70-130ND
1,1,2-Trichloroethane ug/kg 23.223.1 100 70-130ND
1,1-Dichloroethane ug/kg 23.323.1 101 70-130ND
1,1-Dichloroethene ug/kg 21.623.1 94 49-180ND
1,1-Dichloropropene ug/kg 27.023.1 117 70-130ND
1,2,3-Trichlorobenzene ug/kg 12.2 M123.1 53 70-130ND
1,2,3-Trichloropropane ug/kg 25.523.1 111 70-130ND
1,2,4-Trichlorobenzene ug/kg 13.8 M123.1 60 70-130ND
1,2,4-Trimethylbenzene ug/kg 26.623.1 114 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 26.323.1 114 70-130ND
1,2-Dibromoethane (EDB)ug/kg 25.623.1 111 70-130ND
1,2-Dichlorobenzene ug/kg 22.423.1 97 70-130ND
1,2-Dichloroethane ug/kg 22.123.1 96 70-130ND
1,2-Dichloropropane ug/kg 23.223.1 101 70-130ND
1,3,5-Trimethylbenzene ug/kg 27.823.1 120 70-130ND
1,3-Dichlorobenzene ug/kg 25.223.1 109 70-130ND
1,3-Dichloropropane ug/kg 23.923.1 103 70-130ND
1,4-Dichlorobenzene ug/kg 24.223.1 105 70-130ND
2,2-Dichloropropane ug/kg 28.023.1 121 70-130ND
2-Butanone (MEK)ug/kg 44J46.1 95 70-130ND
2-Chlorotoluene ug/kg 27.723.1 120 70-130ND
2-Hexanone ug/kg 41.7J46.1 90 70-130ND
4-Chlorotoluene ug/kg 26.823.1 116 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 44.4J46.1 96 70-130ND
Acetone ug/kg 55.4J46.1 120 70-130ND
Benzene ug/kg 26.123.1 113 50-166ND
Bromobenzene ug/kg 25.723.1 111 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1608080MATRIX SPIKE SAMPLE:
MSSpike
Result
92276028001
Bromochloromethane ug/kg 25.923.1 112 70-130ND
Bromodichloromethane ug/kg 24.123.1 104 70-130ND
Bromoform ug/kg 24.223.1 105 70-130ND
Bromomethane ug/kg 26.823.1 116 70-130ND
Carbon tetrachloride ug/kg 27.823.1 120 70-130ND
Chlorobenzene ug/kg 24.523.1 106 43-169ND
Chloroethane ug/kg 23.123.1 100 70-130ND
Chloroform ug/kg 24.923.1 108 70-130ND
Chloromethane ug/kg 20.723.1 89 70-130ND
cis-1,2-Dichloroethene ug/kg 24.323.1 105 70-130ND
cis-1,3-Dichloropropene ug/kg 24.223.1 105 70-130ND
Dibromochloromethane ug/kg 25.023.1 108 70-130ND
Dibromomethane ug/kg 25.023.1 108 70-130ND
Dichlorodifluoromethane ug/kg 21.023.1 91 70-130ND
Diisopropyl ether ug/kg 20.723.1 90 70-130ND
Ethylbenzene ug/kg 25.123.1 109 70-130ND
Hexachloro-1,3-butadiene ug/kg 19.923.1 86 70-130ND
Isopropylbenzene (Cumene)ug/kg 27.323.1 118 70-130ND
m&p-Xylene ug/kg 50.646.1 109 70-130ND
Methyl-tert-butyl ether ug/kg 21.723.1 94 70-130ND
Methylene Chloride ug/kg 20.3J23.1 88 70-130ND
n-Butylbenzene ug/kg 26.823.1 116 70-130ND
n-Propylbenzene ug/kg 29.523.1 128 70-130ND
Naphthalene ug/kg 16.323.1 71 70-130ND
o-Xylene ug/kg 23.523.1 102 70-130ND
p-Isopropyltoluene ug/kg 28.323.1 122 70-130ND
sec-Butylbenzene ug/kg 30.8 M123.1 133 70-130ND
Styrene ug/kg 23.023.1 99 70-130ND
tert-Butylbenzene ug/kg 27.023.1 117 70-130ND
Tetrachloroethene ug/kg 58.823.1 80 70-13040.2
Toluene ug/kg 25.923.1 110 52-163ND
trans-1,2-Dichloroethene ug/kg 23.623.1 102 70-130ND
trans-1,3-Dichloropropene ug/kg 22.923.1 99 70-130ND
Trichloroethene ug/kg 25.223.1 107 49-167ND
Trichlorofluoromethane ug/kg 22.023.1 95 70-130ND
Vinyl acetate ug/kg 18.8J M146.1 41 70-130ND
Vinyl chloride ug/kg 22.423.1 97 70-130ND
1,2-Dichloroethane-d4 (S)%95 70-132
4-Bromofluorobenzene (S)%93 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92276172015
1608013SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92276172015
1608013SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92276172015
1608013SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%94 1996
4-Bromofluorobenzene (S)%97 1697
Toluene-d8 (S)%88 1788
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/8560
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92276028001
Parameter Units
Dup
Result QualifiersRPDResult
92275957001
1606387SAMPLE DUPLICATE:
Percent Moisture %12.8 711.9
Parameter Units
Dup
Result QualifiersRPDResult
92276069001
1606388SAMPLE DUPLICATE:
Percent Moisture %19.2 1416.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 23
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 23
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92276028
Attando Avenue Brownfields
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92276028002 MSV/34299TRIP BLANK EPA 8260
92276028001 MSV/34305SB-04 (1-2)EPA 8260
92276028001 PMST/8560SB-04 (1-2)ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/19/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 23
Page 22 of 23
Page 23 of 23
12/2/2015
Mr. Carlo Zanon
Terracon Consulting Engineers
2020-E Starita Rd
Charlotte NC 28206
Project Name: ATANDO AVENUE
Project #: 31157718
Dear Mr. Carlo Zanon
The following report includes the data for the above referenced project for sample(s)
received on 11/17/2015 at Air Toxics Ltd.
The data and associated QC analyzed by TO-15 are compliant with the project
requirements or laboratory criteria with the exception of the deviations noted in the
attached case narrative.
Thank you for choosing Eurofins Air Toxics Inc. for your air analysis needs. Eurofins Air
Toxics Inc. is committed to providing accurate data of the highest quality. Please feel free to
contactthe Project Manager: Ausha Scott at 916-985-1000 if you have any questions regarding the
data in this report.
Regards,
Ausha Scott
Project Manager
Workorder #: 1511269A
Page 1 of 12
Mr. Carlo Zanon
Terracon Consulting Engineers
2020-E Starita Rd
Charlotte, NC 28206
WORK ORDER #:1511269A
CLIENT:BILL TO:
PHONE:
Accounts Payable
Terracon Consulting Engineers
51 Lost Mound Dr
Chattanooga, TN 37406
704-509-1777
704-509-1888
11/17/2015
DATE COMPLETED:12/02/2015
P.O. #
PROJECT #31157718 ATANDO AVENUE
Work Order Summary
FAX:
DATE RECEIVED:CONTACT:Ausha Scott
NAMEFRACTION #TEST VAC./PRES.
RECEIPT
PRESSURE
FINAL
01A SV-01 TO-15 6.9 "Hg 14.9 psi
02A SV-02 TO-15 6.7 "Hg 14.9 psi
03A SV-03 TO-15 5.9 "Hg 15 psi
04A SV-04 TO-15 6.7 "Hg 14.8 psi
05A Lab Blank TO-15 NA NA
06A CCV TO-15 NA NA
07A LCS TO-15 NA NA
07AA LCSD TO-15 NA NA
CERTIFIED BY:
Technical Director
DATE:
Name of Accreditation Body: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program)
Accreditation number: CA300005, Effective date: 10/18/2014, Expiration date: 10/17/2015.
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 9563
[phone] . [phone] . FAX [phone]
12/02/15
Page 2 of 12
This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc.
Eurofins Air Toxics Inc.. certifies that the test results contained in this report meet all requirements of the NELAC standards
Certification numbers: AZ Licensure AZ0775, NJ NELAP - CA016, NY NELAP - 11291,
TX NELAP - T104704343-14-7, UT NELAP CA009332014-5, VA NELAP - 460197, WA NELAP - C935
LABORATORY NARRATIVEEPA Method TO-15Terracon Consulting EngineersWorkorder# 1511269A
Four 1 Liter Summa Canister samples were received on November 17, 2015. The laboratory performed analysis
via EPA Method TO-15 using GC/MS in the full scan mode.
This workorder was independently validated prior to submittal using 'USEPA National Functional Guidelines' as
generally applied to the analysis of volatile organic compounds in air. A rules-based, logic driven, independent
validation engine was employed to assess completeness, evaluate pass/fail of relevant project quality control
requirements and verification of all quantified amounts.
There were no receiving discrepancies.
Receiving Notes
Dilution was performed on sample SV-04 due to the presence of high level target species.
All Quality Control Limit exceedances and affected sample results are noted by flags. Each flag is defined at the
bottom of this Case Narrative and on each Sample Result Summary page.
Analytical Notes
Eight qualifiers may have been used on the data analysis sheets and indicates as follows:
B - Compound present in laboratory blank greater than reporting limit (background subtraction not
performed).
J - Estimated value.
E - Exceeds instrument calibration range.
S - Saturated peak.
Q - Exceeds quality control limits.
U - Compound analyzed for but not detected above the reporting limit, LOD, or MDL value. See data
page for project specific U-flag definition.
UJ- Non-detected compound associated with low bias in the CCV
N - The identification is based on presumptive evidence.
File extensions may have been used on the data analysis sheets and indicates
as follows:
a-File was requantified
b-File was quantified by a second column and detector
r1-File was requantified for the purpose of reissue
Definition of Data Qualifying Flags
Page 3 of 12
EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: SV-01
Lab ID#: 1511269A-01A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.3 4.9 5.7 21m,p-Xylene
1.3 4.1 5.7 18o-Xylene
Client Sample ID: SV-02
Lab ID#: 1511269A-02A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.3 7.7 5.6 33Ethyl Benzene
1.3 57 5.6 250m,p-Xylene
1.3 33 5.6 140o-Xylene
2.6 8.2 14 43Naphthalene
Client Sample ID: SV-03
Lab ID#: 1511269A-03A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.3 4.3 8.5 29Tetrachloroethene
Client Sample ID: SV-04
Lab ID#: 1511269A-04A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.8 5.8 9.9 31Trichloroethene
1.8 600 12 4100Tetrachloroethene
1.8 7.5 8.0 33Ethyl Benzene
1.8 32 8.0 140m,p-Xylene
1.8 8.8 8.0 38o-Xylene
Page 4 of 12
Client Sample ID: SV-01
Lab ID#: 1511269A-01A
EPA METHOD TO-15 GC/MS FULL SCAN
j112026File Name:
Dil. Factor:2.62
Date of Collection: 11/12/15 9:47:00 AM
Date of Analysis: 11/21/15 02:02 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.3 Not Detected 3.3 Not DetectedVinyl Chloride
1.3 Not Detected 5.2 Not Detected1,1-Dichloroethene
1.3 Not Detected 5.2 Not Detectedtrans-1,2-Dichloroethene
1.3 Not Detected 5.2 Not Detectedcis-1,2-Dichloroethene
1.3 Not Detected 6.4 Not DetectedChloroform
1.3 Not Detected 4.2 Not DetectedBenzene
1.3 Not Detected 5.3 Not Detected1,2-Dichloroethane
1.3 Not Detected 7.0 Not DetectedTrichloroethene
1.3 Not Detected 8.9 Not DetectedTetrachloroethene
1.3 Not Detected 5.7 Not DetectedEthyl Benzene
1.3 4.9 5.7 21m,p-Xylene
1.3 4.1 5.7 18o-Xylene
2.6 Not Detected 14 Not DetectedNaphthalene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
99 70-130Toluene-d8
104 70-1301,2-Dichloroethane-d4
100 70-1304-Bromofluorobenzene
Page 5 of 12
Client Sample ID: SV-02
Lab ID#: 1511269A-02A
EPA METHOD TO-15 GC/MS FULL SCAN
j112027File Name:
Dil. Factor:2.59
Date of Collection: 11/12/15 12:27:00 PM
Date of Analysis: 11/21/15 02:47 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.3 Not Detected 3.3 Not DetectedVinyl Chloride
1.3 Not Detected 5.1 Not Detected1,1-Dichloroethene
1.3 Not Detected 5.1 Not Detectedtrans-1,2-Dichloroethene
1.3 Not Detected 5.1 Not Detectedcis-1,2-Dichloroethene
1.3 Not Detected 6.3 Not DetectedChloroform
1.3 Not Detected 4.1 Not DetectedBenzene
1.3 Not Detected 5.2 Not Detected1,2-Dichloroethane
1.3 Not Detected 7.0 Not DetectedTrichloroethene
1.3 Not Detected 8.8 Not DetectedTetrachloroethene
1.3 7.7 5.6 33Ethyl Benzene
1.3 57 5.6 250m,p-Xylene
1.3 33 5.6 140o-Xylene
2.6 8.2 14 43Naphthalene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
103 70-130Toluene-d8
100 70-1301,2-Dichloroethane-d4
100 70-1304-Bromofluorobenzene
Page 6 of 12
Client Sample ID: SV-03
Lab ID#: 1511269A-03A
EPA METHOD TO-15 GC/MS FULL SCAN
j112028File Name:
Dil. Factor:2.52
Date of Collection: 11/12/15 11:32:00 AM
Date of Analysis: 11/21/15 03:14 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.3 Not Detected 3.2 Not DetectedVinyl Chloride
1.3 Not Detected 5.0 Not Detected1,1-Dichloroethene
1.3 Not Detected 5.0 Not Detectedtrans-1,2-Dichloroethene
1.3 Not Detected 5.0 Not Detectedcis-1,2-Dichloroethene
1.3 Not Detected 6.2 Not DetectedChloroform
1.3 Not Detected 4.0 Not DetectedBenzene
1.3 Not Detected 5.1 Not Detected1,2-Dichloroethane
1.3 Not Detected 6.8 Not DetectedTrichloroethene
1.3 4.3 8.5 29Tetrachloroethene
1.3 Not Detected 5.5 Not DetectedEthyl Benzene
1.3 Not Detected 5.5 Not Detectedm,p-Xylene
1.3 Not Detected 5.5 Not Detectedo-Xylene
2.5 Not Detected 13 Not DetectedNaphthalene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
101 70-130Toluene-d8
104 70-1301,2-Dichloroethane-d4
100 70-1304-Bromofluorobenzene
Page 7 of 12
Client Sample ID: SV-04
Lab ID#: 1511269A-04A
EPA METHOD TO-15 GC/MS FULL SCAN
j112035File Name:
Dil. Factor:3.69
Date of Collection: 11/12/15 2:25:00 PM
Date of Analysis: 11/21/15 07:59 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.8 Not Detected 4.7 Not DetectedVinyl Chloride
1.8 Not Detected 7.3 Not Detected1,1-Dichloroethene
1.8 Not Detected 7.3 Not Detectedtrans-1,2-Dichloroethene
1.8 Not Detected 7.3 Not Detectedcis-1,2-Dichloroethene
1.8 Not Detected 9.0 Not DetectedChloroform
1.8 Not Detected 5.9 Not DetectedBenzene
1.8 Not Detected 7.5 Not Detected1,2-Dichloroethane
1.8 5.8 9.9 31Trichloroethene
1.8 600 12 4100Tetrachloroethene
1.8 7.5 8.0 33Ethyl Benzene
1.8 32 8.0 140m,p-Xylene
1.8 8.8 8.0 38o-Xylene
3.7 Not Detected 19 Not DetectedNaphthalene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
100 70-130Toluene-d8
99 70-1301,2-Dichloroethane-d4
100 70-1304-Bromofluorobenzene
Page 8 of 12
Client Sample ID: Lab Blank
Lab ID#: 1511269A-05A
EPA METHOD TO-15 GC/MS FULL SCAN
j112011File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 11/20/15 04:13 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.50 Not Detected 1.3 Not DetectedVinyl Chloride
0.50 Not Detected 2.0 Not Detected1,1-Dichloroethene
0.50 Not Detected 2.0 Not Detectedtrans-1,2-Dichloroethene
0.50 Not Detected 2.0 Not Detectedcis-1,2-Dichloroethene
0.50 Not Detected 2.4 Not DetectedChloroform
0.50 Not Detected 1.6 Not DetectedBenzene
0.50 Not Detected 2.0 Not Detected1,2-Dichloroethane
0.50 Not Detected 2.7 Not DetectedTrichloroethene
0.50 Not Detected 3.4 Not DetectedTetrachloroethene
0.50 Not Detected 2.2 Not DetectedEthyl Benzene
0.50 Not Detected 2.2 Not Detectedm,p-Xylene
0.50 Not Detected 2.2 Not Detectedo-Xylene
1.0 Not Detected 5.2 Not DetectedNaphthalene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
103 70-130Toluene-d8
105 70-1301,2-Dichloroethane-d4
98 70-1304-Bromofluorobenzene
Page 9 of 12
Client Sample ID: CCV
Lab ID#: 1511269A-06A
EPA METHOD TO-15 GC/MS FULL SCAN
j112002File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 11/20/15 10:50 AM
%RecoveryCompound
83Vinyl Chloride
831,1-Dichloroethene
83trans-1,2-Dichloroethene
82cis-1,2-Dichloroethene
82Chloroform
82Benzene
801,2-Dichloroethane
78Trichloroethene
83Tetrachloroethene
85Ethyl Benzene
86m,p-Xylene
88o-Xylene
75Naphthalene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
100 70-130Toluene-d8
99 70-1301,2-Dichloroethane-d4
101 70-1304-Bromofluorobenzene
Page 10 of 12
Client Sample ID: LCS
Lab ID#: 1511269A-07A
EPA METHOD TO-15 GC/MS FULL SCAN
j112005File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 11/20/15 12:38 PM
Limits%RecoveryCompound
Method
79 70-130Vinyl Chloride
76 70-1301,1-Dichloroethene
67 Q 70-130trans-1,2-Dichloroethene
86 70-130cis-1,2-Dichloroethene
76 70-130Chloroform
77 70-130Benzene
75 70-1301,2-Dichloroethane
74 70-130Trichloroethene
77 70-130Tetrachloroethene
80 70-130Ethyl Benzene
81 70-130m,p-Xylene
84 70-130o-Xylene
66 60-140Naphthalene
Q = Exceeds Quality Control limits.
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
99 70-130Toluene-d8
99 70-1301,2-Dichloroethane-d4
99 70-1304-Bromofluorobenzene
Page 11 of 12
Client Sample ID: LCSD
Lab ID#: 1511269A-07AA
EPA METHOD TO-15 GC/MS FULL SCAN
j112006File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 11/20/15 01:03 PM
Limits%RecoveryCompound
Method
77 70-130Vinyl Chloride
76 70-1301,1-Dichloroethene
65 Q 70-130trans-1,2-Dichloroethene
84 70-130cis-1,2-Dichloroethene
76 70-130Chloroform
78 70-130Benzene
75 70-1301,2-Dichloroethane
74 70-130Trichloroethene
79 70-130Tetrachloroethene
81 70-130Ethyl Benzene
83 70-130m,p-Xylene
85 70-130o-Xylene
68 60-140Naphthalene
Q = Exceeds Quality Control limits.
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
100 70-130Toluene-d8
97 70-1301,2-Dichloroethane-d4
99 70-1304-Bromofluorobenzene
Page 12 of 12
12/2/2015
Mr. Carlo Zanon
Terracon Consulting Engineers
2020-E Starita Rd
Charlotte NC 28206
Project Name: ATANDO AVENUE
Project #: 31157718
Dear Mr. Carlo Zanon
The following report includes the data for the above referenced project for sample(s)
received on 11/17/2015 at Air Toxics Ltd.
The data and associated QC analyzed by Modified ASTM D-1946 are compliant with
the project requirements or laboratory criteria with the exception of the deviations
noted in the attached case narrative.
Thank you for choosing Eurofins Air Toxics Inc. for your air analysis needs. Eurofins Air
Toxics Inc. is committed to providing accurate data of the highest quality. Please feel free
to contactthe Project Manager: Ausha Scott at 916-985-1000 if you have any questions regarding
the data in this report.
Regards,
Ausha Scott
Project Manager
Workorder #: 1511269C
Page 1 of 9
Mr. Carlo Zanon
Terracon Consulting Engineers
2020-E Starita Rd
Charlotte, NC 28206
WORK ORDER #:1511269C
CLIENT:BILL TO:
PHONE:
Accounts Payable
Terracon Consulting Engineers
51 Lost Mound Dr
Chattanooga, TN 37406
704-509-1777
704-509-1888
11/17/2015
DATE COMPLETED:12/02/2015
P.O. #
PROJECT #31157718 ATANDO AVENUE
Work Order Summary
FAX:
DATE RECEIVED:CONTACT:Ausha Scott
NAMEFRACTION #TEST VAC./PRES.
RECEIPT
PRESSURE
FINAL
03A SV-03 Modified ASTM D-1946 5.9 "Hg 15 psi
04A Lab Blank Modified ASTM D-1946 NA NA
05A LCS Modified ASTM D-1946 NA NA
05AA LCSD Modified ASTM D-1946 NA NA
CERTIFIED BY:
Technical Director
DATE:
Name of Accreditation Body: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program)
Accreditation number: CA300005, Effective date: 10/18/2014, Expiration date: 10/17/2015.
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 9563
[phone] . [phone] . FAX [phone]
12/02/15
Page 2 of 9
This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc.
Eurofins Air Toxics Inc.. certifies that the test results contained in this report meet all requirements of the NELAC standards
Certification numbers: AZ Licensure AZ0775, NJ NELAP - CA016, NY NELAP - 11291,
TX NELAP - T104704343-14-7, UT NELAP CA009332014-5, VA NELAP - 460197, WA NELAP - C935
LABORATORY NARRATIVEModified ASTM D-1946Terracon Consulting EngineersWorkorder# 1511269C
One 1 Liter Summa Canister sample was received on November 17, 2015. The laboratory performed
analysis via Modified ASTM Method D-1946 for Helium in air using GC/TCD. The method involves
direct injection of 1.0 mL of sample.
Method modifications taken to run these samples are summarized in the table below. Specific project
requirements may over-ride the ATL modifications.
Requirement ATL ModificationsASTM D-1946
Calibration A single point
calibration is
performed using a
reference standard
closely matching the
composition of the
unknown.
A minimum of 5-point calibration curve is performed.
Quantitation is based on average Response Factor.
Reference Standard The composition of any
reference standard
must be known to
within 0.01 mol % for
any component.
The standards used by ATL are blended to a >/= 95%
accuracy.
Sample Injection Volume Components whose
concentrations are in
excess of 5 % should
not be analyzed by
using sample volumes
greater than 0.5 mL.
The sample container is connected directly to a fixed
volume sample loop of 1.0 mL on the GC. Linear range
is defined by the calibration curve. Bags are loaded by
vacuum.
Normalization Normalize the mole
percent values by
multiplying each value
by 100 and dividing by
the sum of the original
values. The sum of the
original values should
not differ from 100%
by more than 1.0%.
Results are not normalized. The sum of the reported
values can differ from 100% by as much as 15%, either
due to analytical variability or an unusual sample matrix.
Precision Precision requirements
established at each
concentration level.
Duplicates should agree within 25% RPD for detections
> 5 X's the RL.
Receiving Notes
There were no receiving discrepancies.
There were no analytical discrepancies.
Analytical Notes
Page 3 of 9
Seven qualifiers may have been used on the data analysis sheets and indicate as follows:
B - Compound present in laboratory blank greater than reporting limit.
J - Estimated value.
E - Exceeds instrument calibration range.
S - Saturated peak.
Q - Exceeds quality control limits.
U - Compound analyzed for but not detected above the detection limit.
M - Reported value may be biased due to apparent matrix interferences.
File extensions may have been used on the data analysis sheets and indicates
as follows:
a-File was requantified
b-File was quantified by a second column and detector
r1-File was requantified for the purpose of reissue
Definition of Data Qualifying Flags
Page 4 of 9
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
Summary of Detected Compounds
Client Sample ID: SV-03
Lab ID#: 1511269C-03A
No Detections Were Found.
Page 5 of 9
Client Sample ID: SV-03
Lab ID#: 1511269C-03A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10112316cFile Name:
Dil. Factor:2.52
Date of Collection: 11/12/15 11:32:00 A
Date of Analysis: 11/23/15 03:05 PM
(%)(%)Compound
AmountRpt. Limit
0.13 Not DetectedHelium
Container Type: 1 Liter Summa Canister
Page 6 of 9
Client Sample ID: Lab Blank
Lab ID#: 1511269C-04A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10112303cFile Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 11/23/15 08:04 AM
(%)(%)Compound
AmountRpt. Limit
0.050 Not DetectedHelium
Container Type: NA - Not Applicable
Page 7 of 9
Client Sample ID: LCS
Lab ID#: 1511269C-05A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10112302cFile Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 11/23/15 07:37 AM
Limits%RecoveryCompound
Method
102 85-115Helium
Container Type: NA - Not Applicable
Page 8 of 9
Client Sample ID: LCSD
Lab ID#: 1511269C-05AA
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
10112326cFile Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 11/23/15 10:01 PM
Limits%RecoveryCompound
Method
102 85-115Helium
Container Type: NA - Not Applicable
Page 9 of 9
11/21/2015
Mr. Carlo Zanon
Terracon Consulting Engineers
2020-E Starita Rd
Charlotte NC 28206
Project Name: ATANDO AVENUE
Project #: 31157718
Dear Mr. Carlo Zanon
The following report includes the data for the above referenced project for sample(s)
received on 11/17/2015 at Air Toxics Ltd.
The data and associated QC analyzed by Modified TO-15 SIM are compliant with the
project requirements or laboratory criteria with the exception of the deviations noted in
the attached case narrative.
Thank you for choosing Eurofins Air Toxics Inc. for your air analysis needs. Eurofins Air
Toxics Inc. is committed to providing accurate data of the highest quality. Please feel free
to contactthe Project Manager: Ausha Scott at 916-985-1000 if you have any questions regarding
the data in this report.
Regards,
Ausha Scott
Project Manager
Workorder #: 1511269B
Page 1 of 11
Mr. Carlo Zanon
Terracon Consulting Engineers
2020-E Starita Rd
Charlotte, NC 28206
WORK ORDER #:1511269B
CLIENT:BILL TO:
PHONE:
Accounts Payable
Terracon Consulting Engineers
51 Lost Mound Dr
Chattanooga, TN 37406
704-509-1777
704-509-1888
11/17/2015
DATE COMPLETED:11/21/2015
P.O. #
PROJECT #31157718 ATANDO AVENUE
Work Order Summary
FAX:
DATE RECEIVED:CONTACT:Ausha Scott
NAMEFRACTION #TEST VAC./PRES.
RECEIPT
PRESSURE
FINAL
05A IA-01 Modified TO-15 SIM 8.2 "Hg 4.9 psi
06A OA-01 Modified TO-15 SIM 8 "Hg 5 psi
07A Lab Blank Modified TO-15 SIM NA NA
08A CCV Modified TO-15 SIM NA NA
09A LCS Modified TO-15 SIM NA NA
09AA LCSD Modified TO-15 SIM NA NA
CERTIFIED BY:
Technical Director
DATE:
Name of Accreditation Body: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program)
Accreditation number: CA300005, Effective date: 10/18/2014, Expiration date: 10/17/2015.
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 9563
[phone] . [phone] . FAX [phone]
11/21/15
Page 2 of 11
This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc.
Eurofins Air Toxics Inc.. certifies that the test results contained in this report meet all requirements of the NELAC standards
Certification numbers: AZ Licensure AZ0775, NJ NELAP - CA016, NY NELAP - 11291,
TX NELAP - T104704343-14-7, UT NELAP CA009332014-5, VA NELAP - 460197, WA NELAP - C935
LABORATORY NARRATIVEModified TO-15 SIMTerracon Consulting EngineersWorkorder# 1511269B
Two 6 Liter Summa Canister (SIM Certified) samples were received on November 17, 2015. The
laboratory performed analysis via modified EPA Method TO-15 using GC/MS in the SIM acquisition
mode.
This workorder was independently validated prior to submittal using 'USEPA National Functional
Guidelines' as generally applied to the analysis of volatile organic compounds in air. A rules-based,
logic driven, independent validation engine was employed to assess completeness, evaluate pass/fail of
relevant project quality control requirements and verification of all quantified amounts.
Method modifications taken to run these samples are summarized in the table below. Specific project
requirements may over-ride the ATL modifications.
Requirement ATL ModificationsTO-15
ICAL %RSD acceptance
criteria
</=30% RSD with 2
compounds allowed out
to < 40% RSD
Project specific; default criteria is </=30% RSD with
10% of compounds allowed out to < 40% RSD
Daily Calibration +- 30% Difference Project specific; default criteria is </= 30% Difference
with 10% of compounds allowed out up to </=40%.; flag
and narrate outliers
Blank and standards Zero air Nitrogen
Method Detection Limit Follow 40CFR Pt.136
App. B
The MDL met all relevant requirements in Method
TO-15 (statistical MDL less than the LOQ). The
concentration of the spiked replicate may have exceeded
10X the calculated MDL in some cases
Receiving Notes
There were no receiving discrepancies.
There were no analytical discrepancies.
Analytical Notes
Eight qualifiers may have been used on the data analysis sheets and indicates as follows:
B - Compound present in laboratory blank greater than reporting limit (background subtraction
not performed).
J - Estimated value.
E - Exceeds instrument calibration range.
S - Saturated peak.
Q - Exceeds quality control limits.
U - Compound analyzed for but not detected above the reporting limit, LOD, or MDL value. See
data page for project specific U-flag definition.
UJ- Non-detected compound associated with low bias in the CCV
N - The identification is based on presumptive evidence.
Definition of Data Qualifying Flags
Page 3 of 11
File extensions may have been used on the data analysis sheets and indicates
as follows:
a-File was requantified
b-File was quantified by a second column and detector
r1-File was requantified for the purpose of reissue
Page 4 of 11
MODIFIED EPA METHOD TO-15 GC/MS SIM
Summary of Detected Compounds
Client Sample ID: IA-01
Lab ID#: 1511269B-05A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.037 0.060 0.18 0.29Chloroform
0.092 0.24 0.29 0.75Benzene
0.037 0.16 0.25 1.1Tetrachloroethene
0.037 0.25 0.16 1.1Ethyl Benzene
0.073 0.71 0.32 3.1m,p-Xylene
0.037 0.28 0.16 1.2o-Xylene
0.092 0.12 0.48 0.61Naphthalene
Client Sample ID: OA-01
Lab ID#: 1511269B-06A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.091 0.13 0.29 0.42Benzene
0.073 0.10 0.32 0.45m,p-Xylene
0.036 0.038 0.16 0.16o-Xylene
Page 5 of 11
Client Sample ID: IA-01
Lab ID#: 1511269B-05A
MODIFIED EPA METHOD TO-15 GC/MS SIM
v111807simFile Name:
Dil. Factor:1.83
Date of Collection: 11/12/15 4:00:00 PM
Date of Analysis: 11/18/15 01:07 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.018 Not Detected 0.047 Not DetectedVinyl Chloride
0.018 Not Detected 0.072 Not Detected1,1-Dichloroethene
0.18 Not Detected 0.72 Not Detectedtrans-1,2-Dichloroethene
0.037 Not Detected 0.14 Not Detectedcis-1,2-Dichloroethene
0.037 0.060 0.18 0.29Chloroform
0.092 0.24 0.29 0.75Benzene
0.037 Not Detected 0.15 Not Detected1,2-Dichloroethane
0.037 Not Detected 0.20 Not DetectedTrichloroethene
0.037 0.16 0.25 1.1Tetrachloroethene
0.037 0.25 0.16 1.1Ethyl Benzene
0.073 0.71 0.32 3.1m,p-Xylene
0.037 0.28 0.16 1.2o-Xylene
0.092 0.12 0.48 0.61Naphthalene
Container Type: 6 Liter Summa Canister (SIM Certified)
Limits%RecoverySurrogates
Method
102 70-1301,2-Dichloroethane-d4
100 70-130Toluene-d8
92 70-1304-Bromofluorobenzene
Page 6 of 11
Client Sample ID: OA-01
Lab ID#: 1511269B-06A
MODIFIED EPA METHOD TO-15 GC/MS SIM
v111808simFile Name:
Dil. Factor:1.82
Date of Collection: 11/12/15 3:55:00 PM
Date of Analysis: 11/18/15 01:42 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.018 Not Detected 0.046 Not DetectedVinyl Chloride
0.018 Not Detected 0.072 Not Detected1,1-Dichloroethene
0.18 Not Detected 0.72 Not Detectedtrans-1,2-Dichloroethene
0.036 Not Detected 0.14 Not Detectedcis-1,2-Dichloroethene
0.036 Not Detected 0.18 Not DetectedChloroform
0.091 0.13 0.29 0.42Benzene
0.036 Not Detected 0.15 Not Detected1,2-Dichloroethane
0.036 Not Detected 0.20 Not DetectedTrichloroethene
0.036 Not Detected 0.25 Not DetectedTetrachloroethene
0.036 Not Detected 0.16 Not DetectedEthyl Benzene
0.073 0.10 0.32 0.45m,p-Xylene
0.036 0.038 0.16 0.16o-Xylene
0.091 Not Detected 0.48 Not DetectedNaphthalene
Container Type: 6 Liter Summa Canister (SIM Certified)
Limits%RecoverySurrogates
Method
104 70-1301,2-Dichloroethane-d4
99 70-130Toluene-d8
92 70-1304-Bromofluorobenzene
Page 7 of 11
Client Sample ID: Lab Blank
Lab ID#: 1511269B-07A
MODIFIED EPA METHOD TO-15 GC/MS SIM
v111806simFile Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 11/18/15 11:45 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.010 Not Detected 0.026 Not DetectedVinyl Chloride
0.010 Not Detected 0.040 Not Detected1,1-Dichloroethene
0.10 Not Detected 0.40 Not Detectedtrans-1,2-Dichloroethene
0.020 Not Detected 0.079 Not Detectedcis-1,2-Dichloroethene
0.020 Not Detected 0.098 Not DetectedChloroform
0.050 Not Detected 0.16 Not DetectedBenzene
0.020 Not Detected 0.081 Not Detected1,2-Dichloroethane
0.020 Not Detected 0.11 Not DetectedTrichloroethene
0.020 Not Detected 0.14 Not DetectedTetrachloroethene
0.020 Not Detected 0.087 Not DetectedEthyl Benzene
0.040 Not Detected 0.17 Not Detectedm,p-Xylene
0.020 Not Detected 0.087 Not Detectedo-Xylene
0.050 Not Detected 0.26 Not DetectedNaphthalene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
100 70-1301,2-Dichloroethane-d4
99 70-130Toluene-d8
92 70-1304-Bromofluorobenzene
Page 8 of 11
Client Sample ID: CCV
Lab ID#: 1511269B-08A
MODIFIED EPA METHOD TO-15 GC/MS SIM
v111802simFile Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 11/18/15 08:59 AM
%RecoveryCompound
100Vinyl Chloride
841,1-Dichloroethene
89trans-1,2-Dichloroethene
88cis-1,2-Dichloroethene
93Chloroform
96Benzene
931,2-Dichloroethane
86Trichloroethene
81Tetrachloroethene
89Ethyl Benzene
88m,p-Xylene
87o-Xylene
73Naphthalene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
99 70-1301,2-Dichloroethane-d4
101 70-130Toluene-d8
96 70-1304-Bromofluorobenzene
Page 9 of 11
Client Sample ID: LCS
Lab ID#: 1511269B-09A
MODIFIED EPA METHOD TO-15 GC/MS SIM
v111803simFile Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 11/18/15 09:40 AM
Limits%RecoveryCompound
Method
104 70-130Vinyl Chloride
85 70-1301,1-Dichloroethene
78 70-130trans-1,2-Dichloroethene
99 70-130cis-1,2-Dichloroethene
94 70-130Chloroform
98 70-130Benzene
95 70-1301,2-Dichloroethane
87 70-130Trichloroethene
83 70-130Tetrachloroethene
89 70-130Ethyl Benzene
88 70-130m,p-Xylene
88 70-130o-Xylene
64 60-140Naphthalene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
99 70-1301,2-Dichloroethane-d4
101 70-130Toluene-d8
95 70-1304-Bromofluorobenzene
Page 10 of 11
Client Sample ID: LCSD
Lab ID#: 1511269B-09AA
MODIFIED EPA METHOD TO-15 GC/MS SIM
v111804simFile Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 11/18/15 10:20 AM
Limits%RecoveryCompound
Method
105 70-130Vinyl Chloride
86 70-1301,1-Dichloroethene
80 70-130trans-1,2-Dichloroethene
100 70-130cis-1,2-Dichloroethene
94 70-130Chloroform
100 70-130Benzene
97 70-1301,2-Dichloroethane
88 70-130Trichloroethene
84 70-130Tetrachloroethene
91 70-130Ethyl Benzene
90 70-130m,p-Xylene
90 70-130o-Xylene
71 60-140Naphthalene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
99 70-1301,2-Dichloroethane-d4
101 70-130Toluene-d8
95 70-1304-Bromofluorobenzene
Page 11 of 11