GWMR-09-17-15 65p

09/09/15
Technical Report for
GRI (Geological Resources Inc.)
Anson Mart; 1250 E Caswell, Wadesboro, NC
29457
Accutest Job Number: FA27274
Sampling Date: 09/01/15
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]
ATTN: Nicole Long
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast
09/09/15
e-Hardcopy 2.0
Automated Report
40
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
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FA27274
Table of Contents
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Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................7
3.1: FA27274-1: MW-1 ........................................................................................................8
3.2: FA27274-2: MW-3 ........................................................................................................10
3.3: FA27274-3: MW-4 ........................................................................................................12
3.4: FA27274-4: MW-5 ........................................................................................................14
3.5: FA27274-5: MW-6 ........................................................................................................16
3.6: FA27274-6: TW-1 .........................................................................................................18
3.7: FA27274-7: STREAM-1 ...............................................................................................20
3.8: FA27274-8: TRIP BLANK ...........................................................................................22
Section 4: Misc. Forms ............................................................................................................24
4.1: Chain of Custody ...........................................................................................................25
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................28
5.1: Method Blank Summary ................................................................................................29
5.2: Blank Spike Summary ...................................................................................................33
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................37
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Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA27274
Anson Mart; 1250 E Caswell, Wadesboro, NC
Project No: 29457
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA27274-1 09/01/15 15:16 CB 09/02/15 AQ Ground Water MW-1
FA27274-2 09/01/15 14:18 CB 09/02/15 AQ Ground Water MW-3
FA27274-3 09/01/15 14:01 CB 09/02/15 AQ Ground Water MW-4
FA27274-4 09/01/15 14:09 CB 09/02/15 AQ Ground Water MW-5
FA27274-5 09/01/15 14:54 CB 09/02/15 AQ Ground Water MW-6
FA27274-6 09/01/15 13:16 CB 09/02/15 AQ Ground Water TW-1
FA27274-7 09/01/15 13:48 CB 09/02/15 AQ Ground Water STREAM-1
FA27274-8 09/01/15 00:00 CB 09/02/15 AQ Trip Blank Water TRIP BLANK
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Summary of Hits Page 1 of 3
Job Number:FA27274
Account:GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Collected:09/01/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA27274-1 MW-1
Benzene 537 13 4.3 ug/l SM 6200B
n-Butylbenzene 57.0 13 3.6 ug/l SM 6200B
sec-Butylbenzene 27.7 13 3.5 ug/l SM 6200B
Di-Isopropyl Ether 4.3 J 13 4.0 ug/l SM 6200B
Ethylbenzene 1040 13 3.8 ug/l SM 6200B
Isopropylbenzene 159 13 3.0 ug/l SM 6200B
p-Isopropyltoluene 9.6 J 13 3.1 ug/l SM 6200B
Naphthalene 784 13 3.1 ug/l SM 6200B
n-Propylbenzene 529 13 3.9 ug/l SM 6200B
Toluene 591 13 4.2 ug/l SM 6200B
1,2,4-Trimethylbenzene 1570 50 14 ug/l SM 6200B
1,3,5-Trimethylbenzene 464 13 3.4 ug/l SM 6200B
m,p-Xylene 2290 25 7.4 ug/l SM 6200B
o-Xylene 681 13 3.3 ug/l SM 6200B
Xylene (total)2970 38 11 ug/l SM 6200B
FA27274-2 MW-3
Benzene 122 2.5 0.86 ug/l SM 6200B
n-Butylbenzene 0.65 0.50 0.14 ug/l SM 6200B
sec-Butylbenzene 0.49 J 0.50 0.14 ug/l SM 6200B
Di-Isopropyl Ether 23.9 0.50 0.16 ug/l SM 6200B
Ethylbenzene 12.7 0.50 0.15 ug/l SM 6200B
Isopropylbenzene 3.3 0.50 0.12 ug/l SM 6200B
p-Isopropyltoluene 0.55 0.50 0.12 ug/l SM 6200B
Methyl Tert Butyl Ether 19.3 0.50 0.16 ug/l SM 6200B
Naphthalene 4.3 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 7.4 0.50 0.16 ug/l SM 6200B
Toluene 8.6 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 16.3 0.50 0.14 ug/l SM 6200B
1,3,5-Trimethylbenzene 2.9 0.50 0.14 ug/l SM 6200B
m,p-Xylene 18.8 1.0 0.30 ug/l SM 6200B
o-Xylene 4.0 0.50 0.13 ug/l SM 6200B
Xylene (total)22.7 1.5 0.43 ug/l SM 6200B
FA27274-3 MW-4
Di-Isopropyl Ether 51.7 1.0 0.32 ug/l SM 6200B
Methyl Tert Butyl Ether 88.0 1.0 0.33 ug/l SM 6200B
FA27274-4 MW-5
Benzene 40.6 0.50 0.17 ug/l SM 6200B
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Summary of Hits Page 2 of 3
Job Number:FA27274
Account:GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Collected:09/01/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
n-Butylbenzene 2.2 0.50 0.14 ug/l SM 6200B
sec-Butylbenzene 1.6 0.50 0.14 ug/l SM 6200B
Di-Isopropyl Ether 1.6 0.50 0.16 ug/l SM 6200B
Ethylbenzene 111 5.0 1.5 ug/l SM 6200B
Isopropylbenzene 16.6 0.50 0.12 ug/l SM 6200B
p-Isopropyltoluene 1.0 0.50 0.12 ug/l SM 6200B
Naphthalene 49.2 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 48.4 0.50 0.16 ug/l SM 6200B
Toluene 17.4 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 305 5.0 1.4 ug/l SM 6200B
1,3,5-Trimethylbenzene 70.9 5.0 1.4 ug/l SM 6200B
m,p-Xylene 399 10 3.0 ug/l SM 6200B
o-Xylene 33.9 5.0 1.3 ug/l SM 6200B
Xylene (total)432 15 4.3 ug/l SM 6200B
FA27274-5 MW-6
Benzene 9.6 0.50 0.17 ug/l SM 6200B
Di-Isopropyl Ether 4.3 0.50 0.16 ug/l SM 6200B
Ethylbenzene 0.55 0.50 0.15 ug/l SM 6200B
Isopropylbenzene 0.31 J 0.50 0.12 ug/l SM 6200B
Methyl Tert Butyl Ether 26.5 0.50 0.16 ug/l SM 6200B
n-Propylbenzene 0.49 J 0.50 0.16 ug/l SM 6200B
Toluene 0.92 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.26 J 0.50 0.14 ug/l SM 6200B
m,p-Xylene 1.4 1.0 0.30 ug/l SM 6200B
o-Xylene 0.76 0.50 0.13 ug/l SM 6200B
Xylene (total)2.2 1.5 0.43 ug/l SM 6200B
FA27274-6 TW-1
Benzene 1.5 0.50 0.17 ug/l SM 6200B
Di-Isopropyl Ether 0.71 0.50 0.16 ug/l SM 6200B
Ethylbenzene 0.39 J 0.50 0.15 ug/l SM 6200B
Isopropylbenzene 0.61 0.50 0.12 ug/l SM 6200B
Methyl Tert Butyl Ether 1.5 0.50 0.16 ug/l SM 6200B
n-Propylbenzene 0.65 0.50 0.16 ug/l SM 6200B
Toluene 0.82 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.67 0.50 0.14 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.24 J 0.50 0.14 ug/l SM 6200B
m,p-Xylene 2.1 1.0 0.30 ug/l SM 6200B
o-Xylene 0.15 J 0.50 0.13 ug/l SM 6200B
Xylene (total)2.3 1.5 0.43 ug/l SM 6200B
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Summary of Hits Page 3 of 3
Job Number:FA27274
Account:GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Collected:09/01/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA27274-7 STREAM-1
No hits reported in this sample.
FA27274-8 TRIP BLANK
No hits reported in this sample.
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Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
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Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-1
Lab Sample ID:FA27274-1 Date Sampled:09/01/15
Matrix:AQ - Ground Water Date Received:09/02/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0196387.D 25 09/08/15 TD n/a n/a VA1776
Run #2 A0196327.D 100 09/04/15 TD n/a n/a VA1774
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 537 13 4.3 ug/l
108-86-1 Bromobenzene ND 13 4.0 ug/l
74-97-5 Bromochloromethane ND 13 4.0 ug/l
75-27-4 Bromodichloromethane ND 13 3.7 ug/l
75-25-2 Bromoform ND 13 2.7 ug/l
104-51-8 n-Butylbenzene 57.0 13 3.6 ug/l
135-98-8 sec-Butylbenzene 27.7 13 3.5 ug/l
98-06-6 tert-Butylbenzene ND 13 3.6 ug/l
56-23-5 Carbon Tetrachloride ND 13 3.8 ug/l
108-90-7 Chlorobenzene ND 13 4.0 ug/l
75-00-3 Chloroethane ND 13 5.2 ug/l
67-66-3 Chloroform ND 13 4.3 ug/l
95-49-8 o-Chlorotoluene ND 13 3.8 ug/l
106-43-4 p-Chlorotoluene ND 13 3.4 ug/l
124-48-1 Dibromochloromethane ND 13 3.1 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 13 4.9 ug/l
106-93-4 1,2-Dibromoethane ND 13 3.5 ug/l
75-71-8 Dichlorodifluoromethane ND 13 3.2 ug/l
95-50-1 1,2-Dichlorobenzene ND 13 3.2 ug/l
541-73-1 1,3-Dichlorobenzene ND 13 3.5 ug/l
106-46-7 1,4-Dichlorobenzene ND 13 3.8 ug/l
75-34-3 1,1-Dichloroethane ND 13 4.5 ug/l
107-06-2 1,2-Dichloroethane ND 13 4.1 ug/l
75-35-4 1,1-Dichloroethylene ND 13 4.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 13 4.5 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 13 4.2 ug/l
78-87-5 1,2-Dichloropropane ND 13 4.3 ug/l
142-28-9 1,3-Dichloropropane ND 13 3.7 ug/l
594-20-7 2,2-Dichloropropane ND 13 3.0 ug/l
563-58-6 1,1-Dichloropropene ND 13 4.0 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 13 3.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 13 3.2 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-1
Lab Sample ID:FA27274-1 Date Sampled:09/01/15
Matrix:AQ - Ground Water Date Received:09/02/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 4.3 13 4.0 ug/l J
100-41-4 Ethylbenzene 1040 13 3.8 ug/l
87-68-3 Hexachlorobutadiene ND 13 3.1 ug/l
98-82-8 Isopropylbenzene 159 13 3.0 ug/l
99-87-6 p-Isopropyltoluene 9.6 13 3.1 ug/l J
74-83-9 Methyl Bromide ND 13 4.6 ug/l
74-87-3 Methyl Chloride ND 13 4.0 ug/l
74-95-3 Methylene Bromide ND 13 4.3 ug/l
75-09-2 Methylene Chloride ND 50 25 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 13 4.1 ug/l
91-20-3 Naphthalene 784 13 3.1 ug/l
103-65-1 n-Propylbenzene 529 13 3.9 ug/l
100-42-5 Styrene ND 13 3.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 13 3.1 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 13 3.6 ug/l
127-18-4 Tetrachloroethylene ND 13 3.7 ug/l
108-88-3 Toluene 591 13 4.2 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 13 3.4 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 13 3.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 13 4.0 ug/l
79-00-5 1,1,2-Trichloroethane ND 13 3.5 ug/l
79-01-6 Trichloroethylene ND 13 3.7 ug/l
75-69-4 Trichlorofluoromethane ND 13 4.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 13 3.2 ug/l
95-63-6 1,2,4-Trimethylbenzene 1570 a 50 14 ug/l
108-67-8 1,3,5-Trimethylbenzene 464 13 3.4 ug/l
75-01-4 Vinyl Chloride ND 13 3.3 ug/l
m,p-Xylene 2290 25 7.4 ug/l
95-47-6 o-Xylene 681 13 3.3 ug/l
1330-20-7 Xylene (total)2970 38 11 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%103%70-130%
2037-26-5 Toluene-D8 100%99%70-130%
460-00-4 4-Bromofluorobenzene 103%102%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-3
Lab Sample ID:FA27274-2 Date Sampled:09/01/15
Matrix:AQ - Ground Water Date Received:09/02/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0196395.D 1 09/08/15 TD n/a n/a VA1776
Run #2 A0196331.D 5 09/04/15 TD n/a n/a VA1774
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 122 a 2.5 0.86 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene 0.65 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene 0.49 0.50 0.14 ug/l J
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-3
Lab Sample ID:FA27274-2 Date Sampled:09/01/15
Matrix:AQ - Ground Water Date Received:09/02/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 23.9 0.50 0.16 ug/l
100-41-4 Ethylbenzene 12.7 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 3.3 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene 0.55 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 19.3 0.50 0.16 ug/l
91-20-3 Naphthalene 4.3 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 7.4 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 8.6 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 16.3 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene 2.9 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 18.8 1.0 0.30 ug/l
95-47-6 o-Xylene 4.0 0.50 0.13 ug/l
1330-20-7 Xylene (total)22.7 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%105%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%108%70-130%
2037-26-5 Toluene-D8 100%97%70-130%
460-00-4 4-Bromofluorobenzene 101%100%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-4
Lab Sample ID:FA27274-3 Date Sampled:09/01/15
Matrix:AQ - Ground Water Date Received:09/02/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0196396.D 2 09/08/15 TD n/a n/a VA1776
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 0.34 ug/l
108-86-1 Bromobenzene ND 1.0 0.32 ug/l
74-97-5 Bromochloromethane ND 1.0 0.32 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.29 ug/l
75-25-2 Bromoform ND 1.0 0.22 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.29 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.28 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.29 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.31 ug/l
108-90-7 Chlorobenzene ND 1.0 0.32 ug/l
75-00-3 Chloroethane ND 1.0 0.41 ug/l
67-66-3 Chloroform ND 1.0 0.34 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.30 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.27 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.25 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.0 0.39 ug/l
106-93-4 1,2-Dibromoethane ND 1.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane ND 1.0 0.26 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.26 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.28 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.30 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.36 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.33 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.34 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.36 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.34 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.35 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.29 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.32 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.26 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.25 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-4
Lab Sample ID:FA27274-3 Date Sampled:09/01/15
Matrix:AQ - Ground Water Date Received:09/02/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 51.7 1.0 0.32 ug/l
100-41-4 Ethylbenzene ND 1.0 0.30 ug/l
87-68-3 Hexachlorobutadiene ND 1.0 0.24 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.24 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.24 ug/l
74-83-9 Methyl Bromide ND 1.0 0.36 ug/l
74-87-3 Methyl Chloride ND 1.0 0.32 ug/l
74-95-3 Methylene Bromide ND 1.0 0.34 ug/l
75-09-2 Methylene Chloride ND 4.0 2.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 88.0 1.0 0.33 ug/l
91-20-3 Naphthalene ND 1.0 0.24 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.31 ug/l
100-42-5 Styrene ND 1.0 0.24 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.25 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.28 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.30 ug/l
108-88-3 Toluene ND 1.0 0.33 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 1.0 0.27 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 1.0 0.26 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.32 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.28 ug/l
79-01-6 Trichloroethylene ND 1.0 0.29 ug/l
75-69-4 Trichlorofluoromethane ND 1.0 0.32 ug/l
96-18-4 1,2,3-Trichloropropane ND 1.0 0.25 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.27 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.27 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.26 ug/l
m,p-Xylene ND 2.0 0.59 ug/l
95-47-6 o-Xylene ND 1.0 0.27 ug/l
1330-20-7 Xylene (total)ND 3.0 0.86 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-5
Lab Sample ID:FA27274-4 Date Sampled:09/01/15
Matrix:AQ - Ground Water Date Received:09/02/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0196333.D 1 09/04/15 TD n/a n/a VA1774
Run #2 A0196388.D 10 09/08/15 TD n/a n/a VA1776
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 40.6 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene 2.2 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene 1.6 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-5
Lab Sample ID:FA27274-4 Date Sampled:09/01/15
Matrix:AQ - Ground Water Date Received:09/02/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 1.6 0.50 0.16 ug/l
100-41-4 Ethylbenzene 111 a 5.0 1.5 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 16.6 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene 1.0 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene 49.2 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 48.4 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 17.4 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 305 a 5.0 1.4 ug/l
108-67-8 1,3,5-Trimethylbenzene 70.9 a 5.0 1.4 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 399 a 10 3.0 ug/l
95-47-6 o-Xylene 33.9 a 5.0 1.3 ug/l
1330-20-7 Xylene (total)432 a 15 4.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 93%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%103%70-130%
2037-26-5 Toluene-D8 101%99%70-130%
460-00-4 4-Bromofluorobenzene 100%100%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-6
Lab Sample ID:FA27274-5 Date Sampled:09/01/15
Matrix:AQ - Ground Water Date Received:09/02/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0196381.D 1 09/08/15 TD n/a n/a VA1776
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 9.6 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-6
Lab Sample ID:FA27274-5 Date Sampled:09/01/15
Matrix:AQ - Ground Water Date Received:09/02/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 4.3 0.50 0.16 ug/l
100-41-4 Ethylbenzene 0.55 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 0.31 0.50 0.12 ug/l J
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 26.5 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 0.49 0.50 0.16 ug/l J
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 0.92 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.26 0.50 0.14 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 1.4 1.0 0.30 ug/l
95-47-6 o-Xylene 0.76 0.50 0.13 ug/l
1330-20-7 Xylene (total)2.2 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:TW-1
Lab Sample ID:FA27274-6 Date Sampled:09/01/15
Matrix:AQ - Ground Water Date Received:09/02/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0196382.D 1 09/08/15 TD n/a n/a VA1776
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1.5 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:TW-1
Lab Sample ID:FA27274-6 Date Sampled:09/01/15
Matrix:AQ - Ground Water Date Received:09/02/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.71 0.50 0.16 ug/l
100-41-4 Ethylbenzene 0.39 0.50 0.15 ug/l J
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 0.61 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 1.5 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 0.65 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 0.82 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.67 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.24 0.50 0.14 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 2.1 1.0 0.30 ug/l
95-47-6 o-Xylene 0.15 0.50 0.13 ug/l J
1330-20-7 Xylene (total)2.3 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:STREAM-1
Lab Sample ID:FA27274-7 Date Sampled:09/01/15
Matrix:AQ - Ground Water Date Received:09/02/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0196336.D 1 09/04/15 TD n/a n/a VA1774
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:STREAM-1
Lab Sample ID:FA27274-7 Date Sampled:09/01/15
Matrix:AQ - Ground Water Date Received:09/02/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FA27274-8 Date Sampled:09/01/15
Matrix:AQ - Trip Blank Water Date Received:09/02/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0196337.D 1 09/04/15 TD n/a n/a VA1774
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FA27274-8 Date Sampled:09/01/15
Matrix:AQ - Trip Blank Water Date Received:09/02/15
Method:SM 6200B Percent Solids:n/a
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
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GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
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Method Blank Summary Page 1 of 2
Job Number:FA27274
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1774-MB A0196317.D 1 09/04/15 TD n/a n/a VA1774
The QC reported here applies to the following samples:Method: SM 6200B
FA27274-1, FA27274-2, FA27274-4, FA27274-7, FA27274-8
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
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Method Blank Summary Page 2 of 2
Job Number:FA27274
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1774-MB A0196317.D 1 09/04/15 TD n/a n/a VA1774
The QC reported here applies to the following samples:Method: SM 6200B
FA27274-1, FA27274-2, FA27274-4, FA27274-7, FA27274-8
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
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Method Blank Summary Page 1 of 2
Job Number:FA27274
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1776-MB A0196380.D 1 09/08/15 TD n/a n/a VA1776
The QC reported here applies to the following samples:Method: SM 6200B
FA27274-1, FA27274-2, FA27274-3, FA27274-4, FA27274-5, FA27274-6
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
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Method Blank Summary Page 2 of 2
Job Number:FA27274
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1776-MB A0196380.D 1 09/08/15 TD n/a n/a VA1776
The QC reported here applies to the following samples:Method: SM 6200B
FA27274-1, FA27274-2, FA27274-3, FA27274-4, FA27274-5, FA27274-6
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
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Blank Spike Summary Page 1 of 2
Job Number:FA27274
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1774-BS A0196315.D 1 09/04/15 TD n/a n/a VA1774
The QC reported here applies to the following samples:Method: SM 6200B
FA27274-1, FA27274-2, FA27274-4, FA27274-7, FA27274-8
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.4 94 70-130
108-86-1 Bromobenzene 10 9.8 98 70-130
74-97-5 Bromochloromethane 10 9.5 95 70-130
75-27-4 Bromodichloromethane 10 9.6 96 70-130
75-25-2 Bromoform 10 9.0 90 70-130
104-51-8 n-Butylbenzene 10 10.2 102 70-130
135-98-8 sec-Butylbenzene 10 10.5 105 70-130
98-06-6 tert-Butylbenzene 10 10.1 101 70-130
56-23-5 Carbon Tetrachloride 10 10 100 70-130
108-90-7 Chlorobenzene 10 9.3 93 70-130
75-00-3 Chloroethane 10 11.3 113 60-140
67-66-3 Chloroform 10 9.6 96 70-130
95-49-8 o-Chlorotoluene 10 10.3 103 70-130
106-43-4 p-Chlorotoluene 10 10.1 101 70-130
124-48-1 Dibromochloromethane 10 9.2 92 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.0 90 70-130
106-93-4 1,2-Dibromoethane 10 9.5 95 70-130
75-71-8 Dichlorodifluoromethane 10 9.6 96 60-140
95-50-1 1,2-Dichlorobenzene 10 10.1 101 70-130
541-73-1 1,3-Dichlorobenzene 10 10.3 103 70-130
106-46-7 1,4-Dichlorobenzene 10 10.0 100 70-130
75-34-3 1,1-Dichloroethane 10 9.6 96 70-130
107-06-2 1,2-Dichloroethane 10 9.3 93 70-130
75-35-4 1,1-Dichloroethylene 10 9.5 95 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.0 90 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.0 100 70-130
78-87-5 1,2-Dichloropropane 10 9.3 93 70-130
142-28-9 1,3-Dichloropropane 10 9.3 93 70-130
594-20-7 2,2-Dichloropropane 10 9.5 95 70-130
563-58-6 1,1-Dichloropropene 10 9.7 97 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.5 95 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.6 106 70-130
108-20-3 Di-Isopropyl Ether 10 9.4 94 70-130
100-41-4 Ethylbenzene 10 9.7 97 70-130
87-68-3 Hexachlorobutadiene 10 10.0 100 70-130
98-82-8 Isopropylbenzene 10 9.9 99 70-130
* = Outside of Control Limits.
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Job Number:FA27274
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1774-BS A0196315.D 1 09/04/15 TD n/a n/a VA1774
The QC reported here applies to the following samples:Method: SM 6200B
FA27274-1, FA27274-2, FA27274-4, FA27274-7, FA27274-8
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.1 101 70-130
74-83-9 Methyl Bromide 10 12.0 120 60-140
74-87-3 Methyl Chloride 10 11.2 112 60-140
74-95-3 Methylene Bromide 10 9.6 96 70-130
75-09-2 Methylene Chloride 10 9.0 90 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.5 95 70-130
91-20-3 Naphthalene 10 10.4 104 70-130
103-65-1 n-Propylbenzene 10 10.6 106 70-130
100-42-5 Styrene 10 9.8 98 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.7 97 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.7 97 70-130
127-18-4 Tetrachloroethylene 10 9.7 97 70-130
108-88-3 Toluene 10 9.2 92 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.2 102 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10 100 70-130
71-55-6 1,1,1-Trichloroethane 10 9.8 98 70-130
79-00-5 1,1,2-Trichloroethane 10 9.4 94 70-130
79-01-6 Trichloroethylene 10 9.4 94 70-130
75-69-4 Trichlorofluoromethane 10 12.7 127 60-140
96-18-4 1,2,3-Trichloropropane 10 9.9 99 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10 100 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.9 99 70-130
75-01-4 Vinyl Chloride 10 11.8 118 60-140
m,p-Xylene 20 19.7 99 70-130
95-47-6 o-Xylene 10 9.6 96 70-130
1330-20-7 Xylene (total)30 29.3 98 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
* = Outside of Control Limits.
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Blank Spike Summary Page 1 of 2
Job Number:FA27274
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1776-BS A0196378.D 1 09/08/15 TD n/a n/a VA1776
The QC reported here applies to the following samples:Method: SM 6200B
FA27274-1, FA27274-2, FA27274-3, FA27274-4, FA27274-5, FA27274-6
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.0 90 70-130
108-86-1 Bromobenzene 10 9.3 93 70-130
74-97-5 Bromochloromethane 10 9.0 90 70-130
75-27-4 Bromodichloromethane 10 9.4 94 70-130
75-25-2 Bromoform 10 8.9 89 70-130
104-51-8 n-Butylbenzene 10 9.7 97 70-130
135-98-8 sec-Butylbenzene 10 9.9 99 70-130
98-06-6 tert-Butylbenzene 10 9.7 97 70-130
56-23-5 Carbon Tetrachloride 10 9.6 96 70-130
108-90-7 Chlorobenzene 10 9.0 90 70-130
75-00-3 Chloroethane 10 11.7 117 60-140
67-66-3 Chloroform 10 9.3 93 70-130
95-49-8 o-Chlorotoluene 10 9.9 99 70-130
106-43-4 p-Chlorotoluene 10 9.7 97 70-130
124-48-1 Dibromochloromethane 10 8.9 89 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.9 89 70-130
106-93-4 1,2-Dibromoethane 10 9.1 91 70-130
75-71-8 Dichlorodifluoromethane 10 9.5 95 60-140
95-50-1 1,2-Dichlorobenzene 10 9.6 96 70-130
541-73-1 1,3-Dichlorobenzene 10 9.7 97 70-130
106-46-7 1,4-Dichlorobenzene 10 9.6 96 70-130
75-34-3 1,1-Dichloroethane 10 9.3 93 70-130
107-06-2 1,2-Dichloroethane 10 9.2 92 70-130
75-35-4 1,1-Dichloroethylene 10 9.3 93 70-130
156-59-2 cis-1,2-Dichloroethylene 10 8.6 86 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.8 98 70-130
78-87-5 1,2-Dichloropropane 10 9.1 91 70-130
142-28-9 1,3-Dichloropropane 10 9.0 90 70-130
594-20-7 2,2-Dichloropropane 10 9.4 94 70-130
563-58-6 1,1-Dichloropropene 10 9.4 94 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.1 91 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.4 104 70-130
108-20-3 Di-Isopropyl Ether 10 9.2 92 70-130
100-41-4 Ethylbenzene 10 9.5 95 70-130
87-68-3 Hexachlorobutadiene 10 9.3 93 70-130
98-82-8 Isopropylbenzene 10 9.6 96 70-130
* = Outside of Control Limits.
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Blank Spike Summary Page 2 of 2
Job Number:FA27274
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1776-BS A0196378.D 1 09/08/15 TD n/a n/a VA1776
The QC reported here applies to the following samples:Method: SM 6200B
FA27274-1, FA27274-2, FA27274-3, FA27274-4, FA27274-5, FA27274-6
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.6 96 70-130
74-83-9 Methyl Bromide 10 12.6 126 60-140
74-87-3 Methyl Chloride 10 11.9 119 60-140
74-95-3 Methylene Bromide 10 9.3 93 70-130
75-09-2 Methylene Chloride 10 9.2 92 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.5 95 70-130
91-20-3 Naphthalene 10 10.1 101 70-130
103-65-1 n-Propylbenzene 10 10 100 70-130
100-42-5 Styrene 10 9.2 92 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.6 96 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.5 95 70-130
127-18-4 Tetrachloroethylene 10 9.3 93 70-130
108-88-3 Toluene 10 8.9 89 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.8 98 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.4 94 70-130
71-55-6 1,1,1-Trichloroethane 10 9.5 95 70-130
79-00-5 1,1,2-Trichloroethane 10 9.2 92 70-130
79-01-6 Trichloroethylene 10 9.3 93 70-130
75-69-4 Trichlorofluoromethane 10 12.9 129 60-140
96-18-4 1,2,3-Trichloropropane 10 9.6 96 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.6 96 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.5 95 70-130
75-01-4 Vinyl Chloride 10 12.0 120 60-140
m,p-Xylene 20 19.1 96 70-130
95-47-6 o-Xylene 10 9.4 94 70-130
1330-20-7 Xylene (total)30 28.5 95 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA27274
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA27298-2MS A0196338.D 200 09/04/15 TD n/a n/a VA1774
FA27298-2MSD A0196339.D 200 09/04/15 TD n/a n/a VA1774
FA27298-2 A0196340.D 200 09/04/15 TD n/a n/a VA1774
The QC reported here applies to the following samples:Method: SM 6200B
FA27274-1, FA27274-2, FA27274-4, FA27274-7, FA27274-8
FA27298-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 6200 2000 7980 89 2000 8130 97 2 70-130/20
108-86-1 Bromobenzene ND 2000 1860 93 2000 1870 94 1 70-130/20
74-97-5 Bromochloromethane ND 2000 1780 89 2000 1850 93 4 70-130/20
75-27-4 Bromodichloromethane ND 2000 1780 89 2000 1820 91 2 70-130/20
75-25-2 Bromoform ND 2000 1500 75 2000 1590 80 6 70-130/20
104-51-8 n-Butylbenzene 47.3 J 2000 1930 94 2000 1990 97 3 70-130/20
135-98-8 sec-Butylbenzene ND 2000 1980 99 2000 2010 101 2 70-130/20
98-06-6 tert-Butylbenzene ND 2000 1910 96 2000 1960 98 3 70-130/20
56-23-5 Carbon Tetrachloride ND 2000 1780 89 2000 1830 92 3 70-130/20
108-90-7 Chlorobenzene ND 2000 1770 89 2000 1810 91 2 70-130/20
75-00-3 Chloroethane ND 2000 1960 98 2000 1890 95 4 60-140/20
67-66-3 Chloroform ND 2000 1840 92 2000 1880 94 2 70-130/20
95-49-8 o-Chlorotoluene ND 2000 1970 99 2000 1990 100 1 70-130/20
106-43-4 p-Chlorotoluene ND 2000 1900 95 2000 1930 97 2 70-130/20
124-48-1 Dibromochloromethane ND 2000 1630 82 2000 1700 85 4 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 2000 1650 83 2000 1780 89 8 70-130/20
106-93-4 1,2-Dibromoethane ND 2000 1780 89 2000 1860 93 4 70-130/20
75-71-8 Dichlorodifluoromethane ND 2000 1490 75 2000 1460 73 2 60-140/20
95-50-1 1,2-Dichlorobenzene ND 2000 1900 95 2000 1950 98 3 70-130/20
541-73-1 1,3-Dichlorobenzene ND 2000 1920 96 2000 1960 98 2 70-130/20
106-46-7 1,4-Dichlorobenzene ND 2000 1910 96 2000 1940 97 2 70-130/20
75-34-3 1,1-Dichloroethane ND 2000 1840 92 2000 1850 93 1 70-130/20
107-06-2 1,2-Dichloroethane ND 2000 1780 89 2000 1860 93 4 70-130/20
75-35-4 1,1-Dichloroethylene ND 2000 1800 90 2000 1800 90 0 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 2000 1680 84 2000 1710 86 2 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 2000 1900 95 2000 1910 96 1 70-130/20
78-87-5 1,2-Dichloropropane ND 2000 1790 90 2000 1820 91 2 70-130/20
142-28-9 1,3-Dichloropropane ND 2000 1760 88 2000 1830 92 4 70-130/20
594-20-7 2,2-Dichloropropane ND 2000 1650 83 2000 1670 84 1 70-130/20
563-58-6 1,1-Dichloropropene ND 2000 1830 92 2000 1870 94 2 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 2000 1720 86 2000 1730 87 1 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 2000 1930 97 2000 1990 100 3 70-130/20
108-20-3 Di-Isopropyl Ether ND 2000 1820 91 2000 1870 94 3 70-130/20
100-41-4 Ethylbenzene 2370 2000 4230 93 2000 4320 98 2 70-130/20
87-68-3 Hexachlorobutadiene ND 2000 1780 89 2000 1830 92 3 70-130/20
98-82-8 Isopropylbenzene 111 2000 1980 93 2000 2050 97 3 70-130/20
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA27274
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA27298-2MS A0196338.D 200 09/04/15 TD n/a n/a VA1774
FA27298-2MSD A0196339.D 200 09/04/15 TD n/a n/a VA1774
FA27298-2 A0196340.D 200 09/04/15 TD n/a n/a VA1774
The QC reported here applies to the following samples:Method: SM 6200B
FA27274-1, FA27274-2, FA27274-4, FA27274-7, FA27274-8
FA27298-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 2000 1880 94 2000 1910 96 2 70-130/20
74-83-9 Methyl Bromide ND 2000 2090 105 2000 2080 104 0 60-140/20
74-87-3 Methyl Chloride ND 2000 1840 92 2000 1900 95 3 60-140/20
74-95-3 Methylene Bromide ND 2000 1830 92 2000 1890 95 3 70-130/20
75-09-2 Methylene Chloride ND 2000 1780 89 2000 1800 90 1 70-130/20
1634-04-4 Methyl Tert Butyl Ether 7600 2000 9430 92 2000 9720 106 3 70-130/20
91-20-3 Naphthalene 666 2000 2660 100 2000 2790 106 5 70-130/20
103-65-1 n-Propylbenzene 375 2000 2360 99 2000 2400 101 2 70-130/20
100-42-5 Styrene ND 2000 1820 91 2000 1880 94 3 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 2000 1810 91 2000 1860 93 3 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 2000 1860 93 2000 1940 97 4 70-130/20
127-18-4 Tetrachloroethylene ND 2000 1800 90 2000 1840 92 2 70-130/20
108-88-3 Toluene 145 2000 1860 86 2000 1910 88 3 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 2000 1840 92 2000 1920 96 4 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 2000 1840 92 2000 1870 94 2 70-130/20
71-55-6 1,1,1-Trichloroethane ND 2000 1830 92 2000 1860 93 2 70-130/20
79-00-5 1,1,2-Trichloroethane ND 2000 1840 92 2000 1900 95 3 70-130/20
79-01-6 Trichloroethylene ND 2000 1800 90 2000 1810 91 1 70-130/20
75-69-4 Trichlorofluoromethane ND 2000 2170 109 2000 2150 108 1 60-140/20
96-18-4 1,2,3-Trichloropropane ND 2000 1890 95 2000 1970 99 4 70-130/20
95-63-6 1,2,4-Trimethylbenzene 484 2000 2400 96 2000 2450 98 2 70-130/20
108-67-8 1,3,5-Trimethylbenzene 103 2000 1980 94 2000 2010 95 2 70-130/20
75-01-4 Vinyl Chloride ND 2000 1960 98 2000 1950 98 1 60-140/20
m,p-Xylene 576 4000 4320 94 4000 4440 97 3 70-130/20
95-47-6 o-Xylene 29.0 J 2000 1860 92 2000 1910 94 3 70-130/20
1330-20-7 Xylene (total)605 6000 6180 93 6000 6350 96 3 70-130/20
CAS No.Surrogate Recoveries MS MSD FA27298-2 Limits
1868-53-7 Dibromofluoromethane 100%100%97%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%102%102%70-130%
2037-26-5 Toluene-D8 99%99%100%70-130%
460-00-4 4-Bromofluorobenzene 100%99%101%70-130%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA27274
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA27304-1MS A0196404.D 5 09/08/15 TD n/a n/a VA1776
FA27304-1MSD A0196405.D 5 09/08/15 TD n/a n/a VA1776
FA27304-1 A0196390.D 1 09/08/15 TD n/a n/a VA1776
FA27304-1 A0196392.D 5 09/08/15 TD n/a n/a VA1776
The QC reported here applies to the following samples:Method: SM 6200B
FA27274-1, FA27274-2, FA27274-3, FA27274-4, FA27274-5, FA27274-6
FA27304-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 191 a 50 231 80 50 238 94 3 70-130/20
108-86-1 Bromobenzene ND 50 45.4 91 50 51.5 103 13 70-130/20
74-97-5 Bromochloromethane ND 50 44.4 89 50 44.7 89 1 70-130/20
75-27-4 Bromodichloromethane ND 50 42.1 84 50 42.2 84 0 70-130/20
75-25-2 Bromoform ND 50 31.1 62*50 34.0 68*9 70-130/20
104-51-8 n-Butylbenzene 0.33 J 50 46.1 92 50 46.3 92 0 70-130/20
135-98-8 sec-Butylbenzene 0.65 50 47.9 95 50 47.6 94 1 70-130/20
98-06-6 tert-Butylbenzene 0.21 J 50 46.9 93 50 46.5 93 1 70-130/20
56-23-5 Carbon Tetrachloride ND 50 43.6 87 50 41.9 84 4 70-130/20
108-90-7 Chlorobenzene ND 50 43.2 86 50 44.3 89 3 70-130/20
75-00-3 Chloroethane ND 50 33.3 67 50 34.4 69 3 60-140/20
67-66-3 Chloroform ND 50 44.9 90 50 46.6 93 4 70-130/20
95-49-8 o-Chlorotoluene ND 50 47.1 94 50 46.4 93 1 70-130/20
106-43-4 p-Chlorotoluene ND 50 46.1 92 50 45.5 91 1 70-130/20
124-48-1 Dibromochloromethane ND 50 36.7 73 50 37.6 75 2 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 43.5 87 50 43.9 88 1 70-130/20
106-93-4 1,2-Dibromoethane ND 50 44.1 88 50 45.3 91 3 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 26.7 53*50 27.6 55*3 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 46.4 93 50 46.3 93 0 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 46.4 93 50 46.4 93 0 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 46.3 93 50 45.7 91 1 70-130/20
75-34-3 1,1-Dichloroethane ND 50 45.0 90 50 46.5 93 3 70-130/20
107-06-2 1,2-Dichloroethane 0.44 J 50 43.9 87 50 45.9 91 4 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 43.5 87 50 44.9 90 3 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 41.3 83 50 42.4 85 3 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 46.7 93 50 47.1 94 1 70-130/20
78-87-5 1,2-Dichloropropane ND 50 44.6 89 50 46.6 93 4 70-130/20
142-28-9 1,3-Dichloropropane ND 50 43.5 87 50 45.0 90 3 70-130/20
594-20-7 2,2-Dichloropropane ND 50 38.1 76 50 39.4 79 3 70-130/20
563-58-6 1,1-Dichloropropene ND 50 45.2 90 50 44.9 90 1 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 39.8 80 50 37.1 74 7 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 44.0 88 50 40.7 81 8 70-130/20
108-20-3 Di-Isopropyl Ether ND 50 45.4 91 50 47.4 95 4 70-130/20
100-41-4 Ethylbenzene 67.6 a 50 111 87 50 113 91 2 70-130/20
87-68-3 Hexachlorobutadiene ND 50 41.2 82 50 42.2 84 2 70-130/20
98-82-8 Isopropylbenzene 3.3 50 49.6 93 50 51.4 96 4 70-130/20
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA27274
Account:GRINCC GRI (Geological Resources Inc.)
Project:Anson Mart; 1250 E Caswell, Wadesboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA27304-1MS A0196404.D 5 09/08/15 TD n/a n/a VA1776
FA27304-1MSD A0196405.D 5 09/08/15 TD n/a n/a VA1776
FA27304-1 A0196390.D 1 09/08/15 TD n/a n/a VA1776
FA27304-1 A0196392.D 5 09/08/15 TD n/a n/a VA1776
The QC reported here applies to the following samples:Method: SM 6200B
FA27274-1, FA27274-2, FA27274-3, FA27274-4, FA27274-5, FA27274-6
FA27304-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 0.68 50 46.1 91 50 46.2 91 0 70-130/20
74-83-9 Methyl Bromide ND 50 34.0 68 50 35.1 70 3 60-140/20
74-87-3 Methyl Chloride ND 50 34.8 70 50 36.2 72 4 60-140/20
74-95-3 Methylene Bromide ND 50 45.8 92 50 47.8 96 4 70-130/20
75-09-2 Methylene Chloride ND 50 44.3 89 50 46.5 93 5 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 50 44.7 89 50 47.6 95 6 70-130/20
91-20-3 Naphthalene 37.8 50 95.3 115 50 91.4 107 4 70-130/20
103-65-1 n-Propylbenzene 6.2 50 54.0 96 50 54.0 96 0 70-130/20
100-42-5 Styrene ND 50 39.7 79 50 42.8 86 8 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 44.7 89 50 45.1 90 1 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 47.5 95 50 48.6 97 2 70-130/20
127-18-4 Tetrachloroethylene ND 50 43.9 88 50 44.7 89 2 70-130/20
108-88-3 Toluene 21.6 50 60.3 77 50 61.1 79 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 42.8 86 50 44.7 89 4 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 42.8 86 50 43.8 88 2 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 44.5 89 50 46.3 93 4 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 45.9 92 50 47.8 96 4 70-130/20
79-01-6 Trichloroethylene ND 50 44.4 89 50 44.7 89 1 70-130/20
75-69-4 Trichlorofluoromethane ND 50 38.3 77 50 39.0 78 2 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 47.0 94 50 48.2 96 3 70-130/20
95-63-6 1,2,4-Trimethylbenzene 70.9 a 50 116 90 50 116 90 0 70-130/20
108-67-8 1,3,5-Trimethylbenzene 0.34 J 50 45.8 91 50 45.8 91 0 70-130/20
75-01-4 Vinyl Chloride ND 50 35.0 70 50 35.8 72 2 60-140/20
m,p-Xylene 8.4 a 100 99.0 90 100 102 93 3 70-130/20
95-47-6 o-Xylene 95.7 a 50 140 89 50 145 99 4 70-130/20
1330-20-7 Xylene (total)104 a 150 239 90 150 246 95 3 70-130/20
CAS No.Surrogate Recoveries MS MSD FA27304-1 FA27304-1 Limits
1868-53-7 Dibromofluoromethane 100%100%97%100%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%103%102%103%70-130%
2037-26-5 Toluene-D8 100%100%100%101%70-130%
460-00-4 4-Bromofluorobenzene 101%97%101%101%70-130%
(a) Result is from Run #2.
* = Outside of Control Limits.
40 of 40
FA27274
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