20029_Shops on Innes _Phase II ESA_20170106

Centerlane Innes Street, LLC
Phase II Environmental Site
Assessment (ESA)

Insert job reference

Centerlane Innes Street, LLC
Phase II Environmental Site
Assessment (ESA)
Revision 1

1517, 1539, & 1541 East Innes Street
Salisbury, North Carolina
January 6, 2017
Centerlane Innes Street, LLC Phase II Environmental Site Assessment (ESA)
January 6, 2017 Cardno ii
Phase II Environmental Assessment (ESA) Report - Revision 1
Centerlane Innes Street, LLC
1517, 1539, & 1541 East Innes Street
Salisbury, North Carolina

Date: January 6, 2017

Prepared for City of Salisbury
217 South Main Street
Salisbury, NC 28144
Planning/Brownfields Director, Janet Gapen
Phone: [phone]
[e-mail]

Joselyn Harriger
Brownfields Program Manager
NCDEQ, Division of Waste Management
1646 Mail Service Center
Raleigh, NC 27699
Phone: [phone]
[e-mail]

David Champagne
Brownfields Project Officer
USEPA Region 4
61 Forsyth Street SW
Atlanta, GA 30303
Phone: [phone]
[e-mail]

Prepared by Cardno, Inc.
10988 Richardson Road, Ashland, VA 23005
Joe Morici, Project Manager
Phone: [phone]
[e-mail]

Centerlane Innes Street, LLC Phase II Environmental Site Assessment (ESA)
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Table of Contents
Report Signature iii
Commonly Used Acronyms vi
Distribution List vii
Report Limitations vii
1 Introduction 1
1.1 Purpose 1
1.2 Site Location & Description 2
1.3 Background 3
1.4 Previous Site Assessments 3
2 Sampling Methodology & Results 4
2.1 Ground Penetrating Radar (GPR) 4
2.2 Soil Samples 5
2.3 Soil Samples SQAPP Deviations 6
2.4 Soil Laboratory Results 6
2.4.1 Soil Sample Results—Volatile Organic Compounds (VOCs) 7
2.4.1 Soil Sample Results—Semi-Volatile Organic Compounds (SVOCs) 7
2.4.2 Soil Sample Results—Polychlorinated Biphenyls (PCBs) 7
2.5 Groundwater Monitor Well Installation and Sampling 8
2.6 Groundwater Samples SQAPP Deviations 9
2.7 Groundwater Laboratory Results 9
2.7.1 Groundwater Sample Results—VOCs 9
2.7.2 Groundwater Sample Results—SVOCs 9
3 Receptor Evaluation / Pathways for Contaminant Transport 10
3.1 On-site Exposure 10
3.2 Off-site Exposure 10
4 Potential Pathways for Future Contaminant Exposure 10
4.1 Soils 10
4.2 Groundwater 10
4.3 Vapor Intrusion 11
5 Data Quality 11
5.1 Quality Control Samples 11
5.2 Property Specific Corrective Actions 12
5.3 Quality Control Parameters 12
5.3.1 Precision 12
5.3.2 Accuracy 13
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5.3.3 Representativeness 13
5.3.4 Comparability 13
5.3.5 Completeness 13
5.3.6 Sensitivity 13
5.4 Laboratory Data Evaluation 13
6 Discussion and Conclusions 14
7 References 16
Figures
1. Topographic Site Location
2. Aerial Site Map
3. Sample Locations Map
4. Organics Concentrations Map
5. Groundwater Elevation Contour Map
Tables
Table 1A: VOC and SVOC Analytes Detected In Soil
Table 1B: PCB Congeners Detected In Soil
Table 1C: VOC and SVOC Analytes Detected In Groundwater
Table 2 Quality Control Precision Analysis
Appendices
A. Ground Penetrating Radar Investigation
B. Analytical Reports w/Chains-of-Custody
C. Boring Logs and Well Construction Records
D. Field Logs

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Commonly Used Acronyms
AAI All Appropriate Inquiry
ABCA Analysis of Brownfield Cleanup Alternatives
ACM Asbestos Containing Material
AST Aboveground Storage Tank
ASTM American Society for Testing & Materials
BFA
BLS
Brownfields Agreement
Below Land Surface
Cardno Cardno, Inc.
CERCLA Comprehensive Environmental Response, Compensation, and Liability Act
CERCLIS Comprehensive Environmental Response, Compensation and Liability Information
System
EP Environmental Professional
ERNS Emergency Response Notification System
EPA Environmental Protection Agency
ESA Environmental Site Assessment
ESI Expanded Site Inspection
FOIA Freedom of Information Act
FIRM Flood Insurance Rate Map
IC Institutional Controls
LBP Lead-Based Paint
LUST Leaking Underground Storage Tank
MSL Mean Sea Level
NCDEQ North Carolina Department of Environmental Quality
NCGS North Carolina Geologic Survey
NFRAP No Further Remedial Action Plan
NPL National Priority List
PA/SI Preliminary Assessment/Site Inspection
PAH Polynuclear Aromatic Hydrocarbon
PCB Polychlorinated Biphenyl
PPB Parts per Billion
PPM Parts Per Million
PRG
QAPP
Preliminary Remediation Goal
Quality Assurance Project Plan
RACM Regulated Asbestos Containing Material
RBC Risk Based Concentrations
RBSL Risk Based Screening Level
RCRA Resource Conservation and Recovery Act
REC Recognized Environmental Condition
SVOC
TAL
Semi-volatile Organic Compound
Target Analyte List
TMS Tax Map Serial
USEPA United States Environmental Protection Agency
USGS United States Geological Survey
UST Underground Storage Tank
VOC

Volatile Organic Compound

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Distribution List
This Phase II Environmental Site Assessment (ESA) for the Centerlane Innes Street, LLC
property in Salisbury, North Carolina will be distributed to the following representatives:
 David Champagne, Brownfields Project Officer, USEPA Region 4, 61 Forsyth
Street SW, Atlanta, GA 30303, Phone: [phone], Email:
[e-mail]
 Joselyn Harriger, Brownfields Project Manager, North Carolina Department of
Environmental Quality (NCDEQ), Division of Waste Management, 1646 Mail
Service Center, Raleigh, NC 27699-1646, Phone: [phone], Email:
[e-mail]
 Janet Gapen, City of Salisbury Planning/Brownfields Director, City of Salisbury,
217 South Main Street, Salisbury, NC 28144, Phone: [phone], Email:
[e-mail]
Report Limitations
All work performed by Cardno was completed in accordance with generally accepted
professional practices related to the nature of the work accomplished, in the same or similar
localities, and at the time the services were performed. This report is for the specific application
to the referenced project and for the exclusive use of the City of Salisbury, North Carolina.
Cardno accepts no liability related to site environmental impact, regardless of the date of impact
findings or occurrence.

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1 Introduction
This Phase II Environmental Site Assessment (ESA) report details the assessment activities
conducted in accordance with the Generic Quality Assurance Project Plan (QAPP) and the Site-
specific QAPP Addendum 5A, Revision 1 (Addendum) prepared for the Centerlane Innes
Street, LLC site located at 1517, 1539, & 1541 East Innes Street in Salisbury, North Carolina
(site/subject property). The assessment presented herein was conducted under a Brownfields
Assessment Grant between the U.S. Environmental Protection Agency (EPA) and City of
Salisbury (Grantee), EPA Cooperative Agreement No. BF-00D26514-0.
The site is comprised of three parcels (TMS #070-002, 070-118, & 070-00301) being purchased
by Centerlane Innes Street, LLC. The properties contain two buildings (one on parcel 070-002,
the other on parcel 070-118) with frontage on East Innes Street with paved parking areas
around the buildings. One building has been a dentist office, and the other has been an
automobile maintenance facility. The subject site previously contained one (1) Underground
Storage Tank (UST) that was removed in 1979 from the northern portion of the property.
The City of Salisbury is supporting the assessment of the subject property in order to assist
redevelopment by determining the extent of possible contamination from identified recognized
environmental conditions (RECs) noted in a Phase I ESA Report completed by Summit on
December 12, 2015. By clarifying the environmental conditions at the site via the Phase II ESA,
the purchasers can now develop a plan, enter into the NCDEQ’s Brownfields Program and
secure necessary funding to clean up the property and render it safe for the future planned
reuse. The Addendum was prepared to meet this goal in support of the potential redevelopment
efforts.
The Addendum identified the current site conditions, site-specific methods of assessment, data
quality assurance measures to be employed, program reporting requirements, and the certified
analytical laboratory to be utilized. The Addendum also provided a schedule of implementation
and included the property owner’s contact information. The Addendum was considered
supplementary to the Generic QAPP, submitted under separate cover. The Generic QAPP was
prepared to outline broad data quality goals for all projects conducted under the Brownfields
Program in Salisbury, North Carolina. The Generic QAPP and the Addendum were amended
to reflect comments by EPA and the North Carolina Department of Environmental Quality
(DEQ) technical reviewers, where necessary. Signed, executed copies of each document are
on file with the Grantee and each agency for public review.
1.1 Purpose
The Grantee will use the information gathered from this assessment to assist Centerlane Innes
Street, LLC, in redeveloping the property into commercial restaurant and retail establishments.
Centerlane Innes Street, LLC, is purchasing the properties for redevelopment and has enrolled
them in the NCDEQ’s Brownfields Program.
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This Phase II ESA was conducted to clarify the potential environmental issues identified on the
site. The Phase II ESA included critical data collection of samples of soil and groundwater in
anticipation of facilitating the redevelopment. Determining if soils and groundwater on the site
are impacted with hazardous substances or petroleum in excess of allowable DEQ standards
will aid in decisions on site redevelopment and removal activities to ensure no unacceptable
exposures remain. The sampling and analysis plan was developed in conjunction with the
NCDEQ Project Manager to meet the requirements of the North Carolina Brownfields Program
and facilitate a brownfields agreement between NCDEQ and the developer.
1.2 Site Location & Description
The property is irregularly shaped, totaling approximately 4.07-acres on East Innes Street in
Salisbury, NC. Parcel 070-002 is approximately 3.05 acres and was originally developed as
Fowler Motors, an automobile dealership and repair facility. Parcel 070-118 is approximately
1.0 acres and includes a former dental office. Parcel 070-00301 is approximately 0.015 acres
and is undeveloped. The property coordinates are 35.6525 north latitude, 80.4568 west
longitude. A Site Location Map, consisting of the relevant parts of the United States Geological
Survey (USGS) topographic map, Salisbury Quadrangle, is included as Figure 1.
The commercial buildings on the property have the assigned addresses of 1517 (070-002),
1539 (070-118), and 1541 (070-0031) East Innes Street. The site is bordered to the north, east,
south and west by commercial properties.
According to the USGS and the North Carolina Geologic Survey (NCGS), the subject property
is located in the Piedmont Physiographic Province of North Carolina. The rock type at the site
has been identified as granite. The shallow subsurface in most areas of the Piedmont contains
residual soil overburden, including structure-free residuum, saprolite, and partially weathered rock
(PWR) that derive from in-place weathering of the crystalline bedrock. Occasional areas
containing recent deposits of alluvium in the uppermost subsurface are found near streams and
rivers. Saprolite and PWR typically contain some relict structures from the original rock material.
Depth to rock ranges from ground surface at occasional outcrops to depths of greater than 100
feet in areas of easily weathered rock.
According to the Groundwater Atlas of the United States, the most widespread aquifers in the
Piedmont and Blue Ridge Provinces are the crystalline-rock and undifferentiated sedimentary-
rock aquifers. Most of the rocks that compose these aquifers are crystalline metamorphic and
igneous rocks of many types. The main types of crystalline rocks are coarse-grained gneisses
and schists of various mineral composition; however, fine-grained rocks, such as phyllite and
metamorphosed volcanic rocks, are common in places. The undifferentiated sedimentary-rock
aquifers consist of tightly cemented, predominately clastic rocks, many of which grade into
metamorphic rocks. Unconsolidated material called regolith overlies the crystalline-rock and
undifferentiated sedimentary-rock aquifers almost everywhere. The regolith consists of
saprolite, colluvium, alluvium, and soil. Saprolite is a blanket of decomposed or partially
decomposed rock that is usually thick and clayey, and whose texture varies depending on the
type of parent bedrock from which the saprolite is derived. Colluvium is weathered rock material
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that has slumped downward from hillsides. Alluvium consists mostly of water-transported
sediment in stream valleys and channels. Because the regolith material varies greatly in
thickness, composition, and grain size, its hydraulic properties also vary greatly.
Groundwater in the Piedmont Physiographic Province is typically found in unconfined or semi-
confined conditions with a flow that generally mimics the topography. The USGS Topographic
Map, Salisbury Quadrangle (Figure 1), indicated that regional groundwater was expected to
follow the topography by flowing predominately north towards Town Creek.
On-site groundwater monitoring wells installed as part of this ESA found groundwater at depths
ranging between 16.8 and 20.8 feet bgs. Groundwater flow onsite is to the north and north-
northwest as shown by the Groundwater Elevation Contour Map, Figure 5.
1.3 Background
Parcel 070-002 was originally developed as Fowler Motors, an automobile dealership and
repair facility. After the dealership closed, the buildings were partially leased as a restaurant
and nightclub. An UST was removed from the north side of the building in 1979. The building
is now vacant and in poor condition. The City of Salisbury has condemned the building.
Parcel 070-118 has operated as a dentist office for almost 40 years. Parcel 070-00310 is
undeveloped.
During a site visit conducted with the NCDEQ Project Manager on October 11, 2016, the former
UST, former hydraulic lifts within the dealership building’s maintenance areas, a potential wash
pad on the outside of the dealership building, and off-site former drycleaners were identified as
areas of concern. An aerial photograph of the property is included as Figure 2.
1.4 Previous Site Assessments
2015 Phase I ESA: Summit completed a Phase I ESA of the subject property on December 12,
2015, and identified the following REC:
 The subject site previously contained one (1) Underground Storage Tank (UST) on the
northern portion of the property. The EDR report indicates the UST was removed in
1979. Additionally, the property was previously used as an automobile maintenance
facility. There are floor drains along the western portion of the building.
2016 Limited Phase II ESA: Summit completed a Limited Phase II ESA on the subject property
on February 3, 2016. Two (2) groundwater samples were collected from locations on-site
identified to represent the highest potential for impact from the operation of a former auto repair
facility and associated underground storage tank system. Three (3) sampling locations were
planned for this assessment; however, utility conflicts and current tenant conflicts limited the
installation to samples on the north and south sides of the building. This sampling scope of
services was completed to determine if former site uses may have impacted the subject site.
All groundwater samples were analyzed for the presence of Volatile Organic Compounds
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(VOCs) by EPA method 8260 and Semi-Volatile Organic Compounds (SVOCs) by EPA method
8270.
Tetrachloroethene (a.k.a. PCE) was detected in groundwater collected from a sampling point
on the south side of the building at 16 ug/L, above the NCDEQ regulatory concentration of 0.7
ug/L. Tetrachloroethene is a chlorinated solvent commonly utilized in automotive degreasers,
cleaners, and dry cleaning chemicals. Based on the results, Summit concluded that the site use
as a former auto repair facility has impacted the site.
2 Sampling Methodology & Results
The following sections outline the methodology used for collecting the environmental samples
and the results of the investigation at the site. A Sample Location Map depicting the locations
of the soil borings and groundwater monitor wells is included as Figure 3.
Any deviations from the SOW (Scope of Work) approved in the Addendum are detailed in the
appropriate sections of this report.
Soil boring and well installation, equipment decontamination, and sample collection activities
were conducted using best practices and the professional judgment of Summit personnel in
accordance with the USEPA Region 4 Science and Ecosystem Support Division (SESD) Field
Branches Quality System and Technical Procedures. Careful handling of samples and
equipment was observed throughout the sampling procedures to avoid cross contamination.
Samples were kept at approximately four degrees centigrade (4oC) throughout the operation
and during shipment to Prism Laboratories, Inc. (Prism) for analysis. Chain-of-custody forms
were maintained during the shipping and handling process to document sample integrity.
Copies of these forms are included with the laboratory analytical reports in Appendix B.
Assessment activities at the subject property included the collection of soil and groundwater
samples from predetermined locations across the site for laboratory analysis. Cardno personnel
performed a Ground Penetrating Radar (GPR) field investigation on November 14, 2016.
Summit installed groundwater monitoring wells on November 14 and 15, 2016, and collected
groundwater samples on November 16. The soil samples were collected on November 14 and
15, 2016.
2.1 Ground Penetrating Radar (GPR)
Cardno personnel performed a Ground Penetrating Radar (GPR) field investigation on
November 14, 2016, prior to conducting any soil boring. The GPR used a GSSI Utility Scan LT
GPR system, configured with a 500 MHz antenna array and a 45-nanosecond time range, to
collect radar data. The GPR was confined to areas previously targeted for borings and was not
intended to discover unknown sources across the entire site. The GPR found a large anomaly
at the south of the property near the automotive repair building. The anomaly was found
approximately 2 feet deep and had dimensions of 5 feet in width and 10 feet in length. Based
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on its dimensions and GPR characteristics, the anomaly was determined to most likely be a
previously undiscovered UST. Cardno believes the UST was likely used for heating oil due to
its location at the front of the building (away from the automotive repair areas) and its proximity
to a chimney stack. The GPR report is included as Appendix A.
2.2 Soil Samples
Summit personnel collected eight surface soil (0-2’ bgs) and seven soil borings (majority 8-10’
bgs) in order to assess soil conditions across the property. The soil borings were installed at
the approximate locations depicted in Figure 3. Samples were collected for Target Compound
List (TCL) VOCs by EPA Method 8260; TCL SVOCs by EPA Method 8270; and/or TCL PCBs
by EPA Method 1668.
Samples CIS-01, CIS-02, CIS-03 & CIS-04 were collected via continuous split spoon sampler
that extended into the water table. Samples were screened at one foot intervals for VOCs using
a MiniRAE 2000 Photoionization Detectors (PID) with an 11.7 eV detector lamp. No PID
readings were observed at any depth. Surface soil samples (0-2’ bgs) were collected at each
location as per the Addendum for VOCs and SVOCs. The borings were extended after
collection of the soil samples to install the monitoring wells. Boring logs are provided in
Appendix C.
Samples CIS-05 through -13 were collected via use of a direct-push technology (DPT) rig to
collect continuous soil columns down to ten feet deep. Borings were collected into 4 foot
disposable cellulose acetate butyrate core barrel liners, which were then characterized for soil
morphology and screened with the PID. Borings were collected and screened from both ends
of the former automotive hydraulic lifts in each of the locations CIS-06, CIS-07, CIS-08, CIS-
09, CIS-10, and CIS-12; however, only one sample from each area was selected for laboratory
analysis after PID screening. The specific samples collected for further analysis as per the
Addendum are as follows:
 No PID readings were observed at the CIS-05 location. A surface soil sample (0-2’ bgs)
was collected for VOCs and SVOCs.
 No PID readings were observed at either boring at the CIS-06 location. A subsurface
soil sample (8-10’ bgs) was collected for VOCs, SVOCs and PCBs from the west boring.
 No PID readings were observed at either boring at the CIS-07 location. A surface soil
sample (0-2’ bgs) for VOCs and SVOCs, and a subsurface soil sample (8-10’ bgs) for
VOCs, SVOCs and PCBs was collected from the west boring
 No PID readings were observed at either boring at the CIS-08 location. A subsurface
soil sample (8-10’ bgs) for VOCs, SVOCs and PCBs was collected from the west boring.
 The highest PID reading was observed at 8-10’ bgs in the west boring at the CIS-09
location. No PID readings were observed at in the east boring. A surface soil sample (0-
2’ bgs) for VOCs and SVOCs, and a subsurface soil sample (8-10’ bgs) for VOCs,
SVOCs and PCBs was collected from the west boring.
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 The highest PID reading was observed at 8-10’ bgs in the west boring at the CIS-10
location. No PID readings were observed at in the east boring. A subsurface soil sample
(8-10’ bgs) for VOCs, SVOCs and PCBs was collected from the west boring.
 No PID readings were observed in the boring at the CIS-11 location. A surface soil
sample (0-2’ bgs) for VOCs, SVOCs and PCBs was collected based on observation of
native soil immediately underlying the slab, which was thought suggestive of offering the
highest probability of documenting an impact.
 No PID readings were observed at either boring at the CIS-12 location. A subsurface
soil sample (8-10’ bgs) for VOCs, SVOCs and PCBs was collected from the west boring.
 The highest PID reading was observed at 6’ bgs in the CIS-13 boring. A subsurface soil
sample (4-6’ bgs) for VOCs and SVOCs was collected.
2.3 Soil Samples SQAPP Deviations
The Addendum included collection of subsurface soil samples (greater than 2’ bgs) if PID
screening observed any readings above the water table at locations CIS-01, CIS-02, CIS-03,
and CIS-04. No PID readings were observed in any of these locations and the subsurface
samples were not collected.
The sample location CIS-05 was moved slightly from its planned location to place it closer to
the UST discovered during the GPR investigation. The sample CIS-13-SB was added so as
have a sample location on the other side of that UST.
The location for CIS-11 was listed in the Addendum’s Table 2 as either a surface or subsurface
soil. The soil boring displayed typical native soils, no fill material, and no PID readings. Based
on best professional judgement, the surface sample from just below the slab was determined
to be offer the highest possibility for impacts.
No other deviations occurred from the Addendum.
2.4 Soil Laboratory Results
The soil analytical data are provided in the laboratory analytical reports included in Appendix
B.
The laboratory analytical results were compared to the Industrial Preliminary Soil Remediation
Goals (PSRG) for direct soil exposure and the protection of groundwater, as listed the most
recent (October 2016) version of the NCDEQ Inactive Hazardous Sites Branch (IHSB) PSRG
Table. Analytes detected in the soil samples and the comparisons to the screening values are
presented in Table 1A and 1B and depicted in Figures 4.
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2.4.1 Soil Sample Results—Volatile Organic Compounds (VOCs)
All soil samples were analyzed for VOCs. The VOCs detected in the soil samples and the
comparisons to the screening values are presented in Table 1A.
VOCs were not detected in any of the surface soil samples (0-2’ bgs).
VOCs were not detected in any of the subsurface soil samples with the exception of CIS-09-
SB and CIS-10-SB, which found Acetone, Xylenes, Methyl Butyl Ketone, Methyl Ethyl Ketone,
and Toluene at concentrations several orders of magnitude lower than the applicable NCDEQ
reference values. Tetrachloroethylene was detected in both samples, with the concentration in
CIS-10-SB slightly higher than the NCDEQ Protection of Groundwater reference value. The
detected VOCs are commonly associated with petroleum and solvent-cleaning operations at
repair facilities.
2.4.1 Soil Sample Results—Semi-Volatile Organic Compounds (SVOCs)
All soil samples were analyzed for SVOCs. The SVOCs detected in the soil samples and the
comparisons to the screening values are presented in Table 1A.
SVOCs were not detected in any of the surface soil samples with the exception of CIS-05-SS,
which found Fluoranthene and Pyrene at low estimated concentrations. These SVOCs are
commonly associated with asphalt.
SVOCs were not detected in any of the subsurface soil samples with the exception of CIS-09-
SB, which found 2-Methylnaphthalene, and CIS-10-SB, which found Phenanthrene. These
SVOCs are commonly associated with asphalt and certain automotive fluids from their use as
chemical feedstocks for dyes and plasticizers.
All SVOCs were found at concentrations several orders of magnitude lower than their applicable
NCDEQ reference values
2.4.2 Soil Sample Results—Polychlorinated Biphenyls (PCBs)
The subsurface soil samples collected around each hydraulic lift and one surface soil sample
(at CIS-11) were analyzed for PCBs. The PCBs detected in the soil samples and the
comparisons to the screening values are presented in Table 1B.
The PCBs as listed on the EPA’s TCL are actually mixtures of numerous PCB chemical
compounds known as “congeners”. The TCL compounds become identified as one compound
because the usual analytical method does not distinguish between the congeners but instead
looks for characteristic fingerprint patterns. Since hydraulic fluids reportedly contain trace
concentrations of PCBs, the samples were analyzed for all congeners in order to achieve lower
detection levels at the request of the NCDEQ.
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A total of 98 PCB congeners were detected. Sample CIS-11-SS had 73 congeners and CIS-
09-SB had 69 congeners, whereas only 2 were detected in CIS-07-SB, and the other samples
averaged around 25 each.
The NCDEQ has soil exposure reference values for only three of the 92 PCB congeners. The
detected onsite concentrations of these three congeners (PCB 105, PCB 118, and PCB 156)
are orders of magnitude lower than their respective Industrial PSRG as shown in Table 1B.
The US EPA also recommends evaluation of PCB congener concentrations through use of
Toxicity Equivalence Factors (TEFs). This process considers the health effects of PCBs as if
they were a milder form of a Dioxin compound (2,3,7,8-Tetrachlorodibenzo-p-dioxin). Since the
toxic effects of PCBs are not as severe as the Dioxin compounds, TEFs are used to calculate
the amount of Dioxin that produce the same impact as the PCB concentration (by multiplication
of the PCB concentration times the TEF).
Most PCB congeners do not have assigned TEF values, as the EPA does not have sufficient
data to determine if they have any toxic effect. However, using the assumption that all
congeners are equally as toxic as those with assigned TEFs allows calculation of an upper-
bounds estimate of the Toxic Equivalence (TEQ) of Dioxin in a sample. With few exceptions,
the highest TEFs assigned to PCBs, including the 3 onsite with PSRGs, is 0.00003. CIS-10-SB
had the highest total PCB concentration onsite (103,000 picograms per gram, i.e., 0.1 ppm).
Therefore, if all of this concentration is assumed to be as bad as those with assigned TEFs, the
sample has the TEQ of approximately 3 parts per trillion (ppt) Dioxin, which is considerably less
than the NCDEQ’s Protection of Groundwater 1,100 ppt Dioxin reference value.
The finding of PCB congeners around the hydraulic lifts suggest releases of hydraulic fluids
occurred at the sampled locations; however, the magnitude of the concentrations indicate that
the releases were negligible and of no impact.
2.5 Groundwater Monitor Well Installation and Sampling
Following collection of the soil samples at locations CIS-01 through -04, two-inch diameter,
polyvinyl chloride (PVC) monitoring wells were installed in the borings with hollow-stem augers.
The wells were installed by Summit (Well Driller: Robert Cassell, NC Well Contractor
Certification #4143-A). The sample locations are depicted on Figure 3.
The completed well depths ranged from 30’ to 35’ bgs. Each well had a 20-foot 0.010-inch
screen section installed to bracket the water table. The annular space within the borings was
filled with well-graded, pre-washed silica sand from the total depth to approximately one to two
feet above the screen, and the sand pack was capped by a bentonite seal. Grout was then
used to fill the remaining length of annular space. Well construction information is provided in
Appendix C.
The wells were allowed to equilibrate 24-48 hours prior to purging and sample collection.
Purging was accomplished via the low-flow method using a reverse flow peristaltic pump and
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new dedicated tubing until consistent values (i.e., less than 10% variance between consecutive
readings) were obtained for dissolved oxygen, specific conductivity, and temperature, and pH
measurements. The purging and sample collection details are included in the Field Logs
included as Appendix D.
2.6 Groundwater Samples SQAPP Deviations
No deviations occurred from the Addendum.
2.7 Groundwater Laboratory Results
All groundwater samples were collected for VOC and SVOC analysis. The groundwater
analytical data are provided in the laboratory analytical reports included in Appendix B.
The laboratory analytical results were compared to the North Carolina Groundwater Standards
(2L Standards; Title 15A, NCAC, Subchapter 2L, Part .0202) and the NCDEQ Division of Waste
Management’s Groundwater Vapor Intrusion Screening Levels. Analytes detected in
groundwater and the comparisons to screening values are presented in Table 1C and Figure
5.
2.7.1 Groundwater Sample Results—VOCs
The solvent Tetrachloroethylene (aka Perchloroethylene or PCE) was detected in all wells
above the NCDEQ Groundwater 2L reference value. The PCE concentration in the most
upgradient well, CIS-04-MW, was one to two orders of magnitude higher than in the other wells.
The locations CIS-04 and CIS-02 were situated so as to underlie the footprints of buildings
planned for the site; the PCE concentrations in both exceeded the NCDEQ Groundwater Vapor
Intrusion reference values.
PCE is common in some automotive degreasers, but is mostly known as a drycleaning solvent.
The PCE distribution indicates a dissolved phase plume has moved onto the property from
offsite sources. An automotive repair facility (Tire Kingdom) formerly operated less than 200
feet away in the upgradient direction and was listed as a RCRA Conditionally Exempt Small
Quantity Generator of PCE wastes. A former drycleaner (Avalon Cleaners) operated less than
600 feet away in the upgradient direction; however, the type of drycleaning solvents used are
not identified in the available documentation.
The upgradient monitoring well, CIS-04-MW, also detected Chloroform and
Trichlorofluoromethane at estimated, low concentrations. Both compounds are byproduct
constituents of the drinking water chlorination process. The low levels detected are consistent
with leaking water pipes (either drinking water or waste water) in an upgradient direction.
2.7.2 Groundwater Sample Results—SVOCs
No SVOCs were detected in any of the groundwater samples.
Centerlane Innes Street, LLC Phase II Environmental Site Assessment (ESA)
January 6, 2017 Cardno 10
3 Receptor Evaluation / Pathways for Contaminant Transport
3.1 On-site Exposure
Receptors are unlikely to be currently impacted by contamination since there are no complete
exposure pathways with likely receptors on the property.
This ESA did not find meaningful concentrations of contaminants in any surface soil sample,
suggesting that direct contact is unlikely as a complete pathway even for trespassers onto the
property.
Groundwater at the site is contaminated with high concentrations of PCE, but is not used for
either drinking or irrigation water.
The levels of PCE exceed the NCDEQ Groundwater Vapor Intrusion reference values at two
locations. One of the locations is adjacent to the former automotive repair building, suggesting
that unintended exposures may occur if vapor intrudes into the building. The building is
condemned and unoccupied. It is unlikely to be returned to use without complete
redevelopment of the site.
3.2 Off-site Exposure
It was beyond the scope of this ESA to evaluate contaminant levels off of the subject property.
Cardno believes the onsite groundwater impact is attributable to offsite sources that are
potentially unknown and may be at some distance from the property. Depending on the distance
to these sources, the groundwater plume may spread laterally onto other properties making the
surrounding properties potentially subject to the same risks of groundwater and vapor intrusion
exposure as the property.
It is unknown whether water supply wells are in use nearby. Therefore, complete pathways for
offsite groundwater exposure are unknown and additional assessment may be needed.
4 Potential Pathways for Future Contaminant Exposure
4.1 Soils
The soil samples did not detect meaningful concentrations of contaminants above the direct
exposure reference values.
4.2 Groundwater
Groundwater contaminated with PCE was present at 16 to 21 feet deep. The contamination
appears to be entering the property from offsite sources. However, without a network of
monitoring wells distributed across multiple properties in the upgradient direction (which is
beyond the scope and financial constraints of the EPA grant), it cannot be determined if the
Centerlane Innes Street, LLC Phase II Environmental Site Assessment (ESA)
January 6, 2017 Cardno 11
monitoring wells installed during this ESA are directly in the major component of the plume flow.
Based on the regional topography, the measured groundwater elevations, and the PCE
distribution in the onsite wells, it is likely that high concentrations of PCE may extend to and
beyond the property’s northeast corner. The topography further suggests the water table may
be encountered at slightly shallower depths at the property’s northeast corner.
Although it is unlikely to be used for drinking water, the shallow water table could be easily
accessed for irrigation use with unpermitted well drilling methods such as hand augers or water-
jet drilling. Restrictions to groundwater use at the site are justified to prevent contaminant
transport to receptors, once the property is redeveloped.
4.3 Vapor Intrusion
The PCE concentrations exceed the NCDEQ Groundwater Vapor Intrusion reference values at
the two locations where buildings are planned. As noted above, the plume morphology cannot
adequately be determined without a network of offsite monitoring wells, but it is likely that high
PCE concentrations may extend to and beyond the property’s northeast corner. This finding is
suggestive that a complete exposure pathway may occur in the future development, if the
buildings are constructed without regard to possible vapor intrusion control.
Cardno cautions that vapor intrusion into buildings is highly dependent on climatic factors,
building construction, and the sub-surface soil morphology, geologic features, and
contamination distribution. Cardno is not aware of any local environmental testing to prove or
disprove vapor intrusion as a potential concern to the future buildings. Soil vapor testing and
implementation of protective building practices to limit intrusion may be warranted before
occupancy of the site.
5 Data Quality
The Addendum set forth the procedures and methods for data collection and defined the
specific procedures and adjustments necessary to maintain data quality to support project
decisions. The Addendum required both field and laboratory checks to monitor conformance to
project quality limits. Sample duplicates, equipment blanks, trip blanks, and field blanks were
analyzed in order to help evaluate data quality.
5.1 Quality Control Samples
Duplicate Samples: A duplicate surface soil, CIS-03-SSD, and a duplicate groundwater
sample, CIS-4-MWD, was collected for VOC and SVOC analysis. Duplicate samples were not
collected for PCB analysis due to the high cost of the PCB congener identification method.
Duplicate analytical results are included in Table 1A and 1C.
Centerlane Innes Street, LLC Phase II Environmental Site Assessment (ESA)
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Equipment Blank and Field Blanks: One equipment blank, CIS-3-EB, and one field blank,
CIS-4-FB, were collected for VOC, SVOC and PCB analysis. Analytical results are included in
Table 1A and 1B.
Trip blanks: Trip blanks provided by the laboratory accompanied each cooler of samples
submitted to the laboratory. Four trip blanks were analyzed for VOCs and included in Appendix
B.
No concentrations of analyzed compounds were reported in the equipment blank, field blank,
or trip blank samples above the laboratory reporting limit.
5.2 Property Specific Corrective Actions
A field methods audit was not conducted during the field work for this site; however, the field
practices were conducted in a method consistent with the methodology of the QAPP
documents, relevant standard operating procedures, and professional judgment.
5.3 Quality Control Parameters
To assess whether quality assurance (QA) objectives for this project have been achieved, the
following quality control (QC) parameters were considered: precision, accuracy,
representativeness, comparability, completeness, and sensitivity.
5.3.1 Precision
As described in the QAPP, precision is evaluated using the relative percent difference (RPD)
between an actual sample and a duplicate sample. A comparison of the sample duplicates and
their corresponding sample results was made to evaluate the reproducibility of the sample
results based on the laboratory analysis and sample collection and transportation procedures.
A summary of the comparison is included as Table 2.
For this comparison, if the duplicate or sample results are less than five times the reporting
detection limit (RDL), the comparison is made by the absolute difference between the results
(sample - duplicate). If the difference was less than twice the RDL, precision is considered
“acceptable.” If both the sample and duplicate results are greater than five times the RDL, the
precision is assigned as specified in the SQAPP based on the %RPD (difference in results
divided by the average of the results times 100).
These comparisons were conducted on the analytes detected at any concentration or estimated
concentration in CIS-04-MW and its corresponding Duplicate GIS-04-MWD. Since the soil
sample selected for a duplicate, CIS-03-SS, did not detect any analytes above the laboratory
reporting limits, no comparison could be made for the soil samples.
Concentrations of three VOCs were reported in the groundwater samples. Two were reported
at low concentrations with no reported difference between either original or duplicate sample.
Centerlane Innes Street, LLC Phase II Environmental Site Assessment (ESA)
January 6, 2017 Cardno 13
PCE was reported at high concentrations in both samples, with a calculated %RPD of 12.7%,
which is within the “Acceptable” range.
5.3.2 Accuracy
Accuracy is evaluated using a percent recovery measured in spiked and un-spiked samples.
Accuracy is a function of the laboratory method. Parameters regarding accuracy are included
in the lab reports provided by the laboratory included in Appendix B. The laboratory reported
no deviations in the accuracy parameters that would affect the sample results.
5.3.3 Representativeness
Cardno has evaluated the representativeness of the Phase II ESA activities to document the
degree to which the sample data accurately and precisely represents environmental conditions.
Review of field methods and procedures indicated that sample collection, handling, and
transportation, as well as the placement of sample locations with respect to potential sources
of impact, were conducted in general accordance with the Generic QAPP and Addendum.
5.3.4 Comparability
To produce comparable data, the units specified for analytical results obtained during the field
activities are consistent throughout this project and standardized analytical methods have been
used for each parameter.
5.3.5 Completeness
Laboratory analysis was completed on each of the samples collected in the field and submitted
for analysis. Laboratory completeness was determined to be 100%.
5.3.6 Sensitivity
Laboratory RDLs and method detection limits (MDLs) were sufficient to report concentrations
below regulatory standards for the majority of analytes. Some samples required dilution due to
matrix interferences. Data qualifiers included potential high biases due to elevated continuing
calibration verification and estimated concentrations above the instrument’s calibration range.
However, it is Cardno’s opinion that the dilutions and data qualifiers do not affect the project
objectives.
5.4 Laboratory Data Evaluation
The laboratory completed validation and verification of laboratory processes and data, and
delivered a laboratory report to the Cardno Project Manager. The laboratory report and the QC
information provide documentation of compliance with the Generic QAPP and Addendum.
Data usability determination is also a part of data evaluation. Within any matrix it is likely that
certain samples may have parameters that require qualifier codes. Prism includes various
Centerlane Innes Street, LLC Phase II Environmental Site Assessment (ESA)
January 6, 2017 Cardno 14
qualifiers, listed in Tables 1A through 1C, when presenting data. No qualifier codes were
identified that exclude a data point from being usable.
In reviewing the laboratory results, the detection for Tetrachloroethylene in CIS-04-NCW is
listed with the “Aa” qualifier, indicating the analysis was run out of holding time. Prism confirmed
the result was above calibration on the initial run, so a confirmation run was ran outside of
holding time to confirm the initial result. The initial result was reported; therefore, the qualified
data is considered acceptable for making site management decisions.
Several analytes are also reported as detections with “J” data qualifiers, indicating the reported
value is an estimate reported within the 95% confidence interval. These compounds were
detected above the MDL, but below the RDL. The MDL is the lowest concentration at which an
analyte can be detected in a sample by the particular laboratory method used. “Detected”
indicates that the analyte can be distinguished from the blank with reasonable certainty. The
RDL (also called practical quantitation limit, or PQL) is approximately five times the MDL or the
lower calibration standard, whichever is higher. Results above the report limit can be
distinguished from the blank and fall within applicable standard curves. For the purposes of this
assessment, all “J” qualified data are considered acceptable for making site management
decisions.
6 Discussion and Conclusions
This Phase II ESA was performed in order to determine if soil and groundwater impacts exist
at the site as a result of historical property uses identified during previous Phase I and Phase
II ESAs. The specific concerns thought to impact redevelopment of the site include:
• Potential soil impacts from on-site automobile repair operations and the presence of at
least five (5) hydraulic lifts (a sixth lift was discovered once the building was cleared for
the field work).
• Potential soil impacts from a suspected wash pad on the south side of the automobile
repair building (a suspected UST was also discovered next to the wash pad after a GPR
survey of the site).
• Potential soil impacts from an unknown rectangular pad in the automobile repair facility.
• Potential groundwater impacts from on-site automobile repair operations and offsite dry
cleaners.
The decision rule outlined in the Data Quality Objectives (DQOs) for this brownfields project,
as presented in the Addendum, indicates that entry into the NCDEQ Brownfields program
should be pursued in the event that analytes are observed in site media at concentrations
exceeding regulatory limits.
This Phase II ESA found concentrations of VOCs, SVOCs and PCBs in subsurface soils around
the hydraulic lifts. However, the magnitude of the concentrations suggest that any releases
have been minor and are unlikely to impact redevelopment decisions. PCE is the only soil
Centerlane Innes Street, LLC Phase II Environmental Site Assessment (ESA)
January 6, 2017 Cardno 15
contaminant exceeding a regulatory threshold value, in that it barely exceeds the NCDEQ
Protection of Groundwater value in one sample from a 10 foot depth. Given the high
concentration of PCE that appears to be migrating onto the site from elsewhere, it is uncertain
if the small amount detected onsite will be a contributory factor to further groundwater
contamination. Also, it is possible that the low concentration detected in the deep soil sample
may have originated via the groundwater plume via either a vapor pumping mechanism (as the
hydraulic lifts move up and down) or from variable groundwater levels leading to trapping of
residual concentrations in other organic materials in the soil.
The Phase II ESA did not find evidence of soil impacts from the suspected wash pad, the
unknown rectangular pad, or the suspected UST identified during the GPR survey.
The PCE concentration in groundwater appears to be entering the property from offsite sources;
however, it was beyond the scope of this ESA to determine its upgradient source. Based on the
regional topography, the measured groundwater elevations, and the PCE distribution in the
onsite wells, it is likely that high concentrations of PCE may extend to and beyond the property’s
northeast corner. The PCE concentrations exceed the NCDEQ Groundwater Vapor Intrusion
reference values at the two locations where buildings are planned. This finding is suggestive
that a complete exposure pathway may occur in the future development, if the buildings are
constructed without regard to possible vapor intrusion control.
Soil vapor testing and implementation of protective building practices to limit intrusion may be
warranted before occupancy of the site. Development of the site should proceed under the
oversight of the NCDEQ Brownfields Program to ensure minimal exposure.

Centerlane Innes Street, LLC Phase II Environmental Site Assessment (ESA)
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7 References
Cardno. Site-specific QAPP Addendum 5A for Brownfields Phase II ESA - Revision 1.
Centerlane Innes Street, LLC Site, Salisbury, NC, November 10, 2016
Summit, Phase I Environmental Site Assessment, East Innes Street Project, Salisbury,
North Carolina. December 12, 2015.
Summit, Limited Phase II Environmental Site Assessment, East Innes Street Property,
Salisbury, North Carolina. February 3, 2016
NCDEQ Division of Water Quality. Groundwater Quality Standards, Section 15A NCAC
02L.0202 of the North Carolina Administrative Code Title 15A (9/18/14)
NCDEQ Division of Water Quality. Well Construction Standards, Section 15A NCAC
2C.0108 of the North Carolina Administrative Code Title 15A (October 1, 2009)
NCDEQ Division of Water Quality. Inactive Hazardous Sites Branch Preliminary Soil
Remediation Goals (PSRG) Table. September 2015.
USEPA Region 4. SESD, Field Branches Quality System and Technical Procedures.
February 2013.
USEPA Region 4. SESD, Field Branches Quality System and Technical Procedures.
February 2008.
USEPA Regional Screening Levels Master Table. November 2015.
North Carolina Department of Environment, Health and Natural Resources,
Geochemical Atlas of North Carolina, 1993.
USEPA. Hazardous Waste Land Treatment Trace Chemical Element Content of Natural
Soils. 1983
USEPA. Recommended Toxicity Equivalence Factors (TEFs) for Human Health Risk
Assessments of 2,3,7,8-Tetrachlorodibenzo-p-dioxin and Dioxin-Like Compounds,
December 2010

Centerlane Innes Street, LLC Phase II Environmental Site Assessment (ESA)
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Cardno
FIGURES

File Name:
Project Mngr:
Designed By:
Checked By:
Approved By:Drawn By:
Scale:
Project No.
Date:
JHM
BJK
JHM
JHM
FIGURES_PHASE2_Centerlane_1517-Innes-St.dwg
1812 Lincoln St., Suite 301
Columbia, SC 29201
803-929-6060
Figure 1 - Topographic Site Location
Centerlane Innes St.
1517 E. Innes St.
Salisbury, North Carolina
PB00109000
1" = 1000'
01/03/2017
BJK
Subject Property
Notes:
1. Portions of USGS 7.5" Salisbury Quad
(Feet)
01000 1000500
GRAPHIC SCALE
File Name:
Project Mngr:
Designed By:
Checked By:
Approved By:Drawn By:
Scale:
Project No.
Date:
JHM
BJK
JHM
JHM
FIGURES_PHASE2_Centerlane_1517-Innes-St.dwg
1812 Lincoln St., Suite 301
Columbia, SC 29201
803-929-6060
Figure 2 - Aerial Site Map
Centerlane Innes St.
1517 E. Innes St.
Salisbury, North Carolina
PB00109000
1" = 125'
01/03/2017
BJK
Notes:(Feet)
0125 12575
GRAPHIC SCALE
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Designed By:
Checked By:
Approved By:Drawn By:
Scale:
Project No.
Date:
JHM
BJK
JHM
JHM
FIGURES_PHASE2_Centerlane_1517-Innes-St.dwg
1812 Lincoln St., Suite 301
Columbia, SC 29201
803-929-6060
Figure 3 - Sample Locations Map
Centerlane Innes St.
1517 E. Innes St.
Salisbury, North Carolina
PB00109000
1" = 75'
01/03/2017
BJK
Notes:(Feet)
075 75
GRAPHIC SCALE
LEGEND
Approximate Property Boundary
Monitoring Well/Sample Location
Soil Boring Location
F
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Designed By:
Checked By:
Approved By:Drawn By:
Scale:
Project No.
Date:
JHM
BJK
JHM
JHM
FIGURES_PHASE2_Centerlane_1517-Innes-St.dwg
1812 Lincoln St., Suite 301
Columbia, SC 29201
803-929-6060
Figure 5 - GW Elevation Contour Map
Centerlane Innes St.
1517 E. Innes St.
Salisbury, North Carolina
PB00109000
1" = 75'
01/03/2017
BJK
Notes:
1:GW Contours = 1"
2:Average GW gradient = 0.025 ft/ft
3:Average GW flow direction = NNW
(Feet)
075 75
GRAPHIC SCALE
LEGEND
Monitoring Well / Sample Location
Groundwater Elevation (MSL)
Groundawater Contour
Centerlane Innes Street, LLC Phase II Environmental Site Assessment (ESA)
January 6, 2017
Cardno
TABLES
Table 1A: VOC and SVOC Analytes Detected In Soil
Table 1B: PCB Congeners Detected In Soil
Table 1C: VOC and SVOC Analytes Detected In Groundwater
Table 2: Quality Control Precision Analysis

CAS VOC Analyte PSRG-Industrial Protection of GW Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL
67-64-1 Acetone 1.00E+05 2.4E+01 BRL 0.021 BRL 0.023 BRL 0.022 BRL 0.023 BRL 0.022 BRL 0.025 BRL 0.026 BRL 0.042 0.032 J 0.036
108-38-3/106-42-3m,p-Xylenes 3.88E+02 NA BRL 0.01 BRL 0.012 BRL 0.011 BRL 0.012 BRL 0.011 BRL 0.012 BRL 0.013 BRL 0.021 BRL 0.018591-78-6 Methyl Butyl Ketone (2-Hexanone)2.60E+02 1.7E-01 BRL 0.051 BRL 0.059 BRL 0.054 BRL 0.058 BRL 0.055 BRL 0.062 BRL 0.066 BRL 0.1 BRL 0.09178-93-3 Methyl Ethyl Ketone (2-Butanone)2.84E+04 1.6E+01 BRL 0.021 BRL 0.023 BRL 0.022 BRL 0.023 BRL 0.022 BRL 0.025 BRL 0.026 BRL 0.042 BRL 0.036108-10-1 Methyl Isobutyl Ketone 3.36E+03 4.3E-01 BRL 0.01 BRL 0.012 BRL 0.011 BRL 0.012 BRL 0.011 BRL 0.012 BRL 0.013 BRL 0.021 BRL 0.018
95-47-6 o-Xylene 4.34E+02 NA BRL 0.0051 BRL 0.0059 BRL 0.0054 BRL 0.0058 BRL 0.0055 BRL 0.0062 BRL 0.0066 BRL 0.01 BRL 0.0091
127-18-4 Tetrachloroethylene 7.80E+01 5.0E-03 BRL 0.01 BRL 0.012 BRL 0.011 BRL 0.012 BRL 0.011 BRL 0.012 BRL 0.013 BRL 0.021 BRL 0.018108-88-3 Toluene 8.18E+02 5.5E+00 BRL 0.0051 BRL 0.0059 BRL 0.0054 BRL 0.0058 BRL 0.0055 BRL 0.0062 BRL 0.0066 BRL 0.01 BRL 0.00911330-20-7 Xylenes, total 2.60E+02 6.1E+00 BRL 0.015 BRL 0.018 BRL 0.016 BRL 0.018 BRL 0.016 BRL 0.019 BRL 0.02 BRL 0.031 BRL 0.027
CAS SVOC Analyte PSRG-Industrial Protection of GW Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL
91-57-6 2-Methylnaphthalene 6.00E+02 1.6E+00 BRL 0.37 BRL 0.41 BRL 0.4 BRL 0.4 BRL 0.4 BRL 0.39 BRL 0.39 BRL 0.51 BRL 0.5
206-44-0 Fluoranthene 6.00E+03 3.3E+02 BRL 0.37 BRL 0.41 BRL 0.4 BRL 0.4 BRL 0.4 0.1 J 0.39 BRL 0.39 BRL 0.51 BRL 0.5
85-01-8 Phenanthrene 3.60E+02 3.8E+00 BRL 0.37 BRL 0.41 BRL 0.4 BRL 0.4 BRL 0.4 BRL 0.39 BRL 0.39 BRL 0.51 BRL 0.5
129-00-0 Pyrene 4.60E+03 2.2E+02 BRL 0.37 BRL 0.41 BRL 0.4 BRL 0.4 BRL 0.4 0.12 J 0.39 BRL 0.39 BRL 0.51 BRL 0.5
CAS VOC Analyte PSRG-
Industrial
Protection of
GW Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL
67-64-1 Acetone 1.00E+05 2.4E+01 BRL 0.028 BRL 0.023 0.19 0.02 0.073 0.023 BRL 0.023 BRL 0.022 BRL 0.026 BRL 0.01 BRL 0.01
108-38-3/106-42-3m,p-Xylenes 3.88E+02 NA BRL 0.014 BRL 0.011 0.0059 J 0.01 0.022 0.011 BRL 0.012 BRL 0.011 BRL 0.013 BRL 0.002 BRL 0.002
591-78-6 Methyl Butyl Ketone (2-Hexanone)2.60E+02 1.7E-01 BRL 0.07 BRL 0.057 BRL 0.05 0.0061 J 0.057 BRL 0.058 BRL 0.056 BRL 0.065 BRL 0.005 BRL 0.005
78-93-3 Methyl Ethyl Ketone (2-Butanone)2.84E+04 1.6E+01 BRL 0.028 BRL 0.023 0.031 0.02 0.018 J 0.023 BRL 0.023 BRL 0.022 BRL 0.026 BRL 0.005 BRL 0.005
108-10-1 Methyl Isobutyl Ketone 3.36E+03 4.3E-01 BRL 0.014 BRL 0.011 0.0062 J 0.01 0.0094 J 0.011 BRL 0.012 BRL 0.011 BRL 0.013 BRL 0.005 BRL 0.005
95-47-6 o-Xylene 4.34E+02 NA BRL 0.007 BRL 0.0057 0.0035 J 0.005 0.016 0.0057 BRL 0.0058 BRL 0.0056 BRL 0.0065 BRL 0.001 BRL 0.001
127-18-4 Tetrachloroethylene 7.80E+01 5.0E-03 BRL 0.014 BRL 0.011 0.0038 J 0.01 0.032 0.011 BRL 0.012 BRL 0.011 BRL 0.013 BRL 0.001 BRL 0.001
108-88-3 Toluene 8.18E+02 5.5E+00 BRL 0.007 BRL 0.0057 BRL 0.005 0.0063 0.0057 BRL 0.0058 BRL 0.0056 BRL 0.0065 BRL 0.001 BRL 0.001
1330-20-7 Xylenes, total 2.60E+02 6.1E+00 BRL 0.021 BRL 0.017 0.0095 J 0.015 0.038 0.017 BRL 0.017 BRL 0.017 BRL 0.02 BRL 0.003 BRL 0.003
CAS SVOC Analyte PSRG-
Industrial
Protection of
GW Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL Result RL
91-57-6 2-Methylnaphthalene 6.00E+02 1.6E+00 BRL 0.4 BRL 0.4 0.13 J 0.39 BRL 1.9 BRL 0.39 BRL 0.38 BRL 0.38 BRL 0.01 BRL 0.01206-44-0 Fluoranthene 6.00E+03 3.3E+02 BRL 0.4 BRL 0.4 BRL 0.39 BRL 1.9 BRL 0.39 BRL 0.38 BRL 0.38 BRL 0.01 BRL 0.01
85-01-8 Phenanthrene 3.60E+02 3.8E+00 BRL 0.4 BRL 0.4 BRL 0.39 0.71 J 1.9 BRL 0.39 BRL 0.38 BRL 0.38 BRL 0.01 BRL 0.01
129-00-0 Pyrene 4.60E+03 2.2E+02 BRL 0.4 BRL 0.4 BRL 0.39 BRL 1.9 BRL 0.39 BRL 0.38 BRL 0.38 BRL 0.01 BRL 0.01
BRL= Below Reporting Level J= Estimated Concentration RL=Laboratory Reporting Level
0 to 2’ bgs 0 to 2’ bgs 0 to 2’ bgs 0 to 2’ bgs
CIS-11-SS CIS-4-FB
equip blank field blank8-10' bgs 0 to 2’ bgs 8-10' bgs 4-6' bgsAll Values in mg/kg
CIS-07-SSCIS-05-SS
0 to 2’ bgs 8-10' bgs 0 to 2’ bgs
Nov. 15, 2016 Nov. 15, 2016 Nov. 15, 2016
Table 1A: Soil Samples
NCDEQ Reference Values CIS-10-SB
8-10' bgs 0 to 2’ bgs 8-10' bgs
CIS-07-SB
CIS-08-SB CIS-09-SS CIS-09-SB
CIS-01-SS CIS-02-SS CIS-03-SS CIS-03-SSD CIS-04-SS
Nov. 15, 2016 Nov. 15, 2016
0 to 2’ bgs
CIS-12-SB CIS-13-SB
CIS-06-SB
8-10' bgsNCDEQ Reference ValuesAll Values in mg/kg
CIS-3-EB
Nov. 15, 2016
Nov. 15, 2016 Nov. 15, 2016 Nov. 15, 2016 Nov. 15, 2016 Nov. 15, 2016 Nov. 15, 2016 Nov. 15, 2016 Nov. 15, 2016 Nov. 15, 2016
Nov. 14, 2016 Nov. 14, 2016 Nov. 15, 2016
date coll.
depth
Cas_num Congener*
NCDEQ
PSRG-
Industrial Lab_Result PQL Lab_Result PQL Lab_Result PQL Lab_Result PQL Lab_Result PQL Lab_Result PQL Lab_Result PQL Lab_Result PQL Lab_Result PQL
32598-14-4 2,3,3',4,4'-Pentachlorobiphenyl (105)490000 22.4 16.8 18 U 18 1.75 U 1.75 721 220 654 233 15.7 1.62 4.2 1.7 20.6 U 20.6 20.3 U 20.3
31508-00-6 2,3',4,4',5-Pentachlorobiphenyl (118)490000 60.9 16.8 22.1 18 1.75 U 1.75 1930 220 1150 233 44 1.62 9.13 1.7 20.6 U 20.6 20.3 U 20.3
38380-08-4 2,3,3',4,4',5-Hexachlorobiphenyl (156)500000 33.6 CU 33.6 36.1 CU 36.1 3.51 CU 3.51 554 C 441 465 CU 465 16.4 C 3.24 3.39 CU 3.39 41.3 CU 41.3 40.5 CU 40.5
2051-60-7 2-Chlorobiphenyl (1) 16.8 U 16.8 18 U 18 1.75 U 1.75 2010 220 6200 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
2051-61-8 3-Chlorobiphenyl (2) 16.8 U 16.8 18 U 18 1.75 U 1.75 237 220 345 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
2051-62-9 4-Chlorobiphenyl (3) 16.8 U 16.8 18 U 18 1.75 U 1.75 1580 220 1290 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
13029-08-8 2,2'-Dichlorobiphenyl (4) 16.8 U 16.8 18 U 18 1.75 U 1.75 769 220 4590 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
16605-91-7 2,3-Dichlorobiphenyl (5) 16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 278 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
25569-80-6 2,3'-Dichlorobiphenyl (6) 16.8 U 16.8 18 U 18 1.75 U 1.75 476 220 2420 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
33284-50-3 2,4-Dichlorobiphenyl (7) 16.8 U 16.8 18 U 18 1.75 U 1.75 229 220 1040 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
34883-43-7 2,4'-Dichlorobiphenyl (8) 16.8 U 16.8 18 U 18 1.75 U 1.75 1570 220 8060 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
34883-39-1 2,5-Dichlorobiphenyl (9) 16.8 U 16.8 18 U 18 1.75 U 1.75 239 220 1030 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
33146-45-1 2,6-Dichlorobiphenyl (10) 16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 544 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
2974-92-7 3,4-Dichlorobiphenyl (12) 33.6 CU 33.6 36.1 CU 36.1 3.51 CU 3.51 441 CU 441 1230 C 465 3.24 CU 3.24 3.39 CU 3.39 41.3 CU 41.3 40.5 CU 40.5
2050-68-2 4,4'-Dichlorobiphenyl (15) 16.8 U 16.8 18 U 18 1.75 U 1.75 1190 220 5840 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
38444-78-9 2,2',3-Trichlorobiphenyl (16) 16.8 U 16.8 18 U 18 1.75 U 1.75 490 220 2070 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
37680-66-3 2,2',4-Trichlorobiphenyl (17) 16.8 U 16.8 18 U 18 1.75 U 1.75 475 220 2190 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
37680-65-2 2,2',5-Trichlorobiphenyl (18) 33.6 CU 33.6 36.1 CU 36.1 3.51 CU 3.51 1020 C 441 4830 C 465 3.24 CU 3.24 3.39 CU 3.39 41.3 CU 41.3 40.5 CU 40.5
38444-73-4 2,2',6-Trichlorobiphenyl (19) 16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 575 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
38444-84-7 2,3,3'-Trichlorobiphenyl (20) 33.6 CU 33.6 36.1 CU 36.1 3.51 CU 3.51 1410 C 441 5210 C 465 4.63 C 3.24 3.39 CU 3.39 41.3 CU 41.3 40.5 CU 40.5
55702-46-0 2,3,4-Trichlorobiphenyl (21) 33.6 CU 33.6 36.1 CU 36.1 3.51 CU 3.51 681 C 441 2350 C 465 3.24 CU 3.24 3.39 CU 3.39 41.3 CU 41.3 40.5 CU 40.5
38444-85-8 2,3,4'-Trichlorobiphenyl (22) 16.8 U 16.8 18 U 18 1.75 U 1.75 485 220 1570 233 1.94 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
55712-37-3 2,3',4-Trichlorobiphenyl (25) 16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 390 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
38444-81-4 2,3',5-Trichlorobiphenyl (26) 33.6 CU 33.6 36.1 CU 36.1 3.51 CU 3.51 441 CU 441 923 C 465 3.24 CU 3.24 3.39 CU 3.39 41.3 CU 41.3 40.5 CU 40.5
38444-76-7 2,3',6-Trichlorobiphenyl (27) 16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 495 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
16606-02-3 2,4',5-Trichlorobiphenyl (31) 16.8 U 16.8 18 U 18 1.75 U 1.75 1030 220 3700 233 3.89 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
38444-77-8 2,4',6-Trichlorobiphenyl (32) 16.8 U 16.8 18 U 18 1.75 U 1.75 340 220 1260 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
38444-90-5 3,4,4'-Trichlorobiphenyl (37) 16.8 U 16.8 18 U 18 1.75 U 1.75 412 220 1580 233 1.81 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
38444-93-8 2,2',3,3'-Tetrachlorobiphenyl (40) 33.6 CU 33.6 36.1 CU 36.1 3.51 CU 3.51 441 CU 441 1420 C 465 3.24 CU 3.24 3.39 CU 3.39 41.3 CU 41.3 40.5 CU 40.5
52663-59-9 2,2',3,4-Tetrachlorobiphenyl (41) 16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 573 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
36559-22-5 2,2',3,4'-Tetrachlorobiphenyl (42) 16.8 U 16.8 18 U 18 1.75 U 1.75 277 220 759 233 1.64 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
41464-39-5 2,2',3,5'-Tetrachlorobiphenyl (44) 50.3 CU 50.3 54.1 CU 54.1 5.26 CU 5.26 996 C 661 2660 C 698 9.28 C 4.87 5.09 CU 5.09 61.9 CU 61.9 60.8 CU 60.8
70362-45-7 2,2',3,6-Tetrachlorobiphenyl (45) 33.6 CU 33.6 36.1 CU 36.1 3.51 CU 3.51 441 CU 441 903 C 465 3.24 CU 3.24 3.39 CU 3.39 41.3 CU 41.3 40.5 CU 40.5
41464-47-5 2,2',3,6'-Tetrachlorobiphenyl (46) 16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 356 233 1.62 U 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
41464-40-8 2,2',4,5'-Tetrachlorobiphenyl (49) 33.6 CU 33.6 36.1 CU 36.1 3.51 CU 3.51 584 C 441 1270 C 465 4.83 C 3.24 3.39 CU 3.39 41.3 CU 41.3 40.5 CU 40.5
62796-65-0 2,2',4,6-Tetrachlorobiphenyl (50) 33.6 CU 33.6 36.1 CU 36.1 3.51 CU 3.51 441 CU 441 615 C 465 3.24 CU 3.24 3.39 CU 3.39 41.3 CU 41.3 40.5 CU 40.5
35693-99-3 2,2',5,5'-Tetrachlorobiphenyl (52) 32.6 16.8 18 U 18 1.75 U 1.75 1230 220 3120 233 16.3 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
41464-43-1 2,3,3',4'-Tetrachlorobiphenyl (56) 16.8 U 16.8 18 U 18 1.75 U 1.75 534 220 1390 233 4.27 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
33025-41-1 2,3,4,4'-Tetrachlorobiphenyl (60) 16.8 U 16.8 18 U 18 1.75 U 1.75 291 220 756 233 2.42 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
33284-53-6 2,3,4,5-Tetrachlorobiphenyl (61) 67.1 CU 67.1 72.2 CU 72.2 7.01 CU 7.01 2040 C 881 4270 C 930 25.3 C 6.49 6.78 CU 6.78 82.5 CU 82.5 81.1 CU 81.1
52663-58-8 2,3,4',6-Tetrachlorobiphenyl (64) 16.8 U 16.8 18 U 18 1.75 U 1.75 541 220 1280 233 3.6 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
32598-10-0 2,3',4,4'-Tetrachlorobiphenyl (66) 17 16.8 18 U 18 1.75 U 1.75 858 220 2110 233 7.25 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
52663-62-4 2,2',3,3',4-Pentachlorobiphenyl (82) 16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 233 U 233 3.61 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
60145-20-2 2,2',3,3',5-Pentachlorobiphenyl (83) 16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 233 U 233 3.28 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
52663-60-2 2,2',3,3',6-Pentachlorobiphenyl (84) 16.8 U 16.8 18 U 18 1.75 U 1.75 343 220 419 233 8.22 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
65510-45-4 2,2',3,4,4'-Pentachlorobiphenyl (85) 50.3 CU 50.3 54.1 CU 54.1 5.26 CU 5.26 661 CU 661 698 CU 698 7.39 C 4.87 5.09 CU 5.09 61.9 CU 61.9 60.8 CU 60.8
55312-69-1 2,2',3,4,5-Pentachlorobiphenyl (86) 101 CU 101 108 CU 108 10.5 CU 10.5 1320 CU 1320 1400 CU 1400 29.4 C 9.73 10.2 CU 10.2 124 CU 124 122 CU 122
55215-17-3 2,2',3,4,6-Pentachlorobiphenyl (88) 33.6 CU 33.6 36.1 CU 36.1 3.51 CU 3.51 441 CU 441 465 CU 465 3.26 C 3.24 3.39 CU 3.39 41.3 CU 41.3 40.5 CU 40.5
68194-07-0 2,2',3,4',5-Pentachlorobiphenyl (90) 73.9 C 50.3 54.1 CU 54.1 5.26 CU 5.26 2850 C 661 1600 C 698 89.1 C 4.87 6.46 C 5.09 61.9 CU 61.9 60.8 CU 60.8
52663-61-3 2,2',3,5,5'-Pentachlorobiphenyl (92) 16.8 U 16.8 18 U 18 1.75 U 1.75 358 220 233 U 233 10.5 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
38379-99-6 2,2',3,5',6-Pentachlorobiphenyl (95) 42.4 16.8 18 U 18 1.75 U 1.75 1750 220 1450 233 50.8 1.62 2.53 1.7 20.6 U 20.6 20.3 U 20.3
38380-01-7 2,2',4,4',5-Pentachlorobiphenyl (99) 25.8 16.8 18 U 18 1.75 U 1.75 681 220 679 233 11.5 1.62 2.36 1.7 20.6 U 20.6 20.3 U 20.3
70424-68-9 2,3,3',4',5-Pentachlorobiphenyl (107) 16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 233 U 233 2 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
38380-03-9 2,3,3',4',6-Pentachlorobiphenyl (110) 73.6 C 33.6 36.1 CU 36.1 3.51 CU 3.51 2240 C 441 1540 C 465 61.1 C 3.24 9.6 C 3.39 41.3 CU 41.3 40.5 CU 40.5
38380-07-3 2,2',3,3',4,4'-Hexachlorobiphenyl (128) 33.6 CU 33.6 36.1 CU 36.1 3.51 CU 3.51 441 CU 441 465 CU 465 14.3 C 3.24 3.39 CU 3.39 41.3 CU 41.3 40.5 CU 40.5
55215-18-4 2,2',3,3',4,5-Hexachlorobiphenyl (129) 87.7 C 50.3 54.1 CU 54.1 37.2 C 5.26 6000 C 661 1640 C 698 205 C 4.87 16.5 C 5.09 61.9 CU 61.9 60.8 CU 60.8
52663-66-8 2,2',3,3',4,5'-Hexachlorobiphenyl (130)16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 233 U 233 6.28 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
0 to 2’ bgs 8-10' bgs8-10' bgs 8-10' bgs 8-10' bgs 8-10' bgs
Table 1B: Soil PCB Congeners All
values in pg/g (parts per trillion)
8-10' bgs
Nov. 15, 2016 Nov. 15, 2016 Nov. 15, 2016 Nov. 15, 2016 Nov. 15, 2016
C1S-12-SB C1S-3-EB C1S-4-FB
Nov. 15, 2016
C1S-6-SB C1S-7-SB C1S-8-SB C1S-9-SB C1S-10-SB C1S-11-SS
4-6' bgs
Nov. 15, 2016
N/A
Nov. 15, 2016 Nov. 15, 2016
date coll.
depth
Cas_num Congener*
NCDEQ
PSRG-
Industrial Lab_Result PQL Lab_Result PQL Lab_Result PQL Lab_Result PQL Lab_Result PQL Lab_Result PQL Lab_Result PQL Lab_Result PQL Lab_Result PQL
0 to 2’ bgs 8-10' bgs8-10' bgs 8-10' bgs 8-10' bgs 8-10' bgs
Table 1B: Soil PCB Congeners All
values in pg/g (parts per trillion)
8-10' bgs
Nov. 15, 2016 Nov. 15, 2016 Nov. 15, 2016 Nov. 15, 2016 Nov. 15, 2016
C1S-12-SB C1S-3-EB C1S-4-FB
Nov. 15, 2016
C1S-6-SB C1S-7-SB C1S-8-SB C1S-9-SB C1S-10-SB C1S-11-SS
4-6' bgs
Nov. 15, 2016
N/A
Nov. 15, 2016 Nov. 15, 2016
38380-05-1 2,2',3,3',4,6'-Hexachlorobiphenyl (132) 28 16.8 18 U 18 4.36 1.75 1610 220 435 233 63.1 1.62 4.87 1.7 20.6 U 20.6 20.3 U 20.3
35694-04-3 2,2',3,3',5,5'-Hexachlorobiphenyl (133) 16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 233 U 233 2.08 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
52704-70-8 2,2',3,3',5,6-Hexachlorobiphenyl (134) 16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 233 U 233 7.02 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
52744-13-5 2,2',3,3',5,6'-Hexachlorobiphenyl (135) 40.4 C 33.6 36.1 CU 36.1 11.4 C 3.51 2580 C 441 723 C 465 102 C 3.24 4.37 C 3.39 41.3 CU 41.3 40.5 CU 40.5
38411-22-2 2,2',3,3',6,6'-Hexachlorobiphenyl (136) 16.8 U 16.8 18 U 18 1.75 U 1.75 677 220 249 233 29.7 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
35694-06-5 2,2',3,4,4',5-Hexachlorobiphenyl (137) 16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 233 U 233 4.94 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
52712-04-6 2,2',3,4,5,5'-Hexachlorobiphenyl (141) 19.8 16.8 18 U 18 7.76 1.75 1560 220 233 U 233 61 1.62 3.34 1.7 20.6 U 20.6 20.3 U 20.3
68194-14-9 2,2',3,4,5',6-Hexachlorobiphenyl (144) 16.8 U 16.8 18 U 18 1.75 U 1.75 402 220 233 U 233 14.1 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
51908-16-8 2,2',3,4',5,5'-Hexachlorobiphenyl (146) 16.8 U 16.8 18 U 18 3.93 1.75 812 220 233 U 233 23.1 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
68194-13-8 2,2',3,4',5,6-Hexachlorobiphenyl (147) 79.4 C 33.6 36.1 CU 36.1 14.3 C 3.51 5090 C 441 1490 C 465 209 C 3.24 9.95 C 3.39 41.3 CU 41.3 40.5 CU 40.5
35065-27-1 2,2',4,4',5,5'-Hexachlorobiphenyl (153) 86.5 C 33.6 36.1 CU 36.1 21.6 C 3.51 6210 C 441 1470 C 465 221 C 3.24 12.8 C 3.39 41.3 CU 41.3 40.5 CU 40.5
38380-08-4 2,3,3',4,4',5-Hexachlorobiphenyl (156)33.6 CU 33.6 36.1 CU 36.1 3.51 CU 3.51 554 C 441 465 CU 465 16.4 C 3.24 3.39 CU 3.39 41.3 CU 41.3 40.5 CU 40.5
74472-42-7 2,3,3',4,4',6-Hexachlorobiphenyl (158) 16.8 U 16.8 18 U 18 2.76 1.75 515 220 233 U 233 18.4 1.62 1.82 1.7 20.6 U 20.6 20.3 U 20.3
74472-45-0 2,3,3',4',5',6-Hexachlorobiphenyl (164) 16.8 U 16.8 18 U 18 3.14 1.75 397 220 233 U 233 14.1 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
52663-72-6 2,3',4,4',5,5'-Hexachlorobiphenyl (167)16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 233 U 233 5.39 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
35065-30-6 2,2',3,3',4,4',5-Heptachlorobiphenyl (170) 22.9 16.8 18 U 18 22.4 1.75 3220 220 618 233 90.8 1.62 5.55 1.7 20.6 U 20.6 20.3 U 20.3
52663-71-5 2,2',3,3',4,4',6-Heptachlorobiphenyl (171) 33.6 CU 33.6 36.1 CU 36.1 7.11 C 3.51 930 C 441 465 CU 465 30.7 C 3.24 3.39 CU 3.39 41.3 CU 41.3 40.5 CU 40.5
52663-74-8 2,2',3,3',4,5,5'-Heptachlorobiphenyl (172) 16.8 U 16.8 18 U 18 3.87 1.75 569 220 233 U 233 17.3 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
38411-25-5 2,2',3,3',4,5,6'-Heptachlorobiphenyl (174) 39.5 16.8 18 U 18 25.9 1.75 3610 220 827 233 115 1.62 6.48 1.7 20.6 U 20.6 20.3 U 20.3
40186-70-7 2,2',3,3',4,5',6-Heptachlorobiphenyl (175) 16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 233 U 233 4.51 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
52663-65-7 2,2',3,3',4,6,6'-Heptachlorobiphenyl (176) 16.8 U 16.8 18 U 18 2.54 1.75 399 220 233 U 233 14.3 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
52663-70-4 2,2',3,3',4',5,6-Heptachlorobiphenyl (177) 18.9 16.8 18 U 18 13.8 1.75 1880 220 413 233 59.7 1.62 3.36 1.7 20.6 U 20.6 20.3 U 20.3
52663-67-9 2,2',3,3',5,5',6-Heptachlorobiphenyl (178) 16.8 U 16.8 18 U 18 4.97 1.75 724 220 233 U 233 22 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
52663-64-6 2,2',3,3',5,6,6'-Heptachlorobiphenyl (179) 20.4 16.8 18 U 18 10.7 1.75 1420 220 366 233 47 1.62 2.11 1.7 20.6 U 20.6 20.3 U 20.335065-29-3 2,2',3,4,4',5,5'-Heptachlorobiphenyl (180) 76 C 33.6 36.1 CU 36.1 56.9 C 3.51 9350 C 441 1880 C 465 252 C 3.24 14.1 C 3.39 41.3 CU 41.3 40.5 CU 40.5
52663-69-1 2,2',3,4,4',5',6-Heptachlorobiphenyl (183) 33.6 CU 33.6 36.1 CU 36.1 17.1 C 3.51 2750 C 441 590 C 465 83.9 C 3.24 4.55 C 3.39 41.3 CU 41.3 40.5 CU 40.5
52663-68-0 2,2',3,4',5,5',6-Heptachlorobiphenyl (187) 56.1 16.8 21 18 30.3 1.75 4970 220 1190 233 136 1.62 7.5 1.7 20.6 U 20.6 20.3 U 20.3
39635-31-9 2,3,3',4,4',5,5'-Heptachlorobiphenyl (189)16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 233 U 233 3.31 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
41411-64-7 2,3,3',4,4',5,6-Heptachlorobiphenyl (190) 16.8 U 16.8 18 U 18 5.09 1.75 672 220 233 U 233 20.3 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
74472-50-7 2,3,3',4,4',5',6-Heptachlorobiphenyl (191) 16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 233 U 233 3.74 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
35694-08-7 2,2',3,3',4,4',5,5'-Octachlorobiphenyl (194) 18.7 16.8 18 U 18 11.8 1.75 2840 220 631 233 50.1 1.62 2.99 1.7 20.6 U 20.6 20.3 U 20.3
52663-78-2 2,2',3,3',4,4',5,6-Octachlorobiphenyl (195) 16.8 U 16.8 18 U 18 5.2 1.75 1060 220 233 U 233 20.9 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
42740-50-1 2,2',3,3',4,4',5,6'-Octachlorobiphenyl (196) 16.8 U 16.8 18 U 18 6.27 1.75 1470 220 291 233 29.4 1.62 1.83 1.7 20.6 U 20.6 20.3 U 20.3
33091-17-7 2,2',3,3',4,4',6,6'-Octachlorobiphenyl (197) 33.6 CU 33.6 36.1 CU 36.1 3.51 CU 3.51 441 CU 441 465 CU 465 9.79 C 3.24 3.39 CU 3.39 41.3 CU 41.3 40.5 CU 40.5
68194-17-2 2,2',3,3',4,5,5',6-Octachlorobiphenyl (198) 33.6 CU 33.6 36.1 CU 36.1 12.7 C 3.51 3050 C 441 654 C 465 62.1 C 3.24 3.73 C 3.39 41.3 CU 41.3 40.5 CU 40.5
40186-71-8 2,2',3,3',4,5',6,6'-Octachlorobiphenyl (201) 16.8 U 16.8 18 U 18 1.75 U 1.75 300 220 233 U 233 7.49 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
2136-99-4 2,2',3,3',5,5',6,6'-Octachlorobiphenyl (202) 16.8 U 16.8 18 U 18 2.09 1.75 498 220 233 U 233 10.2 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
52663-76-0 2,2',3,4,4',5,5',6-Octachlorobiphenyl (203) 17.9 16.8 18 U 18 8.02 1.75 2120 220 470 233 37.7 1.62 2.25 1.7 20.6 U 20.6 20.3 U 20.3
74472-53-0 2,3,3',4,4',5,5',6-Octachlorobiphenyl (205) 16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 233 U 233 2.51 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
40186-72-9 2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl (206) 16.8 U 16.8 18 U 18 2.36 1.75 1060 220 402 233 13 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
52663-79-3 2,2',3,3',4,4',5,6,6'-Nonachlorobiphenyl (207) 16.8 U 16.8 18 U 18 1.75 U 1.75 220 U 220 233 U 233 1.97 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
52663-77-1 2,2',3,3',4,5,5',6,6'-Nonachlorobiphenyl (208) 16.8 U 16.8 18 U 18 1.75 U 1.75 227 220 233 U 233 2.78 1.62 1.7 U 1.7 20.6 U 20.6 20.3 U 20.3
1336-36-3 Total PCBs 961 16.8 43.1 18 356 1.75 102000 220 103000 233 2590 1.62 142 1.7 20.6 U 20.6 20.3 U 20.3
TOTAL NUMBER OF CONGENERS IN SAMPLE 22 2 28 69 64 73 24 0 0
* Number in ( ) refers to Ballschmiter PCB Congener Number System U- Not detected in sample above PQL PQL= Laboratory Practical Quantitation LevelC- Congener co-elutes with other congeners CU= Congener co-elutes but not detected in sample
0.00003
Dioxin TEQ**0.0288 0.00129 0.0107 3.06 3.09 0.0777 0.0043
Congeners in BOLD have assigned Toxic Equivalecy Factors (TEF) of
**assumes all congeners are equally toxic as those with assigned TEFs
H2O level
Coll. Date
CAS Analyte
'15A NCAC
02L .0202
GW Vapor
Intrusion Result RL Result RL Result RL Result RL Result RL
67-66-3 Chloroform 70 8.14 0.53 J 1.0 0.53 J 1.0 BRL 1.0 BRL 1.0 BRL 1.0
127-18-4 Tetrachloroethylene 0.7 11.5 590 Aa 1.0 520 10 49 1.0 3.8 1.0 3.3 1.0
75-69-4 Trichlorofluoromethane 2000 36.8 1.4 J 2.0 1.4 J 2.0 BRL 2.0 BRL 2.0 BRL 2.0
BRL= Below Reporting Level RL=Laboratory Reporting Level Aa:= Concentration confirmed outside of Hold Time.
CIS-4-NCW CIS-4-MWDAll Values in µg/l NCDEQ Reference Values CIS-1-MWCIS-2-MW CIS-3-MW
736.772 msl
Nov.16, 2016
Upgradient Well
742.419 msl
Nov. 16, 2016
741.797 msl
Nov.16, 2016
741.518 msl
Nov.16, 2016 Table 1C: Groundwater Samples
Table 2: QC Precision Analysis
Parameter RL result/rl RL result/rl
Chloroform 0.53 J 1.0 0.53 0.53 J 1.0 0.53 Absolute Difference =0 Acceptable
Tetrachloroethylene 590 1.0 590 520 10 52 RPD method 12.73%RPD Acceptable
Trichlorofluoromethane 1.4 J 2.0 0.7 1.4 J 2.0 0.7 Absolute Difference =0 Acceptable
Basis for evaluation
 if the duplicate or sample result is less than five (5) times the reporting limit then the comparison is made by the absolute difference between the results (Sample - Duplicate).
– For soil samples, if the difference is less than twice the magnitude of the (higher) reporting limit, precision is considered “acceptable.”
 If these differences are within two (2) times the “acceptable” limits, they are considered “slightly high” (anything beyond that would be considered “high”).
 If both sample and duplicate results are greater than five (5) times the reporting limit (the higher of the two RLs, if they are not the same), then precision is assessed by the %RPD
– %RPD (difference in results divided by the average of the two results X 100)
 <35% RPD = “good/acceptable”, >35% but < 50% = variability is “slightly high”, >50% = “high”.
CIS-4-NCW CIS-4-MWD
Centerlane Innes Street, LLC Phase II Environmental Site Assessment (ESA)
January 6, 2017
Cardno
APPENDIX A: Ground Penetrating Radar Investigation

Cardno, Inc.

FINAL REPORT GROUND PENETRATING RADAR
SUBSURFACE INVESTIGATION
Centerlane Innes St Salisbury, NC
Prepared for:

Cardno, Inc. Attn: Craig Dukes Senior Staff Scientist
1812 Lincoln Street, Suite 301
Columbia, SC 29201
Prepared by:

Cardno, Inc.
9800 Southern Pine Boulevard, Suite I Charlotte, NC 28273
December 22nd, 2016

Cardno, Inc.

TABLE OF CONTENTS

Section Title Page
1.0 INTRODUCTION. ………………………………………………… 1
1.1 Scope of Work………………………………………………. 1

2.0 METHODOLOGY………………………………………………….. 2 2.1 GPR Equipment and Principles of Operation……....…….…. 2 2.2 GPR Investigation Procedures…………………………….… 3
2.3 Qualifications of Field Staff………………………………… 4

3.0 RESULTS AND INTERPRETATIONS…………………….……… 5 4.0 RECOMMENDATIONS…………………………………………… 5

5.0 REFERENCES……………………………………………………... 5

Cardno, Inc.
1
1.0 INTRODUCTION

Cardno, Inc. employed ground penetrating radar, GPR, a non-invasive geophysical investigation technique, to study the subsurface beneath the property located at 1517 E Innes St, Salisbury, NC. GPR
was one of the methods utilized to clear environmental soil sampling locations. During the
course of clearing one of the soil sampling locations, an anomaly was found that Cardno suspects
to be an underground storage tank.

1.1 Scope of Work

Cardno’s scope of work consisted of:

• Mobilizing to site and establishing the process for GPR data collection
throughout the site;

• Collecting GPR data in the area identified and performing on-site interpretation
of the resulting data;

• Communicating findings to Cardno’s representatives;

• Demobilizing from site;

• Preparing a final report summarizing results of GPR investigation.

2.0 METHODOLOGY

2.1 GPR Equipment and Principles of Operation
Cardno, Inc.
2

Ground penetrating radar is a wave-based electromagnetic geophysical method that detects
interfaces between subsurface materials possessing varying electrical (dielectric) characteristics.
The GPR system consists of transmitting and receiving antenna elements; a central control unit
which produces the transmitted electromagnetic (EM) signal, processes the received signal by
amplifying and recording the incoming signal and converting it to a digital format; and a field-
ruggedized color laptop video display unit that receives the digital information from the control
unit and produces a graphical representation of the acquired data as a real-time two-dimensional
continuous depth profile that includes horizontal antenna position and vertical target depth
information.

GPR operates by emitting electromagnetic radar impulses into a media (ground) at a high
repetition rate, from an antenna array moving along the ground surface. Subsurface reflections
occur at interfaces of materials with differing electrical characteristics (dielectric permittivities).
Reflections of various amplitudes, depending on the incoming signal frequency, the difference in
dielectric constants of the two materials and the conductivity/resistivity of the soil, are produced
at the interface and detected by the receiving antenna element. Common subsurface reflectors
are 1) natural conditions such as soil composition or horizons, geologic bedding or foliation, void
space, or water saturation level (freshwater and saltwater); or 2) anthropomorphic conditions
such as gravesites, disturbed soil, soil backfilled areas, buried pipelines, utilities or tanks, and
other buried debris.

GPR data can be analyzed qualitatively at the time of data collection, as data is recorded and
displayed in real-time, and/or it can be digitally filtered and downloaded and analyzed as a
continuous profile hard copy in the field or office. The data reflected in the output files are a
slice profile of the subsurface directly beneath the antenna that is moved along the ground. To
acquire the best information during a GPR investigation, data is acquired along transects of a
predetermined survey grid. In this way, specific locations can be reestablished and a virtual
subsurface model of a project site can be created.

Cardno, Inc.
3
The primary limiting factor of a GPR study is the maximum attainable depth of investigation.
The phenomenon of signal attenuation (absorption) of subsurface materials is the most pervasive
factor affecting the depths to which electromagnetic (EM) radar energy will penetrate. Signal
attenuation is dependent on the electrical conductivity/resistivity of the subsurface materials.
Highly conductive/low resistive materials, such as clays and saline water, possess the highest
attenuation characteristics and are not conducive to significant radar energy penetration. Signal
attenuation is minimal in low conductive/highly resistive materials, such as dry quartz sand,
bedrock and ice.

Also affecting the depth of investigation is the frequency of the transmitting antenna. Generally,
the depth of investigation increases with a decrease in transmitting frequency. However,
consequently, the resolution of subsurface reflectors is reduced with a decrease in transmitting
frequency. Following this line of reasoning, as depth increases the minimum size necessary for a
feature to be detected must also increase. Other environmental factors that may affect the
propagation of GPR energy into the ground are the groundwater table or presence of water in the
soil pores, and some compositions of concrete or asphalt.

2.2 GPR Investigation Procedures

The GPR field investigation took place on November 14, 2016. A GSSI Utility Scan LT GPR
system, configured with a 500 MHz antenna array and a 45-nanosecond time range, was utilized
to collect radar data for this investigation.

2.3 Qualifications of Field Staff

The GPR field investigation was performed by SUE Supervisor Prasit Frazee. Mr. Frazee has
over 16 years of field experience in subsurface utility engineering. Much of this experience
includes full mapping of multiple underground utilities using a suite of surface geophysical
method tools including pipe and cable locators and ground penetrating radar. Mr. Frazee has
Cardno, Inc.
4
experience with investigating the presence of underground storage tanks in various parts of the
southeast.

Relative Project Experience:
Under the direction of Cardno’s Engineering & Environmental Services Division, Mr. Frazee
performed GPR investigation services for a suspected underground storage tank site located in
Salisbury, NC. The investigation was performed in medium-light density clay soils and resulted
in data that was used to determine the approximate presence of a suspected underground storage
tank. The horizontal position of the designated UST was then surveyed and reduced onto survey
drawings to be used for redevelopment of site. Because of the investigation the developer,
engineer and construction contractor can take appropriate actions when constructing around the
suspected underground storage tank.

On another project for Cardno’s Engineering & Environmental Services Division, Mr. Frazee
performed GPR investigations at a former gas station in Aberdeen, NC. Eight suspected USTs
were found. After the horizontal locations of these USTs were designated, steps were taken to
begin the environmental remediation process at this site.

ATC Assoicates contracted out Cardno to perform GPR investigation services for a suspected
underground storage tank site located in Wilmington, NC. Mr. Frazee was able to determine the
location of two large underground storage tanks. ATC was able to safely perform mitigation
services that required exposing the tanks, draining and filling the tanks with approved
construction materials.

3.0 RESULTS AND INTERPRETATIONS

Upon investigation, a large anomaly was found approximately 2 feet in depth, 5 feet in width and
10 feet in length at the south of the property near the building. The anomaly was consistent in
width and depth and based on previous experience with similar sites searching for USTs, Mr.
Frazee concluded that the anomaly is likely to be an underground storage tank.

Cardno, Inc.
5
4.0 RECOMMENDATIONS

As no data collected from the surface can absolutely predict the conditions in the subsurface, it is
recommended that additional care be exercised during work in this area.

5.0 REFERENCES

RAMAC/GPR Software Manual Version 2.28, Malå GeoScience, Inc., August 1997.

Ground-Penetrating Radar: An Introduction for Archaeologists. Conyers, Lawrence B. and
Goodman, Dean. Altimira Press, 1997.

ATTACHMENT A

The interpretations, conclusions and recommendations presented herein are based on inferences
from subsurface radar data collected during the site investigation. The ground penetrating radar
assessment of this site is based on our professional evaluation of the acquired geophysical data.
This report was prepared in accordance with general scientific practice and meets the standards
of care of our profession. However, while due care was exercised in the acquisition and
interpretation of GPR measurements, Cardno, Inc. can offer no warranties or guarantees with
respect to existing subsurface conditions.
Cardno, Inc.
6

Cardno, Inc.
7

Cardno, Inc.
8

Centerlane Innes Street, LLC Phase II Environmental Site Assessment (ESA)
January 6, 2017
Cardno
Appendix B: Analytical Reports w/Chains-of-Custody

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December 20, 2016

Mr. Ashley Amick
Access Analytical, Inc.
7478 Carlisle Street
Irmo, South Carolina 29063

Re: Lab Subcontract
Work Order: 10122
SDG: 6110379

Dear Mr. Amick:
Cape Fear Analytical, LLC (CFA) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received
on November 19, 2016. This revised data report has been prepared and reviewed in accordance with CFA’s standard operating procedures.
Refer to the fractional case narrative for revision details.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time.
We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (910)
795-0421.

Sincerely,
Cynde Larkins
Project Manager

Enclosures

Page 1 of 149
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Subject: RE: CFA AAIS 10122 (6110379)
From: Angela MarƟn <amarƟn@axs‐inc.com>
Date: 12/20/2016 3:13 PM
To: Cynde Larkins <cynde.larkins@cfanalyƟcal.com>, Ashley Amick <aamick@axs‐inc.com>
CC: "melissa.odorisio@cfanalyƟcal.com" <melissa.odorisio@cfanalyƟcal.com>
Cynde,
Would you please have the client Laboratory ID added to this workorder? Thanks
Angela Martin
Project Manager

Access Analytical, Inc.
Comprehensive Environmental Laboratory Services
7478 Carlisle St.
Irmo, SC 29063
Main Office:         803‐781‐4243
This e‐mail and any attachments contain confidential information that may be proprietary or 
privileged. If you receive this message in error or are not the intended recipient, you should 
not retain, distribute, disclose or use any of this information and you should destroy the 
e‐mail and any attachments or copies.
‐‐‐‐‐Original Message‐‐‐‐‐
From: Cynde Larkins [mailto:[e-mail]] 
Sent: Wednesday, December 14, 2016 2:58 PM
To: Angela Martin <amartin@axs‐inc.com>; Ashley Amick <aamick@axs‐inc.com>
Cc: [e-mail]; [e-mail]
Subject: CFA AAIS 10122 (6110379)
Please find the mini package and EDD results for 6110379 attached.  The CD with raw data will 
arrive tomorrow.  Let me know if there are any questions or if anything else is needed.
Thanks, 
Cynde Larkins
CONFIDENTIALITY NOTICE: This e‐mail and any files transmitted with it are the property of The 
GEL Group, Inc. and its affiliates. All rights, including without limitation copyright, are 
reserved. The proprietary information contained in this e‐mail message, and any files 
transmitted with it, is intended for the use of the recipient(s) named above. If the reader of 
this e‐mail is not the intended recipient, you are hereby notified that you have received this 
e‐mail in error and that any review, distribution or copying of this e‐mail or any files 
transmitted with it is strictly prohibited. If you have received this e‐mail in error, please 
notify the sender immediately and delete the original message and any files transmitted. The 
unauthorized use of this e‐mail or any files transmitted with it is prohibited and disclaimed by 
The GEL Group, Inc. and its affiliates.
RE: CFA AAIS 10122 (6110379)
1 of 1 12/20/2016 3:18 PMPage 5 of 149
PCB Congeners
Analysis
Page 6 of 149
Case Narrative
Page 7 of 149
PCBC Case Narrative
Access Analytical, Inc. (AAIS)
SDG 6110379
Work Order 10122
Revision Information
Sample IDs have been amended in this revised report per client request.

Method/Analysis Information

Product: PCB Congeners by EPA Method 1668A
Analytical Method: EPA Method 1668A
Extraction Method: SW846 3540C, 3520C
Analytical Batch Number: 33410, 33438, 33485
Clean Up Batch Number: 33433, 33409, 33475
Extraction Batch Number: 33408, 33432, 33474
Sample Analysis
The following samples were analyzed using the analytical protocol as established in EPA
Method 1668A:
Sample ID Client ID
10122001 6110379-07 CIS-6-SB
10122002 6110379-09 CIS-7-SB
10122003 6110379-10 CIS-8-SB
10122004 6110379-12 CIS-9-SB
10122005 6110379-13 CIS-10-SB
10122006 6110379-14 CIS-11-SB
10122007 6110379-15 CIS-12-SB
10122008 6110379-17 CIS-3-EB
10122009 6110379-18 CIS-4-FB
12017426 Method Blank (MB)
12017427 Laboratory Control Sample (LCS)
12017428 Laboratory Control Sample Duplicate (LCSD)
12017429 10122001(6110379-07) Matrix Spike (MS)
12017430 10122001(6110379-07) Matrix Spike Duplicate (MSD)
12017453 Method Blank (MB)
12017454 Laboratory Control Sample (LCS)
12017455 Laboratory Control Sample Duplicate (LCSD)
12017481 Method Blank (MB)
12017482 Laboratory Control Sample (LCS)
12017483 Laboratory Control Sample Duplicate (LCSD)
Page 8 of 149
Samples 10122 001, 002, 003, 004, 005, 006 and 007 in this SDG were analyzed on a "dry
weight" basis. Samples 10122 008 and 009 in this SDG were analyzed on an "as received" basis.
SOP Reference
Procedure for preparation, analysis and reporting of analytical data are controlled by Cape Fear
Analytical LLC (CFA) as Standard Operating Procedure (SOP). The data discussed in this
narrative has been analyzed in accordance with CF-OA-E-003 REV# 6.
Raw data reports are processed and reviewed by the analyst using the TargetLynx software
package.
Calibration Information

Initial Calibration
All initial calibration requirements have been met for this sample delivery group (SDG).

Continuing Calibration Verification (CCV) Requirements
All associated calibration verification standard(s) (ICV or CCV) met the acceptance criteria.
Quality Control (QC) Information

Certification Statement
The test results presented in this document are certified to meet all requirements of the 2009 TNI
Standard.

Method Blank (MB) Statement
The MB(s) analyzed with this SDG met the acceptance criteria.

Surrogate Recoveries
Three surrogates recovered outside the acceptance limits. 12017481 (MB), 12017482 (LCS) and
12017483 (LCSD)- Batch 33485.

Laboratory Control Sample (LCS) Recovery
The LCS spike recoveries met the acceptance limits.

Laboratory Control Sample Duplicate (LCSD) Recovery
The LCSD spike recoveries met the acceptance limits.

LCS/LCSD Relative Percent Difference (RPD) Statement
The RPD(s) between the LCS and LCSD met the acceptance limits.

QC Sample Designation
Sample 10122001 (6110379-07 CIS-6-SB)- Batch 33410 was selected for analysis as the matrix
spike and matrix spike duplicate.

Page 9 of 149

Matrix Spike (MS) Recovery Statement
The MS recoveries were within the established acceptance limits.

Matrix Spike Duplicate (MSD) Recovery Statement
The MSD recoveries were within the established acceptance limits.

MS/MSD Relative Percent Difference (RPD) Statement
The RPD(s) between the MS and MSD met the acceptance limits.

Technical Information

Holding Time Specifications
CFA assigns holding times based on the associated methodology, which assigns the date and
time from sample collection. Those holding times expressed in hours are calculated in the
AlphaLIMS system. Those holding times expressed as days expire at midnight on the day of
expiration. All samples in this SDG met the specified holding time.

Preparation/Analytical Method Verification
All procedures were performed as stated in the SOP.

Sample Dilutions
Samples 10122001 (6110379-07 CIS-6-SB), 10122002 (6110379-09 CIS-7-SB), 12017429 MS
(6110379-07 CIS-7-SB), 12017430 MSD (6110379-07 CIS-7-SB)- Batch 33410, 10122004
(6110379-12 CIS-9-SB) and 10122005 (6110379-13 CIS-10-SB)- Batch 33485 were diluted due to
the presence of non-target interferences.

Sample Re-extraction/Re-analysis
The samples were re-extracted using a 1g aliquot due to matrix interferences. 10122004
(6110379-12 CIS-9-SB) and 10122005 (6110379-13 CIS-10-SB)- Batch 33485.
Miscellaneous Information

Nonconformance (NCR) Documentation
A NCR was not required for this SDG.

Manual Integrations
Manual integrations were required for data files in this SDG. Certain standards and QC samples
required manual integrations to correctly position the baseline as set in the calibration standard
injections. Where manual integrations were performed, copies of all manual integration peak
profiles are included in the raw data section of this fraction.

Page 10 of 149
System Configuration
This analysis was performed on the following instrument configuration:

Instrument ID Instrument System Configuration Column ID Column Description
HRP791_1 PCB Analysis PCB Analysis SPB-Octyl 30m x 0.25mm, 0.25um
HRP875_1 PCB Analysis PCB Analysis SPB-Octyl 30m x 0.25mm, 0.25um
Electronic Packaging Comment
This data package was generated using an electronic data processing program referred to as
virtual packaging. In an effort to increase quality and efficiency, the laboratory has developed
systems to generate all data packages electronically. The following change from traditional
packages should be noted: Analyst/peer reviewer initials and dates are not present on the
electronic data files. Presently, all initials and dates are present on the original raw data. These
hard copies are temporarily stored in the laboratory. An electronic signature page inserted after
the case narrative will include the data validator's signature and title. The signature page also
includes the data qualifiers used in the fractional package. Data that are not generated
electronically, such as hand written pages, will be scanned and inserted into the electronic
package.
Page 11 of 149
Sample Data Summary
Page 12 of 149
Cape Fear Analytical, LLC
3306 Kitty Hawk Road Suite 120, Wilmington, NC 28405 - [phone] - www.capefearanalytical.com
Certificate of Analysis Report
AAIS001 Access Analytical, Inc.
Client SDG: 6110379 CFA Work Order: 10122
Cape Fear Analytical requires all analytical data to be verified by a qualified data reviewer.
The following data validator verified the information presented in this case narrative:
The Qualifiers in this report are defined as follows:
* A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a surrogate compound
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
J Value is estimated
K Estimated Maximum Possible Concentration
U Analyte was analyzed for, but not detected above the specified detection limit.
for
Signature:Name:
Date:Title:22 DEC 2016
Mike Larkins
Technical Director
Review/Validation
Page 13 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 1 of 8
SDG Number:6110379
Lab Sample ID:10122001 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 15.5
Date Collected:11/15/2016 16:00
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
168
33.6
16.8
16.8
16.8
16.8
33.6
16.8
33.6
33.6
16.8
16.8
16.8
16.8
33.6
16.8
16.8
16.8
U
U
U
U
U
U
U
U
U
U
U
CU
C12
U
U
U
U
CU
U
CU
CU
U
U
U
U
CU
U
C20
C26
C18
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 06:41 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-07 CIS-6-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.1 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_2-8Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
2-MoCB
3-MoCB
4-DiCB
5-DiCB
6-DiCB
7-DiCB
8-DiCB
9-DiCB
10-DiCB
11-DiCB
12-DiCB
13-DiCB
14-DiCB
15-DiCB
16-TrCB
17-TrCB
18-TrCB
19-TrCB
20-TrCB
21-TrCB
22-TrCB
23-TrCB
24-TrCB
25-TrCB
26-TrCB
27-TrCB
28-TrCB
29-TrCB
30-TrCB
31-TrCB
32-TrCB
2051-60-7
2051-61-8
2051-62-9
13029-08-8
16605-91-7
25569-80-6
33284-50-3
34883-43-7
34883-39-1
33146-45-1
2050-67-1
2974-92-7
2974-90-5
34883-41-5
2050-68-2
38444-78-9
37680-66-3
37680-65-2
38444-73-4
38444-84-7
55702-46-0
38444-85-8
55720-44-0
55702-45-9
55712-37-3
38444-81-4
38444-76-7
7012-37-5
15862-07-4
35693-92-6
16606-02-3
38444-77-8
Client Sample:
PQL
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
168
33.6
16.8
16.8
16.8
16.8
33.6
16.8
33.6
33.6
16.8
16.8
16.8
16.8
33.6
16.8
16.8
16.8
Page 14 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 2 of 8
SDG Number:6110379
Lab Sample ID:10122001 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 15.5
Date Collected:11/15/2016 16:00
16.8
16.8
16.8
16.8
16.8
16.8
33.6
16.8
16.8
16.8
50.3
33.6
16.8
16.8
33.6
33.6
32.6
16.8
16.8
16.8
16.8
16.8
50.3
16.8
67.1
16.8
16.8
C21
U
U
U
U
U
U
CU
U
U
U
CU
CU
U
C44
U
CU
CU
C45
C50
U
U
U
U
U
CU
U
CU
C59
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 06:41 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-07 CIS-6-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.1 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_2-8Data File:
Prep SOP Ref: CF-OA-E-001
33-TrCB
34-TrCB
35-TrCB
36-TrCB
37-TrCB
38-TrCB
39-TrCB
40-TeCB
41-TeCB
42-TeCB
43-TeCB
44-TeCB
45-TeCB
46-TeCB
47-TeCB
48-TeCB
49-TeCB
50-TeCB
51-TeCB
52-TeCB
53-TeCB
54-TeCB
55-TeCB
56-TeCB
57-TeCB
58-TeCB
59-TeCB
60-TeCB
61-TeCB
62-TeCB
63-TeCB
64-TeCB
38444-86-9
37680-68-5
37680-69-6
38444-87-0
38444-90-5
53555-66-1
38444-88-1
38444-93-8
52663-59-9
36559-22-5
70362-46-8
41464-39-5
70362-45-7
41464-47-5
2437-79-8
70362-47-9
41464-40-8
62796-65-0
68194-04-7
35693-99-3
41464-41-9
15968-05-5
74338-24-2
41464-43-1
70424-67-8
41464-49-7
74472-33-6
33025-41-1
33284-53-6
54230-22-7
74472-34-7
52663-58-8
Client Sample:
PQL
16.8
16.8
16.8
16.8
16.8
16.8
33.6
16.8
16.8
16.8
50.3
33.6
16.8
16.8
33.6
33.6
16.8
16.8
16.8
16.8
16.8
16.8
50.3
16.8
67.1
16.8
16.8
Page 15 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 3 of 8
SDG Number:6110379
Lab Sample ID:10122001 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 15.5
Date Collected:11/15/2016 16:00
17.0
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
50.3
101
33.6
16.8
73.9
16.8
33.6
16.8
42.4
16.8
C44
U
U
C49
C61
C40
U
U
C61
C59
C61
U
U
U
U
U
U
U
U
CU
CU
C86
CU
U
C
C88
U
CU
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 06:41 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-07 CIS-6-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.1 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_2-8Data File:
Prep SOP Ref: CF-OA-E-001
65-TeCB
66-TeCB
67-TeCB
68-TeCB
69-TeCB
70-TeCB
71-TeCB
72-TeCB
73-TeCB
74-TeCB
75-TeCB
76-TeCB
77-TeCB
78-TeCB
79-TeCB
80-TeCB
81-TeCB
82-PeCB
83-PeCB
84-PeCB
85-PeCB
86-PeCB
87-PeCB
88-PeCB
89-PeCB
90-PeCB
91-PeCB
92-PeCB
93-PeCB
94-PeCB
95-PeCB
96-PeCB
33284-54-7
32598-10-0
73575-53-8
73575-52-7
60233-24-1
32598-11-1
41464-46-4
41464-42-0
74338-23-1
32690-93-0
32598-12-2
70362-48-0
32598-13-3
70362-49-1
41464-48-6
33284-52-5
70362-50-4
52663-62-4
60145-20-2
52663-60-2
65510-45-4
55312-69-1
38380-02-8
55215-17-3
73575-57-2
68194-07-0
68194-05-8
52663-61-3
73575-56-1
73575-55-0
38379-99-6
73575-54-9
Client Sample:
PQL
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
50.3
101
33.6
16.8
50.3
16.8
33.6
16.8
16.8
16.8
Page 16 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 4 of 8
SDG Number:6110379
Lab Sample ID:10122001 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 15.5
Date Collected:11/15/2016 16:00
33.6
25.8
16.8
16.8
22.4
16.8
16.8
33.6
73.6
16.8
16.8
16.8
60.9
16.8
16.8
16.8
16.8
16.8
16.8
33.6
C86
CU
C93
C90
C98
U
U
U
U
CU
C86
C
U
U
C90
U
C110
C85
C85
C86
U
U
U
U
C108
C86
U
U
CU
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 06:41 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-07 CIS-6-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.1 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_2-8Data File:
Prep SOP Ref: CF-OA-E-001
97-PeCB
98-PeCB
99-PeCB
100-PeCB
101-PeCB
102-PeCB
103-PeCB
104-PeCB
105-PeCB
106-PeCB
107-PeCB
108-PeCB
109-PeCB
110-PeCB
111-PeCB
112-PeCB
113-PeCB
114-PeCB
115-PeCB
116-PeCB
117-PeCB
118-PeCB
119-PeCB
120-PeCB
121-PeCB
122-PeCB
123-PeCB
124-PeCB
125-PeCB
126-PeCB
127-PeCB
128-HxCB
41464-51-1
60233-25-2
38380-01-7
39485-83-1
37680-73-2
68194-06-9
60145-21-3
56558-16-8
32598-14-4
70424-69-0
70424-68-9
70362-41-3
74472-35-8
38380-03-9
39635-32-0
74472-36-9
68194-10-5
74472-37-0
74472-38-1
18259-05-7
68194-11-6
31508-00-6
56558-17-9
68194-12-7
56558-18-0
76842-07-4
65510-44-3
70424-70-3
74472-39-2
57465-28-8
39635-33-1
38380-07-3
Client Sample:
PQL
33.6
16.8
16.8
16.8
16.8
16.8
16.8
33.6
33.6
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
33.6
Page 17 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 5 of 8
SDG Number:6110379
Lab Sample ID:10122001 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 15.5
Date Collected:11/15/2016 16:00
87.7
16.8
16.8
28.0
16.8
16.8
40.4
16.8
16.8
33.6
19.8
16.8
16.8
16.8
16.8
16.8
79.4
16.8
16.8
16.8
86.5
16.8
16.8
33.6
16.8
16.8
16.8
C
U
U
U
U
C
U
U
C129
CU
C139
U
U
U
U
U
C
U
C147
U
C135
U
C
U
U
CU
C156
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 06:41 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-07 CIS-6-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.1 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_2-8Data File:
Prep SOP Ref: CF-OA-E-001
129-HxCB
130-HxCB
131-HxCB
132-HxCB
133-HxCB
134-HxCB
135-HxCB
136-HxCB
137-HxCB
138-HxCB
139-HxCB
140-HxCB
141-HxCB
142-HxCB
143-HxCB
144-HxCB
145-HxCB
146-HxCB
147-HxCB
148-HxCB
149-HxCB
150-HxCB
151-HxCB
152-HxCB
153-HxCB
154-HxCB
155-HxCB
156-HxCB
157-HxCB
158-HxCB
159-HxCB
160-HxCB
55215-18-4
52663-66-8
61798-70-7
38380-05-1
35694-04-3
52704-70-8
52744-13-5
38411-22-2
35694-06-5
35065-28-2
56030-56-9
59291-64-4
52712-04-6
41411-61-4
68194-15-0
68194-14-9
74472-40-5
51908-16-8
68194-13-8
74472-41-6
38380-04-0
68194-08-1
52663-63-5
68194-09-2
35065-27-1
60145-22-4
33979-03-2
38380-08-4
69782-90-7
74472-42-7
39635-35-3
41411-62-5
Client Sample:
PQL
50.3
16.8
16.8
16.8
16.8
16.8
33.6
16.8
16.8
33.6
16.8
16.8
16.8
16.8
16.8
16.8
33.6
16.8
16.8
16.8
33.6
16.8
16.8
33.6
16.8
16.8
16.8
Page 18 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 6 of 8
SDG Number:6110379
Lab Sample ID:10122001 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 15.5
Date Collected:11/15/2016 16:00
16.8
16.8
16.8
16.8
16.8
16.8
22.9
33.6
16.8
39.5
16.8
16.8
18.9
16.8
20.4
76.0
16.8
16.8
33.6
16.8
16.8
56.1
16.8
16.8
16.8
16.8
16.8
U
U
C129
U
U
C128
U
C153
U
CU
U
C171
U
U
U
C
U
U
CU
U
C183
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 06:41 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-07 CIS-6-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.1 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_2-8Data File:
Prep SOP Ref: CF-OA-E-001
161-HxCB
162-HxCB
163-HxCB
164-HxCB
165-HxCB
166-HxCB
167-HxCB
168-HxCB
169-HxCB
170-HpCB
171-HpCB
172-HpCB
173-HpCB
174-HpCB
175-HpCB
176-HpCB
177-HpCB
178-HpCB
179-HpCB
180-HpCB
181-HpCB
182-HpCB
183-HpCB
184-HpCB
185-HpCB
186-HpCB
187-HpCB
188-HpCB
189-HpCB
190-HpCB
191-HpCB
192-HpCB
74472-43-8
39635-34-2
74472-44-9
74472-45-0
74472-46-1
41411-63-6
52663-72-6
59291-65-5
32774-16-6
35065-30-6
52663-71-5
52663-74-8
68194-16-1
38411-25-5
40186-70-7
52663-65-7
52663-70-4
52663-67-9
52663-64-6
35065-29-3
74472-47-2
60145-23-5
52663-69-1
74472-48-3
52712-05-7
74472-49-4
52663-68-0
74487-85-7
39635-31-9
41411-64-7
74472-50-7
74472-51-8
Client Sample:
PQL
16.8
16.8
16.8
16.8
16.8
16.8
16.8
33.6
16.8
16.8
16.8
16.8
16.8
16.8
16.8
33.6
16.8
16.8
33.6
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
Page 19 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 7 of 8
SDG Number:6110379
Lab Sample ID:10122001 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 15.5
Date Collected:11/15/2016 16:00
Surrogate/Tracer recovery Recovery%Acceptable Limits
18.7
16.8
16.8
33.6
33.6
16.8
16.8
17.9
16.8
16.8
16.8
16.8
16.8
16.8
961
C180
U
U
CU
CU
C198
C197
U
U
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
50.2
58.2
59.9
82.0
67.3
98.5
79.8
113
111
81.2
103
101
99.2
103
101
95.0
98.6
101
101
87.2
96.8
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 06:41 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-07 CIS-6-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.1 g
Result Nominal
84.2
97.7
101
138
113
165
134
189
187
136
172
170
166
174
170
159
331
169
169
146
162
168
168
168
168
168
168
168
168
168
168
168
168
168
168
168
168
336
168
168
168
168
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d01dec16b_2-8Data File:
Prep SOP Ref: CF-OA-E-001
193-HpCB
194-OcCB
195-OcCB
196-OcCB
197-OcCB
198-OcCB
199-OcCB
200-OcCB
201-OcCB
202-OcCB
203-OcCB
204-OcCB
205-OcCB
206-NoCB
207-NoCB
208-NoCB
209-DeCB
Total PCB Congeners
69782-91-8
35694-08-7
52663-78-2
42740-50-1
33091-17-7
68194-17-2
52663-75-9
52663-73-7
40186-71-8
2136-99-4
52663-76-0
74472-52-9
74472-53-0
40186-72-9
52663-79-3
52663-77-1
2051-24-3
1336-36-3
Client Sample:
UnitsQual
C
C156L
PQL
16.8
16.8
16.8
33.6
33.6
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
Page 20 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 8 of 8
SDG Number:6110379
Lab Sample ID:10122001 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 15.5
Date Collected:11/15/2016 16:00
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
86.0
101
88.1
83.3
111
89.7
79.9
99.9
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 06:41 Analyst:MJC

Units
6110379-07 CIS-6-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.1 g
Result Nominal
144
169
148
140
187
151
134
168
168
168
168
168
168
168
168
168
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_2-8Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
PQL
Page 21 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 1 of 8
SDG Number:6110379
Lab Sample ID:10122002 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 28.3
Date Collected:11/15/2016 15:10
18
18
18
18
18
18
18
18
18
18
180
36.1
18
18
18
18
36.1
18
36.1
36.1
18
18
18
18
36.1
18
18
18
U
U
U
U
U
U
U
U
U
U
U
CU
C12
U
U
U
U
CU
U
CU
CU
U
U
U
U
CU
U
C20
C26
C18
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 09:59 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-09 CIS-7-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 15.47 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_2-11Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
2-MoCB
3-MoCB
4-DiCB
5-DiCB
6-DiCB
7-DiCB
8-DiCB
9-DiCB
10-DiCB
11-DiCB
12-DiCB
13-DiCB
14-DiCB
15-DiCB
16-TrCB
17-TrCB
18-TrCB
19-TrCB
20-TrCB
21-TrCB
22-TrCB
23-TrCB
24-TrCB
25-TrCB
26-TrCB
27-TrCB
28-TrCB
29-TrCB
30-TrCB
31-TrCB
32-TrCB
2051-60-7
2051-61-8
2051-62-9
13029-08-8
16605-91-7
25569-80-6
33284-50-3
34883-43-7
34883-39-1
33146-45-1
2050-67-1
2974-92-7
2974-90-5
34883-41-5
2050-68-2
38444-78-9
37680-66-3
37680-65-2
38444-73-4
38444-84-7
55702-46-0
38444-85-8
55720-44-0
55702-45-9
55712-37-3
38444-81-4
38444-76-7
7012-37-5
15862-07-4
35693-92-6
16606-02-3
38444-77-8
Client Sample:
PQL
18.0
18.0
18.0
18.0
18.0
18.0
18.0
18.0
18.0
18.0
180
36.1
18.0
18.0
18.0
18.0
36.1
18.0
36.1
36.1
18.0
18.0
18.0
18.0
36.1
18.0
18.0
18.0
Page 22 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 2 of 8
SDG Number:6110379
Lab Sample ID:10122002 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 28.3
Date Collected:11/15/2016 15:10
18
18
18
18
18
18
36.1
18
18
18
54.1
36.1
18
18
36.1
36.1
18
18
18
18
18
18
54.1
18
72.2
18
18
C21
U
U
U
U
U
U
CU
U
U
U
CU
CU
U
C44
U
CU
CU
C45
U
C50
U
U
U
U
U
CU
U
CU
C59
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 09:59 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-09 CIS-7-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 15.47 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_2-11Data File:
Prep SOP Ref: CF-OA-E-001
33-TrCB
34-TrCB
35-TrCB
36-TrCB
37-TrCB
38-TrCB
39-TrCB
40-TeCB
41-TeCB
42-TeCB
43-TeCB
44-TeCB
45-TeCB
46-TeCB
47-TeCB
48-TeCB
49-TeCB
50-TeCB
51-TeCB
52-TeCB
53-TeCB
54-TeCB
55-TeCB
56-TeCB
57-TeCB
58-TeCB
59-TeCB
60-TeCB
61-TeCB
62-TeCB
63-TeCB
64-TeCB
38444-86-9
37680-68-5
37680-69-6
38444-87-0
38444-90-5
53555-66-1
38444-88-1
38444-93-8
52663-59-9
36559-22-5
70362-46-8
41464-39-5
70362-45-7
41464-47-5
2437-79-8
70362-47-9
41464-40-8
62796-65-0
68194-04-7
35693-99-3
41464-41-9
15968-05-5
74338-24-2
41464-43-1
70424-67-8
41464-49-7
74472-33-6
33025-41-1
33284-53-6
54230-22-7
74472-34-7
52663-58-8
Client Sample:
PQL
18.0
18.0
18.0
18.0
18.0
18.0
36.1
18.0
18.0
18.0
54.1
36.1
18.0
18.0
36.1
36.1
18.0
18.0
18.0
18.0
18.0
18.0
54.1
18.0
72.2
18.0
18.0
Page 23 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 3 of 8
SDG Number:6110379
Lab Sample ID:10122002 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 28.3
Date Collected:11/15/2016 15:10
18
18
18
18
18
18
18
18
18
18
18
18
18
54.1
108
36.1
18
54.1
18
36.1
18
18
18
C44
U
U
U
C49
C61
C40
U
U
C61
C59
C61
U
U
U
U
U
U
U
U
CU
CU
C86
CU
U
CU
C88
U
CU
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 09:59 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-09 CIS-7-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 15.47 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_2-11Data File:
Prep SOP Ref: CF-OA-E-001
65-TeCB
66-TeCB
67-TeCB
68-TeCB
69-TeCB
70-TeCB
71-TeCB
72-TeCB
73-TeCB
74-TeCB
75-TeCB
76-TeCB
77-TeCB
78-TeCB
79-TeCB
80-TeCB
81-TeCB
82-PeCB
83-PeCB
84-PeCB
85-PeCB
86-PeCB
87-PeCB
88-PeCB
89-PeCB
90-PeCB
91-PeCB
92-PeCB
93-PeCB
94-PeCB
95-PeCB
96-PeCB
33284-54-7
32598-10-0
73575-53-8
73575-52-7
60233-24-1
32598-11-1
41464-46-4
41464-42-0
74338-23-1
32690-93-0
32598-12-2
70362-48-0
32598-13-3
70362-49-1
41464-48-6
33284-52-5
70362-50-4
52663-62-4
60145-20-2
52663-60-2
65510-45-4
55312-69-1
38380-02-8
55215-17-3
73575-57-2
68194-07-0
68194-05-8
52663-61-3
73575-56-1
73575-55-0
38379-99-6
73575-54-9
Client Sample:
PQL
18.0
18.0
18.0
18.0
18.0
18.0
18.0
18.0
18.0
18.0
18.0
18.0
18.0
54.1
108
36.1
18.0
54.1
18.0
36.1
18.0
18.0
18.0
Page 24 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 4 of 8
SDG Number:6110379
Lab Sample ID:10122002 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 28.3
Date Collected:11/15/2016 15:10
36.1
18
18
18
18
18
18
36.1
36.1
18
18
18
22.1
18
18
18
18
18
18
36.1
C86
CU
U
C93
C90
C98
U
U
U
U
U
CU
C86
CU
U
U
C90
U
C110
C85
C85
C86
U
U
U
U
C108
C86
U
U
CU
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 09:59 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-09 CIS-7-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 15.47 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_2-11Data File:
Prep SOP Ref: CF-OA-E-001
97-PeCB
98-PeCB
99-PeCB
100-PeCB
101-PeCB
102-PeCB
103-PeCB
104-PeCB
105-PeCB
106-PeCB
107-PeCB
108-PeCB
109-PeCB
110-PeCB
111-PeCB
112-PeCB
113-PeCB
114-PeCB
115-PeCB
116-PeCB
117-PeCB
118-PeCB
119-PeCB
120-PeCB
121-PeCB
122-PeCB
123-PeCB
124-PeCB
125-PeCB
126-PeCB
127-PeCB
128-HxCB
41464-51-1
60233-25-2
38380-01-7
39485-83-1
37680-73-2
68194-06-9
60145-21-3
56558-16-8
32598-14-4
70424-69-0
70424-68-9
70362-41-3
74472-35-8
38380-03-9
39635-32-0
74472-36-9
68194-10-5
74472-37-0
74472-38-1
18259-05-7
68194-11-6
31508-00-6
56558-17-9
68194-12-7
56558-18-0
76842-07-4
65510-44-3
70424-70-3
74472-39-2
57465-28-8
39635-33-1
38380-07-3
Client Sample:
PQL
36.1
18.0
18.0
18.0
18.0
18.0
18.0
36.1
36.1
18.0
18.0
18.0
18.0
18.0
18.0
18.0
18.0
18.0
18.0
36.1
Page 25 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 5 of 8
SDG Number:6110379
Lab Sample ID:10122002 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 28.3
Date Collected:11/15/2016 15:10
54.1
18
18
18
18
18
36.1
18
18
36.1
18
18
18
18
18
18
36.1
18
18
18
36.1
18
18
36.1
18
18
18
CU
U
U
U
U
U
CU
U
U
C129
CU
C139
U
U
U
U
U
U
CU
U
C147
U
C135
U
CU
U
U
CU
C156
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 09:59 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-09 CIS-7-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 15.47 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_2-11Data File:
Prep SOP Ref: CF-OA-E-001
129-HxCB
130-HxCB
131-HxCB
132-HxCB
133-HxCB
134-HxCB
135-HxCB
136-HxCB
137-HxCB
138-HxCB
139-HxCB
140-HxCB
141-HxCB
142-HxCB
143-HxCB
144-HxCB
145-HxCB
146-HxCB
147-HxCB
148-HxCB
149-HxCB
150-HxCB
151-HxCB
152-HxCB
153-HxCB
154-HxCB
155-HxCB
156-HxCB
157-HxCB
158-HxCB
159-HxCB
160-HxCB
55215-18-4
52663-66-8
61798-70-7
38380-05-1
35694-04-3
52704-70-8
52744-13-5
38411-22-2
35694-06-5
35065-28-2
56030-56-9
59291-64-4
52712-04-6
41411-61-4
68194-15-0
68194-14-9
74472-40-5
51908-16-8
68194-13-8
74472-41-6
38380-04-0
68194-08-1
52663-63-5
68194-09-2
35065-27-1
60145-22-4
33979-03-2
38380-08-4
69782-90-7
74472-42-7
39635-35-3
41411-62-5
Client Sample:
PQL
54.1
18.0
18.0
18.0
18.0
18.0
36.1
18.0
18.0
36.1
18.0
18.0
18.0
18.0
18.0
18.0
36.1
18.0
18.0
18.0
36.1
18.0
18.0
36.1
18.0
18.0
18.0
Page 26 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 6 of 8
SDG Number:6110379
Lab Sample ID:10122002 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 28.3
Date Collected:11/15/2016 15:10
18
18
18
18
18
18
18
36.1
18
18
18
18
18
18
18
36.1
18
18
36.1
18
18
21.0
18
18
18
18
18
U
U
C129
U
U
C128
U
C153
U
U
CU
U
C171
U
U
U
U
U
U
CU
U
U
CU
U
C183
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 09:59 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-09 CIS-7-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 15.47 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_2-11Data File:
Prep SOP Ref: CF-OA-E-001
161-HxCB
162-HxCB
163-HxCB
164-HxCB
165-HxCB
166-HxCB
167-HxCB
168-HxCB
169-HxCB
170-HpCB
171-HpCB
172-HpCB
173-HpCB
174-HpCB
175-HpCB
176-HpCB
177-HpCB
178-HpCB
179-HpCB
180-HpCB
181-HpCB
182-HpCB
183-HpCB
184-HpCB
185-HpCB
186-HpCB
187-HpCB
188-HpCB
189-HpCB
190-HpCB
191-HpCB
192-HpCB
74472-43-8
39635-34-2
74472-44-9
74472-45-0
74472-46-1
41411-63-6
52663-72-6
59291-65-5
32774-16-6
35065-30-6
52663-71-5
52663-74-8
68194-16-1
38411-25-5
40186-70-7
52663-65-7
52663-70-4
52663-67-9
52663-64-6
35065-29-3
74472-47-2
60145-23-5
52663-69-1
74472-48-3
52712-05-7
74472-49-4
52663-68-0
74487-85-7
39635-31-9
41411-64-7
74472-50-7
74472-51-8
Client Sample:
PQL
18.0
18.0
18.0
18.0
18.0
18.0
18.0
36.1
18.0
18.0
18.0
18.0
18.0
18.0
18.0
36.1
18.0
18.0
36.1
18.0
18.0
18.0
18.0
18.0
18.0
18.0
18.0
Page 27 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 7 of 8
SDG Number:6110379
Lab Sample ID:10122002 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 28.3
Date Collected:11/15/2016 15:10
Surrogate/Tracer recovery Recovery%Acceptable Limits
18
18
18
36.1
36.1
18
18
18
18
18
18
18
18
18
43.1
C180
U
U
U
CU
CU
C198
C197
U
U
U
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
29.3
38.4
39.0
60.8
48.3
74.7
59.2
95.1
94.0
62.2
86.2
84.3
84.3
86.8
87.8
73.4
85.1
86.6
86.5
66.6
78.3
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 09:59 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-09 CIS-7-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 15.47 g
Result Nominal
52.8
69.3
70.3
110
87.2
135
107
172
170
112
156
152
152
157
158
132
307
156
156
120
141
180
180
180
180
180
180
180
180
180
180
180
180
180
180
180
180
361
180
180
180
180
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d01dec16b_2-11Data File:
Prep SOP Ref: CF-OA-E-001
193-HpCB
194-OcCB
195-OcCB
196-OcCB
197-OcCB
198-OcCB
199-OcCB
200-OcCB
201-OcCB
202-OcCB
203-OcCB
204-OcCB
205-OcCB
206-NoCB
207-NoCB
208-NoCB
209-DeCB
Total PCB Congeners
69782-91-8
35694-08-7
52663-78-2
42740-50-1
33091-17-7
68194-17-2
52663-75-9
52663-73-7
40186-71-8
2136-99-4
52663-76-0
74472-52-9
74472-53-0
40186-72-9
52663-79-3
52663-77-1
2051-24-3
1336-36-3
Client Sample:
UnitsQual
C
C156L
PQL
18.0
18.0
18.0
36.1
36.1
18.0
18.0
18.0
18.0
18.0
18.0
18.0
18.0
18.0
18.0
Page 28 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 8 of 8
SDG Number:6110379
Lab Sample ID:10122002 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 28.3
Date Collected:11/15/2016 15:10
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
69.4
81.7
71.3
67.3
86.3
80.7
75.8
88.6
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 09:59 Analyst:MJC

Units
6110379-09 CIS-7-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 15.47 g
Result Nominal
125
147
129
121
156
146
137
160
180
180
180
180
180
180
180
180
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_2-11Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
PQL
Page 29 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 1 of 8
SDG Number:6110379
Lab Sample ID:10122003 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 19.2
Date Collected:11/15/2016 16:55
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
17.5
3.51
1.75
1.75
1.75
1.75
3.51
1.75
3.51
3.51
1.75
1.75
1.75
1.75
3.51
1.75
1.75
1.75
U
U
U
U
U
U
U
U
U
U
U
CU
C12
U
U
U
U
CU
U
CU
CU
U
U
U
U
CU
U
C20
C26
C18
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/02/2016 13:30 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-10 CIS-8-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.12 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_3-3Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
2-MoCB
3-MoCB
4-DiCB
5-DiCB
6-DiCB
7-DiCB
8-DiCB
9-DiCB
10-DiCB
11-DiCB
12-DiCB
13-DiCB
14-DiCB
15-DiCB
16-TrCB
17-TrCB
18-TrCB
19-TrCB
20-TrCB
21-TrCB
22-TrCB
23-TrCB
24-TrCB
25-TrCB
26-TrCB
27-TrCB
28-TrCB
29-TrCB
30-TrCB
31-TrCB
32-TrCB
2051-60-7
2051-61-8
2051-62-9
13029-08-8
16605-91-7
25569-80-6
33284-50-3
34883-43-7
34883-39-1
33146-45-1
2050-67-1
2974-92-7
2974-90-5
34883-41-5
2050-68-2
38444-78-9
37680-66-3
37680-65-2
38444-73-4
38444-84-7
55702-46-0
38444-85-8
55720-44-0
55702-45-9
55712-37-3
38444-81-4
38444-76-7
7012-37-5
15862-07-4
35693-92-6
16606-02-3
38444-77-8
Client Sample:
PQL
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
17.5
3.51
1.75
1.75
1.75
1.75
3.51
1.75
3.51
3.51
1.75
1.75
1.75
1.75
3.51
1.75
1.75
1.75
Page 30 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 2 of 8
SDG Number:6110379
Lab Sample ID:10122003 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 19.2
Date Collected:11/15/2016 16:55
1.75
1.75
1.75
1.75
1.75
1.75
3.51
1.75
1.75
1.75
5.26
3.51
1.75
1.75
3.51
3.51
1.75
1.75
1.75
1.75
1.75
1.75
5.26
1.75
7.01
1.75
1.75
C21
U
U
U
U
U
U
CU
U
U
U
CU
CU
U
C44
U
CU
CU
C45
U
C50
U
U
U
U
U
CU
U
CU
C59
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/02/2016 13:30 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-10 CIS-8-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.12 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_3-3Data File:
Prep SOP Ref: CF-OA-E-001
33-TrCB
34-TrCB
35-TrCB
36-TrCB
37-TrCB
38-TrCB
39-TrCB
40-TeCB
41-TeCB
42-TeCB
43-TeCB
44-TeCB
45-TeCB
46-TeCB
47-TeCB
48-TeCB
49-TeCB
50-TeCB
51-TeCB
52-TeCB
53-TeCB
54-TeCB
55-TeCB
56-TeCB
57-TeCB
58-TeCB
59-TeCB
60-TeCB
61-TeCB
62-TeCB
63-TeCB
64-TeCB
38444-86-9
37680-68-5
37680-69-6
38444-87-0
38444-90-5
53555-66-1
38444-88-1
38444-93-8
52663-59-9
36559-22-5
70362-46-8
41464-39-5
70362-45-7
41464-47-5
2437-79-8
70362-47-9
41464-40-8
62796-65-0
68194-04-7
35693-99-3
41464-41-9
15968-05-5
74338-24-2
41464-43-1
70424-67-8
41464-49-7
74472-33-6
33025-41-1
33284-53-6
54230-22-7
74472-34-7
52663-58-8
Client Sample:
PQL
1.75
1.75
1.75
1.75
1.75
1.75
3.51
1.75
1.75
1.75
5.26
3.51
1.75
1.75
3.51
3.51
1.75
1.75
1.75
1.75
1.75
1.75
5.26
1.75
7.01
1.75
1.75
Page 31 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 3 of 8
SDG Number:6110379
Lab Sample ID:10122003 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 19.2
Date Collected:11/15/2016 16:55
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
5.26
10.5
3.51
1.75
5.26
1.75
3.51
1.75
1.75
1.75
C44
U
U
U
C49
C61
C40
U
U
C61
C59
C61
U
U
U
U
U
U
U
U
CU
CU
C86
CU
U
CU
C88
U
CU
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/02/2016 13:30 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-10 CIS-8-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.12 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_3-3Data File:
Prep SOP Ref: CF-OA-E-001
65-TeCB
66-TeCB
67-TeCB
68-TeCB
69-TeCB
70-TeCB
71-TeCB
72-TeCB
73-TeCB
74-TeCB
75-TeCB
76-TeCB
77-TeCB
78-TeCB
79-TeCB
80-TeCB
81-TeCB
82-PeCB
83-PeCB
84-PeCB
85-PeCB
86-PeCB
87-PeCB
88-PeCB
89-PeCB
90-PeCB
91-PeCB
92-PeCB
93-PeCB
94-PeCB
95-PeCB
96-PeCB
33284-54-7
32598-10-0
73575-53-8
73575-52-7
60233-24-1
32598-11-1
41464-46-4
41464-42-0
74338-23-1
32690-93-0
32598-12-2
70362-48-0
32598-13-3
70362-49-1
41464-48-6
33284-52-5
70362-50-4
52663-62-4
60145-20-2
52663-60-2
65510-45-4
55312-69-1
38380-02-8
55215-17-3
73575-57-2
68194-07-0
68194-05-8
52663-61-3
73575-56-1
73575-55-0
38379-99-6
73575-54-9
Client Sample:
PQL
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
5.26
10.5
3.51
1.75
5.26
1.75
3.51
1.75
1.75
1.75
Page 32 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 4 of 8
SDG Number:6110379
Lab Sample ID:10122003 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 19.2
Date Collected:11/15/2016 16:55
3.51
1.75
1.75
1.75
1.75
1.75
1.75
3.51
3.51
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
3.51
C86
CU
U
C93
C90
C98
U
U
U
U
U
CU
C86
CU
U
U
C90
U
C110
C85
C85
U
C86
U
U
U
U
C108
C86
U
U
CU
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/02/2016 13:30 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-10 CIS-8-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.12 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_3-3Data File:
Prep SOP Ref: CF-OA-E-001
97-PeCB
98-PeCB
99-PeCB
100-PeCB
101-PeCB
102-PeCB
103-PeCB
104-PeCB
105-PeCB
106-PeCB
107-PeCB
108-PeCB
109-PeCB
110-PeCB
111-PeCB
112-PeCB
113-PeCB
114-PeCB
115-PeCB
116-PeCB
117-PeCB
118-PeCB
119-PeCB
120-PeCB
121-PeCB
122-PeCB
123-PeCB
124-PeCB
125-PeCB
126-PeCB
127-PeCB
128-HxCB
41464-51-1
60233-25-2
38380-01-7
39485-83-1
37680-73-2
68194-06-9
60145-21-3
56558-16-8
32598-14-4
70424-69-0
70424-68-9
70362-41-3
74472-35-8
38380-03-9
39635-32-0
74472-36-9
68194-10-5
74472-37-0
74472-38-1
18259-05-7
68194-11-6
31508-00-6
56558-17-9
68194-12-7
56558-18-0
76842-07-4
65510-44-3
70424-70-3
74472-39-2
57465-28-8
39635-33-1
38380-07-3
Client Sample:
PQL
3.51
1.75
1.75
1.75
1.75
1.75
1.75
3.51
3.51
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
3.51
Page 33 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 5 of 8
SDG Number:6110379
Lab Sample ID:10122003 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 19.2
Date Collected:11/15/2016 16:55
37.2
1.75
1.75
4.36
1.75
1.75
11.4
1.75
1.75
3.51
7.76
1.75
1.75
1.75
1.75
3.93
14.3
1.75
1.75
1.75
21.6
1.75
1.75
3.51
2.76
1.75
1.75
C
U
U
U
U
C
U
U
C129
CU
C139
U
U
U
U
C
U
C147
U
C135
U
C
U
U
CU
C156
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/02/2016 13:30 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-10 CIS-8-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.12 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_3-3Data File:
Prep SOP Ref: CF-OA-E-001
129-HxCB
130-HxCB
131-HxCB
132-HxCB
133-HxCB
134-HxCB
135-HxCB
136-HxCB
137-HxCB
138-HxCB
139-HxCB
140-HxCB
141-HxCB
142-HxCB
143-HxCB
144-HxCB
145-HxCB
146-HxCB
147-HxCB
148-HxCB
149-HxCB
150-HxCB
151-HxCB
152-HxCB
153-HxCB
154-HxCB
155-HxCB
156-HxCB
157-HxCB
158-HxCB
159-HxCB
160-HxCB
55215-18-4
52663-66-8
61798-70-7
38380-05-1
35694-04-3
52704-70-8
52744-13-5
38411-22-2
35694-06-5
35065-28-2
56030-56-9
59291-64-4
52712-04-6
41411-61-4
68194-15-0
68194-14-9
74472-40-5
51908-16-8
68194-13-8
74472-41-6
38380-04-0
68194-08-1
52663-63-5
68194-09-2
35065-27-1
60145-22-4
33979-03-2
38380-08-4
69782-90-7
74472-42-7
39635-35-3
41411-62-5
Client Sample:
PQL
5.26
1.75
1.75
1.75
1.75
1.75
3.51
1.75
1.75
3.51
1.75
1.75
1.75
1.75
1.75
1.75
3.51
1.75
1.75
1.75
3.51
1.75
1.75
3.51
1.75
1.75
1.75
Page 34 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 6 of 8
SDG Number:6110379
Lab Sample ID:10122003 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 19.2
Date Collected:11/15/2016 16:55
1.75
1.75
3.14
1.75
1.75
1.75
22.4
7.11
3.87
25.9
1.75
2.54
13.8
4.97
10.7
56.9
1.75
1.75
17.1
1.75
1.75
30.3
1.75
1.75
5.09
1.75
1.75
U
U
C129
U
C128
U
C153
U
C
C171
U
C
U
U
C
U
C183
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/02/2016 13:30 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-10 CIS-8-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.12 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_3-3Data File:
Prep SOP Ref: CF-OA-E-001
161-HxCB
162-HxCB
163-HxCB
164-HxCB
165-HxCB
166-HxCB
167-HxCB
168-HxCB
169-HxCB
170-HpCB
171-HpCB
172-HpCB
173-HpCB
174-HpCB
175-HpCB
176-HpCB
177-HpCB
178-HpCB
179-HpCB
180-HpCB
181-HpCB
182-HpCB
183-HpCB
184-HpCB
185-HpCB
186-HpCB
187-HpCB
188-HpCB
189-HpCB
190-HpCB
191-HpCB
192-HpCB
74472-43-8
39635-34-2
74472-44-9
74472-45-0
74472-46-1
41411-63-6
52663-72-6
59291-65-5
32774-16-6
35065-30-6
52663-71-5
52663-74-8
68194-16-1
38411-25-5
40186-70-7
52663-65-7
52663-70-4
52663-67-9
52663-64-6
35065-29-3
74472-47-2
60145-23-5
52663-69-1
74472-48-3
52712-05-7
74472-49-4
52663-68-0
74487-85-7
39635-31-9
41411-64-7
74472-50-7
74472-51-8
Client Sample:
PQL
1.75
1.75
1.75
1.75
1.75
1.75
1.75
3.51
1.75
1.75
1.75
1.75
1.75
1.75
1.75
3.51
1.75
1.75
3.51
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
Page 35 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 7 of 8
SDG Number:6110379
Lab Sample ID:10122003 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 19.2
Date Collected:11/15/2016 16:55
Surrogate/Tracer recovery Recovery%Acceptable Limits
11.8
5.20
6.27
3.51
12.7
1.75
2.09
8.02
1.75
1.75
2.36
1.75
1.75
1.75
356
C180
CU
C
C198
C197
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
52.7
56.0
56.1
132
82.8
97.7
51.4
129
129
70.8
107
105
103
106
112
80.7
101
102
113
62.2
88.3
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/02/2016 13:30 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-10 CIS-8-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.12 g
Result Nominal
92.4
98.2
98.3
231
145
171
90.1
227
226
124
188
183
181
186
197
141
355
178
198
109
155
175
175
175
175
175
175
175
175
175
175
175
175
175
175
175
175
351
175
175
175
175
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d01dec16b_3-3Data File:
Prep SOP Ref: CF-OA-E-001
193-HpCB
194-OcCB
195-OcCB
196-OcCB
197-OcCB
198-OcCB
199-OcCB
200-OcCB
201-OcCB
202-OcCB
203-OcCB
204-OcCB
205-OcCB
206-NoCB
207-NoCB
208-NoCB
209-DeCB
Total PCB Congeners
69782-91-8
35694-08-7
52663-78-2
42740-50-1
33091-17-7
68194-17-2
52663-75-9
52663-73-7
40186-71-8
2136-99-4
52663-76-0
74472-52-9
74472-53-0
40186-72-9
52663-79-3
52663-77-1
2051-24-3
1336-36-3
Client Sample:
UnitsQual
C
C156L
PQL
1.75
1.75
1.75
3.51
3.51
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
1.75
Page 36 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 8 of 8
SDG Number:6110379
Lab Sample ID:10122003 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 19.2
Date Collected:11/15/2016 16:55
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
66.3
98.3
86.2
73.5
105
96.0
58.3
102
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/02/2016 13:30 Analyst:MJC

Units
6110379-10 CIS-8-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.12 g
Result Nominal
116
172
151
129
184
168
102
178
175
175
175
175
175
175
175
175
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_3-3Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
PQL
Page 37 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 1 of 8
SDG Number:6110379
Lab Sample ID:10122004 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 14.4
Date Collected:11/15/2016 12:45
2010
237
1580
769
220
476
229
1570
239
220
2200
441
220
1190
490
475
1020
220
1410
681
485
220
220
220
441
220
1030
340
U
U
U
CU
C12
U
C
U
C
C
U
U
U
CU
U
C20
C26
C18
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
10
Run Date:12/08/2016 17:46 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-12 CIS-9-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 1.06 g
33474 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d08dec16a-8Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
2-MoCB
3-MoCB
4-DiCB
5-DiCB
6-DiCB
7-DiCB
8-DiCB
9-DiCB
10-DiCB
11-DiCB
12-DiCB
13-DiCB
14-DiCB
15-DiCB
16-TrCB
17-TrCB
18-TrCB
19-TrCB
20-TrCB
21-TrCB
22-TrCB
23-TrCB
24-TrCB
25-TrCB
26-TrCB
27-TrCB
28-TrCB
29-TrCB
30-TrCB
31-TrCB
32-TrCB
2051-60-7
2051-61-8
2051-62-9
13029-08-8
16605-91-7
25569-80-6
33284-50-3
34883-43-7
34883-39-1
33146-45-1
2050-67-1
2974-92-7
2974-90-5
34883-41-5
2050-68-2
38444-78-9
37680-66-3
37680-65-2
38444-73-4
38444-84-7
55702-46-0
38444-85-8
55720-44-0
55702-45-9
55712-37-3
38444-81-4
38444-76-7
7012-37-5
15862-07-4
35693-92-6
16606-02-3
38444-77-8
Client Sample:
PQL
220
220
220
220
220
220
220
220
220
220
2200
441
220
220
220
220
441
220
441
441
220
220
220
220
441
220
220
220
Page 38 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 2 of 8
SDG Number:6110379
Lab Sample ID:10122004 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 14.4
Date Collected:11/15/2016 12:45
220
220
220
412
220
220
441
220
277
220
996
441
220
220
584
441
1230
220
220
534
220
220
661
291
2040
220
541
C21
U
U
U
U
U
CU
U
U
C
CU
U
C44
U
C
CU
C45
C50
U
U
U
U
CU
C
C59
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
10
Run Date:12/08/2016 17:46 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-12 CIS-9-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 1.06 g
33474 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d08dec16a-8Data File:
Prep SOP Ref: CF-OA-E-001
33-TrCB
34-TrCB
35-TrCB
36-TrCB
37-TrCB
38-TrCB
39-TrCB
40-TeCB
41-TeCB
42-TeCB
43-TeCB
44-TeCB
45-TeCB
46-TeCB
47-TeCB
48-TeCB
49-TeCB
50-TeCB
51-TeCB
52-TeCB
53-TeCB
54-TeCB
55-TeCB
56-TeCB
57-TeCB
58-TeCB
59-TeCB
60-TeCB
61-TeCB
62-TeCB
63-TeCB
64-TeCB
38444-86-9
37680-68-5
37680-69-6
38444-87-0
38444-90-5
53555-66-1
38444-88-1
38444-93-8
52663-59-9
36559-22-5
70362-46-8
41464-39-5
70362-45-7
41464-47-5
2437-79-8
70362-47-9
41464-40-8
62796-65-0
68194-04-7
35693-99-3
41464-41-9
15968-05-5
74338-24-2
41464-43-1
70424-67-8
41464-49-7
74472-33-6
33025-41-1
33284-53-6
54230-22-7
74472-34-7
52663-58-8
Client Sample:
PQL
220
220
220
220
220
220
441
220
220
220
661
441
220
220
441
441
220
220
220
220
220
220
661
220
881
220
220
Page 39 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 3 of 8
SDG Number:6110379
Lab Sample ID:10122004 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 14.4
Date Collected:11/15/2016 12:45
858
220
220
220
220
220
220
220
220
220
220
220
343
661
1320
441
220
2850
358
441
220
1750
220
C44
U
U
C49
C61
C40
U
U
C61
C59
C61
U
U
U
U
U
U
U
CU
CU
C86
CU
U
C
C88
CU
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
10
Run Date:12/08/2016 17:46 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-12 CIS-9-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 1.06 g
33474 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d08dec16a-8Data File:
Prep SOP Ref: CF-OA-E-001
65-TeCB
66-TeCB
67-TeCB
68-TeCB
69-TeCB
70-TeCB
71-TeCB
72-TeCB
73-TeCB
74-TeCB
75-TeCB
76-TeCB
77-TeCB
78-TeCB
79-TeCB
80-TeCB
81-TeCB
82-PeCB
83-PeCB
84-PeCB
85-PeCB
86-PeCB
87-PeCB
88-PeCB
89-PeCB
90-PeCB
91-PeCB
92-PeCB
93-PeCB
94-PeCB
95-PeCB
96-PeCB
33284-54-7
32598-10-0
73575-53-8
73575-52-7
60233-24-1
32598-11-1
41464-46-4
41464-42-0
74338-23-1
32690-93-0
32598-12-2
70362-48-0
32598-13-3
70362-49-1
41464-48-6
33284-52-5
70362-50-4
52663-62-4
60145-20-2
52663-60-2
65510-45-4
55312-69-1
38380-02-8
55215-17-3
73575-57-2
68194-07-0
68194-05-8
52663-61-3
73575-56-1
73575-55-0
38379-99-6
73575-54-9
Client Sample:
PQL
220
220
220
220
220
220
220
220
220
220
220
220
220
661
1320
441
220
661
220
441
220
220
220
Page 40 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 4 of 8
SDG Number:6110379
Lab Sample ID:10122004 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 14.4
Date Collected:11/15/2016 12:45
441
681
220
220
721
220
220
441
2240
220
220
220
1930
220
220
220
220
220
220
441
C86
CU
C93
C90
C98
U
U
U
U
CU
C86
C
U
U
C90
U
C110
C85
C85
C86
U
U
U
U
C108
C86
U
U
CU
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
10
Run Date:12/08/2016 17:46 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-12 CIS-9-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 1.06 g
33474 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d08dec16a-8Data File:
Prep SOP Ref: CF-OA-E-001
97-PeCB
98-PeCB
99-PeCB
100-PeCB
101-PeCB
102-PeCB
103-PeCB
104-PeCB
105-PeCB
106-PeCB
107-PeCB
108-PeCB
109-PeCB
110-PeCB
111-PeCB
112-PeCB
113-PeCB
114-PeCB
115-PeCB
116-PeCB
117-PeCB
118-PeCB
119-PeCB
120-PeCB
121-PeCB
122-PeCB
123-PeCB
124-PeCB
125-PeCB
126-PeCB
127-PeCB
128-HxCB
41464-51-1
60233-25-2
38380-01-7
39485-83-1
37680-73-2
68194-06-9
60145-21-3
56558-16-8
32598-14-4
70424-69-0
70424-68-9
70362-41-3
74472-35-8
38380-03-9
39635-32-0
74472-36-9
68194-10-5
74472-37-0
74472-38-1
18259-05-7
68194-11-6
31508-00-6
56558-17-9
68194-12-7
56558-18-0
76842-07-4
65510-44-3
70424-70-3
74472-39-2
57465-28-8
39635-33-1
38380-07-3
Client Sample:
PQL
441
220
220
220
220
220
220
441
441
220
220
220
220
220
220
220
220
220
220
441
Page 41 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 5 of 8
SDG Number:6110379
Lab Sample ID:10122004 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 14.4
Date Collected:11/15/2016 12:45
6000
220
220
1610
220
220
2580
677
220
441
1560
220
220
402
220
812
5090
220
220
220
6210
220
220
554
515
220
220
C
U
U
U
U
C
U
C129
CU
C139
U
U
U
C
U
C147
U
C135
U
C
U
U
C
C156
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
10
Run Date:12/08/2016 17:46 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-12 CIS-9-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 1.06 g
33474 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d08dec16a-8Data File:
Prep SOP Ref: CF-OA-E-001
129-HxCB
130-HxCB
131-HxCB
132-HxCB
133-HxCB
134-HxCB
135-HxCB
136-HxCB
137-HxCB
138-HxCB
139-HxCB
140-HxCB
141-HxCB
142-HxCB
143-HxCB
144-HxCB
145-HxCB
146-HxCB
147-HxCB
148-HxCB
149-HxCB
150-HxCB
151-HxCB
152-HxCB
153-HxCB
154-HxCB
155-HxCB
156-HxCB
157-HxCB
158-HxCB
159-HxCB
160-HxCB
55215-18-4
52663-66-8
61798-70-7
38380-05-1
35694-04-3
52704-70-8
52744-13-5
38411-22-2
35694-06-5
35065-28-2
56030-56-9
59291-64-4
52712-04-6
41411-61-4
68194-15-0
68194-14-9
74472-40-5
51908-16-8
68194-13-8
74472-41-6
38380-04-0
68194-08-1
52663-63-5
68194-09-2
35065-27-1
60145-22-4
33979-03-2
38380-08-4
69782-90-7
74472-42-7
39635-35-3
41411-62-5
Client Sample:
PQL
661
220
220
220
220
220
441
220
220
441
220
220
220
220
220
220
441
220
220
220
441
220
220
441
220
220
220
Page 42 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 6 of 8
SDG Number:6110379
Lab Sample ID:10122004 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 14.4
Date Collected:11/15/2016 12:45
220
220
397
220
220
220
3220
930
569
3610
220
399
1880
724
1420
9350
220
220
2750
220
220
4970
220
220
672
220
220
U
U
C129
U
C128
U
C153
U
C
C171
U
C
U
U
C
U
C183
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
10
Run Date:12/08/2016 17:46 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-12 CIS-9-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 1.06 g
33474 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d08dec16a-8Data File:
Prep SOP Ref: CF-OA-E-001
161-HxCB
162-HxCB
163-HxCB
164-HxCB
165-HxCB
166-HxCB
167-HxCB
168-HxCB
169-HxCB
170-HpCB
171-HpCB
172-HpCB
173-HpCB
174-HpCB
175-HpCB
176-HpCB
177-HpCB
178-HpCB
179-HpCB
180-HpCB
181-HpCB
182-HpCB
183-HpCB
184-HpCB
185-HpCB
186-HpCB
187-HpCB
188-HpCB
189-HpCB
190-HpCB
191-HpCB
192-HpCB
74472-43-8
39635-34-2
74472-44-9
74472-45-0
74472-46-1
41411-63-6
52663-72-6
59291-65-5
32774-16-6
35065-30-6
52663-71-5
52663-74-8
68194-16-1
38411-25-5
40186-70-7
52663-65-7
52663-70-4
52663-67-9
52663-64-6
35065-29-3
74472-47-2
60145-23-5
52663-69-1
74472-48-3
52712-05-7
74472-49-4
52663-68-0
74487-85-7
39635-31-9
41411-64-7
74472-50-7
74472-51-8
Client Sample:
PQL
220
220
220
220
220
220
220
441
220
220
220
220
220
220
220
441
220
220
441
220
220
220
220
220
220
220
220
Page 43 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 7 of 8
SDG Number:6110379
Lab Sample ID:10122004 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 14.4
Date Collected:11/15/2016 12:45
Surrogate/Tracer recovery Recovery%Acceptable Limits
2840
1060
1470
441
3050
300
498
2120
220
220
1060
220
227
220
102000
C180
CU
C
C198
C197
U
U
U
U
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
70.8
76.1
68.4
88.8
78.4
120
109
126
123
90.0
117
116
116
111
123
100
119
118
121
86.1
109
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
10
Run Date:12/08/2016 17:46 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-12 CIS-9-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 1.06 g
Result Nominal
1560
1680
1510
1960
1730
2650
2400
2770
2710
1980
2580
2550
2550
2440
2720
2210
5220
2610
2670
1900
2410
2200
2200
2200
2200
2200
2200
2200
2200
2200
2200
2200
2200
2200
2200
2200
2200
4410
2200
2200
2200
2200
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33474 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d08dec16a-8Data File:
Prep SOP Ref: CF-OA-E-001
193-HpCB
194-OcCB
195-OcCB
196-OcCB
197-OcCB
198-OcCB
199-OcCB
200-OcCB
201-OcCB
202-OcCB
203-OcCB
204-OcCB
205-OcCB
206-NoCB
207-NoCB
208-NoCB
209-DeCB
Total PCB Congeners
69782-91-8
35694-08-7
52663-78-2
42740-50-1
33091-17-7
68194-17-2
52663-75-9
52663-73-7
40186-71-8
2136-99-4
52663-76-0
74472-52-9
74472-53-0
40186-72-9
52663-79-3
52663-77-1
2051-24-3
1336-36-3
Client Sample:
UnitsQual
C
C156L
PQL
220
220
220
441
441
220
220
220
220
220
220
220
220
220
220
Page 44 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 8 of 8
SDG Number:6110379
Lab Sample ID:10122004 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 14.4
Date Collected:11/15/2016 12:45
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
86.8
110
91.1
89.9
106
94.7
111
105
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
10
Run Date:12/08/2016 17:46 Analyst:MJC

Units
6110379-12 CIS-9-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 1.06 g
Result Nominal
1910
2420
2010
1980
2330
2090
2440
2310
2200
2200
2200
2200
2200
2200
2200
2200
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33474 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d08dec16a-8Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
PQL
Page 45 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 1 of 8
SDG Number:6110379
Lab Sample ID:10122005 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 16.5
Date Collected:11/15/2016 13:05
6200
345
1290
4590
278
2420
1040
8060
1030
544
2330
1230
233
5840
2070
2190
4830
575
5210
2350
1570
233
233
390
923
495
3700
1260
U
C
C12
U
C
C
C
U
U
C
C20
C26
C18
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
10
Run Date:12/08/2016 18:52 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-13 CIS-10-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 1.03 g
33474 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d08dec16a-9Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
2-MoCB
3-MoCB
4-DiCB
5-DiCB
6-DiCB
7-DiCB
8-DiCB
9-DiCB
10-DiCB
11-DiCB
12-DiCB
13-DiCB
14-DiCB
15-DiCB
16-TrCB
17-TrCB
18-TrCB
19-TrCB
20-TrCB
21-TrCB
22-TrCB
23-TrCB
24-TrCB
25-TrCB
26-TrCB
27-TrCB
28-TrCB
29-TrCB
30-TrCB
31-TrCB
32-TrCB
2051-60-7
2051-61-8
2051-62-9
13029-08-8
16605-91-7
25569-80-6
33284-50-3
34883-43-7
34883-39-1
33146-45-1
2050-67-1
2974-92-7
2974-90-5
34883-41-5
2050-68-2
38444-78-9
37680-66-3
37680-65-2
38444-73-4
38444-84-7
55702-46-0
38444-85-8
55720-44-0
55702-45-9
55712-37-3
38444-81-4
38444-76-7
7012-37-5
15862-07-4
35693-92-6
16606-02-3
38444-77-8
Client Sample:
PQL
233
233
233
233
233
233
233
233
233
233
2330
465
233
233
233
233
465
233
465
465
233
233
233
233
465
233
233
233
Page 46 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 2 of 8
SDG Number:6110379
Lab Sample ID:10122005 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 16.5
Date Collected:11/15/2016 13:05
233
233
233
1580
233
233
1420
573
759
233
2660
903
356
233
1270
615
3120
233
233
1390
233
233
698
756
4270
233
1280
C21
U
U
U
U
U
C
U
C
C
C44
U
C
C
C45
C50
U
U
U
U
CU
C
C59
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
10
Run Date:12/08/2016 18:52 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-13 CIS-10-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 1.03 g
33474 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d08dec16a-9Data File:
Prep SOP Ref: CF-OA-E-001
33-TrCB
34-TrCB
35-TrCB
36-TrCB
37-TrCB
38-TrCB
39-TrCB
40-TeCB
41-TeCB
42-TeCB
43-TeCB
44-TeCB
45-TeCB
46-TeCB
47-TeCB
48-TeCB
49-TeCB
50-TeCB
51-TeCB
52-TeCB
53-TeCB
54-TeCB
55-TeCB
56-TeCB
57-TeCB
58-TeCB
59-TeCB
60-TeCB
61-TeCB
62-TeCB
63-TeCB
64-TeCB
38444-86-9
37680-68-5
37680-69-6
38444-87-0
38444-90-5
53555-66-1
38444-88-1
38444-93-8
52663-59-9
36559-22-5
70362-46-8
41464-39-5
70362-45-7
41464-47-5
2437-79-8
70362-47-9
41464-40-8
62796-65-0
68194-04-7
35693-99-3
41464-41-9
15968-05-5
74338-24-2
41464-43-1
70424-67-8
41464-49-7
74472-33-6
33025-41-1
33284-53-6
54230-22-7
74472-34-7
52663-58-8
Client Sample:
PQL
233
233
233
233
233
233
465
233
233
233
698
465
233
233
465
465
233
233
233
233
233
233
698
233
930
233
233
Page 47 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 3 of 8
SDG Number:6110379
Lab Sample ID:10122005 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 16.5
Date Collected:11/15/2016 13:05
2110
233
233
233
233
233
233
233
233
233
233
233
419
698
1400
465
233
1600
233
465
233
1450
233
C44
U
U
C49
C61
C40
U
U
C61
C59
C61
U
U
U
U
U
U
U
CU
CU
C86
CU
U
C
C88
U
CU
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
10
Run Date:12/08/2016 18:52 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-13 CIS-10-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 1.03 g
33474 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d08dec16a-9Data File:
Prep SOP Ref: CF-OA-E-001
65-TeCB
66-TeCB
67-TeCB
68-TeCB
69-TeCB
70-TeCB
71-TeCB
72-TeCB
73-TeCB
74-TeCB
75-TeCB
76-TeCB
77-TeCB
78-TeCB
79-TeCB
80-TeCB
81-TeCB
82-PeCB
83-PeCB
84-PeCB
85-PeCB
86-PeCB
87-PeCB
88-PeCB
89-PeCB
90-PeCB
91-PeCB
92-PeCB
93-PeCB
94-PeCB
95-PeCB
96-PeCB
33284-54-7
32598-10-0
73575-53-8
73575-52-7
60233-24-1
32598-11-1
41464-46-4
41464-42-0
74338-23-1
32690-93-0
32598-12-2
70362-48-0
32598-13-3
70362-49-1
41464-48-6
33284-52-5
70362-50-4
52663-62-4
60145-20-2
52663-60-2
65510-45-4
55312-69-1
38380-02-8
55215-17-3
73575-57-2
68194-07-0
68194-05-8
52663-61-3
73575-56-1
73575-55-0
38379-99-6
73575-54-9
Client Sample:
PQL
233
233
233
233
233
233
233
233
233
233
233
233
233
698
1400
465
233
698
233
465
233
233
233
Page 48 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 4 of 8
SDG Number:6110379
Lab Sample ID:10122005 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 16.5
Date Collected:11/15/2016 13:05
465
679
233
233
654
233
233
465
1540
233
233
233
1150
233
233
233
233
233
233
465
C86
CU
C93
C90
C98
U
U
U
U
CU
C86
C
U
U
C90
U
C110
C85
C85
C86
U
U
U
U
C108
C86
U
U
CU
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
10
Run Date:12/08/2016 18:52 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-13 CIS-10-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 1.03 g
33474 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d08dec16a-9Data File:
Prep SOP Ref: CF-OA-E-001
97-PeCB
98-PeCB
99-PeCB
100-PeCB
101-PeCB
102-PeCB
103-PeCB
104-PeCB
105-PeCB
106-PeCB
107-PeCB
108-PeCB
109-PeCB
110-PeCB
111-PeCB
112-PeCB
113-PeCB
114-PeCB
115-PeCB
116-PeCB
117-PeCB
118-PeCB
119-PeCB
120-PeCB
121-PeCB
122-PeCB
123-PeCB
124-PeCB
125-PeCB
126-PeCB
127-PeCB
128-HxCB
41464-51-1
60233-25-2
38380-01-7
39485-83-1
37680-73-2
68194-06-9
60145-21-3
56558-16-8
32598-14-4
70424-69-0
70424-68-9
70362-41-3
74472-35-8
38380-03-9
39635-32-0
74472-36-9
68194-10-5
74472-37-0
74472-38-1
18259-05-7
68194-11-6
31508-00-6
56558-17-9
68194-12-7
56558-18-0
76842-07-4
65510-44-3
70424-70-3
74472-39-2
57465-28-8
39635-33-1
38380-07-3
Client Sample:
PQL
465
233
233
233
233
233
233
465
465
233
233
233
233
233
233
233
233
233
233
465
Page 49 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 5 of 8
SDG Number:6110379
Lab Sample ID:10122005 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 16.5
Date Collected:11/15/2016 13:05
1640
233
233
435
233
233
723
249
233
465
233
233
233
233
233
233
1490
233
233
233
1470
233
233
465
233
233
233
C
U
U
U
U
C
U
C129
CU
C139
U
U
U
U
U
U
C
U
C147
U
C135
U
C
U
U
CU
C156
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
10
Run Date:12/08/2016 18:52 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-13 CIS-10-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 1.03 g
33474 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d08dec16a-9Data File:
Prep SOP Ref: CF-OA-E-001
129-HxCB
130-HxCB
131-HxCB
132-HxCB
133-HxCB
134-HxCB
135-HxCB
136-HxCB
137-HxCB
138-HxCB
139-HxCB
140-HxCB
141-HxCB
142-HxCB
143-HxCB
144-HxCB
145-HxCB
146-HxCB
147-HxCB
148-HxCB
149-HxCB
150-HxCB
151-HxCB
152-HxCB
153-HxCB
154-HxCB
155-HxCB
156-HxCB
157-HxCB
158-HxCB
159-HxCB
160-HxCB
55215-18-4
52663-66-8
61798-70-7
38380-05-1
35694-04-3
52704-70-8
52744-13-5
38411-22-2
35694-06-5
35065-28-2
56030-56-9
59291-64-4
52712-04-6
41411-61-4
68194-15-0
68194-14-9
74472-40-5
51908-16-8
68194-13-8
74472-41-6
38380-04-0
68194-08-1
52663-63-5
68194-09-2
35065-27-1
60145-22-4
33979-03-2
38380-08-4
69782-90-7
74472-42-7
39635-35-3
41411-62-5
Client Sample:
PQL
698
233
233
233
233
233
465
233
233
465
233
233
233
233
233
233
465
233
233
233
465
233
233
465
233
233
233
Page 50 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 6 of 8
SDG Number:6110379
Lab Sample ID:10122005 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 16.5
Date Collected:11/15/2016 13:05
233
233
233
233
233
233
618
465
233
827
233
233
413
233
366
1880
233
233
590
233
233
1190
233
233
233
233
233
U
U
C129
U
U
C128
U
C153
U
CU
U
C171
U
U
U
C
U
U
C
U
C183
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
10
Run Date:12/08/2016 18:52 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-13 CIS-10-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 1.03 g
33474 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d08dec16a-9Data File:
Prep SOP Ref: CF-OA-E-001
161-HxCB
162-HxCB
163-HxCB
164-HxCB
165-HxCB
166-HxCB
167-HxCB
168-HxCB
169-HxCB
170-HpCB
171-HpCB
172-HpCB
173-HpCB
174-HpCB
175-HpCB
176-HpCB
177-HpCB
178-HpCB
179-HpCB
180-HpCB
181-HpCB
182-HpCB
183-HpCB
184-HpCB
185-HpCB
186-HpCB
187-HpCB
188-HpCB
189-HpCB
190-HpCB
191-HpCB
192-HpCB
74472-43-8
39635-34-2
74472-44-9
74472-45-0
74472-46-1
41411-63-6
52663-72-6
59291-65-5
32774-16-6
35065-30-6
52663-71-5
52663-74-8
68194-16-1
38411-25-5
40186-70-7
52663-65-7
52663-70-4
52663-67-9
52663-64-6
35065-29-3
74472-47-2
60145-23-5
52663-69-1
74472-48-3
52712-05-7
74472-49-4
52663-68-0
74487-85-7
39635-31-9
41411-64-7
74472-50-7
74472-51-8
Client Sample:
PQL
233
233
233
233
233
233
233
465
233
233
233
233
233
233
233
465
233
233
465
233
233
233
233
233
233
233
233
Page 51 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 7 of 8
SDG Number:6110379
Lab Sample ID:10122005 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 16.5
Date Collected:11/15/2016 13:05
Surrogate/Tracer recovery Recovery%Acceptable Limits
631
233
291
465
654
233
233
470
233
233
402
233
233
233
103000
C180
U
CU
C
C198
C197
U
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
91.3
92.9
79.4
97.6
111
122
131
118
121
99.8
101
110
114
110
90.8
122
108
106
109
90.4
106
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
10
Run Date:12/08/2016 18:52 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-13 CIS-10-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 1.03 g
Result Nominal
2120
2160
1850
2270
2590
2850
3050
2730
2820
2320
2350
2560
2660
2570
2110
2840
5050
2470
2530
2100
2470
2330
2330
2330
2330
2330
2330
2330
2330
2330
2330
2330
2330
2330
2330
2330
2330
4650
2330
2330
2330
2330
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33474 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d08dec16a-9Data File:
Prep SOP Ref: CF-OA-E-001
193-HpCB
194-OcCB
195-OcCB
196-OcCB
197-OcCB
198-OcCB
199-OcCB
200-OcCB
201-OcCB
202-OcCB
203-OcCB
204-OcCB
205-OcCB
206-NoCB
207-NoCB
208-NoCB
209-DeCB
Total PCB Congeners
69782-91-8
35694-08-7
52663-78-2
42740-50-1
33091-17-7
68194-17-2
52663-75-9
52663-73-7
40186-71-8
2136-99-4
52663-76-0
74472-52-9
74472-53-0
40186-72-9
52663-79-3
52663-77-1
2051-24-3
1336-36-3
Client Sample:
UnitsQual
C
C156L
PQL
233
233
233
465
465
233
233
233
233
233
233
233
233
233
233
Page 52 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 8 of 8
SDG Number:6110379
Lab Sample ID:10122005 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 16.5
Date Collected:11/15/2016 13:05
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
91.9
109
91.5
80.5
116
93.8
124
98.3
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
10
Run Date:12/08/2016 18:52 Analyst:MJC

Units
6110379-13 CIS-10-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 1.03 g
Result Nominal
2140
2530
2130
1870
2690
2180
2870
2290
2330
2330
2330
2330
2330
2330
2330
2330
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33474 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d08dec16a-9Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
PQL
Page 53 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 1 of 8
SDG Number:6110379
Lab Sample ID:10122006 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 14
Date Collected:11/15/2016 13:20
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
16.2
3.24
1.62
1.62
1.62
1.62
3.24
1.62
4.63
3.24
1.94
1.62
1.62
1.62
3.24
1.62
3.89
1.62
U
U
U
U
U
U
U
U
U
U
U
CU
C12
U
U
U
U
CU
U
C
CU
U
U
U
CU
U
C20
C26
C18
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/02/2016 14:36 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-14 CIS-11-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.34 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_3-4Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
2-MoCB
3-MoCB
4-DiCB
5-DiCB
6-DiCB
7-DiCB
8-DiCB
9-DiCB
10-DiCB
11-DiCB
12-DiCB
13-DiCB
14-DiCB
15-DiCB
16-TrCB
17-TrCB
18-TrCB
19-TrCB
20-TrCB
21-TrCB
22-TrCB
23-TrCB
24-TrCB
25-TrCB
26-TrCB
27-TrCB
28-TrCB
29-TrCB
30-TrCB
31-TrCB
32-TrCB
2051-60-7
2051-61-8
2051-62-9
13029-08-8
16605-91-7
25569-80-6
33284-50-3
34883-43-7
34883-39-1
33146-45-1
2050-67-1
2974-92-7
2974-90-5
34883-41-5
2050-68-2
38444-78-9
37680-66-3
37680-65-2
38444-73-4
38444-84-7
55702-46-0
38444-85-8
55720-44-0
55702-45-9
55712-37-3
38444-81-4
38444-76-7
7012-37-5
15862-07-4
35693-92-6
16606-02-3
38444-77-8
Client Sample:
PQL
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
16.2
3.24
1.62
1.62
1.62
1.62
3.24
1.62
3.24
3.24
1.62
1.62
1.62
1.62
3.24
1.62
1.62
1.62
Page 54 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 2 of 8
SDG Number:6110379
Lab Sample ID:10122006 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 14
Date Collected:11/15/2016 13:20
1.62
1.62
1.62
1.81
1.62
1.62
3.24
1.62
1.64
1.62
9.28
3.24
1.62
1.62
4.83
3.24
16.3
1.62
1.62
4.27
1.62
1.62
4.87
2.42
25.3
1.62
3.60
C21
U
U
U
U
U
CU
U
U
C
CU
U
C44
U
C
CU
C45
C50
U
U
U
U
CU
C
C59
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/02/2016 14:36 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-14 CIS-11-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.34 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_3-4Data File:
Prep SOP Ref: CF-OA-E-001
33-TrCB
34-TrCB
35-TrCB
36-TrCB
37-TrCB
38-TrCB
39-TrCB
40-TeCB
41-TeCB
42-TeCB
43-TeCB
44-TeCB
45-TeCB
46-TeCB
47-TeCB
48-TeCB
49-TeCB
50-TeCB
51-TeCB
52-TeCB
53-TeCB
54-TeCB
55-TeCB
56-TeCB
57-TeCB
58-TeCB
59-TeCB
60-TeCB
61-TeCB
62-TeCB
63-TeCB
64-TeCB
38444-86-9
37680-68-5
37680-69-6
38444-87-0
38444-90-5
53555-66-1
38444-88-1
38444-93-8
52663-59-9
36559-22-5
70362-46-8
41464-39-5
70362-45-7
41464-47-5
2437-79-8
70362-47-9
41464-40-8
62796-65-0
68194-04-7
35693-99-3
41464-41-9
15968-05-5
74338-24-2
41464-43-1
70424-67-8
41464-49-7
74472-33-6
33025-41-1
33284-53-6
54230-22-7
74472-34-7
52663-58-8
Client Sample:
PQL
1.62
1.62
1.62
1.62
1.62
1.62
3.24
1.62
1.62
1.62
4.87
3.24
1.62
1.62
3.24
3.24
1.62
1.62
1.62
1.62
1.62
1.62
4.87
1.62
6.49
1.62
1.62
Page 55 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 3 of 8
SDG Number:6110379
Lab Sample ID:10122006 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 14
Date Collected:11/15/2016 13:20
7.25
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
3.61
3.28
8.22
7.39
29.4
3.26
1.62
89.1
10.5
3.24
1.62
50.8
1.62
C44
U
U
C49
C61
C40
U
U
C61
C59
C61
U
U
U
U
U
C
C
C86
C
U
C
C88
CU
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/02/2016 14:36 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-14 CIS-11-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.34 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_3-4Data File:
Prep SOP Ref: CF-OA-E-001
65-TeCB
66-TeCB
67-TeCB
68-TeCB
69-TeCB
70-TeCB
71-TeCB
72-TeCB
73-TeCB
74-TeCB
75-TeCB
76-TeCB
77-TeCB
78-TeCB
79-TeCB
80-TeCB
81-TeCB
82-PeCB
83-PeCB
84-PeCB
85-PeCB
86-PeCB
87-PeCB
88-PeCB
89-PeCB
90-PeCB
91-PeCB
92-PeCB
93-PeCB
94-PeCB
95-PeCB
96-PeCB
33284-54-7
32598-10-0
73575-53-8
73575-52-7
60233-24-1
32598-11-1
41464-46-4
41464-42-0
74338-23-1
32690-93-0
32598-12-2
70362-48-0
32598-13-3
70362-49-1
41464-48-6
33284-52-5
70362-50-4
52663-62-4
60145-20-2
52663-60-2
65510-45-4
55312-69-1
38380-02-8
55215-17-3
73575-57-2
68194-07-0
68194-05-8
52663-61-3
73575-56-1
73575-55-0
38379-99-6
73575-54-9
Client Sample:
PQL
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
4.87
9.73
3.24
1.62
4.87
1.62
3.24
1.62
1.62
1.62
Page 56 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 4 of 8
SDG Number:6110379
Lab Sample ID:10122006 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 14
Date Collected:11/15/2016 13:20
3.24
11.5
1.62
1.62
15.7
1.62
2.00
3.24
61.1
1.62
1.62
1.62
44.0
1.62
1.62
1.62
1.62
1.62
1.62
14.3
C86
CU
C93
C90
C98
U
U
U
CU
C86
C
U
U
C90
U
C110
C85
C85
C86
U
U
U
U
C108
C86
U
U
C
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/02/2016 14:36 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-14 CIS-11-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.34 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_3-4Data File:
Prep SOP Ref: CF-OA-E-001
97-PeCB
98-PeCB
99-PeCB
100-PeCB
101-PeCB
102-PeCB
103-PeCB
104-PeCB
105-PeCB
106-PeCB
107-PeCB
108-PeCB
109-PeCB
110-PeCB
111-PeCB
112-PeCB
113-PeCB
114-PeCB
115-PeCB
116-PeCB
117-PeCB
118-PeCB
119-PeCB
120-PeCB
121-PeCB
122-PeCB
123-PeCB
124-PeCB
125-PeCB
126-PeCB
127-PeCB
128-HxCB
41464-51-1
60233-25-2
38380-01-7
39485-83-1
37680-73-2
68194-06-9
60145-21-3
56558-16-8
32598-14-4
70424-69-0
70424-68-9
70362-41-3
74472-35-8
38380-03-9
39635-32-0
74472-36-9
68194-10-5
74472-37-0
74472-38-1
18259-05-7
68194-11-6
31508-00-6
56558-17-9
68194-12-7
56558-18-0
76842-07-4
65510-44-3
70424-70-3
74472-39-2
57465-28-8
39635-33-1
38380-07-3
Client Sample:
PQL
3.24
1.62
1.62
1.62
1.62
1.62
1.62
3.24
3.24
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
3.24
Page 57 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 5 of 8
SDG Number:6110379
Lab Sample ID:10122006 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 14
Date Collected:11/15/2016 13:20
205
6.28
1.62
63.1
2.08
7.02
102
29.7
4.94
3.24
61.0
1.62
1.62
14.1
1.62
23.1
209
1.62
1.62
1.62
221
1.62
1.62
16.4
18.4
1.62
1.62
C
U
C
C129
CU
C139
U
U
U
C
U
C147
U
C135
U
C
U
U
C
C156
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/02/2016 14:36 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-14 CIS-11-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.34 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_3-4Data File:
Prep SOP Ref: CF-OA-E-001
129-HxCB
130-HxCB
131-HxCB
132-HxCB
133-HxCB
134-HxCB
135-HxCB
136-HxCB
137-HxCB
138-HxCB
139-HxCB
140-HxCB
141-HxCB
142-HxCB
143-HxCB
144-HxCB
145-HxCB
146-HxCB
147-HxCB
148-HxCB
149-HxCB
150-HxCB
151-HxCB
152-HxCB
153-HxCB
154-HxCB
155-HxCB
156-HxCB
157-HxCB
158-HxCB
159-HxCB
160-HxCB
55215-18-4
52663-66-8
61798-70-7
38380-05-1
35694-04-3
52704-70-8
52744-13-5
38411-22-2
35694-06-5
35065-28-2
56030-56-9
59291-64-4
52712-04-6
41411-61-4
68194-15-0
68194-14-9
74472-40-5
51908-16-8
68194-13-8
74472-41-6
38380-04-0
68194-08-1
52663-63-5
68194-09-2
35065-27-1
60145-22-4
33979-03-2
38380-08-4
69782-90-7
74472-42-7
39635-35-3
41411-62-5
Client Sample:
PQL
4.87
1.62
1.62
1.62
1.62
1.62
3.24
1.62
1.62
3.24
1.62
1.62
1.62
1.62
1.62
1.62
3.24
1.62
1.62
1.62
3.24
1.62
1.62
3.24
1.62
1.62
1.62
Page 58 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 6 of 8
SDG Number:6110379
Lab Sample ID:10122006 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 14
Date Collected:11/15/2016 13:20
1.62
1.62
14.1
1.62
5.39
1.62
90.8
30.7
17.3
115
4.51
14.3
59.7
22.0
47.0
252
1.62
1.62
83.9
1.62
1.62
136
1.62
3.31
20.3
3.74
1.62
U
U
C129
U
C128
C153
U
C
C171
C
U
U
C
U
C183
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/02/2016 14:36 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-14 CIS-11-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.34 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_3-4Data File:
Prep SOP Ref: CF-OA-E-001
161-HxCB
162-HxCB
163-HxCB
164-HxCB
165-HxCB
166-HxCB
167-HxCB
168-HxCB
169-HxCB
170-HpCB
171-HpCB
172-HpCB
173-HpCB
174-HpCB
175-HpCB
176-HpCB
177-HpCB
178-HpCB
179-HpCB
180-HpCB
181-HpCB
182-HpCB
183-HpCB
184-HpCB
185-HpCB
186-HpCB
187-HpCB
188-HpCB
189-HpCB
190-HpCB
191-HpCB
192-HpCB
74472-43-8
39635-34-2
74472-44-9
74472-45-0
74472-46-1
41411-63-6
52663-72-6
59291-65-5
32774-16-6
35065-30-6
52663-71-5
52663-74-8
68194-16-1
38411-25-5
40186-70-7
52663-65-7
52663-70-4
52663-67-9
52663-64-6
35065-29-3
74472-47-2
60145-23-5
52663-69-1
74472-48-3
52712-05-7
74472-49-4
52663-68-0
74487-85-7
39635-31-9
41411-64-7
74472-50-7
74472-51-8
Client Sample:
PQL
1.62
1.62
1.62
1.62
1.62
1.62
1.62
3.24
1.62
1.62
1.62
1.62
1.62
1.62
1.62
3.24
1.62
1.62
3.24
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
Page 59 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 7 of 8
SDG Number:6110379
Lab Sample ID:10122006 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 14
Date Collected:11/15/2016 13:20
Surrogate/Tracer recovery Recovery%Acceptable Limits
50.1
20.9
29.4
9.79
62.1
7.49
10.2
37.7
1.62
2.51
13.0
1.97
2.78
1.62
2590
C180
C
C
C198
C197
U
U
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
51.9
56.0
56.8
113
73.1
90.0
56.8
113
112
69.7
94.3
93.3
91.4
94.1
99.1
78.3
93.2
94.0
99.8
67.9
84.5
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/02/2016 14:36 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-14 CIS-11-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.34 g
Result Nominal
84.2
90.8
92.1
183
119
146
92.1
183
182
113
153
151
148
153
161
127
302
153
162
110
137
162
162
162
162
162
162
162
162
162
162
162
162
162
162
162
162
324
162
162
162
162
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d01dec16b_3-4Data File:
Prep SOP Ref: CF-OA-E-001
193-HpCB
194-OcCB
195-OcCB
196-OcCB
197-OcCB
198-OcCB
199-OcCB
200-OcCB
201-OcCB
202-OcCB
203-OcCB
204-OcCB
205-OcCB
206-NoCB
207-NoCB
208-NoCB
209-DeCB
Total PCB Congeners
69782-91-8
35694-08-7
52663-78-2
42740-50-1
33091-17-7
68194-17-2
52663-75-9
52663-73-7
40186-71-8
2136-99-4
52663-76-0
74472-52-9
74472-53-0
40186-72-9
52663-79-3
52663-77-1
2051-24-3
1336-36-3
Client Sample:
UnitsQual
C
C156L
PQL
1.62
1.62
1.62
3.24
3.24
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
1.62
Page 60 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 8 of 8
SDG Number:6110379
Lab Sample ID:10122006 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 14
Date Collected:11/15/2016 13:20
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
71.6
90.5
78.7
73.3
95.8
84.0
60.7
89.3
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/02/2016 14:36 Analyst:MJC

Units
6110379-14 CIS-11-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.34 g
Result Nominal
116
147
128
119
155
136
98.5
145
162
162
162
162
162
162
162
162
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_3-4Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
PQL
Page 61 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 1 of 8
SDG Number:6110379
Lab Sample ID:10122007 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 17.1
Date Collected:11/15/2016 13:20
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
17
3.39
1.7
1.7
1.7
1.7
3.39
1.7
3.39
3.39
1.7
1.7
1.7
1.7
3.39
1.7
1.7
1.7
U
U
U
U
U
U
U
U
U
U
U
CU
C12
U
U
U
U
CU
U
CU
CU
U
U
U
U
CU
U
C20
C26
C18
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 16:30 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-15 CIS-12-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.22 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a-5Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
2-MoCB
3-MoCB
4-DiCB
5-DiCB
6-DiCB
7-DiCB
8-DiCB
9-DiCB
10-DiCB
11-DiCB
12-DiCB
13-DiCB
14-DiCB
15-DiCB
16-TrCB
17-TrCB
18-TrCB
19-TrCB
20-TrCB
21-TrCB
22-TrCB
23-TrCB
24-TrCB
25-TrCB
26-TrCB
27-TrCB
28-TrCB
29-TrCB
30-TrCB
31-TrCB
32-TrCB
2051-60-7
2051-61-8
2051-62-9
13029-08-8
16605-91-7
25569-80-6
33284-50-3
34883-43-7
34883-39-1
33146-45-1
2050-67-1
2974-92-7
2974-90-5
34883-41-5
2050-68-2
38444-78-9
37680-66-3
37680-65-2
38444-73-4
38444-84-7
55702-46-0
38444-85-8
55720-44-0
55702-45-9
55712-37-3
38444-81-4
38444-76-7
7012-37-5
15862-07-4
35693-92-6
16606-02-3
38444-77-8
Client Sample:
PQL
1.70
1.70
1.70
1.70
1.70
1.70
1.70
1.70
1.70
1.70
17.0
3.39
1.70
1.70
1.70
1.70
3.39
1.70
3.39
3.39
1.70
1.70
1.70
1.70
3.39
1.70
1.70
1.70
Page 62 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 2 of 8
SDG Number:6110379
Lab Sample ID:10122007 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 17.1
Date Collected:11/15/2016 13:20
1.7
1.7
1.7
1.7
1.7
1.7
3.39
1.7
1.7
1.7
5.09
3.39
1.7
1.7
3.39
3.39
1.7
1.7
1.7
1.7
1.7
1.7
5.09
1.7
6.78
1.7
1.7
C21
U
U
U
U
U
U
CU
U
U
U
CU
CU
U
C44
U
CU
CU
C45
U
C50
U
U
U
U
U
CU
U
CU
C59
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 16:30 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-15 CIS-12-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.22 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a-5Data File:
Prep SOP Ref: CF-OA-E-001
33-TrCB
34-TrCB
35-TrCB
36-TrCB
37-TrCB
38-TrCB
39-TrCB
40-TeCB
41-TeCB
42-TeCB
43-TeCB
44-TeCB
45-TeCB
46-TeCB
47-TeCB
48-TeCB
49-TeCB
50-TeCB
51-TeCB
52-TeCB
53-TeCB
54-TeCB
55-TeCB
56-TeCB
57-TeCB
58-TeCB
59-TeCB
60-TeCB
61-TeCB
62-TeCB
63-TeCB
64-TeCB
38444-86-9
37680-68-5
37680-69-6
38444-87-0
38444-90-5
53555-66-1
38444-88-1
38444-93-8
52663-59-9
36559-22-5
70362-46-8
41464-39-5
70362-45-7
41464-47-5
2437-79-8
70362-47-9
41464-40-8
62796-65-0
68194-04-7
35693-99-3
41464-41-9
15968-05-5
74338-24-2
41464-43-1
70424-67-8
41464-49-7
74472-33-6
33025-41-1
33284-53-6
54230-22-7
74472-34-7
52663-58-8
Client Sample:
PQL
1.70
1.70
1.70
1.70
1.70
1.70
3.39
1.70
1.70
1.70
5.09
3.39
1.70
1.70
3.39
3.39
1.70
1.70
1.70
1.70
1.70
1.70
5.09
1.70
6.78
1.70
1.70
Page 63 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 3 of 8
SDG Number:6110379
Lab Sample ID:10122007 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 17.1
Date Collected:11/15/2016 13:20
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
5.09
10.2
3.39
1.7
6.46
1.7
3.39
1.7
2.53
1.7
C44
U
U
U
C49
C61
C40
U
U
C61
C59
C61
U
U
U
U
U
U
U
U
CU
CU
C86
CU
U
C
C88
U
CU
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 16:30 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-15 CIS-12-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.22 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a-5Data File:
Prep SOP Ref: CF-OA-E-001
65-TeCB
66-TeCB
67-TeCB
68-TeCB
69-TeCB
70-TeCB
71-TeCB
72-TeCB
73-TeCB
74-TeCB
75-TeCB
76-TeCB
77-TeCB
78-TeCB
79-TeCB
80-TeCB
81-TeCB
82-PeCB
83-PeCB
84-PeCB
85-PeCB
86-PeCB
87-PeCB
88-PeCB
89-PeCB
90-PeCB
91-PeCB
92-PeCB
93-PeCB
94-PeCB
95-PeCB
96-PeCB
33284-54-7
32598-10-0
73575-53-8
73575-52-7
60233-24-1
32598-11-1
41464-46-4
41464-42-0
74338-23-1
32690-93-0
32598-12-2
70362-48-0
32598-13-3
70362-49-1
41464-48-6
33284-52-5
70362-50-4
52663-62-4
60145-20-2
52663-60-2
65510-45-4
55312-69-1
38380-02-8
55215-17-3
73575-57-2
68194-07-0
68194-05-8
52663-61-3
73575-56-1
73575-55-0
38379-99-6
73575-54-9
Client Sample:
PQL
1.70
1.70
1.70
1.70
1.70
1.70
1.70
1.70
1.70
1.70
1.70
1.70
1.70
5.09
10.2
3.39
1.70
5.09
1.70
3.39
1.70
1.70
1.70
Page 64 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 4 of 8
SDG Number:6110379
Lab Sample ID:10122007 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 17.1
Date Collected:11/15/2016 13:20
3.39
2.36
1.7
1.7
4.20
1.7
1.7
3.39
9.60
1.7
1.7
1.7
9.13
1.7
1.7
1.7
1.7
1.7
1.7
3.39
C86
CU
C93
C90
C98
U
U
U
U
CU
C86
C
U
U
C90
U
C110
C85
C85
C86
U
U
U
U
C108
C86
U
U
CU
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 16:30 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-15 CIS-12-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.22 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a-5Data File:
Prep SOP Ref: CF-OA-E-001
97-PeCB
98-PeCB
99-PeCB
100-PeCB
101-PeCB
102-PeCB
103-PeCB
104-PeCB
105-PeCB
106-PeCB
107-PeCB
108-PeCB
109-PeCB
110-PeCB
111-PeCB
112-PeCB
113-PeCB
114-PeCB
115-PeCB
116-PeCB
117-PeCB
118-PeCB
119-PeCB
120-PeCB
121-PeCB
122-PeCB
123-PeCB
124-PeCB
125-PeCB
126-PeCB
127-PeCB
128-HxCB
41464-51-1
60233-25-2
38380-01-7
39485-83-1
37680-73-2
68194-06-9
60145-21-3
56558-16-8
32598-14-4
70424-69-0
70424-68-9
70362-41-3
74472-35-8
38380-03-9
39635-32-0
74472-36-9
68194-10-5
74472-37-0
74472-38-1
18259-05-7
68194-11-6
31508-00-6
56558-17-9
68194-12-7
56558-18-0
76842-07-4
65510-44-3
70424-70-3
74472-39-2
57465-28-8
39635-33-1
38380-07-3
Client Sample:
PQL
3.39
1.70
1.70
1.70
1.70
1.70
1.70
3.39
3.39
1.70
1.70
1.70
1.70
1.70
1.70
1.70
1.70
1.70
1.70
3.39
Page 65 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 5 of 8
SDG Number:6110379
Lab Sample ID:10122007 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 17.1
Date Collected:11/15/2016 13:20
16.5
1.7
1.7
4.87
1.7
1.7
4.37
1.7
1.7
3.39
3.34
1.7
1.7
1.7
1.7
1.7
9.95
1.7
1.7
1.7
12.8
1.7
1.7
3.39
1.82
1.7
1.7
C
U
U
U
U
C
U
U
C129
CU
C139
U
U
U
U
U
C
U
C147
U
C135
U
C
U
U
CU
C156
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 16:30 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-15 CIS-12-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.22 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a-5Data File:
Prep SOP Ref: CF-OA-E-001
129-HxCB
130-HxCB
131-HxCB
132-HxCB
133-HxCB
134-HxCB
135-HxCB
136-HxCB
137-HxCB
138-HxCB
139-HxCB
140-HxCB
141-HxCB
142-HxCB
143-HxCB
144-HxCB
145-HxCB
146-HxCB
147-HxCB
148-HxCB
149-HxCB
150-HxCB
151-HxCB
152-HxCB
153-HxCB
154-HxCB
155-HxCB
156-HxCB
157-HxCB
158-HxCB
159-HxCB
160-HxCB
55215-18-4
52663-66-8
61798-70-7
38380-05-1
35694-04-3
52704-70-8
52744-13-5
38411-22-2
35694-06-5
35065-28-2
56030-56-9
59291-64-4
52712-04-6
41411-61-4
68194-15-0
68194-14-9
74472-40-5
51908-16-8
68194-13-8
74472-41-6
38380-04-0
68194-08-1
52663-63-5
68194-09-2
35065-27-1
60145-22-4
33979-03-2
38380-08-4
69782-90-7
74472-42-7
39635-35-3
41411-62-5
Client Sample:
PQL
5.09
1.70
1.70
1.70
1.70
1.70
3.39
1.70
1.70
3.39
1.70
1.70
1.70
1.70
1.70
1.70
3.39
1.70
1.70
1.70
3.39
1.70
1.70
3.39
1.70
1.70
1.70
Page 66 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 6 of 8
SDG Number:6110379
Lab Sample ID:10122007 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 17.1
Date Collected:11/15/2016 13:20
1.7
1.7
1.7
1.7
1.7
1.7
5.55
3.39
1.7
6.48
1.7
1.7
3.36
1.7
2.11
14.1
1.7
1.7
4.55
1.7
1.7
7.50
1.7
1.7
1.7
1.7
1.7
U
U
C129
U
U
C128
U
C153
U
CU
U
C171
U
U
U
C
U
U
C
U
C183
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 16:30 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-15 CIS-12-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.22 g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a-5Data File:
Prep SOP Ref: CF-OA-E-001
161-HxCB
162-HxCB
163-HxCB
164-HxCB
165-HxCB
166-HxCB
167-HxCB
168-HxCB
169-HxCB
170-HpCB
171-HpCB
172-HpCB
173-HpCB
174-HpCB
175-HpCB
176-HpCB
177-HpCB
178-HpCB
179-HpCB
180-HpCB
181-HpCB
182-HpCB
183-HpCB
184-HpCB
185-HpCB
186-HpCB
187-HpCB
188-HpCB
189-HpCB
190-HpCB
191-HpCB
192-HpCB
74472-43-8
39635-34-2
74472-44-9
74472-45-0
74472-46-1
41411-63-6
52663-72-6
59291-65-5
32774-16-6
35065-30-6
52663-71-5
52663-74-8
68194-16-1
38411-25-5
40186-70-7
52663-65-7
52663-70-4
52663-67-9
52663-64-6
35065-29-3
74472-47-2
60145-23-5
52663-69-1
74472-48-3
52712-05-7
74472-49-4
52663-68-0
74487-85-7
39635-31-9
41411-64-7
74472-50-7
74472-51-8
Client Sample:
PQL
1.70
1.70
1.70
1.70
1.70
1.70
1.70
3.39
1.70
1.70
1.70
1.70
1.70
1.70
1.70
3.39
1.70
1.70
3.39
1.70
1.70
1.70
1.70
1.70
1.70
1.70
1.70
Page 67 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 7 of 8
SDG Number:6110379
Lab Sample ID:10122007 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 17.1
Date Collected:11/15/2016 13:20
Surrogate/Tracer recovery Recovery%Acceptable Limits
2.99
1.7
1.83
3.39
3.73
1.7
1.7
2.25
1.7
1.7
1.7
1.7
1.7
1.7
142
C180
U
CU
C
C198
C197
U
U
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
41.9
50.8
53.6
99.7
73.1
108
65.3
140
141
69.0
111
108
105
108
123
75.7
103
103
112
61.7
88.0
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 16:30 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-15 CIS-12-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.22 g
Result Nominal
71.1
86.1
90.9
169
124
184
111
237
239
117
189
182
178
183
209
128
351
174
189
105
149
170
170
170
170
170
170
170
170
170
170
170
170
170
170
170
170
339
170
170
170
170
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d06dec16a-5Data File:
Prep SOP Ref: CF-OA-E-001
193-HpCB
194-OcCB
195-OcCB
196-OcCB
197-OcCB
198-OcCB
199-OcCB
200-OcCB
201-OcCB
202-OcCB
203-OcCB
204-OcCB
205-OcCB
206-NoCB
207-NoCB
208-NoCB
209-DeCB
Total PCB Congeners
69782-91-8
35694-08-7
52663-78-2
42740-50-1
33091-17-7
68194-17-2
52663-75-9
52663-73-7
40186-71-8
2136-99-4
52663-76-0
74472-52-9
74472-53-0
40186-72-9
52663-79-3
52663-77-1
2051-24-3
1336-36-3
Client Sample:
UnitsQual
C
C156L
PQL
1.70
1.70
1.70
3.39
3.39
1.70
1.70
1.70
1.70
1.70
1.70
1.70
1.70
1.70
1.70
Page 68 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 8 of 8
SDG Number:6110379
Lab Sample ID:10122007 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 17.1
Date Collected:11/15/2016 13:20
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
69.5
99.3
87.8
75.7
107
88.3
63.3
92.6
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 16:30 Analyst:MJC

Units
6110379-15 CIS-12-SB
1668A Soil
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.22 g
Result Nominal
118
168
149
128
181
150
107
157
170
170
170
170
170
170
170
170
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a-5Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
PQL
Page 69 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 1 of 8
SDG Number:6110379
Lab Sample ID:10122008 Matrix:WATER
Date Received:11/19/2016 09:50
Date Collected:11/15/2016 10:20
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
103
41.3
20.6
20.6
20.6
20.6
41.3
20.6
41.3
41.3
20.6
20.6
20.6
20.6
41.3
20.6
20.6
20.6
U
U
U
U
U
U
U
U
U
U
U
CU
C12
U
U
U
U
CU
U
CU
CU
U
U
U
U
CU
U
C20
C26
C18
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/04/2016 02:29 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
6110379-17 CIS-3-EB
1668A Water
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 969.6 mL
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_6-6Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
2-MoCB
3-MoCB
4-DiCB
5-DiCB
6-DiCB
7-DiCB
8-DiCB
9-DiCB
10-DiCB
11-DiCB
12-DiCB
13-DiCB
14-DiCB
15-DiCB
16-TrCB
17-TrCB
18-TrCB
19-TrCB
20-TrCB
21-TrCB
22-TrCB
23-TrCB
24-TrCB
25-TrCB
26-TrCB
27-TrCB
28-TrCB
29-TrCB
30-TrCB
31-TrCB
32-TrCB
2051-60-7
2051-61-8
2051-62-9
13029-08-8
16605-91-7
25569-80-6
33284-50-3
34883-43-7
34883-39-1
33146-45-1
2050-67-1
2974-92-7
2974-90-5
34883-41-5
2050-68-2
38444-78-9
37680-66-3
37680-65-2
38444-73-4
38444-84-7
55702-46-0
38444-85-8
55720-44-0
55702-45-9
55712-37-3
38444-81-4
38444-76-7
7012-37-5
15862-07-4
35693-92-6
16606-02-3
38444-77-8
Client Sample:
PQL
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
103
41.3
20.6
20.6
20.6
20.6
41.3
20.6
41.3
41.3
20.6
20.6
20.6
20.6
41.3
20.6
20.6
20.6
Page 70 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 2 of 8
SDG Number:6110379
Lab Sample ID:10122008 Matrix:WATER
Date Received:11/19/2016 09:50
Date Collected:11/15/2016 10:20
20.6
20.6
20.6
20.6
20.6
20.6
41.3
20.6
20.6
20.6
61.9
41.3
20.6
20.6
41.3
41.3
20.6
20.6
20.6
20.6
20.6
20.6
61.9
20.6
82.5
20.6
20.6
C21
U
U
U
U
U
U
CU
U
U
U
CU
CU
U
C44
U
CU
CU
C45
U
C50
U
U
U
U
U
CU
U
CU
C59
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/04/2016 02:29 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
6110379-17 CIS-3-EB
1668A Water
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 969.6 mL
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_6-6Data File:
Prep SOP Ref: CF-OA-E-001
33-TrCB
34-TrCB
35-TrCB
36-TrCB
37-TrCB
38-TrCB
39-TrCB
40-TeCB
41-TeCB
42-TeCB
43-TeCB
44-TeCB
45-TeCB
46-TeCB
47-TeCB
48-TeCB
49-TeCB
50-TeCB
51-TeCB
52-TeCB
53-TeCB
54-TeCB
55-TeCB
56-TeCB
57-TeCB
58-TeCB
59-TeCB
60-TeCB
61-TeCB
62-TeCB
63-TeCB
64-TeCB
38444-86-9
37680-68-5
37680-69-6
38444-87-0
38444-90-5
53555-66-1
38444-88-1
38444-93-8
52663-59-9
36559-22-5
70362-46-8
41464-39-5
70362-45-7
41464-47-5
2437-79-8
70362-47-9
41464-40-8
62796-65-0
68194-04-7
35693-99-3
41464-41-9
15968-05-5
74338-24-2
41464-43-1
70424-67-8
41464-49-7
74472-33-6
33025-41-1
33284-53-6
54230-22-7
74472-34-7
52663-58-8
Client Sample:
PQL
20.6
20.6
20.6
20.6
20.6
20.6
41.3
20.6
20.6
20.6
61.9
41.3
20.6
20.6
41.3
41.3
20.6
20.6
20.6
20.6
20.6
20.6
61.9
20.6
82.5
20.6
20.6
Page 71 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 3 of 8
SDG Number:6110379
Lab Sample ID:10122008 Matrix:WATER
Date Received:11/19/2016 09:50
Date Collected:11/15/2016 10:20
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
61.9
124
41.3
20.6
61.9
20.6
41.3
20.6
20.6
20.6
C44
U
U
U
C49
C61
C40
U
U
C61
C59
C61
U
U
U
U
U
U
U
U
CU
CU
C86
CU
U
CU
C88
U
CU
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/04/2016 02:29 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
6110379-17 CIS-3-EB
1668A Water
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 969.6 mL
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_6-6Data File:
Prep SOP Ref: CF-OA-E-001
65-TeCB
66-TeCB
67-TeCB
68-TeCB
69-TeCB
70-TeCB
71-TeCB
72-TeCB
73-TeCB
74-TeCB
75-TeCB
76-TeCB
77-TeCB
78-TeCB
79-TeCB
80-TeCB
81-TeCB
82-PeCB
83-PeCB
84-PeCB
85-PeCB
86-PeCB
87-PeCB
88-PeCB
89-PeCB
90-PeCB
91-PeCB
92-PeCB
93-PeCB
94-PeCB
95-PeCB
96-PeCB
33284-54-7
32598-10-0
73575-53-8
73575-52-7
60233-24-1
32598-11-1
41464-46-4
41464-42-0
74338-23-1
32690-93-0
32598-12-2
70362-48-0
32598-13-3
70362-49-1
41464-48-6
33284-52-5
70362-50-4
52663-62-4
60145-20-2
52663-60-2
65510-45-4
55312-69-1
38380-02-8
55215-17-3
73575-57-2
68194-07-0
68194-05-8
52663-61-3
73575-56-1
73575-55-0
38379-99-6
73575-54-9
Client Sample:
PQL
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
61.9
124
41.3
20.6
61.9
20.6
41.3
20.6
20.6
20.6
Page 72 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 4 of 8
SDG Number:6110379
Lab Sample ID:10122008 Matrix:WATER
Date Received:11/19/2016 09:50
Date Collected:11/15/2016 10:20
41.3
20.6
20.6
20.6
20.6
20.6
20.6
41.3
41.3
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
41.3
C86
CU
U
C93
C90
C98
U
U
U
U
U
CU
C86
CU
U
U
C90
U
C110
C85
C85
U
C86
U
U
U
U
C108
C86
U
U
CU
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/04/2016 02:29 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
6110379-17 CIS-3-EB
1668A Water
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 969.6 mL
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_6-6Data File:
Prep SOP Ref: CF-OA-E-001
97-PeCB
98-PeCB
99-PeCB
100-PeCB
101-PeCB
102-PeCB
103-PeCB
104-PeCB
105-PeCB
106-PeCB
107-PeCB
108-PeCB
109-PeCB
110-PeCB
111-PeCB
112-PeCB
113-PeCB
114-PeCB
115-PeCB
116-PeCB
117-PeCB
118-PeCB
119-PeCB
120-PeCB
121-PeCB
122-PeCB
123-PeCB
124-PeCB
125-PeCB
126-PeCB
127-PeCB
128-HxCB
41464-51-1
60233-25-2
38380-01-7
39485-83-1
37680-73-2
68194-06-9
60145-21-3
56558-16-8
32598-14-4
70424-69-0
70424-68-9
70362-41-3
74472-35-8
38380-03-9
39635-32-0
74472-36-9
68194-10-5
74472-37-0
74472-38-1
18259-05-7
68194-11-6
31508-00-6
56558-17-9
68194-12-7
56558-18-0
76842-07-4
65510-44-3
70424-70-3
74472-39-2
57465-28-8
39635-33-1
38380-07-3
Client Sample:
PQL
41.3
20.6
20.6
20.6
20.6
20.6
20.6
41.3
41.3
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
41.3
Page 73 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 5 of 8
SDG Number:6110379
Lab Sample ID:10122008 Matrix:WATER
Date Received:11/19/2016 09:50
Date Collected:11/15/2016 10:20
61.9
20.6
20.6
20.6
20.6
20.6
41.3
20.6
20.6
41.3
20.6
20.6
20.6
20.6
20.6
20.6
41.3
20.6
20.6
20.6
41.3
20.6
20.6
41.3
20.6
20.6
20.6
CU
U
U
U
U
U
CU
U
U
C129
CU
C139
U
U
U
U
U
U
CU
U
C147
U
C135
U
CU
U
U
CU
C156
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/04/2016 02:29 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
6110379-17 CIS-3-EB
1668A Water
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 969.6 mL
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_6-6Data File:
Prep SOP Ref: CF-OA-E-001
129-HxCB
130-HxCB
131-HxCB
132-HxCB
133-HxCB
134-HxCB
135-HxCB
136-HxCB
137-HxCB
138-HxCB
139-HxCB
140-HxCB
141-HxCB
142-HxCB
143-HxCB
144-HxCB
145-HxCB
146-HxCB
147-HxCB
148-HxCB
149-HxCB
150-HxCB
151-HxCB
152-HxCB
153-HxCB
154-HxCB
155-HxCB
156-HxCB
157-HxCB
158-HxCB
159-HxCB
160-HxCB
55215-18-4
52663-66-8
61798-70-7
38380-05-1
35694-04-3
52704-70-8
52744-13-5
38411-22-2
35694-06-5
35065-28-2
56030-56-9
59291-64-4
52712-04-6
41411-61-4
68194-15-0
68194-14-9
74472-40-5
51908-16-8
68194-13-8
74472-41-6
38380-04-0
68194-08-1
52663-63-5
68194-09-2
35065-27-1
60145-22-4
33979-03-2
38380-08-4
69782-90-7
74472-42-7
39635-35-3
41411-62-5
Client Sample:
PQL
61.9
20.6
20.6
20.6
20.6
20.6
41.3
20.6
20.6
41.3
20.6
20.6
20.6
20.6
20.6
20.6
41.3
20.6
20.6
20.6
41.3
20.6
20.6
41.3
20.6
20.6
20.6
Page 74 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 6 of 8
SDG Number:6110379
Lab Sample ID:10122008 Matrix:WATER
Date Received:11/19/2016 09:50
Date Collected:11/15/2016 10:20
20.6
20.6
20.6
20.6
20.6
20.6
20.6
41.3
20.6
20.6
20.6
20.6
20.6
20.6
20.6
41.3
20.6
20.6
41.3
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
U
U
C129
U
U
C128
U
C153
U
U
CU
U
C171
U
U
U
U
U
U
CU
U
U
CU
U
C183
U
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/04/2016 02:29 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
6110379-17 CIS-3-EB
1668A Water
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 969.6 mL
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_6-6Data File:
Prep SOP Ref: CF-OA-E-001
161-HxCB
162-HxCB
163-HxCB
164-HxCB
165-HxCB
166-HxCB
167-HxCB
168-HxCB
169-HxCB
170-HpCB
171-HpCB
172-HpCB
173-HpCB
174-HpCB
175-HpCB
176-HpCB
177-HpCB
178-HpCB
179-HpCB
180-HpCB
181-HpCB
182-HpCB
183-HpCB
184-HpCB
185-HpCB
186-HpCB
187-HpCB
188-HpCB
189-HpCB
190-HpCB
191-HpCB
192-HpCB
74472-43-8
39635-34-2
74472-44-9
74472-45-0
74472-46-1
41411-63-6
52663-72-6
59291-65-5
32774-16-6
35065-30-6
52663-71-5
52663-74-8
68194-16-1
38411-25-5
40186-70-7
52663-65-7
52663-70-4
52663-67-9
52663-64-6
35065-29-3
74472-47-2
60145-23-5
52663-69-1
74472-48-3
52712-05-7
74472-49-4
52663-68-0
74487-85-7
39635-31-9
41411-64-7
74472-50-7
74472-51-8
Client Sample:
PQL
20.6
20.6
20.6
20.6
20.6
20.6
20.6
41.3
20.6
20.6
20.6
20.6
20.6
20.6
20.6
41.3
20.6
20.6
41.3
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
Page 75 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 7 of 8
SDG Number:6110379
Lab Sample ID:10122008 Matrix:WATER
Date Received:11/19/2016 09:50
Date Collected:11/15/2016 10:20
Surrogate/Tracer recovery Recovery%Acceptable Limits
20.6
20.6
20.6
41.3
41.3
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
C180
U
U
U
CU
CU
C198
C197
U
U
U
U
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
56.0
60.0
61.8
97.6
72.4
99.4
68.4
122
123
73.5
105
103
101
106
111
83.5
101
102
109
66.9
87.2
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/04/2016 02:29 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
6110379-17 CIS-3-EB
1668A Water
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 969.6 mL
Result Nominal
1160
1240
1270
2010
1490
2050
1410
2520
2530
1520
2160
2130
2090
2180
2280
1720
4190
2110
2250
1380
1800
2060
2060
2060
2060
2060
2060
2060
2060
2060
2060
2060
2060
2060
2060
2060
2060
4130
2060
2060
2060
2060
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d01dec16b_6-6Data File:
Prep SOP Ref: CF-OA-E-001
193-HpCB
194-OcCB
195-OcCB
196-OcCB
197-OcCB
198-OcCB
199-OcCB
200-OcCB
201-OcCB
202-OcCB
203-OcCB
204-OcCB
205-OcCB
206-NoCB
207-NoCB
208-NoCB
209-DeCB
Total PCB Congeners
69782-91-8
35694-08-7
52663-78-2
42740-50-1
33091-17-7
68194-17-2
52663-75-9
52663-73-7
40186-71-8
2136-99-4
52663-76-0
74472-52-9
74472-53-0
40186-72-9
52663-79-3
52663-77-1
2051-24-3
1336-36-3
Client Sample:
UnitsQual
C
C156L
PQL
20.6
20.6
20.6
41.3
41.3
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
20.6
Page 76 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 8 of 8
SDG Number:6110379
Lab Sample ID:10122008 Matrix:WATER
Date Received:11/19/2016 09:50
Date Collected:11/15/2016 10:20
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-28-TrCB
13C-111-PeCB
13C-178-HpCB
71.0
99.4
86.3
72.9
108
73.6
92.7
103
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/04/2016 02:29 Analyst:MJC

Units
6110379-17 CIS-3-EB
1668A Water
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 969.6 mL
Result Nominal
1470
2050
1780
1500
2230
1520
1910
2130
2060
2060
2060
2060
2060
2060
2060
2060
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_6-6Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
PQL
Page 77 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 1 of 8
SDG Number:6110379
Lab Sample ID:10122009 Matrix:WATER
Date Received:11/19/2016 09:50
Date Collected:11/15/2016 12:00
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
101
40.5
20.3
20.3
20.3
20.3
40.5
20.3
40.5
40.5
20.3
20.3
20.3
20.3
40.5
20.3
20.3
20.3
U
U
U
U
U
U
U
U
U
U
U
CU
C12
U
U
U
U
CU
U
CU
CU
U
U
U
U
CU
U
C20
C26
C18
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/04/2016 03:35 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
6110379-18 CIS-4-FB
1668A Water
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 987 mL
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_6-7Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
2-MoCB
3-MoCB
4-DiCB
5-DiCB
6-DiCB
7-DiCB
8-DiCB
9-DiCB
10-DiCB
11-DiCB
12-DiCB
13-DiCB
14-DiCB
15-DiCB
16-TrCB
17-TrCB
18-TrCB
19-TrCB
20-TrCB
21-TrCB
22-TrCB
23-TrCB
24-TrCB
25-TrCB
26-TrCB
27-TrCB
28-TrCB
29-TrCB
30-TrCB
31-TrCB
32-TrCB
2051-60-7
2051-61-8
2051-62-9
13029-08-8
16605-91-7
25569-80-6
33284-50-3
34883-43-7
34883-39-1
33146-45-1
2050-67-1
2974-92-7
2974-90-5
34883-41-5
2050-68-2
38444-78-9
37680-66-3
37680-65-2
38444-73-4
38444-84-7
55702-46-0
38444-85-8
55720-44-0
55702-45-9
55712-37-3
38444-81-4
38444-76-7
7012-37-5
15862-07-4
35693-92-6
16606-02-3
38444-77-8
Client Sample:
PQL
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
101
40.5
20.3
20.3
20.3
20.3
40.5
20.3
40.5
40.5
20.3
20.3
20.3
20.3
40.5
20.3
20.3
20.3
Page 78 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 2 of 8
SDG Number:6110379
Lab Sample ID:10122009 Matrix:WATER
Date Received:11/19/2016 09:50
Date Collected:11/15/2016 12:00
20.3
20.3
20.3
20.3
20.3
20.3
40.5
20.3
20.3
20.3
60.8
40.5
20.3
20.3
40.5
40.5
20.3
20.3
20.3
20.3
20.3
20.3
60.8
20.3
81.1
20.3
20.3
C21
U
U
U
U
U
U
CU
U
U
U
CU
CU
U
C44
U
CU
CU
C45
U
C50
U
U
U
U
U
CU
U
CU
C59
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/04/2016 03:35 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
6110379-18 CIS-4-FB
1668A Water
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 987 mL
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_6-7Data File:
Prep SOP Ref: CF-OA-E-001
33-TrCB
34-TrCB
35-TrCB
36-TrCB
37-TrCB
38-TrCB
39-TrCB
40-TeCB
41-TeCB
42-TeCB
43-TeCB
44-TeCB
45-TeCB
46-TeCB
47-TeCB
48-TeCB
49-TeCB
50-TeCB
51-TeCB
52-TeCB
53-TeCB
54-TeCB
55-TeCB
56-TeCB
57-TeCB
58-TeCB
59-TeCB
60-TeCB
61-TeCB
62-TeCB
63-TeCB
64-TeCB
38444-86-9
37680-68-5
37680-69-6
38444-87-0
38444-90-5
53555-66-1
38444-88-1
38444-93-8
52663-59-9
36559-22-5
70362-46-8
41464-39-5
70362-45-7
41464-47-5
2437-79-8
70362-47-9
41464-40-8
62796-65-0
68194-04-7
35693-99-3
41464-41-9
15968-05-5
74338-24-2
41464-43-1
70424-67-8
41464-49-7
74472-33-6
33025-41-1
33284-53-6
54230-22-7
74472-34-7
52663-58-8
Client Sample:
PQL
20.3
20.3
20.3
20.3
20.3
20.3
40.5
20.3
20.3
20.3
60.8
40.5
20.3
20.3
40.5
40.5
20.3
20.3
20.3
20.3
20.3
20.3
60.8
20.3
81.1
20.3
20.3
Page 79 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 3 of 8
SDG Number:6110379
Lab Sample ID:10122009 Matrix:WATER
Date Received:11/19/2016 09:50
Date Collected:11/15/2016 12:00
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
60.8
122
40.5
20.3
60.8
20.3
40.5
20.3
20.3
20.3
C44
U
U
U
C49
C61
C40
U
U
C61
C59
C61
U
U
U
U
U
U
U
U
CU
CU
C86
CU
U
CU
C88
U
CU
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/04/2016 03:35 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
6110379-18 CIS-4-FB
1668A Water
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 987 mL
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_6-7Data File:
Prep SOP Ref: CF-OA-E-001
65-TeCB
66-TeCB
67-TeCB
68-TeCB
69-TeCB
70-TeCB
71-TeCB
72-TeCB
73-TeCB
74-TeCB
75-TeCB
76-TeCB
77-TeCB
78-TeCB
79-TeCB
80-TeCB
81-TeCB
82-PeCB
83-PeCB
84-PeCB
85-PeCB
86-PeCB
87-PeCB
88-PeCB
89-PeCB
90-PeCB
91-PeCB
92-PeCB
93-PeCB
94-PeCB
95-PeCB
96-PeCB
33284-54-7
32598-10-0
73575-53-8
73575-52-7
60233-24-1
32598-11-1
41464-46-4
41464-42-0
74338-23-1
32690-93-0
32598-12-2
70362-48-0
32598-13-3
70362-49-1
41464-48-6
33284-52-5
70362-50-4
52663-62-4
60145-20-2
52663-60-2
65510-45-4
55312-69-1
38380-02-8
55215-17-3
73575-57-2
68194-07-0
68194-05-8
52663-61-3
73575-56-1
73575-55-0
38379-99-6
73575-54-9
Client Sample:
PQL
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
60.8
122
40.5
20.3
60.8
20.3
40.5
20.3
20.3
20.3
Page 80 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 4 of 8
SDG Number:6110379
Lab Sample ID:10122009 Matrix:WATER
Date Received:11/19/2016 09:50
Date Collected:11/15/2016 12:00
40.5
20.3
20.3
20.3
20.3
20.3
20.3
40.5
40.5
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
40.5
C86
CU
U
C93
C90
C98
U
U
U
U
U
CU
C86
CU
U
U
C90
U
C110
C85
C85
U
C86
U
U
U
U
C108
C86
U
U
CU
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/04/2016 03:35 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
6110379-18 CIS-4-FB
1668A Water
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 987 mL
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_6-7Data File:
Prep SOP Ref: CF-OA-E-001
97-PeCB
98-PeCB
99-PeCB
100-PeCB
101-PeCB
102-PeCB
103-PeCB
104-PeCB
105-PeCB
106-PeCB
107-PeCB
108-PeCB
109-PeCB
110-PeCB
111-PeCB
112-PeCB
113-PeCB
114-PeCB
115-PeCB
116-PeCB
117-PeCB
118-PeCB
119-PeCB
120-PeCB
121-PeCB
122-PeCB
123-PeCB
124-PeCB
125-PeCB
126-PeCB
127-PeCB
128-HxCB
41464-51-1
60233-25-2
38380-01-7
39485-83-1
37680-73-2
68194-06-9
60145-21-3
56558-16-8
32598-14-4
70424-69-0
70424-68-9
70362-41-3
74472-35-8
38380-03-9
39635-32-0
74472-36-9
68194-10-5
74472-37-0
74472-38-1
18259-05-7
68194-11-6
31508-00-6
56558-17-9
68194-12-7
56558-18-0
76842-07-4
65510-44-3
70424-70-3
74472-39-2
57465-28-8
39635-33-1
38380-07-3
Client Sample:
PQL
40.5
20.3
20.3
20.3
20.3
20.3
20.3
40.5
40.5
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
40.5
Page 81 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 5 of 8
SDG Number:6110379
Lab Sample ID:10122009 Matrix:WATER
Date Received:11/19/2016 09:50
Date Collected:11/15/2016 12:00
60.8
20.3
20.3
20.3
20.3
20.3
40.5
20.3
20.3
40.5
20.3
20.3
20.3
20.3
20.3
20.3
40.5
20.3
20.3
20.3
40.5
20.3
20.3
40.5
20.3
20.3
20.3
CU
U
U
U
U
U
CU
U
U
C129
CU
C139
U
U
U
U
U
U
CU
U
C147
U
C135
U
CU
U
U
CU
C156
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/04/2016 03:35 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
6110379-18 CIS-4-FB
1668A Water
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 987 mL
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_6-7Data File:
Prep SOP Ref: CF-OA-E-001
129-HxCB
130-HxCB
131-HxCB
132-HxCB
133-HxCB
134-HxCB
135-HxCB
136-HxCB
137-HxCB
138-HxCB
139-HxCB
140-HxCB
141-HxCB
142-HxCB
143-HxCB
144-HxCB
145-HxCB
146-HxCB
147-HxCB
148-HxCB
149-HxCB
150-HxCB
151-HxCB
152-HxCB
153-HxCB
154-HxCB
155-HxCB
156-HxCB
157-HxCB
158-HxCB
159-HxCB
160-HxCB
55215-18-4
52663-66-8
61798-70-7
38380-05-1
35694-04-3
52704-70-8
52744-13-5
38411-22-2
35694-06-5
35065-28-2
56030-56-9
59291-64-4
52712-04-6
41411-61-4
68194-15-0
68194-14-9
74472-40-5
51908-16-8
68194-13-8
74472-41-6
38380-04-0
68194-08-1
52663-63-5
68194-09-2
35065-27-1
60145-22-4
33979-03-2
38380-08-4
69782-90-7
74472-42-7
39635-35-3
41411-62-5
Client Sample:
PQL
60.8
20.3
20.3
20.3
20.3
20.3
40.5
20.3
20.3
40.5
20.3
20.3
20.3
20.3
20.3
20.3
40.5
20.3
20.3
20.3
40.5
20.3
20.3
40.5
20.3
20.3
20.3
Page 82 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 6 of 8
SDG Number:6110379
Lab Sample ID:10122009 Matrix:WATER
Date Received:11/19/2016 09:50
Date Collected:11/15/2016 12:00
20.3
20.3
20.3
20.3
20.3
20.3
20.3
40.5
20.3
20.3
20.3
20.3
20.3
20.3
20.3
40.5
20.3
20.3
40.5
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
U
U
C129
U
U
C128
U
C153
U
U
CU
U
C171
U
U
U
U
U
U
CU
U
U
CU
U
C183
U
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/04/2016 03:35 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
6110379-18 CIS-4-FB
1668A Water
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 987 mL
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_6-7Data File:
Prep SOP Ref: CF-OA-E-001
161-HxCB
162-HxCB
163-HxCB
164-HxCB
165-HxCB
166-HxCB
167-HxCB
168-HxCB
169-HxCB
170-HpCB
171-HpCB
172-HpCB
173-HpCB
174-HpCB
175-HpCB
176-HpCB
177-HpCB
178-HpCB
179-HpCB
180-HpCB
181-HpCB
182-HpCB
183-HpCB
184-HpCB
185-HpCB
186-HpCB
187-HpCB
188-HpCB
189-HpCB
190-HpCB
191-HpCB
192-HpCB
74472-43-8
39635-34-2
74472-44-9
74472-45-0
74472-46-1
41411-63-6
52663-72-6
59291-65-5
32774-16-6
35065-30-6
52663-71-5
52663-74-8
68194-16-1
38411-25-5
40186-70-7
52663-65-7
52663-70-4
52663-67-9
52663-64-6
35065-29-3
74472-47-2
60145-23-5
52663-69-1
74472-48-3
52712-05-7
74472-49-4
52663-68-0
74487-85-7
39635-31-9
41411-64-7
74472-50-7
74472-51-8
Client Sample:
PQL
20.3
20.3
20.3
20.3
20.3
20.3
20.3
40.5
20.3
20.3
20.3
20.3
20.3
20.3
20.3
40.5
20.3
20.3
40.5
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
Page 83 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 7 of 8
SDG Number:6110379
Lab Sample ID:10122009 Matrix:WATER
Date Received:11/19/2016 09:50
Date Collected:11/15/2016 12:00
Surrogate/Tracer recovery Recovery%Acceptable Limits
20.3
20.3
20.3
40.5
40.5
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
C180
U
U
U
CU
CU
C198
C197
U
U
U
U
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
55.5
61.5
64.0
96.6
73.8
104
73.1
127
125
77.3
113
111
112
114
113
86.0
109
109
120
67.9
94.3
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/04/2016 03:35 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
6110379-18 CIS-4-FB
1668A Water
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 987 mL
Result Nominal
1130
1250
1300
1960
1500
2100
1480
2570
2530
1570
2290
2260
2260
2320
2290
1740
4400
2220
2440
1370
1910
2030
2030
2030
2030
2030
2030
2030
2030
2030
2030
2030
2030
2030
2030
2030
2030
4050
2030
2030
2030
2030
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d01dec16b_6-7Data File:
Prep SOP Ref: CF-OA-E-001
193-HpCB
194-OcCB
195-OcCB
196-OcCB
197-OcCB
198-OcCB
199-OcCB
200-OcCB
201-OcCB
202-OcCB
203-OcCB
204-OcCB
205-OcCB
206-NoCB
207-NoCB
208-NoCB
209-DeCB
Total PCB Congeners
69782-91-8
35694-08-7
52663-78-2
42740-50-1
33091-17-7
68194-17-2
52663-75-9
52663-73-7
40186-71-8
2136-99-4
52663-76-0
74472-52-9
74472-53-0
40186-72-9
52663-79-3
52663-77-1
2051-24-3
1336-36-3
Client Sample:
UnitsQual
C
C156L
PQL
20.3
20.3
20.3
40.5
40.5
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
Page 84 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 8 of 8
SDG Number:6110379
Lab Sample ID:10122009 Matrix:WATER
Date Received:11/19/2016 09:50
Date Collected:11/15/2016 12:00
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-28-TrCB
13C-111-PeCB
13C-178-HpCB
73.2
103
88.4
77.7
106
79.0
99.7
103
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/04/2016 03:35 Analyst:MJC

Units
6110379-18 CIS-4-FB
1668A Water
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 987 mL
Result Nominal
1480
2080
1790
1570
2160
1600
2020
2090
2030
2030
2030
2030
2030
2030
2030
2030
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_6-7Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
PQL
Page 85 of 149
Quality Control
Summary
Page 86 of 149
Cape Fear Analytical LLC
Surrogate Recovery Report
PCB Congeners
Report Date:December 22, 2016
Page 1 of 12
SDG Number:6110379
Matrix Type:LIQUID
Surrogate
Acceptance
Limits
49.4
52.4
55.2
90.9
66.8
94.2
65.3
120
120
67.1
102
99.0
97.9
101
106
74.1
89.8
93.6
93.5
76.6
88.0
78.4
89.8
76.3
72.9
90.9
67.0
87.2
91.4
51.1
55.1
59.4
105
77.5
104
70.5
135
135
73.1
117
113
111
115
125
77.9
103
105
110
77.6
97.5
12017454
12017455
Sample ID Client ID
LCS for batch 33432
LCSD for batch 33432
(15%-140%)
(15%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(40%-125%)
(40%-125%)
(40%-125%)
(15%-140%)
(15%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
Recovery
(%)
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-28-TrCB
13C-111-PeCB
13C-178-HpCB
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
QUAL
C
C156L
C
C156L
Page 87 of 149
Cape Fear Analytical LLC
Surrogate Recovery Report
PCB Congeners
Report Date:December 22, 2016
Page 2 of 12
SDG Number:6110379
Matrix Type:LIQUID
Surrogate
Acceptance
Limits
82.6
100
84.9
81.2
100
73.7
96.6
103
50.5
54.0
56.9
90.2
70.8
90.9
65.6
117
116
67.7
104
102
99.5
102
111
70.2
91.0
93.7
96.8
68.8
85.1
72.5
88.7
75.3
72.2
89.9
68.0
86.8
91.4
56.0
60.0
61.8
97.6
72.4
99.4
68.4
122
123
73.5
105
103
101
12017455
12017453
10122008
Sample ID Client ID
LCSD for batch 33432
MB for batch 33432
6110379-17 CIS-3-EB
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(40%-125%)
(40%-125%)
(40%-125%)
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
Recovery
(%)
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-28-TrCB
13C-111-PeCB
13C-178-HpCB
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-28-TrCB
13C-111-PeCB
13C-178-HpCB
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
QUAL
C
C156L
Page 88 of 149
Cape Fear Analytical LLC
Surrogate Recovery Report
PCB Congeners
Report Date:December 22, 2016
Page 3 of 12
SDG Number:6110379
Matrix Type:LIQUID
Surrogate
Acceptance
Limits
106
111
83.5
101
102
109
66.9
87.2
71.0
99.4
86.3
72.9
108
73.6
92.7
103
55.5
61.5
64.0
96.6
73.8
104
73.1
127
125
77.3
113
111
112
114
113
86.0
109
109
120
67.9
94.3
73.2
103
88.4
77.7
106
79.0
99.7
103
10122008
10122009
Sample ID Client ID
6110379-17 CIS-3-EB
6110379-18 CIS-4-FB
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
* Recovery outside Acceptance Limits
# Column to be used to flag recovery values
D Sample Diluted
Recovery
(%)
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-28-TrCB
13C-111-PeCB
13C-178-HpCB
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-28-TrCB
13C-111-PeCB
13C-178-HpCB
QUAL
C
C156L
C
C156L
Page 89 of 149
Cape Fear Analytical LLC
Surrogate Recovery Report
PCB Congeners
Report Date:December 22, 2016
Page 4 of 12
SDG Number:6110379
Matrix Type:SOLID
Surrogate
Acceptance
Limits
50.2
58.2
59.9
82.0
67.3
98.5
79.8
113
111
81.2
103
101
99.2
103
101
95.0
98.6
101
101
87.2
96.8
86.0
101
88.1
83.3
111
89.7
79.9
99.9
56.7
62.4
64.9
85.1
71.5
90.4
79.4
111
110
77.1
95.8
93.6
92.0
95.8
97.1
87.9
88.3
91.3
91.9
79.1
86.0
10122001
12017429
Sample ID Client ID
6110379-07 CIS-6-SB
6110379-07 CIS-6-SB(10122001MS)
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
Recovery
(%)
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
QUAL
C
C156L
C
C156L
Page 90 of 149
Cape Fear Analytical LLC
Surrogate Recovery Report
PCB Congeners
Report Date:December 22, 2016
Page 5 of 12
SDG Number:6110379
Matrix Type:SOLID
Surrogate
Acceptance
Limits
78.4
91.4
79.1
74.0
93.4
79.1
77.4
85.8
45.7
52.4
54.4
72.4
61.1
76.6
71.5
94.6
93.9
67.6
83.5
80.8
80.3
84.4
82.0
81.1
78.6
81.5
80.0
75.2
78.1
71.6
80.9
69.4
67.7
85.2
75.3
70.8
82.9
29.3
38.4
39.0
60.8
48.3
74.7
59.2
95.1
94.0
62.2
86.2
84.3
84.3
12017429
12017430
10122002
Sample ID Client ID
6110379-07 CIS-6-SB(10122001MS)
6110379-07 CIS-6-SB(10122001MSD)
6110379-09 CIS-7-SB
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
Recovery
(%)
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
QUAL
C
C156L
Page 91 of 149
Cape Fear Analytical LLC
Surrogate Recovery Report
PCB Congeners
Report Date:December 22, 2016
Page 6 of 12
SDG Number:6110379
Matrix Type:SOLID
Surrogate
Acceptance
Limits
86.8
87.8
73.4
85.1
86.6
86.5
66.6
78.3
69.4
81.7
71.3
67.3
86.3
80.7
75.8
88.6
52.7
56.0
56.1
132
82.8
97.7
51.4
129
129
70.8
107
105
103
106
112
80.7
101
102
113
62.2
88.3
66.3
98.3
86.2
73.5
105
96.0
58.3
102
51.9
56.0
56.8
113
10122002
10122003
10122006
Sample ID Client ID
6110379-09 CIS-7-SB
6110379-10 CIS-8-SB
6110379-14 CIS-11-SB
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
Recovery
(%)
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
QUAL
C
C156L
C
C156L
Page 92 of 149
Cape Fear Analytical LLC
Surrogate Recovery Report
PCB Congeners
Report Date:December 22, 2016
Page 7 of 12
SDG Number:6110379
Matrix Type:SOLID
Surrogate
Acceptance
Limits
73.1
90.0
56.8
113
112
69.7
94.3
93.3
91.4
94.1
99.1
78.3
93.2
94.0
99.8
67.9
84.5
71.6
90.5
78.7
73.3
95.8
84.0
60.7
89.3
42.3
49.7
53.2
99.0
71.5
90.6
56.8
124
124
59.9
107
102
98.9
102
116
68.5
95.4
95.8
103
58.9
82.0
68.0
94.2
82.6
72.1
10122006
12017427
Sample ID Client ID
6110379-14 CIS-11-SB
LCS for batch 33408
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
(15%-140%)
(15%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
Recovery
(%)
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
QUAL
C
C156L
C
C156L
Page 93 of 149
Cape Fear Analytical LLC
Surrogate Recovery Report
PCB Congeners
Report Date:December 22, 2016
Page 8 of 12
SDG Number:6110379
Matrix Type:SOLID
Surrogate
Acceptance
Limits
103
84.6
54.2
89.2
44.9
51.6
55.4
100
74.2
91.0
59.5
127
126
59.6
103
101
100
103
115
68.6
95.2
95.1
103
57.2
81.7
66.0
92.3
81.9
70.8
101
83.1
56.1
86.9
24.1
33.1
35.1
83.7
54.7
82.6
50.1
123
121
55.9
100
96.3
93.9
96.6
110
63.5
91.0
12017427
12017428
12017426
Sample ID Client ID
LCS for batch 33408
LCSD for batch 33408
MB for batch 33408
(30%-140%)
(40%-125%)
(40%-125%)
(40%-125%)
(15%-140%)
(15%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(40%-125%)
(40%-125%)
(40%-125%)
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
Recovery
(%)
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
QUAL
C
C156L
C
Page 94 of 149
Cape Fear Analytical LLC
Surrogate Recovery Report
PCB Congeners
Report Date:December 22, 2016
Page 9 of 12
SDG Number:6110379
Matrix Type:SOLID
Surrogate
Acceptance
Limits
90.6
98.4
54.4
77.5
62.9
87.4
77.9
67.6
96.7
83.2
56.9
86.1
41.9
50.8
53.6
99.7
73.1
108
65.3
140
141
69.0
111
108
105
108
123
75.7
103
103
112
61.7
88.0
69.5
99.3
87.8
75.7
107
88.3
63.3
92.6
57.8
65.8
70.4
111
85.3
123
88.8
192 *
12017426
10122007
12017482
Sample ID Client ID
MB for batch 33408
6110379-15 CIS-12-SB
LCS for batch 33474
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
(15%-140%)
(15%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
Recovery
(%)
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
QUAL
C156L
C
C156L
Page 95 of 149
Cape Fear Analytical LLC
Surrogate Recovery Report
PCB Congeners
Report Date:December 22, 2016
Page 10 of 12
SDG Number:6110379
Matrix Type:SOLID
Surrogate
Acceptance
Limits
192 *
65.2
131
128
126
131
142 *
84.2
112
113
124
74.3
98.0
80.9
112
98.0
85.7
121
108
79.4
110
47.8
55.2
60.6
94.6
73.8
117
72.3
152 *
156 *
70.2
121
118
119
124
126
86.2
105
107
113
76.3
94.1
80.7
108
95.0
84.9
116
105
68.5
107
12017482
12017483
Sample ID Client ID
LCS for batch 33474
LCSD for batch 33474
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(40%-125%)
(40%-125%)
(40%-125%)
(15%-140%)
(15%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(40%-125%)
(40%-125%)
(40%-125%)
Recovery
(%)
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
QUAL
C
C156L
C
C156L
Page 96 of 149
Cape Fear Analytical LLC
Surrogate Recovery Report
PCB Congeners
Report Date:December 22, 2016
Page 11 of 12
SDG Number:6110379
Matrix Type:SOLID
Surrogate
Acceptance
Limits
35.1
44.5
47.2
92.7
64.4
115
71.5
157 *
158 *
64.1
123
118
115
117
139
75.1
110
111
124
63.7
93.0
73.8
107
94.1
81.4
115
105
80.8
109
70.8
76.1
68.4
88.8
78.4
120
109
126
123
90.0
117
116
116
111
123
100
119
118
121
86.1
109
12017481
10122004
Sample ID Client ID
MB for batch 33474
6110379-12 CIS-9-SB D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
Recovery
(%)
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
QUAL
C
C156L
C
C156L
Page 97 of 149
Cape Fear Analytical LLC
Surrogate Recovery Report
PCB Congeners
Report Date:December 22, 2016
Page 12 of 12
SDG Number:6110379
Matrix Type:SOLID
Surrogate
Acceptance
Limits
86.8
110
91.1
89.9
106
111
94.7
105
91.3
92.9
79.4
97.6
111
122
131
118
121
99.8
101
110
114
110
90.8
122
108
106
109
90.4
106
91.9
109
91.5
80.5
116
124
93.8
98.3
10122004
10122005
Sample ID Client ID
6110379-12 CIS-9-SB
6110379-13 CIS-10-SB
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
D
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
* Recovery outside Acceptance Limits
# Column to be used to flag recovery values
D Sample Diluted
Recovery
(%)
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-28-TrCB
13C-111-PeCB
13C-178-HpCB
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-28-TrCB
13C-111-PeCB
13C-178-HpCB
QUAL
C
C156L
Page 98 of 149
Cape Fear Analytical LLC
Quality Control Summary
Spike Recovery Report
PCB Congeners
Report Date:December 14, 2016
Page 1 of 2
SDG Number:6110379
Client ID:LCS for batch 33408
Lab Sample ID:12017427
Matrix:SOIL
Sample Type: Laboratory Control Sample
2051-60-7
2051-62-9
13029-08-8
2050-68-2
38444-73-4
38444-90-5
15968-05-5
32598-13-3
70362-50-4
56558-16-8
32598-14-4
74472-37-0
31508-00-6
65510-44-3
57465-28-8
33979-03-2
38380-08-4
69782-90-7
52663-72-6
32774-16-6
74487-85-7
39635-31-9
2136-99-4
74472-53-0
40186-72-9
52663-77-1
2051-24-3
1-MoCB
3-MoCB
4-DiCB
15-DiCB
19-TrCB
37-TrCB
54-TeCB
77-TeCB
81-TeCB
104-PeCB
105-PeCB
114-PeCB
118-PeCB
123-PeCB
126-PeCB
155-HxCB
156-HxCB
157-HxCB
167-HxCB
169-HxCB
188-HpCB
189-HpCB
202-OcCB
205-OcCB
206-NoCB
208-NoCB
209-DeCB
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
101
108
94.4
112
96.9
99.8
94.1
95.4
115
123
127
111
104
92.2
116
103
118
120
107
98.6
102
93.7
94.6
95.8
102
89.7
50.0
50.0
50.0
50.0
50.0
50.0
100
100
100
100
100
100
100
100
100
100
200
100
100
100
100
150
150
150
150
150
50.4
53.8
47.2
55.9
48.5
49.9
94.1
95.4
115
123
127
111
104
92.2
116
103
235
120
107
98.6
102
141
142
144
153
135
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
CAS No.Parmname
Acceptance
Limits
Recovery
Amount
Added
pg/g
Spike
Conc.
pg/g
Instrument:HRP875
Analyst:MJC

Analysis Date:
Prep Batch ID:
Batch ID:
12/06/2016 13:12
33410
Dilution:1
%
33408
C
C156
Page 99 of 149
Cape Fear Analytical LLC
Quality Control Summary
Spike Recovery Report
PCB Congeners
Report Date:December 14, 2016
Page 2 of 2
SDG Number:6110379
Client ID:LCSD for batch 33408
Lab Sample ID:12017428
Matrix:SOIL
Sample Type: Laboratory Control Sample Duplicate
2051-60-7
2051-62-9
13029-08-8
2050-68-2
38444-73-4
38444-90-5
15968-05-5
32598-13-3
70362-50-4
56558-16-8
32598-14-4
74472-37-0
31508-00-6
65510-44-3
57465-28-8
33979-03-2
38380-08-4
69782-90-7
52663-72-6
32774-16-6
74487-85-7
39635-31-9
2136-99-4
74472-53-0
40186-72-9
52663-77-1
2051-24-3
1-MoCB
3-MoCB
4-DiCB
15-DiCB
19-TrCB
37-TrCB
54-TeCB
77-TeCB
81-TeCB
104-PeCB
105-PeCB
114-PeCB
118-PeCB
123-PeCB
126-PeCB
155-HxCB
156-HxCB
157-HxCB
167-HxCB
169-HxCB
188-HpCB
189-HpCB
202-OcCB
205-OcCB
206-NoCB
208-NoCB
209-DeCB
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
98.8
111
88.9
112
95
100
94.8
96.3
113
124
126
111
102
101
115
103
115
120
106
96.7
100
93.3
94.7
94.8
101
89.3
50.0
50.0
50.0
50.0
50.0
50.0
100
100
100
100
100
100
100
100
100
100
200
100
100
100
100
150
150
150
150
150
49.4
55.6
44.4
55.8
47.5
50.1
94.8
96.3
113
124
126
111
102
101
115
103
230
120
106
96.7
100
140
142
142
151
134
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
2.00
3.40
6.01
0.258
2.02
0.252
0.720
0.926
1.73
0.893
1.04
0.188
1.52
9.01
1.21
0.274
2.24
0.363
0.670
1.92
2.16
0.469
0.154
1.10
1.27
0.504
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
CAS No.Parmname
Acceptance
Limits
Recovery
Amount
Added
pg/g
Spike
Conc.Acceptance
Limits
RPD
pg/g
Instrument:HRP875
Analyst:MJC

Analysis Date:
Prep Batch ID:
Batch ID:
12/06/2016 14:18
33410
Dilution:1
%%
33408
C
C156
Page 100 of 149
Cape Fear Analytical LLC
Quality Control Summary
Spike Recovery Report
PCB Congeners
Report Date:December 22, 2016
Page 1 of 2
SDG Number:6110379
Client ID:6110379-07 CIS-6-SB(10122001MS)
Lab Sample ID:12017429
Matrix:SOIL
Sample Type:
%Moisture:
Matrix Spike
15.5
2051-60-7
2051-62-9
13029-08-8
2050-68-2
38444-73-4
38444-90-5
15968-05-5
32598-13-3
70362-50-4
56558-16-8
32598-14-4
74472-37-0
31508-00-6
65510-44-3
57465-28-8
33979-03-2
38380-08-4
69782-90-7
52663-72-6
32774-16-6
74487-85-7
39635-31-9
2136-99-4
74472-53-0
40186-72-9
52663-77-1
2051-24-3
1-MoCB
3-MoCB
4-DiCB
15-DiCB
19-TrCB
37-TrCB
54-TeCB
77-TeCB
81-TeCB
104-PeCB
105-PeCB
114-PeCB
118-PeCB
123-PeCB
126-PeCB
155-HxCB
156-HxCB
157-HxCB
167-HxCB
169-HxCB
188-HpCB
189-HpCB
202-OcCB
205-OcCB
206-NoCB
208-NoCB
209-DeCB
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
119
127
97
129
92
107
102
102
122
122
119
112
81.5
109
120
103
124
126
113
98.8
103
96.6
95.4
101
106
92.1
41.9
41.9
41.9
41.9
41.9
41.9
83.7
83.7
83.7
83.7
83.7
83.7
83.7
83.7
83.7
83.7
167
83.7
83.7
83.7
83.7
126
126
126
126
126
49.8
53.1
40.6
54.1
38.5
44.7
85.2
85.4
102
102
122
94.0
129
91.3
101
86.1
207
106
94.8
82.7
86.1
121
120
127
133
116
MS
MS
MS
MS
MS
MS
MS
MS
MS
MS
MS
MS
MS
MS
MS
MS
MS
MS
MS
MS
MS
MS
MS
MS
MS
MS
MS
CAS No.Parmname
Acceptance
Limits
Recovery
Amount
Added
pg/g
Spike
Conc.
pg/g
Instrument:HRP875
Analyst:MJC

Analysis Date:
Prep Batch ID:
Batch ID:
12/02/2016 07:47
33410
Dilution:10
%
U
U
U
U
U
U
U
U
U
U
U
U
U
U
CU
C156
U
U
U
U
U
U
U
U
U
33408
Page 101 of 149
Cape Fear Analytical LLC
Quality Control Summary
Spike Recovery Report
PCB Congeners
Report Date:December 22, 2016
Page 2 of 2
SDG Number:6110379
Client ID:6110379-07 CIS-6-SB(10122001MSD)
Lab Sample ID:12017430
Matrix:SOIL
Sample Type:
%Moisture:
Matrix Spike Duplicate
15.5
2051-60-7
2051-62-9
13029-08-8
2050-68-2
38444-73-4
38444-90-5
15968-05-5
32598-13-3
70362-50-4
56558-16-8
32598-14-4
74472-37-0
31508-00-6
65510-44-3
57465-28-8
33979-03-2
38380-08-4
69782-90-7
52663-72-6
32774-16-6
74487-85-7
39635-31-9
2136-99-4
74472-53-0
40186-72-9
52663-77-1
2051-24-3
1-MoCB
3-MoCB
4-DiCB
15-DiCB
19-TrCB
37-TrCB
54-TeCB
77-TeCB
81-TeCB
104-PeCB
105-PeCB
114-PeCB
118-PeCB
123-PeCB
126-PeCB
155-HxCB
156-HxCB
157-HxCB
167-HxCB
169-HxCB
188-HpCB
189-HpCB
202-OcCB
205-OcCB
206-NoCB
208-NoCB
209-DeCB
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
120
122
96.3
130
92.7
114
100
103
125
122
118
114
91.2
105
121
99
123
130
112
96.3
105
97.3
96.1
104
109
93.9
42.0
42.0
42.0
42.0
42.0
42.0
84.0
84.0
84.0
84.0
84.0
84.0
84.0
84.0
84.0
84.0
168
84.0
84.0
84.0
84.0
126
126
126
126
126
50.6
51.2
40.5
54.5
38.9
48.1
84.1
86.7
105
102
122
95.4
138
88.3
102
83.2
207
109
94.4
80.9
87.8
123
121
131
137
118
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
1.55
3.74
0.423
0.843
1.06
7.36
1.33
1.45
2.66
0.0551
0.249
1.53
6.24
3.38
1.25
3.41
0.169
3.11
0.404
2.22
1.94
1.04
1.07
3.58
2.91
2.26
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
MSD
CAS No.Parmname
Acceptance
Limits
Recovery
Amount
Added
pg/g
Spike
Conc.Acceptance
Limits
RPD
pg/g
Instrument:HRP875
Analyst:MJC

Analysis Date:
Prep Batch ID:
Batch ID:
12/02/2016 08:53
33410
Dilution:10
%%
U
U
U
U
U
U
U
U
U
U
U
U
U
U
CU
C156
U
U
U
U
U
U
U
U
U
33408
Page 102 of 149
Cape Fear Analytical LLC
Quality Control Summary
Spike Recovery Report
PCB Congeners
Report Date:December 14, 2016
Page 1 of 2
SDG Number:6110379
Client ID:LCS for batch 33432
Lab Sample ID:12017454
Matrix:WATER
Sample Type: Laboratory Control Sample
2051-60-7
2051-62-9
13029-08-8
2050-68-2
38444-73-4
38444-90-5
15968-05-5
32598-13-3
70362-50-4
56558-16-8
32598-14-4
74472-37-0
31508-00-6
65510-44-3
57465-28-8
33979-03-2
38380-08-4
69782-90-7
52663-72-6
32774-16-6
74487-85-7
39635-31-9
2136-99-4
74472-53-0
40186-72-9
52663-77-1
2051-24-3
1-MoCB
3-MoCB
4-DiCB
15-DiCB
19-TrCB
37-TrCB
54-TeCB
77-TeCB
81-TeCB
104-PeCB
105-PeCB
114-PeCB
118-PeCB
123-PeCB
126-PeCB
155-HxCB
156-HxCB
157-HxCB
167-HxCB
169-HxCB
188-HpCB
189-HpCB
202-OcCB
205-OcCB
206-NoCB
208-NoCB
209-DeCB
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
100
114
87.8
115
97.2
102
101
100
117
120
126
111
102
102
117
103
119
124
109
97
105
93.4
96.2
97.3
104
91.4
500
500
500
500
500
500
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
2000
1000
1000
1000
1000
1500
1500
1500
1500
1500
502
568
439
577
486
508
1010
1000
1170
1200
1260
1110
1020
1020
1170
1030
2390
1240
1090
970
1050
1400
1440
1460
1560
1370
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
CAS No.Parmname
Acceptance
Limits
Recovery
Amount
Added
pg/L
Spike
Conc.
pg/L
Instrument:HRP875
Analyst:MJC

Analysis Date:
Prep Batch ID:
Batch ID:
12/02/2016 21:26
33438
Dilution:1
%
33432
C
C156
Page 103 of 149
Cape Fear Analytical LLC
Quality Control Summary
Spike Recovery Report
PCB Congeners
Report Date:December 14, 2016
Page 2 of 2
SDG Number:6110379
Client ID:LCSD for batch 33432
Lab Sample ID:12017455
Matrix:WATER
Sample Type: Laboratory Control Sample Duplicate
2051-60-7
2051-62-9
13029-08-8
2050-68-2
38444-73-4
38444-90-5
15968-05-5
32598-13-3
70362-50-4
56558-16-8
32598-14-4
74472-37-0
31508-00-6
65510-44-3
57465-28-8
33979-03-2
38380-08-4
69782-90-7
52663-72-6
32774-16-6
74487-85-7
39635-31-9
2136-99-4
74472-53-0
40186-72-9
52663-77-1
2051-24-3
1-MoCB
3-MoCB
4-DiCB
15-DiCB
19-TrCB
37-TrCB
54-TeCB
77-TeCB
81-TeCB
104-PeCB
105-PeCB
114-PeCB
118-PeCB
123-PeCB
126-PeCB
155-HxCB
156-HxCB
157-HxCB
167-HxCB
169-HxCB
188-HpCB
189-HpCB
202-OcCB
205-OcCB
206-NoCB
208-NoCB
209-DeCB
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
102
111
87.5
117
96.2
102
101
100
118
119
126
110
104
103
116
102
118
123
108
96.4
104
92.5
95.7
96.1
104
91.1
500
500
500
500
500
500
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
2000
1000
1000
1000
1000
1500
1500
1500
1500
1500
509
557
437
584
481
512
1010
1000
1180
1190
1260
1100
1040
1030
1160
1020
2360
1230
1080
964
1040
1390
1440
1440
1550
1370
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
1.44
1.99
0.356
1.31
1.01
0.768
0.161
0.214
0.388
0.793
0.0366
0.226
1.54
0.273
0.774
1.29
1.22
0.327
0.406
0.612
0.889
0.937
0.555
1.25
0.0926
0.359
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
CAS No.Parmname
Acceptance
Limits
Recovery
Amount
Added
pg/L
Spike
Conc.Acceptance
Limits
RPD
pg/L
Instrument:HRP875
Analyst:MJC

Analysis Date:
Prep Batch ID:
Batch ID:
12/02/2016 22:32
33438
Dilution:1
%%
33432
C
C156
Page 104 of 149
Cape Fear Analytical LLC
Quality Control Summary
Spike Recovery Report
PCB Congeners
Report Date:December 14, 2016
Page 1 of 2
SDG Number:6110379
Client ID:LCS for batch 33474
Lab Sample ID:12017482
Matrix:SOIL
Sample Type: Laboratory Control Sample
2051-60-7
2051-62-9
13029-08-8
2050-68-2
38444-73-4
38444-90-5
15968-05-5
32598-13-3
70362-50-4
56558-16-8
32598-14-4
74472-37-0
31508-00-6
65510-44-3
57465-28-8
33979-03-2
38380-08-4
69782-90-7
52663-72-6
32774-16-6
74487-85-7
39635-31-9
2136-99-4
74472-53-0
40186-72-9
52663-77-1
2051-24-3
1-MoCB
3-MoCB
4-DiCB
15-DiCB
19-TrCB
37-TrCB
54-TeCB
77-TeCB
81-TeCB
104-PeCB
105-PeCB
114-PeCB
118-PeCB
123-PeCB
126-PeCB
155-HxCB
156-HxCB
157-HxCB
167-HxCB
169-HxCB
188-HpCB
189-HpCB
202-OcCB
205-OcCB
206-NoCB
208-NoCB
209-DeCB
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
101
110
87.7
107
93
95.1
91.4
94.8
113
123
124
110
102
97.6
114
96
114
119
103
95.1
100
91.2
92.5
92.9
100
88.5
50.0
50.0
50.0
50.0
50.0
50.0
100
100
100
100
100
100
100
100
100
100
200
100
100
100
100
150
150
150
150
150
50.5
54.9
43.8
53.7
46.5
47.6
91.4
94.8
113
123
124
110
102
97.6
114
96.0
229
119
103
95.1
100
137
139
139
151
133
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
LCS
CAS No.Parmname
Acceptance
Limits
Recovery
Amount
Added
pg/g
Spike
Conc.
pg/g
Instrument:HRP875
Analyst:MJC

Analysis Date:
Prep Batch ID:
Batch ID:
12/06/2016 18:54
33485
Dilution:1
%
33474
C
C156
Page 105 of 149
Cape Fear Analytical LLC
Quality Control Summary
Spike Recovery Report
PCB Congeners
Report Date:December 14, 2016
Page 2 of 2
SDG Number:6110379
Client ID:LCSD for batch 33474
Lab Sample ID:12017483
Matrix:SOIL
Sample Type: Laboratory Control Sample Duplicate
2051-60-7
2051-62-9
13029-08-8
2050-68-2
38444-73-4
38444-90-5
15968-05-5
32598-13-3
70362-50-4
56558-16-8
32598-14-4
74472-37-0
31508-00-6
65510-44-3
57465-28-8
33979-03-2
38380-08-4
69782-90-7
52663-72-6
32774-16-6
74487-85-7
39635-31-9
2136-99-4
74472-53-0
40186-72-9
52663-77-1
2051-24-3
1-MoCB
3-MoCB
4-DiCB
15-DiCB
19-TrCB
37-TrCB
54-TeCB
77-TeCB
81-TeCB
104-PeCB
105-PeCB
114-PeCB
118-PeCB
123-PeCB
126-PeCB
155-HxCB
156-HxCB
157-HxCB
167-HxCB
169-HxCB
188-HpCB
189-HpCB
202-OcCB
205-OcCB
206-NoCB
208-NoCB
209-DeCB
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
100
104
83.7
113
94.8
99.9
95
96.6
112
121
125
113
103
96.6
114
92.6
115
120
104
96.7
102
93
94.2
94.9
101
89.7
50.0
50.0
50.0
50.0
50.0
50.0
100
100
100
100
100
100
100
100
100
100
200
100
100
100
100
150
150
150
150
150
50.1
52.2
41.9
56.3
47.4
50.0
95.0
96.6
112
121
125
113
103
96.6
114
92.6
230
120
104
96.7
102
139
141
142
151
135
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0.828
5.10
4.63
4.75
1.97
4.93
3.77
1.87
0.676
1.86
1.25
2.94
0.784
1.05
0.0914
3.67
0.748
0.655
0.518
1.69
2.39
1.94
1.82
2.06
0.248
1.41
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
LCSD
CAS No.Parmname
Acceptance
Limits
Recovery
Amount
Added
pg/g
Spike
Conc.Acceptance
Limits
RPD
pg/g
Instrument:HRP875
Analyst:MJC

Analysis Date:
Prep Batch ID:
Batch ID:
12/06/2016 20:00
33485
Dilution:1
%%
33474
C
C156
Page 106 of 149
Cape Fear Analytical LLC
Method Blank Summary
December 22, 2016Report Date:
Page 1 of 1
SDG Number:6110379
Client ID:MB for batch 33408
Lab Sample ID:12017426
Matrix:SOILClient:AAIS001
Client Sample ID Lab Sample ID File ID Date Analyzed
6110379-07 CIS-6-SB
6110379-07 CIS-6-SB(10122001MS)
6110379-07 CIS-6-SB(10122001MSD)
6110379-09 CIS-7-SB
6110379-10 CIS-8-SB
6110379-14 CIS-11-SB
LCS for batch 33408
LCSD for batch 33408
6110379-15 CIS-12-SB
01
02
03
04
05
06
07
08
09
12/02/16
12/02/16
12/02/16
12/02/16
12/02/16
12/02/16
12/06/16
12/06/16
12/06/16
d01dec16b_2-8
d01dec16b_2-9
d01dec16b_2-10
d01dec16b_2-11
d01dec16b_3-3
d01dec16b_3-4
d06dec16a-2
d06dec16a-3
d06dec16a-5
This method blank applies to the following samples and quality control samples:
Analyzed:12/06/16 15:24Prep Date:28-NOV-16
Data File:d06dec16a-4
Time Analyzed
0641
0747
0853
0959
1330
1436
1312
1418
1630
10122001
12017429
12017430
10122002
10122003
10122006
12017427
12017428
10122007
Instrument ID:HRP875
Column:
Page 107 of 149
Cape Fear Analytical LLC
Method Blank Summary
December 22, 2016Report Date:
Page 1 of 1
SDG Number:6110379
Client ID:MB for batch 33432
Lab Sample ID:12017453
Matrix:WATERClient:AAIS001
Client Sample ID Lab Sample ID File ID Date Analyzed
LCS for batch 33432
LCSD for batch 33432
6110379-17 CIS-3-EB
6110379-18 CIS-4-FB
01
02
03
04
12/02/16
12/02/16
12/04/16
12/04/16
d01dec16b_4-2
d01dec16b_4-3
d01dec16b_6-6
d01dec16b_6-7
This method blank applies to the following samples and quality control samples:
Analyzed:12/02/16 23:38Prep Date:30-NOV-16
Data File:d01dec16b_4-4
Time Analyzed
2126
2232
0229
0335
12017454
12017455
10122008
10122009
Instrument ID:HRP875
Column:
Page 108 of 149
Cape Fear Analytical LLC
Method Blank Summary
December 22, 2016Report Date:
Page 1 of 1
SDG Number:6110379
Client ID:MB for batch 33474
Lab Sample ID:12017481
Matrix:SOILClient:AAIS001
Client Sample ID Lab Sample ID File ID Date Analyzed
LCS for batch 33474
LCSD for batch 33474
6110379-12 CIS-9-SB
6110379-13 CIS-10-SB
01
02
03
04
12/06/16
12/06/16
12/08/16
12/08/16
d06dec16a_2-2
d06dec16a_2-3
d08dec16a-8
d08dec16a-9
This method blank applies to the following samples and quality control samples:
Analyzed:12/06/16 21:06Prep Date:05-DEC-16
Data File:d06dec16a_2-4
Time Analyzed
1854
2000
1746
1852
12017482
12017483
10122004
10122005
Instrument ID:HRP875
Column:
Page 109 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 1 of 8
SDG Number:6110379
Lab Sample ID:12017426 Matrix:SOIL
2
2
2
2
2
2
2
2
2
2
20
4
2
2
2
2
4
2
4
4
2
2
2
2
4
2
2
2
U
U
U
U
U
U
U
U
U
U
U
CU
C12
U
U
U
U
CU
U
CU
CU
U
U
U
U
CU
U
C20
C26
C18
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 15:24 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
MB for batch 33408
QC for batch 33408
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 10 g
33408 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a-4Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
2-MoCB
3-MoCB
4-DiCB
5-DiCB
6-DiCB
7-DiCB
8-DiCB
9-DiCB
10-DiCB
11-DiCB
12-DiCB
13-DiCB
14-DiCB
15-DiCB
16-TrCB
17-TrCB
18-TrCB
19-TrCB
20-TrCB
21-TrCB
22-TrCB
23-TrCB
24-TrCB
25-TrCB
26-TrCB
27-TrCB
28-TrCB
29-TrCB
30-TrCB
31-TrCB
32-TrCB
2051-60-7
2051-61-8
2051-62-9
13029-08-8
16605-91-7
25569-80-6
33284-50-3
34883-43-7
34883-39-1
33146-45-1
2050-67-1
2974-92-7
2974-90-5
34883-41-5
2050-68-2
38444-78-9
37680-66-3
37680-65-2
38444-73-4
38444-84-7
55702-46-0
38444-85-8
55720-44-0
55702-45-9
55712-37-3
38444-81-4
38444-76-7
7012-37-5
15862-07-4
35693-92-6
16606-02-3
38444-77-8
Client Sample:
PQL
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
20.0
4.00
2.00
2.00
2.00
2.00
4.00
2.00
4.00
4.00
2.00
2.00
2.00
2.00
4.00
2.00
2.00
2.00
Page 110 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 2 of 8
SDG Number:6110379
Lab Sample ID:12017426 Matrix:SOIL
2
2
2
2
2
2
4
2
2
2
6
4
2
2
4
4
2
2
2
2
2
2
6
2
8
2
2
C21
U
U
U
U
U
U
CU
U
U
U
CU
CU
U
C44
U
CU
CU
C45
U
C50
U
U
U
U
U
CU
U
CU
C59
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 15:24 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
MB for batch 33408
QC for batch 33408
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 10 g
33408 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a-4Data File:
Prep SOP Ref: CF-OA-E-001
33-TrCB
34-TrCB
35-TrCB
36-TrCB
37-TrCB
38-TrCB
39-TrCB
40-TeCB
41-TeCB
42-TeCB
43-TeCB
44-TeCB
45-TeCB
46-TeCB
47-TeCB
48-TeCB
49-TeCB
50-TeCB
51-TeCB
52-TeCB
53-TeCB
54-TeCB
55-TeCB
56-TeCB
57-TeCB
58-TeCB
59-TeCB
60-TeCB
61-TeCB
62-TeCB
63-TeCB
64-TeCB
38444-86-9
37680-68-5
37680-69-6
38444-87-0
38444-90-5
53555-66-1
38444-88-1
38444-93-8
52663-59-9
36559-22-5
70362-46-8
41464-39-5
70362-45-7
41464-47-5
2437-79-8
70362-47-9
41464-40-8
62796-65-0
68194-04-7
35693-99-3
41464-41-9
15968-05-5
74338-24-2
41464-43-1
70424-67-8
41464-49-7
74472-33-6
33025-41-1
33284-53-6
54230-22-7
74472-34-7
52663-58-8
Client Sample:
PQL
2.00
2.00
2.00
2.00
2.00
2.00
4.00
2.00
2.00
2.00
6.00
4.00
2.00
2.00
4.00
4.00
2.00
2.00
2.00
2.00
2.00
2.00
6.00
2.00
8.00
2.00
2.00
Page 111 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 3 of 8
SDG Number:6110379
Lab Sample ID:12017426 Matrix:SOIL
2
2
2
2
2
2
2
2
2
2
2
2
2
6
12
4
2
6
2
4
2
2
2
C44
U
U
U
C49
C61
C40
U
U
C61
C59
C61
U
U
U
U
U
U
U
U
CU
CU
C86
CU
U
CU
C88
U
CU
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 15:24 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
MB for batch 33408
QC for batch 33408
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 10 g
33408 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a-4Data File:
Prep SOP Ref: CF-OA-E-001
65-TeCB
66-TeCB
67-TeCB
68-TeCB
69-TeCB
70-TeCB
71-TeCB
72-TeCB
73-TeCB
74-TeCB
75-TeCB
76-TeCB
77-TeCB
78-TeCB
79-TeCB
80-TeCB
81-TeCB
82-PeCB
83-PeCB
84-PeCB
85-PeCB
86-PeCB
87-PeCB
88-PeCB
89-PeCB
90-PeCB
91-PeCB
92-PeCB
93-PeCB
94-PeCB
95-PeCB
96-PeCB
33284-54-7
32598-10-0
73575-53-8
73575-52-7
60233-24-1
32598-11-1
41464-46-4
41464-42-0
74338-23-1
32690-93-0
32598-12-2
70362-48-0
32598-13-3
70362-49-1
41464-48-6
33284-52-5
70362-50-4
52663-62-4
60145-20-2
52663-60-2
65510-45-4
55312-69-1
38380-02-8
55215-17-3
73575-57-2
68194-07-0
68194-05-8
52663-61-3
73575-56-1
73575-55-0
38379-99-6
73575-54-9
Client Sample:
PQL
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
6.00
12.0
4.00
2.00
6.00
2.00
4.00
2.00
2.00
2.00
Page 112 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 4 of 8
SDG Number:6110379
Lab Sample ID:12017426 Matrix:SOIL
4
2
2
2
2
2
2
4
4
2
2
2
2
2
2
2
2
2
2
4
C86
CU
U
C93
C90
C98
U
U
U
U
U
CU
C86
CU
U
U
C90
U
C110
C85
C85
U
C86
U
U
U
U
C108
C86
U
U
CU
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 15:24 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
MB for batch 33408
QC for batch 33408
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 10 g
33408 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a-4Data File:
Prep SOP Ref: CF-OA-E-001
97-PeCB
98-PeCB
99-PeCB
100-PeCB
101-PeCB
102-PeCB
103-PeCB
104-PeCB
105-PeCB
106-PeCB
107-PeCB
108-PeCB
109-PeCB
110-PeCB
111-PeCB
112-PeCB
113-PeCB
114-PeCB
115-PeCB
116-PeCB
117-PeCB
118-PeCB
119-PeCB
120-PeCB
121-PeCB
122-PeCB
123-PeCB
124-PeCB
125-PeCB
126-PeCB
127-PeCB
128-HxCB
41464-51-1
60233-25-2
38380-01-7
39485-83-1
37680-73-2
68194-06-9
60145-21-3
56558-16-8
32598-14-4
70424-69-0
70424-68-9
70362-41-3
74472-35-8
38380-03-9
39635-32-0
74472-36-9
68194-10-5
74472-37-0
74472-38-1
18259-05-7
68194-11-6
31508-00-6
56558-17-9
68194-12-7
56558-18-0
76842-07-4
65510-44-3
70424-70-3
74472-39-2
57465-28-8
39635-33-1
38380-07-3
Client Sample:
PQL
4.00
2.00
2.00
2.00
2.00
2.00
2.00
4.00
4.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
4.00
Page 113 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 5 of 8
SDG Number:6110379
Lab Sample ID:12017426 Matrix:SOIL
6
2
2
2
2
2
4
2
2
4
2
2
2
2
2
2
4
2
2
2
4
2
2
4
2
2
2
CU
U
U
U
U
U
CU
U
U
C129
CU
C139
U
U
U
U
U
U
CU
U
C147
U
C135
U
CU
U
U
CU
C156
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 15:24 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
MB for batch 33408
QC for batch 33408
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 10 g
33408 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a-4Data File:
Prep SOP Ref: CF-OA-E-001
129-HxCB
130-HxCB
131-HxCB
132-HxCB
133-HxCB
134-HxCB
135-HxCB
136-HxCB
137-HxCB
138-HxCB
139-HxCB
140-HxCB
141-HxCB
142-HxCB
143-HxCB
144-HxCB
145-HxCB
146-HxCB
147-HxCB
148-HxCB
149-HxCB
150-HxCB
151-HxCB
152-HxCB
153-HxCB
154-HxCB
155-HxCB
156-HxCB
157-HxCB
158-HxCB
159-HxCB
160-HxCB
55215-18-4
52663-66-8
61798-70-7
38380-05-1
35694-04-3
52704-70-8
52744-13-5
38411-22-2
35694-06-5
35065-28-2
56030-56-9
59291-64-4
52712-04-6
41411-61-4
68194-15-0
68194-14-9
74472-40-5
51908-16-8
68194-13-8
74472-41-6
38380-04-0
68194-08-1
52663-63-5
68194-09-2
35065-27-1
60145-22-4
33979-03-2
38380-08-4
69782-90-7
74472-42-7
39635-35-3
41411-62-5
Client Sample:
PQL
6.00
2.00
2.00
2.00
2.00
2.00
4.00
2.00
2.00
4.00
2.00
2.00
2.00
2.00
2.00
2.00
4.00
2.00
2.00
2.00
4.00
2.00
2.00
4.00
2.00
2.00
2.00
Page 114 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 6 of 8
SDG Number:6110379
Lab Sample ID:12017426 Matrix:SOIL
2
2
2
2
2
2
2
4
2
2
2
2
2
2
2
4
2
2
4
2
2
4
2
2
2
2
2
U
U
C129
U
U
C128
U
C153
U
U
CU
U
C171
U
U
U
U
U
U
CU
U
U
CU
U
C183
U
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 15:24 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
MB for batch 33408
QC for batch 33408
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 10 g
33408 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a-4Data File:
Prep SOP Ref: CF-OA-E-001
161-HxCB
162-HxCB
163-HxCB
164-HxCB
165-HxCB
166-HxCB
167-HxCB
168-HxCB
169-HxCB
170-HpCB
171-HpCB
172-HpCB
173-HpCB
174-HpCB
175-HpCB
176-HpCB
177-HpCB
178-HpCB
179-HpCB
180-HpCB
181-HpCB
182-HpCB
183-HpCB
184-HpCB
185-HpCB
186-HpCB
187-HpCB
188-HpCB
189-HpCB
190-HpCB
191-HpCB
192-HpCB
74472-43-8
39635-34-2
74472-44-9
74472-45-0
74472-46-1
41411-63-6
52663-72-6
59291-65-5
32774-16-6
35065-30-6
52663-71-5
52663-74-8
68194-16-1
38411-25-5
40186-70-7
52663-65-7
52663-70-4
52663-67-9
52663-64-6
35065-29-3
74472-47-2
60145-23-5
52663-69-1
74472-48-3
52712-05-7
74472-49-4
52663-68-0
74487-85-7
39635-31-9
41411-64-7
74472-50-7
74472-51-8
Client Sample:
PQL
2.00
2.00
2.00
2.00
2.00
2.00
2.00
4.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
4.00
2.00
2.00
4.00
2.00
2.00
4.00
2.00
2.00
2.00
2.00
2.00
Page 115 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 7 of 8
SDG Number:6110379
Lab Sample ID:12017426 Matrix:SOIL
Surrogate/Tracer recovery Recovery%Acceptable Limits
2
2
2
4
4
2
2
2
2
2
2
2
2
2
2
C180
U
U
U
CU
CU
C198
C197
U
U
U
U
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
24.1
33.1
35.1
83.7
54.7
82.6
50.1
123
121
55.9
100
96.3
93.9
96.6
110
63.5
91.0
90.6
98.4
54.4
77.5
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 15:24 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
MB for batch 33408
QC for batch 33408
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 10 g
Result Nominal
48.2
66.2
70.3
167
109
165
100
245
242
112
200
193
188
193
220
127
364
181
197
109
155
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
400
200
200
200
200
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d06dec16a-4Data File:
Prep SOP Ref: CF-OA-E-001
193-HpCB
194-OcCB
195-OcCB
196-OcCB
197-OcCB
198-OcCB
199-OcCB
200-OcCB
201-OcCB
202-OcCB
203-OcCB
204-OcCB
205-OcCB
206-NoCB
207-NoCB
208-NoCB
209-DeCB
Total PCB Congeners
69782-91-8
35694-08-7
52663-78-2
42740-50-1
33091-17-7
68194-17-2
52663-75-9
52663-73-7
40186-71-8
2136-99-4
52663-76-0
74472-52-9
74472-53-0
40186-72-9
52663-79-3
52663-77-1
2051-24-3
1336-36-3
Client Sample:
UnitsQual
C
C156L
PQL
2.00
2.00
2.00
4.00
4.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
Page 116 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 8 of 8
SDG Number:6110379
Lab Sample ID:12017426 Matrix:SOIL
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
62.9
87.4
77.9
67.6
96.7
83.2
56.9
86.1
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 15:24 Analyst:MJC

Units
MB for batch 33408
QC for batch 33408
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 10 g
Result Nominal
126
175
156
135
193
166
114
172
200
200
200
200
200
200
200
200
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a-4Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
PQL
Page 117 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 1 of 2
SDG Number:6110379
Lab Sample ID:12017427 Matrix:SOIL
Surrogate/Tracer recovery Recovery%Acceptable Limits
50.4
53.8
47.2
55.9
48.5
49.9
94.1
95.4
115
123
127
111
104
92.2
116
103
235
120
107
98.6
102
141
142
144
153
135
C
C156
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
42.3
49.7
53.2
99.0
71.5
90.6
56.8
124
124
59.9
107
102
98.9
(15%-140%)
(15%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 13:12 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
LCS for batch 33408
QC for batch 33408
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 10 g
Result Nominal
84.7
99.4
106
198
143
181
114
249
248
120
213
204
198
200
200
200
200
200
200
200
200
200
200
200
200
200
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d06dec16a-2Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
3-MoCB
4-DiCB
15-DiCB
19-TrCB
37-TrCB
54-TeCB
77-TeCB
81-TeCB
104-PeCB
105-PeCB
114-PeCB
118-PeCB
123-PeCB
126-PeCB
155-HxCB
156-HxCB
157-HxCB
167-HxCB
169-HxCB
188-HpCB
189-HpCB
202-OcCB
205-OcCB
206-NoCB
208-NoCB
209-DeCB
2051-60-7
2051-62-9
13029-08-8
2050-68-2
38444-73-4
38444-90-5
15968-05-5
32598-13-3
70362-50-4
56558-16-8
32598-14-4
74472-37-0
31508-00-6
65510-44-3
57465-28-8
33979-03-2
38380-08-4
69782-90-7
52663-72-6
32774-16-6
74487-85-7
39635-31-9
2136-99-4
74472-53-0
40186-72-9
52663-77-1
2051-24-3
Client Sample:
UnitsQual
PQL
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
4.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
Page 118 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 2 of 2
SDG Number:6110379
Lab Sample ID:12017427 Matrix:SOIL
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
102
116
68.5
95.4
95.8
103
58.9
82.0
68.0
94.2
82.6
72.1
103
84.6
54.2
89.2
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(40%-125%)
(40%-125%)
(40%-125%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 13:12 Analyst:MJC

Units
LCS for batch 33408
QC for batch 33408
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 10 g
Result Nominal
204
231
137
382
192
207
118
164
136
188
165
144
207
169
108
178
200
200
200
400
200
200
200
200
200
200
200
200
200
200
200
200
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
Prep Batch:
d06dec16a-2Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
C
C156L
PQL
Page 119 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 1 of 2
SDG Number:6110379
Lab Sample ID:12017428 Matrix:SOIL
Surrogate/Tracer recovery Recovery%Acceptable Limits
49.4
55.6
44.4
55.8
47.5
50.1
94.8
96.3
113
124
126
111
102
101
115
103
230
120
106
96.7
100
140
142
142
151
134
C
C156
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
44.9
51.6
55.4
100
74.2
91.0
59.5
127
126
59.6
103
101
100
(15%-140%)
(15%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 14:18 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
LCSD for batch 33408
QC for batch 33408
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 10 g
Result Nominal
89.7
103
111
201
148
182
119
253
253
119
206
203
200
200
200
200
200
200
200
200
200
200
200
200
200
200
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d06dec16a-3Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
3-MoCB
4-DiCB
15-DiCB
19-TrCB
37-TrCB
54-TeCB
77-TeCB
81-TeCB
104-PeCB
105-PeCB
114-PeCB
118-PeCB
123-PeCB
126-PeCB
155-HxCB
156-HxCB
157-HxCB
167-HxCB
169-HxCB
188-HpCB
189-HpCB
202-OcCB
205-OcCB
206-NoCB
208-NoCB
209-DeCB
2051-60-7
2051-62-9
13029-08-8
2050-68-2
38444-73-4
38444-90-5
15968-05-5
32598-13-3
70362-50-4
56558-16-8
32598-14-4
74472-37-0
31508-00-6
65510-44-3
57465-28-8
33979-03-2
38380-08-4
69782-90-7
52663-72-6
32774-16-6
74487-85-7
39635-31-9
2136-99-4
74472-53-0
40186-72-9
52663-77-1
2051-24-3
Client Sample:
UnitsQual
PQL
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
4.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
Page 120 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 2 of 2
SDG Number:6110379
Lab Sample ID:12017428 Matrix:SOIL
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
103
115
68.6
95.2
95.1
103
57.2
81.7
66.0
92.3
81.9
70.8
101
83.1
56.1
86.9
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(40%-125%)
(40%-125%)
(40%-125%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
1
Run Date:12/06/2016 14:18 Analyst:MJC

Units
LCSD for batch 33408
QC for batch 33408
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 10 g
Result Nominal
206
231
137
381
190
206
114
163
132
185
164
142
201
166
112
174
200
200
200
400
200
200
200
200
200
200
200
200
200
200
200
200
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
Prep Batch:
d06dec16a-3Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
C
C156L
PQL
Page 121 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 1 of 2
SDG Number:6110379
Lab Sample ID:12017429 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 15.5
Date Collected:11/15/2016 16:00
Surrogate/Tracer recovery Recovery%Acceptable Limits
49.8
53.1
40.6
54.1
38.5
44.7
85.2
85.4
102
102
122
94.0
129
91.3
101
86.1
207
106
94.8
82.7
86.1
121
120
127
133
116
C
C156
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
56.7
62.4
64.9
85.1
71.5
90.4
79.4
111
110
77.1
95.8
93.6
92.0
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 07:47 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-07 CIS-6-SB(10122001MS)
QC for batch 33408
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.13 g
Result Nominal
94.9
105
109
143
120
151
133
186
184
129
160
157
154
167
167
167
167
167
167
167
167
167
167
167
167
167
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d01dec16b_2-9Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
3-MoCB
4-DiCB
15-DiCB
19-TrCB
37-TrCB
54-TeCB
77-TeCB
81-TeCB
104-PeCB
105-PeCB
114-PeCB
118-PeCB
123-PeCB
126-PeCB
155-HxCB
156-HxCB
157-HxCB
167-HxCB
169-HxCB
188-HpCB
189-HpCB
202-OcCB
205-OcCB
206-NoCB
208-NoCB
209-DeCB
2051-60-7
2051-62-9
13029-08-8
2050-68-2
38444-73-4
38444-90-5
15968-05-5
32598-13-3
70362-50-4
56558-16-8
32598-14-4
74472-37-0
31508-00-6
65510-44-3
57465-28-8
33979-03-2
38380-08-4
69782-90-7
52663-72-6
32774-16-6
74487-85-7
39635-31-9
2136-99-4
74472-53-0
40186-72-9
52663-77-1
2051-24-3
Client Sample:
UnitsQual
PQL
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
33.5
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
Page 122 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 2 of 2
SDG Number:6110379
Lab Sample ID:12017429 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 15.5
Date Collected:11/15/2016 16:00
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
95.8
97.1
87.9
88.3
91.3
91.9
79.1
86.0
78.4
91.4
79.1
74.0
93.4
79.1
77.4
85.8
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 07:47 Analyst:MJC

Units
6110379-07 CIS-6-SB(10122001MS)
QC for batch 33408
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.13 g
Result Nominal
160
163
147
296
153
154
133
144
131
153
132
124
156
132
130
144
167
167
167
335
167
167
167
167
167
167
167
167
167
167
167
167
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_2-9Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
C
C156L
PQL
Page 123 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 1 of 2
SDG Number:6110379
Lab Sample ID:12017430 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 15.5
Date Collected:11/15/2016 16:00
Surrogate/Tracer recovery Recovery%Acceptable Limits
50.6
51.2
40.5
54.5
38.9
48.1
84.1
86.7
105
102
122
95.4
138
88.3
102
83.2
207
109
94.4
80.9
87.8
123
121
131
137
118
C
C156
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
45.7
52.4
54.4
72.4
61.1
76.6
71.5
94.6
93.9
67.6
83.5
80.8
80.3
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 08:53 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
6110379-07 CIS-6-SB(10122001MSD
QC for batch 33408
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.08 g
Result Nominal
76.8
88.1
91.4
122
103
129
120
159
158
114
140
136
135
168
168
168
168
168
168
168
168
168
168
168
168
168
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d01dec16b_2-10Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
3-MoCB
4-DiCB
15-DiCB
19-TrCB
37-TrCB
54-TeCB
77-TeCB
81-TeCB
104-PeCB
105-PeCB
114-PeCB
118-PeCB
123-PeCB
126-PeCB
155-HxCB
156-HxCB
157-HxCB
167-HxCB
169-HxCB
188-HpCB
189-HpCB
202-OcCB
205-OcCB
206-NoCB
208-NoCB
209-DeCB
2051-60-7
2051-62-9
13029-08-8
2050-68-2
38444-73-4
38444-90-5
15968-05-5
32598-13-3
70362-50-4
56558-16-8
32598-14-4
74472-37-0
31508-00-6
65510-44-3
57465-28-8
33979-03-2
38380-08-4
69782-90-7
52663-72-6
32774-16-6
74487-85-7
39635-31-9
2136-99-4
74472-53-0
40186-72-9
52663-77-1
2051-24-3
Client Sample:
UnitsQual
PQL
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
33.6
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
16.8
Page 124 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 22, 2016Report Date:
Page 2 of 2
SDG Number:6110379
Lab Sample ID:12017430 Matrix:SOIL
Date Received:%Moisture:11/19/2016 09:50 15.5
Date Collected:11/15/2016 16:00
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
84.4
82.0
81.1
78.6
81.5
80.0
75.2
78.1
71.6
80.9
69.4
67.7
85.2
75.3
70.8
82.9
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33410
Instrument:HRP875
10
Run Date:12/02/2016 08:53 Analyst:MJC

Units
6110379-07 CIS-6-SB(10122001MSD
QC for batch 33408
Client ID:
Prep Date:Prep Aliquot:28-NOV-16 14.08 g
Result Nominal
142
138
136
264
137
134
126
131
120
136
117
114
143
127
119
139
168
168
168
336
168
168
168
168
168
168
168
168
168
168
168
168
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33408 SW846 3540C
Dry Weight
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_2-10Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
C
C156L
PQL
Page 125 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 1 of 8
SDG Number:6110379
Lab Sample ID:12017453 Matrix:WATER
20
20
20
20
20
20
20
20
20
20
100
40
20
20
20
20
40
20
40
40
20
20
20
20
40
20
20
20
U
U
U
U
U
U
U
U
U
U
U
CU
C12
U
U
U
U
CU
U
CU
CU
U
U
U
U
CU
U
C20
C26
C18
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/02/2016 23:38 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
MB for batch 33432
QC for batch 33432
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 1000 mL
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
J Value is estimated
K Estimated Maximum Possible Concentration
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_4-4Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
2-MoCB
3-MoCB
4-DiCB
5-DiCB
6-DiCB
7-DiCB
8-DiCB
9-DiCB
10-DiCB
11-DiCB
12-DiCB
13-DiCB
14-DiCB
15-DiCB
16-TrCB
17-TrCB
18-TrCB
19-TrCB
20-TrCB
21-TrCB
22-TrCB
23-TrCB
24-TrCB
25-TrCB
26-TrCB
27-TrCB
28-TrCB
29-TrCB
30-TrCB
31-TrCB
32-TrCB
2051-60-7
2051-61-8
2051-62-9
13029-08-8
16605-91-7
25569-80-6
33284-50-3
34883-43-7
34883-39-1
33146-45-1
2050-67-1
2974-92-7
2974-90-5
34883-41-5
2050-68-2
38444-78-9
37680-66-3
37680-65-2
38444-73-4
38444-84-7
55702-46-0
38444-85-8
55720-44-0
55702-45-9
55712-37-3
38444-81-4
38444-76-7
7012-37-5
15862-07-4
35693-92-6
16606-02-3
38444-77-8
Client Sample:
PQL
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
100
40.0
20.0
20.0
20.0
20.0
40.0
20.0
40.0
40.0
20.0
20.0
20.0
20.0
40.0
20.0
20.0
20.0
Page 126 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 2 of 8
SDG Number:6110379
Lab Sample ID:12017453 Matrix:WATER
20
20
20
20
20
20
40
20
20
20
60
40
20
20
40
40
20
20
20
20
20
20
60
20
80
20
20
C21
U
U
U
U
U
U
CU
U
U
U
CU
CU
U
C44
U
CU
CU
C45
U
C50
U
U
U
U
U
CU
U
CU
C59
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/02/2016 23:38 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
MB for batch 33432
QC for batch 33432
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 1000 mL
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
J Value is estimated
K Estimated Maximum Possible Concentration
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_4-4Data File:
Prep SOP Ref: CF-OA-E-001
33-TrCB
34-TrCB
35-TrCB
36-TrCB
37-TrCB
38-TrCB
39-TrCB
40-TeCB
41-TeCB
42-TeCB
43-TeCB
44-TeCB
45-TeCB
46-TeCB
47-TeCB
48-TeCB
49-TeCB
50-TeCB
51-TeCB
52-TeCB
53-TeCB
54-TeCB
55-TeCB
56-TeCB
57-TeCB
58-TeCB
59-TeCB
60-TeCB
61-TeCB
62-TeCB
63-TeCB
64-TeCB
38444-86-9
37680-68-5
37680-69-6
38444-87-0
38444-90-5
53555-66-1
38444-88-1
38444-93-8
52663-59-9
36559-22-5
70362-46-8
41464-39-5
70362-45-7
41464-47-5
2437-79-8
70362-47-9
41464-40-8
62796-65-0
68194-04-7
35693-99-3
41464-41-9
15968-05-5
74338-24-2
41464-43-1
70424-67-8
41464-49-7
74472-33-6
33025-41-1
33284-53-6
54230-22-7
74472-34-7
52663-58-8
Client Sample:
PQL
20.0
20.0
20.0
20.0
20.0
20.0
40.0
20.0
20.0
20.0
60.0
40.0
20.0
20.0
40.0
40.0
20.0
20.0
20.0
20.0
20.0
20.0
60.0
20.0
80.0
20.0
20.0
Page 127 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 3 of 8
SDG Number:6110379
Lab Sample ID:12017453 Matrix:WATER
20
20
20
20
20
20
20
20
20
20
20
20
20
60
120
40
20
60
20
40
20
20
20
C44
U
U
U
C49
C61
C40
U
U
C61
C59
C61
U
U
U
U
U
U
U
U
CU
CU
C86
CU
U
CU
C88
U
CU
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/02/2016 23:38 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
MB for batch 33432
QC for batch 33432
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 1000 mL
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
J Value is estimated
K Estimated Maximum Possible Concentration
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_4-4Data File:
Prep SOP Ref: CF-OA-E-001
65-TeCB
66-TeCB
67-TeCB
68-TeCB
69-TeCB
70-TeCB
71-TeCB
72-TeCB
73-TeCB
74-TeCB
75-TeCB
76-TeCB
77-TeCB
78-TeCB
79-TeCB
80-TeCB
81-TeCB
82-PeCB
83-PeCB
84-PeCB
85-PeCB
86-PeCB
87-PeCB
88-PeCB
89-PeCB
90-PeCB
91-PeCB
92-PeCB
93-PeCB
94-PeCB
95-PeCB
96-PeCB
33284-54-7
32598-10-0
73575-53-8
73575-52-7
60233-24-1
32598-11-1
41464-46-4
41464-42-0
74338-23-1
32690-93-0
32598-12-2
70362-48-0
32598-13-3
70362-49-1
41464-48-6
33284-52-5
70362-50-4
52663-62-4
60145-20-2
52663-60-2
65510-45-4
55312-69-1
38380-02-8
55215-17-3
73575-57-2
68194-07-0
68194-05-8
52663-61-3
73575-56-1
73575-55-0
38379-99-6
73575-54-9
Client Sample:
PQL
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
60.0
120
40.0
20.0
60.0
20.0
40.0
20.0
20.0
20.0
Page 128 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 4 of 8
SDG Number:6110379
Lab Sample ID:12017453 Matrix:WATER
40
20
20
20
20
20
20
40
40
20
20
20
20
20
20
20
20
20
20
40
C86
CU
U
C93
C90
C98
U
U
U
U
U
CU
C86
CU
U
U
C90
U
C110
C85
C85
U
C86
U
U
U
U
C108
C86
U
U
CU
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/02/2016 23:38 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
MB for batch 33432
QC for batch 33432
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 1000 mL
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
J Value is estimated
K Estimated Maximum Possible Concentration
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_4-4Data File:
Prep SOP Ref: CF-OA-E-001
97-PeCB
98-PeCB
99-PeCB
100-PeCB
101-PeCB
102-PeCB
103-PeCB
104-PeCB
105-PeCB
106-PeCB
107-PeCB
108-PeCB
109-PeCB
110-PeCB
111-PeCB
112-PeCB
113-PeCB
114-PeCB
115-PeCB
116-PeCB
117-PeCB
118-PeCB
119-PeCB
120-PeCB
121-PeCB
122-PeCB
123-PeCB
124-PeCB
125-PeCB
126-PeCB
127-PeCB
128-HxCB
41464-51-1
60233-25-2
38380-01-7
39485-83-1
37680-73-2
68194-06-9
60145-21-3
56558-16-8
32598-14-4
70424-69-0
70424-68-9
70362-41-3
74472-35-8
38380-03-9
39635-32-0
74472-36-9
68194-10-5
74472-37-0
74472-38-1
18259-05-7
68194-11-6
31508-00-6
56558-17-9
68194-12-7
56558-18-0
76842-07-4
65510-44-3
70424-70-3
74472-39-2
57465-28-8
39635-33-1
38380-07-3
Client Sample:
PQL
40.0
20.0
20.0
20.0
20.0
20.0
20.0
40.0
40.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
40.0
Page 129 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 5 of 8
SDG Number:6110379
Lab Sample ID:12017453 Matrix:WATER
60
20
20
20
20
20
40
20
20
40
20
20
20
20
20
20
40
20
20
20
40
20
20
40
20
20
20
CU
U
U
U
U
U
CU
U
U
C129
CU
C139
U
U
U
U
U
U
CU
U
C147
U
C135
U
CU
U
U
CU
C156
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/02/2016 23:38 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
MB for batch 33432
QC for batch 33432
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 1000 mL
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
J Value is estimated
K Estimated Maximum Possible Concentration
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_4-4Data File:
Prep SOP Ref: CF-OA-E-001
129-HxCB
130-HxCB
131-HxCB
132-HxCB
133-HxCB
134-HxCB
135-HxCB
136-HxCB
137-HxCB
138-HxCB
139-HxCB
140-HxCB
141-HxCB
142-HxCB
143-HxCB
144-HxCB
145-HxCB
146-HxCB
147-HxCB
148-HxCB
149-HxCB
150-HxCB
151-HxCB
152-HxCB
153-HxCB
154-HxCB
155-HxCB
156-HxCB
157-HxCB
158-HxCB
159-HxCB
160-HxCB
55215-18-4
52663-66-8
61798-70-7
38380-05-1
35694-04-3
52704-70-8
52744-13-5
38411-22-2
35694-06-5
35065-28-2
56030-56-9
59291-64-4
52712-04-6
41411-61-4
68194-15-0
68194-14-9
74472-40-5
51908-16-8
68194-13-8
74472-41-6
38380-04-0
68194-08-1
52663-63-5
68194-09-2
35065-27-1
60145-22-4
33979-03-2
38380-08-4
69782-90-7
74472-42-7
39635-35-3
41411-62-5
Client Sample:
PQL
60.0
20.0
20.0
20.0
20.0
20.0
40.0
20.0
20.0
40.0
20.0
20.0
20.0
20.0
20.0
20.0
40.0
20.0
20.0
20.0
40.0
20.0
20.0
40.0
20.0
20.0
20.0
Page 130 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 6 of 8
SDG Number:6110379
Lab Sample ID:12017453 Matrix:WATER
20
20
20
20
20
20
20
40
20
20
20
20
20
20
20
40
20
20
40
20
20
20
20
20
20
20
20
U
U
C129
U
U
C128
U
C153
U
U
CU
U
C171
U
U
U
U
U
U
CU
U
U
CU
U
C183
U
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/02/2016 23:38 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
MB for batch 33432
QC for batch 33432
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 1000 mL
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
J Value is estimated
K Estimated Maximum Possible Concentration
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_4-4Data File:
Prep SOP Ref: CF-OA-E-001
161-HxCB
162-HxCB
163-HxCB
164-HxCB
165-HxCB
166-HxCB
167-HxCB
168-HxCB
169-HxCB
170-HpCB
171-HpCB
172-HpCB
173-HpCB
174-HpCB
175-HpCB
176-HpCB
177-HpCB
178-HpCB
179-HpCB
180-HpCB
181-HpCB
182-HpCB
183-HpCB
184-HpCB
185-HpCB
186-HpCB
187-HpCB
188-HpCB
189-HpCB
190-HpCB
191-HpCB
192-HpCB
74472-43-8
39635-34-2
74472-44-9
74472-45-0
74472-46-1
41411-63-6
52663-72-6
59291-65-5
32774-16-6
35065-30-6
52663-71-5
52663-74-8
68194-16-1
38411-25-5
40186-70-7
52663-65-7
52663-70-4
52663-67-9
52663-64-6
35065-29-3
74472-47-2
60145-23-5
52663-69-1
74472-48-3
52712-05-7
74472-49-4
52663-68-0
74487-85-7
39635-31-9
41411-64-7
74472-50-7
74472-51-8
Client Sample:
PQL
20.0
20.0
20.0
20.0
20.0
20.0
20.0
40.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
40.0
20.0
20.0
40.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
Page 131 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 7 of 8
SDG Number:6110379
Lab Sample ID:12017453 Matrix:WATER
Surrogate/Tracer recovery Recovery%Acceptable Limits
20
20
20
40
40
20
20
20
20
20
20
20
20
20
20
C180
U
U
U
CU
CU
C198
C197
U
U
U
U
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
50.5
54.0
56.9
90.2
70.8
90.9
65.6
117
116
67.7
104
102
99.5
102
111
70.2
91.0
93.7
96.8
68.8
85.1
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/02/2016 23:38 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
MB for batch 33432
QC for batch 33432
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 1000 mL
Result Nominal
1010
1080
1140
1800
1420
1820
1310
2340
2320
1350
2070
2040
1990
2040
2220
1400
3640
1870
1940
1380
1700
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d01dec16b_4-4Data File:
Prep SOP Ref: CF-OA-E-001
193-HpCB
194-OcCB
195-OcCB
196-OcCB
197-OcCB
198-OcCB
199-OcCB
200-OcCB
201-OcCB
202-OcCB
203-OcCB
204-OcCB
205-OcCB
206-NoCB
207-NoCB
208-NoCB
209-DeCB
Total PCB Congeners
69782-91-8
35694-08-7
52663-78-2
42740-50-1
33091-17-7
68194-17-2
52663-75-9
52663-73-7
40186-71-8
2136-99-4
52663-76-0
74472-52-9
74472-53-0
40186-72-9
52663-79-3
52663-77-1
2051-24-3
1336-36-3
Client Sample:
UnitsQual
C
C156L
PQL
20.0
20.0
20.0
40.0
40.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
Page 132 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 8 of 8
SDG Number:6110379
Lab Sample ID:12017453 Matrix:WATER
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-28-TrCB
13C-111-PeCB
13C-178-HpCB
72.5
88.7
75.3
72.2
89.9
68.0
86.8
91.4
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/02/2016 23:38 Analyst:MJC

Units
MB for batch 33432
QC for batch 33432
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 1000 mL
Result Nominal
1450
1770
1510
1440
1800
1360
1740
1830
2000
2000
2000
2000
2000
2000
2000
2000
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
J Value is estimated
K Estimated Maximum Possible Concentration
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d01dec16b_4-4Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
PQL
Page 133 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 1 of 2
SDG Number:6110379
Lab Sample ID:12017454 Matrix:WATER
Surrogate/Tracer recovery Recovery%Acceptable Limits
502
568
439
577
486
508
1010
1000
1170
1200
1260
1110
1020
1020
1170
1030
2390
1240
1090
970
1050
1400
1440
1460
1560
1370
C
C156
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
49.4
52.4
55.2
90.9
66.8
94.2
65.3
120
120
67.1
102
99.0
97.9
(15%-140%)
(15%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/02/2016 21:26 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
LCS for batch 33432
QC for batch 33432
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 1000 mL
Result Nominal
988
1050
1100
1820
1340
1880
1310
2400
2400
1340
2040
1980
1960
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d01dec16b_4-2Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
3-MoCB
4-DiCB
15-DiCB
19-TrCB
37-TrCB
54-TeCB
77-TeCB
81-TeCB
104-PeCB
105-PeCB
114-PeCB
118-PeCB
123-PeCB
126-PeCB
155-HxCB
156-HxCB
157-HxCB
167-HxCB
169-HxCB
188-HpCB
189-HpCB
202-OcCB
205-OcCB
206-NoCB
208-NoCB
209-DeCB
2051-60-7
2051-62-9
13029-08-8
2050-68-2
38444-73-4
38444-90-5
15968-05-5
32598-13-3
70362-50-4
56558-16-8
32598-14-4
74472-37-0
31508-00-6
65510-44-3
57465-28-8
33979-03-2
38380-08-4
69782-90-7
52663-72-6
32774-16-6
74487-85-7
39635-31-9
2136-99-4
74472-53-0
40186-72-9
52663-77-1
2051-24-3
Client Sample:
UnitsQual
PQL
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
40.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
Page 134 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 2 of 2
SDG Number:6110379
Lab Sample ID:12017454 Matrix:WATER
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-28-TrCB
13C-111-PeCB
13C-178-HpCB
101
106
74.1
89.8
93.6
93.5
76.6
88.0
78.4
89.8
76.3
72.9
90.9
67.0
87.2
91.4
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(40%-125%)
(40%-125%)
(40%-125%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/02/2016 21:26 Analyst:MJC

Units
LCS for batch 33432
QC for batch 33432
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 1000 mL
Result Nominal
2020
2110
1480
3590
1870
1870
1530
1760
1570
1800
1530
1460
1820
1340
1740
1830
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
Prep Batch:
d01dec16b_4-2Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
C
C156L
PQL
Page 135 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 1 of 2
SDG Number:6110379
Lab Sample ID:12017455 Matrix:WATER
Surrogate/Tracer recovery Recovery%Acceptable Limits
509
557
437
584
481
512
1010
1000
1180
1190
1260
1100
1040
1030
1160
1020
2360
1230
1080
964
1040
1390
1440
1440
1550
1370
C
C156
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
51.1
55.1
59.4
105
77.5
104
70.5
135
135
73.1
117
113
111
(15%-140%)
(15%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/02/2016 22:32 Analyst:MJC

Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
LCSD for batch 33432
QC for batch 33432
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 1000 mL
Result Nominal
1020
1100
1190
2100
1550
2080
1410
2700
2700
1460
2330
2260
2220
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d01dec16b_4-3Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
3-MoCB
4-DiCB
15-DiCB
19-TrCB
37-TrCB
54-TeCB
77-TeCB
81-TeCB
104-PeCB
105-PeCB
114-PeCB
118-PeCB
123-PeCB
126-PeCB
155-HxCB
156-HxCB
157-HxCB
167-HxCB
169-HxCB
188-HpCB
189-HpCB
202-OcCB
205-OcCB
206-NoCB
208-NoCB
209-DeCB
2051-60-7
2051-62-9
13029-08-8
2050-68-2
38444-73-4
38444-90-5
15968-05-5
32598-13-3
70362-50-4
56558-16-8
32598-14-4
74472-37-0
31508-00-6
65510-44-3
57465-28-8
33979-03-2
38380-08-4
69782-90-7
52663-72-6
32774-16-6
74487-85-7
39635-31-9
2136-99-4
74472-53-0
40186-72-9
52663-77-1
2051-24-3
Client Sample:
UnitsQual
PQL
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
40.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
Page 136 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 2 of 2
SDG Number:6110379
Lab Sample ID:12017455 Matrix:WATER
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-28-TrCB
13C-111-PeCB
13C-178-HpCB
115
125
77.9
103
105
110
77.6
97.5
82.6
100
84.9
81.2
100
73.7
96.6
103
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(40%-125%)
(40%-125%)
(40%-125%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33438
Instrument:HRP875
1
Run Date:12/02/2016 22:32 Analyst:MJC

Units
LCSD for batch 33432
QC for batch 33432
Client ID:
Prep Date:Prep Aliquot:30-NOV-16 1000 mL
Result Nominal
2290
2510
1560
4120
2110
2200
1550
1950
1650
2010
1700
1620
2000
1470
1930
2060
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
33432 SW846 3520C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
Prep Batch:
d01dec16b_4-3Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
C
C156L
PQL
Page 137 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 1 of 8
SDG Number:6110379
Lab Sample ID:12017481 Matrix:SOIL
2
2
2
2
2
2
2
2
2
2
20
4
2
2
2
2
4
2
4
4
2
2
2
2
4
2
2
2
U
U
U
U
U
U
U
U
U
U
U
CU
C12
U
U
U
U
CU
U
CU
CU
U
U
U
U
CU
U
C20
C26
C18
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
1
Run Date:12/06/2016 21:06 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
MB for batch 33474
QC for batch 33474
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 10 g
33474 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a_2-4Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
2-MoCB
3-MoCB
4-DiCB
5-DiCB
6-DiCB
7-DiCB
8-DiCB
9-DiCB
10-DiCB
11-DiCB
12-DiCB
13-DiCB
14-DiCB
15-DiCB
16-TrCB
17-TrCB
18-TrCB
19-TrCB
20-TrCB
21-TrCB
22-TrCB
23-TrCB
24-TrCB
25-TrCB
26-TrCB
27-TrCB
28-TrCB
29-TrCB
30-TrCB
31-TrCB
32-TrCB
2051-60-7
2051-61-8
2051-62-9
13029-08-8
16605-91-7
25569-80-6
33284-50-3
34883-43-7
34883-39-1
33146-45-1
2050-67-1
2974-92-7
2974-90-5
34883-41-5
2050-68-2
38444-78-9
37680-66-3
37680-65-2
38444-73-4
38444-84-7
55702-46-0
38444-85-8
55720-44-0
55702-45-9
55712-37-3
38444-81-4
38444-76-7
7012-37-5
15862-07-4
35693-92-6
16606-02-3
38444-77-8
Client Sample:
PQL
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
20.0
4.00
2.00
2.00
2.00
2.00
4.00
2.00
4.00
4.00
2.00
2.00
2.00
2.00
4.00
2.00
2.00
2.00
Page 138 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 2 of 8
SDG Number:6110379
Lab Sample ID:12017481 Matrix:SOIL
2
2
2
2
2
2
4
2
2
2
6
4
2
2
4
4
2
2
2
2
2
2
6
2
8
2
2
C21
U
U
U
U
U
U
CU
U
U
U
CU
CU
U
C44
U
CU
CU
C45
U
C50
U
U
U
U
U
CU
U
CU
C59
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
1
Run Date:12/06/2016 21:06 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
MB for batch 33474
QC for batch 33474
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 10 g
33474 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a_2-4Data File:
Prep SOP Ref: CF-OA-E-001
33-TrCB
34-TrCB
35-TrCB
36-TrCB
37-TrCB
38-TrCB
39-TrCB
40-TeCB
41-TeCB
42-TeCB
43-TeCB
44-TeCB
45-TeCB
46-TeCB
47-TeCB
48-TeCB
49-TeCB
50-TeCB
51-TeCB
52-TeCB
53-TeCB
54-TeCB
55-TeCB
56-TeCB
57-TeCB
58-TeCB
59-TeCB
60-TeCB
61-TeCB
62-TeCB
63-TeCB
64-TeCB
38444-86-9
37680-68-5
37680-69-6
38444-87-0
38444-90-5
53555-66-1
38444-88-1
38444-93-8
52663-59-9
36559-22-5
70362-46-8
41464-39-5
70362-45-7
41464-47-5
2437-79-8
70362-47-9
41464-40-8
62796-65-0
68194-04-7
35693-99-3
41464-41-9
15968-05-5
74338-24-2
41464-43-1
70424-67-8
41464-49-7
74472-33-6
33025-41-1
33284-53-6
54230-22-7
74472-34-7
52663-58-8
Client Sample:
PQL
2.00
2.00
2.00
2.00
2.00
2.00
4.00
2.00
2.00
2.00
6.00
4.00
2.00
2.00
4.00
4.00
2.00
2.00
2.00
2.00
2.00
2.00
6.00
2.00
8.00
2.00
2.00
Page 139 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 3 of 8
SDG Number:6110379
Lab Sample ID:12017481 Matrix:SOIL
2
2
2
2
2
2
2
2
2
2
2
2
2
6
12
4
2
6
2
4
2
2
2
C44
U
U
U
C49
C61
C40
U
U
C61
C59
C61
U
U
U
U
U
U
U
U
CU
CU
C86
CU
U
CU
C88
U
CU
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
1
Run Date:12/06/2016 21:06 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
MB for batch 33474
QC for batch 33474
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 10 g
33474 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a_2-4Data File:
Prep SOP Ref: CF-OA-E-001
65-TeCB
66-TeCB
67-TeCB
68-TeCB
69-TeCB
70-TeCB
71-TeCB
72-TeCB
73-TeCB
74-TeCB
75-TeCB
76-TeCB
77-TeCB
78-TeCB
79-TeCB
80-TeCB
81-TeCB
82-PeCB
83-PeCB
84-PeCB
85-PeCB
86-PeCB
87-PeCB
88-PeCB
89-PeCB
90-PeCB
91-PeCB
92-PeCB
93-PeCB
94-PeCB
95-PeCB
96-PeCB
33284-54-7
32598-10-0
73575-53-8
73575-52-7
60233-24-1
32598-11-1
41464-46-4
41464-42-0
74338-23-1
32690-93-0
32598-12-2
70362-48-0
32598-13-3
70362-49-1
41464-48-6
33284-52-5
70362-50-4
52663-62-4
60145-20-2
52663-60-2
65510-45-4
55312-69-1
38380-02-8
55215-17-3
73575-57-2
68194-07-0
68194-05-8
52663-61-3
73575-56-1
73575-55-0
38379-99-6
73575-54-9
Client Sample:
PQL
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
6.00
12.0
4.00
2.00
6.00
2.00
4.00
2.00
2.00
2.00
Page 140 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 4 of 8
SDG Number:6110379
Lab Sample ID:12017481 Matrix:SOIL
4
2
2
2
2
2
2
4
4
2
2
2
2
2
2
2
2
2
2
4
C86
CU
U
C93
C90
C98
U
U
U
U
U
CU
C86
CU
U
U
C90
U
C110
C85
C85
U
C86
U
U
U
U
C108
C86
U
U
CU
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
1
Run Date:12/06/2016 21:06 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
MB for batch 33474
QC for batch 33474
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 10 g
33474 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a_2-4Data File:
Prep SOP Ref: CF-OA-E-001
97-PeCB
98-PeCB
99-PeCB
100-PeCB
101-PeCB
102-PeCB
103-PeCB
104-PeCB
105-PeCB
106-PeCB
107-PeCB
108-PeCB
109-PeCB
110-PeCB
111-PeCB
112-PeCB
113-PeCB
114-PeCB
115-PeCB
116-PeCB
117-PeCB
118-PeCB
119-PeCB
120-PeCB
121-PeCB
122-PeCB
123-PeCB
124-PeCB
125-PeCB
126-PeCB
127-PeCB
128-HxCB
41464-51-1
60233-25-2
38380-01-7
39485-83-1
37680-73-2
68194-06-9
60145-21-3
56558-16-8
32598-14-4
70424-69-0
70424-68-9
70362-41-3
74472-35-8
38380-03-9
39635-32-0
74472-36-9
68194-10-5
74472-37-0
74472-38-1
18259-05-7
68194-11-6
31508-00-6
56558-17-9
68194-12-7
56558-18-0
76842-07-4
65510-44-3
70424-70-3
74472-39-2
57465-28-8
39635-33-1
38380-07-3
Client Sample:
PQL
4.00
2.00
2.00
2.00
2.00
2.00
2.00
4.00
4.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
4.00
Page 141 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 5 of 8
SDG Number:6110379
Lab Sample ID:12017481 Matrix:SOIL
6
2
2
2
2
2
4
2
2
4
2
2
2
2
2
2
4
2
2
2
4
2
2
4
2
2
2
CU
U
U
U
U
U
CU
U
U
C129
CU
C139
U
U
U
U
U
U
CU
U
C147
U
C135
U
CU
U
U
CU
C156
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
1
Run Date:12/06/2016 21:06 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
MB for batch 33474
QC for batch 33474
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 10 g
33474 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a_2-4Data File:
Prep SOP Ref: CF-OA-E-001
129-HxCB
130-HxCB
131-HxCB
132-HxCB
133-HxCB
134-HxCB
135-HxCB
136-HxCB
137-HxCB
138-HxCB
139-HxCB
140-HxCB
141-HxCB
142-HxCB
143-HxCB
144-HxCB
145-HxCB
146-HxCB
147-HxCB
148-HxCB
149-HxCB
150-HxCB
151-HxCB
152-HxCB
153-HxCB
154-HxCB
155-HxCB
156-HxCB
157-HxCB
158-HxCB
159-HxCB
160-HxCB
55215-18-4
52663-66-8
61798-70-7
38380-05-1
35694-04-3
52704-70-8
52744-13-5
38411-22-2
35694-06-5
35065-28-2
56030-56-9
59291-64-4
52712-04-6
41411-61-4
68194-15-0
68194-14-9
74472-40-5
51908-16-8
68194-13-8
74472-41-6
38380-04-0
68194-08-1
52663-63-5
68194-09-2
35065-27-1
60145-22-4
33979-03-2
38380-08-4
69782-90-7
74472-42-7
39635-35-3
41411-62-5
Client Sample:
PQL
6.00
2.00
2.00
2.00
2.00
2.00
4.00
2.00
2.00
4.00
2.00
2.00
2.00
2.00
2.00
2.00
4.00
2.00
2.00
2.00
4.00
2.00
2.00
4.00
2.00
2.00
2.00
Page 142 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 6 of 8
SDG Number:6110379
Lab Sample ID:12017481 Matrix:SOIL
2
2
2
2
2
2
2
4
2
2
2
2
2
2
2
4
2
2
4
2
2
2
2
2
2
2
2
U
U
C129
U
U
C128
U
C153
U
U
CU
U
C171
U
U
U
U
U
U
CU
U
U
CU
U
C183
U
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
1
Run Date:12/06/2016 21:06 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
MB for batch 33474
QC for batch 33474
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 10 g
33474 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a_2-4Data File:
Prep SOP Ref: CF-OA-E-001
161-HxCB
162-HxCB
163-HxCB
164-HxCB
165-HxCB
166-HxCB
167-HxCB
168-HxCB
169-HxCB
170-HpCB
171-HpCB
172-HpCB
173-HpCB
174-HpCB
175-HpCB
176-HpCB
177-HpCB
178-HpCB
179-HpCB
180-HpCB
181-HpCB
182-HpCB
183-HpCB
184-HpCB
185-HpCB
186-HpCB
187-HpCB
188-HpCB
189-HpCB
190-HpCB
191-HpCB
192-HpCB
74472-43-8
39635-34-2
74472-44-9
74472-45-0
74472-46-1
41411-63-6
52663-72-6
59291-65-5
32774-16-6
35065-30-6
52663-71-5
52663-74-8
68194-16-1
38411-25-5
40186-70-7
52663-65-7
52663-70-4
52663-67-9
52663-64-6
35065-29-3
74472-47-2
60145-23-5
52663-69-1
74472-48-3
52712-05-7
74472-49-4
52663-68-0
74487-85-7
39635-31-9
41411-64-7
74472-50-7
74472-51-8
Client Sample:
PQL
2.00
2.00
2.00
2.00
2.00
2.00
2.00
4.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
4.00
2.00
2.00
4.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
Page 143 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 7 of 8
SDG Number:6110379
Lab Sample ID:12017481 Matrix:SOIL
Surrogate/Tracer recovery Recovery%Acceptable Limits
2
2
2
4
4
2
2
2
2
2
2
2
2
2
2
C180
U
U
U
CU
CU
C198
C197
U
U
U
U
U
U
U
U
U
U
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
35.1
44.5
47.2
92.7
64.4
115
71.5
157
158
64.1
123
118
115
117
139
75.1
110
111
124
63.7
93.0
*
*
(15%-150%)
(15%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
1
Run Date:12/06/2016 21:06 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
MB for batch 33474
QC for batch 33474
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 10 g
Result Nominal
70.1
88.9
94.5
185
129
229
143
314
316
128
246
237
230
235
278
150
442
221
247
127
186
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
400
200
200
200
200
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33474 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d06dec16a_2-4Data File:
Prep SOP Ref: CF-OA-E-001
193-HpCB
194-OcCB
195-OcCB
196-OcCB
197-OcCB
198-OcCB
199-OcCB
200-OcCB
201-OcCB
202-OcCB
203-OcCB
204-OcCB
205-OcCB
206-NoCB
207-NoCB
208-NoCB
209-DeCB
Total PCB Congeners
69782-91-8
35694-08-7
52663-78-2
42740-50-1
33091-17-7
68194-17-2
52663-75-9
52663-73-7
40186-71-8
2136-99-4
52663-76-0
74472-52-9
74472-53-0
40186-72-9
52663-79-3
52663-77-1
2051-24-3
1336-36-3
Client Sample:
UnitsQual
C
C156L
PQL
2.00
2.00
2.00
4.00
4.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
Page 144 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 8 of 8
SDG Number:6110379
Lab Sample ID:12017481 Matrix:SOIL
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
73.8
107
94.1
81.4
115
105
80.8
109
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(25%-150%)
(30%-135%)
(30%-135%)
(30%-135%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
1
Run Date:12/06/2016 21:06 Analyst:MJC

Units
MB for batch 33474
QC for batch 33474
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 10 g
Result Nominal
148
213
188
163
230
210
162
219
200
200
200
200
200
200
200
200
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33474 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
U Analyte was analyzed for, but not detected above the specified detection limit.
Prep Batch:
d06dec16a_2-4Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
PQL
Page 145 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 1 of 2
SDG Number:6110379
Lab Sample ID:12017482 Matrix:SOIL
Surrogate/Tracer recovery Recovery%Acceptable Limits
50.5
54.9
43.8
53.7
46.5
47.6
91.4
94.8
113
123
124
110
102
97.6
114
96.0
229
119
103
95.1
100
137
139
139
151
133
C
C156
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
57.8
65.8
70.4
111
85.3
123
88.8
192
192
65.2
131
128
126
*
*
(15%-140%)
(15%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
1
Run Date:12/06/2016 18:54 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
LCS for batch 33474
QC for batch 33474
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 10 g
Result Nominal
116
132
141
222
171
245
178
383
384
130
262
255
253
200
200
200
200
200
200
200
200
200
200
200
200
200
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33474 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d06dec16a_2-2Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
3-MoCB
4-DiCB
15-DiCB
19-TrCB
37-TrCB
54-TeCB
77-TeCB
81-TeCB
104-PeCB
105-PeCB
114-PeCB
118-PeCB
123-PeCB
126-PeCB
155-HxCB
156-HxCB
157-HxCB
167-HxCB
169-HxCB
188-HpCB
189-HpCB
202-OcCB
205-OcCB
206-NoCB
208-NoCB
209-DeCB
2051-60-7
2051-62-9
13029-08-8
2050-68-2
38444-73-4
38444-90-5
15968-05-5
32598-13-3
70362-50-4
56558-16-8
32598-14-4
74472-37-0
31508-00-6
65510-44-3
57465-28-8
33979-03-2
38380-08-4
69782-90-7
52663-72-6
32774-16-6
74487-85-7
39635-31-9
2136-99-4
74472-53-0
40186-72-9
52663-77-1
2051-24-3
Client Sample:
UnitsQual
PQL
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
4.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
Page 146 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 2 of 2
SDG Number:6110379
Lab Sample ID:12017482 Matrix:SOIL
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
131
142
84.2
112
113
124
74.3
98.0
80.9
112
98.0
85.7
121
108
79.4
110
*
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(40%-125%)
(40%-125%)
(40%-125%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
1
Run Date:12/06/2016 18:54 Analyst:MJC

Units
LCS for batch 33474
QC for batch 33474
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 10 g
Result Nominal
263
283
168
449
226
247
149
196
162
224
196
171
241
215
159
220
200
200
200
400
200
200
200
200
200
200
200
200
200
200
200
200
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33474 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
Prep Batch:
d06dec16a_2-2Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
C
C156L
PQL
Page 147 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 1 of 2
SDG Number:6110379
Lab Sample ID:12017483 Matrix:SOIL
Surrogate/Tracer recovery Recovery%Acceptable Limits
50.1
52.2
41.9
56.3
47.4
50.0
95.0
96.6
112
121
125
113
103
96.6
114
92.6
230
120
104
96.7
102
139
141
142
151
135
C
C156
Client: AAIS001 Project: AAIS00110
13C-1-MoCB
13C-3-MoCB
13C-4-DiCB
13C-15-DiCB
13C-19-TrCB
13C-37-TrCB
13C-54-TeCB
13C-77-TeCB
13C-81-TeCB
13C-104-PeCB
13C-105-PeCB
13C-114-PeCB
13C-118-PeCB
47.8
55.2
60.6
94.6
73.8
117
72.3
152
156
70.2
121
118
119
*
*
(15%-140%)
(15%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
1
Run Date:12/06/2016 20:00 Analyst:MJC

Units
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
LCSD for batch 33474
QC for batch 33474
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 10 g
Result Nominal
95.5
110
121
189
148
234
145
304
313
140
243
237
238
200
200
200
200
200
200
200
200
200
200
200
200
200
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33474 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Prep Batch:
d06dec16a_2-3Data File:
Prep SOP Ref: CF-OA-E-001
1-MoCB
3-MoCB
4-DiCB
15-DiCB
19-TrCB
37-TrCB
54-TeCB
77-TeCB
81-TeCB
104-PeCB
105-PeCB
114-PeCB
118-PeCB
123-PeCB
126-PeCB
155-HxCB
156-HxCB
157-HxCB
167-HxCB
169-HxCB
188-HpCB
189-HpCB
202-OcCB
205-OcCB
206-NoCB
208-NoCB
209-DeCB
2051-60-7
2051-62-9
13029-08-8
2050-68-2
38444-73-4
38444-90-5
15968-05-5
32598-13-3
70362-50-4
56558-16-8
32598-14-4
74472-37-0
31508-00-6
65510-44-3
57465-28-8
33979-03-2
38380-08-4
69782-90-7
52663-72-6
32774-16-6
74487-85-7
39635-31-9
2136-99-4
74472-53-0
40186-72-9
52663-77-1
2051-24-3
Client Sample:
UnitsQual
PQL
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
4.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
Page 148 of 149
Cape Fear Analytical LLC
PCB Congeners
Certificate of Analysis
Sample Summary
December 14, 2016Report Date:
Page 2 of 2
SDG Number:6110379
Lab Sample ID:12017483 Matrix:SOIL
Surrogate/Tracer recovery Recovery%Acceptable Limits
Client: AAIS001 Project: AAIS00110
13C-123-PeCB
13C-126-PeCB
13C-155-HxCB
13C-156-HxCB
13C-157-HxCB
13C-167-HxCB
13C-169-HxCB
13C-188-HpCB
13C-189-HpCB
13C-202-OcCB
13C-205-OcCB
13C-206-NoCB
13C-208-NoCB
13C-209-DeCB
13C-111-PeCB
13C-28-TrCB
13C-178-HpCB
124
126
86.2
105
107
113
76.3
94.1
80.7
108
95.0
84.9
116
105
68.5
107
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(30%-140%)
(40%-125%)
(40%-125%)
(40%-125%)
CAS No.Parmname ResultQual
Method:EPA Method 1668ABatch ID:33485
Instrument:HRP875
1
Run Date:12/06/2016 20:00 Analyst:MJC

Units
LCSD for batch 33474
QC for batch 33474
Client ID:
Prep Date:Prep Aliquot:05-DEC-16 10 g
Result Nominal
248
252
172
422
215
227
153
188
161
215
190
170
233
210
137
215
200
200
200
400
200
200
200
200
200
200
200
200
200
200
200
200
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
pg/g
33474 SW846 3540C
As Received
Prep Method:
Prep Basis:
Dilution:
Comments:
C Congener has coeluters. When Cxxx, refer to congener number xxx for data
Prep Batch:
d06dec16a_2-3Data File:
Prep SOP Ref: CF-OA-E-001
Client Sample:
UnitsQual
C
C156L
PQL
Page 149 of 149
Centerlane Innes Street, LLC Phase II Environmental Site Assessment (ESA)
January 6, 2017
Cardno
Appendix C: Boring Logs and Well Construction Records

Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-1
Date(s)
Drilled 11/14/16
Drilling
Method HSA
Drill Rig
Type CME 55
Groundwater Level
and Date Measured 20.8'
Borehole
Backfill
Logged By PWL
Drill Bit
Size/Type 9.25
Drilling
Contractor SUMMIT
Sampling
Method(s)Split Spoon
Location CIS-1, north side of building
Checked By MZ
Total Depth
of Borehole 36.5
Approximate
Surface Elevation
Hammer
Data

M
a
t
e
r
i
a
l

T
y
p
e
ML
ML
ML

O
d
o
r
None
None
None
none
none
none
none
none
none
none
none
none
none
none

G
r
a
p
h
i
c

L
o
g

W
e
l
l

L
o
g

M
o
i
s
t
u
r
e

C
o
n
t
e
n
t
0
0
0
0
0
0
0
0
1
2
3
4
4
2

P
I
D
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
MATERIAL DESCRIPTION
Gravel/Pavement
Tan, Orange SILT
Brown, Yellow SILT
Brown, Yellow Fine Sandy SILT
Brown, Gray Fine Sandy SILT

D
e
p
t
h

(
f
e
e
t
)
0
5
10
15
20
25
30
C:
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g
s
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]
Sheet 1 of 2
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-1

M
a
t
e
r
i
a
l

T
y
p
e
ML
PWR

O
d
o
r
none
none
none
none

G
r
a
p
h
i
c

L
o
g

W
e
l
l

L
o
g

M
o
i
s
t
u
r
e

C
o
n
t
e
n
t
0
0
0
0

P
I
D
0.0
0.0
0.0
0.0
MATERIAL DESCRIPTION
Brown SILT with rock fragments and mica
Partially Weathered Rock
Bottom of Boring

D
e
p
t
h

(
f
e
e
t
)
30
35
40
45
50
55
60
65
C:
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a
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i
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]
Sheet 2 of 2
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-2
Date(s)
Drilled 11/14/16
Drilling
Method HSA
Drill Rig
Type CME 55
Groundwater Level
and Date Measured 16.8
Borehole
Backfill
Logged By PWL
Drill Bit
Size/Type 9.25
Drilling
Contractor SUMMIT
Sampling
Method(s)Split Spoon
Location CIS-2 east side of building. Location of proposed building.
Checked By MZ
Total Depth
of Borehole 36.1
Approximate
Surface Elevation
Hammer
Data

M
a
t
e
r
i
a
l

T
y
p
e
ML
ML
ML

O
d
o
r
None
None
None
none
none
none
none
none
none
none
none
none
none
none

G
r
a
p
h
i
c

L
o
g

W
e
l
l

L
o
g

M
o
i
s
t
u
r
e

C
o
n
t
e
n
t
0
0
0
0
0
0
0
0
0
0
0
0
2
4

P
I
D
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
MATERIAL DESCRIPTION
Gravel/Pavement
Tan, Brown SILT
Tan, Yellow fine Sandy SILT
Tan SILT with rock fragments and mica
Initial 11/14/16
11/15/16

D
e
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t
h

(
f
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)
0
5
10
15
20
25
30
C:
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[
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p
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]
Sheet 1 of 2
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-2

M
a
t
e
r
i
a
l

T
y
p
e
ML
PWR

O
d
o
r
none
none
none
none

G
r
a
p
h
i
c

L
o
g

W
e
l
l

L
o
g

M
o
i
s
t
u
r
e

C
o
n
t
e
n
t
0
0
0
0

P
I
D
0.0
0.0
0.0
0.0
MATERIAL DESCRIPTION
Tan SILT with rock fragments and mica
Partially Weathered Rock
Bottom of Boring

D
e
p
t
h

(
f
e
e
t
)
30
35
40
45
50
55
60
65
C:
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s
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\
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a
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L
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\
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m
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]
Sheet 2 of 2
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-3
Date(s)
Drilled 11/15/16
Drilling
Method HSA
Drill Rig
Type CME 55
Groundwater Level
and Date Measured 17.95
Borehole
Backfill
Logged By PWL
Drill Bit
Size/Type 9.25
Drilling
Contractor SUMMIT
Sampling
Method(s)Split Spoon
Location CIS-3, south side of building.
Checked By MZ
Total Depth
of Borehole 31.1
Approximate
Surface Elevation
Hammer
Data

M
a
t
e
r
i
a
l

T
y
p
e
ML
ML
PWR

O
d
o
r
None
None
None
none
none
none
none
none
none
none
none
none
none
none

G
r
a
p
h
i
c

L
o
g

W
e
l
l

L
o
g

M
o
i
s
t
u
r
e

C
o
n
t
e
n
t
0
0
0
0
0
0
2
4
0
0
0
0
0
0

P
I
D
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
MATERIAL DESCRIPTION
Gravel/Pavement
Tan, Orange SILT
Brown SILT with mica and rock fragments.
Some fine sand lenses.
Partially Weathered Rock
Initial 11/15/16
11/16/16

D
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p
t
h

(
f
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t
)
0
5
10
15
20
25
30
C:
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]
Sheet 1 of 2
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-3

M
a
t
e
r
i
a
l

T
y
p
e
PWR

O
d
o
r
none

G
r
a
p
h
i
c

L
o
g

W
e
l
l

L
o
g

M
o
i
s
t
u
r
e

C
o
n
t
e
n
t
0

P
I
D
0.0
MATERIAL DESCRIPTION
Partially Weathered Rock
Bottom of Boring - Auger Refusal

D
e
p
t
h

(
f
e
e
t
)
30
35
40
45
50
55
60
65
C:
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s
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p
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D
a
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a
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L
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]
Sheet 2 of 2
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-4
Date(s)
Drilled 11/15/16
Drilling
Method HSA
Drill Rig
Type CME 55
Groundwater Level
and Date Measured 16.8
Borehole
Backfill
Logged By PWL
Drill Bit
Size/Type 9.25
Drilling
Contractor SUMMIT
Sampling
Method(s)Split Spoon
Location CIS-4, southwest portion of site.
Checked By MZ
Total Depth
of Borehole 31.9
Approximate
Surface Elevation
Hammer
Data

M
a
t
e
r
i
a
l

T
y
p
e
ML
ML
ML
PWR

O
d
o
r
None
None
None
none
none
none
none
none
none
none
none
none
none
none

G
r
a
p
h
i
c

L
o
g

W
e
l
l

L
o
g

M
o
i
s
t
u
r
e

C
o
n
t
e
n
t
0
0
0
0
0
0
1
2
0
0
4
3
3
3

P
I
D
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
MATERIAL DESCRIPTION
Gravel/Pavement
Brown, Orange SILT
Brown, Yellow SILT
Gray, Green fine Sandy SILT
Partially Weathered Rock and SILT
Initial 11/15/16
11/16/16

D
e
p
t
h

(
f
e
e
t
)
0
5
10
15
20
25
30
C:
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]
Sheet 1 of 2
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-4

M
a
t
e
r
i
a
l

T
y
p
e
PWR

O
d
o
r
none

G
r
a
p
h
i
c

L
o
g

W
e
l
l

L
o
g

M
o
i
s
t
u
r
e

C
o
n
t
e
n
t
0

P
I
D
0.0
MATERIAL DESCRIPTION
Partially Weathered Rock and SILT
Bottom of Boring - Auger Refusal

D
e
p
t
h

(
f
e
e
t
)
30
35
40
45
50
55
60
65
C:
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D
a
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a
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L
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a
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\
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m
p
\
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i
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g
s
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]
Sheet 2 of 2
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Key to Log of Boring

M
a
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e
r
i
a
l

T
y
p
e

O
d
o
r

G
r
a
p
h
i
c

L
o
g

W
e
l
l

L
o
g

M
o
i
s
t
u
r
e

C
o
n
t
e
n
t

P
I
D
MATERIAL DESCRIPTION

D
e
p
t
h

(
f
e
e
t
)
1 2 3 4 5 6 7 8
COLUMN DESCRIPTIONS
1 Depth (feet): Depth in feet below the ground surface.
2 Material Type: Type of material encountered.
3 Graphic Log: Graphic depiction of the subsurface material
encountered.
4 MATERIAL DESCRIPTION: Description of material encountered.
May include consistency, moisture, color, and other descriptive
text.
5 Well Log: Graphical representation of well installed upon
completion of drilling and sampling.
6 Moisture Content: Water content of the soil sample, expressed
as percentage of dry weight of sample.
7 PID: PID
8 Odor: Comments and observations regarding drilling or
sampling made by driller or field personnel.
FIELD AND LABORATORY TEST ABBREVIATIONS
CHEM: Chemical tests to assess corrosivity
COMP: Compaction test
CONS: One-dimensional consolidation test
LL: Liquid Limit, percent
PI: Plasticity Index, percent
SA: Sieve analysis (percent passing No. 200 Sieve)
UC: Unconfined compressive strength test, Qu, in ksf
WA: Wash sieve (percent passing No. 200 Sieve)
MATERIAL GRAPHIC SYMBOLS
Bentonite chips
Bentonite plug
Gravel
SILT, SILT w/SAND, SANDY SILT (ML)
Well graded SAND (SW)
TYPICAL SAMPLER GRAPHIC SYMBOLS
Auger sampler
Bulk Sample
3-inch-OD California w/
brass rings
CME Sampler
Grab Sample
2.5-inch-OD Modified
California w/ brass liners
Pitcher Sample
2-inch-OD unlined split
spoon (SPT)
Shelby Tube (Thin-walled,
fixed head)
OTHER GRAPHIC SYMBOLS
Water level (at time of drilling, ATD)
Water level (after waiting)
Minor change in material properties within a
stratum
Inferred/gradational contact between strata
?Queried contact between strata
GENERAL NOTES
1: Soil classifications are based on the Unified Soil Classification System. Descriptions and stratum lines are interpretive, and actual lithologic changes may be
gradual. Field descriptions may have been modified to reflect results of lab tests.
2: Descriptions on these logs apply only at the specific boring locations and at the time the borings were advanced. They are not warranted to be representative
of subsurface conditions at other locations or times.
C:
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c
a
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]
Figure B-1
Sheet 1 of 1
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-5
Date(s)
Drilled 11/15/16
Drilling
Method Direct Push
Drill Rig
Type GeoProbe
Groundwater Level
and Date Measured NA
Borehole
Backfill Grout
Logged By CE
Drill Bit
Size/Type 2.5"
Drilling
Contractor EPDS
Sampling
Method(s)MacroCore
Location Wash Pad Area - Adjacent to found Heating Oil UST
Checked By PWL
Total Depth
of Borehole 10
Approximate
Surface Elevation
Hammer
Data
Ma
t
e
r
i
a
l

T
y
p
e
Concrete
ML
ML
REMARKS AND OTHER TESTS
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Gr
a
p
h
i
c

L
o
g
MATERIAL DESCRIPTION
Concrete Wash Pad
Tan, Brown Fine Sandy SILT
Tan, Brown SILT
Bottom of Boring
PI
D

R
e
a
d
i
n
g
,

p
p
m
0.0
0.0
0.0
0.0
0.0
0.0
De
p
t
h

(
f
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t
)
0
5
10
15
20
25
30
Sa
m
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]
Sheet 1 of 1
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-6B
Date(s)
Drilled 11/15/16
Drilling
Method Direct Push
Drill Rig
Type GeoProbe
Groundwater Level
and Date Measured NA
Borehole
Backfill Grout
Logged By CE
Drill Bit
Size/Type 2.5"
Drilling
Contractor EPDS
Sampling
Method(s)MacroCore
Location Hydraulic Lift CIS-6 eastern hydraulic post
Checked By PWL
Total Depth
of Borehole 10
Approximate
Surface Elevation
Hammer
Data
Ma
t
e
r
i
a
l

T
y
p
e
Concrete
ML
ML
ML
ML
REMARKS AND OTHER TESTS
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Gr
a
p
h
i
c

L
o
g
MATERIAL DESCRIPTION
Concrete Floor
Tan, Gray SILT
Tan, Orange Fine Sandy SILT
Tan, Orange Fine Sandy SILT
Tan, Fine Sandy SILT
Bottom of Boring
PI
D

R
e
a
d
i
n
g
,

p
p
m
0.0
0.0
0.0
0.0
0.0
0.0
De
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t
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(
f
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)
0
5
10
15
20
25
30
Sa
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Sheet 1 of 1
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-6A
Date(s)
Drilled 11/15/16
Drilling
Method Direct Push
Drill Rig
Type GeoProbe
Groundwater Level
and Date Measured NA
Borehole
Backfill Grout
Logged By CE
Drill Bit
Size/Type 2.5"
Drilling
Contractor EPDS
Sampling
Method(s)MacroCore
Location Hydraulic Lift CIS-6 western hydraulic post
Checked By PWL
Total Depth
of Borehole 10
Approximate
Surface Elevation
Hammer
Data
Ma
t
e
r
i
a
l

T
y
p
e
Concrete
ML
ML
ML
REMARKS AND OTHER TESTS
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Gr
a
p
h
i
c

L
o
g
MATERIAL DESCRIPTION
Concrete Floor
Tan, Orange Fine Sandy SILT
Tan SILT
Tan, Gray SILT
Bottom of Boring
PI
D

R
e
a
d
i
n
g
,

p
p
m
0.0
0.0
0.0
0.0
0.0
0.0
De
p
t
h

(
f
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t
)
0
5
10
15
20
25
30
Sa
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p
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T
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C:
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]
Sheet 1 of 1
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-7A
Date(s)
Drilled 11/15/16
Drilling
Method Direct Push
Drill Rig
Type GeoProbe
Groundwater Level
and Date Measured NA
Borehole
Backfill Grout
Logged By CE
Drill Bit
Size/Type 2.5"
Drilling
Contractor EPDS
Sampling
Method(s)MacroCore
Location Hydraulic Lift CIS-7 western hydraulic post
Checked By PWL
Total Depth
of Borehole 10
Approximate
Surface Elevation
Hammer
Data
Ma
t
e
r
i
a
l

T
y
p
e
Concrete
ML
REMARKS AND OTHER TESTS
Moist, No Odor
Moist, No Odor
Moist, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Gr
a
p
h
i
c

L
o
g
MATERIAL DESCRIPTION
Concrete Floor
Tan, Orange Fine SILT
Bottom of Boring
PI
D

R
e
a
d
i
n
g
,

p
p
m
0.0
0.0
0.0
0.0
0.0
0.0
De
p
t
h

(
f
e
e
t
)
0
5
10
15
20
25
30
Sa
m
p
l
e

N
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Sa
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e

T
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C:
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.
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]
Sheet 1 of 1
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-7B
Date(s)
Drilled 11/15/16
Drilling
Method Direct Push
Drill Rig
Type GeoProbe
Groundwater Level
and Date Measured NA
Borehole
Backfill Grout
Logged By CE
Drill Bit
Size/Type 2.5"
Drilling
Contractor EPDS
Sampling
Method(s)MacroCore
Location Hydraulic Lift CIS-7 eastern hydraulic post
Checked By PWL
Total Depth
of Borehole 10
Approximate
Surface Elevation
Hammer
Data
Ma
t
e
r
i
a
l

T
y
p
e
Concrete
ML
ML
REMARKS AND OTHER TESTS
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Gr
a
p
h
i
c

L
o
g
MATERIAL DESCRIPTION
Concrete Floor
Tan, Orange SILT
Tan SILT
Bottom of Boring
PI
D

R
e
a
d
i
n
g
,

p
p
m
0.0
0.0
0.0
0.0
0.0
0.0
De
p
t
h

(
f
e
e
t
)
0
5
10
15
20
25
30
Sa
m
p
l
e

N
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r
Sa
m
p
l
e

T
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C:
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.
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.
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]
Sheet 1 of 1
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-8A
Date(s)
Drilled 11/15/16
Drilling
Method Direct Push
Drill Rig
Type GeoProbe
Groundwater Level
and Date Measured NA
Borehole
Backfill Grout
Logged By CE
Drill Bit
Size/Type 2.5"
Drilling
Contractor EPDS
Sampling
Method(s)MacroCore
Location Hydraulic Lift CIS-8 western hydraulic post
Checked By PWL
Total Depth
of Borehole 10
Approximate
Surface Elevation
Hammer
Data
Ma
t
e
r
i
a
l

T
y
p
e
Concrete
ML
ML
ML
ML
ML
REMARKS AND OTHER TESTS
Moist, No Odor
Moist, No Odor
Moist, No Odor
Moist, No Odor
Moist, No Odor
Moist, No Odor
Gr
a
p
h
i
c

L
o
g
MATERIAL DESCRIPTION
Concrete Floor
Orange SILT
Orange SILT
Tan SILT
Orange SILT
Orange SILT
Bottom of Boring
PI
D

R
e
a
d
i
n
g
,

p
p
m
0.0
0.0
0.0
0.0
0.0
0.0
De
p
t
h

(
f
e
e
t
)
0
5
10
15
20
25
30
Sa
m
p
l
e

N
u
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b
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r
Sa
m
p
l
e

T
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p
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C:
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.
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[
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.
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]
Sheet 1 of 1
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-8B
Date(s)
Drilled 11/15/16
Drilling
Method Direct Push
Drill Rig
Type GeoProbe
Groundwater Level
and Date Measured NA
Borehole
Backfill Grout
Logged By CE
Drill Bit
Size/Type 2.5"
Drilling
Contractor EPDS
Sampling
Method(s)MacroCore
Location Hydraulic Lift CIS-8 eastern hydraulic post
Checked By PWL
Total Depth
of Borehole 10
Approximate
Surface Elevation
Hammer
Data
Ma
t
e
r
i
a
l

T
y
p
e
Concrete
ML
ML
ML
ML
ML
REMARKS AND OTHER TESTS
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Gr
a
p
h
i
c

L
o
g
MATERIAL DESCRIPTION
Concrete Floor
Tan SILT
Tan SILT
Tan SILT
Tan SILT
Tan SILT
Bottom of Boring
PI
D

R
e
a
d
i
n
g
,

p
p
m
0.0
0.0
0.0
0.0
0.0
0.0
De
p
t
h

(
f
e
e
t
)
0
5
10
15
20
25
30
Sa
m
p
l
e

N
u
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r
Sa
m
p
l
e

T
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p
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C:
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.
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]
Sheet 1 of 1
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-9A
Date(s)
Drilled 11/15/16
Drilling
Method Direct Push
Drill Rig
Type GeoProbe
Groundwater Level
and Date Measured NA
Borehole
Backfill Grout
Logged By CE
Drill Bit
Size/Type 2.5"
Drilling
Contractor EPDS
Sampling
Method(s)MacroCore
Location Hydraulic Lift CIS-9 western hydraulic post
Checked By PWL
Total Depth
of Borehole 10
Approximate
Surface Elevation
Hammer
Data
Ma
t
e
r
i
a
l

T
y
p
e
Concrete
ML
ML
ML
ML
ML
REMARKS AND OTHER TESTS
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Gr
a
p
h
i
c

L
o
g
MATERIAL DESCRIPTION
Concrete Floor
Tan, Orange SILT
Tan, Orange SILT
Tan, Orange SILT
Tan, Orange SILT
Tan, Orange, Gray SILT
Bottom of Boring
PI
D

R
e
a
d
i
n
g
,

p
p
m
0.0
0.0
0.0
0.0
1.6
3.6
De
p
t
h

(
f
e
e
t
)
0
5
10
15
20
25
30
Sa
m
p
l
e

N
u
m
b
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r
Sa
m
p
l
e

T
y
p
e
C:
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\
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p
p
D
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a
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L
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m
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\
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.
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[
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)
c
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.
t
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]
Sheet 1 of 1
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-9B
Date(s)
Drilled 11/15/16
Drilling
Method Direct Push
Drill Rig
Type GeoProbe
Groundwater Level
and Date Measured NA
Borehole
Backfill Grout
Logged By CE
Drill Bit
Size/Type 2.5"
Drilling
Contractor EPDS
Sampling
Method(s)MacroCore
Location Hydraulic Lift CIS-9 eastern hydraulic post
Checked By PWL
Total Depth
of Borehole 10
Approximate
Surface Elevation
Hammer
Data
Ma
t
e
r
i
a
l

T
y
p
e
Concrete
ML
ML
ML
ML
ML
REMARKS AND OTHER TESTS
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Gr
a
p
h
i
c

L
o
g
MATERIAL DESCRIPTION
Concrete Floor
Tan, Orange SILT
Tan, Orange SILT
Tan, Orange SILT
Tan, Orange SILT
Tan, Orange SILT
Bottom of Boring
PI
D

R
e
a
d
i
n
g
,

p
p
m
0.0
0.0
0.0
0.0
0.0
0.0
De
p
t
h

(
f
e
e
t
)
0
5
10
15
20
25
30
Sa
m
p
l
e

N
u
m
b
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r
Sa
m
p
l
e

T
y
p
e
C:
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s
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.
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]
Sheet 1 of 1
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-10A
Date(s)
Drilled 11/15/16
Drilling
Method Direct Push
Drill Rig
Type GeoProbe
Groundwater Level
and Date Measured NA
Borehole
Backfill Grout
Logged By CE
Drill Bit
Size/Type 2.5"
Drilling
Contractor EPDS
Sampling
Method(s)MacroCore
Location Hydraulic Lift CIS-10 western hydraulic post
Checked By PWL
Total Depth
of Borehole 10
Approximate
Surface Elevation
Hammer
Data
Ma
t
e
r
i
a
l

T
y
p
e
Concrete
ML
ML
ML
ML
ML
REMARKS AND OTHER TESTS
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Gr
a
p
h
i
c

L
o
g
MATERIAL DESCRIPTION
Concrete Floor
Tan, Orange SILT
Tan, Orange SILT
Tan, Orange SILT
Tan, Orange SILT
Tan, Brown SILT
Bottom of Boring
PI
D

R
e
a
d
i
n
g
,

p
p
m
0.0
0.0
0.0
1.8
4.0
3.7
De
p
t
h

(
f
e
e
t
)
0
5
10
15
20
25
30
Sa
m
p
l
e

N
u
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b
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r
Sa
m
p
l
e

T
y
p
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C:
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s
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Sheet 1 of 1
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-10B
Date(s)
Drilled 11/15/16
Drilling
Method Direct Push
Drill Rig
Type GeoProbe
Groundwater Level
and Date Measured NA
Borehole
Backfill Grout
Logged By CE
Drill Bit
Size/Type 2.5"
Drilling
Contractor EPDS
Sampling
Method(s)MacroCore
Location Hydraulic Lift CIS-10 eastern hydraulic post
Checked By PWL
Total Depth
of Borehole 10
Approximate
Surface Elevation
Hammer
Data
Ma
t
e
r
i
a
l

T
y
p
e
Concrete
ML
ML
ML
ML
ML
REMARKS AND OTHER TESTS
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Gr
a
p
h
i
c

L
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MATERIAL DESCRIPTION
Concrete Floor
Tan, Orange SILT
Tan, Orange SILT
Tan, Orange SILT
Tan, Orange SILT
Tan SILT
Bottom of Boring
PI
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Sheet 1 of 1
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-11
Date(s)
Drilled 11/15/16
Drilling
Method Direct Push
Drill Rig
Type GeoProbe
Groundwater Level
and Date Measured NA
Borehole
Backfill Grout
Logged By CE
Drill Bit
Size/Type 2.5"
Drilling
Contractor EPDS
Sampling
Method(s)MacroCore
Location Unknown rectangular pad inside building
Checked By PWL
Total Depth
of Borehole 10
Approximate
Surface Elevation
Hammer
Data
Ma
t
e
r
i
a
l

T
y
p
e
Concrete
ML
ML
ML
ML
ML
REMARKS AND OTHER TESTS
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Gr
a
p
h
i
c

L
o
g
MATERIAL DESCRIPTION
Concrete Floor
Tan, Orange SILT
Tan, Orange SILT
Tan, Orange SILT
Tan, Orange SILT
Tan, Orange SILT
Bottom of Boring
PI
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0.0
0.0
0.0
0.0
0.0
0.0
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10
15
20
25
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Sheet 1 of 1
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-12A
Date(s)
Drilled 11/15/16
Drilling
Method Direct Push
Drill Rig
Type GeoProbe
Groundwater Level
and Date Measured NA
Borehole
Backfill Grout
Logged By CE
Drill Bit
Size/Type 2.5"
Drilling
Contractor EPDS
Sampling
Method(s)MacroCore
Location Hydraulic lift CIS-12 western post
Checked By PWL
Total Depth
of Borehole 10
Approximate
Surface Elevation
Hammer
Data
Ma
t
e
r
i
a
l

T
y
p
e
Concrete
ML
ML
ML
ML
ML
REMARKS AND OTHER TESTS
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Gr
a
p
h
i
c

L
o
g
MATERIAL DESCRIPTION
Concrete Floor
Tan, Orange SILT
Tan, Orange SILT
Tan, Orange SILT
Tan, Brown SILT
Tan, Brown SILT
Bottom of Boring
PI
D

R
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a
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i
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g
,

p
p
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0.0
0.0
0.0
0.4
0.0
0.0
De
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t
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(
f
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t
)
0
5
10
15
20
25
30
Sa
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Sa
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T
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Sheet 1 of 1
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-12B
Date(s)
Drilled 11/15/16
Drilling
Method Direct Push
Drill Rig
Type GeoProbe
Groundwater Level
and Date Measured NA
Borehole
Backfill Grout
Logged By CE
Drill Bit
Size/Type 2.5"
Drilling
Contractor EPDS
Sampling
Method(s)MacroCore
Location Hydraulic lift CIS-12 eastern post
Checked By PWL
Total Depth
of Borehole 10
Approximate
Surface Elevation
Hammer
Data
Ma
t
e
r
i
a
l

T
y
p
e
Concrete
ML
ML
ML
ML
ML
REMARKS AND OTHER TESTS
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, No Odor
Gr
a
p
h
i
c

L
o
g
MATERIAL DESCRIPTION
Concrete Floor
Tan, Orange SILT
Tan, Orange SILT
Tan, Orange SILT
Tan, Brown SILT
Tan, Brown SILT
Bottom of Boring
PI
D

R
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a
d
i
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g
,

p
p
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0.0
0.0
0.0
0.0
0.0
0.0
De
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(
f
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)
0
5
10
15
20
25
30
Sa
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Sa
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T
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Sheet 1 of 1
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Log of Boring CIS-13
Date(s)
Drilled 11/15/16
Drilling
Method Direct Push
Drill Rig
Type GeoProbe
Groundwater Level
and Date Measured NA
Borehole
Backfill Grout
Logged By CE
Drill Bit
Size/Type 2.5"
Drilling
Contractor EPDS
Sampling
Method(s)MacroCore
Location Boring adjacent to east side of found heating oil UST
Checked By PWL
Total Depth
of Borehole 10
Approximate
Surface Elevation
Hammer
Data
Ma
t
e
r
i
a
l

T
y
p
e
Concrete
ML
ML
ML
ML
ML
REMARKS AND OTHER TESTS
Dry, No Odor
Dry, No Odor
Dry, No Odor
Dry, Slight Petro Odor - No staining
Dry, No Odor
Dry, No Odor
Gr
a
p
h
i
c

L
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g
MATERIAL DESCRIPTION
Concrete Floor
Tan, SILT
Tan SILT
Tan SILT
Tan SILT
Tan Fine Sandy SILT
Bottom of Boring
PI
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a
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p
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0.0
6.7
1.6
11.9
2.0
1.3
De
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5
10
15
20
25
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Sheet 1 of 1
Project:Centerline Innes Street, LLC
Project Location:1517 E. Innes Street, Salisbury, NC
Project Number:SUMMIT No. 4333.500
Key to Log of Boring
Ma
t
e
r
i
a
l

T
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p
e
REMARKS AND OTHER TESTSGr
a
p
h
i
c

L
o
g
MATERIAL DESCRIPTIONPI
D

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a
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i
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g
,

p
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(
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1 2 3 4 5 6 7 8
COLUMN DESCRIPTIONS
1 Depth (feet): Depth in feet below the ground surface.
2 Sample Type: Type of soil sample collected at the depth interval
shown.
3 Sample Number: Sample identification number.
4 PID Reading, ppm: The reading from a photo-ionization detector,
in parts per million.
5 Material Type: Type of material encountered.
6 Graphic Log: Graphic depiction of the subsurface material
encountered.
7 MATERIAL DESCRIPTION: Description of material encountered.
May include consistency, moisture, color, and other descriptive
text.
8 REMARKS AND OTHER TESTS: Comments and observations
regarding drilling or sampling made by driller or field personnel.
FIELD AND LABORATORY TEST ABBREVIATIONS
CHEM: Chemical tests to assess corrosivity
COMP: Compaction test
CONS: One-dimensional consolidation test
LL: Liquid Limit, percent
PI: Plasticity Index, percent
SA: Sieve analysis (percent passing No. 200 Sieve)
UC: Unconfined compressive strength test, Qu, in ksf
WA: Wash sieve (percent passing No. 200 Sieve)
MATERIAL GRAPHIC SYMBOLS
Portland Cement Concrete SILT, SILT w/SAND, SANDY SILT (ML)
TYPICAL SAMPLER GRAPHIC SYMBOLS
Auger sampler
Bulk Sample
3-inch-OD California w/
brass rings
CME Sampler
Grab Sample
2.5-inch-OD Modified
California w/ brass liners
Pitcher Sample
2-inch-OD unlined split
spoon (SPT)
Shelby Tube (Thin-walled,
fixed head)
OTHER GRAPHIC SYMBOLS
Water level (at time of drilling, ATD)
Water level (after waiting)
Minor change in material properties within a
stratum
Inferred/gradational contact between strata
?Queried contact between strata
GENERAL NOTES
1: Soil classifications are based on the Unified Soil Classification System. Descriptions and stratum lines are interpretive, and actual lithologic changes may be
gradual. Field descriptions may have been modified to reflect results of lab tests.
2: Descriptions on these logs apply only at the specific boring locations and at the time the borings were advanced. They are not warranted to be representative
of subsurface conditions at other locations or times.
C:
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Figure B-1
Sheet 1 of 1
Centerlane Innes Street, LLC Phase II Environmental Site Assessment (ESA)
January 6, 2017
Cardno
Appendix D: Field Logs

fff"!'' tl / t+ / tL /0o6 Losged By '/Mt-Checked By
il,:lll% ils,(3il:,?i'" 8.2 r lisff:fl ve ,
illJ- &$E 3:li'il:"", S-^** l-Approximate
Surface Elevation
:i3'J:,:t"J:"#! r o.l ' tt trq/tt ilXltff, 4t,r c,^ou Hammer
Data
Boreho e
Backfill Location _ Clvt"-t*l
Project: Centerline Innes Street LLC
Project Location: 1517 E.Innes Street
Project Number: 4333.500
Log of Boring: CIS- Z
Sheet 1 of 1
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Project: Genterline Innes Street LLC
Project Location: 1517 E.Innes Street
Log of Boring: CIS- 2
Sheet 1 of 1
Proiect Number: 4333.500
Date(s)
Drilled It/ ttl/tt t5oo Lossed By fl^'lt-Checked By
'r:n% lts.t Drill Bit
Size/TVpe 9,t-f,"#Sff:[ v&/
Drill R g
Type CHE Drilling
Contractor f3--12n'?Approximate
Surface Elevation
:;:Hi:1"J1",Y:i 20 .7 / nttUL Sampling
l\4ethod(s)
Hammer
Data
Boreho e
Backfill Location uwL-lL
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Project: Genterline Innes Street LLC
Project Location: 1517 E.Innes Street
Project Number: 4333.500
Log of Boring: CIS- 3
Sheet 1 of 1
3lli"';' tr /tg/ tr,
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MATERIAL DESCRIPTION
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Project: Centerline Innes Street LLG
Project Location: 1517 E.Innes Street
Project Number: 4333.500
Log of Boring: CIS- f
Sheet 1 of 1
Date(s)
Drilled n/E/lt Lossed By Pt Checked By
il,:lil% t+s,4 Drill Bit
Size/Tvoe ,.2{-I|S,T3[ 3 | /
Drill R g
Tvoe Crq E Drilling
Contractor fun^-7 Approximate
Surface Elevation
Groundwater Level;ffiil'Hffi e.b.z rtlrdllt Sampling
Method(s)
Hammer
Data
Boreho e
Backfill Location Gr.rrr-rl
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Project: Centerline Innes Street LLC
Project Location: 1517 E.Innes Street
Project Number: 4333.500
Log of Boring: CIS- S
Sheet 1 of 1
Date(s)
Drilled tr /rs /u,Lossed By (F Checked By
"r:HX G.-flJ*u Drill Bit
Size/Type
Total Depth
of Borehole
?JlJ' z*ot)Drilling
Contractor
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Surface Elevat on
Groundwater Level;;;;;;;;;;;a A14 Samplrng
Method(s)
Hammer
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Borehole
Backfill Location
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Project: Genterline Innes Street LLG
Project Location: 1517 E.Innes Street
Project Number: 4333.500
Log of Boring: CIS- 6 A
Sheet 1 of 1
ffli"f' u /rs /th Logged By Checked By
il:ll:% (,., Qdoc.Drill Bit
Size/Type
Total Depth
of Borehole
illJ- 7so6 Drilling
Contractor
Approximate
Surface Elevation
Groundwater Level .
and Date Measured N A Sampling
l\4ethod(s)
Hammer
Data
Borehole
Backfill Location
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Project: Genterline Innes Street LLC
Project Location: 1517 E.Innes Street
Project Number: 4333.500
Log of Boring: CIS- 6B
Sheet 'l oI'l
3:Ef) rr /rs /ic Logged By Checked By
fl':lffi G=oQ..'b<Drill Bit
Size/TVpe
Total Depth
of BoreholeillJ' vt*Drilling
Contractor
Approximate
Surface Elevation
:i:Ti,:xl"J:"#1, ry 4 Sampling
Method(s)
Hammer
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Project: Centerline Innes Street LLC
Project Location: 1517 E.Innes Street
Log of Boring: CIS- 7A
Sheet 1 of 1
Number: 4333.500
Date(s) | rtDrirred' \l /ta /l(Logged By Checked By
il:lffi G'o, P,,o\"r.Drill Bit
Size/Tvpe
Total Depth
of Borehole
illJ' 78e>Drilling
Contractor
Approximate
Surface Elevation
Groundwater Level ,
and Date Measured l\\ A
Sampling
lVlethod(s)
Flammer
Data
Borehole
Backfill Location
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lla
Project: Genterline Innes Street LLC
Project Location: 1517 E.Innes Street
Project Number: 4333.500
Log of Boring: CIS- ?G
Sheet 1 of 1
ffli"f' l lts /ru Logged By Checked By
il,:llffi G-o e,*,2-Drill Bit
Size/Tvoe
Total Depth
of Borehole
Drill R g
Tvpe 2 5oo Drilling
Contractor
Approximate
Surface Elevation
Groundwater Level . I
and Date Measured N/v
Sampling
Method(s)
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Backfill Location
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Project: Centerline lnnes Street LLC
Project Location: 1517 E.Innes Street
Project Number: 4333.500
Log of Boring: CIS-.? A
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Size/Type
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Method(s)
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Backfill Location
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Project: Centerline Innes Street LLC
Project Location: 1517 E.Innes Street
Project Number: 4333.500
Log of Boring: CIS- (9
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Backfill Location
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Project: Centerline Innes Street LLC
Project Location: 1517 E.Innes Street
Project Number: 4333.500
Log of Boring: CIS- 1 A
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Backfill Location
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Project: Centerline Innes Street LLC
Project Location: 1517 E.lnnes Street
Project Number: 4333.500
Log of Boring: CIS-
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Backfill Location
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Project: Centerline Innes Street LLC
Project Location: 1517 E.Innes Street
Project Number: 4333.500
Log of Boring: CIS-
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Backfill Location
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Project: Centerline lnnes Street LLG
Project Location: 1517 E.Innes Street
Project Number: 4333.500
Log toBof Boring: CIS-
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Contractor
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:i:T:,:t"J*"#! c\A Sampling
lVlethod(s)
nammer
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Boreho e
Backfill LOCat On
Project: Genterline Innes Street LLC
Project Location: 1517 E.Innes Street
Project Number: 4333.500
Log of Boring: GIS- l\
Sheet 1 oI 1
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Backfill Location
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Project: Centerline Innes Street LLC
Project Location: 1517 E.Innes Street
Project Number: 4333.500
Log of Boring: CIS- tZ A
Sheet 1 oI 1
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i,:l;:% 6-o P.ou-Drill Bit
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Total Depth
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Contractor
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Method(s)
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Backfill Location
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Project: Centerline Innes Street LLG
Project Location: 1517 E.Innes Street
Log of Boring: CIS-
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Method(s)
Hammer
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Backfill Location
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Method(s)
Hammer
Borehole
Backfill Location
Project: Centerline Innes Street LLC
Project Location: 1517 E.Innes Street
Project Number: 4333.500
Log of Boring: CIS- 13Sheet 1 of 1
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GROUNDWATER SAMPLING LOG
SITE
NAME:Centerline Innes
SITE
LocAIoN: 1517 Innes Street, Salisbury, NC
wer-r No: CIS - |SAMPLEID: C/t- I -*tt^t DArE: tl llb/k
PURGING DATA
WELL
DIAMETER (inches): 2
TUBING
DIAMETER (inches): 5/8
WELL SCREEN INTERVAL
DEPTH.I6. Sfeet to J(,{teet
STATIC DEPTH
TO WATER (feet): 2O./
PURGE PUMP TYPE
OR BAILER: RtrPP
WELL VOLUME PURGE:
(only fill out if applicable)
1 WELL VOLUME = (TOTAL WELL DEPTH
=( 36'{ t..t
STATIC DEPTH TO WATER)
2O,f reet)
X WELL CAPACITY
O.147 oalons/root = 2. dX qa ons
EoUIPMENTVoLUME PURGE: 1 EQUIPMENTVoL. = PUMPVoLUME + (TUBING CAPACITY X TUBING LENGTH) + FLoWCELLVOLUME
(only fill out if applicable) - gailons + ( gailons/foot x feet) + gailons =gailons
INITIAL PUMP OR TUBING
DEPTH lN WELL (feet):
FINAL PUMP OR TUBING
DEPTH lN WELL (feet):
PURGING
INITIATED AT:
PURGING
ENDED AT:
TOTAL VOLUME
PURGED (gallons):
TME VOLUME
PURGED
(gallons)
CUMUL
VOLUME
PURGED
(gallons)
PURGE
RATE
(spm)
DEPTH
TO
WATER
pH
(standard
units)
TEMP,
(oc)
COND
(circle units)
pmnOS/Cm
or tS/cm
DISSOLVED
OXYGEN
(circle units)
mg/L or
% saturation
TURBIDITY
(NTUS)
COLOR
(describe)
ODOR
(describe)
lt30 ()2o.t 2.7lt w.1?O,3'17 d,17 ) tooo ( l6-.k/n6Vr<
6.26 7.'7l (t.?2 o.2g c .(.61 Trt a
t.b 7. t1 |t,6tr . 277 .i. 2 l-]3
L.o ?, bo tt.f n L7(q.7 76 (la^u
2,r 7.o7 20.2 .Ztt 7L ?F\.Y 7. o3 tq.qy . 2lt 1,5 2o.r
/)oo t.o lx. t 7-07 n.8 o 28a U,9 lo, I J
WELLCAPACITY(GallonsPerFoot)r 0.75"=0.o2, 1"=004; 1.25"=006; 2" =016,
TUBING INSIDE DlA. CAPACITY (Gal /Ft ): 1/8" = 0 0006: 3/16" = 0.0014: 1/4" = 0 0026:
3"=037r 4"=065: 5"=1.02, 6"=147, 12"=588
5/16"=0004; 3/8"=0006; 112" =oo10, 5/8"=0016
PURGING EQUIPMENT CODES: B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; Peristaltic Pump; O = Other (Specify)
SAMPLING DATA
SAMPLED BY (PRINT) / AFFILIATION:
eUvL '5,s*,.'-.-(-SAMPLING
lNlrlArEDAT: l)-d)SAMPLINGENDEDAT:
-PUMP OR TUBING
DEPTH lN WELL (feet):
TUBING
MATERIAL CODE:
FIELD-FILTERED: Y
Filtration Equipment Type:
FILTER SIZE: _ Fm
DUPLICATE: Y
SAMPLE CONTAINER SPECIFICATION SAMPLE PRESERVATION INTENDED
ANALYSIS AND/OR
METHOD
SAMPLING
EOUIPMENT
CODE
SAMPLE PUMP
FLOW RATE
(mL per minute)SAMPLE
ID CODE
F
CONIAINERS
I\4ATERIAL
CODE VOLUME PRESERVATIVE
USED
TOTAL VOL
ADDED lN FIELD (mL)
F NAL
nH
REMARKS:S**rtJ e ltoO /t/ 16/ t c
MATERTALCODES: AG=Amberclass; CG=Clearclass; PE=Polyethylene; PP=Polypropylene; S=Silicone; T=Teflon; O=Other(Specify)
SAMPLING EQUIPMENT CODES: APP = After Peristaltic Pump; B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump;
RFPP = Reverse Flow Peristaltic Pump; SM = Straw Method (Tubing Gravity Drain); O = Other (Specify)
GROUNDWATER SAMPLING LOG
JI IE
NAME:Centerline Innes
SITE
LocAIoN:1517 Innes Street, Salisbury, NC
WELL No:ClS - I SAMeLE lD: C I S _ Z _,/vtu)DArE: l(/k/lt
PURGING DATA
WELL
DIAMETER (inches): 2
TUBING
DIAMETER (inches): 5/8
WELL SCREEN INTERVAL
DEPrH:/( ./ feet to ]l.l reet ;;Tf,?=-t:' /6.s' | 3H1?="'.H"*'
WELL VOLUME PURGE:
(only fill out if applicable)
1 WELL VOLUME = (TOTAL WELL DEPTH -STAT|C DEPTH TO WATER)
/( . Y reet)
X WELL CAPACITY
A. /6? qattons/root = 3'/ 7=( 3C./ reet X qallons
EQUIPMENT VOLUME PURGE: 1 EQUIPMENT VOL, = PUMP VOLUME + (TUBING CAPACITY X TUBING LENGTH) + FLOW CELL VOLUME
(only fill out if applicable)
gallons+ ( Sallons/footX feet) +gallons =gailons
INITIAL PUMP OR TUBING
DEPTH lN WELL (feet):
FINAL PUMP OR TUBING
DEPTH lN WELL (feet):
PURGING
INITIATED AT:
PURGING
ENDED AT:
TOTAL VOLUME
PURGED (gallons):
TIME VOLUME
PURGED
(gallons)
CUMUL,
VOLUME
PURGED
(gallons)
PURGE
RATE
(gpm)
DEPTH
TO
WATER
pH
(standard
units)
TEMP
(oc)
COND
(circle units)
pmhos/cm
or pS/cm
DISSOLVED
OXYGEN
(circle units)
mg/L or
% saturation
TURBIDITY
(NTUs)
COLOR
(describe)
ODOR
(describe)
t 7oo ()o O.to lL.y'Lz ).o'ell ?70 q.L qt (lz,.u A6AT
t I (.f,7 27..t'7 32-7 2,.1./9r I
I 2 (c.Sf,2-3,7 . .l z-r-r.{2 6s.?
I t L. s3 23.6?,7?t-.1.67 t?.t-
ll zc:I L.l /8. I /^. <a Z3.oz , l2r 11 65-o.o V v
WELLCAPACITY(GallonsPerFoot): 0.75"=002; 1"=004; 1.25"=006; 2"=016;
TUBING INSIDE DlA. CAPACITY (Gal /Ft ): 1/8" = 0 0006; 3/15" = 0 0014: t/4" = 0 0026:
3"=037; 4"=065; 5"=102; 6"=1.47, 12"=5885/15"=0004: 3/8"=0006: 1/2"=0010; 5/8"=0.016
PURGINGEQUIPMENTCODES: B=Barler; BP=BladderPump; ESP=ElectricSubmersiblePump; PP=PeristalticPump; O=Other(Specify)
SAMPLING DATA
SAMPLED B FFILIATION:SAM (S):l^iiliiifi. t3L,)SAMPL|NG -/ENDEDAT: ,/
PUMP OR TUBING
DEPTH lN WELL (feet):
TUBING
MATERIAL CODE:
FIELD-FILTERED: Y N FILTERSIZE:
-1lm
Filtration Equipment Type: \
FIELD DECONTAMINATTON: eUrr/ln ( V) N TUBING v ( treOtac"o)DUPLICATE: v (N !)
SAMPLE CONTAINER SPECIFICATION SAMPLE PRESERVATION INTENDED
ANALYSIS AND/OR
METHOD
SAMPLING
EQUIPMENT
CODE
SAMPLE PUMP
FLOW RATE
(mL per minute)SAIVII'Lt
ID CODE
F
CONTAINERS
MATERIAL
CODE VOLUME PRESERVATIVE
USED
TOTAL VOL
ADDED IN FIELD (mL)
F NAL
nH
REMARKS
9*n'h e /l za
MATERIALCODES: AG=AmberGlass; cG=Clearclass; PE=Polyethylene; PP=Polypropylene; S=Silicone; T=Teflon; O=Other(Specify)
SAMPLING EQUIPMENT CODES: APP = After Peristaltic Pump; B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump;
RFPP = Reverse Flow Peristaltic Pump; SM = Straw Method (Tubing Gravity Drain); O = Other (Specify)
GROUNDWATER SAMPLING LOG
SITE
NAME:Centerline Innes
SITE
LocAloN:1517 Innes Street, Salisbury, NC
wELLNo:ClS -3 SAMPLEID: C/S- 3_tvr6 DArE: il/ Ie/l(
PURGING DATA
WELL
DIAMETER (inches): 2
TUBING
DIAMETER (inches): 5/8
WELL SCREEN INTERVAL
DEPTH: / /./ feet to ]1./ feet
STATIC DEPTH
rowArER (teet). 17, ?E-
PURGE PUMP TY
OR BAILER:
WELL VOLUME PURGE:
(only fill out if applicable)
1 WELL VOLUME = (TOTAL WELL DEPTH
=( 7/./ reet
STATIC DEPTH TO WATER)
/ 7, ?J- reet)
X WELL CAPACITY
, / 47 oalons/foot = 2'X k1/oailons
EQUIPMENT VoLUME PURGE: 1 EQUIPMENT VOL. = PUMP VOLUME + (TUBING CAPACITY X TUBING LENGTH) + FLOW CELL VOLUME
(onlyfill outifapplicable) - gailons+( gailons/footx feet) + gailons =gailons
INITIAL PUMP OR TUBING
DEPTH IN WELL (feet):
FINAL PUMP OR TUBING
DEPTH IN WELL (feet):
PURGING
INITIATED AT:
PURGING
ENDED AT:
TOTAL VOLUME
PURGED (gallons):
TIME VOLUME
PURGED
(gallons)
CUMUL,
VOLUME
PURGED
(gallons)
PURGE
RATE
(spm)
DEPTH
TO
WATER
pH
(standard
units)
TEMP
(oc)
COND
(circle units)
pmhos/cm
or pS/cm
DISSOLVED
OXYGEN
(circle units)
mg/L or
o/^ crtr rrrtian
TURBIDITY
(NrUs)
COLOR
(describe)
ODOR
(describe)
l'{oo o o .20 t7.qf -7.2Y 27.q1 .22 z q.oG .r67 (.1 ^.lr n6l/at
I 7. 21 21,.13 , zr.l %rz 167 t,
I 2.7. 'a zq,of l,c 9.79 ty Clan
5 -7.17 2t. ev l.ro 6.t7 I Y.r
lq16 ,r-l )\.7'7.71 2z-ze -tr{ I a. ol 8.6 \7
WELLCAPACITY(GallonsPerFoot): 0.75"=002; 1"=004; 1.25"=006; 2"=016;
TUBING INSIDE DlA. CAPACITY (Gal /Ft ): 1/8" = 0 0006: 3/16" = 0 0014: 1/4" = 0 0026:
3"=037; 4"=065; 5"=102., 6"='l 47, 12"=588
5/16" = 0 004: 3/8" = 0 006; '112" =0010, 5/8" = 0 016
PURGINGEQUIPMENTCODES: B=Bailer; BP=BladderPump; ESP=ElectricSubmersiblePump; PP=PeristalticPump; O=Other(Specify)
SAMPLING DATA
SAMPL SAMPLING
lNlrlArED et /tl) d
SAMPLING
ENDED AT:
PUMP OR TUBING
DEPTH IN WELL (feet)
TUBING
MATERIAL CODE:
FIELD-FILTERED: Y
Filtration Equipment Typ
FILTER SIZE: _ pm
FIELD DECONTAMINATION: PUMP( N TUBING v (ru lreptace-91)DUPLICATE: Y
SAMPLE CONTAINER SPECIFICATION SAMPLE PRESERVATION INTENDED
ANALYSIS AND/OR
METHOD
SAMPLING
EQUIPMENT
UUUE
SAMPLE PUMP
FLOW RATE
(mL per minute)SAMPLE
ID CODE
T
CONTAINERS
MATERIAL
CODE VOLUME PRESERVATIVE
USED
TOTAL VOL
ADDED IN FIELD (mL)
FINAL
nH
REMARKS:
3,nqu/-a /qr)
MATERIALCODES: AG=Amberclass; CG=Clearclass; PE=Polyethylene; PP=Polypropylene; S=Silicone; T=Teflon; O=Other(Specify)
SAMPLING EQUIPMENT CODES: APP = After Peristaltic Pump; B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump;
RFPP = Reverse Flow Peristaltic Pump; SM = Straw Method (Tubing Gravity Drain); O = Other (Specify)
GROUNDWATER SAMPLING LOG
Jt ttr
NAME:Centerline Innes
SITE
LocAloN: 1517 Innes Street, Salisbury, NC
wELL No: CIS - q SAMPLElD: (t 5- al _ltttt DArE: ll /lL/l(
PURGING DATA
WELL
DIAMETER (inches): 2
TUBING
DIAMETER (inches):5t8
WELL SCREEN INTERVAL
DEPrH: Il. jl feetto, I . I feel
STATIC DEPTH
To WATER (teet): l(, 9'
PURGE PUMP T
OR BAILER: f
WELL VOLUME PURGE:
(only fill out if applicable)
1 WELL VoLUME = (TOTAL WELL DEPTH -STAT|C DEPTH TO WATER)
k..f feet)
X WELL CAPACITY
, /(7 oattons/foot = 2'q=( 7/-7 reet X oailons
EQUIPMENT VOLUME PURGE: 1 EQUIPMENT VOL. = PUMP VOLUME + (TUBING CAPACITY X TUBING LENGTH) + FLOW CELL VOLUME
(only fill out if applicable) - gailons + ( gailons/foot X feet) + garons = garons
INITIAL PUMP OR TUBING
DEPTH IN WELL (feet):
FINAL PUMP OR TUBING
DEPTH IN WELL (feet):
PURGING
INITIATED AT:
PURGING
ENDED AT:
TOTAL VOLUME
PURGED (gallons):
TME VOLUME
PURGED
(gallons)
CUMUL
VOLUME
PURGED
(gallons)
PURGE
RATE
(gpm)
DEPTH
TO
WATER
pH
(standard
units)
TEMP
(oc)
COND
(circle units)
IrmnOS/Cm
or pS/cm
DISSOLVED
OXYGEN
(circle units)
mg/L or
% saturation
TURBIDITY
(NTUs)
COLOR
(describe)
ODOR
(describe)
lt60 ()h ,20 t.9 (.75-22.6'{,277 il. zc fl Ck-*t*14,
I I 6.c( I 2t.7'. Lr"(.rr rrrlz(.16 2//, t.t r Lk6 /.LK tK. b
ls36 3 22.t 6."7 26.7>, Zc4 /:.76 ,.y J v/
WELLCAPACITY(GallonsPerFoot): 0.75"=002, 1"=004; 1.25"=006; 2"=016;
TUBING INSIDE DlA. CAPACITY (Gal /Ft ): 1/8" = 0 0006: 3/16" = 0 0014: 1/4" = 0 0026:
3"=037i 4"=065; 5"=102, 6"=I47, 12"=5.885/16"=0004: 3/8"=0006: 112" =0.010, 5/8"=0016
PURGINGEQUIPMENTCODES: B=Bailer; BP=BladderPump; ESP=ElectricSubmersiblePump; PP=PeristalticPump; O=Other(Specify)
SAMPLING DATA
SAMPLED ILIATION:SAMPLING
lNlrlArED Ar: /.tJO SAMPLING
ENDED Ar: /tr9-6
PUMP OR TUBING
DEPTH lN WELL (feet):
TUBING
MATERIAL CODE:
FIELD-FILTERED: Y
Filtration Equipment TVp
FILTER SIZE: _ pm
DUPLICATE: ( N
SAMPLE CONTAINER SPECIFICATION SAMPLE PRESERVATION INTENDED
ANALYSIS AND/OR
METHOD
SAMPLING
EQUIPMENT
CODE
SAMPLE PUMP
FLOW RATE
(mL per minute)SAMPLE
ID CODE
F
CONIAINERS
IVIATERIAL
CODE VOLUME PRESERVATIVE
USED
TOTAL VOL
ADDED lN FIELD (mL)
F NAL
PH
REMARKS:
9,^--rtf- e /5- 30 /fs-o
MATERIALGODES: AG=AmberGlass; CG=ClearGlass; PE=Polyeihylene; PP=Polypropylene; S=Siliconet T=Teflon; O=Other(Specify)
SAMPLING EQUIPMENT'CODES: APP = After Peristaltic Pump; B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump;
RFPP = Reverse Flow Peristaltic Pump; SM = Straw Method (Tubing Gravity Drain); O = Other (Specify)
PREPARTD
BY:
DATE:
illL
CHECKED BY:
(wt-
PROJECT NO:
SHEET NO
OF
SUMMIT
t--1_
lt
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I
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