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ARCADIS
Infrastructure · Water · Environment· Buildings
Mr. James Brown
NCDENR-UST Section
Fayetteville Regional Office
225 Green Street, Suite 714, Systel Building
Fayetteville, North Carolina 28301
Subject:
1st Semi-Annual Corrective Action Plan Monitoring Report-2014
Former ExxonMobil Facility #40962
5001 Raeford Road
Fayetteville, North Carolina 28304
Incident Number: 3483
Risk Classification: Intermediate
Dear Mr. Brown:
On behalf of ExxonMobil Environmental Services (EMES), ARCADIS G&M of North
Carolina, Inc. (ARCADIS) is submitting the attached 1st Semi-Annual Corrective
Action Plan Monitoring Report-2014 dated May 13, 2014 for the above referenced
site. An electronic copy of this report including the associated laboratory analytical
report is included with the attached CD.
Please contact me at (276) 322-3879 extension 23807 with any questions or
concerns related to the Report or this incident number.
Sincerely,
Imagine the result
ARCADIS G&M of North Carolina,
Inc.
801 Corporate Center Drive
Suite 300
Raleigh
North Carolina 27607
Tel919 854 1282
Fax 919 854 5448
www.arcadis-us.com
Environment
Date:
May 14, 2014
Contact:
Jon Farley
Phone:
276.322.3879 X 23807
Email:
Jon.Farley@arcadis-us.con
Our ref:
80085851 .0025
ARCADIS G&M of North Carolina,
Inc.
NC Engineering License # C-1869
NC Surveying License # C-1869
ARCADIS
Attachments:
Attachment A-1st Semi-Annual Corrective Action Plan Monitoring Report-2014
(CD)
Copies:
Ms. Jewel Cox-EMES
File -EM 40962
Mr. James Brown
May 14, 2014
Page:
2/2
~ARCADIS
Attachment A
Imagine the result
ExxonMobil Environmental Services
Corporation
1st Semi-Annual Corrective
Action Plan Monitoring Report
- 2014
Former ExxonMobil Facility #40962 5001 Raeford Road
Fayetteville, Cumberland County, North Carolina
Groundwater Incident # 3483
May 2014
~ARCADIS
1st Semi-Annual Corrective
Action Plan Monitoring Report-
2014
Former ExxonMobil Facility
#40962
Prepared for:
ExxonMobil Environmental Services
Ms. Jewel Cox-Project Manager
1016 W. Poplar Avenue
Suite 106 #232
Collierville, Tennessee 38017
Prepared by:
ARCADIS G&M of North Carolina, Inc.
801 Corporate Center Drive
Suite 300
Raleigh, North Carolina 27607
Tel919.854.1282
Fax 919.854.5448
www.arcadis-us.com
Our Ref.:
80085851.0025
Date:
May 13, 2014
This document is intended only for the use
of the individual or entity for which it was
prepared and may contain information that
is privileged, confidential and exempt from
disclosure under applicable law. Any
dissemination, distribution or copying of
this document is strictly prohibited.
~ARCADIS 1"1 Semi-Annual Corrective
Action Plan Monitoring
Report -2014
15T SEMI-ANNUAL CORRECTIVE ACTION PLAN MONITORING REPORT-2014
Former Exxon Mobil Facility #40962
5001 Raeford Road
Fayetteville, Cumberland County, North Carolina, 28304
Latitude 35° 03' 31" Longitude 78° 58' 13"
(Reference Figure 1)
Groundwater Incident#:
Risk Classification:
Reason for Risk Classification:
Land Use Category:
Source of Release:
Date of Release Discovery:
Estimated Quantity of Release:
Cause of Release:
Responsible Party:
Property Owners:
3483
Intermediate
Free product present on site
Commercial
Former gasoline UST system(s)
July 1987
Unknown
Leaking product line discovered
during tightness testing
ExxonMobil Corporation
Environmental Service Company
Attn: Ms. Jewel Cox
1016 W. Poplar Avenue
Suite 106 #232
Collierville, TN 38017
(901) 850-9009
Li'l Thrift Food Mart
1007 Arsenal Avenue
Fayetteville, North Carolina 28305
(910) 433-4490
, a Professional Engineer for ARCADIS G&M of North
Carolina, Inc. do certify that the information contained in this report is correct and accurate to the best of my
knowledge. ARCADIS G&M of North Carolina, Inc. is licensed to practice geology and engineering in North
Carolina. The license numbers of the company are C-155 (geology) and C-1869 (engineering).
i
1st Semi-Annual Corrective
Action Plan Monitoring
Report – 2014
Executive Summary
During the first half of 2014, on behalf of ExxonMobil Environmental Services (EMES),
ARCADIS G&M of North Carolina (ARCADIS) completed monthly manual free product
monitoring events, and a liquid level monitoring and sampling event at the former
ExxonMobil Facility #40962 located at 5001 Raeford Road, Fayetteville, Cumberland
County, North Carolina (the site). The objective of the groundwater monitoring and
sampling program is to determine concentrations of dissolved-phase chemicals of concern
(COCs) and maintain compliance with the North Carolina Department of Environment and
Natural Resources (NCDENR) Underground Storage Tank (UST) Program requirements for
the site.
On March 26, 2014 three (3) groundwater monitoring wells, MW-11D, MW-14, and MW-15,
and three (3) soil vapor extraction (SVE) wells, SVE-1/MW-9, SVE-2, and SVE-3, were
gauged during the monitoring event to determine depth to bottom (DTB), depth to water
(DTW), and depth to product (DTP), if present. Depth to water ranged from 22.48 feet
below top of well casing (btoc) in groundwater monitoring well MW-11D to 27.81 feet btoc in
SVE well SVE-2. Free product was not detected during the March 26, 2014 gauging event
in any wells. Groundwater flow direction was observed to be toward the southeast which is
consistent with historical observed groundwater flow direction.
Groundwater samples were collected from SVE wells SVE-1/MW-9 and SVE-2 on March
26, 2014. The maximum concentrations of selected dissolved-phase COCs are presented
below:
Maximum Groundwater Concentrations (March 26, 2014)
Chemical of Concern
(COC)
Monitoring
Well ID
Concentration
(µg/L)
GCL Standard
(µg/L)
Benzene SVE-2 229 5,000
Toluene SVE-2 24,100 260,000
Ethylbenzene SVE-2 3,580 84,500
Xylenes (total) SVE-2 31,400 85,500
Methyl tert-Butyl Ether SVE-2 354 20,000
Diisopropyl ether MW-9/SVE-1 4.24 70,000
Naphthalene SVE-2 1,290 6,000
1,2,4-Trimethylbenzene MW-9/SVE-1 5,830 28,500
1,3,5-Trimethylbenzene SVE-2 1,550 25,000
Tetrachloroethene (PCE) MW-9/SVE-1 1,820 700
Note: Concentrations in Bold exceed the applicable GCL
µg/L = micrograms per liter
No dissolved-phase concentrations of COCs derived from gasoline constituents were
detected in groundwater samples collected at the site on March 26, 2014 in concentrations
exceeding the applicable North Carolina Gross Contaminant Level (GCL) standards.
ii
1st Semi-Annual Corrective
Action Plan Monitoring
Report – 2014
Dissolved-phase concentrations of tetrachloroethene (PCE) were detected in
groundwater samples collected at SVE well MW-9/SVE-1 exceeding the applicable
North Carolina GCL standard.
Dissolved-phase concentrations of PCE at the site can be attributed to the chlorinated
solvent release at the former dry cleaner property located adjacent to the site across
Raeford Road. This property has been assigned NCDENR Dry-Cleaning Solvent Act
(DCSA) Identification Number DC260006 and is located upgradient with respect to
groundwater flow direction from the site.
Monthly free product monitoring visits were conducted on January 8, 2014, February 5,
2014, March 12, 2014, and April 9, 2014. Results of the monthly monitoring and manual
recovery events indicated the following:
· January 8, 2014: Free product was not detected at either SVE wells SVE-2 or
SVE-1/MW-9 during this event.
· February 5, 2014: Free product was not detected at either SVE wells SVE-2 or
SVE-1/MW-9 during this event.
· March 12, 2014: Free product was not detected at either SVE wells SVE-2 or SVE-
1/MW-9 during this event.
· April 9, 2014: Free product was not detected at either SVE wells SVE-2 or SVE-
1/MW-9 during this event.
ARCADIS recommends the continuation of monthly free product monitoring events at SVE
wells SVE-1/MW-9 and SVE-2. The last detection of free product at the site was at SVE-
1/MW-9 on September 23, 2013. The next semi-annual groundwater monitoring and
sampling event is scheduled for September 2014. All groundwater monitoring wells and
SVE wells associated with the site will be gauged to check for the presence of free product
and to determine the potentiometric surface of the site. ARCADIS will collect groundwater
samples from SVE wells SVE-1/MW-9 and SVE-2 to be analyzed for volatile organic
compounds (VOCs) by Standard Method (SM) 6200B. A groundwater monitoring report
detailing the results of the groundwater monitoring and sampling and the monthly free
product monitoring events will be submitted to NCDENR for review within 45 days of receipt
of the laboratory analytical report.
If no free product is detected through September 2014, and gasoline-constituent dissolved-
phase COCs are not detected in September 2014 in concentrations exceeding the
applicable North Carolina GCL Standards, ARCADIS will respectfully recommend a
reclassification of the risk ranking for the site from Intermediate to Low, the completion and
filing of a Notice of Residual Petroleum (NORP) with the Cumberland County Register of
Deeds, and that No Further Action (NFA) status be granted for the subject incident number.
iii
1st Semi-Annual Corrective
Action Plan Monitoring
Report – 2014
Table of Contents
Executive Summary ii
1.0 Site History and Characterization 1
2.0 Free Product 2
3.0 Groundwater Monitoring 3
3.1 Groundwater Gauging 3
3.2 Groundwater Sampling 3
3.3 Groundwater Analytical Results 4
4.0 Site Remediation 5
4.1 Site Remediation to Date 5
5.0 Conclusions and Recommendations 6
Figures
1. Site Location Map
2. Site Map
3. Potentiometric Surface Map – March 26, 2014
4. Groundwater Analytical Map – March 26, 2014
5. Tetrachloroethene Isoconcentration Map – March 26, 2014
Tables
1. Groundwater Elevation Data
2. Groundwater Analytical Data
Appendices
A. Laboratory Analytical Report and Chain-of-Custody
1
1st Semi-Annual CAP
Monitoring Report - 2014
1.0 Site History and Characterization
Former ExxonMobil (Exxon) Facility #40962, located at 5001 Raeford Road, Fayetteville,
Cumberland County, North Carolina is currently occupied by Li’l Thrift Food Mart, a retail
gasoline facility and convenience store. In 1987, a release was discovered from a product
line during a tightness test. Three 6,000-gallon gasoline underground storage tanks
(USTs), one 570-gallon fuel oil UST, and one 1,000-gallon used oil UST were removed,
along with associated piping and dispensers, in February of 1992.
Through October 1999, the site underwent active remediation by soil vapor extraction
(SVE). The SVE system was connected to monitoring wells MW-9, MW-14 and six vapor
extraction wells (VE-1 through VE-6). On October 27, 1999, the SVE system was shut
down due to a breach in the subsurface piping. The SVE equipment had been damaged as
a result of large quantities of sand moving through the system. ExxonMobil continued hot
spot remediation efforts by conducting a series of aggressive fluid vapor recovery (AFVR)
events. Additionally, a passive product recovery device was installed in monitoring well
SVE-1/MW-9 until 1999.
In August 2000, the SVE system was modified and re-connected to monitoring well MW-14
due to high concentrations of dissolved-phase benzene in the monitoring well. Free product
was detected in monitoring wells SVE-1/MW-9 and MW-14. Subsequently, SVE-1/MW-9
was re-connected to the SVE system in August 2002. The SVE system operated at
monitoring wells SVE-1/MW-9 and MW-14 from August 2002 until May 2005, when the
system was shut down due to damaged SVE piping once again. A mobile multi-phase
extraction (MMPE) event was conducted in May 2009. Two (2) additional SVE wells (SVE-
2 and SVE-3) were also installed in 2009.
The site is located in a commercially developed area of Fayetteville within the city limits.
Topography at the site is generally flat with an average grade of approximately 1.0% to the
northwest. Soils at the site generally consist of sandstone and sandy mudstone, with clays
present. The water table occurs at depths of 11 to 31 feet below ground surface (bgs) and
groundwater generally flows to the southeast in the vicinity of the site. The nearest surface
water body to the site is Beaver Creek, located approximately 4,200 feet to the southwest.
On October 23, 2011, an updated potable well survey was submitted to NCDENR. The
updated potable well survey indicated that two potable wells were located upgradient of the
site. Based on an evaluation of the historic potentiometric/groundwater flow direction and
the lack of off-site impacts, ARCADIS determined that impacts to the upgradient potable
wells would not occur. After reviewing the results of the updated potable well survey,
NCDENR lowered the site risk classification from High to Intermediate. As an intermediate
risk site, groundwater analytical cleanup standards will be held to the North Carolina Gross
2
1st Semi-Annual CAP
Monitoring Report - 2014
Contaminant Levels (GCLs). A Site Location Map is presented in Figure 1 and a Site Map
is shown as Figure 2.
2.0 Free Product
From June 1996 to present, free product has been historically observed in groundwater
monitoring wells MW-1 and MW-14 and SVE wells SVE-1/MW-9, SVE-2 and SVE-3 at
maximum thicknesses of 0.01 feet, 2.00 feet, 2.63 feet, 3.12 feet, and 0.07 feet,
respectively.
Monthly free product monitoring was conducted at the site during the first half of the 2014
monitoring period. SVE wells SVE-1/MW-9 and SVE-2 were gauged monthly to determine
depth to bottom (DTB), depth to water (DTW) and depth to product (DTP), if present.
· January 8, 2014: Free product was not detected at either
SVE wells SVE-2 or SVE-1/MW-9 during this event.
· February 5, 2014: Free product was not detected at either
SVE wells SVE-2 or SVE-1/MW-9 during this event.
· March 11, 2014: Free product was not detected at either SVE
wells SVE-2 or SVE-1/MW-9 during this event.
· April 9, 2014: Free product was not detected at either SVE
wells SVE-2 or SVE-1/MW-9 during this event.
Free product has historically been recovered by manual bailing methods using a
polyethylene bailer and nylon rope, and by placing petroleum absorbent socks in the SVE
wells to facilitate passive free product recovery at the completion of the manual bailing
activities. Recovered free product was stored in a dedicated 55-gallon department of
transportation (DOT) approved steel drum and was characterized as non-hazardous.
Free product was last detected at the site at SVE well MW-9/SVE-1 on September 23,
2014 at a maximum apparent thickness of 0.12 feet. Current and historical groundwater
elevations along with free product thickness data are summarized in Table 1.
3
1st Semi-Annual CAP
Monitoring Report - 2014
3.0 Groundwater Monitoring
3.1 Groundwater Gauging
On March 26, 2014, ARCADIS G&M of North Carolina, Inc. (ARCADIS) personnel gauged
three (3) groundwater monitoring wells MW-11D, MW-14, and MW-15, and three (3) SVE
wells, SVE-1/MW-9, SVE-2 and SVE-3. Groundwater monitoring wells MW-12, MW-13,
MW-16, and MW-20 were could not be located during the March 26, 2014 gauging event.
Groundwater gauging was conducted with an oil/water interface probe (IP) prior to purging
and sampling to determine DTB, DTW and DTP, if present. The IP and attached tape,
marked in 0.01-foot increments, was properly decontaminated before each use with
Alconox soap and rinsed with distilled water. The DTW was measured from the marked
survey point on the top of the well casing (TOC). All measurements were recorded to the
nearest 0.01-foot increment. Current and historical groundwater elevations are summarized
in Table 1.
Depths to water from the March 26, 2014 groundwater gauging event ranged from 22.48
feet below top of well casing (btoc) in groundwater monitoring well MW-11D to 27.81 feet
btoc in soil vapor extraction well SVE-1. Free product was not detected during the March
26, 2014 groundwater gauging event.
A potentiometric surface map showing groundwater elevations for all groundwater
monitoring wells gauged is presented as Figure 3. Groundwater flow direction was
observed to be toward the southeast which is consistent with historical observed
groundwater flow direction.
3.2 Groundwater Sampling
On March 26, 2014, soil vapor extraction wells SVE-1/MW-9 and SVE-2 were purged of
stagnant water. Prior to purging, the amount of water to be removed was calculated using
the following formula:
3.1415 x r2 x (TD – DTW) x 7.481 = gallons of water (1 well volume)
Where: r = radius of well (in feet)
TD = total depth of well (in feet)
DTW = depth to water (in feet)
In order to ensure that the water in the SVE well after purging was representative of the
water in the aquifer, a minimum of three well volumes was removed. Groundwater
monitoring wells that did not generate three well volumes of water were bailed dry and then
4
1st Semi-Annual CAP
Monitoring Report - 2014
given sufficient time to allow for recharging. All sampling tasks were completed within 24
hours of purging.
Groundwater samples were obtained from soil vapor extraction wells SVE-1/MW-9 and
SVE-2 using a disposable polyethylene bailer and new nylon rope. All groundwater
samples were placed in laboratory-supplied containers and shipped on wet ice to
TestAmerica, Inc. in Nashville, Tennessee, for analysis of volatile organic compounds
(VOCs) by Standard Method (SM) 6200B. Groundwater samples submitted for VOC
analysis were placed in triplicate 40-milliliter (mL) volatile organic analysis (VOA) glass vials
with Teflon-lined septa screw caps preserved with hydrochloric acid (HCl). Laboratory
analytical results and chain-of-custody documentation are included as Appendix A.
3.3 Groundwater Analytical Results
Analytical data from the March 26, 2014 groundwater sampling event indicated the
following:
· Dissolved-phase concentrations of tetrachloroethene (PCE) were detected in
concentrations exceeding the applicable North Carolina Gross Contaminant Level
(GCL) Standard (700 microgram per liter (µg/L)) at SVE well MW-9/SVE-1 at 1,820
µg/L.
Dissolved-phase concentrations of PCE at the site can be attributed to the chlorinated
solvent release at the former dry cleaner property located adjacent to the site across
Raeford Road. This property has been assigned NCDENR Dry-Cleaning Solvent Act
(DCSA) Identification Number DC260006 and is located upgradient with respect to
groundwater flow direction from the site.
Current and historical groundwater analytical data is presented in Table 2. A groundwater
analytical map is presented as Figure 4. An isoconcentration map depicting the dissolved-
phase extent of PCE at the site in included as Figure 5. The Laboratory analytical results
and chain-of-custody documentation are included as Appendix A
The maximum dissolved phase concentrations for select COCs detected on March 26,
2014 are listed in the table below:
5
1st Semi-Annual CAP
Monitoring Report - 2014
Maximum Groundwater Concentrations (March 26, 2014)
Chemical of Concern
(COC)
Monitoring
Well ID
Concentration
(µg/L)
GCL Standard
(µg/L)
Benzene SVE-2 229 5,000
Toluene SVE-2 24,100 260,000
Ethylbenzene SVE-2 3,580 84,500
Xylenes (total) SVE-2 31,400 85,500
Methyl tert-Butyl Ether
(MTBE)
SVE-2 354 20,000
Diisopropyl ether (IPE) MW-9/SVE-1 4.24 70,000
Naphthalene SVE-2 1,290 6,000
1,2,4-Trimethylbenzene MW-9/SVE-1 5,830 28,500
1,3,5-Trimethylbenzene SVE-2 1,550 25,000
Tetrachloroethene (PCE) MW-9/SVE-1 1,820 700
Note: Concentrations in Bold exceed the applicable GCL
µg/L = micrograms per liter
4.0 Site Remediation
4.1 Remediation Activities to Date
Summarized in the table below is a chronology of remediation activities performed at the
site to date:
6
1st Semi-Annual CAP
Monitoring Report - 2014
Remediation Activities to Date
Date Activity
1987 to 1998 Manual and passive recovery and SVE System
operated – 893.5 pounds (lbs.) of TPH recovered.
August 2000 – May 2005 SVE system continually operated.
9/28/1999 AFVR event – 2.97 lbs. of TPH and 1,226 gallons of
water recovered.
6/1/2009 MMPE Event – 198.77 lbs. of TPH and 6,880 gallons
of water recovered.
10/19/2009 MMPE Event – 143.90 lbs. of TPH and 450 gallons of
water recovered.
6/28/2011 AFVR Event – 94.81 lbs. of TPH and 886 gallons of
water recovered.
7/27/2011 AFVR Event – 27.98 lbs. of TPH and 886 gallons of
water recovered.
8/25/2011 AFVR Event – 59.47 lbs. of TPH and 1,522 gallons of
water recovered.
9/19/2011 AFVR Event – 37.04 lbs. of TPH and 1,702 gallons of
water recovered.
10/23-27/2011 AFVR Event – 306.12 lbs. of TPH and 13,641 gallons
of water recovered.
8/7/2012 AFVR Event – 55.97 lbs. of TPH and 1,227 gallons of
water recovered.
8/13/2013 AFVR Event – 15.35 lbs. of TPH and 1,226 gallons of
water recovered.
5.0 Conclusions and Recommendations
Monthly free product monitoring visits were conducted during the first half of 2014 on
January 8, 2014, February 5, 2014, March 12, 2014 and April 9, 2014. Free product was
not detected during any of the monthly visits. Free product was last detected at the site on
September 23, 2013 at SVE well MW-9/SVE-1 at a maximum apparent thickness of 0.12
feet.
7
1st Semi-Annual CAP
Monitoring Report - 2014
No dissolved-phase concentrations of COCs derived from gasoline constituents were
detected in groundwater samples collected at the site on March 26, 2014 in concentrations
exceeding the applicable North Carolina Gross Contaminant Level (GCL) standards.
Dissolved-phase concentrations of PCE were detected in groundwater samples collected at
SVE well MW-9/SVE-1 exceeding the applicable North Carolina GCL standard.
Dissolved-phase concentrations of PCE at the site can be attributed to the chlorinated
solvent release at the former dry cleaner property located adjacent to the site across
Raeford Road. This property has been assigned NCDENR Dry-Cleaning Solvent Act
(DCSA) Identification Number DC260006 and is located upgradient with respect to
groundwater flow direction from the site.
ARCADIS recommends the continuation of monthly free product monitoring events at SVE
wells SVE-1/MW-9 and SVE-2. The next semi-annual groundwater monitoring and
sampling event is scheduled for September 2014. All groundwater monitoring wells and
SVE wells associated with the site will be gauged to check for the presence of free product
and to determine the potentiometric surface of the site. ARCADIS will collect groundwater
samples from SVE wells SVE-1/MW-9 and SVE-2 to be analyzed for VOCs by SM 6200B.
A groundwater monitoring report detailing the results of the groundwater monitoring and
sampling and the monthly free product monitoring events will be submitted to NCDENR for
review within 45 days of receipt of the laboratory analytical report.
If free product is not detected through September 2014, and gasoline-constituent dissolved-
phase COCs are not detected in September 2014 in concentrations exceeding the
applicable North Carolina GCL Standards, ARCADIS will respectfully recommend a
reclassification of the risk ranking for the site from Intermediate to Low, the completion and
filing of a Notice of Residual Petroleum (NORP) with the Cumberland County Register of
Deeds, and that No Further Action (NFA) status be granted for the subject incident number.
~ARCADIS
Figures
REFERENCE: BASE MAP USGS 7.5. MIN. TOPO. QUAD., FAYETTEVILLE, NORTH CAROLINA, 1957, PHOTOREVISED 1987.
Approximate Scale: 1 in. = 2000 ft.
0 2000'4000'
SITE LOCATION
NORTH CAROLINA
SITE LOCATION MAP
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AREA
LOCATION
EXXONMOBIL REFINING AND SUPPLY COMPANY
FORMER EXXONMOBIL FACILITY #40962
5001 RAEFORD ROAD
FAYETTEVILLE, NORTH CAROLINA1ST SEMI-ANNUAL CORRECTIVE ACTION PLAN
MONITORING REPORT - 2014
SITE MAP
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FIGURE
EXXONMOBIL REFINING AND SUPPLY COMPANY
FORMER EXXONMOBIL FACILITY #40962
5001 RAEFORD ROADFAYETTEVILLE, NORTH CAROLINA
1ST SEMI-ANNUAL CORRECTIVE ACTION PLAN
MONITORING REPORT - 2014
2
MW20
0
AUTO ZONE
Al1 (1)
' ' '
VEs !, ~MW1
' ' ~AI2
' ' .\VE5
' ' I I
),. ......... ....... \ ..... r. \
..... 'IU \ .,..,.,.. MW11D \ SYSTEM~ \~(.,. ~9-~ \
PIPING .,.,.. ... , \ r:)\':fVYi<'OS 6J \
........ \ ' ,.:;\..'i>l ..1 ~'1 .,. \ ~ VE4 ----,...,..,., ' \~ N'-,. \ \ \AI3 ..-\_~15 \ ~14 VE3 \ -~W9/SVE1 w ' 1.1) A...,. ... .....-.,""
\ _.CI ---\
VE2.\. .,.'!""2 ---I ..,.., fi>''~l I '"'.., • .,. 5\IE2 I FORMER I
\ DISPENSER \
\ ISLANDS \
\ I
I '~-
m
9
0
(()
~
~
--OHE --
-ST--ST--
NOTE:
LEGEND:
CATCH BASIN
UTILITY POLE
MONITORING WELL
AIR SPARGE WELL
VAPOR EXTRACTION WELL
ABANDONED/DESTROYED WELL
REMEDIATION TRENCH
OVERHEAD ELECTRIC LINE
UNDERGROUND STORM SEWER LINE
MONITORING WELLS MW1 AND MW17 WERE
ABANDONED ON 5/24/2012 AS PART OF
ROAD CONSTRUCTION ACTIVITIES.
0 40' 80'
GRAPHIC SCALE
~ARCADIS
POTENTIOMETRIC SURFACE MAP
MARCH 26, 2014
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FIGURE
EXXONMOBIL REFINING AND SUPPLY COMPANY
FORMER EXXONMOBIL FACILITY #40962
5001 RAEFORD ROADFAYETTEVILLE, NORTH CAROLINA
1ST SEMI-ANNUAL CORRECTIVE ACTION PLAN
MONITORING REPORT - 2014
3
MW20 ~(NL)
AUTO ZONE
LEGEND:
m CATCH BASIN
9 UTILITY POLE
~ MONITORING WELL
(() AIR SPARGE WELL
~ VAPOR EXTRACTION WELL
~ ABANDONED/DESTROYED WELL
--OHE --
REMEDIATION TRENCH
OVERHEAD ELECTRIC LINE
-ST--ST--UNDERGROUND STORM SEWER LINE
(472.15) GROUNDWATER ELEVATION
471 .00 -------ESTIMATED GROUNDWATER ELEVATION
CONTOUR (DASHED WHERE INFERRED)
•
(NS)
(NL)
GROUNDWATER FLOW DIRECTION
NOT SURVEYED
NOT LOCATED
NOTES:
1. MONITORING WELLS MW1 AND MW17
WERE ABANDONED ON 5/24/2012 AS
PART OF ROAD CONSTRUCTION
ACTIVITIES.
2. GROUNDWATER MONITORING WELL
MW-11D IS A DEEP WELL AND WAS
NOT UTILIZED TO DEVELOP
POTIENTIOMETRIC SURFACE.
0 40' 80'
GRAPHIC SCALE
~ARCADIS
5,000
260,000
84,500
85,500
20,000
70,000
6,000
28,500
25,000
700
BOLD
1,820
GROUNDWATER ANALYTICAL MAP
MARCH 26, 2014
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D
FIGURE
EXXONMOBIL REFINING AND SUPPLY COMPANY
FORMER EXXONMOBIL FACILITY #40962
5001 RAEFORD ROADFAYETTEVILLE, NORTH CAROLINA
1ST SEMI-ANNUAL CORRECTIVE ACTION PLAN
MONITORING REPORT - 2014
4MICROGRAMS PER LITER
(µg/L)
TETRACHLORO ETHYLENE (PCE)
ISOCONCENTRATION MAP
MARCH 26, 2014
IM
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FIGURE
EXXONMOBIL REFINING AND SUPPLY COMPANY
FORMER EXXONMOBIL FACILITY #40962
5001 RAEFORD ROADFAYETTEVILLE, NORTH CAROLINA
1ST SEMI-ANNUAL CORRECTIVE ACTION PLAN
MONITORING REPORT - 2014
5
MW20
0(NL)
AUTO ZONE
Al1 (1)
' ' ' VEs !, ~MW1
' ' ~AI2
' ' .\VE5
' ' I I
),. ......... ....... \ ..... r. \
..... 'IU \ SYSTEM~ \ ,.,..,..,.,.. M~1D \ PIPING _.-,~ 'Y.-~9C ~ \ ,.. .,. ,.. \ \ r;:l:f t>-~QS ~ \
.......... \ \~'""'-_ ..... > ~ \ .....
.,. .. ' ' \ 4 .e---
... : ' \ ,~~~W9~VE1 \ \ Al4 VE3~~., 'I I~ ~ \ (}) ,k ,.. ..... -1 I (1 ,820)
Al5 .\. "" --~ .., VE2ft._.,...,.~ I _, \
...... ...... SVE2 \ FC'iRtiER \
(279) \ DISPENSER \
\ ISLANDS \
\ I
I '~-
LEGEND:
m CATCH BASIN
9 UTILITY POLE
0 MONITORING WELL
(() AIR SPARGE WELL
~ VAPOR EXTRACTION WELL
~ ABANDONED/DESTROYED WELL
----------REMEDIATION TRENCH
--OHE --OVERHEAD ELECTRIC LINE
-ST--ST--UNDERGROUND STORM SEWER LINE
700
(1 ,820) PCE CONCENTRATION (ug/L)
ESTIMATED ISO CONCENTRATION CONTOI ----(DASHED WHERE INFERRED)
ug/L MICROGRAMS PER LITER
NOTES:
1. MONITORING WELLS MW1 AND MW17
WERE ABANDONED ON 5/24/2012 AS
PART OF ROAD CONSTRUCTION
ACTlVITIES.
2. THE NORTH CAROLINA GROSS
CONTAMINATE LEVEL {GCL) STANDARD
FOR TETRACHLORO ETHYLENE (PCE) IS
700 ug/L
0 40' 80'
GRAPHIC SCALE
~ARCADIS
~ARCADIS
Tables
Table 1: Groundwater Elevation Data
Revision Date: 5/14/2014 Incident Number: 3483 Facility ID #: Former ExxonMobil Facility #40962
1 of 6
6/22/96 498.05 NG NG NG NG NG NG11/20/97 498.05 23.95 NA NA 474.10 --4"12/23/02 498.05 27.02 NA NA 471.03 --4"
1/18/06 498.05 25.33 NA NA 472.72 --4"
11/7/06 498.05 25.9 NA NA 472.15 --4"11/19/07 498.05 26.09 NA NA 471.96 28.00 4"6/23/08 498.05 25.86 25.85 0.01 472.19 28.05 4"
3/3/09 498.05 25.88 NA NA 472.17 28.05 4"
11/4/09 498.05 25.89 NA NA 472.16 27.15 4"
5/19/10 498.05 25.84 NA NA 472.21 27.15 4"11/4/10 498.05 19.57 NA NA 478.48 --4"
3/7/11 498.05 26.00 NA NA 472.05 28.00 4"
10/17/11 498.05 26.81 NA NA 471.24 28.10 4"
3/14/12 498.05 27.18 NA NA 470.87 28.07 4"
12/10/98 497.43 23.09 NA NA 474.34 ----12/21/99 497.43 23.05 NA NA 474.38 ----
3/24/00 497.43 19.70 NA NA 477.73 ----
12/13/01 497.43 23.50 NA NA 473.93 ----
12/23/02 497.43 25.39 NA NA 472.04 ----12/23/03
1/22/98 498.34 26.18 25.35 0.83 472.77 --2"2/12/98 498.34 NA NA 0.67 ----2"
3/4/98 498.34 NA NA 0.33 ----2"
3/13/98 498.34 25.51 25.04 0.47 473.18 --2"3/26/98 498.34 25.50 24.80 0.70 473.36 --2"4/1/98 498.34 NA NA 0.67 ----2"
4/7/98 498.34 NA NA 0.75 ----2"
4/30/98 498.34 25.05 24.38 0.67 473.79 --2"
5/21/98 498.34 NA NA 0.42 ----2"5/30/98 498.34 NA NA 0.25 ----2"
6/4/98 498.34 NA NA 0.33 ----2"
6/10/98 498.34 NA NA 0.18 ----2"
7/2/98 498.34 NA NA 0.33 ----2"7/16/98 498.34 NA NA 0.50 ----2"
8/3/98 498.34 NA NA 0.50 ----2"
12/10/98 498.34 NA NA 0.33 ----2"
2/24/99 498.34 24.89 24.60 0.29 473.66 --2"3/26/99 498.34 25.60 25.20 0.40 473.04 --2"
4/14/99 498.34 25.81 25.60 0.21 472.69 --2"
5/26/99 498.34 25.68 25.65 0.03 472.68 --2"
6/16/99 498.34 25.78 25.73 0.05 472.60 --2"7/26/99 498.34 25.98 25.89 0.09 472.43 --2"8/26/99 498.34 25.97 NA 0.00 472.37 --2"
9/28/99 498.34 26.08 NA NA 472.26 --2"
10/27/99 498.34 26.19 26.18 0.01 472.16 --2"12/21/99 498.34 25.94 NA NA 472.40 --2"3/24/00 498.34 25.50 NA NA 472.84 --2"
6/15/00 498.34 25.07 NA NA 473.27 --2"
6/15/00 498.34 28.61 NA NA 469.73 --2"9/12/00 498.34 25.05 NA NA 473.29 --2"12/13/01 498.34 29.60 NA NA 468.74 --2"
2/28/02 498.34 28.29 26.62 1.67 470.05 --2"
Depth to
Product (ft btoc)
Top of Casing
Elevation (ft asl)
Well destroyed
19.0-29.0
Screened
Interval (ft btoc)
12.5-32.5
Free Product
Thickness (ft)
Well
Diameter
MW-6
Depth to
Bottom (ft btoc)
Depth to
Water (ft btoc)
Ground
Water
Elevation (ft asl)
10.0-30.0MW-1
Well ID Sampling
Date
Abandoned by the NCDOT on May 24, 2012
MW-9
Table 1: Groundwater Elevation Data
Revision Date: 5/14/2014 Incident Number: 3483 Facility ID #: Former ExxonMobil Facility #40962
2 of 6
Depth to
Product (ft btoc)
Top of Casing
Elevation (ft asl)
Screened
Interval (ft btoc)
Free Product
Thickness (ft)
Well
Diameter
Depth to
Bottom (ft btoc)
Depth to
Water (ft btoc)
Ground
Water
Elevation (ft asl)
Well ID Sampling
Date
3/22/02 498.34 29.30 27.00 2.30 469.04 --2"3/29/02 498.34 27.67 26.28 1.39 470.67 --2"12/23/02 498.34 29.41 27.09 2.32 468.93 --2"
12/23/03 498.34 NA NA 1.50 NA --2"
11/23/04 498.34 NA NA 2.00 NA --2"
1/18/06 498.34 NA NA 0.62 NA --2"11/7/06 498.34 27.50 26.50 1.00 NA --2"
11/19/07 498.34 27.71 26.58 1.13 470.63 30.80 2"
6/23/08 498.34 29.70 27.07 2.63 468.64 30.70 2"
3/3/09 498.34 27.01 26.09 0.92 472.01 30.70 2"11/4/09 498.34 27.10 NA NA 471.24 31.41 6"
5/19/10 498.34 26.88 26.84 0.04 471.46 31.41 6"
11/4/10 498.34 26.79 26.72 0.07 471.55 --6"
3/7/11 498.34 27.50 27.45 0.05 470.88 31.41 6"4/29/11 498.34 27.70 27.65 0.05 470.68 31.41 6"
5/17/11 498.34 27.70 27.68 0.02 470.65 31.41 6"
6/7/11 498.34 27.75 NA NA 470.59 31.41 6"
7/20/11 498.34 27.60 NA NA 470.74 31.41 6"8/23/11 498.34 28.10 27.85 0.25 470.43 31.41 6"9/13/11 498.34 27.88 27.85 0.03 470.48 31.41 6"
10/13/11 498.34 27.97 27.95 0.02 470.38 --6"
10/17/11 498.34 28.00 NA NA 470.34 32.50 6"10/25/11 498.34 28.01 NA NA 470.33 32.50 6"10/28/11 498.34 28.24 NA NA 470.10 32.50 6"
12/1/11 498.34 28.15 NA NA 470.19 --6"
12/21/11 498.34 28.12 NA NA 470.22 --6"1/17/12 498.34 28.21 NA NA 470.13 33.50 6"2/7/12 498.34 28.28 NA NA 470.06 --6"
3/14/12 498.34 28.62 28.39 0.23 469.89 31.50 6"
5/14/12 498.34 28.90 28.43 0.47 469.79 --6"
6/27/12 498.34 29.50 28.35 1.15 469.69 --6"7/26/12 498.34 29.31 28.34 0.97 469.75 --6"
8/7/12 498.34 28.78 28.68 0.10 469.63 --6"
8/30/12 498.34 28.25 NA NA 470.09 --6"
9/27/12 498.34 28.20 28.05 0.15 470.25 --6"10/18/12 498.34 27.98 NA NA 470.36 --6"
11/14/12 498.34 27.88 NA NA 470.46 --6"
1/10/13 498.34 28.12 NA NA 470.22 --6"
2/21/13 498.34 28.60 28.25 0.35 469.74 --6"3/13/13 498.34 28.55 28.52 0.03 469.79 --6"
4/11/13 498.34 28.30 28.25 0.05 470.04 --6"
5/30/13 498.34 29.10 NA NA 469.24 --6"
6/19/13 498.34 28.05 NA NA 470.29 --6"7/31/13 498.34 28.12 NA NA 470.22 --6"8/29/13 498.34 27.47 NA NA 470.87 --6"
9/23/13 498.34 27.40 27.28 0.12 471.03 --6"
9/25/13 498.34 27.25 NA NA 471.09 --6"10/23/13 498.34 27.50 NA NA 470.84 --6"11/13/13 498.34 27.22 NA NA 471.12 --6"
12/4/13 498.34 27.14 NA NA 471.20 --6"
1/8/14 498.34 27.51 NA NA 470.83 --6"2/5/14 498.34 27.48 NA NA 470.86 --6"3/12/14 498.34 27.34 NA NA 471.00 --6"
3/26/14 498.34 27.41 NA NA 470.93 --6"
4/9/14 498.34 27.29 NA NA 471.05 --6"
12.5-32.5
MW-9
Continued
Renamed
SVE-1
Nov 2009
Table 1: Groundwater Elevation Data
Revision Date: 5/14/2014 Incident Number: 3483 Facility ID #: Former ExxonMobil Facility #40962
3 of 6
Depth to
Product (ft btoc)
Top of Casing
Elevation (ft asl)
Screened
Interval (ft btoc)
Free Product
Thickness (ft)
Well
Diameter
Depth to
Bottom (ft btoc)
Depth to
Water (ft btoc)
Ground
Water
Elevation (ft asl)
Well ID Sampling
Date
12/10/98 498.96 27.13 NA NA 471.83 59.90 2"9/28/99 498.96 28.86 NA NA 470.10 59.90 2"12/21/99 498.96 18.30 NA NA 480.66 59.90 2"
3/24/00 498.96 23.25 NA NA 475.71 59.90 2"
12/13/01 498.96 22.68 NA NA 476.28 59.90 2"
12/23/02 498.96 29.08 NA NA 469.88 59.90 2"6/12/03 498.96 31.02 NA NA 467.94 59.90 2"
12/23/03 498.96 28.88 NA NA 470.08 59.90 2"
6/8/04 498.96 31.02 NA NA 467.94 59.90 2"
11/23/04 498.96 27.20 NA NA 471.76 59.90 2"1/18/06 498.96 28.65 NA NA 470.31 59.90 2"
11/7/06 498.96 24.00 NA NA 474.96 59.90 2"
11/19/07 498.96 24.40 NA NA 474.56 59.90 2"
6/23/08 498.96 11.88 NA NA 487.08 59.90 2"3/3/09 498.96 24.12 NA NA 474.84 59.90 2"
11/4/09 498.96 23.91 NA NA 475.05 59.85 2"
5/19/10 498.96 24.12 NA NA 474.84 59.85 2"
11/4/10 498.96 24.06 NA NA 474.90 59.92 2"3/7/11 498.96 25.30 NA NA 473.66 59.92 2"10/17/11 498.96 21.12 NA NA 477.84 60.00 2"
3/14/12 498.96 26.12 NA NA 472.84 59.90 2"
10/18/12 498.96 23.37 NA NA 475.59 60.00 2"
2/21/13 498.96 24.85 NA NA 474.11 60.00 2"
9/23/13 498.96 22.71 NA NA 476.25 60.00 2"3/26/14 498.96 22.48 NA NA 476.48 60.00 2"
12/10/98 497.50 24.73 NA NA 472.77 29.17 2"12/21/99 497.50 25.55 NA NA 471.95 29.17 2"
3/24/00 497.50 25.10 NA NA 472.40 29.17 2"
6/15/00 497.50 28.61 NA NA 468.89 29.17 2"
9/12/00 497.50 25.50 NA NA 472.00 29.17 2"12/13/01 497.50 26.73 26.70 0.03 470.77 29.17 2"
2/28/02 497.50 27.10 NA NA 470.40 29.17 2"
3/22/02 497.50 26.51 26.16 0.35 470.99 29.17 2"
3/29/02 497.50 27.31 470.19 29.17 2"12/23/02 497.50 28.64 468.86 29.17 2"
12/23/03 497.50 25.00 23.00 2.00 472.50 29.17 2"
11/23/04 497.50 25.97 NA NA 471.53 29.17 2"
1/18/06 497.50 27.30 NA NA 470.20 29.17 2"11/7/06 497.50 27.60 NA NA 469.90 29.17 2"6/23/08 497.50 28.53 NA NA 468.97 29.17 2'
3/3/09 497.50 NA NA NA NA 29.17 2"
11/4/09 497.50 27.63 NA NA NA 29.12 2"5/19/10 497.50 27.36 NA NA 470.14 29.12 2"11/4/10 497.50 27.17 NA NA 470.33 29.77 2"
3/7/11 497.50 27.95 NA NA 469.55 29.77 2"
10/17/11 497.50 28.20 NA NA 469.30 29.20 2"10/25/11 497.50 28.49 NA NA 469.01 29.00 2"10/28/11 497.50 28.59 NA NA 468.91 29.00 2"
3/14/12 497.50 28.88 NA NA 468.62 30.10 2"
10/18/12 497.50 28.36 NA NA 469.14 29.00 2"
2/21/13 497.50 28.76 NA NA 468.74 29.00 2"9/23/13 497.50 27.72 NA NA 469.78 29.00 2"3/26/14 497.50 27.51 NA NA 469.99 29.00 2"
Sheen <0.01 ft
MW-11D 55.0-60.0
MW-14
Sheen <0.01 ft
9.0-29.0
Table 1: Groundwater Elevation Data
Revision Date: 5/14/2014 Incident Number: 3483 Facility ID #: Former ExxonMobil Facility #40962
4 of 6
Depth to
Product (ft btoc)
Top of Casing
Elevation (ft asl)
Screened
Interval (ft btoc)
Free Product
Thickness (ft)
Well
Diameter
Depth to
Bottom (ft btoc)
Depth to
Water (ft btoc)
Ground
Water
Elevation (ft asl)
Well ID Sampling
Date
12/10/98 497.50 22.94 NA NA 474.56 29.75 2'12/21/99 497.50 23.67 NA NA 473.83 29.75 2'3/24/00 497.50 23.26 NA NA 474.24 29.75 2'
12/13/01 497.50 25.07 NA NA 472.43 29.75 2'
12/23/02 497.50 26.28 NA NA 471.22 29.75 2'
12/23/03 497.50 23.16 NA NA 474.34 29.75 2'11/23/04 497.50 23.51 NA NA 473.99 29.75 2'
1/18/06 497.50 24.60 NA NA 472.90 29.75 2'
11/7/06 497.50 25.00 NA NA 472.50 29.75 2'
11/19/07 497.50 25.31 NA NA 472.19 29.75 2'6/23/08 497.50 26.10 NA NA 471.40 29.80 2"
3/3/09 497.50 24.87 NA NA 472.63 29.80 2"
11/4/09 497.50 25.13 NA NA 472.37 29.76 2"
5/19/10 497.50 24.79 NA NA 472.71 29.76 2"11/4/10 497.50 24.77 NA NA 472.73 29.85 2"
3/7/11 497.50 25.45 NA NA 472.05 29.85 2"
10/17/11 497.50 26.00 NA NA 471.50 30.00 2"
3/14/12 497.50 26.40 NA NA 471.10 30.00 2"10/18/12 497.50 26.09 NA NA 471.41 30.00 2"2/21/13 497.50 26.32 NA NA 471.18 30.00 2"
9/23/13 497.50 25.38 NA NA 472.12 30.00 2"3/26/14 497.50 25.35 NA NA 472.15 30.00 2"
12/10/98 497.29 23.07 NA NA 474.22 ----
12/21/99 497.29 22.80 NA NA 474.49 ----
3/24/00 497.29 23.46 NA NA 473.83 ----
12/13/01 497.29 25.22 NA NA 472.07 ----12/23/02 497.29 26.38 NA NA 470.91 ----
1/18/06 497.29 NL
3/3/09 497.09 2"
11/4/09 497.09 2"10/18/12 497.09 2"
2/13/13 497.09 2"
9/23/13 497.09 2"
3/26/14 497.09 2"
12/10/98 497.95 22.85 NA NA 475.10 32.70 2"
12/21/99 497.95 22.90 NA NA 475.05 32.70 2"3/24/00 497.95 22.95 NA NA 475.00 32.70 2"
6/12/03 497.95 24.78 NA NA 473.17 32.70 2"
12/23/03 497.95 23.06 NA NA 474.89 32.70 2"
6/8/04 497.95 24.78 NA NA 473.17 32.70 2"11/23/04 497.95 23.47 NA NA 474.48 32.70 2"
1/18/06 497.95 23.80 NA NA 474.15 32.70 2"
11/7/06 497.95 24.15 NA NA 473.80 32.70 2"
11/19/07 497.95 24.33 NA NA 473.62 32.70 2"6/23/08 497.95 24.68 NA NA 473.27 32.15 2"
3/3/09 497.95 24.09 NA NA 473.86 32.15 2"
11/4/09 497.95 2"
5/19/10 497.95 24.38 NA NA 473.57 32.15 2"11/4/10 497.95 23.84 NA NA 474.11 --2"3/7/11 497.95 24.45 NA NA 473.50 --2"
10/17/11 497.95 24.91 NA NA 473.04 32.20 2"
3/14/12 497.95 25.24 NA NA 472.71 32.20 2"
Could Not Locate
Could Not Locate
Inaccessible
Could Not Locate
MW-17
Could Not Locate
Could Not Locate
10.5-30.5
Could Not Locate
14.0-34.0
14.0-34.0
Abandoned by the NCDOT on May 24, 2012
MW-15 10.0-30.0
MW-16
Could Not Locate
Table 1: Groundwater Elevation Data
Revision Date: 5/14/2014 Incident Number: 3483 Facility ID #: Former ExxonMobil Facility #40962
5 of 6
Depth to
Product (ft btoc)
Top of Casing
Elevation (ft asl)
Screened
Interval (ft btoc)
Free Product
Thickness (ft)
Well
Diameter
Depth to
Bottom (ft btoc)
Depth to
Water (ft btoc)
Ground
Water
Elevation (ft asl)
Well ID Sampling
Date
12/10/98 499.59 27.00 NA NA 472.59 --2"12/21/99 499.59 27.40 NA NA 472.19 --2"3/24/00 499.59 27.04 NA NA 472.55 --2"
12/13/01 499.59 29.07 NA NA 470.52 --2"
12/23/02 499.59 30.07 NA NA 469.52 --2"
12/23/03 499.59 26.89 NA NA 472.70 --2"1/18/06 499.59 --
6/23/08 499.59 --
3/3/09 499.59 --
11/4/09 499.59 --10/18/12 499.59 --
2/21/13 499.59 --
9/23/13 499.59 --
3/26/14 499.59 --
11/4/09 NS 27.44 27.42 0.02 NA 30.88 6"
5/19/10 NS 29.98 29.03 0.95 NA 30.88 6"11/4/10 NS 27.03 26.98 0.05 NA --6"
3/7/11 NS 28.45 27.70 0.75 NA 30.20 6"
4/29/11 NS 29.44 27.72 1.72 NA 30.20 6"
5/17/11 NS 29.70 27.80 1.90 NA 30.20 6"6/7/11 NS 29.70 27.80 1.90 NA 30.20 6"
7/20/11 NS 29.90 27.85 2.05 NA 30.20 6"
8/23/11 NS 30.00 27.85 2.15 NA 30.20 6"
9/13/11 NS 29.00 28.10 0.90 NA 30.20 6"10/13/11 NS 29.07 28.17 0.90 NA --6"
10/17/11 NS 29.30 29.01 0.29 NA 30.20 6"
10/25/11 NS 28.68 28.67 0.01 NA 30.20 6"
10/28/11 NS 28.35 28.34 0.01 NA 30.20 6"12/1/11 NS 30.37 28.97 1.40 NA --6"12/21/11 NS 30.23 28.83 1.40 NA --6"
1/17/12 NS 28.94 28.32 0.62 NA 32.00 6"
2/7/12 NS 30.69 28.62 2.07 NA --6"3/14/12 NS 31.42 28.30 3.12 NA 31.50 6"5/14/12 NS 30.85 28.98 1.87 NA --6"
6/27/12 NS 30.00 29.00 1.00 NA 32.00 6"
7/26/12 NS 29.94 29.15 0.79 NA 32.00 6"8/7/12 NS 29.52 29.50 0.02 NA 32.00 6"8/30/12 NS 28.50 28.30 0.20 NA 32.00 6"
9/27/12 NS 28.65 28.42 0.23 NA 32.00 6"
10/18/12 NS 28.67 NA NA NA 32.00 6"
11/15/12 NS 28.22 NA NA NA 32.00 6"1/10/13 NS 28.48 NA NA NA 32.00 6"
2/21/13 NS 28.68 NA*NA NA 32.00 6"
3/13/13 NS 28.35 28.42 0.07 NA 32.00 6"
4/11/13 NS 28.80 28.78 0.02 NA 32.00 6"5/30/13 NS 28.50 28.49 0.01 NA 32.00 6"
6/19/13 NS 28.46 28.45 0.01 NA 32.00 6"
7/31/13 NS 28.39 NA NA NA 32.00 6"
8/29/13 NS 27.80 NA NA NA 32.00 6"9/23/13 NS 27.66 NA NA NA 32.00 6"
9/25/13 NS 27.52 NA NA NA 32.00 6"
10/23/13 NS 28.01 NA NA NA 32.00 6"
11/13/13 NS 27.54 NA NA NA 32.00 6"12/4/13 NS 27.50 NA NA NA 32.00 6"1/8/14 NS 27.79 NA NA NA 32.00 6"
2/5/14 NS 27.82 NA NA NA 32.00 6"
3/12/14 NS 27.84 NA NA NA 32.00 6"3/26/14 NS 27.81 NA NA NA 32.00 6"4/9/14 NS 27.61 NA NA NA 32.00 6"
SVE-2 12.0-32.0
Could Not Locate
Could Not Locate
Could Not Locate
Could Not Locate
Could Not Locate
15.0-35.0
MW-20
Could Not Locate
Could Not Locate
Could Not Locate
Table 1: Groundwater Elevation Data
Revision Date: 5/14/2014 Incident Number: 3483 Facility ID #: Former ExxonMobil Facility #40962
6 of 6
Depth to
Product (ft btoc)
Top of Casing
Elevation (ft asl)
Screened
Interval (ft btoc)
Free Product
Thickness (ft)
Well
Diameter
Depth to
Bottom (ft btoc)
Depth to
Water (ft btoc)
Ground
Water
Elevation (ft asl)
Well ID Sampling
Date
11/4/09 NS 27.30 NA NA NA 32.25 6"5/19/10 NS 26.98 NA NA NA 32.25 6"3/7/11 NS 27.65 27.60 0.05 NA 32.50 6"
4/29/11 NS 27.87 27.80 0.07 NA 32.50 6"
5/17/11 NS 28.72 28.70 0.02 NA 32.50 6"
6/7/11 NS 27.90 NA NA NA 32.50 6"7/20/11 NS 28.02 NA NA NA 32.50 6"
8/23/11 NS 28.10 NA NA NA 32.50 6"
9/13/11 NS 28.00 NA NA NA 32.50 6"
10/13/11 NS 28.07 28.06 0.01 NA --6"10/17/11 NS 28.20 NA NA NA 32.70 6"
10/25/11 NS 28.21 NA NA NA 32.50 6"
10/28/11 NS 28.59 NA NA NA 32.50 6"
12/1/11 NS 28.30 NA NA NA --6"12/21/11 NS 28.38 NA NA NA --6"
1/17/12 NS 28.35 NA NA NA 33.00 6"
2/7/12 NS 28.41 NA NA NA --6"
3/14/12 NS 28.55 NA NA NA 32.00 6"5/14/12 NS 28.62 NA NA NA --6"6/27/12 NS 28.75 NA NA NA 32.00 6"
7/26/12 NS 28.93 NA NA NA 32.00 6"
8/30/12 NS 29.50 NA NA NA 32.00 6"9/27/12 NS 28.15 NA NA NA 32.00 6"10/18/12 NS 28.01 NA NA NA 32.00 6"
11/15/12 NS 28.92 NA NA NA 32.00 6"
1/10/13 NS 28.00 NA NA NA 32.00 6"2/21/13 NS 28.68 NA NA NA 32.00 6"
9/23/13 NS 27.39 NA NA NA 32.00 6"3/26/14 NS 27.39 NA NA NA 32.00 6"
Notes:
ft asl = feet relative to arbitrary site level of 500 feet
ft btoc = below top of well casing
NG = Not gaugedNA = Not applicable
NS = Not surveyed
* = Free product not detected upon initial gauging.However, free product detected post purge
SVE-3 12.0-32.0
Table 2: Groundwater Analytical Data
Revision Date: 5/14/2014 Incident Number: 3483 Facility ID#: Former ExxonMobil Facility #40962
1 of 3
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GCLs 5,000 260,000 84,500 85,500 6,000 20,000 70,000 6,900 8,500 30,000 25,000 NE 700 70,000 NE 590,000 70,000 100,000 30 28,500 25,000 3,000 70,000 7,000 50 15,000 NE NE NE
11/22/1997 128 3,910 609 5,380 --25.3 ND ------------------------------------------1/18/2006 102 68.1 488 2,620 NA 122 150 ----------1.28 ND --ND ND ND ND ND --ND ------64.4 8,690 4,850 6,75011/7/2006 3.43 163 257 2,040 124 ND ND ----------7.64 3.31 --ND ND ND ND ND --1.27 ------218 4,610 7,000 2,280
11/20/2007 4.1 178 394 2,976 227 ND ND ----------1.8 15.3 --ND ND ND ND ND --ND ------536 5,870 11,600 5,090
6/23/2008 --------------------------------------------------
3/3/2009 ND 49.2 84.3 957 85.2 5.34 ND 11.8 0.91 10.4 4.57 1.83 29.1 2.3 1.18 ND ND ND ND 291 0.82 113 ------28.3 1,730 520 1,220
11/4/2009 <0.500 1.37 3.08 29.4 <5.00 <0.500 <0.500 1.45 <0.500 1.18 <0.500 <0.500 0.880 <0.500 <0.500 NA <0.500 <0.500 <0.500 14.5 5.04 <0.500 <0.500 <0.500 <0.500 60.4 NA NA NA
5/19/2010 ND<0.500 1.79 3.39 38.4 ND<5.00 ND<0.500 ND<0.500 1.27 ND<0.500 0.66 ND<0.500 ND<0.500 4.34 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 10.1 ND<0.500 5.32 ND<0.500 ND<0.500 ND<0.500 67.8 NA NA NA11/4/2010 ND<0.500 ND<0.500 ND<0.500 ND<1.00 ND<5.00 ND<0.500 ND<0.500 2.03 ND<0.500 ND<0.500 ND<0.500 ND<0.500 1.59 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 0.77 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 --------
3/7/2011 ND<0.500 8.56 21.3 149 10.8 ND<0.500 ND<0.500 11.9 1.32 7.20 1.99 1.33 1.23 4.82 ND<0.500 --ND<0.500 ND<0.500 ND<0.500 51.2 26 ND<0.500 ND<0.500 ND<0.500 ND<0.500 --------
12/10/1998 55 478 218 900 --ND ND --------------------------------------------
12/21/1999 98 1,010 530 1,950 --ND ND --------------------------------------------3/24/2000 73 1,050 637 3,250 --795 164 --------------------------------------------12/13/2001 30.5 489 560 3,000 --78.5 112 --------------------------------------------12/23/2002 36.6 435 1,400 7,300 --71.6 145 --------------------------------------------
12/10/1998 478 10,800 2,790 6,600 --ND 254 ------------------------------------------12/21/1999 38 32,200 1,720 3,890 --ND 858 --------------------------------------------3/24/2000 34 27,600 1,690 7,670 --880 758 --------------------------------------------6/15/2000 ND 19,200 2,140 8,500 --96 176 --------------------------------------------
9/12/2000 40 38,800 2,370 19,200 --232 310 --------------------------------------------
12/13/2001 --------------------------------------------------
12/23/2003 --------------------------------------------------
11/23/2004 --------------------------------------------------
1/18/2006 --------------------------------------------------11/7/2006 --------------------------------------------------11/20/2007 --------------------------------------------------6/23/2008 --------------------------------------------------
3/3/2009 --------------------------------------------------
11/4/2009 3,430 57,000 5,030 28,600 738 68.8 58.1 74.7 14.9 570 163 10.1 80.9 57.7 <0.500 NA <0.500 <0.500 <0.500 4,300 1,140 30.9 644 <0.500 13.8 --------
10/17/2011 18.2 2,190 1,640 17,700 1,250 111 ND<10.0 148 30.8 430 177 22.6 2,930 193 ND<10.0 --ND<10.0 ND<10.0 ND<10.0 6,440 1,610 145 ND<10.0 ND<10.0 ND<10.0 --------
3/14/2012 --------------------------------------------------
3/26/2014 29.4 673 1,080 16,900 1,140 76.2 4.24 109 31.5 314 113 16.7 1,820 125 ND<0.500 --ND<0.500 1.37 ND<0.500 5,830 1,450 331 ND<0.500 ND<0.500 ND<0.500 --------
12/10/1998 ND ND ND ND --ND ND --------------------------------------------
12/21/1999 5.8 60.6 8.4 40.5 --2 2 --------------------------------------------
3/24/2000 1.7 16.2 1.6 8.7 --ND ND --------------------------------------------
12/13/2001 ND 1.9 2.7 2.8 --ND ND --------------------------------------------
12/23/2002 ND ND ND 1.6 --ND ND --------------------------------------------6/12/2003 ND ND ND ND --ND ND --------------------------------------------12/23/2003 ND ND ND ND --ND ND --------------------------------------------6/8/2004 ND ND ND ND --ND ND --------------------------------------------
11/23/2004 ND 2.4 1 3.9 --ND ND --------------------------------------------
6/23/2005 ND ND 1.3 ND --ND ND --------------------------------------------
1/18/2006 ND ND ND ND NA ND ND ----------ND ND --ND ND ND ND ND --ND ------ND ND 141 ND
11/7/2006 ND ND ND ND ND ND ND ----------ND ND --ND ND ND ND ND --ND ------ND ND ND ND
11/20/2007 ND 3.11 1.54 11.2 10.9 ND ND ----------ND ND --ND ND ND ND ND --ND ------ND ND 300 1616/24/2008 ND 0.56 ND 1.74 ND ND ND ----------ND ND --2.05 ND ND ND 1.07 --ND ------ND ND 110 ND3/3/2009 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.63 ND ND ND ------ND ND ND ND11/4/2009 <0.500 <0.500 <0.500 1.64 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NA <0.500 <0.500 <0.500 1.36 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 ------
5/19/2010 ND<0.500 1.9 5 67.7 39.5 ND<0.500 ND<0.500 13.4 1.89 8.55 2.2 1.29 0.5 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 141 ND<0.500 36.5 ND<0.500 ND<0.500 ND<0.500 ND<0.005 ------
11/4/2010 ND<0.500 0.52 ND<0.500 1.81 ND<5.00 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 1.83 0.51 ND<0.500 ND<0.500 ND<0.500 ND<0.500 --------
3/7/2011 ND<0.500 1.25 0.56 4.19 ND<5.00 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 --ND<0.500 ND<0.500 ND<0.500 4.50 1.57 ND<0.500 ND<0.500 ND<0.500 ND<0.500 --------
**NAPL in Well**
MW-9/SVE-1*
**NAPL in Well**
**NAPL in Well**
**NAPL in Well**
MADEP VPH (µg/l)Volatile Organic Compounds by SM 6200B (Historical used 6210D) µg/l
**NAPL in Well**
**NAPL in Well**
MW-1 **NAPL in Well**
**NAPL in Well**
**NAPL in Well**
MW-6
MW-11D
**NAPL in Well**
Table 2: Groundwater Analytical Data
Revision Date: 5/14/2014 Incident Number: 3483 Facility ID#: Former ExxonMobil Facility #40962
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MADEP VPH (µg/l)Volatile Organic Compounds by SM 6200B (Historical used 6210D) µg/l
5/24/90 60 30 8.4 3.9 NA NA ----------------------------------------------10/16/90 7.8 32 1.5 14 NA NA ----------------------------------------------
1/8/91 ND 14 ND 17 NA NA ----------------------------------------------
5/29/91 34 51 3.5 38 NA NA ----------------------------------------------
3/9/93 78 70 6.6 61 20 21 ----------------------------------------------
9/8/93 43 9.4 2 25 14 27 ----------------------------------------------
2/22/94 35.8 4.5 1.6 17.1 51.7 22 ----------------------------------------------
8/12/94 24 3 ND 14 ND 13 ----------------------------------------------2/23/95 15 3 1 37 50 20 ----------------------------------------------9/29/95 3 ND ND 2 ND 13 ----------------------------------------------2/8/96 3 ND ND 2 ND 13 ----------------------------------------------
6/22/96 ND ND ND ND ND 14 ----------------------------------------------5/24/90 40 53 9 56 NA NA ----------------------------------------------7/17/90 55 190 3.4 100 NA NA ----------------------------------------------10/16/90 28 110 2 51 NA NA ----------------------------------------------
1/8/91 7.4 34 1.5 26 NA NA ----------------------------------------------
5/29/91 15 45 ND 32 NA NA ----------------------------------------------
2/22/93 152 488 30 306 188 161 ----------------------------------------------
8/12/94 84 236 11 186 45 134 ----------------------------------------------
2/23/95 31 12 2 123 85 82 ----------------------------------------------9/29/95 2 ND ND ND ND 54 ----------------------------------------------2/8/96 2 1 1 2 ND 64 ----------------------------------------------6/22/96 ND ND ND ND ND 97 ----------------------------------------------
12/10/1998 9,180 15,000 1,580 8,500 --219 7,420 --------------------------------------------12/21/1999 10,000 33,200 9,800 3,750 --ND 2,850 --------------------------------------------3/24/2000 10,400 32,500 2,230 13,200 --595 3,800 --------------------------------------------6/15/2000 9,810 32,700 1,740 11,200 --ND 3,030 --------------------------------------------
9/12/2000 3,200 8,660 845 5,970 --90 1,100 --------------------------------------------
12/13/2001 --------------------------------------------------
12/23/2002 --------------------------------------------------
12/23/2003 --------------------------------------------------
11/23/2004 --------------------------------------------------1/18/2006 2,000 15,900 1,270 7,560 NA 951 144 ----------45.3 31 --ND ND ND ND ND --604 ------41.4 58,700 16,800 7,17011/7/2006 2,100 26,700 2,700 12,300 451 109 39.7 ----------41 25.1 --ND 1.15 1.56 0.59 ND --538 ------20.5 64,100 21,300 3,7006/23/2008 --------------------------------------------------
11/4/2009 1,510 14,900 1,920 12,100 640 910 3.4 59.6 9.91 180 69.4 7.25 26.4 40 <0.500 NA <0.500 2.55 <0.500 1,960 512 748 302 1.26 <0.500 11.1 ------
5/19/2010 5.67 99.7 18.5 149 12.2 0.88 ND<0.500 1.71 ND<0.500 2.16 0.76 ND<0.500 1.47 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 28 7.23 9.07 ND<0.500 ND<0.500 ND<0.500 11.7 ------
11/4/2010 128 835 138 1,030 67.1 524 0.63 6.96 0.78 14.3 4.72 0.83 8.9 5.27 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 200 59 31.7 ND<0.500 ND<0.500 ND<0.500 --------
3/7/2011 16.6 786 154 1,360 76.9 3.43 ND<0.500 40.3 5.94 43.2 14.6 5.11 6.25 ND<0.500 ND<0.500 --ND<0.500 ND<0.500 ND<0.500 771 118 18.3 ND<0.500 ND<0.500 ND<0.500 --------
10/17/2011 156 359 48.0 256 29.0 210 0.680 4.66 0.570 5.44 1.48 0.760 5.41 8.24 ND<0.500 NA ND<5.00 0.530 ND<5.00 54.7 17.0 41.3 ND<0.500 ND<0.500 ND<0.500 --------
MW-12
**NAPL in Well**
MW-14 **NAPL in Well**
MW-13
**NAPL in Well**
Could not sample due to limited water in well
**NAPL Sheen in Well**
Table 2: Groundwater Analytical Data
Revision Date: 5/14/2014 Incident Number: 3483 Facility ID#: Former ExxonMobil Facility #40962
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MADEP VPH (µg/l)Volatile Organic Compounds by SM 6200B (Historical used 6210D) µg/l
12/10/1998 75 746 201 462 --ND ND --------------------------------------------12/21/1999 114 136 109 401 --15 ND --------------------------------------------
3/24/2000 114 691 369 1,400 --368 76 --------------------------------------------
12/13/2001 7.9 2.2 1.5 31.7 --7.7 5.9 --------------------------------------------
12/23/2002 5.7 ND ND ND --2.6 1.3 --------------------------------------------
12/23/2003 32.1 690 490 1,020 --85.5 48.1 --------------------------------------------
11/23/2004 7.5 3.4 48.6 59.7 --24.9 ND --------------------------------------------
1/18/2006 3.95 1.77 ND ND NA 11.1 5.41 ----------31.7 15.6 --ND ND ND ND ND --5.45 ------ND 1,370 109 17711/7/2006 ND ND ND ND ND ND ND ----------1.7 ND --ND ND ND ND ND --ND ------ND ND ND ND11/19/2007 0.75 ND ND ND ND ND ND ----------3.13 1.15 --ND ND ND ND ND --0.87 ------ND ND ND ND6/23/2008 --------------------------------------------------
3/3/2009 ND ND ND ND ND ND ND ND ND ND ND ND 3.67 ND ND ND ND ND ND ND 0.9 ND ------ND ND ND ND
11/4/2009 1.84 <0.500 1.49 4.64 34.3 <0.500 <0.500 0.68 0.75 0.53 8.5 <0.500 2.4 2.35 <0.500 NA <0.500 <0.500 <0.500 0.59 2.23 2.87 <0.500 <0.500 <0.500 <5.00 ------
5/19/2010 ND<0.500 ND<0.500 ND<0.500 ND<1.00 ND<5.00 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 2.49 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 1.99 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.005 ------
11/4/2010 ND<0.500 0.54 ND<0.500 1.65 ND<5.00 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 2.80 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 0.63 ND<0.500 1.08 ND<0.500 ND<0.500 ND<0.500 --------
3/7/2011 2.91 1.99 7.88 66 15.7 ND<0.500 ND<0.500 ND<0.500 0.53 ND<0.500 4.66 ND<0.500 1.91 1.83 ND<0.500 --ND<0.500 ND<0.500 ND<0.500 11.1 1.08 2.96 ND<0.500 ND<0.500 ND<0.500 --------
10/17/2011 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<5.00 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<1.00 ND<0.500 2.19 0.800 ND<0.500 --ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 1.39 ND<0.500 ND<0.500 ND<0.500 --------
12/10/1998 ND 2.8 ND ND --ND 2 --------------------------------------------
12/21/1999 ND 1 ND ND --ND 5 --------------------------------------------
3/24/2000 ND 2.9 ND ND --ND 8 --------------------------------------------12/13/2001 ND 1.1 ND ND --ND ND --------------------------------------------
12/23/2002 ND ND ND ND --ND ND --------------------------------------------
12/10/1998 ND 2.4 ND ND --ND 128 --------------------------------------------
12/21/1999 ND 4 ND 3.3 --ND 106 --------------------------------------------3/24/2000 ND 1.6 ND 1.8 --29.7 99 --------------------------------------------6/12/2003 ND ND ND ND --ND 10.8 --------------------------------------------12/23/2003 ND ND ND ND --1.7 ND --------------------------------------------
6/8/2004 ND ND ND ND --2.4 78.3 --------------------------------------------
11/23/2004 ND ND ND ND --ND 1 --------------------------------------------
6/23/2005 ND ND ND ND --ND ND --------------------------------------------
1/18/2006 ND 2.02 1.94 ND NA ND ND ----------126 56 --ND ND ND ND ND --3.06 ------ND 117 ND ND
11/7/2006 ND ND ND ND ND ND ND ----------107 48.6 --ND ND 0.89 1.25 ND --2.46 ------ND ND ND ND11/20/2007 ND ND ND ND ND ND ND ----------94.3 47 --ND ND 0.88 1.38 ND --2.93 ------19.2 ND ND ND6/24/2008 ND ND ND ND ND ND ND ----------153 49.9 --ND ND 0.87 1.1 ND --3.67 ------7.6 ND ND ND3/3/2009 ND ND ND ND ND ND ND ND ND ND ND ND ND 42.5 ND ND ND 0.67 0.87 ND 3.02 ND ------ND ND ND ND
5/19/2010 ND<0.500 0.58 ND<0.500 5.86 7.98 ND<0.500 ND<0.500 1.53 ND<0.500 0.77 ND<0.500 ND<0.500 129 38.1 ND<0.500 ND<0.500 ND<0.500 0.67 0.84 16 3.21 3.82 ND<0.500 ND<0.500 ND<0.500 ND<0.005 ------
11/4/2010 ND<0.500 ND<0.500 ND<0.500 ND<1.00 ND<5.00 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 154 45.3 ND<0.500 ND<0.500 ND<0.500 0.98 0.97 ND<0.500 ND<0.500 2.97 ND<0.500 ND<0.500 ND<0.500 --------
3/7/2011 ND<0.500 ND<0.500 ND<0.500 ND<1.00 ND<5.00 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 101 35.8 ND<0.500 --ND<0.500 0.75 0.64 ND<0.500 ND<0.500 2.97 ND<0.500 ND<0.500 ND<0.500 --------
10/17/2011 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<5.00 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 ND<0.500 145 38.8 ND<0.500 --ND<0.500 0.840 0.590 ND<0.500 ND<0.500 3.5 ND<0.500 ND<0.500 ND<0.500 --------
12/10/1998 1.7 2.9 1.7 2.9 --11.3 45 --------------------------------------------
12/21/1999 22.4 68.4 61.6 27.8 --ND 49 --------------------------------------------
3/24/2000 3.7 4.6 8.8 3.8 --104 23 --------------------------------------------
12/13/2001 65.3 511 1,010 259 --49.1 ND --------------------------------------------
12/23/2002 222 156 594 516 --133 35.5 --------------------------------------------
12/23/2003 5.5 2.7 15.1 5.4 --16.8 ND --------------------------------------------
9/23/2013 241 27,300 3,590 29,700 1,300 950 ND<5.00 177 47.6 633 210 19.8 390 45.0 ND<5.00 --ND<5.00 --ND<5.00 5,290 1,610 683 635 ND<5.00 ND<5.00 --------
3/26/2014 229 24,100 3,580 31,400 1,290 354 ND<10.0 179 46.3 632 203 21.3 279 15.9 ND<10.0 --ND<10.0 ND<10.0 ND<10.0 5,800 1,550 133 523 ND<10.0 ND<10.0 --------
11/4/2009 112 3,840 1,860 16,600 1,090 1,020 12 109 18.8 389 120 15.1 2,340 45.8 <0.500 NA <0.500 0.52 <0.500 5,570 1,400 163 191 <0.500 2.58 58 ------
5/19/2010 2,450 48,900 3,130 22,300 585 167 27.8 32.2 7.2 175 88 5.29 256 52.6 ND<0.500 ND<0.500 ND<0.500 0.68 ND<0.500 2,200 142 564 138 ND<0.500 11.2 91.1 ------
10/17/2011 229 14,300 1,730 11,700 683 ND<25.0 ND<25.0 55.5 ND<25.0 202 81.0 ND<25.0 296 48.0 ND<25.0 --ND<25.0 ND<25.0 ND<25.0 2,310 651 724 269 ND<25.0 ND<25.0 --------
3/14/2012 194 14,000 1,540 9,600 380 28.8 ND<5.00 30 6.5 148 56.2 ND<5.00 637 92.9 ND<5.00 --ND<5.00 ND<5.00 ND<5.00 1,470 370 1,170 217 ND<5.00 ND<5.00 --------
Notes:
NE = Not Established
ND<# = Non-Detect, Below Lab Detection Limit
-- = Data not availableBold = detected above applicable NC2L standards*well was formerly designated MW-9, redesignated when overdrilled to improve remedial event effectiveness
SVE-2
SVE-3
MW-15
MW-17
MW-20
MW-16
Could not sample due to limited water in well
Appendix A
Groundwater Laboratory
Analytical Report and Chain-of-
Custody Record
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: (615)726-0177
TestAmerica Job ID: 490-49621-1
TestAmerica SDG: 5001 Raeford Road, Fayetteville, NC
Client Project/Site: EM 40962
For:
ARCADIS U.S. Inc
111-D Sanders Lane
Bluefield, Virginia 24605
Attn: Jon Farley
Authorized for release by:
4/11/2014 5:10:41 PM
Jennifer Huckaba, Project Manager II
(615)301-5042
jennifer.huckaba@testamericainc.com
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
1
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Table of Contents
Client: ARCADIS U.S. Inc
Project/Site: EM 40962
TestAmerica Job ID: 490-49621-1
SDG: 5001 Raeford Road, Fayetteville, NC
Page 2 of 30 TestAmerica Nashville4/11/2014
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .25
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .26
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .27
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .28
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .30
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Sample Summary
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-49621-1 SVE-1/MW-9 Ground Water 03/26/14 09:00 03/28/14 08:15
490-49621-2 SVE-2 Ground Water 03/26/14 09:30 03/28/14 08:15
490-49621-3 Trip Blank Water 03/26/14 00:01 03/28/14 08:15
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Case Narrative
Client: ARCADIS U.S. Inc TestAmerica Job ID: 490-49621-1
Project/Site: EM 40962 SDG: 5001 Raeford Road, Fayetteville, NC
Job ID: 490-49621-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-49621-1
Comments
No additional comments.
Receipt
The samples were received on 3/29/2014 8:15 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 2.1º C.
Except:
The following sample was received and observed with headspace in 1 of the 2 sample vials: Trip Blank (490-49621-3). The vial was
designated not to be used, therefore, no affect on the data.
GC/MS VOA
Method(s) SM6200-B: The following sample(s) was diluted due to the nature of the sample matrix: SVE-2 (490-49621-2). Elevated
reporting limits (RLs) are provided.
No other analytical or quality issues were noted.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Qualifiers
GC/MS VOA
Qualifier Description
F2 MS/MSD RPD exceeds control limits
Qualifier
F1 MS and/or MSD Recovery exceeds the control limits
E Result exceeded calibration range.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Lab Sample ID: 490-49621-1Client Sample ID: SVE-1/MW-9
Matrix: Ground WaterDate Collected: 03/26/14 09:00
Date Received: 03/28/14 08:15
Method: SM6200-B - Volatile Organic Compounds
RL MDL
Benzene 29.4 0.500 ug/L 04/03/14 16:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.500 ug/L 04/03/14 16:33 1BromobenzeneND
0.500 ug/L 04/03/14 16:33 1BromochloromethaneND
0.500 ug/L 04/03/14 16:33 1BromodichloromethaneND
0.500 ug/L 04/03/14 16:33 1BromoformND
0.500 ug/L 04/03/14 16:33 1BromomethaneND
0.500 ug/L 04/03/14 16:33 1Carbon tetrachloride ND
0.500 ug/L 04/03/14 16:33 1ChlorobenzeneND
0.500 ug/L 04/03/14 16:33 1ChloroethaneND
0.500 ug/L 04/03/14 16:33 1ChloroformND
0.500 ug/L 04/03/14 16:33 1ChloromethaneND
0.500 ug/L 04/03/14 16:33 12-Chlorotoluene ND
0.500 ug/L 04/03/14 16:33 14-Chlorotoluene ND
0.500 ug/L 04/03/14 16:33 1cis-1,2-Dichloroethene 125
0.500 ug/L 04/03/14 16:33 1cis-1,3-Dichloropropene ND
0.500 ug/L 04/03/14 16:33 1DibromochloromethaneND
5.00 ug/L 04/03/14 16:33 11,2-Dibromo-3-Chloropropane ND
0.500 ug/L 04/03/14 16:33 11,2-Dibromoethane (EDB)ND
0.500 ug/L 04/03/14 16:33 1DibromomethaneND
0.500 ug/L 04/03/14 16:33 11,2-Dichlorobenzene ND
0.500 ug/L 04/03/14 16:33 11,3-Dichlorobenzene ND
0.500 ug/L 04/03/14 16:33 11,4-Dichlorobenzene ND
0.500 ug/L 04/03/14 16:33 1DichlorodifluoromethaneND
0.500 ug/L 04/03/14 16:33 11,1-Dichloroethane ND
0.500 ug/L 04/03/14 16:33 11,2-Dichloroethane ND
0.500 ug/L 04/03/14 16:33 11,1-Dichloroethene ND
0.500 ug/L 04/03/14 16:33 11,2-Dichloropropane ND
0.500 ug/L 04/03/14 16:33 11,3-Dichloropropane ND
0.500 ug/L 04/03/14 16:33 12,2-Dichloropropane ND
0.500 ug/L 04/03/14 16:33 11,1-Dichloropropene ND
0.500 ug/L 04/03/14 16:33 1Diisopropyl ether 4.24
100 ug/L 04/03/14 16:33 1EthanolND
10.0 ug/L 04/04/14 06:36 20Ethylbenzene1080
1.00 ug/L 04/03/14 16:33 1HexachlorobutadieneND
1.00 ug/L 04/03/14 16:33 1Isopropylbenzene113
5.00 ug/L 04/03/14 16:33 1Methylene Chloride ND
0.500 ug/L 04/03/14 16:33 1Methyl tert-butyl ether 76.2
100 ug/L 04/04/14 06:36 20Naphthalene1140
0.500 ug/L 04/03/14 16:33 1n-Butylbenzene 109
10.0 ug/L 04/04/14 06:36 20N-Propylbenzene 314
0.500 ug/L 04/03/14 16:33 1p-Isopropyltoluene 16.7
0.500 ug/L 04/03/14 16:33 1sec-Butylbenzene 31.5
0.500 ug/L 04/03/14 16:33 1StyreneND
0.500 ug/L 04/03/14 16:33 1tert-Butylbenzene ND
0.500 ug/L 04/03/14 16:33 11,1,1,2-Tetrachloroethane ND
0.500 ug/L 04/03/14 16:33 11,1,2,2-Tetrachloroethane ND
10.0 ug/L 04/04/14 06:36 20Tetrachloroethene1820
10.0 ug/L 04/04/14 06:36 20Toluene673
0.500 ug/L 04/03/14 16:33 1trans-1,2-Dichloroethene 1.37
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Client Sample Results
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Lab Sample ID: 490-49621-1Client Sample ID: SVE-1/MW-9
Matrix: Ground WaterDate Collected: 03/26/14 09:00
Date Received: 03/28/14 08:15
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
trans-1,3-Dichloropropene ND 0.500 ug/L 04/03/14 16:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.500 ug/L 04/03/14 16:33 11,2,3-Trichlorobenzene ND
0.500 ug/L 04/03/14 16:33 11,2,4-Trichlorobenzene ND
0.500 ug/L 04/03/14 16:33 11,1,1-Trichloroethane ND
0.500 ug/L 04/03/14 16:33 11,1,2-Trichloroethane ND
10.0 ug/L 04/04/14 06:36 20Trichloroethene331
0.500 ug/L 04/03/14 16:33 1TrichlorofluoromethaneND
0.500 ug/L 04/03/14 16:33 11,2,3-Trichloropropane ND
100 ug/L 04/04/14 07:05 2001,2,4-Trimethylbenzene 5830
10.0 ug/L 04/04/14 06:36 201,3,5-Trimethylbenzene 1450
0.500 ug/L 04/03/14 16:33 1Vinyl chloride ND
100 ug/L 04/04/14 07:05 200Xylenes, Total 16900
4-Bromofluorobenzene (Surr)113 70-130 04/03/14 16:33 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 04/04/14 06:36 2070-130
4-Bromofluorobenzene (Surr)95 04/04/14 07:05 20070-130
Dibromofluoromethane (Surr)106 04/03/14 16:33 170-130
Dibromofluoromethane (Surr)99 04/04/14 06:36 2070-130
Dibromofluoromethane (Surr)98 04/04/14 07:05 20070-130
1,2-Dichloroethane-d4 (Surr)122 04/03/14 16:33 170-130
1,2-Dichloroethane-d4 (Surr)98 04/04/14 06:36 2070-130
1,2-Dichloroethane-d4 (Surr)96 04/04/14 07:05 20070-130
Toluene-d8 (Surr)99 04/03/14 16:33 170-130
Toluene-d8 (Surr)97 04/04/14 06:36 2070-130
Toluene-d8 (Surr)97 04/04/14 07:05 20070-130
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Client Sample Results
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Lab Sample ID: 490-49621-2Client Sample ID: SVE-2
Matrix: Ground WaterDate Collected: 03/26/14 09:30
Date Received: 03/28/14 08:15
Method: SM6200-B - Volatile Organic Compounds
RL MDL
Benzene 229 10.0 ug/L 04/03/14 15:40 20
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 ug/L 04/03/14 15:40 20BromobenzeneND
10.0 ug/L 04/03/14 15:40 20BromochloromethaneND
10.0 ug/L 04/03/14 15:40 20BromodichloromethaneND
10.0 ug/L 04/03/14 15:40 20BromoformND
10.0 ug/L 04/03/14 15:40 20BromomethaneND
10.0 ug/L 04/03/14 15:40 20Carbon tetrachloride ND
10.0 ug/L 04/03/14 15:40 20ChlorobenzeneND
10.0 ug/L 04/03/14 15:40 20ChloroethaneND
10.0 ug/L 04/03/14 15:40 20ChloroformND
10.0 ug/L 04/03/14 15:40 20ChloromethaneND
10.0 ug/L 04/03/14 15:40 202-Chlorotoluene ND
10.0 ug/L 04/03/14 15:40 204-Chlorotoluene ND
10.0 ug/L 04/03/14 15:40 20cis-1,2-Dichloroethene 15.9
10.0 ug/L 04/03/14 15:40 20cis-1,3-Dichloropropene ND
10.0 ug/L 04/03/14 15:40 20DibromochloromethaneND
100 ug/L 04/03/14 15:40 201,2-Dibromo-3-Chloropropane ND
10.0 ug/L 04/03/14 15:40 201,2-Dibromoethane (EDB)ND
10.0 ug/L 04/03/14 15:40 20DibromomethaneND
10.0 ug/L 04/03/14 15:40 201,2-Dichlorobenzene ND
10.0 ug/L 04/03/14 15:40 201,3-Dichlorobenzene ND
10.0 ug/L 04/03/14 15:40 201,4-Dichlorobenzene ND
10.0 ug/L 04/03/14 15:40 20DichlorodifluoromethaneND
10.0 ug/L 04/03/14 15:40 201,1-Dichloroethane ND
10.0 ug/L 04/03/14 15:40 201,2-Dichloroethane ND
10.0 ug/L 04/03/14 15:40 201,1-Dichloroethene ND
10.0 ug/L 04/03/14 15:40 201,2-Dichloropropane ND
10.0 ug/L 04/03/14 15:40 201,3-Dichloropropane ND
10.0 ug/L 04/03/14 15:40 202,2-Dichloropropane ND
10.0 ug/L 04/03/14 15:40 201,1-Dichloropropene ND
10.0 ug/L 04/03/14 15:40 20Diisopropyl ether ND
2000 ug/L 04/03/14 15:40 20EthanolND
10.0 ug/L 04/03/14 15:40 20Ethylbenzene3580
20.0 ug/L 04/03/14 15:40 20HexachlorobutadieneND
20.0 ug/L 04/03/14 15:40 20Isopropylbenzene203
100 ug/L 04/03/14 15:40 20Methylene Chloride ND
10.0 ug/L 04/03/14 15:40 20Methyl tert-butyl ether 354
100 ug/L 04/03/14 15:40 20Naphthalene1290
10.0 ug/L 04/03/14 15:40 20n-Butylbenzene 179
10.0 ug/L 04/03/14 15:40 20N-Propylbenzene 632
10.0 ug/L 04/03/14 15:40 20p-Isopropyltoluene 21.3
10.0 ug/L 04/03/14 15:40 20sec-Butylbenzene 46.3
10.0 ug/L 04/03/14 15:40 20Styrene523
10.0 ug/L 04/03/14 15:40 20tert-Butylbenzene ND
10.0 ug/L 04/03/14 15:40 201,1,1,2-Tetrachloroethane ND
10.0 ug/L 04/03/14 15:40 201,1,2,2-Tetrachloroethane ND
10.0 ug/L 04/03/14 15:40 20Tetrachloroethene279
100 ug/L 04/03/14 16:06 200Toluene24100
10.0 ug/L 04/03/14 15:40 20trans-1,2-Dichloroethene ND
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Client Sample Results
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Lab Sample ID: 490-49621-2Client Sample ID: SVE-2
Matrix: Ground WaterDate Collected: 03/26/14 09:30
Date Received: 03/28/14 08:15
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
trans-1,3-Dichloropropene ND 10.0 ug/L 04/03/14 15:40 20
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 ug/L 04/03/14 15:40 201,2,3-Trichlorobenzene ND
10.0 ug/L 04/03/14 15:40 201,2,4-Trichlorobenzene ND
10.0 ug/L 04/03/14 15:40 201,1,1-Trichloroethane ND
10.0 ug/L 04/03/14 15:40 201,1,2-Trichloroethane ND
10.0 ug/L 04/03/14 15:40 20Trichloroethene133
10.0 ug/L 04/03/14 15:40 20TrichlorofluoromethaneND
10.0 ug/L 04/03/14 15:40 201,2,3-Trichloropropane ND
100 ug/L 04/03/14 16:06 2001,2,4-Trimethylbenzene 5800
10.0 ug/L 04/03/14 15:40 201,3,5-Trimethylbenzene 1550
10.0 ug/L 04/03/14 15:40 20Vinyl chloride ND
100 ug/L 04/03/14 16:06 200Xylenes, Total 31400
4-Bromofluorobenzene (Surr)105 70-130 04/03/14 15:40 20
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)104 04/03/14 16:06 20070-130
Dibromofluoromethane (Surr)106 04/03/14 15:40 2070-130
Dibromofluoromethane (Surr)108 04/03/14 16:06 20070-130
1,2-Dichloroethane-d4 (Surr)119 04/03/14 15:40 2070-130
1,2-Dichloroethane-d4 (Surr)122 04/03/14 16:06 20070-130
Toluene-d8 (Surr)104 04/03/14 15:40 2070-130
Toluene-d8 (Surr)100 04/03/14 16:06 20070-130
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Client Sample Results
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Lab Sample ID: 490-49621-3Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 03/26/14 00:01
Date Received: 03/28/14 08:15
Method: SM6200-B - Volatile Organic Compounds
RL MDL
Benzene ND 0.500 ug/L 04/03/14 13:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.500 ug/L 04/03/14 13:29 1BromobenzeneND
0.500 ug/L 04/03/14 13:29 1BromochloromethaneND
0.500 ug/L 04/03/14 13:29 1BromodichloromethaneND
0.500 ug/L 04/03/14 13:29 1BromoformND
0.500 ug/L 04/03/14 13:29 1BromomethaneND
0.500 ug/L 04/03/14 13:29 1Carbon tetrachloride ND
0.500 ug/L 04/03/14 13:29 1ChlorobenzeneND
0.500 ug/L 04/03/14 13:29 1ChloroethaneND
0.500 ug/L 04/03/14 13:29 1ChloroformND
0.500 ug/L 04/03/14 13:29 1ChloromethaneND
0.500 ug/L 04/03/14 13:29 12-Chlorotoluene ND
0.500 ug/L 04/03/14 13:29 14-Chlorotoluene ND
0.500 ug/L 04/03/14 13:29 1cis-1,2-Dichloroethene ND
0.500 ug/L 04/03/14 13:29 1cis-1,3-Dichloropropene ND
0.500 ug/L 04/03/14 13:29 1DibromochloromethaneND
5.00 ug/L 04/03/14 13:29 11,2-Dibromo-3-Chloropropane ND
0.500 ug/L 04/03/14 13:29 11,2-Dibromoethane (EDB)ND
0.500 ug/L 04/03/14 13:29 1DibromomethaneND
0.500 ug/L 04/03/14 13:29 11,2-Dichlorobenzene ND
0.500 ug/L 04/03/14 13:29 11,3-Dichlorobenzene ND
0.500 ug/L 04/03/14 13:29 11,4-Dichlorobenzene ND
0.500 ug/L 04/03/14 13:29 1DichlorodifluoromethaneND
0.500 ug/L 04/03/14 13:29 11,1-Dichloroethane ND
0.500 ug/L 04/03/14 13:29 11,2-Dichloroethane ND
0.500 ug/L 04/03/14 13:29 11,1-Dichloroethene ND
0.500 ug/L 04/03/14 13:29 11,2-Dichloropropane ND
0.500 ug/L 04/03/14 13:29 11,3-Dichloropropane ND
0.500 ug/L 04/03/14 13:29 12,2-Dichloropropane ND
0.500 ug/L 04/03/14 13:29 11,1-Dichloropropene ND
0.500 ug/L 04/03/14 13:29 1Diisopropyl ether ND
100 ug/L 04/03/14 13:29 1EthanolND
0.500 ug/L 04/03/14 13:29 1EthylbenzeneND
1.00 ug/L 04/03/14 13:29 1HexachlorobutadieneND
1.00 ug/L 04/03/14 13:29 1IsopropylbenzeneND
5.00 ug/L 04/03/14 13:29 1Methylene Chloride ND
0.500 ug/L 04/03/14 13:29 1Methyl tert-butyl ether ND
5.00 ug/L 04/03/14 13:29 1NaphthaleneND
0.500 ug/L 04/03/14 13:29 1n-Butylbenzene ND
0.500 ug/L 04/03/14 13:29 1N-Propylbenzene ND
0.500 ug/L 04/03/14 13:29 1p-Isopropyltoluene ND
0.500 ug/L 04/03/14 13:29 1sec-Butylbenzene ND
0.500 ug/L 04/03/14 13:29 1StyreneND
0.500 ug/L 04/03/14 13:29 1tert-Butylbenzene ND
0.500 ug/L 04/03/14 13:29 11,1,1,2-Tetrachloroethane ND
0.500 ug/L 04/03/14 13:29 11,1,2,2-Tetrachloroethane ND
0.500 ug/L 04/03/14 13:29 1TetrachloroetheneND
0.500 ug/L 04/03/14 13:29 1TolueneND
0.500 ug/L 04/03/14 13:29 1trans-1,2-Dichloroethene ND
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Client Sample Results
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Lab Sample ID: 490-49621-3Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 03/26/14 00:01
Date Received: 03/28/14 08:15
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
trans-1,3-Dichloropropene ND 0.500 ug/L 04/03/14 13:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.500 ug/L 04/03/14 13:29 11,2,3-Trichlorobenzene ND
0.500 ug/L 04/03/14 13:29 11,2,4-Trichlorobenzene ND
0.500 ug/L 04/03/14 13:29 11,1,1-Trichloroethane ND
0.500 ug/L 04/03/14 13:29 11,1,2-Trichloroethane ND
0.500 ug/L 04/03/14 13:29 1TrichloroetheneND
0.500 ug/L 04/03/14 13:29 1TrichlorofluoromethaneND
0.500 ug/L 04/03/14 13:29 11,2,3-Trichloropropane ND
0.500 ug/L 04/03/14 13:29 11,2,4-Trimethylbenzene ND
0.500 ug/L 04/03/14 13:29 11,3,5-Trimethylbenzene ND
0.500 ug/L 04/03/14 13:29 1Vinyl chloride ND
0.500 ug/L 04/03/14 13:29 1Xylenes, Total ND
4-Bromofluorobenzene (Surr)103 70-130 04/03/14 13:29 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)103 04/03/14 13:29 170-130
1,2-Dichloroethane-d4 (Surr)113 04/03/14 13:29 170-130
Toluene-d8 (Surr)102 04/03/14 13:29 170-130
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QC Sample Results
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Method: SM6200-B - Volatile Organic Compounds
Client Sample ID: Method BlankLab Sample ID: MB 490-152417/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 152417
RL MDL
Benzene ND 0.500 ug/L 04/03/14 13:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.500 ug/L 04/03/14 13:03 1Bromobenzene
ND 0.500 ug/L 04/03/14 13:03 1Bromochloromethane
ND 0.500 ug/L 04/03/14 13:03 1Bromodichloromethane
ND 0.500 ug/L 04/03/14 13:03 1Bromoform
ND 0.500 ug/L 04/03/14 13:03 1Bromomethane
ND 0.500 ug/L 04/03/14 13:03 1Carbon tetrachloride
ND 0.500 ug/L 04/03/14 13:03 1Chlorobenzene
ND 0.500 ug/L 04/03/14 13:03 1Chloroethane
ND 0.500 ug/L 04/03/14 13:03 1Chloroform
ND 0.500 ug/L 04/03/14 13:03 1Chloromethane
ND 0.500 ug/L 04/03/14 13:03 12-Chlorotoluene
ND 0.500 ug/L 04/03/14 13:03 14-Chlorotoluene
ND 0.500 ug/L 04/03/14 13:03 1cis-1,2-Dichloroethene
ND 0.500 ug/L 04/03/14 13:03 1cis-1,3-Dichloropropene
ND 0.500 ug/L 04/03/14 13:03 1Dibromochloromethane
ND 5.00 ug/L 04/03/14 13:03 11,2-Dibromo-3-Chloropropane
ND 0.500 ug/L 04/03/14 13:03 11,2-Dibromoethane (EDB)
ND 0.500 ug/L 04/03/14 13:03 1Dibromomethane
ND 0.500 ug/L 04/03/14 13:03 11,2-Dichlorobenzene
ND 0.500 ug/L 04/03/14 13:03 11,3-Dichlorobenzene
ND 0.500 ug/L 04/03/14 13:03 11,4-Dichlorobenzene
ND 0.500 ug/L 04/03/14 13:03 1Dichlorodifluoromethane
ND 0.500 ug/L 04/03/14 13:03 11,1-Dichloroethane
ND 0.500 ug/L 04/03/14 13:03 11,2-Dichloroethane
ND 0.500 ug/L 04/03/14 13:03 11,1-Dichloroethene
ND 0.500 ug/L 04/03/14 13:03 11,2-Dichloropropane
ND 0.500 ug/L 04/03/14 13:03 11,3-Dichloropropane
ND 0.500 ug/L 04/03/14 13:03 12,2-Dichloropropane
ND 0.500 ug/L 04/03/14 13:03 11,1-Dichloropropene
ND 0.500 ug/L 04/03/14 13:03 1Diisopropyl ether
ND 100 ug/L 04/03/14 13:03 1Ethanol
ND 0.500 ug/L 04/03/14 13:03 1Ethylbenzene
ND 1.00 ug/L 04/03/14 13:03 1Hexachlorobutadiene
ND 1.00 ug/L 04/03/14 13:03 1Isopropylbenzene
ND 5.00 ug/L 04/03/14 13:03 1Methylene Chloride
ND 0.500 ug/L 04/03/14 13:03 1Methyl tert-butyl ether
ND 5.00 ug/L 04/03/14 13:03 1Naphthalene
ND 0.500 ug/L 04/03/14 13:03 1n-Butylbenzene
ND 0.500 ug/L 04/03/14 13:03 1N-Propylbenzene
ND 0.500 ug/L 04/03/14 13:03 1p-Isopropyltoluene
ND 0.500 ug/L 04/03/14 13:03 1sec-Butylbenzene
ND 0.500 ug/L 04/03/14 13:03 1Styrene
ND 0.500 ug/L 04/03/14 13:03 1tert-Butylbenzene
ND 0.500 ug/L 04/03/14 13:03 11,1,1,2-Tetrachloroethane
ND 0.500 ug/L 04/03/14 13:03 11,1,2,2-Tetrachloroethane
ND 0.500 ug/L 04/03/14 13:03 1Tetrachloroethene
ND 0.500 ug/L 04/03/14 13:03 1Toluene
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QC Sample Results
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-152417/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 152417
RL MDL
trans-1,2-Dichloroethene ND 0.500 ug/L 04/03/14 13:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.500 ug/L 04/03/14 13:03 1trans-1,3-Dichloropropene
ND 0.500 ug/L 04/03/14 13:03 11,2,3-Trichlorobenzene
ND 0.500 ug/L 04/03/14 13:03 11,2,4-Trichlorobenzene
ND 0.500 ug/L 04/03/14 13:03 11,1,1-Trichloroethane
ND 0.500 ug/L 04/03/14 13:03 11,1,2-Trichloroethane
ND 0.500 ug/L 04/03/14 13:03 1Trichloroethene
ND 0.500 ug/L 04/03/14 13:03 1Trichlorofluoromethane
ND 0.500 ug/L 04/03/14 13:03 11,2,3-Trichloropropane
ND 0.500 ug/L 04/03/14 13:03 11,2,4-Trimethylbenzene
ND 0.500 ug/L 04/03/14 13:03 11,3,5-Trimethylbenzene
ND 0.500 ug/L 04/03/14 13:03 1Vinyl chloride
ND 0.500 ug/L 04/03/14 13:03 1Xylenes, Total
4-Bromofluorobenzene (Surr)104 70-130 04/03/14 13:03 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
109 04/03/14 13:03 1Dibromofluoromethane (Surr)70-130
123 04/03/14 13:03 11,2-Dichloroethane-d4 (Surr)70-130
102 04/03/14 13:03 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-152417/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 152417
Benzene 50.0 46.87 ug/L 94 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Bromobenzene 50.0 51.52 ug/L 103 70 -130
Bromochloromethane 50.0 48.42 ug/L 97 70 -130
Bromodichloromethane 50.0 54.98 ug/L 110 70 -130
Bromoform 50.0 59.47 ug/L 119 70 -130
Bromomethane 50.0 37.06 ug/L 74 60 -140
Carbon tetrachloride 50.0 60.14 ug/L 120 70 -130
Chlorobenzene 50.0 51.67 ug/L 103 70 -130
Chloroethane 50.0 42.38 ug/L 85 60 -140
Chloroform 50.0 52.40 ug/L 105 70 -130
Chloromethane 50.0 35.37 ug/L 71 60 -140
2-Chlorotoluene 50.0 50.32 ug/L 101 70 -130
4-Chlorotoluene 50.0 54.04 ug/L 108 70 -130
cis-1,2-Dichloroethene 50.0 47.59 ug/L 95 70 -130
cis-1,3-Dichloropropene 50.0 52.11 ug/L 104 70 -130
Dibromochloromethane 50.0 60.16 ug/L 120 70 -130
1,2-Dibromo-3-Chloropropane 50.0 56.74 ug/L 113 70 -130
Dibromomethane 50.0 52.13 ug/L 104 70 -130
1,2-Dichlorobenzene 50.0 53.70 ug/L 107 70 -130
1,3-Dichlorobenzene 50.0 53.61 ug/L 107 70 -130
1,4-Dichlorobenzene 50.0 52.79 ug/L 106 70 -130
Dichlorodifluoromethane 50.0 55.92 ug/L 112 60 -140
1,1-Dichloroethane 50.0 46.16 ug/L 92 70 -130
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QC Sample Results
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-152417/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 152417
1,2-Dichloroethane 50.0 56.39 ug/L 113 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1-Dichloroethene 50.0 50.93 ug/L 102 70 -130
1,2-Dichloropropane 50.0 43.64 ug/L 87 70 -130
1,3-Dichloropropane 50.0 53.56 ug/L 107 70 -130
2,2-Dichloropropane 50.0 53.32 ug/L 107 70 -130
1,1-Dichloropropene 50.0 50.11 ug/L 100 70 -130
Diisopropyl ether 50.0 40.78 ug/L 82 70 -130
Ethanol 2500 2103 ug/L 84 60 -140
Ethylbenzene 50.0 55.04 ug/L 110 70 -130
Hexachlorobutadiene 50.0 60.20 ug/L 120 70 -130
Isopropylbenzene 50.0 55.14 ug/L 110 70 -130
Methylene Chloride 50.0 49.21 ug/L 98 70 -130
Methyl tert-butyl ether 50.0 53.50 ug/L 107 70 -130
Naphthalene 50.0 59.82 ug/L 120 70 -130
n-Butylbenzene 50.0 54.20 ug/L 108 70 -130
N-Propylbenzene 50.0 54.46 ug/L 109 70 -130
p-Isopropyltoluene 50.0 56.29 ug/L 113 70 -130
sec-Butylbenzene 50.0 55.55 ug/L 111 70 -130
Styrene 50.0 56.81 ug/L 114 70 -130
tert-Butylbenzene 50.0 54.96 ug/L 110 70 -130
1,1,1,2-Tetrachloroethane 50.0 57.38 ug/L 115 70 -130
1,1,2,2-Tetrachloroethane 50.0 51.89 ug/L 104 70 -130
Tetrachloroethene 50.0 51.95 ug/L 104 70 -130
Toluene 50.0 52.02 ug/L 104 70 -130
trans-1,2-Dichloroethene 50.0 46.20 ug/L 92 70 -130
trans-1,3-Dichloropropene 50.0 58.13 ug/L 116 70 -130
1,2,3-Trichlorobenzene 50.0 60.88 ug/L 122 70 -130
1,2,4-Trichlorobenzene 50.0 56.97 ug/L 114 70 -130
1,1,1-Trichloroethane 50.0 57.39 ug/L 115 70 -130
1,1,2-Trichloroethane 50.0 51.58 ug/L 103 70 -130
Trichloroethene 50.0 52.02 ug/L 104 70 -130
Trichlorofluoromethane 50.0 55.22 ug/L 110 60 -140
1,2,3-Trichloropropane 50.0 54.28 ug/L 109 70 -130
1,2,4-Trimethylbenzene 50.0 55.62 ug/L 111 70 -130
1,3,5-Trimethylbenzene 50.0 55.86 ug/L 112 70 -130
Vinyl chloride 50.0 43.85 ug/L 88 60 -140
Xylenes, Total 100 109.0 ug/L 109 70 -130
4-Bromofluorobenzene (Surr)70 -130
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
104Dibromofluoromethane (Surr)70 -130
1201,2-Dichloroethane-d4 (Surr)70 -130
105Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-49372-B-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 152417
Benzene ND 50.0 48.63 ug/L 97 70 -130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Bromobenzene ND 50.0 53.81 ug/L 108 70 -130
Bromochloromethane ND 50.0 49.35 ug/L 99 70 -130
Bromodichloromethane ND 50.0 56.02 ug/L 112 70 -130
Bromoform ND 50.0 58.17 ug/L 116 70 -130
Bromomethane ND 50.0 30.01 ug/L 60 60 -140
Carbon tetrachloride ND 50.0 64.32 ug/L 129 70 -130
Chlorobenzene ND 50.0 52.96 ug/L 106 70 -130
Chloroethane ND 50.0 43.90 ug/L 88 60 -140
Chloroform ND 50.0 54.79 ug/L 110 70 -130
Chloromethane ND 50.0 39.15 ug/L 78 60 -140
2-Chlorotoluene ND 50.0 52.68 ug/L 105 70 -130
4-Chlorotoluene ND 50.0 55.63 ug/L 111 70 -130
cis-1,2-Dichloroethene ND 50.0 49.57 ug/L 99 70 -130
cis-1,3-Dichloropropene ND 50.0 53.52 ug/L 107 70 -130
Dibromochloromethane ND 50.0 60.06 ug/L 120 70 -130
1,2-Dibromo-3-Chloropropane ND 50.0 57.86 ug/L 116 70 -130
Dibromomethane ND 50.0 52.58 ug/L 105 70 -130
1,2-Dichlorobenzene ND 50.0 54.92 ug/L 110 70 -130
1,3-Dichlorobenzene ND 50.0 55.88 ug/L 112 70 -130
1,4-Dichlorobenzene ND 50.0 55.01 ug/L 110 70 -130
Dichlorodifluoromethane ND 50.0 39.55 ug/L 79 60 -140
1,1-Dichloroethane ND 50.0 49.42 ug/L 99 70 -130
1,2-Dichloroethane ND 50.0 56.99 ug/L 114 70 -130
1,1-Dichloroethene ND 50.0 54.73 ug/L 109 70 -130
1,2-Dichloropropane ND 50.0 44.75 ug/L 89 70 -130
1,3-Dichloropropane ND 50.0 55.77 ug/L 112 70 -130
2,2-Dichloropropane ND 50.0 54.27 ug/L 109 70 -130
1,1-Dichloropropene ND 50.0 53.13 ug/L 106 70 -130
Diisopropyl ether ND 50.0 42.84 ug/L 86 70 -130
Ethanol ND 2500 2006 ug/L 80 60 -140
Ethylbenzene ND 50.0 56.30 ug/L 113 70 -130
Hexachlorobutadiene ND 50.0 60.67 ug/L 121 70 -130
Isopropylbenzene ND 50.0 57.11 ug/L 114 70 -130
Methylene Chloride ND 50.0 50.97 ug/L 102 70 -130
Methyl tert-butyl ether ND 50.0 55.05 ug/L 110 70 -130
Naphthalene ND 50.0 62.17 ug/L 124 70 -130
n-Butylbenzene ND 50.0 57.69 ug/L 115 70 -130
N-Propylbenzene ND 50.0 58.32 ug/L 117 70 -130
p-Isopropyltoluene ND 50.0 59.08 ug/L 118 70 -130
sec-Butylbenzene ND 50.0 57.74 ug/L 115 70 -130
Styrene ND 50.0 57.12 ug/L 114 70 -130
tert-Butylbenzene ND 50.0 57.02 ug/L 114 70 -130
1,1,1,2-Tetrachloroethane ND 50.0 58.55 ug/L 117 70 -130
1,1,2,2-Tetrachloroethane ND 50.0 54.65 ug/L 109 70 -130
Tetrachloroethene ND 50.0 56.54 ug/L 113 70 -130
Toluene ND 50.0 53.91 ug/L 108 70 -130
trans-1,2-Dichloroethene ND 50.0 49.70 ug/L 99 70 -130
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QC Sample Results
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-49372-B-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 152417
trans-1,3-Dichloropropene ND 50.0 57.35 ug/L 115 70 -130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,2,3-Trichlorobenzene ND 50.0 61.96 ug/L 124 70 -130
1,2,4-Trichlorobenzene ND 50.0 58.16 ug/L 116 70 -130
1,1,1-Trichloroethane ND 50.0 61.61 ug/L 123 70 -130
1,1,2-Trichloroethane ND 50.0 52.80 ug/L 106 70 -130
Trichloroethene ND 50.0 54.13 ug/L 108 70 -130
Trichlorofluoromethane ND 50.0 59.70 ug/L 119 60 -140
1,2,3-Trichloropropane ND 50.0 56.51 ug/L 113 70 -130
1,2,4-Trimethylbenzene ND 50.0 57.98 ug/L 116 70 -130
1,3,5-Trimethylbenzene ND 50.0 57.85 ug/L 116 70 -130
Vinyl chloride ND 50.0 46.29 ug/L 93 60 -140
Xylenes, Total ND 100 112.2 ug/L 112 70 -130
4-Bromofluorobenzene (Surr)70 -130
Surrogate
107
MS MS
Qualifier Limits%Recovery
108Dibromofluoromethane (Surr)70 -130
1221,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-49372-C-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 152417
Benzene ND 50.0 49.32 ug/L 99 70 -130 1 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Bromobenzene ND 50.0 54.09 ug/L 108 70 -130 1 20
Bromochloromethane ND 50.0 49.54 ug/L 99 70 -130 0 20
Bromodichloromethane ND 50.0 56.39 ug/L 113 70 -130 1 20
Bromoform ND 50.0 55.49 ug/L 111 70 -130 5 20
Bromomethane ND 50.0 39.25 F2 ug/L 79 60 -140 27 20
Carbon tetrachloride ND 50.0 64.64 ug/L 129 70 -130 1 20
Chlorobenzene ND 50.0 53.06 ug/L 106 70 -130 0 20
Chloroethane ND 50.0 44.56 ug/L 89 60 -140 1 20
Chloroform ND 50.0 54.86 ug/L 110 70 -130 0 20
Chloromethane ND 50.0 38.62 ug/L 77 60 -140 1 20
2-Chlorotoluene ND 50.0 52.95 ug/L 106 70 -130 1 20
4-Chlorotoluene ND 50.0 55.95 ug/L 112 70 -130 1 20
cis-1,2-Dichloroethene ND 50.0 49.73 ug/L 99 70 -130 0 20
cis-1,3-Dichloropropene ND 50.0 53.72 ug/L 107 70 -130 0 20
Dibromochloromethane ND 50.0 59.42 ug/L 119 70 -130 1 20
1,2-Dibromo-3-Chloropropane ND 50.0 54.65 ug/L 109 70 -130 6 20
Dibromomethane ND 50.0 51.98 ug/L 104 70 -130 1 20
1,2-Dichlorobenzene ND 50.0 55.18 ug/L 110 70 -130 0 20
1,3-Dichlorobenzene ND 50.0 56.38 ug/L 113 70 -130 1 20
1,4-Dichlorobenzene ND 50.0 54.83 ug/L 110 70 -130 0 20
Dichlorodifluoromethane ND 50.0 49.61 F2 ug/L 99 60 -140 23 20
1,1-Dichloroethane ND 50.0 48.94 ug/L 98 70 -130 1 20
1,2-Dichloroethane ND 50.0 56.69 ug/L 113 70 -130 1 20
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QC Sample Results
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-49372-C-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 152417
1,1-Dichloroethene ND 50.0 54.12 ug/L 108 70 -130 1 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
1,2-Dichloropropane ND 50.0 45.23 ug/L 90 70 -130 1 20
1,3-Dichloropropane ND 50.0 53.26 ug/L 107 70 -130 5 20
2,2-Dichloropropane ND 50.0 54.40 ug/L 109 70 -130 0 20
1,1-Dichloropropene ND 50.0 53.40 ug/L 107 70 -130 0 20
Diisopropyl ether ND 50.0 41.19 ug/L 82 70 -130 4 20
Ethanol ND 2500 1422 F1 F2 ug/L 57 60 -140 34 20
Ethylbenzene ND 50.0 56.51 ug/L 113 70 -130 0 20
Hexachlorobutadiene ND 50.0 60.38 ug/L 121 70 -130 0 20
Isopropylbenzene ND 50.0 56.47 ug/L 113 70 -130 1 20
Methylene Chloride ND 50.0 50.53 ug/L 101 70 -130 1 20
Methyl tert-butyl ether ND 50.0 52.41 ug/L 105 70 -130 5 20
Naphthalene ND 50.0 57.35 ug/L 115 70 -130 8 20
n-Butylbenzene ND 50.0 58.65 ug/L 117 70 -130 2 20
N-Propylbenzene ND 50.0 58.82 ug/L 118 70 -130 1 20
p-Isopropyltoluene ND 50.0 59.61 ug/L 119 70 -130 1 20
sec-Butylbenzene ND 50.0 59.28 ug/L 119 70 -130 3 20
Styrene ND 50.0 56.55 ug/L 113 70 -130 1 20
tert-Butylbenzene ND 50.0 58.66 ug/L 117 70 -130 3 20
1,1,1,2-Tetrachloroethane ND 50.0 57.62 ug/L 115 70 -130 2 20
1,1,2,2-Tetrachloroethane ND 50.0 51.67 ug/L 103 70 -130 6 20
Tetrachloroethene ND 50.0 55.50 ug/L 111 70 -130 2 20
Toluene ND 50.0 54.07 ug/L 108 70 -130 0 20
trans-1,2-Dichloroethene ND 50.0 49.40 ug/L 99 70 -130 1 20
trans-1,3-Dichloropropene ND 50.0 57.67 ug/L 115 70 -130 1 20
1,2,3-Trichlorobenzene ND 50.0 60.20 ug/L 120 70 -130 3 20
1,2,4-Trichlorobenzene ND 50.0 56.65 ug/L 113 70 -130 3 20
1,1,1-Trichloroethane ND 50.0 60.68 ug/L 121 70 -130 2 20
1,1,2-Trichloroethane ND 50.0 51.94 ug/L 104 70 -130 2 20
Trichloroethene ND 50.0 54.51 ug/L 109 70 -130 1 20
Trichlorofluoromethane ND 50.0 60.12 ug/L 120 60 -140 1 20
1,2,3-Trichloropropane ND 50.0 52.62 ug/L 105 70 -130 7 20
1,2,4-Trimethylbenzene ND 50.0 58.96 ug/L 118 70 -130 2 20
1,3,5-Trimethylbenzene ND 50.0 58.12 ug/L 116 70 -130 0 20
Vinyl chloride ND 50.0 45.39 ug/L 91 60 -140 2 20
Xylenes, Total ND 100 111.0 ug/L 111 70 -130 1 20
4-Bromofluorobenzene (Surr)70 -130
Surrogate
104
MSD MSD
Qualifier Limits%Recovery
105Dibromofluoromethane (Surr)70 -130
1191,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-152647/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 152647
RL MDL
Benzene ND 0.500 ug/L 04/04/14 01:23 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.500 ug/L 04/04/14 01:23 1Bromobenzene
ND 0.500 ug/L 04/04/14 01:23 1Bromochloromethane
ND 0.500 ug/L 04/04/14 01:23 1Bromodichloromethane
ND 0.500 ug/L 04/04/14 01:23 1Bromoform
ND 0.500 ug/L 04/04/14 01:23 1Bromomethane
ND 0.500 ug/L 04/04/14 01:23 1Carbon tetrachloride
ND 0.500 ug/L 04/04/14 01:23 1Chlorobenzene
ND 0.500 ug/L 04/04/14 01:23 1Chloroethane
ND 0.500 ug/L 04/04/14 01:23 1Chloroform
ND 0.500 ug/L 04/04/14 01:23 1Chloromethane
ND 0.500 ug/L 04/04/14 01:23 12-Chlorotoluene
ND 0.500 ug/L 04/04/14 01:23 14-Chlorotoluene
ND 0.500 ug/L 04/04/14 01:23 1cis-1,2-Dichloroethene
ND 0.500 ug/L 04/04/14 01:23 1cis-1,3-Dichloropropene
ND 0.500 ug/L 04/04/14 01:23 1Dibromochloromethane
ND 5.00 ug/L 04/04/14 01:23 11,2-Dibromo-3-Chloropropane
ND 0.500 ug/L 04/04/14 01:23 11,2-Dibromoethane (EDB)
ND 0.500 ug/L 04/04/14 01:23 1Dibromomethane
ND 0.500 ug/L 04/04/14 01:23 11,2-Dichlorobenzene
ND 0.500 ug/L 04/04/14 01:23 11,3-Dichlorobenzene
ND 0.500 ug/L 04/04/14 01:23 11,4-Dichlorobenzene
ND 0.500 ug/L 04/04/14 01:23 1Dichlorodifluoromethane
ND 0.500 ug/L 04/04/14 01:23 11,1-Dichloroethane
ND 0.500 ug/L 04/04/14 01:23 11,2-Dichloroethane
ND 0.500 ug/L 04/04/14 01:23 11,1-Dichloroethene
ND 0.500 ug/L 04/04/14 01:23 11,2-Dichloropropane
ND 0.500 ug/L 04/04/14 01:23 11,3-Dichloropropane
ND 0.500 ug/L 04/04/14 01:23 12,2-Dichloropropane
ND 0.500 ug/L 04/04/14 01:23 11,1-Dichloropropene
ND 0.500 ug/L 04/04/14 01:23 1Diisopropyl ether
ND 100 ug/L 04/04/14 01:23 1Ethanol
ND 0.500 ug/L 04/04/14 01:23 1Ethylbenzene
ND 1.00 ug/L 04/04/14 01:23 1Hexachlorobutadiene
ND 1.00 ug/L 04/04/14 01:23 1Isopropylbenzene
ND 5.00 ug/L 04/04/14 01:23 1Methylene Chloride
ND 0.500 ug/L 04/04/14 01:23 1Methyl tert-butyl ether
ND 5.00 ug/L 04/04/14 01:23 1Naphthalene
ND 0.500 ug/L 04/04/14 01:23 1n-Butylbenzene
ND 0.500 ug/L 04/04/14 01:23 1N-Propylbenzene
ND 0.500 ug/L 04/04/14 01:23 1p-Isopropyltoluene
ND 0.500 ug/L 04/04/14 01:23 1sec-Butylbenzene
ND 0.500 ug/L 04/04/14 01:23 1Styrene
ND 0.500 ug/L 04/04/14 01:23 1tert-Butylbenzene
ND 0.500 ug/L 04/04/14 01:23 11,1,1,2-Tetrachloroethane
ND 0.500 ug/L 04/04/14 01:23 11,1,2,2-Tetrachloroethane
ND 0.500 ug/L 04/04/14 01:23 1Tetrachloroethene
ND 0.500 ug/L 04/04/14 01:23 1Toluene
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QC Sample Results
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-152647/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 152647
RL MDL
trans-1,2-Dichloroethene ND 0.500 ug/L 04/04/14 01:23 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.500 ug/L 04/04/14 01:23 1trans-1,3-Dichloropropene
ND 0.500 ug/L 04/04/14 01:23 11,2,3-Trichlorobenzene
ND 0.500 ug/L 04/04/14 01:23 11,2,4-Trichlorobenzene
ND 0.500 ug/L 04/04/14 01:23 11,1,1-Trichloroethane
ND 0.500 ug/L 04/04/14 01:23 11,1,2-Trichloroethane
ND 0.500 ug/L 04/04/14 01:23 1Trichloroethene
ND 0.500 ug/L 04/04/14 01:23 1Trichlorofluoromethane
ND 0.500 ug/L 04/04/14 01:23 11,2,3-Trichloropropane
ND 0.500 ug/L 04/04/14 01:23 11,2,4-Trimethylbenzene
ND 0.500 ug/L 04/04/14 01:23 11,3,5-Trimethylbenzene
ND 0.500 ug/L 04/04/14 01:23 1Vinyl chloride
ND 0.500 ug/L 04/04/14 01:23 1Xylenes, Total
4-Bromofluorobenzene (Surr)95 70-130 04/04/14 01:23 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
100 04/04/14 01:23 1Dibromofluoromethane (Surr)70-130
102 04/04/14 01:23 11,2-Dichloroethane-d4 (Surr)70-130
99 04/04/14 01:23 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-152647/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 152647
Benzene 50.0 50.60 ug/L 101 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Bromobenzene 50.0 49.72 ug/L 99 70 -130
Bromochloromethane 50.0 53.93 ug/L 108 70 -130
Bromodichloromethane 50.0 52.23 ug/L 104 70 -130
Bromoform 50.0 56.72 ug/L 113 70 -130
Bromomethane 50.0 58.47 ug/L 117 60 -140
Carbon tetrachloride 50.0 53.55 ug/L 107 70 -130
Chlorobenzene 50.0 50.96 ug/L 102 70 -130
Chloroethane 50.0 51.46 ug/L 103 60 -140
Chloroform 50.0 52.51 ug/L 105 70 -130
Chloromethane 50.0 52.36 ug/L 105 60 -140
2-Chlorotoluene 50.0 49.41 ug/L 99 70 -130
4-Chlorotoluene 50.0 51.16 ug/L 102 70 -130
cis-1,2-Dichloroethene 50.0 55.20 ug/L 110 70 -130
cis-1,3-Dichloropropene 50.0 51.60 ug/L 103 70 -130
Dibromochloromethane 50.0 55.27 ug/L 111 70 -130
1,2-Dibromo-3-Chloropropane 50.0 53.48 ug/L 107 70 -130
Dibromomethane 50.0 51.56 ug/L 103 70 -130
1,2-Dichlorobenzene 50.0 53.49 ug/L 107 70 -130
1,3-Dichlorobenzene 50.0 53.03 ug/L 106 70 -130
1,4-Dichlorobenzene 50.0 52.18 ug/L 104 70 -130
Dichlorodifluoromethane 50.0 59.80 ug/L 120 60 -140
1,1-Dichloroethane 50.0 48.22 ug/L 96 70 -130
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QC Sample Results
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-152647/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 152647
1,2-Dichloroethane 50.0 50.11 ug/L 100 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1-Dichloroethene 50.0 50.21 ug/L 100 70 -130
1,2-Dichloropropane 50.0 50.44 ug/L 101 70 -130
1,3-Dichloropropane 50.0 50.14 ug/L 100 70 -130
2,2-Dichloropropane 50.0 49.17 ug/L 98 70 -130
1,1-Dichloropropene 50.0 51.06 ug/L 102 70 -130
Diisopropyl ether 50.0 50.08 ug/L 100 70 -130
Ethanol 2500 2734 ug/L 109 60 -140
Ethylbenzene 50.0 50.77 ug/L 102 70 -130
Hexachlorobutadiene 50.0 54.82 ug/L 110 70 -130
Isopropylbenzene 50.0 52.13 ug/L 104 70 -130
Methylene Chloride 50.0 52.04 ug/L 104 70 -130
Methyl tert-butyl ether 50.0 48.95 ug/L 98 70 -130
Naphthalene 50.0 55.71 ug/L 111 70 -130
n-Butylbenzene 50.0 52.73 ug/L 105 70 -130
N-Propylbenzene 50.0 53.39 ug/L 107 70 -130
p-Isopropyltoluene 50.0 54.89 ug/L 110 70 -130
sec-Butylbenzene 50.0 53.16 ug/L 106 70 -130
Styrene 50.0 53.52 ug/L 107 70 -130
tert-Butylbenzene 50.0 53.09 ug/L 106 70 -130
1,1,1,2-Tetrachloroethane 50.0 52.99 ug/L 106 70 -130
1,1,2,2-Tetrachloroethane 50.0 50.81 ug/L 102 70 -130
Tetrachloroethene 50.0 50.59 ug/L 101 70 -130
Toluene 50.0 49.59 ug/L 99 70 -130
trans-1,2-Dichloroethene 50.0 51.10 ug/L 102 70 -130
trans-1,3-Dichloropropene 50.0 53.92 ug/L 108 70 -130
1,2,3-Trichlorobenzene 50.0 57.29 ug/L 115 70 -130
1,2,4-Trichlorobenzene 50.0 54.34 ug/L 109 70 -130
1,1,1-Trichloroethane 50.0 52.18 ug/L 104 70 -130
1,1,2-Trichloroethane 50.0 49.16 ug/L 98 70 -130
Trichloroethene 50.0 51.88 ug/L 104 70 -130
Trichlorofluoromethane 50.0 52.38 ug/L 105 60 -140
1,2,3-Trichloropropane 50.0 54.18 ug/L 108 70 -130
1,2,4-Trimethylbenzene 50.0 53.38 ug/L 107 70 -130
1,3,5-Trimethylbenzene 50.0 52.78 ug/L 106 70 -130
Vinyl chloride 50.0 53.22 ug/L 106 60 -140
Xylenes, Total 100 101.8 ug/L 102 70 -130
4-Bromofluorobenzene (Surr)70 -130
Surrogate
99
LCS LCS
Qualifier Limits%Recovery
101Dibromofluoromethane (Surr)70 -130
1001,2-Dichloroethane-d4 (Surr)70 -130
99Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-49617-B-3 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 152647
Benzene ND 50.0 52.65 ug/L 104 70 -130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Bromobenzene ND 50.0 50.80 ug/L 102 70 -130
Bromochloromethane ND 50.0 52.65 ug/L 105 70 -130
Bromodichloromethane ND 50.0 52.67 ug/L 105 70 -130
Bromoform ND 50.0 54.49 ug/L 109 70 -130
Bromomethane ND 50.0 55.14 ug/L 110 60 -140
Carbon tetrachloride ND 50.0 58.00 ug/L 116 70 -130
Chlorobenzene ND 50.0 52.96 ug/L 106 70 -130
Chloroethane ND 50.0 52.28 ug/L 105 60 -140
Chloroform ND 50.0 53.52 ug/L 107 70 -130
Chloromethane ND 50.0 46.13 ug/L 92 60 -140
2-Chlorotoluene ND 50.0 51.75 ug/L 104 70 -130
4-Chlorotoluene ND 50.0 53.98 ug/L 108 70 -130
cis-1,2-Dichloroethene ND 50.0 54.01 ug/L 108 70 -130
cis-1,3-Dichloropropene ND 50.0 52.97 ug/L 106 70 -130
Dibromochloromethane ND 50.0 54.51 ug/L 109 70 -130
1,2-Dibromo-3-Chloropropane ND 50.0 50.48 ug/L 101 70 -130
Dibromomethane ND 50.0 51.93 ug/L 104 70 -130
1,2-Dichlorobenzene ND 50.0 54.16 ug/L 108 70 -130
1,3-Dichlorobenzene ND 50.0 56.23 ug/L 112 70 -130
1,4-Dichlorobenzene ND 50.0 54.30 ug/L 109 70 -130
Dichlorodifluoromethane ND 50.0 51.10 ug/L 102 60 -140
1,1-Dichloroethane ND 50.0 56.35 ug/L 113 70 -130
1,2-Dichloroethane 9.31 50.0 58.21 ug/L 98 70 -130
1,1-Dichloroethene ND 50.0 55.67 ug/L 111 70 -130
1,2-Dichloropropane ND 50.0 50.75 ug/L 101 70 -130
1,3-Dichloropropane ND 50.0 48.29 ug/L 97 70 -130
2,2-Dichloropropane ND 50.0 54.37 E ug/L 109 70 -130
1,1-Dichloropropene ND 50.0 55.36 ug/L 111 70 -130
Diisopropyl ether 97.4 50.0 152.2 ug/L 110 70 -130
Ethanol ND 2500 1180 F1 ug/L 47 60 -140
Ethylbenzene ND 50.0 52.91 ug/L 106 70 -130
Hexachlorobutadiene ND 50.0 61.75 ug/L 123 70 -130
Isopropylbenzene ND 50.0 55.02 ug/L 110 70 -130
Methylene Chloride ND 50.0 55.34 ug/L 110 70 -130
Methyl tert-butyl ether 12.8 50.0 61.64 ug/L 98 70 -130
Naphthalene ND 50.0 51.13 ug/L 102 70 -130
n-Butylbenzene ND 50.0 57.47 ug/L 115 70 -130
N-Propylbenzene ND 50.0 57.38 ug/L 115 70 -130
p-Isopropyltoluene ND 50.0 58.95 ug/L 118 70 -130
sec-Butylbenzene ND 50.0 57.45 ug/L 115 70 -130
Styrene ND 50.0 54.29 ug/L 109 70 -130
tert-Butylbenzene ND 50.0 57.23 ug/L 114 70 -130
1,1,1,2-Tetrachloroethane ND 50.0 54.36 ug/L 109 70 -130
1,1,2,2-Tetrachloroethane ND 50.0 49.42 ug/L 99 70 -130
Tetrachloroethene ND 50.0 56.23 ug/L 112 70 -130
Toluene 0.568 50.0 52.71 ug/L 104 70 -130
trans-1,2-Dichloroethene ND 50.0 56.03 ug/L 112 70 -130
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QC Sample Results
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-49617-B-3 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 152647
trans-1,3-Dichloropropene ND 50.0 54.43 ug/L 109 70 -130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,2,3-Trichlorobenzene ND 50.0 54.72 ug/L 109 70 -130
1,2,4-Trichlorobenzene ND 50.0 55.67 ug/L 111 70 -130
1,1,1-Trichloroethane ND 50.0 55.26 ug/L 111 70 -130
1,1,2-Trichloroethane ND 50.0 48.80 ug/L 98 70 -130
Trichloroethene ND 50.0 56.32 ug/L 113 70 -130
Trichlorofluoromethane ND 50.0 56.60 ug/L 113 60 -140
1,2,3-Trichloropropane ND 50.0 52.44 ug/L 105 70 -130
1,2,4-Trimethylbenzene ND 50.0 56.55 ug/L 113 70 -130
1,3,5-Trimethylbenzene ND 50.0 56.39 ug/L 113 70 -130
Vinyl chloride ND 50.0 52.95 ug/L 106 60 -140
Xylenes, Total ND 100 106.7 ug/L 107 70 -130
4-Bromofluorobenzene (Surr)70 -130
Surrogate
100
MS MS
Qualifier Limits%Recovery
101Dibromofluoromethane (Surr)70 -130
981,2-Dichloroethane-d4 (Surr)70 -130
98Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-49617-C-3 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 152647
Benzene ND 50.0 53.55 ug/L 106 70 -130 2 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Bromobenzene ND 50.0 53.01 ug/L 106 70 -130 4 20
Bromochloromethane ND 50.0 53.13 ug/L 106 70 -130 1 20
Bromodichloromethane ND 50.0 54.24 ug/L 108 70 -130 3 20
Bromoform ND 50.0 56.33 ug/L 113 70 -130 3 20
Bromomethane ND 50.0 54.15 ug/L 108 60 -140 2 20
Carbon tetrachloride ND 50.0 58.94 ug/L 118 70 -130 2 20
Chlorobenzene ND 50.0 54.09 ug/L 108 70 -130 2 20
Chloroethane ND 50.0 52.17 ug/L 104 60 -140 0 20
Chloroform ND 50.0 54.35 ug/L 109 70 -130 2 20
Chloromethane ND 50.0 47.35 ug/L 95 60 -140 3 20
2-Chlorotoluene ND 50.0 53.69 ug/L 107 70 -130 4 20
4-Chlorotoluene ND 50.0 55.48 ug/L 111 70 -130 3 20
cis-1,2-Dichloroethene ND 50.0 53.19 ug/L 106 70 -130 2 20
cis-1,3-Dichloropropene ND 50.0 54.80 ug/L 110 70 -130 3 20
Dibromochloromethane ND 50.0 55.90 ug/L 112 70 -130 3 20
1,2-Dibromo-3-Chloropropane ND 50.0 51.57 ug/L 103 70 -130 2 20
Dibromomethane ND 50.0 53.01 ug/L 106 70 -130 2 20
1,2-Dichlorobenzene ND 50.0 54.86 ug/L 110 70 -130 1 20
1,3-Dichlorobenzene ND 50.0 57.53 ug/L 115 70 -130 2 20
1,4-Dichlorobenzene ND 50.0 55.23 ug/L 110 70 -130 2 20
Dichlorodifluoromethane ND 50.0 51.68 ug/L 103 60 -140 1 20
1,1-Dichloroethane ND 50.0 54.98 ug/L 110 70 -130 2 20
1,2-Dichloroethane 9.31 50.0 59.04 ug/L 99 70 -130 1 20
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QC Sample Results
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-49617-C-3 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 152647
1,1-Dichloroethene ND 50.0 55.35 ug/L 111 70 -130 1 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
1,2-Dichloropropane ND 50.0 51.38 ug/L 103 70 -130 1 20
1,3-Dichloropropane ND 50.0 49.68 ug/L 99 70 -130 3 20
2,2-Dichloropropane ND 50.0 53.36 E ug/L 107 70 -130 2 20
1,1-Dichloropropene ND 50.0 55.87 ug/L 112 70 -130 1 20
Diisopropyl ether 97.4 50.0 149.4 ug/L 104 70 -130 2 20
Ethanol ND 2500 2535 F2 ug/L 101 60 -140 73 20
Ethylbenzene ND 50.0 54.05 ug/L 108 70 -130 2 20
Hexachlorobutadiene ND 50.0 64.32 ug/L 129 70 -130 4 20
Isopropylbenzene ND 50.0 56.07 ug/L 112 70 -130 2 20
Methylene Chloride ND 50.0 55.41 ug/L 110 70 -130 0 20
Methyl tert-butyl ether 12.8 50.0 61.59 ug/L 98 70 -130 0 20
Naphthalene ND 50.0 56.68 ug/L 113 70 -130 10 20
n-Butylbenzene ND 50.0 59.42 ug/L 119 70 -130 3 20
N-Propylbenzene ND 50.0 59.68 ug/L 119 70 -130 4 20
p-Isopropyltoluene ND 50.0 60.73 ug/L 121 70 -130 3 20
sec-Butylbenzene ND 50.0 59.04 ug/L 118 70 -130 3 20
Styrene ND 50.0 55.64 ug/L 111 70 -130 2 20
tert-Butylbenzene ND 50.0 59.42 ug/L 119 70 -130 4 20
1,1,1,2-Tetrachloroethane ND 50.0 55.51 ug/L 111 70 -130 2 20
1,1,2,2-Tetrachloroethane ND 50.0 51.00 ug/L 102 70 -130 3 20
Tetrachloroethene ND 50.0 57.12 ug/L 114 70 -130 2 20
Toluene 0.568 50.0 53.47 ug/L 106 70 -130 1 20
trans-1,2-Dichloroethene ND 50.0 56.82 ug/L 114 70 -130 1 20
trans-1,3-Dichloropropene ND 50.0 55.88 ug/L 112 70 -130 3 20
1,2,3-Trichlorobenzene ND 50.0 61.11 ug/L 122 70 -130 11 20
1,2,4-Trichlorobenzene ND 50.0 59.03 ug/L 118 70 -130 6 20
1,1,1-Trichloroethane ND 50.0 56.00 ug/L 112 70 -130 1 20
1,1,2-Trichloroethane ND 50.0 49.86 ug/L 100 70 -130 2 20
Trichloroethene ND 50.0 56.64 ug/L 113 70 -130 1 20
Trichlorofluoromethane ND 50.0 56.60 ug/L 113 60 -140 0 20
1,2,3-Trichloropropane ND 50.0 54.67 ug/L 109 70 -130 4 20
1,2,4-Trimethylbenzene ND 50.0 57.32 ug/L 115 70 -130 1 20
1,3,5-Trimethylbenzene ND 50.0 57.46 ug/L 115 70 -130 2 20
Vinyl chloride ND 50.0 53.03 ug/L 106 60 -140 0 20
Xylenes, Total ND 100 109.0 ug/L 109 70 -130 2 20
4-Bromofluorobenzene (Surr)70 -130
Surrogate
101
MSD MSD
Qualifier Limits%Recovery
101Dibromofluoromethane (Surr)70 -130
971,2-Dichloroethane-d4 (Surr)70 -130
99Toluene-d8 (Surr)70 -130
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QC Association Summary
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
GC/MS VOA
Analysis Batch: 152417
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM6200-B490-49372-B-1 MS Matrix Spike Total/NA
Water SM6200-B490-49372-C-1 MSD Matrix Spike Duplicate Total/NA
Ground Water SM6200-B490-49621-1 SVE-1/MW-9 Total/NA
Ground Water SM6200-B490-49621-2 SVE-2 Total/NA
Ground Water SM6200-B490-49621-2 SVE-2 Total/NA
Water SM6200-B490-49621-3 Trip Blank Total/NA
Water SM6200-BLCS 490-152417/3 Lab Control Sample Total/NA
Water SM6200-BMB 490-152417/6 Method Blank Total/NA
Analysis Batch: 152647
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM6200-B490-49617-B-3 MS Matrix Spike Total/NA
Water SM6200-B490-49617-C-3 MSD Matrix Spike Duplicate Total/NA
Ground Water SM6200-B490-49621-1 SVE-1/MW-9 Total/NA
Ground Water SM6200-B490-49621-1 SVE-1/MW-9 Total/NA
Water SM6200-BLCS 490-152647/4 Lab Control Sample Total/NA
Water SM6200-BMB 490-152647/8 Method Blank Total/NA
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Lab Chronicle
Client: ARCADIS U.S. Inc TestAmerica Job ID: 490-49621-1
Project/Site: EM 40962 SDG: 5001 Raeford Road, Fayetteville, NC
Client Sample ID: SVE-1/MW-9 Lab Sample ID: 490-49621-1
Matrix: Ground WaterDate Collected: 03/26/14 09:00
Date Received: 03/28/14 08:15
Analysis SM6200-B EML04/04/14 06:3620 TAL NSH152647
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Analysis SM6200-B 200 152647 04/04/14 07:05 EML TAL NSHTotal/NA 10 mL 10 mL
Analysis SM6200-B 1 152417 04/03/14 16:33 EML TAL NSHTotal/NA 10 mL 10 mL
Client Sample ID: SVE-2 Lab Sample ID: 490-49621-2
Matrix: Ground WaterDate Collected: 03/26/14 09:30
Date Received: 03/28/14 08:15
Analysis SM6200-B EML04/03/14 15:4020 TAL NSH152417
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Analysis SM6200-B 200 152417 04/03/14 16:06 EML TAL NSHTotal/NA 10 mL 10 mL
Client Sample ID: Trip Blank Lab Sample ID: 490-49621-3
Matrix: WaterDate Collected: 03/26/14 00:01
Date Received: 03/28/14 08:15
Analysis SM6200-B EML04/03/14 13:291 TAL NSH152417
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177
TestAmerica Nashville
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Method Summary
TestAmerica Job ID: 490-49621-1Client: ARCADIS U.S. Inc
SDG: 5001 Raeford Road, Fayetteville, NCProject/Site: EM 40962
Method Method Description LaboratoryProtocol
SMSM6200-B Volatile Organic Compounds TAL NSH
Protocol References:
SM = "Standard Methods For The Examination Of Water And Wastewater",
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177
TestAmerica Nashville
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Certification Summary
Client: ARCADIS U.S. Inc TestAmerica Job ID: 490-49621-1
Project/Site: EM 40962 SDG: 5001 Raeford Road, Fayetteville, NC
Laboratory: TestAmerica Nashville
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
North Carolina DENR 3874State Program 12-31-14
TestAmerica Nashville
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Login Sample Receipt Checklist
Client: ARCADIS U.S. Inc Job Number: 490-49621-1
SDG Number: 5001 Raeford Road, Fayetteville, NC
Login Number: 49621
Question Answer Comment
Creator: Huckaba, Jimmy
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
FalseContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
Refer to Job Narrative for details.
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
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