19007_North Graham Street_CAP Report_2012618

CORRECTIVE ACTION PLAN
SOUTHERN PUMP AND TANK COMPANY
4800 NORTH GRAHAM STREETCHARLOTTE, NORTH CAROLINANCDENR INCIDENT: 36702
Prepared for:
D & B FINANCE COMPANY, LLC
AND
SOUTHERN PUMP AND TANK COMPANY, LLC
Prepared by:
AMEC Environment & Infrastructure, Inc.
2801 YORKMONT ROADCHARLOTTE, NORTH CAROLINA 28208
AMEC Project No. 6228-13-0135
JUNE 18, 2012REVISEDJANUARY20,2015
EXECUTIVE SUMMARY
AMEC Environment and Infrastructure, Inc.
I
EXECUTIVE SUMMARY
The purpose of this report is to summarize environmental conditions and to evaluate and
propose actions to remediate soil and groundwater contamination at the Southern Pump and
Tank Company (SPATCO) facility (Site) in Charlotte, North Carolina. This Corrective Action
Plan (CAP) was prepared in general accordance with the requirements outlined in the Notice of
Regulatory Requirements (NORR) issued by the North Carolina Department of Environment
and Natural Resources (NCDENR) dated July 29, 2011, subsequent Notices of Violation (NOV)
dated August 31, 2012 and July 22, 2013,and the NCDENR’s Guidelines for Assessment and
Corrective Action for UST Releases (Guidelines), effective July 15, 2008 (change 2, effective
October 1, 2012).Copies of the NORR and subsequent NOVs have been included in
Appendix A.
The Site is located at 4800 North Graham Street in a mixed-use residential/commercial/
industrial area of Charlotte, Mecklenburg County, North Carolina (Figure 1). The Site is
occupied by SPATCO and used for administrative offices and to store and clean petroleum
dispensing equipment. Reportedly, 12 underground storage tanks (USTs) containing various
petroleum products and wash water from the cleaning of petroleum equipment (which involved
the use of some chlorinated solvent cleaning compounds)were removed prior to 1988.
In October 2008 AMEC (as MACTEC Engineering and Consulting, Inc.) conducted a soil quality
evaluation.As part of this evaluation,AMEC collected soil samples from several areas of the
Site including a former UST basin north of the on-site building (former Northern UST Basin), a
former UST basin located west of the on-site building (former Western UST Basin) and a floor
pit located inside the maintenance portion of the on-site building. Results of soil samples
collected during the initial assessment indicated the presence of volatile organic compound
(VOC) impacted soils in the vicinity of the three investigation areas. Based on information
obtained from SPATCO personnel, the former Northern UST Basin contained two USTs of
unknown contents, while the former Western UST Basin contained 10 USTs and an associated
dispenser island. Reportedly, the majority of tanks in the former Western UST Basin contained
diesel and gasoline for use in SPATCO fleet and service vehicles with two USTs receiving wash
water generated during cleaning of petroleum dispensers and parts inside the building.
EXECUTIVE SUMMARY
AMEC Environment and Infrastructure, Inc.
II
Subsequent assessment activities included completion of a Limited Site Assessment (LSA)
between February and May 2009, a Comprehensive Site Assessment (CSA) in January 2010,
and an Addendum to the CSA between January and April 2011.A total of 18 Type II monitoring
wells (MW-1 through MW-18) and two Type III monitoring wells (DMW-1 and DMW-2) were
installed during these activities. Please note that well MW-2 was installed as a 1-inch diameter
well due to limitations on the accessibility of equipment under the metal canopy in the rear of the
building. The results of these assessment activities were documented in a LSA Report dated
July 15, 2009, a CSA Report dated May 26, 2010, and an Addendum to the CSA Report dated
July 2, 2011. The locations of wells installed during these previous investigations are shown on
Figure 2.
The contaminants of concern at the Site are primarily petroleum-related, with the exception of
trichloroethene (TCE), tetrachloroethene (PCE) and vinyl chloride which are present at
concentrations above their respective groundwater quality (2L)and Gross Contaminant Level
(GCL)standards in several monitoring wells.
The release was initially assigned a High Risk Classification with a ranking of H225D in a NORR
issued by NCDENR and dated July 21, 2009. The basis for the “High” risk classification was
presumably the presence of several water-supply wells within 1,000 feet of the source area.
Sampling of four water-supply wells located within 500 feet of the source area indicated no
detectable levels of contamination in three of the four wells sampled. Naphthalene and o-xylene
were detected in the sample collected from the fourth well, but the concentrations were below
2L Standards.Subsequent to sampling, the NCDENR performed a Health Risk Evaluation
(HRE) of the well located where naphthalene and o-xylene were detected. The NCDENR
confirmed that the concentrations of contaminants detected did not exceed the applicable water
quality standards. Therefore, no restrictions on the use of the well were recommended.
After consultation with NCDENR staff responsible for this site, the proposed remedies for soil
and groundwater contamination at the Site include Soil Vapor Extraction (SVE) and Air Sparging
(AS) with on-going groundwater quality monitoring.The goal of the proposed corrective action
is to restore the groundwater quality to concentrations that are equal to or less than the
standards established in 15A NCAC 2L .0202 and/or reducing the risk posed by the release to
EXECUTIVE SUMMARY
AMEC Environment and Infrastructure, Inc.
III
ultimately achieve site closure via a Notice of Residual Petroleum with appropriate land and
groundwater use restrictions under 15A NCAC 2L .0106(l).
TITLE PAGE
AMEC Environment and Infrastructure, Inc.III
TITLE PAGE
1.1 SITE INFORMATION
Date of Report:January 14, 2015
Facility ID:Unknown
UST Incident No.:36702
Site Risk:High
Site Rank:H225D
Land Use Classification:Industrial/Commercial
Site Name:Southern Pump and Tank Company
Site Address:4800 North Graham Street
City/Town:Charlotte
Zip Code:28269
County:Mecklenburg
Description of Geographical
Data Point:MW-1 (source area well)
Location Method:GPS
Latitude:35.278783 North
Longitude:-80.805486 West
1.2 CONTACT INFORMATION
Property Owner:D & B Finance Company LLCAddress:4823 North Graham Street
Charlotte, North Carolina 28269
UST Owner/Operator and Southern Pump and Tank Company, LLC
Property Occupant:4800 North Graham StreetAddress:Charlotte, North Carolina 28269
Consultant/Contractor:AMEC Environment & Infrastructure, Inc.
Address:2801 Yorkmont RoadCharlotte, North Carolina 28208
Analytical Laboratory:Pace Analytical Services, Inc.Address:9800 Kincey Avenue, Suite 100
Huntersville, North Carolina 28078
1.3 RELEASE INFORMATION
Date Discovered:October 2008
Estimated Quantity of Release:Unknown
Cause of Release:Unknown
Source of Release:Two Former UST Basins
TABLE OF CONTENTS
AMEC Environment and Infrastructure, Inc.V
Name Page No.
EXECUTIVE SUMMARY ...............................................................................................................I
TITLE PAGE ................................................................................................................................III
1.1 Site Information..............................................................................................................III
1.2 Contact Information........................................................................................................III1.3 Release Information.......................................................................................................III
1.0 Site History and Characterization .......................................................................................1
1.1 UST/AST Owner/Operator and Other Responsible Party Information .............................11.2 UST/AST System and Other Release Information...........................................................2
1.3 Release Information........................................................................................................2
1.4 Site Characteristics .........................................................................................................31.5 Owner/Occupant Information ..........................................................................................4
1.6 Receptor Information ......................................................................................................41.6.1 Water-Supply Wells .................................................................................................41.6.2 Public Water Supplies..............................................................................................5
1.6.3 Surface Water Bodies..............................................................................................6
1.6.4 Wellhead Protection Areas.......................................................................................61.6.5 Deep Aquifers in the Coastal Plain Region ..............................................................6
1.6.6 Subsurface Structures .............................................................................................61.6.7 Land Use .................................................................................................................61.6.8 Adjacent Property Owners .......................................................................................6
1.7 Previous Reports ............................................................................................................61.8 Initial Abatement and Corrective Actions.........................................................................7
2.0 Summary of site assessment information ...........................................................................8
2.1 Soil .................................................................................................................................82.2 Groundwater...................................................................................................................9
2.3 Surface Water...............................................................................................................10
2.4 Free Product.................................................................................................................102.5 Geology and Hydrogeology...........................................................................................10
2.5.1 Regional Setting ....................................................................................................10
2.5.2 Site Setting ............................................................................................................11
3.0 Objectives of Corrective Action.........................................................................................12
3.1 Notice of Regulatory Requirements ..............................................................................12
3.2 Purpose and Objectives of the CAP..............................................................................123.3 Cleanup Goals of the CAP............................................................................................12
4.0 COMPREHENSIVE EVALUATION OF REMEDIAL ACTIONS .........................................14
4.1 Soil Remediation...........................................................................................................144.1.1 In-situ Soil Blending ...............................................................................................15
4.1.2 Soil Excavation and Off-site Disposal ....................................................................174.1.3 Soil Vapor Extraction .............................................................................................19
4.2 Groundwater Remediation ............................................................................................21
4.2.1 In-situ Chemical Application...................................................................................214.2.2 Monitored Natural Attenuation ...............................................................................24
4.2.2.1 Plume Stabilization ...............................................................................................24
4.2.3 Air Sparging...........................................................................................................26
TABLE OF CONTENTS
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4.3 Risk Reduction..............................................................................................................28
5.0 PROPOSED REMEDIATION PLAN ......................................................................................30
5.1 SELECTED TECHNOLOGIES..........................................................................................30
5.1.1 Permitting Requirements ............................................................................................315.2 SENTINEL WELL INSTALLATION....................................................................................31
5.3 GROUNDWATER QUALITY MONITORING..................................................................325.4 Cost Estimate ...............................................................................................................335.5 Schedule.......................................................................................................................33
5.6 Public Notification/CAP Certification .............................................................................33
LIST OF TABLES
TABLE 1 –SUMMARY OF ADJACENT PROPERTY OWNER INFORMATION
TABLE 2 –SUMMARY OF WELL CONSTRUCTION AND GROUNDWATER ELEVATION DATATABLE3–SUMMARY OF WATER-SUPPLY WELL INFORMATION
TABLE 4 –SUMMARY OF LABORATORY ANALYSES –SOIL SAMPLES (OCTOBER 2008-DECEMBER 2011)TABLE 5 –SUMMARY OF LABORATORY ANALYSES –GROUNDWATER SAMPLES (FEBRUARY 2009 –JUNE 2014)
TABLE 6 –SUMMARY OF SLUG TEST DATATABLE7–SUMMARY OF NATURAL ATTENUATION PARAMETERS FOR GROUNDWATER (DECEMBER
2011)
LIST OF FIGURES
FIGURE 1 –SITE LOCATION MAP
FIGURE 2 –SITE MAP
FIGURE 3 –GROUNDWATER CONTOUR MAPFIGURE4–LAND USE AND RECEPTOR MAP
FIGURE 5 –SOIL QUALITY MAPFIGURE6–GROUNDWATER QUALITY MAPFIGURE7–BENZENE ISOCONCENTRATION MAP
FIGURE 8 –TETRACHLOROETHENE ISOCONCENTRATION MAPFIGURE9–TRICHLOROETHENE ISOCONCENTRATION MAP
FIGURE 10 –CIS-1,2-DICHLOROETHANE ISOCONCENTRATION MAP
FIGURE 11 –1,2-DICHLOROETHANE ISOCONCENTRATION MAPFIGURE12–ETHYLBENZENE ISOCONCENTRATION MAP
FIGURE 13 –PROPOSED REMEDIAL SYSTEM LAYOUT
FIGURE 14 –TYPICAL AIR SPARGE WELL DETAIL
LIST OF APPENDICES
APPENDIX A –REGULATORY CORRESPONDENCE
APPENDIX B –LABORATORY REPORT OF ANALYSES –SOIL SAMPLES (DECEMBER 2011)
APPENDIX C –LABORATORY REPORT OF ANALYSES –GROUNDWATER SAMPLES (JUNE 2014)
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1.0 SITE HISTORY AND CHARACTERIZATION
1.1 UST/AST OWNER/OPERATOR AND OTHER RESPONSIBLE PARTY INFORMATION
UST ID Number Unknown Facility ID Number Unknown
Name of Owner Dates of Operation(mm/dd/yy to mm/dd/yy)
Southern Pump and Tank Company 1962 to Present
Street Address
4800 North Graham Street
City State Zip Telephone Number
Charlotte NC 28269 [phone]
Name of Operator Dates of Operation(mm/dd/yy to mm/dd/yy)
Southern Pump and Tank Company 1962 to Present
Street Address
4800 North Graham Street
City State Zip Telephone Number
Charlotte NC 28269 [phone]
Incident Number 36702
Name of Other Responsible Party Dates of Release(s)(mm/dd/yy to mm/dd/yy)
None Unknown
Street Address
City State Zip Telephone Number
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1.2 UST/AST SYSTEM AND OTHER RELEASE INFORMATION
1.3 RELEASE INFORMATION
In November 1997, AMEC (then LAW)completed a Phase I Environmental Site Assessment
Report (dated November 26, 1997). According to this report, the former UST basin, floor drains
and on-site septic tank drain field, two on-site concrete-lined waste pits, storage of used
petroleum dispensers, truck repair pit, former varsol AST piping and an unknown concrete patch
area and vent pipe were noted as recognized environmental concerns.
UST IDNumber
Current/LastContents
PreviousContents Capacity(gallons)ConstructionDetails
TankDimensions(feet)
DescriptionofAssociatedPiping andPumps
DateTankInstalled
Status ofUST
WasReleaseAssociatedWith USTSystem?
1U Petroleum Unknown 560 Steel Unknown Unknown Unknown RemovedPrior to
1988
Yes
2U WashWater Unknown Unknown Steel Unknown Unknown Unknown RemovedPrior to1988 Yes
3U Petroleum Unknown 550 Steel Unknown Unknown Unknown
Removed
Prior to1988 Yes
4U Petroleum Unknown 550 Steel Unknown Unknown Unknown RemovedPrior to
1988
Yes
5U Diesel Unknown 10,000 Steel Unknown Unknown Unknown RemovedPrior to1988 Yes
6U Diesel Unknown 5,000 Steel Unknown Unknown Unknown RemovedPrior to
1988
Yes
7U Gasoline Unknown 20,000 Steel Unknown Unknown Unknown RemovedPrior to1988 Yes
8U Unknown Unknown 550 Steel Unknown Unknown Unknown
Removed
Prior to1988 Yes
9U Unknown Unknown 550 Steel Unknown Unknown Unknown RemovedPrior to
1988
Yes
10 Unknown Unknown Unknown Unknown Unknown Unknown Unknown
RemovedPrior to1988 Yes
11 Used Oil
AST Unknown Unknown Unknown Unknown Unknown Unknown Unknown Yes
12 VarsolAST Unknown 150 steel 3 x 4.5
APP flex
double wallpipe with
std. suctionpump
1995 2011 Yes
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AMEC Environment and Infrastructure, Inc.3
In September 2008, AMEC (then MACTEC) evaluated Site conditions including the
presence/status of previously identified environmental concerns, location of underground utilities
and the potential need for additional sampling. During the Site visit, AMEC personnel identified
the former UST basin on the western portion of the property (former Western UST Basin), but
could not identify specific tank locations within the basin. Additionally, AMEC observed one
AST used to store waste oil. AMEC also observed a parts washing station along the northern
interior wall of the building where dispenser parts were cleaned with varsol. The used varsol
was carried via a floor drain system to a vaulted AST outside the northern wall of the building.
Representatives of SPATCO confirmed that two USTs were formerly located in this area (former
Northern UST Basin).
In October 2008,AMEC conducted limited soil assessment activities within the former Western
UST Basin, the former Northern UST Basin, and adjacent to a floor pit inside the building.
Evidence of a release was confirmed by concentrations of Total Petroleum Hydrocarbons
(TPH), Diesel Range Organics (DRO) and Gasoline Range Organics (GRO) that exceeded the
NCDENR regulatory threshold of 10 mg/kg in soil samples collected within the former Northern
UST Basin. Additionally, concentrations of one or more volatile organic compounds (VOCs) and
semi-volatile organic compounds (SVOCs) that exceeded the NCDENR Soil-to-Water Maximum
Soil Contaminant Concentrations (MSCCs)were reported in soil samples collected from the
former Western UST Basin.
1.4 SITE CHARACTERISTICS
The Site was initially developed as SPATCO’s corporate headquarters in 1963 and continues to
be used as such.SPATCO stores petroleum dispensing equipment and containers used to
clean the equipment on-site. The Site is in a mixed-use commercial/industrial and residential
area of Charlotte, North Carolina.A summary of adjacent property owner information is
included in Table 1.
Based on soils logged during well installation at the Site, subsurface soils consist of sandy and
clayey silt to an approximate depth of 35 feet below ground surface (bgs). Saprolite was
encountered from approximately 35 feet to 97 feet bgs and was underlain by competent bedrock
to 105 feet bgs, the maximum depth of penetration at the Site.
Recent groundwater measurement data (June 10, 2014) found the depth to water in the
monitoring wells ranged from 9.30 feet below top of well casing (BTOC) in well MW-4 to 14.60
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feet BTOC in well MW-12. Groundwater elevations on the same date ranged from 766.10 feet
above mean sea level (feet MSL) in well MW-4 to 758.03 feet MSL in well MW-7. Based on
these data, groundwater flow was generally toward the southeast. A summary of groundwater
elevation data obtained on June 10, 2014 is included on Table 2.A Groundwater Contour Map
based on the June 2014 data is included as Figure 3.
1.5 OWNER/OCCUPANT INFORMATION
The Site is comprised of two parcels, identified as Parcels #04506301 and #04506209 in the
Charlotte-Mecklenburg Property Ownership and Land Records Information System (POLARIS).
Property ownership and occupant information for the two parcels is presented in the following
table.
Tax Parcel
Number/Map ID Owner/Address Occupant/Address Land Use
04506301
D&B Finance Company LLC
4823 N. Graham Street
Charlotte, NC 28269
SPATCO
4800 North Graham St.
Charlotte, NC 28269
Industrial
04506209
D&B Finance Company LLC
4823 N. Graham Street
Charlotte, NC 28269
SPATCO
4800 North Graham St.
Charlotte, NC 28269
Industrial
1.6 RECEPTOR INFORMATION
AMEC (as MACTEC)completed a receptor survey in the vicinity of the Site as part of the CSA
in May 2010. The locations of potential receptors identified during the receptor survey are
shown on Figure 4 and discussed in the sections that follow.
1.6.1 Water-Supply Wells
AMEC personnel conducted a potable well search by walking through the surrounding
neighborhood within 500 feet of the source area, and performing a driving reconnaissance of
streets and properties within 1,500 feet of the source area. AMEC identified 19 properties within
a 1,500-foot radius of the source area served by water-supply wells. Of these 19 properties,
four are located within a 500-foot radius of the source area (Figure 3).Based on information
received from the well owners, these four wells are used for drinking water purposes.Based on
AMEC’s groundwater elevation data,two of the water-supply wells are situated hydraulically
upgradient from the contaminant source area with the nearest two wells situated cross-gradient
from the source area.No water-supply wells were identified hydraulically downgradient from the
contaminant source area.A summary of property ownership information and water-supply well
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information, where applicable, is provided on Table 3.The remaining surrounding properties
are connected to municipal water.
Pursuant to the requirements of the Notice of Violation (NOV) issued by the NCDENR on July
22, 2010, AMEC collected water samples from the four private water-supply wells located within
500 feet of the source area(s) between January 6 and 18, 2011.The results of analyses
indicated the presence of naphthalene and o-xylene in the water sample collected from the well
at 4801 Wild Rose Lane. However, the concentrations did not exceed the 2L Standards.It
should be noted that a gasoline-powered lawnmower was stored inside the well house at the
time of sampling.The results of laboratory analyses were documented in a Report of Water
Supply Well Sampling prepared by AMEC and submitted to NCDENR on March 18, 2011.
Subsequently,NCDENR performed a Health Risk Evaluation (HRE) of the well located at 4801
Wild Rose Lane. The NCDENR concluded that none of the contaminants detected exceeded
applicable water quality standards and,therefore, no restrictions on the use of the well were
recommended.
On June 12, 2014, AMEC collected water samples from one private water-supply well (1823
Cannon Avenue)located within 500 feet of the source area(s).AMEC did not collect water
samples from the remaining three water-supply wells in the site vicinity (4800, 4801 and 4819
Wild Rose Lane) during this event because the property occupants were not home on the date
that we visited the residences.The sample from the 1823 Cannon Avenue water-supply well
was analyzed for VOCs via SM 6200B. The results of the laboratory analysis did not identify
VOC concentrations above the laboratory reporting limits.
Based on these laboratory data, the results of the HRE, and the length of time that has elapsed
since the USTs were removed prior to 1988, the release does not currently represent a risk to
private water-supply well users in the vicinity of the site.
1.6.2 Public Water Supplies
AMEC observed water-meter vaults along the streets and sidewalks while walking within 500
feet of the source area. AMEC mailed water-supply well information surveys to surrounding
property owners within a 500-foot radius of the source area. While there is no restriction on use
of water wells in the city, public water is available to the majority of the residents and
businesses within 1,500 feet of the contaminant source areas.AMEC confirmed with Charlotte-
Mecklenburg Utilities that a municipal water line is present along Cannon Avenue. However, no
municipal water lines are present along Wild Rose Lane.Completed well survey questionnaires
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that were distributed during the LSA and returned to AMEC were previously included in the LSA
Report.
1.6.3 Surface Water Bodies
An unnamed tributary of Little Sugar Creek is located approximately 2,000 feet southeast of the
Site.
1.6.4 Wellhead Protection Areas
The Site is not located in a designated wellhead protection area.
1.6.5 Deep Aquifers in the Coastal Plain Region
The Site is not located in the Atlantic Coastal Plain Physiographic Province of North Carolina.
1.6.6 Subsurface Structures
Basements were not observed at the Site, and were not confirmed at adjacent buildings.
Underground utilities include natural gas, sanitary sewer, storm drains, water lines, and
communication lines.
1.6.7 Land Use
Land use within a 1,500-foot radius of the Site is classified primarily as industrial/commercial
and residential. The zoning for the Site and surrounding properties is included as Figure 4.
The Site is occupied by SPATCO and used to store petroleum dispensers and other petroleum
related dispensing equipment. Containers used to clean the equipment are also stored on-site.
1.6.8 Adjacent Property Owners
Ownership information for properties contiguous to the Site is listed in Table 1.
1.7 PREVIOUS REPORTS
Previous reports summarizing assessment activities on-site include:
Phase I Environmental Site Assessment,prepared by AMEC (then LAW) (1997);the
former UST basin, floor drains and on-site septic tank drain field, two on-site concrete-lined waste pits, storage of used petroleum dispensers, truck repair pit, former varsol
AST piping and an unknown concrete patch area and vent pipe were noted as
recognized environmental concerns.
Report of Limited Site Assessment (LSA), prepared by AMEC (then MACTEC) (2009),
summarizes the results of the Phase I and Phase II Limited Site Assessment activities;submitted to NCDENR on March 18, 2009.
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Comprehensive Site Assessment (CSA)Report, prepared by AMEC (then MACTEC)
(2010), summarizes the results of soil and groundwater assessment activities conducted in
January 2010; submitted to NCDENR on May 26, 2010.
Revised Report of Water Supply Well Sampling,prepared by AMEC (then MACTEC)
(2011),summarizes the results of water supply well sampling activities conducted inJanuary 2011; submitted to NCDENR on March 28, 2011.
Addendum to the Comprehensive Site Assessment Report, prepared by AMEC (thenMACTEC) (2011), summarizes the results of vertical and horizontal delineation as well as
the collection of water samples from private water supply wells; submitted to NCDENR on
June 2, 2011.
Corrective Action Plan (CAP), prepared by AMEC (then MACTEC), summarizes site
assessment activities conducted between October 2008 and August 2013, and evaluatesremedial options for the site; submitted to NCDENR on June 18, 2012 and revised on
November 9, 2012 and August 29, 2013.
1.8 INITIAL ABATEMENT AND CORRECTIVE ACTIONS
Initial abatement and corrective actions have not been performed at the Site.
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2.0 SUMMARY OF SITE ASSESSMENT INFORMATION
2.1 SOIL
Soil quality data were obtained during four separate sampling events conducted between
October 2008 and December 2011. The soil assessment activities focused on two areas of the
Site: the former Northern UST basin and the former Western UST basin. A total of 22 soil
samples were collected from 11 soil borings advanced in the vicinity of the former Northern UST
Basin, while 18 soil samples were collected from nine borings within the former Western UST
Basin and former dispenser island. Laboratory analyses were performed on soil samples in
accordance with NCDENR’s Guidelines for Assessment and Corrective Action for UST
Releases (Guidelines)and varied depending on the phase of work and materials formerly
contained in the USTs in each area. In general, soil samples were analyzed for Total Petroleum
Hydrocarbons (TPH), Diesel Range Organics (DRO) and Gasoline Range Organics (GRO),
volatile organic compounds (VOCs), semi-volatile organic compounds (SVOCs) and metals.
Constituents detected in soil at concentrations exceeding the Soil-to-Water MSCCs and target
cleanup concentrations (both in milligrams per kilogram (mg/kg))are listed in the table below.
Compound Phase of Work /Date Sample ID /Depth(ft bgs)
MaximumConcentration(mg/kg)
Soil-to-Water MSCC orState Action Level(mg/kg)
TPH-DRO Initial Assessment T-1 (14-15)12,400 10
TPH-GRO LSA GP-1 (13-15)1,670 10
C5-C8 Aliphatic CSA GP-8 (15)289 68
C9-C18 Aliphatics LSA MW-1 (5)4,232.10 3,300
C9-C22 Aromatics LSA MW-1 (5)1,770 34
Benzene CSA GP-8 (15)8.76 0.0056
1,2-Dichlorobenzene CSA GP-8 (15)0.746 0.23
cis-1,2-Dichloroethene LSA MW-1 (15)32.4 0.35
Ethylbenzene LSA MW-1 (15)7.74 4.6
Isopropylbenzene LSA MW-1 (15)1.93 1.7
Methylene chloride LSA MW-2 (15)0.172 0.02
MTBE Pre-CAP SB-7 (7)0.808 0.091
Naphthalene LSA MW-1 (15)25.5 0.58
n-Propylbenzene CSA GP-8 (15)4.56 1.7
1,3,5-Trimethylbenzene LSA MW-1 (15)15.3 7.3
1,2,4-Trimethylbenzene LSA MW-1 (15)41.3 7.5
1,1,2,2-Trichloroethane LSA MW-1 (15)2.44 0.001
Tetrachloroethene (PCE)CSA GP-8 (15)19.1 0.0074
Toluene Initial Assessment FP-2 (3-4)22.6 4.3
Trichloroethene (TCE)CSA GP-8 (15)1.41 0.019
Vinyl chloride LSA MW-2 (15)0.323 0.000094
Xylenes Initial Assessment FP-2 (3-4)32.4 5
Note: Bold-face concentrations exceeded the Soil-to-Water MSCCs; shaded concentration exceeded the
Industrial/Commercial MSCC.
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A summary of laboratory analyses of soil samples collected between October 2008 and
December 2011 is presented in Table 4. Soil sample locations are shown on Figure 5. A copy
of the laboratory report for soil samples collected during Pre-CAP activities in December 2011 is
included in Appendix B.Please refer to the LSA, CSA and Addendum to CSA Reports for
copies of laboratory reports for soil samples collected during prior phases of work at the Site.
2.2 GROUNDWATER
Groundwater quality data were obtained from sampling of monitoring wells installed and/or
sampled during LSA (2009), CSA (2010),and CSA Addendum (June 2011)activities at the Site.
In December 2011, AMEC gauged, developed and sampled a total of 18 Type II monitoring
wells and two Type III monitoring wells as part of a Pre-CAP monitoring program.These wells
were resampled, pursuant to the requirements of the August 31, 2012 NOV, between October
15 and 17, 2012.Subsequent annual Pre-CAP monitoring events were performed by AMEC in
August 2013 and June 2014.
Based on the data obtained,petroleum-related and chlorinated VOCs are present in on-and off-
site monitoring wells at concentrations that exceed the 2L Standards.Constituents detected in
groundwater at concentrations exceeding the 2L standards are listed in the table below.
Maximum constituent concentrations in groundwater, based on the groundwater quality data
obtained during the Pre-CAP sampling event in October 2012, and target cleanup
concentrations (both in micrograms per liter (g/L)) are summarized as follows:
Compound Sample ID
Maximum
Concentration
(g/l)
NC 2L
Groundwater
Standard (g/l)
1,1-Dicholorethane MW-2 17.7 6
1,2-Dichloroethane MW-3 625 0.4
1,2-Dichloropropane MW-3 47.5 0.6
Benzene MW-3 10,500 1
Diisopropyl ether MW-3 102 70
MTBE MW-2 583 20
Methylene chloride MW-1 66.7 5
Naphthalene MW-1 408 6
Tetrachloroethene (PCE)MW-1 977 0.7
Trichloroethene (TCE)MW-1 444 3
Vinyl chloride MW-1 5.6 0.03
cis-1,2-Dichloroethene MW-1 42,800 70
Notes:1.Bold-face concentrations exceeded the 2L Standards; shaded concentrations exceeded the GCL.
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Based on this groundwater quality data, the highest concentrations of impacted groundwater are
generally found either adjacent to (MW-3)and down-gradient (MW-1)of the former dispenser
island/former Western UST Basin or in the vicinity of the former Northern UST Basin (MW-2).In
general, concentrations of site-specific contaminants of concern in source area wells MW-1,
MW-2 and MW-3 have remained about the same between the December 2011 and June 2014
groundwater sampling events, with the exception of the chlorinated solvents concentrations
which have decreased during the time monitored. The increased concentration of cis-1,2-
dichloroethene in the groundwater sample collected from well MW-1 suggests degradation of
the chlorinated solvent portion of the groundwater contaminant plume in this area.
The groundwater contaminant plume is horizontally delineated, to the extent possible based on
off-site access obtained, and extends south onto the Plastics-Plus property. SPATCO was
denied access to the adjacent property south of wells MW-7 and MW-11 for the purpose of
plume delineation in that direction. The vertical extent of groundwater contamination is
delineated by well DMW-2 (screened from 100’-105’ bgs).Well construction data is presented
in Table 2.Groundwater quality data obtained during the December 2011 Pre-CAP monitoring
event are shown adjacent to the respective monitoring well locations on Figure 6 and are
summarized in Table 5. Copies of the laboratory reports for groundwater samples analyzed
during the June 2014 Pre-CAP monitoring event are included in Appendix C.
2.3 SURFACE WATER
The nearest surface water body is an unnamed tributary of Little Sugar Creek, located
approximately 2,000 feet southeast of the source area.Based on this location, surface water
sampling was not conducted as part of this assessment.
2.4 FREE PRODUCT
Light non-aqueous phase liquid (LNAPL) was present in well MW-12 (0.34 feet thick) at the time
of the June 2014 sampling event. LNAPL was previously detected in this well in 2012.
2.5 GEOLOGY AND HYDROGEOLOGY
2.5.1 Regional Setting
The Site is located within the Charlotte Belt of the Piedmont Physiographic Province consisting
of low rounded hills and long rolling northeast to southwest trending ridges with incised creek
channels. Based on a review of the Geologic Map of North Carolina dated 1985, the Site is
underlain by metamorphosed quartz diorite.
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The Soil Survey of Mecklenburg County indicates that soils at the Site are classified as Urban
Land. The natural characteristics of these soils have been altered or destroyed by construction
activities.Since no geologic features were identified on or near the Site, it is reasonable to
assume that the direction of near-surface groundwater flow under static conditions (no pumping
interference) approximates the surface topography of the Site. Surface and subsurface drainage
patterns within the Piedmont typically indicate the direction contaminants would be transported by
surface water or groundwater. The direction and movement of groundwater through soil is
dependent on soil type and the presence of relict structures and textures of the underlying rock.
Fractures, faults, folds and foliation planes affect the migration of groundwater in rock.
2.5.2 Site Setting
Based on data obtained during subsurface investigations to date, the Site is underlain at
relatively shallow depths by undifferentiated, saprolitic silts and clays. Competent rock was
encountered during installation of the second Type III monitoring well (DMW-2) at a depth of 97
feet bgs immediately down-gradient of the source area.
Based on data obtained during the recent Pre-CAP groundwater sampling event, the depths to
groundwater measured in June 2014 ranged from 9.30 feet BTOC in monitoring well MW-4 to
14.60 feet BTOC in monitoring well MW-12, after a correction for the presence of 0.34 feet of
LNAPL was applied. Based on these data, groundwater flow direction was toward the
southeast.The hydraulic gradient measured parallel to the direction of groundwater flow
between the most up-gradient well (MW-4) and the most down-gradient well (MW-7) was 0.014
feet per foot. A Groundwater Contour Map, based on data obtained in June 2014, has been
included as Figure 3. A summary of well construction details and groundwater elevation data is
presented in Table 2.
Rising head slug tests were conducted using monitoring wells MW-1, MW-6 and MW-10 on
January 22, 2010. Hydraulic conductivities in the Type II monitoring wells, calculated using the
Bouwer and Rice method, ranged from 6.81 x 10-4 to 9.45 x 10-4 feet per minute (0.98 to 1.36
feet per day).Seepage velocities, calculated using the equation V = K (dh/dl)/n e,ranged from
0.09 to 0.12 feet per day (31.12 to 43.19 feet per year), using an assumed effective porosity of
0.23.A summary of the results of slug test analyses is presented in Table 6. Please refer to
the CSA Report (May 2010) for slug test raw data and calculations.
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3.0 OBJECTIVES OF CORRECTIVE ACTION
The principal intent of this document is to propose a corrective measure(s)that comply with the
requirements of applicable laws and regulations.
3.1 NOTICE OF REGULATORY REQUIREMENTS
On July 29, 2011, NCDENR issued a NORR requiring that a CAP Report be submitted to
remediate environmental contamination at the Site. A copy of the NORR has been included in
Appendix A.
3.2 PURPOSE AND OBJECTIVES OF THE CAP
The objective of the CAP is to propose, evaluate and select an effective remedial action(s) to
remediate VOC-impacted soil and groundwater beneath the Site to concentrations that comply
with requirements of applicable laws and regulations.This CAP also proposes an estimated
budget and schedule for implementation of the proposed remedy, as well as providing on-going
groundwater monitoring to evaluate the effectiveness of the selected remedy.
3.3 CLEANUP GOALS OF THE CAP
For the purpose of this CAP and in light of the current classification of the site as “high risk”
under the Underground Storage Tank Section’s Guidelines for Assessment and Corrective
Action, AMEC currently proposes to remediate groundwater to levels at or below the standards
set forth in 15A NCAC 2L .0202 (2L Standards) subject to the applicable provisions of 15A
NCAC 2L .0106 which allow for termination of corrective action in certain situations without
remediation of the groundwater to those standards. If the classification of the site is changed to
“low risk”, groundwater will be remediated to the UST Section’s risk-based standards, whereby
remediation may also include the filing of an approved Notice of Residual Petroleum (NRP).
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The 2L Standards for the primary VOCs in groundwater at the Site are presented in the
following table:
VOC Compound 2L Standard
(ug/L)
1,1-Dicholorethane 6
1,2-Dichloroethane 0.4
1,2-Dichloropropane 0.6
Benzene 1
MTBE 20
Methylene chloride 5
Naphthalene 6
Tetrachloroethene (PCE)0.7
Trichloroethene (TCE)3
Vinyl chloride 0.03
cis-1,2-Dichloroethene 70
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4.0 COMPREHENSIVE EVALUATION OF REMEDIAL ACTIONS
Both active in-situ and ex-situ treatments for affected soil and groundwater were considered in
preparation of this CAP.
The bulk of VOC-impacted soil is concentrated in the vicinity of the former dispenser island
associated with the former Western UST Basin.In the majority of soil borings advanced in this
area, soil contamination extended vertically to the water table. As such, these soils likely
represent a continuing source of groundwater contamination. Active remediation of affected
soils in this area is proposed in this CAP.
The bulk of VOC-impacted groundwater is and has historically been concentrated in and around
wells MW-1, MW-2,MW-3 and MW-6.Remedial options are focused on active treatment of this
area with on-going groundwater quality monitoring.
A key component of this remedial evaluation is that after some period of active remediation,
conditions will exist that will allow the risk classification of the site to be lowered allowing for the
use of land and groundwater use restrictions and institutional controls in the form of a NRP
along with the application of Gross Contaminant Levels (GCLs)as the applicable cleanup
criteria.
4.1 SOIL REMEDIATION
Soil quality assessments conducted at the Site between October 2008 and December 2011
have identified affected soils in the vicinity of the former Western UST Basin and the associated
dispenser island. A total of 22 soil samples were collected from 14 soil borings in this area.
Concentrations of target analytes that exceeded the Soil-to-Water MSCCs and extended
vertically downward to the water table were present in each soil boring. Based on these data,
the estimated extent of contaminated soil that exceeded the Soil-to-Water MSCCs is
approximately 40’ x 50’x 15’. Several remedial technologies are available to address the extent
and level of soil contamination present on-site.The following three alternatives were evaluated
for the Site:
In-situ Soil Blending
Soil Excavation and Off-site Disposal
Soil Vapor Extraction
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Soil remedial options are discussed in the following sections of the CAP Report.
4.1.1 In-situ Soil Blending
The process of in-situ soil blending involves using mechanical equipment to effectively distribute
chemical amendments throughout a given treatment zone to chemically treat contaminants of
concern.Potential chemical amendments include oxidants, reductants, bio-stimulants,and soil
stabilizers. The mixing apparatus typically consists of a rotary in-situ blender mounted on a
large excavator capable of mixing dry soil as well as sludge material to depths of up to 20 feet
bgs.
Since many chemical remediation alternatives require direct contact with the target
contaminants, the effectiveness of this remediation strategy is often limited by the ability to
distribute the chemical amendments throughout the soil medium.In-situ blending can acheive
production rates comparable to conventional excavation, and is generally a cheaper alternative
than excavation and off-site disposal of affected soils.
For a treatment area the size of that proposed in the vicinity of the former Western UST Basin
(40’ x 50’ x 15’), the in-situ blending process would be performed systematically by subdividing
the treatment area into smaller cells.The cell dimensions and chemical loading requirements
would be determined prior to mobilization.Each cell would be further subdivided into 5-foot
vertical lifts.Each lift would be mixed separately with predetermined quantities of chemical
amendments.Then the entire soil column would be mixed ensuring that proper vertical
distribution is achieved.
For the purpose of this CAP, AMEC evaluated in-situ soil blending by introducing reactive
chemical oxidants into soil (In-situ Chemical Oxidation (ISCO)) to rapidly reduce contaminant
concentrations from the surface to approximately 20 feet bgs.Based on the concentrations and
distribution of contaminants in this area, AMEC estimated blending approximately 44,000 pounds
of sodium persulfate into the treatment zone over an estimated six-day period.
The evaluation of this remedial technology using the criteria specified in the Guidelines is
presented below.
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Criteria Evaluation
A.Nature of Contamination Contaminants of concern in this area include petroleum-
related VOCs (benzene, toluene, ethylbenzene, xylenes,naphthalene, cis-1,2-dichloroethene) and chlorinated VOCs
(tetrachloroethene,trichloroethene,1-2-dichloroethane).
The horizontal extent of VOC-impacted soil in the vicinity of
the former Western UST Basin is estimated to be 40’ x 50’.
The vertical extent of VOC-impacted soil in this area extendsfrom near surface soils (six inches bgs) to the seasonal high
water table (15 feet bgs).
Free product has not been observed in soil borings ormonitoring wells.
B.Description of Remedial
Technology In-situ soil blending would be utilized to chemically treat soil
and shallow groundwater using an in-situ blender mountedon a conventional track excavator.
The proposed treatment zone measures approximately 40’ x
50’ x 15’and would be divided into smaller cells. Each cellwould be further divided into 5-foot vertical lifts to achieve
mixing goals.
Though the technology has previously been approved forremedial applications in North Carolina, it is considered an
Innovative Technology and will be subject to approval by theNCDENR Innovative Technology Committee prior to use at
the Site.
An Underground Injection Control (UIC) permit will be
required to implement the technology.
Injectate would be expected to either chemically react withimpactedsoil and groundwater and/or enhance naturally
occurring bioremediation for a period that lasts up to 30days.
C.Feasibility and effectiveness Feasibility of in-situ soil blending is good, as this remedy canbe applied in stages, thereby enabling continued use of the
Site with minimal disruption to workers at and visitors to theSite.
The estimated life cycle of the proposed chemicalamendments is 30 days; as an in-situ technology, it is not a
permanent remedial alternative. Rather, its intendedpurpose at the Site would be to actively treat impacted soil
and groundwater, then passively improve subsurfaceconditions so that natural attenuation of contaminants can
continue.
D.Remedial System Operation andMaintenance O&M is not required for this remedy, as no permanent
structures/systems would be installed at the Site.
E.Waste Treatment/Disposal Plan Waste products are not generated during in-situ soil
blending.
F.Schedule In-situ soil blending, as proposed, should take 6 days to
complete.
G.Cost The estimated cost for in-situ soil blending is $165,000.
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This remedial technology is not proposed for the Site since chemical application is considered an
Innovative Technology and would be subject to approval by the NCDENR Innovative
Technology Committee prior to implementation.Furthermore, NCDENR has indicated that they
would not approve injection as a remedial method for the Site given the presence of water-
supply wells within 500 feet of the source area.
4.1.2 Soil Excavation and Off-site Disposal
Based on soil quality data obtained from the former Western UST Basin and associated
dispenser island, AMEC considers soils in this area to be a continuing source of contamination
to groundwater.The estimated limits of excavation are 40’ x 50’ x 15’. Soil removal could be
accomplished via use of a track excavator capable of reaching depths of 15 feet without
benching into the proposed excavation. Excavated soils would likely require post-excavation
waste characterization prior to transport to a permitted disposal facility for treatment and/or
disposal.The sequence of events relative to soil excavation would likely include placement of
the soil in roll-off containers to allow for toxicity characterization. Due to the presence of
chlorinated solvents in the soil, there is potential for the leachable solvent concentrations to
exceed the applicable regulatory level for PCE. If this were the case, the excavated soil may
require treatment/disposal at a permitted hazardous waste facility. Such disposal is prohibitively
expensive and would not be reimbursable by the State Trust Fund.
The evaluation of this remedial technology using the criteria specified in the Guidelines is
presented below.
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Criteria Evaluation
A.Nature of Contamination Contaminants of concern in this area include petroleum-
related VOCs (benzene, toluene, ethylbenzene, xylenes,naphthalene, cis-1,2-dichloroethene) and chlorinated VOCs
(tetrachloroethene,trichloroethene,1-2-dichloroethane).
The horizontal extent of VOC-affected soil in the vicinity of
the former Western UST Basin is estimated to be 40’ x 50’.
The vertical extent of VOC-affected soil in this area extendsfrom near surface soils (six inches bgs) to the seasonal high
water table (15 feet bgs).
Free product has not been observed in soil borings ormonitoring wells.
B.Description of Remedial
Technology Impacted soil would be removed in the vicinity of the former
Western UST Basin and dispenser island using a trackexcavator.
Excavated soils would likely require post-excavation waste
characterization prior to transport to a permitted disposalfacility for treatment and/or disposal. The sequence of
events relative to soil excavation would likely includeplacement of the soil in roll-off containers to allow for toxicity
characterization.Subsequent to review of post-excavationsoil sample lab data, the excavation will be backfilled with
clean fill.
C.Feasibility and effectiveness Feasibility of soil excavation at the Site is good. The
excavation may be completed in stages so as to allowcontinued use of the Site with minimal disruption to daily
activities.
Effectiveness of soil excavation is high since it will
permanently remove affected soil from the Site.
D.Remedial System Operation andMaintenance O&M is not required for this remedy, as no permanent
structures/systems would be installed at the Site.
E.Waste Treatment/Disposal Plan Affected soil could be transported as non-hazardous waste(contingent upon favorable toxicity characterization results)
to an off-site facility permitted to accept soil impacted by aUST release.
F.Schedule Given the size of the proposed excavation area, excavationactivities are estimated to take 15 days to complete.
G.Cost The estimated cost for soil removal and disposal is
$152,000, assuming non-hazardous disposal.
On behalf of D & B Finance Company, LLC, AMEC prepared a Trust Fund Pre-approval Task
Authorization (TA)for soil excavation and disposal and submitted the TA to NCDENR for
approval.NCDENR denied approval of the funding for this remedial technology.
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4.1.3 Soil Vapor Extraction
Soil vapor extraction (SVE)is an in-situ remedial technology that reduces concentrations of
volatile constituents in petroleum products adsorbed to soils in the unsaturated zone. In this
technology, a vacuum is applied through wells near the source of contamination in the soil.
Volatile constituents of the contaminant mass "evaporate" and the vapors are drawn toward the
extraction wells.Extracted vapor is then treated if legally required (commonly with carbon
adsorption) before being released to the atmosphere.The increased air flow through the
subsurface can also stimulate biodegradation of some of the contaminants, especially those that
are less volatile.
Soil vapor extraction is a technology that is based on the theory of gas movement in porous
media, and may be utilized for the removal of VOCs from a soil matrix. VOC vapors within the
soils will approach equilibrium with surrounding pressures according to Henry’s Law. Soil vapors
tend to migrate in the direction of least pressure. Therefore, the creation of a negative pressure
gradient (i.e. vacuum) in the soil through vapor extraction will induce migration of the subsurface
vapors toward extraction points at depths corresponding to the vadose zone.
The primary constraint on the effectiveness of SVE at the Site is the permeability of subsurface
soils.The permeability of the soil affects the rate of air and vapor movement through the soil; the
higher the permeability of the soil, the faster the movement and (ideally) the greater the amount of
vapors that can be extracted.Prior to installation of a SVE system, a pilot test may be required to
evaluate soil permeability as it pertains to the effectiveness of SVE at the Site.The evaluation of
this remedial technology using the criteria specified in the Guidelines is presented below.
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Criteria Evaluation
A.Nature of Contamination Contaminants of concern in this area include petroleum-
related VOCs (benzene, toluene, ethylbenzene, xylenes,naphthalene, cis-1,2-dichloroethene) and chlorinated VOCs
(tetrachloroethene,trichloroethene,1-2-dichloroethane).
The horizontal extent of VOC-impacted soil in the vicinity of
the former Western UST Basin is estimated to be 40’ x 50’.
The vertical extent of VOC-impacted soil in this area extendsfrom near surface soils (six inches bgs) to the seasonal high
water table (15 feet bgs).
B.Description of Remedial
Technology SVE would be utilized to enhance volatilization andextraction of the contaminants in the soil in the vicinity of the
former Western UST Basin and the dispenser island.
Extracted vapor is treated if legally required (commonly with
carbon adsorption) before being released to the atmosphere.
The increased air flow through the subsurface can alsostimulate biodegradation of some of the contaminants,
especially those that are less volatile.
C.Feasibility and effectiveness Feasibility of SVE at the Site is subject to limitation of
minimizing impacts of a permanent system on on-goingoperations at the Site.
Effectiveness of SVE would be evaluated during a short-term (1 to 30 days) pilot test utilizing existing monitoring well
MW-3 as the extraction well, if approved by NCDENR.
SVE paired with air sparging is typically a highly effectiveapproach to reducing concentrations of the VOCs.
D.Remedial System Operation and
Maintenance Weekly O&M would be required to maintain the vacuum andblower equipment.
E.Waste Treatment/Disposal Plan Waste products are not generated during SVE.
F.Schedule Given the size of the proposed treatment area, SVE pilottesting could be performed in 1 day.Installation of a SVE
system typically takes 2-3 weeks to complete.
G.Cost The estimated cost for SVE is $90,000.
This remedial technology is proposed for the Site because SVE is a cost-effective and reliable
technology for removing VOCs from a soil matrix.
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4.2 GROUNDWATER REMEDIATION
Between February 2009 and April 2011, AMEC installed a total of 18 Type II and two Type III
groundwater monitoring wells on-and off-site to evaluate the horizontal and vertical extent of
VOC-impacted groundwater. Based on analytical results obtained during the recent Pre-CAP
monitoring event conducted in October 2012, the horizontal extent of contamination is delineated,
to the extent possible, and extends onto the adjacent property south of the Site. The vertical
extent of groundwater contamination has been sufficiently delineated by well DMW-2, which is
screened from 100’ to 105’ bgs.In general, groundwater in the vicinity of the former Northern
UST Basin is impacted by petroleum-related VOCs and break-down products above the 2L
Standards. Groundwater in the vicinity and down-gradient of the former Western UST Basin and
associated dispenser island is affected by petroleum-related and chlorinated VOCs that exceed
the 2L Standards.Groundwater in the vicinity of wells MW-5, MW-12 and MW-13 is generally
affected by chlorinated VOCs above the 2L Standards.Note that LNAPL was present in well MW-
12 (0.34 feet thick) during the June 2014 groundwater sampling event.
AMEC evaluated several remedial technologies capable of addressing petroleum-related and
chlorinated VOC-affected groundwater.The following three alternatives were evaluated for the
Site:
In-situ Chemical Application
Monitored Natural Attenuation
Air Sparging
Groundwater remedial options are discussed in the following sections of the CAP Report.
4.2.1 In-situ Chemical Application
AMEC evaluated in-situ chemical treatment of affected groundwater to enhance natural
degradation of organic contaminants through controlled chemical reactions and bioremediation.
Specifically, AMEC identified three distinct treatment areas on-site, each with specific chemical
and biological treatment requirements.Based on field parameter and laboratory data collected
from wells MW-2 and MW-10, AMEC evaluated treatment of the former Northern UST Basin area
using enhanced aerobic biodegradation. In this area, an oxygen releasing compound would be
introduced into the groundwater via 60-80 direct-push technology (DPT) injection points spaced
on approximate 8-foot centers covering approximately 4,080 square feet (sq. ft.). The treatment
zone would be from 13’ to 23’ bgs, targeting the upper 10 feet of the unconfined aquifer. An
estimated 3,400 pounds (lbs.) of oxidant and 950 gallons of water would be needed.
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For the area south of the main building and in the vicinity of wells MW-5, MW-12 and MW-13,
AMEC evaluated treatment of chlorinated VOC-affected groundwater via injection of an electron
donor compound to enhance the reductive dechlorination process in this area. The electron donor
compound would be introduced to groundwater via 40 DPT injection points spaced on
approximate 15-foot centers covering an approximate area of 9,000 sq. ft. The treatment zone
would extend from 15 feet bgs to 30 feet bgs, based on historic and current depth to water
measurements in wells in this area. An estimated 10,000 lbs. of electron donor compound and
10,750 gallons of water would be necessary to deliver the product.
The evaluation of this remedial technology using the criteria specified in the Guidelines is
presented below.
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Criteria Evaluation
A.Nature of Contamination The horizontal and vertical extent of groundwater is
delineated at the Site. The primary treatment areas areestimated to include approximately 15,000 square feet of
areal extent; however,affected groundwater (above 2LStandards)is present on the adjacent Plastics-Plus property.
Accessibility to this property has been historically difficult. Itis reasonable to expect that treated groundwater on-site will
influence down-gradient groundwater quality conditions.
B.Description of RemedialTechnology In-situ chemical application would be implemented in threeareas of the Site. It would be applied via DPT injections.
Though the technology proposed has previously been
approved for remedial applications in North Carolina, it isconsidered an Innovative Technology and will be subject to
approval by the NCDENR Innovative Technology Committeeprior to use at the Site.
An Underground Injection Control (UIC) permit will be
required to implement the technology.
Injectate would be expected to either chemically react with
impacted groundwater and/or enhance naturally occurringbioremediation for a period that lasts between 30 days
(ISCO) to 3-4 years (electron donor compounds).
Average hydraulic conductivity values calculated from slugtesting in wells MW-1, MW-6 and MW-10 was 1.15 ft/day.
Radius of influence of individual injection points is estimatedto be approximately 3 to 5 feet.
C.Feasibility and effectiveness Feasibility of injection and direct application is good, as thisremedy can be applied in stages, thereby enabling
continued use of the Site with minimal disruption to on-goingoperations.
The estimated life cycle of the proposed injectates variesfrom 30 days to 4 years.As an in-situ technology, it is not a
permanent remedial alternative. Rather, its intendedpurpose at the Site would be to actively treat impacted
groundwater, then passively improve subsurface conditionsso that natural attenuation of contaminants can continue.
D.Remedial System Operation and
Maintenance O&M is not required for this remedy, as no permanentstructures/systems would be installed at the Site.
E.Waste Treatment/Disposal Plan Waste products are not generated during in-situ chemicalapplication.
F.Schedule In-situ chemical application, as proposed, should take
between 30 and 45 days to complete for a single application.
G.Cost The estimated cost for in-situ chemical oxidation of all threeproposed areas at the site is $370,000.
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This remedial technology is not proposed for the Site since chemical application is considered an
Innovative Technology and would be subject to approval by the NCDENR Innovative
Technology Committee prior to implementation.
4.2.2 Monitored Natural Attenuation
Natural attenuation refers to the reliance of natural processes to achieve site-specific
remediation objectives within a time frame that is reasonable compared to that offered by other
more active methods. The natural reduction of contaminant concentrations is typically achieved
through a combination of biological, chemical and physical processes. Biodegradation of
hydrocarbon plumes in groundwater has been shown to be particularly effective in reducing both
contaminant mass and transformation of toxic contaminants to non-toxic byproducts by
combining electron donors (petroleum hydrocarbons) with electron acceptors such as oxygen,
nitrate, manganese (IV), ferric iron, sulfate and carbon dioxide. Carbon dioxide, water, nitrogen
gas, manganese (II), ferrous iron, hydrogen sulfide, and methane are some of the metabolic
byproducts typically produced from biodegradation of petroleum hydrocarbons. When
assessing the efficiency of natural attenuation, the following two lines of evidence should be
evaluated on a site-specific basis:
Historical groundwater chemistry data showing plume stabilization and/or contaminant
mass loss over time, and
Groundwater chemistry data showing that geochemical conditions are suitable for
biodegradation, and that active biodegradation has occurred as indicated by theconsumption of electron acceptors and/or production of final byproducts.
In addition to analysis for total VOCs, AMEC analyzed groundwater samples collected during
the Pre-CAP monitoring event in December 2011 for natural attenuation parameters including
total alkalinity, ferrous/ferric iron, manganese, sulfide, sulfate, nitrate, nitrite,total organic
nitrogen, methane, ethane and ethene. AMEC also recorded dissolved oxygen (DO),oxidation
reduction potential (ORP), specific conductance, pH and temperature in the field during purging
and prior to sample collection. The following sub-sections discuss the results of the December
2011 sampling event as they pertain to the potential for monitored natural attenuation at the
Site.
4.2.2.1 Plume Stabilization
Petroleum constituents have historically been present at concentrations exceeding the 2L
Standards in each well at the Site with the exception of wells MW-4, MW-7, MW-15 and DMW-2
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with the highest concentrations observed in groundwater samples collected from wells MW-1,
MW-2, MW-3 and MW-6. In general, an overall decreasing trend is observed in primary
contaminants of concern (tetrachlorethene, vinyl chloride, cis-1,2-dichloroethene) in wells MW-2
and MW-3.Although historical groundwater quality is limited to 2009 to present, this steady
reduction in contaminant concentrations may indicate that natural attenuation of the
contaminant plume is occurring. Benzene concentrations in well MW-3 have fluctuated
somewhat, but have generally remained consistent, further supporting the conclusion that
affected soil in the vicinity of well MW-3 acts as a continuing source of groundwater
contamination.
4.2.2.2 Natural Attenuation Parameter Results
Dissolved Oxygen
In general, dissolved oxygen (DO) concentrations less than 0.5 mg/L are indicative of anaerobic
conditions. Biodegradation of petroleum hydrocarbons occurs more readily under aerobic
conditions. In zones of high BTEX constituent concentrations, there will be a high demand for
oxygen by microbes degrading the contaminants and oxygen concentrations should be lower
than in areas outside of the plume. DO concentrations recorded during the December 2011
sampling event ranged from 4.31 mg/L in well MW-3 to 7.52 mg/L in well MW-16. The DO
concentrations in source area wells MW-1, MW-2, and MW-3 were 5.69 mg/L, 4.59 mg/L, and
4.31 mg/L, respectively, among the lowest measured on-site. The DO concentrations of
background wells MW-4, MW-7 and MW-15 were 5.11 mg/L, 5.79 mg/L, and 7.12 mg/L,
respectively. As such, it appears that DO conditions are indicative of natural attenuation at the
Site.
Oxidation/Reduction Potential
The oxidation/reduction potential (ORP) of groundwater reflects the relative oxidizing or
reducing nature of the groundwater system. ORP is influenced by the nature of the biologically
mediated degradation of contaminants,and may range from 800 millivolts (mV) (oxygenated) to
less than -400 mV (strongly reducing). Similar to DO, lower source area ORP readings can be
indicative that biodegradation is occurring. ORP readings recorded during the December 2011
sampling event ranged from -60 mV in well MW-2 to 440 mV in well MW-5. The ORP readings
in source area wells MW-1, MW-2, and MW-3 were 158 mV,-60 mV and 0 mV, respectively.
The ORP readings in background wells MW-4, MW-7 and MW-15 were 259 mV, 276 mV, and
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68 mV, respectively. As such, it appears that ORP conditions are favorable for natural
attenuation at the Site.
Nitrate
After DO has been depleted, nitrate may be used as a substrate for microbial respiration. If
biodegradation is occurring, it is expected that nitrate will be depleted within the dissolved plume
(source area). Nitrate concentrations ranged from <0.20 mg/L in several wells to 15 mg/L in
well MW-15. Nitrate was not detected above the laboratory reporting limit in the source area
wells MW-1, MW-2 or MW-3 or in the down-gradient mid-plume well MW-6. Therefore, it may
be inferred that nitrate has been consumed in the source area as fuel for microbial respiration
and that natural attenuation of the plume is occurring.
Ferrous Iron
Once the available oxygen and nitrate are depleted, subsurface organisms may use oxidized
ferric iron (Fe3+) as an electron acceptor. The reduction of ferric iron results in increased ferrous
iron (Fe2+) concentrations. Ferrous iron concentrations ranged from non-detect in several wells
to 6.0 mg/L in well MW-6. Ferrous iron concentrations in source area wells MW-1, MW-2, and
MW-3 were 5.0 mg/L, 3.0 mg/L and 1.1 mg/L, respectively. Ferrous iron was not detected
above the laboratory reporting limit in background wells MW-4, MW-7 and MW-15. Therefore, it
can be inferred that biodegradation of contaminants is occurring in the source area, resulting in
elevated ferrous iron concentrations in source area monitoring wells.
Summary
These data cumulatively suggest that enhanced natural attenuation (or biodegradation) is
occurring at the Site. A summary of field readings and natural attenuation parameter results are
presented in Table 7. Monitored natural attenuation may be a viable follow-up alternative
remedial measure (passive monitoring phase), subsequent to initial, more active remediation.
4.2.3 Air Sparging
Air sparging is a technology based on the theory of mass transfer of a substance from one
media to another, such as oxygen to the groundwater. This mass transfer of oxygen to the
subsurface will assist in the removal of organic constituents that have been detected at the site.
The oxygen is introduced into the subsurface via air sparging points at depths corresponding to
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the vertical extent of impact. Typically, the oxygen source is ambient atmospheric air and is
introduced into the subsurface at low pressures and flow rates to minimize lateral groundwater
displacement.
Air sparging is an in situ remedial technology that reduces concentrations of volatile constituents
in petroleum products that are adsorbed to soils and dissolved in groundwater. This technology,
which is also known as "in situ air stripping" and "in situ volatilization," involves the injection of
contaminant-free air into the subsurface saturated zone,enabling a phase transfer of
hydrocarbons from a dissolved state to a vapor phase. The air is then vented through the
unsaturated zone.
Air sparging is most often used together with soil vapor extraction (SVE),but it can also be used
with other remedial technologies. When air sparging (AS) is combined with SVE, the SVE
system creates a negative pressure in the unsaturated zone through a series of extraction wells
to control the vapor plume migration. This combined system is called AS/SVE.
Application
When used appropriately, air sparging has been found to be effective in reducing concentrations
of VOCs such as chlorinated solvents and petroleum hydrocarbons.Air sparging is generally
more applicable to the lighter gasoline constituents (i.e., benzene, ethylbenzene, toluene, and
xylene [BTEX]), because they readily transfer from the dissolved to the gaseous phase. Air
sparging is less applicable to diesel fuel and kerosene. Appropriate use of air sparging may
require that it be combined with other remedial methods (e.g., SVE or pump-and-treat). An air
sparging system can use either vertical or horizontal sparge wells. Well orientation should be
based on site-specific needs and conditions.
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Criteria Evaluation
A.Nature of Contamination Contaminants of concern in this area include petroleum-
related VOCs (benzene, toluene, ethylbenzene, xylenes,naphthalene, cis-1,2-dichloroethene) and chlorinated VOCs
(tetrachloroethene, trichloroethene, 1-2-dichloroethane).
The horizontal extent of VOC-affected groundwater at the
site encompasses about 2 acres.
The vertical extent of VOC-affected groundwater issufficiently delineated by well DMW-2. AS wells should be
installed to about 50 feet below grade.
Free product was recently detected in well MW-12.Handbailing of the free product identified in this well should begin
immediately, potentially followed by one Mobile Multi-PhaseExtraction (MMPE) event, if the presence of free product
persists.
B.Description of RemedialTechnology AS would be utilized to enhance volatilization (i.e. stripping)of the VOCs in the groundwater at the site.Stripped VOCs
would be captured and extracted by the installation ofhorizontal SVE piping lain in shallow trenches within the
sparge area.
The increased air flow through the subsurface can alsostimulate biodegradation of some of the contaminants,
especially those that are less volatile.
C.Feasibility and effectiveness Feasibility of AS at the Site is subject to limitation of
minimizing impacts of a permanent system on on-goingoperations at the Site.
The native soil at the site is reasonably permeable to allowfor migration of the injected air and the stripped vapors.
D.Remedial System Operation andMaintenance Weekly O&M would be required to maintain the compressor
and associated equipment.
E.Waste Treatment/Disposal Plan Waste products are not generated during AS.
F.Schedule Given the size of the proposed treatment area,AS pilot
testing could be conducted in 1 or 2 days, if funding isapproved by the Trust Fund branch. Installation of an AS
system typically takes 2-3 weeks to complete.
G.Cost The estimated cost for AS is $90,000.
This remedial technology is proposed for the site because air sparging is a cost-effective and
reliable technology for removing VOCs from groundwater.
4.3 RISK REDUCTION
In accordance with the Guidelines, the comprehensive evaluation of remedial options is to
include an evaluation of risk reduction mechanisms (e.g. connecting water-supply well users to
alternate water sources). In this specific case, the release has been classified as “High Risk”
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AMEC Environment and Infrastructure, Inc.29
based on the presence of private water-supply wells within 1,000 feet of a confirmed release.
Thus, the discussion of risk reduction mechanisms is limited to potential elimination of those
water-supply wells as potential receptors in the event that a risk does exist.
Based on the receptor survey conducted by AMEC in 2009,four wells used for drinking water
purposes are located within 1,000 feet of the site. The wells are located north/northeast of the
site.As shown on Figure 3, groundwater flow direction is to the southeast, meaning that the four
wells are located hydraulically cross-or upgradient of the site.No water-supply wells were
identified downgradient of the contaminant source area.Sampling and analysis of water from
these wells, along with other non-potable supply wells in this area has not identified
contaminants attributable to the Site. The only contaminant detected in these wells was
naphthalene (3.6 g/L)in a well located at 4801 Wild Rose Lane where a gasoline-powered
lawnmower was stored inside of the well house. As contamination has existed at the site since
prior to 1988 when the USTs were removed, it appears that contamination has not been drawn
into the private water-supply wells as a result of the pumping influence of these wells.
AMEC confirmed with Charlotte-Mecklenburg Utilities, that no municipal water lines are present
along Wild Rose Lane. Therefore, it is impractical to consider connection of the residences at
4800, 4801 and 4819 Wild Rose Lane to municipal water.No receptors have been identified
down-gradient of the site.
Before any decision can be made to implement this “risk reduction” mechanism,a determination
first has to be made if there is an actual risk. As previously stated,four wells used for drinking
water purposes located within 1,000 feet of the site are not hydraulically down-gradient and
there is no indication that the release has affected these wells.
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5.0 PROPOSED REMEDIATION PLAN
The following sections discuss the proposed remediation plan, as well as post-remediation
monitoring.AMEC’s selection of the proposed corrective action approach and the components of
the remediation system was based on the following criteria:
Anticipated Effectiveness of the Proposed Remediation System –Each component of the
proposed remediation system is designed to work in conjunction with the other
components to provide effective remediation at the site.
Feasibility of Application –Existing site conditions, including the concentrations and extentof affected groundwater at the site, subsurface soil characteristics, and hydrogeology
require that several remedial options be evaluated so that a practical and efficient methodof remediation is employed.
System Cost –In an effort to reduce costs, the system was configured to provide aneffective remediation method at a reasonable cost to the State Trust Fund for Leaking
USTs.
5.1 SELECTED TECHNOLOGIES
Based on the aforementioned criteria, AMEC believes that air sparging and soil vapor extraction is
the best alternative available for the site. This alternative was selected for the following reasons:
Protection of public health –With the injection of air as a proposed remedy at a locationwith occupied buildings, vacuum extraction will minimize the potential for contaminant
vapor intrusion into the structures.
Limited lateral extent of groundwater impact –The majority of the dissolved phase
constituents of concern are restricted to the area bounded by wells MW-2, MW-18, MW-11and MW-12.This represents an approximate affected area measuring 340 feet by 360feet.
Lack of groundwater discharge options –Implementation of a pump and treat multi-phase
extraction system is precluded by the absence of discharge options. There are no surface
waters on or bordering the site to which a discharge under a NPDES permit can be made.The Charlotte Mecklenburg Utility Department prohibits the discharge of remediated
groundwater into the municipal sewer system.
Low monthly O & M costs –Operation of the air sparging and SVE systems require O & M
visits to the site on a one or two-week basis. This is more cost-effective that otherrecovery methods (i.e. pump and treat or multi-phase extraction) that require more
intensive O & M, permitting and sampling activities.
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The conceptual design of the proposed remediation system was developed based on our
knowledge of the site conditions and experience on similar projects. AMEC developed a
conceptual sparge point layout using a 30-foot spacing with 75 feet between sparging rows. The
rows would be oriented cross-gradient of the plume.The proposed conceptual remedial system
layout is shown on Figure 13.A diagram for a typical air sparge well is shown on Figure 14. The
slotted SVE piping would be installed horizontally in shallow trenches as shown on Figure 13.
5.1.1 Permitting Requirements
NCDENR does not require a permit for the injection of air in the subsurface for air sparging as
long as the wells are located on the subject site.The Mecklenburg County Department of
Environmental Protection (MCDEP) does not require permitting for VOC emissions from vapor
extraction systems. Typically, the system is registered with the county.
A National Pollutant Discharge Elimination System (NPDES) permit would not be needed since
there will not be liquid discharged from the system.
5.2 SENTINEL WELL INSTALLATION
Because four water-supply wells were identified to the north/northeast of the subject property,
representatives of NCDENR requested that a “sentinel” monitoring well be installed in the
vicinity of monitoring well MW-18 (between the contaminant source area and the two nearest
water-supply wells located at 4800 and 4801 Wild Rose Lane).The proposed location of the
well is shown on Figure 13.The purpose of the sentinel well is to provide a groundwater
monitoring point situated generally upgradient from the water-supply wells. If future
groundwater monitoring results detect chlorinated solvents in samples from the sentinel well, it
will serve as an indicator that the contaminant plume is migrating nearer to the water-supply
wells.
AMEC proposes that the sentinel well (designated MW-18S) be constructed as a double-cased
monitoring well with the screened interval placed at about 55 to 60 feet below ground surface.
Existing site monitoring well DMW-1 is constructed as a double-cased monitoring well screened
from 55 to 60 feet below ground surface. Groundwater monitoring results have historically
shown chlorinated solvents in well DMW-1, suggesting that the depth interval of 55 to 60 feet
would be a reasonable depth to detect these contaminants.
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For well MW-18S, AMEC proposes drilling an 8 to 10-inch diameter boring to a depth of about
45 feet below ground surface using the hollow-stem auger technique. When the desired depth
is reached, a 6-inch diameter PVC outer casing will be installed in the borehole to a depth of
about 45 feet below ground surface. The annulus between the borehole and the outer casing
will be filled with cement and allowed to cure overnight. When the cement has sufficiently
cured, AMEC’s drilling contractor will drill through the bottom of the outer casing and cement to
a depth of about 60 feet below grade using the mud/rotary drilling method. A 2-inch diameter
monitoring well will be constructed of Schedule 40 PVC screen (0.010” slot) and casing will be
installed to the termination depth of the boring. The bottom five-foot section of the well will be
screened. AMEC will develop the new well by pumping groundwater from the well until
measurements of water quality parameters have stabilized. The development water will be
containerized in a 55-gallon drum and disposed as a non-hazardous waste.
5.3 GROUNDWATER QUALITY MONITORING
AMEC proposes to perform groundwater monitoring to evaluate the effectiveness of the
implemented remedial technologies.The proposed monitoring program includes:
Measurement of depth-to-groundwater in wells MW-1 through MW-18, MW-18S,DMW-1 and DMW-2 to monitor groundwater flow direction on a quarterly basis for
the first year and then semi-annually thereafter.
Sampling and laboratory analysis of groundwater from monitoring wells MW-1
through MW-18, MW-18S,DMW-1 and DMW-2 to document degradation of the
constituent plume on a quarterly basis for the first year and then semi-annuallythereafter. Groundwater samples will be analyzed for VOCs using EPA Method
6200B.
Quarterly reports will be prepared and forwarded to the NCDENR to document each sampling
event. The reports will summarize the field activities performed, historical groundwater quality
data for each monitoring well,and an evaluation of the effectiveness of remediation of
constituents in groundwater at the Site.A potentiometric map from each event will be presented,
and changes in groundwater flow patterns with time will be noted. The analytical data will be
presented in tabular form and will include the laboratory results from the sampling events.
The monitoring plan will be evaluated annually to consider appropriate adjustments to the
sampling frequency and analytical program.
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AMEC Environment and Infrastructure, Inc.33
5.4 COST ESTIMATE
The estimated cost for remediation, as proposed above, is shown in the table below:
Remedial Activity Estimated Cost
Sentinel Well Installation $9,237
Design & Specify Remedial Systems $5,000
Installation of Remedial Systems $181,763 (actual cost to be determined through bidprocess)
O & M of Remedial Systems (per year)$40,000
Quarterly Groundwater Monitoring (per year)$64,000
ESTIMATED TOTAL $300,000
5.5 SCHEDULE
Implementation of the corrective action is proposed in general accordance with the following
schedule:
Remedial Activity Timeframe Estimated CompletionDate
Revised Corrective Action Plan
submittal
January 2015 January 2015
Prepare and Submit TA to Design
and Specify Remedial Systems(Task Code 7.015)December 2014 December 2014
Remedial Design Submittal January to February 2015 February 2015
Remedial System Installation April to June 2015 June 2015
Remedial System Operational July 2015 to July 2018 July 2018
Groundwater Quality Monitoring Quarterly or Semi-Annual (as
approved by NCDENR)July 2018
Site Closure via Notice of ResidualPetroleum July 2018 July 2018
The project site closure date is a general estimate only. The actual time for closure of the Site
will depend on site conditions and regulatory review.
5.6 PUBLIC NOTIFICATION/CAP CERTIFICATION
Copies of the required letters of notification for this CAP will be submitted to the chief
administrative officer for the City of Charlotte, Health Director for Mecklenburg County, and all
property owners and occupants within or contiguous to the area underlain by the contaminant
plume by certified mail in accordance with Title 15A of the North Carolina Administrative Code
(NCAC), Subchapter 2L, Section .0114, dated November 8, 1993, last revised December 5, 1995.
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AMEC Environment and Infrastructure, Inc.34
Copies of the letters and the delivery receipts will be submitted to the NCDENR after they are
received.
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AMEC Environment and Infrastructure, Inc.35
6.0 REFERENCES
Brown, L.A. and R. Fraxedas. 1992. Air sparging extending volatilization to contaminated
aquifers, in Proceedings of the Symposium on Soil Venting, April 29-May 1, 1991, Houston,
Texas, pp. 249-269. U.S. EPA, Office of Research and Development. EPA/600/R-92/174.
Johnson, R.L., P.C. Johnson, D.B. McWhorter, R.E. Hinchee, and I. Goodman. 1993. An
overview of in situ air sparging. Ground Water Monitoring Review. Vol. 13, No. 4, pp. 127-135.
Hinchee, R.E. 1994. Air Sparging for Site Remediation. Boca Raton,FL: Lewis Publishers.
Marley, M., D.J. Hazenbronck, and M.T. Walsh. 1992. The application of in situ air sparging as
an innovative soils and groundwater remediation technology. Ground Water Monitoring Review.Vol. 12, No. 2, pp. 137-145.
Martin, L.M., R.J. Sarnelli, and M.T. Walsh. 1992. Pilot-scale evaluation of groundwater airsparging: site-specific advantages and limitations, in Proceedings of R&D 92-National Research
and Development Conference on the Control of Hazardous Materials. Greenbelt, MD:
Hazardous Materials Control Research Institute.
U.S. Environmental Protection Agency (EPA). 1992. A Technology Assessment of Soil Vapor
Extraction and Air Sparging. Washington, D.C.: Office of Research and Development.EPA/600/R-92/173.
TABLES
AMEC Environment and Infrastructure, Inc.
TABLES
Parcel Number Land Owner and Address Parcel Address
04506401
National Rental Properties LP
450 South Orange Ave. #900
Orlando, FL 32801
4718 N. Graham St.
04506303
Plastic-Plus Awards Company
4321 Equipmant Dr.
Charlotte, NC 28269
4321 Equipment Dr.
04506306
Hertz Equipment Rental Corp.
225 Brae Boulevard
Park Ridge, NJ 07656
4429 Equipment Dr.
04506310
BGCS Property Associates, LLC
7500 Reba Dr.
Raleigh, NC 27616
4501 Equipment Dr.
04506201
Jordan Sorrells
4801 Wild Rose Ln.
Charlotte, NC 28269
4801 Wild Rose Ln.
04506204
Rick Hager, LLC
1809 Cannon Ave.
Charlotte, NC 28262
1809 Cannon Ave.
04506205
James Ervin, Sr.
4818 N. Graham St.
Charlotte, NC 28213
1815 Cannon Ave.
04506206
Jack Hendricks
1823 Cannon Ave.
Charlotte, NC 28269
1823 Cannon Ave.
04506207
Galloway & Associates, LLC
16601 Capps Rd.
Charlotte, NC 28278
4824 N. Graham St.
04519101
D&B Finance Company, LLC
4823 N. Graham St.
Charlotte, NC 28269
4801 N. Graham St.
Prepared By/Date:AJF 11-9-12
Checked By/Date:MPF 11-9-12
Summary of Adjacent Property Owner Information
Southern Pump and Tank Company
4800 North Graham Street, Charlotte, North Carolina
AMEC Project: 6228-09-5100
Table 1
Table 2
Summary of Well Construction and Groundwater Elevation Data
Southern Pump and Tank Company
4800 North Graham Street, Charlotte, North Carolina
AMEC Project: 6228-13-0135
Well Date
Completed
TOC Elevation
(ft above MSL)Date Depth to Water
(ft below TOC)
Groundwater
Elevation
(ft above MSL)
Screened Interval
(ft below TOC)
Constructed
Well Depth
(ft below TOC)
1/22/2010 20.68 754.47
4/26/2011 17.18 757.97
12/23/2011 17.68 757.47
10/15/2012 20.86 754.29
8/7/2013 16.05 759.10
6/10/2014 14.64 760.51
4/26/2011 16.36 758.71
12/20/2011 19.16 755.91
10/15/2012 20.00 755.07
8/7/2013 15.45 759.62
6/10/2014 13.54 761.53
5/22/2009 15.58 760.17
1/22/2010 14.85 760.90
4/26/2011 16.60 759.15
12/28/2011 18.00 757.75
10/15/2012 20.31 755.448/7/2013 15.20 760.556/10/2014 14.27 761.48
5/22/2009 15.08 762.45
1/25/2010 13.75 763.78
4/26/2011 16.29 761.24
12/23/2011 16.46 761.0710/17/2012 20.30 757.238/7/2013 7.62 769.916/10/2014 12.75 764.78
5/22/2009 15.91 760.16
1/21/2010 13.94 762.134/26/2011 16.05 760.0212/22/2011 17.78 758.29
10/16/2012 19.92 756.15
8/7/2013 14.07 762.00
6/10/2014 12.26 763.81
5/22/2009 11.61 763.791/21/2010 10.18 765.22
4/26/2011 12.70 762.70
12/22/2011 13.92 761.48
10/17/2012 16.04 759.36
8/7/2013 10.31 765.09
6/10/2014 9.30 766.10
5/22/2009 16.93 760.56
1/22/2010 16.23 761.26
4/26/2011 17.81 759.68
12/22/2012 19.36 758.13
10/15/2012 DRY NA
8/7/2013 16.39 761.10
6/10/2014 14.65 762.84
5/22/2009 15.02 760.46
1/25/2010 13.75 761.73
4/26/2011 15.59 759.89
12/28/2011 17.60 757.88
10/16/2012 19.72*755.788/7/2013 15.08 760.406/10/2014 13.82 761.66
5/22/2009 14.95 757.21
1/22/2010 13.99 758.17
4/26/2011 16.00 756.16
12/22/2011 16.43 755.7310/16/2012 19.42 752.748/7/2013 15.50 756.666/10/2014 14.13 758.03
1/22/2010 15.04 759.21
4/26/2011 16.73 757.5212/22/2011 18.36 755.8910/16/2012 DRY DRY
8/7/2013 15.70 758.556/10/2014 14.31 759.94
MW-2 2/5/2009 777.53 13-28 28
MW-1 2/5/2009 775.75 15-25 25
MW-4 5/21/2009 775.40 12-22 22
MW-3 5/21/2009 776.07 12-22 22
MW-5 5/21/2009 777.49 12-22 22
MW-7 5/21/2009 772.16 12-22 22
MW-6 5/21/2009 775.48 12-22 22
MW-8 1/11/2010 774.25 10-20 20
DMW-1 1/14/2010 775.15 55-60 60
DMW-2 4/1/2011 775.07 100-105 105
Page 1 of 2 Prepared by/Date:MDF 6-20-14Checked by/Date: BLH 6-24-14
Table 2
Summary of Well Construction and Groundwater Elevation Data
Southern Pump and Tank Company
4800 North Graham Street, Charlotte, North Carolina
AMEC Project: 6228-13-0135
Well Date
Completed
TOC Elevation
(ft above MSL)Date Depth to Water
(ft below TOC)
Groundwater
Elevation
(ft above MSL)
Screened Interval
(ft below TOC)
Constructed
Well Depth
(ft below TOC)
DMW-1 1/14/2010 775.15 55-60 60
1/21/2010 14.58 759.474/26/2011 16.34 757.7112/23/2011 18.11 755.94
10/16/2012 20.05 754.00
8/7/2013 15.27 758.78
6/10/2014 13.72 760.33
1/21/2010 12.85 762.514/26/2011 14.91 760.45
12/22/2011 16.75 758.61
10/17/2012 19.70 755.66
8/7/2013 14.07 761.29
6/10/2014 13.40 761.96
1/22/2010 14.45 759.46
4/26/2011 16.31 757.60
12/28/2011 17.38 756.53
10/16/2012 19.98 753.93
8/7/2013 15.52 758.39
6/10/2014 14.46 759.45
1/22/2010 16.35 761.53
4/26/2011 18.10 759.78
12/29/2011 19.43 758.45
10/15/2012 21.75*756.43
8/7/2013 NM NM
6/10/2014 14.60*763.89
1/22/2010 15.80 761.24
4/26/2011 17.36 759.68
12/29/2011 18.47 758.57
10/15/2012 20.98 756.06
8/7/2013 16.09 760.95
6/10/2014 14.50 762.54
1/25/2010 14.24 760.06
4/26/2011 15.98 758.32
12/29/2011 17.97 756.33
10/17/2012 19.41 754.89
8/7/2013 15.12 759.18
6/10/2014 13.83 760.47
1/25/2010 13.30 759.41
4/26/2011 15.32 757.39
12/29/2011 16.21 756.50
10/17/2012 18.66 754.05
8/7/2013 14.72 757.996/10/2014 13.78 758.93
4/26/2011 16.29 756.45
12/20/2011 17.83 754.91
10/16/2012 19.98 752.76
8/7/2013 15.53 757.216/10/2014 14.23 758.51
4/26/2011 13.20 760.45
12/28/2011 14.96 758.69
10/17/2012 18.20 755.45
8/7/2013 12.06 761.59
6/10/2014 10.22 763.43
4/26/2011 13.65 757.84
12/23/2011 15.65 755.84
10/16/2012 17.60 753.89
8/7/2013 12.79 758.70
6/10/2014 11.34 760.15
Notes:
1. TOC = Top of casing
2. MSL = Mean sea level
3. * = Depths to groundwater corrected for the presence of free product with an assumed density of 0.866.
4. DRY = Well dry at the time of sampling.
5. NM = Not meausred; well contained free product at the time of sampling.
MW-9 1/11/2010 774.05 13-23 23
MW-11 1/12/2010 773.91 13-23 23
MW-10 1/12/2010 775.36 13-23 23
MW-13 1/12/2010 777.04 13-23 23
MW-12 1/12/2010 777.88 13-23 23
MW-15 1/21/10 772.71 13-23 23
MW-14 1/21/10 774.30 13-23 23
MW-16 1/6/2011 772.74 15-25 25
MW-17 4/13/11 773.65 11-21 21
21MW-18 4/13/2011 771.49 11-21
Page 2 of 2 Prepared by/Date:MDF 6-20-14Checked by/Date: BLH 6-24-14
Well #Well Owner/ User Address Phone Number Well Use Well Depth
(ft. bgs)Type of Well
Well Casing
Depth (ft.
bgs)
Well Screen
Interval (ft.
bgs)
Distance from
source area of
release (ft.)
8708109 Tryon Imports, Inc.4320 Old Interstate Rd.
Charlotte, NC 28206 Unknown Private water
supply 320 Water supply Unknown Unknown 1,400
4506107 Arnold Carroll 1719 Canon Ave.
Charlotte, NC 28269 704-596-1919 Private water
supply Unknown Water supply Unknown Unknown 650
4506110 James Nunn 4800 Wild Rose Ln.Charlotte, NC 28269 Unknown Private watersupply 270 (casedto 200)Water supply Unknown Unknown 450
4506109 Arnold Carroll 4820 Wild Rose Ln.
Charlotte, NC 28269 704-597-7080 Private water
supply Unknown Water supply Unknown Unknown 550
4506202 James Nunn 4819 Wild Rose Ln.
Charlotte, NC 28269 Unknown Private water
supply
110 (cased
to 98)Water supply Unknown Unknown 480
4506201 Jordan Sorrells 4801 Wild Rose Ln.
Charlotte, NC 28269 Unknown Private water
supply Unknown Water supply Unknown Unknown 390
4506206 Jack Hendricks 1823 Cannon Ave.
Charlotte, NC 28269 704-596-1295 Private water
supply Unknown Water supply Unknown Unknown 440
4509311 Arnold Carroll 1644 Cannon Ave.
Charlotte, NC 28269 Unknown Private water
supply Unknown Water supply Unknown Unknown 1,050
4509312 Richard Railey 1640 Cannon Ave.
Charlotte, NC 28269 704-921-9565 Private water
supply 30 Water supply Unknown Unknown 1,100
4509206 Carolyn Davis 4906 N. Graham St.Charlotte, NC 28269 704-596-2559 Private watersupply Unknown Water supply Unknown Unknown 700
4509204 Lloyd Burris 4930 N. Graham St.
Charlotte, NC 28269 704-596-6356 Private water
supply Unknown Water supply Unknown Unknown 950
4509111 Janet Bickett 5018 N. Graham St.
Charlotte, NC 28269 Unknown Private water
supply Unknown Water supply Unknown Unknown 1,110
4519101 D&B Finance
Company, LLC
4801 N. Graham St.
Charlotte, NC 28269 Unknown Private water
supply Unknown Water supply Unknown Unknown 510
4509112 Kinsaka Clement 1818 Oneida Rd.
Charlotte, NC 28269 Unknown Private water
supply Unknown Water supply Unknown Unknown 1,100
4509113 Mario Bautista 1810 Oneida Rd.
Charlotte, NC 28269 Unknown Private water
supply Unknown Water supply Unknown Unknown 1,100
4509203 Michael Gilstrap 1819 Oneida Rd.
Charlotte, NC 28269 Unknown Private water
supply Unknown Water supply Unknown Unknown 850
4509202 James Nunn 1811 Oneida Rd.Charlotte, NC 28269 704-596-0409 Private watersupply Unknown Water supply Unknown Unknown 850
4509207 Edith Dellinger 1818 Cannon Ave.
Charlotte, NC 28269 Unknown Private water
supply Unknown Water supply Unknown Unknown 650
4509209 Arnold Carroll 1800 Cannon Ave.
Charlotte, NC 28269 Unknown Private water
supply Unknown Water supply Unknown Unknown 650
Revised By/Date:AJF 11-9-12
Checked By/Date:RCF 11-14-2014
Summary of Water-Supply Well Information
Southern Pump and Tank Company
4800 North Graham Street, Charlotte, North Carolina
AMEC Project: 6228-13-0135
Table 3
TABLE 4
Summary of Laboratory Analyses - Soil Samples (October 2008-December 2011)
Southern Pump and Tank Company
4800 North Graham Street, Charlotte, North Carolina
AMEC Project:6228-09-5100ConstituentFP-1 FP-2 T-1 T-2 T-3 T-4 T-5 T-6 GP-1 GP-2 GP-3 GP-4 GP-5 (10)GP-5 (15)GP-5 (5)GP-6 (10)GP-6 (15)
Date Collected 10/1/2008 10/1/2008 10/1/2008 10/1/2008 10/1/2008 10/1/2008 10/1/2008 10/1/2008 2/5/2009 2/5/2009 2/5/2009 2/5/2009 1/13/2010 1/13/2010 1/13/2010 1/13/2010 1/13/2010
Depth (feet bgs)6.5-7.5 3-4 14-15 14-15 10-11 14-15 10-11 5-6 13-15 8-10 8-10 13-15 10 15 5 10 15
Volatile Organic Compounds (VOCs) by EPA 8260
1,1,1,2-Tetrachloroethane NSL NSL <0.0058 <1.33 --------------------<0.0045 <0.468 <0.0039 <0.0045 <0.0069
1,1-Dichloroethane 0.032 1,000 <0.0058 <1.33 --------------------<0.0045 <0.468 <0.0039 <0.0045 <0.0069
1,2,4-Trimethylbenzene 8.5 20,440 <0.0058 18.2 --------------------5.14 8.36 0.0102 <0.0045 <0.0069
1,2-Dichlorobenzene 0.23 36,000 <0.443 <1.33 --------------------<0.0045 <0.468 <0.0039 <0.0045 <0.0069
1,2-Dichloroethane 0.0019 63 <0.0058 <1.33 --------------------0.0223 <0.468 <0.0039 <0.0045 0.0121
1,3,5-Trimethylbenzene 8.3 20,440 <0.0058 5.55 --------------------0.132 2.77 <0.0039 <0.0045 <0.0069
4-Methyl-2-pentanone (MIBK)NSL NSL <0.058 <13.3 --------------------<0.045 <4.68 <0.039 <0.045 <0.069
Aliphatic (C05-C08)68 24,528 --------------------------13.9 ----<13.0
Aliphatic (C09-C12)540 40,000 --------------------------13.8 ----<13.0
Aliphatic (C09-C18)540 40,000 --------------------------163 ----<15.7
Aliphatic (C19-C36)###810,000 --------------------------<62.7 ----<15.7
Aromatic (C09-C10)31 12,264 --------------------------<8.6 ----<13.0
Aromatic (C11-C22)31 12,264 --------------------------47.4 ----<15.7
Benzene 0.0056 164 <0.0058 1.88 --------------------2.47 4.37 0.0998 0.0839 0.160
Diisopropyl ether 0.37 4,088 <0.0058 <1.33 --------------------<0.0045 <0.468 <0.0039 <0.0045 <0.0069
Ethylbenzene 4.9 40,000 <0.0058 6.41 --------------------2.30 3.66 0.0548 0.0153 <0.0069
Isopropylbenzene (Cumene)1.7 40,880 <0.0058 <1.33 --------------------0.0253 <0.468 0.0042 <0.0045 <0.0069
Methyl-tert-butyl ether 0.091 3,100 <0.0058 <1.33 --------------------<0.0045 <0.468 <0.0039 <0.0045 <0.0069
Methylene Chloride 0.02 763 <0.023 <5.33 --------------------<0.018 <1.87 <0.016 <0.018 <0.028
Naphthalene 0.16 8,176 <0.443 4.24 --------------------0.181 2.01 0.0175 <0.0045 0.0197
Tetrachloroethene 0.0074 10 0.0354 <1.33 --------------------0.0684 1.04 <0.0039 <0.0045 <0.0069
Toluene 4.3 32,000 <0.0058 22.6 --------------------8.22 7.92 <0.0039 <0.0045 <0.0069
Trichloroethene 0.019 120 0.0134 <1.33 --------------------<0.0045 <0.468 <0.0039 <0.0045 <0.0069
Vinyl chloride 0.00018 4.1 <0.012 <2.67 --------------------<0.0091 <0.935 <0.0079 <0.0090 <0.014
Xylene (Total)4.6 81,760 <0.012 32.4 --------------------10.5 17.3 <0.0079 <0.0090 <0.014
cis-1,2-Dichloroethene 0.35 4,000 0.0994 1.65 --------------------0.0337 <0.468 <0.0039 0.0111 0.0196
m&p-Xylene 4.6 81,760 <0.012 24.6 --------------------7.66 12.5 <0.0079 <0.0090 <0.014
n-Butylbenzene 4.3 16,350 <0.0058 <1.33 --------------------0.0354 0.782 <0.0039 <0.0045 <0.0069
n-Propylbenzene 1.7 16,350 <0.0058 2.65 --------------------0.0795 1.33 0.0148 <0.0045 <0.0069
o-Xylene 4.6 81,760 <0.0058 7.81 --------------------2.88 4.81 <0.0039 <0.0045 0.0069
p-Isopropyltoluene NSL NSL <0.0058 <1.33 --------------------0.0217 <0.468 <0.0039 <0.0045 <0.0069
sec-Butylbenzene 3.3 16,350 <0.0058 <1.33 --------------------0.0093 <0.468 <0.0039 <0.0045 <0.0069
tert-Butylbenzene 3.4 16,350 <0.0058 <1.33 --------------------<0.0045 <0.468 <0.0039 <0.0045 <0.0069
trans-1,2-Dichloroethene 0.54 8,200 <0.0058 <1.33 --------------------<0.0045 <0.468 <0.0039 <0.0045 <0.0069
Semi-Volatile Organic Compounds (SVOCs) by EPA 8270
1-Methylnaphthalene NSL NSL <0.443 1.93 ------------------------------
2-Methylnaphthalene 3.6 1,635 <0.443 3.80 ------------------------------
Metals by EPA 6010 and EPA 7471
Arsenic NSL NSL 1.4 2.7 ------------------------------
Barium 290 81,000 14.8 46.6 ------------------------------
Cadmium NSL NSL 1.9 0.52 ------------------------------
Chromium 5.4 1,226 12.4 21.9 ------------------------------
Lead 270 400 3.6 13.6 ------------------------------
Mercury NSL NSL 0.15 0.060 ------------------------------
Selenium NSL NSL 6.7 2.7 ------------------------------
Total Petroleum Hydrocarbons (TPH) by EPA 8015
Diesel Range Organics DRO)NSL NSL ----12400 949 409 3510 175 15.5 724 1300 270 1390 69.7 576 8.3 <6.8 <7.8
Gasoline Range Organics (GRO)NSL NSL ----265 66.7 23.2 188 167 <6.3 1670 1170 122 278 53.0 394 <4.7 <5.7 <8.5
Notes:
1. Concentrations shown in mg/kg (ppm)Prepared By/Date:
2. -- = Not Analyzed
3. NSL = No Standard Listed Checked By/Date:
4. ### = Considered Immobile
5. MSCCs = Maximum Soil Contaminant Concentraions
6. Soil-to-Water MSCCS and Industrial/Commercial MSCCs, dated January 2010
8. State Action Level for TPH DRO and TPH GRO is 10 mg/kg
9. Bold/Underlined values exceed the Soil-to-Water MSCCs/State Action Level
10. Highlighted values exceed the Industrial/Commercial MSCCs
Soil-to-Water
MSCCs
Industrial/
Commercial
MSCCs
AJF 4-5-12
MPF 11-9-12
1 of 3
TABLE 4
Summary of Laboratory Analyses - Soil Samples (October 2008-December 2011)
Southern Pump and Tank Company
4800 North Graham Street, Charlotte, North Carolina
AMEC Project:6228-09-5100Constituent
Date Collected
Depth (feet bgs)
Volatile Organic Compounds (VOCs) by EPA 8260
1,1,1,2-Tetrachloroethane NSL NSL
1,1-Dichloroethane 0.032 1,000
1,2,4-Trimethylbenzene 8.5 20,440
1,2-Dichlorobenzene 0.23 36,000
1,2-Dichloroethane 0.0019 63
1,3,5-Trimethylbenzene 8.3 20,440
4-Methyl-2-pentanone (MIBK)NSL NSL
Aliphatic (C05-C08)68 24,528
Aliphatic (C09-C12)540 40,000
Aliphatic (C09-C18)540 40,000
Aliphatic (C19-C36)###810,000
Aromatic (C09-C10)31 12,264
Aromatic (C11-C22)31 12,264
Benzene 0.0056 164
Diisopropyl ether 0.37 4,088
Ethylbenzene 4.9 40,000
Isopropylbenzene (Cumene)1.7 40,880
Methyl-tert-butyl ether 0.091 3,100
Methylene Chloride 0.02 763
Naphthalene 0.16 8,176
Tetrachloroethene 0.0074 10
Toluene 4.3 32,000
Trichloroethene 0.019 120
Vinyl chloride 0.00018 4.1
Xylene (Total)4.6 81,760
cis-1,2-Dichloroethene 0.35 4,000
m&p-Xylene 4.6 81,760
n-Butylbenzene 4.3 16,350
n-Propylbenzene 1.7 16,350
o-Xylene 4.6 81,760
p-Isopropyltoluene NSL NSL
sec-Butylbenzene 3.3 16,350
tert-Butylbenzene 3.4 16,350
trans-1,2-Dichloroethene 0.54 8,200
Semi-Volatile Organic Compounds (SVOCs) by EPA 8270
1-Methylnaphthalene NSL NSL
2-Methylnaphthalene 3.6 1,635
Metals by EPA 6010 and EPA 7471
Arsenic NSL NSL
Barium 290 81,000
Cadmium NSL NSL
Chromium 5.4 1,226
Lead 270 400
Mercury NSL NSL
Selenium NSL NSL
Total Petroleum Hydrocarbons (TPH) by EPA 8015
Diesel Range Organics DRO)NSL NSL
Gasoline Range Organics (GRO)NSL NSL
Notes:
1. Concentrations shown in mg/kg (ppm)
2. -- = Not Analyzed
3. NSL = No Standard Listed
4. ### = Considered Immobile
5. MSCCs = Maximum Soil Contaminant Concentraions
6. Soil-to-Water MSCCS and Industrial/Commercial MSCCs, dated January 2010
8. State Action Level for TPH DRO and TPH GRO is 10 mg/kg
9. Bold/Underlined values exceed the Soil-to-Water MSCCs/State Action Level
10. Highlighted values exceed the Industrial/Commercial MSCCs
Soil-to-Water
MSCCs
Industrial/
Commercial
MSCCs
GP-6 (5)GP-7 (10)GP-7 (15)GP-7 (5)GP-8 (10)GP-8 (15)MW-1 (10)MW-1 (15)MW-1 (5)MW-2 (1')MW-2 (10)MW-2 (15)MW-2 (5)SB-1 (12')SB-1 (5')SB-2 (1.5')SB-3 (13')
1/13/2010 1/13/2010 1/13/2010 1/13/2010 1/13/2010 1/13/2010 2/5/2009 2/5/2009 2/5/2009 9/20/2011 2/6/2009 2/6/2009 2/6/2009 12/15/2011 12/15/2011 12/15/2011 12/15/2011
5 10 15 5 10 15 10 15 5 1 10 15 5 12 5 1.5 13
<0.0044 <1.20 <0.0044 <0.233 <0.423 <0.522 --<0.264 <0.0050 <0.204 --<0.0064 <0.0057 <0.0059 <0.0049 <0.230 <0.246
<0.0044 <1.20 <0.0044 <0.233 <0.423 <0.522 --<0.264 <0.0050 <0.204 --0.0586 0.0185 <0.0059 <0.0049 <0.230 <0.246
<0.0044 11.7 0.405 <0.233 <0.423 15.9 --41.3 0.0108 24.6 --0.159 0.436 <0.0059 <0.0049 2.26 0.381
<0.0044 <1.20 0.0141 <0.233 <0.423 0.746 --<8.45 <0.418 <2.08 --<0.500 <0.408 <0.0059 <0.0049 <0.230 <0.246
<0.0044 <1.20 <0.0044 <0.233 <0.423 <0.522 --<0.264 <0.0050 <0.204 --<0.0064 <0.0057 <0.0059 <0.0049 <0.230 <0.246
<0.0044 4.48 0.111 <0.233 <0.423 12.1 --15.3 0.0131 12.8 --0.0398 0.128 <0.0059 <0.0049 0.263 <0.246
<0.044 <12.0 <0.044 <2.33 <4.23 <5.22 --5.92 <0.051 <2.04 --<0.064 <0.057 <0.059 <0.049 <2.30 <2.46
--22.4 ------289 52.2 49.4 <13.5 --<15.0 <14.3 <9.3 --------
--188 ------756 403 459 42.1 --25.2 <14.3 9.5 --------
--3730 ------3410 3210 <12.8 4190 --55.0 72.2 111 --------
--<2600 ------<1390 228 <12.8 296 --<13.6 55.3 41.0 --------
--37.6 ------171 131 153 <13.5 --<15.0 <14.3 <9.3 --------
--1160 ------971 627 <12.8 1770 --33.2 62.3 63.5 --------
0.0520 <1.20 0.0706 <0.233 <0.423 8.76 --1.35 0.0155 0.431 --0.157 0.179 0.0060 <0.0049 0.428 <0.246
<0.0044 <1.20 <0.0044 <0.233 <0.423 <0.522 --<0.264 <0.0050 <0.204 --0.0467 0.0660 <0.0059 <0.0049 <0.230 <0.246
0.0094 1.69 0.0206 <0.233 <0.423 5.66 --7.74 <0.0050 2.62 --0.0814 0.194 <0.0059 <0.0049 0.621 <0.246
<0.0044 <1.20 0.0180 <0.233 <0.423 1.66 --1.93 <0.0050 0.362 --<0.0064 0.0117 <0.0059 <0.0049 <0.230 <0.246
<0.0044 <1.20 <0.0044 <0.233 <0.423 <0.522 --<0.264 <0.0050 0.318 --0.150 1.99 0.0195 0.0353 <0.230 0.522
<0.018 <4.79 <0.018 <0.933 <1.69 <2.09 --<1.06 <0.020 <0.816 --0.172 <0.023 <0.024 <0.020 <0.922 <0.983
<0.0044 4.65 0.299 <0.233 0.944 15.7 --25.5 <0.418 8.12 --2.14 0.419 <0.0059 <0.0049 1.45 <0.246
<0.0044 14.9 0.543 <0.233 <0.423 19.1 --0.928 0.200 <0.204 --5.19 <0.0057 <0.0059 <0.0049 <0.230 <0.246
<0.0044 3.39 0.0208 <0.233 <0.423 0.540 --0.360 <0.0050 <0.204 --0.551 0.0796 <0.0059 <0.0049 <0.230 <0.246
<0.0044 <1.20 0.0113 <0.233 <0.423 1.41 --<0.264 0.0139 <0.204 --0.101 <0.0057 <0.0059 <0.0049 <0.230 <0.246
<0.0087 <2.39 <0.0088 <0.467 <0.846 <1.04 --<0.528 <0.010 <0.408 --0.323 0.0358 <0.012 <0.0098 <0.461 <0.492
<0.0087 9.61 0.257 <0.467 <0.846 14.3 --24.8 0.0268 21.8 --0.440 0.640 <0.012 <0.0098 1.02 <0.492
0.0075 <1.20 0.0570 <0.233 <0.423 10.1 --32.4 0.300 <0.204 --8.01 0.918 0.0244 <0.0049 <0.230 <0.246
<0.0087 6.86 0.169 <0.467 <0.846 13.1 --20.0 <0.010 21.7 --0.278 0.517 <0.012 <0.0098 0.975 <0.492
<0.0044 1.61 0.0571 <0.233 <0.423 4.11 --3.49 <0.0050 <0.204 --<0.0064 0.0190 <0.0059 <0.0049 0.402 <0.246
<0.0044 1.47 0.0430 <0.233 <0.423 4.56 --4.36 <0.0050 1.10 --0.0163 0.0422 <0.0059 <0.0049 0.380 <0.246
<0.0044 2.74 0.0877 <0.233 <0.423 1.17 --4.80 0.0253 <0.204 --0.162 0.123 <0.0059 <0.0049 <0.230 <0.246
<0.0044 2.10 0.0749 <0.233 <0.423 4.85 --6.26 <0.0050 1.58 --0.0071 0.0146 <0.0059 <0.0049 <0.230 <0.246
<0.0044 <1.20 0.0257 <0.233 <0.423 1.78 --<0.264 <0.0050 0.393 --<0.0064 0.0058 <0.0059 <0.0049 <0.230 <0.246
<0.0044 <1.20 0.0051 <0.233 <0.423 <0.522 --<0.264 <0.0050 <0.204 --<0.0064 <0.0057 <0.0059 <0.0049 <0.230 <0.246
<0.0044 <1.20 <0.0044 <0.233 <0.423 <0.522 --<0.264 <0.0050 <0.204 --0.0095 <0.0057 <0.0059 <0.0049 <0.230 <0.246
--------------48.1 <0.418 2.19 --1.75 0.563 --------
--------------62.5 <0.418 3.76 --2.62 0.623 --------
----------------------------------
----------------------------------
----------------------------------
----------------------31.7 32.5 --------
----------------------4.5 4.3 --------
----------------------------------
----------------------------------
<5.8 5720 1450 19.6 157 6030 ----------------------
<4.7 1090 49.3 <5.4 48.5 750 ----------------------
Prepared By/Date:
Checked By/Date:
AJF 4-5-12
MPF 11-9-12
2 of 3
TABLE 4
Summary of Laboratory Analyses - Soil Samples (October 2008-December 2011)
Southern Pump and Tank Company
4800 North Graham Street, Charlotte, North Carolina
AMEC Project:6228-09-5100Constituent
Date Collected
Depth (feet bgs)
Volatile Organic Compounds (VOCs) by EPA 8260
1,1,1,2-Tetrachloroethane NSL NSL
1,1-Dichloroethane 0.032 1,000
1,2,4-Trimethylbenzene 8.5 20,440
1,2-Dichlorobenzene 0.23 36,000
1,2-Dichloroethane 0.0019 63
1,3,5-Trimethylbenzene 8.3 20,440
4-Methyl-2-pentanone (MIBK)NSL NSL
Aliphatic (C05-C08)68 24,528
Aliphatic (C09-C12)540 40,000
Aliphatic (C09-C18)540 40,000
Aliphatic (C19-C36)###810,000
Aromatic (C09-C10)31 12,264
Aromatic (C11-C22)31 12,264
Benzene 0.0056 164
Diisopropyl ether 0.37 4,088
Ethylbenzene 4.9 40,000
Isopropylbenzene (Cumene)1.7 40,880
Methyl-tert-butyl ether 0.091 3,100
Methylene Chloride 0.02 763
Naphthalene 0.16 8,176
Tetrachloroethene 0.0074 10
Toluene 4.3 32,000
Trichloroethene 0.019 120
Vinyl chloride 0.00018 4.1
Xylene (Total)4.6 81,760
cis-1,2-Dichloroethene 0.35 4,000
m&p-Xylene 4.6 81,760
n-Butylbenzene 4.3 16,350
n-Propylbenzene 1.7 16,350
o-Xylene 4.6 81,760
p-Isopropyltoluene NSL NSL
sec-Butylbenzene 3.3 16,350
tert-Butylbenzene 3.4 16,350
trans-1,2-Dichloroethene 0.54 8,200
Semi-Volatile Organic Compounds (SVOCs) by EPA 8270
1-Methylnaphthalene NSL NSL
2-Methylnaphthalene 3.6 1,635
Metals by EPA 6010 and EPA 7471
Arsenic NSL NSL
Barium 290 81,000
Cadmium NSL NSL
Chromium 5.4 1,226
Lead 270 400
Mercury NSL NSL
Selenium NSL NSL
Total Petroleum Hydrocarbons (TPH) by EPA 8015
Diesel Range Organics DRO)NSL NSL
Gasoline Range Organics (GRO)NSL NSL
Notes:
1. Concentrations shown in mg/kg (ppm)
2. -- = Not Analyzed
3. NSL = No Standard Listed
4. ### = Considered Immobile
5. MSCCs = Maximum Soil Contaminant Concentraions
6. Soil-to-Water MSCCS and Industrial/Commercial MSCCs, dated January 2010
8. State Action Level for TPH DRO and TPH GRO is 10 mg/kg
9. Bold/Underlined values exceed the Soil-to-Water MSCCs/State Action Level
10. Highlighted values exceed the Industrial/Commercial MSCCs
Soil-to-Water
MSCCs
Industrial/
Commercial
MSCCs
SB-3 (7')SB-4 (16')SB-4 (6')SB-5 (13')SB-5 (17')SB-6 (10')SB-6 (17')SB-7 (16')SB-7 (7')SB-8 (16')SB-8 (7')SB-9 (16')SB-9 (6')SB-10 (10')SB-10 (17')
12/15/2011 12/15/2011 12/15/2011 12/15/2011 12/15/2011 12/15/2011 12/15/2011 12/15/2011 12/15/2011 12/15/2011 12/15/2011 12/15/2011 12/15/2011 12/15/2011 12/15/2011
7 16 6 13 17 10 17 16 7 16 7 16 6 10 17
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 <0.145 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 <0.0052 <0.0057
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 <0.145 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 0.0052 0.0095
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 0.542 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 0.0391 0.0106
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 <0.145 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 <0.0052 <0.0057
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 <0.145 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 <0.0052 <0.0057
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 <0.145 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 0.0094 <0.0057
<0.041 <0.049 <0.047 <0.046 <0.043 <0.053 <0.050 <1.45 <1.14 <0.049 <0.048 <0.054 <0.043 <0.052 <0.057
------------------------------
------------------------------
------------------------------
------------------------------
------------------------------
------------------------------
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 <0.145 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 <0.0052 <0.0057
0.0053 <0.0049 0.0049 <0.0046 <0.0043 <0.0053 <0.0050 <0.145 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 <0.0052 <0.0057
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 <0.145 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 <0.0052 <0.0057
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 <0.145 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 <0.0052 <0.0057
0.0780 0.0454 0.0542 <0.0046 <0.0043 0.0184 <0.0050 0.584 0.808 <0.0049 0.0055 <0.0054 <0.0043 0.0065 0.0067
<0.016 <0.020 <0.019 <0.018 <0.017 <0.021 <0.020 <0.581 <0.458 <0.020 <0.019 <0.021 <0.017 <0.021 <0.023
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 0.511 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 0.0805 <0.0057
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 0.321 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 <0.0052 <0.0057
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 <0.145 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 <0.0052 <0.0057
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 <0.145 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 <0.0052 <0.0057
<0.0082 <0.0098 <0.0094 <0.0092 <0.0085 <0.011 <0.010 <0.291 <0.229 <0.0098 <0.0095 <0.011 <0.0087 <0.010 <0.011
<0.0082 <0.0098 <0.0094 <0.0092 <0.0085 <0.011 <0.010 <0.291 <0.229 <0.0098 <0.0095 <0.011 <0.0087 0.0314 0.0423
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 0.330 <0.114 0.0112 0.0087 <0.0054 <0.0043 0.0535 0.0856
<0.0082 <0.0098 <0.0094 <0.0092 <0.0085 <0.011 <0.010 <0.291 <0.229 <0.0098 <0.0095 <0.011 <0.0087 0.0195 0.0260
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 0.172 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 0.0053 <0.0057
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 <0.145 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 <0.0052 <0.0057
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 <0.145 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 0.0119 0.0163
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 <0.145 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 0.0074 <0.0057
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 <0.145 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 <0.0052 <0.0057
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 <0.145 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 <0.0052 <0.0057
<0.0041 <0.0049 <0.0047 <0.0046 <0.0043 <0.0053 <0.0050 <0.145 <0.114 <0.0049 <0.0048 <0.0054 <0.0043 <0.0052 <0.0057
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Prepared By/Date:
Checked By/Date:
AJF 4-5-12
MPF 11-9-12
3 of 3
TABLE 5
Summary of Laboratory Analyses - Groundwater Samples (February 2009 - June 2014)
Southern Pump and Tank Company4800 North Graham Street, Charlotte, North CarolinaAMEC Project:6228-13-0135
Constituent
Date Collected 2/6/2009 1/22/2010 12/28/2011 10/15/2012 8/8/2013 6/11/2014 2/6/2009 1/25/2010 12/23/2011 10/17/2012 8/8/2013 6/10/2014 5/22/2009 1/21/2010 12/23/2011 10/16/2012 8/7/2013 6/11/2014 1/21/2010 12/20/2011 10/17/2012 8/8/2013 6/10/2014 5/22/2009 1/22/2010 12/22/2011 10/2012 8/8/13 6/11/2014 5/22/2009 1/25/2010 12/28/2011 10/2012 8/8/13 6/11/2014
VOCs by SM 6200B
tert-Amyl Alcohol NSL NSL ----<40000 687 <25000 <50000 ----<1000 <1000 <500 <500 ----72300 65500 96100 71800 --<100 <100 <100 <100 ----<200 NS <100 <100 ----<2500 NS <500 <1000tert-Amylmethyl ether NSL NSL ----<4000 <50.0 <2500 <5000 ----137 <100 <50.0 <50.0 ----<1000 <250 <1000 <1000 --<10.0 <10.0 <10.0 <10.0 ----<20.0 NS <10.0 <10.0 ----<250 NS <50.0 <100Benzene15,000 733 651 763 745 690 725 100 1070 1160 270 220 187 10800 12200 14700 10500 14000 14000 <0.50 <0.50 1.6 1.2 <0.50 --0.77 <1.0 NS <0.50 <0.50 84.7 78.1 51.1 NS 51.3 41.9BromobenzeneNSLNSL<10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.0BromochloromethaneNSLNSL<10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.0Bromodichloromethane0.6 NSL <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.0Bromoform44,000 <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.0BromomethaneNSLNSL<50.0 <25.0 <2000 <25.0 <1250 <2500 <10.0 <50.0 <50.0 <50.0 <25.0 <25.0 <100 <25.0 <500 <125 <500 <500 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <5.0 <10.0 NS <5.0 <5.0 <50.0 <5.0 <125 NS <25.0 <50.0tert-Butyl Alcohol NSL NSL ----<4000 97.9 <2500 <5000 ----<100 265 68.0 259 ----<1000 1550 2420 1960 --<10.0 <10.0 <10.0 <10.0 ----<20.0 NS <10.0 <10.0 ----<250 NS <50.0 <100n-Butylbenzene 70 6,900 --<2.5 <200 <2.5 <125 <250 --<5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.0sec-Butylbenzene 70 8,500 --<2.5 <200 2.5 <125 <250 --<5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.0tert-Butylbenzene 70 15,000 --<2.5 <200 <2.5 <125 <250 --<5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.0tert-Butyl Formate NSL NSL ----<8000 <100 <5000 <10000 ----<200 <200 <100 <100 ----<2000 <500 <2000 <2000 --<20.0 <20.0 <20.0 <20.0 ----<40.0 NS <20.0 <20.0 ----<500 NS <100 <200Carbon tetrachloride 0.3 NSL <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.0Chlorobenzene5050,000 <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 <25.0 1.2 <12.5 NS <2.5 <5.0Chloroethane3,000 NSL <10.0 <5.0 <400 <5.0 <250 <500 <2.0 <10.0 <10.0 <10.0 <5.0 <5.0 <100 <5.0 <100 <25.0 <100 <100 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 NS <1.0 <1.0 <50.0 <1.0 <25.0 NS <5.0 <10.0Chloroform7070,000 <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 124 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 62.2 <0.50 <12.5 NS <2.5 <5.0
Chloromethane 3 3,000 <10.0 <5.0 <400 <5.0 <250 <500 <2.0 <10.0 <10.0 <10.0 <5.0 <5.0 <100 <5.0 <100 <25.0 <100 <100 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 NS <1.0 <1.0 <50.0 <1.0 <25.0 NS <5.0 <10.02-Chlorotoluene 100 NSL <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.04-Chlorotoluene NSL NSL <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.01,2-Dibromo-3-chloropropane 0.04 NSL <30.0 <5.0 <400 <5.0 <250 <500 <6.0 <10.0 <10.0 <10.0 <5.0 <5.0 <100 <5.0 <100 <25.0 <100 <100 <1.0 <1.0 <1.0 <1.0 <1.0 --<1.0 <2.0 NS <1.0 <1.0 <50.0 <1.0 <25.0 NS <5.0 <10.0Dibromochloromethane0.4 400 <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.01,2-Dibromoethane (EDB)0.02 50 <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.0DibromomethaneNSLNSL<10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.01,2-Dichlorobenzene 20 20,000 <10.0 6.4 <200 7.2 <125 <250 6.3 5.5 <5.0 <5.0 <2.5 <2.5 <50.0 13.1 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 26.1 29.8 21.1 NS 31.7 25.4
1,3-Dichlorobenzene 200 25,000 <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 <25.0 3.7 <12.5 NS 3.7 <5.01,4-Dichlorobenzene 6 6,000 <10.0 <2.5 <200 <2.5 <125 <250 2.5 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 3.4 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 1.5 0.95 <1.0 NS <0.50 <0.50 <25.0 7.4 <12.5 NS 7.5 6.8Dichlorodifluoromethane1,000 140,000 <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.01,1-Dichloroethane 6 6,000 <10.0 6.2 <200 8.8 <125 <250 <2.0 45.9 22.2 17.7 3.8 23.6 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 <25.0 5.6 <12.5 NS 2.7 <5.01,2-Dichloroethane 0.4 400 121 103 <200 111 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 618 695 869 625 894 752 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 0.59 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.01,1-Dichloroethene 7 7,000 23.0 9.3 <200 25.0 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 3.4 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 <25.0 3.2 <12.5 NS <2.5 <5.0cis-1,2-Dichloroethene 70 70,000 44800 40100 37200 42800 45200 43500 396 1770 187 <5.0 3.5 33.4 560 3440 3850 2300 3040 3020 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 13.2 <1.0 NS 8.1 <0.50 3980 2920 1970 NS 1810 979trans-1,2-Dichloroethene 100 100,000 44.4 460 <200 111 <125 <250 2.7 6.9 <5.0 <5.0 <2.5 <2.5 <50.0 4.0 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 <25.0 29.5 <12.5 NS <2.5 <5.01,2-Dichloropropane 0.6 600 <10.0 5.7 <200 7.1 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 54.7 70.8 47.5 64.3 65.5 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.01,3-Dichloropropane NSL NSL <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.02,2-Dichloropropane NSL NSL <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.01,1-Dichloropropene NSL NSL <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.0cis-1,3-Dichloropropene 0.4 400 <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.0trans-1,3-Dichloropropene 0.4 400 <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.0Diisopropyl ether 70 70,000 54900 79.1 <200 79.4 <125 <250 16.0 120 49.6 22.6 6.1 24.5 110 119 141 102 148 113 <0.50 <0.50 <0.50 <0.50 <0.50 --1.0 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.0EthanolNSLNSL----<4000 --<50000 <100000 ----<100 --<1000 <1000 <20000 --<1000 --<20000 <20000 --<10.0 <10.0 <200 <200 ----<20.0 NS <200 <200 <10000 --<250 NS <1000 <2000Ethylbenzene60084,500 197 198 <200 181 135 <250 31.9 305 241 194 87.1 26.3 211 185 490 296 728 631 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 57.4 119 71.9 NS 171 134
Hexachloro-1,3-butadiene NSL NSL <10.0 <10.0 <800 <10.0 <500 <1000 <2.0 <20.0 <20.0 <20.0 <10.0 <10.0 <200 <10.0 <200 <50.0 <200 <200 <2.0 <2.0 <2.0 <2.0 <2.0 --<2.0 <4.0 NS <2.0 <2.0 <100 <2.0 <50.0 NS <10.0 <20.0Isopropylbenzene (Cumene)70 25,000 --18.3 <200 16.4 <125 <250 --19.2 21.9 34.7 6.9 7.9 <50.0 28.6 <50.0 25.2 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 <25.0 29.1 14.4 NS 22.9 17.9Methylene Chloride 5 5,000 74.8 56.9 <800 66.7 <500 <1000 9.7 <20.0 33.8 <20.0 13.1 <10.0 483 <10.0 449 <50.0 <200 <200 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <4.0 NS <2.0 <2.0 210 <2.0 <50.0 NS <10.0 <20.0Methyl-tert-butyl ether 20 20,000 <10.0 <2.5 <200 <2.5 <125 <250 68.3 2440 1080 583 126 422 <50.0 6.0 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.0Naphthalene66,000 544 348 <800 408 <500 <1000 170 366 166 192 62.3 42.4 652 381 <200 157 347 336 <2.0 <2.0 <2.0 <2.0 <2.0 --<40.0 <4.0 NS <2.0 <2.0 470 433 344 NS 409 312n-Propylbenzene 70 30,000 --31.6 <200 26.2 <125 <250 --39.7 30.0 67.9 17.7 14.7 60.8 51.9 <50.0 49.8 73.9 84.2 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 34.0 38.4 17.4 NS 36.1 26.4Styrene7070,000 <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.01,1,1,2-Tetrachloroethane NSL NSL <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.01,1,2,2-Tetrachloroethane 0.2 200 <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.0Tetrachloroethene0.7 700 1260 1540 1160 977 <125 292 153 10.7 <5.0 <5.0 <2.5 <2.5 1230 61.5 <50.0 18.3 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 238 427 188 NS 377 343 963 219 <12.5 NS 73.3 21.3Toluene600260,000 224 222 <200 190 152 393 41.7 1540 132 10 55.2 12.3 938 100 431 324 589 429 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 <25.0 12.6 <12.5 NS 8.2 <5.01,2,3-Trichlorobenzene NSL NSL <10.0 <10.0 <800 <10.0 <500 <1000 <2.0 <20.0 <20.0 <20.0 <10.0 <10.0 <200 <10.0 <200 <50.0 <200 <200 <2.0 <2.0 <2.0 <2.0 <2.0 --<2.0 <4.0 NS <2.0 <2.0 <100 <2.0 <50.0 NS <10.0 <20.01,2,4-Trichlorobenzene 70 70,000 <10.0 <10.0 <800 <10.0 <500 <1000 3.9 <20.0 <20.0 <20.0 <10.0 <10.0 <200 <10.0 <200 <50.0 346 <200 <2.0 <2.0 <2.0 <2.0 <2.0 --<2.0 <4.0 NS <2.0 <2.0 <100 2.7 <50.0 NS <10.0 <20.01,1,1-Trichloroethane 200 200,000 <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.01,1,2-Trichloroethane NSL NSL <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 <0.50 <1.0 NS <0.50 <0.50 <25.0 0.70 <12.5 NS <2.5 <5.0Trichloroethene33,000 281 292 333 444 <125 <250 20.3 <5.0 <5.0 <5.0 <2.5 <2.5 119 27.0 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 9.0 7.0 5.2 NS 7.3 6.7 44.2 34.9 <12.5 NS 12.8 <5.0Trichlorofluoromethane2,000 2,000,000 <10.0 <5.0 <400 <5.0 <250 <500 <2.0 <10.0 <10.0 <10.0 <5.0 <5.0 <100 <5.0 <100 <25.0 <100 <100 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 NS <1.0 <1.0 <50.0 <1.0 <25.0 NS <5.0 <10.01,2,3-Trichloropropane 0.005 NSL <10.0 <2.5 <200 <2.5 <125 <250 <2.0 <5.0 <5.0 <5.0 <2.5 <2.5 <50.0 <2.5 <50.0 <12.5 <50.0 <50.0 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 <25.0 <0.50 <12.5 NS <2.5 <5.01,2,4-Trimethylbenzene 400 28,500 --322 <200 316 214 <250 --541 357 678 265 164 310 150 122 71.2 <200 286 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 463 452 247 NS 434 3321,3,5-Trimethylbenzene 400 25,000 --94.7 <200 96.4 <125 <250 --439 122 283 131 62.0 121 124 86.4 71.3 159 155 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 <25.0 81.8 31.9 NS 89.2 30.2Vinyl chloride 0.03 30 <10.0 6.3 <400 5.6 <250 <500 80.2 944 51.4 <10.0 <5.0 10.9 <100 18.1 <100 <25.0 <100 <100 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 NS <1.0 <1.0 377 504 295 NS 276 221m&p-Xylene 500 85,500 574 459 <400 242 <250 <500 139 1320 738 646 558 86.7 817 179 678 306 1360 1140 <1.0 <1.0 <1.0 <1.0 <1.0 --<1.0 <2.0 NS <1.0 <1.0 187 186 89.9 NS 155 89.8o-Xylene 500 85,500 396 355 296 362 230 <250 76.1 666 127 6.3 40.8 <2.5 269 21.6 114 63.0 256 215 <0.50 <0.50 <0.50 <0.50 <0.50 --<0.50 <1.0 NS <0.50 <0.50 211 93.5 37.0 NS 63.1 31.7EPH by MADEP MethodsAliphatic (C09-C18)700 NSL <122 314 --103 192 1140 <119 228 --400 185 378 <118 <143 --1220 <100 <100 <133 --<100 <100 <100 <116 <143 --NS <111 <100 --168 --NS 164 139
Aliphatic (C19-C36)10,000 NSL <122 <122 --<100 <100 <100 <119 <167 --213 <100 126 <118 <143 --<200 <100 <100 <133 --<100 <100 <100 <116 <143 --NS <111 <100 --<125 --NS <100 <100Aromatic (C11-C22)200 NSL 1030 1280 --631 1010 1210 552 1000 --222 327 667 1090 1060 --909 890 658 <133 --<100 <100 <100 <116 <143 --NS <111 <100 --1290 --NS 1750 770VPH by MADEP MethodsAliphatic (C05-C08)400 NSL 3420 4230 --3540 2980 52300 495 7810 --2990 915 740 26800 27700 --32600 56000 71700 836 --<50.0 <50.0 <50.0 153 134 --NS 112 229 824 596 --NS 321 1080
Aliphatic (C09-C12)700 NSL 5820 9540 --3300 2900 <10000 2130 14600 --7520 3100 1430 10700 7280 --2940 11900 <10000 134 --<50.0 <50.0 <50.0 <100 <100 --NS <50.0 <50.0 4730 5990 --NS 2460 1920Aromatic (C09-C10)200 NSL 1340 1410 --990 836 <10000 632 1750 --2360 871 625 1930 1290 --<2500 <5000 <10000 <100 --<50.0 <50.0 <50.0 <100 <100 --NS <50.0 <50.0 1280 1280 --NS 996 748Metals by EPA Method 6010/3030CChromium 10 10,000 -- -- --<5.0 9.6 6.0 -- -- --11.7 <5.0 <5.0 -- -- --69.9 <5.0 <5.0 -- --<5.0 <5.0 23.6 -- -- --NS 6.9 <5.0 -- -- --NS <5.0 <5.0Lead1515,000 5.2 5.3 --11.4 8.0 <5.0 <5.0 5.1 --21.0 <5.0 <5.0 <5.0 5.2 --9.3 <5.0 <5.0 7.0 --<5.0 <5.0 <5.0 --<5.0 --NS <5.0 <5.0 <5.0 <5.0 --NS <5.0 <5.0
MW-6NC 2LStandards GCLs MW-1 MW-2 MW-3 MW-4 MW-5
1 of 3 Prepared by/Date: MDF 6/26/14Checked by/Date: BH 6/26/14
TABLE 5
Summary of Laboratory Analyses - Groundwater Samples (February 2009 - June 2014)
Southern Pump and Tank Company4800 North Graham Street, Charlotte, North CarolinaAMEC Project:6228-13-0135
Constituent
Date Collected
VOCs by SM 6200B
tert-Amyl Alcohol NSL NSLtert-Amylmethyl ether NSL NSLBenzene15,000BromobenzeneNSLNSL
Bromochloromethane NSL NSLBromodichloromethane0.6 NSLBromoform44,000BromomethaneNSLNSLtert-Butyl Alcohol NSL NSLn-Butylbenzene 70 6,900sec-Butylbenzene 70 8,500tert-Butylbenzene 70 15,000tert-Butyl Formate NSL NSLCarbon tetrachloride 0.3 NSLChlorobenzene5050,000Chloroethane3,000 NSLChloroform7070,000
Chloromethane 3 3,0002-Chlorotoluene 100 NSL4-Chlorotoluene NSL NSL1,2-Dibromo-3-chloropropane 0.04 NSL
Dibromochloromethane 0.4 4001,2-Dibromoethane (EDB)0.02 50DibromomethaneNSLNSL1,2-Dichlorobenzene 20 20,000
1,3-Dichlorobenzene 200 25,0001,4-Dichlorobenzene 6 6,000Dichlorodifluoromethane1,000 140,0001,1-Dichloroethane 6 6,000
1,2-Dichloroethane 0.4 4001,1-Dichloroethene 7 7,000cis-1,2-Dichloroethene 70 70,000trans-1,2-Dichloroethene 100 100,0001,2-Dichloropropane 0.6 6001,3-Dichloropropane NSL NSL2,2-Dichloropropane NSL NSL1,1-Dichloropropene NSL NSLcis-1,3-Dichloropropene 0.4 400trans-1,3-Dichloropropene 0.4 400Diisopropyl ether 70 70,000EthanolNSLNSLEthylbenzene60084,500
Hexachloro-1,3-butadiene NSL NSLIsopropylbenzene (Cumene)70 25,000Methylene Chloride 5 5,000Methyl-tert-butyl ether 20 20,000
Naphthalene 6 6,000n-Propylbenzene 70 30,000Styrene7070,0001,1,1,2-Tetrachloroethane NSL NSL
1,1,2,2-Tetrachloroethane 0.2 200Tetrachloroethene0.7 700Toluene600260,0001,2,3-Trichlorobenzene NSL NSL
1,2,4-Trichlorobenzene 70 70,0001,1,1-Trichloroethane 200 200,0001,1,2-Trichloroethane NSL NSLTrichloroethene33,000Trichlorofluoromethane2,000 2,000,0001,2,3-Trichloropropane 0.005 NSL1,2,4-Trimethylbenzene 400 28,5001,3,5-Trimethylbenzene 400 25,000Vinyl chloride 0.03 30m&p-Xylene 500 85,500o-Xylene 500 85,500EPH by MADEP MethodsAliphatic (C09-C18)700 NSL
Aliphatic (C19-C36)10,000 NSLAromatic (C11-C22)200 NSLVPH by MADEP MethodsAliphatic (C05-C08)400 NSL
Aliphatic (C09-C12)700 NSLAromatic (C09-C10)200 NSLMetals by EPA Method 6010/3030CChromium 10 10,000Lead1515,000
NC 2LStandards GCLs 5/22/2009 1/22/2010 12/22/2011 10/16/2012 8/7/2013 6/10/2014 1/22/2010 12/22/2011 10/2012 8/7/13 6/10/2014 1/21/2010 12/23/2011 10/16/2012 87/13 6/10/2014 1/21/2010 12/22/2011 10/17/2012 8/7/2013 6/11/2014 1/22/2010 12/28/2011 10/16/2012 8/7/2013 6/10/2014 1/22/2010 12/29/2011 10/16/2012 8/7/2013 6/10/2014 1/22/2010 12/29/2011 10/15/2012 8/8/2013 6/11/2014
----<100 <100 <100 <100 --<200 NS <100 <100 --<100 <100 <100 <100 --7530 7610 13700 10300 --<100 <100 <100 <100 --<250 <5000 NS NS --<250 <100 <250 <100----<10.0 <10.0 <10.0 <10.0 --<20.0 NS <10.0 <10.0 --<10.0 <10.0 <10.0 <10.0 --<250 <250 <200 <100 --<10.0 <10.0 <10.0 <10.0 --<25.0 <500 NS NS --<25.0 <10.0 <25.0 <10.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.83 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 2770 3650 2620 4660 2720 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 15.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10.0 NS <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <100 <125 <125 <100 <50.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <12.5 <250 NS NS <12.5 <12.5 <5.0 <12.5 <5.0----<10.0 <10.0 <10.0 <10.0 --<20.0 NS <10.0 <10.0 --<10.0 <10.0 <10.0 <10.0 --<250 <250 <200 129 --<10.0 <10.0 <10.0 <10.0 --<25.0 <500 NS NS --<25.0 <10.0 <25.0 <10.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 7.6 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 77.8 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50----<20.0 <20.0 <20.0 <20.0 --<40.0 NS <20.0 <20.0 --<20.0 <20.0 <20.0 <20.0 --<500 <500 <400 <200 --<20.0 <20.0 <20.0 <20.0 --<50.0 <1000 NS NS --<50.0 <20.0 <50.0 <20.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <20.0 <25.0 <25.0 <20.0 <10.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.5 <50.0 NS NS <2.5 <2.5 <1.0 <2.5 <1.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50
<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <20.0 <25.0 <25.0 <20.0 <10.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.5 <50.0 NS NS <2.5 <2.5 <1.0 <2.5 <1.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <20.0 <25.0 <25.0 <20.0 <10.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.5 <50.0 NS NS <2.5 <2.5 <1.0 <2.5 <1.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.52 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 11.6 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 45.6 55.1 46.5 66.2 43.2 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <1.0 NS <0.50 <0.50 2.2 1.8 1.9 1.2 0.73 25.0 516 506 792 555 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 8.2 <25.0 NS NS <1.2 3.8 <0.50 3.5 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 14.1 12.8 16.8 12.7 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 15.2 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<200 --<10.0 <10.0 <200 <200 --<20.0 NS <200 <200 --<10.0 <10.0 <200 <200 --<250 --<4000 <2000 --<10.0 --<200 <200 --<25.0 --NS NS --<25.0 --<500 <200<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 372 406 358 838 514 <0.50 <0.50 <0.50 <0.50 <0.50 0.51 70.7 111 NS NS <1.2 <1.2 6.5 <1.2 <0.50
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <4.0 NS <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <40.0 <50.0 <50.0 <40.0 <20.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <5.0 <100 NS NS <5.0 <5.0 <2.0 <5.0 <2.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 23.5 17.8 31.2 39.6 33.8 <0.50 <0.50 <0.50 <0.50 <0.50 0.51 14.0 34.7 NS NS <1.2 <1.2 1.9 <1.2 <0.50<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <4.0 NS <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <40.0 102 <50.0 <40.0 <20.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <5.0 <100 NS NS <5.0 <5.0 <2.0 <5.0 <2.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <40.0 <4.0 NS <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 119 91.2 58.2 225 108 <2.0 <2.0 <2.0 <2.0 <2.0 2.3 159 335 NS NS <5.0 <5.0 18.5 <5.0 <2.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 41.1 28.7 41.8 81.2 58.6 <0.50 <0.50 <0.50 <0.50 <0.50 0.71 18.3 66.5 NS NS <1.2 <1.2 3.3 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 0.86 <0.50 <0.50 535 212 NS 178 241 6.2 19.3 27.8 105 123 252 <12.5 <12.5 <10.0 <5.0 10.0 3.1 1.9 1.6 1.5 124 40.2 68.3 NS NS 365 496 330 592 431<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 437 47.2 52.0 123 71.4 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 132 139 NS NS <1.2 <1.2 5.7 <1.2 <0.50<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <4.0 NS <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <40.0 <50.0 <50.0 <40.0 <20.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <5.0 <100 NS NS <5.0 <5.0 <2.0 <5.0 <2.0<2.0 <2.0 <2.0 <2.0 <0.50 <2.0 <2.0 <4.0 NS <0.50 <2.0 <2.0 <2.0 <2.0 <0.50 <2.0 <40.0 <50.0 <50.0 231 <20.0 <2.0 <2.0 <2.0 <0.50 <2.0 <2.0 <5.0 <100 NS NS <5.0 <5.0 <2.0 <5.0 <2.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 11.0 5.9 NS 3.9 4.5 <0.50 <0.50 <0.50 <0.50 <0.50 18.7 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 0.72 1.5 <25.0 NS NS 2.3 3.1 2.3 3.1 2.6<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <20.0 <25.0 <25.1 <20.0 <10.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.5 <50.0 NS NS <2.5 <2.5 <1.0 <2.5 <1.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <10.0 <12.5 <12.5 <10.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.2 <25.0 NS NS <1.2 <1.2 <0.50 <1.2 <0.501.3 <0.50 <0.50 <0.50 <2.0 <0.50 0.53 <1.0 NS <2.0 <0.50 <0.50 0.90 <0.50 <2.0 <0.50 212 54.4 28.2 <40.0 53.0 <0.50 <0.50 <0.50 <2.0 <0.50 10.3 241 738 NS NS <1.2 4.7 35.2 <1.2 <0.500.61 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 70.5 23.5 21.9 78.9 29.6 <0.50 <0.50 <0.50 <0.50 <0.50 4.4 59.9 221 NS NS <1.2 1.8 10.4 <1.2 <0.50<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.0 <2.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <20.0 <25.0 <25.0 <20.0 <10.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.5 <50.0 NS NS <2.5 <2.5 <1.0 <2.5 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 NS <1.0 <1.0 <1.0 1.6 <1.0 <1.0 <1.0 565 84.5 56.8 537 129 <1.0 <1.0 <1.0 <1.0 <1.0 4.3 296 508 NS NS <2.5 <2.5 28.7 <2.5 <1.00.77 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 855 17.4 15.2 92.6 51.0 <0.50 <0.50 <0.50 <0.50 <0.50 4.9 222 327 NS NS <1.2 <1.2 18.2 <1.2 <0.50
--<125 --<100 <100 <100 <125 --NS <100 <100 <125 --<100 <100 <100 <133 --<100 <110 <100 <133 --<100 <100 <100 <125 --3,510,000,000 NS NS <118 --3660 <100 <100
--<125 --<100 <100 <100 <125 --NS <100 <100 <125 --<100 <100 <100 <133 --<100 <110 <100 <133 --<100 <100 <100 <125 --153,000,000 NS NS <118 --<400 <100 <100--<125 --<100 <100 <100 <125 --NS <100 <100 <125 --<100 <100 <100 255 --102 499 188 <133 --<100 <100 <100 <125 --458,000,000 NS NS <118 --995 <100 <100
<100 <100 --<50.0 <50.0 <50.0 156 --NS 60.7 164 <100 --<50.0 <50.0 60.9 7050 --10900 15500 20300 <100 --<50.0 <50.0 <50.0 <100 --362 NS NS 109 --166 191 241<100 <100 --<50.0 <50.0 <50.0 <100 --NS <50.0 <50.0 <100 --<50.0 <50.0 <50.0 10900 --2340 4870 2120 <100 --<50.0 <50.0 <50.0 <100 --5350 NS NS <100 --311 <50.0 <50.0<100 <100 --<50.0 <50.0 <50.0 <100 --NS <50.0 <50.0 <100 --<50.0 <50.0 <50.0 1040 --<1250 <1000 <1250 <100 --<50.0 <50.0 <50.0 <100 --1790 NS NS <100 --143 <50.0 <50.0
-- -- --5.7 <5.0 <5.0 -- --NS 26.9 <5.0 -- --<5.0 <5.0 11.5 -- --<5.0 <5.0 <5.0 -- --<5.0 7.1 <5.0 -- --<5.0 NS NS -- --1800 <5.0 <5.0<5.0 <5.0 --<5.0 <5.0 <5.0 24.0 --NS <5.0 <5.0 <5.0 --<5.0 <5.0 <5.0 <5.0 --<5.0 <5.0 <5.0 <5.0 --<5.0 <5.0 <5.0 5.2 --<5.0 NS NS <5.0 --<5.0 <5.0 <5.0
MW-7 MW-8 MW-9 MW-11 MW-12*MW-13MW-10
2 of 3 Prepared by/Date: MDF 6/26/14Checked by/Date: BH 6/26/14
TABLE 5
Summary of Laboratory Analyses - Groundwater Samples (February 2009 - June 2014)
Southern Pump and Tank Company4800 North Graham Street, Charlotte, North CarolinaAMEC Project:6228-13-0135
Constituent
Date Collected
VOCs by SM 6200B
tert-Amyl Alcohol NSL NSLtert-Amylmethyl ether NSL NSLBenzene15,000BromobenzeneNSLNSL
Bromochloromethane NSL NSLBromodichloromethane0.6 NSLBromoform44,000BromomethaneNSLNSLtert-Butyl Alcohol NSL NSLn-Butylbenzene 70 6,900sec-Butylbenzene 70 8,500tert-Butylbenzene 70 15,000tert-Butyl Formate NSL NSLCarbon tetrachloride 0.3 NSLChlorobenzene5050,000Chloroethane3,000 NSLChloroform7070,000
Chloromethane 3 3,0002-Chlorotoluene 100 NSL4-Chlorotoluene NSL NSL1,2-Dibromo-3-chloropropane 0.04 NSL
Dibromochloromethane 0.4 4001,2-Dibromoethane (EDB)0.02 50DibromomethaneNSLNSL1,2-Dichlorobenzene 20 20,000
1,3-Dichlorobenzene 200 25,0001,4-Dichlorobenzene 6 6,000Dichlorodifluoromethane1,000 140,0001,1-Dichloroethane 6 6,000
1,2-Dichloroethane 0.4 4001,1-Dichloroethene 7 7,000cis-1,2-Dichloroethene 70 70,000trans-1,2-Dichloroethene 100 100,0001,2-Dichloropropane 0.6 6001,3-Dichloropropane NSL NSL2,2-Dichloropropane NSL NSL1,1-Dichloropropene NSL NSLcis-1,3-Dichloropropene 0.4 400trans-1,3-Dichloropropene 0.4 400Diisopropyl ether 70 70,000EthanolNSLNSLEthylbenzene60084,500
Hexachloro-1,3-butadiene NSL NSLIsopropylbenzene (Cumene)70 25,000Methylene Chloride 5 5,000Methyl-tert-butyl ether 20 20,000
Naphthalene 6 6,000n-Propylbenzene 70 30,000Styrene7070,0001,1,1,2-Tetrachloroethane NSL NSL
1,1,2,2-Tetrachloroethane 0.2 200Tetrachloroethene0.7 700Toluene600260,0001,2,3-Trichlorobenzene NSL NSL
1,2,4-Trichlorobenzene 70 70,0001,1,1-Trichloroethane 200 200,0001,1,2-Trichloroethane NSL NSLTrichloroethene33,000Trichlorofluoromethane2,000 2,000,0001,2,3-Trichloropropane 0.005 NSL1,2,4-Trimethylbenzene 400 28,5001,3,5-Trimethylbenzene 400 25,000Vinyl chloride 0.03 30m&p-Xylene 500 85,500o-Xylene 500 85,500EPH by MADEP MethodsAliphatic (C09-C18)700 NSL
Aliphatic (C19-C36)10,000 NSLAromatic (C11-C22)200 NSLVPH by MADEP MethodsAliphatic (C05-C08)400 NSL
Aliphatic (C09-C12)700 NSLAromatic (C09-C10)200 NSLMetals by EPA Method 6010/3030CChromium 10 10,000Lead1515,000
NC 2LStandards GCLs 1/25/2010 12/29/2011 10/17/2012 8/8/2013 6/11/2014 1/25/2010 12/29/2011 10/17/2012 8/8/2013 6/11/2014 4/26/2011 12/20/2011 10/16/2012 8/7/2013 6/10/2014 4/26/2011 12/28/2011 10/17/2012 8/7/2013 6/10/2014 4/26/2011 12/23/2011 10/16/2012 8/7/2013 6/10/2014 1/22/2010 12/23/2011 10/15/2012 8/7/2013 6/10/2014 4/26/2011 12/20/2011 10/15/2012 8/7/2013 6/10/2014
--<100 <100 <100 <100 --<100 <100 <100 <100 --<100 <100 <100 <100 --<100 <100 <100 <100 --<100 <100 <100 <100 --<100 <100 <100 <100 --<100 <100 <100 <100--<10.0 <10.0 <10.0 <10.0 --<10.0 <10.0 <10.0 <10.0 --<10.0 <10.0 <10.0 <10.0 --<10.0 <10.0 <10.0 <10.0 --<10.0 <10.0 <10.0 <10.0 --<10.0 <10.0 <10.0 <10.0 --<10.0 <10.0 <10.0 <10.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5.5 2.2 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 6.0 <0.50 0.74 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.1 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0--<10.0 <10.0 <10.0 <10.0 --<10.0 <10.0 <10.0 <10.0 --<10.0 <10.0 <10.0 <10.0 --<10.0 <10.1 <10.0 <10.0 --<10.0 <10.0 <10.0 <10.0 --<10.0 <10.0 <10.0 <10.0 --<10.0 <10.0 <10.0 <10.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.51 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50--<20.0 <20.0 <20.0 <20.0 --<20.0 <20.0 <20.0 <20.0 --<20.0 <20.0 <20.0 <20.0 --<20.0 <20.0 <20.0 <20.0 --<20.0 <20.0 <20.0 <20.0 --<20.0 <20.0 <20.0 <20.0 --<20.0 <20.0 <20.0 <20.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 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<0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5.8 2.7 5.1 3.5 3.0 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 2.8 3.1 4.1 4.0 4.8 <0.50 <0.50 <0.50 <0.50 <0.50 135 31.4 118 53.2 49.2 <0.50 <0.50 13.7 3.5 1.7<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.68 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.59 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 1.4 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50--<10.0 <10.0 <200 <200 --<10.0 <10.0 <200 <200 --<10.0 --<200 <200 --<10.0 <10.0 <200 <200 --<10.0 <10.0 <200 <200 --<10.0 --<200 <200 --<10.0 --<200 <200<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 1.1 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.55 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 85.5 74.6 71.3 25.4 0.78 0.62 1.0 <0.50 1.9 1.2 0.88 1.3 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.505.6 3.0 15.6 2.4 0.67 <0.50 <0.50 <0.50 <0.50 <0.50 0.71 0.55 0.87 0.79 0.98 7.1 5.0 7.1 5.8 8.2 8.3 5.0 6.7 2.5 2.7 108 24.9 73.4 55.4 53.7 <0.50 <0.50 1.4 0.90 0.51<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 1.3 <0.50<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <0.50 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <0.50 <0.50 <2.0 <2.0 <2.0 <2.0 <0.50 <2.0 <2.0 <2.0 <2.0 <0.50 <2.0 <2.0 <2.0 <2.0 <0.50 <2.0 <2.0 <2.0 <2.0 <0.50 <2.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 8.1 7.2 8.2 7.0 9.8 <0.50 <0.50 <0.50 <0.50 <0.50 8.3 2.9 6.6 4.1 3.8 <0.50 <0.50 <0.50 <0.50 <0.50<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 2.4 <2.0 <0.50 <0.50 <0.50 1.1 <2.0 <0.50<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 1.1 <0.50 1.0 <0.50 <0.50 <0.50 <0.50 0.54 <0.50 <0.50
<125 --<100 <100 <100 <133 --<100 <100 <100 ----<100 <100 <100 ----<100 <111 <100 ----<100 <100 <100 <167 --<100 <111 <100 ----<100 <100 <100
<125 --<100 <100 <100 <133 --<100 <100 <100 ----<100 <100 <100 ----<100 <111 <100 ----<100 <100 <100 <167 --<100 <111 <100 ----<100 <100 <100<125 --<100 <100 <100 <133 --<100 <100 <100 ----<100 <100 <100 ----<100 <111 <100 ----<100 <100 <100 <167 --<100 <111 <100 ----<100 <100 <100
<100 --<50.0 <50.0 <50.0 <100 --<50.0 <50.0 <50.0 ----52.4 <50.0 <50.0 ----<50.0 <50.0 <50.0 ----<50.0 <50.0 <50.0 <100 --<50.0 <50.0 77.2 ----<50.0 <50.0 <50.0<100 --<50.0 <50.0 <50.0 <100 --<50.0 <50.0 <50.0 ----<50.0 <50.0 <50.0 ----<50.0 <50.0 <50.0 ----<50.0 <50.0 <50.0 <100 --<50.0 <50.0 <50.0 ----<50.0 <50.0 <50.0<100 --<50.0 <50.0 <50.0 <100 --<50.0 <50.0 <50.0 ----<50.0 <50.0 <50.0 ----<50.0 <50.0 <50.0 ----<50.0 <50.0 <50.0 <100 --<50.0 <50.0 <50.0 ----<50.0 <50.0 <50.0
-- --<5.0 <5.0 48.7 -- --42.8 <5.0 <5.0 -- --<5.0 <5.0 10.9 -- --<5.0 <5.0 <5.0 -- --<5.0 <5.0 <5.0 -- --78.8 10.3 64.6 -- --9.5 23.0 5.7<5.0 --<5.0 <5.0 21.4 <5.0 --25.8 <5.0 <5.0 <5.0 --<5.0 <5.0 <5.0 31.6 --<5.0 <5.0 <5.0 <5.0 --<5.0 <5.0 <5.0 <5.0 --<5.0 <5.0 <5.0 <5.0 --<5.0 <5.0 <5.0
Notes:1. Concentrations shown in µg/L (ppb)2. -- = Not Analyzed3. NSL = No Standard Listed4. NS = Not sampled: Wells MW-5 and MW-8 were dry; Well MW-6 contained 0.02 feet of free product.5. * = Well MW-12 contained 0.34 feet of product, however, a grab groundwater sample was collected below the product using a bailer.6. North Carolina (NC) 2L Standards, dated Janury 20107. Gross Contamination Level (GCL) Standards, dated Januray 20108. Bold/underlined values exceed the NC 2L Standards9. Shaded values exceed the GCL Standards
DMW-2MW-14 MW-15 MW-16 MW-17 MW-18 DMW-1
3 of 3 Prepared by/Date: MDF 6/26/14Checked by/Date: BH 6/26/14
ft/min ft/day ft/day ft/year
MW-1 9.45 x 10-4 1.36 0.12 43.19
MW-6 6.81 x 10-4 0.98 0.09 31.12
MW-10 7.68 x 10-4 1.11 0.10 35.23
Notes:
1. Slug tests were performed on January 22, 2010 during CSA activities.
2. Seepage velocities calculated using the equation V = K(dh/dl)/ne, where:
K = hydraulic conductivity
dh/dl = hyraulic gradient = 0.02 ft/ft
ne = effective porosity = 0.23
Prepared By/Date:AJF 11-9-12
Checked By/Date:MPF 11-9-12
Table 6
MACTEC Project: 6228-09-5100
Well No.Hydraulic Conductivity Seepage Velocity2
Summary of Slug Test Data
Southern Pump and Tank Company
4800 North Graham Street, Charlotte, North Carolina
Table 7
Summary of Natural Attenuation Parameters for Groundwater (December 2011)
Southern Pump and Tank Company
4800 North Graham Street, Charlotte, North Carolina
AMEC Project: 6228-09-5100
Sample ID DMW-1 DMW-2 MW-1 MW-2 MW-3 MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 MW-16 MW-17 MW-18
Conductivity (uS/cm)--0.176 0.402 0.148 0.999 0.900 0.088 0.106 0.202 0.161 0.162 0.237 0.676 0.188 0.072 0.046 0.663 0.649 0.332 0.531 0.400
Turbidity (NTU)----22.3 311 101 521 301 221 303 52.4 247 696 105 763 381 81 ----114 173 188
DO (mg/L)--6.29 7.51 5.69 4.59 4.31 5.11 7.38 6.2 5.79 5.65 5.24 5.71 7.2 5.04 6.05 5.29 7.12 7.52 6.08 4.89
Temp (°C)--20.23 18.02 16.37 17.76 21.96 17.33 21.44 16.99 15.38 20.05 20.23 20.38 15.21 16.25 15.79 16.76 16.93 17.01 16.44 17.87
ORP (mV)--222 -470 158 -60 0 259 440 35 276 427 218 40 290 276 342 129 68 329 143 -27
Sulfate 250000 ND 13600 ND 40000 ND ND ND ND ND ND ND ND 7200 ND ND ND ND ND ND ND
Nitrogen, Ammonia --ND ND ND 460 ND ND ND 190 ND ND ND ND 13600 ND ND ND ND ND ND ND
Nitrogen, Kjeldahl, Total --ND ND 550 6200 ND ND ND ND 510 ND ND ND 11400 ND ND ND ND ND ND ND
Nitrogen, Nitrate --550 ND ND ND ND ND 2000 ND 1100 1600 290 ND 10400 ND 2400 2900 15000 3900 ND 480
Nitrogen, Nitrite --510 ND ND 160 ND ND ND ND ND ND 140 ND ND ND ND ND ND ND ND ND
Iron 300 13600 267 6750 8910 5160 1650 470 22700 1040 77.9 3620 6580 228 2540 ND 92600 2360 7430 5080 968
Field Parameters
Laboratory Analyses
12/20/2011 12/20/2011Date
Collected 12/23/201112/23/2011 12/28/2011 12/23/2011
2L
Standards
(ug/L)12/22/201112/22/2011 12/22/2011 12/22/201112/20/2011 12/23/201112/28/201112/28/201112/28/2011 12/23/2011 12/29/2011 12/29/2011 12/29/2011 12/29/2011
Iron 300 13600 267 6750 8910 5160 1650 470 22700 1040 77.9 3620 6580 228 2540 ND 92600 2360 7430 5080 968
Manganese 50 327 22.3 31200 4330 9580 21.1 126 34000 15.7 561 165 2570 931 755 261 5570 5830 174 386 1080
Ethane --ND ND ND 285 ND ND ND 60.8 ND ND ND ND ND ND ND ND ND ND ND ND
Ethene --ND 11.6 ND 177 ND ND ND 146 ND ND ND ND ND ND ND ND ND ND ND ND
Methane --ND ND ND 4030 172 10.2 ND 3180 ND ND ND 913 ND 723 ND ND ND ND ND 110
Alkalinity, Total as CaCO3 --40800 90100 26800 336000 428000 7500 ND 81600 44000 ND 56900 204000 ND ND ND 9700 ND 48300 51500 73000
Iron, Ferrous --ND ND 5000 3000 1100 ND ND 6000 ND ND ND 2400 ND 2100 ND ND ND ND ND ND
Sulfide --ND ND ND 120 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Total Organic Nitrogen --ND ND 540 5700 ND ND ND ND 510 ND ND ND ND ND ND ND ND ND ND ND
Notes:Prepared by/Date:AJF 4-15-12
ND = Not Detected Checked by/Date:MPF 6/18/12
Constituent values shown in ug/l
Bold = Exceedance of 2L Standard
FIGURES
AMEC Environment and Infrastructure, Inc.
FIGURES
PREPAREDBY DATE CHECKED DATE JOB NUMBER FIGURE
±0 2,000 4,000 6,000 8,0001,000 Feet
16228-13-0135
SITE LOCATION MAPSOUTHERN PUMP AND TANK COMPANY4800 N. GRAHAM STREETCHARLOTTE, NORTH CAROLINA
Sources: Esri, HERE, DeLorme, TomTom, Intermap, increment P Corp.,GEBCO, USGS, FAO, NPS, NRCAN, GeoBase, IGN, Kadaster NL, OrdnanceSurvey, Esri Japan, METI, Esri China (Hong Kong), swisstopo, MapmyIndia, ©OpenStreetMap contributors, and the GIS User Community
SS 12/9/14 RCF 12/9/14
Project Site
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PREPAREDBY DATE CHECKED DATE JOB NUMBER FIGURE
±0 500 1,000 1,500 2,000250Feet
4
Source: Aerial Photography Provided by Charlotte-Mecklenburg GIS, 2013.
6228-13-0135
LAND USE AND RECEPTOR MAPSOUTHERN PUMP AND TANK COMPANY4800 N. GRAHAM STREETCHARLOTTE, NORTH CAROLINA
N G r a h a m S t
§¨¦85
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1823 Cannon Ave
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4801 Wild Rose Lane
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4800 Wild Rose Lane
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4819 Wild Rose Lane
Unidentified SurfaceWater BodyR-4
R-4
I-2
I-1
R-6(CD)
R-12MF I-1(CD)
I-1
R-4
I-2
I-1
B-2(CD)R-22MF
I-1 B-2I-1(CD)I-2
B-2(CD)
I-1(CD)
I-2
I-1I-2(CD)Copyright(c) City of Charlotte, Mecklenburg County, NC
Subject Property Sites with Water Supply Wells Zoning Boundary
Measured groundwater flow direction (June 2014)
Zoning DesignationR-4 - Single Family 4.0 units per acreR-12MF - Multi-family 12.0 units per acreI-2 - General IndustrialI-1(CD) - Light Industrial (Conditional Zoning)
I-1 - Light IndustrialB-2(CD) - General Business (Conditional Zoning)B-2 - General Business
SS 12/9/14 RCF 12/9/14
SB-2
(1.5')
1,1-Dichloroethane ND
1,2,4-Trimethylbenzene 2260
1,3,5-Trimethylbenzene 263
Benzene 0.428
Diisopropyl ether ND
Ethylbenzene 621
Methyl-tert-butyl ether ND
Naphthalene 1450
Tetrachloroethene ND
Xylene (Total) 1020
cis-1,2-Dichloroethene ND
n-Butylbenzene 0.402
n-Propylbenzene 380
Constituent
(13') (7')
1,1-Dichloroethane ND ND
1,2,4-Trimethylbenzene 381 ND
1,3,5-Trimethylbenzene ND ND
Benzene ND ND
Diisopropyl ether ND 5.3
Ethylbenzene ND ND
Methyl-tert-butyl ether 522 78.0
Naphthalene ND ND
Tetrachloroethene ND ND
Xylene (Total) ND ND
cis-1,2-Dichloroethene ND ND
n-Butylbenzene ND ND
n-Propylbenzene ND ND
Constituent SB-3
(16') (6')
1,1-Dichloroethane ND ND
1,2,4-Trimethylbenzene ND ND
1,3,5-Trimethylbenzene ND ND
Benzene ND ND
Diisopropyl ether ND 4.9
Ethylbenzene ND ND
Methyl-tert-butyl ether 45.4 54.2
Naphthalene ND ND
Tetrachloroethene ND ND
Xylene (Total) ND ND
cis-1,2-Dichloroethene ND ND
n-Butylbenzene ND ND
n-Propylbenzene ND ND
Constituent SB-4
(13') (17')
1,1-Dichloroethane ND ND
1,2,4-Trimethylbenzene ND ND
1,3,5-Trimethylbenzene ND ND
Benzene ND ND
Diisopropyl ether ND ND
Ethylbenzene ND ND
Methyl-tert-butyl ether ND ND
Naphthalene ND ND
Tetrachloroethene ND ND
Xylene (Total) ND ND
cis-1,2-Dichloroethene ND ND
n-Butylbenzene ND ND
n-Propylbenzene ND ND
Constituent SB-5
(10') (17')
1,1-Dichloroethane ND ND
1,2,4-Trimethylbenzene ND ND
1,3,5-Trimethylbenzene ND ND
Benzene ND ND
Diisopropyl ether ND ND
Ethylbenzene ND ND
Methyl-tert-butyl ether 18.4 ND
Naphthalene ND ND
Tetrachloroethene ND ND
Xylene (Total) ND ND
cis-1,2-Dichloroethene ND ND
n-Butylbenzene ND ND
n-Propylbenzene ND ND
Constituent SB-6
(16') (7')
1,1-Dichloroethane ND ND
1,2,4-Trimethylbenzene 542 ND
1,3,5-Trimethylbenzene ND ND
Benzene ND ND
Diisopropyl ether ND ND
Ethylbenzene ND ND
Methyl-tert-butyl ether 584 808
Naphthalene 511 ND
Tetrachloroethene 321 ND
Xylene (Total) ND ND
cis-1,2-Dichloroethene 330 ND
n-Butylbenzene 172 ND
n-Propylbenzene ND ND
Constituent SB-7
(16') (7')
1,1-Dichloroethane ND ND
1,2,4-Trimethylbenzene ND ND
1,3,5-Trimethylbenzene ND ND
Benzene ND ND
Diisopropyl ether ND ND
Ethylbenzene ND ND
Methyl-tert-butyl ether ND 5.5
Naphthalene ND ND
Tetrachloroethene ND ND
Xylene (Total) ND ND
cis-1,2-Dichloroethene 11.2 8.7
n-Butylbenzene ND ND
n-Propylbenzene ND ND
Constituent SB-8
(16') (6')
1,1-Dichloroethane ND ND
1,2,4-Trimethylbenzene ND ND
1,3,5-Trimethylbenzene ND ND
Benzene ND ND
Diisopropyl ether ND ND
Ethylbenzene ND ND
Methyl-tert-butyl ether ND ND
Naphthalene ND ND
Tetrachloroethene ND ND
Xylene (Total) ND ND
cis-1,2-Dichloroethene ND ND
n-Butylbenzene ND ND
n-Propylbenzene ND ND
Constituent SB-9
(10') (17')
1,1-Dichloroethane 5.2 9.5
1,2,4-Trimethylbenzene 39.1 10.6
1,3,5-Trimethylbenzene 9.4 ND
Benzene ND ND
Diisopropyl ether ND ND
Ethylbenzene ND ND
Methyl-tert-butyl ether 6.5 6.7
Naphthalene 80.5 ND
Tetrachloroethene ND ND
Xylene (Total) 31.4 42.3
cis-1,2-Dichloroethene 53.5 85.6
n-Butylbenzene 5.3 ND
n-Propylbenzene ND ND
Constituent SB-10
(5') (12')
1,1-Dichloroethane ND ND
1,2,4-Trimethylbenzene ND ND
1,3,5-Trimethylbenzene ND ND
Benzene ND 6.0
Diisopropyl ether ND ND
Ethylbenzene ND ND
Methyl-tert-butyl ether 35.3 19.5
Naphthalene ND ND
Tetrachloroethene ND ND
Xylene (Total) ND ND
cis-1,2-Dichloroethene ND 24.4
n-Butylbenzene ND ND
n-Propylbenzene ND ND
SB-1Constituent
Constituent
Action
Level
(mg/kg)
Soil-to-
Groundwater
MSCC
(ug/kg)
Residential
MSCC
(ug/kg)
Industrial/
Commercial
MSCC
(ug/kg)
TPH-DRO 10 ‐‐ ‐‐  ‐‐
TPH-GRO 10 ‐‐ ‐‐  ‐‐
1,1-Dichloroethane -- 32 110000 1000000
1,2,4-Trimethylbenzene -- 8500 782000 2040000
1,3,5-Trimethylbenzene -- 8300 782000 2040000
Benzene -- 5.6 18000 164000
Diisopropyl ether -- 370 156000 4090000
Ethylbenzene -- 4900 1560000 4000000
Methyl-tert-butyl ether -- 91 350000 3100000
Naphthalene -- 160 313000 8180000
Tetrachloroethene -- 7.4 1100 10000
Xylene (Total) -- 4600 3130000 8180000
cis-1,2-Dichloroethene -- 350 156000 4000000
n-Butylbenzene -- 4300 626000 1640000
n-Propylbenzene --1700 626000 1640000
Constituent GP-1
TPH-DRO 724
TPH-GRO 1670
Constituent GP-2
TPH-DRO 1300
TPH-GRO 1170
Constituent GP-3
TPH-DRO 270
TPH-GRO 122
Constituent GP-4
TPH-DRO 1390
TPH-GRO 278
(5') (10') (15')
TPH-DRO 8.3 69.7 576
TPH-GRO ND 53.0 394
Benzene 99.8 2470 4370
Tetrachloroethene ND 68.4 1040
Constituent GP-5
(5') (10') (15')
TPH-DRO ND ND ND
TPH-GRO ND ND ND
Benzene 52.0 83.9 160
Tetrachloroethene ND ND ND
Constituent GP-6
(5') (10') (15')
TPH-DRO 19.6 5720 1450
TPH-GRO ND 1090 49.3
Benzene ND ND 70.6
Tetrachloroethene ND 14900 543
Constituent GP-7
(5') (10') (15')
TPH-DRO NS 157 6030
TPH-GRO NS 48.5 750
Benzene NS ND 8760
Tetrachloroethene NS ND 19100
Constituent GP-8
Constituent NC 2L Standards GCLs
Benzene 15,000
1,2-Dichloroethane 0.4 400
1,1-Dichloroethene 77,000
cis-1,2-Dichloroethene 70 70,000
trans-1,2-Dichloroethene 100 100,000
1,2-Dichloropropane 0.6 600
Diisopropyl ether 70 70,000
Methyl-tert-butyl ether 20 20,000
Naphthalene 66,000Tetrachloroethene0.7 700Trichloroethene33,000Vinyl chloride 0.03 30Aliphatic (C09-C18)700 NSLAliphatic (C19-C36)10,000 NSL
Aromatic (C11-C22)200 NSL
Aliphatic (C05-C08)400 NSL
Aliphatic (C09-C12)700 NSL
Aromatic (C09-C10)200 NSL
Chromium 10 10,000
Lead 15 15,000
Constituent MW-15
VOCs by SM 6200B
Benzene <0.50
1,2-Dichloroethane <0.50
1,1-Dichloroethene <0.50cis-1,2-Dichloroethene <0.50
trans-1,2-Dichloroethene <0.50
1,2-Dichloropropane <0.50
Diisopropyl ether <0.50
Methyl-tert-butyl ether <0.50
Naphthalene <2.0
Tetrachloroethene <0.50
Trichloroethene <0.50
Vinyl chloride <1.0
Metals by EPA Method 6010/3030CChromium <5.0
Lead <5.0
Constituent MW-1
VOCs by SM 6200B
Benzene 725
1,2-Dichloroethane <250
1,1-Dichloroethene <250
cis-1,2-Dichloroethene 43500trans-1,2-Dichloroethene <250
1,2-Dichloropropane <250
Diisopropyl ether <250
Methyl-tert-butyl ether <250
Naphthalene <1000
Tetrachloroethene 292
Trichloroethene <250
Vinyl chloride <500
Metals by EPA Method 6010/3030C
Chromium 6.0
Lead <5.0
Constituent MW-2
VOCs by SM 6200B
Benzene 187
1,2-Dichloroethane <2.5
1,1-Dichloroethene <2.5
cis-1,2-Dichloroethene 33.4
trans-1,2-Dichloroethene <2.5
1,2-Dichloropropane <2.5
Diisopropyl ether 24.5
Methyl-tert-butyl ether 422Naphthalene42.4
Tetrachloroethene <2.5
Trichloroethene <2.5
Vinyl chloride 10.9
Metals by EPA Method 6010/3030CChromium <5.0
Lead <5.0
Constituent MW-3
VOCs by SM 6200B
Benzene 140001,2-Dichloroethane 752
1,1-Dichloroethene <50.0
cis-1,2-Dichloroethene 3020
trans-1,2-Dichloroethene <50.0
1,2-Dichloropropane 65.5Diisopropyl ether 113
Methyl-tert-butyl ether <50.0
Naphthalene 336
Tetrachloroethene <50.0
Trichloroethene <50.0
Vinyl chloride <100
Metals by EPA Method 6010/3030C
Chromium <5.0
Lead <5.0
Constituent MW-4
VOCs by SM 6200B
Benzene <0.50
1,2-Dichloroethane <0.501,1-Dichloroethene <0.50
cis-1,2-Dichloroethene <0.50
trans-1,2-Dichloroethene <0.50
1,2-Dichloropropane <0.50
Diisopropyl ether <0.50Methyl-tert-butyl ether <0.50
Naphthalene <2.0
Tetrachloroethene <0.50
Trichloroethene <0.50
Vinyl chloride <1.0
Metals by EPA Method 6010/3030C
Chromium 23.6
Lead <5.0
Constituent MW-7
VOCs by SM 6200B
Benzene <0.50
1,2-Dichloroethane <0.50
1,1-Dichloroethene <0.50
cis-1,2-Dichloroethene <0.50
trans-1,2-Dichloroethene <0.50
1,2-Dichloropropane <0.50
Diisopropyl ether <0.50
Methyl-tert-butyl ether <0.50
Naphthalene <2.0
Tetrachloroethene <0.50
Trichloroethene <0.50Vinyl chloride <1.0
Metals by EPA Method 6010/3030C
Chromium <5.0
Lead <5.0
Constituent MW-9
VOCs by SM 6200BBenzene <0.501,2-Dichloroethane <0.50
1,1-Dichloroethene <0.50
cis-1,2-Dichloroethene 0.73
trans-1,2-Dichloroethene <0.50
1,2-Dichloropropane <0.50Diisopropyl ether <0.50
Methyl-tert-butyl ether <0.50
Naphthalene <2.0
Tetrachloroethene 123Trichloroethene <0.50Vinyl chloride <1.0
Metals by EPA Method 6010/3030C
Chromium 11.5
Lead <5.0
Constituent MW-10
VOCs by SM 6200BBenzene 2720
1,2-Dichloroethane 43.2
1,1-Dichloroethene <5.0
cis-1,2-Dichloroethene 555
trans-1,2-Dichloroethene <5.0
1,2-Dichloropropane 12.7
Diisopropyl ether <5.0
Methyl-tert-butyl ether <5.0
Naphthalene 108
Tetrachloroethene <5.0
Trichloroethene <5.0
Vinyl chloride <10.0
Metals by EPA Method 6010/3030C
Chromium <5.0
Lead <5.0
Constituent MW-11
VOCs by SM 6200B
Benzene <0.50
1,2-Dichloroethane <0.50
1,1-Dichloroethene <0.50
cis-1,2-Dichloroethene <0.50
trans-1,2-Dichloroethene <0.50
1,2-Dichloropropane <0.50
Diisopropyl ether <0.50
Methyl-tert-butyl ether <0.50
Naphthalene <2.0
Tetrachloroethene 1.5
Trichloroethene <0.50
Vinyl chloride <1.0
Metals by EPA Method 6010/3030C
Chromium <5.0
Lead <5.0
Constituent MW-13
VOCs by SM 6200B
Benzene <0.50
1,2-Dichloroethane <0.50
1,1-Dichloroethene <0.50cis-1,2-Dichloroethene <0.50
trans-1,2-Dichloroethene <0.50
1,2-Dichloropropane <0.50
Diisopropyl ether <0.50
Methyl-tert-butyl ether <0.50Naphthalene <2.0
Tetrachloroethene 431
Trichloroethene 2.6
Vinyl chloride <1.0
Metals by EPA Method 6010/3030CChromium <5.0
Lead <5.0
Constituent MW-14
VOCs by SM 6200BBenzene <0.50
1,2-Dichloroethane <0.50
1,1-Dichloroethene <0.50
cis-1,2-Dichloroethene <0.50
trans-1,2-Dichloroethene <0.50
1,2-Dichloropropane <0.50
Diisopropyl ether <0.50
Methyl-tert-butyl ether <0.50
Naphthalene <2.0
Tetrachloroethene 0.67
Trichloroethene <0.50
Vinyl chloride <1.0
Metals by EPA Method 6010/3030C
Chromium 48.7
Lead 21.4
Constituent MW-16
VOCs by SM 6200B
Benzene <0.50
1,2-Dichloroethane <0.50
1,1-Dichloroethene <0.50
cis-1,2-Dichloroethene <0.50
trans-1,2-Dichloroethene <0.50
1,2-Dichloropropane <0.50
Diisopropyl ether <0.50
Methyl-tert-butyl ether 0.78
Naphthalene <2.0
Tetrachloroethene 0.98
Trichloroethene <0.50
Vinyl chloride <1.0
Metals by EPA Method 6010/3030C
Chromium 10.9
Lead <5.0
Constituent MW-17
VOCs by SM 6200B
Benzene <0.50
1,2-Dichloroethane <0.50
1,1-Dichloroethene <0.50cis-1,2-Dichloroethene 4.8
trans-1,2-Dichloroethene <0.50
1,2-Dichloropropane <0.50
Diisopropyl ether <0.50
Methyl-tert-butyl ether 1.2Naphthalene <2.0
Tetrachloroethene 8.2
Trichloroethene 9.8
Vinyl chloride <1.0
Metals by EPA Method 6010/3030CChromium <5.0
Lead <5.0
Constituent MW-18
VOCs by SM 6200B
Benzene <0.50
1,2-Dichloroethane <0.50
1,1-Dichloroethene <0.50
cis-1,2-Dichloroethene <0.50
trans-1,2-Dichloroethene <0.50
1,2-Dichloropropane <0.50
Diisopropyl ether <0.50
Methyl-tert-butyl ether <0.50
Naphthalene <2.0
Tetrachloroethene 2.7
Trichloroethene <0.50
Vinyl chloride <1.0
Metals by EPA Method 6010/3030C
Chromium <5.0
Lead <5.0
Constituent DMW-1
VOCs by SM 6200BBenzene <0.501,2-Dichloroethane 3.0
1,1-Dichloroethene <0.50
cis-1,2-Dichloroethene 49.2
trans-1,2-Dichloroethene <0.50
1,2-Dichloropropane <0.50Diisopropyl ether <0.50
Methyl-tert-butyl ether <0.50
Naphthalene <2.0
Tetrachloroethene 53.7Trichloroethene3.8Vinyl chloride <1.0
Metals by EPA Method 6010/3030C
Chromium 64.6
Lead <5.0
Constituent DMW-2
VOCs by SM 6200B
Benzene <0.50
1,2-Dichloroethane <0.50
1,1-Dichloroethene <0.50
cis-1,2-Dichloroethene 1.7
trans-1,2-Dichloroethene <0.50
1,2-Dichloropropane <0.50
Diisopropyl ether <0.50
Methyl-tert-butyl ether <0.50
Naphthalene <2.0
Tetrachloroethene 0.51
Trichloroethene <0.50
Vinyl chloride <1.0
Metals by EPA Method 6010/3030C
Chromium 5.7
Lead <5.0
Constituent MW-5
VOCs by SM 6200B
Benzene <0.50
1,2-Dichloroethane <0.50
1,1-Dichloroethene <0.50
cis-1,2-Dichloroethene <0.50
trans-1,2-Dichloroethene <0.50
1,2-Dichloropropane <0.50
Diisopropyl ether <0.50
Methyl-tert-butyl ether <0.50
Naphthalene <2.0
Tetrachloroethene 343
Trichloroethene 6.7
Vinyl chloride <1.0
Metals by EPA Method 6010/3030C
Chromium <5.0
Lead <5.0
Constituent MW-6
VOCs by SM 6200BBenzene 41.9
1,2-Dichloroethane <5.0
1,1-Dichloroethene <5.0
cis-1,2-Dichloroethene 979
trans-1,2-Dichloroethene <5.01,2-Dichloropropane <5.0
Diisopropyl ether <5.0
Methyl-tert-butyl ether <5.0
Naphthalene 312Tetrachloroethene21.3Trichloroethene <5.0
Vinyl chloride 221
Metals by EPA Method 6010/3030C
Chromium <5.0
Lead <5.0
Constituent MW-8
VOCs by SM 6200B
Benzene <0.50
1,2-Dichloroethane <0.50
1,1-Dichloroethene <0.50
cis-1,2-Dichloroethene <0.50
trans-1,2-Dichloroethene <0.50
1,2-Dichloropropane <0.50
Diisopropyl ether <0.50
Methyl-tert-butyl ether <0.50
Naphthalene <2.0
Tetrachloroethene 241
Trichloroethene 4.5
Vinyl chloride <1.0
Metals by EPA Method 6010/3030CChromium <5.0
Lead <5.0
APPENDIX A
AMEC Environment and Infrastructure, Inc.
APPENDIX A
REGULATORY CORRESPONDENCE
APPENDIX B
AMEC Environment and Infrastructure, Inc.
APPENDIX B
LABORATORY REPORT OF ANALYSES –SOIL SAMPLES (DECEMBER 2011)
December 22, 2011
LIMS USE: FR - MARK FILARDI
LIMS OBJECT ID: 92108640
92108640
Project:
Pace Project No.:
RE:
Mr. Mark Filardi
AMEC-Charlotte
2801 Yorkmont Road
Charlotte, NC 28208
DIMMETTE CHARLOTTE 6228095100
Dear Mr. Filardi:
Enclosed are the analytical results for sample(s) received by the laboratory on December 16, 2011.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001South Carolina Drinking Water Cert. #: 99006003Virginia Drinking Water Certification #: 00213
Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031West Virginia Certification #: 357Virginia/VELAP Certification #: 460144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92108640001 SB-1 (12')EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
92108640002 SB-1 (5')EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
92108640003 SB-2 (1.5')EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
92108640004 SB-3 (7')EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
92108640005 SB-3 (13')EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
92108640006 SB-4 (6')EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
92108640007 SB-4 (16')EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
92108640008 SB-5 (13')EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
92108640009 SB-5 (17')EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
92108640010 SB-6 (10')EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
92108640011 SB-6 (17')EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
92108640012 SB-7 (7')EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
92108640013 SB-7 (16')EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
92108640014 SB-8 (7')EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
92108640015 SB-8 (16')EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
92108640016 SB-9 (6')EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
92108640017 SB-9 (16')EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
92108640018 SB-10 (10')EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
92108640019 SB-10 (17')EPA 8260 71 PASI-CDLK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-1 (12')Lab ID:92108640001 Collected:12/15/11 09:25 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 12/21/11 14:30 67-64-1118
Benzene 6.0 ug/kg 1 12/21/11 14:30 71-43-25.9
Bromobenzene ND ug/kg 1 12/21/11 14:30 108-86-15.9
Bromochloromethane ND ug/kg 1 12/21/11 14:30 74-97-55.9
Bromodichloromethane ND ug/kg 1 12/21/11 14:30 75-27-45.9
Bromoform ND ug/kg 1 12/21/11 14:30 75-25-25.9
Bromomethane ND ug/kg 1 12/21/11 14:30 74-83-911.8
2-Butanone (MEK)ND ug/kg 1 12/21/11 14:30 78-93-3118
n-Butylbenzene ND ug/kg 1 12/21/11 14:30 104-51-85.9
sec-Butylbenzene ND ug/kg 1 12/21/11 14:30 135-98-85.9
tert-Butylbenzene ND ug/kg 1 12/21/11 14:30 98-06-65.9
Carbon tetrachloride ND ug/kg 1 12/21/11 14:30 56-23-55.9
Chlorobenzene ND ug/kg 1 12/21/11 14:30 108-90-75.9
Chloroethane ND ug/kg 1 12/21/11 14:30 75-00-311.8
Chloroform ND ug/kg 1 12/21/11 14:30 67-66-35.9
Chloromethane ND ug/kg 1 12/21/11 14:30 74-87-311.8
2-Chlorotoluene ND ug/kg 1 12/21/11 14:30 95-49-85.9
4-Chlorotoluene ND ug/kg 1 12/21/11 14:30 106-43-45.9
1,2-Dibromo-3-chloropropane ND ug/kg 1 12/21/11 14:30 96-12-85.9
Dibromochloromethane ND ug/kg 1 12/21/11 14:30 124-48-15.9
1,2-Dibromoethane (EDB)ND ug/kg 1 12/21/11 14:30 106-93-45.9
Dibromomethane ND ug/kg 1 12/21/11 14:30 74-95-35.9
1,2-Dichlorobenzene ND ug/kg 1 12/21/11 14:30 95-50-15.9
1,3-Dichlorobenzene ND ug/kg 1 12/21/11 14:30 541-73-15.9
1,4-Dichlorobenzene ND ug/kg 1 12/21/11 14:30 106-46-75.9
Dichlorodifluoromethane ND ug/kg 1 12/21/11 14:30 75-71-811.8
1,1-Dichloroethane ND ug/kg 1 12/21/11 14:30 75-34-35.9
1,2-Dichloroethane ND ug/kg 1 12/21/11 14:30 107-06-25.9
1,1-Dichloroethene ND ug/kg 1 12/21/11 14:30 75-35-45.9
cis-1,2-Dichloroethene 24.4 ug/kg 1 12/21/11 14:30 156-59-25.9
trans-1,2-Dichloroethene ND ug/kg 1 12/21/11 14:30 156-60-55.9
1,2-Dichloropropane ND ug/kg 1 12/21/11 14:30 78-87-55.9
1,3-Dichloropropane ND ug/kg 1 12/21/11 14:30 142-28-95.9
2,2-Dichloropropane ND ug/kg 1 12/21/11 14:30 594-20-75.9
1,1-Dichloropropene ND ug/kg 1 12/21/11 14:30 563-58-65.9
cis-1,3-Dichloropropene ND ug/kg 1 12/21/11 14:30 10061-01-55.9
trans-1,3-Dichloropropene ND ug/kg 1 12/21/11 14:30 10061-02-65.9
Diisopropyl ether ND ug/kg 1 12/21/11 14:30 108-20-35.9
Ethylbenzene ND ug/kg 1 12/21/11 14:30 100-41-45.9
Hexachloro-1,3-butadiene ND ug/kg 1 12/21/11 14:30 87-68-35.9
2-Hexanone ND ug/kg 1 12/21/11 14:30 591-78-659.1
Isopropylbenzene (Cumene)ND ug/kg 1 12/21/11 14:30 98-82-85.9
p-Isopropyltoluene ND ug/kg 1 12/21/11 14:30 99-87-65.9
Methylene Chloride ND ug/kg 1 12/21/11 14:30 75-09-223.6
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 12/21/11 14:30 108-10-159.1
Methyl-tert-butyl ether 19.5 ug/kg 1 12/21/11 14:30 1634-04-45.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 5 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-1 (12')Lab ID:92108640001 Collected:12/15/11 09:25 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Naphthalene ND ug/kg 1 12/21/11 14:30 91-20-35.9
n-Propylbenzene ND ug/kg 1 12/21/11 14:30 103-65-15.9
Styrene ND ug/kg 1 12/21/11 14:30 100-42-55.9
1,1,1,2-Tetrachloroethane ND ug/kg 1 12/21/11 14:30 630-20-65.9
1,1,2,2-Tetrachloroethane ND ug/kg 1 12/21/11 14:30 79-34-55.9
Tetrachloroethene ND ug/kg 1 12/21/11 14:30 127-18-45.9
Toluene ND ug/kg 1 12/21/11 14:30 108-88-35.9
1,2,3-Trichlorobenzene ND ug/kg 1 12/21/11 14:30 87-61-65.9
1,2,4-Trichlorobenzene ND ug/kg 1 12/21/11 14:30 120-82-15.9
1,1,1-Trichloroethane ND ug/kg 1 12/21/11 14:30 71-55-65.9
1,1,2-Trichloroethane ND ug/kg 1 12/21/11 14:30 79-00-55.9
Trichloroethene ND ug/kg 1 12/21/11 14:30 79-01-65.9
Trichlorofluoromethane ND ug/kg 1 12/21/11 14:30 75-69-45.9
1,2,3-Trichloropropane ND ug/kg 1 12/21/11 14:30 96-18-45.9
1,2,4-Trimethylbenzene ND ug/kg 1 12/21/11 14:30 95-63-65.9
1,3,5-Trimethylbenzene ND ug/kg 1 12/21/11 14:30 108-67-85.9
Vinyl acetate ND ug/kg 1 12/21/11 14:30 108-05-459.1
Vinyl chloride ND ug/kg 1 12/21/11 14:30 75-01-411.8
Xylene (Total)ND ug/kg 1 12/21/11 14:30 1330-20-711.8
m&p-Xylene ND ug/kg 1 12/21/11 14:30 179601-23-111.8
o-Xylene ND ug/kg 1 12/21/11 14:30 95-47-65.9
Surrogates
Dibromofluoromethane (S)97 %1 12/21/11 14:30 1868-53-770-130
Toluene-d8 (S)101 %1 12/21/11 14:30 2037-26-570-130
4-Bromofluorobenzene (S)97 %1 12/21/11 14:30 460-00-470-130
1,2-Dichloroethane-d4 (S)93 %1 12/21/11 14:30 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 32.7 %1 12/19/11 08:580.10
Sample:SB-1 (5')Lab ID:92108640002 Collected:12/15/11 09:20 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 12/22/11 12:43 67-64-198.5
Benzene ND ug/kg 1 12/22/11 12:43 71-43-24.9
Bromobenzene ND ug/kg 1 12/22/11 12:43 108-86-14.9
Bromochloromethane ND ug/kg 1 12/22/11 12:43 74-97-54.9
Bromodichloromethane ND ug/kg 1 12/22/11 12:43 75-27-44.9
Bromoform ND ug/kg 1 12/22/11 12:43 75-25-24.9
Bromomethane ND ug/kg 1 12/22/11 12:43 74-83-99.8
2-Butanone (MEK)ND ug/kg 1 12/22/11 12:43 78-93-398.5
n-Butylbenzene ND ug/kg 1 12/22/11 12:43 104-51-84.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 6 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-1 (5')Lab ID:92108640002 Collected:12/15/11 09:20 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
sec-Butylbenzene ND ug/kg 1 12/22/11 12:43 135-98-84.9
tert-Butylbenzene ND ug/kg 1 12/22/11 12:43 98-06-64.9
Carbon tetrachloride ND ug/kg 1 12/22/11 12:43 56-23-54.9
Chlorobenzene ND ug/kg 1 12/22/11 12:43 108-90-74.9
Chloroethane ND ug/kg 1 12/22/11 12:43 75-00-39.8
Chloroform ND ug/kg 1 12/22/11 12:43 67-66-34.9
Chloromethane ND ug/kg 1 12/22/11 12:43 74-87-39.8
2-Chlorotoluene ND ug/kg 1 12/22/11 12:43 95-49-84.9
4-Chlorotoluene ND ug/kg 1 12/22/11 12:43 106-43-44.9
1,2-Dibromo-3-chloropropane ND ug/kg 1 12/22/11 12:43 96-12-84.9
Dibromochloromethane ND ug/kg 1 12/22/11 12:43 124-48-14.9
1,2-Dibromoethane (EDB)ND ug/kg 1 12/22/11 12:43 106-93-44.9
Dibromomethane ND ug/kg 1 12/22/11 12:43 74-95-34.9
1,2-Dichlorobenzene ND ug/kg 1 12/22/11 12:43 95-50-14.9
1,3-Dichlorobenzene ND ug/kg 1 12/22/11 12:43 541-73-14.9
1,4-Dichlorobenzene ND ug/kg 1 12/22/11 12:43 106-46-74.9
Dichlorodifluoromethane ND ug/kg 1 12/22/11 12:43 75-71-89.8
1,1-Dichloroethane ND ug/kg 1 12/22/11 12:43 75-34-34.9
1,2-Dichloroethane ND ug/kg 1 12/22/11 12:43 107-06-24.9
1,1-Dichloroethene ND ug/kg 1 12/22/11 12:43 75-35-44.9
cis-1,2-Dichloroethene ND ug/kg 1 12/22/11 12:43 156-59-24.9
trans-1,2-Dichloroethene ND ug/kg 1 12/22/11 12:43 156-60-54.9
1,2-Dichloropropane ND ug/kg 1 12/22/11 12:43 78-87-54.9
1,3-Dichloropropane ND ug/kg 1 12/22/11 12:43 142-28-94.9
2,2-Dichloropropane ND ug/kg 1 12/22/11 12:43 594-20-74.9
1,1-Dichloropropene ND ug/kg 1 12/22/11 12:43 563-58-64.9
cis-1,3-Dichloropropene ND ug/kg 1 12/22/11 12:43 10061-01-54.9
trans-1,3-Dichloropropene ND ug/kg 1 12/22/11 12:43 10061-02-64.9
Diisopropyl ether ND ug/kg 1 12/22/11 12:43 108-20-34.9
Ethylbenzene ND ug/kg 1 12/22/11 12:43 100-41-44.9
Hexachloro-1,3-butadiene ND ug/kg 1 12/22/11 12:43 87-68-34.9
2-Hexanone ND ug/kg 1 12/22/11 12:43 591-78-649.2
Isopropylbenzene (Cumene)ND ug/kg 1 12/22/11 12:43 98-82-84.9
p-Isopropyltoluene ND ug/kg 1 12/22/11 12:43 99-87-64.9
Methylene Chloride ND ug/kg 1 12/22/11 12:43 75-09-219.7
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 12/22/11 12:43 108-10-149.2
Methyl-tert-butyl ether 35.3 ug/kg 1 12/22/11 12:43 1634-04-44.9
Naphthalene ND ug/kg 1 12/22/11 12:43 91-20-34.9
n-Propylbenzene ND ug/kg 1 12/22/11 12:43 103-65-14.9
Styrene ND ug/kg 1 12/22/11 12:43 100-42-54.9
1,1,1,2-Tetrachloroethane ND ug/kg 1 12/22/11 12:43 630-20-64.9
1,1,2,2-Tetrachloroethane ND ug/kg 1 12/22/11 12:43 79-34-54.9
Tetrachloroethene ND ug/kg 1 12/22/11 12:43 127-18-44.9
Toluene ND ug/kg 1 12/22/11 12:43 108-88-34.9
1,2,3-Trichlorobenzene ND ug/kg 1 12/22/11 12:43 87-61-64.9
1,2,4-Trichlorobenzene ND ug/kg 1 12/22/11 12:43 120-82-14.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 7 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-1 (5')Lab ID:92108640002 Collected:12/15/11 09:20 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1-Trichloroethane ND ug/kg 1 12/22/11 12:43 71-55-64.9
1,1,2-Trichloroethane ND ug/kg 1 12/22/11 12:43 79-00-54.9
Trichloroethene ND ug/kg 1 12/22/11 12:43 79-01-64.9
Trichlorofluoromethane ND ug/kg 1 12/22/11 12:43 75-69-44.9
1,2,3-Trichloropropane ND ug/kg 1 12/22/11 12:43 96-18-44.9
1,2,4-Trimethylbenzene ND ug/kg 1 12/22/11 12:43 95-63-64.9
1,3,5-Trimethylbenzene ND ug/kg 1 12/22/11 12:43 108-67-84.9
Vinyl acetate ND ug/kg 1 12/22/11 12:43 108-05-449.2
Vinyl chloride ND ug/kg 1 12/22/11 12:43 75-01-49.8
Xylene (Total)ND ug/kg 1 12/22/11 12:43 1330-20-79.8
m&p-Xylene ND ug/kg 1 12/22/11 12:43 179601-23-19.8
o-Xylene ND ug/kg 1 12/22/11 12:43 95-47-64.9
Surrogates
Dibromofluoromethane (S)103 %1 12/22/11 12:43 1868-53-770-130
Toluene-d8 (S)100 %1 12/22/11 12:43 2037-26-570-130
4-Bromofluorobenzene (S)96 %1 12/22/11 12:43 460-00-470-130
1,2-Dichloroethane-d4 (S)98 %1 12/22/11 12:43 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 21.0 %1 12/19/11 08:590.10
Sample:SB-2 (1.5')Lab ID:92108640003 Collected:12/15/11 10:00 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 50 12/21/11 15:10 67-64-14610
Benzene 428 ug/kg 50 12/21/11 15:10 71-43-2230
Bromobenzene ND ug/kg 50 12/21/11 15:10 108-86-1230
Bromochloromethane ND ug/kg 50 12/21/11 15:10 74-97-5230
Bromodichloromethane ND ug/kg 50 12/21/11 15:10 75-27-4230
Bromoform ND ug/kg 50 12/21/11 15:10 75-25-2230
Bromomethane ND ug/kg 50 12/21/11 15:10 74-83-9461
2-Butanone (MEK)ND ug/kg 50 12/21/11 15:10 78-93-34610
n-Butylbenzene 402 ug/kg 50 12/21/11 15:10 104-51-8230
sec-Butylbenzene ND ug/kg 50 12/21/11 15:10 135-98-8230
tert-Butylbenzene ND ug/kg 50 12/21/11 15:10 98-06-6230
Carbon tetrachloride ND ug/kg 50 12/21/11 15:10 56-23-5230
Chlorobenzene ND ug/kg 50 12/21/11 15:10 108-90-7230
Chloroethane ND ug/kg 50 12/21/11 15:10 75-00-3461
Chloroform ND ug/kg 50 12/21/11 15:10 67-66-3230
Chloromethane ND ug/kg 50 12/21/11 15:10 74-87-3461
2-Chlorotoluene ND ug/kg 50 12/21/11 15:10 95-49-8230
4-Chlorotoluene ND ug/kg 50 12/21/11 15:10 106-43-4230
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 8 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-2 (1.5')Lab ID:92108640003 Collected:12/15/11 10:00 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dibromo-3-chloropropane ND ug/kg 50 12/21/11 15:10 96-12-8230
Dibromochloromethane ND ug/kg 50 12/21/11 15:10 124-48-1230
1,2-Dibromoethane (EDB)ND ug/kg 50 12/21/11 15:10 106-93-4230
Dibromomethane ND ug/kg 50 12/21/11 15:10 74-95-3230
1,2-Dichlorobenzene ND ug/kg 50 12/21/11 15:10 95-50-1230
1,3-Dichlorobenzene ND ug/kg 50 12/21/11 15:10 541-73-1230
1,4-Dichlorobenzene ND ug/kg 50 12/21/11 15:10 106-46-7230
Dichlorodifluoromethane ND ug/kg 50 12/21/11 15:10 75-71-8 D3461
1,1-Dichloroethane ND ug/kg 50 12/21/11 15:10 75-34-3230
1,2-Dichloroethane ND ug/kg 50 12/21/11 15:10 107-06-2230
1,1-Dichloroethene ND ug/kg 50 12/21/11 15:10 75-35-4230
cis-1,2-Dichloroethene ND ug/kg 50 12/21/11 15:10 156-59-2230
trans-1,2-Dichloroethene ND ug/kg 50 12/21/11 15:10 156-60-5230
1,2-Dichloropropane ND ug/kg 50 12/21/11 15:10 78-87-5230
1,3-Dichloropropane ND ug/kg 50 12/21/11 15:10 142-28-9230
2,2-Dichloropropane ND ug/kg 50 12/21/11 15:10 594-20-7230
1,1-Dichloropropene ND ug/kg 50 12/21/11 15:10 563-58-6230
cis-1,3-Dichloropropene ND ug/kg 50 12/21/11 15:10 10061-01-5230
trans-1,3-Dichloropropene ND ug/kg 50 12/21/11 15:10 10061-02-6230
Diisopropyl ether ND ug/kg 50 12/21/11 15:10 108-20-3230
Ethylbenzene 621 ug/kg 50 12/21/11 15:10 100-41-4230
Hexachloro-1,3-butadiene ND ug/kg 50 12/21/11 15:10 87-68-3230
2-Hexanone ND ug/kg 50 12/21/11 15:10 591-78-62300
Isopropylbenzene (Cumene)ND ug/kg 50 12/21/11 15:10 98-82-8230
p-Isopropyltoluene ND ug/kg 50 12/21/11 15:10 99-87-6230
Methylene Chloride ND ug/kg 50 12/21/11 15:10 75-09-2922
4-Methyl-2-pentanone (MIBK)ND ug/kg 50 12/21/11 15:10 108-10-12300
Methyl-tert-butyl ether ND ug/kg 50 12/21/11 15:10 1634-04-4230
Naphthalene 1450 ug/kg 50 12/21/11 15:10 91-20-3230
n-Propylbenzene 380 ug/kg 50 12/21/11 15:10 103-65-1230
Styrene ND ug/kg 50 12/21/11 15:10 100-42-5230
1,1,1,2-Tetrachloroethane ND ug/kg 50 12/21/11 15:10 630-20-6230
1,1,2,2-Tetrachloroethane ND ug/kg 50 12/21/11 15:10 79-34-5230
Tetrachloroethene ND ug/kg 50 12/21/11 15:10 127-18-4230
Toluene ND ug/kg 50 12/21/11 15:10 108-88-3230
1,2,3-Trichlorobenzene ND ug/kg 50 12/21/11 15:10 87-61-6230
1,2,4-Trichlorobenzene ND ug/kg 50 12/21/11 15:10 120-82-1230
1,1,1-Trichloroethane ND ug/kg 50 12/21/11 15:10 71-55-6230
1,1,2-Trichloroethane ND ug/kg 50 12/21/11 15:10 79-00-5230
Trichloroethene ND ug/kg 50 12/21/11 15:10 79-01-6230
Trichlorofluoromethane ND ug/kg 50 12/21/11 15:10 75-69-4230
1,2,3-Trichloropropane ND ug/kg 50 12/21/11 15:10 96-18-4230
1,2,4-Trimethylbenzene 2260 ug/kg 50 12/21/11 15:10 95-63-6230
1,3,5-Trimethylbenzene 263 ug/kg 50 12/21/11 15:10 108-67-8230
Vinyl acetate ND ug/kg 50 12/21/11 15:10 108-05-42300
Vinyl chloride ND ug/kg 50 12/21/11 15:10 75-01-4461
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 9 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-2 (1.5')Lab ID:92108640003 Collected:12/15/11 10:00 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Xylene (Total)1020 ug/kg 50 12/21/11 15:10 1330-20-7461
m&p-Xylene 975 ug/kg 50 12/21/11 15:10 179601-23-1461
o-Xylene ND ug/kg 50 12/21/11 15:10 95-47-6230
Surrogates
Dibromofluoromethane (S)106 %50 12/21/11 15:10 1868-53-770-130
Toluene-d8 (S)100 %50 12/21/11 15:10 2037-26-570-130
4-Bromofluorobenzene (S)96 %50 12/21/11 15:10 460-00-470-130
1,2-Dichloroethane-d4 (S)107 %50 12/21/11 15:10 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 16.8 %1 12/19/11 08:590.10
Sample:SB-3 (7')Lab ID:92108640004 Collected:12/15/11 10:25 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 12/22/11 13:02 67-64-182.0
Benzene ND ug/kg 1 12/22/11 13:02 71-43-24.1
Bromobenzene ND ug/kg 1 12/22/11 13:02 108-86-14.1
Bromochloromethane ND ug/kg 1 12/22/11 13:02 74-97-54.1
Bromodichloromethane ND ug/kg 1 12/22/11 13:02 75-27-44.1
Bromoform ND ug/kg 1 12/22/11 13:02 75-25-24.1
Bromomethane ND ug/kg 1 12/22/11 13:02 74-83-98.2
2-Butanone (MEK)ND ug/kg 1 12/22/11 13:02 78-93-382.0
n-Butylbenzene ND ug/kg 1 12/22/11 13:02 104-51-84.1
sec-Butylbenzene ND ug/kg 1 12/22/11 13:02 135-98-84.1
tert-Butylbenzene ND ug/kg 1 12/22/11 13:02 98-06-64.1
Carbon tetrachloride ND ug/kg 1 12/22/11 13:02 56-23-54.1
Chlorobenzene ND ug/kg 1 12/22/11 13:02 108-90-74.1
Chloroethane ND ug/kg 1 12/22/11 13:02 75-00-38.2
Chloroform ND ug/kg 1 12/22/11 13:02 67-66-34.1
Chloromethane ND ug/kg 1 12/22/11 13:02 74-87-38.2
2-Chlorotoluene ND ug/kg 1 12/22/11 13:02 95-49-84.1
4-Chlorotoluene ND ug/kg 1 12/22/11 13:02 106-43-44.1
1,2-Dibromo-3-chloropropane ND ug/kg 1 12/22/11 13:02 96-12-84.1
Dibromochloromethane ND ug/kg 1 12/22/11 13:02 124-48-14.1
1,2-Dibromoethane (EDB)ND ug/kg 1 12/22/11 13:02 106-93-44.1
Dibromomethane ND ug/kg 1 12/22/11 13:02 74-95-34.1
1,2-Dichlorobenzene ND ug/kg 1 12/22/11 13:02 95-50-14.1
1,3-Dichlorobenzene ND ug/kg 1 12/22/11 13:02 541-73-14.1
1,4-Dichlorobenzene ND ug/kg 1 12/22/11 13:02 106-46-74.1
Dichlorodifluoromethane ND ug/kg 1 12/22/11 13:02 75-71-88.2
1,1-Dichloroethane ND ug/kg 1 12/22/11 13:02 75-34-34.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 10 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-3 (7')Lab ID:92108640004 Collected:12/15/11 10:25 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dichloroethane ND ug/kg 1 12/22/11 13:02 107-06-24.1
1,1-Dichloroethene ND ug/kg 1 12/22/11 13:02 75-35-44.1
cis-1,2-Dichloroethene ND ug/kg 1 12/22/11 13:02 156-59-24.1
trans-1,2-Dichloroethene ND ug/kg 1 12/22/11 13:02 156-60-54.1
1,2-Dichloropropane ND ug/kg 1 12/22/11 13:02 78-87-54.1
1,3-Dichloropropane ND ug/kg 1 12/22/11 13:02 142-28-94.1
2,2-Dichloropropane ND ug/kg 1 12/22/11 13:02 594-20-74.1
1,1-Dichloropropene ND ug/kg 1 12/22/11 13:02 563-58-64.1
cis-1,3-Dichloropropene ND ug/kg 1 12/22/11 13:02 10061-01-54.1
trans-1,3-Dichloropropene ND ug/kg 1 12/22/11 13:02 10061-02-64.1
Diisopropyl ether 5.3 ug/kg 1 12/22/11 13:02 108-20-34.1
Ethylbenzene ND ug/kg 1 12/22/11 13:02 100-41-44.1
Hexachloro-1,3-butadiene ND ug/kg 1 12/22/11 13:02 87-68-34.1
2-Hexanone ND ug/kg 1 12/22/11 13:02 591-78-641.0
Isopropylbenzene (Cumene)ND ug/kg 1 12/22/11 13:02 98-82-84.1
p-Isopropyltoluene ND ug/kg 1 12/22/11 13:02 99-87-64.1
Methylene Chloride ND ug/kg 1 12/22/11 13:02 75-09-216.4
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 12/22/11 13:02 108-10-141.0
Methyl-tert-butyl ether 78.0 ug/kg 1 12/22/11 13:02 1634-04-44.1
Naphthalene ND ug/kg 1 12/22/11 13:02 91-20-34.1
n-Propylbenzene ND ug/kg 1 12/22/11 13:02 103-65-14.1
Styrene ND ug/kg 1 12/22/11 13:02 100-42-54.1
1,1,1,2-Tetrachloroethane ND ug/kg 1 12/22/11 13:02 630-20-64.1
1,1,2,2-Tetrachloroethane ND ug/kg 1 12/22/11 13:02 79-34-54.1
Tetrachloroethene ND ug/kg 1 12/22/11 13:02 127-18-44.1
Toluene ND ug/kg 1 12/22/11 13:02 108-88-34.1
1,2,3-Trichlorobenzene ND ug/kg 1 12/22/11 13:02 87-61-64.1
1,2,4-Trichlorobenzene ND ug/kg 1 12/22/11 13:02 120-82-14.1
1,1,1-Trichloroethane ND ug/kg 1 12/22/11 13:02 71-55-64.1
1,1,2-Trichloroethane ND ug/kg 1 12/22/11 13:02 79-00-54.1
Trichloroethene ND ug/kg 1 12/22/11 13:02 79-01-64.1
Trichlorofluoromethane ND ug/kg 1 12/22/11 13:02 75-69-44.1
1,2,3-Trichloropropane ND ug/kg 1 12/22/11 13:02 96-18-44.1
1,2,4-Trimethylbenzene ND ug/kg 1 12/22/11 13:02 95-63-64.1
1,3,5-Trimethylbenzene ND ug/kg 1 12/22/11 13:02 108-67-84.1
Vinyl acetate ND ug/kg 1 12/22/11 13:02 108-05-441.0
Vinyl chloride ND ug/kg 1 12/22/11 13:02 75-01-48.2
Xylene (Total)ND ug/kg 1 12/22/11 13:02 1330-20-78.2
m&p-Xylene ND ug/kg 1 12/22/11 13:02 179601-23-18.2
o-Xylene ND ug/kg 1 12/22/11 13:02 95-47-64.1
Surrogates
Dibromofluoromethane (S)104 %1 12/22/11 13:02 1868-53-770-130
Toluene-d8 (S)98 %1 12/22/11 13:02 2037-26-570-130
4-Bromofluorobenzene (S)95 %1 12/22/11 13:02 460-00-470-130
1,2-Dichloroethane-d4 (S)98 %1 12/22/11 13:02 17060-07-070-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 11 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-3 (7')Lab ID:92108640004 Collected:12/15/11 10:25 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 14.8 %1 12/19/11 08:590.10
Sample:SB-3 (13')Lab ID:92108640005 Collected:12/15/11 10:30 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 50 12/21/11 15:50 67-64-14920
Benzene ND ug/kg 50 12/21/11 15:50 71-43-2246
Bromobenzene ND ug/kg 50 12/21/11 15:50 108-86-1246
Bromochloromethane ND ug/kg 50 12/21/11 15:50 74-97-5246
Bromodichloromethane ND ug/kg 50 12/21/11 15:50 75-27-4246
Bromoform ND ug/kg 50 12/21/11 15:50 75-25-2246
Bromomethane ND ug/kg 50 12/21/11 15:50 74-83-9492
2-Butanone (MEK)ND ug/kg 50 12/21/11 15:50 78-93-34920
n-Butylbenzene ND ug/kg 50 12/21/11 15:50 104-51-8246
sec-Butylbenzene ND ug/kg 50 12/21/11 15:50 135-98-8246
tert-Butylbenzene ND ug/kg 50 12/21/11 15:50 98-06-6246
Carbon tetrachloride ND ug/kg 50 12/21/11 15:50 56-23-5246
Chlorobenzene ND ug/kg 50 12/21/11 15:50 108-90-7246
Chloroethane ND ug/kg 50 12/21/11 15:50 75-00-3492
Chloroform ND ug/kg 50 12/21/11 15:50 67-66-3246
Chloromethane ND ug/kg 50 12/21/11 15:50 74-87-3492
2-Chlorotoluene ND ug/kg 50 12/21/11 15:50 95-49-8246
4-Chlorotoluene ND ug/kg 50 12/21/11 15:50 106-43-4246
1,2-Dibromo-3-chloropropane ND ug/kg 50 12/21/11 15:50 96-12-8246
Dibromochloromethane ND ug/kg 50 12/21/11 15:50 124-48-1246
1,2-Dibromoethane (EDB)ND ug/kg 50 12/21/11 15:50 106-93-4246
Dibromomethane ND ug/kg 50 12/21/11 15:50 74-95-3246
1,2-Dichlorobenzene ND ug/kg 50 12/21/11 15:50 95-50-1246
1,3-Dichlorobenzene ND ug/kg 50 12/21/11 15:50 541-73-1246
1,4-Dichlorobenzene ND ug/kg 50 12/21/11 15:50 106-46-7246
Dichlorodifluoromethane ND ug/kg 50 12/21/11 15:50 75-71-8 D3492
1,1-Dichloroethane ND ug/kg 50 12/21/11 15:50 75-34-3246
1,2-Dichloroethane ND ug/kg 50 12/21/11 15:50 107-06-2246
1,1-Dichloroethene ND ug/kg 50 12/21/11 15:50 75-35-4246
cis-1,2-Dichloroethene ND ug/kg 50 12/21/11 15:50 156-59-2246
trans-1,2-Dichloroethene ND ug/kg 50 12/21/11 15:50 156-60-5246
1,2-Dichloropropane ND ug/kg 50 12/21/11 15:50 78-87-5246
1,3-Dichloropropane ND ug/kg 50 12/21/11 15:50 142-28-9246
2,2-Dichloropropane ND ug/kg 50 12/21/11 15:50 594-20-7246
1,1-Dichloropropene ND ug/kg 50 12/21/11 15:50 563-58-6246
cis-1,3-Dichloropropene ND ug/kg 50 12/21/11 15:50 10061-01-5246
trans-1,3-Dichloropropene ND ug/kg 50 12/21/11 15:50 10061-02-6246
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 12 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-3 (13')Lab ID:92108640005 Collected:12/15/11 10:30 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Diisopropyl ether ND ug/kg 50 12/21/11 15:50 108-20-3246
Ethylbenzene ND ug/kg 50 12/21/11 15:50 100-41-4246
Hexachloro-1,3-butadiene ND ug/kg 50 12/21/11 15:50 87-68-3246
2-Hexanone ND ug/kg 50 12/21/11 15:50 591-78-62460
Isopropylbenzene (Cumene)ND ug/kg 50 12/21/11 15:50 98-82-8246
p-Isopropyltoluene ND ug/kg 50 12/21/11 15:50 99-87-6246
Methylene Chloride ND ug/kg 50 12/21/11 15:50 75-09-2983
4-Methyl-2-pentanone (MIBK)ND ug/kg 50 12/21/11 15:50 108-10-12460
Methyl-tert-butyl ether 522 ug/kg 50 12/21/11 15:50 1634-04-4246
Naphthalene ND ug/kg 50 12/21/11 15:50 91-20-3246
n-Propylbenzene ND ug/kg 50 12/21/11 15:50 103-65-1246
Styrene ND ug/kg 50 12/21/11 15:50 100-42-5246
1,1,1,2-Tetrachloroethane ND ug/kg 50 12/21/11 15:50 630-20-6246
1,1,2,2-Tetrachloroethane ND ug/kg 50 12/21/11 15:50 79-34-5246
Tetrachloroethene ND ug/kg 50 12/21/11 15:50 127-18-4246
Toluene ND ug/kg 50 12/21/11 15:50 108-88-3246
1,2,3-Trichlorobenzene ND ug/kg 50 12/21/11 15:50 87-61-6246
1,2,4-Trichlorobenzene ND ug/kg 50 12/21/11 15:50 120-82-1246
1,1,1-Trichloroethane ND ug/kg 50 12/21/11 15:50 71-55-6246
1,1,2-Trichloroethane ND ug/kg 50 12/21/11 15:50 79-00-5246
Trichloroethene ND ug/kg 50 12/21/11 15:50 79-01-6246
Trichlorofluoromethane ND ug/kg 50 12/21/11 15:50 75-69-4246
1,2,3-Trichloropropane ND ug/kg 50 12/21/11 15:50 96-18-4246
1,2,4-Trimethylbenzene 381 ug/kg 50 12/21/11 15:50 95-63-6246
1,3,5-Trimethylbenzene ND ug/kg 50 12/21/11 15:50 108-67-8246
Vinyl acetate ND ug/kg 50 12/21/11 15:50 108-05-42460
Vinyl chloride ND ug/kg 50 12/21/11 15:50 75-01-4492
Xylene (Total)ND ug/kg 50 12/21/11 15:50 1330-20-7492
m&p-Xylene ND ug/kg 50 12/21/11 15:50 179601-23-1492
o-Xylene ND ug/kg 50 12/21/11 15:50 95-47-6246
Surrogates
Dibromofluoromethane (S)92 %50 12/21/11 15:50 1868-53-770-130
Toluene-d8 (S)100 %50 12/21/11 15:50 2037-26-570-130
4-Bromofluorobenzene (S)93 %50 12/21/11 15:50 460-00-470-130
1,2-Dichloroethane-d4 (S)78 %50 12/21/11 15:50 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 22.6 %1 12/19/11 08:590.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 13 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-4 (6')Lab ID:92108640006 Collected:12/15/11 11:15 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 12/21/11 16:10 67-64-193.7
Benzene ND ug/kg 1 12/21/11 16:10 71-43-24.7
Bromobenzene ND ug/kg 1 12/21/11 16:10 108-86-14.7
Bromochloromethane ND ug/kg 1 12/21/11 16:10 74-97-54.7
Bromodichloromethane ND ug/kg 1 12/21/11 16:10 75-27-44.7
Bromoform ND ug/kg 1 12/21/11 16:10 75-25-24.7
Bromomethane ND ug/kg 1 12/21/11 16:10 74-83-99.4
2-Butanone (MEK)ND ug/kg 1 12/21/11 16:10 78-93-393.7
n-Butylbenzene ND ug/kg 1 12/21/11 16:10 104-51-84.7
sec-Butylbenzene ND ug/kg 1 12/21/11 16:10 135-98-84.7
tert-Butylbenzene ND ug/kg 1 12/21/11 16:10 98-06-64.7
Carbon tetrachloride ND ug/kg 1 12/21/11 16:10 56-23-54.7
Chlorobenzene ND ug/kg 1 12/21/11 16:10 108-90-74.7
Chloroethane ND ug/kg 1 12/21/11 16:10 75-00-39.4
Chloroform ND ug/kg 1 12/21/11 16:10 67-66-34.7
Chloromethane ND ug/kg 1 12/21/11 16:10 74-87-39.4
2-Chlorotoluene ND ug/kg 1 12/21/11 16:10 95-49-84.7
4-Chlorotoluene ND ug/kg 1 12/21/11 16:10 106-43-44.7
1,2-Dibromo-3-chloropropane ND ug/kg 1 12/21/11 16:10 96-12-84.7
Dibromochloromethane ND ug/kg 1 12/21/11 16:10 124-48-14.7
1,2-Dibromoethane (EDB)ND ug/kg 1 12/21/11 16:10 106-93-44.7
Dibromomethane ND ug/kg 1 12/21/11 16:10 74-95-34.7
1,2-Dichlorobenzene ND ug/kg 1 12/21/11 16:10 95-50-14.7
1,3-Dichlorobenzene ND ug/kg 1 12/21/11 16:10 541-73-14.7
1,4-Dichlorobenzene ND ug/kg 1 12/21/11 16:10 106-46-74.7
Dichlorodifluoromethane ND ug/kg 1 12/21/11 16:10 75-71-89.4
1,1-Dichloroethane ND ug/kg 1 12/21/11 16:10 75-34-34.7
1,2-Dichloroethane ND ug/kg 1 12/21/11 16:10 107-06-24.7
1,1-Dichloroethene ND ug/kg 1 12/21/11 16:10 75-35-44.7
cis-1,2-Dichloroethene ND ug/kg 1 12/21/11 16:10 156-59-24.7
trans-1,2-Dichloroethene ND ug/kg 1 12/21/11 16:10 156-60-54.7
1,2-Dichloropropane ND ug/kg 1 12/21/11 16:10 78-87-54.7
1,3-Dichloropropane ND ug/kg 1 12/21/11 16:10 142-28-94.7
2,2-Dichloropropane ND ug/kg 1 12/21/11 16:10 594-20-74.7
1,1-Dichloropropene ND ug/kg 1 12/21/11 16:10 563-58-64.7
cis-1,3-Dichloropropene ND ug/kg 1 12/21/11 16:10 10061-01-54.7
trans-1,3-Dichloropropene ND ug/kg 1 12/21/11 16:10 10061-02-64.7
Diisopropyl ether 4.9 ug/kg 1 12/21/11 16:10 108-20-34.7
Ethylbenzene ND ug/kg 1 12/21/11 16:10 100-41-44.7
Hexachloro-1,3-butadiene ND ug/kg 1 12/21/11 16:10 87-68-34.7
2-Hexanone ND ug/kg 1 12/21/11 16:10 591-78-646.9
Isopropylbenzene (Cumene)ND ug/kg 1 12/21/11 16:10 98-82-84.7
p-Isopropyltoluene ND ug/kg 1 12/21/11 16:10 99-87-64.7
Methylene Chloride ND ug/kg 1 12/21/11 16:10 75-09-218.7
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 12/21/11 16:10 108-10-146.9
Methyl-tert-butyl ether 54.2 ug/kg 1 12/21/11 16:10 1634-04-44.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 14 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-4 (6')Lab ID:92108640006 Collected:12/15/11 11:15 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Naphthalene ND ug/kg 1 12/21/11 16:10 91-20-34.7
n-Propylbenzene ND ug/kg 1 12/21/11 16:10 103-65-14.7
Styrene ND ug/kg 1 12/21/11 16:10 100-42-54.7
1,1,1,2-Tetrachloroethane ND ug/kg 1 12/21/11 16:10 630-20-64.7
1,1,2,2-Tetrachloroethane ND ug/kg 1 12/21/11 16:10 79-34-54.7
Tetrachloroethene ND ug/kg 1 12/21/11 16:10 127-18-44.7
Toluene ND ug/kg 1 12/21/11 16:10 108-88-34.7
1,2,3-Trichlorobenzene ND ug/kg 1 12/21/11 16:10 87-61-64.7
1,2,4-Trichlorobenzene ND ug/kg 1 12/21/11 16:10 120-82-14.7
1,1,1-Trichloroethane ND ug/kg 1 12/21/11 16:10 71-55-64.7
1,1,2-Trichloroethane ND ug/kg 1 12/21/11 16:10 79-00-54.7
Trichloroethene ND ug/kg 1 12/21/11 16:10 79-01-64.7
Trichlorofluoromethane ND ug/kg 1 12/21/11 16:10 75-69-44.7
1,2,3-Trichloropropane ND ug/kg 1 12/21/11 16:10 96-18-44.7
1,2,4-Trimethylbenzene ND ug/kg 1 12/21/11 16:10 95-63-64.7
1,3,5-Trimethylbenzene ND ug/kg 1 12/21/11 16:10 108-67-84.7
Vinyl acetate ND ug/kg 1 12/21/11 16:10 108-05-446.9
Vinyl chloride ND ug/kg 1 12/21/11 16:10 75-01-49.4
Xylene (Total)ND ug/kg 1 12/21/11 16:10 1330-20-79.4
m&p-Xylene ND ug/kg 1 12/21/11 16:10 179601-23-19.4
o-Xylene ND ug/kg 1 12/21/11 16:10 95-47-64.7
Surrogates
Dibromofluoromethane (S)99 %1 12/21/11 16:10 1868-53-770-130
Toluene-d8 (S)103 %1 12/21/11 16:10 2037-26-570-130
4-Bromofluorobenzene (S)100 %1 12/21/11 16:10 460-00-470-130
1,2-Dichloroethane-d4 (S)95 %1 12/21/11 16:10 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 20.3 %1 12/19/11 08:590.10
Sample:SB-4 (16')Lab ID:92108640007 Collected:12/15/11 11:20 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 12/22/11 13:22 67-64-197.9
Benzene ND ug/kg 1 12/22/11 13:22 71-43-24.9
Bromobenzene ND ug/kg 1 12/22/11 13:22 108-86-14.9
Bromochloromethane ND ug/kg 1 12/22/11 13:22 74-97-54.9
Bromodichloromethane ND ug/kg 1 12/22/11 13:22 75-27-44.9
Bromoform ND ug/kg 1 12/22/11 13:22 75-25-24.9
Bromomethane ND ug/kg 1 12/22/11 13:22 74-83-99.8
2-Butanone (MEK)ND ug/kg 1 12/22/11 13:22 78-93-397.9
n-Butylbenzene ND ug/kg 1 12/22/11 13:22 104-51-84.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 15 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-4 (16')Lab ID:92108640007 Collected:12/15/11 11:20 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
sec-Butylbenzene ND ug/kg 1 12/22/11 13:22 135-98-84.9
tert-Butylbenzene ND ug/kg 1 12/22/11 13:22 98-06-64.9
Carbon tetrachloride ND ug/kg 1 12/22/11 13:22 56-23-54.9
Chlorobenzene ND ug/kg 1 12/22/11 13:22 108-90-74.9
Chloroethane ND ug/kg 1 12/22/11 13:22 75-00-39.8
Chloroform ND ug/kg 1 12/22/11 13:22 67-66-34.9
Chloromethane ND ug/kg 1 12/22/11 13:22 74-87-39.8
2-Chlorotoluene ND ug/kg 1 12/22/11 13:22 95-49-84.9
4-Chlorotoluene ND ug/kg 1 12/22/11 13:22 106-43-44.9
1,2-Dibromo-3-chloropropane ND ug/kg 1 12/22/11 13:22 96-12-84.9
Dibromochloromethane ND ug/kg 1 12/22/11 13:22 124-48-14.9
1,2-Dibromoethane (EDB)ND ug/kg 1 12/22/11 13:22 106-93-44.9
Dibromomethane ND ug/kg 1 12/22/11 13:22 74-95-34.9
1,2-Dichlorobenzene ND ug/kg 1 12/22/11 13:22 95-50-14.9
1,3-Dichlorobenzene ND ug/kg 1 12/22/11 13:22 541-73-14.9
1,4-Dichlorobenzene ND ug/kg 1 12/22/11 13:22 106-46-74.9
Dichlorodifluoromethane ND ug/kg 1 12/22/11 13:22 75-71-89.8
1,1-Dichloroethane ND ug/kg 1 12/22/11 13:22 75-34-34.9
1,2-Dichloroethane ND ug/kg 1 12/22/11 13:22 107-06-24.9
1,1-Dichloroethene ND ug/kg 1 12/22/11 13:22 75-35-44.9
cis-1,2-Dichloroethene ND ug/kg 1 12/22/11 13:22 156-59-24.9
trans-1,2-Dichloroethene ND ug/kg 1 12/22/11 13:22 156-60-54.9
1,2-Dichloropropane ND ug/kg 1 12/22/11 13:22 78-87-54.9
1,3-Dichloropropane ND ug/kg 1 12/22/11 13:22 142-28-94.9
2,2-Dichloropropane ND ug/kg 1 12/22/11 13:22 594-20-74.9
1,1-Dichloropropene ND ug/kg 1 12/22/11 13:22 563-58-64.9
cis-1,3-Dichloropropene ND ug/kg 1 12/22/11 13:22 10061-01-54.9
trans-1,3-Dichloropropene ND ug/kg 1 12/22/11 13:22 10061-02-64.9
Diisopropyl ether ND ug/kg 1 12/22/11 13:22 108-20-34.9
Ethylbenzene ND ug/kg 1 12/22/11 13:22 100-41-44.9
Hexachloro-1,3-butadiene ND ug/kg 1 12/22/11 13:22 87-68-34.9
2-Hexanone ND ug/kg 1 12/22/11 13:22 591-78-649.0
Isopropylbenzene (Cumene)ND ug/kg 1 12/22/11 13:22 98-82-84.9
p-Isopropyltoluene ND ug/kg 1 12/22/11 13:22 99-87-64.9
Methylene Chloride ND ug/kg 1 12/22/11 13:22 75-09-219.6
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 12/22/11 13:22 108-10-149.0
Methyl-tert-butyl ether 45.4 ug/kg 1 12/22/11 13:22 1634-04-44.9
Naphthalene ND ug/kg 1 12/22/11 13:22 91-20-34.9
n-Propylbenzene ND ug/kg 1 12/22/11 13:22 103-65-14.9
Styrene ND ug/kg 1 12/22/11 13:22 100-42-54.9
1,1,1,2-Tetrachloroethane ND ug/kg 1 12/22/11 13:22 630-20-64.9
1,1,2,2-Tetrachloroethane ND ug/kg 1 12/22/11 13:22 79-34-54.9
Tetrachloroethene ND ug/kg 1 12/22/11 13:22 127-18-44.9
Toluene ND ug/kg 1 12/22/11 13:22 108-88-34.9
1,2,3-Trichlorobenzene ND ug/kg 1 12/22/11 13:22 87-61-64.9
1,2,4-Trichlorobenzene ND ug/kg 1 12/22/11 13:22 120-82-14.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 16 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-4 (16')Lab ID:92108640007 Collected:12/15/11 11:20 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1-Trichloroethane ND ug/kg 1 12/22/11 13:22 71-55-64.9
1,1,2-Trichloroethane ND ug/kg 1 12/22/11 13:22 79-00-54.9
Trichloroethene ND ug/kg 1 12/22/11 13:22 79-01-64.9
Trichlorofluoromethane ND ug/kg 1 12/22/11 13:22 75-69-44.9
1,2,3-Trichloropropane ND ug/kg 1 12/22/11 13:22 96-18-44.9
1,2,4-Trimethylbenzene ND ug/kg 1 12/22/11 13:22 95-63-64.9
1,3,5-Trimethylbenzene ND ug/kg 1 12/22/11 13:22 108-67-84.9
Vinyl acetate ND ug/kg 1 12/22/11 13:22 108-05-449.0
Vinyl chloride ND ug/kg 1 12/22/11 13:22 75-01-49.8
Xylene (Total)ND ug/kg 1 12/22/11 13:22 1330-20-79.8
m&p-Xylene ND ug/kg 1 12/22/11 13:22 179601-23-19.8
o-Xylene ND ug/kg 1 12/22/11 13:22 95-47-64.9
Surrogates
Dibromofluoromethane (S)108 %1 12/22/11 13:22 1868-53-770-130
Toluene-d8 (S)100 %1 12/22/11 13:22 2037-26-570-130
4-Bromofluorobenzene (S)96 %1 12/22/11 13:22 460-00-470-130
1,2-Dichloroethane-d4 (S)102 %1 12/22/11 13:22 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 22.3 %1 12/19/11 09:000.10
Sample:SB-5 (13')Lab ID:92108640008 Collected:12/15/11 11:55 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 12/22/11 13:42 67-64-192.0
Benzene ND ug/kg 1 12/22/11 13:42 71-43-24.6
Bromobenzene ND ug/kg 1 12/22/11 13:42 108-86-14.6
Bromochloromethane ND ug/kg 1 12/22/11 13:42 74-97-54.6
Bromodichloromethane ND ug/kg 1 12/22/11 13:42 75-27-44.6
Bromoform ND ug/kg 1 12/22/11 13:42 75-25-24.6
Bromomethane ND ug/kg 1 12/22/11 13:42 74-83-99.2
2-Butanone (MEK)ND ug/kg 1 12/22/11 13:42 78-93-392.0
n-Butylbenzene ND ug/kg 1 12/22/11 13:42 104-51-84.6
sec-Butylbenzene ND ug/kg 1 12/22/11 13:42 135-98-84.6
tert-Butylbenzene ND ug/kg 1 12/22/11 13:42 98-06-64.6
Carbon tetrachloride ND ug/kg 1 12/22/11 13:42 56-23-54.6
Chlorobenzene ND ug/kg 1 12/22/11 13:42 108-90-74.6
Chloroethane ND ug/kg 1 12/22/11 13:42 75-00-39.2
Chloroform ND ug/kg 1 12/22/11 13:42 67-66-34.6
Chloromethane ND ug/kg 1 12/22/11 13:42 74-87-39.2
2-Chlorotoluene ND ug/kg 1 12/22/11 13:42 95-49-84.6
4-Chlorotoluene ND ug/kg 1 12/22/11 13:42 106-43-44.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 17 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-5 (13')Lab ID:92108640008 Collected:12/15/11 11:55 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dibromo-3-chloropropane ND ug/kg 1 12/22/11 13:42 96-12-84.6
Dibromochloromethane ND ug/kg 1 12/22/11 13:42 124-48-14.6
1,2-Dibromoethane (EDB)ND ug/kg 1 12/22/11 13:42 106-93-44.6
Dibromomethane ND ug/kg 1 12/22/11 13:42 74-95-34.6
1,2-Dichlorobenzene ND ug/kg 1 12/22/11 13:42 95-50-14.6
1,3-Dichlorobenzene ND ug/kg 1 12/22/11 13:42 541-73-14.6
1,4-Dichlorobenzene ND ug/kg 1 12/22/11 13:42 106-46-74.6
Dichlorodifluoromethane ND ug/kg 1 12/22/11 13:42 75-71-89.2
1,1-Dichloroethane ND ug/kg 1 12/22/11 13:42 75-34-34.6
1,2-Dichloroethane ND ug/kg 1 12/22/11 13:42 107-06-24.6
1,1-Dichloroethene ND ug/kg 1 12/22/11 13:42 75-35-44.6
cis-1,2-Dichloroethene ND ug/kg 1 12/22/11 13:42 156-59-24.6
trans-1,2-Dichloroethene ND ug/kg 1 12/22/11 13:42 156-60-54.6
1,2-Dichloropropane ND ug/kg 1 12/22/11 13:42 78-87-54.6
1,3-Dichloropropane ND ug/kg 1 12/22/11 13:42 142-28-94.6
2,2-Dichloropropane ND ug/kg 1 12/22/11 13:42 594-20-74.6
1,1-Dichloropropene ND ug/kg 1 12/22/11 13:42 563-58-64.6
cis-1,3-Dichloropropene ND ug/kg 1 12/22/11 13:42 10061-01-54.6
trans-1,3-Dichloropropene ND ug/kg 1 12/22/11 13:42 10061-02-64.6
Diisopropyl ether ND ug/kg 1 12/22/11 13:42 108-20-34.6
Ethylbenzene ND ug/kg 1 12/22/11 13:42 100-41-44.6
Hexachloro-1,3-butadiene ND ug/kg 1 12/22/11 13:42 87-68-34.6
2-Hexanone ND ug/kg 1 12/22/11 13:42 591-78-646.0
Isopropylbenzene (Cumene)ND ug/kg 1 12/22/11 13:42 98-82-84.6
p-Isopropyltoluene ND ug/kg 1 12/22/11 13:42 99-87-64.6
Methylene Chloride ND ug/kg 1 12/22/11 13:42 75-09-218.4
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 12/22/11 13:42 108-10-146.0
Methyl-tert-butyl ether ND ug/kg 1 12/22/11 13:42 1634-04-44.6
Naphthalene ND ug/kg 1 12/22/11 13:42 91-20-34.6
n-Propylbenzene ND ug/kg 1 12/22/11 13:42 103-65-14.6
Styrene ND ug/kg 1 12/22/11 13:42 100-42-54.6
1,1,1,2-Tetrachloroethane ND ug/kg 1 12/22/11 13:42 630-20-64.6
1,1,2,2-Tetrachloroethane ND ug/kg 1 12/22/11 13:42 79-34-54.6
Tetrachloroethene ND ug/kg 1 12/22/11 13:42 127-18-44.6
Toluene ND ug/kg 1 12/22/11 13:42 108-88-34.6
1,2,3-Trichlorobenzene ND ug/kg 1 12/22/11 13:42 87-61-64.6
1,2,4-Trichlorobenzene ND ug/kg 1 12/22/11 13:42 120-82-14.6
1,1,1-Trichloroethane ND ug/kg 1 12/22/11 13:42 71-55-64.6
1,1,2-Trichloroethane ND ug/kg 1 12/22/11 13:42 79-00-54.6
Trichloroethene ND ug/kg 1 12/22/11 13:42 79-01-64.6
Trichlorofluoromethane ND ug/kg 1 12/22/11 13:42 75-69-44.6
1,2,3-Trichloropropane ND ug/kg 1 12/22/11 13:42 96-18-44.6
1,2,4-Trimethylbenzene ND ug/kg 1 12/22/11 13:42 95-63-64.6
1,3,5-Trimethylbenzene ND ug/kg 1 12/22/11 13:42 108-67-84.6
Vinyl acetate ND ug/kg 1 12/22/11 13:42 108-05-446.0
Vinyl chloride ND ug/kg 1 12/22/11 13:42 75-01-49.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 18 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-5 (13')Lab ID:92108640008 Collected:12/15/11 11:55 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Xylene (Total)ND ug/kg 1 12/22/11 13:42 1330-20-79.2
m&p-Xylene ND ug/kg 1 12/22/11 13:42 179601-23-19.2
o-Xylene ND ug/kg 1 12/22/11 13:42 95-47-64.6
Surrogates
Dibromofluoromethane (S)108 %1 12/22/11 13:42 1868-53-770-130
Toluene-d8 (S)101 %1 12/22/11 13:42 2037-26-570-130
4-Bromofluorobenzene (S)97 %1 12/22/11 13:42 460-00-470-130
1,2-Dichloroethane-d4 (S)99 %1 12/22/11 13:42 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 20.8 %1 12/19/11 09:000.10
Sample:SB-5 (17')Lab ID:92108640009 Collected:12/15/11 12:00 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 12/21/11 17:10 67-64-185.1
Benzene ND ug/kg 1 12/21/11 17:10 71-43-24.3
Bromobenzene ND ug/kg 1 12/21/11 17:10 108-86-14.3
Bromochloromethane ND ug/kg 1 12/21/11 17:10 74-97-54.3
Bromodichloromethane ND ug/kg 1 12/21/11 17:10 75-27-44.3
Bromoform ND ug/kg 1 12/21/11 17:10 75-25-24.3
Bromomethane ND ug/kg 1 12/21/11 17:10 74-83-98.5
2-Butanone (MEK)ND ug/kg 1 12/21/11 17:10 78-93-385.1
n-Butylbenzene ND ug/kg 1 12/21/11 17:10 104-51-84.3
sec-Butylbenzene ND ug/kg 1 12/21/11 17:10 135-98-84.3
tert-Butylbenzene ND ug/kg 1 12/21/11 17:10 98-06-64.3
Carbon tetrachloride ND ug/kg 1 12/21/11 17:10 56-23-54.3
Chlorobenzene ND ug/kg 1 12/21/11 17:10 108-90-74.3
Chloroethane ND ug/kg 1 12/21/11 17:10 75-00-38.5
Chloroform ND ug/kg 1 12/21/11 17:10 67-66-34.3
Chloromethane ND ug/kg 1 12/21/11 17:10 74-87-38.5
2-Chlorotoluene ND ug/kg 1 12/21/11 17:10 95-49-84.3
4-Chlorotoluene ND ug/kg 1 12/21/11 17:10 106-43-44.3
1,2-Dibromo-3-chloropropane ND ug/kg 1 12/21/11 17:10 96-12-84.3
Dibromochloromethane ND ug/kg 1 12/21/11 17:10 124-48-14.3
1,2-Dibromoethane (EDB)ND ug/kg 1 12/21/11 17:10 106-93-44.3
Dibromomethane ND ug/kg 1 12/21/11 17:10 74-95-34.3
1,2-Dichlorobenzene ND ug/kg 1 12/21/11 17:10 95-50-14.3
1,3-Dichlorobenzene ND ug/kg 1 12/21/11 17:10 541-73-14.3
1,4-Dichlorobenzene ND ug/kg 1 12/21/11 17:10 106-46-74.3
Dichlorodifluoromethane ND ug/kg 1 12/21/11 17:10 75-71-88.5
1,1-Dichloroethane ND ug/kg 1 12/21/11 17:10 75-34-34.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 19 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-5 (17')Lab ID:92108640009 Collected:12/15/11 12:00 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dichloroethane ND ug/kg 1 12/21/11 17:10 107-06-24.3
1,1-Dichloroethene ND ug/kg 1 12/21/11 17:10 75-35-44.3
cis-1,2-Dichloroethene ND ug/kg 1 12/21/11 17:10 156-59-24.3
trans-1,2-Dichloroethene ND ug/kg 1 12/21/11 17:10 156-60-54.3
1,2-Dichloropropane ND ug/kg 1 12/21/11 17:10 78-87-54.3
1,3-Dichloropropane ND ug/kg 1 12/21/11 17:10 142-28-94.3
2,2-Dichloropropane ND ug/kg 1 12/21/11 17:10 594-20-74.3
1,1-Dichloropropene ND ug/kg 1 12/21/11 17:10 563-58-64.3
cis-1,3-Dichloropropene ND ug/kg 1 12/21/11 17:10 10061-01-54.3
trans-1,3-Dichloropropene ND ug/kg 1 12/21/11 17:10 10061-02-64.3
Diisopropyl ether ND ug/kg 1 12/21/11 17:10 108-20-34.3
Ethylbenzene ND ug/kg 1 12/21/11 17:10 100-41-44.3
Hexachloro-1,3-butadiene ND ug/kg 1 12/21/11 17:10 87-68-34.3
2-Hexanone ND ug/kg 1 12/21/11 17:10 591-78-642.5
Isopropylbenzene (Cumene)ND ug/kg 1 12/21/11 17:10 98-82-84.3
p-Isopropyltoluene ND ug/kg 1 12/21/11 17:10 99-87-64.3
Methylene Chloride ND ug/kg 1 12/21/11 17:10 75-09-217.0
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 12/21/11 17:10 108-10-142.5
Methyl-tert-butyl ether ND ug/kg 1 12/21/11 17:10 1634-04-44.3
Naphthalene ND ug/kg 1 12/21/11 17:10 91-20-34.3
n-Propylbenzene ND ug/kg 1 12/21/11 17:10 103-65-14.3
Styrene ND ug/kg 1 12/21/11 17:10 100-42-54.3
1,1,1,2-Tetrachloroethane ND ug/kg 1 12/21/11 17:10 630-20-64.3
1,1,2,2-Tetrachloroethane ND ug/kg 1 12/21/11 17:10 79-34-54.3
Tetrachloroethene ND ug/kg 1 12/21/11 17:10 127-18-44.3
Toluene ND ug/kg 1 12/21/11 17:10 108-88-34.3
1,2,3-Trichlorobenzene ND ug/kg 1 12/21/11 17:10 87-61-64.3
1,2,4-Trichlorobenzene ND ug/kg 1 12/21/11 17:10 120-82-14.3
1,1,1-Trichloroethane ND ug/kg 1 12/21/11 17:10 71-55-64.3
1,1,2-Trichloroethane ND ug/kg 1 12/21/11 17:10 79-00-54.3
Trichloroethene ND ug/kg 1 12/21/11 17:10 79-01-64.3
Trichlorofluoromethane ND ug/kg 1 12/21/11 17:10 75-69-44.3
1,2,3-Trichloropropane ND ug/kg 1 12/21/11 17:10 96-18-44.3
1,2,4-Trimethylbenzene ND ug/kg 1 12/21/11 17:10 95-63-64.3
1,3,5-Trimethylbenzene ND ug/kg 1 12/21/11 17:10 108-67-84.3
Vinyl acetate ND ug/kg 1 12/21/11 17:10 108-05-442.5
Vinyl chloride ND ug/kg 1 12/21/11 17:10 75-01-48.5
Xylene (Total)ND ug/kg 1 12/21/11 17:10 1330-20-78.5
m&p-Xylene ND ug/kg 1 12/21/11 17:10 179601-23-18.5
o-Xylene ND ug/kg 1 12/21/11 17:10 95-47-64.3
Surrogates
Dibromofluoromethane (S)102 %1 12/21/11 17:10 1868-53-770-130
Toluene-d8 (S)100 %1 12/21/11 17:10 2037-26-570-130
4-Bromofluorobenzene (S)96 %1 12/21/11 17:10 460-00-470-130
1,2-Dichloroethane-d4 (S)95 %1 12/21/11 17:10 17060-07-070-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 20 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-5 (17')Lab ID:92108640009 Collected:12/15/11 12:00 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 24.1 %1 12/19/11 09:000.10
Sample:SB-6 (10')Lab ID:92108640010 Collected:12/15/11 13:25 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 12/22/11 14:02 67-64-1105
Benzene ND ug/kg 1 12/22/11 14:02 71-43-25.3
Bromobenzene ND ug/kg 1 12/22/11 14:02 108-86-15.3
Bromochloromethane ND ug/kg 1 12/22/11 14:02 74-97-55.3
Bromodichloromethane ND ug/kg 1 12/22/11 14:02 75-27-45.3
Bromoform ND ug/kg 1 12/22/11 14:02 75-25-25.3
Bromomethane ND ug/kg 1 12/22/11 14:02 74-83-910.5
2-Butanone (MEK)ND ug/kg 1 12/22/11 14:02 78-93-3105
n-Butylbenzene ND ug/kg 1 12/22/11 14:02 104-51-85.3
sec-Butylbenzene ND ug/kg 1 12/22/11 14:02 135-98-85.3
tert-Butylbenzene ND ug/kg 1 12/22/11 14:02 98-06-65.3
Carbon tetrachloride ND ug/kg 1 12/22/11 14:02 56-23-55.3
Chlorobenzene ND ug/kg 1 12/22/11 14:02 108-90-75.3
Chloroethane ND ug/kg 1 12/22/11 14:02 75-00-310.5
Chloroform ND ug/kg 1 12/22/11 14:02 67-66-35.3
Chloromethane ND ug/kg 1 12/22/11 14:02 74-87-310.5
2-Chlorotoluene ND ug/kg 1 12/22/11 14:02 95-49-85.3
4-Chlorotoluene ND ug/kg 1 12/22/11 14:02 106-43-45.3
1,2-Dibromo-3-chloropropane ND ug/kg 1 12/22/11 14:02 96-12-85.3
Dibromochloromethane ND ug/kg 1 12/22/11 14:02 124-48-15.3
1,2-Dibromoethane (EDB)ND ug/kg 1 12/22/11 14:02 106-93-45.3
Dibromomethane ND ug/kg 1 12/22/11 14:02 74-95-35.3
1,2-Dichlorobenzene ND ug/kg 1 12/22/11 14:02 95-50-15.3
1,3-Dichlorobenzene ND ug/kg 1 12/22/11 14:02 541-73-15.3
1,4-Dichlorobenzene ND ug/kg 1 12/22/11 14:02 106-46-75.3
Dichlorodifluoromethane ND ug/kg 1 12/22/11 14:02 75-71-810.5
1,1-Dichloroethane ND ug/kg 1 12/22/11 14:02 75-34-35.3
1,2-Dichloroethane ND ug/kg 1 12/22/11 14:02 107-06-25.3
1,1-Dichloroethene ND ug/kg 1 12/22/11 14:02 75-35-45.3
cis-1,2-Dichloroethene ND ug/kg 1 12/22/11 14:02 156-59-25.3
trans-1,2-Dichloroethene ND ug/kg 1 12/22/11 14:02 156-60-55.3
1,2-Dichloropropane ND ug/kg 1 12/22/11 14:02 78-87-55.3
1,3-Dichloropropane ND ug/kg 1 12/22/11 14:02 142-28-95.3
2,2-Dichloropropane ND ug/kg 1 12/22/11 14:02 594-20-75.3
1,1-Dichloropropene ND ug/kg 1 12/22/11 14:02 563-58-65.3
cis-1,3-Dichloropropene ND ug/kg 1 12/22/11 14:02 10061-01-55.3
trans-1,3-Dichloropropene ND ug/kg 1 12/22/11 14:02 10061-02-65.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 21 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-6 (10')Lab ID:92108640010 Collected:12/15/11 13:25 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Diisopropyl ether ND ug/kg 1 12/22/11 14:02 108-20-35.3
Ethylbenzene ND ug/kg 1 12/22/11 14:02 100-41-45.3
Hexachloro-1,3-butadiene ND ug/kg 1 12/22/11 14:02 87-68-35.3
2-Hexanone ND ug/kg 1 12/22/11 14:02 591-78-652.7
Isopropylbenzene (Cumene)ND ug/kg 1 12/22/11 14:02 98-82-85.3
p-Isopropyltoluene ND ug/kg 1 12/22/11 14:02 99-87-65.3
Methylene Chloride ND ug/kg 1 12/22/11 14:02 75-09-221.1
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 12/22/11 14:02 108-10-152.7
Methyl-tert-butyl ether 18.4 ug/kg 1 12/22/11 14:02 1634-04-45.3
Naphthalene ND ug/kg 1 12/22/11 14:02 91-20-35.3
n-Propylbenzene ND ug/kg 1 12/22/11 14:02 103-65-15.3
Styrene ND ug/kg 1 12/22/11 14:02 100-42-55.3
1,1,1,2-Tetrachloroethane ND ug/kg 1 12/22/11 14:02 630-20-65.3
1,1,2,2-Tetrachloroethane ND ug/kg 1 12/22/11 14:02 79-34-55.3
Tetrachloroethene ND ug/kg 1 12/22/11 14:02 127-18-45.3
Toluene ND ug/kg 1 12/22/11 14:02 108-88-35.3
1,2,3-Trichlorobenzene ND ug/kg 1 12/22/11 14:02 87-61-65.3
1,2,4-Trichlorobenzene ND ug/kg 1 12/22/11 14:02 120-82-15.3
1,1,1-Trichloroethane ND ug/kg 1 12/22/11 14:02 71-55-65.3
1,1,2-Trichloroethane ND ug/kg 1 12/22/11 14:02 79-00-55.3
Trichloroethene ND ug/kg 1 12/22/11 14:02 79-01-65.3
Trichlorofluoromethane ND ug/kg 1 12/22/11 14:02 75-69-45.3
1,2,3-Trichloropropane ND ug/kg 1 12/22/11 14:02 96-18-45.3
1,2,4-Trimethylbenzene ND ug/kg 1 12/22/11 14:02 95-63-65.3
1,3,5-Trimethylbenzene ND ug/kg 1 12/22/11 14:02 108-67-85.3
Vinyl acetate ND ug/kg 1 12/22/11 14:02 108-05-452.7
Vinyl chloride ND ug/kg 1 12/22/11 14:02 75-01-410.5
Xylene (Total)ND ug/kg 1 12/22/11 14:02 1330-20-710.5
m&p-Xylene ND ug/kg 1 12/22/11 14:02 179601-23-110.5
o-Xylene ND ug/kg 1 12/22/11 14:02 95-47-65.3
Surrogates
Dibromofluoromethane (S)113 %1 12/22/11 14:02 1868-53-770-130
Toluene-d8 (S)101 %1 12/22/11 14:02 2037-26-570-130
4-Bromofluorobenzene (S)96 %1 12/22/11 14:02 460-00-470-130
1,2-Dichloroethane-d4 (S)105 %1 12/22/11 14:02 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 30.2 %1 12/19/11 09:000.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 22 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-6 (17')Lab ID:92108640011 Collected:12/15/11 13:30 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 12/21/11 17:50 67-64-1100
Benzene ND ug/kg 1 12/21/11 17:50 71-43-25.0
Bromobenzene ND ug/kg 1 12/21/11 17:50 108-86-15.0
Bromochloromethane ND ug/kg 1 12/21/11 17:50 74-97-55.0
Bromodichloromethane ND ug/kg 1 12/21/11 17:50 75-27-45.0
Bromoform ND ug/kg 1 12/21/11 17:50 75-25-25.0
Bromomethane ND ug/kg 1 12/21/11 17:50 74-83-910.0
2-Butanone (MEK)ND ug/kg 1 12/21/11 17:50 78-93-3100
n-Butylbenzene ND ug/kg 1 12/21/11 17:50 104-51-85.0
sec-Butylbenzene ND ug/kg 1 12/21/11 17:50 135-98-85.0
tert-Butylbenzene ND ug/kg 1 12/21/11 17:50 98-06-65.0
Carbon tetrachloride ND ug/kg 1 12/21/11 17:50 56-23-55.0
Chlorobenzene ND ug/kg 1 12/21/11 17:50 108-90-75.0
Chloroethane ND ug/kg 1 12/21/11 17:50 75-00-310.0
Chloroform ND ug/kg 1 12/21/11 17:50 67-66-35.0
Chloromethane ND ug/kg 1 12/21/11 17:50 74-87-310.0
2-Chlorotoluene ND ug/kg 1 12/21/11 17:50 95-49-85.0
4-Chlorotoluene ND ug/kg 1 12/21/11 17:50 106-43-45.0
1,2-Dibromo-3-chloropropane ND ug/kg 1 12/21/11 17:50 96-12-85.0
Dibromochloromethane ND ug/kg 1 12/21/11 17:50 124-48-15.0
1,2-Dibromoethane (EDB)ND ug/kg 1 12/21/11 17:50 106-93-45.0
Dibromomethane ND ug/kg 1 12/21/11 17:50 74-95-35.0
1,2-Dichlorobenzene ND ug/kg 1 12/21/11 17:50 95-50-15.0
1,3-Dichlorobenzene ND ug/kg 1 12/21/11 17:50 541-73-15.0
1,4-Dichlorobenzene ND ug/kg 1 12/21/11 17:50 106-46-75.0
Dichlorodifluoromethane ND ug/kg 1 12/21/11 17:50 75-71-810.0
1,1-Dichloroethane ND ug/kg 1 12/21/11 17:50 75-34-35.0
1,2-Dichloroethane ND ug/kg 1 12/21/11 17:50 107-06-25.0
1,1-Dichloroethene ND ug/kg 1 12/21/11 17:50 75-35-45.0
cis-1,2-Dichloroethene ND ug/kg 1 12/21/11 17:50 156-59-25.0
trans-1,2-Dichloroethene ND ug/kg 1 12/21/11 17:50 156-60-55.0
1,2-Dichloropropane ND ug/kg 1 12/21/11 17:50 78-87-55.0
1,3-Dichloropropane ND ug/kg 1 12/21/11 17:50 142-28-95.0
2,2-Dichloropropane ND ug/kg 1 12/21/11 17:50 594-20-75.0
1,1-Dichloropropene ND ug/kg 1 12/21/11 17:50 563-58-65.0
cis-1,3-Dichloropropene ND ug/kg 1 12/21/11 17:50 10061-01-55.0
trans-1,3-Dichloropropene ND ug/kg 1 12/21/11 17:50 10061-02-65.0
Diisopropyl ether ND ug/kg 1 12/21/11 17:50 108-20-35.0
Ethylbenzene ND ug/kg 1 12/21/11 17:50 100-41-45.0
Hexachloro-1,3-butadiene ND ug/kg 1 12/21/11 17:50 87-68-35.0
2-Hexanone ND ug/kg 1 12/21/11 17:50 591-78-650.0
Isopropylbenzene (Cumene)ND ug/kg 1 12/21/11 17:50 98-82-85.0
p-Isopropyltoluene ND ug/kg 1 12/21/11 17:50 99-87-65.0
Methylene Chloride ND ug/kg 1 12/21/11 17:50 75-09-220.0
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 12/21/11 17:50 108-10-150.0
Methyl-tert-butyl ether ND ug/kg 1 12/21/11 17:50 1634-04-45.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 23 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-6 (17')Lab ID:92108640011 Collected:12/15/11 13:30 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Naphthalene ND ug/kg 1 12/21/11 17:50 91-20-35.0
n-Propylbenzene ND ug/kg 1 12/21/11 17:50 103-65-15.0
Styrene ND ug/kg 1 12/21/11 17:50 100-42-55.0
1,1,1,2-Tetrachloroethane ND ug/kg 1 12/21/11 17:50 630-20-65.0
1,1,2,2-Tetrachloroethane ND ug/kg 1 12/21/11 17:50 79-34-55.0
Tetrachloroethene ND ug/kg 1 12/21/11 17:50 127-18-45.0
Toluene ND ug/kg 1 12/21/11 17:50 108-88-35.0
1,2,3-Trichlorobenzene ND ug/kg 1 12/21/11 17:50 87-61-65.0
1,2,4-Trichlorobenzene ND ug/kg 1 12/21/11 17:50 120-82-15.0
1,1,1-Trichloroethane ND ug/kg 1 12/21/11 17:50 71-55-65.0
1,1,2-Trichloroethane ND ug/kg 1 12/21/11 17:50 79-00-55.0
Trichloroethene ND ug/kg 1 12/21/11 17:50 79-01-65.0
Trichlorofluoromethane ND ug/kg 1 12/21/11 17:50 75-69-45.0
1,2,3-Trichloropropane ND ug/kg 1 12/21/11 17:50 96-18-45.0
1,2,4-Trimethylbenzene ND ug/kg 1 12/21/11 17:50 95-63-65.0
1,3,5-Trimethylbenzene ND ug/kg 1 12/21/11 17:50 108-67-85.0
Vinyl acetate ND ug/kg 1 12/21/11 17:50 108-05-450.0
Vinyl chloride ND ug/kg 1 12/21/11 17:50 75-01-410.0
Xylene (Total)ND ug/kg 1 12/21/11 17:50 1330-20-710.0
m&p-Xylene ND ug/kg 1 12/21/11 17:50 179601-23-110.0
o-Xylene ND ug/kg 1 12/21/11 17:50 95-47-65.0
Surrogates
Dibromofluoromethane (S)98 %1 12/21/11 17:50 1868-53-770-130
Toluene-d8 (S)100 %1 12/21/11 17:50 2037-26-570-130
4-Bromofluorobenzene (S)93 %1 12/21/11 17:50 460-00-470-130
1,2-Dichloroethane-d4 (S)93 %1 12/21/11 17:50 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 24.7 %1 12/19/11 09:000.10
Sample:SB-7 (7')Lab ID:92108640012 Collected:12/15/11 14:00 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 25 12/21/11 18:10 67-64-12290
Benzene ND ug/kg 25 12/21/11 18:10 71-43-2114
Bromobenzene ND ug/kg 25 12/21/11 18:10 108-86-1114
Bromochloromethane ND ug/kg 25 12/21/11 18:10 74-97-5114
Bromodichloromethane ND ug/kg 25 12/21/11 18:10 75-27-4114
Bromoform ND ug/kg 25 12/21/11 18:10 75-25-2114
Bromomethane ND ug/kg 25 12/21/11 18:10 74-83-9229
2-Butanone (MEK)ND ug/kg 25 12/21/11 18:10 78-93-32290
n-Butylbenzene ND ug/kg 25 12/21/11 18:10 104-51-8114
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 24 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-7 (7')Lab ID:92108640012 Collected:12/15/11 14:00 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
sec-Butylbenzene ND ug/kg 25 12/21/11 18:10 135-98-8114
tert-Butylbenzene ND ug/kg 25 12/21/11 18:10 98-06-6114
Carbon tetrachloride ND ug/kg 25 12/21/11 18:10 56-23-5114
Chlorobenzene ND ug/kg 25 12/21/11 18:10 108-90-7114
Chloroethane ND ug/kg 25 12/21/11 18:10 75-00-3229
Chloroform ND ug/kg 25 12/21/11 18:10 67-66-3114
Chloromethane ND ug/kg 25 12/21/11 18:10 74-87-3229
2-Chlorotoluene ND ug/kg 25 12/21/11 18:10 95-49-8114
4-Chlorotoluene ND ug/kg 25 12/21/11 18:10 106-43-4114
1,2-Dibromo-3-chloropropane ND ug/kg 25 12/21/11 18:10 96-12-8114
Dibromochloromethane ND ug/kg 25 12/21/11 18:10 124-48-1114
1,2-Dibromoethane (EDB)ND ug/kg 25 12/21/11 18:10 106-93-4114
Dibromomethane ND ug/kg 25 12/21/11 18:10 74-95-3114
1,2-Dichlorobenzene ND ug/kg 25 12/21/11 18:10 95-50-1114
1,3-Dichlorobenzene ND ug/kg 25 12/21/11 18:10 541-73-1114
1,4-Dichlorobenzene ND ug/kg 25 12/21/11 18:10 106-46-7114
Dichlorodifluoromethane ND ug/kg 25 12/21/11 18:10 75-71-8 D3229
1,1-Dichloroethane ND ug/kg 25 12/21/11 18:10 75-34-3114
1,2-Dichloroethane ND ug/kg 25 12/21/11 18:10 107-06-2114
1,1-Dichloroethene ND ug/kg 25 12/21/11 18:10 75-35-4114
cis-1,2-Dichloroethene ND ug/kg 25 12/21/11 18:10 156-59-2114
trans-1,2-Dichloroethene ND ug/kg 25 12/21/11 18:10 156-60-5114
1,2-Dichloropropane ND ug/kg 25 12/21/11 18:10 78-87-5114
1,3-Dichloropropane ND ug/kg 25 12/21/11 18:10 142-28-9114
2,2-Dichloropropane ND ug/kg 25 12/21/11 18:10 594-20-7114
1,1-Dichloropropene ND ug/kg 25 12/21/11 18:10 563-58-6114
cis-1,3-Dichloropropene ND ug/kg 25 12/21/11 18:10 10061-01-5114
trans-1,3-Dichloropropene ND ug/kg 25 12/21/11 18:10 10061-02-6114
Diisopropyl ether ND ug/kg 25 12/21/11 18:10 108-20-3114
Ethylbenzene ND ug/kg 25 12/21/11 18:10 100-41-4114
Hexachloro-1,3-butadiene ND ug/kg 25 12/21/11 18:10 87-68-3114
2-Hexanone ND ug/kg 25 12/21/11 18:10 591-78-61140
Isopropylbenzene (Cumene)ND ug/kg 25 12/21/11 18:10 98-82-8114
p-Isopropyltoluene ND ug/kg 25 12/21/11 18:10 99-87-6114
Methylene Chloride ND ug/kg 25 12/21/11 18:10 75-09-2458
4-Methyl-2-pentanone (MIBK)ND ug/kg 25 12/21/11 18:10 108-10-11140
Methyl-tert-butyl ether 808 ug/kg 25 12/21/11 18:10 1634-04-4114
Naphthalene ND ug/kg 25 12/21/11 18:10 91-20-3114
n-Propylbenzene ND ug/kg 25 12/21/11 18:10 103-65-1114
Styrene ND ug/kg 25 12/21/11 18:10 100-42-5114
1,1,1,2-Tetrachloroethane ND ug/kg 25 12/21/11 18:10 630-20-6114
1,1,2,2-Tetrachloroethane ND ug/kg 25 12/21/11 18:10 79-34-5114
Tetrachloroethene ND ug/kg 25 12/21/11 18:10 127-18-4114
Toluene ND ug/kg 25 12/21/11 18:10 108-88-3114
1,2,3-Trichlorobenzene ND ug/kg 25 12/21/11 18:10 87-61-6114
1,2,4-Trichlorobenzene ND ug/kg 25 12/21/11 18:10 120-82-1114
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 25 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-7 (7')Lab ID:92108640012 Collected:12/15/11 14:00 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1-Trichloroethane ND ug/kg 25 12/21/11 18:10 71-55-6114
1,1,2-Trichloroethane ND ug/kg 25 12/21/11 18:10 79-00-5114
Trichloroethene ND ug/kg 25 12/21/11 18:10 79-01-6114
Trichlorofluoromethane ND ug/kg 25 12/21/11 18:10 75-69-4114
1,2,3-Trichloropropane ND ug/kg 25 12/21/11 18:10 96-18-4114
1,2,4-Trimethylbenzene ND ug/kg 25 12/21/11 18:10 95-63-6114
1,3,5-Trimethylbenzene ND ug/kg 25 12/21/11 18:10 108-67-8114
Vinyl acetate ND ug/kg 25 12/21/11 18:10 108-05-41140
Vinyl chloride ND ug/kg 25 12/21/11 18:10 75-01-4229
Xylene (Total)ND ug/kg 25 12/21/11 18:10 1330-20-7229
m&p-Xylene ND ug/kg 25 12/21/11 18:10 179601-23-1229
o-Xylene ND ug/kg 25 12/21/11 18:10 95-47-6114
Surrogates
Dibromofluoromethane (S)101 %25 12/21/11 18:10 1868-53-770-130
Toluene-d8 (S)101 %25 12/21/11 18:10 2037-26-570-130
4-Bromofluorobenzene (S)93 %25 12/21/11 18:10 460-00-470-130
1,2-Dichloroethane-d4 (S)96 %25 12/21/11 18:10 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 20.2 %1 12/19/11 09:000.10
Sample:SB-7 (16')Lab ID:92108640013 Collected:12/15/11 14:05 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 25 12/21/11 18:30 67-64-12910
Benzene ND ug/kg 25 12/21/11 18:30 71-43-2145
Bromobenzene ND ug/kg 25 12/21/11 18:30 108-86-1145
Bromochloromethane ND ug/kg 25 12/21/11 18:30 74-97-5145
Bromodichloromethane ND ug/kg 25 12/21/11 18:30 75-27-4145
Bromoform ND ug/kg 25 12/21/11 18:30 75-25-2145
Bromomethane ND ug/kg 25 12/21/11 18:30 74-83-9291
2-Butanone (MEK)ND ug/kg 25 12/21/11 18:30 78-93-32910
n-Butylbenzene 172 ug/kg 25 12/21/11 18:30 104-51-8145
sec-Butylbenzene ND ug/kg 25 12/21/11 18:30 135-98-8145
tert-Butylbenzene ND ug/kg 25 12/21/11 18:30 98-06-6145
Carbon tetrachloride ND ug/kg 25 12/21/11 18:30 56-23-5145
Chlorobenzene ND ug/kg 25 12/21/11 18:30 108-90-7145
Chloroethane ND ug/kg 25 12/21/11 18:30 75-00-3291
Chloroform ND ug/kg 25 12/21/11 18:30 67-66-3145
Chloromethane ND ug/kg 25 12/21/11 18:30 74-87-3291
2-Chlorotoluene ND ug/kg 25 12/21/11 18:30 95-49-8145
4-Chlorotoluene ND ug/kg 25 12/21/11 18:30 106-43-4145
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 26 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-7 (16')Lab ID:92108640013 Collected:12/15/11 14:05 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dibromo-3-chloropropane ND ug/kg 25 12/21/11 18:30 96-12-8145
Dibromochloromethane ND ug/kg 25 12/21/11 18:30 124-48-1145
1,2-Dibromoethane (EDB)ND ug/kg 25 12/21/11 18:30 106-93-4145
Dibromomethane ND ug/kg 25 12/21/11 18:30 74-95-3145
1,2-Dichlorobenzene ND ug/kg 25 12/21/11 18:30 95-50-1145
1,3-Dichlorobenzene ND ug/kg 25 12/21/11 18:30 541-73-1145
1,4-Dichlorobenzene ND ug/kg 25 12/21/11 18:30 106-46-7145
Dichlorodifluoromethane ND ug/kg 25 12/21/11 18:30 75-71-8 D3291
1,1-Dichloroethane ND ug/kg 25 12/21/11 18:30 75-34-3145
1,2-Dichloroethane ND ug/kg 25 12/21/11 18:30 107-06-2145
1,1-Dichloroethene ND ug/kg 25 12/21/11 18:30 75-35-4145
cis-1,2-Dichloroethene 330 ug/kg 25 12/21/11 18:30 156-59-2145
trans-1,2-Dichloroethene ND ug/kg 25 12/21/11 18:30 156-60-5145
1,2-Dichloropropane ND ug/kg 25 12/21/11 18:30 78-87-5145
1,3-Dichloropropane ND ug/kg 25 12/21/11 18:30 142-28-9145
2,2-Dichloropropane ND ug/kg 25 12/21/11 18:30 594-20-7145
1,1-Dichloropropene ND ug/kg 25 12/21/11 18:30 563-58-6145
cis-1,3-Dichloropropene ND ug/kg 25 12/21/11 18:30 10061-01-5145
trans-1,3-Dichloropropene ND ug/kg 25 12/21/11 18:30 10061-02-6145
Diisopropyl ether ND ug/kg 25 12/21/11 18:30 108-20-3145
Ethylbenzene ND ug/kg 25 12/21/11 18:30 100-41-4145
Hexachloro-1,3-butadiene ND ug/kg 25 12/21/11 18:30 87-68-3145
2-Hexanone ND ug/kg 25 12/21/11 18:30 591-78-61450
Isopropylbenzene (Cumene)ND ug/kg 25 12/21/11 18:30 98-82-8145
p-Isopropyltoluene ND ug/kg 25 12/21/11 18:30 99-87-6145
Methylene Chloride ND ug/kg 25 12/21/11 18:30 75-09-2581
4-Methyl-2-pentanone (MIBK)ND ug/kg 25 12/21/11 18:30 108-10-11450
Methyl-tert-butyl ether 584 ug/kg 25 12/21/11 18:30 1634-04-4145
Naphthalene 511 ug/kg 25 12/21/11 18:30 91-20-3145
n-Propylbenzene ND ug/kg 25 12/21/11 18:30 103-65-1145
Styrene ND ug/kg 25 12/21/11 18:30 100-42-5145
1,1,1,2-Tetrachloroethane ND ug/kg 25 12/21/11 18:30 630-20-6145
1,1,2,2-Tetrachloroethane ND ug/kg 25 12/21/11 18:30 79-34-5145
Tetrachloroethene 321 ug/kg 25 12/21/11 18:30 127-18-4145
Toluene ND ug/kg 25 12/21/11 18:30 108-88-3145
1,2,3-Trichlorobenzene ND ug/kg 25 12/21/11 18:30 87-61-6145
1,2,4-Trichlorobenzene ND ug/kg 25 12/21/11 18:30 120-82-1145
1,1,1-Trichloroethane ND ug/kg 25 12/21/11 18:30 71-55-6145
1,1,2-Trichloroethane ND ug/kg 25 12/21/11 18:30 79-00-5145
Trichloroethene ND ug/kg 25 12/21/11 18:30 79-01-6145
Trichlorofluoromethane ND ug/kg 25 12/21/11 18:30 75-69-4145
1,2,3-Trichloropropane ND ug/kg 25 12/21/11 18:30 96-18-4145
1,2,4-Trimethylbenzene 542 ug/kg 25 12/21/11 18:30 95-63-6145
1,3,5-Trimethylbenzene ND ug/kg 25 12/21/11 18:30 108-67-8145
Vinyl acetate ND ug/kg 25 12/21/11 18:30 108-05-41450
Vinyl chloride ND ug/kg 25 12/21/11 18:30 75-01-4291
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 27 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-7 (16')Lab ID:92108640013 Collected:12/15/11 14:05 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Xylene (Total)ND ug/kg 25 12/21/11 18:30 1330-20-7291
m&p-Xylene ND ug/kg 25 12/21/11 18:30 179601-23-1291
o-Xylene ND ug/kg 25 12/21/11 18:30 95-47-6145
Surrogates
Dibromofluoromethane (S)102 %25 12/21/11 18:30 1868-53-770-130
Toluene-d8 (S)103 %25 12/21/11 18:30 2037-26-570-130
4-Bromofluorobenzene (S)96 %25 12/21/11 18:30 460-00-470-130
1,2-Dichloroethane-d4 (S)96 %25 12/21/11 18:30 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 29.8 %1 12/19/11 09:010.10
Sample:SB-8 (7')Lab ID:92108640014 Collected:12/15/11 14:30 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 12/21/11 18:50 67-64-195.2
Benzene ND ug/kg 1 12/21/11 18:50 71-43-24.8
Bromobenzene ND ug/kg 1 12/21/11 18:50 108-86-14.8
Bromochloromethane ND ug/kg 1 12/21/11 18:50 74-97-54.8
Bromodichloromethane ND ug/kg 1 12/21/11 18:50 75-27-44.8
Bromoform ND ug/kg 1 12/21/11 18:50 75-25-24.8
Bromomethane ND ug/kg 1 12/21/11 18:50 74-83-99.5
2-Butanone (MEK)ND ug/kg 1 12/21/11 18:50 78-93-395.2
n-Butylbenzene ND ug/kg 1 12/21/11 18:50 104-51-84.8
sec-Butylbenzene ND ug/kg 1 12/21/11 18:50 135-98-84.8
tert-Butylbenzene ND ug/kg 1 12/21/11 18:50 98-06-64.8
Carbon tetrachloride ND ug/kg 1 12/21/11 18:50 56-23-54.8
Chlorobenzene ND ug/kg 1 12/21/11 18:50 108-90-74.8
Chloroethane ND ug/kg 1 12/21/11 18:50 75-00-39.5
Chloroform ND ug/kg 1 12/21/11 18:50 67-66-34.8
Chloromethane ND ug/kg 1 12/21/11 18:50 74-87-39.5
2-Chlorotoluene ND ug/kg 1 12/21/11 18:50 95-49-84.8
4-Chlorotoluene ND ug/kg 1 12/21/11 18:50 106-43-44.8
1,2-Dibromo-3-chloropropane ND ug/kg 1 12/21/11 18:50 96-12-84.8
Dibromochloromethane ND ug/kg 1 12/21/11 18:50 124-48-14.8
1,2-Dibromoethane (EDB)ND ug/kg 1 12/21/11 18:50 106-93-44.8
Dibromomethane ND ug/kg 1 12/21/11 18:50 74-95-34.8
1,2-Dichlorobenzene ND ug/kg 1 12/21/11 18:50 95-50-14.8
1,3-Dichlorobenzene ND ug/kg 1 12/21/11 18:50 541-73-14.8
1,4-Dichlorobenzene ND ug/kg 1 12/21/11 18:50 106-46-74.8
Dichlorodifluoromethane ND ug/kg 1 12/21/11 18:50 75-71-89.5
1,1-Dichloroethane ND ug/kg 1 12/21/11 18:50 75-34-34.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 28 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-8 (7')Lab ID:92108640014 Collected:12/15/11 14:30 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dichloroethane ND ug/kg 1 12/21/11 18:50 107-06-24.8
1,1-Dichloroethene ND ug/kg 1 12/21/11 18:50 75-35-44.8
cis-1,2-Dichloroethene 8.7 ug/kg 1 12/21/11 18:50 156-59-24.8
trans-1,2-Dichloroethene ND ug/kg 1 12/21/11 18:50 156-60-54.8
1,2-Dichloropropane ND ug/kg 1 12/21/11 18:50 78-87-54.8
1,3-Dichloropropane ND ug/kg 1 12/21/11 18:50 142-28-94.8
2,2-Dichloropropane ND ug/kg 1 12/21/11 18:50 594-20-74.8
1,1-Dichloropropene ND ug/kg 1 12/21/11 18:50 563-58-64.8
cis-1,3-Dichloropropene ND ug/kg 1 12/21/11 18:50 10061-01-54.8
trans-1,3-Dichloropropene ND ug/kg 1 12/21/11 18:50 10061-02-64.8
Diisopropyl ether ND ug/kg 1 12/21/11 18:50 108-20-34.8
Ethylbenzene ND ug/kg 1 12/21/11 18:50 100-41-44.8
Hexachloro-1,3-butadiene ND ug/kg 1 12/21/11 18:50 87-68-34.8
2-Hexanone ND ug/kg 1 12/21/11 18:50 591-78-647.6
Isopropylbenzene (Cumene)ND ug/kg 1 12/21/11 18:50 98-82-84.8
p-Isopropyltoluene ND ug/kg 1 12/21/11 18:50 99-87-64.8
Methylene Chloride ND ug/kg 1 12/21/11 18:50 75-09-219.0
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 12/21/11 18:50 108-10-147.6
Methyl-tert-butyl ether 5.5 ug/kg 1 12/21/11 18:50 1634-04-44.8
Naphthalene ND ug/kg 1 12/21/11 18:50 91-20-34.8
n-Propylbenzene ND ug/kg 1 12/21/11 18:50 103-65-14.8
Styrene ND ug/kg 1 12/21/11 18:50 100-42-54.8
1,1,1,2-Tetrachloroethane ND ug/kg 1 12/21/11 18:50 630-20-64.8
1,1,2,2-Tetrachloroethane ND ug/kg 1 12/21/11 18:50 79-34-54.8
Tetrachloroethene ND ug/kg 1 12/21/11 18:50 127-18-44.8
Toluene ND ug/kg 1 12/21/11 18:50 108-88-34.8
1,2,3-Trichlorobenzene ND ug/kg 1 12/21/11 18:50 87-61-64.8
1,2,4-Trichlorobenzene ND ug/kg 1 12/21/11 18:50 120-82-14.8
1,1,1-Trichloroethane ND ug/kg 1 12/21/11 18:50 71-55-64.8
1,1,2-Trichloroethane ND ug/kg 1 12/21/11 18:50 79-00-54.8
Trichloroethene ND ug/kg 1 12/21/11 18:50 79-01-64.8
Trichlorofluoromethane ND ug/kg 1 12/21/11 18:50 75-69-44.8
1,2,3-Trichloropropane ND ug/kg 1 12/21/11 18:50 96-18-44.8
1,2,4-Trimethylbenzene ND ug/kg 1 12/21/11 18:50 95-63-64.8
1,3,5-Trimethylbenzene ND ug/kg 1 12/21/11 18:50 108-67-84.8
Vinyl acetate ND ug/kg 1 12/21/11 18:50 108-05-447.6
Vinyl chloride ND ug/kg 1 12/21/11 18:50 75-01-49.5
Xylene (Total)ND ug/kg 1 12/21/11 18:50 1330-20-79.5
m&p-Xylene ND ug/kg 1 12/21/11 18:50 179601-23-19.5
o-Xylene ND ug/kg 1 12/21/11 18:50 95-47-64.8
Surrogates
Dibromofluoromethane (S)96 %1 12/21/11 18:50 1868-53-770-130
Toluene-d8 (S)102 %1 12/21/11 18:50 2037-26-570-130
4-Bromofluorobenzene (S)97 %1 12/21/11 18:50 460-00-470-130
1,2-Dichloroethane-d4 (S)96 %1 12/21/11 18:50 17060-07-070-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 29 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-8 (7')Lab ID:92108640014 Collected:12/15/11 14:30 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 22.0 %1 12/19/11 09:010.10
Sample:SB-8 (16')Lab ID:92108640015 Collected:12/15/11 14:35 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 12/21/11 19:10 67-64-197.6
Benzene ND ug/kg 1 12/21/11 19:10 71-43-24.9
Bromobenzene ND ug/kg 1 12/21/11 19:10 108-86-14.9
Bromochloromethane ND ug/kg 1 12/21/11 19:10 74-97-54.9
Bromodichloromethane ND ug/kg 1 12/21/11 19:10 75-27-44.9
Bromoform ND ug/kg 1 12/21/11 19:10 75-25-24.9
Bromomethane ND ug/kg 1 12/21/11 19:10 74-83-99.8
2-Butanone (MEK)ND ug/kg 1 12/21/11 19:10 78-93-397.6
n-Butylbenzene ND ug/kg 1 12/21/11 19:10 104-51-84.9
sec-Butylbenzene ND ug/kg 1 12/21/11 19:10 135-98-84.9
tert-Butylbenzene ND ug/kg 1 12/21/11 19:10 98-06-64.9
Carbon tetrachloride ND ug/kg 1 12/21/11 19:10 56-23-54.9
Chlorobenzene ND ug/kg 1 12/21/11 19:10 108-90-74.9
Chloroethane ND ug/kg 1 12/21/11 19:10 75-00-39.8
Chloroform ND ug/kg 1 12/21/11 19:10 67-66-34.9
Chloromethane ND ug/kg 1 12/21/11 19:10 74-87-39.8
2-Chlorotoluene ND ug/kg 1 12/21/11 19:10 95-49-84.9
4-Chlorotoluene ND ug/kg 1 12/21/11 19:10 106-43-44.9
1,2-Dibromo-3-chloropropane ND ug/kg 1 12/21/11 19:10 96-12-84.9
Dibromochloromethane ND ug/kg 1 12/21/11 19:10 124-48-14.9
1,2-Dibromoethane (EDB)ND ug/kg 1 12/21/11 19:10 106-93-44.9
Dibromomethane ND ug/kg 1 12/21/11 19:10 74-95-34.9
1,2-Dichlorobenzene ND ug/kg 1 12/21/11 19:10 95-50-14.9
1,3-Dichlorobenzene ND ug/kg 1 12/21/11 19:10 541-73-14.9
1,4-Dichlorobenzene ND ug/kg 1 12/21/11 19:10 106-46-74.9
Dichlorodifluoromethane ND ug/kg 1 12/21/11 19:10 75-71-89.8
1,1-Dichloroethane ND ug/kg 1 12/21/11 19:10 75-34-34.9
1,2-Dichloroethane ND ug/kg 1 12/21/11 19:10 107-06-24.9
1,1-Dichloroethene ND ug/kg 1 12/21/11 19:10 75-35-44.9
cis-1,2-Dichloroethene 11.2 ug/kg 1 12/21/11 19:10 156-59-24.9
trans-1,2-Dichloroethene ND ug/kg 1 12/21/11 19:10 156-60-54.9
1,2-Dichloropropane ND ug/kg 1 12/21/11 19:10 78-87-54.9
1,3-Dichloropropane ND ug/kg 1 12/21/11 19:10 142-28-94.9
2,2-Dichloropropane ND ug/kg 1 12/21/11 19:10 594-20-74.9
1,1-Dichloropropene ND ug/kg 1 12/21/11 19:10 563-58-64.9
cis-1,3-Dichloropropene ND ug/kg 1 12/21/11 19:10 10061-01-54.9
trans-1,3-Dichloropropene ND ug/kg 1 12/21/11 19:10 10061-02-64.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 30 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-8 (16')Lab ID:92108640015 Collected:12/15/11 14:35 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Diisopropyl ether ND ug/kg 1 12/21/11 19:10 108-20-34.9
Ethylbenzene ND ug/kg 1 12/21/11 19:10 100-41-44.9
Hexachloro-1,3-butadiene ND ug/kg 1 12/21/11 19:10 87-68-34.9
2-Hexanone ND ug/kg 1 12/21/11 19:10 591-78-648.8
Isopropylbenzene (Cumene)ND ug/kg 1 12/21/11 19:10 98-82-84.9
p-Isopropyltoluene ND ug/kg 1 12/21/11 19:10 99-87-64.9
Methylene Chloride ND ug/kg 1 12/21/11 19:10 75-09-219.5
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 12/21/11 19:10 108-10-148.8
Methyl-tert-butyl ether ND ug/kg 1 12/21/11 19:10 1634-04-44.9
Naphthalene ND ug/kg 1 12/21/11 19:10 91-20-34.9
n-Propylbenzene ND ug/kg 1 12/21/11 19:10 103-65-14.9
Styrene ND ug/kg 1 12/21/11 19:10 100-42-54.9
1,1,1,2-Tetrachloroethane ND ug/kg 1 12/21/11 19:10 630-20-64.9
1,1,2,2-Tetrachloroethane ND ug/kg 1 12/21/11 19:10 79-34-54.9
Tetrachloroethene ND ug/kg 1 12/21/11 19:10 127-18-44.9
Toluene ND ug/kg 1 12/21/11 19:10 108-88-34.9
1,2,3-Trichlorobenzene ND ug/kg 1 12/21/11 19:10 87-61-64.9
1,2,4-Trichlorobenzene ND ug/kg 1 12/21/11 19:10 120-82-14.9
1,1,1-Trichloroethane ND ug/kg 1 12/21/11 19:10 71-55-64.9
1,1,2-Trichloroethane ND ug/kg 1 12/21/11 19:10 79-00-54.9
Trichloroethene ND ug/kg 1 12/21/11 19:10 79-01-64.9
Trichlorofluoromethane ND ug/kg 1 12/21/11 19:10 75-69-44.9
1,2,3-Trichloropropane ND ug/kg 1 12/21/11 19:10 96-18-44.9
1,2,4-Trimethylbenzene ND ug/kg 1 12/21/11 19:10 95-63-64.9
1,3,5-Trimethylbenzene ND ug/kg 1 12/21/11 19:10 108-67-84.9
Vinyl acetate ND ug/kg 1 12/21/11 19:10 108-05-448.8
Vinyl chloride ND ug/kg 1 12/21/11 19:10 75-01-49.8
Xylene (Total)ND ug/kg 1 12/21/11 19:10 1330-20-79.8
m&p-Xylene ND ug/kg 1 12/21/11 19:10 179601-23-19.8
o-Xylene ND ug/kg 1 12/21/11 19:10 95-47-64.9
Surrogates
Dibromofluoromethane (S)106 %1 12/21/11 19:10 1868-53-770-130
Toluene-d8 (S)102 %1 12/21/11 19:10 2037-26-570-130
4-Bromofluorobenzene (S)94 %1 12/21/11 19:10 460-00-470-130
1,2-Dichloroethane-d4 (S)98 %1 12/21/11 19:10 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 17.8 %1 12/19/11 09:010.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 31 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-9 (6')Lab ID:92108640016 Collected:12/15/11 15:00 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 12/21/11 19:30 67-64-186.8
Benzene ND ug/kg 1 12/21/11 19:30 71-43-24.3
Bromobenzene ND ug/kg 1 12/21/11 19:30 108-86-14.3
Bromochloromethane ND ug/kg 1 12/21/11 19:30 74-97-54.3
Bromodichloromethane ND ug/kg 1 12/21/11 19:30 75-27-44.3
Bromoform ND ug/kg 1 12/21/11 19:30 75-25-24.3
Bromomethane ND ug/kg 1 12/21/11 19:30 74-83-98.7
2-Butanone (MEK)ND ug/kg 1 12/21/11 19:30 78-93-386.8
n-Butylbenzene ND ug/kg 1 12/21/11 19:30 104-51-84.3
sec-Butylbenzene ND ug/kg 1 12/21/11 19:30 135-98-84.3
tert-Butylbenzene ND ug/kg 1 12/21/11 19:30 98-06-64.3
Carbon tetrachloride ND ug/kg 1 12/21/11 19:30 56-23-54.3
Chlorobenzene ND ug/kg 1 12/21/11 19:30 108-90-74.3
Chloroethane ND ug/kg 1 12/21/11 19:30 75-00-38.7
Chloroform ND ug/kg 1 12/21/11 19:30 67-66-34.3
Chloromethane ND ug/kg 1 12/21/11 19:30 74-87-38.7
2-Chlorotoluene ND ug/kg 1 12/21/11 19:30 95-49-84.3
4-Chlorotoluene ND ug/kg 1 12/21/11 19:30 106-43-44.3
1,2-Dibromo-3-chloropropane ND ug/kg 1 12/21/11 19:30 96-12-84.3
Dibromochloromethane ND ug/kg 1 12/21/11 19:30 124-48-14.3
1,2-Dibromoethane (EDB)ND ug/kg 1 12/21/11 19:30 106-93-44.3
Dibromomethane ND ug/kg 1 12/21/11 19:30 74-95-34.3
1,2-Dichlorobenzene ND ug/kg 1 12/21/11 19:30 95-50-14.3
1,3-Dichlorobenzene ND ug/kg 1 12/21/11 19:30 541-73-14.3
1,4-Dichlorobenzene ND ug/kg 1 12/21/11 19:30 106-46-74.3
Dichlorodifluoromethane ND ug/kg 1 12/21/11 19:30 75-71-88.7
1,1-Dichloroethane ND ug/kg 1 12/21/11 19:30 75-34-34.3
1,2-Dichloroethane ND ug/kg 1 12/21/11 19:30 107-06-24.3
1,1-Dichloroethene ND ug/kg 1 12/21/11 19:30 75-35-44.3
cis-1,2-Dichloroethene ND ug/kg 1 12/21/11 19:30 156-59-24.3
trans-1,2-Dichloroethene ND ug/kg 1 12/21/11 19:30 156-60-54.3
1,2-Dichloropropane ND ug/kg 1 12/21/11 19:30 78-87-54.3
1,3-Dichloropropane ND ug/kg 1 12/21/11 19:30 142-28-94.3
2,2-Dichloropropane ND ug/kg 1 12/21/11 19:30 594-20-74.3
1,1-Dichloropropene ND ug/kg 1 12/21/11 19:30 563-58-64.3
cis-1,3-Dichloropropene ND ug/kg 1 12/21/11 19:30 10061-01-54.3
trans-1,3-Dichloropropene ND ug/kg 1 12/21/11 19:30 10061-02-64.3
Diisopropyl ether ND ug/kg 1 12/21/11 19:30 108-20-34.3
Ethylbenzene ND ug/kg 1 12/21/11 19:30 100-41-44.3
Hexachloro-1,3-butadiene ND ug/kg 1 12/21/11 19:30 87-68-34.3
2-Hexanone ND ug/kg 1 12/21/11 19:30 591-78-643.4
Isopropylbenzene (Cumene)ND ug/kg 1 12/21/11 19:30 98-82-84.3
p-Isopropyltoluene ND ug/kg 1 12/21/11 19:30 99-87-64.3
Methylene Chloride ND ug/kg 1 12/21/11 19:30 75-09-217.4
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 12/21/11 19:30 108-10-143.4
Methyl-tert-butyl ether ND ug/kg 1 12/21/11 19:30 1634-04-44.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 32 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-9 (6')Lab ID:92108640016 Collected:12/15/11 15:00 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Naphthalene ND ug/kg 1 12/21/11 19:30 91-20-34.3
n-Propylbenzene ND ug/kg 1 12/21/11 19:30 103-65-14.3
Styrene ND ug/kg 1 12/21/11 19:30 100-42-54.3
1,1,1,2-Tetrachloroethane ND ug/kg 1 12/21/11 19:30 630-20-64.3
1,1,2,2-Tetrachloroethane ND ug/kg 1 12/21/11 19:30 79-34-54.3
Tetrachloroethene ND ug/kg 1 12/21/11 19:30 127-18-44.3
Toluene ND ug/kg 1 12/21/11 19:30 108-88-34.3
1,2,3-Trichlorobenzene ND ug/kg 1 12/21/11 19:30 87-61-64.3
1,2,4-Trichlorobenzene ND ug/kg 1 12/21/11 19:30 120-82-14.3
1,1,1-Trichloroethane ND ug/kg 1 12/21/11 19:30 71-55-64.3
1,1,2-Trichloroethane ND ug/kg 1 12/21/11 19:30 79-00-54.3
Trichloroethene ND ug/kg 1 12/21/11 19:30 79-01-64.3
Trichlorofluoromethane ND ug/kg 1 12/21/11 19:30 75-69-44.3
1,2,3-Trichloropropane ND ug/kg 1 12/21/11 19:30 96-18-44.3
1,2,4-Trimethylbenzene ND ug/kg 1 12/21/11 19:30 95-63-64.3
1,3,5-Trimethylbenzene ND ug/kg 1 12/21/11 19:30 108-67-84.3
Vinyl acetate ND ug/kg 1 12/21/11 19:30 108-05-443.4
Vinyl chloride ND ug/kg 1 12/21/11 19:30 75-01-48.7
Xylene (Total)ND ug/kg 1 12/21/11 19:30 1330-20-78.7
m&p-Xylene ND ug/kg 1 12/21/11 19:30 179601-23-18.7
o-Xylene ND ug/kg 1 12/21/11 19:30 95-47-64.3
Surrogates
Dibromofluoromethane (S)117 %1 12/21/11 19:30 1868-53-770-130
Toluene-d8 (S)100 %1 12/21/11 19:30 2037-26-570-130
4-Bromofluorobenzene (S)92 %1 12/21/11 19:30 460-00-470-130
1,2-Dichloroethane-d4 (S)109 %1 12/21/11 19:30 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 18.3 %1 12/19/11 09:010.10
Sample:SB-9 (16')Lab ID:92108640017 Collected:12/15/11 15:05 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 12/21/11 19:50 67-64-1107
Benzene ND ug/kg 1 12/21/11 19:50 71-43-25.4
Bromobenzene ND ug/kg 1 12/21/11 19:50 108-86-15.4
Bromochloromethane ND ug/kg 1 12/21/11 19:50 74-97-55.4
Bromodichloromethane ND ug/kg 1 12/21/11 19:50 75-27-45.4
Bromoform ND ug/kg 1 12/21/11 19:50 75-25-25.4
Bromomethane ND ug/kg 1 12/21/11 19:50 74-83-910.7
2-Butanone (MEK)ND ug/kg 1 12/21/11 19:50 78-93-3107
n-Butylbenzene ND ug/kg 1 12/21/11 19:50 104-51-85.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 33 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-9 (16')Lab ID:92108640017 Collected:12/15/11 15:05 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
sec-Butylbenzene ND ug/kg 1 12/21/11 19:50 135-98-85.4
tert-Butylbenzene ND ug/kg 1 12/21/11 19:50 98-06-65.4
Carbon tetrachloride ND ug/kg 1 12/21/11 19:50 56-23-55.4
Chlorobenzene ND ug/kg 1 12/21/11 19:50 108-90-75.4
Chloroethane ND ug/kg 1 12/21/11 19:50 75-00-310.7
Chloroform ND ug/kg 1 12/21/11 19:50 67-66-35.4
Chloromethane ND ug/kg 1 12/21/11 19:50 74-87-310.7
2-Chlorotoluene ND ug/kg 1 12/21/11 19:50 95-49-85.4
4-Chlorotoluene ND ug/kg 1 12/21/11 19:50 106-43-45.4
1,2-Dibromo-3-chloropropane ND ug/kg 1 12/21/11 19:50 96-12-85.4
Dibromochloromethane ND ug/kg 1 12/21/11 19:50 124-48-15.4
1,2-Dibromoethane (EDB)ND ug/kg 1 12/21/11 19:50 106-93-45.4
Dibromomethane ND ug/kg 1 12/21/11 19:50 74-95-35.4
1,2-Dichlorobenzene ND ug/kg 1 12/21/11 19:50 95-50-15.4
1,3-Dichlorobenzene ND ug/kg 1 12/21/11 19:50 541-73-15.4
1,4-Dichlorobenzene ND ug/kg 1 12/21/11 19:50 106-46-75.4
Dichlorodifluoromethane ND ug/kg 1 12/21/11 19:50 75-71-810.7
1,1-Dichloroethane ND ug/kg 1 12/21/11 19:50 75-34-35.4
1,2-Dichloroethane ND ug/kg 1 12/21/11 19:50 107-06-25.4
1,1-Dichloroethene ND ug/kg 1 12/21/11 19:50 75-35-45.4
cis-1,2-Dichloroethene ND ug/kg 1 12/21/11 19:50 156-59-25.4
trans-1,2-Dichloroethene ND ug/kg 1 12/21/11 19:50 156-60-55.4
1,2-Dichloropropane ND ug/kg 1 12/21/11 19:50 78-87-55.4
1,3-Dichloropropane ND ug/kg 1 12/21/11 19:50 142-28-95.4
2,2-Dichloropropane ND ug/kg 1 12/21/11 19:50 594-20-75.4
1,1-Dichloropropene ND ug/kg 1 12/21/11 19:50 563-58-65.4
cis-1,3-Dichloropropene ND ug/kg 1 12/21/11 19:50 10061-01-55.4
trans-1,3-Dichloropropene ND ug/kg 1 12/21/11 19:50 10061-02-65.4
Diisopropyl ether ND ug/kg 1 12/21/11 19:50 108-20-35.4
Ethylbenzene ND ug/kg 1 12/21/11 19:50 100-41-45.4
Hexachloro-1,3-butadiene ND ug/kg 1 12/21/11 19:50 87-68-35.4
2-Hexanone ND ug/kg 1 12/21/11 19:50 591-78-653.6
Isopropylbenzene (Cumene)ND ug/kg 1 12/21/11 19:50 98-82-85.4
p-Isopropyltoluene ND ug/kg 1 12/21/11 19:50 99-87-65.4
Methylene Chloride ND ug/kg 1 12/21/11 19:50 75-09-221.4
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 12/21/11 19:50 108-10-153.6
Methyl-tert-butyl ether ND ug/kg 1 12/21/11 19:50 1634-04-45.4
Naphthalene ND ug/kg 1 12/21/11 19:50 91-20-35.4
n-Propylbenzene ND ug/kg 1 12/21/11 19:50 103-65-15.4
Styrene ND ug/kg 1 12/21/11 19:50 100-42-55.4
1,1,1,2-Tetrachloroethane ND ug/kg 1 12/21/11 19:50 630-20-65.4
1,1,2,2-Tetrachloroethane ND ug/kg 1 12/21/11 19:50 79-34-55.4
Tetrachloroethene ND ug/kg 1 12/21/11 19:50 127-18-45.4
Toluene ND ug/kg 1 12/21/11 19:50 108-88-35.4
1,2,3-Trichlorobenzene ND ug/kg 1 12/21/11 19:50 87-61-65.4
1,2,4-Trichlorobenzene ND ug/kg 1 12/21/11 19:50 120-82-15.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 34 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-9 (16')Lab ID:92108640017 Collected:12/15/11 15:05 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1-Trichloroethane ND ug/kg 1 12/21/11 19:50 71-55-65.4
1,1,2-Trichloroethane ND ug/kg 1 12/21/11 19:50 79-00-55.4
Trichloroethene ND ug/kg 1 12/21/11 19:50 79-01-65.4
Trichlorofluoromethane ND ug/kg 1 12/21/11 19:50 75-69-45.4
1,2,3-Trichloropropane ND ug/kg 1 12/21/11 19:50 96-18-45.4
1,2,4-Trimethylbenzene ND ug/kg 1 12/21/11 19:50 95-63-65.4
1,3,5-Trimethylbenzene ND ug/kg 1 12/21/11 19:50 108-67-85.4
Vinyl acetate ND ug/kg 1 12/21/11 19:50 108-05-453.6
Vinyl chloride ND ug/kg 1 12/21/11 19:50 75-01-410.7
Xylene (Total)ND ug/kg 1 12/21/11 19:50 1330-20-710.7
m&p-Xylene ND ug/kg 1 12/21/11 19:50 179601-23-110.7
o-Xylene ND ug/kg 1 12/21/11 19:50 95-47-65.4
Surrogates
Dibromofluoromethane (S)102 %1 12/21/11 19:50 1868-53-770-130
Toluene-d8 (S)102 %1 12/21/11 19:50 2037-26-570-130
4-Bromofluorobenzene (S)94 %1 12/21/11 19:50 460-00-470-130
1,2-Dichloroethane-d4 (S)94 %1 12/21/11 19:50 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 26.8 %1 12/19/11 09:010.10
Sample:SB-10 (10')Lab ID:92108640018 Collected:12/15/11 15:30 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 12/21/11 20:10 67-64-1103
Benzene ND ug/kg 1 12/21/11 20:10 71-43-25.2
Bromobenzene ND ug/kg 1 12/21/11 20:10 108-86-15.2
Bromochloromethane ND ug/kg 1 12/21/11 20:10 74-97-55.2
Bromodichloromethane ND ug/kg 1 12/21/11 20:10 75-27-45.2
Bromoform ND ug/kg 1 12/21/11 20:10 75-25-25.2
Bromomethane ND ug/kg 1 12/21/11 20:10 74-83-910.3
2-Butanone (MEK)ND ug/kg 1 12/21/11 20:10 78-93-3103
n-Butylbenzene 5.3 ug/kg 1 12/21/11 20:10 104-51-85.2
sec-Butylbenzene ND ug/kg 1 12/21/11 20:10 135-98-85.2
tert-Butylbenzene ND ug/kg 1 12/21/11 20:10 98-06-65.2
Carbon tetrachloride ND ug/kg 1 12/21/11 20:10 56-23-55.2
Chlorobenzene ND ug/kg 1 12/21/11 20:10 108-90-75.2
Chloroethane ND ug/kg 1 12/21/11 20:10 75-00-310.3
Chloroform ND ug/kg 1 12/21/11 20:10 67-66-35.2
Chloromethane ND ug/kg 1 12/21/11 20:10 74-87-310.3
2-Chlorotoluene ND ug/kg 1 12/21/11 20:10 95-49-85.2
4-Chlorotoluene ND ug/kg 1 12/21/11 20:10 106-43-45.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 35 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-10 (10')Lab ID:92108640018 Collected:12/15/11 15:30 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dibromo-3-chloropropane ND ug/kg 1 12/21/11 20:10 96-12-85.2
Dibromochloromethane ND ug/kg 1 12/21/11 20:10 124-48-15.2
1,2-Dibromoethane (EDB)ND ug/kg 1 12/21/11 20:10 106-93-45.2
Dibromomethane ND ug/kg 1 12/21/11 20:10 74-95-35.2
1,2-Dichlorobenzene ND ug/kg 1 12/21/11 20:10 95-50-15.2
1,3-Dichlorobenzene ND ug/kg 1 12/21/11 20:10 541-73-15.2
1,4-Dichlorobenzene ND ug/kg 1 12/21/11 20:10 106-46-75.2
Dichlorodifluoromethane ND ug/kg 1 12/21/11 20:10 75-71-810.3
1,1-Dichloroethane 5.2 ug/kg 1 12/21/11 20:10 75-34-35.2
1,2-Dichloroethane ND ug/kg 1 12/21/11 20:10 107-06-25.2
1,1-Dichloroethene ND ug/kg 1 12/21/11 20:10 75-35-45.2
cis-1,2-Dichloroethene 53.5 ug/kg 1 12/21/11 20:10 156-59-25.2
trans-1,2-Dichloroethene ND ug/kg 1 12/21/11 20:10 156-60-55.2
1,2-Dichloropropane ND ug/kg 1 12/21/11 20:10 78-87-55.2
1,3-Dichloropropane ND ug/kg 1 12/21/11 20:10 142-28-95.2
2,2-Dichloropropane ND ug/kg 1 12/21/11 20:10 594-20-75.2
1,1-Dichloropropene ND ug/kg 1 12/21/11 20:10 563-58-65.2
cis-1,3-Dichloropropene ND ug/kg 1 12/21/11 20:10 10061-01-55.2
trans-1,3-Dichloropropene ND ug/kg 1 12/21/11 20:10 10061-02-65.2
Diisopropyl ether ND ug/kg 1 12/21/11 20:10 108-20-35.2
Ethylbenzene ND ug/kg 1 12/21/11 20:10 100-41-45.2
Hexachloro-1,3-butadiene ND ug/kg 1 12/21/11 20:10 87-68-35.2
2-Hexanone ND ug/kg 1 12/21/11 20:10 591-78-651.7
Isopropylbenzene (Cumene)ND ug/kg 1 12/21/11 20:10 98-82-85.2
p-Isopropyltoluene 7.4 ug/kg 1 12/21/11 20:10 99-87-65.2
Methylene Chloride ND ug/kg 1 12/21/11 20:10 75-09-220.7
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 12/21/11 20:10 108-10-151.7
Methyl-tert-butyl ether 6.5 ug/kg 1 12/21/11 20:10 1634-04-45.2
Naphthalene 80.5 ug/kg 1 12/21/11 20:10 91-20-35.2
n-Propylbenzene ND ug/kg 1 12/21/11 20:10 103-65-15.2
Styrene ND ug/kg 1 12/21/11 20:10 100-42-55.2
1,1,1,2-Tetrachloroethane ND ug/kg 1 12/21/11 20:10 630-20-65.2
1,1,2,2-Tetrachloroethane ND ug/kg 1 12/21/11 20:10 79-34-55.2
Tetrachloroethene ND ug/kg 1 12/21/11 20:10 127-18-45.2
Toluene ND ug/kg 1 12/21/11 20:10 108-88-35.2
1,2,3-Trichlorobenzene ND ug/kg 1 12/21/11 20:10 87-61-65.2
1,2,4-Trichlorobenzene ND ug/kg 1 12/21/11 20:10 120-82-15.2
1,1,1-Trichloroethane ND ug/kg 1 12/21/11 20:10 71-55-65.2
1,1,2-Trichloroethane ND ug/kg 1 12/21/11 20:10 79-00-55.2
Trichloroethene ND ug/kg 1 12/21/11 20:10 79-01-65.2
Trichlorofluoromethane ND ug/kg 1 12/21/11 20:10 75-69-45.2
1,2,3-Trichloropropane ND ug/kg 1 12/21/11 20:10 96-18-45.2
1,2,4-Trimethylbenzene 39.1 ug/kg 1 12/21/11 20:10 95-63-65.2
1,3,5-Trimethylbenzene 9.4 ug/kg 1 12/21/11 20:10 108-67-85.2
Vinyl acetate ND ug/kg 1 12/21/11 20:10 108-05-451.7
Vinyl chloride ND ug/kg 1 12/21/11 20:10 75-01-410.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 36 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-10 (10')Lab ID:92108640018 Collected:12/15/11 15:30 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Xylene (Total)31.4 ug/kg 1 12/21/11 20:10 1330-20-710.3
m&p-Xylene 19.5 ug/kg 1 12/21/11 20:10 179601-23-110.3
o-Xylene 11.9 ug/kg 1 12/21/11 20:10 95-47-65.2
Surrogates
Dibromofluoromethane (S)103 %1 12/21/11 20:10 1868-53-770-130
Toluene-d8 (S)101 %1 12/21/11 20:10 2037-26-570-130
4-Bromofluorobenzene (S)99 %1 12/21/11 20:10 460-00-470-130
1,2-Dichloroethane-d4 (S)98 %1 12/21/11 20:10 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 23.5 %1 12/19/11 09:010.10
Sample:SB-10 (17')Lab ID:92108640019 Collected:12/15/11 15:35 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 12/21/11 20:30 67-64-1114
Benzene ND ug/kg 1 12/21/11 20:30 71-43-25.7
Bromobenzene ND ug/kg 1 12/21/11 20:30 108-86-15.7
Bromochloromethane ND ug/kg 1 12/21/11 20:30 74-97-55.7
Bromodichloromethane ND ug/kg 1 12/21/11 20:30 75-27-45.7
Bromoform ND ug/kg 1 12/21/11 20:30 75-25-25.7
Bromomethane ND ug/kg 1 12/21/11 20:30 74-83-911.4
2-Butanone (MEK)ND ug/kg 1 12/21/11 20:30 78-93-3114
n-Butylbenzene ND ug/kg 1 12/21/11 20:30 104-51-85.7
sec-Butylbenzene ND ug/kg 1 12/21/11 20:30 135-98-85.7
tert-Butylbenzene ND ug/kg 1 12/21/11 20:30 98-06-65.7
Carbon tetrachloride ND ug/kg 1 12/21/11 20:30 56-23-55.7
Chlorobenzene ND ug/kg 1 12/21/11 20:30 108-90-75.7
Chloroethane ND ug/kg 1 12/21/11 20:30 75-00-311.4
Chloroform ND ug/kg 1 12/21/11 20:30 67-66-35.7
Chloromethane ND ug/kg 1 12/21/11 20:30 74-87-311.4
2-Chlorotoluene ND ug/kg 1 12/21/11 20:30 95-49-85.7
4-Chlorotoluene ND ug/kg 1 12/21/11 20:30 106-43-45.7
1,2-Dibromo-3-chloropropane ND ug/kg 1 12/21/11 20:30 96-12-85.7
Dibromochloromethane ND ug/kg 1 12/21/11 20:30 124-48-15.7
1,2-Dibromoethane (EDB)ND ug/kg 1 12/21/11 20:30 106-93-45.7
Dibromomethane ND ug/kg 1 12/21/11 20:30 74-95-35.7
1,2-Dichlorobenzene ND ug/kg 1 12/21/11 20:30 95-50-15.7
1,3-Dichlorobenzene ND ug/kg 1 12/21/11 20:30 541-73-15.7
1,4-Dichlorobenzene ND ug/kg 1 12/21/11 20:30 106-46-75.7
Dichlorodifluoromethane ND ug/kg 1 12/21/11 20:30 75-71-811.4
1,1-Dichloroethane 9.5 ug/kg 1 12/21/11 20:30 75-34-35.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 37 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-10 (17')Lab ID:92108640019 Collected:12/15/11 15:35 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dichloroethane ND ug/kg 1 12/21/11 20:30 107-06-25.7
1,1-Dichloroethene ND ug/kg 1 12/21/11 20:30 75-35-45.7
cis-1,2-Dichloroethene 85.6 ug/kg 1 12/21/11 20:30 156-59-25.7
trans-1,2-Dichloroethene ND ug/kg 1 12/21/11 20:30 156-60-55.7
1,2-Dichloropropane ND ug/kg 1 12/21/11 20:30 78-87-55.7
1,3-Dichloropropane ND ug/kg 1 12/21/11 20:30 142-28-95.7
2,2-Dichloropropane ND ug/kg 1 12/21/11 20:30 594-20-75.7
1,1-Dichloropropene ND ug/kg 1 12/21/11 20:30 563-58-65.7
cis-1,3-Dichloropropene ND ug/kg 1 12/21/11 20:30 10061-01-55.7
trans-1,3-Dichloropropene ND ug/kg 1 12/21/11 20:30 10061-02-65.7
Diisopropyl ether ND ug/kg 1 12/21/11 20:30 108-20-35.7
Ethylbenzene ND ug/kg 1 12/21/11 20:30 100-41-45.7
Hexachloro-1,3-butadiene ND ug/kg 1 12/21/11 20:30 87-68-35.7
2-Hexanone ND ug/kg 1 12/21/11 20:30 591-78-656.9
Isopropylbenzene (Cumene)ND ug/kg 1 12/21/11 20:30 98-82-85.7
p-Isopropyltoluene ND ug/kg 1 12/21/11 20:30 99-87-65.7
Methylene Chloride ND ug/kg 1 12/21/11 20:30 75-09-222.8
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 12/21/11 20:30 108-10-156.9
Methyl-tert-butyl ether 6.7 ug/kg 1 12/21/11 20:30 1634-04-45.7
Naphthalene ND ug/kg 1 12/21/11 20:30 91-20-35.7
n-Propylbenzene ND ug/kg 1 12/21/11 20:30 103-65-15.7
Styrene ND ug/kg 1 12/21/11 20:30 100-42-55.7
1,1,1,2-Tetrachloroethane ND ug/kg 1 12/21/11 20:30 630-20-65.7
1,1,2,2-Tetrachloroethane ND ug/kg 1 12/21/11 20:30 79-34-55.7
Tetrachloroethene ND ug/kg 1 12/21/11 20:30 127-18-45.7
Toluene ND ug/kg 1 12/21/11 20:30 108-88-35.7
1,2,3-Trichlorobenzene ND ug/kg 1 12/21/11 20:30 87-61-65.7
1,2,4-Trichlorobenzene ND ug/kg 1 12/21/11 20:30 120-82-15.7
1,1,1-Trichloroethane ND ug/kg 1 12/21/11 20:30 71-55-65.7
1,1,2-Trichloroethane ND ug/kg 1 12/21/11 20:30 79-00-55.7
Trichloroethene ND ug/kg 1 12/21/11 20:30 79-01-65.7
Trichlorofluoromethane ND ug/kg 1 12/21/11 20:30 75-69-45.7
1,2,3-Trichloropropane ND ug/kg 1 12/21/11 20:30 96-18-45.7
1,2,4-Trimethylbenzene 10.6 ug/kg 1 12/21/11 20:30 95-63-65.7
1,3,5-Trimethylbenzene ND ug/kg 1 12/21/11 20:30 108-67-85.7
Vinyl acetate ND ug/kg 1 12/21/11 20:30 108-05-456.9
Vinyl chloride ND ug/kg 1 12/21/11 20:30 75-01-411.4
Xylene (Total)42.3 ug/kg 1 12/21/11 20:30 1330-20-711.4
m&p-Xylene 26.0 ug/kg 1 12/21/11 20:30 179601-23-111.4
o-Xylene 16.3 ug/kg 1 12/21/11 20:30 95-47-65.7
Surrogates
Dibromofluoromethane (S)102 %1 12/21/11 20:30 1868-53-770-130
Toluene-d8 (S)105 %1 12/21/11 20:30 2037-26-570-130
4-Bromofluorobenzene (S)98 %1 12/21/11 20:30 460-00-470-130
1,2-Dichloroethane-d4 (S)91 %1 12/21/11 20:30 17060-07-070-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 38 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Sample:SB-10 (17')Lab ID:92108640019 Collected:12/15/11 15:35 Received:12/16/11 09:34 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 28.4 %1 12/20/11 08:170.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 39 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/17724
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92108640001, 92108640003, 92108640005, 92108640006, 92108640009, 92108640011, 92108640012,
92108640013, 92108640014, 92108640015, 92108640016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:702584
Associated Lab Samples:92108640001, 92108640003, 92108640005, 92108640006, 92108640009, 92108640011, 92108640012,
92108640013, 92108640014, 92108640015, 92108640016
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 4.7 12/21/11 11:10
1,1,1-Trichloroethane ug/kg ND 4.7 12/21/11 11:10
1,1,2,2-Tetrachloroethane ug/kg ND 4.7 12/21/11 11:10
1,1,2-Trichloroethane ug/kg ND 4.7 12/21/11 11:10
1,1-Dichloroethane ug/kg ND 4.7 12/21/11 11:10
1,1-Dichloroethene ug/kg ND 4.7 12/21/11 11:10
1,1-Dichloropropene ug/kg ND 4.7 12/21/11 11:10
1,2,3-Trichlorobenzene ug/kg ND 4.7 12/21/11 11:10
1,2,3-Trichloropropane ug/kg ND 4.7 12/21/11 11:10
1,2,4-Trichlorobenzene ug/kg ND 4.7 12/21/11 11:10
1,2,4-Trimethylbenzene ug/kg ND 4.7 12/21/11 11:10
1,2-Dibromo-3-chloropropane ug/kg ND 4.7 12/21/11 11:10
1,2-Dibromoethane (EDB)ug/kg ND 4.7 12/21/11 11:10
1,2-Dichlorobenzene ug/kg ND 4.7 12/21/11 11:10
1,2-Dichloroethane ug/kg ND 4.7 12/21/11 11:10
1,2-Dichloropropane ug/kg ND 4.7 12/21/11 11:10
1,3,5-Trimethylbenzene ug/kg ND 4.7 12/21/11 11:10
1,3-Dichlorobenzene ug/kg ND 4.7 12/21/11 11:10
1,3-Dichloropropane ug/kg ND 4.7 12/21/11 11:10
1,4-Dichlorobenzene ug/kg ND 4.7 12/21/11 11:10
2,2-Dichloropropane ug/kg ND 4.7 12/21/11 11:10
2-Butanone (MEK)ug/kg ND 94.7 12/21/11 11:10
2-Chlorotoluene ug/kg ND 4.7 12/21/11 11:10
2-Hexanone ug/kg ND 47.3 12/21/11 11:10
4-Chlorotoluene ug/kg ND 4.7 12/21/11 11:10
4-Methyl-2-pentanone (MIBK)ug/kg ND 47.3 12/21/11 11:10
Acetone ug/kg ND 94.7 12/21/11 11:10
Benzene ug/kg ND 4.7 12/21/11 11:10
Bromobenzene ug/kg ND 4.7 12/21/11 11:10
Bromochloromethane ug/kg ND 4.7 12/21/11 11:10
Bromodichloromethane ug/kg ND 4.7 12/21/11 11:10
Bromoform ug/kg ND 4.7 12/21/11 11:10
Bromomethane ug/kg ND 9.5 12/21/11 11:10
Carbon tetrachloride ug/kg ND 4.7 12/21/11 11:10
Chlorobenzene ug/kg ND 4.7 12/21/11 11:10
Chloroethane ug/kg ND 9.5 12/21/11 11:10
Chloroform ug/kg ND 4.7 12/21/11 11:10
Chloromethane ug/kg ND 9.5 12/21/11 11:10
cis-1,2-Dichloroethene ug/kg ND 4.7 12/21/11 11:10
cis-1,3-Dichloropropene ug/kg ND 4.7 12/21/11 11:10
Dibromochloromethane ug/kg ND 4.7 12/21/11 11:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 40 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:702584
Associated Lab Samples:92108640001, 92108640003, 92108640005, 92108640006, 92108640009, 92108640011, 92108640012,
92108640013, 92108640014, 92108640015, 92108640016
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 4.7 12/21/11 11:10
Dichlorodifluoromethane ug/kg ND 9.5 12/21/11 11:10
Diisopropyl ether ug/kg ND 4.7 12/21/11 11:10
Ethylbenzene ug/kg ND 4.7 12/21/11 11:10
Hexachloro-1,3-butadiene ug/kg ND 4.7 12/21/11 11:10
Isopropylbenzene (Cumene)ug/kg ND 4.7 12/21/11 11:10
m&p-Xylene ug/kg ND 9.5 12/21/11 11:10
Methyl-tert-butyl ether ug/kg ND 4.7 12/21/11 11:10
Methylene Chloride ug/kg ND 18.9 12/21/11 11:10
n-Butylbenzene ug/kg ND 4.7 12/21/11 11:10
n-Propylbenzene ug/kg ND 4.7 12/21/11 11:10
Naphthalene ug/kg ND 4.7 12/21/11 11:10
o-Xylene ug/kg ND 4.7 12/21/11 11:10
p-Isopropyltoluene ug/kg ND 4.7 12/21/11 11:10
sec-Butylbenzene ug/kg ND 4.7 12/21/11 11:10
Styrene ug/kg ND 4.7 12/21/11 11:10
tert-Butylbenzene ug/kg ND 4.7 12/21/11 11:10
Tetrachloroethene ug/kg ND 4.7 12/21/11 11:10
Toluene ug/kg ND 4.7 12/21/11 11:10
trans-1,2-Dichloroethene ug/kg ND 4.7 12/21/11 11:10
trans-1,3-Dichloropropene ug/kg ND 4.7 12/21/11 11:10
Trichloroethene ug/kg ND 4.7 12/21/11 11:10
Trichlorofluoromethane ug/kg ND 4.7 12/21/11 11:10
Vinyl acetate ug/kg ND 47.3 12/21/11 11:10
Vinyl chloride ug/kg ND 9.5 12/21/11 11:10
Xylene (Total)ug/kg ND 9.5 12/21/11 11:10
1,2-Dichloroethane-d4 (S)%102 70-132 12/21/11 11:10
4-Bromofluorobenzene (S)%96 70-130 12/21/11 11:10
Dibromofluoromethane (S)%107 70-130 12/21/11 11:10
Toluene-d8 (S)%100 70-130 12/21/11 11:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
702585LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 55.650.4 110 70-131
1,1,1-Trichloroethane ug/kg 49.350.4 98 70-141
1,1,2,2-Tetrachloroethane ug/kg 55.450.4 110 70-130
1,1,2-Trichloroethane ug/kg 50.850.4 101 70-132
1,1-Dichloroethane ug/kg 54.650.4 108 70-143
1,1-Dichloroethene ug/kg 51.250.4 102 70-137
1,1-Dichloropropene ug/kg 49.350.4 98 70-135
1,2,3-Trichlorobenzene ug/kg 51.350.4 102 69-153
1,2,3-Trichloropropane ug/kg 51.150.4 101 70-130
1,2,4-Trichlorobenzene ug/kg 53.450.4 106 55-171
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 41 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
702585LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 53.450.4 106 70-149
1,2-Dibromo-3-chloropropane ug/kg 53.950.4 107 68-141
1,2-Dibromoethane (EDB)ug/kg 56.450.4 112 70-130
1,2-Dichlorobenzene ug/kg 53.750.4 107 70-140
1,2-Dichloroethane ug/kg 54.450.4 108 70-137
1,2-Dichloropropane ug/kg 53.750.4 106 70-133
1,3,5-Trimethylbenzene ug/kg 52.750.4 105 70-143
1,3-Dichlorobenzene ug/kg 53.650.4 106 70-144
1,3-Dichloropropane ug/kg 52.550.4 104 70-132
1,4-Dichlorobenzene ug/kg 54.050.4 107 70-142
2,2-Dichloropropane ug/kg 51.950.4 103 68-152
2-Butanone (MEK)ug/kg ND101 100 70-149
2-Chlorotoluene ug/kg 54.250.4 107 70-141
2-Hexanone ug/kg 106101 105 70-149
4-Chlorotoluene ug/kg 56.250.4 111 70-149
4-Methyl-2-pentanone (MIBK)ug/kg 101101 101 70-153
Acetone ug/kg 113101 112 70-157
Benzene ug/kg 53.850.4 107 70-130
Bromobenzene ug/kg 50.650.4 100 70-141
Bromochloromethane ug/kg 50.150.4 99 70-149
Bromodichloromethane ug/kg 51.550.4 102 70-130
Bromoform ug/kg 55.950.4 111 70-131
Bromomethane ug/kg 51.650.4 102 64-136
Carbon tetrachloride ug/kg 53.550.4 106 70-154
Chlorobenzene ug/kg 55.050.4 109 70-135
Chloroethane ug/kg 47.650.4 94 68-151
Chloroform ug/kg 52.650.4 104 70-130
Chloromethane ug/kg 46.350.4 92 70-132
cis-1,2-Dichloroethene ug/kg 48.250.4 96 70-140
cis-1,3-Dichloropropene ug/kg 52.150.4 103 70-137
Dibromochloromethane ug/kg 53.750.4 107 70-130
Dibromomethane ug/kg 47.550.4 94 70-136
Dichlorodifluoromethane ug/kg 45.950.4 91 36-148
Diisopropyl ether ug/kg 47.950.4 95 70-139
Ethylbenzene ug/kg 53.850.4 107 70-137
Hexachloro-1,3-butadiene ug/kg 53.950.4 107 70-145
Isopropylbenzene (Cumene)ug/kg 53.150.4 105 70-141
m&p-Xylene ug/kg 106101 105 70-140
Methyl-tert-butyl ether ug/kg 49.450.4 98 45-150
Methylene Chloride ug/kg 51.250.4 102 70-133
n-Butylbenzene ug/kg 53.550.4 106 65-155
n-Propylbenzene ug/kg 52.150.4 103 70-148
Naphthalene ug/kg 53.350.4 106 70-148
o-Xylene ug/kg 52.250.4 103 70-141
p-Isopropyltoluene ug/kg 54.050.4 107 70-148
sec-Butylbenzene ug/kg 51.250.4 102 70-145
Styrene ug/kg 54.650.4 108 70-138
tert-Butylbenzene ug/kg 51.250.4 102 70-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 42 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
702585LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 52.350.4 104 70-140
Toluene ug/kg 50.850.4 101 70-130
trans-1,2-Dichloroethene ug/kg 49.250.4 98 70-136
trans-1,3-Dichloropropene ug/kg 53.350.4 106 70-138
Trichloroethene ug/kg 55.150.4 109 70-132
Trichlorofluoromethane ug/kg 46.850.4 93 69-134
Vinyl acetate ug/kg 95.1101 94 24-161
Vinyl chloride ug/kg 48.550.4 96 55-140
Xylene (Total)ug/kg 158151 104 70-141
1,2-Dichloroethane-d4 (S)%102 70-132
4-Bromofluorobenzene (S)%101 70-130
Dibromofluoromethane (S)%103 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
703293MATRIX SPIKE SAMPLE:
MSSpike
Result
92108640006
1,1-Dichloroethene ug/kg 42.746.1 92 49-180ND
Benzene ug/kg 40.946.1 85 50-166ND
Chlorobenzene ug/kg 46.746.1 101 43-169ND
Toluene ug/kg 42.646.1 92 52-163ND
Trichloroethene ug/kg 43.846.1 95 49-167ND
1,2-Dichloroethane-d4 (S)%97 70-132
4-Bromofluorobenzene (S)%96 70-130
Dibromofluoromethane (S)%106 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92108640001
703292SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg 2.2JND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 43 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Parameter Units
Dup
Result QualifiersRPDResult
92108640001
703292SAMPLE DUPLICATE:
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg 10.9 R1586.0
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg 36.4 R13924.4
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg 6.3ND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg 23.5 1819.5
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg 3.9JND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 44 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Parameter Units
Dup
Result QualifiersRPDResult
92108640001
703292SAMPLE DUPLICATE:
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg 7.3JND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%95 393
4-Bromofluorobenzene (S)%98 197
Dibromofluoromethane (S)%102 697
Toluene-d8 (S)%102 2101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 45 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/17725
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92108640017, 92108640018, 92108640019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:702586
Associated Lab Samples:92108640017, 92108640018, 92108640019
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.1 12/21/11 10:50
1,1,1-Trichloroethane ug/kg ND 5.1 12/21/11 10:50
1,1,2,2-Tetrachloroethane ug/kg ND 5.1 12/21/11 10:50
1,1,2-Trichloroethane ug/kg ND 5.1 12/21/11 10:50
1,1-Dichloroethane ug/kg ND 5.1 12/21/11 10:50
1,1-Dichloroethene ug/kg ND 5.1 12/21/11 10:50
1,1-Dichloropropene ug/kg ND 5.1 12/21/11 10:50
1,2,3-Trichlorobenzene ug/kg ND 5.1 12/21/11 10:50
1,2,3-Trichloropropane ug/kg ND 5.1 12/21/11 10:50
1,2,4-Trichlorobenzene ug/kg ND 5.1 12/21/11 10:50
1,2,4-Trimethylbenzene ug/kg ND 5.1 12/21/11 10:50
1,2-Dibromo-3-chloropropane ug/kg ND 5.1 12/21/11 10:50
1,2-Dibromoethane (EDB)ug/kg ND 5.1 12/21/11 10:50
1,2-Dichlorobenzene ug/kg ND 5.1 12/21/11 10:50
1,2-Dichloroethane ug/kg ND 5.1 12/21/11 10:50
1,2-Dichloropropane ug/kg ND 5.1 12/21/11 10:50
1,3,5-Trimethylbenzene ug/kg ND 5.1 12/21/11 10:50
1,3-Dichlorobenzene ug/kg ND 5.1 12/21/11 10:50
1,3-Dichloropropane ug/kg ND 5.1 12/21/11 10:50
1,4-Dichlorobenzene ug/kg ND 5.1 12/21/11 10:50
2,2-Dichloropropane ug/kg ND 5.1 12/21/11 10:50
2-Butanone (MEK)ug/kg ND 101 12/21/11 10:50
2-Chlorotoluene ug/kg ND 5.1 12/21/11 10:50
2-Hexanone ug/kg ND 50.5 12/21/11 10:50
4-Chlorotoluene ug/kg ND 5.1 12/21/11 10:50
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.5 12/21/11 10:50
Acetone ug/kg ND 101 12/21/11 10:50
Benzene ug/kg ND 5.1 12/21/11 10:50
Bromobenzene ug/kg ND 5.1 12/21/11 10:50
Bromochloromethane ug/kg ND 5.1 12/21/11 10:50
Bromodichloromethane ug/kg ND 5.1 12/21/11 10:50
Bromoform ug/kg ND 5.1 12/21/11 10:50
Bromomethane ug/kg ND 10.1 12/21/11 10:50
Carbon tetrachloride ug/kg ND 5.1 12/21/11 10:50
Chlorobenzene ug/kg ND 5.1 12/21/11 10:50
Chloroethane ug/kg ND 10.1 12/21/11 10:50
Chloroform ug/kg ND 5.1 12/21/11 10:50
Chloromethane ug/kg ND 10.1 12/21/11 10:50
cis-1,2-Dichloroethene ug/kg ND 5.1 12/21/11 10:50
cis-1,3-Dichloropropene ug/kg ND 5.1 12/21/11 10:50
Dibromochloromethane ug/kg ND 5.1 12/21/11 10:50
Dibromomethane ug/kg ND 5.1 12/21/11 10:50
Dichlorodifluoromethane ug/kg ND 10.1 12/21/11 10:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 46 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:702586
Associated Lab Samples:92108640017, 92108640018, 92108640019
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.1 12/21/11 10:50
Ethylbenzene ug/kg ND 5.1 12/21/11 10:50
Hexachloro-1,3-butadiene ug/kg ND 5.1 12/21/11 10:50
Isopropylbenzene (Cumene)ug/kg ND 5.1 12/21/11 10:50
m&p-Xylene ug/kg ND 10.1 12/21/11 10:50
Methyl-tert-butyl ether ug/kg ND 5.1 12/21/11 10:50
Methylene Chloride ug/kg ND 20.2 12/21/11 10:50
n-Butylbenzene ug/kg ND 5.1 12/21/11 10:50
n-Propylbenzene ug/kg ND 5.1 12/21/11 10:50
Naphthalene ug/kg ND 5.1 12/21/11 10:50
o-Xylene ug/kg ND 5.1 12/21/11 10:50
p-Isopropyltoluene ug/kg ND 5.1 12/21/11 10:50
sec-Butylbenzene ug/kg ND 5.1 12/21/11 10:50
Styrene ug/kg ND 5.1 12/21/11 10:50
tert-Butylbenzene ug/kg ND 5.1 12/21/11 10:50
Tetrachloroethene ug/kg ND 5.1 12/21/11 10:50
Toluene ug/kg ND 5.1 12/21/11 10:50
trans-1,2-Dichloroethene ug/kg ND 5.1 12/21/11 10:50
trans-1,3-Dichloropropene ug/kg ND 5.1 12/21/11 10:50
Trichloroethene ug/kg ND 5.1 12/21/11 10:50
Trichlorofluoromethane ug/kg ND 5.1 12/21/11 10:50
Vinyl acetate ug/kg ND 50.5 12/21/11 10:50
Vinyl chloride ug/kg ND 10.1 12/21/11 10:50
Xylene (Total)ug/kg ND 10.1 12/21/11 10:50
1,2-Dichloroethane-d4 (S)%99 70-132 12/21/11 10:50
4-Bromofluorobenzene (S)%96 70-130 12/21/11 10:50
Dibromofluoromethane (S)%104 70-130 12/21/11 10:50
Toluene-d8 (S)%101 70-130 12/21/11 10:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
702587LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 48.044.5 108 70-131
1,1,1-Trichloroethane ug/kg 45.744.5 103 70-141
1,1,2,2-Tetrachloroethane ug/kg 48.644.5 109 70-130
1,1,2-Trichloroethane ug/kg 47.544.5 107 70-132
1,1-Dichloroethane ug/kg 43.644.5 98 70-143
1,1-Dichloroethene ug/kg 45.644.5 102 70-137
1,1-Dichloropropene ug/kg 46.144.5 104 70-135
1,2,3-Trichlorobenzene ug/kg 48.644.5 109 69-153
1,2,3-Trichloropropane ug/kg 44.744.5 101 70-130
1,2,4-Trichlorobenzene ug/kg 50.344.5 113 55-171
1,2,4-Trimethylbenzene ug/kg 50.244.5 113 70-149
1,2-Dibromo-3-chloropropane ug/kg 50.144.5 113 68-141
1,2-Dibromoethane (EDB)ug/kg 49.244.5 111 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 47 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
702587LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 51.344.5 115 70-140
1,2-Dichloroethane ug/kg 48.944.5 110 70-137
1,2-Dichloropropane ug/kg 49.344.5 111 70-133
1,3,5-Trimethylbenzene ug/kg 48.944.5 110 70-143
1,3-Dichlorobenzene ug/kg 49.744.5 112 70-144
1,3-Dichloropropane ug/kg 45.244.5 102 70-132
1,4-Dichlorobenzene ug/kg 50.644.5 114 70-142
2,2-Dichloropropane ug/kg 46.144.5 104 68-152
2-Butanone (MEK)ug/kg 10289 115 70-149
2-Chlorotoluene ug/kg 44.944.5 101 70-141
2-Hexanone ug/kg 94.989 107 70-149
4-Chlorotoluene ug/kg 53.244.5 119 70-149
4-Methyl-2-pentanone (MIBK)ug/kg 98.989 111 70-153
Acetone ug/kg 97.289 109 70-157
Benzene ug/kg 49.744.5 112 70-130
Bromobenzene ug/kg 42.944.5 97 70-141
Bromochloromethane ug/kg 44.944.5 101 70-149
Bromodichloromethane ug/kg 47.944.5 108 70-130
Bromoform ug/kg 47.544.5 107 70-131
Bromomethane ug/kg 46.344.5 104 64-136
Carbon tetrachloride ug/kg 50.044.5 112 70-154
Chlorobenzene ug/kg 49.744.5 112 70-135
Chloroethane ug/kg 48.544.5 109 68-151
Chloroform ug/kg 47.444.5 106 70-130
Chloromethane ug/kg 42.344.5 95 70-132
cis-1,2-Dichloroethene ug/kg 42.344.5 95 70-140
cis-1,3-Dichloropropene ug/kg 48.244.5 108 70-137
Dibromochloromethane ug/kg 46.244.5 104 70-130
Dibromomethane ug/kg 43.844.5 99 70-136
Dichlorodifluoromethane ug/kg 41.744.5 94 36-148
Diisopropyl ether ug/kg 43.444.5 98 70-139
Ethylbenzene ug/kg 48.444.5 109 70-137
Hexachloro-1,3-butadiene ug/kg 47.644.5 107 70-145
Isopropylbenzene (Cumene)ug/kg 47.244.5 106 70-141
m&p-Xylene ug/kg 95.389 107 70-140
Methyl-tert-butyl ether ug/kg 44.144.5 99 45-150
Methylene Chloride ug/kg 51.144.5 115 70-133
n-Butylbenzene ug/kg 50.644.5 114 65-155
n-Propylbenzene ug/kg 48.844.5 110 70-148
Naphthalene ug/kg 51.144.5 115 70-148
o-Xylene ug/kg 44.244.5 99 70-141
p-Isopropyltoluene ug/kg 50.844.5 114 70-148
sec-Butylbenzene ug/kg 48.544.5 109 70-145
Styrene ug/kg 53.344.5 120 70-138
tert-Butylbenzene ug/kg 48.244.5 108 70-143
Tetrachloroethene ug/kg 46.744.5 105 70-140
Toluene ug/kg 49.344.5 111 70-130
trans-1,2-Dichloroethene ug/kg 43.444.5 98 70-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 48 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
702587LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 49.644.5 111 70-138
Trichloroethene ug/kg 51.444.5 116 70-132
Trichlorofluoromethane ug/kg 45.544.5 102 69-134
Vinyl acetate ug/kg 79.489 89 24-161
Vinyl chloride ug/kg 44.844.5 101 55-140
Xylene (Total)ug/kg 140133 105 70-141
1,2-Dichloroethane-d4 (S)%101 70-132
4-Bromofluorobenzene (S)%98 70-130
Dibromofluoromethane (S)%94 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 49 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/17733
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92108640002, 92108640004, 92108640007, 92108640008, 92108640010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:703372
Associated Lab Samples:92108640002, 92108640004, 92108640007, 92108640008, 92108640010
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 12/22/11 10:23
1,1,1-Trichloroethane ug/kg ND 5.0 12/22/11 10:23
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 12/22/11 10:23
1,1,2-Trichloroethane ug/kg ND 5.0 12/22/11 10:23
1,1-Dichloroethane ug/kg ND 5.0 12/22/11 10:23
1,1-Dichloroethene ug/kg ND 5.0 12/22/11 10:23
1,1-Dichloropropene ug/kg ND 5.0 12/22/11 10:23
1,2,3-Trichlorobenzene ug/kg ND 5.0 12/22/11 10:23
1,2,3-Trichloropropane ug/kg ND 5.0 12/22/11 10:23
1,2,4-Trichlorobenzene ug/kg ND 5.0 12/22/11 10:23
1,2,4-Trimethylbenzene ug/kg ND 5.0 12/22/11 10:23
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 12/22/11 10:23
1,2-Dibromoethane (EDB)ug/kg ND 5.0 12/22/11 10:23
1,2-Dichlorobenzene ug/kg ND 5.0 12/22/11 10:23
1,2-Dichloroethane ug/kg ND 5.0 12/22/11 10:23
1,2-Dichloropropane ug/kg ND 5.0 12/22/11 10:23
1,3,5-Trimethylbenzene ug/kg ND 5.0 12/22/11 10:23
1,3-Dichlorobenzene ug/kg ND 5.0 12/22/11 10:23
1,3-Dichloropropane ug/kg ND 5.0 12/22/11 10:23
1,4-Dichlorobenzene ug/kg ND 5.0 12/22/11 10:23
2,2-Dichloropropane ug/kg ND 5.0 12/22/11 10:23
2-Butanone (MEK)ug/kg ND 101 12/22/11 10:23
2-Chlorotoluene ug/kg ND 5.0 12/22/11 10:23
2-Hexanone ug/kg ND 50.3 12/22/11 10:23
4-Chlorotoluene ug/kg ND 5.0 12/22/11 10:23
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.3 12/22/11 10:23
Acetone ug/kg ND 101 12/22/11 10:23
Benzene ug/kg ND 5.0 12/22/11 10:23
Bromobenzene ug/kg ND 5.0 12/22/11 10:23
Bromochloromethane ug/kg ND 5.0 12/22/11 10:23
Bromodichloromethane ug/kg ND 5.0 12/22/11 10:23
Bromoform ug/kg ND 5.0 12/22/11 10:23
Bromomethane ug/kg ND 10.1 12/22/11 10:23
Carbon tetrachloride ug/kg ND 5.0 12/22/11 10:23
Chlorobenzene ug/kg ND 5.0 12/22/11 10:23
Chloroethane ug/kg ND 10.1 12/22/11 10:23
Chloroform ug/kg ND 5.0 12/22/11 10:23
Chloromethane ug/kg ND 10.1 12/22/11 10:23
cis-1,2-Dichloroethene ug/kg ND 5.0 12/22/11 10:23
cis-1,3-Dichloropropene ug/kg ND 5.0 12/22/11 10:23
Dibromochloromethane ug/kg ND 5.0 12/22/11 10:23
Dibromomethane ug/kg ND 5.0 12/22/11 10:23
Dichlorodifluoromethane ug/kg ND 10.1 12/22/11 10:23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 50 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:703372
Associated Lab Samples:92108640002, 92108640004, 92108640007, 92108640008, 92108640010
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.0 12/22/11 10:23
Ethylbenzene ug/kg ND 5.0 12/22/11 10:23
Hexachloro-1,3-butadiene ug/kg ND 5.0 12/22/11 10:23
Isopropylbenzene (Cumene)ug/kg ND 5.0 12/22/11 10:23
m&p-Xylene ug/kg ND 10.1 12/22/11 10:23
Methyl-tert-butyl ether ug/kg ND 5.0 12/22/11 10:23
Methylene Chloride ug/kg ND 20.1 12/22/11 10:23
n-Butylbenzene ug/kg ND 5.0 12/22/11 10:23
n-Propylbenzene ug/kg ND 5.0 12/22/11 10:23
Naphthalene ug/kg ND 5.0 12/22/11 10:23
o-Xylene ug/kg ND 5.0 12/22/11 10:23
p-Isopropyltoluene ug/kg ND 5.0 12/22/11 10:23
sec-Butylbenzene ug/kg ND 5.0 12/22/11 10:23
Styrene ug/kg ND 5.0 12/22/11 10:23
tert-Butylbenzene ug/kg ND 5.0 12/22/11 10:23
Tetrachloroethene ug/kg ND 5.0 12/22/11 10:23
Toluene ug/kg ND 5.0 12/22/11 10:23
trans-1,2-Dichloroethene ug/kg ND 5.0 12/22/11 10:23
trans-1,3-Dichloropropene ug/kg ND 5.0 12/22/11 10:23
Trichloroethene ug/kg ND 5.0 12/22/11 10:23
Trichlorofluoromethane ug/kg ND 5.0 12/22/11 10:23
Vinyl acetate ug/kg ND 50.3 12/22/11 10:23
Vinyl chloride ug/kg ND 10.1 12/22/11 10:23
Xylene (Total)ug/kg ND 10.1 12/22/11 10:23
1,2-Dichloroethane-d4 (S)%104 70-132 12/22/11 10:23
4-Bromofluorobenzene (S)%99 70-130 12/22/11 10:23
Dibromofluoromethane (S)%108 70-130 12/22/11 10:23
Toluene-d8 (S)%101 70-130 12/22/11 10:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
703373LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 61.952.9 117 70-131
1,1,1-Trichloroethane ug/kg 58.352.9 110 70-141
1,1,2,2-Tetrachloroethane ug/kg 64.052.9 121 70-130
1,1,2-Trichloroethane ug/kg 61.752.9 117 70-132
1,1-Dichloroethane ug/kg 70.352.9 133 70-143
1,1-Dichloroethene ug/kg 60.152.9 114 70-137
1,1-Dichloropropene ug/kg 57.852.9 109 70-135
1,2,3-Trichlorobenzene ug/kg 60.552.9 114 69-153
1,2,3-Trichloropropane ug/kg 59.852.9 113 70-130
1,2,4-Trichlorobenzene ug/kg 62.152.9 118 55-171
1,2,4-Trimethylbenzene ug/kg 62.152.9 118 70-149
1,2-Dibromo-3-chloropropane ug/kg 65.852.9 124 68-141
1,2-Dibromoethane (EDB)ug/kg 63.352.9 120 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 51 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
703373LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 62.552.9 118 70-140
1,2-Dichloroethane ug/kg 64.952.9 123 70-137
1,2-Dichloropropane ug/kg 60.652.9 115 70-133
1,3,5-Trimethylbenzene ug/kg 60.952.9 115 70-143
1,3-Dichlorobenzene ug/kg 60.652.9 115 70-144
1,3-Dichloropropane ug/kg 59.652.9 113 70-132
1,4-Dichlorobenzene ug/kg 61.852.9 117 70-142
2,2-Dichloropropane ug/kg 55.852.9 106 68-152
2-Butanone (MEK)ug/kg 118106 111 70-149
2-Chlorotoluene ug/kg 62.052.9 117 70-141
2-Hexanone ug/kg 123106 116 70-149
4-Chlorotoluene ug/kg 65.852.9 124 70-149
4-Methyl-2-pentanone (MIBK)ug/kg 122106 115 70-153
Acetone ug/kg 137106 129 70-157
Benzene ug/kg 62.652.9 119 70-130
Bromobenzene ug/kg 58.752.9 111 70-141
Bromochloromethane ug/kg 62.052.9 117 70-149
Bromodichloromethane ug/kg 61.552.9 116 70-130
Bromoform ug/kg 61.252.9 116 70-131
Bromomethane ug/kg 60.452.9 114 64-136
Carbon tetrachloride ug/kg 62.352.9 118 70-154
Chlorobenzene ug/kg 62.652.9 118 70-135
Chloroethane ug/kg 61.252.9 116 68-151
Chloroform ug/kg 61.152.9 116 70-130
Chloromethane ug/kg 54.452.9 103 70-132
cis-1,2-Dichloroethene ug/kg 56.752.9 107 70-140
cis-1,3-Dichloropropene ug/kg 60.252.9 114 70-137
Dibromochloromethane ug/kg 59.652.9 113 70-130
Dibromomethane ug/kg 54.052.9 102 70-136
Dichlorodifluoromethane ug/kg 51.252.9 97 36-148
Diisopropyl ether ug/kg 57.052.9 108 70-139
Ethylbenzene ug/kg 59.952.9 113 70-137
Hexachloro-1,3-butadiene ug/kg 59.552.9 113 70-145
Isopropylbenzene (Cumene)ug/kg 59.952.9 113 70-141
m&p-Xylene ug/kg 119106 113 70-140
Methyl-tert-butyl ether ug/kg 56.752.9 107 45-150
Methylene Chloride ug/kg 58.652.9 111 70-133
n-Butylbenzene ug/kg 61.852.9 117 65-155
n-Propylbenzene ug/kg 59.752.9 113 70-148
Naphthalene ug/kg 63.052.9 119 70-148
o-Xylene ug/kg 58.252.9 110 70-141
p-Isopropyltoluene ug/kg 62.252.9 118 70-148
sec-Butylbenzene ug/kg 60.052.9 114 70-145
Styrene ug/kg 60.752.9 115 70-138
tert-Butylbenzene ug/kg 58.252.9 110 70-143
Tetrachloroethene ug/kg 58.152.9 110 70-140
Toluene ug/kg 59.752.9 113 70-130
trans-1,2-Dichloroethene ug/kg 57.952.9 110 70-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 52 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
703373LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 63.252.9 120 70-138
Trichloroethene ug/kg 64.352.9 122 70-132
Trichlorofluoromethane ug/kg 59.952.9 113 69-134
Vinyl acetate ug/kg 119106 112 24-161
Vinyl chloride ug/kg 55.552.9 105 55-140
Xylene (Total)ug/kg 177159 112 70-141
1,2-Dichloroethane-d4 (S)%108 70-132
4-Bromofluorobenzene (S)%99 70-130
Dibromofluoromethane (S)%106 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 53 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/4392
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92108640001, 92108640002, 92108640003, 92108640004, 92108640005, 92108640006, 92108640007,
92108640008, 92108640009, 92108640010, 92108640011, 92108640012, 92108640013, 92108640014,
92108640015, 92108640016, 92108640017, 92108640018
Parameter Units
Dup
Result QualifiersRPDResult
92108637001
700913SAMPLE DUPLICATE:
Percent Moisture %18.9 617.9
Parameter Units
Dup
Result QualifiersRPDResult
92108640018
700914SAMPLE DUPLICATE:
Percent Moisture %25.5 823.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 54 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/4393
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92108640019
Parameter Units
Dup
Result QualifiersRPDResult
92108582001
701661SAMPLE DUPLICATE:
Percent Moisture %47.4 047.3
Parameter Units
Dup
Result QualifiersRPDResult
92108688010
701662SAMPLE DUPLICATE:
Percent Moisture %27.4 127.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 55 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Project No.:
Project:
92108640
DIMMETTE CHARLOTTE 6228095100
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/22/2011 04:33 PM Page 56 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
APPENDIX C
AMEC Environment and Infrastructure, Inc.
APPENDIX CLABORATORYREPORT OF ANALYSES –GROUNDWATER SAMPLES
(JUNE 2014)
#=CL#
June 19, 2014
LIMS USE: FR - ROB FOSTER
LIMS OBJECT ID: 92205134
92205134
Project:
Pace Project No.:
RE:
Mr. Rob Foster
AMEC-Charlotte
2801 Yorkmont Road Suite 100
Charlotte, NC 28208
SPATCO
Dear Mr. Foster:
Enclosed are the analytical results for sample(s) received by the laboratory on June 12, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 19
Reviewed by RFoster on 6-19-2014.
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92205134
SPATCO
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 19
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92205134
SPATCO
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92205134001 1823 CANNON EPA 6010 2 PASI-AJMW
EPA 625 60 PASI-CBPJ
SM 6200B 69 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92205134
SPATCO
Sample: 1823 CANNON Lab ID: 92205134001 Collected: 06/12/14 10:30 Received: 06/12/14 11:32 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium ND ug/L 06/17/14 03:52 7440-47-306/16/14 11:005.0 1
Lead ND ug/L 06/17/14 03:52 7439-92-106/16/14 11:005.0 1
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/18/14 22:19 83-32-906/16/14 11:085.0 1
Acenaphthylene ND ug/L 06/18/14 22:19 208-96-806/16/14 11:085.0 1
Anthracene ND ug/L 06/18/14 22:19 120-12-706/16/14 11:085.0 1
Benzo(a)anthracene ND ug/L 06/18/14 22:19 56-55-306/16/14 11:085.0 1
Benzo(a)pyrene ND ug/L 06/18/14 22:19 50-32-806/16/14 11:085.0 1
Benzo(b)fluoranthene ND ug/L 06/18/14 22:19 205-99-206/16/14 11:085.0 1
Benzo(g,h,i)perylene ND ug/L 06/18/14 22:19 191-24-206/16/14 11:085.0 1
Benzo(k)fluoranthene ND ug/L 06/18/14 22:19 207-08-906/16/14 11:085.0 1
4-Bromophenylphenyl ether ND ug/L 06/18/14 22:19 101-55-306/16/14 11:085.0 1
Butylbenzylphthalate ND ug/L 06/18/14 22:19 85-68-706/16/14 11:085.0 1
4-Chloro-3-methylphenol ND ug/L 06/18/14 22:19 59-50-706/16/14 11:085.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/18/14 22:19 111-91-106/16/14 11:0810.0 1
bis(2-Chloroethyl) ether ND ug/L 06/18/14 22:19 111-44-406/16/14 11:085.0 1
bis(2-Chloroisopropyl) ether ND ug/L 06/18/14 22:19 108-60-106/16/14 11:085.0 1
2-Chloronaphthalene ND ug/L 06/18/14 22:19 91-58-706/16/14 11:085.0 1
2-Chlorophenol ND ug/L 06/18/14 22:19 95-57-806/16/14 11:085.0 1
4-Chlorophenylphenyl ether ND ug/L 06/18/14 22:19 7005-72-306/16/14 11:085.0 1
Chrysene ND ug/L 06/18/14 22:19 218-01-906/16/14 11:085.0 1
Dibenz(a,h)anthracene ND ug/L 06/18/14 22:19 53-70-306/16/14 11:085.0 1
3,3'-Dichlorobenzidine ND ug/L 06/18/14 22:19 91-94-106/16/14 11:0825.0 1
2,4-Dichlorophenol ND ug/L 06/18/14 22:19 120-83-206/16/14 11:085.0 1
Diethylphthalate ND ug/L 06/18/14 22:19 84-66-206/16/14 11:085.0 1
2,4-Dimethylphenol ND ug/L 06/18/14 22:19 105-67-906/16/14 11:0810.0 1
Dimethylphthalate ND ug/L 06/18/14 22:19 131-11-306/16/14 11:085.0 1
Di-n-butylphthalate ND ug/L 06/18/14 22:19 84-74-206/16/14 11:085.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/18/14 22:19 534-52-106/16/14 11:0820.0 1
2,4-Dinitrophenol ND ug/L 06/18/14 22:19 51-28-506/16/14 11:0850.0 1
2,4-Dinitrotoluene ND ug/L 06/18/14 22:19 121-14-206/16/14 11:085.0 1
2,6-Dinitrotoluene ND ug/L 06/18/14 22:19 606-20-206/16/14 11:085.0 1
Di-n-octylphthalate ND ug/L 06/18/14 22:19 117-84-006/16/14 11:085.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/18/14 22:19 117-81-706/16/14 11:085.0 1
Fluoranthene ND ug/L 06/18/14 22:19 206-44-006/16/14 11:085.0 1
Fluorene ND ug/L 06/18/14 22:19 86-73-706/16/14 11:085.0 1
Hexachloro-1,3-butadiene ND ug/L 06/18/14 22:19 87-68-306/16/14 11:085.0 1
Hexachlorobenzene ND ug/L 06/18/14 22:19 118-74-106/16/14 11:085.0 1
Hexachlorocyclopentadiene ND ug/L 06/18/14 22:19 77-47-406/16/14 11:0810.0 1
Hexachloroethane ND ug/L 06/18/14 22:19 67-72-106/16/14 11:085.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/18/14 22:19 193-39-506/16/14 11:085.0 1
Isophorone ND ug/L 06/18/14 22:19 78-59-106/16/14 11:0810.0 1
Naphthalene ND ug/L 06/18/14 22:19 91-20-306/16/14 11:085.0 1
Nitrobenzene ND ug/L 06/18/14 22:19 98-95-306/16/14 11:085.0 1
2-Nitrophenol ND ug/L 06/18/14 22:19 88-75-506/16/14 11:085.0 1
4-Nitrophenol ND ug/L 06/18/14 22:19 100-02-706/16/14 11:0850.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 05:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92205134
SPATCO
Sample: 1823 CANNON Lab ID: 92205134001 Collected: 06/12/14 10:30 Received: 06/12/14 11:32 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
N-Nitrosodimethylamine ND ug/L 06/18/14 22:19 62-75-906/16/14 11:085.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/18/14 22:19 621-64-706/16/14 11:085.0 1
N-Nitrosodiphenylamine ND ug/L 06/18/14 22:19 86-30-606/16/14 11:0810.0 1
Pentachlorophenol ND ug/L 06/18/14 22:19 87-86-506/16/14 11:0810.0 1
Phenanthrene ND ug/L 06/18/14 22:19 85-01-806/16/14 11:085.0 1
Phenol ND ug/L 06/18/14 22:19 108-95-206/16/14 11:085.0 1
Pyrene ND ug/L 06/18/14 22:19 129-00-006/16/14 11:085.0 1
1,2,4-Trichlorobenzene ND ug/L 06/18/14 22:19 120-82-106/16/14 11:085.0 1
2,4,6-Trichlorophenol ND ug/L 06/18/14 22:19 88-06-206/16/14 11:0810.0 1
Surrogates
Nitrobenzene-d5 (S) 57 % 06/18/14 22:19 4165-60-006/16/14 11:0810-120 1
2-Fluorobiphenyl (S) 61 % 06/18/14 22:19 321-60-806/16/14 11:0815-120 1
Terphenyl-d14 (S) 73 % 06/18/14 22:19 1718-51-006/16/14 11:0811-131 1
Phenol-d6 (S) 18 % 06/18/14 22:19 13127-88-306/16/14 11:0810-120 1
2-Fluorophenol (S) 30 % 06/18/14 22:19 367-12-406/16/14 11:0810-120 1
2,4,6-Tribromophenol (S) 60 % 06/18/14 22:19 118-79-606/16/14 11:0810-137 1
Tentatively Identified Compounds
Methylene Chloride 35.9 ug/L 06/18/14 22:19 75-09-2 N06/16/14 11:081
Unknown 138 ug/L 06/18/14 22:19 N06/16/14 11:081
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol ND ug/L 06/17/14 03:45 75-85-4100 1
tert-Amylmethyl ether ND ug/L 06/17/14 03:45 994-05-810.0 1
Benzene ND ug/L 06/17/14 03:45 71-43-20.50 1
Bromobenzene ND ug/L 06/17/14 03:45 108-86-10.50 1
Bromochloromethane ND ug/L 06/17/14 03:45 74-97-50.50 1
Bromodichloromethane ND ug/L 06/17/14 03:45 75-27-40.50 1
Bromoform ND ug/L 06/17/14 03:45 75-25-20.50 1
Bromomethane ND ug/L 06/17/14 03:45 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 06/17/14 03:45 75-65-010.0 1
n-Butylbenzene ND ug/L 06/17/14 03:45 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/17/14 03:45 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/17/14 03:45 98-06-60.50 1
tert-Butyl Formate ND ug/L 06/17/14 03:45 762-75-420.0 1
Carbon tetrachloride ND ug/L 06/17/14 03:45 56-23-50.50 1
Chlorobenzene ND ug/L 06/17/14 03:45 108-90-70.50 1
Chloroethane ND ug/L 06/17/14 03:45 75-00-31.0 1
Chloroform ND ug/L 06/17/14 03:45 67-66-30.50 1
Chloromethane ND ug/L 06/17/14 03:45 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/17/14 03:45 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/17/14 03:45 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/14 03:45 96-12-81.0 1
Dibromochloromethane ND ug/L 06/17/14 03:45 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 06/17/14 03:45 106-93-40.50 1
Dibromomethane ND ug/L 06/17/14 03:45 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/17/14 03:45 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/17/14 03:45 541-73-10.50 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 05:09 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 5 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92205134
SPATCO
Sample: 1823 CANNON Lab ID: 92205134001 Collected: 06/12/14 10:30 Received: 06/12/14 11:32 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
1,4-Dichlorobenzene ND ug/L 06/17/14 03:45 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/17/14 03:45 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/17/14 03:45 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/17/14 03:45 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/17/14 03:45 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/17/14 03:45 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/17/14 03:45 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/17/14 03:45 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/17/14 03:45 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/17/14 03:45 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/17/14 03:45 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/17/14 03:45 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/17/14 03:45 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/17/14 03:45 108-20-30.50 1
Ethanol ND ug/L 06/17/14 03:45 64-17-5200 1
Ethylbenzene ND ug/L 06/17/14 03:45 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 06/17/14 03:45 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 06/17/14 03:45 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 06/17/14 03:45 98-82-80.50 1
Methylene Chloride ND ug/L 06/17/14 03:45 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/17/14 03:45 1634-04-40.50 1
Naphthalene ND ug/L 06/17/14 03:45 91-20-32.0 1
n-Propylbenzene ND ug/L 06/17/14 03:45 103-65-10.50 1
Styrene ND ug/L 06/17/14 03:45 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/17/14 03:45 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/14 03:45 79-34-50.50 1
Tetrachloroethene ND ug/L 06/17/14 03:45 127-18-40.50 1
Toluene ND ug/L 06/17/14 03:45 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/17/14 03:45 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/17/14 03:45 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/17/14 03:45 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/17/14 03:45 79-00-50.50 1
Trichloroethene ND ug/L 06/17/14 03:45 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/17/14 03:45 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/17/14 03:45 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/17/14 03:45 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/17/14 03:45 108-67-80.50 1
Vinyl chloride ND ug/L 06/17/14 03:45 75-01-41.0 1
m&p-Xylene ND ug/L 06/17/14 03:45 179601-23-11.0 1
o-Xylene ND ug/L 06/17/14 03:45 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 94 % 06/17/14 03:45 17060-07-070-130 1
4-Bromofluorobenzene (S) 97 % 06/17/14 03:45 460-00-470-130 1
Toluene-d8 (S) 99 % 06/17/14 03:45 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 05:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 6 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92205134
SPATCO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/16218
EPA 3010
EPA 6010
6010 MET
Associated Lab Samples: 92205134001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1221977
Associated Lab Samples:92205134001
Matrix: Water
Analyzed
Chromium ug/L ND 5.0 06/17/14 02:50
Lead ug/L ND 5.0 06/17/14 02:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1221978LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium ug/L 457500 91 80-120
Lead ug/L 461500 92 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1221979MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92205275001
1221980
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chromium ug/L 500 92 75-12591 050019.5 478 477
Lead ug/L 500 88 75-12589 15009.8 452 455
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 05:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92205134
SPATCO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/27235
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92205134001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1222324
Associated Lab Samples:92205134001
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 06/17/14 01:33
1,1,1-Trichloroethane ug/L ND 0.50 06/17/14 01:33
1,1,2,2-Tetrachloroethane ug/L ND 0.50 06/17/14 01:33
1,1,2-Trichloroethane ug/L ND 0.50 06/17/14 01:33
1,1-Dichloroethane ug/L ND 0.50 06/17/14 01:33
1,1-Dichloroethene ug/L ND 0.50 06/17/14 01:33
1,1-Dichloropropene ug/L ND 0.50 06/17/14 01:33
1,2,3-Trichlorobenzene ug/L ND 2.0 06/17/14 01:33
1,2,3-Trichloropropane ug/L ND 0.50 06/17/14 01:33
1,2,4-Trichlorobenzene ug/L ND 2.0 06/17/14 01:33
1,2,4-Trimethylbenzene ug/L ND 0.50 06/17/14 01:33
1,2-Dibromo-3-chloropropane ug/L ND 1.0 06/17/14 01:33
1,2-Dibromoethane (EDB) ug/L ND 0.50 06/17/14 01:33
1,2-Dichlorobenzene ug/L ND 0.50 06/17/14 01:33
1,2-Dichloroethane ug/L ND 0.50 06/17/14 01:33
1,2-Dichloropropane ug/L ND 0.50 06/17/14 01:33
1,3,5-Trimethylbenzene ug/L ND 0.50 06/17/14 01:33
1,3-Dichlorobenzene ug/L ND 0.50 06/17/14 01:33
1,3-Dichloropropane ug/L ND 0.50 06/17/14 01:33
1,4-Dichlorobenzene ug/L ND 0.50 06/17/14 01:33
2,2-Dichloropropane ug/L ND 0.50 06/17/14 01:33
2-Chlorotoluene ug/L ND 0.50 06/17/14 01:33
4-Chlorotoluene ug/L ND 0.50 06/17/14 01:33
Benzene ug/L ND 0.50 06/17/14 01:33
Bromobenzene ug/L ND 0.50 06/17/14 01:33
Bromochloromethane ug/L ND 0.50 06/17/14 01:33
Bromodichloromethane ug/L ND 0.50 06/17/14 01:33
Bromoform ug/L ND 0.50 06/17/14 01:33
Bromomethane ug/L ND 5.0 06/17/14 01:33
Carbon tetrachloride ug/L ND 0.50 06/17/14 01:33
Chlorobenzene ug/L ND 0.50 06/17/14 01:33
Chloroethane ug/L ND 1.0 06/17/14 01:33
Chloroform ug/L ND 0.50 06/17/14 01:33
Chloromethane ug/L ND 1.0 06/17/14 01:33
cis-1,2-Dichloroethene ug/L ND 0.50 06/17/14 01:33
cis-1,3-Dichloropropene ug/L ND 0.50 06/17/14 01:33
Dibromochloromethane ug/L ND 0.50 06/17/14 01:33
Dibromomethane ug/L ND 0.50 06/17/14 01:33
Dichlorodifluoromethane ug/L ND 0.50 06/17/14 01:33
Diisopropyl ether ug/L ND 0.50 06/17/14 01:33
Ethanol ug/L ND 200 06/17/14 01:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 05:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92205134
SPATCO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1222324
Associated Lab Samples:92205134001
Matrix: Water
Analyzed
Ethyl-tert-butyl ether ug/L ND 10.0 06/17/14 01:33
Ethylbenzene ug/L ND 0.50 06/17/14 01:33
Hexachloro-1,3-butadiene ug/L ND 2.0 06/17/14 01:33
Isopropylbenzene (Cumene) ug/L ND 0.50 06/17/14 01:33
m&p-Xylene ug/L ND 1.0 06/17/14 01:33
Methyl-tert-butyl ether ug/L ND 0.50 06/17/14 01:33
Methylene Chloride ug/L ND 2.0 06/17/14 01:33
n-Butylbenzene ug/L ND 0.50 06/17/14 01:33
n-Propylbenzene ug/L ND 0.50 06/17/14 01:33
Naphthalene ug/L ND 2.0 06/17/14 01:33
o-Xylene ug/L ND 0.50 06/17/14 01:33
sec-Butylbenzene ug/L ND 0.50 06/17/14 01:33
Styrene ug/L ND 0.50 06/17/14 01:33
tert-Amyl Alcohol ug/L ND 100 06/17/14 01:33
tert-Amylmethyl ether ug/L ND 10.0 06/17/14 01:33
tert-Butyl Alcohol ug/L ND 10.0 06/17/14 01:33
tert-Butyl Formate ug/L ND 20.0 06/17/14 01:33
tert-Butylbenzene ug/L ND 0.50 06/17/14 01:33
Tetrachloroethene ug/L ND 0.50 06/17/14 01:33
Toluene ug/L ND 0.50 06/17/14 01:33
trans-1,2-Dichloroethene ug/L ND 0.50 06/17/14 01:33
trans-1,3-Dichloropropene ug/L ND 0.50 06/17/14 01:33
Trichloroethene ug/L ND 0.50 06/17/14 01:33
Trichlorofluoromethane ug/L ND 1.0 06/17/14 01:33
Vinyl chloride ug/L ND 1.0 06/17/14 01:33
1,2-Dichloroethane-d4 (S) % 98 70-130 06/17/14 01:33
4-Bromofluorobenzene (S) % 100 70-130 06/17/14 01:33
Toluene-d8 (S) % 100 70-130 06/17/14 01:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1222325LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.150 102 60-140
1,1,1-Trichloroethane ug/L 49.150 98 60-140
1,1,2,2-Tetrachloroethane ug/L 48.850 98 60-140
1,1,2-Trichloroethane ug/L 49.250 98 60-140
1,1-Dichloroethane ug/L 46.550 93 60-140
1,1-Dichloroethene ug/L 49.750 99 60-140
1,1-Dichloropropene ug/L 49.450 99 60-140
1,2,3-Trichlorobenzene ug/L 50.150 100 60-140
1,2,3-Trichloropropane ug/L 50.250 100 60-140
1,2,4-Trichlorobenzene ug/L 50.150 100 60-140
1,2,4-Trimethylbenzene ug/L 50.850 102 60-140
1,2-Dibromo-3-chloropropane ug/L 51.750 103 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 05:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92205134
SPATCO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1222325LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromoethane (EDB) ug/L 51.050 102 60-140
1,2-Dichlorobenzene ug/L 50.750 101 60-140
1,2-Dichloroethane ug/L 48.450 97 60-140
1,2-Dichloropropane ug/L 48.450 97 60-140
1,3,5-Trimethylbenzene ug/L 50.350 101 60-140
1,3-Dichlorobenzene ug/L 48.850 98 60-140
1,3-Dichloropropane ug/L 49.250 98 60-140
1,4-Dichlorobenzene ug/L 48.950 98 60-140
2,2-Dichloropropane ug/L 47.150 94 60-140
2-Chlorotoluene ug/L 50.150 100 60-140
4-Chlorotoluene ug/L 48.350 97 60-140
Benzene ug/L 50.150 100 60-140
Bromobenzene ug/L 49.350 99 60-140
Bromochloromethane ug/L 48.650 97 60-140
Bromodichloromethane ug/L 51.450 103 60-140
Bromoform ug/L 55.350 111 60-140
Bromomethane ug/L 50.550 101 60-140
Carbon tetrachloride ug/L 49.950 100 60-140
Chlorobenzene ug/L 48.250 96 60-140
Chloroethane ug/L 44.550 89 60-140
Chloroform ug/L 49.350 99 60-140
Chloromethane ug/L 47.250 94 60-140
cis-1,2-Dichloroethene ug/L 49.550 99 60-140
cis-1,3-Dichloropropene ug/L 52.450 105 60-140
Dibromochloromethane ug/L 51.150 102 60-140
Dibromomethane ug/L 50.650 101 60-140
Dichlorodifluoromethane ug/L 49.350 99 60-140
Diisopropyl ether ug/L 47.650 95 60-140
Ethanol ug/L 16702000 83 60-140
Ethyl-tert-butyl ether ug/L 88.9100 89 60-140
Ethylbenzene ug/L 47.850 96 60-140
Hexachloro-1,3-butadiene ug/L 50.250 100 60-140
Isopropylbenzene (Cumene) ug/L 51.050 102 60-140
m&p-Xylene ug/L 97.0100 97 60-140
Methyl-tert-butyl ether ug/L 51.350 103 60-140
Methylene Chloride ug/L 47.450 95 60-140
n-Butylbenzene ug/L 50.050 100 60-140
n-Propylbenzene ug/L 49.350 99 60-140
Naphthalene ug/L 49.850 100 60-140
o-Xylene ug/L 49.450 99 60-140
sec-Butylbenzene ug/L 49.550 99 60-140
Styrene ug/L 52.250 104 60-140
tert-Amyl Alcohol ug/L 10401000 104 60-140
tert-Amylmethyl ether ug/L 109100 109 60-140
tert-Butyl Alcohol ug/L 553500 111 60-140
tert-Butyl Formate ug/L 378400 94 60-140
tert-Butylbenzene ug/L 50.350 101 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 05:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92205134
SPATCO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1222325LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/L 49.250 98 60-140
Toluene ug/L 48.050 96 60-140
trans-1,2-Dichloroethene ug/L 50.450 101 60-140
trans-1,3-Dichloropropene ug/L 53.250 106 60-140
Trichloroethene ug/L 48.450 97 60-140
Trichlorofluoromethane ug/L 47.450 95 60-140
Vinyl chloride ug/L 56.850 114 60-140
1,2-Dichloroethane-d4 (S) % 101 70-130
4-Bromofluorobenzene (S) % 103 70-130
Toluene-d8 (S) % 100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1222718MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92205134001
1222719
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 71 60-14079 1020ND14.2 15.8
1,1,1-Trichloroethane ug/L 20 73 60-14080 920ND14.6 16.0
1,1,2,2-Tetrachloroethane ug/L 20 72 60-14079 920ND14.5 15.8
1,1,2-Trichloroethane ug/L 20 76 60-14081 720ND15.2 16.3
1,1-Dichloroethane ug/L 20 71 60-14078 920ND14.2 15.6
1,1-Dichloroethene ug/L 20 80 60-14087 820ND16.1 17.5
1,1-Dichloropropene ug/L 20 78 60-14085 920ND15.5 17.0
1,2,3-Trichlorobenzene ug/L 20 72 60-14081 1220ND14.4 16.3
1,2,3-Trichloropropane ug/L 20 73 60-14080 920ND14.6 16.0
1,2,4-Trichlorobenzene ug/L 20 73 60-14082 1220ND14.6 16.4
1,2,4-Trimethylbenzene ug/L 20 81 60-14088 920ND16.2 17.6
1,2-Dibromo-3-chloropropane ug/L 20 66 60-14075 1320ND13.2 15.0
1,2-Dibromoethane (EDB) ug/L 20 74 60-14081 920ND14.8 16.2
1,2-Dichlorobenzene ug/L 20 76 60-14083 920ND15.2 16.6
1,2-Dichloroethane ug/L 20 70 60-14077 920ND14.1 15.4
1,2-Dichloropropane ug/L 20 76 60-14082 720ND15.2 16.3
1,3,5-Trimethylbenzene ug/L 20 79 60-14085 820ND15.8 17.1
1,3-Dichlorobenzene ug/L 20 74 60-14082 1020ND14.7 16.3
1,3-Dichloropropane ug/L 20 75 60-14081 820ND15.0 16.2
1,4-Dichlorobenzene ug/L 20 74 60-14082 920ND14.9 16.3
2,2-Dichloropropane ug/L 20 76 60-14085 1120ND15.1 16.9
2-Chlorotoluene ug/L 20 75 60-14083 920ND15.1 16.5
4-Chlorotoluene ug/L 20 74 60-14081 1020ND14.7 16.2
Benzene ug/L 20 81 60-14088 820ND16.2 17.5
Bromobenzene ug/L 20 75 60-14076 120ND15.0 15.2
Bromochloromethane ug/L 20 78 60-14084 820ND15.6 16.9
Bromodichloromethane ug/L 20 73 60-14081 1020ND14.7 16.2
Bromoform ug/L 20 67 60-14074 1120ND13.3 14.9
Bromomethane ug/L 20 63 60-14077 2020ND12.7 15.5
Carbon tetrachloride ug/L 20 73 60-14083 1220ND14.6 16.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 05:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92205134
SPATCO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1222718MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92205134001
1222719
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chlorobenzene ug/L 20 75 60-14081 720ND15.0 16.1
Chloroethane ug/L 20 82 60-14092 1120ND16.5 18.3
Chloroform ug/L 20 75 60-14082 820ND15.1 16.4
Chloromethane ug/L 20 72 60-14078 820ND14.6 15.9
cis-1,2-Dichloroethene ug/L 20 75 60-14081 820ND15.0 16.2
cis-1,3-Dichloropropene ug/L 20 75 60-14082 820ND15.1 16.3
Dibromochloromethane ug/L 20 66 60-14074 1120ND13.3 14.8
Dibromomethane ug/L 20 76 60-14080 620ND15.1 16.1
Dichlorodifluoromethane ug/L 20 79 60-14085 720ND15.9 17.1
Diisopropyl ether ug/L 20 70 60-14075 720ND14.0 15.0
Ethanol ug/L M0800 59 60-14065 11800ND471 523
Ethyl-tert-butyl ether ug/L 40 64 60-14070 840ND25.7 27.9
Ethylbenzene ug/L 20 76 60-14082 820ND15.2 16.5
Hexachloro-1,3-butadiene ug/L 20 80 60-14087 920ND15.9 17.4
Isopropylbenzene (Cumene) ug/L 20 81 60-14088 920ND16.1 17.7
m&p-Xylene ug/L 40 78 60-14085 840ND31.4 34.1
Methyl-tert-butyl ether ug/L 20 73 60-14079 820ND14.6 15.9
Methylene Chloride ug/L 20 61 60-14069 1220ND12.3 13.8
n-Butylbenzene ug/L 20 79 60-14086 920ND15.7 17.3
n-Propylbenzene ug/L 20 79 60-14087 1020ND15.7 17.4
Naphthalene ug/L 20 73 60-14082 1120ND14.8 16.5
o-Xylene ug/L 20 77 60-14084 920ND15.4 16.8
sec-Butylbenzene ug/L 20 78 60-14085 1020ND15.5 17.1
Styrene ug/L 20 80 60-14087 820ND16.0 17.4
tert-Amyl Alcohol ug/L 400 65 60-14074 13400ND260 296
tert-Amylmethyl ether ug/L 40 81 60-14087 740ND32.3 34.8
tert-Butyl Alcohol ug/L 200 85 60-140100 17200ND169 201
tert-Butyl Formate ug/L P5160 46 60-14044 5160ND73.5 69.9
tert-Butylbenzene ug/L 20 77 60-14086 1120ND15.4 17.2
Tetrachloroethene ug/L 20 77 60-14086 1120ND15.5 17.2
Toluene ug/L M020 58 60-14065 1020ND11.7 12.9
trans-1,2-Dichloroethene ug/L 20 78 60-14080 320ND15.6 16.0
trans-1,3-Dichloropropene ug/L 20 74 60-14081 1020ND14.7 16.2
Trichloroethene ug/L 20 77 60-14084 920ND15.4 16.8
Trichlorofluoromethane ug/L 20 80 60-14089 1020ND16.1 17.8
Vinyl chloride ug/L 20 86 60-14095 1020ND17.3 19.0
1,2-Dichloroethane-d4 (S) %95 70-13095
4-Bromofluorobenzene (S) % 100 70-130101
Toluene-d8 (S) % 100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 05:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92205134
SPATCO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/28295
EPA 625
EPA 625
625 MSS
Associated Lab Samples: 92205134001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1222029
Associated Lab Samples:92205134001
Matrix: Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 06/18/14 13:07
2,4,6-Trichlorophenol ug/L ND 10.0 06/18/14 13:07
2,4-Dichlorophenol ug/L ND 5.0 06/18/14 13:07
2,4-Dimethylphenol ug/L ND 10.0 06/18/14 13:07
2,4-Dinitrophenol ug/L ND 50.0 06/18/14 13:07
2,4-Dinitrotoluene ug/L ND 5.0 06/18/14 13:07
2,6-Dinitrotoluene ug/L ND 5.0 06/18/14 13:07
2-Chloronaphthalene ug/L ND 5.0 06/18/14 13:07
2-Chlorophenol ug/L ND 5.0 06/18/14 13:07
2-Nitrophenol ug/L ND 5.0 06/18/14 13:07
3,3'-Dichlorobenzidine ug/L ND 25.0 06/18/14 13:07
4,6-Dinitro-2-methylphenol ug/L ND 20.0 06/18/14 13:07
4-Bromophenylphenyl ether ug/L ND 5.0 06/18/14 13:07
4-Chloro-3-methylphenol ug/L ND 5.0 06/18/14 13:07
4-Chlorophenylphenyl ether ug/L ND 5.0 06/18/14 13:07
4-Nitrophenol ug/L ND 50.0 06/18/14 13:07
Acenaphthene ug/L ND 5.0 06/18/14 13:07
Acenaphthylene ug/L ND 5.0 06/18/14 13:07
Anthracene ug/L ND 5.0 06/18/14 13:07
Benzo(a)anthracene ug/L ND 5.0 06/18/14 13:07
Benzo(a)pyrene ug/L ND 5.0 06/18/14 13:07
Benzo(b)fluoranthene ug/L ND 5.0 06/18/14 13:07
Benzo(g,h,i)perylene ug/L ND 5.0 06/18/14 13:07
Benzo(k)fluoranthene ug/L ND 5.0 06/18/14 13:07
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/18/14 13:07
bis(2-Chloroethyl) ether ug/L ND 5.0 06/18/14 13:07
bis(2-Chloroisopropyl) ether ug/L ND 5.0 06/18/14 13:07
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 06/18/14 13:07
Butylbenzylphthalate ug/L ND 5.0 06/18/14 13:07
Chrysene ug/L ND 5.0 06/18/14 13:07
Di-n-butylphthalate ug/L ND 5.0 06/18/14 13:07
Di-n-octylphthalate ug/L ND 5.0 06/18/14 13:07
Dibenz(a,h)anthracene ug/L ND 5.0 06/18/14 13:07
Diethylphthalate ug/L ND 5.0 06/18/14 13:07
Dimethylphthalate ug/L ND 5.0 06/18/14 13:07
Fluoranthene ug/L ND 5.0 06/18/14 13:07
Fluorene ug/L ND 5.0 06/18/14 13:07
Hexachloro-1,3-butadiene ug/L ND 5.0 06/18/14 13:07
Hexachlorobenzene ug/L ND 5.0 06/18/14 13:07
Hexachlorocyclopentadiene ug/L ND 10.0 06/18/14 13:07
Hexachloroethane ug/L ND 5.0 06/18/14 13:07
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 05:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92205134
SPATCO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1222029
Associated Lab Samples:92205134001
Matrix: Water
Analyzed
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 06/18/14 13:07
Isophorone ug/L ND 10.0 06/18/14 13:07
N-Nitroso-di-n-propylamine ug/L ND 5.0 06/18/14 13:07
N-Nitrosodimethylamine ug/L ND 5.0 06/18/14 13:07
N-Nitrosodiphenylamine ug/L ND 10.0 06/18/14 13:07
Naphthalene ug/L ND 5.0 06/18/14 13:07
Nitrobenzene ug/L ND 5.0 06/18/14 13:07
Pentachlorophenol ug/L ND 10.0 06/18/14 13:07
Phenanthrene ug/L ND 5.0 06/18/14 13:07
Phenol ug/L ND 5.0 06/18/14 13:07
Pyrene ug/L ND 5.0 06/18/14 13:07
2,4,6-Tribromophenol (S) % 62 10-137 06/18/14 13:07
2-Fluorobiphenyl (S) % 59 15-120 06/18/14 13:07
2-Fluorophenol (S) % 36 10-120 06/18/14 13:07
Nitrobenzene-d5 (S) % 58 10-120 06/18/14 13:07
Phenol-d6 (S) % 24 10-120 06/18/14 13:07
Terphenyl-d14 (S) % 72 11-131 06/18/14 13:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1222030LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 28.450 57 44-142
2,4,6-Trichlorophenol ug/L 33.050 66 37-144
2,4-Dichlorophenol ug/L 33.650 67 1-191
2,4-Dimethylphenol ug/L 31.050 62 32-119
2,4-Dinitrophenol ug/L 183250 73 1-181
2,4-Dinitrotoluene ug/L 44.250 88 39-139
2,6-Dinitrotoluene ug/L 44.550 89 50-158
2-Chloronaphthalene ug/L 32.250 64 60-118
2-Chlorophenol ug/L 31.150 62 23-134
2-Nitrophenol ug/L 33.950 68 29-182
3,3'-Dichlorobenzidine ug/L 76.5100 77 1-262
4,6-Dinitro-2-methylphenol ug/L 75.3100 75 1-181
4-Bromophenylphenyl ether ug/L 34.550 69 53-127
4-Chloro-3-methylphenol ug/L 66.5100 67 22-147
4-Chlorophenylphenyl ether ug/L 36.450 73 25-158
4-Nitrophenol ug/L 76.2250 30 1-132
Acenaphthene ug/L 32.850 66 47-145
Acenaphthylene ug/L 33.950 68 33-145
Anthracene ug/L 35.250 70 1-166
Benzo(a)anthracene ug/L 36.750 73 33-143
Benzo(a)pyrene ug/L 36.550 73 17-163
Benzo(b)fluoranthene ug/L 36.550 73 24-159
Benzo(g,h,i)perylene ug/L 37.350 75 1-219
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 05:09 PM
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Page 14 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92205134
SPATCO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1222030LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(k)fluoranthene ug/L 34.750 69 11-162
bis(2-Chloroethoxy)methane ug/L 36.550 73 33-184
bis(2-Chloroethyl) ether ug/L 34.650 69 12-158
bis(2-Chloroisopropyl) ether ug/L 36.050 72 36-166
bis(2-Ethylhexyl)phthalate ug/L 40.150 80 8-158
Butylbenzylphthalate ug/L 40.250 80 1-152
Chrysene ug/L 37.550 75 17-168
Di-n-butylphthalate ug/L 38.450 77 1-118
Di-n-octylphthalate ug/L 40.650 81 4-146
Dibenz(a,h)anthracene ug/L 38.350 77 1-227
Diethylphthalate ug/L 38.050 76 1-114
Dimethylphthalate ug/L 38.050 76 1-112
Fluoranthene ug/L 36.650 73 26-137
Fluorene ug/L 36.250 72 59-121
Hexachloro-1,3-butadiene ug/L 27.150 54 24-116
Hexachlorobenzene ug/L 33.650 67 1-152
Hexachlorocyclopentadiene ug/L 28.250 56 25-150
Hexachloroethane ug/L 26.750 53 40-113
Indeno(1,2,3-cd)pyrene ug/L 29.650 59 1-171
Isophorone ug/L 41.650 83 21-196
N-Nitroso-di-n-propylamine ug/L 36.350 73 1-230
N-Nitrosodimethylamine ug/L 22.550 45 25-150
N-Nitrosodiphenylamine ug/L 36.650 73 25-150
Naphthalene ug/L 30.650 61 21-133
Nitrobenzene ug/L 39.250 78 35-180
Pentachlorophenol ug/L 70.5100 70 14-176
Phenanthrene ug/L 35.150 70 54-120
Phenol ug/L 15.750 31 5-112
Pyrene ug/L 35.450 71 52-115
2,4,6-Tribromophenol (S) % 71 10-137
2-Fluorobiphenyl (S) % 68 15-120
2-Fluorophenol (S) % 37 10-120
Nitrobenzene-d5 (S) % 65 10-120
Phenol-d6 (S) % 26 10-120
Terphenyl-d14 (S) % 73 11-131
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 05:09 PM
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Page 15 of 19
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92205134
SPATCO
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
LOD - Limit of Detection.
LOQ - Limit of Quantitation.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Tentatively identified compound (TIC) based on mass spectral library searchN
The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.P5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 05:09 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 19
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92205134
SPATCO
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92205134001 MPRP/16218 ICP/146591823 CANNON EPA 3010 EPA 6010
92205134001 OEXT/28295 MSSV/92561823 CANNON EPA 625 EPA 625
92205134001 MSV/272351823 CANNON SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 05:09 PM
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Page 17 of 19
Page 18 of 19
Page 19 of 19
#=CL#
June 19, 2014
LIMS USE: FR - ROB FOSTER
LIMS OBJECT ID: 92204984
92204984
Project:
Pace Project No.:
RE:
Mr. Rob Foster
AMEC-Charlotte
2801 Yorkmont Road Suite 100
Charlotte, NC 28208
SPATCO 6228-13-0135
Dear Mr. Foster:
Enclosed are the analytical results for sample(s) received by the laboratory on June 11, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 1 of 67
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Page 2 of 67
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92204984001 MW-1 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 625 68 PASI-CRES
SM 6200B 69 PASI-CCAH
92204984002 MW-3 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 625 68 PASI-CRES
SM 6200B 69 PASI-CCAH
92204984003 MW-5 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 625 61 PASI-CRES
SM 6200B 69 PASI-CCAH
92204984004 MW-6 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 625 67 PASI-CRES
SM 6200B 69 PASI-CCAH
92204984005 MW-10 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 625 68 PASI-CRES
SM 6200B 69 PASI-CCAH
92204984006 MW-13 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 625 60 PASI-CRES
SM 6200B 69 PASI-CCAH
92204984007 MW-14 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 6010 2 PASI-AJMW
EPA 625 59 PASI-CRES
SM 6200B 69 PASI-CCAH
92204984008 MW-15 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 6010 2 PASI-AJMW
EPA 625 58 PASI-CRES
SM 6200B 69 PASI-CCAH
92204984009 MW-2 EPA 6010 2 PASI-AJMW
92204984010 MW-1 EPA 6010 2 PASI-AJMW
92204984011 MW-3 EPA 6010 2 PASI-AJMW
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 3 of 67
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92204984012 MW-5 EPA 6010 2 PASI-AJMW
92204984013 MW-6 EPA 6010 2 PASI-AJMW
92204984014 MW-10 EPA 6010 2 PASI-AJMW
92204984015 MW-13 EPA 6010 2 PASI-AJMW
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 4 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-1 Lab ID:92204984001 Collected:06/11/14 12:00 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)1140 ug/L 06/18/14 16:41 N206/16/14 14:451001
Aliphatic (C19-C36)ND ug/L 06/18/14 16:41 N206/16/14 14:451001
Aromatic (C11-C22)1210 ug/L 06/18/14 16:41 N206/16/14 14:451001
Surrogates
Nonatriacontane (S)65 %06/18/14 16:41 7194-86-706/16/14 14:4540-140 1
o-Terphenyl (S)65 %06/18/14 16:41 84-15-106/16/14 14:4540-140 1
2-Fluorobiphenyl (S)111 %06/18/14 16:41 321-60-806/16/14 14:4540-140 1
2-Bromonaphthalene (S)129 %06/18/14 16:41 580-13-206/16/14 14:4540-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)52300 ug/L 06/19/14 07:41 N210000200
Aliphatic (C09-C12)ND ug/L 06/19/14 07:41 D3,N210000200
Aromatic (C09-C10)ND ug/L 06/19/14 07:41 N210000200
Surrogates
4-Bromofluorobenzene (FID) (S)116 %06/19/14 07:41 460-00-470-130 200
4-Bromofluorobenzene (PID) (S)105 %06/19/14 07:41 460-00-470-130 200
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/16/14 15:39 83-32-906/13/14 12:255.0 1
Acenaphthylene ND ug/L 06/16/14 15:39 208-96-806/13/14 12:255.0 1
Anthracene ND ug/L 06/16/14 15:39 120-12-706/13/14 12:255.0 1
Benzo(a)anthracene ND ug/L 06/16/14 15:39 56-55-306/13/14 12:255.0 1
Benzo(a)pyrene ND ug/L 06/16/14 15:39 50-32-806/13/14 12:255.0 1
Benzo(b)fluoranthene ND ug/L 06/16/14 15:39 205-99-206/13/14 12:255.0 1
Benzo(g,h,i)perylene ND ug/L 06/16/14 15:39 191-24-206/13/14 12:255.0 1
Benzo(k)fluoranthene ND ug/L 06/16/14 15:39 207-08-906/13/14 12:255.0 1
4-Bromophenylphenyl ether ND ug/L 06/16/14 15:39 101-55-306/13/14 12:255.0 1
Butylbenzylphthalate ND ug/L 06/16/14 15:39 85-68-706/13/14 12:255.0 1
4-Chloro-3-methylphenol ND ug/L 06/16/14 15:39 59-50-706/13/14 12:255.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/16/14 15:39 111-91-106/13/14 12:2510.0 1
bis(2-Chloroethyl) ether ND ug/L 06/16/14 15:39 111-44-406/13/14 12:255.0 1
bis(2-Chloroisopropyl) ether ND ug/L 06/16/14 15:39 108-60-106/13/14 12:255.0 1
2-Chloronaphthalene ND ug/L 06/16/14 15:39 91-58-706/13/14 12:255.0 1
2-Chlorophenol ND ug/L 06/16/14 15:39 95-57-806/13/14 12:255.0 1
4-Chlorophenylphenyl ether ND ug/L 06/16/14 15:39 7005-72-306/13/14 12:255.0 1
Chrysene ND ug/L 06/16/14 15:39 218-01-906/13/14 12:255.0 1
Dibenz(a,h)anthracene ND ug/L 06/16/14 15:39 53-70-306/13/14 12:255.0 1
3,3'-Dichlorobenzidine ND ug/L 06/16/14 15:39 91-94-106/13/14 12:2525.0 1
2,4-Dichlorophenol ND ug/L 06/16/14 15:39 120-83-206/13/14 12:255.0 1
Diethylphthalate ND ug/L 06/16/14 15:39 84-66-206/13/14 12:255.0 1
2,4-Dimethylphenol ND ug/L 06/16/14 15:39 105-67-906/13/14 12:2510.0 1
Dimethylphthalate ND ug/L 06/16/14 15:39 131-11-306/13/14 12:255.0 1
Di-n-butylphthalate ND ug/L 06/16/14 15:39 84-74-206/13/14 12:255.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/16/14 15:39 534-52-106/13/14 12:2520.0 1
2,4-Dinitrophenol ND ug/L 06/16/14 15:39 51-28-506/13/14 12:2550.0 1
2,4-Dinitrotoluene ND ug/L 06/16/14 15:39 121-14-206/13/14 12:255.0 1
2,6-Dinitrotoluene ND ug/L 06/16/14 15:39 606-20-206/13/14 12:255.0 1
REPORT OF LABORATORY ANALYSIS
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Page 5 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-1 Lab ID:92204984001 Collected:06/11/14 12:00 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 06/16/14 15:39 117-84-006/13/14 12:255.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/16/14 15:39 117-81-706/13/14 12:255.0 1
Fluoranthene ND ug/L 06/16/14 15:39 206-44-006/13/14 12:255.0 1
Fluorene ND ug/L 06/16/14 15:39 86-73-706/13/14 12:255.0 1
Hexachloro-1,3-butadiene ND ug/L 06/16/14 15:39 87-68-306/13/14 12:255.0 1
Hexachlorobenzene ND ug/L 06/16/14 15:39 118-74-106/13/14 12:255.0 1
Hexachlorocyclopentadiene ND ug/L 06/16/14 15:39 77-47-406/13/14 12:2510.0 1
Hexachloroethane ND ug/L 06/16/14 15:39 67-72-106/13/14 12:255.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/16/14 15:39 193-39-506/13/14 12:255.0 1
Isophorone ND ug/L 06/16/14 15:39 78-59-106/13/14 12:2510.0 1
Naphthalene 122 ug/L 06/17/14 21:42 91-20-306/13/14 12:2510.0 2
Nitrobenzene ND ug/L 06/16/14 15:39 98-95-306/13/14 12:255.0 1
2-Nitrophenol ND ug/L 06/16/14 15:39 88-75-506/13/14 12:255.0 1
4-Nitrophenol ND ug/L 06/16/14 15:39 100-02-706/13/14 12:2550.0 1
N-Nitrosodimethylamine ND ug/L 06/16/14 15:39 62-75-906/13/14 12:255.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/16/14 15:39 621-64-706/13/14 12:255.0 1
N-Nitrosodiphenylamine ND ug/L 06/16/14 15:39 86-30-606/13/14 12:2510.0 1
Pentachlorophenol ND ug/L 06/16/14 15:39 87-86-506/13/14 12:2510.0 1
Phenanthrene ND ug/L 06/16/14 15:39 85-01-806/13/14 12:255.0 1
Phenol 23.9 ug/L 06/16/14 15:39 108-95-206/13/14 12:255.0 1
Pyrene ND ug/L 06/16/14 15:39 129-00-006/13/14 12:255.0 1
1,2,4-Trichlorobenzene ND ug/L 06/16/14 15:39 120-82-106/13/14 12:255.0 1
2,4,6-Trichlorophenol ND ug/L 06/16/14 15:39 88-06-206/13/14 12:2510.0 1
Surrogates
Nitrobenzene-d5 (S)53 %06/16/14 15:39 4165-60-006/13/14 12:2510-120 1
2-Fluorobiphenyl (S)56 %06/16/14 15:39 321-60-806/13/14 12:2515-120 1
Terphenyl-d14 (S)70 %06/16/14 15:39 1718-51-006/13/14 12:2511-131 1
Phenol-d6 (S)21 %06/16/14 15:39 13127-88-306/13/14 12:2510-120 1
2-Fluorophenol (S)30 %06/16/14 15:39 367-12-406/13/14 12:2510-120 1
2,4,6-Tribromophenol (S)73 %06/16/14 15:39 118-79-606/13/14 12:2510-137 1
Tentatively Identified Compounds
Methyl Isobutyl Ketone 242 ug/L 06/16/14 15:39 108-10-1 N06/13/14 12:251
Naphthalene, 1-methyl-12.2 ug/L 06/16/14 15:39 90-12-0 N06/13/14 12:251
Benzoic acid, 2,3-dimeth 26.4 ug/L 06/16/14 15:39 603-79-2 N06/13/14 12:251
Unknown 22.8 ug/L 06/16/14 15:39 N06/13/14 12:251
Unknown 35.8 ug/L 06/16/14 15:39 N06/13/14 12:251
Naphthalene, 1,4,6-trim 32.9 ug/L 06/16/14 15:39 2131-42-2 N06/13/14 12:251
2-Naphthalenecarboxylic 22.5 ug/L 06/16/14 15:39 93-09-4 N06/13/14 12:251
Unknown 12.3 ug/L 06/16/14 15:39 N06/13/14 12:251
Nonadecane 11.9 ug/L 06/16/14 15:39 629-92-5 N06/13/14 12:251
Eicosane 13.8 ug/L 06/16/14 15:39 112-95-8 N06/13/14 12:251
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol ND ug/L 06/13/14 08:15 75-85-450000500
tert-Amylmethyl ether ND ug/L 06/13/14 08:15 994-05-85000500
Benzene 725 ug/L 06/13/14 08:15 71-43-2250500
Bromobenzene ND ug/L 06/13/14 08:15 108-86-1250500
REPORT OF LABORATORY ANALYSIS
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Page 6 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-1 Lab ID:92204984001 Collected:06/11/14 12:00 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Bromochloromethane ND ug/L 06/13/14 08:15 74-97-5250500
Bromodichloromethane ND ug/L 06/13/14 08:15 75-27-4250500
Bromoform ND ug/L 06/13/14 08:15 75-25-2250500
Bromomethane ND ug/L 06/13/14 08:15 74-83-92500500
tert-Butyl Alcohol ND ug/L 06/13/14 08:15 75-65-05000500
n-Butylbenzene ND ug/L 06/13/14 08:15 104-51-8250500
sec-Butylbenzene ND ug/L 06/13/14 08:15 135-98-8250500
tert-Butylbenzene ND ug/L 06/13/14 08:15 98-06-6250500
tert-Butyl Formate ND ug/L 06/13/14 08:15 762-75-410000500
Carbon tetrachloride ND ug/L 06/13/14 08:15 56-23-5250500
Chlorobenzene ND ug/L 06/13/14 08:15 108-90-7250500
Chloroethane ND ug/L 06/13/14 08:15 75-00-3500500
Chloroform ND ug/L 06/13/14 08:15 67-66-3250500
Chloromethane ND ug/L 06/13/14 08:15 74-87-3500500
2-Chlorotoluene ND ug/L 06/13/14 08:15 95-49-8250500
4-Chlorotoluene ND ug/L 06/13/14 08:15 106-43-4250500
1,2-Dibromo-3-chloropropane ND ug/L 06/13/14 08:15 96-12-8500500
Dibromochloromethane ND ug/L 06/13/14 08:15 124-48-1250500
1,2-Dibromoethane (EDB)ND ug/L 06/13/14 08:15 106-93-4250500
Dibromomethane ND ug/L 06/13/14 08:15 74-95-3250500
1,2-Dichlorobenzene ND ug/L 06/13/14 08:15 95-50-1250500
1,3-Dichlorobenzene ND ug/L 06/13/14 08:15 541-73-1250500
1,4-Dichlorobenzene ND ug/L 06/13/14 08:15 106-46-7250500
Dichlorodifluoromethane ND ug/L 06/13/14 08:15 75-71-8250500
1,1-Dichloroethane ND ug/L 06/13/14 08:15 75-34-3250500
1,2-Dichloroethane ND ug/L 06/13/14 08:15 107-06-2250500
1,1-Dichloroethene ND ug/L 06/13/14 08:15 75-35-4250500
cis-1,2-Dichloroethene 43500 ug/L 06/13/14 08:15 156-59-2250500
trans-1,2-Dichloroethene ND ug/L 06/13/14 08:15 156-60-5250500
1,2-Dichloropropane ND ug/L 06/13/14 08:15 78-87-5250500
1,3-Dichloropropane ND ug/L 06/13/14 08:15 142-28-9250500
2,2-Dichloropropane ND ug/L 06/13/14 08:15 594-20-7250500
1,1-Dichloropropene ND ug/L 06/13/14 08:15 563-58-6250500
cis-1,3-Dichloropropene ND ug/L 06/13/14 08:15 10061-01-5250500
trans-1,3-Dichloropropene ND ug/L 06/13/14 08:15 10061-02-6250500
Diisopropyl ether ND ug/L 06/13/14 08:15 108-20-3250500
Ethanol ND ug/L 06/13/14 08:15 64-17-5100000500
Ethylbenzene ND ug/L 06/13/14 08:15 100-41-4250500
Ethyl-tert-butyl ether ND ug/L 06/13/14 08:15 637-92-35000500
Hexachloro-1,3-butadiene ND ug/L 06/13/14 08:15 87-68-31000500
Isopropylbenzene (Cumene)ND ug/L 06/13/14 08:15 98-82-8250500
Methylene Chloride ND ug/L 06/13/14 08:15 75-09-21000500
Methyl-tert-butyl ether ND ug/L 06/13/14 08:15 1634-04-4250500
Naphthalene ND ug/L 06/13/14 08:15 91-20-31000500
n-Propylbenzene ND ug/L 06/13/14 08:15 103-65-1250500
Styrene ND ug/L 06/13/14 08:15 100-42-5250500
1,1,1,2-Tetrachloroethane ND ug/L 06/13/14 08:15 630-20-6250500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-1 Lab ID:92204984001 Collected:06/11/14 12:00 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
1,1,2,2-Tetrachloroethane ND ug/L 06/13/14 08:15 79-34-5250500
Tetrachloroethene 292 ug/L 06/13/14 08:15 127-18-4250500
Toluene 393 ug/L 06/13/14 08:15 108-88-3250500
1,2,3-Trichlorobenzene ND ug/L 06/13/14 08:15 87-61-61000500
1,2,4-Trichlorobenzene ND ug/L 06/13/14 08:15 120-82-11000500
1,1,1-Trichloroethane ND ug/L 06/13/14 08:15 71-55-6250500
1,1,2-Trichloroethane ND ug/L 06/13/14 08:15 79-00-5250500
Trichloroethene ND ug/L 06/13/14 08:15 79-01-6250500
Trichlorofluoromethane ND ug/L 06/13/14 08:15 75-69-4500500
1,2,3-Trichloropropane ND ug/L 06/13/14 08:15 96-18-4250500
1,2,4-Trimethylbenzene ND ug/L 06/13/14 08:15 95-63-6250500
1,3,5-Trimethylbenzene ND ug/L 06/13/14 08:15 108-67-8250500
Vinyl chloride ND ug/L 06/13/14 08:15 75-01-4500500
m&p-Xylene ND ug/L 06/13/14 08:15 179601-23-1500500
o-Xylene ND ug/L 06/13/14 08:15 95-47-6250500
Surrogates
1,2-Dichloroethane-d4 (S)95 %06/13/14 08:15 17060-07-070-130 500
4-Bromofluorobenzene (S)102 %06/13/14 08:15 460-00-470-130 500
Toluene-d8 (S)98 %06/13/14 08:15 2037-26-570-130 500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-3 Lab ID:92204984002 Collected:06/11/14 11:25 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 06/18/14 17:13 N206/16/14 14:451001
Aliphatic (C19-C36)ND ug/L 06/18/14 17:13 N206/16/14 14:451001
Aromatic (C11-C22)658 ug/L 06/18/14 17:13 N206/16/14 14:451001
Surrogates
Nonatriacontane (S)65 %06/18/14 17:13 7194-86-706/16/14 14:4540-140 1
o-Terphenyl (S)67 %06/18/14 17:13 84-15-106/16/14 14:4540-140 1
2-Fluorobiphenyl (S)75 %06/18/14 17:13 321-60-806/16/14 14:4540-140 1
2-Bromonaphthalene (S)99 %06/18/14 17:13 580-13-206/16/14 14:4540-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)71700 ug/L 06/19/14 08:03 N210000200
Aliphatic (C09-C12)ND ug/L 06/19/14 08:03 D3,N210000200
Aromatic (C09-C10)ND ug/L 06/19/14 08:03 N210000200
Surrogates
4-Bromofluorobenzene (FID) (S)121 %06/19/14 08:03 460-00-470-130 200
4-Bromofluorobenzene (PID) (S)107 %06/19/14 08:03 460-00-470-130 200
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/16/14 16:07 83-32-906/13/14 12:255.0 1
Acenaphthylene ND ug/L 06/16/14 16:07 208-96-806/13/14 12:255.0 1
Anthracene ND ug/L 06/16/14 16:07 120-12-706/13/14 12:255.0 1
Benzo(a)anthracene ND ug/L 06/16/14 16:07 56-55-306/13/14 12:255.0 1
Benzo(a)pyrene ND ug/L 06/16/14 16:07 50-32-806/13/14 12:255.0 1
Benzo(b)fluoranthene ND ug/L 06/16/14 16:07 205-99-206/13/14 12:255.0 1
Benzo(g,h,i)perylene ND ug/L 06/16/14 16:07 191-24-206/13/14 12:255.0 1
Benzo(k)fluoranthene ND ug/L 06/16/14 16:07 207-08-906/13/14 12:255.0 1
4-Bromophenylphenyl ether ND ug/L 06/16/14 16:07 101-55-306/13/14 12:255.0 1
Butylbenzylphthalate ND ug/L 06/16/14 16:07 85-68-706/13/14 12:255.0 1
4-Chloro-3-methylphenol ND ug/L 06/16/14 16:07 59-50-706/13/14 12:255.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/16/14 16:07 111-91-106/13/14 12:2510.0 1
bis(2-Chloroethyl) ether ND ug/L 06/16/14 16:07 111-44-406/13/14 12:255.0 1
bis(2-Chloroisopropyl) ether ND ug/L 06/16/14 16:07 108-60-106/13/14 12:255.0 1
2-Chloronaphthalene ND ug/L 06/16/14 16:07 91-58-706/13/14 12:255.0 1
2-Chlorophenol ND ug/L 06/16/14 16:07 95-57-806/13/14 12:255.0 1
4-Chlorophenylphenyl ether ND ug/L 06/16/14 16:07 7005-72-306/13/14 12:255.0 1
Chrysene ND ug/L 06/16/14 16:07 218-01-906/13/14 12:255.0 1
Dibenz(a,h)anthracene ND ug/L 06/16/14 16:07 53-70-306/13/14 12:255.0 1
3,3'-Dichlorobenzidine ND ug/L 06/16/14 16:07 91-94-106/13/14 12:2525.0 1
2,4-Dichlorophenol ND ug/L 06/16/14 16:07 120-83-206/13/14 12:255.0 1
Diethylphthalate ND ug/L 06/16/14 16:07 84-66-206/13/14 12:255.0 1
2,4-Dimethylphenol ND ug/L 06/16/14 16:07 105-67-906/13/14 12:2510.0 1
Dimethylphthalate ND ug/L 06/16/14 16:07 131-11-306/13/14 12:255.0 1
Di-n-butylphthalate ND ug/L 06/16/14 16:07 84-74-206/13/14 12:255.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/16/14 16:07 534-52-106/13/14 12:2520.0 1
2,4-Dinitrophenol ND ug/L 06/16/14 16:07 51-28-506/13/14 12:2550.0 1
2,4-Dinitrotoluene ND ug/L 06/16/14 16:07 121-14-206/13/14 12:255.0 1
2,6-Dinitrotoluene ND ug/L 06/16/14 16:07 606-20-206/13/14 12:255.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-3 Lab ID:92204984002 Collected:06/11/14 11:25 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 06/16/14 16:07 117-84-006/13/14 12:255.0 1
bis(2-Ethylhexyl)phthalate 15.1 ug/L 06/16/14 16:07 117-81-706/13/14 12:255.0 1
Fluoranthene ND ug/L 06/16/14 16:07 206-44-006/13/14 12:255.0 1
Fluorene ND ug/L 06/16/14 16:07 86-73-706/13/14 12:255.0 1
Hexachloro-1,3-butadiene ND ug/L 06/16/14 16:07 87-68-306/13/14 12:255.0 1
Hexachlorobenzene ND ug/L 06/16/14 16:07 118-74-106/13/14 12:255.0 1
Hexachlorocyclopentadiene ND ug/L 06/16/14 16:07 77-47-406/13/14 12:2510.0 1
Hexachloroethane ND ug/L 06/16/14 16:07 67-72-106/13/14 12:255.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/16/14 16:07 193-39-506/13/14 12:255.0 1
Isophorone ND ug/L 06/16/14 16:07 78-59-106/13/14 12:2510.0 1
Naphthalene 181 ug/L 06/17/14 22:10 91-20-306/13/14 12:2520.0 4
Nitrobenzene ND ug/L 06/16/14 16:07 98-95-306/13/14 12:255.0 1
2-Nitrophenol ND ug/L 06/16/14 16:07 88-75-506/13/14 12:255.0 1
4-Nitrophenol ND ug/L 06/16/14 16:07 100-02-706/13/14 12:2550.0 1
N-Nitrosodimethylamine ND ug/L 06/16/14 16:07 62-75-906/13/14 12:255.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/16/14 16:07 621-64-706/13/14 12:255.0 1
N-Nitrosodiphenylamine ND ug/L 06/16/14 16:07 86-30-606/13/14 12:2510.0 1
Pentachlorophenol ND ug/L 06/16/14 16:07 87-86-506/13/14 12:2510.0 1
Phenanthrene ND ug/L 06/16/14 16:07 85-01-806/13/14 12:255.0 1
Phenol 5.4 ug/L 06/16/14 16:07 108-95-206/13/14 12:255.0 1
Pyrene ND ug/L 06/16/14 16:07 129-00-006/13/14 12:255.0 1
1,2,4-Trichlorobenzene ND ug/L 06/16/14 16:07 120-82-106/13/14 12:255.0 1
2,4,6-Trichlorophenol ND ug/L 06/16/14 16:07 88-06-206/13/14 12:2510.0 1
Surrogates
Nitrobenzene-d5 (S)73 %06/16/14 16:07 4165-60-006/13/14 12:2510-120 1
2-Fluorobiphenyl (S)73 %06/16/14 16:07 321-60-806/13/14 12:2515-120 1
Terphenyl-d14 (S)83 %06/16/14 16:07 1718-51-006/13/14 12:2511-131 1
Phenol-d6 (S)36 %06/16/14 16:07 13127-88-306/13/14 12:2510-120 1
2-Fluorophenol (S)49 %06/16/14 16:07 367-12-406/13/14 12:2510-120 1
2,4,6-Tribromophenol (S)76 %06/16/14 16:07 118-79-606/13/14 12:2510-137 1
Tentatively Identified Compounds
Unknown 669 ug/L 06/16/14 16:07 N06/13/14 12:251
2-Pentanol, 2-methyl-2330 ug/L 06/16/14 16:07 590-36-3 N06/13/14 12:251
Cyclopentanol, 1-methyl-1310 ug/L 06/16/14 16:07 1462-03-9 N06/13/14 12:251
2-Hexanol, 2-methyl-656 ug/L 06/16/14 16:07 625-23-0 N06/13/14 12:251
Unknown 1350 ug/L 06/16/14 16:07 N06/13/14 12:251
p-Xylene 309 ug/L 06/16/14 16:07 106-42-3 N06/13/14 12:251
Unknown 172 ug/L 06/16/14 16:07 N06/13/14 12:251
Unknown 206 ug/L 06/16/14 16:07 N06/13/14 12:251
Benzene, 1-ethyl-3-methy 168 ug/L 06/16/14 16:07 620-14-4 N06/13/14 12:251
n-Hexadecanoic acid 87.7 ug/L 06/16/14 16:07 57-10-3 N06/13/14 12:251
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol 71800 ug/L 06/13/14 08:31 75-85-410000100
tert-Amylmethyl ether ND ug/L 06/13/14 08:31 994-05-81000100
Benzene 14000 ug/L 06/13/14 08:31 71-43-250.0 100
Bromobenzene ND ug/L 06/13/14 08:31 108-86-150.0 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-3 Lab ID:92204984002 Collected:06/11/14 11:25 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Bromochloromethane ND ug/L 06/13/14 08:31 74-97-550.0 100
Bromodichloromethane ND ug/L 06/13/14 08:31 75-27-450.0 100
Bromoform ND ug/L 06/13/14 08:31 75-25-250.0 100
Bromomethane ND ug/L 06/13/14 08:31 74-83-9500100
tert-Butyl Alcohol 1960 ug/L 06/13/14 08:31 75-65-01000100
n-Butylbenzene ND ug/L 06/13/14 08:31 104-51-850.0 100
sec-Butylbenzene ND ug/L 06/13/14 08:31 135-98-850.0 100
tert-Butylbenzene ND ug/L 06/13/14 08:31 98-06-650.0 100
tert-Butyl Formate ND ug/L 06/13/14 08:31 762-75-42000100
Carbon tetrachloride ND ug/L 06/13/14 08:31 56-23-550.0 100
Chlorobenzene ND ug/L 06/13/14 08:31 108-90-750.0 100
Chloroethane ND ug/L 06/13/14 08:31 75-00-3100100
Chloroform ND ug/L 06/13/14 08:31 67-66-350.0 100
Chloromethane ND ug/L 06/13/14 08:31 74-87-3100100
2-Chlorotoluene ND ug/L 06/13/14 08:31 95-49-850.0 100
4-Chlorotoluene ND ug/L 06/13/14 08:31 106-43-450.0 100
1,2-Dibromo-3-chloropropane ND ug/L 06/13/14 08:31 96-12-8100100
Dibromochloromethane ND ug/L 06/13/14 08:31 124-48-150.0 100
1,2-Dibromoethane (EDB)ND ug/L 06/13/14 08:31 106-93-450.0 100
Dibromomethane ND ug/L 06/13/14 08:31 74-95-350.0 100
1,2-Dichlorobenzene ND ug/L 06/13/14 08:31 95-50-150.0 100
1,3-Dichlorobenzene ND ug/L 06/13/14 08:31 541-73-150.0 100
1,4-Dichlorobenzene ND ug/L 06/13/14 08:31 106-46-750.0 100
Dichlorodifluoromethane ND ug/L 06/13/14 08:31 75-71-850.0 100
1,1-Dichloroethane ND ug/L 06/13/14 08:31 75-34-350.0 100
1,2-Dichloroethane 752 ug/L 06/13/14 08:31 107-06-250.0 100
1,1-Dichloroethene ND ug/L 06/13/14 08:31 75-35-450.0 100
cis-1,2-Dichloroethene 3020 ug/L 06/13/14 08:31 156-59-250.0 100
trans-1,2-Dichloroethene ND ug/L 06/13/14 08:31 156-60-550.0 100
1,2-Dichloropropane 65.5 ug/L 06/13/14 08:31 78-87-550.0 100
1,3-Dichloropropane ND ug/L 06/13/14 08:31 142-28-950.0 100
2,2-Dichloropropane ND ug/L 06/13/14 08:31 594-20-750.0 100
1,1-Dichloropropene ND ug/L 06/13/14 08:31 563-58-650.0 100
cis-1,3-Dichloropropene ND ug/L 06/13/14 08:31 10061-01-550.0 100
trans-1,3-Dichloropropene ND ug/L 06/13/14 08:31 10061-02-650.0 100
Diisopropyl ether 113 ug/L 06/13/14 08:31 108-20-350.0 100
Ethanol ND ug/L 06/13/14 08:31 64-17-520000100
Ethylbenzene 631 ug/L 06/13/14 08:31 100-41-450.0 100
Ethyl-tert-butyl ether ND ug/L 06/13/14 08:31 637-92-31000100
Hexachloro-1,3-butadiene ND ug/L 06/13/14 08:31 87-68-3200100
Isopropylbenzene (Cumene)ND ug/L 06/13/14 08:31 98-82-850.0 100
Methylene Chloride ND ug/L 06/13/14 08:31 75-09-2200100
Methyl-tert-butyl ether ND ug/L 06/13/14 08:31 1634-04-450.0 100
Naphthalene 336 ug/L 06/13/14 08:31 91-20-3200100
n-Propylbenzene 84.2 ug/L 06/13/14 08:31 103-65-150.0 100
Styrene ND ug/L 06/13/14 08:31 100-42-550.0 100
1,1,1,2-Tetrachloroethane ND ug/L 06/13/14 08:31 630-20-650.0 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-3 Lab ID:92204984002 Collected:06/11/14 11:25 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
1,1,2,2-Tetrachloroethane ND ug/L 06/13/14 08:31 79-34-550.0 100
Tetrachloroethene ND ug/L 06/13/14 08:31 127-18-450.0 100
Toluene 429 ug/L 06/13/14 08:31 108-88-350.0 100
1,2,3-Trichlorobenzene ND ug/L 06/13/14 08:31 87-61-6200100
1,2,4-Trichlorobenzene ND ug/L 06/13/14 08:31 120-82-1200100
1,1,1-Trichloroethane ND ug/L 06/13/14 08:31 71-55-650.0 100
1,1,2-Trichloroethane ND ug/L 06/13/14 08:31 79-00-550.0 100
Trichloroethene ND ug/L 06/13/14 08:31 79-01-650.0 100
Trichlorofluoromethane ND ug/L 06/13/14 08:31 75-69-4100100
1,2,3-Trichloropropane ND ug/L 06/13/14 08:31 96-18-450.0 100
1,2,4-Trimethylbenzene 286 ug/L 06/13/14 08:31 95-63-650.0 100
1,3,5-Trimethylbenzene 155 ug/L 06/13/14 08:31 108-67-850.0 100
Vinyl chloride ND ug/L 06/13/14 08:31 75-01-4100100
m&p-Xylene 1140 ug/L 06/13/14 08:31 179601-23-1100100
o-Xylene 215 ug/L 06/13/14 08:31 95-47-650.0 100
Surrogates
1,2-Dichloroethane-d4 (S)95 %06/13/14 08:31 17060-07-070-130 100
4-Bromofluorobenzene (S)100 %06/13/14 08:31 460-00-470-130 100
Toluene-d8 (S)98 %06/13/14 08:31 2037-26-570-130 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-5 Lab ID:92204984003 Collected:06/11/14 12:45 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 06/18/14 17:46 N206/16/14 14:451001
Aliphatic (C19-C36)ND ug/L 06/18/14 17:46 N206/16/14 14:451001
Aromatic (C11-C22)ND ug/L 06/18/14 17:46 N206/16/14 14:451001
Surrogates
Nonatriacontane (S)78 %06/18/14 17:46 7194-86-706/16/14 14:4540-140 1
o-Terphenyl (S)67 %06/18/14 17:46 84-15-106/16/14 14:4540-140 1
2-Fluorobiphenyl (S)57 %06/18/14 17:46 321-60-806/16/14 14:4540-140 1
2-Bromonaphthalene (S)68 %06/18/14 17:46 580-13-206/16/14 14:4540-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)229 ug/L 06/18/14 23:04 N250.0 1
Aliphatic (C09-C12)ND ug/L 06/18/14 23:04 N250.0 1
Aromatic (C09-C10)ND ug/L 06/18/14 23:04 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)115 %06/18/14 23:04 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)103 %06/18/14 23:04 460-00-470-130 1
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/16/14 16:35 83-32-906/13/14 12:255.0 1
Acenaphthylene ND ug/L 06/16/14 16:35 208-96-806/13/14 12:255.0 1
Anthracene ND ug/L 06/16/14 16:35 120-12-706/13/14 12:255.0 1
Benzo(a)anthracene ND ug/L 06/16/14 16:35 56-55-306/13/14 12:255.0 1
Benzo(a)pyrene ND ug/L 06/16/14 16:35 50-32-806/13/14 12:255.0 1
Benzo(b)fluoranthene ND ug/L 06/16/14 16:35 205-99-206/13/14 12:255.0 1
Benzo(g,h,i)perylene ND ug/L 06/16/14 16:35 191-24-206/13/14 12:255.0 1
Benzo(k)fluoranthene ND ug/L 06/16/14 16:35 207-08-906/13/14 12:255.0 1
4-Bromophenylphenyl ether ND ug/L 06/16/14 16:35 101-55-306/13/14 12:255.0 1
Butylbenzylphthalate ND ug/L 06/16/14 16:35 85-68-706/13/14 12:255.0 1
4-Chloro-3-methylphenol ND ug/L 06/16/14 16:35 59-50-706/13/14 12:255.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/16/14 16:35 111-91-106/13/14 12:2510.0 1
bis(2-Chloroethyl) ether ND ug/L 06/16/14 16:35 111-44-406/13/14 12:255.0 1
bis(2-Chloroisopropyl) ether ND ug/L 06/16/14 16:35 108-60-106/13/14 12:255.0 1
2-Chloronaphthalene ND ug/L 06/16/14 16:35 91-58-706/13/14 12:255.0 1
2-Chlorophenol ND ug/L 06/16/14 16:35 95-57-806/13/14 12:255.0 1
4-Chlorophenylphenyl ether ND ug/L 06/16/14 16:35 7005-72-306/13/14 12:255.0 1
Chrysene ND ug/L 06/16/14 16:35 218-01-906/13/14 12:255.0 1
Dibenz(a,h)anthracene ND ug/L 06/16/14 16:35 53-70-306/13/14 12:255.0 1
3,3'-Dichlorobenzidine ND ug/L 06/16/14 16:35 91-94-106/13/14 12:2525.0 1
2,4-Dichlorophenol ND ug/L 06/16/14 16:35 120-83-206/13/14 12:255.0 1
Diethylphthalate ND ug/L 06/16/14 16:35 84-66-206/13/14 12:255.0 1
2,4-Dimethylphenol ND ug/L 06/16/14 16:35 105-67-906/13/14 12:2510.0 1
Dimethylphthalate ND ug/L 06/16/14 16:35 131-11-306/13/14 12:255.0 1
Di-n-butylphthalate ND ug/L 06/16/14 16:35 84-74-206/13/14 12:255.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/16/14 16:35 534-52-106/13/14 12:2520.0 1
2,4-Dinitrophenol ND ug/L 06/16/14 16:35 51-28-506/13/14 12:2550.0 1
2,4-Dinitrotoluene ND ug/L 06/16/14 16:35 121-14-206/13/14 12:255.0 1
2,6-Dinitrotoluene ND ug/L 06/16/14 16:35 606-20-206/13/14 12:255.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-5 Lab ID:92204984003 Collected:06/11/14 12:45 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 06/16/14 16:35 117-84-006/13/14 12:255.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/16/14 16:35 117-81-706/13/14 12:255.0 1
Fluoranthene ND ug/L 06/16/14 16:35 206-44-006/13/14 12:255.0 1
Fluorene ND ug/L 06/16/14 16:35 86-73-706/13/14 12:255.0 1
Hexachloro-1,3-butadiene ND ug/L 06/16/14 16:35 87-68-306/13/14 12:255.0 1
Hexachlorobenzene ND ug/L 06/16/14 16:35 118-74-106/13/14 12:255.0 1
Hexachlorocyclopentadiene ND ug/L 06/16/14 16:35 77-47-406/13/14 12:2510.0 1
Hexachloroethane ND ug/L 06/16/14 16:35 67-72-106/13/14 12:255.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/16/14 16:35 193-39-506/13/14 12:255.0 1
Isophorone ND ug/L 06/16/14 16:35 78-59-106/13/14 12:2510.0 1
Naphthalene ND ug/L 06/16/14 16:35 91-20-306/13/14 12:255.0 1
Nitrobenzene ND ug/L 06/16/14 16:35 98-95-306/13/14 12:255.0 1
2-Nitrophenol ND ug/L 06/16/14 16:35 88-75-506/13/14 12:255.0 1
4-Nitrophenol ND ug/L 06/16/14 16:35 100-02-706/13/14 12:2550.0 1
N-Nitrosodimethylamine ND ug/L 06/16/14 16:35 62-75-906/13/14 12:255.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/16/14 16:35 621-64-706/13/14 12:255.0 1
N-Nitrosodiphenylamine ND ug/L 06/16/14 16:35 86-30-606/13/14 12:2510.0 1
Pentachlorophenol ND ug/L 06/16/14 16:35 87-86-506/13/14 12:2510.0 1
Phenanthrene ND ug/L 06/16/14 16:35 85-01-806/13/14 12:255.0 1
Phenol ND ug/L 06/16/14 16:35 108-95-206/13/14 12:255.0 1
Pyrene ND ug/L 06/16/14 16:35 129-00-006/13/14 12:255.0 1
1,2,4-Trichlorobenzene ND ug/L 06/16/14 16:35 120-82-106/13/14 12:255.0 1
2,4,6-Trichlorophenol ND ug/L 06/16/14 16:35 88-06-206/13/14 12:2510.0 1
Surrogates
Nitrobenzene-d5 (S)69 %06/16/14 16:35 4165-60-006/13/14 12:2510-120 1
2-Fluorobiphenyl (S)74 %06/16/14 16:35 321-60-806/13/14 12:2515-120 1
Terphenyl-d14 (S)81 %06/16/14 16:35 1718-51-006/13/14 12:2511-131 1
Phenol-d6 (S)23 %06/16/14 16:35 13127-88-306/13/14 12:2510-120 1
2-Fluorophenol (S)34 %06/16/14 16:35 367-12-406/13/14 12:2510-120 1
2,4,6-Tribromophenol (S)67 %06/16/14 16:35 118-79-606/13/14 12:2510-137 1
Tentatively Identified Compounds
2-Pentanol, 2-methyl-12.1 ug/L 06/16/14 16:35 590-36-3 N06/13/14 12:251
Unknown 10.6 ug/L 06/16/14 16:35 N06/13/14 12:251
Tetrachloroethylene 80.6 ug/L 06/16/14 16:35 127-18-4 N06/13/14 12:251
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol ND ug/L 06/13/14 04:39 75-85-41001
tert-Amylmethyl ether ND ug/L 06/13/14 04:39 994-05-810.0 1
Benzene ND ug/L 06/13/14 04:39 71-43-20.50 1
Bromobenzene ND ug/L 06/13/14 04:39 108-86-10.50 1
Bromochloromethane ND ug/L 06/13/14 04:39 74-97-50.50 1
Bromodichloromethane ND ug/L 06/13/14 04:39 75-27-40.50 1
Bromoform ND ug/L 06/13/14 04:39 75-25-20.50 1
Bromomethane ND ug/L 06/13/14 04:39 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 06/13/14 04:39 75-65-010.0 1
n-Butylbenzene ND ug/L 06/13/14 04:39 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/13/14 04:39 135-98-80.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-5 Lab ID:92204984003 Collected:06/11/14 12:45 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
tert-Butylbenzene ND ug/L 06/13/14 04:39 98-06-60.50 1
tert-Butyl Formate ND ug/L 06/13/14 04:39 762-75-420.0 1
Carbon tetrachloride ND ug/L 06/13/14 04:39 56-23-50.50 1
Chlorobenzene ND ug/L 06/13/14 04:39 108-90-70.50 1
Chloroethane ND ug/L 06/13/14 04:39 75-00-31.0 1
Chloroform ND ug/L 06/13/14 04:39 67-66-30.50 1
Chloromethane ND ug/L 06/13/14 04:39 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/13/14 04:39 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/13/14 04:39 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/13/14 04:39 96-12-81.0 1
Dibromochloromethane ND ug/L 06/13/14 04:39 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/13/14 04:39 106-93-40.50 1
Dibromomethane ND ug/L 06/13/14 04:39 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/13/14 04:39 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/13/14 04:39 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/13/14 04:39 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/13/14 04:39 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/13/14 04:39 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/13/14 04:39 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/13/14 04:39 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/13/14 04:39 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/13/14 04:39 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/13/14 04:39 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/13/14 04:39 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/13/14 04:39 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/13/14 04:39 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/13/14 04:39 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/13/14 04:39 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/13/14 04:39 108-20-30.50 1
Ethanol ND ug/L 06/13/14 04:39 64-17-52001
Ethylbenzene ND ug/L 06/13/14 04:39 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 06/13/14 04:39 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 06/13/14 04:39 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/13/14 04:39 98-82-80.50 1
Methylene Chloride ND ug/L 06/13/14 04:39 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/13/14 04:39 1634-04-40.50 1
Naphthalene ND ug/L 06/13/14 04:39 91-20-32.0 1
n-Propylbenzene ND ug/L 06/13/14 04:39 103-65-10.50 1
Styrene ND ug/L 06/13/14 04:39 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/13/14 04:39 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/13/14 04:39 79-34-50.50 1
Tetrachloroethene 343 ug/L 06/16/14 23:21 127-18-42.5 5
Toluene ND ug/L 06/13/14 04:39 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/13/14 04:39 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/13/14 04:39 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/13/14 04:39 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/13/14 04:39 79-00-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-5 Lab ID:92204984003 Collected:06/11/14 12:45 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Trichloroethene 6.7 ug/L 06/13/14 04:39 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/13/14 04:39 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/13/14 04:39 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/13/14 04:39 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/13/14 04:39 108-67-80.50 1
Vinyl chloride ND ug/L 06/13/14 04:39 75-01-41.0 1
m&p-Xylene ND ug/L 06/13/14 04:39 179601-23-11.0 1
o-Xylene ND ug/L 06/13/14 04:39 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %06/13/14 04:39 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %06/13/14 04:39 460-00-470-130 1
Toluene-d8 (S)99 %06/13/14 04:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-6 Lab ID:92204984004 Collected:06/11/14 12:30 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)139 ug/L 06/18/14 18:18 N206/16/14 14:451001
Aliphatic (C19-C36)ND ug/L 06/18/14 18:18 N206/16/14 14:451001
Aromatic (C11-C22)770 ug/L 06/18/14 18:18 N206/16/14 14:451001
Surrogates
Nonatriacontane (S)65 %06/18/14 18:18 7194-86-706/16/14 14:4540-140 1
o-Terphenyl (S)77 %06/18/14 18:18 84-15-106/16/14 14:4540-140 1
2-Fluorobiphenyl (S)90 %06/18/14 18:18 321-60-806/16/14 14:4540-140 1
2-Bromonaphthalene (S)111 %06/18/14 18:18 580-13-206/16/14 14:4540-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)1080 ug/L 06/19/14 06:55 N250010
Aliphatic (C09-C12)1920 ug/L 06/19/14 06:55 N250010
Aromatic (C09-C10)748 ug/L 06/19/14 06:55 N250010
Surrogates
4-Bromofluorobenzene (FID) (S)120 %06/19/14 06:55 460-00-470-130 10
4-Bromofluorobenzene (PID) (S)107 %06/19/14 06:55 460-00-470-130 10
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/16/14 17:03 83-32-906/13/14 12:255.0 1
Acenaphthylene ND ug/L 06/16/14 17:03 208-96-806/13/14 12:255.0 1
Anthracene ND ug/L 06/16/14 17:03 120-12-706/13/14 12:255.0 1
Benzo(a)anthracene ND ug/L 06/16/14 17:03 56-55-306/13/14 12:255.0 1
Benzo(a)pyrene ND ug/L 06/16/14 17:03 50-32-806/13/14 12:255.0 1
Benzo(b)fluoranthene ND ug/L 06/16/14 17:03 205-99-206/13/14 12:255.0 1
Benzo(g,h,i)perylene ND ug/L 06/16/14 17:03 191-24-206/13/14 12:255.0 1
Benzo(k)fluoranthene ND ug/L 06/16/14 17:03 207-08-906/13/14 12:255.0 1
4-Bromophenylphenyl ether ND ug/L 06/16/14 17:03 101-55-306/13/14 12:255.0 1
Butylbenzylphthalate ND ug/L 06/16/14 17:03 85-68-706/13/14 12:255.0 1
4-Chloro-3-methylphenol ND ug/L 06/16/14 17:03 59-50-706/13/14 12:255.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/16/14 17:03 111-91-106/13/14 12:2510.0 1
bis(2-Chloroethyl) ether ND ug/L 06/16/14 17:03 111-44-406/13/14 12:255.0 1
bis(2-Chloroisopropyl) ether ND ug/L 06/16/14 17:03 108-60-106/13/14 12:255.0 1
2-Chloronaphthalene ND ug/L 06/16/14 17:03 91-58-706/13/14 12:255.0 1
2-Chlorophenol ND ug/L 06/16/14 17:03 95-57-806/13/14 12:255.0 1
4-Chlorophenylphenyl ether ND ug/L 06/16/14 17:03 7005-72-306/13/14 12:255.0 1
Chrysene ND ug/L 06/16/14 17:03 218-01-906/13/14 12:255.0 1
Dibenz(a,h)anthracene ND ug/L 06/16/14 17:03 53-70-306/13/14 12:255.0 1
3,3'-Dichlorobenzidine ND ug/L 06/16/14 17:03 91-94-106/13/14 12:2525.0 1
2,4-Dichlorophenol ND ug/L 06/16/14 17:03 120-83-206/13/14 12:255.0 1
Diethylphthalate ND ug/L 06/16/14 17:03 84-66-206/13/14 12:255.0 1
2,4-Dimethylphenol ND ug/L 06/16/14 17:03 105-67-906/13/14 12:2510.0 1
Dimethylphthalate ND ug/L 06/16/14 17:03 131-11-306/13/14 12:255.0 1
Di-n-butylphthalate ND ug/L 06/16/14 17:03 84-74-206/13/14 12:255.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/16/14 17:03 534-52-106/13/14 12:2520.0 1
2,4-Dinitrophenol ND ug/L 06/16/14 17:03 51-28-506/13/14 12:2550.0 1
2,4-Dinitrotoluene ND ug/L 06/16/14 17:03 121-14-206/13/14 12:255.0 1
2,6-Dinitrotoluene ND ug/L 06/16/14 17:03 606-20-206/13/14 12:255.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-6 Lab ID:92204984004 Collected:06/11/14 12:30 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 06/16/14 17:03 117-84-006/13/14 12:255.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/16/14 17:03 117-81-706/13/14 12:255.0 1
Fluoranthene ND ug/L 06/16/14 17:03 206-44-006/13/14 12:255.0 1
Fluorene ND ug/L 06/16/14 17:03 86-73-706/13/14 12:255.0 1
Hexachloro-1,3-butadiene ND ug/L 06/16/14 17:03 87-68-306/13/14 12:255.0 1
Hexachlorobenzene ND ug/L 06/16/14 17:03 118-74-106/13/14 12:255.0 1
Hexachlorocyclopentadiene ND ug/L 06/16/14 17:03 77-47-406/13/14 12:2510.0 1
Hexachloroethane ND ug/L 06/16/14 17:03 67-72-106/13/14 12:255.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/16/14 17:03 193-39-506/13/14 12:255.0 1
Isophorone ND ug/L 06/16/14 17:03 78-59-106/13/14 12:2510.0 1
Naphthalene 189 ug/L 06/17/14 22:38 91-20-306/13/14 12:2520.0 4
Nitrobenzene ND ug/L 06/16/14 17:03 98-95-306/13/14 12:255.0 1
2-Nitrophenol ND ug/L 06/16/14 17:03 88-75-506/13/14 12:255.0 1
4-Nitrophenol ND ug/L 06/16/14 17:03 100-02-706/13/14 12:2550.0 1
N-Nitrosodimethylamine ND ug/L 06/16/14 17:03 62-75-906/13/14 12:255.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/16/14 17:03 621-64-706/13/14 12:255.0 1
N-Nitrosodiphenylamine ND ug/L 06/16/14 17:03 86-30-606/13/14 12:2510.0 1
Pentachlorophenol ND ug/L 06/16/14 17:03 87-86-506/13/14 12:2510.0 1
Phenanthrene ND ug/L 06/16/14 17:03 85-01-806/13/14 12:255.0 1
Phenol ND ug/L 06/16/14 17:03 108-95-206/13/14 12:255.0 1
Pyrene ND ug/L 06/16/14 17:03 129-00-006/13/14 12:255.0 1
1,2,4-Trichlorobenzene ND ug/L 06/16/14 17:03 120-82-106/13/14 12:255.0 1
2,4,6-Trichlorophenol ND ug/L 06/16/14 17:03 88-06-206/13/14 12:2510.0 1
Surrogates
Nitrobenzene-d5 (S)65 %06/16/14 17:03 4165-60-006/13/14 12:2510-120 1
2-Fluorobiphenyl (S)73 %06/16/14 17:03 321-60-806/13/14 12:2515-120 1
Terphenyl-d14 (S)85 %06/16/14 17:03 1718-51-006/13/14 12:2511-131 1
Phenol-d6 (S)30 %06/16/14 17:03 13127-88-306/13/14 12:2510-120 1
2-Fluorophenol (S)41 %06/16/14 17:03 367-12-406/13/14 12:2510-120 1
2,4,6-Tribromophenol (S)83 %06/16/14 17:03 118-79-606/13/14 12:2510-137 1
Tentatively Identified Compounds
Ethylbenzene 67.6 ug/L 06/16/14 17:03 100-41-4 N06/13/14 12:251
p-Xylene 38.9 ug/L 06/16/14 17:03 106-42-3 N06/13/14 12:251
Benzene, 1-ethyl-2-methy 28.3 ug/L 06/16/14 17:03 611-14-3 N06/13/14 12:251
Benzene, 1-ethyl-2,4-dim 29.0 ug/L 06/16/14 17:03 874-41-9 N06/13/14 12:251
Benzene, 2-butenyl-5.2 ug/L 06/16/14 17:03 1560-06-1 N06/13/14 12:251
Naphthalene, 1-methyl-10.0 ug/L 06/16/14 17:03 90-12-0 N06/13/14 12:251
Benzoic acid, 3,5-dimeth 23.5 ug/L 06/16/14 17:03 499-06-9 N06/13/14 12:251
Naphthalene, 1,6-dimethy 22.3 ug/L 06/16/14 17:03 575-43-9 N06/13/14 12:251
Unknown 12.6 ug/L 06/16/14 17:03 N06/13/14 12:251
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol ND ug/L 06/17/14 03:12 75-85-4100010
tert-Amylmethyl ether ND ug/L 06/17/14 03:12 994-05-810010
Benzene 41.9 ug/L 06/17/14 03:12 71-43-25.0 10
Bromobenzene ND ug/L 06/17/14 03:12 108-86-15.0 10
Bromochloromethane ND ug/L 06/17/14 03:12 74-97-55.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-6 Lab ID:92204984004 Collected:06/11/14 12:30 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Bromodichloromethane ND ug/L 06/17/14 03:12 75-27-45.0 10
Bromoform ND ug/L 06/17/14 03:12 75-25-25.0 10
Bromomethane ND ug/L 06/17/14 03:12 74-83-950.0 10
tert-Butyl Alcohol ND ug/L 06/17/14 03:12 75-65-010010
n-Butylbenzene ND ug/L 06/17/14 03:12 104-51-85.0 10
sec-Butylbenzene ND ug/L 06/17/14 03:12 135-98-85.0 10
tert-Butylbenzene ND ug/L 06/17/14 03:12 98-06-65.0 10
tert-Butyl Formate ND ug/L 06/17/14 03:12 762-75-420010
Carbon tetrachloride ND ug/L 06/17/14 03:12 56-23-55.0 10
Chlorobenzene ND ug/L 06/17/14 03:12 108-90-75.0 10
Chloroethane ND ug/L 06/17/14 03:12 75-00-310.0 10
Chloroform ND ug/L 06/17/14 03:12 67-66-35.0 10
Chloromethane ND ug/L 06/17/14 03:12 74-87-310.0 10
2-Chlorotoluene ND ug/L 06/17/14 03:12 95-49-85.0 10
4-Chlorotoluene ND ug/L 06/17/14 03:12 106-43-45.0 10
1,2-Dibromo-3-chloropropane ND ug/L 06/17/14 03:12 96-12-810.0 10
Dibromochloromethane ND ug/L 06/17/14 03:12 124-48-15.0 10
1,2-Dibromoethane (EDB)ND ug/L 06/17/14 03:12 106-93-45.0 10
Dibromomethane ND ug/L 06/17/14 03:12 74-95-35.0 10
1,2-Dichlorobenzene 25.4 ug/L 06/17/14 03:12 95-50-15.0 10
1,3-Dichlorobenzene ND ug/L 06/17/14 03:12 541-73-15.0 10
1,4-Dichlorobenzene 6.8 ug/L 06/17/14 03:12 106-46-75.0 10
Dichlorodifluoromethane ND ug/L 06/17/14 03:12 75-71-85.0 10
1,1-Dichloroethane ND ug/L 06/17/14 03:12 75-34-35.0 10
1,2-Dichloroethane ND ug/L 06/17/14 03:12 107-06-25.0 10
1,1-Dichloroethene ND ug/L 06/17/14 03:12 75-35-45.0 10
cis-1,2-Dichloroethene 979 ug/L 06/17/14 03:12 156-59-25.0 10
trans-1,2-Dichloroethene ND ug/L 06/17/14 03:12 156-60-55.0 10
1,2-Dichloropropane ND ug/L 06/17/14 03:12 78-87-55.0 10
1,3-Dichloropropane ND ug/L 06/17/14 03:12 142-28-95.0 10
2,2-Dichloropropane ND ug/L 06/17/14 03:12 594-20-75.0 10
1,1-Dichloropropene ND ug/L 06/17/14 03:12 563-58-65.0 10
cis-1,3-Dichloropropene ND ug/L 06/17/14 03:12 10061-01-55.0 10
trans-1,3-Dichloropropene ND ug/L 06/17/14 03:12 10061-02-65.0 10
Diisopropyl ether ND ug/L 06/17/14 03:12 108-20-35.0 10
Ethanol ND ug/L 06/17/14 03:12 64-17-5200010
Ethylbenzene 134 ug/L 06/17/14 03:12 100-41-45.0 10
Ethyl-tert-butyl ether ND ug/L 06/17/14 03:12 637-92-310010
Hexachloro-1,3-butadiene ND ug/L 06/17/14 03:12 87-68-320.0 10
Isopropylbenzene (Cumene)17.9 ug/L 06/17/14 03:12 98-82-85.0 10
Methylene Chloride ND ug/L 06/17/14 03:12 75-09-220.0 10
Methyl-tert-butyl ether ND ug/L 06/17/14 03:12 1634-04-45.0 10
Naphthalene 312 ug/L 06/17/14 03:12 91-20-320.0 10
n-Propylbenzene 26.4 ug/L 06/17/14 03:12 103-65-15.0 10
Styrene ND ug/L 06/17/14 03:12 100-42-55.0 10
1,1,1,2-Tetrachloroethane ND ug/L 06/17/14 03:12 630-20-65.0 10
1,1,2,2-Tetrachloroethane ND ug/L 06/17/14 03:12 79-34-55.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-6 Lab ID:92204984004 Collected:06/11/14 12:30 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene 21.3 ug/L 06/17/14 03:12 127-18-45.0 10
Toluene ND ug/L 06/17/14 03:12 108-88-35.0 10
1,2,3-Trichlorobenzene ND ug/L 06/17/14 03:12 87-61-620.0 10
1,2,4-Trichlorobenzene ND ug/L 06/17/14 03:12 120-82-120.0 10
1,1,1-Trichloroethane ND ug/L 06/17/14 03:12 71-55-65.0 10
1,1,2-Trichloroethane ND ug/L 06/17/14 03:12 79-00-55.0 10
Trichloroethene ND ug/L 06/17/14 03:12 79-01-65.0 10
Trichlorofluoromethane ND ug/L 06/17/14 03:12 75-69-410.0 10
1,2,3-Trichloropropane ND ug/L 06/17/14 03:12 96-18-45.0 10
1,2,4-Trimethylbenzene 332 ug/L 06/17/14 03:12 95-63-65.0 10
1,3,5-Trimethylbenzene 30.2 ug/L 06/17/14 03:12 108-67-85.0 10
Vinyl chloride 221 ug/L 06/17/14 03:12 75-01-410.0 10
m&p-Xylene 89.8 ug/L 06/17/14 03:12 179601-23-110.0 10
o-Xylene 31.7 ug/L 06/17/14 03:12 95-47-65.0 10
Surrogates
1,2-Dichloroethane-d4 (S)95 %06/17/14 03:12 17060-07-070-130 10
4-Bromofluorobenzene (S)100 %06/17/14 03:12 460-00-470-130 10
Toluene-d8 (S)100 %06/17/14 03:12 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-10 Lab ID:92204984005 Collected:06/11/14 11:40 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 06/18/14 18:51 N206/16/14 14:451001
Aliphatic (C19-C36)ND ug/L 06/18/14 18:51 N206/16/14 14:451001
Aromatic (C11-C22)188 ug/L 06/18/14 18:51 N206/16/14 14:451001
Surrogates
Nonatriacontane (S)85 %06/18/14 18:51 7194-86-706/16/14 14:4540-140 1
o-Terphenyl (S)61 %06/18/14 18:51 84-15-106/16/14 14:4540-140 1
2-Fluorobiphenyl (S)54 %06/18/14 18:51 321-60-806/16/14 14:4540-140 1
2-Bromonaphthalene (S)75 %06/18/14 18:51 580-13-206/16/14 14:4540-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)20300 ug/L 06/19/14 09:21 N2125025
Aliphatic (C09-C12)2120 ug/L 06/19/14 09:21 N2125025
Aromatic (C09-C10)ND ug/L 06/19/14 09:21 N2125025
Surrogates
4-Bromofluorobenzene (FID) (S)130 %06/19/14 09:21 460-00-470-130 25
4-Bromofluorobenzene (PID) (S)118 %06/19/14 09:21 460-00-470-130 25
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/16/14 17:31 83-32-906/13/14 12:255.0 1
Acenaphthylene ND ug/L 06/16/14 17:31 208-96-806/13/14 12:255.0 1
Anthracene ND ug/L 06/16/14 17:31 120-12-706/13/14 12:255.0 1
Benzo(a)anthracene ND ug/L 06/16/14 17:31 56-55-306/13/14 12:255.0 1
Benzo(a)pyrene ND ug/L 06/16/14 17:31 50-32-806/13/14 12:255.0 1
Benzo(b)fluoranthene ND ug/L 06/16/14 17:31 205-99-206/13/14 12:255.0 1
Benzo(g,h,i)perylene ND ug/L 06/16/14 17:31 191-24-206/13/14 12:255.0 1
Benzo(k)fluoranthene ND ug/L 06/16/14 17:31 207-08-906/13/14 12:255.0 1
4-Bromophenylphenyl ether ND ug/L 06/16/14 17:31 101-55-306/13/14 12:255.0 1
Butylbenzylphthalate ND ug/L 06/16/14 17:31 85-68-706/13/14 12:255.0 1
4-Chloro-3-methylphenol ND ug/L 06/16/14 17:31 59-50-706/13/14 12:255.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/16/14 17:31 111-91-106/13/14 12:2510.0 1
bis(2-Chloroethyl) ether ND ug/L 06/16/14 17:31 111-44-406/13/14 12:255.0 1
bis(2-Chloroisopropyl) ether ND ug/L 06/16/14 17:31 108-60-106/13/14 12:255.0 1
2-Chloronaphthalene ND ug/L 06/16/14 17:31 91-58-706/13/14 12:255.0 1
2-Chlorophenol ND ug/L 06/16/14 17:31 95-57-806/13/14 12:255.0 1
4-Chlorophenylphenyl ether ND ug/L 06/16/14 17:31 7005-72-306/13/14 12:255.0 1
Chrysene ND ug/L 06/16/14 17:31 218-01-906/13/14 12:255.0 1
Dibenz(a,h)anthracene ND ug/L 06/16/14 17:31 53-70-306/13/14 12:255.0 1
3,3'-Dichlorobenzidine ND ug/L 06/16/14 17:31 91-94-106/13/14 12:2525.0 1
2,4-Dichlorophenol ND ug/L 06/16/14 17:31 120-83-206/13/14 12:255.0 1
Diethylphthalate ND ug/L 06/16/14 17:31 84-66-206/13/14 12:255.0 1
2,4-Dimethylphenol ND ug/L 06/16/14 17:31 105-67-906/13/14 12:2510.0 1
Dimethylphthalate ND ug/L 06/16/14 17:31 131-11-306/13/14 12:255.0 1
Di-n-butylphthalate ND ug/L 06/16/14 17:31 84-74-206/13/14 12:255.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/16/14 17:31 534-52-106/13/14 12:2520.0 1
2,4-Dinitrophenol ND ug/L 06/16/14 17:31 51-28-506/13/14 12:2550.0 1
2,4-Dinitrotoluene ND ug/L 06/16/14 17:31 121-14-206/13/14 12:255.0 1
2,6-Dinitrotoluene ND ug/L 06/16/14 17:31 606-20-206/13/14 12:255.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-10 Lab ID:92204984005 Collected:06/11/14 11:40 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 06/16/14 17:31 117-84-006/13/14 12:255.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/16/14 17:31 117-81-706/13/14 12:255.0 1
Fluoranthene ND ug/L 06/16/14 17:31 206-44-006/13/14 12:255.0 1
Fluorene ND ug/L 06/16/14 17:31 86-73-706/13/14 12:255.0 1
Hexachloro-1,3-butadiene ND ug/L 06/16/14 17:31 87-68-306/13/14 12:255.0 1
Hexachlorobenzene ND ug/L 06/16/14 17:31 118-74-106/13/14 12:255.0 1
Hexachlorocyclopentadiene ND ug/L 06/16/14 17:31 77-47-406/13/14 12:2510.0 1
Hexachloroethane ND ug/L 06/16/14 17:31 67-72-106/13/14 12:255.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/16/14 17:31 193-39-506/13/14 12:255.0 1
Isophorone ND ug/L 06/16/14 17:31 78-59-106/13/14 12:2510.0 1
Naphthalene 65.9 ug/L 06/16/14 17:31 91-20-306/13/14 12:255.0 1
Nitrobenzene ND ug/L 06/16/14 17:31 98-95-306/13/14 12:255.0 1
2-Nitrophenol ND ug/L 06/16/14 17:31 88-75-506/13/14 12:255.0 1
4-Nitrophenol ND ug/L 06/16/14 17:31 100-02-706/13/14 12:2550.0 1
N-Nitrosodimethylamine ND ug/L 06/16/14 17:31 62-75-906/13/14 12:255.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/16/14 17:31 621-64-706/13/14 12:255.0 1
N-Nitrosodiphenylamine ND ug/L 06/16/14 17:31 86-30-606/13/14 12:2510.0 1
Pentachlorophenol ND ug/L 06/16/14 17:31 87-86-506/13/14 12:2510.0 1
Phenanthrene ND ug/L 06/16/14 17:31 85-01-806/13/14 12:255.0 1
Phenol ND ug/L 06/16/14 17:31 108-95-206/13/14 12:255.0 1
Pyrene ND ug/L 06/16/14 17:31 129-00-006/13/14 12:255.0 1
1,2,4-Trichlorobenzene ND ug/L 06/16/14 17:31 120-82-106/13/14 12:255.0 1
2,4,6-Trichlorophenol ND ug/L 06/16/14 17:31 88-06-206/13/14 12:2510.0 1
Surrogates
Nitrobenzene-d5 (S)72 %06/16/14 17:31 4165-60-006/13/14 12:2510-120 1
2-Fluorobiphenyl (S)79 %06/16/14 17:31 321-60-806/13/14 12:2515-120 1
Terphenyl-d14 (S)89 %06/16/14 17:31 1718-51-006/13/14 12:2511-131 1
Phenol-d6 (S)30 %06/16/14 17:31 13127-88-306/13/14 12:2510-120 1
2-Fluorophenol (S)44 %06/16/14 17:31 367-12-406/13/14 12:2510-120 1
2,4,6-Tribromophenol (S)76 %06/16/14 17:31 118-79-606/13/14 12:2510-137 1
Tentatively Identified Compounds
2-Butanol, 2,3-dimethyl-168 ug/L 06/16/14 17:31 594-60-5 N06/13/14 12:251
2-Pentanol, 2-methyl-627 ug/L 06/16/14 17:31 590-36-3 N06/13/14 12:251
Cyclopentanol, 1-methyl-432 ug/L 06/16/14 17:31 1462-03-9 N06/13/14 12:251
2-Hexanol, 2-methyl-179 ug/L 06/16/14 17:31 625-23-0 N06/13/14 12:251
Unknown 458 ug/L 06/16/14 17:31 N06/13/14 12:251
Ethylbenzene 215 ug/L 06/16/14 17:31 100-41-4 N06/13/14 12:251
1-Methylcyclohexanol 159 ug/L 06/16/14 17:31 590-67-0 N06/13/14 12:251
Unknown 88.7 ug/L 06/16/14 17:31 N06/13/14 12:251
Benzene, 1-ethyl-2-methy 97.8 ug/L 06/16/14 17:31 611-14-3 N06/13/14 12:251
Unknown 186 ug/L 06/16/14 17:31 N06/13/14 12:251
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol 10300 ug/L 06/13/14 09:05 75-85-4100010
tert-Amylmethyl ether ND ug/L 06/13/14 09:05 994-05-810010
Benzene 2720 ug/L 06/16/14 23:54 71-43-212.5 25
Bromobenzene ND ug/L 06/13/14 09:05 108-86-15.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-10 Lab ID:92204984005 Collected:06/11/14 11:40 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Bromochloromethane ND ug/L 06/13/14 09:05 74-97-55.0 10
Bromodichloromethane ND ug/L 06/13/14 09:05 75-27-45.0 10
Bromoform ND ug/L 06/13/14 09:05 75-25-25.0 10
Bromomethane ND ug/L 06/13/14 09:05 74-83-950.0 10
tert-Butyl Alcohol 129 ug/L 06/13/14 09:05 75-65-010010
n-Butylbenzene 7.6 ug/L 06/13/14 09:05 104-51-85.0 10
sec-Butylbenzene ND ug/L 06/13/14 09:05 135-98-85.0 10
tert-Butylbenzene ND ug/L 06/13/14 09:05 98-06-65.0 10
tert-Butyl Formate ND ug/L 06/13/14 09:05 762-75-420010
Carbon tetrachloride ND ug/L 06/13/14 09:05 56-23-55.0 10
Chlorobenzene ND ug/L 06/13/14 09:05 108-90-75.0 10
Chloroethane ND ug/L 06/13/14 09:05 75-00-310.0 10
Chloroform ND ug/L 06/13/14 09:05 67-66-35.0 10
Chloromethane ND ug/L 06/13/14 09:05 74-87-310.0 10
2-Chlorotoluene ND ug/L 06/13/14 09:05 95-49-85.0 10
4-Chlorotoluene ND ug/L 06/13/14 09:05 106-43-45.0 10
1,2-Dibromo-3-chloropropane ND ug/L 06/13/14 09:05 96-12-810.0 10
Dibromochloromethane ND ug/L 06/13/14 09:05 124-48-15.0 10
1,2-Dibromoethane (EDB)ND ug/L 06/13/14 09:05 106-93-45.0 10
Dibromomethane ND ug/L 06/13/14 09:05 74-95-35.0 10
1,2-Dichlorobenzene ND ug/L 06/13/14 09:05 95-50-15.0 10
1,3-Dichlorobenzene ND ug/L 06/13/14 09:05 541-73-15.0 10
1,4-Dichlorobenzene ND ug/L 06/13/14 09:05 106-46-75.0 10
Dichlorodifluoromethane ND ug/L 06/13/14 09:05 75-71-85.0 10
1,1-Dichloroethane ND ug/L 06/13/14 09:05 75-34-35.0 10
1,2-Dichloroethane 43.2 ug/L 06/13/14 09:05 107-06-25.0 10
1,1-Dichloroethene ND ug/L 06/13/14 09:05 75-35-45.0 10
cis-1,2-Dichloroethene 555 ug/L 06/13/14 09:05 156-59-25.0 10
trans-1,2-Dichloroethene ND ug/L 06/13/14 09:05 156-60-55.0 10
1,2-Dichloropropane 12.7 ug/L 06/13/14 09:05 78-87-55.0 10
1,3-Dichloropropane ND ug/L 06/13/14 09:05 142-28-95.0 10
2,2-Dichloropropane ND ug/L 06/13/14 09:05 594-20-75.0 10
1,1-Dichloropropene ND ug/L 06/13/14 09:05 563-58-65.0 10
cis-1,3-Dichloropropene ND ug/L 06/13/14 09:05 10061-01-55.0 10
trans-1,3-Dichloropropene ND ug/L 06/13/14 09:05 10061-02-65.0 10
Diisopropyl ether ND ug/L 06/13/14 09:05 108-20-35.0 10
Ethanol ND ug/L 06/13/14 09:05 64-17-5200010
Ethylbenzene 514 ug/L 06/13/14 09:05 100-41-45.0 10
Ethyl-tert-butyl ether ND ug/L 06/13/14 09:05 637-92-310010
Hexachloro-1,3-butadiene ND ug/L 06/13/14 09:05 87-68-320.0 10
Isopropylbenzene (Cumene)33.8 ug/L 06/13/14 09:05 98-82-85.0 10
Methylene Chloride ND ug/L 06/13/14 09:05 75-09-220.0 10
Methyl-tert-butyl ether ND ug/L 06/13/14 09:05 1634-04-45.0 10
Naphthalene 108 ug/L 06/13/14 09:05 91-20-320.0 10
n-Propylbenzene 58.6 ug/L 06/13/14 09:05 103-65-15.0 10
Styrene ND ug/L 06/13/14 09:05 100-42-55.0 10
1,1,1,2-Tetrachloroethane ND ug/L 06/13/14 09:05 630-20-65.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-10 Lab ID:92204984005 Collected:06/11/14 11:40 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
1,1,2,2-Tetrachloroethane ND ug/L 06/13/14 09:05 79-34-55.0 10
Tetrachloroethene ND ug/L 06/13/14 09:05 127-18-45.0 10
Toluene 71.4 ug/L 06/13/14 09:05 108-88-35.0 10
1,2,3-Trichlorobenzene ND ug/L 06/13/14 09:05 87-61-620.0 10
1,2,4-Trichlorobenzene ND ug/L 06/13/14 09:05 120-82-120.0 10
1,1,1-Trichloroethane ND ug/L 06/13/14 09:05 71-55-65.0 10
1,1,2-Trichloroethane ND ug/L 06/13/14 09:05 79-00-55.0 10
Trichloroethene ND ug/L 06/13/14 09:05 79-01-65.0 10
Trichlorofluoromethane ND ug/L 06/13/14 09:05 75-69-410.0 10
1,2,3-Trichloropropane ND ug/L 06/13/14 09:05 96-18-45.0 10
1,2,4-Trimethylbenzene 53.0 ug/L 06/13/14 09:05 95-63-65.0 10
1,3,5-Trimethylbenzene 29.6 ug/L 06/13/14 09:05 108-67-85.0 10
Vinyl chloride ND ug/L 06/13/14 09:05 75-01-410.0 10
m&p-Xylene 129 ug/L 06/13/14 09:05 179601-23-110.0 10
o-Xylene 51.0 ug/L 06/13/14 09:05 95-47-65.0 10
Surrogates
1,2-Dichloroethane-d4 (S)97 %06/13/14 09:05 17060-07-070-130 10
4-Bromofluorobenzene (S)102 %06/13/14 09:05 460-00-470-130 10
Toluene-d8 (S)99 %06/13/14 09:05 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-13 Lab ID:92204984006 Collected:06/11/14 13:30 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 06/18/14 19:23 N206/16/14 14:451001
Aliphatic (C19-C36)ND ug/L 06/18/14 19:23 N206/16/14 14:451001
Aromatic (C11-C22)ND ug/L 06/18/14 19:23 N206/16/14 14:451001
Surrogates
Nonatriacontane (S)85 %06/18/14 19:23 7194-86-706/16/14 14:4540-140 1
o-Terphenyl (S)70 %06/18/14 19:23 84-15-106/16/14 14:4540-140 1
2-Fluorobiphenyl (S)72 %06/18/14 19:23 321-60-806/16/14 14:4540-140 1
2-Bromonaphthalene (S)76 %06/18/14 19:23 580-13-206/16/14 14:4540-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)241 ug/L 06/19/14 00:19 N250.0 1
Aliphatic (C09-C12)ND ug/L 06/19/14 00:19 N250.0 1
Aromatic (C09-C10)ND ug/L 06/19/14 00:19 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)116 %06/19/14 00:19 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)107 %06/19/14 00:19 460-00-470-130 1
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/16/14 17:58 83-32-906/13/14 12:255.0 1
Acenaphthylene ND ug/L 06/16/14 17:58 208-96-806/13/14 12:255.0 1
Anthracene ND ug/L 06/16/14 17:58 120-12-706/13/14 12:255.0 1
Benzo(a)anthracene ND ug/L 06/16/14 17:58 56-55-306/13/14 12:255.0 1
Benzo(a)pyrene ND ug/L 06/16/14 17:58 50-32-806/13/14 12:255.0 1
Benzo(b)fluoranthene ND ug/L 06/16/14 17:58 205-99-206/13/14 12:255.0 1
Benzo(g,h,i)perylene ND ug/L 06/16/14 17:58 191-24-206/13/14 12:255.0 1
Benzo(k)fluoranthene ND ug/L 06/16/14 17:58 207-08-906/13/14 12:255.0 1
4-Bromophenylphenyl ether ND ug/L 06/16/14 17:58 101-55-306/13/14 12:255.0 1
Butylbenzylphthalate ND ug/L 06/16/14 17:58 85-68-706/13/14 12:255.0 1
4-Chloro-3-methylphenol ND ug/L 06/16/14 17:58 59-50-706/13/14 12:255.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/16/14 17:58 111-91-106/13/14 12:2510.0 1
bis(2-Chloroethyl) ether ND ug/L 06/16/14 17:58 111-44-406/13/14 12:255.0 1
bis(2-Chloroisopropyl) ether ND ug/L 06/16/14 17:58 108-60-106/13/14 12:255.0 1
2-Chloronaphthalene ND ug/L 06/16/14 17:58 91-58-706/13/14 12:255.0 1
2-Chlorophenol ND ug/L 06/16/14 17:58 95-57-806/13/14 12:255.0 1
4-Chlorophenylphenyl ether ND ug/L 06/16/14 17:58 7005-72-306/13/14 12:255.0 1
Chrysene ND ug/L 06/16/14 17:58 218-01-906/13/14 12:255.0 1
Dibenz(a,h)anthracene ND ug/L 06/16/14 17:58 53-70-306/13/14 12:255.0 1
3,3'-Dichlorobenzidine ND ug/L 06/16/14 17:58 91-94-106/13/14 12:2525.0 1
2,4-Dichlorophenol ND ug/L 06/16/14 17:58 120-83-206/13/14 12:255.0 1
Diethylphthalate ND ug/L 06/16/14 17:58 84-66-206/13/14 12:255.0 1
2,4-Dimethylphenol ND ug/L 06/16/14 17:58 105-67-906/13/14 12:2510.0 1
Dimethylphthalate ND ug/L 06/16/14 17:58 131-11-306/13/14 12:255.0 1
Di-n-butylphthalate ND ug/L 06/16/14 17:58 84-74-206/13/14 12:255.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/16/14 17:58 534-52-106/13/14 12:2520.0 1
2,4-Dinitrophenol ND ug/L 06/16/14 17:58 51-28-506/13/14 12:2550.0 1
2,4-Dinitrotoluene ND ug/L 06/16/14 17:58 121-14-206/13/14 12:255.0 1
2,6-Dinitrotoluene ND ug/L 06/16/14 17:58 606-20-206/13/14 12:255.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-13 Lab ID:92204984006 Collected:06/11/14 13:30 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 06/16/14 17:58 117-84-006/13/14 12:255.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/16/14 17:58 117-81-706/13/14 12:255.0 1
Fluoranthene ND ug/L 06/16/14 17:58 206-44-006/13/14 12:255.0 1
Fluorene ND ug/L 06/16/14 17:58 86-73-706/13/14 12:255.0 1
Hexachloro-1,3-butadiene ND ug/L 06/16/14 17:58 87-68-306/13/14 12:255.0 1
Hexachlorobenzene ND ug/L 06/16/14 17:58 118-74-106/13/14 12:255.0 1
Hexachlorocyclopentadiene ND ug/L 06/16/14 17:58 77-47-406/13/14 12:2510.0 1
Hexachloroethane ND ug/L 06/16/14 17:58 67-72-106/13/14 12:255.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/16/14 17:58 193-39-506/13/14 12:255.0 1
Isophorone ND ug/L 06/16/14 17:58 78-59-106/13/14 12:2510.0 1
Naphthalene ND ug/L 06/16/14 17:58 91-20-306/13/14 12:255.0 1
Nitrobenzene ND ug/L 06/16/14 17:58 98-95-306/13/14 12:255.0 1
2-Nitrophenol ND ug/L 06/16/14 17:58 88-75-506/13/14 12:255.0 1
4-Nitrophenol ND ug/L 06/16/14 17:58 100-02-706/13/14 12:2550.0 1
N-Nitrosodimethylamine ND ug/L 06/16/14 17:58 62-75-906/13/14 12:255.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/16/14 17:58 621-64-706/13/14 12:255.0 1
N-Nitrosodiphenylamine ND ug/L 06/16/14 17:58 86-30-606/13/14 12:2510.0 1
Pentachlorophenol ND ug/L 06/16/14 17:58 87-86-506/13/14 12:2510.0 1
Phenanthrene ND ug/L 06/16/14 17:58 85-01-806/13/14 12:255.0 1
Phenol ND ug/L 06/16/14 17:58 108-95-206/13/14 12:255.0 1
Pyrene ND ug/L 06/16/14 17:58 129-00-006/13/14 12:255.0 1
1,2,4-Trichlorobenzene ND ug/L 06/16/14 17:58 120-82-106/13/14 12:255.0 1
2,4,6-Trichlorophenol ND ug/L 06/16/14 17:58 88-06-206/13/14 12:2510.0 1
Surrogates
Nitrobenzene-d5 (S)67 %06/16/14 17:58 4165-60-006/13/14 12:2510-120 1
2-Fluorobiphenyl (S)76 %06/16/14 17:58 321-60-806/13/14 12:2515-120 1
Terphenyl-d14 (S)90 %06/16/14 17:58 1718-51-006/13/14 12:2511-131 1
Phenol-d6 (S)29 %06/16/14 17:58 13127-88-306/13/14 12:2510-120 1
2-Fluorophenol (S)42 %06/16/14 17:58 367-12-406/13/14 12:2510-120 1
2,4,6-Tribromophenol (S)76 %06/16/14 17:58 118-79-606/13/14 12:2510-137 1
Tentatively Identified Compounds
Tetrachloroethylene 142 ug/L 06/16/14 17:58 127-18-4 N06/13/14 12:251
9,12-Octadecadienoic ac 9.6 ug/L 06/16/14 17:58 60-33-3 N06/13/14 12:251
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol ND ug/L 06/13/14 04:55 75-85-41001
tert-Amylmethyl ether ND ug/L 06/13/14 04:55 994-05-810.0 1
Benzene ND ug/L 06/13/14 04:55 71-43-20.50 1
Bromobenzene ND ug/L 06/13/14 04:55 108-86-10.50 1
Bromochloromethane ND ug/L 06/13/14 04:55 74-97-50.50 1
Bromodichloromethane ND ug/L 06/13/14 04:55 75-27-40.50 1
Bromoform ND ug/L 06/13/14 04:55 75-25-20.50 1
Bromomethane ND ug/L 06/13/14 04:55 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 06/13/14 04:55 75-65-010.0 1
n-Butylbenzene ND ug/L 06/13/14 04:55 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/13/14 04:55 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/13/14 04:55 98-06-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-13 Lab ID:92204984006 Collected:06/11/14 13:30 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
tert-Butyl Formate ND ug/L 06/13/14 04:55 762-75-420.0 1
Carbon tetrachloride ND ug/L 06/13/14 04:55 56-23-50.50 1
Chlorobenzene ND ug/L 06/13/14 04:55 108-90-70.50 1
Chloroethane ND ug/L 06/13/14 04:55 75-00-31.0 1
Chloroform ND ug/L 06/13/14 04:55 67-66-30.50 1
Chloromethane ND ug/L 06/13/14 04:55 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/13/14 04:55 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/13/14 04:55 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/13/14 04:55 96-12-81.0 1
Dibromochloromethane ND ug/L 06/13/14 04:55 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/13/14 04:55 106-93-40.50 1
Dibromomethane ND ug/L 06/13/14 04:55 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/13/14 04:55 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/13/14 04:55 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/13/14 04:55 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/13/14 04:55 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/13/14 04:55 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/13/14 04:55 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/13/14 04:55 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/13/14 04:55 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/13/14 04:55 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/13/14 04:55 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/13/14 04:55 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/13/14 04:55 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/13/14 04:55 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/13/14 04:55 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/13/14 04:55 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/13/14 04:55 108-20-30.50 1
Ethanol ND ug/L 06/13/14 04:55 64-17-52001
Ethylbenzene ND ug/L 06/13/14 04:55 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 06/13/14 04:55 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 06/13/14 04:55 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/13/14 04:55 98-82-80.50 1
Methylene Chloride ND ug/L 06/13/14 04:55 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/13/14 04:55 1634-04-40.50 1
Naphthalene ND ug/L 06/13/14 04:55 91-20-32.0 1
n-Propylbenzene ND ug/L 06/13/14 04:55 103-65-10.50 1
Styrene ND ug/L 06/13/14 04:55 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/13/14 04:55 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/13/14 04:55 79-34-50.50 1
Tetrachloroethene 431 ug/L 06/16/14 23:37 127-18-42.5 5
Toluene ND ug/L 06/13/14 04:55 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/13/14 04:55 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/13/14 04:55 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/13/14 04:55 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/13/14 04:55 79-00-50.50 1
Trichloroethene 2.6 ug/L 06/13/14 04:55 79-01-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-13 Lab ID:92204984006 Collected:06/11/14 13:30 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Trichlorofluoromethane ND ug/L 06/13/14 04:55 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/13/14 04:55 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/13/14 04:55 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/13/14 04:55 108-67-80.50 1
Vinyl chloride ND ug/L 06/13/14 04:55 75-01-41.0 1
m&p-Xylene ND ug/L 06/13/14 04:55 179601-23-11.0 1
o-Xylene ND ug/L 06/13/14 04:55 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)95 %06/13/14 04:55 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %06/13/14 04:55 460-00-470-130 1
Toluene-d8 (S)98 %06/13/14 04:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-14 Lab ID:92204984007 Collected:06/11/14 13:20 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 06/18/14 19:56 N206/16/14 14:451001
Aliphatic (C19-C36)ND ug/L 06/18/14 19:56 N206/16/14 14:451001
Aromatic (C11-C22)ND ug/L 06/18/14 19:56 N206/16/14 14:451001
Surrogates
Nonatriacontane (S)77 %06/18/14 19:56 7194-86-706/16/14 14:4540-140 1
o-Terphenyl (S)47 %06/18/14 19:56 84-15-106/16/14 14:4540-140 1
2-Fluorobiphenyl (S)53 %06/18/14 19:56 321-60-806/16/14 14:4540-140 1
2-Bromonaphthalene (S)67 %06/18/14 19:56 580-13-206/16/14 14:4540-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 06/19/14 00:42 N250.0 1
Aliphatic (C09-C12)ND ug/L 06/19/14 00:42 N250.0 1
Aromatic (C09-C10)ND ug/L 06/19/14 00:42 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)121 %06/19/14 00:42 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)109 %06/19/14 00:42 460-00-470-130 1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium 48.7 ug/L 06/13/14 20:05 7440-47-306/12/14 15:105.0 1
Lead 21.4 ug/L 06/13/14 20:05 7439-92-106/12/14 15:105.0 1
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/16/14 18:26 83-32-906/13/14 12:255.6 1
Acenaphthylene ND ug/L 06/16/14 18:26 208-96-806/13/14 12:255.6 1
Anthracene ND ug/L 06/16/14 18:26 120-12-706/13/14 12:255.6 1
Benzo(a)anthracene ND ug/L 06/16/14 18:26 56-55-306/13/14 12:255.6 1
Benzo(a)pyrene ND ug/L 06/16/14 18:26 50-32-806/13/14 12:255.6 1
Benzo(b)fluoranthene ND ug/L 06/16/14 18:26 205-99-206/13/14 12:255.6 1
Benzo(g,h,i)perylene ND ug/L 06/16/14 18:26 191-24-206/13/14 12:255.6 1
Benzo(k)fluoranthene ND ug/L 06/16/14 18:26 207-08-906/13/14 12:255.6 1
4-Bromophenylphenyl ether ND ug/L 06/16/14 18:26 101-55-306/13/14 12:255.6 1
Butylbenzylphthalate ND ug/L 06/16/14 18:26 85-68-706/13/14 12:255.6 1
4-Chloro-3-methylphenol ND ug/L 06/16/14 18:26 59-50-706/13/14 12:255.6 1
bis(2-Chloroethoxy)methane ND ug/L 06/16/14 18:26 111-91-106/13/14 12:2511.1 1
bis(2-Chloroethyl) ether ND ug/L 06/16/14 18:26 111-44-406/13/14 12:255.6 1
bis(2-Chloroisopropyl) ether ND ug/L 06/16/14 18:26 108-60-106/13/14 12:255.6 1
2-Chloronaphthalene ND ug/L 06/16/14 18:26 91-58-706/13/14 12:255.6 1
2-Chlorophenol ND ug/L 06/16/14 18:26 95-57-806/13/14 12:255.6 1
4-Chlorophenylphenyl ether ND ug/L 06/16/14 18:26 7005-72-306/13/14 12:255.6 1
Chrysene ND ug/L 06/16/14 18:26 218-01-906/13/14 12:255.6 1
Dibenz(a,h)anthracene ND ug/L 06/16/14 18:26 53-70-306/13/14 12:255.6 1
3,3'-Dichlorobenzidine ND ug/L 06/16/14 18:26 91-94-106/13/14 12:2527.8 1
2,4-Dichlorophenol ND ug/L 06/16/14 18:26 120-83-206/13/14 12:255.6 1
Diethylphthalate ND ug/L 06/16/14 18:26 84-66-206/13/14 12:255.6 1
2,4-Dimethylphenol ND ug/L 06/16/14 18:26 105-67-906/13/14 12:2511.1 1
Dimethylphthalate ND ug/L 06/16/14 18:26 131-11-306/13/14 12:255.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-14 Lab ID:92204984007 Collected:06/11/14 13:20 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-butylphthalate ND ug/L 06/16/14 18:26 84-74-206/13/14 12:255.6 1
4,6-Dinitro-2-methylphenol ND ug/L 06/16/14 18:26 534-52-106/13/14 12:2522.2 1
2,4-Dinitrophenol ND ug/L 06/16/14 18:26 51-28-506/13/14 12:2555.6 1
2,4-Dinitrotoluene ND ug/L 06/16/14 18:26 121-14-206/13/14 12:255.6 1
2,6-Dinitrotoluene ND ug/L 06/16/14 18:26 606-20-206/13/14 12:255.6 1
Di-n-octylphthalate ND ug/L 06/16/14 18:26 117-84-006/13/14 12:255.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/16/14 18:26 117-81-706/13/14 12:255.6 1
Fluoranthene ND ug/L 06/16/14 18:26 206-44-006/13/14 12:255.6 1
Fluorene ND ug/L 06/16/14 18:26 86-73-706/13/14 12:255.6 1
Hexachloro-1,3-butadiene ND ug/L 06/16/14 18:26 87-68-306/13/14 12:255.6 1
Hexachlorobenzene ND ug/L 06/16/14 18:26 118-74-106/13/14 12:255.6 1
Hexachlorocyclopentadiene ND ug/L 06/16/14 18:26 77-47-406/13/14 12:2511.1 1
Hexachloroethane ND ug/L 06/16/14 18:26 67-72-106/13/14 12:255.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/16/14 18:26 193-39-506/13/14 12:255.6 1
Isophorone ND ug/L 06/16/14 18:26 78-59-106/13/14 12:2511.1 1
Naphthalene ND ug/L 06/16/14 18:26 91-20-306/13/14 12:255.6 1
Nitrobenzene ND ug/L 06/16/14 18:26 98-95-306/13/14 12:255.6 1
2-Nitrophenol ND ug/L 06/16/14 18:26 88-75-506/13/14 12:255.6 1
4-Nitrophenol ND ug/L 06/16/14 18:26 100-02-706/13/14 12:2555.6 1
N-Nitrosodimethylamine ND ug/L 06/16/14 18:26 62-75-906/13/14 12:255.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/16/14 18:26 621-64-706/13/14 12:255.6 1
N-Nitrosodiphenylamine ND ug/L 06/16/14 18:26 86-30-606/13/14 12:2511.1 1
Pentachlorophenol ND ug/L 06/16/14 18:26 87-86-506/13/14 12:2511.1 1
Phenanthrene ND ug/L 06/16/14 18:26 85-01-806/13/14 12:255.6 1
Phenol ND ug/L 06/16/14 18:26 108-95-206/13/14 12:255.6 1
Pyrene ND ug/L 06/16/14 18:26 129-00-006/13/14 12:255.6 1
1,2,4-Trichlorobenzene ND ug/L 06/16/14 18:26 120-82-106/13/14 12:255.6 1
2,4,6-Trichlorophenol ND ug/L 06/16/14 18:26 88-06-206/13/14 12:2511.1 1
Surrogates
Nitrobenzene-d5 (S)64 %06/16/14 18:26 4165-60-006/13/14 12:2510-120 1
2-Fluorobiphenyl (S)74 %06/16/14 18:26 321-60-806/13/14 12:2515-120 1
Terphenyl-d14 (S)80 %06/16/14 18:26 1718-51-006/13/14 12:2511-131 1
Phenol-d6 (S)42 %06/16/14 18:26 13127-88-306/13/14 12:2510-120 1
2-Fluorophenol (S)51 %06/16/14 18:26 367-12-406/13/14 12:2510-120 1
2,4,6-Tribromophenol (S)74 %06/16/14 18:26 118-79-606/13/14 12:2510-137 1
Tentatively Identified Compounds
Unknown 116 ug/L 06/16/14 18:26 N06/13/14 12:251
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol ND ug/L 06/17/14 02:06 75-85-41001
tert-Amylmethyl ether ND ug/L 06/17/14 02:06 994-05-810.0 1
Benzene ND ug/L 06/17/14 02:06 71-43-20.50 1
Bromobenzene ND ug/L 06/17/14 02:06 108-86-10.50 1
Bromochloromethane ND ug/L 06/17/14 02:06 74-97-50.50 1
Bromodichloromethane ND ug/L 06/17/14 02:06 75-27-40.50 1
Bromoform ND ug/L 06/17/14 02:06 75-25-20.50 1
Bromomethane ND ug/L 06/17/14 02:06 74-83-95.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-14 Lab ID:92204984007 Collected:06/11/14 13:20 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
tert-Butyl Alcohol ND ug/L 06/17/14 02:06 75-65-010.0 1
n-Butylbenzene ND ug/L 06/17/14 02:06 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/17/14 02:06 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/17/14 02:06 98-06-60.50 1
tert-Butyl Formate ND ug/L 06/17/14 02:06 762-75-420.0 1
Carbon tetrachloride ND ug/L 06/17/14 02:06 56-23-50.50 1
Chlorobenzene ND ug/L 06/17/14 02:06 108-90-70.50 1
Chloroethane ND ug/L 06/17/14 02:06 75-00-31.0 1
Chloroform ND ug/L 06/17/14 02:06 67-66-30.50 1
Chloromethane ND ug/L 06/17/14 02:06 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/17/14 02:06 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/17/14 02:06 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/14 02:06 96-12-81.0 1
Dibromochloromethane ND ug/L 06/17/14 02:06 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/14 02:06 106-93-40.50 1
Dibromomethane ND ug/L 06/17/14 02:06 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/17/14 02:06 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/17/14 02:06 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/17/14 02:06 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/17/14 02:06 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/17/14 02:06 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/17/14 02:06 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/17/14 02:06 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/17/14 02:06 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/17/14 02:06 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/17/14 02:06 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/17/14 02:06 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/17/14 02:06 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/17/14 02:06 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/17/14 02:06 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/17/14 02:06 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/17/14 02:06 108-20-30.50 1
Ethanol ND ug/L 06/17/14 02:06 64-17-52001
Ethylbenzene ND ug/L 06/17/14 02:06 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 06/17/14 02:06 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 06/17/14 02:06 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/17/14 02:06 98-82-80.50 1
Methylene Chloride ND ug/L 06/17/14 02:06 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/17/14 02:06 1634-04-40.50 1
Naphthalene ND ug/L 06/17/14 02:06 91-20-32.0 1
n-Propylbenzene ND ug/L 06/17/14 02:06 103-65-10.50 1
Styrene ND ug/L 06/17/14 02:06 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/17/14 02:06 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/14 02:06 79-34-50.50 1
Tetrachloroethene 0.67 ug/L 06/17/14 02:06 127-18-40.50 1
Toluene ND ug/L 06/17/14 02:06 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/17/14 02:06 87-61-62.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-14 Lab ID:92204984007 Collected:06/11/14 13:20 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
1,2,4-Trichlorobenzene ND ug/L 06/17/14 02:06 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/17/14 02:06 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/17/14 02:06 79-00-50.50 1
Trichloroethene ND ug/L 06/17/14 02:06 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/17/14 02:06 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/17/14 02:06 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/17/14 02:06 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/17/14 02:06 108-67-80.50 1
Vinyl chloride ND ug/L 06/17/14 02:06 75-01-41.0 1
m&p-Xylene ND ug/L 06/17/14 02:06 179601-23-11.0 1
o-Xylene ND ug/L 06/17/14 02:06 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %06/17/14 02:06 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %06/17/14 02:06 460-00-470-130 1
Toluene-d8 (S)99 %06/17/14 02:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-15 Lab ID:92204984008 Collected:06/11/14 14:15 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 06/18/14 20:28 N206/16/14 14:451001
Aliphatic (C19-C36)ND ug/L 06/18/14 20:28 N206/16/14 14:451001
Aromatic (C11-C22)ND ug/L 06/18/14 20:28 N206/16/14 14:451001
Surrogates
Nonatriacontane (S)71 %06/18/14 20:28 7194-86-706/16/14 14:4540-140 1
o-Terphenyl (S)86 %06/18/14 20:28 84-15-106/16/14 14:4540-140 1
2-Fluorobiphenyl (S)99 %06/18/14 20:28 321-60-806/16/14 14:4540-140 1
2-Bromonaphthalene (S)109 %06/18/14 20:28 580-13-206/16/14 14:4540-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 06/19/14 01:05 N250.0 1
Aliphatic (C09-C12)ND ug/L 06/19/14 01:05 N250.0 1
Aromatic (C09-C10)ND ug/L 06/19/14 01:05 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)118 %06/19/14 01:05 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)105 %06/19/14 01:05 460-00-470-130 1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium ND ug/L 06/13/14 20:19 7440-47-306/12/14 15:105.0 1
Lead ND ug/L 06/13/14 20:19 7439-92-106/12/14 15:105.0 1
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/16/14 18:54 83-32-906/13/14 12:255.6 1
Acenaphthylene ND ug/L 06/16/14 18:54 208-96-806/13/14 12:255.6 1
Anthracene ND ug/L 06/16/14 18:54 120-12-706/13/14 12:255.6 1
Benzo(a)anthracene ND ug/L 06/16/14 18:54 56-55-306/13/14 12:255.6 1
Benzo(a)pyrene ND ug/L 06/16/14 18:54 50-32-806/13/14 12:255.6 1
Benzo(b)fluoranthene ND ug/L 06/16/14 18:54 205-99-206/13/14 12:255.6 1
Benzo(g,h,i)perylene ND ug/L 06/16/14 18:54 191-24-206/13/14 12:255.6 1
Benzo(k)fluoranthene ND ug/L 06/16/14 18:54 207-08-906/13/14 12:255.6 1
4-Bromophenylphenyl ether ND ug/L 06/16/14 18:54 101-55-306/13/14 12:255.6 1
Butylbenzylphthalate ND ug/L 06/16/14 18:54 85-68-706/13/14 12:255.6 1
4-Chloro-3-methylphenol ND ug/L 06/16/14 18:54 59-50-706/13/14 12:255.6 1
bis(2-Chloroethoxy)methane ND ug/L 06/16/14 18:54 111-91-106/13/14 12:2511.1 1
bis(2-Chloroethyl) ether ND ug/L 06/16/14 18:54 111-44-406/13/14 12:255.6 1
bis(2-Chloroisopropyl) ether ND ug/L 06/16/14 18:54 108-60-106/13/14 12:255.6 1
2-Chloronaphthalene ND ug/L 06/16/14 18:54 91-58-706/13/14 12:255.6 1
2-Chlorophenol ND ug/L 06/16/14 18:54 95-57-806/13/14 12:255.6 1
4-Chlorophenylphenyl ether ND ug/L 06/16/14 18:54 7005-72-306/13/14 12:255.6 1
Chrysene ND ug/L 06/16/14 18:54 218-01-906/13/14 12:255.6 1
Dibenz(a,h)anthracene ND ug/L 06/16/14 18:54 53-70-306/13/14 12:255.6 1
3,3'-Dichlorobenzidine ND ug/L 06/16/14 18:54 91-94-106/13/14 12:2527.8 1
2,4-Dichlorophenol ND ug/L 06/16/14 18:54 120-83-206/13/14 12:255.6 1
Diethylphthalate ND ug/L 06/16/14 18:54 84-66-206/13/14 12:255.6 1
2,4-Dimethylphenol ND ug/L 06/16/14 18:54 105-67-906/13/14 12:2511.1 1
Dimethylphthalate ND ug/L 06/16/14 18:54 131-11-306/13/14 12:255.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-15 Lab ID:92204984008 Collected:06/11/14 14:15 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-butylphthalate ND ug/L 06/16/14 18:54 84-74-206/13/14 12:255.6 1
4,6-Dinitro-2-methylphenol ND ug/L 06/16/14 18:54 534-52-106/13/14 12:2522.2 1
2,4-Dinitrophenol ND ug/L 06/16/14 18:54 51-28-506/13/14 12:2555.6 1
2,4-Dinitrotoluene ND ug/L 06/16/14 18:54 121-14-206/13/14 12:255.6 1
2,6-Dinitrotoluene ND ug/L 06/16/14 18:54 606-20-206/13/14 12:255.6 1
Di-n-octylphthalate ND ug/L 06/16/14 18:54 117-84-006/13/14 12:255.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/16/14 18:54 117-81-706/13/14 12:255.6 1
Fluoranthene ND ug/L 06/16/14 18:54 206-44-006/13/14 12:255.6 1
Fluorene ND ug/L 06/16/14 18:54 86-73-706/13/14 12:255.6 1
Hexachloro-1,3-butadiene ND ug/L 06/16/14 18:54 87-68-306/13/14 12:255.6 1
Hexachlorobenzene ND ug/L 06/16/14 18:54 118-74-106/13/14 12:255.6 1
Hexachlorocyclopentadiene ND ug/L 06/16/14 18:54 77-47-406/13/14 12:2511.1 1
Hexachloroethane ND ug/L 06/16/14 18:54 67-72-106/13/14 12:255.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/16/14 18:54 193-39-506/13/14 12:255.6 1
Isophorone ND ug/L 06/16/14 18:54 78-59-106/13/14 12:2511.1 1
Naphthalene ND ug/L 06/16/14 18:54 91-20-306/13/14 12:255.6 1
Nitrobenzene ND ug/L 06/16/14 18:54 98-95-306/13/14 12:255.6 1
2-Nitrophenol ND ug/L 06/16/14 18:54 88-75-506/13/14 12:255.6 1
4-Nitrophenol ND ug/L 06/16/14 18:54 100-02-706/13/14 12:2555.6 1
N-Nitrosodimethylamine ND ug/L 06/16/14 18:54 62-75-906/13/14 12:255.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/16/14 18:54 621-64-706/13/14 12:255.6 1
N-Nitrosodiphenylamine ND ug/L 06/16/14 18:54 86-30-606/13/14 12:2511.1 1
Pentachlorophenol ND ug/L 06/16/14 18:54 87-86-506/13/14 12:2511.1 1
Phenanthrene ND ug/L 06/16/14 18:54 85-01-806/13/14 12:255.6 1
Phenol ND ug/L 06/16/14 18:54 108-95-206/13/14 12:255.6 1
Pyrene ND ug/L 06/16/14 18:54 129-00-006/13/14 12:255.6 1
1,2,4-Trichlorobenzene ND ug/L 06/16/14 18:54 120-82-106/13/14 12:255.6 1
2,4,6-Trichlorophenol ND ug/L 06/16/14 18:54 88-06-206/13/14 12:2511.1 1
Surrogates
Nitrobenzene-d5 (S)61 %06/16/14 18:54 4165-60-006/13/14 12:2510-120 1
2-Fluorobiphenyl (S)67 %06/16/14 18:54 321-60-806/13/14 12:2515-120 1
Terphenyl-d14 (S)93 %06/16/14 18:54 1718-51-006/13/14 12:2511-131 1
Phenol-d6 (S)24 %06/16/14 18:54 13127-88-306/13/14 12:2510-120 1
2-Fluorophenol (S)35 %06/16/14 18:54 367-12-406/13/14 12:2510-120 1
2,4,6-Tribromophenol (S)66 %06/16/14 18:54 118-79-606/13/14 12:2510-137 1
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol ND ug/L 06/17/14 02:22 75-85-41001
tert-Amylmethyl ether ND ug/L 06/17/14 02:22 994-05-810.0 1
Benzene ND ug/L 06/17/14 02:22 71-43-20.50 1
Bromobenzene ND ug/L 06/17/14 02:22 108-86-10.50 1
Bromochloromethane ND ug/L 06/17/14 02:22 74-97-50.50 1
Bromodichloromethane ND ug/L 06/17/14 02:22 75-27-40.50 1
Bromoform ND ug/L 06/17/14 02:22 75-25-20.50 1
Bromomethane ND ug/L 06/17/14 02:22 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 06/17/14 02:22 75-65-010.0 1
n-Butylbenzene ND ug/L 06/17/14 02:22 104-51-80.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-15 Lab ID:92204984008 Collected:06/11/14 14:15 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
sec-Butylbenzene ND ug/L 06/17/14 02:22 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/17/14 02:22 98-06-60.50 1
tert-Butyl Formate ND ug/L 06/17/14 02:22 762-75-420.0 1
Carbon tetrachloride ND ug/L 06/17/14 02:22 56-23-50.50 1
Chlorobenzene ND ug/L 06/17/14 02:22 108-90-70.50 1
Chloroethane ND ug/L 06/17/14 02:22 75-00-31.0 1
Chloroform ND ug/L 06/17/14 02:22 67-66-30.50 1
Chloromethane ND ug/L 06/17/14 02:22 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/17/14 02:22 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/17/14 02:22 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/14 02:22 96-12-81.0 1
Dibromochloromethane ND ug/L 06/17/14 02:22 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/14 02:22 106-93-40.50 1
Dibromomethane ND ug/L 06/17/14 02:22 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/17/14 02:22 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/17/14 02:22 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/17/14 02:22 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/17/14 02:22 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/17/14 02:22 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/17/14 02:22 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/17/14 02:22 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/17/14 02:22 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/17/14 02:22 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/17/14 02:22 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/17/14 02:22 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/17/14 02:22 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/17/14 02:22 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/17/14 02:22 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/17/14 02:22 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/17/14 02:22 108-20-30.50 1
Ethanol ND ug/L 06/17/14 02:22 64-17-52001
Ethylbenzene ND ug/L 06/17/14 02:22 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 06/17/14 02:22 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 06/17/14 02:22 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/17/14 02:22 98-82-80.50 1
Methylene Chloride ND ug/L 06/17/14 02:22 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/17/14 02:22 1634-04-40.50 1
Naphthalene ND ug/L 06/17/14 02:22 91-20-32.0 1
n-Propylbenzene ND ug/L 06/17/14 02:22 103-65-10.50 1
Styrene ND ug/L 06/17/14 02:22 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/17/14 02:22 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/17/14 02:22 79-34-50.50 1
Tetrachloroethene ND ug/L 06/17/14 02:22 127-18-40.50 1
Toluene ND ug/L 06/17/14 02:22 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/17/14 02:22 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/17/14 02:22 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/17/14 02:22 71-55-60.50 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
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Page 35 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-15 Lab ID:92204984008 Collected:06/11/14 14:15 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
1,1,2-Trichloroethane ND ug/L 06/17/14 02:22 79-00-50.50 1
Trichloroethene ND ug/L 06/17/14 02:22 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/17/14 02:22 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/17/14 02:22 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/17/14 02:22 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/17/14 02:22 108-67-80.50 1
Vinyl chloride ND ug/L 06/17/14 02:22 75-01-41.0 1
m&p-Xylene ND ug/L 06/17/14 02:22 179601-23-11.0 1
o-Xylene ND ug/L 06/17/14 02:22 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %06/17/14 02:22 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %06/17/14 02:22 460-00-470-130 1
Toluene-d8 (S)98 %06/17/14 02:22 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-2 Lab ID:92204984009 Collected:06/11/14 00:00 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium ND ug/L 06/13/14 20:22 7440-47-306/12/14 15:105.0 1
Lead ND ug/L 06/13/14 20:22 7439-92-106/12/14 15:105.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-1 Lab ID:92204984010 Collected:06/11/14 00:00 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium 6.0 ug/L 06/13/14 20:26 7440-47-306/12/14 15:105.0 1
Lead ND ug/L 06/13/14 20:26 7439-92-106/12/14 15:105.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
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[phone]
Page 38 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-3 Lab ID:92204984011 Collected:06/11/14 00:00 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium ND ug/L 06/13/14 20:30 7440-47-306/12/14 15:105.0 1
Lead ND ug/L 06/13/14 20:30 7439-92-106/12/14 15:105.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
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[phone]
Page 39 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-5 Lab ID:92204984012 Collected:06/11/14 00:00 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium ND ug/L 06/13/14 20:33 7440-47-306/12/14 15:105.0 1
Lead ND ug/L 06/13/14 20:33 7439-92-106/12/14 15:105.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
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[phone]
Page 40 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-6 Lab ID:92204984013 Collected:06/11/14 00:00 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium ND ug/L 06/13/14 20:46 7440-47-306/12/14 15:405.0 1
Lead ND ug/L 06/13/14 20:46 7439-92-106/12/14 15:405.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-10 Lab ID:92204984014 Collected:06/11/14 00:00 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium ND ug/L 06/13/14 21:07 7440-47-306/12/14 15:405.0 1
Lead ND ug/L 06/13/14 21:07 7439-92-106/12/14 15:405.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 67
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Sample:MW-13 Lab ID:92204984015 Collected:06/11/14 00:00 Received:06/11/14 17:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium ND ug/L 06/13/14 21:11 7440-47-306/12/14 15:405.0 1
Lead ND ug/L 06/13/14 21:11 7439-92-106/12/14 15:405.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
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Huntersville, NC 28078
[phone]
Page 43 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/8229
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples:92204984001, 92204984002, 92204984003, 92204984004, 92204984005, 92204984006, 92204984007,
92204984008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1222141
Associated Lab Samples:92204984001, 92204984002, 92204984003, 92204984004, 92204984005, 92204984006, 92204984007,
92204984008
Matrix:Water
Analyzed
Aliphatic (C05-C08)ug/L ND 50.0 N206/18/14 17:40
Aliphatic (C09-C12)ug/L ND 50.0 N206/18/14 17:40
Aromatic (C09-C10)ug/L ND 50.0 N206/18/14 17:40
4-Bromofluorobenzene (FID) (S)%129 70-130 06/18/14 17:40
4-Bromofluorobenzene (PID) (S)%115 70-130 06/18/14 17:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1222142LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1222143
Aliphatic (C05-C08)ug/L 262 N23008770-13091274 5 25
Aliphatic (C09-C12)ug/L 248 N23008330-13090269 8 25
Aromatic (C09-C10)ug/L 87.0 N21008770-1309089.9 3 25
4-Bromofluorobenzene (FID) (S)%123 70-130124
4-Bromofluorobenzene (PID) (S)%109 70-130110
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/16198
EPA 3010
EPA 6010
6010 MET
Associated Lab Samples:92204984007, 92204984008, 92204984009, 92204984010, 92204984011, 92204984012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1219986
Associated Lab Samples:92204984007, 92204984008, 92204984009, 92204984010, 92204984011, 92204984012
Matrix:Water
Analyzed
Chromium ug/L ND 5.0 06/13/14 18:59
Lead ug/L ND 5.0 06/13/14 18:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1219987LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium ug/L 478500 96 80-120
Lead ug/L 467500 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1219992MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92204755003
1219993
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chromium ug/L 500 92 75-12592 0500ND462462
Lead ug/L 500 89 75-12590 1500ND445448
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/16200
EPA 3010
EPA 6010
6010 MET
Associated Lab Samples:92204984013, 92204984014, 92204984015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1220260
Associated Lab Samples:92204984013, 92204984014, 92204984015
Matrix:Water
Analyzed
Chromium ug/L ND 5.0 06/13/14 20:40
Lead ug/L ND 5.0 06/13/14 20:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1220261LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium ug/L 462500 92 80-120
Lead ug/L 452500 90 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1220262MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92204984013
1220263
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chromium ug/L 500 92 75-12596 4500ND461480
Lead ug/L 500 88 75-12592 4500ND442461
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/27184
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92204984001, 92204984002, 92204984003, 92204984005, 92204984006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1219847
Associated Lab Samples:92204984001, 92204984002, 92204984003, 92204984005, 92204984006
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 06/13/14 03:49
1,1,1-Trichloroethane ug/L ND 0.50 06/13/14 03:49
1,1,2,2-Tetrachloroethane ug/L ND 0.50 06/13/14 03:49
1,1,2-Trichloroethane ug/L ND 0.50 06/13/14 03:49
1,1-Dichloroethane ug/L ND 0.50 06/13/14 03:49
1,1-Dichloroethene ug/L ND 0.50 06/13/14 03:49
1,1-Dichloropropene ug/L ND 0.50 06/13/14 03:49
1,2,3-Trichlorobenzene ug/L ND 2.0 06/13/14 03:49
1,2,3-Trichloropropane ug/L ND 0.50 06/13/14 03:49
1,2,4-Trichlorobenzene ug/L ND 2.0 06/13/14 03:49
1,2,4-Trimethylbenzene ug/L ND 0.50 06/13/14 03:49
1,2-Dibromo-3-chloropropane ug/L ND 1.0 06/13/14 03:49
1,2-Dibromoethane (EDB)ug/L ND 0.50 06/13/14 03:49
1,2-Dichlorobenzene ug/L ND 0.50 06/13/14 03:49
1,2-Dichloroethane ug/L ND 0.50 06/13/14 03:49
1,2-Dichloropropane ug/L ND 0.50 06/13/14 03:49
1,3,5-Trimethylbenzene ug/L ND 0.50 06/13/14 03:49
1,3-Dichlorobenzene ug/L ND 0.50 06/13/14 03:49
1,3-Dichloropropane ug/L ND 0.50 06/13/14 03:49
1,4-Dichlorobenzene ug/L ND 0.50 06/13/14 03:49
2,2-Dichloropropane ug/L ND 0.50 06/13/14 03:49
2-Chlorotoluene ug/L ND 0.50 06/13/14 03:49
4-Chlorotoluene ug/L ND 0.50 06/13/14 03:49
Benzene ug/L ND 0.50 06/13/14 03:49
Bromobenzene ug/L ND 0.50 06/13/14 03:49
Bromochloromethane ug/L ND 0.50 06/13/14 03:49
Bromodichloromethane ug/L ND 0.50 06/13/14 03:49
Bromoform ug/L ND 0.50 06/13/14 03:49
Bromomethane ug/L ND 5.0 06/13/14 03:49
Carbon tetrachloride ug/L ND 0.50 06/13/14 03:49
Chlorobenzene ug/L ND 0.50 06/13/14 03:49
Chloroethane ug/L ND 1.0 06/13/14 03:49
Chloroform ug/L ND 0.50 06/13/14 03:49
Chloromethane ug/L ND 1.0 06/13/14 03:49
cis-1,2-Dichloroethene ug/L ND 0.50 06/13/14 03:49
cis-1,3-Dichloropropene ug/L ND 0.50 06/13/14 03:49
Dibromochloromethane ug/L ND 0.50 06/13/14 03:49
Dibromomethane ug/L ND 0.50 06/13/14 03:49
Dichlorodifluoromethane ug/L ND 0.50 06/13/14 03:49
Diisopropyl ether ug/L ND 0.50 06/13/14 03:49
Ethanol ug/L ND 200 06/13/14 03:49
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
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Page 47 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1219847
Associated Lab Samples:92204984001, 92204984002, 92204984003, 92204984005, 92204984006
Matrix:Water
Analyzed
Ethyl-tert-butyl ether ug/L ND 10.0 06/13/14 03:49
Ethylbenzene ug/L ND 0.50 06/13/14 03:49
Hexachloro-1,3-butadiene ug/L ND 2.0 06/13/14 03:49
Isopropylbenzene (Cumene)ug/L ND 0.50 06/13/14 03:49
m&p-Xylene ug/L ND 1.0 06/13/14 03:49
Methyl-tert-butyl ether ug/L ND 0.50 06/13/14 03:49
Methylene Chloride ug/L ND 2.0 06/13/14 03:49
n-Butylbenzene ug/L ND 0.50 06/13/14 03:49
n-Propylbenzene ug/L ND 0.50 06/13/14 03:49
Naphthalene ug/L ND 2.0 06/13/14 03:49
o-Xylene ug/L ND 0.50 06/13/14 03:49
sec-Butylbenzene ug/L ND 0.50 06/13/14 03:49
Styrene ug/L ND 0.50 06/13/14 03:49
tert-Amyl Alcohol ug/L ND 100 06/13/14 03:49
tert-Amylmethyl ether ug/L ND 10.0 06/13/14 03:49
tert-Butyl Alcohol ug/L ND 10.0 06/13/14 03:49
tert-Butyl Formate ug/L ND 20.0 06/13/14 03:49
tert-Butylbenzene ug/L ND 0.50 06/13/14 03:49
Tetrachloroethene ug/L ND 0.50 06/13/14 03:49
Toluene ug/L ND 0.50 06/13/14 03:49
trans-1,2-Dichloroethene ug/L ND 0.50 06/13/14 03:49
trans-1,3-Dichloropropene ug/L ND 0.50 06/13/14 03:49
Trichloroethene ug/L ND 0.50 06/13/14 03:49
Trichlorofluoromethane ug/L ND 1.0 06/13/14 03:49
Vinyl chloride ug/L ND 1.0 06/13/14 03:49
1,2-Dichloroethane-d4 (S)%95 70-130 06/13/14 03:49
4-Bromofluorobenzene (S)%103 70-130 06/13/14 03:49
Toluene-d8 (S)%100 70-130 06/13/14 03:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1219848LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 58.350 117 60-140
1,1,1-Trichloroethane ug/L 50.650 101 60-140
1,1,2,2-Tetrachloroethane ug/L 51.350 103 60-140
1,1,2-Trichloroethane ug/L 51.350 103 60-140
1,1-Dichloroethane ug/L 46.450 93 60-140
1,1-Dichloroethene ug/L 50.650 101 60-140
1,1-Dichloropropene ug/L 50.150 100 60-140
1,2,3-Trichlorobenzene ug/L 54.150 108 60-140
1,2,3-Trichloropropane ug/L 52.950 106 60-140
1,2,4-Trichlorobenzene ug/L 52.150 104 60-140
1,2,4-Trimethylbenzene ug/L 53.850 108 60-140
1,2-Dibromo-3-chloropropane ug/L 57.750 115 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
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[phone]
Page 48 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1219848LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromoethane (EDB)ug/L 53.850 108 60-140
1,2-Dichlorobenzene ug/L 54.650 109 60-140
1,2-Dichloroethane ug/L 47.950 96 60-140
1,2-Dichloropropane ug/L 49.050 98 60-140
1,3,5-Trimethylbenzene ug/L 52.650 105 60-140
1,3-Dichlorobenzene ug/L 53.150 106 60-140
1,3-Dichloropropane ug/L 51.150 102 60-140
1,4-Dichlorobenzene ug/L 51.450 103 60-140
2,2-Dichloropropane ug/L 45.350 91 60-140
2-Chlorotoluene ug/L 52.350 105 60-140
4-Chlorotoluene ug/L 50.650 101 60-140
Benzene ug/L 51.450 103 60-140
Bromobenzene ug/L 52.050 104 60-140
Bromochloromethane ug/L 48.750 97 60-140
Bromodichloromethane ug/L 54.950 110 60-140
Bromoform ug/L 48.450 97 60-140
Bromomethane ug/L 31.250 62 60-140
Carbon tetrachloride ug/L 55.150 110 60-140
Chlorobenzene ug/L 52.750 105 60-140
Chloroethane ug/L 38.350 77 60-140
Chloroform ug/L 53.050 106 60-140
Chloromethane ug/L 43.250 86 60-140
cis-1,2-Dichloroethene ug/L 52.450 105 60-140
cis-1,3-Dichloropropene ug/L 54.050 108 60-140
Dibromochloromethane ug/L 49.650 99 60-140
Dibromomethane ug/L 53.650 107 60-140
Dichlorodifluoromethane ug/L 48.750 97 60-140
Diisopropyl ether ug/L 47.850 96 60-140
Ethanol ug/L 23002000 115 60-140
Ethyl-tert-butyl ether ug/L 90.8100 91 60-140
Ethylbenzene ug/L 50.650 101 60-140
Hexachloro-1,3-butadiene ug/L 52.950 106 60-140
Isopropylbenzene (Cumene)ug/L 55.250 110 60-140
m&p-Xylene ug/L 104100 104 60-140
Methyl-tert-butyl ether ug/L 52.250 104 60-140
Methylene Chloride ug/L 49.450 99 60-140
n-Butylbenzene ug/L 52.550 105 60-140
n-Propylbenzene ug/L 52.150 104 60-140
Naphthalene ug/L 53.750 107 60-140
o-Xylene ug/L 53.750 107 60-140
sec-Butylbenzene ug/L 53.050 106 60-140
Styrene ug/L 56.250 112 60-140
tert-Amyl Alcohol ug/L 12101000 121 60-140
tert-Amylmethyl ether ug/L 114100 114 60-140
tert-Butyl Alcohol ug/L 622500 124 60-140
tert-Butyl Formate ug/L 434400 109 60-140
tert-Butylbenzene ug/L 54.150 108 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1219848LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/L 51.650 103 60-140
Toluene ug/L 48.550 97 60-140
trans-1,2-Dichloroethene ug/L 49.750 99 60-140
trans-1,3-Dichloropropene ug/L 45.250 90 60-140
Trichloroethene ug/L 48.750 97 60-140
Trichlorofluoromethane ug/L 44.750 89 60-140
Vinyl chloride ug/L 48.450 97 60-140
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%105 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1219849MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92204979001
1219850
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 118 60-140114 320ND23.6 22.8
1,1,1-Trichloroethane ug/L 20 110 60-140107 320ND22.1 21.4
1,1,2,2-Tetrachloroethane ug/L 20 106 60-140102 420ND21.3 20.4
1,1,2-Trichloroethane ug/L 20 109 60-140107 220ND21.9 21.4
1,1-Dichloroethane ug/L 20 102 60-14098 320ND20.3 19.6
1,1-Dichloroethene ug/L 20 118 60-140115 320ND23.6 23.0
1,1-Dichloropropene ug/L 20 111 60-140107 420ND22.2 21.5
1,2,3-Trichlorobenzene ug/L 20 111 60-140109 220ND22.4 21.9
1,2,3-Trichloropropane ug/L 20 112 60-140108 420ND22.3 21.5
1,2,4-Trichlorobenzene ug/L 20 108 60-140106 220ND21.8 21.4
1,2,4-Trimethylbenzene ug/L 20 116 60-140113 220ND23.1 22.6
1,2-Dibromo-3-chloropropane ug/L 20 107 60-140105 120ND21.3 21.1
1,2-Dibromoethane (EDB)ug/L 20 113 60-140110 320ND22.6 22.0
1,2-Dichlorobenzene ug/L 20 117 60-140114 220ND23.4 22.9
1,2-Dichloroethane ug/L 20 103 60-14099 420ND20.5 19.8
1,2-Dichloropropane ug/L 20 105 60-140103 220ND21.0 20.7
1,3,5-Trimethylbenzene ug/L 20 114 60-140112 220ND22.8 22.4
1,3-Dichlorobenzene ug/L 20 114 60-140112 120ND22.7 22.4
1,3-Dichloropropane ug/L 20 109 60-140105 420ND21.9 20.9
1,4-Dichlorobenzene ug/L 20 113 60-140111 120ND22.5 22.2
2,2-Dichloropropane ug/L 20 84 60-14085 120ND16.8 17.0
2-Chlorotoluene ug/L 20 115 60-140111 320ND23.0 22.3
4-Chlorotoluene ug/L 20 109 60-140107 220ND21.8 21.3
Benzene ug/L 20 114 60-140111 320ND22.8 22.2
Bromobenzene ug/L 20 109 60-140108 120ND21.8 21.5
Bromochloromethane ug/L 20 114 60-140114 020ND22.8 22.8
Bromodichloromethane ug/L 20 113 60-140111 220ND22.7 22.2
Bromoform ug/L 20 97 60-14096 120ND19.4 19.2
Bromomethane ug/L 20 70 60-14073 520ND14.0 14.7
Carbon tetrachloride ug/L 20 119 60-140120 120ND23.9 24.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1219849MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92204979001
1219850
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chlorobenzene ug/L 20 116 60-140113 220ND23.1 22.6
Chloroethane ug/L 20 101 60-14099 320ND20.3 19.7
Chloroform ug/L 20 116 60-140111 420ND23.1 22.1
Chloromethane ug/L 20 100 60-14099 120ND20.1 19.8
cis-1,2-Dichloroethene ug/L 20 113 60-140110 320ND22.6 21.9
cis-1,3-Dichloropropene ug/L 20 102 60-140101 120ND20.3 20.1
Dibromochloromethane ug/L 20 104 60-140102 220ND20.8 20.3
Dibromomethane ug/L 20 113 60-140112 120ND22.6 22.3
Dichlorodifluoromethane ug/L 20 118 60-140114 320ND23.6 22.9
Diisopropyl ether ug/L 20 104 60-140100 320ND20.7 20.0
Ethanol ug/L 800 113 60-140114 1800ND905913
Ethyl-tert-butyl ether ug/L 40 94 60-14092 340ND37.7 36.6
Ethylbenzene ug/L 20 113 60-140109 420ND22.7 21.8
Hexachloro-1,3-butadiene ug/L 20 112 60-140111 120ND22.4 22.2
Isopropylbenzene (Cumene)ug/L 20 120 60-140118 120ND23.9 23.6
m&p-Xylene ug/L 40 115 60-140112 240ND45.9 44.8
Methyl-tert-butyl ether ug/L 20 110 60-140106 320ND21.9 21.2
Methylene Chloride ug/L 20 102 60-14098 320ND20.4 19.7
n-Butylbenzene ug/L 20 110 60-140111 020ND22.1 22.1
n-Propylbenzene ug/L 20 114 60-140112 120ND22.8 22.5
Naphthalene ug/L 20 111 60-140108 320ND22.4 21.7
o-Xylene ug/L 20 115 60-140110 420ND22.9 22.0
sec-Butylbenzene ug/L 20 114 60-140114 020ND22.7 22.7
Styrene ug/L 20 120 60-140115 420ND24.0 23.1
tert-Amyl Alcohol ug/L 400 101 60-140101 0400ND403403
tert-Amylmethyl ether ug/L 40 112 60-140110 340ND44.9 43.8
tert-Butyl Alcohol ug/L M020016460-140164 0200ND329328
tert-Butyl Formate ug/L P51601660-14016 0160ND26.3 26.2
tert-Butylbenzene ug/L 20 117 60-140116 120ND23.4 23.1
Tetrachloroethene ug/L 20 115 60-140112 320ND23.0 22.4
Toluene ug/L 20 107 60-140104 220ND21.4 20.8
trans-1,2-Dichloroethene ug/L 20 117 60-140116 120ND23.5 23.2
trans-1,3-Dichloropropene ug/L 20 91 60-14090 120ND18.2 18.0
Trichloroethene ug/L 20 109 60-140108 120ND21.8 21.5
Trichlorofluoromethane ug/L 20 116 60-140114 120ND23.1 22.8
Vinyl chloride ug/L 20 110 60-140107 320ND22.1 21.4
1,2-Dichloroethane-d4 (S)%96 70-13095
4-Bromofluorobenzene (S)%103 70-130102
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/27235
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92204984004, 92204984007, 92204984008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1222324
Associated Lab Samples:92204984004, 92204984007, 92204984008
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 06/17/14 01:33
1,1,1-Trichloroethane ug/L ND 0.50 06/17/14 01:33
1,1,2,2-Tetrachloroethane ug/L ND 0.50 06/17/14 01:33
1,1,2-Trichloroethane ug/L ND 0.50 06/17/14 01:33
1,1-Dichloroethane ug/L ND 0.50 06/17/14 01:33
1,1-Dichloroethene ug/L ND 0.50 06/17/14 01:33
1,1-Dichloropropene ug/L ND 0.50 06/17/14 01:33
1,2,3-Trichlorobenzene ug/L ND 2.0 06/17/14 01:33
1,2,3-Trichloropropane ug/L ND 0.50 06/17/14 01:33
1,2,4-Trichlorobenzene ug/L ND 2.0 06/17/14 01:33
1,2,4-Trimethylbenzene ug/L ND 0.50 06/17/14 01:33
1,2-Dibromo-3-chloropropane ug/L ND 1.0 06/17/14 01:33
1,2-Dibromoethane (EDB)ug/L ND 0.50 06/17/14 01:33
1,2-Dichlorobenzene ug/L ND 0.50 06/17/14 01:33
1,2-Dichloroethane ug/L ND 0.50 06/17/14 01:33
1,2-Dichloropropane ug/L ND 0.50 06/17/14 01:33
1,3,5-Trimethylbenzene ug/L ND 0.50 06/17/14 01:33
1,3-Dichlorobenzene ug/L ND 0.50 06/17/14 01:33
1,3-Dichloropropane ug/L ND 0.50 06/17/14 01:33
1,4-Dichlorobenzene ug/L ND 0.50 06/17/14 01:33
2,2-Dichloropropane ug/L ND 0.50 06/17/14 01:33
2-Chlorotoluene ug/L ND 0.50 06/17/14 01:33
4-Chlorotoluene ug/L ND 0.50 06/17/14 01:33
Benzene ug/L ND 0.50 06/17/14 01:33
Bromobenzene ug/L ND 0.50 06/17/14 01:33
Bromochloromethane ug/L ND 0.50 06/17/14 01:33
Bromodichloromethane ug/L ND 0.50 06/17/14 01:33
Bromoform ug/L ND 0.50 06/17/14 01:33
Bromomethane ug/L ND 5.0 06/17/14 01:33
Carbon tetrachloride ug/L ND 0.50 06/17/14 01:33
Chlorobenzene ug/L ND 0.50 06/17/14 01:33
Chloroethane ug/L ND 1.0 06/17/14 01:33
Chloroform ug/L ND 0.50 06/17/14 01:33
Chloromethane ug/L ND 1.0 06/17/14 01:33
cis-1,2-Dichloroethene ug/L ND 0.50 06/17/14 01:33
cis-1,3-Dichloropropene ug/L ND 0.50 06/17/14 01:33
Dibromochloromethane ug/L ND 0.50 06/17/14 01:33
Dibromomethane ug/L ND 0.50 06/17/14 01:33
Dichlorodifluoromethane ug/L ND 0.50 06/17/14 01:33
Diisopropyl ether ug/L ND 0.50 06/17/14 01:33
Ethanol ug/L ND 200 06/17/14 01:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1222324
Associated Lab Samples:92204984004, 92204984007, 92204984008
Matrix:Water
Analyzed
Ethyl-tert-butyl ether ug/L ND 10.0 06/17/14 01:33
Ethylbenzene ug/L ND 0.50 06/17/14 01:33
Hexachloro-1,3-butadiene ug/L ND 2.0 06/17/14 01:33
Isopropylbenzene (Cumene)ug/L ND 0.50 06/17/14 01:33
m&p-Xylene ug/L ND 1.0 06/17/14 01:33
Methyl-tert-butyl ether ug/L ND 0.50 06/17/14 01:33
Methylene Chloride ug/L ND 2.0 06/17/14 01:33
n-Butylbenzene ug/L ND 0.50 06/17/14 01:33
n-Propylbenzene ug/L ND 0.50 06/17/14 01:33
Naphthalene ug/L ND 2.0 06/17/14 01:33
o-Xylene ug/L ND 0.50 06/17/14 01:33
sec-Butylbenzene ug/L ND 0.50 06/17/14 01:33
Styrene ug/L ND 0.50 06/17/14 01:33
tert-Amyl Alcohol ug/L ND 100 06/17/14 01:33
tert-Amylmethyl ether ug/L ND 10.0 06/17/14 01:33
tert-Butyl Alcohol ug/L ND 10.0 06/17/14 01:33
tert-Butyl Formate ug/L ND 20.0 06/17/14 01:33
tert-Butylbenzene ug/L ND 0.50 06/17/14 01:33
Tetrachloroethene ug/L ND 0.50 06/17/14 01:33
Toluene ug/L ND 0.50 06/17/14 01:33
trans-1,2-Dichloroethene ug/L ND 0.50 06/17/14 01:33
trans-1,3-Dichloropropene ug/L ND 0.50 06/17/14 01:33
Trichloroethene ug/L ND 0.50 06/17/14 01:33
Trichlorofluoromethane ug/L ND 1.0 06/17/14 01:33
Vinyl chloride ug/L ND 1.0 06/17/14 01:33
1,2-Dichloroethane-d4 (S)%98 70-130 06/17/14 01:33
4-Bromofluorobenzene (S)%100 70-130 06/17/14 01:33
Toluene-d8 (S)%100 70-130 06/17/14 01:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1222325LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.150 102 60-140
1,1,1-Trichloroethane ug/L 49.150 98 60-140
1,1,2,2-Tetrachloroethane ug/L 48.850 98 60-140
1,1,2-Trichloroethane ug/L 49.250 98 60-140
1,1-Dichloroethane ug/L 46.550 93 60-140
1,1-Dichloroethene ug/L 49.750 99 60-140
1,1-Dichloropropene ug/L 49.450 99 60-140
1,2,3-Trichlorobenzene ug/L 50.150 100 60-140
1,2,3-Trichloropropane ug/L 50.250 100 60-140
1,2,4-Trichlorobenzene ug/L 50.150 100 60-140
1,2,4-Trimethylbenzene ug/L 50.850 102 60-140
1,2-Dibromo-3-chloropropane ug/L 51.750 103 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1222325LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromoethane (EDB)ug/L 51.050 102 60-140
1,2-Dichlorobenzene ug/L 50.750 101 60-140
1,2-Dichloroethane ug/L 48.450 97 60-140
1,2-Dichloropropane ug/L 48.450 97 60-140
1,3,5-Trimethylbenzene ug/L 50.350 101 60-140
1,3-Dichlorobenzene ug/L 48.850 98 60-140
1,3-Dichloropropane ug/L 49.250 98 60-140
1,4-Dichlorobenzene ug/L 48.950 98 60-140
2,2-Dichloropropane ug/L 47.150 94 60-140
2-Chlorotoluene ug/L 50.150 100 60-140
4-Chlorotoluene ug/L 48.350 97 60-140
Benzene ug/L 50.150 100 60-140
Bromobenzene ug/L 49.350 99 60-140
Bromochloromethane ug/L 48.650 97 60-140
Bromodichloromethane ug/L 51.450 103 60-140
Bromoform ug/L 55.350 111 60-140
Bromomethane ug/L 50.550 101 60-140
Carbon tetrachloride ug/L 49.950 100 60-140
Chlorobenzene ug/L 48.250 96 60-140
Chloroethane ug/L 44.550 89 60-140
Chloroform ug/L 49.350 99 60-140
Chloromethane ug/L 47.250 94 60-140
cis-1,2-Dichloroethene ug/L 49.550 99 60-140
cis-1,3-Dichloropropene ug/L 52.450 105 60-140
Dibromochloromethane ug/L 51.150 102 60-140
Dibromomethane ug/L 50.650 101 60-140
Dichlorodifluoromethane ug/L 49.350 99 60-140
Diisopropyl ether ug/L 47.650 95 60-140
Ethanol ug/L 16702000 83 60-140
Ethyl-tert-butyl ether ug/L 88.9100 89 60-140
Ethylbenzene ug/L 47.850 96 60-140
Hexachloro-1,3-butadiene ug/L 50.250 100 60-140
Isopropylbenzene (Cumene)ug/L 51.050 102 60-140
m&p-Xylene ug/L 97.0100 97 60-140
Methyl-tert-butyl ether ug/L 51.350 103 60-140
Methylene Chloride ug/L 47.450 95 60-140
n-Butylbenzene ug/L 50.050 100 60-140
n-Propylbenzene ug/L 49.350 99 60-140
Naphthalene ug/L 49.850 100 60-140
o-Xylene ug/L 49.450 99 60-140
sec-Butylbenzene ug/L 49.550 99 60-140
Styrene ug/L 52.250 104 60-140
tert-Amyl Alcohol ug/L 10401000 104 60-140
tert-Amylmethyl ether ug/L 109100 109 60-140
tert-Butyl Alcohol ug/L 553500 111 60-140
tert-Butyl Formate ug/L 378400 94 60-140
tert-Butylbenzene ug/L 50.350 101 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1222325LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/L 49.250 98 60-140
Toluene ug/L 48.050 96 60-140
trans-1,2-Dichloroethene ug/L 50.450 101 60-140
trans-1,3-Dichloropropene ug/L 53.250 106 60-140
Trichloroethene ug/L 48.450 97 60-140
Trichlorofluoromethane ug/L 47.450 95 60-140
Vinyl chloride ug/L 56.850 114 60-140
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1222718MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92205134001
1222719
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 71 60-14079 1020ND14.2 15.8
1,1,1-Trichloroethane ug/L 20 73 60-14080 920ND14.6 16.0
1,1,2,2-Tetrachloroethane ug/L 20 72 60-14079 920ND14.5 15.8
1,1,2-Trichloroethane ug/L 20 76 60-14081 720ND15.2 16.3
1,1-Dichloroethane ug/L 20 71 60-14078 920ND14.2 15.6
1,1-Dichloroethene ug/L 20 80 60-14087 820ND16.1 17.5
1,1-Dichloropropene ug/L 20 78 60-14085 920ND15.5 17.0
1,2,3-Trichlorobenzene ug/L 20 72 60-14081 1220ND14.4 16.3
1,2,3-Trichloropropane ug/L 20 73 60-14080 920ND14.6 16.0
1,2,4-Trichlorobenzene ug/L 20 73 60-14082 1220ND14.6 16.4
1,2,4-Trimethylbenzene ug/L 20 81 60-14088 920ND16.2 17.6
1,2-Dibromo-3-chloropropane ug/L 20 66 60-14075 1320ND13.2 15.0
1,2-Dibromoethane (EDB)ug/L 20 74 60-14081 920ND14.8 16.2
1,2-Dichlorobenzene ug/L 20 76 60-14083 920ND15.2 16.6
1,2-Dichloroethane ug/L 20 70 60-14077 920ND14.1 15.4
1,2-Dichloropropane ug/L 20 76 60-14082 720ND15.2 16.3
1,3,5-Trimethylbenzene ug/L 20 79 60-14085 820ND15.8 17.1
1,3-Dichlorobenzene ug/L 20 74 60-14082 1020ND14.7 16.3
1,3-Dichloropropane ug/L 20 75 60-14081 820ND15.0 16.2
1,4-Dichlorobenzene ug/L 20 74 60-14082 920ND14.9 16.3
2,2-Dichloropropane ug/L 20 76 60-14085 1120ND15.1 16.9
2-Chlorotoluene ug/L 20 75 60-14083 920ND15.1 16.5
4-Chlorotoluene ug/L 20 74 60-14081 1020ND14.7 16.2
Benzene ug/L 20 81 60-14088 820ND16.2 17.5
Bromobenzene ug/L 20 75 60-14076 120ND15.0 15.2
Bromochloromethane ug/L 20 78 60-14084 820ND15.6 16.9
Bromodichloromethane ug/L 20 73 60-14081 1020ND14.7 16.2
Bromoform ug/L 20 67 60-14074 1120ND13.3 14.9
Bromomethane ug/L 20 63 60-14077 2020ND12.7 15.5
Carbon tetrachloride ug/L 20 73 60-14083 1220ND14.6 16.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1222718MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92205134001
1222719
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chlorobenzene ug/L 20 75 60-14081 720ND15.0 16.1
Chloroethane ug/L 20 82 60-14092 1120ND16.5 18.3
Chloroform ug/L 20 75 60-14082 820ND15.1 16.4
Chloromethane ug/L 20 72 60-14078 820ND14.6 15.9
cis-1,2-Dichloroethene ug/L 20 75 60-14081 820ND15.0 16.2
cis-1,3-Dichloropropene ug/L 20 75 60-14082 820ND15.1 16.3
Dibromochloromethane ug/L 20 66 60-14074 1120ND13.3 14.8
Dibromomethane ug/L 20 76 60-14080 620ND15.1 16.1
Dichlorodifluoromethane ug/L 20 79 60-14085 720ND15.9 17.1
Diisopropyl ether ug/L 20 70 60-14075 720ND14.0 15.0
Ethanol ug/L M08005960-14065 11800ND471523
Ethyl-tert-butyl ether ug/L 40 64 60-14070 840ND25.7 27.9
Ethylbenzene ug/L 20 76 60-14082 820ND15.2 16.5
Hexachloro-1,3-butadiene ug/L 20 80 60-14087 920ND15.9 17.4
Isopropylbenzene (Cumene)ug/L 20 81 60-14088 920ND16.1 17.7
m&p-Xylene ug/L 40 78 60-14085 840ND31.4 34.1
Methyl-tert-butyl ether ug/L 20 73 60-14079 820ND14.6 15.9
Methylene Chloride ug/L 20 61 60-14069 1220ND12.3 13.8
n-Butylbenzene ug/L 20 79 60-14086 920ND15.7 17.3
n-Propylbenzene ug/L 20 79 60-14087 1020ND15.7 17.4
Naphthalene ug/L 20 73 60-14082 1120ND14.8 16.5
o-Xylene ug/L 20 77 60-14084 920ND15.4 16.8
sec-Butylbenzene ug/L 20 78 60-14085 1020ND15.5 17.1
Styrene ug/L 20 80 60-14087 820ND16.0 17.4
tert-Amyl Alcohol ug/L 400 65 60-14074 13400ND260296
tert-Amylmethyl ether ug/L 40 81 60-14087 740ND32.3 34.8
tert-Butyl Alcohol ug/L 200 85 60-140100 17200ND169201
tert-Butyl Formate ug/L P51604660-14044 5160ND73.5 69.9
tert-Butylbenzene ug/L 20 77 60-14086 1120ND15.4 17.2
Tetrachloroethene ug/L 20 77 60-14086 1120ND15.5 17.2
Toluene ug/L M0205860-14065 1020ND11.7 12.9
trans-1,2-Dichloroethene ug/L 20 78 60-14080 320ND15.6 16.0
trans-1,3-Dichloropropene ug/L 20 74 60-14081 1020ND14.7 16.2
Trichloroethene ug/L 20 77 60-14084 920ND15.4 16.8
Trichlorofluoromethane ug/L 20 80 60-14089 1020ND16.1 17.8
Vinyl chloride ug/L 20 86 60-14095 1020ND17.3 19.0
1,2-Dichloroethane-d4 (S)%95 70-13095
4-Bromofluorobenzene (S)%100 70-130101
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/28263
EPA 625
EPA 625
625 MSS
Associated Lab Samples:92204984001, 92204984002, 92204984003, 92204984004, 92204984005, 92204984006, 92204984007,
92204984008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1221118
Associated Lab Samples:92204984001, 92204984002, 92204984003, 92204984004, 92204984005, 92204984006, 92204984007,
92204984008
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 06/16/14 14:15
2,4,6-Trichlorophenol ug/L ND 10.0 06/16/14 14:15
2,4-Dichlorophenol ug/L ND 5.0 06/16/14 14:15
2,4-Dimethylphenol ug/L ND 10.0 06/16/14 14:15
2,4-Dinitrophenol ug/L ND 50.0 06/16/14 14:15
2,4-Dinitrotoluene ug/L ND 5.0 06/16/14 14:15
2,6-Dinitrotoluene ug/L ND 5.0 06/16/14 14:15
2-Chloronaphthalene ug/L ND 5.0 06/16/14 14:15
2-Chlorophenol ug/L ND 5.0 06/16/14 14:15
2-Nitrophenol ug/L ND 5.0 06/16/14 14:15
3,3'-Dichlorobenzidine ug/L ND 25.0 06/16/14 14:15
4,6-Dinitro-2-methylphenol ug/L ND 20.0 06/16/14 14:15
4-Bromophenylphenyl ether ug/L ND 5.0 06/16/14 14:15
4-Chloro-3-methylphenol ug/L ND 5.0 06/16/14 14:15
4-Chlorophenylphenyl ether ug/L ND 5.0 06/16/14 14:15
4-Nitrophenol ug/L ND 50.0 06/16/14 14:15
Acenaphthene ug/L ND 5.0 06/16/14 14:15
Acenaphthylene ug/L ND 5.0 06/16/14 14:15
Anthracene ug/L ND 5.0 06/16/14 14:15
Benzo(a)anthracene ug/L ND 5.0 06/16/14 14:15
Benzo(a)pyrene ug/L ND 5.0 06/16/14 14:15
Benzo(b)fluoranthene ug/L ND 5.0 06/16/14 14:15
Benzo(g,h,i)perylene ug/L ND 5.0 06/16/14 14:15
Benzo(k)fluoranthene ug/L ND 5.0 06/16/14 14:15
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/16/14 14:15
bis(2-Chloroethyl) ether ug/L ND 5.0 06/16/14 14:15
bis(2-Chloroisopropyl) ether ug/L ND 5.0 06/16/14 14:15
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 06/16/14 14:15
Butylbenzylphthalate ug/L ND 5.0 06/16/14 14:15
Chrysene ug/L ND 5.0 06/16/14 14:15
Di-n-butylphthalate ug/L ND 5.0 06/16/14 14:15
Di-n-octylphthalate ug/L ND 5.0 06/16/14 14:15
Dibenz(a,h)anthracene ug/L ND 5.0 06/16/14 14:15
Diethylphthalate ug/L ND 5.0 06/16/14 14:15
Dimethylphthalate ug/L ND 5.0 06/16/14 14:15
Fluoranthene ug/L ND 5.0 06/16/14 14:15
Fluorene ug/L ND 5.0 06/16/14 14:15
Hexachloro-1,3-butadiene ug/L ND 5.0 06/16/14 14:15
Hexachlorobenzene ug/L ND 5.0 06/16/14 14:15
Hexachlorocyclopentadiene ug/L ND 10.0 06/16/14 14:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1221118
Associated Lab Samples:92204984001, 92204984002, 92204984003, 92204984004, 92204984005, 92204984006, 92204984007,
92204984008
Matrix:Water
Analyzed
Hexachloroethane ug/L ND 5.0 06/16/14 14:15
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 06/16/14 14:15
Isophorone ug/L ND 10.0 06/16/14 14:15
N-Nitroso-di-n-propylamine ug/L ND 5.0 06/16/14 14:15
N-Nitrosodimethylamine ug/L ND 5.0 06/16/14 14:15
N-Nitrosodiphenylamine ug/L ND 10.0 06/16/14 14:15
Naphthalene ug/L ND 5.0 06/16/14 14:15
Nitrobenzene ug/L ND 5.0 06/16/14 14:15
Pentachlorophenol ug/L ND 10.0 06/16/14 14:15
Phenanthrene ug/L ND 5.0 06/16/14 14:15
Phenol ug/L ND 5.0 06/16/14 14:15
Pyrene ug/L ND 5.0 06/16/14 14:15
2,4,6-Tribromophenol (S)%75 10-137 06/16/14 14:15
2-Fluorobiphenyl (S)%74 15-120 06/16/14 14:15
2-Fluorophenol (S)%41 10-120 06/16/14 14:15
Nitrobenzene-d5 (S)%74 10-120 06/16/14 14:15
Phenol-d6 (S)%27 10-120 06/16/14 14:15
Terphenyl-d14 (S)%91 11-131 06/16/14 14:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1221119LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 33.350 67 44-142
2,4,6-Trichlorophenol ug/L 35.650 71 37-144
2,4-Dichlorophenol ug/L 35.850 72 1-191
2,4-Dimethylphenol ug/L 32.850 66 32-119
2,4-Dinitrophenol ug/L 155250 62 1-181
2,4-Dinitrotoluene ug/L 44.750 89 39-139
2,6-Dinitrotoluene ug/L 44.450 89 50-158
2-Chloronaphthalene ug/L 36.950 74 60-118
2-Chlorophenol ug/L 31.550 63 23-134
2-Nitrophenol ug/L 35.650 71 29-182
3,3'-Dichlorobenzidine ug/L 78.2100 78 1-262
4,6-Dinitro-2-methylphenol ug/L 77.7100 78 1-181
4-Bromophenylphenyl ether ug/L 41.250 82 53-127
4-Chloro-3-methylphenol ug/L 67.0100 67 22-147
4-Chlorophenylphenyl ether ug/L 37.850 76 25-158
4-Nitrophenol ug/L 83.8250 34 1-132
Acenaphthene ug/L 36.350 73 47-145
Acenaphthylene ug/L 36.450 73 33-145
Anthracene ug/L 39.750 79 1-166
Benzo(a)anthracene ug/L 41.150 82 33-143
Benzo(a)pyrene ug/L 42.050 84 17-163
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1221119LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(b)fluoranthene ug/L 40.850 82 24-159
Benzo(g,h,i)perylene ug/L 38.150 76 1-219
Benzo(k)fluoranthene ug/L 42.650 85 11-162
bis(2-Chloroethoxy)methane ug/L 35.550 71 33-184
bis(2-Chloroethyl) ether ug/L 35.950 72 12-158
bis(2-Chloroisopropyl) ether ug/L 32.450 65 36-166
bis(2-Ethylhexyl)phthalate ug/L 47.850 96 8-158
Butylbenzylphthalate ug/L 47.550 95 1-152
Chrysene ug/L 41.750 83 17-168
Di-n-butylphthalate ug/L 41.150 82 1-118
Di-n-octylphthalate ug/L 43.950 88 4-146
Dibenz(a,h)anthracene ug/L 38.850 78 1-227
Diethylphthalate ug/L 37.450 75 1-114
Dimethylphthalate ug/L 37.250 74 1-112
Fluoranthene ug/L 37.150 74 26-137
Fluorene ug/L 37.050 74 59-121
Hexachloro-1,3-butadiene ug/L 32.450 65 24-116
Hexachlorobenzene ug/L 38.050 76 1-152
Hexachlorocyclopentadiene ug/L 36.550 73 25-150
Hexachloroethane ug/L 31.650 63 40-113
Indeno(1,2,3-cd)pyrene ug/L 30.750 61 1-171
Isophorone ug/L 39.050 78 21-196
N-Nitroso-di-n-propylamine ug/L 32.950 66 1-230
N-Nitrosodimethylamine ug/L 23.750 47 25-150
N-Nitrosodiphenylamine ug/L 41.750 83 25-150
Naphthalene ug/L 34.350 69 21-133
Nitrobenzene ug/L 43.350 87 35-180
Pentachlorophenol ug/L 67.1100 67 14-176
Phenanthrene ug/L 38.250 76 54-120
Phenol ug/L 16.150 32 5-112
Pyrene ug/L 46.450 93 52-115
2,4,6-Tribromophenol (S)%77 10-137
2-Fluorobiphenyl (S)%77 15-120
2-Fluorophenol (S)%42 10-120
Nitrobenzene-d5 (S)%70 10-120
Phenol-d6 (S)%28 10-120
Terphenyl-d14 (S)%91 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1221120MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92205225001
1221121
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L M01005444-14241 28100ND54.2 40.9
2,4,6-Trichlorophenol ug/L 100 62 37-14455 13100ND62.5 54.9
2,4-Dichlorophenol ug/L 100 60 1-19146 28100ND60.2 45.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1221120MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92205225001
1221121
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2,4-Dimethylphenol ug/L 100 55 32-11943 26100ND55.2 42.7
2,4-Dinitrophenol ug/L 500 52 1-18154 4500ND262271
2,4-Dinitrotoluene ug/L 100 81 39-13977 5100ND81.0 77.3
2,6-Dinitrotoluene ug/L 100 80 50-15875 5100ND79.6 75.4
2-Chloronaphthalene ug/L M01005860-11846 23100ND58.2 46.3
2-Chlorophenol ug/L 100 53 23-13442 23100ND53.4 42.4
2-Nitrophenol ug/L 100 57 29-18243 28100ND56.9 43.0
3,3'-Dichlorobenzidine ug/L 200 43 1-26251 17200ND85.9 102
4,6-Dinitro-2-methylphenol ug/L 200 66 1-18167 2200ND131134
4-Bromophenylphenyl ether ug/L 100 73 53-12769 6100ND73.2 69.0
4-Chloro-3-methylphenol ug/L 200 63 22-14756 12200ND126111
4-Chlorophenylphenyl ether ug/L 100 66 25-15859 12100ND65.9 58.7
4-Nitrophenol ug/L 500 40 1-13245 11500ND202226
Acenaphthene ug/L 100 59 47-14550 16100ND59.1 50.2
Acenaphthylene ug/L 100 59 33-14551 15100ND58.9 50.5
Anthracene ug/L 100 72 1-16670 3100ND71.9 69.6
Benzo(a)anthracene ug/L 100 73 33-14374 1100ND73.5 74.3
Benzo(a)pyrene ug/L 100 75 17-16375 0100ND75.2 75.0
Benzo(b)fluoranthene ug/L 100 78 24-15977 1100ND77.7 77.0
Benzo(g,h,i)perylene ug/L 100 67 1-21967 1100ND67.0 67.4
Benzo(k)fluoranthene ug/L 100 70 11-16271 1100ND70.1 70.7
bis(2-Chloroethoxy)methane ug/L R11005633-18441 32100ND56.3 40.7
bis(2-Chloroethyl) ether ug/L 100 56 12-15843 25100ND55.5 43.1
bis(2-Chloroisopropyl) ether ug/L 100 48 36-16638 25100ND48.5 37.8
bis(2-Ethylhexyl)phthalate ug/L 100 88 8-15885 4100ND87.8 84.7
Butylbenzylphthalate ug/L 100 87 1-15285 3100ND86.9 84.6
Chrysene ug/L 100 73 17-16875 3100ND73.2 75.4
Di-n-butylphthalate ug/L 100 75 1-11873 2100ND75.0 73.2
Di-n-octylphthalate ug/L 100 85 4-14685 0100ND84.7 85.1
Dibenz(a,h)anthracene ug/L 100 71 1-22773 3100ND71.0 73.3
Diethylphthalate ug/L 100 68 1-11465 5100ND68.4 65.0
Dimethylphthalate ug/L 100 67 1-11263 7100ND67.0 62.7
Fluoranthene ug/L 100 68 26-13767 1100ND67.7 66.9
Fluorene ug/L M01006459-12158 10100ND64.3 57.9
Hexachloro-1,3-butadiene ug/L 100 52 24-11639 27100ND52.1 39.5
Hexachlorobenzene ug/L 100 67 1-15264 6100ND67.3 63.7
Hexachlorocyclopentadiene ug/L 100 53 25-15040 27100ND53.1 40.3
Hexachloroethane ug/L M01005240-11339 27100ND51.6 39.2
Indeno(1,2,3-cd)pyrene ug/L 100 55 1-17156 2100ND54.7 55.6
Isophorone ug/L 100 60 21-19646 26100ND59.9 46.2
N-Nitroso-di-n-propylamine ug/L 100 50 1-23039 25100ND50.1 38.8
N-Nitrosodimethylamine ug/L 100 47 25-15038 21100ND47.0 38.2
N-Nitrosodiphenylamine ug/L 100 75 25-15072 4100ND75.3 72.2
Naphthalene ug/L 100 54 21-13341 27100ND54.0 41.3
Nitrobenzene ug/L 100 66 35-18050 28100ND65.8 49.7
Pentachlorophenol ug/L 200 66 14-17667 1200ND133134
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1221120MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92205225001
1221121
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenanthrene ug/L 100 69 54-12067 3100ND69.4 67.4
Phenol ug/L P6,R11001395-112-29 31100488627459
Pyrene ug/L 100 82 52-11580 3100ND82.4 79.9
2,4,6-Tribromophenol (S)%74 10-13771
2-Fluorobiphenyl (S)%59 15-12046
2-Fluorophenol (S)%41 10-12033
Nitrobenzene-d5 (S)%54 10-12041
Phenol-d6 (S)%30 10-12026
Terphenyl-d14 (S)%81 11-13178
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 67
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/28300
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Associated Lab Samples:92204984001, 92204984002, 92204984003, 92204984004, 92204984005, 92204984006, 92204984007,
92204984008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1222204
Associated Lab Samples:92204984001, 92204984002, 92204984003, 92204984004, 92204984005, 92204984006, 92204984007,
92204984008
Matrix:Water
Analyzed
Aliphatic (C09-C18)ug/L ND 100 N206/18/14 09:06
Aliphatic (C19-C36)ug/L ND 100 N206/18/14 09:06
Aromatic (C11-C22)ug/L ND 100 N206/18/14 09:06
2-Bromonaphthalene (S)%93 40-140 06/18/14 09:06
2-Fluorobiphenyl (S)%84 40-140 06/18/14 09:06
Nonatriacontane (S)%79 40-140 06/18/14 09:06
o-Terphenyl (S)%75 40-140 06/18/14 09:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1222205LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1222206
Aliphatic (C09-C18)ug/L 228 N23007640-14076229 1 50
Aliphatic (C19-C36)ug/L 384 N24009640-14092367 4 50
Aromatic (C11-C22)ug/L 646 N28507640-14076643 1 50
2-Bromonaphthalene (S)%76 40-14089
2-Fluorobiphenyl (S)%74 40-14081
Nonatriacontane (S)%82 40-14087
o-Terphenyl (S)%76 40-14080
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 67
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
LOD - Limit of Detection.
LOQ - Limit of Quantitation.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Tentatively identified compound (TIC) based on mass spectral library searchN
The lab does not hold TNI accreditation for this parameter.N2
The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.P5
Matrix spike recovery was outside laboratory control limits due to a parent sample concentration notably higher than the
spike level.P6
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 67
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92204984
SPATCO 6228-13-0135
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92204984001 OEXT/28300 GCSV/17947MW-1 MADEP EPH MADEP EPH
92204984002 OEXT/28300 GCSV/17947MW-3 MADEP EPH MADEP EPH
92204984003 OEXT/28300 GCSV/17947MW-5 MADEP EPH MADEP EPH
92204984004 OEXT/28300 GCSV/17947MW-6 MADEP EPH MADEP EPH
92204984005 OEXT/28300 GCSV/17947MW-10 MADEP EPH MADEP EPH
92204984006 OEXT/28300 GCSV/17947MW-13 MADEP EPH MADEP EPH
92204984007 OEXT/28300 GCSV/17947MW-14 MADEP EPH MADEP EPH
92204984008 OEXT/28300 GCSV/17947MW-15 MADEP EPH MADEP EPH
92204984001 GCV/8229MW-1 MADEP VPH
92204984002 GCV/8229MW-3 MADEP VPH
92204984003 GCV/8229MW-5 MADEP VPH
92204984004 GCV/8229MW-6 MADEP VPH
92204984005 GCV/8229MW-10 MADEP VPH
92204984006 GCV/8229MW-13 MADEP VPH
92204984007 GCV/8229MW-14 MADEP VPH
92204984008 GCV/8229MW-15 MADEP VPH
92204984007 MPRP/16198 ICP/14644MW-14 EPA 3010 EPA 6010
92204984008 MPRP/16198 ICP/14644MW-15 EPA 3010 EPA 6010
92204984009 MPRP/16198 ICP/14644MW-2 EPA 3010 EPA 6010
92204984010 MPRP/16198 ICP/14644MW-1 EPA 3010 EPA 6010
92204984011 MPRP/16198 ICP/14644MW-3 EPA 3010 EPA 6010
92204984012 MPRP/16198 ICP/14644MW-5 EPA 3010 EPA 6010
92204984013 MPRP/16200 ICP/14642MW-6 EPA 3010 EPA 6010
92204984014 MPRP/16200 ICP/14642MW-10 EPA 3010 EPA 6010
92204984015 MPRP/16200 ICP/14642MW-13 EPA 3010 EPA 6010
92204984001 OEXT/28263 MSSV/9247MW-1 EPA 625 EPA 625
92204984002 OEXT/28263 MSSV/9247MW-3 EPA 625 EPA 625
92204984003 OEXT/28263 MSSV/9247MW-5 EPA 625 EPA 625
92204984004 OEXT/28263 MSSV/9247MW-6 EPA 625 EPA 625
92204984005 OEXT/28263 MSSV/9247MW-10 EPA 625 EPA 625
92204984006 OEXT/28263 MSSV/9247MW-13 EPA 625 EPA 625
92204984007 OEXT/28263 MSSV/9247MW-14 EPA 625 EPA 625
92204984008 OEXT/28263 MSSV/9247MW-15 EPA 625 EPA 625
92204984001 MSV/27184MW-1 SM 6200B
92204984002 MSV/27184MW-3 SM 6200B
92204984003 MSV/27184MW-5 SM 6200B
92204984004 MSV/27235MW-6 SM 6200B
92204984005 MSV/27184MW-10 SM 6200B
92204984006 MSV/27184MW-13 SM 6200B
92204984007 MSV/27235MW-14 SM 6200B
92204984008 MSV/27235MW-15 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/19/2014 03:32 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
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Page 64 of 67
Page 65 of 67
Page 66 of 67
Page 67 of 67
#=CL#
June 25, 2014
LIMS USE: FR - ROB FOSTER
LIMS OBJECT ID: 92204797
92204797
Project:
Pace Project No.:
RE:
Mr. Rob Foster
AMEC-Charlotte
2801 Yorkmont Road Suite 100
Charlotte, NC 28208
SPATCO 6228-13-0135
Dear Mr. Foster:
Enclosed are the analytical results for sample(s) received by the laboratory on June 10, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 77
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 77
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92204797001 DMW-1 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 6010 2 PASI-AJMW
EPA 625 61 PASI-CBPJ
SM 6200B 69 PASI-CCAH
92204797002 DMW-2 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 6010 2 PASI-AJMW
EPA 625 60 PASI-CBPJ
SM 6200B 69 PASI-CCAH
92204797003 MW-2 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 625 66 PASI-CBPJ
SM 6200B 69 PASI-CCAH
92204797004 MW-4 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 625 61 PASI-CBPJ
SM 6200B 69 PASI-CCAH
92204797005 MW-7 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 625 59 PASI-CBPJ
SM 6200B 69 PASI-CCAH
92204797006 MW-8 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 625 59 PASI-CBPJ
SM 6200B 69 PASI-CCAH
92204797007 MW-9 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 625 61 PASI-CBPJ
SM 6200B 69 PASI-CCAH
92204797008 MW-11 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 625 62 PASI-CBPJ
SM 6200B 69 PASI-CCAH
92204797009 MW-16 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 625 59 PASI-CBPJ
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 77
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 6200B 69 PASI-CCAH
92204797010 MW-17 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 625 61 PASI-CBPJ
SM 6200B 69 PASI-CCAH
92204797011 MW-18 MADEP EPH 7 PASI-CJDW1
MADEP VPH 5 PASI-CGAW
EPA 625 59 PASI-CRES
SM 6200B 69 PASI-CCAH
92204797012 MW-4 EPA 6010 2 PASI-AJMW
92204797013 MW-7 EPA 6010 2 PASI-AJMW
92204797014 MW-8 EPA 6010 2 PASI-AJMW
92204797015 MW-9 EPA 6010 2 PASI-AJMW
92204797016 MW-11 EPA 6010 2 PASI-AJMW
92204797017 MW-16 EPA 6010 2 PASI-AJMW
92204797018 MW-17 EPA 6010 2 PASI-AJMW
92204797019 MW-18 EPA 6010 2 PASI-AJMW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:DMW-1 Lab ID:92204797001 Collected:06/10/14 11:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 06/18/14 10:43 N206/16/14 14:451001
Aliphatic (C19-C36)ND ug/L 06/18/14 10:43 N206/16/14 14:451001
Aromatic (C11-C22)ND ug/L 06/18/14 10:43 N206/16/14 14:451001
Surrogates
Nonatriacontane (S)44 %06/18/14 10:43 7194-86-706/16/14 14:4540-140 1
o-Terphenyl (S)52 %06/18/14 10:43 84-15-106/16/14 14:4540-140 1
2-Fluorobiphenyl (S)62 %06/18/14 10:43 321-60-806/16/14 14:4540-140 1
2-Bromonaphthalene (S)73 %06/18/14 10:43 580-13-206/16/14 14:4540-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)77.2 ug/L 06/18/14 18:03 N250.0 1
Aliphatic (C09-C12)ND ug/L 06/18/14 18:03 N250.0 1
Aromatic (C09-C10)ND ug/L 06/18/14 18:03 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)120 %06/18/14 18:03 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)106 %06/18/14 18:03 460-00-470-130 1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium 64.6 ug/L 06/12/14 19:51 7440-47-306/11/14 11:455.0 1
Lead ND ug/L 06/12/14 19:51 7439-92-106/11/14 11:455.0 1
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/12/14 21:37 83-32-906/11/14 16:015.0 1
Acenaphthylene ND ug/L 06/12/14 21:37 208-96-806/11/14 16:015.0 1
Anthracene ND ug/L 06/12/14 21:37 120-12-706/11/14 16:015.0 1
Benzo(a)anthracene ND ug/L 06/12/14 21:37 56-55-306/11/14 16:015.0 1
Benzo(a)pyrene ND ug/L 06/12/14 21:37 50-32-806/11/14 16:015.0 1
Benzo(b)fluoranthene ND ug/L 06/12/14 21:37 205-99-206/11/14 16:015.0 1
Benzo(g,h,i)perylene ND ug/L 06/12/14 21:37 191-24-206/11/14 16:015.0 1
Benzo(k)fluoranthene ND ug/L 06/12/14 21:37 207-08-906/11/14 16:015.0 1
4-Bromophenylphenyl ether ND ug/L 06/12/14 21:37 101-55-306/11/14 16:015.0 1
Butylbenzylphthalate ND ug/L 06/12/14 21:37 85-68-706/11/14 16:015.0 1
4-Chloro-3-methylphenol ND ug/L 06/12/14 21:37 59-50-706/11/14 16:015.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/12/14 21:37 111-91-106/11/14 16:0110.0 1
bis(2-Chloroethyl) ether ND ug/L 06/12/14 21:37 111-44-406/11/14 16:015.0 1
bis(2-Chloroisopropyl) ether ND ug/L 06/12/14 21:37 108-60-106/11/14 16:015.0 1
2-Chloronaphthalene ND ug/L 06/12/14 21:37 91-58-706/11/14 16:015.0 1
2-Chlorophenol ND ug/L 06/12/14 21:37 95-57-806/11/14 16:015.0 1
4-Chlorophenylphenyl ether ND ug/L 06/12/14 21:37 7005-72-306/11/14 16:015.0 1
Chrysene ND ug/L 06/12/14 21:37 218-01-906/11/14 16:015.0 1
Dibenz(a,h)anthracene ND ug/L 06/12/14 21:37 53-70-306/11/14 16:015.0 1
3,3'-Dichlorobenzidine ND ug/L 06/12/14 21:37 91-94-106/11/14 16:0125.0 1
2,4-Dichlorophenol ND ug/L 06/12/14 21:37 120-83-206/11/14 16:015.0 1
Diethylphthalate ND ug/L 06/12/14 21:37 84-66-206/11/14 16:015.0 1
2,4-Dimethylphenol ND ug/L 06/12/14 21:37 105-67-906/11/14 16:0110.0 1
Dimethylphthalate ND ug/L 06/12/14 21:37 131-11-306/11/14 16:015.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:DMW-1 Lab ID:92204797001 Collected:06/10/14 11:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-butylphthalate ND ug/L 06/12/14 21:37 84-74-206/11/14 16:015.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/12/14 21:37 534-52-106/11/14 16:0120.0 1
2,4-Dinitrophenol ND ug/L 06/12/14 21:37 51-28-506/11/14 16:0150.0 1
2,4-Dinitrotoluene ND ug/L 06/12/14 21:37 121-14-206/11/14 16:015.0 1
2,6-Dinitrotoluene ND ug/L 06/12/14 21:37 606-20-206/11/14 16:015.0 1
Di-n-octylphthalate ND ug/L 06/12/14 21:37 117-84-006/11/14 16:015.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/12/14 21:37 117-81-706/11/14 16:015.0 1
Fluoranthene ND ug/L 06/12/14 21:37 206-44-006/11/14 16:015.0 1
Fluorene ND ug/L 06/12/14 21:37 86-73-706/11/14 16:015.0 1
Hexachloro-1,3-butadiene ND ug/L 06/12/14 21:37 87-68-306/11/14 16:015.0 1
Hexachlorobenzene ND ug/L 06/12/14 21:37 118-74-106/11/14 16:015.0 1
Hexachlorocyclopentadiene ND ug/L 06/12/14 21:37 77-47-406/11/14 16:0110.0 1
Hexachloroethane ND ug/L 06/12/14 21:37 67-72-106/11/14 16:015.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/12/14 21:37 193-39-506/11/14 16:015.0 1
Isophorone ND ug/L 06/12/14 21:37 78-59-106/11/14 16:0110.0 1
Naphthalene ND ug/L 06/12/14 21:37 91-20-306/11/14 16:015.0 1
Nitrobenzene ND ug/L 06/12/14 21:37 98-95-306/11/14 16:015.0 1
2-Nitrophenol ND ug/L 06/12/14 21:37 88-75-506/11/14 16:015.0 1
4-Nitrophenol ND ug/L 06/12/14 21:37 100-02-706/11/14 16:0150.0 1
N-Nitrosodimethylamine ND ug/L 06/12/14 21:37 62-75-906/11/14 16:015.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/12/14 21:37 621-64-706/11/14 16:015.0 1
N-Nitrosodiphenylamine ND ug/L 06/12/14 21:37 86-30-606/11/14 16:0110.0 1
Pentachlorophenol ND ug/L 06/12/14 21:37 87-86-506/11/14 16:0110.0 1
Phenanthrene ND ug/L 06/12/14 21:37 85-01-806/11/14 16:015.0 1
Phenol ND ug/L 06/12/14 21:37 108-95-206/11/14 16:015.0 1
Pyrene ND ug/L 06/12/14 21:37 129-00-006/11/14 16:015.0 1
1,2,4-Trichlorobenzene ND ug/L 06/12/14 21:37 120-82-106/11/14 16:015.0 1
2,4,6-Trichlorophenol ND ug/L 06/12/14 21:37 88-06-206/11/14 16:0110.0 1
Surrogates
Nitrobenzene-d5 (S)57 %06/12/14 21:37 4165-60-006/11/14 16:0110-120 1
2-Fluorobiphenyl (S)59 %06/12/14 21:37 321-60-806/11/14 16:0115-120 1
Terphenyl-d14 (S)76 %06/12/14 21:37 1718-51-006/11/14 16:0111-131 1
Phenol-d6 (S)24 %06/12/14 21:37 13127-88-306/11/14 16:0110-120 1
2-Fluorophenol (S)35 %06/12/14 21:37 367-12-406/11/14 16:0110-120 1
2,4,6-Tribromophenol (S)82 %06/12/14 21:37 118-79-606/11/14 16:0110-137 1
Tentatively Identified Compounds
Tetrachloroethylene 9.8 ug/L 06/12/14 21:37 127-18-4 N06/11/14 16:011
Unknown 8.6 ug/L 06/12/14 21:37 N06/11/14 16:011
Unknown 174 ug/L 06/12/14 21:37 N06/11/14 16:011
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol ND ug/L 06/12/14 21:45 75-85-41001
tert-Amylmethyl ether ND ug/L 06/12/14 21:45 994-05-810.0 1
Benzene ND ug/L 06/12/14 21:45 71-43-20.50 1
Bromobenzene ND ug/L 06/12/14 21:45 108-86-10.50 1
Bromochloromethane ND ug/L 06/12/14 21:45 74-97-50.50 1
Bromodichloromethane ND ug/L 06/12/14 21:45 75-27-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:DMW-1 Lab ID:92204797001 Collected:06/10/14 11:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Bromoform ND ug/L 06/12/14 21:45 75-25-20.50 1
Bromomethane ND ug/L 06/12/14 21:45 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 06/12/14 21:45 75-65-010.0 1
n-Butylbenzene ND ug/L 06/12/14 21:45 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/12/14 21:45 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/12/14 21:45 98-06-60.50 1
tert-Butyl Formate ND ug/L 06/12/14 21:45 762-75-420.0 1
Carbon tetrachloride ND ug/L 06/12/14 21:45 56-23-50.50 1
Chlorobenzene ND ug/L 06/12/14 21:45 108-90-70.50 1
Chloroethane ND ug/L 06/12/14 21:45 75-00-31.0 1
Chloroform ND ug/L 06/12/14 21:45 67-66-30.50 1
Chloromethane ND ug/L 06/12/14 21:45 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/12/14 21:45 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/12/14 21:45 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/14 21:45 96-12-81.0 1
Dibromochloromethane ND ug/L 06/12/14 21:45 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/14 21:45 106-93-40.50 1
Dibromomethane ND ug/L 06/12/14 21:45 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/12/14 21:45 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/12/14 21:45 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/12/14 21:45 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/12/14 21:45 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/12/14 21:45 75-34-30.50 1
1,2-Dichloroethane 3.0 ug/L 06/12/14 21:45 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/12/14 21:45 75-35-40.50 1
cis-1,2-Dichloroethene 49.2 ug/L 06/12/14 21:45 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/12/14 21:45 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/12/14 21:45 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/12/14 21:45 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/12/14 21:45 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/12/14 21:45 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/12/14 21:45 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/12/14 21:45 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/12/14 21:45 108-20-30.50 1
Ethanol ND ug/L 06/12/14 21:45 64-17-52001
Ethylbenzene ND ug/L 06/12/14 21:45 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 06/12/14 21:45 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 06/12/14 21:45 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/12/14 21:45 98-82-80.50 1
Methylene Chloride ND ug/L 06/12/14 21:45 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/12/14 21:45 1634-04-40.50 1
Naphthalene ND ug/L 06/12/14 21:45 91-20-32.0 1
n-Propylbenzene ND ug/L 06/12/14 21:45 103-65-10.50 1
Styrene ND ug/L 06/12/14 21:45 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/14 21:45 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/14 21:45 79-34-50.50 1
Tetrachloroethene 53.7 ug/L 06/12/14 21:45 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:DMW-1 Lab ID:92204797001 Collected:06/10/14 11:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 06/12/14 21:45 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/12/14 21:45 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/12/14 21:45 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/12/14 21:45 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/12/14 21:45 79-00-50.50 1
Trichloroethene 3.8 ug/L 06/12/14 21:45 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/12/14 21:45 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/12/14 21:45 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/12/14 21:45 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/12/14 21:45 108-67-80.50 1
Vinyl chloride ND ug/L 06/12/14 21:45 75-01-41.0 1
m&p-Xylene ND ug/L 06/12/14 21:45 179601-23-11.0 1
o-Xylene ND ug/L 06/12/14 21:45 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %06/12/14 21:45 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %06/12/14 21:45 460-00-470-130 1
Toluene-d8 (S)99 %06/12/14 21:45 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:DMW-2 Lab ID:92204797002 Collected:06/10/14 12:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 06/18/14 11:16 N206/16/14 14:451001
Aliphatic (C19-C36)ND ug/L 06/18/14 11:16 N206/16/14 14:451001
Aromatic (C11-C22)ND ug/L 06/18/14 11:16 N206/16/14 14:451001
Surrogates
Nonatriacontane (S)54 %06/18/14 11:16 7194-86-706/16/14 14:4540-140 1
o-Terphenyl (S)66 %06/18/14 11:16 84-15-106/16/14 14:4540-140 1
2-Fluorobiphenyl (S)74 %06/18/14 11:16 321-60-806/16/14 14:4540-140 1
2-Bromonaphthalene (S)85 %06/18/14 11:16 580-13-206/16/14 14:4540-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 06/18/14 18:26 N250.0 1
Aliphatic (C09-C12)ND ug/L 06/18/14 18:26 N250.0 1
Aromatic (C09-C10)ND ug/L 06/18/14 18:26 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)122 %06/18/14 18:26 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)108 %06/18/14 18:26 460-00-470-130 1
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium 5.7 ug/L 06/13/14 19:15 7440-47-306/12/14 15:105.0 1
Lead ND ug/L 06/13/14 19:15 7439-92-106/12/14 15:105.0 1
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/12/14 22:08 83-32-906/11/14 16:015.0 1
Acenaphthylene ND ug/L 06/12/14 22:08 208-96-806/11/14 16:015.0 1
Anthracene ND ug/L 06/12/14 22:08 120-12-706/11/14 16:015.0 1
Benzo(a)anthracene ND ug/L 06/12/14 22:08 56-55-306/11/14 16:015.0 1
Benzo(a)pyrene ND ug/L 06/12/14 22:08 50-32-806/11/14 16:015.0 1
Benzo(b)fluoranthene ND ug/L 06/12/14 22:08 205-99-206/11/14 16:015.0 1
Benzo(g,h,i)perylene ND ug/L 06/12/14 22:08 191-24-206/11/14 16:015.0 1
Benzo(k)fluoranthene ND ug/L 06/12/14 22:08 207-08-906/11/14 16:015.0 1
4-Bromophenylphenyl ether ND ug/L 06/12/14 22:08 101-55-306/11/14 16:015.0 1
Butylbenzylphthalate ND ug/L 06/12/14 22:08 85-68-706/11/14 16:015.0 1
4-Chloro-3-methylphenol ND ug/L 06/12/14 22:08 59-50-706/11/14 16:015.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/12/14 22:08 111-91-106/11/14 16:0110.0 1
bis(2-Chloroethyl) ether ND ug/L 06/12/14 22:08 111-44-406/11/14 16:015.0 1
bis(2-Chloroisopropyl) ether ND ug/L 06/12/14 22:08 108-60-106/11/14 16:015.0 1
2-Chloronaphthalene ND ug/L 06/12/14 22:08 91-58-706/11/14 16:015.0 1
2-Chlorophenol ND ug/L 06/12/14 22:08 95-57-806/11/14 16:015.0 1
4-Chlorophenylphenyl ether ND ug/L 06/12/14 22:08 7005-72-306/11/14 16:015.0 1
Chrysene ND ug/L 06/12/14 22:08 218-01-906/11/14 16:015.0 1
Dibenz(a,h)anthracene ND ug/L 06/12/14 22:08 53-70-306/11/14 16:015.0 1
3,3'-Dichlorobenzidine ND ug/L 06/12/14 22:08 91-94-106/11/14 16:0125.0 1
2,4-Dichlorophenol ND ug/L 06/12/14 22:08 120-83-206/11/14 16:015.0 1
Diethylphthalate ND ug/L 06/12/14 22:08 84-66-206/11/14 16:015.0 1
2,4-Dimethylphenol ND ug/L 06/12/14 22:08 105-67-906/11/14 16:0110.0 1
Dimethylphthalate ND ug/L 06/12/14 22:08 131-11-306/11/14 16:015.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:DMW-2 Lab ID:92204797002 Collected:06/10/14 12:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-butylphthalate ND ug/L 06/12/14 22:08 84-74-206/11/14 16:015.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/12/14 22:08 534-52-106/11/14 16:0120.0 1
2,4-Dinitrophenol ND ug/L 06/12/14 22:08 51-28-506/11/14 16:0150.0 1
2,4-Dinitrotoluene ND ug/L 06/12/14 22:08 121-14-206/11/14 16:015.0 1
2,6-Dinitrotoluene ND ug/L 06/12/14 22:08 606-20-206/11/14 16:015.0 1
Di-n-octylphthalate ND ug/L 06/12/14 22:08 117-84-006/11/14 16:015.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/12/14 22:08 117-81-706/11/14 16:015.0 1
Fluoranthene ND ug/L 06/12/14 22:08 206-44-006/11/14 16:015.0 1
Fluorene ND ug/L 06/12/14 22:08 86-73-706/11/14 16:015.0 1
Hexachloro-1,3-butadiene ND ug/L 06/12/14 22:08 87-68-306/11/14 16:015.0 1
Hexachlorobenzene ND ug/L 06/12/14 22:08 118-74-106/11/14 16:015.0 1
Hexachlorocyclopentadiene ND ug/L 06/12/14 22:08 77-47-406/11/14 16:0110.0 1
Hexachloroethane ND ug/L 06/12/14 22:08 67-72-106/11/14 16:015.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/12/14 22:08 193-39-506/11/14 16:015.0 1
Isophorone ND ug/L 06/12/14 22:08 78-59-106/11/14 16:0110.0 1
Naphthalene ND ug/L 06/12/14 22:08 91-20-306/11/14 16:015.0 1
Nitrobenzene ND ug/L 06/12/14 22:08 98-95-306/11/14 16:015.0 1
2-Nitrophenol ND ug/L 06/12/14 22:08 88-75-506/11/14 16:015.0 1
4-Nitrophenol ND ug/L 06/12/14 22:08 100-02-706/11/14 16:0150.0 1
N-Nitrosodimethylamine ND ug/L 06/12/14 22:08 62-75-906/11/14 16:015.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/12/14 22:08 621-64-706/11/14 16:015.0 1
N-Nitrosodiphenylamine ND ug/L 06/12/14 22:08 86-30-606/11/14 16:0110.0 1
Pentachlorophenol ND ug/L 06/12/14 22:08 87-86-506/11/14 16:0110.0 1
Phenanthrene ND ug/L 06/12/14 22:08 85-01-806/11/14 16:015.0 1
Phenol ND ug/L 06/12/14 22:08 108-95-206/11/14 16:015.0 1
Pyrene ND ug/L 06/12/14 22:08 129-00-006/11/14 16:015.0 1
1,2,4-Trichlorobenzene ND ug/L 06/12/14 22:08 120-82-106/11/14 16:015.0 1
2,4,6-Trichlorophenol ND ug/L 06/12/14 22:08 88-06-206/11/14 16:0110.0 1
Surrogates
Nitrobenzene-d5 (S)68 %06/12/14 22:08 4165-60-006/11/14 16:0110-120 1
2-Fluorobiphenyl (S)72 %06/12/14 22:08 321-60-806/11/14 16:0115-120 1
Terphenyl-d14 (S)83 %06/12/14 22:08 1718-51-006/11/14 16:0111-131 1
Phenol-d6 (S)28 %06/12/14 22:08 13127-88-306/11/14 16:0110-120 1
2-Fluorophenol (S)41 %06/12/14 22:08 367-12-406/11/14 16:0110-120 1
2,4,6-Tribromophenol (S)84 %06/12/14 22:08 118-79-606/11/14 16:0110-137 1
Tentatively Identified Compounds
Butanoic acid 10.5 ug/L 06/12/14 22:08 107-92-6 N06/11/14 16:011
Unknown 11.0 ug/L 06/12/14 22:08 N06/11/14 16:011
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol ND ug/L 06/12/14 22:02 75-85-41001
tert-Amylmethyl ether ND ug/L 06/12/14 22:02 994-05-810.0 1
Benzene ND ug/L 06/12/14 22:02 71-43-20.50 1
Bromobenzene ND ug/L 06/12/14 22:02 108-86-10.50 1
Bromochloromethane ND ug/L 06/12/14 22:02 74-97-50.50 1
Bromodichloromethane ND ug/L 06/12/14 22:02 75-27-40.50 1
Bromoform ND ug/L 06/12/14 22:02 75-25-20.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:DMW-2 Lab ID:92204797002 Collected:06/10/14 12:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Bromomethane ND ug/L 06/12/14 22:02 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 06/12/14 22:02 75-65-010.0 1
n-Butylbenzene ND ug/L 06/12/14 22:02 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/12/14 22:02 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/12/14 22:02 98-06-60.50 1
tert-Butyl Formate ND ug/L 06/12/14 22:02 762-75-420.0 1
Carbon tetrachloride ND ug/L 06/12/14 22:02 56-23-50.50 1
Chlorobenzene ND ug/L 06/12/14 22:02 108-90-70.50 1
Chloroethane ND ug/L 06/12/14 22:02 75-00-31.0 1
Chloroform ND ug/L 06/12/14 22:02 67-66-30.50 1
Chloromethane ND ug/L 06/12/14 22:02 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/12/14 22:02 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/12/14 22:02 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/14 22:02 96-12-81.0 1
Dibromochloromethane ND ug/L 06/12/14 22:02 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/14 22:02 106-93-40.50 1
Dibromomethane ND ug/L 06/12/14 22:02 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/12/14 22:02 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/12/14 22:02 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/12/14 22:02 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/12/14 22:02 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/12/14 22:02 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/12/14 22:02 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/12/14 22:02 75-35-40.50 1
cis-1,2-Dichloroethene 1.7 ug/L 06/12/14 22:02 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/12/14 22:02 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/12/14 22:02 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/12/14 22:02 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/12/14 22:02 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/12/14 22:02 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/12/14 22:02 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/12/14 22:02 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/12/14 22:02 108-20-30.50 1
Ethanol ND ug/L 06/12/14 22:02 64-17-52001
Ethylbenzene ND ug/L 06/12/14 22:02 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 06/12/14 22:02 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 06/12/14 22:02 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/12/14 22:02 98-82-80.50 1
Methylene Chloride ND ug/L 06/12/14 22:02 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/12/14 22:02 1634-04-40.50 1
Naphthalene ND ug/L 06/12/14 22:02 91-20-32.0 1
n-Propylbenzene ND ug/L 06/12/14 22:02 103-65-10.50 1
Styrene ND ug/L 06/12/14 22:02 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/14 22:02 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/14 22:02 79-34-50.50 1
Tetrachloroethene 0.51 ug/L 06/12/14 22:02 127-18-40.50 1
Toluene ND ug/L 06/12/14 22:02 108-88-30.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:DMW-2 Lab ID:92204797002 Collected:06/10/14 12:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
1,2,3-Trichlorobenzene ND ug/L 06/12/14 22:02 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/12/14 22:02 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/12/14 22:02 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/12/14 22:02 79-00-50.50 1
Trichloroethene ND ug/L 06/12/14 22:02 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/12/14 22:02 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/12/14 22:02 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/12/14 22:02 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/12/14 22:02 108-67-80.50 1
Vinyl chloride ND ug/L 06/12/14 22:02 75-01-41.0 1
m&p-Xylene ND ug/L 06/12/14 22:02 179601-23-11.0 1
o-Xylene ND ug/L 06/12/14 22:02 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %06/12/14 22:02 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %06/12/14 22:02 460-00-470-130 1
Toluene-d8 (S)99 %06/12/14 22:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-2 Lab ID:92204797003 Collected:06/10/14 15:15 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)378 ug/L 06/14/14 17:41 N206/12/14 16:001001
Aliphatic (C19-C36)126 ug/L 06/14/14 17:41 N206/12/14 16:001001
Aromatic (C11-C22)667 ug/L 06/14/14 17:09 N206/12/14 16:001001
Surrogates
Nonatriacontane (S)57 %06/14/14 17:41 7194-86-7 P206/12/14 16:0040-140 1
o-Terphenyl (S)75 %06/14/14 17:09 84-15-1 P206/12/14 16:0040-140 1
2-Fluorobiphenyl (S)100 %06/14/14 17:09 321-60-806/12/14 16:0040-140 1
2-Bromonaphthalene (S)120 %06/14/14 17:09 580-13-206/12/14 16:0040-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)740 ug/L 06/23/14 22:19 N22505
Aliphatic (C09-C12)1430 ug/L 06/23/14 22:19 N22505
Aromatic (C09-C10)625 ug/L 06/23/14 22:19 N22505
Surrogates
4-Bromofluorobenzene (FID) (S)96 %06/23/14 22:19 460-00-470-130 5
4-Bromofluorobenzene (PID) (S)96 %06/23/14 22:19 460-00-470-130 5
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/12/14 23:43 83-32-906/11/14 16:015.0 1
Acenaphthylene ND ug/L 06/12/14 23:43 208-96-806/11/14 16:015.0 1
Anthracene ND ug/L 06/12/14 23:43 120-12-706/11/14 16:015.0 1
Benzo(a)anthracene ND ug/L 06/12/14 23:43 56-55-306/11/14 16:015.0 1
Benzo(a)pyrene ND ug/L 06/12/14 23:43 50-32-806/11/14 16:015.0 1
Benzo(b)fluoranthene ND ug/L 06/12/14 23:43 205-99-206/11/14 16:015.0 1
Benzo(g,h,i)perylene ND ug/L 06/12/14 23:43 191-24-206/11/14 16:015.0 1
Benzo(k)fluoranthene ND ug/L 06/12/14 23:43 207-08-906/11/14 16:015.0 1
4-Bromophenylphenyl ether ND ug/L 06/12/14 23:43 101-55-306/11/14 16:015.0 1
Butylbenzylphthalate ND ug/L 06/12/14 23:43 85-68-706/11/14 16:015.0 1
4-Chloro-3-methylphenol ND ug/L 06/12/14 23:43 59-50-706/11/14 16:015.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/12/14 23:43 111-91-106/11/14 16:0110.0 1
bis(2-Chloroethyl) ether ND ug/L 06/12/14 23:43 111-44-406/11/14 16:015.0 1
bis(2-Chloroisopropyl) ether ND ug/L 06/12/14 23:43 108-60-106/11/14 16:015.0 1
2-Chloronaphthalene ND ug/L 06/12/14 23:43 91-58-706/11/14 16:015.0 1
2-Chlorophenol ND ug/L 06/12/14 23:43 95-57-806/11/14 16:015.0 1
4-Chlorophenylphenyl ether ND ug/L 06/12/14 23:43 7005-72-306/11/14 16:015.0 1
Chrysene ND ug/L 06/12/14 23:43 218-01-906/11/14 16:015.0 1
Dibenz(a,h)anthracene ND ug/L 06/12/14 23:43 53-70-306/11/14 16:015.0 1
3,3'-Dichlorobenzidine ND ug/L 06/12/14 23:43 91-94-106/11/14 16:0125.0 1
2,4-Dichlorophenol ND ug/L 06/12/14 23:43 120-83-206/11/14 16:015.0 1
Diethylphthalate ND ug/L 06/12/14 23:43 84-66-206/11/14 16:015.0 1
2,4-Dimethylphenol ND ug/L 06/12/14 23:43 105-67-906/11/14 16:0110.0 1
Dimethylphthalate ND ug/L 06/12/14 23:43 131-11-306/11/14 16:015.0 1
Di-n-butylphthalate ND ug/L 06/12/14 23:43 84-74-206/11/14 16:015.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/12/14 23:43 534-52-106/11/14 16:0120.0 1
2,4-Dinitrophenol ND ug/L 06/12/14 23:43 51-28-506/11/14 16:0150.0 1
2,4-Dinitrotoluene ND ug/L 06/12/14 23:43 121-14-206/11/14 16:015.0 1
2,6-Dinitrotoluene ND ug/L 06/12/14 23:43 606-20-206/11/14 16:015.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-2 Lab ID:92204797003 Collected:06/10/14 15:15 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 06/12/14 23:43 117-84-006/11/14 16:015.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/12/14 23:43 117-81-706/11/14 16:015.0 1
Fluoranthene ND ug/L 06/12/14 23:43 206-44-006/11/14 16:015.0 1
Fluorene ND ug/L 06/12/14 23:43 86-73-706/11/14 16:015.0 1
Hexachloro-1,3-butadiene ND ug/L 06/12/14 23:43 87-68-306/11/14 16:015.0 1
Hexachlorobenzene ND ug/L 06/12/14 23:43 118-74-106/11/14 16:015.0 1
Hexachlorocyclopentadiene ND ug/L 06/12/14 23:43 77-47-406/11/14 16:0110.0 1
Hexachloroethane ND ug/L 06/12/14 23:43 67-72-106/11/14 16:015.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/12/14 23:43 193-39-506/11/14 16:015.0 1
Isophorone ND ug/L 06/12/14 23:43 78-59-106/11/14 16:0110.0 1
Naphthalene ND ug/L 06/12/14 23:43 91-20-306/11/14 16:015.0 1
Nitrobenzene ND ug/L 06/12/14 23:43 98-95-306/11/14 16:015.0 1
2-Nitrophenol ND ug/L 06/12/14 23:43 88-75-506/11/14 16:015.0 1
4-Nitrophenol ND ug/L 06/12/14 23:43 100-02-706/11/14 16:0150.0 1
N-Nitrosodimethylamine ND ug/L 06/12/14 23:43 62-75-906/11/14 16:015.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/12/14 23:43 621-64-706/11/14 16:015.0 1
N-Nitrosodiphenylamine ND ug/L 06/12/14 23:43 86-30-606/11/14 16:0110.0 1
Pentachlorophenol ND ug/L 06/12/14 23:43 87-86-506/11/14 16:0110.0 1
Phenanthrene ND ug/L 06/12/14 23:43 85-01-806/11/14 16:015.0 1
Phenol ND ug/L 06/12/14 23:43 108-95-206/11/14 16:015.0 1
Pyrene ND ug/L 06/12/14 23:43 129-00-006/11/14 16:015.0 1
1,2,4-Trichlorobenzene ND ug/L 06/12/14 23:43 120-82-106/11/14 16:015.0 1
2,4,6-Trichlorophenol ND ug/L 06/12/14 23:43 88-06-206/11/14 16:0110.0 1
Surrogates
Nitrobenzene-d5 (S)22 %06/12/14 23:43 4165-60-006/11/14 16:0110-120 1
2-Fluorobiphenyl (S)27 %06/12/14 23:43 321-60-806/11/14 16:0115-120 1
Terphenyl-d14 (S)43 %06/12/14 23:43 1718-51-006/11/14 16:0111-131 1
Phenol-d6 (S)9 %06/12/14 23:43 13127-88-3 S006/11/14 16:0110-120 1
2-Fluorophenol (S)14 %06/12/14 23:43 367-12-406/11/14 16:0110-120 1
2,4,6-Tribromophenol (S)42 %06/12/14 23:43 118-79-606/11/14 16:0110-137 1
Tentatively Identified Compounds
2-Butanol, 2,3-dimethyl-13.0 ug/L 06/12/14 23:43 594-60-5 N06/11/14 16:011
Unknown 32.4 ug/L 06/12/14 23:43 N06/11/14 16:011
Unknown 21.8 ug/L 06/12/14 23:43 N06/11/14 16:011
Benzene, 1,2,3-trimethyl 16.6 ug/L 06/12/14 23:43 526-73-8 N06/11/14 16:011
Unknown 24.9 ug/L 06/12/14 23:43 N06/11/14 16:011
1-Methylindan-2-one 28.8 ug/L 06/12/14 23:43 35587-60-1 N06/11/14 16:011
Unknown 6.3 ug/L 06/12/14 23:43 N06/11/14 16:011
n-Hexadecanoic acid 24.4 ug/L 06/12/14 23:43 57-10-3 N06/11/14 16:011
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol ND ug/L 06/13/14 01:53 75-85-45005
tert-Amylmethyl ether ND ug/L 06/13/14 01:53 994-05-850.0 5
Benzene 187 ug/L 06/13/14 01:53 71-43-22.5 5
Bromobenzene ND ug/L 06/13/14 01:53 108-86-12.5 5
Bromochloromethane ND ug/L 06/13/14 01:53 74-97-52.5 5
Bromodichloromethane ND ug/L 06/13/14 01:53 75-27-42.5 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-2 Lab ID:92204797003 Collected:06/10/14 15:15 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Bromoform ND ug/L 06/13/14 01:53 75-25-22.5 5
Bromomethane ND ug/L 06/13/14 01:53 74-83-925.0 5
tert-Butyl Alcohol 259 ug/L 06/13/14 01:53 75-65-050.0 5
n-Butylbenzene ND ug/L 06/13/14 01:53 104-51-82.5 5
sec-Butylbenzene ND ug/L 06/13/14 01:53 135-98-82.5 5
tert-Butylbenzene ND ug/L 06/13/14 01:53 98-06-62.5 5
tert-Butyl Formate ND ug/L 06/13/14 01:53 762-75-41005
Carbon tetrachloride ND ug/L 06/13/14 01:53 56-23-52.5 5
Chlorobenzene ND ug/L 06/13/14 01:53 108-90-72.5 5
Chloroethane ND ug/L 06/13/14 01:53 75-00-35.0 5
Chloroform ND ug/L 06/13/14 01:53 67-66-32.5 5
Chloromethane ND ug/L 06/13/14 01:53 74-87-35.0 5
2-Chlorotoluene ND ug/L 06/13/14 01:53 95-49-82.5 5
4-Chlorotoluene ND ug/L 06/13/14 01:53 106-43-42.5 5
1,2-Dibromo-3-chloropropane ND ug/L 06/13/14 01:53 96-12-85.0 5
Dibromochloromethane ND ug/L 06/13/14 01:53 124-48-12.5 5
1,2-Dibromoethane (EDB)ND ug/L 06/13/14 01:53 106-93-42.5 5
Dibromomethane ND ug/L 06/13/14 01:53 74-95-32.5 5
1,2-Dichlorobenzene ND ug/L 06/13/14 01:53 95-50-12.5 5
1,3-Dichlorobenzene ND ug/L 06/13/14 01:53 541-73-12.5 5
1,4-Dichlorobenzene ND ug/L 06/13/14 01:53 106-46-72.5 5
Dichlorodifluoromethane ND ug/L 06/13/14 01:53 75-71-82.5 5
1,1-Dichloroethane 23.6 ug/L 06/13/14 01:53 75-34-32.5 5
1,2-Dichloroethane ND ug/L 06/13/14 01:53 107-06-22.5 5
1,1-Dichloroethene ND ug/L 06/13/14 01:53 75-35-42.5 5
cis-1,2-Dichloroethene 33.4 ug/L 06/13/14 01:53 156-59-22.5 5
trans-1,2-Dichloroethene ND ug/L 06/13/14 01:53 156-60-52.5 5
1,2-Dichloropropane ND ug/L 06/13/14 01:53 78-87-52.5 5
1,3-Dichloropropane ND ug/L 06/13/14 01:53 142-28-92.5 5
2,2-Dichloropropane ND ug/L 06/13/14 01:53 594-20-72.5 5
1,1-Dichloropropene ND ug/L 06/13/14 01:53 563-58-62.5 5
cis-1,3-Dichloropropene ND ug/L 06/13/14 01:53 10061-01-52.5 5
trans-1,3-Dichloropropene ND ug/L 06/13/14 01:53 10061-02-62.5 5
Diisopropyl ether 24.5 ug/L 06/13/14 01:53 108-20-32.5 5
Ethanol ND ug/L 06/13/14 01:53 64-17-510005
Ethylbenzene 26.3 ug/L 06/13/14 01:53 100-41-42.5 5
Ethyl-tert-butyl ether ND ug/L 06/13/14 01:53 637-92-350.0 5
Hexachloro-1,3-butadiene ND ug/L 06/13/14 01:53 87-68-310.0 5
Isopropylbenzene (Cumene)7.9 ug/L 06/13/14 01:53 98-82-82.5 5
Methylene Chloride ND ug/L 06/13/14 01:53 75-09-210.0 5
Methyl-tert-butyl ether 422 ug/L 06/13/14 01:53 1634-04-42.5 5
Naphthalene 42.4 ug/L 06/13/14 01:53 91-20-310.0 5
n-Propylbenzene 14.7 ug/L 06/13/14 01:53 103-65-12.5 5
Styrene ND ug/L 06/13/14 01:53 100-42-52.5 5
1,1,1,2-Tetrachloroethane ND ug/L 06/13/14 01:53 630-20-62.5 5
1,1,2,2-Tetrachloroethane ND ug/L 06/13/14 01:53 79-34-52.5 5
Tetrachloroethene ND ug/L 06/13/14 01:53 127-18-42.5 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-2 Lab ID:92204797003 Collected:06/10/14 15:15 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene 12.3 ug/L 06/13/14 01:53 108-88-32.5 5
1,2,3-Trichlorobenzene ND ug/L 06/13/14 01:53 87-61-610.0 5
1,2,4-Trichlorobenzene ND ug/L 06/13/14 01:53 120-82-110.0 5
1,1,1-Trichloroethane ND ug/L 06/13/14 01:53 71-55-62.5 5
1,1,2-Trichloroethane ND ug/L 06/13/14 01:53 79-00-52.5 5
Trichloroethene ND ug/L 06/13/14 01:53 79-01-62.5 5
Trichlorofluoromethane ND ug/L 06/13/14 01:53 75-69-45.0 5
1,2,3-Trichloropropane ND ug/L 06/13/14 01:53 96-18-42.5 5
1,2,4-Trimethylbenzene 164 ug/L 06/13/14 01:53 95-63-62.5 5
1,3,5-Trimethylbenzene 62.0 ug/L 06/13/14 01:53 108-67-82.5 5
Vinyl chloride 10.9 ug/L 06/13/14 01:53 75-01-45.0 5
m&p-Xylene 86.7 ug/L 06/13/14 01:53 179601-23-15.0 5
o-Xylene ND ug/L 06/13/14 01:53 95-47-62.5 5
Surrogates
1,2-Dichloroethane-d4 (S)96 %06/13/14 01:53 17060-07-070-130 5
4-Bromofluorobenzene (S)99 %06/13/14 01:53 460-00-470-130 5
Toluene-d8 (S)100 %06/13/14 01:53 2037-26-570-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-4 Lab ID:92204797004 Collected:06/10/14 15:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 06/18/14 11:48 N206/16/14 14:451001
Aliphatic (C19-C36)ND ug/L 06/18/14 11:48 N206/16/14 14:451001
Aromatic (C11-C22)ND ug/L 06/18/14 11:48 N206/16/14 14:451001
Surrogates
Nonatriacontane (S)72 %06/18/14 11:48 7194-86-706/16/14 14:4540-140 1
o-Terphenyl (S)63 %06/18/14 11:48 84-15-106/16/14 14:4540-140 1
2-Fluorobiphenyl (S)65 %06/18/14 11:48 321-60-806/16/14 14:4540-140 1
2-Bromonaphthalene (S)73 %06/18/14 11:48 580-13-206/16/14 14:4540-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 06/18/14 19:12 N250.0 1
Aliphatic (C09-C12)ND ug/L 06/18/14 19:12 N250.0 1
Aromatic (C09-C10)ND ug/L 06/18/14 19:12 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)121 %06/18/14 19:12 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)107 %06/18/14 19:12 460-00-470-130 1
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/13/14 00:15 83-32-906/11/14 16:015.0 1
Acenaphthylene ND ug/L 06/13/14 00:15 208-96-806/11/14 16:015.0 1
Anthracene ND ug/L 06/13/14 00:15 120-12-706/11/14 16:015.0 1
Benzo(a)anthracene ND ug/L 06/13/14 00:15 56-55-306/11/14 16:015.0 1
Benzo(a)pyrene ND ug/L 06/13/14 00:15 50-32-806/11/14 16:015.0 1
Benzo(b)fluoranthene ND ug/L 06/13/14 00:15 205-99-206/11/14 16:015.0 1
Benzo(g,h,i)perylene ND ug/L 06/13/14 00:15 191-24-206/11/14 16:015.0 1
Benzo(k)fluoranthene ND ug/L 06/13/14 00:15 207-08-906/11/14 16:015.0 1
4-Bromophenylphenyl ether ND ug/L 06/13/14 00:15 101-55-306/11/14 16:015.0 1
Butylbenzylphthalate ND ug/L 06/13/14 00:15 85-68-706/11/14 16:015.0 1
4-Chloro-3-methylphenol ND ug/L 06/13/14 00:15 59-50-706/11/14 16:015.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/13/14 00:15 111-91-106/11/14 16:0110.0 1
bis(2-Chloroethyl) ether ND ug/L 06/13/14 00:15 111-44-406/11/14 16:015.0 1
bis(2-Chloroisopropyl) ether ND ug/L 06/13/14 00:15 108-60-106/11/14 16:015.0 1
2-Chloronaphthalene ND ug/L 06/13/14 00:15 91-58-706/11/14 16:015.0 1
2-Chlorophenol ND ug/L 06/13/14 00:15 95-57-806/11/14 16:015.0 1
4-Chlorophenylphenyl ether ND ug/L 06/13/14 00:15 7005-72-306/11/14 16:015.0 1
Chrysene ND ug/L 06/13/14 00:15 218-01-906/11/14 16:015.0 1
Dibenz(a,h)anthracene ND ug/L 06/13/14 00:15 53-70-306/11/14 16:015.0 1
3,3'-Dichlorobenzidine ND ug/L 06/13/14 00:15 91-94-106/11/14 16:0125.0 1
2,4-Dichlorophenol ND ug/L 06/13/14 00:15 120-83-206/11/14 16:015.0 1
Diethylphthalate ND ug/L 06/13/14 00:15 84-66-206/11/14 16:015.0 1
2,4-Dimethylphenol ND ug/L 06/13/14 00:15 105-67-906/11/14 16:0110.0 1
Dimethylphthalate ND ug/L 06/13/14 00:15 131-11-306/11/14 16:015.0 1
Di-n-butylphthalate ND ug/L 06/13/14 00:15 84-74-206/11/14 16:015.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/13/14 00:15 534-52-106/11/14 16:0120.0 1
2,4-Dinitrophenol ND ug/L 06/13/14 00:15 51-28-506/11/14 16:0150.0 1
2,4-Dinitrotoluene ND ug/L 06/13/14 00:15 121-14-206/11/14 16:015.0 1
2,6-Dinitrotoluene ND ug/L 06/13/14 00:15 606-20-206/11/14 16:015.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-4 Lab ID:92204797004 Collected:06/10/14 15:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 06/13/14 00:15 117-84-006/11/14 16:015.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/14 00:15 117-81-706/11/14 16:015.0 1
Fluoranthene ND ug/L 06/13/14 00:15 206-44-006/11/14 16:015.0 1
Fluorene ND ug/L 06/13/14 00:15 86-73-706/11/14 16:015.0 1
Hexachloro-1,3-butadiene ND ug/L 06/13/14 00:15 87-68-306/11/14 16:015.0 1
Hexachlorobenzene ND ug/L 06/13/14 00:15 118-74-106/11/14 16:015.0 1
Hexachlorocyclopentadiene ND ug/L 06/13/14 00:15 77-47-406/11/14 16:0110.0 1
Hexachloroethane ND ug/L 06/13/14 00:15 67-72-106/11/14 16:015.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/14 00:15 193-39-506/11/14 16:015.0 1
Isophorone ND ug/L 06/13/14 00:15 78-59-106/11/14 16:0110.0 1
Naphthalene ND ug/L 06/13/14 00:15 91-20-306/11/14 16:015.0 1
Nitrobenzene ND ug/L 06/13/14 00:15 98-95-306/11/14 16:015.0 1
2-Nitrophenol ND ug/L 06/13/14 00:15 88-75-506/11/14 16:015.0 1
4-Nitrophenol ND ug/L 06/13/14 00:15 100-02-706/11/14 16:0150.0 1
N-Nitrosodimethylamine ND ug/L 06/13/14 00:15 62-75-906/11/14 16:015.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/13/14 00:15 621-64-706/11/14 16:015.0 1
N-Nitrosodiphenylamine ND ug/L 06/13/14 00:15 86-30-606/11/14 16:0110.0 1
Pentachlorophenol ND ug/L 06/13/14 00:15 87-86-506/11/14 16:0110.0 1
Phenanthrene ND ug/L 06/13/14 00:15 85-01-806/11/14 16:015.0 1
Phenol ND ug/L 06/13/14 00:15 108-95-206/11/14 16:015.0 1
Pyrene ND ug/L 06/13/14 00:15 129-00-006/11/14 16:015.0 1
1,2,4-Trichlorobenzene ND ug/L 06/13/14 00:15 120-82-106/11/14 16:015.0 1
2,4,6-Trichlorophenol ND ug/L 06/13/14 00:15 88-06-206/11/14 16:0110.0 1
Surrogates
Nitrobenzene-d5 (S)53 %06/13/14 00:15 4165-60-006/11/14 16:0110-120 1
2-Fluorobiphenyl (S)59 %06/13/14 00:15 321-60-806/11/14 16:0115-120 1
Terphenyl-d14 (S)81 %06/13/14 00:15 1718-51-006/11/14 16:0111-131 1
Phenol-d6 (S)22 %06/13/14 00:15 13127-88-306/11/14 16:0110-120 1
2-Fluorophenol (S)32 %06/13/14 00:15 367-12-406/11/14 16:0110-120 1
2,4,6-Tribromophenol (S)73 %06/13/14 00:15 118-79-606/11/14 16:0110-137 1
Tentatively Identified Compounds
Unknown 5.6 ug/L 06/13/14 00:15 N06/11/14 16:011
Unknown 6.6 ug/L 06/13/14 00:15 N06/11/14 16:011
Phenol, 4,4'-butylidene 8.5 ug/L 06/13/14 00:15 85-60-9 N06/11/14 16:011
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol ND ug/L 06/12/14 22:18 75-85-41001
tert-Amylmethyl ether ND ug/L 06/12/14 22:18 994-05-810.0 1
Benzene ND ug/L 06/12/14 22:18 71-43-20.50 1
Bromobenzene ND ug/L 06/12/14 22:18 108-86-10.50 1
Bromochloromethane ND ug/L 06/12/14 22:18 74-97-50.50 1
Bromodichloromethane ND ug/L 06/12/14 22:18 75-27-40.50 1
Bromoform ND ug/L 06/12/14 22:18 75-25-20.50 1
Bromomethane ND ug/L 06/12/14 22:18 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 06/12/14 22:18 75-65-010.0 1
n-Butylbenzene ND ug/L 06/12/14 22:18 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/12/14 22:18 135-98-80.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-4 Lab ID:92204797004 Collected:06/10/14 15:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
tert-Butylbenzene ND ug/L 06/12/14 22:18 98-06-60.50 1
tert-Butyl Formate ND ug/L 06/12/14 22:18 762-75-420.0 1
Carbon tetrachloride ND ug/L 06/12/14 22:18 56-23-50.50 1
Chlorobenzene ND ug/L 06/12/14 22:18 108-90-70.50 1
Chloroethane ND ug/L 06/12/14 22:18 75-00-31.0 1
Chloroform ND ug/L 06/12/14 22:18 67-66-30.50 1
Chloromethane ND ug/L 06/12/14 22:18 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/12/14 22:18 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/12/14 22:18 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/14 22:18 96-12-81.0 1
Dibromochloromethane ND ug/L 06/12/14 22:18 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/14 22:18 106-93-40.50 1
Dibromomethane ND ug/L 06/12/14 22:18 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/12/14 22:18 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/12/14 22:18 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/12/14 22:18 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/12/14 22:18 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/12/14 22:18 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/12/14 22:18 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/12/14 22:18 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/12/14 22:18 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/12/14 22:18 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/12/14 22:18 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/12/14 22:18 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/12/14 22:18 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/12/14 22:18 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/12/14 22:18 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/12/14 22:18 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/12/14 22:18 108-20-30.50 1
Ethanol ND ug/L 06/12/14 22:18 64-17-52001
Ethylbenzene ND ug/L 06/12/14 22:18 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 06/12/14 22:18 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 06/12/14 22:18 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/12/14 22:18 98-82-80.50 1
Methylene Chloride ND ug/L 06/12/14 22:18 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/12/14 22:18 1634-04-40.50 1
Naphthalene ND ug/L 06/12/14 22:18 91-20-32.0 1
n-Propylbenzene ND ug/L 06/12/14 22:18 103-65-10.50 1
Styrene ND ug/L 06/12/14 22:18 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/14 22:18 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/14 22:18 79-34-50.50 1
Tetrachloroethene ND ug/L 06/12/14 22:18 127-18-40.50 1
Toluene ND ug/L 06/12/14 22:18 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/12/14 22:18 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/12/14 22:18 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/12/14 22:18 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/12/14 22:18 79-00-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 19 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-4 Lab ID:92204797004 Collected:06/10/14 15:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Trichloroethene ND ug/L 06/12/14 22:18 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/12/14 22:18 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/12/14 22:18 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/12/14 22:18 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/12/14 22:18 108-67-80.50 1
Vinyl chloride ND ug/L 06/12/14 22:18 75-01-41.0 1
m&p-Xylene ND ug/L 06/12/14 22:18 179601-23-11.0 1
o-Xylene ND ug/L 06/12/14 22:18 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %06/12/14 22:18 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %06/12/14 22:18 460-00-470-130 1
Toluene-d8 (S)100 %06/12/14 22:18 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-7 Lab ID:92204797005 Collected:06/10/14 14:20 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 06/18/14 12:21 N206/16/14 14:451001
Aliphatic (C19-C36)ND ug/L 06/18/14 12:21 N206/16/14 14:451001
Aromatic (C11-C22)ND ug/L 06/18/14 12:21 N206/16/14 14:451001
Surrogates
Nonatriacontane (S)65 %06/18/14 12:21 7194-86-706/16/14 14:4540-140 1
o-Terphenyl (S)66 %06/18/14 12:21 84-15-106/16/14 14:4540-140 1
2-Fluorobiphenyl (S)74 %06/18/14 12:21 321-60-806/16/14 14:4540-140 1
2-Bromonaphthalene (S)80 %06/18/14 12:21 580-13-206/16/14 14:4540-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 06/18/14 19:35 N250.0 1
Aliphatic (C09-C12)ND ug/L 06/18/14 19:35 N250.0 1
Aromatic (C09-C10)ND ug/L 06/18/14 19:35 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)120 %06/18/14 19:35 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)105 %06/18/14 19:35 460-00-470-130 1
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/13/14 00:46 83-32-906/11/14 16:015.0 1
Acenaphthylene ND ug/L 06/13/14 00:46 208-96-806/11/14 16:015.0 1
Anthracene ND ug/L 06/13/14 00:46 120-12-706/11/14 16:015.0 1
Benzo(a)anthracene ND ug/L 06/13/14 00:46 56-55-306/11/14 16:015.0 1
Benzo(a)pyrene ND ug/L 06/13/14 00:46 50-32-806/11/14 16:015.0 1
Benzo(b)fluoranthene ND ug/L 06/13/14 00:46 205-99-206/11/14 16:015.0 1
Benzo(g,h,i)perylene ND ug/L 06/13/14 00:46 191-24-206/11/14 16:015.0 1
Benzo(k)fluoranthene ND ug/L 06/13/14 00:46 207-08-906/11/14 16:015.0 1
4-Bromophenylphenyl ether ND ug/L 06/13/14 00:46 101-55-306/11/14 16:015.0 1
Butylbenzylphthalate ND ug/L 06/13/14 00:46 85-68-706/11/14 16:015.0 1
4-Chloro-3-methylphenol ND ug/L 06/13/14 00:46 59-50-706/11/14 16:015.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/13/14 00:46 111-91-106/11/14 16:0110.0 1
bis(2-Chloroethyl) ether ND ug/L 06/13/14 00:46 111-44-406/11/14 16:015.0 1
bis(2-Chloroisopropyl) ether ND ug/L 06/13/14 00:46 108-60-106/11/14 16:015.0 1
2-Chloronaphthalene ND ug/L 06/13/14 00:46 91-58-706/11/14 16:015.0 1
2-Chlorophenol ND ug/L 06/13/14 00:46 95-57-806/11/14 16:015.0 1
4-Chlorophenylphenyl ether ND ug/L 06/13/14 00:46 7005-72-306/11/14 16:015.0 1
Chrysene ND ug/L 06/13/14 00:46 218-01-906/11/14 16:015.0 1
Dibenz(a,h)anthracene ND ug/L 06/13/14 00:46 53-70-306/11/14 16:015.0 1
3,3'-Dichlorobenzidine ND ug/L 06/13/14 00:46 91-94-106/11/14 16:0125.0 1
2,4-Dichlorophenol ND ug/L 06/13/14 00:46 120-83-206/11/14 16:015.0 1
Diethylphthalate ND ug/L 06/13/14 00:46 84-66-206/11/14 16:015.0 1
2,4-Dimethylphenol ND ug/L 06/13/14 00:46 105-67-906/11/14 16:0110.0 1
Dimethylphthalate ND ug/L 06/13/14 00:46 131-11-306/11/14 16:015.0 1
Di-n-butylphthalate ND ug/L 06/13/14 00:46 84-74-206/11/14 16:015.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/13/14 00:46 534-52-106/11/14 16:0120.0 1
2,4-Dinitrophenol ND ug/L 06/13/14 00:46 51-28-506/11/14 16:0150.0 1
2,4-Dinitrotoluene ND ug/L 06/13/14 00:46 121-14-206/11/14 16:015.0 1
2,6-Dinitrotoluene ND ug/L 06/13/14 00:46 606-20-206/11/14 16:015.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-7 Lab ID:92204797005 Collected:06/10/14 14:20 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 06/13/14 00:46 117-84-006/11/14 16:015.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/14 00:46 117-81-706/11/14 16:015.0 1
Fluoranthene ND ug/L 06/13/14 00:46 206-44-006/11/14 16:015.0 1
Fluorene ND ug/L 06/13/14 00:46 86-73-706/11/14 16:015.0 1
Hexachloro-1,3-butadiene ND ug/L 06/13/14 00:46 87-68-306/11/14 16:015.0 1
Hexachlorobenzene ND ug/L 06/13/14 00:46 118-74-106/11/14 16:015.0 1
Hexachlorocyclopentadiene ND ug/L 06/13/14 00:46 77-47-406/11/14 16:0110.0 1
Hexachloroethane ND ug/L 06/13/14 00:46 67-72-106/11/14 16:015.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/14 00:46 193-39-506/11/14 16:015.0 1
Isophorone ND ug/L 06/13/14 00:46 78-59-106/11/14 16:0110.0 1
Naphthalene ND ug/L 06/13/14 00:46 91-20-306/11/14 16:015.0 1
Nitrobenzene ND ug/L 06/13/14 00:46 98-95-306/11/14 16:015.0 1
2-Nitrophenol ND ug/L 06/13/14 00:46 88-75-506/11/14 16:015.0 1
4-Nitrophenol ND ug/L 06/13/14 00:46 100-02-706/11/14 16:0150.0 1
N-Nitrosodimethylamine ND ug/L 06/13/14 00:46 62-75-906/11/14 16:015.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/13/14 00:46 621-64-706/11/14 16:015.0 1
N-Nitrosodiphenylamine ND ug/L 06/13/14 00:46 86-30-606/11/14 16:0110.0 1
Pentachlorophenol ND ug/L 06/13/14 00:46 87-86-506/11/14 16:0110.0 1
Phenanthrene ND ug/L 06/13/14 00:46 85-01-806/11/14 16:015.0 1
Phenol ND ug/L 06/13/14 00:46 108-95-206/11/14 16:015.0 1
Pyrene ND ug/L 06/13/14 00:46 129-00-006/11/14 16:015.0 1
1,2,4-Trichlorobenzene ND ug/L 06/13/14 00:46 120-82-106/11/14 16:015.0 1
2,4,6-Trichlorophenol ND ug/L 06/13/14 00:46 88-06-206/11/14 16:0110.0 1
Surrogates
Nitrobenzene-d5 (S)60 %06/13/14 00:46 4165-60-006/11/14 16:0110-120 1
2-Fluorobiphenyl (S)64 %06/13/14 00:46 321-60-806/11/14 16:0115-120 1
Terphenyl-d14 (S)83 %06/13/14 00:46 1718-51-006/11/14 16:0111-131 1
Phenol-d6 (S)29 %06/13/14 00:46 13127-88-306/11/14 16:0110-120 1
2-Fluorophenol (S)39 %06/13/14 00:46 367-12-406/11/14 16:0110-120 1
2,4,6-Tribromophenol (S)78 %06/13/14 00:46 118-79-606/11/14 16:0110-137 1
Tentatively Identified Compounds
Unknown 7.4 ug/L 06/13/14 00:46 N06/11/14 16:011
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol ND ug/L 06/12/14 22:35 75-85-41001
tert-Amylmethyl ether ND ug/L 06/12/14 22:35 994-05-810.0 1
Benzene ND ug/L 06/12/14 22:35 71-43-20.50 1
Bromobenzene ND ug/L 06/12/14 22:35 108-86-10.50 1
Bromochloromethane ND ug/L 06/12/14 22:35 74-97-50.50 1
Bromodichloromethane ND ug/L 06/12/14 22:35 75-27-40.50 1
Bromoform ND ug/L 06/12/14 22:35 75-25-20.50 1
Bromomethane ND ug/L 06/12/14 22:35 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 06/12/14 22:35 75-65-010.0 1
n-Butylbenzene ND ug/L 06/12/14 22:35 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/12/14 22:35 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/12/14 22:35 98-06-60.50 1
tert-Butyl Formate ND ug/L 06/12/14 22:35 762-75-420.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-7 Lab ID:92204797005 Collected:06/10/14 14:20 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Carbon tetrachloride ND ug/L 06/12/14 22:35 56-23-50.50 1
Chlorobenzene ND ug/L 06/12/14 22:35 108-90-70.50 1
Chloroethane ND ug/L 06/12/14 22:35 75-00-31.0 1
Chloroform ND ug/L 06/12/14 22:35 67-66-30.50 1
Chloromethane ND ug/L 06/12/14 22:35 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/12/14 22:35 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/12/14 22:35 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/14 22:35 96-12-81.0 1
Dibromochloromethane ND ug/L 06/12/14 22:35 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/14 22:35 106-93-40.50 1
Dibromomethane ND ug/L 06/12/14 22:35 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/12/14 22:35 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/12/14 22:35 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/12/14 22:35 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/12/14 22:35 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/12/14 22:35 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/12/14 22:35 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/12/14 22:35 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/12/14 22:35 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/12/14 22:35 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/12/14 22:35 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/12/14 22:35 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/12/14 22:35 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/12/14 22:35 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/12/14 22:35 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/12/14 22:35 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/12/14 22:35 108-20-30.50 1
Ethanol ND ug/L 06/12/14 22:35 64-17-52001
Ethylbenzene ND ug/L 06/12/14 22:35 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 06/12/14 22:35 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 06/12/14 22:35 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/12/14 22:35 98-82-80.50 1
Methylene Chloride ND ug/L 06/12/14 22:35 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/12/14 22:35 1634-04-40.50 1
Naphthalene ND ug/L 06/12/14 22:35 91-20-32.0 1
n-Propylbenzene ND ug/L 06/12/14 22:35 103-65-10.50 1
Styrene ND ug/L 06/12/14 22:35 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/14 22:35 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/14 22:35 79-34-50.50 1
Tetrachloroethene ND ug/L 06/12/14 22:35 127-18-40.50 1
Toluene ND ug/L 06/12/14 22:35 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/12/14 22:35 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/12/14 22:35 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/12/14 22:35 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/12/14 22:35 79-00-50.50 1
Trichloroethene ND ug/L 06/12/14 22:35 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/12/14 22:35 75-69-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-7 Lab ID:92204797005 Collected:06/10/14 14:20 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
1,2,3-Trichloropropane ND ug/L 06/12/14 22:35 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/12/14 22:35 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/12/14 22:35 108-67-80.50 1
Vinyl chloride ND ug/L 06/12/14 22:35 75-01-41.0 1
m&p-Xylene ND ug/L 06/12/14 22:35 179601-23-11.0 1
o-Xylene ND ug/L 06/12/14 22:35 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %06/12/14 22:35 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %06/12/14 22:35 460-00-470-130 1
Toluene-d8 (S)100 %06/12/14 22:35 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-8 Lab ID:92204797006 Collected:06/10/14 12:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 06/18/14 12:53 N206/16/14 14:451001
Aliphatic (C19-C36)ND ug/L 06/18/14 12:53 N206/16/14 14:451001
Aromatic (C11-C22)ND ug/L 06/18/14 12:53 N206/16/14 14:451001
Surrogates
Nonatriacontane (S)67 %06/18/14 12:53 7194-86-706/16/14 14:4540-140 1
o-Terphenyl (S)86 %06/18/14 12:53 84-15-106/16/14 14:4540-140 1
2-Fluorobiphenyl (S)86 %06/18/14 12:53 321-60-806/16/14 14:4540-140 1
2-Bromonaphthalene (S)89 %06/18/14 12:53 580-13-206/16/14 14:4540-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)164 ug/L 06/18/14 19:58 N250.0 1
Aliphatic (C09-C12)ND ug/L 06/18/14 19:58 N250.0 1
Aromatic (C09-C10)ND ug/L 06/18/14 19:58 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)117 %06/18/14 19:58 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)104 %06/18/14 19:58 460-00-470-130 1
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/13/14 01:18 83-32-906/11/14 16:015.0 1
Acenaphthylene ND ug/L 06/13/14 01:18 208-96-806/11/14 16:015.0 1
Anthracene ND ug/L 06/13/14 01:18 120-12-706/11/14 16:015.0 1
Benzo(a)anthracene ND ug/L 06/13/14 01:18 56-55-306/11/14 16:015.0 1
Benzo(a)pyrene ND ug/L 06/13/14 01:18 50-32-806/11/14 16:015.0 1
Benzo(b)fluoranthene ND ug/L 06/13/14 01:18 205-99-206/11/14 16:015.0 1
Benzo(g,h,i)perylene ND ug/L 06/13/14 01:18 191-24-206/11/14 16:015.0 1
Benzo(k)fluoranthene ND ug/L 06/13/14 01:18 207-08-906/11/14 16:015.0 1
4-Bromophenylphenyl ether ND ug/L 06/13/14 01:18 101-55-306/11/14 16:015.0 1
Butylbenzylphthalate ND ug/L 06/13/14 01:18 85-68-706/11/14 16:015.0 1
4-Chloro-3-methylphenol ND ug/L 06/13/14 01:18 59-50-706/11/14 16:015.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/13/14 01:18 111-91-106/11/14 16:0110.0 1
bis(2-Chloroethyl) ether ND ug/L 06/13/14 01:18 111-44-406/11/14 16:015.0 1
bis(2-Chloroisopropyl) ether ND ug/L 06/13/14 01:18 108-60-106/11/14 16:015.0 1
2-Chloronaphthalene ND ug/L 06/13/14 01:18 91-58-706/11/14 16:015.0 1
2-Chlorophenol ND ug/L 06/13/14 01:18 95-57-806/11/14 16:015.0 1
4-Chlorophenylphenyl ether ND ug/L 06/13/14 01:18 7005-72-306/11/14 16:015.0 1
Chrysene ND ug/L 06/13/14 01:18 218-01-906/11/14 16:015.0 1
Dibenz(a,h)anthracene ND ug/L 06/13/14 01:18 53-70-306/11/14 16:015.0 1
3,3'-Dichlorobenzidine ND ug/L 06/13/14 01:18 91-94-106/11/14 16:0125.0 1
2,4-Dichlorophenol ND ug/L 06/13/14 01:18 120-83-206/11/14 16:015.0 1
Diethylphthalate ND ug/L 06/13/14 01:18 84-66-206/11/14 16:015.0 1
2,4-Dimethylphenol ND ug/L 06/13/14 01:18 105-67-906/11/14 16:0110.0 1
Dimethylphthalate ND ug/L 06/13/14 01:18 131-11-306/11/14 16:015.0 1
Di-n-butylphthalate ND ug/L 06/13/14 01:18 84-74-206/11/14 16:015.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/13/14 01:18 534-52-106/11/14 16:0120.0 1
2,4-Dinitrophenol ND ug/L 06/13/14 01:18 51-28-506/11/14 16:0150.0 1
2,4-Dinitrotoluene ND ug/L 06/13/14 01:18 121-14-206/11/14 16:015.0 1
2,6-Dinitrotoluene ND ug/L 06/13/14 01:18 606-20-206/11/14 16:015.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-8 Lab ID:92204797006 Collected:06/10/14 12:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 06/13/14 01:18 117-84-006/11/14 16:015.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/14 01:18 117-81-706/11/14 16:015.0 1
Fluoranthene ND ug/L 06/13/14 01:18 206-44-006/11/14 16:015.0 1
Fluorene ND ug/L 06/13/14 01:18 86-73-706/11/14 16:015.0 1
Hexachloro-1,3-butadiene ND ug/L 06/13/14 01:18 87-68-306/11/14 16:015.0 1
Hexachlorobenzene ND ug/L 06/13/14 01:18 118-74-106/11/14 16:015.0 1
Hexachlorocyclopentadiene ND ug/L 06/13/14 01:18 77-47-406/11/14 16:0110.0 1
Hexachloroethane ND ug/L 06/13/14 01:18 67-72-106/11/14 16:015.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/14 01:18 193-39-506/11/14 16:015.0 1
Isophorone ND ug/L 06/13/14 01:18 78-59-106/11/14 16:0110.0 1
Naphthalene ND ug/L 06/13/14 01:18 91-20-306/11/14 16:015.0 1
Nitrobenzene ND ug/L 06/13/14 01:18 98-95-306/11/14 16:015.0 1
2-Nitrophenol ND ug/L 06/13/14 01:18 88-75-506/11/14 16:015.0 1
4-Nitrophenol ND ug/L 06/13/14 01:18 100-02-706/11/14 16:0150.0 1
N-Nitrosodimethylamine ND ug/L 06/13/14 01:18 62-75-906/11/14 16:015.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/13/14 01:18 621-64-706/11/14 16:015.0 1
N-Nitrosodiphenylamine ND ug/L 06/13/14 01:18 86-30-606/11/14 16:0110.0 1
Pentachlorophenol ND ug/L 06/13/14 01:18 87-86-506/11/14 16:0110.0 1
Phenanthrene ND ug/L 06/13/14 01:18 85-01-806/11/14 16:015.0 1
Phenol ND ug/L 06/13/14 01:18 108-95-206/11/14 16:015.0 1
Pyrene ND ug/L 06/13/14 01:18 129-00-006/11/14 16:015.0 1
1,2,4-Trichlorobenzene ND ug/L 06/13/14 01:18 120-82-106/11/14 16:015.0 1
2,4,6-Trichlorophenol ND ug/L 06/13/14 01:18 88-06-206/11/14 16:0110.0 1
Surrogates
Nitrobenzene-d5 (S)73 %06/13/14 01:18 4165-60-006/11/14 16:0110-120 1
2-Fluorobiphenyl (S)77 %06/13/14 01:18 321-60-806/11/14 16:0115-120 1
Terphenyl-d14 (S)86 %06/13/14 01:18 1718-51-006/11/14 16:0111-131 1
Phenol-d6 (S)31 %06/13/14 01:18 13127-88-306/11/14 16:0110-120 1
2-Fluorophenol (S)44 %06/13/14 01:18 367-12-406/11/14 16:0110-120 1
2,4,6-Tribromophenol (S)81 %06/13/14 01:18 118-79-606/11/14 16:0110-137 1
Tentatively Identified Compounds
Tetrachloroethylene 62.6 ug/L 06/13/14 01:18 127-18-4 N06/11/14 16:011
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol ND ug/L 06/13/14 01:04 75-85-41001
tert-Amylmethyl ether ND ug/L 06/13/14 01:04 994-05-810.0 1
Benzene ND ug/L 06/13/14 01:04 71-43-20.50 1
Bromobenzene ND ug/L 06/13/14 01:04 108-86-10.50 1
Bromochloromethane ND ug/L 06/13/14 01:04 74-97-50.50 1
Bromodichloromethane ND ug/L 06/13/14 01:04 75-27-40.50 1
Bromoform ND ug/L 06/13/14 01:04 75-25-20.50 1
Bromomethane ND ug/L 06/13/14 01:04 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 06/13/14 01:04 75-65-010.0 1
n-Butylbenzene ND ug/L 06/13/14 01:04 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/13/14 01:04 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/13/14 01:04 98-06-60.50 1
tert-Butyl Formate ND ug/L 06/13/14 01:04 762-75-420.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-8 Lab ID:92204797006 Collected:06/10/14 12:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Carbon tetrachloride ND ug/L 06/13/14 01:04 56-23-50.50 1
Chlorobenzene ND ug/L 06/13/14 01:04 108-90-70.50 1
Chloroethane ND ug/L 06/13/14 01:04 75-00-31.0 1
Chloroform ND ug/L 06/13/14 01:04 67-66-30.50 1
Chloromethane ND ug/L 06/13/14 01:04 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/13/14 01:04 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/13/14 01:04 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/13/14 01:04 96-12-81.0 1
Dibromochloromethane ND ug/L 06/13/14 01:04 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/13/14 01:04 106-93-40.50 1
Dibromomethane ND ug/L 06/13/14 01:04 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/13/14 01:04 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/13/14 01:04 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/13/14 01:04 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/13/14 01:04 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/13/14 01:04 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/13/14 01:04 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/13/14 01:04 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/13/14 01:04 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/13/14 01:04 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/13/14 01:04 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/13/14 01:04 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/13/14 01:04 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/13/14 01:04 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/13/14 01:04 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/13/14 01:04 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/13/14 01:04 108-20-30.50 1
Ethanol ND ug/L 06/13/14 01:04 64-17-52001
Ethylbenzene ND ug/L 06/13/14 01:04 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 06/13/14 01:04 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 06/13/14 01:04 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/13/14 01:04 98-82-80.50 1
Methylene Chloride ND ug/L 06/13/14 01:04 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/13/14 01:04 1634-04-40.50 1
Naphthalene ND ug/L 06/13/14 01:04 91-20-32.0 1
n-Propylbenzene ND ug/L 06/13/14 01:04 103-65-10.50 1
Styrene ND ug/L 06/13/14 01:04 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/13/14 01:04 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/13/14 01:04 79-34-50.50 1
Tetrachloroethene 241 ug/L 06/16/14 23:04 127-18-41.2 2.5
Toluene ND ug/L 06/13/14 01:04 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/13/14 01:04 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/13/14 01:04 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/13/14 01:04 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/13/14 01:04 79-00-50.50 1
Trichloroethene 4.5 ug/L 06/13/14 01:04 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/13/14 01:04 75-69-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-8 Lab ID:92204797006 Collected:06/10/14 12:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
1,2,3-Trichloropropane ND ug/L 06/13/14 01:04 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/13/14 01:04 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/13/14 01:04 108-67-80.50 1
Vinyl chloride ND ug/L 06/13/14 01:04 75-01-41.0 1
m&p-Xylene ND ug/L 06/13/14 01:04 179601-23-11.0 1
o-Xylene ND ug/L 06/13/14 01:04 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %06/13/14 01:04 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %06/13/14 01:04 460-00-470-130 1
Toluene-d8 (S)99 %06/13/14 01:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-9 Lab ID:92204797007 Collected:06/10/14 13:40 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 06/18/14 13:26 N206/16/14 14:451001
Aliphatic (C19-C36)ND ug/L 06/18/14 13:26 N206/16/14 14:451001
Aromatic (C11-C22)ND ug/L 06/18/14 13:26 N206/16/14 14:451001
Surrogates
Nonatriacontane (S)87 %06/18/14 13:26 7194-86-706/16/14 14:4540-140 1
o-Terphenyl (S)68 %06/18/14 13:26 84-15-106/16/14 14:4540-140 1
2-Fluorobiphenyl (S)68 %06/18/14 13:26 321-60-806/16/14 14:4540-140 1
2-Bromonaphthalene (S)73 %06/18/14 13:26 580-13-206/16/14 14:4540-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)60.9 ug/L 06/18/14 20:21 N250.0 1
Aliphatic (C09-C12)ND ug/L 06/18/14 20:21 N250.0 1
Aromatic (C09-C10)ND ug/L 06/18/14 20:21 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)119 %06/18/14 20:21 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)105 %06/18/14 20:21 460-00-470-130 1
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/13/14 01:49 83-32-906/11/14 16:015.0 1
Acenaphthylene ND ug/L 06/13/14 01:49 208-96-806/11/14 16:015.0 1
Anthracene ND ug/L 06/13/14 01:49 120-12-706/11/14 16:015.0 1
Benzo(a)anthracene ND ug/L 06/13/14 01:49 56-55-306/11/14 16:015.0 1
Benzo(a)pyrene ND ug/L 06/13/14 01:49 50-32-806/11/14 16:015.0 1
Benzo(b)fluoranthene ND ug/L 06/13/14 01:49 205-99-206/11/14 16:015.0 1
Benzo(g,h,i)perylene ND ug/L 06/13/14 01:49 191-24-206/11/14 16:015.0 1
Benzo(k)fluoranthene ND ug/L 06/13/14 01:49 207-08-906/11/14 16:015.0 1
4-Bromophenylphenyl ether ND ug/L 06/13/14 01:49 101-55-306/11/14 16:015.0 1
Butylbenzylphthalate ND ug/L 06/13/14 01:49 85-68-706/11/14 16:015.0 1
4-Chloro-3-methylphenol ND ug/L 06/13/14 01:49 59-50-706/11/14 16:015.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/13/14 01:49 111-91-106/11/14 16:0110.0 1
bis(2-Chloroethyl) ether ND ug/L 06/13/14 01:49 111-44-406/11/14 16:015.0 1
bis(2-Chloroisopropyl) ether ND ug/L 06/13/14 01:49 108-60-106/11/14 16:015.0 1
2-Chloronaphthalene ND ug/L 06/13/14 01:49 91-58-706/11/14 16:015.0 1
2-Chlorophenol ND ug/L 06/13/14 01:49 95-57-806/11/14 16:015.0 1
4-Chlorophenylphenyl ether ND ug/L 06/13/14 01:49 7005-72-306/11/14 16:015.0 1
Chrysene ND ug/L 06/13/14 01:49 218-01-906/11/14 16:015.0 1
Dibenz(a,h)anthracene ND ug/L 06/13/14 01:49 53-70-306/11/14 16:015.0 1
3,3'-Dichlorobenzidine ND ug/L 06/13/14 01:49 91-94-106/11/14 16:0125.0 1
2,4-Dichlorophenol ND ug/L 06/13/14 01:49 120-83-206/11/14 16:015.0 1
Diethylphthalate ND ug/L 06/13/14 01:49 84-66-206/11/14 16:015.0 1
2,4-Dimethylphenol ND ug/L 06/13/14 01:49 105-67-906/11/14 16:0110.0 1
Dimethylphthalate ND ug/L 06/13/14 01:49 131-11-306/11/14 16:015.0 1
Di-n-butylphthalate ND ug/L 06/13/14 01:49 84-74-206/11/14 16:015.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/13/14 01:49 534-52-106/11/14 16:0120.0 1
2,4-Dinitrophenol ND ug/L 06/13/14 01:49 51-28-506/11/14 16:0150.0 1
2,4-Dinitrotoluene ND ug/L 06/13/14 01:49 121-14-206/11/14 16:015.0 1
2,6-Dinitrotoluene ND ug/L 06/13/14 01:49 606-20-206/11/14 16:015.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-9 Lab ID:92204797007 Collected:06/10/14 13:40 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 06/13/14 01:49 117-84-006/11/14 16:015.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/14 01:49 117-81-706/11/14 16:015.0 1
Fluoranthene ND ug/L 06/13/14 01:49 206-44-006/11/14 16:015.0 1
Fluorene ND ug/L 06/13/14 01:49 86-73-706/11/14 16:015.0 1
Hexachloro-1,3-butadiene ND ug/L 06/13/14 01:49 87-68-306/11/14 16:015.0 1
Hexachlorobenzene ND ug/L 06/13/14 01:49 118-74-106/11/14 16:015.0 1
Hexachlorocyclopentadiene ND ug/L 06/13/14 01:49 77-47-406/11/14 16:0110.0 1
Hexachloroethane ND ug/L 06/13/14 01:49 67-72-106/11/14 16:015.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/14 01:49 193-39-506/11/14 16:015.0 1
Isophorone ND ug/L 06/13/14 01:49 78-59-106/11/14 16:0110.0 1
Naphthalene ND ug/L 06/13/14 01:49 91-20-306/11/14 16:015.0 1
Nitrobenzene ND ug/L 06/13/14 01:49 98-95-306/11/14 16:015.0 1
2-Nitrophenol ND ug/L 06/13/14 01:49 88-75-506/11/14 16:015.0 1
4-Nitrophenol ND ug/L 06/13/14 01:49 100-02-706/11/14 16:0150.0 1
N-Nitrosodimethylamine ND ug/L 06/13/14 01:49 62-75-906/11/14 16:015.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/13/14 01:49 621-64-706/11/14 16:015.0 1
N-Nitrosodiphenylamine ND ug/L 06/13/14 01:49 86-30-606/11/14 16:0110.0 1
Pentachlorophenol ND ug/L 06/13/14 01:49 87-86-506/11/14 16:0110.0 1
Phenanthrene ND ug/L 06/13/14 01:49 85-01-806/11/14 16:015.0 1
Phenol ND ug/L 06/13/14 01:49 108-95-206/11/14 16:015.0 1
Pyrene ND ug/L 06/13/14 01:49 129-00-006/11/14 16:015.0 1
1,2,4-Trichlorobenzene ND ug/L 06/13/14 01:49 120-82-106/11/14 16:015.0 1
2,4,6-Trichlorophenol ND ug/L 06/13/14 01:49 88-06-206/11/14 16:0110.0 1
Surrogates
Nitrobenzene-d5 (S)27 %06/13/14 01:49 4165-60-006/11/14 16:0110-120 1
2-Fluorobiphenyl (S)29 %06/13/14 01:49 321-60-806/11/14 16:0115-120 1
Terphenyl-d14 (S)53 %06/13/14 01:49 1718-51-006/11/14 16:0111-131 1
Phenol-d6 (S)11 %06/13/14 01:49 13127-88-306/11/14 16:0110-120 1
2-Fluorophenol (S)17 %06/13/14 01:49 367-12-406/11/14 16:0110-120 1
2,4,6-Tribromophenol (S)41 %06/13/14 01:49 118-79-606/11/14 16:0110-137 1
Tentatively Identified Compounds
Tetrachloroethylene 7.2 ug/L 06/13/14 01:49 127-18-4 N06/11/14 16:011
Unknown 11.9 ug/L 06/13/14 01:49 N06/11/14 16:011
Unknown 5.6 ug/L 06/13/14 01:49 N06/11/14 16:011
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol ND ug/L 06/13/14 01:20 75-85-41001
tert-Amylmethyl ether ND ug/L 06/13/14 01:20 994-05-810.0 1
Benzene ND ug/L 06/13/14 01:20 71-43-20.50 1
Bromobenzene ND ug/L 06/13/14 01:20 108-86-10.50 1
Bromochloromethane ND ug/L 06/13/14 01:20 74-97-50.50 1
Bromodichloromethane ND ug/L 06/13/14 01:20 75-27-40.50 1
Bromoform ND ug/L 06/13/14 01:20 75-25-20.50 1
Bromomethane ND ug/L 06/13/14 01:20 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 06/13/14 01:20 75-65-010.0 1
n-Butylbenzene ND ug/L 06/13/14 01:20 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/13/14 01:20 135-98-80.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-9 Lab ID:92204797007 Collected:06/10/14 13:40 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
tert-Butylbenzene ND ug/L 06/13/14 01:20 98-06-60.50 1
tert-Butyl Formate ND ug/L 06/13/14 01:20 762-75-420.0 1
Carbon tetrachloride ND ug/L 06/13/14 01:20 56-23-50.50 1
Chlorobenzene ND ug/L 06/13/14 01:20 108-90-70.50 1
Chloroethane ND ug/L 06/13/14 01:20 75-00-31.0 1
Chloroform ND ug/L 06/13/14 01:20 67-66-30.50 1
Chloromethane ND ug/L 06/13/14 01:20 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/13/14 01:20 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/13/14 01:20 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/13/14 01:20 96-12-81.0 1
Dibromochloromethane ND ug/L 06/13/14 01:20 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/13/14 01:20 106-93-40.50 1
Dibromomethane ND ug/L 06/13/14 01:20 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/13/14 01:20 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/13/14 01:20 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/13/14 01:20 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/13/14 01:20 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/13/14 01:20 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/13/14 01:20 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/13/14 01:20 75-35-40.50 1
cis-1,2-Dichloroethene 0.73 ug/L 06/13/14 01:20 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/13/14 01:20 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/13/14 01:20 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/13/14 01:20 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/13/14 01:20 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/13/14 01:20 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/13/14 01:20 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/13/14 01:20 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/13/14 01:20 108-20-30.50 1
Ethanol ND ug/L 06/13/14 01:20 64-17-52001
Ethylbenzene ND ug/L 06/13/14 01:20 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 06/13/14 01:20 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 06/13/14 01:20 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/13/14 01:20 98-82-80.50 1
Methylene Chloride ND ug/L 06/13/14 01:20 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/13/14 01:20 1634-04-40.50 1
Naphthalene ND ug/L 06/13/14 01:20 91-20-32.0 1
n-Propylbenzene ND ug/L 06/13/14 01:20 103-65-10.50 1
Styrene ND ug/L 06/13/14 01:20 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/13/14 01:20 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/13/14 01:20 79-34-50.50 1
Tetrachloroethene 123 ug/L 06/13/14 01:20 127-18-40.50 1
Toluene ND ug/L 06/13/14 01:20 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/13/14 01:20 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/13/14 01:20 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/13/14 01:20 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/13/14 01:20 79-00-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-9 Lab ID:92204797007 Collected:06/10/14 13:40 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Trichloroethene ND ug/L 06/13/14 01:20 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/13/14 01:20 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/13/14 01:20 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/13/14 01:20 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/13/14 01:20 108-67-80.50 1
Vinyl chloride ND ug/L 06/13/14 01:20 75-01-41.0 1
m&p-Xylene ND ug/L 06/13/14 01:20 179601-23-11.0 1
o-Xylene ND ug/L 06/13/14 01:20 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)94 %06/13/14 01:20 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %06/13/14 01:20 460-00-470-130 1
Toluene-d8 (S)99 %06/13/14 01:20 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-11 Lab ID:92204797008 Collected:06/10/14 13:30 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 06/18/14 13:58 N206/16/14 14:451001
Aliphatic (C19-C36)ND ug/L 06/18/14 13:58 N206/16/14 14:451001
Aromatic (C11-C22)ND ug/L 06/18/14 13:58 N206/16/14 14:451001
Surrogates
Nonatriacontane (S)78 %06/18/14 13:58 7194-86-706/16/14 14:4540-140 1
o-Terphenyl (S)71 %06/18/14 13:58 84-15-106/16/14 14:4540-140 1
2-Fluorobiphenyl (S)77 %06/18/14 13:58 321-60-806/16/14 14:4540-140 1
2-Bromonaphthalene (S)87 %06/18/14 13:58 580-13-206/16/14 14:4540-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 06/18/14 20:46 N250.0 1
Aliphatic (C09-C12)ND ug/L 06/18/14 20:46 N250.0 1
Aromatic (C09-C10)ND ug/L 06/18/14 20:46 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)118 %06/18/14 20:46 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)104 %06/18/14 20:46 460-00-470-130 1
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/13/14 02:20 83-32-906/11/14 16:015.0 1
Acenaphthylene ND ug/L 06/13/14 02:20 208-96-806/11/14 16:015.0 1
Anthracene ND ug/L 06/13/14 02:20 120-12-706/11/14 16:015.0 1
Benzo(a)anthracene ND ug/L 06/13/14 02:20 56-55-306/11/14 16:015.0 1
Benzo(a)pyrene ND ug/L 06/13/14 02:20 50-32-806/11/14 16:015.0 1
Benzo(b)fluoranthene ND ug/L 06/13/14 02:20 205-99-206/11/14 16:015.0 1
Benzo(g,h,i)perylene ND ug/L 06/13/14 02:20 191-24-206/11/14 16:015.0 1
Benzo(k)fluoranthene ND ug/L 06/13/14 02:20 207-08-906/11/14 16:015.0 1
4-Bromophenylphenyl ether ND ug/L 06/13/14 02:20 101-55-306/11/14 16:015.0 1
Butylbenzylphthalate ND ug/L 06/13/14 02:20 85-68-706/11/14 16:015.0 1
4-Chloro-3-methylphenol ND ug/L 06/13/14 02:20 59-50-706/11/14 16:015.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/13/14 02:20 111-91-106/11/14 16:0110.0 1
bis(2-Chloroethyl) ether ND ug/L 06/13/14 02:20 111-44-406/11/14 16:015.0 1
bis(2-Chloroisopropyl) ether ND ug/L 06/13/14 02:20 108-60-106/11/14 16:015.0 1
2-Chloronaphthalene ND ug/L 06/13/14 02:20 91-58-706/11/14 16:015.0 1
2-Chlorophenol ND ug/L 06/13/14 02:20 95-57-806/11/14 16:015.0 1
4-Chlorophenylphenyl ether ND ug/L 06/13/14 02:20 7005-72-306/11/14 16:015.0 1
Chrysene ND ug/L 06/13/14 02:20 218-01-906/11/14 16:015.0 1
Dibenz(a,h)anthracene ND ug/L 06/13/14 02:20 53-70-306/11/14 16:015.0 1
3,3'-Dichlorobenzidine ND ug/L 06/13/14 02:20 91-94-106/11/14 16:0125.0 1
2,4-Dichlorophenol ND ug/L 06/13/14 02:20 120-83-206/11/14 16:015.0 1
Diethylphthalate ND ug/L 06/13/14 02:20 84-66-206/11/14 16:015.0 1
2,4-Dimethylphenol ND ug/L 06/13/14 02:20 105-67-906/11/14 16:0110.0 1
Dimethylphthalate ND ug/L 06/13/14 02:20 131-11-306/11/14 16:015.0 1
Di-n-butylphthalate ND ug/L 06/13/14 02:20 84-74-206/11/14 16:015.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/13/14 02:20 534-52-106/11/14 16:0120.0 1
2,4-Dinitrophenol ND ug/L 06/13/14 02:20 51-28-506/11/14 16:0150.0 1
2,4-Dinitrotoluene ND ug/L 06/13/14 02:20 121-14-206/11/14 16:015.0 1
2,6-Dinitrotoluene ND ug/L 06/13/14 02:20 606-20-206/11/14 16:015.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-11 Lab ID:92204797008 Collected:06/10/14 13:30 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 06/13/14 02:20 117-84-006/11/14 16:015.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/14 02:20 117-81-706/11/14 16:015.0 1
Fluoranthene ND ug/L 06/13/14 02:20 206-44-006/11/14 16:015.0 1
Fluorene ND ug/L 06/13/14 02:20 86-73-706/11/14 16:015.0 1
Hexachloro-1,3-butadiene ND ug/L 06/13/14 02:20 87-68-306/11/14 16:015.0 1
Hexachlorobenzene ND ug/L 06/13/14 02:20 118-74-106/11/14 16:015.0 1
Hexachlorocyclopentadiene ND ug/L 06/13/14 02:20 77-47-406/11/14 16:0110.0 1
Hexachloroethane ND ug/L 06/13/14 02:20 67-72-106/11/14 16:015.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/14 02:20 193-39-506/11/14 16:015.0 1
Isophorone ND ug/L 06/13/14 02:20 78-59-106/11/14 16:0110.0 1
Naphthalene ND ug/L 06/13/14 02:20 91-20-306/11/14 16:015.0 1
Nitrobenzene ND ug/L 06/13/14 02:20 98-95-306/11/14 16:015.0 1
2-Nitrophenol ND ug/L 06/13/14 02:20 88-75-506/11/14 16:015.0 1
4-Nitrophenol ND ug/L 06/13/14 02:20 100-02-706/11/14 16:0150.0 1
N-Nitrosodimethylamine ND ug/L 06/13/14 02:20 62-75-906/11/14 16:015.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/13/14 02:20 621-64-706/11/14 16:015.0 1
N-Nitrosodiphenylamine ND ug/L 06/13/14 02:20 86-30-606/11/14 16:0110.0 1
Pentachlorophenol ND ug/L 06/13/14 02:20 87-86-506/11/14 16:0110.0 1
Phenanthrene ND ug/L 06/13/14 02:20 85-01-806/11/14 16:015.0 1
Phenol ND ug/L 06/13/14 02:20 108-95-206/11/14 16:015.0 1
Pyrene ND ug/L 06/13/14 02:20 129-00-006/11/14 16:015.0 1
1,2,4-Trichlorobenzene ND ug/L 06/13/14 02:20 120-82-106/11/14 16:015.0 1
2,4,6-Trichlorophenol ND ug/L 06/13/14 02:20 88-06-206/11/14 16:0110.0 1
Surrogates
Nitrobenzene-d5 (S)61 %06/13/14 02:20 4165-60-006/11/14 16:0110-120 1
2-Fluorobiphenyl (S)70 %06/13/14 02:20 321-60-806/11/14 16:0115-120 1
Terphenyl-d14 (S)84 %06/13/14 02:20 1718-51-006/11/14 16:0111-131 1
Phenol-d6 (S)21 %06/13/14 02:20 13127-88-306/11/14 16:0110-120 1
2-Fluorophenol (S)35 %06/13/14 02:20 367-12-406/11/14 16:0110-120 1
2,4,6-Tribromophenol (S)74 %06/13/14 02:20 118-79-606/11/14 16:0110-137 1
Tentatively Identified Compounds
Unknown 5.4 ug/L 06/13/14 02:20 N06/11/14 16:011
Unknown 8.8 ug/L 06/13/14 02:20 N06/11/14 16:011
Unknown 25.9 ug/L 06/13/14 02:20 N06/11/14 16:011
Unknown 101 ug/L 06/13/14 02:20 N06/11/14 16:011
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol ND ug/L 06/12/14 22:51 75-85-41001
tert-Amylmethyl ether ND ug/L 06/12/14 22:51 994-05-810.0 1
Benzene ND ug/L 06/12/14 22:51 71-43-20.50 1
Bromobenzene ND ug/L 06/12/14 22:51 108-86-10.50 1
Bromochloromethane ND ug/L 06/12/14 22:51 74-97-50.50 1
Bromodichloromethane ND ug/L 06/12/14 22:51 75-27-40.50 1
Bromoform ND ug/L 06/12/14 22:51 75-25-20.50 1
Bromomethane ND ug/L 06/12/14 22:51 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 06/12/14 22:51 75-65-010.0 1
n-Butylbenzene ND ug/L 06/12/14 22:51 104-51-80.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-11 Lab ID:92204797008 Collected:06/10/14 13:30 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
sec-Butylbenzene ND ug/L 06/12/14 22:51 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/12/14 22:51 98-06-60.50 1
tert-Butyl Formate ND ug/L 06/12/14 22:51 762-75-420.0 1
Carbon tetrachloride ND ug/L 06/12/14 22:51 56-23-50.50 1
Chlorobenzene ND ug/L 06/12/14 22:51 108-90-70.50 1
Chloroethane ND ug/L 06/12/14 22:51 75-00-31.0 1
Chloroform ND ug/L 06/12/14 22:51 67-66-30.50 1
Chloromethane ND ug/L 06/12/14 22:51 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/12/14 22:51 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/12/14 22:51 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/14 22:51 96-12-81.0 1
Dibromochloromethane ND ug/L 06/12/14 22:51 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/14 22:51 106-93-40.50 1
Dibromomethane ND ug/L 06/12/14 22:51 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/12/14 22:51 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/12/14 22:51 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/12/14 22:51 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/12/14 22:51 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/12/14 22:51 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/12/14 22:51 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/12/14 22:51 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/12/14 22:51 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/12/14 22:51 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/12/14 22:51 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/12/14 22:51 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/12/14 22:51 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/12/14 22:51 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/12/14 22:51 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/12/14 22:51 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/12/14 22:51 108-20-30.50 1
Ethanol ND ug/L 06/12/14 22:51 64-17-52001
Ethylbenzene ND ug/L 06/12/14 22:51 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 06/12/14 22:51 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 06/12/14 22:51 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/12/14 22:51 98-82-80.50 1
Methylene Chloride ND ug/L 06/12/14 22:51 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/12/14 22:51 1634-04-40.50 1
Naphthalene ND ug/L 06/12/14 22:51 91-20-32.0 1
n-Propylbenzene ND ug/L 06/12/14 22:51 103-65-10.50 1
Styrene ND ug/L 06/12/14 22:51 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/14 22:51 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/14 22:51 79-34-50.50 1
Tetrachloroethene 1.5 ug/L 06/12/14 22:51 127-18-40.50 1
Toluene ND ug/L 06/12/14 22:51 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/12/14 22:51 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/12/14 22:51 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/12/14 22:51 71-55-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-11 Lab ID:92204797008 Collected:06/10/14 13:30 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
1,1,2-Trichloroethane ND ug/L 06/12/14 22:51 79-00-50.50 1
Trichloroethene ND ug/L 06/12/14 22:51 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/12/14 22:51 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/12/14 22:51 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/12/14 22:51 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/12/14 22:51 108-67-80.50 1
Vinyl chloride ND ug/L 06/12/14 22:51 75-01-41.0 1
m&p-Xylene ND ug/L 06/12/14 22:51 179601-23-11.0 1
o-Xylene ND ug/L 06/12/14 22:51 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %06/12/14 22:51 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %06/12/14 22:51 460-00-470-130 1
Toluene-d8 (S)100 %06/12/14 22:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-16 Lab ID:92204797009 Collected:06/10/14 13:10 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 06/18/14 14:31 N206/16/14 14:451001
Aliphatic (C19-C36)ND ug/L 06/18/14 14:31 N206/16/14 14:451001
Aromatic (C11-C22)ND ug/L 06/18/14 14:31 N206/16/14 14:451001
Surrogates
Nonatriacontane (S)86 %06/18/14 14:31 7194-86-706/16/14 14:4540-140 1
o-Terphenyl (S)77 %06/18/14 14:31 84-15-106/16/14 14:4540-140 1
2-Fluorobiphenyl (S)82 %06/18/14 14:31 321-60-806/16/14 14:4540-140 1
2-Bromonaphthalene (S)89 %06/18/14 14:31 580-13-206/16/14 14:4540-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 06/18/14 21:09 N250.0 1
Aliphatic (C09-C12)ND ug/L 06/18/14 21:09 N250.0 1
Aromatic (C09-C10)ND ug/L 06/18/14 21:09 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)123 %06/18/14 21:09 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)109 %06/18/14 21:09 460-00-470-130 1
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/13/14 02:52 83-32-906/11/14 16:015.0 1
Acenaphthylene ND ug/L 06/13/14 02:52 208-96-806/11/14 16:015.0 1
Anthracene ND ug/L 06/13/14 02:52 120-12-706/11/14 16:015.0 1
Benzo(a)anthracene ND ug/L 06/13/14 02:52 56-55-306/11/14 16:015.0 1
Benzo(a)pyrene ND ug/L 06/13/14 02:52 50-32-806/11/14 16:015.0 1
Benzo(b)fluoranthene ND ug/L 06/13/14 02:52 205-99-206/11/14 16:015.0 1
Benzo(g,h,i)perylene ND ug/L 06/13/14 02:52 191-24-206/11/14 16:015.0 1
Benzo(k)fluoranthene ND ug/L 06/13/14 02:52 207-08-906/11/14 16:015.0 1
4-Bromophenylphenyl ether ND ug/L 06/13/14 02:52 101-55-306/11/14 16:015.0 1
Butylbenzylphthalate ND ug/L 06/13/14 02:52 85-68-706/11/14 16:015.0 1
4-Chloro-3-methylphenol ND ug/L 06/13/14 02:52 59-50-706/11/14 16:015.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/13/14 02:52 111-91-106/11/14 16:0110.0 1
bis(2-Chloroethyl) ether ND ug/L 06/13/14 02:52 111-44-406/11/14 16:015.0 1
bis(2-Chloroisopropyl) ether ND ug/L 06/13/14 02:52 108-60-106/11/14 16:015.0 1
2-Chloronaphthalene ND ug/L 06/13/14 02:52 91-58-706/11/14 16:015.0 1
2-Chlorophenol ND ug/L 06/13/14 02:52 95-57-806/11/14 16:015.0 1
4-Chlorophenylphenyl ether ND ug/L 06/13/14 02:52 7005-72-306/11/14 16:015.0 1
Chrysene ND ug/L 06/13/14 02:52 218-01-906/11/14 16:015.0 1
Dibenz(a,h)anthracene ND ug/L 06/13/14 02:52 53-70-306/11/14 16:015.0 1
3,3'-Dichlorobenzidine ND ug/L 06/13/14 02:52 91-94-106/11/14 16:0125.0 1
2,4-Dichlorophenol ND ug/L 06/13/14 02:52 120-83-206/11/14 16:015.0 1
Diethylphthalate ND ug/L 06/13/14 02:52 84-66-206/11/14 16:015.0 1
2,4-Dimethylphenol ND ug/L 06/13/14 02:52 105-67-906/11/14 16:0110.0 1
Dimethylphthalate ND ug/L 06/13/14 02:52 131-11-306/11/14 16:015.0 1
Di-n-butylphthalate ND ug/L 06/13/14 02:52 84-74-206/11/14 16:015.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/13/14 02:52 534-52-106/11/14 16:0120.0 1
2,4-Dinitrophenol ND ug/L 06/13/14 02:52 51-28-506/11/14 16:0150.0 1
2,4-Dinitrotoluene ND ug/L 06/13/14 02:52 121-14-206/11/14 16:015.0 1
2,6-Dinitrotoluene ND ug/L 06/13/14 02:52 606-20-206/11/14 16:015.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-16 Lab ID:92204797009 Collected:06/10/14 13:10 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 06/13/14 02:52 117-84-006/11/14 16:015.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/14 02:52 117-81-706/11/14 16:015.0 1
Fluoranthene ND ug/L 06/13/14 02:52 206-44-006/11/14 16:015.0 1
Fluorene ND ug/L 06/13/14 02:52 86-73-706/11/14 16:015.0 1
Hexachloro-1,3-butadiene ND ug/L 06/13/14 02:52 87-68-306/11/14 16:015.0 1
Hexachlorobenzene ND ug/L 06/13/14 02:52 118-74-106/11/14 16:015.0 1
Hexachlorocyclopentadiene ND ug/L 06/13/14 02:52 77-47-406/11/14 16:0110.0 1
Hexachloroethane ND ug/L 06/13/14 02:52 67-72-106/11/14 16:015.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/14 02:52 193-39-506/11/14 16:015.0 1
Isophorone ND ug/L 06/13/14 02:52 78-59-106/11/14 16:0110.0 1
Naphthalene ND ug/L 06/13/14 02:52 91-20-306/11/14 16:015.0 1
Nitrobenzene ND ug/L 06/13/14 02:52 98-95-306/11/14 16:015.0 1
2-Nitrophenol ND ug/L 06/13/14 02:52 88-75-506/11/14 16:015.0 1
4-Nitrophenol ND ug/L 06/13/14 02:52 100-02-706/11/14 16:0150.0 1
N-Nitrosodimethylamine ND ug/L 06/13/14 02:52 62-75-906/11/14 16:015.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/13/14 02:52 621-64-706/11/14 16:015.0 1
N-Nitrosodiphenylamine ND ug/L 06/13/14 02:52 86-30-606/11/14 16:0110.0 1
Pentachlorophenol ND ug/L 06/13/14 02:52 87-86-506/11/14 16:0110.0 1
Phenanthrene ND ug/L 06/13/14 02:52 85-01-806/11/14 16:015.0 1
Phenol ND ug/L 06/13/14 02:52 108-95-206/11/14 16:015.0 1
Pyrene ND ug/L 06/13/14 02:52 129-00-006/11/14 16:015.0 1
1,2,4-Trichlorobenzene ND ug/L 06/13/14 02:52 120-82-106/11/14 16:015.0 1
2,4,6-Trichlorophenol ND ug/L 06/13/14 02:52 88-06-206/11/14 16:0110.0 1
Surrogates
Nitrobenzene-d5 (S)56 %06/13/14 02:52 4165-60-006/11/14 16:0110-120 1
2-Fluorobiphenyl (S)63 %06/13/14 02:52 321-60-806/11/14 16:0115-120 1
Terphenyl-d14 (S)71 %06/13/14 02:52 1718-51-006/11/14 16:0111-131 1
Phenol-d6 (S)23 %06/13/14 02:52 13127-88-306/11/14 16:0110-120 1
2-Fluorophenol (S)35 %06/13/14 02:52 367-12-406/11/14 16:0110-120 1
2,4,6-Tribromophenol (S)63 %06/13/14 02:52 118-79-606/11/14 16:0110-137 1
Tentatively Identified Compounds
Unknown 6.6 ug/L 06/13/14 02:52 N06/11/14 16:011
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol ND ug/L 06/12/14 23:08 75-85-41001
tert-Amylmethyl ether ND ug/L 06/12/14 23:08 994-05-810.0 1
Benzene ND ug/L 06/12/14 23:08 71-43-20.50 1
Bromobenzene ND ug/L 06/12/14 23:08 108-86-10.50 1
Bromochloromethane ND ug/L 06/12/14 23:08 74-97-50.50 1
Bromodichloromethane ND ug/L 06/12/14 23:08 75-27-40.50 1
Bromoform ND ug/L 06/12/14 23:08 75-25-20.50 1
Bromomethane ND ug/L 06/12/14 23:08 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 06/12/14 23:08 75-65-010.0 1
n-Butylbenzene ND ug/L 06/12/14 23:08 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/12/14 23:08 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/12/14 23:08 98-06-60.50 1
tert-Butyl Formate ND ug/L 06/12/14 23:08 762-75-420.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-16 Lab ID:92204797009 Collected:06/10/14 13:10 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Carbon tetrachloride ND ug/L 06/12/14 23:08 56-23-50.50 1
Chlorobenzene ND ug/L 06/12/14 23:08 108-90-70.50 1
Chloroethane ND ug/L 06/12/14 23:08 75-00-31.0 1
Chloroform ND ug/L 06/12/14 23:08 67-66-30.50 1
Chloromethane ND ug/L 06/12/14 23:08 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/12/14 23:08 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/12/14 23:08 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/14 23:08 96-12-81.0 1
Dibromochloromethane ND ug/L 06/12/14 23:08 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/14 23:08 106-93-40.50 1
Dibromomethane ND ug/L 06/12/14 23:08 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/12/14 23:08 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/12/14 23:08 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/12/14 23:08 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/12/14 23:08 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/12/14 23:08 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/12/14 23:08 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/12/14 23:08 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/12/14 23:08 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/12/14 23:08 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/12/14 23:08 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/12/14 23:08 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/12/14 23:08 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/12/14 23:08 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/12/14 23:08 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/12/14 23:08 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/12/14 23:08 108-20-30.50 1
Ethanol ND ug/L 06/12/14 23:08 64-17-52001
Ethylbenzene ND ug/L 06/12/14 23:08 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 06/12/14 23:08 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 06/12/14 23:08 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/12/14 23:08 98-82-80.50 1
Methylene Chloride ND ug/L 06/12/14 23:08 75-09-22.0 1
Methyl-tert-butyl ether 0.78 ug/L 06/12/14 23:08 1634-04-40.50 1
Naphthalene ND ug/L 06/12/14 23:08 91-20-32.0 1
n-Propylbenzene ND ug/L 06/12/14 23:08 103-65-10.50 1
Styrene ND ug/L 06/12/14 23:08 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/14 23:08 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/14 23:08 79-34-50.50 1
Tetrachloroethene 0.98 ug/L 06/12/14 23:08 127-18-40.50 1
Toluene ND ug/L 06/12/14 23:08 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/12/14 23:08 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/12/14 23:08 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/12/14 23:08 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/12/14 23:08 79-00-50.50 1
Trichloroethene ND ug/L 06/12/14 23:08 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/12/14 23:08 75-69-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-16 Lab ID:92204797009 Collected:06/10/14 13:10 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
1,2,3-Trichloropropane ND ug/L 06/12/14 23:08 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/12/14 23:08 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/12/14 23:08 108-67-80.50 1
Vinyl chloride ND ug/L 06/12/14 23:08 75-01-41.0 1
m&p-Xylene ND ug/L 06/12/14 23:08 179601-23-11.0 1
o-Xylene ND ug/L 06/12/14 23:08 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %06/12/14 23:08 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %06/12/14 23:08 460-00-470-130 1
Toluene-d8 (S)99 %06/12/14 23:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-17 Lab ID:92204797010 Collected:06/10/14 11:10 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 06/18/14 15:03 N206/16/14 14:451001
Aliphatic (C19-C36)ND ug/L 06/18/14 15:03 N206/16/14 14:451001
Aromatic (C11-C22)ND ug/L 06/18/14 15:03 N206/16/14 14:451001
Surrogates
Nonatriacontane (S)86 %06/18/14 15:03 7194-86-706/16/14 14:4540-140 1
o-Terphenyl (S)74 %06/18/14 15:03 84-15-106/16/14 14:4540-140 1
2-Fluorobiphenyl (S)81 %06/18/14 15:03 321-60-806/16/14 14:4540-140 1
2-Bromonaphthalene (S)86 %06/18/14 15:03 580-13-206/16/14 14:4540-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 06/18/14 21:32 N250.0 1
Aliphatic (C09-C12)ND ug/L 06/18/14 21:32 N250.0 1
Aromatic (C09-C10)ND ug/L 06/18/14 21:32 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)125 %06/18/14 21:32 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)111 %06/18/14 21:32 460-00-470-130 1
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/13/14 03:23 83-32-906/11/14 16:018.3 1
Acenaphthylene ND ug/L 06/13/14 03:23 208-96-806/11/14 16:018.3 1
Anthracene ND ug/L 06/13/14 03:23 120-12-706/11/14 16:018.3 1
Benzo(a)anthracene ND ug/L 06/13/14 03:23 56-55-306/11/14 16:018.3 1
Benzo(a)pyrene ND ug/L 06/13/14 03:23 50-32-806/11/14 16:018.3 1
Benzo(b)fluoranthene ND ug/L 06/13/14 03:23 205-99-206/11/14 16:018.3 1
Benzo(g,h,i)perylene ND ug/L 06/13/14 03:23 191-24-206/11/14 16:018.3 1
Benzo(k)fluoranthene ND ug/L 06/13/14 03:23 207-08-906/11/14 16:018.3 1
4-Bromophenylphenyl ether ND ug/L 06/13/14 03:23 101-55-306/11/14 16:018.3 1
Butylbenzylphthalate ND ug/L 06/13/14 03:23 85-68-706/11/14 16:018.3 1
4-Chloro-3-methylphenol ND ug/L 06/13/14 03:23 59-50-706/11/14 16:018.3 1
bis(2-Chloroethoxy)methane ND ug/L 06/13/14 03:23 111-91-106/11/14 16:0116.7 1
bis(2-Chloroethyl) ether ND ug/L 06/13/14 03:23 111-44-406/11/14 16:018.3 1
bis(2-Chloroisopropyl) ether ND ug/L 06/13/14 03:23 108-60-106/11/14 16:018.3 1
2-Chloronaphthalene ND ug/L 06/13/14 03:23 91-58-706/11/14 16:018.3 1
2-Chlorophenol ND ug/L 06/13/14 03:23 95-57-806/11/14 16:018.3 1
4-Chlorophenylphenyl ether ND ug/L 06/13/14 03:23 7005-72-306/11/14 16:018.3 1
Chrysene ND ug/L 06/13/14 03:23 218-01-906/11/14 16:018.3 1
Dibenz(a,h)anthracene ND ug/L 06/13/14 03:23 53-70-306/11/14 16:018.3 1
3,3'-Dichlorobenzidine ND ug/L 06/13/14 03:23 91-94-106/11/14 16:0141.7 1
2,4-Dichlorophenol ND ug/L 06/13/14 03:23 120-83-206/11/14 16:018.3 1
Diethylphthalate ND ug/L 06/13/14 03:23 84-66-206/11/14 16:018.3 1
2,4-Dimethylphenol ND ug/L 06/13/14 03:23 105-67-906/11/14 16:0116.7 1
Dimethylphthalate ND ug/L 06/13/14 03:23 131-11-306/11/14 16:018.3 1
Di-n-butylphthalate ND ug/L 06/13/14 03:23 84-74-206/11/14 16:018.3 1
4,6-Dinitro-2-methylphenol ND ug/L 06/13/14 03:23 534-52-106/11/14 16:0133.3 1
2,4-Dinitrophenol ND ug/L 06/13/14 03:23 51-28-506/11/14 16:0183.3 1
2,4-Dinitrotoluene ND ug/L 06/13/14 03:23 121-14-206/11/14 16:018.3 1
2,6-Dinitrotoluene ND ug/L 06/13/14 03:23 606-20-206/11/14 16:018.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-17 Lab ID:92204797010 Collected:06/10/14 11:10 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 06/13/14 03:23 117-84-006/11/14 16:018.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/14 03:23 117-81-706/11/14 16:018.3 1
Fluoranthene ND ug/L 06/13/14 03:23 206-44-006/11/14 16:018.3 1
Fluorene ND ug/L 06/13/14 03:23 86-73-706/11/14 16:018.3 1
Hexachloro-1,3-butadiene ND ug/L 06/13/14 03:23 87-68-306/11/14 16:018.3 1
Hexachlorobenzene ND ug/L 06/13/14 03:23 118-74-106/11/14 16:018.3 1
Hexachlorocyclopentadiene ND ug/L 06/13/14 03:23 77-47-406/11/14 16:0116.7 1
Hexachloroethane ND ug/L 06/13/14 03:23 67-72-106/11/14 16:018.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/14 03:23 193-39-506/11/14 16:018.3 1
Isophorone ND ug/L 06/13/14 03:23 78-59-106/11/14 16:0116.7 1
Naphthalene ND ug/L 06/13/14 03:23 91-20-306/11/14 16:018.3 1
Nitrobenzene ND ug/L 06/13/14 03:23 98-95-306/11/14 16:018.3 1
2-Nitrophenol ND ug/L 06/13/14 03:23 88-75-506/11/14 16:018.3 1
4-Nitrophenol ND ug/L 06/13/14 03:23 100-02-706/11/14 16:0183.3 1
N-Nitrosodimethylamine ND ug/L 06/13/14 03:23 62-75-906/11/14 16:018.3 1
N-Nitroso-di-n-propylamine ND ug/L 06/13/14 03:23 621-64-706/11/14 16:018.3 1
N-Nitrosodiphenylamine ND ug/L 06/13/14 03:23 86-30-606/11/14 16:0116.7 1
Pentachlorophenol ND ug/L 06/13/14 03:23 87-86-506/11/14 16:0116.7 1
Phenanthrene ND ug/L 06/13/14 03:23 85-01-806/11/14 16:018.3 1
Phenol ND ug/L 06/13/14 03:23 108-95-206/11/14 16:018.3 1
Pyrene ND ug/L 06/13/14 03:23 129-00-006/11/14 16:018.3 1
1,2,4-Trichlorobenzene ND ug/L 06/13/14 03:23 120-82-106/11/14 16:018.3 1
2,4,6-Trichlorophenol ND ug/L 06/13/14 03:23 88-06-206/11/14 16:0116.7 1
Surrogates
Nitrobenzene-d5 (S)69 %06/13/14 03:23 4165-60-006/11/14 16:0110-120 1
2-Fluorobiphenyl (S)77 %06/13/14 03:23 321-60-806/11/14 16:0115-120 1
Terphenyl-d14 (S)69 %06/13/14 03:23 1718-51-006/11/14 16:0111-131 1
Phenol-d6 (S)24 %06/13/14 03:23 13127-88-306/11/14 16:0110-120 1
2-Fluorophenol (S)40 %06/13/14 03:23 367-12-406/11/14 16:0110-120 1
2,4,6-Tribromophenol (S)77 %06/13/14 03:23 118-79-606/11/14 16:0110-137 1
Tentatively Identified Compounds
Oleic Acid 200 ug/L 06/13/14 03:23 112-80-1 N06/11/14 16:011
Unknown 11.9 ug/L 06/13/14 03:23 N06/11/14 16:011
Unknown 248 ug/L 06/13/14 03:23 N06/11/14 16:011
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol ND ug/L 06/12/14 23:24 75-85-41001
tert-Amylmethyl ether ND ug/L 06/12/14 23:24 994-05-810.0 1
Benzene ND ug/L 06/12/14 23:24 71-43-20.50 1
Bromobenzene ND ug/L 06/12/14 23:24 108-86-10.50 1
Bromochloromethane ND ug/L 06/12/14 23:24 74-97-50.50 1
Bromodichloromethane ND ug/L 06/12/14 23:24 75-27-40.50 1
Bromoform ND ug/L 06/12/14 23:24 75-25-20.50 1
Bromomethane ND ug/L 06/12/14 23:24 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 06/12/14 23:24 75-65-010.0 1
n-Butylbenzene ND ug/L 06/12/14 23:24 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/12/14 23:24 135-98-80.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-17 Lab ID:92204797010 Collected:06/10/14 11:10 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
tert-Butylbenzene ND ug/L 06/12/14 23:24 98-06-60.50 1
tert-Butyl Formate ND ug/L 06/12/14 23:24 762-75-420.0 1
Carbon tetrachloride ND ug/L 06/12/14 23:24 56-23-50.50 1
Chlorobenzene ND ug/L 06/12/14 23:24 108-90-70.50 1
Chloroethane ND ug/L 06/12/14 23:24 75-00-31.0 1
Chloroform ND ug/L 06/12/14 23:24 67-66-30.50 1
Chloromethane ND ug/L 06/12/14 23:24 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/12/14 23:24 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/12/14 23:24 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/14 23:24 96-12-81.0 1
Dibromochloromethane ND ug/L 06/12/14 23:24 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/14 23:24 106-93-40.50 1
Dibromomethane ND ug/L 06/12/14 23:24 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/12/14 23:24 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/12/14 23:24 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/12/14 23:24 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/12/14 23:24 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/12/14 23:24 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/12/14 23:24 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/12/14 23:24 75-35-40.50 1
cis-1,2-Dichloroethene 4.8 ug/L 06/12/14 23:24 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/12/14 23:24 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/12/14 23:24 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/12/14 23:24 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/12/14 23:24 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/12/14 23:24 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/12/14 23:24 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/12/14 23:24 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/12/14 23:24 108-20-30.50 1
Ethanol ND ug/L 06/12/14 23:24 64-17-52001
Ethylbenzene ND ug/L 06/12/14 23:24 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 06/12/14 23:24 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 06/12/14 23:24 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/12/14 23:24 98-82-80.50 1
Methylene Chloride ND ug/L 06/12/14 23:24 75-09-22.0 1
Methyl-tert-butyl ether 1.2 ug/L 06/12/14 23:24 1634-04-40.50 1
Naphthalene ND ug/L 06/12/14 23:24 91-20-32.0 1
n-Propylbenzene ND ug/L 06/12/14 23:24 103-65-10.50 1
Styrene ND ug/L 06/12/14 23:24 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/14 23:24 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/14 23:24 79-34-50.50 1
Tetrachloroethene 8.2 ug/L 06/12/14 23:24 127-18-40.50 1
Toluene ND ug/L 06/12/14 23:24 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/12/14 23:24 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/12/14 23:24 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/12/14 23:24 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/12/14 23:24 79-00-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-17 Lab ID:92204797010 Collected:06/10/14 11:10 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Trichloroethene 9.8 ug/L 06/12/14 23:24 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/12/14 23:24 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/12/14 23:24 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/12/14 23:24 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/12/14 23:24 108-67-80.50 1
Vinyl chloride ND ug/L 06/12/14 23:24 75-01-41.0 1
m&p-Xylene ND ug/L 06/12/14 23:24 179601-23-11.0 1
o-Xylene ND ug/L 06/12/14 23:24 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)95 %06/12/14 23:24 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %06/12/14 23:24 460-00-470-130 1
Toluene-d8 (S)100 %06/12/14 23:24 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-18 Lab ID:92204797011 Collected:06/10/14 10:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 06/18/14 15:36 N206/16/14 14:451001
Aliphatic (C19-C36)ND ug/L 06/18/14 15:36 N206/16/14 14:451001
Aromatic (C11-C22)ND ug/L 06/18/14 15:36 N206/16/14 14:451001
Surrogates
Nonatriacontane (S)62 %06/18/14 15:36 7194-86-706/16/14 14:4540-140 1
o-Terphenyl (S)70 %06/18/14 15:36 84-15-106/16/14 14:4540-140 1
2-Fluorobiphenyl (S)82 %06/18/14 15:36 321-60-806/16/14 14:4540-140 1
2-Bromonaphthalene (S)87 %06/18/14 15:36 580-13-206/16/14 14:4540-140 1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 06/18/14 21:55 N250.0 1
Aliphatic (C09-C12)ND ug/L 06/18/14 21:55 N250.0 1
Aromatic (C09-C10)ND ug/L 06/18/14 21:55 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)120 %06/18/14 21:55 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)106 %06/18/14 21:55 460-00-470-130 1
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 06/17/14 01:28 83-32-906/11/14 16:015.0 1
Acenaphthylene ND ug/L 06/17/14 01:28 208-96-806/11/14 16:015.0 1
Anthracene ND ug/L 06/17/14 01:28 120-12-706/11/14 16:015.0 1
Benzo(a)anthracene ND ug/L 06/17/14 01:28 56-55-306/11/14 16:015.0 1
Benzo(a)pyrene ND ug/L 06/17/14 01:28 50-32-806/11/14 16:015.0 1
Benzo(b)fluoranthene ND ug/L 06/17/14 01:28 205-99-206/11/14 16:015.0 1
Benzo(g,h,i)perylene ND ug/L 06/17/14 01:28 191-24-206/11/14 16:015.0 1
Benzo(k)fluoranthene ND ug/L 06/17/14 01:28 207-08-906/11/14 16:015.0 1
4-Bromophenylphenyl ether ND ug/L 06/17/14 01:28 101-55-306/11/14 16:015.0 1
Butylbenzylphthalate ND ug/L 06/17/14 01:28 85-68-706/11/14 16:015.0 1
4-Chloro-3-methylphenol ND ug/L 06/17/14 01:28 59-50-706/11/14 16:015.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/17/14 01:28 111-91-106/11/14 16:0110.0 1
bis(2-Chloroethyl) ether ND ug/L 06/17/14 01:28 111-44-406/11/14 16:015.0 1
bis(2-Chloroisopropyl) ether ND ug/L 06/17/14 01:28 108-60-106/11/14 16:015.0 1
2-Chloronaphthalene ND ug/L 06/17/14 01:28 91-58-706/11/14 16:015.0 1
2-Chlorophenol ND ug/L 06/17/14 01:28 95-57-806/11/14 16:015.0 1
4-Chlorophenylphenyl ether ND ug/L 06/17/14 01:28 7005-72-306/11/14 16:015.0 1
Chrysene ND ug/L 06/17/14 01:28 218-01-906/11/14 16:015.0 1
Dibenz(a,h)anthracene ND ug/L 06/17/14 01:28 53-70-306/11/14 16:015.0 1
3,3'-Dichlorobenzidine ND ug/L 06/17/14 01:28 91-94-106/11/14 16:0125.0 1
2,4-Dichlorophenol ND ug/L 06/17/14 01:28 120-83-206/11/14 16:015.0 1
Diethylphthalate ND ug/L 06/17/14 01:28 84-66-206/11/14 16:015.0 1
2,4-Dimethylphenol ND ug/L 06/17/14 01:28 105-67-906/11/14 16:0110.0 1
Dimethylphthalate ND ug/L 06/17/14 01:28 131-11-306/11/14 16:015.0 1
Di-n-butylphthalate ND ug/L 06/17/14 01:28 84-74-206/11/14 16:015.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/17/14 01:28 534-52-106/11/14 16:0120.0 1
2,4-Dinitrophenol ND ug/L 06/17/14 01:28 51-28-506/11/14 16:0150.0 1
2,4-Dinitrotoluene ND ug/L 06/17/14 01:28 121-14-206/11/14 16:015.0 1
2,6-Dinitrotoluene ND ug/L 06/17/14 01:28 606-20-206/11/14 16:015.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-18 Lab ID:92204797011 Collected:06/10/14 10:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 06/17/14 01:28 117-84-006/11/14 16:015.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/17/14 01:28 117-81-706/11/14 16:015.0 1
Fluoranthene ND ug/L 06/17/14 01:28 206-44-006/11/14 16:015.0 1
Fluorene ND ug/L 06/17/14 01:28 86-73-706/11/14 16:015.0 1
Hexachloro-1,3-butadiene ND ug/L 06/17/14 01:28 87-68-306/11/14 16:015.0 1
Hexachlorobenzene ND ug/L 06/17/14 01:28 118-74-106/11/14 16:015.0 1
Hexachlorocyclopentadiene ND ug/L 06/17/14 01:28 77-47-406/11/14 16:0110.0 1
Hexachloroethane ND ug/L 06/17/14 01:28 67-72-106/11/14 16:015.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/17/14 01:28 193-39-506/11/14 16:015.0 1
Isophorone ND ug/L 06/17/14 01:28 78-59-106/11/14 16:0110.0 1
Naphthalene ND ug/L 06/17/14 01:28 91-20-306/11/14 16:015.0 1
Nitrobenzene ND ug/L 06/17/14 01:28 98-95-306/11/14 16:015.0 1
2-Nitrophenol ND ug/L 06/17/14 01:28 88-75-506/11/14 16:015.0 1
4-Nitrophenol ND ug/L 06/17/14 01:28 100-02-706/11/14 16:0150.0 1
N-Nitrosodimethylamine ND ug/L 06/17/14 01:28 62-75-906/11/14 16:015.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/17/14 01:28 621-64-706/11/14 16:015.0 1
N-Nitrosodiphenylamine ND ug/L 06/17/14 01:28 86-30-606/11/14 16:0110.0 1
Pentachlorophenol ND ug/L 06/17/14 01:28 87-86-506/11/14 16:0110.0 1
Phenanthrene ND ug/L 06/17/14 01:28 85-01-806/11/14 16:015.0 1
Phenol ND ug/L 06/17/14 01:28 108-95-206/11/14 16:015.0 1
Pyrene ND ug/L 06/17/14 01:28 129-00-006/11/14 16:015.0 1
1,2,4-Trichlorobenzene ND ug/L 06/17/14 01:28 120-82-106/11/14 16:015.0 1
2,4,6-Trichlorophenol ND ug/L 06/17/14 01:28 88-06-206/11/14 16:0110.0 1
Surrogates
Nitrobenzene-d5 (S)75 %06/17/14 01:28 4165-60-006/11/14 16:0110-120 1
2-Fluorobiphenyl (S)84 %06/17/14 01:28 321-60-806/11/14 16:0115-120 1
Terphenyl-d14 (S)97 %06/17/14 01:28 1718-51-006/11/14 16:0111-131 1
Phenol-d6 (S)32 %06/17/14 01:28 13127-88-306/11/14 16:0110-120 1
2-Fluorophenol (S)45 %06/17/14 01:28 367-12-406/11/14 16:0110-120 1
2,4,6-Tribromophenol (S)82 %06/17/14 01:28 118-79-606/11/14 16:0110-137 1
Tentatively Identified Compounds
Unknown 7.7 ug/L 06/17/14 01:28 N06/11/14 16:011
6200B MSV Analytical Method: SM 6200B
tert-Amyl Alcohol ND ug/L 06/12/14 23:41 75-85-41001
tert-Amylmethyl ether ND ug/L 06/12/14 23:41 994-05-810.0 1
Benzene ND ug/L 06/12/14 23:41 71-43-20.50 1
Bromobenzene ND ug/L 06/12/14 23:41 108-86-10.50 1
Bromochloromethane ND ug/L 06/12/14 23:41 74-97-50.50 1
Bromodichloromethane ND ug/L 06/12/14 23:41 75-27-40.50 1
Bromoform ND ug/L 06/12/14 23:41 75-25-20.50 1
Bromomethane ND ug/L 06/12/14 23:41 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 06/12/14 23:41 75-65-010.0 1
n-Butylbenzene ND ug/L 06/12/14 23:41 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/12/14 23:41 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/12/14 23:41 98-06-60.50 1
tert-Butyl Formate ND ug/L 06/12/14 23:41 762-75-420.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-18 Lab ID:92204797011 Collected:06/10/14 10:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Carbon tetrachloride ND ug/L 06/12/14 23:41 56-23-50.50 1
Chlorobenzene ND ug/L 06/12/14 23:41 108-90-70.50 1
Chloroethane ND ug/L 06/12/14 23:41 75-00-31.0 1
Chloroform ND ug/L 06/12/14 23:41 67-66-30.50 1
Chloromethane ND ug/L 06/12/14 23:41 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/12/14 23:41 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/12/14 23:41 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/12/14 23:41 96-12-81.0 1
Dibromochloromethane ND ug/L 06/12/14 23:41 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/12/14 23:41 106-93-40.50 1
Dibromomethane ND ug/L 06/12/14 23:41 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/12/14 23:41 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/12/14 23:41 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/12/14 23:41 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/12/14 23:41 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/12/14 23:41 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/12/14 23:41 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/12/14 23:41 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/12/14 23:41 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/12/14 23:41 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/12/14 23:41 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/12/14 23:41 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/12/14 23:41 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/12/14 23:41 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/12/14 23:41 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/12/14 23:41 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/12/14 23:41 108-20-30.50 1
Ethanol ND ug/L 06/12/14 23:41 64-17-52001
Ethylbenzene ND ug/L 06/12/14 23:41 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 06/12/14 23:41 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 06/12/14 23:41 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/12/14 23:41 98-82-80.50 1
Methylene Chloride ND ug/L 06/12/14 23:41 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/12/14 23:41 1634-04-40.50 1
Naphthalene ND ug/L 06/12/14 23:41 91-20-32.0 1
n-Propylbenzene ND ug/L 06/12/14 23:41 103-65-10.50 1
Styrene ND ug/L 06/12/14 23:41 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/12/14 23:41 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/12/14 23:41 79-34-50.50 1
Tetrachloroethene 2.7 ug/L 06/12/14 23:41 127-18-40.50 1
Toluene ND ug/L 06/12/14 23:41 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/12/14 23:41 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/12/14 23:41 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/12/14 23:41 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/12/14 23:41 79-00-50.50 1
Trichloroethene ND ug/L 06/12/14 23:41 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/12/14 23:41 75-69-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-18 Lab ID:92204797011 Collected:06/10/14 10:00 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
1,2,3-Trichloropropane ND ug/L 06/12/14 23:41 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/12/14 23:41 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/12/14 23:41 108-67-80.50 1
Vinyl chloride ND ug/L 06/12/14 23:41 75-01-41.0 1
m&p-Xylene ND ug/L 06/12/14 23:41 179601-23-11.0 1
o-Xylene ND ug/L 06/12/14 23:41 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %06/12/14 23:41 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %06/12/14 23:41 460-00-470-130 1
Toluene-d8 (S)99 %06/12/14 23:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-4 Lab ID:92204797012 Collected:06/10/14 15:55 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium 23.6 ug/L 06/13/14 19:18 7440-47-306/12/14 15:105.0 1
Lead ND ug/L 06/13/14 19:18 7439-92-106/12/14 15:105.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-7 Lab ID:92204797013 Collected:06/10/14 15:50 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium ND ug/L 06/13/14 19:21 7440-47-306/12/14 15:105.0 1
Lead ND ug/L 06/13/14 19:21 7439-92-106/12/14 15:105.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-8 Lab ID:92204797014 Collected:06/10/14 15:37 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium ND ug/L 06/13/14 19:24 7440-47-306/12/14 15:105.0 1
Lead ND ug/L 06/13/14 19:24 7439-92-106/12/14 15:105.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-9 Lab ID:92204797015 Collected:06/10/14 15:41 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium 11.5 ug/L 06/13/14 19:37 7440-47-306/12/14 15:105.0 1
Lead ND ug/L 06/13/14 19:37 7439-92-106/12/14 15:105.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-11 Lab ID:92204797016 Collected:06/10/14 15:45 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium ND ug/L 06/13/14 19:40 7440-47-306/12/14 15:105.0 1
Lead ND ug/L 06/13/14 19:40 7439-92-106/12/14 15:105.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-16 Lab ID:92204797017 Collected:06/10/14 15:45 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium 10.9 ug/L 06/13/14 19:43 7440-47-306/12/14 15:105.0 1
Lead ND ug/L 06/13/14 19:43 7439-92-106/12/14 15:105.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-17 Lab ID:92204797018 Collected:06/10/14 15:33 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium ND ug/L 06/13/14 19:47 7440-47-306/12/14 15:105.0 1
Lead ND ug/L 06/13/14 19:47 7439-92-106/12/14 15:105.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Sample:MW-18 Lab ID:92204797019 Collected:06/10/14 15:28 Received:06/10/14 17:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Chromium ND ug/L 06/13/14 19:50 7440-47-306/12/14 15:105.0 1
Lead ND ug/L 06/13/14 19:50 7439-92-106/12/14 15:105.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/8229
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples:92204797001, 92204797002, 92204797004, 92204797005, 92204797006, 92204797007, 92204797008,
92204797009, 92204797010, 92204797011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1222141
Associated Lab Samples:92204797001, 92204797002, 92204797004, 92204797005, 92204797006, 92204797007, 92204797008,
92204797009, 92204797010, 92204797011
Matrix:Water
Analyzed
Aliphatic (C05-C08)ug/L ND 50.0 N206/18/14 17:40
Aliphatic (C09-C12)ug/L ND 50.0 N206/18/14 17:40
Aromatic (C09-C10)ug/L ND 50.0 N206/18/14 17:40
4-Bromofluorobenzene (FID) (S)%129 70-130 06/18/14 17:40
4-Bromofluorobenzene (PID) (S)%115 70-130 06/18/14 17:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1222142LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1222143
Aliphatic (C05-C08)ug/L 262 N23008770-13091274 5 25
Aliphatic (C09-C12)ug/L 248 N23008330-13090269 8 25
Aromatic (C09-C10)ug/L 87.0 N21008770-1309089.9 3 25
4-Bromofluorobenzene (FID) (S)%123 70-130124
4-Bromofluorobenzene (PID) (S)%109 70-130110
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/8242
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples:92204797003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1224578
Associated Lab Samples:92204797003
Matrix:Water
Analyzed
Aliphatic (C05-C08)ug/L ND 50.0 N206/23/14 17:20
Aliphatic (C09-C12)ug/L ND 50.0 N206/23/14 17:20
Aromatic (C09-C10)ug/L ND 50.0 N206/23/14 17:20
4-Bromofluorobenzene (FID) (S)%102 70-130 06/23/14 17:20
4-Bromofluorobenzene (PID) (S)%101 70-130 06/23/14 17:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1224579LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1224580
Aliphatic (C05-C08)ug/L 290 N23009770-130101302 4 25
Aliphatic (C09-C12)ug/L 281 N23009430-130102305 8 25
Aromatic (C09-C10)ug/L 89.2 N21008970-1309392.6 4 25
4-Bromofluorobenzene (FID) (S)%103 70-13099
4-Bromofluorobenzene (PID) (S)%102 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/16185
EPA 3010
EPA 6010
6010 MET
Associated Lab Samples:92204797001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1218634
Associated Lab Samples:92204797001
Matrix:Water
Analyzed
Chromium ug/L ND 5.0 06/12/14 18:27
Lead ug/L ND 5.0 06/12/14 18:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1218635LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium ug/L 477500 95 80-120
Lead ug/L 496500 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1218636MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92204440001
1218637
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chromium ug/L 500 94 75-12596 1500ND477484
Lead ug/L 500 97 75-12598 1500ND485492
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/16198
EPA 3010
EPA 6010
6010 MET
Associated Lab Samples:92204797002, 92204797012, 92204797013, 92204797014, 92204797015, 92204797016, 92204797017,
92204797018, 92204797019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1219986
Associated Lab Samples:92204797002, 92204797012, 92204797013, 92204797014, 92204797015, 92204797016, 92204797017,
92204797018, 92204797019
Matrix:Water
Analyzed
Chromium ug/L ND 5.0 06/13/14 18:59
Lead ug/L ND 5.0 06/13/14 18:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1219987LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium ug/L 478500 96 80-120
Lead ug/L 467500 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1219992MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92204755003
1219993
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chromium ug/L 500 92 75-12592 0500ND462462
Lead ug/L 500 89 75-12590 1500ND445448
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/27183
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92204797001, 92204797002, 92204797003, 92204797004, 92204797005, 92204797006, 92204797007,
92204797008, 92204797009, 92204797010, 92204797011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1219831
Associated Lab Samples:92204797001, 92204797002, 92204797003, 92204797004, 92204797005, 92204797006, 92204797007,
92204797008, 92204797009, 92204797010, 92204797011
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 06/12/14 20:22
1,1,1-Trichloroethane ug/L ND 0.50 06/12/14 20:22
1,1,2,2-Tetrachloroethane ug/L ND 0.50 06/12/14 20:22
1,1,2-Trichloroethane ug/L ND 0.50 06/12/14 20:22
1,1-Dichloroethane ug/L ND 0.50 06/12/14 20:22
1,1-Dichloroethene ug/L ND 0.50 06/12/14 20:22
1,1-Dichloropropene ug/L ND 0.50 06/12/14 20:22
1,2,3-Trichlorobenzene ug/L ND 2.0 06/12/14 20:22
1,2,3-Trichloropropane ug/L ND 0.50 06/12/14 20:22
1,2,4-Trichlorobenzene ug/L ND 2.0 06/12/14 20:22
1,2,4-Trimethylbenzene ug/L ND 0.50 06/12/14 20:22
1,2-Dibromo-3-chloropropane ug/L ND 1.0 06/12/14 20:22
1,2-Dibromoethane (EDB)ug/L ND 0.50 06/12/14 20:22
1,2-Dichlorobenzene ug/L ND 0.50 06/12/14 20:22
1,2-Dichloroethane ug/L ND 0.50 06/12/14 20:22
1,2-Dichloropropane ug/L ND 0.50 06/12/14 20:22
1,3,5-Trimethylbenzene ug/L ND 0.50 06/12/14 20:22
1,3-Dichlorobenzene ug/L ND 0.50 06/12/14 20:22
1,3-Dichloropropane ug/L ND 0.50 06/12/14 20:22
1,4-Dichlorobenzene ug/L ND 0.50 06/12/14 20:22
2,2-Dichloropropane ug/L ND 0.50 06/12/14 20:22
2-Chlorotoluene ug/L ND 0.50 06/12/14 20:22
4-Chlorotoluene ug/L ND 0.50 06/12/14 20:22
Benzene ug/L ND 0.50 06/12/14 20:22
Bromobenzene ug/L ND 0.50 06/12/14 20:22
Bromochloromethane ug/L ND 0.50 06/12/14 20:22
Bromodichloromethane ug/L ND 0.50 06/12/14 20:22
Bromoform ug/L ND 0.50 06/12/14 20:22
Bromomethane ug/L ND 5.0 06/12/14 20:22
Carbon tetrachloride ug/L ND 0.50 06/12/14 20:22
Chlorobenzene ug/L ND 0.50 06/12/14 20:22
Chloroethane ug/L ND 1.0 06/12/14 20:22
Chloroform ug/L ND 0.50 06/12/14 20:22
Chloromethane ug/L ND 1.0 06/12/14 20:22
cis-1,2-Dichloroethene ug/L ND 0.50 06/12/14 20:22
cis-1,3-Dichloropropene ug/L ND 0.50 06/12/14 20:22
Dibromochloromethane ug/L ND 0.50 06/12/14 20:22
Dibromomethane ug/L ND 0.50 06/12/14 20:22
Dichlorodifluoromethane ug/L ND 0.50 06/12/14 20:22
Diisopropyl ether ug/L ND 0.50 06/12/14 20:22
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1219831
Associated Lab Samples:92204797001, 92204797002, 92204797003, 92204797004, 92204797005, 92204797006, 92204797007,
92204797008, 92204797009, 92204797010, 92204797011
Matrix:Water
Analyzed
Ethanol ug/L ND 200 06/12/14 20:22
Ethyl-tert-butyl ether ug/L ND 10.0 06/12/14 20:22
Ethylbenzene ug/L ND 0.50 06/12/14 20:22
Hexachloro-1,3-butadiene ug/L ND 2.0 06/12/14 20:22
Isopropylbenzene (Cumene)ug/L ND 0.50 06/12/14 20:22
m&p-Xylene ug/L ND 1.0 06/12/14 20:22
Methyl-tert-butyl ether ug/L ND 0.50 06/12/14 20:22
Methylene Chloride ug/L ND 2.0 06/12/14 20:22
n-Butylbenzene ug/L ND 0.50 06/12/14 20:22
n-Propylbenzene ug/L ND 0.50 06/12/14 20:22
Naphthalene ug/L ND 2.0 06/12/14 20:22
o-Xylene ug/L ND 0.50 06/12/14 20:22
sec-Butylbenzene ug/L ND 0.50 06/12/14 20:22
Styrene ug/L ND 0.50 06/12/14 20:22
tert-Amyl Alcohol ug/L ND 100 06/12/14 20:22
tert-Amylmethyl ether ug/L ND 10.0 06/12/14 20:22
tert-Butyl Alcohol ug/L ND 10.0 06/12/14 20:22
tert-Butyl Formate ug/L ND 20.0 06/12/14 20:22
tert-Butylbenzene ug/L ND 0.50 06/12/14 20:22
Tetrachloroethene ug/L ND 0.50 06/12/14 20:22
Toluene ug/L ND 0.50 06/12/14 20:22
trans-1,2-Dichloroethene ug/L ND 0.50 06/12/14 20:22
trans-1,3-Dichloropropene ug/L ND 0.50 06/12/14 20:22
Trichloroethene ug/L ND 0.50 06/12/14 20:22
Trichlorofluoromethane ug/L ND 1.0 06/12/14 20:22
Vinyl chloride ug/L ND 1.0 06/12/14 20:22
1,2-Dichloroethane-d4 (S)%97 70-130 06/12/14 20:22
4-Bromofluorobenzene (S)%99 70-130 06/12/14 20:22
Toluene-d8 (S)%99 70-130 06/12/14 20:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1219832LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 60.150 120 60-140
1,1,1-Trichloroethane ug/L 53.750 107 60-140
1,1,2,2-Tetrachloroethane ug/L 54.250 108 60-140
1,1,2-Trichloroethane ug/L 55.050 110 60-140
1,1-Dichloroethane ug/L 49.750 99 60-140
1,1-Dichloroethene ug/L 54.850 110 60-140
1,1-Dichloropropene ug/L 53.850 108 60-140
1,2,3-Trichlorobenzene ug/L 56.850 114 60-140
1,2,3-Trichloropropane ug/L 54.850 110 60-140
1,2,4-Trichlorobenzene ug/L 55.650 111 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1219832LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/L 57.350 115 60-140
1,2-Dibromo-3-chloropropane ug/L 59.450 119 60-140
1,2-Dibromoethane (EDB)ug/L 56.750 113 60-140
1,2-Dichlorobenzene ug/L 57.350 115 60-140
1,2-Dichloroethane ug/L 51.450 103 60-140
1,2-Dichloropropane ug/L 53.850 108 60-140
1,3,5-Trimethylbenzene ug/L 56.150 112 60-140
1,3-Dichlorobenzene ug/L 55.750 111 60-140
1,3-Dichloropropane ug/L 55.050 110 60-140
1,4-Dichlorobenzene ug/L 54.750 109 60-140
2,2-Dichloropropane ug/L 54.250 108 60-140
2-Chlorotoluene ug/L 55.350 111 60-140
4-Chlorotoluene ug/L 54.450 109 60-140
Benzene ug/L 56.650 113 60-140
Bromobenzene ug/L 55.450 111 60-140
Bromochloromethane ug/L 52.150 104 60-140
Bromodichloromethane ug/L 59.550 119 60-140
Bromoform ug/L 49.250 98 60-140
Bromomethane ug/L 32.650 65 60-140
Carbon tetrachloride ug/L 58.350 117 60-140
Chlorobenzene ug/L 56.050 112 60-140
Chloroethane ug/L 42.250 84 60-140
Chloroform ug/L 55.950 112 60-140
Chloromethane ug/L 47.450 95 60-140
cis-1,2-Dichloroethene ug/L 56.850 114 60-140
cis-1,3-Dichloropropene ug/L 59.350 119 60-140
Dibromochloromethane ug/L 51.450 103 60-140
Dibromomethane ug/L 56.750 113 60-140
Dichlorodifluoromethane ug/L 52.750 105 60-140
Diisopropyl ether ug/L 52.350 105 60-140
Ethanol ug/L 24002000 120 60-140
Ethyl-tert-butyl ether ug/L 97.4100 97 60-140
Ethylbenzene ug/L 54.650 109 60-140
Hexachloro-1,3-butadiene ug/L 56.650 113 60-140
Isopropylbenzene (Cumene)ug/L 58.750 117 60-140
m&p-Xylene ug/L 112100 112 60-140
Methyl-tert-butyl ether ug/L 55.450 111 60-140
Methylene Chloride ug/L 53.550 107 60-140
n-Butylbenzene ug/L 57.250 114 60-140
n-Propylbenzene ug/L 56.150 112 60-140
Naphthalene ug/L 57.050 114 60-140
o-Xylene ug/L 56.650 113 60-140
sec-Butylbenzene ug/L 56.250 112 60-140
Styrene ug/L 59.250 118 60-140
tert-Amyl Alcohol ug/L 12801000 128 60-140
tert-Amylmethyl ether ug/L 124100 124 60-140
tert-Butyl Alcohol ug/L 631500 126 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1219832LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butyl Formate ug/L 439400 110 60-140
tert-Butylbenzene ug/L 57.150 114 60-140
Tetrachloroethene ug/L 54.250 108 60-140
Toluene ug/L 52.950 106 60-140
trans-1,2-Dichloroethene ug/L 53.950 108 60-140
trans-1,3-Dichloropropene ug/L 49.450 99 60-140
Trichloroethene ug/L 52.450 105 60-140
Trichlorofluoromethane ug/L 48.350 97 60-140
Vinyl chloride ug/L 52.850 106 60-140
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1222293MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92204797004
1222294
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 101 60-140105 420ND20.2 21.0
1,1,1-Trichloroethane ug/L 20 108 60-140112 420ND21.6 22.4
1,1,2,2-Tetrachloroethane ug/L 20 102 60-140105 420ND20.3 21.1
1,1,2-Trichloroethane ug/L 20 105 60-140107 220ND21.0 21.5
1,1-Dichloroethane ug/L 20 105 60-140108 220ND21.0 21.5
1,1-Dichloroethene ug/L 20 117 60-140120 320ND23.4 24.1
1,1-Dichloropropene ug/L 20 113 60-140117 320ND22.7 23.3
1,2,3-Trichlorobenzene ug/L 20 99 60-140103 420ND19.7 20.6
1,2,3-Trichloropropane ug/L 20 102 60-140106 420ND20.4 21.2
1,2,4-Trichlorobenzene ug/L 20 100 60-140101 120ND20.1 20.2
1,2,4-Trimethylbenzene ug/L 20 108 60-140110 220ND21.8 22.2
1,2-Dibromo-3-chloropropane ug/L 20 100 60-140102 220ND20.0 20.4
1,2-Dibromoethane (EDB)ug/L 20 104 60-140108 420ND20.8 21.6
1,2-Dichlorobenzene ug/L 20 105 60-140107 120ND21.1 21.3
1,2-Dichloroethane ug/L 20 104 60-140106 220ND20.8 21.2
1,2-Dichloropropane ug/L 20 105 60-140108 220ND21.1 21.6
1,3,5-Trimethylbenzene ug/L 20 108 60-140110 220ND21.5 22.1
1,3-Dichlorobenzene ug/L 20 103 60-140104 120ND20.6 20.8
1,3-Dichloropropane ug/L 20 103 60-140107 420ND20.6 21.3
1,4-Dichlorobenzene ug/L 20 103 60-140105 220ND20.5 21.0
2,2-Dichloropropane ug/L 20 109 60-140113 420ND21.7 22.7
2-Chlorotoluene ug/L 20 105 60-140109 420ND20.9 21.8
4-Chlorotoluene ug/L 20 102 60-140105 320ND20.5 21.0
Benzene ug/L 20 112 60-140113 120ND22.5 22.8
Bromobenzene ug/L 20 106 60-140108 320ND21.1 21.7
Bromochloromethane ug/L 20 109 60-140114 420ND21.8 22.7
Bromodichloromethane ug/L 20 105 60-140107 220ND21.0 21.4
Bromoform ug/L 20 98 60-140102 420ND19.5 20.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1222293MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92204797004
1222294
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Bromomethane ug/L 20 112 60-140118 620ND22.3 23.6
Carbon tetrachloride ug/L 20 110 60-140113 320ND22.1 22.7
Chlorobenzene ug/L 20 103 60-140107 520ND20.5 21.5
Chloroethane ug/L 20 109 60-140117 820ND21.7 23.5
Chloroform ug/L 20 108 60-140112 320ND21.6 22.3
Chloromethane ug/L 20 107 60-140110 420ND21.3 22.1
cis-1,2-Dichloroethene ug/L 20 110 60-140112 220ND22.0 22.5
cis-1,3-Dichloropropene ug/L 20 107 60-140109 120ND21.4 21.7
Dibromochloromethane ug/L 20 97 60-140101 420ND19.4 20.1
Dibromomethane ug/L 20 103 60-140106 320ND20.6 21.3
Dichlorodifluoromethane ug/L 20 119 60-140121 220ND23.8 24.2
Diisopropyl ether ug/L 20 105 60-140109 420ND21.0 21.8
Ethanol ug/L 800 100 60-140107 6800ND801854
Ethyl-tert-butyl ether ug/L 40 95 60-14098 340ND37.8 39.1
Ethylbenzene ug/L 20 103 60-140107 420ND20.7 21.5
Hexachloro-1,3-butadiene ug/L 20 97 60-140101 520ND19.3 20.2
Isopropylbenzene (Cumene)ug/L 20 109 60-140115 520ND21.7 22.9
m&p-Xylene ug/L 40 105 60-140109 340ND42.3 43.8
Methyl-tert-butyl ether ug/L 20 108 60-140109 120ND21.6 21.9
Methylene Chloride ug/L 20 98 60-140102 420ND19.5 20.4
n-Butylbenzene ug/L 20 106 60-140108 220ND21.2 21.6
n-Propylbenzene ug/L 20 108 60-140111 320ND21.7 22.3
Naphthalene ug/L 20 101 60-140103 120ND20.5 20.7
o-Xylene ug/L 20 103 60-140107 420ND20.7 21.6
sec-Butylbenzene ug/L 20 106 60-140108 220ND21.2 21.7
Styrene ug/L 20 110 60-140114 420ND21.9 22.8
tert-Amyl Alcohol ug/L 400 100 60-14099 1400ND398395
tert-Amylmethyl ether ug/L 40 110 60-140111 140ND43.8 44.5
tert-Butyl Alcohol ug/L M020016260-140166 3200ND324332
tert-Butyl Formate ug/L P51603060-14029 4160ND48.0 46.1
tert-Butylbenzene ug/L 20 107 60-140110 320ND21.3 21.9
Tetrachloroethene ug/L 20 107 60-140110 320ND21.7 22.3
Toluene ug/L 20 89 60-14091 220ND17.7 18.2
trans-1,2-Dichloroethene ug/L 20 105 60-140109 420ND20.9 21.7
trans-1,3-Dichloropropene ug/L 20 103 60-140106 320ND20.7 21.3
Trichloroethene ug/L 20 108 60-140111 220ND21.7 22.2
Trichlorofluoromethane ug/L 20 117 60-140120 320ND23.4 24.0
Vinyl chloride ug/L 20 133 60-140136 220ND26.5 27.1
1,2-Dichloroethane-d4 (S)%101 70-130100
4-Bromofluorobenzene (S)%99 70-130100
Toluene-d8 (S)%101 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/28221
EPA 625
EPA 625
625 MSS
Associated Lab Samples:92204797001, 92204797002, 92204797003, 92204797004, 92204797005, 92204797006, 92204797007,
92204797008, 92204797009, 92204797010, 92204797011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1219172
Associated Lab Samples:92204797001, 92204797002, 92204797003, 92204797004, 92204797005, 92204797006, 92204797007,
92204797008, 92204797009, 92204797010, 92204797011
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 06/12/14 19:29
2,4,6-Trichlorophenol ug/L ND 10.0 06/12/14 19:29
2,4-Dichlorophenol ug/L ND 5.0 06/12/14 19:29
2,4-Dimethylphenol ug/L ND 10.0 06/12/14 19:29
2,4-Dinitrophenol ug/L ND 50.0 06/12/14 19:29
2,4-Dinitrotoluene ug/L ND 5.0 06/12/14 19:29
2,6-Dinitrotoluene ug/L ND 5.0 06/12/14 19:29
2-Chloronaphthalene ug/L ND 5.0 06/12/14 19:29
2-Chlorophenol ug/L ND 5.0 06/12/14 19:29
2-Nitrophenol ug/L ND 5.0 06/12/14 19:29
3,3'-Dichlorobenzidine ug/L ND 25.0 06/12/14 19:29
4,6-Dinitro-2-methylphenol ug/L ND 20.0 06/12/14 19:29
4-Bromophenylphenyl ether ug/L ND 5.0 06/12/14 19:29
4-Chloro-3-methylphenol ug/L ND 5.0 06/12/14 19:29
4-Chlorophenylphenyl ether ug/L ND 5.0 06/12/14 19:29
4-Nitrophenol ug/L ND 50.0 06/12/14 19:29
Acenaphthene ug/L ND 5.0 06/12/14 19:29
Acenaphthylene ug/L ND 5.0 06/12/14 19:29
Anthracene ug/L ND 5.0 06/12/14 19:29
Benzo(a)anthracene ug/L ND 5.0 06/12/14 19:29
Benzo(a)pyrene ug/L ND 5.0 06/12/14 19:29
Benzo(b)fluoranthene ug/L ND 5.0 06/12/14 19:29
Benzo(g,h,i)perylene ug/L ND 5.0 06/12/14 19:29
Benzo(k)fluoranthene ug/L ND 5.0 06/12/14 19:29
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/12/14 19:29
bis(2-Chloroethyl) ether ug/L ND 5.0 06/12/14 19:29
bis(2-Chloroisopropyl) ether ug/L ND 5.0 06/12/14 19:29
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 06/12/14 19:29
Butylbenzylphthalate ug/L ND 5.0 06/12/14 19:29
Chrysene ug/L ND 5.0 06/12/14 19:29
Di-n-butylphthalate ug/L ND 5.0 06/12/14 19:29
Di-n-octylphthalate ug/L ND 5.0 06/12/14 19:29
Dibenz(a,h)anthracene ug/L ND 5.0 06/12/14 19:29
Diethylphthalate ug/L ND 5.0 06/12/14 19:29
Dimethylphthalate ug/L ND 5.0 06/12/14 19:29
Fluoranthene ug/L ND 5.0 06/12/14 19:29
Fluorene ug/L ND 5.0 06/12/14 19:29
Hexachloro-1,3-butadiene ug/L ND 5.0 06/12/14 19:29
Hexachlorobenzene ug/L ND 5.0 06/12/14 19:29
Hexachlorocyclopentadiene ug/L ND 10.0 06/12/14 19:29
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1219172
Associated Lab Samples:92204797001, 92204797002, 92204797003, 92204797004, 92204797005, 92204797006, 92204797007,
92204797008, 92204797009, 92204797010, 92204797011
Matrix:Water
Analyzed
Hexachloroethane ug/L ND 5.0 06/12/14 19:29
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 06/12/14 19:29
Isophorone ug/L ND 10.0 06/12/14 19:29
N-Nitroso-di-n-propylamine ug/L ND 5.0 06/12/14 19:29
N-Nitrosodimethylamine ug/L ND 5.0 06/12/14 19:29
N-Nitrosodiphenylamine ug/L ND 10.0 06/12/14 19:29
Naphthalene ug/L ND 5.0 06/12/14 19:29
Nitrobenzene ug/L ND 5.0 06/12/14 19:29
Pentachlorophenol ug/L ND 10.0 06/12/14 19:29
Phenanthrene ug/L ND 5.0 06/12/14 19:29
Phenol ug/L ND 5.0 06/12/14 19:29
Pyrene ug/L ND 5.0 06/12/14 19:29
2,4,6-Tribromophenol (S)%81 10-137 06/12/14 19:29
2-Fluorobiphenyl (S)%78 15-120 06/12/14 19:29
2-Fluorophenol (S)%42 10-120 06/12/14 19:29
Nitrobenzene-d5 (S)%67 10-120 06/12/14 19:29
Phenol-d6 (S)%26 10-120 06/12/14 19:29
Terphenyl-d14 (S)%88 11-131 06/12/14 19:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1219173LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 36.450 73 44-142
2,4,6-Trichlorophenol ug/L 41.650 83 37-144
2,4-Dichlorophenol ug/L 41.250 82 1-191
2,4-Dimethylphenol ug/L 40.050 80 32-119
2,4-Dinitrophenol ug/L 198250 79 1-181
2,4-Dinitrotoluene ug/L 53.150 106 39-139
2,6-Dinitrotoluene ug/L 51.250 102 50-158
2-Chloronaphthalene ug/L 41.050 82 60-118
2-Chlorophenol ug/L 38.850 78 23-134
2-Nitrophenol ug/L 41.850 84 29-182
3,3'-Dichlorobenzidine ug/L 95.0100 95 1-262
4,6-Dinitro-2-methylphenol ug/L 87.2100 87 1-181
4-Bromophenylphenyl ether ug/L 44.050 88 53-127
4-Chloro-3-methylphenol ug/L 85.9100 86 22-147
4-Chlorophenylphenyl ether ug/L 46.650 93 25-158
4-Nitrophenol ug/L 83.0250 33 1-132
Acenaphthene ug/L 41.550 83 47-145
Acenaphthylene ug/L 41.950 84 33-145
Anthracene ug/L 43.550 87 1-166
Benzo(a)anthracene ug/L 45.050 90 33-143
Benzo(a)pyrene ug/L 44.350 89 17-163
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1219173LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(b)fluoranthene ug/L 45.250 90 24-159
Benzo(g,h,i)perylene ug/L 46.350 93 1-219
Benzo(k)fluoranthene ug/L 44.050 88 11-162
bis(2-Chloroethoxy)methane ug/L 45.250 90 33-184
bis(2-Chloroethyl) ether ug/L 43.850 88 12-158
bis(2-Chloroisopropyl) ether ug/L 41.450 83 36-166
bis(2-Ethylhexyl)phthalate ug/L 48.150 96 8-158
Butylbenzylphthalate ug/L 47.050 94 1-152
Chrysene ug/L 45.450 91 17-168
Di-n-butylphthalate ug/L 47.350 95 1-118
Di-n-octylphthalate ug/L 46.250 92 4-146
Dibenz(a,h)anthracene ug/L 48.050 96 1-227
Diethylphthalate ug/L 45.650 91 1-114
Dimethylphthalate ug/L 44.750 89 1-112
Fluoranthene ug/L 44.950 90 26-137
Fluorene ug/L 44.550 89 59-121
Hexachloro-1,3-butadiene ug/L 36.350 73 24-116
Hexachlorobenzene ug/L 43.850 88 1-152
Hexachlorocyclopentadiene ug/L 35.050 70 25-150
Hexachloroethane ug/L 36.050 72 40-113
Indeno(1,2,3-cd)pyrene ug/L 37.050 74 1-171
Isophorone ug/L 51.350 103 21-196
N-Nitroso-di-n-propylamine ug/L 46.950 94 1-230
N-Nitrosodimethylamine ug/L 27.850 56 25-150
N-Nitrosodiphenylamine ug/L 45.850 92 25-150
Naphthalene ug/L 39.850 80 21-133
Nitrobenzene ug/L 47.750 95 35-180
Pentachlorophenol ug/L 82.9100 83 14-176
Phenanthrene ug/L 43.450 87 54-120
Phenol ug/L 19.950 40 5-112
Pyrene ug/L 42.150 84 52-115
2,4,6-Tribromophenol (S)%88 10-137
2-Fluorobiphenyl (S)%83 15-120
2-Fluorophenol (S)%46 10-120
Nitrobenzene-d5 (S)%77 10-120
Phenol-d6 (S)%32 10-120
Terphenyl-d14 (S)%88 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1219174MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92204797002
1219175
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 100 73 44-14269 5100ND72.6 69.0
2,4,6-Trichlorophenol ug/L 100 79 37-14475 4100ND78.6 75.2
2,4-Dichlorophenol ug/L 100 82 1-19176 9100ND82.3 75.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1219174MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92204797002
1219175
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2,4-Dimethylphenol ug/L 100 82 32-11978 5100ND81.9 77.9
2,4-Dinitrophenol ug/L 500 76 1-18177 0500ND381383
2,4-Dinitrotoluene ug/L 100 103 39-139104 1100ND103104
2,6-Dinitrotoluene ug/L 100 103 50-158102 2100ND103102
2-Chloronaphthalene ug/L 100 80 60-11876 4100ND79.7 76.3
2-Chlorophenol ug/L 100 78 23-13473 7100ND78.3 72.9
2-Nitrophenol ug/L 100 84 29-18276 10100ND84.3 76.0
3,3'-Dichlorobenzidine ug/L 200 85 1-26281 5200ND169162
4,6-Dinitro-2-methylphenol ug/L 200 86 1-18180 7200ND172160
4-Bromophenylphenyl ether ug/L 100 87 53-12781 7100ND86.9 81.2
4-Chloro-3-methylphenol ug/L 200 85 22-14785 0200ND170171
4-Chlorophenylphenyl ether ug/L 100 91 25-15888 3100ND91.0 88.4
4-Nitrophenol ug/L 500 50 1-13249 1500ND248247
Acenaphthene ug/L 100 82 47-14579 4100ND82.0 79.0
Acenaphthylene ug/L 100 81 33-14576 6100ND80.7 76.4
Anthracene ug/L 100 84 1-16681 4100ND84.2 81.1
Benzo(a)anthracene ug/L 100 85 33-14383 2100ND84.5 83.2
Benzo(a)pyrene ug/L 100 87 17-16382 6100ND87.0 82.1
Benzo(b)fluoranthene ug/L 100 83 24-15984 1100ND83.2 84.1
Benzo(g,h,i)perylene ug/L 100 87 1-21982 5100ND86.6 82.1
Benzo(k)fluoranthene ug/L 100 85 11-16278 8100ND84.6 78.0
bis(2-Chloroethoxy)methane ug/L 100 85 33-18482 4100ND85.3 81.7
bis(2-Chloroethyl) ether ug/L 100 85 12-15877 10100ND84.8 76.7
bis(2-Chloroisopropyl) ether ug/L 100 81 36-16675 7100ND81.0 75.2
bis(2-Ethylhexyl)phthalate ug/L 100 90 8-15888 2100ND90.5 88.3
Butylbenzylphthalate ug/L 100 87 1-15288 1100ND87.3 88.0
Chrysene ug/L 100 84 17-16883 1100ND83.9 83.5
Di-n-butylphthalate ug/L 100 91 1-11889 3100ND91.1 88.7
Di-n-octylphthalate ug/L 100 87 4-14685 2100ND87.1 85.1
Dibenz(a,h)anthracene ug/L 100 89 1-22786 3100ND88.8 85.8
Diethylphthalate ug/L 100 89 1-11489 0100ND88.6 88.5
Dimethylphthalate ug/L 100 88 1-11285 3100ND87.5 84.6
Fluoranthene ug/L 100 90 26-13784 6100ND89.5 84.5
Fluorene ug/L 100 87 59-12185 2100ND86.8 85.1
Hexachloro-1,3-butadiene ug/L 100 71 24-11668 4100ND70.8 68.1
Hexachlorobenzene ug/L 100 84 1-15281 3100ND84.1 81.3
Hexachlorocyclopentadiene ug/L 100 75 25-15069 8100ND74.6 68.6
Hexachloroethane ug/L 100 73 40-11366 10100ND72.8 65.5
Indeno(1,2,3-cd)pyrene ug/L 100 70 1-17167 4100ND69.9 67.4
Isophorone ug/L 100 98 21-19695 3100ND98.5 95.2
N-Nitroso-di-n-propylamine ug/L 100 87 1-23085 3100ND87.3 84.8
N-Nitrosodimethylamine ug/L 100 67 25-15061 9100ND66.6 61.1
N-Nitrosodiphenylamine ug/L 100 88 25-15087 1100ND88.0 87.3
Naphthalene ug/L 100 77 21-13372 6100ND76.8 72.3
Nitrobenzene ug/L 100 92 35-18087 5100ND92.1 87.4
Pentachlorophenol ug/L 200 85 14-17677 10200ND171155
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1219174MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92204797002
1219175
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenanthrene ug/L 100 84 54-12079 6100ND84.0 79.3
Phenol ug/L 100 54 5-11251 6100ND57.3 53.9
Pyrene ug/L 100 79 52-11581 2100ND79.1 80.8
2,4,6-Tribromophenol (S)%82 10-13783
2-Fluorobiphenyl (S)%78 15-12074
2-Fluorophenol (S)%56 10-12052
Nitrobenzene-d5 (S)%76 10-12070
Phenol-d6 (S)%43 10-12043
Terphenyl-d14 (S)%78 11-13178
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/28300
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Associated Lab Samples:92204797001, 92204797002, 92204797004, 92204797005, 92204797006, 92204797007, 92204797008,
92204797009, 92204797010, 92204797011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1222204
Associated Lab Samples:92204797001, 92204797002, 92204797004, 92204797005, 92204797006, 92204797007, 92204797008,
92204797009, 92204797010, 92204797011
Matrix:Water
Analyzed
Aliphatic (C09-C18)ug/L ND 100 N206/18/14 09:06
Aliphatic (C19-C36)ug/L ND 100 N206/18/14 09:06
Aromatic (C11-C22)ug/L ND 100 N206/18/14 09:06
2-Bromonaphthalene (S)%93 40-140 06/18/14 09:06
2-Fluorobiphenyl (S)%84 40-140 06/18/14 09:06
Nonatriacontane (S)%79 40-140 06/18/14 09:06
o-Terphenyl (S)%75 40-140 06/18/14 09:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1222205LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1222206
Aliphatic (C09-C18)ug/L 228 N23007640-14076229 1 50
Aliphatic (C19-C36)ug/L 384 N24009640-14092367 4 50
Aromatic (C11-C22)ug/L 646 N28507640-14076643 1 50
2-Bromonaphthalene (S)%76 40-14089
2-Fluorobiphenyl (S)%74 40-14081
Nonatriacontane (S)%82 40-14087
o-Terphenyl (S)%76 40-14080
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 77
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
LOD - Limit of Detection.
LOQ - Limit of Quantitation.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Tentatively identified compound (TIC) based on mass spectral library searchN
The lab does not hold TNI accreditation for this parameter.N2
Re-extraction or re-analysis could not be performed due to insufficient sample amount.P2
The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.P5
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 77
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92204797001 OEXT/28300 GCSV/17947DMW-1 MADEP EPH MADEP EPH
92204797002 OEXT/28300 GCSV/17947DMW-2 MADEP EPH MADEP EPH
92204797003 OEXT/28248 GCSV/17913MW-2 MADEP EPH MADEP EPH
92204797004 OEXT/28300 GCSV/17947MW-4 MADEP EPH MADEP EPH
92204797005 OEXT/28300 GCSV/17947MW-7 MADEP EPH MADEP EPH
92204797006 OEXT/28300 GCSV/17947MW-8 MADEP EPH MADEP EPH
92204797007 OEXT/28300 GCSV/17947MW-9 MADEP EPH MADEP EPH
92204797008 OEXT/28300 GCSV/17947MW-11 MADEP EPH MADEP EPH
92204797009 OEXT/28300 GCSV/17947MW-16 MADEP EPH MADEP EPH
92204797010 OEXT/28300 GCSV/17947MW-17 MADEP EPH MADEP EPH
92204797011 OEXT/28300 GCSV/17947MW-18 MADEP EPH MADEP EPH
92204797001 GCV/8229DMW-1 MADEP VPH
92204797002 GCV/8229DMW-2 MADEP VPH
92204797003 GCV/8242MW-2 MADEP VPH
92204797004 GCV/8229MW-4 MADEP VPH
92204797005 GCV/8229MW-7 MADEP VPH
92204797006 GCV/8229MW-8 MADEP VPH
92204797007 GCV/8229MW-9 MADEP VPH
92204797008 GCV/8229MW-11 MADEP VPH
92204797009 GCV/8229MW-16 MADEP VPH
92204797010 GCV/8229MW-17 MADEP VPH
92204797011 GCV/8229MW-18 MADEP VPH
92204797001 MPRP/16185 ICP/14633DMW-1 EPA 3010 EPA 6010
92204797002 MPRP/16198 ICP/14644DMW-2 EPA 3010 EPA 6010
92204797012 MPRP/16198 ICP/14644MW-4 EPA 3010 EPA 6010
92204797013 MPRP/16198 ICP/14644MW-7 EPA 3010 EPA 6010
92204797014 MPRP/16198 ICP/14644MW-8 EPA 3010 EPA 6010
92204797015 MPRP/16198 ICP/14644MW-9 EPA 3010 EPA 6010
92204797016 MPRP/16198 ICP/14644MW-11 EPA 3010 EPA 6010
92204797017 MPRP/16198 ICP/14644MW-16 EPA 3010 EPA 6010
92204797018 MPRP/16198 ICP/14644MW-17 EPA 3010 EPA 6010
92204797019 MPRP/16198 ICP/14644MW-18 EPA 3010 EPA 6010
92204797001 OEXT/28221 MSSV/9238DMW-1 EPA 625 EPA 625
92204797002 OEXT/28221 MSSV/9238DMW-2 EPA 625 EPA 625
92204797003 OEXT/28221 MSSV/9238MW-2 EPA 625 EPA 625
92204797004 OEXT/28221 MSSV/9238MW-4 EPA 625 EPA 625
92204797005 OEXT/28221 MSSV/9238MW-7 EPA 625 EPA 625
92204797006 OEXT/28221 MSSV/9238MW-8 EPA 625 EPA 625
92204797007 OEXT/28221 MSSV/9238MW-9 EPA 625 EPA 625
92204797008 OEXT/28221 MSSV/9238MW-11 EPA 625 EPA 625
92204797009 OEXT/28221 MSSV/9238MW-16 EPA 625 EPA 625
92204797010 OEXT/28221 MSSV/9238MW-17 EPA 625 EPA 625
92204797011 OEXT/28221 MSSV/9238MW-18 EPA 625 EPA 625
92204797001 MSV/27183DMW-1 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 77
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92204797
SPATCO 6228-13-0135
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92204797002 MSV/27183DMW-2 SM 6200B
92204797003 MSV/27183MW-2 SM 6200B
92204797004 MSV/27183MW-4 SM 6200B
92204797005 MSV/27183MW-7 SM 6200B
92204797006 MSV/27183MW-8 SM 6200B
92204797007 MSV/27183MW-9 SM 6200B
92204797008 MSV/27183MW-11 SM 6200B
92204797009 MSV/27183MW-16 SM 6200B
92204797010 MSV/27183MW-17 SM 6200B
92204797011 MSV/27183MW-18 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/25/2014 07:09 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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