18052_Gelco Trailer_Supplemental Investigation_2013_8_22

August 22, 2013

Mr. Miguel A. Alvalle
Inactive Hazardous Sites Branch
Department of Environment and Natural Resources
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28117

Re: Former GE Trailer Fleet Services Charlotte Facility
(a.k.a. Transport International Pool, TIP)
1906 Bancroft Street
Charlotte, Mecklenburg County, North Carolina

Dear Mr. Alvalle:

On October 17, 2012, AMEC Environment & Infrastructure, Inc. (“AMEC”) submitted a report to the
North Carolina Department of Environment and Natural Resources’ (the “NCDENR”) summarizing
the results of a Phase II environmental assessment at the former General Electric (“GE”) Trailer
Fleet Services (“TFS”) facility located at 1906 Bancroft Street, Charlotte, Mecklenburg County,
North Carolina (the “Site”). The Phase II, “Phase II Environmental Site Assessment, 1906 Bancroft
Street, Charlotte, Mecklenburg County, North Carolina, August 2012” was completed by GE in
preparation of sale of the property. The general location of the Site is shown on Figure 1. The
configuration of the Site, along with key Site features, is shown on Figure 2.

In response to the AMEC Phase II report, NCDENR sent a letter to GE dated April 3, 2013 outlining
additional activities to be completed at the Site. This letter summarizes the investigations and
findings of the August 2012 Phase II, and describes the supplemental activities completed to
address the requirements and suggestions of NCDENR’s April 3, 2013 letter.

Phase II Summary
The August 2012 Phase II completed by AMEC consisted of collecting soil samples from 12 boring
locations, installing nine monitoring wells, collecting groundwater samples from those monitoring
wells and reviewing surrounding properties to identify potential upgradient sources of volatile
organic compounds (VOCs) identified in groundwater. A complete description of the Phase II as
well as all the findings of the investigation is provided in the August 2012 Phase II report previously
submitted to NCDENR.
The analytical data for the soil samples collected during the August 2012 Phase II and these
supplemental investigations were compared to the NCDENR Inactive Hazardous Sites Branch
(IHSB) Preliminary Soil Remediation Goals (SRGs). Groundwater results were compared to the
NCDENR 2L Groundwater Quality Standards (2L Standards).

Former GE Trailer Fleet Services Charlotte Facility (continued)
August 22, 2013
Page 2

The findings of the August 2012 Phase II included:
Soils
 VOCs were not detected in Site soils with the exception of acetone and methyl ethyl ketone
(MEK). Both acetone and MEK were detected at estimated concentrations far below their
respective residential SRGs. Both MEK and acetone are considered laboratory and/or field
preservation artifacts and not representative of Site conditions.
 No semi volatile organic compounds (SVOCs) were detected in Site soils.
 No Total Petroleum Hydrocarbons (TPH) as Gasoline Range Organics (GRO) or Diesel
Range Organics (DRO), or PCBs were detected in Site soils.
 Metals detected in soils included arsenic, barium, chromium, copper, lead, nickel, selenium
and zinc, of which arsenic and selenium were detected above the NCDENR SRGs. The
presence of the arsenic and selenium as well as all other metals detected in soils was
considered to be representative of naturally occurring conditions as these compounds are
commonly found in Piedmont soils.
Groundwater
 VOCs detected in groundwater samples from the Site included chloroform, carbon
tetrachloride, 1,1-dichloroethane (1,1-DCA), 1,1-dichloroethene (1,1-DCE), cis-1,2-
dichloroethene (c1,2-DCE), tetrachloroethene (PCE) and trichloroethylene (TCE), of which
only carbon tetrachloride, 1,1-DCE, PCE and TCE were above the NCDENR 2L Standards.
Based on the distribution of 1,1-DCE, PCE and TCE observed in groundwater in upgradient
wells, the absence of these constituents in Site soils, the industrial nature of the surrounding
properties and the potential sources for these constituents upgradient of the Site, it was
concluded that these constituents were from an upgradient source and not Site related.
 No SVOCs were detected in groundwater samples collected from the Site.
 No TPHs were detected groundwater samples collected from the Site
 Total chromium was the only metal detected above the chromium 2L Standard in
groundwater samples collected from the Site. The detection of chromium was attributed to
turbidity in the newly installed wells. A second round of samples found chromium below the
laboratory Practical Quantitation Limit (PQL).
As discussed in the August Phase II investigation report, with no known chlorinated solvent usage
at the Site, no chlorinated solvents detected in Site soil, and confirmed chlorinated solvents impacts
upgradient of the Site, AMEC concluded that the VOCs identified in groundwater beneath the Site
were from an upgradient source and not related to former TFS operations.

Former GE Trailer Fleet Services Charlotte Facility (continued)
August 22, 2013
Page 3

Supplemental Investigations (April 3, 2013 NCDENR letter)
In response to the AMEC’s August 2012 Phase II report, NCDENR sent a letter to GE ( April 3,
2013), outlining additional required and suggested activities to be completed at the Site with the
objective of confirming AMEC’s conclusion that VOCs detected in groundwater were not Site
related. GE has completed all the items suggested by NCDENR with the exception of collecting
water and sediment samples from the stream located in the southwest portion of the Site. These
activities were not completed because the stream flows through a highly industrialized area
upstream of the Site with confirmed sources of contamination and the stream flows through a
portion of the Site that was not used by TFS.

The upgradient source referenced above and AMEC’s Phase II report was recently confirmed
during a 1% Investigation conducted by NCDENR’s Dry Cleaning Solvent Cleanup Act Program.
The 1% Investigation confirmed a PCE release at the American Dry Cleaner and Laundry. The
American Dry Cleaner and Laundry facility is located approximately 1,000 feet to the west-
northwest of the Site in an upgradient orientation with respect to the Site. The findings of the 1%
Investigation are presented in the Hart & Hickman, PC (H&H) June 17, 2013 report entitled 1%
Investigation Report, American Dry Cleaners and Laundry, DSCA ID: 60-0079, 1806 North Graham
Street, Charlotte, Mecklenburg County, North Caroline Dry-Cleaning Solvent Cleanup Act Program
(the “H&H 1% Report”). The H&H 1% Report states the following: “There is no evidence that TIP
used PCE, and PCE was not detected in soil samples collected at the site. Therefore, the PCE is
suspected to be from an upgradient source.” A copy of the text, tables and figures from the 1%
investigation are included as Attachment A.
Related to the “Required Actions” outlined by NCDENR in their April 3, 2013 letter:

1. GE has completed the “Site Cleanup Questionnaire” and “Notification of an Inactive
Hazardous Substance or Waste Disposal Site”. These documents are attached as
Attachment B.
2. Since the source of the impacted groundwater discovered beneath the Site has been
confirmed to be from from an upgradient source which GE does not control, and sinceGE
did not conduct any activity resulting in the observed impacts to groundwater, GE could not
take initial abatement actions as required under 15A NCAC 2L.

Specific to NCDENR’s suggested activities to confirm that VOCs identified in the groundwater are
not Site related and to further characterize the Site, AMEC on behalf of GE has completed the
following:

1. Collected samples from the vicinity of borings B4 and B5 for analysis of VOCs by United
States Environmental Protection Agency (EPA) Method 8260 and select metals (arsenic and
selenium) by EPA Method 6010.
2. Collected one additional round of groundwater samples from all onsite monitoring wells for
laboratory analysis of VOCs by EPA Method 8260.
Former GE Trailer Fleet Services Charlotte Facility (continued)
August 22, 2013
Page 4

3. Collected soil samples from non-operational portions of the Site to determine whether
metals (arsenic and selenium) detected above NCDENR SRGs during the Phase II are
within natural background concentrations for the Site.
4. Completed a comprehensive survey to determine if any water supply wells and/or surface
water intakes are present within a 1500 foot radius of the Site that are used for potable
water.
5. Evaluated vapor intrusion according to NCDENR’s “Supplemental Guidelines for Evaluation
of Structural Vapor Intrusion Potential”.

The following sections summarize the findings resulting from the activities listed above.

Soil Sampling – Volatile Organic Compounds
To meet NCDENRs request to collect samples from the vicinity of the original Phase II borings B4
and B5, two surface soil samples (i.e., from the upper one foot of the soil column) were collected
along the eastern and southern edges of the maintenance shop. The objective of this effort was to
confirm that chlorinated solvents are not present in shallow soils around the maintenance shop.

The soil samples collected (RR-1 and RR-2) were screened visually and with a photo-ionization
detector (PID). Sample RR-1/0.75 had a PID reading of 54.8 parts per million-air (ppm-air) and
sample RR-1/0.5 had a PID reading of 21.8 ppm-air. The samples collected were submitted to
Accutest Laboratories for VOC analysis by EPA Method 8260.

The laboratory results showed that no chlorinated solvents were detected in either of the collected
soil samples; however compounds typically identified as laboratory artifacts (acetone and methyl
ethyl ketone) were detected as well as compounds typically associated with petroleum product
(ethylbenzene, toluene and xylene (total)). These constituents were detected at concentrations well
below the applicable NCDENR criteria for residential properties. Table 1 provides a summary of
the laboratory results. Laboratory analytical data-sheets are provided in Attachment C.

These data as well as data collected during the August 2012 Phase II support the conclusion that
soil at the Site has not been impacted by chlorinated solvents (i.e., PCE, TCE and associated
degradation products) and that chlorinated solvents identified in groundwater can be attributed to an
upgradient source(s).

Groundwater Sampling
An additional round of groundwater samples was collected from the Site wells on February 20,
2013. Prior to collecting the groundwater samples, water level measurements were collected from
each of the nine monitoring wells. Additionally, in June 2013, AMEC installed staff gauges in the
stream that crosses the southern portion of the Site (with a west-northwest to east-southeast
alignment) and conducted a boundary survey which included locating the on-site monitoring well
network and the newly installed staff gauges. The survey was conducted by KCI Associates of
Former GE Trailer Fleet Services Charlotte Facility (continued)
August 22, 2013
Page 5

North Carolina. Site coordinates and elevations reference the North Carolina State Plane
Coordinate System (North American Datum 1983 horizontal, North American Vertical Datum 1988
vertical).

Groundwater flow across the northern half of the Site is to the south with a south-southwest
component of flow in the southern half of the Site. Groundwater elevations are provided in Table 2,
and groundwater contours for the February 2013 groundwater gauging and sampling event are
provided on Figure 3. Groundwater flow patterns have been consistent throughout this
investigation.

Based on surface water levels measured in the stream channel on June 18, 2013 (taken during the
boundary survey after the staff gauges were installed), flow in the stream channel is from west-
northwest to east-southeast (i.e., surface water elevations were 719.7 feet above mean sea level (ft
amsl) in the west-northwest corner, 715.3 ft amsl generally mid-Site, and 712.7 ft amsl in the east-
southeast corner of the Site). The staff gauges are located within the Site boundary.

The first groundwater sampling event was completed at the Site on May 2, 2011 and included in the
August 2012 Phase II. This sampling event included the five Site monitoring wells in place at that
time. Four additional wells were installed after the May 2, 2011 sampling event to delineate impacts
observed in monitoring wells MW-1 and MW-2. All nine monitoring wells were sampled on June 16
and 17, 2011; those results were also included in the August 2012 Phase II. Following the
submission of the Phase II ESA report, a follow-up round of groundwater samples was collected on
February 20, 2013 from all nine Site monitoring wells. The results from the February 20, 2013
groundwater sampling event are provided with this letter as GE’s response to NCDENR’s request
for an additional round of groundwater sampling. Tabular results from this sampling event are
presented in Table 3 and the laboratory data sheets are presented in Attachment C. Generalized
results from the February 2013 groundwater sampling event are summarized below:

 MW-1: Chloroform, 1,1-DCA, 1,1-DCE, c1,2-DCE, t1,2-DCE, PCE and TCE were detected
with 1,1-DCE, PCE and TCE detected at concentrations above the 2L Standards.

 MW-2: None of the VOCs previously detected (Chloroform, Carbon Tetrachloride, and TCE)
were detected. No other VOCs were detected.

 MW-3: During the prior two sampling events (May 2011 and June 2011), there were no
VOCs detected in MW-3. During the February 20, 2013 sampling event PCE was detected
at a concentration below the 2L Standards.

 MW-4: There were no VOCs detected in MW-4 during the three rounds of sampling.

Former GE Trailer Fleet Services Charlotte Facility (continued)
August 22, 2013
Page 6

 MW-5: PCE was detected in MW-5 at an estimated concentration below the 2L Standards
during the May 2011 sampling event. There were no VOCs detected during the June 2011
and February 2013 sampling events.

 MW-6: 1,1-DCE was detected below the 2L Standards while TCE was detected above the
2L Standards.

 MW-7: 1,1-DCE, PCE and TCE were detected above the 2L Standards. 1,1-DCA, c1,2-
DCE and t1,2-DCE were also detected, but at concentrations below the 2L Standards.

 MW-8: Chloroform and TCE were detected at concentrations below the 2L Standards.

 MW-9: 1,1-DCA, 1,1-DCE, c1,2-DCE, PCE and TCE were detected at concentrations below
the 2L Standards. PCE was detected above the 2L Standards.

Overall, with the exception of the absence of carbon tetrachloride in monitoring well MW-2,
groundwater conditions at the Site have remained generally consistent with conditions observed
during previous groundwater sampling events.

Soil Sampling – Arsenic and Selenium
As requested by NCDENR, samples for arsenic and selenium were collected from six onsite
locations (RR-3 through RR-9) at varying depths (surficial [i.e., upper one-foot], four to 6.5 feet
below ground surface (ft bgs), and seven to 13 ft bgs). The samples were collected at points along
the property fence line and/or in areas with little or no on-Site activity. These samples were
collected in an effort establish background conditions for arsenic and selenium in soils at the Site.

The arsenic and selenium results are provided in Table 1. Laboratory analytical data-sheets are
provided in Attachment C.

Arsenic was detected in all 18 samples collected during these supplemental investigations. Arsenic
concentrations ranged from 0.24 milligrams per kilogram (mg/kg) to 4 mg/kg with an average
concentration of 1.45 mg/kg. During the August 2012 Phase II, arsenic was detected in 14 of the
23 samples at concentrations ranging from 0.64 mg/kg to 2.8 mg/kg with an average concentration
of 1.7 mg/kg. Further, the North Carolina Department of Agriculture and Consumer Services
(NCDACS), Agronomic Division, has published a bulletin entitled Heavy Metals in North Carolina
Soils, Occurrence & Significance which reports that the average concentration of arsenic in soil in
North Carolina is 4.5 parts per million (ppm), well above the average and the maximum
concentrations observed at the Site. These data indicate that the Phase II sample results are within
the range of concentrations detected in the background samples. These lines of evidence support
the Phase II conclusion that arsenic identified in Site soils is naturally occurring and not related to
Site operations.
Former GE Trailer Fleet Services Charlotte Facility (continued)
August 22, 2013
Page 7

Selenium was detected in only one of the 18 background samples collected during the
supplemental activities. The one reported concentration was at an estimated concentration of 0.27
mg/kg. During the August 2012 Phase II, selenium was detected in 10 of the 24 samples at
concentrations ranging from 1.2 mg/Kg to 3.8 mg/Kg, with an average concentration of 2.3 mg/kg.
The selenium Direct Contact soil remediation goal (based on a residential Site use) is 78 mg/Kg.
The selenium soil remediation goal that is protective of groundwater is 2.1 mg/kg. Only four of the
Phase II samples exceeded the protective of groundwater standard of 2.1 mg/Kg Selenium was
not detected in the dissolved state in groundwater and Selenium was detected in two samples at
concentrations in the total (i.e. unfiltered) samples at estimated concentrations (i.e., above the
laboratory method detection limit but below the laboratory reporting limit) of 3.5 micrograms per
Liter (µg/L) and 2.6 µg/L. The selenium 2L groundwater standard is 20 µg/L.

Although not well supported by the selenium background investigation, AMEC maintains that the
selenium observed in Site soils is naturally occurring and not related to the former TFS operations
for the following reasons: 1) selenium was not used in the former TFS operations and the Site was
undeveloped prior to TFS occupying the Site in 1986; 2) three of the four locations where the
NCDENR protection of groundwater soil standard was exceeded during the August 2012 Phase II
were resampled to determine whether the original results were reproducible; the original results
were not reproducible and results for the additional samples collected at that time were below the
laboratory practical quantification limit; and 3) selenium was not detected in groundwater above 2L
groundwater standard of 20 µg/L.

Water Supply Well Search
AMEC conducted a water supply well and surface water intake search by observing the surrounding
properties within 500 feet of the subject property and by performing a driving and walking
reconnaissance of streets and properties within 1,500 feet of the Site. AMEC also reviewed the
Mecklenburg County Well Information System, an on-line service, for records of water supply wells
within 1,500 feet of the subject property. While there is no restriction on use of water wells within
the City of Charlotte, public water is available to the residents and businesses within 1,500 feet of
the Site.

No records of water supply wells were identified in the Mecklenburg County Well Information
System. However, during a prior (2009) receptor survey conducted by MACTEC in the area of the
Site, a potential water supply well was reported to exist at 311 West 24th Street, approximately 400
feet east (cross-gradient) of the Site. The walking reconnaissance conducted by AMEC for this well
search did not reveal any evidence of that water supply well (e.g., wellhead, well pad) at the 311
West 24th Street property. AMEC contacted the registered property owner for that address on July
31, 2013 via Certified U.S. Mail to confirm the presence or absence of a water supply well. If a
response is received from the property owner, AMEC will update NCDENR accordingly.

Former GE Trailer Fleet Services Charlotte Facility (continued)
August 22, 2013
Page 8

Based on a review of Mecklenburg County water supply well listings and a visual reconnaissance of
the area surrounding the Site, there do not appear to be any operational water supply wells within a
1,500 foot radius of the Site. It should also be noted that the Site is not located within a well head
protection area.

In addition to the potable water well search findings, there are also no surface water intakes in the
area of the Site. The water supply for the City of Charlotte is Lake Norman, located approximately
17 miles north/northwest of the Site.

The H&H 1% Investigation of the American Dry Cleaner and Laundry also did not identify any water
supply wells within a 1,500 foot radial search of that property.

Sub-slab Vapor Survey
In August 2012, AMEC conducted a sub-slab vapor survey in the former TFS Site maintenance
shop. The work was conducted in conformance with DENR’s guidance document entitled
Supplemental Guidelines for Evaluation of Structural Vapor Intrusion Potential. To accomplish the
survey, sub-slab samples were collected at four locations from beneath shop floor to determine the
potential for vapor intrusion from groundwater into the building.
A copy of the sub-slab vapor sampling report is provided as Attachment D. The sub-slab vapor
survey findings are summarized below:
 Each sub-slab vapor sample collected exhibited PCE at a concentration below its Inactive
Hazardous Sites Branch (IHSB) soil gas Industrial/Commercial screening level, but above its
method detection limit. No other volatile organic compounds were detected in the samples
collected.

 The sub-slab results were also compared to United States Environmental Protection Agency
(USEPA) Regional Screening Levels (RSLs) for Industrial Air. The RSLs are based on a
Carcinogenic Target Risk of 10-6 and non-cancer Hazard Index (HI) of 1. When considering
a 90 fold attenuation factor (reference USEPA Vapor Intrusion Guidance, December 13,
2012) to account for the concrete slab, the Site results indicate a Carcinogenic Target Risk
of 10-8 and the HI is 0.01 for the Site building.

The sub-slab vapor survey did not identify adverse risk to Site occupants in a slab-on-grade
structure based on the IHSB Industrial/Commercial (i.e., non-residential) Site use.
Conclusion
The August 2012 Phase II and the additional data collected during these supplemental
investigations have shown that:

Former GE Trailer Fleet Services Charlotte Facility
August 22, 2013

FIGURES

0 2000 4000
Approximate scale in Feet
Reference:
1988 Charlotte East
7.5-minute Series
Quadrangle Sheet

Contour interval 10 feet
Former GE TFS Charlotte Branch Location
Supplement Investigation
1906 Bancroft Street, Charlotte
Mecklenburg County, North Carolina

Figure 1 – Site Location Map

Environment & Infrastructure, Inc.
502 West Germantown Pike, Suite 850
Plymouth Meeting PA 19462

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Q:\GE Brownfields Program\Charlotte\DRAFTING\Charlotte Fig 2 Site Plan.dwg Aug 08, 2013 - 11:34am
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Q:\GE Brownfields Program\Charlotte\DRAFTING\Charlotte Fig 3 GW.dwg Aug 08, 2013 - 11:32am
G
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Former GE Trailer Fleet Services Charlotte Facility
August 22, 2013

TABLES

Ta
b
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e

1
So
i
l

A
n
a
l
y
t
i
c
a
l

R
e
s
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s
19
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t
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a
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o
l
i
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a
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t

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a
m
p
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e

I
D
:

N
C

S
o
i
l

N
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S
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C

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o
i
l

R
R
-
1
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0
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7
5

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2
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.
5

R
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3
/
1
.
0

R
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3
/
4
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0

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7
.
5

R
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1
.
0

R
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4
.
5

R
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4
/
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.
0

R
R
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5
/
1
.
0

R
R
-
5
/
5
.
0

R
R
-
5
/
9.5

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6
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0
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5

R
R
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6
/
5
.
5

R
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6
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5
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8
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1

F
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5
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8
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2

F
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8
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3

F
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5
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8
-
4

F
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5
2
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5

F
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5
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0
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-
6

F
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8
-
7

F
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0
8
-
8

F
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5
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8
-
9

F
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1
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F
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2

F
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3

F
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4
Da
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d
:

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a
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e

6
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1
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6
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2
0
1
3

6
/
3
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2
0
1
3

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August 22, 2013

ATTACHMENT A

(Page 1 of 106)
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Former GE Trailer Fleet Services Charlotte Facility
August 22, 2013

ATTACHMENT B

REVISED: November 2011 Page 1 of 5
North Carolina Department of Environment and Natural ResourcesDivision of Waste Management
Superfund SectionInactive Hazardous Sites Branch
NOTIFICATION OF AN INACTIVE HAZARDOUS SUBSTANCE
OR WASTE DISPOSAL SITE
Please read instructions before completing and type or print in black ink.
I. SITE NAME AND LOCATION:
Site Name (one site per form) Location (street address) City US EPA ID# (if known)
County
Directions to Site

Attach a USGS topographic map or map of equal or reasonably similar scale (1 inch = 2000 ft.) showingthe location and vicinity of the site or facility. Label map with the site name.
II. PERSON COMPLETING FORM: Present Owner ___
Name Past Owner ___
Mailing Address Present Operator ___
Past Operator ___
City State Zip Code Other ___
Telephone ( ) (specify)
III. PRESENT OWNER:
Individual Owner or Company Name Corporation ___
Partnership ___
Executive Officer Individual ___
Mailing Address Government Unit ___
Other ___
City State Zip Code (specify)
Telephone ( )
REVISED: November 2011 Page 2 of 5
IV. CURRENT SITE USE:
Check the item or items which describe the current use of the site.
Residential ___Forest Land ___Retirement Home ___
Business ___Farm Land ___Other ___
Industrial ___School/Day Care ___(specify)_____________
Pasture Land ___Hospital _______________________
V. ON-SITE RESIDENTS:
Are there any on-site residents? ___ Yes ___ No
Number of children (# 6 years old) living on site __________ Number of adults __________
VI. SURROUNDING PROPERTY USE:
Check the appropriate description of the area surrounding the site. (More than one may apply.)
Residential ___Forest Land ___Retirement Home ___
Business ___Farm Land ___Other ___
Industrial ___School/Day Care ___(Specify)_____________
Pasture Land ___Hospital _______________________
VII. Site Operations (More than one may apply.):
Current Previous
1. Mining ...................................................___ ___
2. Paper and wood production ...................................___ ___
3. Textiles ...................................................___ ___
4. Fertilizer ..................................................___ ___
5. Printing/painting............................................___ ___
6. Leather tanning.............................................___ ___
7. Iron/steel foundry ...........................................___ ___
8. Chemical, general...........................................___ ___
9. Plating/polishing............................................___ ___
10. Military/ammunition .........................................___ ___
11. Firing range ...............................................___ ___
12. Rubber/plastics .............................................___ ___
13. Utility companies/transformers .................................___ ___
14. Sanitary/refuse .............................................___ ___
15. Photo finishing .............................................___ ___
16. Lab/hospital ...............................................___ ___
17. Wood treating ..............................................___ ___
18. Battery reclamation..........................................___ ___
19. Pesticides formulation, packaging and/or distribution ...............___ ___
20. Herbicide formulation, packaging and/or distribution ...............___ ___
21. Other agrichemical formulation, packaging and/or distribution........___ ___
22. Dry cleaning ...............................................___ ___
23. Petrochemical processing or refining ............................___ ___
24. Furniture manufacturing or finishing ............................___ ___
25. Drum reconditioning.........................................___ ___
26. Unknown .................................................___ ___
27. Other (specify) _________________________________............___ ___
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REVISED: November 2011 Page 4 of 5
X. TOTAL AREA OF ALL DISPOSALS, SPILLS, OR RELEASES OF HAZARDOUS SUBSTANCES OR
WASTE:
___less than 1 acre
___1 acre or more, but less than 5 acres
___5 acres or more, but less than 10 acres
___10 acres or more
___Unknown
XI. AVAILABILITY OF ENVIRONMENTAL ANALYTICAL DATA:
Do any environmental reports or laboratory analytical data exist for the site? ___ Yes ___ No
If yes, attach reports or data to this form.
XII. IDENTIFY WHETHER ANY OF THE FOLLOWING ARE PRESENT OR WERE PRESENT IN THE PASTAT THE SITE (More than one may apply.):
___Debris pile(s)___Tank(s) above ground ___Spill(s)
___Land treatment of sludges ___Septic tank(s)___Wastewater lagoon(s)
___Landfill(s) or buried waste ___Surface impoundment(s)___Drum(s)
___Tank(s) underground ___Underground injection of waste
___Other (specify) __________________________________________________________
XIII. ACCESSIBILITY OF SITE (More than one may apply.):
___24-hour security guard
___Security guard < 24-hour/day
___Physical barrier (steep bank, creek, walls, etc.)
Describe physical barriers

___Site completely surrounded by fence
___Site partially surrounded by fence
___Locked gate
___Unlocked gate
___No control of access to site
___Other (specify)
XIV. WATER SUPPLY SOURCES:
Identify whether the following are present on site or on adjacent property.
Present on site Present on Adjacent Property
Yes No Yes No
Spring ___ ______ ___
Well ___ ______ ___
Surface Water Intake ___ ______ ___
XV. SITE SURFACE WATER:
Indicate whether any surface water bodies (e.g. streams and lakes) exist on the site or the property adjacent to
the site.

0 2000 4000
Approximate scale in Feet
Reference:
1988 Charlotte East
7.5-minute Series
Quadrangle Sheet

Contour interval 10 feet
TFS Charlotte Branch Location
Phase II Environmental Site Assessment
1906 Bancroft Street, Charlotte
Mecklenburg County, North Carolina
AMEC Project #: 572260702
Figure 1 – Site Location Map

Environment & Infrastructure, Inc.
502 West Germantown Pike, Suite 850
Plymouth Meeting PA 19462

SITE
Former GE Trailer Fleet Services Charlotte Facility
August 22, 2013

ATTACHMENT C

08/27/13
Technical Report for
AMEC Environment & Infrastructure, Inc.
GE-TFS; 1906 Bancroft St, Charlotte, NC
781090010
Accutest Job Number: FA1942
Sampling Date: 02/20/13
Report to:
AMEC Earth & Environmental
[e-mail]
ATTN: Steve Tanen
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), AK, AR, GA, KY, MA, NV, OK, UT, VA, WA, WI
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Conference
and/or state specific certification programs as applicable.
Client Service contact: Heather Wandrey 407-425-6700
Harry Behzadi, Ph.D.
Laboratory Director
Southeast
08/27/13
e-Hardcopy 2.0
Automated Report
59
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 59
FA1942
Table of Contents
-1-
Sections:
Section 1: Sample Summary ................................................................................................... 3
Section 2: Case Narrative/Conformance Summary .............................................................. 4
Section 3: Summary of Hits ....................................................................................................5
Section 4: Sample Results ........................................................................................................ 7
4.1:FA1942-1: MW-5 ......................................................................................................... 8
4.2:FA1942-2: MW-3 ......................................................................................................... 10
4.3:FA1942-3: MW-4 ......................................................................................................... 12
4.4:FA1942-4: MW-6 ......................................................................................................... 14
4.5:FA1942-5: MW-2 ......................................................................................................... 16
4.6:FA1942-6: MW-1 ......................................................................................................... 18
4.7:FA1942-7: MW-9 ......................................................................................................... 20
4.8:FA1942-8: MW-7 ......................................................................................................... 22
4.9:FA1942-9: MW-8 ......................................................................................................... 24
4.10:FA1942-10: TRIP BLANK ........................................................................................ 26
4.11:FA1942-11: DUP 1 ..................................................................................................... 28
Section 5: Misc. Forms ............................................................................................................ 30
5.1:Chain of Custody ........................................................................................................... 31
Section 6: GC/MS Volatiles - QC Data Summaries .............................................................. 33
6.1:Method Blank Summary ................................................................................................ 34
6.2:Blank Spike Summary ................................................................................................... 37
6.3:Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 40
6.4:Instrument Performance Checks (BFB) ......................................................................... 43
6.5:Internal Standard Area Summaries ................................................................................ 47
6.6:Surrogate Recovery Summaries ..................................................................................... 50
6.7:Initial and Continuing Calibration Summaries .............................................................. 51
1
2
3
4
5
6
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FA1942
Accutest LabLink@144522 15:14 27-Aug-2013
Sample Summary
AMEC Environment & Infrastructure, Inc.
Job No:FA1942
GE-TFS; 1906 Bancroft St, Charlotte, NC
Project No: 781090010
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA1942-1 02/20/13 08:46 THDS 02/21/13 AQ Ground Water MW-5
FA1942-2 02/20/13 09:05 THDS 02/21/13 AQ Ground Water MW-3
FA1942-3 02/20/13 09:50 THDS 02/21/13 AQ Ground Water MW-4
FA1942-4 02/20/13 10:00 THDS 02/21/13 AQ Ground Water MW-6
FA1942-5 02/20/13 10:40 THDS 02/21/13 AQ Ground Water MW-2
FA1942-6 02/20/13 10:55 THDS 02/21/13 AQ Ground Water MW-1
FA1942-7 02/20/13 11:25 THDS 02/21/13 AQ Ground Water MW-9
FA1942-8 02/20/13 11:50 THDS 02/21/13 AQ Ground Water MW-7
FA1942-9 02/20/13 12:10 THDS 02/21/13 AQ Ground Water MW-8
FA1942-10 02/20/13 00:00 THDS 02/21/13 AQ Trip Blank Water TRIP BLANK
FA1942-11 02/20/13 00:00 THDS 02/21/13 AQ Ground Water DUP 1
3 of 59
FA1942
1
SAMPLE DELIVERY GROUP C ASE NARR ATIVE
Client:AMEC Environment & Infrastructure, Inc.Job:FA1942
Site:GE-TFS; 1906 Bancroft St, Charlotte, NC Report Date:2/25/2013 2:36:44 PM
10 Samples and 1 Trip Blank were collected on 02/20/2013 and were received at Accutest SE on 02/21/2013 properly preserved, at 2.6
Deg. C and intact. These Samples received an Accutest job number of FA1942. A listing of the Laboratory Sample ID, Client Sample ID
and dates of collection are presented in the Results Summary Section of this report.
Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For more
information, please refer to QC summary pages.
Volatiles by GCMS By Method SW846 8260B
Matrix:AQ Batch ID:VZ591
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) FA1711-1MS, FA1711-1MSD were used as the QC samples indicated.
Matrix Spike Duplicate Recovery(s) for Chlorobenzene are outside control limits. Probable cause is due to matrix interference.For
method performance in a clean matrix, refer to Blank Spike.
Matrix:AQ Batch ID:VZ592
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) FA1942-6MS, FA1942-6MSD were used as the QC samples indicated.
Accutest Laboratories Southeast (ALSE) certifies that this report meets the project requirements for analytical data produced
for the samples as received at ALSE and as stated on the COC. ALSE certifies that the data meets the Data Quality Objectives
for precision, accuracy and completeness as specified in the ALSE Quality Manual except as noted above. This report is to be
used in its entirety. ALSE is not responsible for any assumptions of data quality if partial data packages are used.
Narrative prepared by:
______________________________________ Date: February 25, 2013
Kim Benham, Client Services (signature on file)
Monday, February 25, 2013 Page 1 of 1
4 of 59
FA1942
2
Summar y of Hits Page 1 of 2
Job Number:FA1942
Account:AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Collected:02/20/13
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA1942-1 MW-5
No hits reported in this sample.
FA1942-2 MW-3
Tetrachloroethylene 0.49 J 1.0 0.32 ug/l SW846 8260B
FA1942-3 MW-4
No hits reported in this sample.
FA1942-4 MW-6
1,1-Dichloroethylene 0.94 J 1.0 0.20 ug/l SW846 8260B
Trichloroethylene 36.9 1.0 0.31 ug/l SW846 8260B
FA1942-5 MW-2
No hits reported in this sample.
FA1942-6 MW-1
Chloroform 0.79 J 1.0 0.26 ug/l SW846 8260B
1,1-Dichloroethane 1.3 1.0 0.21 ug/l SW846 8260B
1,1-Dichloroethylene 11.1 1.0 0.20 ug/l SW846 8260B
cis-1,2-Dichloroethylene 30.7 1.0 0.24 ug/l SW846 8260B
trans-1,2-Dichloroethylene 0.40 J 1.0 0.23 ug/l SW846 8260B
Tetrachloroethylene 98.5 5.0 1.6 ug/l SW846 8260B
Trichloroethylene 127 5.0 1.6 ug/l SW846 8260B
FA1942-7 MW-9
1,1-Dichloroethane 0.55 J 1.0 0.21 ug/l SW846 8260B
1,1-Dichloroethylene 0.36 J 1.0 0.20 ug/l SW846 8260B
cis-1,2-Dichloroethylene 10.4 1.0 0.24 ug/l SW846 8260B
Tetrachloroethylene 3.0 1.0 0.32 ug/l SW846 8260B
Trichloroethylene 1.7 1.0 0.31 ug/l SW846 8260B
FA1942-8 MW-7
1,1-Dichloroethane 1.4 1.0 0.21 ug/l SW846 8260B
1,1-Dichloroethylene 17.7 1.0 0.20 ug/l SW846 8260B
cis-1,2-Dichloroethylene 39.9 1.0 0.24 ug/l SW846 8260B
trans-1,2-Dichloroethylene 0.58 J 1.0 0.23 ug/l SW846 8260B
5 of 59
FA1942
3
Summar y of Hits Page 2 of 2
Job Number:FA1942
Account:AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Collected:02/20/13
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Tetrachloroethylene 97.3 2.0 0.64 ug/l SW846 8260B
Trichloroethylene 97.6 1.0 0.31 ug/l SW846 8260B
FA1942-9 MW-8
Chloroform 1.3 1.0 0.26 ug/l SW846 8260B
Trichloroethylene 0.34 J 1.0 0.31 ug/l SW846 8260B
FA1942-10 TRIP BLANK
No hits reported in this sample.
FA1942-11 DUP 1
Chloroform 1.2 1.0 0.26 ug/l SW846 8260B
Trichloroethylene 0.38 J 1.0 0.31 ug/l SW846 8260B
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FA1942
3
Accutest LabLink@144522 15:14 27-Aug-2013
Sample Results
Report of Analysis
Southeast
Section 4
7 of 59
FA1942
4
Accutest LabLink@144522 15:14 27-Aug-2013
Repor t of Analysis Page 1 of 2
Client Sample ID:MW-5
Lab Sample ID:FA1942-1 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Z13909.D 1 02/22/13 KW n/a n/a VZ591
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.21 U 1.0 0.21 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.34 U 1.0 0.34 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.26 U 1.0 0.26 ug/l
75-15-0 Carbon disulfide 0.49 U 2.0 0.49 ug/l
56-23-5 Carbon tetrachloride 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 0.21 U 1.0 0.21 ug/l
75-35-4 1,1-Dichloroethylene 0.20 U 1.0 0.20 ug/l
107-06-2 1,2-Dichloroethane 0.22 U 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane 0.26 U 1.0 0.26 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.24 U 1.0 0.24 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.22 U 1.0 0.22 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.23 U 1.0 0.23 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.21 U 1.0 0.21 ug/l
100-41-4 Ethylbenzene 0.29 U 1.0 0.29 ug/l
591-78-6 2-Hexanone 2.0 U 10 2.0 ug/l
108-10-1 4-Methyl-2-pentanone 2.3 U 5.0 2.3 ug/l
74-83-9 Methyl bromide 0.79 U 2.0 0.79 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 3.1 U 5.0 3.1 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.24 U 1.0 0.24 ug/l
79-00-5 1,1,2-Trichloroethane 0.20 U 1.0 0.20 ug/l
127-18-4 Tetrachloroethylene 0.32 U 1.0 0.32 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 0.31 U 1.0 0.31 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 59
FA1942
4
4
.
1
Accutest LabLink@144522 15:14 27-Aug-2013
Repor t of Analysis Page 2 of 2
Client Sample ID:MW-5
Lab Sample ID:FA1942-1 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.44 U 1.0 0.44 ug/l
1330-20-7 Xylene (total) 0.50 U 3.0 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100% 87-116%
17060-07-0 1,2-Dichloroethane-D4 101% 76-127%
2037-26-5 Toluene-D8 98% 86-112%
460-00-4 4-Bromofluorobenzene 101% 84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 59
FA1942
4
4
.
1
Accutest LabLink@144522 15:14 27-Aug-2013
Repor t of Analysis Page 1 of 2
Client Sample ID:MW-3
Lab Sample ID:FA1942-2 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Z13910.D 1 02/22/13 KW n/a n/a VZ591
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.21 U 1.0 0.21 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.34 U 1.0 0.34 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.26 U 1.0 0.26 ug/l
75-15-0 Carbon disulfide 0.49 U 2.0 0.49 ug/l
56-23-5 Carbon tetrachloride 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 0.21 U 1.0 0.21 ug/l
75-35-4 1,1-Dichloroethylene 0.20 U 1.0 0.20 ug/l
107-06-2 1,2-Dichloroethane 0.22 U 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane 0.26 U 1.0 0.26 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.24 U 1.0 0.24 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.22 U 1.0 0.22 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.23 U 1.0 0.23 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.21 U 1.0 0.21 ug/l
100-41-4 Ethylbenzene 0.29 U 1.0 0.29 ug/l
591-78-6 2-Hexanone 2.0 U 10 2.0 ug/l
108-10-1 4-Methyl-2-pentanone 2.3 U 5.0 2.3 ug/l
74-83-9 Methyl bromide 0.79 U 2.0 0.79 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 3.1 U 5.0 3.1 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.24 U 1.0 0.24 ug/l
79-00-5 1,1,2-Trichloroethane 0.20 U 1.0 0.20 ug/l
127-18-4 Tetrachloroethylene 0.49 1.0 0.32 ug/l J
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 0.31 U 1.0 0.31 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-3
Lab Sample ID:FA1942-2 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.44 U 1.0 0.44 ug/l
1330-20-7 Xylene (total) 0.50 U 3.0 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97% 87-116%
17060-07-0 1,2-Dichloroethane-D4 101% 76-127%
2037-26-5 Toluene-D8 99% 86-112%
460-00-4 4-Bromofluorobenzene 101% 84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-4
Lab Sample ID:FA1942-3 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Z13911.D 1 02/22/13 KW n/a n/a VZ591
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.21 U 1.0 0.21 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.34 U 1.0 0.34 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.26 U 1.0 0.26 ug/l
75-15-0 Carbon disulfide 0.49 U 2.0 0.49 ug/l
56-23-5 Carbon tetrachloride 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 0.21 U 1.0 0.21 ug/l
75-35-4 1,1-Dichloroethylene 0.20 U 1.0 0.20 ug/l
107-06-2 1,2-Dichloroethane 0.22 U 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane 0.26 U 1.0 0.26 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.24 U 1.0 0.24 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.22 U 1.0 0.22 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.23 U 1.0 0.23 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.21 U 1.0 0.21 ug/l
100-41-4 Ethylbenzene 0.29 U 1.0 0.29 ug/l
591-78-6 2-Hexanone 2.0 U 10 2.0 ug/l
108-10-1 4-Methyl-2-pentanone 2.3 U 5.0 2.3 ug/l
74-83-9 Methyl bromide 0.79 U 2.0 0.79 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 3.1 U 5.0 3.1 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.24 U 1.0 0.24 ug/l
79-00-5 1,1,2-Trichloroethane 0.20 U 1.0 0.20 ug/l
127-18-4 Tetrachloroethylene 0.32 U 1.0 0.32 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 0.31 U 1.0 0.31 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-4
Lab Sample ID:FA1942-3 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.44 U 1.0 0.44 ug/l
1330-20-7 Xylene (total) 0.50 U 3.0 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100% 87-116%
17060-07-0 1,2-Dichloroethane-D4 103% 76-127%
2037-26-5 Toluene-D8 99% 86-112%
460-00-4 4-Bromofluorobenzene 99% 84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-6
Lab Sample ID:FA1942-4 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Z13912.D 1 02/22/13 KW n/a n/a VZ591
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.21 U 1.0 0.21 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.34 U 1.0 0.34 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.26 U 1.0 0.26 ug/l
75-15-0 Carbon disulfide 0.49 U 2.0 0.49 ug/l
56-23-5 Carbon tetrachloride 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 0.21 U 1.0 0.21 ug/l
75-35-4 1,1-Dichloroethylene 0.94 1.0 0.20 ug/l J
107-06-2 1,2-Dichloroethane 0.22 U 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane 0.26 U 1.0 0.26 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.24 U 1.0 0.24 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.22 U 1.0 0.22 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.23 U 1.0 0.23 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.21 U 1.0 0.21 ug/l
100-41-4 Ethylbenzene 0.29 U 1.0 0.29 ug/l
591-78-6 2-Hexanone 2.0 U 10 2.0 ug/l
108-10-1 4-Methyl-2-pentanone 2.3 U 5.0 2.3 ug/l
74-83-9 Methyl bromide 0.79 U 2.0 0.79 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 3.1 U 5.0 3.1 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.24 U 1.0 0.24 ug/l
79-00-5 1,1,2-Trichloroethane 0.20 U 1.0 0.20 ug/l
127-18-4 Tetrachloroethylene 0.32 U 1.0 0.32 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 36.9 1.0 0.31 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-6
Lab Sample ID:FA1942-4 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.44 U 1.0 0.44 ug/l
1330-20-7 Xylene (total) 0.50 U 3.0 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99% 87-116%
17060-07-0 1,2-Dichloroethane-D4 104% 76-127%
2037-26-5 Toluene-D8 99% 86-112%
460-00-4 4-Bromofluorobenzene 99% 84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-2
Lab Sample ID:FA1942-5 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Z13913.D 1 02/22/13 KW n/a n/a VZ591
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.21 U 1.0 0.21 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.34 U 1.0 0.34 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.26 U 1.0 0.26 ug/l
75-15-0 Carbon disulfide 0.49 U 2.0 0.49 ug/l
56-23-5 Carbon tetrachloride 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 0.21 U 1.0 0.21 ug/l
75-35-4 1,1-Dichloroethylene 0.20 U 1.0 0.20 ug/l
107-06-2 1,2-Dichloroethane 0.22 U 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane 0.26 U 1.0 0.26 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.24 U 1.0 0.24 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.22 U 1.0 0.22 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.23 U 1.0 0.23 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.21 U 1.0 0.21 ug/l
100-41-4 Ethylbenzene 0.29 U 1.0 0.29 ug/l
591-78-6 2-Hexanone 2.0 U 10 2.0 ug/l
108-10-1 4-Methyl-2-pentanone 2.3 U 5.0 2.3 ug/l
74-83-9 Methyl bromide 0.79 U 2.0 0.79 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 3.1 U 5.0 3.1 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.24 U 1.0 0.24 ug/l
79-00-5 1,1,2-Trichloroethane 0.20 U 1.0 0.20 ug/l
127-18-4 Tetrachloroethylene 0.32 U 1.0 0.32 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 0.31 U 1.0 0.31 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-2
Lab Sample ID:FA1942-5 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.44 U 1.0 0.44 ug/l
1330-20-7 Xylene (total) 0.50 U 3.0 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99% 87-116%
17060-07-0 1,2-Dichloroethane-D4 102% 76-127%
2037-26-5 Toluene-D8 98% 86-112%
460-00-4 4-Bromofluorobenzene 97% 84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-1
Lab Sample ID:FA1942-6 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Z13914.D 1 02/22/13 KW n/a n/a VZ591
Run #2 Z13928.D 5 02/25/13 KW n/a n/a VZ592
Purge Volume
Run #1 5.0 ml
Run #2 5.0 ml
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.21 U 1.0 0.21 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.34 U 1.0 0.34 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.79 1.0 0.26 ug/l J
75-15-0 Carbon disulfide 0.49 U 2.0 0.49 ug/l
56-23-5 Carbon tetrachloride 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 1.3 1.0 0.21 ug/l
75-35-4 1,1-Dichloroethylene 11.1 1.0 0.20 ug/l
107-06-2 1,2-Dichloroethane 0.22 U 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane 0.26 U 1.0 0.26 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
156-59-2 cis-1,2-Dichloroethylene 30.7 1.0 0.24 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.22 U 1.0 0.22 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.40 1.0 0.23 ug/l J
10061-02-6 trans-1,3-Dichloropropene 0.21 U 1.0 0.21 ug/l
100-41-4 Ethylbenzene 0.29 U 1.0 0.29 ug/l
591-78-6 2-Hexanone 2.0 U 10 2.0 ug/l
108-10-1 4-Methyl-2-pentanone 2.3 U 5.0 2.3 ug/l
74-83-9 Methyl bromide 0.79 U 2.0 0.79 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 3.1 U 5.0 3.1 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.24 U 1.0 0.24 ug/l
79-00-5 1,1,2-Trichloroethane 0.20 U 1.0 0.20 ug/l
127-18-4 Tetrachloroethylene 98.5
a 5.0 1.6 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 127
a 5.0 1.6 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-1
Lab Sample ID:FA1942-6 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.44 U 1.0 0.44 ug/l
1330-20-7 Xylene (total) 0.50 U 3.0 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99% 98% 87-116%
17060-07-0 1,2-Dichloroethane-D4 102% 98% 76-127%
2037-26-5 Toluene-D8 96% 94% 86-112%
460-00-4 4-Bromofluorobenzene 93% 91% 84-120%
(a) Result is from Run# 2
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-9
Lab Sample ID:FA1942-7 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Z13915.D 1 02/22/13 KW n/a n/a VZ591
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.21 U 1.0 0.21 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.34 U 1.0 0.34 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.26 U 1.0 0.26 ug/l
75-15-0 Carbon disulfide 0.49 U 2.0 0.49 ug/l
56-23-5 Carbon tetrachloride 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 0.55 1.0 0.21 ug/l J
75-35-4 1,1-Dichloroethylene 0.36 1.0 0.20 ug/l J
107-06-2 1,2-Dichloroethane 0.22 U 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane 0.26 U 1.0 0.26 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
156-59-2 cis-1,2-Dichloroethylene 10.4 1.0 0.24 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.22 U 1.0 0.22 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.23 U 1.0 0.23 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.21 U 1.0 0.21 ug/l
100-41-4 Ethylbenzene 0.29 U 1.0 0.29 ug/l
591-78-6 2-Hexanone 2.0 U 10 2.0 ug/l
108-10-1 4-Methyl-2-pentanone 2.3 U 5.0 2.3 ug/l
74-83-9 Methyl bromide 0.79 U 2.0 0.79 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 3.1 U 5.0 3.1 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.24 U 1.0 0.24 ug/l
79-00-5 1,1,2-Trichloroethane 0.20 U 1.0 0.20 ug/l
127-18-4 Tetrachloroethylene 3.0 1.0 0.32 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 1.7 1.0 0.31 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-9
Lab Sample ID:FA1942-7 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.44 U 1.0 0.44 ug/l
1330-20-7 Xylene (total) 0.50 U 3.0 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100% 87-116%
17060-07-0 1,2-Dichloroethane-D4 101% 76-127%
2037-26-5 Toluene-D8 97% 86-112%
460-00-4 4-Bromofluorobenzene 94% 84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-7
Lab Sample ID:FA1942-8 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Z13916.D 1 02/22/13 KW n/a n/a VZ591
Run #2 Z13929.D 2 02/25/13 KW n/a n/a VZ592
Purge Volume
Run #1 5.0 ml
Run #2 5.0 ml
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.21 U 1.0 0.21 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.34 U 1.0 0.34 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.26 U 1.0 0.26 ug/l
75-15-0 Carbon disulfide 0.49 U 2.0 0.49 ug/l
56-23-5 Carbon tetrachloride 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 1.4 1.0 0.21 ug/l
75-35-4 1,1-Dichloroethylene 17.7 1.0 0.20 ug/l
107-06-2 1,2-Dichloroethane 0.22 U 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane 0.26 U 1.0 0.26 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
156-59-2 cis-1,2-Dichloroethylene 39.9 1.0 0.24 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.22 U 1.0 0.22 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.58 1.0 0.23 ug/l J
10061-02-6 trans-1,3-Dichloropropene 0.21 U 1.0 0.21 ug/l
100-41-4 Ethylbenzene 0.29 U 1.0 0.29 ug/l
591-78-6 2-Hexanone 2.0 U 10 2.0 ug/l
108-10-1 4-Methyl-2-pentanone 2.3 U 5.0 2.3 ug/l
74-83-9 Methyl bromide 0.79 U 2.0 0.79 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 3.1 U 5.0 3.1 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.24 U 1.0 0.24 ug/l
79-00-5 1,1,2-Trichloroethane 0.20 U 1.0 0.20 ug/l
127-18-4 Tetrachloroethylene 97.3
a 2.0 0.64 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 97.6 1.0 0.31 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-7
Lab Sample ID:FA1942-8 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.44 U 1.0 0.44 ug/l
1330-20-7 Xylene (total) 0.50 U 3.0 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101% 100% 87-116%
17060-07-0 1,2-Dichloroethane-D4 100% 97% 76-127%
2037-26-5 Toluene-D8 95% 94% 86-112%
460-00-4 4-Bromofluorobenzene 93% 90% 84-120%
(a) Result is from Run# 2
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-8
Lab Sample ID:FA1942-9 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Z13917.D 1 02/22/13 KW n/a n/a VZ591
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.21 U 1.0 0.21 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.34 U 1.0 0.34 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 1.3 1.0 0.26 ug/l
75-15-0 Carbon disulfide 0.49 U 2.0 0.49 ug/l
56-23-5 Carbon tetrachloride 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 0.21 U 1.0 0.21 ug/l
75-35-4 1,1-Dichloroethylene 0.20 U 1.0 0.20 ug/l
107-06-2 1,2-Dichloroethane 0.22 U 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane 0.26 U 1.0 0.26 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.24 U 1.0 0.24 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.22 U 1.0 0.22 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.23 U 1.0 0.23 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.21 U 1.0 0.21 ug/l
100-41-4 Ethylbenzene 0.29 U 1.0 0.29 ug/l
591-78-6 2-Hexanone 2.0 U 10 2.0 ug/l
108-10-1 4-Methyl-2-pentanone 2.3 U 5.0 2.3 ug/l
74-83-9 Methyl bromide 0.79 U 2.0 0.79 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 3.1 U 5.0 3.1 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.24 U 1.0 0.24 ug/l
79-00-5 1,1,2-Trichloroethane 0.20 U 1.0 0.20 ug/l
127-18-4 Tetrachloroethylene 0.32 U 1.0 0.32 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 0.34 1.0 0.31 ug/l J
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-8
Lab Sample ID:FA1942-9 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.44 U 1.0 0.44 ug/l
1330-20-7 Xylene (total) 0.50 U 3.0 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99% 87-116%
17060-07-0 1,2-Dichloroethane-D4 98% 76-127%
2037-26-5 Toluene-D8 96% 86-112%
460-00-4 4-Bromofluorobenzene 92% 84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:TRIP BLANK
Lab Sample ID:FA1942-10 Date Sampled:02/20/13
Matrix:AQ - Trip Blank Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Z13918.D 1 02/22/13 KW n/a n/a VZ591
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.21 U 1.0 0.21 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.34 U 1.0 0.34 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.26 U 1.0 0.26 ug/l
75-15-0 Carbon disulfide 0.49 U 2.0 0.49 ug/l
56-23-5 Carbon tetrachloride 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 0.21 U 1.0 0.21 ug/l
75-35-4 1,1-Dichloroethylene 0.20 U 1.0 0.20 ug/l
107-06-2 1,2-Dichloroethane 0.22 U 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane 0.26 U 1.0 0.26 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.24 U 1.0 0.24 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.22 U 1.0 0.22 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.23 U 1.0 0.23 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.21 U 1.0 0.21 ug/l
100-41-4 Ethylbenzene 0.29 U 1.0 0.29 ug/l
591-78-6 2-Hexanone 2.0 U 10 2.0 ug/l
108-10-1 4-Methyl-2-pentanone 2.3 U 5.0 2.3 ug/l
74-83-9 Methyl bromide 0.79 U 2.0 0.79 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 3.1 U 5.0 3.1 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.24 U 1.0 0.24 ug/l
79-00-5 1,1,2-Trichloroethane 0.20 U 1.0 0.20 ug/l
127-18-4 Tetrachloroethylene 0.32 U 1.0 0.32 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 0.31 U 1.0 0.31 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:TRIP BLANK
Lab Sample ID:FA1942-10 Date Sampled:02/20/13
Matrix:AQ - Trip Blank Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.44 U 1.0 0.44 ug/l
1330-20-7 Xylene (total) 0.50 U 3.0 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99% 87-116%
17060-07-0 1,2-Dichloroethane-D4 98% 76-127%
2037-26-5 Toluene-D8 96% 86-112%
460-00-4 4-Bromofluorobenzene 92% 84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:DUP 1
Lab Sample ID:FA1942-11 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Z13919.D 1 02/22/13 KW n/a n/a VZ591
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.21 U 1.0 0.21 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.34 U 1.0 0.34 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 1.2 1.0 0.26 ug/l
75-15-0 Carbon disulfide 0.49 U 2.0 0.49 ug/l
56-23-5 Carbon tetrachloride 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 0.21 U 1.0 0.21 ug/l
75-35-4 1,1-Dichloroethylene 0.20 U 1.0 0.20 ug/l
107-06-2 1,2-Dichloroethane 0.22 U 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane 0.26 U 1.0 0.26 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.24 U 1.0 0.24 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.22 U 1.0 0.22 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.23 U 1.0 0.23 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.21 U 1.0 0.21 ug/l
100-41-4 Ethylbenzene 0.29 U 1.0 0.29 ug/l
591-78-6 2-Hexanone 2.0 U 10 2.0 ug/l
108-10-1 4-Methyl-2-pentanone 2.3 U 5.0 2.3 ug/l
74-83-9 Methyl bromide 0.79 U 2.0 0.79 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 3.1 U 5.0 3.1 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.24 U 1.0 0.24 ug/l
79-00-5 1,1,2-Trichloroethane 0.20 U 1.0 0.20 ug/l
127-18-4 Tetrachloroethylene 0.32 U 1.0 0.32 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 0.38 1.0 0.31 ug/l J
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:DUP 1
Lab Sample ID:FA1942-11 Date Sampled:02/20/13
Matrix:AQ - Ground Water Date Received:02/21/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.44 U 1.0 0.44 ug/l
1330-20-7 Xylene (total) 0.50 U 3.0 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100% 87-116%
17060-07-0 1,2-Dichloroethane-D4 97% 76-127%
2037-26-5 Toluene-D8 96% 86-112%
460-00-4 4-Bromofluorobenzene 91% 84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 5
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FA1942: Chain of Custody
Page 2 of 2
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GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
• Instrument Performance Checks (BFB)
• Internal Standard Area Summaries
• Surrogate Recovery Summaries
• Initial and Continuing Calibration Summaries
Southeast
Section 6
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Method Blank Summar y Page 1 of 2
Job Number:FA1942
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VZ591-MB Z13899.D 1 02/22/13 KW n/a n/a VZ591
The QC reported here applies to the following samples:Method:SW846 8260B
FA1942-1, FA1942-2, FA1942-3, FA1942-4, FA1942-5, FA1942-6, FA1942-7, FA1942-8, FA1942-9, FA1942-10,
FA1942-11
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.21 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.20 ug/l
75-25-2 Bromoform ND 1.0 0.34 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.50 ug/l
67-66-3 Chloroform ND 1.0 0.26 ug/l
75-15-0 Carbon disulfide ND 2.0 0.49 ug/l
56-23-5 Carbon tetrachloride ND 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.21 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.20 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.26 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.20 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.24 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.22 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.23 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
100-41-4 Ethylbenzene ND 1.0 0.29 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
108-10-1 4-Methyl-2-pentanone ND 5.0 2.3 ug/l
74-83-9 Methyl bromide ND 2.0 0.79 ug/l
74-87-3 Methyl chloride ND 2.0 0.50 ug/l
75-09-2 Methylene chloride ND 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone ND 5.0 3.1 ug/l
100-42-5 Styrene ND 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.24 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.20 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.32 ug/l
108-88-3 Toluene ND 1.0 0.20 ug/l
79-01-6 Trichloroethylene ND 1.0 0.31 ug/l
75-01-4 Vinyl chloride ND 1.0 0.44 ug/l
1330-20-7 Xylene (total) ND 3.0 0.50 ug/l
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Method Blank Summar y Page 2 of 2
Job Number:FA1942
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VZ591-MB Z13899.D 1 02/22/13 KW n/a n/a VZ591
The QC reported here applies to the following samples:Method:SW846 8260B
FA1942-1, FA1942-2, FA1942-3, FA1942-4, FA1942-5, FA1942-6, FA1942-7, FA1942-8, FA1942-9, FA1942-10,
FA1942-11
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 98% 87-116%
17060-07-0 1,2-Dichloroethane-D4 102% 76-127%
2037-26-5 Toluene-D8 98% 86-112%
460-00-4 4-Bromofluorobenzene 102% 84-120%
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Method Blank Summar y Page 1 of 1
Job Number:FA1942
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VZ592-MB Z13927.D 1 02/25/13 KW n/a n/a VZ592
The QC reported here applies to the following samples:Method:SW846 8260B
FA1942-6, FA1942-8
CAS No.Compound Result RL MDL Units Q
127-18-4 Tetrachloroethylene ND 1.0 0.32 ug/l
79-01-6 Trichloroethylene ND 1.0 0.31 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99% 87-116%
17060-07-0 1,2-Dichloroethane-D4 97% 76-127%
2037-26-5 Toluene-D8 94% 86-112%
460-00-4 4-Bromofluorobenzene 93% 84-120%
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Blank Spike Summar y Page 1 of 2
Job Number:FA1942
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VZ591-BS Z13897.D 1 02/22/13 KW n/a n/a VZ591
The QC reported here applies to the following samples:Method:SW846 8260B
FA1942-1, FA1942-2, FA1942-3, FA1942-4, FA1942-5, FA1942-6, FA1942-7, FA1942-8, FA1942-9, FA1942-10,
FA1942-11
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
67-64-1 Acetone 125 148 118 59-134
71-43-2 Benzene 25 27.6 110 83-124
75-27-4 Bromodichloromethane 25 26.0 104 76-116
75-25-2 Bromoform 25 24.1 96 68-128
108-90-7 Chlorobenzene 25 28.6 114 87-115
75-00-3 Chloroethane 25 31.4 126 54-166
67-66-3 Chloroform 25 26.0 104 85-123
75-15-0 Carbon disulfide 25 30.2 121 67-147
56-23-5 Carbon tetrachloride 25 27.9 112 74-139
75-34-3 1,1-Dichloroethane 25 27.1 108 82-127
75-35-4 1,1-Dichloroethylene 25 30.6 122 75-133
107-06-2 1,2-Dichloroethane 25 26.0 104 76-122
78-87-5 1,2-Dichloropropane 25 26.1 104 81-120
124-48-1 Dibromochloromethane 25 25.5 102 74-116
156-59-2 cis-1,2-Dichloroethylene 25 26.4 106 81-114
10061-01-5 cis-1,3-Dichloropropene 25 25.0 100 83-119
156-60-5 trans-1,2-Dichloroethylene 25 27.2 109 82-126
10061-02-6 trans-1,3-Dichloropropene 25 26.6 106 87-123
100-41-4 Ethylbenzene 25 27.7 111 87-118
591-78-6 2-Hexanone 125 122 98 58-125
108-10-1 4-Methyl-2-pentanone 125 118 94 62-125
74-83-9 Methyl bromide 25 30.4 122 55-151
74-87-3 Methyl chloride 25 28.4 114 55-173
75-09-2 Methylene chloride 25 24.7 99 69-125
78-93-3 Methyl ethyl ketone 125 138 110 61-127
100-42-5 Styrene 25 26.3 105 78-118
71-55-6 1,1,1-Trichloroethane 25 27.7 111 79-133
79-34-5 1,1,2,2-Tetrachloroethane 25 24.3 97 71-120
79-00-5 1,1,2-Trichloroethane 25 25.1 100 80-114
127-18-4 Tetrachloroethylene 25 27.8 111 80-131
108-88-3 Toluene 25 27.3 109 86-116
79-01-6 Trichloroethylene 25 27.3 109 85-124
75-01-4 Vinyl chloride 25 28.8 115 57-153
1330-20-7 Xylene (total) 75 85.1 113 86-120
* = Outside of Control Limits.
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Blank Spike Summar y Page 2 of 2
Job Number:FA1942
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VZ591-BS Z13897.D 1 02/22/13 KW n/a n/a VZ591
The QC reported here applies to the following samples:Method:SW846 8260B
FA1942-1, FA1942-2, FA1942-3, FA1942-4, FA1942-5, FA1942-6, FA1942-7, FA1942-8, FA1942-9, FA1942-10,
FA1942-11
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100% 87-116%
17060-07-0 1,2-Dichloroethane-D4 100% 76-127%
2037-26-5 Toluene-D8 100% 86-112%
460-00-4 4-Bromofluorobenzene 99% 84-120%
* = Outside of Control Limits.
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Blank Spike Summar y Page 1 of 1
Job Number:FA1942
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VZ592-BS Z13925.D 1 02/25/13 KW n/a n/a VZ592
The QC reported here applies to the following samples:Method:SW846 8260B
FA1942-6, FA1942-8
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
127-18-4 Tetrachloroethylene 25 27.7 111 80-131
79-01-6 Trichloroethylene 25 26.7 107 85-124
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 99% 87-116%
17060-07-0 1,2-Dichloroethane-D4 98% 76-127%
2037-26-5 Toluene-D8 95% 86-112%
460-00-4 4-Bromofluorobenzene 92% 84-120%
* = Outside of Control Limits.
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Matr ix Spike/Matr ix Spike Duplicate Summary Page 1 of 2
Job Number:FA1942
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA1711-1MS Z13904.D 1 02/22/13 KW n/a n/a VZ591
FA1711-1MSD Z13905.D 1 02/22/13 KW n/a n/a VZ591
FA1711-1 Z13903.D 1 02/22/13 KW n/a n/a VZ591
The QC reported here applies to the following samples:Method:SW846 8260B
FA1942-1, FA1942-2, FA1942-3, FA1942-4, FA1942-5, FA1942-6, FA1942-7, FA1942-8, FA1942-9, FA1942-10,
FA1942-11
FA1711-1 Spike MS MS MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l %RPD Rec/RPD
67-64-1 Acetone ND 125 102 82 112 90 9 59-134/14
71-43-2 Benzene ND 25 26.7 107 27.2 109 2 83-124/11
75-27-4 Bromodichloromethane ND 25 23.9 96 23.0 92 4 76-116/10
75-25-2 Bromoform ND 25 21.0 84 19.9 80 5 68-128/11
108-90-7 Chlorobenzene ND 25 28.0 112 28.9 116* 3 87-115/9
75-00-3 Chloroethane ND 25 36.1 144 36.2 145 0 54-166/20
67-66-3 Chloroform ND 25 25.3 101 26.2 105 3 85-123/10
75-15-0 Carbon disulfide ND 25 23.2 93 21.9 88 6 67-147/12
56-23-5 Carbon tetrachloride ND 25 25.2 101 24.0 96 5 74-139/13
75-34-3 1,1-Dichloroethane ND 25 26.6 106 27.1 108 2 82-127/10
75-35-4 1,1-Dichloroethylene ND 25 28.8 115 30.4 122 5 75-133/13
107-06-2 1,2-Dichloroethane ND 25 26.2 105 27.0 108 3 76-122/11
78-87-5 1,2-Dichloropropane ND 25 25.8 103 27.0 108 5 81-120/11
124-48-1 Dibromochloromethane ND 25 22.6 90 22.0 88 3 74-116/11
156-59-2 cis-1,2-Dichloroethylene ND 25 25.4 102 26.4 106 4 81-114/10
10061-01-5 cis-1,3-Dichloropropene ND 25 22.5 90 21.4 86 5 83-119/10
156-60-5 trans-1,2-Dichloroethylene ND 25 26.2 105 26.6 106 2 82-126/10
10061-02-6 trans-1,3-Dichloropropene ND 25 23.6 94 22.7 91 4 87-123/10
100-41-4 Ethylbenzene ND 25 26.5 106 27.7 111 4 87-118/10
591-78-6 2-Hexanone ND 125 112 90 122 98 9 58-125/14
108-10-1 4-Methyl-2-pentanone ND 125 119 95 130 104 9 62-125/13
74-83-9 Methyl bromide ND 25 34.7 139 34.7 139 0 55-151/21
74-87-3 Methyl chloride ND 25 28.4 114 29.3 117 3 55-173/22
75-09-2 Methylene chloride ND 25 24.7 99 26.2 105 6 69-125/11
78-93-3 Methyl ethyl ketone ND 125 113 90 122 98 8 61-127/13
100-42-5 Styrene ND 25 24.1 96 24.5 98 2 78-118/11
71-55-6 1,1,1-Trichloroethane ND 25 25.3 101 25.7 103 2 79-133/11
79-34-5 1,1,2,2-Tetrachloroethane ND 25 23.0 92 25.2 101 9 71-120/11
79-00-5 1,1,2-Trichloroethane ND 25 24.2 97 25.6 102 6 80-114/11
127-18-4 Tetrachloroethylene ND 25 26.5 106 27.3 109 3 80-131/12
108-88-3 Toluene ND 25 25.8 103 27.1 108 5 86-116/10
79-01-6 Trichloroethylene ND 25 26.1 104 26.5 106 2 85-124/10
75-01-4 Vinyl chloride ND 25 31.6 126 32.8 131 4 57-153/22
1330-20-7 Xylene (total) ND 75 80.3 107 83.1 111 3 86-120/10
* = Outside of Control Limits.
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Matr ix Spike/Matr ix Spike Duplicate Summary Page 2 of 2
Job Number:FA1942
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA1711-1MS Z13904.D 1 02/22/13 KW n/a n/a VZ591
FA1711-1MSD Z13905.D 1 02/22/13 KW n/a n/a VZ591
FA1711-1 Z13903.D 1 02/22/13 KW n/a n/a VZ591
The QC reported here applies to the following samples:Method:SW846 8260B
FA1942-1, FA1942-2, FA1942-3, FA1942-4, FA1942-5, FA1942-6, FA1942-7, FA1942-8, FA1942-9, FA1942-10,
FA1942-11
CAS No.Surrogate Recoveries MS MSD FA1711-1 Limits
1868-53-7 Dibromofluoromethane 100% 101% 99% 87-116%
17060-07-0 1,2-Dichloroethane-D4 101% 101% 102% 76-127%
2037-26-5 Toluene-D8 98% 97% 96% 86-112%
460-00-4 4-Bromofluorobenzene 95% 96% 98% 84-120%
* = Outside of Control Limits.
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Matr ix Spike/Matr ix Spike Duplicate Summary Page 1 of 1
Job Number:FA1942
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA1942-6MS Z13930.D 5 02/25/13 KW n/a n/a VZ592
FA1942-6MSD Z13931.D 5 02/25/13 KW n/a n/a VZ592
FA1942-6 Z13928.D 5 02/25/13 KW n/a n/a VZ592
The QC reported here applies to the following samples:Method:SW846 8260B
FA1942-6, FA1942-8
FA1942-6 Spike MS MS MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l %RPD Rec/RPD
127-18-4 Tetrachloroethylene 98.5 125 234 108 246 118 5 80-131/12
79-01-6 Trichloroethylene 127 125 255 102 268 113 5 85-124/10
CAS No.Surrogate Recoveries MS MSD FA1942-6 Limits
1868-53-7 Dibromofluoromethane 101% 102% 98% 87-116%
17060-07-0 1,2-Dichloroethane-D4 97% 97% 98% 76-127%
2037-26-5 Toluene-D8 94% 94% 94% 86-112%
460-00-4 4-Bromofluorobenzene 89% 90% 91% 84-120%
* = Outside of Control Limits.
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Instrument Per formance Check (BFB)Page 1 of 2
Job Number:FA1942
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample:VZ591-BFB Injection Date:02/22/13
Lab File ID:Z13888.D Injection Time:09:22
Instrument ID:GCMSZ
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 15.0 - 40.0% of mass 95 73328 23.4 Pass
75 30.0 - 60.0% of mass 95 138676 44.2 Pass
95 Base peak, 100% relative abundance 313842 100.0 Pass
96 5.0 - 9.0% of mass 95 20762 6.62 Pass
173 Less than 2.0% of mass 174 1366 0.44 (0.56)
a Pass
174 50.0 - 100.0% of mass 95 244757 78.0 Pass
175 5.0 - 9.0% of mass 174 16502 5.26 (6.74)
a Pass
176 95.0 - 101.0% of mass 174 233899 74.5 (95.6)
a Pass
177 5.0 - 9.0% of mass 176 15060 4.80 (6.44)
b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
VZ591-IC591 Z13889.D 02/22/13 09:43 00:21 Initial cal 1
VZ591-IC591 Z13890.D 02/22/13 10:06 00:44 Initial cal 2
VZ591-IC591 Z13891.D 02/22/13 10:29 01:07 Initial cal 3
VZ591-ICC591 Z13892.D 02/22/13 10:51 01:29 Initial cal 4
VZ591-IC591 Z13893.D 02/22/13 11:14 01:52 Initial cal 5
VZ591-IC591 Z13894.D 02/22/13 11:37 02:15 Initial cal 6
VZ591-ICV591 Z13896.D 02/22/13 12:22 03:00 Initial cal verification 4
VZ591-BS Z13897.D 02/22/13 12:48 03:26 Blank Spike
VZ591-MB Z13899.D 02/22/13 13:32 04:10 Method Blank
ZZZZZZ Z13900.D 02/22/13 13:53 04:31 (unrelated sample)
ZZZZZZ Z13901.D 02/22/13 14:14 04:52 (unrelated sample)
ZZZZZZ Z13902.D 02/22/13 14:35 05:13 (unrelated sample)
FA1711-1 Z13903.D 02/22/13 14:56 05:34 (used for QC only; not part of job FA1942)
FA1711-1MS Z13904.D 02/22/13 15:17 05:55 Matrix Spike
FA1711-1MSD Z13905.D 02/22/13 15:37 06:15 Matrix Spike Duplicate
ZZZZZZ Z13906.D 02/22/13 16:00 06:38 (unrelated sample)
ZZZZZZ Z13908.D 02/22/13 16:42 07:20 (unrelated sample)
FA1942-1 Z13909.D 02/22/13 17:03 07:41 MW-5
FA1942-2 Z13910.D 02/22/13 17:24 08:02 MW-3
FA1942-3 Z13911.D 02/22/13 17:45 08:23 MW-4
FA1942-4 Z13912.D 02/22/13 18:06 08:44 MW-6
FA1942-5 Z13913.D 02/22/13 18:26 09:04 MW-2
FA1942-6 Z13914.D 02/22/13 18:47 09:25 MW-1
FA1942-7 Z13915.D 02/22/13 19:08 09:46 MW-9
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Instrument Per formance Check (BFB)Page 2 of 2
Job Number:FA1942
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample:VZ591-BFB Injection Date:02/22/13
Lab File ID:Z13888.D Injection Time:09:22
Instrument ID:GCMSZ
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
FA1942-8 Z13916.D 02/22/13 19:29 10:07 MW-7
FA1942-9 Z13917.D 02/22/13 19:50 10:28 MW-8
FA1942-10 Z13918.D 02/22/13 20:11 10:49 TRIP BLANK
FA1942-11 Z13919.D 02/22/13 20:32 11:10 DUP 1
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Instrument Per formance Check (BFB)Page 1 of 2
Job Number:FA1942
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample:VZ592-BFB Injection Date:02/25/13
Lab File ID:Z13922.D Injection Time:08:46
Instrument ID:GCMSZ
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 15.0 - 40.0% of mass 95 73632 25.5 Pass
75 30.0 - 60.0% of mass 95 132896 46.0 Pass
95 Base peak, 100% relative abundance 288832 100.0 Pass
96 5.0 - 9.0% of mass 95 19372 6.71 Pass
173 Less than 2.0% of mass 174 1375 0.48 (0.57)
a Pass
174 50.0 - 100.0% of mass 95 242112 83.8 Pass
175 5.0 - 9.0% of mass 174 17541 6.07 (7.24)
a Pass
176 95.0 - 101.0% of mass 174 231488 80.1 (95.6)
a Pass
177 5.0 - 9.0% of mass 176 14714 5.09 (6.36)
b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
VZ592-CC591 Z13924.D 02/25/13 09:36 00:50 Continuing cal 4
VZ592-BS Z13925.D 02/25/13 10:00 01:14 Blank Spike
VZ592-MB Z13927.D 02/25/13 10:45 01:59 Method Blank
FA1942-6 Z13928.D 02/25/13 11:06 02:20 MW-1
FA1942-8 Z13929.D 02/25/13 11:27 02:41 MW-7
FA1942-6MS Z13930.D 02/25/13 11:47 03:01 Matrix Spike
FA1942-6MSD Z13931.D 02/25/13 12:08 03:22 Matrix Spike Duplicate
ZZZZZZ Z13932.D 02/25/13 12:31 03:45 (unrelated sample)
ZZZZZZ Z13933.D 02/25/13 12:51 04:05 (unrelated sample)
ZZZZZZ Z13934.D 02/25/13 13:12 04:26 (unrelated sample)
ZZZZZZ Z13935.D 02/25/13 13:34 04:48 (unrelated sample)
ZZZZZZ Z13936.D 02/25/13 13:55 05:09 (unrelated sample)
ZZZZZZ Z13937.D 02/25/13 14:16 05:30 (unrelated sample)
ZZZZZZ Z13938.D 02/25/13 14:37 05:51 (unrelated sample)
ZZZZZZ Z13939.D 02/25/13 14:58 06:12 (unrelated sample)
ZZZZZZ Z13940.D 02/25/13 15:19 06:33 (unrelated sample)
ZZZZZZ Z13941.D 02/25/13 15:40 06:54 (unrelated sample)
ZZZZZZ Z13942.D 02/25/13 16:01 07:15 (unrelated sample)
ZZZZZZ Z13943.D 02/25/13 16:22 07:36 (unrelated sample)
ZZZZZZ Z13944.D 02/25/13 16:43 07:57 (unrelated sample)
ZZZZZZ Z13945.D 02/25/13 17:04 08:18 (unrelated sample)
ZZZZZZ Z13946.D 02/25/13 17:25 08:39 (unrelated sample)
ZZZZZZ Z13947.D 02/25/13 17:46 09:00 (unrelated sample)
ZZZZZZ Z13948.D 02/25/13 18:07 09:21 (unrelated sample)
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Instrument Per formance Check (BFB)Page 2 of 2
Job Number:FA1942
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample:VZ592-BFB Injection Date:02/25/13
Lab File ID:Z13922.D Injection Time:08:46
Instrument ID:GCMSZ
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
ZZZZZZ Z13949.D 02/25/13 18:28 09:42 (unrelated sample)
ZZZZZZ Z13950.D 02/25/13 18:50 10:04 (unrelated sample)
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Volatile Internal Standar d Ar ea Summar y Page 1 of 1
Job Number:FA1942
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Check Std:VZ591-ICC591 Injection Date:02/22/13
Lab File ID:Z13892.D Injection Time:10:51
Instrument ID:GCMSZ Method:SW846 8260B
IS 1 IS 2 IS 3 IS 4
AREA RT AREA RT AREA RT AREA RT
Initial Cal a 1425705 7.79 1059353 10.89 560196 13.26 174155 5.29
Check Std b 1425705 7.79 1059353 10.89 560196 13.26 174155 5.29
Upper Limit c 2851410 8.29 2118706 11.39 1120392 13.76 348310 5.79
Lower Limit d 712853 7.29 529677 10.39 280098 12.76 87078 4.79
Lab IS 1 IS 2 IS 3 IS 4
Sample ID AREA RT AREA RT AREA RT AREA RT
VZ591-BS 1334365 7.79 1012658 10.89 535229 13.26 153811 5.30
VZ591-MB 1285326 7.79 985154 10.89 501724 13.26 150607 5.30
ZZZZZZ 1129290 7.79 872507 10.89 446722 13.26 155525 5.29
ZZZZZZ 1079268 7.79 825710 10.89 424551 13.26 117316 5.29
ZZZZZZ 1135871 7.79 867119 10.89 446327 13.26 124371 5.30
FA1711-1 1070847 7.79 836389 10.89 420992 13.26 109928 5.29
FA1711-1MS 1042647 7.79 812506 10.89 437874 13.26 116355 5.28
FA1711-1MSD 1064217 7.79 827610 10.89 437081 13.26 122044 5.30
ZZZZZZ 1110329 7.79 876651 10.89 480594 13.26 140719 5.30
ZZZZZZ 1213360 7.79 933668 10.89 493142 13.26 151338 5.29
FA1942-1 1218991 7.79 936044 10.89 476170 13.26 140981 5.29
FA1942-2 1196480 7.79 909597 10.89 460163 13.26 140027 5.30
FA1942-3 1128379 7.79 846075 10.89 434861 13.26 128859 5.30
FA1942-4 1055359 7.78 804029 10.89 413612 13.26 117216 5.29
FA1942-5 987130 7.78 756730 10.89 386705 13.26 106818 5.29
FA1942-6 929786 7.79 726172 10.89 377097 13.26 103154 5.30
FA1942-7 899863 7.79 698705 10.89 363301 13.26 96159 5.30
FA1942-8 872385 7.79 687744 10.89 353417 13.26 94202 5.30
FA1942-9 848874 7.79 663449 10.89 343915 13.26 88843 5.30
FA1942-10 828910 7.79 648209 10.89 335207 13.26 83342* 5.30
FA1942-11 714584 7.78 558784 10.89 289240 13.26 78837* 5.29
IS 1 = Fluorobenzene
IS 2 = Chlorobenzene-D5
IS 3 = 1,4-Dichlorobenzene-d4
IS 4 = Tert Butyl Alcohol-D10
(a) Initial Cal is: VZ591-ICC591 Z13892.D 02/22/13 10:51
(b) Check Std Limit = -50 to +100% of initial cal area.
(c) Upper Limit = +100% of check standard area; Retention time +0.5 minutes.
(d) Lower Limit = -50% of check standard area; Retention time -0.5 minutes.
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Volatile Internal Standar d Ar ea Summar y Page 1 of 2
Job Number:FA1942
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Check Std:VZ592-CC591 Injection Date:02/25/13
Lab File ID:Z13924.D Injection Time:09:36
Instrument ID:GCMSZ Method:SW846 8260B
IS 1 IS 2 IS 3 IS 4
AREA RT AREA RT AREA RT AREA RT
Initial Cal a 1425705 7.79 1059353 10.89 560196 13.26 174155 5.29
Check Std b 1235863 7.78 974058 10.89 530476 13.26 131246 5.29
Upper Limit c 2471726 8.28 1948116 11.39 1060952 13.76 262492 5.79
Lower Limit d 617932 7.28 487029 10.39 265238 12.76 65623 4.79
Lab IS 1 IS 2 IS 3 IS 4
Sample ID AREA RT AREA RT AREA RT AREA RT
VZ592-BS 1248334 7.79 976040 10.89 519943 13.26 143232 5.29
VZ592-MB 1181011 7.79 923359 10.89 475091 13.26 132558 5.30
FA1942-6 1118817 7.79 876927 10.89 449413 13.26 117240 5.30
FA1942-8 1054010 7.79 830662 10.89 428171 13.26 109405 5.30
FA1942-6MS 1042058 7.79 816282 10.89 446284 13.26 112448 5.30
FA1942-6MSD 1116349 7.78 871782 10.89 473890 13.26 118326 5.29
ZZZZZZ 964534 7.79 780234 10.89 435616 13.26 130629 5.29
ZZZZZZ 1233841 7.79 946329 10.89 482555 13.26 137393 5.29
ZZZZZZ 1145900 7.79 872827 10.89 446956 13.26 133156 5.30
ZZZZZZ 1192666 7.79 915327 10.89 460672 13.26 122664 5.30
ZZZZZZ 1121003 7.79 875245 10.89 439726 13.26 115286 5.29
ZZZZZZ 1065660 7.79 825157 10.89 423930 13.26 115661 5.29
ZZZZZZ 1036930 7.79 812549 10.89 411144 13.26 109086 5.30
ZZZZZZ 1004853 7.79 797532 10.89 405993 13.26 107512 5.29
ZZZZZZ 832625 7.79 658591 10.89 334439 13.26 96304 5.30
ZZZZZZ 979000 7.79 771022 10.89 388268 13.26 112339 5.30
ZZZZZZ 943532 7.79 754027 10.89 379421 13.26 103031 5.29
ZZZZZZ 920237 7.79 732936 10.89 369153 13.26 104513 5.30
ZZZZZZ 920327 7.78 728570 10.89 363663 13.26 100390 5.29
ZZZZZZ 888789 7.79 711297 10.89 357437 13.26 95842 5.29
ZZZZZZ 875105 7.79 699175 10.89 351137 13.26 96952 5.30
ZZZZZZ 849020 7.79 681011 10.89 346629 13.26 96838 5.30
ZZZZZZ 856893 7.79 688003 10.89 349791 13.26 92387 5.30
ZZZZZZ 854549 7.79 687414 10.89 359299 13.26 87357 5.29
ZZZZZZ 859769 7.79 692383 10.89 351179 13.26 89853 5.30
IS 1 = Fluorobenzene
IS 2 = Chlorobenzene-D5
IS 3 = 1,4-Dichlorobenzene-d4
IS 4 = Tert Butyl Alcohol-D10
(a) Initial Cal is: VZ591-ICC591 Z13892.D 02/22/13 10:51
(b) Check Std Limit = -50 to +100% of initial cal area.
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Volatile Internal Standar d Ar ea Summar y Page 2 of 2
Job Number:FA1942
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Check Std:VZ592-CC591 Injection Date:02/25/13
Lab File ID:Z13924.D Injection Time:09:36
Instrument ID:GCMSZ Method:SW846 8260B
Lab IS 1 IS 2 IS 3 IS 4
Sample ID AREA RT AREA RT AREA RT AREA RT
(c) Upper Limit = +100% of check standard area; Retention time +0.5 minutes.
(d) Lower Limit = -50% of check standard area; Retention time -0.5 minutes.
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Volatile Sur r ogate Recovery Summary Page 1 of 1
Job Number:FA1942
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Method:SW846 8260B Matr ix:AQ
Samples and QC shown here apply to the above method
Lab Lab
Sample ID File ID S1 S2 S3 S4
FA1942-1 Z13909.D 100.0 101.0 98.0 101.0
FA1942-2 Z13910.D 97.0 101.0 99.0 101.0
FA1942-3 Z13911.D 100.0 103.0 99.0 99.0
FA1942-4 Z13912.D 99.0 104.0 99.0 99.0
FA1942-5 Z13913.D 99.0 102.0 98.0 97.0
FA1942-6 Z13914.D 99.0 102.0 96.0 93.0
FA1942-6 Z13928.D 98.0 98.0 94.0 91.0
FA1942-7 Z13915.D 100.0 101.0 97.0 94.0
FA1942-8 Z13916.D 101.0 100.0 95.0 93.0
FA1942-8 Z13929.D 100.0 97.0 94.0 90.0
FA1942-9 Z13917.D 99.0 98.0 96.0 92.0
FA1942-10 Z13918.D 99.0 98.0 96.0 92.0
FA1942-11 Z13919.D 100.0 97.0 96.0 91.0
FA1711-1MS Z13904.D 100.0 101.0 98.0 95.0
FA1711-1MSD Z13905.D 101.0 101.0 97.0 96.0
FA1942-6MS Z13930.D 101.0 97.0 94.0 89.0
FA1942-6MSD Z13931.D 102.0 97.0 94.0 90.0
VZ591-BS Z13897.D 100.0 100.0 100.0 99.0
VZ591-MB Z13899.D 98.0 102.0 98.0 102.0
VZ592-BS Z13925.D 99.0 98.0 95.0 92.0
VZ592-MB Z13927.D 99.0 97.0 94.0 93.0
Surrogate Recovery
Compounds Limits
S1 = Dibromofluoromethane 87-116%
S2 = 1,2-Dichloroethane-D4 76-127%
S3 = Toluene-D8 86-112%
S4 = 4-Bromofluorobenzene 84-120%
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Initial Calibr ation Summar y Page 1 of 3
Job Number:FA1942 Sample:VZ591-ICC591
Account:AMECPAP AMEC Environment & Infrastructure, Inc.Lab FileID:Z13892.D
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Response Factor Report MSVOA15
Method : C:\msdchem\1\METHODS\8260.M (RTE Integrator)
Title : EPA 624 & SWA 5030B/8260B
Last Update : Fri Feb 22 12:33:35 2013
Response via : Initial Calibration
Calibration Files
1 =Z13889.D 2 =Z13890.D 3 =Z13891.D 4 =Z13892.D
5 =Z13893.D 6 =Z13894.D
Compound 1 2 3 4 5 6 Avg %RSD
---------------------------------------------------------------------------
1) I Fluorobenzene ----------------ISTD---------------------
2) Dichlorodifluoromet 0.208 0.186 0.279 0.297 0.311 0.267 0.258 19.42
---- Quadratic regr., Force(0,0) ---- Coefficient = 0.9948
Response Ratio = 0.00000 + 0.33469 *A + -0.03117 *A^2
3) P Chloromethane 0.397 0.351 0.465 0.487 0.492 0.447 0.440 12.59
4) C Vinyl Chloride 0.300 0.246 0.358 0.384 0.385 0.345 0.336 16.14
---- Quadratic regr., Force(0,0) ---- Coefficient = 0.9979
Response Ratio = 0.00000 + 0.41473 *A + -0.03238 *A^2
5) Bromomethane 0.161 0.131 0.154 0.151 0.131 0.111 0.140 13.38
6) Chloroethane 0.165 0.127 0.169 0.176 0.155 0.128 0.153 13.89
7) Trichlorofluorometh 0.284 0.239 0.343 0.363 0.391 0.323 0.324 17.11
---- Quadratic regr., Force(0,0) ---- Coefficient = 0.9917
Response Ratio = 0.00000 + 0.42338 *A + -0.04559 *A^2
8) Ethyl Ether 0.300 0.268 0.306 0.298 0.307 0.295 0.296 4.81
9) 1,2-Dichlorotrifluo 0.310 0.269 0.379 0.367 0.372 0.360 0.343 12.82
10) Freon 113 0.219 0.213 0.285 0.279 0.290 0.270 0.260 13.29
11) C 1,1-Dichloroethene 0.393 0.377 0.516 0.498 0.504 0.490 0.463 13.23
12) Acetone 0.127 0.084 0.083 0.082 0.087 0.080 0.091 19.64
---- Quadratic regr., Force(0,0) ---- Coefficient = 0.9979
Response Ratio = 0.00000 + 0.08935 *A + -0.00079 *A^2
13) Iodomethane 0.422 0.386 0.493 0.485 0.486 0.476 0.458 9.51
14) Carbon Disulfide 0.750 0.557 0.759 0.734 0.744 0.723 0.711 10.79
15) Methyl acetate 0.194 0.173 0.205 0.207 0.222 0.206 0.201 8.33
16) Methylene Chloride 0.798 0.467 0.507 0.492 0.488 0.480 0.539 23.70
---- Quadratic regr., Force(0,0) ---- Coefficient = 0.9999
Response Ratio = 0.00000 + 0.50534 *A + -0.01280 *A^2
17) Methyl Tert Butyl E 0.774 0.694 0.823 0.815 0.833 0.800 0.790 6.47
18) trans-1,2-Dichloroe 0.472 0.428 0.553 0.536 0.538 0.526 0.509 9.53
19) Acrylonitrile 0.108 0.112 0.134 0.133 0.142 0.129 0.126 10.63
20) Hexane 0.776 0.604 0.776 0.761 0.785 0.741 0.741 9.26
21) Di-isopropyl ether 1.093 1.000 1.194 1.163 1.162 1.147 1.127 6.24
22) Vinyl acetate 0.393 0.386 0.465 0.465 0.483 0.423 0.436 9.40
23) P 1,1-Dichloroethane 0.549 0.509 0.652 0.640 0.638 0.624 0.602 9.77
24) ETBE 1.082 0.993 1.182 1.164 1.183 1.151 1.126 6.64
25) 2-Butanone 0.117 0.109 0.129 0.133 0.141 0.131 0.127 9.20
26) 2,2-Dichloropropane 0.413 0.343 0.430 0.415 0.408 0.397 0.401 7.55
27) cis-1,2-Dichloroeth 0.303 0.251 0.319 0.309 0.308 0.302 0.298 8.04
28) Bromochloromethane 0.141 0.132 0.152 0.150 0.152 0.149 0.146 5.46
29) Tetrahydrofuran 0.108 0.077 0.079 0.078 0.086 0.077 0.084 14.50
30) C Chloroform 0.521 0.444 0.555 0.540 0.540 0.527 0.521 7.60
31) S Dibromofluoromethan 0.285 0.294 0.294 0.290 0.294 0.289 0.291 1.21
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Initial Calibr ation Summar y Page 2 of 3
Job Number:FA1942 Sample:VZ591-ICC591
Account:AMECPAP AMEC Environment & Infrastructure, Inc.Lab FileID:Z13892.D
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
32) 1,1,1-Trichloroetha 0.404 0.357 0.472 0.447 0.457 0.447 0.431 9.84
33) Cyclohexane 0.473 0.447 0.600 0.579 0.597 0.572 0.545 12.27
34) Carbon Tetrachlorid 0.349 0.311 0.424 0.408 0.410 0.399 0.383 11.43
35) 1,1-Dichloropropene 0.311 0.289 0.390 0.376 0.381 0.369 0.353 11.87
36) S 1,2-Dichloroethane- 0.355 0.366 0.366 0.357 0.374 0.362 0.363 1.97
37) TAME 0.716 0.668 0.792 0.788 0.798 0.765 0.755 6.86
38) Benzene 0.953 0.879 1.120 1.085 1.086 1.068 1.032 9.13
39) 1,2-Dichloroethane 0.493 0.425 0.504 0.503 0.505 0.492 0.487 6.32
40) Trichloroethene 0.286 0.230 0.295 0.288 0.291 0.285 0.279 8.75
41) Methylcyclohexane 0.418 0.335 0.455 0.442 0.451 0.426 0.421 10.55
42) C 1,2-Dichloropropane 0.333 0.313 0.373 0.368 0.369 0.363 0.353 6.93
43) Dibromomethane 0.207 0.171 0.197 0.194 0.199 0.190 0.193 6.35
44) Bromodichloromethan 0.395 0.345 0.407 0.403 0.410 0.404 0.394 6.19
45) 2-Chloroethyl vinyl 0.222 0.204 0.243 0.242 0.248 0.236 0.233 7.09
46) 2-Nitropropane 0.072 0.068 0.082 0.083 0.088 0.081 0.079 9.71
47) cis-1,3-Dichloropro 0.446 0.427 0.517 0.515 0.520 0.505 0.488 8.39
48) 4-Methyl-2-pentanon 0.265 0.255 0.297 0.301 0.318 0.293 0.288 8.15
49) I Chlorobenzene-d5 ----------------ISTD---------------------
50) S Toluene-d8 1.258 1.261 1.271 1.285 1.298 1.289 1.277 1.26
51) C Toluene 1.334 1.175 1.529 1.513 1.509 1.491 1.425 9.96
52) trans-1,3-Dichlorop 0.501 0.498 0.572 0.581 0.591 0.577 0.553 7.61
53) 1,1,2-Trichloroetha 0.308 0.254 0.301 0.301 0.307 0.295 0.294 6.89
54) Tetrachloroethene 0.308 0.296 0.400 0.394 0.396 0.388 0.364 13.23
55) 2-hexanone 0.236 0.224 0.270 0.282 0.298 0.277 0.264 10.80
56) 1,3-Dichloropropane 0.550 0.507 0.599 0.605 0.616 0.596 0.579 7.22
57) Dibromochloromethan 0.366 0.341 0.419 0.426 0.436 0.429 0.403 9.82
58) 1,2-Dibromoethane 0.353 0.319 0.371 0.374 0.389 0.379 0.364 6.89
59) 1-Chlorohexane 0.386 0.370 0.497 0.491 0.491 0.481 0.453 12.84
60) P Chlorobenzene 0.868 0.821 1.006 0.986 0.976 0.956 0.935 7.91
61) C Ethylbenzene 1.534 1.354 1.726 1.702 1.685 1.644 1.608 8.80
62) 1,1,1,2-Tetrachloro 0.350 0.322 0.396 0.399 0.397 0.391 0.376 8.57
63) m,p-Xylene 1.168 1.038 1.332 1.302 1.298 1.263 1.233 9.01
64) o-Xylene 1.153 1.085 1.354 1.335 1.330 1.302 1.260 8.92
65) Styrene 0.944 0.900 1.128 1.132 1.132 1.123 1.060 10.17
66) P Bromoform 0.231 0.224 0.271 0.281 0.296 0.286 0.265 11.35
67) I 1,4-Dichlorobenzene-d ----------------ISTD---------------------
68) Isopropylbenzene 2.601 2.469 3.145 3.082 3.097 3.054 2.908 10.08
69) Cyclohexanone 0.045 0.032 0.032 0.029 0.030 0.025 0.032 21.55
---- Quadratic regr., Force(0,0) ---- Coefficient = 0.9962
Response Ratio = 0.00000 + 0.03506 *A + -0.00097 *A^2
70) S 4-Bromofluorobenzen 1.035 1.041 1.025 1.028 1.034 1.042 1.034 0.66
71) P 1,1,2,2-Tetrachloro 0.846 0.754 0.877 0.877 0.901 0.846 0.850 6.10
72) trans-1,4-Dichloro- 0.256 0.274 0.305 0.311 0.332 0.321 0.300 9.70
73) n-Propylbenzene 2.992 2.827 3.666 3.551 3.577 3.543 3.359 10.56
74) Bromobenzene 0.769 0.679 0.825 0.814 0.826 0.823 0.789 7.39
75) 1,2,3-Trichloroprop 0.226 0.205 0.243 0.249 0.259 0.244 0.238 8.05
76) 1,3,5-Trimethylbenz 2.455 2.304 2.950 2.836 2.789 2.697 2.672 9.18
77) 2-Chlorotoluene 2.133 2.062 2.554 2.500 2.460 2.404 2.352 8.70
78) 4-Chlorotoluene 2.046 1.818 2.314 2.296 2.296 2.318 2.181 9.46
79) tert-Butylbenzene 1.228 1.178 1.506 1.468 1.465 1.425 1.378 10.10
80) 1,2,4-Trimethylbenz 2.441 2.356 2.957 2.885 2.865 2.775 2.713 9.29
81) sec-Butylbenzene 2.694 2.577 3.454 3.367 3.332 3.201 3.104 12.04
82) 4-Isopropyltoluene 2.317 2.145 2.763 2.719 2.669 2.562 2.529 9.75
83) 1,3-Dichlorobenzene 1.300 1.251 1.506 1.515 1.507 1.480 1.426 8.32
84) 1,4-Dichlorobenzene 1.488 1.394 1.662 1.665 1.659 1.611 1.580 7.18
85) Benzyl Chloride 0.266 0.275 0.317 0.318 0.326 0.294 0.299 8.28
86) n-Butylbenzene 0.578 0.559 0.749 0.721 0.713 0.666 0.664 11.92
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Initial Calibr ation Summar y Page 3 of 3
Job Number:FA1942 Sample:VZ591-ICC591
Account:AMECPAP AMEC Environment & Infrastructure, Inc.Lab FileID:Z13892.D
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
87) 1,2-Dichlorobenzene 1.278 1.243 1.475 1.464 1.421 1.325 1.368 7.24
88) 1,2-Dibromo-3-Chlor 0.192 0.132 0.126 0.124 0.115 0.091 0.130 25.88
---- Quadratic regr., Force(0,0) ---- Coefficient = 0.9966
Response Ratio = 0.00000 + 0.15065 *A + -0.02915 *A^2
89) 1,2,4-Trichlorobenz 0.741 0.750 0.873 0.814 0.691 0.550 0.736 15.07
---- Quadratic regr., Force(0,0) ---- Coefficient = 0.9996
Response Ratio = 0.00000 + 0.98522 *A + -0.21626 *A^2
90) Hexachlorobutadiene 0.387 0.363 0.471 0.436 0.381 0.323 0.393 13.41
91) Naphthalene 1.611 1.495 1.703 1.598 1.388 1.095 1.482 14.72
92) 1,2,3-Trichlorobenz 0.622 0.577 0.666 0.612 0.508 0.410 0.566 16.40
---- Quadratic regr., Force(0,0) ---- Coefficient = 0.9998
Response Ratio = 0.00000 + 0.73600 *A + -0.16281 *A^2
93) I Tert Butyl alcohol-d1 ----------------ISTD---------------------
94) Acrolein 0.059 0.247 0.234 0.212 0.220 0.219 0.199 34.91
---- Linear regr., Force(0,0) ---- Coefficient = 0.9994
Response Ratio = 0.00000 + 0.21928 *A
95) Tert-Butyl Alcohol 1.398 1.192 1.279 1.290 1.275 1.275 1.285 5.11
96) Tert amyl alcohol 0.986 0.943 0.978 1.004 0.998 1.005 0.986 2.39
97) 1,4-Dioxane 0.081 0.082 0.100 0.097 0.098 0.097 0.092 9.37
----------------------------------------------------------------------------
(#) = Out of Range
8260.M Mon Feb 25 08:40:23 2013
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Initial Calibr ation Ver ification Page 1 of 3
Job Number:FA1942 Sample:VZ591-ICV591
Account:AMECPAP AMEC Environment & Infrastructure, Inc.Lab FileID:Z13896.D
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Evaluate Continuing Calibration Report
Data File : C:\msdchem\1\DATA\022213\Z13896.D Vial: 8
Acq On : 22 Feb 2013 12:22 pm Operator: KarenW
Sample : ICV591-4 Inst : MSVOA15
Misc : MS23457,VZ591,,,,, Multiplr: 1.00
MS Integration Params: RTEINT.P
Method : C:\msdchem\1\METHODS\8260.M (RTE Integrator)
Title : EPA 624 & SWA 5030B/8260B
Last Update : Fri Feb 22 12:33:35 2013
Response via : Multiple Level Calibration
Min. RRF : 0.000 Min. Rel. Area : 50% Max. R.T. Dev 0.50min
Max. RRF Dev : 20% Max. Rel. Area : 200%
Compound AvgRF CCRF %Dev Area% Dev(min)R.T.
----------------------------------------------------------------------------
1 I Fluorobenzene 1.000 1.000 0.0 94 0.00 7.79
----------------------- Amount Calc. %Drift -------------
2 Dichlorodifluoromethane 40.000 43.833 -9.6 107 0.00 2.62
----------------------- AvgRF CCRF %Dev --------------
3 P Chloromethane 0.440 0.466 -5.9 90 0.00 2.84
----------------------- Amount Calc. %Drift -------------
4 C Vinyl Chloride 40.000 42.020 -5.1 100 0.00 2.98
----------------------- AvgRF CCRF %Dev --------------
5 Bromomethane 0.140 0.138 1.4 86 0.00 3.42
6 Chloroethane 0.153 0.168 -9.8 90 0.00 3.58
----------------------- Amount Calc. %Drift -------------
7 Trichlorofluoromethane 40.000 37.629 5.9 95 0.00 3.79
----------------------- AvgRF CCRF %Dev --------------
8 Ethyl Ether 0.296 0.278 6.1 88 0.00 4.10
9 1,2-Dichlorotrifluoroetha 0.343 0.344 -0.3 88 0.00 4.34
10 Freon 113 0.260 0.260 0.0 88 0.00 4.44
11 C 1,1-Dichloroethene 0.463 0.520 -12.3 99 0.00 4.38
----------------------- Amount Calc. %Drift -------------
12 Acetone 200.000 223.440 -11.7 110 0.00 5.07
----------------------- AvgRF CCRF %Dev --------------
13 Iodomethane 0.458 0.452 1.3 88 0.00 4.57
14 Carbon Disulfide 0.711 0.800 -12.5 103 0.00 4.46
15 Methyl acetate 0.201 0.192 4.5 88 0.00 5.20
----------------------- Amount Calc. %Drift -------------
16 Methylene Chloride 40.000 38.860 2.9 92 0.00 5.05
----------------------- AvgRF CCRF %Dev --------------
17 Methyl Tert Butyl Ether 0.790 0.758 4.1 88 0.00 5.33
18 trans-1,2-Dichloroethene 0.509 0.524 -2.9 92 0.00 5.23
19 Acrylonitrile 0.126 0.121 4.0 86 0.00 5.94
20 Hexane 0.741 0.711 4.0 88 0.00 5.30
21 Di-isopropyl ether 1.127 1.062 5.8 86 0.00 5.72
22 Vinyl acetate 0.436 0.484 -11.0 98 0.00 6.13
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Initial Calibr ation Ver ification Page 2 of 3
Job Number:FA1942 Sample:VZ591-ICV591
Account:AMECPAP AMEC Environment & Infrastructure, Inc.Lab FileID:Z13896.D
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
23 P 1,1-Dichloroethane 0.602 0.624 -3.7 92 0.00 5.91
24 ETBE 1.126 1.107 1.7 90 0.00 6.13
25 2-Butanone 0.127 0.138 -8.7 98 0.00 7.05
26 2,2-Dichloropropane 0.401 0.402 -0.2 91 0.00 6.63
27 cis-1,2-Dichloroethene 0.298 0.307 -3.0 94 0.00 6.49
28 Bromochloromethane 0.146 0.149 -2.1 94 0.00 6.71
29 Tetrahydrofuran 0.084 0.073 13.1 89 0.00 6.94
30 C Chloroform 0.521 0.528 -1.3 92 0.00 6.76
31 S Dibromofluoromethane 0.291 0.290 0.3 94 0.00 6.96
32 1,1,1-Trichloroethane 0.431 0.441 -2.3 93 0.00 7.02
33 Cyclohexane 0.545 0.585 -7.3 95 0.00 6.75
34 Carbon Tetrachloride 0.383 0.399 -4.2 92 0.00 6.95
35 1,1-Dichloropropene 0.353 0.383 -8.5 96 0.00 7.13
36 S 1,2-Dichloroethane-d4 0.363 0.365 -0.6 96 0.00 7.51
37 TAME 0.755 0.770 -2.0 92 0.00 7.46
38 Benzene 1.032 1.095 -6.1 95 0.00 7.39
39 1,2-Dichloroethane 0.487 0.507 -4.1 95 0.00 7.58
40 Trichloroethene 0.279 0.287 -2.9 94 0.00 7.97
41 Methylcyclohexane 0.421 0.417 1.0 89 0.00 7.99
42 C 1,2-Dichloropropane 0.353 0.364 -3.1 93 0.00 8.49
43 Dibromomethane 0.193 0.190 1.6 93 0.00 8.39
44 Bromodichloromethane 0.394 0.408 -3.6 96 0.00 8.53
45 2-Chloroethyl vinyl ether 0.233 0.214 8.2 84 0.00 9.05
46 2-Nitropropane 0.079 0.075 5.1 86 0.00 9.61
47 cis-1,3-Dichloropropene 0.488 0.489 -0.2 90 0.00 9.15
48 4-Methyl-2-pentanone 0.288 0.288 0.0 90 0.00 9.72
49 I Chlorobenzene-d5 1.000 1.000 0.0 96 0.00 10.89
50 S Toluene-d8 1.277 1.278 -0.1 95 0.00 9.35
51 C Toluene 1.425 1.510 -6.0 96 0.00 9.39
52 trans-1,3-Dichloropropene 0.553 0.595 -7.6 98 0.00 9.78
53 1,1,2-Trichloroethane 0.294 0.301 -2.4 96 0.00 9.95
54 Tetrachloroethene 0.364 0.383 -5.2 93 0.00 9.80
55 2-hexanone 0.264 0.266 -0.8 91 0.00 10.54
56 1,3-Dichloropropane 0.579 0.595 -2.8 94 0.00 10.23
57 Dibromochloromethane 0.403 0.428 -6.2 96 0.00 10.14
58 1,2-Dibromoethane 0.364 0.377 -3.6 97 0.00 10.41
59 1-Chlorohexane 0.453 0.473 -4.4 92 0.00 10.84
60 P Chlorobenzene 0.935 1.045 -11.8 101 0.00 10.91
61 C Ethylbenzene 1.608 1.703 -5.9 96 0.00 10.91
62 1,1,1,2-Tetrachloroethane 0.376 0.395 -5.1 95 0.00 10.96
63 m,p-Xylene 1.233 1.349 -9.4 99 0.00 11.05
64 o-Xylene 1.260 1.407 -11.7 101 0.00 11.49
65 Styrene 1.060 1.114 -5.1 94 0.00 11.54
66 P Bromoform 0.265 0.268 -1.1 91 0.00 11.60
67 I 1,4-Dichlorobenzene-d4 1.000 1.000 0.0 95 0.00 13.26
68 Isopropylbenzene 2.908 3.270 -12.4 101 0.00 11.80
----------------------- Amount Calc. %Drift -------------
69 Cyclohexanone 200.000 537.099 -168.5# 215 0.00 12.51
----------------------- AvgRF CCRF %Dev --------------
70 S 4-Bromofluorobenzene 1.034 1.035 -0.1 96 0.00 12.11
71 P 1,1,2,2-Tetrachloroethane 0.850 0.864 -1.6 94 0.00 12.28
72 trans-1,4-Dichloro-2-Bute 0.300 0.290 3.3 89 0.00 12.46
73 n-Propylbenzene 3.359 3.833 -14.1 103 0.00 12.22
74 Bromobenzene 0.789 0.822 -4.2 96 0.00 12.23
75 1,2,3-Trichloropropane 0.238 0.247 -3.8 94 0.00 12.44
76 1,3,5-Trimethylbenzene 2.672 2.756 -3.1 93 0.00 12.40
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Initial Calibr ation Ver ification Page 3 of 3
Job Number:FA1942 Sample:VZ591-ICV591
Account:AMECPAP AMEC Environment & Infrastructure, Inc.Lab FileID:Z13896.D
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
77 2-Chlorotoluene 2.352 2.607 -10.8 99 0.00 12.41
78 4-Chlorotoluene 2.181 2.508 -15.0 104 0.00 12.58
79 tert-Butylbenzene 1.378 1.550 -12.5 100 0.00 12.75
80 1,2,4-Trimethylbenzene 2.713 2.831 -4.3 93 0.00 12.81
81 sec-Butylbenzene 3.104 3.563 -14.8 101 0.00 12.93
82 4-Isopropyltoluene 2.529 2.773 -9.6 97 0.00 13.06
83 1,3-Dichlorobenzene 1.426 1.602 -12.3 101 0.00 13.19
84 1,4-Dichlorobenzene 1.580 1.654 -4.7 95 0.00 13.28
85 Benzyl Chloride 0.299 0.295 1.3 88 0.00 13.51
86 n-Butylbenzene 0.664 0.714 -7.5 94 0.00 13.49
87 1,2-Dichlorobenzene 1.368 1.555 -13.7 101 0.00 13.70
----------------------- Amount Calc. %Drift -------------
88 1,2-Dibromo-3-Chloropropa 40.000 38.318 4.2 95 0.00 14.44
89 1,2,4-Trichlorobenzene 40.000 39.748 0.6 95 0.00 15.03
----------------------- AvgRF CCRF %Dev --------------
90 Hexachlorobutadiene 0.393 0.434 -10.4 95 0.00 14.98
91 Naphthalene 1.482 1.544 -4.2 92 0.00 15.32
----------------------- Amount Calc. %Drift -------------
92 1,2,3-Trichlorobenzene 40.000 38.543 3.6 92 0.00 15.48
----------------------- AvgRF CCRF %Dev --------------
93 I Tert Butyl alcohol-d10 1.000 1.000 0.0 91 0.00 5.29
----------------------- Amount Calc. %Drift -------------
94 Acrolein 200.000 1895.068 -847.5# 887 0.00 4.75
----------------------- AvgRF CCRF %Dev --------------
95 Tert-Butyl Alcohol 1.285 1.239 3.6 87 0.00 5.38
96 Tert amyl alcohol 0.986 1.013 -2.7 91 0.00 7.60
97 1,4-Dioxane 0.092 0.100 -8.7 93 0.00 8.71
--------------------------------------------------------------------------
--------------------------------------------------------------------------
(#) = Out of Range SPCC's out = 0 CCC's out = 0
Z13892.D 8260.M Mon Feb 25 08:40:09 2013
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Continuing Calibration Summary Page 1 of 3
Job Number:FA1942 Sample:VZ592-CC591
Account:AMECPAP AMEC Environment & Infrastructure, Inc.Lab FileID:Z13924.D
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Evaluate Continuing Calibration Report
Data File : C:\msdchem\1\DATA\022513\Z13924.D Vial: 1
Acq On : 25 Feb 2013 9:36 am Operator: KarenW
Sample : CC591-4 Inst : MSVOA15
Misc : MS23495,VZ592,,,,, Multiplr: 1.00
MS Integration Params: RTEINT.P
Method : C:\msdchem\1\METHODS\8260.M (RTE Integrator)
Title : EPA 624 & SWA 5030B/8260B
Last Update : Fri Feb 22 12:33:35 2013
Response via : Multiple Level Calibration
Min. RRF : 0.000 Min. Rel. Area : 50% Max. R.T. Dev 0.50min
Max. RRF Dev : 20% Max. Rel. Area : 200%
Compound AvgRF CCRF %Dev Area% Dev(min)R.T.
----------------------------------------------------------------------------
1 I Fluorobenzene 1.000 1.000 0.0 87 0.00 7.78
----------------------- Amount Calc. %Drift -------------
2 Dichlorodifluoromethane 40.000 36.395 9.0 83 0.00 2.62
----------------------- AvgRF CCRF %Dev --------------
3 P Chloromethane 0.440 0.484 -10.0 86 0.00 2.83
----------------------- Amount Calc. %Drift -------------
4 C Vinyl Chloride 40.000 45.510 -13.8 99 0.00 2.98
----------------------- AvgRF CCRF %Dev --------------
5 Bromomethane 0.140 0.221 -57.9# 126 0.00 3.41
6 Chloroethane 0.153 0.221 -44.4# 109 0.00 3.58
----------------------- Amount Calc. %Drift -------------
7 Trichlorofluoromethane 40.000 43.167 -7.9 99 0.00 3.79
----------------------- AvgRF CCRF %Dev --------------
8 Ethyl Ether 0.296 0.281 5.1 82 0.00 4.10
9 1,2-Dichlorotrifluoroetha 0.343 0.356 -3.8 84 -0.01 4.33
10 Freon 113 0.260 0.278 -6.9 86 0.00 4.44
11 C 1,1-Dichloroethene 0.463 0.469 -1.3 82 0.00 4.38
----------------------- Amount Calc. %Drift -------------
12 Acetone 200.000 179.543 10.2 82 0.00 5.07
----------------------- AvgRF CCRF %Dev --------------
13 Iodomethane 0.458 0.501 -9.4 90 0.00 4.57
14 Carbon Disulfide 0.711 0.699 1.7 82 0.00 4.45
15 Methyl acetate 0.201 0.196 2.5 82 0.00 5.19
----------------------- Amount Calc. %Drift -------------
16 Methylene Chloride 40.000 38.764 3.1 85 0.00 5.04
----------------------- AvgRF CCRF %Dev --------------
17 Methyl Tert Butyl Ether 0.790 0.729 7.7 78 0.00 5.33
18 trans-1,2-Dichloroethene 0.509 0.498 2.2 80 0.00 5.22
19 Acrylonitrile 0.126 0.128 -1.6 83 0.00 5.94
20 Hexane 0.741 0.706 4.7 80 0.00 5.30
21 Di-isopropyl ether 1.127 1.101 2.3 82 0.00 5.72
22 Vinyl acetate 0.436 0.468 -7.3 87 0.00 6.13
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Job Number:FA1942 Sample:VZ592-CC591
Account:AMECPAP AMEC Environment & Infrastructure, Inc.Lab FileID:Z13924.D
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
23 P 1,1-Dichloroethane 0.602 0.602 0.0 81 0.00 5.91
24 ETBE 1.126 1.081 4.0 81 0.00 6.12
25 2-Butanone 0.127 0.127 0.0 83 0.00 7.05
26 2,2-Dichloropropane 0.401 0.396 1.2 83 0.00 6.62
27 cis-1,2-Dichloroethene 0.298 0.300 -0.7 84 0.00 6.49
28 Bromochloromethane 0.146 0.151 -3.4 88 0.00 6.71
29 Tetrahydrofuran 0.084 0.072 14.3 80 0.00 6.94
30 C Chloroform 0.521 0.520 0.2 83 0.00 6.76
31 S Dibromofluoromethane 0.291 0.292 -0.3 87 0.00 6.95
32 1,1,1-Trichloroethane 0.431 0.419 2.8 81 0.00 7.02
33 Cyclohexane 0.545 0.551 -1.1 82 0.00 6.75
34 Carbon Tetrachloride 0.383 0.385 -0.5 82 0.00 6.95
35 1,1-Dichloropropene 0.353 0.356 -0.8 82 0.00 7.13
36 S 1,2-Dichloroethane-d4 0.363 0.351 3.3 85 0.00 7.51
37 TAME 0.755 0.697 7.7 77 0.00 7.46
38 Benzene 1.032 1.042 -1.0 83 0.00 7.38
39 1,2-Dichloroethane 0.487 0.474 2.7 82 0.00 7.58
40 Trichloroethene 0.279 0.285 -2.2 86 0.00 7.96
41 Methylcyclohexane 0.421 0.423 -0.5 83 0.00 7.98
42 C 1,2-Dichloropropane 0.353 0.347 1.7 82 0.00 8.49
43 Dibromomethane 0.193 0.192 0.5 86 0.00 8.39
44 Bromodichloromethane 0.394 0.382 3.0 82 0.00 8.53
45 2-Chloroethyl vinyl ether 0.233 0.233 0.0 83 0.00 9.05
46 2-Nitropropane 0.079 0.079 0.0 83 0.00 9.61
47 cis-1,3-Dichloropropene 0.488 0.482 1.2 81 0.00 9.15
48 4-Methyl-2-pentanone 0.288 0.289 -0.3 83 0.00 9.72
49 I Chlorobenzene-d5 1.000 1.000 0.0 92 0.00 10.89
50 S Toluene-d8 1.277 1.212 5.1 87 0.00 9.34
51 C Toluene 1.425 1.376 3.4 84 0.00 9.39
52 trans-1,3-Dichloropropene 0.553 0.533 3.6 84 0.00 9.78
53 1,1,2-Trichloroethane 0.294 0.283 3.7 86 0.00 9.95
54 Tetrachloroethene 0.364 0.378 -3.8 88 0.00 9.80
55 2-hexanone 0.264 0.252 4.5 82 0.00 10.54
56 1,3-Dichloropropane 0.579 0.544 6.0 83 0.00 10.23
57 Dibromochloromethane 0.403 0.385 4.5 83 0.00 10.14
58 1,2-Dibromoethane 0.364 0.347 4.7 86 0.00 10.41
59 1-Chlorohexane 0.453 0.462 -2.0 87 0.00 10.85
60 P Chlorobenzene 0.935 0.949 -1.5 89 0.00 10.91
61 C Ethylbenzene 1.608 1.601 0.4 86 0.00 10.91
62 1,1,1,2-Tetrachloroethane 0.376 0.377 -0.3 87 0.00 10.96
63 m,p-Xylene 1.233 1.212 1.7 86 0.00 11.05
64 o-Xylene 1.260 1.207 4.2 83 0.00 11.49
65 Styrene 1.060 1.025 3.3 83 0.00 11.54
66 P Bromoform 0.265 0.275 -3.8 90 0.00 11.60
67 I 1,4-Dichlorobenzene-d4 1.000 1.000 0.0 95 0.00 13.26
68 Isopropylbenzene 2.908 2.751 5.4 85 0.00 11.80
----------------------- Amount Calc. %Drift -------------
69 Cyclohexanone 200.000 176.332 11.8 90 0.00 12.51
----------------------- AvgRF CCRF %Dev --------------
70 S 4-Bromofluorobenzene 1.034 0.935 9.6 86 0.00 12.11
71 P 1,1,2,2-Tetrachloroethane 0.850 0.800 5.9 86 0.00 12.28
72 trans-1,4-Dichloro-2-Bute 0.300 0.286 4.7 87 0.00 12.46
73 n-Propylbenzene 3.359 3.309 1.5 88 0.00 12.22
74 Bromobenzene 0.789 0.796 -0.9 93 0.00 12.23
75 1,2,3-Trichloropropane 0.238 0.219 8.0 83 0.00 12.44
76 1,3,5-Trimethylbenzene 2.672 2.547 4.7 85 0.00 12.40
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Continuing Calibration Summary Page 3 of 3
Job Number:FA1942 Sample:VZ592-CC591
Account:AMECPAP AMEC Environment & Infrastructure, Inc.Lab FileID:Z13924.D
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
77 2-Chlorotoluene 2.352 2.278 3.1 86 0.00 12.41
78 4-Chlorotoluene 2.181 2.062 5.5 85 0.00 12.57
79 tert-Butylbenzene 1.378 1.311 4.9 85 0.00 12.74
80 1,2,4-Trimethylbenzene 2.713 2.610 3.8 86 0.00 12.81
81 sec-Butylbenzene 3.104 3.098 0.2 87 0.00 12.93
82 4-Isopropyltoluene 2.529 2.506 0.9 87 0.00 13.06
83 1,3-Dichlorobenzene 1.426 1.439 -0.9 90 0.00 13.19
84 1,4-Dichlorobenzene 1.580 1.590 -0.6 90 0.00 13.28
85 Benzyl Chloride 0.299 0.309 -3.3 92 0.00 13.51
86 n-Butylbenzene 0.664 0.691 -4.1 91 0.00 13.49
87 1,2-Dichlorobenzene 1.368 1.401 -2.4 91 0.00 13.70
----------------------- Amount Calc. %Drift -------------
88 1,2-Dibromo-3-Chloropropa 40.000 31.156 22.1# 79 0.00 14.44
89 1,2,4-Trichlorobenzene 40.000 38.795 3.0 92 0.00 15.03
----------------------- AvgRF CCRF %Dev --------------
90 Hexachlorobutadiene 0.393 0.420 -6.9 91 0.00 14.98
91 Naphthalene 1.482 1.469 0.9 87 0.00 15.31
----------------------- Amount Calc. %Drift -------------
92 1,2,3-Trichlorobenzene 40.000 39.759 0.6 93 0.00 15.48
----------------------- AvgRF CCRF %Dev --------------
93 I Tert Butyl alcohol-d10 1.000 1.000 0.0 75 0.00 5.29
----------------------- Amount Calc. %Drift -------------
94 Acrolein 200.000 247.359 -23.7# 96 -0.01 4.75
----------------------- AvgRF CCRF %Dev --------------
95 Tert-Butyl Alcohol 1.285 1.284 0.1 75 0.00 5.37
96 Tert amyl alcohol 0.986 0.975 1.1 73 0.00 7.60
97 1,4-Dioxane 0.092 0.113 -22.8# 88 0.00 8.71
--------------------------------------------------------------------------
--------------------------------------------------------------------------
(#) = Out of Range SPCC's out = 0 CCC's out = 0
Z13892.D 8260.M Mon Feb 25 12:56:03 2013
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08/27/13
Technical Report for
AMEC Environment & Infrastructure, Inc.
GE-TFS; 1906 Bancroft St, Charlotte, NC
781090010.
Accutest Job Number: FA5208
Sampling Date: 06/03/13
Report to:
AMEC Earth & Environmental
[e-mail]
ATTN: Steve Tanen
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), AK, AR, GA, KY, MA, NV, OK, UT, VA, WA, WI
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Conference
and/or state specific certification programs as applicable.
Client Service contact: Heather Wandrey 407-425-6700
Harry Behzadi, Ph.D.
Laboratory Director
Southeast
08/27/13
e-Hardcopy 2.0
Automated Report
116
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
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FA5208
Table of Contents
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Sections:
Section 1: Sample Summary ................................................................................................... 4
Section 2: Case Narrative/Conformance Summary .............................................................. 6
Section 3: Summary of Hits ....................................................................................................8
Section 4: Sample Results ........................................................................................................ 11
4.1:FA5208-1: RR-1/0.75 ................................................................................................... 12
4.2:FA5208-2: RR-2/0.5 ..................................................................................................... 14
4.3:FA5208-3: RR-3/1.0 ..................................................................................................... 16
4.4:FA5208-4: RR-3/4.0 ..................................................................................................... 17
4.5:FA5208-5: RR-3/7.5 ..................................................................................................... 18
4.6:FA5208-6: RR-4/1.0 ..................................................................................................... 19
4.7:FA5208-7: RR-4/4.5 ..................................................................................................... 20
4.8:FA5208-8: RR-4/7.0 ..................................................................................................... 21
4.9:FA5208-9: RR-5/1.0 ..................................................................................................... 22
4.10:FA5208-10: RR-5/5.0 ................................................................................................. 23
4.11:FA5208-11: RR-5/9.5 ................................................................................................. 24
4.12:FA5208-12: RR-6/0.5 ................................................................................................. 25
4.13:FA5208-13: RR-6/5.5 ................................................................................................. 26
4.14:FA5208-14: RR-6/11.5 ............................................................................................... 27
4.15:FA5208-15: RR-7/1.0 ................................................................................................. 28
4.16:FA5208-16: RR-7/6.5 ................................................................................................. 29
4.17:FA5208-17: RR-7/13 .................................................................................................. 30
4.18:FA5208-18: RR-8/1.0 ................................................................................................. 31
4.19:FA5208-19: RR-8/5.0 ................................................................................................. 32
4.20:FA5208-20: RR-8/10.0 ............................................................................................... 33
4.21:FA5208-21: TRIP BLANK ........................................................................................ 34
Section 5: Misc. Forms ............................................................................................................ 36
5.1:Chain of Custody ........................................................................................................... 37
Section 6: GC/MS Volatiles - QC Data Summaries .............................................................. 40
6.1:Method Blank Summary ................................................................................................ 41
6.2:Blank Spike Summary ................................................................................................... 43
6.3:Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 45
6.4:Instrument Performance Checks (BFB) ......................................................................... 47
6.5:Internal Standard Area Summaries ................................................................................ 50
6.6:Surrogate Recovery Summaries ..................................................................................... 51
6.7:Initial and Continuing Calibration Summaries .............................................................. 52
Section 7: Metals Analysis - QC Data Summaries ................................................................ 61
7.1:Inst QC MA10817: As,Se .............................................................................................. 62
7.2:Inst QC MA10821: As,Se .............................................................................................. 76
7.3:Prep QC MP25296: As,Se ............................................................................................. 98
7.4:Prep QC MP25297: As,Se ............................................................................................. 104
7.5:IDL and Linear Range Summaries ................................................................................ 110
Section 8: General Chemistry - QC Data Summaries .......................................................... 112
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Table of Contents
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Sections:
8.1:Percent Solids Raw Data Summary ............................................................................... 113
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Accutest LabLink@144523 15:21 27-Aug-2013
Sample Summary
AMEC Environment & Infrastructure, Inc.
Job No:FA5208
GE-TFS; 1906 Bancroft St, Charlotte, NC
Project No: 781090010.
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA5208-1 06/03/13 10:20 DS 06/04/13 SO Soil RR-1/0.75
FA5208-2 06/03/13 10:35 DS 06/04/13 SO Soil RR-2/0.5
FA5208-3 06/03/13 11:10 DS 06/04/13 SO Soil RR-3/1.0
FA5208-4 06/03/13 11:15 DS 06/04/13 SO Soil RR-3/4.0
FA5208-5 06/03/13 11:25 DS 06/04/13 SO Soil RR-3/7.5
FA5208-6 06/03/13 11:45 DS 06/04/13 SO Soil RR-4/1.0
FA5208-7 06/03/13 11:50 DS 06/04/13 SO Soil RR-4/4.5
FA5208-8 06/03/13 11:55 DS 06/04/13 SO Soil RR-4/7.0
FA5208-9 06/03/13 12:20 DS 06/04/13 SO Soil RR-5/1.0
FA5208-10 06/03/13 12:25 DS 06/04/13 SO Soil RR-5/5.0
FA5208-11 06/03/13 12:30 DS 06/04/13 SO Soil RR-5/9.5
FA5208-12 06/03/13 12:55 DS 06/04/13 SO Soil RR-6/0.5
FA5208-13 06/03/13 13:05 DS 06/04/13 SO Soil RR-6/5.5
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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Accutest LabLink@144523 15:21 27-Aug-2013
Sample Summary
(continued)
AMEC Environment & Infrastructure, Inc.
Job No:FA5208
GE-TFS; 1906 Bancroft St, Charlotte, NC
Project No: 781090010.
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA5208-14 06/03/13 13:10 DS 06/04/13 SO Soil RR-6/11.5
FA5208-15 06/03/13 13:25 DS 06/04/13 SO Soil RR-7/1.0
FA5208-16 06/03/13 13:30 DS 06/04/13 SO Soil RR-7/6.5
FA5208-17 06/03/13 13:35 DS 06/04/13 SO Soil RR-7/13
FA5208-18 06/03/13 13:55 DS 06/04/13 SO Soil RR-8/1.0
FA5208-19 06/03/13 14:00 DS 06/04/13 SO Soil RR-8/5.0
FA5208-20 06/03/13 14:05 DS 06/04/13 SO Soil RR-8/10.0
FA5208-21 06/03/13 00:00 DS 06/04/13 SO Trip Blank Soil TRIP BLANK
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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SAMPLE DELIVERY GROUP C ASE NARR ATIVE
Client:AMEC Environment & Infrastructure, Inc.Job:FA5208
Site:GE-TFS; 1906 Bancroft St, Charlotte, NC Report Date:6/17/2013 9:16:14 AM
20 Samples and 1 Trip Blank were collected on 06/03/2013 and were received at Accutest SE on 06/04/2013 properly preserved, at 2.6
Deg. C and intact. These Samples received an Accutest job number of FA5208. A listing of the Laboratory Sample ID, Client Sample
ID and dates of collection are presented in the Results Summary Section of this report.
Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For more
information, please refer to QC summary pages.
Volatiles by GCMS By Method SW846 8260B
Matrix:SO Batch ID:VY409
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) FA5170-4MS, FA5170-4MSD were used as the QC samples indicated.
Metals By Method SW846 6010C
Matrix:SO Batch ID:MP25296
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) FA5145-25RDUP, FA5145-25RMS, FA5145-25RMSD, FA5145-25RPS, FA5145-25RSDL were used as the QC
samples for metals.
RPD(s) for Duplicate for Arsenic are outside control limits for sample MP25296-D1. RPD acceptable due to low duplicate
and sample concentrations.
RPD(s) for Serial Dilution for Arsenic, Selenium are outside control limits for sample MP25296-SD1. Percent difference
acceptable due to low initial sample concentration (< 50 times IDL).
FA5208-12 for Arsenic: Elevated reporting limit(s) due to matrix interference.
FA5208-12 for Selenium: Elevated reporting limit(s) due to matrix interference.
FA5208-14 for Arsenic: Elevated reporting limit(s) due to matrix interference.
FA5208-14 for Selenium: Elevated reporting limit(s) due to matrix interference.
Matrix:SO Batch ID:MP25297
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) FA5208-15DUP, FA5208-15MSD, FA5208-15PS, FA5208-15SDL were used as the QC samples for metals.
Matrix Spike Recovery(s)/Matrix Spike Duplicate Recovery(s) for Arsenic, Selenium are outside control limits. Spike recovery
indicates possible matrix interference and/or sample non-homogeneity.
RPD(s) for Duplicate for Arsenic are outside control limits for sample MP25297-D1. RPD acceptable due to low duplicate
and sample concentrations.
RPD(s) for Serial Dilution for Arsenic are outside control limits for sample MP25297-SD1. Percent difference acceptable due
to low initial sample concentration (< 50 times IDL).
FA5208-16 for Arsenic: Elevated reporting limit(s) due to matrix interference.
FA5208-16 for Selenium: Elevated reporting limit(s) due to matrix interference.
FA5208-17 for Arsenic: Elevated reporting limit(s) due to matrix interference.
FA5208-17 for Selenium: Elevated reporting limit(s) due to matrix interference.
FA5208-19 for Selenium: Elevated reporting limit(s) due to matrix interference.
FA5208-20 for Arsenic: Elevated reporting limit(s) due to matrix interference.
FA5208-20 for Selenium: Elevated reporting limit(s) due to matrix interference.
Monday, J une 17, 2013 Page 1 of 2
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Wet Chemistry By Method SM19 2540G
Matrix:SO Batch ID:GN56124
Sample(s) FA5208-10DUP, FA5208-19DUP were used as the QC samples for Solids, Percent.
RPD(s) for Duplicate for Solids, Percent are outside control limits for sample GN56124-D2. Probable cause is due to sample
non-homogeneity.
Matrix:SO Batch ID:GN56125
Sample(s) FA5274-1DUP was used as the QC sample for Solids, Percent.
Accutest Laboratories Southeast (ALSE) certifies that this report meets the project requirements for analytical data produced
for the samples as received at ALSE and as stated on the COC. ALSE certifies that the data meets the Data Quality Objectives
for precision, accuracy and completeness as specified in the ALSE Quality Manual except as noted above. This report is to be
used in its entirety. ALSE is not responsible for any assumptions of data quality if partial data packages are used.
Narrative prepared by:
______________________________________ Date: June 17, 2013
Kim Benham, Client Services (signature on file)
Manual Integr ation Su mmar y
Lab Sample ID Analysis Type File ID Manual
VY404-IC404 MSVOA Y9181.D 1,4-Dioxane
VY404-IC404 MSVOA Y9187.D Ethyl alcohol
VY404-ICC404 MSVOA Y9185.D Ethyl alcohol
VY409-CC404 MSVOA Y9318.D Cyclohexane, Freon 113
4 Manual Integrations were found for FA5208
Monday, J une 17, 2013 Page 2 of 2
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Summar y of Hits Page 1 of 3
Job Number:FA5208
Account:AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Collected:06/03/13
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA5208-1 RR-1/0.75
Toluene 2.5 J 4.9 0.98 ug/kg SW846 8260B
FA5208-2 RR-2/0.5
Acetone 36.4 J 58 23 ug/kg SW846 8260B
Ethylbenzene 10.6 5.8 1.3 ug/kg SW846 8260B
Methyl ethyl ketone 8.3 J 29 5.8 ug/kg SW846 8260B
Toluene 11.1 5.8 1.2 ug/kg SW846 8260B
Xylene (total) 57.4 17 3.5 ug/kg SW846 8260B
FA5208-3 RR-3/1.0
Arsenic 0.72 0.51 0.082 mg/kg SW846 6010C
FA5208-4 RR-3/4.0
Arsenic 0.88 0.51 0.082 mg/kg SW846 6010C
FA5208-5 RR-3/7.5
Arsenic 1.6 0.45 0.073 mg/kg SW846 6010C
FA5208-6 RR-4/1.0
Arsenic 1.8 0.58 0.093 mg/kg SW846 6010C
FA5208-7 RR-4/4.5
Arsenic 1.2 0.51 0.082 mg/kg SW846 6010C
FA5208-8 RR-4/7.0
Arsenic 0.27 J 0.49 0.078 mg/kg SW846 6010C
FA5208-9 RR-5/1.0
Arsenic 1.9 0.52 0.083 mg/kg SW846 6010C
FA5208-10 RR-5/5.0
Arsenic 2.3 0.57 0.091 mg/kg SW846 6010C
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Job Number:FA5208
Account:AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Collected:06/03/13
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA5208-11 RR-5/9.5
Arsenic 0.69 0.51 0.082 mg/kg SW846 6010C
FA5208-12 RR-6/0.5
Arsenic a 2.3 0.93 0.15 mg/kg SW846 6010C
FA5208-13 RR-6/5.5
Arsenic 0.24 J 0.48 0.077 mg/kg SW846 6010C
Selenium 0.27 J 0.96 0.14 mg/kg SW846 6010C
FA5208-14 RR-6/11.5
Arsenic a 1.3 J 2.1 0.34 mg/kg SW846 6010C
FA5208-15 RR-7/1.0
Arsenic 1.6 0.53 0.084 mg/kg SW846 6010C
FA5208-16 RR-7/6.5
Arsenic a 4.0 J 5.6 0.89 mg/kg SW846 6010C
FA5208-17 RR-7/13
Arsenic a 1.7 J 2.4 0.39 mg/kg SW846 6010C
FA5208-18 RR-8/1.0
Arsenic 1.1 0.70 0.11 mg/kg SW846 6010C
FA5208-19 RR-8/5.0
Arsenic 0.98 0.59 0.094 mg/kg SW846 6010C
FA5208-20 RR-8/10.0
Arsenic a 1.6 J 2.8 0.44 mg/kg SW846 6010C
FA5208-21 TRIP BLANK
No hits reported in this sample.
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Summar y of Hits Page 3 of 3
Job Number:FA5208
Account:AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Collected:06/03/13
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
(a) Elevated reporting limit(s) due to matrix interference.
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Sample Results
Report of Analysis
Southeast
Section 4
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Client Sample ID:RR-1/0.75
Lab Sample ID:FA5208-1 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Method:SW846 8260B Percent Solids:93.3
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y9335.D 1 06/05/13 EP n/a n/a VY409
Run #2
Initial Weight
Run #1 5.47 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 20 U 49 20 ug/kg
71-43-2 Benzene 0.98 U 4.9 0.98 ug/kg
75-27-4 Bromodichloromethane 1.4 U 4.9 1.4 ug/kg
75-25-2 Bromoform 0.98 U 4.9 0.98 ug/kg
108-90-7 Chlorobenzene 0.98 U 4.9 0.98 ug/kg
75-00-3 Chloroethane 2.0 U 4.9 2.0 ug/kg
67-66-3 Chloroform 0.98 U 4.9 0.98 ug/kg
75-15-0 Carbon disulfide 2.0 U 4.9 2.0 ug/kg
56-23-5 Carbon tetrachloride 1.1 U 4.9 1.1 ug/kg
75-34-3 1,1-Dichloroethane 0.98 U 4.9 0.98 ug/kg
75-35-4 1,1-Dichloroethylene 1.2 U 4.9 1.2 ug/kg
107-06-2 1,2-Dichloroethane 1.2 U 4.9 1.2 ug/kg
78-87-5 1,2-Dichloropropane 0.98 U 4.9 0.98 ug/kg
124-48-1 Dibromochloromethane 0.98 U 4.9 0.98 ug/kg
156-59-2 cis-1,2-Dichloroethylene 0.98 U 4.9 0.98 ug/kg
10061-01-5 cis-1,3-Dichloropropene 0.98 U 4.9 0.98 ug/kg
156-60-5 trans-1,2-Dichloroethylene 0.98 U 4.9 0.98 ug/kg
10061-02-6 trans-1,3-Dichloropropene 0.98 U 4.9 0.98 ug/kg
100-41-4 Ethylbenzene 1.1 U 4.9 1.1 ug/kg
591-78-6 2-Hexanone 4.9 U 24 4.9 ug/kg
108-10-1 4-Methyl-2-pentanone 4.9 U 24 4.9 ug/kg
74-83-9 Methyl bromide 2.0 U 4.9 2.0 ug/kg
74-87-3 Methyl chloride 2.0 U 4.9 2.0 ug/kg
75-09-2 Methylene chloride 4.5 U 9.8 4.5 ug/kg
78-93-3 Methyl ethyl ketone 4.9 U 24 4.9 ug/kg
100-42-5 Styrene 0.98 U 4.9 0.98 ug/kg
71-55-6 1,1,1-Trichloroethane 0.98 U 4.9 0.98 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane 0.98 U 4.9 0.98 ug/kg
79-00-5 1,1,2-Trichloroethane 0.98 U 4.9 0.98 ug/kg
127-18-4 Tetrachloroethylene 1.1 U 4.9 1.1 ug/kg
108-88-3 Toluene 2.5 4.9 0.98 ug/kg J
79-01-6 Trichloroethylene 0.98 U 4.9 0.98 ug/kg
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Repor t of Analysis Page 2 of 2
Client Sample ID:RR-1/0.75
Lab Sample ID:FA5208-1 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Method:SW846 8260B Percent Solids:93.3
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.98 U 4.9 0.98 ug/kg
1330-20-7 Xylene (total) 3.0 U 15 3.0 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 108% 75-124%
2037-26-5 Toluene-D8 102% 75-126%
460-00-4 4-Bromofluorobenzene 101% 71-133%
17060-07-0 1,2-Dichloroethane-D4 114% 72-135%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:RR-2/0.5
Lab Sample ID:FA5208-2 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Method:SW846 8260B Percent Solids:84.3
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y9336.D 1 06/05/13 EP n/a n/a VY409
Run #2
Initial Weight
Run #1 5.13 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 36.4 58 23 ug/kg J
71-43-2 Benzene 1.2 U 5.8 1.2 ug/kg
75-27-4 Bromodichloromethane 1.6 U 5.8 1.6 ug/kg
75-25-2 Bromoform 1.2 U 5.8 1.2 ug/kg
108-90-7 Chlorobenzene 1.2 U 5.8 1.2 ug/kg
75-00-3 Chloroethane 2.3 U 5.8 2.3 ug/kg
67-66-3 Chloroform 1.2 U 5.8 1.2 ug/kg
75-15-0 Carbon disulfide 2.3 U 5.8 2.3 ug/kg
56-23-5 Carbon tetrachloride 1.3 U 5.8 1.3 ug/kg
75-34-3 1,1-Dichloroethane 1.2 U 5.8 1.2 ug/kg
75-35-4 1,1-Dichloroethylene 1.4 U 5.8 1.4 ug/kg
107-06-2 1,2-Dichloroethane 1.4 U 5.8 1.4 ug/kg
78-87-5 1,2-Dichloropropane 1.2 U 5.8 1.2 ug/kg
124-48-1 Dibromochloromethane 1.2 U 5.8 1.2 ug/kg
156-59-2 cis-1,2-Dichloroethylene 1.2 U 5.8 1.2 ug/kg
10061-01-5 cis-1,3-Dichloropropene 1.2 U 5.8 1.2 ug/kg
156-60-5 trans-1,2-Dichloroethylene 1.2 U 5.8 1.2 ug/kg
10061-02-6 trans-1,3-Dichloropropene 1.2 U 5.8 1.2 ug/kg
100-41-4 Ethylbenzene 10.6 5.8 1.3 ug/kg
591-78-6 2-Hexanone 5.8 U 29 5.8 ug/kg
108-10-1 4-Methyl-2-pentanone 5.8 U 29 5.8 ug/kg
74-83-9 Methyl bromide 2.3 U 5.8 2.3 ug/kg
74-87-3 Methyl chloride 2.4 U 5.8 2.4 ug/kg
75-09-2 Methylene chloride 5.3 U 12 5.3 ug/kg
78-93-3 Methyl ethyl ketone 8.3 29 5.8 ug/kg J
100-42-5 Styrene 1.2 U 5.8 1.2 ug/kg
71-55-6 1,1,1-Trichloroethane 1.2 U 5.8 1.2 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane 1.2 U 5.8 1.2 ug/kg
79-00-5 1,1,2-Trichloroethane 1.2 U 5.8 1.2 ug/kg
127-18-4 Tetrachloroethylene 1.3 U 5.8 1.3 ug/kg
108-88-3 Toluene 11.1 5.8 1.2 ug/kg
79-01-6 Trichloroethylene 1.2 U 5.8 1.2 ug/kg
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Repor t of Analysis Page 2 of 2
Client Sample ID:RR-2/0.5
Lab Sample ID:FA5208-2 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Method:SW846 8260B Percent Solids:84.3
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 1.2 U 5.8 1.2 ug/kg
1330-20-7 Xylene (total) 57.4 17 3.5 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105% 75-124%
2037-26-5 Toluene-D8 101% 75-126%
460-00-4 4-Bromofluorobenzene 109% 71-133%
17060-07-0 1,2-Dichloroethane-D4 110% 72-135%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Repor t of Analysis Page 1 of 1
Client Sample ID:RR-3/1.0
Lab Sample ID:FA5208-3 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Percent Solids:88.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.72 0.51 0.082 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
Selenium 0.15 U 1.0 0.15 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA10817
(2) Prep QC Batch: MP25296
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
16 of 116
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4
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Repor t of Analysis Page 1 of 1
Client Sample ID:RR-3/4.0
Lab Sample ID:FA5208-4 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Percent Solids:83.3
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.88 0.51 0.082 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
Selenium 0.15 U 1.0 0.15 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA10817
(2) Prep QC Batch: MP25296
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
17 of 116
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4
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4
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Repor t of Analysis Page 1 of 1
Client Sample ID:RR-3/7.5
Lab Sample ID:FA5208-5 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Percent Solids:83.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 1.6 0.45 0.073 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
Selenium 0.14 U 0.91 0.14 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA10817
(2) Prep QC Batch: MP25296
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
18 of 116
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4
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Repor t of Analysis Page 1 of 1
Client Sample ID:RR-4/1.0
Lab Sample ID:FA5208-6 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Percent Solids:80.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 1.8 0.58 0.093 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
Selenium 0.17 U 1.2 0.17 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA10817
(2) Prep QC Batch: MP25296
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
19 of 116
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4
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6
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Repor t of Analysis Page 1 of 1
Client Sample ID:RR-4/4.5
Lab Sample ID:FA5208-7 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Percent Solids:82.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 1.2 0.51 0.082 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
Selenium 0.15 U 1.0 0.15 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA10817
(2) Prep QC Batch: MP25296
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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4
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Repor t of Analysis Page 1 of 1
Client Sample ID:RR-4/7.0
Lab Sample ID:FA5208-8 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Percent Solids:87.0
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.27 J 0.49 0.078 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
Selenium 0.15 U 0.97 0.15 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA10817
(2) Prep QC Batch: MP25296
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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4
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8
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Client Sample ID:RR-5/1.0
Lab Sample ID:FA5208-9 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Percent Solids:86.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 1.9 0.52 0.083 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
Selenium 0.16 U 1.0 0.16 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA10817
(2) Prep QC Batch: MP25296
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
22 of 116
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4
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9
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Repor t of Analysis Page 1 of 1
Client Sample ID:RR-5/5.0
Lab Sample ID:FA5208-10 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Percent Solids:83.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 2.3 0.57 0.091 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
Selenium 0.17 U 1.1 0.17 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA10817
(2) Prep QC Batch: MP25296
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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4
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1
0
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Repor t of Analysis Page 1 of 1
Client Sample ID:RR-5/9.5
Lab Sample ID:FA5208-11 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Percent Solids:88.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.69 0.51 0.082 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
Selenium 0.15 U 1.0 0.15 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA10817
(2) Prep QC Batch: MP25296
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
24 of 116
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4
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1
1
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Repor t of Analysis Page 1 of 1
Client Sample ID:RR-6/0.5
Lab Sample ID:FA5208-12 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Percent Solids:90.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic a 2.3 0.93 0.15 mg/kg 2 06/11/13 06/13/13 LM SW846 6010C
1 SW846 3050B 2
Selenium a 0.28 U 1.9 0.28 mg/kg 2 06/11/13 06/13/13 LM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA10821
(2) Prep QC Batch: MP25296
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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4
.
1
2
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Repor t of Analysis Page 1 of 1
Client Sample ID:RR-6/5.5
Lab Sample ID:FA5208-13 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Percent Solids:89.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.24 J 0.48 0.077 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
Selenium 0.27 J 0.96 0.14 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA10817
(2) Prep QC Batch: MP25296
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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4
.
1
3
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Repor t of Analysis Page 1 of 1
Client Sample ID:RR-6/11.5
Lab Sample ID:FA5208-14 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Percent Solids:78.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic a 1.3 J 2.1 0.34 mg/kg 4 06/11/13 06/13/13 LM SW846 6010C
1 SW846 3050B 2
Selenium a 0.63 U 4.2 0.63 mg/kg 4 06/11/13 06/13/13 LM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA10821
(2) Prep QC Batch: MP25296
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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4
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1
4
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Client Sample ID:RR-7/1.0
Lab Sample ID:FA5208-15 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Percent Solids:90.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 1.6 0.53 0.084 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
Selenium 0.16 U 1.1 0.16 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA10817
(2) Prep QC Batch: MP25297
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
28 of 116
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4
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1
5
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Client Sample ID:RR-7/6.5
Lab Sample ID:FA5208-16 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Percent Solids:80.2
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic a 4.0 J 5.6 0.89 mg/kg 10 06/11/13 06/13/13 LM SW846 6010C
1 SW846 3050B 2
Selenium a 1.7 U 11 1.7 mg/kg 10 06/11/13 06/13/13 LM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA10821
(2) Prep QC Batch: MP25297
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
29 of 116
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4
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1
6
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Repor t of Analysis Page 1 of 1
Client Sample ID:RR-7/13
Lab Sample ID:FA5208-17 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Percent Solids:85.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic a 1.7 J 2.4 0.39 mg/kg 5 06/11/13 06/13/13 LM SW846 6010C
1 SW846 3050B 2
Selenium a 0.72 U 4.8 0.72 mg/kg 5 06/11/13 06/13/13 LM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA10821
(2) Prep QC Batch: MP25297
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Client Sample ID:RR-8/1.0
Lab Sample ID:FA5208-18 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Percent Solids:66.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 1.1 0.70 0.11 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
Selenium 0.21 U 1.4 0.21 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA10817
(2) Prep QC Batch: MP25297
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Client Sample ID:RR-8/5.0
Lab Sample ID:FA5208-19 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Percent Solids:73.8
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.98 0.59 0.094 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
Selenium a 1.8 U 4.8 1.8 mg/kg 1 06/11/13 06/12/13 LM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA10817
(2) Prep QC Batch: MP25297
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Repor t of Analysis Page 1 of 1
Client Sample ID:RR-8/10.0
Lab Sample ID:FA5208-20 Date Sampled:06/03/13
Matrix:SO - Soil Date Received:06/04/13
Percent Solids:75.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic a 1.6 J 2.8 0.44 mg/kg 5 06/11/13 06/13/13 LM SW846 6010C
1 SW846 3050B 2
Selenium a 0.83 U 5.6 0.83 mg/kg 5 06/11/13 06/13/13 LM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA10821
(2) Prep QC Batch: MP25297
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Client Sample ID:TRIP BLANK
Lab Sample ID:FA5208-21 Date Sampled:06/03/13
Matrix:SO - Trip Blank Soil Date Received:06/04/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y9337.D 1 06/05/13 EP n/a n/a VY409
Run #2
Initial Weight
Run #1 5.00 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 20 U 50 20 ug/kg
71-43-2 Benzene 1.0 U 5.0 1.0 ug/kg
75-27-4 Bromodichloromethane 1.4 U 5.0 1.4 ug/kg
75-25-2 Bromoform 1.0 U 5.0 1.0 ug/kg
108-90-7 Chlorobenzene 1.0 U 5.0 1.0 ug/kg
75-00-3 Chloroethane 2.0 U 5.0 2.0 ug/kg
67-66-3 Chloroform 1.0 U 5.0 1.0 ug/kg
75-15-0 Carbon disulfide 2.0 U 5.0 2.0 ug/kg
56-23-5 Carbon tetrachloride 1.1 U 5.0 1.1 ug/kg
75-34-3 1,1-Dichloroethane 1.0 U 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene 1.2 U 5.0 1.2 ug/kg
107-06-2 1,2-Dichloroethane 1.2 U 5.0 1.2 ug/kg
78-87-5 1,2-Dichloropropane 1.0 U 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane 1.0 U 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene 1.0 U 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene 1.0 U 5.0 1.0 ug/kg
156-60-5 trans-1,2-Dichloroethylene 1.0 U 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene 1.0 U 5.0 1.0 ug/kg
100-41-4 Ethylbenzene 1.1 U 5.0 1.1 ug/kg
591-78-6 2-Hexanone 5.0 U 25 5.0 ug/kg
108-10-1 4-Methyl-2-pentanone 5.0 U 25 5.0 ug/kg
74-83-9 Methyl bromide 2.0 U 5.0 2.0 ug/kg
74-87-3 Methyl chloride 2.1 U 5.0 2.1 ug/kg
75-09-2 Methylene chloride 4.6 U 10 4.6 ug/kg
78-93-3 Methyl ethyl ketone 5.0 U 25 5.0 ug/kg
100-42-5 Styrene 1.0 U 5.0 1.0 ug/kg
71-55-6 1,1,1-Trichloroethane 1.0 U 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane 1.0 U 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane 1.0 U 5.0 1.0 ug/kg
127-18-4 Tetrachloroethylene 1.2 U 5.0 1.2 ug/kg
108-88-3 Toluene 1.0 U 5.0 1.0 ug/kg
79-01-6 Trichloroethylene 1.0 U 5.0 1.0 ug/kg
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Repor t of Analysis Page 2 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FA5208-21 Date Sampled:06/03/13
Matrix:SO - Trip Blank Soil Date Received:06/04/13
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 1.0 U 5.0 1.0 ug/kg
1330-20-7 Xylene (total) 3.1 U 15 3.1 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105% 75-124%
2037-26-5 Toluene-D8 102% 75-126%
460-00-4 4-Bromofluorobenzene 106% 71-133%
17060-07-0 1,2-Dichloroethane-D4 108% 72-135%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
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GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
• Instrument Performance Checks (BFB)
• Internal Standard Area Summaries
• Surrogate Recovery Summaries
• Initial and Continuing Calibration Summaries
Southeast
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Method Blank Summar y Page 1 of 2
Job Number:FA5208
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VY409-MB Y9320.D 1 06/05/13 EP n/a n/a VY409
The QC reported here applies to the following samples:Method:SW846 8260B
FA5208-1, FA5208-2, FA5208-21
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 50 20 ug/kg
71-43-2 Benzene ND 5.0 1.0 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.4 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.0 ug/kg
75-15-0 Carbon disulfide ND 5.0 2.0 ug/kg
56-23-5 Carbon tetrachloride ND 5.0 1.1 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.2 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.2 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.1 ug/kg
591-78-6 2-Hexanone ND 25 5.0 ug/kg
108-10-1 4-Methyl-2-pentanone ND 25 5.0 ug/kg
74-83-9 Methyl bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl chloride ND 5.0 2.1 ug/kg
75-09-2 Methylene chloride ND 10 4.6 ug/kg
78-93-3 Methyl ethyl ketone ND 25 5.0 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.2 ug/kg
108-88-3 Toluene ND 5.0 1.0 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg
75-01-4 Vinyl chloride ND 5.0 1.0 ug/kg
1330-20-7 Xylene (total) ND 15 3.1 ug/kg
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Method Blank Summar y Page 2 of 2
Job Number:FA5208
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VY409-MB Y9320.D 1 06/05/13 EP n/a n/a VY409
The QC reported here applies to the following samples:Method:SW846 8260B
FA5208-1, FA5208-2, FA5208-21
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101% 75-124%
2037-26-5 Toluene-D8 107% 75-126%
460-00-4 4-Bromofluorobenzene 104% 71-133%
17060-07-0 1,2-Dichloroethane-D4 101% 72-135%
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Blank Spike Summar y Page 1 of 2
Job Number:FA5208
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VY409-BS Y9319.D 1 06/05/13 EP n/a n/a VY409
The QC reported here applies to the following samples:Method:SW846 8260B
FA5208-1, FA5208-2, FA5208-21
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 332 133 61-152
71-43-2 Benzene 50 50.8 102 76-126
75-27-4 Bromodichloromethane 50 50.9 102 74-130
75-25-2 Bromoform 50 53.5 107 76-127
108-90-7 Chlorobenzene 50 53.6 107 81-129
75-00-3 Chloroethane 50 51.2 102 68-133
67-66-3 Chloroform 50 50.1 100 72-123
75-15-0 Carbon disulfide 50 58.4 117 72-122
56-23-5 Carbon tetrachloride 50 55.1 110 78-133
75-34-3 1,1-Dichloroethane 50 51.8 104 73-125
75-35-4 1,1-Dichloroethylene 50 55.4 111 81-136
107-06-2 1,2-Dichloroethane 50 52.7 105 74-128
78-87-5 1,2-Dichloropropane 50 50.3 101 74-125
124-48-1 Dibromochloromethane 50 52.8 106 76-127
156-59-2 cis-1,2-Dichloroethylene 50 50.1 100 74-126
10061-01-5 cis-1,3-Dichloropropene 50 49.1 98 80-123
156-60-5 trans-1,2-Dichloroethylene 50 52.7 105 70-127
10061-02-6 trans-1,3-Dichloropropene 50 50.8 102 75-131
100-41-4 Ethylbenzene 50 50.2 100 77-123
591-78-6 2-Hexanone 250 294 118 72-133
108-10-1 4-Methyl-2-pentanone 250 279 112 76-132
74-83-9 Methyl bromide 50 51.0 102 65-139
74-87-3 Methyl chloride 50 50.5 101 71-144
75-09-2 Methylene chloride 50 49.1 98 74-137
78-93-3 Methyl ethyl ketone 250 309 124 75-137
100-42-5 Styrene 50 50.1 100 78-125
71-55-6 1,1,1-Trichloroethane 50 54.3 109 70-129
79-34-5 1,1,2,2-Tetrachloroethane 50 53.2 106 71-126
79-00-5 1,1,2-Trichloroethane 50 52.5 105 74-124
127-18-4 Tetrachloroethylene 50 49.5 99 79-130
108-88-3 Toluene 50 49.4 99 76-124
79-01-6 Trichloroethylene 50 52.5 105 75-128
75-01-4 Vinyl chloride 50 51.9 104 76-141
1330-20-7 Xylene (total) 150 158 105 80-129
* = Outside of Control Limits.
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Blank Spike Summar y Page 2 of 2
Job Number:FA5208
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VY409-BS Y9319.D 1 06/05/13 EP n/a n/a VY409
The QC reported here applies to the following samples:Method:SW846 8260B
FA5208-1, FA5208-2, FA5208-21
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101% 75-124%
2037-26-5 Toluene-D8 102% 75-126%
460-00-4 4-Bromofluorobenzene 101% 71-133%
17060-07-0 1,2-Dichloroethane-D4 101% 72-135%
* = Outside of Control Limits.
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Matr ix Spike/Matr ix Spike Duplicate Summary Page 1 of 2
Job Number:FA5208
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA5170-4MS Y9338.D 1 06/05/13 EP n/a n/a VY409
FA5170-4MSD Y9339.D 1 06/05/13 EP n/a n/a VY409
FA5170-4 Y9327.D 1 06/05/13 EP n/a n/a VY409
The QC reported here applies to the following samples:Method:SW846 8260B
FA5208-1, FA5208-2, FA5208-21
FA5170-4 Spike MS MS MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg %RPD Rec/RPD
67-64-1 Acetone ND 342 347 101 359 105 3 61-152/27
71-43-2 Benzene 1.5 J 68.4 65.5 94 65.1 93 1 76-126/26
75-27-4 Bromodichloromethane ND 68.4 65.9 96 65.9 96 0 74-130/25
75-25-2 Bromoform ND 68.4 66.9 98 65.5 96 2 76-127/26
108-90-7 Chlorobenzene ND 68.4 69.2 101 68.8 100 1 81-129/29
75-00-3 Chloroethane ND 68.4 72.2 106 68.7 100 5 68-133/29
67-66-3 Chloroform ND 68.4 65.8 96 63.9 93 3 72-123/26
75-15-0 Carbon disulfide ND 68.4 74.4 109 72.0 105 3 72-122/29
56-23-5 Carbon tetrachloride ND 68.4 70.5 103 68.2 99 3 78-133/29
75-34-3 1,1-Dichloroethane ND 68.4 65.6 96 64.8 95 1 73-125/27
75-35-4 1,1-Dichloroethylene ND 68.4 70.2 103 69.7 102 1 81-136/28
107-06-2 1,2-Dichloroethane ND 68.4 68.2 100 66.5 97 3 74-128/23
78-87-5 1,2-Dichloropropane ND 68.4 65.8 96 66.3 97 1 74-125/25
124-48-1 Dibromochloromethane ND 68.4 66.7 98 66.8 97 0 76-127/27
156-59-2 cis-1,2-Dichloroethylene ND 68.4 64.3 94 64.3 94 0 74-126/26
10061-01-5 cis-1,3-Dichloropropene ND 68.4 63.7 93 62.2 91 2 80-123/26
156-60-5 trans-1,2-Dichloroethylene ND 68.4 64.9 95 65.3 95 1 70-127/27
10061-02-6 trans-1,3-Dichloropropene ND 68.4 63.3 93 63.1 92 0 75-131/28
100-41-4 Ethylbenzene ND 68.4 66.3 97 65.3 95 2 77-123/31
591-78-6 2-Hexanone ND 342 339 99 343 100 1 72-133/26
108-10-1 4-Methyl-2-pentanone ND 342 332 97 337 98 1 76-132/26
74-83-9 Methyl bromide ND 68.4 70.7 103 69.1 101 2 65-139/31
74-87-3 Methyl chloride ND 68.4 58.7 86 61.7 90 5 71-144/27
75-09-2 Methylene chloride ND 68.4 65.0 95 64.7 94 0 74-137/28
78-93-3 Methyl ethyl ketone ND 342 337 99 349 102 3 75-137/25
100-42-5 Styrene ND 68.4 65.7 96 64.9 95 1 78-125/30
71-55-6 1,1,1-Trichloroethane ND 68.4 70.9 104 69.9 102 1 70-129/27
79-34-5 1,1,2,2-Tetrachloroethane ND 68.4 64.9 95 64.0 93 1 71-126/30
79-00-5 1,1,2-Trichloroethane ND 68.4 64.2 94 65.9 96 3 74-124/28
127-18-4 Tetrachloroethylene ND 68.4 66.9 98 69.1 101 3 79-130/31
108-88-3 Toluene ND 68.4 64.0 94 64.7 94 1 76-124/30
79-01-6 Trichloroethylene ND 68.4 67.5 99 67.8 99 0 75-128/27
75-01-4 Vinyl chloride ND 68.4 64.2 94 66.8 97 4 76-141/27
1330-20-7 Xylene (total) ND 205 206 100 204 99 1 80-129/30
* = Outside of Control Limits.
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Job Number:FA5208
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA5170-4MS Y9338.D 1 06/05/13 EP n/a n/a VY409
FA5170-4MSD Y9339.D 1 06/05/13 EP n/a n/a VY409
FA5170-4 Y9327.D 1 06/05/13 EP n/a n/a VY409
The QC reported here applies to the following samples:Method:SW846 8260B
FA5208-1, FA5208-2, FA5208-21
CAS No.Surrogate Recoveries MS MSD FA5170-4 Limits
1868-53-7 Dibromofluoromethane 104% 102% 106% 75-124%
2037-26-5 Toluene-D8 105% 104% 103% 75-126%
460-00-4 4-Bromofluorobenzene 104% 103% 103% 71-133%
17060-07-0 1,2-Dichloroethane-D4 99% 96% 116% 72-135%
* = Outside of Control Limits.
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Instrument Per formance Check (BFB)Page 1 of 2
Job Number:FA5208
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample:VY404-BFB Injection Date:05/29/13
Lab File ID:Y9181.D Injection Time:10:15
Instrument ID:GCMSY
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 15.0 - 40.0% of mass 95 75168 22.4 Pass
75 30.0 - 60.0% of mass 95 172736 51.5 Pass
95 Base peak, 100% relative abundance 335232 100.0 Pass
96 5.0 - 9.0% of mass 95 23648 7.05 Pass
173 Less than 2.0% of mass 174 0 0.00 (0.00)
a Pass
174 50.0 - 100.0% of mass 95 221120 66.0 Pass
175 5.0 - 9.0% of mass 174 18448 5.50 (8.34)
a Pass
176 95.0 - 101.0% of mass 174 217664 64.9 (98.4)
a Pass
177 5.0 - 9.0% of mass 176 16472 4.91 (7.57)
b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
VY404-IC404 Y9181.D 05/29/13 10:15 00:00 Initial cal 1
VY404-IC404 Y9182.D 05/29/13 10:41 00:26 Initial cal 2
VY404-IC404 Y9183.D 05/29/13 11:06 00:51 Initial cal 3
VY404-IC404 Y9184.D 05/29/13 11:32 01:17 Initial cal 4
VY404-ICC404 Y9185.D 05/29/13 11:57 01:42 Initial cal 5
VY404-IC404 Y9186.D 05/29/13 12:23 02:08 Initial cal 6
VY404-IC404 Y9187.D 05/29/13 12:48 02:33 Initial cal 7
VY404-ICV404 Y9189.D 05/29/13 13:39 03:24 Initial cal verification 4
VY404-BS Y9190.D 05/29/13 14:05 03:50 Blank Spike
VY404-MB Y9191.D 05/29/13 14:30 04:15 Method Blank
ZZZZZZ Y9192.D 05/29/13 14:56 04:41 (unrelated sample)
ZZZZZZ Y9193.D 05/29/13 15:22 05:07 (unrelated sample)
ZZZZZZ Y9194.D 05/29/13 15:47 05:32 (unrelated sample)
ZZZZZZ Y9195.D 05/29/13 16:13 05:58 (unrelated sample)
ZZZZZZ Y9196.D 05/29/13 16:38 06:23 (unrelated sample)
FA4978-2 Y9197.D 05/29/13 17:04 06:49 (used for QC only; not part of job FA5208)
FA4978-2MS Y9198.D 05/29/13 17:29 07:14 Matrix Spike
FA4978-2MSD Y9199.D 05/29/13 17:55 07:40 Matrix Spike Duplicate
ZZZZZZ Y9200.D 05/29/13 18:20 08:05 (unrelated sample)
ZZZZZZ Y9201.D 05/29/13 18:46 08:31 (unrelated sample)
ZZZZZZ Y9202.D 05/29/13 19:11 08:56 (unrelated sample)
ZZZZZZ Y9203.D 05/29/13 19:37 09:22 (unrelated sample)
ZZZZZZ Y9204.D 05/29/13 20:02 09:47 (unrelated sample)
ZZZZZZ Y9205.D 05/29/13 20:28 10:13 (unrelated sample)
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Instrument Per formance Check (BFB)Page 2 of 2
Job Number:FA5208
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample:VY404-BFB Injection Date:05/29/13
Lab File ID:Y9181.D Injection Time:10:15
Instrument ID:GCMSY
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
ZZZZZZ Y9206.D 05/29/13 20:53 10:38 (unrelated sample)
ZZZZZZ Y9207.D 05/29/13 21:19 11:04 (unrelated sample)
ZZZZZZ Y9209.D 05/29/13 22:10 11:55 (unrelated sample)
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Instrument Per formance Check (BFB)Page 1 of 1
Job Number:FA5208
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample:VY409-BFB Injection Date:06/05/13
Lab File ID:Y9317.D Injection Time:08:09
Instrument ID:GCMSY
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 15.0 - 40.0% of mass 95 57059 20.4 Pass
75 30.0 - 60.0% of mass 95 139650 50.0 Pass
95 Base peak, 100% relative abundance 279168 100.0 Pass
96 5.0 - 9.0% of mass 95 18075 6.47 Pass
173 Less than 2.0% of mass 174 873 0.31 (0.45)
a Pass
174 50.0 - 100.0% of mass 95 195477 70.0 Pass
175 5.0 - 9.0% of mass 174 15212 5.45 (7.78)
a Pass
176 95.0 - 101.0% of mass 174 191146 68.5 (97.8)
a Pass
177 5.0 - 9.0% of mass 176 12638 4.53 (6.61)
b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
VY409-CC404 Y9318.D 06/05/13 08:34 00:25 Continuing cal 4
VY409-BS Y9319.D 06/05/13 09:00 00:51 Blank Spike
VY409-MB Y9320.D 06/05/13 09:25 01:16 Method Blank
ZZZZZZ Y9321.D 06/05/13 09:51 01:42 (unrelated sample)
ZZZZZZ Y9322.D 06/05/13 10:16 02:07 (unrelated sample)
ZZZZZZ Y9324.D 06/05/13 11:08 02:59 (unrelated sample)
ZZZZZZ Y9325.D 06/05/13 11:33 03:24 (unrelated sample)
ZZZZZZ Y9326.D 06/05/13 11:59 03:50 (unrelated sample)
FA5170-4 Y9327.D 06/05/13 12:24 04:15 (used for QC only; not part of job FA5208)
ZZZZZZ Y9328.D 06/05/13 12:50 04:41 (unrelated sample)
ZZZZZZ Y9329.D 06/05/13 13:15 05:06 (unrelated sample)
ZZZZZZ Y9330.D 06/05/13 13:41 05:32 (unrelated sample)
ZZZZZZ Y9331.D 06/05/13 14:06 05:57 (unrelated sample)
ZZZZZZ Y9332.D 06/05/13 14:32 06:23 (unrelated sample)
ZZZZZZ Y9333.D 06/05/13 14:57 06:48 (unrelated sample)
ZZZZZZ Y9334.D 06/05/13 15:23 07:14 (unrelated sample)
FA5208-1 Y9335.D 06/05/13 15:48 07:39 RR-1/0.75
FA5208-2 Y9336.D 06/05/13 16:14 08:05 RR-2/0.5
FA5208-21 Y9337.D 06/05/13 16:40 08:31 TRIP BLANK
FA5170-4MS Y9338.D 06/05/13 17:05 08:56 Matrix Spike
FA5170-4MSD Y9339.D 06/05/13 17:31 09:22 Matrix Spike Duplicate
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Volatile Internal Standar d Ar ea Summar y Page 1 of 1
Job Number:FA5208
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Check Std:VY409-CC404 Injection Date:06/05/13
Lab File ID:Y9318.D Injection Time:08:34
Instrument ID:GCMSY Method:SW846 8260B
IS 1 IS 2 IS 3 IS 4
AREA RT AREA RT AREA RT AREA RT
Initial Cal a 1110495 6.80 828619 9.93 396015 12.30 152028 4.41
Check Std b 1268889 6.81 934092 9.93 448708 12.29 152089 4.40
Upper Limit c 2537778 7.31 1868184 10.43 897416 12.79 304178 4.90
Lower Limit d 634445 6.31 467046 9.43 224354 11.79 76045 3.90
Lab IS 1 IS 2 IS 3 IS 4
Sample ID AREA RT AREA RT AREA RT AREA RT
VY409-BS 1315002 6.80 987330 9.93 476233 12.30 181240 4.40
VY409-MB 1260020 6.80 930138 9.93 420476 12.29 152823 4.43
ZZZZZZ 1127146 6.80 844886 9.93 383679 12.30 150658 4.40
ZZZZZZ 1162850 6.80 858986 9.93 395863 12.30 134440 4.43
ZZZZZZ 1024607 6.80 924136 9.94 494117 12.30 249930 4.40
ZZZZZZ 1276598 6.80 970013 9.93 465334 12.29 334249* 4.40
ZZZZZZ 1206476 6.80 899059 9.93 426665 12.29 289060 4.40
FA5170-4 1191069 6.80 901584 9.93 442068 12.30 298417 4.40
ZZZZZZ 1141869 6.80 871636 9.93 416581 12.29 253319 4.40
ZZZZZZ 1191160 6.80 907133 9.93 448029 12.30 132697 4.42
ZZZZZZ 1272415 6.80 951457 9.93 445230 12.30 420895* 4.41
ZZZZZZ 1212146 6.80 943958 9.93 438954 12.30 298366 4.40
ZZZZZZ 1196614 6.80 911020 9.93 428659 12.30 189271 4.39
ZZZZZZ 1132502 6.81 868603 9.93 414100 12.29 277976 4.40
ZZZZZZ 1118809 6.80 840268 9.93 401739 12.29 224948 4.40
FA5208-1 1085123 6.80 844800 9.93 404347 12.30 316289* 4.39
FA5208-2 1087088 6.80 816740 9.93 364638 12.30 241724 4.40
FA5208-21 1076731 6.80 799268 9.93 371274 12.29 189290 4.40
FA5170-4MS 1164801 6.80 881137 9.93 424158 12.29 118893 4.40
FA5170-4MSD 1178834 6.80 882247 9.93 428558 12.30 148658 4.40
IS 1 = Fluorobenzene
IS 2 = Chlorobenzene-D5
IS 3 = 1,4-Dichlorobenzene-d4
IS 4 = Tert Butyl Alcohol-D10
(a) Initial Cal is: VY404-ICC404 Y9185.D 05/29/13 11:57
(b) Check Std Limit = -50 to +100% of initial cal area.
(c) Upper Limit = +100% of check standard area; Retention time +0.5 minutes.
(d) Lower Limit = -50% of check standard area; Retention time -0.5 minutes.
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Volatile Sur r ogate Recovery Summary Page 1 of 1
Job Number:FA5208
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Method:SW846 8260B Matr ix:SO
Samples and QC shown here apply to the above method
Lab Lab
Sample ID File ID S1 S2 S3 S4
FA5208-1 Y9335.D 108.0 102.0 101.0 114.0
FA5208-2 Y9336.D 105.0 101.0 109.0 110.0
FA5208-21 Y9337.D 105.0 102.0 106.0 108.0
FA5170-4MS Y9338.D 104.0 105.0 104.0 99.0
FA5170-4MSD Y9339.D 102.0 104.0 103.0 96.0
VY409-BS Y9319.D 101.0 102.0 101.0 101.0
VY409-MB Y9320.D 101.0 107.0 104.0 101.0
Surrogate Recovery
Compounds Limits
S1 = Dibromofluoromethane 75-124%
S2 = Toluene-D8 75-126%
S3 = 4-Bromofluorobenzene 71-133%
S4 = 1,2-Dichloroethane-D4 72-135%
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Initial Calibr ation Summar y Page 1 of 3
Job Number:FA5208 Sample:VY404-ICC404
Account:AMECPAP AMEC Environment & Infrastructure, Inc.Lab FileID:Y9185.D
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Response Factor Report MSVOA14
Method : C:\msdchem\1\METHODS\052913APP9-Y.m (RTE Integrator)
Title : SW-846 Method 5035A/8260B
Last Update : Wed May 29 14:23:39 2013
Response via : Initial Calibration
Calibration Files
1 =Y9181.D 2 =Y9182.D 3 =Y9183.D 4 =Y9184.D
5 =Y9185.D 6 =Y9186.D 7 =Y9187.D
Compound 1 2 3 4 5 6 7 Avg %RSD
---------------------------------------------------------------------------
1) I Fluorobenzene ----------------ISTD---------------------
2) Dichlorodifluorom 0.206 0.202 0.221 0.192 0.236 0.228 0.210 0.214 7.19
3)P Chloromethane 0.321 0.291 0.339 0.287 0.351 0.340 0.314 0.320 7.81
4)C Vinyl Chloride 0.286 0.261 0.280 0.239 0.285 0.276 0.253 0.269 6.75
5) Bromomethane 0.199 0.178 0.191 0.171 0.203 0.197 0.178 0.188 6.54
6) Chloroethane 0.168 0.146 0.168 0.153 0.186 0.185 0.159 0.167 9.14
7) Trichlorofluorome 0.285 0.276 0.331 0.277 0.347 0.345 0.319 0.311 10.10
8) Ethyl Ether 0.269 0.242 0.290 0.246 0.287 0.284 0.259 0.268 7.35
9) 1,2-Dichlorotrifl 0.308 0.255 0.319 0.256 0.299 0.297 0.272 0.287 8.92
10)C 1,1-Dichloroethen 0.380 0.318 0.383 0.322 0.389 0.383 0.353 0.361 8.43
11) Freon 113 0.154 0.162 0.192 0.156 0.186 0.179 0.165 0.171 8.84
12) Carbon Disulfide 0.706 0.589 0.712 0.588 0.687 0.679 0.625 0.655 8.16
13) Iodomethane 0.437 0.363 0.413 0.348 0.412 0.394 0.366 0.390 8.32
14) Allyl chloride 0.494 0.420 0.477 0.393 0.475 0.440 0.423 0.446 8.25
15) Methylene Chlorid 0.540 0.433 0.474 0.375 0.432 0.415 0.375 0.435 13.27
16) Acetone 0.074 0.072 0.076 0.071 0.082 0.071 0.069 0.074 5.67
17) Methyl acetate 0.303 0.253 0.261 0.234 0.279 0.261 0.239 0.261 9.10
18) trans-1,2-Dichlor 0.390 0.348 0.380 0.332 0.405 0.393 0.350 0.371 7.53
19) Hexane 0.199 0.183 0.206 0.175 0.215 0.208 0.186 0.196 7.60
20) Methyl Tert Butyl 0.832 0.770 0.869 0.777 0.927 0.871 0.813 0.837 6.72
21) Acetonitrile 0.030 0.030 0.034 0.030 0.034 0.030 0.028 0.031 6.56
22) Di-isopropyl ethe 1.122 0.998 1.174 0.995 1.194 1.148 1.028 1.094 7.78
23) Chloroprene 0.326 0.326 0.373 0.316 0.391 0.374 0.335 0.349 8.47
24)P 1,1-Dichloroethan 0.534 0.447 0.528 0.447 0.539 0.517 0.461 0.496 8.56
25) Acrylonitrile 0.085 0.082 0.093 0.090 0.103 0.092 0.091 0.091 7.44
26) ETBE 0.946 0.860 0.980 0.878 1.053 1.015 0.931 0.952 7.38
27) Vinyl acetate 0.144 0.303 0.463 0.463 0.495 0.462 0.437 0.395 32.21
---- Quadratic regr., Force(0,0) ---- Coefficient = 0.9989
Response Ratio = 0.00000 + 0.51501 *A + -0.00373 *A^2
28) cis-1,2-Dichloroe 0.280 0.253 0.280 0.238 0.291 0.273 0.248 0.266 7.49
29) 2,2-Dichloropropa 0.296 0.255 0.282 0.239 0.278 0.256 0.223 0.261 9.84
30) Bromochloromethan 0.130 0.121 0.130 0.119 0.143 0.136 0.124 0.129 6.48
31) Cyclohexane 0.293 0.327 0.365 0.320 0.398 0.378 0.340 0.346 10.53
32)C Chloroform 0.511 0.447 0.510 0.429 0.515 0.500 0.451 0.480 7.59
33) Ethyl acetate 0.252 0.240 0.287 0.264 0.302 0.262 0.271 0.268 7.79
34) Tetrahydrofuran 0.102 0.074 0.099 0.084 0.107 0.095 0.093 0.093 12.08
35)S Dibromofluorometh 0.249 0.231 0.248 0.250 0.248 0.236 0.218 0.240 5.03
36) Carbon Tetrachlor 0.288 0.267 0.303 0.258 0.314 0.297 0.266 0.285 7.46
37) 1,1,1-Trichloroet 0.369 0.327 0.377 0.316 0.377 0.361 0.319 0.349 7.98
38) 2-Butanone 0.122 0.116 0.131 0.127 0.150 0.131 0.129 0.129 8.19
39) 1,1-Dichloroprope 0.291 0.286 0.331 0.284 0.347 0.335 0.298 0.310 8.57
40) Propionitrile 0.037 0.032 0.038 0.036 0.043 0.038 0.037 0.037 8.40
41) Methacrylonitrile 0.177 0.159 0.183 0.167 0.204 0.184 0.179 0.179 8.02
42) Benzene 1.077 0.968 1.110 0.926 1.118 1.078 0.971 1.035 7.53
43) TAME 0.866 0.767 0.919 0.799 0.948 0.915 0.851 0.866 7.64
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Initial Calibr ation Summar y Page 2 of 3
Job Number:FA5208 Sample:VY404-ICC404
Account:AMECPAP AMEC Environment & Infrastructure, Inc.Lab FileID:Y9185.D
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
44)S 1,2-Dichloroethan 0.302 0.288 0.309 0.305 0.304 0.291 0.272 0.296 4.40
45) 1,2-Dichloroethan 0.394 0.353 0.398 0.353 0.412 0.395 0.361 0.381 6.45
46) Trichloroethene 0.264 0.238 0.272 0.220 0.274 0.266 0.235 0.253 8.41
47) Methylcyclohexane 0.321 0.341 0.397 0.333 0.421 0.418 0.367 0.371 11.20
48) Dibromomethane 0.165 0.151 0.172 0.152 0.178 0.172 0.158 0.164 6.50
49)C 1,2-Dichloropropa 0.309 0.277 0.318 0.272 0.327 0.309 0.283 0.299 7.28
50) Bromodichlorometh 0.371 0.335 0.388 0.337 0.401 0.394 0.355 0.369 7.35
51) Methyl methacryla 0.263 0.237 0.269 0.251 0.308 0.291 0.267 0.269 8.84
52) 2-Chloroethyl vin 0.157 0.146 0.175 0.167 0.201 0.187 0.179 0.173 10.67
53) cis-1,3-Dichlorop 0.505 0.451 0.522 0.459 0.548 0.521 0.474 0.497 7.30
54) I Chlorobenzene-d5 ----------------ISTD---------------------
55)S Toluene-d8 1.416 1.278 1.343 1.336 1.303 1.265 1.125 1.295 6.98
56)C Toluene 1.629 1.384 1.588 1.305 1.588 1.576 1.378 1.493 8.82
57) 2-Nitropropane 0.097 0.092 0.102 0.096 0.116 0.105 0.098 0.101 7.77
58) 4-Methyl-2-pentan 0.414 0.376 0.423 0.388 0.473 0.422 0.411 0.415 7.47
59) trans-1,3-Dichlor 0.544 0.535 0.617 0.524 0.635 0.631 0.581 8.93
---- Linear regr., Force(0,0) ---- Coefficient = 0.9968
Response Ratio = 0.00000 + 0.62418 *A
60) Tetrachloroethene 0.331 0.325 0.360 0.295 0.386 0.382 0.346 0.347 9.40
61) Ethyl methacrylat 0.297 0.363 0.487 0.459 0.551 0.501 0.491 0.450 19.69
---- Linear regr., Force(0,0) ---- Coefficient = 0.9959
Response Ratio = 0.00000 + 0.50050 *A
62) 1,1,2-Trichloroet 0.277 0.261 0.295 0.254 0.292 0.280 0.250 0.273 6.55
63) Dibromochlorometh 0.343 0.317 0.368 0.326 0.392 0.384 0.348 0.354 7.99
64) 1,3-Dichloropropa 0.601 0.533 0.594 0.522 0.625 0.603 0.543 0.574 7.10
65) 1,2-Dibromoethane 0.309 0.273 0.311 0.281 0.334 0.321 0.290 0.303 7.30
66) 2-hexanone 0.264 0.249 0.289 0.275 0.334 0.297 0.293 0.286 9.58
67) 1-Chlorohexane 0.425 0.410 0.466 0.381 0.479 0.484 0.413 0.437 9.04
68)C Ethylbenzene 1.706 1.542 1.763 1.468 1.797 1.804 1.594 1.668 8.01
69)P Chlorobenzene 0.931 0.834 0.928 0.793 0.963 0.963 0.840 0.893 7.73
70) 1,1,1,2-Tetrachlo 0.359 0.317 0.365 0.306 0.370 0.364 0.323 0.344 7.84
71) m,p-Xylene 1.267 1.134 1.299 1.093 1.365 1.383 1.217 1.251 8.79
72) o-Xylene 1.276 1.082 1.263 1.078 1.336 1.332 1.174 1.220 8.99
73) Styrene 0.926 0.847 1.004 0.900 1.103 1.098 0.975 0.979 9.94
74)P Bromoform 0.202 0.177 0.212 0.204 0.243 0.235 0.215 0.212 10.26
75) Isopropylbenzene 1.411 1.213 1.439 1.220 1.513 1.526 1.331 1.379 9.33
76) I 1,4-Dichlorobenzene-d ----------------ISTD---------------------
77)S 4-Bromofluorobenz 0.779 0.716 0.729 0.775 0.730 0.708 0.629 0.724 6.90
78) cis-1,4-Dichloro- 0.219 0.211 0.264 0.249 0.296 0.276 0.256 0.253 11.99
79) n-Propylbenzene 3.687 3.332 3.785 3.274 3.991 4.027 3.462 3.651 8.34
80) Bromobenzene 0.862 0.757 0.842 0.713 0.857 0.837 0.720 0.799 8.26
81)P 1,1,2,2-Tetrachlo 0.918 0.837 0.918 0.827 0.959 0.891 0.808 0.880 6.40
82) 1,3,5-Trimethylbe 2.842 2.625 3.002 2.560 3.116 3.140 2.706 2.856 8.25
83) 2-Chlorotoluene 2.687 2.419 2.707 2.317 2.791 2.803 2.434 2.594 7.66
84) trans-1,4-Dichlor 0.278 0.259 0.301 0.290 0.345 0.315 0.293 0.297 9.28
85) 1,2,3-Trichloropr 0.268 0.228 0.252 0.229 0.275 0.245 0.229 0.247 7.92
86) Cyclohexanone 0.031 0.030 0.033 0.029 0.034 0.030 0.029 0.031 6.33
---- Quadratic regr., Force(0,0) ---- Coefficient = 0.9970
Response Ratio = 0.00000 + 0.03546 *A + -0.00033 *A^2
87) 4-Chlorotoluene 2.331 2.148 2.428 2.113 2.541 2.499 2.153 2.316 7.74
88) tert-Butylbenzene 1.400 1.351 1.519 1.325 1.610 1.604 1.366 1.454 8.36
89) 1,2,4-Trimethylbe 2.899 2.653 3.004 2.597 3.142 3.137 2.722 2.879 7.86
90) Pentachloroethane 0.404 0.365 0.430 0.363 0.418 0.395 0.323 0.385 9.62
91) sec-Butylbenzene 3.132 2.920 3.348 2.798 3.408 3.408 2.923 3.134 8.23
92) 4-Isopropyltoluen 2.573 2.413 2.691 2.342 2.897 2.870 2.438 2.603 8.55
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Initial Calibr ation Summar y Page 3 of 3
Job Number:FA5208 Sample:VY404-ICC404
Account:AMECPAP AMEC Environment & Infrastructure, Inc.Lab FileID:Y9185.D
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
93) 1,3-Dichlorobenze 1.360 1.258 1.448 1.243 1.479 1.442 1.266 1.356 7.47
94) 1,4-Dichlorobenze 1.650 1.448 1.618 1.348 1.629 1.601 1.389 1.526 8.31
95) n-Butylbenzene 1.552 1.523 1.710 1.462 1.821 1.803 1.548 1.631 8.86
96) Benzyl Chloride 0.361 0.311 0.367 0.334 0.398 0.373 0.342 0.355 8.12
97) 1,2-Dichlorobenze 1.408 1.248 1.383 1.182 1.423 1.377 1.241 1.323 7.31
98) 1,2-Dibromo-3-Chl 0.166 0.140 0.167 0.154 0.181 0.160 0.157 0.161 8.01
99) Hexachlorobutadie 0.355 0.375 0.374 0.315 0.389 0.364 0.328 0.357 7.54
100) 1,2,4-Trichlorobe 0.887 0.807 0.905 0.783 0.952 0.866 0.809 0.858 7.15
101) Naphthalene 2.196 1.981 2.243 2.132 2.502 2.198 2.203 2.208 7.04
102) 1,2,3-Trichlorobe 0.814 0.704 0.821 0.693 0.800 0.722 0.703 0.751 7.66
103) I Tert Butyl Alcohol-d1 ----------------ISTD---------------------
104) Ethanol 0.125 0.102 0.098 0.094 0.101 0.089 0.088 0.100 12.63
105) Acrolein 1.740 1.915 2.001 1.892 1.942 1.951 1.749 1.884 5.38
106) Tert butyl alcoho 1.433 1.324 1.276 1.242 1.321 1.328 1.163 1.298 6.47
107) Isobutyl alcohol 0.358 0.320 0.352 0.332 0.357 0.360 0.318 0.342 5.41
108) Tert Amyl Alcohol 1.097 1.093 1.107 1.090 1.182 1.170 1.061 1.114 4.02
109) 1,4-Dioxane 0.093 0.084 0.090 0.092 0.094 0.108 0.091 0.093 7.88
----------------------------------------------------------------------------
(#) = Out of Range
052913APP9-Y.m Thu May 30 08:14:50 2013
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Initial Calibr ation Ver ification Page 1 of 3
Job Number:FA5208 Sample:VY404-ICV404
Account:AMECPAP AMEC Environment & Infrastructure, Inc.Lab FileID:Y9189.D
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Evaluate Continuing Calibration Report
Data File : C:\msdchem\1\DATA\052913\Y9189.D Vial: 9
Acq On : 29 May 2013 1:39 pm Operator: ERICP
Sample : ICV404-4 Inst : MSVOA14
Misc : MS24312,VY404,5.00,,,,, Multiplr: 1.00
MS Integration Params: rteint.p
Method : C:\msdchem\1\METHODS\052913APP9-Y.m (RTE Integrator)
Title : SW-846 Method 5035A/8260B
Last Update : Wed May 29 14:23:39 2013
Response via : Multiple Level Calibration
Min. RRF : 0.000 Min. Rel. Area : 50% Max. R.T. Dev 0.50min
Max. RRF Dev : 20% Max. Rel. Area : 200%
Compound AvgRF CCRF %Dev Area% Dev(min)R.T.
----------------------------------------------------------------------------
1 I Fluorobenzene 1.000 1.000 0.0 96 0.00 6.80
2 Dichlorodifluoromethane 0.214 0.197 7.9 99 0.00 2.04
3 P Chloromethane 0.320 0.358 -11.9 120 0.00 2.25
4 C Vinyl Chloride 0.269 0.295 -9.7 119 0.00 2.36
5 Bromomethane 0.188 0.211 -12.2 118 0.00 2.72
6 Chloroethane 0.167 0.178 -6.6 112 0.00 2.87
7 Trichlorofluoromethane 0.311 0.328 -5.5 114 0.00 2.99
8 Ethyl Ether 0.268 0.285 -6.3 111 0.00 3.31
9 1,2-Dichlorotrifluoroetha 0.287 0.290 -1.0 109 0.00 3.50
10 C 1,1-Dichloroethene 0.361 0.390 -8.0 117 0.00 3.54
11 Freon 113 0.171 0.160 6.4 99 0.00 3.60
12 Carbon Disulfide 0.655 0.763 -16.5 125 0.00 3.58
13 Iodomethane 0.390 0.400 -2.6 111 0.00 3.69
14 Allyl chloride 0.446 0.456 -2.2 112 0.00 4.02
15 Methylene Chloride 0.435 0.453 -4.1 116 0.00 4.13
16 Acetone 0.074 0.081 -9.5 110 0.00 4.17
17 Methyl acetate 0.261 0.242 7.3 100 0.00 4.30
18 trans-1,2-Dichloroethene 0.371 0.398 -7.3 116 0.00 4.30
19 Hexane 0.196 0.202 -3.1 112 0.00 4.38
20 Methyl Tert Butyl Ether 0.837 0.892 -6.6 111 0.00 4.41
21 Acetonitrile 0.031 0.034 -9.7 109 0.00 4.65
22 Di-isopropyl ether 1.094 1.144 -4.6 111 0.00 4.78
23 Chloroprene 0.349 0.348 0.3 106 0.00 4.92
24 P 1,1-Dichloroethane 0.496 0.541 -9.1 117 0.00 4.94
25 Acrylonitrile 0.091 0.105 -15.4 112 0.00 4.97
26 ETBE 0.952 0.991 -4.1 109 0.00 5.17
----------------------- Amount Calc. %Drift -------------
27 Vinyl acetate 250.000 341.000 -36.4# 139 0.00 5.17
----------------------- AvgRF CCRF %Dev --------------
28 cis-1,2-Dichloroethene 0.266 0.280 -5.3 113 0.00 5.49
29 2,2-Dichloropropane 0.261 0.284 -8.8 114 0.00 5.61
30 Bromochloromethane 0.129 0.137 -6.2 111 0.00 5.70
31 Cyclohexane 0.346 0.381 -10.1 114 0.00 5.73
32 C Chloroform 0.480 0.508 -5.8 114 0.00 5.76
33 Ethyl acetate 0.268 0.320 -19.4 117 0.00 5.87
34 Tetrahydrofuran 0.093 0.107 -15.1 122 0.00 5.95
35 S Dibromofluoromethane 0.240 0.250 -4.2 96 0.00 5.96
36 Carbon Tetrachloride 0.285 0.291 -2.1 109 0.00 5.94
37 1,1,1-Trichloroethane 0.349 0.381 -9.2 116 0.00 6.00
38 2-Butanone 0.129 0.144 -11.6 109 0.00 6.07
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Job Number:FA5208 Sample:VY404-ICV404
Account:AMECPAP AMEC Environment & Infrastructure, Inc.Lab FileID:Y9189.D
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
39 1,1-Dichloropropene 0.310 0.353 -13.9 120 0.00 6.13
40 Propionitrile 0.037 0.040 -8.1 107 0.00 6.38
41 Methacrylonitrile 0.179 0.187 -4.5 108 0.00 6.41
42 Benzene 1.035 1.080 -4.3 112 0.00 6.38
43 TAME 0.866 0.914 -5.5 110 0.00 6.48
44 S 1,2-Dichloroethane-d4 0.296 0.290 2.0 92 0.00 6.52
45 1,2-Dichloroethane 0.381 0.413 -8.4 113 0.00 6.59
46 Trichloroethene 0.253 0.269 -6.3 118 0.00 6.98
47 Methylcyclohexane 0.371 0.371 0.0 107 0.00 6.99
48 Dibromomethane 0.164 0.178 -8.5 113 0.00 7.41
49 C 1,2-Dichloropropane 0.299 0.317 -6.0 112 0.00 7.51
50 Bromodichloromethane 0.369 0.397 -7.6 113 0.00 7.56
51 Methyl methacrylate 0.269 0.279 -3.7 107 0.00 7.69
52 2-Chloroethyl vinyl ether 0.173 0.186 -7.5 107 0.00 8.10
53 cis-1,3-Dichloropropene 0.497 0.511 -2.8 107 0.00 8.19
54 I Chlorobenzene-d5 1.000 1.000 0.0 94 0.00 9.93
55 S Toluene-d8 1.295 1.358 -4.9 96 0.00 8.38
56 C Toluene 1.493 1.548 -3.7 112 0.00 8.43
57 2-Nitropropane 0.101 0.114 -12.9 112 0.00 8.65
58 4-Methyl-2-pentanone 0.415 0.445 -7.2 108 0.00 8.78
----------------------- Amount Calc. %Drift -------------
59 trans-1,3-Dichloropropene 50.000 52.257 -4.5 118 0.00 8.83
----------------------- AvgRF CCRF %Dev --------------
60 Tetrachloroethene 0.347 0.358 -3.2 115 0.00 8.83
----------------------- Amount Calc. %Drift -------------
61 Ethyl methacrylate 50.000 51.812 -3.6 107 0.00 8.96
----------------------- AvgRF CCRF %Dev --------------
62 1,1,2-Trichloroethane 0.273 0.297 -8.8 110 0.00 8.99
63 Dibromochloromethane 0.354 0.393 -11.0 114 0.00 9.18
64 1,3-Dichloropropane 0.574 0.632 -10.1 115 0.00 9.27
65 1,2-Dibromoethane 0.303 0.342 -12.9 115 0.00 9.43
66 2-hexanone 0.286 0.317 -10.8 109 0.00 9.61
67 1-Chlorohexane 0.437 0.432 1.1 107 0.00 9.91
68 C Ethylbenzene 1.668 1.737 -4.1 112 0.00 9.96
69 P Chlorobenzene 0.893 1.007 -12.8 120 0.00 9.95
70 1,1,1,2-Tetrachloroethane 0.344 0.373 -8.4 115 0.00 10.00
71 m,p-Xylene 1.251 1.352 -8.1 117 0.00 10.10
72 o-Xylene 1.220 1.387 -13.7 122 0.00 10.54
73 Styrene 0.979 1.049 -7.2 110 0.00 10.59
74 P Bromoform 0.212 0.236 -11.3 109 0.00 10.64
75 Isopropylbenzene 1.379 1.581 -14.6 122 0.00 10.85
76 I 1,4-Dichlorobenzene-d4 1.000 1.000 0.0 97 0.00 12.30
77 S 4-Bromofluorobenzene 0.724 0.757 -4.6 95 0.00 11.15
78 cis-1,4-Dichloro-2-butene 0.253 0.276 -9.1 107 0.00 11.19
79 n-Propylbenzene 3.651 4.061 -11.2 120 0.00 11.27
80 Bromobenzene 0.799 0.845 -5.8 115 0.00 11.27
81 P 1,1,2,2-Tetrachloroethane 0.880 0.951 -8.1 112 0.00 11.33
82 1,3,5-Trimethylbenzene 2.856 2.866 -0.4 109 0.00 11.46
83 2-Chlorotoluene 2.594 2.808 -8.2 118 0.00 11.44
84 trans-1,4-Dichloro-2-Bute 0.297 0.313 -5.4 105 0.00 11.51
85 1,2,3-Trichloropropane 0.247 0.269 -8.9 114 0.00 11.48
----------------------- Amount Calc. %Drift -------------
86 Cyclohexanone 250.000 292.984 -17.2 131 0.00 11.54
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Job Number:FA5208 Sample:VY404-ICV404
Account:AMECPAP AMEC Environment & Infrastructure, Inc.Lab FileID:Y9189.D
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
----------------------- AvgRF CCRF %Dev --------------
87 4-Chlorotoluene 2.316 2.671 -15.3 123 0.00 11.61
88 tert-Butylbenzene 1.454 1.648 -13.3 121 0.00 11.79
89 1,2,4-Trimethylbenzene 2.879 2.951 -2.5 110 0.00 11.86
90 Pentachloroethane 0.385 0.394 -2.3 105 0.00 11.83
91 sec-Butylbenzene 3.134 3.454 -10.2 120 0.00 11.97
92 4-Isopropyltoluene 2.603 2.830 -8.7 117 0.00 12.11
93 1,3-Dichlorobenzene 1.356 1.559 -15.0 122 0.00 12.22
94 1,4-Dichlorobenzene 1.526 1.591 -4.3 115 0.00 12.31
95 n-Butylbenzene 1.631 1.649 -1.1 109 0.00 12.55
96 Benzyl Chloride 0.355 0.361 -1.7 105 0.00 12.56
97 1,2-Dichlorobenzene 1.323 1.466 -10.8 120 0.00 12.75
98 1,2-Dibromo-3-Chloropropa 0.161 0.181 -12.4 114 0.00 13.56
99 Hexachlorobutadiene 0.357 0.381 -6.7 118 0.00 14.16
100 1,2,4-Trichlorobenzene 0.858 0.902 -5.1 112 0.00 14.19
101 Naphthalene 2.208 2.422 -9.7 110 0.00 14.48
102 1,2,3-Trichlorobenzene 0.751 0.755 -0.5 106 0.00 14.64
103 I Tert Butyl Alcohol-d10 1.000 1.000 0.0 111 0.00 4.40
104 Ethanol 0.100 0.090 10.0 107 0.00 3.44
105 Acrolein 1.884 2.088 -10.8 122 0.00 3.88
106 Tert butyl alcohol 1.298 1.323 -1.9 118 0.00 4.48
107 Isobutyl alcohol 0.342 0.328 4.1 109 0.00 6.55
108 Tert Amyl Alcohol 1.114 1.136 -2.0 116 0.00 6.66
109 1,4-Dioxane 0.093 0.099 -6.5 119 0.00 7.75
--------------------------------------------------------------------------
--------------------------------------------------------------------------
(#) = Out of Range SPCC's out = 0 CCC's out = 0
Y9184.D 052913APP9-Y.m Thu May 30 08:14:37 2013
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Continuing Calibration Summary Page 1 of 3
Job Number:FA5208 Sample:VY409-CC404
Account:AMECPAP AMEC Environment & Infrastructure, Inc.Lab FileID:Y9318.D
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Evaluate Continuing Calibration Report
Data File : C:\msdchem\1\DATA\060513\Y9318.D Vial: 1
Acq On : 5 Jun 2013 8:34 am Operator: ERICP
Sample : CC404-4 Inst : MSVOA14
Misc : MS24370,VY409,5.00,,,,, Multiplr: 1.00
MS Integration Params: rteint.p
Method : C:\msdchem\1\METHODS\052913APP9-Y.m (RTE Integrator)
Title : SW-846 Method 5035A/8260B
Last Update : Thu May 30 08:59:28 2013
Response via : Multiple Level Calibration
Min. RRF : 0.000 Min. Rel. Area : 50% Max. R.T. Dev 0.50min
Max. RRF Dev : 20% Max. Rel. Area : 200%
Compound AvgRF CCRF %Dev Area% Dev(min)R.T.
----------------------------------------------------------------------------
1 I Fluorobenzene 1.000 1.000 0.0 101 0.00 6.81
2 Dichlorodifluoromethane 0.214 0.232 -8.4 122 0.00 2.04
3 P Chloromethane 0.320 0.324 -1.3 114 0.00 2.26
4 C Vinyl Chloride 0.269 0.277 -3.0 117 0.00 2.36
5 Bromomethane 0.188 0.198 -5.3 116 0.00 2.72
6 Chloroethane 0.167 0.182 -9.0 120 0.00 2.87
7 Trichlorofluoromethane 0.311 0.353 -13.5 129 0.00 3.00
8 Ethyl Ether 0.268 0.270 -0.7 111 0.00 3.31
9 1,2-Dichlorotrifluoroetha 0.287 0.323 -12.5 127 0.00 3.51
10 C 1,1-Dichloroethene 0.361 0.389 -7.8 122 0.00 3.54
11 Freon 113 0.171 0.199 -16.4 128 0.00 3.59
12 Carbon Disulfide 0.655 0.698 -6.6 120 0.00 3.59
13 Iodomethane 0.390 0.406 -4.1 118 0.00 3.70
14 Allyl chloride 0.446 0.473 -6.1 121 0.00 4.03
15 Methylene Chloride 0.435 0.420 3.4 113 0.00 4.14
16 Acetone 0.074 0.069 6.8 99 0.00 4.18
17 Methyl acetate 0.261 0.242 7.3 104 0.00 4.30
18 trans-1,2-Dichloroethene 0.371 0.387 -4.3 118 0.00 4.31
19 Hexane 0.196 0.234 -19.4 135 0.00 4.38
20 Methyl Tert Butyl Ether 0.837 0.846 -1.1 110 0.00 4.41
21 Acetonitrile 0.031 0.031 0.0 105 0.00 4.65
22 Di-isopropyl ether 1.094 1.103 -0.8 112 0.00 4.79
23 Chloroprene 0.349 0.383 -9.7 122 0.00 4.92
24 P 1,1-Dichloroethane 0.496 0.520 -4.8 117 0.00 4.94
25 Acrylonitrile 0.091 0.100 -9.9 112 0.00 4.98
26 ETBE 0.952 0.977 -2.6 112 0.00 5.16
----------------------- Amount Calc. %Drift -------------
27 Vinyl acetate 250.000 268.350 -7.3 116 0.00 5.17
----------------------- AvgRF CCRF %Dev --------------
28 cis-1,2-Dichloroethene 0.266 0.269 -1.1 114 0.00 5.49
29 2,2-Dichloropropane 0.261 0.309 -18.4 130 0.00 5.61
30 Bromochloromethane 0.129 0.135 -4.7 114 0.00 5.70
31 Cyclohexane 0.346 0.410 -18.5 129 0.00 5.73
32 C Chloroform 0.480 0.499 -4.0 117 0.00 5.77
33 Ethyl acetate 0.268 0.279 -4.1 107 0.00 5.86
34 Tetrahydrofuran 0.093 0.097 -4.3 116 0.00 5.95
35 S Dibromofluoromethane 0.240 0.244 -1.7 98 0.00 5.96
36 Carbon Tetrachloride 0.285 0.319 -11.9 124 0.00 5.94
37 1,1,1-Trichloroethane 0.349 0.379 -8.6 121 0.00 6.00
38 2-Butanone 0.129 0.126 2.3 100 0.00 6.08
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Job Number:FA5208 Sample:VY409-CC404
Account:AMECPAP AMEC Environment & Infrastructure, Inc.Lab FileID:Y9318.D
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
39 1,1-Dichloropropene 0.310 0.352 -13.5 125 0.00 6.13
40 Propionitrile 0.037 0.036 2.7 101 0.00 6.38
41 Methacrylonitrile 0.179 0.179 0.0 109 0.00 6.41
42 Benzene 1.035 1.089 -5.2 119 0.00 6.39
43 TAME 0.866 0.874 -0.9 110 0.00 6.48
44 S 1,2-Dichloroethane-d4 0.296 0.288 2.7 95 0.00 6.52
45 1,2-Dichloroethane 0.381 0.393 -3.1 112 0.00 6.59
46 Trichloroethene 0.253 0.257 -1.6 118 0.00 6.98
47 Methylcyclohexane 0.371 0.443 -19.4 134 0.00 6.99
48 Dibromomethane 0.164 0.165 -0.6 110 0.00 7.41
49 C 1,2-Dichloropropane 0.299 0.306 -2.3 113 0.00 7.51
50 Bromodichloromethane 0.369 0.373 -1.1 112 0.00 7.56
51 Methyl methacrylate 0.269 0.259 3.7 104 0.00 7.69
52 2-Chloroethyl vinyl ether 0.173 0.173 0.0 105 0.00 8.11
53 cis-1,3-Dichloropropene 0.497 0.513 -3.2 113 0.00 8.19
54 I Chlorobenzene-d5 1.000 1.000 0.0 98 0.00 9.93
55 S Toluene-d8 1.295 1.378 -6.4 101 0.00 8.38
56 C Toluene 1.493 1.551 -3.9 117 0.00 8.43
57 2-Nitropropane 0.101 0.103 -2.0 105 0.00 8.64
58 4-Methyl-2-pentanone 0.415 0.414 0.2 105 0.00 8.78
----------------------- Amount Calc. %Drift -------------
59 trans-1,3-Dichloropropene 50.000 46.948 6.1 110 0.00 8.83
----------------------- AvgRF CCRF %Dev --------------
60 Tetrachloroethene 0.347 0.341 1.7 113 0.00 8.83
----------------------- Amount Calc. %Drift -------------
61 Ethyl methacrylate 50.000 49.733 0.5 106 0.00 8.97
----------------------- AvgRF CCRF %Dev --------------
62 1,1,2-Trichloroethane 0.273 0.278 -1.8 107 0.00 9.00
63 Dibromochloromethane 0.354 0.367 -3.7 110 0.00 9.18
64 1,3-Dichloropropane 0.574 0.584 -1.7 110 0.00 9.27
65 1,2-Dibromoethane 0.303 0.313 -3.3 109 0.00 9.43
66 2-hexanone 0.286 0.290 -1.4 104 0.00 9.60
67 1-Chlorohexane 0.437 0.490 -12.1 126 0.00 9.90
68 C Ethylbenzene 1.668 1.764 -5.8 118 0.00 9.96
69 P Chlorobenzene 0.893 0.927 -3.8 115 0.00 9.95
70 1,1,1,2-Tetrachloroethane 0.344 0.340 1.2 109 0.00 10.01
71 m,p-Xylene 1.251 1.327 -6.1 119 0.00 10.10
72 o-Xylene 1.220 1.274 -4.4 116 0.00 10.54
73 Styrene 0.979 1.021 -4.3 111 0.00 10.59
74 P Bromoform 0.212 0.218 -2.8 105 0.00 10.63
75 Isopropylbenzene 1.379 1.488 -7.9 120 0.00 10.85
76 I 1,4-Dichlorobenzene-d4 1.000 1.000 0.0 101 0.00 12.29
77 S 4-Bromofluorobenzene 0.724 0.748 -3.3 98 0.00 11.15
78 cis-1,4-Dichloro-2-butene 0.253 0.243 4.0 99 0.00 11.20
79 n-Propylbenzene 3.651 3.853 -5.5 119 0.00 11.27
80 Bromobenzene 0.799 0.785 1.8 111 0.00 11.27
81 P 1,1,2,2-Tetrachloroethane 0.880 0.898 -2.0 110 0.00 11.33
82 1,3,5-Trimethylbenzene 2.856 2.991 -4.7 118 0.00 11.46
83 2-Chlorotoluene 2.594 2.709 -4.4 118 0.00 11.44
84 trans-1,4-Dichloro-2-Bute 0.297 0.296 0.3 103 0.00 11.51
85 1,2,3-Trichloropropane 0.247 0.241 2.4 106 0.00 11.48
----------------------- Amount Calc. %Drift -------------
86 Cyclohexanone 250.000 223.390 10.6 105 0.00 11.53
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Continuing Calibration Summary Page 3 of 3
Job Number:FA5208 Sample:VY409-CC404
Account:AMECPAP AMEC Environment & Infrastructure, Inc.Lab FileID:Y9318.D
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
----------------------- AvgRF CCRF %Dev --------------
87 4-Chlorotoluene 2.316 2.389 -3.2 114 0.00 11.61
88 tert-Butylbenzene 1.454 1.560 -7.3 119 0.00 11.79
89 1,2,4-Trimethylbenzene 2.879 3.007 -4.4 117 0.00 11.86
90 Pentachloroethane 0.385 0.438 -13.8 122 0.00 11.83
91 sec-Butylbenzene 3.134 3.393 -8.3 123 0.00 11.98
92 4-Isopropyltoluene 2.603 2.789 -7.1 120 0.00 12.12
93 1,3-Dichlorobenzene 1.356 1.394 -2.8 113 0.00 12.22
94 1,4-Dichlorobenzene 1.526 1.534 -0.5 115 0.00 12.31
95 n-Butylbenzene 1.631 1.798 -10.2 124 0.00 12.55
96 Benzyl Chloride 0.355 0.388 -9.3 117 0.00 12.55
97 1,2-Dichlorobenzene 1.323 1.337 -1.1 114 0.00 12.75
98 1,2-Dibromo-3-Chloropropa 0.161 0.155 3.7 102 0.00 13.56
99 Hexachlorobutadiene 0.357 0.386 -8.1 124 0.00 14.16
100 1,2,4-Trichlorobenzene 0.858 0.875 -2.0 113 0.00 14.20
101 Naphthalene 2.208 2.174 1.5 103 0.00 14.48
102 1,2,3-Trichlorobenzene 0.751 0.714 4.9 104 0.00 14.64
103 I Tert Butyl Alcohol-d10 1.000 1.000 0.0 98 0.00 4.40
104 Ethanol 0.100 0.098 2.0 103 0.01 3.45
105 Acrolein 1.884 2.102 -11.6 109 0.00 3.88
106 Tert butyl alcohol 1.298 1.286 0.9 102 0.00 4.48
107 Isobutyl alcohol 0.342 0.343 -0.3 101 0.00 6.54
108 Tert Amyl Alcohol 1.114 1.188 -6.6 107 0.00 6.66
109 1,4-Dioxane 0.093 0.094 -1.1 100 0.00 7.76
--------------------------------------------------------------------------
--------------------------------------------------------------------------
(#) = Out of Range SPCC's out = 0 CCC's out = 0
Y9184.D 052913APP9-Y.m Thu Jun 06 08:53:42 2013
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Accutest LabLink@144523 15:22 27-Aug-2013
Metals Analysis
QC Data Summaries
Includes the following where applicable:
• Instrument Runlogs
• Initial and Continuing Calibration Blanks
• Initial and Continuing Calibration Checks
• High and Low Check Standards
• Interfering Element Check Standards
• Method Blank Summaries
• Matrix Spike and Duplicate Summaries
• Blank Spike and Lab Control Sample Summaries
• Serial Dilution Summaries
• IDL and Linear Range Summaries
Southeast
Section 7
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Accutest Laboratories Instrument Runlog
Inorganics Analyses
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061213M1.ICP Date Analyzed: 06/12/13 Methods: SW846 6010C
Analyst: LM Run ID: MA10817
Parameters: As,Se
Sample Dilution PS
Time Description Factor Recov Comments
08:06 MA10817-STD1 1 STDA
08:10 MA10817-STD2 1 STDB
08:14 MA10817-STD3 1 STDC
08:18 MA10817-STD4 1 STDD
08:24 MA10817-HSTD1 1
08:34 MA10817-ICV1 1
08:41 MA10817-ICB1 1
08:45 MA10817-CRIA1 1
08:53 MA10817-ICSA1 1
09:03 MA10817-ICSAB1 1
09:11 MA10817-CCV1 1
09:20 MA10817-CCB1 1
09:26 MP25296-MB1 1
09:31 MP25296-B1 1
09:35 FA5145-25R 1 (sample used for QC only; not part of login FA5208)
09:39 MP25296-D1 1
09:44 MP25296-SD1 5
09:48 MP25296-PS1 1
09:53 MP25296-S1 1
09:57 MP25296-S2 1
10:01 ZZZZZZ 1
10:06 ZZZZZZ 1
10:10 MA10817-CCV2 1
10:14 MA10817-CCB2 1
10:19 ZZZZZZ 1
10:23 ZZZZZZ 1
10:28 ZZZZZZ 1
10:32 ZZZZZZ 1
10:37 ZZZZZZ 1
10:41 FA5208-3 1
10:46 FA5208-4 1
10:51 FA5208-5 1
10:56 FA5208-6 1
_________________________________________________________________________________________________________
Page 1
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Accutest Laboratories Instrument Runlog
Inorganics Analyses
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061213M1.ICP Date Analyzed: 06/12/13 Methods: SW846 6010C
Analyst: LM Run ID: MA10817
Parameters: As,Se
Sample Dilution PS
Time Description Factor Recov Comments
11:00 FA5208-7 1
11:05 MA10817-CCV3 1
11:09 MA10817-CCB3 1
11:14 FA5208-8 1
11:18 FA5208-9 1
11:23 FA5208-10 1
11:27 FA5208-11 1
11:36 FA5208-13 1
11:45 MP25297-MB1 1
11:50 MP25297-B1 1
11:54 FA5208-15 1
11:59 MA10817-CCV4 1
12:03 MA10817-CCB4 1
12:08 MP25297-D1 1
12:13 MP25297-SD1 5
12:17 MP25297-PS1 1
12:22 MP25297-S1 1
12:26 MP25297-S2 1
12:41 FA5208-18 1
12:46 FA5208-19 1
-----------> Last reportable sample/prep for job FA5208
12:55 MA10817-CCV5 1
12:59 MA10817-CCB5 1
13:08 ZZZZZZ 1
13:13 ZZZZZZ 1
13:18 ZZZZZZ 200
13:22 ZZZZZZ 10
13:27 ZZZZZZ 4
13:31 ZZZZZZ 10
13:36 ZZZZZZ 4
13:40 ZZZZZZ 4
13:44 ZZZZZZ 5
13:49 MA10817-CCV6 1
13:53 MA10817-CCB6 1
_________________________________________________________________________________________________________
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Accutest Laboratories Instrument Runlog
Inorganics Analyses
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061213M1.ICP Date Analyzed: 06/12/13 Methods: SW846 6010C
Analyst: LM Run ID: MA10817
Parameters: As,Se
Sample Dilution PS
Time Description Factor Recov Comments
13:58 ZZZZZZ 2
14:02 ZZZZZZ 2
14:06 MA10817-CRIA2 1
14:11 MA10817-ICSA2 1
14:16 MA10817-ICSAB2 1
14:20 MA10817-CCV7 1
14:24 MA10817-CCB7 1
-----------> Last reportable CCB for job FA5208
Refer to raw data for calibration curve and standards.
_________________________________________________________________________________________________________
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INTERNAL STANDARD SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061213M1.ICP Date Analyzed: 06/12/13 Methods: SW846 6010C
Analyst: LM Run ID: MA10817
Parameters: As,Se
Sample
Time Description Istd#1 Istd#2 Istd#3 Istd#4
08:06 MA10817-STD1 1701 17808 7361 982
08:10 MA10817-STD2 1669 17320 7300 915
08:14 MA10817-STD3 1596 16733 7222 828
08:18 MA10817-STD4 1533 16281 7153 762
08:24 MA10817-HSTD1 1539 16388 7126 762
08:34 MA10817-ICV1 1603 16786 7201 826
08:41 MA10817-ICB1 1713 R 17940 R 7374 R 980 R
08:45 MA10817-CRIA1 1692 17585 7345 944
08:53 MA10817-ICSA1 1415 14606 6694 702
09:03 MA10817-ICSAB1 1411 14546 6664 690
09:11 MA10817-CCV1 1596 16749 7216 823
09:20 MA10817-CCB1 1705 17965 7328 975
09:26 MP25296-MB1 1662 17724 7205 955
09:31 MP25296-B1 1627 16906 7190 864
09:35 FA5145-25R 1521 16007 7055 737
09:39 MP25296-D1 1504 15725 7028 689
09:44 MP25296-SD1 1620 16969 7224 867
09:48 MP25296-PS1 1514 15895 7027 730
09:53 MP25296-S1 1487 15539 6904 696
09:57 MP25296-S2 1480 15472 6903 697
10:01 ZZZZZZ 1672 17390 7390 864
10:06 ZZZZZZ 2357 ! 24310 ! 10619 ! 801
10:10 MA10817-CCV2 1611 16857 7236 829
10:14 MA10817-CCB2 1707 17882 7335 977
10:19 ZZZZZZ 1676 17455 7306 908
10:23 ZZZZZZ 1688 17690 7369 920
10:28 ZZZZZZ 1755 18272 7757 873
10:32 ZZZZZZ 1679 17771 7287 939
10:37 ZZZZZZ 1715 17907 7499 901
10:41 FA5208-3 1824 19177 8351 726
10:46 FA5208-4 1932 20385 8837 734
10:51 FA5208-5 1920 20272 8661 836
10:56 FA5208-6 2039 21352 9117 842
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INTERNAL STANDARD SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061213M1.ICP Date Analyzed: 06/12/13 Methods: SW846 6010C
Analyst: LM Run ID: MA10817
Parameters: As,Se
Sample
Time Description Istd#1 Istd#2 Istd#3 Istd#4
11:00 FA5208-7 1821 19156 8103 860
11:05 MA10817-CCV3 1620 16942 7198 829
11:09 MA10817-CCB3 1719 18069 7277 976
11:14 FA5208-8 1956 20378 8606 850
11:18 FA5208-9 1863 19877 8456 833
11:23 FA5208-10 1588 16953 7277 852
11:27 FA5208-11 1642 17214 7205 878
11:36 FA5208-13 1661 17135 7199 870
11:45 MP25297-MB1 1680 17746 7175 960
11:50 MP25297-B1 1598 16662 7022 845
11:54 FA5208-15 1929 20232 8601 844
11:59 MA10817-CCV4 1620 16879 7158 827
12:03 MA10817-CCB4 1712 17906 7255 976
12:08 MP25297-D1 1960 20648 8791 830
12:13 MP25297-SD1 1754 18308 7580 919
12:17 MP25297-PS1 1906 19921 8517 828
12:22 MP25297-S1 1865 19517 8418 801
12:26 MP25297-S2 1881 19692 8467 802
12:41 FA5208-18 1701 17934 7705 812
12:46 FA5208-19 2134 22543 8817 800
12:55 MA10817-CCV5 1613 16881 7112 828
12:59 MA10817-CCB5 1710 17909 7215 974
13:08 ZZZZZZ 2185 22998 9721 795
13:13 ZZZZZZ 2680 ! 27736 ! 11752 ! 808
13:18 ZZZZZZ 1681 17154 7187 907
13:22 ZZZZZZ 1929 19590 8236 915
13:27 ZZZZZZ 1889 19261 8208 856
13:31 ZZZZZZ 1802 18344 7683 926
13:36 ZZZZZZ 1898 19387 8180 906
13:40 ZZZZZZ 1918 19578 8265 903
13:44 ZZZZZZ 1718 18392 7773 905
13:49 MA10817-CCV6 1613 16396 7086 832
13:53 MA10817-CCB6 1717 17500 7183 985
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INTERNAL STANDARD SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061213M1.ICP Date Analyzed: 06/12/13 Methods: SW846 6010C
Analyst: LM Run ID: MA10817
Parameters: As,Se
Sample
Time Description Istd#1 Istd#2 Istd#3 Istd#4
13:58 ZZZZZZ 2004 20351 8818 851
14:02 ZZZZZZ 1972 20016 8602 870
14:06 MA10817-CRIA2 1701 17212 7198 947
14:11 MA10817-ICSA2 1436 14389 6621 712
14:16 MA10817-ICSAB2 1434 14380 6600 700
14:20 MA10817-CCV7 1606 16258 7030 832
14:24 MA10817-CCB7 1708 17347 7201 981
R = Reference for ISTD limits. ! = Outside limits.
LEGEND:
Istd# Parameter Limits_______ ________________________ __________
Istd#1 Yttrium (2243) 60-125 %
Istd#2 Yttrium (3600) 60-125 %
Istd#3 Yttrium (3710) 60-125 %
Istd#4 Indium 60-125 %
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BLANK RESULTS SUMMARY
Part 1 - Initial and Continuing Calibration Blanks
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061213M1.ICP Date Analyzed: 06/12/13 Methods: SW846 6010C
QC Limits: result < RL Run ID: MA10817 Units: ug/l
Time: 08:41 09:20 10:14 11:09
Sample ID: ICB1 CCB1 CCB2 CCB3
Metal RL IDL raw final raw final raw final raw final
Aluminum 200 15 anr
Antimony 20 1.3
Arsenic 10 1.6 0.40 <10 0.30 <10 0.30 <10 0.90 <10
Barium 200 1 anr
Beryllium 5.0 .5
Cadmium 4.0 .5 anr
Calcium 5000 50
Chromium 10 1.8 anr
Cobalt 50 .5
Copper 25 1 anr
Iron 300 29 anr
Lead 20 1.1 anr
Magnesium 5000 74
Manganese 15 .7
Molybdenum 50 .6
Nickel 40 .5 anr
Potassium 10000 200
Selenium 20 2 0.90 <20 0.80 <20 2.1 <20 3.8 <20
Silver 10 .5 anr
Sodium 10000 500 anr
Strontium 10 .5
Thallium 10 1.3 anr
Tin 50 .7
Titanium 10 .9
Vanadium 50 .5 anr
Zinc 20 3
(*) Outside of QC limits
(anr) Analyte not requested
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BLANK RESULTS SUMMARY
Part 1 - Initial and Continuing Calibration Blanks
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061213M1.ICP Date Analyzed: 06/12/13 Methods: SW846 6010C
QC Limits: result < RL Run ID: MA10817 Units: ug/l
Time: 12:03 12:59 13:53 14:24
Sample ID: CCB4 CCB5 CCB6 CCB7
Metal RL IDL raw final raw final raw final raw final
Aluminum 200 15 anr
Antimony 20 1.3
Arsenic 10 1.6 0.50 <10 0.0 <10 0.20 <10 -0.30 <10
Barium 200 1 anr
Beryllium 5.0 .5
Cadmium 4.0 .5 anr
Calcium 5000 50
Chromium 10 1.8 anr
Cobalt 50 .5
Copper 25 1 anr
Iron 300 29 anr
Lead 20 1.1 anr
Magnesium 5000 74
Manganese 15 .7
Molybdenum 50 .6
Nickel 40 .5 anr
Potassium 10000 200
Selenium 20 2 3.0 <20 4.1 <20 2.3 <20 0.30 <20
Silver 10 .5 anr
Sodium 10000 500 anr
Strontium 10 .5
Thallium 10 1.3 anr
Tin 50 .7
Titanium 10 .9
Vanadium 50 .5 anr
Zinc 20 3
(*) Outside of QC limits
(anr) Analyte not requested
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CALIBRATION CHECK STANDARDS SUMMARY
Initial and Continuing Calibration Checks
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061213M1.ICP Date Analyzed: 06/12/13 Methods: SW846 6010C
QC Limits: 90 to 110 % Recovery Run ID: MA10817 Units: ug/l
Time: 08:34 09:11 10:10
Sample ID: ICV ICV1 CCV CCV1 CCV CCV2
Metal True Results % Rec True Results % Rec True Results % Rec
Aluminum anr
Antimony
Arsenic 2000 2020 101.0 2000 2010 100.5 2000 2000 100.0
Barium anr
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper anr
Iron anr
Lead anr
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium 2000 2020 101.0 2000 2010 100.5 2000 2010 100.5
Silver anr
Sodium anr
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc
(*) Outside of QC limits
(anr) Analyte not requested
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CALIBRATION CHECK STANDARDS SUMMARY
Initial and Continuing Calibration Checks
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061213M1.ICP Date Analyzed: 06/12/13 Methods: SW846 6010C
QC Limits: 90 to 110 % Recovery Run ID: MA10817 Units: ug/l
Time: 11:05 11:59 12:55
Sample ID: CCV CCV3 CCV CCV4 CCV CCV5
Metal True Results % Rec True Results % Rec True Results % Rec
Aluminum anr
Antimony
Arsenic 2000 2010 100.5 2000 2020 101.0 2000 2020 101.0
Barium anr
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper anr
Iron anr
Lead anr
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium 2000 2020 101.0 2000 2010 100.5 2000 2020 101.0
Silver anr
Sodium anr
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc
(*) Outside of QC limits
(anr) Analyte not requested
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CALIBRATION CHECK STANDARDS SUMMARY
Initial and Continuing Calibration Checks
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061213M1.ICP Date Analyzed: 06/12/13 Methods: SW846 6010C
QC Limits: 90 to 110 % Recovery Run ID: MA10817 Units: ug/l
Time: 13:49 14:20
Sample ID: CCV CCV6 CCV CCV7
Metal True Results % Rec True Results % Rec
Aluminum anr
Antimony
Arsenic 2000 2030 101.5 2000 2040 102.0
Barium anr
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper anr
Iron anr
Lead anr
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium 2000 2040 102.0 2000 2050 102.5
Silver anr
Sodium anr
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc
(*) Outside of QC limits
(anr) Analyte not requested
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HIGH STANDARD CHECK SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061213M1.ICP Date Analyzed: 06/12/13 Methods: SW846 6010C
QC Limits: 95 to 105 % Recovery Run ID: MA10817 Units: ug/l
Time: 08:24
Sample ID: HSTD HSTD1
Metal True Results % Rec
Aluminum anr
Antimony
Arsenic 4000 4020 100.5
Barium anr
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper anr
Iron anr
Lead anr
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium 4000 3980 99.5
Silver anr
Sodium anr
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc
(*) Outside of QC limits
(anr) Analyte not requested
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LOW CALIBRATION CHECK STANDARDS SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061213M1.ICP Date Analyzed: 06/12/13 Methods: SW846 6010C
QC Limits: CRI 70-130% CRIA 70-130% Run ID: MA10817 Units: ug/l
Time: 08:45 14:06
Sample ID: CRI CRIA CRIA1 CRIA2
Metal True True Results % Rec Results % Rec
Aluminum 400 200 anr
Antimony 10 5.0
Arsenic 20 10 10.8 108.0 10.8 108.0
Barium 400 200 anr
Beryllium 10 5.0
Cadmium 10 5.0 anr
Calcium 2000 1000
Chromium 20 10 anr
Cobalt 100 50
Copper 50 25 anr
Iron 600 300 anr
Lead 10 5.0 anr
Magnesium 10000 5000
Manganese 30 15
Molybdenum 100 50
Nickel 80 40 anr
Potassium 20000 10000
Selenium 20 10 11.1 111.0 11.7 117.0
Silver 20 10 anr
Sodium 20000 10000 anr
Strontium 20 10
Thallium 20 10 anr
Tin 100 50
Titanium 20 10
Vanadium 100 50 anr
Zinc 40 20
(*) Outside of QC limits
(anr) Analyte not requested
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INTERFERING ELEMENT CHECK STANDARDS SUMMARY
Part 1 - ICSA and ICSAB Standards
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061213M1.ICP Date Analyzed: 06/12/13 Methods: SW846 6010C
QC Limits: 80 to 120 % Recovery Run ID: MA10817 Units: ug/l
Time: 08:53 09:03 14:11 14:16
Sample ID: ICSA ICSAB ICSA1 ICSAB1 ICSA2 ICSAB2
Metal True True Results % Rec Results % Rec Results % Rec Results % Rec
Aluminum 500000 500000 527000 105.4 528000 105.6 516000 103.2 513000 102.6
Antimony 1000 0.0 1070 107.0 1.8 1070 107.0
Arsenic 1000 -0.50 1080 108.0 2.0 1080 108.0
Barium 500 -0.30 539 107.8 -0.40 534 106.8
Beryllium 500 -0.50 527 105.4 -0.50 525 105.0
Cadmium 1000 0.10 969 96.9 -1.1 985 98.5
Calcium 500000 500000 509000 101.8 510000 102.0 520000 104.0 519000 103.8
Chromium 500 -0.40 507 101.4 -0.10 527 105.4
Cobalt 500 -1.2 481 96.2 -1.1 480 96.0
Copper 500 0.0 565 113.0 -0.80 570 114.0
Iron 200000 200000 193000 96.5 204000 102.0 195000 97.5 206000 103.0
Lead 1000 -0.10 983 98.3 -2.6 996 99.6
Magnesium 500000 500000 533000 106.6 536000 107.2 538000 107.6 535000 107.0
Manganese 500 0.20 518 103.6 -0.10 533 106.6
Molybdenum 1000 -0.90 938 93.8 -1.0 931 93.1
Nickel 1000 0.0 953 95.3 -0.40 965 96.5
Potassium -0.40 -25 -80 -41
Selenium 1000 0.0 1020 102.0 7.7 1030 103.0
Silver 1000 0.40 1050 105.0 0.10 1070 107.0
Sodium 89.3 119 77.1 128
Strontium 1000 11.9 1060 106.0 11.9 1050 105.0
Thallium 1000 0.10 960 96.0 3.9 974 97.4
Tin 1000 4.8 938 93.8 4.9 945 94.5
Titanium 1000 -2.3 1010 101.0 -2.3 1040 104.0
Vanadium 500 0.0 502 100.4 0.10 514 102.8
Zinc 1000 -3.0 985 98.5 -3.2 1010 101.0
(*) Outside of QC limits
(anr) Analyte not requested
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Accutest Laboratories Instrument Runlog
Inorganics Analyses
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
Analyst: LM Run ID: MA10821
Parameters: As,Se
Sample Dilution PS
Time Description Factor Recov Comments
07:57 MA10821-STD1 1 STDA
08:00 MA10821-STD2 1 STDB
08:06 MA10821-STD3 1 STDC
08:09 MA10821-STD4 1 STDD
08:14 MA10821-HSTD1 1
08:22 MA10821-ICV1 1
08:29 MA10821-ICB1 1
08:34 MA10821-CRIA1 1
08:42 MA10821-ICSA1 1
08:54 MA10821-ICSAB1 1
09:00 MA10821-CCV1 1
09:06 MA10821-CCB1 1
09:10 MP25301-MB1 1
09:15 MP25301-B1 1
09:19 FA5428-1 1 (sample used for QC only; not part of login FA5208)
09:23 MP25301-D1 1
09:28 MP25301-SD1 5
09:32 MP25301-PS1 1
09:37 MP25301-S1 1
09:41 MP25301-S2 1
09:45 ZZZZZZ 1
09:49 ZZZZZZ 1
09:54 MA10821-CCV2 1
09:58 MA10821-CCB2 1
10:02 ZZZZZZ 1
10:07 ZZZZZZ 1
10:11 ZZZZZZ 1
10:16 ZZZZZZ 1
10:20 ZZZZZZ 1
10:25 ZZZZZZ 1
10:29 ZZZZZZ 1
10:34 ZZZZZZ 1
10:38 ZZZZZZ 1
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Accutest Laboratories Instrument Runlog
Inorganics Analyses
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
Analyst: LM Run ID: MA10821
Parameters: As,Se
Sample Dilution PS
Time Description Factor Recov Comments
10:43 ZZZZZZ 1
10:47 MA10821-CCV3 1
10:51 MA10821-CCB3 1
10:56 ZZZZZZ 1
11:00 ZZZZZZ 1
11:05 ZZZZZZ 1
11:09 ZZZZZZ 1
11:14 ZZZZZZ 1
11:18 ZZZZZZ 1
11:23 ZZZZZZ 1
11:27 MP25306-MB1 1
11:31 MP25306-B1 1
11:36 FA5349-1 1 (sample used for QC only; not part of login FA5208)
11:40 MA10821-CCV4 1
11:45 MA10821-CCB4 1
11:49 MP25306-D1 1
11:54 MP25306-SD1 5
11:58 MP25306-S1 1
12:03 MP25306-S2 1
12:07 ZZZZZZ 1
12:12 ZZZZZZ 1
12:16 FA5395-3 1 (sample used for QC only; not part of login FA5208)
12:21 ZZZZZZ 1
12:26 ZZZZZZ 1
12:30 ZZZZZZ 1
12:35 MA10821-CCV5 1
12:39 MA10821-CCB5 1
12:44 MP25306-D2 1
12:48 MP25306-D3 1
12:53 MP25306-MB2 1
12:58 MP25306-B2 1
13:02 MP25306-MB3 1
13:07 MP25306-B3 1
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Accutest Laboratories Instrument Runlog
Inorganics Analyses
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
Analyst: LM Run ID: MA10821
Parameters: As,Se
Sample Dilution PS
Time Description Factor Recov Comments
13:11 FA5145-25R 2 (sample used for QC only; not part of login FA5208)
13:16 MP25296-D1 2
13:20 MP25296-S1 2
13:25 MP25296-S2 2
13:29 MA10821-CCV6 1
13:33 MA10821-CCB6 1
13:38 MP25296-PS1 2
13:42 MP25296-SD1 10
13:46 ZZZZZZ 2
13:51 FA5208-12 2
13:55 FA5208-14 4
14:00 FA5208-16 10
14:04 FA5208-17 5
14:08 FA5208-20 5
-----------> Last reportable sample/prep for job FA5208
14:13 ZZZZZZ 2
14:17 ZZZZZZ 4
14:22 MA10821-CCV7 1
14:26 MA10821-CCB7 1
14:51 MA10821-CCV8 1
14:55 MA10821-CCB8 1
15:00 MP25307-MB1 1
15:04 MP25307-B1 1
15:08 FA5343-1 1 (sample used for QC only; not part of login FA5208)
15:13 MP25307-D1 1
15:17 MP25307-SD1 5
15:22 MP25307-PS1 1
15:26 MP25307-S1 1
15:31 MP25307-S2 1
15:35 ZZZZZZ 1
15:39 ZZZZZZ 1
15:44 MA10821-CCV9 1
15:48 MA10821-CCB9 1
15:53 ZZZZZZ 1
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Accutest Laboratories Instrument Runlog
Inorganics Analyses
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
Analyst: LM Run ID: MA10821
Parameters: As,Se
Sample Dilution PS
Time Description Factor Recov Comments
15:57 ZZZZZZ 1
16:02 ZZZZZZ 1
16:06 ZZZZZZ 1
16:10 ZZZZZZ 1
16:15 ZZZZZZ 1
16:19 ZZZZZZ 1
16:24 ZZZZZZ 1
16:28 ZZZZZZ 1
16:33 ZZZZZZ 1
16:37 MA10821-CCV10 1
16:42 MA10821-CCB10 1
16:46 ZZZZZZ 1
16:51 ZZZZZZ 1
16:55 ZZZZZZ 1
16:59 ZZZZZZ 1
17:04 ZZZZZZ 1
17:08 ZZZZZZ 1
17:18 MP25307-MB2A 1
17:22 MP25308-MB1 1
17:27 MP25308-B1 1
17:31 MA10821-CCV11 1
17:35 MA10821-CCB11 1
17:40 FA5387-1 1 (sample used for QC only; not part of login FA5208)
17:44 MP25308-D1 1
17:49 MP25308-SD1 5
17:53 MP25308-PS1 1
17:58 MP25308-S1 1
18:02 MP25308-S2 1
18:06 ZZZZZZ 1
18:11 ZZZZZZ 1
18:15 ZZZZZZ 1
18:20 ZZZZZZ 1
18:24 MA10821-CCV12 1
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Accutest Laboratories Instrument Runlog
Inorganics Analyses
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
Analyst: LM Run ID: MA10821
Parameters: As,Se
Sample Dilution PS
Time Description Factor Recov Comments
18:28 MA10821-CCB12 1
18:33 ZZZZZZ 1
18:38 ZZZZZZ 1
18:42 ZZZZZZ 1
18:46 ZZZZZZ 1
18:51 ZZZZZZ 1
18:55 ZZZZZZ 1
19:00 ZZZZZZ 1
19:04 ZZZZZZ 1
19:09 ZZZZZZ 1
19:13 ZZZZZZ 1
19:18 MA10821-CCV13 1
19:22 MA10821-CCB13 1
19:27 ZZZZZZ 1
19:31 ZZZZZZ 1
19:36 ZZZZZZ 1
19:40 ZZZZZZ 1
19:45 MP25308-MB2A 1
19:49 MP25308-MB3A 1
19:54 MA10821-CRIA2 1
19:58 MA10821-ICSA2 1
20:03 MA10821-ICSAB2 1
20:07 MA10821-CCV14 1
20:12 MA10821-CCB14 1
-----------> Last reportable CCB for job FA5208
Refer to raw data for calibration curve and standards.
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INTERNAL STANDARD SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
Analyst: LM Run ID: MA10821
Parameters: As,Se
Sample
Time Description Istd#1 Istd#2 Istd#3 Istd#4
07:57 MA10821-STD1 4105 30601 8382 1927
08:00 MA10821-STD2 4085 30160 8425 1808
08:06 MA10821-STD3 3949 29159 8353 1643
08:09 MA10821-STD4 3803 28474 8247 1523
08:14 MA10821-HSTD1 3806 28390 8218 1519
08:22 MA10821-ICV1 3946 29165 8278 1653
08:29 MA10821-ICB1 4129 R 30548 R 8416 R 1936 R
08:34 MA10821-CRIA1 4081 30255 8409 1867
08:42 MA10821-ICSA1 3667 26562 8101 1416
08:54 MA10821-ICSAB1 3646 26585 8002 1385
09:00 MA10821-CCV1 3960 29404 8266 1644
09:06 MA10821-CCB1 4121 30659 8365 1928
09:10 MP25301-MB1 4126 30963 8468 1929
09:15 MP25301-B1 4013 29631 8380 1727
09:19 FA5428-1 4057 30126 8449 1809
09:23 MP25301-D1 4055 30311 8485 1818
09:28 MP25301-SD1 4131 30789 8411 1912
09:32 MP25301-PS1 4032 30100 8445 1767
09:37 MP25301-S1 3983 29599 8400 1676
09:41 MP25301-S2 3972 29628 8359 1669
09:45 ZZZZZZ 3993 29888 8345 1757
09:49 ZZZZZZ 4031 30010 8453 1759
09:54 MA10821-CCV2 3997 29627 8375 1658
09:58 MA10821-CCB2 4122 30779 8384 1925
10:02 ZZZZZZ 4032 30075 8448 1736
10:07 ZZZZZZ 4160 31442 8503 1947
10:11 ZZZZZZ 3965 29738 8510 1656
10:16 ZZZZZZ 3957 30117 8384 1791
10:20 ZZZZZZ 3977 29910 8371 1779
10:25 ZZZZZZ 3863 28993 8161 1758
10:29 ZZZZZZ 3849 28941 8145 1696
10:34 ZZZZZZ 3974 29914 8328 1811
10:38 ZZZZZZ 4060 30744 8355 1935
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INTERNAL STANDARD SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
Analyst: LM Run ID: MA10821
Parameters: As,Se
Sample
Time Description Istd#1 Istd#2 Istd#3 Istd#4
10:43 ZZZZZZ 4055 30828 8356 1934
10:47 MA10821-CCV3 3903 29273 8138 1651
10:51 MA10821-CCB3 4060 30499 8245 1928
10:56 ZZZZZZ 3984 30019 8283 1839
11:00 ZZZZZZ 3921 29783 8283 1773
11:05 ZZZZZZ 4122 31086 8683 1784
11:09 ZZZZZZ 3803 28699 8062 1723
11:14 ZZZZZZ 4067 30691 8570 1775
11:18 ZZZZZZ 3918 29623 8297 1764
11:23 ZZZZZZ 4140 31345 8741 1792
11:27 MP25306-MB1 4063 30953 8311 1935
11:31 MP25306-B1 3940 29683 8242 1724
11:36 FA5349-1 3837 28613 8184 1713
11:40 MA10821-CCV4 3890 29259 8172 1638
11:45 MA10821-CCB4 4049 30626 8201 1920
11:49 MP25306-D1 3846 28734 8194 1707
11:54 MP25306-SD1 3967 29852 8091 1833
11:58 MP25306-S1 3818 28639 8200 1615
12:03 MP25306-S2 3825 28637 8186 1620
12:07 ZZZZZZ 3797 28350 8159 1669
12:12 ZZZZZZ 3779 28455 8169 1652
12:16 FA5395-3 3759 28770 8121 1688
12:21 ZZZZZZ 3763 28775 8182 1686
12:26 ZZZZZZ 3760 28813 8133 1692
12:30 ZZZZZZ 3761 28412 8217 1653
12:35 MA10821-CCV5 3876 29183 8156 1635
12:39 MA10821-CCB5 4024 30391 8237 1910
12:44 MP25306-D2 3821 28629 8196 1705
12:48 MP25306-D3 3761 28729 8179 1691
12:53 MP25306-MB2 3799 28430 8216 1696
12:58 MP25306-B2 3794 28554 8193 1607
13:02 MP25306-MB3 4036 30915 8400 1927
13:07 MP25306-B3 3906 29755 8281 1718
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INTERNAL STANDARD SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
Analyst: LM Run ID: MA10821
Parameters: As,Se
Sample
Time Description Istd#1 Istd#2 Istd#3 Istd#4
13:11 FA5145-25R 3860 29165 8178 1603
13:16 MP25296-D1 3810 28711 8188 1521
13:20 MP25296-S1 3815 28647 8119 1533
13:25 MP25296-S2 3842 28890 8242 1555
13:29 MA10821-CCV6 3885 29284 8100 1635
13:33 MA10821-CCB6 4019 30503 8193 1909
13:38 MP25296-PS1 3830 28970 8191 1578
13:42 MP25296-SD1 3963 29825 8141 1778
13:46 ZZZZZZ 4856 36289 10082 1693
13:51 FA5208-12 4855 36382 9978 1746
13:55 FA5208-14 5070 37930 10454 1685
14:00 FA5208-16 4907 36877 10194 1741
14:04 FA5208-17 4934 36996 10290 1694
14:08 FA5208-20 4956 36844 10321 1702
14:13 ZZZZZZ 5131 38197 10595 1741
14:17 ZZZZZZ 4644 34941 9566 1744
14:22 MA10821-CCV7 3855 29147 8107 1629
14:26 MA10821-CCB7 4016 30448 8155 1901
14:51 MA10821-CCV8 3842 29168 8100 1621
14:55 MA10821-CCB8 4003 30406 8167 1900
15:00 MP25307-MB1 4000 30637 8335 1900
15:04 MP25307-B1 3873 29511 8164 1693
15:08 FA5343-1 3949 30306 8243 1843
15:13 MP25307-D1 3961 30380 8315 1852
15:17 MP25307-SD1 4000 30511 8246 1896
15:22 MP25307-PS1 3934 29989 8215 1781
15:26 MP25307-S1 3866 29381 8230 1672
15:31 MP25307-S2 3878 29538 8167 1682
15:35 ZZZZZZ 3992 30705 8278 1888
15:39 ZZZZZZ 4004 30521 8325 1878
15:44 MA10821-CCV9 3824 29038 8086 1617
15:48 MA10821-CCB9 3986 30310 8205 1904
15:53 ZZZZZZ 3990 30506 8306 1891
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INTERNAL STANDARD SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
Analyst: LM Run ID: MA10821
Parameters: As,Se
Sample
Time Description Istd#1 Istd#2 Istd#3 Istd#4
15:57 ZZZZZZ 3983 30579 8318 1886
16:02 ZZZZZZ 3987 30503 8335 1887
16:06 ZZZZZZ 4023 30700 8405 1844
16:10 ZZZZZZ 3929 30009 8258 1853
16:15 ZZZZZZ 3968 30253 8213 1878
16:19 ZZZZZZ 3959 30230 8239 1873
16:24 ZZZZZZ 3977 30448 8271 1884
16:28 ZZZZZZ 3927 29766 8322 1746
16:33 ZZZZZZ 3860 29444 8267 1746
16:37 MA10821-CCV10 3822 29003 8112 1619
16:42 MA10821-CCB10 3959 30244 8134 1894
16:46 ZZZZZZ 3852 29386 8289 1695
16:51 ZZZZZZ 3864 29426 8211 1768
16:55 ZZZZZZ 3906 29941 8318 1784
16:59 ZZZZZZ 3934 29867 8420 1689
17:04 ZZZZZZ 3856 29532 8275 1756
17:08 ZZZZZZ 3723 28403 8122 1649
17:18 MP25307-MB2A 3956 30523 8294 1894
17:22 MP25308-MB1 3964 30636 8197 1901
17:27 MP25308-B1 3845 29441 8222 1696
17:31 MA10821-CCV11 3805 29038 8119 1617
17:35 MA10821-CCB11 3966 30331 8197 1897
17:40 FA5387-1 3924 30225 8323 1855
17:44 MP25308-D1 3926 30212 8258 1864
17:49 MP25308-SD1 3965 30378 8271 1888
17:53 MP25308-PS1 3913 30112 8297 1789
17:58 MP25308-S1 3853 29386 8268 1674
18:02 MP25308-S2 3832 29251 8216 1666
18:06 ZZZZZZ 3937 30369 8313 1864
18:11 ZZZZZZ 3905 30053 8242 1853
18:15 ZZZZZZ 3984 30651 8313 1889
18:20 ZZZZZZ 3995 30656 8292 1891
18:24 MA10821-CCV12 3810 28832 8117 1611
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INTERNAL STANDARD SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
Analyst: LM Run ID: MA10821
Parameters: As,Se
Sample
Time Description Istd#1 Istd#2 Istd#3 Istd#4
18:28 MA10821-CCB12 3987 30364 8172 1903
18:33 ZZZZZZ 3960 30301 8206 1858
18:38 ZZZZZZ 3868 29628 8173 1804
18:42 ZZZZZZ 3861 29528 8237 1805
18:46 ZZZZZZ 3851 29514 8188 1803
18:51 ZZZZZZ 3754 28596 8078 1703
18:55 ZZZZZZ 3809 29095 8155 1763
19:00 ZZZZZZ 3809 28987 8176 1749
19:04 ZZZZZZ 3957 30066 8253 1877
19:09 ZZZZZZ 3901 29577 8233 1801
19:13 ZZZZZZ 3775 28753 8079 1721
19:18 MA10821-CCV13 3818 28815 8096 1629
19:22 MA10821-CCB13 3958 29829 8140 1901
19:27 ZZZZZZ 3801 28892 8173 1751
19:31 ZZZZZZ 3812 28986 8113 1753
19:36 ZZZZZZ 3956 30073 8252 1874
19:40 ZZZZZZ 3858 29161 8167 1789
19:45 MP25308-MB2A 3969 30369 8285 1906
19:49 MP25308-MB3A 3961 30152 8239 1906
19:54 MA10821-CRIA2 3912 29429 8125 1832
19:58 MA10821-ICSA2 3498 25801 7814 1386
20:03 MA10821-ICSAB2 3480 25736 7759 1366
20:07 MA10821-CCV14 3800 28459 8001 1619
20:12 MA10821-CCB14 3942 29664 8082 1898
R = Reference for ISTD limits. ! = Outside limits.
LEGEND:
Istd# Parameter Limits_______ ________________________ __________
Istd#1 Yttrium (2243) 60-125 %
Istd#2 Yttrium (3600) 60-125 %
Istd#3 Yttrium (3710) 60-125 %
Istd#4 Indium 60-125 %
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BLANK RESULTS SUMMARY
Part 1 - Initial and Continuing Calibration Blanks
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
QC Limits: result < RL Run ID: MA10821 Units: ug/l
Time: 08:29 09:06 09:58 10:51
Sample ID: ICB1 CCB1 CCB2 CCB3
Metal RL IDL raw final raw final raw final raw final
Aluminum 200 15 anr
Antimony 6.0 1.3 anr
Arsenic 10 1.6 0.20 <10 -0.20 <10 0.30 <10 0.80 <10
Barium 200 1 anr
Beryllium 4.0 .5 anr
Cadmium 5.0 .5 anr
Calcium 1000 50 anr
Chromium 10 1.8 anr
Cobalt 50 .5 anr
Copper 25 1 anr
Iron 300 29 anr
Lead 5.0 1.1 anr
Magnesium 5000 74 anr
Manganese 15 .7 anr
Molybdenum 50 .6
Nickel 40 .5 anr
Potassium 10000 200 anr
Selenium 10 2 1.6 <10 1.1 <10 2.3 <10 0.20 <10
Silver 10 .5 anr
Sodium 10000 500 anr
Strontium 10 .5
Thallium 10 1.3 anr
Tin 50 .7
Titanium 10 .9
Vanadium 50 .5 anr
Zinc 20 3 anr
(*) Outside of QC limits
(anr) Analyte not requested
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BLANK RESULTS SUMMARY
Part 1 - Initial and Continuing Calibration Blanks
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
QC Limits: result < RL Run ID: MA10821 Units: ug/l
Time: 11:45 12:39 13:33 14:26
Sample ID: CCB4 CCB5 CCB6 CCB7
Metal RL IDL raw final raw final raw final raw final
Aluminum 200 15 anr
Antimony 6.0 1.3 anr
Arsenic 10 1.6 -0.10 <10 0.70 <10 -0.10 <10 -0.10 <10
Barium 200 1 anr
Beryllium 4.0 .5 anr
Cadmium 5.0 .5 anr
Calcium 1000 50 anr
Chromium 10 1.8 anr
Cobalt 50 .5 anr
Copper 25 1 anr
Iron 300 29 anr
Lead 5.0 1.1 anr
Magnesium 5000 74 anr
Manganese 15 .7 anr
Molybdenum 50 .6
Nickel 40 .5 anr
Potassium 10000 200 anr
Selenium 10 2 1.4 <10 2.7 <10 2.7 <10 1.0 <10
Silver 10 .5 anr
Sodium 10000 500 anr
Strontium 10 .5
Thallium 10 1.3 anr
Tin 50 .7
Titanium 10 .9
Vanadium 50 .5 anr
Zinc 20 3 anr
(*) Outside of QC limits
(anr) Analyte not requested
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BLANK RESULTS SUMMARY
Part 1 - Initial and Continuing Calibration Blanks
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
QC Limits: result < RL Run ID: MA10821 Units: ug/l
Time: 14:55 15:48 16:42 17:35
Sample ID: CCB8 CCB9 CCB10 CCB11
Metal RL IDL raw final raw final raw final raw final
Aluminum 200 15 anr
Antimony 6.0 1.3 anr
Arsenic 10 1.6 0.60 <10 0.20 <10 0.70 <10 0.20 <10
Barium 200 1 anr
Beryllium 4.0 .5 anr
Cadmium 5.0 .5 anr
Calcium 1000 50 anr
Chromium 10 1.8 anr
Cobalt 50 .5 anr
Copper 25 1 anr
Iron 300 29 anr
Lead 5.0 1.1 anr
Magnesium 5000 74 anr
Manganese 15 .7 anr
Molybdenum 50 .6
Nickel 40 .5 anr
Potassium 10000 200 anr
Selenium 10 2 0.60 <10 0.50 <10 0.80 <10 -0.10 <10
Silver 10 .5 anr
Sodium 10000 500 anr
Strontium 10 .5
Thallium 10 1.3 anr
Tin 50 .7
Titanium 10 .9
Vanadium 50 .5 anr
Zinc 20 3 anr
(*) Outside of QC limits
(anr) Analyte not requested
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BLANK RESULTS SUMMARY
Part 1 - Initial and Continuing Calibration Blanks
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
QC Limits: result < RL Run ID: MA10821 Units: ug/l
Time: 18:28 19:22 20:12
Sample ID: CCB12 CCB13 CCB14
Metal RL IDL raw final raw final raw final
Aluminum 200 15 anr
Antimony 6.0 1.3 anr
Arsenic 10 1.6 0.20 <10 0.50 <10 0.20 <10
Barium 200 1 anr
Beryllium 4.0 .5 anr
Cadmium 5.0 .5 anr
Calcium 1000 50 anr
Chromium 10 1.8 anr
Cobalt 50 .5 anr
Copper 25 1 anr
Iron 300 29 anr
Lead 5.0 1.1 anr
Magnesium 5000 74 anr
Manganese 15 .7 anr
Molybdenum 50 .6
Nickel 40 .5 anr
Potassium 10000 200 anr
Selenium 10 2 0.0 <10 0.10 <10 1.0 <10
Silver 10 .5 anr
Sodium 10000 500 anr
Strontium 10 .5
Thallium 10 1.3 anr
Tin 50 .7
Titanium 10 .9
Vanadium 50 .5 anr
Zinc 20 3 anr
(*) Outside of QC limits
(anr) Analyte not requested
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CALIBRATION CHECK STANDARDS SUMMARY
Initial and Continuing Calibration Checks
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
QC Limits: 90 to 110 % Recovery Run ID: MA10821 Units: ug/l
Time: 08:22 09:00 09:54
Sample ID: ICV ICV1 CCV CCV1 CCV CCV2
Metal True Results % Rec True Results % Rec True Results % Rec
Aluminum anr
Antimony anr
Arsenic 2000 2030 101.5 2000 2010 100.5 2000 1990 99.5
Barium anr
Beryllium anr
Cadmium anr
Calcium anr
Chromium anr
Cobalt anr
Copper anr
Iron anr
Lead anr
Magnesium anr
Manganese anr
Molybdenum
Nickel anr
Potassium anr
Selenium 2000 2050 102.5 2000 2020 101.0 2000 2000 100.0
Silver anr
Sodium anr
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc anr
(*) Outside of QC limits
(anr) Analyte not requested
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CALIBRATION CHECK STANDARDS SUMMARY
Initial and Continuing Calibration Checks
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
QC Limits: 90 to 110 % Recovery Run ID: MA10821 Units: ug/l
Time: 10:47 11:40 12:35
Sample ID: CCV CCV3 CCV CCV4 CCV CCV5
Metal True Results % Rec True Results % Rec True Results % Rec
Aluminum anr
Antimony anr
Arsenic 2000 2050 102.5 2000 2050 102.5 2000 2050 102.5
Barium anr
Beryllium anr
Cadmium anr
Calcium anr
Chromium anr
Cobalt anr
Copper anr
Iron anr
Lead anr
Magnesium anr
Manganese anr
Molybdenum
Nickel anr
Potassium anr
Selenium 2000 2050 102.5 2000 2050 102.5 2000 2060 103.0
Silver anr
Sodium anr
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc anr
(*) Outside of QC limits
(anr) Analyte not requested
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CALIBRATION CHECK STANDARDS SUMMARY
Initial and Continuing Calibration Checks
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
QC Limits: 90 to 110 % Recovery Run ID: MA10821 Units: ug/l
Time: 13:29 14:22 14:51
Sample ID: CCV CCV6 CCV CCV7 CCV CCV8
Metal True Results % Rec True Results % Rec True Results % Rec
Aluminum anr
Antimony anr
Arsenic 2000 2050 102.5 2000 2060 103.0 2000 1990 99.5
Barium anr
Beryllium anr
Cadmium anr
Calcium anr
Chromium anr
Cobalt anr
Copper anr
Iron anr
Lead anr
Magnesium anr
Manganese anr
Molybdenum
Nickel anr
Potassium anr
Selenium 2000 2050 102.5 2000 2060 103.0 2000 2000 100.0
Silver anr
Sodium anr
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc anr
(*) Outside of QC limits
(anr) Analyte not requested
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CALIBRATION CHECK STANDARDS SUMMARY
Initial and Continuing Calibration Checks
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
QC Limits: 90 to 110 % Recovery Run ID: MA10821 Units: ug/l
Time: 15:44 16:37 17:31
Sample ID: CCV CCV9 CCV CCV10 CCV CCV11
Metal True Results % Rec True Results % Rec True Results % Rec
Aluminum anr
Antimony anr
Arsenic 2000 2000 100.0 2000 2000 100.0 2000 2020 101.0
Barium anr
Beryllium anr
Cadmium anr
Calcium anr
Chromium anr
Cobalt anr
Copper anr
Iron anr
Lead anr
Magnesium anr
Manganese anr
Molybdenum
Nickel anr
Potassium anr
Selenium 2000 2010 100.5 2000 2010 100.5 2000 2030 101.5
Silver anr
Sodium anr
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc anr
(*) Outside of QC limits
(anr) Analyte not requested
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CALIBRATION CHECK STANDARDS SUMMARY
Initial and Continuing Calibration Checks
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
QC Limits: 90 to 110 % Recovery Run ID: MA10821 Units: ug/l
Time: 18:24 19:18 20:07
Sample ID: CCV CCV12 CCV CCV13 CCV CCV14
Metal True Results % Rec True Results % Rec True Results % Rec
Aluminum anr
Antimony anr
Arsenic 2000 2020 101.0 2000 2020 101.0 2000 2030 101.5
Barium anr
Beryllium anr
Cadmium anr
Calcium anr
Chromium anr
Cobalt anr
Copper anr
Iron anr
Lead anr
Magnesium anr
Manganese anr
Molybdenum
Nickel anr
Potassium anr
Selenium 2000 2040 102.0 2000 2030 101.5 2000 2050 102.5
Silver anr
Sodium anr
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc anr
(*) Outside of QC limits
(anr) Analyte not requested
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HIGH STANDARD CHECK SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
QC Limits: 95 to 105 % Recovery Run ID: MA10821 Units: ug/l
Time: 08:14
Sample ID: HSTD HSTD1
Metal True Results % Rec
Aluminum anr
Antimony anr
Arsenic 4000 4030 100.8
Barium anr
Beryllium anr
Cadmium anr
Calcium anr
Chromium anr
Cobalt anr
Copper anr
Iron anr
Lead anr
Magnesium anr
Manganese anr
Molybdenum
Nickel anr
Potassium anr
Selenium 4000 4010 100.3
Silver anr
Sodium anr
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc anr
(*) Outside of QC limits
(anr) Analyte not requested
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LOW CALIBRATION CHECK STANDARDS SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
QC Limits: CRI 70-130% CRIA 70-130% Run ID: MA10821 Units: ug/l
Time: 08:34 19:54
Sample ID: CRI CRIA CRIA1 CRIA2
Metal True True Results % Rec Results % Rec
Aluminum 400 200 anr
Antimony 10 5.0 anr
Arsenic 20 10 10.3 103.0 11.5 115.0
Barium 400 200 anr
Beryllium 10 5.0 anr
Cadmium 10 5.0 anr
Calcium 2000 1000 anr
Chromium 20 10 anr
Cobalt 100 50 anr
Copper 50 25 anr
Iron 600 300 anr
Lead 10 5.0 anr
Magnesium 10000 5000 anr
Manganese 30 15 anr
Molybdenum 100 50
Nickel 80 40 anr
Potassium 20000 10000 anr
Selenium 20 10 12.9 129.0 11.0 110.0
Silver 20 10 anr
Sodium 20000 10000 anr
Strontium 20 10
Thallium 20 10 anr
Tin 100 50
Titanium 20 10
Vanadium 100 50 anr
Zinc 40 20 anr
(*) Outside of QC limits
(anr) Analyte not requested
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INTERFERING ELEMENT CHECK STANDARDS SUMMARY
Part 1 - ICSA and ICSAB Standards
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID: SA061313M1.ICP Date Analyzed: 06/13/13 Methods: SW846 6010C
QC Limits: 80 to 120 % Recovery Run ID: MA10821 Units: ug/l
Time: 08:42 08:54 19:58 20:03
Sample ID: ICSA ICSAB ICSA1 ICSAB1 ICSA2 ICSAB2
Metal True True Results % Rec Results % Rec Results % Rec Results % Rec
Aluminum 500000 500000 511000 102.2 515000 103.0 496000 99.2 500000 100.0
Antimony 1000 1.8 1030 103.0 2.6 1040 104.0
Arsenic 1000 -0.50 1030 103.0 -0.20 1050 105.0
Barium 500 0.10 530 106.0 0.20 528 105.6
Beryllium 500 -0.40 506 101.2 -0.20 504 100.8
Cadmium 1000 0.0 932 93.2 0.30 951 95.1
Calcium 500000 500000 479000 95.8 477000 95.4 475000 95.0 474000 94.8
Chromium 500 -0.20 483 96.6 0.50 502 100.4
Cobalt 500 -0.90 467 93.4 -0.90 464 92.8
Copper 500 0.0 538 107.6 0.20 545 109.0
Iron 200000 200000 186000 93.0 197000 98.5 187000 93.5 198000 99.0
Lead 1000 0.10 989 98.9 2.2 981 98.1
Magnesium 500000 500000 501000 100.2 504000 100.8 492000 98.4 494000 98.8
Manganese 500 0.0 497 99.4 0.10 510 102.0
Molybdenum 1000 -0.20 909 90.9 0.10 901 90.1
Nickel 1000 0.0 923 92.3 0.30 934 93.4
Potassium -29 -5.6 91.8 85.2
Selenium 1000 0.0 991 99.1 -0.10 1020 102.0
Silver 1000 0.20 1030 103.0 0.20 1040 104.0
Sodium 95.6 151 131 192
Strontium 1000 11.9 1030 103.0 12.3 1040 104.0
Thallium 1000 0.0 986 98.6 1.5 976 97.6
Tin 1000 2.8 905 90.5 3.4 907 90.7
Titanium 1000 -3.3 963 96.3 -3.2 991 99.1
Vanadium 500 -0.10 482 96.4 0.10 493 98.6
Zinc 1000 -1.6 940 94.0 -1.2 947 94.7
(*) Outside of QC limits
(anr) Analyte not requested
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BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
QC Batch ID: MP25296 Methods: SW846 6010C
Matrix Type: SOLID Units: mg/kg
Prep Date: 06/11/13
MB
Metal RL IDL MDL raw final
Aluminum 10 .75 1
Antimony 1.0 .065 .095
Arsenic 0.50 .08 .08 -0.065 <0.50
Barium 10 .05 .25
Beryllium 0.25 .025 .025
Cadmium 0.20 .025 .025
Calcium 250 2.5 2.5
Chromium 0.50 .09 .09
Cobalt 2.5 .025 .025
Copper 1.3 .05 .09
Iron 15 1.5 3.5
Lead 1.0 .055 .055
Magnesium 250 3.7 3.8
Manganese 0.75 .035 .045
Molybdenum 2.5 .03 .03
Nickel 2.0 .025 .025
Potassium 500 10 10
Selenium 1.0 .1 .15 0.18 <1.0
Silver 0.50 .025 .025
Sodium 500 25 25
Strontium 0.50 .025 .025
Thallium 0.50 .065 .09
Tin 2.5 .035 .035
Titanium 0.50 .045 .045
Vanadium 2.5 .025 .025
Zinc 1.0 .15 .15
Associated samples MP25296: FA5208-3, FA5208-4, FA5208-5, FA5208-6, FA5208-7, FA5208-8, FA5208-9, FA5208-
10, FA5208-11, FA5208-12, FA5208-13, FA5208-14
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
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MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
QC Batch ID: MP25296 Methods: SW846 6010C
Matrix Type: SOLID Units: mg/kg
Prep Date: 06/11/13 06/11/13
FA5145-25R QC FA5145-25R Spikelot QC
Metal Original DUP RPD Limits Original MS MPFLICP1 % Rec Limits
Aluminum anr
Antimony
Arsenic 0.66 0.91 33.3 (a) 0-20 0.66 104 103 100.2 80-120
Barium
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron anr
Lead anr
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium 0.30 0.32 (b) 6.5 0-20 0.30 107 (b) 103 103.5 80-120
Silver anr
Sodium
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc
Associated samples MP25296: FA5208-3, FA5208-4, FA5208-5, FA5208-6, FA5208-7, FA5208-8, FA5208-9, FA5208-
10, FA5208-11, FA5208-12, FA5208-13, FA5208-14
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
(a) RPD acceptable due to low duplicate and sample concentrations.
(b) Elevated reporting limit(s) due to matrix interference.
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MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
QC Batch ID: MP25296 Methods: SW846 6010C
Matrix Type: SOLID Units: mg/kg
Prep Date: 06/11/13
FA5145-25R Spikelot MSD QC
Metal Original MSD MPFLICP1 % Rec RPD Limit
Aluminum anr
Antimony
Arsenic 0.66 115 112 101.9 10.0 20
Barium
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron anr
Lead anr
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium 0.30 117 (a) 112 104.0 8.9 20
Silver anr
Sodium
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc
Associated samples MP25296: FA5208-3, FA5208-4, FA5208-5, FA5208-6, FA5208-7, FA5208-8, FA5208-9, FA5208-
10, FA5208-11, FA5208-12, FA5208-13, FA5208-14
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
(a) Elevated reporting limit(s) due to matrix interference.
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SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
QC Batch ID: MP25296 Methods: SW846 6010C
Matrix Type: SOLID Units: mg/kg
Prep Date: 06/11/13
BSP Spikelot QC
Metal Result MPFLICP1 % Rec Limits
Aluminum anr
Antimony
Arsenic 100 100 100.0 80-120
Barium
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron anr
Lead anr
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium 98.1 100 98.1 80-120
Silver anr
Sodium
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc
Associated samples MP25296: FA5208-3, FA5208-4, FA5208-5, FA5208-6, FA5208-7, FA5208-8, FA5208-9, FA5208-
10, FA5208-11, FA5208-12, FA5208-13, FA5208-14
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
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SERIAL DILUTION RESULTS SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
QC Batch ID: MP25296 Methods: SW846 6010C
Matrix Type: SOLID Units: ug/l
Prep Date: 06/11/13
FA5145-25R QC
Metal Original SDL 1:5 %DIF Limits
Aluminum anr
Antimony
Arsenic 11.1 0.00 100.0(a) 0-10
Barium
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron anr
Lead anr
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium 5.00 0.00 100.0(a) 0-10
Silver anr
Sodium
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc
Associated samples MP25296: FA5208-3, FA5208-4, FA5208-5, FA5208-6, FA5208-7, FA5208-8, FA5208-9, FA5208-
10, FA5208-11, FA5208-12, FA5208-13, FA5208-14
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
_________________________________________________________________________________________________________
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POST DIGESTATE SPIKE SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
QC Batch ID: MP25296 Methods: SW846 6010C
Matrix Type: SOLID Units: ug/l
Prep Date: 06/11/13
Sample Final FA5145-25R PS Spike Spike Spike QC
Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits
Aluminum
Antimony
Arsenic 9.8 10 11.1 10.682 112.8 0.2 5 100 102.1 80-120
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 9.8 10 5 4.9 113 0.2 5 100 108.1 80-120
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP25296: FA5208-3, FA5208-4, FA5208-5, FA5208-6, FA5208-7, FA5208-8, FA5208-9, FA5208-
10, FA5208-11, FA5208-12, FA5208-13, FA5208-14
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(**) Corr. sample result = Raw * (sample volume / final volume)
(anr) Analyte not requested
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BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
QC Batch ID: MP25297 Methods: SW846 6010C
Matrix Type: SOLID Units: mg/kg
Prep Date: 06/11/13
MB
Metal RL IDL MDL raw final
Aluminum 10 .75 1
Antimony 1.0 .065 .095
Arsenic 0.50 .08 .08 -0.13 <0.50
Barium 10 .05 .25
Beryllium 0.25 .025 .025
Cadmium 0.20 .025 .025
Calcium 250 2.5 2.5
Chromium 0.50 .09 .09
Cobalt 2.5 .025 .025
Copper 1.3 .05 .09
Iron 15 1.5 3.5
Lead 1.0 .055 .055
Magnesium 250 3.7 3.8
Manganese 0.75 .035 .045
Molybdenum 2.5 .03 .03
Nickel 2.0 .025 .025
Potassium 500 10 10
Selenium 1.0 .1 .15 0.085 <1.0
Silver 0.50 .025 .025
Sodium 500 25 25
Strontium 0.50 .025 .025
Thallium 0.50 .065 .09
Tin 2.5 .035 .035
Titanium 0.50 .045 .045
Vanadium 2.5 .025 .025
Zinc 1.0 .15 .15
Associated samples MP25297: FA5208-15, FA5208-16, FA5208-17, FA5208-18, FA5208-19, FA5208-20
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
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MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
QC Batch ID: MP25297 Methods: SW846 6010C
Matrix Type: SOLID Units: mg/kg
Prep Date: 06/11/13 06/11/13
FA5208-15 QC FA5208-15 Spikelot QC
Metal Original DUP RPD Limits Original MS MPFLICP1 % Rec Limits
Aluminum
Antimony
Arsenic 1.6 2.0 22.2 (a) 0-20 1.6 71.9 98.7 71.3N(b) 80-120
Barium anr
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper anr
Iron anr
Lead anr
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium 0.0 0.0 NC 0-20 0.0 70.6 98.7 71.6N(b) 80-120
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP25297: FA5208-15, FA5208-16, FA5208-17, FA5208-18, FA5208-19, FA5208-20
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
(a) RPD acceptable due to low duplicate and sample concentrations.
(b) Spike recovery indicates possible matrix interference and/or sample non-homogeneity.
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MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
QC Batch ID: MP25297 Methods: SW846 6010C
Matrix Type: SOLID Units: mg/kg
Prep Date: 06/11/13
FA5208-15 Spikelot MSD QC
Metal Original MSD MPFLICP1 % Rec RPD Limit
Aluminum
Antimony
Arsenic 1.6 70.9 97.8 70.9N(a) 1.4 20
Barium anr
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper anr
Iron anr
Lead anr
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium 0.0 70.1 97.8 71.7N(a) 0.7 20
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP25297: FA5208-15, FA5208-16, FA5208-17, FA5208-18, FA5208-19, FA5208-20
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
(a) Spike recovery indicates possible matrix interference and/or sample non-homogeneity.
_________________________________________________________________________________________________________
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SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
QC Batch ID: MP25297 Methods: SW846 6010C
Matrix Type: SOLID Units: mg/kg
Prep Date: 06/11/13
BSP Spikelot QC
Metal Result MPFLICP1 % Rec Limits
Aluminum
Antimony
Arsenic 102 100 102.0 80-120
Barium anr
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper anr
Iron anr
Lead anr
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium 101 100 101.0 80-120
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP25297: FA5208-15, FA5208-16, FA5208-17, FA5208-18, FA5208-19, FA5208-20
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
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SERIAL DILUTION RESULTS SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
QC Batch ID: MP25297 Methods: SW846 6010C
Matrix Type: SOLID Units: ug/l
Prep Date: 06/11/13
FA5208-15 QC
Metal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic 30.0 37.7 25.7 (a) 0-10
Barium anr
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper anr
Iron anr
Lead anr
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium 0.00 0.00 NC 0-10
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP25297: FA5208-15, FA5208-16, FA5208-17, FA5208-18, FA5208-19, FA5208-20
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
_________________________________________________________________________________________________________
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POST DIGESTATE SPIKE SUMMARY
Login Number: FA5208
Account: AMECPAP - AMEC Environment & Infrastructure, Inc.
Project: GE-TFS; 1906 Bancroft St, Charlotte, NC
QC Batch ID: MP25297 Methods: SW846 6010C
Matrix Type: SOLID Units: ug/l
Prep Date: 06/11/13
Sample Final FA5208-15 PS Spike Spike Spike QC
Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits
Aluminum
Antimony
Arsenic 9.8 10 30 29.4 113 0.2 5 100 83.6 80-120
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 9.8 10 80.6 0.2 5 100 80.6 80-120
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP25297: FA5208-15, FA5208-16, FA5208-17, FA5208-18, FA5208-19, FA5208-20
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(**) Corr. sample result = Raw * (sample volume / final volume)
(anr) Analyte not requested
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Instrument Detection Limits Page 1 of 1
Job Number:FA5208
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Instrument ID:SSTRACE1 Effective Date:10/01/12
IDL
Analyte ug/l
Aluminum 15
Antimony 1.3
Arsenic 1.6
Barium 1
Beryllium .5
Cadmium .5
Calcium 50
Chromium 1.8
Cobalt .5
Copper 1
Iron 29
Lead 1.1
Magnesium 74
Manganese .7
Molybdenum .6
Nickel .5
Potassium 200
Selenium 2
Silicon 5
Silver .5
Sodium 500
Strontium .5
Thallium 1.3
Tin .7
Titanium .9
Vanadium .5
Zinc 3
The above applies to the following instrument runs:
MA10817,MA10821
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Instrument Linear Ranges Page 1 of 1
Job Number:FA5208
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Instrument ID:SSTRACE1 Effective Date:04/21/10
Linear Range
Analyte ug/l
Aluminum 500000
Antimony 10000
Arsenic 10000
Barium 10000
Beryllium 10000
Cadmium 10000
Calcium 500000
Chromium 10000
Cobalt 10000
Copper 10000
Iron 500000
Lead 10000
Magnesium 500000
Manganese 10000
Molybdenum 10000
Nickel 10000
Potassium 80000
Selenium 10000
Silver 1000
Sodium 80000
Strontium 10000
Thallium 10000
Tin 10000
Titanium 10000
Vanadium 10000
Zinc 10000
The above applies to the following instrument runs:
MA10817,MA10821
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Accutest LabLink@144523 15:22 27-Aug-2013
General Chemistry
QC Data Summaries
Includes the following where applicable:
• Percent Solids Raw Data Summary
Southeast
Section 8
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Percent Solids Raw Data Summary Page 1 of 4
Job Number:FA5208
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample:FA5208-1 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-1/0.75
Wet Weight (Total) 6.85 g
Tare Weight 1.04 g
Dry Weight (Total) 6.46 g
Solids, Percent 93.3 %
Sample:FA5208-2 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-2/0.5
Wet Weight (Total) 8.42 g
Tare Weight 1.05 g
Dry Weight (Total) 7.26 g
Solids, Percent 84.3 %
Sample:FA5208-3 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-3/1.0
Wet Weight (Total) 7.91 g
Tare Weight 1 g
Dry Weight (Total) 7.14 g
Solids, Percent 88.9 %
Sample:FA5208-4 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-3/4.0
Wet Weight (Total) 7.76 g
Tare Weight 1.01 g
Dry Weight (Total) 6.63 g
Solids, Percent 83.3 %
Sample:FA5208-5 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-3/7.5
Wet Weight (Total) 7.41 g
Tare Weight 1.03 g
Dry Weight (Total) 6.38 g
Solids, Percent 83.9 %
Sample:FA5208-6 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-4/1.0
Wet Weight (Total) 7 g
Tare Weight 1.02 g
Dry Weight (Total) 5.86 g
Solids, Percent 80.9 %
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Percent Solids Raw Data Summary Page 2 of 4
Job Number:FA5208
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample:FA5208-7 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-4/4.5
Wet Weight (Total) 6.78 g
Tare Weight 1.04 g
Dry Weight (Total) 5.77 g
Solids, Percent 82.4 %
Sample:FA5208-8 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-4/7.0
Wet Weight (Total) 8.45 g
Tare Weight 1.05 g
Dry Weight (Total) 7.49 g
Solids, Percent 87 %
Sample:FA5208-9 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-5/1.0
Wet Weight (Total) 6.88 g
Tare Weight 1 g
Dry Weight (Total) 6.1 g
Solids, Percent 86.7 %
Sample:FA5208-10 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-5/5.0
Wet Weight (Total) 7.53 g
Tare Weight 1.05 g
Dry Weight (Total) 6.47 g
Solids, Percent 83.6 %
Sample:FA5208-11 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-5/9.5
Wet Weight (Total) 6.25 g
Tare Weight 1.03 g
Dry Weight (Total) 5.67 g
Solids, Percent 88.9 %
Sample:FA5208-12 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-6/0.5
Wet Weight (Total) 6.9 g
Tare Weight .98 g
Dry Weight (Total) 6.33 g
Solids, Percent 90.4 %
114 of 116
FA5208
8
8
.
1
Percent Solids Raw Data Summary Page 3 of 4
Job Number:FA5208
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample:FA5208-13 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-6/5.5
Wet Weight (Total) 7.67 g
Tare Weight 1.05 g
Dry Weight (Total) 6.97 g
Solids, Percent 89.4 %
Sample:FA5208-14 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-6/11.5
Wet Weight (Total) 7.45 g
Tare Weight 1.05 g
Dry Weight (Total) 6.05 g
Solids, Percent 78.1 %
Sample:FA5208-15 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-7/1.0
Wet Weight (Total) 6.59 g
Tare Weight 1.01 g
Dry Weight (Total) 6.06 g
Solids, Percent 90.5 %
Sample:FA5208-16 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-7/6.5
Wet Weight (Total) 6.32 g
Tare Weight 1.03 g
Dry Weight (Total) 5.27 g
Solids, Percent 80.2 %
Sample:FA5208-17 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-7/13
Wet Weight (Total) 6.57 g
Tare Weight 1.05 g
Dry Weight (Total) 5.78 g
Solids, Percent 85.7 %
Sample:FA5208-18 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-8/1.0
Wet Weight (Total) 7.06 g
Tare Weight 1.04 g
Dry Weight (Total) 5.05 g
Solids, Percent 66.6 %
115 of 116
FA5208
8
8
.
1
Percent Solids Raw Data Summary Page 4 of 4
Job Number:FA5208
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Sample:FA5208-19 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-8/5.0
Wet Weight (Total) 7.6 g
Tare Weight .99 g
Dry Weight (Total) 5.87 g
Solids, Percent 73.8 %
Sample:FA5208-20 Analyzed:07-JUN-13 by LE Method:SM19 2540G
ClientID:RR-8/10.0
Wet Weight (Total) 6.43 g
Tare Weight 1.02 g
Dry Weight (Total) 5.11 g
Solids, Percent 75.6 %
116 of 116
FA5208
8
8
.
1
Former GE Trailer Fleet Services Charlotte Facility
August 22, 2013

ATTACHMENT D

AMEC Environmental & Infrastructure, Inc.
502 West Germantown Pike, Suite 850
Plymouth Meeting, PA 19462
610.828.8100 / fax: [phone] www.amec.com
August 22, 2013

Dr. James Van Nortwick
GE Corporate Environmental Programs
500 West Monroe Street- 10th Floor
Chicago, Illinois 60661

Re: Vapor Intrusion Assessment Report
GE Trailer Fleet Services
1906 Bancroft Street in Charlotte, North Carolina
AMEC Project: 572260702

Dear Dr. Van Nortwick:

AMEC Environment & Infrastructure, Inc. (AMEC) is pleased to report the findings of the sub-
slab soil vapor sampling performed at 1906 Bancroft Street in Charlotte, North Carolina (Site).
The purpose of this sampling was to determine if gases volatilizing from potentially impacted
shallow groundwater may be adversely impacting indoor air quality in the on-site structures.
This investigation was completed in accordance to the North Carolina Department of
Environment and Natural Resources (NCDENR), Division of Waste Management (DWM)
Inactive Hazardous Sites Branch (IHSB) guidance. The investigation concluded that the sub-
slab vapor survey did not identify adverse risk to Site occupants in a slab-on-grade structure
based on the IHSB Industrial/Commercial (i.e., non-residential) Site use.

Should you have any questions regarding this assessment report, please contact Stephen Cline
at [phone].

Respectfully Submitted,

AMEC Environment & Infrastructure, Inc.

Steven Tanen Stephen P. Cline
Senior Project Geologist Associate Geologist

Attachment

TABLE OF CONTENTS

1.0 INTRODUCTION ............................................................................................................ 1 
1.1 Background ................................................................................................................. 1 
2.0 SAMPLING ACTIVITIES ............................................................................................... 2 
3.0 ANALYTICAL RESULTS .............................................................................................. 4 
3.1 Sub-slab Air Sampling Results .................................................................................... 4 
3.2 Risk Calculations ......................................................................................................... 4 
4.0 SUMMATION ................................................................................................................. 5 

FIGURES

Figure 1 Site Location Map
Figure 2 Site Layout
Figure 3 Groundwater Sampling Exceedences – 6/16/11
Figure 4 Sub-slab Sample Locations
Figure 5 Sub-slab Vapor Data

TABLES

Table 1 Groundwater Analytical Results – Detected VOCs
Table 2 Sub-slab Sample Information – Volatile Organic Compounds
Table 3 Sub-slab Sample Results – Volatile Organic Compounds

APPENDICES

Appendix A Photo Log - August 2012 Vapor Intrusion Sampling Event
Appendix B Laboratory Analytical Data Report
Appendix C Risk Calculations

Results of Sub-slab Vapor Sampling
TFS Charlotte Branch
1906 Bancroft Street, Charlotte, North Carolina

-1-

1.0 INTRODUCTION
AMEC Environment & Infrastructure, Inc. (AMEC) was retained by Transport International Pool,
Inc. (TFS) to conduct an indoor vapor assessment for the property located at 1906 Bancroft
Street in Charlotte, North Carolina (Figure 1) (the “Site”). This TFS property consists of
approximately 7.93 acres and is improved with a 3,750 square foot slab-on-grade shop building.
1.1 Background
TFS owns but no longer occupies the Site, which is currently vacant. TFS used the Site from
1986 to 2011 as a branch location for the leasing, parking, storage, and minor repair of over-
the-road trailers. Prior to 1986 the property was undeveloped woodland. The general layout of
the Site while it was operational is shown on Figure 2.
The Site is located in an area with mixed industrial and commercial use, with several industrial
and commercial establishments located within a half mile both north and west of the Site.
Residential properties are located southwest of the property. A number of the upgradient
industrial/commercial properties have a history of solvent use and confirmed impacts to soil and
groundwater. based on a search of environmental databases and review of readily available
reports.
Phase II investigations completed at the Site by AMEC for TFS did not detect any volatile
organic compounds (VOCs) in soil other than acetone and methyl ethyl ketone (MEK). Both
compounds were detected at estimated concentrations and below NCDENR Soil Remediation
Goals. Neither acetone nor MEK were detected in groundwater and both were identified as
likely laboratory and/or sample preservations artifacts and, therefore, judged not to be
representative of actual Site conditions. However, the same investigations revealed impacts to
Site groundwater in the southern portion of the parcel at both the upgradient and downgradient
Site boundaries from chloroform, carbon tetrachloride, 1,1-dichloroethane (1,1-DCA), 1,1-
dichloroethene (1,1-DCE), cis-1,2-Dichloroethene (cis-1,2-DCE), trans-1,2-dichloroethene
(trans-1,2-DCE), tetrachloroethene (PCE) and trichloroethene (TCE). The compounds carbon
tetrachloride, 1,1-DCE, PCE and TCE were detected at concentrations above the North
Carolina Department of Environment and Natural Resources (NCDENR) 2L Groundwater
Quality Standards. Results from groundwater testing are provided in Table 1 and groundwater
sampling locations are shown on Figure 3. These results appear to be due to releases from an
upgradient source, which has had documented use and confirmed releases of such solvents.
Due to identified groundwater impacts at the Site within 100 feet of the on-site shop building,
TFS authorized collection of sub-slab soil vapor samples from beneath that building to
determine if gases volatizing from impacted shallow groundwater may be impacting indoor air
quality.
The following sections summarize the activities completed with regard to the vapor sampling
and the results obtained from those activities.
Results of Sub-slab Vapor Sampling
TFS Charlotte Branch
1906 Bancroft Street, Charlotte, North Carolina

-2-

2.0 SAMPLING ACTIVITIES
The Site consists of a slab on grade shop building (”shop”) (Figure 2), which covers
approximately 3,750 square feet. Prior to any sub-slab sampling, North Carolina One-Call was
notified in accordance with State requirements and utilities marked (ticket confirmation number:
A122231658).
Four sub-slab vapor samples (SS-1 through SS-4) were collected inside of the shop, along with
one duplicate sample (SS-5) for sample SS-1.
The building was gridded into four sections with one sample collected from each section.
Sample locations are shown on Figure 2. All sub-slab vapor samples were collected from
immediately beneath the concrete slab inside the building (Figure 4). A small hole was bored
through the concrete floor and then inert 0.170 x 0.25-inch polyethylene tubing equipped with a
sterile stainless steel screen covering its orifice was installed in the borehole within two inches
of the bottom of the slab. Sand-sized glass beads were used as backfill material to fill the
sampling area to a depth such that the bottom one inch of the tubing was covered. The
remaining space within the hole was filled with volatile organic carbon (VOC)-free bentonite
pellets, which were then hydrated to seal the tubing in place and to isolate the sample point
from ambient air conditions within the shop. The remaining annulus was filled with grout to the
top of the floor slab.
Once the grout had set, the tubing was purged to remove air introduced to the sub-slab airspace
during concrete boring and tubing installation, as well as the ambient air within the tubing. One
liter of air was purged using a peristaltic pump prior to sampling. In order to minimize ambient
air intrusion, air flow was maintained at a rate below 200 milliliters per minute during purging.
After purging, the tubing was immediately connected to a batch certified 1-liter summa canister
for air collection. The sample was collected with a flow controller that regulated air flow to fill the
summa canister at a constant rate over a 30 minute period. The summa canister identification
number, sampler identification number, pump start and end time, and the starting and ending
summa canister vacuums were recorded (Table 2).
For one sample (SS-1), helium was employed as a tracer gas to provide a means of assessing
whether air from above the slab was able to pass through the bentonite seal during sampling.
To achieve this, a plastic bag filled with helium was placed over the tubing and borehole
throughout the sampling period. Photographs of the sampling activities are provided in
Appendix A.
The samples were transported under strict chain-of-custody protocol to Air Toxics, Ltd., of
Folsom, California, for analysis of United States Environmental Protection Agency (USEPA)
Method TO-15 constituents (carbon tetrachloride, chloroethane, chloroform, chloromethane,
1,1-DCA, 1,1-DCE, cis-1,2-DCE, trans-1,2-DCE, ethanol, methylene chloride, PCE, TCE, 1,1,1-
trichloroethane and vinyl chloride). Following sample collection, the slab was repaired with
cement grout.
Results of Sub-slab Vapor Sampling
TFS Charlotte Branch
1906 Bancroft Street, Charlotte, North Carolina

-3-

The sampling event was conducted in accordance with the NCDENR procedures presented in
the document Supplemental Guidelines for the Evaluation of Structural Vapor Intrusion Potential
for Site Assessments and Remedial Actions Under the Inactive Hazardous Sites Branch, dated
June 21, 2011.

Results of Sub-slab Vapor Sampling
TFS Charlotte Branch
1906 Bancroft Street, Charlotte, North Carolina

-4-

3.0 ANALYTICAL RESULTS
3.1 Sub-slab Air Sampling Results
Analytical results were reported in micrograms per cubic meter (µg/m3) and have been
compared to the NCDENR Division of Waste Management (DWM) Inactive Hazardous Sites
Branch (IHSB) Industrial/Commercial soil gas screening levels. PCE was present in each sub-
slab sample at concentrations below the PCE IHSB soil gas industrial/commercial screening
level (350 µg/m3). Reported concentrations for PCE ranged from 18 to 230 µg/m3 with the
highest concentration detected in sample SS-2. Sample SS-2 was located in the western
quadrant of the Site building. No other constituents were detected. Sub-slab sampling results
are presented in Table 3 and are summarized on Figure 5.
Sample SS-5 was collected as a duplicate of SS-1 to assess the overall precision and
reproducibility of data as it pertains to both field collection methods and laboratory analysis.
These samples exhibited PCE concentrations of 62 µg/m3 (SS-1) and 64 µg/m3 (SS-5),
respectively. The calculated relative percent difference (RPD) between the two samples is 3.1-
percent. An RPD of less than 10-percent indicates a good correlation between the two samples
and these results are within an acceptable range of accuracy. The laboratory analytical report
and chain-of-custody documentation are included in Appendix B.
3.2 Risk Calculations
As stated above, PCE was present at concentrations below its respective soil gas
industrial/commercial screening level, 350 µg/m3. This screening level is based on a
carcinogenic target risk of 1 x 10-5 and a hazard index (HI) of 0.2. These values include a safety
factor to account for the synergistic effect of an additional four VOCs.
For additional comparison, AMEC calculated the cumulative risk associated with each of the
samples based on PCE only (i.e., the only compound detected). The concentrations were
compared to USEPA Regional Screening Levels (RSL) for Industrial Air (April 2012). The RSLs
are based on Carcinogenic Target Risk of 10-6 and non-cancer HI of 1. The risk based
calculations are provided in Appendix C and summarized below.
When evaluating soil gas and sub-slab sampling results at commercial/industrial sites, a 90 fold
attenuation factor is applied to account for the concrete slab material which impedes the upward
movement of the vapors1. This 100 fold attenuation factor was applied so the results could be
compared to indoor air vapor standards. These calculation tables are provided in Appendix C.
The risk calculations for PCE indicate that, at the highest concentration observed (230 µg/m3
PCE in sample SS-2), the cumulative risk value, when the 100 fold attenuation factor is applied,
is less than 10-8 with a hazard index of 0.01.

1 USEPA Vapor Intrusion Guidance, December 13, 2012
Results of Sub-slab Vapor Sampling
TFS Charlotte Branch
1906 Bancroft Street, Charlotte, North Carolina

-5-

4.0 SUMMATION
Sub-slab samples were collected at four locations beneath the at-grade floor slab in the shop.
The samples were collected to evaluate the potential for vapor intrusion from groundwater into
the building. The VOCs detected in groundwater at the Site were not detected in Site soils.
Acetone and MEK were detected in Site soils at estimated concentrations and were judged to
be likely laboratory and/or sample preservation artifacts.
The results showed that each sub-slab vapor sample exhibited PCE at a concentration below its
IHSB soil gas industrial/commercial screening level, but above its method detection limit. No
other VOCs were detected in the samples collected.
The sub-slab results were also compared to USEPA RSLs for Industrial Air. The RSLs are
based on a Carcinogenic Target Risk of 10-6 and non-cancer HI of 1. When considering a 100
fold attenuation factor to account for the concrete slab, in order to compare the Site results to
indoor air vapor standards, the Carcinogenic Target Risk is 10-8 and the HI is 0.01.
Based on the sub-slab vapor sampling results from this investigation, additional air sampling
within the shop building is not warranted as the observed concentrations pose no adverse risk
to building occupants. The sub-slab vapor survey did not identify adverse risk to Site occupants
in a slab-on-grade structure based on the IHSB Industrial/Commercial (i.e., non-residential) Site
use.

Results of Sub-slab Vapor Sampling
TFS Charlotte Branch
1906 Bancroft Street, Charlotte, North Carolina

FIGURES

TFS Charlotte Branch Location
Vapor Intrusion Assessment
1906 Bancroft Street
Charlotte, North Carolina
TFS Charlotte Branch Location
Vapor Intrusion Assessment
1906 Bancroft Street
Charlotte, North Carolina

Figure 2
Site Layout

Environment & Infrastructure, Inc.
502 West Germantown Pike, Suite 850
Plymouth Meeting PA 19462

Modular 
Office
Shop 
Building 
Aerial of Site while Site 
operational (i.e., pre‐2012) 

Site at time of Vapor 
Intrusion Survey was 
vacant. 
TFS Charlotte Branch Location
Vapor Intrusion Assessment
1906 Bancroft Street
Charlotte, North Carolina

Figure 3
Groundwater Exceedences 6/16/11

Environment & Infrastructure, Inc.
502 West Germantown Pike, Suite 850
Plymouth Meeting PA 19462
0 50 100
Approximate Scale in Feet

ref:  www.maps.google.com 
       Monitoring well 

µg/L   micrograms per Liter 

NE   No Exceedances 
MW‐5 
NE 
MW‐8
NE
MW‐3
NE 
MW‐4 
NE 
MW‐1 
ug/L Conc Criteria 
11DCE 11.2 7 
PCE 111 0.7 
TCE 143 3 
MW‐2 
ug/L Conc Criteria 
Carbon Tet 1.8 0.3 
MW‐6 
ug/L Conc Criteria 
TCE 17.7 3 
MW‐7 
ug/L Conc Criteria 
11DCE 16.5 7 
PCE 103 0.7 
TCE 90.1 3 
MW‐9 
ug/L Conc Criteria 
PCE 5.6 0.7 
TCE 2.9 3 
TFS Charlotte Branch Location
Vapor Intrusion Assessment
1906 Bancroft Street
Charlotte, North Carolina

Figure 4
Sub-slab Sample Locations

Environment & Infrastructure, Inc.
502 West Germantown Pike, Suite 850
Plymouth Meeting PA 19462

Sub‐slab Sample Location

Mecklenburg County Parcel
Aerial of Site while Site 
operational (i.e., pre‐2012) 

Site at time of Vapor 
Intrusion Survey was 
vacant. 
TFS Charlotte Branch Location
Vapor Intrusion Assessment
1906 Bancroft Street
Charlotte, North Carolina

Figure 5
Sub-Slab Vapor Data

Environment & Infrastructure, Inc.
502 West Germantown Pike, Suite 850
Plymouth Meeting PA 19462

Legend 
       Sub‐Slab Sampling Location 
PCE:  Tetrachloroethene 
Units:  micrograms per cubic meter (µg/m3) 
350 µg/m3:  PCE IHSB (Industrial) Acceptable Soil Gas Concentration 
PCE 62
PCE 18 PCE 230
PCE 18
Aerial of Site while Site 
operational (i.e., pre‐2012) 

Site at time of Vapor 
Intrusion Survey was 
vacant. 
Results of Sub-slab Vapor Sampling
TFS Charlotte Branch
1906 Bancroft Street, Charlotte, North Carolina

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n
m
e
n
t

a
n
d

N
a
t
u
r
a
l

R
e
s
o
u
r
c
e
s
Sh
a
d
e
d

c
e
l
l

i
n
d
i
c
a
t
e
s

c
o
m
p
o
u
n
d

d
e
t
e
c
t
e
d

a
t

o
r

a
b
o
v
e

t
h
e

N
C
D
E
N
R

2
L

S
t
a
n
d
a
r
d
NC

2
L

G
W
S
:

N
o
r
t
h

C
a
r
o
l
i
n
a

D
e
p
a
r
t
m
e
n
t

o
f

E
n
v
i
r
o
n
m
e
n
t

a
n
d

N
a
t
u
r
a
l

R
e
s
o
u
r
c
e
s

G
r
o
u
n
d
w
a
t
e
r

S
t
a
n
d
a
r
d

(
J
a
n
u
a
r
y

2
0
1
0
)
µg
/
L
:

m
i
c
r
o
g
r
a
m
s

p
e
r

L
i
t
e
r
U:

c
o
m
p
o
u
n
d

n
o
t

d
e
t
e
c
t
e
d

a
t

o
r

a
b
o
v
e

t
h
e

p
o
s
t
e
d

l
a
b
o
r
a
t
o
r
y

r
e
p
o
r
t
i
n
g

l
i
m
i
t
J:

i
n
d
i
c
a
t
e
s

e
s
t
i
m
a
t
e
d

c
o
n
c
e
n
t
r
a
t
i
o
n

(
c
o
m
p
o
u
n
d

d
e
t
e
c
t
e
d

h
o
w
e
v
e
r

a
t

a

c
o
n
c
e
n
t
r
a
t
i
o
n

b
e
l
o
w

t
h
e

l
a
b
o
r
a
t
o
r
y

P
Q
L

b
u
t

a
b
o
v
e

t
h
e

M
D
L
)
-

i
n
d
i
c
a
t
e
s

c
o
m
p
o
u
n
d

n
o
t

a
n
a
l
y
z
e
d

f
o
r
MW-6
MW
-
1
MW
-
2

M
W
-
3

M
W
-
4

M
W
-
5
F8
2
0
0
4
-
1

F
8
3
5
0
8
-
1

F
8
2
0
0
4
-
2

F
8
3
5
2
0
-
9
MW-7

M
W
-
8

M
W
-
9
F8
2
0
3
8
-
1

F
8
3
5
2
0
-
3

F
8
2
0
3
8
-
2

F
8
3
5
2
0
-
4

F
8
2
0
3
8
-
3

F
8
3
5
2
0
-
2

F
8
3
5
2
0
-
5
5/
2
/
2
0
1
1

6
/
1
7
/
2
0
1
1

5
/
2
/
2
0
1
1

6
/
1
6
/
2
0
1
1

5
/
3
/
2
0
1
1

6
/
1
6
/
2
0
1
1
F83520-6

F
8
3
5
2
0
-
7

F
8
3
5
2
0
-
8
6/16/2011
5/
3
/
2
0
1
1

6
/
1
6
/
2
0
1
1

5
/
3
/
2
0
1
1

6
/
1
6
/
2
0
1
1

6
/
1
6
/
2
0
1
1

6
/
1
6
/
2
0
1
1

6
/
1
6
/
2
0
1
1
Table 2
Sub-slab Sample Information - Volatile Organic Compounds
TFS - Charlotte Branch
1906 Bancroft Street, Charlotte, North Carolina
August 2012
Date Canister
Serial #Certification
Flow
Controller
Serial #
Start Time End Time
Start
Vacuum
(inches Hg)
End
Vacuum
(inches Hg)
8/15/2012 22968 Batch 40825 1048 1146 -28.5 -3.5
8/15/2012 37684 Batch FC00408 1158 1252 -29.5 -4
8/15/2012 37325 Batch FC00563 1132 1217 -29 -3.5
8/15/2012 37398 Batch FC00680 1149 1250 -30 -3.5
8/15/2012 37390 Batch FC00211 1151 1310 -26.5 -0.5
Sample Date Time
Wind Speed
(mph)
1052 5.8
1152 3.5
1252 5.8
1352 3.5
Notes:
* = Duplicate sample of SS-1
Weather Condition Details
Air Sample Details
Sample
SS-1
SS-2
SS-3
SS-4
SS-5*
8/15/2012
Temperature
ºF
79
81
82
82
Humidity
(%)
29.94
29.94
29.94
29.94
Pressure
(inches Hg)
77
72
69
67
Ta
b
l
e

3
Su
b
-
S
l
a
b

S
a
m
p
l
e

R
e
s
u
l
t
s

–

V
o
l
a
t
i
l
e

O
r
g
a
n
i
c

C
o
m
p
o
u
n
d
s
TF
S

-

C
h
a
r
l
o
t
t
e

B
r
a
n
c
h
19
0
6

B
a
n
c
r
o
f
t

S
t
r
e
e
t
,

C
h
a
r
l
o
t
t
e
,

N
o
r
t
h

C
a
r
o
l
i
n
a
Au
g
u
s
t

2
0
1
2
Sa
m
p
l
e

I
D

S
a
m
p
l
e

D
a
t
e
C
a
r
b
o
n

T
e
t
r
a
c
h
l
o
r
i
d
e
C
h
l
o
r
o
e
t
h
a
n
e
C
h
l
o
r
o
f
o
r
m
C
h
l
o
r
o
m
e
t
h
a
n
e
1
,
1
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e
1
,
1
-
D
i
c
h
l
o
r
o
e
t
h
e
n
e
c
i
s
-
1
,
2
-
D
i
c
h
l
o
r
o
e
t
h
e
n
e
t
r
a
n
s
-
1
,
2
-
D
i
c
h
l
o
r
o
e
t
h
e
n
e
E
t
h
a
n
o
l
M
e
t
h
y
l
e
n
e

C
h
l
o
r
i
d
e
T
e
t
r
a
c
h
l
o
r
o
e
t
h
e
n
e
T
r
i
c
h
l
o
r
o
e
t
h
e
n
e
1
,
1
,
1
-
T
r
i
c
h
l
o
r
o
e
t
h
a
n
e
V
i
n
y
l

C
h
l
o
r
i
d
e
Helium**
20
0

N
A

5
3

7
8
0

7
7
0

1
,
7
6
0
.
0

N
A

5
2
0

N
A

5
,
3
0
0

3
5
0

1
8

4
4
,
0
0
0

2
8
0

N
A
ASTM D-1946 (µg/L)
SS
-
1

8
/
1
5
/
2
0
1
2

<
4
.
7

<
7
.
9

<
3
.
6

<
1
5

<
3
.
0

<
3
.
0

<
3
.
0

<
3
.
0

<
5
.
6

<
2
6

6
2

<
4
.
0

<
4
.
1

<
1
.
9

<
1
6
3
.
6
SS
-
2

8
/
1
5
/
2
0
1
2

<
4
.
8

<
8
.
0

<
3
.
7

<
1
6

<
3
.
1

<
3
.
0

<
3
.
0

<
3
.
0

<
5
.
7

<
2
6

2
3
0

<
4
.
1

<
4
.
1

<
1
.
9

N
R
SS
-
3

8
/
1
5
/
2
0
1
2

<
5
.
0

<
8
.
3

<
3
.
8

<
1
6

<
3
.
2

<
3
.
1

<
3
.
1

<
3
.
1

<
6
.
0

<
2
7

1
8

<
4
.
2

<
4
.
3

<
2
.
0

N
R
SS
-
4

8
/
1
5
/
2
0
1
2

<
4
.
9

<
8
.
2

<
3
.
8

<
1
6

<
3
.
1

<
3
.
1

<
3
.
1

<
3
.
1

<
5
.
8

<
2
7

1
8

<
4
.
2

<
4
.
2

<
2
.
0

N
R
SS
-
5

(
S
S
-
1

D
u
p
)
*

8
/
1
5
/
2
0
1
2

<
4
.
5

<
7
.
6

<
3
.
5

<
1
5

<
2
.
9

<
2
.
8

<
2
.
8

<
2
.
8

<
5
.
4

<
2
5

6
4

<
3
.
9

<
3
.
9

<
1
.
8

N
R
No
t
e
s
µg
/
m
3 =

m
i
c
r
o
g
r
a
m
s

p
e
r

c
u
b
i
c

m
e
t
e
r
IH
S
B

=

I
n
a
c
t
i
v
e

H
a
z
a
r
d
o
u
s

S
i
t
e
s

B
r
a
n
c
h

(
J
u
l
y

2
0
1
2
)
NE

=

N
o
t

e
s
t
a
b
l
i
s
h
e
d
NR

=

N
o
t

r
e
p
o
r
t
e
d
*
=

D
u
p
l
i
c
a
t
e

s
a
m
p
l
e

o
f

S
S
-
1
**

=

S
a
m
p
l
e

r
e
s
u
l
t
s

w
i
t
h

a

c
o
n
c
e
n
t
r
a
t
i
o
n

o
f

u
p

t
o

2
0
0

µ
g
/
l

a
r
e

c
o
n
s
i
d
e
r
e
d

u
s
a
b
l
e

a
c
c
o
r
d
i
n
g

t
o

I
H
S
B

G
u
i
d
a
n
c
e
IH
S
B

A
c
c
e
p
t
a
b
l
e

S
o
i
l

G
a
s

Co
n
c
e
n
t
r
a
t
i
o
n

-

In
d
u
s
t
r
i
a
l
/
C
o
m
m
e
r
c
i
a
l
VO
C

T
O
-
1
5

(
µ
g
/
m
3
)
Su
b
-
S
l
a
b

S
a
m
p
l
e
s
Results of Sub-slab Vapor Sampling
TFS Charlotte Branch
1906 Bancroft Street, Charlotte, North Carolina

APPENDIX A

Photo 1
Sub-slab samples SS-2 (top)
and SS-3 (bottom). View is
facing northwest.
Photo 2
Sub-slab samples SS-3 (top)
and SS-2 (bottom). View is
facing southeast.
PHOTOGRAPH LOG
4021 Stirrup Creek Drive, Suite 100Durham, NC 27703
PROCESSED Anthony Kellogg
DATE 9/5/2012
PAGE
PHOTOGRAPH LOG
August 2012 Vapor Intrusion Sampling Event
TFS Charlotte Branch
1906 Bancroft Street, Charlotte, NC1
Photo 3
Sub-slab samples SS-1/SS-5
(top) and SS-2 (bottom).
View is facing north.
Photo 4
Sub-slab samples SS-1/SS-
5 (bottom) and SS-4 (top).
View is facing southeast.
PHOTOGRAPH LOG
4021 Stirrup Creek Drive, Suite 100Durham, NC 27703
PROCESSED Anthony Kellogg
DATE 9/5/2012
PAGE
PHOTOGRAPH LOG
August 2012 Vapor Intrusion Sampling Event
TFS Charlotte Branch
1906 Bancroft Street, Charlotte, NC2
Photo 5
A view of a patched boring pg
location. Each boring was
patched to surface with
grout.
PHOTOGRAPH LOG
4021 Stirrup Creek Drive, Suite 100Durham, NC 27703
PROCESSED Anthony Kellogg
DATE 9/5/2012
PAGE
PHOTOGRAPH LOG
August 2012 Vapor Intrusion Sampling Event
TFS Charlotte Branch
1906 Bancroft Street, Charlotte, NC3
Results of Sub-slab Vapor Sampling
TFS Charlotte Branch
1906 Bancroft Street, Charlotte, North Carolina

APPENDIX B

9/2/2012
Mr. Anthony Kellogg
AMEC Environment & Infrastructure
4021 Stirrup Creek Drive
Suite 100
Durham NC 27703
Project Name: GE-CHARLOTTE
Project #: GE-CHARLOTTE
Dear Mr. Anthony Kellogg
The following report includes the data for the above referenced project for sample(s)
received on 8/17/2012 at Air Toxics Ltd.
The data and associated QC analyzed by Modified TO-15 are compliant with the
project requirements or laboratory criteria with the exception of the deviations noted in
the attached case narrative.
Thank you for choosing Air Toxics Ltd. for your air analysis needs. Air Toxics Ltd. is
committed to providing accurate data of the highest quality. Please feel free to contact
the Project Manager: Ausha Scott at 916-985-1000 if you have any questions regarding
the data in this report.
Regards,
Ausha Scott
Project Manager
Workorder #: 1208404A
Page 1 of 17
Mr. Anthony Kellogg
AMEC Environment & Infrastructure
4021 Stirrup Creek Drive
Suite 100
Durham, NC 27703
WORK ORDER #:1208404A
CLIENT:BILL TO:
PHONE:
Accounts Payable-Durham
AMEC Environment & Infrastructure
4021 Stirrup Creek Drive
Suite 100
Durham, NC 27703
919-381-9900
08/17/2012
DATE COMPLETED:09/02/2012
P.O. #C012500874
PROJECT #GE-CHARLOTTE GE-CHARLOTTE
Work Order Summary
FAX:
DATE RECEIVED:CONTACT:Ausha Scott
NAMEFRACTION #TEST VAC./PRES.
RECEIPT
PRESSURE
FINAL
01A SS-1 Modified TO-15 3.0 "Hg 5 psi
02A SS-2 Modified TO-15 3.5 "Hg 5 psi
03A SS-3 Modified TO-15 4.5 "Hg 5 psi
04A SS-4 Modified TO-15 4.0 "Hg 5 psi
05A SS-5 Modified TO-15 2.0 "Hg 5 psi
06A Lab Blank Modified TO-15 NA NA
06B Lab Blank Modified TO-15 NA NA
07A CCV Modified TO-15 NA NA
07B CCV Modified TO-15 NA NA
08A LCS Modified TO-15 NA NA
08AA LCSD Modified TO-15 NA NA
08B LCS Modified TO-15 NA NA
08BB LCSD Modified TO-15 NA NA
CERTIFIED BY:
Technical Director
DATE:
Name of Accrediting Agency: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program)
Accreditation number: CA300005, Effective date: 10/18/2011, Expiration date: 10/17/2012.
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 9563
[phone] . [phone] . FAX [phone]
09/02/12
Page 2 of 17
This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc.
Eurofins Air Toxics Ltd. certifies that the test results contained in this report meet all requirements of the NELAC standards
Certfication numbers: AZ Licensure AZ0775, CA NELAP - 12282CA, NY NELAP - 11291,
TX NELAP - T104704434-12-5, UT NELAP CA009332012-3, WA NELAP - C935
LABORATORY NARRATIVEEPA Method TO-15AMEC Environment & InfrastructureWorkorder# 1208404A
Five 1 Liter Summa Canister samples were received on August 17, 2012. The laboratory performed
analysis via EPA Method TO-15 using GC/MS in the full scan mode.
This workorder was independently validated prior to submittal using 'USEPA National Functional
Guidelines' as generally applied to the analysis of volatile organic compounds in air. A rules-based, logic
driven, independent validation engine was employed to assess completeness, evaluate pass/fail of relevant
project quality control requirements and verification of all quantified amounts.
There were no receiving discrepancies.
Receiving Notes
All Quality Control Limit exceedances and affected sample results are noted by flags. Each flag is defined
at the bottom of this Case Narrative and on each Sample Result Summary page.
Analytical Notes
Eight qualifiers may have been used on the data analysis sheets and indicates as follows:
B - Compound present in laboratory blank greater than reporting limit (background subtraction not
performed).
J - Estimated value.
E - Exceeds instrument calibration range.
S - Saturated peak.
Q - Exceeds quality control limits.
U - Compound analyzed for but not detected above the reporting limit.
UJ- Non-detected compound associated with low bias in the CCV and/or LCS.
N - The identification is based on presumptive evidence.
File extensions may have been used on the data analysis sheets and indicates
as follows:
a-File was requantified
b-File was quantified by a second column and detector
r1-File was requantified for the purpose of reissue
Definition of Data Qualifying Flags
Page 3 of 17
EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: SS-1
Lab ID#: 1208404A-01A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.74 9.1 5.0 62Tetrachloroethene
Client Sample ID: SS-2
Lab ID#: 1208404A-02A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.76 34 5.2 230Tetrachloroethene
Client Sample ID: SS-3
Lab ID#: 1208404A-03A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.79 2.7 5.4 18Tetrachloroethene
Client Sample ID: SS-4
Lab ID#: 1208404A-04A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.78 2.7 5.2 18Tetrachloroethene
Client Sample ID: SS-5
Lab ID#: 1208404A-05A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.72 9.4 4.9 64Tetrachloroethene
Page 4 of 17
Client Sample ID: SS-1
Lab ID#: 1208404A-01A
EPA METHOD TO-15 GC/MS FULL SCAN
2082331File Name:
Dil. Factor:1.49
Date of Collection: 8/15/12 11:46:00 AM
Date of Analysis: 8/24/12 01:36 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
7.4 Not Detected 15 Not DetectedChloromethane
0.74 Not Detected 1.9 Not DetectedVinyl Chloride
3.0 Not Detected 7.9 Not DetectedChloroethane
3.0 Not Detected 5.6 Not DetectedEthanol
0.74 Not Detected 3.0 Not Detected1,1-Dichloroethene
7.4 Not Detected 26 Not DetectedMethylene Chloride
0.74 Not Detected 3.0 Not Detectedtrans-1,2-Dichloroethene
0.74 Not Detected 3.0 Not Detected1,1-Dichloroethane
0.74 Not Detected 3.0 Not Detectedcis-1,2-Dichloroethene
0.74 Not Detected 3.6 Not DetectedChloroform
0.74 Not Detected 4.1 Not Detected1,1,1-Trichloroethane
0.74 Not Detected 4.7 Not DetectedCarbon Tetrachloride
0.74 Not Detected 4.0 Not DetectedTrichloroethene
0.74 9.1 5.0 62Tetrachloroethene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
100 70-130Toluene-d8
103 70-1301,2-Dichloroethane-d4
105 70-1304-Bromofluorobenzene
Page 5 of 17
Client Sample ID: SS-2
Lab ID#: 1208404A-02A
EPA METHOD TO-15 GC/MS FULL SCAN
2082332File Name:
Dil. Factor:1.52
Date of Collection: 8/15/12 12:52:00 PM
Date of Analysis: 8/24/12 02:25 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
7.6 Not Detected 16 Not DetectedChloromethane
0.76 Not Detected 1.9 Not DetectedVinyl Chloride
3.0 Not Detected 8.0 Not DetectedChloroethane
3.0 Not Detected 5.7 Not DetectedEthanol
0.76 Not Detected 3.0 Not Detected1,1-Dichloroethene
7.6 Not Detected 26 Not DetectedMethylene Chloride
0.76 Not Detected 3.0 Not Detectedtrans-1,2-Dichloroethene
0.76 Not Detected 3.1 Not Detected1,1-Dichloroethane
0.76 Not Detected 3.0 Not Detectedcis-1,2-Dichloroethene
0.76 Not Detected 3.7 Not DetectedChloroform
0.76 Not Detected 4.1 Not Detected1,1,1-Trichloroethane
0.76 Not Detected 4.8 Not DetectedCarbon Tetrachloride
0.76 Not Detected 4.1 Not DetectedTrichloroethene
0.76 34 5.2 230Tetrachloroethene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
101 70-130Toluene-d8
104 70-1301,2-Dichloroethane-d4
100 70-1304-Bromofluorobenzene
Page 6 of 17
Client Sample ID: SS-3
Lab ID#: 1208404A-03A
EPA METHOD TO-15 GC/MS FULL SCAN
2082333File Name:
Dil. Factor:1.58
Date of Collection: 8/15/12 12:17:00 PM
Date of Analysis: 8/24/12 03:11 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
7.9 Not Detected 16 Not DetectedChloromethane
0.79 Not Detected 2.0 Not DetectedVinyl Chloride
3.2 Not Detected 8.3 Not DetectedChloroethane
3.2 Not Detected 6.0 Not DetectedEthanol
0.79 Not Detected 3.1 Not Detected1,1-Dichloroethene
7.9 Not Detected 27 Not DetectedMethylene Chloride
0.79 Not Detected 3.1 Not Detectedtrans-1,2-Dichloroethene
0.79 Not Detected 3.2 Not Detected1,1-Dichloroethane
0.79 Not Detected 3.1 Not Detectedcis-1,2-Dichloroethene
0.79 Not Detected 3.8 Not DetectedChloroform
0.79 Not Detected 4.3 Not Detected1,1,1-Trichloroethane
0.79 Not Detected 5.0 Not DetectedCarbon Tetrachloride
0.79 Not Detected 4.2 Not DetectedTrichloroethene
0.79 2.7 5.4 18Tetrachloroethene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
99 70-130Toluene-d8
104 70-1301,2-Dichloroethane-d4
99 70-1304-Bromofluorobenzene
Page 7 of 17
Client Sample ID: SS-4
Lab ID#: 1208404A-04A
EPA METHOD TO-15 GC/MS FULL SCAN
2082334File Name:
Dil. Factor:1.55
Date of Collection: 8/15/12 12:50:00 PM
Date of Analysis: 8/24/12 03:55 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
7.8 Not Detected 16 Not DetectedChloromethane
0.78 Not Detected 2.0 Not DetectedVinyl Chloride
3.1 Not Detected 8.2 Not DetectedChloroethane
3.1 Not Detected 5.8 Not DetectedEthanol
0.78 Not Detected 3.1 Not Detected1,1-Dichloroethene
7.8 Not Detected 27 Not DetectedMethylene Chloride
0.78 Not Detected 3.1 Not Detectedtrans-1,2-Dichloroethene
0.78 Not Detected 3.1 Not Detected1,1-Dichloroethane
0.78 Not Detected 3.1 Not Detectedcis-1,2-Dichloroethene
0.78 Not Detected 3.8 Not DetectedChloroform
0.78 Not Detected 4.2 Not Detected1,1,1-Trichloroethane
0.78 Not Detected 4.9 Not DetectedCarbon Tetrachloride
0.78 Not Detected 4.2 Not DetectedTrichloroethene
0.78 2.7 5.2 18Tetrachloroethene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
100 70-130Toluene-d8
97 70-1301,2-Dichloroethane-d4
100 70-1304-Bromofluorobenzene
Page 8 of 17
Client Sample ID: SS-5
Lab ID#: 1208404A-05A
EPA METHOD TO-15 GC/MS FULL SCAN
2082406File Name:
Dil. Factor:1.44
Date of Collection: 8/15/12 1:10:00 PM
Date of Analysis: 8/24/12 08:37 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
7.2 Not Detected 15 Not DetectedChloromethane
0.72 Not Detected 1.8 Not DetectedVinyl Chloride
2.9 Not Detected 7.6 Not DetectedChloroethane
2.9 Not Detected 5.4 Not DetectedEthanol
0.72 Not Detected 2.8 Not Detected1,1-Dichloroethene
7.2 Not Detected 25 Not DetectedMethylene Chloride
0.72 Not Detected 2.8 Not Detectedtrans-1,2-Dichloroethene
0.72 Not Detected 2.9 Not Detected1,1-Dichloroethane
0.72 Not Detected 2.8 Not Detectedcis-1,2-Dichloroethene
0.72 Not Detected 3.5 Not DetectedChloroform
0.72 Not Detected 3.9 Not Detected1,1,1-Trichloroethane
0.72 Not Detected 4.5 Not DetectedCarbon Tetrachloride
0.72 Not Detected 3.9 Not DetectedTrichloroethene
0.72 9.4 4.9 64Tetrachloroethene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
101 70-130Toluene-d8
101 70-1301,2-Dichloroethane-d4
99 70-1304-Bromofluorobenzene
Page 9 of 17
Client Sample ID: Lab Blank
Lab ID#: 1208404A-06A
EPA METHOD TO-15 GC/MS FULL SCAN
2082330File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 8/24/12 12:24 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
5.0 Not Detected 10 Not DetectedChloromethane
0.50 Not Detected 1.3 Not DetectedVinyl Chloride
2.0 Not Detected 5.3 Not DetectedChloroethane
2.0 Not Detected 3.8 Not DetectedEthanol
0.50 Not Detected 2.0 Not Detected1,1-Dichloroethene
5.0 Not Detected 17 Not DetectedMethylene Chloride
0.50 Not Detected 2.0 Not Detectedtrans-1,2-Dichloroethene
0.50 Not Detected 2.0 Not Detected1,1-Dichloroethane
0.50 Not Detected 2.0 Not Detectedcis-1,2-Dichloroethene
0.50 Not Detected 2.4 Not DetectedChloroform
0.50 Not Detected 2.7 Not Detected1,1,1-Trichloroethane
0.50 Not Detected 3.1 Not DetectedCarbon Tetrachloride
0.50 Not Detected 2.7 Not DetectedTrichloroethene
0.50 Not Detected 3.4 Not DetectedTetrachloroethene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
99 70-130Toluene-d8
103 70-1301,2-Dichloroethane-d4
102 70-1304-Bromofluorobenzene
Page 10 of 17
Client Sample ID: Lab Blank
Lab ID#: 1208404A-06B
EPA METHOD TO-15 GC/MS FULL SCAN
2082405File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 8/24/12 07:20 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
5.0 Not Detected 10 Not DetectedChloromethane
0.50 Not Detected 1.3 Not DetectedVinyl Chloride
2.0 Not Detected 5.3 Not DetectedChloroethane
2.0 Not Detected 3.8 Not DetectedEthanol
0.50 Not Detected 2.0 Not Detected1,1-Dichloroethene
5.0 Not Detected 17 Not DetectedMethylene Chloride
0.50 Not Detected 2.0 Not Detectedtrans-1,2-Dichloroethene
0.50 Not Detected 2.0 Not Detected1,1-Dichloroethane
0.50 Not Detected 2.0 Not Detectedcis-1,2-Dichloroethene
0.50 Not Detected 2.4 Not DetectedChloroform
0.50 Not Detected 2.7 Not Detected1,1,1-Trichloroethane
0.50 Not Detected 3.1 Not DetectedCarbon Tetrachloride
0.50 Not Detected 2.7 Not DetectedTrichloroethene
0.50 Not Detected 3.4 Not DetectedTetrachloroethene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
100 70-130Toluene-d8
99 70-1301,2-Dichloroethane-d4
96 70-1304-Bromofluorobenzene
Page 11 of 17
Client Sample ID: CCV
Lab ID#: 1208404A-07A
EPA METHOD TO-15 GC/MS FULL SCAN
2082319aFile Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 8/23/12 07:44 PM
%RecoveryCompound
92Chloromethane
84Vinyl Chloride
93Chloroethane
99Ethanol
821,1-Dichloroethene
85Methylene Chloride
86trans-1,2-Dichloroethene
841,1-Dichloroethane
87cis-1,2-Dichloroethene
85Chloroform
881,1,1-Trichloroethane
90Carbon Tetrachloride
87Trichloroethene
85Tetrachloroethene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
103 70-130Toluene-d8
98 70-1301,2-Dichloroethane-d4
104 70-1304-Bromofluorobenzene
Page 12 of 17
Client Sample ID: CCV
Lab ID#: 1208404A-07B
EPA METHOD TO-15 GC/MS FULL SCAN
2082402File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 8/24/12 05:20 PM
%RecoveryCompound
113Chloromethane
102Vinyl Chloride
112Chloroethane
133 QEthanol
991,1-Dichloroethene
103Methylene Chloride
102trans-1,2-Dichloroethene
981,1-Dichloroethane
102cis-1,2-Dichloroethene
99Chloroform
1011,1,1-Trichloroethane
104Carbon Tetrachloride
104Trichloroethene
101Tetrachloroethene
Q = Exceeds Quality Control limits.
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
101 70-130Toluene-d8
96 70-1301,2-Dichloroethane-d4
99 70-1304-Bromofluorobenzene
Page 13 of 17
Client Sample ID: LCS
Lab ID#: 1208404A-08A
EPA METHOD TO-15 GC/MS FULL SCAN
2082326File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 8/24/12 09:56 AM
%RecoveryCompound
112Chloromethane
100Vinyl Chloride
106Chloroethane
121Ethanol
1001,1-Dichloroethene
96Methylene Chloride
109trans-1,2-Dichloroethene
961,1-Dichloroethane
98cis-1,2-Dichloroethene
97Chloroform
1001,1,1-Trichloroethane
103Carbon Tetrachloride
101Trichloroethene
96Tetrachloroethene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
100 70-130Toluene-d8
98 70-1301,2-Dichloroethane-d4
103 70-1304-Bromofluorobenzene
Page 14 of 17
Client Sample ID: LCSD
Lab ID#: 1208404A-08AA
EPA METHOD TO-15 GC/MS FULL SCAN
2082327File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 8/24/12 10:26 AM
%RecoveryCompound
105Chloromethane
94Vinyl Chloride
104Chloroethane
119Ethanol
1011,1-Dichloroethene
94Methylene Chloride
109trans-1,2-Dichloroethene
951,1-Dichloroethane
99cis-1,2-Dichloroethene
96Chloroform
981,1,1-Trichloroethane
101Carbon Tetrachloride
100Trichloroethene
96Tetrachloroethene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
100 70-130Toluene-d8
96 70-1301,2-Dichloroethane-d4
104 70-1304-Bromofluorobenzene
Page 15 of 17
Client Sample ID: LCS
Lab ID#: 1208404A-08B
EPA METHOD TO-15 GC/MS FULL SCAN
2082403File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 8/24/12 06:03 PM
%RecoveryCompound
103Chloromethane
92Vinyl Chloride
99Chloroethane
101Ethanol
941,1-Dichloroethene
89Methylene Chloride
101trans-1,2-Dichloroethene
881,1-Dichloroethane
92cis-1,2-Dichloroethene
89Chloroform
901,1,1-Trichloroethane
93Carbon Tetrachloride
92Trichloroethene
89Tetrachloroethene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
100 70-130Toluene-d8
94 70-1301,2-Dichloroethane-d4
102 70-1304-Bromofluorobenzene
Page 16 of 17
Client Sample ID: LCSD
Lab ID#: 1208404A-08BB
EPA METHOD TO-15 GC/MS FULL SCAN
2082404File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 8/24/12 06:33 PM
%RecoveryCompound
96Chloromethane
88Vinyl Chloride
95Chloroethane
102Ethanol
931,1-Dichloroethene
89Methylene Chloride
98trans-1,2-Dichloroethene
871,1-Dichloroethane
92cis-1,2-Dichloroethene
88Chloroform
901,1,1-Trichloroethane
91Carbon Tetrachloride
92Trichloroethene
88Tetrachloroethene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
101 70-130Toluene-d8
96 70-1301,2-Dichloroethane-d4
103 70-1304-Bromofluorobenzene
Page 17 of 17
8/30/2012
Mr. Anthony Kellogg
AMEC Environment & Infrastructure
4021 Stirrup Creek Drive
Suite 100
Durham NC 27703
Project Name: GE-CHARLOTTE
Project #: GE-CHARLOTTE
Dear Mr. Anthony Kellogg
The following report includes the data for the above referenced project for sample(s)
received on 8/17/2012 at Air Toxics Ltd.
The data and associated QC analyzed by Modified ASTM D-1946 are compliant with
the project requirements or laboratory criteria with the exception of the deviations
noted in the attached case narrative.
Thank you for choosing Air Toxics Ltd. for your air analysis needs. Air Toxics Ltd. is
committed to providing accurate data of the highest quality. Please feel free to contact
the Project Manager: Ausha Scott at 916-985-1000 if you have any questions regarding
the data in this report.
Regards,
Ausha Scott
Project Manager
Workorder #: 1208404B
Page 1 of 9
Mr. Anthony Kellogg
AMEC Environment & Infrastructure
4021 Stirrup Creek Drive
Suite 100
Durham, NC 27703
WORK ORDER #:1208404B
CLIENT:BILL TO:
PHONE:
Accounts Payable-Durham
AMEC Environment & Infrastructure
4021 Stirrup Creek Drive
Suite 100
Durham, NC 27703
919-381-9900
08/17/2012
DATE COMPLETED:08/30/2012
P.O. #C012500874
PROJECT #GE-CHARLOTTE GE-CHARLOTTE
Work Order Summary
FAX:
DATE RECEIVED:CONTACT:Ausha Scott
NAMEFRACTION #TEST VAC./PRES.
RECEIPT
PRESSURE
FINAL
01A SS-1 Modified ASTM D-1946 3.0 "Hg 5 psi
02A Lab Blank Modified ASTM D-1946 NA NA
03A LCS Modified ASTM D-1946 NA NA
03AA LCSD Modified ASTM D-1946 NA NA
CERTIFIED BY:
Technical Director
DATE:
Name of Accrediting Agency: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program)
Accreditation number: CA300005, Effective date: 10/18/2011, Expiration date: 10/17/2012.
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 9563
[phone] . [phone] . FAX [phone]
08/30/12
Page 2 of 9
This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc.
Eurofins Air Toxics Ltd. certifies that the test results contained in this report meet all requirements of the NELAC standards
Certfication numbers: AZ Licensure AZ0775, CA NELAP - 12282CA, NY NELAP - 11291,
TX NELAP - T104704434-12-5, UT NELAP CA009332012-3, WA NELAP - C935
LABORATORY NARRATIVEModified ASTM D-1946AMEC Environment & InfrastructureWorkorder# 1208404B
One 1 Liter Summa Canister sample was received on August 17, 2012. The laboratory performed
analysis via Modified ASTM Method D-1946 for Helium in air using GC/TCD. The method involves
direct injection of 1.0 mL of sample.
Method modifications taken to run these samples are summarized in the table below. Specific project
requirements may over-ride the ATL modifications.
Requirement ATL ModificationsASTM D-1946
Calibration A single point
calibration is
performed using a
reference standard
closely matching the
composition of the
unknown.
A 3-point calibration curve is performed. Quantitation is
based on a daily calibration standard which may or may
not resemble the composition of the associated samples.
Reference Standard The composition of any
reference standard
must be known to
within 0.01 mol % for
any component.
The standards used by ATL are blended to a >/= 95%
accuracy.
Sample Injection Volume Components whose
concentrations are in
excess of 5 % should
not be analyzed by
using sample volumes
greater than 0.5 mL.
The sample container is connected directly to a fixed
volume sample loop of 1.0 mL on the GC. Linear range
is defined by the calibration curve. Bags are loaded by
vacuum.
Normalization Normalize the mole
percent values by
multiplying each value
by 100 and dividing by
the sum of the original
values. The sum of the
original values should
not differ from 100%
by more than 1.0%.
Results are not normalized. The sum of the reported
values can differ from 100% by as much as 15%, either
due to analytical variability or an unusual sample matrix.
Precision Precision requirements
established at each
concentration level.
Duplicates should agree within 25% RPD for detections
> 5 X's the RL.
Receiving Notes
There were no receiving discrepancies.
There were no analytical discrepancies.
Analytical Notes
Page 3 of 9
Seven qualifiers may have been used on the data analysis sheets and indicate as follows:
B - Compound present in laboratory blank greater than reporting limit.
J - Estimated value.
E - Exceeds instrument calibration range.
S - Saturated peak.
Q - Exceeds quality control limits.
U - Compound analyzed for but not detected above the detection limit.
M - Reported value may be biased due to apparent matrix interferences.
File extensions may have been used on the data analysis sheets and indicates
as follows:
a-File was requantified
b-File was quantified by a second column and detector
r1-File was requantified for the purpose of reissue
Definition of Data Qualifying Flags
Page 4 of 9
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
Summary of Detected Compounds
Client Sample ID: SS-1
Lab ID#: 1208404B-01A
No Detections Were Found.
Page 5 of 9
Client Sample ID: SS-1
Lab ID#: 1208404B-01A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
9082940File Name:
Dil. Factor:2.00
Date of Collection: 8/15/12 11:46:00 AM
Date of Analysis: 8/30/12 07:33 AM
(%)(%)Compound
AmountRpt. Limit
0.10 Not DetectedHelium
Container Type: 1 Liter Summa Canister
Page 6 of 9
Client Sample ID: Lab Blank
Lab ID#: 1208404B-02A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
9082926File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 8/29/12 09:10 PM
(%)(%)Compound
AmountRpt. Limit
0.050 Not DetectedHelium
Container Type: NA - Not Applicable
Page 7 of 9
Client Sample ID: LCS
Lab ID#: 1208404B-03A
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
9082925File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 8/29/12 09:02 PM
%RecoveryCompound
99Helium
Container Type: NA - Not Applicable
Page 8 of 9
Client Sample ID: LCSD
Lab ID#: 1208404B-03AA
NATURAL GAS ANALYSIS BY MODIFIED ASTM D-1946
9082941File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 8/30/12 07:48 AM
%RecoveryCompound
100Helium
Container Type: NA - Not Applicable
Page 9 of 9
Results of Sub-slab Vapor Sampling
TFS Charlotte Branch
1906 Bancroft Street, Charlotte, North Carolina

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d
e
x

(
H
I
)
=
1
]

µ
g
/
m
3
Ra
t
i
o

=

M
a
x

C
o
n
c
e
n
t
r
a
t
i
o
n

÷

E
P
A

R
S
L
CU
M
U
L
A
T
I
V
E

H
I

(
s
u
m

o
f

r
a
t
i
o
s
)

0
.
3
4

C
U
M
U
L
A
T
I
V
E

H
I

w
i
t
h

9
0
x

A
t
t
e
n

F
a
c
t
o
r
Ra
t
i
o

=

M
a
x

C
o
n
c
e
n
t
r
a
t
i
o
n

÷

E
P
A

R
S
L
Cu
m
u
l
a
t
i
v
e

R
i
s
k

f
o
r

B
u
i
l
d
i
n
g

O
c
c
u
p
a
n
t
GE

F
T
S
Cu
m
u
l
a
t
i
v
e

R
i
s
k

C
a
l
c
u
l
a
t
i
o
n

f
o
r

I
n
d
o
o
r

A
i
r

P
a
t
h
w
a
y

(
R
e
s
i
d
e
n
t
i
a
l
)
Ma
x
i
m
u
m

C
o
n
c
e
n
t
r
a
t
i
o
n

D
e
t
e
c
t
e
d

(
µ
g
/
m
3 )
IH
S
B

A
c
c
e
p
t
a
b
l
e

I
n
d
o
o
r

A
i
r

C
o
n
c
e
n
t
r
a
i
o
n

(
C
i
a
)

u
g
/
m
3

Ca
r
c
i
n
o
g
e
n
i
c

T
a
r
g
e
t

R
i
s
k

(
T
R
)

=

1
E
-
0
6

µ
g
/
m
3
Si
t
e
:

S
a
m
p
l
e

I
D
:

S
S
-
2
P
C
E
23
0
35
.
0
0
6.
5
7
P
C
E
23
0
18
0
1.
2
7
7
8
No
t
e
s
:
1.

R
S
L
s

a
v
a
i
l
a
b
l
e

a
t
:

ht
t
p
:
/
/
w
w
w
.
e
p
a
.
g
o
v
/
r
e
g
3
h
w
m
d
/
r
i
s
k
/
h
u
m
a
n
/
r
b
-
c
o
n
c
e
n
t
r
a
t
i
o
n
_
t
a
b
l
e
/
G
e
n
e
r
i
c
_
T
a
b
l
e
s
/
i
n
d
e
x
.
h
t
m
2.

A
t
t
e
n
u
a
t
i
o
n

F
a
c
t
o
r

b
a
s
e
d

o
n

U
S
E
P
A

V
a
p
o
r

I
n
t
r
u
s
i
o
n

G
u
i
d
a
n
c
e
,

D
e
c
e
m
b
e
r

1
3
,

2
0
1
2
On
l
y

c
o
m
p
o
u
n
d
s

w
i
t
h

c
u
m
u
l
a
t
i
v
e

r
i
s
k

a
n
d
/
o
r

H
I

v
a
l
u
e
s

w
e
r
e

i
n
c
l
u
d
e
d

i
n

t
h
e

c
a
l
c
u
l
a
t
i
o
n
Ra
t
i
o

=

M
a
x

C
o
n
c
e
n
t
r
a
t
i
o
n

÷

E
P
A

R
S
L
Cu
m
u
l
a
t
i
v
e

R
i
s
k

f
o
r

B
u
i
l
d
i
n
g

O
c
c
u
p
a
n
t
TF
S

C
h
a
r
l
o
t
t
e

B
r
a
n
c
h
Cu
m
u
l
a
t
i
v
e

R
i
s
k

C
a
l
c
u
l
a
t
i
o
n

f
o
r

I
n
d
o
o
r

A
i
r

P
a
t
h
w
a
y

(
R
e
s
i
d
e
n
t
i
a
l
)
Ma
x
i
m
u
m

C
o
n
c
e
n
t
r
a
t
i
o
n

D
e
t
e
c
t
e
d

(
µ
g
/
m
3 )
IH
S
B

A
c
c
e
p
t
a
b
l
e

I
n
d
o
o
r

A
i
r

C
o
n
c
e
n
t
r
a
i
o
n

(
C
i
a
)

u
g
/
m
3

Ca
r
c
i
n
o
g
e
n
i
c

T
a
r
g
e
t

R
i
s
k

(
T
R
)

=

1
E
-
0
6

µ
g
/
m
3
0.01
CU
M
U
L
A
T
I
V
E

R
I
S
K

(
s
u
m

o
f

r
a
t
i
o
s

x

1
0
-6
)
6.
5
7
E
-
0
6

C
U
M
U
L
A
T
I
V
E

R
I
S
K

W
i
t
h

9
0
x

A
t
t
e
n
u
a
t
i
o
n

F
a
c
t
o
r

7
.
3
0
E
-
0
8
Cu
m
u
l
a
t
i
v
e

H
a
z
a
r
d

I
n
d
e
x

(
H
I
)

C
a
l
c
u
l
a
t
i
o
n

f
o
r

I
n
d
o
o
r

A
i
r

P
a
t
h
w
a
y

(
R
e
s
i
d
e
n
t
i
a
l
)
Ma
x
i
m
u
m

C
o
n
c
e
n
t
r
a
t
i
o
n

D
e
t
e
c
t
e
d

EP
A

R
e
g
i
o
n
a
l

S
c
r
e
e
n
i
n
g

L
e
v
e
l

(
R
S
L
)

f
o
r

R
e
s
i
d
e
n
t
i
a
l

Ai
r

[
n
o
n
c
a
n
c
e
r

H
a
z
a
r
d

I
n
d
e
x

(
H
I
)
=
1
]

µ
g
/
m
3
Ra
t
i
o

=

M
a
x

C
o
n
c
e
n
t
r
a
t
i
o
n

÷

E
P
A

R
S
L
CU
M
U
L
A
T
I
V
E

H
I

(
s
u
m

o
f

r
a
t
i
o
s
)

1
.
2
8

C
U
M
U
L
A
T
I
V
E

H
I

w
i
t
h

9
0
x

A
t
t
e
n
u
a
t
i
o
n

F
a
c
t
o
r
Si
t
e
:

S
a
m
p
l
e

I
D
:

S
S
-
3
P
C
E
18
35
.
0
0
0.
5
1
P
C
E
18
18
0
0.
1
0
0
0
No
t
e
s
:
1.

R
S
L
s

a
v
a
i
l
a
b
l
e

a
t
:

ht
t
p
:
/
/
w
w
w
.
e
p
a
.
g
o
v
/
r
e
g
3
h
w
m
d
/
r
i
s
k
/
h
u
m
a
n
/
r
b
-
c
o
n
c
e
n
t
r
a
t
i
o
n
_
t
a
b
l
e
/
G
e
n
e
r
i
c
_
T
a
b
l
e
s
/
i
n
d
e
x
.
h
t
m
2.

A
t
t
e
n
u
a
t
i
o
n

F
a
c
t
o
r

b
a
s
e
d

o
n

U
S
E
P
A

V
a
p
o
r

I
n
t
r
u
s
i
o
n

G
u
i
d
a
n
c
e
,

D
e
c
e
m
b
e
r

1
3
,

2
0
1
2
On
l
y

c
o
m
p
o
u
n
d
s

w
i
t
h

c
u
m
u
l
a
t
i
v
e

r
i
s
k

a
n
d
/
o
r

H
I

v
a
l
u
e
s

w
e
r
e

i
n
c
l
u
d
e
d

i
n

t
h
e

c
a
l
c
u
l
a
t
i
o
n
Ra
t
i
o

=

M
a
x

C
o
n
c
e
n
t
r
a
t
i
o
n

÷

E
P
A

R
S
L
Cu
m
u
l
a
t
i
v
e

R
i
s
k

f
o
r

B
u
i
l
d
i
n
g

O
c
c
u
p
a
n
t
GE

F
T
S
Cu
m
u
l
a
t
i
v
e

R
i
s
k

C
a
l
c
u
l
a
t
i
o
n

f
o
r

I
n
d
o
o
r

A
i
r

P
a
t
h
w
a
y

(
R
e
s
i
d
e
n
t
i
a
l
)
Ma
x
i
m
u
m

C
o
n
c
e
n
t
r
a
t
i
o
n

D
e
t
e
c
t
e
d

(
µ
g
/
m
3 )
IH
S
B

A
c
c
e
p
t
a
b
l
e

I
n
d
o
o
r

A
i
r

C
o
n
c
e
n
t
r
a
i
o
n

(
C
i
a
)

u
g
/
m
3

Ca
r
c
i
n
o
g
e
n
i
c

T
a
r
g
e
t

R
i
s
k

(
T
R
)

=

1
E
-
0
6

µ
g
/
m
3
0.00
CU
M
U
L
A
T
I
V
E

R
I
S
K

(
s
u
m

o
f

r
a
t
i
o
s

x

1
0
-6
)
5.
1
4
E
-
0
7

C
U
M
U
L
A
T
I
V
E

R
I
S
K

W
i
t
h

9
0
x

A
t
t
e
n

F
a
c
t
o
r

5
.
7
1
E
-
0
9
Cu
m
u
l
a
t
i
v
e

H
a
z
a
r
d

I
n
d
e
x

(
H
I
)

C
a
l
c
u
l
a
t
i
o
n

f
o
r

I
n
d
o
o
r

A
i
r

P
a
t
h
w
a
y

(
R
e
s
i
d
e
n
t
i
a
l
)
Ma
x
i
m
u
m

C
o
n
c
e
n
t
r
a
t
i
o
n

D
e
t
e
c
t
e
d

EP
A

R
e
g
i
o
n
a
l

S
c
r
e
e
n
i
n
g

L
e
v
e
l

(
R
S
L
)

f
o
r

R
e
s
i
d
e
n
t
i
a
l

Ai
r

[
n
o
n
c
a
n
c
e
r

H
a
z
a
r
d

I
n
d
e
x

(
H
I
)
=
1
]

µ
g
/
m
3
Ra
t
i
o

=

M
a
x

C
o
n
c
e
n
t
r
a
t
i
o
n

÷

E
P
A

R
S
L
CU
M
U
L
A
T
I
V
E

H
I

(
s
u
m

o
f

r
a
t
i
o
s
)

0
.
1
0

C
U
M
U
L
A
T
I
V
E

H
I

w
i
t
h

9
0
x

A
t
t
e
n

F
a
c
t
o
r
Si
t
e
:

S
a
m
p
l
e

I
D
:

S
S
-
4
P
C
E
18
35
.
0
0
0.
5
1
P
C
E
18
18
0
0.
1
0
0
0
No
t
e
s
:
1.

R
S
L
s

a
v
a
i
l
a
b
l
e

a
t
:

ht
t
p
:
/
/
w
w
w
.
e
p
a
.
g
o
v
/
r
e
g
3
h
w
m
d
/
r
i
s
k
/
h
u
m
a
n
/
r
b
-
c
o
n
c
e
n
t
r
a
t
i
o
n
_
t
a
b
l
e
/
G
e
n
e
r
i
c
_
T
a
b
l
e
s
/
i
n
d
e
x
.
h
t
m
2.

A
t
t
e
n
u
a
t
i
o
n

F
a
c
t
o
r

b
a
s
e
d

o
n

U
S
E
P
A

V
a
p
o
r

I
n
t
r
u
s
i
o
n

G
u
i
d
a
n
c
e
,

D
e
c
e
m
b
e
r

1
3
,

2
0
1
2
On
l
y

c
o
m
p
o
u
n
d
s

w
i
t
h

c
u
m
u
l
a
t
i
v
e

r
i
s
k

a
n
d
/
o
r

H
I

v
a
l
u
e
s

w
e
r
e

i
n
c
l
u
d
e
d

i
n

t
h
e

c
a
l
c
u
l
a
t
i
o
n
Ra
t
i
o

=

M
a
x

C
o
n
c
e
n
t
r
a
t
i
o
n

÷

E
P
A

R
S
L
Cu
m
u
l
a
t
i
v
e

R
i
s
k

f
o
r

B
u
i
l
d
i
n
g

O
c
c
u
p
a
n
t
GE

F
T
S
Cu
m
u
l
a
t
i
v
e

R
i
s
k

C
a
l
c
u
l
a
t
i
o
n

f
o
r

I
n
d
o
o
r

A
i
r

P
a
t
h
w
a
y

(
R
e
s
i
d
e
n
t
i
a
l
)
Ma
x
i
m
u
m

C
o
n
c
e
n
t
r
a
t
i
o
n

D
e
t
e
c
t
e
d

(
µ
g
/
m
3 )
IH
S
B

A
c
c
e
p
t
a
b
l
e

I
n
d
o
o
r

A
i
r

C
o
n
c
e
n
t
r
a
i
o
n

(
C
i
a
)

u
g
/
m
3

Ca
r
c
i
n
o
g
e
n
i
c

T
a
r
g
e
t

R
i
s
k

(
T
R
)

=

1
E
-
0
6

µ
g
/
m
3
0.00
CU
M
U
L
A
T
I
V
E

R
I
S
K

(
s
u
m

o
f

r
a
t
i
o
s

x

1
0
-6
)
5.
1
4
E
-
0
7

C
U
M
U
L
A
T
I
V
E

R
I
S
K

W
i
t
h

9
0
x

A
t
t
e
n

F
a
c
t
o
r

5
.
7
1
E
-
0
9
Cu
m
u
l
a
t
i
v
e

H
a
z
a
r
d

I
n
d
e
x

(
H
I
)

C
a
l
c
u
l
a
t
i
o
n

f
o
r

I
n
d
o
o
r

A
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