HomeMy WebLinkAbout18052_Gelco Trailer_Phase II ESA_2012_8Phase II Environmental Site Assessment
Trailer Fleet Services
Charlotte North Carolina Branch
August 2012
ES-1
Executive Summary
AMEC Environment and Infrastructure, Inc. (AMEC) conducted a Phase II Environmental Site
Assessment (ESA) at the GE Trailer Fleet Services (TFS) Charlotte branch located at 1906
Bancroft Street, in Charlotte, Mecklenberg County, North Carolina (the “Site”).
The Site is owned by TFS as Transport International Pool, Inc. however, TFS no longer
occupies the Site and the Site is currently vacant. The Site was used by TFS from 1986 to 2011
as a branch location for the leasing, parking, storage, and minor repair of over-the-road trailers.
Minor repairs and typical maintenance included skin repair, hub oil changes, tire changes, brake
cleaning and change outs, and service to refrigerated units. Prior to 1986 the property was
undeveloped woodland.
The Site is located in an area with mixed industrial and commercial use, with several industrial
and commercial establishments located both north and west of the Site, i.e., in an upgradient
orientation with respect to the Site and within a half mile of the Site. A number of these
upgradient Sites have a history of solvent use and confirmed impacts to soil and groundwater
based on a search of environmental databases and review of readily available reports.
This Phase II ESA was conducted in two phases. The initial phase consisted of collecting soil
samples at 12 boring locations, with two soil samples collected from each boring for analysis of
volatile organic compounds (VOCs), semi-volatile organic compounds (SVOCs), total petroleum
hydrocarbons (TPH) for gasoline range organics (GRO) and diesel range organics (DRO), and
Priority Pollutant List Metals plus barium and tin. Samples were collected from a shallow
interval (generally 0.5 to 2 feet below ground surface (ft-bgs)) and a deeper interval
(approximately one to two feet above the observed water-table if wet soil conditions were
encountered in the upper 10 to 15 feet of the soil column, otherwise soil samples were collected
from the 10 to 12 ft-bgs). Additionally, a shallow soil sample was collected from each boring for
analysis of polychlorinated biphenyls (PCBs).
Five of the soil borings were converted into monitoring wells, the remaining borings were
backfilled with a cement/bentonite slurry. Soils not used for laboratory analysis were drummed
for offsite disposal by Safety-Kleen.
The monitoring wells were developed and later, purged and sampled for VOCs, SVOCs and
metals (both total and dissolved). Based on the results of the initial round of groundwater
sampling, during which VOCs were detected, four additional wells were installed to assess if
onsite sources existed, and to assess groundwater conditions along the upgradient Site
boundary.
The analytical data for the soil samples were compared to the North Carolina Department of
Environment and Natural Resources (NCDENR) Inactive Hazardous Sites Branch (IHSB)
Preliminary Soil Remediation Goals (SRGs), last updated February 2012. The NCDENR Soil
Remediation Goals (SRGs) are based on a comparison of the Preliminary Industrial Health-
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August 2012
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Based Soil Remediation Goal (IHSRG) and the Protection of Groundwater Preliminary Site
Remediation Goal (PSRG). The lower of the IHSRG and PSRG is the SRG. The use of the
IHSRG in lieu of the Preliminary Residential Health-Based Soil Remediation Goal (PRHSRG)
will result in an industrial restricted land use.
Values for soil TPH were compared to NCDENR screening values. The NCDENR TPH-GRO
and DRO screening criterion for soil is 10 milligrams per Kilogram (mg/Kg).
Groundwater results were compared to the NCDENR 2L Groundwater Quality Standards (2L
Standards) last updated January 1, 2010 with interim standards for select compounds being
updated July 12, 2012.
The following was identified based on the findings of this Phase II ESA:
Soils
Soils encountered during drilling were generally sandy clays to approximately 7.5 ft-bgs,
clay to 9.5 ft-bgs and then sandy silt/silty sand to the total depth of the boring. At some
locations, weathered rock was encountered at approximately 23 ft-bgs.
With the exception of acetone and methyl ethyl ketone (MEK) VOCs were not detected
in Site soils. Both acetone and MEK were below their respective SRG and reported as
estimated concentrations (i.e., below the laboratory Practical Quantitation Limit (PQL),
but above the MDL). Both MEK and acetone are considered laboratory and/or field
preservation artifacts and not representative of Site conditions.
No SVOCs were detected in Site soils.
No TPH-GRO, TPH-DRO or PCBs were detected in Site soils.
Metals detected in soils included arsenic, barium, chromium, copper, lead, nickel,
selenium and zinc, of which arsenic, chromium and selenium were detected above the
NCDENR SRGs. NCDENR does not have an SRG for total chromium; therefore, total
chromium results were compared to the hexavalent chromium SRG.
Reported total chromium concentrations in soils were above the hexavalent chromium
SRG, but below the trivalent chromium SRG. To confirm the reported total chromium
was not comprised of hexavalent chromium, the five sample locations with the highest
total chromium concentrations were resampled and analyzed specifically for hexavalent
chromium. Hexavalent chromium was not detected in the samples analyzed. Based on
the absence of hexavalent chromium in the samples analyzed and the Site history (no
industrial past and no confirmed fill materials), the chromium concentrations observed at
the Site were compared to the trivalent chromium SRG and there were no exceedences
to the trivalent chromium SRG. Therefore, based on the noted conditions, the presence
of chromium is considered to be representative of naturally occurring conditions and no
additional investigation is warranted.
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Arsenic concentrations across the Site were generally consistent both horizontally and at
depth, and were below the average arsenic concentration in North Carolina of 4.5 mg/Kg
as reported by the North Carolina Department of Agriculture and Consumer Services
(NCDACS, 2008). Arsenic concentrations ranged from 0.64 mg/Kg to 2.8 mg/Kg with an
average concentration of 1.7 mg/Kg. The arsenic concentrations observed at the Site
are considered representative of background and/or naturally occuring conditions.
Selenium was detected a concentrations ranging from 1.2 mg/Kg to 3.8 mg/Kg with an
average concentration of 2.3 mg/Kg as compared to the SRG of 2.1 mg/Kg. The
locations with selenium exceedences were resampled to confirm the results from the first
sampling event. The original results could not be reproduced. Therefore, there were no
exceedences of the selenium SRG, and the presence of selenium is considered to be
reflective of naturally occurring conditions. Therefore, no additional investigation is
warranted.
Groundwater
Wet soil conditions were first encountered between 18 and 28.5 ft-bgs. Based on water
levels observed in onsite groundwater monitoring wells, groundwater flows onto the Site
from the north and west and generally flows toward the south and then southeast in the
southern portion of the Site. Based on the southeast flow direction monitor wells MW-6,
MW-7 and MW-9 are considered upgradient wells for Site in the southern end of the Site
and MW-5 is an upgradient well in the northern portion of the Site. Therefore, properties
to the north and west are considered to be in an upgradient orientation with respect to
the Site.
VOCs detected in groundwater samples from the Site include chloroform, carbon
tetrachloride, 1,1-dichloroethane (1,1-DCA), 1,1-dichloroethene (1,1-DCE), cis-1,2-
dichloroethene (c1,2-DCE), tetrachloroethene (PCE) and trichloroethylene (TCE), of
which only carbon tetrachloride, 1,1-DCE, PCE and TCE were above the NCDENR 2L
Standards. TCE, 1,1- DCE, and PCE were detected in samples from upgradient wells
as well as in samples from downgradient well MW-1 at similar, but slightly higher
concentrations. Carbon tetrachloride was detected in only one downgradient well.
Based on the distribution of 1,1-DCE, PCE and TCE observed in groundwater in
upgradient wells, the absence of these constituents in Site soils, the industrial nature of
the surrounding properties and the potential sources for these constituents upgradient of
the Site, it is likely that the presence these constituents in Site groundwater are the
result of an upgradient source.
Carbon tetrachloride was detected in groundwater samples collected from downgradient
well MW-2, but not in any other wells on the property. Carbon tetrachloride was a
cleaning and refrigeration solvent phased out from use in the mid-1980s. The Site was
first developed by TFS in 1986 and there were no fill materials observed on the Site.
Based on the date TFS first occupied the site, 1986, and the fact that carbon
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tetrachloride was not detected in Site soils, it is unlikely that the carbon tetrachloride
detected in groundwater is the result of Site operations.
No SVOCs were detected in groundwater samples collected from the Site.
No TPHs were detected groundwater samples collected from the Site
Total chromium was the only metal detected above the chromium 2L Standard in
groundwater samples collected from the Site. The 2L Standards for metals are based
on total (i.e., unfiltered) samples. Total chromium (above the 2L Standard) was detected
in both filtered and non-filtered samples from wells, MW-1 and MW-5, during the initial
round of groundwater sampling, possibly due to turbidity in the newly installed wells. A
second round of samples were collected from wells MW-1 and MW-5 and analyzed for
both total and dissolved chromium. The chromium results from the second sampling
event (both filtered and non-filtered) were below the laboratory Practical Quantitation
Limit (PQL) and did not exceed the 2L Standards in either well.
Following the completion of the Phase II ESA sampling activities and as a result of VOC
detections in groundwater, AMEC conducted a records search for nearby dry cleaners
and industrial facilities in the area of the Site. The records search identified several
facilities to the north and northwest (upgradient) of the Site with confirmed VOC impacts
in soil and/or groundwater. The nearest facilities, with respect to the Site, are a former
dry cleaner in the Hutchinson Shopping Center located approximately 750 feet to the
northwest of the Site, and property with automobile and truck service bays located to the
north of the Site on the abutting property along the northeast corner of the Site.
Compounds detected in soils and/or groundwater at the former dry cleaner location in
the Hutchinson Center included PCE (soil), TCE (soil) and c1,2-DCE (soil) and vinyl
chloride (soil and groundwater) and 1,2-DCE at the former dry cleaner in the Hutchinson
Shopping Center. Compounds detected in groundwater (soil samples were not analyzed
for VOCs) at the property to the north with automotive and truck service bays were PCE,
1,1,1-TCA, 1,2-DCA and chloroform. This property is in a likely side-gradient or potential
upgradient orientation with respect to the Site. AMEC also identified a former
Department of Defense (DoD) facility approximately 1,100 feet to the west-northwest
with VOC (i.e., TCE) impacts to groundwater.
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TABLE OF CONTENTS
Section Page
1.0 INTRODUCTION ............................................................................................................... 1
1.1 Site Location and Description ................................................................................ 1
2.0 INVESTIGATION SCOPE OF WORK .............................................................................. 2
2.1 Investigation Objectives ........................................................................................ 2
2.2 Pre-Field Activities ................................................................................................. 2
2.3 Phase II ESA Field Activities ................................................................................. 2
2.3.1 Soil Sampling .......................................................................................... 3
2.3.2 Groundwater ........................................................................................... 4
3.0 SITE CHARACTERISTICS ............................................................................................... 7
3.1 Topography ........................................................................................................... 7
3.2 Site Soils ............................................................................................................... 7
3.3 Surface Water and Groundwater ........................................................................... 7
3.4 Area Groundwater Impacts ................................................................................... 8
4.0 RESULTS ......................................................................................................................... 9
4.1 Soil Analytical Results ........................................................................................... 9
4.1.1 Volatile Organic Compounds (VOCs) ..................................................... 9
4.1.2 Semivolatile Organic Compounds (SVOCs) ......................................... 10
4.1.3 Metals ................................................................................................... 10
4.1.4 Polychlorinated Biphenyls (PCBs) ........................................................ 12
4.1.5 Petroleum Hydrocarbons ...................................................................... 12
4.2 Groundwater Analytical Results .......................................................................... 12
4.2.1 Volatile Organic Compounds (VOCs) ................................................... 13
4.2.2 Semivolatile Organic Compounds (SVOCs) ......................................... 15
4.2.3 Metals ................................................................................................... 15
4.2.4 Petroleum Hydrocarbons ...................................................................... 17
5.0 SUMMARY OF FINDINGS ............................................................................................. 19
6.0 CERTIFICATION ............................................................................................................ 23
7.0 REFERENCES ................................................................................................................ 24
LIST OF FIGURES
Figure 1 Site Location Map
Figure 2 Exploration Locations
Figure 3 Groundwater Contours – 5/2/11
Figure 4 Groundwater Contours – 6/16/11
Figure 5 Potential Off-Site Source Locations
Figure 6 Groundwater Exceedences – 6/16/2011
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LIST OF TABLES
Table 1 Depth to Groundwater/Groundwater Elevations
Table 2 Nearby Commercial/Industrial and Drycleaning Sites with Potential or
Confirmed Solvent Use
Table 3 Soil Analytical Results – Detected Compounds
Table 4 Groundwater Analytical Results – Detected Compounds
LIST OF APPENDICES
APPENDIX A Soil Boring Logs
APPENDIX B Phase II ESA Laboratory Analytical Reports
APPENDIX C Hutchinson Shopping Center Reports
APPENDIX D BellSouth Work Center Site Characterization Assessment
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1.0 INTRODUCTION
AMEC Environment and Infrastructure, Inc. (AMEC) conducted a Phase II Environmental Site
Assessment (ESA) at the GE Trailer Fleet Services (TFS) Charlotte branch located at 1906
Bancroft Street, in Charlotte, Mecklenberg County, North Carolina (the “Site”). The general
location of the Site is shown on Figure 1.
The Phase II ESA activities were initiated by TFS as part of their overall due diligence program
and to assess if Site operations had affected environmental conditions at the Site. A detailed
discussion of overall Site condition while the TFS business was operational at the Site is
provided in the AMEC Phase I ESA report entitled: Phase I Environmental Site Assessment,
1906 Bancroft Street, Charlotte, North Carolina, dated May 31, 2011 (the “AMEC Phase I ESA
Report”). A copy of the AMEC Phase I ESA Report has been submitted to TFS.
1.1 Site Location and Description
The Site is currently owned by TFS as Transport International Pool, Inc.; however, TFS no
longer occupies the Site and the Site has remained vacant since the TFS operation was
terminated in 2011. While TFS occupied the Site, the Site was used as a branch location for the
leasing, parking, storage, and minor repair of over-the-road trailers. Minor repairs and typical
maintenance included skin repair, hub oil changes, tire changes, brake cleaning and change
outs, and service to refrigerated units.
TFS initially purchased the property in 1986 to run main branch operations on the Site. The Site
has a one-story 3,750 square foot (ft2) corrugated steel building with concrete floor and two
garage bays. TFS used the garage bays for maintenance of over-the-road trailers. The Site
also has a 2,016 ft2 modular office building. Both the shop and maintenance building were
constructed in 1996. The modular unit office building at the Site replaced the original office
building that was constructed in 1986 and subsequently demolished in 1996. The lot is primarily
gravel covered. The Site is connected to the municipal water supply and municipal sanitary
sewer services, both of which are provided by Charlotte Mecklenburg Utilities.
Prior to 1986 the Site was undeveloped, vacant land, owned by the Carolina Investment Group.
The first known use of the Site was by TFS for its trailer leasing operation.
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2.0 INVESTIGATION SCOPE OF WORK
2.1 Investigation Objectives
The specific objective of this Phase II ESA was to establish baseline environmental conditions
at the Site following the cessation of TFS operations. To attain this objective, AMEC completed
both soil and groundwater sampling as described herein.
2.2 Pre-Field Activities
Prior to conducting field activities, AMEC prepared a site-specific health and safety plan (HASP)
to ensure that safe working conditions were maintained for AMEC employees and AMEC
subcontractors while field activities were being conducted. The elements of the HASP were
based on the requirements described in the Occupation Safety and Health Administration
(OSHA) rules (29 CFR 1910.120). The HASP addressed the potential hazards associated with
the field activities and the personnel protective measures to be implemented in response to
these hazards.
Prior to the commencement of field activities, all utilities were cleared via the North Carolina 811
one call system. All drilling locations were also cleared with on-Site personnel prior to
mobilizing to the Site. On-site personnel made sure trailers were not obstructing access to the
drilling locations.
2.3 Phase II ESA Field Activities
From April 28 to May 3, 2011 AMEC performed an initial subsurface investigation program at
the Site. This phase of the investigation consisted of the drilling at 12 locations (see Figure 2)
to collect shallow soil samples (from depths of 0.5 to 2 feet below ground surface (ft-bgs) and
deeper soil samples (from approximately one foot above the water table). Five of the soil boring
locations were completed as monitoring wells. A second round of soil sampling and
groundwater monitoring well installation was conducted on June 9, 2011.
The soil borings and monitoring wells were installed by a North Carolina licensed well driller with
SAEDACCO, Inc. of Fort Mill, South Carolina. Soil borings and monitoring well locations MW-3,
MW-4 and MW-5 were advanced using direct-push drilling techniques with a GeoProbe.
Following soil sampling, the monitoring wells were drilled using hollow stem auger (HSA) drilling
techniques, with locations MW-3, MW-4 and MW-5 being drilled out with HSA for monitoring
well installation. At two of the monitoring well locations (MW-1 and MW-2), a split-spoon
sampler was driven in advance of the HSA to collect soil samples. Split-spoon sampling was
conducted in conformance with the American Society for Testing and Materials (ASTM)
Standard D1586-08a (Standard Test Method for Standard Penetration Test and Split-Barrel
Sampling of Soils).
Based on the first round of soil and groundwater analytical results, on June 9, 2011, additional
soil borings were drilled to confirm the presence or absence of initially detected compounds
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(i.e., to evaluate whether results were reproducible). Additional soil borings were drilled during
this second drilling effort at the following locations: B-2 (B2A), B-6 (B6A), MW-3 (MW3A) and
MW-5 (MW5A). These borings were advanced using direct push drilling techniques and
allowed for confirmatory soil sampling based on the initial round of soil sampling results. Four
additional groundwater monitoring wells (MW-6, MW-7, MW-8 and MW-9) were also installed
using air rotary drilling techniques. These wells allowed for further evaluation of VOCs detected
in groundwater based on the first round of groundwater sampling.
An AMEC geologist was on Site during the investigation to oversee drilling, log the soil borings,
and collect soil samples. Soil samples were collected continuously to groundwater. All
recovered soil cores were visually classified, and inspected for staining and odors, and then
were screened on approximate six-inch intervals and at stratigraphic breaks for volatile organic
vapors using a photo-ionization detector (PID) equipped with a 10.2 electron-volt lamp. The PID
was calibrated daily, prior to the start of work. Subsurface conditions at the Site have been
documented on the soil boring logs provided in Appendix A.
2.3.1 Soil Sampling
A total of 24 samples (two per borings, a shallow sample (0.5 to 2 feet below groundsurface (ft-
bgs) and a deep sample (generally one to two feet above first encountered wet soil conditions if
wet conditions were encountered in the upper 10 to 15 feet of the soil column, otherwise soil
samples were collected from the 10 to 12 ft-bgs)) were collected for laboratory analysis of
volatile organic compounds (VOCs), semi-volatile organic compounds (SVOCs), total petroleum
hydrocarbons (TPH) for gasoline range organics (GRO) and diesel range organics (DRO),
metals (see list below). The shallow sample (i.e., 0.5 to 2 ft-bgs) was also analyzed for
polychlorinated biphenyls (PCBs) during the initial round of sampling.
Seven additional soil samples were then collected for analysis of selenium (B2A (0.5 to 2 ft-
bgs), MW3A (1.5 to 2 ft-bgs and 11 to 12 ft-bgs), MW5A (0.5 to 2 ft-bgs) and chromium
speciation (B2A (0.5 to 2 ft-bgs and 11 to 12 ft-bgs), B6A (1 to 2 ft-bgs and 10.5 to 11.5 ft-bgs),
MW3A (1.5 to 2 ft-bgs) and MW5A (0.5 to 2 ft-bgs).
Laboratory methods used for Phase II ESA soil analytical program are presented below:
VOCs by United States Environmental Protection Agency (EPA) Method 5035/8260;
SVOCs by EPA Method 8270;
TPH-GRO and TPH-DRO by EPA Method 8015C; follow-up samples were analyzed for
Volatile Petroleum Hydrocarbon (VPH) and Extractable Petroleum Hydrocarbons (EPH)
using Massachusetts Department of Environmental Protection (MADEP) methodologies.
The North Carolina Department of Environment and Natural Resources (NCDENR)
references the MADEP VPH/EPH methodologies.
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Select metals by EPA Method 6010 (antimony, arsenic, barium, beryllium, cadmium,
chromium, copper, lead, molybdenum, nickel, selenium, silver, tin and zinc) and EPA
method 7471 (mercury). Samples collected during the April 2011 sampling event were
all analyzed for total concentrations for chromium.
Polychlorinated Biphenyls (PCBs) by EPA Method 8080 from the shallow horizon.
Hexavalent chromium by EPA Method 7196. Soil samples were collected for hexavalent
chromium (i.e., speciation) analysis, during the June 2011 soil sampling event to assess
whether chromium detected in Site soil during the May 2011 soil sampling was
hexavalent chromium or trivalent chromium; the State standards are based on
hexavalent chromium or trivalent chromium and not total chromium. Trivalent chromium
is the difference between total chromium in soil and detected hexavalent chromium in
soil. Typically the speciation analysis is only conducted if the total chromium values
exceed the hexavalent chromium soil standards.
Samples for VOC analysis were collected first and placed in pre-weighed laboratory provided
glassware that was preset with preservation solvents in accordance with EPA Method 5035.
The remaining bottleware was then filled. Between each successive use, all downhole sampling
equipment and sample handling tools were washed in a solution of Alconox and water, followed
by a potable water rinse.
Once filled, the sample containers were sealed, labeled, and placed in an ice-filled cooler for
delivery to the testing laboratory. At the conclusion of each sampling day, sample coolers were
transported by AMEC field personnel to a Federal Express full-service facility for overnight
shipment to the AccuTest laboratory in Orlando, Florida. AccuTest is a North Carolina
registered laboratory and certified under the National Environmental Laboratory Accreditation
Program (NELAP) in North Carolina for the analytical program conducted as part of this Phase II
ESA. Chain of custody documentation was initiated at the Site and accompanied the samples
to the laboratory. Analytical results are described in Section 4.0. Laboratory analytical reports
are presented in Appendix B.
All drill cuttings and soil core remnants were contained in labeled 55-gallon steel drums for
subsequent transportation and off-site disposal by Safety-Kleen. The boreholes not completed
as monitoring wells were backfilled with a bentonite slurry.
2.3.2 Groundwater
Monitoring wells were drilled to a completion depth of approximately seven feet below presumed
water-table conditions based on the occurrence of wet soils. Monitoring wells MW-1 through
MW-5 were constructed through the HSA and monitoring wells MW-6 through MW-9 were
drilled using air-rotary techniques. Monitoring wells were constructed using 2-inch (inside
diameter (ID)) 0.01-inch machine slotted (10-slot) Schedule 40 polyvinyl chloride (PVC) 10-foot
long well screen and solid PVC screen to the ground surface. A quartz sand filter pack was
installed to a depth of approximately one foot above the top of the well screen, followed by two
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feet of bentonite chips that were hydrated in place, followed by cement/bentonite grout to the
surface. All wells were finished with flush-mount manholes, locking caps and concrete pads.
Each well screen was set to intersect the observed water table (i.e., seven feet within the
saturated zone and three feet above).
Monitoring wells were developed using a submersible pump, which was run at a high rate for
the first fifteen minutes of development with the pump being raised and lowered along the
screened interval. After 15 minutes, well development continued at a low flow rate of
approximately 500 milliliters per minute (mL/min) until water quality parameters (temperature,
pH, conductance and turbidity) stabilized (i.e., three consecutive readings within 10-percent of
the prior reading over five to seven minute intervals). Monitoring wells MW-1 through MW-5
were allowed to equilibrate for approximately 72 hours before being purged and sampled.
Monitoring wells MW-6 through MW-9 were allowed to equilibrate for six days prior to being
purged and sampled.
Groundwater samples were collected from each monitoring well, via low-flow purge and
sampling techniques. Groundwater was purged from the monitoring wells using a stainless
steel submersible pump with the intake located approximately one foot above the base of the
well. Water quality parameters were collected on four minute intervals using a flow-through cell
to monitor temperature, pH, conductivity, oxidation-reduction potential, and dissolved oxygen.
Turbidity was monitored separately. The pumping rate was maintained between 100 and 500
mL/min to maintain minimal drawdown effects and to limit suspension of sediments or aeration
of the water being sampled. Water quality parameters were recorded approximately every four
minutes. Groundwater samples were collected once water quality parameter readings had
stabilized (i.e., three consecutive readings within 10 percent of the prior reading taken at four
minute intervals).
Once water quality parameters had stabilized, the tubing was disconnected from the flow-
through cell and the laboratory provided bottleware was filled directly from the discharge tube.
A total of five samples were submitted to the laboratory for analyses of VOCs, SVOCs, TPH-
GRO and TPH-DRO and metals (for both total and dissolved analysis, filtered and unfiltered
samples, respectively). After bottleware for total (i.e., unfiltered) metals was filled, an in-line
filter (0.45-micron) was attached to the discharge tubing, and then bottleware for dissolved
analysis was filled. Laboratory methods for the groundwater analytical program are presented
below:
VOCs by EPA Method 8260;
SVOCs by EPA Method 8270, Polynuclear Aromatic Hydrocarbons (PAHs) were
analyzed using low-level SIM analytical methods;
TPH-GRO and TPH-DRO by EPA Method 8015C.
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Select metals by EPA Method 6010 (antimony, arsenic, barium, beryllium, cadmium,
chromium, copper, lead, molybdenum, nickel, selenium, silver, tin and zinc) and EPA
Method 7471 (mercury). All metals were analyzed for both total and dissolved metals.
Samples bottles for VOC analysis were filled first, followed by samples for SVOCs, TPH and
then metals. Between each successive use, the submersible pump was washed in a solution of
Liquinox and water, followed by a distilled water rinse. New, disposable, Teflon-lined tubing and
new, disposable single use, in-line filters were used at each well location.
Once filled, the sample containers were sealed, labeled, and placed in an ice-filled cooler for
delivery to the testing laboratory. At the conclusion of each sampling day, sample coolers were
transported by AMEC field personnel to either a lab courier or to a Federal Express full-service
facility for overnight shipment to the AccuTest laboratory in Orlando, Florida. Chain of custody
documentation was initiated at the Site and accompanied the samples to the laboratory.
Analytical results are described in Section 4.0. Laboratory analytical reports are presented in
Appendix B.
The first round of groundwater sampling was conducted on monitoring wells (MW-1 through
MW-5) in May 2011. Based on the findings of the May 2011 event (discussed in Section 4.2),
four additional monitoring wells were installed (MW-6 through MW-9) and sampled for VOCs
with select wells (MW-1 and MW-5) also being sampled for total (i.e., unfiltered) and dissolved
(i.e., filtered) chromium in June 2011. All subsequent groundwater sampling events were also
conducted using the low-flow purge and sampling techniques discussed above.
All purge water and decontamination water was contained in labeled 55-gallon steel drums for
subsequent transportation and off-site disposal by Safety-Kleen.
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3.0 SITE CHARACTERISTICS
3.1 Topography
The general location of the Site is shown on the United States Geologic Survey (USGS)
Charlotte East, 7.5-minute series quadrangle sheet (see Figure 1). Based on the USGS
quadrangle map, the Site is located at an elevation of approximately 740 feet above mean sea
level (amsl). The Site is relatively level, with a slight grade to the southeast. Overall, elevations
in the area of the Site decrease from northwest to southeast.
3.2 Site Soils
Soil conditions at the Site were assessed during this Phase II ESA. Soils at the Site were
generally described as being a dry orange sandy clay to approximately 2.5 ft-bgs, becoming a
green silty clay to 7.5 ft-bgs, a brown to red clay to 9.5 ft-bgs and then a gray to brown to blue
sandy silt/silty sand to the end of the boring. At some locations, weathered rock was
encountered at approximately 23 ft-bgs. Wet soil conditions were first encountered between 18
and 28.5 ft-bgs. Soil boring logs are provided in Appendix A.
Soils were screened with a PID immediately after the split-barrel sampler or macrocore liner
was opened. Soils were screened on approximate 0.5-foot intervals and along notable
stratigraphic breaks (e.g., fill to natural soil contacts). PID readings ranged from no volatile
vapors being detected (MW-4, MW-7, MW-9, B3, B6 and B7) to less than 3.6 parts per million-
air (ppm-air) in the remaining borings. Overall, the PID readings appear consistent with PID drift
and background observations
3.3 Surface Water and Groundwater
The nearest surface water feature with respect to the Site is an unnamed stream located to the
south/southwest, along the southern Site boundary. Based on local ground surface topography,
it would be expected that surface water flow would be to the south and southeast. Groundwater
flow is also expected to be towards the south and southeast based on ground surface
topography and the occurrence of surface water features in the area, with shallow groundwater
ultimately discharging into Little Sugar Creek. Little Sugar Creek is located approximately 3,500
feet to the southeast of the Site (see Figure 1).
Onsite well data indicates that groundwater is migrating onto the Site from both the north and
west-northwest (see Figures 3 and 4). This flow pattern is based on groundwater depth
measurements taken on May 2, 2011 (Figure 3) and June 16, 2011 (Figure 4). Overall,
groundwater flow patterns observed on May 2, 2011 were similar to groundwater flow patterns
observed on June 16, 2011, with a more distinct southeastern flow pattern being observed in
the southern area of the Site based on readings from MW-7, MW-9 and MW-1. Groundwater
measurements are summarized in Table 1. All groundwater elevations are based on a site-
specific datum.
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3.4 Area Groundwater Impacts
The Site is located in an area of mixed industrial and commercial use including several facilities
located both north and west of the Site, (i.e., in an upgradient orientation with respect to the
Site) that have a history of solvent use based on a search of environmental databases (see
Table 2) and a review of readily available files. Table 2 includes locations with confirmed or
suspect solvent use located in presumed upgradient orientations with repect to the Site,
although not all of the facilities listed in Table 2 have confirmed releases.
The records search identified several facilities to the north and northwest (i.e., upgradient) of the
Site with confirmed VOC impacts in soil and/or groundwater. The most notable facilities were a
former dry cleaner in the Hutchinson Shopping Center located approximately 750 feet to the
northwest of the Site, and a property with automobile and truck service bays located to the north
of the Site on the abutting property along the northeast corner of the Site. Compounds detected
in soil and/or groundwater at the former dry cleaner location in the Hutchinson Center included
PCE (soil), TCE (soil) and c1,2-DCE (soil) and vinyl chloride (soil and groundwater) and 1,2-
DCE (see Appendix C). Compounds detected in groundwater (soil samples were not analyzed
for VOCs) at the service bay property to the north were PCE, 1,1,1-TCA, 1,2-DCA and
chloroform at the abutting property with automobile and truck service bays (see Appendix D).
This property is in a likely side-gradient or potential upgradient orientation with respect to the
Site. There was also a former Department of Defense (DoD) property located approximately
1,100 feet to the west-northwest of the Site (which is being addressed by the DoD) with TCE
groundwater impacts.
AMEC also identified a December 2010 Notice of Brownfields Property with respect to the dry
cleaner in the Hutchinson Shopping Center which notes “contaminated soil and groundwater.”
This notice was approved by NCDENR and details various land use restrictions and
management of contaminated soil and groundwater. The December 2010 notice is provided in
Appendix C. As noted, the Hutchinson Shopping Center is upgradient of the Site.
The locations of these three properties, with respect to the Site, are shown on Figure 5.
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4.0 RESULTS
A summary of the analytical results for this Phase II ESA are presented below. The analytical
data for the soil samples were compared to the NCDENR Inactive Hazardous Sites Branch
(IHSB) Preliminary Soil Remediation Goals (SRGs), last updated February 2012. The NCDENR
Soil Remediation Goals (SRGs) presented below are based on a comparison of the Preliminary
Industrial Health-Based Soil Remediation Goal (IHSRG) and the Protection of Groundwater
Preliminary Site Remediation Goal (PSRG). The lower of the IHSRG and PSRG is the SRG.
The use of the IHSRG in lieu of the Preliminary Residential Health-Based Soil Remediation
Goal (PRHSRG) will result in an industrial restricted land use. For presentation purposes the
PRHSRG, the IHSRG, and the PSRG are provided in Table 3, although for the purposes of this
report the findings presented herein are based on a non-residential (industrial) Site use and
derviation of the SRG is based on a comparison of the the IHSRG to the PSRG.
Values for soil TPH were compared to NCDENR screening values. The NCDENR TPH-GRO
and DRO screening criterion for soil is 10 milligrams per Kilogram (mg/Kg).
Groundwater results were compared to the NCDENR 2L Groundwater Quality Standards (2L
Standards), effective January 1, 2010. NCDENR also implemented interim maximum allowable
concentrations for select compounds, last updated July 12, 2012.
The discussion herein references both the practical quantitation limit (PQL) and the method
detection limit (MDL). The MDL is the minimum concentration that the laboratory can measure
and report with 99 percent confidence that the analyte concentration is greater than zero. The
PQL is the lowest concentration that can be reliably reported by the laboratory within specified
limits of precision and accuracy by a given analytical method during routine laboratory analysis.
Analytes detected above the MDL, but below the PQL, are “J” flagged and referred to as
estimated concentrations. In soil, all of the organic analysis was reported to the MDL, while all
inorganic analysis (metals) was reported to the PQL. In groundwater all analytical results (both
organic and inorganic) were reported to the MDL
4.1 Soil Analytical Results
Soil analytical results for detected compounds are presented in Table 3, with the full analytical
list being presented in Appendix B, Table B-1. Laboratory analytical data-sheets are provided
in Appendix B. The following sections provide an overview of the soil sampling results.
4.1.1 Volatile Organic Compounds (VOCs)
There were no concentrations of VOCs detected in soil above the laboratory PQL. Acetone
and methyl ethyl ketone (MEK), also known as 2-butanone were reported as estimated
concentrations above the MDL, but below the PQL and below their respective SRGs. Acetone
was reported in the soil samples at both B4 (2 to 4 ft-bgs) and MW-1 (10 to 11 ft-bgs), and MEK
was reported in the MW-1 (10 to 11 ft-bgs) soil sample.
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Both acetone and MEK are considered by the EPA to be common laboratory artifacts, while
acetone can also be a field preservation artifact when EPA Method 5035 is used as the field
preservation technique. Both compounds are considered to be a laboratory artifact and/or a
sample preservation artifact and are therefore not considered to be representative of Site
conditions.
4.1.2 Semivolatile Organic Compounds (SVOCs)
There were no SVOCs detected in Site soil above the laboratory MDLs.
4.1.3 Metals
Nine of the 15 metals analyzed for were detected in soil samples at the Site. The metals
detected in Site soils were arsenic, barium, beryllium, chromium (as total chromium), copper,
lead, nickel, selenium and zinc. With the exception of arsenic, selenium and chromium, all
reported concentrations were below the SRGs (see Table 3).
The following sections discuss in greater detail the soil results for arsenic, selenium and both
total speciated chromium (i.e., total, hexavalent and trivalent).
Arsenic
Arsenic was detected in 14 of the 24 soil samples collected during the April 2011 sampling
event at concentrations ranging from 0.64 mg/Kg to 2.8 mg/Kg, with an average concentration
of 1.7 mg/Kg. The arsenic SRG is 1.6 mg/Kg. which is based on the IHSRG. Seven locations
had a concentration above the IHSRG, five in the shallow horizon and two in the deeper
horizons. There were no reported concentrations above the PSRG (5.8 mg/Kg), which is
protective of groundwater.
Arsenic concentrations in the shallow soils (0 to 2 ft-bgs) ranged from 0.83 mg/Kg to 2.8 mg/Kg
with an average concentration of 1.8 mg/Kg, while arsenic concentrations in the deeper soils (10
to 12 ft-bgs) ranged from 0.64 mg/Kg to 2.8 mg/Kg with an average concentration of 1.6 mg/Kg.
The North Carolina Department of Agriculture and Consumer Services (NCDACS), Agronomic
Division, has published a bulletin entitled Heavy Metals in North Carolina Soils, Occurrence &
Significance which reports that the average concentration of arsenic in soil in North Carolina is
4.5 parts per million (ppm), well above the average and the maximum concentrations observed
at the Site. The concentrations observed in soil samples collected from the Site are considered
reflective of background and/or naturally occurring conditions.
Selenium
Selenium was detected in 10 of the 24 samples initially collected from the Site at concentrations
ranging from 1.2 to 3.8 mg/Kg. Four of the 24 samples collected exceeded the SRG for
selenium. Each of these samples was collected from the shallow (0.5 to 2 ft-bgs) soil horizon.
Selenium results for the soil samples collected from the deeper horizon were below the SRGs.
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The SRG for selenium is based on the PSRG of 2.1 mg/Kg. The IHSRG for selenium is 78
mg/Kg.
To confirm the original results three locations that exceeded the SRG were resampled for
selenium to determine if the original results were reproducible, B2 (as sample B2A), MW-3 (as
sample MW3A) and MW-5 (as sample MW5A). The original selenium results were not
reproducible since there were no reported concentrations above the PQL.
Although four soil samples collected from the Site were above the SRG (which is based on the
PSRG), these concentrations were not reproducible and all other concentrations of selenium
above the PQL were below the SRG, and consistent across the Site; therefore, no additional
investigation is warranted. Further as noted in Section 4.2.3 below, selenium concentrations
in groundwater at the Site (both total and dissolved) were below the 2L Standards. These
results indicate that selenium present in soil at the Site is reflective of naturally occurring
conditions and has not had an adverse impact on groundwater quality at the Site.
Chromium (total, hexavalent and trivalent)
NCDENR does not provide SRGs for total chromium, but rather provides SRGs for trivalent
chromium and hexavalent chromium. Absent specific data for both trivalent and hexavalent
chromium, total chromium results must be compared to the lower hexavalent chromium SRGs.
The hexavalent chromium SRG (based on the PSRG) is 3.8 mg/Kg. The trivalent chromium
SRG (based on the IHSRG) is 100,000 mg/Kg.
Total chromium ranging from 7.8 mg/Kg to 106 mg/Kg was reported in all 24 soil samples
collected during the initial sampling event completed in April 2011. These results were above
the hexavalent chromium SRG, but below the trivalent chromium SRG. Total chromium
concentrations in the shallow soils (i.e., 0.5 to 2 ft-bgs) ranged from 14.8 mg/Kg to 105 mg/Kg
with an average concentration of 38.9 mg/Kg. Total chromium concentrations in the deeper
soils ranged from 7.8 to 106 mg/Kg with an average concentration of 31.9 mg/Kg.
To assess whether hexavalent chromium is present on-site, a subsequent round of soil
sampling was conducted in June 2011 focusing on collecting soil samples from the locations
(and associated depth intervals) generally having the higher total chromium concentrations
(based on the April 2011 results). Seven soil samples were collected for speciated chromium
analysis (i.e., total, hexavalent and trivalent) using EPA Method 7196. Hexavalent chromium
was not detected above laboratory PQL in any of the samples analyzed. These data indicate
that the soil chromium concentrations observed in Site soils are reflective of trivalent chromium
and not hexavalent chromium, and that the appropriate SRG for the Site is 100,000 mg/Kg for
which there are no exceedances
Table 3 provides the June 2011 total chromium and speciated chromium results. Based on the
historical use of the Site and the results of the speciated chromium analysis, the observed total
chromium concentrations are considered reflective of naturally occurring concentrations.
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4.1.4 Polychlorinated Biphenyls (PCBs)
There were no PCB Aroclors detected in the soil samples above the MDL. All MDLs were
below the applicable SRG.
4.1.5 Petroleum Hydrocarbons
There were no concentrations of TPH-GRO (C6-C10) above the MDL or concentrations of TPH-
DRO (C10-C28) above applicable screening levels in soils sampled at the Site.
4.2 Groundwater Analytical Results
Two groundwater sampling events were conducted at the Site, the first in May 2011 and the
second in June 2011. The May 2011 groundwater sampling event was for wells MW-1 through
MW-5 (i.e., the only wells onsite at the time). Groundwater samples collected during the May
2011 sampling event were analyzed for VOCs, SVOCs and select metals. Metals were
analyzed for both the total and the dissolved fractions (unfiltered and filtered, respectively).
Four additional wells were installed in June 2011 as a result of VOC detections above the 2L
standards in samples collected during the May 2011 groundwater sampling event. The VOCs
detected above the 2L Standards were carbon tetrachloride, 1,1-dichloroethene (1,1-DCE),
tetrachloroethylene (PCE) and trichloroethylene (TCE). All of the Site groundwater monitoring
wells (i.e., MW-1 through MW-9) were sampled for VOCs during the June 2011 groundwater
sampling event. Groundwater samples were also collected from MW-1 and MW-5 for analysis
of total and dissolved chromium. Groundwater monitoring wells MW-1 and MW-5 were
resampled for total (unfiltered) and dissolved (filtered) chromium since during the May 2011
event the total chromium results were above the total chromium 2L Standard.
There were no sheens or odors observed during monitoring well development, well purging or
groundwater sampling activities for either the May 2011 or June 2011 groundwater sampling
events.
Groundwater flow, based on the May 2, 2011 water level readings taken from MW-1 through
MW-5, was to the south-southeast (see Figure 3). Additional groundwater monitoring wells
(MW-6, MW-7 and MW-9) were installed along the western Site boundary in the southern end of
the Site to monitor groundwater flowing onto the Site in the area where PCE and TCE were
detected. Groundwater flow patterns, based on the June 16, 2011 water level readings (see
Figure 4), were similar to the May 2, 2011 groundwater patterns, with a more distinct
southeastern flow pattern being observed in the southern area of the Site based on readings
from MW-7, MW-9 and MW-1. Groundwater monitoring wells located along the upgradient Site
boundary are MW-5, MW-3, MW-6, MW-7 and MW-8. Groundwater monitoring wells located
along the downgradient Site boundary are MW-1 and MW-2.
The following sections provide an overview of the groundwater sampling results. Reporting
limits for all groundwater results reference the MDL. Analytes detected above the MDL, but
below the PQL, are “J” flagged and referred to as estimated concentrations. Compounds
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detected in groundwater are presented in Table 4. All compounds analyzed for in groundwater,
with reporting limits, are presented in Appendix B, Table B-2. Laboratory analytical data-
sheets are provided in Appendix B.
4.2.1 Volatile Organic Compounds (VOCs)
VOCs detected in groundwater at the Site include chloroform, carbon tetrachloride, 1,1-
dichloroethane (1,1-DCA), 1,1-DCE, cis-1,2-dichloroethene (c1,2-DCE), PCE and TCE of which
carbon tetrachloride, 1,1-DCE, PCE and TCE were detected above the 2L Standards.
Along the upgradient property boundary 1,1-DCA, 1,1- DCE,c1,2-DCE, PCE and TCE were
detected, with 1,1-DCE, PCE and TCE occurring at concentrations above the 2L Standards.
Chloroform, 1,1-DCA, 1,1-DCE, c1,2-DCE, PCE and TCE were detected in MW-2, located near
the downgradient edge of the Site, at concentrations similar to but slightly higher than the
concentrations observed along the upgradient Site boundary. Carbon tetrachloride was
detected in only one downgradient well. Figure 6 presents compounds detected in groundwater
above the 2L Standards. Analytical results are discussed below and presented in Table 4.
Chloroform
Chloroform was detected in groundwater sampled at wells MW-1, MW-2 and MW-8. Reported
concentrations ranged from an estimated 0.76 micrograms per Liter (µg/L) to 2.1 µg/L, with an
average concentration of 1.1 µg/L. There were no reported concentrations above the 2L
Standard for chloroform of 70 µg/L.
Carbon Tetrachloride
Carbon tetrachloride was detected in groundwater sampled at well MW-2 during both
groundwater sampling events at concentrations above the 2L Standard of 0.3 µg/L. Carbon
tetrachloride concentrations were 1.4 µg/L and 1.8 µg/L during the May 2011 and June 2011
groundwater sampling events, respectively.
1,1-DCA
Groundwater sampled at downgradient well MW-1 and upgradient wells MW-7 and MW-9 had
estimated concentrations of 1,1-DCA that ranged from 0.92 µg/L (MW-1) to 1.9 µg/L (MW-7)
with an average concentration of 1.2 µg/L. There were no reported concentrations above the
1,1-DCA 2L Standard of 6 µg/L.
1,1-DCE
Groundwater sampled at downgradient well MW-1 and upgradient wells MW-6, MW-7 and
MW-9 had concentrations of 1,1-DCE that ranged from an estimated concentration of 0.49 µg/L
(MW-6) to 16.5 µg/L (MW-7). The 1,1-DCE 2L Standard is 7 µg/L. The 2L Standard was
exceeded in samples collected from upgradient well MW-7 (16.5 µg/L) and downgradient well
MW-1 (11.2 µg/L) for samples collected during the June 2011 groundwater sampling event.
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c1,2-DCE
Groundwater sampled at downgradient well MW-1 and upgradient wells MW-7 and MW-9 had
concentrations of c1,1-DCE that ranged from 18.5 µg/L (MW-9) to 47.4 (MW-7) with an average
concentration of 27.2 µg/L. There were no reported concentrations above the c1,2-DCE 2L
Standard of 70 µg/L.
PCE
Groundwater sampled at downgradient well MW-1 and upgradient wells MW-5, MW-7 and
MW-9 had concentrations of PCE that ranged from an estimated concentration of 0.29 µg/L
(MW-5) to 111 µg/L (MW-1). The PCE 2L Standard is 0.7 µg/L.
The PCE 2L Standard was exceeded in samples collected from upgradient wells MW-7
(103 µg/L) and MW-9 (5.6 µg/L), and in downgradient well MW-1 (71.6 µg/L and 111 µg/L
during the May 2011 and June 2011 sampling events, respectively). Wells MW-6 through MW-9
were installed after the May 2011 sampling event. PCE was not detected in well MW-5 during
the June 2011 sampling event.
TCE
Groundwater sampled at downgradient wells MW-1 and MW-2 and upgradient wells MW-6,
MW-7 and MW-9 had concentrations of TCE that ranged from an estimated concentration of
0.77 µg/L (MW-2) to 143 µg/L (MW-1). The TCE 2L Standard is 3 µg/L.
The TCE 2L Standard was exceeded in samples collected from upgradient wells MW-6 (17.7
µg/L) and MW-9 (90.1 µg/L) and downgradient well MW-1 (104 µg/L and 143 µg/L during the
May 2011 and June 2011 sampling events, respectively). Wells MW-6 through MW-9 were
installed subsequent to the May 2011 sampling event.
Methylene Chloride
Methylene chloride was reported in the groundwater sample collected from MW-1; however, the
laboratory quantified this result as being a laboratory artifact. Therefore, the reporting of
methylene chloride by the analytical laboratory is not considered to be representative of Site
conditions.
Summary
The Site was undeveloped woodland until 1986, at which time it was developed for use by TFS
for an over-the-road-trailer leasing business. Chlorinated solvents have been identified in soil
and groundwater at facilities located upgradient of the Site (see Section 3.4). In addition to
parent products such as PCE and TCE and 1,1,1-TCA, chlorinated solvent degradation
products such as c1,2-DCE, 1,1DCE and vinyl chloride have been detected in groundwater both
locally and in onsite wells. However, the VOCs detected in groundwater were not detected in
Site soil either as parent product or as degradation products. These findings indicate that the
VOCs detected in groundwater at the Site are likely from an upgradient source and not the TFS
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Site.
Historically, carbon tetrachloride has been used to make refrigeration fluids, propellants for
aerosols, as an industrial cleaning fluid. Carbon tetrachloride was also one of the original dry
cleaning fluids. Other uses of carbon tetrachloride included use as a pesticide to kill insects in
grain. Most uses of carbon tetrachloride were discontinued in the 1960s, while the use of
carbon tetrachloride as a pesticide was stopped in the mid-1980s (ATSDR, 2005). Carbon
tetrachloride was detected in one well on site, but not in Site soils. It is unlikely that the
identified carbon tetrachloride is a result of TFS operations.
4.2.2 Semivolatile Organic Compounds (SVOCs)
There were no SVOCs detected in groundwater sampled at the Site above the laboratory MDL.
4.2.3 Metals
Groundwater samples were analyzed for PPL-Metals plus barium and tin, with all samples being
collected for analysis for the total fraction and the dissolved fraction. The total fraction is
conducted on unfiltered samples; therefore the analytical result could be biased high due to
metals being analyzed that were associated with sediments entrained in the groundwater
sample. The dissolved fraction undergoes filtering to remove sediments in the sample matrix
prior to analysis. NCDENR recognizes only the total (i.e. unfiltered) analysis for comparison to
the 2L Standards. The dissolved fraction was collected for analysis for information purposes
only.
Total chromium was the only metal detected above 2L Standards. The total chromium 2L
Standard was exceeded in MW-1 and MW-5 during the May 2011 groundwater sampling event.
There were no exceedences of total chromium in wells MW-1 and MW-5 during the June 2011
groundwater sampling event. As discussed below, other metals detected in groundwater
(based on total concentrations) were barium, chromium, copper, lead, nickel, mercury, nickel,
selenium and zinc. Metals detected in groundwater based on dissolved (or filtered)
concentrations were barium, chromium, copper, nickel, mercury, nickel, selenium and zinc.
Lead was not detected in the dissolved (i.e., field-filtered) fraction. Analytical results are
discussed below and presented in Table 4.
Barium
Barium (total) was detected in wells MW-1 through MW-5 (during the May 2011 groundwater
sampling event) at concentrations ranging from 36.2 µg/L to 146 µg/L with an average
concentration of 77.2 µg/L. The barium 2L Standard is 700 µg/L. There were no exceedences
of the 2L Standard for barium
Barium (dissolved) was detected in wells MW-1 through MW-5 (during the May 2011
groundwater sampling event) at concentrations ranging from 26.5 µg/L to 56.7 µg/L with an
average concentration of 37.4 µg/L.
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Chromium
The chromium 2L Standard of 10 µg/L is based on the total (i.e. unfiltered) sample. Unlike soil,
there are no hexavalent or trivalent (i.e., speciated) chromium 2L Standards.
During the May 2011 groundwater sampling event, total chromium was detected in groundwater
at all five locations (MW-1 through MW-5) at concentrations ranging from 3.6 µg/L to 93.8 µg/L
with an average concentration of 34.7 µg/L. The chromium 2L Standard is 10 µg/L. The 2L
Standard was exceeded in groundwater samples from two wells only, wells MW-1 (63.3 µg/L)
and MW-5 (93.8 µg/L). Total chromium concentrations in wells MW-2, MW-3 and MW-4 ranged
from an estimated concentration of 5 µg/L (MW-2) to 7.7 µg/L (MW-3).
Wells MW-1 through MW-5 were also sampled for dissolved chromium and the reported
concentrations ranged from an estimated concentration of 1.4 µg/L to 34 µg/L with an average
concentration of 9.7 µg/L. Dissolved chromium was not detected in well MW-4. The dissolved
concentrations in MW-1 (estimated at 1.4 µg/L), MW-2 (estimated at 1.4 µg/L) and MW-3
(estimated at 1.9 µg/L) were below the 2L Standard. The only dissolved sample having a
concentration above the 2L Standard was MW-5 (34 µg/L).
Wells MW-1 and MW-5 were resampled for both total and dissolved chromium during the June
2011 groundwater sampling event. There were no reported exceedences in either the total or
dissolved fractions for chromium during the June 2011 sampling event at either MW-1 or MW-5.
The total concentrations in MW-1 and MW-5 were estimated concentrations of 7.8 µg/L and 5.4
µg/L, respectively. The dissolved concentrations were estimated concentrations of 1.8 µg/L and
1.9 µg/L in MW-1 and MW-5, respectively. During the May 2011 groundwater sampling event,
while the samples appeared to be relatively clear (as compared to the initial observations at the
start-up of sampling), the stabilized Nephelometric Turbidity Units (NTUs) for MW-1 and MW-5
were 97.3 NTUs and 79.4 NTUs, respectively. During the June 2011 sampling event, the
stabilized NTUs at MW-1 and MW-5 were 27 and 8.5 NTUs, respectively. Therefore the
elevated chromium readings at MW-1 and MW-5 during the May 2011 groundwater sampling
event are attributed to being turbidity related.
Copper
Copper (total) was detected in wells MW-1 through MW-5 (during the May 2011 groundwater
sampling event) at concentrations ranging from 4.4 µg/L to 36.6 µg/L with an average
concentration of 18 µg/L. The copper 2L Standard is 1,000 µg/L. There were no exceedences
of the 2L Standard for copper
Copper (dissolved) was detected in well MW-3 (during the May 2011 groundwater sampling
event) at an estimated concentration of 6 µg/L.
Lead
Lead (total) was detected in wells MW-3, MW-4 and MW-5 (during the May 2011 groundwater
sampling event) at concentrations ranging from an estimated concentration of 1.8 µg/L to 6.4
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µg/L with an average concentration of 3.5 µg/L. The lead 2L Standard is 15 µg/L. There were
no exceedences of the 2L Standard for lead.
Lead was not detected in the dissolved fraction.
Mercury
Mercury (total) was detected in well MW-5 (during the May 2011 groundwater sampling event)
at an estimated concentration of 0.11 µg/L. The mercury 2L Standard is 1 µg/L. There were no
exceedences of the 2L Standard for mercury.
Mercury (dissolved) was detected in wells MW-3 and MW-4 (during the May 2011 groundwater
sampling event) at estimated concentrations of 0.05 µg/L and 0.07 µg/L, respectively.
Nickel
Nickel (total) was detected in wells MW-1 through MW-5 (during the May 2011 groundwater
sampling event) at estimated concentrations ranging from 2.2 µg/L to 31.3 µg/L with an average
concentration of 13.6 µg/L. The nickel 2L Standard is 100 µg/L. There were no exceedences of
the 2L Standard for nickel.
Nickel (dissolved) was detected in wells MW-2, MW-3, and MW-5 (during the May 2011
groundwater sampling event) at an estimated concentrations ranging from 2.4 µg/L to 2.9 µg/L
with an average concentration of 2.7 µg/L.
Selenium
Selenium (total) was detected in wells MW-4 and MW-5 (during the May 2011 groundwater
sampling event) at estimated concentrations ranging 3.5 µg/L and 2.6 µg/L, respectively. The
selenium 2L Standard is 20 µg/L. There were no exceedences of the 2L Standard for selenium.
Selenium was not detected in the dissolved fraction.
Zinc
Zinc (total) was detected in wells MW-1 through MW-5 (during the May 2011 groundwater
sampling event) at concentrations ranging from 18.2 µg/L to 80.1 µg/L with an average
concentration of 36.8 µg/L. The zinc 2L Standard is 1,000 µg/L. There were no exceedences of
the 2L Standard for zinc.
Zinc (dissolved) was detected in wells MW-1 through MW-5 (during the May 2011 groundwater
sampling event) at concentrations ranging from 9.4 µg/L to 22 µg/L with an average
concentration of 14.4 µg/L.
4.2.4 Petroleum Hydrocarbons
TPH-GRO was detected in one sample (MW-1 during the May 2011 groundwater sampling
event) at a concentration of 0.105 milligrams per Liter (mg/L). There were no gasoline related
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compounds in the VOC or SVOC fraction detected in groundwater sampled at MW-1 above the
MDL. NCDENR does not have a screening criteria for TPH-GRO; however, since the sample
was also analyzed for the full VOC and SVOC fraction, and no petroleum related constituents
were detected, no additional analysis is considered warranted
TPH-DRO was not detected in groundwater sampled at the Site.
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5.0 SUMMARY OF FINDINGS
The Site is owned by TFS as Transport International Pool, Inc. however, TFS no longer
occupies the Site and the Site is currently vacant. The Site was used by TFS from 1986 to 2011
as a branch location for the leasing, parking, storage, and minor repair of over-the-road trailers.
Minor repairs and typical maintenance included skin repair, hub oil changes, tire changes, brake
cleaning and change outs, and service to refrigerated units. Prior to 1986 the property was
undeveloped woodland.
The Site is located in an area with mixed industrial and commercial use, with several industrial
and commercial establishments located both north and west of the Site, i.e., in an upgradient
orientation with respect to the Site and within a half mile of the Site. A number of these
upgradient Sites have a history of solvent use and confirmed impacts to soil and groundwater
based on a search of environmental databases and review of readily available reports.
This Phase II ESA was conducted in two phases. The initial phase consisted of collecting soil
samples at 12 boring locations, with two soil samples collected from each boring for analysis of
VOCs, SVOCs, total petroleum hydrocarbons (TPH) for GRO and DRO, and Priority Pollutant
List Metals plus barium and tin. Samples were collected from a shallow interval (generally 0.5
to 2 ft-bgs) and a deeper interval (approximately one to two feet above the observed water-table
if wet soil conditions were encountered in the upper 10 to 15 feet of the soil column, otherwise
soil samples were collected from the 10 to 12 ft-bgs). Additionally, a shallow soil sample was
collected from each boring for analysis of PCBs.
Five of the soil borings were converted into monitoring wells, the remaining borings were
backfilled with a cement/bentonite slurry. Soils not used for laboratory analysis were drummed
for offsite disposal by Safety-Kleen.
The monitoring wells were developed and later, purged and sampled for VOCs, SVOCs and
metals (both total and dissolved). Based on the results of the initial round of groundwater
sampling, during which VOCs were detected, four additional wells were installed to assess if
onsite sources existed, and to assess groundwater conditions along the upgradient Site
boundary.
The analytical data for the soil samples were compared to the NCDENR Inactive Hazardous
Sites Branch (IHSB) Preliminary Soil Remediation Goals (SRGs), last updated February 2012.
The NCDENR Soil Remediation Goals (SRGs) are based on a comparison of the Preliminary
Industrial Health-Based Soil Remediation Goal (IHSRG) and the Protection of Groundwater
Preliminary Site Remediation Goal (PSRG). The lower of the IHSRG and PSRG is the SRG.
The use of the IHSRG in lieu of the Preliminary Residential Health-Based Soil Remediation
Goal (PRHSRG) will result in an industrial restricted land use.
Values for soil TPH were compared to NCDENR screening values. The NCDENR TPH-GRO
and DRO screening criterion for soil is 10 milligrams per Kilogram (mg/Kg).
Phase II Environmental Site Assessment
Trailer Fleet Services
Charlotte North Carolina Branch
August 2012
-20-
Groundwater results were compared to the NCDENR 2L Groundwater Quality Standards (2L
Standards) last updated January 1, 2010 with interim standards for select compounds being
updated July 12, 2012.
The following was identified based on the findings of this Phase II ESA:
Soils
Soils encountered during drilling were generally sandy clays to approximately 7.5 ft-bgs,
clay to 9.5 ft-bgs and then sandy silt/silty sand to the total depth of the boring. At some
locations, weathered rock was encountered at approximately 23 ft-bgs.
With the exception of acetone and methyl ethyl ketone (MEK) VOCs were not detected
in Site soils. Both acetone and MEK were below their respective SRG and reported as
estimated concentrations (i.e., below the laboratory PQL, but above the MDL). Both
MEK and acetone are considered laboratory and/or field preservation artifacts and not
representative of Site conditions.
No SVOCs were detected in Site soils.
No TPH-GRO, TPH-DRO or PCBs were detected in Site soils.
Metals detected in soils included arsenic, barium, chromium, copper, lead, nickel,
selenium and zinc, of which arsenic, chromium and selenium were detected above the
NCDENR SRGs. NCDENR does not have an SRG for total chromium; therefore, total
chromium results were compared to the hexavalent chromium SRG.
Reported total chromium concentrations in soils were above the hexavalent chromium
SRG, but below the trivalent chromium SRG. To confirm the reported total chromium
was not comprised of hexavalent chromium, the five sample locations with the highest
total chromium concentrations were resampled and analyzed specifically for hexavalent
chromium. Hexavalent chromium was not detected in the samples analyzed. Based on
the absence of hexavalent chromium in the samples analyzed and the Site history (no
industrial past and no confirmed fill materials), the chromium concentrations observed at
the Site were compared to the trivalent chromium SRG and there were no exceedences
to the trivalent chromium SRG. Therefore, based on the noted conditions, the presence
of chromium is considered to be representative of naturally occurring conditions and no
additional investigation is warranted.
Arsenic concentrations across the Site were generally consistent both horizontally and at
depth, and were below the average arsenic concentration in North Carolina of 4.5 mg/Kg
as reported by the North Carolina Department of Agriculture and Consumer Services
(NCDACS, 2008). Arsenic concentrations ranged from 0.64 mg/Kg to 2.8 mg/Kg with an
average concentration of 1.7 mg/Kg. The arsenic concentrations observed at the Site
are considered representative of background and/or naturally occuring conditions.
Selenium was detected a concentrations ranging from 1.2 mg/Kg to 3.8 mg/Kg with an
average concentration of 2.3 mg/Kg as compared to the SRG of 2.1 mg/Kg. The
Phase II Environmental Site Assessment
Trailer Fleet Services
Charlotte North Carolina Branch
August 2012
-21-
locations with selenium exceedences were resampled to confirm the results from the first
sampling event. The original results could not be reproduced. Therefore, there were no
exceedences of the selenium SRG, and the presence of selenium is considered to be
reflective of naturally occurring conditions. Therefore, no additional investigation is
warranted.
Groundwater
Wet soil conditions were first encountered between 18 and 28.5 ft-bgs. Based on water
levels observed in onsite groundwater monitoring wells, groundwater flows onto the Site
from the north and west and generally flows toward the south and then southeast in the
southern portion of the Site. Based on the southeast flow direction monitor wells MW-6,
MW-7 and MW-9 are considered upgradient wells for Site in the southern end of the Site
and MW-5 is an upgradient well in the northern portion of the Site. Therefore, properties
to the north and west are considered to be in an upgradient orientation with respect to
the Site.
VOCs detected in groundwater samples from the Site include chloroform, carbon
tetrachloride, 1,1-dichloroethane (1,1-DCA), 1,1-dichloroethene (1,1-DCE), cis-1,2-
dichloroethene (c1,2-DCE), tetrachloroethene (PCE) and trichloroethylene (TCE), of
which only carbon tetrachloride, 1,1-DCE, PCE and TCE were above the NCDENR 2L
Standards. TCE, 1,1- DCE, and PCE were detected in samples from upgradient wells
as well as in samples from downgradient well MW-1 at similar, but slightly higher
concentrations. Carbon tetrachloride was detected in only one downgradient well.
Based on the distribution of 1,1-DCE, PCE and TCE observed in groundwater in
upgradient wells, the absence of these constituents in Site soils, the industrial nature of
the surrounding properties and the potential sources for these constituents upgradient of
the Site, it is likely that the presence these constituents in Site groundwater are the
result of an upgradient source.
Carbon tetrachloride was detected in groundwater samples collected from downgradient
well MW-2, but not in any other wells on the property. Carbon tetrachloride was a
cleaning and refrigeration solvent phased out from use in the mid-1980s. The Site was
first developed by TFS in 1986 and there were no fill materials observed on the Site.
Based on the date TFS first occupied the site, 1986, and the fact that carbon
tetrachloride was not detected in Site soils, it is unlikely that the carbon tetrachloride
detected in groundwater is the result of Site operations.
No SVOCs were detected in groundwater samples collected from the Site.
No TPHs were detected groundwater samples collected from the Site
Total chromium was the only metal detected above the chromium 2L Standard in
groundwater samples collected from the Site. The 2L Standards for metals are based
on total (i.e., unfiltered) samples. Total chromium (above the 2L Standard) was detected
in both filtered and non-filtered samples from wells, MW-1 and MW-5, during the initial
Phase II Environmental Site Assessment
Trailer Fleet Services
Charlotte North Carolina Branch
August 2012
-22-
round of groundwater sampling, possibly due to turbidity in the newly installed wells. A
second round of samples were collected from wells MW-1 and MW-5 and analyzed for
both total and dissolved chromium. The chromium results from the second sampling
event (both filtered and non-filtered) were below the laboratory Practical Quantitation
Limit (PQL) and did not exceed the 2L Standards in either well.
Following the completion of the Phase II ESA sampling activities and as a result of VOC
detections in groundwater, AMEC conducted a records search for nearby dry cleaners
and industrial facilities in the area of the Site. The records search identified several
facilities to the north and northwest (upgradient) of the Site with confirmed VOC impacts
in soil and/or groundwater. The nearest facilities, with respect to the Site, are a former
dry cleaner in the Hutchinson Shopping Center located approximately 750 feet to the
northwest of the Site, and property with automobile and truck service bays located to the
north of the Site on the abutting property along the northeast corner of the Site.
Compounds detected in soils and/or groundwater at the former dry cleaner location in
the Hutchinson Center included PCE (soil), TCE (soil) and c1,2-DCE (soil) and vinyl
chloride (soil and groundwater) and 1,2-DCE at the former dry cleaner in the Hutchinson
Shopping Center. Compounds detected in groundwater (soil samples were not analyzed
for VOCs) at the property to the north with automotive and truck service bays were PCE,
1,1,1-TCA, 1,2-DCA and chloroform. This property is in a likely side-gradient or potential
upgradient orientation with respect to the Site. AMEC also identified a former DoD
facility, located approximately 1,100 feet to the west-northwest of the Site, with VOC
(i.e., TCE) impacts to groundwater.
Phase II Environmental Site Assessment
Trailer Fleet Services
Charlotte North Carolina Branch
August 2012
-24-
7.0 REFERENCES
EDR (2011), The EDR Radius Map™ Report with GeoCheck®, GE Multi-Site Portfolio, 1906
Bancroft Street, Charlotte, NC 28206, Inquiry Number: 2974164.138s, Environmental Data
Resources Inc, Milford, CT, January 25, 2011
ESE (1997), Site Characterization Assessment, BellSouth Work Center, 24th Street, Charlotte,
North Carolina, ESE Job Number 2597331, T0400, prepared for NCDEHNR, Mooresville, North
Carolina, prepared by ESE Engineering, P.C., Charlotte, North Carolina, June 25, 1997
NCDENR (2012), Inactive Hazardous Sites Program, Guidelines for Assessment and Cleanup,
North Carolina Department of Environment and Natural Resources, updated February 2012.
NCDACS (2008), Heavy Metals in North Carolina Soils, Occurrence & Significance, North
Carolina Department of Agriculture and Consumer Services.
FIGURES
0 2000 4000
Approximate scale in Feet
Reference:
1988 Charlotte East
7.5-minute Series
Quadrangle Sheet
Contour interval 10 feet
TFS Charlotte Branch Location
Phase II Environmental Site Assessment
1906 Bancroft Street, Charlotte
Mecklenburg County, North Carolina
AMEC Project #: 572260702
Figure 1 – Site Location Map
Environment & Infrastructure, Inc.
502 West Germantown Pike, Suite 850
Plymouth Meeting PA 19462
SITE
TFS Branch Location
Phase II Environmental Site Assessment
1906 Bancroft
Charlotte, North Carolina
AMEC Project #: 572260702
Figure 2
Exploration Locations
Environment & Infrastructure, Inc.
502 West Germantown Pike, Suite 850
Plymouth Meeting PA 19462
ref: www.maps.google.com
Boring location
Monitoring well location
B2
B4
B5
B3
B1
B6
B7
MW‐9
MW‐8
MW‐7
MW‐6
MW‐4
MW‐3
MW‐5
MW‐2
MW‐1
0 50 100
Approximate Scale in Feet
Figure 3
Groundwater Contours - 5/2/11
Environment & Infrastructure, Inc.
502 West Germantown Pike, Suite 850
Plymouth Meeting PA 19462
0 50 100
Approximate Scale in Feet
TFS Branch Location
Phase II Environmental Site Assessment
1906 Bancroft
Charlotte
Mecklenburg County, North Carolina
AMEC Project #: 572260702
MW‐4
83.38
MW‐5
88.66
MW‐3
85.86
MW‐2
80.99
MW‐1
80.97
ref: www.maps.google.com
Monitoring well
MW‐1
80.13
Monitoring Well ID
Groundwater Elevation
Groundwater Flow Direction
TFS Branch Location
Phase II Environmental Site Assessment
1906 Bancroft
Charlotte
Mecklenburg County, North Carolina
AMEC Project #: 572260702
Figure 4
Groundwater Contours – 6/16/11
Environment & Infrastructure, Inc.
502 West Germantown Pike, Suite 850
Plymouth Meeting PA 19462
0 50 100
Approximate Scale in Feet
ref: www.maps.google.com
Monitoring well
MW‐1
80.13
MW‐5
87.96
MW‐1
80.13
MW‐9
81.97
MW‐7
82.05
MW‐8
82.19
MW‐6
82.55
MW‐3
84.58
MW‐4
82.68
MW‐2
80.11
Monitoring Well ID
Groundwater Elevation
Groundwater Flow Direction
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Phase II Environmental Site Assessment
1906 Bancroft
Charlotte
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AMEC Project #: 572260702
Figure 6
Groundwater Exceedences 6/16/11
Environment & Infrastructure, Inc.
502 West Germantown Pike, Suite 850
Plymouth Meeting PA 19462
0 50 100
Approximate Scale in Feet
ref: www.maps.google.com
Monitoring well
µg/L micrograms per Liter
MW‐5
MW‐8
MW‐3
MW‐4
MW‐1
ug/L Conc Criteria
11DCE 11.2 7
PCE 111 0.7
TCE 143 3
MW‐2
ug/L Conc Criteria
Carbon Tet 1.8 0.3
MW‐6
ug/L Conc Criteria
TCE 17.7 3
MW‐7
ug/L Conc Criteria
11DCE 16.5 7
PCE 103 0.7
TCE 90.1 3
MW‐9
ug/L Conc Criteria
PCE 5.6 0.7
TCE 2.9 3
TABLES
Table 1
Depth to Groundwater/Groundwater Elevations
1906 Bancroft Street
Charlotte, Mecklenburg County, North Carolina
Location
Ground
Elevation(
1)
TOR
Elevation(
1)
Depth to
Water(2)
05/02/2011
Groundwater
Elevation(1)
05/02/2011
Depth to
Water(2)
06/16/2011
Groundwater
Elevation(1)
06/16/2011
MW-1 88.41 88.18 7.21 80.97 8.05 80.13
MW-2 89.41 89.12 8.13 80.99 9.01 80.11
MW-3 100.74 100.30 14.44 85.86 15.72 84.58
MW-4 94.77 94.39 11.01 83.38 11.71 82.68
MW-5 104.38 104.06 15.40 88.66 16.10 87.96
MW-6 98.25 97.97 -- -- 15.42 82.55
MW-7 92.90 92.46 -- -- 10.41 82.05
MW-8 95.75 95.44 -- -- 13.25 82.19
MW-9 90.00 89.69 -- -- 7.72 81.97
TOR: Top of well PVC well riser
(1) Elevation based on site-specific datum
(2) feet below TOR
-- Indicates well not installed for May 2, 2011 groundwater sampling event
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APPENDIX A
Client: TIP - Trailer Fleet Services
Project Number: 572260702
Site Location: 1906 Bancroft St., Charlotte, NC
Coordinates: LS Elevation: Sheet: 1 of 1
Drilling Method: GeoProbe Monitoring Well Installed: No
Sample Type(s): Grab Boring Diameter: Screened Interval: NA
Weather: Sunny, 90's, Humid Logged By: AK Date/Time Started: 6/9/11 1245 Depth of Boring: 12 ft-bgs
Drilling Contractor: SAEDACCO L.S. Elevation:Date/Time Finished: 6/9/11 1315 Water Level: not encountered
BORING ID: B2A
Drilling Contractor: SAEDACCO L.S. Elevation: Date/Time Finished: 6/9/11 1315 Water Level: not encountered
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)
MATERIALS: Color, size, range, MAIN COMPONENT, minor
component(s), moisture content, structure, angularity, maximum grain size,
odor, and Geologic Unit (If Known)
coarse to fine sandy GRAVEL
1.3 Brownish red silty medium to fine SAND, no odor, dry
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1 1.4 B2A/0.5-2
2.9
1.2
0.6
1.0
0.5
2
1
Marbled red and yellow silty medium to fine SAND, no odor, dry
4
3
0.1
0.2 Reddish brown fine sandy SILT, no odor, soft, moist
8
7
6
5
0.3
0
0.2
0.6
0.4
0.9 Light brown silty fine SAND, no odor, moist B2A/11-12
1.5
11
10
Boring terminated at 12 ft bgs
12
9
13
14
15
16
Boring terminated at 12 ft-bgs
17
18
19
16
Date Time Depth to groundwater while drilling
NOTES:ft-bgs: feet below ground surface
PID: Photo-ionization Detector
ppm-air: volatile organic vapors in parts per milltion - air
Client: TIP - Trailer Fleet Services
Project Number: 572260702
Site Location: 1906 Bancroft St., Charlotte, NC
Coordinates: LS Elevation: Sheet: 1 of 1
Drilling Method: GeoProbe Monitoring Well Installed: No
Sample Type(s): Grab Boring Diameter: Screened Interval:
Weather: Sunny, 90's, Humid Logged By: TH Date/Time Started: 6/9/11 1235 Depth of Boring: 12 ft-bgs
Drilling Contractor: SAEDACCO L.S. Elevation:Date/Time Finished: 6/9/11 1255 Water Level: not encountered
BORING ID: B6A
Drilling Contractor: SAEDACCO L.S. Elevation: Date/Time Finished: 6/9/11 1255 Water Level: not encountered
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MATERIALS: Color, size, range, MAIN COMPONENT, minor
component(s), moisture content, structure, angularity, maximum grain size,
odor, and Geologic Unit (If Known)
0 coarse to fine sandy GRAVEL
0 red clay, moist
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1 0 B6A/1-2
0.1 Red/yellow marbled clayey SILT, moist
0.1
0
0.0
0.1
1
2
3
4
Tan gravelly SILT, dry
0
0
5
6
7
8
0 Orange/yellow marbled clayey SILT, moist
0.1
0.1
0.3
0.1
0 Orange clayey SILT, moist B6A/10.5-11.5
0
9
10
11
12
13
14
15
16
19
16
17
18
Date Time Depth to groundwater while drilling
NOTES:ft-bgs: feet below ground surface
PID: Photo-ionization Detector
ppm-air: volatile organic vapors in parts per milltion - air
Client: TIP - Trailer Fleet Services
Project Number: 572260702
Site Location: 1906 Bancroft St., Charlotte, NC
Coordinates: LS Elevation: Sheet: 1 of 1
Drilling Method: GeoProbe Monitoring Well Installed:
Sample Type(s): Grab Boring Diameter: Screened Interval:
Weather: Sunny, 90's, Humid Logged By: TH Date/Time Started: 6/9/11 1310 Depth of Boring: 12 ft-bgs
Drilling Contractor: SAEDACCO L.S. Elevation:Date/Time Finished: 6/9/11 1340 Water Level: not encountered
BORING ID: MW-3A
Drilling Contractor: SAEDACCO L.S. Elevation: Date/Time Finished: 6/9/11 1340 Water Level: not encountered
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MATERIALS: Color, size, range, MAIN COMPONENT, minor
component(s), moisture content, structure, angularity, maximum grain size,
odor, and Geologic Unit (If Known)
coarse to fine sandy GRAVEL
0.4 Orange, clayey SILT, moist
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Well Schematic
1 4.6 Orange/yellow marbled clayey SILT
1.3 MW-3A/1.5-2
0.9
0.8
0.3
0.5
1
2
3
4
Orange clayey SILT, moist
0
0
5
6
7
8
0.1
0
0
0
0
0 MW-3A/11-12
0
9
10
11
12
13
14
15
16
19
16
17
18
Date Time Depth to groundwater while drilling
NOTES:ft-bgs: feet below ground surface
PID: Photo-ionization Detector
ppm-air: volatile organic vapors in parts per milltion - air
Client: TIP - Trailer Fleet Services
Project Number: 572260702
Site Location: 1906 Bancroft St., Charlotte, NC
Coordinates: LS Elevation: Sheet: 1 of 1
Drilling Method: GeoProbe Monitoring Well Installed:
Sample Type(s): Grab Boring Diameter: Screened Interval:
Weather: Sunny, 80's, Humid Logged By: AK Date/Time Started: 6/9/11 0920 Depth of Boring: 4 ft-bgs
Drilling Contractor: SAEDACCO L.S. Elevation:Date/Time Finished: 6/9/11 1010 Water Level: not encountered
BORING ID: MW-5A
Drilling Contractor: SAEDACCO L.S. Elevation: Date/Time Finished: 6/9/11 1010 Water Level: not encountered
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MATERIALS: Color, size, range, MAIN COMPONENT, minor
component(s), moisture content, structure, angularity, maximum grain size,
odor, and Geologic Unit (If Known)
coarse to fine sandy GRAVEL
Orangish red silty fine SAND, no odor, dry
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Well Schematic
1 1.4 MW-5A/0.5-2
5.2
4.3
4.3 Orangish red, clayay SILT, no odor, dry
0.9
0.8
1
2
3
Boring terminated at 4 ft-bgs4
5
6
7
8
9
10
11
12
13
14
15
16
18
19
16
17
Date Time Depth to groundwater while drilling
NOTES:ft-bgs: feet below ground surface
PID: Photo-ionization Detector
ppm-air: volatile organic vapors in parts per milltion - air
Checked by ______________________________Date:________________
Client: TIP - Trailer Fleet Services
Project Number: 572260702
Site Location: 1906 Bancroft St., Charlotte, NC
Coordinates: LS Elevation: Sheet: 1 of 1
Drilling Method: Hollow Stem Auger/Split-Spoon Monitoring Well Installed:
Sample Type(s): Grab Boring Diameter: Screened Interval: 15 - 25 ft-bgs
Weather: Logged By: BE Date/Time Started: 4/27/11 Depth of Boring: 25 ft-bgs
Drilling Contractor: SAEDACCO L S Elevation:Date/Time Finished: 4/27/11 Water Level:19 ft bgs
BORING ID: MW-1
Drilling Contractor: SAEDACCO L.S. Elevation: Date/Time Finished: 4/27/11 Water Level: 19 ft-bgs
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MATERIALS: Color, size, range, MAIN COMPONENT, minor
component(s), moisture content, structure, angularity, maximum grain size,
odor, and Geologic Unit (If Known)
2.7 coares to fine sandy GRAVEL
2.9 dry, orange sandy Clay
27 MW 1/0 5 2
Well Schematic
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Flushmount manhole in concrete pad
1 2.7
3.1
3.1
3.1 dry, white gravelly coarse to fine SAND
3.1 dry, green silty CLAY
3.1
3.1
3.1 - orange band
3.1
31
MW-1/0.5-21
Cement/Bentonite Grout
2
3
4
5
6 3.1
3.1
3.3 - gray becoming brown
3.1
3.1
3.1
3.1
3.1 - dry, red CLAY
3.3
3.3
*(no recovery 11 5 to 13)
MW-1/10-11
7
8
9
10
11 (no recovery 11.5 to 13)
*
*
*
3.1 dry, brown to blue layered sandy CLAY
3.1
3.1 3.1
3.4
3.4
3.6
15
16
Bentonite Seal12
13
14
3.6
3.4
3.4 dry, brown sandy SILT
3.4
3.4▼*
*
*
*
*
- wet
20
21
17
18
19 Gravel Pack
*
*
*
*
*
*
*
NOTES:ft-bgs: feet below ground surface; PID: Photo-ionization Detector; ppm-air: parts per million-air; * indicated no reading Date Time Depth to groundwater while drilling
Well Construction:4/27/2011 19 ft-bgs
Bottom Cap
Boring terminated at 25 ft-bgs
22
23
24
25
2-inch ID Schedule 40 PVC Riser and Screen
10 feet of 10-slot machine slotted well screen (15 ft-bgs to 25 ft-bgs)
Flushmount completion with manhole in concrete pad, locking water tight riser plug, bottom cap
Well Gravel from 25 ft-bgs to 13 ft-bgs
Bentonite Seal from 13 ft-bgs to 11 ft-bgs
Cement/benontie grout from 11 ft-bgs to 0.5 ft-bgs
Client: TIP - Trailer Fleet Services
Project Number: 572260702
Site Location: 1906 Bancroft St., Charlotte, NC
Coordinates: LS Elevation: Sheet: 1 of 1
Drilling Method: Hollow Stem Auger/Split-Spoon Monitoring Well Installed:
Sample Type(s): Grab Boring Diameter: Screened Interval: 13-23 ft-bgs
Weather:Logged By: BE Date/Time Started: 4/27/11 Depth of Boring: 23 ft-bgs
Drilling Contractor: SAEDACCO L S Elevation:Date/Time Finished:4/27/11 Water Level:17 ft bgs
BORING ID: MW-2
Drilling Contractor: SAEDACCO L.S. Elevation: Date/Time Finished:4/27/11 Water Level: 17 ft-bgs
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MATERIALS: Color, size, range, MAIN COMPONENT, minor
component(s), moisture content, structure, angularity, maximum grain size,
odor, and Geologic Unit (If Known)
*coares to fine sandy GRAVEL
1.2 Cement/Bentonite Grout dry, red sandy CLAY
12
Well Schematic
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1 1.2
1.2
1.2
1.0 - becoming dark red
1.0
1.0 dry, brown clayey SILT
1.0
1.1 - becoming orange
1.0
1.0
10
1
2
3
4
5
6
MW-2/0.5-2
1.0
1.0 dry, gray sandy CLAY
1.0
1.0
0.8
0.8
0.8
0.8
0.8
1.0 dry, brown silty CLAY
10
Bentonite Seal
7
8
9
10
11 MW-2/10-121.0
1.0
1.0
2.4
2.5
2.3
2.3 2
1.8
1.8
2dry brown sandy CLAY
15
16
12
13
14
yy▼1.7
1.7
1.7 - dry
1.7 1.7▼*
*
* dry, white sandy SILT (possible weathered rock)
*
*
- wet horizonGravel Pack
- wet
20
21
17
18
19
*
**
NOTES:ft-bgs: feet below ground surface; PID: Photo-ionization Detector; ppm-air: parts per million-air; * indicated no reading Date Time Depth to groundwater while drilling
Well Construction:4/27/2011 17 ft-bgs
Bottom Cap
Boring terminated at 23 ft-bgs
22
23
24
25
2-inch ID Schedule 40 PVC Riser and Screen 4/27/2011 19.5 ft-bgs
10 feet of 10-slot machine slotted well screen (13 ft-bgs to 23 ft-bgs)
Flushmount completion with manhole in concrete pad, locking water tight riser plug, bottom cap
Well Gravel from 23 ft-bgs to 11 ft-bgs
Bentonite Seal from 11 ft-bgs to 9.5 ft-bgs
Cement/benontie grout from 9.5 ft-bgs to 0.5 ft-bgs
Client: TIP - Trailer Fleet Services
Project Number: 572260702
Site Location: 1906 Bancroft St., Charlotte, NC
Coordinates: LS Elevation: Sheet: 1 of 1
Drilling Method: Hollow Stem Auger/Direct-Push Monitoring Well Installed:
Sample Type(s): Grab Boring Diameter: Screened Interval: 15 - 25 ft-bgs
Weather: Logged By: BE Date/Time Started: 4/27/11 Depth of Boring: 25 ft-bgs
Drilling Contractor: SAEDACCO L S Elevation:Date/Time Finished: 4/27/11 Water Level:15 ft bgs
BORING ID: MW-3
Drilling Contractor: SAEDACCO L.S. Elevation: Date/Time Finished: 4/27/11 Water Level: 15 ft-bgs
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MATERIALS: Color, size, range, MAIN COMPONENT, minor
component(s), moisture content, structure, angularity, maximum grain size,
odor, and Geologic Unit (If Known)
2.1 coares to fine sandy GRAVEL
1.9 dry, red silty CLAY
Well Schematic
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Flushmount manhole in concrete pad
1 MW 3/0 5 22.1
2.1
2.1
2.0
2.1
2.1
1.0 dry, gray GRAVEL
1.0 dry, red silty CLAY
1.0
1.0
106
1
Cement/Bentonite Grout
MW-3/0.5-2
2
3
4
5
1.0
1.0
1.3
1.3
*(no recovery 8.5 to 10)
*dry, orange silty CLAY
*
*
0.9
1.0
10 (no recovery 11 5 to 13)
7
8
9
10
11 1.0 (no recovery 11.5 to 13)
1.3
1.0
1.0
1.0 dry, red silty CLAY
1.0
0.9▼0.9
1.3
*
*
- wet, orange silty CLAY
MW-3/11-12
14
15
16
Bentonite Seal12
13
*
*
*
*
* *
*
0.0 - dry
0.0
0.0 - wet21
Gravel Pack
17
18
19
20
0.0
0.0
0.0
0.0 - dry
*
*
*
NOTES:ft-bgs: feet below ground surface; PID: Photo-ionization Detector; ppm-air: parts per million-air; * indicated no reading Date Time Depth to groundwater while drilling
Well Construction:4/27/2011 15 ft-bgs
Boring terminated at 25 ft-bgs
22
23
24
25 Bottom Cap
2-inch ID Schedule 40 PVC Riser and Screen
10 feet of 10-slot machine slotted well screen (15 ft-bgs to 25 ft-bgs)
Flushmount completion with manhole in concrete pad, locking water tight riser plug, bottom cap
Well Gravel from 25 ft-bgs to 13 ft-bgs
Bentonite Seal from 13 ft-bgs to 11 ft-bgs
Cement/benontie grout from 11 ft-bgs to 0.5 ft-bgs
Client: TIP - Trailer Fleet Services
Project Number: 572260702
Site Location: 1906 Bancroft St., Charlotte, NC
Coordinates: LS Elevation: Sheet: 1 of 1
Drilling Method: Hollow Stem Auger/Direct-Push Monitoring Well Installed:
Sample Type(s): Grab Boring Diameter: Screened Interval: 15 - 25 ft-bgs
Weather: Logged By: BE Date/Time Started: 4/27/11 Depth of Boring: 25 ft-bgs
Drilling Contractor: SAEDACCO L S Elevation:Date/Time Finished: 4/27/11 Water Level:24 5 ft bgs
BORING ID: MW-4
Drilling Contractor: SAEDACCO L.S. Elevation: Date/Time Finished: 4/27/11 Water Level: 24.5 ft-bgs
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MATERIALS: Color, size, range, MAIN COMPONENT, minor
component(s), moisture content, structure, angularity, maximum grain size,
odor, and Geologic Unit (If Known)
0 coares to fine sandy GRAVEL
0 dry, red clayey SILT
d l SILT
Well Schematic
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1 MW 4/0 5 20dry, orange clayey SILT
0
0
0
0
0
0 dry, orange-brown sandy CLAY
0
0
0
06
1
Cement/Bentonite Grout
MW-4/0.5-2
2
3
4
5
0
0 dry, red silty CLAY
0
0
0
0
0
0 moist, orange sandy CLAY
0
0
0 MW-4/10-12
7
8
9
10
11 0
0
0 moist, red silty CLAY
0 moist, white sandy CLAY
0
0▼0 (water rose to approximately 14.4 ft-bgs) 0
0 moist, orange silty CLAY
0
0 moist, white sandy CLAY
14
15
16
Bentonite Seal12
13
,y
0
0 moist, orange silty CLAY
0
0
0 0 moist orange sandy CLAY
0 moist, orange silty CLAY
0
0
0
Gravel Pack
17
18
19
20
21
0 dry, bronw sandy CLAY
0
0
0 - possible weathered rock
0▼0
0
NOTES:ft-bgs: feet below ground surface; PID: Photo-ionization Detector; ppm-air: parts per million-air; * indicated no reading Date Time Depth to groundwater while drilling
Well Construction:4/27/2011 24.5 ft-bgs then rose to 14.4 ft-bgs
Boring terminated at 25 ft-bgs
22
23
24
25 Bottom Cap
2-inch ID Schedule 40 PVC Riser and Screen
10 feet of 10-slot machine slotted well screen (15 ft-bgs to 25 ft-bgs)
Flushmount completion with manhole in concrete pad, locking water tight riser plug, bottom cap
Well Gravel from 25 ft-bgs to 13 ft-bgs
Bentonite Seal from 13 ft-bgs to 11 ft-bgs
Cement/benontie grout from 11 ft-bgs to 0.5 ft-bgs
Client: TIP - Trailer Fleet Services
Project Number: 572260702
Site Location: 1906 Bancroft St., Charlotte, NC
Coordinates: LS Elevation: Sheet: 1 of 1
Drilling Method: Hollow Stem Auger/Direct-Push Monitoring Well Installed:
Sample Type(s): Grab Boring Diameter: Screened Interval: 15 - 25 ft-bgs
Weather: Logged By: BE Date/Time Started: 4/28/11 Depth of Boring: 32 ft-bgs
Drilling Contractor: SAEDACCO L S Elevation:Date/Time Finished: 4/28/11 Water Level:28 ft bgs
BORING ID: MW-5
Drilling Contractor: SAEDACCO L.S. Elevation: Date/Time Finished: 4/28/11 Water Level: 28 ft-bgs
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MATERIALS: Color, size, range, MAIN COMPONENT, minor
component(s), moisture content, structure, angularity, maximum grain size,
odor, and Geologic Unit (If Known)
3.6 coares to fine sandy GRAVEL
2.8 dry, orange clayey SILT
Well Schematic
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Flushmount manhole in concrete pad
1 MW 5/0 5 23.0
3.3
3.4 dry, yellow silty CLAY
3.6
3.0
3.0
3.5 moist, yeallow sandy CLAY
3.5
3.3
2.7
286
1
Cement/Bentonite Grout
MW-5/0.5-2
2
3
4
5
2.8
3.3
3.2
3.4
3.6 moist, orange silty CLAY
3.8 moist gray gravelly sandy SILT
3.0 moist orange silty CLAY
3.6
3.4
2.8
28
7
8
9
10
MW-5/10-12112.8
3.7
2.9 - becoming brown
3.1
3.1
3.1 2.9 2.9
2.8 moist orange sandy SILT
3.2
3.1 moist orange sandy CLAY
14
15
16
Bentonite Seal12
13
gy
3.1
2.9
3.2
3.1
3.2 2.9 dry, yellow silty CLAY
3.3
3.2
2.7 moist brown sandy CLAY
2.5
Gravel Pack
17
18
19
20
21
2.3
2.6 moist orange silty CLAY
2.7
2.8
2.9 2.5
2.5
NOTES:ft-bgs: feet below ground surface; PID: Photo-ionization Detector; ppm-air: parts per million-air; * indicated no reading Date Time Depth to groundwater while drilling
Well Construction:4/28/2011 28 ft-bgs
23
24
25 Bottom Cap
boring log continued on next page
22
2-inch ID Schedule 40 PVC Riser and Screen
10 feet of 10-slot machine slotted well screen (15 ft-bgs to 25 ft-bgs)
Flushmount completion with manhole in concrete pad, locking water tight riser plug, bottom cap
Well Gravel from 25 ft-bgs to 13 ft-bgs
Bentonite Seal from 13 ft-bgs to 11 ft-bgs
Cement/benontie grout from 11 ft-bgs to 0.5 ft-bgs
Client: TIP - Trailer Fleet Services
Project Number: 572260702
Site Location: 1906 Bancroft St., Charlotte, NC
Coordinates: LS Elevation: Sheet: 2 of 2
Drilling Method: Hollow Stem Auger/Direct-Push Monitoring Well Installed:
Sample Type(s): Grab Boring Diameter: Screened Interval: 15 - 25 ft-bgs
Weather: Logged By: BE Date/Time Started: 4/28/11 Depth of Boring: 32 ft-bgs
Drilling Contractor: SAEDACCO L S Elevation:Date/Time Finished: 4/28/11 Water Level:28 ft bgs
BORING ID: MW-5
Drilling Contractor: SAEDACCO L.S. Elevation: Date/Time Finished: 4/28/11 Water Level: 28 ft-bgs
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MATERIALS: Color, size, range, MAIN COMPONENT, minor
component(s), moisture content, structure, angularity, maximum grain size,
odor, and Geologic Unit (If Known)
iilCLAY
Well Schematic
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25 2.5 moist, orange silty CLAY
2.5
2.5
2.7
2.6 Backfilled
t27ftb*
2.5
2.5
2.6
2.3
2530
- wet
Installed 2-ft thick bentonite seal
25
26
27
28
29
Backfilled to 25 ft-bgs with well
gravel
Backfilled to 28 ft-bgs with well
gravel2.5
2.5
2.4
2.8
31
32
33
34
35
- dry
Boring terminated at 32 ft-bgs
gravel
NOTES:ft-bgs: feet below ground surface; PID: Photo-ionization Detector; ppm-air: parts per million-air; * indicated no reading Date Time Depth to groundwater while drilling
Well Construction:4/28/2011 28 ft-bgs
continued from previous page
2-inch ID Schedule 40 PVC Riser and Screen
10 feet of 10-slot machine slotted well screen (15 ft-bgs to 25 ft-bgs)
Flushmount completion with manhole in concrete pad, locking water tight riser plug, bottom cap
Well Gravel from 25 ft-bgs to 13 ft-bgs
Bentonite Seal from 13 ft-bgs to 11 ft-bgs
Cement/benontie grout from 11 ft-bgs to 0.5 ft-bgs
Client: TIP - Trailer Fleet Services
Project Number: 572260702
Site Location: 1906 Bancroft St., Charlotte, NC
Coordinates: LS Elevation: Sheet: 1 of 1
Drilling Method: Direct Push and Air Rotary Monitoring Well Installed:
Sample Type(s): Grab Boring Diameter: Screened Interval: 15 - 25 ft-bgs
Weather: Sunny, 90's, Humid Logged By: AK Date/Time Started: 6/9/11 1225 Depth of Boring: 25 ft-bgs
Drilling Contractor: SAEDACCO L S Elevation:Date/Time Finished: 6/9/11 1245 Water Level:15 ft bgs
BORING ID: MW-6
Drilling Contractor: SAEDACCO L.S. Elevation: Date/Time Finished: 6/9/11 1245 Water Level: 15 ft-bgs
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MATERIALS: Color, size, range, MAIN COMPONENT, minor
component(s), moisture content, structure, angularity, maximum grain size,
odor, and Geologic Unit (If Known)
coares to fine sandy GRAVEL
Well Schematic
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Flushmount manhole in concrete pad
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Cement/Bentonite Grout
2
3
4
5
6
0.3 dry, reddish orange clayey SILT
0.3
0.4
0.4
0.4 dry, orangish brown saprolitic silty medium to fine SAND
0.3
03
7
8
9
10
11 0.3
0
0 moist, light brown silty fine SAND
0
0
0
0▼0
Bentonite Seal12
13
14
- wet15
16
Gravel Pack
21
17
18
19
20
NOTES:ft-bgs: feet below ground surface; PID: Photo-ionization Detector; ppm-air: parts per million-air; * indicated no reading Date Time Depth to groundwater while drilling
Well Construction:6/9/2011 15 ft-bgs
Boring terminated at 25 ft-bgs
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23
24
25 Bottom Cap
2-inch ID Schedule 40 PVC Riser and Screen
10 feet of 10-slot machine slotted well screen (15 ft-bgs to 25 ft-bgs)
Flushmount completion with manhole in concrete pad, locking water tight riser plug, bottom cap
Well Gravel from 25 ft-bgs to 13 ft-bgs
Bentonite Seal from 13 ft-bgs to 11 ft-bgs
Cement/benontie grout from 11 ft-bgs to 0.5 ft-bgs
Client: TIP - Trailer Fleet Services
Project Number: 572260702
Site Location: 1906 Bancroft St., Charlotte, NC
Coordinates: LS Elevation: Sheet: 1 of 1
Drilling Method: Direct Push and Air Rotary Monitoring Well Installed:
Sample Type(s): Grab Boring Diameter: Screened Interval: 15 - 25 ft-bgs
Weather: Sunny, 80's, Humid Logged By: AK Date/Time Started: 6/9/11 0920 Depth of Boring: 25 ft-bgs
Drilling Contractor: SAEDACCO L S Elevation:Date/Time Finished: 6/9/11 1010 Water Level:17 ft bgs
BORING ID: MW-7
Drilling Contractor: SAEDACCO L.S. Elevation: Date/Time Finished: 6/9/11 1010 Water Level: 17 ft-bgs
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MATERIALS: Color, size, range, MAIN COMPONENT, minor
component(s), moisture content, structure, angularity, maximum grain size,
odor, and Geologic Unit (If Known)
coares to fine sandy GRAVEL
Well Schematic
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Flushmount manhole in concrete pad
1
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Cement/Bentonite Grout
2
3
4
5
6
0 moist, brown silty medium to fine SAND
0
0
0 moist, light brown-gray medin to fine sandy SILT
0
0
0 moist blue-gray clayey SILT
7
8
9
10
11 0 moist, blue gray clayey SILT
0
0
0 moist, blue-gray saprolitic clayey SILT
0
0
0
0
0
0
0
Bentonite Seal12
13
14
15
16
▼0
Gravel Pack
17
18
19
- wet
21
20
NOTES:ft-bgs: feet below ground surface; PID: Photo-ionization Detector; ppm-air: parts per million-air; * indicated no reading Date Time Depth to groundwater while drilling
Well Construction:6/9/2011 17 ft-bgs
Boring terminated at 25 ft-bgs
22
23
24
25 Bottom Cap
2-inch ID Schedule 40 PVC Riser and Screen
10 feet of 10-slot machine slotted well screen (15 ft-bgs to 25 ft-bgs)
Flushmount completion with manhole in concrete pad, locking water tight riser plug, bottom cap
Well Gravel from 25 ft-bgs to 13 ft-bgs
Bentonite Seal from 13 ft-bgs to 11 ft-bgs
Cement/benontie grout from 11 ft-bgs to 0.5 ft-bgs
Client: TIP - Trailer Fleet Services
Project Number: 572260702
Site Location: 1906 Bancroft St., Charlotte, NC
Coordinates: LS Elevation: Sheet: 1 of 1
Drilling Method: Direct Push and Air Rotary Monitoring Well Installed:
Sample Type(s): Grab Boring Diameter: Screened Interval: 15 - 25 ft-bgs
Weather: Sunny, 80's, Humid Logged By: TH Date/Time Started: 6/9/11 0920 Depth of Boring: 25 ft-bgs
Drilling Contractor: SAEDACCO L S Elevation:Date/Time Finished: 6/9/11 1010 Water Level:18 ft bgs
BORING ID: MW-8
Drilling Contractor: SAEDACCO L.S. Elevation: Date/Time Finished: 6/9/11 1010 Water Level: 18 ft-bgs
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MATERIALS: Color, size, range, MAIN COMPONENT, minor
component(s), moisture content, structure, angularity, maximum grain size,
odor, and Geologic Unit (If Known)
coares to fine sandy GRAVEL
Well Schematic
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Flushmount manhole in concrete pad
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Cement/Bentonite Grout
2
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4
5
6
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0 moist yellowish orange clayey SILT, moist
0
0
7
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10
11 0
0
0.1 moist orange clayey SILT
0.1
0.2 moist brown SILT
0.1
0 moist orange/white marbled clayey sandy SILT
0.5
0.3
0
0.2 tan clayey SILT
Bentonite Seal12
13
14
15
16 yy
0.3
0.2▼
Gravel Pack
17
18
19
- wet
21
20
NOTES:ft-bgs: feet below ground surface; PID: Photo-ionization Detector; ppm-air: parts per million-air; * indicated no reading Date Time Depth to groundwater while drilling
Well Construction:6/9/2011 18 ft-bgs
Boring terminated at 25 ft-bgs
22
23
24
25 Bottom Cap
2-inch ID Schedule 40 PVC Riser and Screen
10 feet of 10-slot machine slotted well screen (15 ft-bgs to 25 ft-bgs)
Flushmount completion with manhole in concrete pad, locking water tight riser plug, bottom cap
Well Gravel from 25 ft-bgs to 13 ft-bgs
Bentonite Seal from 13 ft-bgs to 11 ft-bgs
Cement/benontie grout from 11 ft-bgs to 0.5 ft-bgs
Client: TIP - Trailer Fleet Services
Project Number: 572260702
Site Location: 1906 Bancroft St., Charlotte, NC
Coordinates: LS Elevation: Sheet: 1 of 1
Drilling Method: Direct Push and Air Rotary Monitoring Well Installed:
Sample Type(s): Grab Boring Diameter: Screened Interval: 15 - 25 ft-bgs
Weather: Sunny, 80's, Humid Logged By: TH Date/Time Started: 6/9/11 0920 Depth of Boring: 25 ft-bgs
Drilling Contractor: SAEDACCO L S Elevation:Date/Time Finished: 6/9/11 1010 Water Level:15 ft bgs
BORING ID: MW-9
Drilling Contractor: SAEDACCO L.S. Elevation: Date/Time Finished: 6/9/11 1010 Water Level: 15 ft-bgs
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MATERIALS: Color, size, range, MAIN COMPONENT, minor
component(s), moisture content, structure, angularity, maximum grain size,
odor, and Geologic Unit (If Known)
0 coares to fine sandy GRAVEL
Tan gravelly SILT, moist1
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Flushmount manhole in concrete pad
0 Tan SILT
1
2
Cement/Bentonite Grout
3
4
5
6
0
0 Greenish white clayey sandy SILT, moist
0
0
7
8
9
10
11 0
0
0
0 Green and brown marbled clayey sandy SILT, moist
0
0
0 Brown clayey SILT,moist▼0 White tan orange marbled clayey SILT, wet
Tan clayey SILT
Bentonite Seal12
13
14
15
16
Gravel Pack
17
18
19
20
21
NOTES:ft-bgs: feet below ground surface; PID: Photo-ionization Detector; ppm-air: parts per million-air; * indicated no reading Date Time Depth to groundwater while drilling
Well Construction:6/9/2011 15 ft-bgs
25 Bottom Cap
Boring terminated at 25 ft-bgs
24
22
23
2-inch ID Schedule 40 PVC Riser and Screen
10 feet of 10-slot machine slotted well screen (15 ft-bgs to 25 ft-bgs)
Flushmount completion with manhole in concrete pad, locking water tight riser plug, bottom cap
Well Gravel from 25 ft-bgs to 13 ft-bgs
Bentonite Seal from 13 ft-bgs to 11 ft-bgs
Cement/benontie grout from 11 ft-bgs to 0.5 ft-bgs
Site Name: TFS Charlotte Branch
Location: 1906 Bancroft St, Charlotte
Sample Method: DPT Macro Cores
Drilling Method: Direct Push
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0.5 2.6 red silty clay, dry, tight
1 2.5 red silty clay, dry, tight
1.5 2.1 red silty clay, dry, tight
2 2.3 red silty clay, dry, tight
2.5 2.4 red silty clay, dry, tight
3 2.1 red silty clay, dry, tight
35 25 d ilt l d ti ht
Boring/Well No.: B-1
Date: 4/28/11
Job No.: 572260702
AMEC Rep: Beth Espitia
Remarks: Sampled B-1/0.5-2 at 1104; Sampled B-1/10-12 at 1119
3.5 2.5 red silty clay, dry, tight
4 2.4 red silty clay, dry, tight
4.5 2.2 red/orange silty clay, dry, tight
5 2.0 red/orange silty clay, dry, tight
5.5 2.0 red/orange silty clay, dry, tight
6 2.1 red/orange silty clay, dry, tight
6.5 2.1 red/orange silty clay, dry, tight
7 2.1 red/orange silty clay, dry, tight
7.5 2.1 red/orange silty clay, dry, tight
8 2.2 red/orange silty clay, dry, tight
8.5 2.2 orange silty clay, dry
9 2.2 orange silty clay, dry
9.5 2.1 orange silty clay, dry
10 2.1 orange silty clay, dry
10.5 2.1 orange silty clay, dry
11 2.2 yellow, silty clay, dry
11.5 2.1 yellow, silty clay, dry
12 2.1 yellow, silty clay, dry
Site Name: TFS Charlotte Branch
Location: 1906 Bancroft St, Charlotte
Sample Method: DPT Macro Cores
Drilling Method: Direct Push
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0.5 1.6 orange silty clay, dry
1 1.7 orange silty clay, dry
1.5 1.7 orange silty clay, dry
2 1.7 orange silty clay, dry
2.5 1.7 orange silty clay, dry
3 1.8 orange silty clay, dry
35 17 ilt l d
Boring/Well No.: B-2
Date: 4/28/11
Job No.: 572260702
AMEC Rep: Beth Espitia
Remarks: Sampled B-2/0.5-2 at 1235; Sampled B-2/10-12 at 1250
3.5 1.7 orange silty clay, dry
4 1.8 orange silty clay, dry
4.5 1.4 orange silty clay
5 1.4 orange silty clay
5.5 1.4 orange silty clay
6 1.4 orange silty clay
6.5 1.4 orangey yellow silty clay, tight
7 1.5 orangey yellow silty clay, tight
7.5 1.6 orangey yellow silty clay, tight
8 1.6 orangey yellow silty clay, tight
8.5 1.0 red/orange silty clay, soft
9 0.9 red/orange silty clay, soft
9.5 1.0 red/orange silty clay, soft
10 1.2 orange/yellow clayey silt
10.5 1.1 orange/yellow clayey silt
11 1.2 orange/yellow clayey silt
11.5 1.2 orange/yellow clayey silt
12 1.1 orange/yellow clayey silt
Site Name: TFS Charlotte Branch
Location: 1906 Bancroft St, Charlotte
Sample Method: DPT Macro Cores
Drilling Method: Direct Push
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0.5 0.0 dark red silty clay, tight
1 0.0 dark red silty clay, tight
1.5 0.0 dark red silty clay, tight
2 0.0 dark red silty clay, tight
2.5 0.0 dark red silty clay, tight
3 0.0 dark red silty clay, tight
35 00 d k d ilt l ti ht
Boring/Well No.: B-3
Date: 4/28/11
Job No.: 572260702
AMEC Rep: Beth Espitia
Remarks: Sampled B-3/0.5-2 at 1455; Sampled B-3/10-12 at 1510
3.5 0.0 dark red silty clay, tight
4 0.0 dark red silty clay, tight
4.5 0.0 dark red silty clay, tight
5 0.0 dark red silty clay, tight
5.5 0.0 dark red silty clay, tight
6 0.0 dark red silty clay, tight
6.5 0.0 dark red silty clay, tight
7 0.0 dark red silty clay, tight
7.5 0.0 dark red silty clay, tight
8 0.0 dark red silty clay, tight
8.5 0.0 dark red silty clay
9 0.0 dark red silty clay
9.5 0.0 dark red silty clay
10 0.0 dark red silty clay
10.5 0.0 dark red silty clay
11 0.0 dark red silty clay
11.5 0.0 dark red silty clay
12 0.0 dark red silty clay
Site Name: TFS Charlotte Branch
Location: 1906 Bancroft St, Charlotte
Sample Method: DPT Macro Cores
Drilling Method: Direct Push
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0.5 N/A gravel
1 N/A gravel
1.5 N/A gravel
2 0.8 dark red silty clay/tight
2.5 0.8 dark red silty clay/tight
3 1.0 dark red silty clay/tight
35 10 d k d ilt l /ti ht
Boring/Well No.: B-4
Date: 4/28/11
Job No.: 572260702
AMEC Rep: Beth Espitia
Remarks: Sampled B-4/2-4 at 1322 ; Sampled B-4/10-12 at 1345
3.5 1.0 dark red silty clay/tight
4 1.1 dark red silty clay/tight
4.5 0.5 green silty clay
5 0.5 brown silty clay, wet
5.5 0.5 green silty clay
6 0.7 orange silty clay
6.5 0.7 orange silty clay, tight
7 0.7 orange silty clay, tight
7.5 0.8 orange silty clay, tight
8 0.9 orange silty clay, tight
8.5 0.0 yellow silty clay, tight
9 0.0 yellow silty clay, tight
9.5 0.0 yellow silty clay, tight
10 0.0 orange sandy clay
10.5 0.0 orange sandy clay
11 0.3 orange silty clay
11.5 0.0 orange silty clay
12 0.1 orange silty clay
Site Name: TFS Charlotte Branch
Location: 1906 Bancroft St, Charlotte
Sample Method: DPT Macro Cores
Drilling Method: Direct Push
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0.5 N/A gravel
1 N/A gravel
1.5 N/A gravel
2 0.0 dark red silty clay, tight
2.5 0.0 dark red silty clay, tight
3 0.0 dark red silty clay, tight
35 02 d k d ilt l ti ht
Boring/Well No.: B-5
Date: 4/28/11
Job No.: 572260702
AMEC Rep: Beth Espitia
Remarks: Sampled B-5/2-4 at 1410 ; Sampled B-5/10-12 at 1345
3.5 0.2 dark red silty clay, tight
4 0.1 dark red silty clay, tight
4.5 0.0 gravel
5 0.0 dark red silty clay, tight
5.5 0.0 dark red silty clay, tight
6 0.8 orange silty clay, tight
6.5 0.7 orange silty clay, tight
7 0.6 orange silty clay, tight
7.5 1.0 orange silty clay, tight
8 0.8 orange silty clay, tight
8.5 0.0 gravel
9 0.0 orange clayey silt, tight
9.5 0.0 orange clayey silt, tight
10 0.0 orange clayey silt, tight
10.5 0.0 orange clayey silt, tight
11 0.0 orange clayey silt, tight
11.5 0.0 orange clayey silt, tight
12 0.0 orange clayey silt, tight
Site Name: TFS Charlotte Branch
Location: 1906 Bancroft St, Charlotte
Sample Method: DPT Macro Cores
Drilling Method: Direct Push
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0.5 0.0 dark, red silty clay, tight
1 0.0 dark, red silty clay, tight
1.5 0.0 dark, red silty clay, tight
2 0.0 dark, red silty clay, tight
2.5 0.0 dark, red silty clay, tight
3 0.0 dark, red silty clay, tight
35 00 d k d ilt l ti ht
Boring/Well No.: B-6
Date: 4/28/11
Job No.: 572260702
AMEC Rep: Beth Espitia
Remarks: Sampled B-6/0.5-2 at 1530 ; Sampled B-6/10-12 at 1550
3.5 0.0 dark, red silty clay, tight
4 0.0 dark, red silty clay, tight
4.5 0.0 dark, red silty clay, tight
5 0.0 dark, red silty clay, tight
5.5 0.0 dark, red silty clay, tight
6 0.0 dark, red silty clay, tight
6.5 0.0 dark, red silty clay, tight
7 0.0 dark, red silty clay, tight
7.5 0.0 dark, red silty clay, tight
8 0.0 dark, red silty clay, tight
8.5 0.0 dark, red silty clay, tight
9 0.0 dark, red silty clay, tight
9.5 0.0 dark, red silty clay, tight
10 0.0 dark, red silty clay, tight
10.5 0.0 dark, red silty clay, tight
11 0.0 dark, red silty clay, tight
11.5 0.0 dark, red silty clay, tight
12 0.0 dark, red silty clay, tight
Site Name: TFS Charlotte Branch
Location: 1906 Bancroft St, Charlotte
Sample Method: DPT Macro Cores
Drilling Method: Direct Push
Depth
(ft BLS)
PID/OVA Reading
(ppm)Soil/Lithologic Description
0.5 0.0 yellow silty clay, tight
1 0.0 yellow silty clay, tight
1.5 0.0 yellow orange silty clay, tight
2 0.0 yellow orange silty clay, tight
2.5 0.0 yellow orange silty clay, tight
3 0.0 yellow orange silty clay, tight
35 00 ll ilt l ti ht
Boring/Well No.: B-7
Date: 4/28/11
Job No.: 572260702
AMEC Rep: Beth Espitia
Remarks: Sampled B-7/0.5-2 at 1615 ; Sampled B-7/10-12 at 1640
3.5 0.0 yellow orange silty clay, tight
4 0.0 yellow orange silty clay, tight
4.5 0.0 orange silty clay, tight
5 0.0 orange silty clay, tight
5.5 0.0 orange silty clay, tight
6 0.0 orange silty clay, tight
6.5 0.0 orange silty clay, tight
7 0.0 orange silty clay, tight
7.5 0.0 orange silty clay, tight
8 0.0 orange silty clay, tight
8.5 0.0 orange silty clay
9 0.0 orange silty clay
9.5 0.0 orange silty clay
10 0.0 orange silty clay
10.5 0.0 orange silty clay
11 0.0 orange silty clay
11.5 0.0 orange silty clay
12 0.0 orange silty clay
APPENDIX B
02/16/12
Technical Report for
AMEC Environment & Infrastructure, Inc.
GE-TFS; 1906 Bancroft St, Charlotte, NC
572260702
Accutest Job Number: F81875
Sampling Date: 04/27/11
Report to:
AMEC Earth & Environmental
steven.tanen@amec.com
ATTN: Steve Tanen
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), AK, AR, GA, KY, MA, NV, OK, UT, VA, WA, WI
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Conference
and/or state specific certification programs as applicable.
Client Service contact: Heather Wandrey 407-425-6700
Harry Behzadi, Ph.D.
Laboratory Director
Southeast
02/16/12
e-Hardcopy 2.0
Automated Report
81
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 81
F81875
Table of Contents
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Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Case Narrative/Conformance Summary ..............................................................4
Section 3: Sample Results ........................................................................................................8
3.1: F81875-1: MW-1/0.5-2 .................................................................................................9
3.2: F81875-2: MW-1/10-11 ................................................................................................18
3.3: F81875-3: TB-04/27/11 ................................................................................................26
3.4: F81875-4: MW-2/0.5-2 .................................................................................................28
3.5: F81875-5: MW-2/10-12 ................................................................................................37
3.6: F81875-6: MW-3/0.5-2 .................................................................................................45
3.7: F81875-7: MW-3/11-12 ................................................................................................54
3.8: F81875-8: MW-4/0.5-2 .................................................................................................62
3.9: F81875-9: MW-4/10-12 ................................................................................................71
Section 4: Misc. Forms ............................................................................................................79
4.1: Chain of Custody ...........................................................................................................80
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Sample Summary
AMEC Environment & Infrastructure, Inc.
Job No:F81875
GE-TFS; 1906 Bancroft St, Charlotte, NC
Project No: 572260702
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
F81875-1 04/27/11 09:45 BE 04/28/11 SO Soil MW-1/0.5-2
F81875-2 04/27/11 10:17 BE 04/28/11 SO Soil MW-1/10-11
F81875-3 04/27/11 00:00 BE 04/28/11 SO Trip Blank Soil TB-04/27/11
F81875-4 04/27/11 13:48 BE 04/28/11 SO Soil MW-2/0.5-2
F81875-5 04/27/11 14:10 BE 04/28/11 SO Soil MW-2/10-12
F81875-6 04/27/11 14:38 BE 04/28/11 SO Soil MW-3/0.5-2
F81875-7 04/27/11 15:03 BE 04/28/11 SO Soil MW-3/11-12
F81875-8 04/27/11 15:55 BE 04/28/11 SO Soil MW-4/0.5-2
F81875-9 04/27/11 16:10 BE 04/28/11 SO Soil MW-4/10-12
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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SAMPLE DELIVERY GROUP CASE NARRATIVE
Client: AMEC Earth & Environmental Job F81875
Site: GE-TFS; 1906 Bancroft St, Charlotte, NC Report Date: 5/20/2011 7:23:12 AM
8 Samples and 1 Trip Blank were collected on 04/27/2011 and were received at Accutest SE on 04/28/2011 properly preserved, at
3.8 Deg. C and intact. These Samples received an Accutest job number of F81875. A listing of the Laboratory Sample ID, Client
Sample ID and dates of collection are presented in the Results Summary Section of this report.
Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For more
information, please refer to QC summary pages.
Volatiles by GCMS by Method SW846 8260B Matrix: SO Batch ID: VG2719
All samples were analyzed within the recommended method holding time.
Samples F82009-7MS, F82009-7MSD were used as the QC samples indicated.
All method blanks for this batch meet method specific criteria.
Blank Spike Recovery for Acetone is outside control limits.
Matrix Spike Recoverys for 1,1,2-Trichloroethane, 2-Hexanone, 4-Methyl-2-pentanone, Acetone, Bromoform, Dibromochloromethane, Methyl ethyl ketone, Styrene, trans-1,3-Dichloropropene, Xylene (total) are outside control limits. Probable cause due to matrix interference.
Matrix Spike Duplicate Recoverys for 2-Hexanone, Acetone, Bromoform, Dibromochloromethane, Methyl ethyl ketone, trans-1,3-Dichloropropene are outside control limits. Probable cause due to matrix interference.
Matrix: SO Batch ID: VG2720
All samples were analyzed within the recommended method holding time.
Samples F82221-4MS, F82221-4MSD were used as the QC samples indicated.
All method blanks for this batch meet method specific criteria.
Matrix Spike Recoverys for Bromoform, cis-1,3-Dichloropropene, Dibromochloromethane, trans-1,3-Dichloropropene, cis-1,2-Dichloroethylene are outside control limits. Outside control limits due to high level in sample relative to spike
Matrix Spike Duplicate Recoverys for Bromoform, cis-1,2-Dichloroethylene, cis-1,3-Dichloropropene, Dibromochloromethane, trans-1,3-Dichloropropene are outside control limits. Probable cause due to matrix interference.
F81875-2 for Acetone: ICV outside of control limits.
Extractables by GCMS by Method SW846 8270D Matrix: SO Batch ID: OP37013
All samples were extracted within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F81929-13MS, F81929-13MSD were used as the QC samples indicated.
Blank Spike Recovery for Isophorone is outside control limits.
OP37013-BS for Isophorone: Sporadic marginal failure, within limits in MS/MSD.
Matrix: SO Batch ID: OP37029
All samples were extracted within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F81834-2MS, F81834-2MSD were used as the QC samples indicated.
Matrix Spike Recoverys for Benzoic Acid, Isophorone are outside control limits. Probable cause due to matrix interference. Matrix Spike Duplicate Recoverys for 3-Nitroaniline, Benzoic Acid are outside control limits. Probable cause due to matrix interference.
RPD for MSD for Benzoic Acid is outside control limits for sample OP37029-MSD. Probable cause due to sample non-homogeneity.
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Volatiles by GC by Method SW846 8015C Matrix: SO Batch ID: GQR2611
All samples were analyzed within the recommended method holding time. Samples F81875-1MS, F81875-1MSD were used as the QC samples indicated.
All method blanks for this batch meet method specific criteria.
Extractables by GC by Method SW846 8015C Matrix: SO Batch ID: OP37017
All samples were extracted within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F81929-19MS, F81929-19MSD were used as the QC samples indicated.
Extractables by GC by Method SW846 8082A Matrix: SO Batch ID: OP37021
All samples were extracted within the recommended method holding time. All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F81929-13MS, F81929-13MSD were used as the QC samples indicated.
Matrix Spike Recovery for Aroclor 1016 is outside control limits. Probable cause due to matrix interference.
Metals by Method SW846 6010C Matrix: SO Batch ID: MP20510
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F81875-1MS, F81875-1MSD, F81875-1PS, F81875-1SDL, F81875-1DUP were used as the QC samples for metals. Matrix Spike Recoverys for Antimony, Arsenic, Chromium, Molybdenum, Nickel, Selenium, Tin, Zinc are outside control limits. Spike recovery indicates possible matrix interference and/or sample nonhomogeneity.
Matrix Spike Duplicate Recoverys for Arsenic, Barium, Cadmium, Nickel, Selenium, Tin, Zinc, Antimony are outside control limits. Probable cause due to matrix interference.
Matrix Spike Recovery for Copper are outside control limits. Spike amount low relative to the sample amount. Refer to lab control or spike blank for recovery information.
RPD for Duplicate for Selenium is outside control limits for sample MP20510-D1. RPD acceptable due to low duplicate and sample concentrations.
RPD for MSD for Antimony is outside control limits for sample MP20510-S2. High RPD due to possible sample nonhomogeneity.
RPDs for Serial Dilution for Arsenic, Cadmium, Molybdenum, Barium, Chromium, Copper, Lead, Nickel, Zinc are outside control limits for sample MP20510-SD1. Percent difference acceptable due to low initial sample concentration (< 50 times IDL). MP20510-SD1 for Barium, Chromium, Copper, Lead, Nickel, Zinc: Serial dilution indicates possible matrix interference.
MP20510-PS1 for Selenium: Spike recovery indicates matrix interference and/or outside control limits due to high level in sample relative to spike amount.
MP20510-PS1 for Tin: Spike recovery indicates matrix interference and/or outside control limits due to high level in sample relative to spike amount.
MP20510-PS1 for Zinc: Spike recovery indicates matrix interference and/or outside control limits due to high level in sample relative to spike amount.
F81875-7 for Antimony: Elevated reporting limit(s) due to matrix interference.
F81875-6 for Arsenic: Elevated reporting limit(s) due to matrix interference.
F81875-6 for Beryllium: Elevated reporting limit(s) due to matrix interference.
F81875-6 for Cadmium: Elevated reporting limit(s) due to matrix interference.
F81875-6 for Chromium: Elevated reporting limit(s) due to matrix interference.
F81875-6 for Copper: Elevated reporting limit(s) due to matrix interference.
F81875-6 for Molybdenum: Elevated reporting limit(s) due to matrix interference.
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Metals by Method SW846 6010C Matrix: SO Batch ID: MP20510 F81875-6 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81875-6 for Selenium: Elevated reporting limit(s) due to matrix interference.
F81875-6 for Silver: Elevated reporting limit(s) due to matrix interference.
F81875-6 for Tin: Elevated reporting limit(s) due to matrix interference.
F81875-4 for Antimony: Elevated reporting limit(s) due to matrix interference.
F81875-6 for Lead: Elevated reporting limit(s) due to matrix interference.
F81875-6 for Antimony: Elevated reporting limit(s) due to matrix interference.
F81875-7 for Arsenic: Elevated reporting limit(s) due to matrix interference.
F81875-7 for Barium: Elevated reporting limit(s) due to matrix interference.
F81875-7 for Beryllium: Elevated reporting limit(s) due to matrix interference.
F81875-7 for Cadmium: Elevated reporting limit(s) due to matrix interference.
F81875-7 for Chromium: Elevated reporting limit(s) due to matrix interference.
F81875-7 for Copper: Elevated reporting limit(s) due to matrix interference.
F81875-7 for Molybdenum: Elevated reporting limit(s) due to matrix interference.
F81875-7 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81875-7 for Selenium: Elevated reporting limit(s) due to matrix interference.
F81875-7 for Silver: Elevated reporting limit(s) due to matrix interference.
F81875-7 for Tin: Elevated reporting limit(s) due to matrix interference.
F81875-7 for Zinc: Elevated reporting limit(s) due to matrix interference.
F81875-6 for Zinc: Elevated reporting limit(s) due to matrix interference.
F81875-5 for Antimony: Elevated reporting limit(s) due to matrix interference.
F81875-4 for Arsenic: Elevated reporting limit(s) due to matrix interference.
F81875-4 for Barium: Elevated reporting limit(s) due to matrix interference.
F81875-4 for Beryllium: Elevated reporting limit(s) due to matrix interference.
F81875-4 for Cadmium: Elevated reporting limit(s) due to matrix interference.
F81875-4 for Chromium: Elevated reporting limit(s) due to matrix interference.
F81875-4 for Copper: Elevated reporting limit(s) due to matrix interference.
F81875-4 for Molybdenum: Elevated reporting limit(s) due to matrix interference.
F81875-4 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81875-4 for Selenium: Elevated reporting limit(s) due to matrix interference. F81875-4 for Silver: Elevated reporting limit(s) due to matrix interference.
F81875-6 for Barium: Elevated reporting limit(s) due to matrix interference.
F81875-4 for Zinc: Elevated reporting limit(s) due to matrix interference.
F81875-5 for Zinc: Elevated reporting limit(s) due to matrix interference.
F81875-5 for Molybdenum: Elevated reporting limit(s) due to matrix interference.
F81875-5 for Tin: Elevated reporting limit(s) due to matrix interference.
F81875-5 for Silver: Elevated reporting limit(s) due to matrix interference.
F81875-4 for Tin: Elevated reporting limit(s) due to matrix interference.
F81875-5 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81875-5 for Arsenic: Elevated reporting limit(s) due to matrix interference.
F81875-5 for Copper: Elevated reporting limit(s) due to matrix interference.
F81875-5 for Chromium: Elevated reporting limit(s) due to matrix interference.
F81875-5 for Cadmium: Elevated reporting limit(s) due to matrix interference.
F81875-5 for Beryllium: Elevated reporting limit(s) due to matrix interference.
F81875-5 for Barium: Elevated reporting limit(s) due to matrix interference.
F81875-5 for Selenium: Elevated reporting limit(s) due to matrix interference.
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Metals by Method SW846 7471B Matrix: SO Batch ID: MP20537
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria.
Samples F81803-3DUP, F81803-3MS, F81803-3MSD, F81803-3SDL were used as the QC samples for metals.
RPD for Serial Dilution for Mercury is outside control limits for sample MP20537-SD1. Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
Wet Chemistry by Method SM19 2540G Matrix: SO Batch ID: GN44379
Sample F81879-1DUP was used as the QC sample for Solids, Percent.
Accutest Laboratories Southeast (ALSE) certifies that this report meets the project requirements for analytical data produced for the
samples as received at ALSE and as stated on the COC. ALSE certifies that the data meets the Data Quality Objectives for precision,
accuracy and completeness as specified in the ALSE Quality Manual except as noted above. This report is to be used in its entirety.
ALSE is not responsible for any assumptions of data quality if partial data packages are used.
Narrative prepared by:
_______________________________________ Date: May 20, 2011
Ellen Pampel, Inorganic QA (signature on file)
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Sample Results
Report of Analysis
Southeast
Section 3
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Report of Analysis Page 1 of 2
Client Sample ID:MW-1/0.5-2
Lab Sample ID:F81875-1 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8260B Percent Solids:91.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 G0072789.D 1 05/09/11 SH n/a n/a VG2719
Run #2
Initial Weight
Run #1 5.61 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 49 20 ug/kg
71-43-2 Benzene ND 4.9 1.5 ug/kg
75-27-4 Bromodichloromethane ND 4.9 1.1 ug/kg
75-25-2 Bromoform ND 4.9 1.5 ug/kg
108-90-7 Chlorobenzene ND 4.9 0.98 ug/kg
75-00-3 Chloroethane ND 4.9 2.0 ug/kg
67-66-3 Chloroform ND 4.9 1.2 ug/kg
75-15-0 Carbon disulfide ND 4.9 2.0 ug/kg
56-23-5 Carbon tetrachloride ND 4.9 1.8 ug/kg
75-34-3 1,1-Dichloroethane ND 4.9 1.1 ug/kg
75-35-4 1,1-Dichloroethylene ND 4.9 1.4 ug/kg
107-06-2 1,2-Dichloroethane ND 4.9 0.98 ug/kg
78-87-5 1,2-Dichloropropane ND 4.9 1.2 ug/kg
124-48-1 Dibromochloromethane ND 4.9 0.98 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 4.9 1.5 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 4.9 0.98 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 4.9 1.5 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 4.9 1.1 ug/kg
100-41-4 Ethylbenzene ND 4.9 0.98 ug/kg
591-78-6 2-Hexanone ND 24 5.3 ug/kg
108-10-1 4-Methyl-2-pentanone ND 24 5.4 ug/kg
74-83-9 Methyl bromide ND 4.9 2.0 ug/kg
74-87-3 Methyl chloride ND 4.9 2.0 ug/kg
75-09-2 Methylene chloride ND 9.8 4.5 ug/kg
78-93-3 Methyl ethyl ketone ND 24 5.9 ug/kg
100-42-5 Styrene ND 4.9 2.5 ug/kg
71-55-6 1,1,1-Trichloroethane ND 4.9 1.1 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 4.9 1.2 ug/kg
79-00-5 1,1,2-Trichloroethane ND 4.9 1.1 ug/kg
127-18-4 Tetrachloroethylene ND 4.9 0.98 ug/kg
108-88-3 Toluene ND 4.9 1.2 ug/kg
79-01-6 Trichloroethylene ND 4.9 1.2 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-1/0.5-2
Lab Sample ID:F81875-1 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8260B Percent Solids:91.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 4.9 1.5 ug/kg
1330-20-7 Xylene (total)ND 15 3.1 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%80-121%
2037-26-5 Toluene-D8 89%71-130%
460-00-4 4-Bromofluorobenzene 92%59-148%
17060-07-0 1,2-Dichloroethane-D4 108%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-1/0.5-2
Lab Sample ID:F81875-1 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:91.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L051218.D 1 05/05/11 NAF 05/04/11 OP37013 SL2613
Run #2
Initial Weight Final Volume
Run #1 30.2 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 910 320 ug/kg
95-57-8 2-Chlorophenol ND 180 18 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 180 18 ug/kg
120-83-2 2,4-Dichlorophenol ND 180 18 ug/kg
105-67-9 2,4-Dimethylphenol ND 180 23 ug/kg
51-28-5 2,4-Dinitrophenol ND 910 360 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 360 72 ug/kg
95-48-7 2-Methylphenol ND 180 18 ug/kg
3&4-Methylphenol ND 180 26 ug/kg
88-75-5 2-Nitrophenol ND 180 18 ug/kg
100-02-7 4-Nitrophenol ND 910 140 ug/kg
87-86-5 Pentachlorophenol ND 910 220 ug/kg
108-95-2 Phenol ND 180 18 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 180 18 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 180 18 ug/kg
83-32-9 Acenaphthene ND 180 18 ug/kg
208-96-8 Acenaphthylene ND 180 18 ug/kg
120-12-7 Anthracene ND 180 18 ug/kg
56-55-3 Benzo(a)anthracene ND 180 18 ug/kg
50-32-8 Benzo(a)pyrene ND 180 18 ug/kg
205-99-2 Benzo(b)fluoranthene ND 180 18 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 180 18 ug/kg
207-08-9 Benzo(k)fluoranthene ND 180 18 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 180 18 ug/kg
85-68-7 Butyl benzyl phthalate ND 180 36 ug/kg
100-51-6 Benzyl Alcohol ND 180 36 ug/kg
91-58-7 2-Chloronaphthalene ND 180 36 ug/kg
106-47-8 4-Chloroaniline ND 180 18 ug/kg
86-74-8 Carbazole ND 180 18 ug/kg
218-01-9 Chrysene ND 180 18 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 180 18 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 180 18 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-1/0.5-2
Lab Sample ID:F81875-1 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:91.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 180 18 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 180 18 ug/kg
95-50-1 1,2-Dichlorobenzene ND 180 36 ug/kg
541-73-1 1,3-Dichlorobenzene ND 180 36 ug/kg
106-46-7 1,4-Dichlorobenzene ND 180 36 ug/kg
121-14-2 2,4-Dinitrotoluene ND 180 18 ug/kg
606-20-2 2,6-Dinitrotoluene ND 180 21 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 360 36 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 180 18 ug/kg
132-64-9 Dibenzofuran ND 180 18 ug/kg
84-74-2 Di-n-butyl phthalate ND 360 72 ug/kg
117-84-0 Di-n-octyl phthalate ND 180 36 ug/kg
84-66-2 Diethyl phthalate ND 360 72 ug/kg
131-11-3 Dimethyl phthalate ND 180 36 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 360 72 ug/kg
206-44-0 Fluoranthene ND 180 18 ug/kg
86-73-7 Fluorene ND 180 18 ug/kg
118-74-1 Hexachlorobenzene ND 180 18 ug/kg
87-68-3 Hexachlorobutadiene ND 180 36 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 180 80 ug/kg
67-72-1 Hexachloroethane ND 180 36 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 180 18 ug/kg
78-59-1 Isophorone ND 180 18 ug/kg
91-57-6 2-Methylnaphthalene ND 180 18 ug/kg
88-74-4 2-Nitroaniline ND 180 36 ug/kg
99-09-2 3-Nitroaniline ND 180 36 ug/kg
100-01-6 4-Nitroaniline ND 180 36 ug/kg
91-20-3 Naphthalene ND 180 29 ug/kg
98-95-3 Nitrobenzene ND 180 18 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 180 18 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 180 18 ug/kg
85-01-8 Phenanthrene ND 180 18 ug/kg
129-00-0 Pyrene ND 180 18 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 180 18 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 53%40-102%
4165-62-2 Phenol-d5 62%41-100%
118-79-6 2,4,6-Tribromophenol 69%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-1/0.5-2
Lab Sample ID:F81875-1 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:91.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 61%40-105%
321-60-8 2-Fluorobiphenyl 58%43-107%
1718-51-0 Terphenyl-d14 61%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-1/0.5-2
Lab Sample ID:F81875-1 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8015C Percent Solids:91.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060073.D 1 05/09/11 AH n/a n/a GQR2611
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.11 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 4.9 2.5 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 76%56-136%
98-08-8 aaa-Trifluorotoluene 78%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-1/0.5-2
Lab Sample ID:F81875-1 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8082A SW846 3550C Percent Solids:91.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 XX056070.D 1 05/05/11 NJ 05/04/11 OP37021 GXX866
Run #2
Initial Weight Final Volume
Run #1 30.0 g 10.0 ml
Run #2
PCB List
CAS No.Compound Result RL MDL Units Q
12674-11-2 Aroclor 1016 ND 18 7.3 ug/kg
11104-28-2 Aroclor 1221 ND 18 9.1 ug/kg
11141-16-5 Aroclor 1232 ND 18 9.1 ug/kg
53469-21-9 Aroclor 1242 ND 18 7.3 ug/kg
12672-29-6 Aroclor 1248 ND 18 7.3 ug/kg
11097-69-1 Aroclor 1254 ND 18 7.3 ug/kg
11096-82-5 Aroclor 1260 ND 18 7.3 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 67%44-126%
2051-24-3 Decachlorobiphenyl 77%39-157%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-1/0.5-2
Lab Sample ID:F81875-1 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8015C SW846 3550C Percent Solids:91.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40337.D 1 05/05/11 SJL 05/04/11 OP37017 GZF1663
Run #2
Initial Weight Final Volume
Run #1 30.3 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 9.0 3.6 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 92%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-1/0.5-2
Lab Sample ID:F81875-1 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Percent Solids:91.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony <1.1 1.1 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Arsenic 0.83 0.54 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Barium 110 11 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Beryllium <0.27 0.27 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Cadmium <0.21 0.21 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Chromium 14.8 0.54 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Copper 53.0 1.3 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Lead 3.5 1.1 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Mercury <0.079 0.079 mg/kg 1 05/10/11 05/10/11 LM SW846 7471B 2 SW846 7471B 4
Molybdenum <2.7 2.7 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Nickel 14.9 2.1 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Selenium 1.3 1.1 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Silver <0.54 0.54 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Tin <2.7 2.7 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Zinc 50.0 1.1 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
(1) Instrument QC Batch: MA8926
(2) Instrument QC Batch: MA8935
(3) Prep QC Batch: MP20510
(4) Prep QC Batch: MP20537
RL = Reporting Limit
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Client Sample ID:MW-1/10-11
Lab Sample ID:F81875-2 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8260B Percent Solids:89.0
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 G0072816.D 1 05/10/11 SH n/a n/a VG2720
Run #2
Initial Weight
Run #1 6.41 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone a 38.7 44 18 ug/kg J
71-43-2 Benzene ND 4.4 1.3 ug/kg
75-27-4 Bromodichloromethane ND 4.4 0.96 ug/kg
75-25-2 Bromoform ND 4.4 1.3 ug/kg
108-90-7 Chlorobenzene ND 4.4 0.88 ug/kg
75-00-3 Chloroethane ND 4.4 1.8 ug/kg
67-66-3 Chloroform ND 4.4 1.1 ug/kg
75-15-0 Carbon disulfide ND 4.4 1.8 ug/kg
56-23-5 Carbon tetrachloride ND 4.4 1.6 ug/kg
75-34-3 1,1-Dichloroethane ND 4.4 0.96 ug/kg
75-35-4 1,1-Dichloroethylene ND 4.4 1.2 ug/kg
107-06-2 1,2-Dichloroethane ND 4.4 0.88 ug/kg
78-87-5 1,2-Dichloropropane ND 4.4 1.1 ug/kg
124-48-1 Dibromochloromethane ND 4.4 0.88 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 4.4 1.3 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 4.4 0.88 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 4.4 1.3 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 4.4 0.96 ug/kg
100-41-4 Ethylbenzene ND 4.4 0.88 ug/kg
591-78-6 2-Hexanone ND 22 4.7 ug/kg
108-10-1 4-Methyl-2-pentanone ND 22 4.8 ug/kg
74-83-9 Methyl bromide ND 4.4 1.8 ug/kg
74-87-3 Methyl chloride ND 4.4 1.8 ug/kg
75-09-2 Methylene chloride ND 8.8 4.0 ug/kg
78-93-3 Methyl ethyl ketone 7.5 22 5.3 ug/kg J
100-42-5 Styrene ND 4.4 2.3 ug/kg
71-55-6 1,1,1-Trichloroethane ND 4.4 0.96 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 4.4 1.1 ug/kg
79-00-5 1,1,2-Trichloroethane ND 4.4 0.96 ug/kg
127-18-4 Tetrachloroethylene ND 4.4 0.88 ug/kg
108-88-3 Toluene ND 4.4 1.1 ug/kg
79-01-6 Trichloroethylene ND 4.4 1.1 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-1/10-11
Lab Sample ID:F81875-2 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8260B Percent Solids:89.0
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 4.4 1.3 ug/kg
1330-20-7 Xylene (total)ND 13 2.8 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 94%80-121%
2037-26-5 Toluene-D8 96%71-130%
460-00-4 4-Bromofluorobenzene 120%59-148%
17060-07-0 1,2-Dichloroethane-D4 103%77-123%
(a) ICV outside of control limits.
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-1/10-11
Lab Sample ID:F81875-2 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:89.0
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L051219.D 1 05/05/11 NAF 05/04/11 OP37013 SL2613
Run #2
Initial Weight Final Volume
Run #1 30.1 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 930 330 ug/kg
95-57-8 2-Chlorophenol ND 190 19 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 190 19 ug/kg
120-83-2 2,4-Dichlorophenol ND 190 19 ug/kg
105-67-9 2,4-Dimethylphenol ND 190 24 ug/kg
51-28-5 2,4-Dinitrophenol ND 930 370 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 370 75 ug/kg
95-48-7 2-Methylphenol ND 190 19 ug/kg
3&4-Methylphenol ND 190 27 ug/kg
88-75-5 2-Nitrophenol ND 190 19 ug/kg
100-02-7 4-Nitrophenol ND 930 150 ug/kg
87-86-5 Pentachlorophenol ND 930 220 ug/kg
108-95-2 Phenol ND 190 19 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 190 19 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 190 19 ug/kg
83-32-9 Acenaphthene ND 190 19 ug/kg
208-96-8 Acenaphthylene ND 190 19 ug/kg
120-12-7 Anthracene ND 190 19 ug/kg
56-55-3 Benzo(a)anthracene ND 190 19 ug/kg
50-32-8 Benzo(a)pyrene ND 190 19 ug/kg
205-99-2 Benzo(b)fluoranthene ND 190 19 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 190 19 ug/kg
207-08-9 Benzo(k)fluoranthene ND 190 19 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 190 19 ug/kg
85-68-7 Butyl benzyl phthalate ND 190 37 ug/kg
100-51-6 Benzyl Alcohol ND 190 37 ug/kg
91-58-7 2-Chloronaphthalene ND 190 37 ug/kg
106-47-8 4-Chloroaniline ND 190 19 ug/kg
86-74-8 Carbazole ND 190 19 ug/kg
218-01-9 Chrysene ND 190 19 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 190 19 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 190 19 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-1/10-11
Lab Sample ID:F81875-2 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:89.0
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 190 19 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 190 19 ug/kg
95-50-1 1,2-Dichlorobenzene ND 190 37 ug/kg
541-73-1 1,3-Dichlorobenzene ND 190 37 ug/kg
106-46-7 1,4-Dichlorobenzene ND 190 37 ug/kg
121-14-2 2,4-Dinitrotoluene ND 190 19 ug/kg
606-20-2 2,6-Dinitrotoluene ND 190 22 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 370 37 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 190 19 ug/kg
132-64-9 Dibenzofuran ND 190 19 ug/kg
84-74-2 Di-n-butyl phthalate ND 370 75 ug/kg
117-84-0 Di-n-octyl phthalate ND 190 37 ug/kg
84-66-2 Diethyl phthalate ND 370 75 ug/kg
131-11-3 Dimethyl phthalate ND 190 37 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 370 75 ug/kg
206-44-0 Fluoranthene ND 190 19 ug/kg
86-73-7 Fluorene ND 190 19 ug/kg
118-74-1 Hexachlorobenzene ND 190 19 ug/kg
87-68-3 Hexachlorobutadiene ND 190 37 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 190 82 ug/kg
67-72-1 Hexachloroethane ND 190 37 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 190 19 ug/kg
78-59-1 Isophorone ND 190 19 ug/kg
91-57-6 2-Methylnaphthalene ND 190 19 ug/kg
88-74-4 2-Nitroaniline ND 190 37 ug/kg
99-09-2 3-Nitroaniline ND 190 37 ug/kg
100-01-6 4-Nitroaniline ND 190 37 ug/kg
91-20-3 Naphthalene ND 190 30 ug/kg
98-95-3 Nitrobenzene ND 190 19 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 190 19 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 190 19 ug/kg
85-01-8 Phenanthrene ND 190 19 ug/kg
129-00-0 Pyrene ND 190 19 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 190 19 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 61%40-102%
4165-62-2 Phenol-d5 71%41-100%
118-79-6 2,4,6-Tribromophenol 84%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-1/10-11
Lab Sample ID:F81875-2 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:89.0
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 69%40-105%
321-60-8 2-Fluorobiphenyl 67%43-107%
1718-51-0 Terphenyl-d14 68%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-1/10-11
Lab Sample ID:F81875-2 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8015C Percent Solids:89.0
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060074.D 1 05/09/11 AH n/a n/a GQR2611
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.15 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 5.2 2.6 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 75%56-136%
98-08-8 aaa-Trifluorotoluene 78%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-1/10-11
Lab Sample ID:F81875-2 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8015C SW846 3550C Percent Solids:89.0
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40340.D 1 05/05/11 SJL 05/04/11 OP37017 GZF1663
Run #2
Initial Weight Final Volume
Run #1 30.3 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 9.3 3.7 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 79%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-1/10-11
Lab Sample ID:F81875-2 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Percent Solids:89.0
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony <1.1 1.1 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Arsenic 0.64 0.55 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Barium 22.7 11 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Beryllium <0.27 0.27 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Cadmium <0.22 0.22 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Chromium 7.8 0.55 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Copper 4.7 1.4 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Lead 7.2 1.1 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Mercury <0.083 0.083 mg/kg 1 05/10/11 05/10/11 LM SW846 7471B 2 SW846 7471B 4
Molybdenum <2.7 2.7 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Nickel <2.2 2.2 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Selenium <1.1 1.1 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Silver <0.55 0.55 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Tin <2.7 2.7 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Zinc 3.6 1.1 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
(1) Instrument QC Batch: MA8926
(2) Instrument QC Batch: MA8935
(3) Prep QC Batch: MP20510
(4) Prep QC Batch: MP20537
RL = Reporting Limit
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Client Sample ID:TB-04/27/11
Lab Sample ID:F81875-3 Date Sampled:04/27/11
Matrix:SO - Trip Blank Soil Date Received:04/28/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 G0072788.D 1 05/09/11 SH n/a n/a VG2719
Run #2
Initial Weight
Run #1 5.00 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 50 20 ug/kg
71-43-2 Benzene ND 5.0 1.5 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.1 ug/kg
75-25-2 Bromoform ND 5.0 1.5 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.2 ug/kg
75-15-0 Carbon disulfide ND 5.0 2.0 ug/kg
56-23-5 Carbon tetrachloride ND 5.0 1.8 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.1 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.4 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.2 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.5 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.5 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.1 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg
591-78-6 2-Hexanone ND 25 5.4 ug/kg
108-10-1 4-Methyl-2-pentanone ND 25 5.5 ug/kg
74-83-9 Methyl bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl chloride ND 5.0 2.0 ug/kg
75-09-2 Methylene chloride ND 10 4.6 ug/kg
78-93-3 Methyl ethyl ketone ND 25 6.1 ug/kg
100-42-5 Styrene ND 5.0 2.6 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.1 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.2 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.1 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.0 ug/kg
108-88-3 Toluene ND 5.0 1.2 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.2 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:TB-04/27/11
Lab Sample ID:F81875-3 Date Sampled:04/27/11
Matrix:SO - Trip Blank Soil Date Received:04/28/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 5.0 1.5 ug/kg
1330-20-7 Xylene (total)ND 15 3.2 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%80-121%
2037-26-5 Toluene-D8 88%71-130%
460-00-4 4-Bromofluorobenzene 101%59-148%
17060-07-0 1,2-Dichloroethane-D4 102%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest LabLink@128732 10:20 16-Feb-2012
Report of Analysis Page 1 of 2
Client Sample ID:MW-2/0.5-2
Lab Sample ID:F81875-4 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8260B Percent Solids:86.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 G0072791.D 1 05/09/11 SH n/a n/a VG2719
Run #2
Initial Weight
Run #1 5.93 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 49 19 ug/kg
71-43-2 Benzene ND 4.9 1.5 ug/kg
75-27-4 Bromodichloromethane ND 4.9 1.1 ug/kg
75-25-2 Bromoform ND 4.9 1.5 ug/kg
108-90-7 Chlorobenzene ND 4.9 0.97 ug/kg
75-00-3 Chloroethane ND 4.9 1.9 ug/kg
67-66-3 Chloroform ND 4.9 1.2 ug/kg
75-15-0 Carbon disulfide ND 4.9 1.9 ug/kg
56-23-5 Carbon tetrachloride ND 4.9 1.8 ug/kg
75-34-3 1,1-Dichloroethane ND 4.9 1.1 ug/kg
75-35-4 1,1-Dichloroethylene ND 4.9 1.4 ug/kg
107-06-2 1,2-Dichloroethane ND 4.9 0.97 ug/kg
78-87-5 1,2-Dichloropropane ND 4.9 1.2 ug/kg
124-48-1 Dibromochloromethane ND 4.9 0.97 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 4.9 1.5 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 4.9 0.97 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 4.9 1.5 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 4.9 1.1 ug/kg
100-41-4 Ethylbenzene ND 4.9 0.97 ug/kg
591-78-6 2-Hexanone ND 24 5.3 ug/kg
108-10-1 4-Methyl-2-pentanone ND 24 5.4 ug/kg
74-83-9 Methyl bromide ND 4.9 1.9 ug/kg
74-87-3 Methyl chloride ND 4.9 1.9 ug/kg
75-09-2 Methylene chloride ND 9.7 4.5 ug/kg
78-93-3 Methyl ethyl ketone ND 24 5.9 ug/kg
100-42-5 Styrene ND 4.9 2.5 ug/kg
71-55-6 1,1,1-Trichloroethane ND 4.9 1.1 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 4.9 1.2 ug/kg
79-00-5 1,1,2-Trichloroethane ND 4.9 1.1 ug/kg
127-18-4 Tetrachloroethylene ND 4.9 0.97 ug/kg
108-88-3 Toluene ND 4.9 1.2 ug/kg
79-01-6 Trichloroethylene ND 4.9 1.2 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest LabLink@128732 10:20 16-Feb-2012
Report of Analysis Page 2 of 2
Client Sample ID:MW-2/0.5-2
Lab Sample ID:F81875-4 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8260B Percent Solids:86.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 4.9 1.5 ug/kg
1330-20-7 Xylene (total)ND 15 3.1 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%80-121%
2037-26-5 Toluene-D8 90%71-130%
460-00-4 4-Bromofluorobenzene 109%59-148%
17060-07-0 1,2-Dichloroethane-D4 102%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest LabLink@128732 10:20 16-Feb-2012
Report of Analysis Page 1 of 3
Client Sample ID:MW-2/0.5-2
Lab Sample ID:F81875-4 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:86.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X018007.D 1 05/06/11 NAF 05/04/11 OP37013 SX889
Run #2
Initial Weight Final Volume
Run #1 30.1 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 960 340 ug/kg
95-57-8 2-Chlorophenol ND 190 19 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 190 19 ug/kg
120-83-2 2,4-Dichlorophenol ND 190 19 ug/kg
105-67-9 2,4-Dimethylphenol ND 190 24 ug/kg
51-28-5 2,4-Dinitrophenol ND 960 380 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 380 77 ug/kg
95-48-7 2-Methylphenol ND 190 19 ug/kg
3&4-Methylphenol ND 190 28 ug/kg
88-75-5 2-Nitrophenol ND 190 19 ug/kg
100-02-7 4-Nitrophenol ND 960 150 ug/kg
87-86-5 Pentachlorophenol ND 960 230 ug/kg
108-95-2 Phenol ND 190 19 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 190 19 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 190 19 ug/kg
83-32-9 Acenaphthene ND 190 19 ug/kg
208-96-8 Acenaphthylene ND 190 19 ug/kg
120-12-7 Anthracene ND 190 19 ug/kg
56-55-3 Benzo(a)anthracene ND 190 19 ug/kg
50-32-8 Benzo(a)pyrene ND 190 19 ug/kg
205-99-2 Benzo(b)fluoranthene ND 190 19 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 190 19 ug/kg
207-08-9 Benzo(k)fluoranthene ND 190 19 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 190 19 ug/kg
85-68-7 Butyl benzyl phthalate ND 190 38 ug/kg
100-51-6 Benzyl Alcohol ND 190 38 ug/kg
91-58-7 2-Chloronaphthalene ND 190 38 ug/kg
106-47-8 4-Chloroaniline ND 190 19 ug/kg
86-74-8 Carbazole ND 190 19 ug/kg
218-01-9 Chrysene ND 190 19 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 190 19 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 190 19 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest LabLink@128732 10:20 16-Feb-2012
Report of Analysis Page 2 of 3
Client Sample ID:MW-2/0.5-2
Lab Sample ID:F81875-4 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:86.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 190 19 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 190 19 ug/kg
95-50-1 1,2-Dichlorobenzene ND 190 38 ug/kg
541-73-1 1,3-Dichlorobenzene ND 190 38 ug/kg
106-46-7 1,4-Dichlorobenzene ND 190 38 ug/kg
121-14-2 2,4-Dinitrotoluene ND 190 19 ug/kg
606-20-2 2,6-Dinitrotoluene ND 190 23 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 380 38 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 190 19 ug/kg
132-64-9 Dibenzofuran ND 190 19 ug/kg
84-74-2 Di-n-butyl phthalate ND 380 77 ug/kg
117-84-0 Di-n-octyl phthalate ND 190 38 ug/kg
84-66-2 Diethyl phthalate ND 380 77 ug/kg
131-11-3 Dimethyl phthalate ND 190 38 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 380 77 ug/kg
206-44-0 Fluoranthene ND 190 19 ug/kg
86-73-7 Fluorene ND 190 19 ug/kg
118-74-1 Hexachlorobenzene ND 190 19 ug/kg
87-68-3 Hexachlorobutadiene ND 190 38 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 190 84 ug/kg
67-72-1 Hexachloroethane ND 190 38 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 190 19 ug/kg
78-59-1 Isophorone ND 190 19 ug/kg
91-57-6 2-Methylnaphthalene ND 190 19 ug/kg
88-74-4 2-Nitroaniline ND 190 38 ug/kg
99-09-2 3-Nitroaniline ND 190 38 ug/kg
100-01-6 4-Nitroaniline ND 190 38 ug/kg
91-20-3 Naphthalene ND 190 31 ug/kg
98-95-3 Nitrobenzene ND 190 19 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 190 19 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 190 19 ug/kg
85-01-8 Phenanthrene ND 190 19 ug/kg
129-00-0 Pyrene ND 190 19 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 190 19 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 60%40-102%
4165-62-2 Phenol-d5 71%41-100%
118-79-6 2,4,6-Tribromophenol 69%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest LabLink@128732 10:20 16-Feb-2012
Report of Analysis Page 3 of 3
Client Sample ID:MW-2/0.5-2
Lab Sample ID:F81875-4 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:86.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 65%40-105%
321-60-8 2-Fluorobiphenyl 67%43-107%
1718-51-0 Terphenyl-d14 75%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest LabLink@128732 10:20 16-Feb-2012
Report of Analysis Page 1 of 1
Client Sample ID:MW-2/0.5-2
Lab Sample ID:F81875-4 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8015C Percent Solids:86.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060075.D 1 05/09/11 AH n/a n/a GQR2611
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.52 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 5.2 2.6 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 80%56-136%
98-08-8 aaa-Trifluorotoluene 80%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest LabLink@128732 10:20 16-Feb-2012
Report of Analysis Page 1 of 1
Client Sample ID:MW-2/0.5-2
Lab Sample ID:F81875-4 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8082A SW846 3550C Percent Solids:86.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 XX056071.D 1 05/05/11 NJ 05/04/11 OP37021 GXX866
Run #2
Initial Weight Final Volume
Run #1 30.3 g 10.0 ml
Run #2
PCB List
CAS No.Compound Result RL MDL Units Q
12674-11-2 Aroclor 1016 ND 19 7.6 ug/kg
11104-28-2 Aroclor 1221 ND 19 9.5 ug/kg
11141-16-5 Aroclor 1232 ND 19 9.5 ug/kg
53469-21-9 Aroclor 1242 ND 19 7.6 ug/kg
12672-29-6 Aroclor 1248 ND 19 7.6 ug/kg
11097-69-1 Aroclor 1254 ND 19 7.6 ug/kg
11096-82-5 Aroclor 1260 ND 19 7.6 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 85%44-126%
2051-24-3 Decachlorobiphenyl 97%39-157%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest LabLink@128732 10:20 16-Feb-2012
Report of Analysis Page 1 of 1
Client Sample ID:MW-2/0.5-2
Lab Sample ID:F81875-4 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8015C SW846 3550C Percent Solids:86.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40341.D 1 05/05/11 SJL 05/04/11 OP37017 GZF1663
Run #2
Initial Weight Final Volume
Run #1 30.1 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 9.6 3.8 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 100%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest LabLink@128732 10:20 16-Feb-2012
Report of Analysis Page 1 of 1
Client Sample ID:MW-2/0.5-2
Lab Sample ID:F81875-4 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Percent Solids:86.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <5.7 5.7 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Arsenic a <2.8 2.8 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Barium a 86.0 57 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Beryllium a <1.4 1.4 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Cadmium a <1.1 1.1 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Chromium a 27.9 2.8 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Copper a 16.6 7.1 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Lead 19.7 1.1 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 4
Mercury <0.090 0.090 mg/kg 1 05/10/11 05/10/11 LM SW846 7471B 3 SW846 7471B 5
Molybdenum a <14 14 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Nickel a <11 11 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Selenium a <5.7 5.7 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Silver a <2.8 2.8 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Tin a <14 14 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Zinc a 13.6 5.7 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
(1) Instrument QC Batch: MA8926
(2) Instrument QC Batch: MA8929
(3) Instrument QC Batch: MA8935
(4) Prep QC Batch: MP20510
(5) Prep QC Batch: MP20537
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Accutest LabLink@128732 10:20 16-Feb-2012
Report of Analysis Page 1 of 2
Client Sample ID:MW-2/10-12
Lab Sample ID:F81875-5 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8260B Percent Solids:82.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 G0072792.D 1 05/09/11 SH n/a n/a VG2719
Run #2
Initial Weight
Run #1 5.88 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 51 21 ug/kg
71-43-2 Benzene ND 5.1 1.5 ug/kg
75-27-4 Bromodichloromethane ND 5.1 1.1 ug/kg
75-25-2 Bromoform ND 5.1 1.5 ug/kg
108-90-7 Chlorobenzene ND 5.1 1.0 ug/kg
75-00-3 Chloroethane ND 5.1 2.1 ug/kg
67-66-3 Chloroform ND 5.1 1.2 ug/kg
75-15-0 Carbon disulfide ND 5.1 2.1 ug/kg
56-23-5 Carbon tetrachloride ND 5.1 1.9 ug/kg
75-34-3 1,1-Dichloroethane ND 5.1 1.1 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.1 1.4 ug/kg
107-06-2 1,2-Dichloroethane ND 5.1 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.1 1.2 ug/kg
124-48-1 Dibromochloromethane ND 5.1 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.1 1.5 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.1 1.0 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.1 1.5 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.1 1.1 ug/kg
100-41-4 Ethylbenzene ND 5.1 1.0 ug/kg
591-78-6 2-Hexanone ND 26 5.6 ug/kg
108-10-1 4-Methyl-2-pentanone ND 26 5.7 ug/kg
74-83-9 Methyl bromide ND 5.1 2.1 ug/kg
74-87-3 Methyl chloride ND 5.1 2.1 ug/kg
75-09-2 Methylene chloride ND 10 4.7 ug/kg
78-93-3 Methyl ethyl ketone ND 26 6.3 ug/kg
100-42-5 Styrene ND 5.1 2.7 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.1 1.1 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.1 1.2 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.1 1.1 ug/kg
127-18-4 Tetrachloroethylene ND 5.1 1.0 ug/kg
108-88-3 Toluene ND 5.1 1.2 ug/kg
79-01-6 Trichloroethylene ND 5.1 1.2 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest LabLink@128732 10:20 16-Feb-2012
Report of Analysis Page 2 of 2
Client Sample ID:MW-2/10-12
Lab Sample ID:F81875-5 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8260B Percent Solids:82.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 5.1 1.5 ug/kg
1330-20-7 Xylene (total)ND 15 3.3 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 93%80-121%
2037-26-5 Toluene-D8 91%71-130%
460-00-4 4-Bromofluorobenzene 98%59-148%
17060-07-0 1,2-Dichloroethane-D4 98%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest LabLink@128732 10:20 16-Feb-2012
Report of Analysis Page 1 of 3
Client Sample ID:MW-2/10-12
Lab Sample ID:F81875-5 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:82.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X018008.D 1 05/06/11 NAF 05/04/11 OP37013 SX889
Run #2
Initial Weight Final Volume
Run #1 30.1 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1000 350 ug/kg
95-57-8 2-Chlorophenol ND 200 20 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 200 20 ug/kg
120-83-2 2,4-Dichlorophenol ND 200 20 ug/kg
105-67-9 2,4-Dimethylphenol ND 200 25 ug/kg
51-28-5 2,4-Dinitrophenol ND 1000 400 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 400 80 ug/kg
95-48-7 2-Methylphenol ND 200 20 ug/kg
3&4-Methylphenol ND 200 29 ug/kg
88-75-5 2-Nitrophenol ND 200 20 ug/kg
100-02-7 4-Nitrophenol ND 1000 160 ug/kg
87-86-5 Pentachlorophenol ND 1000 240 ug/kg
108-95-2 Phenol ND 200 20 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 200 20 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 200 20 ug/kg
83-32-9 Acenaphthene ND 200 20 ug/kg
208-96-8 Acenaphthylene ND 200 20 ug/kg
120-12-7 Anthracene ND 200 20 ug/kg
56-55-3 Benzo(a)anthracene ND 200 20 ug/kg
50-32-8 Benzo(a)pyrene ND 200 20 ug/kg
205-99-2 Benzo(b)fluoranthene ND 200 20 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 200 20 ug/kg
207-08-9 Benzo(k)fluoranthene ND 200 20 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 200 20 ug/kg
85-68-7 Butyl benzyl phthalate ND 200 40 ug/kg
100-51-6 Benzyl Alcohol ND 200 40 ug/kg
91-58-7 2-Chloronaphthalene ND 200 40 ug/kg
106-47-8 4-Chloroaniline ND 200 20 ug/kg
86-74-8 Carbazole ND 200 20 ug/kg
218-01-9 Chrysene ND 200 20 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 200 20 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 200 20 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest LabLink@128732 10:20 16-Feb-2012
Report of Analysis Page 2 of 3
Client Sample ID:MW-2/10-12
Lab Sample ID:F81875-5 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:82.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 200 20 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 200 20 ug/kg
95-50-1 1,2-Dichlorobenzene ND 200 40 ug/kg
541-73-1 1,3-Dichlorobenzene ND 200 40 ug/kg
106-46-7 1,4-Dichlorobenzene ND 200 40 ug/kg
121-14-2 2,4-Dinitrotoluene ND 200 20 ug/kg
606-20-2 2,6-Dinitrotoluene ND 200 24 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 400 40 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 200 20 ug/kg
132-64-9 Dibenzofuran ND 200 20 ug/kg
84-74-2 Di-n-butyl phthalate ND 400 80 ug/kg
117-84-0 Di-n-octyl phthalate ND 200 40 ug/kg
84-66-2 Diethyl phthalate ND 400 80 ug/kg
131-11-3 Dimethyl phthalate ND 200 40 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 400 80 ug/kg
206-44-0 Fluoranthene ND 200 20 ug/kg
86-73-7 Fluorene ND 200 20 ug/kg
118-74-1 Hexachlorobenzene ND 200 20 ug/kg
87-68-3 Hexachlorobutadiene ND 200 40 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 200 88 ug/kg
67-72-1 Hexachloroethane ND 200 40 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 200 20 ug/kg
78-59-1 Isophorone ND 200 20 ug/kg
91-57-6 2-Methylnaphthalene ND 200 20 ug/kg
88-74-4 2-Nitroaniline ND 200 40 ug/kg
99-09-2 3-Nitroaniline ND 200 40 ug/kg
100-01-6 4-Nitroaniline ND 200 40 ug/kg
91-20-3 Naphthalene ND 200 32 ug/kg
98-95-3 Nitrobenzene ND 200 20 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 200 20 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 200 20 ug/kg
85-01-8 Phenanthrene ND 200 20 ug/kg
129-00-0 Pyrene ND 200 20 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 200 20 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 69%40-102%
4165-62-2 Phenol-d5 82%41-100%
118-79-6 2,4,6-Tribromophenol 75%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-2/10-12
Lab Sample ID:F81875-5 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:82.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 73%40-105%
321-60-8 2-Fluorobiphenyl 75%43-107%
1718-51-0 Terphenyl-d14 80%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-2/10-12
Lab Sample ID:F81875-5 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8015C Percent Solids:82.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060076.D 1 05/09/11 AH n/a n/a GQR2611
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.32 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 6.7 3.4 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 79%56-136%
98-08-8 aaa-Trifluorotoluene 77%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-2/10-12
Lab Sample ID:F81875-5 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8015C SW846 3550C Percent Solids:82.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40342.D 1 05/05/11 SJL 05/04/11 OP37017 GZF1663
Run #2
Initial Weight Final Volume
Run #1 30.4 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 10 4.0 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 96%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-2/10-12
Lab Sample ID:F81875-5 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Percent Solids:82.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <2.3 2.3 mg/kg 2 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Arsenic a <1.1 1.1 mg/kg 2 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Barium a 141 23 mg/kg 2 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Beryllium a <0.57 0.57 mg/kg 2 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Cadmium a <0.45 0.45 mg/kg 2 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Chromium a 26.2 1.1 mg/kg 2 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Copper a 56.8 2.8 mg/kg 2 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Lead 6.6 1.1 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 4
Mercury <0.098 0.098 mg/kg 1 05/10/11 05/10/11 LM SW846 7471B 3 SW846 7471B 5
Molybdenum a <5.7 5.7 mg/kg 2 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Nickel a 15.2 4.5 mg/kg 2 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Selenium a <2.3 2.3 mg/kg 2 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Silver a <1.1 1.1 mg/kg 2 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Tin a <5.7 5.7 mg/kg 2 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Zinc a 41.5 2.3 mg/kg 2 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
(1) Instrument QC Batch: MA8926
(2) Instrument QC Batch: MA8929
(3) Instrument QC Batch: MA8935
(4) Prep QC Batch: MP20510
(5) Prep QC Batch: MP20537
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Report of Analysis Page 1 of 2
Client Sample ID:MW-3/0.5-2
Lab Sample ID:F81875-6 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8260B Percent Solids:71.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 G0072793.D 1 05/09/11 SH n/a n/a VG2719
Run #2
Initial Weight
Run #1 5.17 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 67 27 ug/kg
71-43-2 Benzene ND 6.7 2.0 ug/kg
75-27-4 Bromodichloromethane ND 6.7 1.5 ug/kg
75-25-2 Bromoform ND 6.7 2.0 ug/kg
108-90-7 Chlorobenzene ND 6.7 1.3 ug/kg
75-00-3 Chloroethane ND 6.7 2.7 ug/kg
67-66-3 Chloroform ND 6.7 1.6 ug/kg
75-15-0 Carbon disulfide ND 6.7 2.7 ug/kg
56-23-5 Carbon tetrachloride ND 6.7 2.4 ug/kg
75-34-3 1,1-Dichloroethane ND 6.7 1.5 ug/kg
75-35-4 1,1-Dichloroethylene ND 6.7 1.9 ug/kg
107-06-2 1,2-Dichloroethane ND 6.7 1.3 ug/kg
78-87-5 1,2-Dichloropropane ND 6.7 1.6 ug/kg
124-48-1 Dibromochloromethane ND 6.7 1.3 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 6.7 2.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 6.7 1.3 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 6.7 2.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 6.7 1.5 ug/kg
100-41-4 Ethylbenzene ND 6.7 1.3 ug/kg
591-78-6 2-Hexanone ND 34 7.3 ug/kg
108-10-1 4-Methyl-2-pentanone ND 34 7.4 ug/kg
74-83-9 Methyl bromide ND 6.7 2.7 ug/kg
74-87-3 Methyl chloride ND 6.7 2.7 ug/kg
75-09-2 Methylene chloride ND 13 6.2 ug/kg
78-93-3 Methyl ethyl ketone ND 34 8.2 ug/kg
100-42-5 Styrene ND 6.7 3.5 ug/kg
71-55-6 1,1,1-Trichloroethane ND 6.7 1.5 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 6.7 1.6 ug/kg
79-00-5 1,1,2-Trichloroethane ND 6.7 1.5 ug/kg
127-18-4 Tetrachloroethylene ND 6.7 1.3 ug/kg
108-88-3 Toluene ND 6.7 1.6 ug/kg
79-01-6 Trichloroethylene ND 6.7 1.6 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-3/0.5-2
Lab Sample ID:F81875-6 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8260B Percent Solids:71.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 6.7 2.0 ug/kg
1330-20-7 Xylene (total)ND 20 4.3 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 96%80-121%
2037-26-5 Toluene-D8 88%71-130%
460-00-4 4-Bromofluorobenzene 102%59-148%
17060-07-0 1,2-Dichloroethane-D4 100%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-3/0.5-2
Lab Sample ID:F81875-6 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:71.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L051248.D 1 05/09/11 NAF 05/05/11 OP37029 SL2615
Run #2
Initial Weight Final Volume
Run #1 30.2 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1200 410 ug/kg
95-57-8 2-Chlorophenol ND 230 23 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 230 23 ug/kg
120-83-2 2,4-Dichlorophenol ND 230 23 ug/kg
105-67-9 2,4-Dimethylphenol ND 230 29 ug/kg
51-28-5 2,4-Dinitrophenol ND 1200 460 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 460 92 ug/kg
95-48-7 2-Methylphenol ND 230 23 ug/kg
3&4-Methylphenol ND 230 33 ug/kg
88-75-5 2-Nitrophenol ND 230 23 ug/kg
100-02-7 4-Nitrophenol ND 1200 180 ug/kg
87-86-5 Pentachlorophenol ND 1200 280 ug/kg
108-95-2 Phenol ND 230 23 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 230 23 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 230 23 ug/kg
83-32-9 Acenaphthene ND 230 23 ug/kg
208-96-8 Acenaphthylene ND 230 23 ug/kg
120-12-7 Anthracene ND 230 23 ug/kg
56-55-3 Benzo(a)anthracene ND 230 23 ug/kg
50-32-8 Benzo(a)pyrene ND 230 23 ug/kg
205-99-2 Benzo(b)fluoranthene ND 230 23 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 230 23 ug/kg
207-08-9 Benzo(k)fluoranthene ND 230 23 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 230 23 ug/kg
85-68-7 Butyl benzyl phthalate ND 230 46 ug/kg
100-51-6 Benzyl Alcohol ND 230 46 ug/kg
91-58-7 2-Chloronaphthalene ND 230 46 ug/kg
106-47-8 4-Chloroaniline ND 230 23 ug/kg
86-74-8 Carbazole ND 230 23 ug/kg
218-01-9 Chrysene ND 230 23 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 230 23 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 230 23 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-3/0.5-2
Lab Sample ID:F81875-6 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:71.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 230 23 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 230 23 ug/kg
95-50-1 1,2-Dichlorobenzene ND 230 46 ug/kg
541-73-1 1,3-Dichlorobenzene ND 230 46 ug/kg
106-46-7 1,4-Dichlorobenzene ND 230 46 ug/kg
121-14-2 2,4-Dinitrotoluene ND 230 23 ug/kg
606-20-2 2,6-Dinitrotoluene ND 230 27 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 460 46 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 230 23 ug/kg
132-64-9 Dibenzofuran ND 230 23 ug/kg
84-74-2 Di-n-butyl phthalate ND 460 92 ug/kg
117-84-0 Di-n-octyl phthalate ND 230 46 ug/kg
84-66-2 Diethyl phthalate ND 460 92 ug/kg
131-11-3 Dimethyl phthalate ND 230 46 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 460 92 ug/kg
206-44-0 Fluoranthene ND 230 23 ug/kg
86-73-7 Fluorene ND 230 23 ug/kg
118-74-1 Hexachlorobenzene ND 230 23 ug/kg
87-68-3 Hexachlorobutadiene ND 230 46 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 230 100 ug/kg
67-72-1 Hexachloroethane ND 230 46 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 230 23 ug/kg
78-59-1 Isophorone ND 230 23 ug/kg
91-57-6 2-Methylnaphthalene ND 230 23 ug/kg
88-74-4 2-Nitroaniline ND 230 46 ug/kg
99-09-2 3-Nitroaniline ND 230 46 ug/kg
100-01-6 4-Nitroaniline ND 230 46 ug/kg
91-20-3 Naphthalene ND 230 37 ug/kg
98-95-3 Nitrobenzene ND 230 23 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 230 23 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 230 23 ug/kg
85-01-8 Phenanthrene ND 230 23 ug/kg
129-00-0 Pyrene ND 230 23 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 230 23 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 59%40-102%
4165-62-2 Phenol-d5 73%41-100%
118-79-6 2,4,6-Tribromophenol 80%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-3/0.5-2
Lab Sample ID:F81875-6 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:71.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 69%40-105%
321-60-8 2-Fluorobiphenyl 71%43-107%
1718-51-0 Terphenyl-d14 74%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest LabLink@128732 10:20 16-Feb-2012
Report of Analysis Page 1 of 1
Client Sample ID:MW-3/0.5-2
Lab Sample ID:F81875-6 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8015C Percent Solids:71.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060077.D 1 05/09/11 AH n/a n/a GQR2611
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.13 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 8.7 4.4 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 80%56-136%
98-08-8 aaa-Trifluorotoluene 78%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-3/0.5-2
Lab Sample ID:F81875-6 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8082A SW846 3550C Percent Solids:71.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 XX056072.D 1 05/05/11 NJ 05/04/11 OP37021 GXX866
Run #2
Initial Weight Final Volume
Run #1 30.3 g 10.0 ml
Run #2
PCB List
CAS No.Compound Result RL MDL Units Q
12674-11-2 Aroclor 1016 ND 23 9.2 ug/kg
11104-28-2 Aroclor 1221 ND 23 11 ug/kg
11141-16-5 Aroclor 1232 ND 23 11 ug/kg
53469-21-9 Aroclor 1242 ND 23 9.2 ug/kg
12672-29-6 Aroclor 1248 ND 23 9.2 ug/kg
11097-69-1 Aroclor 1254 ND 23 9.2 ug/kg
11096-82-5 Aroclor 1260 ND 23 9.2 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 71%44-126%
2051-24-3 Decachlorobiphenyl 87%39-157%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-3/0.5-2
Lab Sample ID:F81875-6 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8015C SW846 3550C Percent Solids:71.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40343.D 1 05/05/11 SJL 05/04/11 OP37017 GZF1663
Run #2
Initial Weight Final Volume
Run #1 30.2 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 12 4.6 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 89%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest LabLink@128732 10:20 16-Feb-2012
Report of Analysis Page 1 of 1
Client Sample ID:MW-3/0.5-2
Lab Sample ID:F81875-6 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Percent Solids:71.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <13 13 mg/kg 10 05/05/11 05/06/11 RS SW846 6010C 1 SW846 3050B 3
Arsenic a <6.5 6.5 mg/kg 10 05/05/11 05/06/11 RS SW846 6010C 1 SW846 3050B 3
Barium a <130 130 mg/kg 10 05/05/11 05/06/11 RS SW846 6010C 1 SW846 3050B 3
Beryllium a <3.2 3.2 mg/kg 10 05/05/11 05/06/11 RS SW846 6010C 1 SW846 3050B 3
Cadmium a <2.6 2.6 mg/kg 10 05/05/11 05/06/11 RS SW846 6010C 1 SW846 3050B 3
Chromium a 74.2 6.5 mg/kg 10 05/05/11 05/06/11 RS SW846 6010C 1 SW846 3050B 3
Copper a 242 16 mg/kg 10 05/05/11 05/06/11 RS SW846 6010C 1 SW846 3050B 3
Lead a 14.6 6.5 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 1 SW846 3050B 3
Mercury <0.12 0.12 mg/kg 1 05/10/11 05/10/11 LM SW846 7471B 2 SW846 7471B 4
Molybdenum a <32 32 mg/kg 10 05/05/11 05/06/11 RS SW846 6010C 1 SW846 3050B 3
Nickel a <26 26 mg/kg 10 05/05/11 05/06/11 RS SW846 6010C 1 SW846 3050B 3
Selenium a <13 13 mg/kg 10 05/05/11 05/06/11 RS SW846 6010C 1 SW846 3050B 3
Silver a <6.5 6.5 mg/kg 10 05/05/11 05/06/11 RS SW846 6010C 1 SW846 3050B 3
Tin a <32 32 mg/kg 10 05/05/11 05/06/11 RS SW846 6010C 1 SW846 3050B 3
Zinc a 32.0 13 mg/kg 10 05/05/11 05/06/11 RS SW846 6010C 1 SW846 3050B 3
(1) Instrument QC Batch: MA8929
(2) Instrument QC Batch: MA8935
(3) Prep QC Batch: MP20510
(4) Prep QC Batch: MP20537
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Report of Analysis Page 1 of 2
Client Sample ID:MW-3/11-12
Lab Sample ID:F81875-7 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8260B Percent Solids:71.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 G0072794.D 1 05/09/11 SH n/a n/a VG2719
Run #2
Initial Weight
Run #1 5.01 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 70 28 ug/kg
71-43-2 Benzene ND 7.0 2.1 ug/kg
75-27-4 Bromodichloromethane ND 7.0 1.5 ug/kg
75-25-2 Bromoform ND 7.0 2.1 ug/kg
108-90-7 Chlorobenzene ND 7.0 1.4 ug/kg
75-00-3 Chloroethane ND 7.0 2.8 ug/kg
67-66-3 Chloroform ND 7.0 1.7 ug/kg
75-15-0 Carbon disulfide ND 7.0 2.8 ug/kg
56-23-5 Carbon tetrachloride ND 7.0 2.5 ug/kg
75-34-3 1,1-Dichloroethane ND 7.0 1.5 ug/kg
75-35-4 1,1-Dichloroethylene ND 7.0 2.0 ug/kg
107-06-2 1,2-Dichloroethane ND 7.0 1.4 ug/kg
78-87-5 1,2-Dichloropropane ND 7.0 1.7 ug/kg
124-48-1 Dibromochloromethane ND 7.0 1.4 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 7.0 2.1 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 7.0 1.4 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 7.0 2.1 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 7.0 1.5 ug/kg
100-41-4 Ethylbenzene ND 7.0 1.4 ug/kg
591-78-6 2-Hexanone ND 35 7.5 ug/kg
108-10-1 4-Methyl-2-pentanone ND 35 7.7 ug/kg
74-83-9 Methyl bromide ND 7.0 2.8 ug/kg
74-87-3 Methyl chloride ND 7.0 2.8 ug/kg
75-09-2 Methylene chloride ND 14 6.4 ug/kg
78-93-3 Methyl ethyl ketone ND 35 8.5 ug/kg
100-42-5 Styrene ND 7.0 3.6 ug/kg
71-55-6 1,1,1-Trichloroethane ND 7.0 1.5 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 7.0 1.7 ug/kg
79-00-5 1,1,2-Trichloroethane ND 7.0 1.5 ug/kg
127-18-4 Tetrachloroethylene ND 7.0 1.4 ug/kg
108-88-3 Toluene ND 7.0 1.7 ug/kg
79-01-6 Trichloroethylene ND 7.0 1.7 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-3/11-12
Lab Sample ID:F81875-7 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8260B Percent Solids:71.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 7.0 2.1 ug/kg
1330-20-7 Xylene (total)ND 21 4.5 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%80-121%
2037-26-5 Toluene-D8 85%71-130%
460-00-4 4-Bromofluorobenzene 99%59-148%
17060-07-0 1,2-Dichloroethane-D4 109%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-3/11-12
Lab Sample ID:F81875-7 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:71.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L051249.D 1 05/09/11 NAF 05/05/11 OP37029 SL2615
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1200 410 ug/kg
95-57-8 2-Chlorophenol ND 230 23 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 230 23 ug/kg
120-83-2 2,4-Dichlorophenol ND 230 23 ug/kg
105-67-9 2,4-Dimethylphenol ND 230 29 ug/kg
51-28-5 2,4-Dinitrophenol ND 1200 470 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 470 93 ug/kg
95-48-7 2-Methylphenol ND 230 23 ug/kg
3&4-Methylphenol ND 230 34 ug/kg
88-75-5 2-Nitrophenol ND 230 23 ug/kg
100-02-7 4-Nitrophenol ND 1200 190 ug/kg
87-86-5 Pentachlorophenol ND 1200 280 ug/kg
108-95-2 Phenol ND 230 23 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 230 23 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 230 23 ug/kg
83-32-9 Acenaphthene ND 230 23 ug/kg
208-96-8 Acenaphthylene ND 230 23 ug/kg
120-12-7 Anthracene ND 230 23 ug/kg
56-55-3 Benzo(a)anthracene ND 230 23 ug/kg
50-32-8 Benzo(a)pyrene ND 230 23 ug/kg
205-99-2 Benzo(b)fluoranthene ND 230 23 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 230 23 ug/kg
207-08-9 Benzo(k)fluoranthene ND 230 23 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 230 23 ug/kg
85-68-7 Butyl benzyl phthalate ND 230 47 ug/kg
100-51-6 Benzyl Alcohol ND 230 47 ug/kg
91-58-7 2-Chloronaphthalene ND 230 47 ug/kg
106-47-8 4-Chloroaniline ND 230 23 ug/kg
86-74-8 Carbazole ND 230 23 ug/kg
218-01-9 Chrysene ND 230 23 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 230 23 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 230 23 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-3/11-12
Lab Sample ID:F81875-7 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:71.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 230 23 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 230 23 ug/kg
95-50-1 1,2-Dichlorobenzene ND 230 47 ug/kg
541-73-1 1,3-Dichlorobenzene ND 230 47 ug/kg
106-46-7 1,4-Dichlorobenzene ND 230 47 ug/kg
121-14-2 2,4-Dinitrotoluene ND 230 23 ug/kg
606-20-2 2,6-Dinitrotoluene ND 230 28 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 470 47 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 230 23 ug/kg
132-64-9 Dibenzofuran ND 230 23 ug/kg
84-74-2 Di-n-butyl phthalate ND 470 93 ug/kg
117-84-0 Di-n-octyl phthalate ND 230 47 ug/kg
84-66-2 Diethyl phthalate ND 470 93 ug/kg
131-11-3 Dimethyl phthalate ND 230 47 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 470 93 ug/kg
206-44-0 Fluoranthene ND 230 23 ug/kg
86-73-7 Fluorene ND 230 23 ug/kg
118-74-1 Hexachlorobenzene ND 230 23 ug/kg
87-68-3 Hexachlorobutadiene ND 230 47 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 230 100 ug/kg
67-72-1 Hexachloroethane ND 230 47 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 230 23 ug/kg
78-59-1 Isophorone ND 230 23 ug/kg
91-57-6 2-Methylnaphthalene ND 230 23 ug/kg
88-74-4 2-Nitroaniline ND 230 47 ug/kg
99-09-2 3-Nitroaniline ND 230 47 ug/kg
100-01-6 4-Nitroaniline ND 230 47 ug/kg
91-20-3 Naphthalene ND 230 37 ug/kg
98-95-3 Nitrobenzene ND 230 23 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 230 23 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 230 23 ug/kg
85-01-8 Phenanthrene ND 230 23 ug/kg
129-00-0 Pyrene ND 230 23 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 230 23 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 64%40-102%
4165-62-2 Phenol-d5 78%41-100%
118-79-6 2,4,6-Tribromophenol 82%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-3/11-12
Lab Sample ID:F81875-7 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:71.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 73%40-105%
321-60-8 2-Fluorobiphenyl 72%43-107%
1718-51-0 Terphenyl-d14 73%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-3/11-12
Lab Sample ID:F81875-7 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8015C Percent Solids:71.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060078.D 1 05/09/11 AH n/a n/a GQR2611
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.29 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 8.6 4.3 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 80%56-136%
98-08-8 aaa-Trifluorotoluene 75%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-3/11-12
Lab Sample ID:F81875-7 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8015C SW846 3550C Percent Solids:71.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40344.D 1 05/05/11 SJL 05/04/11 OP37017 GZF1663
Run #2
Initial Weight Final Volume
Run #1 30.1 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 12 4.6 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 95%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-3/11-12
Lab Sample ID:F81875-7 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Percent Solids:71.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <6.4 6.4 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Arsenic a <3.2 3.2 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Barium a <64 64 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Beryllium a <1.6 1.6 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Cadmium a <1.3 1.3 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Chromium a 55.0 3.2 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Copper a 111 7.9 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Lead 5.6 1.3 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 4
Mercury <0.11 0.11 mg/kg 1 05/10/11 05/10/11 LM SW846 7471B 3 SW846 7471B 5
Molybdenum a <16 16 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Nickel a 18.6 13 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Selenium a <6.4 6.4 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Silver a <3.2 3.2 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Tin a <16 16 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
Zinc a 35.3 6.4 mg/kg 5 05/05/11 05/06/11 RS SW846 6010C 2 SW846 3050B 4
(1) Instrument QC Batch: MA8926
(2) Instrument QC Batch: MA8929
(3) Instrument QC Batch: MA8935
(4) Prep QC Batch: MP20510
(5) Prep QC Batch: MP20537
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Report of Analysis Page 1 of 2
Client Sample ID:MW-4/0.5-2
Lab Sample ID:F81875-8 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8260B Percent Solids:88.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 G0072795.D 1 05/09/11 SH n/a n/a VG2719
Run #2
Initial Weight
Run #1 5.22 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 54 22 ug/kg
71-43-2 Benzene ND 5.4 1.6 ug/kg
75-27-4 Bromodichloromethane ND 5.4 1.2 ug/kg
75-25-2 Bromoform ND 5.4 1.6 ug/kg
108-90-7 Chlorobenzene ND 5.4 1.1 ug/kg
75-00-3 Chloroethane ND 5.4 2.2 ug/kg
67-66-3 Chloroform ND 5.4 1.3 ug/kg
75-15-0 Carbon disulfide ND 5.4 2.2 ug/kg
56-23-5 Carbon tetrachloride ND 5.4 2.0 ug/kg
75-34-3 1,1-Dichloroethane ND 5.4 1.2 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.4 1.5 ug/kg
107-06-2 1,2-Dichloroethane ND 5.4 1.1 ug/kg
78-87-5 1,2-Dichloropropane ND 5.4 1.3 ug/kg
124-48-1 Dibromochloromethane ND 5.4 1.1 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.4 1.6 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.4 1.1 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.4 1.6 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.4 1.2 ug/kg
100-41-4 Ethylbenzene ND 5.4 1.1 ug/kg
591-78-6 2-Hexanone ND 27 5.9 ug/kg
108-10-1 4-Methyl-2-pentanone ND 27 6.0 ug/kg
74-83-9 Methyl bromide ND 5.4 2.2 ug/kg
74-87-3 Methyl chloride ND 5.4 2.2 ug/kg
75-09-2 Methylene chloride ND 11 5.0 ug/kg
78-93-3 Methyl ethyl ketone ND 27 6.6 ug/kg
100-42-5 Styrene ND 5.4 2.8 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.4 1.2 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.4 1.3 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.4 1.2 ug/kg
127-18-4 Tetrachloroethylene ND 5.4 1.1 ug/kg
108-88-3 Toluene ND 5.4 1.3 ug/kg
79-01-6 Trichloroethylene ND 5.4 1.3 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-4/0.5-2
Lab Sample ID:F81875-8 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8260B Percent Solids:88.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 5.4 1.6 ug/kg
1330-20-7 Xylene (total)ND 16 3.5 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%80-121%
2037-26-5 Toluene-D8 87%71-130%
460-00-4 4-Bromofluorobenzene 104%59-148%
17060-07-0 1,2-Dichloroethane-D4 101%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-4/0.5-2
Lab Sample ID:F81875-8 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:88.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L051250.D 1 05/09/11 NAF 05/05/11 OP37029 SL2615
Run #2
Initial Weight Final Volume
Run #1 30.4 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 930 330 ug/kg
95-57-8 2-Chlorophenol ND 190 19 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 190 19 ug/kg
120-83-2 2,4-Dichlorophenol ND 190 19 ug/kg
105-67-9 2,4-Dimethylphenol ND 190 24 ug/kg
51-28-5 2,4-Dinitrophenol ND 930 370 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 370 75 ug/kg
95-48-7 2-Methylphenol ND 190 19 ug/kg
3&4-Methylphenol ND 190 27 ug/kg
88-75-5 2-Nitrophenol ND 190 19 ug/kg
100-02-7 4-Nitrophenol ND 930 150 ug/kg
87-86-5 Pentachlorophenol ND 930 220 ug/kg
108-95-2 Phenol ND 190 19 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 190 19 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 190 19 ug/kg
83-32-9 Acenaphthene ND 190 19 ug/kg
208-96-8 Acenaphthylene ND 190 19 ug/kg
120-12-7 Anthracene ND 190 19 ug/kg
56-55-3 Benzo(a)anthracene ND 190 19 ug/kg
50-32-8 Benzo(a)pyrene ND 190 19 ug/kg
205-99-2 Benzo(b)fluoranthene ND 190 19 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 190 19 ug/kg
207-08-9 Benzo(k)fluoranthene ND 190 19 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 190 19 ug/kg
85-68-7 Butyl benzyl phthalate ND 190 37 ug/kg
100-51-6 Benzyl Alcohol ND 190 37 ug/kg
91-58-7 2-Chloronaphthalene ND 190 37 ug/kg
106-47-8 4-Chloroaniline ND 190 19 ug/kg
86-74-8 Carbazole ND 190 19 ug/kg
218-01-9 Chrysene ND 190 19 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 190 19 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 190 19 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-4/0.5-2
Lab Sample ID:F81875-8 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:88.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 190 19 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 190 19 ug/kg
95-50-1 1,2-Dichlorobenzene ND 190 37 ug/kg
541-73-1 1,3-Dichlorobenzene ND 190 37 ug/kg
106-46-7 1,4-Dichlorobenzene ND 190 37 ug/kg
121-14-2 2,4-Dinitrotoluene ND 190 19 ug/kg
606-20-2 2,6-Dinitrotoluene ND 190 22 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 370 37 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 190 19 ug/kg
132-64-9 Dibenzofuran ND 190 19 ug/kg
84-74-2 Di-n-butyl phthalate ND 370 75 ug/kg
117-84-0 Di-n-octyl phthalate ND 190 37 ug/kg
84-66-2 Diethyl phthalate ND 370 75 ug/kg
131-11-3 Dimethyl phthalate ND 190 37 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 370 75 ug/kg
206-44-0 Fluoranthene ND 190 19 ug/kg
86-73-7 Fluorene ND 190 19 ug/kg
118-74-1 Hexachlorobenzene ND 190 19 ug/kg
87-68-3 Hexachlorobutadiene ND 190 37 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 190 82 ug/kg
67-72-1 Hexachloroethane ND 190 37 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 190 19 ug/kg
78-59-1 Isophorone ND 190 19 ug/kg
91-57-6 2-Methylnaphthalene ND 190 19 ug/kg
88-74-4 2-Nitroaniline ND 190 37 ug/kg
99-09-2 3-Nitroaniline ND 190 37 ug/kg
100-01-6 4-Nitroaniline ND 190 37 ug/kg
91-20-3 Naphthalene ND 190 30 ug/kg
98-95-3 Nitrobenzene ND 190 19 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 190 19 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 190 19 ug/kg
85-01-8 Phenanthrene ND 190 19 ug/kg
129-00-0 Pyrene ND 190 19 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 190 19 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 60%40-102%
4165-62-2 Phenol-d5 74%41-100%
118-79-6 2,4,6-Tribromophenol 80%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-4/0.5-2
Lab Sample ID:F81875-8 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:88.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 71%40-105%
321-60-8 2-Fluorobiphenyl 71%43-107%
1718-51-0 Terphenyl-d14 68%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-4/0.5-2
Lab Sample ID:F81875-8 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8015C Percent Solids:88.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060079.D 1 05/09/11 AH n/a n/a GQR2611
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.42 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 5.9 3.0 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 78%56-136%
98-08-8 aaa-Trifluorotoluene 78%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-4/0.5-2
Lab Sample ID:F81875-8 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8082A SW846 3550C Percent Solids:88.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 XX056073.D 1 05/05/11 NJ 05/04/11 OP37021 GXX866
Run #2
Initial Weight Final Volume
Run #1 30.1 g 10.0 ml
Run #2
PCB List
CAS No.Compound Result RL MDL Units Q
12674-11-2 Aroclor 1016 ND 19 7.5 ug/kg
11104-28-2 Aroclor 1221 ND 19 9.4 ug/kg
11141-16-5 Aroclor 1232 ND 19 9.4 ug/kg
53469-21-9 Aroclor 1242 ND 19 7.5 ug/kg
12672-29-6 Aroclor 1248 ND 19 7.5 ug/kg
11097-69-1 Aroclor 1254 ND 19 7.5 ug/kg
11096-82-5 Aroclor 1260 ND 19 7.5 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 85%44-126%
2051-24-3 Decachlorobiphenyl 94%39-157%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-4/0.5-2
Lab Sample ID:F81875-8 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8015C SW846 3550C Percent Solids:88.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40345.D 1 05/05/11 SJL 05/04/11 OP37017 GZF1663
Run #2
Initial Weight Final Volume
Run #1 30.2 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 9.4 3.8 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 85%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-4/0.5-2
Lab Sample ID:F81875-8 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Percent Solids:88.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony <1.0 1.0 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Arsenic 1.8 0.52 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Barium 24.7 10 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Beryllium <0.26 0.26 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Cadmium <0.21 0.21 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Chromium 31.6 0.52 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Copper 16.7 1.3 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Lead 10.9 1.0 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Mercury <0.083 0.083 mg/kg 1 05/10/11 05/10/11 LM SW846 7471B 2 SW846 7471B 4
Molybdenum <2.6 2.6 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Nickel 4.2 2.1 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Selenium 1.2 1.0 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Silver <0.52 0.52 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Tin <2.6 2.6 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Zinc 10.9 1.0 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
(1) Instrument QC Batch: MA8926
(2) Instrument QC Batch: MA8935
(3) Prep QC Batch: MP20510
(4) Prep QC Batch: MP20537
RL = Reporting Limit
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Report of Analysis Page 1 of 2
Client Sample ID:MW-4/10-12
Lab Sample ID:F81875-9 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8260B Percent Solids:89.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 G0072796.D 1 05/09/11 SH n/a n/a VG2719
Run #2
Initial Weight
Run #1 6.37 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 44 18 ug/kg
71-43-2 Benzene ND 4.4 1.3 ug/kg
75-27-4 Bromodichloromethane ND 4.4 0.96 ug/kg
75-25-2 Bromoform ND 4.4 1.3 ug/kg
108-90-7 Chlorobenzene ND 4.4 0.88 ug/kg
75-00-3 Chloroethane ND 4.4 1.8 ug/kg
67-66-3 Chloroform ND 4.4 1.1 ug/kg
75-15-0 Carbon disulfide ND 4.4 1.8 ug/kg
56-23-5 Carbon tetrachloride ND 4.4 1.6 ug/kg
75-34-3 1,1-Dichloroethane ND 4.4 0.96 ug/kg
75-35-4 1,1-Dichloroethylene ND 4.4 1.2 ug/kg
107-06-2 1,2-Dichloroethane ND 4.4 0.88 ug/kg
78-87-5 1,2-Dichloropropane ND 4.4 1.1 ug/kg
124-48-1 Dibromochloromethane ND 4.4 0.88 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 4.4 1.3 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 4.4 0.88 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 4.4 1.3 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 4.4 0.96 ug/kg
100-41-4 Ethylbenzene ND 4.4 0.88 ug/kg
591-78-6 2-Hexanone ND 22 4.7 ug/kg
108-10-1 4-Methyl-2-pentanone ND 22 4.8 ug/kg
74-83-9 Methyl bromide ND 4.4 1.8 ug/kg
74-87-3 Methyl chloride ND 4.4 1.8 ug/kg
75-09-2 Methylene chloride ND 8.8 4.0 ug/kg
78-93-3 Methyl ethyl ketone ND 22 5.3 ug/kg
100-42-5 Styrene ND 4.4 2.3 ug/kg
71-55-6 1,1,1-Trichloroethane ND 4.4 0.96 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 4.4 1.1 ug/kg
79-00-5 1,1,2-Trichloroethane ND 4.4 0.96 ug/kg
127-18-4 Tetrachloroethylene ND 4.4 0.88 ug/kg
108-88-3 Toluene ND 4.4 1.1 ug/kg
79-01-6 Trichloroethylene ND 4.4 1.1 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-4/10-12
Lab Sample ID:F81875-9 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8260B Percent Solids:89.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 4.4 1.3 ug/kg
1330-20-7 Xylene (total)ND 13 2.8 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%80-121%
2037-26-5 Toluene-D8 87%71-130%
460-00-4 4-Bromofluorobenzene 100%59-148%
17060-07-0 1,2-Dichloroethane-D4 108%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-4/10-12
Lab Sample ID:F81875-9 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:89.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L051251.D 1 05/09/11 NAF 05/05/11 OP37029 SL2615
Run #2
Initial Weight Final Volume
Run #1 30.4 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 920 320 ug/kg
95-57-8 2-Chlorophenol ND 180 18 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 180 18 ug/kg
120-83-2 2,4-Dichlorophenol ND 180 18 ug/kg
105-67-9 2,4-Dimethylphenol ND 180 23 ug/kg
51-28-5 2,4-Dinitrophenol ND 920 370 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 370 73 ug/kg
95-48-7 2-Methylphenol ND 180 18 ug/kg
3&4-Methylphenol ND 180 26 ug/kg
88-75-5 2-Nitrophenol ND 180 18 ug/kg
100-02-7 4-Nitrophenol ND 920 150 ug/kg
87-86-5 Pentachlorophenol ND 920 220 ug/kg
108-95-2 Phenol ND 180 18 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 180 18 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 180 18 ug/kg
83-32-9 Acenaphthene ND 180 18 ug/kg
208-96-8 Acenaphthylene ND 180 18 ug/kg
120-12-7 Anthracene ND 180 18 ug/kg
56-55-3 Benzo(a)anthracene ND 180 18 ug/kg
50-32-8 Benzo(a)pyrene ND 180 18 ug/kg
205-99-2 Benzo(b)fluoranthene ND 180 18 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 180 18 ug/kg
207-08-9 Benzo(k)fluoranthene ND 180 18 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 180 18 ug/kg
85-68-7 Butyl benzyl phthalate ND 180 37 ug/kg
100-51-6 Benzyl Alcohol ND 180 37 ug/kg
91-58-7 2-Chloronaphthalene ND 180 37 ug/kg
106-47-8 4-Chloroaniline ND 180 18 ug/kg
86-74-8 Carbazole ND 180 18 ug/kg
218-01-9 Chrysene ND 180 18 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 180 18 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 180 18 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-4/10-12
Lab Sample ID:F81875-9 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:89.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 180 18 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 180 18 ug/kg
95-50-1 1,2-Dichlorobenzene ND 180 37 ug/kg
541-73-1 1,3-Dichlorobenzene ND 180 37 ug/kg
106-46-7 1,4-Dichlorobenzene ND 180 37 ug/kg
121-14-2 2,4-Dinitrotoluene ND 180 18 ug/kg
606-20-2 2,6-Dinitrotoluene ND 180 22 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 370 37 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 180 18 ug/kg
132-64-9 Dibenzofuran ND 180 18 ug/kg
84-74-2 Di-n-butyl phthalate ND 370 73 ug/kg
117-84-0 Di-n-octyl phthalate ND 180 37 ug/kg
84-66-2 Diethyl phthalate ND 370 73 ug/kg
131-11-3 Dimethyl phthalate ND 180 37 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 370 73 ug/kg
206-44-0 Fluoranthene ND 180 18 ug/kg
86-73-7 Fluorene ND 180 18 ug/kg
118-74-1 Hexachlorobenzene ND 180 18 ug/kg
87-68-3 Hexachlorobutadiene ND 180 37 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 180 81 ug/kg
67-72-1 Hexachloroethane ND 180 37 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 180 18 ug/kg
78-59-1 Isophorone ND 180 18 ug/kg
91-57-6 2-Methylnaphthalene ND 180 18 ug/kg
88-74-4 2-Nitroaniline ND 180 37 ug/kg
99-09-2 3-Nitroaniline ND 180 37 ug/kg
100-01-6 4-Nitroaniline ND 180 37 ug/kg
91-20-3 Naphthalene ND 180 29 ug/kg
98-95-3 Nitrobenzene ND 180 18 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 180 18 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 180 18 ug/kg
85-01-8 Phenanthrene ND 180 18 ug/kg
129-00-0 Pyrene ND 180 18 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 180 18 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 60%40-102%
4165-62-2 Phenol-d5 74%41-100%
118-79-6 2,4,6-Tribromophenol 79%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-4/10-12
Lab Sample ID:F81875-9 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8270D SW846 3550C Percent Solids:89.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 70%40-105%
321-60-8 2-Fluorobiphenyl 70%43-107%
1718-51-0 Terphenyl-d14 67%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-4/10-12
Lab Sample ID:F81875-9 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8015C Percent Solids:89.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060080.D 1 05/09/11 AH n/a n/a GQR2611
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.91 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 5.3 2.6 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 82%56-136%
98-08-8 aaa-Trifluorotoluene 79%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-4/10-12
Lab Sample ID:F81875-9 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Method:SW846 8015C SW846 3550C Percent Solids:89.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40346.D 1 05/05/11 SJL 05/04/11 OP37017 GZF1663
Run #2
Initial Weight Final Volume
Run #1 30.2 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 9.2 3.7 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 92%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-4/10-12
Lab Sample ID:F81875-9 Date Sampled:04/27/11
Matrix:SO - Soil Date Received:04/28/11
Percent Solids:89.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony <1.1 1.1 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Arsenic <0.53 0.53 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Barium <11 11 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Beryllium <0.27 0.27 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Cadmium <0.21 0.21 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Chromium 7.8 0.53 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Copper 5.4 1.3 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Lead 3.2 1.1 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Mercury <0.087 0.087 mg/kg 1 05/10/11 05/10/11 LM SW846 7471B 2 SW846 7471B 4
Molybdenum <2.7 2.7 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Nickel <2.1 2.1 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Selenium <1.1 1.1 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Silver <0.53 0.53 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Tin <2.7 2.7 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
Zinc 3.4 1.1 mg/kg 1 05/05/11 05/05/11 RS SW846 6010C 1 SW846 3050B 3
(1) Instrument QC Batch: MA8926
(2) Instrument QC Batch: MA8935
(3) Prep QC Batch: MP20510
(4) Prep QC Batch: MP20537
RL = Reporting Limit
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Certification Exceptions
• Certification Exceptions (NC)
• Chain of Custody
Southeast
Section 4
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02/16/12
Technical Report for
AMEC Environment & Infrastructure, Inc.
GE-TFS; 1906 Bancroft St, Charlotte, NC
572260702
Accutest Job Number: F81928
Sampling Date: 04/28/11
Report to:
AMEC Earth & Environmental
steven.tanen@amec.com
ATTN: Steve Tanen
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), AK, AR, GA, KY, MA, NV, OK, UT, VA, WA, WI
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Conference
and/or state specific certification programs as applicable.
Client Service contact: Heather Wandrey 407-425-6700
Harry Behzadi, Ph.D.
Laboratory Director
Southeast
02/16/12
e-Hardcopy 2.0
Automated Report
154
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 154
F81928
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Case Narrative/Conformance Summary ..............................................................5
Section 3: Sample Results ........................................................................................................12
3.1: F81928-1: MW5/0.5-2 ..................................................................................................13
3.2: F81928-2: MW5/105-12 ...............................................................................................22
3.3: F81928-3: TB-04/28/11 ................................................................................................30
3.4: F81928-4: B1/0.5-2 .......................................................................................................32
3.5: F81928-5: B1/10-12 ......................................................................................................41
3.6: F81928-6: B2/0.5-2 .......................................................................................................49
3.7: F81928-7: B2/10-12 ......................................................................................................58
3.8: F81928-8: B4/2-4 ..........................................................................................................66
3.9: F81928-9: B4/10-12 ......................................................................................................75
3.10: F81928-10: B5/2-4 ......................................................................................................83
3.11: F81928-11: B5/10-12 ..................................................................................................92
3.12: F81928-12: B3/0.5-2 ...................................................................................................100
3.13: F81928-13: B3/10-12 ..................................................................................................109
3.14: F81928-14: B6/0.5-2 ...................................................................................................117
3.15: F81928-15: B6/10-12 ..................................................................................................126
3.16: F81928-16: B7/0.5-2 ...................................................................................................134
3.17: F81928-17: B7/10-12 ..................................................................................................143
Section 4: Misc. Forms ............................................................................................................151
4.1: Chain of Custody ...........................................................................................................152
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Accutest LabLink@128733 10:24 16-Feb-2012
Sample Summary
AMEC Environment & Infrastructure, Inc.
Job No:F81928
GE-TFS; 1906 Bancroft St, Charlotte, NC
Project No: 572260702
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
F81928-1 04/28/11 08:50 BENA 04/29/11 SO Soil MW5/0.5-2
F81928-2 04/28/11 09:20 BENA 04/29/11 SO Soil MW5/105-12
F81928-3 04/28/11 00:00 BENA 04/29/11 SO Trip Blank Soil TB-04/28/11
F81928-4 04/28/11 11:04 BENA 04/29/11 SO Soil B1/0.5-2
F81928-5 04/28/11 11:19 BENA 04/29/11 SO Soil B1/10-12
F81928-6 04/28/11 12:35 BENA 04/29/11 SO Soil B2/0.5-2
F81928-7 04/28/11 12:50 BENA 04/29/11 SO Soil B2/10-12
F81928-8 04/28/11 13:22 BENA 04/29/11 SO Soil B4/2-4
F81928-9 04/28/11 13:45 BENA 04/29/11 SO Soil B4/10-12
F81928-10 04/28/11 14:10 BENA 04/29/11 SO Soil B5/2-4
F81928-11 04/28/11 14:30 BENA 04/29/11 SO Soil B5/10-12
F81928-12 04/28/11 14:55 BENA 04/29/11 SO Soil B3/0.5-2
F81928-13 04/28/11 15:10 BENA 04/29/11 SO Soil B3/10-12
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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Accutest LabLink@128733 10:24 16-Feb-2012
Sample Summary
(continued)
AMEC Environment & Infrastructure, Inc.
Job No:F81928
GE-TFS; 1906 Bancroft St, Charlotte, NC
Project No: 572260702
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
F81928-14 04/28/11 15:30 BENA 04/29/11 SO Soil B6/0.5-2
F81928-15 04/28/11 15:50 BENA 04/29/11 SO Soil B6/10-12
F81928-16 04/28/11 16:15 BENA 04/29/11 SO Soil B7/0.5-2
F81928-17 04/28/11 16:40 BENA 04/29/11 SO Soil B7/10-12
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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SAMPLE DELIVERY GROUP CASE NARRATIVE
Client: AMEC Earth & Environmental Job F81928
Site: GE-TFS; 1906 Bancroft St, Charlotte, NC Report Date: 5/17/2011 4:00:49 PM
16 Samples and 1 Trip Blank were collected on 04/28/2011 and were received at Accutest SE on 04/29/2011 properly preserved,
at 2.8 Deg. C and intact. These Samples received an Accutest job number of F81928. A listing of the Laboratory Sample ID,
Client Sample ID and dates of collection are presented in the Results Summary Section of this report.
Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For more
information, please refer to QC summary pages.
Volatiles by GCMS by Method SW846 8260B Matrix: SO Batch ID: VF1486
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F82006-4MS, F82006-4MSD were used as the QC samples indicated.
Blank Spike Recoverys for Acetone, Methyl ethyl ketone are outside control limits.
Matrix Spike and Matrix Spike Duplicate Recoverys for 2-Hexanone, Chloroethane, Methyl ethyl ketone, Tetrachloroethylene are
outside control limits. Probable cause due to matrix interference.
Matrix: SO Batch ID: VF1487
All samples were analyzed within the recommended method holding time.
Samples F82006-9MS, F82006-9MSD were used as the QC samples indicated.
All method blanks for this batch meet method specific criteria.
Blank Spike Recovery for Acetone is outside control limits.
Matrix Spike Recoverys for 2-Hexanone, 4-Methyl-2-pentanone, Chloroethane, Methyl ethyl ketone, Tetrachloroethylene, Vinyl chloride, cis-1,2-Dichloroethylene are outside control limits. Outside control limits due to high level in sample relative to spike amount.
Matrix Spike Duplicate Recoverys for Chloroethane, Tetrachloroethylene are outside control limits. Probable cause due to matrix interference.
Matrix: SO Batch ID: VF1488
All samples were analyzed within the recommended method holding time.
Samples F81829-6MS, F81829-6MSD were used as the QC samples indicated.
All method blanks for this batch meet method specific criteria.
Blank Spike Recoverys for Acetone, Methyl ethyl ketone are outside control limits.
Matrix Spike and Matrix Spike Duplicate Recoverys for Chloroethane, Tetrachloroethylene are outside control limits. Probable
cause due to matrix interference.
Matrix: SO Batch ID: VF1489
All samples were analyzed within the recommended method holding time.
Samples F81869-2MS, F81869-2MSD were used as the QC samples indicated. All method blanks for this batch meet method specific criteria.
Blank Spike Recoverys for 2-Hexanone, Acetone, Methyl ethyl ketone, Methylene chloride are outside control limits.
Matrix Spike Recoverys for 1,1-Dichloroethane, 1,1-Dichloroethylene, 1,2-Dichloropropane, Benzene, Bromodichloromethane, Chlorobenzene, Chloroethane, Chloroform, cis-1,2-Dichloroethylene, Ethylbenzene, Methylene chloride, Styrene, Tetrachloroethylene, Toluene, trans-1,2-Dichloroethylene, Trichloroethylene, Xylene (total) are outside control limits. Probable cause due to matrix interference.
Matrix Spike Duplicate Recoverys for Chlorobenzene, Chloroethane, Ethylbenzene, Tetrachloroethylene, Toluene are outside control limits. Probable cause due to matrix interference.
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Volatiles by GCMS by Method SW846 8260B
Matrix: SO Batch ID: VG2718
All samples were analyzed within the recommended method holding time. Samples F81777-2MS, F81777-2MSD were used as the QC samples indicated.
All method blanks for this batch meet method specific criteria.
Matrix Spike Recoverys for 2-Hexanone, Bromoform, Chloroethane, Dibromochloromethane, Methyl bromide are outside control limits. Probable cause due to matrix interference.
Matrix Spike Duplicate Recoverys for Bromoform, Chloroethane are outside control limits. Probable cause due to matrix interference.
RPDs for MSD for Chloroethane are outside control limits for sample F81777-2MSD. Probable cause due to sample non-homogeneity.
F81928-7 for Methylene chloride: CCV outside of control limits; results may be biased low.
F81928-8 for Methylene chloride: CCV outside of control limits; results may be biased low.
Extractables by GCMS by Method SW846 8270D
Matrix: SO Batch ID: OP36999
All samples were extracted within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F81928-5MS, F81928-5MSD were used as the QC samples indicated.
Volatiles by GC by Method SW846 8015C Matrix: SO Batch ID: GQR2610
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F81928-1MS, F81928-1MSD were used as the QC samples indicated.
Extractables by GC by Method SW846 8015C Matrix: SO Batch ID: OP36981
All samples were extracted within the recommended method holding time. All samples were analyzed within the recommended method holding time.
Samples F81873-4MS, F81873-4MSD were used as the QC samples indicated.
All method blanks for this batch meet method specific criteria.
Matrix: SO Batch ID: OP37014
All samples were extracted within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
Samples F81929-3MS, F81929-3MSD were used as the QC samples indicated. All method blanks for this batch meet method specific criteria.
Matrix Spike and Matrix Spike Duplicate Recoverys for TPH (C10-C28) are outside control limits. Probable cause due to matrix
interference.
RPD for MSD for TPH (C10-C28) is outside control limits for sample OP37014-MSD. Spike recovery indicates possible sample nonhomogeneity.
Extractables by GC by Method SW846 8082A Matrix: SO Batch ID: OP36984
All samples were extracted within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
Samples F81916-2MS, F81916-2MSD were used as the QC samples indicated.
All method blanks for this batch meet method specific criteria.
Matrix Spike Duplicate Recovery for Aroclor 1016 is outside control limits. Probable cause due to matrix interference.
Tuesday, May 17, 2011
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Metals by Method SW846 6010C Matrix: SO Batch ID: MP20489
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria.
Samples F81928-1DUP, F81928-1MS, F81928-1MSD, F81928-1PS, F81928-1SDL, F81928-1DUP were used as the QC samples for metals.
Matrix Spike Recoverys for Antimony, Arsenic, Copper, Molybdenum, Selenium are outside control limits. Spike recovery indicates possible matrix interference and/or sample nonhomogeneity.
Matrix Spike Duplicate Recoverys for Copper, Antimony, Arsenic, Molybdenum, Selenium, Tin are outside control limits. Probable cause due to matrix interference.
Matrix Spike Recoverys for Chromium are outside control limits. Spike amount low relative to the sample amount. Refer to lab control or spike blank for recovery information.
RPD for Duplicate for Tin is outside control limits for sample MP20489-D1. RPD acceptable due to low duplicate and sample concentrations.
RPDs for MSD for Antimony, Arsenic, Barium, Beryllium, Cadmium, Chromium, Molybdenum, Nickel, Selenium, Silver, Tin, Zinc are outside control limits for sample MP20489-S2. High RPD due to possible sample nonhomogeneity.
RPDs for Serial Dilution for Arsenic, Beryllium, Nickel, Barium, Zinc are outside control limits for sample MP20489-SD1. Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
MP20489-SD1 for Barium, Zinc: Serial dilution indicates possible matrix interference.
F81928-5 for Silver: Elevated reporting limit(s) due to matrix interference.
F81928-5 for Selenium: Elevated reporting limit(s) due to matrix interference. F81928-5 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81928-5 for Molybdenum: Elevated reporting limit(s) due to matrix interference.
F81928-5 for Copper: Elevated reporting limit(s) due to matrix interference.
F81928-5 for Cadmium: Elevated reporting limit(s) due to matrix interference.
F81928-5 for Barium: Elevated reporting limit(s) due to matrix interference.
F81928-5 for Arsenic: Elevated reporting limit(s) due to matrix interference.
F81928-5 for Antimony: Elevated reporting limit(s) due to matrix interference.
F81928-1 for Selenium: Elevated reporting limit(s) due to matrix interference. F81928-4 for Zinc: Elevated reporting limit(s) due to matrix interference. F81928-2 for Antimony: Elevated reporting limit(s) due to matrix interference.
F81928-1 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81928-1 for Zinc: Elevated reporting limit(s) due to matrix interference.
F81928-6 for Antimony: Elevated reporting limit(s) due to matrix interference. F81928-2 for Copper: Elevated reporting limit(s) due to matrix interference.
F81928-2 for Barium: Elevated reporting limit(s) due to matrix interference.
F81928-4 for Chromium: Elevated reporting limit(s) due to matrix interference.
F81928-4 for Copper: Elevated reporting limit(s) due to matrix interference.
F81928-4 for Lead: Elevated reporting limit(s) due to matrix interference.
F81928-2 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81928-2 for Zinc: Elevated reporting limit(s) due to matrix interference.
F81928-4 for Arsenic: Elevated reporting limit(s) due to matrix interference.
F81928-2 for Molybdenum: Elevated reporting limit(s) due to matrix interference.
F81928-4 for Antimony: Elevated reporting limit(s) due to matrix interference.
F81928-2 for Chromium: Elevated reporting limit(s) due to matrix interference.
F81928-2 for Cadmium: Elevated reporting limit(s) due to matrix interference.
F81928-2 for Beryllium: Elevated reporting limit(s) due to matrix interference.
F81928-7 for Antimony: Elevated reporting limit(s) due to matrix interference.
F81928-2 for Arsenic: Elevated reporting limit(s) due to matrix interference.
F81928-4 for Molybdenum: Elevated reporting limit(s) due to matrix interference. F81928-4 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81928-6 for Selenium: Elevated reporting limit(s) due to matrix interference.
F81928-4 for Silver: Elevated reporting limit(s) due to matrix interference.
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Metals by Method SW846 6010C Matrix: SO Batch ID: MP20489 F81928-11 for Zinc: Elevated reporting limit(s) due to matrix interference.
F81928-9 for Beryllium: Elevated reporting limit(s) due to matrix interference.
F81928-7 for Barium: Elevated reporting limit(s) due to matrix interference.
F81928-7 for Beryllium: Elevated reporting limit(s) due to matrix interference.
F81928-7 for Cadmium: Elevated reporting limit(s) due to matrix interference.
F81928-7 for Chromium: Elevated reporting limit(s) due to matrix interference.
F81928-7 for Copper: Elevated reporting limit(s) due to matrix interference.
F81928-7 for Tin: Elevated reporting limit(s) due to matrix interference.
F81928-7 for Zinc: Elevated reporting limit(s) due to matrix interference.
F81928-6 for Arsenic: Elevated reporting limit(s) due to matrix interference.
F81928-6 for Cadmium: Elevated reporting limit(s) due to matrix interference.
F81928-6 for Chromium: Elevated reporting limit(s) due to matrix interference.
F81928-6 for Copper: Elevated reporting limit(s) due to matrix interference. F81928-6 for Lead: Elevated reporting limit(s) due to matrix interference.
F81928-4 for Cadmium: Elevated reporting limit(s) due to matrix interference.
F81928-6 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81928-5 for Zinc: Elevated reporting limit(s) due to matrix interference.
F81928-6 for Silver: Elevated reporting limit(s) due to matrix interference.
F81928-6 for Zinc: Elevated reporting limit(s) due to matrix interference.
F81928-5 for Tin: Elevated reporting limit(s) due to matrix interference.
F81928-4 for Selenium: Elevated reporting limit(s) due to matrix interference. F81928-2 for Tin: Elevated reporting limit(s) due to matrix interference.
F81928-2 for Silver: Elevated reporting limit(s) due to matrix interference.
F81928-2 for Selenium: Elevated reporting limit(s) due to matrix interference.
F81928-7 for Molybdenum: Elevated reporting limit(s) due to matrix interference.
F81928-7 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81928-6 for Molybdenum: Elevated reporting limit(s) due to matrix interference.
F81928-7 for Selenium: Elevated reporting limit(s) due to matrix interference.
F81928-9 for Antimony: Elevated reporting limit(s) due to matrix interference. F81928-7 for Silver: Elevated reporting limit(s) due to matrix interference.
F81928-13 for Silver: Elevated reporting limit(s) due to matrix interference.
F81928-10 for Antimony: Elevated reporting limit(s) due to matrix interference.
F81928-11 for Silver: Elevated reporting limit(s) due to matrix interference.
F81928-11 for Tin: Elevated reporting limit(s) due to matrix interference.
F81928-11 for Beryllium: Elevated reporting limit(s) due to matrix interference.
F81928-9 for Zinc: Elevated reporting limit(s) due to matrix interference.
F81928-9 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81928-11 for Arsenic: Elevated reporting limit(s) due to matrix interference.
F81928-7 for Arsenic: Elevated reporting limit(s) due to matrix interference.
F81928-17 for Chromium: Elevated reporting limit(s) due to matrix interference.
F81928-17 for Cadmium: Elevated reporting limit(s) due to matrix interference.
F81928-15 for Copper: Elevated reporting limit(s) due to matrix interference.
F81928-17 for Barium: Elevated reporting limit(s) due to matrix interference.
F81928-17 for Arsenic: Elevated reporting limit(s) due to matrix interference.
F81928-17 for Antimony: Elevated reporting limit(s) due to matrix interference.
F81928-17 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81928-17 for Molybdenum: Elevated reporting limit(s) due to matrix interference.
F81928-17 for Selenium: Elevated reporting limit(s) due to matrix interference.
F81928-16 for Silver: Elevated reporting limit(s) due to matrix interference.
Tuesday, May 17, 2011
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Metals by Method SW846 6010C Matrix: SO Batch ID: MP20489 F81928-8 for Zinc: Elevated reporting limit(s) due to matrix interference.
F81928-8 for Silver: Elevated reporting limit(s) due to matrix interference.
F81928-8 for Selenium: Elevated reporting limit(s) due to matrix interference.
F81928-8 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81928-8 for Molybdenum: Elevated reporting limit(s) due to matrix interference.
F81928-8 for Chromium: Elevated reporting limit(s) due to matrix interference.
F81928-8 for Copper: Elevated reporting limit(s) due to matrix interference.
F81928-15 for Lead: Elevated reporting limit(s) due to matrix interference. F81928-8 for Lead: Elevated reporting limit(s) due to matrix interference.
F81928-13 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81928-15 for Chromium: Elevated reporting limit(s) due to matrix interference.
F81928-15 for Cadmium: Elevated reporting limit(s) due to matrix interference.
F81928-15 for Arsenic: Elevated reporting limit(s) due to matrix interference.
F81928-15 for Antimony: Elevated reporting limit(s) due to matrix interference.
F81928-13 for Zinc: Elevated reporting limit(s) due to matrix interference.
F81928-13 for Tin: Elevated reporting limit(s) due to matrix interference.
F81928-9 for Arsenic: Elevated reporting limit(s) due to matrix interference.
F81928-13 for Selenium: Elevated reporting limit(s) due to matrix interference.
F81928-9 for Barium: Elevated reporting limit(s) due to matrix interference.
F81928-13 for Molybdenum: Elevated reporting limit(s) due to matrix interference.
F81928-15 for Silver: Elevated reporting limit(s) due to matrix interference.
F81928-8 for Cadmium: Elevated reporting limit(s) due to matrix interference.
F81928-9 for Chromium: Elevated reporting limit(s) due to matrix interference.
F81928-12 for Molybdenum: Elevated reporting limit(s) due to matrix interference.
F81928-9 for Cadmium: Elevated reporting limit(s) due to matrix interference.
F81928-9 for Silver: Elevated reporting limit(s) due to matrix interference.
F81928-9 for Tin: Elevated reporting limit(s) due to matrix interference.
F81928-9 for Molybdenum: Elevated reporting limit(s) due to matrix interference. F81928-8 for Antimony: Elevated reporting limit(s) due to matrix interference.
F81928-8 for Arsenic: Elevated reporting limit(s) due to matrix interference. F81928-9 for Copper: Elevated reporting limit(s) due to matrix interference.
F81928-9 for Selenium: Elevated reporting limit(s) due to matrix interference. F81928-11 for Molybdenum: Elevated reporting limit(s) due to matrix interference.
F81928-10 for Arsenic: Elevated reporting limit(s) due to matrix interference.
F81928-10 for Cadmium: Elevated reporting limit(s) due to matrix interference.
F81928-10 for Chromium: Elevated reporting limit(s) due to matrix interference.
F81928-10 for Copper: Elevated reporting limit(s) due to matrix interference.
F81928-10 for Lead: Elevated reporting limit(s) due to matrix interference.
F81928-10 for Molybdenum: Elevated reporting limit(s) due to matrix interference.
F81928-11 for Chromium: Elevated reporting limit(s) due to matrix interference. F81928-11 for Selenium: Elevated reporting limit(s) due to matrix interference.
F81928-10 for Silver: Elevated reporting limit(s) due to matrix interference.
F81928-11 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81928-11 for Antimony: Elevated reporting limit(s) due to matrix interference.
F81928-11 for Barium: Elevated reporting limit(s) due to matrix interference.
F81928-10 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81928-11 for Cadmium: Elevated reporting limit(s) due to matrix interference.
F81928-10 for Zinc: Elevated reporting limit(s) due to matrix interference.
F81928-11 for Copper: Elevated reporting limit(s) due to matrix interference.
F81928-15 for Molybdenum: Elevated reporting limit(s) due to matrix interference.
Tuesday, May 17, 2011
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Metals by Method SW846 6010C Matrix: SO Batch ID: MP20489 F81928-10 for Selenium: Elevated reporting limit(s) due to matrix interference.
F81928-13 for Copper: Elevated reporting limit(s) due to matrix interference.
F81928-13 for Chromium: Elevated reporting limit(s) due to matrix interference.
F81928-13 for Arsenic: Elevated reporting limit(s) due to matrix interference.
F81928-13 for Barium: Elevated reporting limit(s) due to matrix interference.
F81928-12 for Antimony: Elevated reporting limit(s) due to matrix interference.
F81928-5 for Beryllium: Elevated reporting limit(s) due to matrix interference.
F81928-1 for Silver: Elevated reporting limit(s) due to matrix interference.
F81928-1 for Antimony: Elevated reporting limit(s) due to matrix interference.
F81928-1 for Arsenic: Elevated reporting limit(s) due to matrix interference.
F81928-1 for Cadmium: Elevated reporting limit(s) due to matrix interference.
F81928-1 for Chromium: Elevated reporting limit(s) due to matrix interference.
F81928-1 for Copper: Elevated reporting limit(s) due to matrix interference.
F81928-1 for Lead: Elevated reporting limit(s) due to matrix interference.
F81928-1 for Molybdenum: Elevated reporting limit(s) due to matrix interference.
F81928-5 for Chromium: Elevated reporting limit(s) due to matrix interference.
F81928-13 for Beryllium: Elevated reporting limit(s) due to matrix interference.
F81928-15 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81928-13 for Cadmium: Elevated reporting limit(s) due to matrix interference.
F81928-17 for Beryllium: Elevated reporting limit(s) due to matrix interference.
F81928-16 for Copper: Elevated reporting limit(s) due to matrix interference.
F81928-16 for Lead: Elevated reporting limit(s) due to matrix interference.
F81928-16 for Molybdenum: Elevated reporting limit(s) due to matrix interference.
F81928-12 for Arsenic: Elevated reporting limit(s) due to matrix interference.
F81928-16 for Selenium: Elevated reporting limit(s) due to matrix interference.
F81928-17 for Copper: Elevated reporting limit(s) due to matrix interference.
F81928-16 for Zinc: Elevated reporting limit(s) due to matrix interference.
F81928-15 for Selenium: Elevated reporting limit(s) due to matrix interference. F81928-16 for Chromium: Elevated reporting limit(s) due to matrix interference.
F81928-16 for Cadmium: Elevated reporting limit(s) due to matrix interference. F81928-16 for Arsenic: Elevated reporting limit(s) due to matrix interference.
F81928-16 for Antimony: Elevated reporting limit(s) due to matrix interference.
F81928-15 for Zinc: Elevated reporting limit(s) due to matrix interference.
F81928-16 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81928-12 for Copper: Elevated reporting limit(s) due to matrix interference. F81928-17 for Tin: Elevated reporting limit(s) due to matrix interference. F81928-17 for Zinc: Elevated reporting limit(s) due to matrix interference.
F81928-13 for Antimony: Elevated reporting limit(s) due to matrix interference.
F81928-12 for Zinc: Elevated reporting limit(s) due to matrix interference.
F81928-12 for Silver: Elevated reporting limit(s) due to matrix interference. F81928-12 for Selenium: Elevated reporting limit(s) due to matrix interference.
F81928-12 for Nickel: Elevated reporting limit(s) due to matrix interference.
F81928-17 for Silver: Elevated reporting limit(s) due to matrix interference.
F81928-12 for Lead: Elevated reporting limit(s) due to matrix interference.
F81928-12 for Cadmium: Elevated reporting limit(s) due to matrix interference.
F81928-12 for Chromium: Elevated reporting limit(s) due to matrix interference.
MP20489-PS1 for Zinc: Spike recovery indicates matrix interference and/or outside control limits due to high level in sample relative to spike amount. MP20489-PS1 for Tin: Spike recovery indicates matrix interference and/or outside control limits due to high level in sample relative to spike amount.
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Metals by Method SW846 6010C Matrix: SO Batch ID: MP20489 MP20489-PS1 for Lead: Spike recovery indicates matrix interference and/or outside control limits due to high level in sample relative to spike amount. MP20489-PS1 for Nickel: Spike recovery indicates matrix interference and/or outside control limits due to high level in sample relative to spike amount.
MP20489-PS1 for Antimony: Spike recovery indicates matrix interference and/or outside control limits due to high level in sample relative to spike amount. MP20489-PS1 for Silver: Spike recovery indicates matrix interference and/or outside control limits due to high level in sample relative to spike amount.
MP20489-PS1 for Arsenic: Spike recovery indicates matrix interference and/or outside control limits due to high level in sample relative to spike amount.
MP20489-PS1 for Cadmium: Spike recovery indicates matrix interference and/or outside control limits due to high level in sample relative to spike amount.
MP20489-PS1 for Copper: Spike recovery indicates matrix interference and/or outside control limits due to high level in sample relative to spike amount.
MP20489-PS1 for Molybdenum: Spike recovery indicates matrix interference and/or outside control limits due to high level in sample relative to spike amount. MP20489-PS1 for Selenium: Spike recovery indicates matrix interference and/or outside control limits due to high level in sample relative to spike amount.
Metals by Method SW846 7471B Matrix: SO Batch ID: MP20518
All samples were digested within the recommended method holding time. All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F81916-10MS, F81916-10MSD, F81916-10SDL, F81916-10DUP were used as the QC samples for metals.
RPD for Duplicate for Mercury is outside control limits for sample MP20518-D1. RPD acceptable due to low duplicate and sample concentrations.
RPD for Serial Dilution for Mercury is outside control limits for sample MP20518-SD1. Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
Matrix: SO Batch ID: MP20527
All samples were digested within the recommended method holding time. All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F81991-1MS, F81991-1MSD, F81991-1DUP, F81991-1SDL were used as the QC samples for metals.
RPD for Duplicate for Mercury is outside control limits for sample MP20527-D1. High RPD due to possible sample nonhomogeneity.
RPD for Serial Dilution for Mercury is outside control limits for sample MP20527-SD1. Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
Wet Chemistry by Method SM19 2540G Matrix: SO Batch ID: GN44372
Sample F81928-17DUP was used as the QC sample for Solids, Percent.
Accutest Laboratories Southeast (ALSE) certifies that this report meets the project requirements for analytical data produced for the
samples as received at ALSE and as stated on the COC. ALSE certifies that the data meets the Data Quality Objectives for precision,
accuracy and completeness as specified in the ALSE Quality Manual except as noted above. This report is to be used in its entirety.
ALSE is not responsible for any assumptions of data quality if partial data packages are used.
Narrative prepared by:
_______________________________________ Date: May 17, 2011
Ellen Pampel, Inorganic QA (signature on file)
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Sample Results
Report of Analysis
Southeast
Section 3
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Report of Analysis Page 1 of 2
Client Sample ID:MW5/0.5-2
Lab Sample ID:F81928-1 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:82.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F049406.D 1 05/06/11 CW n/a n/a VF1487
Run #2
Initial Weight
Run #1 5.25 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 58 23 ug/kg
71-43-2 Benzene ND 5.8 1.7 ug/kg
75-27-4 Bromodichloromethane ND 5.8 1.3 ug/kg
75-25-2 Bromoform ND 5.8 1.7 ug/kg
108-90-7 Chlorobenzene ND 5.8 1.2 ug/kg
75-00-3 Chloroethane ND 5.8 2.3 ug/kg
67-66-3 Chloroform ND 5.8 1.4 ug/kg
75-15-0 Carbon disulfide ND 5.8 2.3 ug/kg
56-23-5 Carbon tetrachloride ND 5.8 2.1 ug/kg
75-34-3 1,1-Dichloroethane ND 5.8 1.3 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.8 1.6 ug/kg
107-06-2 1,2-Dichloroethane ND 5.8 1.2 ug/kg
78-87-5 1,2-Dichloropropane ND 5.8 1.4 ug/kg
124-48-1 Dibromochloromethane ND 5.8 1.2 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.8 1.7 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.8 1.2 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.8 1.7 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.8 1.3 ug/kg
100-41-4 Ethylbenzene ND 5.8 1.2 ug/kg
591-78-6 2-Hexanone ND 29 6.2 ug/kg
108-10-1 4-Methyl-2-pentanone ND 29 6.4 ug/kg
74-83-9 Methyl bromide ND 5.8 2.3 ug/kg
74-87-3 Methyl chloride ND 5.8 2.3 ug/kg
75-09-2 Methylene chloride ND 12 5.3 ug/kg
78-93-3 Methyl ethyl ketone ND 29 7.1 ug/kg
100-42-5 Styrene ND 5.8 3.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.8 1.3 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.8 1.4 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.8 1.3 ug/kg
127-18-4 Tetrachloroethylene ND 5.8 1.2 ug/kg
108-88-3 Toluene ND 5.8 1.4 ug/kg
79-01-6 Trichloroethylene ND 5.8 1.4 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW5/0.5-2
Lab Sample ID:F81928-1 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:82.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 5.8 1.7 ug/kg
1330-20-7 Xylene (total)ND 17 3.7 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%80-121%
2037-26-5 Toluene-D8 98%71-130%
460-00-4 4-Bromofluorobenzene 100%59-148%
17060-07-0 1,2-Dichloroethane-D4 104%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW5/0.5-2
Lab Sample ID:F81928-1 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:82.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025248.D 1 05/05/11 MG 05/03/11 OP36999 SU1213
Run #2
Initial Weight Final Volume
Run #1 30.1 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1000 350 ug/kg
95-57-8 2-Chlorophenol ND 200 20 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 200 20 ug/kg
120-83-2 2,4-Dichlorophenol ND 200 20 ug/kg
105-67-9 2,4-Dimethylphenol ND 200 25 ug/kg
51-28-5 2,4-Dinitrophenol ND 1000 400 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 400 81 ug/kg
95-48-7 2-Methylphenol ND 200 20 ug/kg
3&4-Methylphenol ND 200 29 ug/kg
88-75-5 2-Nitrophenol ND 200 20 ug/kg
100-02-7 4-Nitrophenol ND 1000 160 ug/kg
87-86-5 Pentachlorophenol ND 1000 240 ug/kg
108-95-2 Phenol ND 200 20 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 200 20 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 200 20 ug/kg
83-32-9 Acenaphthene ND 200 20 ug/kg
208-96-8 Acenaphthylene ND 200 20 ug/kg
120-12-7 Anthracene ND 200 20 ug/kg
56-55-3 Benzo(a)anthracene ND 200 20 ug/kg
50-32-8 Benzo(a)pyrene ND 200 20 ug/kg
205-99-2 Benzo(b)fluoranthene ND 200 20 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 200 20 ug/kg
207-08-9 Benzo(k)fluoranthene ND 200 20 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 200 20 ug/kg
85-68-7 Butyl benzyl phthalate ND 200 40 ug/kg
100-51-6 Benzyl Alcohol ND 200 40 ug/kg
91-58-7 2-Chloronaphthalene ND 200 40 ug/kg
106-47-8 4-Chloroaniline ND 200 20 ug/kg
86-74-8 Carbazole ND 200 20 ug/kg
218-01-9 Chrysene ND 200 20 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 200 20 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 200 20 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW5/0.5-2
Lab Sample ID:F81928-1 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:82.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 200 20 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 200 20 ug/kg
95-50-1 1,2-Dichlorobenzene ND 200 40 ug/kg
541-73-1 1,3-Dichlorobenzene ND 200 40 ug/kg
106-46-7 1,4-Dichlorobenzene ND 200 40 ug/kg
121-14-2 2,4-Dinitrotoluene ND 200 20 ug/kg
606-20-2 2,6-Dinitrotoluene ND 200 24 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 400 40 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 200 20 ug/kg
132-64-9 Dibenzofuran ND 200 20 ug/kg
84-74-2 Di-n-butyl phthalate ND 400 81 ug/kg
117-84-0 Di-n-octyl phthalate ND 200 40 ug/kg
84-66-2 Diethyl phthalate ND 400 81 ug/kg
131-11-3 Dimethyl phthalate ND 200 40 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 400 81 ug/kg
206-44-0 Fluoranthene ND 200 20 ug/kg
86-73-7 Fluorene ND 200 20 ug/kg
118-74-1 Hexachlorobenzene ND 200 20 ug/kg
87-68-3 Hexachlorobutadiene ND 200 40 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 200 89 ug/kg
67-72-1 Hexachloroethane ND 200 40 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 200 20 ug/kg
78-59-1 Isophorone ND 200 20 ug/kg
91-57-6 2-Methylnaphthalene ND 200 20 ug/kg
88-74-4 2-Nitroaniline ND 200 40 ug/kg
99-09-2 3-Nitroaniline ND 200 40 ug/kg
100-01-6 4-Nitroaniline ND 200 40 ug/kg
91-20-3 Naphthalene ND 200 32 ug/kg
98-95-3 Nitrobenzene ND 200 20 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 200 20 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 200 20 ug/kg
85-01-8 Phenanthrene ND 200 20 ug/kg
129-00-0 Pyrene ND 200 20 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 200 20 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 62%40-102%
4165-62-2 Phenol-d5 70%41-100%
118-79-6 2,4,6-Tribromophenol 65%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW5/0.5-2
Lab Sample ID:F81928-1 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:82.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 63%40-105%
321-60-8 2-Fluorobiphenyl 65%43-107%
1718-51-0 Terphenyl-d14 70%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW5/0.5-2
Lab Sample ID:F81928-1 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C Percent Solids:82.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060043.D 1 05/06/11 AH n/a n/a GQR2610
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 4.61 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 7.6 3.8 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 71%56-136%
98-08-8 aaa-Trifluorotoluene 75%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW5/0.5-2
Lab Sample ID:F81928-1 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8082A SW846 3550C Percent Solids:82.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 XX055988.D 1 05/03/11 NJ 05/02/11 OP36984 GXX864
Run #2
Initial Weight Final Volume
Run #1 29.9 g 10.0 ml
Run #2
PCB List
CAS No.Compound Result RL MDL Units Q
12674-11-2 Aroclor 1016 ND 20 8.1 ug/kg
11104-28-2 Aroclor 1221 ND 20 10 ug/kg
11141-16-5 Aroclor 1232 ND 20 10 ug/kg
53469-21-9 Aroclor 1242 ND 20 8.1 ug/kg
12672-29-6 Aroclor 1248 ND 20 8.1 ug/kg
11097-69-1 Aroclor 1254 ND 20 8.1 ug/kg
11096-82-5 Aroclor 1260 ND 20 8.1 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 74%44-126%
2051-24-3 Decachlorobiphenyl 83%39-157%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW5/0.5-2
Lab Sample ID:F81928-1 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C SW846 3550C Percent Solids:82.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40270.D 1 05/03/11 SJL 05/02/11 OP36981 GZF1661
Run #2
Initial Weight Final Volume
Run #1 29.9 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 10 4.1 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 79%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW5/0.5-2
Lab Sample ID:F81928-1 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Percent Solids:82.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <2.2 2.2 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Arsenic a 1.4 1.1 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Barium 17.2 11 mg/kg 1 05/03/11 05/03/11 RS SW846 6010C 1 SW846 3050B 4
Beryllium <0.28 0.28 mg/kg 1 05/03/11 05/03/11 RS SW846 6010C 1 SW846 3050B 4
Cadmium a <0.45 0.45 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Chromium a 55.1 1.1 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Copper a 23.2 2.8 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Lead a 9.7 2.2 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Mercury <0.10 0.10 mg/kg 1 05/06/11 05/06/11 LM SW846 7471B 3 SW846 7471B 5
Molybdenum a <5.6 5.6 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Nickel a <4.5 4.5 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Selenium a 2.8 2.2 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Silver a <1.1 1.1 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Tin <2.8 2.8 mg/kg 1 05/03/11 05/03/11 RS SW846 6010C 1 SW846 3050B 4
Zinc a 8.9 2.2 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
(1) Instrument QC Batch: MA8921
(2) Instrument QC Batch: MA8926
(3) Instrument QC Batch: MA8928
(4) Prep QC Batch: MP20489
(5) Prep QC Batch: MP20518
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Report of Analysis Page 1 of 2
Client Sample ID:MW5/105-12
Lab Sample ID:F81928-2 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:78.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F049407.D 1 05/06/11 CW n/a n/a VF1487
Run #2
Initial Weight
Run #1 5.22 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 61 24 ug/kg
71-43-2 Benzene ND 6.1 1.8 ug/kg
75-27-4 Bromodichloromethane ND 6.1 1.3 ug/kg
75-25-2 Bromoform ND 6.1 1.8 ug/kg
108-90-7 Chlorobenzene ND 6.1 1.2 ug/kg
75-00-3 Chloroethane ND 6.1 2.4 ug/kg
67-66-3 Chloroform ND 6.1 1.5 ug/kg
75-15-0 Carbon disulfide ND 6.1 2.4 ug/kg
56-23-5 Carbon tetrachloride ND 6.1 2.2 ug/kg
75-34-3 1,1-Dichloroethane ND 6.1 1.3 ug/kg
75-35-4 1,1-Dichloroethylene ND 6.1 1.7 ug/kg
107-06-2 1,2-Dichloroethane ND 6.1 1.2 ug/kg
78-87-5 1,2-Dichloropropane ND 6.1 1.5 ug/kg
124-48-1 Dibromochloromethane ND 6.1 1.2 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 6.1 1.8 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 6.1 1.2 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 6.1 1.8 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 6.1 1.3 ug/kg
100-41-4 Ethylbenzene ND 6.1 1.2 ug/kg
591-78-6 2-Hexanone ND 30 6.6 ug/kg
108-10-1 4-Methyl-2-pentanone ND 30 6.7 ug/kg
74-83-9 Methyl bromide ND 6.1 2.4 ug/kg
74-87-3 Methyl chloride ND 6.1 2.4 ug/kg
75-09-2 Methylene chloride ND 12 5.6 ug/kg
78-93-3 Methyl ethyl ketone ND 30 7.4 ug/kg
100-42-5 Styrene ND 6.1 3.2 ug/kg
71-55-6 1,1,1-Trichloroethane ND 6.1 1.3 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 6.1 1.5 ug/kg
79-00-5 1,1,2-Trichloroethane ND 6.1 1.3 ug/kg
127-18-4 Tetrachloroethylene ND 6.1 1.2 ug/kg
108-88-3 Toluene ND 6.1 1.5 ug/kg
79-01-6 Trichloroethylene ND 6.1 1.5 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW5/105-12
Lab Sample ID:F81928-2 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:78.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 6.1 1.8 ug/kg
1330-20-7 Xylene (total)ND 18 3.9 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%80-121%
2037-26-5 Toluene-D8 97%71-130%
460-00-4 4-Bromofluorobenzene 104%59-148%
17060-07-0 1,2-Dichloroethane-D4 111%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW5/105-12
Lab Sample ID:F81928-2 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:78.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025249.D 1 05/05/11 MG 05/03/11 OP36999 SU1213
Run #2
Initial Weight Final Volume
Run #1 30.3 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1000 370 ug/kg
95-57-8 2-Chlorophenol ND 210 21 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 210 21 ug/kg
120-83-2 2,4-Dichlorophenol ND 210 21 ug/kg
105-67-9 2,4-Dimethylphenol ND 210 26 ug/kg
51-28-5 2,4-Dinitrophenol ND 1000 420 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 420 84 ug/kg
95-48-7 2-Methylphenol ND 210 21 ug/kg
3&4-Methylphenol ND 210 30 ug/kg
88-75-5 2-Nitrophenol ND 210 21 ug/kg
100-02-7 4-Nitrophenol ND 1000 170 ug/kg
87-86-5 Pentachlorophenol ND 1000 250 ug/kg
108-95-2 Phenol ND 210 21 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 210 21 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 210 21 ug/kg
83-32-9 Acenaphthene ND 210 21 ug/kg
208-96-8 Acenaphthylene ND 210 21 ug/kg
120-12-7 Anthracene ND 210 21 ug/kg
56-55-3 Benzo(a)anthracene ND 210 21 ug/kg
50-32-8 Benzo(a)pyrene ND 210 21 ug/kg
205-99-2 Benzo(b)fluoranthene ND 210 21 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 210 21 ug/kg
207-08-9 Benzo(k)fluoranthene ND 210 21 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 210 21 ug/kg
85-68-7 Butyl benzyl phthalate ND 210 42 ug/kg
100-51-6 Benzyl Alcohol ND 210 42 ug/kg
91-58-7 2-Chloronaphthalene ND 210 42 ug/kg
106-47-8 4-Chloroaniline ND 210 21 ug/kg
86-74-8 Carbazole ND 210 21 ug/kg
218-01-9 Chrysene ND 210 21 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 210 21 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 210 21 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW5/105-12
Lab Sample ID:F81928-2 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:78.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 210 21 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 210 21 ug/kg
95-50-1 1,2-Dichlorobenzene ND 210 42 ug/kg
541-73-1 1,3-Dichlorobenzene ND 210 42 ug/kg
106-46-7 1,4-Dichlorobenzene ND 210 42 ug/kg
121-14-2 2,4-Dinitrotoluene ND 210 21 ug/kg
606-20-2 2,6-Dinitrotoluene ND 210 25 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 420 42 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 210 21 ug/kg
132-64-9 Dibenzofuran ND 210 21 ug/kg
84-74-2 Di-n-butyl phthalate ND 420 84 ug/kg
117-84-0 Di-n-octyl phthalate ND 210 42 ug/kg
84-66-2 Diethyl phthalate ND 420 84 ug/kg
131-11-3 Dimethyl phthalate ND 210 42 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 420 84 ug/kg
206-44-0 Fluoranthene ND 210 21 ug/kg
86-73-7 Fluorene ND 210 21 ug/kg
118-74-1 Hexachlorobenzene ND 210 21 ug/kg
87-68-3 Hexachlorobutadiene ND 210 42 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 210 92 ug/kg
67-72-1 Hexachloroethane ND 210 42 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 210 21 ug/kg
78-59-1 Isophorone ND 210 21 ug/kg
91-57-6 2-Methylnaphthalene ND 210 21 ug/kg
88-74-4 2-Nitroaniline ND 210 42 ug/kg
99-09-2 3-Nitroaniline ND 210 42 ug/kg
100-01-6 4-Nitroaniline ND 210 42 ug/kg
91-20-3 Naphthalene ND 210 34 ug/kg
98-95-3 Nitrobenzene ND 210 21 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 210 21 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 210 21 ug/kg
85-01-8 Phenanthrene ND 210 21 ug/kg
129-00-0 Pyrene ND 210 21 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 210 21 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 65%40-102%
4165-62-2 Phenol-d5 75%41-100%
118-79-6 2,4,6-Tribromophenol 68%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW5/105-12
Lab Sample ID:F81928-2 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:78.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 67%40-105%
321-60-8 2-Fluorobiphenyl 68%43-107%
1718-51-0 Terphenyl-d14 73%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW5/105-12
Lab Sample ID:F81928-2 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C Percent Solids:78.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060044.D 1 05/06/11 AH n/a n/a GQR2610
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.58 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 7.1 3.5 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 76%56-136%
98-08-8 aaa-Trifluorotoluene 76%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW5/105-12
Lab Sample ID:F81928-2 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C SW846 3550C Percent Solids:78.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40271.D 1 05/03/11 SJL 05/02/11 OP36981 GZF1661
Run #2
Initial Weight Final Volume
Run #1 29.8 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 11 4.3 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 79%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW5/105-12
Lab Sample ID:F81928-2 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Percent Solids:78.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <2.5 2.5 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Arsenic a 1.4 1.3 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Barium a 197 25 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Beryllium a <0.63 0.63 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Cadmium a <0.50 0.50 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Chromium a 15.7 1.3 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Copper a 26.0 3.1 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Lead 5.9 1.3 mg/kg 1 05/03/11 05/03/11 RS SW846 6010C 1 SW846 3050B 4
Mercury <0.10 0.10 mg/kg 1 05/06/11 05/06/11 LM SW846 7471B 3 SW846 7471B 5
Molybdenum a <6.3 6.3 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Nickel a 12.8 5.0 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Selenium a <2.5 2.5 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Silver a <1.3 1.3 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Tin a <6.3 6.3 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Zinc a 40.2 2.5 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
(1) Instrument QC Batch: MA8921
(2) Instrument QC Batch: MA8926
(3) Instrument QC Batch: MA8928
(4) Prep QC Batch: MP20489
(5) Prep QC Batch: MP20518
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Client Sample ID:TB-04/28/11
Lab Sample ID:F81928-3 Date Sampled:04/28/11
Matrix:SO - Trip Blank Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F049384.D 1 05/05/11 CW n/a n/a VF1486
Run #2
Initial Weight
Run #1 5.00 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 50 20 ug/kg
71-43-2 Benzene ND 5.0 1.5 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.1 ug/kg
75-25-2 Bromoform ND 5.0 1.5 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.2 ug/kg
75-15-0 Carbon disulfide ND 5.0 2.0 ug/kg
56-23-5 Carbon tetrachloride ND 5.0 1.8 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.1 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.4 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.2 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.5 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.5 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.1 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg
591-78-6 2-Hexanone ND 25 5.4 ug/kg
108-10-1 4-Methyl-2-pentanone ND 25 5.5 ug/kg
74-83-9 Methyl bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl chloride ND 5.0 2.0 ug/kg
75-09-2 Methylene chloride ND 10 4.6 ug/kg
78-93-3 Methyl ethyl ketone ND 25 6.1 ug/kg
100-42-5 Styrene ND 5.0 2.6 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.1 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.2 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.1 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.0 ug/kg
108-88-3 Toluene ND 5.0 1.2 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.2 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:TB-04/28/11
Lab Sample ID:F81928-3 Date Sampled:04/28/11
Matrix:SO - Trip Blank Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 5.0 1.5 ug/kg
1330-20-7 Xylene (total)ND 15 3.2 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%80-121%
2037-26-5 Toluene-D8 99%71-130%
460-00-4 4-Bromofluorobenzene 99%59-148%
17060-07-0 1,2-Dichloroethane-D4 106%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B1/0.5-2
Lab Sample ID:F81928-4 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:72.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F049408.D 1 05/06/11 CW n/a n/a VF1487
Run #2
Initial Weight
Run #1 5.75 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 60 24 ug/kg
71-43-2 Benzene ND 6.0 1.8 ug/kg
75-27-4 Bromodichloromethane ND 6.0 1.3 ug/kg
75-25-2 Bromoform ND 6.0 1.8 ug/kg
108-90-7 Chlorobenzene ND 6.0 1.2 ug/kg
75-00-3 Chloroethane ND 6.0 2.4 ug/kg
67-66-3 Chloroform ND 6.0 1.4 ug/kg
75-15-0 Carbon disulfide ND 6.0 2.4 ug/kg
56-23-5 Carbon tetrachloride ND 6.0 2.2 ug/kg
75-34-3 1,1-Dichloroethane ND 6.0 1.3 ug/kg
75-35-4 1,1-Dichloroethylene ND 6.0 1.7 ug/kg
107-06-2 1,2-Dichloroethane ND 6.0 1.2 ug/kg
78-87-5 1,2-Dichloropropane ND 6.0 1.4 ug/kg
124-48-1 Dibromochloromethane ND 6.0 1.2 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 6.0 1.8 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 6.0 1.2 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 6.0 1.8 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 6.0 1.3 ug/kg
100-41-4 Ethylbenzene ND 6.0 1.2 ug/kg
591-78-6 2-Hexanone ND 30 6.5 ug/kg
108-10-1 4-Methyl-2-pentanone ND 30 6.6 ug/kg
74-83-9 Methyl bromide ND 6.0 2.4 ug/kg
74-87-3 Methyl chloride ND 6.0 2.4 ug/kg
75-09-2 Methylene chloride ND 12 5.5 ug/kg
78-93-3 Methyl ethyl ketone ND 30 7.3 ug/kg
100-42-5 Styrene ND 6.0 3.1 ug/kg
71-55-6 1,1,1-Trichloroethane ND 6.0 1.3 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 6.0 1.4 ug/kg
79-00-5 1,1,2-Trichloroethane ND 6.0 1.3 ug/kg
127-18-4 Tetrachloroethylene ND 6.0 1.2 ug/kg
108-88-3 Toluene ND 6.0 1.4 ug/kg
79-01-6 Trichloroethylene ND 6.0 1.4 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B1/0.5-2
Lab Sample ID:F81928-4 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:72.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 6.0 1.8 ug/kg
1330-20-7 Xylene (total)ND 18 3.8 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 107%80-121%
2037-26-5 Toluene-D8 96%71-130%
460-00-4 4-Bromofluorobenzene 101%59-148%
17060-07-0 1,2-Dichloroethane-D4 118%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B1/0.5-2
Lab Sample ID:F81928-4 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:72.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025250.D 1 05/05/11 MG 05/03/11 OP36999 SU1213
Run #2
Initial Weight Final Volume
Run #1 30.2 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1100 400 ug/kg
95-57-8 2-Chlorophenol ND 230 23 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 230 23 ug/kg
120-83-2 2,4-Dichlorophenol ND 230 23 ug/kg
105-67-9 2,4-Dimethylphenol ND 230 29 ug/kg
51-28-5 2,4-Dinitrophenol ND 1100 460 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 460 91 ug/kg
95-48-7 2-Methylphenol ND 230 23 ug/kg
3&4-Methylphenol ND 230 33 ug/kg
88-75-5 2-Nitrophenol ND 230 23 ug/kg
100-02-7 4-Nitrophenol ND 1100 180 ug/kg
87-86-5 Pentachlorophenol ND 1100 270 ug/kg
108-95-2 Phenol ND 230 23 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 230 23 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 230 23 ug/kg
83-32-9 Acenaphthene ND 230 23 ug/kg
208-96-8 Acenaphthylene ND 230 23 ug/kg
120-12-7 Anthracene ND 230 23 ug/kg
56-55-3 Benzo(a)anthracene ND 230 23 ug/kg
50-32-8 Benzo(a)pyrene ND 230 23 ug/kg
205-99-2 Benzo(b)fluoranthene ND 230 23 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 230 23 ug/kg
207-08-9 Benzo(k)fluoranthene ND 230 23 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 230 23 ug/kg
85-68-7 Butyl benzyl phthalate ND 230 46 ug/kg
100-51-6 Benzyl Alcohol ND 230 46 ug/kg
91-58-7 2-Chloronaphthalene ND 230 46 ug/kg
106-47-8 4-Chloroaniline ND 230 23 ug/kg
86-74-8 Carbazole ND 230 23 ug/kg
218-01-9 Chrysene ND 230 23 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 230 23 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 230 23 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:B1/0.5-2
Lab Sample ID:F81928-4 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:72.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 230 23 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 230 23 ug/kg
95-50-1 1,2-Dichlorobenzene ND 230 46 ug/kg
541-73-1 1,3-Dichlorobenzene ND 230 46 ug/kg
106-46-7 1,4-Dichlorobenzene ND 230 46 ug/kg
121-14-2 2,4-Dinitrotoluene ND 230 23 ug/kg
606-20-2 2,6-Dinitrotoluene ND 230 27 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 460 46 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 230 23 ug/kg
132-64-9 Dibenzofuran ND 230 23 ug/kg
84-74-2 Di-n-butyl phthalate ND 460 91 ug/kg
117-84-0 Di-n-octyl phthalate ND 230 46 ug/kg
84-66-2 Diethyl phthalate ND 460 91 ug/kg
131-11-3 Dimethyl phthalate ND 230 46 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 460 91 ug/kg
206-44-0 Fluoranthene ND 230 23 ug/kg
86-73-7 Fluorene ND 230 23 ug/kg
118-74-1 Hexachlorobenzene ND 230 23 ug/kg
87-68-3 Hexachlorobutadiene ND 230 46 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 230 100 ug/kg
67-72-1 Hexachloroethane ND 230 46 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 230 23 ug/kg
78-59-1 Isophorone ND 230 23 ug/kg
91-57-6 2-Methylnaphthalene ND 230 23 ug/kg
88-74-4 2-Nitroaniline ND 230 46 ug/kg
99-09-2 3-Nitroaniline ND 230 46 ug/kg
100-01-6 4-Nitroaniline ND 230 46 ug/kg
91-20-3 Naphthalene ND 230 36 ug/kg
98-95-3 Nitrobenzene ND 230 23 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 230 23 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 230 23 ug/kg
85-01-8 Phenanthrene ND 230 23 ug/kg
129-00-0 Pyrene ND 230 23 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 230 23 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 62%40-102%
4165-62-2 Phenol-d5 69%41-100%
118-79-6 2,4,6-Tribromophenol 68%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B1/0.5-2
Lab Sample ID:F81928-4 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:72.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 64%40-105%
321-60-8 2-Fluorobiphenyl 65%43-107%
1718-51-0 Terphenyl-d14 73%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B1/0.5-2
Lab Sample ID:F81928-4 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C Percent Solids:72.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060046.D 1 05/06/11 AH n/a n/a GQR2610
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 4.87 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 8.9 4.5 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 79%56-136%
98-08-8 aaa-Trifluorotoluene 75%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B1/0.5-2
Lab Sample ID:F81928-4 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8082A SW846 3550C Percent Solids:72.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 XX055989.D 1 05/03/11 NJ 05/02/11 OP36984 GXX864
Run #2
Initial Weight Final Volume
Run #1 30.1 g 10.0 ml
Run #2
PCB List
CAS No.Compound Result RL MDL Units Q
12674-11-2 Aroclor 1016 ND 23 9.1 ug/kg
11104-28-2 Aroclor 1221 ND 23 11 ug/kg
11141-16-5 Aroclor 1232 ND 23 11 ug/kg
53469-21-9 Aroclor 1242 ND 23 9.1 ug/kg
12672-29-6 Aroclor 1248 ND 23 9.1 ug/kg
11097-69-1 Aroclor 1254 ND 23 9.1 ug/kg
11096-82-5 Aroclor 1260 ND 23 9.1 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 72%44-126%
2051-24-3 Decachlorobiphenyl 82%39-157%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B1/0.5-2
Lab Sample ID:F81928-4 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C SW846 3550C Percent Solids:72.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40272.D 1 05/03/11 SJL 05/02/11 OP36981 GZF1661
Run #2
Initial Weight Final Volume
Run #1 29.6 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 12 4.6 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 74%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B1/0.5-2
Lab Sample ID:F81928-4 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Percent Solids:72.7
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <5.0 5.0 mg/kg 4 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Arsenic a 2.5 2.5 mg/kg 4 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Barium 19.2 13 mg/kg 1 05/03/11 05/03/11 RS SW846 6010C 1 SW846 3050B 4
Beryllium 0.59 0.31 mg/kg 1 05/03/11 05/03/11 RS SW846 6010C 1 SW846 3050B 4
Cadmium a <1.0 1.0 mg/kg 4 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Chromium a 32.0 2.5 mg/kg 4 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Copper a 31.5 6.3 mg/kg 4 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Lead a 17.0 5.0 mg/kg 4 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Mercury <0.11 0.11 mg/kg 1 05/06/11 05/06/11 LM SW846 7471B 3 SW846 7471B 5
Molybdenum a <13 13 mg/kg 4 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Nickel a <10 10 mg/kg 4 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Selenium a <5.0 5.0 mg/kg 4 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Silver a <2.5 2.5 mg/kg 4 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Tin <3.1 3.1 mg/kg 1 05/03/11 05/03/11 RS SW846 6010C 1 SW846 3050B 4
Zinc a 19.4 5.0 mg/kg 4 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
(1) Instrument QC Batch: MA8921
(2) Instrument QC Batch: MA8926
(3) Instrument QC Batch: MA8928
(4) Prep QC Batch: MP20489
(5) Prep QC Batch: MP20518
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Client Sample ID:B1/10-12
Lab Sample ID:F81928-5 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:75.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F049409.D 1 05/06/11 CW n/a n/a VF1487
Run #2
Initial Weight
Run #1 5.52 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 60 24 ug/kg
71-43-2 Benzene ND 6.0 1.8 ug/kg
75-27-4 Bromodichloromethane ND 6.0 1.3 ug/kg
75-25-2 Bromoform ND 6.0 1.8 ug/kg
108-90-7 Chlorobenzene ND 6.0 1.2 ug/kg
75-00-3 Chloroethane ND 6.0 2.4 ug/kg
67-66-3 Chloroform ND 6.0 1.4 ug/kg
75-15-0 Carbon disulfide ND 6.0 2.4 ug/kg
56-23-5 Carbon tetrachloride ND 6.0 2.2 ug/kg
75-34-3 1,1-Dichloroethane ND 6.0 1.3 ug/kg
75-35-4 1,1-Dichloroethylene ND 6.0 1.7 ug/kg
107-06-2 1,2-Dichloroethane ND 6.0 1.2 ug/kg
78-87-5 1,2-Dichloropropane ND 6.0 1.4 ug/kg
124-48-1 Dibromochloromethane ND 6.0 1.2 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 6.0 1.8 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 6.0 1.2 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 6.0 1.8 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 6.0 1.3 ug/kg
100-41-4 Ethylbenzene ND 6.0 1.2 ug/kg
591-78-6 2-Hexanone ND 30 6.5 ug/kg
108-10-1 4-Methyl-2-pentanone ND 30 6.6 ug/kg
74-83-9 Methyl bromide ND 6.0 2.4 ug/kg
74-87-3 Methyl chloride ND 6.0 2.4 ug/kg
75-09-2 Methylene chloride ND 12 5.5 ug/kg
78-93-3 Methyl ethyl ketone ND 30 7.4 ug/kg
100-42-5 Styrene ND 6.0 3.1 ug/kg
71-55-6 1,1,1-Trichloroethane ND 6.0 1.3 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 6.0 1.4 ug/kg
79-00-5 1,1,2-Trichloroethane ND 6.0 1.3 ug/kg
127-18-4 Tetrachloroethylene ND 6.0 1.2 ug/kg
108-88-3 Toluene ND 6.0 1.4 ug/kg
79-01-6 Trichloroethylene ND 6.0 1.4 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B1/10-12
Lab Sample ID:F81928-5 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:75.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 6.0 1.8 ug/kg
1330-20-7 Xylene (total)ND 18 3.9 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%80-121%
2037-26-5 Toluene-D8 98%71-130%
460-00-4 4-Bromofluorobenzene 102%59-148%
17060-07-0 1,2-Dichloroethane-D4 111%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:B1/10-12
Lab Sample ID:F81928-5 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:75.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025251.D 1 05/05/11 MG 05/03/11 OP36999 SU1213
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1100 390 ug/kg
95-57-8 2-Chlorophenol ND 220 22 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 220 22 ug/kg
120-83-2 2,4-Dichlorophenol ND 220 22 ug/kg
105-67-9 2,4-Dimethylphenol ND 220 28 ug/kg
51-28-5 2,4-Dinitrophenol ND 1100 440 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 440 89 ug/kg
95-48-7 2-Methylphenol ND 220 22 ug/kg
3&4-Methylphenol ND 220 32 ug/kg
88-75-5 2-Nitrophenol ND 220 22 ug/kg
100-02-7 4-Nitrophenol ND 1100 180 ug/kg
87-86-5 Pentachlorophenol ND 1100 270 ug/kg
108-95-2 Phenol ND 220 22 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 220 22 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 220 22 ug/kg
83-32-9 Acenaphthene ND 220 22 ug/kg
208-96-8 Acenaphthylene ND 220 22 ug/kg
120-12-7 Anthracene ND 220 22 ug/kg
56-55-3 Benzo(a)anthracene ND 220 22 ug/kg
50-32-8 Benzo(a)pyrene ND 220 22 ug/kg
205-99-2 Benzo(b)fluoranthene ND 220 22 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 220 22 ug/kg
207-08-9 Benzo(k)fluoranthene ND 220 22 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 220 22 ug/kg
85-68-7 Butyl benzyl phthalate ND 220 44 ug/kg
100-51-6 Benzyl Alcohol ND 220 44 ug/kg
91-58-7 2-Chloronaphthalene ND 220 44 ug/kg
106-47-8 4-Chloroaniline ND 220 22 ug/kg
86-74-8 Carbazole ND 220 22 ug/kg
218-01-9 Chrysene ND 220 22 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 220 22 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 220 22 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B1/10-12
Lab Sample ID:F81928-5 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:75.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 220 22 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 220 22 ug/kg
95-50-1 1,2-Dichlorobenzene ND 220 44 ug/kg
541-73-1 1,3-Dichlorobenzene ND 220 44 ug/kg
106-46-7 1,4-Dichlorobenzene ND 220 44 ug/kg
121-14-2 2,4-Dinitrotoluene ND 220 22 ug/kg
606-20-2 2,6-Dinitrotoluene ND 220 26 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 440 44 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 220 22 ug/kg
132-64-9 Dibenzofuran ND 220 22 ug/kg
84-74-2 Di-n-butyl phthalate ND 440 89 ug/kg
117-84-0 Di-n-octyl phthalate ND 220 44 ug/kg
84-66-2 Diethyl phthalate ND 440 89 ug/kg
131-11-3 Dimethyl phthalate ND 220 44 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 440 89 ug/kg
206-44-0 Fluoranthene ND 220 22 ug/kg
86-73-7 Fluorene ND 220 22 ug/kg
118-74-1 Hexachlorobenzene ND 220 22 ug/kg
87-68-3 Hexachlorobutadiene ND 220 44 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 220 98 ug/kg
67-72-1 Hexachloroethane ND 220 44 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 220 22 ug/kg
78-59-1 Isophorone ND 220 22 ug/kg
91-57-6 2-Methylnaphthalene ND 220 22 ug/kg
88-74-4 2-Nitroaniline ND 220 44 ug/kg
99-09-2 3-Nitroaniline ND 220 44 ug/kg
100-01-6 4-Nitroaniline ND 220 44 ug/kg
91-20-3 Naphthalene ND 220 36 ug/kg
98-95-3 Nitrobenzene ND 220 22 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 220 22 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 220 22 ug/kg
85-01-8 Phenanthrene ND 220 22 ug/kg
129-00-0 Pyrene ND 220 22 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 220 22 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 66%40-102%
4165-62-2 Phenol-d5 74%41-100%
118-79-6 2,4,6-Tribromophenol 68%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B1/10-12
Lab Sample ID:F81928-5 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:75.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 68%40-105%
321-60-8 2-Fluorobiphenyl 69%43-107%
1718-51-0 Terphenyl-d14 74%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B1/10-12
Lab Sample ID:F81928-5 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C Percent Solids:75.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060047.D 1 05/06/11 AH n/a n/a GQR2610
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.24 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 8.0 4.0 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 75%56-136%
98-08-8 aaa-Trifluorotoluene 76%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B1/10-12
Lab Sample ID:F81928-5 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C SW846 3550C Percent Solids:75.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40273.D 1 05/03/11 SJL 05/02/11 OP36981 GZF1661
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 11 4.4 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 71%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B1/10-12
Lab Sample ID:F81928-5 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Percent Solids:75.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <5.2 5.2 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Arsenic a <2.6 2.6 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Barium a 207 52 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Beryllium a 1.4 1.3 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Cadmium a <1.0 1.0 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Chromium a 12.0 2.6 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Copper a 26.4 6.6 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Lead 5.0 1.0 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Mercury <0.11 0.11 mg/kg 1 05/06/11 05/06/11 LM SW846 7471B 3 SW846 7471B 5
Molybdenum a <13 13 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Nickel a 26.8 10 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Selenium a <5.2 5.2 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Silver a <2.6 2.6 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Tin a <13 13 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Zinc a 79.5 5.2 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
(1) Instrument QC Batch: MA8921
(2) Instrument QC Batch: MA8926
(3) Instrument QC Batch: MA8928
(4) Prep QC Batch: MP20489
(5) Prep QC Batch: MP20518
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Client Sample ID:B2/0.5-2
Lab Sample ID:F81928-6 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:67.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F049410.D 1 05/06/11 CW n/a n/a VF1487
Run #2
Initial Weight
Run #1 4.87 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 76 30 ug/kg
71-43-2 Benzene ND 7.6 2.3 ug/kg
75-27-4 Bromodichloromethane ND 7.6 1.7 ug/kg
75-25-2 Bromoform ND 7.6 2.3 ug/kg
108-90-7 Chlorobenzene ND 7.6 1.5 ug/kg
75-00-3 Chloroethane ND 7.6 3.0 ug/kg
67-66-3 Chloroform ND 7.6 1.8 ug/kg
75-15-0 Carbon disulfide ND 7.6 3.0 ug/kg
56-23-5 Carbon tetrachloride ND 7.6 2.7 ug/kg
75-34-3 1,1-Dichloroethane ND 7.6 1.7 ug/kg
75-35-4 1,1-Dichloroethylene ND 7.6 2.1 ug/kg
107-06-2 1,2-Dichloroethane ND 7.6 1.5 ug/kg
78-87-5 1,2-Dichloropropane ND 7.6 1.8 ug/kg
124-48-1 Dibromochloromethane ND 7.6 1.5 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 7.6 2.3 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 7.6 1.5 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 7.6 2.3 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 7.6 1.7 ug/kg
100-41-4 Ethylbenzene ND 7.6 1.5 ug/kg
591-78-6 2-Hexanone ND 38 8.2 ug/kg
108-10-1 4-Methyl-2-pentanone ND 38 8.4 ug/kg
74-83-9 Methyl bromide ND 7.6 3.0 ug/kg
74-87-3 Methyl chloride ND 7.6 3.0 ug/kg
75-09-2 Methylene chloride ND 15 7.0 ug/kg
78-93-3 Methyl ethyl ketone ND 38 9.3 ug/kg
100-42-5 Styrene ND 7.6 4.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 7.6 1.7 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 7.6 1.8 ug/kg
79-00-5 1,1,2-Trichloroethane ND 7.6 1.7 ug/kg
127-18-4 Tetrachloroethylene ND 7.6 1.5 ug/kg
108-88-3 Toluene ND 7.6 1.8 ug/kg
79-01-6 Trichloroethylene ND 7.6 1.8 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B2/0.5-2
Lab Sample ID:F81928-6 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:67.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 7.6 2.3 ug/kg
1330-20-7 Xylene (total)ND 23 4.9 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 107%80-121%
2037-26-5 Toluene-D8 96%71-130%
460-00-4 4-Bromofluorobenzene 100%59-148%
17060-07-0 1,2-Dichloroethane-D4 116%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:B2/0.5-2
Lab Sample ID:F81928-6 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:67.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025254.D 1 05/05/11 MG 05/03/11 OP36999 SU1213
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1200 430 ug/kg
95-57-8 2-Chlorophenol ND 250 25 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 250 25 ug/kg
120-83-2 2,4-Dichlorophenol ND 250 25 ug/kg
105-67-9 2,4-Dimethylphenol ND 250 31 ug/kg
51-28-5 2,4-Dinitrophenol ND 1200 490 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 490 99 ug/kg
95-48-7 2-Methylphenol ND 250 25 ug/kg
3&4-Methylphenol ND 250 36 ug/kg
88-75-5 2-Nitrophenol ND 250 25 ug/kg
100-02-7 4-Nitrophenol ND 1200 200 ug/kg
87-86-5 Pentachlorophenol ND 1200 300 ug/kg
108-95-2 Phenol ND 250 25 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 250 25 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 250 25 ug/kg
83-32-9 Acenaphthene ND 250 25 ug/kg
208-96-8 Acenaphthylene ND 250 25 ug/kg
120-12-7 Anthracene ND 250 25 ug/kg
56-55-3 Benzo(a)anthracene ND 250 25 ug/kg
50-32-8 Benzo(a)pyrene ND 250 25 ug/kg
205-99-2 Benzo(b)fluoranthene ND 250 25 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 250 25 ug/kg
207-08-9 Benzo(k)fluoranthene ND 250 25 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 250 25 ug/kg
85-68-7 Butyl benzyl phthalate ND 250 49 ug/kg
100-51-6 Benzyl Alcohol ND 250 49 ug/kg
91-58-7 2-Chloronaphthalene ND 250 49 ug/kg
106-47-8 4-Chloroaniline ND 250 25 ug/kg
86-74-8 Carbazole ND 250 25 ug/kg
218-01-9 Chrysene ND 250 25 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 250 25 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 250 25 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:B2/0.5-2
Lab Sample ID:F81928-6 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:67.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 250 25 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 250 25 ug/kg
95-50-1 1,2-Dichlorobenzene ND 250 49 ug/kg
541-73-1 1,3-Dichlorobenzene ND 250 49 ug/kg
106-46-7 1,4-Dichlorobenzene ND 250 49 ug/kg
121-14-2 2,4-Dinitrotoluene ND 250 25 ug/kg
606-20-2 2,6-Dinitrotoluene ND 250 29 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 490 49 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 250 25 ug/kg
132-64-9 Dibenzofuran ND 250 25 ug/kg
84-74-2 Di-n-butyl phthalate ND 490 99 ug/kg
117-84-0 Di-n-octyl phthalate ND 250 49 ug/kg
84-66-2 Diethyl phthalate ND 490 99 ug/kg
131-11-3 Dimethyl phthalate ND 250 49 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 490 99 ug/kg
206-44-0 Fluoranthene ND 250 25 ug/kg
86-73-7 Fluorene ND 250 25 ug/kg
118-74-1 Hexachlorobenzene ND 250 25 ug/kg
87-68-3 Hexachlorobutadiene ND 250 49 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 250 110 ug/kg
67-72-1 Hexachloroethane ND 250 49 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 250 25 ug/kg
78-59-1 Isophorone ND 250 25 ug/kg
91-57-6 2-Methylnaphthalene ND 250 25 ug/kg
88-74-4 2-Nitroaniline ND 250 49 ug/kg
99-09-2 3-Nitroaniline ND 250 49 ug/kg
100-01-6 4-Nitroaniline ND 250 49 ug/kg
91-20-3 Naphthalene ND 250 40 ug/kg
98-95-3 Nitrobenzene ND 250 25 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 250 25 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 250 25 ug/kg
85-01-8 Phenanthrene ND 250 25 ug/kg
129-00-0 Pyrene ND 250 25 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 250 25 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 60%40-102%
4165-62-2 Phenol-d5 67%41-100%
118-79-6 2,4,6-Tribromophenol 66%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:B2/0.5-2
Lab Sample ID:F81928-6 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:67.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 61%40-105%
321-60-8 2-Fluorobiphenyl 62%43-107%
1718-51-0 Terphenyl-d14 68%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B2/0.5-2
Lab Sample ID:F81928-6 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C Percent Solids:67.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060048.D 1 05/06/11 AH n/a n/a GQR2610
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 4.81 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 10 5.1 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 77%56-136%
98-08-8 aaa-Trifluorotoluene 75%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B2/0.5-2
Lab Sample ID:F81928-6 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8082A SW846 3550C Percent Solids:67.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 XX055990.D 1 05/03/11 NJ 05/02/11 OP36984 GXX864
Run #2
Initial Weight Final Volume
Run #1 29.9 g 10.0 ml
Run #2
PCB List
CAS No.Compound Result RL MDL Units Q
12674-11-2 Aroclor 1016 ND 25 9.9 ug/kg
11104-28-2 Aroclor 1221 ND 25 12 ug/kg
11141-16-5 Aroclor 1232 ND 25 12 ug/kg
53469-21-9 Aroclor 1242 ND 25 9.9 ug/kg
12672-29-6 Aroclor 1248 ND 25 9.9 ug/kg
11097-69-1 Aroclor 1254 ND 25 9.9 ug/kg
11096-82-5 Aroclor 1260 ND 25 9.9 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 74%44-126%
2051-24-3 Decachlorobiphenyl 81%39-157%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B2/0.5-2
Lab Sample ID:F81928-6 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C SW846 3550C Percent Solids:67.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40274.D 1 05/03/11 SJL 05/02/11 OP36981 GZF1661
Run #2
Initial Weight Final Volume
Run #1 30.2 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 12 4.9 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 73%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B2/0.5-2
Lab Sample ID:F81928-6 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Percent Solids:67.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <2.6 2.6 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Arsenic a 1.8 1.3 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Barium 47.9 13 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Beryllium 0.52 0.32 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Cadmium a <0.51 0.51 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Chromium a 105 1.3 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Copper a 102 3.2 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Lead a 13.3 2.6 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Mercury <0.11 0.11 mg/kg 1 05/09/11 05/09/11 LM SW846 7471B 3 SW846 7471B 5
Molybdenum a <6.4 6.4 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Nickel a 18.6 5.1 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Selenium a 3.8 2.6 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Silver a <1.3 1.3 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Tin <3.2 3.2 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Zinc a 34.2 2.6 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
(1) Instrument QC Batch: MA8921
(2) Instrument QC Batch: MA8926
(3) Instrument QC Batch: MA8930
(4) Prep QC Batch: MP20489
(5) Prep QC Batch: MP20527
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Client Sample ID:B2/10-12
Lab Sample ID:F81928-7 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:72.0
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 G0072764.D 1 05/06/11 SH n/a n/a VG2718
Run #2
Initial Weight
Run #1 5.51 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 63 25 ug/kg
71-43-2 Benzene ND 6.3 1.9 ug/kg
75-27-4 Bromodichloromethane ND 6.3 1.4 ug/kg
75-25-2 Bromoform ND 6.3 1.9 ug/kg
108-90-7 Chlorobenzene ND 6.3 1.3 ug/kg
75-00-3 Chloroethane ND 6.3 2.5 ug/kg
67-66-3 Chloroform ND 6.3 1.5 ug/kg
75-15-0 Carbon disulfide ND 6.3 2.5 ug/kg
56-23-5 Carbon tetrachloride ND 6.3 2.3 ug/kg
75-34-3 1,1-Dichloroethane ND 6.3 1.4 ug/kg
75-35-4 1,1-Dichloroethylene ND 6.3 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 6.3 1.3 ug/kg
78-87-5 1,2-Dichloropropane ND 6.3 1.5 ug/kg
124-48-1 Dibromochloromethane ND 6.3 1.3 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 6.3 1.9 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 6.3 1.3 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 6.3 1.9 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 6.3 1.4 ug/kg
100-41-4 Ethylbenzene ND 6.3 1.3 ug/kg
591-78-6 2-Hexanone ND 32 6.8 ug/kg
108-10-1 4-Methyl-2-pentanone ND 32 6.9 ug/kg
74-83-9 Methyl bromide ND 6.3 2.5 ug/kg
74-87-3 Methyl chloride ND 6.3 2.5 ug/kg
75-09-2 Methylene chloride a ND 13 5.8 ug/kg
78-93-3 Methyl ethyl ketone ND 32 7.7 ug/kg
100-42-5 Styrene ND 6.3 3.3 ug/kg
71-55-6 1,1,1-Trichloroethane ND 6.3 1.4 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 6.3 1.5 ug/kg
79-00-5 1,1,2-Trichloroethane ND 6.3 1.4 ug/kg
127-18-4 Tetrachloroethylene ND 6.3 1.3 ug/kg
108-88-3 Toluene ND 6.3 1.5 ug/kg
79-01-6 Trichloroethylene ND 6.3 1.5 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:B2/10-12
Lab Sample ID:F81928-7 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:72.0
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 6.3 1.9 ug/kg
1330-20-7 Xylene (total)ND 19 4.0 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 93%80-121%
2037-26-5 Toluene-D8 90%71-130%
460-00-4 4-Bromofluorobenzene 99%59-148%
17060-07-0 1,2-Dichloroethane-D4 97%77-123%
(a) CCV outside of control limits; results may be biased low.
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:B2/10-12
Lab Sample ID:F81928-7 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:72.0
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025255.D 1 05/05/11 MG 05/03/11 OP36999 SU1213
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1200 410 ug/kg
95-57-8 2-Chlorophenol ND 230 23 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 230 23 ug/kg
120-83-2 2,4-Dichlorophenol ND 230 23 ug/kg
105-67-9 2,4-Dimethylphenol ND 230 29 ug/kg
51-28-5 2,4-Dinitrophenol ND 1200 460 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 460 93 ug/kg
95-48-7 2-Methylphenol ND 230 23 ug/kg
3&4-Methylphenol ND 230 33 ug/kg
88-75-5 2-Nitrophenol ND 230 23 ug/kg
100-02-7 4-Nitrophenol ND 1200 190 ug/kg
87-86-5 Pentachlorophenol ND 1200 280 ug/kg
108-95-2 Phenol ND 230 23 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 230 23 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 230 23 ug/kg
83-32-9 Acenaphthene ND 230 23 ug/kg
208-96-8 Acenaphthylene ND 230 23 ug/kg
120-12-7 Anthracene ND 230 23 ug/kg
56-55-3 Benzo(a)anthracene ND 230 23 ug/kg
50-32-8 Benzo(a)pyrene ND 230 23 ug/kg
205-99-2 Benzo(b)fluoranthene ND 230 23 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 230 23 ug/kg
207-08-9 Benzo(k)fluoranthene ND 230 23 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 230 23 ug/kg
85-68-7 Butyl benzyl phthalate ND 230 46 ug/kg
100-51-6 Benzyl Alcohol ND 230 46 ug/kg
91-58-7 2-Chloronaphthalene ND 230 46 ug/kg
106-47-8 4-Chloroaniline ND 230 23 ug/kg
86-74-8 Carbazole ND 230 23 ug/kg
218-01-9 Chrysene ND 230 23 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 230 23 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 230 23 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:B2/10-12
Lab Sample ID:F81928-7 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:72.0
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 230 23 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 230 23 ug/kg
95-50-1 1,2-Dichlorobenzene ND 230 46 ug/kg
541-73-1 1,3-Dichlorobenzene ND 230 46 ug/kg
106-46-7 1,4-Dichlorobenzene ND 230 46 ug/kg
121-14-2 2,4-Dinitrotoluene ND 230 23 ug/kg
606-20-2 2,6-Dinitrotoluene ND 230 27 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 460 46 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 230 23 ug/kg
132-64-9 Dibenzofuran ND 230 23 ug/kg
84-74-2 Di-n-butyl phthalate ND 460 93 ug/kg
117-84-0 Di-n-octyl phthalate ND 230 46 ug/kg
84-66-2 Diethyl phthalate ND 460 93 ug/kg
131-11-3 Dimethyl phthalate ND 230 46 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 460 93 ug/kg
206-44-0 Fluoranthene ND 230 23 ug/kg
86-73-7 Fluorene ND 230 23 ug/kg
118-74-1 Hexachlorobenzene ND 230 23 ug/kg
87-68-3 Hexachlorobutadiene ND 230 46 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 230 100 ug/kg
67-72-1 Hexachloroethane ND 230 46 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 230 23 ug/kg
78-59-1 Isophorone ND 230 23 ug/kg
91-57-6 2-Methylnaphthalene ND 230 23 ug/kg
88-74-4 2-Nitroaniline ND 230 46 ug/kg
99-09-2 3-Nitroaniline ND 230 46 ug/kg
100-01-6 4-Nitroaniline ND 230 46 ug/kg
91-20-3 Naphthalene ND 230 37 ug/kg
98-95-3 Nitrobenzene ND 230 23 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 230 23 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 230 23 ug/kg
85-01-8 Phenanthrene ND 230 23 ug/kg
129-00-0 Pyrene ND 230 23 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 230 23 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 60%40-102%
4165-62-2 Phenol-d5 67%41-100%
118-79-6 2,4,6-Tribromophenol 64%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B2/10-12
Lab Sample ID:F81928-7 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:72.0
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 62%40-105%
321-60-8 2-Fluorobiphenyl 64%43-107%
1718-51-0 Terphenyl-d14 72%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B2/10-12
Lab Sample ID:F81928-7 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C Percent Solids:72.0
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060049.D 1 05/06/11 AH n/a n/a GQR2610
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.47 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 8.3 4.1 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 72%56-136%
98-08-8 aaa-Trifluorotoluene 73%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B2/10-12
Lab Sample ID:F81928-7 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C SW846 3550C Percent Solids:72.0
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40275.D 1 05/03/11 SJL 05/02/11 OP36981 GZF1661
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 12 4.6 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 84%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B2/10-12
Lab Sample ID:F81928-7 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Percent Solids:72.0
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <5.8 5.8 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Arsenic a <2.9 2.9 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Barium a 174 58 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Beryllium a <1.4 1.4 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Cadmium a <1.2 1.2 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Chromium a 106 2.9 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Copper a 69.6 7.2 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Lead 3.1 1.2 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Mercury <0.12 0.12 mg/kg 1 05/09/11 05/09/11 LM SW846 7471B 3 SW846 7471B 5
Molybdenum a <14 14 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Nickel a 63.6 12 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Selenium a <5.8 5.8 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Silver a <2.9 2.9 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Tin a <14 14 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Zinc a 71.2 5.8 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
(1) Instrument QC Batch: MA8921
(2) Instrument QC Batch: MA8926
(3) Instrument QC Batch: MA8930
(4) Prep QC Batch: MP20489
(5) Prep QC Batch: MP20527
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Report of Analysis Page 1 of 2
Client Sample ID:B4/2-4
Lab Sample ID:F81928-8 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:82.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 G0072765.D 1 05/06/11 SH n/a n/a VG2718
Run #2
Initial Weight
Run #1 5.17 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 28.3 59 23 ug/kg J
71-43-2 Benzene ND 5.9 1.8 ug/kg
75-27-4 Bromodichloromethane ND 5.9 1.3 ug/kg
75-25-2 Bromoform ND 5.9 1.8 ug/kg
108-90-7 Chlorobenzene ND 5.9 1.2 ug/kg
75-00-3 Chloroethane ND 5.9 2.3 ug/kg
67-66-3 Chloroform ND 5.9 1.4 ug/kg
75-15-0 Carbon disulfide ND 5.9 2.3 ug/kg
56-23-5 Carbon tetrachloride ND 5.9 2.1 ug/kg
75-34-3 1,1-Dichloroethane ND 5.9 1.3 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.9 1.6 ug/kg
107-06-2 1,2-Dichloroethane ND 5.9 1.2 ug/kg
78-87-5 1,2-Dichloropropane ND 5.9 1.4 ug/kg
124-48-1 Dibromochloromethane ND 5.9 1.2 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.9 1.8 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.9 1.2 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.9 1.8 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.9 1.3 ug/kg
100-41-4 Ethylbenzene ND 5.9 1.2 ug/kg
591-78-6 2-Hexanone ND 29 6.3 ug/kg
108-10-1 4-Methyl-2-pentanone ND 29 6.4 ug/kg
74-83-9 Methyl bromide ND 5.9 2.3 ug/kg
74-87-3 Methyl chloride ND 5.9 2.3 ug/kg
75-09-2 Methylene chloride a ND 12 5.4 ug/kg
78-93-3 Methyl ethyl ketone ND 29 7.2 ug/kg
100-42-5 Styrene ND 5.9 3.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.9 1.3 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.9 1.4 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.9 1.3 ug/kg
127-18-4 Tetrachloroethylene ND 5.9 1.2 ug/kg
108-88-3 Toluene ND 5.9 1.4 ug/kg
79-01-6 Trichloroethylene ND 5.9 1.4 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B4/2-4
Lab Sample ID:F81928-8 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:82.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 5.9 1.8 ug/kg
1330-20-7 Xylene (total)ND 18 3.8 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%80-121%
2037-26-5 Toluene-D8 89%71-130%
460-00-4 4-Bromofluorobenzene 108%59-148%
17060-07-0 1,2-Dichloroethane-D4 105%77-123%
(a) CCV outside of control limits; results may be biased low.
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:B4/2-4
Lab Sample ID:F81928-8 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:82.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025256.D 1 05/05/11 MG 05/03/11 OP36999 SU1213
Run #2
Initial Weight Final Volume
Run #1 29.9 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1000 360 ug/kg
95-57-8 2-Chlorophenol ND 200 20 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 200 20 ug/kg
120-83-2 2,4-Dichlorophenol ND 200 20 ug/kg
105-67-9 2,4-Dimethylphenol ND 200 26 ug/kg
51-28-5 2,4-Dinitrophenol ND 1000 410 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 410 81 ug/kg
95-48-7 2-Methylphenol ND 200 20 ug/kg
3&4-Methylphenol ND 200 29 ug/kg
88-75-5 2-Nitrophenol ND 200 20 ug/kg
100-02-7 4-Nitrophenol ND 1000 160 ug/kg
87-86-5 Pentachlorophenol ND 1000 240 ug/kg
108-95-2 Phenol ND 200 20 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 200 20 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 200 20 ug/kg
83-32-9 Acenaphthene ND 200 20 ug/kg
208-96-8 Acenaphthylene ND 200 20 ug/kg
120-12-7 Anthracene ND 200 20 ug/kg
56-55-3 Benzo(a)anthracene ND 200 20 ug/kg
50-32-8 Benzo(a)pyrene ND 200 20 ug/kg
205-99-2 Benzo(b)fluoranthene ND 200 20 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 200 20 ug/kg
207-08-9 Benzo(k)fluoranthene ND 200 20 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 200 20 ug/kg
85-68-7 Butyl benzyl phthalate ND 200 41 ug/kg
100-51-6 Benzyl Alcohol ND 200 41 ug/kg
91-58-7 2-Chloronaphthalene ND 200 41 ug/kg
106-47-8 4-Chloroaniline ND 200 20 ug/kg
86-74-8 Carbazole ND 200 20 ug/kg
218-01-9 Chrysene ND 200 20 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 200 20 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 200 20 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:B4/2-4
Lab Sample ID:F81928-8 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:82.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 200 20 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 200 20 ug/kg
95-50-1 1,2-Dichlorobenzene ND 200 41 ug/kg
541-73-1 1,3-Dichlorobenzene ND 200 41 ug/kg
106-46-7 1,4-Dichlorobenzene ND 200 41 ug/kg
121-14-2 2,4-Dinitrotoluene ND 200 20 ug/kg
606-20-2 2,6-Dinitrotoluene ND 200 24 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 410 41 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 200 20 ug/kg
132-64-9 Dibenzofuran ND 200 20 ug/kg
84-74-2 Di-n-butyl phthalate ND 410 81 ug/kg
117-84-0 Di-n-octyl phthalate ND 200 41 ug/kg
84-66-2 Diethyl phthalate ND 410 81 ug/kg
131-11-3 Dimethyl phthalate ND 200 41 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 410 81 ug/kg
206-44-0 Fluoranthene ND 200 20 ug/kg
86-73-7 Fluorene ND 200 20 ug/kg
118-74-1 Hexachlorobenzene ND 200 20 ug/kg
87-68-3 Hexachlorobutadiene ND 200 41 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 200 89 ug/kg
67-72-1 Hexachloroethane ND 200 41 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 200 20 ug/kg
78-59-1 Isophorone ND 200 20 ug/kg
91-57-6 2-Methylnaphthalene ND 200 20 ug/kg
88-74-4 2-Nitroaniline ND 200 41 ug/kg
99-09-2 3-Nitroaniline ND 200 41 ug/kg
100-01-6 4-Nitroaniline ND 200 41 ug/kg
91-20-3 Naphthalene ND 200 32 ug/kg
98-95-3 Nitrobenzene ND 200 20 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 200 20 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 200 20 ug/kg
85-01-8 Phenanthrene ND 200 20 ug/kg
129-00-0 Pyrene ND 200 20 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 200 20 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 62%40-102%
4165-62-2 Phenol-d5 69%41-100%
118-79-6 2,4,6-Tribromophenol 68%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:B4/2-4
Lab Sample ID:F81928-8 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:82.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 64%40-105%
321-60-8 2-Fluorobiphenyl 67%43-107%
1718-51-0 Terphenyl-d14 76%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B4/2-4
Lab Sample ID:F81928-8 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C Percent Solids:82.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060050.D 1 05/06/11 AH n/a n/a GQR2610
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.73 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 6.3 3.2 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 77%56-136%
98-08-8 aaa-Trifluorotoluene 75%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B4/2-4
Lab Sample ID:F81928-8 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8082A SW846 3550C Percent Solids:82.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 XX055991.D 1 05/03/11 NJ 05/02/11 OP36984 GXX864
Run #2
Initial Weight Final Volume
Run #1 29.9 g 10.0 ml
Run #2
PCB List
CAS No.Compound Result RL MDL Units Q
12674-11-2 Aroclor 1016 ND 20 8.1 ug/kg
11104-28-2 Aroclor 1221 ND 20 10 ug/kg
11141-16-5 Aroclor 1232 ND 20 10 ug/kg
53469-21-9 Aroclor 1242 ND 20 8.1 ug/kg
12672-29-6 Aroclor 1248 ND 20 8.1 ug/kg
11097-69-1 Aroclor 1254 ND 20 8.1 ug/kg
11096-82-5 Aroclor 1260 ND 20 8.1 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 91%44-126%
2051-24-3 Decachlorobiphenyl 100%39-157%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B4/2-4
Lab Sample ID:F81928-8 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C SW846 3550C Percent Solids:82.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40276.D 1 05/03/11 SJL 05/02/11 OP36981 GZF1661
Run #2
Initial Weight Final Volume
Run #1 29.6 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 10 4.1 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 79%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest LabLink@128733 10:24 16-Feb-2012
Report of Analysis Page 1 of 1
Client Sample ID:B4/2-4
Lab Sample ID:F81928-8 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Percent Solids:82.5
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <1.5 1.5 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Arsenic a 1.4 0.77 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Barium 45.8 7.7 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Beryllium 0.23 0.19 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Cadmium a <0.31 0.31 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Chromium a 72.2 0.77 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Copper a 22.1 1.9 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Lead a 13.1 1.5 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Mercury <0.10 0.10 mg/kg 1 05/09/11 05/09/11 LM SW846 7471B 3 SW846 7471B 5
Molybdenum a <3.9 3.9 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Nickel a 5.3 3.1 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Selenium a 1.7 1.5 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Silver a <0.77 0.77 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Tin <1.9 1.9 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Zinc a 13.5 1.5 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
(1) Instrument QC Batch: MA8921
(2) Instrument QC Batch: MA8926
(3) Instrument QC Batch: MA8930
(4) Prep QC Batch: MP20489
(5) Prep QC Batch: MP20527
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Report of Analysis Page 1 of 2
Client Sample ID:B4/10-12
Lab Sample ID:F81928-9 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:78.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F049466.D 1 05/10/11 CW n/a n/a VF1489
Run #2
Initial Weight
Run #1 5.83 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 54 22 ug/kg
71-43-2 Benzene ND 5.4 1.6 ug/kg
75-27-4 Bromodichloromethane ND 5.4 1.2 ug/kg
75-25-2 Bromoform ND 5.4 1.6 ug/kg
108-90-7 Chlorobenzene ND 5.4 1.1 ug/kg
75-00-3 Chloroethane ND 5.4 2.2 ug/kg
67-66-3 Chloroform ND 5.4 1.3 ug/kg
75-15-0 Carbon disulfide ND 5.4 2.2 ug/kg
56-23-5 Carbon tetrachloride ND 5.4 2.0 ug/kg
75-34-3 1,1-Dichloroethane ND 5.4 1.2 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.4 1.5 ug/kg
107-06-2 1,2-Dichloroethane ND 5.4 1.1 ug/kg
78-87-5 1,2-Dichloropropane ND 5.4 1.3 ug/kg
124-48-1 Dibromochloromethane ND 5.4 1.1 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.4 1.6 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.4 1.1 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.4 1.6 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.4 1.2 ug/kg
100-41-4 Ethylbenzene ND 5.4 1.1 ug/kg
591-78-6 2-Hexanone ND 27 5.9 ug/kg
108-10-1 4-Methyl-2-pentanone ND 27 6.0 ug/kg
74-83-9 Methyl bromide ND 5.4 2.2 ug/kg
74-87-3 Methyl chloride ND 5.4 2.2 ug/kg
75-09-2 Methylene chloride ND 11 5.0 ug/kg
78-93-3 Methyl ethyl ketone ND 27 6.6 ug/kg
100-42-5 Styrene ND 5.4 2.8 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.4 1.2 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.4 1.3 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.4 1.2 ug/kg
127-18-4 Tetrachloroethylene ND 5.4 1.1 ug/kg
108-88-3 Toluene ND 5.4 1.3 ug/kg
79-01-6 Trichloroethylene ND 5.4 1.3 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B4/10-12
Lab Sample ID:F81928-9 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:78.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 5.4 1.6 ug/kg
1330-20-7 Xylene (total)ND 16 3.5 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%80-121%
2037-26-5 Toluene-D8 97%71-130%
460-00-4 4-Bromofluorobenzene 101%59-148%
17060-07-0 1,2-Dichloroethane-D4 106%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B4/10-12
Lab Sample ID:F81928-9 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:78.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025257.D 1 05/05/11 MG 05/03/11 OP36999 SU1213
Run #2
Initial Weight Final Volume
Run #1 30.2 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1000 370 ug/kg
95-57-8 2-Chlorophenol ND 210 21 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 210 21 ug/kg
120-83-2 2,4-Dichlorophenol ND 210 21 ug/kg
105-67-9 2,4-Dimethylphenol ND 210 26 ug/kg
51-28-5 2,4-Dinitrophenol ND 1000 420 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 420 84 ug/kg
95-48-7 2-Methylphenol ND 210 21 ug/kg
3&4-Methylphenol ND 210 30 ug/kg
88-75-5 2-Nitrophenol ND 210 21 ug/kg
100-02-7 4-Nitrophenol ND 1000 170 ug/kg
87-86-5 Pentachlorophenol ND 1000 250 ug/kg
108-95-2 Phenol ND 210 21 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 210 21 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 210 21 ug/kg
83-32-9 Acenaphthene ND 210 21 ug/kg
208-96-8 Acenaphthylene ND 210 21 ug/kg
120-12-7 Anthracene ND 210 21 ug/kg
56-55-3 Benzo(a)anthracene ND 210 21 ug/kg
50-32-8 Benzo(a)pyrene ND 210 21 ug/kg
205-99-2 Benzo(b)fluoranthene ND 210 21 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 210 21 ug/kg
207-08-9 Benzo(k)fluoranthene ND 210 21 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 210 21 ug/kg
85-68-7 Butyl benzyl phthalate ND 210 42 ug/kg
100-51-6 Benzyl Alcohol ND 210 42 ug/kg
91-58-7 2-Chloronaphthalene ND 210 42 ug/kg
106-47-8 4-Chloroaniline ND 210 21 ug/kg
86-74-8 Carbazole ND 210 21 ug/kg
218-01-9 Chrysene ND 210 21 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 210 21 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 210 21 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B4/10-12
Lab Sample ID:F81928-9 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:78.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 210 21 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 210 21 ug/kg
95-50-1 1,2-Dichlorobenzene ND 210 42 ug/kg
541-73-1 1,3-Dichlorobenzene ND 210 42 ug/kg
106-46-7 1,4-Dichlorobenzene ND 210 42 ug/kg
121-14-2 2,4-Dinitrotoluene ND 210 21 ug/kg
606-20-2 2,6-Dinitrotoluene ND 210 25 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 420 42 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 210 21 ug/kg
132-64-9 Dibenzofuran ND 210 21 ug/kg
84-74-2 Di-n-butyl phthalate ND 420 84 ug/kg
117-84-0 Di-n-octyl phthalate ND 210 42 ug/kg
84-66-2 Diethyl phthalate ND 420 84 ug/kg
131-11-3 Dimethyl phthalate ND 210 42 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 420 84 ug/kg
206-44-0 Fluoranthene ND 210 21 ug/kg
86-73-7 Fluorene ND 210 21 ug/kg
118-74-1 Hexachlorobenzene ND 210 21 ug/kg
87-68-3 Hexachlorobutadiene ND 210 42 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 210 92 ug/kg
67-72-1 Hexachloroethane ND 210 42 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 210 21 ug/kg
78-59-1 Isophorone ND 210 21 ug/kg
91-57-6 2-Methylnaphthalene ND 210 21 ug/kg
88-74-4 2-Nitroaniline ND 210 42 ug/kg
99-09-2 3-Nitroaniline ND 210 42 ug/kg
100-01-6 4-Nitroaniline ND 210 42 ug/kg
91-20-3 Naphthalene ND 210 34 ug/kg
98-95-3 Nitrobenzene ND 210 21 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 210 21 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 210 21 ug/kg
85-01-8 Phenanthrene ND 210 21 ug/kg
129-00-0 Pyrene ND 210 21 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 210 21 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 58%40-102%
4165-62-2 Phenol-d5 66%41-100%
118-79-6 2,4,6-Tribromophenol 61%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B4/10-12
Lab Sample ID:F81928-9 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:78.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 60%40-105%
321-60-8 2-Fluorobiphenyl 60%43-107%
1718-51-0 Terphenyl-d14 74%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B4/10-12
Lab Sample ID:F81928-9 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C Percent Solids:78.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060053.D 1 05/06/11 AH n/a n/a GQR2610
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.53 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 7.1 3.5 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 77%56-136%
98-08-8 aaa-Trifluorotoluene 74%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B4/10-12
Lab Sample ID:F81928-9 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C SW846 3550C Percent Solids:78.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40277.D 1 05/03/11 SJL 05/02/11 OP36981 GZF1661
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 11 4.2 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 73%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B4/10-12
Lab Sample ID:F81928-9 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Percent Solids:78.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <6.2 6.2 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Arsenic a <3.1 3.1 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Barium a 299 62 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Beryllium a <1.6 1.6 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Cadmium a <1.2 1.2 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Chromium a 19.4 3.1 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Copper a 181 7.8 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Lead 5.3 1.2 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Mercury <0.097 0.097 mg/kg 1 05/09/11 05/09/11 LM SW846 7471B 3 SW846 7471B 5
Molybdenum a <16 16 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Nickel a 15.6 12 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Selenium a <6.2 6.2 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Silver a <3.1 3.1 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Tin a <16 16 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Zinc a 68.0 6.2 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
(1) Instrument QC Batch: MA8921
(2) Instrument QC Batch: MA8926
(3) Instrument QC Batch: MA8930
(4) Prep QC Batch: MP20489
(5) Prep QC Batch: MP20527
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Client Sample ID:B5/2-4
Lab Sample ID:F81928-10 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:83.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F049467.D 1 05/10/11 CW n/a n/a VF1489
Run #2
Initial Weight
Run #1 6.16 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 49 19 ug/kg
71-43-2 Benzene ND 4.9 1.5 ug/kg
75-27-4 Bromodichloromethane ND 4.9 1.1 ug/kg
75-25-2 Bromoform ND 4.9 1.5 ug/kg
108-90-7 Chlorobenzene ND 4.9 0.97 ug/kg
75-00-3 Chloroethane ND 4.9 1.9 ug/kg
67-66-3 Chloroform ND 4.9 1.2 ug/kg
75-15-0 Carbon disulfide ND 4.9 1.9 ug/kg
56-23-5 Carbon tetrachloride ND 4.9 1.7 ug/kg
75-34-3 1,1-Dichloroethane ND 4.9 1.1 ug/kg
75-35-4 1,1-Dichloroethylene ND 4.9 1.4 ug/kg
107-06-2 1,2-Dichloroethane ND 4.9 0.97 ug/kg
78-87-5 1,2-Dichloropropane ND 4.9 1.2 ug/kg
124-48-1 Dibromochloromethane ND 4.9 0.97 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 4.9 1.5 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 4.9 0.97 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 4.9 1.5 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 4.9 1.1 ug/kg
100-41-4 Ethylbenzene ND 4.9 0.97 ug/kg
591-78-6 2-Hexanone ND 24 5.2 ug/kg
108-10-1 4-Methyl-2-pentanone ND 24 5.3 ug/kg
74-83-9 Methyl bromide ND 4.9 1.9 ug/kg
74-87-3 Methyl chloride ND 4.9 1.9 ug/kg
75-09-2 Methylene chloride ND 9.7 4.5 ug/kg
78-93-3 Methyl ethyl ketone ND 24 5.9 ug/kg
100-42-5 Styrene ND 4.9 2.5 ug/kg
71-55-6 1,1,1-Trichloroethane ND 4.9 1.1 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 4.9 1.2 ug/kg
79-00-5 1,1,2-Trichloroethane ND 4.9 1.1 ug/kg
127-18-4 Tetrachloroethylene ND 4.9 0.97 ug/kg
108-88-3 Toluene ND 4.9 1.2 ug/kg
79-01-6 Trichloroethylene ND 4.9 1.2 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B5/2-4
Lab Sample ID:F81928-10 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:83.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 4.9 1.5 ug/kg
1330-20-7 Xylene (total)ND 15 3.1 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%80-121%
2037-26-5 Toluene-D8 98%71-130%
460-00-4 4-Bromofluorobenzene 104%59-148%
17060-07-0 1,2-Dichloroethane-D4 106%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B5/2-4
Lab Sample ID:F81928-10 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:83.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025258.D 1 05/05/11 MG 05/03/11 OP36999 SU1213
Run #2
Initial Weight Final Volume
Run #1 29.8 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1000 350 ug/kg
95-57-8 2-Chlorophenol ND 200 20 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 200 20 ug/kg
120-83-2 2,4-Dichlorophenol ND 200 20 ug/kg
105-67-9 2,4-Dimethylphenol ND 200 25 ug/kg
51-28-5 2,4-Dinitrophenol ND 1000 400 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 400 80 ug/kg
95-48-7 2-Methylphenol ND 200 20 ug/kg
3&4-Methylphenol ND 200 29 ug/kg
88-75-5 2-Nitrophenol ND 200 20 ug/kg
100-02-7 4-Nitrophenol ND 1000 160 ug/kg
87-86-5 Pentachlorophenol ND 1000 240 ug/kg
108-95-2 Phenol ND 200 20 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 200 20 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 200 20 ug/kg
83-32-9 Acenaphthene ND 200 20 ug/kg
208-96-8 Acenaphthylene ND 200 20 ug/kg
120-12-7 Anthracene ND 200 20 ug/kg
56-55-3 Benzo(a)anthracene ND 200 20 ug/kg
50-32-8 Benzo(a)pyrene ND 200 20 ug/kg
205-99-2 Benzo(b)fluoranthene ND 200 20 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 200 20 ug/kg
207-08-9 Benzo(k)fluoranthene ND 200 20 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 200 20 ug/kg
85-68-7 Butyl benzyl phthalate ND 200 40 ug/kg
100-51-6 Benzyl Alcohol ND 200 40 ug/kg
91-58-7 2-Chloronaphthalene ND 200 40 ug/kg
106-47-8 4-Chloroaniline ND 200 20 ug/kg
86-74-8 Carbazole ND 200 20 ug/kg
218-01-9 Chrysene ND 200 20 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 200 20 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 200 20 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:B5/2-4
Lab Sample ID:F81928-10 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:83.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 200 20 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 200 20 ug/kg
95-50-1 1,2-Dichlorobenzene ND 200 40 ug/kg
541-73-1 1,3-Dichlorobenzene ND 200 40 ug/kg
106-46-7 1,4-Dichlorobenzene ND 200 40 ug/kg
121-14-2 2,4-Dinitrotoluene ND 200 20 ug/kg
606-20-2 2,6-Dinitrotoluene ND 200 24 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 400 40 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 200 20 ug/kg
132-64-9 Dibenzofuran ND 200 20 ug/kg
84-74-2 Di-n-butyl phthalate ND 400 80 ug/kg
117-84-0 Di-n-octyl phthalate ND 200 40 ug/kg
84-66-2 Diethyl phthalate ND 400 80 ug/kg
131-11-3 Dimethyl phthalate ND 200 40 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 400 80 ug/kg
206-44-0 Fluoranthene ND 200 20 ug/kg
86-73-7 Fluorene ND 200 20 ug/kg
118-74-1 Hexachlorobenzene ND 200 20 ug/kg
87-68-3 Hexachlorobutadiene ND 200 40 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 200 88 ug/kg
67-72-1 Hexachloroethane ND 200 40 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 200 20 ug/kg
78-59-1 Isophorone ND 200 20 ug/kg
91-57-6 2-Methylnaphthalene ND 200 20 ug/kg
88-74-4 2-Nitroaniline ND 200 40 ug/kg
99-09-2 3-Nitroaniline ND 200 40 ug/kg
100-01-6 4-Nitroaniline ND 200 40 ug/kg
91-20-3 Naphthalene ND 200 32 ug/kg
98-95-3 Nitrobenzene ND 200 20 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 200 20 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 200 20 ug/kg
85-01-8 Phenanthrene ND 200 20 ug/kg
129-00-0 Pyrene ND 200 20 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 200 20 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 60%40-102%
4165-62-2 Phenol-d5 70%41-100%
118-79-6 2,4,6-Tribromophenol 66%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:B5/2-4
Lab Sample ID:F81928-10 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:83.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 67%40-105%
321-60-8 2-Fluorobiphenyl 66%43-107%
1718-51-0 Terphenyl-d14 74%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B5/2-4
Lab Sample ID:F81928-10 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C Percent Solids:83.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060054.D 1 05/06/11 AH n/a n/a GQR2610
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 4.80 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 7.2 3.6 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 72%56-136%
98-08-8 aaa-Trifluorotoluene 70%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B5/2-4
Lab Sample ID:F81928-10 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8082A SW846 3550C Percent Solids:83.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 XX055992.D 1 05/03/11 NJ 05/02/11 OP36984 GXX864
Run #2
Initial Weight Final Volume
Run #1 29.9 g 10.0 ml
Run #2
PCB List
CAS No.Compound Result RL MDL Units Q
12674-11-2 Aroclor 1016 ND 20 8.0 ug/kg
11104-28-2 Aroclor 1221 ND 20 10 ug/kg
11141-16-5 Aroclor 1232 ND 20 10 ug/kg
53469-21-9 Aroclor 1242 ND 20 8.0 ug/kg
12672-29-6 Aroclor 1248 ND 20 8.0 ug/kg
11097-69-1 Aroclor 1254 ND 20 8.0 ug/kg
11096-82-5 Aroclor 1260 ND 20 8.0 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 76%44-126%
2051-24-3 Decachlorobiphenyl 84%39-157%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B5/2-4
Lab Sample ID:F81928-10 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C SW846 3550C Percent Solids:83.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40278.D 1 05/03/11 SJL 05/02/11 OP36981 GZF1661
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 10 4.0 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 79%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B5/2-4
Lab Sample ID:F81928-10 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Percent Solids:83.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <1.8 1.8 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Arsenic a 1.4 0.91 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Barium 18.2 9.1 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Beryllium <0.23 0.23 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Cadmium a <0.37 0.37 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Chromium a 66.7 0.91 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Copper a 23.0 2.3 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Lead a 12.4 1.8 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Mercury <0.091 0.091 mg/kg 1 05/09/11 05/09/11 LM SW846 7471B 3 SW846 7471B 5
Molybdenum a <4.6 4.6 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Nickel a 5.3 3.7 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Selenium a 1.9 1.8 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Silver a <0.91 0.91 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Tin <2.3 2.3 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Zinc a 15.9 1.8 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
(1) Instrument QC Batch: MA8921
(2) Instrument QC Batch: MA8926
(3) Instrument QC Batch: MA8930
(4) Prep QC Batch: MP20489
(5) Prep QC Batch: MP20527
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Report of Analysis Page 1 of 2
Client Sample ID:B5/10-12
Lab Sample ID:F81928-11 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:80.8
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F049468.D 1 05/10/11 CW n/a n/a VF1489
Run #2
Initial Weight
Run #1 6.20 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 50 20 ug/kg
71-43-2 Benzene ND 5.0 1.5 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.1 ug/kg
75-25-2 Bromoform ND 5.0 1.5 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.2 ug/kg
75-15-0 Carbon disulfide ND 5.0 2.0 ug/kg
56-23-5 Carbon tetrachloride ND 5.0 1.8 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.1 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.4 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.2 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.5 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.5 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.1 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg
591-78-6 2-Hexanone ND 25 5.4 ug/kg
108-10-1 4-Methyl-2-pentanone ND 25 5.5 ug/kg
74-83-9 Methyl bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl chloride ND 5.0 2.0 ug/kg
75-09-2 Methylene chloride ND 10 4.6 ug/kg
78-93-3 Methyl ethyl ketone ND 25 6.1 ug/kg
100-42-5 Styrene ND 5.0 2.6 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.1 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.2 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.1 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.0 ug/kg
108-88-3 Toluene ND 5.0 1.2 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.2 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:B5/10-12
Lab Sample ID:F81928-11 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:80.8
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 5.0 1.5 ug/kg
1330-20-7 Xylene (total)ND 15 3.2 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%80-121%
2037-26-5 Toluene-D8 98%71-130%
460-00-4 4-Bromofluorobenzene 103%59-148%
17060-07-0 1,2-Dichloroethane-D4 114%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:B5/10-12
Lab Sample ID:F81928-11 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:80.8
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025259.D 1 05/05/11 MG 05/03/11 OP36999 SU1213
Run #2
Initial Weight Final Volume
Run #1 30.3 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1000 360 ug/kg
95-57-8 2-Chlorophenol ND 200 20 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 200 20 ug/kg
120-83-2 2,4-Dichlorophenol ND 200 20 ug/kg
105-67-9 2,4-Dimethylphenol ND 200 26 ug/kg
51-28-5 2,4-Dinitrophenol ND 1000 410 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 410 82 ug/kg
95-48-7 2-Methylphenol ND 200 20 ug/kg
3&4-Methylphenol ND 200 29 ug/kg
88-75-5 2-Nitrophenol ND 200 20 ug/kg
100-02-7 4-Nitrophenol ND 1000 160 ug/kg
87-86-5 Pentachlorophenol ND 1000 250 ug/kg
108-95-2 Phenol ND 200 20 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 200 20 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 200 20 ug/kg
83-32-9 Acenaphthene ND 200 20 ug/kg
208-96-8 Acenaphthylene ND 200 20 ug/kg
120-12-7 Anthracene ND 200 20 ug/kg
56-55-3 Benzo(a)anthracene ND 200 20 ug/kg
50-32-8 Benzo(a)pyrene ND 200 20 ug/kg
205-99-2 Benzo(b)fluoranthene ND 200 20 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 200 20 ug/kg
207-08-9 Benzo(k)fluoranthene ND 200 20 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 200 20 ug/kg
85-68-7 Butyl benzyl phthalate ND 200 41 ug/kg
100-51-6 Benzyl Alcohol ND 200 41 ug/kg
91-58-7 2-Chloronaphthalene ND 200 41 ug/kg
106-47-8 4-Chloroaniline ND 200 20 ug/kg
86-74-8 Carbazole ND 200 20 ug/kg
218-01-9 Chrysene ND 200 20 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 200 20 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 200 20 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:B5/10-12
Lab Sample ID:F81928-11 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:80.8
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 200 20 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 200 20 ug/kg
95-50-1 1,2-Dichlorobenzene ND 200 41 ug/kg
541-73-1 1,3-Dichlorobenzene ND 200 41 ug/kg
106-46-7 1,4-Dichlorobenzene ND 200 41 ug/kg
121-14-2 2,4-Dinitrotoluene ND 200 20 ug/kg
606-20-2 2,6-Dinitrotoluene ND 200 24 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 410 41 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 200 20 ug/kg
132-64-9 Dibenzofuran ND 200 20 ug/kg
84-74-2 Di-n-butyl phthalate ND 410 82 ug/kg
117-84-0 Di-n-octyl phthalate ND 200 41 ug/kg
84-66-2 Diethyl phthalate ND 410 82 ug/kg
131-11-3 Dimethyl phthalate ND 200 41 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 410 82 ug/kg
206-44-0 Fluoranthene ND 200 20 ug/kg
86-73-7 Fluorene ND 200 20 ug/kg
118-74-1 Hexachlorobenzene ND 200 20 ug/kg
87-68-3 Hexachlorobutadiene ND 200 41 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 200 90 ug/kg
67-72-1 Hexachloroethane ND 200 41 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 200 20 ug/kg
78-59-1 Isophorone ND 200 20 ug/kg
91-57-6 2-Methylnaphthalene ND 200 20 ug/kg
88-74-4 2-Nitroaniline ND 200 41 ug/kg
99-09-2 3-Nitroaniline ND 200 41 ug/kg
100-01-6 4-Nitroaniline ND 200 41 ug/kg
91-20-3 Naphthalene ND 200 33 ug/kg
98-95-3 Nitrobenzene ND 200 20 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 200 20 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 200 20 ug/kg
85-01-8 Phenanthrene ND 200 20 ug/kg
129-00-0 Pyrene ND 200 20 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 200 20 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 69%40-102%
4165-62-2 Phenol-d5 76%41-100%
118-79-6 2,4,6-Tribromophenol 75%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:B5/10-12
Lab Sample ID:F81928-11 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:80.8
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 71%40-105%
321-60-8 2-Fluorobiphenyl 71%43-107%
1718-51-0 Terphenyl-d14 77%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest LabLink@128733 10:24 16-Feb-2012
Report of Analysis Page 1 of 1
Client Sample ID:B5/10-12
Lab Sample ID:F81928-11 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C Percent Solids:80.8
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060055.D 1 05/06/11 AH n/a n/a GQR2610
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.85 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 6.5 3.2 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 79%56-136%
98-08-8 aaa-Trifluorotoluene 76%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Accutest LabLink@128733 10:24 16-Feb-2012
Report of Analysis Page 1 of 1
Client Sample ID:B5/10-12
Lab Sample ID:F81928-11 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C SW846 3550C Percent Solids:80.8
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40282.D 1 05/03/11 SJL 05/02/11 OP36981 GZF1661
Run #2
Initial Weight Final Volume
Run #1 30.2 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 10 4.1 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 80%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B5/10-12
Lab Sample ID:F81928-11 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Percent Solids:80.8
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <5.8 5.8 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Arsenic a <2.9 2.9 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Barium a 242 58 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Beryllium a <1.5 1.5 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Cadmium a <1.2 1.2 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Chromium a 18.0 2.9 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Copper a 54.2 7.3 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Lead 5.5 1.2 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Mercury <0.097 0.097 mg/kg 1 05/09/11 05/09/11 LM SW846 7471B 3 SW846 7471B 5
Molybdenum a <15 15 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Nickel a <12 12 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Selenium a <5.8 5.8 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Silver a <2.9 2.9 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Tin a <15 15 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Zinc a 48.4 5.8 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
(1) Instrument QC Batch: MA8921
(2) Instrument QC Batch: MA8926
(3) Instrument QC Batch: MA8930
(4) Prep QC Batch: MP20489
(5) Prep QC Batch: MP20527
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Report of Analysis Page 1 of 2
Client Sample ID:B3/0.5-2
Lab Sample ID:F81928-12 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:77.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F049469.D 1 05/10/11 CW n/a n/a VF1489
Run #2
Initial Weight
Run #1 5.48 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 59 24 ug/kg
71-43-2 Benzene ND 5.9 1.8 ug/kg
75-27-4 Bromodichloromethane ND 5.9 1.3 ug/kg
75-25-2 Bromoform ND 5.9 1.8 ug/kg
108-90-7 Chlorobenzene ND 5.9 1.2 ug/kg
75-00-3 Chloroethane ND 5.9 2.4 ug/kg
67-66-3 Chloroform ND 5.9 1.4 ug/kg
75-15-0 Carbon disulfide ND 5.9 2.4 ug/kg
56-23-5 Carbon tetrachloride ND 5.9 2.1 ug/kg
75-34-3 1,1-Dichloroethane ND 5.9 1.3 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.9 1.7 ug/kg
107-06-2 1,2-Dichloroethane ND 5.9 1.2 ug/kg
78-87-5 1,2-Dichloropropane ND 5.9 1.4 ug/kg
124-48-1 Dibromochloromethane ND 5.9 1.2 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.9 1.8 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.9 1.2 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.9 1.8 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.9 1.3 ug/kg
100-41-4 Ethylbenzene ND 5.9 1.2 ug/kg
591-78-6 2-Hexanone ND 30 6.4 ug/kg
108-10-1 4-Methyl-2-pentanone ND 30 6.5 ug/kg
74-83-9 Methyl bromide ND 5.9 2.4 ug/kg
74-87-3 Methyl chloride ND 5.9 2.4 ug/kg
75-09-2 Methylene chloride ND 12 5.4 ug/kg
78-93-3 Methyl ethyl ketone ND 30 7.2 ug/kg
100-42-5 Styrene ND 5.9 3.1 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.9 1.3 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.9 1.4 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.9 1.3 ug/kg
127-18-4 Tetrachloroethylene ND 5.9 1.2 ug/kg
108-88-3 Toluene ND 5.9 1.4 ug/kg
79-01-6 Trichloroethylene ND 5.9 1.4 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:B3/0.5-2
Lab Sample ID:F81928-12 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:77.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 5.9 1.8 ug/kg
1330-20-7 Xylene (total)ND 18 3.8 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%80-121%
2037-26-5 Toluene-D8 99%71-130%
460-00-4 4-Bromofluorobenzene 101%59-148%
17060-07-0 1,2-Dichloroethane-D4 106%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B3/0.5-2
Lab Sample ID:F81928-12 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:77.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025260.D 1 05/05/11 MG 05/03/11 OP36999 SU1213
Run #2
Initial Weight Final Volume
Run #1 30.3 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1100 380 ug/kg
95-57-8 2-Chlorophenol ND 210 21 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 210 21 ug/kg
120-83-2 2,4-Dichlorophenol ND 210 21 ug/kg
105-67-9 2,4-Dimethylphenol ND 210 27 ug/kg
51-28-5 2,4-Dinitrophenol ND 1100 430 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 430 86 ug/kg
95-48-7 2-Methylphenol ND 210 21 ug/kg
3&4-Methylphenol ND 210 31 ug/kg
88-75-5 2-Nitrophenol ND 210 21 ug/kg
100-02-7 4-Nitrophenol ND 1100 170 ug/kg
87-86-5 Pentachlorophenol ND 1100 260 ug/kg
108-95-2 Phenol ND 210 21 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 210 21 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 210 21 ug/kg
83-32-9 Acenaphthene ND 210 21 ug/kg
208-96-8 Acenaphthylene ND 210 21 ug/kg
120-12-7 Anthracene ND 210 21 ug/kg
56-55-3 Benzo(a)anthracene ND 210 21 ug/kg
50-32-8 Benzo(a)pyrene ND 210 21 ug/kg
205-99-2 Benzo(b)fluoranthene ND 210 21 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 210 21 ug/kg
207-08-9 Benzo(k)fluoranthene ND 210 21 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 210 21 ug/kg
85-68-7 Butyl benzyl phthalate ND 210 43 ug/kg
100-51-6 Benzyl Alcohol ND 210 43 ug/kg
91-58-7 2-Chloronaphthalene ND 210 43 ug/kg
106-47-8 4-Chloroaniline ND 210 21 ug/kg
86-74-8 Carbazole ND 210 21 ug/kg
218-01-9 Chrysene ND 210 21 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 210 21 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 210 21 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:B3/0.5-2
Lab Sample ID:F81928-12 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:77.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 210 21 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 210 21 ug/kg
95-50-1 1,2-Dichlorobenzene ND 210 43 ug/kg
541-73-1 1,3-Dichlorobenzene ND 210 43 ug/kg
106-46-7 1,4-Dichlorobenzene ND 210 43 ug/kg
121-14-2 2,4-Dinitrotoluene ND 210 21 ug/kg
606-20-2 2,6-Dinitrotoluene ND 210 25 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 430 43 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 210 21 ug/kg
132-64-9 Dibenzofuran ND 210 21 ug/kg
84-74-2 Di-n-butyl phthalate ND 430 86 ug/kg
117-84-0 Di-n-octyl phthalate ND 210 43 ug/kg
84-66-2 Diethyl phthalate ND 430 86 ug/kg
131-11-3 Dimethyl phthalate ND 210 43 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 430 86 ug/kg
206-44-0 Fluoranthene ND 210 21 ug/kg
86-73-7 Fluorene ND 210 21 ug/kg
118-74-1 Hexachlorobenzene ND 210 21 ug/kg
87-68-3 Hexachlorobutadiene ND 210 43 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 210 94 ug/kg
67-72-1 Hexachloroethane ND 210 43 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 210 21 ug/kg
78-59-1 Isophorone ND 210 21 ug/kg
91-57-6 2-Methylnaphthalene ND 210 21 ug/kg
88-74-4 2-Nitroaniline ND 210 43 ug/kg
99-09-2 3-Nitroaniline ND 210 43 ug/kg
100-01-6 4-Nitroaniline ND 210 43 ug/kg
91-20-3 Naphthalene ND 210 34 ug/kg
98-95-3 Nitrobenzene ND 210 21 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 210 21 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 210 21 ug/kg
85-01-8 Phenanthrene ND 210 21 ug/kg
129-00-0 Pyrene ND 210 21 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 210 21 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 69%40-102%
4165-62-2 Phenol-d5 77%41-100%
118-79-6 2,4,6-Tribromophenol 73%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:B3/0.5-2
Lab Sample ID:F81928-12 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:77.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 72%40-105%
321-60-8 2-Fluorobiphenyl 73%43-107%
1718-51-0 Terphenyl-d14 80%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B3/0.5-2
Lab Sample ID:F81928-12 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C Percent Solids:77.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060056.D 1 05/06/11 AH n/a n/a GQR2610
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.34 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 7.6 3.8 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 77%56-136%
98-08-8 aaa-Trifluorotoluene 75%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B3/0.5-2
Lab Sample ID:F81928-12 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8082A SW846 3550C Percent Solids:77.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 XX055993.D 1 05/03/11 NJ 05/02/11 OP36984 GXX864
Run #2
Initial Weight Final Volume
Run #1 29.9 g 10.0 ml
Run #2
PCB List
CAS No.Compound Result RL MDL Units Q
12674-11-2 Aroclor 1016 ND 22 8.7 ug/kg
11104-28-2 Aroclor 1221 ND 22 11 ug/kg
11141-16-5 Aroclor 1232 ND 22 11 ug/kg
53469-21-9 Aroclor 1242 ND 22 8.7 ug/kg
12672-29-6 Aroclor 1248 ND 22 8.7 ug/kg
11097-69-1 Aroclor 1254 ND 22 8.7 ug/kg
11096-82-5 Aroclor 1260 ND 22 8.7 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 68%44-126%
2051-24-3 Decachlorobiphenyl 78%39-157%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B3/0.5-2
Lab Sample ID:F81928-12 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C SW846 3550C Percent Solids:77.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40283.D 1 05/03/11 SJL 05/02/11 OP36981 GZF1661
Run #2
Initial Weight Final Volume
Run #1 30.1 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 11 4.3 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 75%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B3/0.5-2
Lab Sample ID:F81928-12 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Percent Solids:77.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <2.1 2.1 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Arsenic a 1.3 1.1 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Barium 18.1 11 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Beryllium <0.27 0.27 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Cadmium a <0.43 0.43 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Chromium a 28.8 1.1 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Copper a 40.6 2.7 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Lead a 14.9 2.1 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Mercury <0.11 0.11 mg/kg 1 05/09/11 05/09/11 LM SW846 7471B 3 SW846 7471B 5
Molybdenum a <5.3 5.3 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Nickel a <4.3 4.3 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Selenium a 2.9 2.1 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Silver a <1.1 1.1 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Tin <2.7 2.7 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Zinc a 9.4 2.1 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
(1) Instrument QC Batch: MA8921
(2) Instrument QC Batch: MA8926
(3) Instrument QC Batch: MA8930
(4) Prep QC Batch: MP20489
(5) Prep QC Batch: MP20527
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Client Sample ID:B3/10-12
Lab Sample ID:F81928-13 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:71.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F049446.D 1 05/09/11 CW n/a n/a VF1488
Run #2
Initial Weight
Run #1 5.18 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 68 27 ug/kg
71-43-2 Benzene ND 6.8 2.0 ug/kg
75-27-4 Bromodichloromethane ND 6.8 1.5 ug/kg
75-25-2 Bromoform ND 6.8 2.0 ug/kg
108-90-7 Chlorobenzene ND 6.8 1.4 ug/kg
75-00-3 Chloroethane ND 6.8 2.7 ug/kg
67-66-3 Chloroform ND 6.8 1.6 ug/kg
75-15-0 Carbon disulfide ND 6.8 2.7 ug/kg
56-23-5 Carbon tetrachloride ND 6.8 2.4 ug/kg
75-34-3 1,1-Dichloroethane ND 6.8 1.5 ug/kg
75-35-4 1,1-Dichloroethylene ND 6.8 1.9 ug/kg
107-06-2 1,2-Dichloroethane ND 6.8 1.4 ug/kg
78-87-5 1,2-Dichloropropane ND 6.8 1.6 ug/kg
124-48-1 Dibromochloromethane ND 6.8 1.4 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 6.8 2.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 6.8 1.4 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 6.8 2.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 6.8 1.5 ug/kg
100-41-4 Ethylbenzene ND 6.8 1.4 ug/kg
591-78-6 2-Hexanone ND 34 7.3 ug/kg
108-10-1 4-Methyl-2-pentanone ND 34 7.4 ug/kg
74-83-9 Methyl bromide ND 6.8 2.7 ug/kg
74-87-3 Methyl chloride ND 6.8 2.7 ug/kg
75-09-2 Methylene chloride ND 14 6.2 ug/kg
78-93-3 Methyl ethyl ketone ND 34 8.2 ug/kg
100-42-5 Styrene ND 6.8 3.5 ug/kg
71-55-6 1,1,1-Trichloroethane ND 6.8 1.5 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 6.8 1.6 ug/kg
79-00-5 1,1,2-Trichloroethane ND 6.8 1.5 ug/kg
127-18-4 Tetrachloroethylene ND 6.8 1.4 ug/kg
108-88-3 Toluene ND 6.8 1.6 ug/kg
79-01-6 Trichloroethylene ND 6.8 1.6 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B3/10-12
Lab Sample ID:F81928-13 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:71.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 6.8 2.0 ug/kg
1330-20-7 Xylene (total)ND 20 4.3 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 108%80-121%
2037-26-5 Toluene-D8 96%71-130%
460-00-4 4-Bromofluorobenzene 101%59-148%
17060-07-0 1,2-Dichloroethane-D4 116%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:B3/10-12
Lab Sample ID:F81928-13 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:71.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025261.D 1 05/05/11 MG 05/03/11 OP36999 SU1213
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1200 410 ug/kg
95-57-8 2-Chlorophenol ND 230 23 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 230 23 ug/kg
120-83-2 2,4-Dichlorophenol ND 230 23 ug/kg
105-67-9 2,4-Dimethylphenol ND 230 29 ug/kg
51-28-5 2,4-Dinitrophenol ND 1200 470 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 470 93 ug/kg
95-48-7 2-Methylphenol ND 230 23 ug/kg
3&4-Methylphenol ND 230 34 ug/kg
88-75-5 2-Nitrophenol ND 230 23 ug/kg
100-02-7 4-Nitrophenol ND 1200 190 ug/kg
87-86-5 Pentachlorophenol ND 1200 280 ug/kg
108-95-2 Phenol ND 230 23 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 230 23 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 230 23 ug/kg
83-32-9 Acenaphthene ND 230 23 ug/kg
208-96-8 Acenaphthylene ND 230 23 ug/kg
120-12-7 Anthracene ND 230 23 ug/kg
56-55-3 Benzo(a)anthracene ND 230 23 ug/kg
50-32-8 Benzo(a)pyrene ND 230 23 ug/kg
205-99-2 Benzo(b)fluoranthene ND 230 23 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 230 23 ug/kg
207-08-9 Benzo(k)fluoranthene ND 230 23 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 230 23 ug/kg
85-68-7 Butyl benzyl phthalate ND 230 47 ug/kg
100-51-6 Benzyl Alcohol ND 230 47 ug/kg
91-58-7 2-Chloronaphthalene ND 230 47 ug/kg
106-47-8 4-Chloroaniline ND 230 23 ug/kg
86-74-8 Carbazole ND 230 23 ug/kg
218-01-9 Chrysene ND 230 23 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 230 23 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 230 23 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:B3/10-12
Lab Sample ID:F81928-13 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:71.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 230 23 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 230 23 ug/kg
95-50-1 1,2-Dichlorobenzene ND 230 47 ug/kg
541-73-1 1,3-Dichlorobenzene ND 230 47 ug/kg
106-46-7 1,4-Dichlorobenzene ND 230 47 ug/kg
121-14-2 2,4-Dinitrotoluene ND 230 23 ug/kg
606-20-2 2,6-Dinitrotoluene ND 230 28 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 470 47 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 230 23 ug/kg
132-64-9 Dibenzofuran ND 230 23 ug/kg
84-74-2 Di-n-butyl phthalate ND 470 93 ug/kg
117-84-0 Di-n-octyl phthalate ND 230 47 ug/kg
84-66-2 Diethyl phthalate ND 470 93 ug/kg
131-11-3 Dimethyl phthalate ND 230 47 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 470 93 ug/kg
206-44-0 Fluoranthene ND 230 23 ug/kg
86-73-7 Fluorene ND 230 23 ug/kg
118-74-1 Hexachlorobenzene ND 230 23 ug/kg
87-68-3 Hexachlorobutadiene ND 230 47 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 230 100 ug/kg
67-72-1 Hexachloroethane ND 230 47 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 230 23 ug/kg
78-59-1 Isophorone ND 230 23 ug/kg
91-57-6 2-Methylnaphthalene ND 230 23 ug/kg
88-74-4 2-Nitroaniline ND 230 47 ug/kg
99-09-2 3-Nitroaniline ND 230 47 ug/kg
100-01-6 4-Nitroaniline ND 230 47 ug/kg
91-20-3 Naphthalene ND 230 37 ug/kg
98-95-3 Nitrobenzene ND 230 23 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 230 23 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 230 23 ug/kg
85-01-8 Phenanthrene ND 230 23 ug/kg
129-00-0 Pyrene ND 230 23 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 230 23 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 66%40-102%
4165-62-2 Phenol-d5 75%41-100%
118-79-6 2,4,6-Tribromophenol 70%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:B3/10-12
Lab Sample ID:F81928-13 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:71.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 69%40-105%
321-60-8 2-Fluorobiphenyl 70%43-107%
1718-51-0 Terphenyl-d14 72%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B3/10-12
Lab Sample ID:F81928-13 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C Percent Solids:71.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060057.D 1 05/06/11 AH n/a n/a GQR2610
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.47 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 8.4 4.2 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 74%56-136%
98-08-8 aaa-Trifluorotoluene 74%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B3/10-12
Lab Sample ID:F81928-13 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C SW846 3550C Percent Solids:71.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40284.D 1 05/03/11 SJL 05/02/11 OP36981 GZF1661
Run #2
Initial Weight Final Volume
Run #1 29.8 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 12 4.7 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 77%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B3/10-12
Lab Sample ID:F81928-13 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Percent Solids:71.4
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <5.1 5.1 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Arsenic a <2.6 2.6 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Barium a 113 51 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Beryllium a <1.3 1.3 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Cadmium a <1.0 1.0 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Chromium a 11.1 2.6 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Copper a 60.5 6.4 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Lead 5.5 1.0 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Mercury <0.11 0.11 mg/kg 1 05/09/11 05/09/11 LM SW846 7471B 3 SW846 7471B 5
Molybdenum a <13 13 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Nickel a <10 10 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Selenium a <5.1 5.1 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Silver a <2.6 2.6 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Tin a <13 13 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Zinc a 27.9 5.1 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
(1) Instrument QC Batch: MA8921
(2) Instrument QC Batch: MA8926
(3) Instrument QC Batch: MA8930
(4) Prep QC Batch: MP20489
(5) Prep QC Batch: MP20527
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Client Sample ID:B6/0.5-2
Lab Sample ID:F81928-14 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:87.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F049447.D 1 05/09/11 CW n/a n/a VF1488
Run #2
Initial Weight
Run #1 5.95 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 48 19 ug/kg
71-43-2 Benzene ND 4.8 1.4 ug/kg
75-27-4 Bromodichloromethane ND 4.8 1.1 ug/kg
75-25-2 Bromoform ND 4.8 1.4 ug/kg
108-90-7 Chlorobenzene ND 4.8 0.96 ug/kg
75-00-3 Chloroethane ND 4.8 1.9 ug/kg
67-66-3 Chloroform ND 4.8 1.2 ug/kg
75-15-0 Carbon disulfide ND 4.8 1.9 ug/kg
56-23-5 Carbon tetrachloride ND 4.8 1.7 ug/kg
75-34-3 1,1-Dichloroethane ND 4.8 1.1 ug/kg
75-35-4 1,1-Dichloroethylene ND 4.8 1.3 ug/kg
107-06-2 1,2-Dichloroethane ND 4.8 0.96 ug/kg
78-87-5 1,2-Dichloropropane ND 4.8 1.2 ug/kg
124-48-1 Dibromochloromethane ND 4.8 0.96 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 4.8 1.4 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 4.8 0.96 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 4.8 1.4 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 4.8 1.1 ug/kg
100-41-4 Ethylbenzene ND 4.8 0.96 ug/kg
591-78-6 2-Hexanone ND 24 5.2 ug/kg
108-10-1 4-Methyl-2-pentanone ND 24 5.3 ug/kg
74-83-9 Methyl bromide ND 4.8 1.9 ug/kg
74-87-3 Methyl chloride ND 4.8 1.9 ug/kg
75-09-2 Methylene chloride ND 9.6 4.4 ug/kg
78-93-3 Methyl ethyl ketone ND 24 5.9 ug/kg
100-42-5 Styrene ND 4.8 2.5 ug/kg
71-55-6 1,1,1-Trichloroethane ND 4.8 1.1 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 4.8 1.2 ug/kg
79-00-5 1,1,2-Trichloroethane ND 4.8 1.1 ug/kg
127-18-4 Tetrachloroethylene ND 4.8 0.96 ug/kg
108-88-3 Toluene ND 4.8 1.2 ug/kg
79-01-6 Trichloroethylene ND 4.8 1.2 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B6/0.5-2
Lab Sample ID:F81928-14 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:87.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 4.8 1.4 ug/kg
1330-20-7 Xylene (total)ND 14 3.1 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%80-121%
2037-26-5 Toluene-D8 98%71-130%
460-00-4 4-Bromofluorobenzene 100%59-148%
17060-07-0 1,2-Dichloroethane-D4 114%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:B6/0.5-2
Lab Sample ID:F81928-14 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:87.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025262.D 1 05/05/11 MG 05/03/11 OP36999 SU1213
Run #2
Initial Weight Final Volume
Run #1 30.1 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 950 330 ug/kg
95-57-8 2-Chlorophenol ND 190 19 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 190 19 ug/kg
120-83-2 2,4-Dichlorophenol ND 190 19 ug/kg
105-67-9 2,4-Dimethylphenol ND 190 24 ug/kg
51-28-5 2,4-Dinitrophenol ND 950 380 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 380 76 ug/kg
95-48-7 2-Methylphenol ND 190 19 ug/kg
3&4-Methylphenol ND 190 27 ug/kg
88-75-5 2-Nitrophenol ND 190 19 ug/kg
100-02-7 4-Nitrophenol ND 950 150 ug/kg
87-86-5 Pentachlorophenol ND 950 230 ug/kg
108-95-2 Phenol ND 190 19 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 190 19 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 190 19 ug/kg
83-32-9 Acenaphthene ND 190 19 ug/kg
208-96-8 Acenaphthylene ND 190 19 ug/kg
120-12-7 Anthracene ND 190 19 ug/kg
56-55-3 Benzo(a)anthracene ND 190 19 ug/kg
50-32-8 Benzo(a)pyrene ND 190 19 ug/kg
205-99-2 Benzo(b)fluoranthene ND 190 19 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 190 19 ug/kg
207-08-9 Benzo(k)fluoranthene ND 190 19 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 190 19 ug/kg
85-68-7 Butyl benzyl phthalate ND 190 38 ug/kg
100-51-6 Benzyl Alcohol ND 190 38 ug/kg
91-58-7 2-Chloronaphthalene ND 190 38 ug/kg
106-47-8 4-Chloroaniline ND 190 19 ug/kg
86-74-8 Carbazole ND 190 19 ug/kg
218-01-9 Chrysene ND 190 19 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 190 19 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 190 19 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B6/0.5-2
Lab Sample ID:F81928-14 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:87.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 190 19 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 190 19 ug/kg
95-50-1 1,2-Dichlorobenzene ND 190 38 ug/kg
541-73-1 1,3-Dichlorobenzene ND 190 38 ug/kg
106-46-7 1,4-Dichlorobenzene ND 190 38 ug/kg
121-14-2 2,4-Dinitrotoluene ND 190 19 ug/kg
606-20-2 2,6-Dinitrotoluene ND 190 22 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 380 38 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 190 19 ug/kg
132-64-9 Dibenzofuran ND 190 19 ug/kg
84-74-2 Di-n-butyl phthalate ND 380 76 ug/kg
117-84-0 Di-n-octyl phthalate ND 190 38 ug/kg
84-66-2 Diethyl phthalate ND 380 76 ug/kg
131-11-3 Dimethyl phthalate ND 190 38 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 380 76 ug/kg
206-44-0 Fluoranthene ND 190 19 ug/kg
86-73-7 Fluorene ND 190 19 ug/kg
118-74-1 Hexachlorobenzene ND 190 19 ug/kg
87-68-3 Hexachlorobutadiene ND 190 38 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 190 83 ug/kg
67-72-1 Hexachloroethane ND 190 38 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 190 19 ug/kg
78-59-1 Isophorone ND 190 19 ug/kg
91-57-6 2-Methylnaphthalene ND 190 19 ug/kg
88-74-4 2-Nitroaniline ND 190 38 ug/kg
99-09-2 3-Nitroaniline ND 190 38 ug/kg
100-01-6 4-Nitroaniline ND 190 38 ug/kg
91-20-3 Naphthalene ND 190 30 ug/kg
98-95-3 Nitrobenzene ND 190 19 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 190 19 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 190 19 ug/kg
85-01-8 Phenanthrene ND 190 19 ug/kg
129-00-0 Pyrene ND 190 19 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 190 19 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 62%40-102%
4165-62-2 Phenol-d5 71%41-100%
118-79-6 2,4,6-Tribromophenol 67%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B6/0.5-2
Lab Sample ID:F81928-14 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:87.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 64%40-105%
321-60-8 2-Fluorobiphenyl 66%43-107%
1718-51-0 Terphenyl-d14 74%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B6/0.5-2
Lab Sample ID:F81928-14 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C Percent Solids:87.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060058.D 1 05/06/11 AH n/a n/a GQR2610
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.41 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 6.0 3.0 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 75%56-136%
98-08-8 aaa-Trifluorotoluene 72%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B6/0.5-2
Lab Sample ID:F81928-14 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8082A SW846 3550C Percent Solids:87.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 XX055996.D 1 05/03/11 NJ 05/02/11 OP36984 GXX864
Run #2
Initial Weight Final Volume
Run #1 30.2 g 10.0 ml
Run #2
PCB List
CAS No.Compound Result RL MDL Units Q
12674-11-2 Aroclor 1016 ND 19 7.6 ug/kg
11104-28-2 Aroclor 1221 ND 19 9.4 ug/kg
11141-16-5 Aroclor 1232 ND 19 9.4 ug/kg
53469-21-9 Aroclor 1242 ND 19 7.6 ug/kg
12672-29-6 Aroclor 1248 ND 19 7.6 ug/kg
11097-69-1 Aroclor 1254 ND 19 7.6 ug/kg
11096-82-5 Aroclor 1260 ND 19 7.6 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 86%44-126%
2051-24-3 Decachlorobiphenyl 97%39-157%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B6/0.5-2
Lab Sample ID:F81928-14 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C SW846 3550C Percent Solids:87.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40285.D 1 05/03/11 SJL 05/02/11 OP36981 GZF1661
Run #2
Initial Weight Final Volume
Run #1 30.1 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 9.5 3.8 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 83%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B6/0.5-2
Lab Sample ID:F81928-14 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Percent Solids:87.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony <0.98 0.98 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 3
Arsenic 2.8 0.49 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 3
Barium 24.3 9.8 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 3
Beryllium 0.25 0.24 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 3
Cadmium <0.20 0.20 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 3
Chromium 60.2 0.49 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 3
Copper 13.8 1.2 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 3
Lead 11.7 0.98 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 3
Mercury <0.095 0.095 mg/kg 1 05/09/11 05/09/11 LM SW846 7471B 2 SW846 7471B 4
Molybdenum <2.4 2.4 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 3
Nickel 3.9 2.0 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 3
Selenium 1.5 0.98 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 3
Silver <0.49 0.49 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 3
Tin <2.4 2.4 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 3
Zinc 10.1 0.98 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 3
(1) Instrument QC Batch: MA8921
(2) Instrument QC Batch: MA8930
(3) Prep QC Batch: MP20489
(4) Prep QC Batch: MP20527
RL = Reporting Limit
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Client Sample ID:B6/10-12
Lab Sample ID:F81928-15 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:88.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F049448.D 1 05/09/11 CW n/a n/a VF1488
Run #2
Initial Weight
Run #1 5.16 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 55 22 ug/kg
71-43-2 Benzene ND 5.5 1.6 ug/kg
75-27-4 Bromodichloromethane ND 5.5 1.2 ug/kg
75-25-2 Bromoform ND 5.5 1.6 ug/kg
108-90-7 Chlorobenzene ND 5.5 1.1 ug/kg
75-00-3 Chloroethane ND 5.5 2.2 ug/kg
67-66-3 Chloroform ND 5.5 1.3 ug/kg
75-15-0 Carbon disulfide ND 5.5 2.2 ug/kg
56-23-5 Carbon tetrachloride ND 5.5 2.0 ug/kg
75-34-3 1,1-Dichloroethane ND 5.5 1.2 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.5 1.5 ug/kg
107-06-2 1,2-Dichloroethane ND 5.5 1.1 ug/kg
78-87-5 1,2-Dichloropropane ND 5.5 1.3 ug/kg
124-48-1 Dibromochloromethane ND 5.5 1.1 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.5 1.6 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.5 1.1 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.5 1.6 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.5 1.2 ug/kg
100-41-4 Ethylbenzene ND 5.5 1.1 ug/kg
591-78-6 2-Hexanone ND 27 5.9 ug/kg
108-10-1 4-Methyl-2-pentanone ND 27 6.0 ug/kg
74-83-9 Methyl bromide ND 5.5 2.2 ug/kg
74-87-3 Methyl chloride ND 5.5 2.2 ug/kg
75-09-2 Methylene chloride ND 11 5.1 ug/kg
78-93-3 Methyl ethyl ketone ND 27 6.7 ug/kg
100-42-5 Styrene ND 5.5 2.9 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.5 1.2 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.5 1.3 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.5 1.2 ug/kg
127-18-4 Tetrachloroethylene ND 5.5 1.1 ug/kg
108-88-3 Toluene ND 5.5 1.3 ug/kg
79-01-6 Trichloroethylene ND 5.5 1.3 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B6/10-12
Lab Sample ID:F81928-15 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:88.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 5.5 1.6 ug/kg
1330-20-7 Xylene (total)ND 16 3.5 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%80-121%
2037-26-5 Toluene-D8 101%71-130%
460-00-4 4-Bromofluorobenzene 99%59-148%
17060-07-0 1,2-Dichloroethane-D4 104%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B6/10-12
Lab Sample ID:F81928-15 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:88.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025263.D 1 05/05/11 MG 05/03/11 OP36999 SU1213
Run #2
Initial Weight Final Volume
Run #1 29.5 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 960 340 ug/kg
95-57-8 2-Chlorophenol ND 190 19 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 190 19 ug/kg
120-83-2 2,4-Dichlorophenol ND 190 19 ug/kg
105-67-9 2,4-Dimethylphenol ND 190 24 ug/kg
51-28-5 2,4-Dinitrophenol ND 960 380 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 380 77 ug/kg
95-48-7 2-Methylphenol ND 190 19 ug/kg
3&4-Methylphenol ND 190 28 ug/kg
88-75-5 2-Nitrophenol ND 190 19 ug/kg
100-02-7 4-Nitrophenol ND 960 150 ug/kg
87-86-5 Pentachlorophenol ND 960 230 ug/kg
108-95-2 Phenol ND 190 19 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 190 19 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 190 19 ug/kg
83-32-9 Acenaphthene ND 190 19 ug/kg
208-96-8 Acenaphthylene ND 190 19 ug/kg
120-12-7 Anthracene ND 190 19 ug/kg
56-55-3 Benzo(a)anthracene ND 190 19 ug/kg
50-32-8 Benzo(a)pyrene ND 190 19 ug/kg
205-99-2 Benzo(b)fluoranthene ND 190 19 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 190 19 ug/kg
207-08-9 Benzo(k)fluoranthene ND 190 19 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 190 19 ug/kg
85-68-7 Butyl benzyl phthalate ND 190 38 ug/kg
100-51-6 Benzyl Alcohol ND 190 38 ug/kg
91-58-7 2-Chloronaphthalene ND 190 38 ug/kg
106-47-8 4-Chloroaniline ND 190 19 ug/kg
86-74-8 Carbazole ND 190 19 ug/kg
218-01-9 Chrysene ND 190 19 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 190 19 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 190 19 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B6/10-12
Lab Sample ID:F81928-15 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:88.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 190 19 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 190 19 ug/kg
95-50-1 1,2-Dichlorobenzene ND 190 38 ug/kg
541-73-1 1,3-Dichlorobenzene ND 190 38 ug/kg
106-46-7 1,4-Dichlorobenzene ND 190 38 ug/kg
121-14-2 2,4-Dinitrotoluene ND 190 19 ug/kg
606-20-2 2,6-Dinitrotoluene ND 190 23 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 380 38 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 190 19 ug/kg
132-64-9 Dibenzofuran ND 190 19 ug/kg
84-74-2 Di-n-butyl phthalate ND 380 77 ug/kg
117-84-0 Di-n-octyl phthalate ND 190 38 ug/kg
84-66-2 Diethyl phthalate ND 380 77 ug/kg
131-11-3 Dimethyl phthalate ND 190 38 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 380 77 ug/kg
206-44-0 Fluoranthene ND 190 19 ug/kg
86-73-7 Fluorene ND 190 19 ug/kg
118-74-1 Hexachlorobenzene ND 190 19 ug/kg
87-68-3 Hexachlorobutadiene ND 190 38 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 190 85 ug/kg
67-72-1 Hexachloroethane ND 190 38 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 190 19 ug/kg
78-59-1 Isophorone ND 190 19 ug/kg
91-57-6 2-Methylnaphthalene ND 190 19 ug/kg
88-74-4 2-Nitroaniline ND 190 38 ug/kg
99-09-2 3-Nitroaniline ND 190 38 ug/kg
100-01-6 4-Nitroaniline ND 190 38 ug/kg
91-20-3 Naphthalene ND 190 31 ug/kg
98-95-3 Nitrobenzene ND 190 19 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 190 19 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 190 19 ug/kg
85-01-8 Phenanthrene ND 190 19 ug/kg
129-00-0 Pyrene ND 190 19 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 190 19 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 66%40-102%
4165-62-2 Phenol-d5 73%41-100%
118-79-6 2,4,6-Tribromophenol 69%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B6/10-12
Lab Sample ID:F81928-15 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:88.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 68%40-105%
321-60-8 2-Fluorobiphenyl 70%43-107%
1718-51-0 Terphenyl-d14 74%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B6/10-12
Lab Sample ID:F81928-15 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C Percent Solids:88.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060059.D 1 05/07/11 AH n/a n/a GQR2610
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.68 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 5.7 2.8 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 75%56-136%
98-08-8 aaa-Trifluorotoluene 74%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B6/10-12
Lab Sample ID:F81928-15 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C SW846 3550C Percent Solids:88.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40286.D 1 05/03/11 SJL 05/02/11 OP36981 GZF1661
Run #2
Initial Weight Final Volume
Run #1 30.4 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 9.3 3.7 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 77%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B6/10-12
Lab Sample ID:F81928-15 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Percent Solids:88.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <1.8 1.8 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Arsenic a 1.6 0.92 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Barium <9.2 9.2 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Beryllium <0.23 0.23 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Cadmium a <0.37 0.37 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Chromium a 24.4 0.92 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Copper a 19.9 2.3 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Lead a 8.0 1.8 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Mercury <0.092 0.092 mg/kg 1 05/09/11 05/09/11 LM SW846 7471B 3 SW846 7471B 5
Molybdenum a <4.6 4.6 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Nickel a <3.7 3.7 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Selenium a 2.0 1.8 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Silver a <0.92 0.92 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Tin <2.3 2.3 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Zinc a 6.5 1.8 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
(1) Instrument QC Batch: MA8921
(2) Instrument QC Batch: MA8926
(3) Instrument QC Batch: MA8930
(4) Prep QC Batch: MP20489
(5) Prep QC Batch: MP20527
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Client Sample ID:B7/0.5-2
Lab Sample ID:F81928-16 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:76.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F049449.D 1 05/09/11 CW n/a n/a VF1488
Run #2
Initial Weight
Run #1 6.02 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 55 22 ug/kg
71-43-2 Benzene ND 5.5 1.6 ug/kg
75-27-4 Bromodichloromethane ND 5.5 1.2 ug/kg
75-25-2 Bromoform ND 5.5 1.6 ug/kg
108-90-7 Chlorobenzene ND 5.5 1.1 ug/kg
75-00-3 Chloroethane ND 5.5 2.2 ug/kg
67-66-3 Chloroform ND 5.5 1.3 ug/kg
75-15-0 Carbon disulfide ND 5.5 2.2 ug/kg
56-23-5 Carbon tetrachloride ND 5.5 2.0 ug/kg
75-34-3 1,1-Dichloroethane ND 5.5 1.2 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.5 1.5 ug/kg
107-06-2 1,2-Dichloroethane ND 5.5 1.1 ug/kg
78-87-5 1,2-Dichloropropane ND 5.5 1.3 ug/kg
124-48-1 Dibromochloromethane ND 5.5 1.1 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.5 1.6 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.5 1.1 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.5 1.6 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.5 1.2 ug/kg
100-41-4 Ethylbenzene ND 5.5 1.1 ug/kg
591-78-6 2-Hexanone ND 27 5.9 ug/kg
108-10-1 4-Methyl-2-pentanone ND 27 6.0 ug/kg
74-83-9 Methyl bromide ND 5.5 2.2 ug/kg
74-87-3 Methyl chloride ND 5.5 2.2 ug/kg
75-09-2 Methylene chloride ND 11 5.0 ug/kg
78-93-3 Methyl ethyl ketone ND 27 6.7 ug/kg
100-42-5 Styrene ND 5.5 2.8 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.5 1.2 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.5 1.3 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.5 1.2 ug/kg
127-18-4 Tetrachloroethylene ND 5.5 1.1 ug/kg
108-88-3 Toluene ND 5.5 1.3 ug/kg
79-01-6 Trichloroethylene ND 5.5 1.3 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B7/0.5-2
Lab Sample ID:F81928-16 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:76.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 5.5 1.6 ug/kg
1330-20-7 Xylene (total)ND 16 3.5 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 107%80-121%
2037-26-5 Toluene-D8 98%71-130%
460-00-4 4-Bromofluorobenzene 99%59-148%
17060-07-0 1,2-Dichloroethane-D4 117%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B7/0.5-2
Lab Sample ID:F81928-16 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:76.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025264.D 1 05/05/11 MG 05/03/11 OP36999 SU1213
Run #2
Initial Weight Final Volume
Run #1 29.6 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1100 390 ug/kg
95-57-8 2-Chlorophenol ND 220 22 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 220 22 ug/kg
120-83-2 2,4-Dichlorophenol ND 220 22 ug/kg
105-67-9 2,4-Dimethylphenol ND 220 28 ug/kg
51-28-5 2,4-Dinitrophenol ND 1100 440 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 440 89 ug/kg
95-48-7 2-Methylphenol ND 220 22 ug/kg
3&4-Methylphenol ND 220 32 ug/kg
88-75-5 2-Nitrophenol ND 220 22 ug/kg
100-02-7 4-Nitrophenol ND 1100 180 ug/kg
87-86-5 Pentachlorophenol ND 1100 270 ug/kg
108-95-2 Phenol ND 220 22 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 220 22 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 220 22 ug/kg
83-32-9 Acenaphthene ND 220 22 ug/kg
208-96-8 Acenaphthylene ND 220 22 ug/kg
120-12-7 Anthracene ND 220 22 ug/kg
56-55-3 Benzo(a)anthracene ND 220 22 ug/kg
50-32-8 Benzo(a)pyrene ND 220 22 ug/kg
205-99-2 Benzo(b)fluoranthene ND 220 22 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 220 22 ug/kg
207-08-9 Benzo(k)fluoranthene ND 220 22 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 220 22 ug/kg
85-68-7 Butyl benzyl phthalate ND 220 44 ug/kg
100-51-6 Benzyl Alcohol ND 220 44 ug/kg
91-58-7 2-Chloronaphthalene ND 220 44 ug/kg
106-47-8 4-Chloroaniline ND 220 22 ug/kg
86-74-8 Carbazole ND 220 22 ug/kg
218-01-9 Chrysene ND 220 22 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 220 22 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 220 22 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B7/0.5-2
Lab Sample ID:F81928-16 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:76.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 220 22 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 220 22 ug/kg
95-50-1 1,2-Dichlorobenzene ND 220 44 ug/kg
541-73-1 1,3-Dichlorobenzene ND 220 44 ug/kg
106-46-7 1,4-Dichlorobenzene ND 220 44 ug/kg
121-14-2 2,4-Dinitrotoluene ND 220 22 ug/kg
606-20-2 2,6-Dinitrotoluene ND 220 26 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 440 44 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 220 22 ug/kg
132-64-9 Dibenzofuran ND 220 22 ug/kg
84-74-2 Di-n-butyl phthalate ND 440 89 ug/kg
117-84-0 Di-n-octyl phthalate ND 220 44 ug/kg
84-66-2 Diethyl phthalate ND 440 89 ug/kg
131-11-3 Dimethyl phthalate ND 220 44 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 440 89 ug/kg
206-44-0 Fluoranthene ND 220 22 ug/kg
86-73-7 Fluorene ND 220 22 ug/kg
118-74-1 Hexachlorobenzene ND 220 22 ug/kg
87-68-3 Hexachlorobutadiene ND 220 44 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 220 98 ug/kg
67-72-1 Hexachloroethane ND 220 44 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 220 22 ug/kg
78-59-1 Isophorone ND 220 22 ug/kg
91-57-6 2-Methylnaphthalene ND 220 22 ug/kg
88-74-4 2-Nitroaniline ND 220 44 ug/kg
99-09-2 3-Nitroaniline ND 220 44 ug/kg
100-01-6 4-Nitroaniline ND 220 44 ug/kg
91-20-3 Naphthalene ND 220 36 ug/kg
98-95-3 Nitrobenzene ND 220 22 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 220 22 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 220 22 ug/kg
85-01-8 Phenanthrene ND 220 22 ug/kg
129-00-0 Pyrene ND 220 22 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 220 22 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 69%40-102%
4165-62-2 Phenol-d5 78%41-100%
118-79-6 2,4,6-Tribromophenol 73%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B7/0.5-2
Lab Sample ID:F81928-16 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:76.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 70%40-105%
321-60-8 2-Fluorobiphenyl 71%43-107%
1718-51-0 Terphenyl-d14 79%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B7/0.5-2
Lab Sample ID:F81928-16 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C Percent Solids:76.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060060.D 1 05/07/11 AH n/a n/a GQR2610
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.03 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 7.0 3.5 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 76%56-136%
98-08-8 aaa-Trifluorotoluene 74%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B7/0.5-2
Lab Sample ID:F81928-16 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8082A SW846 3550C Percent Solids:76.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 XX055997.D 1 05/03/11 NJ 05/02/11 OP36984 GXX864
Run #2
Initial Weight Final Volume
Run #1 29.8 g 10.0 ml
Run #2
PCB List
CAS No.Compound Result RL MDL Units Q
12674-11-2 Aroclor 1016 ND 22 8.8 ug/kg
11104-28-2 Aroclor 1221 ND 22 11 ug/kg
11141-16-5 Aroclor 1232 ND 22 11 ug/kg
53469-21-9 Aroclor 1242 ND 22 8.8 ug/kg
12672-29-6 Aroclor 1248 ND 22 8.8 ug/kg
11097-69-1 Aroclor 1254 ND 22 8.8 ug/kg
11096-82-5 Aroclor 1260 ND 22 8.8 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 83%44-126%
2051-24-3 Decachlorobiphenyl 95%39-157%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B7/0.5-2
Lab Sample ID:F81928-16 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C SW846 3550C Percent Solids:76.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40296.D 1 05/04/11 SJL 05/04/11 OP37014 GZF1662
Run #2
Initial Weight Final Volume
Run #1 30.3 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 11 4.3 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 100%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:B7/0.5-2
Lab Sample ID:F81928-16 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Percent Solids:76.1
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <2.5 2.5 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Arsenic a 2.6 1.3 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Barium 13.6 13 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Beryllium <0.31 0.31 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Cadmium a <0.50 0.50 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Chromium a 40.5 1.3 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Copper a 48.3 3.1 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Lead a 11.0 2.5 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Mercury <0.11 0.11 mg/kg 1 05/09/11 05/09/11 LM SW846 7471B 3 SW846 7471B 5
Molybdenum a <6.3 6.3 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Nickel a 6.6 5.0 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Selenium a 3.5 2.5 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Silver a <1.3 1.3 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Tin <3.1 3.1 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Zinc a 13.3 2.5 mg/kg 2 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
(1) Instrument QC Batch: MA8921
(2) Instrument QC Batch: MA8926
(3) Instrument QC Batch: MA8930
(4) Prep QC Batch: MP20489
(5) Prep QC Batch: MP20527
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Report of Analysis Page 1 of 2
Client Sample ID:B7/10-12
Lab Sample ID:F81928-17 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:74.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F049450.D 1 05/09/11 CW n/a n/a VF1488
Run #2
Initial Weight
Run #1 5.34 g
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 63 25 ug/kg
71-43-2 Benzene ND 6.3 1.9 ug/kg
75-27-4 Bromodichloromethane ND 6.3 1.4 ug/kg
75-25-2 Bromoform ND 6.3 1.9 ug/kg
108-90-7 Chlorobenzene ND 6.3 1.3 ug/kg
75-00-3 Chloroethane ND 6.3 2.5 ug/kg
67-66-3 Chloroform ND 6.3 1.5 ug/kg
75-15-0 Carbon disulfide ND 6.3 2.5 ug/kg
56-23-5 Carbon tetrachloride ND 6.3 2.3 ug/kg
75-34-3 1,1-Dichloroethane ND 6.3 1.4 ug/kg
75-35-4 1,1-Dichloroethylene ND 6.3 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 6.3 1.3 ug/kg
78-87-5 1,2-Dichloropropane ND 6.3 1.5 ug/kg
124-48-1 Dibromochloromethane ND 6.3 1.3 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 6.3 1.9 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 6.3 1.3 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 6.3 1.9 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 6.3 1.4 ug/kg
100-41-4 Ethylbenzene ND 6.3 1.3 ug/kg
591-78-6 2-Hexanone ND 31 6.8 ug/kg
108-10-1 4-Methyl-2-pentanone ND 31 6.9 ug/kg
74-83-9 Methyl bromide ND 6.3 2.5 ug/kg
74-87-3 Methyl chloride ND 6.3 2.5 ug/kg
75-09-2 Methylene chloride ND 13 5.8 ug/kg
78-93-3 Methyl ethyl ketone ND 31 7.6 ug/kg
100-42-5 Styrene ND 6.3 3.3 ug/kg
71-55-6 1,1,1-Trichloroethane ND 6.3 1.4 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 6.3 1.5 ug/kg
79-00-5 1,1,2-Trichloroethane ND 6.3 1.4 ug/kg
127-18-4 Tetrachloroethylene ND 6.3 1.3 ug/kg
108-88-3 Toluene ND 6.3 1.5 ug/kg
79-01-6 Trichloroethylene ND 6.3 1.5 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:B7/10-12
Lab Sample ID:F81928-17 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8260B Percent Solids:74.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride ND 6.3 1.9 ug/kg
1330-20-7 Xylene (total)ND 19 4.0 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%80-121%
2037-26-5 Toluene-D8 100%71-130%
460-00-4 4-Bromofluorobenzene 100%59-148%
17060-07-0 1,2-Dichloroethane-D4 107%77-123%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:B7/10-12
Lab Sample ID:F81928-17 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:74.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025265.D 1 05/05/11 MG 05/03/11 OP36999 SU1213
Run #2
Initial Weight Final Volume
Run #1 29.7 g 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1100 400 ug/kg
95-57-8 2-Chlorophenol ND 220 22 ug/kg
59-50-7 4-Chloro-3-methyl phenol ND 220 22 ug/kg
120-83-2 2,4-Dichlorophenol ND 220 22 ug/kg
105-67-9 2,4-Dimethylphenol ND 220 28 ug/kg
51-28-5 2,4-Dinitrophenol ND 1100 450 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 450 90 ug/kg
95-48-7 2-Methylphenol ND 220 22 ug/kg
3&4-Methylphenol ND 220 32 ug/kg
88-75-5 2-Nitrophenol ND 220 22 ug/kg
100-02-7 4-Nitrophenol ND 1100 180 ug/kg
87-86-5 Pentachlorophenol ND 1100 270 ug/kg
108-95-2 Phenol ND 220 22 ug/kg
95-95-4 2,4,5-Trichlorophenol ND 220 22 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 220 22 ug/kg
83-32-9 Acenaphthene ND 220 22 ug/kg
208-96-8 Acenaphthylene ND 220 22 ug/kg
120-12-7 Anthracene ND 220 22 ug/kg
56-55-3 Benzo(a)anthracene ND 220 22 ug/kg
50-32-8 Benzo(a)pyrene ND 220 22 ug/kg
205-99-2 Benzo(b)fluoranthene ND 220 22 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 220 22 ug/kg
207-08-9 Benzo(k)fluoranthene ND 220 22 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 220 22 ug/kg
85-68-7 Butyl benzyl phthalate ND 220 45 ug/kg
100-51-6 Benzyl Alcohol ND 220 45 ug/kg
91-58-7 2-Chloronaphthalene ND 220 45 ug/kg
106-47-8 4-Chloroaniline ND 220 22 ug/kg
86-74-8 Carbazole ND 220 22 ug/kg
218-01-9 Chrysene ND 220 22 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 220 22 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 220 22 ug/kg
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:B7/10-12
Lab Sample ID:F81928-17 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:74.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether ND 220 22 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 220 22 ug/kg
95-50-1 1,2-Dichlorobenzene ND 220 45 ug/kg
541-73-1 1,3-Dichlorobenzene ND 220 45 ug/kg
106-46-7 1,4-Dichlorobenzene ND 220 45 ug/kg
121-14-2 2,4-Dinitrotoluene ND 220 22 ug/kg
606-20-2 2,6-Dinitrotoluene ND 220 27 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 450 45 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 220 22 ug/kg
132-64-9 Dibenzofuran ND 220 22 ug/kg
84-74-2 Di-n-butyl phthalate ND 450 90 ug/kg
117-84-0 Di-n-octyl phthalate ND 220 45 ug/kg
84-66-2 Diethyl phthalate ND 450 90 ug/kg
131-11-3 Dimethyl phthalate ND 220 45 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 450 90 ug/kg
206-44-0 Fluoranthene ND 220 22 ug/kg
86-73-7 Fluorene ND 220 22 ug/kg
118-74-1 Hexachlorobenzene ND 220 22 ug/kg
87-68-3 Hexachlorobutadiene ND 220 45 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 220 99 ug/kg
67-72-1 Hexachloroethane ND 220 45 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 220 22 ug/kg
78-59-1 Isophorone ND 220 22 ug/kg
91-57-6 2-Methylnaphthalene ND 220 22 ug/kg
88-74-4 2-Nitroaniline ND 220 45 ug/kg
99-09-2 3-Nitroaniline ND 220 45 ug/kg
100-01-6 4-Nitroaniline ND 220 45 ug/kg
91-20-3 Naphthalene ND 220 36 ug/kg
98-95-3 Nitrobenzene ND 220 22 ug/kg
621-64-7 N-Nitroso-di-n-propylamine ND 220 22 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 220 22 ug/kg
85-01-8 Phenanthrene ND 220 22 ug/kg
129-00-0 Pyrene ND 220 22 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 220 22 ug/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 64%40-102%
4165-62-2 Phenol-d5 72%41-100%
118-79-6 2,4,6-Tribromophenol 69%42-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:B7/10-12
Lab Sample ID:F81928-17 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8270D SW846 3550C Percent Solids:74.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 65%40-105%
321-60-8 2-Fluorobiphenyl 69%43-107%
1718-51-0 Terphenyl-d14 73%45-119%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B7/10-12
Lab Sample ID:F81928-17 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C Percent Solids:74.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 QR060061.D 1 05/07/11 AH n/a n/a GQR2610
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.48 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 7.8 3.9 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 77%56-136%
98-08-8 aaa-Trifluorotoluene 74%61-121%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B7/10-12
Lab Sample ID:F81928-17 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Method:SW846 8015C SW846 3550C Percent Solids:74.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40297.D 1 05/04/11 SJL 05/04/11 OP37014 GZF1662
Run #2
Initial Weight Final Volume
Run #1 30.2 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 11 4.4 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 94%49-108%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:B7/10-12
Lab Sample ID:F81928-17 Date Sampled:04/28/11
Matrix:SO - Soil Date Received:04/29/11
Percent Solids:74.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <5.2 5.2 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Arsenic a 2.8 2.6 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Barium a 195 52 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Beryllium a <1.3 1.3 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Cadmium a <1.0 1.0 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Chromium a 21.2 2.6 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Copper a 60.4 6.5 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Lead 9.6 1.0 mg/kg 1 05/03/11 05/04/11 RS SW846 6010C 1 SW846 3050B 4
Mercury <0.097 0.097 mg/kg 1 05/09/11 05/09/11 LM SW846 7471B 3 SW846 7471B 5
Molybdenum a <13 13 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Nickel a 17.6 10 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Selenium a <5.2 5.2 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Silver a <2.6 2.6 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Tin a <13 13 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
Zinc a 55.3 5.2 mg/kg 5 05/03/11 05/05/11 RS SW846 6010C 2 SW846 3050B 4
(1) Instrument QC Batch: MA8921
(2) Instrument QC Batch: MA8926
(3) Instrument QC Batch: MA8930
(4) Prep QC Batch: MP20489
(5) Prep QC Batch: MP20527
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Certification Exceptions
• Certification Exceptions (NC)
• Chain of Custody
Southeast
Section 4
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02/16/12
Technical Report for
AMEC Environment & Infrastructure, Inc.
GE-TFS; 1906 Bancroft St, Charlotte, NC
572260702
Accutest Job Number: F82004
Sampling Date: 05/02/11
Report to:
AMEC Earth & Environmental
steven.tanen@amec.com
ATTN: Steve Tanen
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), AK, AR, GA, KY, MA, NV, OK, UT, VA, WA, WI
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Conference
and/or state specific certification programs as applicable.
Client Service contact: Heather Wandrey 407-425-6700
Harry Behzadi, Ph.D.
Laboratory Director
Southeast
02/16/12
Reissue #1
e-Hardcopy 2.0
Automated Report
28
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
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F82004
Florida 4405 Vineland Road Suite C-15 Orlando, FL 32811 tel: 407 425-6700 fax: 407 425-0707 htpp://www.accutest.com www.accutest.com
August 2, 2011
Mr. Steven Tanen
AMEC Earth & Environmental
502 W. Germantown Pike
Suite 850
Plymouth Meeting, PA 19462
RE: Accutest job F82004 Reissue
Dear Mr. Tanen,
The final report for job number F82004 has been edited to reflect requested corrections.
These edits have been incorporated into the revised report.
All data reported to the MDL.
Accutest apologies for any inconvenience this may have caused. Please feel free to contact
us if we can be of further assistance.
Sincerely,
Accutest Laboratories, SE
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F82004
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................4
Section 2: Case Narrative/Conformance Summary ..............................................................5
Section 3: Sample Results ........................................................................................................7
3.1: F82004-1: MW-1 ..........................................................................................................8
3.2: F82004-1F: MW-1 ........................................................................................................16
3.3: F82004-2: MW-2 ..........................................................................................................17
3.4: F82004-2F: MW-2 ........................................................................................................25
Section 4: Misc. Forms ............................................................................................................26
4.1: Chain of Custody ...........................................................................................................27
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2
3
4
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Sample Summary
AMEC Environment & Infrastructure, Inc.
Job No:F82004
GE-TFS; 1906 Bancroft St, Charlotte, NC
Project No: 572260702
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
F82004-1 05/02/11 10:55 BE 05/03/11 AQ Ground Water MW-1
F82004-1F 05/02/11 10:55 BE 05/03/11 AQ Groundwater Filtered MW-1
F82004-2 05/02/11 13:24 BE 05/03/11 AQ Ground Water MW-2
F82004-2F 05/02/11 13:24 BE 05/03/11 AQ Groundwater Filtered MW-2
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SAMPLE DELIVERY GROUP CASE NARRATIVE
Client: AMEC Earth & Environmental Job F82004
Site: GE-TFS; 1906 Bancroft St, Charlotte, NC Report Date: 5/20/2011 7:37:01 AM
2 Samples were collected on 05/02/2011 and were received at Accutest SE on 05/03/2011 properly preserved, at 2.4 Deg. C and
intact. These Samples received an Accutest job number of F82004. A listing of the Laboratory Sample ID, Client Sample ID and
dates of collection are presented in the Results Summary Section of this report.
Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For more
information, please refer to QC summary pages.
Volatiles by GCMS by Method SW846 8260B Matrix: AQ Batch ID: VJ3586
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F81984-1MS, F81984-1MSD were used as the QC samples indicated.
Matrix Spike Duplicate Recoverys for 2-Hexanone, 4-Methyl-2-pentanone, Methyl ethyl ketone are outside control limits. Probable cause due to matrix interference.
F82004-1 for Methylene chloride: Suspected laboratory contaminant.
Extractables by GCMS by Method SW846 8270D Matrix: AQ Batch ID: OP37011
All samples were extracted within the recommended method holding time.
All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria.
Samples F81924-1MS, F81924-1MSD were used as the QC samples indicated.
Matrix Spike Recoverys for 4-Nitrophenol, Phenol are outside control limits. Probable cause due to matrix interference.
Samples OP37011-MS, OP37011-MSD have surrogates outside control limits. Probable cause due to matrix interference.
Volatiles by GC by Method SW846 8015C Matrix: AQ Batch ID: GCD4290
All samples were analyzed within the recommended method holding time.
Samples F82038-1MS, F82038-1MSD, F82095-1DUP were used as the QC samples indicated.
All method blanks for this batch meet method specific criteria.
Extractables by GC by Method SW846 8015C Matrix: AQ Batch ID: OP37019
All samples were extracted within the recommended method holding time. All samples were analyzed within the recommended method holding time.
Samples F81874-1MS, F81874-1MSD were used as the QC samples indicated.
All method blanks for this batch meet method specific criteria.
Matrix Spike and Matrix Spike Duplicate Recoverys for TPH (C10-C28) are outside control limits. Outside control limits due to high level in sample relative to spike amount.
Friday, May 20, 2011
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Metals by Method SW846 6010C Matrix: AQ Batch ID: MP20503
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria.
Samples F81995-2MS, F81995-2MSD, F81995-2PS, F81995-2SDL, F81995-2DUP were used as the QC samples for metals.
RPDs for Duplicate for Chromium, Lead are outside control limits for sample MP20503-D1. RPD acceptable due to low duplicate and sample concentrations.
RPDs for Serial Dilution for Antimony, Barium, Chromium, Zinc are outside control limits for sample MP20503-SD1. Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
Metals by Method SW846 7470A Matrix: AQ Batch ID: MP20507
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F81877-2DUP, F81877-2MS, F81877-2MSD, F81877-2SDL were used as the QC samples for metals.
Accutest Laboratories Southeast (ALSE) certifies that this report meets the project requirements for analytical data produced for the
samples as received at ALSE and as stated on the COC. ALSE certifies that the data meets the Data Quality Objectives for precision,
accuracy and completeness as specified in the ALSE Quality Manual except as noted above. This report is to be used in its entirety.
ALSE is not responsible for any assumptions of data quality if partial data packages are used.
Narrative prepared by:
_______________________________________ Date: May 20, 2011
Ellen Pampel, Inorganic QA (signature on file)
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Sample Results
Report of Analysis
Southeast
Section 3
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Report of Analysis Page 1 of 2
Client Sample ID:MW-1
Lab Sample ID:F82004-1 Date Sampled:05/02/11
Matrix:AQ - Ground Water Date Received:05/03/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 J065525.D 2 05/13/11 MM n/a n/a VJ3586
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 20 U 50 20 ug/l
71-43-2 Benzene 0.40 U 2.0 0.40 ug/l
75-27-4 Bromodichloromethane 0.40 U 2.0 0.40 ug/l
75-25-2 Bromoform 0.40 U 2.0 0.40 ug/l
108-90-7 Chlorobenzene 0.40 U 2.0 0.40 ug/l
75-00-3 Chloroethane 1.0 U 4.0 1.0 ug/l
67-66-3 Chloroform 0.87 2.0 0.44 ug/l J
75-15-0 Carbon disulfide 1.0 U 4.0 1.0 ug/l
56-23-5 Carbon tetrachloride 0.50 U 2.0 0.50 ug/l
75-34-3 1,1-Dichloroethane 0.92 2.0 0.50 ug/l J
75-35-4 1,1-Dichloroethylene 6.7 2.0 0.46 ug/l
107-06-2 1,2-Dichloroethane 0.40 U 2.0 0.40 ug/l
78-87-5 1,2-Dichloropropane 0.50 U 2.0 0.50 ug/l
124-48-1 Dibromochloromethane 0.40 U 2.0 0.40 ug/l
156-59-2 cis-1,2-Dichloroethylene 20.4 2.0 0.52 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.40 U 2.0 0.40 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.70 U 2.0 0.70 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.40 U 2.0 0.40 ug/l
100-41-4 Ethylbenzene 0.40 U 2.0 0.40 ug/l
591-78-6 2-Hexanone 8.0 U 20 8.0 ug/l
108-10-1 4-Methyl-2-pentanone 4.0 U 10 4.0 ug/l
74-83-9 Methyl bromide 1.0 U 4.0 1.0 ug/l
74-87-3 Methyl chloride 1.0 U 4.0 1.0 ug/l
75-09-2 Methylene chloride a 10.9 10 4.0 ug/l
78-93-3 Methyl ethyl ketone 4.0 U 10 4.0 ug/l
100-42-5 Styrene 0.40 U 2.0 0.40 ug/l
71-55-6 1,1,1-Trichloroethane 0.40 U 2.0 0.40 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.46 U 2.0 0.46 ug/l
79-00-5 1,1,2-Trichloroethane 0.44 U 2.0 0.44 ug/l
127-18-4 Tetrachloroethylene 71.6 2.0 0.50 ug/l
108-88-3 Toluene 0.40 U 2.0 0.40 ug/l
79-01-6 Trichloroethylene 104 2.0 0.52 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-1
Lab Sample ID:F82004-1 Date Sampled:05/02/11
Matrix:AQ - Ground Water Date Received:05/03/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.44 U 2.0 0.44 ug/l
1330-20-7 Xylene (total)1.0 U 6.0 1.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%87-116%
17060-07-0 1,2-Dichloroethane-D4 101%76-127%
2037-26-5 Toluene-D8 104%86-112%
460-00-4 4-Bromofluorobenzene 111%84-120%
(a) Suspected laboratory contaminant.
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-1
Lab Sample ID:F82004-1 Date Sampled:05/02/11
Matrix:AQ - Ground Water Date Received:05/03/11
Method:SW846 8270D SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L051239.D 1 05/06/11 NAF 05/04/11 OP37011 SL2614
Run #2
Initial Volume Final Volume
Run #1 1050 ml 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid 9.5 U 48 9.5 ug/l
95-57-8 2-Chlorophenol 0.48 U 4.8 0.48 ug/l
59-50-7 4-Chloro-3-methyl phenol 0.48 U 4.8 0.48 ug/l
120-83-2 2,4-Dichlorophenol 0.48 U 4.8 0.48 ug/l
105-67-9 2,4-Dimethylphenol 1.0 U 4.8 1.0 ug/l
51-28-5 2,4-Dinitrophenol 9.5 U 24 9.5 ug/l
534-52-1 4,6-Dinitro-o-cresol 1.9 U 9.5 1.9 ug/l
95-48-7 2-Methylphenol 0.51 U 4.8 0.51 ug/l
3&4-Methylphenol 1.0 U 4.8 1.0 ug/l
88-75-5 2-Nitrophenol 0.51 U 4.8 0.51 ug/l
100-02-7 4-Nitrophenol 4.8 U 24 4.8 ug/l
87-86-5 Pentachlorophenol 5.1 U 24 5.1 ug/l
108-95-2 Phenol 0.48 U 4.8 0.48 ug/l
95-95-4 2,4,5-Trichlorophenol 0.48 U 4.8 0.48 ug/l
88-06-2 2,4,6-Trichlorophenol 0.48 U 4.8 0.48 ug/l
83-32-9 Acenaphthene 0.48 U 4.8 0.48 ug/l
208-96-8 Acenaphthylene 0.48 U 4.8 0.48 ug/l
120-12-7 Anthracene 0.48 U 4.8 0.48 ug/l
56-55-3 Benzo(a)anthracene 0.48 U 4.8 0.48 ug/l
50-32-8 Benzo(a)pyrene 0.48 U 4.8 0.48 ug/l
205-99-2 Benzo(b)fluoranthene 0.48 U 4.8 0.48 ug/l
191-24-2 Benzo(g,h,i)perylene 0.48 U 4.8 0.48 ug/l
207-08-9 Benzo(k)fluoranthene 0.48 U 4.8 0.48 ug/l
101-55-3 4-Bromophenyl phenyl ether 0.48 U 4.8 0.48 ug/l
85-68-7 Butyl benzyl phthalate 1.0 U 4.8 1.0 ug/l
100-51-6 Benzyl Alcohol 0.95 U 4.8 0.95 ug/l
91-58-7 2-Chloronaphthalene 0.48 U 4.8 0.48 ug/l
106-47-8 4-Chloroaniline 0.48 U 4.8 0.48 ug/l
86-74-8 Carbazole 0.48 U 4.8 0.48 ug/l
218-01-9 Chrysene 0.48 U 4.8 0.48 ug/l
111-91-1 bis(2-Chloroethoxy)methane 0.48 U 4.8 0.48 ug/l
111-44-4 bis(2-Chloroethyl)ether 0.51 U 4.8 0.51 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-1
Lab Sample ID:F82004-1 Date Sampled:05/02/11
Matrix:AQ - Ground Water Date Received:05/03/11
Method:SW846 8270D SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether 0.51 U 4.8 0.51 ug/l
7005-72-3 4-Chlorophenyl phenyl ether 0.48 U 4.8 0.48 ug/l
95-50-1 1,2-Dichlorobenzene 0.95 U 4.8 0.95 ug/l
541-73-1 1,3-Dichlorobenzene 0.95 U 4.8 0.95 ug/l
106-46-7 1,4-Dichlorobenzene 0.95 U 4.8 0.95 ug/l
121-14-2 2,4-Dinitrotoluene 0.48 U 4.8 0.48 ug/l
606-20-2 2,6-Dinitrotoluene 0.48 U 4.8 0.48 ug/l
91-94-1 3,3'-Dichlorobenzidine 0.95 U 9.5 0.95 ug/l
53-70-3 Dibenzo(a,h)anthracene 0.50 U 4.8 0.50 ug/l
132-64-9 Dibenzofuran 0.48 U 4.8 0.48 ug/l
84-74-2 Di-n-butyl phthalate 0.83 U 4.8 0.83 ug/l
117-84-0 Di-n-octyl phthalate 1.0 U 4.8 1.0 ug/l
84-66-2 Diethyl phthalate 1.0 U 4.8 1.0 ug/l
131-11-3 Dimethyl phthalate 0.94 U 4.8 0.94 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate 1.0 U 4.8 1.0 ug/l
206-44-0 Fluoranthene 0.48 U 4.8 0.48 ug/l
86-73-7 Fluorene 0.48 U 4.8 0.48 ug/l
118-74-1 Hexachlorobenzene 0.53 U 4.8 0.53 ug/l
87-68-3 Hexachlorobutadiene 0.95 U 4.8 0.95 ug/l
77-47-4 Hexachlorocyclopentadiene 1.8 U 9.5 1.8 ug/l
67-72-1 Hexachloroethane 0.95 U 4.8 0.95 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene 0.48 U 4.8 0.48 ug/l
78-59-1 Isophorone 0.48 U 4.8 0.48 ug/l
91-57-6 2-Methylnaphthalene 0.54 U 4.8 0.54 ug/l
88-74-4 2-Nitroaniline 0.48 U 4.8 0.48 ug/l
99-09-2 3-Nitroaniline 0.48 U 4.8 0.48 ug/l
100-01-6 4-Nitroaniline 0.48 U 4.8 0.48 ug/l
91-20-3 Naphthalene 0.76 U 4.8 0.76 ug/l
98-95-3 Nitrobenzene 0.56 U 4.8 0.56 ug/l
621-64-7 N-Nitroso-di-n-propylamine 0.48 U 4.8 0.48 ug/l
86-30-6 N-Nitrosodiphenylamine 0.95 U 4.8 0.95 ug/l
85-01-8 Phenanthrene 0.48 U 4.8 0.48 ug/l
129-00-0 Pyrene 0.48 U 4.8 0.48 ug/l
120-82-1 1,2,4-Trichlorobenzene 0.48 U 4.8 0.48 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 32%14-62%
4165-62-2 Phenol-d5 25%10-40%
118-79-6 2,4,6-Tribromophenol 74%33-118%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-1
Lab Sample ID:F82004-1 Date Sampled:05/02/11
Matrix:AQ - Ground Water Date Received:05/03/11
Method:SW846 8270D SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 71%42-108%
321-60-8 2-Fluorobiphenyl 72%40-106%
1718-51-0 Terphenyl-d14 68%39-121%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:F82004-1 Date Sampled:05/02/11
Matrix:AQ - Ground Water Date Received:05/03/11
Method:SW846 8015C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CD104924.D 1 05/06/11 MM n/a n/a GCD4290
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)0.105 0.10 0.050 mg/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 70%57-129%
98-08-8 aaa-Trifluorotoluene 81%58-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:F82004-1 Date Sampled:05/02/11
Matrix:AQ - Ground Water Date Received:05/03/11
Method:SW846 8015C SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40361.D 1 05/05/11 SJL 05/04/11 OP37019 GZF1663
Run #2
Initial Volume Final Volume
Run #1 1040 ml 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)0.096 U 0.24 0.096 mg/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 84%42-114%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:F82004-1 Date Sampled:05/02/11
Matrix:AQ - Ground Water Date Received:05/03/11
Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Total Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Antimony 2.0 U 6.0 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Arsenic 2.0 U 10 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Barium 111 J 200 5.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Beryllium 1.0 U 4.0 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Cadmium 1.0 U 5.0 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Chromium 63.3 10 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Copper 30.7 25 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Lead 1.0 U 5.0 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Mercury 0.050 U 1.0 0.050 ug/l 1 05/05/11 05/05/11 LM SW846 7470A 1 SW846 7470A 4
Molybdenum 2.0 U 50 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Nickel 23.6 J 40 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Selenium 2.0 U 10 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Silver 1.0 U 10 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Tin 1.0 U 50 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Zinc 38.8 20 5.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
(1) Instrument QC Batch: MA8924
(2) Instrument QC Batch: MA8925
(3) Prep QC Batch: MP20503
(4) Prep QC Batch: MP20507
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:F82004-1F Date Sampled:05/02/11
Matrix:AQ - Groundwater Filtered Date Received:05/03/11
Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Dissolved Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Antimony 2.0 U 6.0 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Arsenic 2.0 U 10 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Barium 26.5 J 200 5.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Beryllium 1.0 U 4.0 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Cadmium 1.0 U 5.0 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Chromium 1.4 J 10 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Copper 2.0 U 25 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Lead 1.0 U 5.0 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Mercury 0.050 U 1.0 0.050 ug/l 1 05/05/11 05/05/11 LM SW846 7470A 1 SW846 7470A 4
Molybdenum 2.0 U 50 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Nickel 2.0 U 40 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Selenium 2.0 U 10 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Silver 1.0 U 10 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Tin 1.0 U 50 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Zinc 9.5 J 20 5.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
(1) Instrument QC Batch: MA8924
(2) Instrument QC Batch: MA8925
(3) Prep QC Batch: MP20503
(4) Prep QC Batch: MP20507
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:F82004-2 Date Sampled:05/02/11
Matrix:AQ - Ground Water Date Received:05/03/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 J065526.D 1 05/13/11 MM n/a n/a VJ3586
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.20 U 1.0 0.20 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.20 U 1.0 0.20 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.76 1.0 0.22 ug/l J
75-15-0 Carbon disulfide 0.50 U 2.0 0.50 ug/l
56-23-5 Carbon tetrachloride 1.4 1.0 0.25 ug/l
75-34-3 1,1-Dichloroethane 0.25 U 1.0 0.25 ug/l
75-35-4 1,1-Dichloroethylene 0.23 U 1.0 0.23 ug/l
107-06-2 1,2-Dichloroethane 0.20 U 1.0 0.20 ug/l
78-87-5 1,2-Dichloropropane 0.25 U 1.0 0.25 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.26 U 1.0 0.26 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.35 U 1.0 0.35 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
100-41-4 Ethylbenzene 0.20 U 1.0 0.20 ug/l
591-78-6 2-Hexanone 4.0 U 10 4.0 ug/l
108-10-1 4-Methyl-2-pentanone 2.0 U 5.0 2.0 ug/l
74-83-9 Methyl bromide 0.50 U 2.0 0.50 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 2.0 U 5.0 2.0 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.23 U 1.0 0.23 ug/l
79-00-5 1,1,2-Trichloroethane 0.22 U 1.0 0.22 ug/l
127-18-4 Tetrachloroethylene 0.25 U 1.0 0.25 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 0.77 1.0 0.26 ug/l J
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:F82004-2 Date Sampled:05/02/11
Matrix:AQ - Ground Water Date Received:05/03/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.22 U 1.0 0.22 ug/l
1330-20-7 Xylene (total)0.52 U 3.0 0.52 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%87-116%
17060-07-0 1,2-Dichloroethane-D4 101%76-127%
2037-26-5 Toluene-D8 103%86-112%
460-00-4 4-Bromofluorobenzene 113%84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-2
Lab Sample ID:F82004-2 Date Sampled:05/02/11
Matrix:AQ - Ground Water Date Received:05/03/11
Method:SW846 8270D SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L051240.D 1 05/06/11 NAF 05/04/11 OP37011 SL2614
Run #2
Initial Volume Final Volume
Run #1 1020 ml 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid 9.8 U 49 9.8 ug/l
95-57-8 2-Chlorophenol 0.49 U 4.9 0.49 ug/l
59-50-7 4-Chloro-3-methyl phenol 0.49 U 4.9 0.49 ug/l
120-83-2 2,4-Dichlorophenol 0.49 U 4.9 0.49 ug/l
105-67-9 2,4-Dimethylphenol 1.1 U 4.9 1.1 ug/l
51-28-5 2,4-Dinitrophenol 9.8 U 25 9.8 ug/l
534-52-1 4,6-Dinitro-o-cresol 2.0 U 9.8 2.0 ug/l
95-48-7 2-Methylphenol 0.53 U 4.9 0.53 ug/l
3&4-Methylphenol 1.1 U 4.9 1.1 ug/l
88-75-5 2-Nitrophenol 0.53 U 4.9 0.53 ug/l
100-02-7 4-Nitrophenol 4.9 U 25 4.9 ug/l
87-86-5 Pentachlorophenol 5.3 U 25 5.3 ug/l
108-95-2 Phenol 0.49 U 4.9 0.49 ug/l
95-95-4 2,4,5-Trichlorophenol 0.49 U 4.9 0.49 ug/l
88-06-2 2,4,6-Trichlorophenol 0.49 U 4.9 0.49 ug/l
83-32-9 Acenaphthene 0.49 U 4.9 0.49 ug/l
208-96-8 Acenaphthylene 0.49 U 4.9 0.49 ug/l
120-12-7 Anthracene 0.49 U 4.9 0.49 ug/l
56-55-3 Benzo(a)anthracene 0.49 U 4.9 0.49 ug/l
50-32-8 Benzo(a)pyrene 0.49 U 4.9 0.49 ug/l
205-99-2 Benzo(b)fluoranthene 0.49 U 4.9 0.49 ug/l
191-24-2 Benzo(g,h,i)perylene 0.49 U 4.9 0.49 ug/l
207-08-9 Benzo(k)fluoranthene 0.49 U 4.9 0.49 ug/l
101-55-3 4-Bromophenyl phenyl ether 0.49 U 4.9 0.49 ug/l
85-68-7 Butyl benzyl phthalate 1.1 U 4.9 1.1 ug/l
100-51-6 Benzyl Alcohol 0.98 U 4.9 0.98 ug/l
91-58-7 2-Chloronaphthalene 0.49 U 4.9 0.49 ug/l
106-47-8 4-Chloroaniline 0.49 U 4.9 0.49 ug/l
86-74-8 Carbazole 0.49 U 4.9 0.49 ug/l
218-01-9 Chrysene 0.49 U 4.9 0.49 ug/l
111-91-1 bis(2-Chloroethoxy)methane 0.49 U 4.9 0.49 ug/l
111-44-4 bis(2-Chloroethyl)ether 0.53 U 4.9 0.53 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-2
Lab Sample ID:F82004-2 Date Sampled:05/02/11
Matrix:AQ - Ground Water Date Received:05/03/11
Method:SW846 8270D SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether 0.53 U 4.9 0.53 ug/l
7005-72-3 4-Chlorophenyl phenyl ether 0.49 U 4.9 0.49 ug/l
95-50-1 1,2-Dichlorobenzene 0.98 U 4.9 0.98 ug/l
541-73-1 1,3-Dichlorobenzene 0.98 U 4.9 0.98 ug/l
106-46-7 1,4-Dichlorobenzene 0.98 U 4.9 0.98 ug/l
121-14-2 2,4-Dinitrotoluene 0.49 U 4.9 0.49 ug/l
606-20-2 2,6-Dinitrotoluene 0.49 U 4.9 0.49 ug/l
91-94-1 3,3'-Dichlorobenzidine 0.98 U 9.8 0.98 ug/l
53-70-3 Dibenzo(a,h)anthracene 0.51 U 4.9 0.51 ug/l
132-64-9 Dibenzofuran 0.49 U 4.9 0.49 ug/l
84-74-2 Di-n-butyl phthalate 0.85 U 4.9 0.85 ug/l
117-84-0 Di-n-octyl phthalate 1.1 U 4.9 1.1 ug/l
84-66-2 Diethyl phthalate 1.1 U 4.9 1.1 ug/l
131-11-3 Dimethyl phthalate 0.97 U 4.9 0.97 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate 1.1 U 4.9 1.1 ug/l
206-44-0 Fluoranthene 0.49 U 4.9 0.49 ug/l
86-73-7 Fluorene 0.49 U 4.9 0.49 ug/l
118-74-1 Hexachlorobenzene 0.55 U 4.9 0.55 ug/l
87-68-3 Hexachlorobutadiene 0.98 U 4.9 0.98 ug/l
77-47-4 Hexachlorocyclopentadiene 1.9 U 9.8 1.9 ug/l
67-72-1 Hexachloroethane 0.98 U 4.9 0.98 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene 0.49 U 4.9 0.49 ug/l
78-59-1 Isophorone 0.49 U 4.9 0.49 ug/l
91-57-6 2-Methylnaphthalene 0.56 U 4.9 0.56 ug/l
88-74-4 2-Nitroaniline 0.49 U 4.9 0.49 ug/l
99-09-2 3-Nitroaniline 0.49 U 4.9 0.49 ug/l
100-01-6 4-Nitroaniline 0.49 U 4.9 0.49 ug/l
91-20-3 Naphthalene 0.78 U 4.9 0.78 ug/l
98-95-3 Nitrobenzene 0.58 U 4.9 0.58 ug/l
621-64-7 N-Nitroso-di-n-propylamine 0.49 U 4.9 0.49 ug/l
86-30-6 N-Nitrosodiphenylamine 0.98 U 4.9 0.98 ug/l
85-01-8 Phenanthrene 0.49 U 4.9 0.49 ug/l
129-00-0 Pyrene 0.49 U 4.9 0.49 ug/l
120-82-1 1,2,4-Trichlorobenzene 0.49 U 4.9 0.49 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 45%14-62%
4165-62-2 Phenol-d5 35%10-40%
118-79-6 2,4,6-Tribromophenol 85%33-118%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-2
Lab Sample ID:F82004-2 Date Sampled:05/02/11
Matrix:AQ - Ground Water Date Received:05/03/11
Method:SW846 8270D SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 81%42-108%
321-60-8 2-Fluorobiphenyl 79%40-106%
1718-51-0 Terphenyl-d14 74%39-121%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-2
Lab Sample ID:F82004-2 Date Sampled:05/02/11
Matrix:AQ - Ground Water Date Received:05/03/11
Method:SW846 8015C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CD104925.D 1 05/06/11 MM n/a n/a GCD4290
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)0.050 U 0.10 0.050 mg/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 63%57-129%
98-08-8 aaa-Trifluorotoluene 71%58-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-2
Lab Sample ID:F82004-2 Date Sampled:05/02/11
Matrix:AQ - Ground Water Date Received:05/03/11
Method:SW846 8015C SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40367.D 1 05/06/11 SJL 05/04/11 OP37019 GZF1663
Run #2
Initial Volume Final Volume
Run #1 1040 ml 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)0.096 U 0.24 0.096 mg/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 86%42-114%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-2
Lab Sample ID:F82004-2 Date Sampled:05/02/11
Matrix:AQ - Ground Water Date Received:05/03/11
Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Total Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Antimony 2.0 U 6.0 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Arsenic 2.0 U 10 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Barium 36.2 J 200 5.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Beryllium 1.0 U 4.0 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Cadmium 1.0 U 5.0 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Chromium 5.0 J 10 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Copper 4.4 J 25 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Lead 1.0 U 5.0 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Mercury 0.050 U 1.0 0.050 ug/l 1 05/05/11 05/05/11 LM SW846 7470A 1 SW846 7470A 4
Molybdenum 2.0 U 50 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Nickel 4.4 J 40 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Selenium 2.0 U 10 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Silver 1.0 U 10 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Tin 1.0 U 50 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Zinc 18.2 J 20 5.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
(1) Instrument QC Batch: MA8924
(2) Instrument QC Batch: MA8925
(3) Prep QC Batch: MP20503
(4) Prep QC Batch: MP20507
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Report of Analysis Page 1 of 1
Client Sample ID:MW-2
Lab Sample ID:F82004-2F Date Sampled:05/02/11
Matrix:AQ - Groundwater Filtered Date Received:05/03/11
Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Dissolved Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Antimony 2.0 U 6.0 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Arsenic 2.0 U 10 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Barium 30.0 J 200 5.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Beryllium 1.0 U 4.0 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Cadmium 1.0 U 5.0 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Chromium 1.4 J 10 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Copper 2.0 U 25 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Lead 1.0 U 5.0 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Mercury 0.050 U 1.0 0.050 ug/l 1 05/05/11 05/05/11 LM SW846 7470A 1 SW846 7470A 4
Molybdenum 2.0 U 50 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Nickel 2.8 J 40 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Selenium 2.0 U 10 2.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Silver 1.0 U 10 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Tin 1.0 U 50 1.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
Zinc 16.4 J 20 5.0 ug/l 1 05/05/11 05/05/11 DM SW846 6010C 2 SW846 3010A 3
(1) Instrument QC Batch: MA8924
(2) Instrument QC Batch: MA8925
(3) Prep QC Batch: MP20503
(4) Prep QC Batch: MP20507
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Certification Exceptions
• Certification Exceptions (NC)
• Chain of Custody
Southeast
Section 4
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02/16/12
Technical Report for
AMEC Environment & Infrastructure, Inc.
GE-TFS; 1906 Bancroft St, Charlotte, NC
572260702
Accutest Job Number: F82038
Sampling Date: 05/03/11
Report to:
AMEC Earth & Environmental
steven.tanen@amec.com
ATTN: Steve Tanen
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), AK, AR, GA, KY, MA, NV, OK, UT, VA, WA, WI
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Conference
and/or state specific certification programs as applicable.
Client Service contact: Heather Wandrey 407-425-6700
Harry Behzadi, Ph.D.
Laboratory Director
Southeast
02/16/12
Reissue #1
e-Hardcopy 2.0
Automated Report
39
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
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F82038
Florida 4405 Vineland Road Suite C-15 Orlando, FL 32811 tel: 407 425-6700 fax: 407 425-0707 htpp://www.accutest.com www.accutest.com
August 2, 2011
Mr. Steven Tanen
AMEC Earth & Environmental
502 W. Germantown Pike
Suite 850
Plymouth Meeting, PA 19462
RE: Accutest job F82038 Reissue
Dear Mr. Tanen,
The final report for job number F82038 has been edited to reflect requested corrections.
These edits have been incorporated into the revised report.
All data reported to the MDL.
Accutest apologies for any inconvenience this may have caused. Please feel free to contact
us if we can be of further assistance.
Sincerely,
Accutest Laboratories, SE
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Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................4
Section 2: Case Narrative/Conformance Summary ..............................................................5
Section 3: Sample Results ........................................................................................................7
3.1: F82038-1: MW-3 ..........................................................................................................8
3.2: F82038-1F: MW-3 ........................................................................................................16
3.3: F82038-2: MW-4 ..........................................................................................................17
3.4: F82038-2F: MW-4 ........................................................................................................25
3.5: F82038-3: MW-5 ..........................................................................................................26
3.6: F82038-3F: MW-5 ........................................................................................................34
3.7: F82038-4: TB-05/03/11 ................................................................................................35
Section 4: Misc. Forms ............................................................................................................37
4.1: Chain of Custody ...........................................................................................................38
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Sample Summary
AMEC Environment & Infrastructure, Inc.
Job No:F82038
GE-TFS; 1906 Bancroft St, Charlotte, NC
Project No: 572260702
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
F82038-1 05/03/11 08:25 BE 05/04/11 AQ Ground Water MW-3
F82038-1F 05/03/11 08:25 BE 05/04/11 AQ Groundwater Filtered MW-3
F82038-2 05/03/11 10:50 BE 05/04/11 AQ Ground Water MW-4
F82038-2F 05/03/11 10:50 BE 05/04/11 AQ Groundwater Filtered MW-4
F82038-3 05/03/11 12:35 BE 05/04/11 AQ Ground Water MW-5
F82038-3F 05/03/11 12:35 BE 05/04/11 AQ Groundwater Filtered MW-5
F82038-4 05/03/11 00:00 BE 05/04/11 AQ Trip Blank Water TB-05/03/11
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SAMPLE DELIVERY GROUP CASE NARRATIVE
Client: AMEC Earth & Environmental Job F82038
Site: GE-TFS; 1906 Bancroft St, Charlotte, NC Report Date: 5/24/2011 8:18:06 AM
3 Samples and 1 Trip Blank were collected on 05/03/2011 and were received at Accutest SE on 05/04/2011 properly preserved, at
3.6 Deg. C and intact. These Samples received an Accutest job number of F82038. A listing of the Laboratory Sample ID, Client
Sample ID and dates of collection are presented in the Results Summary Section of this report.
Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For more
information, please refer to QC summary pages.
Volatiles by GCMS by Method SW846 8260B Matrix: AQ Batch ID: VN2080
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F82007-3MS, F82007-3MSD were used as the QC samples indicated.
Matrix Spike Recovery for Bromodichloromethane is outside control limits. Probable cause due to matrix interference.
Matrix Spike Duplicate Recovery for cis-1,2-Dichloroethylene are outside control limits. Probable cause due to matrix interference.
RPD for MSD for trans-1,2-Dichloroethylene is outside control limits for sample F82007-3MSD. Probable cause due to sample non-homogeneity.
Extractables by GCMS by Method SW846 8270D Matrix: AQ Batch ID: OP37028
All samples were extracted within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F82057-2MS, F82057-2MSD were used as the QC samples indicated.
Matrix Spike Recoverys for 3,3’-Dichlorobenzidine, 4-Nitrophenol, Benzoic Acid are outside control limits. Probable cause due to matrix interference.
Matrix Spike Duplicate Recoverys for 3,3’-Dichlorobenzidine, 4-Nitrophenol, Benzoic Acid, Hexachlorocyclopentadiene are outside control limits. Probable cause due to matrix interference.
Samples OP37028-MS, OP37028-MSD have surrogates outside control limits. Probable cause due to matrix interference.
Volatiles by GC by Method SW846 8015C Matrix: AQ Batch ID: GCD4290
F82038-1: Confirmation run.
F82038-1 for 4-Bromofluorobenzene: Outside control limits.
Matrix: AQ Batch ID: GCD4298
All samples were analyzed within the recommended method holding time.
Samples F82143-14MS, F82143-14MSD were used as the QC samples indicated.
All method blanks for this batch meet method specific criteria.
Sample F82038-1 has surrogates outside control limits. Probable cause due to matrix interference.
Tuesday, May 24, 2011
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Extractables by GC by Method SW846 8015C Matrix: AQ Batch ID: OP37059
All samples were extracted within the recommended method holding time.
All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria.
Samples F82034-3MS, F82034-3MSD were used as the QC samples indicated.
Metals by Method SW846 6010C Matrix: AQ Batch ID: MP20513
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F82007-3FDUP, F82007-3FMS, F82007-3FMSD, F82007-3FPS, F82007-3FSDL were used as the QC samples for metals.
RPD for Serial Dilution for Zinc is outside control limits for sample MP20513-SD1. Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
Matrix: AQ Batch ID: MP20514
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F82034-1MS, F82034-1MSD, F82034-1PS, F82034-1SDL, F82034-1DUP were used as the QC samples for metals.
RPD for Duplicate for Lead is outside control limits for sample MP20514-D1. RPD acceptable due to low duplicate and sample concentrations.
RPDs for Serial Dilution for Chromium, Copper, Nickel are outside control limits for sample MP20514-SD1. Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
Metals by Method SW846 7470A Matrix: AQ Batch ID: MP20529
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F82038-1DUP, F82038-1MS, F82038-1MSD, F82038-1SDL were used as the QC samples for metals.
Matrix: AQ Batch ID: MP20548
All samples were digested within the recommended method holding time. All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F82034-3MS, F82034-3MSD, F82034-3SDL, F82034-3DUP were used as the QC samples for metals.
RPD for Duplicate for Mercury is outside control limits for sample MP20548-D1. RPD acceptable due to low duplicate and sample concentrations.
RPD for Serial Dilution for Mercury is outside control limits for sample MP20548-SD1. Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
Accutest Laboratories Southeast (ALSE) certifies that this report meets the project requirements for analytical data produced for the
samples as received at ALSE and as stated on the COC. ALSE certifies that the data meets the Data Quality Objectives for precision,
accuracy and completeness as specified in the ALSE Quality Manual except as noted above. This report is to be used in its entirety.
ALSE is not responsible for any assumptions of data quality if partial data packages are used.
Narrative prepared by:
_______________________________________ Date: May 24, 2011
Ellen Pampel, Inorganic QA (signature on file)
Tuesday, May 24, 2011
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Sample Results
Report of Analysis
Southeast
Section 3
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Report of Analysis Page 1 of 2
Client Sample ID:MW-3
Lab Sample ID:F82038-1 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 N0051141.D 1 05/16/11 NMC n/a n/a VN2080
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.20 U 1.0 0.20 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.20 U 1.0 0.20 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.22 U 1.0 0.22 ug/l
75-15-0 Carbon disulfide 0.50 U 2.0 0.50 ug/l
56-23-5 Carbon tetrachloride 0.25 U 1.0 0.25 ug/l
75-34-3 1,1-Dichloroethane 0.25 U 1.0 0.25 ug/l
75-35-4 1,1-Dichloroethylene 0.23 U 1.0 0.23 ug/l
107-06-2 1,2-Dichloroethane 0.20 U 1.0 0.20 ug/l
78-87-5 1,2-Dichloropropane 0.25 U 1.0 0.25 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.26 U 1.0 0.26 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.35 U 1.0 0.35 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
100-41-4 Ethylbenzene 0.20 U 1.0 0.20 ug/l
591-78-6 2-Hexanone 4.0 U 10 4.0 ug/l
108-10-1 4-Methyl-2-pentanone 2.0 U 5.0 2.0 ug/l
74-83-9 Methyl bromide 0.50 U 2.0 0.50 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 2.0 U 5.0 2.0 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.23 U 1.0 0.23 ug/l
79-00-5 1,1,2-Trichloroethane 0.22 U 1.0 0.22 ug/l
127-18-4 Tetrachloroethylene 0.25 U 1.0 0.25 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 0.26 U 1.0 0.26 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-3
Lab Sample ID:F82038-1 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.22 U 1.0 0.22 ug/l
1330-20-7 Xylene (total)0.52 U 3.0 0.52 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 111%87-116%
17060-07-0 1,2-Dichloroethane-D4 108%76-127%
2037-26-5 Toluene-D8 90%86-112%
460-00-4 4-Bromofluorobenzene 101%84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-3
Lab Sample ID:F82038-1 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8270D SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025282.D 1 05/06/11 NAF 05/05/11 OP37028 SU1214
Run #2
Initial Volume Final Volume
Run #1 1040 ml 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid 9.6 U 48 9.6 ug/l
95-57-8 2-Chlorophenol 0.48 U 4.8 0.48 ug/l
59-50-7 4-Chloro-3-methyl phenol 0.48 U 4.8 0.48 ug/l
120-83-2 2,4-Dichlorophenol 0.48 U 4.8 0.48 ug/l
105-67-9 2,4-Dimethylphenol 1.1 U 4.8 1.1 ug/l
51-28-5 2,4-Dinitrophenol 9.6 U 24 9.6 ug/l
534-52-1 4,6-Dinitro-o-cresol 1.9 U 9.6 1.9 ug/l
95-48-7 2-Methylphenol 0.52 U 4.8 0.52 ug/l
3&4-Methylphenol 1.1 U 4.8 1.1 ug/l
88-75-5 2-Nitrophenol 0.52 U 4.8 0.52 ug/l
100-02-7 4-Nitrophenol 4.8 U 24 4.8 ug/l
87-86-5 Pentachlorophenol 5.2 U 24 5.2 ug/l
108-95-2 Phenol 0.48 U 4.8 0.48 ug/l
95-95-4 2,4,5-Trichlorophenol 0.48 U 4.8 0.48 ug/l
88-06-2 2,4,6-Trichlorophenol 0.48 U 4.8 0.48 ug/l
83-32-9 Acenaphthene 0.48 U 4.8 0.48 ug/l
208-96-8 Acenaphthylene 0.48 U 4.8 0.48 ug/l
120-12-7 Anthracene 0.48 U 4.8 0.48 ug/l
56-55-3 Benzo(a)anthracene 0.48 U 4.8 0.48 ug/l
50-32-8 Benzo(a)pyrene 0.48 U 4.8 0.48 ug/l
205-99-2 Benzo(b)fluoranthene 0.48 U 4.8 0.48 ug/l
191-24-2 Benzo(g,h,i)perylene 0.48 U 4.8 0.48 ug/l
207-08-9 Benzo(k)fluoranthene 0.48 U 4.8 0.48 ug/l
101-55-3 4-Bromophenyl phenyl ether 0.48 U 4.8 0.48 ug/l
85-68-7 Butyl benzyl phthalate 1.1 U 4.8 1.1 ug/l
100-51-6 Benzyl Alcohol 0.96 U 4.8 0.96 ug/l
91-58-7 2-Chloronaphthalene 0.48 U 4.8 0.48 ug/l
106-47-8 4-Chloroaniline 0.48 U 4.8 0.48 ug/l
86-74-8 Carbazole 0.48 U 4.8 0.48 ug/l
218-01-9 Chrysene 0.48 U 4.8 0.48 ug/l
111-91-1 bis(2-Chloroethoxy)methane 0.48 U 4.8 0.48 ug/l
111-44-4 bis(2-Chloroethyl)ether 0.52 U 4.8 0.52 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-3
Lab Sample ID:F82038-1 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8270D SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether 0.52 U 4.8 0.52 ug/l
7005-72-3 4-Chlorophenyl phenyl ether 0.48 U 4.8 0.48 ug/l
95-50-1 1,2-Dichlorobenzene 0.96 U 4.8 0.96 ug/l
541-73-1 1,3-Dichlorobenzene 0.96 U 4.8 0.96 ug/l
106-46-7 1,4-Dichlorobenzene 0.96 U 4.8 0.96 ug/l
121-14-2 2,4-Dinitrotoluene 0.48 U 4.8 0.48 ug/l
606-20-2 2,6-Dinitrotoluene 0.48 U 4.8 0.48 ug/l
91-94-1 3,3'-Dichlorobenzidine 0.96 U 9.6 0.96 ug/l
53-70-3 Dibenzo(a,h)anthracene 0.50 U 4.8 0.50 ug/l
132-64-9 Dibenzofuran 0.48 U 4.8 0.48 ug/l
84-74-2 Di-n-butyl phthalate 0.84 U 4.8 0.84 ug/l
117-84-0 Di-n-octyl phthalate 1.1 U 4.8 1.1 ug/l
84-66-2 Diethyl phthalate 1.1 U 4.8 1.1 ug/l
131-11-3 Dimethyl phthalate 0.95 U 4.8 0.95 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate 1.1 U 4.8 1.1 ug/l
206-44-0 Fluoranthene 0.48 U 4.8 0.48 ug/l
86-73-7 Fluorene 0.48 U 4.8 0.48 ug/l
118-74-1 Hexachlorobenzene 0.54 U 4.8 0.54 ug/l
87-68-3 Hexachlorobutadiene 0.96 U 4.8 0.96 ug/l
77-47-4 Hexachlorocyclopentadiene 1.8 U 9.6 1.8 ug/l
67-72-1 Hexachloroethane 0.96 U 4.8 0.96 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene 0.48 U 4.8 0.48 ug/l
78-59-1 Isophorone 0.48 U 4.8 0.48 ug/l
91-57-6 2-Methylnaphthalene 0.55 U 4.8 0.55 ug/l
88-74-4 2-Nitroaniline 0.48 U 4.8 0.48 ug/l
99-09-2 3-Nitroaniline 0.48 U 4.8 0.48 ug/l
100-01-6 4-Nitroaniline 0.48 U 4.8 0.48 ug/l
91-20-3 Naphthalene 0.77 U 4.8 0.77 ug/l
98-95-3 Nitrobenzene 0.57 U 4.8 0.57 ug/l
621-64-7 N-Nitroso-di-n-propylamine 0.48 U 4.8 0.48 ug/l
86-30-6 N-Nitrosodiphenylamine 0.96 U 4.8 0.96 ug/l
85-01-8 Phenanthrene 0.48 U 4.8 0.48 ug/l
129-00-0 Pyrene 0.48 U 4.8 0.48 ug/l
120-82-1 1,2,4-Trichlorobenzene 0.48 U 4.8 0.48 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 40%14-62%
4165-62-2 Phenol-d5 27%10-40%
118-79-6 2,4,6-Tribromophenol 85%33-118%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-3
Lab Sample ID:F82038-1 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8270D SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 73%42-108%
321-60-8 2-Fluorobiphenyl 74%40-106%
1718-51-0 Terphenyl-d14 83%39-121%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-3
Lab Sample ID:F82038-1 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8015C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CD105090.D 1 05/12/11 MM n/a n/a GCD4298
Run #2 a CD104913.D 1 05/06/11 MM n/a n/a GCD4290
Purge Volume
Run #1 5.0 ml
Run #2 5.0 ml
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)0.050 U 0.10 0.050 mg/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 69%56% b 57-129%
98-08-8 aaa-Trifluorotoluene 75%70%58-120%
(a) Confirmation run.
(b) Outside control limits.
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-3
Lab Sample ID:F82038-1 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8015C SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40428.D 1 05/09/11 SJL 05/07/11 OP37059 GZF1665
Run #2
Initial Volume Final Volume
Run #1 1040 ml 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)0.096 U 0.24 0.096 mg/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 84%42-114%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-3
Lab Sample ID:F82038-1 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Total Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Antimony 2.0 U 6.0 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Arsenic 2.0 U 10 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Barium 41.3 J 200 5.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Beryllium 1.0 U 4.0 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Cadmium 1.0 U 5.0 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Chromium 7.7 J 10 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Copper 8.5 J 25 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Lead 1.8 J 5.0 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Mercury 0.050 U 1.0 0.050 ug/l 1 05/09/11 05/09/11 LM SW846 7470A 2 SW846 7470A 4
Molybdenum 2.0 U 50 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Nickel 6.5 J 40 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Selenium 2.0 U 10 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Silver 1.0 U 10 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Tin 1.0 U 50 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Zinc 28.5 20 5.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
(1) Instrument QC Batch: MA8929
(2) Instrument QC Batch: MA8931
(3) Prep QC Batch: MP20514
(4) Prep QC Batch: MP20529
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Report of Analysis Page 1 of 1
Client Sample ID:MW-3
Lab Sample ID:F82038-1F Date Sampled:05/03/11
Matrix:AQ - Groundwater Filtered Date Received:05/04/11
Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Dissolved Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Antimony 2.0 U 6.0 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Arsenic 2.0 U 10 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Barium 34.8 J 200 5.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Beryllium 1.0 U 4.0 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Cadmium 1.0 U 5.0 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Chromium 1.9 J 10 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Copper 6.0 J 25 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Lead 1.0 U 5.0 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Mercury 0.070 J 1.0 0.050 ug/l 1 05/11/11 05/11/11 LM SW846 7470A 2 SW846 7470A 4
Molybdenum 2.0 U 50 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Nickel 2.9 J 40 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Selenium 2.0 U 10 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Silver 1.0 U 10 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Tin 1.0 U 50 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Zinc 22.0 20 5.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
(1) Instrument QC Batch: MA8929
(2) Instrument QC Batch: MA8939
(3) Prep QC Batch: MP20513
(4) Prep QC Batch: MP20548
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Report of Analysis Page 1 of 2
Client Sample ID:MW-4
Lab Sample ID:F82038-2 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 N0051142.D 1 05/16/11 NMC n/a n/a VN2080
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.20 U 1.0 0.20 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.20 U 1.0 0.20 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.22 U 1.0 0.22 ug/l
75-15-0 Carbon disulfide 0.50 U 2.0 0.50 ug/l
56-23-5 Carbon tetrachloride 0.25 U 1.0 0.25 ug/l
75-34-3 1,1-Dichloroethane 0.25 U 1.0 0.25 ug/l
75-35-4 1,1-Dichloroethylene 0.23 U 1.0 0.23 ug/l
107-06-2 1,2-Dichloroethane 0.20 U 1.0 0.20 ug/l
78-87-5 1,2-Dichloropropane 0.25 U 1.0 0.25 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.26 U 1.0 0.26 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.35 U 1.0 0.35 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
100-41-4 Ethylbenzene 0.20 U 1.0 0.20 ug/l
591-78-6 2-Hexanone 4.0 U 10 4.0 ug/l
108-10-1 4-Methyl-2-pentanone 2.0 U 5.0 2.0 ug/l
74-83-9 Methyl bromide 0.50 U 2.0 0.50 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 2.0 U 5.0 2.0 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.23 U 1.0 0.23 ug/l
79-00-5 1,1,2-Trichloroethane 0.22 U 1.0 0.22 ug/l
127-18-4 Tetrachloroethylene 0.25 U 1.0 0.25 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 0.26 U 1.0 0.26 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-4
Lab Sample ID:F82038-2 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.22 U 1.0 0.22 ug/l
1330-20-7 Xylene (total)0.52 U 3.0 0.52 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 111%87-116%
17060-07-0 1,2-Dichloroethane-D4 109%76-127%
2037-26-5 Toluene-D8 89%86-112%
460-00-4 4-Bromofluorobenzene 100%84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-4
Lab Sample ID:F82038-2 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8270D SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025283.D 1 05/06/11 NAF 05/05/11 OP37028 SU1214
Run #2
Initial Volume Final Volume
Run #1 1040 ml 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid 9.6 U 48 9.6 ug/l
95-57-8 2-Chlorophenol 0.48 U 4.8 0.48 ug/l
59-50-7 4-Chloro-3-methyl phenol 0.48 U 4.8 0.48 ug/l
120-83-2 2,4-Dichlorophenol 0.48 U 4.8 0.48 ug/l
105-67-9 2,4-Dimethylphenol 1.1 U 4.8 1.1 ug/l
51-28-5 2,4-Dinitrophenol 9.6 U 24 9.6 ug/l
534-52-1 4,6-Dinitro-o-cresol 1.9 U 9.6 1.9 ug/l
95-48-7 2-Methylphenol 0.52 U 4.8 0.52 ug/l
3&4-Methylphenol 1.1 U 4.8 1.1 ug/l
88-75-5 2-Nitrophenol 0.52 U 4.8 0.52 ug/l
100-02-7 4-Nitrophenol 4.8 U 24 4.8 ug/l
87-86-5 Pentachlorophenol 5.2 U 24 5.2 ug/l
108-95-2 Phenol 0.48 U 4.8 0.48 ug/l
95-95-4 2,4,5-Trichlorophenol 0.48 U 4.8 0.48 ug/l
88-06-2 2,4,6-Trichlorophenol 0.48 U 4.8 0.48 ug/l
83-32-9 Acenaphthene 0.48 U 4.8 0.48 ug/l
208-96-8 Acenaphthylene 0.48 U 4.8 0.48 ug/l
120-12-7 Anthracene 0.48 U 4.8 0.48 ug/l
56-55-3 Benzo(a)anthracene 0.48 U 4.8 0.48 ug/l
50-32-8 Benzo(a)pyrene 0.48 U 4.8 0.48 ug/l
205-99-2 Benzo(b)fluoranthene 0.48 U 4.8 0.48 ug/l
191-24-2 Benzo(g,h,i)perylene 0.48 U 4.8 0.48 ug/l
207-08-9 Benzo(k)fluoranthene 0.48 U 4.8 0.48 ug/l
101-55-3 4-Bromophenyl phenyl ether 0.48 U 4.8 0.48 ug/l
85-68-7 Butyl benzyl phthalate 1.1 U 4.8 1.1 ug/l
100-51-6 Benzyl Alcohol 0.96 U 4.8 0.96 ug/l
91-58-7 2-Chloronaphthalene 0.48 U 4.8 0.48 ug/l
106-47-8 4-Chloroaniline 0.48 U 4.8 0.48 ug/l
86-74-8 Carbazole 0.48 U 4.8 0.48 ug/l
218-01-9 Chrysene 0.48 U 4.8 0.48 ug/l
111-91-1 bis(2-Chloroethoxy)methane 0.48 U 4.8 0.48 ug/l
111-44-4 bis(2-Chloroethyl)ether 0.52 U 4.8 0.52 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:MW-4
Lab Sample ID:F82038-2 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8270D SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether 0.52 U 4.8 0.52 ug/l
7005-72-3 4-Chlorophenyl phenyl ether 0.48 U 4.8 0.48 ug/l
95-50-1 1,2-Dichlorobenzene 0.96 U 4.8 0.96 ug/l
541-73-1 1,3-Dichlorobenzene 0.96 U 4.8 0.96 ug/l
106-46-7 1,4-Dichlorobenzene 0.96 U 4.8 0.96 ug/l
121-14-2 2,4-Dinitrotoluene 0.48 U 4.8 0.48 ug/l
606-20-2 2,6-Dinitrotoluene 0.48 U 4.8 0.48 ug/l
91-94-1 3,3'-Dichlorobenzidine 0.96 U 9.6 0.96 ug/l
53-70-3 Dibenzo(a,h)anthracene 0.50 U 4.8 0.50 ug/l
132-64-9 Dibenzofuran 0.48 U 4.8 0.48 ug/l
84-74-2 Di-n-butyl phthalate 0.84 U 4.8 0.84 ug/l
117-84-0 Di-n-octyl phthalate 1.1 U 4.8 1.1 ug/l
84-66-2 Diethyl phthalate 1.1 U 4.8 1.1 ug/l
131-11-3 Dimethyl phthalate 0.95 U 4.8 0.95 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate 1.1 U 4.8 1.1 ug/l
206-44-0 Fluoranthene 0.48 U 4.8 0.48 ug/l
86-73-7 Fluorene 0.48 U 4.8 0.48 ug/l
118-74-1 Hexachlorobenzene 0.54 U 4.8 0.54 ug/l
87-68-3 Hexachlorobutadiene 0.96 U 4.8 0.96 ug/l
77-47-4 Hexachlorocyclopentadiene 1.8 U 9.6 1.8 ug/l
67-72-1 Hexachloroethane 0.96 U 4.8 0.96 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene 0.48 U 4.8 0.48 ug/l
78-59-1 Isophorone 0.48 U 4.8 0.48 ug/l
91-57-6 2-Methylnaphthalene 0.55 U 4.8 0.55 ug/l
88-74-4 2-Nitroaniline 0.48 U 4.8 0.48 ug/l
99-09-2 3-Nitroaniline 0.48 U 4.8 0.48 ug/l
100-01-6 4-Nitroaniline 0.48 U 4.8 0.48 ug/l
91-20-3 Naphthalene 0.77 U 4.8 0.77 ug/l
98-95-3 Nitrobenzene 0.57 U 4.8 0.57 ug/l
621-64-7 N-Nitroso-di-n-propylamine 0.48 U 4.8 0.48 ug/l
86-30-6 N-Nitrosodiphenylamine 0.96 U 4.8 0.96 ug/l
85-01-8 Phenanthrene 0.48 U 4.8 0.48 ug/l
129-00-0 Pyrene 0.48 U 4.8 0.48 ug/l
120-82-1 1,2,4-Trichlorobenzene 0.48 U 4.8 0.48 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 42%14-62%
4165-62-2 Phenol-d5 28%10-40%
118-79-6 2,4,6-Tribromophenol 73%33-118%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-4
Lab Sample ID:F82038-2 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8270D SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 69%42-108%
321-60-8 2-Fluorobiphenyl 70%40-106%
1718-51-0 Terphenyl-d14 75%39-121%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-4
Lab Sample ID:F82038-2 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8015C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CD105091.D 1 05/12/11 MM n/a n/a GCD4298
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)0.050 U 0.10 0.050 mg/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 68%57-129%
98-08-8 aaa-Trifluorotoluene 77%58-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-4
Lab Sample ID:F82038-2 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8015C SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40429.D 1 05/09/11 SJL 05/07/11 OP37059 GZF1665
Run #2
Initial Volume Final Volume
Run #1 1040 ml 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)0.096 U 0.24 0.096 mg/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 85%42-114%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-4
Lab Sample ID:F82038-2 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Total Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Antimony 2.0 U 6.0 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Arsenic 2.0 U 10 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Barium 55.1 J 200 5.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Beryllium 1.0 U 4.0 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Cadmium 1.0 U 5.0 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Chromium 3.6 J 10 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Copper 8.8 J 25 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Lead 2.4 J 5.0 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Mercury 0.050 U 1.0 0.050 ug/l 1 05/11/11 05/11/11 LM SW846 7470A 2 SW846 7470A 4
Molybdenum 2.0 U 50 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Nickel 2.2 J 40 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Selenium 3.5 J 10 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Silver 1.0 U 10 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Tin 1.0 U 50 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Zinc 18.3 J 20 5.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
(1) Instrument QC Batch: MA8929
(2) Instrument QC Batch: MA8939
(3) Prep QC Batch: MP20514
(4) Prep QC Batch: MP20548
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Client Sample ID:MW-4
Lab Sample ID:F82038-2F Date Sampled:05/03/11
Matrix:AQ - Groundwater Filtered Date Received:05/04/11
Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Dissolved Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Antimony 2.0 U 6.0 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Arsenic 2.0 U 10 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Barium 38.9 J 200 5.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Beryllium 1.0 U 4.0 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Cadmium 1.0 U 5.0 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Chromium 1.0 U 10 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Copper 2.0 U 25 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Lead 1.0 U 5.0 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Mercury 0.050 J 1.0 0.050 ug/l 1 05/11/11 05/11/11 LM SW846 7470A 2 SW846 7470A 4
Molybdenum 2.0 U 50 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Nickel 2.0 U 40 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Selenium 2.0 U 10 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Silver 1.0 U 10 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Tin 1.0 U 50 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Zinc 9.4 J 20 5.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
(1) Instrument QC Batch: MA8929
(2) Instrument QC Batch: MA8939
(3) Prep QC Batch: MP20513
(4) Prep QC Batch: MP20548
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Report of Analysis Page 1 of 2
Client Sample ID:MW-5
Lab Sample ID:F82038-3 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 N0051143.D 1 05/16/11 NMC n/a n/a VN2080
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.20 U 1.0 0.20 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.20 U 1.0 0.20 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.22 U 1.0 0.22 ug/l
75-15-0 Carbon disulfide 0.50 U 2.0 0.50 ug/l
56-23-5 Carbon tetrachloride 0.25 U 1.0 0.25 ug/l
75-34-3 1,1-Dichloroethane 0.25 U 1.0 0.25 ug/l
75-35-4 1,1-Dichloroethylene 0.23 U 1.0 0.23 ug/l
107-06-2 1,2-Dichloroethane 0.20 U 1.0 0.20 ug/l
78-87-5 1,2-Dichloropropane 0.25 U 1.0 0.25 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.26 U 1.0 0.26 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.35 U 1.0 0.35 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
100-41-4 Ethylbenzene 0.20 U 1.0 0.20 ug/l
591-78-6 2-Hexanone 4.0 U 10 4.0 ug/l
108-10-1 4-Methyl-2-pentanone 2.0 U 5.0 2.0 ug/l
74-83-9 Methyl bromide 0.50 U 2.0 0.50 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 2.0 U 5.0 2.0 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.23 U 1.0 0.23 ug/l
79-00-5 1,1,2-Trichloroethane 0.22 U 1.0 0.22 ug/l
127-18-4 Tetrachloroethylene 0.29 1.0 0.25 ug/l J
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 0.26 U 1.0 0.26 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-5
Lab Sample ID:F82038-3 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.22 U 1.0 0.22 ug/l
1330-20-7 Xylene (total)0.52 U 3.0 0.52 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 112%87-116%
17060-07-0 1,2-Dichloroethane-D4 110%76-127%
2037-26-5 Toluene-D8 89%86-112%
460-00-4 4-Bromofluorobenzene 102%84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:MW-5
Lab Sample ID:F82038-3 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8270D SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 U025284.D 1 05/06/11 NAF 05/05/11 OP37028 SU1214
Run #2
Initial Volume Final Volume
Run #1 1020 ml 1.0 ml
Run #2
ABN TCL List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid 9.8 U 49 9.8 ug/l
95-57-8 2-Chlorophenol 0.49 U 4.9 0.49 ug/l
59-50-7 4-Chloro-3-methyl phenol 0.49 U 4.9 0.49 ug/l
120-83-2 2,4-Dichlorophenol 0.49 U 4.9 0.49 ug/l
105-67-9 2,4-Dimethylphenol 1.1 U 4.9 1.1 ug/l
51-28-5 2,4-Dinitrophenol 9.8 U 25 9.8 ug/l
534-52-1 4,6-Dinitro-o-cresol 2.0 U 9.8 2.0 ug/l
95-48-7 2-Methylphenol 0.53 U 4.9 0.53 ug/l
3&4-Methylphenol 1.1 U 4.9 1.1 ug/l
88-75-5 2-Nitrophenol 0.53 U 4.9 0.53 ug/l
100-02-7 4-Nitrophenol 4.9 U 25 4.9 ug/l
87-86-5 Pentachlorophenol 5.3 U 25 5.3 ug/l
108-95-2 Phenol 0.49 U 4.9 0.49 ug/l
95-95-4 2,4,5-Trichlorophenol 0.49 U 4.9 0.49 ug/l
88-06-2 2,4,6-Trichlorophenol 0.49 U 4.9 0.49 ug/l
83-32-9 Acenaphthene 0.49 U 4.9 0.49 ug/l
208-96-8 Acenaphthylene 0.49 U 4.9 0.49 ug/l
120-12-7 Anthracene 0.49 U 4.9 0.49 ug/l
56-55-3 Benzo(a)anthracene 0.49 U 4.9 0.49 ug/l
50-32-8 Benzo(a)pyrene 0.49 U 4.9 0.49 ug/l
205-99-2 Benzo(b)fluoranthene 0.49 U 4.9 0.49 ug/l
191-24-2 Benzo(g,h,i)perylene 0.49 U 4.9 0.49 ug/l
207-08-9 Benzo(k)fluoranthene 0.49 U 4.9 0.49 ug/l
101-55-3 4-Bromophenyl phenyl ether 0.49 U 4.9 0.49 ug/l
85-68-7 Butyl benzyl phthalate 1.1 U 4.9 1.1 ug/l
100-51-6 Benzyl Alcohol 0.98 U 4.9 0.98 ug/l
91-58-7 2-Chloronaphthalene 0.49 U 4.9 0.49 ug/l
106-47-8 4-Chloroaniline 0.49 U 4.9 0.49 ug/l
86-74-8 Carbazole 0.49 U 4.9 0.49 ug/l
218-01-9 Chrysene 0.49 U 4.9 0.49 ug/l
111-91-1 bis(2-Chloroethoxy)methane 0.49 U 4.9 0.49 ug/l
111-44-4 bis(2-Chloroethyl)ether 0.53 U 4.9 0.53 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-5
Lab Sample ID:F82038-3 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8270D SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Compound Result RL MDL Units Q
108-60-1 bis(2-Chloroisopropyl)ether 0.53 U 4.9 0.53 ug/l
7005-72-3 4-Chlorophenyl phenyl ether 0.49 U 4.9 0.49 ug/l
95-50-1 1,2-Dichlorobenzene 0.98 U 4.9 0.98 ug/l
541-73-1 1,3-Dichlorobenzene 0.98 U 4.9 0.98 ug/l
106-46-7 1,4-Dichlorobenzene 0.98 U 4.9 0.98 ug/l
121-14-2 2,4-Dinitrotoluene 0.49 U 4.9 0.49 ug/l
606-20-2 2,6-Dinitrotoluene 0.49 U 4.9 0.49 ug/l
91-94-1 3,3'-Dichlorobenzidine 0.98 U 9.8 0.98 ug/l
53-70-3 Dibenzo(a,h)anthracene 0.51 U 4.9 0.51 ug/l
132-64-9 Dibenzofuran 0.49 U 4.9 0.49 ug/l
84-74-2 Di-n-butyl phthalate 0.85 U 4.9 0.85 ug/l
117-84-0 Di-n-octyl phthalate 1.1 U 4.9 1.1 ug/l
84-66-2 Diethyl phthalate 1.1 U 4.9 1.1 ug/l
131-11-3 Dimethyl phthalate 0.97 U 4.9 0.97 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate 1.1 U 4.9 1.1 ug/l
206-44-0 Fluoranthene 0.49 U 4.9 0.49 ug/l
86-73-7 Fluorene 0.49 U 4.9 0.49 ug/l
118-74-1 Hexachlorobenzene 0.55 U 4.9 0.55 ug/l
87-68-3 Hexachlorobutadiene 0.98 U 4.9 0.98 ug/l
77-47-4 Hexachlorocyclopentadiene 1.9 U 9.8 1.9 ug/l
67-72-1 Hexachloroethane 0.98 U 4.9 0.98 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene 0.49 U 4.9 0.49 ug/l
78-59-1 Isophorone 0.49 U 4.9 0.49 ug/l
91-57-6 2-Methylnaphthalene 0.56 U 4.9 0.56 ug/l
88-74-4 2-Nitroaniline 0.49 U 4.9 0.49 ug/l
99-09-2 3-Nitroaniline 0.49 U 4.9 0.49 ug/l
100-01-6 4-Nitroaniline 0.49 U 4.9 0.49 ug/l
91-20-3 Naphthalene 0.78 U 4.9 0.78 ug/l
98-95-3 Nitrobenzene 0.58 U 4.9 0.58 ug/l
621-64-7 N-Nitroso-di-n-propylamine 0.49 U 4.9 0.49 ug/l
86-30-6 N-Nitrosodiphenylamine 0.98 U 4.9 0.98 ug/l
85-01-8 Phenanthrene 0.49 U 4.9 0.49 ug/l
129-00-0 Pyrene 0.49 U 4.9 0.49 ug/l
120-82-1 1,2,4-Trichlorobenzene 0.49 U 4.9 0.49 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 38%14-62%
4165-62-2 Phenol-d5 26%10-40%
118-79-6 2,4,6-Tribromophenol 71%33-118%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-5
Lab Sample ID:F82038-3 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8270D SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
ABN TCL List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
4165-60-0 Nitrobenzene-d5 64%42-108%
321-60-8 2-Fluorobiphenyl 66%40-106%
1718-51-0 Terphenyl-d14 78%39-121%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-5
Lab Sample ID:F82038-3 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8015C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CD105092.D 1 05/12/11 MM n/a n/a GCD4298
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)0.050 U 0.10 0.050 mg/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 66%57-129%
98-08-8 aaa-Trifluorotoluene 79%58-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-5
Lab Sample ID:F82038-3 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Method:SW846 8015C SW846 3510C Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZF40430.D 1 05/09/11 SJL 05/07/11 OP37059 GZF1665
Run #2
Initial Volume Final Volume
Run #1 1050 ml 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)0.095 U 0.24 0.095 mg/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 78%42-114%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-5
Lab Sample ID:F82038-3 Date Sampled:05/03/11
Matrix:AQ - Ground Water Date Received:05/04/11
Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Total Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Antimony 2.0 U 6.0 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Arsenic 2.0 U 10 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Barium 146 J 200 5.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Beryllium 1.0 U 4.0 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Cadmium 1.0 U 5.0 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Chromium 93.8 10 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Copper 36.6 25 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Lead 6.4 5.0 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Mercury 0.11 J 1.0 0.050 ug/l 1 05/11/11 05/11/11 LM SW846 7470A 2 SW846 7470A 4
Molybdenum 2.0 U 50 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Nickel 31.3 J 40 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Selenium 2.6 J 10 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Silver 1.0 U 10 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Tin 1.0 U 50 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Zinc 80.1 20 5.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
(1) Instrument QC Batch: MA8929
(2) Instrument QC Batch: MA8939
(3) Prep QC Batch: MP20514
(4) Prep QC Batch: MP20548
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Client Sample ID:MW-5
Lab Sample ID:F82038-3F Date Sampled:05/03/11
Matrix:AQ - Groundwater Filtered Date Received:05/04/11
Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Dissolved Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Antimony 2.0 U 6.0 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Arsenic 2.0 U 10 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Barium 56.7 J 200 5.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Beryllium 1.0 U 4.0 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Cadmium 1.0 U 5.0 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Chromium 34.0 10 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Copper 2.0 U 25 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Lead 1.0 U 5.0 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Mercury 0.050 U 1.0 0.050 ug/l 1 05/11/11 05/11/11 LM SW846 7470A 2 SW846 7470A 4
Molybdenum 2.0 U 50 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Nickel 2.4 J 40 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Selenium 2.0 U 10 2.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Silver 1.0 U 10 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Tin 1.0 U 50 1.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
Zinc 14.7 J 20 5.0 ug/l 1 05/06/11 05/06/11 RS SW846 6010C 1 SW846 3010A 3
(1) Instrument QC Batch: MA8929
(2) Instrument QC Batch: MA8939
(3) Prep QC Batch: MP20513
(4) Prep QC Batch: MP20548
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Client Sample ID:TB-05/03/11
Lab Sample ID:F82038-4 Date Sampled:05/03/11
Matrix:AQ - Trip Blank Water Date Received:05/04/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 N0051144.D 1 05/16/11 NMC n/a n/a VN2080
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.20 U 1.0 0.20 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.20 U 1.0 0.20 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.22 U 1.0 0.22 ug/l
75-15-0 Carbon disulfide 0.50 U 2.0 0.50 ug/l
56-23-5 Carbon tetrachloride 0.25 U 1.0 0.25 ug/l
75-34-3 1,1-Dichloroethane 0.25 U 1.0 0.25 ug/l
75-35-4 1,1-Dichloroethylene 0.23 U 1.0 0.23 ug/l
107-06-2 1,2-Dichloroethane 0.20 U 1.0 0.20 ug/l
78-87-5 1,2-Dichloropropane 0.25 U 1.0 0.25 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.26 U 1.0 0.26 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.35 U 1.0 0.35 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
100-41-4 Ethylbenzene 0.20 U 1.0 0.20 ug/l
591-78-6 2-Hexanone 4.0 U 10 4.0 ug/l
108-10-1 4-Methyl-2-pentanone 2.0 U 5.0 2.0 ug/l
74-83-9 Methyl bromide 0.50 U 2.0 0.50 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 2.0 U 5.0 2.0 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.23 U 1.0 0.23 ug/l
79-00-5 1,1,2-Trichloroethane 0.22 U 1.0 0.22 ug/l
127-18-4 Tetrachloroethylene 0.25 U 1.0 0.25 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 0.26 U 1.0 0.26 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:TB-05/03/11
Lab Sample ID:F82038-4 Date Sampled:05/03/11
Matrix:AQ - Trip Blank Water Date Received:05/04/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.22 U 1.0 0.22 ug/l
1330-20-7 Xylene (total)0.52 U 3.0 0.52 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 113%87-116%
17060-07-0 1,2-Dichloroethane-D4 112%76-127%
2037-26-5 Toluene-D8 89%86-112%
460-00-4 4-Bromofluorobenzene 103%84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Certification Exceptions
• Certification Exceptions (NC)
• Chain of Custody
Southeast
Section 4
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F82038: Chain of Custody
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F82038: Chain of Custody
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02/16/12
Technical Report for
AMEC Environment & Infrastructure, Inc.
GE-TFS; 1906 Bancroft St, Charlotte, NC
572260702
Accutest Job Number: F83247
Sampling Date: 06/09/11
Report to:
AMEC Earth & Environmental
steven.tanen@amec.com
ATTN: Steve Tanen
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), AK, AR, GA, KY, MA, NV, OK, UT, VA, WA, WI
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Conference
and/or state specific certification programs as applicable.
Client Service contact: Heather Wandrey 407-425-6700
Harry Behzadi, Ph.D.
Laboratory Director
Southeast
02/16/12
e-Hardcopy 2.0
Automated Report
24
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
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Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Case Narrative/Conformance Summary ..............................................................4
Section 3: Sample Results ........................................................................................................6
3.1: F83247-1: MW-3A/1.5-2 ..............................................................................................7
3.2: F83247-2: MW-3A/11-12 .............................................................................................9
3.3: F83247-3: B6-A/1-2 .....................................................................................................11
3.4: F83247-4: B6-A/10.5-11.5 ...........................................................................................13
3.5: F83247-5: B2-A/0.5-2 ..................................................................................................15
3.6: F83247-6: B2-A/11-12 .................................................................................................17
3.7: F83247-7: MW-5A/0.5-2 ..............................................................................................19
Section 4: Misc. Forms ............................................................................................................21
4.1: Chain of Custody ...........................................................................................................22
1
2
3
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Sample Summary
AMEC Environment & Infrastructure, Inc.
Job No:F83247
GE-TFS; 1906 Bancroft St, Charlotte, NC
Project No: 572260702
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
F83247-1 06/09/11 13:20 AKTH 06/10/11 SO Soil MW-3A/1.5-2
F83247-2 06/09/11 13:20 AKTH 06/10/11 SO Soil MW-3A/11-12
F83247-3 06/09/11 12:55 AKTH 06/10/11 SO Soil B6-A/1-2
F83247-4 06/09/11 12:55 AKTH 06/10/11 SO Soil B6-A/10.5-11.5
F83247-5 06/09/11 13:15 AKTH 06/10/11 SO Soil B2-A/0.5-2
F83247-6 06/09/11 13:15 AKTH 06/10/11 SO Soil B2-A/11-12
F83247-7 06/09/11 10:10 AKTH 06/10/11 SO Soil MW-5A/0.5-2
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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SAMPLE DELIVERY GROUP CASE NARRATIVE
Client: AMEC Earth & Environmental Job F83247
Site: GE-TFS; 1906 Bancroft St, Charlotte, NC Report Date: 7/2/2011 8:30:37 AM
7 Samples were collected on 06/09/2011 and were received at Accutest SE on 06/10/2011 properly preserved, at 4.6 Deg. C and
intact. These Samples received an Accutest job number of F83247. A listing of the Laboratory Sample ID, Client Sample ID and
dates of collection are presented in the Results Summary Section of this report.
Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For more
information, please refer to QC summary pages.
Metals by Method SW846 6010C Matrix: SO Batch ID: MP20817
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F83179-1MS, F83179-1MSD, F83179-1PS, F83179-1SDL, F83179-1DUP were used as the QC samples for metals.
RPD for Duplicate for Chromium is outside control limits for sample MP20817-D1. RPD acceptable due to low duplicate and sample concentrations.
F83247-6 for Chromium: Elevated reporting limit(s) due to matrix interference. F83247-5 for Chromium: Elevated reporting limit(s) due to matrix interference.
F83247-3 for Chromium: Elevated reporting limit(s) due to matrix interference.
F83247-2 for Chromium: Elevated reporting limit(s) due to matrix interference. F83247-1 for Chromium: Elevated reporting limit(s) due to matrix interference.
F83247-7 for Chromium: Elevated reporting limit(s) due to matrix interference.
Wet Chemistry by Method SM19 2540G Matrix: SO Batch ID: GN45034
Sample F83269-1DUP was used as the QC sample for Solids, Percent.
Wet Chemistry by Method SW846 3060/7196A M
Matrix: SO Batch ID: R25317
F83247-4 for Chromium, Trivalent: Calculated as: (Chromium) - (Chromium, Hexavalent)
Matrix: SO Batch ID: R25320
F83247-2 for Chromium, Trivalent: Calculated as: (Chromium) - (Chromium, Hexavalent)
Matrix: SO Batch ID: R25321
F83247-1 for Chromium, Trivalent: Calculated as: (Chromium) - (Chromium, Hexavalent)
Matrix: SO Batch ID: R25322
F83247-7 for Chromium, Trivalent: Calculated as: (Chromium) - (Chromium, Hexavalent)
Matrix: SO Batch ID: R25323
F83247-6 for Chromium, Trivalent: Calculated as: (Chromium) - (Chromium, Hexavalent)
Matrix: SO Batch ID: R25324
F83247-5 for Chromium, Trivalent: Calculated as: (Chromium) - (Chromium, Hexavalent)
Matrix: SO Batch ID: R25325
F83247-3 for Chromium, Trivalent: Calculated as: (Chromium) - (Chromium, Hexavalent)
Saturday, July 02, 2011
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Wet Chemistry by Method SW846 3060A/7196A Matrix: SO Batch ID: GN45080
All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria.
Samples F83247-1DUP, F83247-1MS were used as the QC samples for Chromium, Hexavalent.
Matrix Spike Recovery for Chromium, Hexavalent is outside control limits. Spike recovery indicates possible matrix interference and/or sample nonhomogeneity.
RPD for Duplicate for Chromium, Hexavalent is outside control limits for sample GN45080-D1. RPD acceptable due to low duplicate and sample concentrations.
Accutest Laboratories Southeast (ALSE) certifies that this report meets the project requirements for analytical data produced for the
samples as received at ALSE and as stated on the COC. ALSE certifies that the data meets the Data Quality Objectives for precision,
accuracy and completeness as specified in the ALSE Quality Manual except as noted above. This report is to be used in its entirety.
ALSE is not responsible for any assumptions of data quality if partial data packages are used.
Narrative prepared by:
_______________________________________ Date: July 2, 2011
Ellen Pampel, Inorganic QA (signature on file)
Saturday, July 02, 2011
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Sample Results
Report of Analysis
Southeast
Section 3
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Report of Analysis Page 1 of 1
Client Sample ID:MW-3A/1.5-2
Lab Sample ID:F83247-1 Date Sampled:06/09/11
Matrix:SO - Soil Date Received:06/10/11
Percent Solids:69.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Chromium a 30.3 2.7 mg/kg 5 06/20/11 06/21/11 RS SW846 6010C 1 SW846 3050B 2
Selenium a <5.4 5.4 mg/kg 5 06/20/11 06/21/11 RS SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA9037
(2) Prep QC Batch: MP20817
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Report of Analysis Page 1 of 1
Client Sample ID:MW-3A/1.5-2
Lab Sample ID:F83247-1 Date Sampled:06/09/11
Matrix:SO - Soil Date Received:06/10/11
Percent Solids:69.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chromium, Hexavalent <2.9 2.9 mg/kg 1 06/20/11 CC SW846 3060A/7196A
Chromium, Trivalent a 28.8 5.6 mg/kg 1 06/21/11 13:51 RS SW846 3060/7196A M
Solids, Percent 69.6 %1 06/16/11 AJC SM19 2540G
(a) Calculated as: (Chromium) - (Chromium, Hexavalent)
RL = Reporting Limit
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Report of Analysis Page 1 of 1
Client Sample ID:MW-3A/11-12
Lab Sample ID:F83247-2 Date Sampled:06/09/11
Matrix:SO - Soil Date Received:06/10/11
Percent Solids:66.2
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Chromium a 34.2 3.1 mg/kg 5 06/20/11 06/21/11 RS SW846 6010C 1 SW846 3050B 2
Selenium a <6.1 6.1 mg/kg 5 06/20/11 06/21/11 RS SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA9037
(2) Prep QC Batch: MP20817
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Report of Analysis Page 1 of 1
Client Sample ID:MW-3A/11-12
Lab Sample ID:F83247-2 Date Sampled:06/09/11
Matrix:SO - Soil Date Received:06/10/11
Percent Solids:66.2
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chromium, Hexavalent <3.0 3.0 mg/kg 1 06/20/11 CC SW846 3060A/7196A
Chromium, Trivalent a 34.2 6.1 mg/kg 1 06/21/11 13:55 RS SW846 3060/7196A M
Solids, Percent 66.2 %1 06/16/11 AJC SM19 2540G
(a) Calculated as: (Chromium) - (Chromium, Hexavalent)
RL = Reporting Limit
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Report of Analysis Page 1 of 1
Client Sample ID:B6-A/1-2
Lab Sample ID:F83247-3 Date Sampled:06/09/11
Matrix:SO - Soil Date Received:06/10/11
Percent Solids:81.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Chromium a 31.2 0.83 mg/kg 2 06/20/11 06/21/11 RS SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA9037
(2) Prep QC Batch: MP20817
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Report of Analysis Page 1 of 1
Client Sample ID:B6-A/1-2
Lab Sample ID:F83247-3 Date Sampled:06/09/11
Matrix:SO - Soil Date Received:06/10/11
Percent Solids:81.9
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chromium, Hexavalent <2.4 2.4 mg/kg 1 06/20/11 CC SW846 3060A/7196A
Chromium, Trivalent a 31.2 3.2 mg/kg 1 06/21/11 14:00 RS SW846 3060/7196A M
Solids, Percent 81.9 %1 06/16/11 AJC SM19 2540G
(a) Calculated as: (Chromium) - (Chromium, Hexavalent)
RL = Reporting Limit
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Report of Analysis Page 1 of 1
Client Sample ID:B6-A/10.5-11.5
Lab Sample ID:F83247-4 Date Sampled:06/09/11
Matrix:SO - Soil Date Received:06/10/11
Percent Solids:82.3
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Chromium 20.1 0.46 mg/kg 1 06/20/11 06/21/11 RS SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA9036
(2) Prep QC Batch: MP20817
RL = Reporting Limit
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Report of Analysis Page 1 of 1
Client Sample ID:B6-A/10.5-11.5
Lab Sample ID:F83247-4 Date Sampled:06/09/11
Matrix:SO - Soil Date Received:06/10/11
Percent Solids:82.3
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chromium, Hexavalent <2.4 2.4 mg/kg 1 06/20/11 CC SW846 3060A/7196A
Chromium, Trivalent a 20.1 2.9 mg/kg 1 06/21/11 01:47 RS SW846 3060/7196A M
Solids, Percent 82.3 %1 06/16/11 AJC SM19 2540G
(a) Calculated as: (Chromium) - (Chromium, Hexavalent)
RL = Reporting Limit
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Report of Analysis Page 1 of 1
Client Sample ID:B2-A/0.5-2
Lab Sample ID:F83247-5 Date Sampled:06/09/11
Matrix:SO - Soil Date Received:06/10/11
Percent Solids:70.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Chromium a 94.2 1.2 mg/kg 2 06/20/11 06/21/11 RS SW846 6010C 1 SW846 3050B 2
Selenium a <2.4 2.4 mg/kg 2 06/20/11 06/21/11 RS SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA9037
(2) Prep QC Batch: MP20817
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Report of Analysis Page 1 of 1
Client Sample ID:B2-A/0.5-2
Lab Sample ID:F83247-5 Date Sampled:06/09/11
Matrix:SO - Soil Date Received:06/10/11
Percent Solids:70.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chromium, Hexavalent <2.8 2.8 mg/kg 1 06/20/11 CC SW846 3060A/7196A
Chromium, Trivalent a 94.2 4.0 mg/kg 1 06/21/11 14:04 RS SW846 3060/7196A M
Solids, Percent 70.6 %1 06/16/11 AJC SM19 2540G
(a) Calculated as: (Chromium) - (Chromium, Hexavalent)
RL = Reporting Limit
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Report of Analysis Page 1 of 1
Client Sample ID:B2-A/11-12
Lab Sample ID:F83247-6 Date Sampled:06/09/11
Matrix:SO - Soil Date Received:06/10/11
Percent Solids:73.8
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Chromium a 99.5 5.7 mg/kg 10 06/20/11 06/21/11 RS SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA9037
(2) Prep QC Batch: MP20817
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Report of Analysis Page 1 of 1
Client Sample ID:B2-A/11-12
Lab Sample ID:F83247-6 Date Sampled:06/09/11
Matrix:SO - Soil Date Received:06/10/11
Percent Solids:73.8
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chromium, Hexavalent <2.7 2.7 mg/kg 1 06/20/11 CC SW846 3060A/7196A
Chromium, Trivalent a 99.5 8.4 mg/kg 1 06/21/11 14:08 RS SW846 3060/7196A M
Solids, Percent 73.8 %1 06/16/11 AJC SM19 2540G
(a) Calculated as: (Chromium) - (Chromium, Hexavalent)
RL = Reporting Limit
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Report of Analysis Page 1 of 1
Client Sample ID:MW-5A/0.5-2
Lab Sample ID:F83247-7 Date Sampled:06/09/11
Matrix:SO - Soil Date Received:06/10/11
Percent Solids:84.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Chromium a 50.5 1.0 mg/kg 2 06/20/11 06/21/11 RS SW846 6010C 1 SW846 3050B 2
Selenium a <2.0 2.0 mg/kg 2 06/20/11 06/21/11 RS SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA9037
(2) Prep QC Batch: MP20817
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
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Report of Analysis Page 1 of 1
Client Sample ID:MW-5A/0.5-2
Lab Sample ID:F83247-7 Date Sampled:06/09/11
Matrix:SO - Soil Date Received:06/10/11
Percent Solids:84.6
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chromium, Hexavalent <2.4 2.4 mg/kg 1 06/20/11 CC SW846 3060A/7196A
Chromium, Trivalent a 50.5 3.4 mg/kg 1 06/21/11 14:12 RS SW846 3060/7196A M
Solids, Percent 84.6 %1 06/16/11 AJC SM19 2540G
(a) Calculated as: (Chromium) - (Chromium, Hexavalent)
RL = Reporting Limit
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Certification Exceptions
• Certification Exceptions (NC)
• Chain of Custody
Southeast
Section 4
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F83247: Chain of Custody
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F83247: Chain of Custody
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02/16/12
Technical Report for
AMEC Environment & Infrastructure, Inc.
GE-TFS; 1906 Bancroft St, Charlotte, NC
572260702
Accutest Job Number: F83508
Sampling Date: 06/17/11
Report to:
AMEC Earth & Environmental
steven.tanen@amec.com
ATTN: Steve Tanen
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), AK, AR, GA, KY, MA, NV, OK, UT, VA, WA, WI
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Conference
and/or state specific certification programs as applicable.
Client Service contact: Heather Wandrey 407-425-6700
Harry Behzadi, Ph.D.
Laboratory Director
Southeast
02/16/12
Reissue #1
e-Hardcopy 2.0
Automated Report
13
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 13
F83508
Florida 4405 Vineland Road Suite C-15 Orlando, FL 32811 tel: 407 425-6700 fax: 407 425-0707 htpp://www.accutest.com www.accutest.com
August 2, 2011
Mr. Steven Tanen
AMEC Earth & Environmental
502 W. Germantown Pike
Suite 850
Plymouth Meeting, PA 19462
RE: Accutest job F83508 Reissue
Dear Mr. Tanen,
The final report for job number F83508 has been edited to reflect requested corrections.
These edits have been incorporated into the revised report.
All data reported to the MDL.
Accutest apologies for any inconvenience this may have caused. Please feel free to contact
us if we can be of further assistance.
Sincerely,
Accutest Laboratories, SE
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Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................4
Section 2: Case Narrative/Conformance Summary ..............................................................5
Section 3: Sample Results ........................................................................................................6
3.1: F83508-1: MW-1 ..........................................................................................................7
3.2: F83508-1F: MW-1 ........................................................................................................10
Section 4: Misc. Forms ............................................................................................................11
4.1: Chain of Custody ...........................................................................................................12
1
2
3
4
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Sample Summary
AMEC Environment & Infrastructure, Inc.
Job No:F83508
GE-TFS; 1906 Bancroft St, Charlotte, NC
Project No: 572260702
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
F83508-1 06/17/11 09:40 BE 06/18/11 AQ Ground Water MW-1
F83508-1F 06/17/11 09:40 BE 06/18/11 AQ Groundwater Filtered MW-1
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SAMPLE DELIVERY GROUP CASE NARRATIVE
Client: AMEC Earth & Environmental Job F83508
Site: GE-TFS; 1906 Bancroft St, Charlotte, NC Report Date: 7/6/2011 9:09:11 AM
1 Sample was collected on 06/17/2011 and was received at Accutest SE on 06/18/2011 properly preserved, at 2.4 Deg. C and
intact. The Sample received an Accutest job number of F83508. A listing of the Laboratory Sample ID, Client Sample ID and
dates of collection are presented in the Results Summary Section of this report.
Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For more
information, please refer to QC summary pages.
Volatiles by GCMS by Method SW846 8260B Matrix: AQ Batch ID: VB3155
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F83547-5MS, F83547-5MSD were used as the QC samples indicated.
F83508-1: Sample was not preserved to a pH < 2; reported results are considered minimum values.
F83508-1 for Methylene chloride: Suspected laboratory contaminant.
Metals by Method SW846 6010C
Matrix: AQ Batch ID: MP20838
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F83312-1DUP, F83312-1MS, F83312-1MSD, F83312-1PS, F83312-1SDL were used as the QC samples for metals.
Accutest Laboratories Southeast (ALSE) certifies that this report meets the project requirements for analytical data produced for the
samples as received at ALSE and as stated on the COC. ALSE certifies that the data meets the Data Quality Objectives for precision,
accuracy and completeness as specified in the ALSE Quality Manual except as noted above. This report is to be used in its entirety.
ALSE is not responsible for any assumptions of data quality if partial data packages are used.
Narrative prepared by:
_______________________________________ Date: July 6, 2011
Ellen Pampel, Inorganic QA (signature on file)
Wednesday, July 06, 2011
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Sample Results
Report of Analysis
Southeast
Section 3
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Report of Analysis Page 1 of 2
Client Sample ID:MW-1
Lab Sample ID:F83508-1 Date Sampled:06/17/11
Matrix:AQ - Ground Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a B076691.D 2 06/30/11 AJ n/a n/a VB3155
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 20 U 50 20 ug/l
71-43-2 Benzene 0.40 U 2.0 0.40 ug/l
75-27-4 Bromodichloromethane 0.40 U 2.0 0.40 ug/l
75-25-2 Bromoform 0.40 U 2.0 0.40 ug/l
108-90-7 Chlorobenzene 0.40 U 2.0 0.40 ug/l
75-00-3 Chloroethane 1.0 U 4.0 1.0 ug/l
67-66-3 Chloroform 0.93 2.0 0.44 ug/l J
75-15-0 Carbon disulfide 1.0 U 4.0 1.0 ug/l
56-23-5 Carbon tetrachloride 0.50 U 2.0 0.50 ug/l
75-34-3 1,1-Dichloroethane 0.97 2.0 0.50 ug/l J
75-35-4 1,1-Dichloroethylene 11.2 2.0 0.46 ug/l
107-06-2 1,2-Dichloroethane 0.40 U 2.0 0.40 ug/l
78-87-5 1,2-Dichloropropane 0.50 U 2.0 0.50 ug/l
124-48-1 Dibromochloromethane 0.40 U 2.0 0.40 ug/l
156-59-2 cis-1,2-Dichloroethylene 22.7 2.0 0.52 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.40 U 2.0 0.40 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.70 U 2.0 0.70 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.40 U 2.0 0.40 ug/l
100-41-4 Ethylbenzene 0.40 U 2.0 0.40 ug/l
591-78-6 2-Hexanone 8.0 U 20 8.0 ug/l
108-10-1 4-Methyl-2-pentanone 4.0 U 10 4.0 ug/l
74-83-9 Methyl bromide 1.0 U 4.0 1.0 ug/l
74-87-3 Methyl chloride 1.0 U 4.0 1.0 ug/l
75-09-2 Methylene chloride b 7.0 10 4.0 ug/l J
78-93-3 Methyl ethyl ketone 4.0 U 10 4.0 ug/l
100-42-5 Styrene 0.40 U 2.0 0.40 ug/l
71-55-6 1,1,1-Trichloroethane 0.40 U 2.0 0.40 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.46 U 2.0 0.46 ug/l
79-00-5 1,1,2-Trichloroethane 0.44 U 2.0 0.44 ug/l
127-18-4 Tetrachloroethylene 111 2.0 0.50 ug/l
108-88-3 Toluene 0.40 U 2.0 0.40 ug/l
79-01-6 Trichloroethylene 143 2.0 0.52 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-1
Lab Sample ID:F83508-1 Date Sampled:06/17/11
Matrix:AQ - Ground Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL List
CAS No.Compound Result RL MDL Units Q
75-01-4 Vinyl chloride 0.44 U 2.0 0.44 ug/l
1330-20-7 Xylene (total)1.0 U 6.0 1.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%87-116%
17060-07-0 1,2-Dichloroethane-D4 100%76-127%
2037-26-5 Toluene-D8 98%86-112%
460-00-4 4-Bromofluorobenzene 102%84-120%
(a) Sample was not preserved to a pH < 2; reported results are considered minimum values.
(b) Suspected laboratory contaminant.
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:F83508-1 Date Sampled:06/17/11
Matrix:AQ - Ground Water Date Received:06/18/11
Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Total Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Chromium 7.8 J 10 1.0 ug/l 1 06/22/11 06/22/11 DM SW846 6010C 1 SW846 3010A 2
(1) Instrument QC Batch: MA9044
(2) Prep QC Batch: MP20838
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:F83508-1F Date Sampled:06/17/11
Matrix:AQ - Groundwater Filtered Date Received:06/18/11
Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Dissolved Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Chromium 1.8 J 10 1.0 ug/l 1 06/22/11 06/22/11 DM SW846 6010C 1 SW846 3010A 2
(1) Instrument QC Batch: MA9044
(2) Prep QC Batch: MP20838
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Certification Exceptions
• Certification Exceptions (NC)
• Chain of Custody
Southeast
Section 4
11 of 13
F83508
4
F83508: Chain of Custody
Page 1 of 2
12 of 13
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4
4
.
1
F83508: Chain of Custody
Page 2 of 2
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1
02/16/12
Technical Report for
AMEC Environment & Infrastructure, Inc.
GE-TFS; 1906 Bancroft St, Charlotte, NC
572260702
Accutest Job Number: F83520
Sampling Date: 06/16/11
Report to:
AMEC Earth & Environmental
steven.tanen@amec.com
ATTN: Steve Tanen
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), AK, AR, GA, KY, MA, NV, OK, UT, VA, WA, WI
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Conference
and/or state specific certification programs as applicable.
Client Service contact: Heather Wandrey 407-425-6700
Harry Behzadi, Ph.D.
Laboratory Director
Southeast
02/16/12
Reissue #1
e-Hardcopy 2.0
Automated Report
30
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 30
F83520
Florida 4405 Vineland Road Suite C-15 Orlando, FL 32811 tel: 407 425-6700 fax: 407 425-0707 htpp://www.accutest.com www.accutest.com
August 2, 2011
Mr. Steven Tanen
AMEC Earth & Environmental
502 W. Germantown Pike
Suite 850
Plymouth Meeting, PA 19462
RE: Accutest job F83520 Reissue
Dear Mr. Tanen,
The final report for job number F83520 has been edited to reflect requested corrections.
These edits have been incorporated into the revised report.
All data reported to the MDL.
Accutest apologies for any inconvenience this may have caused. Please feel free to contact
us if we can be of further assistance.
Sincerely,
Accutest Laboratories, SE
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Table of Contents
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Sections:
Section 1: Sample Summary ...................................................................................................4
Section 2: Case Narrative/Conformance Summary ..............................................................5
Section 3: Sample Results ........................................................................................................6
3.1: F83520-1: TB-06/16/11 ................................................................................................7
3.2: F83520-2: MW-5 ..........................................................................................................9
3.3: F83520-2F: MW-5 ........................................................................................................12
3.4: F83520-3: MW-3 ..........................................................................................................13
3.5: F83520-4: MW-4 ..........................................................................................................15
3.6: F83520-5: MW-6 ..........................................................................................................17
3.7: F83520-6: MW-7 ..........................................................................................................19
3.8: F83520-7: MW-8 ..........................................................................................................21
3.9: F83520-8: MW-9 ..........................................................................................................23
3.10: F83520-9: MW-2 ........................................................................................................25
Section 4: Misc. Forms ............................................................................................................27
4.1: Certification Exceptions ................................................................................................28
4.2: Chain of Custody ...........................................................................................................29
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Sample Summary
AMEC Environment & Infrastructure, Inc.
Job No:F83520
GE-TFS; 1906 Bancroft St, Charlotte, NC
Project No: 572260702
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
F83520-1 06/16/11 00:00 BETH 06/18/11 AQ Trip Blank Water TB-06/16/11
F83520-2 06/16/11 11:05 BETH 06/18/11 AQ Ground Water MW-5
F83520-2F 06/16/11 11:05 BETH 06/18/11 AQ Groundwater Filtered MW-5
F83520-3 06/16/11 11:43 BETH 06/18/11 AQ Ground Water MW-3
F83520-4 06/16/11 13:10 BETH 06/18/11 AQ Ground Water MW-4
F83520-5 06/16/11 13:15 BETH 06/18/11 AQ Ground Water MW-6
F83520-6 06/16/11 15:11 BETH 06/18/11 AQ Ground Water MW-7
F83520-7 06/16/11 15:50 BETH 06/18/11 AQ Ground Water MW-8
F83520-8 06/16/11 16:53 BETH 06/18/11 AQ Ground Water MW-9
F83520-9 06/16/11 16:55 BETH 06/18/11 AQ Ground Water MW-2
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SAMPLE DELIVERY GROUP CASE NARRATIVE
Client: AMEC Earth & Environmental Job F83520
Site: GE-TFS; 1906 Bancroft St, Charlotte, NC Report Date: 7/6/2011 9:11:29 AM
8 Samples and 1 Trip Blank were collected on 06/16/2011 and were received at Accutest SE on 06/18/2011 properly preserved, at
2.6 Deg. C and intact. These Samples received an Accutest job number of F83520. A listing of the Laboratory Sample ID, Client
Sample ID and dates of collection are presented in the Results Summary Section of this report.
Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For more
information, please refer to QC summary pages.
Volatiles by GCMS by Method SW846 8260B Matrix: AQ Batch ID: VJ3632
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F83513-1MS, F83513-1MSD were used as the QC samples indicated.
Matrix Spike Duplicate Recoverys for 1,2-Dichloroethane, Bromochloromethane, Bromodichloromethane, Bromoform, Carbon disulfide, cis-1,3-Dichloropropene, Dibromochloromethane, trans-1,3-Dichloropropene are outside control limits. Probable cause due to matrix interference.
RPDs for MSD for 1,1,2-Trichloroethane, 1,1-Dichloroethane, 1,2-Dibromoethane, 1,2-Dichloroethane, 1,2-Dichloropropane, Benzene, Bromochloromethane, Bromodichloromethane, Bromoform, Carbon disulfide, Carbon tetrachloride, Chlorobenzene, Chloroform, cis-1,2-Dichloroethylene, cis-1,3-Dichloropropene, Dibromochloromethane, m-Dichlorobenzene, Methyl Tert Butyl Ether, Methylene chloride, o-Dichlorobenzene, p-Dichlorobenzene, Styrene, trans-1,2-Dichloroethylene, trans-1,3-Dichloropropene are outside control limits for sample F83513-1MSD. Probable cause due to sample
Sample F83513-1MSD has surrogates outside control limits. Probable cause due to matrix interference.
Metals by Method SW846 6010C Matrix: AQ Batch ID: MP20838
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Samples F83312-1DUP, F83312-1MS, F83312-1MSD, F83312-1PS, F83312-1SDL were used as the QC samples for metals.
Accutest Laboratories Southeast (ALSE) certifies that this report meets the project requirements for analytical data produced for the
samples as received at ALSE and as stated on the COC. ALSE certifies that the data meets the Data Quality Objectives for precision,
accuracy and completeness as specified in the ALSE Quality Manual except as noted above. This report is to be used in its entirety.
ALSE is not responsible for any assumptions of data quality if partial data packages are used.
Narrative prepared by:
_______________________________________ Date: July 6, 2011
Ellen Pampel, Inorganic QA (signature on file)
Wednesday, July 06, 2011
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Sample Results
Report of Analysis
Southeast
Section 3
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Report of Analysis Page 1 of 2
Client Sample ID:TB-06/16/11
Lab Sample ID:F83520-1 Date Sampled:06/16/11
Matrix:AQ - Trip Blank Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 J066773.D 1 06/28/11 MM n/a n/a VJ3632
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 23.2 25 10 ug/l J
71-43-2 Benzene 0.20 U 1.0 0.20 ug/l
74-97-5 Bromochloromethane 0.22 U 1.0 0.22 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.20 U 1.0 0.20 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.22 U 1.0 0.22 ug/l
75-15-0 Carbon disulfide 0.50 U 2.0 0.50 ug/l
56-23-5 Carbon tetrachloride 0.25 U 1.0 0.25 ug/l
110-82-7 Cyclohexane 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 0.25 U 1.0 0.25 ug/l
75-35-4 1,1-Dichloroethylene 0.23 U 1.0 0.23 ug/l
96-12-8 1,2-Dibromo-3-chloropropane 0.50 U 2.0 0.50 ug/l
106-93-4 1,2-Dibromoethane 0.37 U 1.0 0.37 ug/l
107-06-2 1,2-Dichloroethane 0.20 U 1.0 0.20 ug/l
78-87-5 1,2-Dichloropropane 0.25 U 1.0 0.25 ug/l
123-91-1 1,4-Dioxane 25 U 200 25 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
75-71-8 Dichlorodifluoromethane 0.50 U 2.0 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.26 U 1.0 0.26 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
541-73-1 m-Dichlorobenzene 0.20 U 1.0 0.20 ug/l
95-50-1 o-Dichlorobenzene 0.25 U 1.0 0.25 ug/l
106-46-7 p-Dichlorobenzene 0.23 U 1.0 0.23 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.35 U 1.0 0.35 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
100-41-4 Ethylbenzene 0.20 U 1.0 0.20 ug/l
76-13-1 Freon 113 0.47 U 1.0 0.47 ug/l
591-78-6 2-Hexanone 4.0 U 10 4.0 ug/l
98-82-8 Isopropylbenzene 0.20 U 1.0 0.20 ug/l
108-10-1 4-Methyl-2-pentanone 2.0 U 5.0 2.0 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:TB-06/16/11
Lab Sample ID:F83520-1 Date Sampled:06/16/11
Matrix:AQ - Trip Blank Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
79-20-9 Methyl Acetate 5.0 U 20 5.0 ug/l
74-83-9 Methyl bromide 0.50 U 2.0 0.50 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
108-87-2 Methylcyclohexane 0.38 U 1.0 0.38 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 2.0 U 5.0 2.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.34 U 1.0 0.34 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.23 U 1.0 0.23 ug/l
79-00-5 1,1,2-Trichloroethane 0.22 U 1.0 0.22 ug/l
87-61-6 1,2,3-Trichlorobenzene 0.50 U 1.0 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene 0.50 U 1.0 0.50 ug/l
127-18-4 Tetrachloroethylene 0.25 U 1.0 0.25 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 0.26 U 1.0 0.26 ug/l
75-69-4 Trichlorofluoromethane 0.50 U 2.0 0.50 ug/l
75-01-4 Vinyl chloride 0.22 U 1.0 0.22 ug/l
m,p-Xylene 0.32 U 2.0 0.32 ug/l
95-47-6 o-Xylene 0.20 U 1.0 0.20 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 94%87-116%
17060-07-0 1,2-Dichloroethane-D4 92%76-127%
2037-26-5 Toluene-D8 105%86-112%
460-00-4 4-Bromofluorobenzene 100%84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:MW-5
Lab Sample ID:F83520-2 Date Sampled:06/16/11
Matrix:AQ - Ground Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 J066774.D 1 06/28/11 MM n/a n/a VJ3632
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.20 U 1.0 0.20 ug/l
74-97-5 Bromochloromethane 0.22 U 1.0 0.22 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.20 U 1.0 0.20 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.22 U 1.0 0.22 ug/l
75-15-0 Carbon disulfide 0.50 U 2.0 0.50 ug/l
56-23-5 Carbon tetrachloride 0.25 U 1.0 0.25 ug/l
110-82-7 Cyclohexane 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 0.25 U 1.0 0.25 ug/l
75-35-4 1,1-Dichloroethylene 0.23 U 1.0 0.23 ug/l
96-12-8 1,2-Dibromo-3-chloropropane 0.50 U 2.0 0.50 ug/l
106-93-4 1,2-Dibromoethane 0.37 U 1.0 0.37 ug/l
107-06-2 1,2-Dichloroethane 0.20 U 1.0 0.20 ug/l
78-87-5 1,2-Dichloropropane 0.25 U 1.0 0.25 ug/l
123-91-1 1,4-Dioxane 25 U 200 25 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
75-71-8 Dichlorodifluoromethane 0.50 U 2.0 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.26 U 1.0 0.26 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
541-73-1 m-Dichlorobenzene 0.20 U 1.0 0.20 ug/l
95-50-1 o-Dichlorobenzene 0.25 U 1.0 0.25 ug/l
106-46-7 p-Dichlorobenzene 0.23 U 1.0 0.23 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.35 U 1.0 0.35 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
100-41-4 Ethylbenzene 0.20 U 1.0 0.20 ug/l
76-13-1 Freon 113 0.47 U 1.0 0.47 ug/l
591-78-6 2-Hexanone 4.0 U 10 4.0 ug/l
98-82-8 Isopropylbenzene 0.20 U 1.0 0.20 ug/l
108-10-1 4-Methyl-2-pentanone 2.0 U 5.0 2.0 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-5
Lab Sample ID:F83520-2 Date Sampled:06/16/11
Matrix:AQ - Ground Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
79-20-9 Methyl Acetate 5.0 U 20 5.0 ug/l
74-83-9 Methyl bromide 0.50 U 2.0 0.50 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
108-87-2 Methylcyclohexane 0.38 U 1.0 0.38 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 2.0 U 5.0 2.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.34 U 1.0 0.34 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.23 U 1.0 0.23 ug/l
79-00-5 1,1,2-Trichloroethane 0.22 U 1.0 0.22 ug/l
87-61-6 1,2,3-Trichlorobenzene 0.50 U 1.0 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene 0.50 U 1.0 0.50 ug/l
127-18-4 Tetrachloroethylene 0.25 U 1.0 0.25 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 0.26 U 1.0 0.26 ug/l
75-69-4 Trichlorofluoromethane 0.50 U 2.0 0.50 ug/l
75-01-4 Vinyl chloride 0.22 U 1.0 0.22 ug/l
m,p-Xylene 0.32 U 2.0 0.32 ug/l
95-47-6 o-Xylene 0.20 U 1.0 0.20 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 92%87-116%
17060-07-0 1,2-Dichloroethane-D4 89%76-127%
2037-26-5 Toluene-D8 102%86-112%
460-00-4 4-Bromofluorobenzene 101%84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:MW-5
Lab Sample ID:F83520-2 Date Sampled:06/16/11
Matrix:AQ - Ground Water Date Received:06/18/11
Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Total Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Chromium 5.4 J 10 1.0 ug/l 1 06/22/11 06/22/11 DM SW846 6010C 1 SW846 3010A 2
(1) Instrument QC Batch: MA9044
(2) Prep QC Batch: MP20838
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Report of Analysis Page 1 of 1
Client Sample ID:MW-5
Lab Sample ID:F83520-2F Date Sampled:06/16/11
Matrix:AQ - Groundwater Filtered Date Received:06/18/11
Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
Dissolved Metals Analysis
Analyte Result RL MDL Units DF Prep Analyzed By Method Prep Method
Chromium 1.9 J 10 1.0 ug/l 1 06/22/11 06/22/11 DM SW846 6010C 1 SW846 3010A 2
(1) Instrument QC Batch: MA9044
(2) Prep QC Batch: MP20838
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
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Report of Analysis Page 1 of 2
Client Sample ID:MW-3
Lab Sample ID:F83520-3 Date Sampled:06/16/11
Matrix:AQ - Ground Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 J066775.D 1 06/28/11 MM n/a n/a VJ3632
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.20 U 1.0 0.20 ug/l
74-97-5 Bromochloromethane 0.22 U 1.0 0.22 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.20 U 1.0 0.20 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.22 U 1.0 0.22 ug/l
75-15-0 Carbon disulfide 0.50 U 2.0 0.50 ug/l
56-23-5 Carbon tetrachloride 0.25 U 1.0 0.25 ug/l
110-82-7 Cyclohexane 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 0.25 U 1.0 0.25 ug/l
75-35-4 1,1-Dichloroethylene 0.23 U 1.0 0.23 ug/l
96-12-8 1,2-Dibromo-3-chloropropane 0.50 U 2.0 0.50 ug/l
106-93-4 1,2-Dibromoethane 0.37 U 1.0 0.37 ug/l
107-06-2 1,2-Dichloroethane 0.20 U 1.0 0.20 ug/l
78-87-5 1,2-Dichloropropane 0.25 U 1.0 0.25 ug/l
123-91-1 1,4-Dioxane 25 U 200 25 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
75-71-8 Dichlorodifluoromethane 0.50 U 2.0 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.26 U 1.0 0.26 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
541-73-1 m-Dichlorobenzene 0.20 U 1.0 0.20 ug/l
95-50-1 o-Dichlorobenzene 0.25 U 1.0 0.25 ug/l
106-46-7 p-Dichlorobenzene 0.23 U 1.0 0.23 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.35 U 1.0 0.35 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
100-41-4 Ethylbenzene 0.20 U 1.0 0.20 ug/l
76-13-1 Freon 113 0.47 U 1.0 0.47 ug/l
591-78-6 2-Hexanone 4.0 U 10 4.0 ug/l
98-82-8 Isopropylbenzene 0.20 U 1.0 0.20 ug/l
108-10-1 4-Methyl-2-pentanone 2.0 U 5.0 2.0 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-3
Lab Sample ID:F83520-3 Date Sampled:06/16/11
Matrix:AQ - Ground Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
79-20-9 Methyl Acetate 5.0 U 20 5.0 ug/l
74-83-9 Methyl bromide 0.50 U 2.0 0.50 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
108-87-2 Methylcyclohexane 0.38 U 1.0 0.38 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 2.0 U 5.0 2.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.34 U 1.0 0.34 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.23 U 1.0 0.23 ug/l
79-00-5 1,1,2-Trichloroethane 0.22 U 1.0 0.22 ug/l
87-61-6 1,2,3-Trichlorobenzene 0.50 U 1.0 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene 0.50 U 1.0 0.50 ug/l
127-18-4 Tetrachloroethylene 0.25 U 1.0 0.25 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 0.26 U 1.0 0.26 ug/l
75-69-4 Trichlorofluoromethane 0.50 U 2.0 0.50 ug/l
75-01-4 Vinyl chloride 0.22 U 1.0 0.22 ug/l
m,p-Xylene 0.32 U 2.0 0.32 ug/l
95-47-6 o-Xylene 0.20 U 1.0 0.20 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 93%87-116%
17060-07-0 1,2-Dichloroethane-D4 90%76-127%
2037-26-5 Toluene-D8 104%86-112%
460-00-4 4-Bromofluorobenzene 100%84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:MW-4
Lab Sample ID:F83520-4 Date Sampled:06/16/11
Matrix:AQ - Ground Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 J066776.D 1 06/28/11 MM n/a n/a VJ3632
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.20 U 1.0 0.20 ug/l
74-97-5 Bromochloromethane 0.22 U 1.0 0.22 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.20 U 1.0 0.20 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.22 U 1.0 0.22 ug/l
75-15-0 Carbon disulfide 0.50 U 2.0 0.50 ug/l
56-23-5 Carbon tetrachloride 0.25 U 1.0 0.25 ug/l
110-82-7 Cyclohexane 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 0.25 U 1.0 0.25 ug/l
75-35-4 1,1-Dichloroethylene 0.23 U 1.0 0.23 ug/l
96-12-8 1,2-Dibromo-3-chloropropane 0.50 U 2.0 0.50 ug/l
106-93-4 1,2-Dibromoethane 0.37 U 1.0 0.37 ug/l
107-06-2 1,2-Dichloroethane 0.20 U 1.0 0.20 ug/l
78-87-5 1,2-Dichloropropane 0.25 U 1.0 0.25 ug/l
123-91-1 1,4-Dioxane 25 U 200 25 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
75-71-8 Dichlorodifluoromethane 0.50 U 2.0 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.26 U 1.0 0.26 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
541-73-1 m-Dichlorobenzene 0.20 U 1.0 0.20 ug/l
95-50-1 o-Dichlorobenzene 0.25 U 1.0 0.25 ug/l
106-46-7 p-Dichlorobenzene 0.23 U 1.0 0.23 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.35 U 1.0 0.35 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
100-41-4 Ethylbenzene 0.20 U 1.0 0.20 ug/l
76-13-1 Freon 113 0.47 U 1.0 0.47 ug/l
591-78-6 2-Hexanone 4.0 U 10 4.0 ug/l
98-82-8 Isopropylbenzene 0.20 U 1.0 0.20 ug/l
108-10-1 4-Methyl-2-pentanone 2.0 U 5.0 2.0 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-4
Lab Sample ID:F83520-4 Date Sampled:06/16/11
Matrix:AQ - Ground Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
79-20-9 Methyl Acetate 5.0 U 20 5.0 ug/l
74-83-9 Methyl bromide 0.50 U 2.0 0.50 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
108-87-2 Methylcyclohexane 0.38 U 1.0 0.38 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 2.0 U 5.0 2.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.34 U 1.0 0.34 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.23 U 1.0 0.23 ug/l
79-00-5 1,1,2-Trichloroethane 0.22 U 1.0 0.22 ug/l
87-61-6 1,2,3-Trichlorobenzene 0.50 U 1.0 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene 0.50 U 1.0 0.50 ug/l
127-18-4 Tetrachloroethylene 0.25 U 1.0 0.25 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 0.26 U 1.0 0.26 ug/l
75-69-4 Trichlorofluoromethane 0.50 U 2.0 0.50 ug/l
75-01-4 Vinyl chloride 0.22 U 1.0 0.22 ug/l
m,p-Xylene 0.32 U 2.0 0.32 ug/l
95-47-6 o-Xylene 0.20 U 1.0 0.20 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 93%87-116%
17060-07-0 1,2-Dichloroethane-D4 89%76-127%
2037-26-5 Toluene-D8 106%86-112%
460-00-4 4-Bromofluorobenzene 101%84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-6
Lab Sample ID:F83520-5 Date Sampled:06/16/11
Matrix:AQ - Ground Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 J066777.D 1 06/28/11 MM n/a n/a VJ3632
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.20 U 1.0 0.20 ug/l
74-97-5 Bromochloromethane 0.22 U 1.0 0.22 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.20 U 1.0 0.20 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.22 U 1.0 0.22 ug/l
75-15-0 Carbon disulfide 0.50 U 2.0 0.50 ug/l
56-23-5 Carbon tetrachloride 0.25 U 1.0 0.25 ug/l
110-82-7 Cyclohexane 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 0.25 U 1.0 0.25 ug/l
75-35-4 1,1-Dichloroethylene 0.49 1.0 0.23 ug/l J
96-12-8 1,2-Dibromo-3-chloropropane 0.50 U 2.0 0.50 ug/l
106-93-4 1,2-Dibromoethane 0.37 U 1.0 0.37 ug/l
107-06-2 1,2-Dichloroethane 0.20 U 1.0 0.20 ug/l
78-87-5 1,2-Dichloropropane 0.25 U 1.0 0.25 ug/l
123-91-1 1,4-Dioxane 25 U 200 25 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
75-71-8 Dichlorodifluoromethane 0.50 U 2.0 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.26 U 1.0 0.26 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
541-73-1 m-Dichlorobenzene 0.20 U 1.0 0.20 ug/l
95-50-1 o-Dichlorobenzene 0.25 U 1.0 0.25 ug/l
106-46-7 p-Dichlorobenzene 0.23 U 1.0 0.23 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.35 U 1.0 0.35 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
100-41-4 Ethylbenzene 0.20 U 1.0 0.20 ug/l
76-13-1 Freon 113 0.47 U 1.0 0.47 ug/l
591-78-6 2-Hexanone 4.0 U 10 4.0 ug/l
98-82-8 Isopropylbenzene 0.20 U 1.0 0.20 ug/l
108-10-1 4-Methyl-2-pentanone 2.0 U 5.0 2.0 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-6
Lab Sample ID:F83520-5 Date Sampled:06/16/11
Matrix:AQ - Ground Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
79-20-9 Methyl Acetate 5.0 U 20 5.0 ug/l
74-83-9 Methyl bromide 0.50 U 2.0 0.50 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
108-87-2 Methylcyclohexane 0.38 U 1.0 0.38 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 2.0 U 5.0 2.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.34 U 1.0 0.34 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.23 U 1.0 0.23 ug/l
79-00-5 1,1,2-Trichloroethane 0.22 U 1.0 0.22 ug/l
87-61-6 1,2,3-Trichlorobenzene 0.50 U 1.0 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene 0.50 U 1.0 0.50 ug/l
127-18-4 Tetrachloroethylene 0.25 U 1.0 0.25 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 17.7 1.0 0.26 ug/l
75-69-4 Trichlorofluoromethane 0.50 U 2.0 0.50 ug/l
75-01-4 Vinyl chloride 0.22 U 1.0 0.22 ug/l
m,p-Xylene 0.32 U 2.0 0.32 ug/l
95-47-6 o-Xylene 0.20 U 1.0 0.20 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 91%87-116%
17060-07-0 1,2-Dichloroethane-D4 86%76-127%
2037-26-5 Toluene-D8 106%86-112%
460-00-4 4-Bromofluorobenzene 101%84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:MW-7
Lab Sample ID:F83520-6 Date Sampled:06/16/11
Matrix:AQ - Ground Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 J066778.D 2 06/28/11 MM n/a n/a VJ3632
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 20 U 50 20 ug/l
71-43-2 Benzene 0.40 U 2.0 0.40 ug/l
74-97-5 Bromochloromethane 0.44 U 2.0 0.44 ug/l
75-27-4 Bromodichloromethane 0.40 U 2.0 0.40 ug/l
75-25-2 Bromoform 0.40 U 2.0 0.40 ug/l
108-90-7 Chlorobenzene 0.40 U 2.0 0.40 ug/l
75-00-3 Chloroethane 1.0 U 4.0 1.0 ug/l
67-66-3 Chloroform 0.44 U 2.0 0.44 ug/l
75-15-0 Carbon disulfide 1.0 U 4.0 1.0 ug/l
56-23-5 Carbon tetrachloride 0.50 U 2.0 0.50 ug/l
110-82-7 Cyclohexane 0.62 U 2.0 0.62 ug/l
75-34-3 1,1-Dichloroethane 1.9 2.0 0.50 ug/l J
75-35-4 1,1-Dichloroethylene 16.5 2.0 0.46 ug/l
96-12-8 1,2-Dibromo-3-chloropropane 1.0 U 4.0 1.0 ug/l
106-93-4 1,2-Dibromoethane 0.74 U 2.0 0.74 ug/l
107-06-2 1,2-Dichloroethane 0.40 U 2.0 0.40 ug/l
78-87-5 1,2-Dichloropropane 0.50 U 2.0 0.50 ug/l
123-91-1 1,4-Dioxane 50 U 400 50 ug/l
124-48-1 Dibromochloromethane 0.40 U 2.0 0.40 ug/l
75-71-8 Dichlorodifluoromethane 1.0 U 4.0 1.0 ug/l
156-59-2 cis-1,2-Dichloroethylene 47.4 2.0 0.52 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.40 U 2.0 0.40 ug/l
541-73-1 m-Dichlorobenzene 0.40 U 2.0 0.40 ug/l
95-50-1 o-Dichlorobenzene 0.50 U 2.0 0.50 ug/l
106-46-7 p-Dichlorobenzene 0.46 U 2.0 0.46 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.70 U 2.0 0.70 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.40 U 2.0 0.40 ug/l
100-41-4 Ethylbenzene 0.40 U 2.0 0.40 ug/l
76-13-1 Freon 113 0.94 U 2.0 0.94 ug/l
591-78-6 2-Hexanone 8.0 U 20 8.0 ug/l
98-82-8 Isopropylbenzene 0.40 U 2.0 0.40 ug/l
108-10-1 4-Methyl-2-pentanone 4.0 U 10 4.0 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-7
Lab Sample ID:F83520-6 Date Sampled:06/16/11
Matrix:AQ - Ground Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
79-20-9 Methyl Acetate 10 U 40 10 ug/l
74-83-9 Methyl bromide 1.0 U 4.0 1.0 ug/l
74-87-3 Methyl chloride 1.0 U 4.0 1.0 ug/l
108-87-2 Methylcyclohexane 0.76 U 2.0 0.76 ug/l
75-09-2 Methylene chloride 4.0 U 10 4.0 ug/l
78-93-3 Methyl ethyl ketone 4.0 U 10 4.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.68 U 2.0 0.68 ug/l
100-42-5 Styrene 0.40 U 2.0 0.40 ug/l
71-55-6 1,1,1-Trichloroethane 0.40 U 2.0 0.40 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.46 U 2.0 0.46 ug/l
79-00-5 1,1,2-Trichloroethane 0.44 U 2.0 0.44 ug/l
87-61-6 1,2,3-Trichlorobenzene 1.0 U 2.0 1.0 ug/l
120-82-1 1,2,4-Trichlorobenzene 1.0 U 2.0 1.0 ug/l
127-18-4 Tetrachloroethylene 103 2.0 0.50 ug/l
108-88-3 Toluene 0.40 U 2.0 0.40 ug/l
79-01-6 Trichloroethylene 90.1 2.0 0.52 ug/l
75-69-4 Trichlorofluoromethane 1.0 U 4.0 1.0 ug/l
75-01-4 Vinyl chloride 0.44 U 2.0 0.44 ug/l
m,p-Xylene 0.64 U 4.0 0.64 ug/l
95-47-6 o-Xylene 0.40 U 2.0 0.40 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 92%87-116%
17060-07-0 1,2-Dichloroethane-D4 87%76-127%
2037-26-5 Toluene-D8 108%86-112%
460-00-4 4-Bromofluorobenzene 100%84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:MW-8
Lab Sample ID:F83520-7 Date Sampled:06/16/11
Matrix:AQ - Ground Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 J066779.D 1 06/28/11 MM n/a n/a VJ3632
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.20 U 1.0 0.20 ug/l
74-97-5 Bromochloromethane 0.22 U 1.0 0.22 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.20 U 1.0 0.20 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 2.1 1.0 0.22 ug/l
75-15-0 Carbon disulfide 0.50 U 2.0 0.50 ug/l
56-23-5 Carbon tetrachloride 0.25 U 1.0 0.25 ug/l
110-82-7 Cyclohexane 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 0.25 U 1.0 0.25 ug/l
75-35-4 1,1-Dichloroethylene 0.23 U 1.0 0.23 ug/l
96-12-8 1,2-Dibromo-3-chloropropane 0.50 U 2.0 0.50 ug/l
106-93-4 1,2-Dibromoethane 0.37 U 1.0 0.37 ug/l
107-06-2 1,2-Dichloroethane 0.20 U 1.0 0.20 ug/l
78-87-5 1,2-Dichloropropane 0.25 U 1.0 0.25 ug/l
123-91-1 1,4-Dioxane 25 U 200 25 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
75-71-8 Dichlorodifluoromethane 0.50 U 2.0 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.26 U 1.0 0.26 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
541-73-1 m-Dichlorobenzene 0.20 U 1.0 0.20 ug/l
95-50-1 o-Dichlorobenzene 0.25 U 1.0 0.25 ug/l
106-46-7 p-Dichlorobenzene 0.23 U 1.0 0.23 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.35 U 1.0 0.35 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
100-41-4 Ethylbenzene 0.20 U 1.0 0.20 ug/l
76-13-1 Freon 113 0.47 U 1.0 0.47 ug/l
591-78-6 2-Hexanone 4.0 U 10 4.0 ug/l
98-82-8 Isopropylbenzene 0.20 U 1.0 0.20 ug/l
108-10-1 4-Methyl-2-pentanone 2.0 U 5.0 2.0 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:MW-8
Lab Sample ID:F83520-7 Date Sampled:06/16/11
Matrix:AQ - Ground Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
79-20-9 Methyl Acetate 5.0 U 20 5.0 ug/l
74-83-9 Methyl bromide 0.50 U 2.0 0.50 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
108-87-2 Methylcyclohexane 0.38 U 1.0 0.38 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 2.0 U 5.0 2.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.34 U 1.0 0.34 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.23 U 1.0 0.23 ug/l
79-00-5 1,1,2-Trichloroethane 0.22 U 1.0 0.22 ug/l
87-61-6 1,2,3-Trichlorobenzene 0.50 U 1.0 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene 0.50 U 1.0 0.50 ug/l
127-18-4 Tetrachloroethylene 0.25 U 1.0 0.25 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 0.26 U 1.0 0.26 ug/l
75-69-4 Trichlorofluoromethane 0.50 U 2.0 0.50 ug/l
75-01-4 Vinyl chloride 0.22 U 1.0 0.22 ug/l
m,p-Xylene 0.32 U 2.0 0.32 ug/l
95-47-6 o-Xylene 0.20 U 1.0 0.20 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 89%87-116%
17060-07-0 1,2-Dichloroethane-D4 85%76-127%
2037-26-5 Toluene-D8 103%86-112%
460-00-4 4-Bromofluorobenzene 100%84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:MW-9
Lab Sample ID:F83520-8 Date Sampled:06/16/11
Matrix:AQ - Ground Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 J066780.D 1 06/28/11 MM n/a n/a VJ3632
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.20 U 1.0 0.20 ug/l
74-97-5 Bromochloromethane 0.22 U 1.0 0.22 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.20 U 1.0 0.20 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.22 U 1.0 0.22 ug/l
75-15-0 Carbon disulfide 0.50 U 2.0 0.50 ug/l
56-23-5 Carbon tetrachloride 0.25 U 1.0 0.25 ug/l
110-82-7 Cyclohexane 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 1.0 1.0 0.25 ug/l
75-35-4 1,1-Dichloroethylene 0.70 1.0 0.23 ug/l J
96-12-8 1,2-Dibromo-3-chloropropane 0.50 U 2.0 0.50 ug/l
106-93-4 1,2-Dibromoethane 0.37 U 1.0 0.37 ug/l
107-06-2 1,2-Dichloroethane 0.20 U 1.0 0.20 ug/l
78-87-5 1,2-Dichloropropane 0.25 U 1.0 0.25 ug/l
123-91-1 1,4-Dioxane 25 U 200 25 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
75-71-8 Dichlorodifluoromethane 0.50 U 2.0 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene 18.5 1.0 0.26 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
541-73-1 m-Dichlorobenzene 0.20 U 1.0 0.20 ug/l
95-50-1 o-Dichlorobenzene 0.25 U 1.0 0.25 ug/l
106-46-7 p-Dichlorobenzene 0.23 U 1.0 0.23 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.35 U 1.0 0.35 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
100-41-4 Ethylbenzene 0.20 U 1.0 0.20 ug/l
76-13-1 Freon 113 0.47 U 1.0 0.47 ug/l
591-78-6 2-Hexanone 4.0 U 10 4.0 ug/l
98-82-8 Isopropylbenzene 0.20 U 1.0 0.20 ug/l
108-10-1 4-Methyl-2-pentanone 2.0 U 5.0 2.0 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-9
Lab Sample ID:F83520-8 Date Sampled:06/16/11
Matrix:AQ - Ground Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
79-20-9 Methyl Acetate 5.0 U 20 5.0 ug/l
74-83-9 Methyl bromide 0.50 U 2.0 0.50 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
108-87-2 Methylcyclohexane 0.38 U 1.0 0.38 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 2.0 U 5.0 2.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.34 U 1.0 0.34 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.23 U 1.0 0.23 ug/l
79-00-5 1,1,2-Trichloroethane 0.22 U 1.0 0.22 ug/l
87-61-6 1,2,3-Trichlorobenzene 0.50 U 1.0 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene 0.50 U 1.0 0.50 ug/l
127-18-4 Tetrachloroethylene 5.6 1.0 0.25 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 2.9 1.0 0.26 ug/l
75-69-4 Trichlorofluoromethane 0.50 U 2.0 0.50 ug/l
75-01-4 Vinyl chloride 0.22 U 1.0 0.22 ug/l
m,p-Xylene 0.32 U 2.0 0.32 ug/l
95-47-6 o-Xylene 0.20 U 1.0 0.20 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 89%87-116%
17060-07-0 1,2-Dichloroethane-D4 85%76-127%
2037-26-5 Toluene-D8 111%86-112%
460-00-4 4-Bromofluorobenzene 100%84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:F83520-9 Date Sampled:06/16/11
Matrix:AQ - Ground Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 J066781.D 1 06/28/11 MM n/a n/a VJ3632
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10 U 25 10 ug/l
71-43-2 Benzene 0.20 U 1.0 0.20 ug/l
74-97-5 Bromochloromethane 0.22 U 1.0 0.22 ug/l
75-27-4 Bromodichloromethane 0.20 U 1.0 0.20 ug/l
75-25-2 Bromoform 0.20 U 1.0 0.20 ug/l
108-90-7 Chlorobenzene 0.20 U 1.0 0.20 ug/l
75-00-3 Chloroethane 0.50 U 2.0 0.50 ug/l
67-66-3 Chloroform 0.84 1.0 0.22 ug/l J
75-15-0 Carbon disulfide 0.50 U 2.0 0.50 ug/l
56-23-5 Carbon tetrachloride 1.8 1.0 0.25 ug/l
110-82-7 Cyclohexane 0.31 U 1.0 0.31 ug/l
75-34-3 1,1-Dichloroethane 0.25 U 1.0 0.25 ug/l
75-35-4 1,1-Dichloroethylene 0.23 U 1.0 0.23 ug/l
96-12-8 1,2-Dibromo-3-chloropropane 0.50 U 2.0 0.50 ug/l
106-93-4 1,2-Dibromoethane 0.37 U 1.0 0.37 ug/l
107-06-2 1,2-Dichloroethane 0.20 U 1.0 0.20 ug/l
78-87-5 1,2-Dichloropropane 0.25 U 1.0 0.25 ug/l
123-91-1 1,4-Dioxane 25 U 200 25 ug/l
124-48-1 Dibromochloromethane 0.20 U 1.0 0.20 ug/l
75-71-8 Dichlorodifluoromethane 0.50 U 2.0 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.26 U 1.0 0.26 ug/l
10061-01-5 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
541-73-1 m-Dichlorobenzene 0.20 U 1.0 0.20 ug/l
95-50-1 o-Dichlorobenzene 0.25 U 1.0 0.25 ug/l
106-46-7 p-Dichlorobenzene 0.23 U 1.0 0.23 ug/l
156-60-5 trans-1,2-Dichloroethylene 0.35 U 1.0 0.35 ug/l
10061-02-6 trans-1,3-Dichloropropene 0.20 U 1.0 0.20 ug/l
100-41-4 Ethylbenzene 0.20 U 1.0 0.20 ug/l
76-13-1 Freon 113 0.47 U 1.0 0.47 ug/l
591-78-6 2-Hexanone 4.0 U 10 4.0 ug/l
98-82-8 Isopropylbenzene 0.20 U 1.0 0.20 ug/l
108-10-1 4-Methyl-2-pentanone 2.0 U 5.0 2.0 ug/l
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:F83520-9 Date Sampled:06/16/11
Matrix:AQ - Ground Water Date Received:06/18/11
Method:SW846 8260B Percent Solids:n/a
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
VOA TCL (SOM01.1) List
CAS No.Compound Result RL MDL Units Q
79-20-9 Methyl Acetate 5.0 U 20 5.0 ug/l
74-83-9 Methyl bromide 0.50 U 2.0 0.50 ug/l
74-87-3 Methyl chloride 0.50 U 2.0 0.50 ug/l
108-87-2 Methylcyclohexane 0.38 U 1.0 0.38 ug/l
75-09-2 Methylene chloride 2.0 U 5.0 2.0 ug/l
78-93-3 Methyl ethyl ketone 2.0 U 5.0 2.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.34 U 1.0 0.34 ug/l
100-42-5 Styrene 0.20 U 1.0 0.20 ug/l
71-55-6 1,1,1-Trichloroethane 0.20 U 1.0 0.20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 0.23 U 1.0 0.23 ug/l
79-00-5 1,1,2-Trichloroethane 0.22 U 1.0 0.22 ug/l
87-61-6 1,2,3-Trichlorobenzene 0.50 U 1.0 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene 0.50 U 1.0 0.50 ug/l
127-18-4 Tetrachloroethylene 0.25 U 1.0 0.25 ug/l
108-88-3 Toluene 0.20 U 1.0 0.20 ug/l
79-01-6 Trichloroethylene 0.26 U 1.0 0.26 ug/l
75-69-4 Trichlorofluoromethane 0.50 U 2.0 0.50 ug/l
75-01-4 Vinyl chloride 0.22 U 1.0 0.22 ug/l
m,p-Xylene 0.32 U 2.0 0.32 ug/l
95-47-6 o-Xylene 0.20 U 1.0 0.20 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 93%87-116%
17060-07-0 1,2-Dichloroethane-D4 88%76-127%
2037-26-5 Toluene-D8 106%86-112%
460-00-4 4-Bromofluorobenzene 100%84-120%
U = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Certification Exceptions
• Certification Exceptions (NC)
• Chain of Custody
Southeast
Section 4
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Parameter Certification Exceptions Page 1 of 1
Job Number:F83520
Account:AMECPAP AMEC Environment & Infrastructure, Inc.
Project:GE-TFS; 1906 Bancroft St, Charlotte, NC
The following parameters included in this report are exceptions to NELAC certification.
The certification status of each is indicated below.
Parameter CAS#Method Mat Certification Status
Freon 113 76-13-1 SW846 8260B AQ Certified by SOP MS005
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F83520: Chain of Custody
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F83520: Chain of Custody
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APPENDIX C
APPENDIX D