20022_Mount Hope II_Air Summary2_2016_08_26

#=CL#
March 31, 2016
LIMS USE: FR - MIKE SMITH
LIMS OBJECT ID: 92291329
92291329
Project:
Pace Project No.:
RE:
Mike Smith
Smith Environmental Consultants
5503 Meadow Haven Ln
Charlotte, NC 28270
Mt Hope - N108-02
Dear Mike Smith:
Enclosed are the analytical results for sample(s) received by the laboratory on March 24, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 17
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92291329
Mt Hope - N108-02
Minnesota Certification IDs1700 Elm Street SE Suite 200, Minneapolis, MN 55414525 N 8th Street, Salina, KS 67401
A2LA Certification #: 2926.01Alaska Certification #: UST-078Alaska Certification #MN00064Alabama Certification #40770Arizona Certification #: AZ-0014
Arkansas Certification #: 88-0680California Certification #: 01155CAColorado Certification #PaceConnecticut Certification #: PH-0256EPA Region 8 Certification #: 8TMS-L
Florida/NELAP Certification #: E87605Guam Certification #:14-008rGeorgia Certification #: 959Georgia EPD #: PaceIdaho Certification #: MN00064
Hawaii Certification #MN00064Illinois Certification #: 200011Indiana Certification#C-MN-01Iowa Certification #: 368Kansas Certification #: E-10167
Kentucky Dept of Envi. Protection - DW #90062Kentucky Dept of Envi. Protection - WW #:90062Louisiana DEQ Certification #: 3086Louisiana DHH #: LA140001Maine Certification #: 2013011
Maryland Certification #: 322Michigan DEPH Certification #: 9909
Minnesota Certification #: 027-053-137Mississippi Certification #: Pace
Montana Certification #: MT0092Nevada Certification #: MN_00064Nebraska Certification #: PaceNew Jersey Certification #: MN-002New York Certification #: 11647
North Carolina Certification #: 530North Carolina State Public Health #: 27700North Dakota Certification #: R-036Ohio EPA #: 4150Ohio VAP Certification #: CL101
Oklahoma Certification #: 9507Oregon Certification #: MN200001Oregon Certification #: MN300001Pennsylvania Certification #: 68-00563Puerto Rico Certification
Saipan (CNMI) #:MP0003South Carolina #:74003001Texas Certification #: T104704192Tennessee Certification #: 02818Utah Certification #: MN000642013-4
Virginia DGS Certification #: 251Virginia/VELAP Certification #: PaceWashington Certification #: C486West Virginia Certification #: 382West Virginia DHHR #:9952C
Wisconsin Certification #: 999407970
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 17
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92291329
Mt Hope - N108-02
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92291329001 Shop #1 TO-15 58 PASI-MMLS
92291329002 Shop #2 TO-15 58 PASI-MMLS
92291329003 Shop #3 TO-15 58 PASI-MMLS
92291329004 Office #1 TO-15 58 PASI-MMLS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291329
Mt Hope - N108-02
Sample:Shop #1 Lab ID:92291329001 Collected:03/24/16 14:14 Received:03/24/16 14:55 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 34.2 ug/m3 03/30/16 17:00 67-64-13.6 1.49
Benzene ND ug/m3 03/30/16 17:00 71-43-20.97 1.49
Bromodichloromethane ND ug/m3 03/30/16 17:00 75-27-42.0 1.49
Bromoform ND ug/m3 03/30/16 17:00 75-25-23.1 1.49
Bromomethane ND ug/m3 03/30/16 17:00 74-83-91.2 1.49
1,3-Butadiene ND ug/m3 03/30/16 17:00 106-99-00.67 1.49
2-Butanone (MEK)6.2 ug/m3 03/30/16 17:00 78-93-34.5 1.49
Carbon disulfide ND ug/m3 03/30/16 17:00 75-15-00.94 1.49
Carbon tetrachloride ND ug/m3 03/30/16 17:00 56-23-50.95 1.49
Chlorobenzene ND ug/m3 03/30/16 17:00 108-90-71.4 1.49
Chloroethane ND ug/m3 03/30/16 17:00 75-00-30.80 1.49
Chloroform ND ug/m3 03/30/16 17:00 67-66-31.5 1.49
Chloromethane 1.3 ug/m3 03/30/16 17:00 74-87-30.63 1.49
Cyclohexane ND ug/m3 03/30/16 17:00 110-82-71.0 1.49
Dibromochloromethane ND ug/m3 03/30/16 17:00 124-48-12.6 1.49
1,2-Dibromoethane (EDB)ND ug/m3 03/30/16 17:00 106-93-42.3 1.49
1,2-Dichlorobenzene ND ug/m3 03/30/16 17:00 95-50-11.8 1.49
1,3-Dichlorobenzene ND ug/m3 03/30/16 17:00 541-73-14.6 1.49
1,4-Dichlorobenzene ND ug/m3 03/30/16 17:00 106-46-71.8 1.49
Dichlorodifluoromethane 1.9 ug/m3 03/30/16 17:00 75-71-81.5 1.49
1,1-Dichloroethane ND ug/m3 03/30/16 17:00 75-34-31.2 1.49
1,2-Dichloroethane ND ug/m3 03/30/16 17:00 107-06-20.61 1.49
1,1-Dichloroethene ND ug/m3 03/30/16 17:00 75-35-41.2 1.49
cis-1,2-Dichloroethene ND ug/m3 03/30/16 17:00 156-59-21.2 1.49
trans-1,2-Dichloroethene ND ug/m3 03/30/16 17:00 156-60-51.2 1.49
1,2-Dichloropropane ND ug/m3 03/30/16 17:00 78-87-51.4 1.49
cis-1,3-Dichloropropene ND ug/m3 03/30/16 17:00 10061-01-53.4 1.49
trans-1,3-Dichloropropene ND ug/m3 03/30/16 17:00 10061-02-63.4 1.49
Dichlorotetrafluoroethane ND ug/m3 03/30/16 17:00 76-14-22.1 1.49
Ethyl acetate ND ug/m3 03/30/16 17:00 141-78-61.1 1.49
Ethylbenzene ND ug/m3 03/30/16 17:00 100-41-41.3 1.49
4-Ethyltoluene ND ug/m3 03/30/16 17:00 622-96-81.5 1.49
n-Heptane ND ug/m3 03/30/16 17:00 142-82-51.2 1.49
Hexachloro-1,3-butadiene ND ug/m3 03/30/16 17:00 87-68-316.2 1.49
n-Hexane ND ug/m3 03/30/16 17:00 110-54-31.1 1.49
2-Hexanone ND ug/m3 03/30/16 17:00 591-78-66.2 1.49
Methylene Chloride 6.6 ug/m3 03/30/16 17:00 75-09-25.3 1.49
4-Methyl-2-pentanone (MIBK)ND ug/m3 03/30/16 17:00 108-10-16.2 1.49
Methyl-tert-butyl ether ND ug/m3 03/30/16 17:00 1634-04-45.5 1.49
Naphthalene ND ug/m3 03/30/16 17:00 91-20-37.9 1.49
Propylene ND ug/m3 03/30/16 17:00 115-07-11.3 1.49
Styrene ND ug/m3 03/30/16 17:00 100-42-53.2 1.49
1,1,2,2-Tetrachloroethane ND ug/m3 03/30/16 17:00 79-34-55.2 1.49
Tetrachloroethene ND ug/m3 03/30/16 17:00 127-18-41.0 1.49
Tetrahydrofuran ND ug/m3 03/30/16 17:00 109-99-92.2 1.49
Toluene ND ug/m3 03/30/16 17:00 108-88-31.1 1.49
1,2,4-Trichlorobenzene ND ug/m3 03/30/16 17:00 120-82-111.2 1.49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/31/2016 05:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291329
Mt Hope - N108-02
Sample:Shop #1 Lab ID:92291329001 Collected:03/24/16 14:14 Received:03/24/16 14:55 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 03/30/16 17:00 71-55-61.7 1.49
1,1,2-Trichloroethane ND ug/m3 03/30/16 17:00 79-00-50.82 1.49
Trichloroethene ND ug/m3 03/30/16 17:00 79-01-60.82 1.49
Trichlorofluoromethane ND ug/m3 03/30/16 17:00 75-69-41.7 1.49
1,1,2-Trichlorotrifluoroethane ND ug/m3 03/30/16 17:00 76-13-12.4 1.49
1,2,4-Trimethylbenzene ND ug/m3 03/30/16 17:00 95-63-63.7 1.49
1,3,5-Trimethylbenzene ND ug/m3 03/30/16 17:00 108-67-81.5 1.49
Vinyl acetate 2.4 ug/m3 03/30/16 17:00 108-05-41.1 1.49
Vinyl chloride ND ug/m3 03/30/16 17:00 75-01-40.39 1.49
m&p-Xylene ND ug/m3 03/30/16 17:00 179601-23-12.6 1.49
o-Xylene ND ug/m3 03/30/16 17:00 95-47-61.3 1.49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/31/2016 05:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291329
Mt Hope - N108-02
Sample:Shop #2 Lab ID:92291329002 Collected:03/24/16 14:15 Received:03/24/16 14:55 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 13.2 ug/m3 03/30/16 17:31 67-64-13.6 1.49
Benzene ND ug/m3 03/30/16 17:31 71-43-20.97 1.49
Bromodichloromethane ND ug/m3 03/30/16 17:31 75-27-42.0 1.49
Bromoform ND ug/m3 03/30/16 17:31 75-25-23.1 1.49
Bromomethane ND ug/m3 03/30/16 17:31 74-83-91.2 1.49
1,3-Butadiene ND ug/m3 03/30/16 17:31 106-99-00.67 1.49
2-Butanone (MEK)ND ug/m3 03/30/16 17:31 78-93-34.5 1.49
Carbon disulfide ND ug/m3 03/30/16 17:31 75-15-00.94 1.49
Carbon tetrachloride ND ug/m3 03/30/16 17:31 56-23-50.95 1.49
Chlorobenzene ND ug/m3 03/30/16 17:31 108-90-71.4 1.49
Chloroethane ND ug/m3 03/30/16 17:31 75-00-30.80 1.49
Chloroform ND ug/m3 03/30/16 17:31 67-66-31.5 1.49
Chloromethane 1.4 ug/m3 03/30/16 17:31 74-87-30.63 1.49
Cyclohexane ND ug/m3 03/30/16 17:31 110-82-71.0 1.49
Dibromochloromethane ND ug/m3 03/30/16 17:31 124-48-12.6 1.49
1,2-Dibromoethane (EDB)ND ug/m3 03/30/16 17:31 106-93-42.3 1.49
1,2-Dichlorobenzene ND ug/m3 03/30/16 17:31 95-50-11.8 1.49
1,3-Dichlorobenzene ND ug/m3 03/30/16 17:31 541-73-14.6 1.49
1,4-Dichlorobenzene ND ug/m3 03/30/16 17:31 106-46-71.8 1.49
Dichlorodifluoromethane 2.1 ug/m3 03/30/16 17:31 75-71-81.5 1.49
1,1-Dichloroethane ND ug/m3 03/30/16 17:31 75-34-31.2 1.49
1,2-Dichloroethane ND ug/m3 03/30/16 17:31 107-06-20.61 1.49
1,1-Dichloroethene ND ug/m3 03/30/16 17:31 75-35-41.2 1.49
cis-1,2-Dichloroethene ND ug/m3 03/30/16 17:31 156-59-21.2 1.49
trans-1,2-Dichloroethene ND ug/m3 03/30/16 17:31 156-60-51.2 1.49
1,2-Dichloropropane ND ug/m3 03/30/16 17:31 78-87-51.4 1.49
cis-1,3-Dichloropropene ND ug/m3 03/30/16 17:31 10061-01-53.4 1.49
trans-1,3-Dichloropropene ND ug/m3 03/30/16 17:31 10061-02-63.4 1.49
Dichlorotetrafluoroethane ND ug/m3 03/30/16 17:31 76-14-22.1 1.49
Ethyl acetate ND ug/m3 03/30/16 17:31 141-78-61.1 1.49
Ethylbenzene ND ug/m3 03/30/16 17:31 100-41-41.3 1.49
4-Ethyltoluene ND ug/m3 03/30/16 17:31 622-96-81.5 1.49
n-Heptane ND ug/m3 03/30/16 17:31 142-82-51.2 1.49
Hexachloro-1,3-butadiene ND ug/m3 03/30/16 17:31 87-68-316.2 1.49
n-Hexane ND ug/m3 03/30/16 17:31 110-54-31.1 1.49
2-Hexanone ND ug/m3 03/30/16 17:31 591-78-66.2 1.49
Methylene Chloride ND ug/m3 03/30/16 17:31 75-09-25.3 1.49
4-Methyl-2-pentanone (MIBK)ND ug/m3 03/30/16 17:31 108-10-16.2 1.49
Methyl-tert-butyl ether ND ug/m3 03/30/16 17:31 1634-04-45.5 1.49
Naphthalene ND ug/m3 03/30/16 17:31 91-20-37.9 1.49
Propylene ND ug/m3 03/30/16 17:31 115-07-11.3 1.49
Styrene ND ug/m3 03/30/16 17:31 100-42-53.2 1.49
1,1,2,2-Tetrachloroethane ND ug/m3 03/30/16 17:31 79-34-55.2 1.49
Tetrachloroethene ND ug/m3 03/30/16 17:31 127-18-41.0 1.49
Tetrahydrofuran ND ug/m3 03/30/16 17:31 109-99-92.2 1.49
Toluene ND ug/m3 03/30/16 17:31 108-88-31.1 1.49
1,2,4-Trichlorobenzene ND ug/m3 03/30/16 17:31 120-82-111.2 1.49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/31/2016 05:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291329
Mt Hope - N108-02
Sample:Shop #2 Lab ID:92291329002 Collected:03/24/16 14:15 Received:03/24/16 14:55 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 03/30/16 17:31 71-55-61.7 1.49
1,1,2-Trichloroethane ND ug/m3 03/30/16 17:31 79-00-50.82 1.49
Trichloroethene ND ug/m3 03/30/16 17:31 79-01-60.82 1.49
Trichlorofluoromethane ND ug/m3 03/30/16 17:31 75-69-41.7 1.49
1,1,2-Trichlorotrifluoroethane ND ug/m3 03/30/16 17:31 76-13-12.4 1.49
1,2,4-Trimethylbenzene ND ug/m3 03/30/16 17:31 95-63-63.7 1.49
1,3,5-Trimethylbenzene ND ug/m3 03/30/16 17:31 108-67-81.5 1.49
Vinyl acetate ND ug/m3 03/30/16 17:31 108-05-41.1 1.49
Vinyl chloride ND ug/m3 03/30/16 17:31 75-01-40.39 1.49
m&p-Xylene ND ug/m3 03/30/16 17:31 179601-23-12.6 1.49
o-Xylene ND ug/m3 03/30/16 17:31 95-47-61.3 1.49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/31/2016 05:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291329
Mt Hope - N108-02
Sample:Shop #3 Lab ID:92291329003 Collected:03/24/16 14:16 Received:03/24/16 14:55 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 16.0 ug/m3 03/30/16 18:03 67-64-13.7 1.55
Benzene ND ug/m3 03/30/16 18:03 71-43-21.0 1.55
Bromodichloromethane ND ug/m3 03/30/16 18:03 75-27-42.1 1.55
Bromoform ND ug/m3 03/30/16 18:03 75-25-23.3 1.55
Bromomethane ND ug/m3 03/30/16 18:03 74-83-91.2 1.55
1,3-Butadiene ND ug/m3 03/30/16 18:03 106-99-00.70 1.55
2-Butanone (MEK)ND ug/m3 03/30/16 18:03 78-93-34.6 1.55
Carbon disulfide ND ug/m3 03/30/16 18:03 75-15-00.98 1.55
Carbon tetrachloride ND ug/m3 03/30/16 18:03 56-23-50.99 1.55
Chlorobenzene ND ug/m3 03/30/16 18:03 108-90-71.5 1.55
Chloroethane ND ug/m3 03/30/16 18:03 75-00-30.84 1.55
Chloroform ND ug/m3 03/30/16 18:03 67-66-31.5 1.55
Chloromethane 0.87 ug/m3 03/30/16 18:03 74-87-30.65 1.55
Cyclohexane ND ug/m3 03/30/16 18:03 110-82-71.1 1.55
Dibromochloromethane ND ug/m3 03/30/16 18:03 124-48-12.7 1.55
1,2-Dibromoethane (EDB)ND ug/m3 03/30/16 18:03 106-93-42.4 1.55
1,2-Dichlorobenzene ND ug/m3 03/30/16 18:03 95-50-11.9 1.55
1,3-Dichlorobenzene ND ug/m3 03/30/16 18:03 541-73-14.7 1.55
1,4-Dichlorobenzene ND ug/m3 03/30/16 18:03 106-46-71.9 1.55
Dichlorodifluoromethane 2.0 ug/m3 03/30/16 18:03 75-71-81.6 1.55
1,1-Dichloroethane ND ug/m3 03/30/16 18:03 75-34-31.3 1.55
1,2-Dichloroethane ND ug/m3 03/30/16 18:03 107-06-20.64 1.55
1,1-Dichloroethene ND ug/m3 03/30/16 18:03 75-35-41.3 1.55
cis-1,2-Dichloroethene ND ug/m3 03/30/16 18:03 156-59-21.3 1.55
trans-1,2-Dichloroethene ND ug/m3 03/30/16 18:03 156-60-51.3 1.55
1,2-Dichloropropane ND ug/m3 03/30/16 18:03 78-87-51.5 1.55
cis-1,3-Dichloropropene ND ug/m3 03/30/16 18:03 10061-01-53.6 1.55
trans-1,3-Dichloropropene ND ug/m3 03/30/16 18:03 10061-02-63.6 1.55
Dichlorotetrafluoroethane ND ug/m3 03/30/16 18:03 76-14-22.2 1.55
Ethyl acetate ND ug/m3 03/30/16 18:03 141-78-61.1 1.55
Ethylbenzene ND ug/m3 03/30/16 18:03 100-41-41.4 1.55
4-Ethyltoluene ND ug/m3 03/30/16 18:03 622-96-81.6 1.55
n-Heptane ND ug/m3 03/30/16 18:03 142-82-51.3 1.55
Hexachloro-1,3-butadiene ND ug/m3 03/30/16 18:03 87-68-316.8 1.55
n-Hexane ND ug/m3 03/30/16 18:03 110-54-31.1 1.55
2-Hexanone ND ug/m3 03/30/16 18:03 591-78-66.5 1.55
Methylene Chloride ND ug/m3 03/30/16 18:03 75-09-25.5 1.55
4-Methyl-2-pentanone (MIBK)ND ug/m3 03/30/16 18:03 108-10-16.5 1.55
Methyl-tert-butyl ether ND ug/m3 03/30/16 18:03 1634-04-45.7 1.55
Naphthalene ND ug/m3 03/30/16 18:03 91-20-38.3 1.55
Propylene ND ug/m3 03/30/16 18:03 115-07-11.4 1.55
Styrene ND ug/m3 03/30/16 18:03 100-42-53.4 1.55
1,1,2,2-Tetrachloroethane ND ug/m3 03/30/16 18:03 79-34-55.4 1.55
Tetrachloroethene ND ug/m3 03/30/16 18:03 127-18-41.1 1.55
Tetrahydrofuran ND ug/m3 03/30/16 18:03 109-99-92.3 1.55
Toluene ND ug/m3 03/30/16 18:03 108-88-31.2 1.55
1,2,4-Trichlorobenzene ND ug/m3 03/30/16 18:03 120-82-111.7 1.55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/31/2016 05:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291329
Mt Hope - N108-02
Sample:Shop #3 Lab ID:92291329003 Collected:03/24/16 14:16 Received:03/24/16 14:55 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 03/30/16 18:03 71-55-61.7 1.55
1,1,2-Trichloroethane ND ug/m3 03/30/16 18:03 79-00-50.85 1.55
Trichloroethene ND ug/m3 03/30/16 18:03 79-01-60.85 1.55
Trichlorofluoromethane ND ug/m3 03/30/16 18:03 75-69-41.8 1.55
1,1,2-Trichlorotrifluoroethane ND ug/m3 03/30/16 18:03 76-13-12.5 1.55
1,2,4-Trimethylbenzene ND ug/m3 03/30/16 18:03 95-63-63.9 1.55
1,3,5-Trimethylbenzene ND ug/m3 03/30/16 18:03 108-67-81.5 1.55
Vinyl acetate ND ug/m3 03/30/16 18:03 108-05-41.1 1.55
Vinyl chloride ND ug/m3 03/30/16 18:03 75-01-40.40 1.55
m&p-Xylene ND ug/m3 03/30/16 18:03 179601-23-12.7 1.55
o-Xylene ND ug/m3 03/30/16 18:03 95-47-61.4 1.55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/31/2016 05:41 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291329
Mt Hope - N108-02
Sample:Office #1 Lab ID:92291329004 Collected:03/24/16 14:13 Received:03/24/16 14:55 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 28.9 ug/m3 03/30/16 18:34 67-64-13.6 1.49
Benzene ND ug/m3 03/30/16 18:34 71-43-20.97 1.49
Bromodichloromethane ND ug/m3 03/30/16 18:34 75-27-42.0 1.49
Bromoform ND ug/m3 03/30/16 18:34 75-25-23.1 1.49
Bromomethane ND ug/m3 03/30/16 18:34 74-83-91.2 1.49
1,3-Butadiene ND ug/m3 03/30/16 18:34 106-99-00.67 1.49
2-Butanone (MEK)5.7 ug/m3 03/30/16 18:34 78-93-34.5 1.49
Carbon disulfide ND ug/m3 03/30/16 18:34 75-15-00.94 1.49
Carbon tetrachloride ND ug/m3 03/30/16 18:34 56-23-50.95 1.49
Chlorobenzene ND ug/m3 03/30/16 18:34 108-90-71.4 1.49
Chloroethane ND ug/m3 03/30/16 18:34 75-00-30.80 1.49
Chloroform ND ug/m3 03/30/16 18:34 67-66-31.5 1.49
Chloromethane 1.0 ug/m3 03/30/16 18:34 74-87-30.63 1.49
Cyclohexane 2.0 ug/m3 03/30/16 18:34 110-82-71.0 1.49
Dibromochloromethane ND ug/m3 03/30/16 18:34 124-48-12.6 1.49
1,2-Dibromoethane (EDB)ND ug/m3 03/30/16 18:34 106-93-42.3 1.49
1,2-Dichlorobenzene ND ug/m3 03/30/16 18:34 95-50-11.8 1.49
1,3-Dichlorobenzene ND ug/m3 03/30/16 18:34 541-73-14.6 1.49
1,4-Dichlorobenzene ND ug/m3 03/30/16 18:34 106-46-71.8 1.49
Dichlorodifluoromethane 2.0 ug/m3 03/30/16 18:34 75-71-81.5 1.49
1,1-Dichloroethane ND ug/m3 03/30/16 18:34 75-34-31.2 1.49
1,2-Dichloroethane ND ug/m3 03/30/16 18:34 107-06-20.61 1.49
1,1-Dichloroethene ND ug/m3 03/30/16 18:34 75-35-41.2 1.49
cis-1,2-Dichloroethene ND ug/m3 03/30/16 18:34 156-59-21.2 1.49
trans-1,2-Dichloroethene ND ug/m3 03/30/16 18:34 156-60-51.2 1.49
1,2-Dichloropropane ND ug/m3 03/30/16 18:34 78-87-51.4 1.49
cis-1,3-Dichloropropene ND ug/m3 03/30/16 18:34 10061-01-53.4 1.49
trans-1,3-Dichloropropene ND ug/m3 03/30/16 18:34 10061-02-63.4 1.49
Dichlorotetrafluoroethane ND ug/m3 03/30/16 18:34 76-14-22.1 1.49
Ethyl acetate 2.6 ug/m3 03/30/16 18:34 141-78-61.1 1.49
Ethylbenzene ND ug/m3 03/30/16 18:34 100-41-41.3 1.49
4-Ethyltoluene ND ug/m3 03/30/16 18:34 622-96-81.5 1.49
n-Heptane ND ug/m3 03/30/16 18:34 142-82-51.2 1.49
Hexachloro-1,3-butadiene ND ug/m3 03/30/16 18:34 87-68-316.2 1.49
n-Hexane 8.1 ug/m3 03/30/16 18:34 110-54-31.1 1.49
2-Hexanone ND ug/m3 03/30/16 18:34 591-78-66.2 1.49
Methylene Chloride 8.3 ug/m3 03/30/16 18:34 75-09-25.3 1.49
4-Methyl-2-pentanone (MIBK)ND ug/m3 03/30/16 18:34 108-10-16.2 1.49
Methyl-tert-butyl ether ND ug/m3 03/30/16 18:34 1634-04-45.5 1.49
Naphthalene ND ug/m3 03/30/16 18:34 91-20-37.9 1.49
Propylene 1.6 ug/m3 03/30/16 18:34 115-07-11.3 1.49
Styrene ND ug/m3 03/30/16 18:34 100-42-53.2 1.49
1,1,2,2-Tetrachloroethane ND ug/m3 03/30/16 18:34 79-34-55.2 1.49
Tetrachloroethene ND ug/m3 03/30/16 18:34 127-18-41.0 1.49
Tetrahydrofuran 3.3 ug/m3 03/30/16 18:34 109-99-92.2 1.49
Toluene 11.5 ug/m3 03/30/16 18:34 108-88-31.1 1.49
1,2,4-Trichlorobenzene ND ug/m3 03/30/16 18:34 120-82-111.2 1.49
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/31/2016 05:41 PM
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Page 10 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92291329
Mt Hope - N108-02
Sample:Office #1 Lab ID:92291329004 Collected:03/24/16 14:13 Received:03/24/16 14:55 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 03/30/16 18:34 71-55-61.7 1.49
1,1,2-Trichloroethane ND ug/m3 03/30/16 18:34 79-00-50.82 1.49
Trichloroethene 1.8 ug/m3 03/30/16 18:34 79-01-60.82 1.49
Trichlorofluoromethane ND ug/m3 03/30/16 18:34 75-69-41.7 1.49
1,1,2-Trichlorotrifluoroethane ND ug/m3 03/30/16 18:34 76-13-12.4 1.49
1,2,4-Trimethylbenzene ND ug/m3 03/30/16 18:34 95-63-63.7 1.49
1,3,5-Trimethylbenzene ND ug/m3 03/30/16 18:34 108-67-81.5 1.49
Vinyl acetate ND ug/m3 03/30/16 18:34 108-05-41.1 1.49
Vinyl chloride ND ug/m3 03/30/16 18:34 75-01-40.39 1.49
m&p-Xylene 2.8 ug/m3 03/30/16 18:34 179601-23-12.6 1.49
o-Xylene ND ug/m3 03/30/16 18:34 95-47-61.3 1.49
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/31/2016 05:41 PM
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Page 11 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92291329
Mt Hope - N108-02
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
AIR/25568
TO-15
TO-15
TO15 MSV AIR Low Level
Associated Lab Samples:92291329001, 92291329002, 92291329003, 92291329004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2219906
Associated Lab Samples:92291329001, 92291329002, 92291329003, 92291329004
Matrix:Air
Analyzed
1,1,1-Trichloroethane ug/m3 ND 1.1 03/30/16 08:32
1,1,2,2-Tetrachloroethane ug/m3 ND 3.5 03/30/16 08:32
1,1,2-Trichloroethane ug/m3 ND 0.55 03/30/16 08:32
1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.6 03/30/16 08:32
1,1-Dichloroethane ug/m3 ND 0.82 03/30/16 08:32
1,1-Dichloroethene ug/m3 ND 0.81 03/30/16 08:32
1,2,4-Trichlorobenzene ug/m3 ND 7.5 03/30/16 08:32
1,2,4-Trimethylbenzene ug/m3 ND 2.5 03/30/16 08:32
1,2-Dibromoethane (EDB)ug/m3 ND 1.6 03/30/16 08:32
1,2-Dichlorobenzene ug/m3 ND 1.2 03/30/16 08:32
1,2-Dichloroethane ug/m3 ND 0.41 03/30/16 08:32
1,2-Dichloropropane ug/m3 ND 0.94 03/30/16 08:32
1,3,5-Trimethylbenzene ug/m3 ND 1.0 03/30/16 08:32
1,3-Butadiene ug/m3 ND 0.45 03/30/16 08:32
1,3-Dichlorobenzene ug/m3 ND 3.1 03/30/16 08:32
1,4-Dichlorobenzene ug/m3 ND 1.2 03/30/16 08:32
2-Butanone (MEK)ug/m3 ND 3.0 03/30/16 08:32
2-Hexanone ug/m3 ND 4.2 03/30/16 08:32
4-Ethyltoluene ug/m3 ND 1.0 03/30/16 08:32
4-Methyl-2-pentanone (MIBK)ug/m3 ND 4.2 03/30/16 08:32
Acetone ug/m3 ND 2.4 03/30/16 08:32
Benzene ug/m3 ND 0.65 03/30/16 08:32
Bromodichloromethane ug/m3 ND 1.4 03/30/16 08:32
Bromoform ug/m3 ND 2.1 03/30/16 08:32
Bromomethane ug/m3 ND 0.79 03/30/16 08:32
Carbon disulfide ug/m3 ND 0.63 03/30/16 08:32
Carbon tetrachloride ug/m3 ND 0.64 03/30/16 08:32
Chlorobenzene ug/m3 ND 0.94 03/30/16 08:32
Chloroethane ug/m3 ND 0.54 03/30/16 08:32
Chloroform ug/m3 ND 0.99 03/30/16 08:32
Chloromethane ug/m3 ND 0.42 03/30/16 08:32
cis-1,2-Dichloroethene ug/m3 ND 0.81 03/30/16 08:32
cis-1,3-Dichloropropene ug/m3 ND 2.3 03/30/16 08:32
Cyclohexane ug/m3 ND 0.70 03/30/16 08:32
Dibromochloromethane ug/m3 ND 1.7 03/30/16 08:32
Dichlorodifluoromethane ug/m3 ND 1.0 03/30/16 08:32
Dichlorotetrafluoroethane ug/m3 ND 1.4 03/30/16 08:32
Ethyl acetate ug/m3 ND 0.73 03/30/16 08:32
Ethylbenzene ug/m3 ND 0.88 03/30/16 08:32
Hexachloro-1,3-butadiene ug/m3 ND 10.8 03/30/16 08:32
m&p-Xylene ug/m3 ND 1.8 03/30/16 08:32
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/31/2016 05:41 PM
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[phone]
Page 12 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92291329
Mt Hope - N108-02
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2219906
Associated Lab Samples:92291329001, 92291329002, 92291329003, 92291329004
Matrix:Air
Analyzed
Methyl-tert-butyl ether ug/m3 ND 3.7 03/30/16 08:32
Methylene Chloride ug/m3 ND 3.5 03/30/16 08:32
n-Heptane ug/m3 ND 0.83 03/30/16 08:32
n-Hexane ug/m3 ND 0.72 03/30/16 08:32
Naphthalene ug/m3 ND 5.3 03/30/16 08:32
o-Xylene ug/m3 ND 0.88 03/30/16 08:32
Propylene ug/m3 ND 0.88 03/30/16 08:32
Styrene ug/m3 ND 2.2 03/30/16 08:32
Tetrachloroethene ug/m3 ND 0.69 03/30/16 08:32
Tetrahydrofuran ug/m3 ND 1.5 03/30/16 08:32
Toluene ug/m3 ND 0.77 03/30/16 08:32
trans-1,2-Dichloroethene ug/m3 ND 0.81 03/30/16 08:32
trans-1,3-Dichloropropene ug/m3 ND 2.3 03/30/16 08:32
Trichloroethene ug/m3 ND 0.55 03/30/16 08:32
Trichlorofluoromethane ug/m3 ND 1.1 03/30/16 08:32
Vinyl acetate ug/m3 ND 0.72 03/30/16 08:32
Vinyl chloride ug/m3 ND 0.26 03/30/16 08:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2219907LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 53.655.5 97 60-143
1,1,2,2-Tetrachloroethane ug/m3 84.169.8 120 49-150
1,1,2-Trichloroethane ug/m3 55.355.5 100 57-149
1,1,2-Trichlorotrifluoroethane ug/m3 68.077.9 87 66-131
1,1-Dichloroethane ug/m3 38.641.2 94 62-139
1,1-Dichloroethene ug/m3 36.440.3 90 62-135
1,2,4-Trichlorobenzene ug/m3 85.375.5 113 55-146
1,2,4-Trimethylbenzene ug/m3 54.850 110 57-143
1,2-Dibromoethane (EDB)ug/m3 87.278.1 112 63-150
1,2-Dichlorobenzene ug/m3 66.961.2 109 57-141
1,2-Dichloroethane ug/m3 39.041.2 95 61-144
1,2-Dichloropropane ug/m3 47.747 101 63-144
1,3,5-Trimethylbenzene ug/m3 54.750 109 54-147
1,3-Butadiene ug/m3 20.022.5 89 61-140
1,3-Dichlorobenzene ug/m3 68.261.2 112 51-150
1,4-Dichlorobenzene ug/m3 78.361.2 128 57-143
2-Butanone (MEK)ug/m3 151150 101 66-144
2-Hexanone ug/m3 237208 114 63-147
4-Ethyltoluene ug/m3 54.350 109 56-150
4-Methyl-2-pentanone (MIBK)ug/m3 211208 101 58-150
Acetone ug/m3 127121 105 46-140
Benzene ug/m3 33.932.5 104 62-141
Bromodichloromethane ug/m3 70.268.2 103 58-149
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/31/2016 05:41 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 13 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92291329
Mt Hope - N108-02
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2219907LABORATORY CONTROL SAMPLE:
LCSSpike
Bromoform ug/m3 108105 103 61-150
Bromomethane ug/m3 34.539.5 87 58-136
Carbon disulfide ug/m3 28.831.7 91 59-135
Carbon tetrachloride ug/m3 75.064 117 60-149
Chlorobenzene ug/m3 50.846.8 109 60-150
Chloroethane ug/m3 22.626.8 84 61-136
Chloroform ug/m3 46.249.7 93 65-138
Chloromethane ug/m3 19.521 93 62-133
cis-1,2-Dichloroethene ug/m3 41.040.3 102 65-139
cis-1,3-Dichloropropene ug/m3 50.146.2 109 61-149
Cyclohexane ug/m3 40.335 115 64-134
Dibromochloromethane ug/m3 10986.6 126 59-150
Dichlorodifluoromethane ug/m3 46.150.3 92 63-134
Dichlorotetrafluoroethane ug/m3 65.071.1 91 62-134
Ethyl acetate ug/m3 37.236.6 102 55-146
Ethylbenzene ug/m3 47.944.2 109 59-149
Hexachloro-1,3-butadiene ug/m3 143108 132 42-150
m&p-Xylene ug/m3 91.388.3 103 59-146
Methyl-tert-butyl ether ug/m3 180183 98 64-135
Methylene Chloride ug/m3 155177 88 64-128
n-Heptane ug/m3 47.141.7 113 64-140
n-Hexane ug/m3 43.335.8 121 50-138
Naphthalene ug/m3 53.153.3 100 46-146
o-Xylene ug/m3 45.944.2 104 54-149
Propylene ug/m3 18.117.5 103 58-135
Styrene ug/m3 46.043.3 106 54-150
Tetrachloroethene ug/m3 73.769 107 60-142
Tetrahydrofuran ug/m3 32.330 108 56-143
Toluene ug/m3 41.138.3 107 61-138
trans-1,2-Dichloroethene ug/m3 39.540.3 98 67-137
trans-1,3-Dichloropropene ug/m3 46.746.2 101 59-145
Trichloroethene ug/m3 56.254.6 103 60-144
Trichlorofluoromethane ug/m3 50.757.1 89 59-134
Vinyl acetate ug/m3 40.035.8 112 55-143
Vinyl chloride ug/m3 24.526 94 63-135
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/31/2016 05:41 PM
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[phone]
Page 14 of 17
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92291329
Mt Hope - N108-02
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - MinneapolisPASI-M
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/31/2016 05:41 PM
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[phone]
Page 15 of 17
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92291329
Mt Hope - N108-02
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92291329001 AIR/25568Shop #1 TO-15
92291329002 AIR/25568Shop #2 TO-15
92291329003 AIR/25568Shop #3 TO-15
92291329004 AIR/25568Office #1 TO-15
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/31/2016 05:41 PM
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Huntersville, NC 28078
[phone]
Page 16 of 17
Page 17 of 17