20089_Hendrick_Auto_ Soil-GW_Assmt_Rpt_20150323

Report of Additional Soil and Groundwater Assessment
Hendrick Durham Auto Mall
Durham, Durham County, North Carolina
ECS Project: 06:22255-A_Rev-1
March 23, 2015

1

TABLE OF CONTENTS

1. EXECUTIVE SUMMARY ....................................................................................................... 2
2. BACKGROUND INFORMATION ........................................................................................... 5
3. FIELD ACTIVITIES ................................................................................................................ 5
4. LABORATORY ANALYSIS .................................................................................................... 7
5. CONCLUSIONS .................................................................................................................... 8
6. RECOMMENDATIONS ......................................................................................................... 9
7. QUALIFICATIONS OF REPORT ........................................................................................... 9

FIGURES Figure 1 – Site Location Map
Figure 2 – Soil and Groundwater Sample Location Map
Figure 3 – Groundwater Sample Location Map

TABLES Table 1 – Summary of Soil Sample Analytical Results
Table 2 – Summary of Groundwater Analytical Results

APPENDIX Laboratory Test Reports and Chain of Custody Records

Report of Additional Soil and Groundwater Assessment
Hendrick Durham Auto Mall
Durham, Durham County, North Carolina
ECS Project: 06:22255-A_Rev-1
March 23, 2015

1. EXECUTIVE SUMMARY

The subject site is known as the Hendrick Durham Auto Mall site and is located at 409 South
Roxboro Street and 464 East Pettigrew Street in Durham, Durham County, North Carolina
(Figure 1). The site consists of 12.076 acres of land and is currently developed with the
Hendrick Durham Auto Mall and associated parking lots.

ECS previously conducted a Phase I Environmental Site Assessment (ESA) for the site (ECS
Project No. 06:21380). ECS identified the following recognized environmental conditions (RECs)
with respect to the subject site:

 The documented releases associated with the former use of the site as a hosiery mill
and a printing facility;
 The current use of the site as an automotive dealership and maintenance facility; and
 The historical use of surrounding properties as auto repair facilities, dry cleaning
facilities, and industrial uses.
The Phase I ESA also identified the following Controlled Recognized Environmental Conditions
(CRECs):
 The documented releases associated with the subject site.
Based on the results of the Phase I ESA, ECS conducted a Phase II ESA dated February 28,
2014 (ECS Project No. 06:21308-B). Based on the field observation and laboratory analytical
results of the soil and groundwater samples collected during the Phase II ESA, a summary of
ECS’ conclusions are as follows:

 Laboratory analysis of a soil sample located in the eastern portion of the parking lot,
north of the dealership building detected benzene at a concentration that exceeds its
Soil-to-Groundwater Maximum Soil Contamination Concentrations (MSCCs). However,
the concentration does not exceed its Industrial/Commercial Soil Cleanup Levels
(ISCLs);

 Laboratory analysis of a soil sample located in the eastern portion of the parking lot,
north of the dealership building detected benzo(a)anthracene, benzo(a)pyrene,
benzo(b)floranthene, dibenzo(a,h)anthracene, indeno(1,2,3-cd)pyrene, and naphthalene
at concentrations that exceed their respective MSCCs. The concentrations of
benzo(a)anthracene, benzo(a)pyrene, benzo(b)floranthene, dibenzo(a,h)anthracene,
and indeno(1,2,3-cd)pyrene exceed their respective ISCLs; and

 Laboratory analysis of a groundwater sample located in the southwestern portion of the
parking lot north of the dealership building did not detect target volatile organic
compounds (VOCs) or semi-volatile organic compounds (SVOCs) above laboratory
reporting limits.
In an effort to determine if other areas of the subject site had been adversely impacted by routine
operations at the Hendrick Durham Auto Mall, ECS was contracted to conduct an additional soil
and groundwater assessment at the site. Project information is based on correspondence between
Report of Additional Soil and Groundwater Assessment
Hendrick Durham Auto Mall
Durham, Durham County, North Carolina
ECS Project: 06:22255-A_Rev-1
March 23, 2015

3

Mr. Eric Applefield of Durham Partnership Group, LLC., Mr. Tony Duque of NCDENR’s Brownfields
Program, Mr. Brian Smith with ECS, and the previously cited environmental assessments.
On February 3, 2015, ECS conducted a site visit to identify potential environmental concerns
not addressed by previous soil and groundwater sampling. ECS identified an oil water
separator (OWS) located along the northwestern corner of the service garage area; a floor drain
inside the oil change building; a floor drain extending the length of the service garage area; a
drum storage area located along the southeastern corner of the service garage area; an
aboveground storage tank (AST) containing gasoline located east of the service garage area;
and an anomaly marked “UST?” adjacent to the AST.

On February 28, 2015 and March 6, 2015, ECS collected 15 soil samples at the locations
described above. Three of the soil borings were advanced adjacent to the oil water separator;
one of the soil borings was advanced adjacent to the floor drain inside the oil change building;
four of the soil borings were advanced adjacent to the floor drain inside the service garage area;
two of the soil borings were advanced adjacent to the drum storage area; three soil borings
were advanced adjacent to the AST; and two of the soil borings were advanced adjacent to the
underground storage tank (UST) anomaly. The soil borings were advanced to a depth of
approximately ten feet below the ground surface (ft bgs) and/or refusal. ECS did not detect
volatile organic vapors using the photoionization detector (PID) while screening the soil
samples; therefore, the soil samples were collected from two to four ft bgs from each soil boring.

The soil samples were submitted to Pace Analytical Services, Inc. (Pace) for chemical analysis
for total petroleum hydrocarbons (TPH) diesel range organics (DRO) using EPA Method 8015
and VOCs. Additionally, six of the soil samples were analyzed for RCRA metals.

The laboratory reported TPH-DRO at concentrations above the UST Section’s Action Level in
the soil samples collected from one location near the OWS, one location near floor drain inside
the oil change building, two locations near the location of the AST, and two locations located
near the anomaly marked “UST?” adjacent to the AST.

The laboratory did not report VOCs at concentrations above the laboratory reporting limits in the
soil samples collected from the site.

The laboratory reported chromium at concentrations above the Inactive Hazardous Sites Branch
(IHSB) Residential and Industrial Preliminary Soil Remediation Goals (PSRGs) in the soil samples
collected at two locations along the floor drain extending the length of the service garage area,
one soil sample located near the AST, and one soil sample located near the anomaly marked
“UST?” adjacent to the AST.

The laboratory reported lead at concentrations above the IHSB Residential and Industrial PSRGs
in the soil samples collected from one location near the eastern end of the floor drain within the
service garage area and one location near the OWS.

Subsequently, five temporary monitoring wells were installed at the site. One boring was
advanced along the floor drain inside the Service Garage Area, one boring was advanced at the
Oil Change Garage, one boring was advanced at the OWS, one boring was advanced at the
Collision Center, and one boring was advanced in the northeastern portion of the adjacent
Report of Additional Soil and Groundwater Assessment
Hendrick Durham Auto Mall
Durham, Durham County, North Carolina
ECS Project: 06:22255-A_Rev-1
March 23, 2015

4

parking lot. The temporary monitoring wells were drilled to depths ranging from 10 ft bgs to 25 ft
bgs and were constructed using one-inch inner diameter Schedule 40 PVC flush-threaded casing
and screen.

The temporary groundwater monitoring wells were developed by purging approximately three well
volumes or until dryness using a peristaltic pump and tubing dedicated to each well. After
development was completed, groundwater samples were collected from the wells. Immediately
after collection, the groundwater samples were transferred into sample containers provided by the
laboratory. The samples were submitted to Pace for chemical analysis for VOCs and SVOCs.

The laboratory reported several VOCs at concentrations below their respective North Carolina
2L Groundwater Quality Standards (NC2LGWQS) in groundwater samples collected from TMW-
1 through TMW-5.

The laboratory reported bis(2-ethylhexyl)phthalate at a concentration above its NC2LGWQS in
the groundwater sample collected from TMW-3. Bis(2-ethylhexyl)pthalate is common artifact
prevalent in plastics, such as PVC, tubing, and nitrile gloves; therefore, ECS does not believe
that bis(2-ethylhexyl)phthalate is a contaminant of concern at the subject site.

The laboratory did not report additional SVOCs at concentrations above their respective
laboratory reporting limits in the groundwater samples collected from the site monitoring wells.

Upon completion, each groundwater boring was properly abandoned.

Based on the results of the soil and groundwater assessment activities, ECS recommends the
following:

 ECS recommends that if future grading or excavation activities are planned at the site, the
soils at the following locations should be monitored for possible petroleum impacts; the soil
sample located near floor drain inside the oil change building (SS-1), the soil samples
located near the UST anomaly (SS-8 and SS-10), the soil samples located near the AST
(SS-11 and SS-12), and the soil sample located near the OWS (SS-13);

 Chromium and lead were reported at concentrations above their respective IHSB
Residential and Industrial PSRGs. However, the detections are consistent with naturally
occurring metals in soils in this general area.

 Additional groundwater assessment does not appear necessary at the site and is not
recommended at this time;

 ECS recommends updating the Environmental Management Plan (EMP) to include the
information from this report; and

 ECS recommends that a copy of this report be retained by the property owner to document
assessment activities.

Report of Additional Soil and Groundwater Assessment
Hendrick Durham Auto Mall
Durham, Durham County, North Carolina
ECS Project: 06:22255-A_Rev-1
March 23, 2015

5

2. BACKGROUND INFORMATION

The subject site is known as the Hendrick Durham Auto Mall site and is located at 409 South
Roxboro Street and 464 East Pettigrew Street in Durham, Durham County, North Carolina
(Figure 1). The site consists of 12.076-acres of land and is currently developed with the
Hendrick Durham Auto Mall and associated parking lots.

ECS previously conducted a Phase I ESA for the site (ECS Project No. 06:21380). ECS
identified the following RECs with respect to the subject site:

 The documented releases associated with the former use of the site as a hosiery mill
and a printing facility;
 The current use of the site as an automotive dealership and maintenance facility; and
 The historical use of surrounding properties as auto repair facilities, dry cleaning
facilities, and industrial uses.
The Phase I ESA also identified the following Controlled Recognized Environmental Conditions
(CRECs):
 The documented releases associated with the subject site.
Based on the results of the Phase I ESA, ECS conducted a Phase II ESA dated February 28,
2014 (ECS Project No. 06:21308-B). Based on the field observation and laboratory analytical
results of the soil and groundwater samples collected during the Phase II ESA, a summary of
ECS’ conclusions are as follows:
 Laboratory analysis of a soil sample located in the eastern portion of the parking lot,
north of the dealership building detected benzene at a concentration that exceeds its
Soil-to-Groundwater MSCCs. However, the concentration does not exceed its ISCLs;

 Laboratory analysis of a soil sample located in the eastern portion of the parking lot,
north of the dealership building detected benzo(a)anthracene, benzo(a)pyrene,
benzo(b)floranthene, dibenzo(a,h)anthracene, indeno(1,2,3-cd)pyrene, and naphthalene
at concentrations that exceed their respective MSCCs. The concentrations of
benzo(a)anthracene, benzo(a)pyrene, benzo(b)floranthene, dibenzo(a,h)anthracene,
and indeno(1,2,3-cd)pyrene exceed their respective ISCLs; and

 Laboratory analysis of a groundwater sample located in the southwestern portion of the
parking lot north of the dealership building did not detect target VOCs or SVOCs above
laboratory reporting limits.
In an effort to determine if other areas of the subject site had been adversely impacted by routine
operations at the Hendrick Durham Auto Mall, ECS was contracted to conduct an additional soil
and groundwater assessment at the site. Project information is based on correspondence between
Mr. Eric Applefield of Durham Partnership Group, LLC., Mr. Tony Duque of NCDENR’s Brownfields
Program, Mr. Brian Smith with ECS, and the previously cited environmental assessments.

Report of Additional Soil and Groundwater Assessment
Hendrick Durham Auto Mall
Durham, Durham County, North Carolina
ECS Project: 06:22255-A_Rev-1
March 23, 2015

6

3. FIELD ACTIVITIES

On February 3, 2015, ECS conducted a site visit to identify potential environmental concerns
not addressed by previous soil and groundwater sampling. ECS identified an OWS located
along the northwestern corner of the service garage area; a floor drain inside the oil change
building; a floor drain extending the length of the service garage area; a drum storage area
located along the southeastern corner of the service garage area; an AST containing gasoline
located east of the service garage area; and an anomaly marked “UST?” adjacent to the AST.

On February 28, 2015 and March 6, 2015, ECS collected 15 soil samples (SS-1 through SS-15)
at the site (Figure 2). Three of the soil borings were advanced adjacent to the oil water
separator; one of the soil borings was advanced adjacent to the floor drain inside the oil change
building; four of the soil borings were advanced adjacent to the floor drain inside the service
garage area; two of the soil borings were advanced adjacent to the drum storage area; three
soil borings were advanced adjacent to the AST; and two of the soil borings were advanced
adjacent to the UST anomaly. The soil borings were advanced using a Geoprobe® equipped
with direct-push technology to a depth of approximately ten feet below the ground surface (ft bgs)
and/or Geoprobe® refusal. ECS did not detect volatile organic vapors using the photoionization
detector (PID) while screening the soil samples; therefore, the soil samples were collected from
two to four ft bgs from each soil boring.

The sample containers were labeled with ECS project number, sample identification, sample
date and time, and requested analytical analysis. The containers were placed into protective
packaging material and placed into a cooler with ice to maintain the samples at approximately 4
C. The samples were submitted to Pace for analysis for TPH DRO using EPA Method 8015
and VOCs using EPA Method 8260. Additionally, soil samples SS-2, SS-4, SS-6, SS-9, SS-11,
and SS-14 were analyzed for RCRA metals using EPA Method 6010. ECS maintained proper
Chain-of-Custody (COC) procedures throughout the sample collection and transportation process.

Subsequently, five temporary monitoring wells (TMW-1 through TMW-5) were installed at the site
(Figures 2 and 3). One boring was advanced along the floor drain inside the Service Garage
Area, one boring was advanced at the Oil Change Garage, one boring was advanced at the
OWS, one boring was advanced at the Collision Center, and one boring was advanced in the
northeastern portion of the adjacent parking lot. The temporary monitoring wells were drilled to
depths ranging from 10 ft bgs to 25 ft bgs using a Geoprobe® equipped with augers and/or air
rotary. The temporary wells were constructed using one-inch inner diameter Schedule 40 PVC
flush-threaded casing and screen.

ECS was not able to collect a second groundwater sample along the floor drain located inside the
Service Garage Area due to auger refusal. ECS was unable to utilize air rotary at this location due
to the Service Garage still being in operation.

The temporary groundwater monitoring wells were developed by purging approximately three well
volumes or until dryness using a peristaltic pump and tubing dedicated to each well. After
development was completed, groundwater samples were collected from the wells. Immediately
after collection, the groundwater samples were transferred into sample containers provided by the
laboratory.

Report of Additional Soil and Groundwater Assessment
Hendrick Durham Auto Mall
Durham, Durham County, North Carolina
ECS Project: 06:22255-A_Rev-1
March 23, 2015

7

The sample containers were labeled with ECS project number, sample identification, sample
date and time, and requested analytical analysis. The containers were placed into protective
packaging material and placed into a cooler with ice to maintain the samples at approximately 4
C. The samples were submitted to Pace for chemical analysis for VOCs using EPA Method
8260 and SVOCs using EPA Method 8270. ECS maintained proper COC procedures throughout
the sample collection and transportation process.

Upon completion, each groundwater boring was properly abandoned.

4. LABORATORY ANALYSIS

The laboratory reported TPH-DRO at concentrations above the UST Section’s Action Level of
10 mg/kg in the soil samples collected from SS-1, SS-8, SS-10, SS-11, SS-12, and SS-13.

The laboratory reported TPH-DRO at a concentration above the laboratory reporting limit but
below the UST Section’s Action Level in the soil sample collected from SS-5.

The laboratory did not report VOCs at concentrations above the laboratory reporting limits in the
soil samples collected from the site.

The laboratory reported chromium at concentrations above the Inactive Hazardous Sites Branch
(IHSB) Residential and Industrial PSRGs in the soil samples collected from SS-2, SS-4, SS-9, and
SS-11.

The laboratory reported lead at concentrations above the IHSB Residential and Industrial PSRGs
in the soil samples collected from SS-4 and SS-14.

The laboratory reported several additional metals at concentrations above their respective
laboratory reporting limits but below their respective IHSB Residential PSRGs.

The laboratory reported several VOCs at concentrations above their respective laboratory
reporting limits but below their respective NC2LGWQS in groundwater samples collected from
TMW-1 and TMW-4.

The laboratory did not report VOCs at concentrations above their respective laboratory reporting
limits in the groundwater samples collected from TMW-2, TMW-3, and TMW-5.

The laboratory reported bis(2-ethylhexyl)phthalate at a concentration above its NC2LGWQS in
the groundwater sample collected from TMW-3. Bis(2-ethylhexyl)pthalate is common artifact
prevalent in plastics, such as PVC, tubing, and nitrile gloves; therefore, ECS does not believe
that bis(2-ethylhexyl)phthalate is a contaminant of concern at the subject site.

The laboratory did not report additional SVOCs at concentrations above their respective
laboratory reporting limits in the groundwater samples collected from the site monitoring wells.

A summary of the laboratory analytical results is included in Tables 1 and 2.

The laboratory test report and COC are included in Appendix A.
Report of Additional Soil and Groundwater Assessment
Hendrick Durham Auto Mall
Durham, Durham County, North Carolina
ECS Project: 06:22255-A_Rev-1
March 23, 2015

8

5. CONCLUSIONS

Based on the field observation and laboratory analytical results of the soil and groundwater
samples collected during this assessment, ECS concludes the following:

 The laboratory reported TPH-DRO at concentrations above the UST Section’s Action
Level in the soil samples collected from one location near the OWS (SS-13), one
location near floor drain inside the oil change building (SS-1), two locations near the
location of the AST (SS-11 and SS-12), and two locations located near the anomaly
marked “UST?” adjacent to the AST (SS-8, SS-10).

 The laboratory reported TPH-DRO at a concentration above the laboratory reporting limit
but below the UST Section’s Action Level in the soil sample collected from SS-5;

 The laboratory did not report VOCs at concentrations above the laboratory reporting
limits in the soil samples collected from the site;

 The laboratory reported chromium at concentrations above the Inactive Hazardous Sites
Branch (IHSB) Residential and Industrial PSRGs in the soil samples collected from SS-2,
SS-4, SS-9, and SS-11;

 The laboratory reported lead at concentrations above the IHSB Residential and Industrial
PSRGs in the soil samples collected from SS-4 and SS-14;

 The laboratory reported several additional metals at concentrations above their respective
laboratory reporting limits but below their respective IHSB Residential PSRGs;

 The laboratory did not report VOCs at concentrations above their respective
NC2LGWQS in the groundwater samples collected from the site;

 The laboratory reported bis(2-ethylhexyl)phthalate at a concentration above its
NC2LGWQS in the groundwater sample collected from TMW-3. Bis(2-
ethylhexyl)pthalate is common artifact prevalent in plastics, such as PVC, tubing, and
nitrile gloves; therefore, ECS does not believe that bis(2-ethylhexyl)phthalate is a
contaminant of concern at the subject site; and

 The laboratory did not report additional SVOCs at concentrations above their respective
laboratory reporting limits in the groundwater samples collected from the site monitoring
wells.

Report of Additional Soil and Groundwater Assessment
Hendrick Durham Auto Mall
Durham, Durham County, North Carolina
ECS Project: 06:22255-A_Rev-1
March 23, 2015

9

6. RECOMMENDATIONS

Based on the results of the soil and groundwater assessment activities, ECS recommends the
following:

 ECS recommends that if future grading or excavation activities are planned at the site, the
soils at the following locations should be monitored for possible petroleum impacts; the soil
sample located near floor drain inside the oil change building (SS-1), the soil samples
located near the UST anomaly (SS-8 and SS-10), the soil samples located near the AST
(SS-11 and SS-12), and the soil sample located near the OWS (SS-13);

 Chromium and lead were reported at concentrations above their respective IHSB
Residential and Industrial PSRGs. However, the detections are consistent with naturally
occurring metals in soils in this general area.

 Additional groundwater assessment does not appear necessary at the site and is not
recommended at this time;

 ECS recommends updating the Environmental Management Plan (EMP) to include the
information from this report; and

 ECS recommends that a copy of this report be retained by the property owner to document
assessment activities.

7. QUALIFICATIONS OF REPORT

The activities and evaluative approaches used in this assessment are consistent with those
normally employed in soil assessment projects of this type. Our evaluation of site conditions
has been based on our understanding of the site project information and the data obtained
during our previous assessment and field activities.

SOURCE:
USGS TOPOGRAPHIC MAP
SOUTHWEST DURHAM, 1998
1 : 24,000
FIGURE 1
SITE LOCATION MAP
HENDRICK DURHAM AUTO MALL
409 SOUTH ROXBORO STREET and
464 EAST PETTIGREW STREET
DURHAM, DURHAM COUNTY,
NORTH CAROLINA
ECS PROJECT NO: 06:22255-A
Site
SOURCE:
GOOGLE EARTH
DATED 2014
SCALE AS SHOWN
FIGURE 2
SOIL AND GROUNDWATER SAMPLE
LOCATION MAP
HENDRICK DURHAM AUTO MALL
409 SOUTH ROXBORO STREET and
464 EAST PETTIGREW STREET
DURHAM, DURHAM COUNTY,
NORTH CAROLINA
ECS PROJECT NO: 06:22255-A
Oil Change
Floor Drain
AST
UST Anomaly
Service
Garage
Floor Drain
Oil Water
Separator
Drum Storage
SS-3
SS-2
SS-1/TMW-5
SS-5/TMW-1
SS-4
SS-7
SS-6
1 inch = 55 feet
LEGEND
Approximate Location of
Soil Sample
Approximate Location of Soil and
Groundwater Sample
SS-9
SS-11
SS-12
SS-8SS-10
SS-13
SS-14/TMW-4
SS-15
LEGEND
Approximate Location of
Site Boundary
Approximate Location of
Groundwater Sample
SOURCE:
GOOGLE EARTH
DATED 2012
SCALE: AS SHOWN
FIGURE 3
GROUNDWATER SAMPLE LOCATION MAP
HENDRICK DURHAM AUTO MALL
409 SOUTH ROXBORO STREET and
464 EAST PETTIGREW STREET
DURHAM, DURHAM COUNTY,
NORTH CAROLINA
ECS PROJECT NO: 06:22255-A
1 inch = 280 feet
TMW-2
TMW-3
TMW-4
TMW-1
TMW-5
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Non-Residential Vapor Intrusion Screening Levels GWSL (µg/L)
#=CL#
March 11, 2015
LIMS USE: FR - MATTHEW GILLIS
LIMS OBJECT ID: 92239514
92239514
Project:
Pace Project No.:
RE:
Matthew Gillis
ECS
9001 Glenwood Avenue
Raleigh, NC 27617
HENDRICK DURHAM AUTOMALL
Dear Matthew Gillis:
Enclosed are the analytical results for sample(s) received by the laboratory on March 03, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
Enclosures
cc:Matthew Gillis, ECS
Brian Smith, ECS Carolinas LLP
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 33
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 33
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92239514001 SS-1
Diesel Range Organics(C10-C28)46.9 mg/kg 03/05/15 14:575.9EPA 8015 Modified
Percent Moisture 14.6 %03/05/15 08:500.10ASTM D2974-87
92239514002 SS-3
Percent Moisture 10.3 %03/05/15 08:500.10ASTM D2974-87
92239514003 SS-5
Diesel Range Organics(C10-C28)9.7 mg/kg 03/05/15 15:206.9EPA 8015 Modified
Percent Moisture 27.1 %03/05/15 08:500.10ASTM D2974-87
92239514004 SS-2
Barium 302 mg/kg 03/06/15 21:47 M1,R10.43EPA 6010
Cadmium 0.13 mg/kg 03/06/15 21:470.085EPA 6010
Chromium 78.2 mg/kg 03/06/15 21:47 M10.43EPA 6010
Lead 5.1 mg/kg 03/06/15 21:470.43EPA 6010
Selenium 1.6 mg/kg 03/06/15 21:47 M10.85EPA 6010
Mercury 0.024 mg/kg 03/06/15 15:05 M10.0036EPA 7471
Percent Moisture 15.1 %03/05/15 08:500.10ASTM D2974-87
92239514005 SS-4
Arsenic 2.0 mg/kg 03/06/15 21:560.89EPA 6010
Barium 78.2 mg/kg 03/06/15 21:560.45EPA 6010
Cadmium 0.097 mg/kg 03/06/15 21:560.089EPA 6010
Chromium 16.9 mg/kg 03/06/15 21:560.45EPA 6010
Lead 8.9 mg/kg 03/06/15 21:560.45EPA 6010
Silver 0.57 mg/kg 03/06/15 21:560.45EPA 6010
Mercury 0.0064 mg/kg 03/06/15 15:130.0041EPA 7471
Percent Moisture 11.3 %03/05/15 08:500.10ASTM D2974-87
92239514006 TMW-1
Acetone 40.9 ug/L 03/07/15 06:2025.0EPA 8260
Naphthalene 1.8 ug/L 03/07/15 06:201.0EPA 8260
Toluene 8.1 ug/L 03/07/15 06:201.0EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Sample:SS-1 Lab ID:92239514001 Collected:02/28/15 09:15 Received:03/03/15 16:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)46.9 mg/kg 03/05/15 14:5703/04/15 14:305.9 1
Surrogates
n-Pentacosane (S)81 %03/05/15 14:57 629-99-203/04/15 14:3041-119 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/04/15 17:07 67-64-174.0 1
Benzene ND ug/kg 03/04/15 17:07 71-43-23.7 1
Bromobenzene ND ug/kg 03/04/15 17:07 108-86-13.7 1
Bromochloromethane ND ug/kg 03/04/15 17:07 74-97-53.7 1
Bromodichloromethane ND ug/kg 03/04/15 17:07 75-27-43.7 1
Bromoform ND ug/kg 03/04/15 17:07 75-25-23.7 1
Bromomethane ND ug/kg 03/04/15 17:07 74-83-97.4 1
2-Butanone (MEK)ND ug/kg 03/04/15 17:07 78-93-374.0 1
n-Butylbenzene ND ug/kg 03/04/15 17:07 104-51-83.7 1
sec-Butylbenzene ND ug/kg 03/04/15 17:07 135-98-83.7 1
tert-Butylbenzene ND ug/kg 03/04/15 17:07 98-06-63.7 1
Carbon tetrachloride ND ug/kg 03/04/15 17:07 56-23-53.7 1
Chlorobenzene ND ug/kg 03/04/15 17:07 108-90-73.7 1
Chloroethane ND ug/kg 03/04/15 17:07 75-00-37.4 1
Chloroform ND ug/kg 03/04/15 17:07 67-66-33.7 1
Chloromethane ND ug/kg 03/04/15 17:07 74-87-37.4 1
2-Chlorotoluene ND ug/kg 03/04/15 17:07 95-49-83.7 1
4-Chlorotoluene ND ug/kg 03/04/15 17:07 106-43-43.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/04/15 17:07 96-12-83.7 1
Dibromochloromethane ND ug/kg 03/04/15 17:07 124-48-13.7 1
1,2-Dibromoethane (EDB)ND ug/kg 03/04/15 17:07 106-93-43.7 1
Dibromomethane ND ug/kg 03/04/15 17:07 74-95-33.7 1
1,2-Dichlorobenzene ND ug/kg 03/04/15 17:07 95-50-13.7 1
1,3-Dichlorobenzene ND ug/kg 03/04/15 17:07 541-73-13.7 1
1,4-Dichlorobenzene ND ug/kg 03/04/15 17:07 106-46-73.7 1
Dichlorodifluoromethane ND ug/kg 03/04/15 17:07 75-71-87.4 1
1,1-Dichloroethane ND ug/kg 03/04/15 17:07 75-34-33.7 1
1,2-Dichloroethane ND ug/kg 03/04/15 17:07 107-06-23.7 1
1,1-Dichloroethene ND ug/kg 03/04/15 17:07 75-35-43.7 1
cis-1,2-Dichloroethene ND ug/kg 03/04/15 17:07 156-59-23.7 1
trans-1,2-Dichloroethene ND ug/kg 03/04/15 17:07 156-60-53.7 1
1,2-Dichloropropane ND ug/kg 03/04/15 17:07 78-87-53.7 1
1,3-Dichloropropane ND ug/kg 03/04/15 17:07 142-28-93.7 1
2,2-Dichloropropane ND ug/kg 03/04/15 17:07 594-20-73.7 1
1,1-Dichloropropene ND ug/kg 03/04/15 17:07 563-58-63.7 1
cis-1,3-Dichloropropene ND ug/kg 03/04/15 17:07 10061-01-53.7 1
trans-1,3-Dichloropropene ND ug/kg 03/04/15 17:07 10061-02-63.7 1
Diisopropyl ether ND ug/kg 03/04/15 17:07 108-20-33.7 1
Ethylbenzene ND ug/kg 03/04/15 17:07 100-41-43.7 1
Hexachloro-1,3-butadiene ND ug/kg 03/04/15 17:07 87-68-33.7 1
2-Hexanone ND ug/kg 03/04/15 17:07 591-78-637.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Sample:SS-1 Lab ID:92239514001 Collected:02/28/15 09:15 Received:03/03/15 16:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Isopropylbenzene (Cumene)ND ug/kg 03/04/15 17:07 98-82-83.7 1
p-Isopropyltoluene ND ug/kg 03/04/15 17:07 99-87-63.7 1
Methylene Chloride ND ug/kg 03/04/15 17:07 75-09-214.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/04/15 17:07 108-10-137.0 1
Methyl-tert-butyl ether ND ug/kg 03/04/15 17:07 1634-04-43.7 1
Naphthalene ND ug/kg 03/04/15 17:07 91-20-33.7 1
n-Propylbenzene ND ug/kg 03/04/15 17:07 103-65-13.7 1
Styrene ND ug/kg 03/04/15 17:07 100-42-53.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/04/15 17:07 630-20-63.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/04/15 17:07 79-34-53.7 1
Tetrachloroethene ND ug/kg 03/04/15 17:07 127-18-43.7 1
Toluene ND ug/kg 03/04/15 17:07 108-88-33.7 1
1,2,3-Trichlorobenzene ND ug/kg 03/04/15 17:07 87-61-63.7 1
1,2,4-Trichlorobenzene ND ug/kg 03/04/15 17:07 120-82-13.7 1
1,1,1-Trichloroethane ND ug/kg 03/04/15 17:07 71-55-63.7 1
1,1,2-Trichloroethane ND ug/kg 03/04/15 17:07 79-00-53.7 1
Trichloroethene ND ug/kg 03/04/15 17:07 79-01-63.7 1
Trichlorofluoromethane ND ug/kg 03/04/15 17:07 75-69-43.7 1
1,2,3-Trichloropropane ND ug/kg 03/04/15 17:07 96-18-43.7 1
1,2,4-Trimethylbenzene ND ug/kg 03/04/15 17:07 95-63-63.7 1
1,3,5-Trimethylbenzene ND ug/kg 03/04/15 17:07 108-67-83.7 1
Vinyl acetate ND ug/kg 03/04/15 17:07 108-05-437.0 1
Vinyl chloride ND ug/kg 03/04/15 17:07 75-01-47.4 1
Xylene (Total)ND ug/kg 03/04/15 17:07 1330-20-77.4 1
m&p-Xylene ND ug/kg 03/04/15 17:07 179601-23-17.4 1
o-Xylene ND ug/kg 03/04/15 17:07 95-47-63.7 1
Surrogates
Toluene-d8 (S)105 %03/04/15 17:07 2037-26-570-130 1
4-Bromofluorobenzene (S)95 %03/04/15 17:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %03/04/15 17:07 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.6 %03/05/15 08:500.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Sample:SS-3 Lab ID:92239514002 Collected:02/28/15 11:15 Received:03/03/15 16:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 03/05/15 15:2003/04/15 14:305.6 1
Surrogates
n-Pentacosane (S)73 %03/05/15 15:20 629-99-203/04/15 14:3041-119 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/04/15 17:27 67-64-184.5 1
Benzene ND ug/kg 03/04/15 17:27 71-43-24.2 1
Bromobenzene ND ug/kg 03/04/15 17:27 108-86-14.2 1
Bromochloromethane ND ug/kg 03/04/15 17:27 74-97-54.2 1
Bromodichloromethane ND ug/kg 03/04/15 17:27 75-27-44.2 1
Bromoform ND ug/kg 03/04/15 17:27 75-25-24.2 1
Bromomethane ND ug/kg 03/04/15 17:27 74-83-98.4 1
2-Butanone (MEK)ND ug/kg 03/04/15 17:27 78-93-384.5 1
n-Butylbenzene ND ug/kg 03/04/15 17:27 104-51-84.2 1
sec-Butylbenzene ND ug/kg 03/04/15 17:27 135-98-84.2 1
tert-Butylbenzene ND ug/kg 03/04/15 17:27 98-06-64.2 1
Carbon tetrachloride ND ug/kg 03/04/15 17:27 56-23-54.2 1
Chlorobenzene ND ug/kg 03/04/15 17:27 108-90-74.2 1
Chloroethane ND ug/kg 03/04/15 17:27 75-00-38.4 1
Chloroform ND ug/kg 03/04/15 17:27 67-66-34.2 1
Chloromethane ND ug/kg 03/04/15 17:27 74-87-38.4 1
2-Chlorotoluene ND ug/kg 03/04/15 17:27 95-49-84.2 1
4-Chlorotoluene ND ug/kg 03/04/15 17:27 106-43-44.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/04/15 17:27 96-12-84.2 1
Dibromochloromethane ND ug/kg 03/04/15 17:27 124-48-14.2 1
1,2-Dibromoethane (EDB)ND ug/kg 03/04/15 17:27 106-93-44.2 1
Dibromomethane ND ug/kg 03/04/15 17:27 74-95-34.2 1
1,2-Dichlorobenzene ND ug/kg 03/04/15 17:27 95-50-14.2 1
1,3-Dichlorobenzene ND ug/kg 03/04/15 17:27 541-73-14.2 1
1,4-Dichlorobenzene ND ug/kg 03/04/15 17:27 106-46-74.2 1
Dichlorodifluoromethane ND ug/kg 03/04/15 17:27 75-71-88.4 1
1,1-Dichloroethane ND ug/kg 03/04/15 17:27 75-34-34.2 1
1,2-Dichloroethane ND ug/kg 03/04/15 17:27 107-06-24.2 1
1,1-Dichloroethene ND ug/kg 03/04/15 17:27 75-35-44.2 1
cis-1,2-Dichloroethene ND ug/kg 03/04/15 17:27 156-59-24.2 1
trans-1,2-Dichloroethene ND ug/kg 03/04/15 17:27 156-60-54.2 1
1,2-Dichloropropane ND ug/kg 03/04/15 17:27 78-87-54.2 1
1,3-Dichloropropane ND ug/kg 03/04/15 17:27 142-28-94.2 1
2,2-Dichloropropane ND ug/kg 03/04/15 17:27 594-20-74.2 1
1,1-Dichloropropene ND ug/kg 03/04/15 17:27 563-58-64.2 1
cis-1,3-Dichloropropene ND ug/kg 03/04/15 17:27 10061-01-54.2 1
trans-1,3-Dichloropropene ND ug/kg 03/04/15 17:27 10061-02-64.2 1
Diisopropyl ether ND ug/kg 03/04/15 17:27 108-20-34.2 1
Ethylbenzene ND ug/kg 03/04/15 17:27 100-41-44.2 1
Hexachloro-1,3-butadiene ND ug/kg 03/04/15 17:27 87-68-34.2 1
2-Hexanone ND ug/kg 03/04/15 17:27 591-78-642.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Sample:SS-3 Lab ID:92239514002 Collected:02/28/15 11:15 Received:03/03/15 16:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Isopropylbenzene (Cumene)ND ug/kg 03/04/15 17:27 98-82-84.2 1
p-Isopropyltoluene ND ug/kg 03/04/15 17:27 99-87-64.2 1
Methylene Chloride ND ug/kg 03/04/15 17:27 75-09-216.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/04/15 17:27 108-10-142.2 1
Methyl-tert-butyl ether ND ug/kg 03/04/15 17:27 1634-04-44.2 1
Naphthalene ND ug/kg 03/04/15 17:27 91-20-34.2 1
n-Propylbenzene ND ug/kg 03/04/15 17:27 103-65-14.2 1
Styrene ND ug/kg 03/04/15 17:27 100-42-54.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/04/15 17:27 630-20-64.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/04/15 17:27 79-34-54.2 1
Tetrachloroethene ND ug/kg 03/04/15 17:27 127-18-44.2 1
Toluene ND ug/kg 03/04/15 17:27 108-88-34.2 1
1,2,3-Trichlorobenzene ND ug/kg 03/04/15 17:27 87-61-64.2 1
1,2,4-Trichlorobenzene ND ug/kg 03/04/15 17:27 120-82-14.2 1
1,1,1-Trichloroethane ND ug/kg 03/04/15 17:27 71-55-64.2 1
1,1,2-Trichloroethane ND ug/kg 03/04/15 17:27 79-00-54.2 1
Trichloroethene ND ug/kg 03/04/15 17:27 79-01-64.2 1
Trichlorofluoromethane ND ug/kg 03/04/15 17:27 75-69-44.2 1
1,2,3-Trichloropropane ND ug/kg 03/04/15 17:27 96-18-44.2 1
1,2,4-Trimethylbenzene ND ug/kg 03/04/15 17:27 95-63-64.2 1
1,3,5-Trimethylbenzene ND ug/kg 03/04/15 17:27 108-67-84.2 1
Vinyl acetate ND ug/kg 03/04/15 17:27 108-05-442.2 1
Vinyl chloride ND ug/kg 03/04/15 17:27 75-01-48.4 1
Xylene (Total)ND ug/kg 03/04/15 17:27 1330-20-78.4 1
m&p-Xylene ND ug/kg 03/04/15 17:27 179601-23-18.4 1
o-Xylene ND ug/kg 03/04/15 17:27 95-47-64.2 1
Surrogates
Toluene-d8 (S)104 %03/04/15 17:27 2037-26-570-130 1
4-Bromofluorobenzene (S)97 %03/04/15 17:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %03/04/15 17:27 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 10.3 %03/05/15 08:500.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Sample:SS-5 Lab ID:92239514003 Collected:02/28/15 12:30 Received:03/03/15 16:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)9.7 mg/kg 03/05/15 15:2003/04/15 14:306.9 1
Surrogates
n-Pentacosane (S)73 %03/05/15 15:20 629-99-203/04/15 14:3041-119 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/04/15 17:47 67-64-11071
Benzene ND ug/kg 03/04/15 17:47 71-43-25.4 1
Bromobenzene ND ug/kg 03/04/15 17:47 108-86-15.4 1
Bromochloromethane ND ug/kg 03/04/15 17:47 74-97-55.4 1
Bromodichloromethane ND ug/kg 03/04/15 17:47 75-27-45.4 1
Bromoform ND ug/kg 03/04/15 17:47 75-25-25.4 1
Bromomethane ND ug/kg 03/04/15 17:47 74-83-910.7 1
2-Butanone (MEK)ND ug/kg 03/04/15 17:47 78-93-31071
n-Butylbenzene ND ug/kg 03/04/15 17:47 104-51-85.4 1
sec-Butylbenzene ND ug/kg 03/04/15 17:47 135-98-85.4 1
tert-Butylbenzene ND ug/kg 03/04/15 17:47 98-06-65.4 1
Carbon tetrachloride ND ug/kg 03/04/15 17:47 56-23-55.4 1
Chlorobenzene ND ug/kg 03/04/15 17:47 108-90-75.4 1
Chloroethane ND ug/kg 03/04/15 17:47 75-00-310.7 1
Chloroform ND ug/kg 03/04/15 17:47 67-66-35.4 1
Chloromethane ND ug/kg 03/04/15 17:47 74-87-310.7 1
2-Chlorotoluene ND ug/kg 03/04/15 17:47 95-49-85.4 1
4-Chlorotoluene ND ug/kg 03/04/15 17:47 106-43-45.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/04/15 17:47 96-12-85.4 1
Dibromochloromethane ND ug/kg 03/04/15 17:47 124-48-15.4 1
1,2-Dibromoethane (EDB)ND ug/kg 03/04/15 17:47 106-93-45.4 1
Dibromomethane ND ug/kg 03/04/15 17:47 74-95-35.4 1
1,2-Dichlorobenzene ND ug/kg 03/04/15 17:47 95-50-15.4 1
1,3-Dichlorobenzene ND ug/kg 03/04/15 17:47 541-73-15.4 1
1,4-Dichlorobenzene ND ug/kg 03/04/15 17:47 106-46-75.4 1
Dichlorodifluoromethane ND ug/kg 03/04/15 17:47 75-71-810.7 1
1,1-Dichloroethane ND ug/kg 03/04/15 17:47 75-34-35.4 1
1,2-Dichloroethane ND ug/kg 03/04/15 17:47 107-06-25.4 1
1,1-Dichloroethene ND ug/kg 03/04/15 17:47 75-35-45.4 1
cis-1,2-Dichloroethene ND ug/kg 03/04/15 17:47 156-59-25.4 1
trans-1,2-Dichloroethene ND ug/kg 03/04/15 17:47 156-60-55.4 1
1,2-Dichloropropane ND ug/kg 03/04/15 17:47 78-87-55.4 1
1,3-Dichloropropane ND ug/kg 03/04/15 17:47 142-28-95.4 1
2,2-Dichloropropane ND ug/kg 03/04/15 17:47 594-20-75.4 1
1,1-Dichloropropene ND ug/kg 03/04/15 17:47 563-58-65.4 1
cis-1,3-Dichloropropene ND ug/kg 03/04/15 17:47 10061-01-55.4 1
trans-1,3-Dichloropropene ND ug/kg 03/04/15 17:47 10061-02-65.4 1
Diisopropyl ether ND ug/kg 03/04/15 17:47 108-20-35.4 1
Ethylbenzene ND ug/kg 03/04/15 17:47 100-41-45.4 1
Hexachloro-1,3-butadiene ND ug/kg 03/04/15 17:47 87-68-35.4 1
2-Hexanone ND ug/kg 03/04/15 17:47 591-78-653.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Sample:SS-5 Lab ID:92239514003 Collected:02/28/15 12:30 Received:03/03/15 16:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Isopropylbenzene (Cumene)ND ug/kg 03/04/15 17:47 98-82-85.4 1
p-Isopropyltoluene ND ug/kg 03/04/15 17:47 99-87-65.4 1
Methylene Chloride ND ug/kg 03/04/15 17:47 75-09-221.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/04/15 17:47 108-10-153.6 1
Methyl-tert-butyl ether ND ug/kg 03/04/15 17:47 1634-04-45.4 1
Naphthalene ND ug/kg 03/04/15 17:47 91-20-35.4 1
n-Propylbenzene ND ug/kg 03/04/15 17:47 103-65-15.4 1
Styrene ND ug/kg 03/04/15 17:47 100-42-55.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/04/15 17:47 630-20-65.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/04/15 17:47 79-34-55.4 1
Tetrachloroethene ND ug/kg 03/04/15 17:47 127-18-45.4 1
Toluene ND ug/kg 03/04/15 17:47 108-88-35.4 1
1,2,3-Trichlorobenzene ND ug/kg 03/04/15 17:47 87-61-65.4 1
1,2,4-Trichlorobenzene ND ug/kg 03/04/15 17:47 120-82-15.4 1
1,1,1-Trichloroethane ND ug/kg 03/04/15 17:47 71-55-65.4 1
1,1,2-Trichloroethane ND ug/kg 03/04/15 17:47 79-00-55.4 1
Trichloroethene ND ug/kg 03/04/15 17:47 79-01-65.4 1
Trichlorofluoromethane ND ug/kg 03/04/15 17:47 75-69-45.4 1
1,2,3-Trichloropropane ND ug/kg 03/04/15 17:47 96-18-45.4 1
1,2,4-Trimethylbenzene ND ug/kg 03/04/15 17:47 95-63-65.4 1
1,3,5-Trimethylbenzene ND ug/kg 03/04/15 17:47 108-67-85.4 1
Vinyl acetate ND ug/kg 03/04/15 17:47 108-05-453.6 1
Vinyl chloride ND ug/kg 03/04/15 17:47 75-01-410.7 1
Xylene (Total)ND ug/kg 03/04/15 17:47 1330-20-710.7 1
m&p-Xylene ND ug/kg 03/04/15 17:47 179601-23-110.7 1
o-Xylene ND ug/kg 03/04/15 17:47 95-47-65.4 1
Surrogates
Toluene-d8 (S)102 %03/04/15 17:47 2037-26-570-130 1
4-Bromofluorobenzene (S)98 %03/04/15 17:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %03/04/15 17:47 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 27.1 %03/05/15 08:500.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Sample:SS-2 Lab ID:92239514004 Collected:02/28/15 10:15 Received:03/03/15 16:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 03/05/15 16:0803/04/15 14:305.9 1
Surrogates
n-Pentacosane (S)65 %03/05/15 16:08 629-99-203/04/15 14:3041-119 1
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Arsenic ND mg/kg 03/06/15 21:47 7440-38-2 M103/06/15 16:200.85 1
Barium 302 mg/kg 03/06/15 21:47 7440-39-3 M1,R103/06/15 16:200.43 1
Cadmium 0.13 mg/kg 03/06/15 21:47 7440-43-903/06/15 16:200.085 1
Chromium 78.2 mg/kg 03/06/15 21:47 7440-47-3 M103/06/15 16:200.43 1
Lead 5.1 mg/kg 03/06/15 21:47 7439-92-103/06/15 16:200.43 1
Selenium 1.6 mg/kg 03/06/15 21:47 7782-49-2 M103/06/15 16:200.85 1
Silver ND mg/kg 03/06/15 21:47 7440-22-403/06/15 16:200.43 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.024 mg/kg 03/06/15 15:05 7439-97-6 M103/05/15 16:450.0036 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/04/15 18:07 67-64-188.4 1
Benzene ND ug/kg 03/04/15 18:07 71-43-24.4 1
Bromobenzene ND ug/kg 03/04/15 18:07 108-86-14.4 1
Bromochloromethane ND ug/kg 03/04/15 18:07 74-97-54.4 1
Bromodichloromethane ND ug/kg 03/04/15 18:07 75-27-44.4 1
Bromoform ND ug/kg 03/04/15 18:07 75-25-24.4 1
Bromomethane ND ug/kg 03/04/15 18:07 74-83-98.8 1
2-Butanone (MEK)ND ug/kg 03/04/15 18:07 78-93-388.4 1
n-Butylbenzene ND ug/kg 03/04/15 18:07 104-51-84.4 1
sec-Butylbenzene ND ug/kg 03/04/15 18:07 135-98-84.4 1
tert-Butylbenzene ND ug/kg 03/04/15 18:07 98-06-64.4 1
Carbon tetrachloride ND ug/kg 03/04/15 18:07 56-23-54.4 1
Chlorobenzene ND ug/kg 03/04/15 18:07 108-90-74.4 1
Chloroethane ND ug/kg 03/04/15 18:07 75-00-38.8 1
Chloroform ND ug/kg 03/04/15 18:07 67-66-34.4 1
Chloromethane ND ug/kg 03/04/15 18:07 74-87-38.8 1
2-Chlorotoluene ND ug/kg 03/04/15 18:07 95-49-84.4 1
4-Chlorotoluene ND ug/kg 03/04/15 18:07 106-43-44.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/04/15 18:07 96-12-84.4 1
Dibromochloromethane ND ug/kg 03/04/15 18:07 124-48-14.4 1
1,2-Dibromoethane (EDB)ND ug/kg 03/04/15 18:07 106-93-44.4 1
Dibromomethane ND ug/kg 03/04/15 18:07 74-95-34.4 1
1,2-Dichlorobenzene ND ug/kg 03/04/15 18:07 95-50-14.4 1
1,3-Dichlorobenzene ND ug/kg 03/04/15 18:07 541-73-14.4 1
1,4-Dichlorobenzene ND ug/kg 03/04/15 18:07 106-46-74.4 1
Dichlorodifluoromethane ND ug/kg 03/04/15 18:07 75-71-88.8 1
1,1-Dichloroethane ND ug/kg 03/04/15 18:07 75-34-34.4 1
1,2-Dichloroethane ND ug/kg 03/04/15 18:07 107-06-24.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Sample:SS-2 Lab ID:92239514004 Collected:02/28/15 10:15 Received:03/03/15 16:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
1,1-Dichloroethene ND ug/kg 03/04/15 18:07 75-35-44.4 1
cis-1,2-Dichloroethene ND ug/kg 03/04/15 18:07 156-59-24.4 1
trans-1,2-Dichloroethene ND ug/kg 03/04/15 18:07 156-60-54.4 1
1,2-Dichloropropane ND ug/kg 03/04/15 18:07 78-87-54.4 1
1,3-Dichloropropane ND ug/kg 03/04/15 18:07 142-28-94.4 1
2,2-Dichloropropane ND ug/kg 03/04/15 18:07 594-20-74.4 1
1,1-Dichloropropene ND ug/kg 03/04/15 18:07 563-58-64.4 1
cis-1,3-Dichloropropene ND ug/kg 03/04/15 18:07 10061-01-54.4 1
trans-1,3-Dichloropropene ND ug/kg 03/04/15 18:07 10061-02-64.4 1
Diisopropyl ether ND ug/kg 03/04/15 18:07 108-20-34.4 1
Ethylbenzene ND ug/kg 03/04/15 18:07 100-41-44.4 1
Hexachloro-1,3-butadiene ND ug/kg 03/04/15 18:07 87-68-34.4 1
2-Hexanone ND ug/kg 03/04/15 18:07 591-78-644.2 1
Isopropylbenzene (Cumene)ND ug/kg 03/04/15 18:07 98-82-84.4 1
p-Isopropyltoluene ND ug/kg 03/04/15 18:07 99-87-64.4 1
Methylene Chloride ND ug/kg 03/04/15 18:07 75-09-217.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/04/15 18:07 108-10-144.2 1
Methyl-tert-butyl ether ND ug/kg 03/04/15 18:07 1634-04-44.4 1
Naphthalene ND ug/kg 03/04/15 18:07 91-20-34.4 1
n-Propylbenzene ND ug/kg 03/04/15 18:07 103-65-14.4 1
Styrene ND ug/kg 03/04/15 18:07 100-42-54.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/04/15 18:07 630-20-64.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/04/15 18:07 79-34-54.4 1
Tetrachloroethene ND ug/kg 03/04/15 18:07 127-18-44.4 1
Toluene ND ug/kg 03/04/15 18:07 108-88-34.4 1
1,2,3-Trichlorobenzene ND ug/kg 03/04/15 18:07 87-61-64.4 1
1,2,4-Trichlorobenzene ND ug/kg 03/04/15 18:07 120-82-14.4 1
1,1,1-Trichloroethane ND ug/kg 03/04/15 18:07 71-55-64.4 1
1,1,2-Trichloroethane ND ug/kg 03/04/15 18:07 79-00-54.4 1
Trichloroethene ND ug/kg 03/04/15 18:07 79-01-64.4 1
Trichlorofluoromethane ND ug/kg 03/04/15 18:07 75-69-44.4 1
1,2,3-Trichloropropane ND ug/kg 03/04/15 18:07 96-18-44.4 1
1,2,4-Trimethylbenzene ND ug/kg 03/04/15 18:07 95-63-64.4 1
1,3,5-Trimethylbenzene ND ug/kg 03/04/15 18:07 108-67-84.4 1
Vinyl acetate ND ug/kg 03/04/15 18:07 108-05-444.2 1
Vinyl chloride ND ug/kg 03/04/15 18:07 75-01-48.8 1
Xylene (Total)ND ug/kg 03/04/15 18:07 1330-20-78.8 1
m&p-Xylene ND ug/kg 03/04/15 18:07 179601-23-18.8 1
o-Xylene ND ug/kg 03/04/15 18:07 95-47-64.4 1
Surrogates
Toluene-d8 (S)102 %03/04/15 18:07 2037-26-570-130 1
4-Bromofluorobenzene (S)99 %03/04/15 18:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %03/04/15 18:07 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.1 %03/05/15 08:500.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Sample:SS-4 Lab ID:92239514005 Collected:02/28/15 11:50 Received:03/03/15 16:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 03/05/15 16:0803/04/15 14:305.6 1
Surrogates
n-Pentacosane (S)65 %03/05/15 16:08 629-99-203/04/15 14:3041-119 1
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Arsenic 2.0 mg/kg 03/06/15 21:56 7440-38-203/06/15 16:200.89 1
Barium 78.2 mg/kg 03/06/15 21:56 7440-39-303/06/15 16:200.45 1
Cadmium 0.097 mg/kg 03/06/15 21:56 7440-43-903/06/15 16:200.089 1
Chromium 16.9 mg/kg 03/06/15 21:56 7440-47-303/06/15 16:200.45 1
Lead 8.9 mg/kg 03/06/15 21:56 7439-92-103/06/15 16:200.45 1
Selenium ND mg/kg 03/06/15 21:56 7782-49-203/06/15 16:200.89 1
Silver 0.57 mg/kg 03/06/15 21:56 7440-22-403/06/15 16:200.45 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.0064 mg/kg 03/06/15 15:13 7439-97-603/05/15 16:450.0041 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/04/15 18:26 67-64-194.6 1
Benzene ND ug/kg 03/04/15 18:26 71-43-24.7 1
Bromobenzene ND ug/kg 03/04/15 18:26 108-86-14.7 1
Bromochloromethane ND ug/kg 03/04/15 18:26 74-97-54.7 1
Bromodichloromethane ND ug/kg 03/04/15 18:26 75-27-44.7 1
Bromoform ND ug/kg 03/04/15 18:26 75-25-24.7 1
Bromomethane ND ug/kg 03/04/15 18:26 74-83-99.5 1
2-Butanone (MEK)ND ug/kg 03/04/15 18:26 78-93-394.6 1
n-Butylbenzene ND ug/kg 03/04/15 18:26 104-51-84.7 1
sec-Butylbenzene ND ug/kg 03/04/15 18:26 135-98-84.7 1
tert-Butylbenzene ND ug/kg 03/04/15 18:26 98-06-64.7 1
Carbon tetrachloride ND ug/kg 03/04/15 18:26 56-23-54.7 1
Chlorobenzene ND ug/kg 03/04/15 18:26 108-90-74.7 1
Chloroethane ND ug/kg 03/04/15 18:26 75-00-39.5 1
Chloroform ND ug/kg 03/04/15 18:26 67-66-34.7 1
Chloromethane ND ug/kg 03/04/15 18:26 74-87-39.5 1
2-Chlorotoluene ND ug/kg 03/04/15 18:26 95-49-84.7 1
4-Chlorotoluene ND ug/kg 03/04/15 18:26 106-43-44.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/04/15 18:26 96-12-84.7 1
Dibromochloromethane ND ug/kg 03/04/15 18:26 124-48-14.7 1
1,2-Dibromoethane (EDB)ND ug/kg 03/04/15 18:26 106-93-44.7 1
Dibromomethane ND ug/kg 03/04/15 18:26 74-95-34.7 1
1,2-Dichlorobenzene ND ug/kg 03/04/15 18:26 95-50-14.7 1
1,3-Dichlorobenzene ND ug/kg 03/04/15 18:26 541-73-14.7 1
1,4-Dichlorobenzene ND ug/kg 03/04/15 18:26 106-46-74.7 1
Dichlorodifluoromethane ND ug/kg 03/04/15 18:26 75-71-89.5 1
1,1-Dichloroethane ND ug/kg 03/04/15 18:26 75-34-34.7 1
1,2-Dichloroethane ND ug/kg 03/04/15 18:26 107-06-24.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Sample:SS-4 Lab ID:92239514005 Collected:02/28/15 11:50 Received:03/03/15 16:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
1,1-Dichloroethene ND ug/kg 03/04/15 18:26 75-35-44.7 1
cis-1,2-Dichloroethene ND ug/kg 03/04/15 18:26 156-59-24.7 1
trans-1,2-Dichloroethene ND ug/kg 03/04/15 18:26 156-60-54.7 1
1,2-Dichloropropane ND ug/kg 03/04/15 18:26 78-87-54.7 1
1,3-Dichloropropane ND ug/kg 03/04/15 18:26 142-28-94.7 1
2,2-Dichloropropane ND ug/kg 03/04/15 18:26 594-20-74.7 1
1,1-Dichloropropene ND ug/kg 03/04/15 18:26 563-58-64.7 1
cis-1,3-Dichloropropene ND ug/kg 03/04/15 18:26 10061-01-54.7 1
trans-1,3-Dichloropropene ND ug/kg 03/04/15 18:26 10061-02-64.7 1
Diisopropyl ether ND ug/kg 03/04/15 18:26 108-20-34.7 1
Ethylbenzene ND ug/kg 03/04/15 18:26 100-41-44.7 1
Hexachloro-1,3-butadiene ND ug/kg 03/04/15 18:26 87-68-34.7 1
2-Hexanone ND ug/kg 03/04/15 18:26 591-78-647.3 1
Isopropylbenzene (Cumene)ND ug/kg 03/04/15 18:26 98-82-84.7 1
p-Isopropyltoluene ND ug/kg 03/04/15 18:26 99-87-64.7 1
Methylene Chloride ND ug/kg 03/04/15 18:26 75-09-218.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/04/15 18:26 108-10-147.3 1
Methyl-tert-butyl ether ND ug/kg 03/04/15 18:26 1634-04-44.7 1
Naphthalene ND ug/kg 03/04/15 18:26 91-20-34.7 1
n-Propylbenzene ND ug/kg 03/04/15 18:26 103-65-14.7 1
Styrene ND ug/kg 03/04/15 18:26 100-42-54.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/04/15 18:26 630-20-64.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/04/15 18:26 79-34-54.7 1
Tetrachloroethene ND ug/kg 03/04/15 18:26 127-18-44.7 1
Toluene ND ug/kg 03/04/15 18:26 108-88-34.7 1
1,2,3-Trichlorobenzene ND ug/kg 03/04/15 18:26 87-61-64.7 1
1,2,4-Trichlorobenzene ND ug/kg 03/04/15 18:26 120-82-14.7 1
1,1,1-Trichloroethane ND ug/kg 03/04/15 18:26 71-55-64.7 1
1,1,2-Trichloroethane ND ug/kg 03/04/15 18:26 79-00-54.7 1
Trichloroethene ND ug/kg 03/04/15 18:26 79-01-64.7 1
Trichlorofluoromethane ND ug/kg 03/04/15 18:26 75-69-44.7 1
1,2,3-Trichloropropane ND ug/kg 03/04/15 18:26 96-18-44.7 1
1,2,4-Trimethylbenzene ND ug/kg 03/04/15 18:26 95-63-64.7 1
1,3,5-Trimethylbenzene ND ug/kg 03/04/15 18:26 108-67-84.7 1
Vinyl acetate ND ug/kg 03/04/15 18:26 108-05-447.3 1
Vinyl chloride ND ug/kg 03/04/15 18:26 75-01-49.5 1
Xylene (Total)ND ug/kg 03/04/15 18:26 1330-20-79.5 1
m&p-Xylene ND ug/kg 03/04/15 18:26 179601-23-19.5 1
o-Xylene ND ug/kg 03/04/15 18:26 95-47-64.7 1
Surrogates
Toluene-d8 (S)104 %03/04/15 18:26 2037-26-570-130 1
4-Bromofluorobenzene (S)97 %03/04/15 18:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)115 %03/04/15 18:26 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 11.3 %03/05/15 08:500.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Sample:TMW-1 Lab ID:92239514006 Collected:02/28/15 14:30 Received:03/03/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Acetone 40.9 ug/L 03/07/15 06:20 67-64-125.0 1
Benzene ND ug/L 03/07/15 06:20 71-43-21.0 1
Bromobenzene ND ug/L 03/07/15 06:20 108-86-11.0 1
Bromochloromethane ND ug/L 03/07/15 06:20 74-97-51.0 1
Bromodichloromethane ND ug/L 03/07/15 06:20 75-27-41.0 1
Bromoform ND ug/L 03/07/15 06:20 75-25-21.0 1
Bromomethane ND ug/L 03/07/15 06:20 74-83-92.0 1
2-Butanone (MEK)ND ug/L 03/07/15 06:20 78-93-35.0 1
Carbon tetrachloride ND ug/L 03/07/15 06:20 56-23-51.0 1
Chlorobenzene ND ug/L 03/07/15 06:20 108-90-71.0 1
Chloroethane ND ug/L 03/07/15 06:20 75-00-31.0 1
Chloroform ND ug/L 03/07/15 06:20 67-66-31.0 1
Chloromethane ND ug/L 03/07/15 06:20 74-87-31.0 1
2-Chlorotoluene ND ug/L 03/07/15 06:20 95-49-81.0 1
4-Chlorotoluene ND ug/L 03/07/15 06:20 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 03/07/15 06:20 96-12-82.0 1
Dibromochloromethane ND ug/L 03/07/15 06:20 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 03/07/15 06:20 106-93-41.0 1
Dibromomethane ND ug/L 03/07/15 06:20 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 03/07/15 06:20 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 03/07/15 06:20 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 03/07/15 06:20 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 03/07/15 06:20 75-71-81.0 1
1,1-Dichloroethane ND ug/L 03/07/15 06:20 75-34-31.0 1
1,2-Dichloroethane ND ug/L 03/07/15 06:20 107-06-21.0 1
1,1-Dichloroethene ND ug/L 03/07/15 06:20 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 03/07/15 06:20 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 03/07/15 06:20 156-60-51.0 1
1,2-Dichloropropane ND ug/L 03/07/15 06:20 78-87-51.0 1
1,3-Dichloropropane ND ug/L 03/07/15 06:20 142-28-91.0 1
2,2-Dichloropropane ND ug/L 03/07/15 06:20 594-20-71.0 1
1,1-Dichloropropene ND ug/L 03/07/15 06:20 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 03/07/15 06:20 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 03/07/15 06:20 10061-02-61.0 1
Diisopropyl ether ND ug/L 03/07/15 06:20 108-20-31.0 1
Ethylbenzene ND ug/L 03/07/15 06:20 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 03/07/15 06:20 87-68-31.0 1
2-Hexanone ND ug/L 03/07/15 06:20 591-78-65.0 1
p-Isopropyltoluene ND ug/L 03/07/15 06:20 99-87-61.0 1
Methylene Chloride ND ug/L 03/07/15 06:20 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/07/15 06:20 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 03/07/15 06:20 1634-04-41.0 1
Naphthalene 1.8 ug/L 03/07/15 06:20 91-20-31.0 1
Styrene ND ug/L 03/07/15 06:20 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 03/07/15 06:20 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 03/07/15 06:20 79-34-51.0 1
Tetrachloroethene ND ug/L 03/07/15 06:20 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Sample:TMW-1 Lab ID:92239514006 Collected:02/28/15 14:30 Received:03/03/15 16:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Toluene 8.1 ug/L 03/07/15 06:20 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 03/07/15 06:20 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 03/07/15 06:20 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 03/07/15 06:20 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 03/07/15 06:20 79-00-51.0 1
Trichloroethene ND ug/L 03/07/15 06:20 79-01-61.0 1
Trichlorofluoromethane ND ug/L 03/07/15 06:20 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 03/07/15 06:20 96-18-41.0 1
Vinyl acetate ND ug/L 03/07/15 06:20 108-05-42.0 1
Vinyl chloride ND ug/L 03/07/15 06:20 75-01-41.0 1
Xylene (Total)ND ug/L 03/07/15 06:20 1330-20-72.0 1
m&p-Xylene ND ug/L 03/07/15 06:20 179601-23-12.0 1
o-Xylene ND ug/L 03/07/15 06:20 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)107 %03/07/15 06:20 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %03/07/15 06:20 17060-07-070-130 1
Toluene-d8 (S)98 %03/07/15 06:20 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/7637
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:92239514004, 92239514005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1403560
Associated Lab Samples:92239514004, 92239514005
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0050 03/06/15 14:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1403561LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.063.067 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1403562MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92239514004
1403563
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/kg M1.06 70 75-12571 2.0580.024 0.066 0.065
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/18024
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:92239514004, 92239514005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1405113
Associated Lab Samples:92239514004, 92239514005
Matrix:Solid
Analyzed
Arsenic mg/kg ND 1.0 03/06/15 21:41
Barium mg/kg ND 0.50 03/06/15 21:41
Cadmium mg/kg ND 0.10 03/06/15 21:41
Chromium mg/kg ND 0.50 03/06/15 21:41
Lead mg/kg ND 0.50 03/06/15 21:41
Selenium mg/kg ND 1.0 03/06/15 21:41
Silver mg/kg ND 0.50 03/06/15 21:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1405114LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 48.250 96 80-120
Barium mg/kg 50.250 100 80-120
Cadmium mg/kg 49.650 99 80-120
Chromium mg/kg 48.950 98 80-120
Lead mg/kg 48.350 97 80-120
Selenium mg/kg 48.850 98 80-120
Silver mg/kg 24.725 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1405115MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92239514004
1405116
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic mg/kg M146.1 76 75-12574 544.6ND 34.8 33.0
Barium mg/kg M1,R146.1 -249 75-125-113 2944.6302 187 251
Cadmium mg/kg 46.1 81 75-12580 444.60.13 37.2 35.7
Chromium mg/kg M146.1 -11 75-12510 1244.678.2 73.2 82.7
Lead mg/kg 46.1 79 75-12578 444.65.1 41.6 40.1
Selenium mg/kg M146.1 72 75-12570 644.61.6 34.7 32.8
Silver mg/kg 23 83 75-12582 422.3ND 19.4 18.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30594
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92239514006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1403659
Associated Lab Samples:92239514006
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 03/06/15 21:54
1,1,1-Trichloroethane ug/L ND 1.0 03/06/15 21:54
1,1,2,2-Tetrachloroethane ug/L ND 1.0 03/06/15 21:54
1,1,2-Trichloroethane ug/L ND 1.0 03/06/15 21:54
1,1-Dichloroethane ug/L ND 1.0 03/06/15 21:54
1,1-Dichloroethene ug/L ND 1.0 03/06/15 21:54
1,1-Dichloropropene ug/L ND 1.0 03/06/15 21:54
1,2,3-Trichlorobenzene ug/L ND 1.0 03/06/15 21:54
1,2,3-Trichloropropane ug/L ND 1.0 03/06/15 21:54
1,2,4-Trichlorobenzene ug/L ND 1.0 03/06/15 21:54
1,2-Dibromo-3-chloropropane ug/L ND 2.0 03/06/15 21:54
1,2-Dibromoethane (EDB)ug/L ND 1.0 03/06/15 21:54
1,2-Dichlorobenzene ug/L ND 1.0 03/06/15 21:54
1,2-Dichloroethane ug/L ND 1.0 03/06/15 21:54
1,2-Dichloropropane ug/L ND 1.0 03/06/15 21:54
1,3-Dichlorobenzene ug/L ND 1.0 03/06/15 21:54
1,3-Dichloropropane ug/L ND 1.0 03/06/15 21:54
1,4-Dichlorobenzene ug/L ND 1.0 03/06/15 21:54
2,2-Dichloropropane ug/L ND 1.0 03/06/15 21:54
2-Butanone (MEK)ug/L ND 5.0 03/06/15 21:54
2-Chlorotoluene ug/L ND 1.0 03/06/15 21:54
2-Hexanone ug/L ND 5.0 03/06/15 21:54
4-Chlorotoluene ug/L ND 1.0 03/06/15 21:54
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 03/06/15 21:54
Acetone ug/L ND 25.0 03/06/15 21:54
Benzene ug/L ND 1.0 03/06/15 21:54
Bromobenzene ug/L ND 1.0 03/06/15 21:54
Bromochloromethane ug/L ND 1.0 03/06/15 21:54
Bromodichloromethane ug/L ND 1.0 03/06/15 21:54
Bromoform ug/L ND 1.0 03/06/15 21:54
Bromomethane ug/L ND 2.0 03/06/15 21:54
Carbon tetrachloride ug/L ND 1.0 03/06/15 21:54
Chlorobenzene ug/L ND 1.0 03/06/15 21:54
Chloroethane ug/L ND 1.0 03/06/15 21:54
Chloroform ug/L ND 1.0 03/06/15 21:54
Chloromethane ug/L ND 1.0 03/06/15 21:54
cis-1,2-Dichloroethene ug/L ND 1.0 03/06/15 21:54
cis-1,3-Dichloropropene ug/L ND 1.0 03/06/15 21:54
Dibromochloromethane ug/L ND 1.0 03/06/15 21:54
Dibromomethane ug/L ND 1.0 03/06/15 21:54
Dichlorodifluoromethane ug/L ND 1.0 03/06/15 21:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
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Page 18 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1403659
Associated Lab Samples:92239514006
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 1.0 03/06/15 21:54
Ethylbenzene ug/L ND 1.0 03/06/15 21:54
Hexachloro-1,3-butadiene ug/L ND 1.0 03/06/15 21:54
m&p-Xylene ug/L ND 2.0 03/06/15 21:54
Methyl-tert-butyl ether ug/L ND 1.0 03/06/15 21:54
Methylene Chloride ug/L ND 2.0 03/06/15 21:54
Naphthalene ug/L ND 1.0 03/06/15 21:54
o-Xylene ug/L ND 1.0 03/06/15 21:54
p-Isopropyltoluene ug/L ND 1.0 03/06/15 21:54
Styrene ug/L ND 1.0 03/06/15 21:54
Tetrachloroethene ug/L ND 1.0 03/06/15 21:54
Toluene ug/L ND 1.0 03/06/15 21:54
trans-1,2-Dichloroethene ug/L ND 1.0 03/06/15 21:54
trans-1,3-Dichloropropene ug/L ND 1.0 03/06/15 21:54
Trichloroethene ug/L ND 1.0 03/06/15 21:54
Trichlorofluoromethane ug/L ND 1.0 03/06/15 21:54
Vinyl acetate ug/L ND 2.0 03/06/15 21:54
Vinyl chloride ug/L ND 1.0 03/06/15 21:54
Xylene (Total)ug/L ND 2.0 03/06/15 21:54
1,2-Dichloroethane-d4 (S)%99 70-130 03/06/15 21:54
4-Bromofluorobenzene (S)%101 70-130 03/06/15 21:54
Toluene-d8 (S)%98 70-130 03/06/15 21:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1403660LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 45.850 92 70-130
1,1,1-Trichloroethane ug/L 46.550 93 70-130
1,1,2,2-Tetrachloroethane ug/L 44.350 89 70-130
1,1,2-Trichloroethane ug/L 45.450 91 70-130
1,1-Dichloroethane ug/L 43.150 86 70-130
1,1-Dichloroethene ug/L 45.650 91 70-132
1,1-Dichloropropene ug/L 49.650 99 70-130
1,2,3-Trichlorobenzene ug/L 49.050 98 70-135
1,2,3-Trichloropropane ug/L 42.550 85 70-130
1,2,4-Trichlorobenzene ug/L 49.350 99 70-134
1,2-Dibromo-3-chloropropane ug/L 47.250 94 70-130
1,2-Dibromoethane (EDB)ug/L 45.850 92 70-130
1,2-Dichlorobenzene ug/L 44.550 89 70-130
1,2-Dichloroethane ug/L 41.850 84 70-130
1,2-Dichloropropane ug/L 44.150 88 70-130
1,3-Dichlorobenzene ug/L 43.450 87 70-130
1,3-Dichloropropane ug/L 43.650 87 70-130
1,4-Dichlorobenzene ug/L 43.150 86 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 19 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1403660LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 43.450 87 58-145
2-Butanone (MEK)ug/L 89.9100 90 70-145
2-Chlorotoluene ug/L 43.350 87 70-130
2-Hexanone ug/L 105100 105 70-144
4-Chlorotoluene ug/L 42.250 84 70-130
4-Methyl-2-pentanone (MIBK)ug/L 95.4100 95 70-140
Acetone ug/L 94.3100 94 50-175
Benzene ug/L 45.850 92 70-130
Bromobenzene ug/L 43.750 87 70-130
Bromochloromethane ug/L 45.250 90 70-130
Bromodichloromethane ug/L 42.150 84 70-130
Bromoform ug/L 40.850 82 70-130
Bromomethane ug/L 40.450 81 54-130
Carbon tetrachloride ug/L 50.650 101 70-132
Chlorobenzene ug/L 43.950 88 70-130
Chloroethane ug/L 47.150 94 64-134
Chloroform ug/L 40.150 80 70-130
Chloromethane ug/L 44.450 89 64-130
cis-1,2-Dichloroethene ug/L 43.950 88 70-131
cis-1,3-Dichloropropene ug/L 46.550 93 70-130
Dibromochloromethane ug/L 43.150 86 70-130
Dibromomethane ug/L 47.650 95 70-131
Dichlorodifluoromethane ug/L 52.250 104 56-130
Diisopropyl ether ug/L 42.850 86 70-130
Ethylbenzene ug/L 44.650 89 70-130
Hexachloro-1,3-butadiene ug/L 51.850 104 70-130
m&p-Xylene ug/L 89.6100 90 70-130
Methyl-tert-butyl ether ug/L 43.650 87 70-130
Methylene Chloride ug/L 48.650 97 63-130
Naphthalene ug/L 48.950 98 70-138
o-Xylene ug/L 43.350 87 70-130
p-Isopropyltoluene ug/L 45.950 92 70-130
Styrene ug/L 46.350 93 70-130
Tetrachloroethene ug/L 47.750 95 70-130
Toluene ug/L 45.250 90 70-130
trans-1,2-Dichloroethene ug/L 44.150 88 70-130
trans-1,3-Dichloropropene ug/L 48.050 96 70-132
Trichloroethene ug/L 45.250 90 70-130
Trichlorofluoromethane ug/L 46.750 93 62-133
Vinyl acetate ug/L 90.7100 91 66-157
Vinyl chloride ug/L 47.350 95 50-150
Xylene (Total)ug/L 133150 89 70-130
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30575
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92239514001, 92239514002, 92239514003, 92239514004, 92239514005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1402126
Associated Lab Samples:92239514001, 92239514002, 92239514003, 92239514004, 92239514005
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.5 03/04/15 11:51
1,1,1-Trichloroethane ug/kg ND 5.5 03/04/15 11:51
1,1,2,2-Tetrachloroethane ug/kg ND 5.5 03/04/15 11:51
1,1,2-Trichloroethane ug/kg ND 5.5 03/04/15 11:51
1,1-Dichloroethane ug/kg ND 5.5 03/04/15 11:51
1,1-Dichloroethene ug/kg ND 5.5 03/04/15 11:51
1,1-Dichloropropene ug/kg ND 5.5 03/04/15 11:51
1,2,3-Trichlorobenzene ug/kg ND 5.5 03/04/15 11:51
1,2,3-Trichloropropane ug/kg ND 5.5 03/04/15 11:51
1,2,4-Trichlorobenzene ug/kg ND 5.5 03/04/15 11:51
1,2,4-Trimethylbenzene ug/kg ND 5.5 03/04/15 11:51
1,2-Dibromo-3-chloropropane ug/kg ND 5.5 03/04/15 11:51
1,2-Dibromoethane (EDB)ug/kg ND 5.5 03/04/15 11:51
1,2-Dichlorobenzene ug/kg ND 5.5 03/04/15 11:51
1,2-Dichloroethane ug/kg ND 5.5 03/04/15 11:51
1,2-Dichloropropane ug/kg ND 5.5 03/04/15 11:51
1,3,5-Trimethylbenzene ug/kg ND 5.5 03/04/15 11:51
1,3-Dichlorobenzene ug/kg ND 5.5 03/04/15 11:51
1,3-Dichloropropane ug/kg ND 5.5 03/04/15 11:51
1,4-Dichlorobenzene ug/kg ND 5.5 03/04/15 11:51
2,2-Dichloropropane ug/kg ND 5.5 03/04/15 11:51
2-Butanone (MEK)ug/kg ND 109 03/04/15 11:51
2-Chlorotoluene ug/kg ND 5.5 03/04/15 11:51
2-Hexanone ug/kg ND 54.6 03/04/15 11:51
4-Chlorotoluene ug/kg ND 5.5 03/04/15 11:51
4-Methyl-2-pentanone (MIBK)ug/kg ND 54.6 03/04/15 11:51
Acetone ug/kg ND 109 03/04/15 11:51
Benzene ug/kg ND 5.5 03/04/15 11:51
Bromobenzene ug/kg ND 5.5 03/04/15 11:51
Bromochloromethane ug/kg ND 5.5 03/04/15 11:51
Bromodichloromethane ug/kg ND 5.5 03/04/15 11:51
Bromoform ug/kg ND 5.5 03/04/15 11:51
Bromomethane ug/kg ND 10.9 03/04/15 11:51
Carbon tetrachloride ug/kg ND 5.5 03/04/15 11:51
Chlorobenzene ug/kg ND 5.5 03/04/15 11:51
Chloroethane ug/kg ND 10.9 03/04/15 11:51
Chloroform ug/kg ND 5.5 03/04/15 11:51
Chloromethane ug/kg ND 10.9 03/04/15 11:51
cis-1,2-Dichloroethene ug/kg ND 5.5 03/04/15 11:51
cis-1,3-Dichloropropene ug/kg ND 5.5 03/04/15 11:51
Dibromochloromethane ug/kg ND 5.5 03/04/15 11:51
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
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Page 21 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1402126
Associated Lab Samples:92239514001, 92239514002, 92239514003, 92239514004, 92239514005
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 5.5 03/04/15 11:51
Dichlorodifluoromethane ug/kg ND 10.9 03/04/15 11:51
Diisopropyl ether ug/kg ND 5.5 03/04/15 11:51
Ethylbenzene ug/kg ND 5.5 03/04/15 11:51
Hexachloro-1,3-butadiene ug/kg ND 5.5 03/04/15 11:51
Isopropylbenzene (Cumene)ug/kg ND 5.5 03/04/15 11:51
m&p-Xylene ug/kg ND 10.9 03/04/15 11:51
Methyl-tert-butyl ether ug/kg ND 5.5 03/04/15 11:51
Methylene Chloride ug/kg ND 21.8 03/04/15 11:51
n-Butylbenzene ug/kg ND 5.5 03/04/15 11:51
n-Propylbenzene ug/kg ND 5.5 03/04/15 11:51
Naphthalene ug/kg ND 5.5 03/04/15 11:51
o-Xylene ug/kg ND 5.5 03/04/15 11:51
p-Isopropyltoluene ug/kg ND 5.5 03/04/15 11:51
sec-Butylbenzene ug/kg ND 5.5 03/04/15 11:51
Styrene ug/kg ND 5.5 03/04/15 11:51
tert-Butylbenzene ug/kg ND 5.5 03/04/15 11:51
Tetrachloroethene ug/kg ND 5.5 03/04/15 11:51
Toluene ug/kg ND 5.5 03/04/15 11:51
trans-1,2-Dichloroethene ug/kg ND 5.5 03/04/15 11:51
trans-1,3-Dichloropropene ug/kg ND 5.5 03/04/15 11:51
Trichloroethene ug/kg ND 5.5 03/04/15 11:51
Trichlorofluoromethane ug/kg ND 5.5 03/04/15 11:51
Vinyl acetate ug/kg ND 54.6 03/04/15 11:51
Vinyl chloride ug/kg ND 10.9 03/04/15 11:51
Xylene (Total)ug/kg ND 10.9 03/04/15 11:51
1,2-Dichloroethane-d4 (S)%97 70-132 03/04/15 11:51
4-Bromofluorobenzene (S)%95 70-130 03/04/15 11:51
Toluene-d8 (S)%103 70-130 03/04/15 11:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1402127LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 54.854.9 100 74-137
1,1,1-Trichloroethane ug/kg 56.554.9 103 67-140
1,1,2,2-Tetrachloroethane ug/kg 52.354.9 95 72-141
1,1,2-Trichloroethane ug/kg 54.854.9 100 78-138
1,1-Dichloroethane ug/kg 66.554.9 121 69-134
1,1-Dichloroethene ug/kg 61.954.9 113 67-138
1,1-Dichloropropene ug/kg 62.854.9 114 69-139
1,2,3-Trichlorobenzene ug/kg 55.554.9 101 70-146
1,2,3-Trichloropropane ug/kg 48.354.9 88 69-144
1,2,4-Trichlorobenzene ug/kg 57.954.9 105 68-148
1,2,4-Trimethylbenzene ug/kg 57.354.9 104 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1402127LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 51.954.9 94 65-140
1,2-Dibromoethane (EDB)ug/kg 55.354.9 101 77-135
1,2-Dichlorobenzene ug/kg 55.554.9 101 77-141
1,2-Dichloroethane ug/kg 52.054.9 95 65-137
1,2-Dichloropropane ug/kg 57.954.9 105 72-136
1,3,5-Trimethylbenzene ug/kg 56.754.9 103 76-133
1,3-Dichlorobenzene ug/kg 55.254.9 100 74-138
1,3-Dichloropropane ug/kg 55.654.9 101 71-139
1,4-Dichlorobenzene ug/kg 56.754.9 103 76-138
2,2-Dichloropropane ug/kg 58.854.9 107 68-137
2-Butanone (MEK)ug/kg 101J110 92 58-147
2-Chlorotoluene ug/kg 55.954.9 102 73-139
2-Hexanone ug/kg 108110 98 62-145
4-Chlorotoluene ug/kg 55.454.9 101 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 106110 96 64-149
Acetone ug/kg 106J110 97 53-153
Benzene ug/kg 61.554.9 112 73-135
Bromobenzene ug/kg 62.654.9 114 75-133
Bromochloromethane ug/kg 62.154.9 113 73-134
Bromodichloromethane ug/kg 50.254.9 91 71-135
Bromoform ug/kg 52.254.9 95 66-141
Bromomethane ug/kg 62.254.9 113 53-160
Carbon tetrachloride ug/kg 55.454.9 101 60-145
Chlorobenzene ug/kg 56.354.9 102 78-130
Chloroethane ug/kg 77.454.9 141 64-149
Chloroform ug/kg 55.554.9 101 70-134
Chloromethane ug/kg 64.054.9 116 52-150
cis-1,2-Dichloroethene ug/kg 66.654.9 121 70-133
cis-1,3-Dichloropropene ug/kg 57.754.9 105 68-134
Dibromochloromethane ug/kg 49.054.9 89 71-138
Dibromomethane ug/kg 54.054.9 98 74-130
Dichlorodifluoromethane ug/kg 71.354.9 130 40-160
Diisopropyl ether ug/kg 61.954.9 113 69-141
Ethylbenzene ug/kg 56.054.9 102 75-133
Hexachloro-1,3-butadiene ug/kg 57.354.9 104 68-143
Isopropylbenzene (Cumene)ug/kg 55.554.9 101 76-143
m&p-Xylene ug/kg 104110 95 75-136
Methyl-tert-butyl ether ug/kg 56.654.9 103 68-144
Methylene Chloride ug/kg 68.554.9 125 45-154
n-Butylbenzene ug/kg 56.254.9 102 72-137
n-Propylbenzene ug/kg 61.754.9 112 76-136
Naphthalene ug/kg 55.954.9 102 68-151
o-Xylene ug/kg 54.754.9 100 76-141
p-Isopropyltoluene ug/kg 55.154.9 100 76-140
sec-Butylbenzene ug/kg 61.554.9 112 79-139
Styrene ug/kg 57.254.9 104 79-137
tert-Butylbenzene ug/kg 54.754.9 100 74-143
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
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[phone]
Page 23 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1402127LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 57.154.9 104 71-138
Toluene ug/kg 57.354.9 104 74-131
trans-1,2-Dichloroethene ug/kg 66.154.9 120 67-135
trans-1,3-Dichloropropene ug/kg 55.354.9 101 65-146
Trichloroethene ug/kg 58.054.9 105 67-135
Trichlorofluoromethane ug/kg 61.254.9 111 59-144
Vinyl acetate ug/kg 100 F31109140-160
Vinyl chloride ug/kg 64.854.9 118 56-141
Xylene (Total)ug/kg 159165 97 76-137
1,2-Dichloroethane-d4 (S)%88 70-132
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1402902MATRIX SPIKE SAMPLE:
MSSpike
Result
92239497001
1,1,1,2-Tetrachloroethane ug/kg 11.413 88 70-130ND
1,1,1-Trichloroethane ug/kg 11.313 88 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 16.713 129 70-130ND
1,1,2-Trichloroethane ug/kg 14.013 108 70-130ND
1,1-Dichloroethane ug/kg 12.613 97 70-130ND
1,1-Dichloroethene ug/kg 11.013 85 49-180ND
1,1-Dichloropropene ug/kg 12.813 99 70-130ND
1,2,3-Trichlorobenzene ug/kg 9.0 M1136970-130ND
1,2,3-Trichloropropane ug/kg 14.613 113 70-130ND
1,2,4-Trichlorobenzene ug/kg 9.213 71 70-130ND
1,2,4-Trimethylbenzene ug/kg 11.113 85 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 17.4 M11313570-130ND
1,2-Dibromoethane (EDB)ug/kg 14.213 110 70-130ND
1,2-Dichlorobenzene ug/kg 11.713 90 70-130ND
1,2-Dichloroethane ug/kg 13.613 105 70-130ND
1,2-Dichloropropane ug/kg 12.813 99 70-130ND
1,3,5-Trimethylbenzene ug/kg 10.613 82 70-130ND
1,3-Dichlorobenzene ug/kg 10.813 84 70-130ND
1,3-Dichloropropane ug/kg 14.213 110 70-130ND
1,4-Dichlorobenzene ug/kg 12.513 83 70-130ND
2,2-Dichloropropane ug/kg 11.513 89 70-130ND
2-Butanone (MEK)ug/kg 33.3J25.8 129 70-130ND
2-Chlorotoluene ug/kg 11.313 87 70-130ND
2-Hexanone ug/kg 38.8 M125.8 150 70-130ND
4-Chlorotoluene ug/kg 11.213 87 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 36.7 M125.8 142 70-130ND
Acetone ug/kg 39.5J M125.8 153 70-130ND
Benzene ug/kg 13.913 107 50-166ND
Bromobenzene ug/kg 13.913 107 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1402902MATRIX SPIKE SAMPLE:
MSSpike
Result
92239497001
Bromochloromethane ug/kg 14.113 109 70-130ND
Bromodichloromethane ug/kg 10.513 81 70-130ND
Bromoform ug/kg 13.713 106 70-130ND
Bromomethane ug/kg 12.813 99 70-130ND
Carbon tetrachloride ug/kg 9.113 71 70-130ND
Chlorobenzene ug/kg 11.613 90 43-169ND
Chloroethane ug/kg 16.713 129 70-130ND
Chloroform ug/kg 11.413 88 70-130ND
Chloromethane ug/kg 13.213 102 70-130ND
cis-1,2-Dichloroethene ug/kg 14.813 115 70-130ND
cis-1,3-Dichloropropene ug/kg 13.113 102 70-130ND
Dibromochloromethane ug/kg 11.913 92 70-130ND
Dibromomethane ug/kg 13.913 108 70-130ND
Dichlorodifluoromethane ug/kg 13.913 108 70-130ND
Diisopropyl ether ug/kg 15.313 118 70-130ND
Ethylbenzene ug/kg 11.113 86 70-130ND
Hexachloro-1,3-butadiene ug/kg 6.2 M1134870-130ND
Isopropylbenzene (Cumene)ug/kg 10.213 79 70-130ND
m&p-Xylene ug/kg 21.025.8 81 70-130ND
Methyl-tert-butyl ether ug/kg 16.613 128 70-130ND
Methylene Chloride ug/kg 15.813 122 70-130ND
n-Butylbenzene ug/kg 9.313 72 70-130ND
n-Propylbenzene ug/kg 8.6 M1136670-130ND
Naphthalene ug/kg 12.513 95 70-130ND
o-Xylene ug/kg 10.913 84 70-130ND
p-Isopropyltoluene ug/kg 9.413 73 70-130ND
sec-Butylbenzene ug/kg 7.3 M1135670-130ND
Styrene ug/kg 9.713 75 70-130ND
tert-Butylbenzene ug/kg 9.813 76 70-130ND
Tetrachloroethene ug/kg 10.513 81 70-130ND
Toluene ug/kg 12.513 96 52-163ND
trans-1,2-Dichloroethene ug/kg 12.513 97 70-130ND
trans-1,3-Dichloropropene ug/kg 13.913 108 70-130ND
Trichloroethene ug/kg 11.413 88 49-167ND
Trichlorofluoromethane ug/kg 12.013 93 70-130ND
Vinyl acetate ug/kg 34.8 M125.8 135 70-130ND
Vinyl chloride ug/kg 13.113 101 70-130ND
1,2-Dichloroethane-d4 (S)%111 70-132
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%103 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92239309007
1402901SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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Page 25 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92239309007
1402901SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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Page 26 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92239309007
1402901SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%109 7889
4-Bromofluorobenzene (S)%97 6395
Toluene-d8 (S)%102 62100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
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Page 27 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/33328
EPA 3546
EPA 8015 Modified
8015 Solid GCSV
Associated Lab Samples:92239514001, 92239514002, 92239514003, 92239514004, 92239514005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1402525
Associated Lab Samples:92239514001, 92239514002, 92239514003, 92239514004, 92239514005
Matrix:Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 5.0 03/05/15 11:33
n-Pentacosane (S)%86 41-119 03/05/15 11:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1402526LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 58.466.7 88 49-113
n-Pentacosane (S)%84 41-119
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1402527MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92239514003
1402528
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Diesel Range Organics(C10-
C28)mg/kg 91.5 73 10-14660 1791.59.7 76.2 64.4
n-Pentacosane (S)%74 41-11968
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
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Page 28 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/7575
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92239514001, 92239514002, 92239514003, 92239514004, 92239514005
Parameter Units
Dup
Result QualifiersRPDResult
92239332001
1402811SAMPLE DUPLICATE:
Percent Moisture %18.5 218.2
Parameter Units
Dup
Result QualifiersRPDResult
92239514005
1402812SAMPLE DUPLICATE:
Percent Moisture %10.3 1011.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/11/2015 09:21 AM
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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Page 30 of 33
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92239514
HENDRICK DURHAM AUTOMALL
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92239514001 OEXT/33328 GCSV/20532SS-1 EPA 3546 EPA 8015 Modified
92239514002 OEXT/33328 GCSV/20532SS-3 EPA 3546 EPA 8015 Modified
92239514003 OEXT/33328 GCSV/20532SS-5 EPA 3546 EPA 8015 Modified
92239514004 OEXT/33328 GCSV/20532SS-2 EPA 3546 EPA 8015 Modified
92239514005 OEXT/33328 GCSV/20532SS-4 EPA 3546 EPA 8015 Modified
92239514004 MPRP/18024 ICP/16202SS-2 EPA 3050 EPA 6010
92239514005 MPRP/18024 ICP/16202SS-4 EPA 3050 EPA 6010
92239514004 MERP/7637 MERC/7330SS-2 EPA 7471 EPA 7471
92239514005 MERP/7637 MERC/7330SS-4 EPA 7471 EPA 7471
92239514006 MSV/30594TMW-1 EPA 8260
92239514001 MSV/30575SS-1 EPA 8260
92239514002 MSV/30575SS-3 EPA 8260
92239514003 MSV/30575SS-5 EPA 8260
92239514004 MSV/30575SS-2 EPA 8260
92239514005 MSV/30575SS-4 EPA 8260
92239514001 PMST/7575SS-1 ASTM D2974-87
92239514002 PMST/7575SS-3 ASTM D2974-87
92239514003 PMST/7575SS-5 ASTM D2974-87
92239514004 PMST/7575SS-2 ASTM D2974-87
92239514005 PMST/7575SS-4 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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Page 31 of 33
Page 32 of 33
Page 33 of 33
#=CL#
March 16, 2015
LIMS USE: FR - MATTHEW GILLIS
LIMS OBJECT ID: 92240297
92240297
Project:
Pace Project No.:
RE:
Matthew Gillis
ECS
9001 Glenwood Avenue
Raleigh, NC 27617
HENDRICK DURHAM AUTO 22255-A
Dear Matthew Gillis:
Enclosed are the analytical results for sample(s) received by the laboratory on March 09, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
Enclosures
cc:Matthew Gillis, ECS
Brian Smith, ECS Carolinas LLP
REPORT OF LABORATORY ANALYSIS
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Page 1 of 73
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Page 2 of 73
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92240297001 SS-6
Barium 68.0 mg/kg 03/10/15 23:320.44EPA 6010
Chromium 4.2 mg/kg 03/10/15 23:320.44EPA 6010
Lead 6.5 mg/kg 03/10/15 23:320.44EPA 6010
Percent Moisture 8.5 %03/11/15 10:180.10ASTM D2974-87
92240297002 SS-7
Percent Moisture 23.8 %03/11/15 10:180.10ASTM D2974-87
92240297003 SS-8
Diesel Range Organics(C10-C28)111 mg/kg 03/13/15 16:165.6EPA 8015 Modified
Percent Moisture 11.2 %03/11/15 10:190.10ASTM D2974-87
92240297004 SS-9
Barium 75.1 mg/kg 03/10/15 23:410.49EPA 6010
Cadmium 0.12 mg/kg 03/10/15 23:410.098EPA 6010
Chromium 20.8 mg/kg 03/10/15 23:410.49EPA 6010
Lead 7.4 mg/kg 03/10/15 23:410.49EPA 6010
Silver 2.0 mg/kg 03/10/15 23:410.49EPA 6010
Percent Moisture 14.6 %03/11/15 10:190.10ASTM D2974-87
92240297005 SS-10
Diesel Range Organics(C10-C28)130 mg/kg 03/13/15 16:405.5EPA 8015 Modified
Percent Moisture 9.9 %03/11/15 10:230.10ASTM D2974-87
92240297006 SS-11
Diesel Range Organics(C10-C28)165 mg/kg 03/13/15 17:035.5EPA 8015 Modified
Barium 72.4 mg/kg 03/13/15 00:500.42EPA 6010
Chromium 10.4 mg/kg 03/13/15 00:500.42EPA 6010
Lead 4.2 mg/kg 03/13/15 00:500.42EPA 6010
Silver 0.62 mg/kg 03/13/15 00:500.42EPA 6010
Percent Moisture 9.4 %03/11/15 10:240.10ASTM D2974-87
92240297007 SS-12
Diesel Range Organics(C10-C28)83.0 mg/kg 03/13/15 17:035.7EPA 8015 Modified
Percent Moisture 11.8 %03/11/15 10:240.10ASTM D2974-87
92240297008 SS-13
Diesel Range Organics(C10-C28)24.2 mg/kg 03/13/15 17:276.7EPA 8015 Modified
Percent Moisture 25.7 %03/11/15 10:240.10ASTM D2974-87
92240297009 SS-14
Barium 47.4 mg/kg 03/13/15 00:530.47EPA 6010
Chromium 4.0 mg/kg 03/13/15 00:530.47EPA 6010
Lead 10.3 mg/kg 03/13/15 00:530.47EPA 6010
Percent Moisture 16.9 %03/11/15 10:240.10ASTM D2974-87
92240297010 SS-15
Percent Moisture 15.4 %03/11/15 10:240.10ASTM D2974-87
92240297012 TMW-3
bis(2-Ethylhexyl)phthalate 7.3 ug/L 03/12/15 13:076.0EPA 8270
REPORT OF LABORATORY ANALYSIS
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#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92240297013 TMW-4
Acetone 281 ug/L 03/11/15 22:0725.0EPA 8260
Benzene 2.0 ug/L 03/11/15 22:071.0EPA 8260
2-Butanone (MEK)9.1 ug/L 03/11/15 22:075.0EPA 8260
Ethylbenzene 5.4 ug/L 03/11/15 22:071.0EPA 8260
Naphthalene 1.4 ug/L 03/11/15 22:071.0EPA 8260
Toluene 8.5 ug/L 03/11/15 22:071.0EPA 8260
Xylene (Total)22.4 ug/L 03/11/15 22:072.0EPA 8260
m&p-Xylene 11.4 ug/L 03/11/15 22:072.0EPA 8260
o-Xylene 11.1 ug/L 03/11/15 22:071.0EPA 8260
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-6 Lab ID:92240297001 Collected:03/06/15 11:55 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 03/13/15 15:5203/12/15 10:185.5 1
Surrogates
n-Pentacosane (S)57 %03/13/15 15:52 629-99-203/12/15 10:1841-119 1
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Arsenic ND mg/kg 03/10/15 23:32 7440-38-203/10/15 16:300.88 1
Barium 68.0 mg/kg 03/10/15 23:32 7440-39-303/10/15 16:300.44 1
Cadmium ND mg/kg 03/10/15 23:32 7440-43-903/10/15 16:300.088 1
Chromium 4.2 mg/kg 03/10/15 23:32 7440-47-303/10/15 16:300.44 1
Lead 6.5 mg/kg 03/10/15 23:32 7439-92-103/10/15 16:300.44 1
Selenium ND mg/kg 03/10/15 23:32 7782-49-203/10/15 16:300.88 1
Silver ND mg/kg 03/10/15 23:32 7440-22-403/10/15 16:300.44 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury ND mg/kg 03/12/15 14:10 7439-97-603/11/15 13:500.0044 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/11/15 19:34 67-64-182.8 1
Benzene ND ug/kg 03/11/15 19:34 71-43-24.1 1
Bromobenzene ND ug/kg 03/11/15 19:34 108-86-14.1 1
Bromochloromethane ND ug/kg 03/11/15 19:34 74-97-54.1 1
Bromodichloromethane ND ug/kg 03/11/15 19:34 75-27-44.1 1
Bromoform ND ug/kg 03/11/15 19:34 75-25-24.1 1
Bromomethane ND ug/kg 03/11/15 19:34 74-83-98.3 1
2-Butanone (MEK)ND ug/kg 03/11/15 19:34 78-93-382.8 1
n-Butylbenzene ND ug/kg 03/11/15 19:34 104-51-84.1 1
sec-Butylbenzene ND ug/kg 03/11/15 19:34 135-98-84.1 1
tert-Butylbenzene ND ug/kg 03/11/15 19:34 98-06-64.1 1
Carbon tetrachloride ND ug/kg 03/11/15 19:34 56-23-54.1 1
Chlorobenzene ND ug/kg 03/11/15 19:34 108-90-74.1 1
Chloroethane ND ug/kg 03/11/15 19:34 75-00-38.3 1
Chloroform ND ug/kg 03/11/15 19:34 67-66-34.1 1
Chloromethane ND ug/kg 03/11/15 19:34 74-87-38.3 1
2-Chlorotoluene ND ug/kg 03/11/15 19:34 95-49-84.1 1
4-Chlorotoluene ND ug/kg 03/11/15 19:34 106-43-44.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/11/15 19:34 96-12-84.1 1
Dibromochloromethane ND ug/kg 03/11/15 19:34 124-48-14.1 1
1,2-Dibromoethane (EDB)ND ug/kg 03/11/15 19:34 106-93-44.1 1
Dibromomethane ND ug/kg 03/11/15 19:34 74-95-34.1 1
1,2-Dichlorobenzene ND ug/kg 03/11/15 19:34 95-50-14.1 1
1,3-Dichlorobenzene ND ug/kg 03/11/15 19:34 541-73-14.1 1
1,4-Dichlorobenzene ND ug/kg 03/11/15 19:34 106-46-74.1 1
Dichlorodifluoromethane ND ug/kg 03/11/15 19:34 75-71-88.3 1
1,1-Dichloroethane ND ug/kg 03/11/15 19:34 75-34-34.1 1
1,2-Dichloroethane ND ug/kg 03/11/15 19:34 107-06-24.1 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-6 Lab ID:92240297001 Collected:03/06/15 11:55 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
1,1-Dichloroethene ND ug/kg 03/11/15 19:34 75-35-44.1 1
cis-1,2-Dichloroethene ND ug/kg 03/11/15 19:34 156-59-24.1 1
trans-1,2-Dichloroethene ND ug/kg 03/11/15 19:34 156-60-54.1 1
1,2-Dichloropropane ND ug/kg 03/11/15 19:34 78-87-54.1 1
1,3-Dichloropropane ND ug/kg 03/11/15 19:34 142-28-94.1 1
2,2-Dichloropropane ND ug/kg 03/11/15 19:34 594-20-74.1 1
1,1-Dichloropropene ND ug/kg 03/11/15 19:34 563-58-64.1 1
cis-1,3-Dichloropropene ND ug/kg 03/11/15 19:34 10061-01-54.1 1
trans-1,3-Dichloropropene ND ug/kg 03/11/15 19:34 10061-02-64.1 1
Diisopropyl ether ND ug/kg 03/11/15 19:34 108-20-34.1 1
Ethylbenzene ND ug/kg 03/11/15 19:34 100-41-44.1 1
Hexachloro-1,3-butadiene ND ug/kg 03/11/15 19:34 87-68-34.1 1
2-Hexanone ND ug/kg 03/11/15 19:34 591-78-641.4 1
Isopropylbenzene (Cumene)ND ug/kg 03/11/15 19:34 98-82-84.1 1
p-Isopropyltoluene ND ug/kg 03/11/15 19:34 99-87-64.1 1
Methylene Chloride ND ug/kg 03/11/15 19:34 75-09-216.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/11/15 19:34 108-10-141.4 1
Methyl-tert-butyl ether ND ug/kg 03/11/15 19:34 1634-04-44.1 1
Naphthalene ND ug/kg 03/11/15 19:34 91-20-34.1 1
n-Propylbenzene ND ug/kg 03/11/15 19:34 103-65-14.1 1
Styrene ND ug/kg 03/11/15 19:34 100-42-54.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/11/15 19:34 630-20-64.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/11/15 19:34 79-34-54.1 1
Tetrachloroethene ND ug/kg 03/11/15 19:34 127-18-44.1 1
Toluene ND ug/kg 03/11/15 19:34 108-88-34.1 1
1,2,3-Trichlorobenzene ND ug/kg 03/11/15 19:34 87-61-64.1 1
1,2,4-Trichlorobenzene ND ug/kg 03/11/15 19:34 120-82-14.1 1
1,1,1-Trichloroethane ND ug/kg 03/11/15 19:34 71-55-64.1 1
1,1,2-Trichloroethane ND ug/kg 03/11/15 19:34 79-00-54.1 1
Trichloroethene ND ug/kg 03/11/15 19:34 79-01-64.1 1
Trichlorofluoromethane ND ug/kg 03/11/15 19:34 75-69-44.1 1
1,2,3-Trichloropropane ND ug/kg 03/11/15 19:34 96-18-44.1 1
1,2,4-Trimethylbenzene ND ug/kg 03/11/15 19:34 95-63-64.1 1
1,3,5-Trimethylbenzene ND ug/kg 03/11/15 19:34 108-67-84.1 1
Vinyl acetate ND ug/kg 03/11/15 19:34 108-05-441.4 1
Vinyl chloride ND ug/kg 03/11/15 19:34 75-01-48.3 1
Xylene (Total)ND ug/kg 03/11/15 19:34 1330-20-78.3 1
m&p-Xylene ND ug/kg 03/11/15 19:34 179601-23-18.3 1
o-Xylene ND ug/kg 03/11/15 19:34 95-47-64.1 1
Surrogates
Toluene-d8 (S)104 %03/11/15 19:34 2037-26-570-130 1
4-Bromofluorobenzene (S)100 %03/11/15 19:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)119 %03/11/15 19:34 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 8.5 %03/11/15 10:180.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-7 Lab ID:92240297002 Collected:03/06/15 12:10 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 03/13/15 16:1603/12/15 10:186.6 1
Surrogates
n-Pentacosane (S)65 %03/13/15 16:16 629-99-203/12/15 10:1841-119 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/11/15 19:53 67-64-11111
Benzene ND ug/kg 03/11/15 19:53 71-43-25.6 1
Bromobenzene ND ug/kg 03/11/15 19:53 108-86-15.6 1
Bromochloromethane ND ug/kg 03/11/15 19:53 74-97-55.6 1
Bromodichloromethane ND ug/kg 03/11/15 19:53 75-27-45.6 1
Bromoform ND ug/kg 03/11/15 19:53 75-25-25.6 1
Bromomethane ND ug/kg 03/11/15 19:53 74-83-911.1 1
2-Butanone (MEK)ND ug/kg 03/11/15 19:53 78-93-3 M11111
n-Butylbenzene ND ug/kg 03/11/15 19:53 104-51-85.6 1
sec-Butylbenzene ND ug/kg 03/11/15 19:53 135-98-85.6 1
tert-Butylbenzene ND ug/kg 03/11/15 19:53 98-06-65.6 1
Carbon tetrachloride ND ug/kg 03/11/15 19:53 56-23-55.6 1
Chlorobenzene ND ug/kg 03/11/15 19:53 108-90-75.6 1
Chloroethane ND ug/kg 03/11/15 19:53 75-00-311.1 1
Chloroform ND ug/kg 03/11/15 19:53 67-66-35.6 1
Chloromethane ND ug/kg 03/11/15 19:53 74-87-311.1 1
2-Chlorotoluene ND ug/kg 03/11/15 19:53 95-49-85.6 1
4-Chlorotoluene ND ug/kg 03/11/15 19:53 106-43-45.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/11/15 19:53 96-12-8 M15.6 1
Dibromochloromethane ND ug/kg 03/11/15 19:53 124-48-15.6 1
1,2-Dibromoethane (EDB)ND ug/kg 03/11/15 19:53 106-93-45.6 1
Dibromomethane ND ug/kg 03/11/15 19:53 74-95-35.6 1
1,2-Dichlorobenzene ND ug/kg 03/11/15 19:53 95-50-15.6 1
1,3-Dichlorobenzene ND ug/kg 03/11/15 19:53 541-73-15.6 1
1,4-Dichlorobenzene ND ug/kg 03/11/15 19:53 106-46-75.6 1
Dichlorodifluoromethane ND ug/kg 03/11/15 19:53 75-71-811.1 1
1,1-Dichloroethane ND ug/kg 03/11/15 19:53 75-34-35.6 1
1,2-Dichloroethane ND ug/kg 03/11/15 19:53 107-06-25.6 1
1,1-Dichloroethene ND ug/kg 03/11/15 19:53 75-35-45.6 1
cis-1,2-Dichloroethene ND ug/kg 03/11/15 19:53 156-59-25.6 1
trans-1,2-Dichloroethene ND ug/kg 03/11/15 19:53 156-60-55.6 1
1,2-Dichloropropane ND ug/kg 03/11/15 19:53 78-87-55.6 1
1,3-Dichloropropane ND ug/kg 03/11/15 19:53 142-28-95.6 1
2,2-Dichloropropane ND ug/kg 03/11/15 19:53 594-20-75.6 1
1,1-Dichloropropene ND ug/kg 03/11/15 19:53 563-58-65.6 1
cis-1,3-Dichloropropene ND ug/kg 03/11/15 19:53 10061-01-55.6 1
trans-1,3-Dichloropropene ND ug/kg 03/11/15 19:53 10061-02-65.6 1
Diisopropyl ether ND ug/kg 03/11/15 19:53 108-20-35.6 1
Ethylbenzene ND ug/kg 03/11/15 19:53 100-41-45.6 1
Hexachloro-1,3-butadiene ND ug/kg 03/11/15 19:53 87-68-3 M15.6 1
2-Hexanone ND ug/kg 03/11/15 19:53 591-78-6 M155.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-7 Lab ID:92240297002 Collected:03/06/15 12:10 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Isopropylbenzene (Cumene)ND ug/kg 03/11/15 19:53 98-82-85.6 1
p-Isopropyltoluene ND ug/kg 03/11/15 19:53 99-87-65.6 1
Methylene Chloride ND ug/kg 03/11/15 19:53 75-09-2 M122.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/11/15 19:53 108-10-1 M155.6 1
Methyl-tert-butyl ether ND ug/kg 03/11/15 19:53 1634-04-45.6 1
Naphthalene ND ug/kg 03/11/15 19:53 91-20-35.6 1
n-Propylbenzene ND ug/kg 03/11/15 19:53 103-65-15.6 1
Styrene ND ug/kg 03/11/15 19:53 100-42-55.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/11/15 19:53 630-20-65.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/11/15 19:53 79-34-5 M15.6 1
Tetrachloroethene ND ug/kg 03/11/15 19:53 127-18-45.6 1
Toluene ND ug/kg 03/11/15 19:53 108-88-35.6 1
1,2,3-Trichlorobenzene ND ug/kg 03/11/15 19:53 87-61-65.6 1
1,2,4-Trichlorobenzene ND ug/kg 03/11/15 19:53 120-82-15.6 1
1,1,1-Trichloroethane ND ug/kg 03/11/15 19:53 71-55-65.6 1
1,1,2-Trichloroethane ND ug/kg 03/11/15 19:53 79-00-55.6 1
Trichloroethene ND ug/kg 03/11/15 19:53 79-01-65.6 1
Trichlorofluoromethane ND ug/kg 03/11/15 19:53 75-69-45.6 1
1,2,3-Trichloropropane ND ug/kg 03/11/15 19:53 96-18-45.6 1
1,2,4-Trimethylbenzene ND ug/kg 03/11/15 19:53 95-63-65.6 1
1,3,5-Trimethylbenzene ND ug/kg 03/11/15 19:53 108-67-85.6 1
Vinyl acetate ND ug/kg 03/11/15 19:53 108-05-4 M155.6 1
Vinyl chloride ND ug/kg 03/11/15 19:53 75-01-411.1 1
Xylene (Total)ND ug/kg 03/11/15 19:53 1330-20-711.1 1
m&p-Xylene ND ug/kg 03/11/15 19:53 179601-23-111.1 1
o-Xylene ND ug/kg 03/11/15 19:53 95-47-65.6 1
Surrogates
Toluene-d8 (S)103 %03/11/15 19:53 2037-26-570-130 1
4-Bromofluorobenzene (S)104 %03/11/15 19:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %03/11/15 19:53 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 23.8 %03/11/15 10:180.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-8 Lab ID:92240297003 Collected:03/06/15 13:15 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)111 mg/kg 03/13/15 16:1603/12/15 10:185.6 1
Surrogates
n-Pentacosane (S)103 %03/13/15 16:16 629-99-203/12/15 10:1841-119 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/11/15 20:13 67-64-184.4 1
Benzene ND ug/kg 03/11/15 20:13 71-43-24.2 1
Bromobenzene ND ug/kg 03/11/15 20:13 108-86-14.2 1
Bromochloromethane ND ug/kg 03/11/15 20:13 74-97-54.2 1
Bromodichloromethane ND ug/kg 03/11/15 20:13 75-27-44.2 1
Bromoform ND ug/kg 03/11/15 20:13 75-25-24.2 1
Bromomethane ND ug/kg 03/11/15 20:13 74-83-98.4 1
2-Butanone (MEK)ND ug/kg 03/11/15 20:13 78-93-384.4 1
n-Butylbenzene ND ug/kg 03/11/15 20:13 104-51-84.2 1
sec-Butylbenzene ND ug/kg 03/11/15 20:13 135-98-84.2 1
tert-Butylbenzene ND ug/kg 03/11/15 20:13 98-06-64.2 1
Carbon tetrachloride ND ug/kg 03/11/15 20:13 56-23-54.2 1
Chlorobenzene ND ug/kg 03/11/15 20:13 108-90-74.2 1
Chloroethane ND ug/kg 03/11/15 20:13 75-00-38.4 1
Chloroform ND ug/kg 03/11/15 20:13 67-66-34.2 1
Chloromethane ND ug/kg 03/11/15 20:13 74-87-38.4 1
2-Chlorotoluene ND ug/kg 03/11/15 20:13 95-49-84.2 1
4-Chlorotoluene ND ug/kg 03/11/15 20:13 106-43-44.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/11/15 20:13 96-12-84.2 1
Dibromochloromethane ND ug/kg 03/11/15 20:13 124-48-14.2 1
1,2-Dibromoethane (EDB)ND ug/kg 03/11/15 20:13 106-93-44.2 1
Dibromomethane ND ug/kg 03/11/15 20:13 74-95-34.2 1
1,2-Dichlorobenzene ND ug/kg 03/11/15 20:13 95-50-14.2 1
1,3-Dichlorobenzene ND ug/kg 03/11/15 20:13 541-73-14.2 1
1,4-Dichlorobenzene ND ug/kg 03/11/15 20:13 106-46-74.2 1
Dichlorodifluoromethane ND ug/kg 03/11/15 20:13 75-71-88.4 1
1,1-Dichloroethane ND ug/kg 03/11/15 20:13 75-34-34.2 1
1,2-Dichloroethane ND ug/kg 03/11/15 20:13 107-06-24.2 1
1,1-Dichloroethene ND ug/kg 03/11/15 20:13 75-35-44.2 1
cis-1,2-Dichloroethene ND ug/kg 03/11/15 20:13 156-59-24.2 1
trans-1,2-Dichloroethene ND ug/kg 03/11/15 20:13 156-60-54.2 1
1,2-Dichloropropane ND ug/kg 03/11/15 20:13 78-87-54.2 1
1,3-Dichloropropane ND ug/kg 03/11/15 20:13 142-28-94.2 1
2,2-Dichloropropane ND ug/kg 03/11/15 20:13 594-20-74.2 1
1,1-Dichloropropene ND ug/kg 03/11/15 20:13 563-58-64.2 1
cis-1,3-Dichloropropene ND ug/kg 03/11/15 20:13 10061-01-54.2 1
trans-1,3-Dichloropropene ND ug/kg 03/11/15 20:13 10061-02-64.2 1
Diisopropyl ether ND ug/kg 03/11/15 20:13 108-20-34.2 1
Ethylbenzene ND ug/kg 03/11/15 20:13 100-41-44.2 1
Hexachloro-1,3-butadiene ND ug/kg 03/11/15 20:13 87-68-34.2 1
2-Hexanone ND ug/kg 03/11/15 20:13 591-78-642.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-8 Lab ID:92240297003 Collected:03/06/15 13:15 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Isopropylbenzene (Cumene)ND ug/kg 03/11/15 20:13 98-82-84.2 1
p-Isopropyltoluene ND ug/kg 03/11/15 20:13 99-87-64.2 1
Methylene Chloride ND ug/kg 03/11/15 20:13 75-09-216.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/11/15 20:13 108-10-142.2 1
Methyl-tert-butyl ether ND ug/kg 03/11/15 20:13 1634-04-44.2 1
Naphthalene ND ug/kg 03/11/15 20:13 91-20-34.2 1
n-Propylbenzene ND ug/kg 03/11/15 20:13 103-65-14.2 1
Styrene ND ug/kg 03/11/15 20:13 100-42-54.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/11/15 20:13 630-20-64.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/11/15 20:13 79-34-54.2 1
Tetrachloroethene ND ug/kg 03/11/15 20:13 127-18-44.2 1
Toluene ND ug/kg 03/11/15 20:13 108-88-34.2 1
1,2,3-Trichlorobenzene ND ug/kg 03/11/15 20:13 87-61-64.2 1
1,2,4-Trichlorobenzene ND ug/kg 03/11/15 20:13 120-82-14.2 1
1,1,1-Trichloroethane ND ug/kg 03/11/15 20:13 71-55-64.2 1
1,1,2-Trichloroethane ND ug/kg 03/11/15 20:13 79-00-54.2 1
Trichloroethene ND ug/kg 03/11/15 20:13 79-01-64.2 1
Trichlorofluoromethane ND ug/kg 03/11/15 20:13 75-69-44.2 1
1,2,3-Trichloropropane ND ug/kg 03/11/15 20:13 96-18-44.2 1
1,2,4-Trimethylbenzene ND ug/kg 03/11/15 20:13 95-63-64.2 1
1,3,5-Trimethylbenzene ND ug/kg 03/11/15 20:13 108-67-84.2 1
Vinyl acetate ND ug/kg 03/11/15 20:13 108-05-442.2 1
Vinyl chloride ND ug/kg 03/11/15 20:13 75-01-48.4 1
Xylene (Total)ND ug/kg 03/11/15 20:13 1330-20-78.4 1
m&p-Xylene ND ug/kg 03/11/15 20:13 179601-23-18.4 1
o-Xylene ND ug/kg 03/11/15 20:13 95-47-64.2 1
Surrogates
Toluene-d8 (S)100 %03/11/15 20:13 2037-26-570-130 1
4-Bromofluorobenzene (S)99 %03/11/15 20:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)123 %03/11/15 20:13 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 11.2 %03/11/15 10:190.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-9 Lab ID:92240297004 Collected:03/06/15 13:25 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 03/13/15 16:4003/12/15 10:185.9 1
Surrogates
n-Pentacosane (S)76 %03/13/15 16:40 629-99-203/12/15 10:1841-119 1
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Arsenic ND mg/kg 03/10/15 23:41 7440-38-203/10/15 16:300.98 1
Barium 75.1 mg/kg 03/10/15 23:41 7440-39-303/10/15 16:300.49 1
Cadmium 0.12 mg/kg 03/10/15 23:41 7440-43-903/10/15 16:300.098 1
Chromium 20.8 mg/kg 03/10/15 23:41 7440-47-303/10/15 16:300.49 1
Lead 7.4 mg/kg 03/10/15 23:41 7439-92-103/10/15 16:300.49 1
Selenium ND mg/kg 03/10/15 23:41 7782-49-203/10/15 16:300.98 1
Silver 2.0 mg/kg 03/10/15 23:41 7440-22-403/10/15 16:300.49 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury ND mg/kg 03/12/15 14:13 7439-97-603/11/15 13:500.0037 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/11/15 20:33 67-64-198.9 1
Benzene ND ug/kg 03/11/15 20:33 71-43-24.9 1
Bromobenzene ND ug/kg 03/11/15 20:33 108-86-14.9 1
Bromochloromethane ND ug/kg 03/11/15 20:33 74-97-54.9 1
Bromodichloromethane ND ug/kg 03/11/15 20:33 75-27-44.9 1
Bromoform ND ug/kg 03/11/15 20:33 75-25-24.9 1
Bromomethane ND ug/kg 03/11/15 20:33 74-83-99.9 1
2-Butanone (MEK)ND ug/kg 03/11/15 20:33 78-93-398.9 1
n-Butylbenzene ND ug/kg 03/11/15 20:33 104-51-84.9 1
sec-Butylbenzene ND ug/kg 03/11/15 20:33 135-98-84.9 1
tert-Butylbenzene ND ug/kg 03/11/15 20:33 98-06-64.9 1
Carbon tetrachloride ND ug/kg 03/11/15 20:33 56-23-54.9 1
Chlorobenzene ND ug/kg 03/11/15 20:33 108-90-74.9 1
Chloroethane ND ug/kg 03/11/15 20:33 75-00-39.9 1
Chloroform ND ug/kg 03/11/15 20:33 67-66-34.9 1
Chloromethane ND ug/kg 03/11/15 20:33 74-87-39.9 1
2-Chlorotoluene ND ug/kg 03/11/15 20:33 95-49-84.9 1
4-Chlorotoluene ND ug/kg 03/11/15 20:33 106-43-44.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/11/15 20:33 96-12-84.9 1
Dibromochloromethane ND ug/kg 03/11/15 20:33 124-48-14.9 1
1,2-Dibromoethane (EDB)ND ug/kg 03/11/15 20:33 106-93-44.9 1
Dibromomethane ND ug/kg 03/11/15 20:33 74-95-34.9 1
1,2-Dichlorobenzene ND ug/kg 03/11/15 20:33 95-50-14.9 1
1,3-Dichlorobenzene ND ug/kg 03/11/15 20:33 541-73-14.9 1
1,4-Dichlorobenzene ND ug/kg 03/11/15 20:33 106-46-74.9 1
Dichlorodifluoromethane ND ug/kg 03/11/15 20:33 75-71-89.9 1
1,1-Dichloroethane ND ug/kg 03/11/15 20:33 75-34-34.9 1
1,2-Dichloroethane ND ug/kg 03/11/15 20:33 107-06-24.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-9 Lab ID:92240297004 Collected:03/06/15 13:25 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
1,1-Dichloroethene ND ug/kg 03/11/15 20:33 75-35-44.9 1
cis-1,2-Dichloroethene ND ug/kg 03/11/15 20:33 156-59-24.9 1
trans-1,2-Dichloroethene ND ug/kg 03/11/15 20:33 156-60-54.9 1
1,2-Dichloropropane ND ug/kg 03/11/15 20:33 78-87-54.9 1
1,3-Dichloropropane ND ug/kg 03/11/15 20:33 142-28-94.9 1
2,2-Dichloropropane ND ug/kg 03/11/15 20:33 594-20-74.9 1
1,1-Dichloropropene ND ug/kg 03/11/15 20:33 563-58-64.9 1
cis-1,3-Dichloropropene ND ug/kg 03/11/15 20:33 10061-01-54.9 1
trans-1,3-Dichloropropene ND ug/kg 03/11/15 20:33 10061-02-64.9 1
Diisopropyl ether ND ug/kg 03/11/15 20:33 108-20-34.9 1
Ethylbenzene ND ug/kg 03/11/15 20:33 100-41-44.9 1
Hexachloro-1,3-butadiene ND ug/kg 03/11/15 20:33 87-68-34.9 1
2-Hexanone ND ug/kg 03/11/15 20:33 591-78-649.5 1
Isopropylbenzene (Cumene)ND ug/kg 03/11/15 20:33 98-82-84.9 1
p-Isopropyltoluene ND ug/kg 03/11/15 20:33 99-87-64.9 1
Methylene Chloride ND ug/kg 03/11/15 20:33 75-09-219.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/11/15 20:33 108-10-149.5 1
Methyl-tert-butyl ether ND ug/kg 03/11/15 20:33 1634-04-44.9 1
Naphthalene ND ug/kg 03/11/15 20:33 91-20-34.9 1
n-Propylbenzene ND ug/kg 03/11/15 20:33 103-65-14.9 1
Styrene ND ug/kg 03/11/15 20:33 100-42-54.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/11/15 20:33 630-20-64.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/11/15 20:33 79-34-54.9 1
Tetrachloroethene ND ug/kg 03/11/15 20:33 127-18-44.9 1
Toluene ND ug/kg 03/11/15 20:33 108-88-34.9 1
1,2,3-Trichlorobenzene ND ug/kg 03/11/15 20:33 87-61-64.9 1
1,2,4-Trichlorobenzene ND ug/kg 03/11/15 20:33 120-82-14.9 1
1,1,1-Trichloroethane ND ug/kg 03/11/15 20:33 71-55-64.9 1
1,1,2-Trichloroethane ND ug/kg 03/11/15 20:33 79-00-54.9 1
Trichloroethene ND ug/kg 03/11/15 20:33 79-01-64.9 1
Trichlorofluoromethane ND ug/kg 03/11/15 20:33 75-69-44.9 1
1,2,3-Trichloropropane ND ug/kg 03/11/15 20:33 96-18-44.9 1
1,2,4-Trimethylbenzene ND ug/kg 03/11/15 20:33 95-63-64.9 1
1,3,5-Trimethylbenzene ND ug/kg 03/11/15 20:33 108-67-84.9 1
Vinyl acetate ND ug/kg 03/11/15 20:33 108-05-449.5 1
Vinyl chloride ND ug/kg 03/11/15 20:33 75-01-49.9 1
Xylene (Total)ND ug/kg 03/11/15 20:33 1330-20-79.9 1
m&p-Xylene ND ug/kg 03/11/15 20:33 179601-23-19.9 1
o-Xylene ND ug/kg 03/11/15 20:33 95-47-64.9 1
Surrogates
Toluene-d8 (S)104 %03/11/15 20:33 2037-26-570-130 1
4-Bromofluorobenzene (S)100 %03/11/15 20:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)121 %03/11/15 20:33 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.6 %03/11/15 10:190.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-10 Lab ID:92240297005 Collected:03/06/15 13:30 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)130 mg/kg 03/13/15 16:4003/12/15 10:185.5 1
Surrogates
n-Pentacosane (S)98 %03/13/15 16:40 629-99-203/12/15 10:1841-119 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/11/15 20:53 67-64-186.7 1
Benzene ND ug/kg 03/11/15 20:53 71-43-24.3 1
Bromobenzene ND ug/kg 03/11/15 20:53 108-86-14.3 1
Bromochloromethane ND ug/kg 03/11/15 20:53 74-97-54.3 1
Bromodichloromethane ND ug/kg 03/11/15 20:53 75-27-44.3 1
Bromoform ND ug/kg 03/11/15 20:53 75-25-24.3 1
Bromomethane ND ug/kg 03/11/15 20:53 74-83-98.7 1
2-Butanone (MEK)ND ug/kg 03/11/15 20:53 78-93-386.7 1
n-Butylbenzene ND ug/kg 03/11/15 20:53 104-51-84.3 1
sec-Butylbenzene ND ug/kg 03/11/15 20:53 135-98-84.3 1
tert-Butylbenzene ND ug/kg 03/11/15 20:53 98-06-64.3 1
Carbon tetrachloride ND ug/kg 03/11/15 20:53 56-23-54.3 1
Chlorobenzene ND ug/kg 03/11/15 20:53 108-90-74.3 1
Chloroethane ND ug/kg 03/11/15 20:53 75-00-38.7 1
Chloroform ND ug/kg 03/11/15 20:53 67-66-34.3 1
Chloromethane ND ug/kg 03/11/15 20:53 74-87-38.7 1
2-Chlorotoluene ND ug/kg 03/11/15 20:53 95-49-84.3 1
4-Chlorotoluene ND ug/kg 03/11/15 20:53 106-43-44.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/11/15 20:53 96-12-84.3 1
Dibromochloromethane ND ug/kg 03/11/15 20:53 124-48-14.3 1
1,2-Dibromoethane (EDB)ND ug/kg 03/11/15 20:53 106-93-44.3 1
Dibromomethane ND ug/kg 03/11/15 20:53 74-95-34.3 1
1,2-Dichlorobenzene ND ug/kg 03/11/15 20:53 95-50-14.3 1
1,3-Dichlorobenzene ND ug/kg 03/11/15 20:53 541-73-14.3 1
1,4-Dichlorobenzene ND ug/kg 03/11/15 20:53 106-46-74.3 1
Dichlorodifluoromethane ND ug/kg 03/11/15 20:53 75-71-88.7 1
1,1-Dichloroethane ND ug/kg 03/11/15 20:53 75-34-34.3 1
1,2-Dichloroethane ND ug/kg 03/11/15 20:53 107-06-24.3 1
1,1-Dichloroethene ND ug/kg 03/11/15 20:53 75-35-44.3 1
cis-1,2-Dichloroethene ND ug/kg 03/11/15 20:53 156-59-24.3 1
trans-1,2-Dichloroethene ND ug/kg 03/11/15 20:53 156-60-54.3 1
1,2-Dichloropropane ND ug/kg 03/11/15 20:53 78-87-54.3 1
1,3-Dichloropropane ND ug/kg 03/11/15 20:53 142-28-94.3 1
2,2-Dichloropropane ND ug/kg 03/11/15 20:53 594-20-74.3 1
1,1-Dichloropropene ND ug/kg 03/11/15 20:53 563-58-64.3 1
cis-1,3-Dichloropropene ND ug/kg 03/11/15 20:53 10061-01-54.3 1
trans-1,3-Dichloropropene ND ug/kg 03/11/15 20:53 10061-02-64.3 1
Diisopropyl ether ND ug/kg 03/11/15 20:53 108-20-34.3 1
Ethylbenzene ND ug/kg 03/11/15 20:53 100-41-44.3 1
Hexachloro-1,3-butadiene ND ug/kg 03/11/15 20:53 87-68-34.3 1
2-Hexanone ND ug/kg 03/11/15 20:53 591-78-643.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-10 Lab ID:92240297005 Collected:03/06/15 13:30 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Isopropylbenzene (Cumene)ND ug/kg 03/11/15 20:53 98-82-84.3 1
p-Isopropyltoluene ND ug/kg 03/11/15 20:53 99-87-64.3 1
Methylene Chloride ND ug/kg 03/11/15 20:53 75-09-217.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/11/15 20:53 108-10-143.3 1
Methyl-tert-butyl ether ND ug/kg 03/11/15 20:53 1634-04-44.3 1
Naphthalene ND ug/kg 03/11/15 20:53 91-20-34.3 1
n-Propylbenzene ND ug/kg 03/11/15 20:53 103-65-14.3 1
Styrene ND ug/kg 03/11/15 20:53 100-42-54.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/11/15 20:53 630-20-64.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/11/15 20:53 79-34-54.3 1
Tetrachloroethene ND ug/kg 03/11/15 20:53 127-18-44.3 1
Toluene ND ug/kg 03/11/15 20:53 108-88-34.3 1
1,2,3-Trichlorobenzene ND ug/kg 03/11/15 20:53 87-61-64.3 1
1,2,4-Trichlorobenzene ND ug/kg 03/11/15 20:53 120-82-14.3 1
1,1,1-Trichloroethane ND ug/kg 03/11/15 20:53 71-55-64.3 1
1,1,2-Trichloroethane ND ug/kg 03/11/15 20:53 79-00-54.3 1
Trichloroethene ND ug/kg 03/11/15 20:53 79-01-64.3 1
Trichlorofluoromethane ND ug/kg 03/11/15 20:53 75-69-44.3 1
1,2,3-Trichloropropane ND ug/kg 03/11/15 20:53 96-18-44.3 1
1,2,4-Trimethylbenzene ND ug/kg 03/11/15 20:53 95-63-64.3 1
1,3,5-Trimethylbenzene ND ug/kg 03/11/15 20:53 108-67-84.3 1
Vinyl acetate ND ug/kg 03/11/15 20:53 108-05-443.3 1
Vinyl chloride ND ug/kg 03/11/15 20:53 75-01-48.7 1
Xylene (Total)ND ug/kg 03/11/15 20:53 1330-20-78.7 1
m&p-Xylene ND ug/kg 03/11/15 20:53 179601-23-18.7 1
o-Xylene ND ug/kg 03/11/15 20:53 95-47-64.3 1
Surrogates
Toluene-d8 (S)106 %03/11/15 20:53 2037-26-570-130 1
4-Bromofluorobenzene (S)104 %03/11/15 20:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %03/11/15 20:53 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 9.9 %03/11/15 10:230.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-11 Lab ID:92240297006 Collected:03/06/15 13:40 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)165 mg/kg 03/13/15 17:0303/12/15 10:185.5 1
Surrogates
n-Pentacosane (S)101 %03/13/15 17:03 629-99-203/12/15 10:1841-119 1
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Arsenic ND mg/kg 03/13/15 00:50 7440-38-203/12/15 16:550.85 1
Barium 72.4 mg/kg 03/13/15 00:50 7440-39-303/12/15 16:550.42 1
Cadmium ND mg/kg 03/13/15 00:50 7440-43-903/12/15 16:550.085 1
Chromium 10.4 mg/kg 03/13/15 00:50 7440-47-303/12/15 16:550.42 1
Lead 4.2 mg/kg 03/13/15 00:50 7439-92-103/12/15 16:550.42 1
Selenium ND mg/kg 03/13/15 00:50 7782-49-203/12/15 16:550.85 1
Silver 0.62 mg/kg 03/13/15 00:50 7440-22-403/12/15 16:550.42 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury ND mg/kg 03/14/15 16:09 7439-97-603/12/15 18:300.0041 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/11/15 21:13 67-64-180.9 1
Benzene ND ug/kg 03/11/15 21:13 71-43-24.0 1
Bromobenzene ND ug/kg 03/11/15 21:13 108-86-14.0 1
Bromochloromethane ND ug/kg 03/11/15 21:13 74-97-54.0 1
Bromodichloromethane ND ug/kg 03/11/15 21:13 75-27-44.0 1
Bromoform ND ug/kg 03/11/15 21:13 75-25-24.0 1
Bromomethane ND ug/kg 03/11/15 21:13 74-83-98.1 1
2-Butanone (MEK)ND ug/kg 03/11/15 21:13 78-93-380.9 1
n-Butylbenzene ND ug/kg 03/11/15 21:13 104-51-84.0 1
sec-Butylbenzene ND ug/kg 03/11/15 21:13 135-98-84.0 1
tert-Butylbenzene ND ug/kg 03/11/15 21:13 98-06-64.0 1
Carbon tetrachloride ND ug/kg 03/11/15 21:13 56-23-54.0 1
Chlorobenzene ND ug/kg 03/11/15 21:13 108-90-74.0 1
Chloroethane ND ug/kg 03/11/15 21:13 75-00-38.1 1
Chloroform ND ug/kg 03/11/15 21:13 67-66-34.0 1
Chloromethane ND ug/kg 03/11/15 21:13 74-87-38.1 1
2-Chlorotoluene ND ug/kg 03/11/15 21:13 95-49-84.0 1
4-Chlorotoluene ND ug/kg 03/11/15 21:13 106-43-44.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/11/15 21:13 96-12-84.0 1
Dibromochloromethane ND ug/kg 03/11/15 21:13 124-48-14.0 1
1,2-Dibromoethane (EDB)ND ug/kg 03/11/15 21:13 106-93-44.0 1
Dibromomethane ND ug/kg 03/11/15 21:13 74-95-34.0 1
1,2-Dichlorobenzene ND ug/kg 03/11/15 21:13 95-50-14.0 1
1,3-Dichlorobenzene ND ug/kg 03/11/15 21:13 541-73-14.0 1
1,4-Dichlorobenzene ND ug/kg 03/11/15 21:13 106-46-74.0 1
Dichlorodifluoromethane ND ug/kg 03/11/15 21:13 75-71-88.1 1
1,1-Dichloroethane ND ug/kg 03/11/15 21:13 75-34-34.0 1
1,2-Dichloroethane ND ug/kg 03/11/15 21:13 107-06-24.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-11 Lab ID:92240297006 Collected:03/06/15 13:40 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
1,1-Dichloroethene ND ug/kg 03/11/15 21:13 75-35-44.0 1
cis-1,2-Dichloroethene ND ug/kg 03/11/15 21:13 156-59-24.0 1
trans-1,2-Dichloroethene ND ug/kg 03/11/15 21:13 156-60-54.0 1
1,2-Dichloropropane ND ug/kg 03/11/15 21:13 78-87-54.0 1
1,3-Dichloropropane ND ug/kg 03/11/15 21:13 142-28-94.0 1
2,2-Dichloropropane ND ug/kg 03/11/15 21:13 594-20-74.0 1
1,1-Dichloropropene ND ug/kg 03/11/15 21:13 563-58-64.0 1
cis-1,3-Dichloropropene ND ug/kg 03/11/15 21:13 10061-01-54.0 1
trans-1,3-Dichloropropene ND ug/kg 03/11/15 21:13 10061-02-64.0 1
Diisopropyl ether ND ug/kg 03/11/15 21:13 108-20-34.0 1
Ethylbenzene ND ug/kg 03/11/15 21:13 100-41-44.0 1
Hexachloro-1,3-butadiene ND ug/kg 03/11/15 21:13 87-68-34.0 1
2-Hexanone ND ug/kg 03/11/15 21:13 591-78-640.5 1
Isopropylbenzene (Cumene)ND ug/kg 03/11/15 21:13 98-82-84.0 1
p-Isopropyltoluene ND ug/kg 03/11/15 21:13 99-87-64.0 1
Methylene Chloride ND ug/kg 03/11/15 21:13 75-09-216.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/11/15 21:13 108-10-140.5 1
Methyl-tert-butyl ether ND ug/kg 03/11/15 21:13 1634-04-44.0 1
Naphthalene ND ug/kg 03/11/15 21:13 91-20-34.0 1
n-Propylbenzene ND ug/kg 03/11/15 21:13 103-65-14.0 1
Styrene ND ug/kg 03/11/15 21:13 100-42-54.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/11/15 21:13 630-20-64.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/11/15 21:13 79-34-54.0 1
Tetrachloroethene ND ug/kg 03/11/15 21:13 127-18-44.0 1
Toluene ND ug/kg 03/11/15 21:13 108-88-34.0 1
1,2,3-Trichlorobenzene ND ug/kg 03/11/15 21:13 87-61-64.0 1
1,2,4-Trichlorobenzene ND ug/kg 03/11/15 21:13 120-82-14.0 1
1,1,1-Trichloroethane ND ug/kg 03/11/15 21:13 71-55-64.0 1
1,1,2-Trichloroethane ND ug/kg 03/11/15 21:13 79-00-54.0 1
Trichloroethene ND ug/kg 03/11/15 21:13 79-01-64.0 1
Trichlorofluoromethane ND ug/kg 03/11/15 21:13 75-69-44.0 1
1,2,3-Trichloropropane ND ug/kg 03/11/15 21:13 96-18-44.0 1
1,2,4-Trimethylbenzene ND ug/kg 03/11/15 21:13 95-63-64.0 1
1,3,5-Trimethylbenzene ND ug/kg 03/11/15 21:13 108-67-84.0 1
Vinyl acetate ND ug/kg 03/11/15 21:13 108-05-440.5 1
Vinyl chloride ND ug/kg 03/11/15 21:13 75-01-48.1 1
Xylene (Total)ND ug/kg 03/11/15 21:13 1330-20-78.1 1
m&p-Xylene ND ug/kg 03/11/15 21:13 179601-23-18.1 1
o-Xylene ND ug/kg 03/11/15 21:13 95-47-64.0 1
Surrogates
Toluene-d8 (S)104 %03/11/15 21:13 2037-26-570-130 1
4-Bromofluorobenzene (S)99 %03/11/15 21:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %03/11/15 21:13 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 9.4 %03/11/15 10:240.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-12 Lab ID:92240297007 Collected:03/06/15 13:50 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)83.0 mg/kg 03/13/15 17:0303/12/15 10:185.7 1
Surrogates
n-Pentacosane (S)88 %03/13/15 17:03 629-99-203/12/15 10:1841-119 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/11/15 21:32 67-64-193.1 1
Benzene ND ug/kg 03/11/15 21:32 71-43-24.7 1
Bromobenzene ND ug/kg 03/11/15 21:32 108-86-14.7 1
Bromochloromethane ND ug/kg 03/11/15 21:32 74-97-54.7 1
Bromodichloromethane ND ug/kg 03/11/15 21:32 75-27-44.7 1
Bromoform ND ug/kg 03/11/15 21:32 75-25-24.7 1
Bromomethane ND ug/kg 03/11/15 21:32 74-83-99.3 1
2-Butanone (MEK)ND ug/kg 03/11/15 21:32 78-93-393.1 1
n-Butylbenzene ND ug/kg 03/11/15 21:32 104-51-84.7 1
sec-Butylbenzene ND ug/kg 03/11/15 21:32 135-98-84.7 1
tert-Butylbenzene ND ug/kg 03/11/15 21:32 98-06-64.7 1
Carbon tetrachloride ND ug/kg 03/11/15 21:32 56-23-54.7 1
Chlorobenzene ND ug/kg 03/11/15 21:32 108-90-74.7 1
Chloroethane ND ug/kg 03/11/15 21:32 75-00-39.3 1
Chloroform ND ug/kg 03/11/15 21:32 67-66-34.7 1
Chloromethane ND ug/kg 03/11/15 21:32 74-87-39.3 1
2-Chlorotoluene ND ug/kg 03/11/15 21:32 95-49-84.7 1
4-Chlorotoluene ND ug/kg 03/11/15 21:32 106-43-44.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/11/15 21:32 96-12-84.7 1
Dibromochloromethane ND ug/kg 03/11/15 21:32 124-48-14.7 1
1,2-Dibromoethane (EDB)ND ug/kg 03/11/15 21:32 106-93-44.7 1
Dibromomethane ND ug/kg 03/11/15 21:32 74-95-34.7 1
1,2-Dichlorobenzene ND ug/kg 03/11/15 21:32 95-50-14.7 1
1,3-Dichlorobenzene ND ug/kg 03/11/15 21:32 541-73-14.7 1
1,4-Dichlorobenzene ND ug/kg 03/11/15 21:32 106-46-74.7 1
Dichlorodifluoromethane ND ug/kg 03/11/15 21:32 75-71-89.3 1
1,1-Dichloroethane ND ug/kg 03/11/15 21:32 75-34-34.7 1
1,2-Dichloroethane ND ug/kg 03/11/15 21:32 107-06-24.7 1
1,1-Dichloroethene ND ug/kg 03/11/15 21:32 75-35-44.7 1
cis-1,2-Dichloroethene ND ug/kg 03/11/15 21:32 156-59-24.7 1
trans-1,2-Dichloroethene ND ug/kg 03/11/15 21:32 156-60-54.7 1
1,2-Dichloropropane ND ug/kg 03/11/15 21:32 78-87-54.7 1
1,3-Dichloropropane ND ug/kg 03/11/15 21:32 142-28-94.7 1
2,2-Dichloropropane ND ug/kg 03/11/15 21:32 594-20-74.7 1
1,1-Dichloropropene ND ug/kg 03/11/15 21:32 563-58-64.7 1
cis-1,3-Dichloropropene ND ug/kg 03/11/15 21:32 10061-01-54.7 1
trans-1,3-Dichloropropene ND ug/kg 03/11/15 21:32 10061-02-64.7 1
Diisopropyl ether ND ug/kg 03/11/15 21:32 108-20-34.7 1
Ethylbenzene ND ug/kg 03/11/15 21:32 100-41-44.7 1
Hexachloro-1,3-butadiene ND ug/kg 03/11/15 21:32 87-68-34.7 1
2-Hexanone ND ug/kg 03/11/15 21:32 591-78-646.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-12 Lab ID:92240297007 Collected:03/06/15 13:50 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Isopropylbenzene (Cumene)ND ug/kg 03/11/15 21:32 98-82-84.7 1
p-Isopropyltoluene ND ug/kg 03/11/15 21:32 99-87-64.7 1
Methylene Chloride ND ug/kg 03/11/15 21:32 75-09-218.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/11/15 21:32 108-10-146.6 1
Methyl-tert-butyl ether ND ug/kg 03/11/15 21:32 1634-04-44.7 1
Naphthalene ND ug/kg 03/11/15 21:32 91-20-34.7 1
n-Propylbenzene ND ug/kg 03/11/15 21:32 103-65-14.7 1
Styrene ND ug/kg 03/11/15 21:32 100-42-54.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/11/15 21:32 630-20-64.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/11/15 21:32 79-34-54.7 1
Tetrachloroethene ND ug/kg 03/11/15 21:32 127-18-44.7 1
Toluene ND ug/kg 03/11/15 21:32 108-88-34.7 1
1,2,3-Trichlorobenzene ND ug/kg 03/11/15 21:32 87-61-64.7 1
1,2,4-Trichlorobenzene ND ug/kg 03/11/15 21:32 120-82-14.7 1
1,1,1-Trichloroethane ND ug/kg 03/11/15 21:32 71-55-64.7 1
1,1,2-Trichloroethane ND ug/kg 03/11/15 21:32 79-00-54.7 1
Trichloroethene ND ug/kg 03/11/15 21:32 79-01-64.7 1
Trichlorofluoromethane ND ug/kg 03/11/15 21:32 75-69-44.7 1
1,2,3-Trichloropropane ND ug/kg 03/11/15 21:32 96-18-44.7 1
1,2,4-Trimethylbenzene ND ug/kg 03/11/15 21:32 95-63-64.7 1
1,3,5-Trimethylbenzene ND ug/kg 03/11/15 21:32 108-67-84.7 1
Vinyl acetate ND ug/kg 03/11/15 21:32 108-05-446.6 1
Vinyl chloride ND ug/kg 03/11/15 21:32 75-01-49.3 1
Xylene (Total)ND ug/kg 03/11/15 21:32 1330-20-79.3 1
m&p-Xylene ND ug/kg 03/11/15 21:32 179601-23-19.3 1
o-Xylene ND ug/kg 03/11/15 21:32 95-47-64.7 1
Surrogates
Toluene-d8 (S)104 %03/11/15 21:32 2037-26-570-130 1
4-Bromofluorobenzene (S)100 %03/11/15 21:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %03/11/15 21:32 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 11.8 %03/11/15 10:240.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-13 Lab ID:92240297008 Collected:03/06/15 14:20 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)24.2 mg/kg 03/13/15 17:2703/12/15 10:186.7 1
Surrogates
n-Pentacosane (S)68 %03/13/15 17:27 629-99-203/12/15 10:1841-119 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/12/15 16:35 67-64-11201
Benzene ND ug/kg 03/12/15 16:35 71-43-26.0 1
Bromobenzene ND ug/kg 03/12/15 16:35 108-86-16.0 1
Bromochloromethane ND ug/kg 03/12/15 16:35 74-97-56.0 1
Bromodichloromethane ND ug/kg 03/12/15 16:35 75-27-46.0 1
Bromoform ND ug/kg 03/12/15 16:35 75-25-26.0 1
Bromomethane ND ug/kg 03/12/15 16:35 74-83-912.0 1
2-Butanone (MEK)ND ug/kg 03/12/15 16:35 78-93-31201
n-Butylbenzene ND ug/kg 03/12/15 16:35 104-51-86.0 1
sec-Butylbenzene ND ug/kg 03/12/15 16:35 135-98-86.0 1
tert-Butylbenzene ND ug/kg 03/12/15 16:35 98-06-66.0 1
Carbon tetrachloride ND ug/kg 03/12/15 16:35 56-23-56.0 1
Chlorobenzene ND ug/kg 03/12/15 16:35 108-90-76.0 1
Chloroethane ND ug/kg 03/12/15 16:35 75-00-312.0 1
Chloroform ND ug/kg 03/12/15 16:35 67-66-36.0 1
Chloromethane ND ug/kg 03/12/15 16:35 74-87-312.0 1
2-Chlorotoluene ND ug/kg 03/12/15 16:35 95-49-86.0 1
4-Chlorotoluene ND ug/kg 03/12/15 16:35 106-43-46.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/12/15 16:35 96-12-86.0 1
Dibromochloromethane ND ug/kg 03/12/15 16:35 124-48-16.0 1
1,2-Dibromoethane (EDB)ND ug/kg 03/12/15 16:35 106-93-46.0 1
Dibromomethane ND ug/kg 03/12/15 16:35 74-95-36.0 1
1,2-Dichlorobenzene ND ug/kg 03/12/15 16:35 95-50-16.0 1
1,3-Dichlorobenzene ND ug/kg 03/12/15 16:35 541-73-16.0 1
1,4-Dichlorobenzene ND ug/kg 03/12/15 16:35 106-46-76.0 1
Dichlorodifluoromethane ND ug/kg 03/12/15 16:35 75-71-812.0 1
1,1-Dichloroethane ND ug/kg 03/12/15 16:35 75-34-36.0 1
1,2-Dichloroethane ND ug/kg 03/12/15 16:35 107-06-26.0 1
1,1-Dichloroethene ND ug/kg 03/12/15 16:35 75-35-46.0 1
cis-1,2-Dichloroethene ND ug/kg 03/12/15 16:35 156-59-26.0 1
trans-1,2-Dichloroethene ND ug/kg 03/12/15 16:35 156-60-56.0 1
1,2-Dichloropropane ND ug/kg 03/12/15 16:35 78-87-56.0 1
1,3-Dichloropropane ND ug/kg 03/12/15 16:35 142-28-96.0 1
2,2-Dichloropropane ND ug/kg 03/12/15 16:35 594-20-76.0 1
1,1-Dichloropropene ND ug/kg 03/12/15 16:35 563-58-66.0 1
cis-1,3-Dichloropropene ND ug/kg 03/12/15 16:35 10061-01-56.0 1
trans-1,3-Dichloropropene ND ug/kg 03/12/15 16:35 10061-02-66.0 1
Diisopropyl ether ND ug/kg 03/12/15 16:35 108-20-36.0 1
Ethylbenzene ND ug/kg 03/12/15 16:35 100-41-46.0 1
Hexachloro-1,3-butadiene ND ug/kg 03/12/15 16:35 87-68-36.0 1
2-Hexanone ND ug/kg 03/12/15 16:35 591-78-659.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-13 Lab ID:92240297008 Collected:03/06/15 14:20 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Isopropylbenzene (Cumene)ND ug/kg 03/12/15 16:35 98-82-86.0 1
p-Isopropyltoluene ND ug/kg 03/12/15 16:35 99-87-66.0 1
Methylene Chloride ND ug/kg 03/12/15 16:35 75-09-223.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/12/15 16:35 108-10-159.8 1
Methyl-tert-butyl ether ND ug/kg 03/12/15 16:35 1634-04-46.0 1
Naphthalene ND ug/kg 03/12/15 16:35 91-20-36.0 1
n-Propylbenzene ND ug/kg 03/12/15 16:35 103-65-16.0 1
Styrene ND ug/kg 03/12/15 16:35 100-42-56.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/12/15 16:35 630-20-66.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/12/15 16:35 79-34-56.0 1
Tetrachloroethene ND ug/kg 03/12/15 16:35 127-18-46.0 1
Toluene ND ug/kg 03/12/15 16:35 108-88-36.0 1
1,2,3-Trichlorobenzene ND ug/kg 03/12/15 16:35 87-61-66.0 1
1,2,4-Trichlorobenzene ND ug/kg 03/12/15 16:35 120-82-16.0 1
1,1,1-Trichloroethane ND ug/kg 03/12/15 16:35 71-55-66.0 1
1,1,2-Trichloroethane ND ug/kg 03/12/15 16:35 79-00-56.0 1
Trichloroethene ND ug/kg 03/12/15 16:35 79-01-66.0 1
Trichlorofluoromethane ND ug/kg 03/12/15 16:35 75-69-46.0 1
1,2,3-Trichloropropane ND ug/kg 03/12/15 16:35 96-18-46.0 1
1,2,4-Trimethylbenzene ND ug/kg 03/12/15 16:35 95-63-66.0 1
1,3,5-Trimethylbenzene ND ug/kg 03/12/15 16:35 108-67-86.0 1
Vinyl acetate ND ug/kg 03/12/15 16:35 108-05-459.8 1
Vinyl chloride ND ug/kg 03/12/15 16:35 75-01-412.0 1
Xylene (Total)ND ug/kg 03/12/15 16:35 1330-20-712.0 1
m&p-Xylene ND ug/kg 03/12/15 16:35 179601-23-112.0 1
o-Xylene ND ug/kg 03/12/15 16:35 95-47-66.0 1
Surrogates
Toluene-d8 (S)104 %03/12/15 16:35 2037-26-570-130 1
4-Bromofluorobenzene (S)100 %03/12/15 16:35 460-00-470-130 1
1,2-Dichloroethane-d4 (S)118 %03/12/15 16:35 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 25.7 %03/11/15 10:240.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-14 Lab ID:92240297009 Collected:03/06/15 14:30 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 03/13/15 17:2703/12/15 10:186.0 1
Surrogates
n-Pentacosane (S)72 %03/13/15 17:27 629-99-203/12/15 10:1841-119 1
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Arsenic ND mg/kg 03/13/15 00:53 7440-38-203/12/15 16:550.94 1
Barium 47.4 mg/kg 03/13/15 00:53 7440-39-303/12/15 16:550.47 1
Cadmium ND mg/kg 03/13/15 00:53 7440-43-903/12/15 16:550.094 1
Chromium 4.0 mg/kg 03/13/15 00:53 7440-47-303/12/15 16:550.47 1
Lead 10.3 mg/kg 03/13/15 00:53 7439-92-103/12/15 16:550.47 1
Selenium ND mg/kg 03/13/15 00:53 7782-49-203/12/15 16:550.94 1
Silver ND mg/kg 03/13/15 00:53 7440-22-403/12/15 16:550.47 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury ND mg/kg 03/14/15 16:12 7439-97-603/12/15 18:300.0042 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/12/15 16:55 67-64-187.3 1
Benzene ND ug/kg 03/12/15 16:55 71-43-24.4 1
Bromobenzene ND ug/kg 03/12/15 16:55 108-86-14.4 1
Bromochloromethane ND ug/kg 03/12/15 16:55 74-97-54.4 1
Bromodichloromethane ND ug/kg 03/12/15 16:55 75-27-44.4 1
Bromoform ND ug/kg 03/12/15 16:55 75-25-24.4 1
Bromomethane ND ug/kg 03/12/15 16:55 74-83-98.7 1
2-Butanone (MEK)ND ug/kg 03/12/15 16:55 78-93-387.3 1
n-Butylbenzene ND ug/kg 03/12/15 16:55 104-51-84.4 1
sec-Butylbenzene ND ug/kg 03/12/15 16:55 135-98-84.4 1
tert-Butylbenzene ND ug/kg 03/12/15 16:55 98-06-64.4 1
Carbon tetrachloride ND ug/kg 03/12/15 16:55 56-23-54.4 1
Chlorobenzene ND ug/kg 03/12/15 16:55 108-90-74.4 1
Chloroethane ND ug/kg 03/12/15 16:55 75-00-38.7 1
Chloroform ND ug/kg 03/12/15 16:55 67-66-34.4 1
Chloromethane ND ug/kg 03/12/15 16:55 74-87-38.7 1
2-Chlorotoluene ND ug/kg 03/12/15 16:55 95-49-84.4 1
4-Chlorotoluene ND ug/kg 03/12/15 16:55 106-43-44.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/12/15 16:55 96-12-84.4 1
Dibromochloromethane ND ug/kg 03/12/15 16:55 124-48-14.4 1
1,2-Dibromoethane (EDB)ND ug/kg 03/12/15 16:55 106-93-44.4 1
Dibromomethane ND ug/kg 03/12/15 16:55 74-95-34.4 1
1,2-Dichlorobenzene ND ug/kg 03/12/15 16:55 95-50-14.4 1
1,3-Dichlorobenzene ND ug/kg 03/12/15 16:55 541-73-14.4 1
1,4-Dichlorobenzene ND ug/kg 03/12/15 16:55 106-46-74.4 1
Dichlorodifluoromethane ND ug/kg 03/12/15 16:55 75-71-88.7 1
1,1-Dichloroethane ND ug/kg 03/12/15 16:55 75-34-34.4 1
1,2-Dichloroethane ND ug/kg 03/12/15 16:55 107-06-24.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-14 Lab ID:92240297009 Collected:03/06/15 14:30 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
1,1-Dichloroethene ND ug/kg 03/12/15 16:55 75-35-44.4 1
cis-1,2-Dichloroethene ND ug/kg 03/12/15 16:55 156-59-24.4 1
trans-1,2-Dichloroethene ND ug/kg 03/12/15 16:55 156-60-54.4 1
1,2-Dichloropropane ND ug/kg 03/12/15 16:55 78-87-54.4 1
1,3-Dichloropropane ND ug/kg 03/12/15 16:55 142-28-94.4 1
2,2-Dichloropropane ND ug/kg 03/12/15 16:55 594-20-74.4 1
1,1-Dichloropropene ND ug/kg 03/12/15 16:55 563-58-64.4 1
cis-1,3-Dichloropropene ND ug/kg 03/12/15 16:55 10061-01-54.4 1
trans-1,3-Dichloropropene ND ug/kg 03/12/15 16:55 10061-02-64.4 1
Diisopropyl ether ND ug/kg 03/12/15 16:55 108-20-34.4 1
Ethylbenzene ND ug/kg 03/12/15 16:55 100-41-44.4 1
Hexachloro-1,3-butadiene ND ug/kg 03/12/15 16:55 87-68-34.4 1
2-Hexanone ND ug/kg 03/12/15 16:55 591-78-643.6 1
Isopropylbenzene (Cumene)ND ug/kg 03/12/15 16:55 98-82-84.4 1
p-Isopropyltoluene ND ug/kg 03/12/15 16:55 99-87-64.4 1
Methylene Chloride ND ug/kg 03/12/15 16:55 75-09-217.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/12/15 16:55 108-10-143.6 1
Methyl-tert-butyl ether ND ug/kg 03/12/15 16:55 1634-04-44.4 1
Naphthalene ND ug/kg 03/12/15 16:55 91-20-34.4 1
n-Propylbenzene ND ug/kg 03/12/15 16:55 103-65-14.4 1
Styrene ND ug/kg 03/12/15 16:55 100-42-54.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/12/15 16:55 630-20-64.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/12/15 16:55 79-34-54.4 1
Tetrachloroethene ND ug/kg 03/12/15 16:55 127-18-44.4 1
Toluene ND ug/kg 03/12/15 16:55 108-88-34.4 1
1,2,3-Trichlorobenzene ND ug/kg 03/12/15 16:55 87-61-64.4 1
1,2,4-Trichlorobenzene ND ug/kg 03/12/15 16:55 120-82-14.4 1
1,1,1-Trichloroethane ND ug/kg 03/12/15 16:55 71-55-64.4 1
1,1,2-Trichloroethane ND ug/kg 03/12/15 16:55 79-00-54.4 1
Trichloroethene ND ug/kg 03/12/15 16:55 79-01-64.4 1
Trichlorofluoromethane ND ug/kg 03/12/15 16:55 75-69-44.4 1
1,2,3-Trichloropropane ND ug/kg 03/12/15 16:55 96-18-44.4 1
1,2,4-Trimethylbenzene ND ug/kg 03/12/15 16:55 95-63-64.4 1
1,3,5-Trimethylbenzene ND ug/kg 03/12/15 16:55 108-67-84.4 1
Vinyl acetate ND ug/kg 03/12/15 16:55 108-05-443.6 1
Vinyl chloride ND ug/kg 03/12/15 16:55 75-01-48.7 1
Xylene (Total)ND ug/kg 03/12/15 16:55 1330-20-78.7 1
m&p-Xylene ND ug/kg 03/12/15 16:55 179601-23-18.7 1
o-Xylene ND ug/kg 03/12/15 16:55 95-47-64.4 1
Surrogates
Toluene-d8 (S)103 %03/12/15 16:55 2037-26-570-130 1
4-Bromofluorobenzene (S)100 %03/12/15 16:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)113 %03/12/15 16:55 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.9 %03/11/15 10:240.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-15 Lab ID:92240297010 Collected:03/06/15 14:40 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 03/13/15 17:5103/12/15 10:185.9 1
Surrogates
n-Pentacosane (S)77 %03/13/15 17:51 629-99-203/12/15 10:1841-119 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/12/15 17:15 67-64-183.3 1
Benzene ND ug/kg 03/12/15 17:15 71-43-24.2 1
Bromobenzene ND ug/kg 03/12/15 17:15 108-86-14.2 1
Bromochloromethane ND ug/kg 03/12/15 17:15 74-97-54.2 1
Bromodichloromethane ND ug/kg 03/12/15 17:15 75-27-44.2 1
Bromoform ND ug/kg 03/12/15 17:15 75-25-24.2 1
Bromomethane ND ug/kg 03/12/15 17:15 74-83-98.3 1
2-Butanone (MEK)ND ug/kg 03/12/15 17:15 78-93-383.3 1
n-Butylbenzene ND ug/kg 03/12/15 17:15 104-51-84.2 1
sec-Butylbenzene ND ug/kg 03/12/15 17:15 135-98-84.2 1
tert-Butylbenzene ND ug/kg 03/12/15 17:15 98-06-64.2 1
Carbon tetrachloride ND ug/kg 03/12/15 17:15 56-23-54.2 1
Chlorobenzene ND ug/kg 03/12/15 17:15 108-90-74.2 1
Chloroethane ND ug/kg 03/12/15 17:15 75-00-38.3 1
Chloroform ND ug/kg 03/12/15 17:15 67-66-34.2 1
Chloromethane ND ug/kg 03/12/15 17:15 74-87-38.3 1
2-Chlorotoluene ND ug/kg 03/12/15 17:15 95-49-84.2 1
4-Chlorotoluene ND ug/kg 03/12/15 17:15 106-43-44.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/12/15 17:15 96-12-84.2 1
Dibromochloromethane ND ug/kg 03/12/15 17:15 124-48-14.2 1
1,2-Dibromoethane (EDB)ND ug/kg 03/12/15 17:15 106-93-44.2 1
Dibromomethane ND ug/kg 03/12/15 17:15 74-95-34.2 1
1,2-Dichlorobenzene ND ug/kg 03/12/15 17:15 95-50-14.2 1
1,3-Dichlorobenzene ND ug/kg 03/12/15 17:15 541-73-14.2 1
1,4-Dichlorobenzene ND ug/kg 03/12/15 17:15 106-46-74.2 1
Dichlorodifluoromethane ND ug/kg 03/12/15 17:15 75-71-88.3 1
1,1-Dichloroethane ND ug/kg 03/12/15 17:15 75-34-34.2 1
1,2-Dichloroethane ND ug/kg 03/12/15 17:15 107-06-24.2 1
1,1-Dichloroethene ND ug/kg 03/12/15 17:15 75-35-44.2 1
cis-1,2-Dichloroethene ND ug/kg 03/12/15 17:15 156-59-24.2 1
trans-1,2-Dichloroethene ND ug/kg 03/12/15 17:15 156-60-54.2 1
1,2-Dichloropropane ND ug/kg 03/12/15 17:15 78-87-54.2 1
1,3-Dichloropropane ND ug/kg 03/12/15 17:15 142-28-94.2 1
2,2-Dichloropropane ND ug/kg 03/12/15 17:15 594-20-74.2 1
1,1-Dichloropropene ND ug/kg 03/12/15 17:15 563-58-64.2 1
cis-1,3-Dichloropropene ND ug/kg 03/12/15 17:15 10061-01-54.2 1
trans-1,3-Dichloropropene ND ug/kg 03/12/15 17:15 10061-02-64.2 1
Diisopropyl ether ND ug/kg 03/12/15 17:15 108-20-34.2 1
Ethylbenzene ND ug/kg 03/12/15 17:15 100-41-44.2 1
Hexachloro-1,3-butadiene ND ug/kg 03/12/15 17:15 87-68-34.2 1
2-Hexanone ND ug/kg 03/12/15 17:15 591-78-641.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:SS-15 Lab ID:92240297010 Collected:03/06/15 14:40 Received:03/09/15 15:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Isopropylbenzene (Cumene)ND ug/kg 03/12/15 17:15 98-82-84.2 1
p-Isopropyltoluene ND ug/kg 03/12/15 17:15 99-87-64.2 1
Methylene Chloride ND ug/kg 03/12/15 17:15 75-09-216.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/12/15 17:15 108-10-141.6 1
Methyl-tert-butyl ether ND ug/kg 03/12/15 17:15 1634-04-44.2 1
Naphthalene ND ug/kg 03/12/15 17:15 91-20-34.2 1
n-Propylbenzene ND ug/kg 03/12/15 17:15 103-65-14.2 1
Styrene ND ug/kg 03/12/15 17:15 100-42-54.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/12/15 17:15 630-20-64.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/12/15 17:15 79-34-54.2 1
Tetrachloroethene ND ug/kg 03/12/15 17:15 127-18-44.2 1
Toluene ND ug/kg 03/12/15 17:15 108-88-34.2 1
1,2,3-Trichlorobenzene ND ug/kg 03/12/15 17:15 87-61-64.2 1
1,2,4-Trichlorobenzene ND ug/kg 03/12/15 17:15 120-82-14.2 1
1,1,1-Trichloroethane ND ug/kg 03/12/15 17:15 71-55-64.2 1
1,1,2-Trichloroethane ND ug/kg 03/12/15 17:15 79-00-54.2 1
Trichloroethene ND ug/kg 03/12/15 17:15 79-01-64.2 1
Trichlorofluoromethane ND ug/kg 03/12/15 17:15 75-69-44.2 1
1,2,3-Trichloropropane ND ug/kg 03/12/15 17:15 96-18-44.2 1
1,2,4-Trimethylbenzene ND ug/kg 03/12/15 17:15 95-63-64.2 1
1,3,5-Trimethylbenzene ND ug/kg 03/12/15 17:15 108-67-84.2 1
Vinyl acetate ND ug/kg 03/12/15 17:15 108-05-441.6 1
Vinyl chloride ND ug/kg 03/12/15 17:15 75-01-48.3 1
Xylene (Total)ND ug/kg 03/12/15 17:15 1330-20-78.3 1
m&p-Xylene ND ug/kg 03/12/15 17:15 179601-23-18.3 1
o-Xylene ND ug/kg 03/12/15 17:15 95-47-64.2 1
Surrogates
Toluene-d8 (S)104 %03/12/15 17:15 2037-26-570-130 1
4-Bromofluorobenzene (S)103 %03/12/15 17:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %03/12/15 17:15 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.4 %03/11/15 10:240.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:TMW-2 Lab ID:92240297011 Collected:03/06/15 09:05 Received:03/09/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 03/12/15 12:40 83-32-903/10/15 08:1510.0 1
Acenaphthylene ND ug/L 03/12/15 12:40 208-96-803/10/15 08:1510.0 1
Aniline ND ug/L 03/12/15 12:40 62-53-303/10/15 08:1510.0 1
Anthracene ND ug/L 03/12/15 12:40 120-12-703/10/15 08:1510.0 1
Benzo(a)anthracene ND ug/L 03/12/15 12:40 56-55-303/10/15 08:1510.0 1
Benzo(a)pyrene ND ug/L 03/12/15 12:40 50-32-803/10/15 08:1510.0 1
Benzo(b)fluoranthene ND ug/L 03/12/15 12:40 205-99-203/10/15 08:1510.0 1
Benzo(g,h,i)perylene ND ug/L 03/12/15 12:40 191-24-203/10/15 08:1510.0 1
Benzo(k)fluoranthene ND ug/L 03/12/15 12:40 207-08-903/10/15 08:1510.0 1
Benzoic Acid ND ug/L 03/12/15 12:40 65-85-003/10/15 08:1550.0 1
Benzyl alcohol ND ug/L 03/12/15 12:40 100-51-603/10/15 08:1520.0 1
4-Bromophenylphenyl ether ND ug/L 03/12/15 12:40 101-55-303/10/15 08:1510.0 1
Butylbenzylphthalate ND ug/L 03/12/15 12:40 85-68-703/10/15 08:1510.0 1
4-Chloro-3-methylphenol ND ug/L 03/12/15 12:40 59-50-703/10/15 08:1520.0 1
4-Chloroaniline ND ug/L 03/12/15 12:40 106-47-803/10/15 08:1520.0 1
bis(2-Chloroethoxy)methane ND ug/L 03/12/15 12:40 111-91-103/10/15 08:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 03/12/15 12:40 111-44-403/10/15 08:1510.0 1
bis(2-Chloroisopropyl) ether ND ug/L 03/12/15 12:40 108-60-103/10/15 08:1510.0 1
2-Chloronaphthalene ND ug/L 03/12/15 12:40 91-58-703/10/15 08:1510.0 1
2-Chlorophenol ND ug/L 03/12/15 12:40 95-57-803/10/15 08:1510.0 1
4-Chlorophenylphenyl ether ND ug/L 03/12/15 12:40 7005-72-303/10/15 08:1510.0 1
Chrysene ND ug/L 03/12/15 12:40 218-01-903/10/15 08:1510.0 1
Dibenz(a,h)anthracene ND ug/L 03/12/15 12:40 53-70-303/10/15 08:1510.0 1
Dibenzofuran ND ug/L 03/12/15 12:40 132-64-903/10/15 08:1510.0 1
1,2-Dichlorobenzene ND ug/L 03/12/15 12:40 95-50-103/10/15 08:1510.0 1
1,3-Dichlorobenzene ND ug/L 03/12/15 12:40 541-73-103/10/15 08:1510.0 1
1,4-Dichlorobenzene ND ug/L 03/12/15 12:40 106-46-703/10/15 08:1510.0 1
3,3'-Dichlorobenzidine ND ug/L 03/12/15 12:40 91-94-103/10/15 08:1520.0 1
2,4-Dichlorophenol ND ug/L 03/12/15 12:40 120-83-203/10/15 08:1510.0 1
Diethylphthalate ND ug/L 03/12/15 12:40 84-66-203/10/15 08:1510.0 1
2,4-Dimethylphenol ND ug/L 03/12/15 12:40 105-67-903/10/15 08:1510.0 1
Dimethylphthalate ND ug/L 03/12/15 12:40 131-11-303/10/15 08:1510.0 1
Di-n-butylphthalate ND ug/L 03/12/15 12:40 84-74-203/10/15 08:1510.0 1
4,6-Dinitro-2-methylphenol ND ug/L 03/12/15 12:40 534-52-103/10/15 08:1520.0 1
2,4-Dinitrophenol ND ug/L 03/12/15 12:40 51-28-503/10/15 08:1550.0 1
2,4-Dinitrotoluene ND ug/L 03/12/15 12:40 121-14-203/10/15 08:1510.0 1
2,6-Dinitrotoluene ND ug/L 03/12/15 12:40 606-20-203/10/15 08:1510.0 1
Di-n-octylphthalate ND ug/L 03/12/15 12:40 117-84-003/10/15 08:1510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/12/15 12:40 117-81-703/10/15 08:156.0 1
Fluoranthene ND ug/L 03/12/15 12:40 206-44-003/10/15 08:1510.0 1
Fluorene ND ug/L 03/12/15 12:40 86-73-703/10/15 08:1510.0 1
Hexachloro-1,3-butadiene ND ug/L 03/12/15 12:40 87-68-303/10/15 08:1510.0 1
Hexachlorobenzene ND ug/L 03/12/15 12:40 118-74-103/10/15 08:1510.0 1
Hexachlorocyclopentadiene ND ug/L 03/12/15 12:40 77-47-403/10/15 08:1510.0 1
Hexachloroethane ND ug/L 03/12/15 12:40 67-72-103/10/15 08:1510.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/12/15 12:40 193-39-503/10/15 08:1510.0 1
Isophorone ND ug/L 03/12/15 12:40 78-59-103/10/15 08:1510.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:TMW-2 Lab ID:92240297011 Collected:03/06/15 09:05 Received:03/09/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 03/12/15 12:40 90-12-003/10/15 08:1510.0 1
2-Methylnaphthalene ND ug/L 03/12/15 12:40 91-57-603/10/15 08:1510.0 1
2-Methylphenol(o-Cresol)ND ug/L 03/12/15 12:40 95-48-703/10/15 08:1510.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/12/15 12:4003/10/15 08:1510.0 1
Naphthalene ND ug/L 03/12/15 12:40 91-20-303/10/15 08:1510.0 1
2-Nitroaniline ND ug/L 03/12/15 12:40 88-74-403/10/15 08:1550.0 1
3-Nitroaniline ND ug/L 03/12/15 12:40 99-09-203/10/15 08:1550.0 1
4-Nitroaniline ND ug/L 03/12/15 12:40 100-01-603/10/15 08:1520.0 1
Nitrobenzene ND ug/L 03/12/15 12:40 98-95-303/10/15 08:1510.0 1
2-Nitrophenol ND ug/L 03/12/15 12:40 88-75-503/10/15 08:1510.0 1
4-Nitrophenol ND ug/L 03/12/15 12:40 100-02-703/10/15 08:1550.0 1
N-Nitrosodimethylamine ND ug/L 03/12/15 12:40 62-75-903/10/15 08:1510.0 1
N-Nitroso-di-n-propylamine ND ug/L 03/12/15 12:40 621-64-703/10/15 08:1510.0 1
N-Nitrosodiphenylamine ND ug/L 03/12/15 12:40 86-30-603/10/15 08:1510.0 1
Pentachlorophenol ND ug/L 03/12/15 12:40 87-86-503/10/15 08:1525.0 1
Phenanthrene ND ug/L 03/12/15 12:40 85-01-803/10/15 08:1510.0 1
Phenol ND ug/L 03/12/15 12:40 108-95-203/10/15 08:1510.0 1
Pyrene ND ug/L 03/12/15 12:40 129-00-003/10/15 08:1510.0 1
1,2,4-Trichlorobenzene ND ug/L 03/12/15 12:40 120-82-103/10/15 08:1510.0 1
2,4,5-Trichlorophenol ND ug/L 03/12/15 12:40 95-95-403/10/15 08:1510.0 1
2,4,6-Trichlorophenol ND ug/L 03/12/15 12:40 88-06-203/10/15 08:1510.0 1
Surrogates
Nitrobenzene-d5 (S)69 %03/12/15 12:40 4165-60-003/10/15 08:1521-110 1
2-Fluorobiphenyl (S)80 %03/12/15 12:40 321-60-803/10/15 08:1527-110 1
Terphenyl-d14 (S)76 %03/12/15 12:40 1718-51-003/10/15 08:1531-107 1
Phenol-d6 (S)36 %03/12/15 12:40 13127-88-303/10/15 08:1510-110 1
2-Fluorophenol (S)46 %03/12/15 12:40 367-12-403/10/15 08:1512-110 1
2,4,6-Tribromophenol (S)83 %03/12/15 12:40 118-79-603/10/15 08:1527-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/11/15 21:50 67-64-125.0 1
Benzene ND ug/L 03/11/15 21:50 71-43-21.0 1
Bromobenzene ND ug/L 03/11/15 21:50 108-86-11.0 1
Bromochloromethane ND ug/L 03/11/15 21:50 74-97-51.0 1
Bromodichloromethane ND ug/L 03/11/15 21:50 75-27-41.0 1
Bromoform ND ug/L 03/11/15 21:50 75-25-21.0 1
Bromomethane ND ug/L 03/11/15 21:50 74-83-92.0 1
2-Butanone (MEK)ND ug/L 03/11/15 21:50 78-93-35.0 1
Carbon tetrachloride ND ug/L 03/11/15 21:50 56-23-51.0 1
Chlorobenzene ND ug/L 03/11/15 21:50 108-90-71.0 1
Chloroethane ND ug/L 03/11/15 21:50 75-00-31.0 1
Chloroform ND ug/L 03/11/15 21:50 67-66-31.0 1
Chloromethane ND ug/L 03/11/15 21:50 74-87-31.0 1
2-Chlorotoluene ND ug/L 03/11/15 21:50 95-49-81.0 1
4-Chlorotoluene ND ug/L 03/11/15 21:50 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 03/11/15 21:50 96-12-82.0 1
Dibromochloromethane ND ug/L 03/11/15 21:50 124-48-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:TMW-2 Lab ID:92240297011 Collected:03/06/15 09:05 Received:03/09/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 03/11/15 21:50 106-93-41.0 1
Dibromomethane ND ug/L 03/11/15 21:50 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 03/11/15 21:50 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 03/11/15 21:50 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 03/11/15 21:50 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 03/11/15 21:50 75-71-81.0 1
1,1-Dichloroethane ND ug/L 03/11/15 21:50 75-34-31.0 1
1,2-Dichloroethane ND ug/L 03/11/15 21:50 107-06-21.0 1
1,1-Dichloroethene ND ug/L 03/11/15 21:50 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 03/11/15 21:50 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 03/11/15 21:50 156-60-51.0 1
1,2-Dichloropropane ND ug/L 03/11/15 21:50 78-87-51.0 1
1,3-Dichloropropane ND ug/L 03/11/15 21:50 142-28-91.0 1
2,2-Dichloropropane ND ug/L 03/11/15 21:50 594-20-71.0 1
1,1-Dichloropropene ND ug/L 03/11/15 21:50 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 03/11/15 21:50 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 03/11/15 21:50 10061-02-61.0 1
Diisopropyl ether ND ug/L 03/11/15 21:50 108-20-31.0 1
Ethylbenzene ND ug/L 03/11/15 21:50 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 03/11/15 21:50 87-68-31.0 1
2-Hexanone ND ug/L 03/11/15 21:50 591-78-65.0 1
p-Isopropyltoluene ND ug/L 03/11/15 21:50 99-87-61.0 1
Methylene Chloride ND ug/L 03/11/15 21:50 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/11/15 21:50 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 03/11/15 21:50 1634-04-41.0 1
Naphthalene ND ug/L 03/11/15 21:50 91-20-31.0 1
Styrene ND ug/L 03/11/15 21:50 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 03/11/15 21:50 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 03/11/15 21:50 79-34-51.0 1
Tetrachloroethene ND ug/L 03/11/15 21:50 127-18-41.0 1
Toluene ND ug/L 03/11/15 21:50 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 03/11/15 21:50 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 03/11/15 21:50 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 03/11/15 21:50 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 03/11/15 21:50 79-00-51.0 1
Trichloroethene ND ug/L 03/11/15 21:50 79-01-61.0 1
Trichlorofluoromethane ND ug/L 03/11/15 21:50 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 03/11/15 21:50 96-18-41.0 1
Vinyl acetate ND ug/L 03/11/15 21:50 108-05-42.0 1
Vinyl chloride ND ug/L 03/11/15 21:50 75-01-41.0 1
Xylene (Total)ND ug/L 03/11/15 21:50 1330-20-72.0 1
m&p-Xylene ND ug/L 03/11/15 21:50 179601-23-12.0 1
o-Xylene ND ug/L 03/11/15 21:50 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %03/11/15 21:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %03/11/15 21:50 17060-07-070-130 1
Toluene-d8 (S)98 %03/11/15 21:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:TMW-3 Lab ID:92240297012 Collected:03/06/15 11:10 Received:03/09/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 03/12/15 13:07 83-32-903/10/15 08:1510.0 1
Acenaphthylene ND ug/L 03/12/15 13:07 208-96-803/10/15 08:1510.0 1
Aniline ND ug/L 03/12/15 13:07 62-53-303/10/15 08:1510.0 1
Anthracene ND ug/L 03/12/15 13:07 120-12-703/10/15 08:1510.0 1
Benzo(a)anthracene ND ug/L 03/12/15 13:07 56-55-303/10/15 08:1510.0 1
Benzo(a)pyrene ND ug/L 03/12/15 13:07 50-32-803/10/15 08:1510.0 1
Benzo(b)fluoranthene ND ug/L 03/12/15 13:07 205-99-203/10/15 08:1510.0 1
Benzo(g,h,i)perylene ND ug/L 03/12/15 13:07 191-24-203/10/15 08:1510.0 1
Benzo(k)fluoranthene ND ug/L 03/12/15 13:07 207-08-903/10/15 08:1510.0 1
Benzoic Acid ND ug/L 03/12/15 13:07 65-85-003/10/15 08:1550.0 1
Benzyl alcohol ND ug/L 03/12/15 13:07 100-51-603/10/15 08:1520.0 1
4-Bromophenylphenyl ether ND ug/L 03/12/15 13:07 101-55-303/10/15 08:1510.0 1
Butylbenzylphthalate ND ug/L 03/12/15 13:07 85-68-703/10/15 08:1510.0 1
4-Chloro-3-methylphenol ND ug/L 03/12/15 13:07 59-50-703/10/15 08:1520.0 1
4-Chloroaniline ND ug/L 03/12/15 13:07 106-47-803/10/15 08:1520.0 1
bis(2-Chloroethoxy)methane ND ug/L 03/12/15 13:07 111-91-103/10/15 08:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 03/12/15 13:07 111-44-403/10/15 08:1510.0 1
bis(2-Chloroisopropyl) ether ND ug/L 03/12/15 13:07 108-60-103/10/15 08:1510.0 1
2-Chloronaphthalene ND ug/L 03/12/15 13:07 91-58-703/10/15 08:1510.0 1
2-Chlorophenol ND ug/L 03/12/15 13:07 95-57-803/10/15 08:1510.0 1
4-Chlorophenylphenyl ether ND ug/L 03/12/15 13:07 7005-72-303/10/15 08:1510.0 1
Chrysene ND ug/L 03/12/15 13:07 218-01-903/10/15 08:1510.0 1
Dibenz(a,h)anthracene ND ug/L 03/12/15 13:07 53-70-303/10/15 08:1510.0 1
Dibenzofuran ND ug/L 03/12/15 13:07 132-64-903/10/15 08:1510.0 1
1,2-Dichlorobenzene ND ug/L 03/12/15 13:07 95-50-103/10/15 08:1510.0 1
1,3-Dichlorobenzene ND ug/L 03/12/15 13:07 541-73-103/10/15 08:1510.0 1
1,4-Dichlorobenzene ND ug/L 03/12/15 13:07 106-46-703/10/15 08:1510.0 1
3,3'-Dichlorobenzidine ND ug/L 03/12/15 13:07 91-94-103/10/15 08:1520.0 1
2,4-Dichlorophenol ND ug/L 03/12/15 13:07 120-83-203/10/15 08:1510.0 1
Diethylphthalate ND ug/L 03/12/15 13:07 84-66-203/10/15 08:1510.0 1
2,4-Dimethylphenol ND ug/L 03/12/15 13:07 105-67-903/10/15 08:1510.0 1
Dimethylphthalate ND ug/L 03/12/15 13:07 131-11-303/10/15 08:1510.0 1
Di-n-butylphthalate ND ug/L 03/12/15 13:07 84-74-203/10/15 08:1510.0 1
4,6-Dinitro-2-methylphenol ND ug/L 03/12/15 13:07 534-52-103/10/15 08:1520.0 1
2,4-Dinitrophenol ND ug/L 03/12/15 13:07 51-28-503/10/15 08:1550.0 1
2,4-Dinitrotoluene ND ug/L 03/12/15 13:07 121-14-203/10/15 08:1510.0 1
2,6-Dinitrotoluene ND ug/L 03/12/15 13:07 606-20-203/10/15 08:1510.0 1
Di-n-octylphthalate ND ug/L 03/12/15 13:07 117-84-003/10/15 08:1510.0 1
bis(2-Ethylhexyl)phthalate 7.3 ug/L 03/12/15 13:07 117-81-703/10/15 08:156.0 1
Fluoranthene ND ug/L 03/12/15 13:07 206-44-003/10/15 08:1510.0 1
Fluorene ND ug/L 03/12/15 13:07 86-73-703/10/15 08:1510.0 1
Hexachloro-1,3-butadiene ND ug/L 03/12/15 13:07 87-68-303/10/15 08:1510.0 1
Hexachlorobenzene ND ug/L 03/12/15 13:07 118-74-103/10/15 08:1510.0 1
Hexachlorocyclopentadiene ND ug/L 03/12/15 13:07 77-47-403/10/15 08:1510.0 1
Hexachloroethane ND ug/L 03/12/15 13:07 67-72-103/10/15 08:1510.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/12/15 13:07 193-39-503/10/15 08:1510.0 1
Isophorone ND ug/L 03/12/15 13:07 78-59-103/10/15 08:1510.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:TMW-3 Lab ID:92240297012 Collected:03/06/15 11:10 Received:03/09/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 03/12/15 13:07 90-12-003/10/15 08:1510.0 1
2-Methylnaphthalene ND ug/L 03/12/15 13:07 91-57-603/10/15 08:1510.0 1
2-Methylphenol(o-Cresol)ND ug/L 03/12/15 13:07 95-48-703/10/15 08:1510.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/12/15 13:0703/10/15 08:1510.0 1
Naphthalene ND ug/L 03/12/15 13:07 91-20-303/10/15 08:1510.0 1
2-Nitroaniline ND ug/L 03/12/15 13:07 88-74-403/10/15 08:1550.0 1
3-Nitroaniline ND ug/L 03/12/15 13:07 99-09-203/10/15 08:1550.0 1
4-Nitroaniline ND ug/L 03/12/15 13:07 100-01-603/10/15 08:1520.0 1
Nitrobenzene ND ug/L 03/12/15 13:07 98-95-303/10/15 08:1510.0 1
2-Nitrophenol ND ug/L 03/12/15 13:07 88-75-503/10/15 08:1510.0 1
4-Nitrophenol ND ug/L 03/12/15 13:07 100-02-703/10/15 08:1550.0 1
N-Nitrosodimethylamine ND ug/L 03/12/15 13:07 62-75-903/10/15 08:1510.0 1
N-Nitroso-di-n-propylamine ND ug/L 03/12/15 13:07 621-64-703/10/15 08:1510.0 1
N-Nitrosodiphenylamine ND ug/L 03/12/15 13:07 86-30-603/10/15 08:1510.0 1
Pentachlorophenol ND ug/L 03/12/15 13:07 87-86-503/10/15 08:1525.0 1
Phenanthrene ND ug/L 03/12/15 13:07 85-01-803/10/15 08:1510.0 1
Phenol ND ug/L 03/12/15 13:07 108-95-203/10/15 08:1510.0 1
Pyrene ND ug/L 03/12/15 13:07 129-00-003/10/15 08:1510.0 1
1,2,4-Trichlorobenzene ND ug/L 03/12/15 13:07 120-82-103/10/15 08:1510.0 1
2,4,5-Trichlorophenol ND ug/L 03/12/15 13:07 95-95-403/10/15 08:1510.0 1
2,4,6-Trichlorophenol ND ug/L 03/12/15 13:07 88-06-203/10/15 08:1510.0 1
Surrogates
Nitrobenzene-d5 (S)78 %03/12/15 13:07 4165-60-003/10/15 08:1521-110 1
2-Fluorobiphenyl (S)83 %03/12/15 13:07 321-60-803/10/15 08:1527-110 1
Terphenyl-d14 (S)92 %03/12/15 13:07 1718-51-003/10/15 08:1531-107 1
Phenol-d6 (S)44 %03/12/15 13:07 13127-88-303/10/15 08:1510-110 1
2-Fluorophenol (S)52 %03/12/15 13:07 367-12-403/10/15 08:1512-110 1
2,4,6-Tribromophenol (S)94 %03/12/15 13:07 118-79-603/10/15 08:1527-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/11/15 19:02 67-64-125.0 1
Benzene ND ug/L 03/11/15 19:02 71-43-21.0 1
Bromobenzene ND ug/L 03/11/15 19:02 108-86-11.0 1
Bromochloromethane ND ug/L 03/11/15 19:02 74-97-51.0 1
Bromodichloromethane ND ug/L 03/11/15 19:02 75-27-41.0 1
Bromoform ND ug/L 03/11/15 19:02 75-25-21.0 1
Bromomethane ND ug/L 03/11/15 19:02 74-83-92.0 1
2-Butanone (MEK)ND ug/L 03/11/15 19:02 78-93-35.0 1
Carbon tetrachloride ND ug/L 03/11/15 19:02 56-23-51.0 1
Chlorobenzene ND ug/L 03/11/15 19:02 108-90-71.0 1
Chloroethane ND ug/L 03/11/15 19:02 75-00-31.0 1
Chloroform ND ug/L 03/11/15 19:02 67-66-31.0 1
Chloromethane ND ug/L 03/11/15 19:02 74-87-31.0 1
2-Chlorotoluene ND ug/L 03/11/15 19:02 95-49-81.0 1
4-Chlorotoluene ND ug/L 03/11/15 19:02 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 03/11/15 19:02 96-12-82.0 1
Dibromochloromethane ND ug/L 03/11/15 19:02 124-48-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:TMW-3 Lab ID:92240297012 Collected:03/06/15 11:10 Received:03/09/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 03/11/15 19:02 106-93-41.0 1
Dibromomethane ND ug/L 03/11/15 19:02 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 03/11/15 19:02 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 03/11/15 19:02 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 03/11/15 19:02 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 03/11/15 19:02 75-71-81.0 1
1,1-Dichloroethane ND ug/L 03/11/15 19:02 75-34-31.0 1
1,2-Dichloroethane ND ug/L 03/11/15 19:02 107-06-21.0 1
1,1-Dichloroethene ND ug/L 03/11/15 19:02 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 03/11/15 19:02 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 03/11/15 19:02 156-60-51.0 1
1,2-Dichloropropane ND ug/L 03/11/15 19:02 78-87-51.0 1
1,3-Dichloropropane ND ug/L 03/11/15 19:02 142-28-91.0 1
2,2-Dichloropropane ND ug/L 03/11/15 19:02 594-20-71.0 1
1,1-Dichloropropene ND ug/L 03/11/15 19:02 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 03/11/15 19:02 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 03/11/15 19:02 10061-02-61.0 1
Diisopropyl ether ND ug/L 03/11/15 19:02 108-20-31.0 1
Ethylbenzene ND ug/L 03/11/15 19:02 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 03/11/15 19:02 87-68-31.0 1
2-Hexanone ND ug/L 03/11/15 19:02 591-78-65.0 1
p-Isopropyltoluene ND ug/L 03/11/15 19:02 99-87-61.0 1
Methylene Chloride ND ug/L 03/11/15 19:02 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/11/15 19:02 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 03/11/15 19:02 1634-04-41.0 1
Naphthalene ND ug/L 03/11/15 19:02 91-20-31.0 1
Styrene ND ug/L 03/11/15 19:02 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 03/11/15 19:02 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 03/11/15 19:02 79-34-51.0 1
Tetrachloroethene ND ug/L 03/11/15 19:02 127-18-41.0 1
Toluene ND ug/L 03/11/15 19:02 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 03/11/15 19:02 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 03/11/15 19:02 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 03/11/15 19:02 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 03/11/15 19:02 79-00-51.0 1
Trichloroethene ND ug/L 03/11/15 19:02 79-01-61.0 1
Trichlorofluoromethane ND ug/L 03/11/15 19:02 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 03/11/15 19:02 96-18-41.0 1
Vinyl acetate ND ug/L 03/11/15 19:02 108-05-42.0 1
Vinyl chloride ND ug/L 03/11/15 19:02 75-01-41.0 1
Xylene (Total)ND ug/L 03/11/15 19:02 1330-20-72.0 1
m&p-Xylene ND ug/L 03/11/15 19:02 179601-23-12.0 1
o-Xylene ND ug/L 03/11/15 19:02 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %03/11/15 19:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %03/11/15 19:02 17060-07-070-130 1
Toluene-d8 (S)98 %03/11/15 19:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:TMW-4 Lab ID:92240297013 Collected:03/06/15 16:05 Received:03/09/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 03/12/15 13:34 83-32-903/10/15 08:1510.0 1
Acenaphthylene ND ug/L 03/12/15 13:34 208-96-803/10/15 08:1510.0 1
Aniline ND ug/L 03/12/15 13:34 62-53-303/10/15 08:1510.0 1
Anthracene ND ug/L 03/12/15 13:34 120-12-703/10/15 08:1510.0 1
Benzo(a)anthracene ND ug/L 03/12/15 13:34 56-55-303/10/15 08:1510.0 1
Benzo(a)pyrene ND ug/L 03/12/15 13:34 50-32-803/10/15 08:1510.0 1
Benzo(b)fluoranthene ND ug/L 03/12/15 13:34 205-99-203/10/15 08:1510.0 1
Benzo(g,h,i)perylene ND ug/L 03/12/15 13:34 191-24-203/10/15 08:1510.0 1
Benzo(k)fluoranthene ND ug/L 03/12/15 13:34 207-08-903/10/15 08:1510.0 1
Benzoic Acid ND ug/L 03/12/15 13:34 65-85-003/10/15 08:1550.0 1
Benzyl alcohol ND ug/L 03/12/15 13:34 100-51-603/10/15 08:1520.0 1
4-Bromophenylphenyl ether ND ug/L 03/12/15 13:34 101-55-303/10/15 08:1510.0 1
Butylbenzylphthalate ND ug/L 03/12/15 13:34 85-68-703/10/15 08:1510.0 1
4-Chloro-3-methylphenol ND ug/L 03/12/15 13:34 59-50-703/10/15 08:1520.0 1
4-Chloroaniline ND ug/L 03/12/15 13:34 106-47-803/10/15 08:1520.0 1
bis(2-Chloroethoxy)methane ND ug/L 03/12/15 13:34 111-91-103/10/15 08:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 03/12/15 13:34 111-44-403/10/15 08:1510.0 1
bis(2-Chloroisopropyl) ether ND ug/L 03/12/15 13:34 108-60-103/10/15 08:1510.0 1
2-Chloronaphthalene ND ug/L 03/12/15 13:34 91-58-703/10/15 08:1510.0 1
2-Chlorophenol ND ug/L 03/12/15 13:34 95-57-803/10/15 08:1510.0 1
4-Chlorophenylphenyl ether ND ug/L 03/12/15 13:34 7005-72-303/10/15 08:1510.0 1
Chrysene ND ug/L 03/12/15 13:34 218-01-903/10/15 08:1510.0 1
Dibenz(a,h)anthracene ND ug/L 03/12/15 13:34 53-70-303/10/15 08:1510.0 1
Dibenzofuran ND ug/L 03/12/15 13:34 132-64-903/10/15 08:1510.0 1
1,2-Dichlorobenzene ND ug/L 03/12/15 13:34 95-50-103/10/15 08:1510.0 1
1,3-Dichlorobenzene ND ug/L 03/12/15 13:34 541-73-103/10/15 08:1510.0 1
1,4-Dichlorobenzene ND ug/L 03/12/15 13:34 106-46-703/10/15 08:1510.0 1
3,3'-Dichlorobenzidine ND ug/L 03/12/15 13:34 91-94-103/10/15 08:1520.0 1
2,4-Dichlorophenol ND ug/L 03/12/15 13:34 120-83-203/10/15 08:1510.0 1
Diethylphthalate ND ug/L 03/12/15 13:34 84-66-203/10/15 08:1510.0 1
2,4-Dimethylphenol ND ug/L 03/12/15 13:34 105-67-903/10/15 08:1510.0 1
Dimethylphthalate ND ug/L 03/12/15 13:34 131-11-303/10/15 08:1510.0 1
Di-n-butylphthalate ND ug/L 03/12/15 13:34 84-74-203/10/15 08:1510.0 1
4,6-Dinitro-2-methylphenol ND ug/L 03/12/15 13:34 534-52-103/10/15 08:1520.0 1
2,4-Dinitrophenol ND ug/L 03/12/15 13:34 51-28-503/10/15 08:1550.0 1
2,4-Dinitrotoluene ND ug/L 03/12/15 13:34 121-14-203/10/15 08:1510.0 1
2,6-Dinitrotoluene ND ug/L 03/12/15 13:34 606-20-203/10/15 08:1510.0 1
Di-n-octylphthalate ND ug/L 03/12/15 13:34 117-84-003/10/15 08:1510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/12/15 13:34 117-81-703/10/15 08:156.0 1
Fluoranthene ND ug/L 03/12/15 13:34 206-44-003/10/15 08:1510.0 1
Fluorene ND ug/L 03/12/15 13:34 86-73-703/10/15 08:1510.0 1
Hexachloro-1,3-butadiene ND ug/L 03/12/15 13:34 87-68-303/10/15 08:1510.0 1
Hexachlorobenzene ND ug/L 03/12/15 13:34 118-74-103/10/15 08:1510.0 1
Hexachlorocyclopentadiene ND ug/L 03/12/15 13:34 77-47-403/10/15 08:1510.0 1
Hexachloroethane ND ug/L 03/12/15 13:34 67-72-103/10/15 08:1510.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/12/15 13:34 193-39-503/10/15 08:1510.0 1
Isophorone ND ug/L 03/12/15 13:34 78-59-103/10/15 08:1510.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:TMW-4 Lab ID:92240297013 Collected:03/06/15 16:05 Received:03/09/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 03/12/15 13:34 90-12-003/10/15 08:1510.0 1
2-Methylnaphthalene ND ug/L 03/12/15 13:34 91-57-603/10/15 08:1510.0 1
2-Methylphenol(o-Cresol)ND ug/L 03/12/15 13:34 95-48-703/10/15 08:1510.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/12/15 13:3403/10/15 08:1510.0 1
Naphthalene ND ug/L 03/12/15 13:34 91-20-303/10/15 08:1510.0 1
2-Nitroaniline ND ug/L 03/12/15 13:34 88-74-403/10/15 08:1550.0 1
3-Nitroaniline ND ug/L 03/12/15 13:34 99-09-203/10/15 08:1550.0 1
4-Nitroaniline ND ug/L 03/12/15 13:34 100-01-603/10/15 08:1520.0 1
Nitrobenzene ND ug/L 03/12/15 13:34 98-95-303/10/15 08:1510.0 1
2-Nitrophenol ND ug/L 03/12/15 13:34 88-75-503/10/15 08:1510.0 1
4-Nitrophenol ND ug/L 03/12/15 13:34 100-02-703/10/15 08:1550.0 1
N-Nitrosodimethylamine ND ug/L 03/12/15 13:34 62-75-903/10/15 08:1510.0 1
N-Nitroso-di-n-propylamine ND ug/L 03/12/15 13:34 621-64-703/10/15 08:1510.0 1
N-Nitrosodiphenylamine ND ug/L 03/12/15 13:34 86-30-603/10/15 08:1510.0 1
Pentachlorophenol ND ug/L 03/12/15 13:34 87-86-503/10/15 08:1525.0 1
Phenanthrene ND ug/L 03/12/15 13:34 85-01-803/10/15 08:1510.0 1
Phenol ND ug/L 03/12/15 13:34 108-95-203/10/15 08:1510.0 1
Pyrene ND ug/L 03/12/15 13:34 129-00-003/10/15 08:1510.0 1
1,2,4-Trichlorobenzene ND ug/L 03/12/15 13:34 120-82-103/10/15 08:1510.0 1
2,4,5-Trichlorophenol ND ug/L 03/12/15 13:34 95-95-403/10/15 08:1510.0 1
2,4,6-Trichlorophenol ND ug/L 03/12/15 13:34 88-06-203/10/15 08:1510.0 1
Surrogates
Nitrobenzene-d5 (S)71 %03/12/15 13:34 4165-60-003/10/15 08:1521-110 1
2-Fluorobiphenyl (S)68 %03/12/15 13:34 321-60-803/10/15 08:1527-110 1
Terphenyl-d14 (S)86 %03/12/15 13:34 1718-51-003/10/15 08:1531-107 1
Phenol-d6 (S)37 %03/12/15 13:34 13127-88-303/10/15 08:1510-110 1
2-Fluorophenol (S)47 %03/12/15 13:34 367-12-403/10/15 08:1512-110 1
2,4,6-Tribromophenol (S)92 %03/12/15 13:34 118-79-603/10/15 08:1527-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone 281 ug/L 03/11/15 22:07 67-64-125.0 1
Benzene 2.0 ug/L 03/11/15 22:07 71-43-21.0 1
Bromobenzene ND ug/L 03/11/15 22:07 108-86-11.0 1
Bromochloromethane ND ug/L 03/11/15 22:07 74-97-51.0 1
Bromodichloromethane ND ug/L 03/11/15 22:07 75-27-41.0 1
Bromoform ND ug/L 03/11/15 22:07 75-25-21.0 1
Bromomethane ND ug/L 03/11/15 22:07 74-83-92.0 1
2-Butanone (MEK)9.1 ug/L 03/11/15 22:07 78-93-35.0 1
Carbon tetrachloride ND ug/L 03/11/15 22:07 56-23-51.0 1
Chlorobenzene ND ug/L 03/11/15 22:07 108-90-71.0 1
Chloroethane ND ug/L 03/11/15 22:07 75-00-31.0 1
Chloroform ND ug/L 03/11/15 22:07 67-66-31.0 1
Chloromethane ND ug/L 03/11/15 22:07 74-87-31.0 1
2-Chlorotoluene ND ug/L 03/11/15 22:07 95-49-81.0 1
4-Chlorotoluene ND ug/L 03/11/15 22:07 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 03/11/15 22:07 96-12-82.0 1
Dibromochloromethane ND ug/L 03/11/15 22:07 124-48-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:TMW-4 Lab ID:92240297013 Collected:03/06/15 16:05 Received:03/09/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 03/11/15 22:07 106-93-41.0 1
Dibromomethane ND ug/L 03/11/15 22:07 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 03/11/15 22:07 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 03/11/15 22:07 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 03/11/15 22:07 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 03/11/15 22:07 75-71-81.0 1
1,1-Dichloroethane ND ug/L 03/11/15 22:07 75-34-31.0 1
1,2-Dichloroethane ND ug/L 03/11/15 22:07 107-06-21.0 1
1,1-Dichloroethene ND ug/L 03/11/15 22:07 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 03/11/15 22:07 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 03/11/15 22:07 156-60-51.0 1
1,2-Dichloropropane ND ug/L 03/11/15 22:07 78-87-51.0 1
1,3-Dichloropropane ND ug/L 03/11/15 22:07 142-28-91.0 1
2,2-Dichloropropane ND ug/L 03/11/15 22:07 594-20-71.0 1
1,1-Dichloropropene ND ug/L 03/11/15 22:07 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 03/11/15 22:07 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 03/11/15 22:07 10061-02-61.0 1
Diisopropyl ether ND ug/L 03/11/15 22:07 108-20-31.0 1
Ethylbenzene 5.4 ug/L 03/11/15 22:07 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 03/11/15 22:07 87-68-31.0 1
2-Hexanone ND ug/L 03/11/15 22:07 591-78-65.0 1
p-Isopropyltoluene ND ug/L 03/11/15 22:07 99-87-61.0 1
Methylene Chloride ND ug/L 03/11/15 22:07 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/11/15 22:07 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 03/11/15 22:07 1634-04-41.0 1
Naphthalene 1.4 ug/L 03/11/15 22:07 91-20-31.0 1
Styrene ND ug/L 03/11/15 22:07 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 03/11/15 22:07 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 03/11/15 22:07 79-34-51.0 1
Tetrachloroethene ND ug/L 03/11/15 22:07 127-18-41.0 1
Toluene 8.5 ug/L 03/11/15 22:07 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 03/11/15 22:07 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 03/11/15 22:07 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 03/11/15 22:07 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 03/11/15 22:07 79-00-51.0 1
Trichloroethene ND ug/L 03/11/15 22:07 79-01-61.0 1
Trichlorofluoromethane ND ug/L 03/11/15 22:07 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 03/11/15 22:07 96-18-41.0 1
Vinyl acetate ND ug/L 03/11/15 22:07 108-05-42.0 1
Vinyl chloride ND ug/L 03/11/15 22:07 75-01-41.0 1
Xylene (Total)22.4 ug/L 03/11/15 22:07 1330-20-72.0 1
m&p-Xylene 11.4 ug/L 03/11/15 22:07 179601-23-12.0 1
o-Xylene 11.1 ug/L 03/11/15 22:07 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %03/11/15 22:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %03/11/15 22:07 17060-07-070-130 1
Toluene-d8 (S)98 %03/11/15 22:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:TMW-5 Lab ID:92240297014 Collected:03/06/15 16:20 Received:03/09/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 03/12/15 14:01 83-32-903/10/15 08:1510.0 1
Acenaphthylene ND ug/L 03/12/15 14:01 208-96-803/10/15 08:1510.0 1
Aniline ND ug/L 03/12/15 14:01 62-53-303/10/15 08:1510.0 1
Anthracene ND ug/L 03/12/15 14:01 120-12-703/10/15 08:1510.0 1
Benzo(a)anthracene ND ug/L 03/12/15 14:01 56-55-303/10/15 08:1510.0 1
Benzo(a)pyrene ND ug/L 03/12/15 14:01 50-32-803/10/15 08:1510.0 1
Benzo(b)fluoranthene ND ug/L 03/12/15 14:01 205-99-203/10/15 08:1510.0 1
Benzo(g,h,i)perylene ND ug/L 03/12/15 14:01 191-24-203/10/15 08:1510.0 1
Benzo(k)fluoranthene ND ug/L 03/12/15 14:01 207-08-903/10/15 08:1510.0 1
Benzoic Acid ND ug/L 03/12/15 14:01 65-85-003/10/15 08:1550.0 1
Benzyl alcohol ND ug/L 03/12/15 14:01 100-51-603/10/15 08:1520.0 1
4-Bromophenylphenyl ether ND ug/L 03/12/15 14:01 101-55-303/10/15 08:1510.0 1
Butylbenzylphthalate ND ug/L 03/12/15 14:01 85-68-703/10/15 08:1510.0 1
4-Chloro-3-methylphenol ND ug/L 03/12/15 14:01 59-50-703/10/15 08:1520.0 1
4-Chloroaniline ND ug/L 03/12/15 14:01 106-47-803/10/15 08:1520.0 1
bis(2-Chloroethoxy)methane ND ug/L 03/12/15 14:01 111-91-103/10/15 08:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 03/12/15 14:01 111-44-403/10/15 08:1510.0 1
bis(2-Chloroisopropyl) ether ND ug/L 03/12/15 14:01 108-60-103/10/15 08:1510.0 1
2-Chloronaphthalene ND ug/L 03/12/15 14:01 91-58-703/10/15 08:1510.0 1
2-Chlorophenol ND ug/L 03/12/15 14:01 95-57-803/10/15 08:1510.0 1
4-Chlorophenylphenyl ether ND ug/L 03/12/15 14:01 7005-72-303/10/15 08:1510.0 1
Chrysene ND ug/L 03/12/15 14:01 218-01-903/10/15 08:1510.0 1
Dibenz(a,h)anthracene ND ug/L 03/12/15 14:01 53-70-303/10/15 08:1510.0 1
Dibenzofuran ND ug/L 03/12/15 14:01 132-64-903/10/15 08:1510.0 1
1,2-Dichlorobenzene ND ug/L 03/12/15 14:01 95-50-103/10/15 08:1510.0 1
1,3-Dichlorobenzene ND ug/L 03/12/15 14:01 541-73-103/10/15 08:1510.0 1
1,4-Dichlorobenzene ND ug/L 03/12/15 14:01 106-46-703/10/15 08:1510.0 1
3,3'-Dichlorobenzidine ND ug/L 03/12/15 14:01 91-94-103/10/15 08:1520.0 1
2,4-Dichlorophenol ND ug/L 03/12/15 14:01 120-83-203/10/15 08:1510.0 1
Diethylphthalate ND ug/L 03/12/15 14:01 84-66-203/10/15 08:1510.0 1
2,4-Dimethylphenol ND ug/L 03/12/15 14:01 105-67-903/10/15 08:1510.0 1
Dimethylphthalate ND ug/L 03/12/15 14:01 131-11-303/10/15 08:1510.0 1
Di-n-butylphthalate ND ug/L 03/12/15 14:01 84-74-203/10/15 08:1510.0 1
4,6-Dinitro-2-methylphenol ND ug/L 03/12/15 14:01 534-52-103/10/15 08:1520.0 1
2,4-Dinitrophenol ND ug/L 03/12/15 14:01 51-28-503/10/15 08:1550.0 1
2,4-Dinitrotoluene ND ug/L 03/12/15 14:01 121-14-203/10/15 08:1510.0 1
2,6-Dinitrotoluene ND ug/L 03/12/15 14:01 606-20-203/10/15 08:1510.0 1
Di-n-octylphthalate ND ug/L 03/12/15 14:01 117-84-003/10/15 08:1510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/12/15 14:01 117-81-703/10/15 08:156.0 1
Fluoranthene ND ug/L 03/12/15 14:01 206-44-003/10/15 08:1510.0 1
Fluorene ND ug/L 03/12/15 14:01 86-73-703/10/15 08:1510.0 1
Hexachloro-1,3-butadiene ND ug/L 03/12/15 14:01 87-68-303/10/15 08:1510.0 1
Hexachlorobenzene ND ug/L 03/12/15 14:01 118-74-103/10/15 08:1510.0 1
Hexachlorocyclopentadiene ND ug/L 03/12/15 14:01 77-47-403/10/15 08:1510.0 1
Hexachloroethane ND ug/L 03/12/15 14:01 67-72-103/10/15 08:1510.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/12/15 14:01 193-39-503/10/15 08:1510.0 1
Isophorone ND ug/L 03/12/15 14:01 78-59-103/10/15 08:1510.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:TMW-5 Lab ID:92240297014 Collected:03/06/15 16:20 Received:03/09/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 03/12/15 14:01 90-12-003/10/15 08:1510.0 1
2-Methylnaphthalene ND ug/L 03/12/15 14:01 91-57-603/10/15 08:1510.0 1
2-Methylphenol(o-Cresol)ND ug/L 03/12/15 14:01 95-48-703/10/15 08:1510.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/12/15 14:0103/10/15 08:1510.0 1
Naphthalene ND ug/L 03/12/15 14:01 91-20-303/10/15 08:1510.0 1
2-Nitroaniline ND ug/L 03/12/15 14:01 88-74-403/10/15 08:1550.0 1
3-Nitroaniline ND ug/L 03/12/15 14:01 99-09-203/10/15 08:1550.0 1
4-Nitroaniline ND ug/L 03/12/15 14:01 100-01-603/10/15 08:1520.0 1
Nitrobenzene ND ug/L 03/12/15 14:01 98-95-303/10/15 08:1510.0 1
2-Nitrophenol ND ug/L 03/12/15 14:01 88-75-503/10/15 08:1510.0 1
4-Nitrophenol ND ug/L 03/12/15 14:01 100-02-703/10/15 08:1550.0 1
N-Nitrosodimethylamine ND ug/L 03/12/15 14:01 62-75-903/10/15 08:1510.0 1
N-Nitroso-di-n-propylamine ND ug/L 03/12/15 14:01 621-64-703/10/15 08:1510.0 1
N-Nitrosodiphenylamine ND ug/L 03/12/15 14:01 86-30-603/10/15 08:1510.0 1
Pentachlorophenol ND ug/L 03/12/15 14:01 87-86-503/10/15 08:1525.0 1
Phenanthrene ND ug/L 03/12/15 14:01 85-01-803/10/15 08:1510.0 1
Phenol ND ug/L 03/12/15 14:01 108-95-203/10/15 08:1510.0 1
Pyrene ND ug/L 03/12/15 14:01 129-00-003/10/15 08:1510.0 1
1,2,4-Trichlorobenzene ND ug/L 03/12/15 14:01 120-82-103/10/15 08:1510.0 1
2,4,5-Trichlorophenol ND ug/L 03/12/15 14:01 95-95-403/10/15 08:1510.0 1
2,4,6-Trichlorophenol ND ug/L 03/12/15 14:01 88-06-203/10/15 08:1510.0 1
Surrogates
Nitrobenzene-d5 (S)66 %03/12/15 14:01 4165-60-003/10/15 08:1521-110 1
2-Fluorobiphenyl (S)69 %03/12/15 14:01 321-60-803/10/15 08:1527-110 1
Terphenyl-d14 (S)82 %03/12/15 14:01 1718-51-003/10/15 08:1531-107 1
Phenol-d6 (S)35 %03/12/15 14:01 13127-88-303/10/15 08:1510-110 1
2-Fluorophenol (S)42 %03/12/15 14:01 367-12-403/10/15 08:1512-110 1
2,4,6-Tribromophenol (S)77 %03/12/15 14:01 118-79-603/10/15 08:1527-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/11/15 19:19 67-64-125.0 1
Benzene ND ug/L 03/11/15 19:19 71-43-21.0 1
Bromobenzene ND ug/L 03/11/15 19:19 108-86-11.0 1
Bromochloromethane ND ug/L 03/11/15 19:19 74-97-51.0 1
Bromodichloromethane ND ug/L 03/11/15 19:19 75-27-41.0 1
Bromoform ND ug/L 03/11/15 19:19 75-25-21.0 1
Bromomethane ND ug/L 03/11/15 19:19 74-83-92.0 1
2-Butanone (MEK)ND ug/L 03/11/15 19:19 78-93-35.0 1
Carbon tetrachloride ND ug/L 03/11/15 19:19 56-23-51.0 1
Chlorobenzene ND ug/L 03/11/15 19:19 108-90-71.0 1
Chloroethane ND ug/L 03/11/15 19:19 75-00-31.0 1
Chloroform ND ug/L 03/11/15 19:19 67-66-31.0 1
Chloromethane ND ug/L 03/11/15 19:19 74-87-31.0 1
2-Chlorotoluene ND ug/L 03/11/15 19:19 95-49-81.0 1
4-Chlorotoluene ND ug/L 03/11/15 19:19 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 03/11/15 19:19 96-12-82.0 1
Dibromochloromethane ND ug/L 03/11/15 19:19 124-48-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 73
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Sample:TMW-5 Lab ID:92240297014 Collected:03/06/15 16:20 Received:03/09/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 03/11/15 19:19 106-93-41.0 1
Dibromomethane ND ug/L 03/11/15 19:19 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 03/11/15 19:19 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 03/11/15 19:19 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 03/11/15 19:19 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 03/11/15 19:19 75-71-81.0 1
1,1-Dichloroethane ND ug/L 03/11/15 19:19 75-34-31.0 1
1,2-Dichloroethane ND ug/L 03/11/15 19:19 107-06-21.0 1
1,1-Dichloroethene ND ug/L 03/11/15 19:19 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 03/11/15 19:19 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 03/11/15 19:19 156-60-51.0 1
1,2-Dichloropropane ND ug/L 03/11/15 19:19 78-87-51.0 1
1,3-Dichloropropane ND ug/L 03/11/15 19:19 142-28-91.0 1
2,2-Dichloropropane ND ug/L 03/11/15 19:19 594-20-71.0 1
1,1-Dichloropropene ND ug/L 03/11/15 19:19 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 03/11/15 19:19 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 03/11/15 19:19 10061-02-61.0 1
Diisopropyl ether ND ug/L 03/11/15 19:19 108-20-31.0 1
Ethylbenzene ND ug/L 03/11/15 19:19 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 03/11/15 19:19 87-68-31.0 1
2-Hexanone ND ug/L 03/11/15 19:19 591-78-65.0 1
p-Isopropyltoluene ND ug/L 03/11/15 19:19 99-87-61.0 1
Methylene Chloride ND ug/L 03/11/15 19:19 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/11/15 19:19 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 03/11/15 19:19 1634-04-41.0 1
Naphthalene ND ug/L 03/11/15 19:19 91-20-31.0 1
Styrene ND ug/L 03/11/15 19:19 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 03/11/15 19:19 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 03/11/15 19:19 79-34-51.0 1
Tetrachloroethene ND ug/L 03/11/15 19:19 127-18-41.0 1
Toluene ND ug/L 03/11/15 19:19 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 03/11/15 19:19 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 03/11/15 19:19 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 03/11/15 19:19 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 03/11/15 19:19 79-00-51.0 1
Trichloroethene ND ug/L 03/11/15 19:19 79-01-61.0 1
Trichlorofluoromethane ND ug/L 03/11/15 19:19 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 03/11/15 19:19 96-18-41.0 1
Vinyl acetate ND ug/L 03/11/15 19:19 108-05-42.0 1
Vinyl chloride ND ug/L 03/11/15 19:19 75-01-41.0 1
Xylene (Total)ND ug/L 03/11/15 19:19 1330-20-72.0 1
m&p-Xylene ND ug/L 03/11/15 19:19 179601-23-12.0 1
o-Xylene ND ug/L 03/11/15 19:19 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %03/11/15 19:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %03/11/15 19:19 17060-07-070-130 1
Toluene-d8 (S)97 %03/11/15 19:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/7652
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:92240297001, 92240297004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1407883
Associated Lab Samples:92240297001, 92240297004
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0050 03/12/15 13:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1407884LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.057.067 86 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1407885MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92240289027
1407886
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/kg .066 88 75-12594 8.0560.0084 0.066 0.061
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/7656
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:92240297006, 92240297009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1409834
Associated Lab Samples:92240297006, 92240297009
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0050 03/14/15 15:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1409835LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.062.067 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1409836MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92240237001
1409837
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/kg .047 85 75-12590 7.050.021 0.062 0.066
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/18045
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:92240297001, 92240297004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1407132
Associated Lab Samples:92240297001, 92240297004
Matrix:Solid
Analyzed
Arsenic mg/kg ND 1.0 03/10/15 22:19
Barium mg/kg ND 0.50 03/10/15 22:19
Cadmium mg/kg ND 0.10 03/10/15 22:19
Chromium mg/kg ND 0.50 03/10/15 22:19
Lead mg/kg ND 0.50 03/10/15 22:19
Selenium mg/kg ND 1.0 03/10/15 22:19
Silver mg/kg ND 0.50 03/10/15 22:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1407133LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 49.050 98 80-120
Barium mg/kg 46.150 92 80-120
Cadmium mg/kg 48.750 97 80-120
Chromium mg/kg 46.350 93 80-120
Lead mg/kg 48.350 97 80-120
Selenium mg/kg 49.450 99 80-120
Silver mg/kg 24.225 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1407134MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92239874001
1407135
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic mg/kg 47.7 92 75-12594 544.7ND 45.0 42.7
Barium mg/kg 47.7 88 75-125115 1044.752.0 93.8 104
Cadmium mg/kg 47.7 92 75-12592 744.7ND 44.1 41.2
Chromium mg/kg 47.7 89 75-12590 644.72.3 44.7 42.3
Lead mg/kg 47.7 90 75-12589 744.7ND 43.5 40.4
Selenium mg/kg 47.7 94 75-12593 744.7ND 45.0 41.8
Silver mg/kg 23.9 93 75-12592 722.3ND 22.2 20.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/18061
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:92240297006, 92240297009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1409666
Associated Lab Samples:92240297006, 92240297009
Matrix:Solid
Analyzed
Arsenic mg/kg ND 1.0 03/13/15 00:23
Barium mg/kg ND 0.50 03/13/15 00:23
Cadmium mg/kg ND 0.10 03/13/15 00:23
Chromium mg/kg ND 0.50 03/13/15 00:23
Lead mg/kg ND 0.50 03/13/15 00:23
Selenium mg/kg ND 1.0 03/13/15 00:23
Silver mg/kg ND 0.50 03/13/15 00:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1409667LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 47.750 95 80-120
Barium mg/kg 46.950 94 80-120
Cadmium mg/kg 48.550 97 80-120
Chromium mg/kg 47.450 95 80-120
Lead mg/kg 48.550 97 80-120
Selenium mg/kg 48.250 96 80-120
Silver mg/kg 24.225 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1409668MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92240237001
1409669
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic mg/kg M1,R152.4 96 75-12556 3549.527.3 77.7 54.8
Barium mg/kg 52.4 99 75-12578 1649.534.2 86.0 73.0
Cadmium mg/kg 52.4 91 75-12590 749.50.26 47.9 44.8
Chromium mg/kg 52.4 94 75-12588 949.510.5 59.5 54.2
Lead mg/kg 52.4 84 75-12577 949.523.0 66.9 61.2
Selenium mg/kg 52.4 84 75-12585 549.51.3 45.5 43.2
Silver mg/kg 26.2 93 75-12592 724.7ND 24.4 22.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30681
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92240297011, 92240297012, 92240297013, 92240297014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1408199
Associated Lab Samples:92240297011, 92240297012, 92240297013, 92240297014
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 03/11/15 16:49
1,1,1-Trichloroethane ug/L ND 1.0 03/11/15 16:49
1,1,2,2-Tetrachloroethane ug/L ND 1.0 03/11/15 16:49
1,1,2-Trichloroethane ug/L ND 1.0 03/11/15 16:49
1,1-Dichloroethane ug/L ND 1.0 03/11/15 16:49
1,1-Dichloroethene ug/L ND 1.0 03/11/15 16:49
1,1-Dichloropropene ug/L ND 1.0 03/11/15 16:49
1,2,3-Trichlorobenzene ug/L ND 1.0 03/11/15 16:49
1,2,3-Trichloropropane ug/L ND 1.0 03/11/15 16:49
1,2,4-Trichlorobenzene ug/L ND 1.0 03/11/15 16:49
1,2-Dibromo-3-chloropropane ug/L ND 2.0 03/11/15 16:49
1,2-Dibromoethane (EDB)ug/L ND 1.0 03/11/15 16:49
1,2-Dichlorobenzene ug/L ND 1.0 03/11/15 16:49
1,2-Dichloroethane ug/L ND 1.0 03/11/15 16:49
1,2-Dichloropropane ug/L ND 1.0 03/11/15 16:49
1,3-Dichlorobenzene ug/L ND 1.0 03/11/15 16:49
1,3-Dichloropropane ug/L ND 1.0 03/11/15 16:49
1,4-Dichlorobenzene ug/L ND 1.0 03/11/15 16:49
2,2-Dichloropropane ug/L ND 1.0 03/11/15 16:49
2-Butanone (MEK)ug/L ND 5.0 03/11/15 16:49
2-Chlorotoluene ug/L ND 1.0 03/11/15 16:49
2-Hexanone ug/L ND 5.0 03/11/15 16:49
4-Chlorotoluene ug/L ND 1.0 03/11/15 16:49
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 03/11/15 16:49
Acetone ug/L ND 25.0 03/11/15 16:49
Benzene ug/L ND 1.0 03/11/15 16:49
Bromobenzene ug/L ND 1.0 03/11/15 16:49
Bromochloromethane ug/L ND 1.0 03/11/15 16:49
Bromodichloromethane ug/L ND 1.0 03/11/15 16:49
Bromoform ug/L ND 1.0 03/11/15 16:49
Bromomethane ug/L ND 2.0 03/11/15 16:49
Carbon tetrachloride ug/L ND 1.0 03/11/15 16:49
Chlorobenzene ug/L ND 1.0 03/11/15 16:49
Chloroethane ug/L ND 1.0 03/11/15 16:49
Chloroform ug/L ND 1.0 03/11/15 16:49
Chloromethane ug/L ND 1.0 03/11/15 16:49
cis-1,2-Dichloroethene ug/L ND 1.0 03/11/15 16:49
cis-1,3-Dichloropropene ug/L ND 1.0 03/11/15 16:49
Dibromochloromethane ug/L ND 1.0 03/11/15 16:49
Dibromomethane ug/L ND 1.0 03/11/15 16:49
Dichlorodifluoromethane ug/L ND 1.0 03/11/15 16:49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1408199
Associated Lab Samples:92240297011, 92240297012, 92240297013, 92240297014
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 1.0 03/11/15 16:49
Ethylbenzene ug/L ND 1.0 03/11/15 16:49
Hexachloro-1,3-butadiene ug/L ND 1.0 03/11/15 16:49
m&p-Xylene ug/L ND 2.0 03/11/15 16:49
Methyl-tert-butyl ether ug/L ND 1.0 03/11/15 16:49
Methylene Chloride ug/L ND 2.0 03/11/15 16:49
Naphthalene ug/L ND 1.0 03/11/15 16:49
o-Xylene ug/L ND 1.0 03/11/15 16:49
p-Isopropyltoluene ug/L ND 1.0 03/11/15 16:49
Styrene ug/L ND 1.0 03/11/15 16:49
Tetrachloroethene ug/L ND 1.0 03/11/15 16:49
Toluene ug/L ND 1.0 03/11/15 16:49
trans-1,2-Dichloroethene ug/L ND 1.0 03/11/15 16:49
trans-1,3-Dichloropropene ug/L ND 1.0 03/11/15 16:49
Trichloroethene ug/L ND 1.0 03/11/15 16:49
Trichlorofluoromethane ug/L ND 1.0 03/11/15 16:49
Vinyl acetate ug/L ND 2.0 03/11/15 16:49
Vinyl chloride ug/L ND 1.0 03/11/15 16:49
Xylene (Total)ug/L ND 2.0 03/11/15 16:49
1,2-Dichloroethane-d4 (S)%97 70-130 03/11/15 16:49
4-Bromofluorobenzene (S)%97 70-130 03/11/15 16:49
Toluene-d8 (S)%99 70-130 03/11/15 16:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1408200LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.750 101 70-130
1,1,1-Trichloroethane ug/L 52.950 106 70-130
1,1,2,2-Tetrachloroethane ug/L 50.650 101 70-130
1,1,2-Trichloroethane ug/L 49.550 99 70-130
1,1-Dichloroethane ug/L 51.250 102 70-130
1,1-Dichloroethene ug/L 53.350 107 70-132
1,1-Dichloropropene ug/L 57.950 116 70-130
1,2,3-Trichlorobenzene ug/L 54.550 109 70-135
1,2,3-Trichloropropane ug/L 46.750 93 70-130
1,2,4-Trichlorobenzene ug/L 53.550 107 70-134
1,2-Dibromo-3-chloropropane ug/L 53.150 106 70-130
1,2-Dibromoethane (EDB)ug/L 51.850 104 70-130
1,2-Dichlorobenzene ug/L 50.550 101 70-130
1,2-Dichloroethane ug/L 46.650 93 70-130
1,2-Dichloropropane ug/L 49.750 99 70-130
1,3-Dichlorobenzene ug/L 49.550 99 70-130
1,3-Dichloropropane ug/L 50.350 101 70-130
1,4-Dichlorobenzene ug/L 50.550 101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1408200LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 53.650 107 58-145
2-Butanone (MEK)ug/L 102100 102 70-145
2-Chlorotoluene ug/L 52.250 104 70-130
2-Hexanone ug/L 119100 119 70-144
4-Chlorotoluene ug/L 50.850 102 70-130
4-Methyl-2-pentanone (MIBK)ug/L 106100 106 70-140
Acetone ug/L 106100 106 50-175
Benzene ug/L 51.850 104 70-130
Bromobenzene ug/L 52.250 104 70-130
Bromochloromethane ug/L 53.550 107 70-130
Bromodichloromethane ug/L 45.950 92 70-130
Bromoform ug/L 44.650 89 70-130
Bromomethane ug/L 54.950 110 54-130
Carbon tetrachloride ug/L 49.350 99 70-132
Chlorobenzene ug/L 49.150 98 70-130
Chloroethane ug/L 52.550 105 64-134
Chloroform ug/L 46.450 93 70-130
Chloromethane ug/L 56.450 113 64-130
cis-1,2-Dichloroethene ug/L 51.750 103 70-131
cis-1,3-Dichloropropene ug/L 52.950 106 70-130
Dibromochloromethane ug/L 49.550 99 70-130
Dibromomethane ug/L 48.050 96 70-131
Dichlorodifluoromethane ug/L 54.350 109 56-130
Diisopropyl ether ug/L 53.650 107 70-130
Ethylbenzene ug/L 51.350 103 70-130
Hexachloro-1,3-butadiene ug/L 68.3 L35013770-130
m&p-Xylene ug/L 101100 101 70-130
Methyl-tert-butyl ether ug/L 52.350 105 70-130
Methylene Chloride ug/L 54.750 109 63-130
Naphthalene ug/L 57.750 115 70-138
o-Xylene ug/L 49.950 100 70-130
p-Isopropyltoluene ug/L 54.250 108 70-130
Styrene ug/L 52.850 106 70-130
Tetrachloroethene ug/L 53.050 106 70-130
Toluene ug/L 50.950 102 70-130
trans-1,2-Dichloroethene ug/L 52.150 104 70-130
trans-1,3-Dichloropropene ug/L 53.350 107 70-132
Trichloroethene ug/L 49.350 99 70-130
Trichlorofluoromethane ug/L 48.850 98 62-133
Vinyl acetate ug/L 114100 114 66-157
Vinyl chloride ug/L 57.350 115 50-150
Xylene (Total)ug/L 151150 101 70-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1409023MATRIX SPIKE SAMPLE:
MSSpike
Result
92240546003
1,1,1,2-Tetrachloroethane ug/L 18.920 95 70-130ND
1,1,1-Trichloroethane ug/L 20.220 101 70-130ND
1,1,2,2-Tetrachloroethane ug/L 17.920 89 70-130ND
1,1,2-Trichloroethane ug/L 18.420 92 70-130ND
1,1-Dichloroethane ug/L 18.520 92 70-130ND
1,1-Dichloroethene ug/L 20.120 101 70-166ND
1,1-Dichloropropene ug/L 21.620 108 70-130ND
1,2,3-Trichlorobenzene ug/L 20.220 101 70-130ND
1,2,3-Trichloropropane ug/L 17.420 87 70-130ND
1,2,4-Trichlorobenzene ug/L 21.220 106 70-130ND
1,2-Dibromo-3-chloropropane ug/L 18.320 92 70-130ND
1,2-Dibromoethane (EDB)ug/L 18.720 94 70-130ND
1,2-Dichlorobenzene ug/L 19.020 95 70-130ND
1,2-Dichloroethane ug/L 16.920 84 70-130ND
1,2-Dichloropropane ug/L 18.220 91 70-130ND
1,3-Dichlorobenzene ug/L 18.420 92 70-130ND
1,3-Dichloropropane ug/L 18.020 90 70-130ND
1,4-Dichlorobenzene ug/L 18.720 94 70-130ND
2,2-Dichloropropane ug/L 20.320 101 70-130ND
2-Butanone (MEK)ug/L 35.840 90 70-130ND
2-Chlorotoluene ug/L 19.020 95 70-130ND
2-Hexanone ug/L 38.940 97 70-130ND
4-Chlorotoluene ug/L 18.520 93 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 39.540 99 70-130ND
Acetone ug/L 40.040 100 70-130ND
Benzene ug/L 19.520 97 70-148ND
Bromobenzene ug/L 18.620 93 70-130ND
Bromochloromethane ug/L 18.820 94 70-130ND
Bromodichloromethane ug/L 16.620 83 70-130ND
Bromoform ug/L 16.020 80 70-130ND
Bromomethane ug/L 18.120 90 70-130ND
Carbon tetrachloride ug/L 20.220 101 70-130ND
Chlorobenzene ug/L 18.320 91 70-146ND
Chloroethane ug/L 19.820 99 70-130ND
Chloroform ug/L 16.920 84 70-130ND
Chloromethane ug/L 18.720 94 70-130ND
cis-1,2-Dichloroethene ug/L 18.820 94 70-130ND
cis-1,3-Dichloropropene ug/L 18.020 90 70-130ND
Dibromochloromethane ug/L 17.120 86 70-130ND
Dibromomethane ug/L 18.420 92 70-130ND
Dichlorodifluoromethane ug/L 19.420 97 70-130ND
Diisopropyl ether ug/L 18.320 92 70-130ND
Ethylbenzene ug/L 19.320 97 70-130ND
Hexachloro-1,3-butadiene ug/L 25.820 129 70-130ND
m&p-Xylene ug/L 38.840 97 70-130ND
Methyl-tert-butyl ether ug/L 18.420 90 70-130ND
Methylene Chloride ug/L 16.020 80 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1409023MATRIX SPIKE SAMPLE:
MSSpike
Result
92240546003
Naphthalene ug/L 19.320 97 70-130ND
o-Xylene ug/L 18.520 92 70-130ND
p-Isopropyltoluene ug/L 21.220 106 70-130ND
Styrene ug/L 19.120 96 70-130ND
Tetrachloroethene ug/L 22.920 110 70-130ND
Toluene ug/L 19.220 96 70-155ND
trans-1,2-Dichloroethene ug/L 19.120 96 70-130ND
trans-1,3-Dichloropropene ug/L 18.720 93 70-130ND
Trichloroethene ug/L 19.620 98 69-151ND
Trichlorofluoromethane ug/L 19.820 99 70-130ND
Vinyl acetate ug/L 39.340 98 70-130ND
Vinyl chloride ug/L 20.220 101 70-130ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92240546005
1409024SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Chlorotoluene ug/L NDND
2-Hexanone ug/L NDND
4-Chlorotoluene ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Benzene ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92240546005
1409024SAMPLE DUPLICATE:
Bromobenzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Diisopropyl ether ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
m&p-Xylene ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylene Chloride ug/L NDND
Naphthalene ug/L NDND
o-Xylene ug/L NDND
p-Isopropyltoluene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%100 3103
4-Bromofluorobenzene (S)%104 499
Toluene-d8 (S)%98 098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30675
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92240297001, 92240297002, 92240297003, 92240297004, 92240297005, 92240297006, 92240297007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1407872
Associated Lab Samples:92240297001, 92240297002, 92240297003, 92240297004, 92240297005, 92240297006, 92240297007
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.7 03/11/15 11:57
1,1,1-Trichloroethane ug/kg ND 5.7 03/11/15 11:57
1,1,2,2-Tetrachloroethane ug/kg ND 5.7 03/11/15 11:57
1,1,2-Trichloroethane ug/kg ND 5.7 03/11/15 11:57
1,1-Dichloroethane ug/kg ND 5.7 03/11/15 11:57
1,1-Dichloroethene ug/kg ND 5.7 03/11/15 11:57
1,1-Dichloropropene ug/kg ND 5.7 03/11/15 11:57
1,2,3-Trichlorobenzene ug/kg ND 5.7 03/11/15 11:57
1,2,3-Trichloropropane ug/kg ND 5.7 03/11/15 11:57
1,2,4-Trichlorobenzene ug/kg ND 5.7 03/11/15 11:57
1,2,4-Trimethylbenzene ug/kg ND 5.7 03/11/15 11:57
1,2-Dibromo-3-chloropropane ug/kg ND 5.7 03/11/15 11:57
1,2-Dibromoethane (EDB)ug/kg ND 5.7 03/11/15 11:57
1,2-Dichlorobenzene ug/kg ND 5.7 03/11/15 11:57
1,2-Dichloroethane ug/kg ND 5.7 03/11/15 11:57
1,2-Dichloropropane ug/kg ND 5.7 03/11/15 11:57
1,3,5-Trimethylbenzene ug/kg ND 5.7 03/11/15 11:57
1,3-Dichlorobenzene ug/kg ND 5.7 03/11/15 11:57
1,3-Dichloropropane ug/kg ND 5.7 03/11/15 11:57
1,4-Dichlorobenzene ug/kg ND 5.7 03/11/15 11:57
2,2-Dichloropropane ug/kg ND 5.7 03/11/15 11:57
2-Butanone (MEK)ug/kg ND 114 03/11/15 11:57
2-Chlorotoluene ug/kg ND 5.7 03/11/15 11:57
2-Hexanone ug/kg ND 56.8 03/11/15 11:57
4-Chlorotoluene ug/kg ND 5.7 03/11/15 11:57
4-Methyl-2-pentanone (MIBK)ug/kg ND 56.8 03/11/15 11:57
Acetone ug/kg ND 114 03/11/15 11:57
Benzene ug/kg ND 5.7 03/11/15 11:57
Bromobenzene ug/kg ND 5.7 03/11/15 11:57
Bromochloromethane ug/kg ND 5.7 03/11/15 11:57
Bromodichloromethane ug/kg ND 5.7 03/11/15 11:57
Bromoform ug/kg ND 5.7 03/11/15 11:57
Bromomethane ug/kg ND 11.4 03/11/15 11:57
Carbon tetrachloride ug/kg ND 5.7 03/11/15 11:57
Chlorobenzene ug/kg ND 5.7 03/11/15 11:57
Chloroethane ug/kg ND 11.4 03/11/15 11:57
Chloroform ug/kg ND 5.7 03/11/15 11:57
Chloromethane ug/kg ND 11.4 03/11/15 11:57
cis-1,2-Dichloroethene ug/kg ND 5.7 03/11/15 11:57
cis-1,3-Dichloropropene ug/kg ND 5.7 03/11/15 11:57
Dibromochloromethane ug/kg ND 5.7 03/11/15 11:57
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1407872
Associated Lab Samples:92240297001, 92240297002, 92240297003, 92240297004, 92240297005, 92240297006, 92240297007
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 5.7 03/11/15 11:57
Dichlorodifluoromethane ug/kg ND 11.4 03/11/15 11:57
Diisopropyl ether ug/kg ND 5.7 03/11/15 11:57
Ethylbenzene ug/kg ND 5.7 03/11/15 11:57
Hexachloro-1,3-butadiene ug/kg ND 5.7 03/11/15 11:57
Isopropylbenzene (Cumene)ug/kg ND 5.7 03/11/15 11:57
m&p-Xylene ug/kg ND 11.4 03/11/15 11:57
Methyl-tert-butyl ether ug/kg ND 5.7 03/11/15 11:57
Methylene Chloride ug/kg ND 22.7 03/11/15 11:57
n-Butylbenzene ug/kg ND 5.7 03/11/15 11:57
n-Propylbenzene ug/kg ND 5.7 03/11/15 11:57
Naphthalene ug/kg ND 5.7 03/11/15 11:57
o-Xylene ug/kg ND 5.7 03/11/15 11:57
p-Isopropyltoluene ug/kg ND 5.7 03/11/15 11:57
sec-Butylbenzene ug/kg ND 5.7 03/11/15 11:57
Styrene ug/kg ND 5.7 03/11/15 11:57
tert-Butylbenzene ug/kg ND 5.7 03/11/15 11:57
Tetrachloroethene ug/kg ND 5.7 03/11/15 11:57
Toluene ug/kg ND 5.7 03/11/15 11:57
trans-1,2-Dichloroethene ug/kg ND 5.7 03/11/15 11:57
trans-1,3-Dichloropropene ug/kg ND 5.7 03/11/15 11:57
Trichloroethene ug/kg ND 5.7 03/11/15 11:57
Trichlorofluoromethane ug/kg ND 5.7 03/11/15 11:57
Vinyl acetate ug/kg ND 56.8 03/11/15 11:57
Vinyl chloride ug/kg ND 11.4 03/11/15 11:57
Xylene (Total)ug/kg ND 11.4 03/11/15 11:57
1,2-Dichloroethane-d4 (S)%96 70-132 03/11/15 11:57
4-Bromofluorobenzene (S)%104 70-130 03/11/15 11:57
Toluene-d8 (S)%101 70-130 03/11/15 11:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1407873LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 84.880.4 106 74-137
1,1,1-Trichloroethane ug/kg 82.580.4 103 67-140
1,1,2,2-Tetrachloroethane ug/kg 77.380.4 96 72-141
1,1,2-Trichloroethane ug/kg 82.680.4 103 78-138
1,1-Dichloroethane ug/kg 80.580.4 100 69-134
1,1-Dichloroethene ug/kg 80.480.4 100 67-138
1,1-Dichloropropene ug/kg 82.280.4 102 69-139
1,2,3-Trichlorobenzene ug/kg 91.580.4 114 70-146
1,2,3-Trichloropropane ug/kg 84.580.4 105 69-144
1,2,4-Trichlorobenzene ug/kg 88.380.4 110 68-148
1,2,4-Trimethylbenzene ug/kg 88.780.4 110 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1407873LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 78.380.4 97 65-140
1,2-Dibromoethane (EDB)ug/kg 83.880.4 104 77-135
1,2-Dichlorobenzene ug/kg 87.580.4 109 77-141
1,2-Dichloroethane ug/kg 84.880.4 105 65-137
1,2-Dichloropropane ug/kg 80.380.4 100 72-136
1,3,5-Trimethylbenzene ug/kg 86.880.4 108 76-133
1,3-Dichlorobenzene ug/kg 84.780.4 105 74-138
1,3-Dichloropropane ug/kg 81.080.4 101 71-139
1,4-Dichlorobenzene ug/kg 87.880.4 109 76-138
2,2-Dichloropropane ug/kg 81.580.4 101 68-137
2-Butanone (MEK)ug/kg 157J161 98 58-147
2-Chlorotoluene ug/kg 84.080.4 105 73-139
2-Hexanone ug/kg 164161 102 62-145
4-Chlorotoluene ug/kg 86.380.4 107 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 177161 110 64-149
Acetone ug/kg 151J161 94 53-153
Benzene ug/kg 84.180.4 105 73-135
Bromobenzene ug/kg 87.080.4 108 75-133
Bromochloromethane ug/kg 81.080.4 101 73-134
Bromodichloromethane ug/kg 78.080.4 97 71-135
Bromoform ug/kg 77.680.4 97 66-141
Bromomethane ug/kg 84.380.4 105 53-160
Carbon tetrachloride ug/kg 85.280.4 106 60-145
Chlorobenzene ug/kg 82.980.4 103 78-130
Chloroethane ug/kg 83.380.4 104 64-149
Chloroform ug/kg 75.580.4 94 70-134
Chloromethane ug/kg 79.480.4 99 52-150
cis-1,2-Dichloroethene ug/kg 82.280.4 102 70-133
cis-1,3-Dichloropropene ug/kg 82.180.4 102 68-134
Dibromochloromethane ug/kg 75.280.4 93 71-138
Dibromomethane ug/kg 83.980.4 104 74-130
Dichlorodifluoromethane ug/kg 76.680.4 95 40-160
Diisopropyl ether ug/kg 84.280.4 105 69-141
Ethylbenzene ug/kg 85.580.4 106 75-133
Hexachloro-1,3-butadiene ug/kg 83.780.4 104 68-143
Isopropylbenzene (Cumene)ug/kg 87.480.4 109 76-143
m&p-Xylene ug/kg 172161 107 75-136
Methyl-tert-butyl ether ug/kg 75.980.4 94 68-144
Methylene Chloride ug/kg 85.380.4 106 45-154
n-Butylbenzene ug/kg 85.780.4 107 72-137
n-Propylbenzene ug/kg 83.580.4 104 76-136
Naphthalene ug/kg 87.280.4 108 68-151
o-Xylene ug/kg 85.580.4 106 76-141
p-Isopropyltoluene ug/kg 84.180.4 105 76-140
sec-Butylbenzene ug/kg 83.680.4 104 79-139
Styrene ug/kg 87.980.4 109 79-137
tert-Butylbenzene ug/kg 83.980.4 104 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1407873LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 81.180.4 101 71-138
Toluene ug/kg 83.680.4 104 74-131
trans-1,2-Dichloroethene ug/kg 81.880.4 102 67-135
trans-1,3-Dichloropropene ug/kg 85.180.4 106 65-146
Trichloroethene ug/kg 86.180.4 107 67-135
Trichlorofluoromethane ug/kg 79.080.4 98 59-144
Vinyl acetate ug/kg 128 F31618040-160
Vinyl chloride ug/kg 73.780.4 92 56-141
Xylene (Total)ug/kg 258241 107 76-137
1,2-Dichloroethane-d4 (S)%98 70-132
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1409014MATRIX SPIKE SAMPLE:
MSSpike
Result
92240297002
1,1,1,2-Tetrachloroethane ug/kg 21.322.4 95 70-130ND
1,1,1-Trichloroethane ug/kg 20.122.4 90 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 29.6 M122.4 132 70-130ND
1,1,2-Trichloroethane ug/kg 27.822.4 124 70-130ND
1,1-Dichloroethane ug/kg 21.822.4 97 70-130ND
1,1-Dichloroethene ug/kg 19.722.4 88 49-180ND
1,1-Dichloropropene ug/kg 20.822.4 93 70-130ND
1,2,3-Trichlorobenzene ug/kg 22.422.4 100 70-130ND
1,2,3-Trichloropropane ug/kg 28.922.4 129 70-130ND
1,2,4-Trichlorobenzene ug/kg 20.522.4 92 70-130ND
1,2,4-Trimethylbenzene ug/kg 20.322.4 90 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 32.2 M122.4 144 70-130ND
1,2-Dibromoethane (EDB)ug/kg 27.522.4 123 70-130ND
1,2-Dichlorobenzene ug/kg 22.022.4 98 70-130ND
1,2-Dichloroethane ug/kg 26.722.4 119 70-130ND
1,2-Dichloropropane ug/kg 22.922.4 102 70-130ND
1,3,5-Trimethylbenzene ug/kg 19.122.4 85 70-130ND
1,3-Dichlorobenzene ug/kg 20.522.4 92 70-130ND
1,3-Dichloropropane ug/kg 26.622.4 119 70-130ND
1,4-Dichlorobenzene ug/kg 21.922.4 96 70-130ND
2,2-Dichloropropane ug/kg 19.422.4 87 70-130ND
2-Butanone (MEK)ug/kg 69.6J M144.7 155 70-130ND
2-Chlorotoluene ug/kg 19.922.4 89 70-130ND
2-Hexanone ug/kg 71.2 M144.7 159 70-130ND
4-Chlorotoluene ug/kg 20.222.4 90 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 79.2 M144.7 177 70-130ND
Acetone ug/kg 60.1J44.7 93 70-130ND
Benzene ug/kg 21.922.4 98 50-166ND
Bromobenzene ug/kg 22.822.4 102 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1409014MATRIX SPIKE SAMPLE:
MSSpike
Result
92240297002
Bromochloromethane ug/kg 25.022.4 112 70-130ND
Bromodichloromethane ug/kg 21.422.4 95 70-130ND
Bromoform ug/kg 26.222.4 117 70-130ND
Bromomethane ug/kg 20.922.4 94 70-130ND
Carbon tetrachloride ug/kg 19.222.4 86 70-130ND
Chlorobenzene ug/kg 21.322.4 95 43-169ND
Chloroethane ug/kg 20.822.4 93 70-130ND
Chloroform ug/kg 20.522.4 92 70-130ND
Chloromethane ug/kg 17.622.4 78 70-130ND
cis-1,2-Dichloroethene ug/kg 22.722.4 102 70-130ND
cis-1,3-Dichloropropene ug/kg 23.522.4 105 70-130ND
Dibromochloromethane ug/kg 22.722.4 102 70-130ND
Dibromomethane ug/kg 25.722.4 115 70-130ND
Dichlorodifluoromethane ug/kg 15.922.4 71 70-130ND
Diisopropyl ether ug/kg 24.322.4 108 70-130ND
Ethylbenzene ug/kg 20.822.4 93 70-130ND
Hexachloro-1,3-butadiene ug/kg 15.4 M122.4 69 70-130ND
Isopropylbenzene (Cumene)ug/kg 19.922.4 89 70-130ND
m&p-Xylene ug/kg 42.344.7 94 70-130ND
Methyl-tert-butyl ether ug/kg 28.522.4 127 70-130ND
Methylene Chloride ug/kg 22.1J M122.4 66 70-130ND
n-Butylbenzene ug/kg 18.622.4 83 70-130ND
n-Propylbenzene ug/kg 18.622.4 83 70-130ND
Naphthalene ug/kg 27.822.4 122 70-130ND
o-Xylene ug/kg 21.122.4 94 70-130ND
p-Isopropyltoluene ug/kg 18.322.4 82 70-130ND
sec-Butylbenzene ug/kg 18.222.4 81 70-130ND
Styrene ug/kg 22.422.4 100 70-130ND
tert-Butylbenzene ug/kg 18.122.4 81 70-130ND
Tetrachloroethene ug/kg 18.422.4 82 70-130ND
Toluene ug/kg 22.022.4 98 52-163ND
trans-1,2-Dichloroethene ug/kg 20.422.4 91 70-130ND
trans-1,3-Dichloropropene ug/kg 26.622.4 119 70-130ND
Trichloroethene ug/kg 19.922.4 89 49-167ND
Trichlorofluoromethane ug/kg 18.222.4 81 70-130ND
Vinyl acetate ug/kg 61.9 M144.7 138 70-130ND
Vinyl chloride ug/kg 17.322.4 77 70-130ND
1,2-Dichloroethane-d4 (S)%118 70-132
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92240297001
1409013SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92240297001
1409013SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92240297001
1409013SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%125 22119
4-Bromofluorobenzene (S)%104 21100
Toluene-d8 (S)%104 17104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30689
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92240297008, 92240297009, 92240297010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1409139
Associated Lab Samples:92240297008, 92240297009, 92240297010
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 4.8 03/12/15 12:37
1,1,1-Trichloroethane ug/kg ND 4.8 03/12/15 12:37
1,1,2,2-Tetrachloroethane ug/kg ND 4.8 03/12/15 12:37
1,1,2-Trichloroethane ug/kg ND 4.8 03/12/15 12:37
1,1-Dichloroethane ug/kg ND 4.8 03/12/15 12:37
1,1-Dichloroethene ug/kg ND 4.8 03/12/15 12:37
1,1-Dichloropropene ug/kg ND 4.8 03/12/15 12:37
1,2,3-Trichlorobenzene ug/kg ND 4.8 03/12/15 12:37
1,2,3-Trichloropropane ug/kg ND 4.8 03/12/15 12:37
1,2,4-Trichlorobenzene ug/kg ND 4.8 03/12/15 12:37
1,2,4-Trimethylbenzene ug/kg ND 4.8 03/12/15 12:37
1,2-Dibromo-3-chloropropane ug/kg ND 4.8 03/12/15 12:37
1,2-Dibromoethane (EDB)ug/kg ND 4.8 03/12/15 12:37
1,2-Dichlorobenzene ug/kg ND 4.8 03/12/15 12:37
1,2-Dichloroethane ug/kg ND 4.8 03/12/15 12:37
1,2-Dichloropropane ug/kg ND 4.8 03/12/15 12:37
1,3,5-Trimethylbenzene ug/kg ND 4.8 03/12/15 12:37
1,3-Dichlorobenzene ug/kg ND 4.8 03/12/15 12:37
1,3-Dichloropropane ug/kg ND 4.8 03/12/15 12:37
1,4-Dichlorobenzene ug/kg ND 4.8 03/12/15 12:37
2,2-Dichloropropane ug/kg ND 4.8 03/12/15 12:37
2-Butanone (MEK)ug/kg ND 96.0 03/12/15 12:37
2-Chlorotoluene ug/kg ND 4.8 03/12/15 12:37
2-Hexanone ug/kg ND 48.0 03/12/15 12:37
4-Chlorotoluene ug/kg ND 4.8 03/12/15 12:37
4-Methyl-2-pentanone (MIBK)ug/kg ND 48.0 03/12/15 12:37
Acetone ug/kg ND 96.0 03/12/15 12:37
Benzene ug/kg ND 4.8 03/12/15 12:37
Bromobenzene ug/kg ND 4.8 03/12/15 12:37
Bromochloromethane ug/kg ND 4.8 03/12/15 12:37
Bromodichloromethane ug/kg ND 4.8 03/12/15 12:37
Bromoform ug/kg ND 4.8 03/12/15 12:37
Bromomethane ug/kg ND 9.6 03/12/15 12:37
Carbon tetrachloride ug/kg ND 4.8 03/12/15 12:37
Chlorobenzene ug/kg ND 4.8 03/12/15 12:37
Chloroethane ug/kg ND 9.6 03/12/15 12:37
Chloroform ug/kg ND 4.8 03/12/15 12:37
Chloromethane ug/kg ND 9.6 03/12/15 12:37
cis-1,2-Dichloroethene ug/kg ND 4.8 03/12/15 12:37
cis-1,3-Dichloropropene ug/kg ND 4.8 03/12/15 12:37
Dibromochloromethane ug/kg ND 4.8 03/12/15 12:37
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
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Huntersville, NC 28078
[phone]
Page 54 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1409139
Associated Lab Samples:92240297008, 92240297009, 92240297010
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 4.8 03/12/15 12:37
Dichlorodifluoromethane ug/kg ND 9.6 03/12/15 12:37
Diisopropyl ether ug/kg ND 4.8 03/12/15 12:37
Ethylbenzene ug/kg ND 4.8 03/12/15 12:37
Hexachloro-1,3-butadiene ug/kg ND 4.8 03/12/15 12:37
Isopropylbenzene (Cumene)ug/kg ND 4.8 03/12/15 12:37
m&p-Xylene ug/kg ND 9.6 03/12/15 12:37
Methyl-tert-butyl ether ug/kg ND 4.8 03/12/15 12:37
Methylene Chloride ug/kg ND 19.2 03/12/15 12:37
n-Butylbenzene ug/kg ND 4.8 03/12/15 12:37
n-Propylbenzene ug/kg ND 4.8 03/12/15 12:37
Naphthalene ug/kg ND 4.8 03/12/15 12:37
o-Xylene ug/kg ND 4.8 03/12/15 12:37
p-Isopropyltoluene ug/kg ND 4.8 03/12/15 12:37
sec-Butylbenzene ug/kg ND 4.8 03/12/15 12:37
Styrene ug/kg ND 4.8 03/12/15 12:37
tert-Butylbenzene ug/kg ND 4.8 03/12/15 12:37
Tetrachloroethene ug/kg ND 4.8 03/12/15 12:37
Toluene ug/kg ND 4.8 03/12/15 12:37
trans-1,2-Dichloroethene ug/kg ND 4.8 03/12/15 12:37
trans-1,3-Dichloropropene ug/kg ND 4.8 03/12/15 12:37
Trichloroethene ug/kg ND 4.8 03/12/15 12:37
Trichlorofluoromethane ug/kg ND 4.8 03/12/15 12:37
Vinyl acetate ug/kg ND 48.0 03/12/15 12:37
Vinyl chloride ug/kg ND 9.6 03/12/15 12:37
Xylene (Total)ug/kg ND 9.6 03/12/15 12:37
1,2-Dichloroethane-d4 (S)%95 70-132 03/12/15 12:37
4-Bromofluorobenzene (S)%102 70-130 03/12/15 12:37
Toluene-d8 (S)%101 70-130 03/12/15 12:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1409140LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 47.746.6 102 74-137
1,1,1-Trichloroethane ug/kg 45.346.6 97 67-140
1,1,2,2-Tetrachloroethane ug/kg 41.046.6 88 72-141
1,1,2-Trichloroethane ug/kg 48.246.6 103 78-138
1,1-Dichloroethane ug/kg 47.746.6 102 69-134
1,1-Dichloroethene ug/kg 46.346.6 99 67-138
1,1-Dichloropropene ug/kg 47.246.6 101 69-139
1,2,3-Trichlorobenzene ug/kg 50.746.6 109 70-146
1,2,3-Trichloropropane ug/kg 45.346.6 97 69-144
1,2,4-Trichlorobenzene ug/kg 49.446.6 106 68-148
1,2,4-Trimethylbenzene ug/kg 49.246.6 106 74-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 55 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1409140LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 41.746.6 89 65-140
1,2-Dibromoethane (EDB)ug/kg 48.246.6 103 77-135
1,2-Dichlorobenzene ug/kg 48.446.6 104 77-141
1,2-Dichloroethane ug/kg 46.646.6 100 65-137
1,2-Dichloropropane ug/kg 47.546.6 102 72-136
1,3,5-Trimethylbenzene ug/kg 47.846.6 102 76-133
1,3-Dichlorobenzene ug/kg 47.946.6 103 74-138
1,3-Dichloropropane ug/kg 48.246.6 103 71-139
1,4-Dichlorobenzene ug/kg 49.246.6 106 76-138
2,2-Dichloropropane ug/kg 45.746.6 98 68-137
2-Butanone (MEK)ug/kg 87.3J93.3 94 58-147
2-Chlorotoluene ug/kg 47.546.6 102 73-139
2-Hexanone ug/kg 88.993.3 95 62-145
4-Chlorotoluene ug/kg 47.946.6 103 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 98.693.3 106 64-149
Acetone ug/kg 85.4J93.3 92 53-153
Benzene ug/kg 49.746.6 107 73-135
Bromobenzene ug/kg 47.146.6 101 75-133
Bromochloromethane ug/kg 48.146.6 103 73-134
Bromodichloromethane ug/kg 45.446.6 97 71-135
Bromoform ug/kg 43.746.6 94 66-141
Bromomethane ug/kg 48.546.6 104 53-160
Carbon tetrachloride ug/kg 48.446.6 104 60-145
Chlorobenzene ug/kg 46.846.6 100 78-130
Chloroethane ug/kg 48.546.6 104 64-149
Chloroform ug/kg 44.246.6 95 70-134
Chloromethane ug/kg 44.846.6 96 52-150
cis-1,2-Dichloroethene ug/kg 49.446.6 106 70-133
cis-1,3-Dichloropropene ug/kg 48.646.6 104 68-134
Dibromochloromethane ug/kg 43.246.6 93 71-138
Dibromomethane ug/kg 48.946.6 105 74-130
Dichlorodifluoromethane ug/kg 44.346.6 95 40-160
Diisopropyl ether ug/kg 49.146.6 105 69-141
Ethylbenzene ug/kg 48.546.6 104 75-133
Hexachloro-1,3-butadiene ug/kg 46.846.6 100 68-143
Isopropylbenzene (Cumene)ug/kg 47.646.6 102 76-143
m&p-Xylene ug/kg 95.693.3 102 75-136
Methyl-tert-butyl ether ug/kg 44.246.6 95 68-144
Methylene Chloride ug/kg 44.946.6 96 45-154
n-Butylbenzene ug/kg 48.046.6 103 72-137
n-Propylbenzene ug/kg 46.746.6 100 76-136
Naphthalene ug/kg 48.046.6 103 68-151
o-Xylene ug/kg 47.946.6 103 76-141
p-Isopropyltoluene ug/kg 46.646.6 100 76-140
sec-Butylbenzene ug/kg 46.546.6 100 79-139
Styrene ug/kg 49.046.6 105 79-137
tert-Butylbenzene ug/kg 46.546.6 100 74-143
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
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Huntersville, NC 28078
[phone]
Page 56 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1409140LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 46.146.6 99 71-138
Toluene ug/kg 48.246.6 103 74-131
trans-1,2-Dichloroethene ug/kg 47.846.6 102 67-135
trans-1,3-Dichloropropene ug/kg 50.346.6 108 65-146
Trichloroethene ug/kg 50.946.6 109 67-135
Trichlorofluoromethane ug/kg 44.546.6 96 59-144
Vinyl acetate ug/kg 50.0 F393.3 54 40-160
Vinyl chloride ug/kg 43.146.6 92 56-141
Xylene (Total)ug/kg 143140 103 76-137
1,2-Dichloroethane-d4 (S)%94 70-132
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1410073MATRIX SPIKE SAMPLE:
MSSpike
Result
92240612002
1,1,1,2-Tetrachloroethane ug/kg 23.522.4 105 70-130ND
1,1,1-Trichloroethane ug/kg 25.122.4 112 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 20.722.4 92 70-130ND
1,1,2-Trichloroethane ug/kg 21.822.4 98 70-130ND
1,1-Dichloroethane ug/kg 24.822.4 111 70-130ND
1,1-Dichloroethene ug/kg 24.522.4 110 49-180ND
1,1-Dichloropropene ug/kg 23.822.4 106 70-130ND
1,2,3-Trichlorobenzene ug/kg 12.2 M122.4 55 70-130ND
1,2,3-Trichloropropane ug/kg 23.322.4 104 70-130ND
1,2,4-Trichlorobenzene ug/kg 12.5 M122.4 56 70-130ND
1,2,4-Trimethylbenzene ug/kg 30.6 M122.4 137 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 29.022.4 130 70-130ND
1,2-Dibromoethane (EDB)ug/kg 23.122.4 103 70-130ND
1,2-Dichlorobenzene ug/kg 22.322.4 100 70-130ND
1,2-Dichloroethane ug/kg 24.622.4 110 70-130ND
1,2-Dichloropropane ug/kg 24.422.4 109 70-130ND
1,3,5-Trimethylbenzene ug/kg 32.3 M122.4 145 70-130ND
1,3-Dichlorobenzene ug/kg 23.822.4 107 70-130ND
1,3-Dichloropropane ug/kg 26.622.4 119 70-130ND
1,4-Dichlorobenzene ug/kg 24.522.4 109 70-130ND
2,2-Dichloropropane ug/kg 25.022.4 112 70-130ND
2-Butanone (MEK)ug/kg 41.5J44.6 93 70-130ND
2-Chlorotoluene ug/kg 31.5 M122.4 141 70-130ND
2-Hexanone ug/kg 35.8J44.6 80 70-130ND
4-Chlorotoluene ug/kg 29.8 M122.4 133 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 39.2J44.6 88 70-130ND
Acetone ug/kg 76.6J M144.6 171 70-130ND
Benzene ug/kg 25.022.4 112 50-166ND
Bromobenzene ug/kg 29.9 M122.4 134 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1410073MATRIX SPIKE SAMPLE:
MSSpike
Result
92240612002
Bromochloromethane ug/kg 25.222.4 113 70-130ND
Bromodichloromethane ug/kg 21.022.4 94 70-130ND
Bromoform ug/kg 18.322.4 82 70-130ND
Bromomethane ug/kg 17.522.4 79 70-130ND
Carbon tetrachloride ug/kg 24.922.4 111 70-130ND
Chlorobenzene ug/kg 23.322.4 104 43-169ND
Chloroethane ug/kg 25.322.4 113 70-130ND
Chloroform ug/kg 23.122.4 103 70-130ND
Chloromethane ug/kg 21.722.4 97 70-130ND
cis-1,2-Dichloroethene ug/kg 24.022.4 107 70-130ND
cis-1,3-Dichloropropene ug/kg 14.9 M122.4 66 70-130ND
Dibromochloromethane ug/kg 21.622.4 97 70-130ND
Dibromomethane ug/kg 24.322.4 109 70-130ND
Dichlorodifluoromethane ug/kg 21.722.4 97 70-130ND
Diisopropyl ether ug/kg 24.922.4 111 70-130ND
Ethylbenzene ug/kg 26.222.4 117 70-130ND
Hexachloro-1,3-butadiene ug/kg 21.722.4 97 70-130ND
Isopropylbenzene (Cumene)ug/kg 24.622.4 110 70-130ND
m&p-Xylene ug/kg 51.544.6 115 70-130ND
Methyl-tert-butyl ether ug/kg 23.222.4 104 70-130ND
Methylene Chloride ug/kg 22.822.4 96 70-130ND
n-Butylbenzene ug/kg 28.222.4 126 70-130ND
n-Propylbenzene ug/kg 33.3 M122.4 149 70-130ND
Naphthalene ug/kg 13.3 M122.4 59 70-130ND
o-Xylene ug/kg 24.222.4 108 70-130ND
p-Isopropyltoluene ug/kg 30.2 M122.4 135 70-130ND
sec-Butylbenzene ug/kg 32.4 M122.4 145 70-130ND
Styrene ug/kg 20.622.4 92 70-130ND
tert-Butylbenzene ug/kg 32.1 M122.4 144 70-130ND
Tetrachloroethene ug/kg 25.122.4 112 70-130ND
Toluene ug/kg 23.522.4 105 52-163ND
trans-1,2-Dichloroethene ug/kg 23.822.4 107 70-130ND
trans-1,3-Dichloropropene ug/kg 16.122.4 72 70-130ND
Trichloroethene ug/kg 23.622.4 105 49-167ND
Trichlorofluoromethane ug/kg 22.222.4 99 70-130ND
Vinyl acetate ug/kg ND M144.6 18 70-130ND
Vinyl chloride ug/kg 22.622.4 101 70-130ND
1,2-Dichloroethane-d4 (S)%104 70-132
4-Bromofluorobenzene (S)%89 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92240297008
1410072SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
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Page 58 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92240297008
1410072SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg 16.7JND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg 3.4JND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92240297008
1410072SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%113 3118
4-Bromofluorobenzene (S)%104 4100
Toluene-d8 (S)%103 1104
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/33524
EPA 3546
EPA 8015 Modified
8015 Solid GCSV
Associated Lab Samples:92240297001, 92240297002, 92240297003, 92240297004, 92240297005, 92240297006, 92240297007,
92240297008, 92240297009, 92240297010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1409006
Associated Lab Samples:92240297001, 92240297002, 92240297003, 92240297004, 92240297005, 92240297006, 92240297007,
92240297008, 92240297009, 92240297010
Matrix:Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 5.0 03/13/15 14:42
n-Pentacosane (S)%80 41-119 03/13/15 14:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1409007LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 61.566.7 92 49-113
n-Pentacosane (S)%87 41-119
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1409008MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92240187001
1409009
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Diesel Range Organics(C10-
C28)mg/kg 70.8 88 10-14684 370.823.7 85.8 83.0
n-Pentacosane (S)%70 41-11971
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/33445
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92240297011, 92240297012, 92240297013, 92240297014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1406484
Associated Lab Samples:92240297011, 92240297012, 92240297013, 92240297014
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 03/11/15 12:33
1,2-Dichlorobenzene ug/L ND 10.0 03/11/15 12:33
1,3-Dichlorobenzene ug/L ND 10.0 03/11/15 12:33
1,4-Dichlorobenzene ug/L ND 10.0 03/11/15 12:33
1-Methylnaphthalene ug/L ND 10.0 03/11/15 12:33
2,4,5-Trichlorophenol ug/L ND 10.0 03/11/15 12:33
2,4,6-Trichlorophenol ug/L ND 10.0 03/11/15 12:33
2,4-Dichlorophenol ug/L ND 10.0 03/11/15 12:33
2,4-Dimethylphenol ug/L ND 10.0 03/11/15 12:33
2,4-Dinitrophenol ug/L ND 50.0 03/11/15 12:33
2,4-Dinitrotoluene ug/L ND 10.0 03/11/15 12:33
2,6-Dinitrotoluene ug/L ND 10.0 03/11/15 12:33
2-Chloronaphthalene ug/L ND 10.0 03/11/15 12:33
2-Chlorophenol ug/L ND 10.0 03/11/15 12:33
2-Methylnaphthalene ug/L ND 10.0 03/11/15 12:33
2-Methylphenol(o-Cresol)ug/L ND 10.0 03/11/15 12:33
2-Nitroaniline ug/L ND 50.0 03/11/15 12:33
2-Nitrophenol ug/L ND 10.0 03/11/15 12:33
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 03/11/15 12:33
3,3'-Dichlorobenzidine ug/L ND 20.0 03/11/15 12:33
3-Nitroaniline ug/L ND 50.0 03/11/15 12:33
4,6-Dinitro-2-methylphenol ug/L ND 20.0 03/11/15 12:33
4-Bromophenylphenyl ether ug/L ND 10.0 03/11/15 12:33
4-Chloro-3-methylphenol ug/L ND 20.0 03/11/15 12:33
4-Chloroaniline ug/L ND 20.0 03/11/15 12:33
4-Chlorophenylphenyl ether ug/L ND 10.0 03/11/15 12:33
4-Nitroaniline ug/L ND 20.0 03/11/15 12:33
4-Nitrophenol ug/L ND 50.0 03/11/15 12:33
Acenaphthene ug/L ND 10.0 03/11/15 12:33
Acenaphthylene ug/L ND 10.0 03/11/15 12:33
Aniline ug/L ND 10.0 03/11/15 12:33
Anthracene ug/L ND 10.0 03/11/15 12:33
Benzo(a)anthracene ug/L ND 10.0 03/11/15 12:33
Benzo(a)pyrene ug/L ND 10.0 03/11/15 12:33
Benzo(b)fluoranthene ug/L ND 10.0 03/11/15 12:33
Benzo(g,h,i)perylene ug/L ND 10.0 03/11/15 12:33
Benzo(k)fluoranthene ug/L ND 10.0 03/11/15 12:33
Benzoic Acid ug/L ND 50.0 03/11/15 12:33
Benzyl alcohol ug/L ND 20.0 03/11/15 12:33
bis(2-Chloroethoxy)methane ug/L ND 10.0 03/11/15 12:33
bis(2-Chloroethyl) ether ug/L ND 10.0 03/11/15 12:33
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
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Page 62 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1406484
Associated Lab Samples:92240297011, 92240297012, 92240297013, 92240297014
Matrix:Water
Analyzed
bis(2-Chloroisopropyl) ether ug/L ND 10.0 03/11/15 12:33
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 03/11/15 12:33
Butylbenzylphthalate ug/L ND 10.0 03/11/15 12:33
Chrysene ug/L ND 10.0 03/11/15 12:33
Di-n-butylphthalate ug/L ND 10.0 03/11/15 12:33
Di-n-octylphthalate ug/L ND 10.0 03/11/15 12:33
Dibenz(a,h)anthracene ug/L ND 10.0 03/11/15 12:33
Dibenzofuran ug/L ND 10.0 03/11/15 12:33
Diethylphthalate ug/L ND 10.0 03/11/15 12:33
Dimethylphthalate ug/L ND 10.0 03/11/15 12:33
Fluoranthene ug/L ND 10.0 03/11/15 12:33
Fluorene ug/L ND 10.0 03/11/15 12:33
Hexachloro-1,3-butadiene ug/L ND 10.0 03/11/15 12:33
Hexachlorobenzene ug/L ND 10.0 03/11/15 12:33
Hexachlorocyclopentadiene ug/L ND 10.0 03/11/15 12:33
Hexachloroethane ug/L ND 10.0 03/11/15 12:33
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 03/11/15 12:33
Isophorone ug/L ND 10.0 03/11/15 12:33
N-Nitroso-di-n-propylamine ug/L ND 10.0 03/11/15 12:33
N-Nitrosodimethylamine ug/L ND 10.0 03/11/15 12:33
N-Nitrosodiphenylamine ug/L ND 10.0 03/11/15 12:33
Naphthalene ug/L ND 10.0 03/11/15 12:33
Nitrobenzene ug/L ND 10.0 03/11/15 12:33
Pentachlorophenol ug/L ND 25.0 03/11/15 12:33
Phenanthrene ug/L ND 10.0 03/11/15 12:33
Phenol ug/L ND 10.0 03/11/15 12:33
Pyrene ug/L ND 10.0 03/11/15 12:33
2,4,6-Tribromophenol (S)%88 27-110 03/11/15 12:33
2-Fluorobiphenyl (S)%78 27-110 03/11/15 12:33
2-Fluorophenol (S)%41 12-110 03/11/15 12:33
Nitrobenzene-d5 (S)%77 21-110 03/11/15 12:33
Phenol-d6 (S)%27 10-110 03/11/15 12:33
Terphenyl-d14 (S)%100 31-107 03/11/15 12:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1406485LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 27.850 56 31-120
1,2-Dichlorobenzene ug/L 32.850 66 38-120
1,3-Dichlorobenzene ug/L 29.950 60 30-122
1,4-Dichlorobenzene ug/L 32.650 65 37-120
1-Methylnaphthalene ug/L 33.150 66 34-113
2,4,5-Trichlorophenol ug/L 43.750 87 43-113
2,4,6-Trichlorophenol ug/L 44.050 88 42-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
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Page 63 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1406485LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dichlorophenol ug/L 33.750 67 30-120
2,4-Dimethylphenol ug/L 32.450 65 29-111
2,4-Dinitrophenol ug/L 219250 88 19-132
2,4-Dinitrotoluene ug/L 48.650 97 58-128
2,6-Dinitrotoluene ug/L 51.150 102 54-129
2-Chloronaphthalene ug/L 49.050 98 43-117
2-Chlorophenol ug/L 37.850 76 37-120
2-Methylnaphthalene ug/L 30.350 61 33-120
2-Methylphenol(o-Cresol)ug/L 32.150 64 31-120
2-Nitroaniline ug/L 92.6100 93 48-121
2-Nitrophenol ug/L 36.150 72 25-116
3&4-Methylphenol(m&p Cresol)ug/L 24.250 48 23-120
3,3'-Dichlorobenzidine ug/L 93.0100 93 10-154
3-Nitroaniline ug/L 87.3100 87 43-115
4,6-Dinitro-2-methylphenol ug/L 107100 107 44-124
4-Bromophenylphenyl ether ug/L 48.350 97 34-113
4-Chloro-3-methylphenol ug/L 63.7100 64 31-110
4-Chloroaniline ug/L 67.6100 68 20-120
4-Chlorophenylphenyl ether ug/L 46.250 92 34-116
4-Nitroaniline ug/L 89.5100 89 46-128
4-Nitrophenol ug/L 81.3250 33 11-120
Acenaphthene ug/L 44.050 88 48-114
Acenaphthylene ug/L 44.050 88 48-112
Aniline ug/L 29.550 59 26-120
Anthracene ug/L 45.750 91 57-118
Benzo(a)anthracene ug/L 45.450 91 56-121
Benzo(a)pyrene ug/L 47.350 95 55-127
Benzo(b)fluoranthene ug/L 52.750 105 53-128
Benzo(g,h,i)perylene ug/L 47.650 95 54-125
Benzo(k)fluoranthene ug/L 47.650 95 51-123
Benzoic Acid ug/L 41.1J250 16 10-120
Benzyl alcohol ug/L 73.0100 73 27-120
bis(2-Chloroethoxy)methane ug/L 47.750 95 32-120
bis(2-Chloroethyl) ether ug/L 48.850 98 33-111
bis(2-Chloroisopropyl) ether ug/L 43.250 86 15-120
bis(2-Ethylhexyl)phthalate ug/L 44.350 89 50-145
Butylbenzylphthalate ug/L 44.250 88 54-138
Chrysene ug/L 47.650 95 58-127
Di-n-butylphthalate ug/L 48.550 97 56-125
Di-n-octylphthalate ug/L 42.150 84 50-134
Dibenz(a,h)anthracene ug/L 49.450 99 53-129
Dibenzofuran ug/L 46.250 92 45-120
Diethylphthalate ug/L 45.950 92 53-120
Dimethylphthalate ug/L 45.950 92 55-116
Fluoranthene ug/L 44.450 89 57-125
Fluorene ug/L 47.250 94 53-118
Hexachloro-1,3-butadiene ug/L 24.650 49 23-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
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[phone]
Page 64 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1406485LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/L 46.650 93 49-116
Hexachlorocyclopentadiene ug/L 33.150 66 26-158
Hexachloroethane ug/L 32.550 65 30-114
Indeno(1,2,3-cd)pyrene ug/L 50.650 101 55-128
Isophorone ug/L 35.850 72 31-118
N-Nitroso-di-n-propylamine ug/L 44.450 89 32-119
N-Nitrosodimethylamine ug/L 25.350 51 13-120
N-Nitrosodiphenylamine ug/L 47.450 95 43-120
Naphthalene ug/L 31.050 62 32-120
Nitrobenzene ug/L 34.450 69 33-110
Pentachlorophenol ug/L 84.4100 84 10-137
Phenanthrene ug/L 44.850 90 57-117
Phenol ug/L 21.850 44 10-120
Pyrene ug/L 43.050 86 55-122
2,4,6-Tribromophenol (S)%96 27-110
2-Fluorobiphenyl (S)%90 27-110
2-Fluorophenol (S)%46 12-110
Nitrobenzene-d5 (S)%65 21-110
Phenol-d6 (S)%31 10-110
Terphenyl-d14 (S)%100 31-107
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/7596
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92240297001, 92240297002, 92240297003, 92240297004
Parameter Units
Dup
Result QualifiersRPDResult
92240273001
1406446SAMPLE DUPLICATE:
Percent Moisture %14.0 1215.8
Parameter Units
Dup
Result QualifiersRPDResult
92240297004
1406447SAMPLE DUPLICATE:
Percent Moisture %13.3 914.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 73
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/7597
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92240297005, 92240297006, 92240297007, 92240297008, 92240297009, 92240297010
Parameter Units
Dup
Result QualifiersRPDResult
92240087001
1406448SAMPLE DUPLICATE:
Percent Moisture %18.7 118.6
Parameter Units
Dup
Result QualifiersRPDResult
92240302002
1406449SAMPLE DUPLICATE:
Percent Moisture %33.5 332.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
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Page 67 of 73
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
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[phone]
Page 68 of 73
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92240297001 OEXT/33524 GCSV/20627SS-6 EPA 3546 EPA 8015 Modified
92240297002 OEXT/33524 GCSV/20627SS-7 EPA 3546 EPA 8015 Modified
92240297003 OEXT/33524 GCSV/20627SS-8 EPA 3546 EPA 8015 Modified
92240297004 OEXT/33524 GCSV/20627SS-9 EPA 3546 EPA 8015 Modified
92240297005 OEXT/33524 GCSV/20627SS-10 EPA 3546 EPA 8015 Modified
92240297006 OEXT/33524 GCSV/20627SS-11 EPA 3546 EPA 8015 Modified
92240297007 OEXT/33524 GCSV/20627SS-12 EPA 3546 EPA 8015 Modified
92240297008 OEXT/33524 GCSV/20627SS-13 EPA 3546 EPA 8015 Modified
92240297009 OEXT/33524 GCSV/20627SS-14 EPA 3546 EPA 8015 Modified
92240297010 OEXT/33524 GCSV/20627SS-15 EPA 3546 EPA 8015 Modified
92240297001 MPRP/18045 ICP/16219SS-6 EPA 3050 EPA 6010
92240297004 MPRP/18045 ICP/16219SS-9 EPA 3050 EPA 6010
92240297006 MPRP/18061 ICP/16231SS-11 EPA 3050 EPA 6010
92240297009 MPRP/18061 ICP/16231SS-14 EPA 3050 EPA 6010
92240297001 MERP/7652 MERC/7342SS-6 EPA 7471 EPA 7471
92240297004 MERP/7652 MERC/7342SS-9 EPA 7471 EPA 7471
92240297006 MERP/7656 MERC/7346SS-11 EPA 7471 EPA 7471
92240297009 MERP/7656 MERC/7346SS-14 EPA 7471 EPA 7471
92240297011 OEXT/33445 MSSV/10395TMW-2 EPA 3510 EPA 8270
92240297012 OEXT/33445 MSSV/10395TMW-3 EPA 3510 EPA 8270
92240297013 OEXT/33445 MSSV/10395TMW-4 EPA 3510 EPA 8270
92240297014 OEXT/33445 MSSV/10395TMW-5 EPA 3510 EPA 8270
92240297011 MSV/30681TMW-2 EPA 8260
92240297012 MSV/30681TMW-3 EPA 8260
92240297013 MSV/30681TMW-4 EPA 8260
92240297014 MSV/30681TMW-5 EPA 8260
92240297001 MSV/30675SS-6 EPA 8260
92240297002 MSV/30675SS-7 EPA 8260
92240297003 MSV/30675SS-8 EPA 8260
92240297004 MSV/30675SS-9 EPA 8260
92240297005 MSV/30675SS-10 EPA 8260
92240297006 MSV/30675SS-11 EPA 8260
92240297007 MSV/30675SS-12 EPA 8260
92240297008 MSV/30689SS-13 EPA 8260
92240297009 MSV/30689SS-14 EPA 8260
92240297010 MSV/30689SS-15 EPA 8260
92240297001 PMST/7596SS-6 ASTM D2974-87
92240297002 PMST/7596SS-7 ASTM D2974-87
92240297003 PMST/7596SS-8 ASTM D2974-87
92240297004 PMST/7596SS-9 ASTM D2974-87
92240297005 PMST/7597SS-10 ASTM D2974-87
92240297006 PMST/7597SS-11 ASTM D2974-87
92240297007 PMST/7597SS-12 ASTM D2974-87
92240297008 PMST/7597SS-13 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
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[phone]
Page 69 of 73
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92240297
HENDRICK DURHAM AUTO 22255-A
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92240297009 PMST/7597SS-14 ASTM D2974-87
92240297010 PMST/7597SS-15 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/16/2015 04:09 PM
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Page 70 of 73
Page 71 of 73
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