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HomeMy WebLinkAbout19043_C & E Manufacturing_BPA_2015_06_11 Via Fed Ex 2nd Day June 11, 2015 NCDENR Division of Waste Management NC Brownfields Program 1646 Mail Service Center Raleigh, NC 27699 Attention: Ms. Shirley Liggins Re: Brownfields Property Application C&E Manufacturing Ltd. (a.k.a. ADDCO) 1600 Linville Falls Highway Avery County, North Carolina H&H Job No. FCB.014 Dear Shirley: Enclosed please find the original of the Brownfields Property Application for the above referenced project. If you have any questions, please feel free to contact me. Sincerely, Hart & Hickman, PC Matt Ingalls Project Manager MJI/vmg Enclosures cc: Mr. Steve Pollock, First Citizens Bank (via email) Brownfields Property Application C&E Manufacturing Ltd. (a.k.a. ADDCO) 1600 Linville Falls Highway Avery County, North Carolina H&H Job No. FCB.014 June 8, 2015 4 Brownfields Property Application North Carolina Brownfields Program www.ncbrownfields.org I. PROSPECTIVE DEVELOPER (PD) INFORMATION {USE TAB KEY TO GET TO NEXT DATA ENTRY LINE – DO NOT USE THE RETURN KEY} A. PD information: Entity name First-Citizens Bank & Trust Company (FCB) Principal Officer Steve Pollok Representative Steve Pollok Mailing Address Mail Code: DAC36, 100 E Tryon Road, Raleigh, NC 27603 E-mail address Steve.Pollok@firstcitizens.com Phone No. 919-716-8793 Fax No. 919-716-2410 Web site B. PD contact person information (i.e., individual who will serve as the NCBP’s point of contact if different than above): Name Matt Ingalls Company Hart & Hickman, PC Mailing Address 2923 S. Tryon Street #100 Charlotte, NC 28203 E-Mail Address mingalls@harthickman.com Phone No. 704-586-0007 Fax No. 704-586-0373 C. Information regarding all parent companies, subsidiaries or other affiliates of PD (attach separate sheet(s) if necessary): (Use for LLCs) Member-managed or manager-managed? Answer: 5 If manager-managed, provide name of manager and percent of ownership: Name Ownership (%) Mailing Address E-Mail Address Phone No. Fax No. For all LLCs, list all members of the LLC and provide their percent of ownership: Name Ownership (%) Mailing Address E-Mail Address Phone No. Fax No. Name Ownership (%) Mailing Address E-Mail Address Phone No. Fax No. Name Ownership (%) Mailing Address E-Mail Address Phone No. Fax No. 6 Managers of manager-managed LLCs are required to execute all brownfield documents for the LLC; as to member-managed LLCs, state name of member who will sign these documents. List all parent companies, subsidiaries and other affiliates: (Use for Partnerships) Check one: General Partnership Limited Partnership List all partners and percent of ownership: Name Ownership (%) Mailing Address E-Mail Address Phone No. Fax No. Is this person a general or limited partner? Name Ownership (%) Mailing Address E-Mail Address Phone No. Fax No. Is this person a general or limited partner? List all parent companies, subsidiaries and other affiliates: 7 (Use for corporations other than LLCs) (If information is the same as shown in 1.A., please indicate “same as 1.A.” below.) Name same as 1.A. Mailing Address E-Mail Address Phone No. Fax No. List all parent companies, subsidiaries and other affiliates: Steve, please let us know if this is applicable. (Use for individuals) (If individual is the same as shown in 1.A., -please indicate “same as 1.A.” above.) Name Mailing Address E-Mail Address Phone No. Fax No. D. Does PD have or can it obtain the financial means to fully implement a brownfields agreement and assure the safe reuse of the property? (Attach supporting documentation such as letters of credit, financial statements, etc.) Answer Yes Explanation First-Citizens Bank & Trust Company (FCB) was established in 1898 and is a Federal Reserve Member and a Equal Housing Lender. FCB has total assets in an amount greater than $30 Billion and is publicly traded (Nasdaq: FCNCA). FCB is applying for the Brownfields Agreement prior to foreclosing on the C&E Manufacturing Ltd (a.k.a. as ADDCO) property located at 1600 Linville Falls Highway in Avery County, North Carolina. FCB is financially sound and has the ability to fully implement a Brownfields Agreement. 8 E. Does PD have or can it obtain the managerial means to fully implement a brownfields agreement and assure the safe use of the property? Answer Yes Explanation FCB has a strong background in financing real estate development and construction projects. In addition, FCB has retained the services of Hart & Hickman, PC (H&H) who is experienced in Brownfields redevelopment and implementation of Brownfields requirements. Collectively, FCB and H&H have significant experience with redevelopment of challenged properties, and we are aware of the requirements and restrictions that are typically included in the Brownfields Agreement to ensure successful implementation of a Brownfields Agreement and safe use of the property. F. Does PD have or can it obtain the technical means to fully implement a brownfields agreement and assure the safe use of the property? Answer Yes Explanation FCB has a wide range of engineering and environmental experience available to it. FCB has also retained H&H who have extensive experience in environmental matters in Brownfields assessment and implementation of Brownfields agreements. G. Does PD commit that it will comply (and has complied, if PD has had a prior project in the NCBP) with all applicable procedural requirements of the NCBP, including prompt payment of all statutorily required fees? Answer Yes (List all NCBP project name(s) and NCBP project ID numbers where PD or any parent company, subsidiary and other affiliate of PD has been a party to.) NA H. Does PD currently own the property? Answer No If yes, when did PD purchase the property and from whom? (Provide name, address, telephone number and email address of the contact person for the current property owner.) 9 If no, provide the name, address, telephone number and e-mail address of the contact person for the current property owner FCB holds a security interest in the property and intends to foreclose on the property in the future. The parcel is currently owned by the following entity: C & E MANUFACTURING, LTD PO BOX 187 LINVILLE NC 28646 I. If PD does not currently own the property, does PD have the property under contract to purchase? Answer No If yes, provide date of contract. If no, when does the PD intend to purchase the property (e.g., after the project is determined to be eligible for participation in the NCBP, after PD receives a draft BFA, after the conclusion of the brownfields process)? Note: the Act requires the PD to demonstrate that it intends to either buy or sell the property. FCB plans to foreclose on and take ownership of the subject property in the near future (actual date to be determined). J. Describe all activities that have taken place on the property since PD or PD’s parents, subsidiaries and/or other affiliates, and/or lessees or sublessees of PD, took ownership of or operated at the property (e.g., industrial, manufacturing or commercial activities, etc.). (Include a list of all regulated substances as defined at NCGS § 130A-310.31(b)(11) that have been used, stored on, or otherwise present at the property while those activities were conducted, and explain how they were used.) N/A. FCB has conducted certain pre-foreclosure due diligence activities including conducting Phase I and II ESA activities on the property. II. SITE INFORMATION A. Information regarding the proposed brownfields property: Proposed project name C&E Manufacturing Site acreage 5.71 street address(es) 1600 Linville Falls Highway city Linville County Avery zip 28646 10 tax ID(s) or PIN(s) 184407688011 past use(s) The subject property was undeveloped land previously utilized as a nursery prior to development of the industrial buildings on the property beginning in 1994. ADDCO Manufacturing Company, Inc. (ADDCO) has utilized the facility to manufacture automotive anti-sway bars since 1994. current use(s) The property is occupied by three industrial buildings including a 9,000-square ft manufacturing and office building (Building 1), a 14,500 square ft manufacturing/warehouse building (Building 2), and a 20,000-square ft shipping/receiving warehouse with a powder coating application area and former paint booth (Building 3). A solar farm is located in the southeastern portion of the property that was installed and is managed by Eagle Electron Power Partners (EEPP). The western portion of the site consists of undeveloped land. cause(s)/source(s) of contamination: known suspected auto anti-sway bar manufacturing activities B. Regulatory Agency Involvement: List the site names and all identifying numbers (ID No.) previously or currently assigned by any federal, state or local environmental regulatory agencies for the property. The ID No’s may include CERCLIS numbers, RCRA generator numbers for past and present operations, UST database, Division of Water Quality’s incident management database, and/or Inactive Hazardous Sites Branch inventory numbers. (In many instances, the PD will need to actively seek out this information by reading environmental site assessment reports, reviewing government files, contacting government officials, and through the use of government databases, many of which may be available over the internet.) Agency Name/ID No: Agency Name/ID No: Agency Name/ID No: Agency Name/ID No: Agency Name/ID No: C. In what way(s) is the property abandoned, idled, or underused? Upon foreclosure, the occupant will leave and the property will become vacant and thus abandoned and underutilized. The site is located within an econmically challeged area of Avery County. A new tenant and/or property owner will provide a significant public benefit to the surrounding community. D. In what way(s) is the actual or possible contamination at the property a hindrance to development or redevelopment of the property (attach any supporting documentation such as letters from lending institutions)? 11 The presence of soil and groundwater contamination identified during recent Phase II ESA activities conducted on the property is a hindrance to future development. FCB and subsequent potential tenants or buyers would be unlikely to invest in the redevelopment of the property without a Brownfields Agreement because of the potential liability issues and challenges as the result of the contamination. Before FCB acquires the property by foreclosure and offers it for reuse and redevelopment, it needs to ensure that the property will be accepted into the Brownfields Program and that future owners and occupants will have the protections and benefits afforded by a Brownfields Agreement. E. In what way(s) is the redevelopment of the property difficult or impossible without a brownfields agreement (attach any supporting documentation such as letters form lending institutions)? FCB believes that a Brownfields Agreement will be essential for the viable and safe reuse of the property. FCB's risk management strategy includes obtaining a Brownfields Agreement as part of the foreclosure process and it is unlikely that the property would be foreclosed upon and then redeveloped without a Brownfields agreement. F. What are the planned use(s) of the redeveloped brownfields property to which the PD will commit? Be as specific as specific as possible. FCB plans to foreclose on the property with the intent of either selling or leasing the property to a new industrial tenant(s). The property may require redevelopment, renovation, and/or building expansion to address the requirements of the new owner/tenant. G. Current tax value of brownfields property: $918,300 H. Estimated capital investment in redevelopment project: $Unknown at this time I. List and describe the public benefits that will result from the property’s redevelopment. Be as specific as possible. (Examples of public benefits for brownfields projects include job creation, tax base increases, revitalization of blighted areas, preserved green space, preserved historic places, improving disadvantaged neighborhood quality-of-life related retail shopping opportunities, affordable housing, environmental cleanup activities or set asides that have community or environmental benefits. In gauging public benefit, NCBP places great value upon letters of support from community groups and local government that describe anticipated improvements in quality of life for neighboring communities that the project will bring about. The inclusion of such support letters with this application is recommended and encouraged.) 1) maintain and increase the tax base, including both an increase in property tax and taxes associated with possible additional employees and increased economic activitity; 2) create additional construction opportunities to local contractors associated with property improvements; 3) provide postive economic impact to the surrounding community and businesses; 4) provide for use of existing developed properties rather than greenfields in an environmentally sensitive area; and 4) potentially spur additional development in the area resulting in a larger local tax base. 12 Special Note: Please describe all environment-friendly technologies and designs PD plans to utilize in its redevelopment strategy. For example, environment friendly redevelopment plans could include: Leadership in Energy and Environmental Design (LEED) Certification, green building materials; green landscaping techniques such as using drought resistant plants; energy efficient designs, materials, appliances, machinery, etc.; renewable sources of energy, and/or recycling/reuse of old building materials such as brick or wood. A solar farm is located in the southeastern portion of the property that was installed and is managed by Eagle Electron Power Partners (EEPP). FCB desires to maintain EEPP as a tenant on the property. As appropriate, environmentally friendly development techniques and project enhancements will be considered. J. Who will own the brownfields property when the Notice of Brownfields Property is filed with the register of deeds at the conclusion of the brownfields process? (If information is the same as 1.A. above, please indicate.) Name FCB anticpates that either it, or a to-be-formed, wholly-owned single- purpose entity will own the property at the conclusion of the Brownfields process, but it has not made a final decision at this time. Mailing Address E-Mail Address Phone No. Fax No. III. OTHER REQUIRED INFORMATION A. Brownfields Affidavit: PD must provide its certification, in the form of a signed and notarized original of the unmodified model brownfields affidavit provided by NCBP, that it did not cause or contribute to contamination at the property and that it meets all other statutory eligibility requirements. (Note: The form to use for this affidavit is attached to this application. It must be filled out signed notarized, and submitted with this application.) Is the required affidavit, as described above, included with this application? Answer Yes. Please see Exhibit A. B. Proposed Brownfields Agreement Form: PD must provide the completed form Proposed Brownfields Agreement. (Note: The form to use for this document is attached to this application. It must be filled out, initialed, and attached on your submittal.) 13 Is the required Proposed Brownfields Agreement , as described above, included with this application? Answer Yes. Please see Exhibit B. C. Location Map: PD must provide a copy of the relevant portion of the 1:24,000 scale U.S.G.S. topographic quadrangle map that shows the property clearly plotted, and that measures at least an 8 ½ by 11 inches. (Note: these maps can be purchased through the above link, or often through retail outdoor recreation stores that can print out the relevant map. Often environmental reports have location maps that use this type of map as the base for its location map.) Is the required location map included with this application? Answer Yes. Please see Exhibit C. D. Survey Plat: PD must provide a preliminary survey plat of the brownfields property with the property boundaries clearly identified, and a metes and bounds legal description that matches the property description on the plat. At this stage of the brownfields process; one or more existing survey plats from a previous property conveyance will suffice. (Before the brownfields project enters the public comment phase of the brownfields process, the PD will be required to submit a final brownfields survey plat which includes the information listed in the brownfields survey plat guidance.) Is the required preliminary survey plat included with this application? Answer Survey Plat is not available. Please see the Property Deed Legal Description in Exhibit D. E. Site Photographs: PD must provide at least one pre-redevelopment photograph of the property, in either hard copy or electronic format that shows existing facilities and structures. Please note that the NCBP prefers to have electronic photos instead of or in addition to hard copies. Electronic copies of photographs should be emailed to: Shirley.Liggins@ncdenr.gov with a clear indication as to which Brownfields Application they apply to. Are photographs of the property included with this application? Answer Yes. Please see Exhibit E. Have electronic copies of the photographs been emailed to NCBP? Answer Yes. F. Environmental Reports/Data: If it makes an affirmative eligibility determination, the NCBP will request that PD provide any and all existing environmental reports and data for the property on CD only. The brownfields process may be expedited if PD submits such reports/data with this application. Are any environmental reports/data being submitted with this application? Answer Yes. Please see the disc attached as Appendix F. 14 If environmental reports/data are being submitted with this application, please provide the title, date and author of each item being submitted: Phase I ESA, ADDCO Facility, 1600 Linville Falls Highway, Newland (also listed as Linville), NC prepared by Hart & Hickman, PC dated August 25, 2014; Phase II ESA, ADDCO Facility, 1600 Linville Falls Highway, Newland (also listed as Linville), NC prepared by Hart & Hickman, PC dated November 18, 2014; and Additional Phase II ESA, C&E Manufacturing (a.k.a. ADDCO) Facility, 1600 Linville Falls Highway, Newland (also listed as Linville), NC prepared by Hart & Hickman, PC dated January 27, 2015 IV. ADDITIONAL REQUIRED FORMS The following forms are to be filled out and submitted with the application including the Responsibility and Compliance Affidavit and the Proposed Brownfields Agreement. Submittal of the Affidavit requires signature and notarization, and the Proposed Brownfields Application requires an initial. Appendix A NCDENR Affidavit Appendix B Preliminary Proposed Brownfields Agreement 16 Preliminary Proposed Brownfields Agreement I. Property Facts a. Property Address(es): 1600 Linville Falls Highway, Linville, NC 28646 b. Property Seller: C&E Manfacturing Ltd. c. Property Buyer: FCB (taking ownership via property foreclosure) d. Brief Property Usage History: The subject property was undeveloped land previously utilized as a nursery prior to development of the industrial buildings on the property beginning in 1994. ADDCO Manufacturing Company, Inc. (ADDCO) has utilized the facility to manufacture automotive anti-sway bars since 1994. The solar farm located in the southeastern portion of the site was developed on the property in 2010. e. The planned reuse will potentially involve the following use classification(s) (check all that apply): School/childcare/senior care Residential Commercial, retail (specify) Other commercial (specify) Office Light industrial Heavy industrial Recreational Open space Other (specify) II. Contaminant Information a. The contaminant situation at the property is best described by the following (check all that apply): Contaminants are from an on-property source(s) Contaminants are from an off-property source(s) Contaminants are from an unknown source(s) Contaminants have not yet been documented on the property 17 b. Contaminated Media Table. (If known, check appropriate boxes below) Contaminant Types Soil Groundwater and/or Surface Water Private Wells Vapor Intrusion known Suspected known Suspected known suspected known suspected o rg a ni c s Chlorinated Solvents (list): Petroleum: ASTs USTs Other X X Other (list): i n or g an i cs Metals (list): X X (on- site) Other (list): III. Protective Measures I am prepared to take steps necessary to make the property suitable for its planned uses while fully protecting public health and the environment. I propose that NCBP consider a brownfields agreement that will make the property suitable for the planned use(s) through the following mechanism(s) (check all that apply): Contaminant remediation to risk-based levels. Engineered Controls (e.g., low permeability caps, vapor mitigation systems, etc) Land use restrictions that run with the land that will restrict or prohibit uses that are unacceptable from a risk assessment/management perspective. (Important Note: In any Appendix C Site Location Map TITLE PROJECT SITE LOCATION MAP ADDCO FACILITY NEWLAND, NORTH CAROLINA DATE: JOB NO: REVISION NO: FIGURE NO: 8-20-14 0 1FCB-014 0 2000 4000 APPROXIMATE SCALE IN FEETN U.S.G.S. QUADRANGLE MAP QUADRANGLE 7.5 MINUTE SERIES (TOPOGRAPHIC) NEWLAND, NC 1994 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) SITE Appendix D Property Deed Legal Description Appendix E Site Photographs Photograph 2: Building 2 located in the central portion of the site. FC B -01 4 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 1: Building 1 located in the northern portion of the site. ADDCO FACILITY NEWLAND, NORTH CAROLINA Photograph 4: Solar farm located in the southeastern portion of the site. 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 3: Building 3 located in the southern portion of the site. FC B -01 4 ADDCO FACILITY NEWLAND, NORTH CAROLINA Appendix F Previous Environmental Reports Phase I ESA ADDCO Facility 1600 Linville Falls Highway Newland, North Carolina H&H Job No. FCB-014 August 25, 2014 Phase I Environmental Site Assessment ADDCO Facility 1600 Linville Falls Highway Newland, North Carolina H&H Job No. FCB-014 Table of Contents 1.0 Executive Summary ................................................................................................................1 1.1 Property Summary .................................................................................................................1 1.2 Findings, Opinions, and Conclusions ....................................................................................2 2.0 Introduction .............................................................................................................................5 2.1 Purpose and Scope of Services ..............................................................................................5 2.2 Methodology ..........................................................................................................................5 2.3 Limitations and Exceptions of Assessment ...........................................................................6 2.4 Special Terms and Conditions ...............................................................................................6 2.5 Data Gaps ..............................................................................................................................7 3.0 Site and Area Description ......................................................................................................8 3.1 General Site Description and Use ..........................................................................................8 3.2 Site Structures and Improvements .........................................................................................8 3.3 Property Owner, Manager, and Occupant..............................................................................9 3.4 Vicinity Characteristics .........................................................................................................9 3.5 Physical Setting ...................................................................................................................10 4.0 Records Review .....................................................................................................................12 4.1 Standard Environmental Record Sources – Federal, State and Local .................................12 4.2 Regulatory Agency File and Records Review .....................................................................13 4.3 Interviews ............................................................................................................................13 4.4 Historical Use Information ..................................................................................................14 5.0 Site Reconnaissance ..............................................................................................................16 5.1 Hazardous Substances .........................................................................................................16 5.2 Storage Tanks, Drains, and Sumps ......................................................................................18 5.3 Water and Wastewater Issues ..............................................................................................19 i S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc 5.4 Indications of PCBs .............................................................................................................19 5.5 Indications of Waste Disposal .............................................................................................20 5.6 Surface Conditions ..............................................................................................................20 5.7 Stormwater and Flood Information .....................................................................................21 6.0 Signatures of Environmental Professionals ........................................................................22 7.0 Qualifications of Environmental Professionals Conducting the Phase I ESA ................23 List of Figures Figure 1 Site Location Map Figure 2 Site Map List of Appendices Appendix A User Questionnaire Appendix B Avery County Tax Information Appendix C EDR Reports Appendix D Safety Data Sheets Appendix E Site Photographs Appendix F Curriculum Vitae ii S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc Phase I Environmental Site Assessment ADDCO Facility 1600 Linville Falls Highway Newland, North Carolina H&H Job No. FCB-014 1.0 Executive Summary Hart & Hickman, PC (H&H) has performed a Phase I Environmental Site Assessment (ESA) in conformance with the scope and limitations of ASTM Practice E 1527-13 on the property located at 1600 Linville Falls Highway in Newland, Avery County, North Carolina. Any exceptions to, or deletions from, this practice are described in this report. 1.1 Property Summary H&H has provided a brief summary of the current and former uses of the site and nearby area below: Subject Site • The subject property is developed as an industrial manufacturing facility and consists of an approximately 5.71 acre parcel of land. The property is occupied by three industrial buildings including a 9,000-square ft manufacturing and office building (Building 1), a 14,500 square ft manufacturing/warehouse building (Building 2), and a 20,000-square ft shipping/receiving warehouse with a powder coating application area and former paint booth (Building 3). A solar farm is located in the southeastern portion of the property that was installed and is managed by Eagle Electron Power Partners (EEPP). The western portion of the site consists of undeveloped land. • The subject property was undeveloped and land utilized as a nursery prior to development of the industrial buildings on the property beginning in 1994. ADDCO Manufacturing Company, Inc. (ADDCO) has utilized the facility to manufacture automotive anti-sway 1 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc bars since 1994. The solar farm located in the southeastern portion of the site was developed on the property in 2010. Nearby Area • Properties surrounding the subject site include Stor-All Mini-Storage (1438 Linville Falls Highway) to the north; Linville Falls Highway to the east with residences located beyond; a driveway access to Camp Carmel to the south with Classic Stone Works (1710 Linville Falls Highway) located beyond; and undeveloped wooded land to the west. • Surrounding properties have historically been residential, agricultural, or undeveloped wooded land since the 1970s. Development of commercial and industrial properties began along Linville Falls Highway in the 1980s/1990s. 1.2 Findings, Opinions, and Conclusions The purpose of a Phase I ESA is to identify Recognized Environmental Conditions (RECs) in connection with the property. RECs are environmental conditions that include the presence or likely presence of hazardous substances or petroleum products on the property that indicate an existing release, a past release, or a material threat of a release in structures on the property, or into the ground, groundwater, or surface water on the property. Our findings regarding RECs are based upon our review of historical records and maps; review of regulatory database records and/or regulatory agency files; interviews with persons familiar with the property; observations during the site reconnaissance; and data evaluation. Based upon our completion of Phase I ESA activities, H&H has determined the following: This assessment has revealed no evidence of recognized environmental conditions (RECs) in connection with the property except for the following: 2 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc • ADDCO employees apply a powder coating to metal anti-sway bars and other components within an application booth/oven located in the southwestern portion of Building 3. During our inspection, H&H identified black powder coating material on the concrete floor of the powder coating application area and throughout the southwestern portion of Building 3. According to the Safety Data Sheet (SDS), the coating material contains barium sulfate, titanium dioxide, and benzothiazole-2-thiol. H&H also identified black powder coating to the tile-covered floor, floor drain, and within an industrial sink located in a men’s restroom in Building 3. The restroom’s floor drain and sink are connected and convey fluids to a septic tank and septic field system located west and southwest of Building 3, respectively. H&H identified oil stains to an industrial sink located within the office/warehouse Building 1. Site contact Mr. de Marcellus indicated the staining was likely from gear lube, oil, or grease removed during hand washing and possibly parts cleaning activities. The sink drains into a septic tank located adjacent and south of the building and eventually into a septic field located in the southwestern portion of the site. ADDCO employees previously applied paint to various metal parts within a paint booth located in the northwestern portion of Building 3. Mr. de Marcellus reported that water and paint thinner were used to clean paint from sprayers and it appears that paint equipment may have been washed in an industrial sink located in Building 3. H&H identified black paint stains to the concrete floor of the paint booth and to the exterior wall of Building 3 beneath an exterior vent for the former paint booth. H&H did not observe obvious evidence of paint stains to the ground surface below the former paint booth vent. H&H considers the potential discharge of powder coating materials, oil, waste oil, paint, and paint thinner generated during manufacturing activities at the site into the facility septic system to be a REC. 3 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc The following potential environmental concerns (PECs) were identified in connection with the subject property which, based upon our evaluation, are not RECs. • During our site inspection, H&H identified multiple oil stains to the concrete floor in Buildings 1 and 2 below metal cutting and fabrication machinery. Most of the oil stains appeared to be small (< 3 square ft) and appeared to be contained within the building. However, H&H identified three holes in the concrete floor within Building 2 where it appears that the oil from nearby machinery has migrated below the concrete floor to impact underlying soil. H&H probed the soil below the oil stains within the three holes and it appears that the oil stains extends to a depth of approximately 2 inches below the ground surface. H&H considers the oil stains to be a de minimis condition in accordance to the ASTM E 1527-13 Standard. Based on this information, the potential for impact to the subject site appears low, and H&H does not consider the oil stained soil to be a REC. • H&H identified a buried propane UST located south of Building 1 that supplies fuel to power the facility’s fork lifts and to heat the Buildings 1 and 2. Building 3 is heated with natural gas. H&H did not observe gas like odors in the vicinity of the buried propane UST indicative of a propane gas release. Based on this information, the potential for impact to the subject site appears low, and H&H does not consider the buried propane UST to be a REC. • H&H identified an exterior vent hose that discharges powder coating material from the powder coat application booth to the ground surface located near the southwestern corner of Building 3. H&H did not observe obvious evidence of powder coating to the ground surface below the discharge hose. Based on this information, the potential for impact to the subject site appears low, and H&H does not consider the exterior vent hose from the powder coating application area to be a REC. 4 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc 2.0 Introduction This report presents the results of a Phase I ESA conducted on ADDCO facility located at 1600 Linville Falls Highway in Newland, Avery County, North Carolina. H&H conducted this assessment for First Citizens Bank (FCB) in accordance with our authorized scope of work. 2.1 Purpose and Scope of Services The purpose of this assessment was to identify, to the extent feasible pursuant to the processes prescribed herein, recognized environmental conditions in connection with the property. Such environmental conditions include the presence or likely presence of any hazardous substances or petroleum products in, on, or at the property: (1) due to release to the environment; (2) under conditions indicative of a release to the environment; or (3) under conditions that pose a material threat of a future release to the environment. ‘Release’ shall have the same meaning as the definition of ‘release’ as defined in CERCLA 42 U.S.C. § 9601(22) and ‘environment’ shall have the same meaning as the definition of ‘environment’ as defined in CERCLA 42 U.S.C.§ 9601(8). In this assessment, ‘migrate’ and ‘migration’ refers to the movement of hazardous substances or petroleum products in any form, including, for example, solid and liquid at the surface or subsurface, and vapor in the subsurface. 2.2 Methodology H&H performed this Phase I ESA in general conformance with current ASTM Standard E 1527- 13, Standard Practice for ESAs: Phase I Environmental Site Assessment Process. The Phase I ESA is also compliant with the statutory criteria for all appropriate inquiries currently accepted by the United States Environmental Protection Agency under ASTM Standard 1527-13. The scope of services for the Phase I ESA includes the following tasks: 5 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc • Acquisition and Review of Data on Historical Use of the Property; • Site Reconnaissance, Review of Adjacent Properties, and Interviews with Knowledgeable Individuals; • Review of Environmental Databases; • Contacts with Regulatory Officials, as Appropriate; and • Data Analysis and Reporting. 2.3 Limitations and Exceptions of Assessment The following items were beyond the scope of this assessment, and H&H did not address them in this report: • cultural, historical, and archaeological sites survey • radon and indoor air testing • responsibilities of the User of this Phase I ESA to meet all appropriate inquiry as defined in ASTM E1527-13 • asbestos, mold, or lead-based paint survey • drinking water testing • rare and endangered species survey • wetlands verification/delineation The User of this Phase I ESA has certain responsibilities to meet all appropriate inquiry as defined in ASTM E1527-13. H&H provided a User Questionnaire to Mr. Steve Pollok of FCB to in part address the User’s responsibilities. H&H has provided a copy of the completed User Questionnaire in Appendix A. 2.4 Special Terms and Conditions The conclusions presented in this report are professional opinions, based solely upon visual observations of the site and vicinity and our interpretation of the available historical information, 6 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc documents reviewed, and analytical results as described in this report. They are intended exclusively for the purpose outlined herein and at the site location and the project indicated. This report is intended for the sole use of FCB. The report may not be relied upon by other parties without the express written consent of H&H and FCB. The scope of services performed in execution of this investigation may not be appropriate to satisfy the needs of other users, and any use or re-use of this document or the findings, conclusions, or recommendations presented herein is at the sole risk of said user. It should be recognized that this study was not intended to be a definitive investigation of contamination at the subject property. It is possible that currently unrecognized contamination may exist at the site. Opinions and recommendations presented herein apply to site conditions existing at the time of our investigation and those reasonably foreseeable. They necessarily cannot apply to site changes of which H&H is unaware and has not had the opportunity to evaluate. 2.5 Data Gaps H&H identified the following data gap during our Phase I ESA activities: • Details about the early history of the property prior to the 1970s are unknown. This lack of information is considered to be a data gap in accordance with ASTM 1527-13. However, information obtained during the Phase I ESA indicates that the site was primarily undeveloped wooded land or land utilized as a nursery prior to development in 1998 and this limitation is not expected to significantly alter the findings of this investigation. Additionally, if the agricultural chemicals were used during operation as nursery in accordance with manufacturer recommendations, the potential for this data gap to affect the conclusions in this report is low. 7 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc 3.0 Site and Area Description 3.1 General Site Description and Use A general site description and the property use are noted below: Site Description: industrial manufacturing facility and solar farm Site Address: 1600 Linville Falls Highway, Newland, Avery Co., NC Parcel Size: 5.71 acres The property is occupied by ADDCO Manufacturing Company, Inc. (ADDCO) to manufacture automotive anti-sway bars and associated components. A solar farm is located in the southeastern portion of the property and the western portion of the site consists of undeveloped land. 3.2 Site Structures and Improvements Structures and improvements identified on the property include the following: Building: Building 1 – manufacturing and office/warehouse (9,000 square ft) built in 1994 Building 2 - manufacturing/warehouse (14,500 square ft) built in 1999 Building 3 – shipping/receiving warehouse with powder coating application area and former paint booth (22,000 square ft) built in 2001 The property is occupied by three industrial buildings including a 9,000-square ft manufacturing and office building (Building 1), a 14,500 square ft manufacturing/warehouse building (Building 2), and a 20,000-square ft shipping/receiving warehouse with a powder coating application area and former paint booth (Building 3). A solar farm is located in the southeastern portion of the property that was installed and is managed by Eagle Electron Power Partners (EEPP). The western portion of the site consists of undeveloped land. 8 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc Other Improvements: loading docks gravel-paved driveway and parking lot solar farm surrounded by a chain-linked fence concrete pavement Utilities: municipal water – not available sanitary sewage – not available electricity – Mountain Electric Co-op natural gas – Piedmont Natural Gas 3.3 Property Owner, Manager, and Occupant Based upon our site visit and a review of the Avery County tax record, H&H identified the following property owner and site occupant associated with the subject property: Property Owner: C&E Manufacturing Ltd Parcel ID #: 184407688011 (see Appendix B) Property Contact: Mr. Edmond (Ed) de Marcellus (ADDCO) ADDCO manufactures automotive anti-sway bars and associated components. Manufacturing activities include cutting, welding, bending, sanding, painting (previously), and powder coating metal parts. H&H interviewed Mr. de Marcellus during our site visit to obtain information regarding site history and current operations. A summary of our interview with Mr. de Marcellus is presented in Section 4.2 and is included throughout the Phase I ESA report. 3.4 Vicinity Characteristics The table below summarizes properties that surround the subject properties. Location Property Description North Stor-All Mini Storage (1438 Linville Falls Highway) East Linville Falls Highway with residences located beyond South a driveway access to Camp Carmel with Classic Stone Works (1710 Linville Falls Highway) located beyond West undeveloped wooded land 9 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc None of the properties surrounding the subject site are identified on environmental databases in the EDR report (see Section 4.1). 3.5 Physical Setting The subject property’s physical setting is presented as follows: Topography 7.5-Minute Topographic Map: Newland, NC (dated 1994) Site Elevation: 3,600 ft above mean sea level Topographic Gradient: south The topographic gradient in the area of the subject site is in a generally southerly direction toward the Linville River located approximately 0.4-mile south of the subject site. A copy of the USGS topographic quadrangle map is provided as Figure 1. Geology Avery County, including the subject property, is located within the Blue Ridge physiographic province of North Carolina. This province is a northeast trending zone extending from Georgia through Virginia and ranges in width from approximately 15 to 55 miles in North Carolina. The Blue Ridge is a deeply dissected mountainous area of numerous steep mountain ridges, intermontane basins, and trench valleys that intersect at all angles and give the area its rugged mountain character. The site is located within the Grandfather Mountain window of the Blue Ridge province which is characterized by bedrock composed of meta-sedimetary and meta-volcanic rocks. Based on the 1985 Geologic Map of North Carolina, the bedrock underlying the subject property is composed of greenstone and met-arkose with interlayered sedimentary rocks. 10 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc Overlying the bedrock in many areas is a zone of residual soil or saprolite which is developed from the in-situ weathering of the underlying rocks. The saprolite is typically composed of unconsolidated silts, clays, sand, and rock fragments. Groundwater generally occurs under water table conditions within the interconnected saprolite and bedrock zones. The primary source of ground water in the area is from precipitation that reaches the water table through infiltration. The saprolite is generally considered to be a recharge medium for the bedrock aquifer because it holds precipitation and allows ground water to gradually infiltrate into the bedrock joints, faults, and fractures. Groundwater flow is typically from upland areas to lowland areas where ground water discharges to streams. 11 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc 4.0 Records Review 4.1 Standard Environmental Record Sources – Federal, State and Local H&H utilized Environmental Data Resources Inc. (EDR), an environmental database search service, for a cursory review of Federal and State regulatory database files regarding regulated sites within the ASTM-specified search radii. Federal, state, local, tribal, and EDR proprietary databases were searched by EDR on July 29, 2014. The EDR Report is included in Appendix C. Upon our review of the EDR report, H&H identified and summarized the following information pertaining to the subject property, off-site properties, and unmappable orphan properties. Subject Site The subject property is not listed in any of the databases searched by EDR. Off-Site Properties EDR did not identify Federal, State, Local, Tribal, and/or EDR Proprietary database listings for off-site properties in the general vicinity of the subject site. Unmappable Properties H&H reviewed a list of unmappable sites presented in the EDR database report. Unmappable sites do not contain sufficient address information in the environmental databases to plot them on a map. H&H reviewed the area near the subject property for these unmappable sites. Based on the limited information in the EDR report, H&H was unable to locate the listed sites near the subject property. 12 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc 4.2 Regulatory Agency File and Records Review DENR File Review H&H attempted to review regulatory documents on the North Carolina Department of Environment and Natural Resources (DENR) CARA³ web-portal. H&H could not locate documents on the portal related to the ADDCO facility. 4.3 Interviews Fire Department Interview Fire Department Contact: Mr. Garrett Stonesifer Linville Volunteer Fire Department H&H contacted Mr. Garrett Stonesifer and requested information regarding fire department responses to the subject property. Mr. Stonesifer reported that he was not aware of any environmental issues or responses by the fire department to the subject property. Site Contact Interviews H&H interviewed ADCCO Plant Manager Mr. Ed de Marcellus during the Phase I ESA site visit. Mr. de Marcellus reported that he and his father managed the facility from 1998 until the present. Mr. de Marcellus reported that the facility generates a small amount of waste oil from machinery service activities. He stated that ADDCO does not generate significant amounts of potentially hazardous waste during manufacturing activities and is not listed as a Resource Conservation and Recovery Act (RCRA) hazardous waste generator. Mr. de Marcellus reported that ADDCO utilizes hydraulic oil, gear lube oil, cutting/coolant oil, powder coating, and other lubricants as part of their operations. He reported that ADDCO previously (but no longer) operates a paint booth in Building 3. Mr. de Marcellus reported that he is not aware of any additional hazardous material spills or other environmental issues associated with subject property. Copies of Safety Data Sheets (SDS) for oils, lubricants, and powder coatings utilized at the ADDCO facility are included in Appendix D. 13 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc 4.4 Historical Use Information Aerial Photographs H&H utilized EDR’s Aerial Photo Decade Package for historical aerial photographs of the subject property and surrounding area. A review of the provided aerial photographs to identify past site usage is provided in the following table. The Aerial Photo Decade Package is included in Appendix C. Year Scale Subject Property Surrounding Property 1976 1”=1,000’ undeveloped wooded and agricultural land undeveloped wooded and agricultural land; residence is visible across Linville Falls Highway and east of the site 1994 1”=500’ undeveloped wooded land undeveloped wooded and agricultural land are visible to the south and west; residences are visible to the east and across Linville Falls Highway; two storage buildings are visible north of the site 1998 1” = 750’ office/warehouse building is visible in the northern portion of the site similar to the 1994 aerial photograph 2005 1”=500’ office/warehouse building and two industrial warehouses are visible on the property industrial warehouse is visible to the south 2006 1”=500’ similar to the 2005 aerial photograph similar to the 2005 aerial photograph 2008 1”=500’ similar to the 2006 aerial photograph similar to the 2006 aerial photograph 2009 1”=500’ similar to the 2008 aerial photograph self-storage storage facility and industrial warehouse expanded to the north and south of the site, respectively 2010 1”=500’ similar to the 2009 aerial photograph similar to the 2009 aerial photograph 2012 1”=500’ solar farm is visible in the southeastern portion of the site similar to the aerial photograph 14 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc Sanborn Fire Insurance Maps Sanborn Fire Insurance Map coverage: no coverage (source – EDR Certified Sanborn Map report, Appendix C) City Directories City and Cross Reference Directory coverage: 1999 to 2013 (source – EDR City Directory Image Report in Appendix C) The subject site is identified at the address 1596 Linville Falls Highway in the 1999 City Directory and Classic Stone Works, Inc. (adjacent property to the south) is identified in the 2013 City Directory at the address 1710 Linville Falls Highway. User Questionnaire User Questionnaire completed by: Mr. Steve Pollok (FCB) H&H submitted a User Questionnaire to Mr. Pollok to complete. Mr. Pollok indicated that the User is not aware of environmental cleanup liens, activity or use limitations related to contamination, discounted purchase price related to contamination, spills or environmental cleanup on the property, or indications of the presence or likely presence of contamination. H&H has included a copy of the completed User Questionnaire in Appendix A. Historical Use Summary The subject property was undeveloped and occupied by a nursery prior to development of the industrial buildings on the property beginning in 1994. ADDCO has utilized the facility to manufacture anti-sway bars since 1994. The solar farm located in the southeastern portion of the site was developed on the property in 2010. Surrounding properties have historically been residential, agricultural, or undeveloped wooded land since the 1970s. Development of commercial and industrial properties began along Linville Falls Highway in the 1980s/1990s. 15 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc 5.0 Site Reconnaissance Mr. Jay Quattrocchi of H&H conducted a visual reconnaissance of the subject site on July 31, 2014. The weather conditions at the time of the site visit were overcast with temperatures in the 70s °F. General images of the subject property are included as Photographs 1 through 4. H&H has included site photographs in Appendix E. 5.1 Hazardous Substances As mentioned previously, ADDCO manufactures automotive metal anti-sway bars and associated components (Photograph 5). Manufacturing activities include cutting, welding, bending, tooling, painting, and powder coating of metal parts. H&H interviewed Mr. Ed de Marcellus during our site visit to obtain information regarding site history and current operations. Mr. de Marcellus reported that the facility utilizes hydraulic oil, gear lube oil, cutting/coolant oil, powder coating, and other lubricants as part of their operations. He reported that ADDCO previously (but no longer) operates a paint booth in Building 3. A summary of our observations regarding the use of potentially hazardous substances is presented below. Oil/Waste Oil Mr. de Marcellus reported that the facility generates a small amount of waste oil during machine maintenance but does not generate significant amounts of potentially hazardous waste during manufacturing activities, and is not listed as a RCRA hazardous waste generator. Mr. de Marcellus reported that waste oils are collected in 55-gallon drums and are staged indoors within the warehouse prior to transport and disposal by Safety-Kleen on a routine basis (Photograph 6). H&H also identified two 55-gallon waste oil drums staged outdoors between Buildings 2 and 3. H&H did not observe evidence of staining or unusually stressed vegetation to the ground surface below the drums (Photograph 7). During our site inspection, H&H identified multiple oil stains to the concrete floor in Buildings 1 and 2 below metal cutting and fabrication machinery. Most of the oil stains appeared to be small 16 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc (< 3 square ft) and appeared to be contained within the building. However, H&H identified three holes in the concrete floor within Building 2 where it appears that the oil from nearby machinery has migrated below the concrete floor to impact underlying soil (Photographs 8 and 9). H&H probed the soil below the oil stains within the three holes and it appears that the oil stains extends to a depth of approximately 2 inches below the ground surface. H&H identified oil stains to an industrial sink located within the office/warehouse Building 1 (Photograph 10). Site contact Mr. de Marcellus indicated the staining was likely from gear lube, oil, or grease removed during hand washing and possibly parts cleaning activities. The sink drains into a septic tank located adjacent and south of the building and eventually into a septic field located in the southwestern portion of the site. Powder Coating ADDCO employees apply a powder coating to metal sway bars and other components within an application booth/oven located in the southwestern portion of Building 3 (Photograph 11). During our inspection, H&H identified black powder coating material on the concrete floor of the powder coating application area and throughout the southwestern portion of Building 3. According to the Safety Data Sheet (SDS), the coating material contains barium sulfate, titanium dioxide, and benzothiazole-2-thiol. H&H also identified black powder coating to the tile-covered floor, floor drain (Photograph 12), and within an industrial sink located in a men’s restroom in Building 3 (Photograph 13). The restroom’s floor drain and sink are connected and convey fluids to a septic tank and septic field system located west and southwest of Building 3, respectively. H&H identified an exterior vent hose that discharges powder coating material from the powder coat application booth to the ground surface located near the southwestern corner of Building 3 (Photograph 14). H&H did not observe obvious evidence of powder coating to the ground surface below the discharge hose. 17 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc Paint Booth ADDCO employees previously applied paint to various metal parts within a paint booth located in the northwestern portion of Building 3 (Photograph 15). Mr. de Marcellus reported that water and paint thinner were used to clean paint from sprayers. H&H identified black paint stains to the concrete floor of the paint booth and to the exterior wall of Building 3 beneath an exterior vent for the former paint booth. H&H did not observe obvious evidence of paint stains to the ground surface below the former paint booth vent. 5.2 Storage Tanks, Drains, and Sumps During our site visit, H&H visually assessed the subject site for the presence of storage tanks and sumps. A summary of our assessment is presented below. Underground Storage Tanks (USTs): one propane UST Aboveground Storage Tanks (ASTs): none observed or reported Sumps: two septic tanks (see Section 5.3) H&H identified a buried propane UST located south of Building 1 that supplies fuel to power the facility’s fork lifts and to heat the Buildings 1 and 2 (Photograph 16). Building 3 is heated with natural gas. H&H did not observe gas like odors in the vicinity of the buried propane UST indicative of a propane gas release. Wastewater derived from the facility restrooms, floor drains, and industrial sinks discharge into the two septic tanks located south of Building 1 and west of Building 3. Wastewater from the septic tanks discharge into a septic field located in the southwestern portion of the property. Additional information regarding the potential for a release to the facility’s septic systems is presented in Section 5.1. 18 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc 5.3 Water and Wastewater Issues Water and wastewater use is summarized below. Water Municipal Water: not available Water Supply Wells: water supply well located north of Building 1 Wastewater Sanitary Sewage: not available Septic Systems: two septic tanks A water supply well located north of the Building 1 reportedly supplies potable water to the facility. Mr. de Marcellus reported no issues associated with water quality from the on-site well. Mr. de Marcellus reported that the facility discharges domestic wastewater into two septic systems located south of the office/warehouse and in the southwestern portion of the site (Photographs 17 and 18). H&H identified evidence of oil stains and of powder coating material to sinks and floor drains within the site buildings indicative of a potential release to facility’s septic system. The oil stains and powder coating materials are discussed further in Section 5.1. 5.4 Indications of PCBs Polychlorinated biphenyls (PCBs) are sometimes found in mineral oils used in electrical equipment including transformers. PCBs are a potential environmental contaminant. Transformers: three pad-mounted transformers two pole mounted transformers Transformers Owner: Mountain Electric Co-op 19 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc H&H identified three pad-mounted transformers located south of Building 1 and east of Building 3, and two pole mounted transformers located in the northeastern portion of the property (Photograph 19). H&H did not observe evidence of staining to the concrete pads or to the ground surface below the transformers. The transformers identified on the property appeared to be in good condition with no evidence of a release. The transformers are the responsibility of Mountain Electric and the landowner is not responsible for leaks or spills from the transformers. 5.5 Indications of Waste Disposal Indications of waste disposal are summarized below: Waste Containers: one dumpster Debris Piles: scrap wood H&H identified a dumpster on the subject site located between Buildings 2 and 3 that contained office trash, household items, and food containers (Photograph 20). H&H did not observe evidence of significant staining on the ground surface below the dumpster. H&H identified scrap wood located in the southwestern portion of the site (Photograph 21). The wood debris does not appear to pose an environmental risk to the subject site. H&H also identified an abandoned automobile located southwest of Building 3 (Photograph 22). H&H did not observe evidence of staining to the ground surface below the vehicle indicative of a significant environmental release. 5.6 Surface Conditions During our reconnaissance of the subject property, H&H identified the following surface conditions: 20 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc Interior Surface Conditions: concrete floor (warehouses) carpet (offices) floor tile (restrooms and break room) Exterior Surface conditions: gravel parking areas driveways concrete sidewalks and break area undeveloped wood land solar farm As mentioned previously, H&H identified oil stains and powder coating to the concrete floor in the manufacturing areas in the buildings. The stained areas are discussed further in Section 5.1. H&H did not observe other evidence of stained areas, or of disturbed soil, stressed vegetation, mounds, pits, or depressions during our reconnaissance of the rest of the property. H&H did not observe obvious potential environmental issues associated with the solar farm developed in the southeastern portion of the site. 5.7 Stormwater and Flood Information The following is a summary of stormwater and flood information: Stormwater Stormwater from the property flows across the site in a generally southeasterly direction and into drainage swales located along Linville Falls Highway. H&H did not observe obvious environmental concerns associated with the stormwater. Flood Information FEMA Flood Insurance Rate Map (FIRM): Community Panel # 3710183300J (map dated December 2, 2008) The FEMA map indicates that the subject property is not located with the 100- or 500-year flood zones. 21 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc 6.0 Signatures of Environmental Professionals I declare that, to the best of my professional knowledge and belief, I meet the definition of Environmental Professional as defined in Section 312.10 of 40 CFR 312, and I have the specific qualifications based on education, training, and experience to assess a property of the nature, history, and setting of the subject property. I have developed and performed the all appropriate inquiries in conformance with the standards and practices set forth for the environmental professional in 40 CFR Part 312. Environmental Professional: ___ Jay Quattrocchi Environmental Scientist Reviewed by: ___________________________________ Matt Ingalls Project Manager 22 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc 7.0 Qualifications of Environmental Professionals Conducting the Phase I ESA Environmental Professional Jay Quattrocchi, Environmental Scientist, over has 7 years of experience in the environmental consulting industry. Mr. Quattrocchi is currently serving as an Environmental Scientist at H&H performing Phase I ESAs and wetland and stream delineations. He also has experience performing water quality sampling and NPDES inspections. Reviewed by: Matthew J. Ingalls, Project Manager, has over 20 years of experience in environmental site assessments, wetland, stream, asbestos and lead projects. Mr. Ingalls is a certified asbestos building inspector and management planner. Resumes for the above personnel are included in Appendix F. 23 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase I ESA Report\Linville Falls Rd - Phase I ESA.doc TITLE PROJECT SITE LOCATION MAP ADDCO FACILITY NEWLAND, NORTH CAROLINA DATE: JOB NO: REVISION NO: FIGURE NO: 8-20-14 0 1FCB-014 0 2000 4000 APPROXIMATE SCALE IN FEETN U.S.G.S. QUADRANGLE MAP QUADRANGLE 7.5 MINUTE SERIES (TOPOGRAPHIC) NEWLAND, NC 1994 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) SITE SITE MAP ADDCO FACLITY NEWLAND, NORTH CAROLINA DATE: JOB NO: REVISION NO: FIGURE NO: 08/20/2014 0 2FCB-0140200400 APPROXIMATE SCALE IN FEET N 2923 S. Tryon Street, Suite 100Charlotte, NC 28203704.586.0007(p) 704.586.0373(f) Note -Aerial Photograph base map obtained from GoogleEarth and dated November 2013 Pad Transformer Pole Transformer Building 1 Building 2 Building 3 Solar Farm Residences Stor-All Mini Storage (1438 Linville Falls Hwy) Classic Stone Works (1710 Linville Falls Hwy) Undeveloped Land Septic Field Septic Tank Septic Tank Powder Coating Area Former Paint Booth Propane UST Holes in Concrete Floor Dumpster Abandoned Car Scrap Wood Pile Water Supply Well Appendix A User Questionnaire Appendix B Avery County Tax Information 0 150 300ft Avery County, NC Disclaimer:The information contained on this page is taken from aerial mapping, tax mapping, and public records and is NOT to be construed or used as a survey or 'legal description'. Only a licensed professional land surveyor can legally determine precise locations, elevations, length and direction of a line, and areas. C&E Manufacturing Parcels Attributes at point: N: 847970, E: 1146761 http://www.webgis.net Anderson & Associates, Inc. http://www.andassoc.com init: start init: done Parcel Number:184407688011 Account Number:49611 Deed Date:20070518 Acreage:6.430AC Owner Name:C & E MANUFACTURING, LTD Additional Info:1600 LINVILLE FALLS HWY Mailing Addr2:PO BOX 187 Mailing City:LINVILLE Mailing State:NC Mailing Zip:286460000 House Number:1600 Street Name:LINVILLE FALLS Street Type:HWY Bldg Value:751800 Land Value:166500 Total Value:918300 Approved By:1 Year Built:1995 Fire Department:0 Township Code:5 MNBH Number:504 Deed Book:414 Deed Page:1663 Size:6.43 Units:Acres Acres (measured):5.714 Census Tracts (2000) STCNTRBG: 370119902 4 Townships Township: Linville Page 1 of 1Avery County, NC Print Map 7/29/2014http://arcgis.webgis.net/nc/avery/printable.asp Appendix C EDR Reports • The EDR Radius Map Report with GeoCheck • The EDR Aerial Photo Decade Package • The EDR Certified Sanborn Map Report • The EDR City Directory Report FORM-LBD-CCA ®kcehCoeG htiw tropeR ™paM suidaR RDE ehT 6 Armstrong Road, 4th floor Shelton, CT 06484 Toll Free: 800.352.0050 www.edrnet.com C&E Manufacturing 1600 Linville Falls Highway Newland, NC 28657 Inquiry Number: 4020675.2s July 29, 2014 SECTION PAGE Executive Summary ES1 Overview Map 2 Detail Map 3 Map Findings Summary 4 Map Findings 8 Orphan Summary 9 Government Records Searched/Data Currency Tracking GR-1 GEOCHECK ADDENDUM Physical Setting Source Addendum A-1 Physical Setting Source Summary A-2 Physical Setting SSURGO Soil Map A-5 Physical Setting Source Map A-15 Physical Setting Source Map Findings A-17 Physical Setting Source Records Searched PSGR-1 TC4020675.2s Page 1 Thank you for your business. Please contact EDR at 1-800-352-0050 with any questions or comments. Disclaimer - Copyright and Trademark Notice This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL, INCIDENTAL, CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property. Additionally, the information provided in this Report is not to be construed as legal advice. Copyright 2014 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission. EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein are the property of their respective owners. TABLE OF CONTENTS EXECUTIVE SUMMARY TC4020675.2s EXECUTIVE SUMMARY 1 A search of available environmental records was conducted by Environmental Data Resources, Inc (EDR). The report was designed to assist parties seeking to meet the search requirements of EPA’s Standards and Practices for All Appropriate Inquiries (40 CFR Part 312), the ASTM Standard Practice for Environmental Site Assessments (E 1527-13) or custom requirements developed for the evaluation of environmental risk associated with a parcel of real estate. TARGET PROPERTY INFORMATION ADDRESS 1600 LINVILLE FALLS HIGHWAY NEWLAND, NC 28657 COORDINATES 36.0458000 - 36˚ 2’ 44.88’’Latitude (North): 81.8867000 - 81˚ 53’ 12.12’’Longitude (West): Zone 17Universal Tranverse Mercator: 420127.2UTM X (Meters): 3989191.5UTM Y (Meters): 3588 ft. above sea levelElevation: USGS TOPOGRAPHIC MAP ASSOCIATED WITH TARGET PROPERTY 36081-A8 NEWLAND, NCTarget Property Map: 1994Most Recent Revision: 36081-A7 GRANDFATHER MOUNTAIN, NCEast Map: 1994Most Recent Revision: AERIAL PHOTOGRAPHY IN THIS REPORT 20120629Portions of Photo from: USDASource: TARGET PROPERTY SEARCH RESULTS The target property was not listed in any of the databases searched by EDR. DATABASES WITH NO MAPPED SITES No mapped sites were found in EDR’s search of available ("reasonably ascertainable ") government records either on the target property or within the search radius around the target property for the following databases: STANDARD ENVIRONMENTAL RECORDS Federal NPL site list NPL National Priority List EXECUTIVE SUMMARY TC4020675.2s EXECUTIVE SUMMARY 2 Proposed NPL Proposed National Priority List Sites NPL LIENS Federal Superfund Liens Federal Delisted NPL site list Delisted NPL National Priority List Deletions Federal CERCLIS list CERCLIS Comprehensive Environmental Response, Compensation, and Liability Information System FEDERAL FACILITY Federal Facility Site Information listing Federal CERCLIS NFRAP site List CERC-NFRAP CERCLIS No Further Remedial Action Planned Federal RCRA CORRACTS facilities list CORRACTS Corrective Action Report Federal RCRA non-CORRACTS TSD facilities list RCRA-TSDF RCRA - Treatment, Storage and Disposal Federal RCRA generators list RCRA-LQG RCRA - Large Quantity Generators RCRA-SQG RCRA - Small Quantity Generators RCRA-CESQG RCRA - Conditionally Exempt Small Quantity Generator Federal institutional controls / engineering controls registries US ENG CONTROLS Engineering Controls Sites List US INST CONTROL Sites with Institutional Controls LUCIS Land Use Control Information System Federal ERNS list ERNS Emergency Response Notification System State- and tribal - equivalent NPL NC HSDS Hazardous Substance Disposal Site State- and tribal - equivalent CERCLIS SHWS Inactive Hazardous Sites Inventory State and tribal landfill and/or solid waste disposal site lists SWF/LF List of Solid Waste Facilities OLI Old Landfill Inventory State and tribal leaking storage tank lists LUST Regional UST Database EXECUTIVE SUMMARY TC4020675.2s EXECUTIVE SUMMARY 3 LUST TRUST State Trust Fund Database LAST Leaking Aboveground Storage Tanks INDIAN LUST Leaking Underground Storage Tanks on Indian Land State and tribal registered storage tank lists UST Petroleum Underground Storage Tank Database AST AST Database INDIAN UST Underground Storage Tanks on Indian Land FEMA UST Underground Storage Tank Listing State and tribal institutional control / engineering control registries INST CONTROL No Further Action Sites With Land Use Restrictions Monitoring State and tribal voluntary cleanup sites VCP Responsible Party Voluntary Action Sites INDIAN VCP Voluntary Cleanup Priority Listing State and tribal Brownfields sites BROWNFIELDS Brownfields Projects Inventory ADDITIONAL ENVIRONMENTAL RECORDS Local Brownfield lists US BROWNFIELDS A Listing of Brownfields Sites Local Lists of Landfill / Solid Waste Disposal Sites DEBRIS REGION 9 Torres Martinez Reservation Illegal Dump Site Locations ODI Open Dump Inventory HIST LF Solid Waste Facility Listing SWRCY Recycling Center Listing INDIAN ODI Report on the Status of Open Dumps on Indian Lands Local Lists of Hazardous waste / Contaminated Sites US CDL Clandestine Drug Labs US HIST CDL National Clandestine Laboratory Register Local Land Records LIENS 2 CERCLA Lien Information Records of Emergency Release Reports HMIRS Hazardous Materials Information Reporting System IMD Incident Management Database SPILLS 80 SPILLS 80 data from FirstSearch SPILLS 90 SPILLS 90 data from FirstSearch Other Ascertainable Records RCRA NonGen / NLR RCRA - Non Generators / No Longer Regulated EXECUTIVE SUMMARY TC4020675.2s EXECUTIVE SUMMARY 4 DOT OPS Incident and Accident Data DOD Department of Defense Sites FUDS Formerly Used Defense Sites CONSENT Superfund (CERCLA) Consent Decrees ROD Records Of Decision UMTRA Uranium Mill Tailings Sites US MINES Mines Master Index File TRIS Toxic Chemical Release Inventory System TSCA Toxic Substances Control Act FTTS FIFRA/ TSCA Tracking System - FIFRA (Federal Insecticide, Fungicide, & Rodenticide Act)/TSCA (Toxic Substances Control Act) HIST FTTS FIFRA/TSCA Tracking System Administrative Case Listing SSTS Section 7 Tracking Systems ICIS Integrated Compliance Information System PADS PCB Activity Database System MLTS Material Licensing Tracking System RADINFO Radiation Information Database FINDS Facility Index System/Facility Registry System RAATS RCRA Administrative Action Tracking System RMP Risk Management Plans UIC Underground Injection Wells Listing DRYCLEANERS Drycleaning Sites NPDES NPDES Facility Location Listing INDIAN RESERV Indian Reservations SCRD DRYCLEANERS State Coalition for Remediation of Drycleaners Listing 2020 COR ACTION 2020 Corrective Action Program List LEAD SMELTERS Lead Smelter Sites US AIRS Aerometric Information Retrieval System Facility Subsystem PRP Potentially Responsible Parties Financial Assurance Financial Assurance Information Listing COAL ASH EPA Coal Combustion Residues Surface Impoundments List PCB TRANSFORMER PCB Transformer Registration Database COAL ASH DOE Steam-Electric Plant Operation Data COAL ASH Coal Ash Disposal Sites US FIN ASSUR Financial Assurance Information EPA WATCH LIST EPA WATCH LIST EDR HIGH RISK HISTORICAL RECORDS EDR Exclusive Records EDR MGP EDR Proprietary Manufactured Gas Plants EDR US Hist Auto Stat EDR Exclusive Historic Gas Stations EDR US Hist Cleaners EDR Exclusive Historic Dry Cleaners EDR RECOVERED GOVERNMENT ARCHIVES Exclusive Recovered Govt. Archives RGA HWS Recovered Government Archive State Hazardous Waste Facilities List RGA LUST Recovered Government Archive Leaking Underground Storage Tank RGA LF Recovered Government Archive Solid Waste Facilities List SURROUNDING SITES: SEARCH RESULTS Surrounding sites were not identified. Unmappable (orphan) sites are not considered in the foregoing analysis. EXECUTIVE SUMMARY TC4020675.2s EXECUTIVE SUMMARY 5 Due to poor or inadequate address information, the following sites were not mapped. Count: 19 records. Site Name Database(s)____________ ____________ ALTAMONT FACILITY - BELLSOUTH IMD, LUST, LAST AVERY COUNTY TRANSFER STATION SWF/LF, HIST LF, Financial Assurance AVERY COUNTY LANDFILL SWF/LF, HIST LF NCDOT/FRANKLIN RESIDENCE SHWS, IMD PARKWAY JUNCTION IMD, LUST NCDOT-NEWLAND IMD, LUST RAINBOW PANTRY #5 LUST TRUST SPEAR SUPERETTE UST SPEAR SUPERETTE UST ERWIN’S GROCERY UST NEWLAND EXXON UST TIME-OUT CONVENIENCE STORE UST SLUDER FLORAL CO. UST NC DOT - NEWLAND (DIV ELEVEN) UST GRAGG SUNOCO UST CHAMBER OF COMMERCE BLDG UST HUGHES GROC / ALLENS GROC UST CARLOS & SONS BODY SHOP RCRA-CESQG THREE OAKS NURSERY IMD EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc. 4 000 4 0 4039 4 0 0 09 2 0 3 9 2 33833840 3 9 6 0 4 0 3 8 00 38 4 0 3 9 2 0 3800 3 8 8 0 3 7 6 0 3800 3 8 4 0 3 8 0 0 3 7 6 0 3880 3 8 00 3 7 6 0 3 7 2 0 3 7 203 6 8 0 3 6 8 0 3 6 4 0 3 68 0 3 560 380 0 3 8 0 0 3 7 6 0 37 6 0 3 7 2 0 3 8 4 0 3 8 0 0 3 7 6 0 3 7 6 0 37 2 0 3 8 4 0 3 8 40 3720 3 800 38 0 0 37 2 0 3 8 0 0 3 7 6 0 3 6 8 0 3 6 8 0 3 7 6 0 3 7 60 3 7 6 0 3720 3 680 3 6 8 0 3 6 80 3 680 3 6 8 0 3 5 6 0 3 680 3 7 2 0 3 6 8 0 3 6 4 0 3 6 4 0 3 6 4 0 3 5 60 3 6 0 0 3 6 0 0 3 6 0 0 3 6 0 0 360 0 3640 3 7 6 0 3 7 2 0 3 7 2 03680 3 6403600 3 6 40 3 8 0 0 3 6 00 3 7 6 0 3 6 0 0 3 680 3 6 4 0 3 7 2 0 3 7 2 0 00 3 6 8 0 3 6 8 0 3 6 8 0 3 600 3 6003560 3 6 8 0 3 8 0 0 3 7 6 0 3 7 6 0 3 7 2 03720 3 7 2 0 3 7 2 0 3 7 2 0 3 7 2 0 3 7 2 0 3 6 8 0 3680 3 6 8 0 3 6 8 0 3 6 8 0 3 6 8 0 3640 3640 3 6 40 3 6 4 0 3 6 40 3 6 4 0 3 6 4 0 3640 3 6 4 0 560 480 3 5 2 0 35 20 3 5 20 3 5 2 0 35 2 0 3520 3 5 20 3 5 6 0 35 6 0 3560 3 5 6 0 3 5 60 3 5 60 3 5 60 3560 3 5 6 0 3 5 60 35 6 0 3 5 6 0 3560 3 5 6 0 3560 3 6 0 0 3 6 0 0 3 6 0 0 3 6 0 0 3 6 0 0 3 600 3600 3 6 0 0 3 6 0 0 3 6 0 0 3 6 0 0 3 6 00 3 6 0 0 3 6003600 3 6 4 0 3 6 4 0 36 4 0 3 6 4 0 3 6 4 0 3 6 4 0 3 6 4 0 3 6 8 0 3 6 8 0 3 8 0 0 7 6 0 3 7 6 0 3 7 2 0 3 7 2 0 3 7 2 0 3 7 20 3 6 4 0 3 6 4 0 3 6 8 0 3 3 680 3 6 8 0 4000 4 0 4 0 4000 3 720 3 7 2 0 3 7 6 0 4 0 8 0 4 0 4 0 4 0 4 0 4 0 0 0 3 9 6 0 3 9 2 0 3 9 2 0 3 8 8 0 37 2 0 3 9 2 03880 3 6 8 0 388 0 3 6 8 0 3 8 4 0 3 8 4 0 3 8 40384 3 8 0 0 3 8 00 3 8 0 0 3 8 0 0 3 7 60 3760 3720 37 2 0 3 7 2 0 3 6 8 0 3 6 4 0 34 EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc. 3760 37603720 3 6 8 0 37603720 3680 3 6 8 0 3 7 2 0 3 6 8 0 3 6 4 0 3640 3 5 6 0 3 6 0 0 360 0 3 6 0 0 3 6 0 3 5 6 0 356 0 3560 3 6 0 0 3600 3 6 4 0 MAP FINDINGS SUMMARY Search TargetDistance Total Database Property(Miles) < 1/8 1/8 - 1/4 1/4 - 1/2 1/2 - 1 > 1 Plotted STANDARD ENVIRONMENTAL RECORDS Federal NPL site list 0 NR 0 0 0 0 1.000NPL 0 NR 0 0 0 0 1.000Proposed NPL 0 NR NR NR NR NR TPNPL LIENS Federal Delisted NPL site list 0 NR 0 0 0 0 1.000Delisted NPL Federal CERCLIS list 0 NR NR 0 0 0 0.500CERCLIS 0 NR NR 0 0 0 0.500FEDERAL FACILITY Federal CERCLIS NFRAP site List 0 NR NR 0 0 0 0.500CERC-NFRAP Federal RCRA CORRACTS facilities list 0 NR 0 0 0 0 1.000CORRACTS Federal RCRA non-CORRACTS TSD facilities list 0 NR NR 0 0 0 0.500RCRA-TSDF Federal RCRA generators list 0 NR NR NR 0 0 0.250RCRA-LQG 0 NR NR NR 0 0 0.250RCRA-SQG 0 NR NR NR 0 0 0.250RCRA-CESQG Federal institutional controls / engineering controls registries 0 NR NR 0 0 0 0.500US ENG CONTROLS 0 NR NR 0 0 0 0.500US INST CONTROL 0 NR NR 0 0 0 0.500LUCIS Federal ERNS list 0 NR NR NR NR NR TPERNS State- and tribal - equivalent NPL 0 NR 0 0 0 0 1.000NC HSDS State- and tribal - equivalent CERCLIS 0 NR 0 0 0 0 1.000SHWS State and tribal landfill and/or solid waste disposal site lists 0 NR NR 0 0 0 0.500SWF/LF 0 NR NR 0 0 0 0.500OLI State and tribal leaking storage tank lists 0 NR NR 0 0 0 0.500LUST TC4020675.2s Page 4 MAP FINDINGS SUMMARY Search TargetDistance Total Database Property(Miles) < 1/8 1/8 - 1/4 1/4 - 1/2 1/2 - 1 > 1 Plotted 0 NR NR 0 0 0 0.500LUST TRUST 0 NR NR 0 0 0 0.500LAST 0 NR NR 0 0 0 0.500INDIAN LUST State and tribal registered storage tank lists 0 NR NR NR 0 0 0.250UST 0 NR NR NR 0 0 0.250AST 0 NR NR NR 0 0 0.250INDIAN UST 0 NR NR NR 0 0 0.250FEMA UST State and tribal institutional control / engineering control registries 0 NR NR 0 0 0 0.500INST CONTROL State and tribal voluntary cleanup sites 0 NR NR 0 0 0 0.500VCP 0 NR NR 0 0 0 0.500INDIAN VCP State and tribal Brownfields sites 0 NR NR 0 0 0 0.500BROWNFIELDS ADDITIONAL ENVIRONMENTAL RECORDS Local Brownfield lists 0 NR NR 0 0 0 0.500US BROWNFIELDS Local Lists of Landfill / Solid Waste Disposal Sites 0 NR NR 0 0 0 0.500DEBRIS REGION 9 0 NR NR 0 0 0 0.500ODI 0 NR NR 0 0 0 0.500HIST LF 0 NR NR 0 0 0 0.500SWRCY 0 NR NR 0 0 0 0.500INDIAN ODI Local Lists of Hazardous waste / Contaminated Sites 0 NR NR NR NR NR TPUS CDL 0 NR NR NR NR NR TPUS HIST CDL Local Land Records 0 NR NR NR NR NR TPLIENS 2 Records of Emergency Release Reports 0 NR NR NR NR NR TPHMIRS 0 NR NR 0 0 0 0.500IMD 0 NR NR NR NR NR TPSPILLS 80 0 NR NR NR NR NR TPSPILLS 90 Other Ascertainable Records 0 NR NR NR 0 0 0.250RCRA NonGen / NLR TC4020675.2s Page 5 MAP FINDINGS SUMMARY Search TargetDistance Total Database Property(Miles) < 1/8 1/8 - 1/4 1/4 - 1/2 1/2 - 1 > 1 Plotted 0 NR NR NR NR NR TPDOT OPS 0 NR 0 0 0 0 1.000DOD 0 NR 0 0 0 0 1.000FUDS 0 NR 0 0 0 0 1.000CONSENT 0 NR 0 0 0 0 1.000ROD 0 NR NR 0 0 0 0.500UMTRA 0 NR NR NR 0 0 0.250US MINES 0 NR NR NR NR NR TPTRIS 0 NR NR NR NR NR TPTSCA 0 NR NR NR NR NR TPFTTS 0 NR NR NR NR NR TPHIST FTTS 0 NR NR NR NR NR TPSSTS 0 NR NR NR NR NR TPICIS 0 NR NR NR NR NR TPPADS 0 NR NR NR NR NR TPMLTS 0 NR NR NR NR NR TPRADINFO 0 NR NR NR NR NR TPFINDS 0 NR NR NR NR NR TPRAATS 0 NR NR NR NR NR TPRMP 0 NR NR NR NR NR TPUIC 0 NR NR NR 0 0 0.250DRYCLEANERS 0 NR NR NR NR NR TPNPDES 0 NR 0 0 0 0 1.000INDIAN RESERV 0 NR NR 0 0 0 0.500SCRD DRYCLEANERS 0 NR NR NR 0 0 0.2502020 COR ACTION 0 NR NR NR NR NR TPLEAD SMELTERS 0 NR NR NR NR NR TPUS AIRS 0 NR NR NR NR NR TPPRP 0 NR NR NR NR NR TPFinancial Assurance 0 NR NR 0 0 0 0.500COAL ASH EPA 0 NR NR NR NR NR TPPCB TRANSFORMER 0 NR NR NR NR NR TPCOAL ASH DOE 0 NR NR 0 0 0 0.500COAL ASH 0 NR NR NR NR NR TPUS FIN ASSUR 0 NR NR NR NR NR TPEPA WATCH LIST EDR HIGH RISK HISTORICAL RECORDS EDR Exclusive Records 0 NR 0 0 0 0 1.000EDR MGP 0 NR NR NR 0 0 0.250EDR US Hist Auto Stat 0 NR NR NR 0 0 0.250EDR US Hist Cleaners EDR RECOVERED GOVERNMENT ARCHIVES Exclusive Recovered Govt. Archives 0 NR NR NR NR NR TPRGA HWS 0 NR NR NR NR NR TPRGA LUST 0 NR NR NR NR NR TPRGA LF TC4020675.2s Page 6 MAP FINDINGS SUMMARY Search TargetDistance Total Database Property(Miles) < 1/8 1/8 - 1/4 1/4 - 1/2 1/2 - 1 > 1 Plotted NOTES: TP = Target Property NR = Not Requested at this Search Distance Sites may be listed in more than one database TC4020675.2s Page 7 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation NO SITES FOUND TC4020675.2s Page 8 OR P H A N S U M M A R Y Cit y ED R I D Si t e N a m e Si t e A d d r e s s Zip Database(s) Co u n t : 1 9 r e c o r d s . AL T A M O N T S1 0 5 5 1 6 9 0 0 AL T A M O N T F A C I L I T Y - B E L L S O U T H HI G H W A Y 2 2 1 28657 IMD, LUST, LAST NE W L A N D S1 0 5 1 6 3 6 9 5 AV E R Y C O U N T Y L A N D F I L L S. R . 1 1 0 1 SWF/LF, HIST LF NE W L A N D U0 0 3 1 3 8 6 3 6 SP E A R S U P E R E T T E 58 1 0 H W Y 1 9 E . S O U T H 28657 UST NE W L A N D U0 0 1 5 5 8 5 5 1 SP E A R S U P E R E T T E HI G H W A Y 1 9 - S P E A R 28657 UST NE W L A N D U0 0 1 5 5 8 5 0 7 ER W I N ’ S G R O C E R Y HW Y 1 9 A V E R Y 28657 UST NE W L A N D U0 0 3 5 6 2 9 9 7 NE W L A N D E X X O N HI G H W A Y 1 9 4 28657 UST NE W L A N D U0 0 3 1 4 7 1 2 0 TI M E - O U T C O N V E N I E N C E S T O R E 10 0 3 H W Y 1 9 4 S 28657 UST NE W L A N D S1 0 5 2 1 7 8 7 2 RA I N B O W P A N T R Y # 5 SR 1 9 4 & T U R B Y V I L L E LUST TRUST NE W L A N D 10 0 4 7 4 5 9 3 8 CA R L O S & S O N S B O D Y S H O P HW Y 1 9 4 28657 RCRA-CESQG N EW L A N D S 10 5 9 1 2 0 1 7 T HR E E O A K S N U R S E R Y R T 2 B O X 2 8 1 I MD N EW L A N D U 00 3 5 6 2 0 5 8 S LU D E R F L O R A L C O . H WY 2 2 1 28657 U ST N EW L A N D S 10 5 7 6 4 1 4 4 P AR K W A Y J U N C T I O N H IG H W A Y 2 2 1 S O U T H 28657 I MD, LUST N EW L A N D U 00 3 1 3 7 8 7 2 N C D O T - N E W L A N D ( D I V E L E V E N ) B OX 6 3 1 / H W Y 1 8 1 28657 U ST N EW L A N D S 10 5 1 6 3 6 9 6 A VE R Y C O U N T Y T R A N S F E R S T A T I O N 2 17 5 B R U S H Y C R E E K R D . S WF/LF, HIST LF, Financial A ssurance N EW L A N D U 00 1 5 5 8 4 9 2 G RA G G S U N O C O L IN V I L L E A N D A L L E Y 28657 U ST N EW L A N D U 00 1 5 5 8 4 9 1 C HA M B E R O F C O M M E R C E B L D G M AI N S T R E E T - H W Y 1 9 4 28657 U ST N EW L A N D S 10 5 8 9 3 5 9 1 N CD O T - N E W L A N D H WY N C 1 8 1 , B O X 6 3 1 28657 I MD, LUST N EW L A N D S 10 3 1 3 0 8 9 1 N CD O T / F R A N K L I N R E S I D E N C E O FF 1 8 1 , R T 2 S HWS, IMD P LU M T R E E U 00 1 5 5 8 5 1 8 H UG H E S G R O C / A L L E N S G R O C R T 3 28657 U ST TC 4 0 2 0 6 7 5 . 2 s P a g e 9 To maintain currency of the following federal and state databases, EDR contacts the appropriate governmental agency on a monthly or quarterly basis, as required. Number of Days to Update:Provides confirmation that EDR is reporting records that have been updated within 90 days from the date the government agency made the information available to the public. STANDARD ENVIRONMENTAL RECORDS Federal NPL site list NPL: National Priority List National Priorities List (Superfund). The NPL is a subset of CERCLIS and identifies over 1,200 sites for priority cleanup under the Superfund Program. NPL sites may encompass relatively large areas. As such, EDR provides polygon coverage for over 1,000 NPL site boundaries produced by EPA’s Environmental Photographic Interpretation Center (EPIC) and regional EPA offices. Date of Government Version: 10/25/2013 Date Data Arrived at EDR: 11/11/2013 Date Made Active in Reports: 01/28/2014 Number of Days to Update: 78 Source: EPA Telephone: N/A Last EDR Contact: 07/08/2014 Next Scheduled EDR Contact: 10/20/2014 Data Release Frequency: Quarterly NPL Site Boundaries Sources: EPA’s Environmental Photographic Interpretation Center (EPIC) Telephone: 202-564-7333 EPA Region 1 EPA Region 6 Telephone 617-918-1143 Telephone: 214-655-6659 EPA Region 3 EPA Region 7 Telephone 215-814-5418 Telephone: 913-551-7247 EPA Region 4 EPA Region 8 Telephone 404-562-8033 Telephone: 303-312-6774 EPA Region 5 EPA Region 9 Telephone 312-886-6686 Telephone: 415-947-4246 EPA Region 10 Telephone 206-553-8665 Proposed NPL: Proposed National Priority List Sites A site that has been proposed for listing on the National Priorities List through the issuance of a proposed rule in the Federal Register. EPA then accepts public comments on the site, responds to the comments, and places on the NPL those sites that continue to meet the requirements for listing. Date of Government Version: 10/25/2013 Date Data Arrived at EDR: 11/11/2013 Date Made Active in Reports: 01/28/2014 Number of Days to Update: 78 Source: EPA Telephone: N/A Last EDR Contact: 07/08/2014 Next Scheduled EDR Contact: 10/20/2014 Data Release Frequency: Quarterly NPL LIENS: Federal Superfund Liens Federal Superfund Liens. Under the authority granted the USEPA by CERCLA of 1980, the USEPA has the authority to file liens against real property in order to recover remedial action expenditures or when the property owner received notification of potential liability. USEPA compiles a listing of filed notices of Superfund Liens. Date of Government Version: 10/15/1991 Date Data Arrived at EDR: 02/02/1994 Date Made Active in Reports: 03/30/1994 Number of Days to Update: 56 Source: EPA Telephone: 202-564-4267 Last EDR Contact: 08/15/2011 Next Scheduled EDR Contact: 11/28/2011 Data Release Frequency: No Update Planned TC4020675.2s Page GR-1 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING Federal Delisted NPL site list DELISTED NPL: National Priority List Deletions The National Oil and Hazardous Substances Pollution Contingency Plan (NCP) establishes the criteria that the EPA uses to delete sites from the NPL. In accordance with 40 CFR 300.425.(e), sites may be deleted from the NPL where no further response is appropriate. Date of Government Version: 10/25/2013 Date Data Arrived at EDR: 11/11/2013 Date Made Active in Reports: 01/28/2014 Number of Days to Update: 78 Source: EPA Telephone: N/A Last EDR Contact: 07/08/2014 Next Scheduled EDR Contact: 10/20/2014 Data Release Frequency: Quarterly Federal CERCLIS list CERCLIS: Comprehensive Environmental Response, Compensation, and Liability Information System CERCLIS contains data on potentially hazardous waste sites that have been reported to the USEPA by states, municipalities, private companies and private persons, pursuant to Section 103 of the Comprehensive Environmental Response, Compensation, and Liability Act (CERCLA). CERCLIS contains sites which are either proposed to or on the National Priorities List (NPL) and sites which are in the screening and assessment phase for possible inclusion on the NPL. Date of Government Version: 10/25/2013 Date Data Arrived at EDR: 11/11/2013 Date Made Active in Reports: 02/13/2014 Number of Days to Update: 94 Source: EPA Telephone: 703-412-9810 Last EDR Contact: 05/29/2014 Next Scheduled EDR Contact: 09/08/2014 Data Release Frequency: Quarterly FEDERAL FACILITY: Federal Facility Site Information listing A listing of National Priority List (NPL) and Base Realignment and Closure (BRAC) sites found in the Comprehensive Environmental Response, Compensation and Liability Information System (CERCLIS) Database where EPA Federal Facilities Restoration and Reuse Office is involved in cleanup activities. Date of Government Version: 05/31/2013 Date Data Arrived at EDR: 07/08/2013 Date Made Active in Reports: 12/06/2013 Number of Days to Update: 151 Source: Environmental Protection Agency Telephone: 703-603-8704 Last EDR Contact: 07/08/2014 Next Scheduled EDR Contact: 10/20/2014 Data Release Frequency: Varies Federal CERCLIS NFRAP site List CERCLIS-NFRAP: CERCLIS No Further Remedial Action Planned Archived sites are sites that have been removed and archived from the inventory of CERCLIS sites. Archived status indicates that, to the best of EPA’s knowledge, assessment at a site has been completed and that EPA has determined no further steps will be taken to list this site on the National Priorities List (NPL), unless information indicates this decision was not appropriate or other considerations require a recommendation for listing at a later time. This decision does not necessarily mean that there is no hazard associated with a given site; it only means that, based upon available information, the location is not judged to be a potential NPL site. Date of Government Version: 10/25/2013 Date Data Arrived at EDR: 11/11/2013 Date Made Active in Reports: 02/13/2014 Number of Days to Update: 94 Source: EPA Telephone: 703-412-9810 Last EDR Contact: 05/29/2014 Next Scheduled EDR Contact: 09/08/2014 Data Release Frequency: Quarterly Federal RCRA CORRACTS facilities list CORRACTS: Corrective Action Report CORRACTS identifies hazardous waste handlers with RCRA corrective action activity. TC4020675.2s Page GR-2 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING Date of Government Version: 03/11/2014 Date Data Arrived at EDR: 03/13/2014 Date Made Active in Reports: 04/09/2014 Number of Days to Update: 27 Source: EPA Telephone: 800-424-9346 Last EDR Contact: 07/02/2014 Next Scheduled EDR Contact: 10/13/2014 Data Release Frequency: Quarterly Federal RCRA non-CORRACTS TSD facilities list RCRA-TSDF: RCRA - Treatment, Storage and Disposal RCRAInfo is EPA’s comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Transporters are individuals or entities that move hazardous waste from the generator offsite to a facility that can recycle, treat, store, or dispose of the waste. TSDFs treat, store, or dispose of the waste. Date of Government Version: 03/11/2014 Date Data Arrived at EDR: 03/13/2014 Date Made Active in Reports: 04/09/2014 Number of Days to Update: 27 Source: Environmental Protection Agency Telephone: (404) 562-8651 Last EDR Contact: 07/02/2014 Next Scheduled EDR Contact: 10/13/2014 Data Release Frequency: Quarterly Federal RCRA generators list RCRA-LQG: RCRA - Large Quantity Generators RCRAInfo is EPA’s comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Large quantity generators (LQGs) generate over 1,000 kilograms (kg) of hazardous waste, or over 1 kg of acutely hazardous waste per month. Date of Government Version: 03/11/2014 Date Data Arrived at EDR: 03/13/2014 Date Made Active in Reports: 04/09/2014 Number of Days to Update: 27 Source: Environmental Protection Agency Telephone: (404) 562-8651 Last EDR Contact: 07/02/2014 Next Scheduled EDR Contact: 10/13/2014 Data Release Frequency: Quarterly RCRA-SQG: RCRA - Small Quantity Generators RCRAInfo is EPA’s comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Small quantity generators (SQGs) generate between 100 kg and 1,000 kg of hazardous waste per month. Date of Government Version: 03/11/2014 Date Data Arrived at EDR: 03/13/2014 Date Made Active in Reports: 04/09/2014 Number of Days to Update: 27 Source: Environmental Protection Agency Telephone: (404) 562-8651 Last EDR Contact: 07/02/2014 Next Scheduled EDR Contact: 10/13/2014 Data Release Frequency: Quarterly RCRA-CESQG: RCRA - Conditionally Exempt Small Quantity Generators RCRAInfo is EPA’s comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Conditionally exempt small quantity generators (CESQGs) generate less than 100 kg of hazardous waste, or less than 1 kg of acutely hazardous waste per month. Date of Government Version: 03/11/2014 Date Data Arrived at EDR: 03/13/2014 Date Made Active in Reports: 04/09/2014 Number of Days to Update: 27 Source: Environmental Protection Agency Telephone: (404) 562-8651 Last EDR Contact: 07/02/2014 Next Scheduled EDR Contact: 10/13/2014 Data Release Frequency: Varies TC4020675.2s Page GR-3 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING Federal institutional controls / engineering controls registries US ENG CONTROLS: Engineering Controls Sites List A listing of sites with engineering controls in place. Engineering controls include various forms of caps, building foundations, liners, and treatment methods to create pathway elimination for regulated substances to enter environmental media or effect human health. Date of Government Version: 03/19/2014 Date Data Arrived at EDR: 03/21/2014 Date Made Active in Reports: 07/15/2014 Number of Days to Update: 116 Source: Environmental Protection Agency Telephone: 703-603-0695 Last EDR Contact: 06/05/2014 Next Scheduled EDR Contact: 09/22/2014 Data Release Frequency: Varies US INST CONTROL: Sites with Institutional Controls A listing of sites with institutional controls in place. Institutional controls include administrative measures, such as groundwater use restrictions, construction restrictions, property use restrictions, and post remediation care requirements intended to prevent exposure to contaminants remaining on site. Deed restrictions are generally required as part of the institutional controls. Date of Government Version: 03/19/2014 Date Data Arrived at EDR: 03/21/2014 Date Made Active in Reports: 07/15/2014 Number of Days to Update: 116 Source: Environmental Protection Agency Telephone: 703-603-0695 Last EDR Contact: 06/05/2014 Next Scheduled EDR Contact: 09/22/2014 Data Release Frequency: Varies LUCIS: Land Use Control Information System LUCIS contains records of land use control information pertaining to the former Navy Base Realignment and Closure properties. Date of Government Version: 05/28/2014 Date Data Arrived at EDR: 05/30/2014 Date Made Active in Reports: 06/17/2014 Number of Days to Update: 18 Source: Department of the Navy Telephone: 843-820-7326 Last EDR Contact: 05/19/2014 Next Scheduled EDR Contact: 09/01/2014 Data Release Frequency: Varies Federal ERNS list ERNS: Emergency Response Notification System Emergency Response Notification System. ERNS records and stores information on reported releases of oil and hazardous substances. Date of Government Version: 09/30/2013 Date Data Arrived at EDR: 10/01/2013 Date Made Active in Reports: 12/06/2013 Number of Days to Update: 66 Source: National Response Center, United States Coast Guard Telephone: 202-267-2180 Last EDR Contact: 07/03/2014 Next Scheduled EDR Contact: 07/14/2014 Data Release Frequency: Annually State- and tribal - equivalent NPL HSDS: Hazardous Substance Disposal Site Locations of uncontrolled and unregulated hazardous waste sites. The file includes sites on the National Priority List as well as those on the state priority list. Date of Government Version: 08/09/2011 Date Data Arrived at EDR: 11/08/2011 Date Made Active in Reports: 12/05/2011 Number of Days to Update: 27 Source: North Carolina Center for Geographic Information and Analysis Telephone: 919-754-6580 Last EDR Contact: 05/02/2014 Next Scheduled EDR Contact: 08/18/2014 Data Release Frequency: Biennially State- and tribal - equivalent CERCLIS TC4020675.2s Page GR-4 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING SHWS: Inactive Hazardous Sites Inventory State Hazardous Waste Sites. State hazardous waste site records are the states’ equivalent to CERCLIS. These sites may or may not already be listed on the federal CERCLIS list. Priority sites planned for cleanup using state funds (state equivalent of Superfund) are identified along with sites where cleanup will be paid for by potentially responsible parties. Available information varies by state. Date of Government Version: 06/12/2014 Date Data Arrived at EDR: 06/17/2014 Date Made Active in Reports: 07/11/2014 Number of Days to Update: 24 Source: Department of Environment, Health and Natural Resources Telephone: 919-508-8400 Last EDR Contact: 06/17/2014 Next Scheduled EDR Contact: 09/29/2014 Data Release Frequency: Quarterly State and tribal landfill and/or solid waste disposal site lists SWF/LF: List of Solid Waste Facilities Solid Waste Facilities/Landfill Sites. SWF/LF type records typically contain an inventory of solid waste disposal facilities or landfills in a particular state. Depending on the state, these may be active or inactive facilities or open dumps that failed to meet RCRA Subtitle D Section 4004 criteria for solid waste landfills or disposal sites. Date of Government Version: 03/31/2014 Date Data Arrived at EDR: 04/02/2014 Date Made Active in Reports: 04/23/2014 Number of Days to Update: 21 Source: Department of Environment and Natural Resources Telephone: 919-733-0692 Last EDR Contact: 07/02/2014 Next Scheduled EDR Contact: 10/13/2014 Data Release Frequency: Semi-Annually OLI: Old Landfill Inventory Old landfill inventory location information. (Does not include no further action sites and other agency lead sites). Date of Government Version: 04/03/2014 Date Data Arrived at EDR: 04/15/2014 Date Made Active in Reports: 05/19/2014 Number of Days to Update: 34 Source: Department of Environment & Natural Resources Telephone: 919-733-4996 Last EDR Contact: 07/18/2014 Next Scheduled EDR Contact: 10/27/2014 Data Release Frequency: Varies State and tribal leaking storage tank lists LUST: Regional UST Database This database contains information obtained from the Regional Offices. It provides a more detailed explanation of current and historic activity for individual sites, as well as what was previously found in the Incident Management Database. Sites in this database with Incident Numbers are considered LUSTs. Date of Government Version: 05/09/2014 Date Data Arrived at EDR: 05/14/2014 Date Made Active in Reports: 05/19/2014 Number of Days to Update: 5 Source: Department of Environment and Natural Resources Telephone: 919-733-1308 Last EDR Contact: 05/14/2014 Next Scheduled EDR Contact: 08/25/2014 Data Release Frequency: Quarterly LUST TRUST: State Trust Fund Database This database contains information about claims against the State Trust Funds for reimbursements for expenses incurred while remediating Leaking USTs. Date of Government Version: 04/11/2014 Date Data Arrived at EDR: 04/15/2014 Date Made Active in Reports: 05/19/2014 Number of Days to Update: 34 Source: Department of Environment and Natural Resources Telephone: 919-733-1315 Last EDR Contact: 07/16/2014 Next Scheduled EDR Contact: 10/27/2014 Data Release Frequency: Semi-Annually TC4020675.2s Page GR-5 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING LAST: Leaking Aboveground Storage Tanks A listing of leaking aboveground storage tank site locations. Date of Government Version: 05/09/2014 Date Data Arrived at EDR: 05/14/2014 Date Made Active in Reports: 05/19/2014 Number of Days to Update: 5 Source: Department of Environment & Natural Resources Telephone: 877-623-6748 Last EDR Contact: 05/14/2014 Next Scheduled EDR Contact: 08/25/2014 Data Release Frequency: Quarterly INDIAN LUST R10: Leaking Underground Storage Tanks on Indian Land LUSTs on Indian land in Alaska, Idaho, Oregon and Washington. Date of Government Version: 11/06/2013 Date Data Arrived at EDR: 11/07/2013 Date Made Active in Reports: 12/06/2013 Number of Days to Update: 29 Source: EPA Region 10 Telephone: 206-553-2857 Last EDR Contact: 04/28/2014 Next Scheduled EDR Contact: 11/10/2014 Data Release Frequency: Quarterly INDIAN LUST R5: Leaking Underground Storage Tanks on Indian Land Leaking underground storage tanks located on Indian Land in Michigan, Minnesota and Wisconsin. Date of Government Version: 05/12/2014 Date Data Arrived at EDR: 05/12/2014 Date Made Active in Reports: 06/17/2014 Number of Days to Update: 36 Source: EPA, Region 5 Telephone: 312-886-7439 Last EDR Contact: 04/28/2014 Next Scheduled EDR Contact: 11/10/2014 Data Release Frequency: Varies INDIAN LUST R8: Leaking Underground Storage Tanks on Indian Land LUSTs on Indian land in Colorado, Montana, North Dakota, South Dakota, Utah and Wyoming. Date of Government Version: 08/27/2012 Date Data Arrived at EDR: 08/28/2012 Date Made Active in Reports: 10/16/2012 Number of Days to Update: 49 Source: EPA Region 8 Telephone: 303-312-6271 Last EDR Contact: 07/22/2014 Next Scheduled EDR Contact: 11/10/2014 Data Release Frequency: Quarterly INDIAN LUST R9: Leaking Underground Storage Tanks on Indian Land LUSTs on Indian land in Arizona, California, New Mexico and Nevada Date of Government Version: 03/01/2013 Date Data Arrived at EDR: 03/01/2013 Date Made Active in Reports: 04/12/2013 Number of Days to Update: 42 Source: Environmental Protection Agency Telephone: 415-972-3372 Last EDR Contact: 07/22/2014 Next Scheduled EDR Contact: 11/10/2014 Data Release Frequency: Quarterly INDIAN LUST R7: Leaking Underground Storage Tanks on Indian Land LUSTs on Indian land in Iowa, Kansas, and Nebraska Date of Government Version: 04/28/2014 Date Data Arrived at EDR: 05/01/2014 Date Made Active in Reports: 06/17/2014 Number of Days to Update: 47 Source: EPA Region 7 Telephone: 913-551-7003 Last EDR Contact: 04/28/2014 Next Scheduled EDR Contact: 11/10/2014 Data Release Frequency: Varies INDIAN LUST R6: Leaking Underground Storage Tanks on Indian Land LUSTs on Indian land in New Mexico and Oklahoma. Date of Government Version: 05/14/2014 Date Data Arrived at EDR: 05/15/2014 Date Made Active in Reports: 07/15/2014 Number of Days to Update: 61 Source: EPA Region 6 Telephone: 214-665-6597 Last EDR Contact: 07/22/2014 Next Scheduled EDR Contact: 11/20/2014 Data Release Frequency: Varies TC4020675.2s Page GR-6 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING INDIAN LUST R4: Leaking Underground Storage Tanks on Indian Land LUSTs on Indian land in Florida, Mississippi and North Carolina. Date of Government Version: 04/24/2014 Date Data Arrived at EDR: 04/25/2014 Date Made Active in Reports: 06/17/2014 Number of Days to Update: 53 Source: EPA Region 4 Telephone: 404-562-8677 Last EDR Contact: 04/22/2014 Next Scheduled EDR Contact: 08/11/2014 Data Release Frequency: Semi-Annually INDIAN LUST R1: Leaking Underground Storage Tanks on Indian Land A listing of leaking underground storage tank locations on Indian Land. Date of Government Version: 02/01/2013 Date Data Arrived at EDR: 05/01/2013 Date Made Active in Reports: 11/01/2013 Number of Days to Update: 184 Source: EPA Region 1 Telephone: 617-918-1313 Last EDR Contact: 05/02/2014 Next Scheduled EDR Contact: 08/11/2014 Data Release Frequency: Varies State and tribal registered storage tank lists UST: Petroleum Underground Storage Tank Database Registered Underground Storage Tanks. UST’s are regulated under Subtitle I of the Resource Conservation and Recovery Act (RCRA) and must be registered with the state department responsible for administering the UST program. Available information varies by state program. Date of Government Version: 05/09/2014 Date Data Arrived at EDR: 05/14/2014 Date Made Active in Reports: 05/19/2014 Number of Days to Update: 5 Source: Department of Environment and Natural Resources Telephone: 919-733-1308 Last EDR Contact: 05/14/2014 Next Scheduled EDR Contact: 08/25/2014 Data Release Frequency: Quarterly AST: AST Database Facilities with aboveground storage tanks that have a capacity greater than 21,000 gallons. Date of Government Version: 06/19/2014 Date Data Arrived at EDR: 06/23/2014 Date Made Active in Reports: 07/14/2014 Number of Days to Update: 21 Source: Department of Environment and Natural Resources Telephone: 919-715-6183 Last EDR Contact: 06/19/2014 Next Scheduled EDR Contact: 10/06/2014 Data Release Frequency: Semi-Annually INDIAN UST R1: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 1 (Connecticut, Maine, Massachusetts, New Hampshire, Rhode Island, Vermont and ten Tribal Nations). Date of Government Version: 02/01/2013 Date Data Arrived at EDR: 05/01/2013 Date Made Active in Reports: 01/27/2014 Number of Days to Update: 271 Source: EPA, Region 1 Telephone: 617-918-1313 Last EDR Contact: 05/02/2014 Next Scheduled EDR Contact: 08/11/2014 Data Release Frequency: Varies INDIAN UST R7: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 7 (Iowa, Kansas, Missouri, Nebraska, and 9 Tribal Nations). Date of Government Version: 05/28/2014 Date Data Arrived at EDR: 05/01/2014 Date Made Active in Reports: 06/17/2014 Number of Days to Update: 47 Source: EPA Region 7 Telephone: 913-551-7003 Last EDR Contact: 04/28/2014 Next Scheduled EDR Contact: 11/10/2014 Data Release Frequency: Varies TC4020675.2s Page GR-7 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING INDIAN UST R8: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 8 (Colorado, Montana, North Dakota, South Dakota, Utah, Wyoming and 27 Tribal Nations). Date of Government Version: 05/07/2014 Date Data Arrived at EDR: 05/09/2014 Date Made Active in Reports: 06/17/2014 Number of Days to Update: 39 Source: EPA Region 8 Telephone: 303-312-6137 Last EDR Contact: 07/22/2014 Next Scheduled EDR Contact: 11/10/2014 Data Release Frequency: Quarterly INDIAN UST R9: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 9 (Arizona, California, Hawaii, Nevada, the Pacific Islands, and Tribal Nations). Date of Government Version: 05/12/2014 Date Data Arrived at EDR: 05/14/2014 Date Made Active in Reports: 06/17/2014 Number of Days to Update: 34 Source: EPA Region 9 Telephone: 415-972-3368 Last EDR Contact: 07/22/2014 Next Scheduled EDR Contact: 11/10/2014 Data Release Frequency: Quarterly INDIAN UST R10: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 10 (Alaska, Idaho, Oregon, Washington, and Tribal Nations). Date of Government Version: 04/04/2014 Date Data Arrived at EDR: 04/08/2014 Date Made Active in Reports: 06/17/2014 Number of Days to Update: 70 Source: EPA Region 10 Telephone: 206-553-2857 Last EDR Contact: 07/22/2014 Next Scheduled EDR Contact: 11/10/2014 Data Release Frequency: Quarterly INDIAN UST R4: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 4 (Alabama, Florida, Georgia, Kentucky, Mississippi, North Carolina, South Carolina, Tennessee and Tribal Nations) Date of Government Version: 04/24/2014 Date Data Arrived at EDR: 04/25/2014 Date Made Active in Reports: 06/17/2014 Number of Days to Update: 53 Source: EPA Region 4 Telephone: 404-562-9424 Last EDR Contact: 04/22/2014 Next Scheduled EDR Contact: 08/11/2014 Data Release Frequency: Semi-Annually INDIAN UST R5: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 5 (Michigan, Minnesota and Wisconsin and Tribal Nations). Date of Government Version: 05/12/2014 Date Data Arrived at EDR: 05/12/2014 Date Made Active in Reports: 06/17/2014 Number of Days to Update: 36 Source: EPA Region 5 Telephone: 312-886-6136 Last EDR Contact: 04/28/2014 Next Scheduled EDR Contact: 11/10/2014 Data Release Frequency: Varies INDIAN UST R6: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 6 (Louisiana, Arkansas, Oklahoma, New Mexico, Texas and 65 Tribes). Date of Government Version: 05/14/2014 Date Data Arrived at EDR: 05/15/2014 Date Made Active in Reports: 06/17/2014 Number of Days to Update: 33 Source: EPA Region 6 Telephone: 214-665-7591 Last EDR Contact: 07/22/2014 Next Scheduled EDR Contact: 11/10/2014 Data Release Frequency: Semi-Annually TC4020675.2s Page GR-8 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING FEMA UST: Underground Storage Tank Listing A listing of all FEMA owned underground storage tanks. Date of Government Version: 01/01/2010 Date Data Arrived at EDR: 02/16/2010 Date Made Active in Reports: 04/12/2010 Number of Days to Update: 55 Source: FEMA Telephone: 202-646-5797 Last EDR Contact: 07/08/2014 Next Scheduled EDR Contact: 10/27/2014 Data Release Frequency: Varies State and tribal institutional control / engineering control registries INST CONTROL: No Further Action Sites With Land Use Restrictions Monitoring A land use restricted site is a property where there are limits or requirements on future use of the property due to varying levels of cleanup possible, practical, or necessary at the site. Date of Government Version: 06/12/2014 Date Data Arrived at EDR: 06/17/2014 Date Made Active in Reports: 07/11/2014 Number of Days to Update: 24 Source: Department of Environment, Health and Natural Resources Telephone: 919-508-8400 Last EDR Contact: 06/17/2014 Next Scheduled EDR Contact: 09/29/2014 Data Release Frequency: Quarterly State and tribal voluntary cleanup sites VCP: Responsible Party Voluntary Action Sites Responsible Party Voluntary Action site locations. Date of Government Version: 06/12/2014 Date Data Arrived at EDR: 06/17/2014 Date Made Active in Reports: 07/14/2014 Number of Days to Update: 27 Source: Department of Environment and Natural Resources Telephone: 919-508-8400 Last EDR Contact: 06/17/2014 Next Scheduled EDR Contact: 09/29/2014 Data Release Frequency: Semi-Annually INDIAN VCP R1: Voluntary Cleanup Priority Listing A listing of voluntary cleanup priority sites located on Indian Land located in Region 1. Date of Government Version: 03/20/2014 Date Data Arrived at EDR: 04/01/2014 Date Made Active in Reports: 06/17/2014 Number of Days to Update: 77 Source: EPA, Region 1 Telephone: 617-918-1102 Last EDR Contact: 07/01/2014 Next Scheduled EDR Contact: 10/13/2014 Data Release Frequency: Varies INDIAN VCP R7: Voluntary Cleanup Priority Lisitng A listing of voluntary cleanup priority sites located on Indian Land located in Region 7. Date of Government Version: 03/20/2008 Date Data Arrived at EDR: 04/22/2008 Date Made Active in Reports: 05/19/2008 Number of Days to Update: 27 Source: EPA, Region 7 Telephone: 913-551-7365 Last EDR Contact: 04/20/2009 Next Scheduled EDR Contact: 07/20/2009 Data Release Frequency: Varies State and tribal Brownfields sites BROWNFIELDS: Brownfields Projects Inventory A brownfield site is an abandoned, idled, or underused property where the threat of environmental contamination has hindered its redevelopment. All of the sites in the inventory are working toward a brownfield agreement for cleanup and liabitliy control. Date of Government Version: 04/07/2014 Date Data Arrived at EDR: 04/09/2014 Date Made Active in Reports: 04/23/2014 Number of Days to Update: 14 Source: Department of Environment and Natural Resources Telephone: 919-733-4996 Last EDR Contact: 07/08/2014 Next Scheduled EDR Contact: 10/20/2014 Data Release Frequency: Varies TC4020675.2s Page GR-9 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING ADDITIONAL ENVIRONMENTAL RECORDS Local Brownfield lists US BROWNFIELDS: A Listing of Brownfields Sites Brownfields are real property, the expansion, redevelopment, or reuse of which may be complicated by the presence or potential presence of a hazardous substance, pollutant, or contaminant. Cleaning up and reinvesting in these properties takes development pressures off of undeveloped, open land, and both improves and protects the environment. Assessment, Cleanup and Redevelopment Exchange System (ACRES) stores information reported by EPA Brownfields grant recipients on brownfields properties assessed or cleaned up with grant funding as well as information on Targeted Brownfields Assessments performed by EPA Regions. A listing of ACRES Brownfield sites is obtained from Cleanups in My Community. Cleanups in My Community provides information on Brownfields properties for which information is reported back to EPA, as well as areas served by Brownfields grant programs. Date of Government Version: 07/01/2014 Date Data Arrived at EDR: 07/03/2014 Date Made Active in Reports: 07/28/2014 Number of Days to Update: 25 Source: Environmental Protection Agency Telephone: 202-566-2777 Last EDR Contact: 07/03/2014 Next Scheduled EDR Contact: 10/06/2014 Data Release Frequency: Semi-Annually Local Lists of Landfill / Solid Waste Disposal Sites DEBRIS REGION 9: Torres Martinez Reservation Illegal Dump Site Locations A listing of illegal dump sites location on the Torres Martinez Indian Reservation located in eastern Riverside County and northern Imperial County, California. Date of Government Version: 01/12/2009 Date Data Arrived at EDR: 05/07/2009 Date Made Active in Reports: 09/21/2009 Number of Days to Update: 137 Source: EPA, Region 9 Telephone: 415-947-4219 Last EDR Contact: 07/25/2014 Next Scheduled EDR Contact: 11/10/2014 Data Release Frequency: No Update Planned ODI: Open Dump Inventory An open dump is defined as a disposal facility that does not comply with one or more of the Part 257 or Part 258 Subtitle D Criteria. Date of Government Version: 06/30/1985 Date Data Arrived at EDR: 08/09/2004 Date Made Active in Reports: 09/17/2004 Number of Days to Update: 39 Source: Environmental Protection Agency Telephone: 800-424-9346 Last EDR Contact: 06/09/2004 Next Scheduled EDR Contact: N/A Data Release Frequency: No Update Planned SWRCY: Recycling Center Listing A listing of recycling center locations. Date of Government Version: 06/09/2014 Date Data Arrived at EDR: 06/10/2014 Date Made Active in Reports: 07/11/2014 Number of Days to Update: 31 Source: Department of Environment & Natural Resources Telephone: 919-707-8137 Last EDR Contact: 05/19/2014 Next Scheduled EDR Contact: 08/18/2014 Data Release Frequency: Varies HIST LF: Solid Waste Facility Listing A listing of solid waste facilities. Date of Government Version: 11/06/2006 Date Data Arrived at EDR: 02/13/2007 Date Made Active in Reports: 03/02/2007 Number of Days to Update: 17 Source: Department of Environment & Natural Resources Telephone: 919-733-0692 Last EDR Contact: 01/19/2009 Next Scheduled EDR Contact: 04/19/2009 Data Release Frequency: Quarterly TC4020675.2s Page GR-10 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING INDIAN ODI: Report on the Status of Open Dumps on Indian Lands Location of open dumps on Indian land. Date of Government Version: 12/31/1998 Date Data Arrived at EDR: 12/03/2007 Date Made Active in Reports: 01/24/2008 Number of Days to Update: 52 Source: Environmental Protection Agency Telephone: 703-308-8245 Last EDR Contact: 05/02/2014 Next Scheduled EDR Contact: 08/18/2014 Data Release Frequency: Varies Local Lists of Hazardous waste / Contaminated Sites US CDL: Clandestine Drug Labs A listing of clandestine drug lab locations. The U.S. Department of Justice ("the Department") provides this web site as a public service. It contains addresses of some locations where law enforcement agencies reported they found chemicals or other items that indicated the presence of either clandestine drug laboratories or dumpsites. In most cases, the source of the entries is not the Department, and the Department has not verified the entry and does not guarantee its accuracy. Members of the public must verify the accuracy of all entries by, for example, contacting local law enforcement and local health departments. Date of Government Version: 05/28/2014 Date Data Arrived at EDR: 06/20/2014 Date Made Active in Reports: 07/15/2014 Number of Days to Update: 25 Source: Drug Enforcement Administration Telephone: 202-307-1000 Last EDR Contact: 06/04/2014 Next Scheduled EDR Contact: 09/15/2014 Data Release Frequency: Quarterly US HIST CDL: National Clandestine Laboratory Register A listing of clandestine drug lab locations. The U.S. Department of Justice ("the Department") provides this web site as a public service. It contains addresses of some locations where law enforcement agencies reported they found chemicals or other items that indicated the presence of either clandestine drug laboratories or dumpsites. In most cases, the source of the entries is not the Department, and the Department has not verified the entry and does not guarantee its accuracy. Members of the public must verify the accuracy of all entries by, for example, contacting local law enforcement and local health departments. Date of Government Version: 05/28/2014 Date Data Arrived at EDR: 06/20/2014 Date Made Active in Reports: 07/15/2014 Number of Days to Update: 25 Source: Drug Enforcement Administration Telephone: 202-307-1000 Last EDR Contact: 06/04/2014 Next Scheduled EDR Contact: 09/15/2014 Data Release Frequency: No Update Planned Local Land Records LIENS 2: CERCLA Lien Information A Federal CERCLA (’Superfund’) lien can exist by operation of law at any site or property at which EPA has spent Superfund monies. These monies are spent to investigate and address releases and threatened releases of contamination. CERCLIS provides information as to the identity of these sites and properties. Date of Government Version: 02/18/2014 Date Data Arrived at EDR: 03/18/2014 Date Made Active in Reports: 04/24/2014 Number of Days to Update: 37 Source: Environmental Protection Agency Telephone: 202-564-6023 Last EDR Contact: 07/22/2014 Next Scheduled EDR Contact: 11/10/2014 Data Release Frequency: Varies Records of Emergency Release Reports HMIRS: Hazardous Materials Information Reporting System Hazardous Materials Incident Report System. HMIRS contains hazardous material spill incidents reported to DOT. Date of Government Version: 03/31/2014 Date Data Arrived at EDR: 04/01/2014 Date Made Active in Reports: 07/15/2014 Number of Days to Update: 105 Source: U.S. Department of Transportation Telephone: 202-366-4555 Last EDR Contact: 07/01/2014 Next Scheduled EDR Contact: 10/13/2014 Data Release Frequency: Annually TC4020675.2s Page GR-11 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING IMD: Incident Management Database Groundwater and/or soil contamination incidents Date of Government Version: 07/21/2006 Date Data Arrived at EDR: 08/01/2006 Date Made Active in Reports: 08/23/2006 Number of Days to Update: 22 Source: Department of Environment and Natural Resources Telephone: 919-733-3221 Last EDR Contact: 07/01/2011 Next Scheduled EDR Contact: 10/17/2011 Data Release Frequency: No Update Planned SPILLS 80: SPILLS80 data from FirstSearch Spills 80 includes those spill and release records available from FirstSearch databases prior to 1990. Typically, they may include chemical, oil and/or hazardous substance spills recorded before 1990. Duplicate records that are already included in EDR incident and release records are not included in Spills 80. Date of Government Version: 06/14/2001 Date Data Arrived at EDR: 01/03/2013 Date Made Active in Reports: 03/06/2013 Number of Days to Update: 62 Source: FirstSearch Telephone: N/A Last EDR Contact: 01/03/2013 Next Scheduled EDR Contact: N/A Data Release Frequency: No Update Planned SPILLS 90: SPILLS90 data from FirstSearch Spills 90 includes those spill and release records available exclusively from FirstSearch databases. Typically, they may include chemical, oil and/or hazardous substance spills recorded after 1990. Duplicate records that are already included in EDR incident and release records are not included in Spills 90. Date of Government Version: 09/27/2012 Date Data Arrived at EDR: 01/03/2013 Date Made Active in Reports: 03/06/2013 Number of Days to Update: 62 Source: FirstSearch Telephone: N/A Last EDR Contact: 01/03/2013 Next Scheduled EDR Contact: N/A Data Release Frequency: No Update Planned Other Ascertainable Records RCRA NonGen / NLR: RCRA - Non Generators RCRAInfo is EPA’s comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Non-Generators do not presently generate hazardous waste. Date of Government Version: 03/11/2014 Date Data Arrived at EDR: 03/13/2014 Date Made Active in Reports: 04/09/2014 Number of Days to Update: 27 Source: Environmental Protection Agency Telephone: (404) 562-8651 Last EDR Contact: 07/02/2014 Next Scheduled EDR Contact: 10/13/2014 Data Release Frequency: Varies DOT OPS: Incident and Accident Data Department of Transporation, Office of Pipeline Safety Incident and Accident data. Date of Government Version: 07/31/2012 Date Data Arrived at EDR: 08/07/2012 Date Made Active in Reports: 09/18/2012 Number of Days to Update: 42 Source: Department of Transporation, Office of Pipeline Safety Telephone: 202-366-4595 Last EDR Contact: 05/06/2014 Next Scheduled EDR Contact: 08/18/2014 Data Release Frequency: Varies DOD: Department of Defense Sites This data set consists of federally owned or administered lands, administered by the Department of Defense, that have any area equal to or greater than 640 acres of the United States, Puerto Rico, and the U.S. Virgin Islands. TC4020675.2s Page GR-12 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING Date of Government Version: 12/31/2005 Date Data Arrived at EDR: 11/10/2006 Date Made Active in Reports: 01/11/2007 Number of Days to Update: 62 Source: USGS Telephone: 888-275-8747 Last EDR Contact: 07/18/2014 Next Scheduled EDR Contact: 10/27/2014 Data Release Frequency: Semi-Annually FUDS: Formerly Used Defense Sites The listing includes locations of Formerly Used Defense Sites properties where the US Army Corps of Engineers is actively working or will take necessary cleanup actions. Date of Government Version: 12/31/2012 Date Data Arrived at EDR: 02/28/2014 Date Made Active in Reports: 04/24/2014 Number of Days to Update: 55 Source: U.S. Army Corps of Engineers Telephone: 202-528-4285 Last EDR Contact: 06/04/2014 Next Scheduled EDR Contact: 09/22/2014 Data Release Frequency: Varies CONSENT: Superfund (CERCLA) Consent Decrees Major legal settlements that establish responsibility and standards for cleanup at NPL (Superfund) sites. Released periodically by United States District Courts after settlement by parties to litigation matters. Date of Government Version: 12/31/2013 Date Data Arrived at EDR: 01/24/2014 Date Made Active in Reports: 02/24/2014 Number of Days to Update: 31 Source: Department of Justice, Consent Decree Library Telephone: Varies Last EDR Contact: 06/30/2014 Next Scheduled EDR Contact: 10/13/2014 Data Release Frequency: Varies ROD: Records Of Decision Record of Decision. ROD documents mandate a permanent remedy at an NPL (Superfund) site containing technical and health information to aid in the cleanup. Date of Government Version: 11/25/2013 Date Data Arrived at EDR: 12/12/2013 Date Made Active in Reports: 02/24/2014 Number of Days to Update: 74 Source: EPA Telephone: 703-416-0223 Last EDR Contact: 06/10/2014 Next Scheduled EDR Contact: 09/22/2014 Data Release Frequency: Annually UMTRA: Uranium Mill Tailings Sites Uranium ore was mined by private companies for federal government use in national defense programs. When the mills shut down, large piles of the sand-like material (mill tailings) remain after uranium has been extracted from the ore. Levels of human exposure to radioactive materials from the piles are low; however, in some cases tailings were used as construction materials before the potential health hazards of the tailings were recognized. Date of Government Version: 09/14/2010 Date Data Arrived at EDR: 10/07/2011 Date Made Active in Reports: 03/01/2012 Number of Days to Update: 146 Source: Department of Energy Telephone: 505-845-0011 Last EDR Contact: 02/25/2014 Next Scheduled EDR Contact: 06/09/2014 Data Release Frequency: Varies US MINES: Mines Master Index File Contains all mine identification numbers issued for mines active or opened since 1971. The data also includes violation information. Date of Government Version: 01/30/2014 Date Data Arrived at EDR: 03/05/2014 Date Made Active in Reports: 07/15/2014 Number of Days to Update: 132 Source: Department of Labor, Mine Safety and Health Administration Telephone: 303-231-5959 Last EDR Contact: 06/06/2014 Next Scheduled EDR Contact: 09/15/2014 Data Release Frequency: Semi-Annually TRIS: Toxic Chemical Release Inventory System Toxic Release Inventory System. TRIS identifies facilities which release toxic chemicals to the air, water and land in reportable quantities under SARA Title III Section 313. TC4020675.2s Page GR-13 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING Date of Government Version: 12/31/2011 Date Data Arrived at EDR: 07/31/2013 Date Made Active in Reports: 09/13/2013 Number of Days to Update: 44 Source: EPA Telephone: 202-566-0250 Last EDR Contact: 05/30/2014 Next Scheduled EDR Contact: 09/08/2014 Data Release Frequency: Annually TSCA: Toxic Substances Control Act Toxic Substances Control Act. TSCA identifies manufacturers and importers of chemical substances included on the TSCA Chemical Substance Inventory list. It includes data on the production volume of these substances by plant site. Date of Government Version: 12/31/2006 Date Data Arrived at EDR: 09/29/2010 Date Made Active in Reports: 12/02/2010 Number of Days to Update: 64 Source: EPA Telephone: 202-260-5521 Last EDR Contact: 06/25/2014 Next Scheduled EDR Contact: 10/06/2014 Data Release Frequency: Every 4 Years FTTS: FIFRA/ TSCA Tracking System - FIFRA (Federal Insecticide, Fungicide, & Rodenticide Act)/TSCA (Toxic Substances Control Act) FTTS tracks administrative cases and pesticide enforcement actions and compliance activities related to FIFRA, TSCA and EPCRA (Emergency Planning and Community Right-to-Know Act). To maintain currency, EDR contacts the Agency on a quarterly basis. Date of Government Version: 04/09/2009 Date Data Arrived at EDR: 04/16/2009 Date Made Active in Reports: 05/11/2009 Number of Days to Update: 25 Source: EPA/Office of Prevention, Pesticides and Toxic Substances Telephone: 202-566-1667 Last EDR Contact: 05/22/2014 Next Scheduled EDR Contact: 09/08/2014 Data Release Frequency: Quarterly FTTS INSP: FIFRA/ TSCA Tracking System - FIFRA (Federal Insecticide, Fungicide, & Rodenticide Act)/TSCA (Toxic Substances Control Act) A listing of FIFRA/TSCA Tracking System (FTTS) inspections and enforcements. Date of Government Version: 04/09/2009 Date Data Arrived at EDR: 04/16/2009 Date Made Active in Reports: 05/11/2009 Number of Days to Update: 25 Source: EPA Telephone: 202-566-1667 Last EDR Contact: 05/22/2014 Next Scheduled EDR Contact: 09/08/2014 Data Release Frequency: Quarterly HIST FTTS: FIFRA/TSCA Tracking System Administrative Case Listing A complete administrative case listing from the FIFRA/TSCA Tracking System (FTTS) for all ten EPA regions. The information was obtained from the National Compliance Database (NCDB). NCDB supports the implementation of FIFRA (Federal Insecticide, Fungicide, and Rodenticide Act) and TSCA (Toxic Substances Control Act). Some EPA regions are now closing out records. Because of that, and the fact that some EPA regions are not providing EPA Headquarters with updated records, it was decided to create a HIST FTTS database. It included records that may not be included in the newer FTTS database updates. This database is no longer updated. Date of Government Version: 10/19/2006 Date Data Arrived at EDR: 03/01/2007 Date Made Active in Reports: 04/10/2007 Number of Days to Update: 40 Source: Environmental Protection Agency Telephone: 202-564-2501 Last EDR Contact: 12/17/2007 Next Scheduled EDR Contact: 03/17/2008 Data Release Frequency: No Update Planned HIST FTTS INSP: FIFRA/TSCA Tracking System Inspection & Enforcement Case Listing A complete inspection and enforcement case listing from the FIFRA/TSCA Tracking System (FTTS) for all ten EPA regions. The information was obtained from the National Compliance Database (NCDB). NCDB supports the implementation of FIFRA (Federal Insecticide, Fungicide, and Rodenticide Act) and TSCA (Toxic Substances Control Act). Some EPA regions are now closing out records. Because of that, and the fact that some EPA regions are not providing EPA Headquarters with updated records, it was decided to create a HIST FTTS database. It included records that may not be included in the newer FTTS database updates. This database is no longer updated. TC4020675.2s Page GR-14 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING Date of Government Version: 10/19/2006 Date Data Arrived at EDR: 03/01/2007 Date Made Active in Reports: 04/10/2007 Number of Days to Update: 40 Source: Environmental Protection Agency Telephone: 202-564-2501 Last EDR Contact: 12/17/2008 Next Scheduled EDR Contact: 03/17/2008 Data Release Frequency: No Update Planned SSTS: Section 7 Tracking Systems Section 7 of the Federal Insecticide, Fungicide and Rodenticide Act, as amended (92 Stat. 829) requires all registered pesticide-producing establishments to submit a report to the Environmental Protection Agency by March 1st each year. Each establishment must report the types and amounts of pesticides, active ingredients and devices being produced, and those having been produced and sold or distributed in the past year. Date of Government Version: 12/31/2009 Date Data Arrived at EDR: 12/10/2010 Date Made Active in Reports: 02/25/2011 Number of Days to Update: 77 Source: EPA Telephone: 202-564-4203 Last EDR Contact: 07/22/2014 Next Scheduled EDR Contact: 11/10/2014 Data Release Frequency: Annually ICIS: Integrated Compliance Information System The Integrated Compliance Information System (ICIS) supports the information needs of the national enforcement and compliance program as well as the unique needs of the National Pollutant Discharge Elimination System (NPDES) program. Date of Government Version: 05/06/2014 Date Data Arrived at EDR: 05/16/2014 Date Made Active in Reports: 06/17/2014 Number of Days to Update: 32 Source: Environmental Protection Agency Telephone: 202-564-5088 Last EDR Contact: 10/09/2014 Next Scheduled EDR Contact: 10/27/2014 Data Release Frequency: Quarterly PADS: PCB Activity Database System PCB Activity Database. PADS Identifies generators, transporters, commercial storers and/or brokers and disposers of PCB’s who are required to notify the EPA of such activities. Date of Government Version: 06/01/2013 Date Data Arrived at EDR: 07/17/2013 Date Made Active in Reports: 11/01/2013 Number of Days to Update: 107 Source: EPA Telephone: 202-566-0500 Last EDR Contact: 07/18/2014 Next Scheduled EDR Contact: 10/27/2014 Data Release Frequency: Annually MLTS: Material Licensing Tracking System MLTS is maintained by the Nuclear Regulatory Commission and contains a list of approximately 8,100 sites which possess or use radioactive materials and which are subject to NRC licensing requirements. To maintain currency, EDR contacts the Agency on a quarterly basis. Date of Government Version: 07/22/2013 Date Data Arrived at EDR: 08/02/2013 Date Made Active in Reports: 11/01/2013 Number of Days to Update: 91 Source: Nuclear Regulatory Commission Telephone: 301-415-7169 Last EDR Contact: 06/05/2014 Next Scheduled EDR Contact: 09/22/2014 Data Release Frequency: Quarterly RADINFO: Radiation Information Database The Radiation Information Database (RADINFO) contains information about facilities that are regulated by U.S. Environmental Protection Agency (EPA) regulations for radiation and radioactivity. Date of Government Version: 07/07/2014 Date Data Arrived at EDR: 07/10/2014 Date Made Active in Reports: 07/28/2014 Number of Days to Update: 18 Source: Environmental Protection Agency Telephone: 202-343-9775 Last EDR Contact: 07/10/2014 Next Scheduled EDR Contact: 10/20/2014 Data Release Frequency: Quarterly TC4020675.2s Page GR-15 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING FINDS: Facility Index System/Facility Registry System Facility Index System. FINDS contains both facility information and ’pointers’ to other sources that contain more detail. EDR includes the following FINDS databases in this report: PCS (Permit Compliance System), AIRS (Aerometric Information Retrieval System), DOCKET (Enforcement Docket used to manage and track information on civil judicial enforcement cases for all environmental statutes), FURS (Federal Underground Injection Control), C-DOCKET (Criminal Docket System used to track criminal enforcement actions for all environmental statutes), FFIS (Federal Facilities Information System), STATE (State Environmental Laws and Statutes), and PADS (PCB Activity Data System). Date of Government Version: 11/18/2013 Date Data Arrived at EDR: 02/27/2014 Date Made Active in Reports: 03/12/2014 Number of Days to Update: 13 Source: EPA Telephone: (404) 562-9900 Last EDR Contact: 06/13/2014 Next Scheduled EDR Contact: 09/22/2014 Data Release Frequency: Quarterly RAATS: RCRA Administrative Action Tracking System RCRA Administration Action Tracking System. RAATS contains records based on enforcement actions issued under RCRA pertaining to major violators and includes administrative and civil actions brought by the EPA. For administration actions after September 30, 1995, data entry in the RAATS database was discontinued. EPA will retain a copy of the database for historical records. It was necessary to terminate RAATS because a decrease in agency resources made it impossible to continue to update the information contained in the database. Date of Government Version: 04/17/1995 Date Data Arrived at EDR: 07/03/1995 Date Made Active in Reports: 08/07/1995 Number of Days to Update: 35 Source: EPA Telephone: 202-564-4104 Last EDR Contact: 06/02/2008 Next Scheduled EDR Contact: 09/01/2008 Data Release Frequency: No Update Planned RMP: Risk Management Plans When Congress passed the Clean Air Act Amendments of 1990, it required EPA to publish regulations and guidance for chemical accident prevention at facilities using extremely hazardous substances. The Risk Management Program Rule (RMP Rule) was written to implement Section 112(r) of these amendments. The rule, which built upon existing industry codes and standards, requires companies of all sizes that use certain flammable and toxic substances to develop a Risk Management Program, which includes a(n): Hazard assessment that details the potential effects of an accidental release, an accident history of the last five years, and an evaluation of worst-case and alternative accidental releases; Prevention program that includes safety precautions and maintenance, monitoring, and employee training measures; and Emergency response program that spells out emergency health care, employee training measures and procedures for informing the public and response agencies (e.g the fire department) should an accident occur. Date of Government Version: 04/01/2014 Date Data Arrived at EDR: 05/23/2014 Date Made Active in Reports: 07/28/2014 Number of Days to Update: 66 Source: Environmental Protection Agency Telephone: 202-564-8600 Last EDR Contact: 07/22/2014 Next Scheduled EDR Contact: 11/10/2014 Data Release Frequency: Varies BRS: Biennial Reporting System The Biennial Reporting System is a national system administered by the EPA that collects data on the generation and management of hazardous waste. BRS captures detailed data from two groups: Large Quantity Generators (LQG) and Treatment, Storage, and Disposal Facilities. Date of Government Version: 12/31/2011 Date Data Arrived at EDR: 02/26/2013 Date Made Active in Reports: 04/19/2013 Number of Days to Update: 52 Source: EPA/NTIS Telephone: 800-424-9346 Last EDR Contact: 05/30/2014 Next Scheduled EDR Contact: 09/08/2014 Data Release Frequency: Biennially UIC: Underground Injection Wells Listing A listing of uncerground injection wells locations. Date of Government Version: 05/07/2014 Date Data Arrived at EDR: 05/14/2014 Date Made Active in Reports: 05/19/2014 Number of Days to Update: 5 Source: Department of Environment & Natural Resources Telephone: 919-807-6412 Last EDR Contact: 05/12/2014 Next Scheduled EDR Contact: 08/25/2014 Data Release Frequency: Varies TC4020675.2s Page GR-16 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING DRYCLEANERS: Drycleaning Sites Potential and known drycleaning sites, active and abandoned, that the Drycleaning Solvent Cleanup Program has knowledge of and entered into this database. Date of Government Version: 05/14/2014 Date Data Arrived at EDR: 06/25/2014 Date Made Active in Reports: 07/14/2014 Number of Days to Update: 19 Source: Department of Environment & Natural Resources Telephone: 919-508-8400 Last EDR Contact: 06/25/2014 Next Scheduled EDR Contact: 10/06/2014 Data Release Frequency: Varies NPDES: NPDES Facility Location Listing General information regarding NPDES(National Pollutant Discharge Elimination System) permits. Date of Government Version: 05/07/2014 Date Data Arrived at EDR: 06/06/2014 Date Made Active in Reports: 07/17/2014 Number of Days to Update: 41 Source: Department of Environment & Natural Resources Telephone: 919-733-7015 Last EDR Contact: 06/06/2014 Next Scheduled EDR Contact: 08/18/2014 Data Release Frequency: Varies INDIAN RESERV: Indian Reservations This map layer portrays Indian administered lands of the United States that have any area equal to or greater than 640 acres. Date of Government Version: 12/31/2005 Date Data Arrived at EDR: 12/08/2006 Date Made Active in Reports: 01/11/2007 Number of Days to Update: 34 Source: USGS Telephone: 202-208-3710 Last EDR Contact: 07/18/2014 Next Scheduled EDR Contact: 10/27/2014 Data Release Frequency: Semi-Annually SCRD DRYCLEANERS: State Coalition for Remediation of Drycleaners Listing The State Coalition for Remediation of Drycleaners was established in 1998, with support from the U.S. EPA Office of Superfund Remediation and Technology Innovation. It is comprised of representatives of states with established drycleaner remediation programs. Currently the member states are Alabama, Connecticut, Florida, Illinois, Kansas, Minnesota, Missouri, North Carolina, Oregon, South Carolina, Tennessee, Texas, and Wisconsin. Date of Government Version: 03/07/2011 Date Data Arrived at EDR: 03/09/2011 Date Made Active in Reports: 05/02/2011 Number of Days to Update: 54 Source: Environmental Protection Agency Telephone: 615-532-8599 Last EDR Contact: 07/25/2014 Next Scheduled EDR Contact: 11/03/2014 Data Release Frequency: Varies PRP: Potentially Responsible Parties A listing of verified Potentially Responsible Parties Date of Government Version: 04/15/2013 Date Data Arrived at EDR: 07/03/2013 Date Made Active in Reports: 09/13/2013 Number of Days to Update: 72 Source: EPA Telephone: 202-564-6023 Last EDR Contact: 07/01/2014 Next Scheduled EDR Contact: 10/13/2014 Data Release Frequency: Quarterly LEAD SMELTER 2: Lead Smelter Sites A list of several hundred sites in the U.S. where secondary lead smelting was done from 1931and 1964. These sites may pose a threat to public health through ingestion or inhalation of contaminated soil or dust Date of Government Version: 04/05/2001 Date Data Arrived at EDR: 10/27/2010 Date Made Active in Reports: 12/02/2010 Number of Days to Update: 36 Source: American Journal of Public Health Telephone: 703-305-6451 Last EDR Contact: 12/02/2009 Next Scheduled EDR Contact: N/A Data Release Frequency: No Update Planned TC4020675.2s Page GR-17 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING Financial Assurance 3: Financial Assurance Information Hazardous waste financial assurance information. Date of Government Version: 09/30/2012 Date Data Arrived at EDR: 10/19/2012 Date Made Active in Reports: 11/29/2012 Number of Days to Update: 41 Source: Department of Environment & Natural Resources Telephone: 919-707-8222 Last EDR Contact: 06/11/2014 Next Scheduled EDR Contact: 09/29/2014 Data Release Frequency: Varies 2020 COR ACTION: 2020 Corrective Action Program List The EPA has set ambitious goals for the RCRA Corrective Action program by creating the 2020 Corrective Action Universe. This RCRA cleanup baseline includes facilities expected to need corrective action. The 2020 universe contains a wide variety of sites. Some properties are heavily contaminated while others were contaminated but have since been cleaned up. Still others have not been fully investigated yet, and may require little or no remediation. Inclusion in the 2020 Universe does not necessarily imply failure on the part of a facility to meet its RCRA obligations. Date of Government Version: 11/11/2011 Date Data Arrived at EDR: 05/18/2012 Date Made Active in Reports: 05/25/2012 Number of Days to Update: 7 Source: Environmental Protection Agency Telephone: 703-308-4044 Last EDR Contact: 05/16/2014 Next Scheduled EDR Contact: 08/25/2014 Data Release Frequency: Varies LEAD SMELTER 1: Lead Smelter Sites A listing of former lead smelter site locations. Date of Government Version: 06/04/2014 Date Data Arrived at EDR: 06/12/2014 Date Made Active in Reports: 07/28/2014 Number of Days to Update: 46 Source: Environmental Protection Agency Telephone: 703-603-8787 Last EDR Contact: 07/01/2014 Next Scheduled EDR Contact: 10/20/2014 Data Release Frequency: Varies EPA WATCH LIST: EPA WATCH LIST EPA maintains a "Watch List" to facilitate dialogue between EPA, state and local environmental agencies on enforcement matters relating to facilities with alleged violations identified as either significant or high priority. Being on the Watch List does not mean that the facility has actually violated the law only that an investigation by EPA or a state or local environmental agency has led those organizations to allege that an unproven violation has in fact occurred. Being on the Watch List does not represent a higher level of concern regarding the alleged violations that were detected, but instead indicates cases requiring additional dialogue between EPA, state and local agencies - primarily because of the length of time the alleged violation has gone unaddressed or unresolved. Date of Government Version: 08/30/2013 Date Data Arrived at EDR: 03/21/2014 Date Made Active in Reports: 06/17/2014 Number of Days to Update: 88 Source: Environmental Protection Agency Telephone: 617-520-3000 Last EDR Contact: 05/16/2014 Next Scheduled EDR Contact: 08/25/2014 Data Release Frequency: Quarterly US FIN ASSUR: Financial Assurance Information All owners and operators of facilities that treat, store, or dispose of hazardous waste are required to provide proof that they will have sufficient funds to pay for the clean up, closure, and post-closure care of their facilities. Date of Government Version: 06/19/2014 Date Data Arrived at EDR: 06/20/2014 Date Made Active in Reports: 07/28/2014 Number of Days to Update: 38 Source: Environmental Protection Agency Telephone: 202-566-1917 Last EDR Contact: 05/16/2014 Next Scheduled EDR Contact: 09/01/2014 Data Release Frequency: Quarterly Financial Assurance 2: Financial Assurance Information Listing Information for solid waste facilities. Financial assurance is intended to ensure that resources are available to pay for the cost of closure, post-closure care, and corrective measures if the owner or operator of a regulated facility is unable or unwilling to pay. TC4020675.2s Page GR-18 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING Date of Government Version: 10/02/2012 Date Data Arrived at EDR: 10/03/2012 Date Made Active in Reports: 10/26/2012 Number of Days to Update: 23 Source: Department of Environmental & Natural Resources Telephone: 919-508-8496 Last EDR Contact: 06/30/2014 Next Scheduled EDR Contact: 10/13/2014 Data Release Frequency: Varies COAL ASH: Coal Ash Disposal Sites A listing of coal combustion products distribution permits issued by the Division for the treatment, storage, transportation, use and disposal of coal combustion products. Date of Government Version: 12/31/2007 Date Data Arrived at EDR: 08/04/2009 Date Made Active in Reports: 08/17/2009 Number of Days to Update: 13 Source: Department of Environment & Natural Resources Telephone: 919-807-6359 Last EDR Contact: 05/05/2014 Next Scheduled EDR Contact: 08/18/2014 Data Release Frequency: Varies COAL ASH DOE: Sleam-Electric Plan Operation Data A listing of power plants that store ash in surface ponds. Date of Government Version: 12/31/2005 Date Data Arrived at EDR: 08/07/2009 Date Made Active in Reports: 10/22/2009 Number of Days to Update: 76 Source: Department of Energy Telephone: 202-586-8719 Last EDR Contact: 07/18/2014 Next Scheduled EDR Contact: 10/27/2014 Data Release Frequency: Varies FEDLAND: Federal and Indian Lands Federally and Indian administrated lands of the United States. Lands included are administrated by: Army Corps of Engineers, Bureau of Reclamation, National Wild and Scenic River, National Wildlife Refuge, Public Domain Land, Wilderness, Wilderness Study Area, Wildlife Management Area, Bureau of Indian Affairs, Bureau of Land Management, Department of Justice, Forest Service, Fish and Wildlife Service, National Park Service. Date of Government Version: 12/31/2005 Date Data Arrived at EDR: 02/06/2006 Date Made Active in Reports: 01/11/2007 Number of Days to Update: 339 Source: U.S. Geological Survey Telephone: 888-275-8747 Last EDR Contact: 07/18/2014 Next Scheduled EDR Contact: 10/27/2014 Data Release Frequency: N/A US AIRS (AFS): Aerometric Information Retrieval System Facility Subsystem (AFS) The database is a sub-system of Aerometric Information Retrieval System (AIRS). AFS contains compliance data on air pollution point sources regulated by the U.S. EPA and/or state and local air regulatory agencies. This information comes from source reports by various stationary sources of air pollution, such as electric power plants, steel mills, factories, and universities, and provides information about the air pollutants they produce. Action, air program, air program pollutant, and general level plant data. It is used to track emissions and compliance data from industrial plants. Date of Government Version: 10/23/2013 Date Data Arrived at EDR: 11/06/2013 Date Made Active in Reports: 12/06/2013 Number of Days to Update: 30 Source: EPA Telephone: 202-564-2496 Last EDR Contact: 06/25/2014 Next Scheduled EDR Contact: 10/13/2014 Data Release Frequency: Annually US AIRS MINOR: Air Facility System Data A listing of minor source facilities. Date of Government Version: 10/23/2013 Date Data Arrived at EDR: 11/06/2013 Date Made Active in Reports: 12/06/2013 Number of Days to Update: 30 Source: EPA Telephone: 202-564-2496 Last EDR Contact: 06/25/2014 Next Scheduled EDR Contact: 10/13/2014 Data Release Frequency: Annually TC4020675.2s Page GR-19 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING Financial Assurance 1: Financial Assurance Information Listing A listing of financial assurance information for underground storage tank facilities. Financial assurance is intended to ensure that resources are available to pay for the cost of closure, post-closure care, and corrective measures if the owner or operator of a regulated facility is unable or unwilling to pay. Date of Government Version: 06/03/2014 Date Data Arrived at EDR: 06/05/2014 Date Made Active in Reports: 07/11/2014 Number of Days to Update: 36 Source: Department of Environment & Natural Resources Telephone: 919-733-1322 Last EDR Contact: 05/14/2014 Next Scheduled EDR Contact: 08/25/2014 Data Release Frequency: Quarterly COAL ASH EPA: Coal Combustion Residues Surface Impoundments List A listing of coal combustion residues surface impoundments with high hazard potential ratings. Date of Government Version: 03/14/2014 Date Data Arrived at EDR: 06/11/2014 Date Made Active in Reports: 07/28/2014 Number of Days to Update: 47 Source: Environmental Protection Agency Telephone: N/A Last EDR Contact: 06/11/2014 Next Scheduled EDR Contact: 09/22/2014 Data Release Frequency: Varies PCB TRANSFORMER: PCB Transformer Registration Database The database of PCB transformer registrations that includes all PCB registration submittals. Date of Government Version: 02/01/2011 Date Data Arrived at EDR: 10/19/2011 Date Made Active in Reports: 01/10/2012 Number of Days to Update: 83 Source: Environmental Protection Agency Telephone: 202-566-0517 Last EDR Contact: 05/02/2014 Next Scheduled EDR Contact: 08/11/2014 Data Release Frequency: Varies EDR HIGH RISK HISTORICAL RECORDS EDR Exclusive Records EDR MGP: EDR Proprietary Manufactured Gas Plants The EDR Proprietary Manufactured Gas Plant Database includes records of coal gas plants (manufactured gas plants) compiled by EDR’s researchers. Manufactured gas sites were used in the United States from the 1800’s to 1950’s to produce a gas that could be distributed and used as fuel. These plants used whale oil, rosin, coal, or a mixture of coal, oil, and water that also produced a significant amount of waste. Many of the byproducts of the gas production, such as coal tar (oily waste containing volatile and non-volatile chemicals), sludges, oils and other compounds are potentially hazardous to human health and the environment. The byproduct from this process was frequently disposed of directly at the plant site and can remain or spread slowly, serving as a continuous source of soil and groundwater contamination. Date of Government Version: N/A Date Data Arrived at EDR: N/A Date Made Active in Reports: N/A Number of Days to Update: N/A Source: EDR, Inc. Telephone: N/A Last EDR Contact: N/A Next Scheduled EDR Contact: N/A Data Release Frequency: No Update Planned EDR US Hist Auto Stat: EDR Exclusive Historic Gas Stations EDR has searched selected national collections of business directories and has collected listings of potential gas station/filling station/service station sites that were available to EDR researchers. EDR’s review was limited to those categories of sources that might, in EDR’s opinion, include gas station/filling station/service station establishments. The categories reviewed included, but were not limited to gas, gas station, gasoline station, filling station, auto, automobile repair, auto service station, service station, etc. This database falls within a category of information EDR classifies as "High Risk Historical Records", or HRHR. EDR’s HRHR effort presents unique and sometimes proprietary data about past sites and operations that typically create environmental concerns, but may not show up in current government records searches. Date of Government Version: N/A Date Data Arrived at EDR: N/A Date Made Active in Reports: N/A Number of Days to Update: N/A Source: EDR, Inc. Telephone: N/A Last EDR Contact: N/A Next Scheduled EDR Contact: N/A Data Release Frequency: Varies TC4020675.2s Page GR-20 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING EDR US Hist Cleaners: EDR Exclusive Historic Dry Cleaners EDR has searched selected national collections of business directories and has collected listings of potential dry cleaner sites that were available to EDR researchers. EDR’s review was limited to those categories of sources that might, in EDR’s opinion, include dry cleaning establishments. The categories reviewed included, but were not limited to dry cleaners, cleaners, laundry, laundromat, cleaning/laundry, wash & dry etc. This database falls within a category of information EDR classifies as "High Risk Historical Records", or HRHR. EDR’s HRHR effort presents unique and sometimes proprietary data about past sites and operations that typically create environmental concerns, but may not show up in current government records searches. Date of Government Version: N/A Date Data Arrived at EDR: N/A Date Made Active in Reports: N/A Number of Days to Update: N/A Source: EDR, Inc. Telephone: N/A Last EDR Contact: N/A Next Scheduled EDR Contact: N/A Data Release Frequency: Varies EDR RECOVERED GOVERNMENT ARCHIVES Exclusive Recovered Govt. Archives RGA HWS: Recovered Government Archive State Hazardous Waste Facilities List The EDR Recovered Government Archive State Hazardous Waste database provides a list of SHWS incidents derived from historical databases and includes many records that no longer appear in current government lists. Compiled from Records formerly available from the Department of Environment, Health and Natural Resources in North Carolina. Date of Government Version: N/A Date Data Arrived at EDR: 07/01/2013 Date Made Active in Reports: 12/24/2013 Number of Days to Update: 176 Source: Department of Environment, Health and Natural Resources Telephone: N/A Last EDR Contact: 06/01/2012 Next Scheduled EDR Contact: N/A Data Release Frequency: Varies RGA LUST: Recovered Government Archive Leaking Underground Storage Tank The EDR Recovered Government Archive Leaking Underground Storage Tank database provides a list of LUST incidents derived from historical databases and includes many records that no longer appear in current government lists. Compiled from Records formerly available from the Department of Environment, Health and Natural Resources in North Carolina. Date of Government Version: N/A Date Data Arrived at EDR: 07/01/2013 Date Made Active in Reports: 12/20/2013 Number of Days to Update: 172 Source: Department of Environment, Health and Natural Resources Telephone: N/A Last EDR Contact: 06/01/2012 Next Scheduled EDR Contact: N/A Data Release Frequency: Varies RGA LF: Recovered Government Archive Solid Waste Facilities List The EDR Recovered Government Archive Landfill database provides a list of landfills derived from historical databases and includes many records that no longer appear in current government lists. Compiled from Records formerly available from the Department of Environment, Health and Natural Resources in North Carolina. Date of Government Version: N/A Date Data Arrived at EDR: 07/01/2013 Date Made Active in Reports: 01/13/2014 Number of Days to Update: 196 Source: Department of Environment, Health and Natural Resources Telephone: N/A Last EDR Contact: 06/01/2012 Next Scheduled EDR Contact: N/A Data Release Frequency: Varies OTHER DATABASE(S) Depending on the geographic area covered by this report, the data provided in these specialty databases may or may not be complete. For example, the existence of wetlands information data in a specific report does not mean that all wetlands in the area covered by the report are included. Moreover, the absence of any reported wetlands information does not necessarily mean that wetlands do not exist in the area covered by the report. TC4020675.2s Page GR-21 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING CT MANIFEST: Hazardous Waste Manifest Data Facility and manifest data. Manifest is a document that lists and tracks hazardous waste from the generator through transporters to a tsd facility. Date of Government Version: 07/30/2013 Date Data Arrived at EDR: 08/19/2013 Date Made Active in Reports: 10/03/2013 Number of Days to Update: 45 Source: Department of Energy & Environmental Protection Telephone: 860-424-3375 Last EDR Contact: 05/23/2014 Next Scheduled EDR Contact: 09/01/2014 Data Release Frequency: Annually NJ MANIFEST: Manifest Information Hazardous waste manifest information. Date of Government Version: 12/31/2011 Date Data Arrived at EDR: 07/19/2012 Date Made Active in Reports: 08/28/2012 Number of Days to Update: 40 Source: Department of Environmental Protection Telephone: N/A Last EDR Contact: 07/17/2014 Next Scheduled EDR Contact: 10/27/2014 Data Release Frequency: Annually NY MANIFEST: Facility and Manifest Data Manifest is a document that lists and tracks hazardous waste from the generator through transporters to a TSD facility. Date of Government Version: 05/01/2014 Date Data Arrived at EDR: 05/07/2014 Date Made Active in Reports: 06/10/2014 Number of Days to Update: 34 Source: Department of Environmental Conservation Telephone: 518-402-8651 Last EDR Contact: 05/07/2014 Next Scheduled EDR Contact: 08/18/2014 Data Release Frequency: Annually PA MANIFEST: Manifest Information Hazardous waste manifest information. Date of Government Version: 12/31/2012 Date Data Arrived at EDR: 07/24/2013 Date Made Active in Reports: 08/19/2013 Number of Days to Update: 26 Source: Department of Environmental Protection Telephone: 717-783-8990 Last EDR Contact: 07/18/2014 Next Scheduled EDR Contact: 11/03/2014 Data Release Frequency: Annually RI MANIFEST: Manifest information Hazardous waste manifest information Date of Government Version: 12/31/2012 Date Data Arrived at EDR: 06/21/2013 Date Made Active in Reports: 08/05/2013 Number of Days to Update: 45 Source: Department of Environmental Management Telephone: 401-222-2797 Last EDR Contact: 05/27/2014 Next Scheduled EDR Contact: 09/08/2014 Data Release Frequency: Annually WI MANIFEST: Manifest Information Hazardous waste manifest information. Date of Government Version: 12/31/2012 Date Data Arrived at EDR: 08/09/2013 Date Made Active in Reports: 09/27/2013 Number of Days to Update: 49 Source: Department of Natural Resources Telephone: N/A Last EDR Contact: 06/16/2014 Next Scheduled EDR Contact: 09/29/2014 Data Release Frequency: Annually Oil/Gas Pipelines: This data was obtained by EDR from the USGS in 1994. It is referred to by USGS as GeoData Digital Line Graphs from 1:100,000-Scale Maps. It was extracted from the transportation category including some oil, but primarily gas pipelines. Sensitive Receptors: There are individuals deemed sensitive receptors due to their fragile immune systems and special sensitivity to environmental discharges. These sensitive receptors typically include the elderly, the sick, and children. While the location of all sensitive receptors cannot be determined, EDR indicates those buildings and facilities - schools, daycares, hospitals, medical centers, and nursing homes - where individuals who are sensitive receptors are likely to be located. TC4020675.2s Page GR-22 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING AHA Hospitals: Source: American Hospital Association, Inc. Telephone: 312-280-5991 The database includes a listing of hospitals based on the American Hospital Association’s annual survey of hospitals. Medical Centers: Provider of Services Listing Source: Centers for Medicare & Medicaid Services Telephone: 410-786-3000 A listing of hospitals with Medicare provider number, produced by Centers of Medicare & Medicaid Services, a federal agency within the U.S. Department of Health and Human Services. Nursing Homes Source: National Institutes of Health Telephone: 301-594-6248 Information on Medicare and Medicaid certified nursing homes in the United States. Public Schools Source: National Center for Education Statistics Telephone: 202-502-7300 The National Center for Education Statistics’ primary database on elementary and secondary public education in the United States. It is a comprehensive, annual, national statistical database of all public elementary and secondary schools and school districts, which contains data that are comparable across all states. Private Schools Source: National Center for Education Statistics Telephone: 202-502-7300 The National Center for Education Statistics’ primary database on private school locations in the United States. Daycare Centers: Child Care Facility List Source: Department of Health & Human Services Telephone: 919-662-4499 Flood Zone Data: This data, available in select counties across the country, was obtained by EDR in 2003 & 2011 from the Federal Emergency Management Agency (FEMA). Data depicts 100-year and 500-year flood zones as defined by FEMA. NWI: National Wetlands Inventory. This data, available in select counties across the country, was obtained by EDR in 2002, 2005 and 2010 from the U.S. Fish and Wildlife Service. State Wetlands Data: Wetlands Inventory Source: Department of Environment & Natural Resources Telephone: 919-733-2090 Scanned Digital USGS 7.5’ Topographic Map (DRG) Source: United States Geologic Survey A digital raster graphic (DRG) is a scanned image of a U.S. Geological Survey topographic map. The map images are made by scanning published paper maps on high-resolution scanners. The raster image is georeferenced and fit to the Universal Transverse Mercator (UTM) projection. STREET AND ADDRESS INFORMATION © 2010 Tele Atlas North America, Inc. All rights reserved. This material is proprietary and the subject of copyright protection and other intellectual property rights owned by or licensed to Tele Atlas North America, Inc. The use of this material is subject to the terms of a license agreement. You will be held liable for any unauthorized copying or disclosure of this material. TC4020675.2s Page GR-23 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING TC4020675.2s Page A-1 geologic strata. of the soil, and nearby wells. Groundwater flow velocity is generally impacted by the nature of the Groundwater flow direction may be impacted by surface topography, hydrology, hydrogeology, characteristics 2. Groundwater flow velocity. 1. Groundwater flow direction, and Assessment of the impact of contaminant migration generally has two principal investigative components: forming an opinion about the impact of potential contaminant migration. EDR’s GeoCheck Physical Setting Source Addendum is provided to assist the environmental professional in 1994Most Recent Revision: 36081-A7 GRANDFATHER MOUNTAIN, NCEast Map: 1994Most Recent Revision: 36081-A8 NEWLAND, NCTarget Property Map: USGS TOPOGRAPHIC MAP 3588 ft. above sea levelElevation: 3989191.5UTM Y (Meters): 420127.2UTM X (Meters): Zone 17Universal Tranverse Mercator: 81.8867 - 81˚ 53’ 12.12’’Longitude (West): 36.0458 - 36˚ 2’ 44.88’’Latitude (North): TARGET PROPERTY COORDINATES NEWLAND, NC 28657 1600 LINVILLE FALLS HIGHWAY C&E MANUFACTURING TARGET PROPERTY ADDRESS ®GEOCHECK - PHYSICAL SETTING SOURCE ADDENDUM® TC4020675.2s Page A-2 should be field verified. on a relative (not an absolute) basis. Relative elevation information between sites of close proximity Source: Topography has been determined from the USGS 7.5’ Digital Elevation Model and should be evaluated SURROUNDING TOPOGRAPHY: ELEVATION PROFILES El e v a t i o n ( f t ) El e v a t i o n ( f t ) TP TP 0 1/2 1 Miles✩Target Property Elevation: 3588 ft. North South West East 3 7 1 5 3 5 9 3 3 5 5 9 3 5 3 0 3 5 1 6 3 5 2 1 3 5 6 1 3 5 6 1 3 5 9 0 3 5 8 8 3 5 6 1 3 5 6 0 3 5 7 2 3 5 8 8 3 6 0 0 3 6 1 9 3 8 0 7 3 9 5 7 3 8 9 0 3 6 5 7 3 6 3 7 3 6 8 8 3 6 3 1 3 6 0 4 3 5 5 2 3 5 4 8 3 5 4 8 3 6 7 9 3 5 8 8 3 5 9 1 3 6 7 2 3 6 1 4 3 6 3 7 3 6 7 5 3 7 3 6 3 8 6 7 4 0 6 1 3 9 6 5 General WestGeneral Topographic Gradient: TARGET PROPERTY TOPOGRAPHY should contamination exist on the target property, what downgradient sites might be impacted. assist the environmental professional in forming an opinion about the impact of nearby contaminated properties or, Surface topography may be indicative of the direction of surficial groundwater flow. This information can be used to TOPOGRAPHIC INFORMATION collected on nearby properties, and regional groundwater flow information (from deep aquifers). sources of information, such as surface topographic information, hydrologic information, hydrogeologic data using site-specific well data. If such data is not reasonably ascertainable, it may be necessary to rely on other Groundwater flow direction for a particular site is best determined by a qualified environmental professional GROUNDWATER FLOW DIRECTION INFORMATION ®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY® TC4020675.2s Page A-3 Not Reported GENERAL DIRECTIONLOCATION GROUNDWATER FLOWFROM TPMAP ID hydrogeologically, and the depth to water table. authorities at select sites and has extracted the date of the report, groundwater flow direction as determined flow at specific points. EDR has reviewed reports submitted by environmental professionals to regulatory EDR has developed the AQUIFLOW Information System to provide data on the general direction of groundwater AQUIFLOW® Search Radius: 1.000 Mile. contamination exist on the target property, what downgradient sites might be impacted. environmental professional in forming an opinion about the impact of nearby contaminated properties or, should of groundwater flow direction in the immediate area. Such hydrogeologic information can be used to assist the Hydrogeologic information obtained by installation of wells on a specific site can often be an indicator HYDROGEOLOGIC INFORMATION YES - refer to the Overview Map and Detail MapNEWLAND NATIONAL WETLAND INVENTORY NWI Electronic Data CoverageNWI Quad at Target Property Not ReportedAdditional Panels in search area: 37011C - FEMA DFIRM Flood dataFlood Plain Panel at Target Property: YES - refer to the Overview Map and Detail MapAVERY, NC FEMA FLOOD ZONE FEMA Flood Electronic DataTarget Property County and bodies of water). Refer to the Physical Setting Source Map following this summary for hydrologic information (major waterways contamination exist on the target property, what downgradient sites might be impacted. the environmental professional in forming an opinion about the impact of nearby contaminated properties or, should Surface water can act as a hydrologic barrier to groundwater flow. Such hydrologic information can be used to assist HYDROLOGIC INFORMATION ®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY® TC4020675.2s Page A-4 Map, USGS Digital Data Series DDS - 11 (1994). of the Conterminous U.S. at 1:2,500,000 Scale - a digital representation of the 1974 P.B. King and H.M. Beikman Geologic Age and Rock Stratigraphic Unit Source: P.G. Schruben, R.E. Arndt and W.J. Bawiec, Geology ROCK STRATIGRAPHIC UNIT GEOLOGIC AGE IDENTIFICATION Volcanic RocksCategory:PrecambrianEra: PrecambrianSystem: Z volcanic rocksSeries: ZvCode: (decoded above as Era, System & Series) at which contaminant migration may be occurring. Geologic information can be used by the environmental professional in forming an opinion about the relative speed GEOLOGIC INFORMATION IN GENERAL AREA OF TARGET PROPERTY move more quickly through sandy-gravelly types of soils than silty-clayey types of soils. characteristics data collected on nearby properties and regional soil information. In general, contaminant plumes to rely on other sources of information, including geologic age identification, rock stratigraphic unit and soil using site specific geologic and soil strata data. If such data are not reasonably ascertainable, it may be necessary Groundwater flow velocity information for a particular site is best determined by a qualified environmental professional GROUNDWATER FLOW VELOCITY INFORMATION ®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY® EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc. 8 9 7 5 8 4 1 4 3 3 7 5 2 5 3 7 5 6 5 4 6 5 4 5 5 5 0 1/16 1/8 1/4 Miles TC4020675.2s Page A-6 Very poorly drainedSoil Drainage Class: drained and are classified. Class B/D - Drained/undrained hydrology class of soils that can beHydrologic Group: loamSoil Surface Texture: NikwasiSoil Component Name: Soil Map ID: 2 Min: 4.5 Max: 5.5 Min: 4 Max: 14 50%), silt. limit less than Clays (liquid SOILS, Silts and FINE-GRAINED Soils. 200), Silty passing No. than 35 pct. Materials (more Silt-Clay61 inches 9 inches 2 4.5 Max: 6 Min: Min: 14 Max: 42 50%), silt. limit less than Clays (liquid SOILS, Silts and FINE-GRAINED Soils. 200), Silty passing No. than 35 pct. Materials (more Silt-Clayfine sandy loam 9 inches 0 inches 1 Soil Layer Information Boundary Classification Saturated hydraulic conductivity micro m/sec Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil Soil Reaction (pH) > 0 inchesDepth to Watertable Min: > 0 inchesDepth to Bedrock Min: LowCorrosion Potential - Uncoated Steel: Hydric Status: Unknown Well drainedSoil Drainage Class: textures. moderately well and well drained soils with moderately coarse Class B - Moderate infiltration rates. Deep and moderately deep,Hydrologic Group: fine sandy loamSoil Surface Texture: WhiteoakSoil Component Name: Soil Map ID: 1 in a landscape. The following information is based on Soil Conservation Service SSURGO data. for privately owned lands in the United States. A soil map in a soil survey is a representation of soil patterns Survey (NCSS) and is responsible for collecting, storing, maintaining and distributing soil survey information The U.S. Department of Agriculture’s (USDA) Soil Conservation Service (SCS) leads the National Cooperative Soil DOMINANT SOIL COMPOSITION IN GENERAL AREA OF TARGET PROPERTY ®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY® TC4020675.2s Page A-7 > 0 inchesDepth to Watertable Min: > 0 inchesDepth to Bedrock Min: ModerateCorrosion Potential - Uncoated Steel: Hydric Status: Unknown Well drainedSoil Drainage Class: textures. moderately well and well drained soils with moderately coarse Class B - Moderate infiltration rates. Deep and moderately deep,Hydrologic Group: gravelly loamSoil Surface Texture: PineolaSoil Component Name: Soil Map ID: 3 Min: 4.5 Max: 6.5 Min: 42 Max: 141 Silty Sand. Sands with fines, SOILS, Sands, COARSE-GRAINED sand. Poorly graded Clean Sands, SOILS, Sands, COARSE-GRAINED Soils. 200), Silty passing No. than 35 pct. Materials (more Silt-Clay61 inches24 inches 2 Min: 4.5 Max: 6.5 Min: 14 Max: 42 Silty Sand. Sands with fines, SOILS, Sands, COARSE-GRAINED Soils. 200), Silty passing No. than 35 pct. Materials (more Silt-Clayloam24 inches 0 inches 1 Soil Layer Information Boundary Classification Saturated hydraulic conductivity micro m/sec Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil Soil Reaction (pH) > 15 inchesDepth to Watertable Min: > 0 inchesDepth to Bedrock Min: HighCorrosion Potential - Uncoated Steel: Hydric Status: All hydric ®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY® TC4020675.2s Page A-8 > 0 inchesDepth to Watertable Min: > 0 inchesDepth to Bedrock Min: ModerateCorrosion Potential - Uncoated Steel: Hydric Status: Unknown Well drainedSoil Drainage Class: textures. moderately well and well drained soils with moderately coarse Class B - Moderate infiltration rates. Deep and moderately deep,Hydrologic Group: gravelly loamSoil Surface Texture: PineolaSoil Component Name: Soil Map ID: 4 Max: Min: Min: 0 Max: 14 Not reportedNot reported bedrock weathered61 inches31 inches 4 3.5 Max: 6 Min: Min: 4 Max: 14 Clayey sand. Sands with fines, SOILS, Sands, COARSE-GRAINED and Sand. Clayey Gravel 200), Silty, or passing No. pct. or less materials (35 Granular31 inches25 inches 3 3.5 Max: 6 Min: Min: 4 Max: 14 50%), Lean Clay limit less than Clays (liquid SOILS, Silts and FINE-GRAINED Soils. 200), Clayey passing No. than 35 pct. Materials (more Silt-Clay25 inches 7 inches 2 3.5 Max: 6 Min: Min: 14 Max: 42 Clayey sand. Sands with fines, SOILS, Sands, COARSE-GRAINED Soils. 200), Silty passing No. than 35 pct. Materials (more Silt-Claygravelly loam 7 inches 0 inches 1 Soil Layer Information Boundary Classification Saturated hydraulic conductivity micro m/sec Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil Soil Reaction (pH) ®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY® TC4020675.2s Page A-9 > 0 inchesDepth to Watertable Min: > 77 inchesDepth to Bedrock Min: LowCorrosion Potential - Uncoated Steel: Hydric Status: Unknown Well drainedSoil Drainage Class: textures. moderately well and well drained soils with moderately coarse Class B - Moderate infiltration rates. Deep and moderately deep,Hydrologic Group: gravelly sandy loamSoil Surface Texture: CrossnoreSoil Component Name: Soil Map ID: 5 Max: Min: Min: 0 Max: 14 Not reportedNot reported bedrock weathered61 inches31 inches 4 3.5 Max: 6 Min: Min: 4 Max: 14 Clayey sand. Sands with fines, SOILS, Sands, COARSE-GRAINED and Sand. Clayey Gravel 200), Silty, or passing No. pct. or less materials (35 Granular31 inches25 inches 3 3.5 Max: 6 Min: Min: 4 Max: 14 50%), Lean Clay limit less than Clays (liquid SOILS, Silts and FINE-GRAINED Soils. 200), Clayey passing No. than 35 pct. Materials (more Silt-Clay25 inches 7 inches 2 3.5 Max: 6 Min: Min: 14 Max: 42 Clayey sand. Sands with fines, SOILS, Sands, COARSE-GRAINED Soils. 200), Silty passing No. than 35 pct. Materials (more Silt-Claygravelly loam 7 inches 0 inches 1 Soil Layer Information Boundary Classification Saturated hydraulic conductivity micro m/sec Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil Soil Reaction (pH) ®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY® TC4020675.2s Page A-10 > 0 inchesDepth to Watertable Min: > 0 inchesDepth to Bedrock Min: LowCorrosion Potential - Uncoated Steel: Hydric Status: Unknown Well drainedSoil Drainage Class: textures. moderately well and well drained soils with moderately coarse Class B - Moderate infiltration rates. Deep and moderately deep,Hydrologic Group: fine sandy loamSoil Surface Texture: WhiteoakSoil Component Name: Soil Map ID: 6 Max: Min: Min: 0 Max: 14 Not reportedNot reported bedrock weathered61 inches29 inches 4 3.5 Max: 6 Min: Min: 14 Max: 42 Silty Sand. Sands with fines, SOILS, Sands, COARSE-GRAINED and Sand. Clayey Gravel 200), Silty, or passing No. pct. or less materials (35 Granular29 inches22 inches 3 3.5 Max: 6 Min: Min: 14 Max: 42 Clayey sand. Sands with fines, SOILS, Sands, COARSE-GRAINED Soils. 200), Silty passing No. than 35 pct. Materials (more Silt-Clay22 inches 7 inches 2 3.5 Max: 6 Min: Min: 14 Max: 42 Silty Sand. Sands with fines, SOILS, Sands, COARSE-GRAINED Soils. 200), Silty passing No. than 35 pct. Materials (more Silt-Clay loam gravelly sandy 7 inches 0 inches 1 Soil Layer Information Boundary Classification Saturated hydraulic conductivity micro m/sec Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil Soil Reaction (pH) ®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY® TC4020675.2s Page A-11 Well drainedSoil Drainage Class: textures. moderately well and well drained soils with moderately coarse Class B - Moderate infiltration rates. Deep and moderately deep,Hydrologic Group: loamSoil Surface Texture: RosmanSoil Component Name: Soil Map ID: 8 No Layer Information available. > 0 inchesDepth to Watertable Min: > 0 inchesDepth to Bedrock Min: Not ReportedCorrosion Potential - Uncoated Steel: Hydric Status: Unknown Soil Drainage Class: textures. moderately well and well drained soils with moderately coarse Class B - Moderate infiltration rates. Deep and moderately deep,Hydrologic Group: fine sandy loamSoil Surface Texture: WaterSoil Component Name: Soil Map ID: 7 Min: 4.5 Max: 5.5 Min: 4 Max: 14 50%), silt. limit less than Clays (liquid SOILS, Silts and FINE-GRAINED Soils. 200), Silty passing No. than 35 pct. Materials (more Silt-Clay61 inches 9 inches 2 4.5 Max: 6 Min: Min: 14 Max: 42 50%), silt. limit less than Clays (liquid SOILS, Silts and FINE-GRAINED Soils. 200), Silty passing No. than 35 pct. Materials (more Silt-Clayfine sandy loam 9 inches 0 inches 1 Soil Layer Information Boundary Classification Saturated hydraulic conductivity micro m/sec Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil Soil Reaction (pH) ®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY® TC4020675.2s Page A-12 > 114 inchesDepth to Watertable Min: > 0 inchesDepth to Bedrock Min: ModerateCorrosion Potential - Uncoated Steel: Hydric Status: Unknown Well drainedSoil Drainage Class: textures. moderately well and well drained soils with moderately coarse Class B - Moderate infiltration rates. Deep and moderately deep,Hydrologic Group: sandy loamSoil Surface Texture: RosmanSoil Component Name: Soil Map ID: 9 Min: 5.1 Max: 6.5 Min: 14 Max: 42 50%), silt. limit less than Clays (liquid SOILS, Silts and FINE-GRAINED Soils. 200), Silty passing No. than 35 pct. Materials (more Silt-Clay61 inches14 inches 2 Min: 5.1 Max: 6.5 Min: 14 Max: 42 50%), silt. limit less than Clays (liquid SOILS, Silts and FINE-GRAINED Soils. 200), Silty passing No. than 35 pct. Materials (more Silt-Clayloam14 inches 0 inches 1 Soil Layer Information Boundary Classification Saturated hydraulic conductivity micro m/sec Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil Soil Reaction (pH) > 114 inchesDepth to Watertable Min: > 0 inchesDepth to Bedrock Min: ModerateCorrosion Potential - Uncoated Steel: Hydric Status: Unknown ®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY® TC4020675.2s Page A-13 1/2 - 1 Mile SSEUSGS40000892890 19 1/2 - 1 Mile SouthUSGS40000892891 18 1/2 - 1 Mile SEUSGS40000892899 17 1/2 - 1 Mile NWUSGS40000893013 16 1/2 - 1 Mile ENEUSGS40000892961 15 1/4 - 1/2 Mile WSWUSGS40000892933 E13 1/4 - 1/2 Mile SSWUSGS40000892906 D10 1/4 - 1/2 Mile NorthUSGS40000893012 C9 1/4 - 1/2 Mile SSWUSGS40000892905 B7 1/4 - 1/2 Mile SSWUSGS40000892904 B5 1/4 - 1/2 Mile SouthUSGS40000892916 A4 FEDERAL USGS WELL INFORMATION LOCATION FROM TPWELL IDMAP ID 1.000State Database Nearest PWS within 1 mileFederal FRDS PWS 1.000Federal USGS WELL SEARCH DISTANCE INFORMATION SEARCH DISTANCE (miles)DATABASE opinion about the impact of contaminant migration on nearby drinking water wells. professional in assessing sources that may impact ground water flow direction, and in forming an EDR Local/Regional Water Agency records provide water well information to assist the environmental LOCAL / REGIONAL WATER AGENCY RECORDS Min: 5.1 Max: 6.5 Min: 14 Max: 42 50%), silt. limit less than Clays (liquid SOILS, Silts and FINE-GRAINED Soils. 200), Silty passing No. than 35 pct. Materials (more Silt-Clay61 inches 9 inches 2 Min: 5.1 Max: 6.5 Min: 14 Max: 42 Silty Sand. Sands with fines, SOILS, Sands, COARSE-GRAINED Soils. 200), Silty passing No. than 35 pct. Materials (more Silt-Claysandy loam 9 inches 0 inches 1 Soil Layer Information Boundary Classification Saturated hydraulic conductivity micro m/sec Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil Soil Reaction (pH) ®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY® TC4020675.2s Page A-14 Animal NC50003423 Natural Community Occurrence NC50002887 Non Vascular NC50002612 Plants NC50001611 Non Vascular NC50001362 Plants NC50001056 _________ ___ Class ID NORTH CAROLINA NATURAL HERITAGE ELEMENT OCCURRENCES OTHER STATE DATABASE INFORMATION 1/2 - 1 Mile SouthNC2000000007642 G25 1/2 - 1 Mile SouthNC2000000007644 G23 1/4 - 1/2 Mile WestNC2000000007683 E14 1/4 - 1/2 Mile SSWNC2000000007670 D12 1/4 - 1/2 Mile NorthNC2000000007722 C11 1/4 - 1/2 Mile SSWNC2000000007671 B8 1/4 - 1/2 Mile SSWNC2000000007672 B6 1/4 - 1/2 Mile SouthNC2000000007676 A3 1/4 - 1/2 Mile SouthNC2000000007677 A2 STATE DATABASE WELL INFORMATION LOCATION FROM TPWELL IDMAP ID Note: PWS System location is not always the same as well location. 1/8 - 1/4 Mile SWNC0106104 1 FEDERAL FRDS PUBLIC WATER SUPPLY SYSTEM INFORMATION LOCATION FROM TPWELL IDMAP ID 1/2 - 1 Mile SouthUSGS40000892842 28 1/2 - 1 Mile SouthUSGS40000892843 27 1/2 - 1 Mile SSEUSGS40000892864 26 1/2 - 1 Mile SouthUSGS40000892850 G24 1/2 - 1 Mile SouthUSGS40000892852 G22 1/2 - 1 Mile SSEUSGS40000892870 F21 1/2 - 1 Mile SSEUSGS40000892869 F20 FEDERAL USGS WELL INFORMATION LOCATION FROM TPWELL IDMAP ID ®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY® TC4020675.2s Page A-15 NC30000202 NC30000176 _________ Site Name NORTH CAROLINA WILDLIFE RESOURCES COMMISSION GAME LANDS DATABASE ANTHONY CREEK SWAMP FOREST-BOG COMPLEX NC10000250 PINEOLA BOG NC10000248 FLAT ROCK MOUNTAIN NC10000232 LINVILLE RIVER SWAMP FOREST-BOG COMPLEX NC10000230 _________ ___ Name ID NORTH CAROLINA SIGNIFICANT NATURAL HERITAGE AREAS DATABASE: Natural Community Occurrence NC50015635 Natural Community Occurrence NC50015558 Animal NC50015053 Plants NC50012055 Plants NC50009769 Plants NC50009686 Animal NC50009456 Natural Community Occurrence NC50008837 Non Vascular NC50007635 Natural Community Occurrence NC50006440 Invertebrate NC50006359 Plants NC50004516 Plants NC50004478 _________ ___ Class ID NORTH CAROLINA NATURAL HERITAGE ELEMENT OCCURRENCES GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc. 3 8 3 7 6 0 3 7 6 0 3 8 0 0 3 7 6 0 3 7 2 0 3 7 2 0 3 7 2 0 3 84 0 3 720 3 6 4 0 3 6 4 0 404040 3 6 8 0 3 6 8 0 3 680 3 6 8 0 4 000 4 040 4 0 4 0 4000 3 720 3 7 2 0 3720 3 7 2 0 4120 3 7 6 0 3 7 6 0 3 7 6 0 4 0 8 0 4 0 4 0 4 0 4 0 4 0 4 00 4 000 4 0 0 0 3 9 6 0 3 9 6 0 3 9 6 0 3 9 2 0 3 9 2 0 3 9 2 0 3 8 8 0 3 8 8 0 3 880 3720 3 9203880 3 6 8 0 3880 3 6 8 0 3 8 4 0 3 8 4 0 3 8 4 0 3 8 40 3840 3 8 00 3 8 0 0 3 8 00 3 8 0 0 3 8 0 0 37 6 0 3760 3760 3 720 3720 3 560 3 7 2 0 3 6 8 0 3 6 4 0 3 6 0 0 3 5 60 3 5 6 0 3 5 2 0 3 5 2 0 3 480 34 8 0 3 440 33 20 3 2 803240 3 2 0 0 316 0 NC TC4020675.2s Page A-17 disinfectionTreatment objective: hypochlorination, postTreatment process:WellFacility type: WELL #1Facility name: 11902Facility id: corrosion controlTreatment objective: ph adjustmentTreatment process:Treatment_plantFacility type: TREATMENT_PLT_WELL #10Facility name: 5677Facility id: corrosion controlTreatment objective: inhibitor, orthophosphateTreatment process:WellFacility type: WELL #1Facility name: 11902Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:Treatment_plantFacility type: TREATMENT_PLT_WELL #10Facility name: 5677Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:Treatment_plantFacility type: TREATMENT_PLT_WELL #7Facility name: 5676Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:Treatment_plantFacility type: TREATMENT_PLT_WELL #3Facility name: 5675Facility id: 28646Contact zip: LINVILLEContact city: LINVILLE LAND HARBORContact address2: PO BOX 160Contact address1:828-733-8300Contact phone: SIMPSON, MIKEOriginal name: SIMPSON, MIKEContact name: disinfectionTreatment objective: hypochlorination, postTreatment process:Treatment_plantFacility type: TREATMENT_PLT_WELL #1Facility name: 5674Facility id: PrivateOwner type:ActiveStatus: CWSPws type: GroundwaterPWS Source: 1404Pwssvcconn:2280Population Served: LINVILLE LAND HARBORPws name: AveryCounty:NCState: 04Epa region:NC0106104Pwsid: 1 SW 1/8 - 1/4 Mile Higher NC0106104FRDS PWS Map ID Direction Distance Elevation EDR ID NumberDatabase ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-18 disinfectionTreatment objective: hypochlorination, postTreatment process:Treatment_plantFacility type: TREATMENT_PLT_WELL #1Facility name: 5674Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:Distribution_system_zoneFacility type: DISTRIBUTION SYSTEMFacility name: 41530Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:StorageFacility type: STORAGE_GROUND_1Facility name: 1335Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:WellFacility type: WELL #8Facility name: 11908Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:WellFacility type: WELL #7Facility name: 11907Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:WellFacility type: WELL #6Facility name: 11906Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:WellFacility type: WELL #4Facility name: 11905Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:WellFacility type: WELL #6Facility name: 11906Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:WellFacility type: WELL #4Facility name: 11905Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:WellFacility type: WELL #3Facility name: 11904Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:WellFacility type: WELL #10Facility name: 11903Facility id: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-19 corrosion controlTreatment objective: ph adjustmentTreatment process:Treatment_plantFacility type: TREATMENT_PLT_WELL #1Facility name: 5674Facility id: corrosion controlTreatment objective: ph adjustmentTreatment process:Distribution_system_zoneFacility type: DISTRIBUTION SYSTEMFacility name: 41530Facility id: corrosion controlTreatment objective: ph adjustmentTreatment process:StorageFacility type: STORAGE_GROUND_1Facility name: 1335Facility id: corrosion controlTreatment objective: ph adjustmentTreatment process:WellFacility type: WELL #8Facility name: 11908Facility id: corrosion controlTreatment objective: ph adjustmentTreatment process:WellFacility type: WELL #7Facility name: 11907Facility id: corrosion controlTreatment objective: ph adjustmentTreatment process:WellFacility type: WELL #6Facility name: 11906Facility id: corrosion controlTreatment objective: ph adjustmentTreatment process:WellFacility type: WELL #4Facility name: 11905Facility id: corrosion controlTreatment objective: ph adjustmentTreatment process:WellFacility type: WELL #3Facility name: 11904Facility id: corrosion controlTreatment objective: ph adjustmentTreatment process:WellFacility type: WELL #10Facility name: 11903Facility id: corrosion controlTreatment objective: ph adjustmentTreatment process:WellFacility type: WELL #1Facility name: 11902Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:Treatment_plantFacility type: TREATMENT_PLT_WELL #3Facility name: 5675Facility id: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-20 disinfectionTreatment objective: hypochlorination, postTreatment process:StorageFacility type: STORAGE_GROUND_1Facility name: 1335Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:WellFacility type: WELL #8Facility name: 11908Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:WellFacility type: WELL #7Facility name: 11907Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:WellFacility type: WELL #6Facility name: 11906Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:WellFacility type: WELL #4Facility name: 11905Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:WellFacility type: WELL #3Facility name: 11904Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:WellFacility type: WELL #10Facility name: 11903Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:WellFacility type: WELL #1Facility name: 11902Facility id: corrosion controlTreatment objective: ph adjustmentTreatment process:Treatment_plantFacility type: TREATMENT_PLT_WELL #10Facility name: 5677Facility id: corrosion controlTreatment objective: ph adjustmentTreatment process:Treatment_plantFacility type: TREATMENT_PLT_WELL #7Facility name: 5676Facility id: corrosion controlTreatment objective: ph adjustmentTreatment process:Treatment_plantFacility type: TREATMENT_PLT_WELL #3Facility name: 5675Facility id: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-21 LINVILLE, NC 28646 PO BOX 157 FRANCES H BANNER OR MANAGER System Owner/Responsible PartyAddressee / Facility: LINVILLE, NC 28646 LINVILLE LAND HARBORPWS Name: Not ReportedDate Deactivated:Not ReportedDate Initiated: NC0106104PWS ID: corrosion controlTreatment objective: inhibitor, orthophosphateTreatment process:Treatment_plantFacility type: TREATMENT_PLT_WELL #1Facility name: 5674Facility id: corrosion controlTreatment objective: inhibitor, orthophosphateTreatment process:Distribution_system_zoneFacility type: DISTRIBUTION SYSTEMFacility name: 41530Facility id: corrosion controlTreatment objective: inhibitor, orthophosphateTreatment process:StorageFacility type: STORAGE_GROUND_1Facility name: 1335Facility id: corrosion controlTreatment objective: inhibitor, orthophosphateTreatment process:WellFacility type: WELL #8Facility name: 11908Facility id: corrosion controlTreatment objective: inhibitor, orthophosphateTreatment process:WellFacility type: WELL #7Facility name: 11907Facility id: corrosion controlTreatment objective: inhibitor, orthophosphateTreatment process:WellFacility type: WELL #6Facility name: 11906Facility id: corrosion controlTreatment objective: inhibitor, orthophosphateTreatment process:WellFacility type: WELL #4Facility name: 11905Facility id: corrosion controlTreatment objective: inhibitor, orthophosphateTreatment process:WellFacility type: WELL #3Facility name: 11904Facility id: corrosion controlTreatment objective: inhibitor, orthophosphateTreatment process:WellFacility type: WELL #10Facility name: 11903Facility id: disinfectionTreatment objective: hypochlorination, postTreatment process:Distribution_system_zoneFacility type: DISTRIBUTION SYSTEMFacility name: 41530Facility id: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-22 Not ReportedViolmeasur: State Formal NOV IssuedEnf action: 9/10/2003 0:00:00Enfdate:12/31/2025 0:00:00Complperen: 1/1/2003 0:00:00Complperbe: Follow-up and Routine Tap SamplingViol. Type: LEAD & COPPER RULEContaminant:1903Vioid: CPwstypecod:2280Retpopsrvd: LINVILLE LAND HARBORPwsname: NC0106104Pwsid:03/31/2009Truedate: Not ReportedViolmeasur: State Public Notif RequestedEnf action: 9/12/2001 0:00:00Enfdate:7/31/2001 0:00:00Complperen: 7/1/2001 0:00:00Complperbe: Monitoring, Routine Minor (TCR)Viol. Type: COLIFORM (TCR)Contaminant:1801Vioid: CPwstypecod:2280Retpopsrvd: LINVILLE LAND HARBORPwsname: NC0106104Pwsid:03/31/2009Truedate: Not ReportedViolmeasur: State Formal NOV IssuedEnf action: 9/12/2001 0:00:00Enfdate:7/31/2001 0:00:00Complperen: 7/1/2001 0:00:00Complperbe: Monitoring, Routine Minor (TCR)Viol. Type: COLIFORM (TCR)Contaminant:1801Vioid: CPwstypecod:2280Retpopsrvd: LINVILLE LAND HARBORPwsname: NC0106104Pwsid:03/31/2009Truedate: Not ReportedViolmeasur: State Compliance AchievedEnf action: 2/28/2002 0:00:00Enfdate:7/31/2001 0:00:00Complperen: 7/1/2001 0:00:00Complperbe: Monitoring, Routine Minor (TCR)Viol. Type: COLIFORM (TCR)Contaminant:1801Vioid: CPwstypecod:2280Retpopsrvd: LINVILLE LAND HARBORPwsname: NC0106104Pwsid:03/31/2009Truedate: ENFORCEMENT INFORMATION: Violations information not reported. 2000Population:UntreatedTreatment Class: LINVILLECity Served: 81 54 16.0000Facility Longitude:36 3 0.0000Facility Latitude: 81 53 20.0000Facility Longitude:36 2 40.0000Facility Latitude: LINVILLE, NC 28646 PO BOX 157 LINVILLE LAND HARBOR PRON OWN System Owner/Responsible PartyAddressee / Facility: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-23 Not ReportedViolmeasur: 7/8/2009 0:00:00Enf action: No Enf Action as ofEnfdate:12/31/2025 0:00:00Complperen: 9/20/2004 0:00:00Complperbe: Other Non-NPDWR Potential Health RisksViol. Type: 7500Contaminant:4581404Vioid: CPwstypecod:2280Retpopsrvd: LINVILLE LAND HARBORPwsname: NC0106104Pwsid:03/31/2009Truedate: Not ReportedViolmeasur: 7/8/2009 0:00:00Enf action: No Enf Action as ofEnfdate:12/31/2025 0:00:00Complperen: 9/23/2002 0:00:00Complperbe: Other Non-NPDWR Potential Health RisksViol. Type: 7500Contaminant:4199102Vioid: CPwstypecod:2280Retpopsrvd: LINVILLE LAND HARBORPwsname: NC0106104Pwsid:03/31/2009Truedate: Not ReportedViolmeasur: State Public Notif RequestedEnf action: 9/18/2003 0:00:00Enfdate:9/30/2003 0:00:00Complperen: 7/1/2003 0:00:00Complperbe: CCR Complete Failure to ReportViol. Type: 7000Contaminant:2004Vioid: CPwstypecod:2280Retpopsrvd: LINVILLE LAND HARBORPwsname: NC0106104Pwsid:03/31/2009Truedate: Not ReportedViolmeasur: State Compliance AchievedEnf action: 9/30/2003 0:00:00Enfdate:9/30/2003 0:00:00Complperen: 7/1/2003 0:00:00Complperbe: CCR Complete Failure to ReportViol. Type: 7000Contaminant:2004Vioid: CPwstypecod:2280Retpopsrvd: LINVILLE LAND HARBORPwsname: NC0106104Pwsid:03/31/2009Truedate: Not ReportedViolmeasur: State Formal NOV IssuedEnf action: 9/18/2003 0:00:00Enfdate:9/30/2003 0:00:00Complperen: 7/1/2003 0:00:00Complperbe: CCR Complete Failure to ReportViol. Type: 7000Contaminant:2004Vioid: CPwstypecod:2280Retpopsrvd: LINVILLE LAND HARBORPwsname: NC0106104Pwsid:03/31/2009Truedate: Not ReportedViolmeasur: State Public Notif RequestedEnf action: 9/10/2003 0:00:00Enfdate:12/31/2025 0:00:00Complperen: 1/1/2003 0:00:00Complperbe: Follow-up and Routine Tap SamplingViol. Type: LEAD & COPPER RULEContaminant:1903Vioid: CPwstypecod:2280Retpopsrvd: LINVILLE LAND HARBORPwsname: NC0106104Pwsid:03/31/2009Truedate: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-24 State Public Notif RequestedEnf. Action:9/12/2001 0:00:00Enforcement Date: 1801Violation ID: 7/1/2001 0:00:00 - 7/31/2001 0:00:00Compliance Period: COLIFORM (TCR)Contaminant: Monitoring, Routine Minor (TCR)Violation Type: LINVILLE LAND HARBORSystem Name: State Compliance AchievedEnf. Action:2/28/2002 0:00:00Enforcement Date: 1801Violation ID: 7/1/2001 0:00:00 - 7/31/2001 0:00:00Compliance Period: COLIFORM (TCR)Contaminant: Monitoring, Routine Minor (TCR)Violation Type: LINVILLE LAND HARBORSystem Name: State Compliance AchievedEnf. Action:2/28/2002 0:00:00Enforcement Date: 1801Violation ID: 7/1/2001 0:00:00 - 7/31/2001 0:00:00Compliance Period: COLIFORM (TCR)Contaminant: Monitoring, Routine Minor (TCR)Violation Type: LINVILLE LAND HARBORSystem Name: State Formal NOV IssuedEnf. Action:9/12/2001 0:00:00Enforcement Date: 1801Violation ID: 7/1/2001 0:00:00 - 7/31/2001 0:00:00Compliance Period: COLIFORM (TCR)Contaminant: Monitoring, Routine Minor (TCR)Violation Type: LINVILLE LAND HARBORSystem Name: State Public Notif RequestedEnf. Action:9/12/2001 0:00:00Enforcement Date: 1801Violation ID: 7/1/2001 0:00:00 - 7/31/2001 0:00:00Compliance Period: COLIFORM (TCR)Contaminant: Monitoring, Routine Minor (TCR)Violation Type: LINVILLE LAND HARBORSystem Name: State Formal NOV IssuedEnf. Action:9/12/2001 0:00:00Enforcement Date: 1801Violation ID: 7/1/2001 0:00:00 - 7/31/2001 0:00:00Compliance Period: COLIFORM (TCR)Contaminant: Monitoring, Routine Minor (TCR)Violation Type: LINVILLE LAND HARBORSystem Name: Not ReportedEnf. Action:Not ReportedEnforcement Date: 0005025Violation ID: 1999-10-19 - 2015-12-31Compliance Period: 7000Contaminant: CCR Complete Failure to ReportViolation Type: LINVILLE LAND HARBORSystem Name: Not ReportedViolmeasur: State Compliance AchievedEnf action: 12/29/2006 0:00:00Enfdate:12/29/2006 0:00:00Complperen: 3/1/2006 0:00:00Complperbe: Public EducationViol. Type: LEAD & COPPER RULEContaminant:4581607Vioid: CPwstypecod:2280Retpopsrvd: LINVILLE LAND HARBORPwsname: NC0106104Pwsid:03/31/2009Truedate: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-25 State Formal NOV IssuedEnf. Action:9/18/2003 0:00:00Enforcement Date: 2004Violation ID: 7/1/2003 0:00:00 - 9/30/2003 0:00:00Compliance Period: 7000Contaminant: CCR Complete Failure to ReportViolation Type: LINVILLE LAND HARBORSystem Name: State Compliance AchievedEnf. Action:9/30/2003 0:00:00Enforcement Date: 2004Violation ID: 7/1/2003 0:00:00 - 9/30/2003 0:00:00Compliance Period: 7000Contaminant: CCR Complete Failure to ReportViolation Type: LINVILLE LAND HARBORSystem Name: State Compliance AchievedEnf. Action:9/30/2003 0:00:00Enforcement Date: 2004Violation ID: 7/1/2003 0:00:00 - 9/30/2003 0:00:00Compliance Period: 7000Contaminant: CCR Complete Failure to ReportViolation Type: LINVILLE LAND HARBORSystem Name: State Public Notif RequestedEnf. Action:9/18/2003 0:00:00Enforcement Date: 2004Violation ID: 7/1/2003 0:00:00 - 9/30/2003 0:00:00Compliance Period: 7000Contaminant: CCR Complete Failure to ReportViolation Type: LINVILLE LAND HARBORSystem Name: State Formal NOV IssuedEnf. Action:9/18/2003 0:00:00Enforcement Date: 2004Violation ID: 7/1/2003 0:00:00 - 9/30/2003 0:00:00Compliance Period: 7000Contaminant: CCR Complete Failure to ReportViolation Type: LINVILLE LAND HARBORSystem Name: State Public Notif RequestedEnf. Action:9/10/2003 0:00:00Enforcement Date: 1903Violation ID: 1/1/2003 0:00:00 - 12/31/2025 0:00:00Compliance Period: LEAD & COPPER RULEContaminant: Follow-up and Routine Tap SamplingViolation Type: LINVILLE LAND HARBORSystem Name: State Formal NOV IssuedEnf. Action:9/10/2003 0:00:00Enforcement Date: 1903Violation ID: 1/1/2003 0:00:00 - 12/31/2025 0:00:00Compliance Period: LEAD & COPPER RULEContaminant: Follow-up and Routine Tap SamplingViolation Type: LINVILLE LAND HARBORSystem Name: State Formal NOV IssuedEnf. Action:9/10/2003 0:00:00Enforcement Date: 1903Violation ID: 1/1/2003 0:00:00 - 12/31/2025 0:00:00Compliance Period: LEAD & COPPER RULEContaminant: Follow-up and Routine Tap SamplingViolation Type: LINVILLE LAND HARBORSystem Name: State Public Notif RequestedEnf. Action:9/10/2003 0:00:00Enforcement Date: 1903Violation ID: 1/1/2003 0:00:00 - 12/31/2025 0:00:00Compliance Period: LEAD & COPPER RULEContaminant: Follow-up and Routine Tap SamplingViolation Type: LINVILLE LAND HARBORSystem Name: ENFORCEMENT INFORMATION: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-26 A2 South 1/4 - 1/2 Mile Lower NC2000000007677NC WELLS LINVILLE, NC 28646 LINVILLE LAND HARBORAddress 2: PO BOX 160Address: 828-733-8310Phone:C L, LEWISContact: 2280Population:LINVILLE LAND HARBORName: CONTACT INFORMATION: Not ReportedEnf. Action:4/12/2007 0:00:00Enforcement Date: 4581607Violation ID: 3/1/2006 0:00:00 - 12/31/2025 0:00:00Compliance Period: LEAD & COPPER RULEContaminant: Public EducationViolation Type: LINVILLE LAND HARBORSystem Name: 10/17/2006 0:00:00Enf. Action:No Enf Action as ofEnforcement Date: 4581404Violation ID: 9/20/2004 0:00:00 - 12/31/2025 0:00:00Compliance Period: 7500Contaminant: Other Non-NPDWR Potential Health RisksViolation Type: LINVILLE LAND HARBORSystem Name: Not ReportedEnf. Action:4/12/2007 0:00:00Enforcement Date: 4581404Violation ID: 9/20/2004 0:00:00 - 12/31/2025 0:00:00Compliance Period: 7500Contaminant: Other Non-NPDWR Potential Health RisksViolation Type: LINVILLE LAND HARBORSystem Name: 10/17/2006 0:00:00Enf. Action:No Enf Action as ofEnforcement Date: 4199102Violation ID: 9/23/2002 0:00:00 - 12/31/2025 0:00:00Compliance Period: 7500Contaminant: Other Non-NPDWR Potential Health RisksViolation Type: LINVILLE LAND HARBORSystem Name: Not ReportedEnf. Action:4/12/2007 0:00:00Enforcement Date: 4199102Violation ID: 9/23/2002 0:00:00 - 12/31/2025 0:00:00Compliance Period: 7500Contaminant: Other Non-NPDWR Potential Health RisksViolation Type: LINVILLE LAND HARBORSystem Name: State Public Notif RequestedEnf. Action:9/18/2003 0:00:00Enforcement Date: 2004Violation ID: 7/1/2003 0:00:00 - 9/30/2003 0:00:00Compliance Period: 7000Contaminant: CCR Complete Failure to ReportViolation Type: LINVILLE LAND HARBORSystem Name: ENFORCEMENT INFORMATION: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-27 Not ReportedSourcemap scale:-81.8875Longitude: 36.0416667Latitude:Not ReportedContrib drainagearea units: Not ReportedContrib drainagearea:Not ReportedDrainagearea Units: Not ReportedDrainagearea value:Not ReportedHuc code: Nearest town:LINVILLEMonloc desc: WellMonloc type: AV-588Monloc name: USGS-360230081531501Monloc Identifier: USGS North Carolina Water Science CenterFormal name: USGS-NCOrg. Identifier: A4 South 1/4 - 1/2 Mile Lower USGS40000892916FED USGS NC2000000007676Site id: LINVILLE LAND HARBOR POAOwner name: FTWell dep 1: 200Well depth: AAvailavili: -81.887493Longitude : 36.041705Latitude m: W04Facility a: WELL #4Facility n: GWWater type: GWPrimary so: LINVILLECity: AVERYCounty: CPws type: LINVILLE LAND HARBORSystem nam: NC0106104Pwsidentif: A3 South 1/4 - 1/2 Mile Lower NC2000000007676NC WELLS NC2000000007677Site id: LINVILLE RESORTS INCOwner name: Not ReportedWell dep 1: 0Well depth: IAvailavili: -81.887502Longitude : 36.041771Latitude m: W04Facility a: WELL #4Facility n: GWWater type: GWPrimary so: LINVILLECity: AVERYCounty: CPws type: LINVILLE RESORTS INCSystem nam: NC0106105Pwsidentif: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-28 36.040508Latitude m: W08Facility a: WELL #8Facility n: GWWater type: GWPrimary so: LINVILLECity: AVERYCounty: CPws type: LINVILLE LAND HARBORSystem nam: NC0106104Pwsidentif: B6 SSW 1/4 - 1/2 Mile Lower NC2000000007672NC WELLS Ground-water levels, Number of Measurements: 0 Not ReportedWellholedepth units: Not ReportedWellholedepth:ftWelldepth units: 700Welldepth:Not ReportedConstruction date: Not ReportedAquifer type: PhylliteFormation type: Piedmont and Blue Ridge crystalline-rock aquifersAquifername: USCountrycode:NAVD88Vert coord refsys: Interpolated from topographic mapVertcollection method: feetVert accmeasure units: 20Vertacc measure val:feetVert measure units: 3590Vert measure val:NAD83Horiz coord refsys: Global positioning system (GPS), uncorrectedHoriz Collection method: secondsHoriz Acc measure units:.1Horiz Acc measure: Not ReportedSourcemap scale:-81.8886111Longitude: 36.0405556Latitude:Not ReportedContrib drainagearea units: Not ReportedContrib drainagearea:Not ReportedDrainagearea Units: Not ReportedDrainagearea value:Not ReportedHuc code: Nearest town:LINVILLEMonloc desc: WellMonloc type: AV-586Monloc name: USGS-360226081531901Monloc Identifier: USGS North Carolina Water Science CenterFormal name: USGS-NCOrg. Identifier: B5 SSW 1/4 - 1/2 Mile Lower USGS40000892904FED USGS Ground-water levels, Number of Measurements: 0 Not ReportedWellholedepth units: Not ReportedWellholedepth:ftWelldepth units: 200Welldepth:Not ReportedConstruction date: Not ReportedAquifer type: PhylliteFormation type: Piedmont and Blue Ridge crystalline-rock aquifersAquifername: USCountrycode:NAVD88Vert coord refsys: Interpolated from topographic mapVertcollection method: feetVert accmeasure units: 20Vertacc measure val:feetVert measure units: 3600Vert measure val:NAD83Horiz coord refsys: Global positioning system (GPS), uncorrectedHoriz Collection method: secondsHoriz Acc measure units:.1Horiz Acc measure: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-29 36.040463Latitude m: W06Facility a: WELL #6Facility n: GWWater type: GWPrimary so: LINVILLECity: AVERYCounty: CPws type: LINVILLE LAND HARBORSystem nam: NC0106104Pwsidentif: B8 SSW 1/4 - 1/2 Mile Lower NC2000000007671NC WELLS Ground-water levels, Number of Measurements: 0 Not ReportedWellholedepth units: Not ReportedWellholedepth:ftWelldepth units: 400Welldepth:Not ReportedConstruction date: Not ReportedAquifer type: PhylliteFormation type: Piedmont and Blue Ridge crystalline-rock aquifersAquifername: USCountrycode:NAVD88Vert coord refsys: Interpolated from topographic mapVertcollection method: feetVert accmeasure units: 20Vertacc measure val:feetVert measure units: 3570Vert measure val:NAD83Horiz coord refsys: Global positioning system (GPS), uncorrectedHoriz Collection method: secondsHoriz Acc measure units:.1Horiz Acc measure: Not ReportedSourcemap scale:-81.8897222Longitude: 36.0405556Latitude:Not ReportedContrib drainagearea units: Not ReportedContrib drainagearea:Not ReportedDrainagearea Units: Not ReportedDrainagearea value:Not ReportedHuc code: Nearest town:LINVILLEMonloc desc: WellMonloc type: AV-585Monloc name: USGS-360226081532301Monloc Identifier: USGS North Carolina Water Science CenterFormal name: USGS-NCOrg. Identifier: B7 SSW 1/4 - 1/2 Mile Lower USGS40000892905FED USGS NC2000000007672Site id: LINVILLE LAND HARBOR POAOwner name: FTWell dep 1: 700Well depth: AAvailavili: -81.888706Longitude : ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-30 Not ReportedSourcemap scale:-81.89Longitude: 36.0405556Latitude:Not ReportedContrib drainagearea units: Not ReportedContrib drainagearea:Not ReportedDrainagearea Units: Not ReportedDrainagearea value:Not ReportedHuc code: Nearest town:LINVILLEMonloc desc: WellMonloc type: AV-584Monloc name: USGS-360226081532401Monloc Identifier: USGS North Carolina Water Science CenterFormal name: USGS-NCOrg. Identifier: D10 SSW 1/4 - 1/2 Mile Lower USGS40000892906FED USGS Ground-water levels, Number of Measurements: 0 Not ReportedWellholedepth units: Not ReportedWellholedepth:ftWelldepth units: 220Welldepth:Not ReportedConstruction date: Not ReportedAquifer type: PhylliteFormation type: Piedmont and Blue Ridge crystalline-rock aquifersAquifername: USCountrycode:NAVD88Vert coord refsys: Interpolated from topographic mapVertcollection method: feetVert accmeasure units: 20Vertacc measure val:feetVert measure units: 3610Vert measure val:NAD83Horiz coord refsys: Global positioning system (GPS), uncorrectedHoriz Collection method: secondsHoriz Acc measure units:.1Horiz Acc measure: Not ReportedSourcemap scale:-81.8866667Longitude: 36.0516667Latitude:Not ReportedContrib drainagearea units: Not ReportedContrib drainagearea:Not ReportedDrainagearea Units: Not ReportedDrainagearea value:Not ReportedHuc code: Nearest town:NEWLANDMonloc desc: WellMonloc type: AV-594Monloc name: USGS-360306081531201Monloc Identifier: USGS North Carolina Water Science CenterFormal name: USGS-NCOrg. Identifier: C9 North 1/4 - 1/2 Mile Lower USGS40000893012FED USGS NC2000000007671Site id: LINVILLE LAND HARBOR POAOwner name: FTWell dep 1: 400Well depth: AAvailavili: -81.889646Longitude : ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-31 36.04044Latitude m: W10Facility a: WELL #10Facility n: GWWater type: GWPrimary so: LINVILLECity: AVERYCounty: CPws type: LINVILLE LAND HARBORSystem nam: NC0106104Pwsidentif: D12 SSW 1/4 - 1/2 Mile Lower NC2000000007670NC WELLS NC2000000007722Site id: CAROLINA DISTRICT LCL_106486Owner name: FTWell dep 1: 220Well depth: AAvailavili: -81.886666Longitude : 36.051775Latitude m: W01Facility a: WELL #1Facility n: GWWater type: GWPrimary so: NEWLANDCity: AVERYCounty: NCPws type: CAMP LINN HAVENSystem nam: NC0106486Pwsidentif: C11 North 1/4 - 1/2 Mile Lower NC2000000007722NC WELLS Ground-water levels, Number of Measurements: 0 Not ReportedWellholedepth units: Not ReportedWellholedepth:Not ReportedWelldepth units: Not ReportedWelldepth:Not ReportedConstruction date: Not ReportedAquifer type: PhylliteFormation type: Piedmont and Blue Ridge crystalline-rock aquifersAquifername: USCountrycode:NAVD88Vert coord refsys: Interpolated from topographic mapVertcollection method: feetVert accmeasure units: 20Vertacc measure val:feetVert measure units: 3560Vert measure val:NAD83Horiz coord refsys: Global positioning system (GPS), uncorrectedHoriz Collection method: secondsHoriz Acc measure units:.1Horiz Acc measure: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-32 36.044569Latitude m: W07Facility a: WELL #7Facility n: GWWater type: GWPrimary so: LINVILLECity: AVERYCounty: CPws type: LINVILLE LAND HARBORSystem nam: NC0106104Pwsidentif: E14 West 1/4 - 1/2 Mile Lower NC2000000007683NC WELLS Ground-water levels, Number of Measurements: 0 Not ReportedWellholedepth units: Not ReportedWellholedepth:ftWelldepth units: 490Welldepth:Not ReportedConstruction date: Not ReportedAquifer type: PhylliteFormation type: Piedmont and Blue Ridge crystalline-rock aquifersAquifername: USCountrycode:NAVD88Vert coord refsys: Interpolated from topographic mapVertcollection method: feetVert accmeasure units: 20Vertacc measure val:feetVert measure units: 3600Vert measure val:NAD83Horiz coord refsys: Global positioning system (GPS), uncorrectedHoriz Collection method: secondsHoriz Acc measure units:.1Horiz Acc measure: Not ReportedSourcemap scale:-81.8947222Longitude: 36.0444444Latitude:Not ReportedContrib drainagearea units: Not ReportedContrib drainagearea:Not ReportedDrainagearea Units: Not ReportedDrainagearea value:Not ReportedHuc code: Nearest town:LINVILLEMonloc desc: WellMonloc type: AV-589Monloc name: USGS-360240081534101Monloc Identifier: USGS North Carolina Water Science CenterFormal name: USGS-NCOrg. Identifier: E13 WSW 1/4 - 1/2 Mile Lower USGS40000892933FED USGS NC2000000007670Site id: LINVILLE LAND HARBOR POAOwner name: Not ReportedWell dep 1: 0Well depth: AAvailavili: -81.890006Longitude : ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-33 Not ReportedSourcemap scale:-81.893168Longitude: 36.0517939Latitude:Not ReportedContrib drainagearea units: Not ReportedContrib drainagearea:Not ReportedDrainagearea Units: Not ReportedDrainagearea value:03050101Huc code: Not ReportedMonloc desc: WellMonloc type: AV-037Monloc name: USGS-360306081533601Monloc Identifier: USGS North Carolina Water Science CenterFormal name: USGS-NCOrg. Identifier: 16 NW 1/2 - 1 Mile Higher USGS40000893013FED USGS Ground-water levels, Number of Measurements: 0 Not ReportedWellholedepth units: Not ReportedWellholedepth:ftWelldepth units: 150Welldepth:Not ReportedConstruction date: Not ReportedAquifer type: PhylliteFormation type: Piedmont and Blue Ridge crystalline-rock aquifersAquifername: USCountrycode:Not ReportedVert coord refsys: Not ReportedVertcollection method: Not ReportedVert accmeasure units: Not ReportedVertacc measure val:Not ReportedVert measure units: Not ReportedVert measure val:NAD83Horiz coord refsys: Interpolated from mapHoriz Collection method: secondsHoriz Acc measure units:1Horiz Acc measure: Not ReportedSourcemap scale:-81.8778896Longitude: 36.0484609Latitude:Not ReportedContrib drainagearea units: Not ReportedContrib drainagearea:Not ReportedDrainagearea Units: Not ReportedDrainagearea value:03050101Huc code: Not ReportedMonloc desc: WellMonloc type: AV-038Monloc name: USGS-360254081524101Monloc Identifier: USGS North Carolina Water Science CenterFormal name: USGS-NCOrg. Identifier: 15 ENE 1/2 - 1 Mile Higher USGS40000892961FED USGS NC2000000007683Site id: LINVILLE LAND HARBOR POAOwner name: FTWell dep 1: 490Well depth: AAvailavili: -81.894797Longitude : ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-34 Not ReportedSourcemap scale:-81.8863889Longitude: 36.0377778Latitude:Not ReportedContrib drainagearea units: Not ReportedContrib drainagearea:Not ReportedDrainagearea Units: Not ReportedDrainagearea value:03050101Huc code: PineolaMonloc desc: WellMonloc type: AV-082Monloc name: USGS-360216081531101Monloc Identifier: USGS North Carolina Water Science CenterFormal name: USGS-NCOrg. Identifier: 18 South 1/2 - 1 Mile Lower USGS40000892891FED USGS Ground-water levels, Number of Measurements: 0 Not ReportedWellholedepth units: Not ReportedWellholedepth:ftWelldepth units: 240Welldepth:20050120Construction date: Not ReportedAquifer type: PhylliteFormation type: Piedmont and Blue Ridge crystalline-rock aquifersAquifername: USCountrycode:NAVD88Vert coord refsys: Interpolated from topographic mapVertcollection method: feetVert accmeasure units: 40Vertacc measure val:feetVert measure units: 3695Vert measure val:NAD83Horiz coord refsys: Interpolated from mapHoriz Collection method: secondsHoriz Acc measure units:1Horiz Acc measure: Not ReportedSourcemap scale:-81.8802778Longitude: 36.0397222Latitude:Not ReportedContrib drainagearea units: Not ReportedContrib drainagearea:Not ReportedDrainagearea Units: Not ReportedDrainagearea value:03050101Huc code: Nearest town: PINEOLAMonloc desc: WellMonloc type: AV-363Monloc name: USGS-360223081524901Monloc Identifier: USGS North Carolina Water Science CenterFormal name: USGS-NCOrg. Identifier: 17 SE 1/2 - 1 Mile Higher USGS40000892899FED USGS Ground-water levels, Number of Measurements: 0 Not ReportedWellholedepth units: Not ReportedWellholedepth:ftWelldepth units: 76Welldepth:Not ReportedConstruction date: Not ReportedAquifer type: PhylliteFormation type: Piedmont and Blue Ridge crystalline-rock aquifersAquifername: USCountrycode:Not ReportedVert coord refsys: Not ReportedVertcollection method: Not ReportedVert accmeasure units: Not ReportedVertacc measure val:Not ReportedVert measure units: Not ReportedVert measure val:NAD83Horiz coord refsys: Interpolated from mapHoriz Collection method: secondsHoriz Acc measure units:1Horiz Acc measure: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-35 Not ReportedSourcemap scale:-81.8836111Longitude: 36.0361111Latitude:Not ReportedContrib drainagearea units: Not ReportedContrib drainagearea:Not ReportedDrainagearea Units: Not ReportedDrainagearea value:03050101Huc code: Nearest town: CrossnoreMonloc desc: WellMonloc type: AV-400Monloc name: USGS-360210081530101Monloc Identifier: USGS North Carolina Water Science CenterFormal name: USGS-NCOrg. Identifier: F20 SSE 1/2 - 1 Mile Higher USGS40000892869FED USGS Ground-water levels, Number of Measurements: 0 Not ReportedWellholedepth units: Not ReportedWellholedepth:ftWelldepth units: 300Welldepth:20050127Construction date: Not ReportedAquifer type: PhylliteFormation type: Piedmont and Blue Ridge crystalline-rock aquifersAquifername: USCountrycode:NAVD88Vert coord refsys: Interpolated from topographic mapVertcollection method: feetVert accmeasure units: 40Vertacc measure val:feetVert measure units: 3657Vert measure val:NAD83Horiz coord refsys: Interpolated from mapHoriz Collection method: secondsHoriz Acc measure units:1Horiz Acc measure: Not ReportedSourcemap scale:-81.8825Longitude: 36.0377778Latitude:Not ReportedContrib drainagearea units: Not ReportedContrib drainagearea:Not ReportedDrainagearea Units: Not ReportedDrainagearea value:03050101Huc code: Nearest town: PINEOLAMonloc desc: WellMonloc type: AV-366Monloc name: USGS-360216081525701Monloc Identifier: USGS North Carolina Water Science CenterFormal name: USGS-NCOrg. Identifier: 19 SSE 1/2 - 1 Mile Higher USGS40000892890FED USGS Ground-water levels, Number of Measurements: 0 Not ReportedWellholedepth units: Not ReportedWellholedepth:ftWelldepth units: 160Welldepth:19990414Construction date: Not ReportedAquifer type: PhylliteFormation type: Piedmont and Blue Ridge crystalline-rock aquifersAquifername: USCountrycode:NAVD88Vert coord refsys: Interpolated from topographic mapVertcollection method: feetVert accmeasure units: 40Vertacc measure val:feetVert measure units: 3597Vert measure val:NAD83Horiz coord refsys: Interpolated from mapHoriz Collection method: secondsHoriz Acc measure units:1Horiz Acc measure: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-36 Not ReportedSourcemap scale:-81.8886111Longitude: 36.0336111Latitude:Not ReportedContrib drainagearea units: Not ReportedContrib drainagearea:Not ReportedDrainagearea Units: Not ReportedDrainagearea value:Not ReportedHuc code: Nearest town:PINEOLAMonloc desc: WellMonloc type: AV-583Monloc name: USGS-360201081531901Monloc Identifier: USGS North Carolina Water Science CenterFormal name: USGS-NCOrg. Identifier: G22 South 1/2 - 1 Mile Higher USGS40000892852FED USGS Ground-water levels, Number of Measurements: 0 Not ReportedWellholedepth units: Not ReportedWellholedepth:ftWelldepth units: 200Welldepth:20060508Construction date: Not ReportedAquifer type: PhylliteFormation type: Piedmont and Blue Ridge crystalline-rock aquifersAquifername: USCountrycode:NAVD88Vert coord refsys: Interpolated from topographic mapVertcollection method: feetVert accmeasure units: 40Vertacc measure val:feetVert measure units: 3746Vert measure val:NAD83Horiz coord refsys: Interpolated from mapHoriz Collection method: secondsHoriz Acc measure units:1Horiz Acc measure: Not ReportedSourcemap scale:-81.8836111Longitude: 36.0361111Latitude:Not ReportedContrib drainagearea units: Not ReportedContrib drainagearea:Not ReportedDrainagearea Units: Not ReportedDrainagearea value:03050101Huc code: Nearest town: LinvilleMonloc desc: WellMonloc type: AV-404Monloc name: USGS-360210081530102Monloc Identifier: USGS North Carolina Water Science CenterFormal name: USGS-NCOrg. Identifier: F21 SSE 1/2 - 1 Mile Higher USGS40000892870FED USGS Ground-water levels, Number of Measurements: 0 Not ReportedWellholedepth units: Not ReportedWellholedepth:ftWelldepth units: 605Welldepth:20060427Construction date: Not ReportedAquifer type: PhylliteFormation type: Piedmont and Blue Ridge crystalline-rock aquifersAquifername: USCountrycode:NAVD88Vert coord refsys: Interpolated from topographic mapVertcollection method: feetVert accmeasure units: 40Vertacc measure val:feetVert measure units: 3743Vert measure val:NAD83Horiz coord refsys: Interpolated from mapHoriz Collection method: secondsHoriz Acc measure units:1Horiz Acc measure: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-37 Not ReportedSourcemap scale:-81.8886111Longitude: 36.0333333Latitude:Not ReportedContrib drainagearea units: Not ReportedContrib drainagearea:Not ReportedDrainagearea Units: Not ReportedDrainagearea value:Not ReportedHuc code: Nearest town:PINEOLAMonloc desc: WellMonloc type: AV-582Monloc name: USGS-360200081531901Monloc Identifier: USGS North Carolina Water Science CenterFormal name: USGS-NCOrg. Identifier: G24 South 1/2 - 1 Mile Higher USGS40000892850FED USGS NC2000000007644Site id: HUSKINS, LARRYOwner name: FTWell dep 1: 87Well depth: AAvailavili: -81.888675Longitude : 36.033486Latitude m: W02Facility a: WELL #2Facility n: GWWater type: GWPrimary so: PINEOLACity: AVERYCounty: NCPws type: HUSKINS COURTSystem nam: NC0106428Pwsidentif: G23 South 1/2 - 1 Mile Higher NC2000000007644NC WELLS Ground-water levels, Number of Measurements: 0 Not ReportedWellholedepth units: Not ReportedWellholedepth:ftWelldepth units: 87Welldepth:Not ReportedConstruction date: Not ReportedAquifer type: PhylliteFormation type: Piedmont and Blue Ridge crystalline-rock aquifersAquifername: USCountrycode:NAVD88Vert coord refsys: Interpolated from topographic mapVertcollection method: feetVert accmeasure units: 20Vertacc measure val:feetVert measure units: 3600Vert measure val:NAD83Horiz coord refsys: Global positioning system (GPS), uncorrectedHoriz Collection method: secondsHoriz Acc measure units:.1Horiz Acc measure: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-38 Not ReportedSourcemap scale:-81.8780556Longitude: 36.0352778Latitude:Not ReportedContrib drainagearea units: Not ReportedContrib drainagearea:Not ReportedDrainagearea Units: Not ReportedDrainagearea value:03050101Huc code: Nearest town: LinvilleMonloc desc: WellMonloc type: AV-469Monloc name: USGS-360207081524101Monloc Identifier: USGS North Carolina Water Science CenterFormal name: USGS-NCOrg. Identifier: 26 SSE 1/2 - 1 Mile Higher USGS40000892864FED USGS NC2000000007642Site id: HUSKINS, LARRYOwner name: FTWell dep 1: 110Well depth: AAvailavili: -81.888641Longitude : 36.03325Latitude m: W01Facility a: WELL #1Facility n: GWWater type: GWPrimary so: PINEOLACity: AVERYCounty: NCPws type: HUSKINS COURTSystem nam: NC0106428Pwsidentif: G25 South 1/2 - 1 Mile Higher NC2000000007642NC WELLS Ground-water levels, Number of Measurements: 0 Not ReportedWellholedepth units: Not ReportedWellholedepth:ftWelldepth units: 110Welldepth:Not ReportedConstruction date: Not ReportedAquifer type: PhylliteFormation type: Piedmont and Blue Ridge crystalline-rock aquifersAquifername: USCountrycode:NAVD88Vert coord refsys: Interpolated from topographic mapVertcollection method: feetVert accmeasure units: 20Vertacc measure val:feetVert measure units: 3600Vert measure val:NAD83Horiz coord refsys: Global positioning system (GPS), uncorrectedHoriz Collection method: secondsHoriz Acc measure units:.1Horiz Acc measure: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-39 Not ReportedSourcemap scale:-81.8847222Longitude: 36.0322222Latitude:Not ReportedContrib drainagearea units: Not ReportedContrib drainagearea:Not ReportedDrainagearea Units: Not ReportedDrainagearea value:03050101Huc code: Nearest town: LINVILLEMonloc desc: WellMonloc type: AV-386Monloc name: USGS-360156081530501Monloc Identifier: USGS North Carolina Water Science CenterFormal name: USGS-NCOrg. Identifier: 28 South 1/2 - 1 Mile Higher USGS40000892842FED USGS Ground-water levels, Number of Measurements: 0 Not ReportedWellholedepth units: Not ReportedWellholedepth:ftWelldepth units: 200Welldepth:19990225Construction date: Not ReportedAquifer type: PhylliteFormation type: Piedmont and Blue Ridge crystalline-rock aquifersAquifername: USCountrycode:NAVD88Vert coord refsys: Interpolated from topographic mapVertcollection method: feetVert accmeasure units: 40Vertacc measure val:feetVert measure units: 3644Vert measure val:NAD83Horiz coord refsys: Interpolated from mapHoriz Collection method: secondsHoriz Acc measure units:1Horiz Acc measure: Not ReportedSourcemap scale:-81.8877778Longitude: 36.0322222Latitude:Not ReportedContrib drainagearea units: Not ReportedContrib drainagearea:Not ReportedDrainagearea Units: Not ReportedDrainagearea value:03050101Huc code: NewlandMonloc desc: WellMonloc type: AV-086Monloc name: USGS-360156081531601Monloc Identifier: USGS North Carolina Water Science CenterFormal name: USGS-NCOrg. Identifier: 27 South 1/2 - 1 Mile Higher USGS40000892843FED USGS Ground-water levels, Number of Measurements: 0 Not ReportedWellholedepth units: Not ReportedWellholedepth:ftWelldepth units: 925Welldepth:20060920Construction date: Not ReportedAquifer type: PhylliteFormation type: Piedmont and Blue Ridge crystalline-rock aquifersAquifername: USCountrycode:NAVD88Vert coord refsys: Interpolated from topographic mapVertcollection method: feetVert accmeasure units: 40Vertacc measure val:feetVert measure units: 3767Vert measure val:NAD83Horiz coord refsys: Interpolated from mapHoriz Collection method: secondsHoriz Acc measure units:1Horiz Acc measure: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-40 Ground-water levels, Number of Measurements: 0 Not ReportedWellholedepth units: Not ReportedWellholedepth:ftWelldepth units: 240Welldepth:20050722Construction date: Not ReportedAquifer type: PhylliteFormation type: Piedmont and Blue Ridge crystalline-rock aquifersAquifername: USCountrycode:NAVD88Vert coord refsys: Interpolated from topographic mapVertcollection method: feetVert accmeasure units: 40Vertacc measure val:feetVert measure units: 3775Vert measure val:NAD83Horiz coord refsys: Interpolated from mapHoriz Collection method: secondsHoriz Acc measure units:1Horiz Acc measure: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-41 ExtantOccurrence Status: Non VascularClassification by Type: 12214GIS ID: NC50002612NC_NHEO Historic, no evidence of destructionOccurrence Status: PlantsClassification by Type: 12593GIS ID: NC50001611NC_NHEO XOccurrence Status: Non VascularClassification by Type: 22359GIS ID: NC50001362NC_NHEO ExtantOccurrence Status: PlantsClassification by Type: 42921GIS ID: NC50001056NC_NHEO AVERYCounty:PUBStatus: 15223.6337890625Acres:Black Bear SanctuarySite Type: US Forest ServiceOwner: PisgahSite Name: NC30000202NC_WILD AVERYCounty:PUBStatus: 7928.869140625Acres:Game LandSite Type: US Forest ServiceOwner: PisgahSite Name: NC30000176NC_WILD Map ID DirectionDistance EDR ID NumberDatabase ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-42 NC50007635NC_NHEO ExtantOccurrence Status: Natural Community OccurrenceClassification by Type: 11690GIS ID: NC50006440NC_NHEO ExtantOccurrence Status: InvertebrateClassification by Type: 102934GIS ID: NC50006359NC_NHEO ExtantOccurrence Status: PlantsClassification by Type: 41323GIS ID: NC50004516NC_NHEO ExtantOccurrence Status: PlantsClassification by Type: 22726GIS ID: NC50004478NC_NHEO Historic, no evidence of destructionOccurrence Status: AnimalClassification by Type: 32085GIS ID: NC50003423NC_NHEO ExtantOccurrence Status: Natural Community OccurrenceClassification by Type: 41187GIS ID: NC50002887NC_NHEO Map ID DirectionDistance EDR ID NumberDatabase ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-43 ExtantOccurrence Status: AnimalClassification by Type: 432238GIS ID: NC50015053NC_NHEO ExtantOccurrence Status: PlantsClassification by Type: 102309GIS ID: NC50012055NC_NHEO Historic, no evidence of destructionOccurrence Status: PlantsClassification by Type: 12670GIS ID: NC50009769NC_NHEO ExtantOccurrence Status: PlantsClassification by Type: 13196GIS ID: NC50009686NC_NHEO ExtantOccurrence Status: AnimalClassification by Type: 642955GIS ID: NC50009456NC_NHEO ExtantOccurrence Status: Natural Community OccurrenceClassification by Type: 43235GIS ID: NC50008837NC_NHEO ExtantOccurrence Status: Non VascularClassification by Type: 13082GIS ID: North Carolina Locations of Natural Heritage Element Occurrence Sites: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-44 4.36Acres per Polygon: Not ReportedQuality: ANTHONY CREEK SWAMP FOREST-BOG COMPLEXSite Name: NC10000250NC_SNHA 140.73Acres per Polygon: Not ReportedQuality: PINEOLA BOGSite Name: NC10000248NC_SNHA 127.24Acres per Polygon: Not ReportedQuality: FLAT ROCK MOUNTAINSite Name: NC10000232NC_SNHA 31.83Acres per Polygon: Not ReportedQuality: LINVILLE RIVER SWAMP FOREST-BOG COMPLEXSite Name: NC10000230NC_SNHA ExtantOccurrence Status: Natural Community OccurrenceClassification by Type: 221690GIS ID: NC50015635NC_NHEO ExtantOccurrence Status: Natural Community OccurrenceClassification by Type: 13234GIS ID: NC50015558NC_NHEO Map ID DirectionDistance EDR ID NumberDatabase ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC4020675.2s Page A-45 0%100%0%9.000 pCi/LBasement Not ReportedNot ReportedNot ReportedNot ReportedLiving Area - 2nd Floor 0%0%100%0.650 pCi/LLiving Area - 1st Floor % >20 pCi/L% 4-20 pCi/L% <4 pCi/LAverage ActivityArea Number of sites tested: 2 Federal Area Radon Information for Zip Code: 28657 : Zone 3 indoor average level < 2 pCi/L. : Zone 2 indoor average level >= 2 pCi/L and <= 4 pCi/L. Note: Zone 1 indoor average level > 4 pCi/L. Federal EPA Radon Zone for AVERY County: 2 5.95.95.901 7.60.83.2723 __________________________________ Max pCi/LMin pCi/LAvg pCi/LNum Results Radon Test Results State Database: NC Radon AREA RADON INFORMATION ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS RADON ® TOPOGRAPHIC INFORMATION USGS 7.5’ Digital Elevation Model (DEM) Source: United States Geologic Survey EDR acquired the USGS 7.5’ Digital Elevation Model in 2002 and updated it in 2006. The 7.5 minute DEM corresponds to the USGS 1:24,000- and 1:25,000-scale topographic quadrangle maps. The DEM provides elevation data with consistent elevation units and projection. Scanned Digital USGS 7.5’ Topographic Map (DRG) Source: United States Geologic Survey A digital raster graphic (DRG) is a scanned image of a U.S. Geological Survey topographic map. The map images are made by scanning published paper maps on high-resolution scanners. The raster image is georeferenced and fit to the Universal Transverse Mercator (UTM) projection. HYDROLOGIC INFORMATION Flood Zone Data: This data, available in select counties across the country, was obtained by EDR in 2003 & 2011 from the Federal Emergency Management Agency (FEMA). Data depicts 100-year and 500-year flood zones as defined by FEMA. NWI: National Wetlands Inventory. This data, available in select counties across the country, was obtained by EDR in 2002, 2005 and 2010 from the U.S. Fish and Wildlife Service. State Wetlands Data: Wetlands Inventory Source: Department of Environment & Natural Resources Telephone: 919-733-2090 HYDROGEOLOGIC INFORMATION AQUIFLOW Information SystemR Source: EDR proprietary database of groundwater flow information EDR has developed the AQUIFLOW Information System (AIS) to provide data on the general direction of groundwater flow at specific points. EDR has reviewed reports submitted to regulatory authorities at select sites and has extracted the date of the report, hydrogeologically determined groundwater flow direction and depth to water table information. GEOLOGIC INFORMATION Geologic Age and Rock Stratigraphic Unit Source: P.G. Schruben, R.E. Arndt and W.J. Bawiec, Geology of the Conterminous U.S. at 1:2,500,000 Scale - A digital representation of the 1974 P.B. King and H.M. Beikman Map, USGS Digital Data Series DDS - 11 (1994). STATSGO: State Soil Geographic Database Source: Department of Agriculture, Natural Resources Conservation Services The U.S. Department of Agriculture’s (USDA) Natural Resources Conservation Service (NRCS) leads the national Conservation Soil Survey (NCSS) and is responsible for collecting, storing, maintaining and distributing soil survey information for privately owned lands in the United States. A soil map in a soil survey is a representation of soil patterns in a landscape. Soil maps for STATSGO are compiled by generalizing more detailed (SSURGO) soil survey maps. SSURGO: Soil Survey Geographic Database Source: Department of Agriculture, Natural Resources Conservation Services (NRCS) Telephone: 800-672-5559 SSURGO is the most detailed level of mapping done by the Natural Resources Conservation Services, mapping scales generally range from 1:12,000 to 1:63,360. Field mapping methods using national standards are used to construct the soil maps in the Soil Survey Geographic (SSURGO) database. SSURGO digitizing duplicates the original soil survey maps. This level of mapping is designed for use by landowners, townships and county natural resource planning and management. TC4020675.2s Page PSGR-1 PHYSICAL SETTING SOURCE RECORDS SEARCHED LOCAL / REGIONAL WATER AGENCY RECORDS FEDERAL WATER WELLS PWS: Public Water Systems Source: EPA/Office of Drinking Water Telephone: 202-564-3750 Public Water System data from the Federal Reporting Data System. A PWS is any water system which provides water to at least 25 people for at least 60 days annually. PWSs provide water from wells, rivers and other sources. PWS ENF: Public Water Systems Violation and Enforcement Data Source: EPA/Office of Drinking Water Telephone: 202-564-3750 Violation and Enforcement data for Public Water Systems from the Safe Drinking Water Information System (SDWIS) after August 1995. Prior to August 1995, the data came from the Federal Reporting Data System (FRDS). USGS Water Wells: USGS National Water Inventory System (NWIS) This database contains descriptive information on sites where the USGS collects or has collected data on surface water and/or groundwater. The groundwater data includes information on wells, springs, and other sources of groundwater. STATE RECORDS North Carolina Public Water Supply Wells Source: Department of Environmental Health Telephone: 919-715-3243 OTHER STATE DATABASE INFORMATION NC Natural Areas: Significant Natural Heritage Areas Source: Center for Geographic Information and Analysis Telephone: 919-733-2090 A polygon converage identifying sites (terrestrial or aquatic that have particular biodiversity significance. A site’s significance may be due to the presenceof rare species, rare or hight quality natural communities, or other important ecological features. NC Game Lands: Wildlife Resources Commission Game Lands Source: Center for Geographic Information and Analysis Telephone: 919-733-2090 All publicly owned game lands managed by the North Carolina Wildlife Resources Commission and as listed in Hunting and Fishing Maps. NC Natural Heritage Sites: Natural Heritage Element Occurrence Sites Source: Center for Geographic Information and Analysis Telephone: 919-733-2090 A point coverage identifying locations of rare and endangered species, occurrences of exemplary or unique natural ecosystems (terrestrial or aquatic), and special animal habitats (e.g., colonial waterbird nesting sites). RADON State Database: NC Radon Source: Department of Environment & Natural Resources Telephone: 919-733-4984 Radon Statistical and Non Statiscal Data Area Radon Information Source: USGS Telephone: 703-356-4020 The National Radon Database has been developed by the U.S. Environmental Protection Agency (USEPA) and is a compilation of the EPA/State Residential Radon Survey and the National Residential Radon Survey. The study covers the years 1986 - 1992. Where necessary data has been supplemented by information collected at private sources such as universities and research institutions. TC4020675.2s Page PSGR-2 PHYSICAL SETTING SOURCE RECORDS SEARCHED EPA Radon Zones Source: EPA Telephone: 703-356-4020 Sections 307 & 309 of IRAA directed EPA to list and identify areas of U.S. with the potential for elevated indoor radon levels. OTHER Airport Landing Facilities: Private and public use landing facilities Source: Federal Aviation Administration, 800-457-6656 Epicenters: World earthquake epicenters, Richter 5 or greater Source: Department of Commerce, National Oceanic and Atmospheric Administration Earthquake Fault Lines: The fault lines displayed on EDR’s Topographic map are digitized quaternary faultlines, prepared in 1975 by the United State Geological Survey STREET AND ADDRESS INFORMATION © 2010 Tele Atlas North America, Inc. All rights reserved. This material is proprietary and the subject of copyright protection and other intellectual property rights owned by or licensed to Tele Atlas North America, Inc. The use of this material is subject to the terms of a license agreement. You will be held liable for any unauthorized copying or disclosure of this material. TC4020675.2s Page PSGR-3 PHYSICAL SETTING SOURCE RECORDS SEARCHED The EDR Aerial Photo Decade Package C&E Manufacturing 1600 Linville Falls Highway Newland, NC 28657 Inquiry Number: 4020675.5 July 29, 2014 EDR Aerial Photo Decade Package Environmental Data Resources, Inc. (EDR) Aerial Photo Decade Package is a screening tool designed to assist environmental professionals in evaluating potential liability on a target property resulting from past activities. EDR’s professional researchers provide digitally reproduced historical aerial photographs, and when available, provide one photo per decade. When delivered electronically by EDR, the aerial photo images included with this report are for ONE TIME USE ONLY. Further reproduction of these aerial photo images is prohibited without permission from EDR. For more information contact your EDR Account Executive. Thank you for your business. Please contact EDR at 1-800-352-0050 with any questions or comments. Disclaimer - Copyright and Trademark Notice This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL, INCIDENTAL, CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report AS IS. Any analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property. Additionally, the information provided in this Report is not to be construed as legal advice. Copyright 2014 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission. EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein are the property of their respective owners. Date EDR Searched Historical Sources: Aerial Photography July 29, 2014 Target Property: 1600 Linville Falls Highway Newland, NC 28657 Year Scale Details Source 1976 Aerial Photograph. Scale: 1"=1000'Panel #: 36081-A8, Newland, NC;/Flight Date: March 28, 1976 EDR 1994 Aerial Photograph. Scale: 1"=500'Panel #: 36081-A8, Newland, NC;/DOQQ - acquisition dates: April 08, 1994 EDR 1998 Aerial Photograph. Scale: 1"=750'Panel #: 36081-A8, Newland, NC;/Flight Date: April 06, 1998 EDR 2005 Aerial Photograph. Scale: 1"=500'Panel #: 36081-A8, Newland, NC;/Flight Year: 2005 EDR 2006 Aerial Photograph. Scale: 1"=500'Panel #: 36081-A8, Newland, NC;/Flight Year: 2006 EDR 2008 Aerial Photograph. Scale: 1"=500'Panel #: 36081-A8, Newland, NC;/Flight Year: 2008 EDR 2009 Aerial Photograph. Scale: 1"=500'Panel #: 36081-A8, Newland, NC;/Flight Year: 2009 EDR 2010 Aerial Photograph. Scale: 1"=500'Panel #: 36081-A8, Newland, NC;/Flight Year: 2010 EDR 2012 Aerial Photograph. Scale: 1"=500'Panel #: 36081-A8, Newland, NC;/Flight Year: 2012 EDR 4020675.5 2 INQUIRY #: YEAR: 4020675.5 1976 = 1000' INQUIRY #: YEAR: 4020675.5 1994 = 500' INQUIRY #: YEAR: 4020675.5 1998 = 750' INQUIRY #: YEAR: 4020675.5 2005 = 500' INQUIRY #: YEAR: 4020675.5 2006 = 500' INQUIRY #: YEAR: 4020675.5 2008 = 500' INQUIRY #: YEAR: 4020675.5 2009 = 500' INQUIRY #: YEAR: 4020675.5 2010 = 500' INQUIRY #: YEAR: 4020675.5 2012 = 500' Certified Sanborn® Map Report C&E Manufacturing 1600 Linville Falls Highway Newland, NC 28657 Inquiry Number: 4020675.3 July 29, 2014 Certified Sanborn® Map Report 7/29/14 Site Name: C&E Manufacturing 1600 Linville Falls Highway Newland, NC 28657 Client Name: Hart & Hickman, PC 2923 South Tryon Street Charlotte, NC 28203-5449 Contact: Matt IngallsEDR Inquiry # 4020675.3 The Sanborn Library has been searched by EDR and maps covering the target property location as provided by Hart & Hickman, PC were identified for the years listed below. The Sanborn Library is the largest, most complete collection of fire insurance maps. The collection includes maps from Sanborn, Bromley, Perris & Browne, Hopkins, Barlow, and others. Only Environmental Data Resources Inc. (EDR) is authorized to grant rights for commercial reproduction of maps by the Sanborn Library LLC, the copyright holder for the collection. Results can be authenticated by visiting www.edrnet.com/sanborn. The Sanborn Library is continually enhanced with newly identified map archives. This report accesses all maps in the collection as of the day this report was generated. Certified Sanborn Results: Site Name:C&E Manufacturing Address:1600 Linville Falls Highway City, State, Zip:Newland, NC 28657 Cross Street: P.O. #FCB-014 Project:FCB-014 Certification #4C58-4702-B069 Library of Congress University Publications of America EDR Private Collection The Sanborn Library LLC Since 1866™ The Sanborn Library includes more than 1.2 million fire insurance maps from Sanborn, Bromley, Perris & Browne, Hopkins, Barlow and others which track historical property usage in approximately 12,000 American cities and towns. Collections searched: Sanborn® Library search results Certification # 4C58-4702-B069 UNMAPPED PROPERTY This report certifies that the complete holdings of the Sanborn Library, LLC collection have been searched based on client supplied target property information, and fire insurance maps covering the target property were not found. Limited Permission To Make Copies Hart & Hickman, PC (the client) is permitted to make up to FIVE photocopies of this Sanborn Map transmittal and each fire insurance map accompanying this report solely for the limited use of its customer. No one other than the client is authorized to make copies. Upon request made directly to an EDR Account Executive, the client may be permitted to make a limited number of additional photocopies. This permission is conditioned upon compliance by the client, its customer and their agents with EDR's copyright policy; a copy of which is available upon request. Disclaimer - Copyright and Trademark notice This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL, INCIDENTAL CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property. Additionally, the information provided in this Report is not to be construed as legal advice. Copyright 2014 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission. EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein are the property of their respective owners. 4020675 - 3 page 2 C&E Manufacturing 1600 Linville Falls Highway Newland, NC 28657 Inquiry Number: 4020675.9 August 25, 2014 The EDR-City Directory Abstract 6 Armstrong Road Shelton, CT 06484 800.352.0050 www.edrnet.comEnvironmental Data Resources IncEnvironmental Data Resources IncEnvironmental Data Resources IncEnvironmental Data Resources Inc TABLE OF CONTENTS SECTION Executive Summary Findings City Directory Images Thank you for your business. Please contact EDR at 1-800-352-0050 with any questions or comments. Disclaimer - Copyright and Trademark Notice This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OR DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL, INCIDENTAL, CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor should they be interpreted as providing any facts regarding, or prediction orforecast of, any environmental risk for any property. Only a Phase I Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property. Additionally, the information provided in this Report is not to be construed as legal advice. Copyright 2014 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of Environmental Data Resources, Inc. or its affiliates is prohibited without prior written permission. EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein are the property of their respective owners. EXECUTIVE SUMMARY DESCRIPTION Environmental Data Resources, Inc.’s (EDR) City Directory Abstract is a screening tool designed to assist environmental professionals in evaluating potential liability on a target property resulting from past activities. EDR’s City Directory Abstract includes a search and abstract of available city directory data. For each address, the directory lists the name of the corresponding occupant at five year intervals. Business directories including city, cross reference and telephone directories were reviewed, if available, at approximately five year intervals for the years spanning 1999 through 2013. This report compiles information gathered in this review by geocoding the latitude and longitude of properties identified and gathering information about properties within 1320 feet of the target property. A summary of the information obtained is provided in the text of this report. RESEARCH SUMMARY The following research sources were consulted in the preparation of this report. An "X" indicates where information was identified in the source and provided in this report. Source TPYear Adjoining Text Abstract Source Image 2013 Cole Information Services -X X - 2008 Cole Information Services - --- 2003 Cole Information Services - --- 1999 Cole Information Services - X X - 4020675-9 Page 1 FINDINGS TARGET PROPERTY INFORMATION ADDRESS 1600 Linville Falls Highway Newland, NC 28657 FINDINGS DETAIL Target Property research detail. 4020675-9 Page 2 FINDINGS ADJOINING PROPERTY DETAIL The following Adjoining Property addresses were researched for this report. Detailed findings are provided for each address. LINVILLE FALLS HWY 1596 LINVILLE FALLS HWY Year Uses Source 1999 ADDCO MANUFACTURING COMPANY Cole Information Services 1710 LINVILLE FALLS HWY Year Uses Source 2013 CLASSIC STONE WORKS INC Cole Information Services 4020675-9 Page 3 FINDINGS TARGET PROPERTY: ADDRESS NOT IDENTIFIED IN RESEARCH SOURCE The following Target Property addresses were researched for this report, and the addresses were not identified in the research source. Address Researched Address Not Identified in Research Source 1600 Linville Falls Highway 2013, 2008, 2003, 1999 ADJOINING PROPERTY: ADDRESSES NOT IDENTIFIED IN RESEARCH SOURCE The following Adjoining Property addresses were researched for this report, and the addresses were not identified in research source. Address Researched Address Not Identified in Research Source 1596 LINVILLE FALLS HWY 2013, 2008, 2003 1710 LINVILLE FALLS HWY 2008, 2003, 1999 Appendix D Safety Data Sheets Appendix E Site Photographs Photograph 2: Building 2 located in the central portion of the site. FC B -01 4 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 1: Building 1 located in the northern portion of the site. ADDCO FACILITY NEWLAND, NORTH CAROLINA Photograph 4: Solar farm located in the southeastern portion of the site. 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 3: Building 3 located in the southern portion of the site. FC B -01 4 ADDCO FACILITY NEWLAND, NORTH CAROLINA Photograph 6: Waste oil drum staged in Building 1. 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 5: Manufacturing area in Building 1. FC B -01 4 ADDCO FACILITY NEWLAND, NORTH CAROLINA Photograph 8: Oil-stained soil identified in hole to floor of Building 2. 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 7: Waste oil drums staged between Buildings 2 and 3. ADDCO FACILITY NEWLAND, NORTH CAROLINA FC B -01 4 Photograph 10: Oil stains to sink in Building 1. 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 9: Oil-stained soil identified in hole to floor of Building 2. FC B -01 4 ADDCO FACILITY NEWLAND, NORTH CAROLINA Photograph 12: Floor drain in Building 3 restroom. 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 11: Powder coating application area/oven located in the southwestern portion of Building 3. FC B -01 4 ADDCO FACILITY NEWLAND, NORTH CAROLINA Photograph 14: Vent hose identified southwest of Building 3. 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 13: Sink in Building 3 restroom. FC B -01 4 ADDCO FACILITY NEWLAND, NORTH CAROLINA Photograph 16: Propane AST located south of Building 1. 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 15: Former paint booth identified in the northwestern portion of Building 3. FC B -01 4 ADDCO FACILITY NEWLAND, NORTH CAROLINA Photograph 18: Septic tank located west of Building 3. 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 17: Septic tank located south of Building 1. FC B -01 4 ADDCO FACILITY NEWLAND, NORTH CAROLINA SEPTIC TANK SEPTIC TANK Photograph 20: Dumpster located between Buildings 2 and 3. 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 19: Pad transformer located south of Building 1. FC B -01 4 ADDCO FACILITY NEWLAND, NORTH CAROLINA Photograph 22: Abandoned car located southwest of Building 3. 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 21: Scrap wood identified in the southwestern portion of the property. FC B -01 4 ADDCO FACILITY NEWLAND, NORTH CAROLINA Appendix F Curriculum Vitae S:\AAA-Master Marketing Info\CVs\2013 CVs\Quattrocchi 2013 CV.docx CURRICULUM VITAE JAY QUATTROCCHI Title: Environmental Scientist Expertise: Phase I Environmental Site Assessments (ESA) Wetland and Stream delineations Endangered and Threatened species Surveys 404 Clean Water Act Permitting Water Quality Sampling Experience Summary Jay has over six (6) years of experience in the environmental consulting industry. He is currently serving as an Environmental Scientist at Hart & Hickman performing Phase I Environmental Site Assessments and wetland and stream delineations. He also has experience performing Phase II soil sampling, water quality sampling and NPDES inspections. Credentials B.S. in Environmental and Natural Resources, Clemson University, 2006 Phase I Environmental Site Assessment Training, Environmental Institute, 2007 Basic Wetland Delineator Training, Institute for Wetland & Environmental Education & Research, 2008 Forty-hour Hazardous Waste Operations and Emergency Response (HAZWOPER) training, Compliance Solutions, 2013 Red Cross First Aid and CPR Training, 2013 Key Projects Performed numerous Phase I Environmental Site Assessments (Phase I ESAs) at residential developments, small and large undeveloped tracts, industrial sites, shopping centers, and commercial developments throughout the southeast. Performed USACE compliant wetland and stream delineations on sites throughout the southeast (Alabama, Georgia, North Carolina, and Virginia), including Fort Benning, Columbus, GA; Fort Gordon, Augusta, GA; Georgia Power’s Plant McDonough, Cobb County, GA.; Georgia Power’s Plant Scherer, Monroe Co., GA; and a 25-mile Georgia Power transmission line in Augusta, GA. Delineated Georgia State Waters on four proposed maneuver areas (approximately 137 miles) at Fort Benning, GA. Performed Red-cockaded woodpecker and Gopher Tortoise surveys at several Georgia military installations, including Fort Benning and Fort Gordon. Conducted vegetation, fish, and benthic surveys for mitigation and restoration projects throughout the southeast. Monitored and sampled restored streams for water quality (turbidity, dissolved oxygen, Fecal Coliform bacteria, etc.). Installed and maintained water monitoring wells. Performed National Pollutant Discharge Elimination System (NPDES) site inspections to reduce erosion and manage sediment on residential, utility, sewer, and water line construction sites. Tested water samples to ensure compliance with state turbidity standards. Conducted a wetland and stream delineation and endangered species survey near Valdosta on a 50-mile transmission corridor for Georgia Transmission Corporation. s:\aaa-master marketing info\cvs\2012 cvs\ingalls-2010.doc CURRICULUM VITAE MATTHEW J. INGALLS Title: Project Manager Expertise: Phase I Environmental Assessments Asbestos Certified Inspector and Management Planner Lead-Based Paint Assessments Wetlands and Stream Delineation and Permitting Endangered Species Surveys Environmental Assessments Experience Summary 19 years experience providing multi-site Environmental Site Assessments (Phase I ESAs). US EPA AHERA certified asbestos inspector, AHERA asbestos management planner and lead supervisor. Has experience with environmental audits of various facility types and the delineation of wetlands and streams. Has experience performing endangered species surveys and Environmental Assessments (EAs). Also has extensive experience performing soil and ground water sampling. Credentials B.S. in Environmental Design, North Carolina State University (1988) 40 - Hour Health & Safety Training for Hazardous Waste Operations and Emergency Response (1991 – present) Inspector & Management Planner for Asbestos in Buildings, Medical University of South Carolina (1993) with annual AHERA refresher update courses (1994 to 2006) Lead Paint Abatement Worker Training, Maryland State Department of the Environment, AAA Environmental, Inc, (1992) Wetlands Identification and Delineation, Coastal Carolina University (1997) and North Carolina State University (1999) NC Classification and Assessment, North Carolina State University (2005) Piedmont Wetland Plant Identification, North Carolina State University (2005) Licenses NC Asbestos Inspector No. 11433 NC Asbestos Management Planner No. 20718 SC Asbestos Consultant/Management Planner No. 21620 VA Asbestos Inspector No. 3303 003017 VA Professional Wetland Delineator No. 3402 000053 Key Projects Performed, reviewed, and managed over 1,300 Environmental Site Assessments (Phase I ESAs) conducted on undeveloped land and industrial, commercial, and residential facilities located throughout the US. Performed and managed over 400 asbestos surveys of apartment complexes, shopping centers, adult care facilities, hotels, and manufacturing facilities. Managed an asbestos survey and abatement of a former ice cream dairy complex located on behalf of the City of Charlotte. Coordinated activities with State and Local regulators and provided oversight until completion of the demolition. Managed clean up of a 700,000 sq. ft. manufacturing facility contaminated with mercury, lead, asbestos fibers located in Salem, Massachusetts Participated in the asbestos/lead sampling of an EPA Superfund site in Southern Pines, North Carolina. Prepared the asbestos/lead section of the Remedial Design Plan. Managed the asbestos removal activities of multiple residential structures located in Charlotte, NC prior to demolition. Met with local officials for a clearance inspection. Performed and managed numerous environmental reviews of Phase I and II ESA reports on behalf of lenders. Conducted multiple wetlands determination and endangered species screening surveys for sites in North Carolina, Florida, Virginia, Georgia, and South Carolina. Also performed wetland permitting activities on projects located in NC and SC. Extensive Phase II soil and ground water experience involving the installation and sampling of numerous soil borings and shallow, intermediate, and deep monitoring works. Performed and managed multiple Phase I and II ESAs associated with Brownfields Development Projects. Managed an EA of thirty radio tower sites located in Mecklenburg County in support of the Federal funded CharMeck Connect Project. Phase II ESA Addco Facility 1600 Linville Falls Hwy Avery County, North Carolina H&H Job No. FCB-014 November 18, 2014 Via Email November 18, 2014 First Citizens Bank 4300 Six Forks Road Raleigh, NC 27609-5718 Attention: Mr. Steve Pollok Sr. Commercial Resolution Officer Re: Phase II ESA Addco Facility 1600 Linville Falls Highway Newland, Avery County, North Carolina H&H Job No.: FCB-014 1.0 Executive Summary This report presents the methods and results of a Phase II Environmental Site Assessment (ESA) conducted by Hart & Hickman, PC (H&H) at the Addco property (subject site) located at 1600 Linville Falls Highway in Avery County, North Carolina. The purpose of the Phase II ESA activities was to assess the potential for impact from areas of concern associated with current and historical on-site automotive parts manufacturing operations identified during a Phase I ESA conducted by H&H in August 2014. The results of our assessment activities indicate diesel range total petroleum hydrocarbons (TPH- DRO) were detected in soil borings SB-5 and SB-6 collected below the concrete floor at locations adjacent to metal fabrication machines in Building 2 at concentrations of 15.4 and 166 milligrams per kilogram (mg/kg), respectively. The detections are above the North Carolina Department of Environment and Natural Resources (DENR) Action Level of 10 mg/kg. Mr. Steve Pollok November 18, 2014 Page 2 Volatile organic compounds (VOCs) were not detected above DENR Inactive Hazardous Sites Branch (IHSB) residential, industrial, or Protection of Groundwater (POG) soil remediation goals (SRGs) in samples collected adjacent to the septic tank (SB-1), within the septic field (SB-2), below the former paint booth vent (SB-3), or below the powder coating booth vent (SB-4). Additionally, polynuclear aromatic hydrocarbons (PAHs) were not detected above DENR IHSB SRGs in soil samples collected near the septic tank (SB-1) or septic field (SB-2). Manganese was detected in soil sample SB-2 (1-3 ft) collected from the septic leach field at a concentration above residential and POG SRGs. Manganese was also detected above residential SRGs in soil sample SB-3 (1-2 ft) collected below the former paint booth vent and soil sample SB-4 (1-2 ft) collected below the powder coating booth vent. The manganese concentrations in the soil samples listed above exceed site specific background concentrations collected from a soil boring SB-BG (1-2 ft) advanced in an undisturbed area in the eastern portion of the property. Although the manganese concentrations in the soil samples listed above exceed residential and POG SRGs, and site specific background concentrations, the manganese concentrations are below industrial SRGs and are within the range of published literature background concentrations for North Carolina and conterminous United States (US) soils. Naphthalene, lead, and manganese were detected above North Carolina Groundwater Standards (2L groundwater standards) in a groundwater sample collected from temporary monitoring well TMW-2 advanced adjacent to the septic system leach field west of Building 3. Naphthalene and manganese were also detected above 2L groundwater standards in a groundwater sample collected from TMW-1 advanced downgradient of the septic tank south of Building 1. Additional PAHs, VOCs, and HSL metals were not detected above 2L groundwater standards in groundwater samples collected from TMW-1 and TMW-2. S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Report\Phase II ESA - 1600 Linville Falls Hwy - (FCB).doc Mr. Steve Pollok November 18, 2014 Page 3 2.0 Property Description & Background The subject site is developed as an industrial manufacturing facility and consists of an approximately 5.71-acre parcel of land. The property is occupied by three industrial buildings including a 9,000-square ft manufacturing and office building (Building 1), a 14,500 square ft manufacturing/warehouse building (Building 2), and a 20,000-square ft shipping/receiving warehouse with a powder coating application area and former paint booth (Building 3). A solar farm, which was installed and is managed by Eagle Electron Power Partners (EEPP), is located on the southeastern portion of the property. The western portion of the site consists of undeveloped land. A Site Location Map and a Sample Location Map are included as Figures 1 and 2, respectively. H&H conducted Phase I ESA activities at the Site in August 2014 and identified the following potential areas of concern: • potential discharge of powder coating materials, coolant, and petroleum-based products generated during manufacturing activities at the site into the facility septic system which consists of two septic tanks (west of Building3 and south of Building 1) and septic field (west of Building 3); • oil staining to the ground surface in concrete cut-out areas adjacent to metal fabrication machines in Building 2; and • staining to exterior vents for the former paint and powder coat application booths on the exterior of Building 3. H&H conducted Phase II ESA soil and groundwater sampling activities at the subject site on September 25, 2014 to assess the potential for impact from the areas of environmental concern described above. The methods and results of Phase II ESA activities are presented in the following sections. S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Report\Phase II ESA - 1600 Linville Falls Hwy - (FCB).doc Mr. Steve Pollok November 18, 2014 Page 4 3.0 Phase II Scope of Work 3.1 Utility Clearance Prior to conducting soil and groundwater sampling activities, H&H contacted North Carolina One-Call, the public utility locator to mark subsurface utilities located on the Site. In addition, Probe Utility, LLC, a private utility locater was contracted to locate and demark subsurface utilities in the areas of the soil borings and temporary wells. As an additional safety precaution, each boring was initially advanced using a hand auger to a depth of at least 5 feet (ft) below ground surface (bgs) to clear the boring of possible undocumented subsurface utility lines. 3.2 Sampling Activities Soil Sampling H&H utilized Environmental Drilling & Probing Services, LLC (EPDS) to advance soil borings using Geoprobe® direct-push technology (DPT) and hand auger methods. Soil samples were field screened for the presence of odor, staining, and elevated photoionization detector (PID) readings one. A soil sample from each boring that exhibited the greatest evidence of impact (i.e., elevated PID readings, staining, and/or petroleum/chemical odors) was submitted for laboratory analysis. A summary of soil sample locations and analyses are presented below. • Soil sample SB-1 was located adjacent to the septic tank for Buildings 1 and 2 and advanced to a depth of 15 ft bgs. Based upon field screening, a sample was collected from a depth of 5 to 7 ft bgs and submitted for laboratory analysis for VOCs by EPA Method 8260B, PAHs by EPA Method 8270D, and HSL metals by EPA Method 6010C. • Soil sample SB-2 was located adjacent to the septic leach field west of Building 3 and was advanced to a depth of 15 ft bgs. Based upon field screening, a sample was collected S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Report\Phase II ESA - 1600 Linville Falls Hwy - (FCB).doc Mr. Steve Pollok November 18, 2014 Page 5 from a depth of 1 to 3 ft bgs and submitted for laboratory analysis for VOCs by EPA Method 8260B, PAHs by EPA Method 8270D, and HSL metals by EPA Method 6010C. • Soil sample SB-3 was located beneath the former paint booth vent along the western side of Building 3 and was advanced to a depth of 5 ft bgs. Based upon field screening, a sample was collected from a depth of 1 to 2 feet and submitted for laboratory analysis for VOCs by EPA Method 8260B and HSL metals by EPA Method 6010C. • Soil sample SB-4 was located beneath the powder coat application booth located along the western side of Building 3 and was advanced to a depth of 5 ft bgs. Based upon field screening, a sample was collected from a depth of 1 to 2 feet and submitted for laboratory analysis for VOCs by EPA Method 8260B and HSL metals by EPA Method 6010C. • Soil sample SB-5 was located adjacent to a metal fabrication machine in Building 2 and was advanced to a depth of 5 ft bgs. Based upon field screening, a sample was collected from a depth of 1 to 2 ft bgs and submitted for laboratory analysis for TPH-DRO and gasoline range TPH (TPH-GRO) by EPA Method 8015C. • Soil sample SB-6 was located adjacent to a metal fabrication machine in Building 2 and was advanced to a depth of 5 ft bgs. Based upon field screening, a sample was collected from a depth of 1 to 2 ft bgs and submitted for laboratory analysis for TPH-GRO/DRO by EPA Method 8015C. • A background sample was advanced to a depth of 1 to 2 feet bgs and was located on the eastern portion of the subject site. The sample was submitted for laboratory analysis for HSL metals by EPA Method 6010C. S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Report\Phase II ESA - 1600 Linville Falls Hwy - (FCB).doc Mr. Steve Pollok November 18, 2014 Page 6 The samples were submitted to TestAmerica Laboratories, Inc. (TestAmerica), a North Carolina- certified analytical laboratory. Groundwater Sampling H&H oversaw advancement of two temporary groundwater monitoring wells (TMW-1 and TMW-2) at the subject site by EPDS utilizing DPT methods. TMW-1 was installed at a location adjacent to and downgradient of the facility’s septic tank. TMW-2 was installed at a location downgradient of the facility’s septic leach field. The temporary monitoring wells were constructed with one-inch diameter PVC with 10-ft sections of pre-packed screens set to bracket the water table. The temporary groundwater monitoring wells were installed to 15 ft bgs. Following temporary well installation, H&H gauged the temporary monitoring wells. The water levels in TMW-1 and TMW-2 were both approximately 9 ft bgs. H&H subsequently developed TMW-1 and TMW-2 utilizing low-flow techniques. H&H continued development until turbidity in groundwater was below 10 nephelometric turbidity units (NTUs) in both temporary monitoring wells. After purging the wells, H&H collected groundwater samples from TMW-1 and TWM-2 and submitted the samples to TestAmerica for analysis of VOCs by EPA Method 8260, PAHs by EPA Method 8270, and HSL metals by EPA Method 6010C. Soil boring and temporary monitoring well logs are presented in Appendix A. 3.3 Boring Abandonment and Investigation Derived Waste Upon completion of groundwater and soil sampling activities, EPDS abandoned the borings by removing well screen/riser materials, filling the borings with grout, and patching the surfaces to match the surrounding area. Soil cuttings and groundwater generated during Phase II ESA activities were spread on-site in accordance with DENR guidance. S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Report\Phase II ESA - 1600 Linville Falls Hwy - (FCB).doc Mr. Steve Pollok November 18, 2014 Page 7 3.4 QA/QC Process H&H utilized standard quality assurance/quality control (QA/QC) processes during the Phase II ESA activities. Non-dedicated sampling equipment, including DPT tooling, the water level meter, and the hand auger, were decontaminated using Liquinox® detergent and deionized water prior to and between each sampling location. H&H and EPDS wore nitrile gloves while handling samples, and the groundwater samples were collected using new tubing. Groundwater and soil samples were collected in laboratory-provided containers and immediately placed on ice. A completed chain-of-custody (COC) record accompanied the samples and included the sample designation, date and time collected, matrix, sample container information, and requested analyses. H&H sampling personnel signed the completed COC record, and the samples were transported to TestAmerica by local courier and FedEx. 4.0 Site-Specific Topography, Geology, & Hydrogeology 4.1 Topography The elevation of the subject site is approximately 3,600 feet above mean sea level. The topographic gradient in the area of the subject site is in a generally southerly direction toward the Linville River located approximately 0.4-mile south of the subject site. An area topographic map is included as Figure 1. 4.2 Physical Setting Geology Avery County, including the subject property, is located within the Blue Ridge physiographic province of North Carolina. This province is a northeast trending zone extending from Georgia through Virginia and ranges in width from approximately 15 to 55 miles in North Carolina. The S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Report\Phase II ESA - 1600 Linville Falls Hwy - (FCB).doc Mr. Steve Pollok November 18, 2014 Page 8 Blue Ridge is a deeply dissected mountainous area of numerous steep mountain ridges, intermontane basins, and trench valleys that intersect at all angles and give the area its rugged mountain character. The site is located within the Grandfather Mountain window of the Blue Ridge province which is characterized by bedrock composed of meta-sedimetary and meta-volcanic rocks. Based on the 1985 Geologic Map of North Carolina, the bedrock underlying the subject property is composed of greenstone and meta-arkose with interlayered sedimentary rocks. Overlying the bedrock in many areas is a zone of residual soil or saprolite which is developed from the in-situ weathering of the underlying rocks. The saprolite is typically composed of unconsolidated silts, clays, sand, and rock fragments. Hydrogeology Groundwater generally occurs under water table conditions within the interconnected saprolite and bedrock zones. The primary source of ground water in the area is from precipitation that reaches the water table through infiltration. The saprolite is generally considered to be a recharge medium for the bedrock aquifer because it holds precipitation and allows ground water to gradually infiltrate into the bedrock joints, faults, and fractures. Groundwater flow is typically from upland areas to lowland areas where ground water discharges to streams. During Phase II ESA groundwater sampling activities, H&H determined that the depth to groundwater was approximately 9 ft below the ground surface in the two temporary monitoring wells (TMW-1 and TMW-2) advanced at the site. S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Report\Phase II ESA - 1600 Linville Falls Hwy - (FCB).doc Mr. Steve Pollok November 18, 2014 Page 9 5.0 Analytical Laboratory Results Laboratory analytical data reports and chain-of-custody records are included as Appendix B. Soil TPH-DRO was detected in soil samples SB-5 (1-2 ft) and SB-6 (1-2 ft) at concentrations of 15.4 mg/kg and 166 mg/kg, respectively, which is above the DENR Action Level of 10 mg/kg. SB-5 and SB-6 are located adjacent to metal fabrication machines and below the concrete floor of Building 2. A trace concentration of the VOC 1,2,3-trichlorobenzne (0.00279 mg/kg) was detected in SB-4 (1-2 ft) located in soil beneath the powder coat booth vent on the western side of Building 3. In addition, the VOC acetone (0.22 and 0.0938 mg/kg) was detected in soil samples collected in close proximity to the septic tank for Building 1 (SB-1 [5-7 ft]) and the septic leach field west of Building 3 (SB-2 [1-3 ft]), respectively. Trace concentrations of the PAHs fluoranthene (0.087 mg/kg) and pyrene (0.0724 mg/kg) were detected in the soil sample collected from SB-1 (5-7 ft). The detected VOCs and PAHs were not detected at concentrations above IHSB Residential, Industrial, or POG SRGs in soil samples collected at the site. Manganese was detected in soil sample SB-2 (1 to 3 ft) collected from the septic leach field, soil sample SB-3 (1-2 ft) collected below the former paint booth vent, and in soil sample SB-4 (1-2 ft) collected below the powder coat booth vent at concentrations above residential and POG SRGs. The manganese concentrations in the soil samples listed above exceed site specific background concentrations detected from a background soil boring SB-BG (1-2 ft) advanced in an undisturbed area in the eastern portion of the property. The manganese concentrations detected in the background soil sample also exceeded the POG SRG. Although the manganese concentrations in the soil samples from potential areas of concern exceed residential and POG SRGs and site specific background concentrations, the manganese concentrations are below S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Report\Phase II ESA - 1600 Linville Falls Hwy - (FCB).doc Mr. Steve Pollok November 18, 2014 Page 10 industrial SRGs and are within the range of published literature background concentrations for North Carolina and conterminous US soils (see Table 1). Concentrations of arsenic (SB-2), chromium (SB-1 and SB-4), copper (SB-1 and SB-4), lead (SB-2 and SB-4), and nickel (SB-1, SB-2, and SB-4) were detected in soil samples at concentrations above site specific background levels. However, these metal concentrations fall within the range of published literature background concentrations for North Carolina and conterminous US soils (see Table 1). Groundwater Naphthalene (30.4 µg/L), lead (26.1 µg/L), and manganese (7,150 µg/L) were detected above their respective 2L groundwater standards of 6 µg/L, 15 µg/L, and 50 µg/L in a groundwater sample collected from temporary monitoring well TMW-2 advanced adjacent to the septic system leach field. Naphthalene (11.4 µg/L) and manganese (591 µg/L) were also detected above 2L groundwater standards in a groundwater sample collected from TMW-1 advanced downgradient of the septic system. Additional PAHs, VOCs, or HSL metals were not detected above 2L groundwater standards in groundwater samples collected from TMW-1 and TMW-2. 6.0 Findings and Recommendations H&H conducted soil and groundwater assessment activities at the subject site to assess the potential for impact from areas of concern associated with historical and current automotive parts manufacturing operations identified during a Phase I ESA conducted in August 2014. The results of the assessment activities indicate soil impacts were detected above the NC DENR TPH Action Level in two shallow borings advanced below the concrete floor of Building 2. Specifically, TPH-DRO was detected at 15.4 mg/kg and 30 mg/kg in SB-5 (1-2 ft) and SB-6 (1-2 ft), respectively. The DENR Action Level for TPH-DRO is 10 mg/kg. S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Report\Phase II ESA - 1600 Linville Falls Hwy - (FCB).doc Mr. Steve Pollok November 18, 2014 Page 11 Naphthalene, lead, and manganese were detected above 2L groundwater standards in a groundwater sample collected from temporary monitoring well TMW-2 advanced adjacent to the septic leach field west of Building 3. Naphthalene and manganese were also detected above their 2L groundwater standards in a groundwater sample collected from TMW-1 advanced downgradient of the septic tank south of Building 1. Additional PAHs, VOCs, or HSL Metals were not detected above 2L groundwater standards in groundwater samples collected from TMW-1 and TMW-2. The petroleum impacts identified in shallow soil below Building 2 and in groundwater in the vicinity of the facility’s septic tank and septic leach field indicates a release apparently from current and former auto parts manufacturing operations. Because petroleum impacts do not appear to be the result of a release from an underground storage tank (UST), the release incident will likely be addressed under the DENR Division of Waste Management UST Section as a non- UST petroleum release. Further assessment is warranted to determine if the elevated lead and manganese concentrations in groundwater above 2L groundwater standards in the vicinity of the facility’s septic tank and septic leach field and elevated levels of manganese near the septic tank, septic field, former paint booth vent, and powder coat booth vent are the result of current/former auto parts manufacturing activities, or if they are representative of naturally occurring background metal concentrations. If the elevated lead and manganese concentrations are determined to be the result of current/former auto part manufacturing activities, the release incident will likely be addressed under the DENR IHSB. Alternatively, First Citizens Bank may want to consider obtaining a Brownfields Agreement for the property. The Brownfields Agreement is a tool for a prospective purchaser or an entity taking owner via foreclosure of a property to reduce uncertainties in environmental liability. The following are potential benefits of a Brownfields Agreement: S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Report\Phase II ESA - 1600 Linville Falls Hwy - (FCB).doc Mr. Steve Pollok November 18, 2014 Page 12 1) The Brownfields Agreement provides liability protection in the form of a covenant not- to-sue for contamination at a site. 2) The liability protection in the Brownfields Agreement extends to new owners provided that they adhere to the land use restrictions placed on the property. 3) Implementation of engineering controls or remedies under the Brownfields Program will likely be required to prevent exposure and make the site suitable for reuse rather than to meet environmental standards required by DENR. 4) The Brownfields property tax incentive significantly reduces property taxes on the improved value for five years after completion of improvements to the property. Thank you for the opportunity to assist with this project. Should you have any questions or require any additional information concerning this report, please feel free to contact us at (704) 586-0007. Sincerely, Hart & Hickman, PC Hart & Hickman, PC Matt Ingalls Steve Hart, PG Project Manager Principal S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Report\Phase II ESA - 1600 Linville Falls Hwy - (FCB).doc Mr. Steve Pollok November 18, 2014 Page 13 Attachments: Figure 1: Site Location Map Figure 2: Sample Location Map Table 1: Summary of Soil Analytical Data Table 2: Summary of Groundwater Analytical Data Appendix A: Soil Boring Logs Appendix B: Laboratory Analytical Data Reports S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Report\Phase II ESA - 1600 Linville Falls Hwy - (FCB).doc Figures TITLE PROJECT SITE LOCATION MAP ADDCO FACILITY NEWLAND, NORTH CAROLINA DATE: JOB NO: REVISION NO: FIGURE NO: 8-20-14 0 1FCB-014 0 2000 4000 APPROXIMATE SCALE IN FEETN U.S.G.S. QUADRANGLE MAP QUADRANGLE 7.5 MINUTE SERIES (TOPOGRAPHIC) NEWLAND, NC 1994 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) SITE Tables Table 1 Summary of Soil Analytical Data 1600 Linville Falls Hwy Newland, Avery County, North Carolina H&H Job No. FCB-014 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Tables\Analytical Data Tables.xlsx 10/14/2014 Table 1 (Page 2 of 3) Hart & Hickman, PC Sample Location Septic Tank Septic Field Former Paint Booth Vent Powder Coat Booth Vent Building 2 - Metal Fabrication Machine Building 2 - Metal Fabrication Machine Background Soil Sample Sample ID SB-1 SB-2 SB-3 SB-4 SB-5 SB-6 SB-BGSample Depth (ft)5-7 1-3 1-2 1-2 1-2 1-2 1-2 Sample Date 9/25/2014 9/25/2014 9/25/2014 9/25/2014 9/25/2014 9/25/2014 9/25/2014 Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg VOCs (8260)mg/kg mg/kg 1,2,3-Trichlorobenzene <0.192 < 0.0264 < 0.00217 0.00279 NA NA NA 9.8 130 NL ---- Acetone 0.22 0.0938 < 0.0542 < 0.0621 NA NA NA 12,000 100,000 24 ---- PAHs (8270) Fluoranthene 0.087 < 0.0669 NA NA NA NA NA 460 6000 330 ---- Pyrene 0.0724 < 0.0669 NA NA NA NA NA 340 4600 220 ---- HSL Metals (6010/7471/7196)Antimony < 14.6 < 14.4 < 12.5 < 12.6 NA NA <14.7 6.2 94 0.9 <1.0-8.8**0.76** Arsenic < 2.93 5.26 < 2.49 < 2.52 NA NA 3.38 0.67 3 5.8 1.0 - 18 4.8 Beryllium < 1.46 < 1.44 1.35 < 1.26 NA NA <1.47 32 460 63 ND - 2.0 0.11 Cadmium < 1.46 < 1.44 < 1.25 < 1.26 NA NA <1.47 14 200 3 1.0 - 10*4.3* Chromium 10.5 15.6 5.36 25 NA NA 12.0 24000 100000 360000 7.0 - 300 65 Chromium VI AP AP AP AP NA NA AP 0.29 6.3 3.8 NE NE Copper 24.2 13.9 11.5 18.7 NA NA 17.3 620 9400 700 3.0 - 100 34 Lead 21.7 36.2 12.6 36.4 NA NA 23.9 400 800 270 ND - 50 16 Manganese 140 1,050 415 636 NA NA 102 360 5200 65 8.0 - 3,394*594* Nickel 10.7 10.7 8.03 28.4 NA NA 10.4 300 4400 130 ND - 150 23 Selenium < 2.93 < 2.87 < 2.49 < 2.52 NA NA <2.94 78 1200 2.1 NE NE Silver < 1.46 < 1.44 < 1.25 < 1.26 NA NA 1.68 78 1200 3.4 ND-5.0 NE Thallium < 2.93 < 2.87 < 2.49 < 2.52 NA NA <2.94 0.16 2.4 0.28 NE NE Zinc 71 78.6 67.9 113 NA NA 83.7 4600 70000 1200 25 - 124 56 Mercury < 0.149 < 0.143 < 0.124 < 0.124 NA NA <0.152 1.9 3.1 1 0.03 - 0.52 0.121 TPH-GRO/DRO (8015) Diesel Range Organics NA NA NA NA 15.4 166 NA Gasoline Range Organics NA NA NA NA < 6.44 <6.85 NANotes:Units reported in mg/kg 1. NC DENR Inactive Hazardous Sites Branch (IHSB) Residential and Industrial Health Based Soil Remediation Goals (SRGs) - September 2014 2. NC DENR IHSB Protection of Groundwater Soil Remediation Goals (POG SRG) - September 2014 3. NC or Conterminous - US Background Metals in Soil values from Elements in North American Soils by Dragun and Chekiri, 2005 4. Because Chromium (VI) has not been analyzed yet, Chromium (III) screening criteria used for total Chromium * Values for Southeastern USA soils used because North Carolina soils not specified **Values for Eastern USA soils used because North Carolina soils not specified TPH = total petroleum hydrocarbons; DRO = Diesel Range Organics; GRO = Gasoline Range Organics VOCs = Volatile Organic Compounds; PAHs = Polynuclear Aromatic Hydrocarbons; HSL = Hazardous Substance List Only VOC and PAH constituents with at least one detection shown EPA Method follows parameter in parenthesis NA = Not Analyzed; NE = Not Established; AP=Analysis Pending Bold indicates an exceedance of the DENR Action Level; Underline indicates exceedance of Residential SGR; and Italics indicate exceedance of Protection of Groundwater PSRG Background Metals Range 3 Average Background Metals 3Residential SRG1 (mg/kg) Industrial SRG1 (mg/kg) Protection of Groundwater PSRG (mg/kg)2 10 Screening Levels NC DENR ACTION LEVEL (mg/kg) Table 2 Summary of Groundwater Analytical Data 1600 Linville Falls Hwy Newland, Avery County, North Carolina H&H Job No. FCB-014 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Tables\Analytical Data Tables.xlsx 10/14/2014 Table 1 (Page 1 of 3) Hart & Hickman, PC Location Septic Tank Septic System Sample ID TMW-1 TMW-2 Sample Date 09/25/14 09/25/14 Units µg/L µg/L µg/L µg/L µg/L VOCs (8260B) Ethylbenzene < 1.0 1.1 600 34.9 152 PAHs (8270D) Acenaphthene 9.5 8.03 80 NL NL Fluorene 2.53 2.58 300 NL NL Naphthalene 11.4 30.0 6 34.8 146 Phenanthrene <1.82 2.6 200 NL NL HSL Metals Antimony < 0.01 < 0.01 1.0 NL NL Arsenic < 0.01 < 0.01 10 NL NL Beryllium < 0.004 < 0.004 4.0 NL NL Cadmium < 0.001 < 0.001 2 NL NL Chromium < 0.005 9.8 10 NL NL Copper < 0.01 < 0.01 1 (mg/L)NL NL Lead < 0.005 26.1 15 NL NL Manganese 591 7,150 50 NL NL Nickel < 0.01 < 0.01 100 NL NL Selenium < 0.01 < 0.01 20 NL NL Silver < 0.005 < 0.005 20 NL NL Thallium < 0.01 < 0.01 0.2 NL NL Zinc < 0.05 < 0.05 1 (mg/L)NL NL Mercury < 0.0002 < 0.0002 1 0.134 0.563 Notes: 1) NCAC 02L Groundwater Quality Standards and Interim Maximum Allowable Concentrations (April 2013) 2) Division of Waste Management Residential Vapor Intrusion Groundwater Screening Level - June 2014 3) Division of Waste Management Non-Residential Vapor Intrusion Groundwater Screening Level - June 2014 4) Bold indicates exceedance of NC 2L Groundwater Standard VOCs = Volatile Organic Compounds; PAHs = Polynuclear Aromatic Hydrocarbons; and HSL= Hazardous Substance List Screening Criteria Groundwater Samples 2L Groundwater Quality Standard1 DWM Residential Groundwater VI Screening Level2 DWM Non-Residential Groundwater VI Screening Level3 Appendix A Soil Boring Logs 0 0 0 0 0 0 0 0 0 0 0 0 0 0 (GW) Yellowish brown (CH) Yellowish brown with gray mottles (CH) Dark brown with yellowish brown mottles (CH) Gray - indications of groundwater (reduction) Bottom of borehole at 15.0 feet. DRAWN BY: SURFACE ELEV:LOGGED BY JQ BORING COMPLETED:9/24/14 BORING STARTED 9/25/14DRILLING CONTRACTOR:EPDS DEPTH TO WATER: TOTAL DEPTH:15 Remarks: DRILL RIG/ METHOD:DPT SAMPLING METHOD:Soil Boring 1/Temporary MonitoringWell 1 DE P T H (f t ) DE P T H (f t ) LI T H O L O G Y OV A ( p p m ) WELL DIAGRAM RE C O V E R Y ( % ) BK G . SA M P . MATERIAL DESCRIPTION BORING NUMBER SB-1/TMW-1 Sheet 1 of 1 PROJECT:Addco Facility JOB NUMBER:FCB-014 LOCATION:1600 Linville Falls Hwy, Newland, NC LO G O F B O R I N G - H A R T H I C K M A N . G D T - 1 0 / 1 4 / 1 4 1 6 : 5 3 - S : \ A A A - M A S T E R P R O J E C T S \ F I R S T C I T I Z E N S B A N K - F C B \ F C B - 0 1 4 C & E M A N U F A C T U R I N G - N E W L A N D , N C \ P H A S E I I \ B O R I N G \ F C B - 0 1 4 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0 5 10 15 0 5 10 15 0 0 0 0 0 0 0 1.3 1 0 0 0 0 0 (CL-ML) Yellowish brown (CH) Gray (CH) Gray with yellowish brown mottles Bottom of borehole at 15.0 feet. DRAWN BY: SURFACE ELEV:LOGGED BY JQ BORING COMPLETED:9/25/14 BORING STARTED 9/25/14DRILLING CONTRACTOR:EPDS DEPTH TO WATER: TOTAL DEPTH:15 Remarks: DRILL RIG/ METHOD:DPT SAMPLING METHOD:Soil Boring 2/Temporary MonitoringWell 2 DE P T H (f t ) DE P T H (f t ) LI T H O L O G Y OV A ( p p m ) WELL DIAGRAM RE C O V E R Y ( % ) BK G . SA M P . MATERIAL DESCRIPTION BORING NUMBER SB-2/TMW-2 Sheet 1 of 1 PROJECT:Addco Facility JOB NUMBER:FCB-014 LOCATION:1600 Linville Falls Hwy, Newland, NC LO G O F B O R I N G - H A R T H I C K M A N . G D T - 1 0 / 1 4 / 1 4 1 6 : 5 3 - S : \ A A A - M A S T E R P R O J E C T S \ F I R S T C I T I Z E N S B A N K - F C B \ F C B - 0 1 4 C & E M A N U F A C T U R I N G - N E W L A N D , N C \ P H A S E I I \ B O R I N G \ F C B - 0 1 4 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0 5 10 15 0 5 10 15 0 0 0 0 0 0 0 0 (CL) Yellowish brown (CL) Yellowish brown Bottom of borehole at 5.0 feet. DRAWN BY: SURFACE ELEV:LOGGED BY JQ BORING COMPLETED:9/25/14 BORING STARTED 9/25/14DRILLING CONTRACTOR:EPDS DEPTH TO WATER: TOTAL DEPTH:5 Remarks: DRILL RIG/ METHOD:DPT SAMPLING METHOD:Soil Boring 3 DE P T H (f t ) DE P T H (f t ) LI T H O L O G Y OV A ( p p m ) WELL DIAGRAM RE C O V E R Y ( % ) BK G . SA M P . MATERIAL DESCRIPTION BORING NUMBER SB-3 Sheet 1 of 1 PROJECT:Addco Facility JOB NUMBER:FCB-014 LOCATION:1600 Linville Falls Hwy, Newland, NC LO G O F B O R I N G - H A R T H I C K M A N . G D T - 1 0 / 1 4 / 1 4 1 6 : 5 3 - S : \ A A A - M A S T E R P R O J E C T S \ F I R S T C I T I Z E N S B A N K - F C B \ F C B - 0 1 4 C & E M A N U F A C T U R I N G - N E W L A N D , N C \ P H A S E I I \ B O R I N G \ F C B - 0 1 4 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0.0 2.5 5.0 0.0 2.5 5.0 0 0 0 0 0 0 0 0 (ML) Yellowish brown (CL-ML) Yellowish brown Bottom of borehole at 5.0 feet. DRAWN BY: SURFACE ELEV:LOGGED BY JQ BORING COMPLETED:9/25/14 BORING STARTED 9/25/14DRILLING CONTRACTOR:EPDS DEPTH TO WATER: TOTAL DEPTH:5 Remarks: DRILL RIG/ METHOD:DPT SAMPLING METHOD:Soil Boring 4 DE P T H (f t ) DE P T H (f t ) LI T H O L O G Y OV A ( p p m ) WELL DIAGRAM RE C O V E R Y ( % ) BK G . SA M P . MATERIAL DESCRIPTION BORING NUMBER SB-4 Sheet 1 of 1 PROJECT:Addco Facility JOB NUMBER:FCB-014 LOCATION:1600 Linville Falls Hwy, Newland, NC LO G O F B O R I N G - H A R T H I C K M A N . G D T - 1 0 / 1 4 / 1 4 1 6 : 5 3 - S : \ A A A - M A S T E R P R O J E C T S \ F I R S T C I T I Z E N S B A N K - F C B \ F C B - 0 1 4 C & E M A N U F A C T U R I N G - N E W L A N D , N C \ P H A S E I I \ B O R I N G \ F C B - 0 1 4 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0.0 2.5 5.0 0.0 2.5 5.0 0 0 0 0 0 0.6 0 0 (GP-GM) Reddish yellow (CL-ML) Reddish yellow Bottom of borehole at 5.0 feet. DRAWN BY: SURFACE ELEV:LOGGED BY JQ BORING COMPLETED:9/25/14 BORING STARTED 9/25/14DRILLING CONTRACTOR:EPDS DEPTH TO WATER: TOTAL DEPTH:5 Remarks: DRILL RIG/ METHOD:DPT SAMPLING METHOD:Soil Boring 5 DE P T H (f t ) DE P T H (f t ) LI T H O L O G Y OV A ( p p m ) WELL DIAGRAM RE C O V E R Y ( % ) BK G . SA M P . MATERIAL DESCRIPTION BORING NUMBER SB-5 Sheet 1 of 1 PROJECT:Addco Facility JOB NUMBER:FCB-014 LOCATION:1600 Linville Falls Hwy, Newland, NC LO G O F B O R I N G - H A R T H I C K M A N . G D T - 1 0 / 1 4 / 1 4 1 6 : 5 3 - S : \ A A A - M A S T E R P R O J E C T S \ F I R S T C I T I Z E N S B A N K - F C B \ F C B - 0 1 4 C & E M A N U F A C T U R I N G - N E W L A N D , N C \ P H A S E I I \ B O R I N G \ F C B - 0 1 4 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0.0 2.5 5.0 0.0 2.5 5.0 0 0 0 0 0 0 0 0 (GP-GM) Reddish yellow (CL-ML) Reddish yellow Bottom of borehole at 5.0 feet. DRAWN BY: SURFACE ELEV:LOGGED BY JQ BORING COMPLETED:9/25/14 BORING STARTED 9/25/14DRILLING CONTRACTOR:EPDS DEPTH TO WATER: TOTAL DEPTH:5 Remarks: DRILL RIG/ METHOD:DPT SAMPLING METHOD:Soil Boring 6 DE P T H (f t ) DE P T H (f t ) LI T H O L O G Y OV A ( p p m ) WELL DIAGRAM RE C O V E R Y ( % ) BK G . SA M P . MATERIAL DESCRIPTION BORING NUMBER SB-6 Sheet 1 of 1 PROJECT:Addco Facility JOB NUMBER:FCB-014 LOCATION:1600 Linville Falls Hwy, Newland, NC LO G O F B O R I N G - H A R T H I C K M A N . G D T - 1 0 / 1 4 / 1 4 1 6 : 5 3 - S : \ A A A - M A S T E R P R O J E C T S \ F I R S T C I T I Z E N S B A N K - F C B \ F C B - 0 1 4 C & E M A N U F A C T U R I N G - N E W L A N D , N C \ P H A S E I I \ B O R I N G \ F C B - 0 1 4 . G P J 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) 3334 Hillsborough Street Raleigh, North Carolina 27607 919-847-4241(p) 919-847-4261(f) 0.0 2.5 5.0 0.0 2.5 5.0 Appendix B Laboratory Analytical Data Reports ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Nashville 2960 Foster Creighton Drive Nashville, TN 37204 Tel: (615)726-0177 TestAmerica Job ID: 490-62390-1 TestAmerica Sample Delivery Group: FCB-014 Task 2 Client Project/Site: 1600 Linville Falls Hwy, Avery County,NC For: Hart & Hickman, PC 2923 S Tryon Street Suite 100 Charlotte, North Carolina 28203 Attn: Jay Quattrocchi Authorized for release by: 10/6/2014 11:08:50 AM Roxanne Connor, Senior Project Manager (615)301-5761 roxanne.connor@testamericainc.com Designee for Ken Hayes, Project Manager II (615)301-5035 ken.hayes@testamericainc.com The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. 1 2 3 4 5 6 7 8 9 10 11 12 13 Table of Contents Client: Hart & Hickman, PC Project/Site: 1600 Linville Falls Hwy, Avery County,NC TestAmerica Job ID: 490-62390-1 SDG: FCB-014 Task 2 Page 2 of 74 TestAmerica Nashville10/6/2014 Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .25 QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .60 Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .65 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .68 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .69 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .70 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .74 1 2 3 4 5 6 7 8 9 10 11 12 13 Sample Summary TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID Client Sample ID ReceivedCollectedMatrix 490-62390-1 SB-1 (5-7)Solid 09/25/14 09:27 09/26/14 09:00 490-62390-2 SB-2 (1-3)Solid 09/25/14 10:50 09/26/14 09:00 490-62390-3 SB-3 (1-2)Solid 09/25/14 11:30 09/26/14 09:00 490-62390-4 SB-4 (1-2)Solid 09/25/14 11:45 09/26/14 09:00 490-62390-5 SB-5 (1-2)Solid 09/25/14 13:00 09/26/14 09:00 490-62390-6 SB-6 (1-2)Solid 09/25/14 12:45 09/26/14 09:00 490-62390-7 TMW-1 Water 09/25/14 12:17 09/26/14 09:00 490-62390-8 TMW-2 Water 09/25/14 14:01 09/26/14 09:00 490-62390-9 Background (1-2)Solid 09/25/14 13:37 09/26/14 09:00 TestAmerica Nashville Page 3 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Case Narrative Client: Hart & Hickman, PC TestAmerica Job ID: 490-62390-1 Project/Site: 1600 Linville Falls Hwy, Avery County,NC SDG: FCB-014 Task 2 Job ID: 490-62390-1 Laboratory: TestAmerica Nashville Narrative Job Narrative 490-62390-1 Comments No additional comments. Receipt The samples were received on 9/26/2014 9:00 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 2.7º C. GC/MS VOA Method(s) 8260B: Due to sample matrix effect on the internal standard (ISTD), a dilution was required for the following sample(s): SB-1 (5-7) (490-62390-1). Method(s) 8260B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with batch 194478 Method(s) 8260B: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for batch 194702 recovered outside control limits for the following analytes: Chloromethane and Bromomethane. These analytes were biased high in the LCS and were not detected in the associated samples; therefore, the data have been reported. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. GC/MS Semi VOA Method(s) 8270D: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with batch 194206 and 194350. Method(s) 8270D: Batch 194221 is reported without a matrix spike/matrix spike duplicate (MS/MSD). The batch MS/MSD was originally performed on another client's sample, and this test was on hold at client request. This MS/MSD result does not have immediate bearing on any samples except for the actual sample spiked. The associated laboratory control sample (LCS) met acceptance criteria and provides long-term precision and accuracy for this batch. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. GC VOA No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. GC Semi VOA No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. Metals No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. Organic Prep Method(s) 3510C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with batch 194206 and 194350. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. VOA Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. TestAmerica NashvillePage 4 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Definitions/Glossary TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Qualifiers GC/MS VOA Qualifier Description F1 MS and/or MSD Recovery exceeds the control limits Qualifier *ISTD response or retention time outside acceptable limits *LCS or LCSD exceeds the control limits E Result exceeded calibration range. Metals Qualifier Description 4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not applicable. Qualifier F1 MS and/or MSD Recovery exceeds the control limits ^ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: Instrument related QC exceeds the control limits. Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference) Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica Nashville Page 5 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-1Client Sample ID: SB-1 (5-7) Matrix: SolidDate Collected: 09/25/14 09:27 Percent Solids: 67.1Date Received: 09/26/14 09:00 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone 0.220 0.0894 mg/Kg ☼09/27/14 10:09 10/01/14 21:49 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Benzene ND 0.192 mg/Kg 09/27/14 10:08 10/03/14 23:13 1 ☼Bromobenzene ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Bromochloromethane ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Bromodichloromethane ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Bromoform ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1☼Bromomethane ND 0.0894 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼2-Butanone (MEK)ND 0.00894 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Carbon disulfide ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Carbon tetrachloride ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Chlorobenzene ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Chlorodibromomethane ND 0.00894 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Chloroethane ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Chloroform ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Chloromethane ND 0.192 mg/Kg 09/27/14 10:08 10/03/14 23:13 1☼2-Chlorotoluene ND 0.192 mg/Kg 09/27/14 10:08 10/03/14 23:13 1 ☼4-Chlorotoluene ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼cis-1,2-Dichloroethene ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼cis-1,3-Dichloropropene ND 0.480 mg/Kg 09/27/14 10:08 10/03/14 23:13 1☼1,2-Dibromo-3-Chloropropane ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼1,2-Dibromoethane (EDB)ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Dibromomethane ND 0.192 mg/Kg 09/27/14 10:08 10/03/14 23:13 1 ☼1,2-Dichlorobenzene ND 0.192 mg/Kg 09/27/14 10:08 10/03/14 23:13 1 ☼1,3-Dichlorobenzene ND 0.192 mg/Kg 09/27/14 10:08 10/03/14 23:13 1☼1,4-Dichlorobenzene ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Dichlorodifluoromethane ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼1,1-Dichloroethane ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼1,2-Dichloroethane ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1☼1,1-Dichloroethene ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼1,2-Dichloroethene, Total ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼1,2-Dichloropropane ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼1,3-Dichloropropane ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼2,2-Dichloropropane ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1☼1,1-Dichloropropene ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Diisopropyl ether ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Ethylbenzene ND 0.480 mg/Kg 09/27/14 10:08 10/03/14 23:13 1 ☼Hexachlorobutadiene ND 0.0894 mg/Kg 09/27/14 10:09 10/01/14 21:49 1☼2-Hexanone ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Isopropylbenzene ND 0.0179 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Methylene Chloride ND 0.0894 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼4-Methyl-2-pentanone (MIBK)ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Methyl tert-butyl ether ND 0.480 mg/Kg 09/27/14 10:08 10/03/14 23:13 1☼Naphthalene ND 0.192 mg/Kg 09/27/14 10:08 10/03/14 23:13 1 ☼n-Butylbenzene ND 0.192 mg/Kg 09/27/14 10:08 10/03/14 23:13 1 ☼N-Propylbenzene ND 0.192 mg/Kg 09/27/14 10:08 10/03/14 23:13 1 ☼p-Isopropyltoluene ND 0.192 mg/Kg 09/27/14 10:08 10/03/14 23:13 1☼sec-Butylbenzene ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Styrene ND 0.192 mg/Kg 09/27/14 10:08 10/03/14 23:13 1 ☼tert-Butylbenzene ND TestAmerica Nashville Page 6 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-1Client Sample ID: SB-1 (5-7) Matrix: SolidDate Collected: 09/25/14 09:27 Percent Solids: 67.1Date Received: 09/26/14 09:00 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00358 mg/Kg ☼09/27/14 10:09 10/01/14 21:49 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 0.192 mg/Kg 09/27/14 10:08 10/03/14 23:13 1 ☼1,1,2,2-Tetrachloroethane ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1☼Tetrachloroethene ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Toluene ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼trans-1,2-Dichloroethene ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼trans-1,3-Dichloropropene ND 0.192 mg/Kg 09/27/14 10:08 10/03/14 23:13 1☼1,2,3-Trichlorobenzene ND 0.192 mg/Kg 09/27/14 10:08 10/03/14 23:13 1 ☼1,2,4-Trichlorobenzene ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼1,1,1-Trichloroethane ND 0.00894 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼1,1,2-Trichloroethane ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Trichloroethene ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1☼Trichlorofluoromethane ND 0.192 mg/Kg 09/27/14 10:08 10/03/14 23:13 1 ☼1,2,3-Trichloropropane ND 0.192 mg/Kg 09/27/14 10:08 10/03/14 23:13 1 ☼1,2,4-Trimethylbenzene ND 0.192 mg/Kg 09/27/14 10:08 10/03/14 23:13 1 ☼1,3,5-Trimethylbenzene ND 0.00358 mg/Kg 09/27/14 10:09 10/01/14 21:49 1☼Vinyl chloride ND 0.00536 mg/Kg 09/27/14 10:09 10/01/14 21:49 1 ☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)110 *70-130 09/27/14 10:09 10/01/14 21:49 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery 4-Bromofluorobenzene (Surr)103 09/27/14 10:08 10/03/14 23:13 170-130 Dibromofluoromethane (Surr)115 09/27/14 10:09 10/01/14 21:49 170-130 Dibromofluoromethane (Surr)91 09/27/14 10:08 10/03/14 23:13 170-130 1,2-Dichloroethane-d4 (Surr)117 09/27/14 10:09 10/01/14 21:49 170-130 1,2-Dichloroethane-d4 (Surr)85 09/27/14 10:08 10/03/14 23:13 170-130 Toluene-d8 (Surr)111 09/27/14 10:09 10/01/14 21:49 170-130 Toluene-d8 (Surr)87 09/27/14 10:08 10/03/14 23:13 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 0.0663 mg/Kg ☼09/30/14 13:47 10/02/14 00:59 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 0.0663 mg/Kg 09/30/14 13:47 10/02/14 00:59 1 ☼Acenaphthylene ND 0.0663 mg/Kg 09/30/14 13:47 10/02/14 00:59 1 ☼Anthracene ND 0.0663 mg/Kg 09/30/14 13:47 10/02/14 00:59 1☼Benzo[a]anthracene ND 0.0663 mg/Kg 09/30/14 13:47 10/02/14 00:59 1 ☼Benzo[a]pyrene ND 0.0663 mg/Kg 09/30/14 13:47 10/02/14 00:59 1 ☼Benzo[b]fluoranthene ND 0.0663 mg/Kg 09/30/14 13:47 10/02/14 00:59 1 ☼Benzo[g,h,i]perylene ND 0.0663 mg/Kg 09/30/14 13:47 10/02/14 00:59 1 ☼Benzo[k]fluoranthene ND 0.0663 mg/Kg 09/30/14 13:47 10/02/14 00:59 1 ☼Chrysene ND 0.0663 mg/Kg 09/30/14 13:47 10/02/14 00:59 1 ☼Dibenz(a,h)anthracene ND 0.0663 mg/Kg 09/30/14 13:47 10/02/14 00:59 1 ☼Fluoranthene 0.0870 0.0663 mg/Kg 09/30/14 13:47 10/02/14 00:59 1 ☼Fluorene ND 0.0663 mg/Kg 09/30/14 13:47 10/02/14 00:59 1☼Indeno[1,2,3-cd]pyrene ND 0.0663 mg/Kg 09/30/14 13:47 10/02/14 00:59 1 ☼Naphthalene ND 0.0663 mg/Kg 09/30/14 13:47 10/02/14 00:59 1 ☼Phenanthrene ND 0.0663 mg/Kg 09/30/14 13:47 10/02/14 00:59 1 ☼Pyrene 0.0724 2-Fluorobiphenyl (Surr)68 29-120 09/30/14 13:47 10/02/14 00:59 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Nitrobenzene-d5 (Surr)68 09/30/14 13:47 10/02/14 00:59 127-120 TestAmerica Nashville Page 7 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-1Client Sample ID: SB-1 (5-7) Matrix: SolidDate Collected: 09/25/14 09:27 Percent Solids: 67.1Date Received: 09/26/14 09:00 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Terphenyl-d14 (Surr)84 13-120 09/30/14 13:47 10/02/14 00:59 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Method: 6010C - Metals (ICP) RL MDL Antimony ND 14.6 mg/Kg ☼09/29/14 13:45 09/30/14 16:58 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 2.93 mg/Kg 09/29/14 13:45 09/30/14 16:58 1 ☼Arsenic ND 1.46 mg/Kg 09/29/14 13:45 09/30/14 16:58 1☼Beryllium ND 1.46 mg/Kg 09/29/14 13:45 09/30/14 16:58 1 ☼Cadmium ND 1.46 mg/Kg 09/29/14 13:45 09/30/14 16:58 1 ☼Chromium 10.5 2.93 mg/Kg 09/29/14 13:45 09/30/14 16:58 1 ☼Copper 24.2 1.46 mg/Kg 09/29/14 13:45 09/30/14 16:58 1☼Lead 21.7 4.39 mg/Kg 09/29/14 13:45 09/30/14 16:58 1 ☼Manganese 140 2.93 mg/Kg 09/29/14 13:45 09/30/14 16:58 1 ☼Nickel 10.7 2.93 mg/Kg 09/29/14 13:45 09/30/14 16:58 1 ☼Selenium ND 1.46 mg/Kg 09/29/14 13:45 09/30/14 16:58 1 ☼Silver ND 2.93 mg/Kg 09/29/14 13:45 09/30/14 16:58 1 ☼Thallium ND 14.6 mg/Kg 09/29/14 13:45 09/30/14 16:58 1 ☼Zinc 71.0 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury ND 0.149 mg/Kg ☼10/01/14 08:22 10/01/14 10:58 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier General Chemistry RL RL Percent Solids 67 0.10 %09/29/14 13:04 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier TestAmerica Nashville Page 8 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-2Client Sample ID: SB-2 (1-3) Matrix: SolidDate Collected: 09/25/14 10:50 Percent Solids: 68.3Date Received: 09/26/14 09:00 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone 0.0938 0.0660 mg/Kg ☼09/27/14 10:09 10/01/14 21:19 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Benzene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Bromobenzene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Bromochloromethane ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Bromodichloromethane ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Bromoform ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1☼Bromomethane ND 0.0660 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼2-Butanone (MEK)ND 0.00660 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Carbon disulfide ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Carbon tetrachloride ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Chlorobenzene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Chlorodibromomethane ND 0.00660 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Chloroethane ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Chloroform ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Chloromethane ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1☼2-Chlorotoluene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼4-Chlorotoluene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼cis-1,2-Dichloroethene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼cis-1,3-Dichloropropene ND 0.00660 mg/Kg 09/27/14 10:09 10/01/14 21:19 1☼1,2-Dibromo-3-Chloropropane ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼1,2-Dibromoethane (EDB)ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Dibromomethane ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼1,2-Dichlorobenzene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼1,3-Dichlorobenzene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1☼1,4-Dichlorobenzene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Dichlorodifluoromethane ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼1,1-Dichloroethane ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼1,2-Dichloroethane ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1☼1,1-Dichloroethene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼1,2-Dichloroethene, Total ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼1,2-Dichloropropane ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼1,3-Dichloropropane ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼2,2-Dichloropropane ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1☼1,1-Dichloropropene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Diisopropyl ether ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Ethylbenzene ND 0.00660 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Hexachlorobutadiene ND 0.0660 mg/Kg 09/27/14 10:09 10/01/14 21:19 1☼2-Hexanone ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Isopropylbenzene ND 0.0132 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Methylene Chloride ND 0.0660 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼4-Methyl-2-pentanone (MIBK)ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Methyl tert-butyl ether ND 0.00660 mg/Kg 09/27/14 10:09 10/01/14 21:19 1☼Naphthalene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼n-Butylbenzene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼N-Propylbenzene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼p-Isopropyltoluene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1☼sec-Butylbenzene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Styrene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼tert-Butylbenzene ND TestAmerica Nashville Page 9 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-2Client Sample ID: SB-2 (1-3) Matrix: SolidDate Collected: 09/25/14 10:50 Percent Solids: 68.3Date Received: 09/26/14 09:00 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00264 mg/Kg ☼09/27/14 10:09 10/01/14 21:19 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼1,1,2,2-Tetrachloroethane ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1☼Tetrachloroethene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Toluene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼trans-1,2-Dichloroethene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼trans-1,3-Dichloropropene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1☼1,2,3-Trichlorobenzene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼1,2,4-Trichlorobenzene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼1,1,1-Trichloroethane ND 0.00660 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼1,1,2-Trichloroethane ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Trichloroethene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1☼Trichlorofluoromethane ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼1,2,3-Trichloropropane ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼1,2,4-Trimethylbenzene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼1,3,5-Trimethylbenzene ND 0.00264 mg/Kg 09/27/14 10:09 10/01/14 21:19 1☼Vinyl chloride ND 0.00396 mg/Kg 09/27/14 10:09 10/01/14 21:19 1 ☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)100 70-130 09/27/14 10:09 10/01/14 21:19 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Dibromofluoromethane (Surr)112 09/27/14 10:09 10/01/14 21:19 170-130 1,2-Dichloroethane-d4 (Surr)117 09/27/14 10:09 10/01/14 21:19 170-130 Toluene-d8 (Surr)101 09/27/14 10:09 10/01/14 21:19 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 0.0669 mg/Kg ☼09/30/14 13:47 10/02/14 01:23 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 0.0669 mg/Kg 09/30/14 13:47 10/02/14 01:23 1 ☼Acenaphthylene ND 0.0669 mg/Kg 09/30/14 13:47 10/02/14 01:23 1 ☼Anthracene ND 0.0669 mg/Kg 09/30/14 13:47 10/02/14 01:23 1☼Benzo[a]anthracene ND 0.0669 mg/Kg 09/30/14 13:47 10/02/14 01:23 1 ☼Benzo[a]pyrene ND 0.0669 mg/Kg 09/30/14 13:47 10/02/14 01:23 1 ☼Benzo[b]fluoranthene ND 0.0669 mg/Kg 09/30/14 13:47 10/02/14 01:23 1 ☼Benzo[g,h,i]perylene ND 0.0669 mg/Kg 09/30/14 13:47 10/02/14 01:23 1☼Benzo[k]fluoranthene ND 0.0669 mg/Kg 09/30/14 13:47 10/02/14 01:23 1 ☼Chrysene ND 0.0669 mg/Kg 09/30/14 13:47 10/02/14 01:23 1 ☼Dibenz(a,h)anthracene ND 0.0669 mg/Kg 09/30/14 13:47 10/02/14 01:23 1 ☼Fluoranthene ND 0.0669 mg/Kg 09/30/14 13:47 10/02/14 01:23 1 ☼Fluorene ND 0.0669 mg/Kg 09/30/14 13:47 10/02/14 01:23 1☼Indeno[1,2,3-cd]pyrene ND 0.0669 mg/Kg 09/30/14 13:47 10/02/14 01:23 1 ☼Naphthalene ND 0.0669 mg/Kg 09/30/14 13:47 10/02/14 01:23 1 ☼Phenanthrene ND 0.0669 mg/Kg 09/30/14 13:47 10/02/14 01:23 1 ☼Pyrene ND 2-Fluorobiphenyl (Surr)51 29-120 09/30/14 13:47 10/02/14 01:23 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Nitrobenzene-d5 (Surr)51 09/30/14 13:47 10/02/14 01:23 127-120 Terphenyl-d14 (Surr)61 09/30/14 13:47 10/02/14 01:23 113-120 TestAmerica Nashville Page 10 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-2Client Sample ID: SB-2 (1-3) Matrix: SolidDate Collected: 09/25/14 10:50 Percent Solids: 68.3Date Received: 09/26/14 09:00 Method: 6010C - Metals (ICP) RL MDL Antimony ND 14.4 mg/Kg ☼09/29/14 13:45 09/30/14 17:02 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 2.87 mg/Kg 09/29/14 13:45 09/30/14 17:02 1 ☼Arsenic 5.26 1.44 mg/Kg 09/29/14 13:45 09/30/14 17:02 1☼Beryllium ND 1.44 mg/Kg 09/29/14 13:45 09/30/14 17:02 1 ☼Cadmium ND 1.44 mg/Kg 09/29/14 13:45 09/30/14 17:02 1 ☼Chromium 15.6 2.87 mg/Kg 09/29/14 13:45 09/30/14 17:02 1 ☼Copper 13.9 1.44 mg/Kg 09/29/14 13:45 09/30/14 17:02 1☼Lead 36.2 4.31 mg/Kg 09/29/14 13:45 09/30/14 17:02 1 ☼Manganese 1050 2.87 mg/Kg 09/29/14 13:45 09/30/14 17:02 1 ☼Nickel 10.7 2.87 mg/Kg 09/29/14 13:45 09/30/14 17:02 1 ☼Selenium ND 1.44 mg/Kg 09/29/14 13:45 09/30/14 17:02 1 ☼Silver ND 2.87 mg/Kg 09/29/14 13:45 09/30/14 17:02 1☼Thallium ND 14.4 mg/Kg 09/29/14 13:45 09/30/14 17:02 1 ☼Zinc 78.6 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury ND 0.143 mg/Kg ☼10/01/14 08:22 10/01/14 11:00 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier General Chemistry RL RL Percent Solids 68 0.10 %09/29/14 13:04 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier TestAmerica Nashville Page 11 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-3Client Sample ID: SB-3 (1-2) Matrix: SolidDate Collected: 09/25/14 11:30 Percent Solids: 77.6Date Received: 09/26/14 09:00 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone ND 0.0542 mg/Kg ☼09/27/14 10:09 10/01/14 20:50 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Benzene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Bromobenzene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Bromochloromethane ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Bromodichloromethane ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Bromoform ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1☼Bromomethane ND 0.0542 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼2-Butanone (MEK)ND 0.00542 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Carbon disulfide ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Carbon tetrachloride ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Chlorobenzene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Chlorodibromomethane ND 0.00542 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Chloroethane ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Chloroform ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Chloromethane ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1☼2-Chlorotoluene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼4-Chlorotoluene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼cis-1,2-Dichloroethene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼cis-1,3-Dichloropropene ND 0.00542 mg/Kg 09/27/14 10:09 10/01/14 20:50 1☼1,2-Dibromo-3-Chloropropane ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼1,2-Dibromoethane (EDB)ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Dibromomethane ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼1,2-Dichlorobenzene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼1,3-Dichlorobenzene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1☼1,4-Dichlorobenzene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Dichlorodifluoromethane ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼1,1-Dichloroethane ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼1,2-Dichloroethane ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1☼1,1-Dichloroethene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼1,2-Dichloroethene, Total ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼1,2-Dichloropropane ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼1,3-Dichloropropane ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼2,2-Dichloropropane ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1☼1,1-Dichloropropene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Diisopropyl ether ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Ethylbenzene ND 0.00542 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Hexachlorobutadiene ND 0.0542 mg/Kg 09/27/14 10:09 10/01/14 20:50 1☼2-Hexanone ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Isopropylbenzene ND 0.0108 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Methylene Chloride ND 0.0542 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼4-Methyl-2-pentanone (MIBK)ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Methyl tert-butyl ether ND 0.00542 mg/Kg 09/27/14 10:09 10/01/14 20:50 1☼Naphthalene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼n-Butylbenzene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼N-Propylbenzene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼p-Isopropyltoluene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1☼sec-Butylbenzene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Styrene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼tert-Butylbenzene ND TestAmerica Nashville Page 12 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-3Client Sample ID: SB-3 (1-2) Matrix: SolidDate Collected: 09/25/14 11:30 Percent Solids: 77.6Date Received: 09/26/14 09:00 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00217 mg/Kg ☼09/27/14 10:09 10/01/14 20:50 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼1,1,2,2-Tetrachloroethane ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1☼Tetrachloroethene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Toluene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼trans-1,2-Dichloroethene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼trans-1,3-Dichloropropene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1☼1,2,3-Trichlorobenzene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼1,2,4-Trichlorobenzene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼1,1,1-Trichloroethane ND 0.00542 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼1,1,2-Trichloroethane ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Trichloroethene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1☼Trichlorofluoromethane ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼1,2,3-Trichloropropane ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼1,2,4-Trimethylbenzene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼1,3,5-Trimethylbenzene ND 0.00217 mg/Kg 09/27/14 10:09 10/01/14 20:50 1☼Vinyl chloride ND 0.00325 mg/Kg 09/27/14 10:09 10/01/14 20:50 1 ☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)87 70-130 09/27/14 10:09 10/01/14 20:50 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Dibromofluoromethane (Surr)107 09/27/14 10:09 10/01/14 20:50 170-130 1,2-Dichloroethane-d4 (Surr)110 09/27/14 10:09 10/01/14 20:50 170-130 Toluene-d8 (Surr)98 09/27/14 10:09 10/01/14 20:50 170-130 Method: 6010C - Metals (ICP) RL MDL Antimony ND 12.5 mg/Kg ☼09/29/14 13:45 09/30/14 17:05 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 2.49 mg/Kg 09/29/14 13:45 09/30/14 17:05 1 ☼Arsenic ND 1.25 mg/Kg 09/29/14 13:45 09/30/14 17:05 1 ☼Beryllium 1.35 1.25 mg/Kg 09/29/14 13:45 09/30/14 17:05 1☼Cadmium ND 1.25 mg/Kg 09/29/14 13:45 09/30/14 17:05 1 ☼Chromium 5.36 2.49 mg/Kg 09/29/14 13:45 09/30/14 17:05 1 ☼Copper 11.5 1.25 mg/Kg 09/29/14 13:45 09/30/14 17:05 1 ☼Lead 12.6 3.74 mg/Kg 09/29/14 13:45 09/30/14 17:05 1☼Manganese 418 2.49 mg/Kg 09/29/14 13:45 09/30/14 17:05 1 ☼Nickel 8.03 2.49 mg/Kg 09/29/14 13:45 09/30/14 17:05 1 ☼Selenium ND 1.25 mg/Kg 09/29/14 13:45 09/30/14 17:05 1 ☼Silver ND 2.49 mg/Kg 09/29/14 13:45 09/30/14 17:05 1 ☼Thallium ND 12.5 mg/Kg 09/29/14 13:45 09/30/14 17:05 1☼Zinc 67.9 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury ND 0.124 mg/Kg ☼10/01/14 08:22 10/01/14 11:02 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier General Chemistry RL RL Percent Solids 78 0.10 %09/29/14 13:04 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier TestAmerica Nashville Page 13 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-4Client Sample ID: SB-4 (1-2) Matrix: SolidDate Collected: 09/25/14 11:45 Percent Solids: 79.0Date Received: 09/26/14 09:00 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone ND 0.0621 mg/Kg ☼09/27/14 10:09 10/02/14 19:25 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Benzene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Bromobenzene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Bromochloromethane ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Bromodichloromethane ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Bromoform ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1☼Bromomethane ND * 0.0621 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼2-Butanone (MEK)ND 0.00621 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Carbon disulfide ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Carbon tetrachloride ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Chlorobenzene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Chlorodibromomethane ND 0.00621 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Chloroethane ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Chloroform ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Chloromethane ND * 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1☼2-Chlorotoluene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼4-Chlorotoluene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼cis-1,2-Dichloroethene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼cis-1,3-Dichloropropene ND 0.00621 mg/Kg 09/27/14 10:09 10/02/14 19:25 1☼1,2-Dibromo-3-Chloropropane ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼1,2-Dibromoethane (EDB)ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Dibromomethane ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼1,2-Dichlorobenzene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼1,3-Dichlorobenzene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1☼1,4-Dichlorobenzene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Dichlorodifluoromethane ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼1,1-Dichloroethane ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼1,2-Dichloroethane ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1☼1,1-Dichloroethene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼1,2-Dichloroethene, Total ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼1,2-Dichloropropane ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼1,3-Dichloropropane ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼2,2-Dichloropropane ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1☼1,1-Dichloropropene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Diisopropyl ether ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Ethylbenzene ND 0.00621 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Hexachlorobutadiene ND 0.0621 mg/Kg 09/27/14 10:09 10/02/14 19:25 1☼2-Hexanone ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Isopropylbenzene ND 0.0124 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Methylene Chloride ND 0.0621 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼4-Methyl-2-pentanone (MIBK)ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Methyl tert-butyl ether ND 0.00621 mg/Kg 09/27/14 10:09 10/02/14 19:25 1☼Naphthalene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼n-Butylbenzene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼N-Propylbenzene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼p-Isopropyltoluene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1☼sec-Butylbenzene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Styrene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼tert-Butylbenzene ND TestAmerica Nashville Page 14 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-4Client Sample ID: SB-4 (1-2) Matrix: SolidDate Collected: 09/25/14 11:45 Percent Solids: 79.0Date Received: 09/26/14 09:00 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00248 mg/Kg ☼09/27/14 10:09 10/02/14 19:25 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼1,1,2,2-Tetrachloroethane ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1☼Tetrachloroethene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Toluene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼trans-1,2-Dichloroethene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼trans-1,3-Dichloropropene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1☼1,2,3-Trichlorobenzene 0.00279 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼1,2,4-Trichlorobenzene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼1,1,1-Trichloroethane ND 0.00621 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼1,1,2-Trichloroethane ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Trichloroethene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1☼Trichlorofluoromethane ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼1,2,3-Trichloropropane ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼1,2,4-Trimethylbenzene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼1,3,5-Trimethylbenzene ND 0.00248 mg/Kg 09/27/14 10:09 10/02/14 19:25 1☼Vinyl chloride ND 0.00373 mg/Kg 09/27/14 10:09 10/02/14 19:25 1 ☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)89 70-130 09/27/14 10:09 10/02/14 19:25 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Dibromofluoromethane (Surr)109 09/27/14 10:09 10/02/14 19:25 170-130 1,2-Dichloroethane-d4 (Surr)117 09/27/14 10:09 10/02/14 19:25 170-130 Toluene-d8 (Surr)96 09/27/14 10:09 10/02/14 19:25 170-130 Method: 6010C - Metals (ICP) RL MDL Antimony ND 12.6 mg/Kg ☼09/29/14 13:45 09/30/14 17:09 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 2.52 mg/Kg 09/29/14 13:45 09/30/14 17:09 1 ☼Arsenic ND 1.26 mg/Kg 09/29/14 13:45 09/30/14 17:09 1 ☼Beryllium ND 1.26 mg/Kg 09/29/14 13:45 09/30/14 17:09 1☼Cadmium ND 1.26 mg/Kg 09/29/14 13:45 09/30/14 17:09 1 ☼Chromium 25.0 2.52 mg/Kg 09/29/14 13:45 09/30/14 17:09 1 ☼Copper 18.7 1.26 mg/Kg 09/29/14 13:45 09/30/14 17:09 1 ☼Lead 36.4 3.78 mg/Kg 09/29/14 13:45 09/30/14 17:09 1☼Manganese 636 2.52 mg/Kg 09/29/14 13:45 09/30/14 17:09 1 ☼Nickel 28.4 2.52 mg/Kg 09/29/14 13:45 09/30/14 17:09 1 ☼Selenium ND 1.26 mg/Kg 09/29/14 13:45 09/30/14 17:09 1 ☼Silver ND 2.52 mg/Kg 09/29/14 13:45 09/30/14 17:09 1 ☼Thallium ND 12.6 mg/Kg 09/29/14 13:45 09/30/14 17:09 1☼Zinc 113 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury ND 0.124 mg/Kg ☼10/01/14 08:22 10/01/14 11:04 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier General Chemistry RL RL Percent Solids 79 0.10 %09/29/14 13:04 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier TestAmerica Nashville Page 15 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-5Client Sample ID: SB-5 (1-2) Matrix: SolidDate Collected: 09/25/14 13:00 Percent Solids: 78.5Date Received: 09/26/14 09:00 Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL GRO (C6-C10)ND 6.44 mg/Kg ☼09/27/14 10:08 09/30/14 16:51 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier a,a,a-Trifluorotoluene 98 50-150 09/27/14 10:08 09/30/14 16:51 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL Diesel Range Organics [C10-C28]15.4 4.98 mg/Kg ☼09/30/14 10:14 10/01/14 20:58 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier o-Terphenyl (Surr)66 50-150 09/30/14 10:14 10/01/14 20:58 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery General Chemistry RL RL Percent Solids 79 0.10 %09/29/14 13:04 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier TestAmerica Nashville Page 16 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-6Client Sample ID: SB-6 (1-2) Matrix: SolidDate Collected: 09/25/14 12:45 Percent Solids: 78.7Date Received: 09/26/14 09:00 Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) RL MDL GRO (C6-C10)ND 6.85 mg/Kg ☼09/27/14 10:08 09/30/14 17:25 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier a,a,a-Trifluorotoluene 105 50-150 09/27/14 10:08 09/30/14 17:25 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) RL MDL Diesel Range Organics [C10-C28]166 5.00 mg/Kg ☼09/30/14 10:14 10/01/14 21:12 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier o-Terphenyl (Surr)66 50-150 09/30/14 10:14 10/01/14 21:12 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery General Chemistry RL RL Percent Solids 79 0.10 %09/29/14 13:04 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier TestAmerica Nashville Page 17 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-7Client Sample ID: TMW-1 Matrix: WaterDate Collected: 09/25/14 12:17 Date Received: 09/26/14 09:00 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone ND 25.0 ug/L 10/01/14 04:31 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 1.00 ug/L 10/01/14 04:31 1BenzeneND 1.00 ug/L 10/01/14 04:31 1BromobenzeneND 1.00 ug/L 10/01/14 04:31 1BromochloromethaneND 1.00 ug/L 10/01/14 04:31 1BromodichloromethaneND 1.00 ug/L 10/01/14 04:31 1BromoformND 1.00 ug/L 10/01/14 04:31 1BromomethaneND 50.0 ug/L 10/01/14 04:31 12-Butanone (MEK)ND 1.00 ug/L 10/01/14 04:31 1Carbon disulfide ND 1.00 ug/L 10/01/14 04:31 1Carbon tetrachloride ND 1.00 ug/L 10/01/14 04:31 1ChlorobenzeneND 1.00 ug/L 10/01/14 04:31 1ChlorodibromomethaneND 1.00 ug/L 10/01/14 04:31 1ChloroethaneND 1.00 ug/L 10/01/14 04:31 1ChloroformND 1.00 ug/L 10/01/14 04:31 1ChloromethaneND 1.00 ug/L 10/01/14 04:31 12-Chlorotoluene ND 1.00 ug/L 10/01/14 04:31 14-Chlorotoluene ND 1.00 ug/L 10/01/14 04:31 1cis-1,2-Dichloroethene ND 1.00 ug/L 10/01/14 04:31 1cis-1,3-Dichloropropene ND 10.0 ug/L 10/01/14 04:31 11,2-Dibromo-3-Chloropropane ND 1.00 ug/L 10/01/14 04:31 11,2-Dibromoethane (EDB)ND 1.00 ug/L 10/01/14 04:31 1DibromomethaneND 1.00 ug/L 10/01/14 04:31 11,2-Dichlorobenzene ND 1.00 ug/L 10/01/14 04:31 11,3-Dichlorobenzene ND 1.00 ug/L 10/01/14 04:31 11,4-Dichlorobenzene ND 1.00 ug/L 10/01/14 04:31 1DichlorodifluoromethaneND 1.00 ug/L 10/01/14 04:31 11,1-Dichloroethane ND 1.00 ug/L 10/01/14 04:31 11,2-Dichloroethane ND 1.00 ug/L 10/01/14 04:31 11,1-Dichloroethene ND 1.00 ug/L 10/01/14 04:31 11,2-Dichloroethene, Total ND 1.00 ug/L 10/01/14 04:31 11,2-Dichloropropane ND 1.00 ug/L 10/01/14 04:31 11,3-Dichloropropane ND 1.00 ug/L 10/01/14 04:31 12,2-Dichloropropane ND 1.00 ug/L 10/01/14 04:31 11,1-Dichloropropene ND 2.00 ug/L 10/01/14 04:31 1Diisopropyl ether ND 1.00 ug/L 10/01/14 04:31 1EthylbenzeneND 2.00 ug/L 10/01/14 04:31 1HexachlorobutadieneND 10.0 ug/L 10/01/14 04:31 12-Hexanone ND 50.0 ug/L 10/01/14 04:31 1Isopropyl alcohol ND 1.00 ug/L 10/01/14 04:31 1IsopropylbenzeneND 5.00 ug/L 10/01/14 04:31 1Methylene Chloride ND 10.0 ug/L 10/01/14 04:31 14-Methyl-2-pentanone (MIBK)ND 1.00 ug/L 10/01/14 04:31 1Methyl tert-butyl ether ND 5.00 ug/L 10/01/14 04:31 1NaphthaleneND 1.00 ug/L 10/01/14 04:31 1n-Butylbenzene ND 1.00 ug/L 10/01/14 04:31 1N-Propylbenzene ND 1.00 ug/L 10/01/14 04:31 1p-Isopropyltoluene ND 1.00 ug/L 10/01/14 04:31 1sec-Butylbenzene ND 1.00 ug/L 10/01/14 04:31 1StyreneND TestAmerica Nashville Page 18 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-7Client Sample ID: TMW-1 Matrix: WaterDate Collected: 09/25/14 12:17 Date Received: 09/26/14 09:00 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL tert-Butylbenzene ND 1.00 ug/L 10/01/14 04:31 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 1.00 ug/L 10/01/14 04:31 11,1,1,2-Tetrachloroethane ND 1.00 ug/L 10/01/14 04:31 11,1,2,2-Tetrachloroethane ND 1.00 ug/L 10/01/14 04:31 1TetrachloroetheneND 1.00 ug/L 10/01/14 04:31 1TolueneND 1.00 ug/L 10/01/14 04:31 1trans-1,2-Dichloroethene ND 1.00 ug/L 10/01/14 04:31 1trans-1,3-Dichloropropene ND 1.00 ug/L 10/01/14 04:31 11,2,3-Trichlorobenzene ND 1.00 ug/L 10/01/14 04:31 11,2,4-Trichlorobenzene ND 1.00 ug/L 10/01/14 04:31 11,1,1-Trichloroethane ND 1.00 ug/L 10/01/14 04:31 11,1,2-Trichloroethane ND 1.00 ug/L 10/01/14 04:31 1TrichloroetheneND 1.00 ug/L 10/01/14 04:31 1TrichlorofluoromethaneND 1.00 ug/L 10/01/14 04:31 11,2,3-Trichloropropane ND 1.00 ug/L 10/01/14 04:31 11,2,4-Trimethylbenzene ND 1.00 ug/L 10/01/14 04:31 11,3,5-Trimethylbenzene ND 1.00 ug/L 10/01/14 04:31 1Vinyl chloride ND 2.00 ug/L 10/01/14 04:31 1Xylenes, Total ND 4-Bromofluorobenzene (Surr)103 70-130 10/01/14 04:31 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Dibromofluoromethane (Surr)97 10/01/14 04:31 170-130 1,2-Dichloroethane-d4 (Surr)81 10/01/14 04:31 170-130 Toluene-d8 (Surr)107 10/01/14 04:31 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene 9.50 1.82 ug/L 10/01/14 11:28 10/01/14 21:35 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 1.82 ug/L 10/01/14 11:28 10/01/14 21:35 1AcenaphthyleneND 1.82 ug/L 10/01/14 11:28 10/01/14 21:35 1AnthraceneND 1.82 ug/L 10/01/14 11:28 10/01/14 21:35 1Benzo[a]anthracene ND 1.82 ug/L 10/01/14 11:28 10/01/14 21:35 1Benzo[a]pyrene ND 1.82 ug/L 10/01/14 11:28 10/01/14 21:35 1Benzo[b]fluoranthene ND 1.82 ug/L 10/01/14 11:28 10/01/14 21:35 1Benzo[g,h,i]perylene ND 1.82 ug/L 10/01/14 11:28 10/01/14 21:35 1Benzo[k]fluoranthene ND 1.82 ug/L 10/01/14 11:28 10/01/14 21:35 1ChryseneND 1.82 ug/L 10/01/14 11:28 10/01/14 21:35 1Dibenz(a,h)anthracene ND 1.82 ug/L 10/01/14 11:28 10/01/14 21:35 1FluorantheneND 1.82 ug/L 10/01/14 11:28 10/01/14 21:35 1Fluorene2.53 1.82 ug/L 10/01/14 11:28 10/01/14 21:35 1Indeno[1,2,3-cd]pyrene ND 1.82 ug/L 10/01/14 11:28 10/01/14 21:35 1Naphthalene11.4 1.82 ug/L 10/01/14 11:28 10/01/14 21:35 1PhenanthreneND 1.82 ug/L 10/01/14 11:28 10/01/14 21:35 1PyreneND 2-Fluorobiphenyl (Surr)68 29-120 10/01/14 11:28 10/01/14 21:35 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Nitrobenzene-d5 (Surr)77 10/01/14 11:28 10/01/14 21:35 127-120 Terphenyl-d14 (Surr)74 10/01/14 11:28 10/01/14 21:35 113-120 TestAmerica Nashville Page 19 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-7Client Sample ID: TMW-1 Matrix: WaterDate Collected: 09/25/14 12:17 Date Received: 09/26/14 09:00 Method: 6010C - Metals (ICP) RL MDL Antimony ND 0.0100 mg/L 09/30/14 10:07 10/02/14 17:34 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 0.0100 mg/L 09/30/14 10:07 10/02/14 17:34 1ArsenicND 0.00400 mg/L 09/30/14 10:07 10/02/14 17:34 1BerylliumND 0.00100 mg/L 09/30/14 10:07 10/02/14 17:34 1CadmiumND 0.00500 mg/L 09/30/14 10:07 10/02/14 17:34 1ChromiumND 0.0100 mg/L 09/30/14 10:07 10/02/14 17:34 1CopperND 0.00500 mg/L 09/30/14 10:07 10/03/14 16:55 1LeadND 0.0150 mg/L 09/30/14 10:07 10/02/14 17:34 1Manganese0.591 ^ 0.0100 mg/L 09/30/14 10:07 10/02/14 17:34 1NickelND 0.0100 mg/L 09/30/14 10:07 10/02/14 17:34 1SeleniumND 0.00500 mg/L 09/30/14 10:07 10/02/14 17:34 1SilverND 0.0100 mg/L 09/30/14 10:07 10/02/14 17:34 1ThalliumND 0.0500 mg/L 09/30/14 10:07 10/02/14 17:34 1ZincND Method: 7470A - Mercury (CVAA) RL MDL Mercury ND 0.000200 mg/L 10/01/14 06:48 10/01/14 14:33 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier TestAmerica Nashville Page 20 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-8Client Sample ID: TMW-2 Matrix: WaterDate Collected: 09/25/14 14:01 Date Received: 09/26/14 09:00 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone ND 25.0 ug/L 10/01/14 04:05 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 1.00 ug/L 10/01/14 04:05 1BenzeneND 1.00 ug/L 10/01/14 04:05 1BromobenzeneND 1.00 ug/L 10/01/14 04:05 1BromochloromethaneND 1.00 ug/L 10/01/14 04:05 1BromodichloromethaneND 1.00 ug/L 10/01/14 04:05 1BromoformND 1.00 ug/L 10/01/14 04:05 1BromomethaneND 50.0 ug/L 10/01/14 04:05 12-Butanone (MEK)ND 1.00 ug/L 10/01/14 04:05 1Carbon disulfide ND 1.00 ug/L 10/01/14 04:05 1Carbon tetrachloride ND 1.00 ug/L 10/01/14 04:05 1ChlorobenzeneND 1.00 ug/L 10/01/14 04:05 1ChlorodibromomethaneND 1.00 ug/L 10/01/14 04:05 1ChloroethaneND 1.00 ug/L 10/01/14 04:05 1ChloroformND 1.00 ug/L 10/01/14 04:05 1ChloromethaneND 1.00 ug/L 10/01/14 04:05 12-Chlorotoluene ND 1.00 ug/L 10/01/14 04:05 14-Chlorotoluene ND 1.00 ug/L 10/01/14 04:05 1cis-1,2-Dichloroethene ND 1.00 ug/L 10/01/14 04:05 1cis-1,3-Dichloropropene ND 10.0 ug/L 10/01/14 04:05 11,2-Dibromo-3-Chloropropane ND 1.00 ug/L 10/01/14 04:05 11,2-Dibromoethane (EDB)ND 1.00 ug/L 10/01/14 04:05 1DibromomethaneND 1.00 ug/L 10/01/14 04:05 11,2-Dichlorobenzene ND 1.00 ug/L 10/01/14 04:05 11,3-Dichlorobenzene ND 1.00 ug/L 10/01/14 04:05 11,4-Dichlorobenzene ND 1.00 ug/L 10/01/14 04:05 1DichlorodifluoromethaneND 1.00 ug/L 10/01/14 04:05 11,1-Dichloroethane ND 1.00 ug/L 10/01/14 04:05 11,2-Dichloroethane ND 1.00 ug/L 10/01/14 04:05 11,1-Dichloroethene ND 1.00 ug/L 10/01/14 04:05 11,2-Dichloroethene, Total ND 1.00 ug/L 10/01/14 04:05 11,2-Dichloropropane ND 1.00 ug/L 10/01/14 04:05 11,3-Dichloropropane ND 1.00 ug/L 10/01/14 04:05 12,2-Dichloropropane ND 1.00 ug/L 10/01/14 04:05 11,1-Dichloropropene ND 2.00 ug/L 10/01/14 04:05 1Diisopropyl ether ND 1.00 ug/L 10/01/14 04:05 1Ethylbenzene1.10 2.00 ug/L 10/01/14 04:05 1HexachlorobutadieneND 10.0 ug/L 10/01/14 04:05 12-Hexanone ND 50.0 ug/L 10/01/14 04:05 1Isopropyl alcohol ND 1.00 ug/L 10/01/14 04:05 1IsopropylbenzeneND 5.00 ug/L 10/01/14 04:05 1Methylene Chloride ND 10.0 ug/L 10/01/14 04:05 14-Methyl-2-pentanone (MIBK)ND 1.00 ug/L 10/01/14 04:05 1Methyl tert-butyl ether ND 5.00 ug/L 10/01/14 04:05 1NaphthaleneND 1.00 ug/L 10/01/14 04:05 1n-Butylbenzene ND 1.00 ug/L 10/01/14 04:05 1N-Propylbenzene ND 1.00 ug/L 10/01/14 04:05 1p-Isopropyltoluene ND 1.00 ug/L 10/01/14 04:05 1sec-Butylbenzene ND 1.00 ug/L 10/01/14 04:05 1StyreneND TestAmerica Nashville Page 21 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-8Client Sample ID: TMW-2 Matrix: WaterDate Collected: 09/25/14 14:01 Date Received: 09/26/14 09:00 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL tert-Butylbenzene ND 1.00 ug/L 10/01/14 04:05 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 1.00 ug/L 10/01/14 04:05 11,1,1,2-Tetrachloroethane ND 1.00 ug/L 10/01/14 04:05 11,1,2,2-Tetrachloroethane ND 1.00 ug/L 10/01/14 04:05 1TetrachloroetheneND 1.00 ug/L 10/01/14 04:05 1TolueneND 1.00 ug/L 10/01/14 04:05 1trans-1,2-Dichloroethene ND 1.00 ug/L 10/01/14 04:05 1trans-1,3-Dichloropropene ND 1.00 ug/L 10/01/14 04:05 11,2,3-Trichlorobenzene ND 1.00 ug/L 10/01/14 04:05 11,2,4-Trichlorobenzene ND 1.00 ug/L 10/01/14 04:05 11,1,1-Trichloroethane ND 1.00 ug/L 10/01/14 04:05 11,1,2-Trichloroethane ND 1.00 ug/L 10/01/14 04:05 1TrichloroetheneND 1.00 ug/L 10/01/14 04:05 1TrichlorofluoromethaneND 1.00 ug/L 10/01/14 04:05 11,2,3-Trichloropropane ND 1.00 ug/L 10/01/14 04:05 11,2,4-Trimethylbenzene ND 1.00 ug/L 10/01/14 04:05 11,3,5-Trimethylbenzene ND 1.00 ug/L 10/01/14 04:05 1Vinyl chloride ND 2.00 ug/L 10/01/14 04:05 1Xylenes, Total ND 4-Bromofluorobenzene (Surr)104 70-130 10/01/14 04:05 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Dibromofluoromethane (Surr)95 10/01/14 04:05 170-130 1,2-Dichloroethane-d4 (Surr)80 10/01/14 04:05 170-130 Toluene-d8 (Surr)106 10/01/14 04:05 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene 8.03 1.82 ug/L 10/01/14 11:28 10/01/14 21:12 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 1.82 ug/L 10/01/14 11:28 10/01/14 21:12 1AcenaphthyleneND 1.82 ug/L 10/01/14 11:28 10/01/14 21:12 1AnthraceneND 1.82 ug/L 10/01/14 11:28 10/01/14 21:12 1Benzo[a]anthracene ND 1.82 ug/L 10/01/14 11:28 10/01/14 21:12 1Benzo[a]pyrene ND 1.82 ug/L 10/01/14 11:28 10/01/14 21:12 1Benzo[b]fluoranthene ND 1.82 ug/L 10/01/14 11:28 10/01/14 21:12 1Benzo[g,h,i]perylene ND 1.82 ug/L 10/01/14 11:28 10/01/14 21:12 1Benzo[k]fluoranthene ND 1.82 ug/L 10/01/14 11:28 10/01/14 21:12 1ChryseneND 1.82 ug/L 10/01/14 11:28 10/01/14 21:12 1Dibenz(a,h)anthracene ND 1.82 ug/L 10/01/14 11:28 10/01/14 21:12 1FluorantheneND 1.82 ug/L 10/01/14 11:28 10/01/14 21:12 1Fluorene2.58 1.82 ug/L 10/01/14 11:28 10/01/14 21:12 1Indeno[1,2,3-cd]pyrene ND 1.82 ug/L 10/01/14 11:28 10/01/14 21:12 1Naphthalene30.0 1.82 ug/L 10/01/14 11:28 10/01/14 21:12 1Phenanthrene2.60 1.82 ug/L 10/01/14 11:28 10/01/14 21:12 1PyreneND 2-Fluorobiphenyl (Surr)65 29-120 10/01/14 11:28 10/01/14 21:12 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Nitrobenzene-d5 (Surr)72 10/01/14 11:28 10/01/14 21:12 127-120 Terphenyl-d14 (Surr)73 10/01/14 11:28 10/01/14 21:12 113-120 TestAmerica Nashville Page 22 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-8Client Sample ID: TMW-2 Matrix: WaterDate Collected: 09/25/14 14:01 Date Received: 09/26/14 09:00 Method: 6010C - Metals (ICP) RL MDL Antimony ND 0.0100 mg/L 09/30/14 10:07 10/02/14 17:49 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 0.0100 mg/L 09/30/14 10:07 10/02/14 17:49 1ArsenicND 0.00400 mg/L 09/30/14 10:07 10/02/14 17:49 1BerylliumND 0.00100 mg/L 09/30/14 10:07 10/02/14 17:49 1CadmiumND 0.00500 mg/L 09/30/14 10:07 10/02/14 17:49 1Chromium0.00980 0.0100 mg/L 09/30/14 10:07 10/02/14 17:49 1CopperND 0.00500 mg/L 09/30/14 10:07 10/03/14 16:58 1Lead0.0261 0.0150 mg/L 09/30/14 10:07 10/02/14 17:49 1Manganese7.15 ^ 0.0100 mg/L 09/30/14 10:07 10/02/14 17:49 1NickelND 0.0100 mg/L 09/30/14 10:07 10/02/14 17:49 1SeleniumND 0.00500 mg/L 09/30/14 10:07 10/02/14 17:49 1SilverND 0.0100 mg/L 09/30/14 10:07 10/02/14 17:49 1ThalliumND 0.0500 mg/L 09/30/14 10:07 10/02/14 17:49 1ZincND Method: 7470A - Mercury (CVAA) RL MDL Mercury ND 0.000200 mg/L 10/01/14 06:48 10/01/14 14:35 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier TestAmerica Nashville Page 23 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Lab Sample ID: 490-62390-9Client Sample ID: Background (1-2) Matrix: SolidDate Collected: 09/25/14 13:37 Percent Solids: 65.9Date Received: 09/26/14 09:00 Method: 6010C - Metals (ICP) RL MDL Antimony ND 14.7 mg/Kg ☼09/29/14 13:45 09/30/14 17:24 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 2.94 mg/Kg 09/29/14 13:45 09/30/14 17:24 1 ☼Arsenic 3.38 1.47 mg/Kg 09/29/14 13:45 09/30/14 17:24 1 ☼Beryllium ND 1.47 mg/Kg 09/29/14 13:45 09/30/14 17:24 1 ☼Cadmium ND 1.47 mg/Kg 09/29/14 13:45 09/30/14 17:24 1 ☼Chromium 12.0 2.94 mg/Kg 09/29/14 13:45 09/30/14 17:24 1 ☼Copper 17.3 1.47 mg/Kg 09/29/14 13:45 09/30/14 17:24 1☼Lead 23.9 4.41 mg/Kg 09/29/14 13:45 09/30/14 17:24 1 ☼Manganese 102 2.94 mg/Kg 09/29/14 13:45 09/30/14 17:24 1 ☼Nickel 10.4 2.94 mg/Kg 09/29/14 13:45 09/30/14 17:24 1 ☼Selenium ND 1.47 mg/Kg 09/29/14 13:45 09/30/14 17:24 1 ☼Silver 1.68 2.94 mg/Kg 09/29/14 13:45 09/30/14 17:24 1 ☼Thallium ND 14.7 mg/Kg 09/29/14 13:45 09/30/14 17:24 1 ☼Zinc 83.7 Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) RL MDL Mercury ND 0.152 mg/Kg ☼10/01/14 14:28 10/02/14 12:19 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier General Chemistry RL RL Percent Solids 66 0.10 %09/29/14 13:04 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier TestAmerica Nashville Page 24 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 490-194305/8 Matrix: Water Prep Type: Total/NA Analysis Batch: 194305 RL MDL Acetone ND 25.0 ug/L 09/30/14 22:31 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 1.00 ug/L 09/30/14 22:31 1Benzene ND 1.00 ug/L 09/30/14 22:31 1Bromobenzene ND 1.00 ug/L 09/30/14 22:31 1Bromochloromethane ND 1.00 ug/L 09/30/14 22:31 1Bromodichloromethane ND 1.00 ug/L 09/30/14 22:31 1Bromoform ND 1.00 ug/L 09/30/14 22:31 1Bromomethane ND 50.0 ug/L 09/30/14 22:31 12-Butanone (MEK) ND 1.00 ug/L 09/30/14 22:31 1Carbon disulfide ND 1.00 ug/L 09/30/14 22:31 1Carbon tetrachloride ND 1.00 ug/L 09/30/14 22:31 1Chlorobenzene ND 1.00 ug/L 09/30/14 22:31 1Chlorodibromomethane ND 1.00 ug/L 09/30/14 22:31 1Chloroethane ND 1.00 ug/L 09/30/14 22:31 1Chloroform ND 1.00 ug/L 09/30/14 22:31 1Chloromethane ND 1.00 ug/L 09/30/14 22:31 12-Chlorotoluene ND 1.00 ug/L 09/30/14 22:31 14-Chlorotoluene ND 1.00 ug/L 09/30/14 22:31 1cis-1,2-Dichloroethene ND 1.00 ug/L 09/30/14 22:31 1cis-1,3-Dichloropropene ND 10.0 ug/L 09/30/14 22:31 11,2-Dibromo-3-Chloropropane ND 1.00 ug/L 09/30/14 22:31 11,2-Dibromoethane (EDB) ND 1.00 ug/L 09/30/14 22:31 1Dibromomethane ND 1.00 ug/L 09/30/14 22:31 11,2-Dichlorobenzene ND 1.00 ug/L 09/30/14 22:31 11,3-Dichlorobenzene ND 1.00 ug/L 09/30/14 22:31 11,4-Dichlorobenzene ND 1.00 ug/L 09/30/14 22:31 1Dichlorodifluoromethane ND 1.00 ug/L 09/30/14 22:31 11,1-Dichloroethane ND 1.00 ug/L 09/30/14 22:31 11,2-Dichloroethane ND 1.00 ug/L 09/30/14 22:31 11,1-Dichloroethene ND 1.00 ug/L 09/30/14 22:31 11,2-Dichloroethene, Total ND 1.00 ug/L 09/30/14 22:31 11,2-Dichloropropane ND 1.00 ug/L 09/30/14 22:31 11,3-Dichloropropane ND 1.00 ug/L 09/30/14 22:31 12,2-Dichloropropane ND 1.00 ug/L 09/30/14 22:31 11,1-Dichloropropene ND 2.00 ug/L 09/30/14 22:31 1Diisopropyl ether ND 1.00 ug/L 09/30/14 22:31 1Ethylbenzene ND 2.00 ug/L 09/30/14 22:31 1Hexachlorobutadiene ND 10.0 ug/L 09/30/14 22:31 12-Hexanone ND 50.0 ug/L 09/30/14 22:31 1Isopropyl alcohol ND 1.00 ug/L 09/30/14 22:31 1Isopropylbenzene ND 5.00 ug/L 09/30/14 22:31 1Methylene Chloride ND 10.0 ug/L 09/30/14 22:31 14-Methyl-2-pentanone (MIBK) ND 1.00 ug/L 09/30/14 22:31 1Methyl tert-butyl ether ND 5.00 ug/L 09/30/14 22:31 1Naphthalene ND 1.00 ug/L 09/30/14 22:31 1n-Butylbenzene ND 1.00 ug/L 09/30/14 22:31 1N-Propylbenzene ND 1.00 ug/L 09/30/14 22:31 1p-Isopropyltoluene ND 1.00 ug/L 09/30/14 22:31 1sec-Butylbenzene TestAmerica Nashville Page 25 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-194305/8 Matrix: Water Prep Type: Total/NA Analysis Batch: 194305 RL MDL Styrene ND 1.00 ug/L 09/30/14 22:31 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 1.00 ug/L 09/30/14 22:31 1tert-Butylbenzene ND 1.00 ug/L 09/30/14 22:31 11,1,1,2-Tetrachloroethane ND 1.00 ug/L 09/30/14 22:31 11,1,2,2-Tetrachloroethane ND 1.00 ug/L 09/30/14 22:31 1Tetrachloroethene ND 1.00 ug/L 09/30/14 22:31 1Toluene ND 1.00 ug/L 09/30/14 22:31 1trans-1,2-Dichloroethene ND 1.00 ug/L 09/30/14 22:31 1trans-1,3-Dichloropropene ND 1.00 ug/L 09/30/14 22:31 11,2,3-Trichlorobenzene ND 1.00 ug/L 09/30/14 22:31 11,2,4-Trichlorobenzene ND 1.00 ug/L 09/30/14 22:31 11,1,1-Trichloroethane ND 1.00 ug/L 09/30/14 22:31 11,1,2-Trichloroethane ND 1.00 ug/L 09/30/14 22:31 1Trichloroethene ND 1.00 ug/L 09/30/14 22:31 1Trichlorofluoromethane ND 1.00 ug/L 09/30/14 22:31 11,2,3-Trichloropropane ND 1.00 ug/L 09/30/14 22:31 11,2,4-Trimethylbenzene ND 1.00 ug/L 09/30/14 22:31 11,3,5-Trimethylbenzene ND 1.00 ug/L 09/30/14 22:31 1Vinyl chloride ND 2.00 ug/L 09/30/14 22:31 1Xylenes, Total 4-Bromofluorobenzene (Surr)103 70-130 09/30/14 22:31 1 MB MB Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery 95 09/30/14 22:31 1Dibromofluoromethane (Surr)70-130 78 09/30/14 22:31 11,2-Dichloroethane-d4 (Surr)70-130 106 09/30/14 22:31 1Toluene-d8 (Surr)70-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194305/3 Matrix: Water Prep Type: Total/NA Analysis Batch: 194305 Acetone 250 244.6 ug/L 98 54 -145 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Benzene 50.0 51.69 ug/L 103 80 -121 Bromobenzene 50.0 52.37 ug/L 105 68 -130 Bromochloromethane 50.0 53.27 ug/L 107 78 -129 Bromodichloromethane 50.0 48.93 ug/L 98 75 -129 Bromoform 50.0 48.77 ug/L 98 46 -145 Bromomethane 50.0 66.06 ug/L 132 41 -150 2-Butanone (MEK)250 240.3 ug/L 96 62 -133 Carbon disulfide 50.0 50.87 ug/L 102 77 -126 Carbon tetrachloride 50.0 50.43 ug/L 101 64 -147 Chlorobenzene 50.0 51.40 ug/L 103 80 -120 Chlorodibromomethane 50.0 54.24 ug/L 108 69 -133 Chloroethane 50.0 50.60 ug/L 101 72 -120 Chloroform 50.0 48.27 ug/L 97 73 -129 Chloromethane 50.0 43.37 ug/L 87 12 -150 2-Chlorotoluene 50.0 51.71 ug/L 103 75 -126 4-Chlorotoluene 50.0 52.41 ug/L 105 75 -130 TestAmerica Nashville Page 26 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194305/3 Matrix: Water Prep Type: Total/NA Analysis Batch: 194305 cis-1,2-Dichloroethene 50.0 50.11 ug/L 100 76 -125 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits cis-1,3-Dichloropropene 50.0 61.79 ug/L 124 74 -140 1,2-Dibromo-3-Chloropropane 50.0 59.25 ug/L 119 54 -125 1,2-Dibromoethane (EDB)50.0 54.59 ug/L 109 80 -129 Dibromomethane 50.0 48.26 ug/L 97 71 -125 1,2-Dichlorobenzene 50.0 52.49 ug/L 105 80 -121 1,3-Dichlorobenzene 50.0 53.00 ug/L 106 80 -122 1,4-Dichlorobenzene 50.0 53.28 ug/L 107 80 -120 Dichlorodifluoromethane 50.0 48.86 ug/L 98 37 -127 1,1-Dichloroethane 50.0 50.55 ug/L 101 78 -125 1,2-Dichloroethane 50.0 43.14 ug/L 86 77 -121 1,1-Dichloroethene 50.0 50.91 ug/L 102 79 -124 1,2-Dichloroethene, Total 100 101.4 ug/L 101 78 -126 1,2-Dichloropropane 50.0 52.24 ug/L 104 75 -120 1,3-Dichloropropane 50.0 52.43 ug/L 105 80 -125 2,2-Dichloropropane 50.0 51.62 ug/L 103 43 -161 1,1-Dichloropropene 50.0 50.37 ug/L 101 80 -122 Diisopropyl ether 50.0 50.70 ug/L 101 61 -142 Ethylbenzene 50.0 49.37 ug/L 99 80 -130 Hexachlorobutadiene 50.0 51.56 ug/L 103 49 -146 2-Hexanone 250 250.3 ug/L 100 60 -142 Isopropyl alcohol 500 351.4 ug/L 70 65 -150 Isopropylbenzene 50.0 48.78 ug/L 98 80 -141 Methylene Chloride 50.0 48.63 ug/L 97 79 -123 4-Methyl-2-pentanone (MIBK)250 255.0 ug/L 102 60 -137 Methyl tert-butyl ether 50.0 48.36 ug/L 97 72 -133 Naphthalene 50.0 55.29 ug/L 111 62 -138 n-Butylbenzene 50.0 50.58 ug/L 101 68 -132 N-Propylbenzene 50.0 53.08 ug/L 106 75 -129 p-Isopropyltoluene 50.0 52.41 ug/L 105 75 -128 sec-Butylbenzene 50.0 51.64 ug/L 103 76 -128 Styrene 50.0 51.07 ug/L 102 80 -127 tert-Butylbenzene 50.0 51.54 ug/L 103 76 -126 1,1,1,2-Tetrachloroethane 50.0 53.39 ug/L 107 74 -135 1,1,2,2-Tetrachloroethane 50.0 54.64 ug/L 109 69 -131 Tetrachloroethene 50.0 52.76 ug/L 106 80 -126 Toluene 50.0 51.54 ug/L 103 80 -126 trans-1,2-Dichloroethene 50.0 51.30 ug/L 103 79 -126 trans-1,3-Dichloropropene 50.0 60.22 ug/L 120 63 -134 1,2,3-Trichlorobenzene 50.0 57.13 ug/L 114 62 -133 1,2,4-Trichlorobenzene 50.0 53.98 ug/L 108 63 -133 1,1,1-Trichloroethane 50.0 46.91 ug/L 94 78 -135 1,1,2-Trichloroethane 50.0 53.07 ug/L 106 80 -124 Trichloroethene 50.0 52.11 ug/L 104 80 -123 Trichlorofluoromethane 50.0 45.39 ug/L 91 65 -124 1,2,3-Trichloropropane 50.0 60.12 ug/L 120 70 -131 1,2,4-Trimethylbenzene 50.0 51.44 ug/L 103 77 -126 1,3,5-Trimethylbenzene 50.0 52.76 ug/L 106 77 -127 TestAmerica Nashville Page 27 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194305/3 Matrix: Water Prep Type: Total/NA Analysis Batch: 194305 Vinyl chloride 50.0 52.51 ug/L 105 68 -120 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Xylenes, Total 100 98.52 ug/L 99 80 -132 4-Bromofluorobenzene (Surr)70 -130 Surrogate 101 LCS LCS Qualifier Limits%Recovery 95Dibromofluoromethane (Surr)70 -130 801,2-Dichloroethane-d4 (Surr)70 -130 104Toluene-d8 (Surr)70 -130 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-194305/4 Matrix: Water Prep Type: Total/NA Analysis Batch: 194305 Acetone 250 242.1 ug/L 97 54 -145 1 21 Analyte LCSD LCSD DUnitResult Qualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Benzene 50.0 52.06 ug/L 104 80 -121 1 17 Bromobenzene 50.0 50.99 ug/L 102 68 -130 3 20 Bromochloromethane 50.0 52.71 ug/L 105 78 -129 1 17 Bromodichloromethane 50.0 49.00 ug/L 98 75 -129 0 18 Bromoform 50.0 48.33 ug/L 97 46 -145 1 16 Bromomethane 50.0 65.87 ug/L 132 41 -150 0 50 2-Butanone (MEK)250 238.2 ug/L 95 62 -133 1 19 Carbon disulfide 50.0 51.08 ug/L 102 77 -126 0 21 Carbon tetrachloride 50.0 50.60 ug/L 101 64 -147 0 19 Chlorobenzene 50.0 51.54 ug/L 103 80 -120 0 14 Chlorodibromomethane 50.0 54.04 ug/L 108 69 -133 0 15 Chloroethane 50.0 53.38 ug/L 107 72 -120 5 20 Chloroform 50.0 48.99 ug/L 98 73 -129 1 18 Chloromethane 50.0 44.11 ug/L 88 12 -150 2 31 2-Chlorotoluene 50.0 51.26 ug/L 103 75 -126 1 17 4-Chlorotoluene 50.0 51.92 ug/L 104 75 -130 1 18 cis-1,2-Dichloroethene 50.0 50.30 ug/L 101 76 -125 0 17 cis-1,3-Dichloropropene 50.0 62.14 ug/L 124 74 -140 1 15 1,2-Dibromo-3-Chloropropane 50.0 57.88 ug/L 116 54 -125 2 24 1,2-Dibromoethane (EDB)50.0 54.58 ug/L 109 80 -129 0 15 Dibromomethane 50.0 47.55 ug/L 95 71 -125 1 16 1,2-Dichlorobenzene 50.0 51.89 ug/L 104 80 -121 1 15 1,3-Dichlorobenzene 50.0 52.68 ug/L 105 80 -122 1 15 1,4-Dichlorobenzene 50.0 53.48 ug/L 107 80 -120 0 15 Dichlorodifluoromethane 50.0 49.27 ug/L 99 37 -127 1 18 1,1-Dichloroethane 50.0 50.74 ug/L 101 78 -125 0 17 1,2-Dichloroethane 50.0 43.47 ug/L 87 77 -121 1 17 1,1-Dichloroethene 50.0 51.50 ug/L 103 79 -124 1 17 1,2-Dichloroethene, Total 100 102.1 ug/L 102 78 -126 1 33 1,2-Dichloropropane 50.0 52.22 ug/L 104 75 -120 0 17 1,3-Dichloropropane 50.0 52.36 ug/L 105 80 -125 0 14 2,2-Dichloropropane 50.0 51.95 ug/L 104 43 -161 1 18 1,1-Dichloropropene 50.0 50.81 ug/L 102 80 -122 1 17 TestAmerica Nashville Page 28 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-194305/4 Matrix: Water Prep Type: Total/NA Analysis Batch: 194305 Diisopropyl ether 50.0 51.11 ug/L 102 61 -142 1 50 Analyte LCSD LCSD DUnitResult Qualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Ethylbenzene 50.0 49.30 ug/L 99 80 -130 0 15 Hexachlorobutadiene 50.0 52.06 ug/L 104 49 -146 1 23 2-Hexanone 250 255.3 ug/L 102 60 -142 2 15 Isopropyl alcohol 500 368.9 ug/L 74 65 -150 5 30 Isopropylbenzene 50.0 48.86 ug/L 98 80 -141 0 16 Methylene Chloride 50.0 48.83 ug/L 98 79 -123 0 17 4-Methyl-2-pentanone (MIBK)250 254.0 ug/L 102 60 -137 0 17 Methyl tert-butyl ether 50.0 48.64 ug/L 97 72 -133 1 16 Naphthalene 50.0 56.40 ug/L 113 62 -138 2 26 n-Butylbenzene 50.0 50.48 ug/L 101 68 -132 0 18 N-Propylbenzene 50.0 52.65 ug/L 105 75 -129 1 17 p-Isopropyltoluene 50.0 51.95 ug/L 104 75 -128 1 16 sec-Butylbenzene 50.0 51.41 ug/L 103 76 -128 0 16 Styrene 50.0 51.36 ug/L 103 80 -127 1 24 tert-Butylbenzene 50.0 51.83 ug/L 104 76 -126 1 16 1,1,1,2-Tetrachloroethane 50.0 53.32 ug/L 107 74 -135 0 16 1,1,2,2-Tetrachloroethane 50.0 53.45 ug/L 107 69 -131 2 20 Tetrachloroethene 50.0 53.18 ug/L 106 80 -126 1 16 Toluene 50.0 51.81 ug/L 104 80 -126 1 15 trans-1,2-Dichloroethene 50.0 51.78 ug/L 104 79 -126 1 16 trans-1,3-Dichloropropene 50.0 60.25 ug/L 120 63 -134 0 14 1,2,3-Trichlorobenzene 50.0 57.29 ug/L 115 62 -133 0 25 1,2,4-Trichlorobenzene 50.0 53.65 ug/L 107 63 -133 1 19 1,1,1-Trichloroethane 50.0 47.46 ug/L 95 78 -135 1 17 1,1,2-Trichloroethane 50.0 53.09 ug/L 106 80 -124 0 15 Trichloroethene 50.0 52.31 ug/L 105 80 -123 0 17 Trichlorofluoromethane 50.0 46.23 ug/L 92 65 -124 2 18 1,2,3-Trichloropropane 50.0 59.72 ug/L 119 70 -131 1 19 1,2,4-Trimethylbenzene 50.0 51.93 ug/L 104 77 -126 1 16 1,3,5-Trimethylbenzene 50.0 52.16 ug/L 104 77 -127 1 17 Vinyl chloride 50.0 53.26 ug/L 107 68 -120 1 17 Xylenes, Total 100 98.94 ug/L 99 80 -132 0 15 4-Bromofluorobenzene (Surr)70 -130 Surrogate 101 LCSD LCSD Qualifier Limits%Recovery 96Dibromofluoromethane (Surr)70 -130 821,2-Dichloroethane-d4 (Surr)70 -130 105Toluene-d8 (Surr)70 -130 Client Sample ID: Matrix SpikeLab Sample ID: 490-62333-B-11 MS Matrix: Water Prep Type: Total/NA Analysis Batch: 194305 Acetone ND 250 240.2 ug/L 93 45 -141 Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Benzene ND 50.0 53.29 ug/L 107 75 -133 Bromobenzene ND 50.0 53.65 ug/L 107 60 -138 TestAmerica Nashville Page 29 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Matrix SpikeLab Sample ID: 490-62333-B-11 MS Matrix: Water Prep Type: Total/NA Analysis Batch: 194305 Bromochloromethane ND 50.0 53.43 ug/L 107 67 -139 Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Bromodichloromethane ND 50.0 49.39 ug/L 99 70 -140 Bromoform ND 50.0 48.09 ug/L 96 42 -147 Bromomethane ND 50.0 55.08 ug/L 110 16 -163 2-Butanone (MEK)ND 250 237.1 ug/L 95 50 -138 Carbon disulfide ND 50.0 50.77 ug/L 102 48 -152 Carbon tetrachloride ND 50.0 52.08 ug/L 104 62 -164 Chlorobenzene ND 50.0 52.74 ug/L 105 80 -129 Chlorodibromomethane ND 50.0 54.66 ug/L 109 66 -140 Chloroethane ND 50.0 52.43 ug/L 105 58 -137 Chloroform 5.98 50.0 55.30 ug/L 99 66 -138 Chloromethane ND 50.0 44.60 ug/L 89 10 -169 2-Chlorotoluene ND 50.0 52.59 ug/L 105 67 -138 4-Chlorotoluene ND 50.0 53.05 ug/L 106 69 -138 cis-1,2-Dichloroethene ND 50.0 51.11 ug/L 102 68 -138 cis-1,3-Dichloropropene ND 50.0 62.96 ug/L 126 71 -141 1,2-Dibromo-3-Chloropropane ND 50.0 54.23 ug/L 108 52 -126 1,2-Dibromoethane (EDB)ND 50.0 54.66 ug/L 109 75 -137 Dibromomethane ND 50.0 47.60 ug/L 95 58 -140 1,2-Dichlorobenzene ND 50.0 53.32 ug/L 107 79 -128 1,3-Dichlorobenzene ND 50.0 52.55 ug/L 105 77 -131 1,4-Dichlorobenzene ND 50.0 53.15 ug/L 106 78 -126 Dichlorodifluoromethane ND 50.0 47.49 ug/L 95 40 -127 1,1-Dichloroethane ND 50.0 51.62 ug/L 103 71 -139 1,2-Dichloroethane ND 50.0 43.52 ug/L 87 64 -136 1,1-Dichloroethene ND 50.0 53.71 ug/L 107 70 -142 1,2-Dichloroethene, Total ND 100 103.2 ug/L 103 60 -152 1,2-Dichloropropane ND 50.0 52.71 ug/L 105 67 -131 1,3-Dichloropropane ND 50.0 53.06 ug/L 106 72 -134 2,2-Dichloropropane ND 50.0 55.18 ug/L 110 37 -175 1,1-Dichloropropene ND 50.0 52.60 ug/L 105 76 -139 Diisopropyl ether ND 50.0 51.33 ug/L 103 10 -200 Ethylbenzene ND 50.0 52.63 ug/L 105 79 -139 Hexachlorobutadiene ND 50.0 45.77 ug/L 92 45 -155 2-Hexanone ND 250 259.8 ug/L 104 50 -150 Isopropyl alcohol ND 500 296.5 ug/L 59 26 -200 Isopropylbenzene ND 50.0 50.42 ug/L 101 80 -153 Methylene Chloride ND 50.0 49.21 ug/L 98 64 -139 4-Methyl-2-pentanone (MIBK)ND 250 264.1 ug/L 106 50 -147 Methyl tert-butyl ether ND 50.0 48.88 ug/L 98 66 -141 Naphthalene ND 50.0 76.66 F1 ug/L 153 55 -140 n-Butylbenzene ND 50.0 52.25 ug/L 104 66 -141 N-Propylbenzene ND 50.0 55.57 ug/L 111 69 -142 p-Isopropyltoluene ND 50.0 52.26 ug/L 105 71 -137 sec-Butylbenzene ND 50.0 51.83 ug/L 104 73 -138 Styrene ND 50.0 52.21 ug/L 104 61 -148 tert-Butylbenzene ND 50.0 52.40 ug/L 105 70 -138 1,1,1,2-Tetrachloroethane ND 50.0 53.90 ug/L 108 73 -141 TestAmerica Nashville Page 30 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Matrix SpikeLab Sample ID: 490-62333-B-11 MS Matrix: Water Prep Type: Total/NA Analysis Batch: 194305 1,1,2,2-Tetrachloroethane ND 50.0 54.82 ug/L 110 56 -143 Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Tetrachloroethene ND 50.0 55.59 ug/L 110 72 -145 Toluene ND 50.0 53.34 ug/L 106 75 -136 trans-1,2-Dichloroethene ND 50.0 52.05 ug/L 104 66 -143 trans-1,3-Dichloropropene ND 50.0 60.13 ug/L 120 59 -135 1,2,3-Trichlorobenzene ND 50.0 43.74 ug/L 87 55 -138 1,2,4-Trichlorobenzene ND 50.0 46.65 ug/L 93 60 -136 1,1,1-Trichloroethane ND 50.0 49.38 ug/L 99 76 -149 1,1,2-Trichloroethane ND 50.0 53.72 ug/L 107 74 -134 Trichloroethene ND 50.0 53.58 ug/L 107 73 -144 Trichlorofluoromethane ND 50.0 47.21 ug/L 94 58 -139 1,2,3-Trichloropropane ND 50.0 59.88 ug/L 120 53 -144 1,2,4-Trimethylbenzene ND 50.0 55.39 ug/L 111 69 -136 1,3,5-Trimethylbenzene ND 50.0 54.00 ug/L 108 69 -139 Vinyl chloride ND 50.0 53.27 ug/L 107 56 -129 Xylenes, Total ND 100 101.1 ug/L 101 74 -141 4-Bromofluorobenzene (Surr)70 -130 Surrogate 102 MS MS Qualifier Limits%Recovery 96Dibromofluoromethane (Surr)70 -130 791,2-Dichloroethane-d4 (Surr)70 -130 104Toluene-d8 (Surr)70 -130 Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-62333-C-11 MSD Matrix: Water Prep Type: Total/NA Analysis Batch: 194305 Acetone ND 250 242.3 ug/L 94 45 -141 1 21 Analyte MSD MSD DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Benzene ND 50.0 53.71 ug/L 107 75 -133 1 17 Bromobenzene ND 50.0 53.26 ug/L 107 60 -138 1 20 Bromochloromethane ND 50.0 53.54 ug/L 107 67 -139 0 17 Bromodichloromethane ND 50.0 50.26 ug/L 101 70 -140 2 18 Bromoform ND 50.0 48.78 ug/L 98 42 -147 1 16 Bromomethane ND 50.0 60.82 ug/L 122 16 -163 10 50 2-Butanone (MEK)ND 250 239.1 ug/L 96 50 -138 1 19 Carbon disulfide ND 50.0 52.88 ug/L 106 48 -152 4 21 Carbon tetrachloride ND 50.0 53.46 ug/L 107 62 -164 3 19 Chlorobenzene ND 50.0 54.26 ug/L 109 80 -129 3 14 Chlorodibromomethane ND 50.0 55.77 ug/L 112 66 -140 2 15 Chloroethane ND 50.0 54.01 ug/L 108 58 -137 3 20 Chloroform 5.98 50.0 56.51 ug/L 101 66 -138 2 18 Chloromethane ND 50.0 45.47 ug/L 91 10 -169 2 31 2-Chlorotoluene ND 50.0 53.71 ug/L 107 67 -138 2 17 4-Chlorotoluene ND 50.0 55.49 ug/L 111 69 -138 5 18 cis-1,2-Dichloroethene ND 50.0 51.53 ug/L 103 68 -138 1 17 cis-1,3-Dichloropropene ND 50.0 64.31 ug/L 129 71 -141 2 15 1,2-Dibromo-3-Chloropropane ND 50.0 58.14 ug/L 116 52 -126 7 24 TestAmerica Nashville Page 31 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-62333-C-11 MSD Matrix: Water Prep Type: Total/NA Analysis Batch: 194305 1,2-Dibromoethane (EDB)ND 50.0 56.02 ug/L 112 75 -137 2 15 Analyte MSD MSD DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Dibromomethane ND 50.0 47.35 ug/L 95 58 -140 1 16 1,2-Dichlorobenzene ND 50.0 54.18 ug/L 108 79 -128 2 15 1,3-Dichlorobenzene ND 50.0 54.82 ug/L 110 77 -131 4 15 1,4-Dichlorobenzene ND 50.0 54.14 ug/L 108 78 -126 2 15 Dichlorodifluoromethane ND 50.0 47.69 ug/L 95 40 -127 0 18 1,1-Dichloroethane ND 50.0 53.05 ug/L 106 71 -139 3 17 1,2-Dichloroethane ND 50.0 43.49 ug/L 87 64 -136 0 17 1,1-Dichloroethene ND 50.0 53.62 ug/L 107 70 -142 0 17 1,2-Dichloroethene, Total ND 100 105.0 ug/L 105 60 -152 2 33 1,2-Dichloropropane ND 50.0 53.64 ug/L 107 67 -131 2 17 1,3-Dichloropropane ND 50.0 53.57 ug/L 107 72 -134 1 14 2,2-Dichloropropane ND 50.0 55.11 ug/L 110 37 -175 0 18 1,1-Dichloropropene ND 50.0 53.96 ug/L 108 76 -139 3 17 Diisopropyl ether ND 50.0 51.72 ug/L 103 10 -200 1 50 Ethylbenzene ND 50.0 53.18 ug/L 106 79 -139 1 15 Hexachlorobutadiene ND 50.0 49.61 ug/L 99 45 -155 8 23 2-Hexanone ND 250 258.5 ug/L 103 50 -150 1 15 Isopropyl alcohol ND 500 389.4 ug/L 78 26 -200 27 30 Isopropylbenzene ND 50.0 52.21 ug/L 104 80 -153 4 16 Methylene Chloride ND 50.0 49.68 ug/L 99 64 -139 1 17 4-Methyl-2-pentanone (MIBK)ND 250 262.4 ug/L 105 50 -147 1 17 Methyl tert-butyl ether ND 50.0 48.59 ug/L 97 66 -141 1 16 Naphthalene ND 50.0 63.79 ug/L 128 55 -140 18 26 n-Butylbenzene ND 50.0 53.22 ug/L 106 66 -141 2 18 N-Propylbenzene ND 50.0 56.09 ug/L 112 69 -142 1 17 p-Isopropyltoluene ND 50.0 54.99 ug/L 110 71 -137 5 16 sec-Butylbenzene ND 50.0 54.41 ug/L 109 73 -138 5 16 Styrene ND 50.0 53.72 ug/L 107 61 -148 3 24 tert-Butylbenzene ND 50.0 55.50 ug/L 111 70 -138 6 16 1,1,1,2-Tetrachloroethane ND 50.0 55.71 ug/L 111 73 -141 3 16 1,1,2,2-Tetrachloroethane ND 50.0 53.76 ug/L 108 56 -143 2 20 Tetrachloroethene ND 50.0 57.54 ug/L 114 72 -145 3 16 Toluene ND 50.0 55.12 ug/L 110 75 -136 3 15 trans-1,2-Dichloroethene ND 50.0 53.43 ug/L 107 66 -143 3 16 trans-1,3-Dichloropropene ND 50.0 61.60 ug/L 123 59 -135 2 14 1,2,3-Trichlorobenzene ND 50.0 53.56 ug/L 107 55 -138 20 25 1,2,4-Trichlorobenzene ND 50.0 52.89 ug/L 106 60 -136 13 19 1,1,1-Trichloroethane ND 50.0 50.43 ug/L 101 76 -149 2 17 1,1,2-Trichloroethane ND 50.0 54.09 ug/L 108 74 -134 1 15 Trichloroethene ND 50.0 54.34 ug/L 109 73 -144 1 17 Trichlorofluoromethane ND 50.0 47.32 ug/L 95 58 -139 0 18 1,2,3-Trichloropropane ND 50.0 60.10 ug/L 120 53 -144 0 19 1,2,4-Trimethylbenzene ND 50.0 55.20 ug/L 110 69 -136 0 16 1,3,5-Trimethylbenzene ND 50.0 55.41 ug/L 111 69 -139 3 17 Vinyl chloride ND 50.0 55.80 ug/L 112 56 -129 5 17 Xylenes, Total ND 100 105.1 ug/L 105 74 -141 4 15 TestAmerica Nashville Page 32 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-62333-C-11 MSD Matrix: Water Prep Type: Total/NA Analysis Batch: 194305 4-Bromofluorobenzene (Surr)70 -130 Surrogate 101 MSD MSD Qualifier Limits%Recovery 94Dibromofluoromethane (Surr)70 -130 791,2-Dichloroethane-d4 (Surr)70 -130 105Toluene-d8 (Surr)70 -130 Client Sample ID: Method BlankLab Sample ID: MB 490-194478/8 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194478 RL MDL Acetone ND 0.0500 mg/Kg 10/01/14 15:29 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 0.00200 mg/Kg 10/01/14 15:29 1Benzene ND 0.00200 mg/Kg 10/01/14 15:29 1Bromobenzene ND 0.00200 mg/Kg 10/01/14 15:29 1Bromochloromethane ND 0.00200 mg/Kg 10/01/14 15:29 1Bromodichloromethane ND 0.00200 mg/Kg 10/01/14 15:29 1Bromoform ND 0.00200 mg/Kg 10/01/14 15:29 1Bromomethane ND 0.0500 mg/Kg 10/01/14 15:29 12-Butanone (MEK) ND 0.00500 mg/Kg 10/01/14 15:29 1Carbon disulfide ND 0.00200 mg/Kg 10/01/14 15:29 1Carbon tetrachloride ND 0.00200 mg/Kg 10/01/14 15:29 1Chlorobenzene ND 0.00200 mg/Kg 10/01/14 15:29 1Chlorodibromomethane ND 0.00500 mg/Kg 10/01/14 15:29 1Chloroethane ND 0.00200 mg/Kg 10/01/14 15:29 1Chloroform ND 0.00200 mg/Kg 10/01/14 15:29 1Chloromethane ND 0.00200 mg/Kg 10/01/14 15:29 12-Chlorotoluene ND 0.00200 mg/Kg 10/01/14 15:29 14-Chlorotoluene ND 0.00200 mg/Kg 10/01/14 15:29 1cis-1,2-Dichloroethene ND 0.00200 mg/Kg 10/01/14 15:29 1cis-1,3-Dichloropropene ND 0.00500 mg/Kg 10/01/14 15:29 11,2-Dibromo-3-Chloropropane ND 0.00200 mg/Kg 10/01/14 15:29 11,2-Dibromoethane (EDB) ND 0.00200 mg/Kg 10/01/14 15:29 1Dibromomethane ND 0.00200 mg/Kg 10/01/14 15:29 11,2-Dichlorobenzene ND 0.00200 mg/Kg 10/01/14 15:29 11,3-Dichlorobenzene ND 0.00200 mg/Kg 10/01/14 15:29 11,4-Dichlorobenzene ND 0.00200 mg/Kg 10/01/14 15:29 1Dichlorodifluoromethane ND 0.00200 mg/Kg 10/01/14 15:29 11,1-Dichloroethane ND 0.00200 mg/Kg 10/01/14 15:29 11,2-Dichloroethane ND 0.00200 mg/Kg 10/01/14 15:29 11,1-Dichloroethene ND 0.00200 mg/Kg 10/01/14 15:29 11,2-Dichloroethene, Total ND 0.00200 mg/Kg 10/01/14 15:29 11,2-Dichloropropane ND 0.00200 mg/Kg 10/01/14 15:29 11,3-Dichloropropane ND 0.00200 mg/Kg 10/01/14 15:29 12,2-Dichloropropane ND 0.00200 mg/Kg 10/01/14 15:29 11,1-Dichloropropene ND 0.00200 mg/Kg 10/01/14 15:29 1Diisopropyl ether ND 0.00200 mg/Kg 10/01/14 15:29 1Ethylbenzene ND 0.00500 mg/Kg 10/01/14 15:29 1Hexachlorobutadiene ND 0.0500 mg/Kg 10/01/14 15:29 12-Hexanone TestAmerica Nashville Page 33 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-194478/8 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194478 RL MDL Isopropylbenzene ND 0.00200 mg/Kg 10/01/14 15:29 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 0.0100 mg/Kg 10/01/14 15:29 1Methylene Chloride ND 0.0500 mg/Kg 10/01/14 15:29 14-Methyl-2-pentanone (MIBK) ND 0.00200 mg/Kg 10/01/14 15:29 1Methyl tert-butyl ether ND 0.00500 mg/Kg 10/01/14 15:29 1Naphthalene ND 0.00200 mg/Kg 10/01/14 15:29 1n-Butylbenzene ND 0.00200 mg/Kg 10/01/14 15:29 1N-Propylbenzene ND 0.00200 mg/Kg 10/01/14 15:29 1p-Isopropyltoluene ND 0.00200 mg/Kg 10/01/14 15:29 1sec-Butylbenzene ND 0.00200 mg/Kg 10/01/14 15:29 1Styrene ND 0.00200 mg/Kg 10/01/14 15:29 1tert-Butylbenzene ND 0.00200 mg/Kg 10/01/14 15:29 11,1,1,2-Tetrachloroethane ND 0.00200 mg/Kg 10/01/14 15:29 11,1,2,2-Tetrachloroethane ND 0.00200 mg/Kg 10/01/14 15:29 1Tetrachloroethene ND 0.00200 mg/Kg 10/01/14 15:29 1Toluene ND 0.00200 mg/Kg 10/01/14 15:29 1trans-1,2-Dichloroethene ND 0.00200 mg/Kg 10/01/14 15:29 1trans-1,3-Dichloropropene ND 0.00200 mg/Kg 10/01/14 15:29 11,2,3-Trichlorobenzene ND 0.00200 mg/Kg 10/01/14 15:29 11,2,4-Trichlorobenzene ND 0.00200 mg/Kg 10/01/14 15:29 11,1,1-Trichloroethane ND 0.00500 mg/Kg 10/01/14 15:29 11,1,2-Trichloroethane ND 0.00200 mg/Kg 10/01/14 15:29 1Trichloroethene ND 0.00200 mg/Kg 10/01/14 15:29 1Trichlorofluoromethane ND 0.00200 mg/Kg 10/01/14 15:29 11,2,3-Trichloropropane ND 0.00200 mg/Kg 10/01/14 15:29 11,2,4-Trimethylbenzene ND 0.00200 mg/Kg 10/01/14 15:29 11,3,5-Trimethylbenzene ND 0.00200 mg/Kg 10/01/14 15:29 1Vinyl chloride ND 0.00300 mg/Kg 10/01/14 15:29 1Xylenes, Total 4-Bromofluorobenzene (Surr)90 70-130 10/01/14 15:29 1 MB MB Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery 99 10/01/14 15:29 1Dibromofluoromethane (Surr)70-130 96 10/01/14 15:29 11,2-Dichloroethane-d4 (Surr)70-130 101 10/01/14 15:29 1Toluene-d8 (Surr)70-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194478/4 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194478 Acetone 0.250 0.1825 mg/Kg 73 51 -149 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Benzene 0.0500 0.04624 mg/Kg 92 75 -127 Bromobenzene 0.0500 0.04568 mg/Kg 91 75 -130 Bromochloromethane 0.0500 0.04802 mg/Kg 96 70 -132 Bromodichloromethane 0.0500 0.04948 mg/Kg 99 68 -135 Bromoform 0.0500 0.05779 E mg/Kg 116 36 -150 Bromomethane 0.0500 0.05712 mg/Kg 114 43 -142 2-Butanone (MEK)0.250 0.1971 mg/Kg 79 61 -132 TestAmerica Nashville Page 34 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194478/4 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194478 Carbon disulfide 0.0500 0.04714 mg/Kg 94 74 -135 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Carbon tetrachloride 0.0500 0.04935 mg/Kg 99 70 -141 Chlorobenzene 0.0500 0.04695 mg/Kg 94 84 -125 Chlorodibromomethane 0.0500 0.05429 mg/Kg 109 66 -134 Chloroethane 0.0500 0.04409 mg/Kg 88 53 -144 Chloroform 0.0500 0.04527 mg/Kg 91 76 -130 Chloromethane 0.0500 0.03986 mg/Kg 80 23 -150 2-Chlorotoluene 0.0500 0.04578 mg/Kg 92 78 -132 4-Chlorotoluene 0.0500 0.04511 mg/Kg 90 77 -138 cis-1,2-Dichloroethene 0.0500 0.04600 mg/Kg 92 75 -125 cis-1,3-Dichloropropene 0.0500 0.04867 mg/Kg 97 73 -148 1,2-Dibromo-3-Chloropropane 0.0500 0.04979 mg/Kg 100 49 -142 1,2-Dibromoethane (EDB)0.0500 0.04585 mg/Kg 92 80 -135 Dibromomethane 0.0500 0.04550 mg/Kg 91 71 -130 1,2-Dichlorobenzene 0.0500 0.04894 mg/Kg 98 80 -134 1,3-Dichlorobenzene 0.0500 0.04769 mg/Kg 95 79 -137 1,4-Dichlorobenzene 0.0500 0.04600 mg/Kg 92 77 -139 Dichlorodifluoromethane 0.0500 0.04460 mg/Kg 89 12 -144 1,1-Dichloroethane 0.0500 0.04939 mg/Kg 99 75 -124 1,2-Dichloroethane 0.0500 0.04567 mg/Kg 91 65 -134 1,1-Dichloroethene 0.0500 0.04886 mg/Kg 98 75 -131 1,2-Dichloroethene, Total 0.100 0.09390 mg/Kg 94 75 -128 1,2-Dichloropropane 0.0500 0.04588 mg/Kg 92 69 -120 1,3-Dichloropropane 0.0500 0.04509 mg/Kg 90 78 -126 2,2-Dichloropropane 0.0500 0.05034 mg/Kg 101 68 -145 1,1-Dichloropropene 0.0500 0.04644 mg/Kg 93 79 -127 Diisopropyl ether 0.0500 0.04593 mg/Kg 92 68 -124 Ethylbenzene 0.0500 0.04698 mg/Kg 94 80 -134 Hexachlorobutadiene 0.0500 0.04805 mg/Kg 96 65 -148 2-Hexanone 0.250 0.2055 mg/Kg 82 57 -148 Isopropylbenzene 0.0500 0.04740 mg/Kg 95 80 -150 Methylene Chloride 0.0500 0.04771 mg/Kg 95 68 -144 4-Methyl-2-pentanone (MIBK)0.250 0.2059 mg/Kg 82 59 -138 Methyl tert-butyl ether 0.0500 0.05811 mg/Kg 116 70 -136 Naphthalene 0.0500 0.05040 mg/Kg 101 69 -150 n-Butylbenzene 0.0500 0.04471 mg/Kg 89 72 -152 N-Propylbenzene 0.0500 0.04579 mg/Kg 92 75 -137 p-Isopropyltoluene 0.0500 0.04544 mg/Kg 91 77 -141 sec-Butylbenzene 0.0500 0.04489 mg/Kg 90 79 -141 Styrene 0.0500 0.04712 mg/Kg 94 82 -137 tert-Butylbenzene 0.0500 0.04585 mg/Kg 92 80 -132 1,1,1,2-Tetrachloroethane 0.0500 0.05021 mg/Kg 100 80 -136 1,1,2,2-Tetrachloroethane 0.0500 0.04323 mg/Kg 86 66 -134 Tetrachloroethene 0.0500 0.04857 mg/Kg 97 78 -140 Toluene 0.0500 0.04605 mg/Kg 92 80 -132 trans-1,2-Dichloroethene 0.0500 0.04790 mg/Kg 96 76 -128 trans-1,3-Dichloropropene 0.0500 0.05041 mg/Kg 101 62 -139 1,2,3-Trichlorobenzene 0.0500 0.05102 mg/Kg 102 70 -150 TestAmerica Nashville Page 35 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194478/4 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194478 1,2,4-Trichlorobenzene 0.0500 0.04932 mg/Kg 99 62 -150 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits 1,1,1-Trichloroethane 0.0500 0.04793 mg/Kg 96 72 -140 1,1,2-Trichloroethane 0.0500 0.04497 mg/Kg 90 78 -128 Trichloroethene 0.0500 0.04958 mg/Kg 99 77 -127 Trichlorofluoromethane 0.0500 0.04591 mg/Kg 92 50 -140 1,2,3-Trichloropropane 0.0500 0.04288 mg/Kg 86 65 -139 1,2,4-Trimethylbenzene 0.0500 0.04803 mg/Kg 96 77 -139 1,3,5-Trimethylbenzene 0.0500 0.04536 mg/Kg 91 78 -138 Vinyl chloride 0.0500 0.04420 mg/Kg 88 47 -136 Xylenes, Total 0.100 0.09417 mg/Kg 94 80 -137 4-Bromofluorobenzene (Surr)70 -130 Surrogate 99 LCS LCS Qualifier Limits%Recovery 101Dibromofluoromethane (Surr)70 -130 941,2-Dichloroethane-d4 (Surr)70 -130 100Toluene-d8 (Surr)70 -130 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-194478/5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194478 Acetone 0.250 0.1820 mg/Kg 73 51 -149 0 50 Analyte LCSD LCSD DUnitResult Qualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Benzene 0.0500 0.04610 mg/Kg 92 75 -127 0 50 Bromobenzene 0.0500 0.04647 mg/Kg 93 75 -130 2 50 Bromochloromethane 0.0500 0.04821 mg/Kg 96 70 -132 0 50 Bromodichloromethane 0.0500 0.04977 mg/Kg 100 68 -135 1 50 Bromoform 0.0500 0.05885 E mg/Kg 118 36 -150 2 50 Bromomethane 0.0500 0.05477 mg/Kg 110 43 -142 4 50 2-Butanone (MEK)0.250 0.2148 mg/Kg 86 61 -132 9 50 Carbon disulfide 0.0500 0.04619 mg/Kg 92 74 -135 2 50 Carbon tetrachloride 0.0500 0.04892 mg/Kg 98 70 -141 1 50 Chlorobenzene 0.0500 0.04748 mg/Kg 95 84 -125 1 50 Chlorodibromomethane 0.0500 0.05567 mg/Kg 111 66 -134 3 50 Chloroethane 0.0500 0.04269 mg/Kg 85 53 -144 3 50 Chloroform 0.0500 0.04514 mg/Kg 90 76 -130 0 49 Chloromethane 0.0500 0.03182 mg/Kg 64 23 -150 22 50 2-Chlorotoluene 0.0500 0.04556 mg/Kg 91 78 -132 0 50 4-Chlorotoluene 0.0500 0.04570 mg/Kg 91 77 -138 1 50 cis-1,2-Dichloroethene 0.0500 0.04557 mg/Kg 91 75 -125 1 50 cis-1,3-Dichloropropene 0.0500 0.05033 mg/Kg 101 73 -148 3 50 1,2-Dibromo-3-Chloropropane 0.0500 0.05082 mg/Kg 102 49 -142 2 50 1,2-Dibromoethane (EDB)0.0500 0.04721 mg/Kg 94 80 -135 3 50 Dibromomethane 0.0500 0.04661 mg/Kg 93 71 -130 2 50 1,2-Dichlorobenzene 0.0500 0.04839 mg/Kg 97 80 -134 1 50 1,3-Dichlorobenzene 0.0500 0.04705 mg/Kg 94 79 -137 1 50 1,4-Dichlorobenzene 0.0500 0.04505 mg/Kg 90 77 -139 2 50 Dichlorodifluoromethane 0.0500 0.04368 mg/Kg 87 12 -144 2 50 TestAmerica Nashville Page 36 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-194478/5 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194478 1,1-Dichloroethane 0.0500 0.04644 mg/Kg 93 75 -124 6 50 Analyte LCSD LCSD DUnitResult Qualifier %Rec Spike Added %Rec. Limits LimitRPD RPD 1,2-Dichloroethane 0.0500 0.04679 mg/Kg 94 65 -134 2 50 1,1-Dichloroethene 0.0500 0.04794 mg/Kg 96 75 -131 2 50 1,2-Dichloroethene, Total 0.100 0.09270 mg/Kg 93 75 -128 1 41 1,2-Dichloropropane 0.0500 0.04590 mg/Kg 92 69 -120 0 50 1,3-Dichloropropane 0.0500 0.04675 mg/Kg 94 78 -126 4 42 2,2-Dichloropropane 0.0500 0.04904 mg/Kg 98 68 -145 3 50 1,1-Dichloropropene 0.0500 0.04660 mg/Kg 93 79 -127 0 50 Diisopropyl ether 0.0500 0.04566 mg/Kg 91 68 -124 1 45 Ethylbenzene 0.0500 0.04719 mg/Kg 94 80 -134 0 50 Hexachlorobutadiene 0.0500 0.04755 mg/Kg 95 65 -148 1 50 2-Hexanone 0.250 0.2193 mg/Kg 88 57 -148 7 50 Isopropylbenzene 0.0500 0.04773 mg/Kg 95 80 -150 1 50 Methylene Chloride 0.0500 0.04842 mg/Kg 97 68 -144 1 50 4-Methyl-2-pentanone (MIBK)0.250 0.2229 mg/Kg 89 59 -138 8 50 Methyl tert-butyl ether 0.0500 0.05830 mg/Kg 117 70 -136 0 50 Naphthalene 0.0500 0.05210 mg/Kg 104 69 -150 3 50 n-Butylbenzene 0.0500 0.04404 mg/Kg 88 72 -152 2 50 N-Propylbenzene 0.0500 0.04615 mg/Kg 92 75 -137 1 50 p-Isopropyltoluene 0.0500 0.04542 mg/Kg 91 77 -141 0 50 sec-Butylbenzene 0.0500 0.04503 mg/Kg 90 79 -141 0 50 Styrene 0.0500 0.04784 mg/Kg 96 82 -137 2 50 tert-Butylbenzene 0.0500 0.04693 mg/Kg 94 80 -132 2 50 1,1,1,2-Tetrachloroethane 0.0500 0.05137 mg/Kg 103 80 -136 2 50 1,1,2,2-Tetrachloroethane 0.0500 0.04575 mg/Kg 91 66 -134 6 50 Tetrachloroethene 0.0500 0.05007 mg/Kg 100 78 -140 3 50 Toluene 0.0500 0.04850 mg/Kg 97 80 -132 5 50 trans-1,2-Dichloroethene 0.0500 0.04713 mg/Kg 94 76 -128 2 50 trans-1,3-Dichloropropene 0.0500 0.05080 mg/Kg 102 62 -139 1 50 1,2,3-Trichlorobenzene 0.0500 0.05145 mg/Kg 103 70 -150 1 50 1,2,4-Trichlorobenzene 0.0500 0.04898 mg/Kg 98 62 -150 1 50 1,1,1-Trichloroethane 0.0500 0.04847 mg/Kg 97 72 -140 1 50 1,1,2-Trichloroethane 0.0500 0.04616 mg/Kg 92 78 -128 3 50 Trichloroethene 0.0500 0.04939 mg/Kg 99 77 -127 0 50 Trichlorofluoromethane 0.0500 0.04491 mg/Kg 90 50 -140 2 50 1,2,3-Trichloropropane 0.0500 0.04565 mg/Kg 91 65 -139 6 50 1,2,4-Trimethylbenzene 0.0500 0.04810 mg/Kg 96 77 -139 0 50 1,3,5-Trimethylbenzene 0.0500 0.04561 mg/Kg 91 78 -138 1 50 Vinyl chloride 0.0500 0.04313 mg/Kg 86 47 -136 2 50 Xylenes, Total 0.100 0.09555 mg/Kg 96 80 -137 1 50 4-Bromofluorobenzene (Surr)70 -130 Surrogate 98 LCSD LCSD Qualifier Limits%Recovery 99Dibromofluoromethane (Surr)70 -130 931,2-Dichloroethane-d4 (Surr)70 -130 102Toluene-d8 (Surr)70 -130 TestAmerica Nashville Page 37 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-194702/8 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194702 RL MDL Acetone ND 0.0500 mg/Kg 10/02/14 13:34 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 0.00200 mg/Kg 10/02/14 13:34 1Benzene ND 0.00200 mg/Kg 10/02/14 13:34 1Bromobenzene ND 0.00200 mg/Kg 10/02/14 13:34 1Bromochloromethane ND 0.00200 mg/Kg 10/02/14 13:34 1Bromodichloromethane ND 0.00200 mg/Kg 10/02/14 13:34 1Bromoform ND 0.00200 mg/Kg 10/02/14 13:34 1Bromomethane ND 0.0500 mg/Kg 10/02/14 13:34 12-Butanone (MEK) ND 0.00500 mg/Kg 10/02/14 13:34 1Carbon disulfide ND 0.00200 mg/Kg 10/02/14 13:34 1Carbon tetrachloride ND 0.00200 mg/Kg 10/02/14 13:34 1Chlorobenzene ND 0.00200 mg/Kg 10/02/14 13:34 1Chlorodibromomethane ND 0.00500 mg/Kg 10/02/14 13:34 1Chloroethane ND 0.00200 mg/Kg 10/02/14 13:34 1Chloroform ND 0.00200 mg/Kg 10/02/14 13:34 1Chloromethane ND 0.00200 mg/Kg 10/02/14 13:34 12-Chlorotoluene ND 0.00200 mg/Kg 10/02/14 13:34 14-Chlorotoluene ND 0.00200 mg/Kg 10/02/14 13:34 1cis-1,2-Dichloroethene ND 0.00200 mg/Kg 10/02/14 13:34 1cis-1,3-Dichloropropene ND 0.00500 mg/Kg 10/02/14 13:34 11,2-Dibromo-3-Chloropropane ND 0.00200 mg/Kg 10/02/14 13:34 11,2-Dibromoethane (EDB) ND 0.00200 mg/Kg 10/02/14 13:34 1Dibromomethane ND 0.00200 mg/Kg 10/02/14 13:34 11,2-Dichlorobenzene ND 0.00200 mg/Kg 10/02/14 13:34 11,3-Dichlorobenzene ND 0.00200 mg/Kg 10/02/14 13:34 11,4-Dichlorobenzene ND 0.00200 mg/Kg 10/02/14 13:34 1Dichlorodifluoromethane ND 0.00200 mg/Kg 10/02/14 13:34 11,1-Dichloroethane ND 0.00200 mg/Kg 10/02/14 13:34 11,2-Dichloroethane ND 0.00200 mg/Kg 10/02/14 13:34 11,1-Dichloroethene ND 0.00200 mg/Kg 10/02/14 13:34 11,2-Dichloroethene, Total ND 0.00200 mg/Kg 10/02/14 13:34 11,2-Dichloropropane ND 0.00200 mg/Kg 10/02/14 13:34 11,3-Dichloropropane ND 0.00200 mg/Kg 10/02/14 13:34 12,2-Dichloropropane ND 0.00200 mg/Kg 10/02/14 13:34 11,1-Dichloropropene ND 0.00200 mg/Kg 10/02/14 13:34 1Diisopropyl ether ND 0.00200 mg/Kg 10/02/14 13:34 1Ethylbenzene ND 0.00500 mg/Kg 10/02/14 13:34 1Hexachlorobutadiene ND 0.0500 mg/Kg 10/02/14 13:34 12-Hexanone ND 0.00200 mg/Kg 10/02/14 13:34 1Isopropylbenzene ND 0.0100 mg/Kg 10/02/14 13:34 1Methylene Chloride ND 0.0500 mg/Kg 10/02/14 13:34 14-Methyl-2-pentanone (MIBK) ND 0.00200 mg/Kg 10/02/14 13:34 1Methyl tert-butyl ether ND 0.00500 mg/Kg 10/02/14 13:34 1Naphthalene ND 0.00200 mg/Kg 10/02/14 13:34 1n-Butylbenzene ND 0.00200 mg/Kg 10/02/14 13:34 1N-Propylbenzene ND 0.00200 mg/Kg 10/02/14 13:34 1p-Isopropyltoluene ND 0.00200 mg/Kg 10/02/14 13:34 1sec-Butylbenzene ND 0.00200 mg/Kg 10/02/14 13:34 1Styrene TestAmerica Nashville Page 38 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-194702/8 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194702 RL MDL tert-Butylbenzene ND 0.00200 mg/Kg 10/02/14 13:34 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 0.00200 mg/Kg 10/02/14 13:34 11,1,1,2-Tetrachloroethane ND 0.00200 mg/Kg 10/02/14 13:34 11,1,2,2-Tetrachloroethane ND 0.00200 mg/Kg 10/02/14 13:34 1Tetrachloroethene ND 0.00200 mg/Kg 10/02/14 13:34 1Toluene ND 0.00200 mg/Kg 10/02/14 13:34 1trans-1,2-Dichloroethene ND 0.00200 mg/Kg 10/02/14 13:34 1trans-1,3-Dichloropropene ND 0.00200 mg/Kg 10/02/14 13:34 11,2,3-Trichlorobenzene ND 0.00200 mg/Kg 10/02/14 13:34 11,2,4-Trichlorobenzene ND 0.00200 mg/Kg 10/02/14 13:34 11,1,1-Trichloroethane ND 0.00500 mg/Kg 10/02/14 13:34 11,1,2-Trichloroethane ND 0.00200 mg/Kg 10/02/14 13:34 1Trichloroethene ND 0.00200 mg/Kg 10/02/14 13:34 1Trichlorofluoromethane ND 0.00200 mg/Kg 10/02/14 13:34 11,2,3-Trichloropropane ND 0.00200 mg/Kg 10/02/14 13:34 11,2,4-Trimethylbenzene ND 0.00200 mg/Kg 10/02/14 13:34 11,3,5-Trimethylbenzene ND 0.00200 mg/Kg 10/02/14 13:34 1Vinyl chloride ND 0.00300 mg/Kg 10/02/14 13:34 1Xylenes, Total 4-Bromofluorobenzene (Surr)87 70-130 10/02/14 13:34 1 MB MB Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery 116 10/02/14 13:34 1Dibromofluoromethane (Surr)70-130 122 10/02/14 13:34 11,2-Dichloroethane-d4 (Surr)70-130 98 10/02/14 13:34 1Toluene-d8 (Surr)70-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194702/18 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194702 Acetone 0.250 0.2154 mg/Kg 86 51 -149 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Benzene 0.0500 0.04958 mg/Kg 99 75 -127 Bromobenzene 0.0500 0.04843 mg/Kg 97 75 -130 Bromochloromethane 0.0500 0.05444 mg/Kg 109 70 -132 Bromodichloromethane 0.0500 0.05336 mg/Kg 107 68 -135 Bromoform 0.0500 0.06216 E mg/Kg 124 36 -150 Bromomethane 0.0500 0.07027 mg/Kg 141 43 -142 2-Butanone (MEK)0.250 0.2279 mg/Kg 91 61 -132 Carbon disulfide 0.0500 0.05005 mg/Kg 100 74 -135 Carbon tetrachloride 0.0500 0.05518 mg/Kg 110 70 -141 Chlorobenzene 0.0500 0.04854 mg/Kg 97 84 -125 Chlorodibromomethane 0.0500 0.05639 mg/Kg 113 66 -134 Chloroethane 0.0500 0.04888 mg/Kg 98 53 -144 Chloroform 0.0500 0.05002 mg/Kg 100 76 -130 Chloromethane 0.0500 0.08106 *mg/Kg 162 23 -150 2-Chlorotoluene 0.0500 0.04771 mg/Kg 95 78 -132 4-Chlorotoluene 0.0500 0.04799 mg/Kg 96 77 -138 cis-1,2-Dichloroethene 0.0500 0.05107 mg/Kg 102 75 -125 TestAmerica Nashville Page 39 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194702/18 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194702 cis-1,3-Dichloropropene 0.0500 0.04843 mg/Kg 97 73 -148 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits 1,2-Dibromo-3-Chloropropane 0.0500 0.05240 mg/Kg 105 49 -142 1,2-Dibromoethane (EDB)0.0500 0.04842 mg/Kg 97 80 -135 Dibromomethane 0.0500 0.05051 mg/Kg 101 71 -130 1,2-Dichlorobenzene 0.0500 0.04952 mg/Kg 99 80 -134 1,3-Dichlorobenzene 0.0500 0.04972 mg/Kg 99 79 -137 1,4-Dichlorobenzene 0.0500 0.04738 mg/Kg 95 77 -139 Dichlorodifluoromethane 0.0500 0.05861 mg/Kg 117 12 -144 1,1-Dichloroethane 0.0500 0.05179 mg/Kg 104 75 -124 1,2-Dichloroethane 0.0500 0.05499 mg/Kg 110 65 -134 1,1-Dichloroethene 0.0500 0.05260 mg/Kg 105 75 -131 1,2-Dichloroethene, Total 0.100 0.1019 mg/Kg 102 75 -128 1,2-Dichloropropane 0.0500 0.04866 mg/Kg 97 69 -120 1,3-Dichloropropane 0.0500 0.04724 mg/Kg 94 78 -126 2,2-Dichloropropane 0.0500 0.05556 mg/Kg 111 68 -145 1,1-Dichloropropene 0.0500 0.05107 mg/Kg 102 79 -127 Diisopropyl ether 0.0500 0.04882 mg/Kg 98 68 -124 Ethylbenzene 0.0500 0.04773 mg/Kg 95 80 -134 Hexachlorobutadiene 0.0500 0.04884 mg/Kg 98 65 -148 2-Hexanone 0.250 0.2154 mg/Kg 86 57 -148 Isopropylbenzene 0.0500 0.04702 mg/Kg 94 80 -150 Methylene Chloride 0.0500 0.05356 mg/Kg 107 68 -144 4-Methyl-2-pentanone (MIBK)0.250 0.2227 mg/Kg 89 59 -138 Methyl tert-butyl ether 0.0500 0.06243 mg/Kg 125 70 -136 Naphthalene 0.0500 0.04735 mg/Kg 95 69 -150 n-Butylbenzene 0.0500 0.04593 mg/Kg 92 72 -152 N-Propylbenzene 0.0500 0.04698 mg/Kg 94 75 -137 p-Isopropyltoluene 0.0500 0.04558 mg/Kg 91 77 -141 sec-Butylbenzene 0.0500 0.04569 mg/Kg 91 79 -141 Styrene 0.0500 0.04808 mg/Kg 96 82 -137 tert-Butylbenzene 0.0500 0.04592 mg/Kg 92 80 -132 1,1,1,2-Tetrachloroethane 0.0500 0.05325 mg/Kg 106 80 -136 1,1,2,2-Tetrachloroethane 0.0500 0.04582 mg/Kg 92 66 -134 Tetrachloroethene 0.0500 0.05123 mg/Kg 102 78 -140 Toluene 0.0500 0.04815 mg/Kg 96 80 -132 trans-1,2-Dichloroethene 0.0500 0.05085 mg/Kg 102 76 -128 trans-1,3-Dichloropropene 0.0500 0.05171 mg/Kg 103 62 -139 1,2,3-Trichlorobenzene 0.0500 0.05046 mg/Kg 101 70 -150 1,2,4-Trichlorobenzene 0.0500 0.04878 mg/Kg 98 62 -150 1,1,1-Trichloroethane 0.0500 0.05404 mg/Kg 108 72 -140 1,1,2-Trichloroethane 0.0500 0.04765 mg/Kg 95 78 -128 Trichloroethene 0.0500 0.05197 mg/Kg 104 77 -127 Trichlorofluoromethane 0.0500 0.05329 mg/Kg 107 50 -140 1,2,3-Trichloropropane 0.0500 0.04794 mg/Kg 96 65 -139 1,2,4-Trimethylbenzene 0.0500 0.04679 mg/Kg 94 77 -139 1,3,5-Trimethylbenzene 0.0500 0.04710 mg/Kg 94 78 -138 Vinyl chloride 0.0500 0.05247 mg/Kg 105 47 -136 Xylenes, Total 0.100 0.09630 mg/Kg 96 80 -137 TestAmerica Nashville Page 40 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194702/18 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194702 4-Bromofluorobenzene (Surr)70 -130 Surrogate 99 LCS LCS Qualifier Limits%Recovery 104Dibromofluoromethane (Surr)70 -130 1081,2-Dichloroethane-d4 (Surr)70 -130 97Toluene-d8 (Surr)70 -130 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-194702/19 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194702 Acetone 0.250 0.2119 mg/Kg 85 51 -149 2 50 Analyte LCSD LCSD DUnitResult Qualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Benzene 0.0500 0.04869 mg/Kg 97 75 -127 2 50 Bromobenzene 0.0500 0.04422 mg/Kg 88 75 -130 9 50 Bromochloromethane 0.0500 0.05335 mg/Kg 107 70 -132 2 50 Bromodichloromethane 0.0500 0.05341 mg/Kg 107 68 -135 0 50 Bromoform 0.0500 0.06299 E mg/Kg 126 36 -150 1 50 Bromomethane 0.0500 0.07407 *mg/Kg 148 43 -142 5 50 2-Butanone (MEK)0.250 0.2134 mg/Kg 85 61 -132 7 50 Carbon disulfide 0.0500 0.05200 mg/Kg 104 74 -135 4 50 Carbon tetrachloride 0.0500 0.05553 mg/Kg 111 70 -141 1 50 Chlorobenzene 0.0500 0.04865 mg/Kg 97 84 -125 0 50 Chlorodibromomethane 0.0500 0.05803 mg/Kg 116 66 -134 3 50 Chloroethane 0.0500 0.05065 mg/Kg 101 53 -144 4 50 Chloroform 0.0500 0.04996 mg/Kg 100 76 -130 0 49 Chloromethane 0.0500 0.06899 mg/Kg 138 23 -150 16 50 2-Chlorotoluene 0.0500 0.04267 mg/Kg 85 78 -132 11 50 4-Chlorotoluene 0.0500 0.03994 mg/Kg 80 77 -138 18 50 cis-1,2-Dichloroethene 0.0500 0.04960 mg/Kg 99 75 -125 3 50 cis-1,3-Dichloropropene 0.0500 0.04887 mg/Kg 98 73 -148 1 50 1,2-Dibromo-3-Chloropropane 0.0500 0.04829 mg/Kg 97 49 -142 8 50 1,2-Dibromoethane (EDB)0.0500 0.04834 mg/Kg 97 80 -135 0 50 Dibromomethane 0.0500 0.05026 mg/Kg 101 71 -130 0 50 1,2-Dichlorobenzene 0.0500 0.04632 mg/Kg 93 80 -134 7 50 1,3-Dichlorobenzene 0.0500 0.04606 mg/Kg 92 79 -137 8 50 1,4-Dichlorobenzene 0.0500 0.04691 mg/Kg 94 77 -139 1 50 Dichlorodifluoromethane 0.0500 0.05973 mg/Kg 119 12 -144 2 50 1,1-Dichloroethane 0.0500 0.05071 mg/Kg 101 75 -124 2 50 1,2-Dichloroethane 0.0500 0.05302 mg/Kg 106 65 -134 4 50 1,1-Dichloroethene 0.0500 0.05521 mg/Kg 110 75 -131 5 50 1,2-Dichloroethene, Total 0.100 0.1024 mg/Kg 102 75 -128 0 41 1,2-Dichloropropane 0.0500 0.04728 mg/Kg 95 69 -120 3 50 1,3-Dichloropropane 0.0500 0.04771 mg/Kg 95 78 -126 1 42 2,2-Dichloropropane 0.0500 0.05520 mg/Kg 110 68 -145 1 50 1,1-Dichloropropene 0.0500 0.04950 mg/Kg 99 79 -127 3 50 Diisopropyl ether 0.0500 0.04689 mg/Kg 94 68 -124 4 45 Ethylbenzene 0.0500 0.04768 mg/Kg 95 80 -134 0 50 Hexachlorobutadiene 0.0500 0.04583 mg/Kg 92 65 -148 6 50 2-Hexanone 0.250 0.2080 mg/Kg 83 57 -148 3 50 TestAmerica Nashville Page 41 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-194702/19 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194702 Isopropylbenzene 0.0500 0.04667 mg/Kg 93 80 -150 1 50 Analyte LCSD LCSD DUnitResult Qualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Methylene Chloride 0.0500 0.05103 mg/Kg 102 68 -144 5 50 4-Methyl-2-pentanone (MIBK)0.250 0.2142 mg/Kg 86 59 -138 4 50 Methyl tert-butyl ether 0.0500 0.06047 mg/Kg 121 70 -136 3 50 Naphthalene 0.0500 0.04305 mg/Kg 86 69 -150 10 50 n-Butylbenzene 0.0500 0.04087 mg/Kg 82 72 -152 12 50 N-Propylbenzene 0.0500 0.04285 mg/Kg 86 75 -137 9 50 p-Isopropyltoluene 0.0500 0.04214 mg/Kg 84 77 -141 8 50 sec-Butylbenzene 0.0500 0.04129 mg/Kg 83 79 -141 10 50 Styrene 0.0500 0.04796 mg/Kg 96 82 -137 0 50 tert-Butylbenzene 0.0500 0.04223 mg/Kg 84 80 -132 8 50 1,1,1,2-Tetrachloroethane 0.0500 0.05408 mg/Kg 108 80 -136 2 50 1,1,2,2-Tetrachloroethane 0.0500 0.04389 mg/Kg 88 66 -134 4 50 Tetrachloroethene 0.0500 0.05179 mg/Kg 104 78 -140 1 50 Toluene 0.0500 0.04841 mg/Kg 97 80 -132 1 50 trans-1,2-Dichloroethene 0.0500 0.05276 mg/Kg 106 76 -128 4 50 trans-1,3-Dichloropropene 0.0500 0.05120 mg/Kg 102 62 -139 1 50 1,2,3-Trichlorobenzene 0.0500 0.04716 mg/Kg 94 70 -150 7 50 1,2,4-Trichlorobenzene 0.0500 0.04475 mg/Kg 89 62 -150 9 50 1,1,1-Trichloroethane 0.0500 0.05348 mg/Kg 107 72 -140 1 50 1,1,2-Trichloroethane 0.0500 0.04784 mg/Kg 96 78 -128 0 50 Trichloroethene 0.0500 0.05147 mg/Kg 103 77 -127 1 50 Trichlorofluoromethane 0.0500 0.05491 mg/Kg 110 50 -140 3 50 1,2,3-Trichloropropane 0.0500 0.04385 mg/Kg 88 65 -139 9 50 1,2,4-Trimethylbenzene 0.0500 0.04360 mg/Kg 87 77 -139 7 50 1,3,5-Trimethylbenzene 0.0500 0.04301 mg/Kg 86 78 -138 9 50 Vinyl chloride 0.0500 0.05309 mg/Kg 106 47 -136 1 50 Xylenes, Total 0.100 0.09555 mg/Kg 96 80 -137 1 50 4-Bromofluorobenzene (Surr)70 -130 Surrogate 92 LCSD LCSD Qualifier Limits%Recovery 104Dibromofluoromethane (Surr)70 -130 1061,2-Dichloroethane-d4 (Surr)70 -130 100Toluene-d8 (Surr)70 -130 Client Sample ID: Method BlankLab Sample ID: MB 490-194979/10 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194979 RL MDL Acetone ND 2.50 mg/Kg 10/03/14 16:30 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 0.100 mg/Kg 10/03/14 16:30 1Benzene ND 0.100 mg/Kg 10/03/14 16:30 1Bromobenzene ND 0.100 mg/Kg 10/03/14 16:30 1Bromochloromethane ND 0.100 mg/Kg 10/03/14 16:30 1Bromodichloromethane ND 0.100 mg/Kg 10/03/14 16:30 1Bromoform ND 0.100 mg/Kg 10/03/14 16:30 1Bromomethane ND 2.50 mg/Kg 10/03/14 16:30 12-Butanone (MEK) TestAmerica Nashville Page 42 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-194979/10 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194979 RL MDL Carbon disulfide ND 0.250 mg/Kg 10/03/14 16:30 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 0.100 mg/Kg 10/03/14 16:30 1Carbon tetrachloride ND 0.100 mg/Kg 10/03/14 16:30 1Chlorobenzene ND 0.100 mg/Kg 10/03/14 16:30 1Chlorodibromomethane ND 0.250 mg/Kg 10/03/14 16:30 1Chloroethane ND 0.100 mg/Kg 10/03/14 16:30 1Chloroform ND 0.100 mg/Kg 10/03/14 16:30 1Chloromethane ND 0.100 mg/Kg 10/03/14 16:30 12-Chlorotoluene ND 0.100 mg/Kg 10/03/14 16:30 14-Chlorotoluene ND 0.100 mg/Kg 10/03/14 16:30 1cis-1,2-Dichloroethene ND 0.100 mg/Kg 10/03/14 16:30 1cis-1,3-Dichloropropene ND 0.250 mg/Kg 10/03/14 16:30 11,2-Dibromo-3-Chloropropane ND 0.100 mg/Kg 10/03/14 16:30 11,2-Dibromoethane (EDB) ND 0.100 mg/Kg 10/03/14 16:30 1Dibromomethane ND 0.100 mg/Kg 10/03/14 16:30 11,2-Dichlorobenzene ND 0.100 mg/Kg 10/03/14 16:30 11,3-Dichlorobenzene ND 0.100 mg/Kg 10/03/14 16:30 11,4-Dichlorobenzene ND 0.100 mg/Kg 10/03/14 16:30 1Dichlorodifluoromethane ND 0.100 mg/Kg 10/03/14 16:30 11,1-Dichloroethane ND 0.100 mg/Kg 10/03/14 16:30 11,2-Dichloroethane ND 0.100 mg/Kg 10/03/14 16:30 11,1-Dichloroethene ND 0.100 mg/Kg 10/03/14 16:30 11,2-Dichloroethene, Total ND 0.100 mg/Kg 10/03/14 16:30 11,2-Dichloropropane ND 0.100 mg/Kg 10/03/14 16:30 11,3-Dichloropropane ND 0.100 mg/Kg 10/03/14 16:30 12,2-Dichloropropane ND 0.100 mg/Kg 10/03/14 16:30 11,1-Dichloropropene ND 0.100 mg/Kg 10/03/14 16:30 1Diisopropyl ether ND 0.100 mg/Kg 10/03/14 16:30 1Ethylbenzene ND 0.250 mg/Kg 10/03/14 16:30 1Hexachlorobutadiene ND 2.50 mg/Kg 10/03/14 16:30 12-Hexanone ND 0.100 mg/Kg 10/03/14 16:30 1Isopropylbenzene ND 0.500 mg/Kg 10/03/14 16:30 1Methylene Chloride ND 2.50 mg/Kg 10/03/14 16:30 14-Methyl-2-pentanone (MIBK) ND 0.100 mg/Kg 10/03/14 16:30 1Methyl tert-butyl ether ND 0.250 mg/Kg 10/03/14 16:30 1Naphthalene ND 0.100 mg/Kg 10/03/14 16:30 1n-Butylbenzene ND 0.100 mg/Kg 10/03/14 16:30 1N-Propylbenzene ND 0.100 mg/Kg 10/03/14 16:30 1p-Isopropyltoluene ND 0.100 mg/Kg 10/03/14 16:30 1sec-Butylbenzene ND 0.100 mg/Kg 10/03/14 16:30 1Styrene ND 0.100 mg/Kg 10/03/14 16:30 1tert-Butylbenzene ND 0.100 mg/Kg 10/03/14 16:30 11,1,1,2-Tetrachloroethane ND 0.100 mg/Kg 10/03/14 16:30 11,1,2,2-Tetrachloroethane ND 0.100 mg/Kg 10/03/14 16:30 1Tetrachloroethene ND 0.100 mg/Kg 10/03/14 16:30 1Toluene ND 0.100 mg/Kg 10/03/14 16:30 1trans-1,2-Dichloroethene ND 0.100 mg/Kg 10/03/14 16:30 1trans-1,3-Dichloropropene ND 0.100 mg/Kg 10/03/14 16:30 11,2,3-Trichlorobenzene TestAmerica Nashville Page 43 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-194979/10 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194979 RL MDL 1,2,4-Trichlorobenzene ND 0.100 mg/Kg 10/03/14 16:30 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 0.100 mg/Kg 10/03/14 16:30 11,1,1-Trichloroethane ND 0.250 mg/Kg 10/03/14 16:30 11,1,2-Trichloroethane ND 0.100 mg/Kg 10/03/14 16:30 1Trichloroethene ND 0.100 mg/Kg 10/03/14 16:30 1Trichlorofluoromethane ND 0.100 mg/Kg 10/03/14 16:30 11,2,3-Trichloropropane ND 0.100 mg/Kg 10/03/14 16:30 11,2,4-Trimethylbenzene ND 0.100 mg/Kg 10/03/14 16:30 11,3,5-Trimethylbenzene ND 0.100 mg/Kg 10/03/14 16:30 1Vinyl chloride ND 0.150 mg/Kg 10/03/14 16:30 1Xylenes, Total 4-Bromofluorobenzene (Surr)104 70-130 10/03/14 16:30 1 MB MB Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery 94 10/03/14 16:30 1Dibromofluoromethane (Surr)70-130 84 10/03/14 16:30 11,2-Dichloroethane-d4 (Surr)70-130 98 10/03/14 16:30 1Toluene-d8 (Surr)70-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194979/6 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194979 Acetone 5.00 4.995 mg/Kg 100 51 -149 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Benzene 1.00 1.022 mg/Kg 102 75 -127 Bromobenzene 1.00 1.069 mg/Kg 107 75 -130 Bromochloromethane 1.00 1.009 mg/Kg 101 70 -132 Bromodichloromethane 1.00 1.092 mg/Kg 109 68 -135 Bromoform 1.00 0.9697 mg/Kg 97 36 -150 Bromomethane 1.00 0.7499 mg/Kg 75 43 -142 2-Butanone (MEK)5.00 4.348 mg/Kg 87 61 -132 Carbon disulfide 1.00 0.8988 mg/Kg 90 74 -135 Carbon tetrachloride 1.00 0.9287 mg/Kg 93 70 -141 Chlorobenzene 1.00 0.9950 mg/Kg 99 84 -125 Chlorodibromomethane 1.00 0.9468 mg/Kg 95 66 -134 Chloroethane 1.00 0.6621 mg/Kg 66 53 -144 Chloroform 1.00 0.9501 mg/Kg 95 76 -130 Chloromethane 1.00 1.324 mg/Kg 132 23 -150 2-Chlorotoluene 1.00 1.052 mg/Kg 105 78 -132 4-Chlorotoluene 1.00 1.086 mg/Kg 109 77 -138 cis-1,2-Dichloroethene 1.00 0.9758 mg/Kg 98 75 -125 cis-1,3-Dichloropropene 1.00 0.8752 mg/Kg 88 73 -148 1,2-Dibromo-3-Chloropropane 1.00 0.9479 mg/Kg 95 49 -142 1,2-Dibromoethane (EDB)1.00 1.036 mg/Kg 104 80 -135 Dibromomethane 1.00 1.044 mg/Kg 104 71 -130 1,2-Dichlorobenzene 1.00 1.032 mg/Kg 103 80 -134 1,3-Dichlorobenzene 1.00 0.9893 mg/Kg 99 79 -137 1,4-Dichlorobenzene 1.00 1.035 mg/Kg 103 77 -139 Dichlorodifluoromethane 1.00 1.178 mg/Kg 118 12 -144 TestAmerica Nashville Page 44 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194979/6 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194979 1,1-Dichloroethane 1.00 0.9824 mg/Kg 98 75 -124 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits 1,2-Dichloroethane 1.00 0.9215 mg/Kg 92 65 -134 1,1-Dichloroethene 1.00 1.046 mg/Kg 105 75 -131 1,2-Dichloroethene, Total 2.00 1.982 mg/Kg 99 75 -128 1,2-Dichloropropane 1.00 1.055 mg/Kg 106 69 -120 1,3-Dichloropropane 1.00 1.012 mg/Kg 101 78 -126 2,2-Dichloropropane 1.00 0.8769 mg/Kg 88 68 -145 1,1-Dichloropropene 1.00 1.012 mg/Kg 101 79 -127 Diisopropyl ether 1.00 0.9892 mg/Kg 99 68 -124 Ethylbenzene 1.00 0.9974 mg/Kg 100 80 -134 Hexachlorobutadiene 1.00 1.082 mg/Kg 108 65 -148 2-Hexanone 5.00 4.979 mg/Kg 100 57 -148 Isopropylbenzene 1.00 0.9518 mg/Kg 95 80 -150 Methylene Chloride 1.00 1.060 mg/Kg 106 68 -144 4-Methyl-2-pentanone (MIBK)5.00 4.727 mg/Kg 95 59 -138 Methyl tert-butyl ether 1.00 0.9171 mg/Kg 92 70 -136 Naphthalene 1.00 1.194 mg/Kg 119 69 -150 n-Butylbenzene 1.00 0.9882 mg/Kg 99 72 -152 N-Propylbenzene 1.00 1.043 mg/Kg 104 75 -137 p-Isopropyltoluene 1.00 0.9725 mg/Kg 97 77 -141 sec-Butylbenzene 1.00 0.9787 mg/Kg 98 79 -141 Styrene 1.00 0.9580 mg/Kg 96 82 -137 tert-Butylbenzene 1.00 1.021 mg/Kg 102 80 -132 1,1,1,2-Tetrachloroethane 1.00 0.9516 mg/Kg 95 80 -136 1,1,2,2-Tetrachloroethane 1.00 1.078 mg/Kg 108 66 -134 Tetrachloroethene 1.00 1.017 mg/Kg 102 78 -140 Toluene 1.00 0.9933 mg/Kg 99 80 -132 trans-1,2-Dichloroethene 1.00 1.006 mg/Kg 101 76 -128 trans-1,3-Dichloropropene 1.00 0.9018 mg/Kg 90 62 -139 1,2,3-Trichlorobenzene 1.00 1.212 mg/Kg 121 70 -150 1,2,4-Trichlorobenzene 1.00 1.109 mg/Kg 111 62 -150 1,1,1-Trichloroethane 1.00 0.9210 mg/Kg 92 72 -140 1,1,2-Trichloroethane 1.00 1.019 mg/Kg 102 78 -128 Trichloroethene 1.00 1.079 mg/Kg 108 77 -127 Trichlorofluoromethane 1.00 0.8004 mg/Kg 80 50 -140 1,2,3-Trichloropropane 1.00 1.029 mg/Kg 103 65 -139 1,2,4-Trimethylbenzene 1.00 1.013 mg/Kg 101 77 -139 1,3,5-Trimethylbenzene 1.00 1.019 mg/Kg 102 78 -138 Vinyl chloride 1.00 1.228 mg/Kg 123 47 -136 Xylenes, Total 2.00 1.921 mg/Kg 96 80 -137 4-Bromofluorobenzene (Surr)70 -130 Surrogate 106 LCS LCS Qualifier Limits%Recovery 96Dibromofluoromethane (Surr)70 -130 851,2-Dichloroethane-d4 (Surr)70 -130 96Toluene-d8 (Surr)70 -130 TestAmerica Nashville Page 45 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Matrix SpikeLab Sample ID: 490-62699-A-1-A MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 194979 Prep Batch: 195039 Acetone ND 18.7 18.18 mg/Kg 97 19 -175☼ Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Benzene ND 3.74 4.040 mg/Kg 106 31 -143☼ Bromobenzene ND 3.74 4.003 mg/Kg 107 12 -157☼ Bromochloromethane ND 3.74 4.009 mg/Kg 107 31 -141☼ Bromodichloromethane ND 3.74 4.262 mg/Kg 114 19 -148☼ Bromoform ND 3.74 4.048 E mg/Kg 108 10 -165☼ Bromomethane ND 3.74 1.914 mg/Kg 51 10 -164☼ 2-Butanone (MEK)ND 18.7 17.42 mg/Kg 93 18 -153☼ Carbon disulfide ND 3.74 3.310 mg/Kg 88 32 -144☼ Carbon tetrachloride ND 3.74 3.784 mg/Kg 101 31 -149☼ Chlorobenzene ND 3.74 3.921 mg/Kg 105 25 -152☼ Chlorodibromomethane ND 3.74 3.717 mg/Kg 99 14 -146☼ Chloroethane ND 3.74 2.464 mg/Kg 66 10 -151☼ Chloroform ND 3.74 3.654 mg/Kg 98 34 -160☼ Chloromethane ND 3.74 4.882 mg/Kg 128 10 -156☼ 2-Chlorotoluene ND 3.74 3.904 mg/Kg 104 20 -156☼ 4-Chlorotoluene ND 3.74 4.099 mg/Kg 109 17 -159☼ cis-1,2-Dichloroethene ND 3.74 3.765 mg/Kg 101 36 -139☼ cis-1,3-Dichloropropene ND 3.74 3.684 mg/Kg 98 15 -166☼ 1,2-Dibromo-3-Chloropropane ND 3.74 3.313 mg/Kg 88 10 -147☼ 1,2-Dibromoethane (EDB)ND 3.74 4.006 mg/Kg 107 18 -156☼ Dibromomethane ND 3.74 3.981 mg/Kg 106 20 -146☼ 1,2-Dichlorobenzene ND 3.74 4.035 mg/Kg 108 10 -160☼ 1,3-Dichlorobenzene ND 3.74 3.828 mg/Kg 102 10 -162☼ 1,4-Dichlorobenzene ND 3.74 3.832 mg/Kg 102 11 -159☼ Dichlorodifluoromethane ND 3.74 5.166 mg/Kg 138 10 -143☼ 1,1-Dichloroethane ND 3.74 3.969 mg/Kg 106 42 -136☼ 1,2-Dichloroethane ND 3.74 3.574 mg/Kg 95 28 -138☼ 1,1-Dichloroethene ND 3.74 4.128 mg/Kg 110 41 -143☼ 1,2-Dichloroethene, Total ND 7.49 7.745 mg/Kg 103 36 -140☼ 1,2-Dichloropropane ND 3.74 4.201 mg/Kg 112 20 -146☼ 1,3-Dichloropropane ND 3.74 3.986 mg/Kg 106 22 -148☼ 2,2-Dichloropropane ND 3.74 3.467 mg/Kg 93 33 -148☼ 1,1-Dichloropropene ND 3.74 4.183 mg/Kg 112 38 -145☼ Diisopropyl ether ND 3.74 3.993 mg/Kg 107 35 -135☼ Ethylbenzene ND 3.74 4.046 mg/Kg 108 23 -161☼ Hexachlorobutadiene ND 3.74 3.850 mg/Kg 103 10 -171☼ 2-Hexanone ND 18.7 20.20 mg/Kg 108 10 -169☼ Isopropylbenzene ND 3.74 4.038 mg/Kg 108 23 -181☼ Methylene Chloride ND 3.74 4.085 mg/Kg 109 24 -182☼ 4-Methyl-2-pentanone (MIBK)ND 18.7 18.14 mg/Kg 97 10 -168☼ Methyl tert-butyl ether ND 3.74 3.612 mg/Kg 96 28 -141☼ Naphthalene ND 3.74 3.798 mg/Kg 101 10 -176☼ n-Butylbenzene ND 3.74 4.043 mg/Kg 108 10 -175☼ N-Propylbenzene ND 3.74 4.105 mg/Kg 110 19 -162☼ p-Isopropyltoluene ND 3.74 4.002 mg/Kg 107 12 -168☼ sec-Butylbenzene ND 3.74 4.055 mg/Kg 108 12 -170☼ Styrene ND 3.74 3.985 mg/Kg 106 10 -165☼ TestAmerica Nashville Page 46 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Matrix SpikeLab Sample ID: 490-62699-A-1-A MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 194979 Prep Batch: 195039 tert-Butylbenzene ND 3.74 4.047 mg/Kg 108 20 -164☼ Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits 1,1,1,2-Tetrachloroethane ND 3.74 3.904 mg/Kg 104 19 -158☼ 1,1,2,2-Tetrachloroethane ND 3.74 3.777 mg/Kg 101 10 -162☼ Tetrachloroethene ND 3.74 4.142 mg/Kg 111 33 -161☼ Toluene ND 3.74 3.674 mg/Kg 98 30 -155☼ trans-1,2-Dichloroethene ND 3.74 3.980 mg/Kg 106 39 -140☼ trans-1,3-Dichloropropene ND 3.74 3.613 mg/Kg 97 10 -157☼ 1,2,3-Trichlorobenzene ND 3.74 3.745 mg/Kg 100 10 -157☼ 1,2,4-Trichlorobenzene ND 3.74 3.934 mg/Kg 105 10 -167☼ 1,1,1-Trichloroethane ND 3.74 3.723 mg/Kg 99 35 -149☼ 1,1,2-Trichloroethane ND 3.74 3.965 mg/Kg 106 19 -157☼ Trichloroethene ND 3.74 4.266 mg/Kg 114 27 -153☼ Trichlorofluoromethane ND 3.74 2.282 mg/Kg 61 25 -140☼ 1,2,3-Trichloropropane ND 3.74 3.576 mg/Kg 96 10 -157☼ 1,2,4-Trimethylbenzene ND 3.74 3.946 mg/Kg 105 14 -165☼ 1,3,5-Trimethylbenzene ND 3.74 3.990 mg/Kg 107 18 -164☼ Vinyl chloride ND 3.74 4.805 mg/Kg 128 20 -141☼ Xylenes, Total ND 7.49 7.888 mg/Kg 105 25 -162☼ 4-Bromofluorobenzene (Surr)70 -130 Surrogate 102 MS MS Qualifier Limits%Recovery 93Dibromofluoromethane (Surr)70 -130 851,2-Dichloroethane-d4 (Surr)70 -130 90Toluene-d8 (Surr)70 -130 Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-62699-A-1-A MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 194979 Prep Batch: 195039 Acetone ND 18.7 19.76 mg/Kg 106 19 -175 8 50 ☼ Analyte MSD MSD DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Benzene ND 3.74 3.928 mg/Kg 103 31 -143 3 50 ☼ Bromobenzene ND 3.74 4.001 mg/Kg 107 12 -157 0 50 ☼ Bromochloromethane ND 3.74 3.810 mg/Kg 102 31 -141 5 50☼ Bromodichloromethane ND 3.74 4.232 mg/Kg 113 19 -148 1 50 ☼ Bromoform ND 3.74 4.038 E mg/Kg 108 10 -165 0 50 ☼ Bromomethane ND 3.74 2.615 mg/Kg 70 10 -164 31 50 ☼ 2-Butanone (MEK)ND 18.7 17.28 mg/Kg 92 18 -153 1 50 ☼ Carbon disulfide ND 3.74 3.258 mg/Kg 87 32 -144 2 50 ☼ Carbon tetrachloride ND 3.74 3.687 mg/Kg 98 31 -149 3 50 ☼ Chlorobenzene ND 3.74 3.885 mg/Kg 104 25 -152 1 50 ☼ Chlorodibromomethane ND 3.74 3.652 mg/Kg 98 14 -146 2 50 ☼ Chloroethane ND 3.74 2.446 mg/Kg 65 10 -151 1 50☼ Chloroform ND 3.74 3.530 mg/Kg 94 34 -160 3 49 ☼ Chloromethane ND 3.74 4.925 mg/Kg 129 10 -156 1 50 ☼ 2-Chlorotoluene ND 3.74 3.982 mg/Kg 106 20 -156 2 50 ☼ 4-Chlorotoluene ND 3.74 4.103 mg/Kg 110 17 -159 0 50 ☼ cis-1,2-Dichloroethene ND 3.74 3.658 mg/Kg 98 36 -139 3 50 ☼ TestAmerica Nashville Page 47 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-62699-A-1-A MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 194979 Prep Batch: 195039 cis-1,3-Dichloropropene ND 3.74 3.599 mg/Kg 96 15 -166 2 50 ☼ Analyte MSD MSD DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD 1,2-Dibromo-3-Chloropropane ND 3.74 3.543 mg/Kg 95 10 -147 7 50☼ 1,2-Dibromoethane (EDB)ND 3.74 3.943 mg/Kg 105 18 -156 2 50 ☼ Dibromomethane ND 3.74 3.866 mg/Kg 103 20 -146 3 50 ☼ 1,2-Dichlorobenzene ND 3.74 4.021 mg/Kg 107 10 -160 0 50 ☼ 1,3-Dichlorobenzene ND 3.74 3.921 mg/Kg 105 10 -162 2 50 ☼ 1,4-Dichlorobenzene ND 3.74 3.859 mg/Kg 103 11 -159 1 50☼ Dichlorodifluoromethane ND 3.74 5.305 mg/Kg 142 10 -143 3 50 ☼ 1,1-Dichloroethane ND 3.74 3.828 mg/Kg 102 42 -136 4 50 ☼ 1,2-Dichloroethane ND 3.74 3.411 mg/Kg 91 28 -138 5 50 ☼ 1,1-Dichloroethene ND 3.74 4.086 mg/Kg 109 41 -143 1 50☼ 1,2-Dichloroethene, Total ND 7.49 7.510 mg/Kg 100 36 -140 3 41 ☼ 1,2-Dichloropropane ND 3.74 4.037 mg/Kg 108 20 -146 4 50 ☼ 1,3-Dichloropropane ND 3.74 3.956 mg/Kg 106 22 -148 1 42 ☼ 2,2-Dichloropropane ND 3.74 3.441 mg/Kg 92 33 -148 1 50 ☼ 1,1-Dichloropropene ND 3.74 4.023 mg/Kg 107 38 -145 4 50☼ Diisopropyl ether ND 3.74 3.775 mg/Kg 101 35 -135 6 45 ☼ Ethylbenzene ND 3.74 3.984 mg/Kg 106 23 -161 2 50 ☼ Hexachlorobutadiene ND 3.74 4.480 mg/Kg 120 10 -171 15 50 ☼ 2-Hexanone ND 18.7 20.02 mg/Kg 107 10 -169 1 50☼ Isopropylbenzene ND 3.74 3.999 mg/Kg 107 23 -181 1 50 ☼ Methylene Chloride ND 3.74 3.863 mg/Kg 103 24 -182 6 50 ☼ 4-Methyl-2-pentanone (MIBK)ND 18.7 18.02 mg/Kg 96 10 -168 1 50 ☼ Methyl tert-butyl ether ND 3.74 3.484 mg/Kg 93 28 -141 4 50 ☼ Naphthalene ND 3.74 4.523 mg/Kg 121 10 -176 17 50☼ n-Butylbenzene ND 3.74 4.292 mg/Kg 115 10 -175 6 50 ☼ N-Propylbenzene ND 3.74 4.074 mg/Kg 109 19 -162 1 50 ☼ p-Isopropyltoluene ND 3.74 4.151 mg/Kg 111 12 -168 4 50 ☼ sec-Butylbenzene ND 3.74 4.142 mg/Kg 111 12 -170 2 50☼ Styrene ND 3.74 3.908 mg/Kg 104 10 -165 2 50 ☼ tert-Butylbenzene ND 3.74 4.019 mg/Kg 107 20 -164 1 50 ☼ 1,1,1,2-Tetrachloroethane ND 3.74 3.760 mg/Kg 100 19 -158 4 50 ☼ 1,1,2,2-Tetrachloroethane ND 3.74 3.842 mg/Kg 103 10 -162 2 50 ☼ Tetrachloroethene ND 3.74 3.987 mg/Kg 106 33 -161 4 50☼ Toluene ND 3.74 3.624 mg/Kg 97 30 -155 1 50 ☼ trans-1,2-Dichloroethene ND 3.74 3.852 mg/Kg 103 39 -140 3 50 ☼ trans-1,3-Dichloropropene ND 3.74 3.549 mg/Kg 95 10 -157 2 50 ☼ 1,2,3-Trichlorobenzene ND 3.74 4.496 mg/Kg 120 10 -157 18 50☼ 1,2,4-Trichlorobenzene ND 3.74 4.488 mg/Kg 120 10 -167 13 50 ☼ 1,1,1-Trichloroethane ND 3.74 3.585 mg/Kg 96 35 -149 4 50 ☼ 1,1,2-Trichloroethane ND 3.74 3.929 mg/Kg 105 19 -157 1 50 ☼ Trichloroethene ND 3.74 4.147 mg/Kg 111 27 -153 3 50 ☼ Trichlorofluoromethane ND 3.74 2.288 mg/Kg 61 25 -140 0 50☼ 1,2,3-Trichloropropane ND 3.74 3.645 mg/Kg 97 10 -157 2 50 ☼ 1,2,4-Trimethylbenzene ND 3.74 3.929 mg/Kg 105 14 -165 0 50 ☼ 1,3,5-Trimethylbenzene ND 3.74 4.073 mg/Kg 109 18 -164 2 50 ☼ Vinyl chloride ND 3.74 4.883 mg/Kg 130 20 -141 2 50☼ Xylenes, Total ND 7.49 7.878 mg/Kg 105 25 -162 0 50 ☼ TestAmerica Nashville Page 48 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-62699-A-1-A MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 194979 Prep Batch: 195039 4-Bromofluorobenzene (Surr)70 -130 Surrogate 102 MSD MSD Qualifier Limits%Recovery 95Dibromofluoromethane (Surr)70 -130 831,2-Dichloroethane-d4 (Surr)70 -130 90Toluene-d8 (Surr)70 -130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 490-194221/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 194440 Prep Batch: 194221 RL MDL Acenaphthene ND 0.0670 mg/Kg 09/30/14 13:47 10/01/14 17:04 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 0.0670 mg/Kg 09/30/14 13:47 10/01/14 17:04 1Acenaphthylene ND 0.0670 mg/Kg 09/30/14 13:47 10/01/14 17:04 1Anthracene ND 0.0670 mg/Kg 09/30/14 13:47 10/01/14 17:04 1Benzo[a]anthracene ND 0.0670 mg/Kg 09/30/14 13:47 10/01/14 17:04 1Benzo[a]pyrene ND 0.0670 mg/Kg 09/30/14 13:47 10/01/14 17:04 1Benzo[b]fluoranthene ND 0.0670 mg/Kg 09/30/14 13:47 10/01/14 17:04 1Benzo[g,h,i]perylene ND 0.0670 mg/Kg 09/30/14 13:47 10/01/14 17:04 1Benzo[k]fluoranthene ND 0.0670 mg/Kg 09/30/14 13:47 10/01/14 17:04 1Chrysene ND 0.0670 mg/Kg 09/30/14 13:47 10/01/14 17:04 1Dibenz(a,h)anthracene ND 0.0670 mg/Kg 09/30/14 13:47 10/01/14 17:04 1Fluoranthene ND 0.0670 mg/Kg 09/30/14 13:47 10/01/14 17:04 1Fluorene ND 0.0670 mg/Kg 09/30/14 13:47 10/01/14 17:04 1Indeno[1,2,3-cd]pyrene ND 0.0670 mg/Kg 09/30/14 13:47 10/01/14 17:04 1Naphthalene ND 0.0670 mg/Kg 09/30/14 13:47 10/01/14 17:04 1Phenanthrene ND 0.0670 mg/Kg 09/30/14 13:47 10/01/14 17:04 1Pyrene 2-Fluorobiphenyl (Surr)49 29-120 10/01/14 17:04 1 MB MB Surrogate 09/30/14 13:47 Dil FacPrepared AnalyzedQualifier Limits%Recovery 50 09/30/14 13:47 10/01/14 17:04 1Nitrobenzene-d5 (Surr)27-120 55 09/30/14 13:47 10/01/14 17:04 1Terphenyl-d14 (Surr)13-120 Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194221/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 194440 Prep Batch: 194221 Acenaphthene 1.67 1.408 mg/Kg 84 36 -120 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Acenaphthylene 1.67 1.434 mg/Kg 86 38 -120 Anthracene 1.67 1.427 mg/Kg 86 46 -124 Benzo[a]anthracene 1.67 1.466 mg/Kg 88 45 -120 Benzo[a]pyrene 1.67 1.465 mg/Kg 88 45 -120 Benzo[b]fluoranthene 1.67 1.495 mg/Kg 90 42 -120 Benzo[g,h,i]perylene 1.67 1.402 mg/Kg 84 38 -120 Benzo[k]fluoranthene 1.67 1.367 mg/Kg 82 42 -120 TestAmerica Nashville Page 49 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194221/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 194440 Prep Batch: 194221 Chrysene 1.67 1.396 mg/Kg 84 43 -120 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Dibenz(a,h)anthracene 1.67 1.442 mg/Kg 87 32 -128 Fluoranthene 1.67 1.456 mg/Kg 87 46 -120 Fluorene 1.67 1.493 mg/Kg 90 42 -120 Indeno[1,2,3-cd]pyrene 1.67 1.426 mg/Kg 86 41 -121 Naphthalene 1.67 1.352 mg/Kg 81 32 -120 Phenanthrene 1.67 1.400 mg/Kg 84 45 -120 Pyrene 1.67 1.390 mg/Kg 83 43 -120 2-Fluorobiphenyl (Surr)29 -120 Surrogate 73 LCS LCS Qualifier Limits%Recovery 74Nitrobenzene-d5 (Surr)27 -120 81Terphenyl-d14 (Surr)13 -120 Client Sample ID: Method BlankLab Sample ID: MB 490-194350/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 194448 Prep Batch: 194350 RL MDL Acenaphthene ND 2.00 ug/L 10/01/14 06:43 10/01/14 15:24 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 2.00 ug/L 10/01/14 06:43 10/01/14 15:24 1Acenaphthylene ND 2.00 ug/L 10/01/14 06:43 10/01/14 15:24 1Anthracene ND 2.00 ug/L 10/01/14 06:43 10/01/14 15:24 1Benzo[a]anthracene ND 2.00 ug/L 10/01/14 06:43 10/01/14 15:24 1Benzo[a]pyrene ND 2.00 ug/L 10/01/14 06:43 10/01/14 15:24 1Benzo[b]fluoranthene ND 2.00 ug/L 10/01/14 06:43 10/01/14 15:24 1Benzo[g,h,i]perylene ND 2.00 ug/L 10/01/14 06:43 10/01/14 15:24 1Benzo[k]fluoranthene ND 2.00 ug/L 10/01/14 06:43 10/01/14 15:24 1Chrysene ND 2.00 ug/L 10/01/14 06:43 10/01/14 15:24 1Dibenz(a,h)anthracene ND 2.00 ug/L 10/01/14 06:43 10/01/14 15:24 1Fluoranthene ND 2.00 ug/L 10/01/14 06:43 10/01/14 15:24 1Fluorene ND 2.00 ug/L 10/01/14 06:43 10/01/14 15:24 1Indeno[1,2,3-cd]pyrene ND 2.00 ug/L 10/01/14 06:43 10/01/14 15:24 1Naphthalene ND 2.00 ug/L 10/01/14 06:43 10/01/14 15:24 1Phenanthrene ND 2.00 ug/L 10/01/14 06:43 10/01/14 15:24 1Pyrene 2-Fluorobiphenyl (Surr)71 29-120 10/01/14 15:24 1 MB MB Surrogate 10/01/14 06:43 Dil FacPrepared AnalyzedQualifier Limits%Recovery 72 10/01/14 06:43 10/01/14 15:24 1Nitrobenzene-d5 (Surr)27-120 91 10/01/14 06:43 10/01/14 15:24 1Terphenyl-d14 (Surr)13-120 Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194350/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 194448 Prep Batch: 194350 Acenaphthene 40.0 27.27 ug/L 68 46 -120 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Acenaphthylene 40.0 27.19 ug/L 68 48 -120 TestAmerica Nashville Page 50 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194350/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 194448 Prep Batch: 194350 Anthracene 40.0 31.48 ug/L 79 58 -130 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Benzo[a]anthracene 40.0 32.08 ug/L 80 57 -120 Benzo[a]pyrene 40.0 32.30 ug/L 81 57 -124 Benzo[b]fluoranthene 40.0 34.53 ug/L 86 51 -125 Benzo[g,h,i]perylene 40.0 33.36 ug/L 83 51 -123 Benzo[k]fluoranthene 40.0 28.92 ug/L 72 51 -120 Chrysene 40.0 30.63 ug/L 77 55 -120 Dibenz(a,h)anthracene 40.0 33.44 ug/L 84 50 -125 Fluoranthene 40.0 32.85 ug/L 82 56 -120 Fluorene 40.0 30.85 ug/L 77 52 -120 Indeno[1,2,3-cd]pyrene 40.0 32.76 ug/L 82 54 -125 Naphthalene 40.0 19.15 ug/L 48 37 -120 Phenanthrene 40.0 30.37 ug/L 76 56 -120 Pyrene 40.0 30.33 ug/L 76 53 -129 2-Fluorobiphenyl (Surr)29 -120 Surrogate 57 LCS LCS Qualifier Limits%Recovery 46Nitrobenzene-d5 (Surr)27 -120 73Terphenyl-d14 (Surr)13 -120 Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) Client Sample ID: Matrix SpikeLab Sample ID: 490-62402-B-1-B MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 194274 Prep Batch: 193684 GRO (C6-C10)ND 747 651.9 mg/Kg 87 56 -130☼ Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits a,a,a-Trifluorotoluene 50 -150 Surrogate 115 MS MS Qualifier Limits%Recovery Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-62402-B-1-C MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 194274 Prep Batch: 193684 GRO (C6-C10)ND 747 793.4 mg/Kg 106 56 -130 20 21 ☼ Analyte MSD MSD DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD a,a,a-Trifluorotoluene 50 -150 Surrogate 129 MSD MSD Qualifier Limits%Recovery TestAmerica Nashville Page 51 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-194274/6 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194274 RL MDL GRO (C6-C10)ND 5.00 mg/Kg 09/30/14 15:12 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier a,a,a-Trifluorotoluene 109 50-150 09/30/14 15:12 1 MB MB Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194274/36 Matrix: Solid Prep Type: Total/NA Analysis Batch: 194274 GRO (C6-C10)10.0 10.51 mg/Kg 105 70 -130 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits a,a,a-Trifluorotoluene 50 -150 Surrogate 116 LCS LCS Qualifier Limits%Recovery Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) Client Sample ID: Method BlankLab Sample ID: MB 490-194115/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 194607 Prep Batch: 194115 RL MDL Diesel Range Organics [C10-C28]ND 5.00 mg/Kg 09/30/14 10:14 10/01/14 17:13 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier o-Terphenyl (Surr)73 50-150 10/01/14 17:13 1 MB MB Surrogate 09/30/14 10:14 Dil FacPrepared AnalyzedQualifier Limits%Recovery Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194115/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 194607 Prep Batch: 194115 Diesel Range Organics [C10-C28] 40.0 27.64 mg/Kg 69 54 -130 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits o-Terphenyl (Surr)50 -150 Surrogate 67 LCS LCS Qualifier Limits%Recovery Client Sample ID: Matrix SpikeLab Sample ID: 490-62388-A-1-B MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 194607 Prep Batch: 194115 Diesel Range Organics [C10-C28] ND 49.3 32.61 mg/Kg 66 10 -142☼ Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits TestAmerica Nashville Page 52 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) (Continued) Client Sample ID: Matrix SpikeLab Sample ID: 490-62388-A-1-B MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 194607 Prep Batch: 194115 o-Terphenyl (Surr)50 -150 Surrogate 65 MS MS Qualifier Limits%Recovery Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-62388-A-1-C MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 194607 Prep Batch: 194115 Diesel Range Organics [C10-C28] ND 48.4 39.96 mg/Kg 82 10 -142 20 47 ☼ Analyte MSD MSD DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD o-Terphenyl (Surr)50 -150 Surrogate 82 MSD MSD Qualifier Limits%Recovery Method: 6010C - Metals (ICP) Client Sample ID: Method BlankLab Sample ID: MB 490-193952/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 194369 Prep Batch: 193952 RL MDL Antimony ND 9.58 mg/Kg 09/29/14 13:45 09/30/14 15:26 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 1.92 mg/Kg 09/29/14 13:45 09/30/14 15:26 1Arsenic ND 0.958 mg/Kg 09/29/14 13:45 09/30/14 15:26 1Beryllium ND 0.958 mg/Kg 09/29/14 13:45 09/30/14 15:26 1Cadmium ND 0.958 mg/Kg 09/29/14 13:45 09/30/14 15:26 1Chromium ND 1.92 mg/Kg 09/29/14 13:45 09/30/14 15:26 1Copper ND 0.958 mg/Kg 09/29/14 13:45 09/30/14 15:26 1Lead ND 2.87 mg/Kg 09/29/14 13:45 09/30/14 15:26 1Manganese ND 1.92 mg/Kg 09/29/14 13:45 09/30/14 15:26 1Nickel ND 1.92 mg/Kg 09/29/14 13:45 09/30/14 15:26 1Selenium ND 0.958 mg/Kg 09/29/14 13:45 09/30/14 15:26 1Silver ND 1.92 mg/Kg 09/29/14 13:45 09/30/14 15:26 1Thallium ND 9.58 mg/Kg 09/29/14 13:45 09/30/14 15:26 1Zinc Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-193952/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 194369 Prep Batch: 193952 Antimony 39.8 38.88 mg/Kg 98 80 -120 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Arsenic 19.9 17.21 mg/Kg 86 80 -120 Beryllium 19.9 18.80 mg/Kg 94 80 -120 Cadmium 19.9 18.57 mg/Kg 93 80 -120 Chromium 79.7 74.72 mg/Kg 94 80 -120 Copper 99.6 93.03 mg/Kg 93 80 -120 Lead 19.9 18.67 mg/Kg 94 80 -120 Manganese 199 192.7 mg/Kg 97 80 -120 TestAmerica Nashville Page 53 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 6010C - Metals (ICP) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-193952/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 194369 Prep Batch: 193952 Nickel 199 184.4 mg/Kg 93 80 -120 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Selenium 19.9 17.55 mg/Kg 88 80 -120 Silver 19.9 20.78 mg/Kg 104 80 -120 Thallium 19.9 19.82 mg/Kg 99 80 -120 Zinc 199 180.8 mg/Kg 91 80 -120 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-193952/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 194369 Prep Batch: 193952 Antimony 39.8 39.24 mg/Kg 99 80 -120 1 20 Analyte LCSD LCSD DUnitResult Qualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Arsenic 19.9 17.61 mg/Kg 88 80 -120 2 20 Beryllium 19.9 19.10 mg/Kg 96 80 -120 2 20 Cadmium 19.9 18.78 mg/Kg 94 80 -120 1 20 Chromium 79.7 75.70 mg/Kg 95 80 -120 1 20 Copper 99.6 93.96 mg/Kg 94 80 -120 1 20 Lead 19.9 18.75 mg/Kg 94 80 -120 0 20 Manganese 199 194.2 mg/Kg 97 80 -120 1 20 Nickel 199 186.3 mg/Kg 94 80 -120 1 20 Selenium 19.9 17.87 mg/Kg 90 80 -120 2 20 Silver 19.9 21.10 mg/Kg 106 80 -120 2 20 Thallium 19.9 20.04 mg/Kg 101 80 -120 1 20 Zinc 199 183.0 mg/Kg 92 80 -120 1 20 Client Sample ID: Matrix SpikeLab Sample ID: 460-83377-C-1-B MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 194369 Prep Batch: 193952 Antimony ND 41.3 41.55 mg/Kg 100 75 -125☼ Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Arsenic ND 20.7 19.85 mg/Kg 96 75 -125☼ Beryllium ND 20.7 20.24 mg/Kg 98 75 -125☼ Cadmium ND 20.7 19.72 mg/Kg 92 75 -125☼ Chromium 34.6 82.7 112.0 mg/Kg 94 75 -125☼ Copper 534 103 649.2 4 mg/Kg 111 75 -125☼ Lead 23.4 20.7 43.46 mg/Kg 97 75 -125☼ Manganese 1780 207 1978 4 mg/Kg 96 75 -125☼ Nickel 8.78 207 201.3 mg/Kg 93 75 -125☼ Selenium 4.57 20.7 23.82 mg/Kg 93 75 -125☼ Silver 3.25 20.7 23.44 mg/Kg 98 75 -125☼ Thallium ND 20.7 19.81 mg/Kg 96 75 -125☼ Zinc 511 207 697.1 mg/Kg 90 75 -125☼ TestAmerica Nashville Page 54 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 6010C - Metals (ICP) (Continued) Client Sample ID: Matrix Spike DuplicateLab Sample ID: 460-83377-C-1-C MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 194369 Prep Batch: 193952 Antimony ND 42.1 40.14 mg/Kg 95 75 -125 3 20 ☼ Analyte MSD MSD DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Arsenic ND 21.0 18.74 mg/Kg 89 75 -125 6 20 ☼ Beryllium ND 21.0 20.30 mg/Kg 96 75 -125 0 20☼ Cadmium ND 21.0 19.73 mg/Kg 91 75 -125 0 20 ☼ Chromium 34.6 84.2 112.6 mg/Kg 93 75 -125 1 20 ☼ Copper 534 105 638.3 4 mg/Kg 99 75 -125 2 20 ☼ Lead 23.4 21.0 43.13 mg/Kg 94 75 -125 1 20 ☼ Manganese 1780 210 1945 4 mg/Kg 79 75 -125 2 20☼ Nickel 8.78 210 201.1 mg/Kg 91 75 -125 0 20 ☼ Selenium 4.57 21.0 23.60 mg/Kg 90 75 -125 1 20 ☼ Silver 3.25 21.0 23.94 mg/Kg 98 75 -125 2 20 ☼ Thallium ND 21.0 18.43 mg/Kg 88 75 -125 7 20☼ Zinc 511 210 686.9 mg/Kg 84 75 -125 1 20 ☼ Client Sample ID: Method BlankLab Sample ID: MB 490-194105/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 195008 Prep Batch: 194105 RL MDL Antimony ND 0.0100 mg/L 09/30/14 10:07 10/02/14 16:31 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 0.0100 mg/L 09/30/14 10:07 10/02/14 16:31 1Arsenic ND 0.00400 mg/L 09/30/14 10:07 10/02/14 16:31 1Beryllium ND 0.00100 mg/L 09/30/14 10:07 10/02/14 16:31 1Cadmium ND 0.00500 mg/L 09/30/14 10:07 10/02/14 16:31 1Chromium ND 0.0100 mg/L 09/30/14 10:07 10/02/14 16:31 1Copper ND 0.0150 mg/L 09/30/14 10:07 10/02/14 16:31 1Manganese ND 0.0100 mg/L 09/30/14 10:07 10/02/14 16:31 1Nickel ND 0.0100 mg/L 09/30/14 10:07 10/02/14 16:31 1Selenium ND 0.00500 mg/L 09/30/14 10:07 10/02/14 16:31 1Silver ND 0.0100 mg/L 09/30/14 10:07 10/02/14 16:31 1Thallium ND 0.0500 mg/L 09/30/14 10:07 10/02/14 16:31 1Zinc Client Sample ID: Method BlankLab Sample ID: MB 490-194105/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 195573 Prep Batch: 194105 RL MDL Antimony ND 0.0100 mg/L 09/30/14 10:07 10/03/14 16:02 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194105/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 195008 Prep Batch: 194105 Antimony 0.100 0.1117 mg/L 112 80 -120 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Arsenic 0.0500 0.04940 mg/L 99 80 -120 Beryllium 0.0500 0.05210 mg/L 104 80 -120 Cadmium 0.0500 0.05080 mg/L 102 80 -120 Chromium 0.200 0.2051 mg/L 103 80 -120 TestAmerica Nashville Page 55 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 6010C - Metals (ICP) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194105/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 195008 Prep Batch: 194105 Copper 0.250 0.2524 mg/L 101 80 -120 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Manganese 0.500 0.5263 mg/L 105 80 -120 Nickel 0.500 0.5177 mg/L 104 80 -120 Selenium 0.0500 0.05220 mg/L 104 80 -120 Silver 0.0500 0.05050 mg/L 101 80 -120 Thallium 0.0500 0.04980 mg/L 100 80 -120 Zinc 0.500 0.4993 mg/L 100 80 -120 Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194105/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 195573 Prep Batch: 194105 Lead 0.0500 0.05260 mg/L 105 80 -120 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-194105/3-A Matrix: Water Prep Type: Total/NA Analysis Batch: 195008 Prep Batch: 194105 Antimony 0.100 0.1103 mg/L 110 80 -120 1 20 Analyte LCSD LCSD DUnitResult Qualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Arsenic 0.0500 0.04680 mg/L 94 80 -120 5 20 Beryllium 0.0500 0.05170 mg/L 103 80 -120 1 20 Cadmium 0.0500 0.04970 mg/L 99 80 -120 2 20 Chromium 0.200 0.1999 mg/L 100 80 -120 3 20 Copper 0.250 0.2532 mg/L 101 80 -120 0 20 Manganese 0.500 0.5171 mg/L 103 80 -120 2 20 Nickel 0.500 0.5100 mg/L 102 80 -120 1 20 Selenium 0.0500 0.04960 mg/L 99 80 -120 5 20 Silver 0.0500 0.04920 mg/L 98 80 -120 3 20 Thallium 0.0500 0.04930 mg/L 99 80 -120 1 20 Zinc 0.500 0.4917 mg/L 98 80 -120 2 20 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-194105/3-A Matrix: Water Prep Type: Total/NA Analysis Batch: 195573 Prep Batch: 194105 Lead 0.0500 0.05060 mg/L 101 80 -120 4 20 Analyte LCSD LCSD DUnitResult Qualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Client Sample ID: Matrix SpikeLab Sample ID: 490-62417-G-1-B MS Matrix: Water Prep Type: Total/NA Analysis Batch: 195008 Prep Batch: 194105 Antimony ND 0.100 0.1070 mg/L 107 75 -125 Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Arsenic 0.0737 0.0500 0.1239 mg/L 100 75 -125 Beryllium ND 0.0500 0.05090 mg/L 102 75 -125 Cadmium ND 0.0500 0.05020 mg/L 100 75 -125 TestAmerica Nashville Page 56 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 6010C - Metals (ICP) (Continued) Client Sample ID: Matrix SpikeLab Sample ID: 490-62417-G-1-B MS Matrix: Water Prep Type: Total/NA Analysis Batch: 195008 Prep Batch: 194105 Chromium ND 0.200 0.1975 mg/L 99 75 -125 Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Copper ND 0.250 0.2496 mg/L 100 75 -125 Manganese 1.62 ^0.500 2.128 mg/L 101 75 -125 Nickel ND 0.500 0.4996 mg/L 100 75 -125 Selenium ND 0.0500 0.05170 mg/L 103 75 -125 Silver ND 0.0500 0.05190 mg/L 104 75 -125 Thallium ND 0.0500 0.05240 mg/L 105 75 -125 Zinc 0.166 0.500 0.6583 mg/L 99 75 -125 Client Sample ID: Matrix SpikeLab Sample ID: 490-62417-G-1-B MS Matrix: Water Prep Type: Total/NA Analysis Batch: 195573 Prep Batch: 194105 Lead 0.00670 0.0500 0.06210 mg/L 111 75 -125 Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-62417-G-1-C MSD Matrix: Water Prep Type: Total/NA Analysis Batch: 195008 Prep Batch: 194105 Antimony ND 0.100 0.1075 mg/L 108 75 -125 0 20 Analyte MSD MSD DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Arsenic 0.0737 0.0500 0.1236 mg/L 100 75 -125 0 20 Beryllium ND 0.0500 0.05050 mg/L 101 75 -125 1 20 Cadmium ND 0.0500 0.04880 mg/L 98 75 -125 3 20 Chromium ND 0.200 0.1909 mg/L 95 75 -125 3 20 Copper ND 0.250 0.2438 mg/L 98 75 -125 2 20 Manganese 1.62 ^0.500 2.055 mg/L 87 75 -125 3 20 Nickel ND 0.500 0.4846 mg/L 97 75 -125 3 20 Selenium ND 0.0500 0.05270 mg/L 105 75 -125 2 20 Silver ND 0.0500 0.05040 mg/L 101 75 -125 3 20 Thallium ND 0.0500 0.05170 mg/L 103 75 -125 1 20 Zinc 0.166 0.500 0.6406 mg/L 95 75 -125 3 20 Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-62417-G-1-C MSD Matrix: Water Prep Type: Total/NA Analysis Batch: 195573 Prep Batch: 194105 Lead 0.00670 0.0500 0.05900 mg/L 105 75 -125 5 20 Analyte MSD MSD DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Method: 7470A - Mercury (CVAA) Client Sample ID: Method BlankLab Sample ID: MB 490-194352/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 194570 Prep Batch: 194352 RL MDL Mercury ND 0.000200 mg/L 10/01/14 06:48 10/01/14 13:25 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier TestAmerica Nashville Page 57 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 7470A - Mercury (CVAA) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194352/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 194570 Prep Batch: 194352 Mercury 0.00100 0.0008716 mg/L 87 80 -120 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Client Sample ID: Matrix SpikeLab Sample ID: 490-62129-D-3-C MS Matrix: Water Prep Type: Total/NA Analysis Batch: 194570 Prep Batch: 194352 Mercury ND 0.00100 0.0005691 F1 mg/L 57 75 -125 Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-62129-D-3-D MSD Matrix: Water Prep Type: Total/NA Analysis Batch: 194570 Prep Batch: 194352 Mercury ND 0.00100 0.0005255 F1 mg/L 53 75 -125 8 20 Analyte MSD MSD DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Client Sample ID: Method BlankLab Sample ID: MB 490-194384/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 194477 Prep Batch: 194384 RL MDL Mercury ND 0.100 mg/Kg 10/01/14 08:22 10/01/14 10:12 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194384/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 194477 Prep Batch: 194384 Mercury 0.166 0.1407 mg/Kg 85 80 -120 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-194384/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 194477 Prep Batch: 194384 Mercury 0.162 0.1383 mg/Kg 85 80 -120 2 20 Analyte LCSD LCSD DUnitResult Qualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Client Sample ID: Matrix SpikeLab Sample ID: 490-62475-B-1-E MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 194477 Prep Batch: 194384 Mercury ND 0.192 0.1590 mg/Kg 83 80 -120☼ Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits TestAmerica Nashville Page 58 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method: 7471B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) (Continued) Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-62475-B-1-F MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 194477 Prep Batch: 194384 Mercury ND 0.190 0.1496 F1 mg/Kg 79 80 -120 6 20 ☼ Analyte MSD MSD DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Client Sample ID: Method BlankLab Sample ID: MB 490-194540/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 194816 Prep Batch: 194540 RL MDL Mercury ND 0.101 mg/Kg 10/01/14 14:28 10/02/14 12:02 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-194540/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 194816 Prep Batch: 194540 Mercury 0.160 0.1642 mg/Kg 102 80 -120 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-194540/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 194816 Prep Batch: 194540 Mercury 0.161 0.1597 mg/Kg 99 80 -120 3 20 Analyte LCSD LCSD DUnitResult Qualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Client Sample ID: Matrix SpikeLab Sample ID: 490-62384-A-1-C MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 194816 Prep Batch: 194540 Mercury ND 0.168 0.1876 mg/Kg 112 80 -120 Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-62384-A-1-D MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 194816 Prep Batch: 194540 Mercury ND 0.167 0.1849 mg/Kg 111 80 -120 1 20 Analyte MSD MSD DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Method: Moisture - Percent Moisture Client Sample ID: DuplicateLab Sample ID: 490-62388-A-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 193935 Percent Solids 80 77 %3 20 Analyte DU DU DUnitResult Qualifier Sample Result Sample Qualifier LimitRPD RPD TestAmerica Nashville Page 59 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC GC/MS VOA Prep Batch: 193627 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035490-62390-1 SB-1 (5-7)Total/NA Prep Batch: 193628 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035490-62390-1 SB-1 (5-7)Total/NA Solid 5035490-62390-2 SB-2 (1-3)Total/NA Solid 5035490-62390-3 SB-3 (1-2)Total/NA Solid 5035490-62390-4 SB-4 (1-2)Total/NA Analysis Batch: 194305 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 8260B490-62333-B-11 MS Matrix Spike Total/NA Water 8260B490-62333-C-11 MSD Matrix Spike Duplicate Total/NA Water 8260B490-62390-7 TMW-1 Total/NA Water 8260B490-62390-8 TMW-2 Total/NA Water 8260BLCS 490-194305/3 Lab Control Sample Total/NA Water 8260BLCSD 490-194305/4 Lab Control Sample Dup Total/NA Water 8260BMB 490-194305/8 Method Blank Total/NA Analysis Batch: 194478 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260B 193628490-62390-1 SB-1 (5-7)Total/NA Solid 8260B 193628490-62390-2 SB-2 (1-3)Total/NA Solid 8260B 193628490-62390-3 SB-3 (1-2)Total/NA Solid 8260BLCS 490-194478/4 Lab Control Sample Total/NA Solid 8260BLCSD 490-194478/5 Lab Control Sample Dup Total/NA Solid 8260BMB 490-194478/8 Method Blank Total/NA Analysis Batch: 194702 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260B 193628490-62390-4 SB-4 (1-2)Total/NA Solid 8260BLCS 490-194702/18 Lab Control Sample Total/NA Solid 8260BLCSD 490-194702/19 Lab Control Sample Dup Total/NA Solid 8260BMB 490-194702/8 Method Blank Total/NA Analysis Batch: 194979 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260B 193627490-62390-1 SB-1 (5-7)Total/NA Solid 8260B 195039490-62699-A-1-A MS Matrix Spike Total/NA Solid 8260B 195039490-62699-A-1-A MSD Matrix Spike Duplicate Total/NA Solid 8260BLCS 490-194979/6 Lab Control Sample Total/NA Solid 8260BMB 490-194979/10 Method Blank Total/NA Prep Batch: 195039 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035490-62699-A-1-A MS Matrix Spike Total/NA Solid 5035490-62699-A-1-A MSD Matrix Spike Duplicate Total/NA TestAmerica Nashville Page 60 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC GC/MS Semi VOA Prep Batch: 194221 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3550C490-62390-1 SB-1 (5-7)Total/NA Solid 3550C490-62390-2 SB-2 (1-3)Total/NA Solid 3550CLCS 490-194221/2-A Lab Control Sample Total/NA Solid 3550CMB 490-194221/1-A Method Blank Total/NA Prep Batch: 194350 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 3510C490-62390-7 TMW-1 Total/NA Water 3510C490-62390-8 TMW-2 Total/NA Water 3510CLCS 490-194350/2-A Lab Control Sample Total/NA Water 3510CMB 490-194350/1-A Method Blank Total/NA Analysis Batch: 194440 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270D 194221490-62390-1 SB-1 (5-7)Total/NA Solid 8270D 194221490-62390-2 SB-2 (1-3)Total/NA Solid 8270D 194221LCS 490-194221/2-A Lab Control Sample Total/NA Solid 8270D 194221MB 490-194221/1-A Method Blank Total/NA Analysis Batch: 194448 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 8270D 194350490-62390-7 TMW-1 Total/NA Water 8270D 194350490-62390-8 TMW-2 Total/NA Water 8270D 194350LCS 490-194350/2-A Lab Control Sample Total/NA Water 8270D 194350MB 490-194350/1-A Method Blank Total/NA GC VOA Prep Batch: 193627 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035490-62390-5 SB-5 (1-2)Total/NA Solid 5035490-62390-6 SB-6 (1-2)Total/NA Prep Batch: 193684 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035490-62402-B-1-B MS Matrix Spike Total/NA Solid 5035490-62402-B-1-C MSD Matrix Spike Duplicate Total/NA Analysis Batch: 194274 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8015C 193627490-62390-5 SB-5 (1-2)Total/NA Solid 8015C 193627490-62390-6 SB-6 (1-2)Total/NA Solid 8015C 193684490-62402-B-1-B MS Matrix Spike Total/NA Solid 8015C 193684490-62402-B-1-C MSD Matrix Spike Duplicate Total/NA Solid 8015CLCS 490-194274/36 Lab Control Sample Total/NA Solid 8015CMB 490-194274/6 Method Blank Total/NA TestAmerica Nashville Page 61 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC GC Semi VOA Prep Batch: 194115 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3550C490-62388-A-1-B MS Matrix Spike Total/NA Solid 3550C490-62388-A-1-C MSD Matrix Spike Duplicate Total/NA Solid 3550C490-62390-5 SB-5 (1-2)Total/NA Solid 3550C490-62390-6 SB-6 (1-2)Total/NA Solid 3550CLCS 490-194115/2-A Lab Control Sample Total/NA Solid 3550CMB 490-194115/1-A Method Blank Total/NA Analysis Batch: 194607 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8015C 194115490-62388-A-1-B MS Matrix Spike Total/NA Solid 8015C 194115490-62388-A-1-C MSD Matrix Spike Duplicate Total/NA Solid 8015C 194115490-62390-5 SB-5 (1-2)Total/NA Solid 8015C 194115490-62390-6 SB-6 (1-2)Total/NA Solid 8015C 194115LCS 490-194115/2-A Lab Control Sample Total/NA Solid 8015C 194115MB 490-194115/1-A Method Blank Total/NA Metals Prep Batch: 193952 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3051A460-83377-C-1-B MS Matrix Spike Total/NA Solid 3051A460-83377-C-1-C MSD Matrix Spike Duplicate Total/NA Solid 3051A490-62390-1 SB-1 (5-7)Total/NA Solid 3051A490-62390-2 SB-2 (1-3)Total/NA Solid 3051A490-62390-3 SB-3 (1-2)Total/NA Solid 3051A490-62390-4 SB-4 (1-2)Total/NA Solid 3051A490-62390-9 Background (1-2)Total/NA Solid 3051ALCS 490-193952/2-A Lab Control Sample Total/NA Solid 3051ALCSD 490-193952/3-A Lab Control Sample Dup Total/NA Solid 3051AMB 490-193952/1-A Method Blank Total/NA Prep Batch: 194105 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 3010A490-62390-7 TMW-1 Total/NA Water 3010A490-62390-8 TMW-2 Total/NA Water 3010A490-62417-G-1-B MS Matrix Spike Total/NA Water 3010A490-62417-G-1-C MSD Matrix Spike Duplicate Total/NA Water 3010ALCS 490-194105/2-A Lab Control Sample Total/NA Water 3010ALCSD 490-194105/3-A Lab Control Sample Dup Total/NA Water 3010AMB 490-194105/1-A Method Blank Total/NA Prep Batch: 194352 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 7470A490-62129-D-3-C MS Matrix Spike Total/NA Water 7470A490-62129-D-3-D MSD Matrix Spike Duplicate Total/NA Water 7470A490-62390-7 TMW-1 Total/NA Water 7470A490-62390-8 TMW-2 Total/NA Water 7470ALCS 490-194352/2-A Lab Control Sample Total/NA Water 7470AMB 490-194352/1-A Method Blank Total/NA TestAmerica Nashville Page 62 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Metals (Continued) Analysis Batch: 194369 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6010C 193952460-83377-C-1-B MS Matrix Spike Total/NA Solid 6010C 193952460-83377-C-1-C MSD Matrix Spike Duplicate Total/NA Solid 6010C 193952490-62390-1 SB-1 (5-7)Total/NA Solid 6010C 193952490-62390-2 SB-2 (1-3)Total/NA Solid 6010C 193952490-62390-3 SB-3 (1-2)Total/NA Solid 6010C 193952490-62390-4 SB-4 (1-2)Total/NA Solid 6010C 193952490-62390-9 Background (1-2)Total/NA Solid 6010C 193952LCS 490-193952/2-A Lab Control Sample Total/NA Solid 6010C 193952LCSD 490-193952/3-A Lab Control Sample Dup Total/NA Solid 6010C 193952MB 490-193952/1-A Method Blank Total/NA Prep Batch: 194384 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 7471B490-62390-1 SB-1 (5-7)Total/NA Solid 7471B490-62390-2 SB-2 (1-3)Total/NA Solid 7471B490-62390-3 SB-3 (1-2)Total/NA Solid 7471B490-62390-4 SB-4 (1-2)Total/NA Solid 7471B490-62475-B-1-E MS Matrix Spike Total/NA Solid 7471B490-62475-B-1-F MSD Matrix Spike Duplicate Total/NA Solid 7471BLCS 490-194384/2-A Lab Control Sample Total/NA Solid 7471BLCSD 490-194384/3-A Lab Control Sample Dup Total/NA Solid 7471BMB 490-194384/1-A Method Blank Total/NA Analysis Batch: 194477 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 7471B 194384490-62390-1 SB-1 (5-7)Total/NA Solid 7471B 194384490-62390-2 SB-2 (1-3)Total/NA Solid 7471B 194384490-62390-3 SB-3 (1-2)Total/NA Solid 7471B 194384490-62390-4 SB-4 (1-2)Total/NA Solid 7471B 194384490-62475-B-1-E MS Matrix Spike Total/NA Solid 7471B 194384490-62475-B-1-F MSD Matrix Spike Duplicate Total/NA Solid 7471B 194384LCS 490-194384/2-A Lab Control Sample Total/NA Solid 7471B 194384LCSD 490-194384/3-A Lab Control Sample Dup Total/NA Solid 7471B 194384MB 490-194384/1-A Method Blank Total/NA Prep Batch: 194540 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 7471B490-62384-A-1-C MS Matrix Spike Total/NA Solid 7471B490-62384-A-1-D MSD Matrix Spike Duplicate Total/NA Solid 7471B490-62390-9 Background (1-2)Total/NA Solid 7471BLCS 490-194540/2-A Lab Control Sample Total/NA Solid 7471BLCSD 490-194540/3-A Lab Control Sample Dup Total/NA Solid 7471BMB 490-194540/1-A Method Blank Total/NA Analysis Batch: 194570 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 7470A 194352490-62129-D-3-C MS Matrix Spike Total/NA Water 7470A 194352490-62129-D-3-D MSD Matrix Spike Duplicate Total/NA Water 7470A 194352490-62390-7 TMW-1 Total/NA Water 7470A 194352490-62390-8 TMW-2 Total/NA Water 7470A 194352LCS 490-194352/2-A Lab Control Sample Total/NA TestAmerica Nashville Page 63 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Metals (Continued) Analysis Batch: 194570 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 7470A 194352MB 490-194352/1-A Method Blank Total/NA Analysis Batch: 194816 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 7471B 194540490-62384-A-1-C MS Matrix Spike Total/NA Solid 7471B 194540490-62384-A-1-D MSD Matrix Spike Duplicate Total/NA Solid 7471B 194540490-62390-9 Background (1-2)Total/NA Solid 7471B 194540LCS 490-194540/2-A Lab Control Sample Total/NA Solid 7471B 194540LCSD 490-194540/3-A Lab Control Sample Dup Total/NA Solid 7471B 194540MB 490-194540/1-A Method Blank Total/NA Analysis Batch: 195008 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 6010C 194105490-62390-7 TMW-1 Total/NA Water 6010C 194105490-62390-8 TMW-2 Total/NA Water 6010C 194105490-62417-G-1-B MS Matrix Spike Total/NA Water 6010C 194105490-62417-G-1-C MSD Matrix Spike Duplicate Total/NA Water 6010C 194105LCS 490-194105/2-A Lab Control Sample Total/NA Water 6010C 194105LCSD 490-194105/3-A Lab Control Sample Dup Total/NA Water 6010C 194105MB 490-194105/1-A Method Blank Total/NA Analysis Batch: 195573 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 6010C 194105490-62390-7 TMW-1 Total/NA Water 6010C 194105490-62390-8 TMW-2 Total/NA Water 6010C 194105490-62417-G-1-B MS Matrix Spike Total/NA Water 6010C 194105490-62417-G-1-C MSD Matrix Spike Duplicate Total/NA Water 6010C 194105LCS 490-194105/2-A Lab Control Sample Total/NA Water 6010C 194105LCSD 490-194105/3-A Lab Control Sample Dup Total/NA Water 6010C 194105MB 490-194105/1-A Method Blank Total/NA General Chemistry Analysis Batch: 193935 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture490-62388-A-1 DU Duplicate Total/NA Solid Moisture490-62390-1 SB-1 (5-7)Total/NA Solid Moisture490-62390-2 SB-2 (1-3)Total/NA Solid Moisture490-62390-3 SB-3 (1-2)Total/NA Solid Moisture490-62390-4 SB-4 (1-2)Total/NA Solid Moisture490-62390-5 SB-5 (1-2)Total/NA Solid Moisture490-62390-6 SB-6 (1-2)Total/NA Solid Moisture490-62390-9 Background (1-2)Total/NA TestAmerica Nashville Page 64 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Lab Chronicle Client: Hart & Hickman, PC TestAmerica Job ID: 490-62390-1 Project/Site: 1600 Linville Falls Hwy, Avery County,NC SDG: FCB-014 Task 2 Client Sample ID: SB-1 (5-7)Lab Sample ID: 490-62390-1 Matrix: SolidDate Collected: 09/25/14 09:27 Percent Solids: 67.1Date Received: 09/26/14 09:00 Prep 5035 JLP09/27/14 10:08 TAL NSH193627 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.21 g 5.0 mL Analysis 8260B 1 194979 10/03/14 23:13 JJR TAL NSHTotal/NA 5.21 g 5.0 mL Prep 5035 193628 09/27/14 10:09 JLP TAL NSHTotal/NA 4.169 g 5.0 mL Analysis 8260B 1 194478 10/01/14 21:49 KKK TAL NSHTotal/NA 4.169 g 5.0 mL Prep 3550C 194221 09/30/14 13:47 RMS TAL NSHTotal/NA 45.18 g 1.00 mL Analysis 8270D 1 194440 10/02/14 00:59 SNR TAL NSHTotal/NA 45.18 g 1.00 mL Prep 3051A 193952 09/29/14 13:45 TDP TAL NSHTotal/NA 0.509 g 100 mL Analysis 6010C 1 194369 09/30/14 16:58 LTB TAL NSHTotal/NA 0.509 g 100 mL Prep 7471B 194384 10/01/14 08:22 AAS TAL NSHTotal/NA 0.600 g 100 mL Analysis 7471B 1 194477 10/01/14 10:58 AAS TAL NSHTotal/NA 0.600 g 100 mL Analysis Moisture 1 193935 09/29/14 13:04 RRS TAL NSHTotal/NA Client Sample ID: SB-2 (1-3)Lab Sample ID: 490-62390-2 Matrix: SolidDate Collected: 09/25/14 10:50 Percent Solids: 68.3Date Received: 09/26/14 09:00 Prep 5035 JLP09/27/14 10:09 TAL NSH193628 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.543 g 5.0 mL Analysis 8260B 1 194478 10/01/14 21:19 KKK TAL NSHTotal/NA 5.543 g 5.0 mL Prep 3550C 194221 09/30/14 13:47 RMS TAL NSHTotal/NA 43.95 g 1.00 mL Analysis 8270D 1 194440 10/02/14 01:23 SNR TAL NSHTotal/NA 43.95 g 1.00 mL Prep 3051A 193952 09/29/14 13:45 TDP TAL NSHTotal/NA 0.509 g 100 mL Analysis 6010C 1 194369 09/30/14 17:02 LTB TAL NSHTotal/NA 0.509 g 100 mL Prep 7471B 194384 10/01/14 08:22 AAS TAL NSHTotal/NA 0.616 g 100 mL Analysis 7471B 1 194477 10/01/14 11:00 AAS TAL NSHTotal/NA 0.616 g 100 mL Analysis Moisture 1 193935 09/29/14 13:04 RRS TAL NSHTotal/NA Client Sample ID: SB-3 (1-2)Lab Sample ID: 490-62390-3 Matrix: SolidDate Collected: 09/25/14 11:30 Percent Solids: 77.6Date Received: 09/26/14 09:00 Prep 5035 JLP09/27/14 10:09 TAL NSH193628 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.943 g 5.0 mL Analysis 8260B 1 194478 10/01/14 20:50 KKK TAL NSHTotal/NA 5.943 g 5.0 mL Prep 3051A 193952 09/29/14 13:45 TDP TAL NSHTotal/NA 0.517 g 100 mL Analysis 6010C 1 194369 09/30/14 17:05 LTB TAL NSHTotal/NA 0.517 g 100 mL Prep 7471B 194384 10/01/14 08:22 AAS TAL NSHTotal/NA 0.625 g 100 mL Analysis 7471B 1 194477 10/01/14 11:02 AAS TAL NSHTotal/NA 0.625 g 100 mL Analysis Moisture 1 193935 09/29/14 13:04 RRS TAL NSHTotal/NA TestAmerica Nashville Page 65 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Lab Chronicle Client: Hart & Hickman, PC TestAmerica Job ID: 490-62390-1 Project/Site: 1600 Linville Falls Hwy, Avery County,NC SDG: FCB-014 Task 2 Client Sample ID: SB-4 (1-2)Lab Sample ID: 490-62390-4 Matrix: SolidDate Collected: 09/25/14 11:45 Percent Solids: 79.0Date Received: 09/26/14 09:00 Prep 5035 JLP09/27/14 10:09 TAL NSH193628 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.094 g 5.0 mL Analysis 8260B 1 194702 10/02/14 19:25 KKK TAL NSHTotal/NA 5.094 g 5.0 mL Prep 3051A 193952 09/29/14 13:45 TDP TAL NSHTotal/NA 0.502 g 100 mL Analysis 6010C 1 194369 09/30/14 17:09 LTB TAL NSHTotal/NA 0.502 g 100 mL Prep 7471B 194384 10/01/14 08:22 AAS TAL NSHTotal/NA 0.612 g 100 mL Analysis 7471B 1 194477 10/01/14 11:04 AAS TAL NSHTotal/NA 0.612 g 100 mL Analysis Moisture 1 193935 09/29/14 13:04 RRS TAL NSHTotal/NA Client Sample ID: SB-5 (1-2)Lab Sample ID: 490-62390-5 Matrix: SolidDate Collected: 09/25/14 13:00 Percent Solids: 78.5Date Received: 09/26/14 09:00 Prep 5035 JLP09/27/14 10:08 TAL NSH193627 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 6.272 g 5.0 mL Analysis 8015C 1 194274 09/30/14 16:51 AMC TAL NSHTotal/NA 6.272 g 5.0 mL Prep 3550C 194115 09/30/14 10:14 LDC TAL NSHTotal/NA 31.97 g 1.00 mL Analysis 8015C 1 194607 10/01/14 20:58 JPS TAL NSHTotal/NA 31.97 g 1.00 mL Analysis Moisture 1 193935 09/29/14 13:04 RRS TAL NSHTotal/NA Client Sample ID: SB-6 (1-2)Lab Sample ID: 490-62390-6 Matrix: SolidDate Collected: 09/25/14 12:45 Percent Solids: 78.7Date Received: 09/26/14 09:00 Prep 5035 JLP09/27/14 10:08 TAL NSH193627 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.78 g 5.0 mL Analysis 8015C 1 194274 09/30/14 17:25 AMC TAL NSHTotal/NA 5.78 g 5.0 mL Prep 3550C 194115 09/30/14 10:14 LDC TAL NSHTotal/NA 31.79 g 1.00 mL Analysis 8015C 1 194607 10/01/14 21:12 JPS TAL NSHTotal/NA 31.79 g 1.00 mL Analysis Moisture 1 193935 09/29/14 13:04 RRS TAL NSHTotal/NA Client Sample ID: TMW-1 Lab Sample ID: 490-62390-7 Matrix: WaterDate Collected: 09/25/14 12:17 Date Received: 09/26/14 09:00 Analysis 8260B BJM10/01/14 04:311 TAL NSH194305 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 10 mL 10 mL Prep 3510C 194350 10/01/14 11:28 CLM TAL NSHTotal/NA 275 mL 1.0 mL Analysis 8270D 1 194448 10/01/14 21:35 BES TAL NSHTotal/NA 275 mL 1.0 mL Prep 3010A 194105 09/30/14 10:07 ADN TAL NSHTotal/NA 50 mL 50 mL Analysis 6010C 1 195008 10/02/14 17:34 LTB TAL NSHTotal/NA 50 mL 50 mL Prep 3010A 194105 09/30/14 10:07 ADN TAL NSHTotal/NA 50 mL 50 mL Analysis 6010C 1 195573 10/03/14 16:55 LTB TAL NSHTotal/NA 50 mL 50 mL Prep 7470A 194352 10/01/14 06:48 AAS TAL NSHTotal/NA 30 mL 30 mL TestAmerica Nashville Page 66 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Lab Chronicle Client: Hart & Hickman, PC TestAmerica Job ID: 490-62390-1 Project/Site: 1600 Linville Falls Hwy, Avery County,NC SDG: FCB-014 Task 2 Client Sample ID: TMW-1 Lab Sample ID: 490-62390-7 Matrix: WaterDate Collected: 09/25/14 12:17 Date Received: 09/26/14 09:00 Analysis 7470A AAS10/01/14 14:331 TAL NSH194570 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 30 mL 30 mL Client Sample ID: TMW-2 Lab Sample ID: 490-62390-8 Matrix: WaterDate Collected: 09/25/14 14:01 Date Received: 09/26/14 09:00 Analysis 8260B BJM10/01/14 04:051 TAL NSH194305 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 10 mL 10 mL Prep 3510C 194350 10/01/14 11:28 CLM TAL NSHTotal/NA 275 mL 1.0 mL Analysis 8270D 1 194448 10/01/14 21:12 BES TAL NSHTotal/NA 275 mL 1.0 mL Prep 3010A 194105 09/30/14 10:07 ADN TAL NSHTotal/NA 50 mL 50 mL Analysis 6010C 1 195008 10/02/14 17:49 LTB TAL NSHTotal/NA 50 mL 50 mL Prep 3010A 194105 09/30/14 10:07 ADN TAL NSHTotal/NA 50 mL 50 mL Analysis 6010C 1 195573 10/03/14 16:58 LTB TAL NSHTotal/NA 50 mL 50 mL Prep 7470A 194352 10/01/14 06:48 AAS TAL NSHTotal/NA 30 mL 30 mL Analysis 7470A 1 194570 10/01/14 14:35 AAS TAL NSHTotal/NA 30 mL 30 mL Client Sample ID: Background (1-2)Lab Sample ID: 490-62390-9 Matrix: SolidDate Collected: 09/25/14 13:37 Percent Solids: 65.9Date Received: 09/26/14 09:00 Prep 3051A TDP09/29/14 13:45 TAL NSH193952 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 0.516 g 100 mL Analysis 6010C 1 194369 09/30/14 17:24 LTB TAL NSHTotal/NA 0.516 g 100 mL Prep 7471B 194540 10/01/14 14:28 AAS TAL NSHTotal/NA 0.598 g 100 mL Analysis 7471B 1 194816 10/02/14 12:19 AAS TAL NSHTotal/NA 0.598 g 100 mL Analysis Moisture 1 193935 09/29/14 13:04 RRS TAL NSHTotal/NA Laboratory References: TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177 TestAmerica Nashville Page 67 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Method Summary TestAmerica Job ID: 490-62390-1Client: Hart & Hickman, PC SDG: FCB-014 Task 2Project/Site: 1600 Linville Falls Hwy, Avery County,NC Method Method Description LaboratoryProtocol SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH SW8468270DSemivolatile Organic Compounds (GC/MS)TAL NSH SW8468015CNonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)TAL NSH SW8468015CNonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)TAL NSH SW8466010CMetals (ICP)TAL NSH SW8467470AMercury (CVAA)TAL NSH SW8467471BMercury in Solid or Semisolid Waste (Manual Cold Vapor Technique)TAL NSH EPAMoisturePercent Moisture TAL NSH Protocol References: EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177 TestAmerica Nashville Page 68 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Certification Summary Client: Hart & Hickman, PC TestAmerica Job ID: 490-62390-1 Project/Site: 1600 Linville Falls Hwy, Avery County,NC SDG: FCB-014 Task 2 Laboratory: TestAmerica Nashville Unless otherwise noted, all analytes for this laboratory were covered under each certification below. Authority Program EPA Region Certification ID Expiration Date North Carolina (WW/SW)3874State Program 12-31-14 Analysis Method Prep Method Matrix Analyte The following analytes are included in this report, but certification is not offered by the governing authority: Moisture Solid Percent Solids TestAmerica Nashville Page 69 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Page 70 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Page 71 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Page 72 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Page 73 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Login Sample Receipt Checklist Client: Hart & Hickman, PC Job Number: 490-62390-1 SDG Number: FCB-014 Task 2 Login Number: 62390 Question Answer Comment Creator: Huckaba, Jimmy List Source: TestAmerica Nashville List Number: 1 TrueRadioactivity wasn't checked or is </= background as measured by a survey meter. TrueThe cooler's custody seal, if present, is intact. N/ASample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded. TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time. TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. N/ASample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. TrueResidual Chlorine Checked. TestAmerica Nashville Page 74 of 74 10/6/2014 1 2 3 4 5 6 7 8 9 10 11 12 13 Via Email January 27, 2015 First Citizens Bank 4300 Six Forks Road Raleigh, NC 27609-5718 Attention: Mr. Steve Pollok Sr. Commercial Resolution Officer Re: Additional Phase II ESA C&E Manufacturing, Ltd. 1600 Linville Falls Highway Avery County, North Carolina H&H Job No. FCB-014 Dear Steve: 1.0 Executive Summary This report presents the methods and results of additional Phase II Environmental Site Assessment (ESA) activities conducted by Hart & Hickman, PC (H&H) at the Addco property located at 1600 Linville Falls Highway in Avery County, North Carolina (subject site). The purpose of the additional Phase II ESA activities was to further assess the presence of the polynuclear aromatic hydrocarbon (PAH) naphthalene, lead, and manganese which were detected in concentrations above North Carolina Groundwater Standards (2L groundwater standards) in the vicinity of the facility’s septic tank and septic leach field during previous Phase II ESA activities conducted in September 2014. The additional Phase II ESA activities included installation of temporary monitor wells along the downgradient property boundary, sampling of the facility’s water supply well, and performance of a cursory receptor survey in the vicinity of the site. Mr. Steve Pollok January 27, 2015 Page 2 The results of our assessment activities indicate that manganese was detected above the 2L groundwater standard in groundwater samples collected from temporary monitoring wells TMW- 3 and TMW-4 advanced downgradient of the site’s septic system leach field near the southwestern property boundaries. Other compounds were not detected above 2L groundwater standards in groundwater samples collected from TMW-3 and TMW-4. It appears that the manganese detections in groundwater may be site-related and extend off-site. The results of water supply well sampling activities indicate that lead was detected above the 2L groundwater standard and drinking water maximum contaminant level (MCL) in a water sample. Copper and zinc were also detected in the water sample; however, at concentrations below their respective 2L groundwater standards (and drinking water MCLs or secondary MCLs). The source of the lead is not known but could be related to site activities or from piping used in the water supply well and/or piping. 2.0 Property Description and Background The subject site is developed as an industrial manufacturing facility and consists of an approximately 5.71-acre parcel of land. The property is occupied by three industrial buildings including a 9,000-square ft manufacturing and office building (Building 1), a 14,500 square ft manufacturing/warehouse building (Building 2), and a 20,000-square ft shipping/receiving warehouse with a powder coating application area and former paint booth (Building 3). A solar farm, which was installed and is managed by Eagle Electron Power Partners (EEPP), is located on the southeastern portion of the property. The western portion of the site consists of undeveloped land. A Site Location Map and a Sample Location Map are included as Figures 1 and 2, respectively. H&H conducted Phase I ESA activities at the Site in August 2014 and identified the following potential areas of concern: S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Additional Phase II ESA Activities\Additional Phase II ESA Report - 1600 Linville Falls Hwy (First Citizens Bank).doc Mr. Steve Pollok January 27, 2015 Page 3 • potential discharge of powder coating materials, coolant, and petroleum-based products generated during manufacturing activities at the site into the facility septic system which consists of two septic tanks (west of Building 3 and south of Building 1) and septic field (west of Building 3); • oil staining to the ground surface in concrete cut-out areas adjacent to metal fabrication machines in Building 2; and • staining to exterior vents for the former paint and powder coat application booths on the exterior of Building 3. In September 2014, H&H completed initial Phase II ESA activities on the property. The results of our assessment activities indicated the following (see also Tables 1 and 2): Soil impacts were detected above the NC Department of Environment and Natural Resources (DENR) total petroleum hydrocarbon (TPH) Action Level in two shallow borings advanced below the concrete floor of Building 2. Specifically, diesel range TPH (TPH-DRO) was detected at 15.4 mg/kg and 30 mg/kg in SB-5 (1-2 ft) and SB-6 (1-2 ft), respectively. The DENR Action Level for TPH-DRO is 10 mg/kg. VOCs were not detected above DENR Inactive Hazardous Sites Branch (IHSB) Residential, Industrial, or Protection of Groundwater (POG) preliminary soil remediation goals (PSRGs) in samples collected adjacent to the septic tank (SB-1), within the septic field (SB-2), below the former paint booth vent (SB-3), or below the powder coating booth vent (SB-4). Additionally, polynuclear aromatic hydrocarbons (PAHs) were not detected above DENR IHSB PSRGs in soil samples collected near the septic tank (SB-1) or septic field (SB-2). Manganese was detected in soil sample SB-2 (1-3 ft) collected from the septic leach field at a concentration above Residential and POG PSRGs. Manganese was also detected above Residential PSRGs in soil sample SB-3 (1-2 ft) collected below the former paint booth vent and S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Additional Phase II ESA Activities\Additional Phase II ESA Report - 1600 Linville Falls Hwy (First Citizens Bank).doc Mr. Steve Pollok January 27, 2015 Page 4 soil sample SB-4 (1-2 ft) collected below the powder coating booth vent. The manganese concentrations in the soil samples listed above exceed site specific background concentrations collected from a soil boring SB-BG (1-2 ft) advanced in an undisturbed area in the eastern portion of the property. Although the manganese concentrations in the soil samples listed above exceed Residential and POG PSRGs, and site specific background concentrations, the manganese concentrations are below Industrial SRGs and are within the range of published literature background concentrations for North Carolina and conterminous United States (US) soils. Naphthalene, lead, and manganese were detected above NC 2L groundwater standards in a groundwater sample collected from temporary monitoring well TMW-2 advanced adjacent to the septic leach field west of Building 3. Naphthalene and manganese were also detected above their 2L groundwater standards in a groundwater sample collected from TMW-1 advanced downgradient of the septic tank south of Building 1. Other PAHs and metals were also detected in TMW-1 and TMW-2 but at concentrations below groundwater standards. H&H conducted additional Phase II ESA groundwater sampling activities at the subject site on January 9, 2015 to 1) further assess the naphthalene, lead, and manganese concentrations in groundwater above 2L groundwater standards in the vicinity of the facility’s septic tank and septic leach field to evaluate if they may have migrated off-site; 2) sample the facility’s water supply well to evaluate potential impacts to deeper groundwater; and 3) perform a cursory receptor survey in the area of the site. The methods and results of Phase II ESA activities are presented in the following sections. 3.0 Phase II ESA Scope of Work 3.1 Utility Clearance Prior to conducting the additional sampling activities, H&H contacted North Carolina One-Call, the public utility locator to mark subsurface utilities located on the site. In addition, Probe S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Additional Phase II ESA Activities\Additional Phase II ESA Report - 1600 Linville Falls Hwy (First Citizens Bank).doc Mr. Steve Pollok January 27, 2015 Page 5 Utility, LLC, a private utility locater was contracted to locate and demark subsurface utilities in the areas of the soil borings and temporary wells. As an additional safety precaution, each boring was initially advanced using a hand auger to a depth of at least 5 feet (ft) below ground surface (bgs) to clear the boring of possible undocumented subsurface utility lines. 3.2 Groundwater Sampling Activities Temporary Monitoring Well Groundwater Sampling H&H oversaw advancement of two additional temporary groundwater monitoring wells (TMW-3 and TMW-4) at the subject site by EPDS utilizing direct push technology (DPT) methods. TMW-3 was installed near the western property boundary at a location adjacent to and cross- gradient of the facility’s septic tank. TMW-4 was installed near the southern property boundary at a location downgradient of the facility’s septic leach field. The temporary monitoring wells were constructed with one-inch diameter PVC with 10-ft sections of pre-packed screens set to bracket the water table. The temporary groundwater monitoring wells TMW-3 and TMW-4 were installed to 15 and 16 ft bgs, respectively. Following temporary well installation, H&H gauged the temporary monitoring wells. The water levels in TMW-3 and TMW-4 were both approximately 9 ft bgs. H&H subsequently developed TMW-3 and TMW-4 utilizing low-flow techniques. H&H continued development until turbidity in groundwater was below 10 nephelometric turbidity units (NTUs) in both temporary monitoring wells. After purging the wells, H&H collected groundwater samples from TMW-3 and TWM-4 and submitted the samples to TestAmerica for analysis of VOCs by EPA Method 8260, PAHs by EPA Method 8270, and lead and manganese by EPA Method 6010C. Temporary monitoring well logs are presented in Appendix A. Water Supply Well Groundwater Sampling H&H collected a groundwater sample from the facility’s water supply well located in the northern portion of the site. The water supply well’s galvanized steel casing is approximately 4- S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Additional Phase II ESA Activities\Additional Phase II ESA Report - 1600 Linville Falls Hwy (First Citizens Bank).doc Mr. Steve Pollok January 27, 2015 Page 6 inches in diameter and extends to a depth of approximately 96 ft bgs per the well tag. H&H could not gauge the water level within the well; however, the well tag noted that static water level within the well is approximately 20 ft bgs. Prior to sampling, H&H purged approximately 50 gallons of groundwater from the well. After purging, H&H sampled the facility’s water supply well from a steel pipe equipped with brass spigot closest to the well head and submitted the sample to TestAmerica for analysis of VOCs by EPA Method 8260, SVOCs by EPA Method 8270, and hazardous substance list (HSL) metals by EPA Method 6010C. 3.3 Boring Abandonment and Investigation Derived Waste Upon completion of groundwater sampling activities, EPDS abandoned the temporary monitoring well borings by removing well screen/riser materials, filling the borings with grout, and patching the surfaces to match the surrounding area. Soil cuttings and groundwater generated during Phase II ESA activities were spread on-site in accordance with DENR guidance. 3.4 QA/QC Process H&H utilized standard quality assurance/quality control (QA/QC) processes during the Phase II ESA activities. Non-dedicated sampling equipment, including DPT tooling, the water level meter, and the hand auger, were decontaminated using Liquinox® detergent and deionized water prior to and between each sampling location. H&H and EPDS wore nitrile gloves while handling samples, and the groundwater samples were collected using new tubing. Groundwater samples were collected in laboratory-provided containers and immediately placed on ice. A completed chain-of-custody (COC) record accompanied the samples and included the sample designation, date and time collected, matrix, sample container information, and requested analyses. H&H sampling personnel signed the completed COC record, and the samples were transported to TestAmerica by local courier and FedEx. S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Additional Phase II ESA Activities\Additional Phase II ESA Report - 1600 Linville Falls Hwy (First Citizens Bank).doc Mr. Steve Pollok January 27, 2015 Page 7 4.0 Site-Specific Topography, Geology, & Hydrogeology 4.1 Topography The elevation of the subject site is approximately 3,600 feet above mean sea level. The topographic gradient in the area of the subject site is in a generally southerly direction toward the Linville River located approximately 0.4 mile south of the subject site. An area topographic map is included as Figure 1. 4.2 Physical Setting Geology Avery County, including the subject property, is located within the Blue Ridge physiographic province of North Carolina. This province is a northeast trending zone extending from Georgia through Virginia and ranges in width from approximately 15 to 55 miles in North Carolina. The Blue Ridge is a deeply dissected mountainous area of numerous steep mountain ridges, intermontane basins, and trench valleys that intersect at angles and give the area its rugged mountain character. The site is located within the Grandfather Mountain window of the Blue Ridge province which is characterized by bedrock composed of meta-sedimetary and meta-volcanic rocks. Based on the 1985 Geologic Map of North Carolina, the bedrock underlying the subject property is composed of greenstone and meta-arkose with interlayered sedimentary rocks. Overlying the bedrock in many areas is a zone of residual soil or saprolite which is developed from the in-situ weathering of the underlying rocks. The saprolite is typically composed of unconsolidated silts, clays, sand, and rock fragments. S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Additional Phase II ESA Activities\Additional Phase II ESA Report - 1600 Linville Falls Hwy (First Citizens Bank).doc Mr. Steve Pollok January 27, 2015 Page 8 Hydrogeology Groundwater generally occurs under water table conditions within the interconnected saprolite and bedrock zones. The primary source of ground water in the area is from precipitation that reaches the water table through infiltration. The saprolite is generally considered to be a recharge medium for the bedrock aquifer because it holds precipitation and allows ground water to gradually infiltrate into the bedrock joints, faults, and fractures. Groundwater flow is typically from upland areas to lowland areas where ground water discharges to streams. During Phase II ESA groundwater sampling activities, H&H determined that the depth to groundwater was approximately 9 ft below the ground surface in the two temporary monitoring wells (TMW-1 and TMW-2) advanced at the site. 5.0 Receptor Survey H&H conducted a cursory receptor survey of the surrounding area. During the receptor survey, H&H identified as many as nine water supply wells located within a 0.25-mile radius of the site based on our review of readily accessible public areas. The wells are located on residential and commercial properties, and the approximate locations of the identified water supply wells are depicted on Figure 1. Municipal water is not available in the area of the site. According to Avery County tax information, the land use designation for the subject site and surrounding properties is presented below: Subject Site or Adjacent Property Occupant Address – Linville Falls Highway Parcel # Land Use Designation Water Supply Well Observed or Suspected Subject Site Addco 1600 184407688011 Lt Manufacturing Observed North Adjacent Property Stor-All Mini- Storage 1580 184407686392 Mini- Warehouse/ Industrial Suspected S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Additional Phase II ESA Activities\Additional Phase II ESA Report - 1600 Linville Falls Hwy (First Citizens Bank).doc Mr. Steve Pollok January 27, 2015 Page 9 East Adjacent Property McLean Residence 1585 184407782372 Residential Observed South Adjacent Property Classic Stone Works 1700 184407676564 Lt. Manufacturing Suspected West Adjacent Property Camp Carmel Church Camp 1676 184407588362 Church Camp Suspected Based on our review of the USGS topographic map and our reconnaissance of the surrounding area, H&H did not observe obvious surface water features located within 0.25-mile of the subject site. 6.0 Analytical Laboratory Results Laboratory analytical data reports and chain-of-custody records are included as Appendix B. The data are summarized in Table 2. Manganese (67.8 µg/L and 277 µg/L) was detected above the 2L groundwater standard of 50 µg/L in groundwater samples collected from temporary monitoring wells TMW-3 and TMW-4 advanced along the western and southern property boundaries near the septic system leach field. Lead was not detected in the samples. In addition, low levels of petroleum-related VOCs and naphthalene were detected in TMW-4 but at concentrations below 2L groundwater standards. . In the water supply well sample, lead (28.3 µg/L) was detected above the 2L groundwater standard (and drinking water MCL) of 15 µg/L. Copper (64.2 µg/L) and zinc (117 µg/L) were also detected in the water sample; however, at concentrations below their respective 2L groundwater standards and drinking water MCLs or secondary MCLs. S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Additional Phase II ESA Activities\Additional Phase II ESA Report - 1600 Linville Falls Hwy (First Citizens Bank).doc Mr. Steve Pollok January 27, 2015 Page 10 7.0 Findings and Recommendations H&H conducted additional groundwater assessment activities at the subject site in January 2015 to further assess the presence of naphthalene, lead, and manganese in groundwater detected in the area of the facility’s septic system during previous Phase II ESA activities conducted in September 2014. Manganese (67.8 µg/L and 277 µg/L) was detected above the 2L groundwater standard in groundwater samples collected from temporary monitoring wells TMW-3 and TMW-4 advanced along the western and southern property boundaries near the septic system leach field. These concentrations are lower than the concentration detected in previous sample TMW-2 advanced in the facility’s septic leach field of 7,150 µg/L. Naphthalene and lead were not detected above 2L groundwater standards in the samples from TMW-3 and TMW-4. Based on the results of previous soil and groundwater sampling activities, it appears that the elevated manganese concentrations may be the result of current/former auto part manufacturing activities and may extend off-site. Please note that manganese is a naturally occurring metal and its presence in groundwater could be associated with background groundwater conditions. Manganese was not listed as a compound in material safety data sheets that H&H revised for compounds used at the site; however, manganese phosphates are frequently used as a rust inhibitor prior to powder coating. Based upon the high level of manganese detected in TMW-2 and the presence of manganese in soil in the septic area, the manganese detections appear to be at least partly attributable to site activities. Lead was detected above the 2L groundwater standard (and drinking water MCL) in a water sample collected from the facility’s water supply well. As noted previously, lead was also detected above the 2L standard in groundwater in the area of the septic system. Copper and zinc were also detected in the water sample but below their respective 2L groundwater standards and MCLs. The presence of lead in combination with lead and zinc may be an indication that the S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Additional Phase II ESA Activities\Additional Phase II ESA Report - 1600 Linville Falls Hwy (First Citizens Bank).doc Mr. Steve Pollok January 27, 2015 Page 11 presence of these metals is associated with steel well casing or plumbing/piping; however their presence could also be related to site activities. The results of the receptor survey indicate that municipal water is not available to the subject site area and water utilized by adjacent surrounding properties is supplied by water supply wells. Thank you for the opportunity to assist with this project. Should you have any questions or require any additional information concerning this report, please feel free to contact us at (704) 586-0007. Sincerely, Hart & Hickman, PC Hart & Hickman, PC Matt Ingalls Steve Hart, PG Project Manager Principal S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Additional Phase II ESA Activities\Additional Phase II ESA Report - 1600 Linville Falls Hwy (First Citizens Bank).doc Ta b l e 1 Su m m a r y o f S o i l A n a l y t i c a l D a t a 16 0 0 L i n v i l l e F a l l s H w y Av e r y C o u n t y , N o r t h C a r o l i n a H& H J o b N o . F C B - 0 1 4 Sa m p l e L o c a t i o n S e p t i c T a n k S e p t i c F i e l d Fo r m e r P a i n t Bo o t h V e n t P o w d e r C o a t Bo o t h V e n t Bu i l d i n g 2 - M e t a l Fa b r i c a t i o n Ma c h i n e Bu i l d i n g 2 - M e t a l Fa b r i c a t i o n Ma c h i n e Sa m p l e I D SB - 1 S B - 2 S B - 3 S B - 4 S B - 5 S B - 6 Sa m p l e D e p t h ( f t ) 5- 7 1 - 3 1 - 2 1 - 2 1 - 2 1 - 2 Sa m p l e D a t e 9/ 2 5 / 2 0 1 4 9 / 2 5 / 2 0 1 4 9 / 2 5 / 2 0 1 4 9 / 2 5 / 2 0 1 4 9 / 2 5 / 2 0 1 4 9 / 2 5 / 2 0 1 4 Un i t s mg / k g m g / k g m g / k g m g / k g m g / k g m g / k g VO C s ( 8 2 6 0 ) mg/kg m g / k g 1,2 , 3 - T r i c h l o r o b e n z e n e <0 . 1 9 2 < 0 . 0 2 6 4 < 0 . 0 0 2 1 7 0 . 0 0 2 7 9 N A N A 9 . 8 1 3 0 N L -- - - Ac e t o n e 0. 2 2 0. 0 9 3 8 < 0 . 0 5 4 2 < 0 . 0 6 2 1 N A N A 12 , 0 0 0 1 0 0 , 0 0 0 2 4 - - - - PA H s ( 8 2 7 0 ) Fl u o r a n t h e n e ( m g / k g ) 0.0 8 7 < 0 . 0 6 6 9 N A N A N A N A 46 0 6 , 0 0 0 3 3 0 - - - - Py r e n e ( m g / k g ) 0. 0 7 2 4 < 0 . 0 6 6 9 N A N A N A N A 34 0 4 , 6 0 0 2 2 0 - - - - HS L M e t a l s An t i m o n y < 1 4 . 6 < 1 4 . 4 < 1 2 . 5 < 1 2 . 6 NA N A 6. 2 9 4 0 . 9 <1.0-8.8 0 . 7 6 Ar s e n i c < 2 . 9 3 5 . 2 6 < 2 . 4 9 < 2 . 5 2 NA N A 0. 6 7 3 . 0 5 . 8 1.0 - 18 4 . 8 Be r y l l i u m < 1 . 4 6 < 1 . 4 4 1 . 3 5 < 1 . 2 6 NA N A 32 4 6 0 6 3 ND - 2.0 0 . 1 1 Ca d m i u m < 1 . 4 6 < 1 . 4 4 < 1 . 2 5 < 1 . 2 6 NA N A 14 2 0 0 3 1.0 - 10 4 . 3 Ch r o m i u m 1 0 . 5 1 5 . 6 5 . 3 6 2 5 NA N A 24 , 0 0 0 1 0 0 , 0 0 0 3 6 0 , 0 0 0 7.0 - 300 6 5 Co p p e r 2 4 . 2 1 3 . 9 1 1 . 5 1 8 . 7 NA N A 62 0 9 , 4 0 0 7 0 0 3.0 - 100 3 4 Le a d 2 1 . 7 3 6 . 2 1 2 . 6 3 6 . 4 NA N A 40 0 8 0 0 2 7 0 ND - 50 1 6 Ma n g a n e s e 1 4 0 1,0 5 0 41 5 63 6 NA NA 36 0 5,2 0 0 65 0 8.0 - 3,394 5 9 4 Ni c k e l 10 . 7 10 . 7 8. 0 3 28 . 4 NA NA 30 0 4,4 0 0 13 0 ND - 150 23 Se l e n i u m < 2 . 9 3 < 2 . 8 7 < 2 . 4 9 < 2 . 5 2 NA NA 78 1,2 0 0 21 NE NE Sil v e r < 1 . 4 6 < 1 . 4 4 < 1 . 2 5 < 1 . 2 6 NA NA 78 1,2 0 0 34 ND-5.0 NE Th a l l i u m < 2 . 9 3 < 2 . 8 7 < 2 . 4 9 < 2 . 5 2 NA NA NL NL NL NE NE Zi n c 71 78 . 6 < 1 2 . 5 < 1 2 . 6 NA NA 4,6 0 0 70 , 0 0 0 1, 2 0 0 25 - 124 56 Me r c u r y < 0 . 1 4 9 < 0 . 1 4 3 < 0 . 1 2 4 < 0 . 1 2 4 NA NA 1. 9 3. 1 1.0 0.03 - 0.52 0 . 1 2 1 TP H - G R O / D R O ( m g / k g ) Die s e l R a n g e O r g a n i c s NA NA NA NA 15 . 4 16 6 Ga s o l i n e R a n g e O r g a n i c s NA NA NA NA < 6 . 4 4 <6 . 8 5 No t e s : 1) N C D E N R I n a c t i v e H a z a r d o u s S i t e s B r a n c h ( I H S B ) R e s i d e n t i a l a n d I n d u s t r i a l H e a l t h B a s e d S o i l R e m e d i a t i o n G o a l s ( S R G s ) - S e p t e mb e r 2 0 1 4 2) N C D E N R I H S B P r o t e c t i o n o f G r o u n d w a t e r S o i l R e m e d i a t i o n G o a l s ( P O G S R G ) - S e p t e m b e r 2 0 1 4 3) B a c k g r o u n d c o n c e n t r a t i o n s f o r m e t a l s ( e x c e p t m a n g a n e s e ) o b t a i n e d f r o m D r a g u n , J a m e s P h D . A n d K h a l e d C h e k i r i P h D . E l e m e n t s Bo l d in d i c a t e s a n e x c e e d a n c e o f t h e D E N R A c t i o n L e v e l ; U n d e r l i n e i n d i c a t e s e x c e e d a n c e o f R e s i d e n t i a l S G R ; a n d It a l i c s i n d i c a t e e x c e e d a n c e o f P r o t e c t i o n o f G r o u n d w a t e r P S R G VO C s = V o l a t i l e O r g a n i c C o m p o u n d s ; P A H s = P o l y n u c l e a r A r o m a t i c H y d r o c a r b o n s ; T P H = T o t a l p e t r o l e u m h y d r o c a r b o n s ; N S = N o t A n a l y ze d ; N L - N o t L i s t e d Background Metals Range 3Average Background Metals 3 Re s i d e n t i a l S R G 1 (m g / k g ) In d u s t r i a l S R G 1 (m g / k g ) Pr o t e c t i o n o f Gr o u n d w a t e r PS R G ( m g / k g ) 2 10 Sc r e e n i n g L e v e l s NC D E N R A C T I O N L E V E L ( m g / k g ) S: \ A A A - M a s t e r P r o j e c t s \ F i r s t C i t i z e n s B an k - F C B \ F C B - 0 1 4 C & E M a n u f a c t u r i n g - N e w l a n d , NC \ P h a s e I I \ T a b l e s \ A n a l y t i c a l D a t a T a b l e s 10 / 8 / 2 0 1 4 Table 1 (Page 1 of 1)Hart & Hickman, PC Table 2 Summary of Groundwater Analytical Data 1600 Linville Falls Hwy Newland, Avery County, North Carolina H&H Job No. FCB-014 S:\AAA-Master Projects\First Citizens Bank - FCB\FCB-014 C&E Manufacturing - Newland, NC\Phase II\Tables\Analytical Data Tables.xlsx 1/27/2015 Table 1 (Page 1 of 1) Hart & Hickman, PC Location Septic Tank Septic System Western Property Boundary (Cross- Gradient of Septic System) Southwestern Property Boundary (Downgradient of Septic System) Water Supply Well - Northern Property Boundary Sample ID TMW-1 TMW-2 TMW-3 TMW-4 WSW-1 Sample Date 09/25/14 09/25/14 01/09/15 01/09/15 01/09/15 Units µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L VOCs (8260B) Ethylbenzene < 1.0 1.1 <1.0 <1.0 <1.0 600 700 34.9 152 Toluene < 1.0 <1.0 <1.0 1.84 <1.0 600 1,000 3,840 16,100 1,2,4-Trimethylbenzene < 1.0 <1.0 <1.0 1.87 <1.0 400 NS 5.80 24.4 Total Xylenes <2.0 <2.0 <2.0 2.44 <2.0 500 10,000 98.5 414 PAH/SVOCs (8270D)5 Acenaphthene 9.5 8.03 <1.61 <1.61 <2.04 80 NS NS NL Fluorene 2.53 2.58 <1.61 <1.61 <2.04 300 NS NS NL Naphthalene 11.4 30.0 <1.61 1.84 <2.04 6 NS 34.8 146 Phenanthrene <1.82 2.6 <1.61 <1.61 <2.04 200 NS NS NL HSL Metals Antimony < 0.01 < 0.01 NA NA < 0.01 1.0 6 NS NL Arsenic < 0.01 < 0.01 NA NA < 0.01 10 10 NS NL Beryllium < 0.004 < 0.004 NA NA < 0.004 4.0 4 NS NL Cadmium < 0.001 < 0.001 NA NA < 0.001 2 5 NS NL Chromium < 0.005 9.8 NA NA <0.005 10 100 NS NL Copper < 0.01 < 0.01 NA NA 64.2 1,000 1,300*NS NL Lead < 0.005 26.1 <0.0055 <0.0055 28.3 15 15*NS NL Manganese 591 7,150 67.8 277.0 <0.015 50 50**NS NL Nickel < 0.01 < 0.01 NA NA <0.01 100 NS NS NL Selenium < 0.01 < 0.01 NA NA <0.01 20 50 NS NL Silver < 0.005 < 0.005 NA NA <0.005 20 100**NS NL Thallium < 0.01 < 0.01 NA NA <0.01 0.2 2 NS NL Zinc < 0.05 < 0.05 NA NA 117 1,000 5,000**NS NL Mercury < 0.0002 < 0.0002 NA NA < 0.0002 1 2 0.134 0.563 Notes: 1) NCAC 02L Groundwater Quality Standards and Interim Maximum Allowable Concentrations (April 2013) 2) Division of Waste Management Residential Vapor Intrusion Groundwater Screening Level (June 2014) 3) Division of Waste Management Non-Residential Vapor Intrusion Groundwater Screening Level (June 2014) 4) Bold indicates exceedance of NC 2L Groundwater Standard 5) Groundwater sample collected from WSW-1 analyzed for SVOCs by EPA Method 8270D. Remaining groundwater samples analyzed for PAHs by EPA Method 8270D EPA=Environmental Protection Agency; MCLs=Maximum Contaminant Levels; NA=Not Analyzed; NS=No Standard; VOCs = Volatile Organic Compounds; PAHs = Polynuclear Aromatic Hydrocarbons; SVOCs = Semi-Volatile Organic Compounds; and HSL= Hazardous Substance List Screening Criteria Groundwater Samples 2L Groundwater Quality Standard1 DWM Residential Groundwater VI Screening Level2 DWM Non-Residential Groundwater VI Screening Level3EPA Drinking Water MCLs TITLE PROJECT SITE LOCATION MAP ADDCO FACILITY NEWLAND, NORTH CAROLINA DATE: JOB NO: REVISION NO: FIGURE NO: 8-20-14 0 1FCB-014 0 2000 4000 APPROXIMATE SCALE IN FEETN U.S.G.S. QUADRANGLE MAP QUADRANGLE 7.5 MINUTE SERIES (TOPOGRAPHIC) NEWLAND, NC 1994 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) SITE Approximate Location of Water Supply Well Appendix A Analytical Data ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Nashville 2960 Foster Creighton Drive Nashville, TN 37204 Tel: (615)726-0177 TestAmerica Job ID: 490-70180-1 TestAmerica Sample Delivery Group: FCB.014 Client Project/Site: ADDCO Facility For: Hart & Hickman, PC 2923 S Tryon Street Suite 100 Charlotte, North Carolina 28203 Attn: Matt Ingalls Authorized for release by: 1/21/2015 3:13:56 PM Ken Hayes, Project Manager II (615)301-5035 ken.hayes@testamericainc.com The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. 1 2 3 4 5 6 7 8 9 10 11 12 13 Table of Contents Client: Hart & Hickman, PC Project/Site: ADDCO Facility TestAmerica Job ID: 490-70180-1 SDG: FCB.014 Page 2 of 39 TestAmerica Nashville1/21/2015 Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16 QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32 Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .36 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .37 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39 1 2 3 4 5 6 7 8 9 10 11 12 13 Sample Summary TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Lab Sample ID Client Sample ID ReceivedCollectedMatrix 490-70180-1 TMW-4 Water 01/09/15 11:40 01/10/15 08:45 490-70180-2 TMW-3 Water 01/09/15 12:45 01/10/15 08:45 490-70180-3 WSW-1 Water 01/09/15 13:25 01/10/15 08:45 TestAmerica Nashville Page 3 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Case Narrative Client: Hart & Hickman, PC TestAmerica Job ID: 490-70180-1 Project/Site: ADDCO Facility SDG: FCB.014 Job ID: 490-70180-1 Laboratory: TestAmerica Nashville Narrative Job Narrative 490-70180-1 Comments No additional comments. Receipt The samples were received on 1/10/2015 8:45 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 2.7º C. GC/MS VOA No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. GC/MS Semi VOA Method(s) 8270D: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with batches 219917 and 219903. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Metals No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. Organic Prep Method(s) 3510C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with batch 219917 and 219903. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. VOA Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. TestAmerica NashvillePage 4 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Definitions/Glossary TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Qualifiers GC/MS VOA Qualifier Description F2 MS/MSD RPD exceeds control limits Qualifier Metals Qualifier Description F1 MS and/or MSD Recovery exceeds the control limits Qualifier Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference) Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica Nashville Page 5 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Lab Sample ID: 490-70180-1Client Sample ID: TMW-4 Matrix: WaterDate Collected: 01/09/15 11:40 Date Received: 01/10/15 08:45 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone ND 25.0 ug/L 01/13/15 20:08 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 1.00 ug/L 01/13/15 20:08 1BenzeneND 1.00 ug/L 01/13/15 20:08 1BromobenzeneND 1.00 ug/L 01/13/15 20:08 1BromochloromethaneND 1.00 ug/L 01/13/15 20:08 1BromodichloromethaneND 1.00 ug/L 01/13/15 20:08 1BromoformND 1.00 ug/L 01/13/15 20:08 1BromomethaneND 50.0 ug/L 01/13/15 20:08 12-Butanone (MEK)ND 1.00 ug/L 01/13/15 20:08 1Carbon disulfide ND 1.00 ug/L 01/13/15 20:08 1Carbon tetrachloride ND 1.00 ug/L 01/13/15 20:08 1ChlorobenzeneND 1.00 ug/L 01/13/15 20:08 1ChlorodibromomethaneND 1.00 ug/L 01/13/15 20:08 1ChloroethaneND 1.00 ug/L 01/13/15 20:08 1ChloroformND 1.00 ug/L 01/13/15 20:08 1ChloromethaneND 1.00 ug/L 01/13/15 20:08 12-Chlorotoluene ND 1.00 ug/L 01/13/15 20:08 14-Chlorotoluene ND 1.00 ug/L 01/13/15 20:08 1cis-1,2-Dichloroethene ND 1.00 ug/L 01/13/15 20:08 1cis-1,3-Dichloropropene ND 10.0 ug/L 01/13/15 20:08 11,2-Dibromo-3-Chloropropane ND 1.00 ug/L 01/13/15 20:08 11,2-Dibromoethane (EDB)ND 1.00 ug/L 01/13/15 20:08 1DibromomethaneND 1.00 ug/L 01/13/15 20:08 11,2-Dichlorobenzene ND 1.00 ug/L 01/13/15 20:08 11,3-Dichlorobenzene ND 1.00 ug/L 01/13/15 20:08 11,4-Dichlorobenzene ND 1.00 ug/L 01/13/15 20:08 1DichlorodifluoromethaneND 1.00 ug/L 01/13/15 20:08 11,1-Dichloroethane ND 1.00 ug/L 01/13/15 20:08 11,2-Dichloroethane ND 1.00 ug/L 01/13/15 20:08 11,1-Dichloroethene ND 1.00 ug/L 01/13/15 20:08 11,2-Dichloroethene, Total ND 1.00 ug/L 01/13/15 20:08 11,2-Dichloropropane ND 1.00 ug/L 01/13/15 20:08 11,3-Dichloropropane ND 1.00 ug/L 01/13/15 20:08 12,2-Dichloropropane ND 1.00 ug/L 01/13/15 20:08 11,1-Dichloropropene ND 2.00 ug/L 01/13/15 20:08 1Diisopropyl ether ND 1.00 ug/L 01/13/15 20:08 1EthylbenzeneND 2.00 ug/L 01/13/15 20:08 1HexachlorobutadieneND 10.0 ug/L 01/13/15 20:08 12-Hexanone ND 1.00 ug/L 01/13/15 20:08 1IsopropylbenzeneND 5.00 ug/L 01/13/15 20:08 1Methylene Chloride ND 10.0 ug/L 01/13/15 20:08 14-Methyl-2-pentanone (MIBK)ND 1.00 ug/L 01/13/15 20:08 1Methyl tert-butyl ether ND 5.00 ug/L 01/13/15 20:08 1NaphthaleneND 1.00 ug/L 01/13/15 20:08 1n-Butylbenzene ND 1.00 ug/L 01/13/15 20:08 1N-Propylbenzene ND 1.00 ug/L 01/13/15 20:08 1p-Isopropyltoluene ND 1.00 ug/L 01/13/15 20:08 1sec-Butylbenzene ND 1.00 ug/L 01/13/15 20:08 1StyreneND 1.00 ug/L 01/13/15 20:08 1tert-Butylbenzene ND TestAmerica Nashville Page 6 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Lab Sample ID: 490-70180-1Client Sample ID: TMW-4 Matrix: WaterDate Collected: 01/09/15 11:40 Date Received: 01/10/15 08:45 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 1.00 ug/L 01/13/15 20:08 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 1.00 ug/L 01/13/15 20:08 11,1,2,2-Tetrachloroethane ND 1.00 ug/L 01/13/15 20:08 1TetrachloroetheneND 1.00 ug/L 01/13/15 20:08 1Toluene1.64 1.00 ug/L 01/13/15 20:08 1trans-1,2-Dichloroethene ND 1.00 ug/L 01/13/15 20:08 1trans-1,3-Dichloropropene ND 1.00 ug/L 01/13/15 20:08 11,2,3-Trichlorobenzene ND 1.00 ug/L 01/13/15 20:08 11,2,4-Trichlorobenzene ND 1.00 ug/L 01/13/15 20:08 11,1,1-Trichloroethane ND 1.00 ug/L 01/13/15 20:08 11,1,2-Trichloroethane ND 1.00 ug/L 01/13/15 20:08 1TrichloroetheneND 1.00 ug/L 01/13/15 20:08 1TrichlorofluoromethaneND 1.00 ug/L 01/13/15 20:08 11,2,3-Trichloropropane ND 1.00 ug/L 01/13/15 20:08 11,2,4-Trimethylbenzene 1.87 1.00 ug/L 01/13/15 20:08 11,3,5-Trimethylbenzene ND 1.00 ug/L 01/13/15 20:08 1Vinyl chloride ND 2.00 ug/L 01/13/15 20:08 1Xylenes, Total 2.44 4-Bromofluorobenzene (Surr)86 70-130 01/13/15 20:08 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Dibromofluoromethane (Surr)116 01/13/15 20:08 170-130 1,2-Dichloroethane-d4 (Surr)105 01/13/15 20:08 170-130 Toluene-d8 (Surr)106 01/13/15 20:08 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 1.61 ug/L 01/13/15 08:23 01/14/15 14:44 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 1.61 ug/L 01/13/15 08:23 01/14/15 14:44 1AcenaphthyleneND 1.61 ug/L 01/13/15 08:23 01/14/15 14:44 1AnthraceneND 1.61 ug/L 01/13/15 08:23 01/14/15 14:44 1Benzo[a]anthracene ND 1.61 ug/L 01/13/15 08:23 01/14/15 14:44 1Benzo[a]pyrene ND 1.61 ug/L 01/13/15 08:23 01/14/15 14:44 1Benzo[b]fluoranthene ND 1.61 ug/L 01/13/15 08:23 01/14/15 14:44 1Benzo[g,h,i]perylene ND 1.61 ug/L 01/13/15 08:23 01/14/15 14:44 1Benzo[k]fluoranthene ND 1.61 ug/L 01/13/15 08:23 01/14/15 14:44 1ChryseneND 1.61 ug/L 01/13/15 08:23 01/14/15 14:44 1Dibenz(a,h)anthracene ND 1.61 ug/L 01/13/15 08:23 01/14/15 14:44 1FluorantheneND 1.61 ug/L 01/13/15 08:23 01/14/15 14:44 1FluoreneND 1.61 ug/L 01/13/15 08:23 01/14/15 14:44 1Indeno[1,2,3-cd]pyrene ND 1.61 ug/L 01/13/15 08:23 01/14/15 14:44 1Naphthalene1.94 1.61 ug/L 01/13/15 08:23 01/14/15 14:44 1PhenanthreneND 1.61 ug/L 01/13/15 08:23 01/14/15 14:44 1PyreneND 2-Fluorobiphenyl (Surr)65 29-120 01/13/15 08:23 01/14/15 14:44 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Nitrobenzene-d5 (Surr)64 01/13/15 08:23 01/14/15 14:44 127-120 Terphenyl-d14 (Surr)74 01/13/15 08:23 01/14/15 14:44 113-120 TestAmerica Nashville Page 7 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Lab Sample ID: 490-70180-1Client Sample ID: TMW-4 Matrix: WaterDate Collected: 01/09/15 11:40 Date Received: 01/10/15 08:45 Method: 6010C - Metals (ICP) RL MDL Manganese 0.277 0.0150 mg/L 01/13/15 07:42 01/13/15 15:43 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 0.00500 mg/L 01/13/15 07:42 01/13/15 15:43 1LeadND TestAmerica Nashville Page 8 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Lab Sample ID: 490-70180-2Client Sample ID: TMW-3 Matrix: WaterDate Collected: 01/09/15 12:45 Date Received: 01/10/15 08:45 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone ND 25.0 ug/L 01/13/15 20:36 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 1.00 ug/L 01/13/15 20:36 1BenzeneND 1.00 ug/L 01/13/15 20:36 1BromobenzeneND 1.00 ug/L 01/13/15 20:36 1BromochloromethaneND 1.00 ug/L 01/13/15 20:36 1BromodichloromethaneND 1.00 ug/L 01/13/15 20:36 1BromoformND 1.00 ug/L 01/13/15 20:36 1BromomethaneND 50.0 ug/L 01/13/15 20:36 12-Butanone (MEK)ND 1.00 ug/L 01/13/15 20:36 1Carbon disulfide ND 1.00 ug/L 01/13/15 20:36 1Carbon tetrachloride ND 1.00 ug/L 01/13/15 20:36 1ChlorobenzeneND 1.00 ug/L 01/13/15 20:36 1ChlorodibromomethaneND 1.00 ug/L 01/13/15 20:36 1ChloroethaneND 1.00 ug/L 01/13/15 20:36 1ChloroformND 1.00 ug/L 01/13/15 20:36 1ChloromethaneND 1.00 ug/L 01/13/15 20:36 12-Chlorotoluene ND 1.00 ug/L 01/13/15 20:36 14-Chlorotoluene ND 1.00 ug/L 01/13/15 20:36 1cis-1,2-Dichloroethene ND 1.00 ug/L 01/13/15 20:36 1cis-1,3-Dichloropropene ND 10.0 ug/L 01/13/15 20:36 11,2-Dibromo-3-Chloropropane ND 1.00 ug/L 01/13/15 20:36 11,2-Dibromoethane (EDB)ND 1.00 ug/L 01/13/15 20:36 1DibromomethaneND 1.00 ug/L 01/13/15 20:36 11,2-Dichlorobenzene ND 1.00 ug/L 01/13/15 20:36 11,3-Dichlorobenzene ND 1.00 ug/L 01/13/15 20:36 11,4-Dichlorobenzene ND 1.00 ug/L 01/13/15 20:36 1DichlorodifluoromethaneND 1.00 ug/L 01/13/15 20:36 11,1-Dichloroethane ND 1.00 ug/L 01/13/15 20:36 11,2-Dichloroethane ND 1.00 ug/L 01/13/15 20:36 11,1-Dichloroethene ND 1.00 ug/L 01/13/15 20:36 11,2-Dichloroethene, Total ND 1.00 ug/L 01/13/15 20:36 11,2-Dichloropropane ND 1.00 ug/L 01/13/15 20:36 11,3-Dichloropropane ND 1.00 ug/L 01/13/15 20:36 12,2-Dichloropropane ND 1.00 ug/L 01/13/15 20:36 11,1-Dichloropropene ND 2.00 ug/L 01/13/15 20:36 1Diisopropyl ether ND 1.00 ug/L 01/13/15 20:36 1EthylbenzeneND 2.00 ug/L 01/13/15 20:36 1HexachlorobutadieneND 10.0 ug/L 01/13/15 20:36 12-Hexanone ND 1.00 ug/L 01/13/15 20:36 1IsopropylbenzeneND 5.00 ug/L 01/13/15 20:36 1Methylene Chloride ND 10.0 ug/L 01/13/15 20:36 14-Methyl-2-pentanone (MIBK)ND 1.00 ug/L 01/13/15 20:36 1Methyl tert-butyl ether ND 5.00 ug/L 01/13/15 20:36 1NaphthaleneND 1.00 ug/L 01/13/15 20:36 1n-Butylbenzene ND 1.00 ug/L 01/13/15 20:36 1N-Propylbenzene ND 1.00 ug/L 01/13/15 20:36 1p-Isopropyltoluene ND 1.00 ug/L 01/13/15 20:36 1sec-Butylbenzene ND 1.00 ug/L 01/13/15 20:36 1StyreneND 1.00 ug/L 01/13/15 20:36 1tert-Butylbenzene ND TestAmerica Nashville Page 9 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Lab Sample ID: 490-70180-2Client Sample ID: TMW-3 Matrix: WaterDate Collected: 01/09/15 12:45 Date Received: 01/10/15 08:45 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 1.00 ug/L 01/13/15 20:36 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 1.00 ug/L 01/13/15 20:36 11,1,2,2-Tetrachloroethane ND 1.00 ug/L 01/13/15 20:36 1TetrachloroetheneND 1.00 ug/L 01/13/15 20:36 1TolueneND 1.00 ug/L 01/13/15 20:36 1trans-1,2-Dichloroethene ND 1.00 ug/L 01/13/15 20:36 1trans-1,3-Dichloropropene ND 1.00 ug/L 01/13/15 20:36 11,2,3-Trichlorobenzene ND 1.00 ug/L 01/13/15 20:36 11,2,4-Trichlorobenzene ND 1.00 ug/L 01/13/15 20:36 11,1,1-Trichloroethane ND 1.00 ug/L 01/13/15 20:36 11,1,2-Trichloroethane ND 1.00 ug/L 01/13/15 20:36 1TrichloroetheneND 1.00 ug/L 01/13/15 20:36 1TrichlorofluoromethaneND 1.00 ug/L 01/13/15 20:36 11,2,3-Trichloropropane ND 1.00 ug/L 01/13/15 20:36 11,2,4-Trimethylbenzene ND 1.00 ug/L 01/13/15 20:36 11,3,5-Trimethylbenzene ND 1.00 ug/L 01/13/15 20:36 1Vinyl chloride ND 2.00 ug/L 01/13/15 20:36 1Xylenes, Total ND 4-Bromofluorobenzene (Surr)87 70-130 01/13/15 20:36 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Dibromofluoromethane (Surr)104 01/13/15 20:36 170-130 1,2-Dichloroethane-d4 (Surr)98 01/13/15 20:36 170-130 Toluene-d8 (Surr)105 01/13/15 20:36 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 1.61 ug/L 01/13/15 08:23 01/14/15 15:06 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 1.61 ug/L 01/13/15 08:23 01/14/15 15:06 1AcenaphthyleneND 1.61 ug/L 01/13/15 08:23 01/14/15 15:06 1AnthraceneND 1.61 ug/L 01/13/15 08:23 01/14/15 15:06 1Benzo[a]anthracene ND 1.61 ug/L 01/13/15 08:23 01/14/15 15:06 1Benzo[a]pyrene ND 1.61 ug/L 01/13/15 08:23 01/14/15 15:06 1Benzo[b]fluoranthene ND 1.61 ug/L 01/13/15 08:23 01/14/15 15:06 1Benzo[g,h,i]perylene ND 1.61 ug/L 01/13/15 08:23 01/14/15 15:06 1Benzo[k]fluoranthene ND 1.61 ug/L 01/13/15 08:23 01/14/15 15:06 1ChryseneND 1.61 ug/L 01/13/15 08:23 01/14/15 15:06 1Dibenz(a,h)anthracene ND 1.61 ug/L 01/13/15 08:23 01/14/15 15:06 1FluorantheneND 1.61 ug/L 01/13/15 08:23 01/14/15 15:06 1FluoreneND 1.61 ug/L 01/13/15 08:23 01/14/15 15:06 1Indeno[1,2,3-cd]pyrene ND 1.61 ug/L 01/13/15 08:23 01/14/15 15:06 1NaphthaleneND 1.61 ug/L 01/13/15 08:23 01/14/15 15:06 1PhenanthreneND 1.61 ug/L 01/13/15 08:23 01/14/15 15:06 1PyreneND 2-Fluorobiphenyl (Surr)66 29-120 01/13/15 08:23 01/14/15 15:06 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Nitrobenzene-d5 (Surr)59 01/13/15 08:23 01/14/15 15:06 127-120 Terphenyl-d14 (Surr)74 01/13/15 08:23 01/14/15 15:06 113-120 TestAmerica Nashville Page 10 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Lab Sample ID: 490-70180-2Client Sample ID: TMW-3 Matrix: WaterDate Collected: 01/09/15 12:45 Date Received: 01/10/15 08:45 Method: 6010C - Metals (ICP) RL MDL Manganese 0.0578 0.0150 mg/L 01/13/15 07:42 01/13/15 15:47 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 0.00500 mg/L 01/13/15 07:42 01/13/15 15:47 1LeadND TestAmerica Nashville Page 11 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Lab Sample ID: 490-70180-3Client Sample ID: WSW-1 Matrix: WaterDate Collected: 01/09/15 13:25 Date Received: 01/10/15 08:45 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone ND 25.0 ug/L 01/13/15 14:26 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 1.00 ug/L 01/13/15 14:26 1BenzeneND 1.00 ug/L 01/13/15 14:26 1BromobenzeneND 1.00 ug/L 01/13/15 14:26 1BromochloromethaneND 1.00 ug/L 01/13/15 14:26 1BromodichloromethaneND 1.00 ug/L 01/13/15 14:26 1BromoformND 1.00 ug/L 01/13/15 14:26 1BromomethaneND 50.0 ug/L 01/13/15 14:26 12-Butanone (MEK)ND 1.00 ug/L 01/13/15 14:26 1Carbon disulfide ND 1.00 ug/L 01/13/15 14:26 1Carbon tetrachloride ND 1.00 ug/L 01/13/15 14:26 1ChlorobenzeneND 1.00 ug/L 01/13/15 14:26 1ChlorodibromomethaneND 1.00 ug/L 01/13/15 14:26 1ChloroethaneND 1.00 ug/L 01/13/15 14:26 1ChloroformND 1.00 ug/L 01/13/15 14:26 1ChloromethaneND 1.00 ug/L 01/13/15 14:26 12-Chlorotoluene ND 1.00 ug/L 01/13/15 14:26 14-Chlorotoluene ND 1.00 ug/L 01/13/15 14:26 1cis-1,2-Dichloroethene ND 1.00 ug/L 01/13/15 14:26 1cis-1,3-Dichloropropene ND 10.0 ug/L 01/13/15 14:26 11,2-Dibromo-3-Chloropropane ND 1.00 ug/L 01/13/15 14:26 11,2-Dibromoethane (EDB)ND 1.00 ug/L 01/13/15 14:26 1DibromomethaneND 1.00 ug/L 01/13/15 14:26 11,2-Dichlorobenzene ND 1.00 ug/L 01/13/15 14:26 11,3-Dichlorobenzene ND 1.00 ug/L 01/13/15 14:26 11,4-Dichlorobenzene ND 1.00 ug/L 01/13/15 14:26 1DichlorodifluoromethaneND 1.00 ug/L 01/13/15 14:26 11,1-Dichloroethane ND 1.00 ug/L 01/13/15 14:26 11,2-Dichloroethane ND 1.00 ug/L 01/13/15 14:26 11,1-Dichloroethene ND 1.00 ug/L 01/13/15 14:26 11,2-Dichloroethene, Total ND 1.00 ug/L 01/13/15 14:26 11,2-Dichloropropane ND 1.00 ug/L 01/13/15 14:26 11,3-Dichloropropane ND 1.00 ug/L 01/13/15 14:26 12,2-Dichloropropane ND 1.00 ug/L 01/13/15 14:26 11,1-Dichloropropene ND 2.00 ug/L 01/13/15 14:26 1Diisopropyl ether ND 1.00 ug/L 01/13/15 14:26 1EthylbenzeneND 2.00 ug/L 01/13/15 14:26 1HexachlorobutadieneND 10.0 ug/L 01/13/15 14:26 12-Hexanone ND 1.00 ug/L 01/13/15 14:26 1IsopropylbenzeneND 5.00 ug/L 01/13/15 14:26 1Methylene Chloride ND 10.0 ug/L 01/13/15 14:26 14-Methyl-2-pentanone (MIBK)ND 1.00 ug/L 01/13/15 14:26 1Methyl tert-butyl ether ND 5.00 ug/L 01/13/15 14:26 1NaphthaleneND 1.00 ug/L 01/13/15 14:26 1n-Butylbenzene ND 1.00 ug/L 01/13/15 14:26 1N-Propylbenzene ND 1.00 ug/L 01/13/15 14:26 1p-Isopropyltoluene ND 1.00 ug/L 01/13/15 14:26 1sec-Butylbenzene ND 1.00 ug/L 01/13/15 14:26 1StyreneND 1.00 ug/L 01/13/15 14:26 1tert-Butylbenzene ND TestAmerica Nashville Page 12 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Lab Sample ID: 490-70180-3Client Sample ID: WSW-1 Matrix: WaterDate Collected: 01/09/15 13:25 Date Received: 01/10/15 08:45 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 1.00 ug/L 01/13/15 14:26 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 1.00 ug/L 01/13/15 14:26 11,1,2,2-Tetrachloroethane ND 1.00 ug/L 01/13/15 14:26 1TetrachloroetheneND 1.00 ug/L 01/13/15 14:26 1TolueneND 1.00 ug/L 01/13/15 14:26 1trans-1,2-Dichloroethene ND 1.00 ug/L 01/13/15 14:26 1trans-1,3-Dichloropropene ND 1.00 ug/L 01/13/15 14:26 11,2,3-Trichlorobenzene ND 1.00 ug/L 01/13/15 14:26 11,2,4-Trichlorobenzene ND 1.00 ug/L 01/13/15 14:26 11,1,1-Trichloroethane ND 1.00 ug/L 01/13/15 14:26 11,1,2-Trichloroethane ND 1.00 ug/L 01/13/15 14:26 1TrichloroetheneND 1.00 ug/L 01/13/15 14:26 1TrichlorofluoromethaneND 1.00 ug/L 01/13/15 14:26 11,2,3-Trichloropropane ND 1.00 ug/L 01/13/15 14:26 11,2,4-Trimethylbenzene ND 1.00 ug/L 01/13/15 14:26 11,3,5-Trimethylbenzene ND 1.00 ug/L 01/13/15 14:26 1Vinyl chloride ND 2.00 ug/L 01/13/15 14:26 1Xylenes, Total ND 4-Bromofluorobenzene (Surr)88 70-130 01/13/15 14:26 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Dibromofluoromethane (Surr)105 01/13/15 14:26 170-130 1,2-Dichloroethane-d4 (Surr)93 01/13/15 14:26 170-130 Toluene-d8 (Surr)93 01/13/15 14:26 170-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 2.04 ug/L 01/13/15 07:26 01/21/15 01:45 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 2.04 ug/L 01/13/15 07:26 01/21/15 01:45 1AcenaphthyleneND 2.04 ug/L 01/13/15 07:26 01/21/15 01:45 1AnthraceneND 2.04 ug/L 01/13/15 07:26 01/21/15 01:45 1Benzo[a]anthracene ND 2.04 ug/L 01/13/15 07:26 01/21/15 01:45 1Benzo[a]pyrene ND 2.04 ug/L 01/13/15 07:26 01/21/15 01:45 1Benzo[b]fluoranthene ND 2.04 ug/L 01/13/15 07:26 01/21/15 01:45 1Benzo[g,h,i]perylene ND 2.04 ug/L 01/13/15 07:26 01/21/15 01:45 1Benzo[k]fluoranthene ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1Bis(2-chloroethoxy)methane ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1Bis(2-chloroethyl)ether ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1bis (2-chloroisopropyl) ether ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1Bis(2-ethylhexyl) phthalate ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 14-Bromophenyl phenyl ether ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1Butyl benzyl phthalate ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1CarbazoleND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 14-Chloroaniline ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 14-Chloro-3-methylphenol ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 12-Chloronaphthalene ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 12-Chlorophenol ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 14-Chlorophenyl phenyl ether ND 2.04 ug/L 01/13/15 07:26 01/21/15 01:45 1ChryseneND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1CresolsND 2.04 ug/L 01/13/15 07:26 01/21/15 01:45 1Dibenz(a,h)anthracene ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1DibenzofuranND TestAmerica Nashville Page 13 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Lab Sample ID: 490-70180-3Client Sample ID: WSW-1 Matrix: WaterDate Collected: 01/09/15 13:25 Date Received: 01/10/15 08:45 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 1,2-Dichlorobenzene ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 11,3-Dichlorobenzene ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 11,4-Dichlorobenzene ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 13,3'-Dichlorobenzidine ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 12,4-Dichlorophenol ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1Diethyl phthalate ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 12,4-Dimethylphenol ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1Dimethyl phthalate ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1Di-n-butyl phthalate ND 25.5 ug/L 01/13/15 07:26 01/21/15 01:45 14,6-Dinitro-2-methylphenol ND 25.5 ug/L 01/13/15 07:26 01/21/15 01:45 12,4-Dinitrophenol ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 12,4-Dinitrotoluene ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 12,6-Dinitrotoluene ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1Di-n-octyl phthalate ND 2.04 ug/L 01/13/15 07:26 01/21/15 01:45 1FluorantheneND 2.04 ug/L 01/13/15 07:26 01/21/15 01:45 1FluoreneND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1HexachlorobenzeneND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1HexachlorobutadieneND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1HexachlorocyclopentadieneND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1HexachloroethaneND 2.04 ug/L 01/13/15 07:26 01/21/15 01:45 1Indeno[1,2,3-cd]pyrene ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1IsophoroneND 2.04 ug/L 01/13/15 07:26 01/21/15 01:45 11-Methylnaphthalene ND 2.04 ug/L 01/13/15 07:26 01/21/15 01:45 12-Methylnaphthalene ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 12-Methylphenol ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 13 & 4 Methylphenol ND 2.04 ug/L 01/13/15 07:26 01/21/15 01:45 1NaphthaleneND 25.5 ug/L 01/13/15 07:26 01/21/15 01:45 12-Nitroaniline ND 25.5 ug/L 01/13/15 07:26 01/21/15 01:45 13-Nitroaniline ND 25.5 ug/L 01/13/15 07:26 01/21/15 01:45 14-Nitroaniline ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1NitrobenzeneND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 12-Nitrophenol ND 25.5 ug/L 01/13/15 07:26 01/21/15 01:45 14-Nitrophenol ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1N-Nitrosodi-n-propylamine ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1n-Nitrosodiphenylamine(as diphenylamine) ND 25.5 ug/L 01/13/15 07:26 01/21/15 01:45 1PentachlorophenolND 2.04 ug/L 01/13/15 07:26 01/21/15 01:45 1PhenanthreneND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 1PhenolND 2.04 ug/L 01/13/15 07:26 01/21/15 01:45 1PyreneND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 11,2,4-Trichlorobenzene ND 25.5 ug/L 01/13/15 07:26 01/21/15 01:45 12,4,5-Trichlorophenol ND 10.2 ug/L 01/13/15 07:26 01/21/15 01:45 12,4,6-Trichlorophenol ND 2-Fluorobiphenyl (Surr)60 29-120 01/13/15 07:26 01/21/15 01:45 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery 2-Fluorophenol (Surr)34 01/13/15 07:26 01/21/15 01:45 110-120 Nitrobenzene-d5 (Surr)57 01/13/15 07:26 01/21/15 01:45 127-120 Phenol-d5 (Surr)23 01/13/15 07:26 01/21/15 01:45 110-120 Terphenyl-d14 (Surr)63 01/13/15 07:26 01/21/15 01:45 113-120 TestAmerica Nashville Page 14 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Lab Sample ID: 490-70180-3Client Sample ID: WSW-1 Matrix: WaterDate Collected: 01/09/15 13:25 Date Received: 01/10/15 08:45 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) 2,4,6-Tribromophenol (Surr)66 10-120 01/13/15 07:26 01/21/15 01:45 1 Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery Method: 6010C - Metals (ICP) RL MDL Antimony ND 0.0100 mg/L 01/13/15 07:42 01/13/15 15:52 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier 0.0100 mg/L 01/13/15 07:42 01/13/15 15:52 1ArsenicND 0.00400 mg/L 01/13/15 07:42 01/13/15 15:52 1BerylliumND 0.00100 mg/L 01/13/15 07:42 01/13/15 15:52 1CadmiumND 0.00500 mg/L 01/13/15 07:42 01/13/15 15:52 1ChromiumND 0.0100 mg/L 01/13/15 07:42 01/13/15 15:52 1Copper0.0542 0.00500 mg/L 01/13/15 07:42 01/13/15 15:52 1Lead0.0283 0.0150 mg/L 01/13/15 07:42 01/13/15 15:52 1ManganeseND 0.0100 mg/L 01/13/15 07:42 01/13/15 15:52 1NickelND 0.0100 mg/L 01/13/15 07:42 01/13/15 15:52 1SeleniumND 0.00500 mg/L 01/13/15 07:42 01/13/15 15:52 1SilverND 0.0100 mg/L 01/16/15 08:12 01/19/15 15:39 1ThalliumND 0.0500 mg/L 01/13/15 07:42 01/13/15 15:52 1Zinc0.117 Method: 7470A - Mercury (CVAA) RL MDL Mercury ND 0.00200 mg/L 01/14/15 10:48 01/15/15 18:55 1 Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier TestAmerica Nashville Page 15 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Method: 8260B - Volatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 490-219934/7 Matrix: Water Prep Type: Total/NA Analysis Batch: 219934 RL MDL Acetone ND 25.0 ug/L 01/13/15 12:04 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 1.00 ug/L 01/13/15 12:04 1Benzene ND 1.00 ug/L 01/13/15 12:04 1Bromobenzene ND 1.00 ug/L 01/13/15 12:04 1Bromochloromethane ND 1.00 ug/L 01/13/15 12:04 1Bromodichloromethane ND 1.00 ug/L 01/13/15 12:04 1Bromoform ND 1.00 ug/L 01/13/15 12:04 1Bromomethane ND 50.0 ug/L 01/13/15 12:04 12-Butanone (MEK) ND 1.00 ug/L 01/13/15 12:04 1Carbon disulfide ND 1.00 ug/L 01/13/15 12:04 1Carbon tetrachloride ND 1.00 ug/L 01/13/15 12:04 1Chlorobenzene ND 1.00 ug/L 01/13/15 12:04 1Chlorodibromomethane ND 1.00 ug/L 01/13/15 12:04 1Chloroethane ND 1.00 ug/L 01/13/15 12:04 1Chloroform ND 1.00 ug/L 01/13/15 12:04 1Chloromethane ND 1.00 ug/L 01/13/15 12:04 12-Chlorotoluene ND 1.00 ug/L 01/13/15 12:04 14-Chlorotoluene ND 1.00 ug/L 01/13/15 12:04 1cis-1,2-Dichloroethene ND 1.00 ug/L 01/13/15 12:04 1cis-1,3-Dichloropropene ND 10.0 ug/L 01/13/15 12:04 11,2-Dibromo-3-Chloropropane ND 1.00 ug/L 01/13/15 12:04 11,2-Dibromoethane (EDB) ND 1.00 ug/L 01/13/15 12:04 1Dibromomethane ND 1.00 ug/L 01/13/15 12:04 11,2-Dichlorobenzene ND 1.00 ug/L 01/13/15 12:04 11,3-Dichlorobenzene ND 1.00 ug/L 01/13/15 12:04 11,4-Dichlorobenzene ND 1.00 ug/L 01/13/15 12:04 1Dichlorodifluoromethane ND 1.00 ug/L 01/13/15 12:04 11,1-Dichloroethane ND 1.00 ug/L 01/13/15 12:04 11,2-Dichloroethane ND 1.00 ug/L 01/13/15 12:04 11,1-Dichloroethene ND 1.00 ug/L 01/13/15 12:04 11,2-Dichloroethene, Total ND 1.00 ug/L 01/13/15 12:04 11,2-Dichloropropane ND 1.00 ug/L 01/13/15 12:04 11,3-Dichloropropane ND 1.00 ug/L 01/13/15 12:04 12,2-Dichloropropane ND 1.00 ug/L 01/13/15 12:04 11,1-Dichloropropene ND 2.00 ug/L 01/13/15 12:04 1Diisopropyl ether ND 1.00 ug/L 01/13/15 12:04 1Ethylbenzene ND 2.00 ug/L 01/13/15 12:04 1Hexachlorobutadiene ND 10.0 ug/L 01/13/15 12:04 12-Hexanone ND 1.00 ug/L 01/13/15 12:04 1Isopropylbenzene ND 5.00 ug/L 01/13/15 12:04 1Methylene Chloride ND 10.0 ug/L 01/13/15 12:04 14-Methyl-2-pentanone (MIBK) ND 1.00 ug/L 01/13/15 12:04 1Methyl tert-butyl ether ND 5.00 ug/L 01/13/15 12:04 1Naphthalene ND 1.00 ug/L 01/13/15 12:04 1n-Butylbenzene ND 1.00 ug/L 01/13/15 12:04 1N-Propylbenzene ND 1.00 ug/L 01/13/15 12:04 1p-Isopropyltoluene ND 1.00 ug/L 01/13/15 12:04 1sec-Butylbenzene ND 1.00 ug/L 01/13/15 12:04 1Styrene TestAmerica Nashville Page 16 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-219934/7 Matrix: Water Prep Type: Total/NA Analysis Batch: 219934 RL MDL tert-Butylbenzene ND 1.00 ug/L 01/13/15 12:04 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 1.00 ug/L 01/13/15 12:04 11,1,1,2-Tetrachloroethane ND 1.00 ug/L 01/13/15 12:04 11,1,2,2-Tetrachloroethane ND 1.00 ug/L 01/13/15 12:04 1Tetrachloroethene ND 1.00 ug/L 01/13/15 12:04 1Toluene ND 1.00 ug/L 01/13/15 12:04 1trans-1,2-Dichloroethene ND 1.00 ug/L 01/13/15 12:04 1trans-1,3-Dichloropropene ND 1.00 ug/L 01/13/15 12:04 11,2,3-Trichlorobenzene ND 1.00 ug/L 01/13/15 12:04 11,2,4-Trichlorobenzene ND 1.00 ug/L 01/13/15 12:04 11,1,1-Trichloroethane ND 1.00 ug/L 01/13/15 12:04 11,1,2-Trichloroethane ND 1.00 ug/L 01/13/15 12:04 1Trichloroethene ND 1.00 ug/L 01/13/15 12:04 1Trichlorofluoromethane ND 1.00 ug/L 01/13/15 12:04 11,2,3-Trichloropropane ND 1.00 ug/L 01/13/15 12:04 11,2,4-Trimethylbenzene ND 1.00 ug/L 01/13/15 12:04 11,3,5-Trimethylbenzene ND 1.00 ug/L 01/13/15 12:04 1Vinyl chloride ND 2.00 ug/L 01/13/15 12:04 1Xylenes, Total 4-Bromofluorobenzene (Surr)89 70-130 01/13/15 12:04 1 MB MB Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery 106 01/13/15 12:04 1Dibromofluoromethane (Surr)70-130 96 01/13/15 12:04 11,2-Dichloroethane-d4 (Surr)70-130 103 01/13/15 12:04 1Toluene-d8 (Surr)70-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-219934/3 Matrix: Water Prep Type: Total/NA Analysis Batch: 219934 Acetone 250 181.3 ug/L 73 54 -145 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Benzene 50.0 50.00 ug/L 100 80 -121 Bromobenzene 50.0 55.07 ug/L 110 68 -130 Bromochloromethane 50.0 49.57 ug/L 99 78 -129 Bromodichloromethane 50.0 50.16 ug/L 100 75 -129 Bromoform 50.0 50.97 ug/L 102 46 -145 Bromomethane 50.0 43.21 ug/L 86 41 -150 2-Butanone (MEK)250 216.2 ug/L 86 62 -133 Carbon disulfide 50.0 41.15 ug/L 82 77 -126 Carbon tetrachloride 50.0 47.94 ug/L 96 64 -147 Chlorobenzene 50.0 54.55 ug/L 109 80 -120 Chlorodibromomethane 50.0 53.70 ug/L 107 69 -133 Chloroethane 50.0 46.54 ug/L 93 72 -120 Chloroform 50.0 46.52 ug/L 93 73 -129 Chloromethane 50.0 42.78 ug/L 86 12 -150 2-Chlorotoluene 50.0 59.24 ug/L 118 75 -126 4-Chlorotoluene 50.0 59.06 ug/L 118 75 -130 cis-1,2-Dichloroethene 50.0 48.80 ug/L 98 76 -125 TestAmerica Nashville Page 17 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-219934/3 Matrix: Water Prep Type: Total/NA Analysis Batch: 219934 cis-1,3-Dichloropropene 50.0 54.48 ug/L 109 74 -140 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits 1,2-Dibromo-3-Chloropropane 50.0 53.17 ug/L 106 54 -125 1,2-Dibromoethane (EDB)50.0 49.79 ug/L 100 80 -129 Dibromomethane 50.0 48.03 ug/L 96 71 -125 1,2-Dichlorobenzene 50.0 53.83 ug/L 108 80 -121 1,3-Dichlorobenzene 50.0 55.59 ug/L 111 80 -122 1,4-Dichlorobenzene 50.0 53.99 ug/L 108 80 -120 Dichlorodifluoromethane 50.0 48.32 ug/L 97 37 -127 1,1-Dichloroethane 50.0 44.54 ug/L 89 78 -125 1,2-Dichloroethane 50.0 45.42 ug/L 91 77 -121 1,1-Dichloroethene 50.0 43.78 ug/L 88 79 -124 1,2-Dichloroethene, Total 100 89.75 ug/L 90 78 -126 1,2-Dichloropropane 50.0 49.32 ug/L 99 75 -120 1,3-Dichloropropane 50.0 51.24 ug/L 102 80 -125 2,2-Dichloropropane 50.0 49.80 ug/L 100 43 -161 1,1-Dichloropropene 50.0 50.03 ug/L 100 80 -122 Diisopropyl ether 50.0 44.55 ug/L 89 61 -142 Ethylbenzene 50.0 55.83 ug/L 112 80 -130 Hexachlorobutadiene 50.0 54.72 ug/L 109 49 -146 2-Hexanone 250 239.7 ug/L 96 60 -142 Isopropylbenzene 50.0 52.83 ug/L 106 80 -141 Methylene Chloride 50.0 42.25 ug/L 84 79 -123 4-Methyl-2-pentanone (MIBK)250 237.5 ug/L 95 60 -137 Methyl tert-butyl ether 50.0 42.45 ug/L 85 72 -133 Naphthalene 50.0 53.94 ug/L 108 62 -138 n-Butylbenzene 50.0 54.77 ug/L 110 68 -132 N-Propylbenzene 50.0 61.23 ug/L 122 75 -129 p-Isopropyltoluene 50.0 56.45 ug/L 113 75 -128 sec-Butylbenzene 50.0 57.53 ug/L 115 76 -128 Styrene 50.0 56.25 ug/L 113 80 -127 tert-Butylbenzene 50.0 61.63 ug/L 123 76 -126 1,1,1,2-Tetrachloroethane 50.0 53.40 ug/L 107 74 -135 1,1,2,2-Tetrachloroethane 50.0 49.24 ug/L 98 69 -131 Tetrachloroethene 50.0 56.21 ug/L 112 80 -126 Toluene 50.0 55.85 ug/L 112 80 -126 trans-1,2-Dichloroethene 50.0 40.95 ug/L 82 79 -126 trans-1,3-Dichloropropene 50.0 53.45 ug/L 107 63 -134 1,2,3-Trichlorobenzene 50.0 60.71 ug/L 121 62 -133 1,2,4-Trichlorobenzene 50.0 53.01 ug/L 106 63 -133 1,1,1-Trichloroethane 50.0 49.39 ug/L 99 78 -135 1,1,2-Trichloroethane 50.0 50.95 ug/L 102 80 -124 Trichloroethene 50.0 52.24 ug/L 104 80 -123 Trichlorofluoromethane 50.0 43.58 ug/L 87 65 -124 1,2,3-Trichloropropane 50.0 51.55 ug/L 103 70 -131 1,2,4-Trimethylbenzene 50.0 56.61 ug/L 113 77 -126 1,3,5-Trimethylbenzene 50.0 56.52 ug/L 113 77 -127 Vinyl chloride 50.0 46.51 ug/L 93 68 -120 Xylenes, Total 100 110.6 ug/L 111 80 -132 TestAmerica Nashville Page 18 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-219934/3 Matrix: Water Prep Type: Total/NA Analysis Batch: 219934 4-Bromofluorobenzene (Surr)70 -130 Surrogate 90 LCS LCS Qualifier Limits%Recovery 101Dibromofluoromethane (Surr)70 -130 931,2-Dichloroethane-d4 (Surr)70 -130 106Toluene-d8 (Surr)70 -130 Client Sample ID: WSW-1Lab Sample ID: 490-70180-3 MS Matrix: Water Prep Type: Total/NA Analysis Batch: 219934 Acetone ND 250 169.4 ug/L 68 45 -141 Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Benzene ND 50.0 47.61 ug/L 95 75 -133 Bromobenzene ND 50.0 53.28 ug/L 107 60 -138 Bromochloromethane ND 50.0 51.17 ug/L 102 67 -139 Bromodichloromethane ND 50.0 51.40 ug/L 103 70 -140 Bromoform ND 50.0 49.23 ug/L 98 42 -147 Bromomethane ND 50.0 41.31 ug/L 83 16 -163 2-Butanone (MEK)ND 250 203.9 ug/L 82 50 -138 Carbon disulfide ND 50.0 44.08 ug/L 88 48 -152 Carbon tetrachloride ND 50.0 46.06 ug/L 92 62 -164 Chlorobenzene ND 50.0 54.32 ug/L 109 80 -129 Chlorodibromomethane ND 50.0 51.35 ug/L 103 66 -140 Chloroethane ND 50.0 49.15 ug/L 98 58 -137 Chloroform ND 50.0 48.40 ug/L 97 66 -138 Chloromethane ND 50.0 44.80 ug/L 90 10 -169 2-Chlorotoluene ND 50.0 60.15 ug/L 120 67 -138 4-Chlorotoluene ND 50.0 59.10 ug/L 118 69 -138 cis-1,2-Dichloroethene ND 50.0 49.38 ug/L 99 68 -138 cis-1,3-Dichloropropene ND 50.0 51.66 ug/L 103 71 -141 1,2-Dibromo-3-Chloropropane ND 50.0 48.70 ug/L 97 52 -126 1,2-Dibromoethane (EDB)ND 50.0 48.64 ug/L 97 75 -137 Dibromomethane ND 50.0 49.10 ug/L 98 58 -140 1,2-Dichlorobenzene ND 50.0 53.80 ug/L 108 79 -128 1,3-Dichlorobenzene ND 50.0 55.54 ug/L 111 77 -131 1,4-Dichlorobenzene ND 50.0 53.81 ug/L 108 78 -126 Dichlorodifluoromethane ND 50.0 49.99 ug/L 100 40 -127 1,1-Dichloroethane ND 50.0 48.95 ug/L 98 71 -139 1,2-Dichloroethane ND 50.0 43.52 ug/L 87 64 -136 1,1-Dichloroethene ND 50.0 52.09 ug/L 104 70 -142 1,2-Dichloroethene, Total ND 100 96.96 ug/L 97 60 -152 1,2-Dichloropropane ND 50.0 49.46 ug/L 99 67 -131 1,3-Dichloropropane ND 50.0 49.27 ug/L 99 72 -134 2,2-Dichloropropane ND 50.0 49.24 ug/L 98 37 -175 1,1-Dichloropropene ND 50.0 49.12 ug/L 98 76 -139 Diisopropyl ether ND 50.0 44.84 ug/L 90 10 -200 Ethylbenzene ND 50.0 57.02 ug/L 114 79 -139 Hexachlorobutadiene ND 50.0 56.79 ug/L 114 45 -155 2-Hexanone ND 250 210.7 ug/L 84 50 -150 TestAmerica Nashville Page 19 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: WSW-1Lab Sample ID: 490-70180-3 MS Matrix: Water Prep Type: Total/NA Analysis Batch: 219934 Isopropylbenzene ND 50.0 54.23 ug/L 108 80 -153 Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Methylene Chloride ND 50.0 46.56 ug/L 93 64 -139 4-Methyl-2-pentanone (MIBK)ND 250 216.9 ug/L 87 50 -147 Methyl tert-butyl ether ND 50.0 45.64 ug/L 91 66 -141 Naphthalene ND 50.0 48.65 ug/L 97 55 -140 n-Butylbenzene ND 50.0 55.42 ug/L 111 66 -141 N-Propylbenzene ND 50.0 62.35 ug/L 125 69 -142 p-Isopropyltoluene ND 50.0 57.46 ug/L 115 71 -137 sec-Butylbenzene ND 50.0 58.75 ug/L 118 73 -138 Styrene ND 50.0 56.93 ug/L 114 61 -148 tert-Butylbenzene ND 50.0 62.81 ug/L 126 70 -138 1,1,1,2-Tetrachloroethane ND 50.0 53.73 ug/L 107 73 -141 1,1,2,2-Tetrachloroethane ND 50.0 46.59 ug/L 93 56 -143 Tetrachloroethene ND 50.0 59.12 ug/L 118 72 -145 Toluene ND 50.0 55.78 ug/L 112 75 -136 trans-1,2-Dichloroethene ND 50.0 47.58 ug/L 95 66 -143 trans-1,3-Dichloropropene ND 50.0 50.76 ug/L 102 59 -135 1,2,3-Trichlorobenzene ND 50.0 56.48 ug/L 113 55 -138 1,2,4-Trichlorobenzene ND 50.0 49.87 ug/L 100 60 -136 1,1,1-Trichloroethane ND 50.0 48.68 ug/L 97 76 -149 1,1,2-Trichloroethane ND 50.0 49.58 ug/L 99 74 -134 Trichloroethene ND 50.0 55.89 ug/L 112 73 -144 Trichlorofluoromethane ND 50.0 54.65 ug/L 109 58 -139 1,2,3-Trichloropropane ND 50.0 50.03 ug/L 100 53 -144 1,2,4-Trimethylbenzene ND 50.0 56.67 ug/L 113 69 -136 1,3,5-Trimethylbenzene ND 50.0 56.52 ug/L 113 69 -139 Vinyl chloride ND 50.0 49.17 ug/L 98 56 -129 Xylenes, Total ND 100 113.5 ug/L 114 74 -141 4-Bromofluorobenzene (Surr)70 -130 Surrogate 88 MS MS Qualifier Limits%Recovery 97Dibromofluoromethane (Surr)70 -130 901,2-Dichloroethane-d4 (Surr)70 -130 104Toluene-d8 (Surr)70 -130 Client Sample ID: WSW-1Lab Sample ID: 490-70180-3 MSD Matrix: Water Prep Type: Total/NA Analysis Batch: 219934 Acetone ND 250 199.1 ug/L 80 45 -141 16 21 Analyte MSD MSD DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Benzene ND 50.0 58.79 F2 ug/L 118 75 -133 21 17 Bromobenzene ND 50.0 57.31 ug/L 115 60 -138 7 20 Bromochloromethane ND 50.0 60.64 ug/L 121 67 -139 17 17 Bromodichloromethane ND 50.0 59.93 ug/L 120 70 -140 15 18 Bromoform ND 50.0 52.75 ug/L 105 42 -147 7 16 Bromomethane ND 50.0 53.91 ug/L 108 16 -163 26 50 2-Butanone (MEK)ND 250 219.7 ug/L 88 50 -138 7 19 TestAmerica Nashville Page 20 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: WSW-1Lab Sample ID: 490-70180-3 MSD Matrix: Water Prep Type: Total/NA Analysis Batch: 219934 Carbon disulfide ND 50.0 55.58 F2 ug/L 111 48 -152 23 21 Analyte MSD MSD DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Carbon tetrachloride ND 50.0 60.16 F2 ug/L 120 62 -164 27 19 Chlorobenzene ND 50.0 57.72 ug/L 115 80 -129 6 14 Chlorodibromomethane ND 50.0 55.10 ug/L 110 66 -140 7 15 Chloroethane ND 50.0 56.75 ug/L 114 58 -137 14 20 Chloroform ND 50.0 57.04 ug/L 114 66 -138 16 18 Chloromethane ND 50.0 53.90 ug/L 108 10 -169 18 31 2-Chlorotoluene ND 50.0 63.52 ug/L 127 67 -138 5 17 4-Chlorotoluene ND 50.0 62.63 ug/L 125 69 -138 6 18 cis-1,2-Dichloroethene ND 50.0 53.71 ug/L 107 68 -138 8 17 cis-1,3-Dichloropropene ND 50.0 54.91 ug/L 110 71 -141 6 15 1,2-Dibromo-3-Chloropropane ND 50.0 52.59 ug/L 105 52 -126 8 24 1,2-Dibromoethane (EDB)ND 50.0 51.79 ug/L 104 75 -137 6 15 Dibromomethane ND 50.0 57.52 ug/L 115 58 -140 16 16 1,2-Dichlorobenzene ND 50.0 57.16 ug/L 114 79 -128 6 15 1,3-Dichlorobenzene ND 50.0 58.74 ug/L 117 77 -131 6 15 1,4-Dichlorobenzene ND 50.0 56.92 ug/L 114 78 -126 6 15 Dichlorodifluoromethane ND 50.0 59.12 ug/L 118 40 -127 17 18 1,1-Dichloroethane ND 50.0 51.37 ug/L 103 71 -139 5 17 1,2-Dichloroethane ND 50.0 56.23 F2 ug/L 112 64 -136 25 17 1,1-Dichloroethene ND 50.0 56.83 ug/L 114 70 -142 9 17 1,2-Dichloroethene, Total ND 100 109.3 ug/L 109 60 -152 12 33 1,2-Dichloropropane ND 50.0 57.70 ug/L 115 67 -131 15 17 1,3-Dichloropropane ND 50.0 52.31 ug/L 105 72 -134 6 14 2,2-Dichloropropane ND 50.0 53.93 ug/L 108 37 -175 9 18 1,1-Dichloropropene ND 50.0 63.20 F2 ug/L 126 76 -139 25 17 Diisopropyl ether ND 50.0 50.71 ug/L 101 10 -200 12 50 Ethylbenzene ND 50.0 60.34 ug/L 121 79 -139 6 15 Hexachlorobutadiene ND 50.0 59.72 ug/L 119 45 -155 5 23 2-Hexanone ND 250 226.5 ug/L 91 50 -150 7 15 Isopropylbenzene ND 50.0 57.44 ug/L 115 80 -153 6 16 Methylene Chloride ND 50.0 55.12 ug/L 110 64 -139 17 17 4-Methyl-2-pentanone (MIBK)ND 250 235.1 ug/L 94 50 -147 8 17 Methyl tert-butyl ether ND 50.0 54.53 F2 ug/L 109 66 -141 18 16 Naphthalene ND 50.0 54.61 ug/L 109 55 -140 12 26 n-Butylbenzene ND 50.0 58.99 ug/L 118 66 -141 6 18 N-Propylbenzene ND 50.0 66.06 ug/L 132 69 -142 6 17 p-Isopropyltoluene ND 50.0 60.79 ug/L 122 71 -137 6 16 sec-Butylbenzene ND 50.0 62.48 ug/L 125 73 -138 6 16 Styrene ND 50.0 59.83 ug/L 120 61 -148 5 24 tert-Butylbenzene ND 50.0 66.73 ug/L 133 70 -138 6 16 1,1,1,2-Tetrachloroethane ND 50.0 56.95 ug/L 114 73 -141 6 16 1,1,2,2-Tetrachloroethane ND 50.0 49.69 ug/L 99 56 -143 6 20 Tetrachloroethene ND 50.0 61.66 ug/L 123 72 -145 4 16 Toluene ND 50.0 59.56 ug/L 119 75 -136 7 15 trans-1,2-Dichloroethene ND 50.0 55.61 ug/L 111 66 -143 16 16 trans-1,3-Dichloropropene ND 50.0 54.89 ug/L 110 59 -135 8 14 1,2,3-Trichlorobenzene ND 50.0 62.79 ug/L 126 55 -138 11 25 TestAmerica Nashville Page 21 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: WSW-1Lab Sample ID: 490-70180-3 MSD Matrix: Water Prep Type: Total/NA Analysis Batch: 219934 1,2,4-Trichlorobenzene ND 50.0 55.08 ug/L 110 60 -136 10 19 Analyte MSD MSD DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD 1,1,1-Trichloroethane ND 50.0 62.75 F2 ug/L 126 76 -149 25 17 1,1,2-Trichloroethane ND 50.0 52.83 ug/L 106 74 -134 6 15 Trichloroethene ND 50.0 64.99 ug/L 130 73 -144 15 17 Trichlorofluoromethane ND 50.0 63.03 ug/L 126 58 -139 14 18 1,2,3-Trichloropropane ND 50.0 52.70 ug/L 105 53 -144 5 19 1,2,4-Trimethylbenzene ND 50.0 59.08 ug/L 118 69 -136 4 16 1,3,5-Trimethylbenzene ND 50.0 59.14 ug/L 118 69 -139 5 17 Vinyl chloride ND 50.0 57.98 ug/L 116 56 -129 16 17 Xylenes, Total ND 100 119.0 ug/L 119 74 -141 5 15 4-Bromofluorobenzene (Surr)70 -130 Surrogate 87 MSD MSD Qualifier Limits%Recovery 117Dibromofluoromethane (Surr)70 -130 1061,2-Dichloroethane-d4 (Surr)70 -130 104Toluene-d8 (Surr)70 -130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 490-219903/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 221742 Prep Batch: 219903 RL MDL Acenaphthene ND 2.00 ug/L 01/13/15 07:26 01/20/15 23:07 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 2.00 ug/L 01/13/15 07:26 01/20/15 23:07 1Acenaphthylene ND 2.00 ug/L 01/13/15 07:26 01/20/15 23:07 1Anthracene ND 2.00 ug/L 01/13/15 07:26 01/20/15 23:07 1Benzo[a]anthracene ND 2.00 ug/L 01/13/15 07:26 01/20/15 23:07 1Benzo[a]pyrene ND 2.00 ug/L 01/13/15 07:26 01/20/15 23:07 1Benzo[b]fluoranthene ND 2.00 ug/L 01/13/15 07:26 01/20/15 23:07 1Benzo[g,h,i]perylene ND 2.00 ug/L 01/13/15 07:26 01/20/15 23:07 1Benzo[k]fluoranthene ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Bis(2-chloroethoxy)methane ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Bis(2-chloroethyl)ether ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1bis (2-chloroisopropyl) ether ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Bis(2-ethylhexyl) phthalate ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 14-Bromophenyl phenyl ether ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Butyl benzyl phthalate ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Carbazole ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 14-Chloroaniline ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 14-Chloro-3-methylphenol ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 12-Chloronaphthalene ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 12-Chlorophenol ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 14-Chlorophenyl phenyl ether ND 2.00 ug/L 01/13/15 07:26 01/20/15 23:07 1Chrysene ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Cresols ND 2.00 ug/L 01/13/15 07:26 01/20/15 23:07 1Dibenz(a,h)anthracene ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Dibenzofuran TestAmerica Nashville Page 22 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-219903/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 221742 Prep Batch: 219903 RL MDL 1,2-Dichlorobenzene ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 11,3-Dichlorobenzene ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 11,4-Dichlorobenzene ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 13,3'-Dichlorobenzidine ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 12,4-Dichlorophenol ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Diethyl phthalate ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 12,4-Dimethylphenol ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Dimethyl phthalate ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Di-n-butyl phthalate ND 25.0 ug/L 01/13/15 07:26 01/20/15 23:07 14,6-Dinitro-2-methylphenol ND 25.0 ug/L 01/13/15 07:26 01/20/15 23:07 12,4-Dinitrophenol ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 12,4-Dinitrotoluene ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 12,6-Dinitrotoluene ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Di-n-octyl phthalate ND 2.00 ug/L 01/13/15 07:26 01/20/15 23:07 1Fluoranthene ND 2.00 ug/L 01/13/15 07:26 01/20/15 23:07 1Fluorene ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Hexachlorobenzene ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Hexachlorobutadiene ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Hexachlorocyclopentadiene ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Hexachloroethane ND 2.00 ug/L 01/13/15 07:26 01/20/15 23:07 1Indeno[1,2,3-cd]pyrene ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Isophorone ND 2.00 ug/L 01/13/15 07:26 01/20/15 23:07 11-Methylnaphthalene ND 2.00 ug/L 01/13/15 07:26 01/20/15 23:07 12-Methylnaphthalene ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 12-Methylphenol ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 13 & 4 Methylphenol ND 2.00 ug/L 01/13/15 07:26 01/20/15 23:07 1Naphthalene ND 25.0 ug/L 01/13/15 07:26 01/20/15 23:07 12-Nitroaniline ND 25.0 ug/L 01/13/15 07:26 01/20/15 23:07 13-Nitroaniline ND 25.0 ug/L 01/13/15 07:26 01/20/15 23:07 14-Nitroaniline ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Nitrobenzene ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 12-Nitrophenol ND 25.0 ug/L 01/13/15 07:26 01/20/15 23:07 14-Nitrophenol ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1N-Nitrosodi-n-propylamine ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1n-Nitrosodiphenylamine(as diphenylamine) ND 25.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Pentachlorophenol ND 2.00 ug/L 01/13/15 07:26 01/20/15 23:07 1Phenanthrene ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 1Phenol ND 2.00 ug/L 01/13/15 07:26 01/20/15 23:07 1Pyrene ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 11,2,4-Trichlorobenzene ND 25.0 ug/L 01/13/15 07:26 01/20/15 23:07 12,4,5-Trichlorophenol ND 10.0 ug/L 01/13/15 07:26 01/20/15 23:07 12,4,6-Trichlorophenol 2-Fluorobiphenyl (Surr)66 29-120 01/20/15 23:07 1 MB MB Surrogate 01/13/15 07:26 Dil FacPrepared AnalyzedQualifier Limits%Recovery 37 01/13/15 07:26 01/20/15 23:07 12-Fluorophenol (Surr)10-120 65 01/13/15 07:26 01/20/15 23:07 1Nitrobenzene-d5 (Surr)27-120 TestAmerica Nashville Page 23 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-219903/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 221742 Prep Batch: 219903 Phenol-d5 (Surr)24 10-120 01/20/15 23:07 1 MB MB Surrogate 01/13/15 07:26 Dil FacPrepared AnalyzedQualifier Limits%Recovery 71 01/13/15 07:26 01/20/15 23:07 1Terphenyl-d14 (Surr)13-120 65 01/13/15 07:26 01/20/15 23:07 12,4,6-Tribromophenol (Surr)10-120 Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-219903/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 221742 Prep Batch: 219903 Acenaphthene 50.0 35.43 ug/L 71 46 -120 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Acenaphthylene 50.0 35.53 ug/L 71 48 -120 Anthracene 50.0 35.22 ug/L 70 58 -130 Benzo[a]anthracene 50.0 35.78 ug/L 72 57 -120 Benzo[a]pyrene 50.0 36.18 ug/L 72 57 -124 Benzo[b]fluoranthene 50.0 36.40 ug/L 73 51 -125 Benzo[g,h,i]perylene 50.0 39.61 ug/L 79 51 -123 Benzo[k]fluoranthene 50.0 37.41 ug/L 75 51 -120 Bis(2-chloroethoxy)methane 50.0 33.66 ug/L 67 44 -120 Bis(2-chloroethyl)ether 50.0 32.00 ug/L 64 47 -120 bis (2-chloroisopropyl) ether 50.0 30.78 ug/L 62 44 -120 Bis(2-ethylhexyl) phthalate 50.0 38.78 ug/L 78 47 -138 4-Bromophenyl phenyl ether 50.0 35.26 ug/L 71 47 -127 Butyl benzyl phthalate 50.0 37.78 ug/L 76 51 -146 Carbazole 50.0 34.98 ug/L 70 54 -123 4-Chloroaniline 50.0 34.21 ug/L 68 44 -120 4-Chloro-3-methylphenol 50.0 32.95 ug/L 66 44 -120 2-Chloronaphthalene 50.0 33.53 ug/L 67 39 -120 2-Chlorophenol 50.0 31.89 ug/L 64 40 -120 4-Chlorophenyl phenyl ether 50.0 35.59 ug/L 71 50 -120 Chrysene 50.0 36.11 ug/L 72 55 -120 Cresols 100 53.11 ug/L 53 33 -120 Dibenz(a,h)anthracene 50.0 38.66 ug/L 77 50 -125 Dibenzofuran 50.0 34.82 ug/L 70 50 -120 1,2-Dichlorobenzene 50.0 28.94 ug/L 58 32 -120 1,3-Dichlorobenzene 50.0 28.10 ug/L 56 32 -120 1,4-Dichlorobenzene 50.0 29.00 ug/L 58 31 -120 3,3'-Dichlorobenzidine 50.0 37.43 ug/L 75 46 -129 2,4-Dichlorophenol 50.0 33.82 ug/L 68 38 -120 Diethyl phthalate 50.0 35.79 ug/L 72 54 -128 2,4-Dimethylphenol 50.0 20.94 ug/L 42 21 -126 Dimethyl phthalate 50.0 35.83 ug/L 72 53 -127 Di-n-butyl phthalate 50.0 36.27 ug/L 73 54 -140 4,6-Dinitro-2-methylphenol 100 73.29 ug/L 73 19 -150 2,4-Dinitrophenol 100 72.88 ug/L 73 20 -150 2,4-Dinitrotoluene 50.0 36.82 ug/L 74 46 -132 2,6-Dinitrotoluene 50.0 38.26 ug/L 77 54 -128 Di-n-octyl phthalate 50.0 38.93 ug/L 78 50 -142 Fluoranthene 50.0 36.09 ug/L 72 56 -120 TestAmerica Nashville Page 24 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-219903/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 221742 Prep Batch: 219903 Fluorene 50.0 36.99 ug/L 74 52 -120 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Hexachlorobenzene 50.0 34.53 ug/L 69 48 -131 Hexachlorobutadiene 50.0 29.28 ug/L 59 28 -120 Hexachlorocyclopentadiene 50.0 27.26 ug/L 55 17 -120 Hexachloroethane 50.0 29.19 ug/L 58 30 -120 Indeno[1,2,3-cd]pyrene 50.0 38.32 ug/L 77 54 -125 Isophorone 50.0 33.83 ug/L 68 47 -120 1-Methylnaphthalene 50.0 32.52 ug/L 65 36 -120 2-Methylnaphthalene 50.0 32.79 ug/L 66 31 -120 2-Methylphenol 50.0 28.14 ug/L 56 38 -120 3 & 4 Methylphenol 50.0 24.97 ug/L 50 33 -120 Naphthalene 50.0 31.80 ug/L 64 37 -120 2-Nitroaniline 50.0 36.49 ug/L 73 46 -131 3-Nitroaniline 50.0 35.89 ug/L 72 54 -121 4-Nitroaniline 50.0 37.14 ug/L 74 55 -123 Nitrobenzene 50.0 32.36 ug/L 65 36 -120 2-Nitrophenol 50.0 34.81 ug/L 70 32 -120 4-Nitrophenol 100 27.82 ug/L 28 10 -120 N-Nitrosodi-n-propylamine 50.0 34.18 ug/L 68 51 -120 n-Nitrosodiphenylamine(as diphenylamine) 42.8 34.85 ug/L 82 58 -149 Pentachlorophenol 100 69.82 ug/L 70 21 -150 Phenanthrene 50.0 35.35 ug/L 71 56 -120 Phenol 50.0 11.61 ug/L 23 14 -120 Pyrene 50.0 36.11 ug/L 72 53 -129 1,2,4-Trichlorobenzene 50.0 31.77 ug/L 64 30 -120 2,4,5-Trichlorophenol 50.0 35.74 ug/L 71 40 -129 2,4,6-Trichlorophenol 50.0 36.08 ug/L 72 39 -135 2-Fluorobiphenyl (Surr)29 -120 Surrogate 65 LCS LCS Qualifier Limits%Recovery 302-Fluorophenol (Surr)10 -120 63Nitrobenzene-d5 (Surr)27 -120 21Phenol-d5 (Surr)10 -120 67Terphenyl-d14 (Surr)13 -120 702,4,6-Tribromophenol (Surr)10 -120 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-219903/4-A Matrix: Water Prep Type: Total/NA Analysis Batch: 221742 Prep Batch: 219903 Acenaphthene 50.0 38.31 ug/L 77 46 -120 8 31 Analyte LCSD LCSD DUnitResult Qualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Acenaphthylene 50.0 38.41 ug/L 77 48 -120 8 31 Anthracene 50.0 38.06 ug/L 76 58 -130 8 28 Benzo[a]anthracene 50.0 39.00 ug/L 78 57 -120 9 27 Benzo[a]pyrene 50.0 38.32 ug/L 77 57 -124 6 27 Benzo[b]fluoranthene 50.0 38.04 ug/L 76 51 -125 4 39 TestAmerica Nashville Page 25 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-219903/4-A Matrix: Water Prep Type: Total/NA Analysis Batch: 221742 Prep Batch: 219903 Benzo[g,h,i]perylene 50.0 40.43 ug/L 81 51 -123 2 27 Analyte LCSD LCSD DUnitResult Qualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Benzo[k]fluoranthene 50.0 38.57 ug/L 77 51 -120 3 32 Bis(2-chloroethoxy)methane 50.0 37.60 ug/L 75 44 -120 11 31 Bis(2-chloroethyl)ether 50.0 33.94 ug/L 68 47 -120 6 38 bis (2-chloroisopropyl) ether 50.0 32.42 ug/L 65 44 -120 5 36 Bis(2-ethylhexyl) phthalate 50.0 40.85 ug/L 82 47 -138 5 28 4-Bromophenyl phenyl ether 50.0 38.60 ug/L 77 47 -127 9 29 Butyl benzyl phthalate 50.0 40.27 ug/L 81 51 -146 6 31 Carbazole 50.0 38.03 ug/L 76 54 -123 8 29 4-Chloroaniline 50.0 37.15 ug/L 74 44 -120 8 26 4-Chloro-3-methylphenol 50.0 37.49 ug/L 75 44 -120 13 22 2-Chloronaphthalene 50.0 36.51 ug/L 73 39 -120 8 36 2-Chlorophenol 50.0 34.24 ug/L 68 40 -120 7 46 4-Chlorophenyl phenyl ether 50.0 38.70 ug/L 77 50 -120 8 29 Chrysene 50.0 38.16 ug/L 76 55 -120 6 27 Cresols 100 56.66 ug/L 57 33 -120 6 34 Dibenz(a,h)anthracene 50.0 40.84 ug/L 82 50 -125 6 28 Dibenzofuran 50.0 37.42 ug/L 75 50 -120 7 29 1,2-Dichlorobenzene 50.0 31.17 ug/L 62 32 -120 7 42 1,3-Dichlorobenzene 50.0 31.27 ug/L 63 32 -120 11 42 1,4-Dichlorobenzene 50.0 32.07 ug/L 64 31 -120 10 44 3,3'-Dichlorobenzidine 50.0 38.87 ug/L 78 46 -129 4 30 2,4-Dichlorophenol 50.0 37.59 ug/L 75 38 -120 11 30 Diethyl phthalate 50.0 38.37 ug/L 77 54 -128 7 28 2,4-Dimethylphenol 50.0 22.63 ug/L 45 21 -126 8 48 Dimethyl phthalate 50.0 38.64 ug/L 77 53 -127 8 27 Di-n-butyl phthalate 50.0 39.45 ug/L 79 54 -140 8 27 4,6-Dinitro-2-methylphenol 100 79.03 ug/L 79 19 -150 8 34 2,4-Dinitrophenol 100 77.60 ug/L 78 20 -150 6 31 2,4-Dinitrotoluene 50.0 40.09 ug/L 80 46 -132 8 26 2,6-Dinitrotoluene 50.0 41.77 ug/L 84 54 -128 9 29 Di-n-octyl phthalate 50.0 40.57 ug/L 81 50 -142 4 28 Fluoranthene 50.0 38.42 ug/L 77 56 -120 6 28 Fluorene 50.0 39.29 ug/L 79 52 -120 6 28 Hexachlorobenzene 50.0 38.51 ug/L 77 48 -131 11 28 Hexachlorobutadiene 50.0 34.45 ug/L 69 28 -120 16 43 Hexachlorocyclopentadiene 50.0 29.10 ug/L 58 17 -120 7 43 Hexachloroethane 50.0 31.85 ug/L 64 30 -120 9 45 Indeno[1,2,3-cd]pyrene 50.0 39.87 ug/L 80 54 -125 4 27 Isophorone 50.0 37.41 ug/L 75 47 -120 10 31 1-Methylnaphthalene 50.0 36.75 ug/L 74 36 -120 12 36 2-Methylnaphthalene 50.0 36.34 ug/L 73 31 -120 10 35 2-Methylphenol 50.0 29.86 ug/L 60 38 -120 6 32 3 & 4 Methylphenol 50.0 26.80 ug/L 54 33 -120 7 34 Naphthalene 50.0 36.12 ug/L 72 37 -120 13 37 2-Nitroaniline 50.0 39.48 ug/L 79 46 -131 8 24 3-Nitroaniline 50.0 38.69 ug/L 77 54 -121 7 26 4-Nitroaniline 50.0 39.11 ug/L 78 55 -123 5 26 TestAmerica Nashville Page 26 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-219903/4-A Matrix: Water Prep Type: Total/NA Analysis Batch: 221742 Prep Batch: 219903 Nitrobenzene 50.0 36.52 ug/L 73 36 -120 12 28 Analyte LCSD LCSD DUnitResult Qualifier %Rec Spike Added %Rec. Limits LimitRPD RPD 2-Nitrophenol 50.0 38.75 ug/L 78 32 -120 11 31 4-Nitrophenol 100 32.99 ug/L 33 10 -120 17 38 N-Nitrosodi-n-propylamine 50.0 35.44 ug/L 71 51 -120 4 37 n-Nitrosodiphenylamine(as diphenylamine) 42.8 38.21 ug/L 89 58 -149 9 26 Pentachlorophenol 100 75.77 ug/L 76 21 -150 8 31 Phenanthrene 50.0 38.06 ug/L 76 56 -120 7 26 Phenol 50.0 12.97 ug/L 26 14 -120 11 42 Pyrene 50.0 39.65 ug/L 79 53 -129 9 29 1,2,4-Trichlorobenzene 50.0 35.71 ug/L 71 30 -120 12 35 2,4,5-Trichlorophenol 50.0 39.47 ug/L 79 40 -129 10 34 2,4,6-Trichlorophenol 50.0 38.65 ug/L 77 39 -135 7 40 2-Fluorobiphenyl (Surr)29 -120 Surrogate 67 LCSD LCSD Qualifier Limits%Recovery 322-Fluorophenol (Surr)10 -120 69Nitrobenzene-d5 (Surr)27 -120 23Phenol-d5 (Surr)10 -120 70Terphenyl-d14 (Surr)13 -120 752,4,6-Tribromophenol (Surr)10 -120 Client Sample ID: Method BlankLab Sample ID: MB 490-219917/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 220233 Prep Batch: 219917 RL MDL Acenaphthene ND 2.00 ug/L 01/13/15 08:23 01/14/15 13:35 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 2.00 ug/L 01/13/15 08:23 01/14/15 13:35 1Acenaphthylene ND 2.00 ug/L 01/13/15 08:23 01/14/15 13:35 1Anthracene ND 2.00 ug/L 01/13/15 08:23 01/14/15 13:35 1Benzo[a]anthracene ND 2.00 ug/L 01/13/15 08:23 01/14/15 13:35 1Benzo[a]pyrene ND 2.00 ug/L 01/13/15 08:23 01/14/15 13:35 1Benzo[b]fluoranthene ND 2.00 ug/L 01/13/15 08:23 01/14/15 13:35 1Benzo[g,h,i]perylene ND 2.00 ug/L 01/13/15 08:23 01/14/15 13:35 1Benzo[k]fluoranthene ND 2.00 ug/L 01/13/15 08:23 01/14/15 13:35 1Chrysene ND 2.00 ug/L 01/13/15 08:23 01/14/15 13:35 1Dibenz(a,h)anthracene ND 2.00 ug/L 01/13/15 08:23 01/14/15 13:35 1Fluoranthene ND 2.00 ug/L 01/13/15 08:23 01/14/15 13:35 1Fluorene ND 2.00 ug/L 01/13/15 08:23 01/14/15 13:35 1Indeno[1,2,3-cd]pyrene ND 2.00 ug/L 01/13/15 08:23 01/14/15 13:35 1Naphthalene ND 2.00 ug/L 01/13/15 08:23 01/14/15 13:35 1Phenanthrene ND 2.00 ug/L 01/13/15 08:23 01/14/15 13:35 1Pyrene 2-Fluorobiphenyl (Surr)91 29-120 01/14/15 13:35 1 MB MB Surrogate 01/13/15 08:23 Dil FacPrepared AnalyzedQualifier Limits%Recovery 85 01/13/15 08:23 01/14/15 13:35 1Nitrobenzene-d5 (Surr)27-120 95 01/13/15 08:23 01/14/15 13:35 1Terphenyl-d14 (Surr)13-120 TestAmerica Nashville Page 27 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-219917/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 220233 Prep Batch: 219917 Acenaphthene 40.0 39.20 ug/L 98 46 -120 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Acenaphthylene 40.0 39.22 ug/L 98 48 -120 Anthracene 40.0 40.30 ug/L 101 58 -130 Benzo[a]anthracene 40.0 41.42 ug/L 104 57 -120 Benzo[a]pyrene 40.0 41.00 ug/L 102 57 -124 Benzo[b]fluoranthene 40.0 47.63 ug/L 119 51 -125 Benzo[g,h,i]perylene 40.0 40.92 ug/L 102 51 -123 Benzo[k]fluoranthene 40.0 37.52 ug/L 94 51 -120 Chrysene 40.0 38.18 ug/L 95 55 -120 Dibenz(a,h)anthracene 40.0 41.96 ug/L 105 50 -125 Fluoranthene 40.0 40.31 ug/L 101 56 -120 Fluorene 40.0 42.53 ug/L 106 52 -120 Indeno[1,2,3-cd]pyrene 40.0 40.70 ug/L 102 54 -125 Naphthalene 40.0 35.23 ug/L 88 37 -120 Phenanthrene 40.0 40.96 ug/L 102 56 -120 Pyrene 40.0 43.45 ug/L 109 53 -129 2-Fluorobiphenyl (Surr)29 -120 Surrogate 81 LCS LCS Qualifier Limits%Recovery 71Nitrobenzene-d5 (Surr)27 -120 87Terphenyl-d14 (Surr)13 -120 Method: 6010C - Metals (ICP) Client Sample ID: Method BlankLab Sample ID: MB 490-219907/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 220189 Prep Batch: 219907 RL MDL Antimony ND 0.0100 mg/L 01/13/15 07:42 01/13/15 14:52 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier ND 0.0100 mg/L 01/13/15 07:42 01/13/15 14:52 1Arsenic ND 0.00400 mg/L 01/13/15 07:42 01/13/15 14:52 1Beryllium ND 0.00100 mg/L 01/13/15 07:42 01/13/15 14:52 1Cadmium ND 0.00500 mg/L 01/13/15 07:42 01/13/15 14:52 1Chromium ND 0.0100 mg/L 01/13/15 07:42 01/13/15 14:52 1Copper ND 0.00500 mg/L 01/13/15 07:42 01/13/15 14:52 1Lead ND 0.0150 mg/L 01/13/15 07:42 01/13/15 14:52 1Manganese ND 0.0100 mg/L 01/13/15 07:42 01/13/15 14:52 1Nickel ND 0.0100 mg/L 01/13/15 07:42 01/13/15 14:52 1Selenium ND 0.00500 mg/L 01/13/15 07:42 01/13/15 14:52 1Silver ND 0.0100 mg/L 01/13/15 07:42 01/13/15 14:52 1Thallium ND 0.0500 mg/L 01/13/15 07:42 01/13/15 14:52 1Zinc TestAmerica Nashville Page 28 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Method: 6010C - Metals (ICP) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-219907/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 220189 Prep Batch: 219907 Antimony 0.100 0.1060 mg/L 106 80 -120 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Arsenic 0.0500 0.05120 mg/L 102 80 -120 Beryllium 0.0500 0.05350 mg/L 107 80 -120 Cadmium 0.0500 0.05170 mg/L 103 80 -120 Chromium 0.200 0.2058 mg/L 103 80 -120 Copper 0.250 0.2578 mg/L 103 80 -120 Lead 0.0500 0.05120 mg/L 102 80 -120 Manganese 0.500 0.5249 mg/L 105 80 -120 Nickel 0.500 0.5364 mg/L 107 80 -120 Selenium 0.0500 0.05160 mg/L 103 80 -120 Silver 0.0500 0.05090 mg/L 102 80 -120 Zinc 0.500 0.5111 mg/L 102 80 -120 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-219907/3-A Matrix: Water Prep Type: Total/NA Analysis Batch: 220189 Prep Batch: 219907 Antimony 0.100 0.1051 mg/L 105 80 -120 1 20 Analyte LCSD LCSD DUnitResult Qualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Arsenic 0.0500 0.04780 mg/L 96 80 -120 7 20 Beryllium 0.0500 0.05210 mg/L 104 80 -120 3 20 Cadmium 0.0500 0.05070 mg/L 101 80 -120 2 20 Chromium 0.200 0.2026 mg/L 101 80 -120 2 20 Copper 0.250 0.2504 mg/L 100 80 -120 3 20 Lead 0.0500 0.05070 mg/L 101 80 -120 1 20 Manganese 0.500 0.5144 mg/L 103 80 -120 2 20 Nickel 0.500 0.5269 mg/L 105 80 -120 2 20 Selenium 0.0500 0.05000 mg/L 100 80 -120 3 20 Silver 0.0500 0.04980 mg/L 100 80 -120 2 20 Zinc 0.500 0.5006 mg/L 100 80 -120 2 20 Client Sample ID: Matrix SpikeLab Sample ID: 490-70176-D-8-B MS Matrix: Water Prep Type: Total/NA Analysis Batch: 220189 Prep Batch: 219907 Antimony ND 0.100 0.1061 mg/L 106 75 -125 Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Arsenic ND 0.0500 0.04870 mg/L 97 75 -125 Beryllium ND 0.0500 0.05250 mg/L 105 75 -125 Cadmium ND 0.0500 0.05080 mg/L 102 75 -125 Chromium ND 0.200 0.2031 mg/L 102 75 -125 Copper ND 0.250 0.2513 mg/L 101 75 -125 Lead ND 0.0500 0.05060 mg/L 101 75 -125 Manganese ND 0.500 0.5152 mg/L 103 75 -125 Nickel ND 0.500 0.5272 mg/L 105 75 -125 Selenium ND 0.0500 0.05010 mg/L 100 75 -125 Silver ND 0.0500 0.05040 mg/L 101 75 -125 Thallium ND *0.0500 0.03620 F1 mg/L 72 75 -125 TestAmerica Nashville Page 29 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Method: 6010C - Metals (ICP) (Continued) Client Sample ID: Matrix SpikeLab Sample ID: 490-70176-D-8-B MS Matrix: Water Prep Type: Total/NA Analysis Batch: 220189 Prep Batch: 219907 Zinc ND 0.500 0.5026 mg/L 101 75 -125 Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-70176-D-8-C MSD Matrix: Water Prep Type: Total/NA Analysis Batch: 220189 Prep Batch: 219907 Antimony ND 0.100 0.1048 mg/L 105 75 -125 1 20 Analyte MSD MSD DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Arsenic ND 0.0500 0.04980 mg/L 100 75 -125 2 20 Beryllium ND 0.0500 0.05240 mg/L 105 75 -125 0 20 Cadmium ND 0.0500 0.05070 mg/L 101 75 -125 0 20 Chromium ND 0.200 0.2017 mg/L 101 75 -125 1 20 Copper ND 0.250 0.2494 mg/L 100 75 -125 1 20 Lead ND 0.0500 0.05000 mg/L 100 75 -125 1 20 Manganese ND 0.500 0.5132 mg/L 103 75 -125 0 20 Nickel ND 0.500 0.5247 mg/L 105 75 -125 0 20 Selenium ND 0.0500 0.05100 mg/L 102 75 -125 2 20 Silver ND 0.0500 0.04970 mg/L 99 75 -125 1 20 Thallium ND *0.0500 0.03630 F1 mg/L 73 75 -125 0 20 Zinc ND 0.500 0.5016 mg/L 100 75 -125 0 20 Client Sample ID: Method BlankLab Sample ID: MB 490-220731/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 221412 Prep Batch: 220731 RL MDL Thallium ND 0.0100 mg/L 01/16/15 08:12 01/19/15 13:25 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-220731/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 221412 Prep Batch: 220731 Thallium 0.0500 0.05420 mg/L 108 80 -120 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-220731/3-A Matrix: Water Prep Type: Total/NA Analysis Batch: 221412 Prep Batch: 220731 Thallium 0.0500 0.05410 mg/L 108 80 -120 0 20 Analyte LCSD LCSD DUnitResult Qualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Client Sample ID: Matrix SpikeLab Sample ID: 490-70383-D-1-B MS Matrix: Water Prep Type: Total/NA Analysis Batch: 221412 Prep Batch: 220731 Thallium ND 0.0500 0.05170 mg/L 103 75 -125 Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits TestAmerica Nashville Page 30 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Method: 6010C - Metals (ICP) (Continued) Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-70383-D-1-C MSD Matrix: Water Prep Type: Total/NA Analysis Batch: 221412 Prep Batch: 220731 Thallium ND 0.0500 0.05260 mg/L 105 75 -125 2 20 Analyte MSD MSD DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Method: 7470A - Mercury (CVAA) Client Sample ID: Method BlankLab Sample ID: MB 490-220225/1-A Matrix: Water Prep Type: Total/NA Analysis Batch: 220737 Prep Batch: 220225 RL MDL Mercury ND 0.00200 mg/L 01/14/15 10:48 01/15/15 18:26 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-220225/2-A Matrix: Water Prep Type: Total/NA Analysis Batch: 220737 Prep Batch: 220225 Mercury 0.0100 0.009790 mg/L 98 80 -120 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-220225/3-A Matrix: Water Prep Type: Total/NA Analysis Batch: 220737 Prep Batch: 220225 Mercury 0.0100 0.009981 mg/L 100 80 -120 2 20 Analyte LCSD LCSD DUnitResult Qualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Client Sample ID: Matrix SpikeLab Sample ID: 490-70198-D-1-D MS Matrix: Water Prep Type: Total/NA Analysis Batch: 220737 Prep Batch: 220225 Mercury ND 0.0100 0.009315 mg/L 93 75 -125 Analyte MS MS DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-70198-D-1-E MSD Matrix: Water Prep Type: Total/NA Analysis Batch: 220737 Prep Batch: 220225 Mercury ND 0.0100 0.009572 mg/L 96 75 -125 3 20 Analyte MSD MSD DUnitResult Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD TestAmerica Nashville Page 31 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility GC/MS VOA Analysis Batch: 219934 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 8260B490-70180-1 TMW-4 Total/NA Water 8260B490-70180-2 TMW-3 Total/NA Water 8260B490-70180-3 WSW-1 Total/NA Water 8260B490-70180-3 MS WSW-1 Total/NA Water 8260B490-70180-3 MSD WSW-1 Total/NA Water 8260BLCS 490-219934/3 Lab Control Sample Total/NA Water 8260BMB 490-219934/7 Method Blank Total/NA GC/MS Semi VOA Prep Batch: 219903 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 3510C490-70180-3 WSW-1 Total/NA Water 3510CLCS 490-219903/2-A Lab Control Sample Total/NA Water 3510CLCSD 490-219903/4-A Lab Control Sample Dup Total/NA Water 3510CMB 490-219903/1-A Method Blank Total/NA Prep Batch: 219917 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 3510C490-70180-1 TMW-4 Total/NA Water 3510C490-70180-2 TMW-3 Total/NA Water 3510CLCS 490-219917/2-A Lab Control Sample Total/NA Water 3510CMB 490-219917/1-A Method Blank Total/NA Analysis Batch: 220233 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 8270D 219917490-70180-1 TMW-4 Total/NA Water 8270D 219917490-70180-2 TMW-3 Total/NA Water 8270D 219917LCS 490-219917/2-A Lab Control Sample Total/NA Water 8270D 219917MB 490-219917/1-A Method Blank Total/NA Analysis Batch: 221742 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 8270D 219903490-70180-3 WSW-1 Total/NA Water 8270D 219903LCS 490-219903/2-A Lab Control Sample Total/NA Water 8270D 219903LCSD 490-219903/4-A Lab Control Sample Dup Total/NA Water 8270D 219903MB 490-219903/1-A Method Blank Total/NA Metals Prep Batch: 219907 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 3010A490-70176-D-8-B MS Matrix Spike Total/NA Water 3010A490-70176-D-8-C MSD Matrix Spike Duplicate Total/NA Water 3010A490-70180-1 TMW-4 Total/NA Water 3010A490-70180-2 TMW-3 Total/NA Water 3010A490-70180-3 WSW-1 Total/NA Water 3010ALCS 490-219907/2-A Lab Control Sample Total/NA Water 3010ALCSD 490-219907/3-A Lab Control Sample Dup Total/NA Water 3010AMB 490-219907/1-A Method Blank Total/NA TestAmerica Nashville Page 32 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Metals (Continued) Analysis Batch: 220189 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 6010C 219907490-70176-D-8-B MS Matrix Spike Total/NA Water 6010C 219907490-70176-D-8-C MSD Matrix Spike Duplicate Total/NA Water 6010C 219907490-70180-1 TMW-4 Total/NA Water 6010C 219907490-70180-2 TMW-3 Total/NA Water 6010C 219907490-70180-3 WSW-1 Total/NA Water 6010C 219907LCS 490-219907/2-A Lab Control Sample Total/NA Water 6010C 219907LCSD 490-219907/3-A Lab Control Sample Dup Total/NA Water 6010C 219907MB 490-219907/1-A Method Blank Total/NA Prep Batch: 220225 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 7470A490-70180-3 WSW-1 Total/NA Water 7470A490-70198-D-1-D MS Matrix Spike Total/NA Water 7470A490-70198-D-1-E MSD Matrix Spike Duplicate Total/NA Water 7470ALCS 490-220225/2-A Lab Control Sample Total/NA Water 7470ALCSD 490-220225/3-A Lab Control Sample Dup Total/NA Water 7470AMB 490-220225/1-A Method Blank Total/NA Prep Batch: 220731 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 3010A490-70180-3 WSW-1 Total/NA Water 3010A490-70383-D-1-B MS Matrix Spike Total/NA Water 3010A490-70383-D-1-C MSD Matrix Spike Duplicate Total/NA Water 3010ALCS 490-220731/2-A Lab Control Sample Total/NA Water 3010ALCSD 490-220731/3-A Lab Control Sample Dup Total/NA Water 3010AMB 490-220731/1-A Method Blank Total/NA Analysis Batch: 220737 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 7470A 220225490-70180-3 WSW-1 Total/NA Water 7470A 220225490-70198-D-1-D MS Matrix Spike Total/NA Water 7470A 220225490-70198-D-1-E MSD Matrix Spike Duplicate Total/NA Water 7470A 220225LCS 490-220225/2-A Lab Control Sample Total/NA Water 7470A 220225LCSD 490-220225/3-A Lab Control Sample Dup Total/NA Water 7470A 220225MB 490-220225/1-A Method Blank Total/NA Analysis Batch: 221412 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 6010C 220731490-70180-3 WSW-1 Total/NA Water 6010C 220731490-70383-D-1-B MS Matrix Spike Total/NA Water 6010C 220731490-70383-D-1-C MSD Matrix Spike Duplicate Total/NA Water 6010C 220731LCS 490-220731/2-A Lab Control Sample Total/NA Water 6010C 220731LCSD 490-220731/3-A Lab Control Sample Dup Total/NA Water 6010C 220731MB 490-220731/1-A Method Blank Total/NA TestAmerica Nashville Page 33 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Lab Chronicle Client: Hart & Hickman, PC TestAmerica Job ID: 490-70180-1 Project/Site: ADDCO Facility SDG: FCB.014 Client Sample ID: TMW-4 Lab Sample ID: 490-70180-1 Matrix: WaterDate Collected: 01/09/15 11:40 Date Received: 01/10/15 08:45 Analysis 8260B JMG01/13/15 20:081 TAL NSH219934 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 10 mL 10 mL Prep 3510C 219917 01/13/15 08:23 CLM TAL NSHTotal/NA 310 mL 1.0 mL Analysis 8270D 1 220233 01/14/15 14:44 BES TAL NSHTotal/NA 310 mL 1.0 mL Prep 3010A 219907 01/13/15 07:42 AJD TAL NSHTotal/NA 50 mL 50 mL Analysis 6010C 1 220189 01/13/15 15:43 ADN TAL NSHTotal/NA 50 mL 50 mL Client Sample ID: TMW-3 Lab Sample ID: 490-70180-2 Matrix: WaterDate Collected: 01/09/15 12:45 Date Received: 01/10/15 08:45 Analysis 8260B JMG01/13/15 20:361 TAL NSH219934 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 10 mL 10 mL Prep 3510C 219917 01/13/15 08:23 CLM TAL NSHTotal/NA 310 mL 1.0 mL Analysis 8270D 1 220233 01/14/15 15:06 BES TAL NSHTotal/NA 310 mL 1.0 mL Prep 3010A 219907 01/13/15 07:42 AJD TAL NSHTotal/NA 50 mL 50 mL Analysis 6010C 1 220189 01/13/15 15:47 ADN TAL NSHTotal/NA 50 mL 50 mL Client Sample ID: WSW-1 Lab Sample ID: 490-70180-3 Matrix: WaterDate Collected: 01/09/15 13:25 Date Received: 01/10/15 08:45 Analysis 8260B JMG01/13/15 14:261 TAL NSH219934 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 10 mL 10 mL Prep 3510C 219903 01/13/15 07:26 CLM TAL NSHTotal/NA 980 mL 1.0 mL Analysis 8270D 1 221742 01/21/15 01:45 SNR TAL NSHTotal/NA 980 mL 1.0 mL Prep 3010A 220731 01/16/15 08:12 AJD TAL NSHTotal/NA 50 mL 50 mL Analysis 6010C 1 221412 01/19/15 15:39 CME TAL NSHTotal/NA 50 mL 50 mL Prep 3010A 219907 01/13/15 07:42 AJD TAL NSHTotal/NA 50 mL 50 mL Analysis 6010C 1 220189 01/13/15 15:52 ADN TAL NSHTotal/NA 50 mL 50 mL Prep 7470A 220225 01/14/15 10:48 TDP TAL NSHTotal/NA 3 mL 30 mL Analysis 7470A 1 220737 01/15/15 18:55 CME TAL NSHTotal/NA 3 mL 30 mL Laboratory References: TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177 TestAmerica Nashville Page 34 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Method Summary TestAmerica Job ID: 490-70180-1Client: Hart & Hickman, PC SDG: FCB.014Project/Site: ADDCO Facility Method Method Description LaboratoryProtocol SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH SW8468270DSemivolatile Organic Compounds (GC/MS)TAL NSH SW8466010CMetals (ICP)TAL NSH SW8467470AMercury (CVAA)TAL NSH Protocol References: SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177 TestAmerica Nashville Page 35 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Certification Summary Client: Hart & Hickman, PC TestAmerica Job ID: 490-70180-1 Project/Site: ADDCO Facility SDG: FCB.014 Laboratory: TestAmerica Nashville The certifications listed below are applicable to this report. Authority Program EPA Region Certification ID Expiration Date North Carolina (WW/SW)3874State Program 12-31-15 TestAmerica Nashville Page 36 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Page 37 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13 Page 38 of 39 1/21/2015 1234567 8 9 10 11 12 13 Login Sample Receipt Checklist Client: Hart & Hickman, PC Job Number: 490-70180-1 SDG Number: FCB.014 Login Number: 70180 Question Answer Comment Creator: Gambill, Shane List Source: TestAmerica Nashville List Number: 1 TrueRadioactivity wasn't checked or is </= background as measured by a survey meter. TrueThe cooler's custody seal, if present, is intact. TrueSample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded.2.7 TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time. TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. N/ASample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. TrueResidual Chlorine Checked. TestAmerica Nashville Page 39 of 39 1/21/2015 1 2 3 4 5 6 7 8 9 10 11 12 13