Phase II ESA; Carolina Freightliner 5-4-16

PHASE II ENVIRONMENTAL SITE ASSESSMENT
CAROLINA FREIGHTLINER
3500 YONKERS ROAD
RALEIGH, WAKE COUNTY
NORTH CAROLINA

Prepared for:
Mr. Carl Howard
Carolina Truckworks LLC 3500 Yonkers Road
Raleigh, North Carolina 27604

Prepared by:
Resolve Environmental Services, PLLC
410 East Franklin Street
Monroe, North Carolina 28112

May 4, 2016

___________________
Laura Minor Project Manager

____________________
W. Scott Ball
Senior Project Manager
EXECUTIVE SUMMARY
Workscope: Phase II Environmental Assessment
Client: Carolina Truckworks LLC
c/o Mr. Carl Howard
3500 Yonkers Road
Raleigh, NC 27604
Contractor: Resolve Environmental Services, PLLC Project Information: Carolina Freightliner
3500 Yonkers Road
Raleigh, North Carolina
Wake County PIN: 1724247496
Property Acreage: 5.15 acres
Resolve Project Manager: Laura Minor

Work Scope: Resolve collected four soil samples (GP-2-6’, GP-3-6’, GP-4-1’ and GP-4-5’) and four ground water samples (GP-1 through GP-4) from temporary
monitoring wells installed at the site. The samples were collected and
submitted for laboratory analyses for volatile organic compounds by SW846
8260B. These locations were chosen to determine if the property has been
affected from on-site activities.

Findings Summary: Detectable and/or estimated concentrations of acetone, tetrachloroethylene, MEK and/or MIBK were reported in the soil samples collected at the site.
However, none of the concentrations exceeded the North Carolina
Department of Environmental Quality (NCDEQ’s) soil-to-ground water
maximum contaminant concentrations (MCC’s). An estimated
concentration of chloroform was reported in the ground water sample
collected from GP-3. However, the concentration did not exceed NCDEQ’s ground water quality standard (GWQS). Concentrations of cis-1,2-
dichloroethylene, tetrachloroethylene and trichloroethylene that exceeded the
NCGWQS were reported in GP-4. A concentration of trans-1,2-
dichloroethylene was also reported in GP-4; however, the concentration did
not exceed the NCGWQS. No detectable concentrations of requested
method constituents were reported in GP-1 or GP-2.
Conclusions: Concentrations of volatile organic compounds indicative of a solvent release
was detected in ground water sample, GP-4, collected at the site in an area
where runoff from the parking lot reportedly drained. The concentrations of
cis-1,2-dichloroethylene, tetrachloroethylene (also known as PERC) and
trichloroethylene exceeded the applicable NC ground water quality
standards; therefore, a ground water quality violation exists at the site.
Recommendations: The property owner is responsible for reporting these findings to the
NCDEQ. Upon review, the NCDEQ may or may not require additional
assessment at the site.
TABLE OF CONTENTS
1.0 Site History .............................................................................................................................................. 1
2.0 Phase II Subsurface Activities ................................................................................................................ 1
3.0 Soil Analytical Results ............................................................................................................................ 1
4.0 Ground Water Analytical Results .......................................................................................................... 2
5.0 Conclusions and Recommendations ...................................................................................................... 2
6.0 Limitations ............................................................................................................................................... 2

FIGURES
Figure 1: Site Location Map
Figure 2: Soil Sampling Map
Figure 3: Ground Water Sampling Map

TABLE

Table 1: Summary of Soil Analytical Results
Table 2: Summary of Ground Water Analytical Results

APPENDICES

Appendix A: Boring Logs
Appendix B: Laboratory Analytical Report

Phase II ESA Carolina Freightliner
Raleigh, NC
1

1.0 Site History
In April 2016, Resolve Environmental Services, PLLC (Resolve) was contracted by Mr. Carl Howard of
Carolina Trucking LLC to conduct Phase II Environmental Assessment (ESA) activities at Wake County,
North Carolina parcel ID 1724247496 (5.15 acres) located at 3500 Yonkers Road in Raleigh, North Carolina
(Figure 1). Based on the Report of Phase I Environmental Site Assessment dated February 19, 2016
completed by Environmental Hydrogeological Consultants, Inc. (EHC) and addressed to Carolina Truckworks
LLC of Raleigh, NC and Mercedes Benz Financial Service USA LLC of Farmington Hills, MI, several
recognized environmental conditions (RECs) were identified on the property. Namely, the two (2) on-site oil-
water separators (OWS), the former underground storage tank basin (UST) and the area located on the
southwest corner of the property which held runoff drainage from the parking lot. Based on this, Resolve
proposed to conduct a Phase II ESA at the site in order to address these concerns by collecting soil and ground
water samples. The Phase II ESA activities are detailed below.

2.0 Phase II Subsurface Activities
Resolve personnel supervised the installation of four temporary monitoring wells at the subject site (GP-1, GP-
2, GP-3 and GP-4). The ground water screening points were installed into the water table utilizing Geoprobe
™ direct push techniques. The screening points were installed at the site in the inferred vicinity of the former
UST(s) based on field observations (GP-1), adjacent to both on-site oil-water separators (GP-2/GP-2-6’ and
GP-3/GP-3-6’) and in the runoff area near the southwest corner of the property (GP-4/GP-4-1’/GP-4-5’). The
screening locations were chosen to determine if recognized environmental conditions specified in the Phase I
ESA had affected the property. Soil samples were collected at depths ranging from 1 to 6 feet below grade
level (BGL) using discrete sample macro-core tubing during advancement of GP-2 through GP-4.

The four ground water sampling points were completed to depths ranging from 36 and 40 feet. Ground water
samples were collected from clean, disposable polyurethane tubing inserted into the discrete sampler of each
screening point. The samples were collected by Resolve personnel using clean, disposable nitrile gloves. The
samples were placed directly into laboratory supplied glassware, placed on ice and transported to a NC
certified for analyses of VOCs by SM 846 8260B. Subsequent to sample collection, each sampling point was
properly abandoned. Boring logs for the temporary ground water sampling points are provided in Appendix
A.

3.0 Soil Analytical Results
Based upon the laboratory analytical report, detectable and/or estimated concentrations of acetone,
tetrachloroethylene, MEK and/or MIBK were reported in the soil samples collected at the site. However, none
Phase II ESA Carolina Freightliner
Raleigh, NC
2

of the concentrations exceeded the North Carolina Department of Environmental Quality (NCDEQ’s) soil-to-
ground water maximum contaminant concentrations (MCC’s). A soil sample location map is provided as
Figure 2. A summary of the soil quality analyses is presented in Table 1.

4.0 Ground Water Analytical Results
Based upon the laboratory analytical report, an estimated concentration of chloroform was reported in the ground water sample collected from GP-3. However, the concentration did not exceed NCDEQ’s ground
water quality standard (GWQS). Concentrations of cis-1,2-dichloroethylene, tetrachloroethylene and
trichloroethylene that exceeded the NCGWQS were reported in GP-4. A concentration of trans-1,2-
dichloroethylene was also reported in GP-4; however, the concentration did not exceed the NCGWQS. No
detectable concentrations of requested method constituents were reported in GP-1 or GP-2. A ground water
sample location map is provided as Figure 3. A summary of the ground water quality analyses is presented in
Table 2. A copy of the laboratory analytical report and chain of custody are attached as Appendix C.

5.0 Conclusions and Recommendations
Concentrations of volatile organic compounds indicative of a solvent release was detected in ground water
sample, GP-4, collected at the site in an area where runoff from the parking lot reportedly drained. The
concentrations of cis-1,2-dichloroethylene, tetrachloroethylene (also known as PERC) and
trichloroethylene exceeded the applicable NC ground water quality standards; therefore, a ground
water quality violation exists at the site.

The property owner is responsible for reporting these findings to the NCDEQ. Upon review, the NCDEQ may require additional assessment at the site.

6.0 Limitations
The work performed in conjunction with this study and the data developed are intended to describe information
available on the specified dates and locations. This report does not warrant against future operations or
conditions, nor does it warrant against operations or conditions present of a type or at locations not
investigated.

Resolve has based its assessment upon prior site history through interviews, available records, and conditions
and activities observable during a physical site inspection. This report is not intended to determine whether
soil contamination or waste emplacement may exist at the site. Such determinations would require
comprehensive subsurface exploration and additional sampling activities.

FIGURES
GP-2-6'GP-3-6'
GP-4-1'/GP-4-5'
DisclaimeriMaps makes every effort to produce and publish the most current and accurate information possible.However, the maps are produced for information purposes,and are NOT surveys. No warranties, expressed or implied,are provided for the data therein, its use,or its interpretation.
CAROLINA FREIGHTLINER 0 110 22055 ft
1 inch = 100 feet±
GP-1
GP-2GP-3
GP-4
DisclaimeriMaps makes every effort to produce and publish the most current and accurate information possible.However, the maps are produced for information purposes,and are NOT surveys. No warranties, expressed or implied,are provided for the data therein, its use,or its interpretation.
CAROLINA FREIGHTLINER 0 110 22055 ft
1 inch = 100 feet±

TABLES
Sample ID
Depth
Sample
Collected
(in feet)
Date Collected
(m/dd/yy)
GP-2-6'6 4/22/2016 0.0298J <0.0017 <0.012 <0.014
GP-3-6'6 4/22/2016 0.0315J 0.0050J <0.012 <0.015
GP-4-1'1 4/22/2016 0.336 <0.0025 0.0583 0.140
GP-4-5'5 4/22/2016 0.0426J <0.0015 <0.010 <0.012
24 0.0074 16 0.4
Notes:
• < : Less than the method detection limit specified in the laboratory report.
• J: Estimated value.
Soil-to-Water MCC (mg/kg)
• MCC: Maximum contaminant concentration.
TABLE 1
SUMMARY OF SOIL ANALYTICAL RESULTS
CAROLINA FREIGHTLINER
RALEIGH, WAKE COUNTY, NORTH CAROLINA
APRIL 22, 2016
Analytical Method Method SW846 8260B
Contaminant of Concern 
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(M
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Sample ID
Date
Collected
(m/dd/yy)
GP-1 4/22/2016 <0.30 <0.31 <0.33 <0.30 <0.27
GP-2 4/22/2016 <0.30 <0.31 <0.33 <0.30 <0.27
GP-3 4/22/2016 0.57J <0.31 <0.33 <0.30 <0.27
GP-4 4/22/2016 <0.30 74.6 1.7 33.5 10.8
70 60 60 0.7 3
Notes:
• < : Less than the method detection limit specified in the laboratory report.
• Results reported in micrograms per liter (µg/L).
• J: Estimated value.
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Analytical Method 
Contaminant of Concern 
• NCGWQS: North Carolina Ground Water Quality Standards.
• Concentrations in bold-face exceed the NCGWQS.
TABLE 2
SUMMARY OF GROUND WATER ANALYTICAL RESULTS
CAROLINA FREIGHTLINER
RALEIGH, WAKE COUNTY, NORTH CAROLINA
APRIL 22, 2016
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NCGWQS

APPENDICES

APPENDIX A
Boring Logs

Resolve Environmental Services, PLLC Phone: [phone] E. Franklin Street Fax:[phone]
Monroe, NC 28112
SUBSURFACE LOG
Project Carolina Freightliner
Address 3500 Yonkers Road, Raleigh, NC
Boring Number GP-1 Date Drilled
Sample Method Discrete Sampler Drilling Method Direct Push
Completion Details Boring terminated at 40'; Abandoned with bentonite/grout
Driller GRI-Radford Log By Kennedy
Lab Sample OVADepthSampleInterval(ft)ppm LITHOLOGY/COMMENTS
0 0-40'No cuttings collected
2
4
6
8
10
12
14
16
18
20
22

24
26
28

30
32
34

36 GP-1 36'-40'
38

40 TD 40'
04/22/16
Resolve Environmental Services, PLLC Phone: [phone] E. Franklin Street Fax:[phone]
Monroe, NC 28112
SUBSURFACE LOG
Project Carolina Freightliner
Address 3500 Yonkers Road, Raleigh, NC
Boring Number GP-2 Date Drilled
Sample Method Macrocore/Discrete Sampler Drilling Method Direct Push
Completion Details Boring terminated at 40'; Abandoned with bentonite/grout
Driller GRI-Radford Log By Kennedy
Lab Sample OVADepthSampleInterval(ft)ppm LITHOLOGY/COMMENTS
0 0-6'Red clayey SILT; no odor; dry
2
4
6 GP-2-6'6'6'-40'No Cuttings Collected
8
10
12
14
16
18
20
22

24
26
28

30
32
34

36 GP-2 36'-40'
38

40 TD 40'
04/22/16
Resolve Environmental Services, PLLC Phone: [phone] E. Franklin Street Fax:[phone]
Monroe, NC 28112
SUBSURFACE LOG
Project Carolina Freightliner
Address 3500 Yonkers Road, Raleigh, NC raleigh
Boring Number GP-3 Date Drilled
Sample Method Macrocore/Discrete Sampler Drilling Method Direct Push
Completion Details Boring terminated at 40'; Abandoned with bentonite/grout
Driller GRI-Radford Log By Kennedy
Lab Sample OVADepthSampleInterval(ft)ppm LITHOLOGY/COMMENTS
0 0-6'Red clayey SILT; no odor; dry
2
4
6 GP-3-6'6'6'-40'No Cuttings Collected
8
10
12
14
16
18
20
22

24
26
28

30
32
34

36 GP-3 36'-40'
38

40 TD 40'
04/22/16
Resolve Environmental Services, PLLC Phone: [phone] E. Franklin Street Fax:[phone]
Monroe, NC 28112
SUBSURFACE LOG
Project Carolina Freightliner
Address 3500 Yonkers Road, Raleigh, NC
Boring Number GP-4 Date Drilled
Sample Method Macrocore/Discrete Sampler Drilling Method Direct Push
Completion Details Boring terminated at 40'; Abandoned with bentonite/grout
Driller GRI-Radford Log By Kennedy
Lab Sample OVADepthSampleInterval(ft)ppm LITHOLOGY/COMMENTS
0 0-1'Black fine silty SAND; no odor; dry
GP-4-1'1'1'-5'Red clayey SILT; dry no odor
2
4
GP-4-5'5'5'-36'No Cuttings Collected
6
8
10
12
14
16
18
20
22

24
26
28

30
32 GP-4 32'-36'
34

36 TD 36'
38

40
04/22/16

APPENDIX B
Laboratory Analytical Report

04/29/16
Technical Report for
Resolve Environmental
Yonkers Rd, NC
SGS Accutest Job Number: FA33365
Sampling Date: 04/22/16
Report to:
Resolve Environmental
410 E Franklin St
Monroe, NC 28112
[e-mail]
ATTN: Laura Minor
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of SGS Accutest.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast 04/29/16
e-Hardcopy 2.0
Automated Report
57
SGS Accutest is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
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FA33365
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: FA33365-1: GP-1 ..........................................................................................................6
3.2: FA33365-2: GP-2-6' ......................................................................................................8
3.3: FA33365-3: GP-2 ..........................................................................................................11
3.4: FA33365-4: GP-3-6' ......................................................................................................13
3.5: FA33365-5: GP-3 ..........................................................................................................16
3.6: FA33365-6: GP-4-1' ......................................................................................................18
3.7: FA33365-7: GP-4-5' ......................................................................................................20
3.8: FA33365-8: GP-4 ..........................................................................................................23
Section 4: Misc. Forms ............................................................................................................25
4.1: Certification Exceptions ................................................................................................26
4.2: Chain of Custody ...........................................................................................................27
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................30
5.1: Method Blank Summary ................................................................................................31
5.2: Blank Spike Summary ...................................................................................................40
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................49
1
2
3
4
5
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FA33365
SGS Accutest
Sample Summary
Resolve Environmental
Job No:FA33365
Yonkers Rd, NC
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA33365-1 04/22/16 08:34 TK 04/23/16 AQ Ground Water GP-1
FA33365-2 04/22/16 08:53 TK 04/23/16 SO Soil GP-2-6'
FA33365-3 04/22/16 09:06 TK 04/23/16 AQ Ground Water GP-2
FA33365-4 04/22/16 09:26 TK 04/23/16 SO Soil GP-3-6'
FA33365-5 04/22/16 09:40 TK 04/23/16 AQ Ground Water GP-3
FA33365-6 04/22/16 10:00 TK 04/23/16 SO Soil GP-4-1'
FA33365-7 04/22/16 10:09 TK 04/23/16 SO Soil GP-4-5'
FA33365-8 04/22/16 10:17 TK 04/23/16 AQ Ground Water GP-4
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
3 of 57
FA33365
1
Summary of Hits Page 1 of 1
Job Number:FA33365
Account:Resolve Environmental
Project:Yonkers Rd, NC
Collected:04/22/16
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA33365-1 GP-1
No hits reported in this sample.
FA33365-2 GP-2-6'
Acetone 0.0298 J 0.066 0.014 mg/kg SW846 8260B
FA33365-3 GP-2
No hits reported in this sample.
FA33365-4 GP-3-6'
Acetone 0.0315 J 0.068 0.014 mg/kg SW846 8260B
Tetrachloroethylene 0.0050 J 0.0068 0.0018 mg/kg SW846 8260B
FA33365-5 GP-3
Chloroform 0.57 J 1.0 0.30 ug/l SW846 8260B
FA33365-6 GP-4-1'
Acetone 0.336 0.095 0.019 mg/kg SW846 8260B
2-Butanone (MEK)0.0583 0.048 0.017 mg/kg SW846 8260B
4-Methyl-2-pentanone (MIBK)0.140 0.048 0.020 mg/kg SW846 8260B
FA33365-7 GP-4-5'
Acetone 0.0426 J 0.056 0.011 mg/kg SW846 8260B
FA33365-8 GP-4
cis-1,2-Dichloroethylene 74.6 1.0 0.31 ug/l SW846 8260B
trans-1,2-Dichloroethylene 1.7 1.0 0.33 ug/l SW846 8260B
Tetrachloroethylene 33.5 1.0 0.30 ug/l SW846 8260B
Trichloroethylene 10.8 1.0 0.27 ug/l SW846 8260B
4 of 57
FA33365
2
SGS Accutest
Sample Results
Report of Analysis
Southeast
Section 3
5 of 57
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SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:GP-1
Lab Sample ID:FA33365-1 Date Sampled:04/22/16
Matrix:AQ - Ground Water Date Received:04/23/16
Method:SW846 8260B Percent Solids:n/a
Project:Yonkers Rd, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 J0976118.D 1 04/27/16 DP n/a n/a VJ5276
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.20 ug/l
108-86-1 Bromobenzene ND 1.0 0.42 ug/l
74-97-5 Bromochloromethane ND 1.0 0.42 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.46 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.6 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.43 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.25 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.40 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.30 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.63 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.24 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.36 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.26 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.33 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.27 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.24 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.39 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.26 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.28 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.22 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.31 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.33 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.34 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.27 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.29 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.26 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 of 57
FA33365
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.
1
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:GP-1
Lab Sample ID:FA33365-1 Date Sampled:04/22/16
Matrix:AQ - Ground Water Date Received:04/23/16
Method:SW846 8260B Percent Solids:n/a
Project:Yonkers Rd, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.25 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.23 ug/l
64-17-5 Ethyl Alcohol ND 200 50 ug/l
100-41-4 Ethylbenzene ND 1.0 0.25 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.33 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.28 ug/l
74-83-9 Methyl Bromide ND 2.0 0.50 ug/l
74-87-3 Methyl Chloride ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.4 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.20 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.20 ug/l
100-42-5 Styrene ND 1.0 0.24 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.33 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.30 ug/l
108-88-3 Toluene ND 1.0 0.20 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.51 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.20 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.37 ug/l
79-01-6 Trichloroethylene ND 1.0 0.27 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.66 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.20 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.20 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.31 ug/l
m,p-Xylene ND 2.0 0.30 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.56 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%83-118%
17060-07-0 1,2-Dichloroethane-D4 102%79-125%
2037-26-5 Toluene-D8 95%85-112%
460-00-4 4-Bromofluorobenzene 103%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:GP-2-6'
Lab Sample ID:FA33365-2 Date Sampled:04/22/16
Matrix:SO - Soil Date Received:04/23/16
Method:SW846 8260B Percent Solids:79.9
Project:Yonkers Rd, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F0076978.D 1 04/26/16 EP n/a n/a VF2643
Run #2
Initial Weight Final Volume
Run #1 4.71 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.0298 0.066 0.014 mg/kg J
71-43-2 Benzene ND 0.0066 0.0017 mg/kg
108-86-1 Bromobenzene ND 0.0066 0.0016 mg/kg
74-97-5 Bromochloromethane ND 0.0066 0.0015 mg/kg
75-27-4 Bromodichloromethane ND 0.0066 0.0013 mg/kg
75-25-2 Bromoform a ND 0.0066 0.0013 mg/kg
78-93-3 2-Butanone (MEK)ND 0.033 0.012 mg/kg
104-51-8 n-Butylbenzene ND 0.0066 0.0013 mg/kg
135-98-8 sec-Butylbenzene ND 0.0066 0.0013 mg/kg
98-06-6 tert-Butylbenzene ND 0.0066 0.0013 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0066 0.0024 mg/kg
108-90-7 Chlorobenzene ND 0.0066 0.0013 mg/kg
75-00-3 Chloroethane ND 0.0066 0.0027 mg/kg
67-66-3 Chloroform ND 0.0066 0.0016 mg/kg
95-49-8 o-Chlorotoluene ND 0.0066 0.0013 mg/kg
106-43-4 p-Chlorotoluene ND 0.0066 0.0013 mg/kg
124-48-1 Dibromochloromethane ND 0.0066 0.0013 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0066 0.0013 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0066 0.0033 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0066 0.0013 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0066 0.0013 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0066 0.0014 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0066 0.0022 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0066 0.0013 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0066 0.0013 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0066 0.0016 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0066 0.0020 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0066 0.0021 mg/kg
142-28-9 1,3-Dichloropropane ND 0.0066 0.0013 mg/kg
594-20-7 2,2-Dichloropropane ND 0.0066 0.0013 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0066 0.0017 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0066 0.0025 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:GP-2-6'
Lab Sample ID:FA33365-2 Date Sampled:04/22/16
Matrix:SO - Soil Date Received:04/23/16
Method:SW846 8260B Percent Solids:79.9
Project:Yonkers Rd, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0066 0.0013 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.0066 0.0016 mg/kg
64-17-5 Ethyl Alcohol ND 0.53 0.11 mg/kg
100-41-4 Ethylbenzene ND 0.0066 0.0014 mg/kg
591-78-6 2-Hexanone ND 0.033 0.012 mg/kg
98-82-8 Isopropylbenzene ND 0.0066 0.0019 mg/kg
99-87-6 p-Isopropyltoluene ND 0.0066 0.0013 mg/kg
74-83-9 Methyl Bromide ND 0.0066 0.0034 mg/kg
74-87-3 Methyl Chloride ND 0.0066 0.0032 mg/kg
75-09-2 Methylene Chloride ND 0.013 0.0053 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.033 0.014 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0066 0.0015 mg/kg
91-20-3 Naphthalene ND 0.0066 0.0027 mg/kg
103-65-1 n-Propylbenzene ND 0.0066 0.0016 mg/kg
100-42-5 Styrene ND 0.0066 0.0013 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0066 0.0015 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0066 0.0029 mg/kg
127-18-4 Tetrachloroethylene ND 0.0066 0.0017 mg/kg
108-88-3 Toluene ND 0.0066 0.0015 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0066 0.0026 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0066 0.0020 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0066 0.0013 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0066 0.0024 mg/kg
79-01-6 Trichloroethylene ND 0.0066 0.0016 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0066 0.0025 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0066 0.0022 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0066 0.0013 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0066 0.0013 mg/kg
108-05-4 Vinyl Acetate ND 0.033 0.012 mg/kg
75-01-4 Vinyl Chloride ND 0.0066 0.0022 mg/kg
m,p-Xylene ND 0.013 0.0023 mg/kg
95-47-6 o-Xylene ND 0.0066 0.0015 mg/kg
1330-20-7 Xylene (total)ND 0.020 0.0038 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%75-124%
17060-07-0 1,2-Dichloroethane-D4 132%72-135%
2037-26-5 Toluene-D8 102%75-126%
460-00-4 4-Bromofluorobenzene 117%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:GP-2-6'
Lab Sample ID:FA33365-2 Date Sampled:04/22/16
Matrix:SO - Soil Date Received:04/23/16
Method:SW846 8260B Percent Solids:79.9
Project:Yonkers Rd, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:GP-2
Lab Sample ID:FA33365-3 Date Sampled:04/22/16
Matrix:AQ - Ground Water Date Received:04/23/16
Method:SW846 8260B Percent Solids:n/a
Project:Yonkers Rd, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 J0976119.D 1 04/27/16 DP n/a n/a VJ5276
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.20 ug/l
108-86-1 Bromobenzene ND 1.0 0.42 ug/l
74-97-5 Bromochloromethane ND 1.0 0.42 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.46 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.6 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.43 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.25 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.40 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.30 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.63 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.24 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.36 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.26 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.33 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.27 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.24 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.39 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.26 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.28 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.22 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.31 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.33 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.34 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.27 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.29 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.26 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:GP-2
Lab Sample ID:FA33365-3 Date Sampled:04/22/16
Matrix:AQ - Ground Water Date Received:04/23/16
Method:SW846 8260B Percent Solids:n/a
Project:Yonkers Rd, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.25 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.23 ug/l
64-17-5 Ethyl Alcohol ND 200 50 ug/l
100-41-4 Ethylbenzene ND 1.0 0.25 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.33 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.28 ug/l
74-83-9 Methyl Bromide ND 2.0 0.50 ug/l
74-87-3 Methyl Chloride ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.4 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.20 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.20 ug/l
100-42-5 Styrene ND 1.0 0.24 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.33 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.30 ug/l
108-88-3 Toluene ND 1.0 0.20 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.51 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.20 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.37 ug/l
79-01-6 Trichloroethylene ND 1.0 0.27 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.66 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.20 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.20 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.31 ug/l
m,p-Xylene ND 2.0 0.30 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.56 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%83-118%
17060-07-0 1,2-Dichloroethane-D4 99%79-125%
2037-26-5 Toluene-D8 103%85-112%
460-00-4 4-Bromofluorobenzene 104%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:GP-3-6'
Lab Sample ID:FA33365-4 Date Sampled:04/22/16
Matrix:SO - Soil Date Received:04/23/16
Method:SW846 8260B Percent Solids:66.9
Project:Yonkers Rd, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F0076979.D 1 04/26/16 EP n/a n/a VF2643
Run #2
Initial Weight Final Volume
Run #1 5.46 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.0315 0.068 0.014 mg/kg J
71-43-2 Benzene ND 0.0068 0.0017 mg/kg
108-86-1 Bromobenzene ND 0.0068 0.0017 mg/kg
74-97-5 Bromochloromethane ND 0.0068 0.0015 mg/kg
75-27-4 Bromodichloromethane ND 0.0068 0.0014 mg/kg
75-25-2 Bromoform a ND 0.0068 0.0014 mg/kg
78-93-3 2-Butanone (MEK)ND 0.034 0.012 mg/kg
104-51-8 n-Butylbenzene ND 0.0068 0.0014 mg/kg
135-98-8 sec-Butylbenzene ND 0.0068 0.0014 mg/kg
98-06-6 tert-Butylbenzene ND 0.0068 0.0014 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0068 0.0024 mg/kg
108-90-7 Chlorobenzene ND 0.0068 0.0014 mg/kg
75-00-3 Chloroethane ND 0.0068 0.0027 mg/kg
67-66-3 Chloroform ND 0.0068 0.0017 mg/kg
95-49-8 o-Chlorotoluene ND 0.0068 0.0014 mg/kg
106-43-4 p-Chlorotoluene ND 0.0068 0.0014 mg/kg
124-48-1 Dibromochloromethane ND 0.0068 0.0014 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0068 0.0014 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0068 0.0034 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0068 0.0014 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0068 0.0014 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0068 0.0014 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0068 0.0023 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0068 0.0014 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0068 0.0014 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0068 0.0016 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0068 0.0021 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0068 0.0022 mg/kg
142-28-9 1,3-Dichloropropane ND 0.0068 0.0014 mg/kg
594-20-7 2,2-Dichloropropane ND 0.0068 0.0014 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0068 0.0018 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0068 0.0026 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:GP-3-6'
Lab Sample ID:FA33365-4 Date Sampled:04/22/16
Matrix:SO - Soil Date Received:04/23/16
Method:SW846 8260B Percent Solids:66.9
Project:Yonkers Rd, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0068 0.0014 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.0068 0.0016 mg/kg
64-17-5 Ethyl Alcohol ND 0.55 0.11 mg/kg
100-41-4 Ethylbenzene ND 0.0068 0.0015 mg/kg
591-78-6 2-Hexanone ND 0.034 0.012 mg/kg
98-82-8 Isopropylbenzene ND 0.0068 0.0019 mg/kg
99-87-6 p-Isopropyltoluene ND 0.0068 0.0014 mg/kg
74-83-9 Methyl Bromide ND 0.0068 0.0035 mg/kg
74-87-3 Methyl Chloride ND 0.0068 0.0033 mg/kg
75-09-2 Methylene Chloride ND 0.014 0.0055 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.034 0.015 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0068 0.0015 mg/kg
91-20-3 Naphthalene ND 0.0068 0.0027 mg/kg
103-65-1 n-Propylbenzene ND 0.0068 0.0017 mg/kg
100-42-5 Styrene ND 0.0068 0.0014 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0068 0.0015 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0068 0.0030 mg/kg
127-18-4 Tetrachloroethylene 0.0050 0.0068 0.0018 mg/kg J
108-88-3 Toluene ND 0.0068 0.0015 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0068 0.0027 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0068 0.0020 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0068 0.0014 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0068 0.0025 mg/kg
79-01-6 Trichloroethylene ND 0.0068 0.0016 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0068 0.0026 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0068 0.0022 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0068 0.0014 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0068 0.0014 mg/kg
108-05-4 Vinyl Acetate ND 0.034 0.013 mg/kg
75-01-4 Vinyl Chloride ND 0.0068 0.0023 mg/kg
m,p-Xylene ND 0.014 0.0024 mg/kg
95-47-6 o-Xylene ND 0.0068 0.0015 mg/kg
1330-20-7 Xylene (total)ND 0.021 0.0039 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 108%75-124%
17060-07-0 1,2-Dichloroethane-D4 122%72-135%
2037-26-5 Toluene-D8 96%75-126%
460-00-4 4-Bromofluorobenzene 110%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:GP-3-6'
Lab Sample ID:FA33365-4 Date Sampled:04/22/16
Matrix:SO - Soil Date Received:04/23/16
Method:SW846 8260B Percent Solids:66.9
Project:Yonkers Rd, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:GP-3
Lab Sample ID:FA33365-5 Date Sampled:04/22/16
Matrix:AQ - Ground Water Date Received:04/23/16
Method:SW846 8260B Percent Solids:n/a
Project:Yonkers Rd, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 J0976120.D 1 04/27/16 DP n/a n/a VJ5276
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.20 ug/l
108-86-1 Bromobenzene ND 1.0 0.42 ug/l
74-97-5 Bromochloromethane ND 1.0 0.42 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.46 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.6 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.43 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.25 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.40 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.30 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.63 ug/l
67-66-3 Chloroform 0.57 1.0 0.30 ug/l J
95-49-8 o-Chlorotoluene ND 1.0 0.24 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.36 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.26 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.33 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.27 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.24 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.39 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.26 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.28 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.22 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.31 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.33 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.34 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.27 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.29 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.26 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:GP-3
Lab Sample ID:FA33365-5 Date Sampled:04/22/16
Matrix:AQ - Ground Water Date Received:04/23/16
Method:SW846 8260B Percent Solids:n/a
Project:Yonkers Rd, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.25 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.23 ug/l
64-17-5 Ethyl Alcohol ND 200 50 ug/l
100-41-4 Ethylbenzene ND 1.0 0.25 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.33 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.28 ug/l
74-83-9 Methyl Bromide ND 2.0 0.50 ug/l
74-87-3 Methyl Chloride ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.4 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.20 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.20 ug/l
100-42-5 Styrene ND 1.0 0.24 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.33 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.30 ug/l
108-88-3 Toluene ND 1.0 0.20 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.51 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.20 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.37 ug/l
79-01-6 Trichloroethylene ND 1.0 0.27 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.66 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.20 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.20 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.31 ug/l
m,p-Xylene ND 2.0 0.30 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.56 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%83-118%
17060-07-0 1,2-Dichloroethane-D4 100%79-125%
2037-26-5 Toluene-D8 96%85-112%
460-00-4 4-Bromofluorobenzene 104%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:GP-4-1'
Lab Sample ID:FA33365-6 Date Sampled:04/22/16
Matrix:SO - Soil Date Received:04/23/16
Method:SW846 8260B Percent Solids:58.9
Project:Yonkers Rd, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F0077028.D 1 04/28/16 EP n/a n/a VF2644
Run #2
Initial Weight Final Volume
Run #1 4.46 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.336 0.095 0.019 mg/kg
71-43-2 Benzene ND 0.0095 0.0024 mg/kg
108-86-1 Bromobenzene ND 0.0095 0.0023 mg/kg
74-97-5 Bromochloromethane ND 0.0095 0.0021 mg/kg
75-27-4 Bromodichloromethane ND 0.0095 0.0019 mg/kg
75-25-2 Bromoform ND 0.0095 0.0019 mg/kg
78-93-3 2-Butanone (MEK)0.0583 0.048 0.017 mg/kg
104-51-8 n-Butylbenzene ND 0.0095 0.0019 mg/kg
135-98-8 sec-Butylbenzene ND 0.0095 0.0019 mg/kg
98-06-6 tert-Butylbenzene ND 0.0095 0.0019 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0095 0.0034 mg/kg
108-90-7 Chlorobenzene ND 0.0095 0.0019 mg/kg
75-00-3 Chloroethane ND 0.0095 0.0038 mg/kg
67-66-3 Chloroform ND 0.0095 0.0023 mg/kg
95-49-8 o-Chlorotoluene ND 0.0095 0.0019 mg/kg
106-43-4 p-Chlorotoluene ND 0.0095 0.0019 mg/kg
124-48-1 Dibromochloromethane ND 0.0095 0.0019 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0095 0.0019 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0095 0.0047 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0095 0.0019 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0095 0.0019 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0095 0.0019 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0095 0.0032 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0095 0.0019 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0095 0.0019 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0095 0.0023 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0095 0.0029 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0095 0.0030 mg/kg
142-28-9 1,3-Dichloropropane ND 0.0095 0.0019 mg/kg
594-20-7 2,2-Dichloropropane ND 0.0095 0.0019 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0095 0.0025 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0095 0.0036 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:GP-4-1'
Lab Sample ID:FA33365-6 Date Sampled:04/22/16
Matrix:SO - Soil Date Received:04/23/16
Method:SW846 8260B Percent Solids:58.9
Project:Yonkers Rd, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0095 0.0019 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.0095 0.0023 mg/kg
64-17-5 Ethyl Alcohol ND 0.76 0.16 mg/kg
100-41-4 Ethylbenzene ND 0.0095 0.0021 mg/kg
591-78-6 2-Hexanone ND 0.048 0.017 mg/kg
98-82-8 Isopropylbenzene ND 0.0095 0.0027 mg/kg
99-87-6 p-Isopropyltoluene ND 0.0095 0.0019 mg/kg
74-83-9 Methyl Bromide ND 0.0095 0.0049 mg/kg
74-87-3 Methyl Chloride ND 0.0095 0.0046 mg/kg
75-09-2 Methylene Chloride ND 0.019 0.0076 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)0.140 0.048 0.020 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0095 0.0021 mg/kg
91-20-3 Naphthalene ND 0.0095 0.0038 mg/kg
103-65-1 n-Propylbenzene ND 0.0095 0.0024 mg/kg
100-42-5 Styrene ND 0.0095 0.0019 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0095 0.0021 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0095 0.0042 mg/kg
127-18-4 Tetrachloroethylene ND 0.0095 0.0025 mg/kg
108-88-3 Toluene ND 0.0095 0.0022 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0095 0.0038 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0095 0.0028 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0095 0.0019 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0095 0.0034 mg/kg
79-01-6 Trichloroethylene ND 0.0095 0.0022 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0095 0.0036 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0095 0.0031 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0095 0.0019 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0095 0.0019 mg/kg
108-05-4 Vinyl Acetate ND 0.048 0.018 mg/kg
75-01-4 Vinyl Chloride ND 0.0095 0.0032 mg/kg
m,p-Xylene ND 0.019 0.0033 mg/kg
95-47-6 o-Xylene ND 0.0095 0.0021 mg/kg
1330-20-7 Xylene (total)ND 0.029 0.0054 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%75-124%
17060-07-0 1,2-Dichloroethane-D4 110%72-135%
2037-26-5 Toluene-D8 124%75-126%
460-00-4 4-Bromofluorobenzene 127%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:GP-4-5'
Lab Sample ID:FA33365-7 Date Sampled:04/22/16
Matrix:SO - Soil Date Received:04/23/16
Method:SW846 8260B Percent Solids:82.9
Project:Yonkers Rd, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F0076981.D 1 04/26/16 EP n/a n/a VF2643
Run #2
Initial Weight Final Volume
Run #1 5.35 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.0426 0.056 0.011 mg/kg J
71-43-2 Benzene ND 0.0056 0.0014 mg/kg
108-86-1 Bromobenzene ND 0.0056 0.0014 mg/kg
74-97-5 Bromochloromethane ND 0.0056 0.0013 mg/kg
75-27-4 Bromodichloromethane ND 0.0056 0.0011 mg/kg
75-25-2 Bromoform a ND 0.0056 0.0011 mg/kg
78-93-3 2-Butanone (MEK)ND 0.028 0.010 mg/kg
104-51-8 n-Butylbenzene ND 0.0056 0.0011 mg/kg
135-98-8 sec-Butylbenzene ND 0.0056 0.0011 mg/kg
98-06-6 tert-Butylbenzene ND 0.0056 0.0011 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0056 0.0020 mg/kg
108-90-7 Chlorobenzene ND 0.0056 0.0011 mg/kg
75-00-3 Chloroethane ND 0.0056 0.0023 mg/kg
67-66-3 Chloroform ND 0.0056 0.0014 mg/kg
95-49-8 o-Chlorotoluene ND 0.0056 0.0011 mg/kg
106-43-4 p-Chlorotoluene ND 0.0056 0.0011 mg/kg
124-48-1 Dibromochloromethane ND 0.0056 0.0011 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0056 0.0011 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0056 0.0028 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0056 0.0011 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0056 0.0011 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0056 0.0011 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0056 0.0019 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0056 0.0011 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0056 0.0011 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0056 0.0014 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0056 0.0017 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0056 0.0018 mg/kg
142-28-9 1,3-Dichloropropane ND 0.0056 0.0011 mg/kg
594-20-7 2,2-Dichloropropane ND 0.0056 0.0011 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0056 0.0015 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0056 0.0021 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:GP-4-5'
Lab Sample ID:FA33365-7 Date Sampled:04/22/16
Matrix:SO - Soil Date Received:04/23/16
Method:SW846 8260B Percent Solids:82.9
Project:Yonkers Rd, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0056 0.0011 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.0056 0.0013 mg/kg
64-17-5 Ethyl Alcohol ND 0.45 0.094 mg/kg
100-41-4 Ethylbenzene ND 0.0056 0.0012 mg/kg
591-78-6 2-Hexanone ND 0.028 0.0098 mg/kg
98-82-8 Isopropylbenzene ND 0.0056 0.0016 mg/kg
99-87-6 p-Isopropyltoluene ND 0.0056 0.0011 mg/kg
74-83-9 Methyl Bromide ND 0.0056 0.0029 mg/kg
74-87-3 Methyl Chloride ND 0.0056 0.0027 mg/kg
75-09-2 Methylene Chloride ND 0.011 0.0045 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.028 0.012 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0056 0.0013 mg/kg
91-20-3 Naphthalene ND 0.0056 0.0023 mg/kg
103-65-1 n-Propylbenzene ND 0.0056 0.0014 mg/kg
100-42-5 Styrene ND 0.0056 0.0011 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0056 0.0013 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0056 0.0025 mg/kg
127-18-4 Tetrachloroethylene ND 0.0056 0.0015 mg/kg
108-88-3 Toluene ND 0.0056 0.0013 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0056 0.0022 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0056 0.0017 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0056 0.0011 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0056 0.0020 mg/kg
79-01-6 Trichloroethylene ND 0.0056 0.0013 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0056 0.0021 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0056 0.0018 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0056 0.0011 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0056 0.0011 mg/kg
108-05-4 Vinyl Acetate ND 0.028 0.011 mg/kg
75-01-4 Vinyl Chloride ND 0.0056 0.0019 mg/kg
m,p-Xylene ND 0.011 0.0020 mg/kg
95-47-6 o-Xylene ND 0.0056 0.0012 mg/kg
1330-20-7 Xylene (total)ND 0.017 0.0032 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 112%75-124%
17060-07-0 1,2-Dichloroethane-D4 130%72-135%
2037-26-5 Toluene-D8 100%75-126%
460-00-4 4-Bromofluorobenzene 109%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:GP-4-5'
Lab Sample ID:FA33365-7 Date Sampled:04/22/16
Matrix:SO - Soil Date Received:04/23/16
Method:SW846 8260B Percent Solids:82.9
Project:Yonkers Rd, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:GP-4
Lab Sample ID:FA33365-8 Date Sampled:04/22/16
Matrix:AQ - Ground Water Date Received:04/23/16
Method:SW846 8260B Percent Solids:n/a
Project:Yonkers Rd, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 J0976121.D 1 04/27/16 DP n/a n/a VJ5276
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.20 ug/l
108-86-1 Bromobenzene ND 1.0 0.42 ug/l
74-97-5 Bromochloromethane ND 1.0 0.42 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.46 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.6 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.43 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.25 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.40 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.30 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.63 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.24 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.36 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.26 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.33 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.27 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.24 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.39 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.26 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.28 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.22 ug/l
156-59-2 cis-1,2-Dichloroethylene 74.6 1.0 0.31 ug/l
156-60-5 trans-1,2-Dichloroethylene 1.7 1.0 0.33 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.34 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.27 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.29 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.26 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:GP-4
Lab Sample ID:FA33365-8 Date Sampled:04/22/16
Matrix:AQ - Ground Water Date Received:04/23/16
Method:SW846 8260B Percent Solids:n/a
Project:Yonkers Rd, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.25 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.23 ug/l
64-17-5 Ethyl Alcohol ND 200 50 ug/l
100-41-4 Ethylbenzene ND 1.0 0.25 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.33 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.28 ug/l
74-83-9 Methyl Bromide ND 2.0 0.50 ug/l
74-87-3 Methyl Chloride ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.4 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.20 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.20 ug/l
100-42-5 Styrene ND 1.0 0.24 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.33 ug/l
127-18-4 Tetrachloroethylene 33.5 1.0 0.30 ug/l
108-88-3 Toluene ND 1.0 0.20 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.51 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.20 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.37 ug/l
79-01-6 Trichloroethylene 10.8 1.0 0.27 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.66 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.20 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.20 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.31 ug/l
m,p-Xylene ND 2.0 0.30 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.56 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%83-118%
17060-07-0 1,2-Dichloroethane-D4 102%79-125%
2037-26-5 Toluene-D8 94%85-112%
460-00-4 4-Bromofluorobenzene 102%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Certification Exceptions
• Chain of Custody
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Parameter Certification Exceptions Page 1 of 1
Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
The following parameters included in this report are exceptions to NELAC certification.
The certification status of each is indicated below.
Parameter CAS#Method Mat Certification Status
Di-Isopropyl Ether 108-20-3 SW846 8260B AQ Certified by SOP MS005
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GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
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Method Blank Summary Page 1 of 3
Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2643-MB F0076964.D 1 04/26/16 EP n/a n/a VF2643
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-2, FA33365-4, FA33365-7
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 50 10 ug/kg
71-43-2 Benzene ND 5.0 1.3 ug/kg
108-86-1 Bromobenzene ND 5.0 1.2 ug/kg
74-97-5 Bromochloromethane ND 5.0 1.1 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 9.1 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/kg
98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.8 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.2 ug/kg
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg
106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.5 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.0 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.7 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.2 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.5 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.6 ug/kg
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/kg
563-58-6 1,1-Dichloropropene ND 5.0 1.3 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.9 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
108-20-3 Di-Isopropyl Ether ND 5.0 1.2 ug/kg
64-17-5 Ethyl Alcohol ND 400 84 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.1 ug/kg
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Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2643-MB F0076964.D 1 04/26/16 EP n/a n/a VF2643
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-2, FA33365-4, FA33365-7
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 25 8.7 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.4 ug/kg
99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.6 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.4 ug/kg
75-09-2 Methylene Chloride ND 10 4.0 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 11 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.1 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.2 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.1 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 2.2 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 5.0 1.1 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.0 2.0 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.5 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.8 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.2 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 1.9 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.0 1.6 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
108-05-4 Vinyl Acetate ND 25 9.4 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.7 ug/kg
m,p-Xylene ND 10 1.8 ug/kg
95-47-6 o-Xylene ND 5.0 1.1 ug/kg
1330-20-7 Xylene (total)ND 15 2.9 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 102%75-124%
17060-07-0 1,2-Dichloroethane-D4 119%72-135%
2037-26-5 Toluene-D8 104%75-126%
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Method Blank Summary Page 3 of 3
Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2643-MB F0076964.D 1 04/26/16 EP n/a n/a VF2643
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-2, FA33365-4, FA33365-7
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 109%71-133%
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Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VJ5276-MB J0976105.D 1 04/27/16 DP n/a n/a VJ5276
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-1, FA33365-3, FA33365-5, FA33365-8
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.20 ug/l
108-86-1 Bromobenzene ND 1.0 0.42 ug/l
74-97-5 Bromochloromethane ND 1.0 0.42 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.46 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.6 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.43 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.25 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.40 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.30 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.63 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.24 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.36 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.26 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.33 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.27 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.24 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.39 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.26 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.28 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.22 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.31 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.33 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.34 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.27 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.29 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.26 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.25 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.23 ug/l
64-17-5 Ethyl Alcohol ND 200 50 ug/l
100-41-4 Ethylbenzene ND 1.0 0.25 ug/l
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Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VJ5276-MB J0976105.D 1 04/27/16 DP n/a n/a VJ5276
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-1, FA33365-3, FA33365-5, FA33365-8
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.33 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.28 ug/l
74-83-9 Methyl Bromide ND 2.0 0.50 ug/l
74-87-3 Methyl Chloride ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.4 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.20 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.20 ug/l
100-42-5 Styrene ND 1.0 0.24 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.33 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.30 ug/l
108-88-3 Toluene ND 1.0 0.20 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.51 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.20 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.37 ug/l
79-01-6 Trichloroethylene ND 1.0 0.27 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.66 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.20 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.20 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.31 ug/l
m,p-Xylene ND 2.0 0.30 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.56 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%83-118%
17060-07-0 1,2-Dichloroethane-D4 100%79-125%
2037-26-5 Toluene-D8 101%85-112%
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Method Blank Summary Page 3 of 3
Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VJ5276-MB J0976105.D 1 04/27/16 DP n/a n/a VJ5276
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-1, FA33365-3, FA33365-5, FA33365-8
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 106%83-118%
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Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2644-MB F0077037.D 1 04/28/16 EP n/a n/a VF2644
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-6
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 50 10 ug/kg
71-43-2 Benzene ND 5.0 1.3 ug/kg
108-86-1 Bromobenzene ND 5.0 1.2 ug/kg
74-97-5 Bromochloromethane ND 5.0 1.1 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 9.1 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/kg
98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.8 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.2 ug/kg
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg
106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.5 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.0 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.7 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.2 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.5 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.6 ug/kg
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/kg
563-58-6 1,1-Dichloropropene ND 5.0 1.3 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.9 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
108-20-3 Di-Isopropyl Ether ND 5.0 1.2 ug/kg
64-17-5 Ethyl Alcohol ND 400 84 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.1 ug/kg
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Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2644-MB F0077037.D 1 04/28/16 EP n/a n/a VF2644
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-6
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 25 8.7 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.4 ug/kg
99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.6 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.4 ug/kg
75-09-2 Methylene Chloride ND 10 4.0 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 11 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.1 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.2 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.1 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 2.2 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 5.0 1.1 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.0 2.0 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.5 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.8 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.2 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 1.9 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.0 1.6 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
108-05-4 Vinyl Acetate ND 25 9.4 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.7 ug/kg
m,p-Xylene ND 10 1.8 ug/kg
95-47-6 o-Xylene ND 5.0 1.1 ug/kg
1330-20-7 Xylene (total)ND 15 2.9 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%75-124%
17060-07-0 1,2-Dichloroethane-D4 105%72-135%
2037-26-5 Toluene-D8 97%75-126%
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Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2644-MB F0077037.D 1 04/28/16 EP n/a n/a VF2644
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-6
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 111%71-133%
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Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2643-BS F0076963.D 1 04/26/16 EP n/a n/a VF2643
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-2, FA33365-4, FA33365-7
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 247 99 61-152
71-43-2 Benzene 50 47.4 95 76-126
108-86-1 Bromobenzene 50 53.8 108 76-122
74-97-5 Bromochloromethane 50 51.6 103 77-120
75-27-4 Bromodichloromethane 50 49.7 99 74-130
75-25-2 Bromoform 50 35.2 70* a 76-127
78-93-3 2-Butanone (MEK)250 226 90 75-137
104-51-8 n-Butylbenzene 50 56.3 113 71-128
135-98-8 sec-Butylbenzene 50 54.9 110 79-135
98-06-6 tert-Butylbenzene 50 55.0 110 77-133
56-23-5 Carbon Tetrachloride 50 47.6 95 78-133
108-90-7 Chlorobenzene 50 51.5 103 81-129
75-00-3 Chloroethane 50 46.6 93 68-133
67-66-3 Chloroform 50 47.9 96 72-123
95-49-8 o-Chlorotoluene 50 55.2 110 77-129
106-43-4 p-Chlorotoluene 50 54.4 109 80-134
124-48-1 Dibromochloromethane 50 50.1 100 76-127
106-93-4 1,2-Dibromoethane 50 52.7 105 77-126
75-71-8 Dichlorodifluoromethane 50 44.6 89 68-168
95-50-1 1,2-Dichlorobenzene 50 54.6 109 80-129
541-73-1 1,3-Dichlorobenzene 50 53.7 107 81-129
106-46-7 1,4-Dichlorobenzene 50 55.1 110 76-130
75-34-3 1,1-Dichloroethane 50 45.8 92 73-125
107-06-2 1,2-Dichloroethane 50 47.1 94 74-128
75-35-4 1,1-Dichloroethylene 50 46.7 93 81-136
156-59-2 cis-1,2-Dichloroethylene 50 48.8 98 74-126
156-60-5 trans-1,2-Dichloroethylene 50 46.8 94 70-127
78-87-5 1,2-Dichloropropane 50 48.4 97 74-125
142-28-9 1,3-Dichloropropane 50 47.8 96 76-122
594-20-7 2,2-Dichloropropane 50 50.4 101 77-133
563-58-6 1,1-Dichloropropene 50 47.7 95 75-130
10061-01-5 cis-1,3-Dichloropropene 50 50.3 101 80-123
10061-02-6 trans-1,3-Dichloropropene 50 49.1 98 75-131
108-20-3 Di-Isopropyl Ether 50 48.8 98 75-122
64-17-5 Ethyl Alcohol 1000 1030 103 53-154
100-41-4 Ethylbenzene 50 50.9 102 77-123
* = Outside of Control Limits.
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Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2643-BS F0076963.D 1 04/26/16 EP n/a n/a VF2643
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-2, FA33365-4, FA33365-7
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
591-78-6 2-Hexanone 250 230 92 72-133
98-82-8 Isopropylbenzene 50 47.5 95 80-136
99-87-6 p-Isopropyltoluene 50 56.2 112 77-131
74-83-9 Methyl Bromide 50 47.9 96 65-139
74-87-3 Methyl Chloride 50 42.9 86 71-144
75-09-2 Methylene Chloride 50 50.2 100 74-137
108-10-1 4-Methyl-2-pentanone (MIBK)250 210 84 76-132
1634-04-4 Methyl Tert Butyl Ether 50 49.7 99 77-120
91-20-3 Naphthalene 50 53.9 108 79-129
103-65-1 n-Propylbenzene 50 55.4 111 80-135
100-42-5 Styrene 50 48.0 96 78-125
630-20-6 1,1,1,2-Tetrachloroethane 50 52.1 104 78-126
79-34-5 1,1,2,2-Tetrachloroethane 50 48.9 98 71-126
127-18-4 Tetrachloroethylene 50 49.9 100 79-130
108-88-3 Toluene 50 49.7 99 76-124
87-61-6 1,2,3-Trichlorobenzene 50 55.7 111 77-128
120-82-1 1,2,4-Trichlorobenzene 50 60.4 121 78-130
71-55-6 1,1,1-Trichloroethane 50 48.3 97 70-129
79-00-5 1,1,2-Trichloroethane 50 48.0 96 74-124
79-01-6 Trichloroethylene 50 48.2 96 75-128
75-69-4 Trichlorofluoromethane 50 48.4 97 73-145
96-18-4 1,2,3-Trichloropropane 50 48.3 97 74-127
95-63-6 1,2,4-Trimethylbenzene 50 56.9 114 74-123
108-67-8 1,3,5-Trimethylbenzene 50 56.3 113 73-122
108-05-4 Vinyl Acetate 250 239 96 48-164
75-01-4 Vinyl Chloride 50 45.7 91 76-141
m,p-Xylene 100 102 102 80-128
95-47-6 o-Xylene 50 49.3 99 80-132
1330-20-7 Xylene (total)150 151 101 80-129
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%75-124%
17060-07-0 1,2-Dichloroethane-D4 97%72-135%
2037-26-5 Toluene-D8 101%75-126%
* = Outside of Control Limits.
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Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2643-BS F0076963.D 1 04/26/16 EP n/a n/a VF2643
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-2, FA33365-4, FA33365-7
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 102%71-133%
(a) Sporadic marginal failure.
* = Outside of Control Limits.
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Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VJ5276-BS J0976104.D 1 04/27/16 DP n/a n/a VJ5276
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-1, FA33365-3, FA33365-5, FA33365-8
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
67-64-1 Acetone 125 106 85 50-147
71-43-2 Benzene 25 26.4 106 81-122
108-86-1 Bromobenzene 25 26.6 106 80-121
74-97-5 Bromochloromethane 25 24.8 99 76-123
75-27-4 Bromodichloromethane 25 27.8 111 79-123
75-25-2 Bromoform 25 25.4 102 66-123
78-93-3 2-Butanone (MEK)125 114 91 56-143
104-51-8 n-Butylbenzene 25 27.8 111 79-126
135-98-8 sec-Butylbenzene 25 29.2 117 83-133
98-06-6 tert-Butylbenzene 25 27.2 109 80-133
56-23-5 Carbon Tetrachloride 25 31.6 126 76-136
108-90-7 Chlorobenzene 25 26.2 105 82-124
75-00-3 Chloroethane 25 31.4 126 62-144
67-66-3 Chloroform 25 26.4 106 80-124
95-49-8 o-Chlorotoluene 25 28.0 112 81-127
106-43-4 p-Chlorotoluene 25 27.6 110 83-130
124-48-1 Dibromochloromethane 25 26.9 108 78-122
106-93-4 1,2-Dibromoethane 25 23.9 96 75-120
75-71-8 Dichlorodifluoromethane 25 27.0 108 42-167
95-50-1 1,2-Dichlorobenzene 25 25.1 100 82-124
541-73-1 1,3-Dichlorobenzene 25 26.7 107 84-125
106-46-7 1,4-Dichlorobenzene 25 26.0 104 78-120
75-34-3 1,1-Dichloroethane 25 28.4 114 81-122
107-06-2 1,2-Dichloroethane 25 24.4 98 75-125
75-35-4 1,1-Dichloroethylene 25 29.8 119 78-137
156-59-2 cis-1,2-Dichloroethylene 25 24.8 99 78-120
156-60-5 trans-1,2-Dichloroethylene 25 29.9 120 76-127
78-87-5 1,2-Dichloropropane 25 25.9 104 76-124
142-28-9 1,3-Dichloropropane 25 23.3 93 80-118
594-20-7 2,2-Dichloropropane 25 28.6 114 74-139
563-58-6 1,1-Dichloropropene 25 27.7 111 79-131
10061-01-5 cis-1,3-Dichloropropene 25 26.0 104 75-118
10061-02-6 trans-1,3-Dichloropropene 25 26.1 104 80-120
108-20-3 Di-Isopropyl Ether 25 25.2 101 68-123
64-17-5 Ethyl Alcohol 500 570 114 46-145
100-41-4 Ethylbenzene 25 27.3 109 81-121
* = Outside of Control Limits.
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Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VJ5276-BS J0976104.D 1 04/27/16 DP n/a n/a VJ5276
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-1, FA33365-3, FA33365-5, FA33365-8
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
591-78-6 2-Hexanone 125 118 94 61-129
98-82-8 Isopropylbenzene 25 27.6 110 83-132
99-87-6 p-Isopropyltoluene 25 28.0 112 79-130
74-83-9 Methyl Bromide 25 27.8 111 59-143
74-87-3 Methyl Chloride 25 28.9 116 50-159
75-09-2 Methylene Chloride 25 28.8 115 69-135
108-10-1 4-Methyl-2-pentanone (MIBK)125 113 90 66-122
1634-04-4 Methyl Tert Butyl Ether 25 24.5 98 72-117
91-20-3 Naphthalene 25 21.1 84 63-132
103-65-1 n-Propylbenzene 25 29.7 119 82-133
100-42-5 Styrene 25 23.8 95 78-119
630-20-6 1,1,1,2-Tetrachloroethane 25 27.2 109 77-122
79-34-5 1,1,2,2-Tetrachloroethane 25 24.2 97 72-120
127-18-4 Tetrachloroethylene 25 24.8 99 76-135
108-88-3 Toluene 25 25.3 101 80-120
87-61-6 1,2,3-Trichlorobenzene 25 23.0 92 68-131
120-82-1 1,2,4-Trichlorobenzene 25 24.0 96 73-129
71-55-6 1,1,1-Trichloroethane 25 27.5 110 75-130
79-00-5 1,1,2-Trichloroethane 25 24.8 99 76-119
79-01-6 Trichloroethylene 25 26.7 107 81-126
75-69-4 Trichlorofluoromethane 25 32.5 130 71-156
96-18-4 1,2,3-Trichloropropane 25 25.1 100 77-120
95-63-6 1,2,4-Trimethylbenzene 25 27.7 111 79-120
108-67-8 1,3,5-Trimethylbenzene 25 27.7 111 79-120
108-05-4 Vinyl Acetate 125 132 106 43-154
75-01-4 Vinyl Chloride 25 31.2 125 69-159
m,p-Xylene 50 51.6 103 79-126
95-47-6 o-Xylene 25 26.5 106 80-127
1330-20-7 Xylene (total)75 78.1 104 80-126
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 104%83-118%
17060-07-0 1,2-Dichloroethane-D4 100%79-125%
2037-26-5 Toluene-D8 97%85-112%
* = Outside of Control Limits.
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Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VJ5276-BS J0976104.D 1 04/27/16 DP n/a n/a VJ5276
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-1, FA33365-3, FA33365-5, FA33365-8
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 99%83-118%
* = Outside of Control Limits.
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Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2644-BS F0077024.D 1 04/28/16 EP n/a n/a VF2644
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-6
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 223 89 61-152
71-43-2 Benzene 50 52.2 104 76-126
108-86-1 Bromobenzene 50 50.7 101 76-122
74-97-5 Bromochloromethane 50 50.5 101 77-120
75-27-4 Bromodichloromethane 50 50.1 100 74-130
75-25-2 Bromoform 50 49.9 100 76-127
78-93-3 2-Butanone (MEK)250 257 103 75-137
104-51-8 n-Butylbenzene 50 46.6 93 71-128
135-98-8 sec-Butylbenzene 50 53.7 107 79-135
98-06-6 tert-Butylbenzene 50 50.6 101 77-133
56-23-5 Carbon Tetrachloride 50 53.4 107 78-133
108-90-7 Chlorobenzene 50 51.9 104 81-129
75-00-3 Chloroethane 50 41.2 82 68-133
67-66-3 Chloroform 50 51.1 102 72-123
95-49-8 o-Chlorotoluene 50 54.1 108 77-129
106-43-4 p-Chlorotoluene 50 51.6 103 80-134
124-48-1 Dibromochloromethane 50 47.3 95 76-127
106-93-4 1,2-Dibromoethane 50 48.5 97 77-126
75-71-8 Dichlorodifluoromethane 50 51.9 104 68-168
95-50-1 1,2-Dichlorobenzene 50 51.0 102 80-129
541-73-1 1,3-Dichlorobenzene 50 49.9 100 81-129
106-46-7 1,4-Dichlorobenzene 50 48.6 97 76-130
75-34-3 1,1-Dichloroethane 50 44.0 88 73-125
107-06-2 1,2-Dichloroethane 50 49.8 100 74-128
75-35-4 1,1-Dichloroethylene 50 50.0 100 81-136
156-59-2 cis-1,2-Dichloroethylene 50 51.4 103 74-126
156-60-5 trans-1,2-Dichloroethylene 50 50.7 101 70-127
78-87-5 1,2-Dichloropropane 50 50.1 100 74-125
142-28-9 1,3-Dichloropropane 50 49.7 99 76-122
594-20-7 2,2-Dichloropropane 50 52.9 106 77-133
563-58-6 1,1-Dichloropropene 50 51.1 102 75-130
10061-01-5 cis-1,3-Dichloropropene 50 52.1 104 80-123
10061-02-6 trans-1,3-Dichloropropene 50 51.8 104 75-131
108-20-3 Di-Isopropyl Ether 50 47.1 94 75-122
64-17-5 Ethyl Alcohol 1000 962 96 53-154
100-41-4 Ethylbenzene 50 53.5 107 77-123
* = Outside of Control Limits.
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Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2644-BS F0077024.D 1 04/28/16 EP n/a n/a VF2644
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-6
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
591-78-6 2-Hexanone 250 280 112 72-133
98-82-8 Isopropylbenzene 50 48.6 97 80-136
99-87-6 p-Isopropyltoluene 50 49.3 99 77-131
74-83-9 Methyl Bromide 50 53.4 107 65-139
74-87-3 Methyl Chloride 50 50.7 101 71-144
75-09-2 Methylene Chloride 50 46.4 93 74-137
108-10-1 4-Methyl-2-pentanone (MIBK)250 285 114 76-132
1634-04-4 Methyl Tert Butyl Ether 50 50.0 100 77-120
91-20-3 Naphthalene 50 50.4 101 79-129
103-65-1 n-Propylbenzene 50 50.0 100 80-135
100-42-5 Styrene 50 53.9 108 78-125
630-20-6 1,1,1,2-Tetrachloroethane 50 51.4 103 78-126
79-34-5 1,1,2,2-Tetrachloroethane 50 49.4 99 71-126
127-18-4 Tetrachloroethylene 50 47.0 94 79-130
108-88-3 Toluene 50 57.3 115 76-124
87-61-6 1,2,3-Trichlorobenzene 50 53.3 107 77-128
120-82-1 1,2,4-Trichlorobenzene 50 48.4 97 78-130
71-55-6 1,1,1-Trichloroethane 50 53.7 107 70-129
79-00-5 1,1,2-Trichloroethane 50 50.6 101 74-124
79-01-6 Trichloroethylene 50 49.1 98 75-128
75-69-4 Trichlorofluoromethane 50 51.5 103 73-145
96-18-4 1,2,3-Trichloropropane 50 52.0 104 74-127
95-63-6 1,2,4-Trimethylbenzene 50 49.4 99 74-123
108-67-8 1,3,5-Trimethylbenzene 50 50.1 100 73-122
108-05-4 Vinyl Acetate 250 261 104 48-164
75-01-4 Vinyl Chloride 50 50.7 101 76-141
m,p-Xylene 100 113 113 80-128
95-47-6 o-Xylene 50 48.4 97 80-132
1330-20-7 Xylene (total)150 162 108 80-129
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%75-124%
17060-07-0 1,2-Dichloroethane-D4 95%72-135%
2037-26-5 Toluene-D8 113%75-126%
* = Outside of Control Limits.
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Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2644-BS F0077024.D 1 04/28/16 EP n/a n/a VF2644
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-6
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 98%71-133%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA33363-5MS F0076976.D 1 04/26/16 EP n/a n/a VF2643
FA33363-5MSD F0076977.D 1 04/26/16 EP n/a n/a VF2643
FA33363-5 F0076970.D 1 04/26/16 EP n/a n/a VF2643
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-2, FA33365-4, FA33365-7
FA33363-5 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone 38.4 J 311 324 92 310 323 92 0 61-152/27
71-43-2 Benzene 5.1 U 62.2 58.1 93 62.1 56.0 90 4 76-126/26
108-86-1 Bromobenzene 5.1 U 62.2 63.0 101 62.1 59.2 95 6 76-122/32
74-97-5 Bromochloromethane 5.1 U 62.2 68.5 110 62.1 56.7 91 19 77-120/24
75-27-4 Bromodichloromethane 5.1 U 62.2 60.5 97 62.1 61.0 98 1 74-130/25
75-25-2 Bromoform 5.1 U 62.2 48.8 78 62.1 48.0 77 2 76-127/26
78-93-3 2-Butanone (MEK)26 U 311 293 94 310 293 94 0 75-137/25
104-51-8 n-Butylbenzene 5.1 U 62.2 58.6 94 62.1 49.9 80 16 71-128/35
135-98-8 sec-Butylbenzene 5.1 U 62.2 59.6 96 62.1 51.6 83 14 79-135/34
98-06-6 tert-Butylbenzene 5.1 U 62.2 61.3 99 62.1 54.8 88 11 77-133/34
56-23-5 Carbon Tetrachloride 5.1 U 62.2 53.2 86 62.1 51.5 83 3 78-133/29
108-90-7 Chlorobenzene 5.1 U 62.2 60.4 97 62.1 56.8 91 6 81-129/29
75-00-3 Chloroethane 5.1 U 62.2 54.0 87 62.1 52.5 85 3 68-133/29
67-66-3 Chloroform 5.1 U 62.2 66.7 107 62.1 60.0 97 11 72-123/26
95-49-8 o-Chlorotoluene 5.1 U 62.2 64.4 104 62.1 59.1 95 9 77-129/33
106-43-4 p-Chlorotoluene 5.1 U 62.2 64.0 103 62.1 59.7 96 7 80-134/33
124-48-1 Dibromochloromethane 5.1 U 62.2 56.5 91 62.1 56.7 91 0 76-127/27
106-93-4 1,2-Dibromoethane 5.1 U 62.2 57.0 92 62.1 54.9 88 4 77-126/26
75-71-8 Dichlorodifluoromethane 5.1 U 62.2 49.9 80 62.1 48.1 77 4 68-168/29
95-50-1 1,2-Dichlorobenzene 5.1 U 62.2 58.3 94 62.1 53.7 87 8 80-129/32
541-73-1 1,3-Dichlorobenzene 5.1 U 62.2 61.5 99 62.1 54.7 88 12 81-129/33
106-46-7 1,4-Dichlorobenzene 5.1 U 62.2 61.2 98 62.1 54.7 88 11 76-130/32
75-34-3 1,1-Dichloroethane 5.1 U 62.2 63.6 102 62.1 62.2 100 2 73-125/27
107-06-2 1,2-Dichloroethane 5.1 U 62.2 67.7 109 62.1 66.9 108 1 74-128/23
75-35-4 1,1-Dichloroethylene 5.1 U 62.2 60.6 97 62.1 59.0 95 3 81-136/28
156-59-2 cis-1,2-Dichloroethylene 5.1 U 62.2 65.0 104 62.1 53.8 87 19 74-126/26
156-60-5 trans-1,2-Dichloroethylene 5.1 U 62.2 64.6 104 62.1 62.2 100 4 70-127/27
78-87-5 1,2-Dichloropropane 5.1 U 62.2 59.7 96 62.1 58.6 94 2 74-125/25
142-28-9 1,3-Dichloropropane 5.1 U 62.2 56.3 90 62.1 55.8 90 1 76-122/26
594-20-7 2,2-Dichloropropane 5.1 U 62.2 64.8 104 62.1 55.7 90 15 77-133/28
563-58-6 1,1-Dichloropropene 5.1 U 62.2 57.5 92 62.1 55.2 89 4 75-130/28
10061-01-5 cis-1,3-Dichloropropene 5.1 U 62.2 60.9 98 62.1 59.2 95 3 80-123/26
10061-02-6 trans-1,3-Dichloropropene 5.1 U 62.2 63.3 102 62.1 61.3 99 3 75-131/28
108-20-3 Di-Isopropyl Ether 5.1 U 62.2 65.3 105 62.1 64.1 103 2 75-122/25
64-17-5 Ethyl Alcohol 410 U 1240 2420 194*1240 2020 163*18 53-154/42
100-41-4 Ethylbenzene 5.1 U 62.2 61.3 99 62.1 56.5 91 8 77-123/31
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA33363-5MS F0076976.D 1 04/26/16 EP n/a n/a VF2643
FA33363-5MSD F0076977.D 1 04/26/16 EP n/a n/a VF2643
FA33363-5 F0076970.D 1 04/26/16 EP n/a n/a VF2643
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-2, FA33365-4, FA33365-7
FA33363-5 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
591-78-6 2-Hexanone 26 U 311 268 86 310 278 90 4 72-133/26
98-82-8 Isopropylbenzene 5.1 U 62.2 57.0 92 62.1 50.4 81 12 80-136/32
99-87-6 p-Isopropyltoluene 5.1 U 62.2 59.9 96 62.1 52.4 84 13 77-131/34
74-83-9 Methyl Bromide 5.1 U 62.2 64.2 103 62.1 62.9 101 2 65-139/31
74-87-3 Methyl Chloride 5.1 U 62.2 59.2 95 62.1 59.0 95 0 71-144/27
75-09-2 Methylene Chloride 10 U 62.2 75.3 121 62.1 70.6 114 6 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK)26 U 311 291 94 310 296 95 2 76-132/26
1634-04-4 Methyl Tert Butyl Ether 5.1 U 62.2 65.2 105 62.1 64.2 103 2 77-120/24
91-20-3 Naphthalene 5.1 U 62.2 46.4 75*62.1 41.7 67*11 79-129/33
103-65-1 n-Propylbenzene 5.1 U 62.2 65.0 104 62.1 59.7 96 9 80-135/33
100-42-5 Styrene 5.1 U 62.2 55.1 89 62.1 50.3 81 9 78-125/30
630-20-6 1,1,1,2-Tetrachloroethane 5.1 U 62.2 60.7 98 62.1 58.2 94 4 78-126/27
79-34-5 1,1,2,2-Tetrachloroethane 5.1 U 62.2 60.3 97 62.1 60.7 98 1 71-126/30
127-18-4 Tetrachloroethylene 5.1 U 62.2 55.5 89 62.1 50.2 81 10 79-130/31
108-88-3 Toluene 5.1 U 62.2 57.8 93 62.1 55.0 89 5 76-124/30
87-61-6 1,2,3-Trichlorobenzene 5.1 U 62.2 46.3 74*62.1 37.7 61*20 77-128/35
120-82-1 1,2,4-Trichlorobenzene 5.1 U 62.2 49.7 80 62.1 41.2 66*19 78-130/34
71-55-6 1,1,1-Trichloroethane 5.1 U 62.2 56.7 91 62.1 56.5 91 0 70-129/27
79-00-5 1,1,2-Trichloroethane 5.1 U 62.2 59.4 95 62.1 58.2 94 2 74-124/28
79-01-6 Trichloroethylene 1.3 J 62.2 58.5 92 62.1 56.5 89 3 75-128/27
75-69-4 Trichlorofluoromethane 5.1 U 62.2 60.9 98 62.1 57.3 92 6 73-145/31
96-18-4 1,2,3-Trichloropropane 5.1 U 62.2 61.5 99 62.1 61.1 98 1 74-127/27
95-63-6 1,2,4-Trimethylbenzene 5.1 U 62.2 64.8 104 62.1 57.9 93 11 74-123/34
108-67-8 1,3,5-Trimethylbenzene 5.1 U 62.2 64.2 103 62.1 57.0 92 12 73-122/33
108-05-4 Vinyl Acetate 26 U 311 232 75 310 234 75 1 48-164/37
75-01-4 Vinyl Chloride 5.1 U 62.2 58.3 94 62.1 57.1 92 2 76-141/27
m,p-Xylene 10 U 124 120 96 124 110 89 9 80-128/30
95-47-6 o-Xylene 5.1 U 62.2 57.7 93 62.1 53.9 87 7 80-132/30
1330-20-7 Xylene (total)15 U 187 178 95 186 164 88 8 80-129/30
CAS No.Surrogate Recoveries MS MSD FA33363-5 Limits
1868-53-7 Dibromofluoromethane 104%102%102%75-124%
17060-07-0 1,2-Dichloroethane-D4 113%119%105%72-135%
2037-26-5 Toluene-D8 99%97%105%75-126%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA33363-5MS F0076976.D 1 04/26/16 EP n/a n/a VF2643
FA33363-5MSD F0076977.D 1 04/26/16 EP n/a n/a VF2643
FA33363-5 F0076970.D 1 04/26/16 EP n/a n/a VF2643
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-2, FA33365-4, FA33365-7
CAS No.Surrogate Recoveries MS MSD FA33363-5 Limits
460-00-4 4-Bromofluorobenzene 103%108%110%71-133%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA33336-10MS J0976125.D 5 04/27/16 DP n/a n/a VJ5276
FA33336-10MSD J0976126.D 5 04/27/16 DP n/a n/a VJ5276
FA33336-10 J0976113.D 5 04/27/16 DP n/a n/a VJ5276
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-1, FA33365-3, FA33365-5, FA33365-8
FA33336-10 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
67-64-1 Acetone ND 625 546 87 625 590 94 8 50-147/21
71-43-2 Benzene ND 125 135 108 125 134 107 1 81-122/14
108-86-1 Bromobenzene ND 125 133 106 125 134 107 1 80-121/14
74-97-5 Bromochloromethane ND 125 125 100 125 122 98 2 76-123/14
75-27-4 Bromodichloromethane ND 125 132 106 125 121 97 9 79-123/19
75-25-2 Bromoform ND 125 111 89 125 105 84 6 66-123/21
78-93-3 2-Butanone (MEK)ND 625 569 91 625 596 95 5 56-143/18
104-51-8 n-Butylbenzene ND 125 137 110 125 133 106 3 79-126/16
135-98-8 sec-Butylbenzene ND 125 147 118 125 141 113 4 83-133/16
98-06-6 tert-Butylbenzene ND 125 135 108 125 134 107 1 80-133/16
56-23-5 Carbon Tetrachloride ND 125 151 121 125 135 108 11 76-136/23
108-90-7 Chlorobenzene ND 125 132 106 125 130 104 2 82-124/14
75-00-3 Chloroethane ND 125 148 118 125 146 117 1 62-144/20
67-66-3 Chloroform ND 125 131 105 125 134 107 2 80-124/15
95-49-8 o-Chlorotoluene ND 125 141 113 125 138 110 2 81-127/15
106-43-4 p-Chlorotoluene ND 125 135 108 125 137 110 1 83-130/15
124-48-1 Dibromochloromethane ND 125 123 98 125 114 91 8 78-122/19
106-93-4 1,2-Dibromoethane ND 125 117 94 125 120 96 3 75-120/13
75-71-8 Dichlorodifluoromethane ND 125 119 95 125 115 92 3 42-167/19
95-50-1 1,2-Dichlorobenzene ND 125 125 100 125 125 100 0 82-124/14
541-73-1 1,3-Dichlorobenzene ND 125 134 107 125 132 106 2 84-125/14
106-46-7 1,4-Dichlorobenzene ND 125 128 102 125 127 102 1 78-120/15
75-34-3 1,1-Dichloroethane ND 125 136 109 125 139 111 2 81-122/15
107-06-2 1,2-Dichloroethane ND 125 121 97 125 121 97 0 75-125/14
75-35-4 1,1-Dichloroethylene ND 125 139 111 125 145 116 4 78-137/18
156-59-2 cis-1,2-Dichloroethylene ND 125 120 96 125 120 96 0 78-120/15
156-60-5 trans-1,2-Dichloroethylene ND 125 144 115 125 146 117 1 76-127/17
78-87-5 1,2-Dichloropropane ND 125 124 99 125 126 101 2 76-124/14
142-28-9 1,3-Dichloropropane ND 125 114 91 125 115 92 1 80-118/13
594-20-7 2,2-Dichloropropane ND 125 121 97 125 120 96 1 74-139/17
563-58-6 1,1-Dichloropropene ND 125 135 108 125 132 106 2 79-131/16
10061-01-5 cis-1,3-Dichloropropene ND 125 113 90 125 105 84 7 75-118/23
10061-02-6 trans-1,3-Dichloropropene ND 125 120 96 125 112 90 7 80-120/22
108-20-3 Di-Isopropyl Ether 3.3 J 125 123 96 125 128 100 4 68-123/16
64-17-5 Ethyl Alcohol ND 2500 2830 113 2500 3060 122 8 46-145/30
100-41-4 Ethylbenzene ND 125 136 109 125 134 107 1 81-121/14
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA33336-10MS J0976125.D 5 04/27/16 DP n/a n/a VJ5276
FA33336-10MSD J0976126.D 5 04/27/16 DP n/a n/a VJ5276
FA33336-10 J0976113.D 5 04/27/16 DP n/a n/a VJ5276
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-1, FA33365-3, FA33365-5, FA33365-8
FA33336-10 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
591-78-6 2-Hexanone ND 625 579 93 625 620 99 7 61-129/18
98-82-8 Isopropylbenzene ND 125 136 109 125 136 109 0 83-132/15
99-87-6 p-Isopropyltoluene ND 125 139 111 125 137 110 1 79-130/16
74-83-9 Methyl Bromide ND 125 127 102 125 123 98 3 59-143/19
74-87-3 Methyl Chloride ND 125 132 106 125 132 106 0 50-159/19
75-09-2 Methylene Chloride 12.1 J 125 134 98 125 135 98 1 69-135/16
108-10-1 4-Methyl-2-pentanone (MIBK)ND 625 566 91 625 603 96 6 66-122/16
1634-04-4 Methyl Tert Butyl Ether 299 125 424 100 125 446 118* a 5 72-117/14
91-20-3 Naphthalene ND 125 99.6 80 125 105 84 5 63-132/25
103-65-1 n-Propylbenzene ND 125 149 119 125 147 118 1 82-133/15
100-42-5 Styrene ND 125 117 94 125 114 91 3 78-119/23
630-20-6 1,1,1,2-Tetrachloroethane ND 125 132 106 125 127 102 4 77-122/19
79-34-5 1,1,2,2-Tetrachloroethane ND 125 123 98 125 125 100 2 72-120/14
127-18-4 Tetrachloroethylene ND 125 124 99 125 120 96 3 76-135/16
108-88-3 Toluene ND 125 129 103 125 128 102 1 80-120/14
87-61-6 1,2,3-Trichlorobenzene ND 125 108 86 125 112 90 4 68-131/25
120-82-1 1,2,4-Trichlorobenzene ND 125 113 90 125 117 94 3 73-129/20
71-55-6 1,1,1-Trichloroethane ND 125 132 106 125 130 104 2 75-130/16
79-00-5 1,1,2-Trichloroethane ND 125 123 98 125 125 100 2 76-119/14
79-01-6 Trichloroethylene ND 125 136 109 125 139 111 2 81-126/15
75-69-4 Trichlorofluoromethane ND 125 153 122 125 147 118 4 71-156/21
96-18-4 1,2,3-Trichloropropane ND 125 131 105 125 133 106 2 77-120/16
95-63-6 1,2,4-Trimethylbenzene ND 125 138 110 125 137 110 1 79-120/18
108-67-8 1,3,5-Trimethylbenzene ND 125 139 111 125 136 109 2 79-120/19
108-05-4 Vinyl Acetate ND 625 595 95 625 611 98 3 43-154/14
75-01-4 Vinyl Chloride ND 125 140 112 125 137 110 2 69-159/18
m,p-Xylene ND 250 257 103 250 251 100 2 79-126/15
95-47-6 o-Xylene ND 125 128 102 125 129 103 1 80-127/14
1330-20-7 Xylene (total)ND 375 386 103 375 380 101 2 80-126/15
CAS No.Surrogate Recoveries MS MSD FA33336-10 Limits
1868-53-7 Dibromofluoromethane 101%103%100%83-118%
17060-07-0 1,2-Dichloroethane-D4 102%102%101%79-125%
2037-26-5 Toluene-D8 97%97%103%85-112%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA33336-10MS J0976125.D 5 04/27/16 DP n/a n/a VJ5276
FA33336-10MSD J0976126.D 5 04/27/16 DP n/a n/a VJ5276
FA33336-10 J0976113.D 5 04/27/16 DP n/a n/a VJ5276
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-1, FA33365-3, FA33365-5, FA33365-8
CAS No.Surrogate Recoveries MS MSD FA33336-10 Limits
460-00-4 4-Bromofluorobenzene 99%102%102%83-118%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA33409-3MS F0077038.D 1 04/28/16 EP n/a n/a VF2644
FA33409-3MSD F0077039.D 1 04/28/16 EP n/a n/a VF2644
FA33409-3 F0077027.D 1 04/28/16 EP n/a n/a VF2644
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-6
FA33409-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone 40.4 300 201 54*304 212 56*5 61-152/27
71-43-2 Benzene ND 60 50.6 84 60.8 57.0 94 12 76-126/26
108-86-1 Bromobenzene ND 60 46.9 78 60.8 54.6 90 15 76-122/32
74-97-5 Bromochloromethane ND 60 47.6 79 60.8 53.5 88 12 77-120/24
75-27-4 Bromodichloromethane ND 60 51.6 86 60.8 59.1 97 14 74-130/25
75-25-2 Bromoform ND 60 47.0 78 60.8 53.0 87 12 76-127/26
78-93-3 2-Butanone (MEK)ND 300 252 84 304 260 86 3 75-137/25
104-51-8 n-Butylbenzene 9.4 60 56.7 79 60.8 74.9 108 28 71-128/35
135-98-8 sec-Butylbenzene 5.8 60 55.5 83 60.8 70.4 106 24 79-135/34
98-06-6 tert-Butylbenzene ND 60 47.5 79 60.8 57.7 95 19 77-133/34
56-23-5 Carbon Tetrachloride ND 60 53.2 89 60.8 59.1 97 11 78-133/29
108-90-7 Chlorobenzene ND 60 50.1 84 60.8 57.7 95 14 81-129/29
75-00-3 Chloroethane ND 60 33.0 55*60.8 39.0 64*17 68-133/29
67-66-3 Chloroform ND 60 49.8 83 60.8 57.2 94 14 72-123/26
95-49-8 o-Chlorotoluene ND 60 51.8 86 60.8 60.5 100 15 77-129/33
106-43-4 p-Chlorotoluene ND 60 52.2 87 60.8 63.0 104 19 80-134/33
124-48-1 Dibromochloromethane ND 60 44.8 75*60.8 51.4 85 14 76-127/27
106-93-4 1,2-Dibromoethane ND 60 46.7 78 60.8 54.5 90 15 77-126/26
75-71-8 Dichlorodifluoromethane ND 60 50.3 84 60.8 56.7 93 12 68-168/29
95-50-1 1,2-Dichlorobenzene ND 60 51.6 86 60.8 60.6 100 16 80-129/32
541-73-1 1,3-Dichlorobenzene ND 60 51.5 86 60.8 60.1 99 15 81-129/33
106-46-7 1,4-Dichlorobenzene ND 60 49.7 83 60.8 57.0 94 14 76-130/32
75-34-3 1,1-Dichloroethane ND 60 43.4 72*60.8 48.9 80 12 73-125/27
107-06-2 1,2-Dichloroethane ND 60 49.3 82 60.8 53.6 88 8 74-128/23
75-35-4 1,1-Dichloroethylene 0.95 J 60 50.8 83 60.8 56.6 92 11 81-136/28
156-59-2 cis-1,2-Dichloroethylene ND 60 47.1 79 60.8 56.3 93 18 74-126/26
156-60-5 trans-1,2-Dichloroethylene ND 60 53.7 90 60.8 60.1 99 11 70-127/27
78-87-5 1,2-Dichloropropane ND 60 49.7 83 60.8 56.1 92 12 74-125/25
142-28-9 1,3-Dichloropropane ND 60 44.5 74*60.8 53.2 88 18 76-122/26
594-20-7 2,2-Dichloropropane ND 60 47.2 79 60.8 58.7 97 22 77-133/28
563-58-6 1,1-Dichloropropene ND 60 51.0 85 60.8 60.1 99 16 75-130/28
10061-01-5 cis-1,3-Dichloropropene ND 60 49.4 82 60.8 50.8 84 3 80-123/26
10061-02-6 trans-1,3-Dichloropropene ND 60 56.2 94 60.8 58.5 96 4 75-131/28
108-20-3 Di-Isopropyl Ether ND 60 42.2 70*60.8 51.6 85 20 75-122/25
64-17-5 Ethyl Alcohol ND 1200 1170 98 1220 1390 114 17 53-154/42
100-41-4 Ethylbenzene 23.0 60 53.2 50*60.8 64.0 67*18 77-123/31
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA33409-3MS F0077038.D 1 04/28/16 EP n/a n/a VF2644
FA33409-3MSD F0077039.D 1 04/28/16 EP n/a n/a VF2644
FA33409-3 F0077027.D 1 04/28/16 EP n/a n/a VF2644
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-6
FA33409-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
591-78-6 2-Hexanone ND 300 272 91 304 313 103 14 72-133/26
98-82-8 Isopropylbenzene 10.6 60 51.4 68*60.8 66.1 91 25 80-136/32
99-87-6 p-Isopropyltoluene 1.2 J 60 49.0 80 60.8 59.9 97 20 77-131/34
74-83-9 Methyl Bromide ND 60 49.8 83 60.8 63.2 104 24 65-139/31
74-87-3 Methyl Chloride ND 60 49.3 82 60.8 56.4 93 13 71-144/27
75-09-2 Methylene Chloride ND 60 47.1 79 60.8 52.3 86 10 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK)ND 300 275 92 304 275 90 0 76-132/26
1634-04-4 Methyl Tert Butyl Ether ND 60 45.3 76*60.8 54.9 90 19 77-120/24
91-20-3 Naphthalene 18.3 60 77.5 99 60.8 91.7 121 17 79-129/33
103-65-1 n-Propylbenzene 44.7 60 59.3 24*60.8 85.8 68*37*80-135/33
100-42-5 Styrene ND 60 51.3 86 60.8 61.4 101 18 78-125/30
630-20-6 1,1,1,2-Tetrachloroethane ND 60 48.0 80 60.8 56.5 93 16 78-126/27
79-34-5 1,1,2,2-Tetrachloroethane ND 60 45.1 75 60.8 49.6 82 10 71-126/30
127-18-4 Tetrachloroethylene ND 60 83.0 138*60.8 79.1 130 5 79-130/31
108-88-3 Toluene 2.8 60 54.8 87 60.8 53.0 83 3 76-124/30
87-61-6 1,2,3-Trichlorobenzene ND 60 60.9 102 60.8 63.6 105 4 77-128/35
120-82-1 1,2,4-Trichlorobenzene ND 60 61.1 102 60.8 67.3 111 10 78-130/34
71-55-6 1,1,1-Trichloroethane ND 60 48.4 81 60.8 55.4 91 13 70-129/27
79-00-5 1,1,2-Trichloroethane ND 60 48.4 81 60.8 54.1 89 11 74-124/28
79-01-6 Trichloroethylene ND 60 53.2 89 60.8 61.2 101 14 75-128/27
75-69-4 Trichlorofluoromethane ND 60 50.8 85 60.8 57.8 95 13 73-145/31
96-18-4 1,2,3-Trichloropropane ND 60 46.8 78 60.8 54.5 90 15 74-127/27
95-63-6 1,2,4-Trimethylbenzene ND 60 47.1 79 60.8 56.1 92 17 74-123/34
108-67-8 1,3,5-Trimethylbenzene ND 60 45.9 77 60.8 55.7 92 19 73-122/33
108-05-4 Vinyl Acetate ND 300 146 49 304 159 52 9 48-164/37
75-01-4 Vinyl Chloride ND 60 50.6 84 60.8 57.0 94 12 76-141/27
m,p-Xylene 1.2 J 120 110 91 122 129 105 16 80-128/30
95-47-6 o-Xylene ND 60 46.4 77*60.8 61.0 100 27 80-132/30
1330-20-7 Xylene (total)ND 180 157 87 182 190 104 19 80-129/30
CAS No.Surrogate Recoveries MS MSD FA33409-3 Limits
1868-53-7 Dibromofluoromethane 103%100%100%75-124%
17060-07-0 1,2-Dichloroethane-D4 103%98%110%72-135%
2037-26-5 Toluene-D8 106%89%86%75-126%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA33365
Account:RENCM Resolve Environmental
Project:Yonkers Rd, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA33409-3MS F0077038.D 1 04/28/16 EP n/a n/a VF2644
FA33409-3MSD F0077039.D 1 04/28/16 EP n/a n/a VF2644
FA33409-3 F0077027.D 1 04/28/16 EP n/a n/a VF2644
The QC reported here applies to the following samples:Method: SW846 8260B
FA33365-6
CAS No.Surrogate Recoveries MS MSD FA33409-3 Limits
460-00-4 4-Bromofluorobenzene 98%106%110%71-133%
* = Outside of Control Limits.
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