Phase II ESA Freightliner - Hart & Hickman 7-14-16

ATTORNEY-CLIENT PRIVILEGED

Via E-mail

July 14, 2016

Howard, Stallings, From, Hutson, Atkins, Angell & Davis, P.A.
5410 Trinity Rd., Suite 210
Raleigh, NC 27607

Attn: Mr. Nicholas Brown

Re: Phase II Environmental Site Assessment Report
Carolina Freightliner of Raleigh Site
3500 Yonkers Road
Raleigh, NC 27604
H&H Project No. TPP.001

Dear Nick:

Hart & Hickman, PC (H&H) is pleased to provide this Phase II Environmental Site Assessment
Report for the Carolina Freightliner of Raleigh site (the Site) at 3500 Yonkers Road in Raleigh,
North Carolina (Figure 1). The general site layout that illustrates current and historic uses and
locations of potential contaminant source areas such as the former paint spray booth, current
wash rack, floor drains, etc., is presented on Figure 2. The completed scope of work was based
upon our meeting on June 2, 2016 and our review of the historical documents.

Tri-Point Properties, LLC is selling the Site to Carolina Freightliner of Raleigh, LLC. As part of
that transaction a Phase I Environmental Site Assessment (ESA) and a limited Phase II ESA
were completed by others in February and May 2016, respectively. Results of the Phase II ESA
indicated that groundwater at one location (GP-4) contained tetrachloroethylene (PCE),
trichloroethylene (TCE) and cis-1,2-dichloroethylene (1,2-DCE) at concentrations above their
applicable North Carolina groundwater standards (2L Standards). GP-4 was located near the
southwestern property boundary, where parking lot runoff flows and generally downgradient of
Mr. Nicholas Brown
July 14, 2016
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the truck repair facilities. Based upon this information, it was agreed in our meeting that
additional limited soil and groundwater assessment should be conducted to aid in determining
the source and extent of the contamination. This letter report outlines the work completed and
the results of this assessment.

Phase II ESA Field Activities

Based upon the historical information, the results of the April 2016 Phase II ESA, and our
discussions regarding specific site use, the following additional assessment activities were
completed on June 20 – 22, 2016:

 On June 20, 2016 a private utility locator marked underground utilities in the areas of the
proposed borings. Additionally, 811 was called so the major utility companies could
mark their utilities in the area.

 On June 21, 2016 an H&H field staff oversaw and directed Regional Probing (a North
Carolina certified drilling contractor) to advance 5 soil borings to the water table at
locations illustrated on Figure 3. The boring locations were selected to target potential
source areas (paint booth {GP-7} and wash rack {GP-8}), the area between GP-4 and the
building/potential source areas (GP-5 and GP-6), and upgradient of the building (GP-9)
to aid in determining if contamination may be coming from an offsite source. The
borings were advanced using Direct Push Technology (DPT) which limits the amount of
investigation derived waste, such as soil cuttings and water.

 As the borings were advanced, the soil was screened in the field for obvious soil
contamination using a photo-ionization detector (PID) plus visual and olfactory
observations. The soil was also logged to determine the soil type and general moisture
content. Boring logs are included in Appendix A.
Mr. Nicholas Brown
July 14, 2016
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 Based upon field observations, two soil samples (0-1’ below land surface {bls} and 4-5’
bls) were collected from borings GP-7 and GP-8 and submitted to Test America Labs (a
NC-Certified Laboratory) for analysis of Volatile Organic Compounds (VOCs) using
EPA Method 8260. This analysis was used because it detects the previously identified
VOCs. No other soil samples were collected for laboratory analysis because there were
no field observations that indicated contamination in the other borings.

 Soil cuttings generated from installation of borings GP-7 and GP-8 were containerized in
a 55-gallon drum and staged onsite pending receipt of analytical data. Because no
contamination was noted in the other borings, and because they were not located in
potential source areas the soil from borings GP-5, GP-6 and GP-9 was spread on the
unpaved ground at the rear of the facility. Upon receipt of the analytical data which
indicated no detectable contamination in the drummed soil, it was spread onsite.

 A one-inch diameter PVC temporary monitoring well with 10 feet of screen was installed
in each boring to allow collection of a groundwater sample. Well construction details are
provided on Table 1 and in Appendix A.

 The wells were developed to remove suspended fine soil particles and to allow collection
of representative samples by removing groundwater using a peristaltic pump. The purge
water was containerized in DOT-approved 5-gallon buckets with lids and staged onsite
for proper disposal after receipt of analytical data. Because the analytical data indicated
the presence of contamination in the groundwater, the purge water will be disposed
offsite at a properly permitted facility.

 The wells were surveyed for relative elevations by H&H personnel and located laterally
by taking measurements from permanent structures. The relative elevations are provided
on Table 1.
Mr. Nicholas Brown
July 14, 2016
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 The wells were sampled on June 22, 2016. Prior to sampling, depth-to-water
measurements were collected from each temporary well to aid in determining the
generalized groundwater flow direction (Figure 4). Each well was purged and sampled
using a peristaltic pump with new dedicated polyethylene tubing. The samples were
placed into properly preserved, laboratory-provided 40 ml glass vials, placed in iced
coolers and submitted to Test American Labs under standard chain-of-custody protocols.

 On June 22, 2016, upon completion of fieldwork, the wells were abandoned in place by
filling with grout and patched at land surface to match the surrounding area (asphalt or
concrete).

Results of Assessment

The primary purpose of the Phase II Assessment was to determine if the VOCs detected in
groundwater during the May 2016 Phase II was an anomaly, or if the site is indeed impacted as a
result of historic site activities or as a result of an off-site source. This section provides a
discussion of the results. The laboratory analytical data is included in Appendix B. A summary
of the groundwater analytical data is provided on Table 2.

Site Hydrogeological Findings
Five boreholes were advanced to depths varying from approximately 27 ft bls to 32 ft bls. Based
upon the data from these borings, the site is generally underlain with saprolitic soil consisting of
silty clay and clayey silt coarsening downward to a sandy silt and silty sand. Depth to
groundwater varies from approximately 24 ft bls at GP-9, located near Yonkers Road to
approximately 30 ft bls at GP-7, located beneath the former paint spray booth. Groundwater
flow direction is to the southwest toward Crabtree Creek (Figure 4). The lateral hydraulic
gradient at the time of data collection was 0.022 ft/ft.
Mr. Nicholas Brown
July 14, 2016
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Soil Sampling Results
No obvious contamination was noted in any of the five soil borings advanced at the site.
Based upon slightly elevated PID readings, soil samples were collected at depths of 0-1 ft bls
and 4-5 ft bls from borings GP-7 and GP-8, which were located at the former paint spray booth
and current wash rack, respectively. None of the four samples submitted for laboratory
analysis contained detectable concentrations of VOCs using EPA Method 8260.

Groundwater Sampling Results
The five temporary groundwater monitoring wells, designated GP-5 to GP-9, were sampled on
June 22, 2016. The samples were submitted for analysis of VOCs using EPA Method 8260. A
summary of the groundwater analytical data is presented in Table 2 and illustrated on Figure 5.

PCE, TCE and 1,2-DCE were detected in all of the wells except GP-9, which was located in
a hydraulically upgradient position near Yonkers Road. PCE was detected above its 2L
Groundwater Standard in wells GP-5 through GP-8. TCE was detected above its 2L
Standard in wells GP-6 through GP-8. 1,2-DCE was not detected above its 2L Standard in
any of the wells.

The groundwater analytical results were also compared to the current Division of Waste
Management (DWM) Residential and Non-Residential Vapor Intrusion Screening Levels.
Although both PCE and TCE exceeded their Residential Screening Levels at several wells,
none of the samples exceeded the current Non-Residential Vapor Intrusion Screening
Levels, which are applicable to the site.

Mr. Nicholas Brown
July 14, 2016
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Discussion and Summary

The VOC constituents detected in groundwater at the Site are chlorinated solvents, which were
historically used by various industries for cleaning machinery, metal parts, dry cleaning of
clothes, etc. PCE is considered the parent compound and it typically degrades over time to TCE
and then to 1,2-DCE. However, many solvents used in the automobile industry used TCE as the
primary constituent. The presence of relatively low concentrations of these CVOCs in
groundwater at the site, and the lack of CVOCs in the upgradient well, suggests there has been a
historic release or releases at the Site. The source of the release(s) has not been determined at
this point and neither has the vertical or lateral extent of the associated groundwater plume.
Additional assessment will be necessary to determine the source(s) and the extent of the
impacts. Potential source areas include the floor drains, wash rack, former paint spray booth,
former parts washer locations and possible small surface releases. Once these have been
determined and the plume delineated, possible remedial action strategies can be evaluated
and implemented.

We appreciate the opportunity to assist with this project. Should you have any questions, please
do not hesitate to call us at [phone].

Sincerely,
Hart & Hickman, PC

Leonard Moretz, PG Joseph E. Starr, PE
Senior Consultant Senior Consultant

Attachments

TABLES
Table 1
Summary of Monitoring Well Details and Ground Water Elevations
Carolina Freightliner
Raleigh, North Carolina
H&H Job No. TPP-001
S:\AAA-Master Projects\Tri-Point Land LLC - TPP\Carolina Freightliner of Raleigh\Tables\Tables June 2016 Table 1 (Page 1 of 1)
Hart & Hickman, PC
Well Screen Well TOC Depth to Ground Water
Monitoring Date Date Depth Interval Elevation Water Elevation
Well ID Installed Abandoned (ft - bgs)(ft - bgs)(ft)(ft)(ft)
GP-5 6/21/2016 6/22/2016 28.35 18.35-28.35 92.10 25.44 66.66
GP-6 6/21/2016 6/22/2016 28.52 18.52-28.52 93.54 27.12 66.42
GP-7 6/21/2016 6/22/2016 31.25 21.25-31.25 100.00 30.08 69.92
GP-8 6/21/2016 6/22/2016 32.40 22.40-32.40 101.04 28.83 72.21
GP-9 6/21/2016 6/22/2016 27.81 17.81-27.81 100.28 23.76 76.52
Notes:
TOC = Top of Casing
TOC elevations are relative to GP-7; GP-7 TOC elevation was set to 100 ft for surveying purposes
BGS = Below Ground Surface
NA = Information not available
June 22, 2016
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Table 2 (Page 1 of 1)Hart & Hickman, PC

FIGURES
SITE
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
RALEIGH EAST, NC 2002
TITLE
PROJECT
SITE LOCATION MAP
CAROLINA FREIGHTLINER
3500 YONKERS ROAD
RALEIGH, NC
DATE:
JOB NO:
REVISION NO:
FIGURE:
6-27-16 0
1TPP-001
3334 Hillsborough Street
Raleigh, NC 27607919.847.4241(p) 919.847.4261 (f)
JOB NO. TPP.001
REVISION NO. 0DATE: 06-27-16
FIGURE NO. 2
SITE LAYOUT
TRI-POINT PROPERTIES/CAROLINA FREIGHTLINER
3500 YONKERS ROAD
RALEIGH, NORTH CAROLINA
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
License # C-1269 / #C-245 Geology
ADDITIONAL
SHOP
TRUCK
REPAIR
MAIN
SHOP
PARTS STORAGE
(FORMER DIESEL SHOP)
NEW PARTS
STORAGE &
LIGHT TRUCK
REPAIRS
PARTS
STORAGE
FORMER
PAINT SPRAY
BOOTH
SERVICE
DEPT. OFFICE
COMPRESSOR SHED
& ASTs
SURFACE
DRAINAGE
OFFICES
& ADMIN.
WASH
RACK
Y
O
N
K
E
R
S

R
O
A
D
OIL/WATER
SEPARATORS
FLOOR
DRAINS
JOB NO. TPP.001
REVISION NO. 0DATE: 06-27-16
FIGURE NO. 3
BORING LOCATIONS
LEGEND
GEOPROBE BORING LOCATION
GP-9
GP-8
GP-7
GP-5
GP-6
TRI-POINT PROPERTIES/CAROLINA FREIGHTLINER
3500 YONKERS ROAD
RALEIGH, NORTH CAROLINA
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
License # C-1269 / #C-245 Geology
JOB NO. TPP.001
REVISION NO. 0DATE: 06-27-16
FIGURE NO. 4
TRI-POINT PROPERTIES/CAROLINA FREIGHTLINER
3500 YONKERS ROAD
RALEIGH, NORTH CAROLINA
GENERALIZED GROUNDWATER
FLOW DIRECTION
LEGEND
GEOPROBE BORING LOCATION
GROUNDWATER ELEVATION CONTOUR (ft.)
GROUNDWATER ELEVATION (ft.)
INFERRED GROUNDWATER FLOW DIRECTION
73
(72.21)
GP-7
(69.92)
GP-5
(66.66)
GP-6
(66.42)
GP-8
(72.21)
GP-9
(76.52)
67
68
69
70
71
72
73
74
75
76
76
75
74
73
7271
70
69
68
67
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
License # C-1269 / #C-245 Geology
JOB NO. TPP.001
REVISION NO. 0DATE: 06-27-16
FIGURE NO. 5
CVOC'S IN GROUNDWATER
LEGEND
GEOPROBE BORING LOCATION
NON DETECT
CONCENTRATION IN ug/L (ppb)
GP-9
GP-8
GP-7
GP-5
GP-6
TRI-POINT PROPERTIES/CAROLINA FREIGHTLINER
3500 YONKERS ROAD
RALEIGH, NORTH CAROLINA
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
License # C-1269 / #C-245 Geology
GP-8
1,2 DCE 31.4
PCE 12.0
TCE 4.09
GP-7
1,2 DCE 13.4
PCE 19.8
TCE 4.27
GP-5
1,2 DCE 8.73
PCE 10.7
TCE 2.26
GP-9 (ND)
GP-6
1,2 DCE 28
PCE 12.6
TCE 3.05
ND
28

APPENDIX A

BORING LOGS AND WELL CONSTRUCTION DETAILS
Asphalt
Dry, medium, red, clayey SILT
Dry, medium, red w/ many rocks, SILT
Dry, weak, redish orange w/ many rocks, sandy SILT
Dry, weak, orangish brown, sandy SILT
Moist, weak, tan, sandy SILT
Moist, weak, grey, sandy SILT
Moist, weak, tan, sandy SILT
Moist, medium, light brown, sandy CLAY
Moist, medium, brown, clayey SILT
Bottom of borehole at 28.4 feet.
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
BentoniteSeal1" Dia Sch.
40 Riser
Sand
1" Dia Sch.40 PVE0.010" SlotScreen
DRAWN BY:JAO
BORING COMPLETED:6/21/16
DRILLING CONTRACTOR:Regional Probing Remarks:
DRILL RIG/ METHOD:Geoprobe 5410 / HA/DPT
SAMPLING METHOD:Hand Auger/ Macro-Core Groundwater sample collected.
BORING STARTED:6/21/16
LOGGED BY:JAO
TOTAL DEPTH: 28.4 ft.
TOP OF CASING ELEV: 92.1 ft.
DEPTH TO WATER:
DE
P
T
H
(f
t
)
DE
P
T
H
(f
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)
LI
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MATERIAL DESCRIPTION
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(
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)
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SA
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.
BORING DIAGRAM
Sheet 1 of 1
BORING NUMBER GP-5
PROJECT:Carolina Freightliner
JOB NUMBER:TPP-001
LOCATION:Raleigh, Wake County, NC
BO
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-

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-
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0
1
.
G
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J
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
20
25
30
0
5
10
15
20
25
30
Asphalt
Dry, medium, red, silty CLAY
Dry, weak, red w/ many rocks, sandy SILT
Dry, medium, red w/ orange moltting, clayey SILT
Dry, weak, red w/ orange moltting, sandy SILT
Dry, weak, tan, SAND
Moist, weak, brown, silty SAND
Moist, weak, brown w/ mica, sandy SILT
Moist, medium, orangish brown w/ mica, sandy SILT
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
4.5
5.7
2.1
1.6
0
3.5
3.9
6.5
4.7
Bentonite
Seal1" Dia Sch.40 Riser
Sand1" Dia Sch.40 PVE0.010" SlotScreen
DRAWN BY:JAO
BORING COMPLETED:6/21/16
DRILLING CONTRACTOR:Regional Probing Remarks:
DRILL RIG/ METHOD:Geoprobe 5410 / HA/DPT
SAMPLING METHOD:Hand Auger/ Macro-Core Groundwater sample collected.
BORING STARTED:6/21/16
LOGGED BY:JAO
TOTAL DEPTH: 31.3 ft.
TOP OF CASING ELEV: 93.54 ft.
DEPTH TO WATER:
(Continued Next Page)
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MATERIAL DESCRIPTION
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BORING DIAGRAM
Sheet 1 of 2
BORING NUMBER GP-6
PROJECT:Carolina Freightliner
JOB NUMBER:TPP-001
LOCATION:Raleigh, Wake County, NC
BO
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2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
20
25
30
0
5
10
15
20
25
30
Bottom of borehole at 31.3 feet.
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MATERIAL DESCRIPTION
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BORING DIAGRAM
Sheet 2 of 2
BORING NUMBER GP-6
PROJECT:Carolina Freightliner
JOB NUMBER:TPP-001
LOCATION:Raleigh, Wake County, NC
BO
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0
1
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2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
30
35
40
45
50
55
60
30
35
40
45
50
55
60
Concrete
Dry, medium, red w/ orange mottling, CLAY
Dry, medium, red, silty CLAY
Dry, weak, orangish brown, sandy SILT
Dry, medium, red, silty CLAY
Moist, medium, tan, sandy SILT
Moist, medium, dark brown shinny w/ black mottling, mica, SILT
Moist, medium, grey shinny w/ mica, SILT
Moist, weak, brown w/ mica, silty SAND
Moist, weak, brown shinny w/ black mottling and mica, silty SAND
Bottom of borehole at 31.3 feet.
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
5.4
7.6
6.9
3.8
4.5
2.9
6.2
2.8
9.9
7.2
6.4
6.1
7.4
5.3
5
Bentonite
Seal1" Dia Sch.40 Riser
Sand1" Dia Sch.40 PVE
0.010" SlotScreen
DRAWN BY:JAO
BORING COMPLETED:6/21/16
DRILLING CONTRACTOR:Regional Probing Remarks:
DRILL RIG/ METHOD:Geoprobe 5410 / HA/DPT
SAMPLING METHOD:Hand Auger/ Macro-Core Soil sample collected 0-1' interval, and4-5' interval. Groundwater samplecollected.
BORING STARTED:6/21/16
LOGGED BY:JAO
TOTAL DEPTH: 31.3 ft.
TOP OF CASING ELEV: 100 ft.
DEPTH TO WATER:
DE
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(f
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)
DE
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(f
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LI
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MATERIAL DESCRIPTION
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BORING DIAGRAM
Sheet 1 of 1
BORING NUMBER GP-7
PROJECT:Carolina Freightliner
JOB NUMBER:TPP-001
LOCATION:Raleigh, Wake County, NC
BO
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0
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2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
20
25
30
0
5
10
15
20
25
30
Concrete
Dry, medium, red w/ orange mottling, CLAY
Dry, firm, red w/ light orange mottling, CLAY
Dry, medium, red, clayey SILT
Dry, medium, red, silty CLAY
Moist, medium, red, sandy SILT
Moist, weak, orangish brown w/ rocks, sandy SILT
Moist, weak, grey w/ white feldspar and mica, sandy SILT
Moist, weak, pinkish white w/ feldspar, sandy SILT
Moist, weak, pinkish white w/ light grey and feldspar, sandy CLAY
Bottom of borehole at 32.4 feet.
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
5.8
6.1
6.9
3.8
3.1
6.3
5.8
7.5
8.2
11.8
5.2
9.3
5.8
7.1
5.8
Bentonite
Seal1" Dia Sch.
40 Riser
Sand1" Dia Sch.40 PVE
0.010" SlotScreen
DRAWN BY:JAO
BORING COMPLETED:6/21/16
DRILLING CONTRACTOR:Regional Probing Remarks:
DRILL RIG/ METHOD:Geoprobe 5410 / HA/DPT
SAMPLING METHOD:Hand Auger/ Macro-Core Soil sample collected 0-1' interval, and4-5' interval. Groundwater samplecollected.
BORING STARTED:6/21/16
LOGGED BY:JAO
TOTAL DEPTH: 32.4 ft.
TOP OF CASING ELEV: 101.04 ft.
DEPTH TO WATER:
DE
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(f
t
)
DE
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)
LI
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MATERIAL DESCRIPTION
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BORING DIAGRAM
Sheet 1 of 1
BORING NUMBER GP-8
PROJECT:Carolina Freightliner
JOB NUMBER:TPP-001
LOCATION:Raleigh, Wake County, NC
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2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
20
25
30
0
5
10
15
20
25
30
Asphalt
Dry, medium, brownish red, clayey SILT
Dry, weak, orangish brown, sandy SILT
Dry, medium, light tan w/ red common rocks, silty CLAY
Dry, medium, orangish brown, silty CLAY
Moist, medium, orangish red w. common rocks, clayey SILT
Moist, medium, brown w/ red and black, clayey SILT
Moist, medium, brownish red, sandy CLAY
Moist, medium, greyish brown, sandy SILT
Moist, medium, orangish brown, sandy SILT
Bottom of borehole at 27.8 feet.
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Bentonite
Seal1" Dia Sch.40 Riser
Sand1" Dia Sch.40 PVE
0.010" SlotScreen
DRAWN BY:JAO
BORING COMPLETED:6/21/16
DRILLING CONTRACTOR:Regional Probing Remarks:
DRILL RIG/ METHOD:Geoprobe 5410 / HA/DPT
SAMPLING METHOD:Hand Auger/ Macro-Core Groundwater sample collected.
BORING STARTED:6/21/16
LOGGED BY:JAO
TOTAL DEPTH: 27.8 ft.
TOP OF CASING ELEV: 100.28 ft.
DEPTH TO WATER:
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)
DE
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BORING DIAGRAM
Sheet 1 of 1
BORING NUMBER GP-9
PROJECT:Carolina Freightliner
JOB NUMBER:TPP-001
LOCATION:Raleigh, Wake County, NC
BO
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0
1
.
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2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
20
25
0
5
10
15
20
25

APPENDIX B

LABORATORY ANALYTICAL DATA

ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-106464-1
TestAmerica Sample Delivery Group: TPP-001
Client Project/Site: Carolina Freightliner
For:
Hart & Hickman, PC
3334 Hillsborough Street
Raleigh, North Carolina 27607
Attn: Leo Moretz
Authorized for release by:
6/30/2016 11:37:26 AM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Hart & Hickman, PC
Project/Site: Carolina Freightliner
TestAmerica Job ID: 490-106464-1
SDG: TPP-001
Page 2 of 47 TestAmerica Nashville6/30/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .26
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .40
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .43
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .44
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .45
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .47
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Sample Summary
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-106464-1 GP-7 (0-1)Soil 06/21/16 13:55 06/24/16 09:50
490-106464-2 GP-7 (4-5)Soil 06/21/16 14:05 06/24/16 09:50
490-106464-3 GP-8 (0-1)Soil 06/21/16 15:40 06/24/16 09:50
490-106464-4 GP-8 (4-5)Soil 06/21/16 15:45 06/24/16 09:50
490-106464-5 GP-5 Water 06/22/16 09:45 06/24/16 09:50
490-106464-6 GP-6 Water 06/22/16 10:30 06/24/16 09:50
490-106464-7 GP-7 Water 06/22/16 12:30 06/24/16 09:50
490-106464-8 GP-8 Water 06/22/16 11:35 06/24/16 09:50
490-106464-9 GP-9 Water 06/22/16 08:55 06/24/16 09:50
490-106464-10 Trip Blank Water 06/22/16 01:01 06/24/16 09:50
TestAmerica Nashville
Page 3 of 47 6/30/2016
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Case Narrative
Client: Hart & Hickman, PC TestAmerica Job ID: 490-106464-1
Project/Site: Carolina Freightliner SDG: TPP-001
Job ID: 490-106464-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-106464-1
Comments
No additional comments.
Receipt
The samples were received on 6/24/2016 9:50 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 1.8º C.
GC/MS VOA
Method(s) 8260B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
analytical batch 490-350852.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
TestAmerica NashvillePage 4 of 47 6/30/2016
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Definitions/Glossary
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Nashville
Page 5 of 47 6/30/2016
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-1Client Sample ID: GP-7 (0-1)
Matrix: SoilDate Collected: 06/21/16 13:55
Percent Solids: 83.7Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0615 mg/Kg ☼06/21/16 13:55 06/27/16 17:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Benzene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Bromobenzene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Bromochloromethane ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Bromodichloromethane ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Bromoform ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Bromomethane ND
0.0615 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼2-Butanone (MEK)ND
0.00615 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Carbon disulfide ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Carbon tetrachloride ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Chlorobenzene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Chlorodibromomethane ND
0.00615 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Chloroethane ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Chloroform ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Chloromethane ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼2-Chlorotoluene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼4-Chlorotoluene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼cis-1,2-Dichloroethene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼cis-1,3-Dichloropropene ND
0.00615 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,2-Dibromo-3-Chloropropane ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,2-Dibromoethane (EDB)ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Dibromomethane ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,2-Dichlorobenzene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,3-Dichlorobenzene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,4-Dichlorobenzene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Dichlorodifluoromethane ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,1-Dichloroethane ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,2-Dichloroethane ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,1-Dichloroethene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,2-Dichloroethene, Total ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,2-Dichloropropane ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,3-Dichloropropane ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼2,2-Dichloropropane ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,1-Dichloropropene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Diisopropyl ether ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Ethylbenzene ND
0.00615 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Hexachlorobutadiene ND
0.0615 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼2-Hexanone ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Isopropylbenzene ND
0.0123 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Methylene Chloride ND
0.0615 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼4-Methyl-2-pentanone (MIBK)ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Methyl tert-butyl ether ND
0.00615 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Naphthalene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼n-Butylbenzene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼N-Propylbenzene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼p-Isopropyltoluene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼sec-Butylbenzene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Styrene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-1Client Sample ID: GP-7 (0-1)
Matrix: SoilDate Collected: 06/21/16 13:55
Percent Solids: 83.7Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00246 mg/Kg ☼06/21/16 13:55 06/27/16 17:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,1,2,2-Tetrachloroethane ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Tetrachloroethene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Toluene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼trans-1,2-Dichloroethene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼trans-1,3-Dichloropropene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,2,3-Trichlorobenzene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,2,4-Trichlorobenzene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,1,1-Trichloroethane ND
0.00615 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,1,2-Trichloroethane ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Trichloroethene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Trichlorofluoromethane ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,2,3-Trichloropropane ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,2,4-Trimethylbenzene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼1,3,5-Trimethylbenzene ND
0.00246 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Vinyl chloride ND
0.00738 mg/Kg 06/21/16 13:55 06/27/16 17:19 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)106 70-130 06/21/16 13:55 06/27/16 17:19 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)105 06/21/16 13:55 06/27/16 17:19 170-130
1,2-Dichloroethane-d4 (Surr)107 06/21/16 13:55 06/27/16 17:19 170-130
Toluene-d8 (Surr)102 06/21/16 13:55 06/27/16 17:19 170-130
General Chemistry
RL RL
Percent Solids 83.7 0.1 %06/26/16 11:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-2Client Sample ID: GP-7 (4-5)
Matrix: SoilDate Collected: 06/21/16 14:05
Percent Solids: 83.4Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0516 mg/Kg ☼06/21/16 14:05 06/27/16 17:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Benzene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Bromobenzene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Bromochloromethane ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Bromodichloromethane ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Bromoform ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Bromomethane ND
0.0516 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼2-Butanone (MEK)ND
0.00516 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Carbon disulfide ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Carbon tetrachloride ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Chlorobenzene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Chlorodibromomethane ND
0.00516 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Chloroethane ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Chloroform ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Chloromethane ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼2-Chlorotoluene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼4-Chlorotoluene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼cis-1,2-Dichloroethene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼cis-1,3-Dichloropropene ND
0.00516 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,2-Dibromo-3-Chloropropane ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,2-Dibromoethane (EDB)ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Dibromomethane ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,2-Dichlorobenzene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,3-Dichlorobenzene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,4-Dichlorobenzene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Dichlorodifluoromethane ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,1-Dichloroethane ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,2-Dichloroethane ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,1-Dichloroethene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,2-Dichloroethene, Total ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,2-Dichloropropane ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,3-Dichloropropane ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼2,2-Dichloropropane ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,1-Dichloropropene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Diisopropyl ether ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Ethylbenzene ND
0.00516 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Hexachlorobutadiene ND
0.0516 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼2-Hexanone ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Isopropylbenzene ND
0.0103 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Methylene Chloride ND
0.0516 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼4-Methyl-2-pentanone (MIBK)ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Methyl tert-butyl ether ND
0.00516 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Naphthalene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼n-Butylbenzene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼N-Propylbenzene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼p-Isopropyltoluene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼sec-Butylbenzene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Styrene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-2Client Sample ID: GP-7 (4-5)
Matrix: SoilDate Collected: 06/21/16 14:05
Percent Solids: 83.4Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00206 mg/Kg ☼06/21/16 14:05 06/27/16 17:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,1,2,2-Tetrachloroethane ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Tetrachloroethene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Toluene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼trans-1,2-Dichloroethene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼trans-1,3-Dichloropropene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,2,3-Trichlorobenzene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,2,4-Trichlorobenzene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,1,1-Trichloroethane ND
0.00516 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,1,2-Trichloroethane ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Trichloroethene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Trichlorofluoromethane ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,2,3-Trichloropropane ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,2,4-Trimethylbenzene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼1,3,5-Trimethylbenzene ND
0.00206 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Vinyl chloride ND
0.00619 mg/Kg 06/21/16 14:05 06/27/16 17:46 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)104 70-130 06/21/16 14:05 06/27/16 17:46 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)104 06/21/16 14:05 06/27/16 17:46 170-130
1,2-Dichloroethane-d4 (Surr)106 06/21/16 14:05 06/27/16 17:46 170-130
Toluene-d8 (Surr)104 06/21/16 14:05 06/27/16 17:46 170-130
General Chemistry
RL RL
Percent Solids 83.4 0.1 %06/26/16 11:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-3Client Sample ID: GP-8 (0-1)
Matrix: SoilDate Collected: 06/21/16 15:40
Percent Solids: 67.9Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0597 mg/Kg ☼06/21/16 15:40 06/27/16 18:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Benzene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Bromobenzene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Bromochloromethane ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Bromodichloromethane ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Bromoform ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Bromomethane ND
0.0597 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼2-Butanone (MEK)ND
0.00597 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Carbon disulfide ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Carbon tetrachloride ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Chlorobenzene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Chlorodibromomethane ND
0.00597 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Chloroethane ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Chloroform ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Chloromethane ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼2-Chlorotoluene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼4-Chlorotoluene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼cis-1,2-Dichloroethene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼cis-1,3-Dichloropropene ND
0.00597 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,2-Dibromo-3-Chloropropane ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,2-Dibromoethane (EDB)ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Dibromomethane ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,2-Dichlorobenzene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,3-Dichlorobenzene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,4-Dichlorobenzene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Dichlorodifluoromethane ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,1-Dichloroethane ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,2-Dichloroethane ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,1-Dichloroethene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,2-Dichloroethene, Total ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,2-Dichloropropane ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,3-Dichloropropane ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼2,2-Dichloropropane ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,1-Dichloropropene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Diisopropyl ether ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Ethylbenzene ND
0.00597 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Hexachlorobutadiene ND
0.0597 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼2-Hexanone ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Isopropylbenzene ND
0.0119 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Methylene Chloride ND
0.0597 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼4-Methyl-2-pentanone (MIBK)ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Methyl tert-butyl ether ND
0.00597 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Naphthalene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼n-Butylbenzene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼N-Propylbenzene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼p-Isopropyltoluene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼sec-Butylbenzene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Styrene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-3Client Sample ID: GP-8 (0-1)
Matrix: SoilDate Collected: 06/21/16 15:40
Percent Solids: 67.9Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00239 mg/Kg ☼06/21/16 15:40 06/27/16 18:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,1,2,2-Tetrachloroethane ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Tetrachloroethene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Toluene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼trans-1,2-Dichloroethene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼trans-1,3-Dichloropropene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,2,3-Trichlorobenzene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,2,4-Trichlorobenzene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,1,1-Trichloroethane ND
0.00597 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,1,2-Trichloroethane ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Trichloroethene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Trichlorofluoromethane ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,2,3-Trichloropropane ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,2,4-Trimethylbenzene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼1,3,5-Trimethylbenzene ND
0.00239 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Vinyl chloride ND
0.00717 mg/Kg 06/21/16 15:40 06/27/16 18:14 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)104 70-130 06/21/16 15:40 06/27/16 18:14 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)104 06/21/16 15:40 06/27/16 18:14 170-130
1,2-Dichloroethane-d4 (Surr)104 06/21/16 15:40 06/27/16 18:14 170-130
Toluene-d8 (Surr)104 06/21/16 15:40 06/27/16 18:14 170-130
General Chemistry
RL RL
Percent Solids 67.9 0.1 %06/26/16 11:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-4Client Sample ID: GP-8 (4-5)
Matrix: SoilDate Collected: 06/21/16 15:45
Percent Solids: 79.8Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0609 mg/Kg ☼06/21/16 14:45 06/27/16 18:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Benzene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Bromobenzene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Bromochloromethane ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Bromodichloromethane ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Bromoform ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Bromomethane ND
0.0609 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼2-Butanone (MEK)ND
0.00609 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Carbon disulfide ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Carbon tetrachloride ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Chlorobenzene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Chlorodibromomethane ND
0.00609 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Chloroethane ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Chloroform ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Chloromethane ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼2-Chlorotoluene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼4-Chlorotoluene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼cis-1,2-Dichloroethene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼cis-1,3-Dichloropropene ND
0.00609 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,2-Dibromo-3-Chloropropane ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,2-Dibromoethane (EDB)ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Dibromomethane ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,2-Dichlorobenzene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,3-Dichlorobenzene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,4-Dichlorobenzene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Dichlorodifluoromethane ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,1-Dichloroethane ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,2-Dichloroethane ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,1-Dichloroethene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,2-Dichloroethene, Total ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,2-Dichloropropane ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,3-Dichloropropane ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼2,2-Dichloropropane ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,1-Dichloropropene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Diisopropyl ether ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Ethylbenzene ND
0.00609 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Hexachlorobutadiene ND
0.0609 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼2-Hexanone ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Isopropylbenzene ND
0.0122 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Methylene Chloride ND
0.0609 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼4-Methyl-2-pentanone (MIBK)ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Methyl tert-butyl ether ND
0.00609 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Naphthalene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼n-Butylbenzene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼N-Propylbenzene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼p-Isopropyltoluene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼sec-Butylbenzene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Styrene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-4Client Sample ID: GP-8 (4-5)
Matrix: SoilDate Collected: 06/21/16 15:45
Percent Solids: 79.8Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00244 mg/Kg ☼06/21/16 14:45 06/27/16 18:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,1,2,2-Tetrachloroethane ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Tetrachloroethene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Toluene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼trans-1,2-Dichloroethene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼trans-1,3-Dichloropropene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,2,3-Trichlorobenzene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,2,4-Trichlorobenzene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,1,1-Trichloroethane ND
0.00609 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,1,2-Trichloroethane ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Trichloroethene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Trichlorofluoromethane ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,2,3-Trichloropropane ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,2,4-Trimethylbenzene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼1,3,5-Trimethylbenzene ND
0.00244 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Vinyl chloride ND
0.00731 mg/Kg 06/21/16 14:45 06/27/16 18:41 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)104 70-130 06/21/16 14:45 06/27/16 18:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)104 06/21/16 14:45 06/27/16 18:41 170-130
1,2-Dichloroethane-d4 (Surr)104 06/21/16 14:45 06/27/16 18:41 170-130
Toluene-d8 (Surr)102 06/21/16 14:45 06/27/16 18:41 170-130
General Chemistry
RL RL
Percent Solids 79.8 0.1 %06/26/16 11:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-5Client Sample ID: GP-5
Matrix: WaterDate Collected: 06/22/16 09:45
Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 06/27/16 14:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 06/27/16 14:35 1BenzeneND
1.00 ug/L 06/27/16 14:35 1BromobenzeneND
1.00 ug/L 06/27/16 14:35 1BromochloromethaneND
1.00 ug/L 06/27/16 14:35 1BromodichloromethaneND
1.00 ug/L 06/27/16 14:35 1BromoformND
1.00 ug/L 06/27/16 14:35 1BromomethaneND
50.0 ug/L 06/27/16 14:35 12-Butanone (MEK)ND
1.00 ug/L 06/27/16 14:35 1Carbon disulfide ND
1.00 ug/L 06/27/16 14:35 1Carbon tetrachloride ND
1.00 ug/L 06/27/16 14:35 1ChlorobenzeneND
1.00 ug/L 06/27/16 14:35 1ChlorodibromomethaneND
1.00 ug/L 06/27/16 14:35 1ChloroethaneND
1.00 ug/L 06/27/16 14:35 1ChloroformND
1.00 ug/L 06/27/16 14:35 1ChloromethaneND
1.00 ug/L 06/27/16 14:35 12-Chlorotoluene ND
1.00 ug/L 06/27/16 14:35 14-Chlorotoluene ND
1.00 ug/L 06/27/16 14:35 1cis-1,2-Dichloroethene 8.73
1.00 ug/L 06/27/16 14:35 1cis-1,3-Dichloropropene ND
10.0 ug/L 06/27/16 14:35 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 06/27/16 14:35 11,2-Dibromoethane (EDB)ND
1.00 ug/L 06/27/16 14:35 1DibromomethaneND
1.00 ug/L 06/27/16 14:35 11,2-Dichlorobenzene ND
1.00 ug/L 06/27/16 14:35 11,3-Dichlorobenzene ND
1.00 ug/L 06/27/16 14:35 11,4-Dichlorobenzene ND
1.00 ug/L 06/27/16 14:35 1DichlorodifluoromethaneND
1.00 ug/L 06/27/16 14:35 11,1-Dichloroethane ND
1.00 ug/L 06/27/16 14:35 11,2-Dichloroethane ND
1.00 ug/L 06/27/16 14:35 11,1-Dichloroethene ND
1.00 ug/L 06/27/16 14:35 11,2-Dichloroethene, Total 8.73
1.00 ug/L 06/27/16 14:35 11,2-Dichloropropane ND
1.00 ug/L 06/27/16 14:35 11,3-Dichloropropane ND
1.00 ug/L 06/27/16 14:35 12,2-Dichloropropane ND
1.00 ug/L 06/27/16 14:35 11,1-Dichloropropene ND
2.00 ug/L 06/27/16 14:35 1Diisopropyl ether ND
1.00 ug/L 06/27/16 14:35 1EthylbenzeneND
2.00 ug/L 06/27/16 14:35 1HexachlorobutadieneND
10.0 ug/L 06/27/16 14:35 12-Hexanone ND
1.00 ug/L 06/27/16 14:35 1IsopropylbenzeneND
5.00 ug/L 06/27/16 14:35 1Methylene Chloride ND
10.0 ug/L 06/27/16 14:35 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 06/27/16 14:35 1Methyl tert-butyl ether ND
5.00 ug/L 06/27/16 14:35 1NaphthaleneND
1.00 ug/L 06/27/16 14:35 1n-Butylbenzene ND
1.00 ug/L 06/27/16 14:35 1N-Propylbenzene ND
1.00 ug/L 06/27/16 14:35 1p-Isopropyltoluene ND
1.00 ug/L 06/27/16 14:35 1sec-Butylbenzene ND
1.00 ug/L 06/27/16 14:35 1StyreneND
1.00 ug/L 06/27/16 14:35 1tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-5Client Sample ID: GP-5
Matrix: WaterDate Collected: 06/22/16 09:45
Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 06/27/16 14:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 06/27/16 14:35 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 06/27/16 14:35 1Tetrachloroethene10.7
1.00 ug/L 06/27/16 14:35 1TolueneND
1.00 ug/L 06/27/16 14:35 1trans-1,2-Dichloroethene ND
1.00 ug/L 06/27/16 14:35 1trans-1,3-Dichloropropene ND
1.00 ug/L 06/27/16 14:35 11,2,3-Trichlorobenzene ND
1.00 ug/L 06/27/16 14:35 11,2,4-Trichlorobenzene ND
1.00 ug/L 06/27/16 14:35 11,1,1-Trichloroethane ND
1.00 ug/L 06/27/16 14:35 11,1,2-Trichloroethane ND
1.00 ug/L 06/27/16 14:35 1Trichloroethene2.26
1.00 ug/L 06/27/16 14:35 1TrichlorofluoromethaneND
1.00 ug/L 06/27/16 14:35 11,2,3-Trichloropropane ND
1.00 ug/L 06/27/16 14:35 11,2,4-Trimethylbenzene ND
1.00 ug/L 06/27/16 14:35 11,3,5-Trimethylbenzene ND
1.00 ug/L 06/27/16 14:35 1Vinyl chloride ND
3.00 ug/L 06/27/16 14:35 1Xylenes, Total ND
4-Bromofluorobenzene (Surr)89 70-130 06/27/16 14:35 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)97 06/27/16 14:35 170-130
1,2-Dichloroethane-d4 (Surr)93 06/27/16 14:35 170-130
Toluene-d8 (Surr)102 06/27/16 14:35 170-130
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-6Client Sample ID: GP-6
Matrix: WaterDate Collected: 06/22/16 10:30
Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 06/27/16 15:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 06/27/16 15:01 1BenzeneND
1.00 ug/L 06/27/16 15:01 1BromobenzeneND
1.00 ug/L 06/27/16 15:01 1BromochloromethaneND
1.00 ug/L 06/27/16 15:01 1BromodichloromethaneND
1.00 ug/L 06/27/16 15:01 1BromoformND
1.00 ug/L 06/27/16 15:01 1BromomethaneND
50.0 ug/L 06/27/16 15:01 12-Butanone (MEK)ND
1.00 ug/L 06/27/16 15:01 1Carbon disulfide ND
1.00 ug/L 06/27/16 15:01 1Carbon tetrachloride ND
1.00 ug/L 06/27/16 15:01 1ChlorobenzeneND
1.00 ug/L 06/27/16 15:01 1ChlorodibromomethaneND
1.00 ug/L 06/27/16 15:01 1ChloroethaneND
1.00 ug/L 06/27/16 15:01 1ChloroformND
1.00 ug/L 06/27/16 15:01 1ChloromethaneND
1.00 ug/L 06/27/16 15:01 12-Chlorotoluene ND
1.00 ug/L 06/27/16 15:01 14-Chlorotoluene ND
1.00 ug/L 06/27/16 15:01 1cis-1,2-Dichloroethene 28.0
1.00 ug/L 06/27/16 15:01 1cis-1,3-Dichloropropene ND
10.0 ug/L 06/27/16 15:01 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 06/27/16 15:01 11,2-Dibromoethane (EDB)ND
1.00 ug/L 06/27/16 15:01 1DibromomethaneND
1.00 ug/L 06/27/16 15:01 11,2-Dichlorobenzene ND
1.00 ug/L 06/27/16 15:01 11,3-Dichlorobenzene ND
1.00 ug/L 06/27/16 15:01 11,4-Dichlorobenzene ND
1.00 ug/L 06/27/16 15:01 1DichlorodifluoromethaneND
1.00 ug/L 06/27/16 15:01 11,1-Dichloroethane ND
1.00 ug/L 06/27/16 15:01 11,2-Dichloroethane ND
1.00 ug/L 06/27/16 15:01 11,1-Dichloroethene ND
1.00 ug/L 06/27/16 15:01 11,2-Dichloroethene, Total 28.0
1.00 ug/L 06/27/16 15:01 11,2-Dichloropropane ND
1.00 ug/L 06/27/16 15:01 11,3-Dichloropropane ND
1.00 ug/L 06/27/16 15:01 12,2-Dichloropropane ND
1.00 ug/L 06/27/16 15:01 11,1-Dichloropropene ND
2.00 ug/L 06/27/16 15:01 1Diisopropyl ether ND
1.00 ug/L 06/27/16 15:01 1EthylbenzeneND
2.00 ug/L 06/27/16 15:01 1HexachlorobutadieneND
10.0 ug/L 06/27/16 15:01 12-Hexanone ND
1.00 ug/L 06/27/16 15:01 1IsopropylbenzeneND
5.00 ug/L 06/27/16 15:01 1Methylene Chloride ND
10.0 ug/L 06/27/16 15:01 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 06/27/16 15:01 1Methyl tert-butyl ether ND
5.00 ug/L 06/27/16 15:01 1NaphthaleneND
1.00 ug/L 06/27/16 15:01 1n-Butylbenzene ND
1.00 ug/L 06/27/16 15:01 1N-Propylbenzene ND
1.00 ug/L 06/27/16 15:01 1p-Isopropyltoluene ND
1.00 ug/L 06/27/16 15:01 1sec-Butylbenzene ND
1.00 ug/L 06/27/16 15:01 1StyreneND
1.00 ug/L 06/27/16 15:01 1tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-6Client Sample ID: GP-6
Matrix: WaterDate Collected: 06/22/16 10:30
Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 06/27/16 15:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 06/27/16 15:01 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 06/27/16 15:01 1Tetrachloroethene12.6
1.00 ug/L 06/27/16 15:01 1TolueneND
1.00 ug/L 06/27/16 15:01 1trans-1,2-Dichloroethene ND
1.00 ug/L 06/27/16 15:01 1trans-1,3-Dichloropropene ND
1.00 ug/L 06/27/16 15:01 11,2,3-Trichlorobenzene ND
1.00 ug/L 06/27/16 15:01 11,2,4-Trichlorobenzene ND
1.00 ug/L 06/27/16 15:01 11,1,1-Trichloroethane ND
1.00 ug/L 06/27/16 15:01 11,1,2-Trichloroethane ND
1.00 ug/L 06/27/16 15:01 1Trichloroethene3.05
1.00 ug/L 06/27/16 15:01 1TrichlorofluoromethaneND
1.00 ug/L 06/27/16 15:01 11,2,3-Trichloropropane ND
1.00 ug/L 06/27/16 15:01 11,2,4-Trimethylbenzene ND
1.00 ug/L 06/27/16 15:01 11,3,5-Trimethylbenzene ND
1.00 ug/L 06/27/16 15:01 1Vinyl chloride ND
3.00 ug/L 06/27/16 15:01 1Xylenes, Total ND
4-Bromofluorobenzene (Surr)88 70-130 06/27/16 15:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)98 06/27/16 15:01 170-130
1,2-Dichloroethane-d4 (Surr)96 06/27/16 15:01 170-130
Toluene-d8 (Surr)98 06/27/16 15:01 170-130
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-7Client Sample ID: GP-7
Matrix: WaterDate Collected: 06/22/16 12:30
Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 06/27/16 15:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 06/27/16 15:28 1BenzeneND
1.00 ug/L 06/27/16 15:28 1BromobenzeneND
1.00 ug/L 06/27/16 15:28 1BromochloromethaneND
1.00 ug/L 06/27/16 15:28 1BromodichloromethaneND
1.00 ug/L 06/27/16 15:28 1BromoformND
1.00 ug/L 06/27/16 15:28 1BromomethaneND
50.0 ug/L 06/27/16 15:28 12-Butanone (MEK)ND
1.00 ug/L 06/27/16 15:28 1Carbon disulfide ND
1.00 ug/L 06/27/16 15:28 1Carbon tetrachloride ND
1.00 ug/L 06/27/16 15:28 1ChlorobenzeneND
1.00 ug/L 06/27/16 15:28 1ChlorodibromomethaneND
1.00 ug/L 06/27/16 15:28 1ChloroethaneND
1.00 ug/L 06/27/16 15:28 1ChloroformND
1.00 ug/L 06/27/16 15:28 1ChloromethaneND
1.00 ug/L 06/27/16 15:28 12-Chlorotoluene ND
1.00 ug/L 06/27/16 15:28 14-Chlorotoluene ND
1.00 ug/L 06/27/16 15:28 1cis-1,2-Dichloroethene 13.4
1.00 ug/L 06/27/16 15:28 1cis-1,3-Dichloropropene ND
10.0 ug/L 06/27/16 15:28 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 06/27/16 15:28 11,2-Dibromoethane (EDB)ND
1.00 ug/L 06/27/16 15:28 1DibromomethaneND
1.00 ug/L 06/27/16 15:28 11,2-Dichlorobenzene ND
1.00 ug/L 06/27/16 15:28 11,3-Dichlorobenzene ND
1.00 ug/L 06/27/16 15:28 11,4-Dichlorobenzene ND
1.00 ug/L 06/27/16 15:28 1DichlorodifluoromethaneND
1.00 ug/L 06/27/16 15:28 11,1-Dichloroethane ND
1.00 ug/L 06/27/16 15:28 11,2-Dichloroethane ND
1.00 ug/L 06/27/16 15:28 11,1-Dichloroethene ND
1.00 ug/L 06/27/16 15:28 11,2-Dichloroethene, Total 13.4
1.00 ug/L 06/27/16 15:28 11,2-Dichloropropane ND
1.00 ug/L 06/27/16 15:28 11,3-Dichloropropane ND
1.00 ug/L 06/27/16 15:28 12,2-Dichloropropane ND
1.00 ug/L 06/27/16 15:28 11,1-Dichloropropene ND
2.00 ug/L 06/27/16 15:28 1Diisopropyl ether ND
1.00 ug/L 06/27/16 15:28 1EthylbenzeneND
2.00 ug/L 06/27/16 15:28 1HexachlorobutadieneND
10.0 ug/L 06/27/16 15:28 12-Hexanone ND
1.00 ug/L 06/27/16 15:28 1IsopropylbenzeneND
5.00 ug/L 06/27/16 15:28 1Methylene Chloride ND
10.0 ug/L 06/27/16 15:28 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 06/27/16 15:28 1Methyl tert-butyl ether ND
5.00 ug/L 06/27/16 15:28 1NaphthaleneND
1.00 ug/L 06/27/16 15:28 1n-Butylbenzene ND
1.00 ug/L 06/27/16 15:28 1N-Propylbenzene ND
1.00 ug/L 06/27/16 15:28 1p-Isopropyltoluene ND
1.00 ug/L 06/27/16 15:28 1sec-Butylbenzene ND
1.00 ug/L 06/27/16 15:28 1StyreneND
1.00 ug/L 06/27/16 15:28 1tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-7Client Sample ID: GP-7
Matrix: WaterDate Collected: 06/22/16 12:30
Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 06/27/16 15:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 06/27/16 15:28 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 06/27/16 15:28 1Tetrachloroethene19.8
1.00 ug/L 06/27/16 15:28 1TolueneND
1.00 ug/L 06/27/16 15:28 1trans-1,2-Dichloroethene ND
1.00 ug/L 06/27/16 15:28 1trans-1,3-Dichloropropene ND
1.00 ug/L 06/27/16 15:28 11,2,3-Trichlorobenzene ND
1.00 ug/L 06/27/16 15:28 11,2,4-Trichlorobenzene ND
1.00 ug/L 06/27/16 15:28 11,1,1-Trichloroethane ND
1.00 ug/L 06/27/16 15:28 11,1,2-Trichloroethane ND
1.00 ug/L 06/27/16 15:28 1Trichloroethene4.27
1.00 ug/L 06/27/16 15:28 1TrichlorofluoromethaneND
1.00 ug/L 06/27/16 15:28 11,2,3-Trichloropropane ND
1.00 ug/L 06/27/16 15:28 11,2,4-Trimethylbenzene ND
1.00 ug/L 06/27/16 15:28 11,3,5-Trimethylbenzene ND
1.00 ug/L 06/27/16 15:28 1Vinyl chloride ND
3.00 ug/L 06/27/16 15:28 1Xylenes, Total ND
4-Bromofluorobenzene (Surr)88 70-130 06/27/16 15:28 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)98 06/27/16 15:28 170-130
1,2-Dichloroethane-d4 (Surr)95 06/27/16 15:28 170-130
Toluene-d8 (Surr)96 06/27/16 15:28 170-130
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-8Client Sample ID: GP-8
Matrix: WaterDate Collected: 06/22/16 11:35
Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 06/27/16 15:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 06/27/16 15:54 1BenzeneND
1.00 ug/L 06/27/16 15:54 1BromobenzeneND
1.00 ug/L 06/27/16 15:54 1BromochloromethaneND
1.00 ug/L 06/27/16 15:54 1BromodichloromethaneND
1.00 ug/L 06/27/16 15:54 1BromoformND
1.00 ug/L 06/27/16 15:54 1BromomethaneND
50.0 ug/L 06/27/16 15:54 12-Butanone (MEK)ND
1.00 ug/L 06/27/16 15:54 1Carbon disulfide ND
1.00 ug/L 06/27/16 15:54 1Carbon tetrachloride ND
1.00 ug/L 06/27/16 15:54 1ChlorobenzeneND
1.00 ug/L 06/27/16 15:54 1ChlorodibromomethaneND
1.00 ug/L 06/27/16 15:54 1ChloroethaneND
1.00 ug/L 06/27/16 15:54 1ChloroformND
1.00 ug/L 06/27/16 15:54 1ChloromethaneND
1.00 ug/L 06/27/16 15:54 12-Chlorotoluene ND
1.00 ug/L 06/27/16 15:54 14-Chlorotoluene ND
1.00 ug/L 06/27/16 15:54 1cis-1,2-Dichloroethene 31.4
1.00 ug/L 06/27/16 15:54 1cis-1,3-Dichloropropene ND
10.0 ug/L 06/27/16 15:54 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 06/27/16 15:54 11,2-Dibromoethane (EDB)ND
1.00 ug/L 06/27/16 15:54 1DibromomethaneND
1.00 ug/L 06/27/16 15:54 11,2-Dichlorobenzene ND
1.00 ug/L 06/27/16 15:54 11,3-Dichlorobenzene ND
1.00 ug/L 06/27/16 15:54 11,4-Dichlorobenzene ND
1.00 ug/L 06/27/16 15:54 1DichlorodifluoromethaneND
1.00 ug/L 06/27/16 15:54 11,1-Dichloroethane ND
1.00 ug/L 06/27/16 15:54 11,2-Dichloroethane ND
1.00 ug/L 06/27/16 15:54 11,1-Dichloroethene ND
1.00 ug/L 06/27/16 15:54 11,2-Dichloroethene, Total 31.4
1.00 ug/L 06/27/16 15:54 11,2-Dichloropropane ND
1.00 ug/L 06/27/16 15:54 11,3-Dichloropropane ND
1.00 ug/L 06/27/16 15:54 12,2-Dichloropropane ND
1.00 ug/L 06/27/16 15:54 11,1-Dichloropropene ND
2.00 ug/L 06/27/16 15:54 1Diisopropyl ether ND
1.00 ug/L 06/27/16 15:54 1EthylbenzeneND
2.00 ug/L 06/27/16 15:54 1HexachlorobutadieneND
10.0 ug/L 06/27/16 15:54 12-Hexanone ND
1.00 ug/L 06/27/16 15:54 1IsopropylbenzeneND
5.00 ug/L 06/27/16 15:54 1Methylene Chloride ND
10.0 ug/L 06/27/16 15:54 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 06/27/16 15:54 1Methyl tert-butyl ether ND
5.00 ug/L 06/27/16 15:54 1NaphthaleneND
1.00 ug/L 06/27/16 15:54 1n-Butylbenzene ND
1.00 ug/L 06/27/16 15:54 1N-Propylbenzene ND
1.00 ug/L 06/27/16 15:54 1p-Isopropyltoluene ND
1.00 ug/L 06/27/16 15:54 1sec-Butylbenzene ND
1.00 ug/L 06/27/16 15:54 1StyreneND
1.00 ug/L 06/27/16 15:54 1tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-8Client Sample ID: GP-8
Matrix: WaterDate Collected: 06/22/16 11:35
Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 06/27/16 15:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 06/27/16 15:54 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 06/27/16 15:54 1Tetrachloroethene12.0
1.00 ug/L 06/27/16 15:54 1TolueneND
1.00 ug/L 06/27/16 15:54 1trans-1,2-Dichloroethene ND
1.00 ug/L 06/27/16 15:54 1trans-1,3-Dichloropropene ND
1.00 ug/L 06/27/16 15:54 11,2,3-Trichlorobenzene ND
1.00 ug/L 06/27/16 15:54 11,2,4-Trichlorobenzene ND
1.00 ug/L 06/27/16 15:54 11,1,1-Trichloroethane ND
1.00 ug/L 06/27/16 15:54 11,1,2-Trichloroethane ND
1.00 ug/L 06/27/16 15:54 1Trichloroethene4.09
1.00 ug/L 06/27/16 15:54 1TrichlorofluoromethaneND
1.00 ug/L 06/27/16 15:54 11,2,3-Trichloropropane ND
1.00 ug/L 06/27/16 15:54 11,2,4-Trimethylbenzene ND
1.00 ug/L 06/27/16 15:54 11,3,5-Trimethylbenzene ND
1.00 ug/L 06/27/16 15:54 1Vinyl chloride ND
3.00 ug/L 06/27/16 15:54 1Xylenes, Total ND
4-Bromofluorobenzene (Surr)87 70-130 06/27/16 15:54 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)99 06/27/16 15:54 170-130
1,2-Dichloroethane-d4 (Surr)97 06/27/16 15:54 170-130
Toluene-d8 (Surr)98 06/27/16 15:54 170-130
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-9Client Sample ID: GP-9
Matrix: WaterDate Collected: 06/22/16 08:55
Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 06/27/16 16:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 06/27/16 16:20 1BenzeneND
1.00 ug/L 06/27/16 16:20 1BromobenzeneND
1.00 ug/L 06/27/16 16:20 1BromochloromethaneND
1.00 ug/L 06/27/16 16:20 1BromodichloromethaneND
1.00 ug/L 06/27/16 16:20 1BromoformND
1.00 ug/L 06/27/16 16:20 1BromomethaneND
50.0 ug/L 06/27/16 16:20 12-Butanone (MEK)ND
1.00 ug/L 06/27/16 16:20 1Carbon disulfide ND
1.00 ug/L 06/27/16 16:20 1Carbon tetrachloride ND
1.00 ug/L 06/27/16 16:20 1ChlorobenzeneND
1.00 ug/L 06/27/16 16:20 1ChlorodibromomethaneND
1.00 ug/L 06/27/16 16:20 1ChloroethaneND
1.00 ug/L 06/27/16 16:20 1ChloroformND
1.00 ug/L 06/27/16 16:20 1ChloromethaneND
1.00 ug/L 06/27/16 16:20 12-Chlorotoluene ND
1.00 ug/L 06/27/16 16:20 14-Chlorotoluene ND
1.00 ug/L 06/27/16 16:20 1cis-1,2-Dichloroethene ND
1.00 ug/L 06/27/16 16:20 1cis-1,3-Dichloropropene ND
10.0 ug/L 06/27/16 16:20 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 06/27/16 16:20 11,2-Dibromoethane (EDB)ND
1.00 ug/L 06/27/16 16:20 1DibromomethaneND
1.00 ug/L 06/27/16 16:20 11,2-Dichlorobenzene ND
1.00 ug/L 06/27/16 16:20 11,3-Dichlorobenzene ND
1.00 ug/L 06/27/16 16:20 11,4-Dichlorobenzene ND
1.00 ug/L 06/27/16 16:20 1DichlorodifluoromethaneND
1.00 ug/L 06/27/16 16:20 11,1-Dichloroethane ND
1.00 ug/L 06/27/16 16:20 11,2-Dichloroethane ND
1.00 ug/L 06/27/16 16:20 11,1-Dichloroethene ND
1.00 ug/L 06/27/16 16:20 11,2-Dichloroethene, Total ND
1.00 ug/L 06/27/16 16:20 11,2-Dichloropropane ND
1.00 ug/L 06/27/16 16:20 11,3-Dichloropropane ND
1.00 ug/L 06/27/16 16:20 12,2-Dichloropropane ND
1.00 ug/L 06/27/16 16:20 11,1-Dichloropropene ND
2.00 ug/L 06/27/16 16:20 1Diisopropyl ether ND
1.00 ug/L 06/27/16 16:20 1EthylbenzeneND
2.00 ug/L 06/27/16 16:20 1HexachlorobutadieneND
10.0 ug/L 06/27/16 16:20 12-Hexanone ND
1.00 ug/L 06/27/16 16:20 1IsopropylbenzeneND
5.00 ug/L 06/27/16 16:20 1Methylene Chloride ND
10.0 ug/L 06/27/16 16:20 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 06/27/16 16:20 1Methyl tert-butyl ether ND
5.00 ug/L 06/27/16 16:20 1NaphthaleneND
1.00 ug/L 06/27/16 16:20 1n-Butylbenzene ND
1.00 ug/L 06/27/16 16:20 1N-Propylbenzene ND
1.00 ug/L 06/27/16 16:20 1p-Isopropyltoluene ND
1.00 ug/L 06/27/16 16:20 1sec-Butylbenzene ND
1.00 ug/L 06/27/16 16:20 1StyreneND
1.00 ug/L 06/27/16 16:20 1tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-9Client Sample ID: GP-9
Matrix: WaterDate Collected: 06/22/16 08:55
Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 06/27/16 16:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 06/27/16 16:20 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 06/27/16 16:20 1TetrachloroetheneND
1.00 ug/L 06/27/16 16:20 1TolueneND
1.00 ug/L 06/27/16 16:20 1trans-1,2-Dichloroethene ND
1.00 ug/L 06/27/16 16:20 1trans-1,3-Dichloropropene ND
1.00 ug/L 06/27/16 16:20 11,2,3-Trichlorobenzene ND
1.00 ug/L 06/27/16 16:20 11,2,4-Trichlorobenzene ND
1.00 ug/L 06/27/16 16:20 11,1,1-Trichloroethane ND
1.00 ug/L 06/27/16 16:20 11,1,2-Trichloroethane ND
1.00 ug/L 06/27/16 16:20 1TrichloroetheneND
1.00 ug/L 06/27/16 16:20 1TrichlorofluoromethaneND
1.00 ug/L 06/27/16 16:20 11,2,3-Trichloropropane ND
1.00 ug/L 06/27/16 16:20 11,2,4-Trimethylbenzene ND
1.00 ug/L 06/27/16 16:20 11,3,5-Trimethylbenzene ND
1.00 ug/L 06/27/16 16:20 1Vinyl chloride ND
3.00 ug/L 06/27/16 16:20 1Xylenes, Total ND
4-Bromofluorobenzene (Surr)89 70-130 06/27/16 16:20 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)99 06/27/16 16:20 170-130
1,2-Dichloroethane-d4 (Surr)96 06/27/16 16:20 170-130
Toluene-d8 (Surr)95 06/27/16 16:20 170-130
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-10Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 06/22/16 01:01
Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 06/27/16 14:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 06/27/16 14:09 1BenzeneND
1.00 ug/L 06/27/16 14:09 1BromobenzeneND
1.00 ug/L 06/27/16 14:09 1BromochloromethaneND
1.00 ug/L 06/27/16 14:09 1BromodichloromethaneND
1.00 ug/L 06/27/16 14:09 1BromoformND
1.00 ug/L 06/27/16 14:09 1BromomethaneND
50.0 ug/L 06/27/16 14:09 12-Butanone (MEK)ND
1.00 ug/L 06/27/16 14:09 1Carbon disulfide ND
1.00 ug/L 06/27/16 14:09 1Carbon tetrachloride ND
1.00 ug/L 06/27/16 14:09 1ChlorobenzeneND
1.00 ug/L 06/27/16 14:09 1ChlorodibromomethaneND
1.00 ug/L 06/27/16 14:09 1ChloroethaneND
1.00 ug/L 06/27/16 14:09 1ChloroformND
1.00 ug/L 06/27/16 14:09 1ChloromethaneND
1.00 ug/L 06/27/16 14:09 12-Chlorotoluene ND
1.00 ug/L 06/27/16 14:09 14-Chlorotoluene ND
1.00 ug/L 06/27/16 14:09 1cis-1,2-Dichloroethene ND
1.00 ug/L 06/27/16 14:09 1cis-1,3-Dichloropropene ND
10.0 ug/L 06/27/16 14:09 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 06/27/16 14:09 11,2-Dibromoethane (EDB)ND
1.00 ug/L 06/27/16 14:09 1DibromomethaneND
1.00 ug/L 06/27/16 14:09 11,2-Dichlorobenzene ND
1.00 ug/L 06/27/16 14:09 11,3-Dichlorobenzene ND
1.00 ug/L 06/27/16 14:09 11,4-Dichlorobenzene ND
1.00 ug/L 06/27/16 14:09 1DichlorodifluoromethaneND
1.00 ug/L 06/27/16 14:09 11,1-Dichloroethane ND
1.00 ug/L 06/27/16 14:09 11,2-Dichloroethane ND
1.00 ug/L 06/27/16 14:09 11,1-Dichloroethene ND
1.00 ug/L 06/27/16 14:09 11,2-Dichloroethene, Total ND
1.00 ug/L 06/27/16 14:09 11,2-Dichloropropane ND
1.00 ug/L 06/27/16 14:09 11,3-Dichloropropane ND
1.00 ug/L 06/27/16 14:09 12,2-Dichloropropane ND
1.00 ug/L 06/27/16 14:09 11,1-Dichloropropene ND
2.00 ug/L 06/27/16 14:09 1Diisopropyl ether ND
1.00 ug/L 06/27/16 14:09 1EthylbenzeneND
2.00 ug/L 06/27/16 14:09 1HexachlorobutadieneND
10.0 ug/L 06/27/16 14:09 12-Hexanone ND
1.00 ug/L 06/27/16 14:09 1IsopropylbenzeneND
5.00 ug/L 06/27/16 14:09 1Methylene Chloride ND
10.0 ug/L 06/27/16 14:09 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 06/27/16 14:09 1Methyl tert-butyl ether ND
5.00 ug/L 06/27/16 14:09 1NaphthaleneND
1.00 ug/L 06/27/16 14:09 1n-Butylbenzene ND
1.00 ug/L 06/27/16 14:09 1N-Propylbenzene ND
1.00 ug/L 06/27/16 14:09 1p-Isopropyltoluene ND
1.00 ug/L 06/27/16 14:09 1sec-Butylbenzene ND
1.00 ug/L 06/27/16 14:09 1StyreneND
1.00 ug/L 06/27/16 14:09 1tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Lab Sample ID: 490-106464-10Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 06/22/16 01:01
Date Received: 06/24/16 09:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 06/27/16 14:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 06/27/16 14:09 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 06/27/16 14:09 1TetrachloroetheneND
1.00 ug/L 06/27/16 14:09 1TolueneND
1.00 ug/L 06/27/16 14:09 1trans-1,2-Dichloroethene ND
1.00 ug/L 06/27/16 14:09 1trans-1,3-Dichloropropene ND
1.00 ug/L 06/27/16 14:09 11,2,3-Trichlorobenzene ND
1.00 ug/L 06/27/16 14:09 11,2,4-Trichlorobenzene ND
1.00 ug/L 06/27/16 14:09 11,1,1-Trichloroethane ND
1.00 ug/L 06/27/16 14:09 11,1,2-Trichloroethane ND
1.00 ug/L 06/27/16 14:09 1TrichloroetheneND
1.00 ug/L 06/27/16 14:09 1TrichlorofluoromethaneND
1.00 ug/L 06/27/16 14:09 11,2,3-Trichloropropane ND
1.00 ug/L 06/27/16 14:09 11,2,4-Trimethylbenzene ND
1.00 ug/L 06/27/16 14:09 11,3,5-Trimethylbenzene ND
1.00 ug/L 06/27/16 14:09 1Vinyl chloride ND
3.00 ug/L 06/27/16 14:09 1Xylenes, Total ND
4-Bromofluorobenzene (Surr)89 70-130 06/27/16 14:09 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)98 06/27/16 14:09 170-130
1,2-Dichloroethane-d4 (Surr)96 06/27/16 14:09 170-130
Toluene-d8 (Surr)98 06/27/16 14:09 170-130
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QC Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-350852/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 350852
RL MDL
Acetone ND 0.0500 mg/Kg 06/27/16 12:43 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00200 mg/Kg 06/27/16 12:43 1Benzene
ND 0.00200 mg/Kg 06/27/16 12:43 1Bromobenzene
ND 0.00200 mg/Kg 06/27/16 12:43 1Bromochloromethane
ND 0.00200 mg/Kg 06/27/16 12:43 1Bromodichloromethane
ND 0.00200 mg/Kg 06/27/16 12:43 1Bromoform
ND 0.00200 mg/Kg 06/27/16 12:43 1Bromomethane
ND 0.0500 mg/Kg 06/27/16 12:43 12-Butanone (MEK)
ND 0.00500 mg/Kg 06/27/16 12:43 1Carbon disulfide
ND 0.00200 mg/Kg 06/27/16 12:43 1Carbon tetrachloride
ND 0.00200 mg/Kg 06/27/16 12:43 1Chlorobenzene
ND 0.00200 mg/Kg 06/27/16 12:43 1Chlorodibromomethane
ND 0.00500 mg/Kg 06/27/16 12:43 1Chloroethane
ND 0.00200 mg/Kg 06/27/16 12:43 1Chloroform
ND 0.00200 mg/Kg 06/27/16 12:43 1Chloromethane
ND 0.00200 mg/Kg 06/27/16 12:43 12-Chlorotoluene
ND 0.00200 mg/Kg 06/27/16 12:43 14-Chlorotoluene
ND 0.00200 mg/Kg 06/27/16 12:43 1cis-1,2-Dichloroethene
ND 0.00200 mg/Kg 06/27/16 12:43 1cis-1,3-Dichloropropene
ND 0.00500 mg/Kg 06/27/16 12:43 11,2-Dibromo-3-Chloropropane
ND 0.00200 mg/Kg 06/27/16 12:43 11,2-Dibromoethane (EDB)
ND 0.00200 mg/Kg 06/27/16 12:43 1Dibromomethane
ND 0.00200 mg/Kg 06/27/16 12:43 11,2-Dichlorobenzene
ND 0.00200 mg/Kg 06/27/16 12:43 11,3-Dichlorobenzene
ND 0.00200 mg/Kg 06/27/16 12:43 11,4-Dichlorobenzene
ND 0.00200 mg/Kg 06/27/16 12:43 1Dichlorodifluoromethane
ND 0.00200 mg/Kg 06/27/16 12:43 11,1-Dichloroethane
ND 0.00200 mg/Kg 06/27/16 12:43 11,2-Dichloroethane
ND 0.00200 mg/Kg 06/27/16 12:43 11,1-Dichloroethene
ND 0.00200 mg/Kg 06/27/16 12:43 11,2-Dichloroethene, Total
ND 0.00200 mg/Kg 06/27/16 12:43 11,2-Dichloropropane
ND 0.00200 mg/Kg 06/27/16 12:43 11,3-Dichloropropane
ND 0.00200 mg/Kg 06/27/16 12:43 12,2-Dichloropropane
ND 0.00200 mg/Kg 06/27/16 12:43 11,1-Dichloropropene
ND 0.00200 mg/Kg 06/27/16 12:43 1Diisopropyl ether
ND 0.00200 mg/Kg 06/27/16 12:43 1Ethylbenzene
ND 0.00500 mg/Kg 06/27/16 12:43 1Hexachlorobutadiene
ND 0.0500 mg/Kg 06/27/16 12:43 12-Hexanone
ND 0.00200 mg/Kg 06/27/16 12:43 1Isopropylbenzene
ND 0.0100 mg/Kg 06/27/16 12:43 1Methylene Chloride
ND 0.0500 mg/Kg 06/27/16 12:43 14-Methyl-2-pentanone (MIBK)
ND 0.00200 mg/Kg 06/27/16 12:43 1Methyl tert-butyl ether
ND 0.00500 mg/Kg 06/27/16 12:43 1Naphthalene
ND 0.00200 mg/Kg 06/27/16 12:43 1n-Butylbenzene
ND 0.00200 mg/Kg 06/27/16 12:43 1N-Propylbenzene
ND 0.00200 mg/Kg 06/27/16 12:43 1p-Isopropyltoluene
ND 0.00200 mg/Kg 06/27/16 12:43 1sec-Butylbenzene
ND 0.00200 mg/Kg 06/27/16 12:43 1Styrene
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QC Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-350852/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 350852
RL MDL
tert-Butylbenzene ND 0.00200 mg/Kg 06/27/16 12:43 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00200 mg/Kg 06/27/16 12:43 11,1,1,2-Tetrachloroethane
ND 0.00200 mg/Kg 06/27/16 12:43 11,1,2,2-Tetrachloroethane
ND 0.00200 mg/Kg 06/27/16 12:43 1Tetrachloroethene
ND 0.00200 mg/Kg 06/27/16 12:43 1Toluene
ND 0.00200 mg/Kg 06/27/16 12:43 1trans-1,2-Dichloroethene
ND 0.00200 mg/Kg 06/27/16 12:43 1trans-1,3-Dichloropropene
ND 0.00200 mg/Kg 06/27/16 12:43 11,2,3-Trichlorobenzene
ND 0.00200 mg/Kg 06/27/16 12:43 11,2,4-Trichlorobenzene
ND 0.00200 mg/Kg 06/27/16 12:43 11,1,1-Trichloroethane
ND 0.00500 mg/Kg 06/27/16 12:43 11,1,2-Trichloroethane
ND 0.00200 mg/Kg 06/27/16 12:43 1Trichloroethene
ND 0.00200 mg/Kg 06/27/16 12:43 1Trichlorofluoromethane
ND 0.00200 mg/Kg 06/27/16 12:43 11,2,3-Trichloropropane
ND 0.00200 mg/Kg 06/27/16 12:43 11,2,4-Trimethylbenzene
ND 0.00200 mg/Kg 06/27/16 12:43 11,3,5-Trimethylbenzene
ND 0.00200 mg/Kg 06/27/16 12:43 1Vinyl chloride
ND 0.00600 mg/Kg 06/27/16 12:43 1Xylenes, Total
4-Bromofluorobenzene (Surr)98 70-130 06/27/16 12:43 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
103 06/27/16 12:43 1Dibromofluoromethane (Surr)70-130
97 06/27/16 12:43 11,2-Dichloroethane-d4 (Surr)70-130
99 06/27/16 12:43 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-350852/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 350852
Acetone 0.250 0.2505 mg/Kg 100 45 -145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 0.0500 0.05256 mg/Kg 105 70 -130
Bromobenzene 0.0500 0.05157 mg/Kg 103 67 -130
Bromochloromethane 0.0500 0.05578 mg/Kg 112 70 -133
Bromodichloromethane 0.0500 0.05259 mg/Kg 105 70 -130
Bromoform 0.0500 0.05279 mg/Kg 106 59 -137
Bromomethane 0.0500 0.03813 mg/Kg 76 32 -150
2-Butanone (MEK)0.250 0.2698 mg/Kg 108 50 -149
Carbon disulfide 0.0500 0.05098 mg/Kg 102 66 -138
Carbon tetrachloride 0.0500 0.05314 mg/Kg 106 70 -131
Chlorobenzene 0.0500 0.05450 mg/Kg 109 70 -130
Chlorodibromomethane 0.0500 0.05384 mg/Kg 108 70 -130
Chloroethane 0.0500 0.05221 mg/Kg 104 37 -150
Chloroform 0.0500 0.05151 mg/Kg 103 70 -130
Chloromethane 0.0500 0.04431 mg/Kg 89 53 -150
2-Chlorotoluene 0.0500 0.05329 mg/Kg 107 70 -132
4-Chlorotoluene 0.0500 0.05335 mg/Kg 107 67 -135
cis-1,2-Dichloroethene 0.0500 0.05285 mg/Kg 106 70 -132
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QC Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-350852/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 350852
cis-1,3-Dichloropropene 0.0500 0.05221 mg/Kg 104 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dibromo-3-Chloropropane 0.0500 0.05209 mg/Kg 104 47 -144
1,2-Dibromoethane (EDB)0.0500 0.05326 mg/Kg 107 69 -130
Dibromomethane 0.0500 0.05280 mg/Kg 106 70 -130
1,2-Dichlorobenzene 0.0500 0.05365 mg/Kg 107 70 -134
1,3-Dichlorobenzene 0.0500 0.05326 mg/Kg 107 69 -137
1,4-Dichlorobenzene 0.0500 0.05272 mg/Kg 105 66 -134
Dichlorodifluoromethane 0.0500 0.04623 mg/Kg 92 32 -150
1,1-Dichloroethane 0.0500 0.05060 mg/Kg 101 70 -130
1,2-Dichloroethane 0.0500 0.04912 mg/Kg 98 65 -134
1,1-Dichloroethene 0.0500 0.05189 mg/Kg 104 70 -131
1,2-Dichloroethene, Total 0.100 0.1052 mg/Kg 105 70 -130
1,2-Dichloropropane 0.0500 0.05242 mg/Kg 105 70 -130
1,3-Dichloropropane 0.0500 0.05230 mg/Kg 105 70 -130
2,2-Dichloropropane 0.0500 0.05106 mg/Kg 102 57 -150
1,1-Dichloropropene 0.0500 0.05241 mg/Kg 105 70 -130
Diisopropyl ether 0.0500 0.05138 mg/Kg 103 68 -134
Ethylbenzene 0.0500 0.05293 mg/Kg 106 70 -130
Hexachlorobutadiene 0.0500 0.05131 mg/Kg 103 64 -137
2-Hexanone 0.250 0.2583 mg/Kg 103 47 -148
Isopropylbenzene 0.0500 0.05421 mg/Kg 108 70 -130
Methylene Chloride 0.0500 0.05231 mg/Kg 105 69 -130
4-Methyl-2-pentanone (MIBK)0.250 0.2588 mg/Kg 104 48 -150
Methyl tert-butyl ether 0.0500 0.05244 mg/Kg 105 54 -145
Naphthalene 0.0500 0.05207 mg/Kg 104 55 -149
n-Butylbenzene 0.0500 0.05091 mg/Kg 102 57 -150
N-Propylbenzene 0.0500 0.05383 mg/Kg 108 62 -150
p-Isopropyltoluene 0.0500 0.05197 mg/Kg 104 66 -147
sec-Butylbenzene 0.0500 0.05314 mg/Kg 106 68 -147
Styrene 0.0500 0.05360 mg/Kg 107 70 -131
tert-Butylbenzene 0.0500 0.05411 mg/Kg 108 70 -138
1,1,1,2-Tetrachloroethane 0.0500 0.05339 mg/Kg 107 70 -130
1,1,2,2-Tetrachloroethane 0.0500 0.05320 mg/Kg 106 61 -134
Tetrachloroethene 0.0500 0.05294 mg/Kg 106 70 -130
Toluene 0.0500 0.05310 mg/Kg 106 70 -130
trans-1,2-Dichloroethene 0.0500 0.05232 mg/Kg 105 70 -130
trans-1,3-Dichloropropene 0.0500 0.05138 mg/Kg 103 67 -130
1,2,3-Trichlorobenzene 0.0500 0.05357 mg/Kg 107 57 -146
1,2,4-Trichlorobenzene 0.0500 0.05237 mg/Kg 105 47 -150
1,1,1-Trichloroethane 0.0500 0.05198 mg/Kg 104 70 -130
1,1,2-Trichloroethane 0.0500 0.05150 mg/Kg 103 70 -130
Trichloroethene 0.0500 0.05522 mg/Kg 110 70 -130
Trichlorofluoromethane 0.0500 0.04871 mg/Kg 97 53 -150
1,2,3-Trichloropropane 0.0500 0.05375 mg/Kg 107 60 -139
1,2,4-Trimethylbenzene 0.0500 0.05266 mg/Kg 105 70 -140
1,3,5-Trimethylbenzene 0.0500 0.05306 mg/Kg 106 69 -141
Vinyl chloride 0.0500 0.05084 mg/Kg 102 63 -150
Xylenes, Total 0.100 0.1045 mg/Kg 105 70 -130
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QC Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-350852/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 350852
4-Bromofluorobenzene (Surr)70 -130
Surrogate
98
LCS LCS
Qualifier Limits%Recovery
101Dibromofluoromethane (Surr)70 -130
911,2-Dichloroethane-d4 (Surr)70 -130
100Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-350852/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 350852
Acetone 0.250 0.2473 mg/Kg 99 45 -145 1 38
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 0.0500 0.05240 mg/Kg 105 70 -130 0 37
Bromobenzene 0.0500 0.05063 mg/Kg 101 67 -130 2 40
Bromochloromethane 0.0500 0.05418 mg/Kg 108 70 -133 3 15
Bromodichloromethane 0.0500 0.05077 mg/Kg 102 70 -130 4 20
Bromoform 0.0500 0.05286 mg/Kg 106 59 -137 0 17
Bromomethane 0.0500 0.03921 mg/Kg 78 32 -150 3 45
2-Butanone (MEK)0.250 0.2627 mg/Kg 105 50 -149 3 39
Carbon disulfide 0.0500 0.05061 mg/Kg 101 66 -138 1 41
Carbon tetrachloride 0.0500 0.05336 mg/Kg 107 70 -131 0 41
Chlorobenzene 0.0500 0.05370 mg/Kg 107 70 -130 1 40
Chlorodibromomethane 0.0500 0.05347 mg/Kg 107 70 -130 1 14
Chloroethane 0.0500 0.05076 mg/Kg 102 37 -150 3 50
Chloroform 0.0500 0.05111 mg/Kg 102 70 -130 1 15
Chloromethane 0.0500 0.04346 mg/Kg 87 53 -150 2 47
2-Chlorotoluene 0.0500 0.05215 mg/Kg 104 70 -132 2 41
4-Chlorotoluene 0.0500 0.05168 mg/Kg 103 67 -135 3 41
cis-1,2-Dichloroethene 0.0500 0.05184 mg/Kg 104 70 -132 2 18
cis-1,3-Dichloropropene 0.0500 0.05169 mg/Kg 103 70 -130 1 42
1,2-Dibromo-3-Chloropropane 0.0500 0.05148 mg/Kg 103 47 -144 1 38
1,2-Dibromoethane (EDB)0.0500 0.05320 mg/Kg 106 69 -130 0 17
Dibromomethane 0.0500 0.05281 mg/Kg 106 70 -130 0 19
1,2-Dichlorobenzene 0.0500 0.05227 mg/Kg 105 70 -134 3 40
1,3-Dichlorobenzene 0.0500 0.05229 mg/Kg 105 69 -137 2 41
1,4-Dichlorobenzene 0.0500 0.05248 mg/Kg 105 66 -134 0 41
Dichlorodifluoromethane 0.0500 0.04571 mg/Kg 91 32 -150 1 50
1,1-Dichloroethane 0.0500 0.05128 mg/Kg 103 70 -130 1 42
1,2-Dichloroethane 0.0500 0.04991 mg/Kg 100 65 -134 2 16
1,1-Dichloroethene 0.0500 0.05041 mg/Kg 101 70 -131 3 43
1,2-Dichloroethene, Total 0.100 0.1019 mg/Kg 102 70 -130 3 41
1,2-Dichloropropane 0.0500 0.05101 mg/Kg 102 70 -130 3 15
1,3-Dichloropropane 0.0500 0.05190 mg/Kg 104 70 -130 1 15
2,2-Dichloropropane 0.0500 0.04993 mg/Kg 100 57 -150 2 42
1,1-Dichloropropene 0.0500 0.05161 mg/Kg 103 70 -130 2 41
Diisopropyl ether 0.0500 0.05055 mg/Kg 101 68 -134 2 36
Ethylbenzene 0.0500 0.05202 mg/Kg 104 70 -130 2 38
Hexachlorobutadiene 0.0500 0.05005 mg/Kg 100 64 -137 2 44
2-Hexanone 0.250 0.2568 mg/Kg 103 47 -148 1 38
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QC Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-350852/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 350852
Isopropylbenzene 0.0500 0.05330 mg/Kg 107 70 -130 2 39
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Methylene Chloride 0.0500 0.05145 mg/Kg 103 69 -130 2 19
4-Methyl-2-pentanone (MIBK)0.250 0.2546 mg/Kg 102 48 -150 2 41
Methyl tert-butyl ether 0.0500 0.05096 mg/Kg 102 54 -145 3 36
Naphthalene 0.0500 0.05252 mg/Kg 105 55 -149 1 37
n-Butylbenzene 0.0500 0.04852 mg/Kg 97 57 -150 5 39
N-Propylbenzene 0.0500 0.05180 mg/Kg 104 62 -150 4 38
p-Isopropyltoluene 0.0500 0.05095 mg/Kg 102 66 -147 2 38
sec-Butylbenzene 0.0500 0.05242 mg/Kg 105 68 -147 1 38
Styrene 0.0500 0.05288 mg/Kg 106 70 -131 1 40
tert-Butylbenzene 0.0500 0.05293 mg/Kg 106 70 -138 2 38
1,1,1,2-Tetrachloroethane 0.0500 0.05294 mg/Kg 106 70 -130 1 41
1,1,2,2-Tetrachloroethane 0.0500 0.05395 mg/Kg 108 61 -134 1 16
Tetrachloroethene 0.0500 0.05175 mg/Kg 104 70 -130 2 41
Toluene 0.0500 0.05204 mg/Kg 104 70 -130 2 40
trans-1,2-Dichloroethene 0.0500 0.05004 mg/Kg 100 70 -130 4 41
trans-1,3-Dichloropropene 0.0500 0.05172 mg/Kg 103 67 -130 1 41
1,2,3-Trichlorobenzene 0.0500 0.05224 mg/Kg 104 57 -146 3 42
1,2,4-Trichlorobenzene 0.0500 0.05127 mg/Kg 103 47 -150 2 43
1,1,1-Trichloroethane 0.0500 0.05096 mg/Kg 102 70 -130 2 41
1,1,2-Trichloroethane 0.0500 0.05148 mg/Kg 103 70 -130 0 17
Trichloroethene 0.0500 0.05492 mg/Kg 110 70 -130 1 41
Trichlorofluoromethane 0.0500 0.04782 mg/Kg 96 53 -150 2 49
1,2,3-Trichloropropane 0.0500 0.05256 mg/Kg 105 60 -139 2 16
1,2,4-Trimethylbenzene 0.0500 0.05151 mg/Kg 103 70 -140 2 38
1,3,5-Trimethylbenzene 0.0500 0.05217 mg/Kg 104 69 -141 2 38
Vinyl chloride 0.0500 0.04980 mg/Kg 100 63 -150 2 46
Xylenes, Total 0.100 0.1036 mg/Kg 104 70 -130 1 38
4-Bromofluorobenzene (Surr)70 -130
Surrogate
99
LCSD LCSD
Qualifier Limits%Recovery
102Dibromofluoromethane (Surr)70 -130
931,2-Dichloroethane-d4 (Surr)70 -130
99Toluene-d8 (Surr)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 490-350878/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 350878
RL MDL
Acetone ND 25.0 ug/L 06/27/16 13:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.00 ug/L 06/27/16 13:17 1Benzene
ND 1.00 ug/L 06/27/16 13:17 1Bromobenzene
ND 1.00 ug/L 06/27/16 13:17 1Bromochloromethane
ND 1.00 ug/L 06/27/16 13:17 1Bromodichloromethane
ND 1.00 ug/L 06/27/16 13:17 1Bromoform
ND 1.00 ug/L 06/27/16 13:17 1Bromomethane
ND 50.0 ug/L 06/27/16 13:17 12-Butanone (MEK)
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QC Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-350878/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 350878
RL MDL
Carbon disulfide ND 1.00 ug/L 06/27/16 13:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.00 ug/L 06/27/16 13:17 1Carbon tetrachloride
ND 1.00 ug/L 06/27/16 13:17 1Chlorobenzene
ND 1.00 ug/L 06/27/16 13:17 1Chlorodibromomethane
ND 1.00 ug/L 06/27/16 13:17 1Chloroethane
ND 1.00 ug/L 06/27/16 13:17 1Chloroform
ND 1.00 ug/L 06/27/16 13:17 1Chloromethane
ND 1.00 ug/L 06/27/16 13:17 12-Chlorotoluene
ND 1.00 ug/L 06/27/16 13:17 14-Chlorotoluene
ND 1.00 ug/L 06/27/16 13:17 1cis-1,2-Dichloroethene
ND 1.00 ug/L 06/27/16 13:17 1cis-1,3-Dichloropropene
ND 10.0 ug/L 06/27/16 13:17 11,2-Dibromo-3-Chloropropane
ND 1.00 ug/L 06/27/16 13:17 11,2-Dibromoethane (EDB)
ND 1.00 ug/L 06/27/16 13:17 1Dibromomethane
ND 1.00 ug/L 06/27/16 13:17 11,2-Dichlorobenzene
ND 1.00 ug/L 06/27/16 13:17 11,3-Dichlorobenzene
ND 1.00 ug/L 06/27/16 13:17 11,4-Dichlorobenzene
ND 1.00 ug/L 06/27/16 13:17 1Dichlorodifluoromethane
ND 1.00 ug/L 06/27/16 13:17 11,1-Dichloroethane
ND 1.00 ug/L 06/27/16 13:17 11,2-Dichloroethane
ND 1.00 ug/L 06/27/16 13:17 11,1-Dichloroethene
ND 1.00 ug/L 06/27/16 13:17 11,2-Dichloroethene, Total
ND 1.00 ug/L 06/27/16 13:17 11,2-Dichloropropane
ND 1.00 ug/L 06/27/16 13:17 11,3-Dichloropropane
ND 1.00 ug/L 06/27/16 13:17 12,2-Dichloropropane
ND 1.00 ug/L 06/27/16 13:17 11,1-Dichloropropene
ND 2.00 ug/L 06/27/16 13:17 1Diisopropyl ether
ND 1.00 ug/L 06/27/16 13:17 1Ethylbenzene
ND 2.00 ug/L 06/27/16 13:17 1Hexachlorobutadiene
ND 10.0 ug/L 06/27/16 13:17 12-Hexanone
ND 1.00 ug/L 06/27/16 13:17 1Isopropylbenzene
ND 5.00 ug/L 06/27/16 13:17 1Methylene Chloride
ND 10.0 ug/L 06/27/16 13:17 14-Methyl-2-pentanone (MIBK)
ND 1.00 ug/L 06/27/16 13:17 1Methyl tert-butyl ether
ND 5.00 ug/L 06/27/16 13:17 1Naphthalene
ND 1.00 ug/L 06/27/16 13:17 1n-Butylbenzene
ND 1.00 ug/L 06/27/16 13:17 1N-Propylbenzene
ND 1.00 ug/L 06/27/16 13:17 1p-Isopropyltoluene
ND 1.00 ug/L 06/27/16 13:17 1sec-Butylbenzene
ND 1.00 ug/L 06/27/16 13:17 1Styrene
ND 1.00 ug/L 06/27/16 13:17 1tert-Butylbenzene
ND 1.00 ug/L 06/27/16 13:17 11,1,1,2-Tetrachloroethane
ND 1.00 ug/L 06/27/16 13:17 11,1,2,2-Tetrachloroethane
ND 1.00 ug/L 06/27/16 13:17 1Tetrachloroethene
ND 1.00 ug/L 06/27/16 13:17 1Toluene
ND 1.00 ug/L 06/27/16 13:17 1trans-1,2-Dichloroethene
ND 1.00 ug/L 06/27/16 13:17 1trans-1,3-Dichloropropene
ND 1.00 ug/L 06/27/16 13:17 11,2,3-Trichlorobenzene
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QC Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-350878/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 350878
RL MDL
1,2,4-Trichlorobenzene ND 1.00 ug/L 06/27/16 13:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.00 ug/L 06/27/16 13:17 11,1,1-Trichloroethane
ND 1.00 ug/L 06/27/16 13:17 11,1,2-Trichloroethane
ND 1.00 ug/L 06/27/16 13:17 1Trichloroethene
ND 1.00 ug/L 06/27/16 13:17 1Trichlorofluoromethane
ND 1.00 ug/L 06/27/16 13:17 11,2,3-Trichloropropane
ND 1.00 ug/L 06/27/16 13:17 11,2,4-Trimethylbenzene
ND 1.00 ug/L 06/27/16 13:17 11,3,5-Trimethylbenzene
ND 1.00 ug/L 06/27/16 13:17 1Vinyl chloride
ND 3.00 ug/L 06/27/16 13:17 1Xylenes, Total
4-Bromofluorobenzene (Surr)90 70-130 06/27/16 13:17 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
99 06/27/16 13:17 1Dibromofluoromethane (Surr)70-130
96 06/27/16 13:17 11,2-Dichloroethane-d4 (Surr)70-130
97 06/27/16 13:17 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-350878/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 350878
Acetone 250 244.9 ug/L 98 39 -150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 50.0 49.27 ug/L 99 70 -130
Bromobenzene 50.0 53.44 ug/L 107 70 -130
Bromochloromethane 50.0 49.53 ug/L 99 70 -130
Bromodichloromethane 50.0 43.68 ug/L 87 70 -130
Bromoform 50.0 54.74 ug/L 109 70 -137
Bromomethane 50.0 30.06 ug/L 60 53 -150
2-Butanone (MEK)250 239.7 ug/L 96 55 -143
Carbon disulfide 50.0 46.38 ug/L 93 64 -135
Carbon tetrachloride 50.0 49.93 ug/L 100 70 -147
Chlorobenzene 50.0 51.87 ug/L 104 70 -130
Chlorodibromomethane 50.0 53.02 ug/L 106 70 -133
Chloroethane 50.0 46.25 ug/L 93 60 -138
Chloroform 50.0 47.69 ug/L 95 70 -130
Chloromethane 50.0 30.76 ug/L 62 33 -150
2-Chlorotoluene 50.0 48.60 ug/L 97 70 -130
4-Chlorotoluene 50.0 48.45 ug/L 97 70 -130
cis-1,2-Dichloroethene 50.0 46.80 ug/L 94 70 -130
cis-1,3-Dichloropropene 50.0 48.93 ug/L 98 70 -133
1,2-Dibromo-3-Chloropropane 50.0 49.32 ug/L 99 45 -138
1,2-Dibromoethane (EDB)50.0 51.41 ug/L 103 70 -130
Dibromomethane 50.0 44.11 ug/L 88 70 -130
1,2-Dichlorobenzene 50.0 53.45 ug/L 107 70 -130
1,3-Dichlorobenzene 50.0 53.36 ug/L 107 70 -130
1,4-Dichlorobenzene 50.0 52.66 ug/L 105 70 -130
Dichlorodifluoromethane 50.0 40.11 ug/L 80 48 -150
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QC Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-350878/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 350878
1,1-Dichloroethane 50.0 48.31 ug/L 97 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dichloroethane 50.0 46.63 ug/L 93 70 -130
1,1-Dichloroethene 50.0 50.73 ug/L 101 70 -132
1,2-Dichloroethene, Total 100 95.32 ug/L 95 70 -130
1,2-Dichloropropane 50.0 43.82 ug/L 88 70 -130
1,3-Dichloropropane 50.0 50.34 ug/L 101 70 -130
2,2-Dichloropropane 50.0 48.41 ug/L 97 60 -143
1,1-Dichloropropene 50.0 48.91 ug/L 98 70 -130
Diisopropyl ether 50.0 48.41 ug/L 97 66 -142
Ethylbenzene 50.0 48.46 ug/L 97 70 -130
Hexachlorobutadiene 50.0 54.08 ug/L 108 70 -138
2-Hexanone 250 244.2 ug/L 98 54 -142
Isopropylbenzene 50.0 49.11 ug/L 98 70 -131
Methylene Chloride 50.0 47.43 ug/L 95 70 -130
4-Methyl-2-pentanone (MIBK)250 249.2 ug/L 100 60 -137
Methyl tert-butyl ether 50.0 49.95 ug/L 100 70 -130
Naphthalene 50.0 47.05 ug/L 94 54 -150
n-Butylbenzene 50.0 49.12 ug/L 98 68 -137
N-Propylbenzene 50.0 47.82 ug/L 96 70 -134
p-Isopropyltoluene 50.0 48.44 ug/L 97 66 -130
sec-Butylbenzene 50.0 48.24 ug/L 96 70 -135
Styrene 50.0 50.69 ug/L 101 70 -130
tert-Butylbenzene 50.0 49.00 ug/L 98 70 -130
1,1,1,2-Tetrachloroethane 50.0 52.78 ug/L 106 70 -130
1,1,2,2-Tetrachloroethane 50.0 48.56 ug/L 97 69 -131
Tetrachloroethene 50.0 54.63 ug/L 109 70 -130
Toluene 50.0 48.59 ug/L 97 70 -130
trans-1,2-Dichloroethene 50.0 48.52 ug/L 97 70 -130
trans-1,3-Dichloropropene 50.0 48.78 ug/L 98 63 -142
1,2,3-Trichlorobenzene 50.0 50.59 ug/L 101 46 -150
1,2,4-Trichlorobenzene 50.0 52.67 ug/L 105 58 -147
1,1,1-Trichloroethane 50.0 47.02 ug/L 94 70 -135
1,1,2-Trichloroethane 50.0 50.11 ug/L 100 70 -130
Trichloroethene 50.0 45.55 ug/L 91 70 -130
Trichlorofluoromethane 50.0 49.27 ug/L 99 59 -150
1,2,3-Trichloropropane 50.0 46.05 ug/L 92 70 -131
1,2,4-Trimethylbenzene 50.0 47.70 ug/L 95 70 -130
1,3,5-Trimethylbenzene 50.0 48.64 ug/L 97 70 -130
Vinyl chloride 50.0 48.47 ug/L 97 57 -137
Xylenes, Total 100 97.60 ug/L 98 70 -132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
91
LCS LCS
Qualifier Limits%Recovery
98Dibromofluoromethane (Surr)70 -130
921,2-Dichloroethane-d4 (Surr)70 -130
99Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-350878/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 350878
Acetone 250 237.3 ug/L 95 39 -150 3 23
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 50.0 50.14 ug/L 100 70 -130 2 12
Bromobenzene 50.0 54.25 ug/L 109 70 -130 2 16
Bromochloromethane 50.0 50.13 ug/L 100 70 -130 1 16
Bromodichloromethane 50.0 44.35 ug/L 89 70 -130 2 14
Bromoform 50.0 55.87 ug/L 112 70 -137 2 14
Bromomethane 50.0 33.33 ug/L 67 53 -150 10 19
2-Butanone (MEK)250 235.7 ug/L 94 55 -143 2 19
Carbon disulfide 50.0 47.51 ug/L 95 64 -135 2 16
Carbon tetrachloride 50.0 50.54 ug/L 101 70 -147 1 16
Chlorobenzene 50.0 52.59 ug/L 105 70 -130 1 12
Chlorodibromomethane 50.0 53.47 ug/L 107 70 -133 1 13
Chloroethane 50.0 46.94 ug/L 94 60 -138 1 15
Chloroform 50.0 49.97 ug/L 100 70 -130 5 14
Chloromethane 50.0 31.08 ug/L 62 33 -150 1 20
2-Chlorotoluene 50.0 51.30 ug/L 103 70 -130 5 15
4-Chlorotoluene 50.0 49.63 ug/L 99 70 -130 2 15
cis-1,2-Dichloroethene 50.0 47.73 ug/L 95 70 -130 2 15
cis-1,3-Dichloropropene 50.0 48.93 ug/L 98 70 -133 0 15
1,2-Dibromo-3-Chloropropane 50.0 50.48 ug/L 101 45 -138 2 19
1,2-Dibromoethane (EDB)50.0 52.18 ug/L 104 70 -130 1 13
Dibromomethane 50.0 44.70 ug/L 89 70 -130 1 14
1,2-Dichlorobenzene 50.0 54.88 ug/L 110 70 -130 3 12
1,3-Dichlorobenzene 50.0 54.43 ug/L 109 70 -130 2 13
1,4-Dichlorobenzene 50.0 53.60 ug/L 107 70 -130 2 12
Dichlorodifluoromethane 50.0 40.89 ug/L 82 48 -150 2 16
1,1-Dichloroethane 50.0 48.82 ug/L 98 70 -130 1 17
1,2-Dichloroethane 50.0 46.81 ug/L 94 70 -130 0 13
1,1-Dichloroethene 50.0 52.17 ug/L 104 70 -132 3 20
1,2-Dichloroethene, Total 100 96.73 ug/L 97 70 -130 1 14
1,2-Dichloropropane 50.0 46.85 ug/L 94 70 -130 7 15
1,3-Dichloropropane 50.0 50.60 ug/L 101 70 -130 0 12
2,2-Dichloropropane 50.0 48.65 ug/L 97 60 -143 1 20
1,1-Dichloropropene 50.0 49.49 ug/L 99 70 -130 1 16
Diisopropyl ether 50.0 48.91 ug/L 98 66 -142 1 14
Ethylbenzene 50.0 49.39 ug/L 99 70 -130 2 12
Hexachlorobutadiene 50.0 56.66 ug/L 113 70 -138 5 16
2-Hexanone 250 244.2 ug/L 98 54 -142 0 17
Isopropylbenzene 50.0 50.12 ug/L 100 70 -131 2 13
Methylene Chloride 50.0 48.08 ug/L 96 70 -130 1 15
4-Methyl-2-pentanone (MIBK)250 248.2 ug/L 99 60 -137 0 21
Methyl tert-butyl ether 50.0 50.46 ug/L 101 70 -130 1 16
Naphthalene 50.0 47.92 ug/L 96 54 -150 2 15
n-Butylbenzene 50.0 50.12 ug/L 100 68 -137 2 14
N-Propylbenzene 50.0 48.80 ug/L 98 70 -134 2 14
p-Isopropyltoluene 50.0 49.53 ug/L 99 66 -130 2 13
sec-Butylbenzene 50.0 49.24 ug/L 98 70 -135 2 14
Styrene 50.0 51.34 ug/L 103 70 -130 1 12
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QC Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-350878/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 350878
tert-Butylbenzene 50.0 49.95 ug/L 100 70 -130 2 14
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1,1,2-Tetrachloroethane 50.0 52.87 ug/L 106 70 -130 0 13
1,1,2,2-Tetrachloroethane 50.0 49.78 ug/L 100 69 -131 2 15
Tetrachloroethene 50.0 54.62 ug/L 109 70 -130 0 17
Toluene 50.0 49.17 ug/L 98 70 -130 1 13
trans-1,2-Dichloroethene 50.0 49.00 ug/L 98 70 -130 1 15
trans-1,3-Dichloropropene 50.0 49.14 ug/L 98 63 -142 1 13
1,2,3-Trichlorobenzene 50.0 52.67 ug/L 105 46 -150 4 16
1,2,4-Trichlorobenzene 50.0 54.20 ug/L 108 58 -147 3 15
1,1,1-Trichloroethane 50.0 48.00 ug/L 96 70 -135 2 15
1,1,2-Trichloroethane 50.0 50.56 ug/L 101 70 -130 1 13
Trichloroethene 50.0 45.64 ug/L 91 70 -130 0 14
Trichlorofluoromethane 50.0 50.43 ug/L 101 59 -150 2 22
1,2,3-Trichloropropane 50.0 47.08 ug/L 94 70 -131 2 14
1,2,4-Trimethylbenzene 50.0 48.23 ug/L 96 70 -130 1 13
1,3,5-Trimethylbenzene 50.0 49.53 ug/L 99 70 -130 2 14
Vinyl chloride 50.0 49.84 ug/L 100 57 -137 3 15
Xylenes, Total 100 99.04 ug/L 99 70 -132 1 11
4-Bromofluorobenzene (Surr)70 -130
Surrogate
92
LCSD LCSD
Qualifier Limits%Recovery
97Dibromofluoromethane (Surr)70 -130
911,2-Dichloroethane-d4 (Surr)70 -130
98Toluene-d8 (Surr)70 -130
Client Sample ID: GP-5Lab Sample ID: 490-106464-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 350878
Acetone ND 250 213.7 ug/L 85 39 -150
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Benzene ND 50.0 49.42 ug/L 99 55 -147
Bromobenzene ND 50.0 50.04 ug/L 100 60 -133
Bromochloromethane ND 50.0 48.42 ug/L 97 59 -132
Bromodichloromethane ND 50.0 43.26 ug/L 87 70 -140
Bromoform ND 50.0 50.60 ug/L 101 53 -150
Bromomethane ND 50.0 21.26 ug/L 43 30 -150
2-Butanone (MEK)ND 250 217.3 ug/L 87 50 -143
Carbon disulfide ND 50.0 46.12 ug/L 92 35 -150
Carbon tetrachloride ND 50.0 49.81 ug/L 100 56 -150
Chlorobenzene ND 50.0 50.55 ug/L 101 70 -130
Chlorodibromomethane ND 50.0 49.29 ug/L 99 66 -140
Chloroethane ND 50.0 45.04 ug/L 90 58 -141
Chloroform ND 50.0 47.16 ug/L 94 66 -138
Chloromethane ND 50.0 27.93 ug/L 56 10 -150
2-Chlorotoluene ND 50.0 45.34 ug/L 91 67 -138
4-Chlorotoluene ND 50.0 46.33 ug/L 93 69 -138
cis-1,2-Dichloroethene 8.73 50.0 53.86 ug/L 90 68 -131
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QC Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: GP-5Lab Sample ID: 490-106464-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 350878
cis-1,3-Dichloropropene ND 50.0 43.00 ug/L 86 70 -133
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,2-Dibromo-3-Chloropropane ND 50.0 42.95 ug/L 86 38 -138
1,2-Dibromoethane (EDB)ND 50.0 45.47 ug/L 91 65 -137
Dibromomethane ND 50.0 41.63 ug/L 83 70 -130
1,2-Dichlorobenzene ND 50.0 49.82 ug/L 100 70 -130
1,3-Dichlorobenzene ND 50.0 50.07 ug/L 100 68 -131
1,4-Dichlorobenzene ND 50.0 49.58 ug/L 99 70 -130
Dichlorodifluoromethane ND 50.0 34.84 ug/L 70 10 -150
1,1-Dichloroethane ND 50.0 46.82 ug/L 94 61 -139
1,2-Dichloroethane ND 50.0 44.58 ug/L 89 64 -136
1,1-Dichloroethene ND 50.0 50.84 ug/L 102 54 -150
1,2-Dichloroethene, Total 8.73 100 100.3 ug/L 92 60 -134
1,2-Dichloropropane ND 50.0 46.56 ug/L 93 67 -130
1,3-Dichloropropane ND 50.0 45.30 ug/L 91 70 -130
2,2-Dichloropropane ND 50.0 44.78 ug/L 90 50 -146
1,1-Dichloropropene ND 50.0 47.36 ug/L 95 54 -150
Diisopropyl ether ND 50.0 45.65 ug/L 91 56 -142
Ethylbenzene ND 50.0 47.05 ug/L 94 65 -139
Hexachlorobutadiene ND 50.0 48.91 ug/L 98 61 -141
2-Hexanone ND 250 202.9 ug/L 81 44 -150
Isopropylbenzene ND 50.0 48.22 ug/L 96 70 -137
Methylene Chloride ND 50.0 45.49 ug/L 91 64 -130
4-Methyl-2-pentanone (MIBK)ND 250 208.0 ug/L 83 50 -140
Methyl tert-butyl ether ND 50.0 45.17 ug/L 90 55 -141
Naphthalene ND 50.0 39.25 ug/L 78 32 -150
n-Butylbenzene ND 50.0 46.08 ug/L 92 61 -141
N-Propylbenzene ND 50.0 45.63 ug/L 91 53 -150
p-Isopropyltoluene ND 50.0 46.06 ug/L 92 66 -137
sec-Butylbenzene ND 50.0 45.89 ug/L 92 55 -136
Styrene ND 50.0 49.90 ug/L 100 70 -130
tert-Butylbenzene ND 50.0 46.10 ug/L 92 70 -138
1,1,1,2-Tetrachloroethane ND 50.0 49.31 ug/L 99 70 -131
1,1,2,2-Tetrachloroethane ND 50.0 44.06 ug/L 88 56 -145
Tetrachloroethene 10.7 50.0 60.14 ug/L 99 57 -138
Toluene ND 50.0 47.09 ug/L 93 64 -136
trans-1,2-Dichloroethene ND 50.0 46.45 ug/L 93 59 -143
trans-1,3-Dichloropropene ND 50.0 42.77 ug/L 86 63 -142
1,2,3-Trichlorobenzene ND 50.0 41.45 ug/L 83 36 -150
1,2,4-Trichlorobenzene ND 50.0 43.88 ug/L 88 47 -147
1,1,1-Trichloroethane ND 50.0 46.51 ug/L 93 68 -144
1,1,2-Trichloroethane ND 50.0 46.14 ug/L 92 70 -130
Trichloroethene 2.26 50.0 47.06 ug/L 90 63 -135
Trichlorofluoromethane ND 50.0 49.16 ug/L 98 44 -150
1,2,3-Trichloropropane ND 50.0 43.69 ug/L 87 65 -131
1,2,4-Trimethylbenzene ND 50.0 45.20 ug/L 90 64 -136
1,3,5-Trimethylbenzene ND 50.0 46.86 ug/L 94 69 -139
Vinyl chloride ND 50.0 46.32 ug/L 93 57 -150
Xylenes, Total ND 100 95.12 ug/L 95 69 -132
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QC Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: GP-5Lab Sample ID: 490-106464-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 350878
4-Bromofluorobenzene (Surr)70 -130
Surrogate
88
MS MS
Qualifier Limits%Recovery
99Dibromofluoromethane (Surr)70 -130
921,2-Dichloroethane-d4 (Surr)70 -130
92Toluene-d8 (Surr)70 -130
Client Sample ID: GP-5Lab Sample ID: 490-106464-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 350878
Acetone ND 250 245.1 ug/L 98 39 -150 14 28
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Benzene ND 50.0 53.54 ug/L 107 55 -147 8 22
Bromobenzene ND 50.0 55.80 ug/L 112 60 -133 11 18
Bromochloromethane ND 50.0 52.89 ug/L 106 59 -132 9 21
Bromodichloromethane ND 50.0 45.07 ug/L 90 70 -140 4 196
Bromoform ND 50.0 57.18 ug/L 114 53 -150 12 20
Bromomethane ND 50.0 31.72 ug/L 63 30 -150 39 44
2-Butanone (MEK)ND 250 244.9 ug/L 98 50 -143 12 28
Carbon disulfide ND 50.0 48.67 ug/L 97 35 -150 5 34
Carbon tetrachloride ND 50.0 54.78 ug/L 110 56 -150 10 18
Chlorobenzene ND 50.0 55.39 ug/L 111 70 -130 9 15
Chlorodibromomethane ND 50.0 55.02 ug/L 110 66 -140 11 19
Chloroethane ND 50.0 50.00 ug/L 100 58 -141 10 31
Chloroform ND 50.0 51.80 ug/L 104 66 -138 9 21
Chloromethane ND 50.0 28.52 ug/L 57 10 -150 2 43
2-Chlorotoluene ND 50.0 50.09 ug/L 100 67 -138 10 17
4-Chlorotoluene ND 50.0 50.92 ug/L 102 69 -138 9 15
cis-1,2-Dichloroethene 8.73 50.0 57.10 ug/L 97 68 -131 6 21
cis-1,3-Dichloropropene ND 50.0 48.32 ug/L 97 70 -133 12 19
1,2-Dibromo-3-Chloropropane ND 50.0 51.73 ug/L 103 38 -138 19 26
1,2-Dibromoethane (EDB)ND 50.0 51.64 ug/L 103 65 -137 13 21
Dibromomethane ND 50.0 45.92 ug/L 92 70 -130 10 19
1,2-Dichlorobenzene ND 50.0 55.57 ug/L 111 70 -130 11 15
1,3-Dichlorobenzene ND 50.0 55.29 ug/L 111 68 -131 10 14
1,4-Dichlorobenzene ND 50.0 54.76 ug/L 110 70 -130 10 14
Dichlorodifluoromethane ND 50.0 39.54 ug/L 79 10 -150 13 50
1,1-Dichloroethane ND 50.0 51.84 ug/L 104 61 -139 10 23
1,2-Dichloroethane ND 50.0 49.03 ug/L 98 64 -136 10 22
1,1-Dichloroethene ND 50.0 56.01 ug/L 112 54 -150 10 24
1,2-Dichloroethene, Total 8.73 100 108.5 ug/L 100 60 -134 8 22
1,2-Dichloropropane ND 50.0 51.25 ug/L 103 67 -130 10 19
1,3-Dichloropropane ND 50.0 50.90 ug/L 102 70 -130 12 17
2,2-Dichloropropane ND 50.0 48.83 ug/L 98 50 -146 9 20
1,1-Dichloropropene ND 50.0 52.41 ug/L 105 54 -150 10 24
Diisopropyl ether ND 50.0 50.73 ug/L 101 56 -142 11 22
Ethylbenzene ND 50.0 51.92 ug/L 104 65 -139 10 18
Hexachlorobutadiene ND 50.0 55.19 ug/L 110 61 -141 12 26
2-Hexanone ND 250 237.1 ug/L 95 44 -150 16 21
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QC Sample Results
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: GP-5Lab Sample ID: 490-106464-5 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 350878
Isopropylbenzene ND 50.0 52.99 ug/L 106 70 -137 9 17
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Methylene Chloride ND 50.0 50.63 ug/L 101 64 -130 11 22
4-Methyl-2-pentanone (MIBK)ND 250 241.1 ug/L 96 50 -140 15 24
Methyl tert-butyl ether ND 50.0 51.43 ug/L 103 55 -141 13 24
Naphthalene ND 50.0 46.42 ug/L 93 32 -150 17 40
n-Butylbenzene ND 50.0 50.56 ug/L 101 61 -141 9 17
N-Propylbenzene ND 50.0 50.05 ug/L 100 53 -150 9 18
p-Isopropyltoluene ND 50.0 50.40 ug/L 101 66 -137 9 16
sec-Butylbenzene ND 50.0 50.53 ug/L 101 55 -136 10 50
Styrene ND 50.0 54.36 ug/L 109 70 -130 9 16
tert-Butylbenzene ND 50.0 51.09 ug/L 102 70 -138 10 17
1,1,1,2-Tetrachloroethane ND 50.0 54.63 ug/L 109 70 -131 10 16
1,1,2,2-Tetrachloroethane ND 50.0 50.74 ug/L 101 56 -145 14 19
Tetrachloroethene 10.7 50.0 66.40 ug/L 111 57 -138 10 17
Toluene ND 50.0 51.76 ug/L 102 64 -136 9 18
trans-1,2-Dichloroethene ND 50.0 51.37 ug/L 103 59 -143 10 25
trans-1,3-Dichloropropene ND 50.0 48.40 ug/L 97 63 -142 12 18
1,2,3-Trichlorobenzene ND 50.0 49.90 ug/L 100 36 -150 19 43
1,2,4-Trichlorobenzene ND 50.0 51.05 ug/L 102 47 -147 15 24
1,1,1-Trichloroethane ND 50.0 52.74 ug/L 105 68 -144 13 17
1,1,2-Trichloroethane ND 50.0 51.39 ug/L 103 70 -130 11 18
Trichloroethene 2.26 50.0 51.07 ug/L 98 63 -135 8 17
Trichlorofluoromethane ND 50.0 54.83 ug/L 110 44 -150 11 32
1,2,3-Trichloropropane ND 50.0 48.65 ug/L 97 65 -131 11 19
1,2,4-Trimethylbenzene ND 50.0 49.71 ug/L 99 64 -136 10 18
1,3,5-Trimethylbenzene ND 50.0 51.34 ug/L 103 69 -139 9 17
Vinyl chloride ND 50.0 51.25 ug/L 102 57 -150 10 37
Xylenes, Total ND 100 105.0 ug/L 105 69 -132 10 17
4-Bromofluorobenzene (Surr)70 -130
Surrogate
90
MSD MSD
Qualifier Limits%Recovery
98Dibromofluoromethane (Surr)70 -130
931,2-Dichloroethane-d4 (Surr)70 -130
94Toluene-d8 (Surr)70 -130
Method: Moisture - Percent Moisture
Client Sample ID: DuplicateLab Sample ID: 490-106456-C-2 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 350765
Percent Solids 75.0 75.5 %
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
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QC Association Summary
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
GC/MS VOA
Analysis Batch: 350852
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260B 350883490-106464-1 GP-7 (0-1)Total/NA
Soil 8260B 350883490-106464-2 GP-7 (4-5)Total/NA
Soil 8260B 350883490-106464-3 GP-8 (0-1)Total/NA
Soil 8260B 350883490-106464-4 GP-8 (4-5)Total/NA
Solid 8260BLCS 490-350852/4 Lab Control Sample Total/NA
Solid 8260BLCSD 490-350852/5 Lab Control Sample Dup Total/NA
Solid 8260BMB 490-350852/7 Method Blank Total/NA
Analysis Batch: 350878
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-106464-5 GP-5 Total/NA
Water 8260B490-106464-5 MS GP-5 Total/NA
Water 8260B490-106464-5 MSD GP-5 Total/NA
Water 8260B490-106464-6 GP-6 Total/NA
Water 8260B490-106464-7 GP-7 Total/NA
Water 8260B490-106464-8 GP-8 Total/NA
Water 8260B490-106464-9 GP-9 Total/NA
Water 8260B490-106464-10 Trip Blank Total/NA
Water 8260BLCS 490-350878/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-350878/4 Lab Control Sample Dup Total/NA
Water 8260BMB 490-350878/6 Method Blank Total/NA
Prep Batch: 350883
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 5035490-106464-1 GP-7 (0-1)Total/NA
Soil 5035490-106464-2 GP-7 (4-5)Total/NA
Soil 5035490-106464-3 GP-8 (0-1)Total/NA
Soil 5035490-106464-4 GP-8 (4-5)Total/NA
General Chemistry
Analysis Batch: 350765
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture490-106456-C-1 MS Matrix Spike Total/NA
Solid Moisture490-106456-C-1 MSD Matrix Spike Duplicate Total/NA
Solid Moisture490-106456-C-2 DU Duplicate Total/NA
Soil Moisture490-106464-1 GP-7 (0-1)Total/NA
Soil Moisture490-106464-2 GP-7 (4-5)Total/NA
Soil Moisture490-106464-3 GP-8 (0-1)Total/NA
Soil Moisture490-106464-4 GP-8 (4-5)Total/NA
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-106464-1
Project/Site: Carolina Freightliner SDG: TPP-001
Client Sample ID: GP-7 (0-1)Lab Sample ID: 490-106464-1
Matrix: SoilDate Collected: 06/21/16 13:55
Date Received: 06/24/16 09:50
Analysis Moisture AAB06/26/16 11:481 TAL NSH350765
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: GP-7 (0-1)Lab Sample ID: 490-106464-1
Matrix: SoilDate Collected: 06/21/16 13:55
Percent Solids: 83.7Date Received: 06/24/16 09:50
Prep 5035 JLP06/21/16 13:55 TAL NSH350883
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.857 g 5.0 mL
Analysis 8260B 1 350852 06/27/16 17:19 EML TAL NSHTotal/NA 4.857 g 5.0 mL
Client Sample ID: GP-7 (4-5)Lab Sample ID: 490-106464-2
Matrix: SoilDate Collected: 06/21/16 14:05
Date Received: 06/24/16 09:50
Analysis Moisture AAB06/26/16 11:481 TAL NSH350765
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: GP-7 (4-5)Lab Sample ID: 490-106464-2
Matrix: SoilDate Collected: 06/21/16 14:05
Percent Solids: 83.4Date Received: 06/24/16 09:50
Prep 5035 JLP06/21/16 14:05 TAL NSH350883
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.813 g 5.0 mL
Analysis 8260B 1 350852 06/27/16 17:46 EML TAL NSHTotal/NA 5.813 g 5.0 mL
Client Sample ID: GP-8 (0-1)Lab Sample ID: 490-106464-3
Matrix: SoilDate Collected: 06/21/16 15:40
Date Received: 06/24/16 09:50
Analysis Moisture AAB06/26/16 11:481 TAL NSH350765
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: GP-8 (0-1)Lab Sample ID: 490-106464-3
Matrix: SoilDate Collected: 06/21/16 15:40
Percent Solids: 67.9Date Received: 06/24/16 09:50
Prep 5035 JLP06/21/16 15:40 TAL NSH350883
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.167 g 5.0 mL
Analysis 8260B 1 350852 06/27/16 18:14 EML TAL NSHTotal/NA 6.167 g 5.0 mL
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-106464-1
Project/Site: Carolina Freightliner SDG: TPP-001
Client Sample ID: GP-8 (4-5)Lab Sample ID: 490-106464-4
Matrix: SoilDate Collected: 06/21/16 15:45
Date Received: 06/24/16 09:50
Analysis Moisture AAB06/26/16 11:481 TAL NSH350765
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: GP-8 (4-5)Lab Sample ID: 490-106464-4
Matrix: SoilDate Collected: 06/21/16 15:45
Percent Solids: 79.8Date Received: 06/24/16 09:50
Prep 5035 JLP06/21/16 14:45 TAL NSH350883
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.142 g 5.0 mL
Analysis 8260B 1 350852 06/27/16 18:41 EML TAL NSHTotal/NA 5.142 g 5.0 mL
Client Sample ID: GP-5 Lab Sample ID: 490-106464-5
Matrix: WaterDate Collected: 06/22/16 09:45
Date Received: 06/24/16 09:50
Analysis 8260B RP06/27/16 14:351 TAL NSH350878
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Client Sample ID: GP-6 Lab Sample ID: 490-106464-6
Matrix: WaterDate Collected: 06/22/16 10:30
Date Received: 06/24/16 09:50
Analysis 8260B RP06/27/16 15:011 TAL NSH350878
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Client Sample ID: GP-7 Lab Sample ID: 490-106464-7
Matrix: WaterDate Collected: 06/22/16 12:30
Date Received: 06/24/16 09:50
Analysis 8260B RP06/27/16 15:281 TAL NSH350878
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Client Sample ID: GP-8 Lab Sample ID: 490-106464-8
Matrix: WaterDate Collected: 06/22/16 11:35
Date Received: 06/24/16 09:50
Analysis 8260B RP06/27/16 15:541 TAL NSH350878
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-106464-1
Project/Site: Carolina Freightliner SDG: TPP-001
Client Sample ID: GP-9 Lab Sample ID: 490-106464-9
Matrix: WaterDate Collected: 06/22/16 08:55
Date Received: 06/24/16 09:50
Analysis 8260B RP06/27/16 16:201 TAL NSH350878
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Client Sample ID: Trip Blank Lab Sample ID: 490-106464-10
Matrix: WaterDate Collected: 06/22/16 01:01
Date Received: 06/24/16 09:50
Analysis 8260B RP06/27/16 14:091 TAL NSH350878
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Method Summary
TestAmerica Job ID: 490-106464-1Client: Hart & Hickman, PC
SDG: TPP-001Project/Site: Carolina Freightliner
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
EPAMoisturePercent Moisture TAL NSH
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Certification Summary
Client: Hart & Hickman, PC TestAmerica Job ID: 490-106464-1
Project/Site: Carolina Freightliner SDG: TPP-001
Laboratory: TestAmerica Nashville
Unless otherwise noted, all analytes for this laboratory were covered under each certification below.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-16
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but certification is not offered by the governing authority:
Moisture Soil Percent Solids
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Login Sample Receipt Checklist
Client: Hart & Hickman, PC Job Number: 490-106464-1
SDG Number: TPP-001
Login Number: 106464
Question Answer Comment
Creator: McBride, Mike
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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