Silverman_Soil_and_GW_Assessment_-FINAL_ (1)-OCR

SOIL AND GROUNDWATER
ASSESSMENT REPORT
SILVERMAN PROPERTY
48 SWANNANOA RIVER ROAD
ASHEVILLE, NORTH CAROLINA
S&ME Project No. 1411-09-025
Brownfields Project No. 12020-08-011

Prepared for:
Awenasa, LLC
P.O. Box 2326
Asheville, North Carolina 28802

Prepared by:

44 Buck Shoals Road, Suite C-3
Arden, North Carolina 28704

August 25, 2009

August 25, 2009

Awenasa, LLC
P.O. Box 2326
Asheville, North Carolina 28802

Attention: Mr. David Madera

Reference: Soil and Groundwater Assessment Report
Silverman Property
48 Swannanoa River Road
Asheville, North Carolina
S&ME Project No. 1411-09-025
Brownfields Project No. 12020-08-11

Dear Mr. Madera:

S&ME, Inc. has completed the soil and groundwater assessment activities at the property
known as Silverman Property addressed at 48 Swannanoa River Road in Asheville, North
Carolina in general accordance with S&ME Proposal No. ENV-258-08 Rev 2 dated
March 12, 2009. The assessment activities were performed to determine if groundwater,
surface soil, and sub-surface soil contamination on-site poses a threat to human health
and the environment if the site is redeveloped for mixed use including residential, retail,
office, community/open space, and parking. Two (2) copies of this report were provided
to:

U.S. EPA Region 4
RCRA Division, Restoration and Underground
Storage Tank Branch
61 Forsyth Street, SW
Atlanta, GA 30303
Attention: Ms. Wanda Jennings, Brownfields Project Manager

One (1) copy of this report was provided to:

North Carolina Department of Environment and Natural Resources
Division of Waste Management
Asheville Office
c/o Land of Sky Regional Council
339 New Leicester Highway, Suite 140
Asheville, North Carolina 28806
Attention: Ms. Tracy Wahl, Brownfields Project Manager
1

TABLE OF CONTENTS
1. BACKGROUND........................................................................................................ 1
1.1 Site Information .................................................................................................. 1
1.2 Project History .................................................................................................... 1
1.2.1 Phase I Environmental Site Assessment (September 2007)............... 1
1.2.2 Brownfields Assessment Activities .................................................... 2
2. SOIL ASSESSMENT ACTIVITIES........................................................................ 3
2.1 Sandblasting Booth ............................................................................................. 3
2.1.1 Field Activities.................................................................................... 3
2.1.2 Laboratory Results .............................................................................. 4
2.2 Paint Mixing Room............................................................................................. 4
2.2.1 Field Activities.................................................................................... 4
2.2.2 Laboratory Results .............................................................................. 4
2.3 Outdoor Painting Area and Breezeway............................................................... 5
2.3.1 Field Activities.................................................................................... 5
2.3.2 Laboratory Results .............................................................................. 5
2.4 Machine Shop ..................................................................................................... 6
2.4.1 Field Activities.................................................................................... 6
2.4.2 Laboratory Results .............................................................................. 6
2.5 Fabrication Building ........................................................................................... 6
2.5.1 Field Activities.................................................................................... 6
2.5.2 Laboratory Results .............................................................................. 7
2.6 Potential Underground Storage Tanks ................................................................ 7
2.6.1 Field Activities.................................................................................... 7
2.6.2 Laboratory Results .............................................................................. 9
2.7 Debris Piles ......................................................................................................... 9
2.7.1 Field Activities.................................................................................... 9
2.7.2 Laboratory Results .............................................................................. 9
2.8 Go-Cart Track ................................................................................................... 10
2.8.1 Field Activities.................................................................................. 10
2.8.2 Laboratory Results ............................................................................ 11
2.9 Soil Sampling Techniques ................................................................................ 11
2.9.1 Near Surface Soil Sampling.............................................................. 11
2.9.2 Subsurface Soil Sampling ................................................................. 11
2.10 Quality Control ................................................................................................. 12
2.10.1 Sampling Equipment......................................................................... 12
2.10.2 Duplicate Samples ............................................................................ 13
2.10.3 Trip Blanks........................................................................................ 13
2.10.4 Investigation-Derived Wastes........................................................... 14
3. GROUNDWATER ASSESSMENT ....................................................................... 14
3.1 Temporary Wells .............................................................................................. 14
3.1.1 Field Activities.................................................................................. 14
3.1.2 Groundwater Sampling Methods ...................................................... 15
3.1.3 Laboratory Results ............................................................................ 16
3.2 Quality Control ................................................................................................. 16
i

ii
3.2.1 Sampling Equipment......................................................................... 16
3.2.2 Duplicate Samples ............................................................................ 17
3.2.3 Trip Blanks........................................................................................ 17
3.2.4 Field Blanks ...................................................................................... 17
3.4 Investigation-Derived Wastes........................................................................... 17
3.5 Groundwater Flow ............................................................................................ 18
4. CONCLUSIONS AND RECOMMENDATIONS ................................................ 18
4.1 UST East of Former Paint Booth ...................................................................... 18
4.2 Gasoline Tank on Sanborn Maps...................................................................... 18
4.3 Sandblasting Booth ........................................................................................... 18
4.4 Outdoor Painting Area, Machine Shop, and Breezeway .................................. 19
4.5 Areas of Impacted Soil...................................................................................... 19
4.6 Additional Assessment Locations..................................................................... 22
5. SOLE USE STATEMENT...................................................................................... 22
APPENDIX I ......................................................................................................................I
APPENDIX II...................................................................................................................II
APPENDIX III ................................................................................................................III
APPENDIX IV ................................................................................................................IV
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road - Asheville, NC August 25, 2009

1
1. BACKGROUND
1.1 Site Information
The subject property (subject site; the site) is located northwest of the intersection of
Swannanoa River Road and Caledonia Road in the City of Asheville, Buncombe County,
North Carolina. The approximate location of the site is indicated on Figure 1. Two
parcels comprise the subject property covering a total of approximately 4.19 acres. The
parcels are currently owned by David Madera. A portion of the former fabrication building
on the property is currently being utilized as office space. The property is identified as
Silverman Property and is being considered for mixed use redevelopment by the current
owner.
1.2 Project History
The subject property was historically utilized as a scrap yard and metal fabrication
facility. The following is a summary of the assessment activities that have been
conducted in association with the subject site:
1.2.1 Phase I Environmental Site Assessment (September 2007)
In September 2007, under contract with Silverman Company, a Phase I Environmental
Site Assessment (ESA) was performed for the subject property by Mountain
Environmental Services, Inc. (Mountain). The Phase I ESA identified:

• an inactive 550 gallon underground heating oil tank adjacent to the repair shop,

• the previous use of the property as a scrap yard,

• three above-ground petroleum storage tanks (ASTs) without secondary
containment,

• soil staining at various locations around the site,

• a battery servicing operation and outdoor battery storage area,

• the potential presence of asbestos containing materials within the apartment
onsite, and

• the site was flooded in 2004.

Mountain recommended a Phase II ESA be performed including the collection of soil
samples in the vicinity of the underground heating oil tank, in the vicinity of the old paint
booth and outdoor painting areas, in the vicinity of the battery operation, and from
beneath the inactive vehicles onsite. Mountain also recommended providing concrete
containment beneath the three active petroleum tanks and obtaining ceiling tile and
sheetrock samples from the apartment and office building to analyze for asbestos content.
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

2
1.2.2 Brownfields Assessment Activities
On July 9, 2008, a Brownfields Property Application to enter into a Brownfields
Agreement was submitted to the Brownfields Program of the North Carolina Department
of Environment and Natural Resources (NCDENR) Division of Waste Management. The
subject site was determined to be eligible to enter into the Brownfields Program by
NCDENR to work towards obtaining a Brownfields Agreement.

In October 2008, under contract with the Land of Sky Regional Council (LOSRC),
S&ME performed a (1) Phase I ESA and (2) Brownfields Area Reconnaissance and
Receptor Survey in association with the subject property. The Phase I ESA and Receptor
Survey were performed in general accordance with S&ME Proposal No. ENV-153-08
dated June 30, 2008.

The Phase I ESA identified the following recognized environmental conditions (RECs) in
association with the subject property:

• The gasoline tank(s) formerly located on the northwest corner of the storage
building.

• The potential UST located adjacent to the five-bay garage located on the northern
portion of the property.

• The potential UST or former fuel dispenser located near the northeast corner of
the fabrication building.

• The paint mixing room with a dirt floor located on the northwest corner of the
fabrication building.

• A fill port and vent pipe indicative of a UST adjacent to the east side of the
paint booth.

• The sandblasting booth located onsite.

• The stained soil associated with the former location of an air compressor adjacent
to the northeast corner of the sandblasting booth.

• The floor drain system with drains located in the fabrication building, the
breezeway between the fabrication building and the shop, and in the shop.

• Floor staining located at two locations within the fabrication building.

• The priming/painting area under the metal canopy north of the fabrication
building.

• The former presence of a blacksmith shop and machine shop on the property.

Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

3
The Site Plan showing the layout of the features on the property is included as Figure 2.

S&ME completed the Work Plan for Soil and Groundwater Assessment dated April 1,
2009. The work plan was approval was received on April 16, 2009. S&ME completed
the Draft - Quality Assurance Project Plan (QAPP) dated May 18, 2009. On June 23,
2009, S&ME received QAPP approval and comments via electronic mail from Wanda
Jennings, EPA Region 4 Brownfields Coordinator. Ms. Jennings identified four
comments in her June 23rd electronic mail correspondence. On June 26, 2009, S&ME
completed and submitted the QAPP Revision 1, addressing the four comments in Ms.
Jennings June 23rd electronic mail correspondence.

The soil and groundwater assessment activities were performed in general accordance
with the approved Work Plan and QAPP.
2. SOIL ASSESSMENT ACTIVITIES
2.1 Sandblasting Booth
2.1.1 Field Activities
On June 30, 2009 S&ME collected near surface soil samples from three (3) locations
adjacent to the former sandblasting booth onsite. Two (2) of the soil samples were
collected on the south side of the former sandblasting booth, where during the site
reconnaissance, and associated with the booth was observed outside of the booth on the
bare ground. One (1) of the soil samples was collected on the northeast corner of the
sandblasting booth where a permanent air compressor was formerly located. Soil sample
locations were triangulated and mapped using a tape measure and hardscape features on
the property. The soil sample locations are labeled SB1, SB2, and SB3 on Figure 3. For
ease of reading and reporting, sample names were abbreviated. Example, we are
referring to sample SILV-SB1-06-09 as SB1. The soil samples were collected using a
decontaminated stainless steel hand auger. The procedure utilized for collecting the soil
samples is outlined in Section 2.9.1. Trip blank, equipment blank, and duplicate samples
were collected to provide the necessary quality control.

Soil samples SB1 and SB2 were collected from the south side of the former sandblasting
booth from depths of approximately 0.5 to 1 foot below land surface (bls). No stained
soil was observed during the completion of these soil borings. Soil sample SB3 was
collected from the northeast corner of the sandblasting booth in the former location of an
air compressor from a depth of approximately 0.5 to 1 foot bls. Stained soil was
observed in this location during the completion of this soil boring.

The soil samples were placed directly into laboratory-prepared containers. Soil samples
SB1 and SB2 were analyzed for hazardous substance list (HSL) metals including
antimony, arsenic, beryllium, cadmium, chromium, copper, lead, manganese, nickel,
selenium, silver, thallium, and zinc by SW-846 Methods 6010, and mercury by SW-846
Method 7471. Soil sample SB3 was analyzed for oil and grease by SW-846 Method
9071.
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

4
2.1.2 Laboratory Results
Analytical results for soil samples collected from the area adjacent to the former
sandblasting booth are presented on Table 1. Only analytes detected above the
laboratory reporting limit are presented on the table. The analytical laboratory report is
included in Appendix IV. Arsenic was detected in soil sample SB2 at a concentration of
5.3 milligrams per kilogram (mg/Kg), which is greater than the Inactive Hazardous Sites
Branch (IHSB) Soil Remediation Goals (SRGs) for arsenic of 4.4 mg/Kg. A copy of the
October 2008 IHSB SRGs are included in Appendix III.

Oil and grease was detected in soil sample SB3 at a concentration of 6,920 mg/Kg which
exceeds the North Carolina Department of Environment and Natural Resources
(NCDENR) Non-UST Action Level of 250 mg/Kg, as outlined in the UST Section
Guidelines for the Investigation and Remediation of Contamination from Non-UST
Petroleum Releases, effective July 1, 2007. A copy of pages from the NCDENR
guidelines is included in Appendix III.
2.2 Paint Mixing Room
2.2.1 Field Activities
On July 1, 2009 S&ME collected two (2) soil samples from one (1) location adjacent to
the storm water catch basin located outside of and adjacent to the former paint mixing
room on the northwest corner of the fabrication building. During the Phase I ESA site
reconnaissance, stained soils were observed in the paint mixing room apparently
terminating at this drain, the cover to the catch basin was covered in paint, and a sheen
was observed on the liquid within the basin. Soil sample locations were triangulated and
mapped using a tape measure and hardscape features on the property. The soil sample
locations are labeled TW3-SS1 and TW3-SS2 on Figure 3. The soil samples were
collected using direct push techniques and new or decontaminated equipment. The
procedure utilized for collecting the soil samples is outlined in Section 2.9.2.

Soil samples TW3-SS1 and TW3-SS2 were collected from the same soil boring located
to the southwest of the catch basin adjacent to the paint mixing room from depths of
approximately 1 to 2 feet and 9 to 10 feet bls, respectively. No stained soil was visually
observed or organic vapors were detected by screening with an organic vapor analyzer
(OVA) during the completion of this soil boring. The location of the collected soil
samples are indicated on Figure 3.

The soil samples were placed directly into laboratory-prepared containers. Soil sample
SB3 was analyzed for volatile organic compounds (VOCs) by SW-846 Method 8260 and
lead by SW-846 Method 6010.
2.2.2 Laboratory Results
Analytical results for soil samples collected adjacent to the storm water catch basin west
of the paint mixing room on the northwest corner of the fabrication building are presented
on Table 1. The analytical laboratory report is included in Appendix IV. Acetone,
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

5
chloromethane, methylene chloride, and lead were detected in soil samples TW3-SS1 and
TW3-SS2 at concentrations less than their respective IHSB SRGs.
2.3 Outdoor Painting Area and Breezeway
2.3.1 Field Activities
On June 30, 2009 S&ME collected near-surface soil samples from four (4) outdoor
locations north of the fabrication building. Two (2) of the soil samples were collected
from the north side of the outdoor painting area beneath the metal canopy where priming
of metal was performed. One (1) soil sample was collected from beneath the concrete
slab adjacent to the floor drain in the breezeway between the fabrication building and the
shop, and one (1) soil sample was collected from beneath the concrete slab adjacent to
floor drain beneath the sink in the outdoor painting area. It is unknown how these floor
drains were utilized or what chemicals may have entered the floor drain system. The soil
sample locations labeled SB4, SB5, SB6, and SB7 are depicted on Figure 3. The soil
samples were collected using a decontaminated stainless steel hand auger. Prior to the
collection of soil samples SB6 and SB7, a concrete coring machine was utilized to access
the soil beneath the slab. The procedure utilized for collecting the soil samples is
outlined in Section 2.9.1.

Soil samples SB4 and SB5 were collected in the northwest and northeast portions of the
outdoor area under the metal canopy, respectively. Soil sample SB6 was collected
beneath the concrete slab adjacent to the outdoor floor drain located in the breezeway
between the fabrication building and the machine shop. Soil sample SB7 was collected
beneath the concrete slab adjacent to the floor drain beneath the sink in the outdoor
painting area. Soil samples SB4 and SB5 were collected from depths of approximately
0.5 to 1 foot bls. Soil samples SB6 and SB6 were collected from depths of approximately
0.5 to 1 foot beneath the concrete slab. No stained soil was observed during the
collection of the soil samples. The location of the collected soil samples are indicated on
Figure 3.

The soil samples were placed directly into laboratory-prepared containers. Soil samples
SB4 and SB5 were analyzed for VOCs by SW-846 Method 8260 and lead by SW-846
Method 6010. Soil samples SB6 and SB7 were analyzed for VOCs by SW-846 Method
8260, oil and grease by SW-846 Method 9071, lead and chromium by SW-846 Method
6010, and mercury by SW-846 Method 7471.
2.3.2 Laboratory Results
Analytical results for soil samples collected from the north side of the outdoor painting
area beneath the metal canopy, beneath the concrete slab adjacent to the floor drain in the
breezeway, and beneath the concrete slab adjacent to floor drain beneath the sink in the
outdoor painting area are presented on Table 1. The analytical laboratory report is
included in Appendix IV.

Lead was detected in soil samples SB4 (6,560 mg/Kg), SB6 (427 mg/Kg), and SB7
(1,090 mg/Kg) at concentrations exceeding the IHSB SRG for lead of 400 mg/Kg. Lead
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

6
was detected in soil sample SB5 at a concentration of 86.6 which is below the IHSB SRG
for lead. Mercury was detected in soil sample SB7 at a concentration of 3.1 mg/Kg
which exceeds the IHSB SRG for mercury of 1.3 mg/Kg. An oil and grease
concentration of 867 mg/Kg was detected in soil sample SB7 which is in exceedence of
the NCDENR Non-UST Action Level of 250 mg/Kg.
2.4 Machine Shop
2.4.1 Field Activities
On June 30, 2009 S&ME collected one (1) near surface soil sample from beneath the
concrete slab adjacent to the floor drain within the former machine shop onsite. It is
unknown how this floor drain was utilized or what chemicals, if any, may have entered
the floor drain system. The soil sample location was triangulated and mapped using a
tape measure and hardscape features on the property. The soil sample location is labeled
SB8 on Figure 3. The soil sample was collected using a decontaminated stainless steel
hand auger. Prior to the collection of soil sample SB8, a concrete coring machine was
utilized access the soil beneath the slab. The procedure utilized for collecting the soil
samples is outlined in Section 2.9.1.

Soil sample SB8 was collected beneath the concrete slab adjacent to and west of the floor
drain located on the interior of the former machine shop. The soil sample was collected
from a depth of approximately 0.5 to 1 foot beneath the concrete slab. No stained soil
was observed during the collection of soil sample SB8. The location of the collected soil
sample is indicated on Figure 3.

The soil sample was placed directly into laboratory prepared containers. Soil sample SB8
was analyzed for VOCs by SW-846 Method 8260 , lead and chromium by SW-846
Method 6010, and oil and grease by SW-846 Method 9071.
2.4.2 Laboratory Results
Analytical results for the soil sample collected from beneath the concrete slab adjacent to
the floor drain in the former machine shop are presented on Table 1. The analytical
laboratory report is included in Appendix IV.

Lead was detected in soil samples SB8 at a concentration of 1,150 which exceeds the
IHSB SRG for lead of 400 mg/Kg. An oil and grease concentration of 3,210 mg/Kg was
detected in soil sample SB8 which is in exceedence of the NCDENR Non-UST Action
Level of 250 mg/Kg.
2.5 Fabrication Building
2.5.1 Field Activities
On June 30, 2009 S&ME collected near surface soil samples from three (3) locations
within the former fabrication building. Two (2) of the soil samples were collected from
beneath the concrete slab where stained concrete was observed. One (1) soil sample was
collected from beneath the concrete slab adjacent to floor drain beneath the utility sink
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

7
within the fabrication building. It is unknown how this floor drain was utilized or what
chemicals, if any, may have entered the floor drain system. The soil sample locations
were triangulated and mapped using a tape measure and hardscape features on the
property. The soil sample locations labeled SB9, SB10, and SB11 are depicted on Figure
3. The soil samples were collected using a decontaminated stainless steel hand auger.
Prior to the collection of the soil samples, a concrete coring machine was utilized access
the soil beneath the slab. The procedure utilized for collecting the soil samples is
outlined in Section 2.9.1.

Soil sample SB9 was collected from beneath the concrete slab in the area of stained
concrete on the west side of the fabrication building. Soil sample SB10 was collected
from beneath the concrete slab in the area of stained concrete on the east side of the
western portion of the fabrication building. Soil sample SB11 was collected beneath the
concrete slab adjacent to the outdoor floor drain located beneath the utility sink in the
fabrication building. The soil samples were collected from depths of approximately 0.5
to 1 foot beneath the concrete slab. No stained soil was observed during the collection of
the soil samples. The location of the collected soil samples are indicated on Figure 3.

The soil samples were placed directly into laboratory-prepared containers. The soil
samples were analyzed for oil and grease by SW-846 Method 9071. Soil sample SB11
was also analyzed for VOCs by SW-846 Method 8260 and lead and chromium by SW-
846 Method 6010.
2.5.2 Laboratory Results
Analytical results for soil samples collected from beneath the concrete slab where stained
concrete was observed and from beneath the concrete slab adjacent to floor drain beneath
the utility sink within the fabrication building area are presented on Table 1. The
analytical laboratory report is included in Appendix IV.

Oil and grease was detected in soil sample SB10 at a concentration of 698 mg/Kg which
exceeds the NCDENR Non-UST Action Level of 250 mg/Kg.
2.6 Potential Underground Storage Tanks
2.6.1 Field Activities
On July 1, 2009 S&ME collected soil samples from five (5) boring locations adjacent to
the location of suspected petroleum storage tanks and/or dispenser locations. One (1) soil
sample was collected in the vicinity of where a gasoline tank is depicted on the northwest
corner of the storage building on the 1950 and 1954 Sanborn maps. One (1) soil sample
was collected adjacent to a capped pipe representing a potential UST that was identified
adjacent to the second bay from the west of the five-bay garage. One (1) soil sample was
collected adjacent to the two pipes representing a potential UST or former fuel dispenser
identified adjacent to the northeast corner of the former fabrication building. Two (2)
soil samples were collected adjacent to the fill port and vent pipe indicative of a UST
observed adjacent to the east side of the former paint booth onsite.

Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

8
Prior to the installation of the soil borings and collection of the soil samples, the
contracted private utility locator attempted to identify the presence of USTs associated
with the observed potential UST site features. The utility locater identified the location
of a UST in proximity to the vent pipe and fill port located adjacent to the former paint
booth using a metal detector. Verification of the UST was performed by using a probe
rod.

USTs were not identified associated with the other identified potential UST site features.
Two soil samples were originally proposed to be collected from the areas adjacent to the
capped pipe near the five-bay garage, and adjacent to the two pipes identified at the
northeast corner of the former fabrication building. The two proposed samples assumed
that a UST would be identified associated with these features and a sample would be
collected from each end of the identified tank. Because USTs were not identified by the
private utility locator, only one soil sample was collected in each of these locations.
Therefore, soil samples SB-12 and SB-16 were not collected as part of the assessment.

The soil sample locations labeled SB13, SB14, SB15, SB17 and SB18 are depicted on
Figure 3. The soil samples were collected using direct push techniques. The procedure
utilized for collecting the soil samples is outlined in Section 2.9.2.

A soil boring was installed adjacent to the capped pipe south of the second bay from the
west of the five-bay garage. Soil sample SB13 was collected from the boring from a
depth of approximately 9 to 10 feet bls. No stained soil or elevated volatile
concentrations were detected during the installation of the soil boring.

Two soil borings were installed adjacent to the identified UST located at the northeast
corner of the former fabrication building. Soil sample SB14 was collected from the soil
boring installed on the north side of the identified UST from approximately 5 to 6 feet
bls. OVA readings were detected (operating in the flame ionization detector (FID mode)
1 to 5 parts per million (ppm), non-specific) from approximately 4 to 6 feet bls. Soil
sample SB15 was collected from the soil boring installed on the south side of the
identified UST from approximately 4 to 5 feet bls. OVA readings were detected (FID 3
to 24 ppm) from approximately 4 to 8 feet bls.

A soil boring was installed adjacent to the northeast corner of the former fabrication
building. Soil sample SB17 was collected from the boring from a depth of approximately
8 to 9 feet bls. No stained soil or OVA readings were detected during the installation of
the soil boring.

A soil boring was installed in the vicinity of where a gasoline tank is depicted on the
northwest corner of the storage building on the 1950 and 1954 Sanborn maps. Soil
sample SB18 was collected from the boring at a depth of approximately 9 to 10 feet bls.
Petroleum odors and OVA readings were detected from approximately 4 to 10 feet bls,
with the greatest OVA readings (photo-ionization detector (PID) 600 to 850 ppm and FID
9,000 to 22,000 ppm) detected at a depth of approximately 9 to 10 feet bls.

Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

9
The locations of the collected soil samples are indicated on Figure 3. The soil samples
were collected and placed directly into laboratory-prepared containers. The soil samples
were analyzed for total petroleum hydrocarbons (TPH), diesel range organics (DRO) by
SW-846 Method 3550 and gasoline range organics (GRO) by SW-846 Method 5030.
2.6.2 Laboratory Results
Analytical results for soil samples collected adjacent to the location of suspected
underground petroleum storage tanks and/or dispenser locations are presented on Table 1.
The analytical laboratory report is included in Appendix IV.

TPH-DRO was detected in soil sample SB14 at a concentration of 181mg/Kg which
exceeds the NCDENR UST Action Level of 10 mg/Kg. The soil NCDENR UST Action
Levels are outlined in the UST Section Guidelines for Site Checks, Tank Closure, and
Initial Response and Abatement for UST Releases, March 1, 2007 Version, Change 3,
effective December 1, 2008. A copy of pages from the Guidelines is included in
Appendix III. TPH-DRO was detected in soil sample SB18 at a concentration of 769
mg/Kg which exceeds the NCDENR Non-UST Action Level of 40 mg/Kg.
2.7 Debris Piles
2.7.1 Field Activities
On June 30, 2009 S&ME collected near-surface soil samples from the seven (7) existing
and former (determined from historical aerial photographs of the site) debris piles on the
eastern portion of the property. The soil sample locations were triangulated and mapped
using a tape measure and hardscape features on the property. The soil sample locations
labeled SB19, SB20, SB21, SB22, SB23, SB24, and SB25 are depicted on Figure 3. The
soil samples were collected using a decontaminated stainless steel hand auger. The
procedure utilized for collecting the soil samples is outlined in Section 2.9.1.

The soil samples were collected from depths of approximately 0.5 to 1 foot bls. No
stained soil was observed during the completion of these soil borings. Petroleum odors
were associated with soil sample SB25 collected in the northeast corner of the subject
property. The soil samples were placed directly into laboratory-prepared containers. Soil
samples SB19 through SB25 were analyzed for VOCs by SW-846 Method 8260, semi-
volatile organic compounds (SVOCs) by SW-846 Method 8270, TPH-DRO and GRO, oil
and grease by SW-846 Method 9071, and HSL metals.
2.7.2 Laboratory Results
Analytical results for soil samples collected associated with existing and former debris
piles are presented on Table 1. The analytical laboratory report is included in Appendix
IV.

Soil sample SB19 had a concentration of TPH-DRO (847 mg/Kg) detected above the
NCDENR Non-UST Action Level of 40 mg/Kg.

Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

10
Soil sample SB20 had concentrations of antimony (8.6 mg/Kg), arsenic (5.7 mg/Kg), lead
(1,220 mg/Kg), and manganese (464 mg/Kg) detected above their respective IHSB SRGs
of 6.2 mg/Kg, 4.4 mg/Kg, 400 mg/Kg, and 360 mg/Kg.

Soil sample SB21 had a concentrations of thallium (1.0 mg/Kg) detected equal to the
IHSB SRG for thallium of 1.0 mg/Kg.

Soil sample SB22 had a concentration of TPH-DRO (65.3 mg/Kg) detected above the
NCDENR Non-UST Action Level of 40 mg/Kg, and concentrations of antimony (8.2
mg/Kg), arsenic (6.3 mg/Kg), and manganese (482 mg/Kg) detected above their
respective IHSB SRGs of 6.2 mg/Kg, 4.4 mg/Kg, and 360 mg/Kg.

Soil sample SB23 had concentrations of TPH-DRO (151 mg/Kg) and oil and grease
(1,240 mg/Kg) detected above the NCDENR Non-UST Action Levels of 40 mg/Kg and
250 mg/Kg, respectively. Manganese (440 mg/Kg) and benzo(a)pyrene (0.385 mg/Kg)
were detected in soil sample SB23 at concentrations exceeding their respective IHSB
SRGs of 360 mg/Kg and 0.15 mg/Kg. Phenanthrene was detected in soil sample SB23 at
a concentration of 0.813 mg/Kg. Currently no IHSB SRG has been established for
phenanthrene.

Soil sample SB24 had concentrations of TPH-DRO (40.4 mg/Kg) and oil and grease (586
mg/Kg) detected above the NCDENR Non-UST Action Levels of 40 mg/Kg and 250
mg/Kg, respectively. Antimony (7.3 mg/Kg), lead (522 mg/Kg), manganese (440
mg/Kg), thallium (1.1 mg/Kg), benzo(a)anthracene (2.31 mg/Kg), benzo(a)pyrene (2.85
mg/Kg), benzo(b)fluoranthene (1.6 mg/Kg), and benzo(k)fluoranthene (1.83 mg/Kg)
were detected in soil sample SB23 at concentrations exceeding their respective IHSB
SRGs. Phenanthrene and benzo(g,h,i)perylene were detected in soil sample SB23 at
concentrations of 8.23 mg/Kg and 0.99 mg/Kg, respectively. Currently no IHSB SRGs
have been established for phenanthrene or benzo(g,h,i)perylene.

Soil sample SB25 had concentrations of TPH-DRO (1,080 mg/Kg) and oil and grease
(3,850 mg/Kg) detected above the NCDENR Non-UST Action Levels of 40 mg/Kg and
250 mg/Kg, respectively. Manganese was detected in soil sample SB25 at a
concentration of 371 mg/Kg, which exceeds the IHSB SRG for manganese of 360
mg/Kg.
2.8 Go-Cart Track
2.8.1 Field Activities
On June 30, 2009 S&ME collected near-surface soil samples from the two (2) locations
from within the go-cart track located in the northeast corner of the subject property. The
soil sample locations labeled SB26 and SB27 are depicted on Figure 3. The soil samples
were collected using a decontaminated stainless steel hand auger. The procedure utilized
for collecting the soil samples is outlined in Section 2.9.1.

The soil samples were collected from depths of approximately 0.5 to 1 foot bls. No
stained soil was observed during the completion of these soil borings. The soil samples
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

11
were placed directly into laboratory-prepared containers. Soil samples SB26 and SB27
were analyzed for TPH-DRO and -GRO.
2.8.2 Laboratory Results
Analytical results for soil samples collected within the interior of the go-cart track are
presented on Table 1. The analytical laboratory report is included in Appendix IV.

Soil sample SB26 had a concentration of TPH-DRO (19.9 mg/Kg) detected below the
NCDENR Non-UST Action Level of 40 mg/Kg. Soil sample SB27 had a concentration
of TPH-DRO (56.2 mg/Kg) detected above the NCDENR Non-UST Action Level of 40
mg/Kg.
2.9 Soil Sampling Techniques
2.9.1 Near Surface Soil Sampling
The near surface soil samples were collected from soil borings created using a
decontaminated stainless steel hand auger (see Section 2.10). The soil samples were
collected from an approximate 0.5 foot interval of material contained in the auger bucket.
When multiple analytical suites were scheduled for analyses, they were collected in the
following order:
1. VOCs
2. SVOCs
3. TPH (GRO and DRO)
4. Oil and Grease
5. Metals

Soil samples chosen for laboratory analyses were properly preserved, labeled, logged
onto a chain-of-custody form, and placed into an iced cooler for shipment. All
laboratory-analyzed soil samples were sent to the laboratory within 48 hours of sample
collection.
2.9.2 Subsurface Soil Sampling
The subsurface soil samples were collected from soil borings created using direct push
techniques (i.e. Geoprobe®). Prior to beginning field work activities and in between
each soil boring location, the Geoprobe® rods and Macro-Core® sampler were
decontaminated using a steam cleaner. Continuous soil samples were collected during
completion of each soil boring and field screened. Each soil sample interval was
collected in new polyvinylchloride (PVC) tubes placed in the decontaminated Macro-
Core® sampler. Each collected sample was placed in a new Ziplok®, allowed to sit for
approximately 5 minutes to equilibrate with the ambient outside air temperature, and the
head space within the bag was then field-screened for VOCs using an OVA (PID and FID
readings) calibrated to isobutylene gas. The soil samples were collected from an
approximate 1 foot interval of material contained in the PVC tube. When multiple
analytical suites were scheduled for analyses, they were collected in the following order:
1. VOCs
2. SVOCs
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

12
3. TPH (GRO and DRO)
4. Oil and Grease
5. Metals

Soil samples chosen for laboratory analyses were properly preserved, labeled, logged
onto a chain-of-custody form, and placed into an iced cooler for shipment. All
laboratory-analyzed soil samples were sent to the laboratory within 48 hours of sample
collection.
2.10 Quality Control
2.10.1 Sampling Equipment
Equipment used to complete soil borings and to collect soil samples was decontaminated
according to the Quality Assurance Project Plan (Revision 1) dated June 26, 2009. A
clean separate decontamination (decon) station was set up in a clean area at the site. The
decon station was used to decontaminate sampling equipment. Nitrile phthalate-free
gloves were worn by sampling personnel during all sampling and equipment handling
activities.

Prior to use and after each sampling event, all small sampling equipment was
decontaminated and cleaned to prevent cross-contamination. The equipment
decontamination procedure consisted of a potable water rinse to remove visible dirt and
debris followed by an Alconox® wash, another potable water rinse, a deionized water
rinse, an isopropyl alcohol wash, and final deionized water rinse followed by air drying
of the equipment.

The larger equipment, including Geoprobe® rods and Macro-Core® samplers and the rig
itself, were cleaned with a high-pressure, hot water steam cleaner. The equipment was
rinsed once with the steam cleaner then scrubbed to remove any remaining loose debris,
followed by another wash with the steam cleaner and then air-dried. All of the large
equipment decontamination rinsate was contained within a bermed area and pumped into
55-gallon drums and labeled as to their contents.

One equipment rinsate sample (Equip Rinsate) was collected on June 30, 2009 after
decontamination of the stainless steel hand auger. The rinsate sample was collected by
pouring commercially purchased de-ionized water through the hand auger bucket into
laboratory prepared sampling containers. The equipment rinsate sample was analyzed for
VOCs by SW-846 Method 8260, SVOCs by SW-846 Method 8270, TPH-DRO and
GRO, HSL Metals by SW-846 Methods 200.7 and 7471, (5) oil and grease by SW-846
Method 9071.

One equipment rinsate sample (Equip Rinsate) was collected on July 1, 2009 after the
decontamination of the Macro-Core sampler. The rinsate sample was collected by
pouring de-ionized water through the sampler into laboratory prepared sampling
containers. The equipment rinsate sample was analyzed for (1) VOCs by SW-846
Method 8260 and (2) lead by SW-846 Method 200.7.
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

13

No target compounds were detected in the equipment rinsate samples. The equipment
rinsate analytical results are summarized in Table 4, and the laboratory reports are
included in Appendix IV.
2.10.2 Duplicate Samples
A duplicate soil sample was submitted for soil samples SB18, SB19, and TW3-SS2. The
duplicate of soil sample SB18 was labeled Duplicate 2 and submitted for analysis for
TPH-DRO and GRO. The duplicate of soil sample SB19 was labeled Duplicate 1 and
submitted for analysis for VOCs by SW-846 Method 8260, SVOCs by SW-846 Method
8270, HSL Metals by SW-846 Methods 6010 and 7471, oil and grease by SW-846
Method 9071 and TPH-DRO and GRO. The duplicate of soil sample TW3-SS2 was
labeled Duplicate 1 and submitted for analysis for VOCs by SW-846 Method 8260 and
for lead by SW-846 Method 6010.

The laboratory results for soil samples SB18, Duplicate 2, SB19, Duplicate 1, TW3-SS2,
and Duplicate 1 are summarized in Table 1. The analytical laboratory report is included
in Appendix IV. Relative percent difference (RPD), a measure of precision, was used to
compare analytical results between sample and duplicate pair. RPD is calculated by:

RPD (%) = [X1-X2] / Xave * 100

where:

X1 = concentration of sample

X2 = concentration of duplicate pair

Xave = ((X1 + X2) / 2)

The laboratory results for the detected compounds in soil sample SB18 and its blind
duplicate (Duplicate 2) had RPDs between 17% and 26%. The laboratory results for the
detected compounds in soil sample SB19 and its blind duplicate (Duplicate 1) had RPDs
between 5% and 131%. The laboratory results for the detected compounds in soil sample
TW3-SS2 and its blind duplicate (Duplicate 1) had RPDs between 1% and 19%.
During the RPD calculations, for concentrations of analytes not detected by the
laboratory method, the concentrations were set equal to the laboratory reporting limit.
2.10.3 Trip Blanks
Four trip blanks (Trip Blank 1, Trip Blank 2, and Trip Blank 3 on 6-30-09, and Trip
Blank 1 on 7-1-09) were shipped with the soil samples. The trip blanks were analyzed
for volatile organic compounds by SW-846 Method 8260. No target 8260 compounds
were detected in the trip blanks. The trip blank analytical results are summarized in
Table 4, and the laboratory reports are included in Appendix IV.
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

14
2.10.4 Investigation-Derived Wastes
Soil cuttings generated during the collection of the near surface soil samples (0.5 to 1 foot
bls) backfilled into the hand auger borings. Soil cuttings generated during completion of
all soil borings, except the boring associated with the installation of temporary well TW-
3, were spread onsite in accordance with the following guidelines:

• UST Section Guidelines for the Investigation and Remediation of
Contamination from Non-UST Petroleum Releases developed by the
NCDENR-DWM UST Section, effective July 1, 2007.

• Guidelines for Assessment and Corrective Action for UST Releases developed
by the NCDENR-DWM UST Section, effective December 1, 2008.

According to the referenced guidelines, drill cuttings/mud with petroleum contamination
can be placed on the ground surface in proximity to the well/boring.

The soil cuttings generated during the completion of the soil borings associated with
temporary well TW-3 were containerized in a labeled and sealed drum that is now staged
onsite.

Wastewater generated during decontamination activities was placed into labeled and
sealed 55-gallon drums that are staged onsite.

Investigation-derived wastes contained onsite will be sampled and analyzed to determine
the appropriate disposal method.

General consumable equipment from the sampling (e.g., nitrile gloves, polyethyelene
tubing, etc.) was contained in plastic garbage bags for landfill disposal.
3. GROUNDWATER ASSESSMENT
3.1 Temporary Wells
3.1.1 Field Activities
On July 1, 2009 S&ME installed six (6) temporary monitoring wells on the subject
property. Five of the wells were installed for the collection of shallow groundwater
samples located above consolidated material (i.e. rock) at the site. One of the wells (TW-
2) was installed solely to assist in determining groundwater flow direction on the site. No
groundwater samples were collected from monitoring well TW-2. No drilling within
rock was performed. The monitoring well locations were triangulated and mapped using
a tape measure and are labeled TW-1, TW-2, TW-3, TW-4, TW-5, and TW-6 on Figure
3.

Prior to the installation of the monitoring wells, continuous soil samples were collected
from the unconsolidated material using direct push techniques. The lithology of each soil
sample was recorded in the project field book. Temporary monitioring wells were
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

15
installed by a NC Licensed Well Driller. Well construction data are presented in Table 2.
Well construction logs for each monitoring well installation are presented in Appendix I.

The temporary monitoring wells consisted of 1-inch diameter schedule 40, flush-thread,
PVC pipe inserted into a 2.25-inch diameter bore hole. The construction of the lower
portion of five of the monitoring wells consisted of manufactured well screen with 0.010-
inch slots. The length of the well screen pipe was determined based the depth of the
apparent water table. Medium-to-fine grained, washed sand was placed in the annular
space of the well to a level approximately 1 foot above the top of the well screen, with an
approximate 1-foot thick bentonite seal positioned on top of the sand pack. The lower
portion of monitoring well TW-3 consisted of manufactured well screen with 0.010-inch
slots and a 5-foot section of pre-packed sand filter, and an approximate 1-foot thick
bentonite seal positioned above the pre-packed sand filter. (Note: The well screen length
and depth were situated so top of the water table intersects the well at the well screen.)
The annular space above the bentonite seal was left un-grouted. The wells were secured
by a locking expansion plug and protected from surface runoff using unopened bags of
bentonite at the ground surface.
3.1.2 Groundwater Sampling Methods
Before purging and sampling of the monitoring wells, the water level and depth of the
temporary monitoring wells was measured and recorded. Groundwater elevation data are
presented on Table 2. Each well was developed and purged for sampling using a
variable speed, electric, peristaltic pump. The purge water was monitored for
temperature, dissolved oxygen, pH, oxidation/reduction potential, and conductivity using
a flow-through multi-meter. Turbidity of the purge water was monitored using a
turbidimeter. The well was considered sufficiently purged when the temperature,
dissolved oxygen, pH, and conductivity of the ground water stabilized and the turbidity
either stabilized or was less than 10 Nephelometric Turbidity Units (NTUs). Ten NTUs
is the goal for most groundwater sampling objectives. Stabilization occurred when
dissolved oxygen, pH, conductivity, and turbidity varied no more than 10% and the
temperature was constant for three consecutive readings. Purge water monitoring data
for each monitoring well were recorded on well sampling forms. A copy of the well
sampling forms is included in Appendix II.

Prior to purging each well, new silicone tubing (at the pump head) and polyethylene
tubing (downwell) was installed. The groundwater samples were placed directly into
laboratory-prepared containers.

When multiple analytical suites were scheduled for analyses, they were collected in the
following order:
1.VOCs
2.SVOCs
3.TPH (GRO and DRO)
4. Oil and Grease
5. Metals

Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

16
The collected groundwater samples were analyzed for VOCs by SW-846 Method 8260
and SVOCs by SW-846 Method 8270. The groundwater sample collected from
monitoring well TW-3 was also analyzed for lead by SW-846 Method 200.7.

The temporary monitoring wells were properly abandoned by a NC Licensed Well Driller
after the groundwater samples were collected.
3.1.3 Laboratory Results
Analytical results for groundwater samples collected from the monitoring wells located
onsite are presented on Table 3. The analytical laboratory report is included in Appendix
IV. A copy of the North Carolina Groundwater Quality Standards published on
December 7, 2006 is presented in Appendix III.

The groundwater samples collected from monitoring wells TW-1, TW-4, and TW-6 were
below laboratory reporting limits for all analytes on the SW-846 Method 8260 and 8270
target lists.

Methyl-tert-butyl ether (MTBE) was detected in the groundwater sample collected from
monitoring well TW-5 at a concentration of 1.0 microgram per liter (µg/L) which is
below the North Carolina Groundwater Quality Standard (NCAC 2L) for MTBE of 200
µg/L.

Lead was detected in the groundwater sample collected from monitoring well TW-3 at a
concentration of 85.4 µg/L which exceeds the NCAC 2L standard for lead of 15 µg/L.
Cis-1,2-dichloroethene was also detected in monitoring well TW-3 at a concentration of
1.4 µg/L which is below the NCAC 2L standard for cis-1,2-dichloroethene of 70 µg/L.
3.2 Quality Control
3.2.1 Sampling Equipment
Equipment used to install monitoring wells and to collect groundwater samples was
decontaminated according to the Quality Assurance Project Plan Revision 1 dated June
26, 2009. The decon station was used to decontaminate both personnel and small
sampling equipment.

The decontamination procedure for small sampling equipment such as flow through
multi-meter and the electronic water level meter consisted of a potable water rinse to
remove visible dirt and debris, followed by an Alconox® wash, another potable water
rinse, a deionized water rinse, an isopropyl alcohol wash, and final deionized water rinse
followed by air drying of the equipment.

The larger equipment, including Geoprobe® rods and Macro-Core® samplers and the rig
itself, were cleaned with a high-pressure, hot water steam cleaner. The equipment was
rinsed once with the steam cleaner then scrubbed to remove any remaining loose debris,
followed by another wash with the steam cleaner and then air-dried. All of the large
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

17
equipment decontamination rinsate was contained within a bermed area and pumped into
55-gallon drums and labeled as to their contents.

New silicone tubing (at the pump head) and polyethylene tubing (downwell) was used to
collect each groundwater sample.

All sampling equipment and laboratory containers were handled by personnel with nitrile
phthalate-free gloves.
3.2.2 Duplicate Samples
A duplicate groundwater sample (Duplicate 1) was submitted for the groundwater sample
collected from monitoring well TW-5. Both samples were submitted for analysis for
VOCs by SW-846 Method 8260 and SVOCs by SW-846 Method 8270. The laboratory
results for groundwater samples TW-5 and Duplicate 1 are summarized in Table 3. A
copy of the laboratory report is included in Appendix IV. RPD, a measure of precision,
was used to compare analytical results between sample and duplicate pair.

MTBE was detected in groundwater sample Duplicate 1 at a concentration of 1.0 µg/L
and not detected in sample TW-5 (< 1.0 µg/L). For comparative purposes these are
essentially the same reportable concentrations (0% RPD). Groundwater sample
analytical results for TW-5 and Duplicate 1 were below laboratory reporting limits for all
additional analytes on the SW-846 Method 8260 and 8270 target compound lists.
3.2.3 Trip Blanks
One trip blank (Trip Blank 1 on 7-2-09) was shipped with the groundwater samples and
analyzed for VOCs by SW-846 Method 8260. No target 8260 compounds were detected
in Trip Blank 1.

The analytical results are summarized in Table 4 and the laboratory report is included in
Appendix IV.
3.2.4 Field Blanks
A field blank sample (Field Blank) was prepared during collection of groundwater
sample TW-1. The field blank sample was analyzed for VOCs by SW-846 Method 8260.
No target compounds were detected in Field Blank.

The laboratory results are summarized in Table 4 and the laboratory report is included in
Appendix IV.
3.4 Investigation-Derived Wastes
The development and purge water from the monitoring wells was placed in labeled and
sealed drums and staged onsite. The groundwater sample laboratory results will be used
to determine the method of disposal for that waste.
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

18
3.5 Groundwater Flow
The top of casing and ground surface elevations for each of the temporary monitoring
wells onsite were surveyed by S&ME personnel on July 2, 2009. Prior to collecting
groundwater samples, the depth to groundwater below the top of casing was gauged in
each well using an electronic water level meter. The groundwater elevation data are
presented on Table 2.

A shallow groundwater potentiometric map of the site was prepared based on the relative
groundwater elevations and is presented as Figure 4. Approximate groundwater flow
direction was determined based on the relative groundwater elevations. Based on this
information, groundwater flow beneath the subject property appears to be to the south,
towards the Swannanoa River.
4. CONCLUSIONS AND RECOMMENDATIONS
4.1 UST East of Former Paint Booth
An apparent release from the underground storage tank located adjacent to the east side
of the former paint booth onsite was identified during the assessment. A TPH – DRO
concentration of 181 mg/Kg was detected in soil sample SB14 collected from
approximately 5 to 6 feet bls on the south side of this UST. Based on the collection depth
and location of this soil sample, the TPH-DRO impacts likely originated from the UST. The
impacted soil adjacent to this UST should be reported to the NCDENR UST Section. The
UST Section will likely require removal of the UST and additional assessment and/or
remediation.
4.2 Gasoline Tank on Sanborn Maps
Petroleum impacted soil was detected in the soil boring installed in the vicinity of where a
gasoline tank is depicted on the northwest corner of the storage building on the 1950 and
1954 Sanborn maps. Soil sample SB18 was collected from a depth of approximately 9 to
10 feet bls in the approximate location of the depicted gasoline tank. A TPH-DRO
concentration of 769 mg/Kg was detected in soil sample SB18. The horizontal and
vertical extent of petroleum contaminated soil has not been delineated in this location.
S&ME recommends further soil assessment in this area to attempt to quantify the volume
of petroleum impacted soil in this area.
4.3 Sandblasting Booth
Soil sample SB3 was collected from the northeast corner of the sandblasting booth in the
former location of an air compressor from a depth of approximately 0.5 to 1 foot bls.
Stained soil was observed in this location during the completion of this soil boring. Oil
and grease was detected in soil sample SB3 at a concentration of 6,920 mg/Kg which
exceeds the NCDENR Non-UST Action Level of 250 mg/Kg. The horizontal and
vertical extent of oil and grease contaminated soil has not been delineated in this location.
S&ME recommends further soil assessment in this area to attempt to quantify the volume
of oil and grease impacted soil in this area. S&ME recommends analyzing the oil and
grease samples collected in this area by SW-846 Method 9071 with silica gel cleanup to
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

19
determine the TPH fraction of the collected samples. The silica gel cleanup component
of the analysis will remove bias due to naturally-existing biogenic fats in the soil.
4.4 Outdoor Painting Area, Machine Shop, and Breezeway
Lead was detected above the IHSB SRG in soil samples SB4, SB6, SB7, and SB8
collected from the area of the outdoor painting area, the former machine shop and the
breezeway between the fabrication building and the breezeway. Lead was also detected
in the groundwater sample collected from temporary monitoring well TW-3 at a
concentration exceeding the North Carolina Groundwater Quality Standards. Temporary
well TW-3 is located hydraulically downgradient of the former machine shop and
breezeway areas. The horizontal and vertical extent of lead contaminated soil has not
been delineated in this location. S&ME recommends further soil assessment in this area
to attempt to quantify the volume of lead impacted soil in this location. Additionally,
S&ME recommends analyzing a soil sample from the vicinity of soil sample SB4 by the
Toxicity Characteristic Leaching Procedure (TCLP) for lead to ascertain if the associated
soil, upon removal, would be determined to be a hazardous waste per the lead
characteristic metric.

Oil and grease concentrations were detected at concentrations exceeding the NCDENR
Non-UST Action Levels in soil samples SB7 and SB8. Mercury was also detected in soil
sample SB7 at a concentration of 3.1 mg/Kg, which exceeds the IHSB SRG of 1.3
mg/Kg. The horizontal and vertical extent of oil and grease contaminated soil has not
been delineated in these locations. Also, the horizontal and vertical extent of mercury has
not been delineated surrounding soil sample SB7. S&ME recommends further soil
assessment in these two areas to attempt to quantify the volume of oil and grease in these
areas, and the quantity of mercury contaminated soil surrounding soil sample SB7.
S&ME recommends analyzing the oil and grease samples collected in this area by SW-
846 Method 9071 with silica gel cleanup to determine the TPH fraction of the collected
samples.
4.5 Areas of Impacted Soil
Arsenic was detected in soil sample SB2 at a concentration of 5.3 mg/Kg, which exceeds
the IHSB SRG for arsenic of 4.4 mg/Kg. According to the U.S. Geological Survey
Professional Paper 1648 Geochemical Landscapes of Conterminous United States-New
Map Presentations for 22 Elements (http://pubs.usgs.gov/pp/p1648/p1648.pdf), arsenic
has been documented as existing in western North Carolina at concentrations ranging
from approximately 4.0 mg/Kg to 7.0 mg/Kg. Based on this information, it is possible
that the concentration of arsenic detected in soil sample SB2 is not elevated due to any
previous or current use of the property. Due to the relatively low concentrations of
arsenic in this location, and that it may be naturally occurring at its detected
concentration, S&ME at this time does not recommend additional sampling for arsenic.
However, S&ME does recommend that concurrence with this recommendation be
obtained from NCDENR.

Oil and grease was detected in soil samples SB10 and SB19 at concentrations exceeding
the NCDENR Non-UST Action Level. The horizontal and vertical extent of oil and
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

20
grease contaminated soil has not been delineated in these locations. S&ME recommends
further soil assessment to attempt to quantify the volume of oil and grease impacted soil
in these areas. S&ME recommends analyzing the oil and grease samples collected in this
area by SW-846 Method 9071 with silica gel cleanup to determine the TPH fraction of
the collected samples.

Soil sample SB20 had concentrations of antimony, arsenic, lead, and manganese detected
above their respective IHSB SRGs. According to the U.S. Geological Survey
Professional Paper 1648 Geochemical Landscapes of Conterminous United States-New
Map Presentations for 22 Elements (http://pubs.usgs.gov/pp/p1648/p1648.pdf),
manganese have been documented as existing in western North Carolina at
concentrations from approximately 300 mg/kg to 600 mg/kg. Based on this information,
it is possible that the concentrations of arsenic and manganese detected in soil sample
SB20 are not due to any previous or current use of the property. The horizontal and
vertical extent of antimony and lead contaminated soil has not been delineated in this
location. S&ME recommends further soil assessment in this area to attempt to quantify
the volume of antimony and lead impacted soil in this location. Due to the relatively low
concentrations of manganese and arsenic in this location, and that they may be naturally
occurring at their detected concentrations, S&ME does not recommend additional
sampling for manganese or arsenic. However, S&ME does recommend that concurrence
with this recommendation be obtained from NCDENR.

Thallium was detected in soil sample SB21 at a concentration of 1.0 mg/Kg which is
equal to the IHSB SRG for thallium. The horizontal and vertical extent of thallium
contaminated soil has not been delineated in this location. S&ME recommends further
soil assessment to attempt to quantify the volume of thallium-impacted soil in this area.

Soil sample SB22 had concentrations of antimony, arsenic, and manganese detected
above their respective IHSB SRGs. TPH – DRO was also detected in soil sample SB22
at a concentration exceeding the NCDENR Non-UST Action Level. It is possible that the
concentrations of arsenic and manganese detected in soil sample SB22 are not due to any
previous or current use of the property. The horizontal and vertical extent of antimony
and TPH-DRO contaminated soil has not been delineated in this location. S&ME
recommends further soil assessment in this area to attempt to quantify the volume of
antimony and TPH-DRO impacted soil in this location. Due to the relatively low
concentrations of manganese and arsenic in this location, and that they may be naturally
occurring at their detected concentrations, S&ME does not recommend additional
sampling for manganese or arsenic. However, S&ME does recommend that concurrence
with this recommendation be obtained from NCDENR.

Soil sample SB23 had concentrations of manganese and benzo(b)fluoranthene detected
above their respective IHSB SRGs. Oil and grease and TPH – DRO were also detected
in soil sample SB23 at concentrations exceeding the NCDENR Non-UST Action Levels.
Phenanthrene was detected in soil sample SB23 at a concentration of 0.813 mg/Kg.
Currently no IHSB SRG has been established for phenanthrene. It is possible that the
concentration of manganese (440 mg/Kg) detected in soil sample SB23 is not due to any
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

21
previous or current use of the property. The horizontal and vertical extent of oil and
grease, TPH-DRO, and benzo(b)fluoranthene contaminated soil has not been delineated
in this location. S&ME recommends further soil assessment in this area to attempt to
quantify the volume of impacted soil in this location. S&ME recommends analyzing the
oil and grease samples collected in this area by SW-846 Method 9071 with silica gel
cleanup to determine the TPH fraction of the collected samples. Due to the relatively low
concentration of manganese in this location, and that it may be naturally occurring at its
detected concentration, S&ME does not recommend additional sampling for manganese.
However, S&ME does recommend that concurrence with this recommendation be
obtained from NCDENR.

Soil sample SB24 had concentrations of antimony, lead, manganese, thallium, and
several polycyclic aromatic hydrocarbons (PAHs) detected above their respective IHSB
SRGs. Oil and grease and TPH – DRO were also detected in soil sample SB24 at
concentrations exceeding the NCDENR Non-UST Action Levels. Phenanthrene (8.23
mg/Kg) and benzo(g,h,i)perylene (0.99 mg/Kg) were also detected in soil sample SB24.
Currently no IHSB SRGs have been established for phenanthrene or
benzo(g,h,i)perylene. It is possible that the concentration of manganese (440 mg/Kg)
detected in soil sample SB23 is not due to any previous or current use of the property.
The horizontal and vertical extent of antimony, lead, thallium, PAHs, oil and grease, and
TPH-DRO contaminated soil has not been delineated in this location. S&ME
recommends further soil assessment in this area to attempt to quantify the volume of
impacted soil in this location. S&ME recommends analyzing the oil and grease samples
collected in this area by SW-846 Method 9071 with silica gel cleanup to determine the
TPH fraction of the collected samples. Due to the relatively low concentration of
manganese in this location, and that it may be naturally occurring at its detected
concentration, S&ME does not recommend additional sampling for manganese.
However, S&ME does recommend that concurrence with this recommendation be
obtained from NCDENR.

Soil sample SB25 had a concentrations of manganese detected above the IHSB SRG. Oil
and grease and TPH – DRO were also detected in soil sample SB25 at concentrations
exceeding the NCDENR Non-UST Action Levels. It is possible that the concentration of
manganese (371 mg/Kg) detected in soil sample SB25 is not due to any previous or
current use of the property. The horizontal and vertical extent of oil and grease and TPH-
DRO contaminated soil has not been delineated in this location. S&ME recommends
further soil assessment in this area to attempt to quantify the volume of impacted soil in
this location. S&ME recommends analyzing the oil and grease samples collected in this
area by SW-846 Method 9071 with silica gel cleanup to determine the TPH fraction of
the collected samples. Due to the relatively low concentration of manganese in this
location, and that it may be naturally occurring at its detected concentration, S&ME does
not recommend additional sampling for manganese. However, S&ME does recommend
that concurrence with this recommendation be obtained from NCDENR.

A TPH-DRO concentration of 56.2 mg/Kg was detected in soil sample SB27. This
concentration exceeds the NCDENR Non-UST Action Level of 40 mg/Kg. The
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

22
horizontal and vertical extent of petroleum contaminated soil has not been delineated in
this location. S&ME recommends further soil assessment in this area to attempt to
quantify the volume of petroleum impacted soil in this area.
4.6 Additional Assessment Locations
A relatively small number of near surface soil samples were collected across the property
in comparison to the size of the subject property. Near surface soil samples were not
collected and analyzed from a majority of the western portion of the property, west of the
former fabrication building, and on the eastern portion of the property, east of the storage
building. S&ME recommends performing near-surface soil sampling on a grid pattern
over these areas of the site. Collected soil samples should focus on analyses for lead,
chromium, hexavelent chromium, TPH-DRO and oil and grease. The results of these soil
samples in conjunction with soil samples collected at depth will be used to estimate the
volume of impacted soil across the site.
5. SOLE USE STATEMENT
All materials and information used for this project were obtained by S&ME. This report
is provided for the sole use of Awenasa, LLC, United States Environmental Protection
Agency, and the North Carolina Department of Environment and Natural Resources for
this project. Use of this report by any parties other than Awenasa, LLC, United States
Environmental Protection Agency, and the North Carolina Department of Environment
and Natural Resources will be at such party's sole risk. S&ME disclaims liability for any
use of or reliance on this report by third parties.

Sample ID1 SB1 SB2 SB3 SB4 SB5 SB6 SB7
Sample Date 6/30/2009 6/30/2009 6/30/2009 6/30/2009 6/30/2009 6/30/2009 6/30/2009
Sample Time 13:25 13:15 13:00 12:35 12:50 10:45 11:10
Sample Depth (ft bls)0.5 - 1 0.5 - 1 0.5 - 1 0.5 - 1 0.5 - 1 0.5 - 1 0.5 - 1
Method 8260
Acetone2 NA NA NA 0.339 0.115 < 0.119 < 0.114 12,000 - -
Chloromethane NA NA NA 0.313 < 0.0091 < 0.0119 < 0.0144 1.7 - -
Methylene Chloride NA NA NA 0.0455 < 0.0181 <0.0239 < 0.0288 1.1 - -
Method 8270
1-Methylnaphthalene NA NA NA NA NA NA NA 22 - -
2-Methylnaphthalene NA NA NA NA NA NA NA 62 - -
Napthalene NA NA NA NA NA NA NA 3.9 - -
Anthracene NA NA NA NA NA NA NA 3,400 - -
Benzo(a)anthracene NA NA NA NA NA NA NA 0.15 - -
Benzo(a)pyrene NA NA NA NA NA NA NA 0.015 - -
Benzo(b)fluoranthene NA NA NA NA NA NA NA 0.15 - -
Benzo(g,h,i)perylene NA NA NA NA NA NA NA NGE - -
Benzo(k)fluoranthene NA NA NA NA NA NA NA 1.5 - -
Chrysene NA NA NA NA NA NA NA 15 - -
Fluoranthene NA NA NA NA NA NA NA 460 - -
Phenanthrene NA NA NA NA NA NA NA NGE - -
Pyrene NA NA NA NA NA NA NA 340 - -
Fluorene NA NA NA NA NA NA NA 460 - -
bis(2-Ethylhexyl)phthalate NA NA NA NA NA NA NA 35 - -
Method 6010
Antimony 1.5 2.7 NA NA NA NA NA 6.2 - -
Arsenic 0.57 5.3 NA NA NA NA NA 4.4 - -
Beryllium < 0.091 0.17 NA NA NA NA NA 32 - -
Cadmium 0.14 2.3 NA NA NA NA NA 14 - -
Chromium III 9.6 16.1 NA NA NA 21.9 31.2 24,000 - -
Copper 10.7 31.9 NA NA NA NA NA 620 - -
Lead 61.5 126 NA 6,560 86.6 427 1,090 400 - -
Manganese 151 239 NA NA NA NA NA 360 - -
Nickel 4.4 13.9 NA NA NA NA NA 320 - -
Selenium < 0.91 < 1.0 NA NA NA NA NA 78 - -
Silver < 0.46 < 0.52 NA NA NA NA NA 78 - -
Thallium < 0.91 < 1.0 NA NA NA NA NA 1.0 - -
Zinc 145 378 NA NA NA NA NA 4,600 - -
Method 7471 (Mercury)0.035 0.14 NA NA NA 0.21 3.1 1.3 - -
Method 9071 (O&G)NA NA 6,920 NA NA < 104 867 - 250 -
Method 8015 (DRO)NA NA NA NA NA NA NA 40 10
Method 5035 (GRO)NA NA NA NA NA NA NA -1010
Notes: Concentrations reported in milligrams per kilogram (mg/Kg)
1Sample IDs actually use the following nomenclature; Example: Sample SB1 is acutally called SILV-SB1-06-09 in the laboratory reports
2Acetone is a common laboratory contaminant
NA = Not analyzed
NGE = No goal established
ft bls = Feet below land surface
DRO = Total Petroleum Hydrocarbons - Diesel Range Orgainics
GRO = Total Petroleum Hydrocarbons - Gasoline Range Orgainics
IHSB SRGs = Inactive Hazardous Sites Branch Health-Based Soil Remediation Goals
NCDENR Non-UST Action Levels = North Carolina Department of Natural Resources, Division of Waste Manangement, Non-UST Action Levels
NCDENR UST Action Levels = North Carolina Department of Natural Resources, Division of Waste Manangement, UST Action Levels
- = Not applicable
Concentrations in bold exceed exceed the corresponding SRG, NCDENR UST Action Limit or Non-UST Action Limit
Only Method 8260 and 8270 analytes detected above their respective laboratory reporting limits are presented on the table
NCDENR
UST Action
Levels
Table 1
Summary of Soil Analytical Data
Silverman Property
Asheville, North Carolina
S&ME Project No. 1411-09-025
NCDENR
Non-UST
Action
Levels
IHSB
SRGs
1 of 4
Sample ID1 SB8 SB9 SB10 SB11 SB13 SB14 SB15 SB17
Sample Date 6/30/2009 6/30/2009 6/30/2009 6/30/2009 7/1/2009 7/1/2009 7/1/2009 7/1/2009
Sample Time 10:30 11:35 12:05 12:15 14:15 14:05 13:55 13:45
Sample Depth (ft bls)0.5 - 1 0.5 - 1 0.5 - 1 0.5 - 1 9 - 10 5 - 6 4 - 5 8 - 9
Method 8260
Acetone2 < 0.139 NA NA < 0.125 NA NA NA NA 12,000 - -
Chloromethane < 0.0139 NA NA < 0.0125 NA NA NA NA 1.7 --
Methylene Chloride < 0.0278 NA NA < 0.0251 NA NA NA NA 1.1 --
Method 8270
1-Methylnaphthalene NA NA NA NA NA NA NA NA 22 --
2-Methylnaphthalene NA NA NA NA NA NA NA NA 62 --
Napthalene NA NA NA NA NA NA NA NA 3.9 --
Anthracene NA NA NA NA NA NA NA NA 3,400 --
Benzo(a)anthracene NA NA NA NA NA NA NA NA 0.15 --
Benzo(a)pyrene NA NA NA NA NA NA NA NA 0.015 --
Benzo(b)fluoranthene NA NA NA NA NA NA NA NA 0.15 --
Benzo(g,h,i)perylene NA NA NA NA NA NA NA NA NGE --
Benzo(k)fluoranthene NA NA NA NA NA NA NA NA 1.5 --
Chrysene NA NA NA NA NA NA NA NA 15 --
Fluoranthene NA NA NA NA NA NA NA NA 460 --
Phenanthrene NA NA NA NA NA NA NA NA NGE --
Pyrene NA NA NA NA NA NA NA NA 340 --
Fluorene NA NA NA NA NA NA NA NA 460 --
bis(2-Ethylhexyl)phthalate NA NA NA NA NA NA NA NA 35 --
Method 6010
Antimony NA NA NA NA NA NA NA NA 6.2 --
Arsenic NA NA NA NA NA NA NA NA 4.4 --
Beryllium NA NA NA NA NA NA NA NA 32 --
Cadmium NA NA NA NA NA NA NA NA 14 --
Chromium III 8.1 NA NA 28.7 NA NA NA NA 24,000 --
Copper NA NA NA NA NA NA NA NA 620 --
Lead 1,150 NA NA 6.1 NA NA NA NA 400 --
Manganese NA NA NA NA NA NA NA NA 360 --
Nickel NA NA NA NA NA NA NA NA 320 --
Selenium NA NA NA NA NA NA NA NA 78 --
Silver NA NA NA NA NA NA NA NA 78 --
Thallium NA NA NA NA NA NA NA NA 1.0 --
Zinc NA NA NA NA NA NA NA NA 4,600 --
Method 7471 (Mercury)NA NA NA NA NA NA NA NA 1.3 --
Method 9071 (O&G) 3,210 141 698 < 88.8 NA NA NA NA - 250 -
Method 8015 (DRO)NA NA NA NA < 32.1 181 < 6.8 < 6.4 40 10
Method 5035 (GRO)NA NA NA NA < 5.6 < 6.0 < 6.2 < 5.9 -10 10
Notes: Concentrations reported in milligrams per kilogram (mg/Kg)
1Sample IDs actually use the following nomenclature; Example: Sample SB1 is acutally called SILV-SB1-06-09 in the laboratory reports
2Acetone is a common laboratory contaminant
NA = Not analyzed
NGE = No goal established
ft bls = Feet below land surface
DRO = Total Petroleum Hydrocarbons - Diesel Range Orgainics
GRO = Total Petroleum Hydrocarbons - Gasoline Range Orgainics
IHSB SRGs = Inactive Hazardous Sites Branch Health-Based Soil Remediation Goals
NCDENR Non-UST Action Levels = North Carolina Department of Natural Resources, Division of Waste Manangement, Non-UST Action Levels
NCDENR UST Action Levels = North Carolina Department of Natural Resources, Division of Waste Manangement, UST Action Levels
- = Not applicable
Concentrations in bold exceed exceed the corresponding SRG, NCDENR UST Action Limit or Non-UST Action Limit
Only Method 8260 and 8270 analytes detected above their respective laboratory reporting limits are presented on the table
NCDENR
UST Action
Levels
Table 1
Summary of Soil Analytical Data
Silverman Property
Asheville, North Carolina
S&ME Project No. 1411-09-025
NCDENR
Non-UST
Action
Levels
IHSB
SRGs
2 of 4
Sample ID1 SB18 Duplicate 2 SB19 Duplicate 1 SB20 SB21 SB22 SB23
Sample Date 7/1/2009 7/1/2009 6/30/2009 6/30/2009 6/30/2009 6/30/2009 6/30/2009 6/30/2009
Sample Time 13:30 (SB18) 13:40 (SB-19) 14:45 15:00 15:30 15:50
Sample Depth (ft bls)9 - 10 9 - 10 0.5 - 1 0.5 - 1 0.5 - 1 0.5 - 1 0.5 - 1 0.5 - 1
Method 8260
Acetone2 NA NA < 0.0792 0.113 < 0.0927 0.172 < 0.106 < 0.0906 12,000 - -
Chloromethane NA NA < 0.0079 < 0.0101 < 0.0093 < 0.0128 < 0.0106 < 0.0091 1.7 --
Methylene Chloride NA NA < 0.0158 <0.0201 < 0.0185 < 0.0255 < 0.0212 < 0.0181 1.1 --
Method 8270
1-Methylnaphthalene NA NA < 0.358 < 0.365 < 0.351 < 0.352 0.549 0.46 22 --
2-Methylnaphthalene NA NA < 0.358 < 0.365 < 0.351 < 0.352 0.626 0.529 62 --
Napthalene NA NA < 0.358 < 0.365 < 0.351 < 0.352 0.557 0.434 3.9 --
Anthracene NA NA < 0.358 < 0.365 < 0.351 < 0.352 < 0.383 < 0.367 3,400 --
Benzo(a)anthracene NA NA < 0.358 < 0.365 < 0.351 < 0.352 < 0.383 < 0.367 0.15 --
Benzo(a)pyrene NA NA < 0.358 < 0.365 < 0.351 < 0.352 < 0.383 < 0.367 0.015 --
Benzo(b)fluoranthene NA NA < 0.358 < 0.365 < 0.351 < 0.352 < 0.383 0.385 0.15 --
Benzo(g,h,i)perylene NA NA < 0.358 < 0.365 < 0.351 < 0.352 < 0.383 < 0.367 NGE --
Benzo(k)fluoranthene NA NA < 0.358 < 0.365 < 0.351 < 0.352 < 0.383 0.453 1.5 --
Chrysene NA NA < 0.358 < 0.365 < 0.351 < 0.352 < 0.383 0.506 15 --
Fluoranthene NA NA < 0.358 < 0.365 < 0.351 < 0.352 < 0.383 0.703 460 --
Phenanthrene NA NA < 0.358 < 0.365 < 0.351 < 0.352 < 0.383 0.813 NGE --
Pyrene NA NA < 0.358 < 0.365 < 0.351 < 0.352 < 0.383 1.38 340 --
Fluorene NA NA < 0.358 < 0.365 < 0.351 < 0.352 < 0.383 < 0.367 460 --
bis(2-Ethylhexyl)phthalate NA NA < 0.358 < 0.365 < 0.351 < 0.352 < 0.383 < 0.367 35 --
Method 6010
Antimony NA NA 1.5 1.5 8.6 1.6 8.2 3.2 6.2 --
Arsenic NA NA 0.51 < 0.44 5.7 < 0.36 6.3 3.1 4.4 --
Beryllium NA NA 0.22 0.17 0.66 0.31 0.72 0.78 32 --
Cadmium NA NA 1.2 1.1 11 2.5 8.7 3.5 14 --
Chromium NA NA 18.7 19.6 42.4 21.9 118 30 24,000 --
Copper NA NA 21.7 19.3 596 25 92.7 90.5 620 --
Lead NA NA 101 39.4 1,220 39.4 212 149 400 --
Manganese NA NA 237 222 464 272 482 440 360 --
Nickel NA NA 8.8 8.2 25.7 11.5 43.4 19.3 320 --
Selenium NA NA < 1.0 1.6 1.9 0.84 3.0 1.7 78 --
Silver NA NA < 0.50 < 0.44 < 0.40 < 0.36 < 0.52 < 0.51 78 --
Thallium NA NA < 1.0 < 0.88 0.91 1.0 < 1.0 < 1.0 1.0 --
Zinc NA NA 78.5 64.4 2,300 138 808 547 4,600 --
Method 7471 (Mercury)NA NA 0.04 0.0084 1.0 0.054 0.51 0.31 1.3 --
Method 9071 (O&G)NA NA 847 490 103 235 221 1,240 - 250 -
Method 8015 (DRO) 769 590 39.1 35 < 5.3 12.1 65.3 151 40 10
Method 5035 (GRO)< 6.2 < 5.2 < 7.6 < 6.3 < 5.2 <11.4 < 9.4 < 6.5 -10 10
Notes: Concentrations reported in milligrams per kilogram (mg/Kg)
1Sample IDs actually use the following nomenclature; Example: Sample SB1 is acutally called SILV-SB1-06-09 in the laboratory reports
2Acetone is a common laboratory contaminant
NA = Not analyzed
NGE = No goal established
ft bls = Feet below land surface
DRO = Total Petroleum Hydrocarbons - Diesel Range Orgainics
GRO = Total Petroleum Hydrocarbons - Gasoline Range Orgainics
IHSB SRGs = Inactive Hazardous Sites Branch Health-Based Soil Remediation Goals
NCDENR Non-UST Action Levels = North Carolina Department of Natural Resources, Division of Waste Manangement, Non-UST Action Levels
NCDENR UST Action Levels = North Carolina Department of Natural Resources, Division of Waste Manangement, UST Action Levels
- = Not applicable
Concentrations in bold exceed exceed the corresponding SRG, NCDENR UST Action Limit or Non-UST Action Limit
Only Method 8260 and 8270 analytes detected above their respective laboratory reporting limits are presented on the table
NCDENR
UST Action
Levels
Table 1
Summary of Soil Analytical Data
Silverman Property
Asheville, North Carolina
S&ME Project No. 1411-09-025
NCDENR
Non-UST
Action
Levels
IHSB
SRGs
3 of 4
Sample ID1 SB24 SB25 SB26 SB27 TW3-SS1 TW3-SS2 Duplicate 1
Sample Date 6/30/2009 6/30/2009 6/30/2009 6/30/2009 7/1/2009 7/1/2009 7/1/2009
Sample Time 16:10 16:55 16:25 16:40 11:45 11:50 (TW3-SS2)
Sample Depth (ft bls)0.5 - 1 0.5 - 1 0.5 - 1 0.5 - 1 1 - 2 9 - 10 9 - 10
Method 8260
Acetone2 < 0.10 0.222 NA NA 0.0963 0.0904 0.0915 12,000 - -
Chloromethane < 0.010 < 0.0109 NA NA 0.0096 0.0090 0.0092 1.7 - -
Methylene Chloride < 0.020 < 0.0219 NA NA 0.0193 0.0181 0.0183 1.1 - -
Method 8270
1-Methylnaphthalene < 0.384 < 0.354 NA NA NA NA NA 22 - -
2-Methylnaphthalene < 0.384 < 0.354 NA NA NA NA NA 62 - -
Napthalene < 0.384 < 0.354 NA NA NA NA NA 3.9 - -
Anthracene 1.24 < 0.354 NA NA NA NA NA 3,400 - -
Benzo(a)anthracene 2.31 < 0.354 NA NA NA NA NA 0.15 - -
Benzo(a)pyrene 2.85 < 0.354 NA NA NA NA NA 0.015 - -
Benzo(b)fluoranthene 1.60 < 0.354 NA NA NA NA NA 0.15 - -
Benzo(g,h,i)perylene 0.99 < 0.354 NA NA NA NA NA NGE - -
Benzo(k)fluoranthene 1.83 < 0.354 NA NA NA NA NA 1.5 - -
Chrysene 2.67 < 0.354 NA NA NA NA NA 15 - -
Fluoranthene 6.76 < 0.354 NA NA NA NA NA 460 - -
Phenanthrene 8.23 < 0.354 NA NA NA NA NA NGE - -
Pyrene 8.92 0.416 NA NA NA NA NA 340 - -
Fluorene 0.578 < 0.354 NA NA NA NA NA 460 - -
bis(2-Ethylhexyl)phthalate < 0.384 0.498 NA NA NA NA NA 35 - -
Method 6010
Antimony 7.3 1.2 NA NA NA NA NA 6.2 - -
Arsenic 2.4 < 0.49 NA NA NA NA NA 4.4 - -
Beryllium 0.64 0.36 NA NA NA NA NA 32 - -
Cadmium 2.6 1.2 NA NA NA NA NA 14 - -
Chromium III 42.3 17.7 NA NA NA NA NA 24,000 - -
Copper 146 18.9 NA NA NA NA NA 620 - -
Lead 522 59.1 NA NA 6.9 3.4 4.1 400 - -
Manganese 440 371 NA NA NA NA NA 360 - -
Nickel 15.0 10.6 NA NA NA NA NA 320 - -
Selenium 1.9 1.6 NA NA NA NA NA 78 - -
Silver < 0.56 < 0.49 NA NA NA NA NA 78 - -
Thallium 1.1 < 0.97 NA NA NA NA NA 1.0 - -
Zinc 675 138 NA NA NA NA NA 4,600 - -
Method 7471 (Mercury)0.099 0.032 NA NA NA NA NA 1.3 - -
Method 9071 (O&G) 586 3,850 NA NA NA NA NA - 250 -
Method 8015 (DRO) 40.4 1,080 19.9 56.2 NA NA NA 40 10
Method 5035 (GRO)< 9.8 < 7.6 < 5.3 < 8.6 NA NA NA -10 10
Notes: Concentrations reported in milligrams per kilogram (mg/Kg)
1Sample IDs actually use the following nomenclature; Example: Sample SB1 is acutally called SILV-SB1-06-09 in the laboratory reports
2Acetone is a common laboratory contaminant
ND = Not detected
NA = Not analyzed
NGE = No goal established
ft bls = Feet below land surface
DRO = Total Petroleum Hydrocarbons - Diesel Range Orgainics
GRO = Total Petroleum Hydrocarbons - Gasoline Range Orgainics
IHSB SRGs = Inactive Hazardous Sites Branch Health-Based Soil Remediation Goals
NCDENR Non-UST Action Levels = North Carolina Department of Natural Resources, Division of Waste Manangement, Non-UST Action Levels
NCDENR UST Action Levels = North Carolina Department of Natural Resources, Division of Waste Manangement, UST Action Levels
- = Not applicable
Concentrations in bold exceed exceed the corresponding SRG, NCDENR UST Action Limit or Non-UST Action Limit
Only Method 8260 and 8270 analytes detected above their respective laboratory reporting limits are presented on the table
NCDENR
UST Action
Levels
Table 1
Summary of Soil Analytical Data
Silverman Property
Asheville, North Carolina
S&ME Project No. 1411-09-025
NCDENR
Non-UST
Action
Levels
IHSB
SRGs
4 of 4
We
l
l

I
D
In
s
t
a
l
l
a
t
i
o
n

Da
t
e
We
l
l

Di
a
m
e
t
e
r

(i
n
c
h
e
s
)
To
t
a
l

D
e
p th

(f
t

b
e
l
o
w

T
O
C
)
TO
C

E
l
e
v
a
t
i
o
n
1

(f
t

a
b
o
v
e

d
a
t
u
m
)
Gr
o
u
n
d

S
u
r
f
a
c
e

El
e
v
a
t
i
o
n
1

(f
t

a
b
o
v
e

d
a
t
u
m
)
To
p

o
f

S
c
r
e
e
n

El
e
v
a
t
i
o
n

(f
t

a
b
o
v
e

d
a
t
u
m
)
Bo
t
t
o
m

o
f

S
c
r
e
e
n

El
e
v
a
t
i
o
n

(f
t

a
b
o
v
e

d
a
t
u
m
)
De
p
t
h

t
o

W
a
t
e
r

fr
o
m

T
O
C

(f
e
e
t
)
Gr
o
u
n
d
w
a
t
e
r

El
e
v
a
t
i
o
n

(f
t

a
b
o
v
e

d
a
t
u
m
)
TW
-
1

7
/
1
/
2
0
0
9

1
14
.
8
1
99
.
7
9
98
.
6
8
94
.
9
8
84
.
9
8
13
.
5
6
86
.
2
3
TW
-
2

7
/
1
/
2
0
0
9

1
12
.
7
2
98
.
9
3
98
.
2
3
96
.
2
1
86
.
2
1
7.
4
2
91
.
5
1
TW
-
3

7
/
1
/
2
0
0
9

1
14
.
9
5
98
.
4
9
98
.
2
3
88
.
5
4
83
.
5
4
11
.
0
0
87
.
4
9
TW
-
4

7
/
1
/
2
0
0
9

1
14
.
8
0
99
.
4
1
98
.
4
2
94
.
6
1
84
.
6
1
13
.
0
5
86
.
3
6
TW
-
5

7
/
1
/
2
0
0
9

1
16
.
6
0
98
.
6
9
98
.
8
4
92
.
0
9
82
.
0
9
10
.
9
4
87
.
7
5
TW
-
6

7
/
1
/
2
0
0
9

1
14
.
8
2
10
0
.
2
5
99
.
6
1
95
.
4
3
85
.
4
3
13
.
1
4
87
.
1
1
No
t
e
s
:

T
O
C

=

T
o
p

o
f

c
a
s
i
n
g

f
t

=

f
e
e
t

1
El
e
v
a
t
i
o
n
s

p
r
o
v
i
d
e
d

b
a
s
e
d

o
n

r
e
l
a
t
i
v
e

d
a
t
u
m

e
s
t
a
b
l
i
s
h
e
d

o
n
s
i
t
e

D
e
p
t
h

t
o

g
r
o
u
n
d
w
a
t
e
r

m
e
a
s
u
r
e
m
e
n
t
s

t
a
k
e
n

o
n

7
-
2
-
0
9
S&
M
E

P
r
o
j
e
c
t

N
o
.

1
4
1
1
-
0
9
-
0
2
5
Ta
b
l
e

2
We
l
l

C
o
n
s
t
r
u
c
t
i
o
n

a
n
d

G
r
o
u
n
d
w
a
t
e
r

E
l
e
v
a
t
i
o
n

D
a
t
a
Si
l
v
e
r
m
a
n

P
r
o
p
e
r
t
y
As
h
e
v
i
l
l
e
,

N
o
r
t
h

C
a
r
o
l
i
n
a
Sa
m
p
l
e

I
D
1
TW
-
1
TW
-
3

T
W
-
4

T
W
-
5

D
u
p
l
i
c
a
t
e

1
TW
-
6
Sa
m
p
l
e

D
a
t
e
7/
2
/
2
0
0
9

7
/
2
/
2
0
0
9

7
/
2
/
2
0
0
9

7
/
2
/
2
0
0
9

7
/
2
/
2
0
0
9

7
/
2
/
2
0
0
9
Sa
m
p
l
e

T
i
m
e
8:
3
0
11
:
1
5
10
:
1
5

1
3
:
0
0

(
T
W
-
5
)

1
3
:
4
5
Me
t
h
o
d

8
2
6
0
ci
s
-
1
,
2
-
D
i
c
h
l
o
r
o
e
t
h
e
n
e
<
1
.
0

1
.
4

<

1
.
0

<

1
.
0

<

1
.
0

<

1
.
0
70
MT
B
E

<

1
.
0

<

1
.
0

<

1
.
0

<

1
.
0

1
.
0

<

1
.
0
20
0
Me
t
h
o
d

8
2
7
0
ND

N
D

N
D

N
D

N
D

N
D
-
Le
a
d
NA
85
.
4
NA

N
A

N
A

N
A
15
No
t
e
s
:

C
o
n
c
e
n
t
r
a
t
i
o
n
s

r
e
p
o
r
t
e
d

i
n

m
i
c
r
o
g
r
a
m
s

p
e
r

l
i
t
e
r

(
μ g/
L
)

1 Sa
m
p
l
e

I
D
s

a
c
t
u
a
l
l
y

u
s
e

t
h
e

f
o
l
l
o
w
i
n
g

n
o
m
e
n
c
l
a
t
u
r
e
;

E
x
a
m
p
l
e
:

S
a
m
p
l
e

T
W
-
1

i
s

a
c
u
t
a
l
l
y

c
a
l
l
e
d

S
I
L
V
-
T
W
-
1
-
0
7
-
0
9

i
n

t
h
e

l
a
b
o
r
a
t
o
r
y

r
e
p
o
r
t
s
.

N
D

=

N
o
t

d
e
t
e
c
t
e
d

N
A

=

N
o
t

a
n
a
l
y
z
e
d

M
T
B
E

=

M
e
t
h
y
l
-
t
e
r
t
-
b
u
t
y
l

e
t
h
e
r

C
o
n
c
e
n
t
r
a
t
i
o
n
s

i
n

bo
l
d
e
x
c
e
e
d

t
h
e

N
C
A
C

2
L

G
r
o
u
n
d
w
a
t
e
r

Q
u
a
l
i
t
y

S
t
a
n
d
a
r
d
s

N
C
A
C

2
L

S
t
a
n
d
a
r
d
s

=

N
o
r
t
h

C
a
r
o
l
i
n
a

G
r
o
u
n
d
w
a
t
e
r

Q
u
a
l
i
t
y

S
t
a
n
d
a
r
d
s

-

=

N
o
t

a
p
p
l
i
c
a
b
l
e

O
n
l
y

M
e
t
h
o
d

8
2
6
0

a
n
d

8
2
7
0

a
n
a
l
y
t
e
s

d
e
t
e
c
t
e
d

a
b
o
v
e

t
h
e
i
r

r
e
s
p
e
c
t
i
v
e

l
a
b
o
r
a
t
o
r
y

r
e
p
o
r
t
i
n
g

l
i
m
i
t
s

a
r
e

p
r
e
s
e
n
t
e
d

o
n

t
h
e

t
a
b
l
e
S&
M
E

P
r
o
j
e
c
t

N
o
.

1
4
1
1
-
0
9
-
0
2
5
NC
A
C

2
L

St
a
n
d
a
r
d
s
Ta
b
l
e

3
Su
m
m
a
r
y

o
f

G
r
o
u
n
d
w
a
t
e
r

A
n
a
l
y
t
i
c
a
l

D
a
t
a
Si
l
v
e
r
m
a
n

P
r
o
p
e
r
t
y
As
h
e
v
i
l
l
e
,

N
o
r
t
h

C
a
r
o
l
i
n
a
Sa
m
p
l
e

I
D
1
Eq
u
i
p

R
i
n
s
a
t
e

T
r
i
p

B
l
a
n
k

1

T
r
i
p

B
l
a
n
k

2

T
r
i
p

B
l
a
n
k

3

E
q
u
i
p

R
i
n
s
a
t
e

T
r
i
p

B
l
a
n
k

1

F
i
e
l
d

B
l
a
n
k

T
r
i
p

B
l
a
n
k

1
Sa
m
p
l
e

D
a
t
e
6/
3
0
/
2
0
0
9

6
/
3
0
/
2
0
0
9

6
/
3
0
/
2
0
0
9

6
/
3
0
/
2
0
0
9

7
/
1
/
2
0
0
9

7
/
1
/
2
0
0
9

7
/
2
/
2
0
0
9

7
/
2
/
2
0
0
9
Sa
m
p
l
e

T
i
m
e
14
:
2
0

-

-

-

1
2
:
4
5

-

8
:
1
5

-
Me
t
h
o
d

8
2
6
0
ND

N
D

N
D

N
D

N
D

N
D

N
D

N
D
-
Me
t
h
o
d

8
2
7
0
ND

N
A

N
A

N
A

N
A

N
A

N
A

N
A
-
Me
t
h
o
d

2
0
0
.
7
An
t
i
m
o
n
y

<

5
.
0

N
A

N
A

N
A

N
A

N
A

N
A

N
A
NS
E
Ar
s
e
n
i
c

<
5
.
0

N
A

N
A

N
A

N
A

N
A

N
A

N
A
50
Be
r
y
l
l
i
u
m

<
1
.
0

N
A

N
A

N
A

N
A

N
A

N
A

N
A
NS
E
Ca
d
m
i
u
m

<

5
.
0

N
A

N
A

N
A

N
A

N
A

N
A

N
A
1.
7
5
Ch
r
o
m
i
u
m
*

<
5
.
0

N
A

N
A

N
A

N
A

N
A

N
A

N
A
50
Co
p
p
e
r

<

5
.
0

N
A

N
A

N
A

N
A

N
A

N
A

N
A
1,
0
0
0
Le
a
d

<
5
.
0

N
A

N
A

N
A

<

5
.
0

N
A

N
A

N
A
15
Ma
n
g
a
n
e
s
e

<

5
.
0

N
A

N
A

N
A

N
A

N
A

N
A

N
A
50
Ni
c
k
e
l

<

5
.
0

N
A

N
A

N
A

N
A

N
A

N
A

N
A
10
0
Se
l
e
n
i
u
m

<

1
0
.
0

N
A

N
A

N
A

N
A

N
A

N
A

N
A
50
Si
l
v
e
r

<

5
.
0

N
A

N
A

N
A

N
A

N
A

N
A

N
A
17
.
5
Th
a
l
l
i
u
m

<

1
0
.
0

N
A

N
A

N
A

N
A

N
A

N
A

N
A
NS
E
Zi
n
c

<

1
0
.
0

N
A

N
A

N
A

N
A

N
A

N
A

N
A
1,
0
5
0
Me
t
h
o
d

7
4
7
1

(
M
e
r
c
u
r
y
)
<
0
.
2
0

N
A

N
A

N
A

N
A

N
A

N
A

N
A
1.
0
5
Me
t
h
o
d

9
0
7
1

(
O
&
G
)
<
5
,
0
0
0

N
A

N
A

N
A

N
A

N
A

N
A

N
A
NS
E
Me
t
h
o
d

8
0
1
5

(
D
R
O
)
<
1
0
0

N
A

N
A

N
A

N
A

N
A

N
A

N
A
NS
E
Me
t
h
o
d

5
0
3
5

(
G
R
O
)
<
8
0

N
A

N
A

N
A

N
A

N
A

N
A

N
A
NS
E
No
t
e
s
:

C
o
n
c
e
n
t
r
a
t
i
o
n
s

r
e
p
o
r
t
e
d

i
n

m
i
c
r
o
g
r
a
m
s

p
e
r

l
i
t
e
r

(
μ g/
L
)

1 Sa
m
p
l
e

I
D
s

a
c
t
u
a
l
l
y

u
s
e

t
h
e

f
o
l
l
o
w
i
n
g

n
o
m
e
n
c
l
a
t
u
r
e
;

E
x
a
m
p
l
e
:

S
a
m
p
l
e

T
r
i
p

B
l
a
n
k

1

i
s

a
c
u
t
a
l
l
y

c
a
l
l
e
d

S
I
L
V
-
T
r
i
p

B
l
a
n
k

1
-
0
6
-
0
9

i
n

t
h
e

l
a
b
o
r
a
t
o
r
y

r
e
p
o
r
t
s
.

N
D

=

N
o
t

d
e
t
e
c
t
e
d

N
A

=

N
o
t

a
n
a
l
y
z
e
d

N
S
E

=

N
o

s
t
a
n
d
a
r
d

e
s
t
a
b
i
l
i
s
h
e
d

C
o
n
c
e
n
t
r
a
t
i
o
n
s

i
n

bo
l
d
e
x
c
e
e
d

t
h
e

N
C
A
C

2
L

G
r
o
u
n
d
w
a
t
e
r

Q
u
a
l
i
t
y

S
t
a
n
d
a
r
d
s

N
C
A
C

2
L

S
t
a
n
d
a
r
d
s

=

N
o
r
t
h

C
a
r
o
l
i
n
a

G
r
o
u
n
d
w
a
t
e
r

Q
u
a
l
i
t
y

S
t
a
n
d
a
r
d
s

-

=

N
o
t

a
p
p
l
i
c
a
b
l
e
S&
M
E

P
r
o
j
e
c
t

N
o
.

1
4
1
1
-
0
9
-
0
2
5
NC
A
C

2
L

St
a
n
d
a
r
d
s
Ta
b
l
e

4
Su
m
m
a
r
y

o
f

Q
u
a
l
i
t
y

C
o
n
t
r
o
l

A
n
a
l
y
t
i
c
a
l

D
a
t
a
Si
l
v
e
r
m
a
n

P
r
o
p
e
r
t
y
As
h
e
v
i
l
l
e
,

N
o
r
t
h

C
a
r
o
l
i
n
a
SC
A
L
E
:
As

s
h
o
w
n
Pr
o
j
e
c
t

L
o
c
a
t
i
o
n

M
a
p
FI
G
U
R
E

N
O
.
CH
E
C
K
E
D

B
Y
:

WH
W
Si
l
v
e
r
m
a
n

P
r
o
p
e
r
t
y
So
u
r
c
e

o
f

S
t
r
e
e
t

M
a
p
:

h
t
t
p
:
/
/
w
w
w
.
m
a
p
q
u
e
s
t
.
c
o
m
/

DR
A
W
N

B
Y
:
SA
S
48

S
w
a
n
n
a
n
o
a

R
i
v
e
r

R
d
,

A
s
h
e
v
i
l
l
e
,

N
C
DA
T
E
:
8/
2
5
/
2
0
0
8
JO
B

N
O
.
14
1
1
-
0
9
-
0
2
5
1
SU
B
J
E
C
T

SI
T
E
Sw
a
n
n
a
n
o
a

R
i
v
e
r

R
o
a
d
N OT
E
:

P
r
o
p
e
r
t
y

b
o
u
n
d
a
r
i
e
s

ap
p
r
o
x
i
m
a
t
e
d
.

F
o
r

v
i
s
u
a
l
i
z
a
t
i
o
n
SC
A
L
E
:
As

s
h
o
w
n
Si
t
e

P
l
a
n
FI
G
U
R
E

N
O
.
pu
r
p
o
s
e
s

o
n
l
y
.

2
0
0
6

A
e
r
i
a
l

P
h
o
t
o
g
r
a
p
h
CH
E
C
K
E
D

B
Y
:

WH
W
Si
l
v
e
r
m
a
n

P
r
o
p
e
r
t
y
So
u
r
c
e

o
f

A
e
r
i
a
l

P
h
o
t
o
g
r
a
p
h
:

B
u
n
c
o
m
b
e

C
o
u
n
t
y

G
I
S
DR
A
W
N

B
Y
:
SA
S
48

S
w
a
n
n
a
n
o
a

R
i
v
e
r

R
d
,

A
s
h
e
v
i
l
l
e
,

N
C
P
r
o
p
e
r
t
y

I
n
f
o
r
m
a
t
i
o
n

S
y
s
t
e
m
DA
T
E
:
9/
2
2
/
2
0
0
8
JO
B

N
O
.
14
1
1
-
0
9
-
0
2
5
2
Fl
a
g

s
t
a
n
d

an
d

O
f
f
i
c
e
Pa
i
n
t

B
o
o
t
h

an
d

S
h
o
p
Pa
i
n
t

M
i
x
i
n
g

Ro
o
m
Go
-
c
a
r
t

Tr
a
c
k
St
o
r
a
g
e

Bu
i
l
d
i
n
g
Me
t
a
l

C
a
n
o
p
y
Sa
n
d
b
l
a
s
t
i
n
g

Bo
o
t
h
Fa
b
r
i
c
a
t
i
o
n

Bu
i
l
d
i
n
g
Ga
r
a
g
e
s

w
i
t
h

at
t
a
c
h
e
d

A
p
a
r
t
m
e
n
t
Sw
a
n
n
a
n
o
a

R
i
v
e
r
Po
t
e
n
t
i
a
l

US
T
s
De
b
r
i
s

P
i
l
e
s
De
b
r
i
s

Pi
l
e
Po
l
e
-
m
o
u
n
t
e
d

Tr
a
n
s
f
o
r
m
e
r
s
Fo
r
m
e
r

U
S
T

a
n
d

Ga
s
o
l
i
n
e

T
a
n
k
Ap
p
r
o
x
i
m
a
t
e

S
i
t
e

Bo
u
n
d
a
r
y
Du
m
p
s
t
e
r

a
n
d

Ro
l
l
o
f
f

B
o
x
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

I-1
APPENDIX I
(WELL CONSTRUCTION LOGS)

SY
M
B
O
L
STRATA
EL
E
V
A
T
I
O
N
(f
t
.
)
WELL
DETAILS
DE
P
T
H
(f
t
.
)
None
Type:
Interval:None
FILTERPACK
Probe Technology
Direct push with a 2.25 inch diameter Macrocore
7/1/09
Diameter:
Type:
Interval:
Diameter:
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE DRILLED:
Brown to Gray
Gravely Fine toMedium SAND
Brown to RedMicaceous Sandy
SILT
Brown Silty FineSAND with Gravel
TSC
TD
DE
P
T
H
(f
t
.
)
2.00
4.00
14.00
LE
G
E
N
D
DESCRIPTION WELL CONSTRUCTION DETAILS
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
LOGGED BY:
0.010"PVC
4.0 - 14.0
SEAL
TOP OF CASING
GROUND SURFACEBENTONITE SEAL
FILTER PACKTOP OF SCREENBOTTOM OF SCREEN
TOTAL DEPTHCEMENT GROUT
FILTER PACK
BENTONITE
CEMENT GROUT
CUTTINGS / BACKFILL
STATIC WATER LEVEL
LEGEND
0
5
10
COMPLETION REPORT OF
WELL No. TW-1
TOC
GSBS
FPTSCBSC
TDCG
MO
N
I
T
O
R
I
N
G

W
E
L
L

W
E
L
L

L
O
G
S
.
G
P
J

S
&
M
E
.
G
D
T

8
/
2
5
/
0
9
Sheet 1 of 1
Type:
Interval:
0.00
MSL
S. Spinner
RISER CASING
GROUT
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
SCREEN
Bentonite2.0 - 4.0
GS
COMPLETION REPORT OF WELL No. TW-1
PROJECT:
PROJECT NO:
PROJECT LOCATION:
1"
PVC
-2.0 - 4.0
Silverman Property1411-09-025
Asheville, NC
Sheet 1 of 1
12.45 feet BG (24 hour)WATER LEVEL:
EL
E
V
A
T
I
O
N
(f
t
.
)
WELL
DETAILS
SY
M
B
O
L
None
Type:
Interval:None
FILTERPACK
Probe Technology
Direct push with a 2.25 inch diameter Macrocore
7/1/09
Diameter:
Type:
Interval:
Diameter:
Type:
Interval:
SEAL
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
LOGGED BY:
Brown Gravely Fine to
Medium SAND
Brown Gravely,micaceous Sandy
SILT
Brown Silty Fine
SAND
TSC
TD
STRATA
0.010"PVC
1.0 - 11.0
1.00
11.00
LE
G
E
N
D
DESCRIPTION WELL CONSTRUCTION DETAILS
DE
P
T
H
(f
t
.
)DE
P
T
H
(f
t
.
)
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE DRILLED:
TOP OF CASING
GROUND SURFACEBENTONITE SEAL
FILTER PACKTOP OF SCREENBOTTOM OF SCREEN
TOTAL DEPTHCEMENT GROUT
FILTER PACK
BENTONITE
CEMENT GROUT
CUTTINGS / BACKFILL
STATIC WATER LEVEL
1"
PVC
-2.0 - 1.0
LEGEND
0
5
10
COMPLETION REPORT OF
WELL No. TW-2
TOC
GSBS
FPTSCBSC
TDCG
MO
N
I
T
O
R
I
N
G

W
E
L
L

W
E
L
L

L
O
G
S
.
G
P
J

S
&
M
E
.
G
D
T

8
/
2
5
/
0
9
Sheet 1 of 1
GS
Type:
Interval:
SCREEN
Bentonite0.0 - 1.0
0.00
MSL
S. Spinner
RISER CASING
GROUT
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
COMPLETION REPORT OF WELL No. TW-2
PROJECT:
PROJECT NO:
PROJECT LOCATION:
Silverman Property1411-09-025
Asheville, NC
Sheet 1 of 1
6.72 feet BG (24 hour)WATER LEVEL:
SY
M
B
O
L
STRATA
EL
E
V
A
T
I
O
N
(f
t
.
)
WELL
DETAILS
DE
P
T
H
(f
t
.
)
None
Type:
Interval:10.0 - 15.0
FILTERPACK
Probe Technology
Direct push with a 2.25 inch diameter Macrocore
7/1/09
Diameter:
Type:
Interval:
Diameter:
Type:
Interval:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE DRILLED:
Brown Gravely
Medium SAND
Brown MicaceousSandy SILT
Brown MicaceousSilty Fine to MediumSAND
TSC
TD
DE
P
T
H
(f
t
.
)
8.00
10.00
15.00
LE
G
E
N
D
DESCRIPTION WELL CONSTRUCTION DETAILS
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
LOGGED BY:
0.010"Prepacked Well Screen
10.0 - 15.0
SEAL
TOP OF CASING
GROUND SURFACEBENTONITE SEAL
FILTER PACKTOP OF SCREENBOTTOM OF SCREEN
TOTAL DEPTHCEMENT GROUT
FILTER PACK
BENTONITE
CEMENT GROUT
CUTTINGS / BACKFILL
STATIC WATER LEVEL
LEGEND
0
5
10
COMPLETION REPORT OF
WELL No. TW-3
TOC
GSBS
FPTSCBSC
TDCG
MO
N
I
T
O
R
I
N
G

W
E
L
L

W
E
L
L

L
O
G
S
.
G
P
J

S
&
M
E
.
G
D
T

8
/
2
5
/
0
9
Sheet 1 of 1
Type:
Interval:
0.00
MSL
S. Spinner
RISER CASING
GROUT
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
SCREEN
Bentonite8.0 - 10.0
GS
COMPLETION REPORT OF WELL No. TW-3
PROJECT:
PROJECT NO:
PROJECT LOCATION:
1"
PVC
-2.0 - 10.0
Silverman Property1411-09-025
Asheville, NC
Sheet 1 of 1
10.74 feet BG (24 hour)WATER LEVEL:
Diameter:
Type:
Interval:
WELL CONSTRUCTION DETAILS
DE
P
T
H
(f
t
.
)DE
P
T
H
(f
t
.
)
SY
M
B
O
L
STRATA
EL
E
V
A
T
I
O
N
(f
t
.
)
WELL
DETAILSDESCRIPTION
LE
G
E
N
D
None
Type:
Interval:None
Probe Technology
Direct push with a 2.25 inch diameter Macrocore
7/1/09
Brown Gravely Silty
SAND
Brown MicaceousSandy SILT
Brown Micaceous
Silty Fine SAND
Brown Micaceous
Sandy SILT
Alluvium:TD
Diameter:
Type:
Interval:
2.00
4.00
14.00
TSC
LEGEND
SEAL
FILTERPACK
TOP OF CASING
GROUND SURFACEBENTONITE SEAL
FILTER PACKTOP OF SCREENBOTTOM OF SCREEN
TOTAL DEPTHCEMENT GROUT
0
5
10
COMPLETION REPORT OF
WELL No. TW-4
TOC
GSBS
FPTSCBSC
TDCG
MO
N
I
T
O
R
I
N
G

W
E
L
L

W
E
L
L

L
O
G
S
.
G
P
J

S
&
M
E
.
G
D
T

8
/
2
5
/
0
9
Sheet 1 of 1
FILTER PACK
BENTONITE
CEMENT GROUT
CUTTINGS / BACKFILL
STATIC WATER LEVEL
Bentonite2.0 - 4.0Type:
Interval:
Diameter:
Type:
Interval:
GROUT
RISER CASING
0.00
COMPLETION REPORT OF WELL No. TW-4
SCREEN
Type:
Interval:
1"
PVC
-2.0 - 4.0
0.010"PVC
4.0 - 14.0
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
LOGGED BY:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE DRILLED:MSL
S. Spinner
Sheet 1 of 1
GS
PROJECT:
PROJECT NO:
PROJECT LOCATION:
Silverman Property1411-09-025
Asheville, NC
PROTECTIVE CASING
WATER LEVEL:12.06 feet BG (24 hour)
Diameter:
Type:
Interval:
WELL CONSTRUCTION DETAILS
DE
P
T
H
(f
t
.
)DE
P
T
H
(f
t
.
)
SY
M
B
O
L
STRATA
EL
E
V
A
T
I
O
N
(f
t
.
)
WELL
DETAILSDESCRIPTION
LE
G
E
N
D
None
Type:
Interval:None
Probe Technology
Direct push with a 2.25 inch diameter Macrocore
7/1/09
Asphalt
Tan Micaceous
Sandy SILT
Tan Micaceous SiltyFine to Medium
SAND
Tan MicaceousSandy SILT
Tan Micaceous SiltyFine to MediumSAND
TD
Diameter:
Type:
Interval:
6.00
8.00
18.00
TSC
LEGEND
SEAL
FILTERPACK
TOP OF CASING
GROUND SURFACEBENTONITE SEAL
FILTER PACKTOP OF SCREENBOTTOM OF SCREEN
TOTAL DEPTHCEMENT GROUT
0
5
10
15
COMPLETION REPORT OF
WELL No. TW-5
TOC
GSBS
FPTSCBSC
TDCG
MO
N
I
T
O
R
I
N
G

W
E
L
L

W
E
L
L

L
O
G
S
.
G
P
J

S
&
M
E
.
G
D
T

8
/
2
5
/
0
9
Sheet 1 of 1
FILTER PACK
BENTONITE
CEMENT GROUT
CUTTINGS / BACKFILL
STATIC WATER LEVEL
Bentonite6.0 - 8.0Type:
Interval:
Diameter:
Type:
Interval:
GROUT
RISER CASING
0.00
COMPLETION REPORT OF WELL No. TW-5
SCREEN
Type:
Interval:
1"
PVC
-2.0 - 8.0
0.010"PVC
8.0 - 18.0
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
LOGGED BY:
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE DRILLED:MSL
S. Spinner
Sheet 1 of 1
GS
PROJECT:
PROJECT NO:
PROJECT LOCATION:
Silverman Property1411-09-025
Asheville, NC
PROTECTIVE CASING
WATER LEVEL:11.09 feet BG (24 hour)
None
EL
E
V
A
T
I
O
N
(f
t
.
)
WELL
DETAILS
STRATA
SY
M
B
O
L
Type:
Interval:None
FILTERPACK
Probe Technology
Direct push with a 2.25 inch diameter Macrocore
7/1/09
Diameter:
Type:
Interval:
Diameter:
Type:
Interval:
SEAL
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE DRILLED:
0.010"PVC
4.0 - 14.0
Brown Micaceous
Sandy SILT
Brown MicaceousSilty Fine to MediumSAND
TSC
TD
1"
PVC
-2.0 - 4.0
2.00
4.00
14.00
LE
G
E
N
D
DESCRIPTION WELL CONSTRUCTION DETAILS
DE
P
T
H
(f
t
.
)DE
P
T
H
(f
t
.
)
LATITUDE:
LONGITUDE:
TOP OF CASING ELEVATION:
DATUM:
LOGGED BY:
TOP OF CASING
GROUND SURFACEBENTONITE SEAL
FILTER PACKTOP OF SCREENBOTTOM OF SCREEN
TOTAL DEPTHCEMENT GROUT
FILTER PACK
BENTONITE
CEMENT GROUT
CUTTINGS / BACKFILL
STATIC WATER LEVEL
Type:
Interval:
LEGEND
0
5
10
15
COMPLETION REPORT OF
WELL No. TW-6
TOC
GSBS
FPTSCBSC
TDCG
MO
N
I
T
O
R
I
N
G

W
E
L
L

W
E
L
L

L
O
G
S
.
G
P
J

S
&
M
E
.
G
D
T

8
/
2
5
/
0
9
Sheet 1 of 1
GS
SCREEN
Bentonite2.0 - 4.0
0.00
MSL
S. Spinner
RISER CASING
GROUT
Diameter:
Type:
Interval:
Type:
Interval:
PROTECTIVE CASING
COMPLETION REPORT OF WELL No. TW-6
PROJECT:
PROJECT NO:
PROJECT LOCATION:
Silverman Property1411-09-025
Asheville, NC
Sheet 1 of 1
12.50 feet BG (24 hour)WATER LEVEL:
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

II-1
APPENDIX II
(FIELD DATA SHEETS)
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

III-1
APPENDIX III
(SOIL AND WATER REGULATORY STANDARDS)
UST SECTION GUIDELINES FOR THE
INVESTIGATION AND REMEDIATION OF
CONTAMINATION FROM NON-UST PETROLEUM
RELEASES
STATE of NORTH CAROLINA
DEPARTMENT of ENVIRONMENT and NATURAL RESOURCES
DIVISION of WASTE MANAGEMENT
UST SECTION
Effective July 1, 2007
12
5.0 Cleanup Requirements for Contaminated Soil
The goal of soil restoration is to ensure that groundwater contamination does not occur or
continue to occur. Table 1 outlines the required analytical methods for contaminated soil. In
response to the need for a simple method for contaminant identification and to lower the cost of
analysis, for the present time the UST Section will continue to allow the use of the TPH method
analyses for suspected or known petroleum contamination. The TPH Action Levels are as
follows:
Analytical Method Action Level
EPA Method 8015B 10 ppm TPH
EPA Method 8015B 40 ppm TPH
EPA Method 9071B (Oil & Grease) 250 ppm Oil & Grease
In the event petroleum contaminated soil is located near the groundwater, the regional office for
the UST Section may require analyses in addition to or in lieu of TPH. These additional
requirements are outlined in Table 2, however you should contact the appropriate regional office
to determine if they are necessary.
Soil cleanup levels have been established for some commonly encountered compounds. The soil-
to-groundwater maximum soil contaminant concentrations were established to protect
groundwater from the leaching of contaminants in soil. Contaminated soil must be cleaned up
to the soil-to-groundwater maximum contaminant concentrations. Contaminated soil clean-
up levels are provided in Table 3. The most recent version of these cleanup levels may be
downloaded from the Internet from the following web site address
http://www.wastenotnc.org/ust/docs/tblmscc.pdf.
The equations used by the Department to calculate the soil-to-groundwater maximum soil
contaminant concentrations are provided in Figure 3. The soil organic carbon-water partition
coefficients, soil-water partition coefficients and Henry’s Law Constants used to calculate the
soil-to-groundwater maximum contaminant concentrations for organic and inorganic compounds
were obtained from the following references:
ß EPA, 1996. Soil Screening Guidance: Technical Background Document. (EPA/540/R95/128);
ß EPA, 1986. Superfund Public Health Evaluation Manual. Office of Emergency and Remedial Response
(EPA/540/1-86/060);
ß Agency for Toxic Substances and Disease Registry, “Toxicological Profile for [individual chemical]. ” U.S.
Public Health Service;
ß Montgomery, J.H., 1996. Groundwater Chemicals Desk Reference. CRC Press, Inc.;
ß Sims, R.C., J.L. Sims and S.G. Hansen, 1991. Soil Transport and Fate Database, Version 2.0. EPA Robert S.
Kerr Environmental Laboratory; and
ß Baes, C.F., III, R.D. Sharp, A.L. Sjoreen, and R.W. Shor, 1984. A Review and Analysis of Parameters for
Assessing Transport of Environmentally Released Radionuclides through Agriculture. Oak Ridge National
Laboratory;
ß Other appropriate, published, peer-reviewed and scientifically valid data.
INACTIVE HAZARDOUS SITES BRANCH
HEALTH-BASED SOIL REMEDIATION GOALS1
These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance
documents and apply only at sites with signed administrative agreements with the Division of Waste Management.
In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If
sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the
proposed remedial alternative.

Page 1 of 16
See
Csat RG (ppm) footnote
Contaminant CASRN
Foot
note (mg/kg) (mg/kg) 8
Acephate* 30560-19-1 4.80E+01 N
Acetaldehyde* 75-07-0 1.10E+05 1.10E+01 C
Acetochlor 34256-82-1 2.40E+02 N
Acetone 67-64-1 3 1.10E+05 1.20E+04 N
Acetone Cyanohydrin 75-86-5 1.10E+05 4.00E+01 N
Acetonitrile 75-05-8 1.30E+05 1.70E+02 N
Acetophenone 98-86-2 3 2.30E+03 1.60E+03 N
Acrolein 107-02-8 2.50E+04 3.20E-02 N
Acrylamide* 79-06-1 1.10E-01 C
Acrylic Acid 79-10-7 6.00E+03 N
Acrylonitrile* 107-13-1 1.10E+04 2.40E-01 C
Adiponitrile 111-69-3 1.70E+06 N
Alachlor* 15972-60-8 2.40E+01 C
ALAR 1596-84-5 1.80E+03 N
Aldicarb 116-06-3 1.20E+01 N
Aldicarb Sulfone 1646-88-4 1.20E+01 N
Aldrin* 309-00-2 2.90E-02 C
Ally 74223-64-6 3.00E+03 N
Allyl Alcohol 107-18-6 6.20E+01 N
Allyl Chloride 107-05-1 1.50E+03 3.60E-01 N
Aluminum 7429-90-5 1.50E+04 N
Aluminum Phosphide 20859-73-8 6.20E+00 N
Amdro 67485-29-4 3.60E+00 N
Ametryn 834-12-8 1.10E+02 N
Aminophenol, m- 591-27-5 9.80E+02 N
Aminophenol, p- 123-30-8 2.40E+02 N
Amitraz 33089-61-1 3.00E+01 N
Ammonia 7664-41-7 2.80E+07 N
Ammonium Perchlorate 7790-98-9 1.10E+01 N
Ammonium Sulfamate 7773-06-0 3.20E+03 N
Aniline* 62-53-3 8.50E+01 C
Antimony (metallic) 7440-36-0 6.20E+00 N
Antimony Pentoxide 1314-60-9 7.80E+00 N
Antimony Potassium Tartrate 304-61-0 1.40E+01 N
Antimony Tetroxide 1332-81-6 6.20E+00 N
Antimony Trioxide 1309-64-4 6.20E+00 N
Apollo 74115-24-5 1.60E+02 N
Aramite* 140-57-8 1.90E+01 C
Arsenic, Inorganic* 7440-38-2 2 4.40E+00 N
Arsine 7784-42-1 1.40E+04 N
Assure 76578-14-8 1.10E+02 N
Asulam 3337-71-1 6.20E+02 N
October 2008
INACTIVE HAZARDOUS SITES BRANCH
HEALTH-BASED SOIL REMEDIATION GOALS1
These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance
documents and apply only at sites with signed administrative agreements with the Division of Waste Management.
In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If
sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the
proposed remedial alternative.

Page 2 of 16
See
Csat RG (ppm) footnote
Contaminant CASRN
Foot
note (mg/kg) (mg/kg) 8
Atrazine* 1912-24-9 2.10E+00 C
Avermectin B1 65195-55-3 4.80E+00 N
Azobenzene 103-33-3 4.90E+00 C
Barium 7440-39-3 3.00E+03 N
Baygon 114-26-1 4.80E+01 N
Bayleton 43121-43-3 3.60E+02 N
Baythroid 68359-37-5 3.00E+02 N
Benefin 1861-40-1 3.60E+03 N
Benomyl 17804-35-2 6.20E+02 N
Bentazon 25057-89-0 3.60E+02 N
Benzaldehyde 100-52-7 3 1.90E+03 1.60E+03 N
Benzene* 71-43-2 2.00E+03 1.10E+00 C
Benzenethiol 108-98-5 1.40E+03 1.60E-01 N
Benzidine 92-87-5 5.00E-04 C,M
Benzoic Acid 65-85-0 4.80E+04 N
Benzotrichloride 98-07-7 1.60E+02 4.90E-02 C
Benzyl Alcohol 100-51-6 6.20E+03 N
Benzyl Chloride 100-44-7 6.40E+01 3.80E+00 C
Beryllium and compounds 7440-41-7 3.20E+01 N
Bidrin 141-66-2 1.20E+00 N
Bifenox 42576-02-3 1.10E+02 N
Biphenthrin 82657-04-3 1.80E+02 N
Biphenyl, 1,1'- 92-52-4 2.60E+02 2.60E+02 Csat
Bis(2-chloroethoxy)methane 111-91-1 3.60E+01 N
Bis(2-chloroethyl)ether 111-44-4 3.30E+03 1.90E-01 C
Bis(2-chloro-1-methylethyl) ether 108-60-1 5.70E+02 3.50E+00 C
Bis(2-ethylhexyl)phthalate* 117-81-7 3.50E+01 C
Bis(chloromethyl)ether 542-88-1 2.80E+03 2.70E-04 C
Bisphenol A 80-05-7 6.20E+02 N
Boron And Borates Only 7440-42-8 3.20E+03 N
Boron Trifluoride 7637-07-2 2.00E+05 N
Bromate* 15541-45-4 9.10E-01 C
Bromodichloromethane* 75-27-4 9.90E+02 1.00E+01 C
Bromoform* 75-25-2 6.10E+01 C
Bromomethane 74-83-9 3.60E+03 1.60E+00 N
Bromophos 2104-96-3 6.20E+01 N
Bromoxynil 1689-84-5 2.40E+02 N
Bromoxynil Octanoate 1689-99-2 2.40E+02 N
Butadiene, 1,3-* 106-99-0 6.90E+02 7.70E-02 C
Butanol, N- 71-36-3 1.20E+03 N
Butyl Benzyl Phthlate 85-68-7 2.60E+02 C
Butylate 2008-41-5 6.20E+02 N
October 2008
INACTIVE HAZARDOUS SITES BRANCH
HEALTH-BASED SOIL REMEDIATION GOALS1
These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance
documents and apply only at sites with signed administrative agreements with the Division of Waste Management.
In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If
sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the
proposed remedial alternative.

Page 3 of 16
See
Csat RG (ppm) footnote
Contaminant CASRN
Foot
note (mg/kg) (mg/kg) 8
Butylphthalyl Butylglycolate 85-70-1 1.20E+04 N
Cacodylic Acid 75-60-5 2.40E+02 N
Cadmium (Diet) 7440-43-9 1.40E+01 N
Caprolactam 105-60-2 6.20E+03 N
Captafol* 2425-06-1 3.20E+00 C
Captan* 133-06-2 2.10E+02 C
Carbaryl 63-25-2 1.20E+03 N
Carbazole 86-74-8 2.40E+01 C
Carbofuran 1563-66-2 6.20E+01 N
Carbon Disulfide 75-15-0 3 2.60E+02 1.30E+02 N
Carbon Tetrachloride* 56-23-5 4.80E+02 2.50E-01 C
Carbosulfan 55285-14-8 1.20E+02 N
Carboxin 5234-68-4 1.20E+03 N
Chloral Hydrate 302-17-0 1.20E+03 N
Chloramben 133-90-4 1.80E+02 N
Chloranil 118-75-2 1.20E+00 C
Chlordane* 57-74-9 1.60E+00 C
Chlordecone (Kepone) 143-50-0 3.00E-02 C
Chlorimuron, Ethyl- 90982-32-4 2.40E+02 N
Chlorine 7782-50-5 1.50E+03 N
Chlorine Dioxide 10049-04-4 4.60E+02 N
Chlorite (Sodium Salt) 7758-19-2 4.60E+02 N
Chloro-1,1-difluoroethane, 1- 75-68-3 1.20E+03 1.20E+03 Csat
Chloro-1,3-butadiene, 2- 126-99-8 8.20E+02 1.70E+00 N
Chloro-2-methylaniline HCl, 4- 3165-93-3 1.10E+00 C
Chloro-2-methylaniline, 4- 95-69-2 1.80E+00 C
Chloroacetic Acid 79-11-8 2.40E+01 N
Chloroacetophenone, 2- 532-27-4 8.60E+03 N
Chloroaniline, p- 106-47-8 4.80E+01 N
Chlorobenzene 108-90-7 8.60E+02 9.00E+00 C
Chlorobenzilate* 510-15-6 4.40E+00 C
Chlorobenzotrifluoride, 4- 98-56-6 5.50E+02 4.20E+01 N
Chlorobutane, 1- 109-69-3 3 7.90E+02 6.20E+02 N
Chlorodifluoromethane 75-45-6 1.70E+03 1.70E+03 Csat
Chloroform 67-66-3 2.70E+03 3.00E-01 C
Chloromethane* 74-87-3 1.40E+03 1.70E+00 C
Chloronaphthalene, Beta- 91-58-7 2.10E+02 2.10E+02 Csat
Chlorophenol, 2- 95-57-8 7.90E+04 7.80E+01 N
Chlorothalonil* 1897-45-6 1.60E+02 C
Chlorotoluene, o- 95-49-8 3 1.00E+03 3.20E+02 N
Chlorotoluene, p- 106-43-4 2.90E+02 2.90E+02 Csat
Chlorpropham 101-21-3 2.40E+03 N
October 2008
INACTIVE HAZARDOUS SITES BRANCH
HEALTH-BASED SOIL REMEDIATION GOALS1
These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance
documents and apply only at sites with signed administrative agreements with the Division of Waste Management.
In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If
sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the
proposed remedial alternative.

Page 4 of 16
See
Csat RG (ppm) footnote
Contaminant CASRN
Foot
note (mg/kg) (mg/kg) 8
Chlorpyrifos 2921-88-2 3.60E+01 N
Chlorpyrifos Methyl 5598-13-0 1.20E+02 N
Chlorsulfuron 64902-72-3 6.20E+02 N
Chlorthiophos 60238-56-4 9.80E+00 N
Chromium (III) (Insoluble Salts) 16065-83-1 2.40E+04 N
Chromium VI (particulates) 18540-29-9 4.60E+01 N
Copper 7440-50-8 6.20E+02 N
Cresol, m- 108-39-4 6.20E+02 N
Cresol, o- 95-48-7 6.20E+02 N
Cresol, p- 106-44-5 6.20E+01 N
Crotonaldehyde, trans- 123-73-9 2.40E+04 3.40E-01 C
Cumene 98-82-8 3.10E+02 3.10E+02 Csat
Cyanazine* 21725-46-2 5.80E-01 C
Cyanides
Calcium Cyanide 592-01-8 6.20E+02 N
Copper Cyanide 544-92-3 7.80E+01 N
Cyanide (CN-) 57-12-5 3.20E+02 N
Cyanogen 460-19-5 6.20E+02 N
Cyanogen Bromide 506-68-3 1.40E+03 N
Cyanogen Chloride 506-77-4 7.80E+02 N
Hydrogen Cyanide 74-90-8 3.20E+02 N
Potassium Cyanide 151-50-8 7.80E+02 N
Potassium Silver Cyanide 506-61-6 3.20E+03 N
Silver Cyanide 506-64-9 1.60E+03 N
Sodium Cyanide 143-33-9 6.20E+02 N
Thiocyanate 463-56-9 5.60E+03 3.20E+00 N
Zinc Cyanide 557-21-1 7.80E+02 N
Cyclohexane 110-82-7 1.20E+02 1.20E+02 Csat
Cyclohexane, 1,2,3,4,5-pentabromo-6-chloro- 87-84-3 2.10E+01 C
Cyclohexanone 108-94-1 6.20E+04 N
Cyclohexylamine 108-91-8 2.40E+03 N
Cyhalothrin/karate 68085-85-8 6.20E+01 N
Cypermethrin 52315-07-8 1.20E+02 N
Cyromazine 66215-27-8 9.20E+01 N
Dacthal 1861-32-1 1.20E+02 N
Dalapon 75-99-0 3.60E+02 N
DDD 72-54-8 2.00E+00 C
DDE, p,p'- 72-55-9 1.40E+00 C
DDT* 50-29-3 1.70E+00 C
Decabromodiphenyl Ether 1163-19-5 8.60E+01 N
Demeton 8065-48-3 4.80E-01 N
Di(2-ethylhexyl)adipate* 103-23-1 4.00E+02 C
October 2008
INACTIVE HAZARDOUS SITES BRANCH
HEALTH-BASED SOIL REMEDIATION GOALS1
These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance
documents and apply only at sites with signed administrative agreements with the Division of Waste Management.
In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If
sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the
proposed remedial alternative.

Page 5 of 16
See
Csat RG (ppm) footnote
Contaminant CASRN
Foot
note (mg/kg) (mg/kg) 8
Diallate 2303-16-4 8.00E+00 C
Diazinon 333-41-5 1.10E+01 N
Dibromo-3-chloropropane, 1,2- 96-12-8 1.10E+03 5.60E-03 C
Dibromobenzene, 1,4- 106-37-6 1.20E+02 N
Dibromochloromethane* 124-48-1 8.50E+02 5.80E+00 C
Dibromoethane, 1,2- 106-93-4 1.40E+03 3.40E-02 C
Dibromomethane (Methylene Bromide) 74-95-3 3.00E+03 1.60E+02 N
Dibutyl Phthalate 84-74-2 1.20E+03 N
Dibutyltin Compounds NA 3.60E+00 N
Dicamba 1918-00-9 3.60E+02 N
Dichloro-2-butene, 1,4- 764-41-0 6.10E+02 3.20E-03 C
Dichloroacetic Acid* 79-43-6 9.70E+00 N
Dichlorobenzene, 1,2- 95-50-1 2.20E+02 2.20E+02 Csat
Dichlorobenzene, 1,4- 106-46-7 2.60E+00 C
Dichlorobenzidine, 3,3'- 91-94-1 1.10E+00 C
Dichlorodifluoromethane 75-71-8 8.50E+02 3.80E+01 N
Dichloroethane, 1,1-* 75-34-3 1.80E+03 3.40E+00 C
Dichloroethane, 1,2- 107-06-2 1.90E+03 4.50E-01 C
Dichloroethylene, 1,1- 75-35-4 1.20E+03 5.00E+01 N
Dichloroethylene, 1,2- (Mixed Isomers) 540-59-0 1.40E+03 1.40E+02 N
Dichloroethylene, 1,2-cis- 156-59-2 1.40E+03 1.60E+02 N
Dichloroethylene, 1,2-trans- 156-60-5 1.50E+03 2.20E+01 N
Dichlorophenol, 2,4- 120-83-2 3.60E+01 N
Dichlorophenoxy Acetic Acid, 2,4- 94-75-7 1.40E+02 N
Dichlorophenoxy)butyric Acid, 4-(2,4- 94-82-6 9.80E+01 N
Dichloropropane, 1,2-* 78-87-5 1.50E+03 9.30E-01 C
Dichloropropane, 1,3- 142-28-9 3 1.60E+03 3.20E+02 N
Dichloropropanol, 2,3- 616-23-9 3.60E+01 N
Dichloropropene, 1,3-* 542-75-6 1.70E+03 1.70E+00 C
Dichlorvos* 62-73-7 1.70E+00 C
Dicyclopentadiene 77-73-6 5.90E+02 5.80E+00 N
Dieldrin* 60-57-1 3.00E-02 C
Diethyl Phthalate 84-66-2 9.80E+03 N
Diethylformamide 617-84-5 1.20E+01 N
Diethylstilbestrol 56-53-1 1.40E-03 C
Difenzoquat 43222-48-6 9.80E+02 N
Diflubenzuron 35367-38-5 2.40E+02 N
Difluoroethane, 1,1- 75-37-6 1.50E+03 1.50E+03 Csat
Diisopropyl Methylphosphonate 1445-75-6 4.30E+02 4.30E+02 Csat
Dimethipin 55290-64-7 2.40E+02 N
Dimethoate 60-51-5 2.40E+00 N
Dimethoxybenzidine, 3,3'- 119-90-4 3.50E+01 C
October 2008
INACTIVE HAZARDOUS SITES BRANCH
HEALTH-BASED SOIL REMEDIATION GOALS1
These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance
documents and apply only at sites with signed administrative agreements with the Division of Waste Management.
In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If
sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the
proposed remedial alternative.

Page 6 of 16
See
Csat RG (ppm) footnote
Contaminant CASRN
Foot
note (mg/kg) (mg/kg) 8
Dimethyl methylphosphonate* 756-79-6 2.90E+02 C
Dimethylaniline HCl, 2,4- 21436-96-4 8.40E-01 C
Dimethylaniline, 2,4- 95-68-1 6.50E-01 C
Dimethylaniline, N,N- 121-69-7 8.20E+02 3.20E+01 N
Dimethylformamide 68-12-2 1.20E+03 N
Dimethylphenol, 2,4- 105-67-9 2.40E+02 N
Dimethylphenol, 2,6- 576-26-1 7.40E+00 N
Dimethylphenol, 3,4- 95-65-8 1.20E+01 N
Dimethylterephthalate 120-61-6 6.10E+00 6.10E+00 Csat
Dinitro-o-cyclohexyl Phenol, 4,6- 131-89-5 2.40E+01 N
Dinitrobenzene, 1,2- 528-29-0 1.20E+00 N
Dinitrobenzene, 1,3- 99-65-0 1.20E+00 N
Dinitrobenzene, 1,4- 100-25-4 1.20E+00 N
Dinitrophenol, 2,4- 51-28-5 2.40E+01 N
Dinitrotoluene Mixture, 2,4/2,6-* 25321-14-6 7.10E-01 C
Dinitrotoluene, 2,4- 121-14-2 2.40E+01 N
Dinitrotoluene, 2,6- 606-20-2 1.20E+01 N
Dinitrotoluene, 2-Amino-4,6- 35572-78-2 3.00E+01 N
Dinitrotoluene, 4-Amino-2,6- 19406-51-0 3.00E+01 N
Dinoseb 88-85-7 1.20E+01 N
Dioxane, 1,4- 123-91-1 4.40E+01 C
Dioxins 4
Hexachlorodibenzo-p-dioxin 34465-46-8 4.50E-05 C
Hexachlorodibenzo-p-dioxin, Mixture NA 9.40E-05 C
HpCDD, 2,3,7,8- 37871-00-4 4.50E-04 C
OCDD 3268-87-9 1.50E-02 C
PeCDD, 2,3,7,8- 36088-22-9 4.50E-06 C
TCDD, 2,3,7,8-* 1746-01-6 4.50E-06 C
Diphenamid 957-51-7 3.60E+02 N
Diphenylamine 122-39-4 3.00E+02 N
Diphenylhydrazine, 1,2- 122-66-7 6.10E-01 C
Diquat 85-00-7 2.60E+01 N
Direct Black 38 1937-37-7 6.60E-02 C
Direct Blue 6 2602-46-2 6.60E-02 C
Direct Brown 95 16071-86-6 7.20E-02 C
Disulfoton 298-04-4 4.80E-01 N
Dithiane, 1,4- 505-29-3 1.20E+02 N
Diuron 330-54-1 2.40E+01 N
Dodine 2439-10-3 4.80E+01 N
Endosulfan 115-29-7 7.40E+01 N
Endothall 145-73-3 2.40E+02 N
Endrin 72-20-8 3.60E+00 N
October 2008
INACTIVE HAZARDOUS SITES BRANCH
HEALTH-BASED SOIL REMEDIATION GOALS1
These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance
documents and apply only at sites with signed administrative agreements with the Division of Waste Management.
In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If
sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the
proposed remedial alternative.

Page 7 of 16
See
Csat RG (ppm) footnote
Contaminant CASRN
Foot
note (mg/kg) (mg/kg) 8
Epichlorohydrin 106-89-8 8.40E+03 3.60E+00 N
Epoxybutane, 1,2- 106-88-7 1.20E+04 3.00E+01 N
EPTC3 759-94-4 6.20E+02 4.00E+02 N
Ethephon 16672-87-0 6.20E+01 N
Ethion 563-12-2 6.20E+00 N
Ethoxyethanol Acetate, 2- 111-15-9 3.60E+03 N
Ethoxyethanol, 2- 110-80-5 4.80E+04 N
Ethyl Acetate 141-78-6 1.10E+04 1.10E+04 Csat
Ethyl Acrylate 140-88-5 2.60E+03 1.30E+01 C
Ethyl Chloride 75-00-3 2.20E+03 2.20E+03 Csat
Ethyl Ether3 60-29-7 8.20E+03 3.20E+03 N
Ethyl Methacrylate 97-63-2 1.20E+03 1.20E+03 Csat
Ethyl-p-nitrophenyl Phosphonate 2104-64-5 1.20E-01 N
Ethylbenzene3 100-41-4 5.50E+02 5.70E+00 C
Ethylene Cyanohydrin 109-78-4 3.60E+02 N
Ethylene Diamine 107-15-3 1.10E+03 N
Ethylene Glycol 107-21-1 2.40E+04 N
Ethylene Glycol Monobutyl Ether 111-76-2 6.20E+03 N
Ethylene Oxide 75-21-8 1.10E+05 1.60E-01 C
Ethylene Thiourea 96-45-7 9.80E-01 N
Ethylphthalyl Ethyl Glycolate 84-72-0 3.60E+04 N
Express 101200-48-0 9.80E+01 N
Fenamiphos 22224-92-6 3.00E+00 N
Fenpropathrin 39515-41-8 3.00E+02 N
Fluometuron 2164-17-2 1.60E+02 N
Fluorine (Soluble Fluoride) 7782-41-4 9.40E+02 N
Fluridone 59756-60-4 9.80E+02 N
Flurprimidol 56425-91-3 2.40E+02 N
Flutolanil 66332-96-5 7.40E+02 N
Fluvalinate 69409-94-5 1.20E+02 N
Folpet* 133-07-3 1.40E+02 C
Fomesafen 72178-02-0 2.60E+00 C
Fonofos 944-22-9 2.40E+01 N
Formaldehyde 50-00-0 2.40E+03 N
Formic Acid 64-18-6 2.40E+04 N
Fosetyl-AL 39148-24-8 3.60E+04 N
Furans 4
Furan 110-00-9 6.80E+03 1.60E+01 N
HpCDF, 2,3,7,8- 38998-75-3 3.70E-04 C
HxCDF, 2,3,7,8- 55684-94-1 3.70E-05 C
OCDF 39001-02-0 1.20E-02 C
PeCDF, 1,2,3,7,8- 57117-41-6 1.20E-04 C
October 2008
INACTIVE HAZARDOUS SITES BRANCH
HEALTH-BASED SOIL REMEDIATION GOALS1
These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance
documents and apply only at sites with signed administrative agreements with the Division of Waste Management.
In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If
sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the
proposed remedial alternative.

Page 8 of 16
See
Csat RG (ppm) footnote
Contaminant CASRN
Foot
note (mg/kg) (mg/kg) 8
PeCDF, 2,3,4,7,8- 57117-31-4 1.20E-05 C
TCDF, 2,3,7,8- 51207-31-9 3.70E-05 C
Furazolidone 67-45-8 1.30E-01 C
Furfural 98-01-1 3.60E+01 N
Furium 531-82-8 3.20E-01 C
Furmecyclox 60568-05-0 1.60E+01 C
Glufosinate, Ammonium 77182-82-2 4.80E+00 N
Glycidyl 765-34-4 4.80E+00 N
Glyphosate 1071-83-6 1.20E+03 N
Goal 42874-03-3 3.60E+01 N
Haloxyfop, Methyl 69806-40-2 6.20E-01 N
Harmony 79277-27-3 1.60E+02 N
Heptachlor* 76-44-8 1.10E-01 C
Heptachlor Epoxide* 1024-57-3 5.30E-02 C
Hexabromobenzene 87-82-1 2.40E+01 N
Hexachlorobenzene* 118-74-1 3.00E-01 C
Hexachlorobutadiene* 87-68-3 6.20E+00 C
Hexachlorocyclohexane, Alpha- 319-84-6 7.70E-02 C
Hexachlorocyclohexane, Beta- 319-85-7 2.70E-01 C
Hexachlorocyclohexane, Gamma- (Lindane)* 58-89-9 5.20E-01 C
Hexachlorocyclohexane, Technical 608-73-1 2.70E-01 C
Hexachlorocyclopentadiene 77-47-4 7.40E+01 N
Hexachloroethane 67-72-1 1.20E+01 N
Hexachlorophene 70-30-4 3.60E+00 N
Hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX)* 121-82-4 5.50E+00 C
Hexamethylene Diisocyanate, 1,6- 822-06-0 4.10E+03 7.40E-01 N
Hexane, N-3 110-54-3 1.40E+02 1.10E+02 N
Hexanedioic Acid 124-04-9 2.40E+04 N
Hexazinone 51235-04-2 4.00E+02 N
Hydrazine 302-01-2 2.10E-01 C
Hydrazine Sulfate 10034-93-2 2.10E-01 C
Hydrogen Chloride 7647-01-0 5.60E+06 N
Hydrogen Sulfide 7783-06-4 5.60E+05 N
Imazalil 35554-44-0 1.60E+02 N
Imazaquin 81335-37-7 3.00E+03 N
Iprodione 36734-19-7 4.80E+02 N
Iron 7439-89-6 1.10E+04 N
Isobutyl Alcohol3 78-83-1 9.60E+03 4.60E+03 N
Isophorone* 78-59-1 5.10E+02 C
Isopropalin 33820-53-0 1.80E+02 N
Isopropyl Methyl Phosphonic Acid 1832-54-8 1.20E+03 N
Isoxaben 82558-50-7 6.20E+02 N
October 2008
INACTIVE HAZARDOUS SITES BRANCH
HEALTH-BASED SOIL REMEDIATION GOALS1
These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance
documents and apply only at sites with signed administrative agreements with the Division of Waste Management.
In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If
sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the
proposed remedial alternative.

Page 9 of 16
See
Csat RG (ppm) footnote
Contaminant CASRN
Foot
note (mg/kg) (mg/kg) 8
Kerb 23950-58-5 9.20E+02 N
Lactofen 77501-63-4 2.40E+01 N
Lead Compounds
Lead and Compounds 7439-92-1 5 4.00E+02
Tetraethyl Lead 78-00-2 1.20E-03 N
Linuron 330-55-2 2.40E+01 N
Lithium Perchlorate 7791-03-9 1.10E+01 N
Londax 83055-99-6 2.40E+03 N
Malathion 121-75-5 2.40E+02 N
Maleic Anhydride 108-31-6 1.20E+03 N
Maleic Hydrazide 123-33-1 6.20E+03 N
Malononitrile 109-77-3 1.20E+00 N
Mancozeb 8018-01-7 3.60E+02 N
Maneb 12427-38-2 6.20E+01 N
Manganese (Water) 7439-96-5 3.60E+02 N
MCPA 94-74-6 6.20E+00 N
MCPB 94-81-5 1.20E+02 N
MCPP 93-65-2 1.20E+01 N
Mephosfolan 950-10-7 1.10E+00 N
Mepiquat Chloride 24307-26-4 3.60E+02 N
Mercury Compounds
Mercuric Chloride 7487-94-7 4.60E+00 N
Mercuric Sulfide 1344-48-5 4.60E+00 N
Mercury (elemental) 7439-97-6 3 3.10E+00 1.30E+00 N
Mercury, Inorganic Salts NA 4.60E+00 N
Methyl Mercury 22967-92-6 1.60E+00 N
Phenylmercuric Acetate 62-38-4 9.80E-01 N
Merphos 150-50-5 3.60E-01 N
Merphos Oxide 78-48-8 3.60E-01 N
Metalaxyl 57837-19-1 7.40E+02 N
Methacrylonitrile 126-98-7 4.50E+03 6.40E-01 N
Methamidophos 10265-92-6 6.20E-01 N
Methanol 67-56-1 6.20E+03 N
Methidathion 950-37-8 1.20E+01 N
Methomyl 16752-77-5 3.00E+02 N
Methoxy-5-nitroaniline, 2- 99-59-2 9.90E+00 C
Methoxychlor 72-43-5 6.20E+01 N
Methoxyethanol Acetate, 2- 110-49-6 2.40E+01 N
Methoxyethanol, 2- 109-86-4 3.60E+01 N
Methyl Acetate 79-20-9 3 2.90E+04 1.60E+04 N
Methyl Acrylate 96-33-3 6.90E+03 4.60E+02 N
Methyl Ethyl Ketone (2-Butanone) 78-93-3 3 2.80E+04 5.60E+03 N
October 2008
INACTIVE HAZARDOUS SITES BRANCH
HEALTH-BASED SOIL REMEDIATION GOALS1
These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance
documents and apply only at sites with signed administrative agreements with the Division of Waste Management.
In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If
sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the
proposed remedial alternative.

Page 10 of 16
See
Csat RG (ppm) footnote
Contaminant CASRN
Foot
note (mg/kg) (mg/kg) 8
Methyl Isobutyl Ketone (4-methyl-2-pentanone) 108-10-1 3 3.20E+03 1.10E+03 N
Methyl Methacrylate 80-62-6 3 2.50E+03 9.40E+02 N
Methyl Parathion 298-00-0 3.00E+00 N
Methyl Styrene (Mixed Isomers) 25013-15-4 4.50E+02 3.80E+01 N
Methyl tert-Butyl Ether (MTBE)* 1634-04-4 3 6.90E+03 3.90E+01 C
Methyl-5-Nitroaniline, 2- 99-55-8 1.50E+01 C
Methylaniline Hydrochloride, 2- 636-21-5 3.70E+00 C
Methylarsonic acid 124-58-3 1.20E+02 N
Methylene Chloride* 75-09-2 3.50E+03 1.10E+01 C
Methylene-bis(2-chloroaniline), 4,4'-* 101-14-4 M 1.20E+00 C
Methylene-bis(N,N-dimethyl) Aniline, 4,4'- 101-61-1 1.10E+01 C
Methylenebisbenzenamine, 4,4'- 101-77-9 3.00E-01 C
Methylenediphenyl Diisocyanate 101-68-8 1.70E-05 N
Methylstyrene, Alpha- 98-83-9 4.50E+02 4.50E+02 Csat
Metolachlor 51218-45-2 1.80E+03 N
Metribuzin 21087-64-9 3.00E+02 N
Mirex* 2385-85-5 2.70E-02 C
Molinate 2212-67-1 2.40E+01 N
Molybdenum 7439-98-7 7.80E+01 N
Monochloramine 10599-90-3 1.60E+03 N
Monomethylaniline 100-61-8 2.40E+01 N
N,N'-Diphenyl-1,4-benzenediamine 74-31-7 3.60E+00 N
Naled 300-76-5 2.40E+01 N
Napropamide 15299-99-7 1.20E+03 N
Nickel Refinery Dust NA 1.40E+04 C
Nickel Soluble Salts 7440-02-0 3.20E+02 N
Nickel Subsulfide 12035-72-2 6.90E+03 C
Nitrate 14797-55-8 2.60E+04 N
Nitrite 14797-65-0 1.60E+03 N
Nitrobenzene 98-95-3 2.60E+03 6.20E+00 N
Nitrofurantoin 67-20-9 8.60E+02 N
Nitrofurazone 59-87-0 3.70E-01 C
Nitroglycerin 55-63-0 1.20E+00 N
Nitroguanidine 556-88-7 1.20E+03 N
Nitromethane* 75-52-5 1.70E+04 4.70E+00 C
Nitropropane, 2- 79-46-9 4.30E+03 1.20E-02 C
Nitroso-di-N-butylamine, N- 924-16-3 1.30E+04 9.30E-02 C
Nitroso-di-N-propylamine, N- 621-64-7 6.90E-02 C
Nitroso-N-ethylurea, N- 759-73-9 4.30E-03 C,M
Nitrosodiethanolamine, N- 1116-54-7 1.70E-01 C
Nitrosodiethylamine, N- 55-18-5 7.70E-04 C,M
Nitrosodimethylamine, N-* 62-75-9 2.30E-03 C,M
October 2008
INACTIVE HAZARDOUS SITES BRANCH
HEALTH-BASED SOIL REMEDIATION GOALS1
These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance
documents and apply only at sites with signed administrative agreements with the Division of Waste Management.
In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If
sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the
proposed remedial alternative.

Page 11 of 16
See
Csat RG (ppm) footnote
Contaminant CASRN
Foot
note (mg/kg) (mg/kg) 8
Nitrosodiphenylamine, N- 86-30-6 9.90E+01 C
Nitrosomethylethylamine, N- 10595-95-6 2.20E-02 C
Nitrosopyrrolidine, N- 930-55-2 2.30E-01 C
Nitrotoluene, o- 88-72-2 1.30E+03 2.90E+00 C
Nitrotoluene, p-* 99-99-0 3.00E+01 C
Norflurazon 27314-13-2 4.80E+02 N
Nustar 85509-19-9 8.60E+00 N
Octabromodiphenyl Ether 32536-52-0 3.60E+01 N
Octahydro-1,3,5,7-tetranitro-1,3,5,7-tetra (HMX) 2691-41-0 7.6E+02 N
Octamethylpyrophosphoramide 152-16-9 2.40E+01 N
Oryzalin 19044-88-3 6.20E+02 N
Oxadiazon 19666-30-9 6.20E+01 N
Oxamyl 23135-22-0 3.00E+02 N
Paclobutrazol 76738-62-0 1.60E+02 N
Polynuclear Aromatic Hydrocarbons (PAHs) 7
Acenaphthene 83-32-9 6.80E+02 N
Anthracene 120-12-7 3.40E+03 N
Benz[a]anthracene 56-55-3 1.50E-01 C,M
Benzo[a]pyrene 50-32-8 1.50E-02 C,M
Benzo[b]fluoranthene 205-99-2 1.50E-01 C,M
Benzo[k]fluoranthene 207-08-9 1.50E+00 C,M
Chrysene 218-01-9 1.50E+01 C,M
Dibenz[a,h]anthracene 53-70-3 1.50E-02 C,M
Fluoranthene 206-44-0 4.60E+02 N
Fluorene 86-73-7 4.60E+02 N
Indeno[1,2,3-cd]pyrene 193-39-5 1.50E-01 C,M
Methylnaphthalene, 1- 90-12-0 3 4.60E+02 2.20E+01 C
Methylnaphthalene, 2- 91-57-6 3 4.40E+02 6.20E+01 N
Naphthalene* 91-20-3 3.90E+00 C
Pyrene 129-00-0 3.40E+02 N
Paraquat Dichloride 1910-42-5 5.40E+01 N
Parathion 56-38-2 7.40E+01 N
Polychlorinated Biphenyls (PCBs) 7 1.00E+00 6
Pebulate 1114-71-2 6.20E+02 N
Pendimethalin 40487-42-1 4.80E+02 N
Pentabromodiphenyl Ether 32534-81-9 2.40E+01 N
Pentachlorobenzene 608-93-5 9.80E+00 N
Pentachloronitrobenzene* 82-68-8 1.90E+00 C
Pentachlorophenol* 87-86-5 3.00E+00 C
Perchlorate and Perchlorate Salts 14797-73-0 1.10E+01 N
Permethrin 52645-53-1 6.20E+02 N
Phenmedipham 13684-63-4 3.00E+03 N
October 2008
INACTIVE HAZARDOUS SITES BRANCH
HEALTH-BASED SOIL REMEDIATION GOALS1
These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance
documents and apply only at sites with signed administrative agreements with the Division of Waste Management.
In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If
sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the
proposed remedial alternative.

Page 12 of 16
See
Csat RG (ppm) footnote
Contaminant CASRN
Foot
note (mg/kg) (mg/kg) 8
Phenol 108-95-2 3.60E+03 N
Phenylenediamine, m- 108-45-2 7.40E+01 N
Phenylenediamine, o- 95-54-5 1.00E+01 C
Phenylenediamine, p- 106-50-3 2.40E+03 N
Phenylphenol, 2- 90-43-7 2.50E+02 N
Phorate 298-02-2 2.40E+00 N
Phosgene 75-44-5 8.70E+04 8.00E-02 N
Phosmet 732-11-6 2.40E+02 N
Phosphine 7803-51-2 4.60E+00 N
Phosphoric Acid 7664-38-2 2.80E+06 N
Phosphorus, White 7723-14-0 3.20E-01 N
Phthalic Acid, P- 100-21-0 1.20E-04 N
Phthalic Anhydride 85-44-9 2.40E-04 N
Picloram 1918-02-1 8.60E+02 N
Pirimiphos, Methyl 29232-93-7 1.20E+02 N
Polybrominated Biphenyls* 59536-65-1 1.60E-02 C
Polymeric Methylene Diphenyl Diisocyanate (PMDI) 9016-87-9 1.70E+05 N
Potassium Perchlorate 7778-74-7 1.10E+01 N
Prochloraz* 67747-09-5 3.20E+00 C
Profluralin 26399-36-0 7.40E+01 N
Prometon 1610-18-0 1.80E+02 N
Prometryn 7287-19-6 4.80E+01 N
Propachlor 1918-16-7 1.60E+02 N
Propanil 709-98-8 6.20E+01 N
Propargite 2312-35-8 2.40E+02 N
Propargyl Alcohol 107-19-7 2.40E+01 N
Propazine 139-40-2 2.40E+02 N
Propham 122-42-9 2.40E+02 N
Propiconazole 60207-90-1 1.60E+02 N
Propylene Glycol 57-55-6 2.40E+05 N
Propylene Glycol Dinitrate 6423-43-4 1.40E+03 1.20E+01 N
Propylene Glycol Monoethyl Ether 1569-02-4 8.60E+03 N
Propylene Glycol Monomethyl Ether 107-98-2 8.60E+03 N
Propylene Oxide* 75-56-9 6.80E+04 1.90E+00 C
Pursuit 81335-77-5 3.00E+03 N
Pydrin 51630-58-1 3.00E+02 N
Pyridine 110-86-1 3.00E+05 1.60E+01 N
Quinalphos 13593-03-8 6.20E+00 N
Quinoline 91-22-5 1.60E-01 C
Refractory Ceramic Fibers NA 8.60E+06 N
Resmethrin 10453-86-8 3.60E+02 N
Ronnel 299-84-3 6.20E+02 N
October 2008
INACTIVE HAZARDOUS SITES BRANCH
HEALTH-BASED SOIL REMEDIATION GOALS1
These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance
documents and apply only at sites with signed administrative agreements with the Division of Waste Management.
In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If
sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the
proposed remedial alternative.

Page 13 of 16
See
Csat RG (ppm) footnote
Contaminant CASRN
Foot
note (mg/kg) (mg/kg) 8
Rotenone 83-79-4 4.80E+01 N
Savey 78587-05-0 3.00E+02 N
Selenious Acid 7783-00-8 7.80E+01 N
Selenium 7782-49-2 7.80E+01 N
Selenourea 630-10-4 6.20E+01 N
Sethoxydim 74051-80-2 1.10E+03 N
Silver 7440-22-4 7.80E+01 N
Simazine* 122-34-9 4.00E+00 C
Sodium Acifluorfen 62476-59-9 1.60E+02 N
Sodium Azide 26628-22-8 6.20E+01 N
Sodium Diethyldithiocarbamate 148-18-5 1.80E+00 C
Sodium Fluoroacetate 62-74-8 2.40E-01 N
Sodium Metavanadate 13718-26-8 1.60E+01 N
Sodium Perchlorate 7601-89-0 1.10E+01 N
Stirofos (Tetrachlorovinphos)* 961-11-5 2.00E+01 C
Strontium, Stable 7440-24-6 9.40E+03 N
Strychnine 57-24-9 3.60E+00 N
Styrene 100-42-5 1.00E+03 1.00E+03 Csat
Systhane 88671-89-0 3.00E+02 N
TCMTB 21564-17-0 3.60E+02 N
Tebuthiuron 34014-18-1 8.60E+02 N
Temephos 3383-96-8 2.40E+02 N
Terbacil 5902-51-2 1.60E+02 N
Terbufos 13071-79-9 3.00E-01 N
Terbutryn 886-50-0 1.20E+01 N
Tetrachlorobenzene, 1,2,4,5- 95-94-3 3.60E+00 N
Tetrachloroethane, 1,1,1,2- 630-20-6 7.50E+02 2.00E+00 C
Tetrachloroethane, 1,1,2,2- 79-34-5 2.10E+03 5.90E-01 C
Tetrachloroethylene 127-18-4 1.80E+02 5.70E-01 C
Tetrachlorophenol, 2,3,4,6- 58-90-2 3.60E+02 N
Tetrachlorotoluene, p- alpha, alpha, alpha- 5216-25-1 2.40E-02 C
Tetraethyl Dithiopyrophosphate 3689-24-5 6.20E+00 N
Tetrafluoroethane, 1,1,1,2- 811-97-2 8.20E+02 8.20E+02 Csat
Tetryl (Trinitrophenylmethylnitramine) 479-45-8 4.80E+01 N
Thallium (I) Nitrate 10102-45-1 1.40E+00 N
Thallium (Soluble Salts) 7440-28-0 1.00E+00 N
Thallium Acetate 563-68-8 1.40E+00 N
Thallium Carbonate 6533-73-9 1.30E+00 N
Thallium Chloride 7791-12-0 1.30E+00 N
Thallium Sulfate 7446-18-6 1.30E+00 N
Thiobencarb 28249-77-6 1.20E+02 N
Thiofanox 39196-18-4 3.60E+00 N
October 2008
INACTIVE HAZARDOUS SITES BRANCH
HEALTH-BASED SOIL REMEDIATION GOALS1
These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance
documents and apply only at sites with signed administrative agreements with the Division of Waste Management.
In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If
sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the
proposed remedial alternative.

Page 14 of 16
See
Csat RG (ppm) footnote
Contaminant CASRN
Foot
note (mg/kg) (mg/kg) 8
Thiophanate, Methyl 23564-05-8 9.80E+02 N
Thiram 137-26-8 6.20E+01 N
Tin 7440-31-5 9.40E+03 N
Toluene 108-88-3 9.30E+02 9.30E+02 Csat
Toluene diisocyanate mixture (TDI) 26471-62-5 2.10E+03 1.10E+01 N
Toluene-2,4-diamine 95-80-7 1.30E-01 C
Toluene-2,5-diamine 95-70-5 7.40E+03 N
Toluene-2,6-diamine 823-40-5 3.60E+02 N
Toluidine, o- (Methylaniline, 2-) 95-53-4 2.70E+00 C
Toluidine, p- 106-49-0 2.60E+00 C
Toxaphene 8001-35-2 4.40E-01 C
Tralomethrin 66841-25-6 9.20E+01 N
Triallate 2303-17-5 1.60E+02 N
Triasulfuron 82097-50-5 1.20E+02 N
Tribromobenzene, 1,2,4- 615-54-3 6.20E+01 N
Tributyltin Compounds NA 3.60E+00 N
Tributyltin Oxide 56-35-9 3.60E+00 N
Trichloro-1,2,2-trifluoroethane, 1,1,2- 76-13-1 9.40E+02 9.40E+02 Csat
Trichloroaniline HCl, 2,4,6- 33663-50-2 1.70E+01 C
Trichloroaniline, 2,4,6- 634-93-5 1.40E+01 C
Trichlorobenzene, 1,2,4-* 120-82-1 3 2.20E+02 1.74E+01 N
Trichloroethane, 1,1,1- 71-55-6 6.80E+02 6.80E+02 Csat
Trichloroethane, 1,1,2-* 79-00-5 5.60E+02 1.10E+00 C
Trichloroethylene 79-01-6 7.50E+02 2.80E+00 C
Trichlorofluoromethane 75-69-4 1.30E+03 1.60E+02 N
Trichlorophenol, 2,4,5- 95-95-4 1.20E+03 N
Trichlorophenol, 2,4,6-* 88-06-2 1.20E+01 N
Trichlorophenoxy) Propionic Acid, 2(2,4,5- 93-72-1 9.80E+01 N
Trichlorophenoxyacetic Acid, 2,4,5- 93-76-5 1.20E+02 N
Trichloropropane, 1,1,2- 598-77-6 1.40E+03 7.80E+01 N
Trichloropropane, 1,2,3- 96-18-4 1.60E+03 9.10E-02 C
Tridiphane 58138-08-2 3.60E+01 N
Triethylamine 121-44-8 5.50E+04 3.40E+01 N
Trifluralin* 1582-09-8 6.30E+01 C
Trimethyl Phosphate 512-56-1 1.30E+01 N
Trimethylbenzene, 1,2,4- 95-63-6 2.50E+02 1.30E+01 N
Trinitrobenzene, 1,3,5- 99-35-4 4.40E+02 N
Trinitrotoluene, 2,4,6-* 118-96-7 1.90E+01 C
Tri-n-butyltin 688-73-3 3.60E+00 N
Uranium (Soluble Salts) NA 4.60E+01 N
Vanadium Pentoxide 1314-62-1 1.40E+02 N
Vanadium Sulfate 36907-42-3 3.20E+02 N
October 2008
INACTIVE HAZARDOUS SITES BRANCH
HEALTH-BASED SOIL REMEDIATION GOALS1
These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance
documents and apply only at sites with signed administrative agreements with the Division of Waste Management.
In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If
sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the
proposed remedial alternative.

Page 15 of 16
See
Csat RG (ppm) footnote
Contaminant CASRN
Foot
note (mg/kg) (mg/kg) 8
Vanadium and Compounds NA 7.80E+01 N
Vanadium, Metallic 7440-62-2 1.10E+02 N
Vanadyl Sulfate 27774-13-6 3.20E+02 N
Vernolate 1929-77-7 1.20E+01 N
Vinclozolin 50471-44-8 3.00E+02 N
Vinyl Acetate 108-05-4 2.80E+03 2.00E+02 N
Vinyl Bromide 593-60-2 1.70E+03 1.10E-01 C
Vinyl Chloride 75-01-4 4.00E+03 6.00E-02 C,M
Warfarin 81-81-2 3.60E+00 N
Xylene, Mixture 1330-20-7 3 3.00E+02 1.20E+02 N
Xylene, P- 106-42-3 4.50E+02 4.50E+02 Csat
Xylene, m- 108-38-3 4.40E+02 4.40E+02 Csat
Xylene, o- 95-47-6 3.00E+02 3.00E+02 Csat
Zinc (Metallic) 7440-66-6 4.60E+03 N
Zinc Phosphide 1314-84-7 4.60E+00 N
Zineb 12122-67-7 6.20E+02 N

* - Contaminant exhibits both carcinogenic and non-carcinogenic effects. The lower of the carcinogenic
remediation goal at 1.0E-06 risk or the non-carcinogenic remediation goal at a hazard quotient of 0.2 is listed.
1 - Adapted from the 2008 USEPA Regional Screening Tables. Cleanup below method detection limits using
analytical methods prescribed in the guidelines, is not required.
2 - The arsenic value is the non-carcinogenic value because the carcinogenic value is below the laboratory
method detection limit (MDL).
3 - When adjusting the remediation goals for a chemical as described in appendix E of the REC guidelines, its
Soil Saturation Concentration (Csat) must not be exceeded unless protection of groundwater concentration
have been met.
4 - Remediation goals for dioxins and furans can also be calculated as a toxic equivalency concentration (TEQ)
by using the toxicity equivalence factor (TEF) methodology. (See TEF table for dioxins and furans.)
5 - The RG is based on USEPA guidance on lead cleanup levels. The value cannot be adjusted.
6 - Remediation goals for carcinogenic PAHs can also be calculated as a toxic equivalency concentration (TEQ)
by using the toxicity equivalence factor (TEF) methodology. (See TEF table for carcinogenic PAHs.)
7 - The RG is based on USEPA policy for cleanup of PCBs at Superfund Sites. The Branch is currently
reviewing the PCB remediation goal policy and may issue further guidance at a later date.
8 - C - The RG is based on the carcinogenic endpoint and corresponds to an excess lifetime cancer risk of 1 in
1,000,000.
N - The RG is based on the non-carcinogenic endpoint and corresponds to a hazard quotient of 0.2.
M - Contaminant is a mutagen.
Csat – Soil Saturation Concentration.
NA- Not available.
October 2008

Page 16 of 16

INACTIVE HAZARDOUS SITES BRANCH
Toxic Equivalent Factor Tables for Calculation of Soil Remediation Goals

Toxic Equivalent Factor (TEF) Table for Dioxins and Furans
CHEMICAL CASRN TEF*
Dioxins and Furans 4
CDDs
2,3,7,8-TetraCDD 1
1,2,3,7,8-PentaCDD 1
1,2,3,4,7,8-HexaCDD 0.1
1,2,3,6,7,8-HexaCDD 0.1
1,2,3,7,8,9-HexaCDD 0.1
1,2,3,4,6,7,8-HeptaCDD 0.01
1,2,3,4,6,7,8,9-OctaCDD 0.0003
CDFs
2,3,7,8-TetraCDF 0.1
1,2,3,7,8-PentaCDF 0.03
2,3,4,7,8-PentaCDF 0.3
1,2,3,4,7,8-HexaCDF 0.1
1,2,3,6,7,8-HexaCDF 0.1
1,2,3,7,8,9-HexaCDF 0.1
2,3,4,6,7,8-HexaCDF 0.1
1,2,3,4,6,7,8-HeptaCDF 0.01
1,2,3,4,7,8,9-HeptaCDF 0.01
1,2,3,4,6,7,8,9-OctaCDF 0.0003

Toxic Equivalent Factor (TEF) Table for Carcinogenic Polyaromatic Hydrocarbons (PAHs)
CHEMICAL CASRN TEF*
Polynuclear aromatic hydrocarbons 6
Benzo[a]pyrene 50328 1.0
Benzo[b]fluoranthene 205992 0.1
Benzo[k]fluoranthene 207089 0.01
Benz[a]anthracene 56553 0.1
Chrysene 218019 0.001
Dibenz[a,h]anthracene 53703 1.0
Indeno(1,2,3-cd)pyrene 193395 0.1

*These toxic equivalent factors (TEF) are to be used as per footnotes 4 and 6 on the previous page.
October 2008
26
(f) Groundwater quality standards specified in Paragraphs (g) and (h) of this Rule and interim maximum
allowable concentrations established pursuant to Paragraph (c) of this Rule shall be reviewed on a
triennial basis. Appropriate modifications to established standards shall be made in accordance with the
procedure prescribed in Paragraph (d) of this Rule where modifications are considered appropriate based
on data published subsequent to the previous review.
(g) Class GA Standards. Where not otherwise indicated, the standard refers to the total concentration in
milligrams per liter of any constituent in a dissolved, colloidal or particulate form which is mobile in
groundwater. This does not apply to sediment or other particulate matter which is preserved in a
groundwater sample as a result of well construction or sampling procedures.
(1) acetone: 0.7
(2) acenaphthene: 0.08
(3) acenaphthylene: 0.21
(4) acrylamide (propenamide): 0.000008
(5) anthracene: 2.1
(6) arsenic: 0.05
(7) atrazine and chlorotriazine metabolites: 0.0030
(8) barium: 2.0
(9) benzene: 0.001
(10) benzo(a)anthracene (benz(a)anthracene): 0.0000479
(11) benzo(b)fluoranthene: 4.79 x 10- 5
(12) benzo(k)fluoranthene: 4.79 x 10- 4
(13) benzo(g,h,i,)perylene: 0.21
(14) benzo(a)pyrene: 4.79 x 10-6
(15) boron: 0.315
(16) bromodichloromethane: 0.00056
(17) bromoform (tribromomethane): 0.00443
(18) n-butylbenzene: 0.07
(19) sec-butylbenzene: 0.07
(20) tert-butylbenzene: 0.07
(21) butylbenzyl phthalate: 0.10
(22) cadmium: 0.00175
(23) caprolactam: 3.5
(24) carbofuran: 0.035
(25) carbon disulfide: 0.7
(26) carbon tetrachloride: 0.000269
(27) chlordane: 1.0 x 10-4
(28) chloride: 250.0
(29) chlorobenzene: 0.05
(30) chloroethane: 2.80
(31) chloroform (trichloromethane): 0.07
27
(32) chloromethane (methyl chloride): 2.6 x 10-3
(33) 2-chlorophenol: 0.00036
(34) 2-chlorotoluene: 0.14
(35) chromium: 0.05
(36) chrysene: 0.00479
(37) cis-1,2-dichloroethene: 0.07
(38) coliform organisms (total): 1 per 100 milliliters
(39) color: 15 color units
(40) copper: 1.0
(41) cyanide (free cyanide): 0.07
(42) 2, 4-D (2,4-dichlorophenoxy acetic acid): 0.07
(43) dibenz(a,h)anthracene: 4.7 x 10-6
(44) 1,2-dibromo-3-chloropropane: 2.5 x 10-5
(45) dichlorodifluoromethane (Freon-12; Halon): 1.4
(46) p,p’-dichlorodiphenyl dichloroethane (DDD): 1.4 x 10-4
(47) p,p’-dichlorodiphenyltrichloroethane (DDT): 1.0 x 10-4
(48) 1,1-dichloroethane: 0.07
(49) 1,2-dichloroethane (ethylene dichloride): 0.00038
(50) 1,1-dichloroethylene (vinylidene chloride): 0.007
(51) 1,2-dichloropropane: 0.00051
(52) 1,3-dichloropropene (cis and trans isomers): 0.00019
(53) dieldrin: 2.2 x 10-6
(54) di-n-butyl (or dibutyl) phthalate (DBP): 0.7
(55) diethylphthalate (DEP): 5.0
(56) di(2-ethylhexyl) phthalate (DEHP): 0.0025
(57) 2,4-dimethylphenol (m-xylenol): 0.14
(58) di-n-octyl phthalate: 0.14
(59) p-dioxane (1,4-diethylene dioxide): 0.007
(60) dioxin: 2.2 x 10-10
(61) diphenyl (1,1– diphenyl): 0.35
(62) dissolved solids (total): 500
(63) disulfoton: 2.8 x 10-4
(64) diundecyl phthalate (Santicizer 711): 0.14
(65) endosulfan II (beta-endosulfan): 0.0420
(66) endrin: 0.002
(67) endrin (total endrin: includes endrin, endrin aldehyde, and endrin ketone): 2.1 x 10-3
(68) epichlorohydrin (1-chloro-2,3-epoxypropane): 0.00354
(69) ethylbenzene: 0.550
(70) ethylene dibromide (EDB; 1,2-dibromoethane): 4.0 x 10-7
(71) ethylene glycol: 14.0
28
(72) fluoranthene: 0.28
(73) fluorene: 0.28
(74) fluoride: 2.0
(75) foaming agents: 0.5
(76) gross alpha (adjusted)particle activity (excluding radium-226 and uranium): 15 pCi/l
(77) heptachlor: 7.8 x 10-6
(78) heptachlor epoxide: 3.8 x 10-6
(79) heptane: 0.42
(80) hexachlorobenzene (perchlorobenzene): 0.00002
(81) hexachlorocyclohexane isomers (total hexachlorocyclohexane: includes
alpha,beta,delta,gamma, and epsilon isomers): 1.9 x 10-5
(82) n-hexane: 0.42
(83) indeno(1,2,3-cd)pyrene: 4.79 x 10-5
(84) iron: 0.3
(85) isophorone: 0.0368
(86) isopropylbenzene: 0.070
(87) isopropyl ether (diisopropyl ether): 0.070
(88) lead: 0.015
(89) lindane: 2.0 x 10-4
(90) manganese: 0.05
(91) mercury: 0.00105
(92) metadichlorobenzene (1,3-dichlorobenzene): 0.170
(93) methanol: 3.5
(94) methoxychlor: 0.035
(95) methylene chloride (dichloromethane): 0.0046
(96) methyl ethyl ketone (MEK; 2-butanone): 4.20
(97) 2-methylnaphthalene: 0.0140
(98) 3-methylphenol (m-cresol): 0.0350
(99) 4-methylphenol (p-cresol): 3.5 x 10-3
(100) methyl tert-butyl ether (MTBE): 0.2
(101) naphthalene: 0.021
(102) nickel: 0.1
(103) nitrate: (as N) 10.0
(104) nitrite: (as N) 1.0
(105) N-nitrosodimethylamine: 7.0 x 10-7
(106) orthodichlorobenzene (1,2-dichlorobenzene): 0.024
(107) oxamyl: 0.175
(108) paradichlorobenzene (1,4-dichlorobenzene): 0.0014
(109) pentachlorophenol: 0.00029
(110) petroleum aliphatic carbon fraction class C5 - C8: 0.42
29
(111) petroleum aliphatic carbon fraction class C9 - C18: 4.20
(112) petroleum aliphatic carbon fraction class C19 - C36: 42.0
(113) petroleum aromatics carbon fraction class C9 – C22: 0.210
(114) pH: 6.5 - 8.5
(115) phenanthrene: 0.21
(116) phenol: 0.30
(117) phorate: 1.4 x 10-3
(118) n-propylbenzene: 0.070
(119) pyrene: 0.21
(120) selenium: 0.05
(121) silver: 0.0175
(122) simazine: 0.004
(123) styrene (ethenylbenzene): 0.1
(124) sulfate: 250.0
(125) tetrachloroethylene (perchloroethylene; PCE): 0.0007
(126) 2,3,4,6-tetrachlorophenol: 0.210
(127) toluene (methylbenzene): 1.0
(128) toxaphene: 3.1 x 10-5
(129) 2, 4, 5,-TP (Silvex): 0.05
(130) trans-1,2-dichloroethene: 0.10
(131) 1,1,1-trichloroethane (methyl chloroform): 0.2
(132) trichloroethylene (TCE): 0.0028
(133) trichlorofluoromethane: 2.1
(134) 1,1,2-trichloro-1,2,2-trifluoroethane (CFC-113): 210.0
(135) 1,2,3- trichloropropane: 5.0 x 10-6
(136) 1,2,4-trimethylbenzene: 0.350
(137) 1,3,5-trimethylbenzene: 0.350
(138) vinyl chloride (chloroethylene): 1.5 x 10-5
(139) xylenes (o-, m-, and p-): 0.53
(140) zinc: 1.05
(h) Class GSA Standards. The standards for this class shall be the same as those for Class GA except as
follows:
(1) chloride: allowable increase not to exceed 100 percent of the natural quality
concentration.
(2) total dissolved solids: 1000 mg/l.
(i) Class GC Waters.
(1) The concentrations of substances which, at the time of classification exceed the standards
applicable to Class GA or GSA groundwaters shall not be caused to increase, nor shall
the concentrations of other substances be caused to exceed the GA or GSA standards as a
30
result of further disposal of contaminants to or beneath the surface of the land within the
boundary of the area classified GC.
(2) The concentrations of substances which, at the time of classification, exceed the
standards applicable to GA or GSA groundwaters shall not be caused to migrate as a
result of activities within the boundary of the GC classification, so as to violate the
groundwater or surface water quality standards in adjoining waters of a different class.
(3) Concentrations of specific substances, which exceed the established standard at the time
of classification, shall be listed in Section .0300 of this Subchapter.
History Note: Authority G.S. 143-214.1; 143B-282(a)(2);
Eff. June 10, 1979;
Amended Eff. November 1, 1994; October 1, 1993; September 1, 1992; August 1, 1989;
Temporary Amendment Eff. June 30, 2002;
Amended Eff. August 1, 2002;
Temporary Amendment Expired February 9, 2003;
Amended Eff. April 1, 2005.
SECTION .0300 - ASSIGNMENT OF UNDERGROUND WATER CLASSIFICATIONS
15A NCAC 02L .0301 CLASSIFICATIONS: GENERAL
(a) Schedule of Classifications. The classifications are based on the quality, occurrence and existing or
contemplated best usage of the groundwaters as established in Section .0200 of this Subchapter and are
assigned statewide except where supplemented or supplanted by specific classification assignments by
major river basins.
(b) Classifications and Water Quality Standards. The classifications and standards assigned to the
groundwaters are denoted by the letters GA, GSA, or GC. These classifications refer to the
classifications and standards established by Rule .0201 of this Subchapter.
History Note: Authority G.S. 143-214.1; 143B-282(2);
Eff. December 30, 1983;
Amended Eff. August 1, 1989.
15A NCAC 02L .0302 STATEWIDE

GUIDELINES FOR SITE CHECKS, TANK CLOSURE,
AND INITIAL RESPONSE AND ABATEMENT
FOR UST RELEASES

UST Section

North Carolina
Department of Environment and Natural Resources
Division of Waste Management

March 1, 2007 Version
Change 3, Effective December 1, 2008

4
4.0 UST Site Check Guidelines for Regulated UST Systems

4.1 Regulatory Authority

A site check is required if a release from a regulated UST system has been suspected or confirmed
by the presence, at the site or nearby, of the regulated substance as free product, dissolved product,
or vapor in soils, sewer and utility lines, surface water, groundwater, etc; by unusual operating
conditions; or by leak detection and/or tightness testing results, in accordance with 15A NCAC 2N
.0601 and .0603 and .0701- .0704. A site check is required if a spill or overfill is known to have
occurred at the site. A site check is also required if the UST system is suspected to be the source of
an off-site impact, in accordance with 15A NCAC 2N .0602.

4.2 Site Check Description

The site check assessment procedure requires sampling where contamination is observed or is
most likely to be present at the site. The scope of assessment therefore includes the soil
surrounding the entire UST system and the groundwater. The sampling procedure requires the
same sampling protocol required for UST closure. The sampling protocol must consider the
nature of the stored substance, the type of initial alarm or cause for suspicion, the type of
backfill, the depth to groundwater, and any other factors appropriate for identifying the presence
and source of the release. Site check activities are required of owners and operators of UST
systems in any of the circumstances described below:

1) Evidence of a release is present at the UST site or is found offsite and may be related to a
release at the UST site. Such evidence includes, but is not limited to, the discovery of the
presence of regulated substances (such as dissolved product, free product, or vapors) in soils,
basements, sewer or utility lines, and nearby surface water and groundwater;

2) Tightness test results for the UST system do not indicate that a leak exists, but
environmental contamination indicates that a release from the UST system may have
occurred;

3) The applied method of leak detection indicates a suspected release and a follow-up
tightness test confirms that result;

4) A spill or overfill of a regulated substance has occurred.

If State Trust Fund reimbursement is anticipated, please refer to the current version of the
Reasonable Rate Document for information about allowed reimbursement.

4.3 Site Check Requirements

When conducting a site check, the procedures below must be included:

5
1) Soil samples must be collected around the perimeter of a single UST or around the
perimeter of a set of USTs in a single pit, according to the sampling procedure described in
item #1 of 5.3.B, Removal of UST(s) underlain by a concrete pad. Samples must be
collected within 3 feet of the UST(s) at a depth equal to the depth of the tank bottom(s) or no
deeper than 2 feet below the depth of the tank bottom into the native soil.

2) One sample must be collected at the fill port of each UST (or under any catchment basin
at the fill port) to document overfills.

3) Soil samples must also be collected underneath associated product lines, dispensers,
containment sumps, turbine pumps or turbine containment sumps, and other areas where
contamination is suspected or observed, as described in 5.3.F.

Note that it may not be necessary to collect samples from around the entire system, as
indicated in items 1-3 above, if the area of the suspected release is localized.

Note also that if the UST system contains an ethanol-gasoline blend, the UST Section will
determine if the assessment required in items 1-3 is adequate.

4) All soil samples must be analyzed by approved methods as specified in Table 1, p. 31.

5) If required by the UST Section, a permanent monitoring well, constructed according to
Title 15A NCAC 2C, Well Construction Standards, must be installed as close as possible to
and within 5 feet of the (part of the) UST system with the (suspected) release in a
downgradient direction, and a groundwater sample must be collected and analyzed as
specified in Tables 2 and 6.

6) If the results of the site check indicate that no soil contamination equals or exceeds 10
mg/kg TPH for petroleum (or exceeds the soil-to-groundwater MSCC, or the MDL if no
MSCC is established, for regulated hazardous substances), no groundwater contamination
exceeds the groundwater quality standard established in 15A NCAC 2L .0202, and no free
product is present, then the results must be reported to the UST Section in a Site Check
Report (Appendix A, p. 48). The Site Check Report must be submitted to the branch of the
UST Section which requested it (to Permits and Inspections Branch, if required by a UST
inspector, or to the appropriate regional office of the Corrective Action Branch, if required by
an incident manager). The Site Check Report must be received by the UST Section within
30 days of the receipt of the Notice of Regulatory Requirements or the Notice of Violation.
If it was necessary to remove all or part of the UST system to allow access for site check
sampling, then the required UST closure report elements (UST-12 Format with UST-2 Form,
Appendix A, p. 60) should be submitted as part of the Site Check Report. The reporting
requirements are described in Section 8.0, and the outline of the format is presented in
Appendix A, p. 48. No further action will be required.

7) If the results of the site check indicate that soil contamination equals or exceeds 10 mg/kg
TPH for petroleum (or exceeds the soil-to-groundwater MSCCs, or the MDL if no MSCC is
established, for regulated hazardous substances), groundwater contamination exceeds the 2L

Change 2 6
standards, or free product is present, then the initial response and abatement actions must be
performed. A flowchart illustrating the requirements for releases discovered during site
checks is presented as Figure 1 on p. 41.

Initial response actions which are required include submittal of a 24-Hour Release and
Reporting Form (Appendix A, p. 54) to the UST Section within 24 hours following discovery
of the release; action to stop the release; and identification and mitigation of hazards from
exposure to pollutants.

Initial abatement actions include determination of the source of the release (if not previously
identified); investigation and removal of free product; submittal of a 20-Day Report
(Appendix A, p. 56) to the UST Section within 20 days following discovery of the release;
and excavation of contaminated soil to the maximum extent possible, followed by
confirmation sampling as described in Section 9.1 and in Table 1, p. 31. The final results of
the initial abatement actions for a petroleum release must be reported in an Initial Abatement
Action Report (Appendix A, p. 66), which must be submitted to the UST Section within 90
days following discovery of the release. (The final results of the initial abatement actions for
a hazardous substance release must be reported in a 45-Day Report, the requirements for
which are addressed in the current version of the Guidelines for Assessment and Corrective
Action for UST Releases; the 45-Day Report must be submitted within 45 days following
discovery of the release.)

The 24-Hour Report, the 20-Day-Report, and the Initial Abatement Action Report (or the 45-
Day Report, for a hazardous substance release) must be submitted to the branch of the UST
Section which requested it (to Permits and Inspections Branch, if required by a UST
inspector, or to the appropriate regional office of the Corrective Action Branch, if required by
an incident manager). If it was necessary to remove all or part of the UST system to allow
access for site check sampling and/or excavation, then the required UST closure report
elements (UST-12 Format with UST-2 Form, Appendix A, p. 60) should be submitted as part
of the Initial Abatement Action Report. The reporting requirements are described in Section
8.0, and the outline of the format is presented in Appendix A, p. 66.

8) If the Initial Abatement Action Report for a petroleum release shows that post-excavation
soil contaminant concentrations do not exceed the lower of the soil-to-groundwater or
residential maximum soil contaminant concentrations (MSCCs) and reports that neither
groundwater nor bedrock has been encountered in the excavation, then no further action will
be required. However, if the Initial Abatement Action Report indicates that soil contaminant
concentrations exceed the lower of the soil-to-groundwater or residential MSCCs or reports
that groundwater or bedrock has been encountered in the excavation, then the responsible
party must perform further assessment and submit a Limited Site Assessment Report within
120 days of the discovery of the release. The Limited Site Assessment Report format is
presented in the Guidelines for Assessment and Corrective for UST Releases, current version.

44
Figure 4
Flowchart of Requirements for Non-Regulated Petroleum UST System Releases

PERFORM INITIAL ABATEMENT ACTIONS
Submit 24-hour
Release and Report
Form within 24 hours
of discovery of release
Submit 20-Day Report
within 20 days of
confirmation of release
Excavate contaminated soil
to maximum extent
possible (mandatory)
See Section 7.0
Perform and submit Limited Site Assessment Report
within 120 days of discovery of release. (Refer to
Guidelines for Assessment and Corrective Action)
Submit Initial Abatement Action
(including Excavation, Post-
Excavation Soil Contamination
Assessment) Report within 90 days of
discovery of release
No further action
If soil >lowest MSCCs,
bedrock is encountered in
excavation, or
groundwater is
encountered and is >2L
If soil <lowest MSCCs,
bedrock is not
encountered in
excavation, and
groundwater is not
encountered (or is
encountered but is <2L)
Collect/analyze post-excavation soil samples; and, if groundwater is
encountered in the excavation, install a monitoring well and
sample/analyze groundwater.
ID &
mitigate fire,
explosion,
vapor
hazards
ID & mitigate
hazards from
exposure to
pollutants
(supply alternate
water)
Determine source
or presence of
release if previous
activities have
failed to do so.
Act to
prevent
further
release
On discovery of evidence of a release (vapors,
staining, FP sheen), sample soil to confirm. If
release is confirmed, remove UST and collect and
analyze additional soil (and groundwater samples)
using regulated closure assessment procedure and
analytical methods (TPH).
If soil >10 mg/kg TPH
or groundwater or
bedrock is encountered
(and groundwater is>2L)
If soil <10 mg/kg TPH
and groundwater and
bedrock are not
encountered (or
groundwater is <2L)
No
further
action
PERFORM INITIAL RESPONSE ACTIONS
Investigate/
begin to
recover FP
within 14 days
Soil and Groundwater Assessment Report S&ME Project No. 1411-09-025
Silverman Property / 48 Swannanoa River Road, Asheville, NC August 25, 2009

IV-1
APPENDIX IV
(LABORATORY REPORTS)

July 27, 2009
LIMS USE: FR - SCOTT SPINNER
LIMS OBJECT ID: 9247665
9247665
Project:
Pace Project No.:
RE:
Mr. Scott SpinnerS&ME44 Buck Shoals RoadArden, NC 28704
SILVERMAN PROPERTY 1411-09-025
Dear Mr. Spinner:
Enclosed are the analytical results for sample(s) received by the laboratory between June 30, 2009
and July 02, 2009. The results relate only to the samples included in this report. Results reportedherein conform to the most current NELAC standards, where applicable, unless otherwise narrated
in the body of the report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Charlotte Certification IDsWest Virginia Certification #: 357Virginia Certification #: 00213Tennessee Certification #: 04010South Carolina Drinking Water Cert. #: 990060003South Carolina Certification #: 990060001Pennsylvania Certification #: 68-00784Connecticut Certification #: PH-0104
North Carolina Field Services Certification #: 5342North Carolina Drinking Water Certification #: 37706New Jersey Certification #: NC012Louisiana/LELAP Certification #: 04034Kentucky UST Certification #: 84Florida/NELAP Certification #: E87627North Carolina Wastewater Certification #: 12
Asheville Certification IDsWest Virginia Certification #: 356Virginia Certification #: 00072Connecticut Certification #: PH-0106Florida/NELAP Certification #: E87648Tennessee Certification #: 2980South Carolina Certification #: 99030001South Carolina Bioassay Certification #: 99030002
Pennsylvania Certification #: 68-03578North Carolina Wastewater Certification #: 40North Carolina Drinking Water Certification #: 37712North Carolina Bioassay Certification #: 9New Jersey Certification #: NC011Massachusetts Certification #: M-NC030Louisiana/LELAP Certification #: 03095
Eden Certification IDsNorth Carolina Wastewater Certification #: 633Virginia Drinking Water Certification #: 00424 North Carolina Drinking Water Certification #: 37738
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
9247665001 SILV-SB8-06-09 9071B ASE 1 PASI-CDNP
ASTM D2974-87 1 PASI-CTNM
EPA 6010 2 PASI-ASHB
EPA 8260 71 PASI-CDLK
9247665002 SILV-SB6-06-09 9071B ASE 1 PASI-CDNP
ASTM D2974-87 1 PASI-CTNM
EPA 6010 2 PASI-ASHB
EPA 7471 1 PASI-ASAJ
EPA 8260 71 PASI-CDLK
9247665003 SILV-SB7-06-09 9071B ASE 1 PASI-CDNP
ASTM D2974-87 1 PASI-CTNM
EPA 6010 2 PASI-ASHB
EPA 7471 1 PASI-ASAJ
EPA 8260 71 PASI-CDLK
9247665004 SILV-SB9-06-09 9071B ASE 1 PASI-CDNP
ASTM D2974-87 1 PASI-CTNM
9247665005 SILV-SB10-06-09 9071B ASE 1 PASI-CDNP
ASTM D2974-87 1 PASI-CTNM
9247665006 SILV-SB11-06-09 9071B ASE 1 PASI-CDNP
ASTM D2974-87 1 PASI-CTNM
EPA 6010 2 PASI-ASHB
EPA 8260 71 PASI-CDLK
9247665007 SILV-SB4-06-09 ASTM D2974-87 1 PASI-CTNM
EPA 6010 1 PASI-ASHB
EPA 8260 71 PASI-CDLK
9247665008 SILV-SB5-06-09 ASTM D2974-87 1 PASI-CTNM
EPA 6010 1 PASI-ASHB
EPA 8260 71 PASI-CDLK
9247665009 SILV-SB3-06-09 9071B ASE 1 PASI-CDNP
ASTM D2974-87 1 PASI-CTNM
9247665010 SILV-SB2-06-09 ASTM D2974-87 1 PASI-CTNM
EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-ASAJ
9247665011 SILV-SB1-06-09 ASTM D2974-87 1 PASI-CTNM
EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-ASAJ
9247665012 SILV-SB19-06-09 9071B ASE 1 PASI-CDNP
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
ASTM D2974-87 1 PASI-CTNM
EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-ASAJ
EPA 8015 Modified 4 PASI-CDHW, JAC
EPA 8260 71 PASI-CDLK
EPA 8270 75 PASI-CBET
9247665013 SILV-DUPLICATE 1 06-09 9071B ASE 1 PASI-CDNP
ASTM D2974-87 1 PASI-CTNM
EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-ASAJ
EPA 8015 Modified 4 PASI-CHM, JAC
EPA 8260 71 PASI-CDLK
EPA 8270 75 PASI-CBET
9247665014 SILV-SB20-06-09 9071B ASE 1 PASI-CDNP
ASTM D2974-87 1 PASI-CTNM
EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-ASAJ
EPA 8015 Modified 4 PASI-CHM, JAC
EPA 8260 71 PASI-CDLK
EPA 8270 75 PASI-CBET
9247665015 SILV-SB21-06-09 9071B ASE 1 PASI-CDNP
ASTM D2974-87 1 PASI-CTNM
EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-ASAJ
EPA 8015 Modified 4 PASI-CHM, JAC
EPA 8260 71 PASI-CDLK
EPA 8270 75 PASI-CBET
9247665016 SILV-SB22-06-09 9071B ASE 1 PASI-CDNP
ASTM D2974-87 1 PASI-CTNM
EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-ASAJ
EPA 8015 Modified 4 PASI-CHM, JAC
EPA 8260 71 PASI-CDLK
EPA 8270 75 PASI-CBET
9247665017 SILV-SB23-06-09 9071B ASE 1 PASI-CDNP
ASTM D2974-87 1 PASI-CTNM
EPA 6010 13 PASI-ASHB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7471 1 PASI-ASAJ
EPA 8015 Modified 4 PASI-CHM, JAC
EPA 8260 71 PASI-CDLK
EPA 8270 75 PASI-CBET
9247665018 SILV-SB24-06-09 9071B ASE 1 PASI-CDNP
ASTM D2974-87 1 PASI-CTNM
EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-ASAJ
EPA 8015 Modified 4 PASI-CHM, JAC
EPA 8260 71 PASI-CDLK
EPA 8270 75 PASI-CBET
9247665019 SILV-SB25-06-09 9071B ASE 1 PASI-CDNP
ASTM D2974-87 1 PASI-CTNM
EPA 6010 13 PASI-ASHB
EPA 7471 1 PASI-ASAJ
EPA 8015 Modified 4 PASI-CHM, JAC
EPA 8260 71 PASI-CDLK
EPA 8270 75 PASI-CBET
9247665020 SILV-SB26-06-09 ASTM D2974-87 1 PASI-CTNM
EPA 8015 Modified 4 PASI-CHM, JAC
9247665021 SILV-SB27-06-09 ASTM D2974-87 1 PASI-CTNM
EPA 8015 Modified 4 PASI-CHM, JAC
9247665022 SILV-EQUIP RINSATE-06-09 EPA 1664A 1 PASI-CDNP
EPA 200.7 13 PASI-ASHB
EPA 245.1 1 PASI-ASHB
EPA 5030/8015 Mod.2 PASI-CDHW
EPA 8015 Modified 2 PASI-CJAC
EPA 8260 63 PASI-CMCK
EPA 8270 75 PASI-CBET
9247665023 SILV-TRIP BLANK 1-06-09 EPA 8260 63 PASI-CMCK
9247665024 SILV-TRIP BLANK 2-06-09 EPA 8260 63 PASI-CMCK
9247665025 SILV-TRIP BLANK 3-06-09 EPA 8260 63 PASI-CMCK
9247665026 SILV-TW3-SS1-07-09 ASTM D2974-87 1 PASI-CTNM
EPA 6010 1 PASI-ASHB
EPA 8260 71 PASI-CDLK
9247665027 SILV-TW3-SS2-07-09 ASTM D2974-87 1 PASI-CTNM
EPA 6010 1 PASI-ASHB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8260 71 PASI-CDLK
9247665028 SILV-DUPLICATE1-07-09 ASTM D2974-87 1 PASI-CTNM
EPA 6010 1 PASI-ASHB
EPA 8260 71 PASI-CDLK
9247665029 SILV-SB18-07-09 ASTM D2974-87 1 PASI-CTNM
EPA 8015 Modified 4 PASI-CDHW, JAC
9247665030 SILV-DUPLICATE 2-07-09 ASTM D2974-87 1 PASI-CTNM
EPA 8015 Modified 4 PASI-CDHW, JAC
9247665031 SILV-SB17-07-09 ASTM D2974-87 1 PASI-CTNM
EPA 8015 Modified 4 PASI-CDHW, JAC
9247665032 SILV-SB15-07-09 ASTM D2974-87 1 PASI-CTNM
EPA 8015 Modified 4 PASI-CDHW, JAC
9247665033 SILV-SB14-07-09 ASTM D2974-87 1 PASI-CTNM
EPA 8015 Modified 4 PASI-CHM, JAC
9247665034 SILV-SB13-07-09 ASTM D2974-87 1 PASI-CTNM
EPA 8015 Modified 4 PASI-CHM, JAC
9247665035 SILV-TRIP BLANK 1 07-09 EPA 8260 63 PASI-CMCK
9247665036 SILV-EQUIP RINSATE 07-09 EPA 200.7 1 PASI-ASHB
EPA 8260 63 PASI-CMCK
9247665037 SILV-FIELD BLANK-07-09 EPA 8260 63 PASI-CMCK
9247665038 SILV-TW1-07-09 EPA 8260 63 PASI-CMCK
EPA 8270 75 PASI-CBET
9247665039 SILV-TW4-07-09 EPA 8260 63 PASI-CMCK
EPA 8270 75 PASI-CBET
9247665040 SILV-TW3-07-09 EPA 200.7 1 PASI-ASHB
EPA 8260 63 PASI-CMCK
9247665041 SILV-TW5-07-09 EPA 8260 63 PASI-CMCK
EPA 8270 75 PASI-CBET
9247665042 SILV-DUPLICATE1-07-09 EPA 8260 63 PASI-CMCK
EPA 8270 75 PASI-CBET
9247665043 SILV-TW6-07-09 EPA 8260 63 PASI-CMCK
EPA 8270 75 PASI-CBET
9247665044 SILV-TRIP BLANK1-07-09 EPA 8260 63 PASI-CMCK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB8-06-09 Lab ID:9247665001 Collected:06/30/09 10:30 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
9071 Oil and Grease Analytical Method: 9071B ASE Preparation Method: 9071B ASE
Oil and Grease 3210 mg/kg 1 07/09/09 14:2907/09/09 13:1089.8
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Chromium 8.1 mg/kg 1 07/07/09 17:48 7440-47-307/06/09 15:100.48
Lead 1150 mg/kg 5 07/08/09 13:57 7439-92-107/06/09 15:102.4
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/07/09 13:32 67-64-1139
Benzene ND ug/kg 1 07/07/09 13:32 71-43-26.9
Bromobenzene ND ug/kg 1 07/07/09 13:32 108-86-16.9
Bromochloromethane ND ug/kg 1 07/07/09 13:32 74-97-56.9
Bromodichloromethane ND ug/kg 1 07/07/09 13:32 75-27-46.9
Bromoform ND ug/kg 1 07/07/09 13:32 75-25-26.9
Bromomethane ND ug/kg 1 07/07/09 13:32 74-83-913.9
2-Butanone (MEK)ND ug/kg 1 07/07/09 13:32 78-93-3139
n-Butylbenzene ND ug/kg 1 07/07/09 13:32 104-51-86.9
sec-Butylbenzene ND ug/kg 1 07/07/09 13:32 135-98-86.9
tert-Butylbenzene ND ug/kg 1 07/07/09 13:32 98-06-66.9
Carbon tetrachloride ND ug/kg 1 07/07/09 13:32 56-23-56.9
Chlorobenzene ND ug/kg 1 07/07/09 13:32 108-90-76.9
Chloroethane ND ug/kg 1 07/07/09 13:32 75-00-313.9
Chloroform ND ug/kg 1 07/07/09 13:32 67-66-36.9
Chloromethane ND ug/kg 1 07/07/09 13:32 74-87-313.9
2-Chlorotoluene ND ug/kg 1 07/07/09 13:32 95-49-86.9
4-Chlorotoluene ND ug/kg 1 07/07/09 13:32 106-43-46.9
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/07/09 13:32 96-12-86.9
Dibromochloromethane ND ug/kg 1 07/07/09 13:32 124-48-16.9
1,2-Dibromoethane (EDB)ND ug/kg 1 07/07/09 13:32 106-93-46.9
Dibromomethane ND ug/kg 1 07/07/09 13:32 74-95-36.9
1,2-Dichlorobenzene ND ug/kg 1 07/07/09 13:32 95-50-16.9
1,3-Dichlorobenzene ND ug/kg 1 07/07/09 13:32 541-73-16.9
1,4-Dichlorobenzene ND ug/kg 1 07/07/09 13:32 106-46-76.9
Dichlorodifluoromethane ND ug/kg 1 07/07/09 13:32 75-71-813.9
1,1-Dichloroethane ND ug/kg 1 07/07/09 13:32 75-34-36.9
1,2-Dichloroethane ND ug/kg 1 07/07/09 13:32 107-06-26.9
1,1-Dichloroethene ND ug/kg 1 07/07/09 13:32 75-35-46.9
cis-1,2-Dichloroethene ND ug/kg 1 07/07/09 13:32 156-59-26.9
trans-1,2-Dichloroethene ND ug/kg 1 07/07/09 13:32 156-60-56.9
1,2-Dichloropropane ND ug/kg 1 07/07/09 13:32 78-87-56.9
1,3-Dichloropropane ND ug/kg 1 07/07/09 13:32 142-28-96.9
2,2-Dichloropropane ND ug/kg 1 07/07/09 13:32 594-20-76.9
1,1-Dichloropropene ND ug/kg 1 07/07/09 13:32 563-58-66.9
cis-1,3-Dichloropropene ND ug/kg 1 07/07/09 13:32 10061-01-56.9
trans-1,3-Dichloropropene ND ug/kg 1 07/07/09 13:32 10061-02-66.9
Diisopropyl ether ND ug/kg 1 07/07/09 13:32 108-20-36.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 7 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB8-06-09 Lab ID:9247665001 Collected:06/30/09 10:30 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/07/09 13:32 100-41-46.9
Hexachloro-1,3-butadiene ND ug/kg 1 07/07/09 13:32 87-68-36.9
2-Hexanone ND ug/kg 1 07/07/09 13:32 591-78-669.4
Isopropylbenzene (Cumene)ND ug/kg 1 07/07/09 13:32 98-82-86.9
p-Isopropyltoluene ND ug/kg 1 07/07/09 13:32 99-87-66.9
Methylene Chloride ND ug/kg 1 07/07/09 13:32 75-09-227.8
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/07/09 13:32 108-10-169.4
Methyl-tert-butyl ether ND ug/kg 1 07/07/09 13:32 1634-04-46.9
Naphthalene ND ug/kg 1 07/07/09 13:32 91-20-36.9
n-Propylbenzene ND ug/kg 1 07/07/09 13:32 103-65-16.9
Styrene ND ug/kg 1 07/07/09 13:32 100-42-56.9
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/07/09 13:32 630-20-66.9
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/07/09 13:32 79-34-56.9
Tetrachloroethene ND ug/kg 1 07/07/09 13:32 127-18-46.9
Toluene ND ug/kg 1 07/07/09 13:32 108-88-36.9
1,2,3-Trichlorobenzene ND ug/kg 1 07/07/09 13:32 87-61-66.9
1,2,4-Trichlorobenzene ND ug/kg 1 07/07/09 13:32 120-82-16.9
1,1,1-Trichloroethane ND ug/kg 1 07/07/09 13:32 71-55-66.9
1,1,2-Trichloroethane ND ug/kg 1 07/07/09 13:32 79-00-56.9
Trichloroethene ND ug/kg 1 07/07/09 13:32 79-01-66.9
Trichlorofluoromethane ND ug/kg 1 07/07/09 13:32 75-69-46.9
1,2,3-Trichloropropane ND ug/kg 1 07/07/09 13:32 96-18-46.9
1,2,4-Trimethylbenzene ND ug/kg 1 07/07/09 13:32 95-63-66.9
1,3,5-Trimethylbenzene ND ug/kg 1 07/07/09 13:32 108-67-86.9
Vinyl acetate ND ug/kg 1 07/07/09 13:32 108-05-469.4
Vinyl chloride ND ug/kg 1 07/07/09 13:32 75-01-413.9
Xylene (Total)ND ug/kg 1 07/07/09 13:32 1330-20-713.9
m&p-Xylene ND ug/kg 1 07/07/09 13:32 1330-20-713.9
o-Xylene ND ug/kg 1 07/07/09 13:32 95-47-66.9
Dibromofluoromethane (S)110 %1 07/07/09 13:32 1868-53-779-116
Toluene-d8 (S)93 %1 07/07/09 13:32 2037-26-588-110
4-Bromofluorobenzene (S)82 %1 07/07/09 13:32 460-00-474-115
1,2-Dichloroethane-d4 (S)103 %1 07/07/09 13:32 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 22.0 %1 07/03/09 08:260.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 8 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB6-06-09 Lab ID:9247665002 Collected:06/30/09 10:45 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
9071 Oil and Grease Analytical Method: 9071B ASE Preparation Method: 9071B ASE
Oil and Grease ND mg/kg 1 07/09/09 14:3007/09/09 13:10104
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Chromium 21.9 mg/kg 1 07/07/09 17:52 7440-47-307/06/09 15:100.65
Lead 427 mg/kg 1 07/07/09 17:52 7439-92-107/06/09 15:100.65
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.21 mg/kg 5 07/13/09 13:56 7439-97-607/13/09 10:440.034
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/06/09 19:43 67-64-1119
Benzene ND ug/kg 1 07/06/09 19:43 71-43-26.0
Bromobenzene ND ug/kg 1 07/06/09 19:43 108-86-16.0
Bromochloromethane ND ug/kg 1 07/06/09 19:43 74-97-56.0
Bromodichloromethane ND ug/kg 1 07/06/09 19:43 75-27-46.0
Bromoform ND ug/kg 1 07/06/09 19:43 75-25-26.0
Bromomethane ND ug/kg 1 07/06/09 19:43 74-83-911.9
2-Butanone (MEK)ND ug/kg 1 07/06/09 19:43 78-93-3119
n-Butylbenzene ND ug/kg 1 07/06/09 19:43 104-51-86.0
sec-Butylbenzene ND ug/kg 1 07/06/09 19:43 135-98-86.0
tert-Butylbenzene ND ug/kg 1 07/06/09 19:43 98-06-66.0
Carbon tetrachloride ND ug/kg 1 07/06/09 19:43 56-23-56.0
Chlorobenzene ND ug/kg 1 07/06/09 19:43 108-90-76.0
Chloroethane ND ug/kg 1 07/06/09 19:43 75-00-311.9
Chloroform ND ug/kg 1 07/06/09 19:43 67-66-36.0
Chloromethane ND ug/kg 1 07/06/09 19:43 74-87-311.9
2-Chlorotoluene ND ug/kg 1 07/06/09 19:43 95-49-86.0
4-Chlorotoluene ND ug/kg 1 07/06/09 19:43 106-43-46.0
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/06/09 19:43 96-12-86.0
Dibromochloromethane ND ug/kg 1 07/06/09 19:43 124-48-16.0
1,2-Dibromoethane (EDB)ND ug/kg 1 07/06/09 19:43 106-93-46.0
Dibromomethane ND ug/kg 1 07/06/09 19:43 74-95-36.0
1,2-Dichlorobenzene ND ug/kg 1 07/06/09 19:43 95-50-16.0
1,3-Dichlorobenzene ND ug/kg 1 07/06/09 19:43 541-73-16.0
1,4-Dichlorobenzene ND ug/kg 1 07/06/09 19:43 106-46-76.0
Dichlorodifluoromethane ND ug/kg 1 07/06/09 19:43 75-71-811.9
1,1-Dichloroethane ND ug/kg 1 07/06/09 19:43 75-34-36.0
1,2-Dichloroethane ND ug/kg 1 07/06/09 19:43 107-06-26.0
1,1-Dichloroethene ND ug/kg 1 07/06/09 19:43 75-35-46.0
cis-1,2-Dichloroethene ND ug/kg 1 07/06/09 19:43 156-59-26.0
trans-1,2-Dichloroethene ND ug/kg 1 07/06/09 19:43 156-60-56.0
1,2-Dichloropropane ND ug/kg 1 07/06/09 19:43 78-87-56.0
1,3-Dichloropropane ND ug/kg 1 07/06/09 19:43 142-28-96.0
2,2-Dichloropropane ND ug/kg 1 07/06/09 19:43 594-20-76.0
1,1-Dichloropropene ND ug/kg 1 07/06/09 19:43 563-58-66.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 9 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB6-06-09 Lab ID:9247665002 Collected:06/30/09 10:45 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
cis-1,3-Dichloropropene ND ug/kg 1 07/06/09 19:43 10061-01-56.0
trans-1,3-Dichloropropene ND ug/kg 1 07/06/09 19:43 10061-02-66.0
Diisopropyl ether ND ug/kg 1 07/06/09 19:43 108-20-36.0
Ethylbenzene ND ug/kg 1 07/06/09 19:43 100-41-46.0
Hexachloro-1,3-butadiene ND ug/kg 1 07/06/09 19:43 87-68-36.0
2-Hexanone ND ug/kg 1 07/06/09 19:43 591-78-659.7
Isopropylbenzene (Cumene)ND ug/kg 1 07/06/09 19:43 98-82-86.0
p-Isopropyltoluene ND ug/kg 1 07/06/09 19:43 99-87-66.0
Methylene Chloride ND ug/kg 1 07/06/09 19:43 75-09-223.9
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/06/09 19:43 108-10-159.7
Methyl-tert-butyl ether ND ug/kg 1 07/06/09 19:43 1634-04-46.0
Naphthalene ND ug/kg 1 07/06/09 19:43 91-20-36.0
n-Propylbenzene ND ug/kg 1 07/06/09 19:43 103-65-16.0
Styrene ND ug/kg 1 07/06/09 19:43 100-42-56.0
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/06/09 19:43 630-20-66.0
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/06/09 19:43 79-34-56.0
Tetrachloroethene ND ug/kg 1 07/06/09 19:43 127-18-46.0
Toluene ND ug/kg 1 07/06/09 19:43 108-88-36.0
1,2,3-Trichlorobenzene ND ug/kg 1 07/06/09 19:43 87-61-66.0
1,2,4-Trichlorobenzene ND ug/kg 1 07/06/09 19:43 120-82-16.0
1,1,1-Trichloroethane ND ug/kg 1 07/06/09 19:43 71-55-66.0
1,1,2-Trichloroethane ND ug/kg 1 07/06/09 19:43 79-00-56.0
Trichloroethene ND ug/kg 1 07/06/09 19:43 79-01-66.0
Trichlorofluoromethane ND ug/kg 1 07/06/09 19:43 75-69-46.0
1,2,3-Trichloropropane ND ug/kg 1 07/06/09 19:43 96-18-46.0
1,2,4-Trimethylbenzene ND ug/kg 1 07/06/09 19:43 95-63-66.0
1,3,5-Trimethylbenzene ND ug/kg 1 07/06/09 19:43 108-67-86.0
Vinyl acetate ND ug/kg 1 07/06/09 19:43 108-05-459.7
Vinyl chloride ND ug/kg 1 07/06/09 19:43 75-01-411.9
Xylene (Total)ND ug/kg 1 07/06/09 19:43 1330-20-711.9
m&p-Xylene ND ug/kg 1 07/06/09 19:43 1330-20-711.9
o-Xylene ND ug/kg 1 07/06/09 19:43 95-47-66.0
Dibromofluoromethane (S)105 %1 07/06/09 19:43 1868-53-779-116
Toluene-d8 (S)96 %1 07/06/09 19:43 2037-26-588-110
4-Bromofluorobenzene (S)91 %1 07/06/09 19:43 460-00-474-115
1,2-Dichloroethane-d4 (S)103 %1 07/06/09 19:43 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 32.6 %1 07/03/09 08:260.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 10 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB7-06-09 Lab ID:9247665003 Collected:06/30/09 11:10 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
9071 Oil and Grease Analytical Method: 9071B ASE Preparation Method: 9071B ASE
Oil and Grease 867 mg/kg 1 07/09/09 14:3007/09/09 13:1083.5
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Chromium 31.2 mg/kg 1 07/07/09 17:56 7440-47-307/06/09 15:100.39
Lead 1090 mg/kg 5 07/08/09 14:01 7439-92-107/06/09 15:102.0
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 3.1 mg/kg 50 07/13/09 13:59 7439-97-607/13/09 10:440.22
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/06/09 17:17 67-64-1144
Benzene ND ug/kg 1 07/06/09 17:17 71-43-27.2
Bromobenzene ND ug/kg 1 07/06/09 17:17 108-86-17.2
Bromochloromethane ND ug/kg 1 07/06/09 17:17 74-97-57.2
Bromodichloromethane ND ug/kg 1 07/06/09 17:17 75-27-47.2
Bromoform ND ug/kg 1 07/06/09 17:17 75-25-27.2
Bromomethane ND ug/kg 1 07/06/09 17:17 74-83-914.4
2-Butanone (MEK)ND ug/kg 1 07/06/09 17:17 78-93-3144
n-Butylbenzene ND ug/kg 1 07/06/09 17:17 104-51-87.2
sec-Butylbenzene ND ug/kg 1 07/06/09 17:17 135-98-87.2
tert-Butylbenzene ND ug/kg 1 07/06/09 17:17 98-06-67.2
Carbon tetrachloride ND ug/kg 1 07/06/09 17:17 56-23-57.2
Chlorobenzene ND ug/kg 1 07/06/09 17:17 108-90-77.2
Chloroethane ND ug/kg 1 07/06/09 17:17 75-00-314.4
Chloroform ND ug/kg 1 07/06/09 17:17 67-66-37.2
Chloromethane ND ug/kg 1 07/06/09 17:17 74-87-314.4
2-Chlorotoluene ND ug/kg 1 07/06/09 17:17 95-49-87.2
4-Chlorotoluene ND ug/kg 1 07/06/09 17:17 106-43-47.2
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/06/09 17:17 96-12-87.2
Dibromochloromethane ND ug/kg 1 07/06/09 17:17 124-48-17.2
1,2-Dibromoethane (EDB)ND ug/kg 1 07/06/09 17:17 106-93-47.2
Dibromomethane ND ug/kg 1 07/06/09 17:17 74-95-37.2
1,2-Dichlorobenzene ND ug/kg 1 07/06/09 17:17 95-50-17.2
1,3-Dichlorobenzene ND ug/kg 1 07/06/09 17:17 541-73-17.2
1,4-Dichlorobenzene ND ug/kg 1 07/06/09 17:17 106-46-77.2
Dichlorodifluoromethane ND ug/kg 1 07/06/09 17:17 75-71-814.4
1,1-Dichloroethane ND ug/kg 1 07/06/09 17:17 75-34-37.2
1,2-Dichloroethane ND ug/kg 1 07/06/09 17:17 107-06-27.2
1,1-Dichloroethene ND ug/kg 1 07/06/09 17:17 75-35-47.2
cis-1,2-Dichloroethene ND ug/kg 1 07/06/09 17:17 156-59-27.2
trans-1,2-Dichloroethene ND ug/kg 1 07/06/09 17:17 156-60-57.2
1,2-Dichloropropane ND ug/kg 1 07/06/09 17:17 78-87-57.2
1,3-Dichloropropane ND ug/kg 1 07/06/09 17:17 142-28-97.2
2,2-Dichloropropane ND ug/kg 1 07/06/09 17:17 594-20-77.2
1,1-Dichloropropene ND ug/kg 1 07/06/09 17:17 563-58-67.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 11 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB7-06-09 Lab ID:9247665003 Collected:06/30/09 11:10 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
cis-1,3-Dichloropropene ND ug/kg 1 07/06/09 17:17 10061-01-57.2
trans-1,3-Dichloropropene ND ug/kg 1 07/06/09 17:17 10061-02-67.2
Diisopropyl ether ND ug/kg 1 07/06/09 17:17 108-20-37.2
Ethylbenzene ND ug/kg 1 07/06/09 17:17 100-41-47.2
Hexachloro-1,3-butadiene ND ug/kg 1 07/06/09 17:17 87-68-37.2
2-Hexanone ND ug/kg 1 07/06/09 17:17 591-78-672.1
Isopropylbenzene (Cumene)ND ug/kg 1 07/06/09 17:17 98-82-87.2
p-Isopropyltoluene ND ug/kg 1 07/06/09 17:17 99-87-67.2
Methylene Chloride ND ug/kg 1 07/06/09 17:17 75-09-228.8
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/06/09 17:17 108-10-172.1
Methyl-tert-butyl ether ND ug/kg 1 07/06/09 17:17 1634-04-47.2
Naphthalene ND ug/kg 1 07/06/09 17:17 91-20-37.2
n-Propylbenzene ND ug/kg 1 07/06/09 17:17 103-65-17.2
Styrene ND ug/kg 1 07/06/09 17:17 100-42-57.2
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/06/09 17:17 630-20-67.2
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/06/09 17:17 79-34-57.2
Tetrachloroethene ND ug/kg 1 07/06/09 17:17 127-18-47.2
Toluene ND ug/kg 1 07/06/09 17:17 108-88-37.2
1,2,3-Trichlorobenzene ND ug/kg 1 07/06/09 17:17 87-61-67.2
1,2,4-Trichlorobenzene ND ug/kg 1 07/06/09 17:17 120-82-17.2
1,1,1-Trichloroethane ND ug/kg 1 07/06/09 17:17 71-55-67.2
1,1,2-Trichloroethane ND ug/kg 1 07/06/09 17:17 79-00-57.2
Trichloroethene ND ug/kg 1 07/06/09 17:17 79-01-67.2
Trichlorofluoromethane ND ug/kg 1 07/06/09 17:17 75-69-47.2
1,2,3-Trichloropropane ND ug/kg 1 07/06/09 17:17 96-18-47.2
1,2,4-Trimethylbenzene ND ug/kg 1 07/06/09 17:17 95-63-67.2
1,3,5-Trimethylbenzene ND ug/kg 1 07/06/09 17:17 108-67-87.2
Vinyl acetate ND ug/kg 1 07/06/09 17:17 108-05-472.1
Vinyl chloride ND ug/kg 1 07/06/09 17:17 75-01-414.4
Xylene (Total)ND ug/kg 1 07/06/09 17:17 1330-20-714.4
m&p-Xylene ND ug/kg 1 07/06/09 17:17 1330-20-714.4
o-Xylene ND ug/kg 1 07/06/09 17:17 95-47-67.2
Dibromofluoromethane (S)102 %1 07/06/09 17:17 1868-53-779-116
Toluene-d8 (S)100 %1 07/06/09 17:17 2037-26-588-110
4-Bromofluorobenzene (S)97 %1 07/06/09 17:17 460-00-474-115
1,2-Dichloroethane-d4 (S)101 %1 07/06/09 17:17 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 16.2 %1 07/03/09 08:260.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 12 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB9-06-09 Lab ID:9247665004 Collected:06/30/09 11:35 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
9071 Oil and Grease Analytical Method: 9071B ASE Preparation Method: 9071B ASE
Oil and Grease 141 mg/kg 1 07/09/09 14:3107/09/09 13:1092.3
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 24.2 %1 07/06/09 08:400.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 13 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB10-06-09 Lab ID:9247665005 Collected:06/30/09 12:05 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
9071 Oil and Grease Analytical Method: 9071B ASE Preparation Method: 9071B ASE
Oil and Grease 698 mg/kg 1 07/09/09 14:3107/09/09 13:1082.3
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 14.9 %1 07/03/09 08:290.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 14 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB11-06-09 Lab ID:9247665006 Collected:06/30/09 12:15 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
9071 Oil and Grease Analytical Method: 9071B ASE Preparation Method: 9071B ASE
Oil and Grease ND mg/kg 1 07/09/09 14:3107/09/09 13:1088.8
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Chromium 28.7 mg/kg 1 07/07/09 18:02 7440-47-307/06/09 15:100.45
Lead 6.1 mg/kg 1 07/07/09 18:02 7439-92-107/06/09 15:100.45
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/06/09 17:35 67-64-1125
Benzene ND ug/kg 1 07/06/09 17:35 71-43-26.3
Bromobenzene ND ug/kg 1 07/06/09 17:35 108-86-16.3
Bromochloromethane ND ug/kg 1 07/06/09 17:35 74-97-56.3
Bromodichloromethane ND ug/kg 1 07/06/09 17:35 75-27-46.3
Bromoform ND ug/kg 1 07/06/09 17:35 75-25-26.3
Bromomethane ND ug/kg 1 07/06/09 17:35 74-83-912.5
2-Butanone (MEK)ND ug/kg 1 07/06/09 17:35 78-93-3125
n-Butylbenzene ND ug/kg 1 07/06/09 17:35 104-51-86.3
sec-Butylbenzene ND ug/kg 1 07/06/09 17:35 135-98-86.3
tert-Butylbenzene ND ug/kg 1 07/06/09 17:35 98-06-66.3
Carbon tetrachloride ND ug/kg 1 07/06/09 17:35 56-23-56.3
Chlorobenzene ND ug/kg 1 07/06/09 17:35 108-90-76.3
Chloroethane ND ug/kg 1 07/06/09 17:35 75-00-312.5
Chloroform ND ug/kg 1 07/06/09 17:35 67-66-36.3
Chloromethane ND ug/kg 1 07/06/09 17:35 74-87-312.5
2-Chlorotoluene ND ug/kg 1 07/06/09 17:35 95-49-86.3
4-Chlorotoluene ND ug/kg 1 07/06/09 17:35 106-43-46.3
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/06/09 17:35 96-12-86.3
Dibromochloromethane ND ug/kg 1 07/06/09 17:35 124-48-16.3
1,2-Dibromoethane (EDB)ND ug/kg 1 07/06/09 17:35 106-93-46.3
Dibromomethane ND ug/kg 1 07/06/09 17:35 74-95-36.3
1,2-Dichlorobenzene ND ug/kg 1 07/06/09 17:35 95-50-16.3
1,3-Dichlorobenzene ND ug/kg 1 07/06/09 17:35 541-73-16.3
1,4-Dichlorobenzene ND ug/kg 1 07/06/09 17:35 106-46-76.3
Dichlorodifluoromethane ND ug/kg 1 07/06/09 17:35 75-71-812.5
1,1-Dichloroethane ND ug/kg 1 07/06/09 17:35 75-34-36.3
1,2-Dichloroethane ND ug/kg 1 07/06/09 17:35 107-06-26.3
1,1-Dichloroethene ND ug/kg 1 07/06/09 17:35 75-35-46.3
cis-1,2-Dichloroethene ND ug/kg 1 07/06/09 17:35 156-59-26.3
trans-1,2-Dichloroethene ND ug/kg 1 07/06/09 17:35 156-60-56.3
1,2-Dichloropropane ND ug/kg 1 07/06/09 17:35 78-87-56.3
1,3-Dichloropropane ND ug/kg 1 07/06/09 17:35 142-28-96.3
2,2-Dichloropropane ND ug/kg 1 07/06/09 17:35 594-20-76.3
1,1-Dichloropropene ND ug/kg 1 07/06/09 17:35 563-58-66.3
cis-1,3-Dichloropropene ND ug/kg 1 07/06/09 17:35 10061-01-56.3
trans-1,3-Dichloropropene ND ug/kg 1 07/06/09 17:35 10061-02-66.3
Diisopropyl ether ND ug/kg 1 07/06/09 17:35 108-20-36.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 15 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB11-06-09 Lab ID:9247665006 Collected:06/30/09 12:15 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Ethylbenzene ND ug/kg 1 07/06/09 17:35 100-41-46.3
Hexachloro-1,3-butadiene ND ug/kg 1 07/06/09 17:35 87-68-36.3
2-Hexanone ND ug/kg 1 07/06/09 17:35 591-78-662.7
Isopropylbenzene (Cumene)ND ug/kg 1 07/06/09 17:35 98-82-86.3
p-Isopropyltoluene ND ug/kg 1 07/06/09 17:35 99-87-66.3
Methylene Chloride ND ug/kg 1 07/06/09 17:35 75-09-225.1
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/06/09 17:35 108-10-162.7
Methyl-tert-butyl ether ND ug/kg 1 07/06/09 17:35 1634-04-46.3
Naphthalene ND ug/kg 1 07/06/09 17:35 91-20-36.3
n-Propylbenzene ND ug/kg 1 07/06/09 17:35 103-65-16.3
Styrene ND ug/kg 1 07/06/09 17:35 100-42-56.3
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/06/09 17:35 630-20-66.3
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/06/09 17:35 79-34-56.3
Tetrachloroethene ND ug/kg 1 07/06/09 17:35 127-18-46.3
Toluene ND ug/kg 1 07/06/09 17:35 108-88-36.3
1,2,3-Trichlorobenzene ND ug/kg 1 07/06/09 17:35 87-61-66.3
1,2,4-Trichlorobenzene ND ug/kg 1 07/06/09 17:35 120-82-16.3
1,1,1-Trichloroethane ND ug/kg 1 07/06/09 17:35 71-55-66.3
1,1,2-Trichloroethane ND ug/kg 1 07/06/09 17:35 79-00-56.3
Trichloroethene ND ug/kg 1 07/06/09 17:35 79-01-66.3
Trichlorofluoromethane ND ug/kg 1 07/06/09 17:35 75-69-46.3
1,2,3-Trichloropropane ND ug/kg 1 07/06/09 17:35 96-18-46.3
1,2,4-Trimethylbenzene ND ug/kg 1 07/06/09 17:35 95-63-66.3
1,3,5-Trimethylbenzene ND ug/kg 1 07/06/09 17:35 108-67-86.3
Vinyl acetate ND ug/kg 1 07/06/09 17:35 108-05-462.7
Vinyl chloride ND ug/kg 1 07/06/09 17:35 75-01-412.5
Xylene (Total)ND ug/kg 1 07/06/09 17:35 1330-20-712.5
m&p-Xylene ND ug/kg 1 07/06/09 17:35 1330-20-712.5
o-Xylene ND ug/kg 1 07/06/09 17:35 95-47-66.3
Dibromofluoromethane (S)104 %1 07/06/09 17:35 1868-53-779-116
Toluene-d8 (S)100 %1 07/06/09 17:35 2037-26-588-110
4-Bromofluorobenzene (S)102 %1 07/06/09 17:35 460-00-474-115
1,2-Dichloroethane-d4 (S)105 %1 07/06/09 17:35 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 21.1 %1 07/06/09 08:370.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 16 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB4-06-09 Lab ID:9247665007 Collected:06/30/09 12:35 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Lead 6560 mg/kg 10 07/08/09 14:05 7439-92-107/06/09 15:104.0
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 339 ug/kg 1 07/07/09 13:13 67-64-1 C9,IR189
Benzene ND ug/kg 1 07/07/09 13:13 71-43-29.4
Bromobenzene ND ug/kg 1 07/07/09 13:13 108-86-19.4
Bromochloromethane ND ug/kg 1 07/07/09 13:13 74-97-59.4
Bromodichloromethane ND ug/kg 1 07/07/09 13:13 75-27-49.4
Bromoform ND ug/kg 1 07/07/09 13:13 75-25-29.4
Bromomethane ND ug/kg 1 07/07/09 13:13 74-83-9 IR18.9
2-Butanone (MEK)ND ug/kg 1 07/07/09 13:13 78-93-3189
n-Butylbenzene ND ug/kg 1 07/07/09 13:13 104-51-89.4
sec-Butylbenzene ND ug/kg 1 07/07/09 13:13 135-98-89.4
tert-Butylbenzene ND ug/kg 1 07/07/09 13:13 98-06-69.4
Carbon tetrachloride ND ug/kg 1 07/07/09 13:13 56-23-59.4
Chlorobenzene ND ug/kg 1 07/07/09 13:13 108-90-79.4
Chloroethane ND ug/kg 1 07/07/09 13:13 75-00-318.9
Chloroform ND ug/kg 1 07/07/09 13:13 67-66-39.4
Chloromethane 313 ug/kg 1 07/07/09 13:13 74-87-3 IR18.9
2-Chlorotoluene ND ug/kg 1 07/07/09 13:13 95-49-89.4
4-Chlorotoluene ND ug/kg 1 07/07/09 13:13 106-43-49.4
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/07/09 13:13 96-12-89.4
Dibromochloromethane ND ug/kg 1 07/07/09 13:13 124-48-19.4
1,2-Dibromoethane (EDB)ND ug/kg 1 07/07/09 13:13 106-93-49.4
Dibromomethane ND ug/kg 1 07/07/09 13:13 74-95-39.4
1,2-Dichlorobenzene ND ug/kg 1 07/07/09 13:13 95-50-19.4
1,3-Dichlorobenzene ND ug/kg 1 07/07/09 13:13 541-73-19.4
1,4-Dichlorobenzene ND ug/kg 1 07/07/09 13:13 106-46-79.4
Dichlorodifluoromethane ND ug/kg 1 07/07/09 13:13 75-71-818.9
1,1-Dichloroethane ND ug/kg 1 07/07/09 13:13 75-34-39.4
1,2-Dichloroethane ND ug/kg 1 07/07/09 13:13 107-06-29.4
1,1-Dichloroethene ND ug/kg 1 07/07/09 13:13 75-35-49.4
cis-1,2-Dichloroethene ND ug/kg 1 07/07/09 13:13 156-59-29.4
trans-1,2-Dichloroethene ND ug/kg 1 07/07/09 13:13 156-60-59.4
1,2-Dichloropropane ND ug/kg 1 07/07/09 13:13 78-87-59.4
1,3-Dichloropropane ND ug/kg 1 07/07/09 13:13 142-28-99.4
2,2-Dichloropropane ND ug/kg 1 07/07/09 13:13 594-20-79.4
1,1-Dichloropropene ND ug/kg 1 07/07/09 13:13 563-58-69.4
cis-1,3-Dichloropropene ND ug/kg 1 07/07/09 13:13 10061-01-59.4
trans-1,3-Dichloropropene ND ug/kg 1 07/07/09 13:13 10061-02-69.4
Diisopropyl ether ND ug/kg 1 07/07/09 13:13 108-20-39.4
Ethylbenzene ND ug/kg 1 07/07/09 13:13 100-41-49.4
Hexachloro-1,3-butadiene ND ug/kg 1 07/07/09 13:13 87-68-39.4
2-Hexanone ND ug/kg 1 07/07/09 13:13 591-78-694.5
Isopropylbenzene (Cumene)ND ug/kg 1 07/07/09 13:13 98-82-89.4
p-Isopropyltoluene ND ug/kg 1 07/07/09 13:13 99-87-69.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 17 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB4-06-09 Lab ID:9247665007 Collected:06/30/09 12:35 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Methylene Chloride 45.5 ug/kg 1 07/07/09 13:13 75-09-2 C9,IR37.8
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/07/09 13:13 108-10-194.5
Methyl-tert-butyl ether ND ug/kg 1 07/07/09 13:13 1634-04-49.4
Naphthalene ND ug/kg 1 07/07/09 13:13 91-20-39.4
n-Propylbenzene ND ug/kg 1 07/07/09 13:13 103-65-19.4
Styrene ND ug/kg 1 07/07/09 13:13 100-42-59.4
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/07/09 13:13 630-20-69.4
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/07/09 13:13 79-34-59.4
Tetrachloroethene ND ug/kg 1 07/07/09 13:13 127-18-49.4
Toluene ND ug/kg 1 07/07/09 13:13 108-88-39.4
1,2,3-Trichlorobenzene ND ug/kg 1 07/07/09 13:13 87-61-69.4
1,2,4-Trichlorobenzene ND ug/kg 1 07/07/09 13:13 120-82-19.4
1,1,1-Trichloroethane ND ug/kg 1 07/07/09 13:13 71-55-69.4
1,1,2-Trichloroethane ND ug/kg 1 07/07/09 13:13 79-00-59.4
Trichloroethene ND ug/kg 1 07/07/09 13:13 79-01-69.4
Trichlorofluoromethane ND ug/kg 1 07/07/09 13:13 75-69-49.4
1,2,3-Trichloropropane ND ug/kg 1 07/07/09 13:13 96-18-49.4
1,2,4-Trimethylbenzene ND ug/kg 1 07/07/09 13:13 95-63-69.4
1,3,5-Trimethylbenzene ND ug/kg 1 07/07/09 13:13 108-67-89.4
Vinyl acetate ND ug/kg 1 07/07/09 13:13 108-05-494.5
Vinyl chloride ND ug/kg 1 07/07/09 13:13 75-01-418.9
Xylene (Total)ND ug/kg 1 07/07/09 13:13 1330-20-718.9
m&p-Xylene ND ug/kg 1 07/07/09 13:13 1330-20-718.9
o-Xylene ND ug/kg 1 07/07/09 13:13 95-47-69.4
Dibromofluoromethane (S)116 %1 07/07/09 13:13 1868-53-779-116
Toluene-d8 (S)89 %1 07/07/09 13:13 2037-26-588-110
4-Bromofluorobenzene (S)97 %1 07/07/09 13:13 460-00-474-115
1,2-Dichloroethane-d4 (S)119 %1 07/07/09 13:13 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 13.0 %1 07/06/09 08:370.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 18 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB5-06-09 Lab ID:9247665008 Collected:06/30/09 12:50 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Lead 86.6 mg/kg 1 07/07/09 18:14 7439-92-107/06/09 15:100.52
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 115 ug/kg 1 07/07/09 12:55 67-64-1 C990.7
Benzene ND ug/kg 1 07/07/09 12:55 71-43-24.5
Bromobenzene ND ug/kg 1 07/07/09 12:55 108-86-14.5
Bromochloromethane ND ug/kg 1 07/07/09 12:55 74-97-54.5
Bromodichloromethane ND ug/kg 1 07/07/09 12:55 75-27-44.5
Bromoform ND ug/kg 1 07/07/09 12:55 75-25-24.5
Bromomethane ND ug/kg 1 07/07/09 12:55 74-83-99.1
2-Butanone (MEK)ND ug/kg 1 07/07/09 12:55 78-93-390.7
n-Butylbenzene ND ug/kg 1 07/07/09 12:55 104-51-84.5
sec-Butylbenzene ND ug/kg 1 07/07/09 12:55 135-98-84.5
tert-Butylbenzene ND ug/kg 1 07/07/09 12:55 98-06-64.5
Carbon tetrachloride ND ug/kg 1 07/07/09 12:55 56-23-54.5
Chlorobenzene ND ug/kg 1 07/07/09 12:55 108-90-74.5
Chloroethane ND ug/kg 1 07/07/09 12:55 75-00-39.1
Chloroform ND ug/kg 1 07/07/09 12:55 67-66-34.5
Chloromethane ND ug/kg 1 07/07/09 12:55 74-87-39.1
2-Chlorotoluene ND ug/kg 1 07/07/09 12:55 95-49-84.5
4-Chlorotoluene ND ug/kg 1 07/07/09 12:55 106-43-44.5
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/07/09 12:55 96-12-84.5
Dibromochloromethane ND ug/kg 1 07/07/09 12:55 124-48-14.5
1,2-Dibromoethane (EDB)ND ug/kg 1 07/07/09 12:55 106-93-44.5
Dibromomethane ND ug/kg 1 07/07/09 12:55 74-95-34.5
1,2-Dichlorobenzene ND ug/kg 1 07/07/09 12:55 95-50-14.5
1,3-Dichlorobenzene ND ug/kg 1 07/07/09 12:55 541-73-14.5
1,4-Dichlorobenzene ND ug/kg 1 07/07/09 12:55 106-46-74.5
Dichlorodifluoromethane ND ug/kg 1 07/07/09 12:55 75-71-89.1
1,1-Dichloroethane ND ug/kg 1 07/07/09 12:55 75-34-34.5
1,2-Dichloroethane ND ug/kg 1 07/07/09 12:55 107-06-24.5
1,1-Dichloroethene ND ug/kg 1 07/07/09 12:55 75-35-44.5
cis-1,2-Dichloroethene ND ug/kg 1 07/07/09 12:55 156-59-24.5
trans-1,2-Dichloroethene ND ug/kg 1 07/07/09 12:55 156-60-54.5
1,2-Dichloropropane ND ug/kg 1 07/07/09 12:55 78-87-54.5
1,3-Dichloropropane ND ug/kg 1 07/07/09 12:55 142-28-94.5
2,2-Dichloropropane ND ug/kg 1 07/07/09 12:55 594-20-74.5
1,1-Dichloropropene ND ug/kg 1 07/07/09 12:55 563-58-64.5
cis-1,3-Dichloropropene ND ug/kg 1 07/07/09 12:55 10061-01-54.5
trans-1,3-Dichloropropene ND ug/kg 1 07/07/09 12:55 10061-02-64.5
Diisopropyl ether ND ug/kg 1 07/07/09 12:55 108-20-34.5
Ethylbenzene ND ug/kg 1 07/07/09 12:55 100-41-44.5
Hexachloro-1,3-butadiene ND ug/kg 1 07/07/09 12:55 87-68-34.5
2-Hexanone ND ug/kg 1 07/07/09 12:55 591-78-645.3
Isopropylbenzene (Cumene)ND ug/kg 1 07/07/09 12:55 98-82-84.5
p-Isopropyltoluene ND ug/kg 1 07/07/09 12:55 99-87-64.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 19 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB5-06-09 Lab ID:9247665008 Collected:06/30/09 12:50 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Methylene Chloride ND ug/kg 1 07/07/09 12:55 75-09-218.1
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/07/09 12:55 108-10-145.3
Methyl-tert-butyl ether ND ug/kg 1 07/07/09 12:55 1634-04-44.5
Naphthalene ND ug/kg 1 07/07/09 12:55 91-20-34.5
n-Propylbenzene ND ug/kg 1 07/07/09 12:55 103-65-14.5
Styrene ND ug/kg 1 07/07/09 12:55 100-42-54.5
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/07/09 12:55 630-20-64.5
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/07/09 12:55 79-34-54.5
Tetrachloroethene ND ug/kg 1 07/07/09 12:55 127-18-44.5
Toluene ND ug/kg 1 07/07/09 12:55 108-88-34.5
1,2,3-Trichlorobenzene ND ug/kg 1 07/07/09 12:55 87-61-64.5
1,2,4-Trichlorobenzene ND ug/kg 1 07/07/09 12:55 120-82-14.5
1,1,1-Trichloroethane ND ug/kg 1 07/07/09 12:55 71-55-64.5
1,1,2-Trichloroethane ND ug/kg 1 07/07/09 12:55 79-00-54.5
Trichloroethene ND ug/kg 1 07/07/09 12:55 79-01-64.5
Trichlorofluoromethane ND ug/kg 1 07/07/09 12:55 75-69-44.5
1,2,3-Trichloropropane ND ug/kg 1 07/07/09 12:55 96-18-44.5
1,2,4-Trimethylbenzene ND ug/kg 1 07/07/09 12:55 95-63-64.5
1,3,5-Trimethylbenzene ND ug/kg 1 07/07/09 12:55 108-67-84.5
Vinyl acetate ND ug/kg 1 07/07/09 12:55 108-05-445.3
Vinyl chloride ND ug/kg 1 07/07/09 12:55 75-01-49.1
Xylene (Total)ND ug/kg 1 07/07/09 12:55 1330-20-79.1
m&p-Xylene ND ug/kg 1 07/07/09 12:55 1330-20-79.1
o-Xylene ND ug/kg 1 07/07/09 12:55 95-47-64.5
Dibromofluoromethane (S)105 %1 07/07/09 12:55 1868-53-779-116
Toluene-d8 (S)100 %1 07/07/09 12:55 2037-26-588-110
4-Bromofluorobenzene (S)97 %1 07/07/09 12:55 460-00-474-115
1,2-Dichloroethane-d4 (S)102 %1 07/07/09 12:55 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 7.3 %1 07/06/09 08:370.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 20 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB3-06-09 Lab ID:9247665009 Collected:06/30/09 13:00 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
9071 Oil and Grease Analytical Method: 9071B ASE Preparation Method: 9071B ASE
Oil and Grease 6920 mg/kg 1 07/09/09 14:3307/09/09 13:1082.9
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 15.6 %1 07/06/09 08:370.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 21 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB2-06-09 Lab ID:9247665010 Collected:06/30/09 13:15 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 2.7 mg/kg 1 07/07/09 18:19 7440-36-007/06/09 15:100.52
Arsenic 5.3 mg/kg 1 07/07/09 18:19 7440-38-207/06/09 15:100.52
Beryllium 0.17 mg/kg 1 07/07/09 18:19 7440-41-707/06/09 15:100.10
Cadmium 2.3 mg/kg 1 07/07/09 18:19 7440-43-907/06/09 15:100.10
Chromium 16.1 mg/kg 1 07/07/09 18:19 7440-47-307/06/09 15:100.52
Copper 31.9 mg/kg 1 07/07/09 18:19 7440-50-807/06/09 15:100.52
Lead 126 mg/kg 1 07/07/09 18:19 7439-92-107/06/09 15:100.52
Manganese 239 mg/kg 1 07/07/09 18:19 7439-96-507/06/09 15:100.52
Nickel 13.9 mg/kg 1 07/07/09 18:19 7440-02-007/06/09 15:100.52
Selenium ND mg/kg 1 07/07/09 18:19 7782-49-207/06/09 15:101.0
Silver ND mg/kg 1 07/07/09 18:19 7440-22-407/06/09 15:100.52
Thallium ND mg/kg 1 07/07/09 18:19 7440-28-007/06/09 15:101.0
Zinc 378 mg/kg 1 07/07/09 18:19 7440-66-607/06/09 15:101.0
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.14 mg/kg 5 07/13/09 14:01 7439-97-607/13/09 10:440.027
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 5.7 %1 07/08/09 13:550.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 22 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB1-06-09 Lab ID:9247665011 Collected:06/30/09 13:25 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 1.5 mg/kg 1 07/07/09 18:23 7440-36-007/06/09 15:100.46
Arsenic 0.57 mg/kg 1 07/07/09 18:23 7440-38-207/06/09 15:100.46
Beryllium ND mg/kg 1 07/07/09 18:23 7440-41-707/06/09 15:100.091
Cadmium 0.14 mg/kg 1 07/07/09 18:23 7440-43-907/06/09 15:100.091
Chromium 9.6 mg/kg 1 07/07/09 18:23 7440-47-307/06/09 15:100.46
Copper 10.7 mg/kg 1 07/07/09 18:23 7440-50-807/06/09 15:100.46
Lead 61.5 mg/kg 1 07/07/09 18:23 7439-92-107/06/09 15:100.46
Manganese 151 mg/kg 1 07/07/09 18:23 7439-96-507/06/09 15:100.46
Nickel 4.4 mg/kg 1 07/07/09 18:23 7440-02-007/06/09 15:100.46
Selenium ND mg/kg 1 07/07/09 18:23 7782-49-207/06/09 15:100.91
Silver ND mg/kg 1 07/07/09 18:23 7440-22-407/06/09 15:100.46
Thallium ND mg/kg 1 07/07/09 18:23 7440-28-007/06/09 15:100.91
Zinc 145 mg/kg 1 07/07/09 18:23 7440-66-607/06/09 15:100.91
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.035 mg/kg 1 07/13/09 12:51 7439-97-607/13/09 10:440.0046
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 7.1 %1 07/08/09 13:550.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 23 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB19-06-09 Lab ID:9247665012 Collected:06/30/09 13:40 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 39.1 mg/kg 1 07/14/09 14:41 68334-30-507/09/09 15:308.1
n-Pentacosane (S)111 %1 07/14/09 14:41 629-99-207/09/09 15:3050-135
9071 Oil and Grease Analytical Method: 9071B ASE Preparation Method: 9071B ASE
Oil and Grease 847 mg/kg 1 07/09/09 14:3307/09/09 13:1076.0
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/14/09 03:01 8006-61-907/02/09 11:147.6
4-Bromofluorobenzene (S)83 %1 07/14/09 03:01 460-00-407/02/09 11:1450-135
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 1.5 mg/kg 1 07/07/09 18:37 7440-36-007/06/09 15:100.50
Arsenic 0.51 mg/kg 1 07/07/09 18:37 7440-38-207/06/09 15:100.50
Beryllium 0.22 mg/kg 1 07/07/09 18:37 7440-41-707/06/09 15:100.10
Cadmium 1.2 mg/kg 1 07/07/09 18:37 7440-43-9 R107/06/09 15:100.10
Chromium 18.7 mg/kg 1 07/07/09 18:37 7440-47-307/06/09 15:100.50
Copper 21.7 mg/kg 1 07/07/09 18:37 7440-50-807/06/09 15:100.50
Lead 101 mg/kg 1 07/07/09 18:37 7439-92-1 M007/06/09 15:100.50
Manganese 237 mg/kg 1 07/07/09 18:37 7439-96-5 R107/06/09 15:100.50
Nickel 8.8 mg/kg 1 07/07/09 18:37 7440-02-007/06/09 15:100.50
Selenium ND mg/kg 1 07/07/09 18:37 7782-49-207/06/09 15:101.0
Silver ND mg/kg 1 07/07/09 18:37 7440-22-407/06/09 15:100.50
Thallium ND mg/kg 1 07/07/09 18:37 7440-28-0 M007/06/09 15:101.0
Zinc 78.5 mg/kg 1 07/07/09 18:37 7440-66-607/06/09 15:101.0
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.040 mg/kg 1 07/13/09 12:54 7439-97-6 M007/13/09 10:440.0054
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/10/09 20:53 83-32-907/09/09 10:15358
Acenaphthylene ND ug/kg 1 07/10/09 20:53 208-96-807/09/09 10:15358
Aniline ND ug/kg 1 07/10/09 20:53 62-53-307/09/09 10:15358
Anthracene ND ug/kg 1 07/10/09 20:53 120-12-707/09/09 10:15358
Benzo(a)anthracene ND ug/kg 1 07/10/09 20:53 56-55-307/09/09 10:15358
Benzo(a)pyrene ND ug/kg 1 07/10/09 20:53 50-32-807/09/09 10:15358
Benzo(b)fluoranthene ND ug/kg 1 07/10/09 20:53 205-99-207/09/09 10:15358
Benzo(g,h,i)perylene ND ug/kg 1 07/10/09 20:53 191-24-207/09/09 10:15358
Benzo(k)fluoranthene ND ug/kg 1 07/10/09 20:53 207-08-907/09/09 10:15358
Benzoic Acid ND ug/kg 1 07/10/09 20:53 65-85-007/09/09 10:151790
Benzyl alcohol ND ug/kg 1 07/10/09 20:53 100-51-607/09/09 10:15716
4-Bromophenylphenyl ether ND ug/kg 1 07/10/09 20:53 101-55-307/09/09 10:15358
Butylbenzylphthalate ND ug/kg 1 07/10/09 20:53 85-68-707/09/09 10:15358
4-Chloro-3-methylphenol ND ug/kg 1 07/10/09 20:53 59-50-707/09/09 10:15716
4-Chloroaniline ND ug/kg 1 07/10/09 20:53 106-47-807/09/09 10:151790
bis(2-Chloroethoxy)methane ND ug/kg 1 07/10/09 20:53 111-91-107/09/09 10:15358
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 24 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB19-06-09 Lab ID:9247665012 Collected:06/30/09 13:40 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
bis(2-Chloroethyl) ether ND ug/kg 1 07/10/09 20:53 111-44-407/09/09 10:15358
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/10/09 20:53 108-60-107/09/09 10:15358
2-Chloronaphthalene ND ug/kg 1 07/10/09 20:53 91-58-707/09/09 10:15358
2-Chlorophenol ND ug/kg 1 07/10/09 20:53 95-57-807/09/09 10:15358
4-Chlorophenylphenyl ether ND ug/kg 1 07/10/09 20:53 7005-72-307/09/09 10:15358
Chrysene ND ug/kg 1 07/10/09 20:53 218-01-907/09/09 10:15358
Dibenz(a,h)anthracene ND ug/kg 1 07/10/09 20:53 53-70-307/09/09 10:15358
Dibenzofuran ND ug/kg 1 07/10/09 20:53 132-64-907/09/09 10:15358
1,2-Dichlorobenzene ND ug/kg 1 07/10/09 20:53 95-50-107/09/09 10:15358
1,3-Dichlorobenzene ND ug/kg 1 07/10/09 20:53 541-73-107/09/09 10:15358
1,4-Dichlorobenzene ND ug/kg 1 07/10/09 20:53 106-46-707/09/09 10:15358
3,3'-Dichlorobenzidine ND ug/kg 1 07/10/09 20:53 91-94-107/09/09 10:151790
2,4-Dichlorophenol ND ug/kg 1 07/10/09 20:53 120-83-207/09/09 10:15358
Diethylphthalate ND ug/kg 1 07/10/09 20:53 84-66-207/09/09 10:15358
2,4-Dimethylphenol ND ug/kg 1 07/10/09 20:53 105-67-907/09/09 10:15358
Dimethylphthalate ND ug/kg 1 07/10/09 20:53 131-11-307/09/09 10:15358
Di-n-butylphthalate ND ug/kg 1 07/10/09 20:53 84-74-207/09/09 10:15358
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/10/09 20:53 534-52-107/09/09 10:15716
2,4-Dinitrophenol ND ug/kg 1 07/10/09 20:53 51-28-507/09/09 10:151790
2,4-Dinitrotoluene ND ug/kg 1 07/10/09 20:53 121-14-207/09/09 10:15358
2,6-Dinitrotoluene ND ug/kg 1 07/10/09 20:53 606-20-207/09/09 10:15358
Di-n-octylphthalate ND ug/kg 1 07/10/09 20:53 117-84-007/09/09 10:15358
1,2-Diphenylhydrazine ND ug/kg 1 07/10/09 20:53 122-66-707/09/09 10:15358
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/10/09 20:53 117-81-707/09/09 10:15358
Fluoranthene ND ug/kg 1 07/10/09 20:53 206-44-007/09/09 10:15358
Fluorene ND ug/kg 1 07/10/09 20:53 86-73-707/09/09 10:15358
Hexachloro-1,3-butadiene ND ug/kg 1 07/10/09 20:53 87-68-307/09/09 10:15358
Hexachlorobenzene ND ug/kg 1 07/10/09 20:53 118-74-107/09/09 10:15358
Hexachlorocyclopentadiene ND ug/kg 1 07/10/09 20:53 77-47-407/09/09 10:15358
Hexachloroethane ND ug/kg 1 07/10/09 20:53 67-72-107/09/09 10:15358
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/10/09 20:53 193-39-507/09/09 10:15358
Isophorone ND ug/kg 1 07/10/09 20:53 78-59-107/09/09 10:15358
1-Methylnaphthalene ND ug/kg 1 07/10/09 20:53 90-12-007/09/09 10:15358
2-Methylnaphthalene ND ug/kg 1 07/10/09 20:53 91-57-607/09/09 10:15358
2-Methylphenol(o-Cresol)ND ug/kg 1 07/10/09 20:53 95-48-707/09/09 10:15358
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/10/09 20:5307/09/09 10:15358
Naphthalene ND ug/kg 1 07/10/09 20:53 91-20-307/09/09 10:15358
2-Nitroaniline ND ug/kg 1 07/10/09 20:53 88-74-407/09/09 10:151790
3-Nitroaniline ND ug/kg 1 07/10/09 20:53 99-09-207/09/09 10:151790
4-Nitroaniline ND ug/kg 1 07/10/09 20:53 100-01-607/09/09 10:15716
Nitrobenzene ND ug/kg 1 07/10/09 20:53 98-95-307/09/09 10:15358
2-Nitrophenol ND ug/kg 1 07/10/09 20:53 88-75-507/09/09 10:15358
4-Nitrophenol ND ug/kg 1 07/10/09 20:53 100-02-707/09/09 10:151790
N-Nitrosodimethylamine ND ug/kg 1 07/10/09 20:53 62-75-907/09/09 10:15358
N-Nitroso-di-n-propylamine ND ug/kg 1 07/10/09 20:53 621-64-707/09/09 10:15358
N-Nitrosodiphenylamine ND ug/kg 1 07/10/09 20:53 86-30-607/09/09 10:15358
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 25 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB19-06-09 Lab ID:9247665012 Collected:06/30/09 13:40 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Pentachlorophenol ND ug/kg 1 07/10/09 20:53 87-86-507/09/09 10:151790
Phenanthrene ND ug/kg 1 07/10/09 20:53 85-01-807/09/09 10:15358
Phenol ND ug/kg 1 07/10/09 20:53 108-95-207/09/09 10:15358
Pyrene ND ug/kg 1 07/10/09 20:53 129-00-007/09/09 10:15358
1,2,4-Trichlorobenzene ND ug/kg 1 07/10/09 20:53 120-82-107/09/09 10:15358
2,4,5-Trichlorophenol ND ug/kg 1 07/10/09 20:53 95-95-407/09/09 10:15358
2,4,6-Trichlorophenol ND ug/kg 1 07/10/09 20:53 88-06-207/09/09 10:15358
Nitrobenzene-d5 (S)59 %1 07/10/09 20:53 4165-60-007/09/09 10:1530-150
2-Fluorobiphenyl (S)74 %1 07/10/09 20:53 321-60-807/09/09 10:1546-120
Terphenyl-d14 (S)120 %1 07/10/09 20:53 1718-51-007/09/09 10:1538-108
Phenol-d6 (S)60 %1 07/10/09 20:53 13127-88-307/09/09 10:1535-120
2-Fluorophenol (S)63 %1 07/10/09 20:53 367-12-407/09/09 10:1524-120
2,4,6-Tribromophenol (S)63 %1 07/10/09 20:53 118-79-607/09/09 10:1544-136
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/06/09 17:53 67-64-179.2
Benzene ND ug/kg 1 07/06/09 17:53 71-43-24.0
Bromobenzene ND ug/kg 1 07/06/09 17:53 108-86-14.0
Bromochloromethane ND ug/kg 1 07/06/09 17:53 74-97-54.0
Bromodichloromethane ND ug/kg 1 07/06/09 17:53 75-27-44.0
Bromoform ND ug/kg 1 07/06/09 17:53 75-25-24.0
Bromomethane ND ug/kg 1 07/06/09 17:53 74-83-97.9
2-Butanone (MEK)ND ug/kg 1 07/06/09 17:53 78-93-379.2
n-Butylbenzene ND ug/kg 1 07/06/09 17:53 104-51-84.0
sec-Butylbenzene ND ug/kg 1 07/06/09 17:53 135-98-84.0
tert-Butylbenzene ND ug/kg 1 07/06/09 17:53 98-06-64.0
Carbon tetrachloride ND ug/kg 1 07/06/09 17:53 56-23-54.0
Chlorobenzene ND ug/kg 1 07/06/09 17:53 108-90-74.0
Chloroethane ND ug/kg 1 07/06/09 17:53 75-00-37.9
Chloroform ND ug/kg 1 07/06/09 17:53 67-66-34.0
Chloromethane ND ug/kg 1 07/06/09 17:53 74-87-37.9
2-Chlorotoluene ND ug/kg 1 07/06/09 17:53 95-49-84.0
4-Chlorotoluene ND ug/kg 1 07/06/09 17:53 106-43-44.0
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/06/09 17:53 96-12-84.0
Dibromochloromethane ND ug/kg 1 07/06/09 17:53 124-48-14.0
1,2-Dibromoethane (EDB)ND ug/kg 1 07/06/09 17:53 106-93-44.0
Dibromomethane ND ug/kg 1 07/06/09 17:53 74-95-34.0
1,2-Dichlorobenzene ND ug/kg 1 07/06/09 17:53 95-50-14.0
1,3-Dichlorobenzene ND ug/kg 1 07/06/09 17:53 541-73-14.0
1,4-Dichlorobenzene ND ug/kg 1 07/06/09 17:53 106-46-74.0
Dichlorodifluoromethane ND ug/kg 1 07/06/09 17:53 75-71-87.9
1,1-Dichloroethane ND ug/kg 1 07/06/09 17:53 75-34-34.0
1,2-Dichloroethane ND ug/kg 1 07/06/09 17:53 107-06-24.0
1,1-Dichloroethene ND ug/kg 1 07/06/09 17:53 75-35-44.0
cis-1,2-Dichloroethene ND ug/kg 1 07/06/09 17:53 156-59-24.0
trans-1,2-Dichloroethene ND ug/kg 1 07/06/09 17:53 156-60-54.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 26 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB19-06-09 Lab ID:9247665012 Collected:06/30/09 13:40 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dichloropropane ND ug/kg 1 07/06/09 17:53 78-87-54.0
1,3-Dichloropropane ND ug/kg 1 07/06/09 17:53 142-28-94.0
2,2-Dichloropropane ND ug/kg 1 07/06/09 17:53 594-20-74.0
1,1-Dichloropropene ND ug/kg 1 07/06/09 17:53 563-58-64.0
cis-1,3-Dichloropropene ND ug/kg 1 07/06/09 17:53 10061-01-54.0
trans-1,3-Dichloropropene ND ug/kg 1 07/06/09 17:53 10061-02-64.0
Diisopropyl ether ND ug/kg 1 07/06/09 17:53 108-20-34.0
Ethylbenzene ND ug/kg 1 07/06/09 17:53 100-41-44.0
Hexachloro-1,3-butadiene ND ug/kg 1 07/06/09 17:53 87-68-34.0
2-Hexanone ND ug/kg 1 07/06/09 17:53 591-78-639.6
Isopropylbenzene (Cumene)ND ug/kg 1 07/06/09 17:53 98-82-84.0
p-Isopropyltoluene ND ug/kg 1 07/06/09 17:53 99-87-64.0
Methylene Chloride ND ug/kg 1 07/06/09 17:53 75-09-215.8
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/06/09 17:53 108-10-139.6
Methyl-tert-butyl ether ND ug/kg 1 07/06/09 17:53 1634-04-44.0
Naphthalene ND ug/kg 1 07/06/09 17:53 91-20-34.0
n-Propylbenzene ND ug/kg 1 07/06/09 17:53 103-65-14.0
Styrene ND ug/kg 1 07/06/09 17:53 100-42-54.0
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/06/09 17:53 630-20-64.0
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/06/09 17:53 79-34-54.0
Tetrachloroethene ND ug/kg 1 07/06/09 17:53 127-18-44.0
Toluene ND ug/kg 1 07/06/09 17:53 108-88-34.0
1,2,3-Trichlorobenzene ND ug/kg 1 07/06/09 17:53 87-61-64.0
1,2,4-Trichlorobenzene ND ug/kg 1 07/06/09 17:53 120-82-14.0
1,1,1-Trichloroethane ND ug/kg 1 07/06/09 17:53 71-55-64.0
1,1,2-Trichloroethane ND ug/kg 1 07/06/09 17:53 79-00-54.0
Trichloroethene ND ug/kg 1 07/06/09 17:53 79-01-64.0
Trichlorofluoromethane ND ug/kg 1 07/06/09 17:53 75-69-44.0
1,2,3-Trichloropropane ND ug/kg 1 07/06/09 17:53 96-18-44.0
1,2,4-Trimethylbenzene ND ug/kg 1 07/06/09 17:53 95-63-64.0
1,3,5-Trimethylbenzene ND ug/kg 1 07/06/09 17:53 108-67-84.0
Vinyl acetate ND ug/kg 1 07/06/09 17:53 108-05-439.6
Vinyl chloride ND ug/kg 1 07/06/09 17:53 75-01-47.9
Xylene (Total)ND ug/kg 1 07/06/09 17:53 1330-20-77.9
m&p-Xylene ND ug/kg 1 07/06/09 17:53 1330-20-77.9
o-Xylene ND ug/kg 1 07/06/09 17:53 95-47-64.0
Dibromofluoromethane (S)104 %1 07/06/09 17:53 1868-53-779-116
Toluene-d8 (S)98 %1 07/06/09 17:53 2037-26-588-110
4-Bromofluorobenzene (S)96 %1 07/06/09 17:53 460-00-474-115
1,2-Dichloroethane-d4 (S)103 %1 07/06/09 17:53 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 7.9 %1 07/06/09 08:380.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 27 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-DUPLICATE 1 06-09 Lab ID:9247665013 Collected:06/30/09 00:00 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 35.0 mg/kg 1 07/14/09 15:10 68334-30-507/09/09 15:305.5
n-Pentacosane (S)91 %1 07/14/09 15:10 629-99-207/09/09 15:3050-135
9071 Oil and Grease Analytical Method: 9071B ASE Preparation Method: 9071B ASE
Oil and Grease 490 mg/kg 1 07/09/09 14:3507/09/09 13:1077.3
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/02/09 21:23 8006-61-907/02/09 15:066.3
4-Bromofluorobenzene (S)84 %1 07/02/09 21:23 460-00-407/02/09 15:0650-135
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 1.5 mg/kg 1 07/07/09 18:51 7440-36-007/06/09 15:100.44
Arsenic ND mg/kg 1 07/07/09 18:51 7440-38-207/06/09 15:100.44
Beryllium 0.17 mg/kg 1 07/07/09 18:51 7440-41-707/06/09 15:100.088
Cadmium 1.1 mg/kg 1 07/07/09 18:51 7440-43-907/06/09 15:100.088
Chromium 19.6 mg/kg 1 07/07/09 18:51 7440-47-307/06/09 15:100.44
Copper 19.3 mg/kg 1 07/07/09 18:51 7440-50-807/06/09 15:100.44
Lead 39.4 mg/kg 1 07/07/09 18:51 7439-92-107/06/09 15:100.44
Manganese 222 mg/kg 1 07/07/09 18:51 7439-96-507/06/09 15:100.44
Nickel 8.2 mg/kg 1 07/07/09 18:51 7440-02-007/06/09 15:100.44
Selenium 1.6 mg/kg 1 07/07/09 18:51 7782-49-207/06/09 15:100.88
Silver ND mg/kg 1 07/07/09 18:51 7440-22-407/06/09 15:100.44
Thallium ND mg/kg 1 07/07/09 18:51 7440-28-007/06/09 15:100.88
Zinc 64.4 mg/kg 1 07/07/09 18:51 7440-66-607/06/09 15:100.88
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.0084 mg/kg 1 07/13/09 13:03 7439-97-607/13/09 10:440.0055
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/12/09 01:46 83-32-907/01/09 14:30365
Acenaphthylene ND ug/kg 1 07/12/09 01:46 208-96-807/01/09 14:30365
Aniline ND ug/kg 1 07/12/09 01:46 62-53-307/01/09 14:30365
Anthracene ND ug/kg 1 07/12/09 01:46 120-12-707/01/09 14:30365
Benzo(a)anthracene ND ug/kg 1 07/12/09 01:46 56-55-307/01/09 14:30365
Benzo(a)pyrene ND ug/kg 1 07/12/09 01:46 50-32-807/01/09 14:30365
Benzo(b)fluoranthene ND ug/kg 1 07/12/09 01:46 205-99-207/01/09 14:30365
Benzo(g,h,i)perylene ND ug/kg 1 07/12/09 01:46 191-24-207/01/09 14:30365
Benzo(k)fluoranthene ND ug/kg 1 07/12/09 01:46 207-08-907/01/09 14:30365
Benzoic Acid ND ug/kg 1 07/12/09 01:46 65-85-007/01/09 14:301820
Benzyl alcohol ND ug/kg 1 07/12/09 01:46 100-51-607/01/09 14:30729
4-Bromophenylphenyl ether ND ug/kg 1 07/12/09 01:46 101-55-307/01/09 14:30365
Butylbenzylphthalate ND ug/kg 1 07/12/09 01:46 85-68-707/01/09 14:30365
4-Chloro-3-methylphenol ND ug/kg 1 07/12/09 01:46 59-50-707/01/09 14:30729
4-Chloroaniline ND ug/kg 1 07/12/09 01:46 106-47-807/01/09 14:301820
bis(2-Chloroethoxy)methane ND ug/kg 1 07/12/09 01:46 111-91-107/01/09 14:30365
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 28 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-DUPLICATE 1 06-09 Lab ID:9247665013 Collected:06/30/09 00:00 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
bis(2-Chloroethyl) ether ND ug/kg 1 07/12/09 01:46 111-44-407/01/09 14:30365
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/12/09 01:46 108-60-107/01/09 14:30365
2-Chloronaphthalene ND ug/kg 1 07/12/09 01:46 91-58-707/01/09 14:30365
2-Chlorophenol ND ug/kg 1 07/12/09 01:46 95-57-807/01/09 14:30365
4-Chlorophenylphenyl ether ND ug/kg 1 07/12/09 01:46 7005-72-307/01/09 14:30365
Chrysene ND ug/kg 1 07/12/09 01:46 218-01-907/01/09 14:30365
Dibenz(a,h)anthracene ND ug/kg 1 07/12/09 01:46 53-70-307/01/09 14:30365
Dibenzofuran ND ug/kg 1 07/12/09 01:46 132-64-907/01/09 14:30365
1,2-Dichlorobenzene ND ug/kg 1 07/12/09 01:46 95-50-107/01/09 14:30365
1,3-Dichlorobenzene ND ug/kg 1 07/12/09 01:46 541-73-107/01/09 14:30365
1,4-Dichlorobenzene ND ug/kg 1 07/12/09 01:46 106-46-707/01/09 14:30365
3,3'-Dichlorobenzidine ND ug/kg 1 07/12/09 01:46 91-94-107/01/09 14:301820
2,4-Dichlorophenol ND ug/kg 1 07/12/09 01:46 120-83-207/01/09 14:30365
Diethylphthalate ND ug/kg 1 07/12/09 01:46 84-66-207/01/09 14:30365
2,4-Dimethylphenol ND ug/kg 1 07/12/09 01:46 105-67-907/01/09 14:30365
Dimethylphthalate ND ug/kg 1 07/12/09 01:46 131-11-307/01/09 14:30365
Di-n-butylphthalate ND ug/kg 1 07/12/09 01:46 84-74-207/01/09 14:30365
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/12/09 01:46 534-52-107/01/09 14:30729
2,4-Dinitrophenol ND ug/kg 1 07/12/09 01:46 51-28-507/01/09 14:301820
2,4-Dinitrotoluene ND ug/kg 1 07/12/09 01:46 121-14-207/01/09 14:30365
2,6-Dinitrotoluene ND ug/kg 1 07/12/09 01:46 606-20-207/01/09 14:30365
Di-n-octylphthalate ND ug/kg 1 07/12/09 01:46 117-84-007/01/09 14:30365
1,2-Diphenylhydrazine ND ug/kg 1 07/12/09 01:46 122-66-707/01/09 14:30365
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/12/09 01:46 117-81-707/01/09 14:30365
Fluoranthene ND ug/kg 1 07/12/09 01:46 206-44-007/01/09 14:30365
Fluorene ND ug/kg 1 07/12/09 01:46 86-73-707/01/09 14:30365
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/09 01:46 87-68-307/01/09 14:30365
Hexachlorobenzene ND ug/kg 1 07/12/09 01:46 118-74-107/01/09 14:30365
Hexachlorocyclopentadiene ND ug/kg 1 07/12/09 01:46 77-47-407/01/09 14:30365
Hexachloroethane ND ug/kg 1 07/12/09 01:46 67-72-107/01/09 14:30365
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/12/09 01:46 193-39-507/01/09 14:30365
Isophorone ND ug/kg 1 07/12/09 01:46 78-59-107/01/09 14:30365
1-Methylnaphthalene ND ug/kg 1 07/12/09 01:46 90-12-007/01/09 14:30365
2-Methylnaphthalene ND ug/kg 1 07/12/09 01:46 91-57-607/01/09 14:30365
2-Methylphenol(o-Cresol)ND ug/kg 1 07/12/09 01:46 95-48-707/01/09 14:30365
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/12/09 01:4607/01/09 14:30365
Naphthalene ND ug/kg 1 07/12/09 01:46 91-20-307/01/09 14:30365
2-Nitroaniline ND ug/kg 1 07/12/09 01:46 88-74-407/01/09 14:301820
3-Nitroaniline ND ug/kg 1 07/12/09 01:46 99-09-207/01/09 14:301820
4-Nitroaniline ND ug/kg 1 07/12/09 01:46 100-01-607/01/09 14:30729
Nitrobenzene ND ug/kg 1 07/12/09 01:46 98-95-307/01/09 14:30365
2-Nitrophenol ND ug/kg 1 07/12/09 01:46 88-75-507/01/09 14:30365
4-Nitrophenol ND ug/kg 1 07/12/09 01:46 100-02-707/01/09 14:301820
N-Nitrosodimethylamine ND ug/kg 1 07/12/09 01:46 62-75-907/01/09 14:30365
N-Nitroso-di-n-propylamine ND ug/kg 1 07/12/09 01:46 621-64-707/01/09 14:30365
N-Nitrosodiphenylamine ND ug/kg 1 07/12/09 01:46 86-30-607/01/09 14:30365
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 29 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-DUPLICATE 1 06-09 Lab ID:9247665013 Collected:06/30/09 00:00 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Pentachlorophenol ND ug/kg 1 07/12/09 01:46 87-86-507/01/09 14:301820
Phenanthrene ND ug/kg 1 07/12/09 01:46 85-01-807/01/09 14:30365
Phenol ND ug/kg 1 07/12/09 01:46 108-95-207/01/09 14:30365
Pyrene ND ug/kg 1 07/12/09 01:46 129-00-007/01/09 14:30365
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/09 01:46 120-82-107/01/09 14:30365
2,4,5-Trichlorophenol ND ug/kg 1 07/12/09 01:46 95-95-407/01/09 14:30365
2,4,6-Trichlorophenol ND ug/kg 1 07/12/09 01:46 88-06-207/01/09 14:30365
Nitrobenzene-d5 (S)69 %1 07/12/09 01:46 4165-60-007/01/09 14:3030-150
2-Fluorobiphenyl (S)78 %1 07/12/09 01:46 321-60-807/01/09 14:3046-120
Terphenyl-d14 (S)146 %1 07/12/09 01:46 1718-51-0 2g07/01/09 14:3038-108
Phenol-d6 (S)44 %1 07/12/09 01:46 13127-88-307/01/09 14:3035-120
2-Fluorophenol (S)37 %1 07/12/09 01:46 367-12-407/01/09 14:3024-120
2,4,6-Tribromophenol (S)58 %1 07/12/09 01:46 118-79-607/01/09 14:3044-136
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 113 ug/kg 1 07/06/09 18:12 67-64-1 C9101
Benzene ND ug/kg 1 07/06/09 18:12 71-43-25.0
Bromobenzene ND ug/kg 1 07/06/09 18:12 108-86-15.0
Bromochloromethane ND ug/kg 1 07/06/09 18:12 74-97-55.0
Bromodichloromethane ND ug/kg 1 07/06/09 18:12 75-27-45.0
Bromoform ND ug/kg 1 07/06/09 18:12 75-25-25.0
Bromomethane ND ug/kg 1 07/06/09 18:12 74-83-910.1
2-Butanone (MEK)ND ug/kg 1 07/06/09 18:12 78-93-3101
n-Butylbenzene ND ug/kg 1 07/06/09 18:12 104-51-85.0
sec-Butylbenzene ND ug/kg 1 07/06/09 18:12 135-98-85.0
tert-Butylbenzene ND ug/kg 1 07/06/09 18:12 98-06-65.0
Carbon tetrachloride ND ug/kg 1 07/06/09 18:12 56-23-55.0
Chlorobenzene ND ug/kg 1 07/06/09 18:12 108-90-75.0
Chloroethane ND ug/kg 1 07/06/09 18:12 75-00-310.1
Chloroform ND ug/kg 1 07/06/09 18:12 67-66-35.0
Chloromethane ND ug/kg 1 07/06/09 18:12 74-87-310.1
2-Chlorotoluene ND ug/kg 1 07/06/09 18:12 95-49-85.0
4-Chlorotoluene ND ug/kg 1 07/06/09 18:12 106-43-45.0
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/06/09 18:12 96-12-85.0
Dibromochloromethane ND ug/kg 1 07/06/09 18:12 124-48-15.0
1,2-Dibromoethane (EDB)ND ug/kg 1 07/06/09 18:12 106-93-45.0
Dibromomethane ND ug/kg 1 07/06/09 18:12 74-95-35.0
1,2-Dichlorobenzene ND ug/kg 1 07/06/09 18:12 95-50-15.0
1,3-Dichlorobenzene ND ug/kg 1 07/06/09 18:12 541-73-15.0
1,4-Dichlorobenzene ND ug/kg 1 07/06/09 18:12 106-46-75.0
Dichlorodifluoromethane ND ug/kg 1 07/06/09 18:12 75-71-810.1
1,1-Dichloroethane ND ug/kg 1 07/06/09 18:12 75-34-35.0
1,2-Dichloroethane ND ug/kg 1 07/06/09 18:12 107-06-25.0
1,1-Dichloroethene ND ug/kg 1 07/06/09 18:12 75-35-45.0
cis-1,2-Dichloroethene ND ug/kg 1 07/06/09 18:12 156-59-25.0
trans-1,2-Dichloroethene ND ug/kg 1 07/06/09 18:12 156-60-55.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 30 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-DUPLICATE 1 06-09 Lab ID:9247665013 Collected:06/30/09 00:00 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dichloropropane ND ug/kg 1 07/06/09 18:12 78-87-55.0
1,3-Dichloropropane ND ug/kg 1 07/06/09 18:12 142-28-95.0
2,2-Dichloropropane ND ug/kg 1 07/06/09 18:12 594-20-75.0
1,1-Dichloropropene ND ug/kg 1 07/06/09 18:12 563-58-65.0
cis-1,3-Dichloropropene ND ug/kg 1 07/06/09 18:12 10061-01-55.0
trans-1,3-Dichloropropene ND ug/kg 1 07/06/09 18:12 10061-02-65.0
Diisopropyl ether ND ug/kg 1 07/06/09 18:12 108-20-35.0
Ethylbenzene ND ug/kg 1 07/06/09 18:12 100-41-45.0
Hexachloro-1,3-butadiene ND ug/kg 1 07/06/09 18:12 87-68-35.0
2-Hexanone ND ug/kg 1 07/06/09 18:12 591-78-650.3
Isopropylbenzene (Cumene)ND ug/kg 1 07/06/09 18:12 98-82-85.0
p-Isopropyltoluene ND ug/kg 1 07/06/09 18:12 99-87-65.0
Methylene Chloride ND ug/kg 1 07/06/09 18:12 75-09-220.1
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/06/09 18:12 108-10-150.3
Methyl-tert-butyl ether ND ug/kg 1 07/06/09 18:12 1634-04-45.0
Naphthalene ND ug/kg 1 07/06/09 18:12 91-20-35.0
n-Propylbenzene ND ug/kg 1 07/06/09 18:12 103-65-15.0
Styrene ND ug/kg 1 07/06/09 18:12 100-42-55.0
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/06/09 18:12 630-20-65.0
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/06/09 18:12 79-34-55.0
Tetrachloroethene ND ug/kg 1 07/06/09 18:12 127-18-45.0
Toluene ND ug/kg 1 07/06/09 18:12 108-88-35.0
1,2,3-Trichlorobenzene ND ug/kg 1 07/06/09 18:12 87-61-65.0
1,2,4-Trichlorobenzene ND ug/kg 1 07/06/09 18:12 120-82-15.0
1,1,1-Trichloroethane ND ug/kg 1 07/06/09 18:12 71-55-65.0
1,1,2-Trichloroethane ND ug/kg 1 07/06/09 18:12 79-00-55.0
Trichloroethene ND ug/kg 1 07/06/09 18:12 79-01-65.0
Trichlorofluoromethane ND ug/kg 1 07/06/09 18:12 75-69-45.0
1,2,3-Trichloropropane ND ug/kg 1 07/06/09 18:12 96-18-45.0
1,2,4-Trimethylbenzene ND ug/kg 1 07/06/09 18:12 95-63-65.0
1,3,5-Trimethylbenzene ND ug/kg 1 07/06/09 18:12 108-67-85.0
Vinyl acetate ND ug/kg 1 07/06/09 18:12 108-05-450.3
Vinyl chloride ND ug/kg 1 07/06/09 18:12 75-01-410.1
Xylene (Total)ND ug/kg 1 07/06/09 18:12 1330-20-710.1
m&p-Xylene ND ug/kg 1 07/06/09 18:12 1330-20-710.1
o-Xylene ND ug/kg 1 07/06/09 18:12 95-47-65.0
Dibromofluoromethane (S)103 %1 07/06/09 18:12 1868-53-779-116
Toluene-d8 (S)98 %1 07/06/09 18:12 2037-26-588-110
4-Bromofluorobenzene (S)97 %1 07/06/09 18:12 460-00-474-115
1,2-Dichloroethane-d4 (S)100 %1 07/06/09 18:12 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 9.5 %1 07/06/09 08:380.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 31 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB20-06-09 Lab ID:9247665014 Collected:06/30/09 14:45 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components ND mg/kg 1 07/14/09 15:39 68334-30-507/09/09 15:305.3
n-Pentacosane (S)60 %1 07/14/09 15:39 629-99-207/09/09 15:3050-135
9071 Oil and Grease Analytical Method: 9071B ASE Preparation Method: 9071B ASE
Oil and Grease 103 mg/kg 1 07/09/09 14:3707/09/09 13:1074.5
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/02/09 21:46 8006-61-907/02/09 15:065.2
4-Bromofluorobenzene (S)96 %1 07/02/09 21:46 460-00-407/02/09 15:0650-135
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 8.6 mg/kg 1 07/08/09 22:45 7440-36-007/07/09 14:200.40
Arsenic 5.7 mg/kg 1 07/08/09 22:45 7440-38-207/07/09 14:200.40
Beryllium 0.66 mg/kg 1 07/08/09 22:45 7440-41-707/07/09 14:200.079
Cadmium 11.0 mg/kg 1 07/08/09 22:45 7440-43-907/07/09 14:200.079
Chromium 42.4 mg/kg 1 07/08/09 22:45 7440-47-307/07/09 14:200.40
Copper 596 mg/kg 1 07/08/09 22:45 7440-50-807/07/09 14:200.40
Lead 1220 mg/kg 5 07/09/09 16:08 7439-92-107/07/09 14:202.0
Manganese 464 mg/kg 1 07/08/09 22:45 7439-96-507/07/09 14:200.40
Nickel 25.7 mg/kg 1 07/08/09 22:45 7440-02-007/07/09 14:200.40
Selenium 1.9 mg/kg 1 07/08/09 22:45 7782-49-207/07/09 14:200.79
Silver ND mg/kg 1 07/08/09 22:45 7440-22-407/07/09 14:200.40
Thallium 0.91 mg/kg 1 07/08/09 22:45 7440-28-007/07/09 14:200.79
Zinc 2300 mg/kg 5 07/09/09 16:08 7440-66-607/07/09 14:204.0
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 1.0 mg/kg 50 07/13/09 14:04 7439-97-607/13/09 10:440.26
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/12/09 02:13 83-32-907/01/09 14:30351
Acenaphthylene ND ug/kg 1 07/12/09 02:13 208-96-807/01/09 14:30351
Aniline ND ug/kg 1 07/12/09 02:13 62-53-307/01/09 14:30351
Anthracene ND ug/kg 1 07/12/09 02:13 120-12-707/01/09 14:30351
Benzo(a)anthracene ND ug/kg 1 07/12/09 02:13 56-55-307/01/09 14:30351
Benzo(a)pyrene ND ug/kg 1 07/12/09 02:13 50-32-807/01/09 14:30351
Benzo(b)fluoranthene ND ug/kg 1 07/12/09 02:13 205-99-207/01/09 14:30351
Benzo(g,h,i)perylene ND ug/kg 1 07/12/09 02:13 191-24-207/01/09 14:30351
Benzo(k)fluoranthene ND ug/kg 1 07/12/09 02:13 207-08-907/01/09 14:30351
Benzoic Acid ND ug/kg 1 07/12/09 02:13 65-85-007/01/09 14:301760
Benzyl alcohol ND ug/kg 1 07/12/09 02:13 100-51-607/01/09 14:30703
4-Bromophenylphenyl ether ND ug/kg 1 07/12/09 02:13 101-55-307/01/09 14:30351
Butylbenzylphthalate ND ug/kg 1 07/12/09 02:13 85-68-707/01/09 14:30351
4-Chloro-3-methylphenol ND ug/kg 1 07/12/09 02:13 59-50-707/01/09 14:30703
4-Chloroaniline ND ug/kg 1 07/12/09 02:13 106-47-807/01/09 14:301760
bis(2-Chloroethoxy)methane ND ug/kg 1 07/12/09 02:13 111-91-107/01/09 14:30351
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 32 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB20-06-09 Lab ID:9247665014 Collected:06/30/09 14:45 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
bis(2-Chloroethyl) ether ND ug/kg 1 07/12/09 02:13 111-44-407/01/09 14:30351
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/12/09 02:13 108-60-107/01/09 14:30351
2-Chloronaphthalene ND ug/kg 1 07/12/09 02:13 91-58-707/01/09 14:30351
2-Chlorophenol ND ug/kg 1 07/12/09 02:13 95-57-807/01/09 14:30351
4-Chlorophenylphenyl ether ND ug/kg 1 07/12/09 02:13 7005-72-307/01/09 14:30351
Chrysene ND ug/kg 1 07/12/09 02:13 218-01-907/01/09 14:30351
Dibenz(a,h)anthracene ND ug/kg 1 07/12/09 02:13 53-70-307/01/09 14:30351
Dibenzofuran ND ug/kg 1 07/12/09 02:13 132-64-907/01/09 14:30351
1,2-Dichlorobenzene ND ug/kg 1 07/12/09 02:13 95-50-107/01/09 14:30351
1,3-Dichlorobenzene ND ug/kg 1 07/12/09 02:13 541-73-107/01/09 14:30351
1,4-Dichlorobenzene ND ug/kg 1 07/12/09 02:13 106-46-707/01/09 14:30351
3,3'-Dichlorobenzidine ND ug/kg 1 07/12/09 02:13 91-94-107/01/09 14:301760
2,4-Dichlorophenol ND ug/kg 1 07/12/09 02:13 120-83-207/01/09 14:30351
Diethylphthalate ND ug/kg 1 07/12/09 02:13 84-66-207/01/09 14:30351
2,4-Dimethylphenol ND ug/kg 1 07/12/09 02:13 105-67-907/01/09 14:30351
Dimethylphthalate ND ug/kg 1 07/12/09 02:13 131-11-307/01/09 14:30351
Di-n-butylphthalate ND ug/kg 1 07/12/09 02:13 84-74-207/01/09 14:30351
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/12/09 02:13 534-52-107/01/09 14:30703
2,4-Dinitrophenol ND ug/kg 1 07/12/09 02:13 51-28-507/01/09 14:301760
2,4-Dinitrotoluene ND ug/kg 1 07/12/09 02:13 121-14-207/01/09 14:30351
2,6-Dinitrotoluene ND ug/kg 1 07/12/09 02:13 606-20-207/01/09 14:30351
Di-n-octylphthalate ND ug/kg 1 07/12/09 02:13 117-84-007/01/09 14:30351
1,2-Diphenylhydrazine ND ug/kg 1 07/12/09 02:13 122-66-707/01/09 14:30351
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/12/09 02:13 117-81-707/01/09 14:30351
Fluoranthene ND ug/kg 1 07/12/09 02:13 206-44-007/01/09 14:30351
Fluorene ND ug/kg 1 07/12/09 02:13 86-73-707/01/09 14:30351
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/09 02:13 87-68-307/01/09 14:30351
Hexachlorobenzene ND ug/kg 1 07/12/09 02:13 118-74-107/01/09 14:30351
Hexachlorocyclopentadiene ND ug/kg 1 07/12/09 02:13 77-47-407/01/09 14:30351
Hexachloroethane ND ug/kg 1 07/12/09 02:13 67-72-107/01/09 14:30351
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/12/09 02:13 193-39-507/01/09 14:30351
Isophorone ND ug/kg 1 07/12/09 02:13 78-59-107/01/09 14:30351
1-Methylnaphthalene ND ug/kg 1 07/12/09 02:13 90-12-007/01/09 14:30351
2-Methylnaphthalene ND ug/kg 1 07/12/09 02:13 91-57-607/01/09 14:30351
2-Methylphenol(o-Cresol)ND ug/kg 1 07/12/09 02:13 95-48-707/01/09 14:30351
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/12/09 02:1307/01/09 14:30351
Naphthalene ND ug/kg 1 07/12/09 02:13 91-20-307/01/09 14:30351
2-Nitroaniline ND ug/kg 1 07/12/09 02:13 88-74-407/01/09 14:301760
3-Nitroaniline ND ug/kg 1 07/12/09 02:13 99-09-207/01/09 14:301760
4-Nitroaniline ND ug/kg 1 07/12/09 02:13 100-01-607/01/09 14:30703
Nitrobenzene ND ug/kg 1 07/12/09 02:13 98-95-307/01/09 14:30351
2-Nitrophenol ND ug/kg 1 07/12/09 02:13 88-75-507/01/09 14:30351
4-Nitrophenol ND ug/kg 1 07/12/09 02:13 100-02-707/01/09 14:301760
N-Nitrosodimethylamine ND ug/kg 1 07/12/09 02:13 62-75-907/01/09 14:30351
N-Nitroso-di-n-propylamine ND ug/kg 1 07/12/09 02:13 621-64-707/01/09 14:30351
N-Nitrosodiphenylamine ND ug/kg 1 07/12/09 02:13 86-30-607/01/09 14:30351
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 33 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB20-06-09 Lab ID:9247665014 Collected:06/30/09 14:45 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Pentachlorophenol ND ug/kg 1 07/12/09 02:13 87-86-507/01/09 14:301760
Phenanthrene ND ug/kg 1 07/12/09 02:13 85-01-807/01/09 14:30351
Phenol ND ug/kg 1 07/12/09 02:13 108-95-207/01/09 14:30351
Pyrene ND ug/kg 1 07/12/09 02:13 129-00-007/01/09 14:30351
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/09 02:13 120-82-107/01/09 14:30351
2,4,5-Trichlorophenol ND ug/kg 1 07/12/09 02:13 95-95-407/01/09 14:30351
2,4,6-Trichlorophenol ND ug/kg 1 07/12/09 02:13 88-06-207/01/09 14:30351
Nitrobenzene-d5 (S)66 %1 07/12/09 02:13 4165-60-007/01/09 14:3030-150
2-Fluorobiphenyl (S)79 %1 07/12/09 02:13 321-60-807/01/09 14:3046-120
Terphenyl-d14 (S)143 %1 07/12/09 02:13 1718-51-0 2g07/01/09 14:3038-108
Phenol-d6 (S)44 %1 07/12/09 02:13 13127-88-307/01/09 14:3035-120
2-Fluorophenol (S)34 %1 07/12/09 02:13 367-12-407/01/09 14:3024-120
2,4,6-Tribromophenol (S)49 %1 07/12/09 02:13 118-79-607/01/09 14:3044-136
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/06/09 18:30 67-64-192.7
Benzene ND ug/kg 1 07/06/09 18:30 71-43-24.6
Bromobenzene ND ug/kg 1 07/06/09 18:30 108-86-14.6
Bromochloromethane ND ug/kg 1 07/06/09 18:30 74-97-54.6
Bromodichloromethane ND ug/kg 1 07/06/09 18:30 75-27-44.6
Bromoform ND ug/kg 1 07/06/09 18:30 75-25-24.6
Bromomethane ND ug/kg 1 07/06/09 18:30 74-83-99.3
2-Butanone (MEK)ND ug/kg 1 07/06/09 18:30 78-93-392.7
n-Butylbenzene ND ug/kg 1 07/06/09 18:30 104-51-84.6
sec-Butylbenzene ND ug/kg 1 07/06/09 18:30 135-98-84.6
tert-Butylbenzene ND ug/kg 1 07/06/09 18:30 98-06-64.6
Carbon tetrachloride ND ug/kg 1 07/06/09 18:30 56-23-54.6
Chlorobenzene ND ug/kg 1 07/06/09 18:30 108-90-74.6
Chloroethane ND ug/kg 1 07/06/09 18:30 75-00-39.3
Chloroform ND ug/kg 1 07/06/09 18:30 67-66-34.6
Chloromethane ND ug/kg 1 07/06/09 18:30 74-87-39.3
2-Chlorotoluene ND ug/kg 1 07/06/09 18:30 95-49-84.6
4-Chlorotoluene ND ug/kg 1 07/06/09 18:30 106-43-44.6
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/06/09 18:30 96-12-84.6
Dibromochloromethane ND ug/kg 1 07/06/09 18:30 124-48-14.6
1,2-Dibromoethane (EDB)ND ug/kg 1 07/06/09 18:30 106-93-44.6
Dibromomethane ND ug/kg 1 07/06/09 18:30 74-95-34.6
1,2-Dichlorobenzene ND ug/kg 1 07/06/09 18:30 95-50-14.6
1,3-Dichlorobenzene ND ug/kg 1 07/06/09 18:30 541-73-14.6
1,4-Dichlorobenzene ND ug/kg 1 07/06/09 18:30 106-46-74.6
Dichlorodifluoromethane ND ug/kg 1 07/06/09 18:30 75-71-89.3
1,1-Dichloroethane ND ug/kg 1 07/06/09 18:30 75-34-34.6
1,2-Dichloroethane ND ug/kg 1 07/06/09 18:30 107-06-24.6
1,1-Dichloroethene ND ug/kg 1 07/06/09 18:30 75-35-44.6
cis-1,2-Dichloroethene ND ug/kg 1 07/06/09 18:30 156-59-24.6
trans-1,2-Dichloroethene ND ug/kg 1 07/06/09 18:30 156-60-54.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 34 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB20-06-09 Lab ID:9247665014 Collected:06/30/09 14:45 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dichloropropane ND ug/kg 1 07/06/09 18:30 78-87-54.6
1,3-Dichloropropane ND ug/kg 1 07/06/09 18:30 142-28-94.6
2,2-Dichloropropane ND ug/kg 1 07/06/09 18:30 594-20-74.6
1,1-Dichloropropene ND ug/kg 1 07/06/09 18:30 563-58-64.6
cis-1,3-Dichloropropene ND ug/kg 1 07/06/09 18:30 10061-01-54.6
trans-1,3-Dichloropropene ND ug/kg 1 07/06/09 18:30 10061-02-64.6
Diisopropyl ether ND ug/kg 1 07/06/09 18:30 108-20-34.6
Ethylbenzene ND ug/kg 1 07/06/09 18:30 100-41-44.6
Hexachloro-1,3-butadiene ND ug/kg 1 07/06/09 18:30 87-68-34.6
2-Hexanone ND ug/kg 1 07/06/09 18:30 591-78-646.4
Isopropylbenzene (Cumene)ND ug/kg 1 07/06/09 18:30 98-82-84.6
p-Isopropyltoluene ND ug/kg 1 07/06/09 18:30 99-87-64.6
Methylene Chloride ND ug/kg 1 07/06/09 18:30 75-09-218.5
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/06/09 18:30 108-10-146.4
Methyl-tert-butyl ether ND ug/kg 1 07/06/09 18:30 1634-04-44.6
Naphthalene ND ug/kg 1 07/06/09 18:30 91-20-34.6
n-Propylbenzene ND ug/kg 1 07/06/09 18:30 103-65-14.6
Styrene ND ug/kg 1 07/06/09 18:30 100-42-54.6
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/06/09 18:30 630-20-64.6
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/06/09 18:30 79-34-54.6
Tetrachloroethene ND ug/kg 1 07/06/09 18:30 127-18-44.6
Toluene ND ug/kg 1 07/06/09 18:30 108-88-34.6
1,2,3-Trichlorobenzene ND ug/kg 1 07/06/09 18:30 87-61-64.6
1,2,4-Trichlorobenzene ND ug/kg 1 07/06/09 18:30 120-82-14.6
1,1,1-Trichloroethane ND ug/kg 1 07/06/09 18:30 71-55-64.6
1,1,2-Trichloroethane ND ug/kg 1 07/06/09 18:30 79-00-54.6
Trichloroethene ND ug/kg 1 07/06/09 18:30 79-01-64.6
Trichlorofluoromethane ND ug/kg 1 07/06/09 18:30 75-69-44.6
1,2,3-Trichloropropane ND ug/kg 1 07/06/09 18:30 96-18-44.6
1,2,4-Trimethylbenzene ND ug/kg 1 07/06/09 18:30 95-63-64.6
1,3,5-Trimethylbenzene ND ug/kg 1 07/06/09 18:30 108-67-84.6
Vinyl acetate ND ug/kg 1 07/06/09 18:30 108-05-446.4
Vinyl chloride ND ug/kg 1 07/06/09 18:30 75-01-49.3
Xylene (Total)ND ug/kg 1 07/06/09 18:30 1330-20-79.3
m&p-Xylene ND ug/kg 1 07/06/09 18:30 1330-20-79.3
o-Xylene ND ug/kg 1 07/06/09 18:30 95-47-64.6
Dibromofluoromethane (S)103 %1 07/06/09 18:30 1868-53-779-116
Toluene-d8 (S)100 %1 07/06/09 18:30 2037-26-588-110
4-Bromofluorobenzene (S)103 %1 07/06/09 18:30 460-00-474-115
1,2-Dichloroethane-d4 (S)104 %1 07/06/09 18:30 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 6.1 %1 07/06/09 08:380.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 35 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB21-06-09 Lab ID:9247665015 Collected:06/30/09 15:00 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 12.1 mg/kg 1 07/14/09 15:39 68334-30-507/09/09 15:305.3
n-Pentacosane (S)70 %1 07/14/09 15:39 629-99-207/09/09 15:3050-135
9071 Oil and Grease Analytical Method: 9071B ASE Preparation Method: 9071B ASE
Oil and Grease 235 mg/kg 1 07/09/09 14:3707/09/09 13:1074.7
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/02/09 22:10 8006-61-907/02/09 15:0611.4
4-Bromofluorobenzene (S)88 %1 07/02/09 22:10 460-00-407/02/09 15:0650-135
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 1.6 mg/kg 1 07/08/09 22:52 7440-36-007/07/09 14:200.36
Arsenic ND mg/kg 1 07/08/09 22:52 7440-38-207/07/09 14:200.36
Beryllium 0.31 mg/kg 1 07/08/09 22:52 7440-41-707/07/09 14:200.072
Cadmium 2.5 mg/kg 1 07/08/09 22:52 7440-43-907/07/09 14:200.072
Chromium 21.9 mg/kg 1 07/08/09 22:52 7440-47-307/07/09 14:200.36
Copper 25.0 mg/kg 1 07/08/09 22:52 7440-50-807/07/09 14:200.36
Lead 39.4 mg/kg 1 07/08/09 22:52 7439-92-107/07/09 14:200.36
Manganese 272 mg/kg 1 07/08/09 22:52 7439-96-507/07/09 14:200.36
Nickel 11.5 mg/kg 1 07/08/09 22:52 7440-02-007/07/09 14:200.36
Selenium 0.84 mg/kg 1 07/08/09 22:52 7782-49-207/07/09 14:200.72
Silver ND mg/kg 1 07/08/09 22:52 7440-22-407/07/09 14:200.36
Thallium 1.0 mg/kg 1 07/08/09 22:52 7440-28-007/07/09 14:200.72
Zinc 138 mg/kg 1 07/08/09 22:52 7440-66-607/07/09 14:200.72
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.054 mg/kg 1 07/13/09 13:17 7439-97-607/13/09 10:440.0048
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/12/09 02:40 83-32-907/01/09 14:30352
Acenaphthylene ND ug/kg 1 07/12/09 02:40 208-96-807/01/09 14:30352
Aniline ND ug/kg 1 07/12/09 02:40 62-53-307/01/09 14:30352
Anthracene ND ug/kg 1 07/12/09 02:40 120-12-707/01/09 14:30352
Benzo(a)anthracene ND ug/kg 1 07/12/09 02:40 56-55-307/01/09 14:30352
Benzo(a)pyrene ND ug/kg 1 07/12/09 02:40 50-32-807/01/09 14:30352
Benzo(b)fluoranthene ND ug/kg 1 07/12/09 02:40 205-99-207/01/09 14:30352
Benzo(g,h,i)perylene ND ug/kg 1 07/12/09 02:40 191-24-207/01/09 14:30352
Benzo(k)fluoranthene ND ug/kg 1 07/12/09 02:40 207-08-907/01/09 14:30352
Benzoic Acid ND ug/kg 1 07/12/09 02:40 65-85-007/01/09 14:301760
Benzyl alcohol ND ug/kg 1 07/12/09 02:40 100-51-607/01/09 14:30704
4-Bromophenylphenyl ether ND ug/kg 1 07/12/09 02:40 101-55-307/01/09 14:30352
Butylbenzylphthalate ND ug/kg 1 07/12/09 02:40 85-68-707/01/09 14:30352
4-Chloro-3-methylphenol ND ug/kg 1 07/12/09 02:40 59-50-707/01/09 14:30704
4-Chloroaniline ND ug/kg 1 07/12/09 02:40 106-47-807/01/09 14:301760
bis(2-Chloroethoxy)methane ND ug/kg 1 07/12/09 02:40 111-91-107/01/09 14:30352
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 36 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB21-06-09 Lab ID:9247665015 Collected:06/30/09 15:00 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
bis(2-Chloroethyl) ether ND ug/kg 1 07/12/09 02:40 111-44-407/01/09 14:30352
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/12/09 02:40 108-60-107/01/09 14:30352
2-Chloronaphthalene ND ug/kg 1 07/12/09 02:40 91-58-707/01/09 14:30352
2-Chlorophenol ND ug/kg 1 07/12/09 02:40 95-57-807/01/09 14:30352
4-Chlorophenylphenyl ether ND ug/kg 1 07/12/09 02:40 7005-72-307/01/09 14:30352
Chrysene ND ug/kg 1 07/12/09 02:40 218-01-907/01/09 14:30352
Dibenz(a,h)anthracene ND ug/kg 1 07/12/09 02:40 53-70-307/01/09 14:30352
Dibenzofuran ND ug/kg 1 07/12/09 02:40 132-64-907/01/09 14:30352
1,2-Dichlorobenzene ND ug/kg 1 07/12/09 02:40 95-50-107/01/09 14:30352
1,3-Dichlorobenzene ND ug/kg 1 07/12/09 02:40 541-73-107/01/09 14:30352
1,4-Dichlorobenzene ND ug/kg 1 07/12/09 02:40 106-46-707/01/09 14:30352
3,3'-Dichlorobenzidine ND ug/kg 1 07/12/09 02:40 91-94-107/01/09 14:301760
2,4-Dichlorophenol ND ug/kg 1 07/12/09 02:40 120-83-207/01/09 14:30352
Diethylphthalate ND ug/kg 1 07/12/09 02:40 84-66-207/01/09 14:30352
2,4-Dimethylphenol ND ug/kg 1 07/12/09 02:40 105-67-907/01/09 14:30352
Dimethylphthalate ND ug/kg 1 07/12/09 02:40 131-11-307/01/09 14:30352
Di-n-butylphthalate ND ug/kg 1 07/12/09 02:40 84-74-207/01/09 14:30352
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/12/09 02:40 534-52-107/01/09 14:30704
2,4-Dinitrophenol ND ug/kg 1 07/12/09 02:40 51-28-507/01/09 14:301760
2,4-Dinitrotoluene ND ug/kg 1 07/12/09 02:40 121-14-207/01/09 14:30352
2,6-Dinitrotoluene ND ug/kg 1 07/12/09 02:40 606-20-207/01/09 14:30352
Di-n-octylphthalate ND ug/kg 1 07/12/09 02:40 117-84-007/01/09 14:30352
1,2-Diphenylhydrazine ND ug/kg 1 07/12/09 02:40 122-66-707/01/09 14:30352
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/12/09 02:40 117-81-707/01/09 14:30352
Fluoranthene ND ug/kg 1 07/12/09 02:40 206-44-007/01/09 14:30352
Fluorene ND ug/kg 1 07/12/09 02:40 86-73-707/01/09 14:30352
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/09 02:40 87-68-307/01/09 14:30352
Hexachlorobenzene ND ug/kg 1 07/12/09 02:40 118-74-107/01/09 14:30352
Hexachlorocyclopentadiene ND ug/kg 1 07/12/09 02:40 77-47-407/01/09 14:30352
Hexachloroethane ND ug/kg 1 07/12/09 02:40 67-72-107/01/09 14:30352
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/12/09 02:40 193-39-507/01/09 14:30352
Isophorone ND ug/kg 1 07/12/09 02:40 78-59-107/01/09 14:30352
1-Methylnaphthalene ND ug/kg 1 07/12/09 02:40 90-12-007/01/09 14:30352
2-Methylnaphthalene ND ug/kg 1 07/12/09 02:40 91-57-607/01/09 14:30352
2-Methylphenol(o-Cresol)ND ug/kg 1 07/12/09 02:40 95-48-707/01/09 14:30352
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/12/09 02:4007/01/09 14:30352
Naphthalene ND ug/kg 1 07/12/09 02:40 91-20-307/01/09 14:30352
2-Nitroaniline ND ug/kg 1 07/12/09 02:40 88-74-407/01/09 14:301760
3-Nitroaniline ND ug/kg 1 07/12/09 02:40 99-09-207/01/09 14:301760
4-Nitroaniline ND ug/kg 1 07/12/09 02:40 100-01-607/01/09 14:30704
Nitrobenzene ND ug/kg 1 07/12/09 02:40 98-95-307/01/09 14:30352
2-Nitrophenol ND ug/kg 1 07/12/09 02:40 88-75-507/01/09 14:30352
4-Nitrophenol ND ug/kg 1 07/12/09 02:40 100-02-707/01/09 14:301760
N-Nitrosodimethylamine ND ug/kg 1 07/12/09 02:40 62-75-907/01/09 14:30352
N-Nitroso-di-n-propylamine ND ug/kg 1 07/12/09 02:40 621-64-707/01/09 14:30352
N-Nitrosodiphenylamine ND ug/kg 1 07/12/09 02:40 86-30-607/01/09 14:30352
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 37 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB21-06-09 Lab ID:9247665015 Collected:06/30/09 15:00 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Pentachlorophenol ND ug/kg 1 07/12/09 02:40 87-86-507/01/09 14:301760
Phenanthrene ND ug/kg 1 07/12/09 02:40 85-01-807/01/09 14:30352
Phenol ND ug/kg 1 07/12/09 02:40 108-95-207/01/09 14:30352
Pyrene ND ug/kg 1 07/12/09 02:40 129-00-007/01/09 14:30352
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/09 02:40 120-82-107/01/09 14:30352
2,4,5-Trichlorophenol ND ug/kg 1 07/12/09 02:40 95-95-407/01/09 14:30352
2,4,6-Trichlorophenol ND ug/kg 1 07/12/09 02:40 88-06-207/01/09 14:30352
Nitrobenzene-d5 (S)31 %1 07/12/09 02:40 4165-60-007/01/09 14:3030-150
2-Fluorobiphenyl (S)39 %1 07/12/09 02:40 321-60-8 2g07/01/09 14:3046-120
Terphenyl-d14 (S)74 %1 07/12/09 02:40 1718-51-007/01/09 14:3038-108
Phenol-d6 (S)40 %1 07/12/09 02:40 13127-88-307/01/09 14:3035-120
2-Fluorophenol (S)37 %1 07/12/09 02:40 367-12-407/01/09 14:3024-120
2,4,6-Tribromophenol (S)39 %1 07/12/09 02:40 118-79-6 1g07/01/09 14:3044-136
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 172 ug/kg 1 07/06/09 18:48 67-64-1 C9128
Benzene ND ug/kg 1 07/06/09 18:48 71-43-26.4
Bromobenzene ND ug/kg 1 07/06/09 18:48 108-86-16.4
Bromochloromethane ND ug/kg 1 07/06/09 18:48 74-97-56.4
Bromodichloromethane ND ug/kg 1 07/06/09 18:48 75-27-46.4
Bromoform ND ug/kg 1 07/06/09 18:48 75-25-26.4
Bromomethane ND ug/kg 1 07/06/09 18:48 74-83-912.8
2-Butanone (MEK)ND ug/kg 1 07/06/09 18:48 78-93-3128
n-Butylbenzene ND ug/kg 1 07/06/09 18:48 104-51-86.4
sec-Butylbenzene ND ug/kg 1 07/06/09 18:48 135-98-86.4
tert-Butylbenzene ND ug/kg 1 07/06/09 18:48 98-06-66.4
Carbon tetrachloride ND ug/kg 1 07/06/09 18:48 56-23-56.4
Chlorobenzene ND ug/kg 1 07/06/09 18:48 108-90-76.4
Chloroethane ND ug/kg 1 07/06/09 18:48 75-00-312.8
Chloroform ND ug/kg 1 07/06/09 18:48 67-66-36.4
Chloromethane ND ug/kg 1 07/06/09 18:48 74-87-312.8
2-Chlorotoluene ND ug/kg 1 07/06/09 18:48 95-49-86.4
4-Chlorotoluene ND ug/kg 1 07/06/09 18:48 106-43-46.4
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/06/09 18:48 96-12-86.4
Dibromochloromethane ND ug/kg 1 07/06/09 18:48 124-48-16.4
1,2-Dibromoethane (EDB)ND ug/kg 1 07/06/09 18:48 106-93-46.4
Dibromomethane ND ug/kg 1 07/06/09 18:48 74-95-36.4
1,2-Dichlorobenzene ND ug/kg 1 07/06/09 18:48 95-50-16.4
1,3-Dichlorobenzene ND ug/kg 1 07/06/09 18:48 541-73-16.4
1,4-Dichlorobenzene ND ug/kg 1 07/06/09 18:48 106-46-76.4
Dichlorodifluoromethane ND ug/kg 1 07/06/09 18:48 75-71-812.8
1,1-Dichloroethane ND ug/kg 1 07/06/09 18:48 75-34-36.4
1,2-Dichloroethane ND ug/kg 1 07/06/09 18:48 107-06-26.4
1,1-Dichloroethene ND ug/kg 1 07/06/09 18:48 75-35-46.4
cis-1,2-Dichloroethene ND ug/kg 1 07/06/09 18:48 156-59-26.4
trans-1,2-Dichloroethene ND ug/kg 1 07/06/09 18:48 156-60-56.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 38 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB21-06-09 Lab ID:9247665015 Collected:06/30/09 15:00 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dichloropropane ND ug/kg 1 07/06/09 18:48 78-87-56.4
1,3-Dichloropropane ND ug/kg 1 07/06/09 18:48 142-28-96.4
2,2-Dichloropropane ND ug/kg 1 07/06/09 18:48 594-20-76.4
1,1-Dichloropropene ND ug/kg 1 07/06/09 18:48 563-58-66.4
cis-1,3-Dichloropropene ND ug/kg 1 07/06/09 18:48 10061-01-56.4
trans-1,3-Dichloropropene ND ug/kg 1 07/06/09 18:48 10061-02-66.4
Diisopropyl ether ND ug/kg 1 07/06/09 18:48 108-20-36.4
Ethylbenzene ND ug/kg 1 07/06/09 18:48 100-41-46.4
Hexachloro-1,3-butadiene ND ug/kg 1 07/06/09 18:48 87-68-36.4
2-Hexanone ND ug/kg 1 07/06/09 18:48 591-78-663.8
Isopropylbenzene (Cumene)ND ug/kg 1 07/06/09 18:48 98-82-86.4
p-Isopropyltoluene ND ug/kg 1 07/06/09 18:48 99-87-66.4
Methylene Chloride ND ug/kg 1 07/06/09 18:48 75-09-225.5
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/06/09 18:48 108-10-163.8
Methyl-tert-butyl ether ND ug/kg 1 07/06/09 18:48 1634-04-46.4
Naphthalene ND ug/kg 1 07/06/09 18:48 91-20-36.4
n-Propylbenzene ND ug/kg 1 07/06/09 18:48 103-65-16.4
Styrene ND ug/kg 1 07/06/09 18:48 100-42-56.4
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/06/09 18:48 630-20-66.4
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/06/09 18:48 79-34-56.4
Tetrachloroethene ND ug/kg 1 07/06/09 18:48 127-18-46.4
Toluene ND ug/kg 1 07/06/09 18:48 108-88-36.4
1,2,3-Trichlorobenzene ND ug/kg 1 07/06/09 18:48 87-61-66.4
1,2,4-Trichlorobenzene ND ug/kg 1 07/06/09 18:48 120-82-16.4
1,1,1-Trichloroethane ND ug/kg 1 07/06/09 18:48 71-55-66.4
1,1,2-Trichloroethane ND ug/kg 1 07/06/09 18:48 79-00-56.4
Trichloroethene ND ug/kg 1 07/06/09 18:48 79-01-66.4
Trichlorofluoromethane ND ug/kg 1 07/06/09 18:48 75-69-46.4
1,2,3-Trichloropropane ND ug/kg 1 07/06/09 18:48 96-18-46.4
1,2,4-Trimethylbenzene ND ug/kg 1 07/06/09 18:48 95-63-66.4
1,3,5-Trimethylbenzene ND ug/kg 1 07/06/09 18:48 108-67-86.4
Vinyl acetate ND ug/kg 1 07/06/09 18:48 108-05-463.8
Vinyl chloride ND ug/kg 1 07/06/09 18:48 75-01-412.8
Xylene (Total)ND ug/kg 1 07/06/09 18:48 1330-20-712.8
m&p-Xylene ND ug/kg 1 07/06/09 18:48 1330-20-712.8
o-Xylene ND ug/kg 1 07/06/09 18:48 95-47-66.4
Dibromofluoromethane (S)107 %1 07/06/09 18:48 1868-53-779-116
Toluene-d8 (S)92 %1 07/06/09 18:48 2037-26-588-110
4-Bromofluorobenzene (S)88 %1 07/06/09 18:48 460-00-474-115
1,2-Dichloroethane-d4 (S)105 %1 07/06/09 18:48 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 6.3 %1 07/06/09 08:390.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 39 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB22-06-09 Lab ID:9247665016 Collected:06/30/09 15:30 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 65.3 mg/kg 1 07/14/09 16:07 68334-30-507/09/09 15:305.8
n-Pentacosane (S)98 %1 07/14/09 16:07 629-99-207/09/09 15:3050-135
9071 Oil and Grease Analytical Method: 9071B ASE Preparation Method: 9071B ASE
Oil and Grease 221 mg/kg 1 07/09/09 14:3707/09/09 13:1081.3
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/02/09 22:33 8006-61-907/02/09 15:069.4
4-Bromofluorobenzene (S)90 %1 07/02/09 22:33 460-00-407/02/09 15:0650-135
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 8.2 mg/kg 1 07/08/09 23:00 7440-36-007/07/09 14:200.52
Arsenic 6.3 mg/kg 1 07/08/09 23:00 7440-38-207/07/09 14:200.52
Beryllium 0.72 mg/kg 1 07/08/09 23:00 7440-41-707/07/09 14:200.10
Cadmium 8.7 mg/kg 1 07/08/09 23:00 7440-43-907/07/09 14:200.10
Chromium 118 mg/kg 1 07/08/09 23:00 7440-47-307/07/09 14:200.52
Copper 92.7 mg/kg 1 07/08/09 23:00 7440-50-807/07/09 14:200.52
Lead 212 mg/kg 1 07/08/09 23:00 7439-92-107/07/09 14:200.52
Manganese 482 mg/kg 1 07/08/09 23:00 7439-96-507/07/09 14:200.52
Nickel 43.4 mg/kg 1 07/08/09 23:00 7440-02-007/07/09 14:200.52
Selenium 3.0 mg/kg 1 07/08/09 23:00 7782-49-207/07/09 14:201.0
Silver ND mg/kg 1 07/08/09 23:00 7440-22-407/07/09 14:200.52
Thallium ND mg/kg 1 07/08/09 23:00 7440-28-007/07/09 14:201.0
Zinc 808 mg/kg 1 07/08/09 23:00 7440-66-607/07/09 14:201.0
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.51 mg/kg 50 07/13/09 14:06 7439-97-607/13/09 10:440.27
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/12/09 03:06 83-32-907/01/09 14:30383
Acenaphthylene ND ug/kg 1 07/12/09 03:06 208-96-807/01/09 14:30383
Aniline ND ug/kg 1 07/12/09 03:06 62-53-307/01/09 14:30383
Anthracene ND ug/kg 1 07/12/09 03:06 120-12-707/01/09 14:30383
Benzo(a)anthracene ND ug/kg 1 07/12/09 03:06 56-55-307/01/09 14:30383
Benzo(a)pyrene ND ug/kg 1 07/12/09 03:06 50-32-807/01/09 14:30383
Benzo(b)fluoranthene ND ug/kg 1 07/12/09 03:06 205-99-207/01/09 14:30383
Benzo(g,h,i)perylene ND ug/kg 1 07/12/09 03:06 191-24-207/01/09 14:30383
Benzo(k)fluoranthene ND ug/kg 1 07/12/09 03:06 207-08-907/01/09 14:30383
Benzoic Acid ND ug/kg 1 07/12/09 03:06 65-85-007/01/09 14:301920
Benzyl alcohol ND ug/kg 1 07/12/09 03:06 100-51-607/01/09 14:30766
4-Bromophenylphenyl ether ND ug/kg 1 07/12/09 03:06 101-55-307/01/09 14:30383
Butylbenzylphthalate ND ug/kg 1 07/12/09 03:06 85-68-707/01/09 14:30383
4-Chloro-3-methylphenol ND ug/kg 1 07/12/09 03:06 59-50-707/01/09 14:30766
4-Chloroaniline ND ug/kg 1 07/12/09 03:06 106-47-807/01/09 14:301920
bis(2-Chloroethoxy)methane ND ug/kg 1 07/12/09 03:06 111-91-107/01/09 14:30383
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 40 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB22-06-09 Lab ID:9247665016 Collected:06/30/09 15:30 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
bis(2-Chloroethyl) ether ND ug/kg 1 07/12/09 03:06 111-44-407/01/09 14:30383
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/12/09 03:06 108-60-107/01/09 14:30383
2-Chloronaphthalene ND ug/kg 1 07/12/09 03:06 91-58-707/01/09 14:30383
2-Chlorophenol ND ug/kg 1 07/12/09 03:06 95-57-807/01/09 14:30383
4-Chlorophenylphenyl ether ND ug/kg 1 07/12/09 03:06 7005-72-307/01/09 14:30383
Chrysene ND ug/kg 1 07/12/09 03:06 218-01-907/01/09 14:30383
Dibenz(a,h)anthracene ND ug/kg 1 07/12/09 03:06 53-70-307/01/09 14:30383
Dibenzofuran ND ug/kg 1 07/12/09 03:06 132-64-907/01/09 14:30383
1,2-Dichlorobenzene ND ug/kg 1 07/12/09 03:06 95-50-107/01/09 14:30383
1,3-Dichlorobenzene ND ug/kg 1 07/12/09 03:06 541-73-107/01/09 14:30383
1,4-Dichlorobenzene ND ug/kg 1 07/12/09 03:06 106-46-707/01/09 14:30383
3,3'-Dichlorobenzidine ND ug/kg 1 07/12/09 03:06 91-94-107/01/09 14:301920
2,4-Dichlorophenol ND ug/kg 1 07/12/09 03:06 120-83-207/01/09 14:30383
Diethylphthalate ND ug/kg 1 07/12/09 03:06 84-66-207/01/09 14:30383
2,4-Dimethylphenol ND ug/kg 1 07/12/09 03:06 105-67-907/01/09 14:30383
Dimethylphthalate ND ug/kg 1 07/12/09 03:06 131-11-307/01/09 14:30383
Di-n-butylphthalate ND ug/kg 1 07/12/09 03:06 84-74-207/01/09 14:30383
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/12/09 03:06 534-52-107/01/09 14:30766
2,4-Dinitrophenol ND ug/kg 1 07/12/09 03:06 51-28-507/01/09 14:301920
2,4-Dinitrotoluene ND ug/kg 1 07/12/09 03:06 121-14-207/01/09 14:30383
2,6-Dinitrotoluene ND ug/kg 1 07/12/09 03:06 606-20-207/01/09 14:30383
Di-n-octylphthalate ND ug/kg 1 07/12/09 03:06 117-84-007/01/09 14:30383
1,2-Diphenylhydrazine ND ug/kg 1 07/12/09 03:06 122-66-707/01/09 14:30383
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/12/09 03:06 117-81-707/01/09 14:30383
Fluoranthene ND ug/kg 1 07/12/09 03:06 206-44-007/01/09 14:30383
Fluorene ND ug/kg 1 07/12/09 03:06 86-73-707/01/09 14:30383
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/09 03:06 87-68-307/01/09 14:30383
Hexachlorobenzene ND ug/kg 1 07/12/09 03:06 118-74-107/01/09 14:30383
Hexachlorocyclopentadiene ND ug/kg 1 07/12/09 03:06 77-47-407/01/09 14:30383
Hexachloroethane ND ug/kg 1 07/12/09 03:06 67-72-107/01/09 14:30383
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/12/09 03:06 193-39-507/01/09 14:30383
Isophorone ND ug/kg 1 07/12/09 03:06 78-59-107/01/09 14:30383
1-Methylnaphthalene 549 ug/kg 1 07/12/09 03:06 90-12-007/01/09 14:30383
2-Methylnaphthalene 626 ug/kg 1 07/12/09 03:06 91-57-607/01/09 14:30383
2-Methylphenol(o-Cresol)ND ug/kg 1 07/12/09 03:06 95-48-707/01/09 14:30383
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/12/09 03:0607/01/09 14:30383
Naphthalene 557 ug/kg 1 07/12/09 03:06 91-20-307/01/09 14:30383
2-Nitroaniline ND ug/kg 1 07/12/09 03:06 88-74-407/01/09 14:301920
3-Nitroaniline ND ug/kg 1 07/12/09 03:06 99-09-207/01/09 14:301920
4-Nitroaniline ND ug/kg 1 07/12/09 03:06 100-01-607/01/09 14:30766
Nitrobenzene ND ug/kg 1 07/12/09 03:06 98-95-307/01/09 14:30383
2-Nitrophenol ND ug/kg 1 07/12/09 03:06 88-75-507/01/09 14:30383
4-Nitrophenol ND ug/kg 1 07/12/09 03:06 100-02-707/01/09 14:301920
N-Nitrosodimethylamine ND ug/kg 1 07/12/09 03:06 62-75-907/01/09 14:30383
N-Nitroso-di-n-propylamine ND ug/kg 1 07/12/09 03:06 621-64-707/01/09 14:30383
N-Nitrosodiphenylamine ND ug/kg 1 07/12/09 03:06 86-30-607/01/09 14:30383
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 41 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB22-06-09 Lab ID:9247665016 Collected:06/30/09 15:30 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Pentachlorophenol ND ug/kg 1 07/12/09 03:06 87-86-507/01/09 14:301920
Phenanthrene ND ug/kg 1 07/12/09 03:06 85-01-807/01/09 14:30383
Phenol ND ug/kg 1 07/12/09 03:06 108-95-207/01/09 14:30383
Pyrene ND ug/kg 1 07/12/09 03:06 129-00-007/01/09 14:30383
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/09 03:06 120-82-107/01/09 14:30383
2,4,5-Trichlorophenol ND ug/kg 1 07/12/09 03:06 95-95-407/01/09 14:30383
2,4,6-Trichlorophenol ND ug/kg 1 07/12/09 03:06 88-06-207/01/09 14:30383
Nitrobenzene-d5 (S)57 %1 07/12/09 03:06 4165-60-007/01/09 14:3030-150
2-Fluorobiphenyl (S)57 %1 07/12/09 03:06 321-60-807/01/09 14:3046-120
Terphenyl-d14 (S)103 %1 07/12/09 03:06 1718-51-007/01/09 14:3038-108
Phenol-d6 (S)41 %1 07/12/09 03:06 13127-88-307/01/09 14:3035-120
2-Fluorophenol (S)31 %1 07/12/09 03:06 367-12-407/01/09 14:3024-120
2,4,6-Tribromophenol (S)45 %1 07/12/09 03:06 118-79-607/01/09 14:3044-136
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/06/09 19:06 67-64-1106
Benzene ND ug/kg 1 07/06/09 19:06 71-43-25.3
Bromobenzene ND ug/kg 1 07/06/09 19:06 108-86-15.3
Bromochloromethane ND ug/kg 1 07/06/09 19:06 74-97-55.3
Bromodichloromethane ND ug/kg 1 07/06/09 19:06 75-27-45.3
Bromoform ND ug/kg 1 07/06/09 19:06 75-25-25.3
Bromomethane ND ug/kg 1 07/06/09 19:06 74-83-910.6
2-Butanone (MEK)ND ug/kg 1 07/06/09 19:06 78-93-3106
n-Butylbenzene ND ug/kg 1 07/06/09 19:06 104-51-85.3
sec-Butylbenzene ND ug/kg 1 07/06/09 19:06 135-98-85.3
tert-Butylbenzene ND ug/kg 1 07/06/09 19:06 98-06-65.3
Carbon tetrachloride ND ug/kg 1 07/06/09 19:06 56-23-55.3
Chlorobenzene ND ug/kg 1 07/06/09 19:06 108-90-75.3
Chloroethane ND ug/kg 1 07/06/09 19:06 75-00-310.6
Chloroform ND ug/kg 1 07/06/09 19:06 67-66-35.3
Chloromethane ND ug/kg 1 07/06/09 19:06 74-87-310.6
2-Chlorotoluene ND ug/kg 1 07/06/09 19:06 95-49-85.3
4-Chlorotoluene ND ug/kg 1 07/06/09 19:06 106-43-45.3
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/06/09 19:06 96-12-85.3
Dibromochloromethane ND ug/kg 1 07/06/09 19:06 124-48-15.3
1,2-Dibromoethane (EDB)ND ug/kg 1 07/06/09 19:06 106-93-45.3
Dibromomethane ND ug/kg 1 07/06/09 19:06 74-95-35.3
1,2-Dichlorobenzene ND ug/kg 1 07/06/09 19:06 95-50-15.3
1,3-Dichlorobenzene ND ug/kg 1 07/06/09 19:06 541-73-15.3
1,4-Dichlorobenzene ND ug/kg 1 07/06/09 19:06 106-46-75.3
Dichlorodifluoromethane ND ug/kg 1 07/06/09 19:06 75-71-810.6
1,1-Dichloroethane ND ug/kg 1 07/06/09 19:06 75-34-35.3
1,2-Dichloroethane ND ug/kg 1 07/06/09 19:06 107-06-25.3
1,1-Dichloroethene ND ug/kg 1 07/06/09 19:06 75-35-45.3
cis-1,2-Dichloroethene ND ug/kg 1 07/06/09 19:06 156-59-25.3
trans-1,2-Dichloroethene ND ug/kg 1 07/06/09 19:06 156-60-55.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 42 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB22-06-09 Lab ID:9247665016 Collected:06/30/09 15:30 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dichloropropane ND ug/kg 1 07/06/09 19:06 78-87-55.3
1,3-Dichloropropane ND ug/kg 1 07/06/09 19:06 142-28-95.3
2,2-Dichloropropane ND ug/kg 1 07/06/09 19:06 594-20-75.3
1,1-Dichloropropene ND ug/kg 1 07/06/09 19:06 563-58-65.3
cis-1,3-Dichloropropene ND ug/kg 1 07/06/09 19:06 10061-01-55.3
trans-1,3-Dichloropropene ND ug/kg 1 07/06/09 19:06 10061-02-65.3
Diisopropyl ether ND ug/kg 1 07/06/09 19:06 108-20-35.3
Ethylbenzene ND ug/kg 1 07/06/09 19:06 100-41-45.3
Hexachloro-1,3-butadiene ND ug/kg 1 07/06/09 19:06 87-68-35.3
2-Hexanone ND ug/kg 1 07/06/09 19:06 591-78-652.9
Isopropylbenzene (Cumene)ND ug/kg 1 07/06/09 19:06 98-82-85.3
p-Isopropyltoluene ND ug/kg 1 07/06/09 19:06 99-87-65.3
Methylene Chloride ND ug/kg 1 07/06/09 19:06 75-09-221.2
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/06/09 19:06 108-10-152.9
Methyl-tert-butyl ether ND ug/kg 1 07/06/09 19:06 1634-04-45.3
Naphthalene ND ug/kg 1 07/06/09 19:06 91-20-35.3
n-Propylbenzene ND ug/kg 1 07/06/09 19:06 103-65-15.3
Styrene ND ug/kg 1 07/06/09 19:06 100-42-55.3
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/06/09 19:06 630-20-65.3
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/06/09 19:06 79-34-55.3
Tetrachloroethene ND ug/kg 1 07/06/09 19:06 127-18-45.3
Toluene ND ug/kg 1 07/06/09 19:06 108-88-35.3
1,2,3-Trichlorobenzene ND ug/kg 1 07/06/09 19:06 87-61-65.3
1,2,4-Trichlorobenzene ND ug/kg 1 07/06/09 19:06 120-82-15.3
1,1,1-Trichloroethane ND ug/kg 1 07/06/09 19:06 71-55-65.3
1,1,2-Trichloroethane ND ug/kg 1 07/06/09 19:06 79-00-55.3
Trichloroethene ND ug/kg 1 07/06/09 19:06 79-01-65.3
Trichlorofluoromethane ND ug/kg 1 07/06/09 19:06 75-69-45.3
1,2,3-Trichloropropane ND ug/kg 1 07/06/09 19:06 96-18-45.3
1,2,4-Trimethylbenzene ND ug/kg 1 07/06/09 19:06 95-63-65.3
1,3,5-Trimethylbenzene ND ug/kg 1 07/06/09 19:06 108-67-85.3
Vinyl acetate ND ug/kg 1 07/06/09 19:06 108-05-452.9
Vinyl chloride ND ug/kg 1 07/06/09 19:06 75-01-410.6
Xylene (Total)ND ug/kg 1 07/06/09 19:06 1330-20-710.6
m&p-Xylene ND ug/kg 1 07/06/09 19:06 1330-20-710.6
o-Xylene ND ug/kg 1 07/06/09 19:06 95-47-65.3
Dibromofluoromethane (S)103 %1 07/06/09 19:06 1868-53-779-116
Toluene-d8 (S)100 %1 07/06/09 19:06 2037-26-588-110
4-Bromofluorobenzene (S)101 %1 07/06/09 19:06 460-00-474-115
1,2-Dichloroethane-d4 (S)104 %1 07/06/09 19:06 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 13.9 %1 07/06/09 08:380.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 43 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB23-06-09 Lab ID:9247665017 Collected:06/30/09 15:50 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 151 mg/kg 1 07/14/09 16:07 68334-30-507/09/09 15:305.6
n-Pentacosane (S)202 %1 07/14/09 16:07 629-99-2 4g07/09/09 15:3050-135
9071 Oil and Grease Analytical Method: 9071B ASE Preparation Method: 9071B ASE
Oil and Grease 1240 mg/kg 1 07/09/09 14:3807/09/09 13:1077.9
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/02/09 22:57 8006-61-907/02/09 15:066.5
4-Bromofluorobenzene (S)92 %1 07/02/09 22:57 460-00-407/02/09 15:0650-135
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 3.2 mg/kg 1 07/08/09 23:05 7440-36-007/07/09 14:200.51
Arsenic 3.1 mg/kg 1 07/08/09 23:05 7440-38-207/07/09 14:200.51
Beryllium 0.78 mg/kg 1 07/08/09 23:05 7440-41-707/07/09 14:200.10
Cadmium 3.5 mg/kg 1 07/08/09 23:05 7440-43-907/07/09 14:200.10
Chromium 30.0 mg/kg 1 07/08/09 23:05 7440-47-307/07/09 14:200.51
Copper 90.5 mg/kg 1 07/08/09 23:05 7440-50-807/07/09 14:200.51
Lead 149 mg/kg 1 07/08/09 23:05 7439-92-107/07/09 14:200.51
Manganese 440 mg/kg 1 07/08/09 23:05 7439-96-507/07/09 14:200.51
Nickel 19.3 mg/kg 1 07/08/09 23:05 7440-02-007/07/09 14:200.51
Selenium 1.7 mg/kg 1 07/08/09 23:05 7782-49-207/07/09 14:201.0
Silver ND mg/kg 1 07/08/09 23:05 7440-22-407/07/09 14:200.51
Thallium ND mg/kg 1 07/08/09 23:05 7440-28-007/07/09 14:201.0
Zinc 547 mg/kg 1 07/08/09 23:05 7440-66-607/07/09 14:201.0
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.31 mg/kg 10 07/13/09 14:08 7439-97-607/13/09 10:440.045
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/12/09 03:33 83-32-907/01/09 14:30367
Acenaphthylene ND ug/kg 1 07/12/09 03:33 208-96-807/01/09 14:30367
Aniline ND ug/kg 1 07/12/09 03:33 62-53-307/01/09 14:30367
Anthracene ND ug/kg 1 07/12/09 03:33 120-12-707/01/09 14:30367
Benzo(a)anthracene ND ug/kg 1 07/12/09 03:33 56-55-307/01/09 14:30367
Benzo(a)pyrene ND ug/kg 1 07/12/09 03:33 50-32-807/01/09 14:30367
Benzo(b)fluoranthene 385 ug/kg 1 07/12/09 03:33 205-99-207/01/09 14:30367
Benzo(g,h,i)perylene ND ug/kg 1 07/12/09 03:33 191-24-207/01/09 14:30367
Benzo(k)fluoranthene 453 ug/kg 1 07/12/09 03:33 207-08-907/01/09 14:30367
Benzoic Acid ND ug/kg 1 07/12/09 03:33 65-85-007/01/09 14:301840
Benzyl alcohol ND ug/kg 1 07/12/09 03:33 100-51-607/01/09 14:30734
4-Bromophenylphenyl ether ND ug/kg 1 07/12/09 03:33 101-55-307/01/09 14:30367
Butylbenzylphthalate ND ug/kg 1 07/12/09 03:33 85-68-707/01/09 14:30367
4-Chloro-3-methylphenol ND ug/kg 1 07/12/09 03:33 59-50-707/01/09 14:30734
4-Chloroaniline ND ug/kg 1 07/12/09 03:33 106-47-807/01/09 14:301840
bis(2-Chloroethoxy)methane ND ug/kg 1 07/12/09 03:33 111-91-107/01/09 14:30367
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 44 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB23-06-09 Lab ID:9247665017 Collected:06/30/09 15:50 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
bis(2-Chloroethyl) ether ND ug/kg 1 07/12/09 03:33 111-44-407/01/09 14:30367
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/12/09 03:33 108-60-107/01/09 14:30367
2-Chloronaphthalene ND ug/kg 1 07/12/09 03:33 91-58-707/01/09 14:30367
2-Chlorophenol ND ug/kg 1 07/12/09 03:33 95-57-807/01/09 14:30367
4-Chlorophenylphenyl ether ND ug/kg 1 07/12/09 03:33 7005-72-307/01/09 14:30367
Chrysene 506 ug/kg 1 07/12/09 03:33 218-01-907/01/09 14:30367
Dibenz(a,h)anthracene ND ug/kg 1 07/12/09 03:33 53-70-307/01/09 14:30367
Dibenzofuran ND ug/kg 1 07/12/09 03:33 132-64-907/01/09 14:30367
1,2-Dichlorobenzene ND ug/kg 1 07/12/09 03:33 95-50-107/01/09 14:30367
1,3-Dichlorobenzene ND ug/kg 1 07/12/09 03:33 541-73-107/01/09 14:30367
1,4-Dichlorobenzene ND ug/kg 1 07/12/09 03:33 106-46-707/01/09 14:30367
3,3'-Dichlorobenzidine ND ug/kg 1 07/12/09 03:33 91-94-107/01/09 14:301840
2,4-Dichlorophenol ND ug/kg 1 07/12/09 03:33 120-83-207/01/09 14:30367
Diethylphthalate ND ug/kg 1 07/12/09 03:33 84-66-207/01/09 14:30367
2,4-Dimethylphenol ND ug/kg 1 07/12/09 03:33 105-67-907/01/09 14:30367
Dimethylphthalate ND ug/kg 1 07/12/09 03:33 131-11-307/01/09 14:30367
Di-n-butylphthalate ND ug/kg 1 07/12/09 03:33 84-74-207/01/09 14:30367
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/12/09 03:33 534-52-107/01/09 14:30734
2,4-Dinitrophenol ND ug/kg 1 07/12/09 03:33 51-28-507/01/09 14:301840
2,4-Dinitrotoluene ND ug/kg 1 07/12/09 03:33 121-14-207/01/09 14:30367
2,6-Dinitrotoluene ND ug/kg 1 07/12/09 03:33 606-20-207/01/09 14:30367
Di-n-octylphthalate ND ug/kg 1 07/12/09 03:33 117-84-007/01/09 14:30367
1,2-Diphenylhydrazine ND ug/kg 1 07/12/09 03:33 122-66-707/01/09 14:30367
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/12/09 03:33 117-81-707/01/09 14:30367
Fluoranthene 703 ug/kg 1 07/12/09 03:33 206-44-007/01/09 14:30367
Fluorene ND ug/kg 1 07/12/09 03:33 86-73-707/01/09 14:30367
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/09 03:33 87-68-307/01/09 14:30367
Hexachlorobenzene ND ug/kg 1 07/12/09 03:33 118-74-107/01/09 14:30367
Hexachlorocyclopentadiene ND ug/kg 1 07/12/09 03:33 77-47-407/01/09 14:30367
Hexachloroethane ND ug/kg 1 07/12/09 03:33 67-72-107/01/09 14:30367
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/12/09 03:33 193-39-507/01/09 14:30367
Isophorone ND ug/kg 1 07/12/09 03:33 78-59-107/01/09 14:30367
1-Methylnaphthalene 460 ug/kg 1 07/12/09 03:33 90-12-007/01/09 14:30367
2-Methylnaphthalene 529 ug/kg 1 07/12/09 03:33 91-57-607/01/09 14:30367
2-Methylphenol(o-Cresol)ND ug/kg 1 07/12/09 03:33 95-48-707/01/09 14:30367
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/12/09 03:3307/01/09 14:30367
Naphthalene 434 ug/kg 1 07/12/09 03:33 91-20-307/01/09 14:30367
2-Nitroaniline ND ug/kg 1 07/12/09 03:33 88-74-407/01/09 14:301840
3-Nitroaniline ND ug/kg 1 07/12/09 03:33 99-09-207/01/09 14:301840
4-Nitroaniline ND ug/kg 1 07/12/09 03:33 100-01-607/01/09 14:30734
Nitrobenzene ND ug/kg 1 07/12/09 03:33 98-95-307/01/09 14:30367
2-Nitrophenol ND ug/kg 1 07/12/09 03:33 88-75-507/01/09 14:30367
4-Nitrophenol ND ug/kg 1 07/12/09 03:33 100-02-707/01/09 14:301840
N-Nitrosodimethylamine ND ug/kg 1 07/12/09 03:33 62-75-907/01/09 14:30367
N-Nitroso-di-n-propylamine ND ug/kg 1 07/12/09 03:33 621-64-707/01/09 14:30367
N-Nitrosodiphenylamine ND ug/kg 1 07/12/09 03:33 86-30-607/01/09 14:30367
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 45 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB23-06-09 Lab ID:9247665017 Collected:06/30/09 15:50 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Pentachlorophenol ND ug/kg 1 07/12/09 03:33 87-86-507/01/09 14:301840
Phenanthrene 813 ug/kg 1 07/12/09 03:33 85-01-807/01/09 14:30367
Phenol ND ug/kg 1 07/12/09 03:33 108-95-207/01/09 14:30367
Pyrene 1380 ug/kg 1 07/12/09 03:33 129-00-007/01/09 14:30367
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/09 03:33 120-82-107/01/09 14:30367
2,4,5-Trichlorophenol ND ug/kg 1 07/12/09 03:33 95-95-407/01/09 14:30367
2,4,6-Trichlorophenol ND ug/kg 1 07/12/09 03:33 88-06-207/01/09 14:30367
Nitrobenzene-d5 (S)55 %1 07/12/09 03:33 4165-60-007/01/09 14:3030-150
2-Fluorobiphenyl (S)60 %1 07/12/09 03:33 321-60-807/01/09 14:3046-120
Terphenyl-d14 (S)127 %1 07/12/09 03:33 1718-51-0 2g07/01/09 14:3038-108
Phenol-d6 (S)41 %1 07/12/09 03:33 13127-88-307/01/09 14:3035-120
2-Fluorophenol (S)39 %1 07/12/09 03:33 367-12-407/01/09 14:3024-120
2,4,6-Tribromophenol (S)53 %1 07/12/09 03:33 118-79-607/01/09 14:3044-136
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/07/09 14:08 67-64-190.6
Benzene ND ug/kg 1 07/07/09 14:08 71-43-24.5
Bromobenzene ND ug/kg 1 07/07/09 14:08 108-86-14.5
Bromochloromethane ND ug/kg 1 07/07/09 14:08 74-97-54.5
Bromodichloromethane ND ug/kg 1 07/07/09 14:08 75-27-44.5
Bromoform ND ug/kg 1 07/07/09 14:08 75-25-24.5
Bromomethane ND ug/kg 1 07/07/09 14:08 74-83-99.1
2-Butanone (MEK)ND ug/kg 1 07/07/09 14:08 78-93-390.6
n-Butylbenzene ND ug/kg 1 07/07/09 14:08 104-51-84.5
sec-Butylbenzene ND ug/kg 1 07/07/09 14:08 135-98-84.5
tert-Butylbenzene ND ug/kg 1 07/07/09 14:08 98-06-64.5
Carbon tetrachloride ND ug/kg 1 07/07/09 14:08 56-23-54.5
Chlorobenzene ND ug/kg 1 07/07/09 14:08 108-90-74.5
Chloroethane ND ug/kg 1 07/07/09 14:08 75-00-39.1
Chloroform ND ug/kg 1 07/07/09 14:08 67-66-34.5
Chloromethane ND ug/kg 1 07/07/09 14:08 74-87-39.1
2-Chlorotoluene ND ug/kg 1 07/07/09 14:08 95-49-84.5
4-Chlorotoluene ND ug/kg 1 07/07/09 14:08 106-43-44.5
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/07/09 14:08 96-12-84.5
Dibromochloromethane ND ug/kg 1 07/07/09 14:08 124-48-14.5
1,2-Dibromoethane (EDB)ND ug/kg 1 07/07/09 14:08 106-93-44.5
Dibromomethane ND ug/kg 1 07/07/09 14:08 74-95-34.5
1,2-Dichlorobenzene ND ug/kg 1 07/07/09 14:08 95-50-14.5
1,3-Dichlorobenzene ND ug/kg 1 07/07/09 14:08 541-73-14.5
1,4-Dichlorobenzene ND ug/kg 1 07/07/09 14:08 106-46-74.5
Dichlorodifluoromethane ND ug/kg 1 07/07/09 14:08 75-71-89.1
1,1-Dichloroethane ND ug/kg 1 07/07/09 14:08 75-34-34.5
1,2-Dichloroethane ND ug/kg 1 07/07/09 14:08 107-06-24.5
1,1-Dichloroethene ND ug/kg 1 07/07/09 14:08 75-35-44.5
cis-1,2-Dichloroethene ND ug/kg 1 07/07/09 14:08 156-59-24.5
trans-1,2-Dichloroethene ND ug/kg 1 07/07/09 14:08 156-60-54.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 46 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB23-06-09 Lab ID:9247665017 Collected:06/30/09 15:50 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dichloropropane ND ug/kg 1 07/07/09 14:08 78-87-54.5
1,3-Dichloropropane ND ug/kg 1 07/07/09 14:08 142-28-94.5
2,2-Dichloropropane ND ug/kg 1 07/07/09 14:08 594-20-74.5
1,1-Dichloropropene ND ug/kg 1 07/07/09 14:08 563-58-64.5
cis-1,3-Dichloropropene ND ug/kg 1 07/07/09 14:08 10061-01-54.5
trans-1,3-Dichloropropene ND ug/kg 1 07/07/09 14:08 10061-02-64.5
Diisopropyl ether ND ug/kg 1 07/07/09 14:08 108-20-34.5
Ethylbenzene ND ug/kg 1 07/07/09 14:08 100-41-44.5
Hexachloro-1,3-butadiene ND ug/kg 1 07/07/09 14:08 87-68-34.5
2-Hexanone ND ug/kg 1 07/07/09 14:08 591-78-645.3
Isopropylbenzene (Cumene)ND ug/kg 1 07/07/09 14:08 98-82-84.5
p-Isopropyltoluene ND ug/kg 1 07/07/09 14:08 99-87-64.5
Methylene Chloride ND ug/kg 1 07/07/09 14:08 75-09-218.1
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/07/09 14:08 108-10-145.3
Methyl-tert-butyl ether ND ug/kg 1 07/07/09 14:08 1634-04-44.5
Naphthalene ND ug/kg 1 07/07/09 14:08 91-20-34.5
n-Propylbenzene ND ug/kg 1 07/07/09 14:08 103-65-14.5
Styrene ND ug/kg 1 07/07/09 14:08 100-42-54.5
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/07/09 14:08 630-20-64.5
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/07/09 14:08 79-34-54.5
Tetrachloroethene ND ug/kg 1 07/07/09 14:08 127-18-44.5
Toluene ND ug/kg 1 07/07/09 14:08 108-88-34.5
1,2,3-Trichlorobenzene ND ug/kg 1 07/07/09 14:08 87-61-64.5
1,2,4-Trichlorobenzene ND ug/kg 1 07/07/09 14:08 120-82-14.5
1,1,1-Trichloroethane ND ug/kg 1 07/07/09 14:08 71-55-64.5
1,1,2-Trichloroethane ND ug/kg 1 07/07/09 14:08 79-00-54.5
Trichloroethene ND ug/kg 1 07/07/09 14:08 79-01-64.5
Trichlorofluoromethane ND ug/kg 1 07/07/09 14:08 75-69-44.5
1,2,3-Trichloropropane ND ug/kg 1 07/07/09 14:08 96-18-44.5
1,2,4-Trimethylbenzene ND ug/kg 1 07/07/09 14:08 95-63-64.5
1,3,5-Trimethylbenzene ND ug/kg 1 07/07/09 14:08 108-67-84.5
Vinyl acetate ND ug/kg 1 07/07/09 14:08 108-05-445.3
Vinyl chloride ND ug/kg 1 07/07/09 14:08 75-01-49.1
Xylene (Total)ND ug/kg 1 07/07/09 14:08 1330-20-79.1
m&p-Xylene ND ug/kg 1 07/07/09 14:08 1330-20-79.1
o-Xylene ND ug/kg 1 07/07/09 14:08 95-47-64.5
Dibromofluoromethane (S)98 %1 07/07/09 14:08 1868-53-779-116
Toluene-d8 (S)99 %1 07/07/09 14:08 2037-26-588-110
4-Bromofluorobenzene (S)98 %1 07/07/09 14:08 460-00-474-115
1,2-Dichloroethane-d4 (S)96 %1 07/07/09 14:08 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 10.1 %1 07/06/09 08:380.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 47 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB24-06-09 Lab ID:9247665018 Collected:06/30/09 16:10 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 40.4 mg/kg 1 07/14/09 16:36 68334-30-507/09/09 15:305.8
n-Pentacosane (S)93 %1 07/14/09 16:36 629-99-207/09/09 15:3050-135
9071 Oil and Grease Analytical Method: 9071B ASE Preparation Method: 9071B ASE
Oil and Grease 586 mg/kg 1 07/09/09 14:3807/09/09 13:1081.5
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/02/09 23:21 8006-61-907/02/09 15:069.8
4-Bromofluorobenzene (S)84 %1 07/02/09 23:21 460-00-407/02/09 15:0650-135
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 7.3 mg/kg 1 07/08/09 23:10 7440-36-007/07/09 14:200.56
Arsenic 2.4 mg/kg 1 07/08/09 23:10 7440-38-207/07/09 14:200.56
Beryllium 0.64 mg/kg 1 07/08/09 23:10 7440-41-707/07/09 14:200.11
Cadmium 2.6 mg/kg 1 07/08/09 23:10 7440-43-907/07/09 14:200.11
Chromium 42.3 mg/kg 1 07/08/09 23:10 7440-47-307/07/09 14:200.56
Copper 146 mg/kg 1 07/08/09 23:10 7440-50-807/07/09 14:200.56
Lead 522 mg/kg 1 07/08/09 23:10 7439-92-107/07/09 14:200.56
Manganese 440 mg/kg 1 07/08/09 23:10 7439-96-507/07/09 14:200.56
Nickel 15.0 mg/kg 1 07/08/09 23:10 7440-02-007/07/09 14:200.56
Selenium 1.9 mg/kg 1 07/08/09 23:10 7782-49-207/07/09 14:201.1
Silver ND mg/kg 1 07/08/09 23:10 7440-22-407/07/09 14:200.56
Thallium 1.1 mg/kg 1 07/08/09 23:10 7440-28-007/07/09 14:201.1
Zinc 675 mg/kg 1 07/08/09 23:10 7440-66-607/07/09 14:201.1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.099 mg/kg 1 07/13/09 13:26 7439-97-607/13/09 10:440.0048
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/12/09 04:00 83-32-907/01/09 14:30384
Acenaphthylene ND ug/kg 1 07/12/09 04:00 208-96-807/01/09 14:30384
Aniline ND ug/kg 1 07/12/09 04:00 62-53-307/01/09 14:30384
Anthracene 1240 ug/kg 1 07/12/09 04:00 120-12-707/01/09 14:30384
Benzo(a)anthracene 2310 ug/kg 1 07/12/09 04:00 56-55-307/01/09 14:30384
Benzo(a)pyrene 2850 ug/kg 1 07/12/09 04:00 50-32-807/01/09 14:30384
Benzo(b)fluoranthene 1600 ug/kg 1 07/12/09 04:00 205-99-207/01/09 14:30384
Benzo(g,h,i)perylene 990 ug/kg 1 07/12/09 04:00 191-24-207/01/09 14:30384
Benzo(k)fluoranthene 1830 ug/kg 1 07/12/09 04:00 207-08-907/01/09 14:30384
Benzoic Acid ND ug/kg 1 07/12/09 04:00 65-85-007/01/09 14:301920
Benzyl alcohol ND ug/kg 1 07/12/09 04:00 100-51-607/01/09 14:30768
4-Bromophenylphenyl ether ND ug/kg 1 07/12/09 04:00 101-55-307/01/09 14:30384
Butylbenzylphthalate ND ug/kg 1 07/12/09 04:00 85-68-707/01/09 14:30384
4-Chloro-3-methylphenol ND ug/kg 1 07/12/09 04:00 59-50-707/01/09 14:30768
4-Chloroaniline ND ug/kg 1 07/12/09 04:00 106-47-807/01/09 14:301920
bis(2-Chloroethoxy)methane ND ug/kg 1 07/12/09 04:00 111-91-107/01/09 14:30384
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 48 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB24-06-09 Lab ID:9247665018 Collected:06/30/09 16:10 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
bis(2-Chloroethyl) ether ND ug/kg 1 07/12/09 04:00 111-44-407/01/09 14:30384
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/12/09 04:00 108-60-107/01/09 14:30384
2-Chloronaphthalene ND ug/kg 1 07/12/09 04:00 91-58-707/01/09 14:30384
2-Chlorophenol ND ug/kg 1 07/12/09 04:00 95-57-807/01/09 14:30384
4-Chlorophenylphenyl ether ND ug/kg 1 07/12/09 04:00 7005-72-307/01/09 14:30384
Chrysene 2670 ug/kg 1 07/12/09 04:00 218-01-907/01/09 14:30384
Dibenz(a,h)anthracene ND ug/kg 1 07/12/09 04:00 53-70-307/01/09 14:30384
Dibenzofuran ND ug/kg 1 07/12/09 04:00 132-64-907/01/09 14:30384
1,2-Dichlorobenzene ND ug/kg 1 07/12/09 04:00 95-50-107/01/09 14:30384
1,3-Dichlorobenzene ND ug/kg 1 07/12/09 04:00 541-73-107/01/09 14:30384
1,4-Dichlorobenzene ND ug/kg 1 07/12/09 04:00 106-46-707/01/09 14:30384
3,3'-Dichlorobenzidine ND ug/kg 1 07/12/09 04:00 91-94-107/01/09 14:301920
2,4-Dichlorophenol ND ug/kg 1 07/12/09 04:00 120-83-207/01/09 14:30384
Diethylphthalate ND ug/kg 1 07/12/09 04:00 84-66-207/01/09 14:30384
2,4-Dimethylphenol ND ug/kg 1 07/12/09 04:00 105-67-907/01/09 14:30384
Dimethylphthalate ND ug/kg 1 07/12/09 04:00 131-11-307/01/09 14:30384
Di-n-butylphthalate ND ug/kg 1 07/12/09 04:00 84-74-207/01/09 14:30384
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/12/09 04:00 534-52-107/01/09 14:30768
2,4-Dinitrophenol ND ug/kg 1 07/12/09 04:00 51-28-507/01/09 14:301920
2,4-Dinitrotoluene ND ug/kg 1 07/12/09 04:00 121-14-207/01/09 14:30384
2,6-Dinitrotoluene ND ug/kg 1 07/12/09 04:00 606-20-207/01/09 14:30384
Di-n-octylphthalate ND ug/kg 1 07/12/09 04:00 117-84-007/01/09 14:30384
1,2-Diphenylhydrazine ND ug/kg 1 07/12/09 04:00 122-66-707/01/09 14:30384
bis(2-Ethylhexyl)phthalate ND ug/kg 1 07/12/09 04:00 117-81-707/01/09 14:30384
Fluoranthene 6760 ug/kg 5 07/14/09 11:46 206-44-007/01/09 14:301920
Fluorene 578 ug/kg 1 07/12/09 04:00 86-73-707/01/09 14:30384
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/09 04:00 87-68-307/01/09 14:30384
Hexachlorobenzene ND ug/kg 1 07/12/09 04:00 118-74-107/01/09 14:30384
Hexachlorocyclopentadiene ND ug/kg 1 07/12/09 04:00 77-47-407/01/09 14:30384
Hexachloroethane ND ug/kg 1 07/12/09 04:00 67-72-107/01/09 14:30384
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/12/09 04:00 193-39-507/01/09 14:30384
Isophorone ND ug/kg 1 07/12/09 04:00 78-59-107/01/09 14:30384
1-Methylnaphthalene ND ug/kg 1 07/12/09 04:00 90-12-007/01/09 14:30384
2-Methylnaphthalene ND ug/kg 1 07/12/09 04:00 91-57-607/01/09 14:30384
2-Methylphenol(o-Cresol)ND ug/kg 1 07/12/09 04:00 95-48-707/01/09 14:30384
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/12/09 04:0007/01/09 14:30384
Naphthalene ND ug/kg 1 07/12/09 04:00 91-20-307/01/09 14:30384
2-Nitroaniline ND ug/kg 1 07/12/09 04:00 88-74-407/01/09 14:301920
3-Nitroaniline ND ug/kg 1 07/12/09 04:00 99-09-207/01/09 14:301920
4-Nitroaniline ND ug/kg 1 07/12/09 04:00 100-01-607/01/09 14:30768
Nitrobenzene ND ug/kg 1 07/12/09 04:00 98-95-307/01/09 14:30384
2-Nitrophenol ND ug/kg 1 07/12/09 04:00 88-75-507/01/09 14:30384
4-Nitrophenol ND ug/kg 1 07/12/09 04:00 100-02-707/01/09 14:301920
N-Nitrosodimethylamine ND ug/kg 1 07/12/09 04:00 62-75-907/01/09 14:30384
N-Nitroso-di-n-propylamine ND ug/kg 1 07/12/09 04:00 621-64-707/01/09 14:30384
N-Nitrosodiphenylamine ND ug/kg 1 07/12/09 04:00 86-30-607/01/09 14:30384
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 49 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB24-06-09 Lab ID:9247665018 Collected:06/30/09 16:10 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Pentachlorophenol ND ug/kg 1 07/12/09 04:00 87-86-507/01/09 14:301920
Phenanthrene 8230 ug/kg 5 07/14/09 11:46 85-01-807/01/09 14:301920
Phenol ND ug/kg 1 07/12/09 04:00 108-95-207/01/09 14:30384
Pyrene 8920 ug/kg 5 07/14/09 11:46 129-00-007/01/09 14:301920
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/09 04:00 120-82-107/01/09 14:30384
2,4,5-Trichlorophenol ND ug/kg 1 07/12/09 04:00 95-95-407/01/09 14:30384
2,4,6-Trichlorophenol ND ug/kg 1 07/12/09 04:00 88-06-207/01/09 14:30384
Nitrobenzene-d5 (S)93 %1 07/12/09 04:00 4165-60-007/01/09 14:3030-150
2-Fluorobiphenyl (S)97 %1 07/12/09 04:00 321-60-807/01/09 14:3046-120
Terphenyl-d14 (S)91 %1 07/12/09 04:00 1718-51-007/01/09 14:3038-108
Phenol-d6 (S)34 %1 07/12/09 04:00 13127-88-3 1g07/01/09 14:3035-120
2-Fluorophenol (S)37 %1 07/12/09 04:00 367-12-407/01/09 14:3024-120
2,4,6-Tribromophenol (S)46 %1 07/12/09 04:00 118-79-607/01/09 14:3044-136
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/07/09 14:26 67-64-1100
Benzene ND ug/kg 1 07/07/09 14:26 71-43-25.0
Bromobenzene ND ug/kg 1 07/07/09 14:26 108-86-15.0
Bromochloromethane ND ug/kg 1 07/07/09 14:26 74-97-55.0
Bromodichloromethane ND ug/kg 1 07/07/09 14:26 75-27-45.0
Bromoform ND ug/kg 1 07/07/09 14:26 75-25-25.0
Bromomethane ND ug/kg 1 07/07/09 14:26 74-83-910.0
2-Butanone (MEK)ND ug/kg 1 07/07/09 14:26 78-93-3100
n-Butylbenzene ND ug/kg 1 07/07/09 14:26 104-51-85.0
sec-Butylbenzene ND ug/kg 1 07/07/09 14:26 135-98-85.0
tert-Butylbenzene ND ug/kg 1 07/07/09 14:26 98-06-65.0
Carbon tetrachloride ND ug/kg 1 07/07/09 14:26 56-23-55.0
Chlorobenzene ND ug/kg 1 07/07/09 14:26 108-90-75.0
Chloroethane ND ug/kg 1 07/07/09 14:26 75-00-310.0
Chloroform ND ug/kg 1 07/07/09 14:26 67-66-35.0
Chloromethane ND ug/kg 1 07/07/09 14:26 74-87-310.0
2-Chlorotoluene ND ug/kg 1 07/07/09 14:26 95-49-85.0
4-Chlorotoluene ND ug/kg 1 07/07/09 14:26 106-43-45.0
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/07/09 14:26 96-12-85.0
Dibromochloromethane ND ug/kg 1 07/07/09 14:26 124-48-15.0
1,2-Dibromoethane (EDB)ND ug/kg 1 07/07/09 14:26 106-93-45.0
Dibromomethane ND ug/kg 1 07/07/09 14:26 74-95-35.0
1,2-Dichlorobenzene ND ug/kg 1 07/07/09 14:26 95-50-15.0
1,3-Dichlorobenzene ND ug/kg 1 07/07/09 14:26 541-73-15.0
1,4-Dichlorobenzene ND ug/kg 1 07/07/09 14:26 106-46-75.0
Dichlorodifluoromethane ND ug/kg 1 07/07/09 14:26 75-71-810.0
1,1-Dichloroethane ND ug/kg 1 07/07/09 14:26 75-34-35.0
1,2-Dichloroethane ND ug/kg 1 07/07/09 14:26 107-06-25.0
1,1-Dichloroethene ND ug/kg 1 07/07/09 14:26 75-35-45.0
cis-1,2-Dichloroethene ND ug/kg 1 07/07/09 14:26 156-59-25.0
trans-1,2-Dichloroethene ND ug/kg 1 07/07/09 14:26 156-60-55.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 50 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB24-06-09 Lab ID:9247665018 Collected:06/30/09 16:10 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dichloropropane ND ug/kg 1 07/07/09 14:26 78-87-55.0
1,3-Dichloropropane ND ug/kg 1 07/07/09 14:26 142-28-95.0
2,2-Dichloropropane ND ug/kg 1 07/07/09 14:26 594-20-75.0
1,1-Dichloropropene ND ug/kg 1 07/07/09 14:26 563-58-65.0
cis-1,3-Dichloropropene ND ug/kg 1 07/07/09 14:26 10061-01-55.0
trans-1,3-Dichloropropene ND ug/kg 1 07/07/09 14:26 10061-02-65.0
Diisopropyl ether ND ug/kg 1 07/07/09 14:26 108-20-35.0
Ethylbenzene ND ug/kg 1 07/07/09 14:26 100-41-45.0
Hexachloro-1,3-butadiene ND ug/kg 1 07/07/09 14:26 87-68-35.0
2-Hexanone ND ug/kg 1 07/07/09 14:26 591-78-650.1
Isopropylbenzene (Cumene)ND ug/kg 1 07/07/09 14:26 98-82-85.0
p-Isopropyltoluene ND ug/kg 1 07/07/09 14:26 99-87-65.0
Methylene Chloride ND ug/kg 1 07/07/09 14:26 75-09-220.0
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/07/09 14:26 108-10-150.1
Methyl-tert-butyl ether ND ug/kg 1 07/07/09 14:26 1634-04-45.0
Naphthalene ND ug/kg 1 07/07/09 14:26 91-20-35.0
n-Propylbenzene ND ug/kg 1 07/07/09 14:26 103-65-15.0
Styrene ND ug/kg 1 07/07/09 14:26 100-42-55.0
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/07/09 14:26 630-20-65.0
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/07/09 14:26 79-34-55.0
Tetrachloroethene ND ug/kg 1 07/07/09 14:26 127-18-45.0
Toluene ND ug/kg 1 07/07/09 14:26 108-88-35.0
1,2,3-Trichlorobenzene ND ug/kg 1 07/07/09 14:26 87-61-65.0
1,2,4-Trichlorobenzene ND ug/kg 1 07/07/09 14:26 120-82-15.0
1,1,1-Trichloroethane ND ug/kg 1 07/07/09 14:26 71-55-65.0
1,1,2-Trichloroethane ND ug/kg 1 07/07/09 14:26 79-00-55.0
Trichloroethene ND ug/kg 1 07/07/09 14:26 79-01-65.0
Trichlorofluoromethane ND ug/kg 1 07/07/09 14:26 75-69-45.0
1,2,3-Trichloropropane ND ug/kg 1 07/07/09 14:26 96-18-45.0
1,2,4-Trimethylbenzene ND ug/kg 1 07/07/09 14:26 95-63-65.0
1,3,5-Trimethylbenzene ND ug/kg 1 07/07/09 14:26 108-67-85.0
Vinyl acetate ND ug/kg 1 07/07/09 14:26 108-05-450.1
Vinyl chloride ND ug/kg 1 07/07/09 14:26 75-01-410.0
Xylene (Total)ND ug/kg 1 07/07/09 14:26 1330-20-710.0
m&p-Xylene ND ug/kg 1 07/07/09 14:26 1330-20-710.0
o-Xylene ND ug/kg 1 07/07/09 14:26 95-47-65.0
Dibromofluoromethane (S)99 %1 07/07/09 14:26 1868-53-779-116
Toluene-d8 (S)100 %1 07/07/09 14:26 2037-26-588-110
4-Bromofluorobenzene (S)102 %1 07/07/09 14:26 460-00-474-115
1,2-Dichloroethane-d4 (S)96 %1 07/07/09 14:26 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 14.1 %1 07/06/09 12:340.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 51 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB25-06-09 Lab ID:9247665019 Collected:06/30/09 16:55 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 1080 mg/kg 1 07/14/09 16:36 68334-30-5 P307/09/09 15:3026.8
n-Pentacosane (S)0 %1 07/14/09 16:36 629-99-2 S407/09/09 15:3050-135
9071 Oil and Grease Analytical Method: 9071B ASE Preparation Method: 9071B ASE
Oil and Grease 3850 mg/kg 1 07/09/09 14:3907/09/09 13:1075.0
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/02/09 23:44 8006-61-907/02/09 15:067.6
4-Bromofluorobenzene (S)93 %1 07/02/09 23:44 460-00-407/02/09 15:0650-135
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony 1.2 mg/kg 1 07/08/09 23:16 7440-36-007/07/09 14:200.49
Arsenic ND mg/kg 1 07/08/09 23:16 7440-38-207/07/09 14:200.49
Beryllium 0.36 mg/kg 1 07/08/09 23:16 7440-41-707/07/09 14:200.097
Cadmium 1.2 mg/kg 1 07/08/09 23:16 7440-43-907/07/09 14:200.097
Chromium 17.7 mg/kg 1 07/08/09 23:16 7440-47-307/07/09 14:200.49
Copper 18.9 mg/kg 1 07/08/09 23:16 7440-50-807/07/09 14:200.49
Lead 59.1 mg/kg 1 07/08/09 23:16 7439-92-107/07/09 14:200.49
Manganese 371 mg/kg 1 07/08/09 23:16 7439-96-507/07/09 14:200.49
Nickel 10.6 mg/kg 1 07/08/09 23:16 7440-02-007/07/09 14:200.49
Selenium 1.6 mg/kg 1 07/08/09 23:16 7782-49-207/07/09 14:200.97
Silver ND mg/kg 1 07/08/09 23:16 7440-22-407/07/09 14:200.49
Thallium ND mg/kg 1 07/08/09 23:16 7440-28-007/07/09 14:200.97
Zinc 138 mg/kg 1 07/08/09 23:16 7440-66-607/07/09 14:200.97
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.032 mg/kg 1 07/13/09 13:29 7439-97-607/13/09 10:440.0049
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 07/12/09 04:26 83-32-907/01/09 14:30354
Acenaphthylene ND ug/kg 1 07/12/09 04:26 208-96-807/01/09 14:30354
Aniline ND ug/kg 1 07/12/09 04:26 62-53-307/01/09 14:30354
Anthracene ND ug/kg 1 07/12/09 04:26 120-12-707/01/09 14:30354
Benzo(a)anthracene ND ug/kg 1 07/12/09 04:26 56-55-307/01/09 14:30354
Benzo(a)pyrene ND ug/kg 1 07/12/09 04:26 50-32-807/01/09 14:30354
Benzo(b)fluoranthene ND ug/kg 1 07/12/09 04:26 205-99-207/01/09 14:30354
Benzo(g,h,i)perylene ND ug/kg 1 07/12/09 04:26 191-24-207/01/09 14:30354
Benzo(k)fluoranthene ND ug/kg 1 07/12/09 04:26 207-08-907/01/09 14:30354
Benzoic Acid ND ug/kg 1 07/12/09 04:26 65-85-007/01/09 14:301770
Benzyl alcohol ND ug/kg 1 07/12/09 04:26 100-51-607/01/09 14:30707
4-Bromophenylphenyl ether ND ug/kg 1 07/12/09 04:26 101-55-307/01/09 14:30354
Butylbenzylphthalate ND ug/kg 1 07/12/09 04:26 85-68-707/01/09 14:30354
4-Chloro-3-methylphenol ND ug/kg 1 07/12/09 04:26 59-50-707/01/09 14:30707
4-Chloroaniline ND ug/kg 1 07/12/09 04:26 106-47-807/01/09 14:301770
bis(2-Chloroethoxy)methane ND ug/kg 1 07/12/09 04:26 111-91-107/01/09 14:30354
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 52 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB25-06-09 Lab ID:9247665019 Collected:06/30/09 16:55 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
bis(2-Chloroethyl) ether ND ug/kg 1 07/12/09 04:26 111-44-407/01/09 14:30354
bis(2-Chloroisopropyl) ether ND ug/kg 1 07/12/09 04:26 108-60-107/01/09 14:30354
2-Chloronaphthalene ND ug/kg 1 07/12/09 04:26 91-58-707/01/09 14:30354
2-Chlorophenol ND ug/kg 1 07/12/09 04:26 95-57-807/01/09 14:30354
4-Chlorophenylphenyl ether ND ug/kg 1 07/12/09 04:26 7005-72-307/01/09 14:30354
Chrysene ND ug/kg 1 07/12/09 04:26 218-01-907/01/09 14:30354
Dibenz(a,h)anthracene ND ug/kg 1 07/12/09 04:26 53-70-307/01/09 14:30354
Dibenzofuran ND ug/kg 1 07/12/09 04:26 132-64-907/01/09 14:30354
1,2-Dichlorobenzene ND ug/kg 1 07/12/09 04:26 95-50-107/01/09 14:30354
1,3-Dichlorobenzene ND ug/kg 1 07/12/09 04:26 541-73-107/01/09 14:30354
1,4-Dichlorobenzene ND ug/kg 1 07/12/09 04:26 106-46-707/01/09 14:30354
3,3'-Dichlorobenzidine ND ug/kg 1 07/12/09 04:26 91-94-107/01/09 14:301770
2,4-Dichlorophenol ND ug/kg 1 07/12/09 04:26 120-83-207/01/09 14:30354
Diethylphthalate ND ug/kg 1 07/12/09 04:26 84-66-207/01/09 14:30354
2,4-Dimethylphenol ND ug/kg 1 07/12/09 04:26 105-67-907/01/09 14:30354
Dimethylphthalate ND ug/kg 1 07/12/09 04:26 131-11-307/01/09 14:30354
Di-n-butylphthalate ND ug/kg 1 07/12/09 04:26 84-74-207/01/09 14:30354
4,6-Dinitro-2-methylphenol ND ug/kg 1 07/12/09 04:26 534-52-107/01/09 14:30707
2,4-Dinitrophenol ND ug/kg 1 07/12/09 04:26 51-28-507/01/09 14:301770
2,4-Dinitrotoluene ND ug/kg 1 07/12/09 04:26 121-14-207/01/09 14:30354
2,6-Dinitrotoluene ND ug/kg 1 07/12/09 04:26 606-20-207/01/09 14:30354
Di-n-octylphthalate ND ug/kg 1 07/12/09 04:26 117-84-007/01/09 14:30354
1,2-Diphenylhydrazine ND ug/kg 1 07/12/09 04:26 122-66-707/01/09 14:30354
bis(2-Ethylhexyl)phthalate 498 ug/kg 1 07/12/09 04:26 117-81-707/01/09 14:30354
Fluoranthene ND ug/kg 1 07/12/09 04:26 206-44-007/01/09 14:30354
Fluorene ND ug/kg 1 07/12/09 04:26 86-73-707/01/09 14:30354
Hexachloro-1,3-butadiene ND ug/kg 1 07/12/09 04:26 87-68-307/01/09 14:30354
Hexachlorobenzene ND ug/kg 1 07/12/09 04:26 118-74-107/01/09 14:30354
Hexachlorocyclopentadiene ND ug/kg 1 07/12/09 04:26 77-47-407/01/09 14:30354
Hexachloroethane ND ug/kg 1 07/12/09 04:26 67-72-107/01/09 14:30354
Indeno(1,2,3-cd)pyrene ND ug/kg 1 07/12/09 04:26 193-39-507/01/09 14:30354
Isophorone ND ug/kg 1 07/12/09 04:26 78-59-107/01/09 14:30354
1-Methylnaphthalene ND ug/kg 1 07/12/09 04:26 90-12-007/01/09 14:30354
2-Methylnaphthalene ND ug/kg 1 07/12/09 04:26 91-57-607/01/09 14:30354
2-Methylphenol(o-Cresol)ND ug/kg 1 07/12/09 04:26 95-48-707/01/09 14:30354
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 07/12/09 04:2607/01/09 14:30354
Naphthalene ND ug/kg 1 07/12/09 04:26 91-20-307/01/09 14:30354
2-Nitroaniline ND ug/kg 1 07/12/09 04:26 88-74-407/01/09 14:301770
3-Nitroaniline ND ug/kg 1 07/12/09 04:26 99-09-207/01/09 14:301770
4-Nitroaniline ND ug/kg 1 07/12/09 04:26 100-01-607/01/09 14:30707
Nitrobenzene ND ug/kg 1 07/12/09 04:26 98-95-307/01/09 14:30354
2-Nitrophenol ND ug/kg 1 07/12/09 04:26 88-75-507/01/09 14:30354
4-Nitrophenol ND ug/kg 1 07/12/09 04:26 100-02-707/01/09 14:301770
N-Nitrosodimethylamine ND ug/kg 1 07/12/09 04:26 62-75-907/01/09 14:30354
N-Nitroso-di-n-propylamine ND ug/kg 1 07/12/09 04:26 621-64-707/01/09 14:30354
N-Nitrosodiphenylamine ND ug/kg 1 07/12/09 04:26 86-30-607/01/09 14:30354
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 53 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB25-06-09 Lab ID:9247665019 Collected:06/30/09 16:55 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Pentachlorophenol ND ug/kg 1 07/12/09 04:26 87-86-507/01/09 14:301770
Phenanthrene ND ug/kg 1 07/12/09 04:26 85-01-807/01/09 14:30354
Phenol ND ug/kg 1 07/12/09 04:26 108-95-207/01/09 14:30354
Pyrene 416 ug/kg 1 07/12/09 04:26 129-00-007/01/09 14:30354
1,2,4-Trichlorobenzene ND ug/kg 1 07/12/09 04:26 120-82-107/01/09 14:30354
2,4,5-Trichlorophenol ND ug/kg 1 07/12/09 04:26 95-95-407/01/09 14:30354
2,4,6-Trichlorophenol ND ug/kg 1 07/12/09 04:26 88-06-207/01/09 14:30354
Nitrobenzene-d5 (S)69 %1 07/12/09 04:26 4165-60-007/01/09 14:3030-150
2-Fluorobiphenyl (S)74 %1 07/12/09 04:26 321-60-807/01/09 14:3046-120
Terphenyl-d14 (S)189 %1 07/12/09 04:26 1718-51-0 2g07/01/09 14:3038-108
Phenol-d6 (S)55 %1 07/12/09 04:26 13127-88-307/01/09 14:3035-120
2-Fluorophenol (S)46 %1 07/12/09 04:26 367-12-407/01/09 14:3024-120
2,4,6-Tribromophenol (S)69 %1 07/12/09 04:26 118-79-607/01/09 14:3044-136
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 222 ug/kg 1 07/07/09 14:45 67-64-1 C9109
Benzene ND ug/kg 1 07/07/09 14:45 71-43-25.5
Bromobenzene ND ug/kg 1 07/07/09 14:45 108-86-15.5
Bromochloromethane ND ug/kg 1 07/07/09 14:45 74-97-55.5
Bromodichloromethane ND ug/kg 1 07/07/09 14:45 75-27-45.5
Bromoform ND ug/kg 1 07/07/09 14:45 75-25-25.5
Bromomethane ND ug/kg 1 07/07/09 14:45 74-83-910.9
2-Butanone (MEK)ND ug/kg 1 07/07/09 14:45 78-93-3109
n-Butylbenzene ND ug/kg 1 07/07/09 14:45 104-51-85.5
sec-Butylbenzene ND ug/kg 1 07/07/09 14:45 135-98-85.5
tert-Butylbenzene ND ug/kg 1 07/07/09 14:45 98-06-65.5
Carbon tetrachloride ND ug/kg 1 07/07/09 14:45 56-23-55.5
Chlorobenzene ND ug/kg 1 07/07/09 14:45 108-90-75.5
Chloroethane ND ug/kg 1 07/07/09 14:45 75-00-310.9
Chloroform ND ug/kg 1 07/07/09 14:45 67-66-35.5
Chloromethane ND ug/kg 1 07/07/09 14:45 74-87-310.9
2-Chlorotoluene ND ug/kg 1 07/07/09 14:45 95-49-85.5
4-Chlorotoluene ND ug/kg 1 07/07/09 14:45 106-43-45.5
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/07/09 14:45 96-12-85.5
Dibromochloromethane ND ug/kg 1 07/07/09 14:45 124-48-15.5
1,2-Dibromoethane (EDB)ND ug/kg 1 07/07/09 14:45 106-93-45.5
Dibromomethane ND ug/kg 1 07/07/09 14:45 74-95-35.5
1,2-Dichlorobenzene ND ug/kg 1 07/07/09 14:45 95-50-15.5
1,3-Dichlorobenzene ND ug/kg 1 07/07/09 14:45 541-73-15.5
1,4-Dichlorobenzene ND ug/kg 1 07/07/09 14:45 106-46-75.5
Dichlorodifluoromethane ND ug/kg 1 07/07/09 14:45 75-71-810.9
1,1-Dichloroethane ND ug/kg 1 07/07/09 14:45 75-34-35.5
1,2-Dichloroethane ND ug/kg 1 07/07/09 14:45 107-06-25.5
1,1-Dichloroethene ND ug/kg 1 07/07/09 14:45 75-35-45.5
cis-1,2-Dichloroethene ND ug/kg 1 07/07/09 14:45 156-59-25.5
trans-1,2-Dichloroethene ND ug/kg 1 07/07/09 14:45 156-60-55.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 54 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB25-06-09 Lab ID:9247665019 Collected:06/30/09 16:55 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dichloropropane ND ug/kg 1 07/07/09 14:45 78-87-55.5
1,3-Dichloropropane ND ug/kg 1 07/07/09 14:45 142-28-95.5
2,2-Dichloropropane ND ug/kg 1 07/07/09 14:45 594-20-75.5
1,1-Dichloropropene ND ug/kg 1 07/07/09 14:45 563-58-65.5
cis-1,3-Dichloropropene ND ug/kg 1 07/07/09 14:45 10061-01-55.5
trans-1,3-Dichloropropene ND ug/kg 1 07/07/09 14:45 10061-02-65.5
Diisopropyl ether ND ug/kg 1 07/07/09 14:45 108-20-35.5
Ethylbenzene ND ug/kg 1 07/07/09 14:45 100-41-45.5
Hexachloro-1,3-butadiene ND ug/kg 1 07/07/09 14:45 87-68-35.5
2-Hexanone ND ug/kg 1 07/07/09 14:45 591-78-654.7
Isopropylbenzene (Cumene)ND ug/kg 1 07/07/09 14:45 98-82-85.5
p-Isopropyltoluene ND ug/kg 1 07/07/09 14:45 99-87-65.5
Methylene Chloride ND ug/kg 1 07/07/09 14:45 75-09-221.9
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/07/09 14:45 108-10-154.7
Methyl-tert-butyl ether ND ug/kg 1 07/07/09 14:45 1634-04-45.5
Naphthalene ND ug/kg 1 07/07/09 14:45 91-20-35.5
n-Propylbenzene ND ug/kg 1 07/07/09 14:45 103-65-15.5
Styrene ND ug/kg 1 07/07/09 14:45 100-42-55.5
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/07/09 14:45 630-20-65.5
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/07/09 14:45 79-34-55.5
Tetrachloroethene ND ug/kg 1 07/07/09 14:45 127-18-45.5
Toluene ND ug/kg 1 07/07/09 14:45 108-88-35.5
1,2,3-Trichlorobenzene ND ug/kg 1 07/07/09 14:45 87-61-65.5
1,2,4-Trichlorobenzene ND ug/kg 1 07/07/09 14:45 120-82-15.5
1,1,1-Trichloroethane ND ug/kg 1 07/07/09 14:45 71-55-65.5
1,1,2-Trichloroethane ND ug/kg 1 07/07/09 14:45 79-00-55.5
Trichloroethene ND ug/kg 1 07/07/09 14:45 79-01-65.5
Trichlorofluoromethane ND ug/kg 1 07/07/09 14:45 75-69-45.5
1,2,3-Trichloropropane ND ug/kg 1 07/07/09 14:45 96-18-45.5
1,2,4-Trimethylbenzene ND ug/kg 1 07/07/09 14:45 95-63-65.5
1,3,5-Trimethylbenzene ND ug/kg 1 07/07/09 14:45 108-67-85.5
Vinyl acetate ND ug/kg 1 07/07/09 14:45 108-05-454.7
Vinyl chloride ND ug/kg 1 07/07/09 14:45 75-01-410.9
Xylene (Total)ND ug/kg 1 07/07/09 14:45 1330-20-710.9
m&p-Xylene ND ug/kg 1 07/07/09 14:45 1330-20-710.9
o-Xylene ND ug/kg 1 07/07/09 14:45 95-47-65.5
Dibromofluoromethane (S)101 %1 07/07/09 14:45 1868-53-779-116
Toluene-d8 (S)99 %1 07/07/09 14:45 2037-26-588-110
4-Bromofluorobenzene (S)97 %1 07/07/09 14:45 460-00-474-115
1,2-Dichloroethane-d4 (S)100 %1 07/07/09 14:45 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 6.7 %1 07/06/09 12:340.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 55 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB26-06-09 Lab ID:9247665020 Collected:06/30/09 16:25 Received:06/30/09 18:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 19.9 mg/kg 1 07/14/09 17:05 68334-30-507/09/09 15:305.3
n-Pentacosane (S)82 %1 07/14/09 17:05 629-99-207/09/09 15:3050-135
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/03/09 00:08 8006-61-907/02/09 15:065.3
4-Bromofluorobenzene (S)89 %1 07/03/09 00:08 460-00-407/02/09 15:0650-135
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 5.0 %1 07/06/09 12:350.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 56 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB27-06-09 Lab ID:9247665021 Collected:06/30/09 16:40 Received:07/01/09 10:55 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 56.2 mg/kg 1 07/14/09 17:05 68334-30-507/09/09 15:307.0
n-Pentacosane (S)58 %1 07/14/09 17:05 629-99-207/09/09 15:3050-135
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/03/09 00:31 8006-61-907/02/09 15:068.6
4-Bromofluorobenzene (S)94 %1 07/03/09 00:31 460-00-407/02/09 15:0650-135
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 28.4 %1 07/06/09 12:350.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 57 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-EQUIP RINSATE-06-
09
Lab ID:9247665022 Collected:06/30/09 14:20 Received:07/01/09 10:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
HEM, Oil and Grease Analytical Method: EPA 1664A
Oil and Grease ND mg/L 1 07/16/09 11:405.0
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3510
Diesel Components ND mg/L 1 07/09/09 22:46 68334-30-507/07/09 13:300.10
n-Pentacosane (S)87 %1 07/09/09 22:46 629-99-207/07/09 13:3050-135
Gasoline Range Organics Analytical Method: EPA 5030/8015 Mod.
Gasoline Range Organics ND mg/L 1 07/14/09 17:31 8006-61-90.080
4-Bromofluorobenzene (S)83 %1 07/14/09 17:31 460-00-450-150
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Antimony ND ug/L 1 07/02/09 22:16 7440-36-007/02/09 11:005.0
Arsenic ND ug/L 1 07/02/09 22:16 7440-38-207/02/09 11:005.0
Beryllium ND ug/L 1 07/02/09 22:16 7440-41-707/02/09 11:001.0
Cadmium ND ug/L 1 07/02/09 22:16 7440-43-907/02/09 11:001.0
Chromium ND ug/L 1 07/02/09 22:16 7440-47-307/02/09 11:005.0
Copper ND ug/L 1 07/02/09 22:16 7440-50-807/02/09 11:005.0
Lead ND ug/L 1 07/02/09 22:16 7439-92-107/02/09 11:005.0
Manganese ND ug/L 1 07/02/09 22:16 7439-96-507/02/09 11:005.0
Nickel ND ug/L 1 07/02/09 22:16 7440-02-007/02/09 11:005.0
Selenium ND ug/L 1 07/02/09 22:16 7782-49-207/02/09 11:0010.0
Silver ND ug/L 1 07/02/09 22:16 7440-22-407/02/09 11:005.0
Thallium ND ug/L 1 07/02/09 22:16 7440-28-007/02/09 11:0010.0
Zinc ND ug/L 1 07/02/09 22:16 7440-66-607/02/09 11:0010.0
245.1 Mercury Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Mercury ND ug/L 1 07/02/09 18:02 7439-97-607/02/09 11:000.20
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 07/13/09 22:02 83-32-907/06/09 12:0011.6
Acenaphthylene ND ug/L 1 07/13/09 22:02 208-96-807/06/09 12:0011.6
Aniline ND ug/L 1 07/13/09 22:02 62-53-307/06/09 12:0011.6
Anthracene ND ug/L 1 07/13/09 22:02 120-12-707/06/09 12:0011.6
Benzo(a)anthracene ND ug/L 1 07/13/09 22:02 56-55-307/06/09 12:0011.6
Benzo(a)pyrene ND ug/L 1 07/13/09 22:02 50-32-807/06/09 12:0011.6
Benzo(b)fluoranthene ND ug/L 1 07/13/09 22:02 205-99-207/06/09 12:0011.6
Benzo(g,h,i)perylene ND ug/L 1 07/13/09 22:02 191-24-207/06/09 12:0011.6
Benzo(k)fluoranthene ND ug/L 1 07/13/09 22:02 207-08-907/06/09 12:0011.6
Benzoic Acid ND ug/L 1 07/13/09 22:02 65-85-007/06/09 12:0058.1
Benzyl alcohol ND ug/L 1 07/13/09 22:02 100-51-607/06/09 12:0023.3
4-Bromophenylphenyl ether ND ug/L 1 07/13/09 22:02 101-55-307/06/09 12:0011.6
Butylbenzylphthalate ND ug/L 1 07/13/09 22:02 85-68-707/06/09 12:0011.6
4-Chloro-3-methylphenol ND ug/L 1 07/13/09 22:02 59-50-707/06/09 12:0023.3
4-Chloroaniline ND ug/L 1 07/13/09 22:02 106-47-807/06/09 12:0058.1
bis(2-Chloroethoxy)methane ND ug/L 1 07/13/09 22:02 111-91-107/06/09 12:0011.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 58 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-EQUIP RINSATE-06-
09
Lab ID:9247665022 Collected:06/30/09 14:20 Received:07/01/09 10:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
bis(2-Chloroethyl) ether ND ug/L 1 07/13/09 22:02 111-44-407/06/09 12:0011.6
bis(2-Chloroisopropyl) ether ND ug/L 1 07/13/09 22:02 108-60-107/06/09 12:0011.6
2-Chloronaphthalene ND ug/L 1 07/13/09 22:02 91-58-707/06/09 12:0011.6
2-Chlorophenol ND ug/L 1 07/13/09 22:02 95-57-807/06/09 12:0011.6
4-Chlorophenylphenyl ether ND ug/L 1 07/13/09 22:02 7005-72-307/06/09 12:0011.6
Chrysene ND ug/L 1 07/13/09 22:02 218-01-907/06/09 12:0011.6
Dibenz(a,h)anthracene ND ug/L 1 07/13/09 22:02 53-70-307/06/09 12:0011.6
Dibenzofuran ND ug/L 1 07/13/09 22:02 132-64-907/06/09 12:0011.6
1,2-Dichlorobenzene ND ug/L 1 07/13/09 22:02 95-50-107/06/09 12:0011.6
1,3-Dichlorobenzene ND ug/L 1 07/13/09 22:02 541-73-107/06/09 12:0011.6
1,4-Dichlorobenzene ND ug/L 1 07/13/09 22:02 106-46-707/06/09 12:0011.6
3,3'-Dichlorobenzidine ND ug/L 1 07/13/09 22:02 91-94-107/06/09 12:0058.1
2,4-Dichlorophenol ND ug/L 1 07/13/09 22:02 120-83-207/06/09 12:0011.6
Diethylphthalate ND ug/L 1 07/13/09 22:02 84-66-207/06/09 12:0011.6
2,4-Dimethylphenol ND ug/L 1 07/13/09 22:02 105-67-907/06/09 12:0011.6
Dimethylphthalate ND ug/L 1 07/13/09 22:02 131-11-307/06/09 12:0011.6
Di-n-butylphthalate ND ug/L 1 07/13/09 22:02 84-74-207/06/09 12:0011.6
4,6-Dinitro-2-methylphenol ND ug/L 1 07/13/09 22:02 534-52-107/06/09 12:0023.3
2,4-Dinitrophenol ND ug/L 1 07/13/09 22:02 51-28-507/06/09 12:0058.1
2,4-Dinitrotoluene ND ug/L 1 07/13/09 22:02 121-14-207/06/09 12:0011.6
2,6-Dinitrotoluene ND ug/L 1 07/13/09 22:02 606-20-207/06/09 12:0011.6
Di-n-octylphthalate ND ug/L 1 07/13/09 22:02 117-84-007/06/09 12:0011.6
1,2-Diphenylhydrazine ND ug/L 1 07/13/09 22:02 122-66-707/06/09 12:0011.6
bis(2-Ethylhexyl)phthalate ND ug/L 1 07/13/09 22:02 117-81-707/06/09 12:0011.6
Fluoranthene ND ug/L 1 07/13/09 22:02 206-44-007/06/09 12:0011.6
Fluorene ND ug/L 1 07/13/09 22:02 86-73-707/06/09 12:0011.6
Hexachloro-1,3-butadiene ND ug/L 1 07/13/09 22:02 87-68-307/06/09 12:0011.6
Hexachlorobenzene ND ug/L 1 07/13/09 22:02 118-74-107/06/09 12:0011.6
Hexachlorocyclopentadiene ND ug/L 1 07/13/09 22:02 77-47-407/06/09 12:0011.6
Hexachloroethane ND ug/L 1 07/13/09 22:02 67-72-107/06/09 12:0011.6
Indeno(1,2,3-cd)pyrene ND ug/L 1 07/13/09 22:02 193-39-507/06/09 12:0011.6
Isophorone ND ug/L 1 07/13/09 22:02 78-59-107/06/09 12:0011.6
1-Methylnaphthalene ND ug/L 1 07/13/09 22:02 90-12-007/06/09 12:0011.6
2-Methylnaphthalene ND ug/L 1 07/13/09 22:02 91-57-607/06/09 12:0011.6
2-Methylphenol(o-Cresol)ND ug/L 1 07/13/09 22:02 95-48-707/06/09 12:0011.6
3&4-Methylphenol(m&p Cresol)ND ug/L 1 07/13/09 22:0207/06/09 12:0011.6
Naphthalene ND ug/L 1 07/13/09 22:02 91-20-307/06/09 12:0011.6
2-Nitroaniline ND ug/L 1 07/13/09 22:02 88-74-407/06/09 12:0058.1
3-Nitroaniline ND ug/L 1 07/13/09 22:02 99-09-207/06/09 12:0058.1
4-Nitroaniline ND ug/L 1 07/13/09 22:02 100-01-607/06/09 12:0058.1
Nitrobenzene ND ug/L 1 07/13/09 22:02 98-95-307/06/09 12:0011.6
2-Nitrophenol ND ug/L 1 07/13/09 22:02 88-75-507/06/09 12:0011.6
4-Nitrophenol ND ug/L 1 07/13/09 22:02 100-02-707/06/09 12:0058.1
N-Nitrosodimethylamine ND ug/L 1 07/13/09 22:02 62-75-907/06/09 12:0011.6
N-Nitroso-di-n-propylamine ND ug/L 1 07/13/09 22:02 621-64-707/06/09 12:0011.6
N-Nitrosodiphenylamine ND ug/L 1 07/13/09 22:02 86-30-607/06/09 12:0011.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 59 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-EQUIP RINSATE-06-
09
Lab ID:9247665022 Collected:06/30/09 14:20 Received:07/01/09 10:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Pentachlorophenol ND ug/L 1 07/13/09 22:02 87-86-507/06/09 12:0058.1
Phenanthrene ND ug/L 1 07/13/09 22:02 85-01-807/06/09 12:0011.6
Phenol ND ug/L 1 07/13/09 22:02 108-95-207/06/09 12:0011.6
Pyrene ND ug/L 1 07/13/09 22:02 129-00-007/06/09 12:0011.6
1,2,4-Trichlorobenzene ND ug/L 1 07/13/09 22:02 120-82-107/06/09 12:0011.6
2,4,5-Trichlorophenol ND ug/L 1 07/13/09 22:02 95-95-407/06/09 12:0011.6
2,4,6-Trichlorophenol ND ug/L 1 07/13/09 22:02 88-06-207/06/09 12:0011.6
Nitrobenzene-d5 (S)67 %1 07/13/09 22:02 4165-60-007/06/09 12:0030-150
2-Fluorobiphenyl (S)66 %1 07/13/09 22:02 321-60-807/06/09 12:0030-150
Terphenyl-d14 (S)88 %1 07/13/09 22:02 1718-51-007/06/09 12:0030-150
Phenol-d6 (S)27 %1 07/13/09 22:02 13127-88-307/06/09 12:0025-150
2-Fluorophenol (S)38 %1 07/13/09 22:02 367-12-407/06/09 12:0025-150
2,4,6-Tribromophenol (S)69 %1 07/13/09 22:02 118-79-607/06/09 12:0025-150
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 07/07/09 23:36 67-64-125.0
Benzene ND ug/L 1 07/07/09 23:36 71-43-21.0
Bromobenzene ND ug/L 1 07/07/09 23:36 108-86-11.0
Bromochloromethane ND ug/L 1 07/07/09 23:36 74-97-51.0
Bromodichloromethane ND ug/L 1 07/07/09 23:36 75-27-41.0
Bromoform ND ug/L 1 07/07/09 23:36 75-25-21.0
Bromomethane ND ug/L 1 07/07/09 23:36 74-83-95.0
2-Butanone (MEK)ND ug/L 1 07/07/09 23:36 78-93-35.0
Carbon tetrachloride ND ug/L 1 07/07/09 23:36 56-23-51.0
Chlorobenzene ND ug/L 1 07/07/09 23:36 108-90-71.0
Chloroethane ND ug/L 1 07/07/09 23:36 75-00-31.0
Chloroform ND ug/L 1 07/07/09 23:36 67-66-31.0
Chloromethane ND ug/L 1 07/07/09 23:36 74-87-31.0
2-Chlorotoluene ND ug/L 1 07/07/09 23:36 95-49-81.0
4-Chlorotoluene ND ug/L 1 07/07/09 23:36 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 07/07/09 23:36 96-12-83.0
Dibromochloromethane ND ug/L 1 07/07/09 23:36 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 07/07/09 23:36 106-93-41.0
Dibromomethane ND ug/L 1 07/07/09 23:36 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 07/07/09 23:36 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 07/07/09 23:36 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 07/07/09 23:36 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 07/07/09 23:36 75-71-81.0
1,1-Dichloroethane ND ug/L 1 07/07/09 23:36 75-34-31.0
1,2-Dichloroethane ND ug/L 1 07/07/09 23:36 107-06-21.0
1,1-Dichloroethene ND ug/L 1 07/07/09 23:36 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 07/07/09 23:36 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 07/07/09 23:36 156-60-51.0
1,2-Dichloropropane ND ug/L 1 07/07/09 23:36 78-87-51.0
1,3-Dichloropropane ND ug/L 1 07/07/09 23:36 142-28-91.0
2,2-Dichloropropane ND ug/L 1 07/07/09 23:36 594-20-71.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 60 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-EQUIP RINSATE-06-
09
Lab ID:9247665022 Collected:06/30/09 14:20 Received:07/01/09 10:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
1,1-Dichloropropene ND ug/L 1 07/07/09 23:36 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 07/07/09 23:36 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 07/07/09 23:36 10061-02-61.0
Diisopropyl ether ND ug/L 1 07/07/09 23:36 108-20-31.0
Ethylbenzene ND ug/L 1 07/07/09 23:36 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 07/07/09 23:36 87-68-31.0
2-Hexanone ND ug/L 1 07/07/09 23:36 591-78-65.0
p-Isopropyltoluene ND ug/L 1 07/07/09 23:36 99-87-61.0
Methylene Chloride ND ug/L 1 07/07/09 23:36 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 07/07/09 23:36 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 07/07/09 23:36 1634-04-41.0
Naphthalene ND ug/L 1 07/07/09 23:36 91-20-31.0
Styrene ND ug/L 1 07/07/09 23:36 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 07/07/09 23:36 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 07/07/09 23:36 79-34-51.0
Tetrachloroethene ND ug/L 1 07/07/09 23:36 127-18-41.0
Toluene ND ug/L 1 07/07/09 23:36 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 07/07/09 23:36 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 07/07/09 23:36 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 07/07/09 23:36 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 07/07/09 23:36 79-00-51.0
Trichloroethene ND ug/L 1 07/07/09 23:36 79-01-61.0
Trichlorofluoromethane ND ug/L 1 07/07/09 23:36 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 07/07/09 23:36 96-18-41.0
Vinyl acetate ND ug/L 1 07/07/09 23:36 108-05-42.0
Vinyl chloride ND ug/L 1 07/07/09 23:36 75-01-41.0
m&p-Xylene ND ug/L 1 07/07/09 23:36 1330-20-72.0
o-Xylene ND ug/L 1 07/07/09 23:36 95-47-61.0
4-Bromofluorobenzene (S)95 %1 07/07/09 23:36 460-00-487-109
Dibromofluoromethane (S)110 %1 07/07/09 23:36 1868-53-785-115
1,2-Dichloroethane-d4 (S)108 %1 07/07/09 23:36 17060-07-079-120
Toluene-d8 (S)102 %1 07/07/09 23:36 2037-26-570-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 61 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TRIP BLANK 1-06-09 Lab ID:9247665023 Collected:06/30/09 00:00 Received:07/01/09 10:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 07/08/09 11:57 67-64-125.0
Benzene ND ug/L 1 07/08/09 11:57 71-43-21.0
Bromobenzene ND ug/L 1 07/08/09 11:57 108-86-11.0
Bromochloromethane ND ug/L 1 07/08/09 11:57 74-97-51.0
Bromodichloromethane ND ug/L 1 07/08/09 11:57 75-27-41.0
Bromoform ND ug/L 1 07/08/09 11:57 75-25-21.0
Bromomethane ND ug/L 1 07/08/09 11:57 74-83-95.0
2-Butanone (MEK)ND ug/L 1 07/08/09 11:57 78-93-35.0
Carbon tetrachloride ND ug/L 1 07/08/09 11:57 56-23-51.0
Chlorobenzene ND ug/L 1 07/08/09 11:57 108-90-71.0
Chloroethane ND ug/L 1 07/08/09 11:57 75-00-31.0
Chloroform ND ug/L 1 07/08/09 11:57 67-66-31.0
Chloromethane ND ug/L 1 07/08/09 11:57 74-87-31.0
2-Chlorotoluene ND ug/L 1 07/08/09 11:57 95-49-81.0
4-Chlorotoluene ND ug/L 1 07/08/09 11:57 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 07/08/09 11:57 96-12-83.0
Dibromochloromethane ND ug/L 1 07/08/09 11:57 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 07/08/09 11:57 106-93-41.0
Dibromomethane ND ug/L 1 07/08/09 11:57 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 07/08/09 11:57 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 07/08/09 11:57 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 07/08/09 11:57 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 07/08/09 11:57 75-71-81.0
1,1-Dichloroethane ND ug/L 1 07/08/09 11:57 75-34-31.0
1,2-Dichloroethane ND ug/L 1 07/08/09 11:57 107-06-21.0
1,1-Dichloroethene ND ug/L 1 07/08/09 11:57 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 07/08/09 11:57 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 07/08/09 11:57 156-60-51.0
1,2-Dichloropropane ND ug/L 1 07/08/09 11:57 78-87-51.0
1,3-Dichloropropane ND ug/L 1 07/08/09 11:57 142-28-91.0
2,2-Dichloropropane ND ug/L 1 07/08/09 11:57 594-20-71.0
1,1-Dichloropropene ND ug/L 1 07/08/09 11:57 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 07/08/09 11:57 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 07/08/09 11:57 10061-02-61.0
Diisopropyl ether ND ug/L 1 07/08/09 11:57 108-20-31.0
Ethylbenzene ND ug/L 1 07/08/09 11:57 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 07/08/09 11:57 87-68-31.0
2-Hexanone ND ug/L 1 07/08/09 11:57 591-78-65.0
p-Isopropyltoluene ND ug/L 1 07/08/09 11:57 99-87-61.0
Methylene Chloride ND ug/L 1 07/08/09 11:57 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 07/08/09 11:57 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 07/08/09 11:57 1634-04-41.0
Naphthalene ND ug/L 1 07/08/09 11:57 91-20-31.0
Styrene ND ug/L 1 07/08/09 11:57 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 07/08/09 11:57 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 07/08/09 11:57 79-34-51.0
Tetrachloroethene ND ug/L 1 07/08/09 11:57 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 62 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TRIP BLANK 1-06-09 Lab ID:9247665023 Collected:06/30/09 00:00 Received:07/01/09 10:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 07/08/09 11:57 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 07/08/09 11:57 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 07/08/09 11:57 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 07/08/09 11:57 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 07/08/09 11:57 79-00-51.0
Trichloroethene ND ug/L 1 07/08/09 11:57 79-01-61.0
Trichlorofluoromethane ND ug/L 1 07/08/09 11:57 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 07/08/09 11:57 96-18-41.0
Vinyl acetate ND ug/L 1 07/08/09 11:57 108-05-42.0
Vinyl chloride ND ug/L 1 07/08/09 11:57 75-01-41.0
m&p-Xylene ND ug/L 1 07/08/09 11:57 1330-20-72.0
o-Xylene ND ug/L 1 07/08/09 11:57 95-47-61.0
4-Bromofluorobenzene (S)97 %1 07/08/09 11:57 460-00-487-109
Dibromofluoromethane (S)107 %1 07/08/09 11:57 1868-53-785-115
1,2-Dichloroethane-d4 (S)102 %1 07/08/09 11:57 17060-07-079-120
Toluene-d8 (S)102 %1 07/08/09 11:57 2037-26-570-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 63 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TRIP BLANK 2-06-09 Lab ID:9247665024 Collected:06/30/09 00:00 Received:07/01/09 10:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 07/07/09 15:06 67-64-125.0
Benzene ND ug/L 1 07/07/09 15:06 71-43-21.0
Bromobenzene ND ug/L 1 07/07/09 15:06 108-86-11.0
Bromochloromethane ND ug/L 1 07/07/09 15:06 74-97-51.0
Bromodichloromethane ND ug/L 1 07/07/09 15:06 75-27-41.0
Bromoform ND ug/L 1 07/07/09 15:06 75-25-21.0
Bromomethane ND ug/L 1 07/07/09 15:06 74-83-95.0
2-Butanone (MEK)ND ug/L 1 07/07/09 15:06 78-93-35.0
Carbon tetrachloride ND ug/L 1 07/07/09 15:06 56-23-51.0
Chlorobenzene ND ug/L 1 07/07/09 15:06 108-90-71.0
Chloroethane ND ug/L 1 07/07/09 15:06 75-00-31.0
Chloroform ND ug/L 1 07/07/09 15:06 67-66-31.0
Chloromethane ND ug/L 1 07/07/09 15:06 74-87-31.0
2-Chlorotoluene ND ug/L 1 07/07/09 15:06 95-49-81.0
4-Chlorotoluene ND ug/L 1 07/07/09 15:06 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 07/07/09 15:06 96-12-83.0
Dibromochloromethane ND ug/L 1 07/07/09 15:06 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 07/07/09 15:06 106-93-41.0
Dibromomethane ND ug/L 1 07/07/09 15:06 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 07/07/09 15:06 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 07/07/09 15:06 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 07/07/09 15:06 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 07/07/09 15:06 75-71-81.0
1,1-Dichloroethane ND ug/L 1 07/07/09 15:06 75-34-31.0
1,2-Dichloroethane ND ug/L 1 07/07/09 15:06 107-06-21.0
1,1-Dichloroethene ND ug/L 1 07/07/09 15:06 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 07/07/09 15:06 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 07/07/09 15:06 156-60-51.0
1,2-Dichloropropane ND ug/L 1 07/07/09 15:06 78-87-51.0
1,3-Dichloropropane ND ug/L 1 07/07/09 15:06 142-28-91.0
2,2-Dichloropropane ND ug/L 1 07/07/09 15:06 594-20-71.0
1,1-Dichloropropene ND ug/L 1 07/07/09 15:06 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 07/07/09 15:06 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 07/07/09 15:06 10061-02-61.0
Diisopropyl ether ND ug/L 1 07/07/09 15:06 108-20-31.0
Ethylbenzene ND ug/L 1 07/07/09 15:06 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 07/07/09 15:06 87-68-31.0
2-Hexanone ND ug/L 1 07/07/09 15:06 591-78-65.0
p-Isopropyltoluene ND ug/L 1 07/07/09 15:06 99-87-61.0
Methylene Chloride ND ug/L 1 07/07/09 15:06 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 07/07/09 15:06 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 07/07/09 15:06 1634-04-41.0
Naphthalene ND ug/L 1 07/07/09 15:06 91-20-31.0
Styrene ND ug/L 1 07/07/09 15:06 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 07/07/09 15:06 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 07/07/09 15:06 79-34-51.0
Tetrachloroethene ND ug/L 1 07/07/09 15:06 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 64 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TRIP BLANK 2-06-09 Lab ID:9247665024 Collected:06/30/09 00:00 Received:07/01/09 10:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 07/07/09 15:06 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 07/07/09 15:06 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 07/07/09 15:06 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 07/07/09 15:06 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 07/07/09 15:06 79-00-51.0
Trichloroethene ND ug/L 1 07/07/09 15:06 79-01-61.0
Trichlorofluoromethane ND ug/L 1 07/07/09 15:06 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 07/07/09 15:06 96-18-41.0
Vinyl acetate ND ug/L 1 07/07/09 15:06 108-05-42.0
Vinyl chloride ND ug/L 1 07/07/09 15:06 75-01-41.0
m&p-Xylene ND ug/L 1 07/07/09 15:06 1330-20-72.0
o-Xylene ND ug/L 1 07/07/09 15:06 95-47-61.0
4-Bromofluorobenzene (S)99 %1 07/07/09 15:06 460-00-487-109
Dibromofluoromethane (S)107 %1 07/07/09 15:06 1868-53-785-115
1,2-Dichloroethane-d4 (S)105 %1 07/07/09 15:06 17060-07-079-120
Toluene-d8 (S)101 %1 07/07/09 15:06 2037-26-570-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 65 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TRIP BLANK 3-06-09 Lab ID:9247665025 Collected:06/30/09 00:00 Received:07/01/09 10:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 07/07/09 15:25 67-64-125.0
Benzene ND ug/L 1 07/07/09 15:25 71-43-21.0
Bromobenzene ND ug/L 1 07/07/09 15:25 108-86-11.0
Bromochloromethane ND ug/L 1 07/07/09 15:25 74-97-51.0
Bromodichloromethane ND ug/L 1 07/07/09 15:25 75-27-41.0
Bromoform ND ug/L 1 07/07/09 15:25 75-25-21.0
Bromomethane ND ug/L 1 07/07/09 15:25 74-83-95.0
2-Butanone (MEK)ND ug/L 1 07/07/09 15:25 78-93-35.0
Carbon tetrachloride ND ug/L 1 07/07/09 15:25 56-23-51.0
Chlorobenzene ND ug/L 1 07/07/09 15:25 108-90-71.0
Chloroethane ND ug/L 1 07/07/09 15:25 75-00-31.0
Chloroform ND ug/L 1 07/07/09 15:25 67-66-31.0
Chloromethane ND ug/L 1 07/07/09 15:25 74-87-31.0
2-Chlorotoluene ND ug/L 1 07/07/09 15:25 95-49-81.0
4-Chlorotoluene ND ug/L 1 07/07/09 15:25 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 07/07/09 15:25 96-12-83.0
Dibromochloromethane ND ug/L 1 07/07/09 15:25 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 07/07/09 15:25 106-93-41.0
Dibromomethane ND ug/L 1 07/07/09 15:25 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 07/07/09 15:25 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 07/07/09 15:25 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 07/07/09 15:25 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 07/07/09 15:25 75-71-81.0
1,1-Dichloroethane ND ug/L 1 07/07/09 15:25 75-34-31.0
1,2-Dichloroethane ND ug/L 1 07/07/09 15:25 107-06-21.0
1,1-Dichloroethene ND ug/L 1 07/07/09 15:25 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 07/07/09 15:25 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 07/07/09 15:25 156-60-51.0
1,2-Dichloropropane ND ug/L 1 07/07/09 15:25 78-87-51.0
1,3-Dichloropropane ND ug/L 1 07/07/09 15:25 142-28-91.0
2,2-Dichloropropane ND ug/L 1 07/07/09 15:25 594-20-71.0
1,1-Dichloropropene ND ug/L 1 07/07/09 15:25 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 07/07/09 15:25 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 07/07/09 15:25 10061-02-61.0
Diisopropyl ether ND ug/L 1 07/07/09 15:25 108-20-31.0
Ethylbenzene ND ug/L 1 07/07/09 15:25 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 07/07/09 15:25 87-68-31.0
2-Hexanone ND ug/L 1 07/07/09 15:25 591-78-65.0
p-Isopropyltoluene ND ug/L 1 07/07/09 15:25 99-87-61.0
Methylene Chloride ND ug/L 1 07/07/09 15:25 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 07/07/09 15:25 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 07/07/09 15:25 1634-04-41.0
Naphthalene ND ug/L 1 07/07/09 15:25 91-20-31.0
Styrene ND ug/L 1 07/07/09 15:25 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 07/07/09 15:25 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 07/07/09 15:25 79-34-51.0
Tetrachloroethene ND ug/L 1 07/07/09 15:25 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 66 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TRIP BLANK 3-06-09 Lab ID:9247665025 Collected:06/30/09 00:00 Received:07/01/09 10:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 07/07/09 15:25 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 07/07/09 15:25 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 07/07/09 15:25 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 07/07/09 15:25 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 07/07/09 15:25 79-00-51.0
Trichloroethene ND ug/L 1 07/07/09 15:25 79-01-61.0
Trichlorofluoromethane ND ug/L 1 07/07/09 15:25 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 07/07/09 15:25 96-18-41.0
Vinyl acetate ND ug/L 1 07/07/09 15:25 108-05-42.0
Vinyl chloride ND ug/L 1 07/07/09 15:25 75-01-41.0
m&p-Xylene ND ug/L 1 07/07/09 15:25 1330-20-72.0
o-Xylene ND ug/L 1 07/07/09 15:25 95-47-61.0
4-Bromofluorobenzene (S)100 %1 07/07/09 15:25 460-00-487-109
Dibromofluoromethane (S)107 %1 07/07/09 15:25 1868-53-785-115
1,2-Dichloroethane-d4 (S)105 %1 07/07/09 15:25 17060-07-079-120
Toluene-d8 (S)102 %1 07/07/09 15:25 2037-26-570-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 67 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TW3-SS1-07-09 Lab ID:9247665026 Collected:07/01/09 11:45 Received:07/01/09 15:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Lead 6.9 mg/kg 5 07/09/09 15:38 7439-92-1 R107/07/09 14:202.9
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/08/09 02:17 67-64-196.3
Benzene ND ug/kg 1 07/08/09 02:17 71-43-24.8
Bromobenzene ND ug/kg 1 07/08/09 02:17 108-86-14.8
Bromochloromethane ND ug/kg 1 07/08/09 02:17 74-97-54.8
Bromodichloromethane ND ug/kg 1 07/08/09 02:17 75-27-44.8
Bromoform ND ug/kg 1 07/08/09 02:17 75-25-24.8
Bromomethane ND ug/kg 1 07/08/09 02:17 74-83-99.6
2-Butanone (MEK)ND ug/kg 1 07/08/09 02:17 78-93-396.3
n-Butylbenzene ND ug/kg 1 07/08/09 02:17 104-51-84.8
sec-Butylbenzene ND ug/kg 1 07/08/09 02:17 135-98-84.8
tert-Butylbenzene ND ug/kg 1 07/08/09 02:17 98-06-64.8
Carbon tetrachloride ND ug/kg 1 07/08/09 02:17 56-23-54.8
Chlorobenzene ND ug/kg 1 07/08/09 02:17 108-90-74.8
Chloroethane ND ug/kg 1 07/08/09 02:17 75-00-39.6
Chloroform ND ug/kg 1 07/08/09 02:17 67-66-34.8
Chloromethane ND ug/kg 1 07/08/09 02:17 74-87-39.6
2-Chlorotoluene ND ug/kg 1 07/08/09 02:17 95-49-84.8
4-Chlorotoluene ND ug/kg 1 07/08/09 02:17 106-43-44.8
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/08/09 02:17 96-12-84.8
Dibromochloromethane ND ug/kg 1 07/08/09 02:17 124-48-14.8
1,2-Dibromoethane (EDB)ND ug/kg 1 07/08/09 02:17 106-93-44.8
Dibromomethane ND ug/kg 1 07/08/09 02:17 74-95-34.8
1,2-Dichlorobenzene ND ug/kg 1 07/08/09 02:17 95-50-14.8
1,3-Dichlorobenzene ND ug/kg 1 07/08/09 02:17 541-73-14.8
1,4-Dichlorobenzene ND ug/kg 1 07/08/09 02:17 106-46-74.8
Dichlorodifluoromethane ND ug/kg 1 07/08/09 02:17 75-71-89.6
1,1-Dichloroethane ND ug/kg 1 07/08/09 02:17 75-34-34.8
1,2-Dichloroethane ND ug/kg 1 07/08/09 02:17 107-06-24.8
1,1-Dichloroethene ND ug/kg 1 07/08/09 02:17 75-35-44.8
cis-1,2-Dichloroethene ND ug/kg 1 07/08/09 02:17 156-59-24.8
trans-1,2-Dichloroethene ND ug/kg 1 07/08/09 02:17 156-60-54.8
1,2-Dichloropropane ND ug/kg 1 07/08/09 02:17 78-87-54.8
1,3-Dichloropropane ND ug/kg 1 07/08/09 02:17 142-28-94.8
2,2-Dichloropropane ND ug/kg 1 07/08/09 02:17 594-20-74.8
1,1-Dichloropropene ND ug/kg 1 07/08/09 02:17 563-58-64.8
cis-1,3-Dichloropropene ND ug/kg 1 07/08/09 02:17 10061-01-54.8
trans-1,3-Dichloropropene ND ug/kg 1 07/08/09 02:17 10061-02-64.8
Diisopropyl ether ND ug/kg 1 07/08/09 02:17 108-20-34.8
Ethylbenzene ND ug/kg 1 07/08/09 02:17 100-41-44.8
Hexachloro-1,3-butadiene ND ug/kg 1 07/08/09 02:17 87-68-34.8
2-Hexanone ND ug/kg 1 07/08/09 02:17 591-78-648.2
Isopropylbenzene (Cumene)ND ug/kg 1 07/08/09 02:17 98-82-84.8
p-Isopropyltoluene ND ug/kg 1 07/08/09 02:17 99-87-64.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 68 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TW3-SS1-07-09 Lab ID:9247665026 Collected:07/01/09 11:45 Received:07/01/09 15:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Methylene Chloride ND ug/kg 1 07/08/09 02:17 75-09-219.3
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/08/09 02:17 108-10-148.2
Methyl-tert-butyl ether ND ug/kg 1 07/08/09 02:17 1634-04-44.8
Naphthalene ND ug/kg 1 07/08/09 02:17 91-20-34.8
n-Propylbenzene ND ug/kg 1 07/08/09 02:17 103-65-14.8
Styrene ND ug/kg 1 07/08/09 02:17 100-42-54.8
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/08/09 02:17 630-20-64.8
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/08/09 02:17 79-34-54.8
Tetrachloroethene ND ug/kg 1 07/08/09 02:17 127-18-44.8
Toluene ND ug/kg 1 07/08/09 02:17 108-88-34.8
1,2,3-Trichlorobenzene ND ug/kg 1 07/08/09 02:17 87-61-64.8
1,2,4-Trichlorobenzene ND ug/kg 1 07/08/09 02:17 120-82-14.8
1,1,1-Trichloroethane ND ug/kg 1 07/08/09 02:17 71-55-64.8
1,1,2-Trichloroethane ND ug/kg 1 07/08/09 02:17 79-00-54.8
Trichloroethene ND ug/kg 1 07/08/09 02:17 79-01-64.8
Trichlorofluoromethane ND ug/kg 1 07/08/09 02:17 75-69-44.8
1,2,3-Trichloropropane ND ug/kg 1 07/08/09 02:17 96-18-44.8
1,2,4-Trimethylbenzene ND ug/kg 1 07/08/09 02:17 95-63-64.8
1,3,5-Trimethylbenzene ND ug/kg 1 07/08/09 02:17 108-67-84.8
Vinyl acetate ND ug/kg 1 07/08/09 02:17 108-05-448.2
Vinyl chloride ND ug/kg 1 07/08/09 02:17 75-01-49.6
Xylene (Total)ND ug/kg 1 07/08/09 02:17 1330-20-79.6
m&p-Xylene ND ug/kg 1 07/08/09 02:17 1330-20-79.6
o-Xylene ND ug/kg 1 07/08/09 02:17 95-47-64.8
Dibromofluoromethane (S)99 %1 07/08/09 02:17 1868-53-779-116
Toluene-d8 (S)100 %1 07/08/09 02:17 2037-26-588-110
4-Bromofluorobenzene (S)99 %1 07/08/09 02:17 460-00-474-115
1,2-Dichloroethane-d4 (S)98 %1 07/08/09 02:17 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 20.9 %1 07/06/09 12:350.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 69 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TW3-SS2-07-09 Lab ID:9247665027 Collected:07/01/09 11:50 Received:07/01/09 15:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Lead 3.4 mg/kg 1 07/09/09 00:13 7439-92-107/07/09 14:200.43
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/08/09 03:12 67-64-190.4
Benzene ND ug/kg 1 07/08/09 03:12 71-43-24.5
Bromobenzene ND ug/kg 1 07/08/09 03:12 108-86-14.5
Bromochloromethane ND ug/kg 1 07/08/09 03:12 74-97-54.5
Bromodichloromethane ND ug/kg 1 07/08/09 03:12 75-27-44.5
Bromoform ND ug/kg 1 07/08/09 03:12 75-25-24.5
Bromomethane ND ug/kg 1 07/08/09 03:12 74-83-99.0
2-Butanone (MEK)ND ug/kg 1 07/08/09 03:12 78-93-390.4
n-Butylbenzene ND ug/kg 1 07/08/09 03:12 104-51-84.5
sec-Butylbenzene ND ug/kg 1 07/08/09 03:12 135-98-84.5
tert-Butylbenzene ND ug/kg 1 07/08/09 03:12 98-06-64.5
Carbon tetrachloride ND ug/kg 1 07/08/09 03:12 56-23-54.5
Chlorobenzene ND ug/kg 1 07/08/09 03:12 108-90-74.5
Chloroethane ND ug/kg 1 07/08/09 03:12 75-00-39.0
Chloroform ND ug/kg 1 07/08/09 03:12 67-66-34.5
Chloromethane ND ug/kg 1 07/08/09 03:12 74-87-39.0
2-Chlorotoluene ND ug/kg 1 07/08/09 03:12 95-49-84.5
4-Chlorotoluene ND ug/kg 1 07/08/09 03:12 106-43-44.5
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/08/09 03:12 96-12-84.5
Dibromochloromethane ND ug/kg 1 07/08/09 03:12 124-48-14.5
1,2-Dibromoethane (EDB)ND ug/kg 1 07/08/09 03:12 106-93-44.5
Dibromomethane ND ug/kg 1 07/08/09 03:12 74-95-34.5
1,2-Dichlorobenzene ND ug/kg 1 07/08/09 03:12 95-50-14.5
1,3-Dichlorobenzene ND ug/kg 1 07/08/09 03:12 541-73-14.5
1,4-Dichlorobenzene ND ug/kg 1 07/08/09 03:12 106-46-74.5
Dichlorodifluoromethane ND ug/kg 1 07/08/09 03:12 75-71-89.0
1,1-Dichloroethane ND ug/kg 1 07/08/09 03:12 75-34-34.5
1,2-Dichloroethane ND ug/kg 1 07/08/09 03:12 107-06-24.5
1,1-Dichloroethene ND ug/kg 1 07/08/09 03:12 75-35-44.5
cis-1,2-Dichloroethene ND ug/kg 1 07/08/09 03:12 156-59-24.5
trans-1,2-Dichloroethene ND ug/kg 1 07/08/09 03:12 156-60-54.5
1,2-Dichloropropane ND ug/kg 1 07/08/09 03:12 78-87-54.5
1,3-Dichloropropane ND ug/kg 1 07/08/09 03:12 142-28-94.5
2,2-Dichloropropane ND ug/kg 1 07/08/09 03:12 594-20-74.5
1,1-Dichloropropene ND ug/kg 1 07/08/09 03:12 563-58-64.5
cis-1,3-Dichloropropene ND ug/kg 1 07/08/09 03:12 10061-01-54.5
trans-1,3-Dichloropropene ND ug/kg 1 07/08/09 03:12 10061-02-64.5
Diisopropyl ether ND ug/kg 1 07/08/09 03:12 108-20-34.5
Ethylbenzene ND ug/kg 1 07/08/09 03:12 100-41-44.5
Hexachloro-1,3-butadiene ND ug/kg 1 07/08/09 03:12 87-68-34.5
2-Hexanone ND ug/kg 1 07/08/09 03:12 591-78-645.2
Isopropylbenzene (Cumene)ND ug/kg 1 07/08/09 03:12 98-82-84.5
p-Isopropyltoluene ND ug/kg 1 07/08/09 03:12 99-87-64.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 70 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TW3-SS2-07-09 Lab ID:9247665027 Collected:07/01/09 11:50 Received:07/01/09 15:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Methylene Chloride ND ug/kg 1 07/08/09 03:12 75-09-218.1
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/08/09 03:12 108-10-145.2
Methyl-tert-butyl ether ND ug/kg 1 07/08/09 03:12 1634-04-44.5
Naphthalene ND ug/kg 1 07/08/09 03:12 91-20-34.5
n-Propylbenzene ND ug/kg 1 07/08/09 03:12 103-65-14.5
Styrene ND ug/kg 1 07/08/09 03:12 100-42-54.5
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/08/09 03:12 630-20-64.5
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/08/09 03:12 79-34-54.5
Tetrachloroethene ND ug/kg 1 07/08/09 03:12 127-18-44.5
Toluene ND ug/kg 1 07/08/09 03:12 108-88-34.5
1,2,3-Trichlorobenzene ND ug/kg 1 07/08/09 03:12 87-61-64.5
1,2,4-Trichlorobenzene ND ug/kg 1 07/08/09 03:12 120-82-14.5
1,1,1-Trichloroethane ND ug/kg 1 07/08/09 03:12 71-55-64.5
1,1,2-Trichloroethane ND ug/kg 1 07/08/09 03:12 79-00-54.5
Trichloroethene ND ug/kg 1 07/08/09 03:12 79-01-64.5
Trichlorofluoromethane ND ug/kg 1 07/08/09 03:12 75-69-44.5
1,2,3-Trichloropropane ND ug/kg 1 07/08/09 03:12 96-18-44.5
1,2,4-Trimethylbenzene ND ug/kg 1 07/08/09 03:12 95-63-64.5
1,3,5-Trimethylbenzene ND ug/kg 1 07/08/09 03:12 108-67-84.5
Vinyl acetate ND ug/kg 1 07/08/09 03:12 108-05-445.2
Vinyl chloride ND ug/kg 1 07/08/09 03:12 75-01-49.0
Xylene (Total)ND ug/kg 1 07/08/09 03:12 1330-20-79.0
m&p-Xylene ND ug/kg 1 07/08/09 03:12 1330-20-79.0
o-Xylene ND ug/kg 1 07/08/09 03:12 95-47-64.5
Dibromofluoromethane (S)100 %1 07/08/09 03:12 1868-53-779-116
Toluene-d8 (S)98 %1 07/08/09 03:12 2037-26-588-110
4-Bromofluorobenzene (S)98 %1 07/08/09 03:12 460-00-474-115
1,2-Dichloroethane-d4 (S)98 %1 07/08/09 03:12 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 20.9 %1 07/06/09 12:350.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 71 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-DUPLICATE1-07-09 Lab ID:9247665028 Collected:07/01/09 00:00 Received:07/01/09 15:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Lead 4.1 mg/kg 1 07/09/09 00:19 7439-92-107/07/09 14:200.42
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 07/08/09 03:30 67-64-191.5
Benzene ND ug/kg 1 07/08/09 03:30 71-43-24.6
Bromobenzene ND ug/kg 1 07/08/09 03:30 108-86-14.6
Bromochloromethane ND ug/kg 1 07/08/09 03:30 74-97-54.6
Bromodichloromethane ND ug/kg 1 07/08/09 03:30 75-27-44.6
Bromoform ND ug/kg 1 07/08/09 03:30 75-25-24.6
Bromomethane ND ug/kg 1 07/08/09 03:30 74-83-99.2
2-Butanone (MEK)ND ug/kg 1 07/08/09 03:30 78-93-391.5
n-Butylbenzene ND ug/kg 1 07/08/09 03:30 104-51-84.6
sec-Butylbenzene ND ug/kg 1 07/08/09 03:30 135-98-84.6
tert-Butylbenzene ND ug/kg 1 07/08/09 03:30 98-06-64.6
Carbon tetrachloride ND ug/kg 1 07/08/09 03:30 56-23-54.6
Chlorobenzene ND ug/kg 1 07/08/09 03:30 108-90-74.6
Chloroethane ND ug/kg 1 07/08/09 03:30 75-00-39.2
Chloroform ND ug/kg 1 07/08/09 03:30 67-66-34.6
Chloromethane ND ug/kg 1 07/08/09 03:30 74-87-39.2
2-Chlorotoluene ND ug/kg 1 07/08/09 03:30 95-49-84.6
4-Chlorotoluene ND ug/kg 1 07/08/09 03:30 106-43-44.6
1,2-Dibromo-3-chloropropane ND ug/kg 1 07/08/09 03:30 96-12-84.6
Dibromochloromethane ND ug/kg 1 07/08/09 03:30 124-48-14.6
1,2-Dibromoethane (EDB)ND ug/kg 1 07/08/09 03:30 106-93-44.6
Dibromomethane ND ug/kg 1 07/08/09 03:30 74-95-34.6
1,2-Dichlorobenzene ND ug/kg 1 07/08/09 03:30 95-50-14.6
1,3-Dichlorobenzene ND ug/kg 1 07/08/09 03:30 541-73-14.6
1,4-Dichlorobenzene ND ug/kg 1 07/08/09 03:30 106-46-74.6
Dichlorodifluoromethane ND ug/kg 1 07/08/09 03:30 75-71-89.2
1,1-Dichloroethane ND ug/kg 1 07/08/09 03:30 75-34-34.6
1,2-Dichloroethane ND ug/kg 1 07/08/09 03:30 107-06-24.6
1,1-Dichloroethene ND ug/kg 1 07/08/09 03:30 75-35-44.6
cis-1,2-Dichloroethene ND ug/kg 1 07/08/09 03:30 156-59-24.6
trans-1,2-Dichloroethene ND ug/kg 1 07/08/09 03:30 156-60-54.6
1,2-Dichloropropane ND ug/kg 1 07/08/09 03:30 78-87-54.6
1,3-Dichloropropane ND ug/kg 1 07/08/09 03:30 142-28-94.6
2,2-Dichloropropane ND ug/kg 1 07/08/09 03:30 594-20-74.6
1,1-Dichloropropene ND ug/kg 1 07/08/09 03:30 563-58-64.6
cis-1,3-Dichloropropene ND ug/kg 1 07/08/09 03:30 10061-01-54.6
trans-1,3-Dichloropropene ND ug/kg 1 07/08/09 03:30 10061-02-64.6
Diisopropyl ether ND ug/kg 1 07/08/09 03:30 108-20-34.6
Ethylbenzene ND ug/kg 1 07/08/09 03:30 100-41-44.6
Hexachloro-1,3-butadiene ND ug/kg 1 07/08/09 03:30 87-68-34.6
2-Hexanone ND ug/kg 1 07/08/09 03:30 591-78-645.8
Isopropylbenzene (Cumene)ND ug/kg 1 07/08/09 03:30 98-82-84.6
p-Isopropyltoluene ND ug/kg 1 07/08/09 03:30 99-87-64.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 72 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-DUPLICATE1-07-09 Lab ID:9247665028 Collected:07/01/09 00:00 Received:07/01/09 15:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Methylene Chloride ND ug/kg 1 07/08/09 03:30 75-09-218.3
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 07/08/09 03:30 108-10-145.8
Methyl-tert-butyl ether ND ug/kg 1 07/08/09 03:30 1634-04-44.6
Naphthalene ND ug/kg 1 07/08/09 03:30 91-20-34.6
n-Propylbenzene ND ug/kg 1 07/08/09 03:30 103-65-14.6
Styrene ND ug/kg 1 07/08/09 03:30 100-42-54.6
1,1,1,2-Tetrachloroethane ND ug/kg 1 07/08/09 03:30 630-20-64.6
1,1,2,2-Tetrachloroethane ND ug/kg 1 07/08/09 03:30 79-34-54.6
Tetrachloroethene ND ug/kg 1 07/08/09 03:30 127-18-44.6
Toluene ND ug/kg 1 07/08/09 03:30 108-88-34.6
1,2,3-Trichlorobenzene ND ug/kg 1 07/08/09 03:30 87-61-64.6
1,2,4-Trichlorobenzene ND ug/kg 1 07/08/09 03:30 120-82-14.6
1,1,1-Trichloroethane ND ug/kg 1 07/08/09 03:30 71-55-64.6
1,1,2-Trichloroethane ND ug/kg 1 07/08/09 03:30 79-00-54.6
Trichloroethene ND ug/kg 1 07/08/09 03:30 79-01-64.6
Trichlorofluoromethane ND ug/kg 1 07/08/09 03:30 75-69-44.6
1,2,3-Trichloropropane ND ug/kg 1 07/08/09 03:30 96-18-44.6
1,2,4-Trimethylbenzene ND ug/kg 1 07/08/09 03:30 95-63-64.6
1,3,5-Trimethylbenzene ND ug/kg 1 07/08/09 03:30 108-67-84.6
Vinyl acetate ND ug/kg 1 07/08/09 03:30 108-05-445.8
Vinyl chloride ND ug/kg 1 07/08/09 03:30 75-01-49.2
Xylene (Total)ND ug/kg 1 07/08/09 03:30 1330-20-79.2
m&p-Xylene ND ug/kg 1 07/08/09 03:30 1330-20-79.2
o-Xylene ND ug/kg 1 07/08/09 03:30 95-47-64.6
Dibromofluoromethane (S)100 %1 07/08/09 03:30 1868-53-779-116
Toluene-d8 (S)100 %1 07/08/09 03:30 2037-26-588-110
4-Bromofluorobenzene (S)97 %1 07/08/09 03:30 460-00-474-115
1,2-Dichloroethane-d4 (S)99 %1 07/08/09 03:30 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 19.0 %1 07/06/09 12:360.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 73 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB18-07-09 Lab ID:9247665029 Collected:07/01/09 13:30 Received:07/01/09 15:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 769 mg/kg 4 07/15/09 10:21 68334-30-507/09/09 15:3024.3
n-Pentacosane (S)76 %4 07/15/09 10:21 629-99-207/09/09 15:3050-135
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/15/09 02:31 8006-61-907/02/09 15:066.2
4-Bromofluorobenzene (S)86 %1 07/15/09 02:31 460-00-407/02/09 15:0650-135
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 17.8 %1 07/06/09 12:360.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 74 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-DUPLICATE 2-07-09 Lab ID:9247665030 Collected:07/01/09 00:00 Received:07/01/09 15:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 590 mg/kg 2 07/16/09 15:41 68334-30-507/10/09 12:3011.6
n-Pentacosane (S)82 %2 07/16/09 15:41 629-99-207/10/09 12:3050-135
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/15/09 02:54 8006-61-907/02/09 15:065.2
4-Bromofluorobenzene (S)88 %1 07/15/09 02:54 460-00-407/02/09 15:0650-135
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 14.0 %1 07/06/09 12:360.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 75 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB17-07-09 Lab ID:9247665031 Collected:07/01/09 13:45 Received:07/01/09 15:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components ND mg/kg 1 07/21/09 10:07 68334-30-5 3g07/20/09 12:306.4
n-Pentacosane (S)77 %1 07/21/09 10:07 629-99-207/20/09 12:3050-135
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/15/09 03:18 8006-61-907/02/09 15:065.9
4-Bromofluorobenzene (S)83 %1 07/15/09 03:18 460-00-407/02/09 15:0650-135
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 21.8 %1 07/06/09 12:370.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 76 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB15-07-09 Lab ID:9247665032 Collected:07/01/09 13:55 Received:07/01/09 15:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components ND mg/kg 1 07/15/09 13:31 68334-30-507/10/09 12:306.8
n-Pentacosane (S)73 %1 07/15/09 13:31 629-99-207/10/09 12:3050-135
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/14/09 00:04 8006-61-907/02/09 15:066.2
4-Bromofluorobenzene (S)81 %1 07/14/09 00:04 460-00-407/02/09 15:0650-135
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 26.7 %1 07/06/09 12:370.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 77 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB14-07-09 Lab ID:9247665033 Collected:07/01/09 14:05 Received:07/01/09 15:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 181 mg/kg 1 07/15/09 13:31 68334-30-507/10/09 12:306.3
n-Pentacosane (S)196 %1 07/15/09 13:31 629-99-2 4g07/10/09 12:3050-135
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/03/09 06:01 8006-61-907/02/09 15:196.0
4-Bromofluorobenzene (S)95 %1 07/03/09 06:01 460-00-407/02/09 15:1950-135
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 20.5 %1 07/06/09 12:370.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 78 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-SB13-07-09 Lab ID:9247665034 Collected:07/01/09 14:15 Received:07/01/09 15:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components ND mg/kg 1 07/15/09 14:00 68334-30-5 P307/10/09 12:3032.1
n-Pentacosane (S)0 %1 07/15/09 14:00 629-99-2 S407/10/09 12:3050-135
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 1 07/03/09 06:25 8006-61-907/02/09 15:195.6
4-Bromofluorobenzene (S)93 %1 07/03/09 06:25 460-00-407/02/09 15:1950-135
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 22.2 %1 07/06/09 12:370.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 79 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TRIP BLANK 1 07-09 Lab ID:9247665035 Collected:07/01/09 00:00 Received:07/01/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 07/21/09 10:24 67-64-125.0
Benzene ND ug/L 1 07/21/09 10:24 71-43-21.0
Bromobenzene ND ug/L 1 07/21/09 10:24 108-86-11.0
Bromochloromethane ND ug/L 1 07/21/09 10:24 74-97-51.0
Bromodichloromethane ND ug/L 1 07/21/09 10:24 75-27-41.0
Bromoform ND ug/L 1 07/21/09 10:24 75-25-21.0
Bromomethane ND ug/L 1 07/21/09 10:24 74-83-95.0
2-Butanone (MEK)ND ug/L 1 07/21/09 10:24 78-93-35.0
Carbon tetrachloride ND ug/L 1 07/21/09 10:24 56-23-51.0
Chlorobenzene ND ug/L 1 07/21/09 10:24 108-90-71.0
Chloroethane ND ug/L 1 07/21/09 10:24 75-00-31.0
Chloroform ND ug/L 1 07/21/09 10:24 67-66-31.0
Chloromethane ND ug/L 1 07/21/09 10:24 74-87-31.0
2-Chlorotoluene ND ug/L 1 07/21/09 10:24 95-49-81.0
4-Chlorotoluene ND ug/L 1 07/21/09 10:24 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 07/21/09 10:24 96-12-83.0
Dibromochloromethane ND ug/L 1 07/21/09 10:24 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 07/21/09 10:24 106-93-41.0
Dibromomethane ND ug/L 1 07/21/09 10:24 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 07/21/09 10:24 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 07/21/09 10:24 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 07/21/09 10:24 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 07/21/09 10:24 75-71-81.0
1,1-Dichloroethane ND ug/L 1 07/21/09 10:24 75-34-31.0
1,2-Dichloroethane ND ug/L 1 07/21/09 10:24 107-06-21.0
1,1-Dichloroethene ND ug/L 1 07/21/09 10:24 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 07/21/09 10:24 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 07/21/09 10:24 156-60-51.0
1,2-Dichloropropane ND ug/L 1 07/21/09 10:24 78-87-51.0
1,3-Dichloropropane ND ug/L 1 07/21/09 10:24 142-28-91.0
2,2-Dichloropropane ND ug/L 1 07/21/09 10:24 594-20-71.0
1,1-Dichloropropene ND ug/L 1 07/21/09 10:24 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 07/21/09 10:24 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 07/21/09 10:24 10061-02-61.0
Diisopropyl ether ND ug/L 1 07/21/09 10:24 108-20-31.0
Ethylbenzene ND ug/L 1 07/21/09 10:24 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 07/21/09 10:24 87-68-31.0
2-Hexanone ND ug/L 1 07/21/09 10:24 591-78-65.0
p-Isopropyltoluene ND ug/L 1 07/21/09 10:24 99-87-61.0
Methylene Chloride ND ug/L 1 07/21/09 10:24 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 07/21/09 10:24 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 07/21/09 10:24 1634-04-41.0
Naphthalene ND ug/L 1 07/21/09 10:24 91-20-31.0
Styrene ND ug/L 1 07/21/09 10:24 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 07/21/09 10:24 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 07/21/09 10:24 79-34-51.0
Tetrachloroethene ND ug/L 1 07/21/09 10:24 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 80 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TRIP BLANK 1 07-09 Lab ID:9247665035 Collected:07/01/09 00:00 Received:07/01/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 07/21/09 10:24 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 07/21/09 10:24 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 07/21/09 10:24 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 07/21/09 10:24 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 07/21/09 10:24 79-00-51.0
Trichloroethene ND ug/L 1 07/21/09 10:24 79-01-61.0
Trichlorofluoromethane ND ug/L 1 07/21/09 10:24 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 07/21/09 10:24 96-18-41.0
Vinyl acetate ND ug/L 1 07/21/09 10:24 108-05-42.0
Vinyl chloride ND ug/L 1 07/21/09 10:24 75-01-41.0
m&p-Xylene ND ug/L 1 07/21/09 10:24 1330-20-72.0
o-Xylene ND ug/L 1 07/21/09 10:24 95-47-61.0
4-Bromofluorobenzene (S)102 %1 07/21/09 10:24 460-00-4 H187-109
Dibromofluoromethane (S)106 %1 07/21/09 10:24 1868-53-785-115
1,2-Dichloroethane-d4 (S)106 %1 07/21/09 10:24 17060-07-079-120
Toluene-d8 (S)101 %1 07/21/09 10:24 2037-26-570-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 81 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-EQUIP RINSATE 07-09 Lab ID:9247665036 Collected:07/01/09 12:45 Received:07/01/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead ND ug/L 1 07/08/09 21:27 7439-92-107/07/09 15:305.0
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 07/07/09 15:44 67-64-125.0
Benzene ND ug/L 1 07/07/09 15:44 71-43-21.0
Bromobenzene ND ug/L 1 07/07/09 15:44 108-86-11.0
Bromochloromethane ND ug/L 1 07/07/09 15:44 74-97-51.0
Bromodichloromethane ND ug/L 1 07/07/09 15:44 75-27-41.0
Bromoform ND ug/L 1 07/07/09 15:44 75-25-21.0
Bromomethane ND ug/L 1 07/07/09 15:44 74-83-95.0
2-Butanone (MEK)ND ug/L 1 07/07/09 15:44 78-93-35.0
Carbon tetrachloride ND ug/L 1 07/07/09 15:44 56-23-51.0
Chlorobenzene ND ug/L 1 07/07/09 15:44 108-90-71.0
Chloroethane ND ug/L 1 07/07/09 15:44 75-00-31.0
Chloroform ND ug/L 1 07/07/09 15:44 67-66-31.0
Chloromethane ND ug/L 1 07/07/09 15:44 74-87-31.0
2-Chlorotoluene ND ug/L 1 07/07/09 15:44 95-49-81.0
4-Chlorotoluene ND ug/L 1 07/07/09 15:44 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 07/07/09 15:44 96-12-83.0
Dibromochloromethane ND ug/L 1 07/07/09 15:44 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 07/07/09 15:44 106-93-41.0
Dibromomethane ND ug/L 1 07/07/09 15:44 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 07/07/09 15:44 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 07/07/09 15:44 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 07/07/09 15:44 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 07/07/09 15:44 75-71-81.0
1,1-Dichloroethane ND ug/L 1 07/07/09 15:44 75-34-31.0
1,2-Dichloroethane ND ug/L 1 07/07/09 15:44 107-06-21.0
1,1-Dichloroethene ND ug/L 1 07/07/09 15:44 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 07/07/09 15:44 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 07/07/09 15:44 156-60-51.0
1,2-Dichloropropane ND ug/L 1 07/07/09 15:44 78-87-51.0
1,3-Dichloropropane ND ug/L 1 07/07/09 15:44 142-28-91.0
2,2-Dichloropropane ND ug/L 1 07/07/09 15:44 594-20-71.0
1,1-Dichloropropene ND ug/L 1 07/07/09 15:44 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 07/07/09 15:44 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 07/07/09 15:44 10061-02-61.0
Diisopropyl ether ND ug/L 1 07/07/09 15:44 108-20-31.0
Ethylbenzene ND ug/L 1 07/07/09 15:44 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 07/07/09 15:44 87-68-31.0
2-Hexanone ND ug/L 1 07/07/09 15:44 591-78-65.0
p-Isopropyltoluene ND ug/L 1 07/07/09 15:44 99-87-61.0
Methylene Chloride ND ug/L 1 07/07/09 15:44 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 07/07/09 15:44 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 07/07/09 15:44 1634-04-41.0
Naphthalene ND ug/L 1 07/07/09 15:44 91-20-31.0
Styrene ND ug/L 1 07/07/09 15:44 100-42-51.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 82 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-EQUIP RINSATE 07-09 Lab ID:9247665036 Collected:07/01/09 12:45 Received:07/01/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/L 1 07/07/09 15:44 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 07/07/09 15:44 79-34-51.0
Tetrachloroethene ND ug/L 1 07/07/09 15:44 127-18-41.0
Toluene ND ug/L 1 07/07/09 15:44 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 07/07/09 15:44 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 07/07/09 15:44 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 07/07/09 15:44 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 07/07/09 15:44 79-00-51.0
Trichloroethene ND ug/L 1 07/07/09 15:44 79-01-61.0
Trichlorofluoromethane ND ug/L 1 07/07/09 15:44 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 07/07/09 15:44 96-18-41.0
Vinyl acetate ND ug/L 1 07/07/09 15:44 108-05-42.0
Vinyl chloride ND ug/L 1 07/07/09 15:44 75-01-41.0
m&p-Xylene ND ug/L 1 07/07/09 15:44 1330-20-72.0
o-Xylene ND ug/L 1 07/07/09 15:44 95-47-61.0
4-Bromofluorobenzene (S)97 %1 07/07/09 15:44 460-00-487-109
Dibromofluoromethane (S)108 %1 07/07/09 15:44 1868-53-785-115
1,2-Dichloroethane-d4 (S)105 %1 07/07/09 15:44 17060-07-079-120
Toluene-d8 (S)101 %1 07/07/09 15:44 2037-26-570-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 83 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-FIELD BLANK-07-09 Lab ID:9247665037 Collected:07/02/09 08:15 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 07/08/09 15:06 67-64-125.0
Benzene ND ug/L 1 07/08/09 15:06 71-43-21.0
Bromobenzene ND ug/L 1 07/08/09 15:06 108-86-11.0
Bromochloromethane ND ug/L 1 07/08/09 15:06 74-97-51.0
Bromodichloromethane ND ug/L 1 07/08/09 15:06 75-27-41.0
Bromoform ND ug/L 1 07/08/09 15:06 75-25-21.0
Bromomethane ND ug/L 1 07/08/09 15:06 74-83-95.0
2-Butanone (MEK)ND ug/L 1 07/08/09 15:06 78-93-35.0
Carbon tetrachloride ND ug/L 1 07/08/09 15:06 56-23-51.0
Chlorobenzene ND ug/L 1 07/08/09 15:06 108-90-71.0
Chloroethane ND ug/L 1 07/08/09 15:06 75-00-31.0
Chloroform ND ug/L 1 07/08/09 15:06 67-66-31.0
Chloromethane ND ug/L 1 07/08/09 15:06 74-87-31.0
2-Chlorotoluene ND ug/L 1 07/08/09 15:06 95-49-81.0
4-Chlorotoluene ND ug/L 1 07/08/09 15:06 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 07/08/09 15:06 96-12-83.0
Dibromochloromethane ND ug/L 1 07/08/09 15:06 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 07/08/09 15:06 106-93-41.0
Dibromomethane ND ug/L 1 07/08/09 15:06 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 07/08/09 15:06 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 07/08/09 15:06 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 07/08/09 15:06 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 07/08/09 15:06 75-71-81.0
1,1-Dichloroethane ND ug/L 1 07/08/09 15:06 75-34-31.0
1,2-Dichloroethane ND ug/L 1 07/08/09 15:06 107-06-21.0
1,1-Dichloroethene ND ug/L 1 07/08/09 15:06 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 07/08/09 15:06 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 07/08/09 15:06 156-60-51.0
1,2-Dichloropropane ND ug/L 1 07/08/09 15:06 78-87-51.0
1,3-Dichloropropane ND ug/L 1 07/08/09 15:06 142-28-91.0
2,2-Dichloropropane ND ug/L 1 07/08/09 15:06 594-20-71.0
1,1-Dichloropropene ND ug/L 1 07/08/09 15:06 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 07/08/09 15:06 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 07/08/09 15:06 10061-02-61.0
Diisopropyl ether ND ug/L 1 07/08/09 15:06 108-20-31.0
Ethylbenzene ND ug/L 1 07/08/09 15:06 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 07/08/09 15:06 87-68-31.0
2-Hexanone ND ug/L 1 07/08/09 15:06 591-78-65.0
p-Isopropyltoluene ND ug/L 1 07/08/09 15:06 99-87-61.0
Methylene Chloride ND ug/L 1 07/08/09 15:06 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 07/08/09 15:06 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 07/08/09 15:06 1634-04-41.0
Naphthalene ND ug/L 1 07/08/09 15:06 91-20-31.0
Styrene ND ug/L 1 07/08/09 15:06 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 07/08/09 15:06 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 07/08/09 15:06 79-34-51.0
Tetrachloroethene ND ug/L 1 07/08/09 15:06 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 84 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-FIELD BLANK-07-09 Lab ID:9247665037 Collected:07/02/09 08:15 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 07/08/09 15:06 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 07/08/09 15:06 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 07/08/09 15:06 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 07/08/09 15:06 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 07/08/09 15:06 79-00-51.0
Trichloroethene ND ug/L 1 07/08/09 15:06 79-01-61.0
Trichlorofluoromethane ND ug/L 1 07/08/09 15:06 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 07/08/09 15:06 96-18-41.0
Vinyl acetate ND ug/L 1 07/08/09 15:06 108-05-42.0
Vinyl chloride ND ug/L 1 07/08/09 15:06 75-01-41.0
m&p-Xylene ND ug/L 1 07/08/09 15:06 1330-20-72.0
o-Xylene ND ug/L 1 07/08/09 15:06 95-47-61.0
4-Bromofluorobenzene (S)98 %1 07/08/09 15:06 460-00-487-109
Dibromofluoromethane (S)109 %1 07/08/09 15:06 1868-53-785-115
1,2-Dichloroethane-d4 (S)106 %1 07/08/09 15:06 17060-07-079-120
Toluene-d8 (S)101 %1 07/08/09 15:06 2037-26-570-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 85 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TW1-07-09 Lab ID:9247665038 Collected:07/02/09 08:30 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 07/14/09 23:05 83-32-907/09/09 10:0014.3
Acenaphthylene ND ug/L 1 07/14/09 23:05 208-96-807/09/09 10:0014.3
Aniline ND ug/L 1 07/14/09 23:05 62-53-307/09/09 10:0014.3
Anthracene ND ug/L 1 07/14/09 23:05 120-12-707/09/09 10:0014.3
Benzo(a)anthracene ND ug/L 1 07/14/09 23:05 56-55-307/09/09 10:0014.3
Benzo(a)pyrene ND ug/L 1 07/14/09 23:05 50-32-807/09/09 10:0014.3
Benzo(b)fluoranthene ND ug/L 1 07/14/09 23:05 205-99-207/09/09 10:0014.3
Benzo(g,h,i)perylene ND ug/L 1 07/14/09 23:05 191-24-207/09/09 10:0014.3
Benzo(k)fluoranthene ND ug/L 1 07/14/09 23:05 207-08-907/09/09 10:0014.3
Benzoic Acid ND ug/L 1 07/14/09 23:05 65-85-007/09/09 10:0071.4
Benzyl alcohol ND ug/L 1 07/14/09 23:05 100-51-607/09/09 10:0028.6
4-Bromophenylphenyl ether ND ug/L 1 07/14/09 23:05 101-55-307/09/09 10:0014.3
Butylbenzylphthalate ND ug/L 1 07/14/09 23:05 85-68-707/09/09 10:0014.3
4-Chloro-3-methylphenol ND ug/L 1 07/14/09 23:05 59-50-707/09/09 10:0028.6
4-Chloroaniline ND ug/L 1 07/14/09 23:05 106-47-807/09/09 10:0071.4
bis(2-Chloroethoxy)methane ND ug/L 1 07/14/09 23:05 111-91-107/09/09 10:0014.3
bis(2-Chloroethyl) ether ND ug/L 1 07/14/09 23:05 111-44-407/09/09 10:0014.3
bis(2-Chloroisopropyl) ether ND ug/L 1 07/14/09 23:05 108-60-107/09/09 10:0014.3
2-Chloronaphthalene ND ug/L 1 07/14/09 23:05 91-58-707/09/09 10:0014.3
2-Chlorophenol ND ug/L 1 07/14/09 23:05 95-57-807/09/09 10:0014.3
4-Chlorophenylphenyl ether ND ug/L 1 07/14/09 23:05 7005-72-307/09/09 10:0014.3
Chrysene ND ug/L 1 07/14/09 23:05 218-01-907/09/09 10:0014.3
Dibenz(a,h)anthracene ND ug/L 1 07/14/09 23:05 53-70-307/09/09 10:0014.3
Dibenzofuran ND ug/L 1 07/14/09 23:05 132-64-907/09/09 10:0014.3
1,2-Dichlorobenzene ND ug/L 1 07/14/09 23:05 95-50-107/09/09 10:0014.3
1,3-Dichlorobenzene ND ug/L 1 07/14/09 23:05 541-73-107/09/09 10:0014.3
1,4-Dichlorobenzene ND ug/L 1 07/14/09 23:05 106-46-707/09/09 10:0014.3
3,3'-Dichlorobenzidine ND ug/L 1 07/14/09 23:05 91-94-107/09/09 10:0071.4
2,4-Dichlorophenol ND ug/L 1 07/14/09 23:05 120-83-207/09/09 10:0014.3
Diethylphthalate ND ug/L 1 07/14/09 23:05 84-66-207/09/09 10:0014.3
2,4-Dimethylphenol ND ug/L 1 07/14/09 23:05 105-67-907/09/09 10:0014.3
Dimethylphthalate ND ug/L 1 07/14/09 23:05 131-11-307/09/09 10:0014.3
Di-n-butylphthalate ND ug/L 1 07/14/09 23:05 84-74-207/09/09 10:0014.3
4,6-Dinitro-2-methylphenol ND ug/L 1 07/14/09 23:05 534-52-107/09/09 10:0028.6
2,4-Dinitrophenol ND ug/L 1 07/14/09 23:05 51-28-507/09/09 10:0071.4
2,4-Dinitrotoluene ND ug/L 1 07/14/09 23:05 121-14-207/09/09 10:0014.3
2,6-Dinitrotoluene ND ug/L 1 07/14/09 23:05 606-20-207/09/09 10:0014.3
Di-n-octylphthalate ND ug/L 1 07/14/09 23:05 117-84-007/09/09 10:0014.3
1,2-Diphenylhydrazine ND ug/L 1 07/14/09 23:05 122-66-707/09/09 10:0014.3
bis(2-Ethylhexyl)phthalate ND ug/L 1 07/14/09 23:05 117-81-707/09/09 10:0014.3
Fluoranthene ND ug/L 1 07/14/09 23:05 206-44-007/09/09 10:0014.3
Fluorene ND ug/L 1 07/14/09 23:05 86-73-707/09/09 10:0014.3
Hexachloro-1,3-butadiene ND ug/L 1 07/14/09 23:05 87-68-307/09/09 10:0014.3
Hexachlorobenzene ND ug/L 1 07/14/09 23:05 118-74-107/09/09 10:0014.3
Hexachlorocyclopentadiene ND ug/L 1 07/14/09 23:05 77-47-407/09/09 10:0014.3
Hexachloroethane ND ug/L 1 07/14/09 23:05 67-72-107/09/09 10:0014.3
Indeno(1,2,3-cd)pyrene ND ug/L 1 07/14/09 23:05 193-39-507/09/09 10:0014.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 86 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TW1-07-09 Lab ID:9247665038 Collected:07/02/09 08:30 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Isophorone ND ug/L 1 07/14/09 23:05 78-59-107/09/09 10:0014.3
1-Methylnaphthalene ND ug/L 1 07/14/09 23:05 90-12-007/09/09 10:0014.3
2-Methylnaphthalene ND ug/L 1 07/14/09 23:05 91-57-607/09/09 10:0014.3
2-Methylphenol(o-Cresol)ND ug/L 1 07/14/09 23:05 95-48-707/09/09 10:0014.3
3&4-Methylphenol(m&p Cresol)ND ug/L 1 07/14/09 23:0507/09/09 10:0014.3
Naphthalene ND ug/L 1 07/14/09 23:05 91-20-307/09/09 10:0014.3
2-Nitroaniline ND ug/L 1 07/14/09 23:05 88-74-407/09/09 10:0071.4
3-Nitroaniline ND ug/L 1 07/14/09 23:05 99-09-207/09/09 10:0071.4
4-Nitroaniline ND ug/L 1 07/14/09 23:05 100-01-607/09/09 10:0071.4
Nitrobenzene ND ug/L 1 07/14/09 23:05 98-95-307/09/09 10:0014.3
2-Nitrophenol ND ug/L 1 07/14/09 23:05 88-75-507/09/09 10:0014.3
4-Nitrophenol ND ug/L 1 07/14/09 23:05 100-02-707/09/09 10:0071.4
N-Nitrosodimethylamine ND ug/L 1 07/14/09 23:05 62-75-907/09/09 10:0014.3
N-Nitroso-di-n-propylamine ND ug/L 1 07/14/09 23:05 621-64-707/09/09 10:0014.3
N-Nitrosodiphenylamine ND ug/L 1 07/14/09 23:05 86-30-607/09/09 10:0014.3
Pentachlorophenol ND ug/L 1 07/14/09 23:05 87-86-507/09/09 10:0071.4
Phenanthrene ND ug/L 1 07/14/09 23:05 85-01-807/09/09 10:0014.3
Phenol ND ug/L 1 07/14/09 23:05 108-95-207/09/09 10:0014.3
Pyrene ND ug/L 1 07/14/09 23:05 129-00-007/09/09 10:0014.3
1,2,4-Trichlorobenzene ND ug/L 1 07/14/09 23:05 120-82-107/09/09 10:0014.3
2,4,5-Trichlorophenol ND ug/L 1 07/14/09 23:05 95-95-407/09/09 10:0014.3
2,4,6-Trichlorophenol ND ug/L 1 07/14/09 23:05 88-06-207/09/09 10:0014.3
Nitrobenzene-d5 (S)57 %1 07/14/09 23:05 4165-60-007/09/09 10:0030-150
2-Fluorobiphenyl (S)53 %1 07/14/09 23:05 321-60-807/09/09 10:0030-150
Terphenyl-d14 (S)66 %1 07/14/09 23:05 1718-51-007/09/09 10:0030-150
Phenol-d6 (S)30 %1 07/14/09 23:05 13127-88-307/09/09 10:0025-150
2-Fluorophenol (S)19 %1 07/14/09 23:05 367-12-4 S007/09/09 10:0025-150
2,4,6-Tribromophenol (S)57 %1 07/14/09 23:05 118-79-607/09/09 10:0025-150
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 07/08/09 15:25 67-64-125.0
Benzene ND ug/L 1 07/08/09 15:25 71-43-21.0
Bromobenzene ND ug/L 1 07/08/09 15:25 108-86-11.0
Bromochloromethane ND ug/L 1 07/08/09 15:25 74-97-51.0
Bromodichloromethane ND ug/L 1 07/08/09 15:25 75-27-41.0
Bromoform ND ug/L 1 07/08/09 15:25 75-25-21.0
Bromomethane ND ug/L 1 07/08/09 15:25 74-83-95.0
2-Butanone (MEK)ND ug/L 1 07/08/09 15:25 78-93-35.0
Carbon tetrachloride ND ug/L 1 07/08/09 15:25 56-23-51.0
Chlorobenzene ND ug/L 1 07/08/09 15:25 108-90-71.0
Chloroethane ND ug/L 1 07/08/09 15:25 75-00-31.0
Chloroform ND ug/L 1 07/08/09 15:25 67-66-31.0
Chloromethane ND ug/L 1 07/08/09 15:25 74-87-31.0
2-Chlorotoluene ND ug/L 1 07/08/09 15:25 95-49-81.0
4-Chlorotoluene ND ug/L 1 07/08/09 15:25 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 07/08/09 15:25 96-12-83.0
Dibromochloromethane ND ug/L 1 07/08/09 15:25 124-48-11.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 87 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TW1-07-09 Lab ID:9247665038 Collected:07/02/09 08:30 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
1,2-Dibromoethane (EDB)ND ug/L 1 07/08/09 15:25 106-93-41.0
Dibromomethane ND ug/L 1 07/08/09 15:25 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 07/08/09 15:25 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 07/08/09 15:25 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 07/08/09 15:25 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 07/08/09 15:25 75-71-81.0
1,1-Dichloroethane ND ug/L 1 07/08/09 15:25 75-34-31.0
1,2-Dichloroethane ND ug/L 1 07/08/09 15:25 107-06-21.0
1,1-Dichloroethene ND ug/L 1 07/08/09 15:25 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 07/08/09 15:25 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 07/08/09 15:25 156-60-51.0
1,2-Dichloropropane ND ug/L 1 07/08/09 15:25 78-87-51.0
1,3-Dichloropropane ND ug/L 1 07/08/09 15:25 142-28-91.0
2,2-Dichloropropane ND ug/L 1 07/08/09 15:25 594-20-71.0
1,1-Dichloropropene ND ug/L 1 07/08/09 15:25 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 07/08/09 15:25 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 07/08/09 15:25 10061-02-61.0
Diisopropyl ether ND ug/L 1 07/08/09 15:25 108-20-31.0
Ethylbenzene ND ug/L 1 07/08/09 15:25 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 07/08/09 15:25 87-68-31.0
2-Hexanone ND ug/L 1 07/08/09 15:25 591-78-65.0
p-Isopropyltoluene ND ug/L 1 07/08/09 15:25 99-87-61.0
Methylene Chloride ND ug/L 1 07/08/09 15:25 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 07/08/09 15:25 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 07/08/09 15:25 1634-04-41.0
Naphthalene ND ug/L 1 07/08/09 15:25 91-20-31.0
Styrene ND ug/L 1 07/08/09 15:25 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 07/08/09 15:25 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 07/08/09 15:25 79-34-51.0
Tetrachloroethene ND ug/L 1 07/08/09 15:25 127-18-41.0
Toluene ND ug/L 1 07/08/09 15:25 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 07/08/09 15:25 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 07/08/09 15:25 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 07/08/09 15:25 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 07/08/09 15:25 79-00-51.0
Trichloroethene ND ug/L 1 07/08/09 15:25 79-01-61.0
Trichlorofluoromethane ND ug/L 1 07/08/09 15:25 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 07/08/09 15:25 96-18-41.0
Vinyl acetate ND ug/L 1 07/08/09 15:25 108-05-42.0
Vinyl chloride ND ug/L 1 07/08/09 15:25 75-01-41.0
m&p-Xylene ND ug/L 1 07/08/09 15:25 1330-20-72.0
o-Xylene ND ug/L 1 07/08/09 15:25 95-47-61.0
4-Bromofluorobenzene (S)96 %1 07/08/09 15:25 460-00-487-109
Dibromofluoromethane (S)109 %1 07/08/09 15:25 1868-53-785-115
1,2-Dichloroethane-d4 (S)107 %1 07/08/09 15:25 17060-07-079-120
Toluene-d8 (S)101 %1 07/08/09 15:25 2037-26-570-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 88 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TW4-07-09 Lab ID:9247665039 Collected:07/02/09 10:15 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 07/14/09 23:30 83-32-907/09/09 10:0014.3
Acenaphthylene ND ug/L 1 07/14/09 23:30 208-96-807/09/09 10:0014.3
Aniline ND ug/L 1 07/14/09 23:30 62-53-307/09/09 10:0014.3
Anthracene ND ug/L 1 07/14/09 23:30 120-12-707/09/09 10:0014.3
Benzo(a)anthracene ND ug/L 1 07/14/09 23:30 56-55-307/09/09 10:0014.3
Benzo(a)pyrene ND ug/L 1 07/14/09 23:30 50-32-807/09/09 10:0014.3
Benzo(b)fluoranthene ND ug/L 1 07/14/09 23:30 205-99-207/09/09 10:0014.3
Benzo(g,h,i)perylene ND ug/L 1 07/14/09 23:30 191-24-207/09/09 10:0014.3
Benzo(k)fluoranthene ND ug/L 1 07/14/09 23:30 207-08-907/09/09 10:0014.3
Benzoic Acid ND ug/L 1 07/14/09 23:30 65-85-007/09/09 10:0071.4
Benzyl alcohol ND ug/L 1 07/14/09 23:30 100-51-607/09/09 10:0028.6
4-Bromophenylphenyl ether ND ug/L 1 07/14/09 23:30 101-55-307/09/09 10:0014.3
Butylbenzylphthalate ND ug/L 1 07/14/09 23:30 85-68-707/09/09 10:0014.3
4-Chloro-3-methylphenol ND ug/L 1 07/14/09 23:30 59-50-707/09/09 10:0028.6
4-Chloroaniline ND ug/L 1 07/14/09 23:30 106-47-807/09/09 10:0071.4
bis(2-Chloroethoxy)methane ND ug/L 1 07/14/09 23:30 111-91-107/09/09 10:0014.3
bis(2-Chloroethyl) ether ND ug/L 1 07/14/09 23:30 111-44-407/09/09 10:0014.3
bis(2-Chloroisopropyl) ether ND ug/L 1 07/14/09 23:30 108-60-107/09/09 10:0014.3
2-Chloronaphthalene ND ug/L 1 07/14/09 23:30 91-58-707/09/09 10:0014.3
2-Chlorophenol ND ug/L 1 07/14/09 23:30 95-57-807/09/09 10:0014.3
4-Chlorophenylphenyl ether ND ug/L 1 07/14/09 23:30 7005-72-307/09/09 10:0014.3
Chrysene ND ug/L 1 07/14/09 23:30 218-01-907/09/09 10:0014.3
Dibenz(a,h)anthracene ND ug/L 1 07/14/09 23:30 53-70-307/09/09 10:0014.3
Dibenzofuran ND ug/L 1 07/14/09 23:30 132-64-907/09/09 10:0014.3
1,2-Dichlorobenzene ND ug/L 1 07/14/09 23:30 95-50-107/09/09 10:0014.3
1,3-Dichlorobenzene ND ug/L 1 07/14/09 23:30 541-73-107/09/09 10:0014.3
1,4-Dichlorobenzene ND ug/L 1 07/14/09 23:30 106-46-707/09/09 10:0014.3
3,3'-Dichlorobenzidine ND ug/L 1 07/14/09 23:30 91-94-107/09/09 10:0071.4
2,4-Dichlorophenol ND ug/L 1 07/14/09 23:30 120-83-207/09/09 10:0014.3
Diethylphthalate ND ug/L 1 07/14/09 23:30 84-66-207/09/09 10:0014.3
2,4-Dimethylphenol ND ug/L 1 07/14/09 23:30 105-67-907/09/09 10:0014.3
Dimethylphthalate ND ug/L 1 07/14/09 23:30 131-11-307/09/09 10:0014.3
Di-n-butylphthalate ND ug/L 1 07/14/09 23:30 84-74-207/09/09 10:0014.3
4,6-Dinitro-2-methylphenol ND ug/L 1 07/14/09 23:30 534-52-107/09/09 10:0028.6
2,4-Dinitrophenol ND ug/L 1 07/14/09 23:30 51-28-507/09/09 10:0071.4
2,4-Dinitrotoluene ND ug/L 1 07/14/09 23:30 121-14-207/09/09 10:0014.3
2,6-Dinitrotoluene ND ug/L 1 07/14/09 23:30 606-20-207/09/09 10:0014.3
Di-n-octylphthalate ND ug/L 1 07/14/09 23:30 117-84-007/09/09 10:0014.3
1,2-Diphenylhydrazine ND ug/L 1 07/14/09 23:30 122-66-707/09/09 10:0014.3
bis(2-Ethylhexyl)phthalate ND ug/L 1 07/14/09 23:30 117-81-707/09/09 10:0014.3
Fluoranthene ND ug/L 1 07/14/09 23:30 206-44-007/09/09 10:0014.3
Fluorene ND ug/L 1 07/14/09 23:30 86-73-707/09/09 10:0014.3
Hexachloro-1,3-butadiene ND ug/L 1 07/14/09 23:30 87-68-307/09/09 10:0014.3
Hexachlorobenzene ND ug/L 1 07/14/09 23:30 118-74-107/09/09 10:0014.3
Hexachlorocyclopentadiene ND ug/L 1 07/14/09 23:30 77-47-407/09/09 10:0014.3
Hexachloroethane ND ug/L 1 07/14/09 23:30 67-72-107/09/09 10:0014.3
Indeno(1,2,3-cd)pyrene ND ug/L 1 07/14/09 23:30 193-39-507/09/09 10:0014.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 89 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TW4-07-09 Lab ID:9247665039 Collected:07/02/09 10:15 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Isophorone ND ug/L 1 07/14/09 23:30 78-59-107/09/09 10:0014.3
1-Methylnaphthalene ND ug/L 1 07/14/09 23:30 90-12-007/09/09 10:0014.3
2-Methylnaphthalene ND ug/L 1 07/14/09 23:30 91-57-607/09/09 10:0014.3
2-Methylphenol(o-Cresol)ND ug/L 1 07/14/09 23:30 95-48-707/09/09 10:0014.3
3&4-Methylphenol(m&p Cresol)ND ug/L 1 07/14/09 23:3007/09/09 10:0014.3
Naphthalene ND ug/L 1 07/14/09 23:30 91-20-307/09/09 10:0014.3
2-Nitroaniline ND ug/L 1 07/14/09 23:30 88-74-407/09/09 10:0071.4
3-Nitroaniline ND ug/L 1 07/14/09 23:30 99-09-207/09/09 10:0071.4
4-Nitroaniline ND ug/L 1 07/14/09 23:30 100-01-607/09/09 10:0071.4
Nitrobenzene ND ug/L 1 07/14/09 23:30 98-95-307/09/09 10:0014.3
2-Nitrophenol ND ug/L 1 07/14/09 23:30 88-75-507/09/09 10:0014.3
4-Nitrophenol ND ug/L 1 07/14/09 23:30 100-02-707/09/09 10:0071.4
N-Nitrosodimethylamine ND ug/L 1 07/14/09 23:30 62-75-907/09/09 10:0014.3
N-Nitroso-di-n-propylamine ND ug/L 1 07/14/09 23:30 621-64-707/09/09 10:0014.3
N-Nitrosodiphenylamine ND ug/L 1 07/14/09 23:30 86-30-607/09/09 10:0014.3
Pentachlorophenol ND ug/L 1 07/14/09 23:30 87-86-507/09/09 10:0071.4
Phenanthrene ND ug/L 1 07/14/09 23:30 85-01-807/09/09 10:0014.3
Phenol ND ug/L 1 07/14/09 23:30 108-95-207/09/09 10:0014.3
Pyrene ND ug/L 1 07/14/09 23:30 129-00-007/09/09 10:0014.3
1,2,4-Trichlorobenzene ND ug/L 1 07/14/09 23:30 120-82-107/09/09 10:0014.3
2,4,5-Trichlorophenol ND ug/L 1 07/14/09 23:30 95-95-407/09/09 10:0014.3
2,4,6-Trichlorophenol ND ug/L 1 07/14/09 23:30 88-06-207/09/09 10:0014.3
Nitrobenzene-d5 (S)54 %1 07/14/09 23:30 4165-60-007/09/09 10:0030-150
2-Fluorobiphenyl (S)56 %1 07/14/09 23:30 321-60-807/09/09 10:0030-150
Terphenyl-d14 (S)56 %1 07/14/09 23:30 1718-51-007/09/09 10:0030-150
Phenol-d6 (S)29 %1 07/14/09 23:30 13127-88-307/09/09 10:0025-150
2-Fluorophenol (S)28 %1 07/14/09 23:30 367-12-407/09/09 10:0025-150
2,4,6-Tribromophenol (S)41 %1 07/14/09 23:30 118-79-607/09/09 10:0025-150
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 07/08/09 15:44 67-64-125.0
Benzene ND ug/L 1 07/08/09 15:44 71-43-21.0
Bromobenzene ND ug/L 1 07/08/09 15:44 108-86-11.0
Bromochloromethane ND ug/L 1 07/08/09 15:44 74-97-51.0
Bromodichloromethane ND ug/L 1 07/08/09 15:44 75-27-41.0
Bromoform ND ug/L 1 07/08/09 15:44 75-25-21.0
Bromomethane ND ug/L 1 07/08/09 15:44 74-83-95.0
2-Butanone (MEK)ND ug/L 1 07/08/09 15:44 78-93-35.0
Carbon tetrachloride ND ug/L 1 07/08/09 15:44 56-23-51.0
Chlorobenzene ND ug/L 1 07/08/09 15:44 108-90-71.0
Chloroethane ND ug/L 1 07/08/09 15:44 75-00-31.0
Chloroform ND ug/L 1 07/08/09 15:44 67-66-31.0
Chloromethane ND ug/L 1 07/08/09 15:44 74-87-31.0
2-Chlorotoluene ND ug/L 1 07/08/09 15:44 95-49-81.0
4-Chlorotoluene ND ug/L 1 07/08/09 15:44 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 07/08/09 15:44 96-12-83.0
Dibromochloromethane ND ug/L 1 07/08/09 15:44 124-48-11.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 90 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TW4-07-09 Lab ID:9247665039 Collected:07/02/09 10:15 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
1,2-Dibromoethane (EDB)ND ug/L 1 07/08/09 15:44 106-93-41.0
Dibromomethane ND ug/L 1 07/08/09 15:44 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 07/08/09 15:44 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 07/08/09 15:44 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 07/08/09 15:44 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 07/08/09 15:44 75-71-81.0
1,1-Dichloroethane ND ug/L 1 07/08/09 15:44 75-34-31.0
1,2-Dichloroethane ND ug/L 1 07/08/09 15:44 107-06-21.0
1,1-Dichloroethene ND ug/L 1 07/08/09 15:44 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 07/08/09 15:44 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 07/08/09 15:44 156-60-51.0
1,2-Dichloropropane ND ug/L 1 07/08/09 15:44 78-87-51.0
1,3-Dichloropropane ND ug/L 1 07/08/09 15:44 142-28-91.0
2,2-Dichloropropane ND ug/L 1 07/08/09 15:44 594-20-71.0
1,1-Dichloropropene ND ug/L 1 07/08/09 15:44 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 07/08/09 15:44 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 07/08/09 15:44 10061-02-61.0
Diisopropyl ether ND ug/L 1 07/08/09 15:44 108-20-31.0
Ethylbenzene ND ug/L 1 07/08/09 15:44 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 07/08/09 15:44 87-68-31.0
2-Hexanone ND ug/L 1 07/08/09 15:44 591-78-65.0
p-Isopropyltoluene ND ug/L 1 07/08/09 15:44 99-87-61.0
Methylene Chloride ND ug/L 1 07/08/09 15:44 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 07/08/09 15:44 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 07/08/09 15:44 1634-04-41.0
Naphthalene ND ug/L 1 07/08/09 15:44 91-20-31.0
Styrene ND ug/L 1 07/08/09 15:44 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 07/08/09 15:44 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 07/08/09 15:44 79-34-51.0
Tetrachloroethene ND ug/L 1 07/08/09 15:44 127-18-41.0
Toluene ND ug/L 1 07/08/09 15:44 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 07/08/09 15:44 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 07/08/09 15:44 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 07/08/09 15:44 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 07/08/09 15:44 79-00-51.0
Trichloroethene ND ug/L 1 07/08/09 15:44 79-01-61.0
Trichlorofluoromethane ND ug/L 1 07/08/09 15:44 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 07/08/09 15:44 96-18-41.0
Vinyl acetate ND ug/L 1 07/08/09 15:44 108-05-42.0
Vinyl chloride ND ug/L 1 07/08/09 15:44 75-01-41.0
m&p-Xylene ND ug/L 1 07/08/09 15:44 1330-20-72.0
o-Xylene ND ug/L 1 07/08/09 15:44 95-47-61.0
4-Bromofluorobenzene (S)97 %1 07/08/09 15:44 460-00-487-109
Dibromofluoromethane (S)108 %1 07/08/09 15:44 1868-53-785-115
1,2-Dichloroethane-d4 (S)104 %1 07/08/09 15:44 17060-07-079-120
Toluene-d8 (S)102 %1 07/08/09 15:44 2037-26-570-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 91 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TW3-07-09 Lab ID:9247665040 Collected:07/02/09 11:15 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead 85.4 ug/L 1 07/09/09 21:00 7439-92-107/09/09 09:105.0
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 07/08/09 16:03 67-64-125.0
Benzene ND ug/L 1 07/08/09 16:03 71-43-21.0
Bromobenzene ND ug/L 1 07/08/09 16:03 108-86-11.0
Bromochloromethane ND ug/L 1 07/08/09 16:03 74-97-51.0
Bromodichloromethane ND ug/L 1 07/08/09 16:03 75-27-41.0
Bromoform ND ug/L 1 07/08/09 16:03 75-25-21.0
Bromomethane ND ug/L 1 07/08/09 16:03 74-83-95.0
2-Butanone (MEK)ND ug/L 1 07/08/09 16:03 78-93-35.0
Carbon tetrachloride ND ug/L 1 07/08/09 16:03 56-23-51.0
Chlorobenzene ND ug/L 1 07/08/09 16:03 108-90-71.0
Chloroethane ND ug/L 1 07/08/09 16:03 75-00-31.0
Chloroform ND ug/L 1 07/08/09 16:03 67-66-31.0
Chloromethane ND ug/L 1 07/08/09 16:03 74-87-31.0
2-Chlorotoluene ND ug/L 1 07/08/09 16:03 95-49-81.0
4-Chlorotoluene ND ug/L 1 07/08/09 16:03 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 07/08/09 16:03 96-12-83.0
Dibromochloromethane ND ug/L 1 07/08/09 16:03 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 07/08/09 16:03 106-93-41.0
Dibromomethane ND ug/L 1 07/08/09 16:03 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 07/08/09 16:03 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 07/08/09 16:03 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 07/08/09 16:03 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 07/08/09 16:03 75-71-81.0
1,1-Dichloroethane ND ug/L 1 07/08/09 16:03 75-34-31.0
1,2-Dichloroethane ND ug/L 1 07/08/09 16:03 107-06-21.0
1,1-Dichloroethene ND ug/L 1 07/08/09 16:03 75-35-41.0
cis-1,2-Dichloroethene 1.4 ug/L 1 07/08/09 16:03 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 07/08/09 16:03 156-60-51.0
1,2-Dichloropropane ND ug/L 1 07/08/09 16:03 78-87-51.0
1,3-Dichloropropane ND ug/L 1 07/08/09 16:03 142-28-91.0
2,2-Dichloropropane ND ug/L 1 07/08/09 16:03 594-20-71.0
1,1-Dichloropropene ND ug/L 1 07/08/09 16:03 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 07/08/09 16:03 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 07/08/09 16:03 10061-02-61.0
Diisopropyl ether ND ug/L 1 07/08/09 16:03 108-20-31.0
Ethylbenzene ND ug/L 1 07/08/09 16:03 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 07/08/09 16:03 87-68-31.0
2-Hexanone ND ug/L 1 07/08/09 16:03 591-78-65.0
p-Isopropyltoluene ND ug/L 1 07/08/09 16:03 99-87-61.0
Methylene Chloride ND ug/L 1 07/08/09 16:03 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 07/08/09 16:03 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 07/08/09 16:03 1634-04-41.0
Naphthalene ND ug/L 1 07/08/09 16:03 91-20-31.0
Styrene ND ug/L 1 07/08/09 16:03 100-42-51.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 92 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TW3-07-09 Lab ID:9247665040 Collected:07/02/09 11:15 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/L 1 07/08/09 16:03 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 07/08/09 16:03 79-34-51.0
Tetrachloroethene ND ug/L 1 07/08/09 16:03 127-18-41.0
Toluene ND ug/L 1 07/08/09 16:03 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 07/08/09 16:03 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 07/08/09 16:03 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 07/08/09 16:03 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 07/08/09 16:03 79-00-51.0
Trichloroethene ND ug/L 1 07/08/09 16:03 79-01-61.0
Trichlorofluoromethane ND ug/L 1 07/08/09 16:03 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 07/08/09 16:03 96-18-41.0
Vinyl acetate ND ug/L 1 07/08/09 16:03 108-05-42.0
Vinyl chloride ND ug/L 1 07/08/09 16:03 75-01-41.0
m&p-Xylene ND ug/L 1 07/08/09 16:03 1330-20-72.0
o-Xylene ND ug/L 1 07/08/09 16:03 95-47-61.0
4-Bromofluorobenzene (S)96 %1 07/08/09 16:03 460-00-487-109
Dibromofluoromethane (S)109 %1 07/08/09 16:03 1868-53-785-115
1,2-Dichloroethane-d4 (S)108 %1 07/08/09 16:03 17060-07-079-120
Toluene-d8 (S)102 %1 07/08/09 16:03 2037-26-570-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 93 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TW5-07-09 Lab ID:9247665041 Collected:07/02/09 13:00 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 07/14/09 23:55 83-32-907/09/09 10:0012.5
Acenaphthylene ND ug/L 1 07/14/09 23:55 208-96-807/09/09 10:0012.5
Aniline ND ug/L 1 07/14/09 23:55 62-53-307/09/09 10:0012.5
Anthracene ND ug/L 1 07/14/09 23:55 120-12-707/09/09 10:0012.5
Benzo(a)anthracene ND ug/L 1 07/14/09 23:55 56-55-307/09/09 10:0012.5
Benzo(a)pyrene ND ug/L 1 07/14/09 23:55 50-32-807/09/09 10:0012.5
Benzo(b)fluoranthene ND ug/L 1 07/14/09 23:55 205-99-207/09/09 10:0012.5
Benzo(g,h,i)perylene ND ug/L 1 07/14/09 23:55 191-24-207/09/09 10:0012.5
Benzo(k)fluoranthene ND ug/L 1 07/14/09 23:55 207-08-907/09/09 10:0012.5
Benzoic Acid ND ug/L 1 07/14/09 23:55 65-85-007/09/09 10:0062.5
Benzyl alcohol ND ug/L 1 07/14/09 23:55 100-51-607/09/09 10:0025.0
4-Bromophenylphenyl ether ND ug/L 1 07/14/09 23:55 101-55-307/09/09 10:0012.5
Butylbenzylphthalate ND ug/L 1 07/14/09 23:55 85-68-707/09/09 10:0012.5
4-Chloro-3-methylphenol ND ug/L 1 07/14/09 23:55 59-50-707/09/09 10:0025.0
4-Chloroaniline ND ug/L 1 07/14/09 23:55 106-47-807/09/09 10:0062.5
bis(2-Chloroethoxy)methane ND ug/L 1 07/14/09 23:55 111-91-107/09/09 10:0012.5
bis(2-Chloroethyl) ether ND ug/L 1 07/14/09 23:55 111-44-407/09/09 10:0012.5
bis(2-Chloroisopropyl) ether ND ug/L 1 07/14/09 23:55 108-60-107/09/09 10:0012.5
2-Chloronaphthalene ND ug/L 1 07/14/09 23:55 91-58-707/09/09 10:0012.5
2-Chlorophenol ND ug/L 1 07/14/09 23:55 95-57-807/09/09 10:0012.5
4-Chlorophenylphenyl ether ND ug/L 1 07/14/09 23:55 7005-72-307/09/09 10:0012.5
Chrysene ND ug/L 1 07/14/09 23:55 218-01-907/09/09 10:0012.5
Dibenz(a,h)anthracene ND ug/L 1 07/14/09 23:55 53-70-307/09/09 10:0012.5
Dibenzofuran ND ug/L 1 07/14/09 23:55 132-64-907/09/09 10:0012.5
1,2-Dichlorobenzene ND ug/L 1 07/14/09 23:55 95-50-107/09/09 10:0012.5
1,3-Dichlorobenzene ND ug/L 1 07/14/09 23:55 541-73-107/09/09 10:0012.5
1,4-Dichlorobenzene ND ug/L 1 07/14/09 23:55 106-46-707/09/09 10:0012.5
3,3'-Dichlorobenzidine ND ug/L 1 07/14/09 23:55 91-94-107/09/09 10:0062.5
2,4-Dichlorophenol ND ug/L 1 07/14/09 23:55 120-83-207/09/09 10:0012.5
Diethylphthalate ND ug/L 1 07/14/09 23:55 84-66-207/09/09 10:0012.5
2,4-Dimethylphenol ND ug/L 1 07/14/09 23:55 105-67-907/09/09 10:0012.5
Dimethylphthalate ND ug/L 1 07/14/09 23:55 131-11-307/09/09 10:0012.5
Di-n-butylphthalate ND ug/L 1 07/14/09 23:55 84-74-207/09/09 10:0012.5
4,6-Dinitro-2-methylphenol ND ug/L 1 07/14/09 23:55 534-52-107/09/09 10:0025.0
2,4-Dinitrophenol ND ug/L 1 07/14/09 23:55 51-28-507/09/09 10:0062.5
2,4-Dinitrotoluene ND ug/L 1 07/14/09 23:55 121-14-207/09/09 10:0012.5
2,6-Dinitrotoluene ND ug/L 1 07/14/09 23:55 606-20-207/09/09 10:0012.5
Di-n-octylphthalate ND ug/L 1 07/14/09 23:55 117-84-007/09/09 10:0012.5
1,2-Diphenylhydrazine ND ug/L 1 07/14/09 23:55 122-66-707/09/09 10:0012.5
bis(2-Ethylhexyl)phthalate ND ug/L 1 07/14/09 23:55 117-81-707/09/09 10:0012.5
Fluoranthene ND ug/L 1 07/14/09 23:55 206-44-007/09/09 10:0012.5
Fluorene ND ug/L 1 07/14/09 23:55 86-73-707/09/09 10:0012.5
Hexachloro-1,3-butadiene ND ug/L 1 07/14/09 23:55 87-68-307/09/09 10:0012.5
Hexachlorobenzene ND ug/L 1 07/14/09 23:55 118-74-107/09/09 10:0012.5
Hexachlorocyclopentadiene ND ug/L 1 07/14/09 23:55 77-47-407/09/09 10:0012.5
Hexachloroethane ND ug/L 1 07/14/09 23:55 67-72-107/09/09 10:0012.5
Indeno(1,2,3-cd)pyrene ND ug/L 1 07/14/09 23:55 193-39-507/09/09 10:0012.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 94 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TW5-07-09 Lab ID:9247665041 Collected:07/02/09 13:00 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Isophorone ND ug/L 1 07/14/09 23:55 78-59-107/09/09 10:0012.5
1-Methylnaphthalene ND ug/L 1 07/14/09 23:55 90-12-007/09/09 10:0012.5
2-Methylnaphthalene ND ug/L 1 07/14/09 23:55 91-57-607/09/09 10:0012.5
2-Methylphenol(o-Cresol)ND ug/L 1 07/14/09 23:55 95-48-707/09/09 10:0012.5
3&4-Methylphenol(m&p Cresol)ND ug/L 1 07/14/09 23:5507/09/09 10:0012.5
Naphthalene ND ug/L 1 07/14/09 23:55 91-20-307/09/09 10:0012.5
2-Nitroaniline ND ug/L 1 07/14/09 23:55 88-74-407/09/09 10:0062.5
3-Nitroaniline ND ug/L 1 07/14/09 23:55 99-09-207/09/09 10:0062.5
4-Nitroaniline ND ug/L 1 07/14/09 23:55 100-01-607/09/09 10:0062.5
Nitrobenzene ND ug/L 1 07/14/09 23:55 98-95-307/09/09 10:0012.5
2-Nitrophenol ND ug/L 1 07/14/09 23:55 88-75-507/09/09 10:0012.5
4-Nitrophenol ND ug/L 1 07/14/09 23:55 100-02-707/09/09 10:0062.5
N-Nitrosodimethylamine ND ug/L 1 07/14/09 23:55 62-75-907/09/09 10:0012.5
N-Nitroso-di-n-propylamine ND ug/L 1 07/14/09 23:55 621-64-707/09/09 10:0012.5
N-Nitrosodiphenylamine ND ug/L 1 07/14/09 23:55 86-30-607/09/09 10:0012.5
Pentachlorophenol ND ug/L 1 07/14/09 23:55 87-86-507/09/09 10:0062.5
Phenanthrene ND ug/L 1 07/14/09 23:55 85-01-807/09/09 10:0012.5
Phenol ND ug/L 1 07/14/09 23:55 108-95-207/09/09 10:0012.5
Pyrene ND ug/L 1 07/14/09 23:55 129-00-007/09/09 10:0012.5
1,2,4-Trichlorobenzene ND ug/L 1 07/14/09 23:55 120-82-107/09/09 10:0012.5
2,4,5-Trichlorophenol ND ug/L 1 07/14/09 23:55 95-95-407/09/09 10:0012.5
2,4,6-Trichlorophenol ND ug/L 1 07/14/09 23:55 88-06-207/09/09 10:0012.5
Nitrobenzene-d5 (S)78 %1 07/14/09 23:55 4165-60-007/09/09 10:0030-150
2-Fluorobiphenyl (S)75 %1 07/14/09 23:55 321-60-807/09/09 10:0030-150
Terphenyl-d14 (S)77 %1 07/14/09 23:55 1718-51-007/09/09 10:0030-150
Phenol-d6 (S)31 %1 07/14/09 23:55 13127-88-307/09/09 10:0025-150
2-Fluorophenol (S)43 %1 07/14/09 23:55 367-12-407/09/09 10:0025-150
2,4,6-Tribromophenol (S)71 %1 07/14/09 23:55 118-79-607/09/09 10:0025-150
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 07/08/09 16:22 67-64-125.0
Benzene ND ug/L 1 07/08/09 16:22 71-43-21.0
Bromobenzene ND ug/L 1 07/08/09 16:22 108-86-11.0
Bromochloromethane ND ug/L 1 07/08/09 16:22 74-97-51.0
Bromodichloromethane ND ug/L 1 07/08/09 16:22 75-27-41.0
Bromoform ND ug/L 1 07/08/09 16:22 75-25-21.0
Bromomethane ND ug/L 1 07/08/09 16:22 74-83-95.0
2-Butanone (MEK)ND ug/L 1 07/08/09 16:22 78-93-35.0
Carbon tetrachloride ND ug/L 1 07/08/09 16:22 56-23-51.0
Chlorobenzene ND ug/L 1 07/08/09 16:22 108-90-71.0
Chloroethane ND ug/L 1 07/08/09 16:22 75-00-31.0
Chloroform ND ug/L 1 07/08/09 16:22 67-66-31.0
Chloromethane ND ug/L 1 07/08/09 16:22 74-87-31.0
2-Chlorotoluene ND ug/L 1 07/08/09 16:22 95-49-81.0
4-Chlorotoluene ND ug/L 1 07/08/09 16:22 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 07/08/09 16:22 96-12-83.0
Dibromochloromethane ND ug/L 1 07/08/09 16:22 124-48-11.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 95 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TW5-07-09 Lab ID:9247665041 Collected:07/02/09 13:00 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
1,2-Dibromoethane (EDB)ND ug/L 1 07/08/09 16:22 106-93-41.0
Dibromomethane ND ug/L 1 07/08/09 16:22 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 07/08/09 16:22 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 07/08/09 16:22 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 07/08/09 16:22 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 07/08/09 16:22 75-71-81.0
1,1-Dichloroethane ND ug/L 1 07/08/09 16:22 75-34-31.0
1,2-Dichloroethane ND ug/L 1 07/08/09 16:22 107-06-21.0
1,1-Dichloroethene ND ug/L 1 07/08/09 16:22 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 07/08/09 16:22 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 07/08/09 16:22 156-60-51.0
1,2-Dichloropropane ND ug/L 1 07/08/09 16:22 78-87-51.0
1,3-Dichloropropane ND ug/L 1 07/08/09 16:22 142-28-91.0
2,2-Dichloropropane ND ug/L 1 07/08/09 16:22 594-20-71.0
1,1-Dichloropropene ND ug/L 1 07/08/09 16:22 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 07/08/09 16:22 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 07/08/09 16:22 10061-02-61.0
Diisopropyl ether ND ug/L 1 07/08/09 16:22 108-20-31.0
Ethylbenzene ND ug/L 1 07/08/09 16:22 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 07/08/09 16:22 87-68-31.0
2-Hexanone ND ug/L 1 07/08/09 16:22 591-78-65.0
p-Isopropyltoluene ND ug/L 1 07/08/09 16:22 99-87-61.0
Methylene Chloride ND ug/L 1 07/08/09 16:22 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 07/08/09 16:22 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 07/08/09 16:22 1634-04-41.0
Naphthalene ND ug/L 1 07/08/09 16:22 91-20-31.0
Styrene ND ug/L 1 07/08/09 16:22 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 07/08/09 16:22 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 07/08/09 16:22 79-34-51.0
Tetrachloroethene ND ug/L 1 07/08/09 16:22 127-18-41.0
Toluene ND ug/L 1 07/08/09 16:22 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 07/08/09 16:22 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 07/08/09 16:22 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 07/08/09 16:22 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 07/08/09 16:22 79-00-51.0
Trichloroethene ND ug/L 1 07/08/09 16:22 79-01-61.0
Trichlorofluoromethane ND ug/L 1 07/08/09 16:22 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 07/08/09 16:22 96-18-41.0
Vinyl acetate ND ug/L 1 07/08/09 16:22 108-05-42.0
Vinyl chloride ND ug/L 1 07/08/09 16:22 75-01-41.0
m&p-Xylene ND ug/L 1 07/08/09 16:22 1330-20-72.0
o-Xylene ND ug/L 1 07/08/09 16:22 95-47-61.0
4-Bromofluorobenzene (S)97 %1 07/08/09 16:22 460-00-487-109
Dibromofluoromethane (S)109 %1 07/08/09 16:22 1868-53-785-115
1,2-Dichloroethane-d4 (S)108 %1 07/08/09 16:22 17060-07-079-120
Toluene-d8 (S)102 %1 07/08/09 16:22 2037-26-570-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 96 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-DUPLICATE1-07-09 Lab ID:9247665042 Collected:07/02/09 00:00 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 07/15/09 00:20 83-32-907/09/09 10:0012.5
Acenaphthylene ND ug/L 1 07/15/09 00:20 208-96-807/09/09 10:0012.5
Aniline ND ug/L 1 07/15/09 00:20 62-53-307/09/09 10:0012.5
Anthracene ND ug/L 1 07/15/09 00:20 120-12-707/09/09 10:0012.5
Benzo(a)anthracene ND ug/L 1 07/15/09 00:20 56-55-307/09/09 10:0012.5
Benzo(a)pyrene ND ug/L 1 07/15/09 00:20 50-32-807/09/09 10:0012.5
Benzo(b)fluoranthene ND ug/L 1 07/15/09 00:20 205-99-207/09/09 10:0012.5
Benzo(g,h,i)perylene ND ug/L 1 07/15/09 00:20 191-24-207/09/09 10:0012.5
Benzo(k)fluoranthene ND ug/L 1 07/15/09 00:20 207-08-907/09/09 10:0012.5
Benzoic Acid ND ug/L 1 07/15/09 00:20 65-85-007/09/09 10:0062.5
Benzyl alcohol ND ug/L 1 07/15/09 00:20 100-51-607/09/09 10:0025.0
4-Bromophenylphenyl ether ND ug/L 1 07/15/09 00:20 101-55-307/09/09 10:0012.5
Butylbenzylphthalate ND ug/L 1 07/15/09 00:20 85-68-707/09/09 10:0012.5
4-Chloro-3-methylphenol ND ug/L 1 07/15/09 00:20 59-50-707/09/09 10:0025.0
4-Chloroaniline ND ug/L 1 07/15/09 00:20 106-47-807/09/09 10:0062.5
bis(2-Chloroethoxy)methane ND ug/L 1 07/15/09 00:20 111-91-107/09/09 10:0012.5
bis(2-Chloroethyl) ether ND ug/L 1 07/15/09 00:20 111-44-407/09/09 10:0012.5
bis(2-Chloroisopropyl) ether ND ug/L 1 07/15/09 00:20 108-60-107/09/09 10:0012.5
2-Chloronaphthalene ND ug/L 1 07/15/09 00:20 91-58-707/09/09 10:0012.5
2-Chlorophenol ND ug/L 1 07/15/09 00:20 95-57-807/09/09 10:0012.5
4-Chlorophenylphenyl ether ND ug/L 1 07/15/09 00:20 7005-72-307/09/09 10:0012.5
Chrysene ND ug/L 1 07/15/09 00:20 218-01-907/09/09 10:0012.5
Dibenz(a,h)anthracene ND ug/L 1 07/15/09 00:20 53-70-307/09/09 10:0012.5
Dibenzofuran ND ug/L 1 07/15/09 00:20 132-64-907/09/09 10:0012.5
1,2-Dichlorobenzene ND ug/L 1 07/15/09 00:20 95-50-107/09/09 10:0012.5
1,3-Dichlorobenzene ND ug/L 1 07/15/09 00:20 541-73-107/09/09 10:0012.5
1,4-Dichlorobenzene ND ug/L 1 07/15/09 00:20 106-46-707/09/09 10:0012.5
3,3'-Dichlorobenzidine ND ug/L 1 07/15/09 00:20 91-94-107/09/09 10:0062.5
2,4-Dichlorophenol ND ug/L 1 07/15/09 00:20 120-83-207/09/09 10:0012.5
Diethylphthalate ND ug/L 1 07/15/09 00:20 84-66-207/09/09 10:0012.5
2,4-Dimethylphenol ND ug/L 1 07/15/09 00:20 105-67-907/09/09 10:0012.5
Dimethylphthalate ND ug/L 1 07/15/09 00:20 131-11-307/09/09 10:0012.5
Di-n-butylphthalate ND ug/L 1 07/15/09 00:20 84-74-207/09/09 10:0012.5
4,6-Dinitro-2-methylphenol ND ug/L 1 07/15/09 00:20 534-52-107/09/09 10:0025.0
2,4-Dinitrophenol ND ug/L 1 07/15/09 00:20 51-28-507/09/09 10:0062.5
2,4-Dinitrotoluene ND ug/L 1 07/15/09 00:20 121-14-207/09/09 10:0012.5
2,6-Dinitrotoluene ND ug/L 1 07/15/09 00:20 606-20-207/09/09 10:0012.5
Di-n-octylphthalate ND ug/L 1 07/15/09 00:20 117-84-007/09/09 10:0012.5
1,2-Diphenylhydrazine ND ug/L 1 07/15/09 00:20 122-66-707/09/09 10:0012.5
bis(2-Ethylhexyl)phthalate ND ug/L 1 07/15/09 00:20 117-81-707/09/09 10:0012.5
Fluoranthene ND ug/L 1 07/15/09 00:20 206-44-007/09/09 10:0012.5
Fluorene ND ug/L 1 07/15/09 00:20 86-73-707/09/09 10:0012.5
Hexachloro-1,3-butadiene ND ug/L 1 07/15/09 00:20 87-68-307/09/09 10:0012.5
Hexachlorobenzene ND ug/L 1 07/15/09 00:20 118-74-107/09/09 10:0012.5
Hexachlorocyclopentadiene ND ug/L 1 07/15/09 00:20 77-47-407/09/09 10:0012.5
Hexachloroethane ND ug/L 1 07/15/09 00:20 67-72-107/09/09 10:0012.5
Indeno(1,2,3-cd)pyrene ND ug/L 1 07/15/09 00:20 193-39-507/09/09 10:0012.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 97 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-DUPLICATE1-07-09 Lab ID:9247665042 Collected:07/02/09 00:00 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Isophorone ND ug/L 1 07/15/09 00:20 78-59-107/09/09 10:0012.5
1-Methylnaphthalene ND ug/L 1 07/15/09 00:20 90-12-007/09/09 10:0012.5
2-Methylnaphthalene ND ug/L 1 07/15/09 00:20 91-57-607/09/09 10:0012.5
2-Methylphenol(o-Cresol)ND ug/L 1 07/15/09 00:20 95-48-707/09/09 10:0012.5
3&4-Methylphenol(m&p Cresol)ND ug/L 1 07/15/09 00:2007/09/09 10:0012.5
Naphthalene ND ug/L 1 07/15/09 00:20 91-20-307/09/09 10:0012.5
2-Nitroaniline ND ug/L 1 07/15/09 00:20 88-74-407/09/09 10:0062.5
3-Nitroaniline ND ug/L 1 07/15/09 00:20 99-09-207/09/09 10:0062.5
4-Nitroaniline ND ug/L 1 07/15/09 00:20 100-01-607/09/09 10:0062.5
Nitrobenzene ND ug/L 1 07/15/09 00:20 98-95-307/09/09 10:0012.5
2-Nitrophenol ND ug/L 1 07/15/09 00:20 88-75-507/09/09 10:0012.5
4-Nitrophenol ND ug/L 1 07/15/09 00:20 100-02-707/09/09 10:0062.5
N-Nitrosodimethylamine ND ug/L 1 07/15/09 00:20 62-75-907/09/09 10:0012.5
N-Nitroso-di-n-propylamine ND ug/L 1 07/15/09 00:20 621-64-707/09/09 10:0012.5
N-Nitrosodiphenylamine ND ug/L 1 07/15/09 00:20 86-30-607/09/09 10:0012.5
Pentachlorophenol ND ug/L 1 07/15/09 00:20 87-86-507/09/09 10:0062.5
Phenanthrene ND ug/L 1 07/15/09 00:20 85-01-807/09/09 10:0012.5
Phenol ND ug/L 1 07/15/09 00:20 108-95-207/09/09 10:0012.5
Pyrene ND ug/L 1 07/15/09 00:20 129-00-007/09/09 10:0012.5
1,2,4-Trichlorobenzene ND ug/L 1 07/15/09 00:20 120-82-107/09/09 10:0012.5
2,4,5-Trichlorophenol ND ug/L 1 07/15/09 00:20 95-95-407/09/09 10:0012.5
2,4,6-Trichlorophenol ND ug/L 1 07/15/09 00:20 88-06-207/09/09 10:0012.5
Nitrobenzene-d5 (S)58 %1 07/15/09 00:20 4165-60-007/09/09 10:0030-150
2-Fluorobiphenyl (S)57 %1 07/15/09 00:20 321-60-807/09/09 10:0030-150
Terphenyl-d14 (S)65 %1 07/15/09 00:20 1718-51-007/09/09 10:0030-150
Phenol-d6 (S)30 %1 07/15/09 00:20 13127-88-307/09/09 10:0025-150
2-Fluorophenol (S)31 %1 07/15/09 00:20 367-12-407/09/09 10:0025-150
2,4,6-Tribromophenol (S)66 %1 07/15/09 00:20 118-79-607/09/09 10:0025-150
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 07/08/09 16:41 67-64-125.0
Benzene ND ug/L 1 07/08/09 16:41 71-43-21.0
Bromobenzene ND ug/L 1 07/08/09 16:41 108-86-11.0
Bromochloromethane ND ug/L 1 07/08/09 16:41 74-97-51.0
Bromodichloromethane ND ug/L 1 07/08/09 16:41 75-27-41.0
Bromoform ND ug/L 1 07/08/09 16:41 75-25-21.0
Bromomethane ND ug/L 1 07/08/09 16:41 74-83-95.0
2-Butanone (MEK)ND ug/L 1 07/08/09 16:41 78-93-35.0
Carbon tetrachloride ND ug/L 1 07/08/09 16:41 56-23-51.0
Chlorobenzene ND ug/L 1 07/08/09 16:41 108-90-71.0
Chloroethane ND ug/L 1 07/08/09 16:41 75-00-31.0
Chloroform ND ug/L 1 07/08/09 16:41 67-66-31.0
Chloromethane ND ug/L 1 07/08/09 16:41 74-87-31.0
2-Chlorotoluene ND ug/L 1 07/08/09 16:41 95-49-81.0
4-Chlorotoluene ND ug/L 1 07/08/09 16:41 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 07/08/09 16:41 96-12-83.0
Dibromochloromethane ND ug/L 1 07/08/09 16:41 124-48-11.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 98 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-DUPLICATE1-07-09 Lab ID:9247665042 Collected:07/02/09 00:00 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
1,2-Dibromoethane (EDB)ND ug/L 1 07/08/09 16:41 106-93-41.0
Dibromomethane ND ug/L 1 07/08/09 16:41 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 07/08/09 16:41 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 07/08/09 16:41 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 07/08/09 16:41 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 07/08/09 16:41 75-71-81.0
1,1-Dichloroethane ND ug/L 1 07/08/09 16:41 75-34-31.0
1,2-Dichloroethane ND ug/L 1 07/08/09 16:41 107-06-21.0
1,1-Dichloroethene ND ug/L 1 07/08/09 16:41 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 07/08/09 16:41 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 07/08/09 16:41 156-60-51.0
1,2-Dichloropropane ND ug/L 1 07/08/09 16:41 78-87-51.0
1,3-Dichloropropane ND ug/L 1 07/08/09 16:41 142-28-91.0
2,2-Dichloropropane ND ug/L 1 07/08/09 16:41 594-20-71.0
1,1-Dichloropropene ND ug/L 1 07/08/09 16:41 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 07/08/09 16:41 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 07/08/09 16:41 10061-02-61.0
Diisopropyl ether ND ug/L 1 07/08/09 16:41 108-20-31.0
Ethylbenzene ND ug/L 1 07/08/09 16:41 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 07/08/09 16:41 87-68-31.0
2-Hexanone ND ug/L 1 07/08/09 16:41 591-78-65.0
p-Isopropyltoluene ND ug/L 1 07/08/09 16:41 99-87-61.0
Methylene Chloride ND ug/L 1 07/08/09 16:41 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 07/08/09 16:41 108-10-15.0
Methyl-tert-butyl ether 1.0 ug/L 1 07/08/09 16:41 1634-04-41.0
Naphthalene ND ug/L 1 07/08/09 16:41 91-20-31.0
Styrene ND ug/L 1 07/08/09 16:41 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 07/08/09 16:41 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 07/08/09 16:41 79-34-51.0
Tetrachloroethene ND ug/L 1 07/08/09 16:41 127-18-41.0
Toluene ND ug/L 1 07/08/09 16:41 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 07/08/09 16:41 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 07/08/09 16:41 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 07/08/09 16:41 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 07/08/09 16:41 79-00-51.0
Trichloroethene ND ug/L 1 07/08/09 16:41 79-01-61.0
Trichlorofluoromethane ND ug/L 1 07/08/09 16:41 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 07/08/09 16:41 96-18-41.0
Vinyl acetate ND ug/L 1 07/08/09 16:41 108-05-42.0
Vinyl chloride ND ug/L 1 07/08/09 16:41 75-01-41.0
m&p-Xylene ND ug/L 1 07/08/09 16:41 1330-20-72.0
o-Xylene ND ug/L 1 07/08/09 16:41 95-47-61.0
4-Bromofluorobenzene (S)95 %1 07/08/09 16:41 460-00-487-109
Dibromofluoromethane (S)108 %1 07/08/09 16:41 1868-53-785-115
1,2-Dichloroethane-d4 (S)105 %1 07/08/09 16:41 17060-07-079-120
Toluene-d8 (S)102 %1 07/08/09 16:41 2037-26-570-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 99 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TW6-07-09 Lab ID:9247665043 Collected:07/02/09 13:45 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 07/15/09 00:45 83-32-907/09/09 10:0015.2
Acenaphthylene ND ug/L 1 07/15/09 00:45 208-96-807/09/09 10:0015.2
Aniline ND ug/L 1 07/15/09 00:45 62-53-307/09/09 10:0015.2
Anthracene ND ug/L 1 07/15/09 00:45 120-12-707/09/09 10:0015.2
Benzo(a)anthracene ND ug/L 1 07/15/09 00:45 56-55-307/09/09 10:0015.2
Benzo(a)pyrene ND ug/L 1 07/15/09 00:45 50-32-807/09/09 10:0015.2
Benzo(b)fluoranthene ND ug/L 1 07/15/09 00:45 205-99-207/09/09 10:0015.2
Benzo(g,h,i)perylene ND ug/L 1 07/15/09 00:45 191-24-207/09/09 10:0015.2
Benzo(k)fluoranthene ND ug/L 1 07/15/09 00:45 207-08-907/09/09 10:0015.2
Benzoic Acid ND ug/L 1 07/15/09 00:45 65-85-007/09/09 10:0075.8
Benzyl alcohol ND ug/L 1 07/15/09 00:45 100-51-607/09/09 10:0030.3
4-Bromophenylphenyl ether ND ug/L 1 07/15/09 00:45 101-55-307/09/09 10:0015.2
Butylbenzylphthalate ND ug/L 1 07/15/09 00:45 85-68-707/09/09 10:0015.2
4-Chloro-3-methylphenol ND ug/L 1 07/15/09 00:45 59-50-707/09/09 10:0030.3
4-Chloroaniline ND ug/L 1 07/15/09 00:45 106-47-807/09/09 10:0075.8
bis(2-Chloroethoxy)methane ND ug/L 1 07/15/09 00:45 111-91-107/09/09 10:0015.2
bis(2-Chloroethyl) ether ND ug/L 1 07/15/09 00:45 111-44-407/09/09 10:0015.2
bis(2-Chloroisopropyl) ether ND ug/L 1 07/15/09 00:45 108-60-107/09/09 10:0015.2
2-Chloronaphthalene ND ug/L 1 07/15/09 00:45 91-58-707/09/09 10:0015.2
2-Chlorophenol ND ug/L 1 07/15/09 00:45 95-57-807/09/09 10:0015.2
4-Chlorophenylphenyl ether ND ug/L 1 07/15/09 00:45 7005-72-307/09/09 10:0015.2
Chrysene ND ug/L 1 07/15/09 00:45 218-01-907/09/09 10:0015.2
Dibenz(a,h)anthracene ND ug/L 1 07/15/09 00:45 53-70-307/09/09 10:0015.2
Dibenzofuran ND ug/L 1 07/15/09 00:45 132-64-907/09/09 10:0015.2
1,2-Dichlorobenzene ND ug/L 1 07/15/09 00:45 95-50-107/09/09 10:0015.2
1,3-Dichlorobenzene ND ug/L 1 07/15/09 00:45 541-73-107/09/09 10:0015.2
1,4-Dichlorobenzene ND ug/L 1 07/15/09 00:45 106-46-707/09/09 10:0015.2
3,3'-Dichlorobenzidine ND ug/L 1 07/15/09 00:45 91-94-107/09/09 10:0075.8
2,4-Dichlorophenol ND ug/L 1 07/15/09 00:45 120-83-207/09/09 10:0015.2
Diethylphthalate ND ug/L 1 07/15/09 00:45 84-66-207/09/09 10:0015.2
2,4-Dimethylphenol ND ug/L 1 07/15/09 00:45 105-67-907/09/09 10:0015.2
Dimethylphthalate ND ug/L 1 07/15/09 00:45 131-11-307/09/09 10:0015.2
Di-n-butylphthalate ND ug/L 1 07/15/09 00:45 84-74-207/09/09 10:0015.2
4,6-Dinitro-2-methylphenol ND ug/L 1 07/15/09 00:45 534-52-107/09/09 10:0030.3
2,4-Dinitrophenol ND ug/L 1 07/15/09 00:45 51-28-507/09/09 10:0075.8
2,4-Dinitrotoluene ND ug/L 1 07/15/09 00:45 121-14-207/09/09 10:0015.2
2,6-Dinitrotoluene ND ug/L 1 07/15/09 00:45 606-20-207/09/09 10:0015.2
Di-n-octylphthalate ND ug/L 1 07/15/09 00:45 117-84-007/09/09 10:0015.2
1,2-Diphenylhydrazine ND ug/L 1 07/15/09 00:45 122-66-707/09/09 10:0015.2
bis(2-Ethylhexyl)phthalate ND ug/L 1 07/15/09 00:45 117-81-707/09/09 10:0015.2
Fluoranthene ND ug/L 1 07/15/09 00:45 206-44-007/09/09 10:0015.2
Fluorene ND ug/L 1 07/15/09 00:45 86-73-707/09/09 10:0015.2
Hexachloro-1,3-butadiene ND ug/L 1 07/15/09 00:45 87-68-307/09/09 10:0015.2
Hexachlorobenzene ND ug/L 1 07/15/09 00:45 118-74-107/09/09 10:0015.2
Hexachlorocyclopentadiene ND ug/L 1 07/15/09 00:45 77-47-407/09/09 10:0015.2
Hexachloroethane ND ug/L 1 07/15/09 00:45 67-72-107/09/09 10:0015.2
Indeno(1,2,3-cd)pyrene ND ug/L 1 07/15/09 00:45 193-39-507/09/09 10:0015.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 100 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TW6-07-09 Lab ID:9247665043 Collected:07/02/09 13:45 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Isophorone ND ug/L 1 07/15/09 00:45 78-59-107/09/09 10:0015.2
1-Methylnaphthalene ND ug/L 1 07/15/09 00:45 90-12-007/09/09 10:0015.2
2-Methylnaphthalene ND ug/L 1 07/15/09 00:45 91-57-607/09/09 10:0015.2
2-Methylphenol(o-Cresol)ND ug/L 1 07/15/09 00:45 95-48-707/09/09 10:0015.2
3&4-Methylphenol(m&p Cresol)ND ug/L 1 07/15/09 00:4507/09/09 10:0015.2
Naphthalene ND ug/L 1 07/15/09 00:45 91-20-307/09/09 10:0015.2
2-Nitroaniline ND ug/L 1 07/15/09 00:45 88-74-407/09/09 10:0075.8
3-Nitroaniline ND ug/L 1 07/15/09 00:45 99-09-207/09/09 10:0075.8
4-Nitroaniline ND ug/L 1 07/15/09 00:45 100-01-607/09/09 10:0075.8
Nitrobenzene ND ug/L 1 07/15/09 00:45 98-95-307/09/09 10:0015.2
2-Nitrophenol ND ug/L 1 07/15/09 00:45 88-75-507/09/09 10:0015.2
4-Nitrophenol ND ug/L 1 07/15/09 00:45 100-02-707/09/09 10:0075.8
N-Nitrosodimethylamine ND ug/L 1 07/15/09 00:45 62-75-907/09/09 10:0015.2
N-Nitroso-di-n-propylamine ND ug/L 1 07/15/09 00:45 621-64-707/09/09 10:0015.2
N-Nitrosodiphenylamine ND ug/L 1 07/15/09 00:45 86-30-607/09/09 10:0015.2
Pentachlorophenol ND ug/L 1 07/15/09 00:45 87-86-507/09/09 10:0075.8
Phenanthrene ND ug/L 1 07/15/09 00:45 85-01-807/09/09 10:0015.2
Phenol ND ug/L 1 07/15/09 00:45 108-95-207/09/09 10:0015.2
Pyrene ND ug/L 1 07/15/09 00:45 129-00-007/09/09 10:0015.2
1,2,4-Trichlorobenzene ND ug/L 1 07/15/09 00:45 120-82-107/09/09 10:0015.2
2,4,5-Trichlorophenol ND ug/L 1 07/15/09 00:45 95-95-407/09/09 10:0015.2
2,4,6-Trichlorophenol ND ug/L 1 07/15/09 00:45 88-06-207/09/09 10:0015.2
Nitrobenzene-d5 (S)69 %1 07/15/09 00:45 4165-60-007/09/09 10:0030-150
2-Fluorobiphenyl (S)65 %1 07/15/09 00:45 321-60-807/09/09 10:0030-150
Terphenyl-d14 (S)76 %1 07/15/09 00:45 1718-51-007/09/09 10:0030-150
Phenol-d6 (S)32 %1 07/15/09 00:45 13127-88-307/09/09 10:0025-150
2-Fluorophenol (S)41 %1 07/15/09 00:45 367-12-407/09/09 10:0025-150
2,4,6-Tribromophenol (S)69 %1 07/15/09 00:45 118-79-607/09/09 10:0025-150
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 07/08/09 17:00 67-64-125.0
Benzene ND ug/L 1 07/08/09 17:00 71-43-21.0
Bromobenzene ND ug/L 1 07/08/09 17:00 108-86-11.0
Bromochloromethane ND ug/L 1 07/08/09 17:00 74-97-51.0
Bromodichloromethane ND ug/L 1 07/08/09 17:00 75-27-41.0
Bromoform ND ug/L 1 07/08/09 17:00 75-25-21.0
Bromomethane ND ug/L 1 07/08/09 17:00 74-83-95.0
2-Butanone (MEK)ND ug/L 1 07/08/09 17:00 78-93-35.0
Carbon tetrachloride ND ug/L 1 07/08/09 17:00 56-23-51.0
Chlorobenzene ND ug/L 1 07/08/09 17:00 108-90-71.0
Chloroethane ND ug/L 1 07/08/09 17:00 75-00-31.0
Chloroform ND ug/L 1 07/08/09 17:00 67-66-31.0
Chloromethane ND ug/L 1 07/08/09 17:00 74-87-31.0
2-Chlorotoluene ND ug/L 1 07/08/09 17:00 95-49-81.0
4-Chlorotoluene ND ug/L 1 07/08/09 17:00 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 07/08/09 17:00 96-12-83.0
Dibromochloromethane ND ug/L 1 07/08/09 17:00 124-48-11.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 101 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TW6-07-09 Lab ID:9247665043 Collected:07/02/09 13:45 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
1,2-Dibromoethane (EDB)ND ug/L 1 07/08/09 17:00 106-93-41.0
Dibromomethane ND ug/L 1 07/08/09 17:00 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 07/08/09 17:00 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 07/08/09 17:00 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 07/08/09 17:00 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 07/08/09 17:00 75-71-81.0
1,1-Dichloroethane ND ug/L 1 07/08/09 17:00 75-34-31.0
1,2-Dichloroethane ND ug/L 1 07/08/09 17:00 107-06-21.0
1,1-Dichloroethene ND ug/L 1 07/08/09 17:00 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 07/08/09 17:00 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 07/08/09 17:00 156-60-51.0
1,2-Dichloropropane ND ug/L 1 07/08/09 17:00 78-87-51.0
1,3-Dichloropropane ND ug/L 1 07/08/09 17:00 142-28-91.0
2,2-Dichloropropane ND ug/L 1 07/08/09 17:00 594-20-71.0
1,1-Dichloropropene ND ug/L 1 07/08/09 17:00 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 07/08/09 17:00 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 07/08/09 17:00 10061-02-61.0
Diisopropyl ether ND ug/L 1 07/08/09 17:00 108-20-31.0
Ethylbenzene ND ug/L 1 07/08/09 17:00 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 07/08/09 17:00 87-68-31.0
2-Hexanone ND ug/L 1 07/08/09 17:00 591-78-65.0
p-Isopropyltoluene ND ug/L 1 07/08/09 17:00 99-87-61.0
Methylene Chloride ND ug/L 1 07/08/09 17:00 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 07/08/09 17:00 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 07/08/09 17:00 1634-04-41.0
Naphthalene ND ug/L 1 07/08/09 17:00 91-20-31.0
Styrene ND ug/L 1 07/08/09 17:00 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 07/08/09 17:00 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 07/08/09 17:00 79-34-51.0
Tetrachloroethene ND ug/L 1 07/08/09 17:00 127-18-41.0
Toluene ND ug/L 1 07/08/09 17:00 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 07/08/09 17:00 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 07/08/09 17:00 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 07/08/09 17:00 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 07/08/09 17:00 79-00-51.0
Trichloroethene ND ug/L 1 07/08/09 17:00 79-01-61.0
Trichlorofluoromethane ND ug/L 1 07/08/09 17:00 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 07/08/09 17:00 96-18-41.0
Vinyl acetate ND ug/L 1 07/08/09 17:00 108-05-42.0
Vinyl chloride ND ug/L 1 07/08/09 17:00 75-01-41.0
m&p-Xylene ND ug/L 1 07/08/09 17:00 1330-20-72.0
o-Xylene ND ug/L 1 07/08/09 17:00 95-47-61.0
4-Bromofluorobenzene (S)98 %1 07/08/09 17:00 460-00-487-109
Dibromofluoromethane (S)109 %1 07/08/09 17:00 1868-53-785-115
1,2-Dichloroethane-d4 (S)107 %1 07/08/09 17:00 17060-07-079-120
Toluene-d8 (S)102 %1 07/08/09 17:00 2037-26-570-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 102 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TRIP BLANK1-07-09 Lab ID:9247665044 Collected:07/02/09 00:00 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 07/08/09 17:19 67-64-125.0
Benzene ND ug/L 1 07/08/09 17:19 71-43-21.0
Bromobenzene ND ug/L 1 07/08/09 17:19 108-86-11.0
Bromochloromethane ND ug/L 1 07/08/09 17:19 74-97-51.0
Bromodichloromethane ND ug/L 1 07/08/09 17:19 75-27-41.0
Bromoform ND ug/L 1 07/08/09 17:19 75-25-21.0
Bromomethane ND ug/L 1 07/08/09 17:19 74-83-95.0
2-Butanone (MEK)ND ug/L 1 07/08/09 17:19 78-93-35.0
Carbon tetrachloride ND ug/L 1 07/08/09 17:19 56-23-51.0
Chlorobenzene ND ug/L 1 07/08/09 17:19 108-90-71.0
Chloroethane ND ug/L 1 07/08/09 17:19 75-00-31.0
Chloroform ND ug/L 1 07/08/09 17:19 67-66-31.0
Chloromethane ND ug/L 1 07/08/09 17:19 74-87-31.0
2-Chlorotoluene ND ug/L 1 07/08/09 17:19 95-49-81.0
4-Chlorotoluene ND ug/L 1 07/08/09 17:19 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 07/08/09 17:19 96-12-83.0
Dibromochloromethane ND ug/L 1 07/08/09 17:19 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 07/08/09 17:19 106-93-41.0
Dibromomethane ND ug/L 1 07/08/09 17:19 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 07/08/09 17:19 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 07/08/09 17:19 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 07/08/09 17:19 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 07/08/09 17:19 75-71-81.0
1,1-Dichloroethane ND ug/L 1 07/08/09 17:19 75-34-31.0
1,2-Dichloroethane ND ug/L 1 07/08/09 17:19 107-06-21.0
1,1-Dichloroethene ND ug/L 1 07/08/09 17:19 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 07/08/09 17:19 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 07/08/09 17:19 156-60-51.0
1,2-Dichloropropane ND ug/L 1 07/08/09 17:19 78-87-51.0
1,3-Dichloropropane ND ug/L 1 07/08/09 17:19 142-28-91.0
2,2-Dichloropropane ND ug/L 1 07/08/09 17:19 594-20-71.0
1,1-Dichloropropene ND ug/L 1 07/08/09 17:19 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 07/08/09 17:19 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 07/08/09 17:19 10061-02-61.0
Diisopropyl ether ND ug/L 1 07/08/09 17:19 108-20-31.0
Ethylbenzene ND ug/L 1 07/08/09 17:19 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 07/08/09 17:19 87-68-31.0
2-Hexanone ND ug/L 1 07/08/09 17:19 591-78-65.0
p-Isopropyltoluene ND ug/L 1 07/08/09 17:19 99-87-61.0
Methylene Chloride ND ug/L 1 07/08/09 17:19 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 07/08/09 17:19 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 07/08/09 17:19 1634-04-41.0
Naphthalene ND ug/L 1 07/08/09 17:19 91-20-31.0
Styrene ND ug/L 1 07/08/09 17:19 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 07/08/09 17:19 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 07/08/09 17:19 79-34-51.0
Tetrachloroethene ND ug/L 1 07/08/09 17:19 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 103 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Sample:SILV-TRIP BLANK1-07-09 Lab ID:9247665044 Collected:07/02/09 00:00 Received:07/02/09 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 07/08/09 17:19 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 07/08/09 17:19 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 07/08/09 17:19 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 07/08/09 17:19 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 07/08/09 17:19 79-00-51.0
Trichloroethene ND ug/L 1 07/08/09 17:19 79-01-61.0
Trichlorofluoromethane ND ug/L 1 07/08/09 17:19 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 07/08/09 17:19 96-18-41.0
Vinyl acetate ND ug/L 1 07/08/09 17:19 108-05-42.0
Vinyl chloride ND ug/L 1 07/08/09 17:19 75-01-41.0
m&p-Xylene ND ug/L 1 07/08/09 17:19 1330-20-72.0
o-Xylene ND ug/L 1 07/08/09 17:19 95-47-61.0
4-Bromofluorobenzene (S)95 %1 07/08/09 17:19 460-00-487-109
Dibromofluoromethane (S)107 %1 07/08/09 17:19 1868-53-785-115
1,2-Dichloroethane-d4 (S)108 %1 07/08/09 17:19 17060-07-079-120
Toluene-d8 (S)103 %1 07/08/09 17:19 2037-26-570-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 104 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/7353
EPA 3546
EPA 8015 Modified
8015 Solid GCSV
Associated Lab Samples:9247665030, 9247665032, 9247665033, 9247665034
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:306322
Associated Lab Samples:9247665030, 9247665032, 9247665033, 9247665034
Matrix:Solid
Analyzed
Diesel Components mg/kg ND 5.0 07/15/09 12:33
n-Pentacosane (S)%76 50-135 07/15/09 12:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
306323LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Components mg/kg 132167 79 50-114
n-Pentacosane (S)%75 50-135
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
306324MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9248249003
306325
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Diesel Components mg/kg P31826750-10768 .3182ND123124
n-Pentacosane (S)%S4050-1350
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 105 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/3333
EPA 5035A/5030B
EPA 8015 Modified
Gasoline Range Organics
Associated Lab Samples:9247665012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:303946
Associated Lab Samples:9247665012
Matrix:Solid
Analyzed
Gasoline Range Organics mg/kg ND 6.0 07/14/09 01:03
4-Bromofluorobenzene (S)%84 50-135 07/14/09 01:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
303947LABORATORY CONTROL SAMPLE:
LCSSpike
Gasoline Range Organics mg/kg 23.925 96 70-150
4-Bromofluorobenzene (S)%89 50-135
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
303987MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9247665012
303988
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Gasoline Range Organics mg/kg 31.6 79 70-14878 131.6ND 25.0 24.7
4-Bromofluorobenzene (S)%81 50-13577
Parameter Units
Dup
Result QualifiersRPDResult
9247856008
303949SAMPLE DUPLICATE:
Gasoline Range Organics mg/kg 2710 22770
4-Bromofluorobenzene (S)%95 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 106 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/7338
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:9247665038, 9247665039, 9247665041, 9247665042, 9247665043
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:305537
Associated Lab Samples:9247665038, 9247665039, 9247665041, 9247665042, 9247665043
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 07/10/09 17:52
1,2-Dichlorobenzene ug/L ND 10.0 07/10/09 17:52
1,2-Diphenylhydrazine ug/L ND 10.0 07/10/09 17:52
1,3-Dichlorobenzene ug/L ND 10.0 07/10/09 17:52
1,4-Dichlorobenzene ug/L ND 10.0 07/10/09 17:52
1-Methylnaphthalene ug/L ND 10.0 07/10/09 17:52
2,4,5-Trichlorophenol ug/L ND 10.0 07/10/09 17:52
2,4,6-Trichlorophenol ug/L ND 10.0 07/10/09 17:52
2,4-Dichlorophenol ug/L ND 10.0 07/10/09 17:52
2,4-Dimethylphenol ug/L ND 10.0 07/10/09 17:52
2,4-Dinitrophenol ug/L ND 50.0 07/10/09 17:52
2,4-Dinitrotoluene ug/L ND 10.0 07/10/09 17:52
2,6-Dinitrotoluene ug/L ND 10.0 07/10/09 17:52
2-Chloronaphthalene ug/L ND 10.0 07/10/09 17:52
2-Chlorophenol ug/L ND 10.0 07/10/09 17:52
2-Methylnaphthalene ug/L ND 10.0 07/10/09 17:52
2-Methylphenol(o-Cresol)ug/L ND 10.0 07/10/09 17:52
2-Nitroaniline ug/L ND 50.0 07/10/09 17:52
2-Nitrophenol ug/L ND 10.0 07/10/09 17:52
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 07/10/09 17:52
3,3'-Dichlorobenzidine ug/L ND 50.0 07/10/09 17:52
3-Nitroaniline ug/L ND 50.0 07/10/09 17:52
4,6-Dinitro-2-methylphenol ug/L ND 20.0 07/10/09 17:52
4-Bromophenylphenyl ether ug/L ND 10.0 07/10/09 17:52
4-Chloro-3-methylphenol ug/L ND 20.0 07/10/09 17:52
4-Chloroaniline ug/L ND 50.0 07/10/09 17:52
4-Chlorophenylphenyl ether ug/L ND 10.0 07/10/09 17:52
4-Nitroaniline ug/L ND 50.0 07/10/09 17:52
4-Nitrophenol ug/L ND 50.0 07/10/09 17:52
Acenaphthene ug/L ND 10.0 07/10/09 17:52
Acenaphthylene ug/L ND 10.0 07/10/09 17:52
Aniline ug/L ND 10.0 07/10/09 17:52
Anthracene ug/L ND 10.0 07/10/09 17:52
Benzo(a)anthracene ug/L ND 10.0 07/10/09 17:52
Benzo(a)pyrene ug/L ND 10.0 07/10/09 17:52
Benzo(b)fluoranthene ug/L ND 10.0 07/10/09 17:52
Benzo(g,h,i)perylene ug/L ND 10.0 07/10/09 17:52
Benzo(k)fluoranthene ug/L ND 10.0 07/10/09 17:52
Benzoic Acid ug/L ND 50.0 07/10/09 17:52
Benzyl alcohol ug/L ND 20.0 07/10/09 17:52
bis(2-Chloroethoxy)methane ug/L ND 10.0 07/10/09 17:52
bis(2-Chloroethyl) ether ug/L ND 10.0 07/10/09 17:52
bis(2-Chloroisopropyl) ether ug/L ND 10.0 07/10/09 17:52
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 107 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:305537
Associated Lab Samples:9247665038, 9247665039, 9247665041, 9247665042, 9247665043
Matrix:Water
Analyzed
bis(2-Ethylhexyl)phthalate ug/L ND 10.0 07/10/09 17:52
Butylbenzylphthalate ug/L ND 10.0 07/10/09 17:52
Chrysene ug/L ND 10.0 07/10/09 17:52
Di-n-butylphthalate ug/L ND 10.0 07/10/09 17:52
Di-n-octylphthalate ug/L ND 10.0 07/10/09 17:52
Dibenz(a,h)anthracene ug/L ND 10.0 07/10/09 17:52
Dibenzofuran ug/L ND 10.0 07/10/09 17:52
Diethylphthalate ug/L ND 10.0 07/10/09 17:52
Dimethylphthalate ug/L ND 10.0 07/10/09 17:52
Fluoranthene ug/L ND 10.0 07/10/09 17:52
Fluorene ug/L ND 10.0 07/10/09 17:52
Hexachloro-1,3-butadiene ug/L ND 10.0 07/10/09 17:52
Hexachlorobenzene ug/L ND 10.0 07/10/09 17:52
Hexachlorocyclopentadiene ug/L ND 10.0 07/10/09 17:52
Hexachloroethane ug/L ND 10.0 07/10/09 17:52
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 07/10/09 17:52
Isophorone ug/L ND 10.0 07/10/09 17:52
N-Nitroso-di-n-propylamine ug/L ND 10.0 07/10/09 17:52
N-Nitrosodimethylamine ug/L ND 10.0 07/10/09 17:52
N-Nitrosodiphenylamine ug/L ND 10.0 07/10/09 17:52
Naphthalene ug/L ND 10.0 07/10/09 17:52
Nitrobenzene ug/L ND 10.0 07/10/09 17:52
Pentachlorophenol ug/L ND 50.0 07/10/09 17:52
Phenanthrene ug/L ND 10.0 07/10/09 17:52
Phenol ug/L ND 10.0 07/10/09 17:52
Pyrene ug/L ND 10.0 07/10/09 17:52
2,4,6-Tribromophenol (S)%57 25-150 07/10/09 17:52
2-Fluorobiphenyl (S)%44 30-150 07/10/09 17:52
2-Fluorophenol (S)%29 25-150 07/10/09 17:52
Nitrobenzene-d5 (S)%39 30-150 07/10/09 17:52
Phenol-d6 (S)%17 25-150 S007/10/09 17:52
Terphenyl-d14 (S)%58 30-150 07/10/09 17:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
305538LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 35.250 70 19-120
1,2-Dichlorobenzene ug/L 32.950 66 19-120
1,2-Diphenylhydrazine ug/L 42.250 84 50-150
1,3-Dichlorobenzene ug/L 30.750 61 15-120
1,4-Dichlorobenzene ug/L 33.050 66 15-120
1-Methylnaphthalene ug/L 46.950 94 21-120
2,4,5-Trichlorophenol ug/L 41.350 83 23-113
2,4,6-Trichlorophenol ug/L 43.950 88 21-113
2,4-Dichlorophenol ug/L 40.750 81 12-127
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 108 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
305538LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dimethylphenol ug/L 35.250 70 24-120
2,4-Dinitrophenol ug/L 48.1J50 96 10-127
2,4-Dinitrotoluene ug/L 41.450 83 36-115
2,6-Dinitrotoluene ug/L 41.950 84 37-114
2-Chloronaphthalene ug/L 38.750 77 36-101
2-Chlorophenol ug/L 32.750 65 24-120
2-Methylnaphthalene ug/L 34.550 69 19-120
2-Methylphenol(o-Cresol)ug/L 28.850 58 25-120
2-Nitroaniline ug/L 42.5J50 85 30-109
2-Nitrophenol ug/L 37.950 76 24-120
3&4-Methylphenol(m&p Cresol)ug/L 28.650 57 24-120
3,3'-Dichlorobenzidine ug/L 48.2J50 96 14-120
3-Nitroaniline ug/L 49.1J50 98 23-133
4,6-Dinitro-2-methylphenol ug/L 40.650 81 10-128
4-Bromophenylphenyl ether ug/L 52.450 105 35-113
4-Chloro-3-methylphenol ug/L 41.150 82 32-107
4-Chloroaniline ug/L 51.150 102 12-150
4-Chlorophenylphenyl ether ug/L 50.850 102 36-110
4-Nitroaniline ug/L 41.8J50 84 12-150
4-Nitrophenol ug/L 60.050 120 10-120
Acenaphthene ug/L 41.350 83 27-102
Acenaphthylene ug/L 44.350 89 25-105
Aniline ug/L 22.050 44 10-150
Anthracene ug/L 45.350 91 30-113
Benzo(a)anthracene ug/L 43.150 86 27-113
Benzo(a)pyrene ug/L 43.550 87 27-119
Benzo(b)fluoranthene ug/L 33.050 66 22-114
Benzo(g,h,i)perylene ug/L 51.850 104 10-129
Benzo(k)fluoranthene ug/L 33.750 67 24-111
Benzoic Acid ug/L ND50 49 24-120
Benzyl alcohol ug/L 31.250 62 24-120
bis(2-Chloroethoxy)methane ug/L 46.550 93 32-120
bis(2-Chloroethyl) ether ug/L 39.550 79 29-120
bis(2-Chloroisopropyl) ether ug/L 39.350 79 22-120
bis(2-Ethylhexyl)phthalate ug/L 46.150 92 29-125
Butylbenzylphthalate ug/L 45.450 91 33-120
Chrysene ug/L 43.250 86 23-112
Di-n-butylphthalate ug/L 46.650 93 38-116
Di-n-octylphthalate ug/L 45.050 90 32-122
Dibenz(a,h)anthracene ug/L 47.350 95 10-129
Dibenzofuran ug/L 42.650 85 37-107
Diethylphthalate ug/L 43.850 88 40-111
Dimethylphthalate ug/L 42.950 86 39-108
Fluoranthene ug/L 43.050 86 27-112
Fluorene ug/L 42.350 85 29-107
Hexachloro-1,3-butadiene ug/L 40.350 81 10-113
Hexachlorobenzene ug/L 42.950 86 29-119
Hexachlorocyclopentadiene ug/L 31.750 63 10-113
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 109 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
305538LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloroethane ug/L 31.050 62 10-120
Indeno(1,2,3-cd)pyrene ug/L 48.250 96 14-123
Isophorone ug/L 41.250 82 23-150
N-Nitroso-di-n-propylamine ug/L 42.250 84 31-104
N-Nitrosodimethylamine ug/L 24.250 48 10-120
N-Nitrosodiphenylamine ug/L 49.550 99 27-139
Naphthalene ug/L 38.750 77 17-120
Nitrobenzene ug/L 45.450 91 27-120
Pentachlorophenol ug/L 32.9J50 66 10-135
Phenanthrene ug/L 39.350 79 28-111
Phenol ug/L 26.650 53 10-120
Pyrene ug/L 41.150 82 27-113
2,4,6-Tribromophenol (S)%85 25-150
2-Fluorobiphenyl (S)%82 30-150
2-Fluorophenol (S)%42 25-150
Nitrobenzene-d5 (S)%78 30-150
Phenol-d6 (S)%37 25-150
Terphenyl-d14 (S)%81 30-150
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
305539MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9247894007
305540
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 100 52 13-12056 7100ND51.8 55.5
1,4-Dichlorobenzene ug/L 100 50 19-12054 7100ND50.4 54.3
2,4-Dinitrotoluene ug/L 100 62 41-10966 7100ND62.0 66.2
2-Chlorophenol ug/L 100 48 33-12050 5100ND48.0 50.5
4-Chloro-3-methylphenol ug/L 100 65 30-10869 6100ND65.2 68.9
4-Nitrophenol ug/L 100 93 10-120102100ND93.4J 102
Acenaphthene ug/L 100 64 27-10172 11100ND64.5 71.7
N-Nitroso-di-n-propylamine ug/L 100 72 34-12079 9100ND72.2 78.7
Pentachlorophenol ug/L 100 48 10-13857100ND48.4J 56.8J
Phenol ug/L 100 53 10-12050 6100ND52.9 49.9
Pyrene ug/L 100 67 31-11069 4100ND67.9 70.6
2,4,6-Tribromophenol (S)%64 25-15072
2-Fluorobiphenyl (S)%59 30-15064
2-Fluorophenol (S)%35 25-15037
Nitrobenzene-d5 (S)%61 30-15064
Phenol-d6 (S)%35 25-15036
Terphenyl-d14 (S)%65 30-15073
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 110 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCSV/5754
9071B ASE
9071B ASE
9071 ASE, Oil and Grease
Associated Lab Samples:9247665001, 9247665002, 9247665003, 9247665004, 9247665005, 9247665006, 9247665009, 9247665012,9247665013, 9247665014, 9247665015, 9247665016, 9247665017, 9247665018, 9247665019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:304756
Associated Lab Samples:9247665001, 9247665002, 9247665003, 9247665004, 9247665005, 9247665006, 9247665009, 9247665012,9247665013, 9247665014, 9247665015, 9247665016, 9247665017, 9247665018, 9247665019
Matrix:Solid
Analyzed
Oil and Grease mg/kg ND 70.0 07/09/09 14:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
304757LABORATORY CONTROL SAMPLE:
LCSSpike
Oil and Grease mg/kg 12701330 95 78-114
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
304758MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9247665012
304759
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Oil and Grease mg/kg P6144014878-114142 3144084729902910
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 111 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/4700
EPA 200.7
EPA 200.7
200.7 MET
Associated Lab Samples:9247665036
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:304349
Associated Lab Samples:9247665036
Matrix:Water
Analyzed
Lead ug/L ND 5.0 07/08/09 20:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
304350LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 498500 100 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
304351MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9247596001
304352
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Lead ug/L 500 94 70-13096 3500ND469481
Parameter Units
Dup
Result QualifiersRPDResult
9247666001
304353SAMPLE DUPLICATE:
Lead ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 112 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/4688
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:9247665001, 9247665002, 9247665003, 9247665006, 9247665007, 9247665008, 9247665010, 9247665011,9247665012, 9247665013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:304093
Associated Lab Samples:9247665001, 9247665002, 9247665003, 9247665006, 9247665007, 9247665008, 9247665010, 9247665011,9247665012, 9247665013
Matrix:Solid
Analyzed
Antimony mg/kg ND 0.50 07/07/09 16:48
Arsenic mg/kg ND 0.50 07/07/09 16:48
Beryllium mg/kg ND 0.10 07/07/09 16:48
Cadmium mg/kg ND 0.10 07/07/09 16:48
Chromium mg/kg ND 0.50 07/07/09 16:48
Copper mg/kg ND 0.50 07/07/09 16:48
Lead mg/kg ND 0.50 07/07/09 16:48
Manganese mg/kg ND 0.50 07/07/09 16:48
Nickel mg/kg ND 0.50 07/07/09 16:48
Selenium mg/kg ND 1.0 07/07/09 16:48
Silver mg/kg ND 0.50 07/07/09 16:48
Thallium mg/kg ND 1.0 07/07/09 16:48
Zinc mg/kg ND 1.0 07/07/09 16:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
304094LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony mg/kg 51.350 103 80-120
Arsenic mg/kg 50.250 100 80-120
Beryllium mg/kg 51.650 103 80-120
Cadmium mg/kg 50.350 101 80-120
Chromium mg/kg 51.450 103 80-120
Copper mg/kg 52.250 104 80-120
Lead mg/kg 50.350 101 80-120
Manganese mg/kg 51.550 103 80-120
Nickel mg/kg 51.050 102 80-120
Selenium mg/kg 50.050 100 80-120
Silver mg/kg 26.025 104 80-120
Thallium mg/kg 47.950 96 80-120
Zinc mg/kg 50.150 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
304097MATRIX SPIKE SAMPLE:
MSSpike
Result
9247665012
Antimony mg/kg 41.749.4 82 75-1251.5
Arsenic mg/kg 44.849.4 90 75-1250.51
Beryllium mg/kg 42.649.4 86 75-1250.22
Cadmium mg/kg 41.949.4 83 75-1251.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 113 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
304097MATRIX SPIKE SAMPLE:
MSSpike
Result
9247665012
Chromium mg/kg 68.549.4 101 75-12518.7
Copper mg/kg 72.349.4 103 75-12521.7
Lead mg/kg 134 M049.4 67 75-125101
Manganese mg/kg 28849.4 102 75-125237
Nickel mg/kg 50.949.4 85 75-1258.8
Selenium mg/kg 46.449.4 92 75-125ND
Silver mg/kg 22.924.6 93 75-125ND
Thallium mg/kg 35.7 M049.4 72 75-125ND
Zinc mg/kg 12949.4 103 75-12578.5
Parameter Units
Dup
Result QualifiersRPDResult
9247665012
304098SAMPLE DUPLICATE:
Antimony mg/kg 1.8 191.5
Arsenic mg/kg .49J0.51
Beryllium mg/kg 0.18 180.22
Cadmium mg/kg 0.74 R1461.2
Chromium mg/kg 16.5 1218.7
Copper mg/kg 21.0 421.7
Lead mg/kg 92.2 9101
Manganese mg/kg 180 R127237
Nickel mg/kg 7.9 118.8
Selenium mg/kg .81JND
Silver mg/kg NDND
Thallium mg/kg .64JND
Zinc mg/kg 66.2 1778.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 114 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCSV/5803
EPA 1664A
EPA 1664A
1664 HEM, Oil and Grease
Associated Lab Samples:9247665022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:308992
Associated Lab Samples:9247665022
Matrix:Water
Analyzed
Oil and Grease mg/L ND 5.0 07/16/09 11:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
308993LABORATORY CONTROL SAMPLE:
LCSSpike
Oil and Grease mg/L 39.640 99 78-114
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
308994MATRIX SPIKE SAMPLE:
MSSpike
Result
9248336001
Oil and Grease mg/L 39.140 91 78-114ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 115 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/4702
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:9247665014, 9247665015, 9247665016, 9247665017, 9247665018, 9247665019, 9247665026, 9247665027,9247665028
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:304416
Associated Lab Samples:9247665014, 9247665015, 9247665016, 9247665017, 9247665018, 9247665019, 9247665026, 9247665027,9247665028
Matrix:Solid
Analyzed
Antimony mg/kg ND 0.50 07/08/09 22:37
Arsenic mg/kg ND 0.50 07/08/09 22:37
Beryllium mg/kg ND 0.10 07/08/09 22:37
Cadmium mg/kg ND 0.10 07/08/09 22:37
Chromium mg/kg ND 0.50 07/08/09 22:37
Copper mg/kg ND 0.50 07/08/09 22:37
Lead mg/kg ND 0.50 07/08/09 22:37
Manganese mg/kg ND 0.50 07/08/09 22:37
Nickel mg/kg ND 0.50 07/08/09 22:37
Selenium mg/kg ND 1.0 07/08/09 22:37
Silver mg/kg ND 0.50 07/08/09 22:37
Thallium mg/kg ND 1.0 07/08/09 22:37
Zinc mg/kg ND 1.0 07/08/09 22:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
304417LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony mg/kg 49.850 100 80-120
Arsenic mg/kg 48.950 98 80-120
Beryllium mg/kg 49.450 99 80-120
Cadmium mg/kg 49.850 100 80-120
Chromium mg/kg 49.150 98 80-120
Copper mg/kg 48.150 96 80-120
Lead mg/kg 48.850 98 80-120
Manganese mg/kg 49.650 99 80-120
Nickel mg/kg 48.950 98 80-120
Selenium mg/kg 48.450 97 80-120
Silver mg/kg 24.625 98 80-120
Thallium mg/kg 47.550 95 80-120
Zinc mg/kg 49.350 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
304420MATRIX SPIKE SAMPLE:
MSSpike
Result
9247665026
Antimony mg/kg 29.7 M043.8 62 75-125ND
Arsenic mg/kg 37.343.8 81 75-125ND
Beryllium mg/kg 36.443.8 80 75-1251.5
Cadmium mg/kg 34.543.8 79 75-125ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 116 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
304420MATRIX SPIKE SAMPLE:
MSSpike
Result
9247665026
Chromium mg/kg 65.443.8 79 75-12530.8
Copper mg/kg 54.843.8 84 75-12517.9
Lead mg/kg 41.943.8 80 75-1256.9
Manganese mg/kg 838 M043.8 -3650 75-1252440
Nickel mg/kg 53.143.8 76 75-12519.5
Selenium mg/kg 37.843.8 80 75-125ND
Silver mg/kg 18.522 84 75-125ND
Thallium mg/kg 33.3 M043.8 74 75-125ND
Zinc mg/kg 11843.8 87 75-12579.8
Parameter Units
Dup
Result QualifiersRPDResult
9247665026
304421SAMPLE DUPLICATE:
Antimony mg/kg 2.4JND
Arsenic mg/kg 2.1JND
Beryllium mg/kg 1.4 21.5
Cadmium mg/kg NDND
Chromium mg/kg 31.2 130.8
Copper mg/kg 18.9 617.9
Lead mg/kg 10.9 R1456.9
Manganese mg/kg 912 R1912440
Nickel mg/kg 19.0 319.5
Selenium mg/kg NDND
Silver mg/kg NDND
Thallium mg/kg NDND
Zinc mg/kg 86.5 879.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 117 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/3327
EPA 5035A/5030B
EPA 8015 Modified
Gasoline Range Organics
Associated Lab Samples:9247665033, 9247665034
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:303089
Associated Lab Samples:9247665033, 9247665034
Matrix:Solid
Analyzed
Gasoline Range Organics mg/kg ND 6.0 07/03/09 03:16
4-Bromofluorobenzene (S)%90 50-135 07/03/09 03:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
303090LABORATORY CONTROL SAMPLE:
LCSSpike
Gasoline Range Organics mg/kg 30.425 122 70-150
4-Bromofluorobenzene (S)%96 50-135
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
303091MATRIX SPIKE SAMPLE:
MSSpike
Result
9247668001
Gasoline Range Organics mg/kg 36.832 109 70-148ND
4-Bromofluorobenzene (S)%95 50-135
Parameter Units
Dup
Result QualifiersRPDResult
9247668002
303092SAMPLE DUPLICATE:
Gasoline Range Organics mg/kg NDND
4-Bromofluorobenzene (S)%92 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 118 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/2247
EPA 245.1
EPA 245.1
245.1 Mercury
Associated Lab Samples:9247665022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:302867
Associated Lab Samples:9247665022
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 07/02/09 17:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
302868LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.82.5 111 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
302869MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9247781001
302870
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 87 70-13085 22.5ND 2.2 2.1
Parameter Units
Dup
Result QualifiersRPDResult
9247781002
302871SAMPLE DUPLICATE:
Mercury ug/L 238 2242
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 119 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/4707
EPA 200.7
EPA 200.7
200.7 MET
Associated Lab Samples:9247665040
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:305112
Associated Lab Samples:9247665040
Matrix:Water
Analyzed
Arsenic ug/L ND 5.0 07/09/09 20:32
Cadmium ug/L ND 1.0 07/09/09 20:32
Chromium ug/L ND 5.0 07/09/09 20:32
Copper ug/L ND 5.0 07/09/09 20:32
Lead ug/L ND 5.0 07/09/09 20:32
Nickel ug/L ND 5.0 07/09/09 20:32
Selenium ug/L ND 10.0 07/09/09 20:32
Silver ug/L ND 5.0 07/09/09 20:32
Zinc ug/L ND 10.0 07/09/09 20:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
305113LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 506500 101 85-115
Cadmium ug/L 516500 103 85-115
Chromium ug/L 524500 105 85-115
Copper ug/L 513500 103 85-115
Lead ug/L 513500 103 85-115
Nickel ug/L 519500 104 85-115
Selenium ug/L 504500 101 85-115
Silver ug/L 261250 104 85-115
Zinc ug/L 519500 104 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
305115MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9247665040
305116
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 97 70-130101 45006.3 493 512
Cadmium ug/L 500 95 70-13098 3500ND474488
Chromium ug/L 500 99 70-130102 250090.8 587 599
Copper ug/L 500 102 70-130104 250093.1 604 614
Lead ug/L 500 90 70-13093 250085.4 536 549
Nickel ug/L 500 96 70-13098 250047.0 526 539
Selenium ug/L 500 97 70-130101 4500ND486507
Silver ug/L 250 100 70-130103 3250ND251258
Zinc ug/L 500 101 70-130104 150060111001120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 120 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
Dup
Result QualifiersRPDResult
9247981001
305114SAMPLE DUPLICATE:
Arsenic ug/L 11.7 912.8
Cadmium ug/L NDND
Chromium ug/L 19.4 318.8
Copper ug/L 6.1 36.3
Lead ug/L NDND
Nickel ug/L 276 1273
Selenium ug/L 4.5J12.2
Silver ug/L .2JND
Zinc ug/L 15.7 215.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 121 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/7344
EPA 3546
EPA 8015 Modified
8015 Solid GCSV
Associated Lab Samples:9247665012, 9247665013, 9247665014, 9247665015, 9247665016, 9247665017, 9247665018, 9247665019,9247665020, 9247665021, 9247665029
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:305779
Associated Lab Samples:9247665012, 9247665013, 9247665014, 9247665015, 9247665016, 9247665017, 9247665018, 9247665019,9247665020, 9247665021, 9247665029
Matrix:Solid
Analyzed
Diesel Components mg/kg ND 5.0 07/14/09 14:12
n-Pentacosane (S)%84 50-135 07/14/09 14:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
305780LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Components mg/kg 100167 60 50-114
n-Pentacosane (S)%60 50-135
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
305781MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9247665012
305782
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Diesel Components mg/kg 271 78 50-10776 227139.1 249 245
n-Pentacosane (S)%102 50-13596
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 122 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/3326
EPA 5035A/5030B
EPA 8015 Modified
Gasoline Range Organics
Associated Lab Samples:9247665013, 9247665014, 9247665015, 9247665016, 9247665017, 9247665018, 9247665019, 9247665020,9247665021, 9247665029, 9247665030, 9247665031, 9247665032
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:303085
Associated Lab Samples:9247665013, 9247665014, 9247665015, 9247665016, 9247665017, 9247665018, 9247665019, 9247665020,9247665021, 9247665029, 9247665030, 9247665031, 9247665032
Matrix:Solid
Analyzed
Gasoline Range Organics mg/kg ND 6.0 07/03/09 06:48
4-Bromofluorobenzene (S)%86 50-135 07/03/09 06:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
303086LABORATORY CONTROL SAMPLE:
LCSSpike
Gasoline Range Organics mg/kg 30.725 123 70-150
4-Bromofluorobenzene (S)%89 50-135
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
303087MATRIX SPIKE SAMPLE:
MSSpike
Result
9247659001
Gasoline Range Organics mg/kg 38.527 111 70-1488.6
4-Bromofluorobenzene (S)%96 50-135
Parameter Units
Dup
Result QualifiersRPDResult
9247659002
303088SAMPLE DUPLICATE:
Gasoline Range Organics mg/kg NDND
4-Bromofluorobenzene (S)%89 .7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 123 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/2572
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:9247665018, 9247665019, 9247665020, 9247665021, 9247665026, 9247665027, 9247665028, 9247665029,9247665030, 9247665031, 9247665032, 9247665033, 9247665034
Parameter Units
Dup
Result QualifiersRPDResult
9247737005
303722SAMPLE DUPLICATE:
Percent Moisture %19.4 119.6
Parameter Units
Dup
Result QualifiersRPDResult
9247891009
303723SAMPLE DUPLICATE:
Percent Moisture %13.5 414.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 124 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/7336
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:9247665012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:305488
Associated Lab Samples:9247665012
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 07/10/09 15:02
1,2-Dichlorobenzene ug/kg ND 330 07/10/09 15:02
1,2-Diphenylhydrazine ug/kg ND 330 07/10/09 15:02
1,3-Dichlorobenzene ug/kg ND 330 07/10/09 15:02
1,4-Dichlorobenzene ug/kg ND 330 07/10/09 15:02
1-Methylnaphthalene ug/kg ND 330 07/10/09 15:02
2,4,5-Trichlorophenol ug/kg ND 330 07/10/09 15:02
2,4,6-Trichlorophenol ug/kg ND 330 07/10/09 15:02
2,4-Dichlorophenol ug/kg ND 330 07/10/09 15:02
2,4-Dimethylphenol ug/kg ND 330 07/10/09 15:02
2,4-Dinitrophenol ug/kg ND 1650 07/10/09 15:02
2,4-Dinitrotoluene ug/kg ND 330 07/10/09 15:02
2,6-Dinitrotoluene ug/kg ND 330 07/10/09 15:02
2-Chloronaphthalene ug/kg ND 330 07/10/09 15:02
2-Chlorophenol ug/kg ND 330 07/10/09 15:02
2-Methylnaphthalene ug/kg ND 330 07/10/09 15:02
2-Methylphenol(o-Cresol)ug/kg ND 330 07/10/09 15:02
2-Nitroaniline ug/kg ND 1650 07/10/09 15:02
2-Nitrophenol ug/kg ND 330 07/10/09 15:02
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 07/10/09 15:02
3,3'-Dichlorobenzidine ug/kg ND 1650 07/10/09 15:02
3-Nitroaniline ug/kg ND 1650 07/10/09 15:02
4,6-Dinitro-2-methylphenol ug/kg ND 660 07/10/09 15:02
4-Bromophenylphenyl ether ug/kg ND 330 07/10/09 15:02
4-Chloro-3-methylphenol ug/kg ND 660 07/10/09 15:02
4-Chloroaniline ug/kg ND 1650 07/10/09 15:02
4-Chlorophenylphenyl ether ug/kg ND 330 07/10/09 15:02
4-Nitroaniline ug/kg ND 660 07/10/09 15:02
4-Nitrophenol ug/kg ND 1650 07/10/09 15:02
Acenaphthene ug/kg ND 330 07/10/09 15:02
Acenaphthylene ug/kg ND 330 07/10/09 15:02
Aniline ug/kg ND 330 07/10/09 15:02
Anthracene ug/kg ND 330 07/10/09 15:02
Benzo(a)anthracene ug/kg ND 330 07/10/09 15:02
Benzo(a)pyrene ug/kg ND 330 07/10/09 15:02
Benzo(b)fluoranthene ug/kg ND 330 07/10/09 15:02
Benzo(g,h,i)perylene ug/kg ND 330 07/10/09 15:02
Benzo(k)fluoranthene ug/kg ND 330 07/10/09 15:02
Benzoic Acid ug/kg ND 1650 07/10/09 15:02
Benzyl alcohol ug/kg ND 660 07/10/09 15:02
bis(2-Chloroethoxy)methane ug/kg ND 330 07/10/09 15:02
bis(2-Chloroethyl) ether ug/kg ND 330 07/10/09 15:02
bis(2-Chloroisopropyl) ether ug/kg ND 330 07/10/09 15:02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 125 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:305488
Associated Lab Samples:9247665012
Matrix:Solid
Analyzed
bis(2-Ethylhexyl)phthalate ug/kg ND 330 07/10/09 15:02
Butylbenzylphthalate ug/kg ND 330 07/10/09 15:02
Chrysene ug/kg ND 330 07/10/09 15:02
Di-n-butylphthalate ug/kg ND 330 07/10/09 15:02
Di-n-octylphthalate ug/kg ND 330 07/10/09 15:02
Dibenz(a,h)anthracene ug/kg ND 330 07/10/09 15:02
Dibenzofuran ug/kg ND 330 07/10/09 15:02
Diethylphthalate ug/kg ND 330 07/10/09 15:02
Dimethylphthalate ug/kg ND 330 07/10/09 15:02
Fluoranthene ug/kg ND 330 07/10/09 15:02
Fluorene ug/kg ND 330 07/10/09 15:02
Hexachloro-1,3-butadiene ug/kg ND 330 07/10/09 15:02
Hexachlorobenzene ug/kg ND 330 07/10/09 15:02
Hexachlorocyclopentadiene ug/kg ND 330 07/10/09 15:02
Hexachloroethane ug/kg ND 330 07/10/09 15:02
Indeno(1,2,3-cd)pyrene ug/kg ND 330 07/10/09 15:02
Isophorone ug/kg ND 330 07/10/09 15:02
N-Nitroso-di-n-propylamine ug/kg ND 330 07/10/09 15:02
N-Nitrosodimethylamine ug/kg ND 330 07/10/09 15:02
N-Nitrosodiphenylamine ug/kg ND 330 07/10/09 15:02
Naphthalene ug/kg ND 330 07/10/09 15:02
Nitrobenzene ug/kg ND 330 07/10/09 15:02
Pentachlorophenol ug/kg ND 1650 07/10/09 15:02
Phenanthrene ug/kg ND 330 07/10/09 15:02
Phenol ug/kg ND 330 07/10/09 15:02
Pyrene ug/kg ND 330 07/10/09 15:02
2,4,6-Tribromophenol (S)%53 44-136 07/10/09 15:02
2-Fluorobiphenyl (S)%71 46-120 07/10/09 15:02
2-Fluorophenol (S)%75 24-120 07/10/09 15:02
Nitrobenzene-d5 (S)%66 30-150 07/10/09 15:02
Phenol-d6 (S)%64 35-120 07/10/09 15:02
Terphenyl-d14 (S)%98 38-108 07/10/09 15:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
305489LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 11401670 68 50-150
1,2-Dichlorobenzene ug/kg 10801670 65 50-150
1,2-Diphenylhydrazine ug/kg 12401670 74 43-130
1,3-Dichlorobenzene ug/kg 11001670 66 50-150
1,4-Dichlorobenzene ug/kg 10701670 64 50-150
1-Methylnaphthalene ug/kg 9691670 58 50-150
2,4,5-Trichlorophenol ug/kg 15101670 91 50-150
2,4,6-Trichlorophenol ug/kg 8481670 51 50-150
2,4-Dichlorophenol ug/kg 10301670 62 50-150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 126 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
305489LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dimethylphenol ug/kg 8681670 52 50-150
2,4-Dinitrophenol ug/kg 1280J1670 77 20-111
2,4-Dinitrotoluene ug/kg 14701670 88 50-150
2,6-Dinitrotoluene ug/kg 12401670 75 50-150
2-Chloronaphthalene ug/kg 15701670 94 50-150
2-Chlorophenol ug/kg 11101670 67 50-150
2-Methylnaphthalene ug/kg 9891670 59 50-150
2-Methylphenol(o-Cresol)ug/kg 9481670 57 50-150
2-Nitroaniline ug/kg 1400J1670 84 50-150
2-Nitrophenol ug/kg 10701670 64 50-150
3&4-Methylphenol(m&p Cresol)ug/kg 9901670 59 50-150
3,3'-Dichlorobenzidine ug/kg 1540J1670 92 50-150
3-Nitroaniline ug/kg 17101670 103 50-150
4,6-Dinitro-2-methylphenol ug/kg 9591670 58 15-136
4-Bromophenylphenyl ether ug/kg 15501670 93 50-150
4-Chloro-3-methylphenol ug/kg 9981670 60 50-150
4-Chloroaniline ug/kg 1340J1670 80 50-150
4-Chlorophenylphenyl ether ug/kg 15601670 93 50-150
4-Nitroaniline ug/kg 15701670 94 50-150
4-Nitrophenol ug/kg 1300J1670 78 33-105
Acenaphthene ug/kg 13101670 79 50-150
Acenaphthylene ug/kg 14901670 89 50-150
Aniline ug/kg 12001670 72 50-150
Anthracene ug/kg 17901670 108 50-150
Benzo(a)anthracene ug/kg 15501670 93 50-150
Benzo(a)pyrene ug/kg 14201670 85 50-150
Benzo(b)fluoranthene ug/kg 9851670 59 50-150
Benzo(g,h,i)perylene ug/kg 16501670 99 24-117
Benzo(k)fluoranthene ug/kg 9871670 59 50-150
Benzoic Acid ug/kg 775J1670 46 15-104
Benzyl alcohol ug/kg 12501670 75 50-150
bis(2-Chloroethoxy)methane ug/kg 9031670 54 50-150
bis(2-Chloroethyl) ether ug/kg 10501670 63 50-150
bis(2-Chloroisopropyl) ether ug/kg 11101670 66 50-150
bis(2-Ethylhexyl)phthalate ug/kg 18301670 110 50-150
Butylbenzylphthalate ug/kg 16201670 97 50-150
Chrysene ug/kg 18001670 108 50-150
Di-n-butylphthalate ug/kg 18501670 111 50-150
Di-n-octylphthalate ug/kg 15401670 92 50-150
Dibenz(a,h)anthracene ug/kg 16201670 97 17-128
Dibenzofuran ug/kg 14401670 86 50-150
Diethylphthalate ug/kg 14501670 87 50-150
Dimethylphthalate ug/kg 12701670 76 50-150
Fluoranthene ug/kg 18001670 108 50-150
Fluorene ug/kg 14101670 85 50-150
Hexachloro-1,3-butadiene ug/kg 11401670 68 50-150
Hexachlorobenzene ug/kg 13001670 78 50-150
Hexachlorocyclopentadiene ug/kg 12601670 75 15-114
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 127 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
305489LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloroethane ug/kg 10601670 64 50-150
Indeno(1,2,3-cd)pyrene ug/kg 16501670 99 19-128
Isophorone ug/kg 10801670 65 50-150
N-Nitroso-di-n-propylamine ug/kg 11101670 67 50-150
N-Nitrosodimethylamine ug/kg 12401670 74 50-150
N-Nitrosodiphenylamine ug/kg 15301670 92 50-150
Naphthalene ug/kg 10201670 61 50-150
Nitrobenzene ug/kg 8321670 50 50-150
Pentachlorophenol ug/kg 1140J1670 69 15-130
Phenanthrene ug/kg 17501670 105 50-150
Phenol ug/kg 12701670 76 42-120
Pyrene ug/kg 17301670 104 50-150
2,4,6-Tribromophenol (S)%69 44-136
2-Fluorobiphenyl (S)%75 46-120
2-Fluorophenol (S)%79 24-120
Nitrobenzene-d5 (S)%67 30-150
Phenol-d6 (S)%75 35-120
Terphenyl-d14 (S)%90 38-108
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
305768MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9247665012
305769
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1810 59 50-15056 51810ND10701010
1,4-Dichlorobenzene ug/kg 1810 51 50-15051 .31810ND928925
2,4-Dinitrotoluene ug/kg 1810 52 50-15052 .11810ND941943
2-Chlorophenol ug/kg 1810 56 50-15052 91810ND1020933
4-Chloro-3-methylphenol ug/kg 1810 60 50-15056 61810ND10901020
4-Nitrophenol ug/kg 1810 53 50-150501810ND962J913J
Acenaphthene ug/kg 1810 69 50-15064 71810ND12401160
N-Nitroso-di-n-propylamine ug/kg 1810 54 50-15060 91810ND9831080
Pentachlorophenol ug/kg 1810 55 50-150551810ND1000J988J
Phenol ug/kg 1810 54 50-15051 41810ND968927
Pyrene ug/kg 1810 95 50-15090 51810ND18101710
2,4,6-Tribromophenol (S)%47 44-13652
2-Fluorobiphenyl (S)%55 46-12063
2-Fluorophenol (S)%36 24-12055
Nitrobenzene-d5 (S)%59 30-15053
Phenol-d6 (S)%39 35-12054
Terphenyl-d14 (S)%51 38-108100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 128 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/7576
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:9247665023, 9247665024, 9247665025, 9247665036
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:304252
Associated Lab Samples:9247665023, 9247665024, 9247665025, 9247665036
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 07/07/09 10:19
1,1,1-Trichloroethane ug/L ND 1.0 07/07/09 10:19
1,1,2,2-Tetrachloroethane ug/L ND 1.0 07/07/09 10:19
1,1,2-Trichloroethane ug/L ND 1.0 07/07/09 10:19
1,1-Dichloroethane ug/L ND 1.0 07/07/09 10:19
1,1-Dichloroethene ug/L ND 1.0 07/07/09 10:19
1,1-Dichloropropene ug/L ND 1.0 07/07/09 10:19
1,2,3-Trichlorobenzene ug/L ND 1.0 07/07/09 10:19
1,2,3-Trichloropropane ug/L ND 1.0 07/07/09 10:19
1,2,4-Trichlorobenzene ug/L ND 1.0 07/07/09 10:19
1,2-Dibromo-3-chloropropane ug/L ND 3.0 07/07/09 10:19
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/07/09 10:19
1,2-Dichlorobenzene ug/L ND 1.0 07/07/09 10:19
1,2-Dichloroethane ug/L ND 1.0 07/07/09 10:19
1,2-Dichloropropane ug/L ND 1.0 07/07/09 10:19
1,3-Dichlorobenzene ug/L ND 1.0 07/07/09 10:19
1,3-Dichloropropane ug/L ND 1.0 07/07/09 10:19
1,4-Dichlorobenzene ug/L ND 1.0 07/07/09 10:19
2,2-Dichloropropane ug/L ND 1.0 07/07/09 10:19
2-Butanone (MEK)ug/L ND 5.0 07/07/09 10:19
2-Chlorotoluene ug/L ND 1.0 07/07/09 10:19
2-Hexanone ug/L ND 5.0 07/07/09 10:19
4-Chlorotoluene ug/L ND 1.0 07/07/09 10:19
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 07/07/09 10:19
Acetone ug/L ND 25.0 07/07/09 10:19
Benzene ug/L ND 1.0 07/07/09 10:19
Bromobenzene ug/L ND 1.0 07/07/09 10:19
Bromochloromethane ug/L ND 1.0 07/07/09 10:19
Bromodichloromethane ug/L ND 1.0 07/07/09 10:19
Bromoform ug/L ND 1.0 07/07/09 10:19
Bromomethane ug/L ND 5.0 07/07/09 10:19
Carbon tetrachloride ug/L ND 1.0 07/07/09 10:19
Chlorobenzene ug/L ND 1.0 07/07/09 10:19
Chloroethane ug/L ND 1.0 07/07/09 10:19
Chloroform ug/L ND 1.0 07/07/09 10:19
Chloromethane ug/L ND 1.0 07/07/09 10:19
cis-1,2-Dichloroethene ug/L ND 1.0 07/07/09 10:19
cis-1,3-Dichloropropene ug/L ND 1.0 07/07/09 10:19
Dibromochloromethane ug/L ND 1.0 07/07/09 10:19
Dibromomethane ug/L ND 1.0 07/07/09 10:19
Dichlorodifluoromethane ug/L ND 1.0 07/07/09 10:19
Diisopropyl ether ug/L ND 1.0 07/07/09 10:19
Ethylbenzene ug/L ND 1.0 07/07/09 10:19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 129 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:304252
Associated Lab Samples:9247665023, 9247665024, 9247665025, 9247665036
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 1.0 07/07/09 10:19
m&p-Xylene ug/L ND 2.0 07/07/09 10:19
Methyl-tert-butyl ether ug/L ND 1.0 07/07/09 10:19
Methylene Chloride ug/L 3.1 2.0 C907/07/09 10:19
Naphthalene ug/L ND 1.0 07/07/09 10:19
o-Xylene ug/L ND 1.0 07/07/09 10:19
p-Isopropyltoluene ug/L ND 1.0 07/07/09 10:19
Styrene ug/L ND 1.0 07/07/09 10:19
Tetrachloroethene ug/L ND 1.0 07/07/09 10:19
Toluene ug/L ND 1.0 07/07/09 10:19
trans-1,2-Dichloroethene ug/L ND 1.0 07/07/09 10:19
trans-1,3-Dichloropropene ug/L ND 1.0 07/07/09 10:19
Trichloroethene ug/L ND 1.0 07/07/09 10:19
Trichlorofluoromethane ug/L ND 1.0 07/07/09 10:19
Vinyl acetate ug/L ND 2.0 07/07/09 10:19
Vinyl chloride ug/L ND 1.0 07/07/09 10:19
1,2-Dichloroethane-d4 (S)%104 79-120 07/07/09 10:19
4-Bromofluorobenzene (S)%96 87-109 07/07/09 10:19
Dibromofluoromethane (S)%107 85-115 07/07/09 10:19
Toluene-d8 (S)%102 70-120 07/07/09 10:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
304253LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.850 104 83-125
1,1,1-Trichloroethane ug/L 60.250 120 80-129
1,1,2,2-Tetrachloroethane ug/L 52.050 104 73-127
1,1,2-Trichloroethane ug/L 55.150 110 77-123
1,1-Dichloroethane ug/L 67.2 L05013476-129
1,1-Dichloroethene ug/L 54.750 109 78-146
1,1-Dichloropropene ug/L 54.150 108 79-134
1,2,3-Trichlorobenzene ug/L 53.750 107 70-150
1,2,3-Trichloropropane ug/L 52.050 104 72-125
1,2,4-Trichlorobenzene ug/L 53.750 107 68-127
1,2-Dibromo-3-chloropropane ug/L 51.350 103 65-128
1,2-Dibromoethane (EDB)ug/L 54.050 108 81-125
1,2-Dichlorobenzene ug/L 53.650 107 82-126
1,2-Dichloroethane ug/L 54.350 109 72-126
1,2-Dichloropropane ug/L 53.750 107 80-127
1,3-Dichlorobenzene ug/L 53.650 107 82-124
1,3-Dichloropropane ug/L 53.750 107 79-124
1,4-Dichlorobenzene ug/L 52.250 104 79-125
2,2-Dichloropropane ug/L 65.950 132 58-140
2-Butanone (MEK)ug/L 109100 109 50-134
2-Chlorotoluene ug/L 52.750 105 81-126
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 130 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
304253LABORATORY CONTROL SAMPLE:
LCSSpike
2-Hexanone ug/L 106100 106 58-138
4-Chlorotoluene ug/L 55.850 112 82-126
4-Methyl-2-pentanone (MIBK)ug/L 95.9100 96 70-131
Acetone ug/L 91.6100 92 50-146
Benzene ug/L 54.250 108 78-128
Bromobenzene ug/L 51.950 104 81-127
Bromochloromethane ug/L 55.650 111 73-124
Bromodichloromethane ug/L 51.350 103 81-125
Bromoform ug/L 50.650 101 71-125
Bromomethane ug/L 60.250 120 50-150
Carbon tetrachloride ug/L 57.950 116 81-137
Chlorobenzene ug/L 53.950 108 82-126
Chloroethane ug/L 45.350 91 69-140
Chloroform ug/L 57.350 115 77-129
Chloromethane ug/L 40.050 80 54-139
cis-1,2-Dichloroethene ug/L 53.450 107 76-133
cis-1,3-Dichloropropene ug/L 49.050 98 76-127
Dibromochloromethane ug/L 51.150 102 77-125
Dibromomethane ug/L 56.350 113 77-125
Dichlorodifluoromethane ug/L 34.050 68 50-150
Diisopropyl ether ug/L 53.450 107 74-131
Ethylbenzene ug/L 52.550 105 80-127
Hexachloro-1,3-butadiene ug/L 52.250 104 78-145
m&p-Xylene ug/L 106100 106 82-127
Methyl-tert-butyl ether ug/L 53.650 107 71-130
Methylene Chloride ug/L 62.050 124 67-133
Naphthalene ug/L 49.050 98 52-136
o-Xylene ug/L 53.250 106 83-124
p-Isopropyltoluene ug/L 53.850 108 73-122
Styrene ug/L 48.350 97 80-130
Tetrachloroethene ug/L 53.950 108 78-128
Toluene ug/L 51.150 102 76-126
trans-1,2-Dichloroethene ug/L 51.350 103 78-134
trans-1,3-Dichloropropene ug/L 47.750 95 75-125
Trichloroethene ug/L 53.050 106 79-127
Trichlorofluoromethane ug/L 45.950 92 76-148
Vinyl acetate ug/L 68.9100 69 50-150
Vinyl chloride ug/L 48.550 97 67-143
1,2-Dichloroethane-d4 (S)%99 79-120
4-Bromofluorobenzene (S)%101 87-109
Dibromofluoromethane (S)%101 85-115
Toluene-d8 (S)%100 70-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 131 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
304254MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9247599003
304255
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 50 146 60-150146 .450ND73.0 72.8
Benzene ug/L 50 131 74-136130 .850ND65.6 65.1
Chlorobenzene ug/L 50 124 79-135124 .150ND62.1 62.2
Toluene ug/L 50 124 73-131123 .450ND61.8 61.6
Trichloroethene ug/L 50 118 73-131117 .550ND58.9 58.6
1,2-Dichloroethane-d4 (S)%106 79-120105
4-Bromofluorobenzene (S)%94 87-10995
Dibromofluoromethane (S)%107 85-115105
Toluene-d8 (S)%99 70-12099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 132 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/2258
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:9247665002, 9247665003, 9247665010, 9247665011, 9247665012, 9247665013, 9247665014, 9247665015,9247665016, 9247665017, 9247665018, 9247665019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:305958
Associated Lab Samples:9247665002, 9247665003, 9247665010, 9247665011, 9247665012, 9247665013, 9247665014, 9247665015,9247665016, 9247665017, 9247665018, 9247665019
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0050 07/13/09 12:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
305959LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.065.067 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
305960MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9247665012
305961
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/kg M0.064 60 75-12552 4.0670.040 0.078 0.076
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 133 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/4682
EPA 200.7
EPA 200.7
200.7 MET
Associated Lab Samples:9247665022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:302889
Associated Lab Samples:9247665022
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 07/02/09 21:28
Arsenic ug/L ND 5.0 07/02/09 21:28
Beryllium ug/L ND 1.0 07/02/09 21:28
Cadmium ug/L ND 1.0 07/02/09 21:28
Chromium ug/L ND 5.0 07/02/09 21:28
Copper ug/L ND 5.0 07/02/09 21:28
Lead ug/L ND 5.0 07/02/09 21:28
Manganese ug/L ND 5.0 07/02/09 21:28
Nickel ug/L ND 5.0 07/02/09 21:28
Selenium ug/L ND 10.0 07/02/09 21:28
Silver ug/L ND 5.0 07/02/09 21:28
Thallium ug/L ND 10.0 07/02/09 21:28
Zinc ug/L ND 10.0 07/02/09 21:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
302890LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 16001670 96 85-115
Arsenic ug/L 15901670 95 85-115
Beryllium ug/L 15101670 91 85-115
Cadmium ug/L 15501670 93 85-115
Chromium ug/L 16001670 96 85-115
Copper ug/L 15501670 93 85-115
Lead ug/L 15201670 91 85-115
Manganese ug/L 15301670 92 85-115
Nickel ug/L 15401670 92 85-115
Selenium ug/L 15601670 94 85-115
Silver ug/L 794833 95 85-115
Thallium ug/L 14601670 87 85-115
Zinc ug/L 15701670 94 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
302891MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9247152003
302892
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 1670 106 70-130108 21670ND17701800
Arsenic ug/L 1670 115 70-130117 216700.0058mg/L 1930 1960
Beryllium ug/L 1670 90 70-13091 .71670ND15001510
Cadmium ug/L 1670 90 70-13091 .71670ND15101520
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 134 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
302891MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9247152003
302892
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chromium ug/L 1670 96 70-13098 116700.026mg/L 1630 1650
Copper ug/L 1670 100 70-130102 216700.020mg/L 1680 1720
Lead ug/L 1670 83 70-13084 11670ND13901410
Manganese ug/L 1670 90 70-13091 116700.097mg/L 1600 1620
Nickel ug/L 1670 89 70-13089 .516700.64mg/L 2120 2140
Selenium ug/L 1670 126 70-130128 21670ND20902140
Silver ug/L 833 113 70-130115 2833ND942960
Thallium ug/L 1670 74 70-13074 11670ND12301240
Zinc ug/L 1670 112 70-130113 116700.33mg/L 2200 2220
Parameter Units
Dup
Result QualifiersRPDResult
9247718008
302893SAMPLE DUPLICATE:
Antimony ug/L NDND
Arsenic ug/L 14.0 120.012 mg/L
Beryllium ug/L NDND
Cadmium ug/L NDND
Chromium ug/L .91JND
Copper ug/L 861 20.88 mg/L
Lead ug/L NDND
Manganese ug/L 331 10.34 mg/L
Nickel ug/L 13.0 40.012 mg/L
Selenium ug/L NDND
Silver ug/L 1.6JND
Thallium ug/L NDND
Zinc ug/L 6.2JND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 135 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/7544
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:9247665002, 9247665007, 9247665008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:303680
Associated Lab Samples:9247665002, 9247665007, 9247665008
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/06/09 10:35
1,1,1-Trichloroethane ug/kg ND 5.0 07/06/09 10:35
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/06/09 10:35
1,1,2-Trichloroethane ug/kg ND 5.0 07/06/09 10:35
1,1-Dichloroethane ug/kg ND 5.0 07/06/09 10:35
1,1-Dichloroethene ug/kg ND 5.0 07/06/09 10:35
1,1-Dichloropropene ug/kg ND 5.0 07/06/09 10:35
1,2,3-Trichlorobenzene ug/kg ND 5.0 07/06/09 10:35
1,2,3-Trichloropropane ug/kg ND 5.0 07/06/09 10:35
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/06/09 10:35
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/06/09 10:35
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 07/06/09 10:35
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/06/09 10:35
1,2-Dichlorobenzene ug/kg ND 5.0 07/06/09 10:35
1,2-Dichloroethane ug/kg ND 5.0 07/06/09 10:35
1,2-Dichloropropane ug/kg ND 5.0 07/06/09 10:35
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/06/09 10:35
1,3-Dichlorobenzene ug/kg ND 5.0 07/06/09 10:35
1,3-Dichloropropane ug/kg ND 5.0 07/06/09 10:35
1,4-Dichlorobenzene ug/kg ND 5.0 07/06/09 10:35
2,2-Dichloropropane ug/kg ND 5.0 07/06/09 10:35
2-Butanone (MEK)ug/kg ND 100 07/06/09 10:35
2-Chlorotoluene ug/kg ND 5.0 07/06/09 10:35
2-Hexanone ug/kg ND 50.0 07/06/09 10:35
4-Chlorotoluene ug/kg ND 5.0 07/06/09 10:35
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/06/09 10:35
Acetone ug/kg ND 100 07/06/09 10:35
Benzene ug/kg ND 5.0 07/06/09 10:35
Bromobenzene ug/kg ND 5.0 07/06/09 10:35
Bromochloromethane ug/kg ND 5.0 07/06/09 10:35
Bromodichloromethane ug/kg ND 5.0 07/06/09 10:35
Bromoform ug/kg ND 5.0 07/06/09 10:35
Bromomethane ug/kg ND 10.0 07/06/09 10:35
Carbon tetrachloride ug/kg ND 5.0 07/06/09 10:35
Chlorobenzene ug/kg ND 5.0 07/06/09 10:35
Chloroethane ug/kg ND 10.0 07/06/09 10:35
Chloroform ug/kg ND 5.0 07/06/09 10:35
Chloromethane ug/kg ND 10.0 07/06/09 10:35
cis-1,2-Dichloroethene ug/kg ND 5.0 07/06/09 10:35
cis-1,3-Dichloropropene ug/kg ND 5.0 07/06/09 10:35
Dibromochloromethane ug/kg ND 5.0 07/06/09 10:35
Dibromomethane ug/kg ND 5.0 07/06/09 10:35
Dichlorodifluoromethane ug/kg ND 10.0 07/06/09 10:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 136 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:303680
Associated Lab Samples:9247665002, 9247665007, 9247665008
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.0 07/06/09 10:35
Ethylbenzene ug/kg ND 5.0 07/06/09 10:35
Hexachloro-1,3-butadiene ug/kg ND 5.0 07/06/09 10:35
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/06/09 10:35
m&p-Xylene ug/kg ND 10.0 07/06/09 10:35
Methyl-tert-butyl ether ug/kg ND 5.0 07/06/09 10:35
Methylene Chloride ug/kg ND 20.0 07/06/09 10:35
n-Butylbenzene ug/kg ND 5.0 07/06/09 10:35
n-Propylbenzene ug/kg ND 5.0 07/06/09 10:35
Naphthalene ug/kg ND 5.0 07/06/09 10:35
o-Xylene ug/kg ND 5.0 07/06/09 10:35
p-Isopropyltoluene ug/kg ND 5.0 07/06/09 10:35
sec-Butylbenzene ug/kg ND 5.0 07/06/09 10:35
Styrene ug/kg ND 5.0 07/06/09 10:35
tert-Butylbenzene ug/kg ND 5.0 07/06/09 10:35
Tetrachloroethene ug/kg ND 5.0 07/06/09 10:35
Toluene ug/kg ND 5.0 07/06/09 10:35
trans-1,2-Dichloroethene ug/kg ND 5.0 07/06/09 10:35
trans-1,3-Dichloropropene ug/kg ND 5.0 07/06/09 10:35
Trichloroethene ug/kg ND 5.0 07/06/09 10:35
Trichlorofluoromethane ug/kg ND 5.0 07/06/09 10:35
Vinyl acetate ug/kg ND 50.0 07/06/09 10:35
Vinyl chloride ug/kg ND 10.0 07/06/09 10:35
Xylene (Total)ug/kg ND 10.0 07/06/09 10:35
1,2-Dichloroethane-d4 (S)%95 69-121 07/06/09 10:35
4-Bromofluorobenzene (S)%102 74-115 07/06/09 10:35
Dibromofluoromethane (S)%101 79-116 07/06/09 10:35
Toluene-d8 (S)%99 88-110 07/06/09 10:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
303681LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 54.850 110 75-137
1,1,1-Trichloroethane ug/kg 58.750 117 70-140
1,1,2,2-Tetrachloroethane ug/kg 53.350 107 74-133
1,1,2-Trichloroethane ug/kg 55.850 112 79-129
1,1-Dichloroethane ug/kg 64.350 129 72-139
1,1-Dichloroethene ug/kg 52.450 105 69-154
1,1-Dichloropropene ug/kg 51.950 104 74-138
1,2,3-Trichlorobenzene ug/kg 49.250 98 71-150
1,2,3-Trichloropropane ug/kg 51.850 104 74-135
1,2,4-Trichlorobenzene ug/kg 51.450 103 68-150
1,2,4-Trimethylbenzene ug/kg 52.150 104 70-130
1,2-Dibromo-3-chloropropane ug/kg 42.250 84 65-146
1,2-Dibromoethane (EDB)ug/kg 56.650 113 77-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 137 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
303681LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 50.950 102 75-141
1,2-Dichloroethane ug/kg 50.250 100 74-134
1,2-Dichloropropane ug/kg 52.550 105 77-138
1,3,5-Trimethylbenzene ug/kg 50.750 101 65-128
1,3-Dichlorobenzene ug/kg 54.650 109 76-133
1,3-Dichloropropane ug/kg 53.550 107 79-132
1,4-Dichlorobenzene ug/kg 49.350 99 75-137
2,2-Dichloropropane ug/kg 60.350 121 73-137
2-Butanone (MEK)ug/kg 99.4J100 99 61-138
2-Chlorotoluene ug/kg 52.950 106 73-138
2-Hexanone ug/kg 99.9100 100 58-159
4-Chlorotoluene ug/kg 54.950 110 75-136
4-Methyl-2-pentanone (MIBK)ug/kg 99.1100 99 74-139
Acetone ug/kg 107100 107 58-150
Benzene ug/kg 54.550 109 71-140
Bromobenzene ug/kg 50.750 101 72-144
Bromochloromethane ug/kg 63.450 127 78-133
Bromodichloromethane ug/kg 52.250 104 78-133
Bromoform ug/kg 54.350 109 74-132
Bromomethane ug/kg 35.050 70 63-184
Carbon tetrachloride ug/kg 58.550 117 73-143
Chlorobenzene ug/kg 57.050 114 77-137
Chloroethane ug/kg 41.450 83 68-146
Chloroform ug/kg 55.450 111 75-137
Chloromethane ug/kg 43.550 87 54-143
cis-1,2-Dichloroethene ug/kg 51.350 103 71-143
cis-1,3-Dichloropropene ug/kg 54.050 108 76-133
Dibromochloromethane ug/kg 53.250 106 77-131
Dibromomethane ug/kg 60.650 121 63-184
Dichlorodifluoromethane ug/kg 33.750 67 36-173
Diisopropyl ether ug/kg 50.050 100 68-144
Ethylbenzene ug/kg 54.350 109 69-141
Hexachloro-1,3-butadiene ug/kg 47.850 96 70-152
Isopropylbenzene (Cumene)ug/kg 54.150 108 77-143
m&p-Xylene ug/kg 106100 106 72-138
Methyl-tert-butyl ether ug/kg 52.750 105 2-138
Methylene Chloride ug/kg 57.250 114 69-136
n-Butylbenzene ug/kg 50.350 101 65-128
n-Propylbenzene ug/kg 52.050 104 72-139
Naphthalene ug/kg 50.050 100 61-138
o-Xylene ug/kg 53.150 106 74-137
p-Isopropyltoluene ug/kg 51.950 104 66-128
sec-Butylbenzene ug/kg 50.950 102 72-140
Styrene ug/kg 55.750 111 76-137
tert-Butylbenzene ug/kg 51.350 103 68-141
Tetrachloroethene ug/kg 57.450 115 72-136
Toluene ug/kg 52.650 105 69-139
trans-1,2-Dichloroethene ug/kg 49.550 99 72-144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 138 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
303681LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 51.950 104 73-135
Trichloroethene ug/kg 56.350 113 75-136
Trichlorofluoromethane ug/kg 45.350 91 69-144
Vinyl acetate ug/kg 100100 100 50-150
Vinyl chloride ug/kg 45.750 91 61-145
Xylene (Total)ug/kg 159150 106 73-138
1,2-Dichloroethane-d4 (S)%89 69-121
4-Bromofluorobenzene (S)%106 74-115
Dibromofluoromethane (S)%98 79-116
Toluene-d8 (S)%100 88-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 139 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/7314
EPA 3510
EPA 8015 Modified
8015 GCS
Associated Lab Samples:9247665022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:304166
Associated Lab Samples:9247665022
Matrix:Water
Analyzed
Diesel Components mg/L ND 0.10 07/09/09 18:56
n-Pentacosane (S)%85 50-135 07/09/09 18:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
304167LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Components mg/L 4.15 83 50-110
n-Pentacosane (S)%86 50-135
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
304405MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9247844002
304406
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Diesel Components mg/L 12.5 58 50-11250 1512.5ND 7.3 6.3
n-Pentacosane (S)%62 50-13559
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 140 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/7278
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:9247665013, 9247665014, 9247665015, 9247665016, 9247665017, 9247665018, 9247665019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:302311
Associated Lab Samples:9247665013, 9247665014, 9247665015, 9247665016, 9247665017, 9247665018, 9247665019
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 07/08/09 18:32
1,2-Dichlorobenzene ug/kg ND 330 07/08/09 18:32
1,2-Diphenylhydrazine ug/kg ND 330 07/08/09 18:32
1,3-Dichlorobenzene ug/kg ND 330 07/08/09 18:32
1,4-Dichlorobenzene ug/kg ND 330 07/08/09 18:32
1-Methylnaphthalene ug/kg ND 330 07/08/09 18:32
2,4,5-Trichlorophenol ug/kg ND 330 07/08/09 18:32
2,4,6-Trichlorophenol ug/kg ND 330 07/08/09 18:32
2,4-Dichlorophenol ug/kg ND 330 07/08/09 18:32
2,4-Dimethylphenol ug/kg ND 330 07/08/09 18:32
2,4-Dinitrophenol ug/kg ND 1650 07/08/09 18:32
2,4-Dinitrotoluene ug/kg ND 330 07/08/09 18:32
2,6-Dinitrotoluene ug/kg ND 330 07/08/09 18:32
2-Chloronaphthalene ug/kg ND 330 07/08/09 18:32
2-Chlorophenol ug/kg ND 330 07/08/09 18:32
2-Methylnaphthalene ug/kg ND 330 07/08/09 18:32
2-Methylphenol(o-Cresol)ug/kg ND 330 07/08/09 18:32
2-Nitroaniline ug/kg ND 1650 07/08/09 18:32
2-Nitrophenol ug/kg ND 330 07/08/09 18:32
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 07/08/09 18:32
3,3'-Dichlorobenzidine ug/kg ND 1650 07/08/09 18:32
3-Nitroaniline ug/kg ND 1650 07/08/09 18:32
4,6-Dinitro-2-methylphenol ug/kg ND 660 07/08/09 18:32
4-Bromophenylphenyl ether ug/kg ND 330 07/08/09 18:32
4-Chloro-3-methylphenol ug/kg ND 660 07/08/09 18:32
4-Chloroaniline ug/kg ND 1650 07/08/09 18:32
4-Chlorophenylphenyl ether ug/kg ND 330 07/08/09 18:32
4-Nitroaniline ug/kg ND 660 07/08/09 18:32
4-Nitrophenol ug/kg ND 1650 07/08/09 18:32
Acenaphthene ug/kg ND 330 07/08/09 18:32
Acenaphthylene ug/kg ND 330 07/08/09 18:32
Aniline ug/kg ND 330 07/08/09 18:32
Anthracene ug/kg ND 330 07/08/09 18:32
Benzo(a)anthracene ug/kg ND 330 07/08/09 18:32
Benzo(a)pyrene ug/kg ND 330 07/08/09 18:32
Benzo(b)fluoranthene ug/kg ND 330 07/08/09 18:32
Benzo(g,h,i)perylene ug/kg ND 330 07/08/09 18:32
Benzo(k)fluoranthene ug/kg ND 330 07/08/09 18:32
Benzoic Acid ug/kg ND 1650 07/08/09 18:32
Benzyl alcohol ug/kg ND 660 07/08/09 18:32
bis(2-Chloroethoxy)methane ug/kg ND 330 07/08/09 18:32
bis(2-Chloroethyl) ether ug/kg ND 330 07/08/09 18:32
bis(2-Chloroisopropyl) ether ug/kg ND 330 07/08/09 18:32
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 141 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:302311
Associated Lab Samples:9247665013, 9247665014, 9247665015, 9247665016, 9247665017, 9247665018, 9247665019
Matrix:Solid
Analyzed
bis(2-Ethylhexyl)phthalate ug/kg ND 330 07/08/09 18:32
Butylbenzylphthalate ug/kg ND 330 07/08/09 18:32
Chrysene ug/kg ND 330 07/08/09 18:32
Di-n-butylphthalate ug/kg ND 330 07/08/09 18:32
Di-n-octylphthalate ug/kg ND 330 07/08/09 18:32
Dibenz(a,h)anthracene ug/kg ND 330 07/08/09 18:32
Dibenzofuran ug/kg ND 330 07/08/09 18:32
Diethylphthalate ug/kg ND 330 07/08/09 18:32
Dimethylphthalate ug/kg ND 330 07/08/09 18:32
Fluoranthene ug/kg ND 330 07/08/09 18:32
Fluorene ug/kg ND 330 07/08/09 18:32
Hexachloro-1,3-butadiene ug/kg ND 330 07/08/09 18:32
Hexachlorobenzene ug/kg ND 330 07/08/09 18:32
Hexachlorocyclopentadiene ug/kg ND 330 07/08/09 18:32
Hexachloroethane ug/kg ND 330 07/08/09 18:32
Indeno(1,2,3-cd)pyrene ug/kg ND 330 07/08/09 18:32
Isophorone ug/kg ND 330 07/08/09 18:32
N-Nitroso-di-n-propylamine ug/kg ND 330 07/08/09 18:32
N-Nitrosodimethylamine ug/kg ND 330 07/08/09 18:32
N-Nitrosodiphenylamine ug/kg ND 330 07/08/09 18:32
Naphthalene ug/kg ND 330 07/08/09 18:32
Nitrobenzene ug/kg ND 330 07/08/09 18:32
Pentachlorophenol ug/kg ND 1650 07/08/09 18:32
Phenanthrene ug/kg ND 330 07/08/09 18:32
Phenol ug/kg ND 330 07/08/09 18:32
Pyrene ug/kg ND 330 07/08/09 18:32
2,4,6-Tribromophenol (S)%67 44-136 07/08/09 18:32
2-Fluorobiphenyl (S)%62 46-120 07/08/09 18:32
2-Fluorophenol (S)%46 24-120 07/08/09 18:32
Nitrobenzene-d5 (S)%54 30-150 07/08/09 18:32
Phenol-d6 (S)%53 35-120 07/08/09 18:32
Terphenyl-d14 (S)%65 38-108 07/08/09 18:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
302312LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 13301670 80 50-150
1,2-Dichlorobenzene ug/kg 12301670 74 50-150
1,2-Diphenylhydrazine ug/kg 15401670 92 43-130
1,3-Dichlorobenzene ug/kg 11701670 70 50-150
1,4-Dichlorobenzene ug/kg 12501670 75 50-150
1-Methylnaphthalene ug/kg 17501670 105 50-150
2,4,5-Trichlorophenol ug/kg 15701670 94 50-150
2,4,6-Trichlorophenol ug/kg 15501670 93 50-150
2,4-Dichlorophenol ug/kg 13601670 82 50-150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 142 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
302312LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dimethylphenol ug/kg 12701670 76 50-150
2,4-Dinitrophenol ug/kg 1270J1670 76 20-111
2,4-Dinitrotoluene ug/kg 14601670 88 50-150
2,6-Dinitrotoluene ug/kg 14501670 87 50-150
2-Chloronaphthalene ug/kg 13501670 81 50-150
2-Chlorophenol ug/kg 11801670 71 50-150
2-Methylnaphthalene ug/kg 12901670 78 50-150
2-Methylphenol(o-Cresol)ug/kg 11701670 70 50-150
2-Nitroaniline ug/kg 1390J1670 84 50-150
2-Nitrophenol ug/kg 13601670 81 50-150
3&4-Methylphenol(m&p Cresol)ug/kg 12901670 77 50-150
3,3'-Dichlorobenzidine ug/kg 17201670 103 50-150
3-Nitroaniline ug/kg 1600J1670 96 50-150
4,6-Dinitro-2-methylphenol ug/kg 13401670 80 15-136
4-Bromophenylphenyl ether ug/kg 17601670 106 50-150
4-Chloro-3-methylphenol ug/kg 13901670 84 50-150
4-Chloroaniline ug/kg 1370J1670 82 50-150
4-Chlorophenylphenyl ether ug/kg 17701670 106 50-150
4-Nitroaniline ug/kg 14401670 87 50-150
4-Nitrophenol ug/kg 1560J1670 93 33-105
Acenaphthene ug/kg 14901670 89 50-150
Acenaphthylene ug/kg 15301670 92 50-150
Aniline ug/kg 10201670 61 50-150
Anthracene ug/kg 14001670 84 50-150
Benzo(a)anthracene ug/kg 14601670 87 50-150
Benzo(a)pyrene ug/kg 14401670 87 50-150
Benzo(b)fluoranthene ug/kg 15101670 91 50-150
Benzo(g,h,i)perylene ug/kg 17301670 104 24-117
Benzo(k)fluoranthene ug/kg 14101670 84 50-150
Benzoic Acid ug/kg 416J1670 25 15-104
Benzyl alcohol ug/kg 12301670 74 50-150
bis(2-Chloroethoxy)methane ug/kg 15501670 93 50-150
bis(2-Chloroethyl) ether ug/kg 13801670 83 50-150
bis(2-Chloroisopropyl) ether ug/kg 13601670 81 50-150
bis(2-Ethylhexyl)phthalate ug/kg 15301670 92 50-150
Butylbenzylphthalate ug/kg 14901670 90 50-150
Chrysene ug/kg 15101670 90 50-150
Di-n-butylphthalate ug/kg 15301670 92 50-150
Di-n-octylphthalate ug/kg 15101670 90 50-150
Dibenz(a,h)anthracene ug/kg 16301670 98 17-128
Dibenzofuran ug/kg 14701670 88 50-150
Diethylphthalate ug/kg 15101670 91 50-150
Dimethylphthalate ug/kg 15001670 90 50-150
Fluoranthene ug/kg 14901670 89 50-150
Fluorene ug/kg 15401670 92 50-150
Hexachloro-1,3-butadiene ug/kg 15501670 93 50-150
Hexachlorobenzene ug/kg 14101670 84 50-150
Hexachlorocyclopentadiene ug/kg 13701670 82 15-114
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 143 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
302312LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloroethane ug/kg 12001670 72 50-150
Indeno(1,2,3-cd)pyrene ug/kg 16801670 101 19-128
Isophorone ug/kg 14101670 85 50-150
N-Nitroso-di-n-propylamine ug/kg 11601670 69 50-150
N-Nitrosodimethylamine ug/kg 12001670 72 50-150
N-Nitrosodiphenylamine ug/kg 15901670 95 50-150
Naphthalene ug/kg 15001670 90 50-150
Nitrobenzene ug/kg 17101670 103 50-150
Pentachlorophenol ug/kg 1150J1670 69 15-130
Phenanthrene ug/kg 13901670 83 50-150
Phenol ug/kg 12201670 73 42-120
Pyrene ug/kg 14101670 85 50-150
2,4,6-Tribromophenol (S)%85 44-136
2-Fluorobiphenyl (S)%76 46-120
2-Fluorophenol (S)%69 24-120
Nitrobenzene-d5 (S)%79 30-150
Phenol-d6 (S)%79 35-120
Terphenyl-d14 (S)%77 38-108
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
302313MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9247658003
302314
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 2010 66 50-15070 62010ND13201410
1,4-Dichlorobenzene ug/kg 2010 65 50-15067 32010ND13101350
2,4-Dinitrotoluene ug/kg 2010 72 50-15076 62010ND14401540
2-Chlorophenol ug/kg 2010 62 50-15063 32010ND12401280
4-Chloro-3-methylphenol ug/kg 2010 77 50-15082 62010ND15401640
4-Nitrophenol ug/kg 2010 110 50-150116 52010ND22202330
Acenaphthene ug/kg 2010 81 50-15086 62010ND16201720
N-Nitroso-di-n-propylamine ug/kg 2010 88 50-15094 62010ND17801890
Pentachlorophenol ug/kg 2010 60 50-150602010ND1200J1210J
Phenol ug/kg 2010 65 50-15066 22010ND13001330
Pyrene ug/kg 2010 103 50-150112 82010ND20702240
2,4,6-Tribromophenol (S)%77 44-13682
2-Fluorobiphenyl (S)%73 46-12072
2-Fluorophenol (S)%60 24-12061
Nitrobenzene-d5 (S)%73 30-15079
Phenol-d6 (S)%70 35-12071
Terphenyl-d14 (S)%2g13138-108132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 144 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/7429
EPA 3546
EPA 8015 Modified
8015 Solid GCSV
Associated Lab Samples:9247665031
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:310400
Associated Lab Samples:9247665031
Matrix:Solid
Analyzed
Diesel Components mg/kg ND 5.0 07/21/09 12:08
n-Pentacosane (S)%70 50-135 07/21/09 12:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
310401LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Components mg/kg 108167 65 50-114
n-Pentacosane (S)%66 50-135
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
310402MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9248786010
310403
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Diesel Components mg/kg M0,R11824150-10770 4218227.0 101 155
n-Pentacosane (S)%83 50-13594
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 145 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/7543
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:9247665001, 9247665003, 9247665006, 9247665012, 9247665013, 9247665014, 9247665015, 9247665016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:303678
Associated Lab Samples:9247665001, 9247665003, 9247665006, 9247665012, 9247665013, 9247665014, 9247665015, 9247665016
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/06/09 10:53
1,1,1-Trichloroethane ug/kg ND 5.0 07/06/09 10:53
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/06/09 10:53
1,1,2-Trichloroethane ug/kg ND 5.0 07/06/09 10:53
1,1-Dichloroethane ug/kg ND 5.0 07/06/09 10:53
1,1-Dichloroethene ug/kg ND 5.0 07/06/09 10:53
1,1-Dichloropropene ug/kg ND 5.0 07/06/09 10:53
1,2,3-Trichlorobenzene ug/kg ND 5.0 07/06/09 10:53
1,2,3-Trichloropropane ug/kg ND 5.0 07/06/09 10:53
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/06/09 10:53
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/06/09 10:53
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 07/06/09 10:53
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/06/09 10:53
1,2-Dichlorobenzene ug/kg ND 5.0 07/06/09 10:53
1,2-Dichloroethane ug/kg ND 5.0 07/06/09 10:53
1,2-Dichloropropane ug/kg ND 5.0 07/06/09 10:53
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/06/09 10:53
1,3-Dichlorobenzene ug/kg ND 5.0 07/06/09 10:53
1,3-Dichloropropane ug/kg ND 5.0 07/06/09 10:53
1,4-Dichlorobenzene ug/kg ND 5.0 07/06/09 10:53
2,2-Dichloropropane ug/kg ND 5.0 07/06/09 10:53
2-Butanone (MEK)ug/kg ND 100 07/06/09 10:53
2-Chlorotoluene ug/kg ND 5.0 07/06/09 10:53
2-Hexanone ug/kg ND 50.0 07/06/09 10:53
4-Chlorotoluene ug/kg ND 5.0 07/06/09 10:53
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/06/09 10:53
Acetone ug/kg ND 100 07/06/09 10:53
Benzene ug/kg ND 5.0 07/06/09 10:53
Bromobenzene ug/kg ND 5.0 07/06/09 10:53
Bromochloromethane ug/kg ND 5.0 07/06/09 10:53
Bromodichloromethane ug/kg ND 5.0 07/06/09 10:53
Bromoform ug/kg ND 5.0 07/06/09 10:53
Bromomethane ug/kg ND 10.0 07/06/09 10:53
Carbon tetrachloride ug/kg ND 5.0 07/06/09 10:53
Chlorobenzene ug/kg ND 5.0 07/06/09 10:53
Chloroethane ug/kg ND 10.0 07/06/09 10:53
Chloroform ug/kg ND 5.0 07/06/09 10:53
Chloromethane ug/kg ND 10.0 07/06/09 10:53
cis-1,2-Dichloroethene ug/kg ND 5.0 07/06/09 10:53
cis-1,3-Dichloropropene ug/kg ND 5.0 07/06/09 10:53
Dibromochloromethane ug/kg ND 5.0 07/06/09 10:53
Dibromomethane ug/kg ND 5.0 07/06/09 10:53
Dichlorodifluoromethane ug/kg ND 10.0 07/06/09 10:53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 146 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:303678
Associated Lab Samples:9247665001, 9247665003, 9247665006, 9247665012, 9247665013, 9247665014, 9247665015, 9247665016
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.0 07/06/09 10:53
Ethylbenzene ug/kg ND 5.0 07/06/09 10:53
Hexachloro-1,3-butadiene ug/kg ND 5.0 07/06/09 10:53
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/06/09 10:53
m&p-Xylene ug/kg ND 10.0 07/06/09 10:53
Methyl-tert-butyl ether ug/kg ND 5.0 07/06/09 10:53
Methylene Chloride ug/kg ND 20.0 07/06/09 10:53
n-Butylbenzene ug/kg ND 5.0 07/06/09 10:53
n-Propylbenzene ug/kg ND 5.0 07/06/09 10:53
Naphthalene ug/kg ND 5.0 07/06/09 10:53
o-Xylene ug/kg ND 5.0 07/06/09 10:53
p-Isopropyltoluene ug/kg ND 5.0 07/06/09 10:53
sec-Butylbenzene ug/kg ND 5.0 07/06/09 10:53
Styrene ug/kg ND 5.0 07/06/09 10:53
tert-Butylbenzene ug/kg ND 5.0 07/06/09 10:53
Tetrachloroethene ug/kg ND 5.0 07/06/09 10:53
Toluene ug/kg ND 5.0 07/06/09 10:53
trans-1,2-Dichloroethene ug/kg ND 5.0 07/06/09 10:53
trans-1,3-Dichloropropene ug/kg ND 5.0 07/06/09 10:53
Trichloroethene ug/kg ND 5.0 07/06/09 10:53
Trichlorofluoromethane ug/kg ND 5.0 07/06/09 10:53
Vinyl acetate ug/kg ND 50.0 07/06/09 10:53
Vinyl chloride ug/kg ND 10.0 07/06/09 10:53
Xylene (Total)ug/kg ND 10.0 07/06/09 10:53
1,2-Dichloroethane-d4 (S)%94 69-121 07/06/09 10:53
4-Bromofluorobenzene (S)%102 74-115 07/06/09 10:53
Dibromofluoromethane (S)%98 79-116 07/06/09 10:53
Toluene-d8 (S)%100 88-110 07/06/09 10:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
303679LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 54.050 108 75-137
1,1,1-Trichloroethane ug/kg 58.250 116 70-140
1,1,2,2-Tetrachloroethane ug/kg 54.050 108 74-133
1,1,2-Trichloroethane ug/kg 55.750 111 79-129
1,1-Dichloroethane ug/kg 64.650 129 72-139
1,1-Dichloroethene ug/kg 52.250 104 69-154
1,1-Dichloropropene ug/kg 52.750 105 74-138
1,2,3-Trichlorobenzene ug/kg 49.550 99 71-150
1,2,3-Trichloropropane ug/kg 52.650 105 74-135
1,2,4-Trichlorobenzene ug/kg 52.150 104 68-150
1,2,4-Trimethylbenzene ug/kg 52.850 106 70-130
1,2-Dibromo-3-chloropropane ug/kg 45.450 91 65-146
1,2-Dibromoethane (EDB)ug/kg 56.050 112 77-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 147 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
303679LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 51.850 104 75-141
1,2-Dichloroethane ug/kg 49.450 99 74-134
1,2-Dichloropropane ug/kg 51.950 104 77-138
1,3,5-Trimethylbenzene ug/kg 51.250 102 65-128
1,3-Dichlorobenzene ug/kg 55.450 111 76-133
1,3-Dichloropropane ug/kg 53.350 107 79-132
1,4-Dichlorobenzene ug/kg 49.750 99 75-137
2,2-Dichloropropane ug/kg 61.050 122 73-137
2-Butanone (MEK)ug/kg 95.9J100 96 61-138
2-Chlorotoluene ug/kg 54.350 109 73-138
2-Hexanone ug/kg 101100 101 58-159
4-Chlorotoluene ug/kg 56.650 113 75-136
4-Methyl-2-pentanone (MIBK)ug/kg 98.7100 99 74-139
Acetone ug/kg 106100 106 58-150
Benzene ug/kg 54.550 109 71-140
Bromobenzene ug/kg 50.550 101 72-144
Bromochloromethane ug/kg 64.150 128 78-133
Bromodichloromethane ug/kg 50.650 101 78-133
Bromoform ug/kg 55.950 112 74-132
Bromomethane ug/kg 32.850 66 63-184
Carbon tetrachloride ug/kg 57.650 115 73-143
Chlorobenzene ug/kg 57.850 116 77-137
Chloroethane ug/kg 44.150 88 68-146
Chloroform ug/kg 54.950 110 75-137
Chloromethane ug/kg 43.850 88 54-143
cis-1,2-Dichloroethene ug/kg 51.250 102 71-143
cis-1,3-Dichloropropene ug/kg 53.150 106 76-133
Dibromochloromethane ug/kg 53.350 107 77-131
Dibromomethane ug/kg 60.550 121 63-184
Dichlorodifluoromethane ug/kg 34.450 69 36-173
Diisopropyl ether ug/kg 49.950 100 68-144
Ethylbenzene ug/kg 55.350 111 69-141
Hexachloro-1,3-butadiene ug/kg 48.150 96 70-152
Isopropylbenzene (Cumene)ug/kg 54.750 109 77-143
m&p-Xylene ug/kg 107100 107 72-138
Methyl-tert-butyl ether ug/kg 53.150 106 2-138
Methylene Chloride ug/kg 58.650 117 69-136
n-Butylbenzene ug/kg 50.850 102 65-128
n-Propylbenzene ug/kg 52.850 106 72-139
Naphthalene ug/kg 51.150 102 61-138
o-Xylene ug/kg 53.250 106 74-137
p-Isopropyltoluene ug/kg 52.350 105 66-128
sec-Butylbenzene ug/kg 51.250 102 72-140
Styrene ug/kg 56.450 113 76-137
tert-Butylbenzene ug/kg 53.050 106 68-141
Tetrachloroethene ug/kg 57.950 116 72-136
Toluene ug/kg 52.850 106 69-139
trans-1,2-Dichloroethene ug/kg 48.750 97 72-144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 148 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
303679LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 50.850 102 73-135
Trichloroethene ug/kg 56.050 112 75-136
Trichlorofluoromethane ug/kg 45.750 91 69-144
Vinyl acetate ug/kg 99.3100 99 50-150
Vinyl chloride ug/kg 45.850 92 61-145
Xylene (Total)ug/kg 161150 107 73-138
1,2-Dichloroethane-d4 (S)%90 69-121
4-Bromofluorobenzene (S)%106 74-115
Dibromofluoromethane (S)%98 79-116
Toluene-d8 (S)%99 88-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
304190MATRIX SPIKE SAMPLE:
MSSpike
Result
9247665012
1,1-Dichloroethene ug/kg 54.251.8 105 33-158ND
Benzene ug/kg 49.051.8 95 46-143ND
Chlorobenzene ug/kg 39.451.8 76 29-159ND
Toluene ug/kg 42.251.8 82 38-145ND
Trichloroethene ug/kg 46.051.8 89 70-130ND
1,2-Dichloroethane-d4 (S)%95 69-121
4-Bromofluorobenzene (S)%99 74-115
Dibromofluoromethane (S)%97 79-116
Toluene-d8 (S)%98 88-110
Parameter Units
Dup
Result QualifiersRPDResult
9247799011
304191SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg 65.3ND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg 22.9ND
1,3-Dichlorobenzene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 149 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
Dup
Result QualifiersRPDResult
9247799011
304191SAMPLE DUPLICATE:
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg 12.1JND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg 1.8JND
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg 3JND
Naphthalene ug/kg 11.2ND
o-Xylene ug/kg 4.4ND
p-Isopropyltoluene ug/kg 36.1ND
sec-Butylbenzene ug/kg 3JND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 150 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
Dup
Result QualifiersRPDResult
9247799011
304191SAMPLE DUPLICATE:
Xylene (Total)ug/kg 5.4J
1,2-Dichloroethane-d4 (S)%94 9104
4-Bromofluorobenzene (S)%99 6107
Dibromofluoromethane (S)%100 5g3105
Toluene-d8 (S)%101 697
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 151 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/7588
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:9247665022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:304558
Associated Lab Samples:9247665022
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 07/07/09 22:39
1,1,1-Trichloroethane ug/L ND 1.0 07/07/09 22:39
1,1,2,2-Tetrachloroethane ug/L ND 1.0 07/07/09 22:39
1,1,2-Trichloroethane ug/L ND 1.0 07/07/09 22:39
1,1-Dichloroethane ug/L ND 1.0 07/07/09 22:39
1,1-Dichloroethene ug/L ND 1.0 07/07/09 22:39
1,1-Dichloropropene ug/L ND 1.0 07/07/09 22:39
1,2,3-Trichlorobenzene ug/L ND 1.0 07/07/09 22:39
1,2,3-Trichloropropane ug/L ND 1.0 07/07/09 22:39
1,2,4-Trichlorobenzene ug/L ND 1.0 07/07/09 22:39
1,2-Dibromo-3-chloropropane ug/L ND 3.0 07/07/09 22:39
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/07/09 22:39
1,2-Dichlorobenzene ug/L ND 1.0 07/07/09 22:39
1,2-Dichloroethane ug/L ND 1.0 07/07/09 22:39
1,2-Dichloropropane ug/L ND 1.0 07/07/09 22:39
1,3-Dichlorobenzene ug/L ND 1.0 07/07/09 22:39
1,3-Dichloropropane ug/L ND 1.0 07/07/09 22:39
1,4-Dichlorobenzene ug/L ND 1.0 07/07/09 22:39
2,2-Dichloropropane ug/L ND 1.0 07/07/09 22:39
2-Butanone (MEK)ug/L ND 5.0 07/07/09 22:39
2-Chlorotoluene ug/L ND 1.0 07/07/09 22:39
2-Hexanone ug/L ND 5.0 07/07/09 22:39
4-Chlorotoluene ug/L ND 1.0 07/07/09 22:39
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 07/07/09 22:39
Acetone ug/L ND 25.0 07/07/09 22:39
Benzene ug/L ND 1.0 07/07/09 22:39
Bromobenzene ug/L ND 1.0 07/07/09 22:39
Bromochloromethane ug/L ND 1.0 07/07/09 22:39
Bromodichloromethane ug/L ND 1.0 07/07/09 22:39
Bromoform ug/L ND 1.0 07/07/09 22:39
Bromomethane ug/L ND 5.0 07/07/09 22:39
Carbon tetrachloride ug/L ND 1.0 07/07/09 22:39
Chlorobenzene ug/L ND 1.0 07/07/09 22:39
Chloroethane ug/L ND 1.0 07/07/09 22:39
Chloroform ug/L ND 1.0 07/07/09 22:39
Chloromethane ug/L ND 1.0 07/07/09 22:39
cis-1,2-Dichloroethene ug/L ND 1.0 07/07/09 22:39
cis-1,3-Dichloropropene ug/L ND 1.0 07/07/09 22:39
Dibromochloromethane ug/L ND 1.0 07/07/09 22:39
Dibromomethane ug/L ND 1.0 07/07/09 22:39
Dichlorodifluoromethane ug/L ND 1.0 07/07/09 22:39
Diisopropyl ether ug/L ND 1.0 07/07/09 22:39
Ethylbenzene ug/L ND 1.0 07/07/09 22:39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 152 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:304558
Associated Lab Samples:9247665022
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 1.0 07/07/09 22:39
m&p-Xylene ug/L ND 2.0 07/07/09 22:39
Methyl-tert-butyl ether ug/L ND 1.0 07/07/09 22:39
Methylene Chloride ug/L 4.2 2.0 B07/07/09 22:39
Naphthalene ug/L ND 1.0 07/07/09 22:39
o-Xylene ug/L ND 1.0 07/07/09 22:39
p-Isopropyltoluene ug/L ND 1.0 07/07/09 22:39
Styrene ug/L ND 1.0 07/07/09 22:39
Tetrachloroethene ug/L ND 1.0 07/07/09 22:39
Toluene ug/L ND 1.0 07/07/09 22:39
trans-1,2-Dichloroethene ug/L ND 1.0 07/07/09 22:39
trans-1,3-Dichloropropene ug/L ND 1.0 07/07/09 22:39
Trichloroethene ug/L ND 1.0 07/07/09 22:39
Trichlorofluoromethane ug/L ND 1.0 07/07/09 22:39
Vinyl acetate ug/L ND 2.0 07/07/09 22:39
Vinyl chloride ug/L ND 1.0 07/07/09 22:39
1,2-Dichloroethane-d4 (S)%108 79-120 07/07/09 22:39
4-Bromofluorobenzene (S)%98 87-109 07/07/09 22:39
Dibromofluoromethane (S)%108 85-115 07/07/09 22:39
Toluene-d8 (S)%101 70-120 07/07/09 22:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
304559LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.950 104 83-125
1,1,1-Trichloroethane ug/L 63.050 126 80-129
1,1,2,2-Tetrachloroethane ug/L 48.450 97 73-127
1,1,2-Trichloroethane ug/L 54.250 108 77-123
1,1-Dichloroethane ug/L 71.1 L05014276-129
1,1-Dichloroethene ug/L 59.150 118 78-146
1,1-Dichloropropene ug/L 56.450 113 79-134
1,2,3-Trichlorobenzene ug/L 52.150 104 70-150
1,2,3-Trichloropropane ug/L 50.650 101 72-125
1,2,4-Trichlorobenzene ug/L 52.650 105 68-127
1,2-Dibromo-3-chloropropane ug/L 52.050 104 65-128
1,2-Dibromoethane (EDB)ug/L 52.350 105 81-125
1,2-Dichlorobenzene ug/L 54.650 109 82-126
1,2-Dichloroethane ug/L 54.650 109 72-126
1,2-Dichloropropane ug/L 56.050 112 80-127
1,3-Dichlorobenzene ug/L 54.550 109 82-124
1,3-Dichloropropane ug/L 53.050 106 79-124
1,4-Dichlorobenzene ug/L 53.750 107 79-125
2,2-Dichloropropane ug/L 60.050 120 58-140
2-Butanone (MEK)ug/L 104100 104 50-134
2-Chlorotoluene ug/L 54.650 109 81-126
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 153 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
304559LABORATORY CONTROL SAMPLE:
LCSSpike
2-Hexanone ug/L 103100 103 58-138
4-Chlorotoluene ug/L 57.050 114 82-126
4-Methyl-2-pentanone (MIBK)ug/L 94.0100 94 70-131
Acetone ug/L 98.0100 98 50-146
Benzene ug/L 56.450 113 78-128
Bromobenzene ug/L 53.750 107 81-127
Bromochloromethane ug/L 55.750 111 73-124
Bromodichloromethane ug/L 52.450 105 81-125
Bromoform ug/L 48.950 98 71-125
Bromomethane ug/L 84.3 L35016950-150
Carbon tetrachloride ug/L 60.450 121 81-137
Chlorobenzene ug/L 54.150 108 82-126
Chloroethane ug/L 50.250 100 69-140
Chloroform ug/L 58.950 118 77-129
Chloromethane ug/L 46.950 94 54-139
cis-1,2-Dichloroethene ug/L 55.850 112 76-133
cis-1,3-Dichloropropene ug/L 48.150 96 76-127
Dibromochloromethane ug/L 50.550 101 77-125
Dibromomethane ug/L 56.950 114 77-125
Dichlorodifluoromethane ug/L 45.150 90 50-150
Diisopropyl ether ug/L 54.350 109 74-131
Ethylbenzene ug/L 53.650 107 80-127
Hexachloro-1,3-butadiene ug/L 52.550 105 78-145
m&p-Xylene ug/L 107100 107 82-127
Methyl-tert-butyl ether ug/L 53.850 108 71-130
Methylene Chloride ug/L 65.350 131 67-133
Naphthalene ug/L 47.350 95 52-136
o-Xylene ug/L 53.550 107 83-124
p-Isopropyltoluene ug/L 54.450 109 73-122
Styrene ug/L 48.450 97 80-130
Tetrachloroethene ug/L 54.750 109 78-128
Toluene ug/L 52.850 106 76-126
trans-1,2-Dichloroethene ug/L 53.950 108 78-134
trans-1,3-Dichloropropene ug/L 47.250 94 75-125
Trichloroethene ug/L 55.150 110 79-127
Trichlorofluoromethane ug/L 52.150 104 76-148
Vinyl acetate ug/L 57.3100 57 50-150
Vinyl chloride ug/L 56.050 112 67-143
1,2-Dichloroethane-d4 (S)%98 79-120
4-Bromofluorobenzene (S)%100 87-109
Dibromofluoromethane (S)%104 85-115
Toluene-d8 (S)%102 70-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 154 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
304560MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9247968005
304561
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 50 145 60-150141 350ND72.5 70.4
Benzene ug/L 50 132 74-136130 250ND66.0 64.8
Chlorobenzene ug/L 50 127 79-135125 250ND63.5 62.3
Toluene ug/L M05013773-131128 750ND68.9 64.1
Trichloroethene ug/L 50 120 73-131119 .950ND60.1 59.5
1,2-Dichloroethane-d4 (S)%100 79-12099
4-Bromofluorobenzene (S)%97 87-10997
Dibromofluoromethane (S)%103 85-115103
Toluene-d8 (S)%100 70-12099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 155 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/3350
EPA 5030/8015 Mod.
EPA 5030/8015 Mod.
Gasoline Range Organics
Associated Lab Samples:9247665022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:307710
Associated Lab Samples:9247665022
Matrix:Water
Analyzed
Gasoline Range Organics mg/L ND 0.080 07/14/09 17:08
4-Bromofluorobenzene (S)%85 50-150 07/14/09 17:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
307711LABORATORY CONTROL SAMPLE:
LCSSpike
Gasoline Range Organics mg/L 0.54.5 107 70-137
4-Bromofluorobenzene (S)%87 50-150
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
307712MATRIX SPIKE SAMPLE:
MSSpike
Result
9247844003
Gasoline Range Organics mg/L 0.52.5 103 53-150ND
4-Bromofluorobenzene (S)%150 50-150
Parameter Units
Dup
Result QualifiersRPDResult
9247844002
307713SAMPLE DUPLICATE:
Gasoline Range Organics mg/L NDND
4-Bromofluorobenzene (S)%86 384
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 156 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/2565
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:9247665001, 9247665002, 9247665003
Parameter Units
Dup
Result QualifiersRPDResult
9247756007
303515SAMPLE DUPLICATE:
Percent Moisture %15.0 .115.0
Parameter Units
Dup
Result QualifiersRPDResult
9247766009
303516SAMPLE DUPLICATE:
Percent Moisture %27.3 328.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 157 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/7303
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:9247665022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:303896
Associated Lab Samples:9247665022
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 07/07/09 18:47
1,2-Dichlorobenzene ug/L ND 10.0 07/07/09 18:47
1,2-Diphenylhydrazine ug/L ND 10.0 07/07/09 18:47
1,3-Dichlorobenzene ug/L ND 10.0 07/07/09 18:47
1,4-Dichlorobenzene ug/L ND 10.0 07/07/09 18:47
1-Methylnaphthalene ug/L ND 10.0 07/07/09 18:47
2,4,5-Trichlorophenol ug/L ND 10.0 07/07/09 18:47
2,4,6-Trichlorophenol ug/L ND 10.0 07/07/09 18:47
2,4-Dichlorophenol ug/L ND 10.0 07/07/09 18:47
2,4-Dimethylphenol ug/L ND 10.0 07/07/09 18:47
2,4-Dinitrophenol ug/L ND 50.0 07/07/09 18:47
2,4-Dinitrotoluene ug/L ND 10.0 07/07/09 18:47
2,6-Dinitrotoluene ug/L ND 10.0 07/07/09 18:47
2-Chloronaphthalene ug/L ND 10.0 07/07/09 18:47
2-Chlorophenol ug/L ND 10.0 07/07/09 18:47
2-Methylnaphthalene ug/L ND 10.0 07/07/09 18:47
2-Methylphenol(o-Cresol)ug/L ND 10.0 07/07/09 18:47
2-Nitroaniline ug/L ND 50.0 07/07/09 18:47
2-Nitrophenol ug/L ND 10.0 07/07/09 18:47
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 07/07/09 18:47
3,3'-Dichlorobenzidine ug/L ND 50.0 07/07/09 18:47
3-Nitroaniline ug/L ND 50.0 07/07/09 18:47
4,6-Dinitro-2-methylphenol ug/L ND 20.0 07/07/09 18:47
4-Bromophenylphenyl ether ug/L ND 10.0 07/07/09 18:47
4-Chloro-3-methylphenol ug/L ND 20.0 07/07/09 18:47
4-Chloroaniline ug/L ND 50.0 07/07/09 18:47
4-Chlorophenylphenyl ether ug/L ND 10.0 07/07/09 18:47
4-Nitroaniline ug/L ND 50.0 07/07/09 18:47
4-Nitrophenol ug/L ND 50.0 07/07/09 18:47
Acenaphthene ug/L ND 10.0 07/07/09 18:47
Acenaphthylene ug/L ND 10.0 07/07/09 18:47
Aniline ug/L ND 10.0 07/07/09 18:47
Anthracene ug/L ND 10.0 07/07/09 18:47
Benzo(a)anthracene ug/L ND 10.0 07/07/09 18:47
Benzo(a)pyrene ug/L ND 10.0 07/07/09 18:47
Benzo(b)fluoranthene ug/L ND 10.0 07/07/09 18:47
Benzo(g,h,i)perylene ug/L ND 10.0 07/07/09 18:47
Benzo(k)fluoranthene ug/L ND 10.0 07/07/09 18:47
Benzoic Acid ug/L ND 50.0 07/07/09 18:47
Benzyl alcohol ug/L ND 20.0 07/07/09 18:47
bis(2-Chloroethoxy)methane ug/L ND 10.0 07/07/09 18:47
bis(2-Chloroethyl) ether ug/L ND 10.0 07/07/09 18:47
bis(2-Chloroisopropyl) ether ug/L ND 10.0 07/07/09 18:47
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 158 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:303896
Associated Lab Samples:9247665022
Matrix:Water
Analyzed
bis(2-Ethylhexyl)phthalate ug/L ND 10.0 07/07/09 18:47
Butylbenzylphthalate ug/L ND 10.0 07/07/09 18:47
Chrysene ug/L ND 10.0 07/07/09 18:47
Di-n-butylphthalate ug/L ND 10.0 07/07/09 18:47
Di-n-octylphthalate ug/L ND 10.0 07/07/09 18:47
Dibenz(a,h)anthracene ug/L ND 10.0 07/07/09 18:47
Dibenzofuran ug/L ND 10.0 07/07/09 18:47
Diethylphthalate ug/L ND 10.0 07/07/09 18:47
Dimethylphthalate ug/L ND 10.0 07/07/09 18:47
Fluoranthene ug/L ND 10.0 07/07/09 18:47
Fluorene ug/L ND 10.0 07/07/09 18:47
Hexachloro-1,3-butadiene ug/L ND 10.0 07/07/09 18:47
Hexachlorobenzene ug/L ND 10.0 07/07/09 18:47
Hexachlorocyclopentadiene ug/L ND 10.0 07/07/09 18:47
Hexachloroethane ug/L ND 10.0 07/07/09 18:47
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 07/07/09 18:47
Isophorone ug/L ND 10.0 07/07/09 18:47
N-Nitroso-di-n-propylamine ug/L ND 10.0 07/07/09 18:47
N-Nitrosodimethylamine ug/L ND 10.0 07/07/09 18:47
N-Nitrosodiphenylamine ug/L ND 10.0 07/07/09 18:47
Naphthalene ug/L ND 10.0 07/07/09 18:47
Nitrobenzene ug/L ND 10.0 07/07/09 18:47
Pentachlorophenol ug/L ND 50.0 07/07/09 18:47
Phenanthrene ug/L ND 10.0 07/07/09 18:47
Phenol ug/L ND 10.0 07/07/09 18:47
Pyrene ug/L ND 10.0 07/07/09 18:47
2,4,6-Tribromophenol (S)%69 25-150 07/07/09 18:47
2-Fluorobiphenyl (S)%66 30-150 07/07/09 18:47
2-Fluorophenol (S)%36 25-150 07/07/09 18:47
Nitrobenzene-d5 (S)%64 30-150 07/07/09 18:47
Phenol-d6 (S)%28 25-150 07/07/09 18:47
Terphenyl-d14 (S)%75 30-150 07/07/09 18:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
303897LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 29.350 59 19-120
1,2-Dichlorobenzene ug/L 26.550 53 19-120
1,2-Diphenylhydrazine ug/L 40.050 80 50-150
1,3-Dichlorobenzene ug/L 24.650 49 15-120
1,4-Dichlorobenzene ug/L 26.850 54 15-120
1-Methylnaphthalene ug/L 44.450 89 21-120
2,4,5-Trichlorophenol ug/L 35.650 71 23-113
2,4,6-Trichlorophenol ug/L 36.650 73 21-113
2,4-Dichlorophenol ug/L 33.450 67 12-127
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 159 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
303897LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dimethylphenol ug/L 31.750 63 24-120
2,4-Dinitrophenol ug/L ND L050510-127
2,4-Dinitrotoluene ug/L 36.950 74 36-115
2,6-Dinitrotoluene ug/L 39.750 79 37-114
2-Chloronaphthalene ug/L 33.950 68 36-101
2-Chlorophenol ug/L 27.350 55 24-120
2-Methylnaphthalene ug/L 29.950 60 19-120
2-Methylphenol(o-Cresol)ug/L 24.850 50 25-120
2-Nitroaniline ug/L 38.3J50 77 30-109
2-Nitrophenol ug/L 33.250 66 24-120
3&4-Methylphenol(m&p Cresol)ug/L 25.350 51 24-120
3,3'-Dichlorobenzidine ug/L 45.9J50 92 14-120
3-Nitroaniline ug/L 43.7J50 87 23-133
4,6-Dinitro-2-methylphenol ug/L 18.8J50 38 10-128
4-Bromophenylphenyl ether ug/L 46.150 92 35-113
4-Chloro-3-methylphenol ug/L 35.350 71 32-107
4-Chloroaniline ug/L 44.5J50 89 12-150
4-Chlorophenylphenyl ether ug/L 45.650 91 36-110
4-Nitroaniline ug/L 38.2J50 76 12-150
4-Nitrophenol ug/L 20.9J50 42 10-120
Acenaphthene ug/L 39.250 78 27-102
Acenaphthylene ug/L 38.350 77 25-105
Aniline ug/L 21.850 44 10-150
Anthracene ug/L 40.850 82 30-113
Benzo(a)anthracene ug/L 38.350 77 27-113
Benzo(a)pyrene ug/L 38.550 77 27-119
Benzo(b)fluoranthene ug/L 34.850 70 22-114
Benzo(g,h,i)perylene ug/L 50.450 101 10-129
Benzo(k)fluoranthene ug/L 32.250 64 24-111
Benzoic Acid ug/L ND L050324-120
Benzyl alcohol ug/L 27.650 55 24-120
bis(2-Chloroethoxy)methane ug/L 40.450 81 32-120
bis(2-Chloroethyl) ether ug/L 33.850 68 29-120
bis(2-Chloroisopropyl) ether ug/L 33.650 67 22-120
bis(2-Ethylhexyl)phthalate ug/L 39.850 80 29-125
Butylbenzylphthalate ug/L 39.950 80 33-120
Chrysene ug/L 39.650 79 23-112
Di-n-butylphthalate ug/L 39.850 80 38-116
Di-n-octylphthalate ug/L 40.350 81 32-122
Dibenz(a,h)anthracene ug/L 44.550 89 10-129
Dibenzofuran ug/L 38.050 76 37-107
Diethylphthalate ug/L 37.650 75 40-111
Dimethylphthalate ug/L 38.050 76 39-108
Fluoranthene ug/L 39.350 79 27-112
Fluorene ug/L 38.550 77 29-107
Hexachloro-1,3-butadiene ug/L 32.850 66 10-113
Hexachlorobenzene ug/L 40.250 80 29-119
Hexachlorocyclopentadiene ug/L 34.050 68 10-113
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 160 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
303897LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloroethane ug/L 25.550 51 10-120
Indeno(1,2,3-cd)pyrene ug/L 46.950 94 14-123
Isophorone ug/L 35.550 71 23-150
N-Nitroso-di-n-propylamine ug/L 39.350 79 31-104
N-Nitrosodimethylamine ug/L 19.950 40 10-120
N-Nitrosodiphenylamine ug/L 42.450 85 27-139
Naphthalene ug/L 33.750 67 17-120
Nitrobenzene ug/L 31.250 62 27-120
Pentachlorophenol ug/L 21.1J50 42 10-135
Phenanthrene ug/L 35.350 71 28-111
Phenol ug/L 12.950 26 10-120
Pyrene ug/L 37.950 76 27-113
2,4,6-Tribromophenol (S)%75 25-150
2-Fluorobiphenyl (S)%65 30-150
2-Fluorophenol (S)%32 25-150
Nitrobenzene-d5 (S)%62 30-150
Phenol-d6 (S)%27 25-150
Terphenyl-d14 (S)%72 30-150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 161 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/7582
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:9247665026, 9247665027, 9247665028
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:304372
Associated Lab Samples:9247665026, 9247665027, 9247665028
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/08/09 01:41
1,1,1-Trichloroethane ug/kg ND 5.0 07/08/09 01:41
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/08/09 01:41
1,1,2-Trichloroethane ug/kg ND 5.0 07/08/09 01:41
1,1-Dichloroethane ug/kg ND 5.0 07/08/09 01:41
1,1-Dichloroethene ug/kg ND 5.0 07/08/09 01:41
1,1-Dichloropropene ug/kg ND 5.0 07/08/09 01:41
1,2,3-Trichlorobenzene ug/kg ND 5.0 07/08/09 01:41
1,2,3-Trichloropropane ug/kg ND 5.0 07/08/09 01:41
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/08/09 01:41
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/08/09 01:41
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 07/08/09 01:41
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/08/09 01:41
1,2-Dichlorobenzene ug/kg ND 5.0 07/08/09 01:41
1,2-Dichloroethane ug/kg ND 5.0 07/08/09 01:41
1,2-Dichloropropane ug/kg ND 5.0 07/08/09 01:41
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/08/09 01:41
1,3-Dichlorobenzene ug/kg ND 5.0 07/08/09 01:41
1,3-Dichloropropane ug/kg ND 5.0 07/08/09 01:41
1,4-Dichlorobenzene ug/kg ND 5.0 07/08/09 01:41
2,2-Dichloropropane ug/kg ND 5.0 07/08/09 01:41
2-Butanone (MEK)ug/kg ND 100 07/08/09 01:41
2-Chlorotoluene ug/kg ND 5.0 07/08/09 01:41
2-Hexanone ug/kg ND 50.0 07/08/09 01:41
4-Chlorotoluene ug/kg ND 5.0 07/08/09 01:41
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/08/09 01:41
Acetone ug/kg ND 100 07/08/09 01:41
Benzene ug/kg ND 5.0 07/08/09 01:41
Bromobenzene ug/kg ND 5.0 07/08/09 01:41
Bromochloromethane ug/kg ND 5.0 07/08/09 01:41
Bromodichloromethane ug/kg ND 5.0 07/08/09 01:41
Bromoform ug/kg ND 5.0 07/08/09 01:41
Bromomethane ug/kg ND 10.0 07/08/09 01:41
Carbon tetrachloride ug/kg ND 5.0 07/08/09 01:41
Chlorobenzene ug/kg ND 5.0 07/08/09 01:41
Chloroethane ug/kg ND 10.0 07/08/09 01:41
Chloroform ug/kg ND 5.0 07/08/09 01:41
Chloromethane ug/kg ND 10.0 07/08/09 01:41
cis-1,2-Dichloroethene ug/kg ND 5.0 07/08/09 01:41
cis-1,3-Dichloropropene ug/kg ND 5.0 07/08/09 01:41
Dibromochloromethane ug/kg ND 5.0 07/08/09 01:41
Dibromomethane ug/kg ND 5.0 07/08/09 01:41
Dichlorodifluoromethane ug/kg ND 10.0 07/08/09 01:41
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 162 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:304372
Associated Lab Samples:9247665026, 9247665027, 9247665028
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.0 07/08/09 01:41
Ethylbenzene ug/kg ND 5.0 07/08/09 01:41
Hexachloro-1,3-butadiene ug/kg ND 5.0 07/08/09 01:41
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/08/09 01:41
m&p-Xylene ug/kg ND 10.0 07/08/09 01:41
Methyl-tert-butyl ether ug/kg ND 5.0 07/08/09 01:41
Methylene Chloride ug/kg ND 20.0 07/08/09 01:41
n-Butylbenzene ug/kg ND 5.0 07/08/09 01:41
n-Propylbenzene ug/kg ND 5.0 07/08/09 01:41
Naphthalene ug/kg ND 5.0 07/08/09 01:41
o-Xylene ug/kg ND 5.0 07/08/09 01:41
p-Isopropyltoluene ug/kg ND 5.0 07/08/09 01:41
sec-Butylbenzene ug/kg ND 5.0 07/08/09 01:41
Styrene ug/kg ND 5.0 07/08/09 01:41
tert-Butylbenzene ug/kg ND 5.0 07/08/09 01:41
Tetrachloroethene ug/kg ND 5.0 07/08/09 01:41
Toluene ug/kg ND 5.0 07/08/09 01:41
trans-1,2-Dichloroethene ug/kg ND 5.0 07/08/09 01:41
trans-1,3-Dichloropropene ug/kg ND 5.0 07/08/09 01:41
Trichloroethene ug/kg ND 5.0 07/08/09 01:41
Trichlorofluoromethane ug/kg ND 5.0 07/08/09 01:41
Vinyl acetate ug/kg ND 50.0 07/08/09 01:41
Vinyl chloride ug/kg ND 10.0 07/08/09 01:41
Xylene (Total)ug/kg ND 10.0 07/08/09 01:41
1,2-Dichloroethane-d4 (S)%97 69-121 07/08/09 01:41
4-Bromofluorobenzene (S)%100 74-115 07/08/09 01:41
Dibromofluoromethane (S)%99 79-116 07/08/09 01:41
Toluene-d8 (S)%100 88-110 07/08/09 01:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
304373LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 52.350 105 75-137
1,1,1-Trichloroethane ug/kg 59.650 119 70-140
1,1,2,2-Tetrachloroethane ug/kg 51.450 103 74-133
1,1,2-Trichloroethane ug/kg 53.450 107 79-129
1,1-Dichloroethane ug/kg 68.150 136 72-139
1,1-Dichloroethene ug/kg 54.550 109 69-154
1,1-Dichloropropene ug/kg 52.150 104 74-138
1,2,3-Trichlorobenzene ug/kg 55.050 110 71-150
1,2,3-Trichloropropane ug/kg 50.750 101 74-135
1,2,4-Trichlorobenzene ug/kg 51.250 102 68-150
1,2,4-Trimethylbenzene ug/kg 52.550 105 70-130
1,2-Dibromo-3-chloropropane ug/kg 50.550 101 65-146
1,2-Dibromoethane (EDB)ug/kg 53.350 107 77-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 163 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
304373LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 54.650 109 75-141
1,2-Dichloroethane ug/kg 52.250 104 74-134
1,2-Dichloropropane ug/kg 52.450 105 77-138
1,3,5-Trimethylbenzene ug/kg 51.050 102 65-128
1,3-Dichlorobenzene ug/kg 53.250 106 76-133
1,3-Dichloropropane ug/kg 52.450 105 79-132
1,4-Dichlorobenzene ug/kg 52.750 105 75-137
2,2-Dichloropropane ug/kg 60.450 121 73-137
2-Butanone (MEK)ug/kg 102100 102 61-138
2-Chlorotoluene ug/kg 53.450 107 73-138
2-Hexanone ug/kg 107100 107 58-159
4-Chlorotoluene ug/kg 54.550 109 75-136
4-Methyl-2-pentanone (MIBK)ug/kg 103100 103 74-139
Acetone ug/kg 114100 114 58-150
Benzene ug/kg 55.050 110 71-140
Bromobenzene ug/kg 53.250 106 72-144
Bromochloromethane ug/kg 57.450 115 78-133
Bromodichloromethane ug/kg 52.350 105 78-133
Bromoform ug/kg 57.850 116 74-132
Bromomethane ug/kg 52.350 105 63-184
Carbon tetrachloride ug/kg 60.550 121 73-143
Chlorobenzene ug/kg 54.950 110 77-137
Chloroethane ug/kg 52.350 105 68-146
Chloroform ug/kg 55.250 110 75-137
Chloromethane ug/kg 53.150 106 54-143
cis-1,2-Dichloroethene ug/kg 53.350 107 71-143
cis-1,3-Dichloropropene ug/kg 54.850 110 76-133
Dibromochloromethane ug/kg 53.250 106 77-131
Dibromomethane ug/kg 58.750 117 63-184
Dichlorodifluoromethane ug/kg 46.650 93 36-173
Diisopropyl ether ug/kg 51.650 103 68-144
Ethylbenzene ug/kg 52.150 104 69-141
Hexachloro-1,3-butadiene ug/kg 50.550 101 70-152
Isopropylbenzene (Cumene)ug/kg 51.650 103 77-143
m&p-Xylene ug/kg 105100 105 72-138
Methyl-tert-butyl ether ug/kg 51.650 103 2-138
Methylene Chloride ug/kg 61.150 122 69-136
n-Butylbenzene ug/kg 50.850 102 65-128
n-Propylbenzene ug/kg 52.150 104 72-139
Naphthalene ug/kg 57.550 115 61-138
o-Xylene ug/kg 52.950 106 74-137
p-Isopropyltoluene ug/kg 51.450 103 66-128
sec-Butylbenzene ug/kg 50.950 102 72-140
Styrene ug/kg 54.350 109 76-137
tert-Butylbenzene ug/kg 51.950 104 68-141
Tetrachloroethene ug/kg 52.050 104 72-136
Toluene ug/kg 51.850 104 69-139
trans-1,2-Dichloroethene ug/kg 51.450 103 72-144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 164 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
304373LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 54.350 109 73-135
Trichloroethene ug/kg 54.050 108 75-136
Trichlorofluoromethane ug/kg 56.050 112 69-144
Vinyl acetate ug/kg 139100 139 50-150
Vinyl chloride ug/kg 58.150 116 61-145
Xylene (Total)ug/kg 158150 105 73-138
1,2-Dichloroethane-d4 (S)%98 69-121
4-Bromofluorobenzene (S)%100 74-115
Dibromofluoromethane (S)%102 79-116
Toluene-d8 (S)%100 88-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
304374MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9247665026
304375
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/kg 50.9 100 33-15895 .554ND51.2 51.4
Benzene ug/kg 50.9 94 46-14388 .354ND47.9 47.8
Chlorobenzene ug/kg 50.9 83 29-15975 554ND42.2 40.3
Toluene ug/kg 50.9 87 38-14580 354ND44.4 43.0
Trichloroethene ug/kg 50.9 94 70-13086 254ND47.7 46.6
1,2-Dichloroethane-d4 (S)%98 69-12198
4-Bromofluorobenzene (S)%98 74-11599
Dibromofluoromethane (S)%99 79-11699
Toluene-d8 (S)%100 88-11099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 165 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/7590
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:9247665037, 9247665038, 9247665039, 9247665040, 9247665041, 9247665042, 9247665043, 9247665044
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:304831
Associated Lab Samples:9247665037, 9247665038, 9247665039, 9247665040, 9247665041, 9247665042, 9247665043, 9247665044
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 07/08/09 11:38
1,1,1-Trichloroethane ug/L ND 1.0 07/08/09 11:38
1,1,2,2-Tetrachloroethane ug/L ND 1.0 07/08/09 11:38
1,1,2-Trichloroethane ug/L ND 1.0 07/08/09 11:38
1,1-Dichloroethane ug/L ND 1.0 07/08/09 11:38
1,1-Dichloroethene ug/L ND 1.0 07/08/09 11:38
1,1-Dichloropropene ug/L ND 1.0 07/08/09 11:38
1,2,3-Trichlorobenzene ug/L ND 1.0 07/08/09 11:38
1,2,3-Trichloropropane ug/L ND 1.0 07/08/09 11:38
1,2,4-Trichlorobenzene ug/L ND 1.0 07/08/09 11:38
1,2-Dibromo-3-chloropropane ug/L ND 3.0 07/08/09 11:38
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/08/09 11:38
1,2-Dichlorobenzene ug/L ND 1.0 07/08/09 11:38
1,2-Dichloroethane ug/L ND 1.0 07/08/09 11:38
1,2-Dichloropropane ug/L ND 1.0 07/08/09 11:38
1,3-Dichlorobenzene ug/L ND 1.0 07/08/09 11:38
1,3-Dichloropropane ug/L ND 1.0 07/08/09 11:38
1,4-Dichlorobenzene ug/L ND 1.0 07/08/09 11:38
2,2-Dichloropropane ug/L ND 1.0 07/08/09 11:38
2-Butanone (MEK)ug/L ND 5.0 07/08/09 11:38
2-Chlorotoluene ug/L ND 1.0 07/08/09 11:38
2-Hexanone ug/L ND 5.0 07/08/09 11:38
4-Chlorotoluene ug/L ND 1.0 07/08/09 11:38
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 07/08/09 11:38
Acetone ug/L ND 25.0 07/08/09 11:38
Benzene ug/L ND 1.0 07/08/09 11:38
Bromobenzene ug/L ND 1.0 07/08/09 11:38
Bromochloromethane ug/L ND 1.0 07/08/09 11:38
Bromodichloromethane ug/L ND 1.0 07/08/09 11:38
Bromoform ug/L ND 1.0 07/08/09 11:38
Bromomethane ug/L ND 5.0 07/08/09 11:38
Carbon tetrachloride ug/L ND 1.0 07/08/09 11:38
Chlorobenzene ug/L ND 1.0 07/08/09 11:38
Chloroethane ug/L ND 1.0 07/08/09 11:38
Chloroform ug/L ND 1.0 07/08/09 11:38
Chloromethane ug/L ND 1.0 07/08/09 11:38
cis-1,2-Dichloroethene ug/L ND 1.0 07/08/09 11:38
cis-1,3-Dichloropropene ug/L ND 1.0 07/08/09 11:38
Dibromochloromethane ug/L ND 1.0 07/08/09 11:38
Dibromomethane ug/L ND 1.0 07/08/09 11:38
Dichlorodifluoromethane ug/L ND 1.0 07/08/09 11:38
Diisopropyl ether ug/L ND 1.0 07/08/09 11:38
Ethylbenzene ug/L ND 1.0 07/08/09 11:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 166 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:304831
Associated Lab Samples:9247665037, 9247665038, 9247665039, 9247665040, 9247665041, 9247665042, 9247665043, 9247665044
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 1.0 07/08/09 11:38
m&p-Xylene ug/L ND 2.0 07/08/09 11:38
Methyl-tert-butyl ether ug/L ND 1.0 07/08/09 11:38
Methylene Chloride ug/L ND 2.0 07/08/09 11:38
Naphthalene ug/L ND 1.0 07/08/09 11:38
o-Xylene ug/L ND 1.0 07/08/09 11:38
p-Isopropyltoluene ug/L ND 1.0 07/08/09 11:38
Styrene ug/L ND 1.0 07/08/09 11:38
Tetrachloroethene ug/L ND 1.0 07/08/09 11:38
Toluene ug/L ND 1.0 07/08/09 11:38
trans-1,2-Dichloroethene ug/L ND 1.0 07/08/09 11:38
trans-1,3-Dichloropropene ug/L ND 1.0 07/08/09 11:38
Trichloroethene ug/L ND 1.0 07/08/09 11:38
Trichlorofluoromethane ug/L ND 1.0 07/08/09 11:38
Vinyl acetate ug/L ND 2.0 07/08/09 11:38
Vinyl chloride ug/L ND 1.0 07/08/09 11:38
1,2-Dichloroethane-d4 (S)%103 79-120 07/08/09 11:38
4-Bromofluorobenzene (S)%97 87-109 07/08/09 11:38
Dibromofluoromethane (S)%108 85-115 07/08/09 11:38
Toluene-d8 (S)%100 70-120 07/08/09 11:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
304832LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.350 105 83-125
1,1,1-Trichloroethane ug/L 62.450 125 80-129
1,1,2,2-Tetrachloroethane ug/L 51.450 103 73-127
1,1,2-Trichloroethane ug/L 53.150 106 77-123
1,1-Dichloroethane ug/L 68.8 L35013876-129
1,1-Dichloroethene ug/L 57.650 115 78-146
1,1-Dichloropropene ug/L 56.050 112 79-134
1,2,3-Trichlorobenzene ug/L 52.350 105 70-150
1,2,3-Trichloropropane ug/L 51.350 103 72-125
1,2,4-Trichlorobenzene ug/L 52.950 106 68-127
1,2-Dibromo-3-chloropropane ug/L 47.950 96 65-128
1,2-Dibromoethane (EDB)ug/L 54.450 109 81-125
1,2-Dichlorobenzene ug/L 55.450 111 82-126
1,2-Dichloroethane ug/L 52.950 106 72-126
1,2-Dichloropropane ug/L 53.550 107 80-127
1,3-Dichlorobenzene ug/L 54.850 110 82-124
1,3-Dichloropropane ug/L 54.150 108 79-124
1,4-Dichlorobenzene ug/L 53.650 107 79-125
2,2-Dichloropropane ug/L 66.050 132 58-140
2-Butanone (MEK)ug/L 104100 104 50-134
2-Chlorotoluene ug/L 53.650 107 81-126
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 167 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
304832LABORATORY CONTROL SAMPLE:
LCSSpike
2-Hexanone ug/L 106100 106 58-138
4-Chlorotoluene ug/L 57.350 115 82-126
4-Methyl-2-pentanone (MIBK)ug/L 92.6100 93 70-131
Acetone ug/L 100100 100 50-146
Benzene ug/L 55.750 111 78-128
Bromobenzene ug/L 52.750 105 81-127
Bromochloromethane ug/L 56.650 113 73-124
Bromodichloromethane ug/L 51.050 102 81-125
Bromoform ug/L 48.950 98 71-125
Bromomethane ug/L 82.0 L35016450-150
Carbon tetrachloride ug/L 58.950 118 81-137
Chlorobenzene ug/L 54.850 110 82-126
Chloroethane ug/L 48.650 97 69-140
Chloroform ug/L 56.150 112 77-129
Chloromethane ug/L 45.550 91 54-139
cis-1,2-Dichloroethene ug/L 54.850 110 76-133
cis-1,3-Dichloropropene ug/L 48.650 97 76-127
Dibromochloromethane ug/L 51.250 102 77-125
Dibromomethane ug/L 56.450 113 77-125
Dichlorodifluoromethane ug/L 42.350 85 50-150
Diisopropyl ether ug/L 52.950 106 74-131
Ethylbenzene ug/L 54.450 109 80-127
Hexachloro-1,3-butadiene ug/L 54.450 109 78-145
m&p-Xylene ug/L 110100 110 82-127
Methyl-tert-butyl ether ug/L 53.250 106 71-130
Methylene Chloride ug/L 63.250 126 67-133
Naphthalene ug/L 48.150 96 52-136
o-Xylene ug/L 54.350 109 83-124
p-Isopropyltoluene ug/L 54.750 109 73-122
Styrene ug/L 49.650 99 80-130
Tetrachloroethene ug/L 55.150 110 78-128
Toluene ug/L 52.550 105 76-126
trans-1,2-Dichloroethene ug/L 53.350 107 78-134
trans-1,3-Dichloropropene ug/L 47.350 95 75-125
Trichloroethene ug/L 53.750 107 79-127
Trichlorofluoromethane ug/L 50.950 102 76-148
Vinyl acetate ug/L 67.7100 68 50-150
Vinyl chloride ug/L 52.650 105 67-143
1,2-Dichloroethane-d4 (S)%96 79-120
4-Bromofluorobenzene (S)%101 87-109
Dibromofluoromethane (S)%102 85-115
Toluene-d8 (S)%99 70-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 168 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
304836MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9247665040
304837
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L M05015460-150147 550ND77.2 73.7
Benzene ug/L 50 136 74-136132 350ND68.0 65.9
Chlorobenzene ug/L 50 128 79-135122 550ND64.2 61.2
Toluene ug/L 50 128 73-131125 250ND64.3 62.9
Trichloroethene ug/L 50 122 73-131116 650ND61.4 57.9
1,2-Dichloroethane-d4 (S)%105 79-120104
4-Bromofluorobenzene (S)%94 87-10993
Dibromofluoromethane (S)%107 85-115107
Toluene-d8 (S)%100 70-120101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 169 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/2568
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:9247665004
Parameter Units
Dup
Result QualifiersRPDResult
9247665004
303525SAMPLE DUPLICATE:
Percent Moisture %24.0 .924.2
Parameter Units
Dup
Result QualifiersRPDResult
9247814001
303526SAMPLE DUPLICATE:
Percent Moisture %5.6 35.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 170 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/7578
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:9247665017, 9247665018, 9247665019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:304277
Associated Lab Samples:9247665017, 9247665018, 9247665019
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/07/09 12:18
1,1,1-Trichloroethane ug/kg ND 5.0 07/07/09 12:18
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/07/09 12:18
1,1,2-Trichloroethane ug/kg ND 5.0 07/07/09 12:18
1,1-Dichloroethane ug/kg ND 5.0 07/07/09 12:18
1,1-Dichloroethene ug/kg ND 5.0 07/07/09 12:18
1,1-Dichloropropene ug/kg ND 5.0 07/07/09 12:18
1,2,3-Trichlorobenzene ug/kg ND 5.0 07/07/09 12:18
1,2,3-Trichloropropane ug/kg ND 5.0 07/07/09 12:18
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/07/09 12:18
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/07/09 12:18
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 07/07/09 12:18
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/07/09 12:18
1,2-Dichlorobenzene ug/kg ND 5.0 07/07/09 12:18
1,2-Dichloroethane ug/kg ND 5.0 07/07/09 12:18
1,2-Dichloropropane ug/kg ND 5.0 07/07/09 12:18
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/07/09 12:18
1,3-Dichlorobenzene ug/kg ND 5.0 07/07/09 12:18
1,3-Dichloropropane ug/kg ND 5.0 07/07/09 12:18
1,4-Dichlorobenzene ug/kg ND 5.0 07/07/09 12:18
2,2-Dichloropropane ug/kg ND 5.0 07/07/09 12:18
2-Butanone (MEK)ug/kg ND 100 07/07/09 12:18
2-Chlorotoluene ug/kg ND 5.0 07/07/09 12:18
2-Hexanone ug/kg ND 50.0 07/07/09 12:18
4-Chlorotoluene ug/kg ND 5.0 07/07/09 12:18
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/07/09 12:18
Acetone ug/kg ND 100 07/07/09 12:18
Benzene ug/kg ND 5.0 07/07/09 12:18
Bromobenzene ug/kg ND 5.0 07/07/09 12:18
Bromochloromethane ug/kg ND 5.0 07/07/09 12:18
Bromodichloromethane ug/kg ND 5.0 07/07/09 12:18
Bromoform ug/kg ND 5.0 07/07/09 12:18
Bromomethane ug/kg ND 10.0 07/07/09 12:18
Carbon tetrachloride ug/kg ND 5.0 07/07/09 12:18
Chlorobenzene ug/kg ND 5.0 07/07/09 12:18
Chloroethane ug/kg ND 10.0 07/07/09 12:18
Chloroform ug/kg ND 5.0 07/07/09 12:18
Chloromethane ug/kg ND 10.0 07/07/09 12:18
cis-1,2-Dichloroethene ug/kg ND 5.0 07/07/09 12:18
cis-1,3-Dichloropropene ug/kg ND 5.0 07/07/09 12:18
Dibromochloromethane ug/kg ND 5.0 07/07/09 12:18
Dibromomethane ug/kg ND 5.0 07/07/09 12:18
Dichlorodifluoromethane ug/kg ND 10.0 07/07/09 12:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 171 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:304277
Associated Lab Samples:9247665017, 9247665018, 9247665019
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.0 07/07/09 12:18
Ethylbenzene ug/kg ND 5.0 07/07/09 12:18
Hexachloro-1,3-butadiene ug/kg ND 5.0 07/07/09 12:18
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/07/09 12:18
m&p-Xylene ug/kg ND 10.0 07/07/09 12:18
Methyl-tert-butyl ether ug/kg ND 5.0 07/07/09 12:18
Methylene Chloride ug/kg ND 20.0 07/07/09 12:18
n-Butylbenzene ug/kg ND 5.0 07/07/09 12:18
n-Propylbenzene ug/kg ND 5.0 07/07/09 12:18
Naphthalene ug/kg ND 5.0 07/07/09 12:18
o-Xylene ug/kg ND 5.0 07/07/09 12:18
p-Isopropyltoluene ug/kg ND 5.0 07/07/09 12:18
sec-Butylbenzene ug/kg ND 5.0 07/07/09 12:18
Styrene ug/kg ND 5.0 07/07/09 12:18
tert-Butylbenzene ug/kg ND 5.0 07/07/09 12:18
Tetrachloroethene ug/kg ND 5.0 07/07/09 12:18
Toluene ug/kg ND 5.0 07/07/09 12:18
trans-1,2-Dichloroethene ug/kg ND 5.0 07/07/09 12:18
trans-1,3-Dichloropropene ug/kg ND 5.0 07/07/09 12:18
Trichloroethene ug/kg ND 5.0 07/07/09 12:18
Trichlorofluoromethane ug/kg ND 5.0 07/07/09 12:18
Vinyl acetate ug/kg ND 50.0 07/07/09 12:18
Vinyl chloride ug/kg ND 10.0 07/07/09 12:18
Xylene (Total)ug/kg ND 10.0 07/07/09 12:18
1,2-Dichloroethane-d4 (S)%94 69-121 07/07/09 12:18
4-Bromofluorobenzene (S)%104 74-115 07/07/09 12:18
Dibromofluoromethane (S)%100 79-116 07/07/09 12:18
Toluene-d8 (S)%100 88-110 07/07/09 12:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
304278LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 56.550 113 75-137
1,1,1-Trichloroethane ug/kg 61.150 122 70-140
1,1,2,2-Tetrachloroethane ug/kg 59.050 118 74-133
1,1,2-Trichloroethane ug/kg 58.750 117 79-129
1,1-Dichloroethane ug/kg 67.550 135 72-139
1,1-Dichloroethene ug/kg 55.450 111 69-154
1,1-Dichloropropene ug/kg 56.650 113 74-138
1,2,3-Trichlorobenzene ug/kg 56.450 113 71-150
1,2,3-Trichloropropane ug/kg 56.750 113 74-135
1,2,4-Trichlorobenzene ug/kg 58.450 117 68-150
1,2,4-Trimethylbenzene ug/kg 57.050 114 70-130
1,2-Dibromo-3-chloropropane ug/kg 46.650 93 65-146
1,2-Dibromoethane (EDB)ug/kg 58.950 118 77-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 172 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
304278LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 55.350 111 75-141
1,2-Dichloroethane ug/kg 51.350 103 74-134
1,2-Dichloropropane ug/kg 55.450 111 77-138
1,3,5-Trimethylbenzene ug/kg 55.450 111 65-128
1,3-Dichlorobenzene ug/kg 58.950 118 76-133
1,3-Dichloropropane ug/kg 56.050 112 79-132
1,4-Dichlorobenzene ug/kg 55.250 110 75-137
2,2-Dichloropropane ug/kg 63.850 128 73-137
2-Butanone (MEK)ug/kg 106100 106 61-138
2-Chlorotoluene ug/kg 56.250 112 73-138
2-Hexanone ug/kg 106100 106 58-159
4-Chlorotoluene ug/kg 60.450 121 75-136
4-Methyl-2-pentanone (MIBK)ug/kg 104100 104 74-139
Acetone ug/kg 107100 107 58-150
Benzene ug/kg 57.250 114 71-140
Bromobenzene ug/kg 54.250 108 72-144
Bromochloromethane ug/kg 65.750 131 78-133
Bromodichloromethane ug/kg 53.250 106 78-133
Bromoform ug/kg 56.450 113 74-132
Bromomethane ug/kg 35.550 71 63-184
Carbon tetrachloride ug/kg 60.350 121 73-143
Chlorobenzene ug/kg 61.950 124 77-137
Chloroethane ug/kg 41.650 83 68-146
Chloroform ug/kg 58.050 116 75-137
Chloromethane ug/kg 45.450 91 54-143
cis-1,2-Dichloroethene ug/kg 53.250 106 71-143
cis-1,3-Dichloropropene ug/kg 56.350 113 76-133
Dibromochloromethane ug/kg 55.950 112 77-131
Dibromomethane ug/kg 62.350 125 63-184
Dichlorodifluoromethane ug/kg 34.250 68 36-173
Diisopropyl ether ug/kg 52.050 104 68-144
Ethylbenzene ug/kg 58.850 118 69-141
Hexachloro-1,3-butadiene ug/kg 54.450 109 70-152
Isopropylbenzene (Cumene)ug/kg 58.950 118 77-143
m&p-Xylene ug/kg 115100 115 72-138
Methyl-tert-butyl ether ug/kg 55.050 110 2-138
Methylene Chloride ug/kg 58.650 117 69-136
n-Butylbenzene ug/kg 56.750 113 65-128
n-Propylbenzene ug/kg 57.050 114 72-139
Naphthalene ug/kg 56.850 114 61-138
o-Xylene ug/kg 57.050 114 74-137
p-Isopropyltoluene ug/kg 57.250 114 66-128
sec-Butylbenzene ug/kg 55.750 111 72-140
Styrene ug/kg 61.550 123 76-137
tert-Butylbenzene ug/kg 55.350 111 68-141
Tetrachloroethene ug/kg 61.850 124 72-136
Toluene ug/kg 56.250 112 69-139
trans-1,2-Dichloroethene ug/kg 52.250 104 72-144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 173 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
304278LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 54.850 110 73-135
Trichloroethene ug/kg 60.250 120 75-136
Trichlorofluoromethane ug/kg 47.250 94 69-144
Vinyl acetate ug/kg 103100 103 50-150
Vinyl chloride ug/kg 46.450 93 61-145
Xylene (Total)ug/kg 172150 115 73-138
1,2-Dichloroethane-d4 (S)%88 69-121
4-Bromofluorobenzene (S)%105 74-115
Dibromofluoromethane (S)%98 79-116
Toluene-d8 (S)%100 88-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
304779MATRIX SPIKE SAMPLE:
MSSpike
Result
9247727003
1,1-Dichloroethene ug/kg 51.753.8 96 33-158ND
Benzene ug/kg 50.453.8 94 46-143ND
Chlorobenzene ug/kg 49.953.8 93 29-159ND
Toluene ug/kg 48.853.8 91 38-145ND
Trichloroethene ug/kg 50.953.8 95 70-130ND
1,2-Dichloroethane-d4 (S)%97 69-121
4-Bromofluorobenzene (S)%97 74-115
Dibromofluoromethane (S)%97 79-116
Toluene-d8 (S)%101 88-110
Parameter Units
Dup
Result QualifiersRPDResult
9247766010
304778SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 174 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
Dup
Result QualifiersRPDResult
9247766010
304778SAMPLE DUPLICATE:
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 175 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
Dup
Result QualifiersRPDResult
9247766010
304778SAMPLE DUPLICATE:
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%98 498
4-Bromofluorobenzene (S)%97 9102
Dibromofluoromethane (S)%98 6100
Toluene-d8 (S)%101 3100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 176 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/7698
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:9247665035
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:310668
Associated Lab Samples:9247665035
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 07/21/09 10:05
1,1,1-Trichloroethane ug/L ND 1.0 07/21/09 10:05
1,1,2,2-Tetrachloroethane ug/L ND 1.0 07/21/09 10:05
1,1,2-Trichloroethane ug/L ND 1.0 07/21/09 10:05
1,1-Dichloroethane ug/L ND 1.0 07/21/09 10:05
1,1-Dichloroethene ug/L ND 1.0 07/21/09 10:05
1,1-Dichloropropene ug/L ND 1.0 07/21/09 10:05
1,2,3-Trichlorobenzene ug/L ND 1.0 07/21/09 10:05
1,2,3-Trichloropropane ug/L ND 1.0 07/21/09 10:05
1,2,4-Trichlorobenzene ug/L ND 1.0 07/21/09 10:05
1,2-Dibromo-3-chloropropane ug/L ND 3.0 07/21/09 10:05
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/21/09 10:05
1,2-Dichlorobenzene ug/L ND 1.0 07/21/09 10:05
1,2-Dichloroethane ug/L ND 1.0 07/21/09 10:05
1,2-Dichloropropane ug/L ND 1.0 07/21/09 10:05
1,3-Dichlorobenzene ug/L ND 1.0 07/21/09 10:05
1,3-Dichloropropane ug/L ND 1.0 07/21/09 10:05
1,4-Dichlorobenzene ug/L ND 1.0 07/21/09 10:05
2,2-Dichloropropane ug/L ND 1.0 07/21/09 10:05
2-Butanone (MEK)ug/L ND 5.0 07/21/09 10:05
2-Chlorotoluene ug/L ND 1.0 07/21/09 10:05
2-Hexanone ug/L ND 5.0 07/21/09 10:05
4-Chlorotoluene ug/L ND 1.0 07/21/09 10:05
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 07/21/09 10:05
Acetone ug/L ND 25.0 07/21/09 10:05
Benzene ug/L ND 1.0 07/21/09 10:05
Bromobenzene ug/L ND 1.0 07/21/09 10:05
Bromochloromethane ug/L ND 1.0 07/21/09 10:05
Bromodichloromethane ug/L ND 1.0 07/21/09 10:05
Bromoform ug/L ND 1.0 07/21/09 10:05
Bromomethane ug/L ND 5.0 07/21/09 10:05
Carbon tetrachloride ug/L ND 1.0 07/21/09 10:05
Chlorobenzene ug/L ND 1.0 07/21/09 10:05
Chloroethane ug/L ND 1.0 07/21/09 10:05
Chloroform ug/L ND 1.0 07/21/09 10:05
Chloromethane ug/L ND 1.0 07/21/09 10:05
cis-1,2-Dichloroethene ug/L ND 1.0 07/21/09 10:05
cis-1,3-Dichloropropene ug/L ND 1.0 07/21/09 10:05
Dibromochloromethane ug/L ND 1.0 07/21/09 10:05
Dibromomethane ug/L ND 1.0 07/21/09 10:05
Dichlorodifluoromethane ug/L ND 1.0 07/21/09 10:05
Diisopropyl ether ug/L ND 1.0 07/21/09 10:05
Ethylbenzene ug/L ND 1.0 07/21/09 10:05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 177 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:310668
Associated Lab Samples:9247665035
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 1.0 07/21/09 10:05
m&p-Xylene ug/L ND 2.0 07/21/09 10:05
Methyl-tert-butyl ether ug/L ND 1.0 07/21/09 10:05
Methylene Chloride ug/L ND 2.0 07/21/09 10:05
Naphthalene ug/L ND 1.0 07/21/09 10:05
o-Xylene ug/L ND 1.0 07/21/09 10:05
p-Isopropyltoluene ug/L ND 1.0 07/21/09 10:05
Styrene ug/L ND 1.0 07/21/09 10:05
Tetrachloroethene ug/L ND 1.0 07/21/09 10:05
Toluene ug/L ND 1.0 07/21/09 10:05
trans-1,2-Dichloroethene ug/L ND 1.0 07/21/09 10:05
trans-1,3-Dichloropropene ug/L ND 1.0 07/21/09 10:05
Trichloroethene ug/L ND 1.0 07/21/09 10:05
Trichlorofluoromethane ug/L ND 1.0 07/21/09 10:05
Vinyl acetate ug/L ND 2.0 07/21/09 10:05
Vinyl chloride ug/L ND 1.0 07/21/09 10:05
1,2-Dichloroethane-d4 (S)%108 79-120 07/21/09 10:05
4-Bromofluorobenzene (S)%100 87-109 07/21/09 10:05
Dibromofluoromethane (S)%106 85-115 07/21/09 10:05
Toluene-d8 (S)%100 70-120 07/21/09 10:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
310669LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.550 111 83-125
1,1,1-Trichloroethane ug/L 62.050 124 80-129
1,1,2,2-Tetrachloroethane ug/L 54.850 110 73-127
1,1,2-Trichloroethane ug/L 53.150 106 77-123
1,1-Dichloroethane ug/L 67.2 L35013476-129
1,1-Dichloroethene ug/L 50.950 102 78-146
1,1-Dichloropropene ug/L 53.450 107 79-134
1,2,3-Trichlorobenzene ug/L 55.450 111 70-150
1,2,3-Trichloropropane ug/L 50.550 101 72-125
1,2,4-Trichlorobenzene ug/L 53.050 106 68-127
1,2-Dibromo-3-chloropropane ug/L 48.450 97 65-128
1,2-Dibromoethane (EDB)ug/L 52.650 105 81-125
1,2-Dichlorobenzene ug/L 54.650 109 82-126
1,2-Dichloroethane ug/L 53.150 106 72-126
1,2-Dichloropropane ug/L 53.350 107 80-127
1,3-Dichlorobenzene ug/L 53.450 107 82-124
1,3-Dichloropropane ug/L 53.050 106 79-124
1,4-Dichlorobenzene ug/L 51.250 102 79-125
2,2-Dichloropropane ug/L 65.350 131 58-140
2-Butanone (MEK)ug/L 102100 102 50-134
2-Chlorotoluene ug/L 53.050 106 81-126
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 178 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
310669LABORATORY CONTROL SAMPLE:
LCSSpike
2-Hexanone ug/L 113100 113 58-138
4-Chlorotoluene ug/L 56.550 113 82-126
4-Methyl-2-pentanone (MIBK)ug/L 107100 107 70-131
Acetone ug/L 106100 106 50-146
Benzene ug/L 54.350 109 78-128
Bromobenzene ug/L 53.750 107 81-127
Bromochloromethane ug/L 58.150 116 73-124
Bromodichloromethane ug/L 50.650 101 81-125
Bromoform ug/L 53.350 107 71-125
Bromomethane ug/L 54.450 109 50-150
Carbon tetrachloride ug/L 59.150 118 81-137
Chlorobenzene ug/L 53.250 106 82-126
Chloroethane ug/L 50.350 101 69-140
Chloroform ug/L 53.250 106 77-129
Chloromethane ug/L 50.150 100 54-139
cis-1,2-Dichloroethene ug/L 52.150 104 76-133
cis-1,3-Dichloropropene ug/L 54.650 109 76-127
Dibromochloromethane ug/L 53.150 106 77-125
Dibromomethane ug/L 57.450 115 77-125
Dichlorodifluoromethane ug/L 53.650 107 50-150
Diisopropyl ether ug/L 48.750 97 74-131
Ethylbenzene ug/L 54.150 108 80-127
Hexachloro-1,3-butadiene ug/L 51.550 103 78-145
m&p-Xylene ug/L 92.5100 93 82-127
Methyl-tert-butyl ether ug/L 48.850 98 71-130
Methylene Chloride ug/L 59.550 119 67-133
Naphthalene ug/L 50.950 102 52-136
o-Xylene ug/L 54.950 110 83-124
p-Isopropyltoluene ug/L 48.050 96 73-122
Styrene ug/L 48.250 96 80-130
Tetrachloroethene ug/L 54.250 108 78-128
Toluene ug/L 50.850 102 76-126
trans-1,2-Dichloroethene ug/L 49.750 99 78-134
trans-1,3-Dichloropropene ug/L 54.250 108 75-125
Trichloroethene ug/L 53.750 107 79-127
Trichlorofluoromethane ug/L 49.750 99 76-148
Vinyl acetate ug/L 84.0100 84 50-150
Vinyl chloride ug/L 48.450 97 67-143
1,2-Dichloroethane-d4 (S)%99 79-120
4-Bromofluorobenzene (S)%101 87-109
Dibromofluoromethane (S)%99 85-115
Toluene-d8 (S)%100 70-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 179 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
310670MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9248774013
310671
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 50 122 60-150120 250ND60.9 59.9
Benzene ug/L 50 116 74-136117 150ND57.8 58.4
Chlorobenzene ug/L 50 110 79-135114 350ND55.2 57.0
Toluene ug/L 50 108 73-131110 250ND54.0 54.8
Trichloroethene ug/L 50 108 73-131110 250ND54.1 55.2
1,2-Dichloroethane-d4 (S)%97 79-120101
4-Bromofluorobenzene (S)%97 87-10995
Dibromofluoromethane (S)%96 85-11596
Toluene-d8 (S)%97 70-12097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 180 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/2571
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:9247665006, 9247665007, 9247665008, 9247665009, 9247665012, 9247665013, 9247665014, 9247665015,9247665016, 9247665017
Parameter Units
Dup
Result QualifiersRPDResult
9247873005
303656SAMPLE DUPLICATE:
Percent Moisture %21.7 221.3
Parameter Units
Dup
Result QualifiersRPDResult
9247665015
303657SAMPLE DUPLICATE:
Percent Moisture %6.8 86.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 181 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/2575
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:9247665010, 9247665011
Parameter Units
Dup
Result QualifiersRPDResult
9247665010
304742SAMPLE DUPLICATE:
Percent Moisture %5.5 25.7
Parameter Units
Dup
Result QualifiersRPDResult
9248034001
304743SAMPLE DUPLICATE:
Percent Moisture %18.9 418.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 182 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/2567
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:9247665005
Parameter Units
Dup
Result QualifiersRPDResult
9247658013
303523SAMPLE DUPLICATE:
Percent Moisture %19.3 620.5
Parameter Units
Dup
Result QualifiersRPDResult
9247672002
303524SAMPLE DUPLICATE:
Percent Moisture %34.2 234.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 183 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALIFIERS
Pace Project No.:
Project:
9247665
SILVERMAN PROPERTY 1411-09-025
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Acid surrogate recovery is outside of control limits. The data was accepted based on valid recovery of the two remainingacid surrogates.1g
Base/neutral surrogate recovery is outside of control limits. The data was accepted based on valid recovery of the tworemaining base/neutral surrogates.2g
Re-extraction conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time.3g
Surrogate recovery outside laboratory control limits due to matrix interferences.4g
The sample was a non-homogenous sample.5g
Analyte was detected in the associated method blank.B
Common Laboratory Contaminant.C9
Analysis conducted outside the EPA method holding time.H1
The internal standard recovery associated with this result exceeds the upper control limit. The reported result should beconsidered an estimated value.IR
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.L3
Matrix spike recovery was outside laboratory control limits.M0
Sample extract could not be concentrated to the routine final volume, resulting in elevated reporting limits.P3
Matrix spike recovery was outside laboratory control limits due to a parent sample concentration notably higher than thespike level.P6
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 07/27/2009 03:47 PM Page 184 of 184
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
I I
/-:ZeAnaJyticar
CHAIN-OF-CUSTODY I Analytical Request Document I
The Chain-of-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
' www.paeelabs.com
Section A Section B Section C
Page: :::<. [ of -~
Required Client Information: Required Project Information: Invoice Information: J 166710 Company: ,<;' .J.-m G ·1..-r Report To: ~,;' ,, ~ /J In J/tD ~ Attention: <:::__
Addres51./£,/ ~ 1 ,c,k ~<..};11~~/2J4 ~Ill) To:
., -, Company Name: ~ ..... rJ JitEGULATORYAGENCY ·y "'-.
J l-rd.ir1 -All/ 2Y 7 {) l./ Address: r· NPDES r GROUND WATER r DRINKING WATER
~ 5-rpk)yvV'fPA~I__,.-;..-Purcfilse Order No.: Pace Quote r UST r RCRA )(I 'I OTH6UvltMl~
~ Reference:
Ph~ ~<;S-'I?: -9 tJ ?f 0 Project Name~J }i/e,/~ /~ .A..-. '4-V Pace Project }c;p.A Jv\ f/ey~ Site Location AJL, l
Manager: )!
Requested Due Date/TAT: _, ~ Project Number: ll/// -o-t; -o;d S-I Pace Profile #: / STATE: l J7'?f I
Requested Analysis Filtered (YIN) -Section D Matrix Codes ~ iL' z
Required Client Information MATRIX I CODE ::;; COLLECTED Preservatives ):: g 0 Drinking Water ow :fl 0 z
Water WT 8 II 0 0 COMPOSITE COMPOSITE j:: V' ~ c1 Waste Water WW " "' ENO/GRAB 0 i z ~1(sf.6; START w ~ Product p Tl! ~ _J ~ SoiVSolid SL " _J
! (!) 0 en .. " ' SAMPLE ID Oil OL II 0 0:: ! <D
Wipe WP ~ f-w I~ c c c
(A-Z, 0-9/ ,-) w <!'. z ~ ,.... -~
I
Air AR 0 w a. ~ al .....J I~ :;:; Sample IDs MUST BE UNIQUE Tissue TS 0 a. ::;; i I~ ~ t ~. () ~ w ~ ~ ~' Other OT u f-z 0 r::: \: x w w 0 <D 0 c ro I 'It ii'. _J _J u "' ... <ti ::> ~o 0 I N Q; r~ "O :E a. a. u. 0 CfJ... .c I-::;; ::;; c. (f) ·u;
Paci
w <!'. 0 z u 1D .c < < <!'. C N <ti <ti 0 <D !:: ::;: (fJ DATE TIME DATE TIME (fJ 'It ::JI I I zz :::?: .. 0:: Project No.~ Lab l.D.
1 >'Jl.l/DulJ)/r~ J ·-Ob -o'i ,5L I~ '1:$o-c:."j -lJ x x )( "Y. v.: "/.. l) I~
2 ~JLV ~ . fu :0 lfir11<Jfp _,-y_ -oG lcJ1 J4:ill 11 ')( '}( )( y )( IV I ("'i~c)J ~
3 ~, Lv ... :<..Vfl.::io --~-.,{.,.. --oG SL '"':'I.'\ " '}I IX )( y IV " ( L '-~I\
4 ~Jl.V -<..t'UJJ -I ' 'O.•oiJ ,, x )( x ). ,~ -=: ' I ::> ~ l \ 0 "" --C> c, j)C )(
s ~ J LV -<:. o .:J:::J -n t-. -(") C-t /l(•<c:. ~ x )l ·~ -p t 1:-~ 1 If 'i y -\
s ~)L.\/' -~p.,;:;r~. -CY--ct; l~Sl JI )( x x )( )( ") ' .:r \ '(.,. I ....
1 ~ 1 L \J -.<.ii..!J4 -o~ -0~ II~· 1" 11 ) " x v .x .1' u \ '-./\
a < 1 L II -...::: ?i -u ~ -D~ //.,.':l5 4 "' ')(' I rlND
~I LV -SlLJ 7-DL-. ·-C> <J ti~;lJ4~ I.I y IX I T)Q\ 9
10 SJLV-~.~,.O,<\ ~ --0 9 '/b:S5 1 j x x x ')( )( rx i ) 1
11 I tr I
12 " ADDITIONAL COMMENTS h INQlj"'lfe.fJdY I AFFILIATI~ ~ DATE TIME /.. ACCEPTED BY I AFFILIATION DA"!:-E TIME SAM E CONDITIONS
~J"-"" &-3D-oC! J'iJ!vo ~(~~ l'./~-;,f. /~ -00 -:;;, / ~ y
~ r V" -~ ~ .. ( (
SAMPLER NAME AND SIGNATURE c: l;; " p o-,., 0 .l9 "'z "'o-E-ORIGINAL PRINT Name of SAMPLER: .""-v ,, [, -..........,/Jt-,-,,. d/ -E -~~ ooz "'z a. 00 "O):: ~):: E "" ".,_ a.-"" 0 a;
SIGNATURE of SAMPLER:~ fl}. ~--~ DATE Signed l:.-b-oct; " " -E f-ct: " "' (MM/DD/YY): (fJ (fJ
*Important Note: By signing this form you are accepting Pace's NET 30 day oavment terms and aareeino to late chanles of 1.5% oer m6Tith for any invoices not paid within 30 days. I F-ALL-Q-020rev . 7, 15-May-2007
/-:lee Analytical'
www.pacelabs.com
CHAIN-OF-CUSTODY I Analytical Request Document
The Chain-of-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C Page: g ljot -3
Required Client Information: Required Project Information: Invoice Information:
Company"Sff'YJ j;;. ;y;}l"Lr r\ Attention: "1 166711 ReportTo: Sr~/J}n~
Addre'4ftf.~vdC~5 /4-Jc·. ~ Copy To: ~ ~
Company Name: REGULATORY AGENCY
IA,r~ ./Jc ~JtJL/ Address: r-11 D~KING w-oTER ~~'e{J< r NPDES r GROUND WATER
~"ZJ ~ (2 5~'>--c .~c:~ase Order No.: Pace Quote
Reference: ; r UST r RCRA
I
,r:x:-o -(;,.~ j7'x.:_. ~ O'&-O !Project Name: ?::.:::>/IVV"~
~J--cA IProjectNumber/V// ..O'j -l>.;JS-1
//a1/Juf-I/
Requested Due Date/TAT:
Pace Project / ,. / /
Manager: f,L1:71 fY'1 ~~Ct
Pace Profile #: ---' __,/
Site location A/[,/ STATE:
'II: :. w t:
Section D
Required Client Information
Matrix Codes ~ iL MATRIX I CODE ~ B 0 Drinking Water ow ~ u
Water WT " II 8 u
Waste Water WW " "'
SAMPLE ID
(A-Z, 0-9 / ,-)
Sample IDs MUST BE UNIQUE
Product p ~ ~ Soil/Solid SL ~ (!)
Oil OL ! II (!) Wipe WP ~
Air AR w 0 w Tissue TS 0 ~
Other OT (.) i': >< w a:: ~ ~ I-~ <{ ~ ~ w
~ILV-/r1/J iJ.)BMk) -Dt..-oct I.drib.
21 Sil I./ -:Tn·~/1..J,~0--ot.. -O'i I 11
3 -:::::,, J \/-Trip ~)~ .2 ~ ~d:t l "1 l\l/ -. I 4
5
6
7
8
9
10
11
COLLECTED
COMPOSITE
START
COMPOSITE
END/GRAB
z 0 ~ w ~ ~ 0 1-~~~~~~~-+-~~~~~~~-1 u
DATE TIME
I
TIME ----
~
~ ~ ~ w ~ ~ ~ ~ w
12 A?
~ w z ~ z 0 (.)
u_
0
'II:
I~
,,;;
1;:;z
Preservatives
"O Q) ~
[lg'l 0 l-l 6 cNZ(.)cc :::>J:J:J:Z
"'10 q, lijl ~ Ci) ..c Q)
N -..C cc Q) -z ::2: 0
-z: ):
Requested Analysis Filtered (YIN)
... to i!_ '\ I~ f ~ -);
x
')
ADDITIONAL COMMENTS ~~SJIED BY I AFFILIA~ DATE I TIME I /_ACCEPTED BY I AFFILIATION DATE I TIME
z ~
Q) c "§ :c (.)
Cii :::J
"O ·c;;
Q)
Ct'.
~ l~-3>cf'tl1~.·cl>I $:.~ ~£..., lt~::<S o IA/./
A""" 11 /
SAMPLERNAME AND SIGNATURE ;
ORIGINAL PRINT Name of SAMPLER: ~ oi.-1-1-~I /)~ ~-
~D<./' _-. ~ 'A __..,.;;.-rDATE Signed / . -,.. 0 s1GNATUREotSAMPL~....4".A-'~---:::-I (MM/DDIYY): ~-~o-0 1
~
.S c. E ~
I
ctrnldn~
I
I
PacU Project No./ Lab l.D.
~ I ~
SAMIUE CONDITIONS
v
c:
0 -.,, z %!~ -~ ~ ,, _
a::
/l./
Q;
>. 0 .,, 0 -~;-; ~ ",,_ u <ii " w
v
tl .sl c: ~~ c.-E "' w ---Important Note: By signing this form you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5% per month for any invoices not paid within 30 days. F-ALL-Q-020rev.ti7. 15-Mav-2007
.;,'.r''~·~u;;•<;~tt~™~~{;. u:.; tOD'f ! An~:!l}r~k:Cil Req;.l~£K~USTODY I Analytical Request Document ' .. ·.·./ -./18ceAri!iJyffcaf·r:;.,._,t. .. .; ,. ;, "' .. t'G•'' ~'· Y• ,,;.;_,,,._Ai•·· """ """ ~,,,o,; ;,,, ·~m.!r1'd~Y is a LEGAL DOCUMENT. All relevant fields must be com~ accUiate1y.
. -...... llS.COlll
Section A Section B Section C Page: I I
Requl,.d Client Information: Requll9d Project Information:
Compeny: ~ 't' ME. I nr IReport To: ~-_-rr-~bJ#1 ~
Invoice Information:
Attenllon: 11166873
r l>ffl!/ ·/Vik ~k }&J-r~w .~ico!iYTo:-- -·-y -.--.. ·~-.. , · ·-.. ·-· --· -~ REGULATORY AGENCY I
Address: -r NPoes r GRouNo wAiER r I pR1NK1NG wATit.R 1 1.,,.! ~:::!a;;,:;:.~...!.-~::..=::;....~..:;;;;~..L;.::;....,1-11-:.--..,......~-=-.,.,.....~~~~~~~~~~~~~~~:8-~~~~ ... ~,~~~~~~~~~~~----1 r usT r RCRA '")('lprHe~~I
fl!:::_ Phone: Siie Location
Requested Due DatefTAT: Project Number: STA7E!
Requested Analysis Filtered (YIN)
SKtlonD
•RequlllldClent lnfmnallon
SAMPLE ID
Matrix Codes
MAJB!X I COPE
Drinki1"9 Waler OW
Water WT
Waste Water WW
Product p
Soil/Solid SL
Oil OL
f ~I s I u I 3! J ~ l (!)
II !2. Wipe WP
(A-Z. 0-91 ,-) Air AR ~ w
Sample IDs MUST BE UNIQUE Tl$sue TS O ~
Other OT 0 1-
• 1 ~ ~ ~ a: ~ w ..... ~
!:: ... i 4li
11su .. v--rw.l-S51-.....:o?-~o'i'P6~
2l'51Lv-/w~ -ss::J-tt7-oct-
3 IS,LV -DulJUcuk I -o/ -oq
·dSJLV-sglf< -o'J. -o~ W
s 1.c;JL.V -&..vii'> ~In~ -07'"llqlWJ
s ~JLV --~Jl lc.ka -07-o«:f lsL
1 ISIL.V -SlbJ? -0 .. ,., -0 q ---·-------
a 15;JLV-S~ I.~ -c/ -oc-1
11~>.LV -~JL/ -o/ -6q
101 ~tL.V -.5~1.~ -D'1-o., -V'l~IV
111 SJLV-Jlroi..-tD~k 1-6~,; , ~ ' 12
COLLECTED
Cor.POSJTE I COMPOSITE
START ENC/GRAB ~ ... 8 l/J a: ..... w < z ~ ~ w ~ .....
~ 0
~
DATE TIME DATE I TIME 4li
!?·J .. 011 Jl!'te\"
! 11~
~~h. •-< UP.15_.....IF
lJ:'l.<f' I t
'l
l&:tl.<t I w
/.:t;<"'\f It:
lt/ltxi IL. I LJ; ,('1 .-&.J--.:::J " ""
Preservatives -z ;:
.. -;: c {!.
:B ... .. -a .!! ~~o li~o :x:l'.&~ lo ~"' :§£~~~~~! i \IS z 26 ..
''ii)(
1 ~f>ll
1.lG I)(;
)(!'}(
~)t1
l~IX
1-x11
~Ix
"f}(
'""1 ~ XI
ADDITIONAL COMlll!NTS ~~BYIAFFI~ DATE TIME I ACCEPTED~~~ DATE TillE
z ~ i~~~~j
Gi ::> 'C ~ Pace Fl'l'oiect NoJ Lab l.D.
I i
SAMPLE! i:<>NDITIONS
f)r..l\_O
R~
rV~
NO,
(1..liO
1'.r->
~\ .('rl
:~
~
~n
~/'r6/Jn5{) -Xfr;._-{';;..-.L_ --~ _°'(' 17-J..oet JS:Ot).I /¥1IA.n~ ""17h 709 V!5f)() 11',&I ~ U IQ
I v " ., . -.,. "-" I -11 I~
i
ORIGINAL
SAMPLER NAME AND SIGNATURE ~ t:: i o-
.5 "<>~ .5-
~ .~c ~1 ., !
--o {!, ~-j
PRINT Name of SAMPLER: -~,. F":5/)f~
SIGNATUREofSAMPLER~I ~;~ '7-1
"lmportanl Nobo: By signing !his fonn lJ'OU are -~ng Pace's NET JO day payment lorms and .,,_;ng to late charges of 1.5% pt; morrlh fat any lrwoic8S no1 paid will*I 30 days.
/-;?ceAnalytical·
www.patelalls.ca
CHAIN-OF-CUSTODY I Analytical Request Document
The Chain-of-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B SectionC Page: l of I
Required Client Information; Requintd PrOject lnformjltion: Invoice Information: 1242204 Company: <\+mr; I .. ~ report To:~~ /,Jt)., Jll.ll/ 'Attention:
Addre'l{.'-/ 81.A/J:.. ~Ji;,~ /lJ[,...3 feollyTo: ,-~ 7 ICornpanyName: ')-~ ~ IREGULATORYAGENCY I ~,Ni/-~10+ I rddress: ....... Ir NPDES r GROUNDWATER r ~':Kl~GWt._T::Jr-~.J\>..... .. __ D ~.,, J r _ Purchase Order No.: Pace Quc'.9 I UST r RCRA \.I' ~ ~ V'IW'Br (,!I c.XT~ _ _ Reference. • '/"'
Project Name: :::){/lier~ :;: ~IYt Site location Nt::. ProjectNumber: J '-JJ1 _ OC1 _ O Pacel'nllle#: STATE:
'II: ::e w !:
SectlonO
RoqulNd Client 111formation
SAMPLE ID
(A-Z, 0-9 / ,-)
Sample IDs MUST BE UNIQUE
Matrix Codes
l\tATRIX I COPE
Drinking Water OW
Water WT
Wastewater WW
Product p
Soi~Solid SL
Oil OL
Wipe WP
/'Jr AR
Tissue TS
Other OT
i ii:'
B 8 ~ "§ 8
:>! Cl)
l ;;? 1 (.!) II ~
lU c w 0 0..
(.) ~ x w ii'. .... 0.. !-l: <I: (1i ~
1 IS JL v-8eJt:I ~v.,;;k -tJ7 ~oj ~-~
2 SJLV -TWl ·-0 ry -O'l
3 I~ J L v -7"1 '"/ ·-o '7 .-o °i
4IS1LV -TW~ -t:i~ -oi.,,-
s 1.< tL\/ -Tl.JS--o/ -o<J
6 I 0 I •/) u 19: fr" 7.,;-tl~ -.
COLLECTED
COMPOSlTE
START
DATE I TIME
~
COMPOSllE I j:::: EN~ ~
~
0.. '::!! !:!
~ 0.. l:
DATE I TIME I (1i
'7 ..J-o'fi:..M: I , iuo
;0;15
JJ:1s
13!1:()
CJ) t:t:: lU :z ~ :z 8
LL 0
"" ~ L.
t.
&,;
11 ........
t..
Preservatives -z ):
Requested Analysis Fiitered (YIN)
i ~ ~ ~ !H ~ C\~~JP
:!2 "' &1 Pace Project NoJ Lab l.D.
m r I~~ I I I I 11 I I 111 '~t I
)(!XI I I I I I I I I I I I '--<Y
{] IYI I I I I I I I I I I q 1>
''Xl">G I I I I I I I I I I I I l.l 1
\.Yv ~
~
11 ~Jlv -Oc10Jtai+eA -o/-or::./ ~~~ I~ s 1 ~I LV --f'we:, -o') ·-o<!. )6:¥5
~
'
91 ~-JL V-Trro BMl<I -1>'7--~ 4l\ f I ~ -' 10
11
12
ADOmOHAL COMMENTS I ~IS!!WW AFFILIATIO~ DATE TIMe I ~D BY I AFFILIATION DATE I T1lillE SAMPLE CONDITIONS
1-*rn5Jm5D-Xfr-A. ~ ~ 17-J-o1 J-'S'OlJ I .A'---.~ 17,.(£..;.1 g~tJO I~. '7_ YI~}' l'WV1"° I \rW ~I""' ., _ · ~ -v,
.....,-I I I -
-~·-~ b ...,,1\ <.~""' t::;.;f.i\V' '" 0 C7" I .,.. -I
1 "'."An I\ ..J.-rf) 0. .. 0 , e::. SAMPLER NAME AND s•~ATURE c..> 5 _ ... a; ~
-k14 IAJ,,V {((JV ce ;e>ccJ&RIGINAL VL<? PRINTNameofSAMPLER: ·~ ~L .~~~ -~~
{.,,l..;. r-dEr·. ~/Jo-->.,../A.11cL" -DATE_S~l?-l'l. ;.}i\ -~1i:,,~-6ret .. 0 s_-_~i'_··u·· \..(...(,, t:eJ v . . '6 , . l -l vvvr l l.I\.. MM bm -u ; _!°'". "!. --~--. '.:> CJ): ! •;,1».li1NY;
·important ote: By signing this fonn you are acceplin; Pace's NET 30 day payment tomis __ O __ l:Q!~t · -.. , _ . . . _ ---__ • _ . _ ' _" :.:::."-. -., · ·"-' ~ •·
.,
f "•