19070_Polo_Fmr_Gussman_Env_Services_20150710

Environmental Services
ECS Carolinas, LLP
Wilmington, North Carolina 28405
910-686-9114

Report of
Gussman Cleaners, New Bern, Craven County, North Carolina

Prepared for
Mr. Charles Dees/ New Bern, NC
July 10, 2015
Gussman Cleaners
New Bern, Craven County, North Carolina
ECS Project No. 22:22171-A
July 10, 2015

TABLE OF CONTENTS

1. PROJECT INFORMATION ................................................................................................. 1
2. SCOPE OF SERVICES....................................................................................................... 2
3. RESULTS ............................................................................................................................ 3
4. SUMMARY, CONCLUSIONS, AND RECOMMENDATIONS .............................................. 3
5. QUALIFICATIONS OF REPORT ........................................................................................ 4

FIGURES
Figure 1 - Site Location Map
Figure 2 - Historical Map
Figure 3 - Sample Location Map

TABLES
Table 1 - Summary of Soil Analytical Results
Table 2 - Summary of Groundwater Analytical Results
Table 3 – Summary of Soil-Gas Analytical Results

APPENDIX
HASP Confirmation Sheet
Laboratory Data Sheets and Chain of Custody Record

Gussman Cleaners
New Bern, Craven County, North Carolina
ECS Project No. 22:22171-A
July 10, 2015

1

1. PROJECT INFORMATION

The site is located at 223 Craven Street in New Bern, Craven County, North Carolina (Figure 1).
ECS Carolinas, LLP (ECS) was provided with the Executive Summary of a Phase I Environmental
Site Assessment (ESA) prepared by Avolis Engineering, P.A. (Avolis). The Executive Summary
referenced the following key factors and observations which contributed to the recognized
environmental conditions (RECs).

 A dry cleaner operated on the property from 1956 through 2007 with dry-cleaning solvents
stored in aboveground storage tanks (ASTs) at the rear of the building.
 Automotive sales and service occurred on the northern adjoining property from 1931 through
1958.
 An automotive sales and machine shop operated on the southern adjoining property dating
back to 1958 and an underground storage tank (UST) containing gasoline was located on
this property, approximately 15 feet south of the site building from 1931 through 1948. A
copy of the historical Sanborn Map is included as Figure 2.

ECS performed a Phase II ESA on the site, dated February 10, 2015 (ECS Project Number 22-
22171). ECS performed soil, groundwater, and soil-gas sampling at two locations identified by Avolis
to assess the above-mentioned RECs.

 On January 22, 2015, ECS observed and documented the advancement of two soil and
groundwater borings and two sub-slab soil-gas borings at the site. The locations of these
borings are shown on Figure 3.
 Groundwater was encountered at an approximate depth of six to seven feet below the
ground surface (bgs).
 Benzo(a)anthracene and benzo(a)pyrene were detected in a soil sample located off-site and
downgradient (B-2), near the former UST, at concentrations exceeding their respective
industrial/commercial maximum soil contaminant concentrations (MSCCs). Concentrations
of targeted compounds were not detected in the soil sample located on-site near the AST (B-
1) at concentrations exceeding their respective MSCCs. The soil sample results are
summarized in Table 1.

 Laboratory analysis of a groundwater sample collected near the on-site AST (TW-1) detected
targeted volatile organic compounds (VOCs) and semi-volatile organic compounds
(SVOCs) at concentrations above laboratory detection limits. 1-methylnaphthalene was
detected at a concentration exceeding its North Carolina 2L Groundwater Quality Standards
(NC2LGWQS) but not its gross contamination level (GCL). Targeted compounds were not
detected above the laboratory detection limit in the groundwater sample collected near the
former UST downgradient of the site (TW-2). Groundwater sample results are summarized in
Table 2.

A copy of the Phase II ESA was submitted to the North Carolina Department of Environmental
and Natural Resources (NCDENR) as notification of a release. The NCDENR provided Mr.
Dees with a Notice of Regulatory Requirement (NORR) dated March 17, 2015 requesting a
Comprehensive Site Assessment (CSA) to assess the identified petroleum contamination. Due
to the possibility of off-site sources for the identified groundwater contamination, ECS submitted
an extension request dated April 9, 2015 requesting time to perform limited groundwater
Gussman Cleaners
New Bern, Craven County, North Carolina
ECS Project No. 22:22171-A
July 10, 2015

2

assessment to determine if the groundwater contamination appears to be migrating onto the site
from an off-site and upgradient source. The below scope of services and activities were performed
to assist in determining the potential source of the groundwater impact.

2. SCOPE OF SERVICES

The environmental assessment consisted of collecting three groundwater samples from
temporary GW borings located to the north and west of groundwater sample TW-1. These
locations were in a presumed upgradient direction based on the topographic map (Figure 1).
Geoprobe® equipment was used to collect the samples. The Geoprobe® consists of a hydraulic
jack mounted on an all-terrain vehicle (ATV). The Geoprobe® is capable of driving various forms
of groundwater, soil, and soil-gas sampling probes into the ground to depths equivalent of auger
refusal. The subcontractor used for this project was Mid Atlantic Drilling, Inc. (MAD). Field
activities were conducted on May 20, 2015.

Public Utility Clearance

Prior to commencing with field activities, ECS contacted North Carolina 811 to locate/mark
public utilities at the site. Required separation distances between subsurface activities and
marked utilities (typically 30-inches) were maintained during the field activities.

Health and Safety Plan

As part of this assessment, ECS prepared a site-specific health and safety plan (HASP) for the
site. The HASP documented the known or suspected hazards, applicable personal protective
equipment (PPE) of site personnel, and emergency response procedures. Prior to commencing
with field activities, ECS site personnel reviewed the site-specific HASP. A copy of the HASP
review confirmation sheet is included in the Appendix.

Geoprobe® Groundwater Borings

On May 20, 2015, ECS and MAD mobilized to the site to perform the sampling activities.
Groundwater boring TW-3 was installed on the southwestern corner of the site, boring TW-4
was installed north of boring TW-1, and boring TW-5 was installed on the northwestern corner
of the site. The groundwater borings were advanced by hydraulically driving a four-foot long,
1.5-inch diameter water-sampling probe into the soil to an approximate depth of thirteen feet
bgs. Groundwater was encountered at approximately eight feet bgs.

The groundwater sampling probe is equipped with a stainless steel screen and a disposable
drive point. The probe is driven to depth and then the rod is retracted to expose the screen.
Groundwater then flows through the screen into the hollow probe rods. The groundwater is
pumped to the surface using a peristaltic pump with dedicated plastic tubing lowered through
the center of the probe rods. Immediately after collection, the groundwater samples were
transferred into sample containers provided by the laboratory. Upon completion of sampling, each
boring was properly abandoned.

The groundwater samples were placed into laboratory prepared containers. The sample
containers were labeled with ECS project number, sample identification, sample date and time,
Gussman Cleaners
New Bern, Craven County, North Carolina
ECS Project No. 22:22171-A
July 10, 2015

3

and requested analytical analysis. The containers were placed into protective packaging
material and placed into a cooler with ice to maintain the samples at approximately 4 Celsius
(C). The groundwater samples were submitted to Pace for chemical analysis. The
groundwater samples were analyzed for VOCs using EPA Method 8260 and for semi-volatile
organic compounds (SVOCs) using EPA Method 8270. ECS maintained proper chain-of-
custody (COC) procedures throughout the sample collection and transportation process. A copy
of the COC is included in the Appendix.

3. RESULTS

Laboratory analysis detected targeted VOCs at concentrations above laboratory detection limits in
samples TW-3 through TW-5. However, 1-methylnaphthalene, which was detected in sample TW-
1 at a concentration exceeding its NC2LGWQS, was not detected in samples TW-3, TW-4, or TW-
5. Chlorobenzene was detected in sample TW-3 at a concentration exceeding its NC2LGWQS;
however, the concentration did not exceed its GCL. Chlorobenzene was also detected in sample
TW-4 and prior sample TW-1; however, the concentrations did not exceed its NC2LGWQS. A
summary of the groundwater sample analytical results is provided in Table 2. The laboratory
analytical data sheets and Chain of Custody Records are included in the Appendix.

On June 10, 2015, ECS discussed the site results with the NCDENR incident manager, Ms.
Sylvia Hunneke. Ms. Hunneke agreed with recommendations to install three permanent
groundwater monitoring wells on the site with one installed in the location of TW-1 and one in the
location of TW-3. Ms. Hunneke also agreed to a 90 day extension for completion of the CSA with
the due date of September 10, 2015.

4. SUMMARY, CONCLUSIONS, AND RECOMMENDATIONS

Upon completion of this, ECS summarizes and concludes the following:

 The on-site groundwater contains concentrations of chlorobenzene and 1-methylnapthalene
at concentrations that exceed the NC2LGWQS.
 The 1-methylnapthalene concentration was greatest adjacent to the AST used to formerly
store dry- cleaning petroleum solvents.
 The chlorobenzene concentration was greatest on the southwestern corner of the site, in a
presumed upgradient direction of the on-site AST.

Based on the results of the assessment, ECS recommends the following:

 ECS recommends installing three permanent groundwater wells on the site as part of the
CSA.

Gussman Cleaners
New Bern, Craven County, North Carolina
ECS Project No. 22:22171-A
July 10, 2015

4

5. QUALIFICATIONS OF REPORT

The activities and evaluative approaches used in this assessment are consistent with those
normally employed in environmental assessment projects of this type. Our evaluation of site
conditions has been based on our understanding of the site project information and the data
obtained during our field activities. This report was prepared for the express use of Avolis
Engineering. Use of this report by other individuals or companies implies their acceptance of the
General Conditions of Service of the original contract.

SOURCE:
UNITED STATES GEOLOGICAL
SURVEY 7.5-MINUTE SERIES
TOPOGRAPHIC MAP:
NEW BERN
NORTH CAROLINA,
DATED 1994
FIGURE 1
SITE LOCATION MAP
GUSSMAN CLEANERS
223 CRAVEN STREET
NEW BERN, CRAVEN COUNTY, NORTH CAROLINA
ECS PROJECT NO. 22-22171-A
SITE
SOURCE:
1948 SANBORN MAP
NC LIVE
SCALE SHOWN ABOVE
FIGURE 2
HISTORICAL MAP
GUSSMAN CLEANERS
223 CRAVEN STREET
NEW BERN, CRAVEN COUNTY, NORTH CAROLINA
ECS PROJECT NO. 22-22171-A
APPROXIMATE PROPERTY BOUNDARY
SOURCE:
GOOGLE EARTH 2014
SCALE SHOWN ABOVE
FIGURE 3
SAMPLE LOCATION MAP
GUSSMAN CLEANERS
223 CRAVEN STREET
NEW BERN, CRAVEN COUNTY, NORTH CAROLINA
ECS PROJECT NO. 22-22171-A
TW-1/ B-1
SG-1
B-1/TW-1
SG-1
APPROXIMATE PROPERTY BOUNDARY
SOIL-GAS SAMPLE LOCATION
SOIL/GROUNDWATER SAMPLE LOCATION
TW-2/ B-2
SG-2
TW-4TW-5
TW-3
Compound B-1 B-2
Analytical
Method
Soil to
Groundwater
MSCC (mg/kg)
Industrial/Commercial
MSCC (mg/kg)
Acetone 0.113 ND 8260 24 360,000
Benzo(a)anthracene ND 8.40 8270 0.35 8
Benzo(a)pyrene ND 8.65 8270 0.096 0.78
Benzo(b)fluoranthene ND 7.79 8270 1.2 8
Benzo(g,h,i)perylene ND 5.46 8270 6400 12,264
Benzo(k)fluoranthene ND 7.18 8270 12 78
Chrysene ND 8.95 8270 39 780
Fluoranthene ND 14.00 8270 290 16,400
Indeno(1,2,3-cd)pyrene ND 5.09 8270 3.4 8
Phenanthrene ND 5.45 8270 56 12,264
Pyrene ND 11.30 8270 270.0 12,264
1,2,4-Trimethylbenzene 0.019 ND 8260 9 20,440
Remainng VOCs ND ND 8260 Varies Varies
Remaining SVOCs ND ND 8270 Varies Varies
Notes:
Parameters reported in milligrams per liter (mg/kg)
MSCC = Maximum Soil Contaminant Concentration
ND = Not Detected,
Samples collected on January 22, 2015
Bold values represent concentrations above Industrial MSCC Standard
New Bern, Craven County, North Carolina
ECS Project Number 22-22171-A
Table 1
Summary of Soil Analytical Results
223 Craven Street
Gussman Cleaners
Co
m
p
o
u
n
d

T
W
-
1

T
W
-
2

T
W
-
3

T
W
-
4

T
W
-
5
An
a
l
y
t
i
c
a
l

Me
t
h
o
d
NC2LGWQS
Sa
m
p
l
e

D
a
t
e

1
/
2
2
/
1
5

1
/
2
2
/
1
5

5
/
2
0
/
1
5

5
/
2
0
/
1
5

5
/
2
0
/
1
5
se
c
-
B
u
t
y
l
b
e
n
z
e
n
e
ND

N
D

1
.
1

N
D

N
D

8
2
6
0
70
te
r
t
-
B
u
t
y
l
b
e
n
z
e
n
e
ND

N
D

1
2
.
2

N
D

1
.
3

8
2
6
0
70
Ch
l
o
r
o
b
e
n
z
e
n
e
10
.
1

N
D
13
1
1.
0

N
D

8
2
6
0

5
0
2-
C
h
l
o
r
o
t
o
l
u
e
n
e
ND

N
D

1
.
5

N
D

N
D

8
2
6
0

1
0
0
1,
2
-
D
i
c
h
l
o
r
o
b
e
n
z
e
n
e
ND

N
D

0
.
8
5

N
D

N
D

8
2
6
0

2
0
1,
3
-
D
i
c
h
l
o
r
o
b
e
n
z
e
n
e
8.
4

N
D

N
D

N
D

N
D

8
2
6
0

2
0
0
1,
4
-
D
i
c
h
l
o
r
o
b
e
n
z
e
n
e
1.
4

N
D

5
.
2

N
D

N
D

8
2
6
0

6
4-
M
e
t
h
y
l
-
2
-
p
e
n
t
a
n
o
n
e

(
M
I
B
K
)
28
.
7

N
D

N
D

N
D

N
D

8
2
6
0

1
0
0
o-
X
y
l
e
n
e
ND

N
D

1
.
4

N
D

N
D

8
2
6
0

5
0
0
1-
M
e
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e

1
5
.
2
ND

N
D

N
D

N
D

8
2
7
0

1
Re
m
a
i
n
i
n
g

V
O
C
s
ND

N
D

N
D

N
D

N
D

8
2
6
0

V
a
r
i
o
u
s
Re
m
a
i
n
i
n
g

S
V
O
C
s
ND

N
D

N
D

N
D

N
D

8
2
7
0

V
a
r
i
o
u
s
No
t
e
s
:

ND

=

N
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D
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Pa
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2
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Parameter ANALTYCIAL
RESULTS
ANALTYCIAL
RESULTS
Sample ID SG-1 SG-2
Collection Date 1/22/2015 1/22/2015
Acetone 34.0 30.1 2,720,000
Benzene 5.7 1.6 1,570
2-Butanone (MEK)14.1 9.0 438,000
Dichlorodifluoromethane (Freon 12)3.3 3.0 876
Ethyl acetate BRL 9.1 6,130
Ethylbenzene 3.4 BRL 4,910
4-Ethyltoluene 2.4 2.2 NS
n-Heptane 5.0 3.8 NS
n-Hexane 11.4 29.6 61,300
2-Hexanone 1.7 BRL 2,630
Methylene Chloride 7.0 33.7 52,600
Propylene 9.6 7.1 263,000
Tetrachloroethene 3.3 3.2 3,500
Tetrahydrofuran 10.9 BRL 175,000
Toluene 14.5 7.8 438,000
1,2,4-Trimethylbenzene 9.4 8.3 613
1,3,5-Trimethylbenzene 2.5 2.1 NS
total Xylenes 18.6 9.1 8,760
Notes:
Results presented in micrograms per cubic meter (ug/m3), analogous to parts per billion (ppb)
BRL = Compound not detected at a concentration above the method reporting limit
North Carolina Department of Environment and Natural Resources, Inactive Hazardous Sites Branch Standard
Compounds not listed were not detected above laboratory reporting limits
NS = No NCDENR IHSB Standard Available
NCDENR IHSB Non-
Residential Sub-Slab and
Exterior Soil-Gas
Screening Level (ug/m3)
Table 3
Summary of Soil-Gas Analytical Results
Gussman Cleaners
223 Craven Street
New Bern, Craven County, North Carolina
ECS Project Number 22-22171-A
HEALTH AND SAFETY PLAN

PROJECT NO: 22:22171-A
PROJECT NAME: Gussman Cleaners

SITE LOCATION: 223 Craven Street, New Bern, NC
CLIENT: Mr. Charles Dees

REVIEW AND APPROVAL

Principal: Brian Smith
Project Manager: Brooks Wall

DATE OF PLAN PREPARATION: 05-13-15
DATES OF PLANNED FIELD ACTIVITIES: 05-13156 through completion

PLANNED FIELD ACTIVITIES

Soil and groundwater investigation. Collection of samples, field screening, place into
laboratory-prepared containers.

SAFETY MEETING CONDUCTED

Location: Site

Date:

EMERGENCY PHONE NUMBERS

Hospital: Carolina East Medical Center
2000 Neuse Blvd, New Bern, NC 28560
Phone: 911 or 252-244-1785

Location for on-site emergency gathering will be determined during Site Safety
Meeting.
_________________________________________________________________
(Location of on-site emergency gathering)

Emergency Medical System (EMS): 911
Fire: 911
Police: 911

HEALTH AND SAFETY OFFICER: Darrell Henderson [phone]
ECS CONTACT: Brooks Wall [phone]
Health and Safety Plan
ECS Project No. 22:22171-A
Gussman Cleaners
New Bern, North Carolina
May 13, 2015

2
DESCRIPTION OF POTENTIAL HAZARDS

• Fire
• Exposure to petroleum/creosote through inhalation, skin absorption, or
ingestion.

PERSONNEL ACCESS

Personnel who attended ECS’s site safety meeting and are authorized to enter this
site:

1) ECS personnel
2) Mid Atlantic Drilling Personnel.

MONITORING PROCEDURES

Ambient air monitoring for the presence of volatile organic compounds will be performed
periodically with a photo-ionization detector (PID). Testing will be conducted for
approximately three minutes at a minimum of one test per hour or at other times when site
conditions (e.g. evidence of free product, increase in detectable odors, site workers
sensitivity) exhibit the need for additional testing. In such a case all site work will cease and
the site will be evacuated pending guidance from the Corporate Health and Safety Officer.

DECONTAMINATION (Petroleum products)

Skin - wash with soap and water
Clothing - wash with detergent and rinse thoroughly
Equipment - steam clean or detergent wash

MEDICAL SURVEILLANCE

Avoid frequent or prolonged skin contact. Monitor skin and eyes for dermatitis, allergic
reaction, and eye irritation. If these or other systems develop, seek qualified medical
attention. Workers with histories of liver, kidney, or nervous disorders should be advised as
to possible increased risk.

Symptoms of Acute Exposure to Volatile Organics: High vapor levels can cause irritation
of the respiratory tract, headaches, nausea, mental confusion, and loss of consciousness.
Liquid contact with skin may cause defatting, drying and irritation. Both vapor and liquid
phases are irritating to the eyes.
Health and Safety Plan
ECS Project No. 22:22171-A
Gussman Cleaners
New Bern, North Carolina
May 13, 2015

3

EMERGENCY PROCEDURES (Petroleum products)

Skin - wash with soap and water, rinse well
Inhalation - move to fresh air at least 50 feet upwind from vapor source. Seek
qualified medical attention.
Eyes - flush for a minimum of ten minutes with clean water while holding
eyes open. Seek qualified medical attention.
Ingestion - do not induce vomiting. If conscious, give water or milk to drink. Seek
qualified medical attention.

HEAT STRESS

Symptoms of heat stress include pale, cool or moist skin, excessive sweating, dizziness,
nausea, and muscle spasms. Symptoms of heat stroke include red, hot and unusually dry
skin, reduced perspiration, nausea, dizziness or confusion, rapid pulse rate and coma. To
prevent heat stress, adjust work schedule, provide shaded rest areas, and maintain body
fluids.

CLOTHING AND PROTECTIVE GEAR

Nitrile rubber gloves, steel-toed boots, protective eyewear, hard hats, and hearing
protection.

**The Project Manager or the Principal Professional should be contacted prior to changes
in personal protective equipment usage.

IN THE EVENT OF PERSONNEL INJURY

Provide basic first aid procedures as required, and note time and circumstances of injuries.
Call for an ambulance or transport to nearest medical facility. Notify Health and Safety
Officer and Principal Project Professional.

IN THE EVENT OF POTENTIAL OR ACTUAL FIRE OR EXPLOSION

Evacuate the area immediately. Assemble in the pre-designated area and conduct a head
count of all personnel. Notify fire department. DO NOT attempt to fight the fire. Notify
Project Manager.

ACCIDENT REPORTING
Health and Safety Plan
ECS Project No. 22:22171-A
Gussman Cleaners
New Bern, North Carolina
May 13, 2015

4

Personnel injuries and vehicle accidents should be reported to the Branch Safety Officer
within 24 hours of incident.

WORK PRECAUTIONS

1) No smoking, eating, drinking or chewing of gum or tobacco products while on
the site. Avoid hand to mouth contact. A designated smoking and break area
may be established off-site. Any such facility must be a minimum of 100 feet
from any source and shall be tested for flammable gasses and vapors at the
start of work and prior to scheduled break periods each day.

2) Hard hats, steel toe boots, and safety glasses are required to be worn at all
times within the site. Persons exposed to vehicular traffic will wear warning
vests.

3) When the potential exists for skin contact with liquid hydrocarbons,
impervious gloves and foot coverings are required to be worn.

4) Decontamination of equipment, clothing and personnel shall be in
accordance with the previous section entitled "Decontamination".

5) Prior to the start of work, any ECS employees or Subcontractor personnel
shall be briefed on the contents of this plan by the ECS Field Representative.

FIELD REPRESENTATIVE SUMMARY

During the work covered by this Safety Plan, there were:

__No observed violations of the Safety Plan provisions.

__The following violations of the Safety Plan provisions (give details in space below and
indicate corrective action taken for each violation noted).

Signature:
Field Representative Date
Health and Safety Plan
ECS Project No. 22:22171-A
Gussman Cleaners
New Bern, North Carolina
May 13, 2015

5
ON-SITE HEALTH AND SAFTEY MEETING

Location:
______________________________________________________________________
______________________________________________________________________

Attendees:

Printed Name Signature Company Date

#=CL#
June 01, 2015
LIMS USE: FR - AMY CONCHAS
LIMS OBJECT ID: 92250854
92250854
Project:
Pace Project No.:
RE:
Amy Conchas
ECS
6714 Netherlands Drive
Wilmington, NC 28405
GUSSMAN CLEANERS
Dear Amy Conchas:
Enclosed are the analytical results for sample(s) received by the laboratory on May 21, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
Enclosures
cc:Ms. Amy Conchas, ECS
Brooks Wall, ECS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
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Page 1 of 30
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
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Page 2 of 30
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92250854001 TW-3 EPA 625 58 PASI-CBPJ
SM 6200B 63 PASI-CCAH
92250854002 TW-4 EPA 625 58 PASI-CBPJ
SM 6200B 63 PASI-CCAH
92250854003 TW-5 EPA 625 58 PASI-CBPJ
SM 6200B 63 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
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Page 3 of 30
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92250854001 TW-3
sec-Butylbenzene 1.1 ug/L 05/29/15 16:530.50SM 6200B
tert-Butylbenzene 12.2 ug/L 05/29/15 16:530.50SM 6200B
Chlorobenzene 131 ug/L 05/29/15 16:530.50SM 6200B
2-Chlorotoluene 1.5 ug/L 05/29/15 16:530.50SM 6200B
1,2-Dichlorobenzene 0.85 ug/L 05/29/15 16:530.50SM 6200B
1,4-Dichlorobenzene 5.2 ug/L 05/29/15 16:530.50SM 6200B
o-Xylene 1.4 ug/L 05/29/15 16:530.50SM 6200B
92250854002 TW-4
Chlorobenzene 1.0 ug/L 05/29/15 01:250.50SM 6200B
92250854003 TW-5
tert-Butylbenzene 1.3 ug/L 05/29/15 01:410.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Page 4 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Sample:TW-3 Lab ID:92250854001 Collected:05/20/15 11:00 Received:05/21/15 10:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Acenaphthene ND ug/L 05/29/15 23:00 83-32-905/26/15 18:305.0 1
Acenaphthylene ND ug/L 05/29/15 23:00 208-96-805/26/15 18:305.0 1
Anthracene ND ug/L 05/29/15 23:00 120-12-705/26/15 18:305.0 1
Benzo(a)anthracene ND ug/L 05/29/15 23:00 56-55-305/26/15 18:305.0 1
Benzo(a)pyrene ND ug/L 05/29/15 23:00 50-32-805/26/15 18:305.0 1
Benzo(b)fluoranthene ND ug/L 05/29/15 23:00 205-99-205/26/15 18:305.0 1
Benzo(g,h,i)perylene ND ug/L 05/29/15 23:00 191-24-205/26/15 18:305.0 1
Benzo(k)fluoranthene ND ug/L 05/29/15 23:00 207-08-905/26/15 18:305.0 1
4-Bromophenylphenyl ether ND ug/L 05/29/15 23:00 101-55-305/26/15 18:305.0 1
Butylbenzylphthalate ND ug/L 05/29/15 23:00 85-68-705/26/15 18:305.0 1
4-Chloro-3-methylphenol ND ug/L 05/29/15 23:00 59-50-705/26/15 18:305.0 1
bis(2-Chloroethoxy)methane ND ug/L 05/29/15 23:00 111-91-105/26/15 18:3010.0 1
bis(2-Chloroethyl) ether ND ug/L 05/29/15 23:00 111-44-405/26/15 18:305.0 1
bis(2-Chloroisopropyl) ether ND ug/L 05/29/15 23:00 108-60-105/26/15 18:305.0 1
2-Chloronaphthalene ND ug/L 05/29/15 23:00 91-58-7 L205/26/15 18:305.0 1
2-Chlorophenol ND ug/L 05/29/15 23:00 95-57-805/26/15 18:305.0 1
4-Chlorophenylphenyl ether ND ug/L 05/29/15 23:00 7005-72-305/26/15 18:305.0 1
Chrysene ND ug/L 05/29/15 23:00 218-01-905/26/15 18:305.0 1
Dibenz(a,h)anthracene ND ug/L 05/29/15 23:00 53-70-305/26/15 18:305.0 1
3,3'-Dichlorobenzidine ND ug/L 05/29/15 23:00 91-94-105/26/15 18:3025.0 1
2,4-Dichlorophenol ND ug/L 05/29/15 23:00 120-83-205/26/15 18:305.0 1
Diethylphthalate ND ug/L 05/29/15 23:00 84-66-205/26/15 18:305.0 1
2,4-Dimethylphenol ND ug/L 05/29/15 23:00 105-67-905/26/15 18:3010.0 1
Dimethylphthalate ND ug/L 05/29/15 23:00 131-11-305/26/15 18:305.0 1
Di-n-butylphthalate ND ug/L 05/29/15 23:00 84-74-205/26/15 18:305.0 1
4,6-Dinitro-2-methylphenol ND ug/L 05/29/15 23:00 534-52-105/26/15 18:3020.0 1
2,4-Dinitrophenol ND ug/L 05/29/15 23:00 51-28-505/26/15 18:3050.0 1
2,4-Dinitrotoluene ND ug/L 05/29/15 23:00 121-14-205/26/15 18:305.0 1
2,6-Dinitrotoluene ND ug/L 05/29/15 23:00 606-20-205/26/15 18:305.0 1
Di-n-octylphthalate ND ug/L 05/29/15 23:00 117-84-005/26/15 18:305.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 05/29/15 23:00 117-81-705/26/15 18:305.0 1
Fluoranthene ND ug/L 05/29/15 23:00 206-44-005/26/15 18:305.0 1
Fluorene ND ug/L 05/29/15 23:00 86-73-705/26/15 18:305.0 1
Hexachloro-1,3-butadiene ND ug/L 05/29/15 23:00 87-68-305/26/15 18:305.0 1
Hexachlorobenzene ND ug/L 05/29/15 23:00 118-74-105/26/15 18:305.0 1
Hexachlorocyclopentadiene ND ug/L 05/29/15 23:00 77-47-405/26/15 18:3010.0 1
Hexachloroethane ND ug/L 05/29/15 23:00 67-72-105/26/15 18:305.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 05/29/15 23:00 193-39-505/26/15 18:305.0 1
Isophorone ND ug/L 05/29/15 23:00 78-59-105/26/15 18:3010.0 1
Naphthalene ND ug/L 05/29/15 23:00 91-20-305/26/15 18:305.0 1
Nitrobenzene ND ug/L 05/29/15 23:00 98-95-305/26/15 18:305.0 1
2-Nitrophenol ND ug/L 05/29/15 23:00 88-75-505/26/15 18:305.0 1
4-Nitrophenol ND ug/L 05/29/15 23:00 100-02-705/26/15 18:3050.0 1
N-Nitrosodimethylamine ND ug/L 05/29/15 23:00 62-75-905/26/15 18:305.0 1
N-Nitroso-di-n-propylamine ND ug/L 05/29/15 23:00 621-64-705/26/15 18:305.0 1
N-Nitrosodiphenylamine ND ug/L 05/29/15 23:00 86-30-605/26/15 18:3010.0 1
Pentachlorophenol ND ug/L 05/29/15 23:00 87-86-505/26/15 18:3010.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
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Page 5 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Sample:TW-3 Lab ID:92250854001 Collected:05/20/15 11:00 Received:05/21/15 10:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Phenanthrene ND ug/L 05/29/15 23:00 85-01-805/26/15 18:305.0 1
Phenol ND ug/L 05/29/15 23:00 108-95-205/26/15 18:305.0 1
Pyrene ND ug/L 05/29/15 23:00 129-00-005/26/15 18:305.0 1
1,2,4-Trichlorobenzene ND ug/L 05/29/15 23:00 120-82-105/26/15 18:305.0 1
2,4,6-Trichlorophenol ND ug/L 05/29/15 23:00 88-06-205/26/15 18:3010.0 1
Surrogates
Nitrobenzene-d5 (S)78 %05/29/15 23:00 4165-60-005/26/15 18:3010-120 1
2-Fluorobiphenyl (S)66 %05/29/15 23:00 321-60-805/26/15 18:3015-120 1
Terphenyl-d14 (S)104 %05/29/15 23:00 1718-51-005/26/15 18:3011-131 1
Phenol-d6 (S)29 %05/29/15 23:00 13127-88-305/26/15 18:3010-120 1
2-Fluorophenol (S)42 %05/29/15 23:00 367-12-405/26/15 18:3010-120 1
2,4,6-Tribromophenol (S)88 %05/29/15 23:00 118-79-605/26/15 18:3010-137 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 05/29/15 16:53 71-43-20.50 1
Bromobenzene ND ug/L 05/29/15 16:53 108-86-10.50 1
Bromochloromethane ND ug/L 05/29/15 16:53 74-97-50.50 1
Bromodichloromethane ND ug/L 05/29/15 16:53 75-27-40.50 1
Bromoform ND ug/L 05/29/15 16:53 75-25-20.50 1
Bromomethane ND ug/L 05/29/15 16:53 74-83-95.0 1
n-Butylbenzene ND ug/L 05/29/15 16:53 104-51-80.50 1
sec-Butylbenzene 1.1 ug/L 05/29/15 16:53 135-98-80.50 1
tert-Butylbenzene 12.2 ug/L 05/29/15 16:53 98-06-60.50 1
Carbon tetrachloride ND ug/L 05/29/15 16:53 56-23-50.50 1
Chlorobenzene 131 ug/L 05/29/15 16:53 108-90-70.50 1
Chloroethane ND ug/L 05/29/15 16:53 75-00-31.0 1
Chloroform ND ug/L 05/29/15 16:53 67-66-30.50 1
Chloromethane ND ug/L 05/29/15 16:53 74-87-31.0 1
2-Chlorotoluene 1.5 ug/L 05/29/15 16:53 95-49-80.50 1
4-Chlorotoluene ND ug/L 05/29/15 16:53 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 05/29/15 16:53 96-12-81.0 1
Dibromochloromethane ND ug/L 05/29/15 16:53 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 05/29/15 16:53 106-93-40.50 1
Dibromomethane ND ug/L 05/29/15 16:53 74-95-30.50 1
1,2-Dichlorobenzene 0.85 ug/L 05/29/15 16:53 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 05/29/15 16:53 541-73-10.50 1
1,4-Dichlorobenzene 5.2 ug/L 05/29/15 16:53 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 05/29/15 16:53 75-71-80.50 1
1,1-Dichloroethane ND ug/L 05/29/15 16:53 75-34-30.50 1
1,2-Dichloroethane ND ug/L 05/29/15 16:53 107-06-20.50 1
1,1-Dichloroethene ND ug/L 05/29/15 16:53 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 05/29/15 16:53 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 05/29/15 16:53 156-60-50.50 1
1,2-Dichloropropane ND ug/L 05/29/15 16:53 78-87-50.50 1
1,3-Dichloropropane ND ug/L 05/29/15 16:53 142-28-90.50 1
2,2-Dichloropropane ND ug/L 05/29/15 16:53 594-20-70.50 1
1,1-Dichloropropene ND ug/L 05/29/15 16:53 563-58-60.50 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
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Page 6 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Sample:TW-3 Lab ID:92250854001 Collected:05/20/15 11:00 Received:05/21/15 10:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
cis-1,3-Dichloropropene ND ug/L 05/29/15 16:53 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 05/29/15 16:53 10061-02-60.50 1
Diisopropyl ether ND ug/L 05/29/15 16:53 108-20-30.50 1
Ethylbenzene ND ug/L 05/29/15 16:53 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 05/29/15 16:53 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 05/29/15 16:53 98-82-80.50 1
Methylene Chloride ND ug/L 05/29/15 16:53 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 05/29/15 16:53 1634-04-40.50 1
Naphthalene ND ug/L 05/29/15 16:53 91-20-32.0 1
n-Propylbenzene ND ug/L 05/29/15 16:53 103-65-10.50 1
Styrene ND ug/L 05/29/15 16:53 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 05/29/15 16:53 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 05/29/15 16:53 79-34-50.50 1
Tetrachloroethene ND ug/L 05/29/15 16:53 127-18-40.50 1
Toluene ND ug/L 05/29/15 16:53 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 05/29/15 16:53 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 05/29/15 16:53 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 05/29/15 16:53 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 05/29/15 16:53 79-00-50.50 1
Trichloroethene ND ug/L 05/29/15 16:53 79-01-60.50 1
Trichlorofluoromethane ND ug/L 05/29/15 16:53 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/29/15 16:53 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 05/29/15 16:53 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 05/29/15 16:53 108-67-80.50 1
Vinyl chloride ND ug/L 05/29/15 16:53 75-01-41.0 1
m&p-Xylene ND ug/L 05/29/15 16:53 179601-23-11.0 1
o-Xylene 1.4 ug/L 05/29/15 16:53 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %05/29/15 16:53 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %05/29/15 16:53 460-00-470-130 1
Toluene-d8 (S)99 %05/29/15 16:53 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 7 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Sample:TW-4 Lab ID:92250854002 Collected:05/20/15 12:00 Received:05/21/15 10:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Acenaphthene ND ug/L 05/29/15 23:28 83-32-905/26/15 18:305.0 1
Acenaphthylene ND ug/L 05/29/15 23:28 208-96-805/26/15 18:305.0 1
Anthracene ND ug/L 05/29/15 23:28 120-12-705/26/15 18:305.0 1
Benzo(a)anthracene ND ug/L 05/29/15 23:28 56-55-305/26/15 18:305.0 1
Benzo(a)pyrene ND ug/L 05/29/15 23:28 50-32-805/26/15 18:305.0 1
Benzo(b)fluoranthene ND ug/L 05/29/15 23:28 205-99-205/26/15 18:305.0 1
Benzo(g,h,i)perylene ND ug/L 05/29/15 23:28 191-24-205/26/15 18:305.0 1
Benzo(k)fluoranthene ND ug/L 05/29/15 23:28 207-08-905/26/15 18:305.0 1
4-Bromophenylphenyl ether ND ug/L 05/29/15 23:28 101-55-305/26/15 18:305.0 1
Butylbenzylphthalate ND ug/L 05/29/15 23:28 85-68-705/26/15 18:305.0 1
4-Chloro-3-methylphenol ND ug/L 05/29/15 23:28 59-50-705/26/15 18:305.0 1
bis(2-Chloroethoxy)methane ND ug/L 05/29/15 23:28 111-91-105/26/15 18:3010.0 1
bis(2-Chloroethyl) ether ND ug/L 05/29/15 23:28 111-44-405/26/15 18:305.0 1
bis(2-Chloroisopropyl) ether ND ug/L 05/29/15 23:28 108-60-105/26/15 18:305.0 1
2-Chloronaphthalene ND ug/L 05/29/15 23:28 91-58-7 L205/26/15 18:305.0 1
2-Chlorophenol ND ug/L 05/29/15 23:28 95-57-805/26/15 18:305.0 1
4-Chlorophenylphenyl ether ND ug/L 05/29/15 23:28 7005-72-305/26/15 18:305.0 1
Chrysene ND ug/L 05/29/15 23:28 218-01-905/26/15 18:305.0 1
Dibenz(a,h)anthracene ND ug/L 05/29/15 23:28 53-70-305/26/15 18:305.0 1
3,3'-Dichlorobenzidine ND ug/L 05/29/15 23:28 91-94-105/26/15 18:3025.0 1
2,4-Dichlorophenol ND ug/L 05/29/15 23:28 120-83-205/26/15 18:305.0 1
Diethylphthalate ND ug/L 05/29/15 23:28 84-66-205/26/15 18:305.0 1
2,4-Dimethylphenol ND ug/L 05/29/15 23:28 105-67-905/26/15 18:3010.0 1
Dimethylphthalate ND ug/L 05/29/15 23:28 131-11-305/26/15 18:305.0 1
Di-n-butylphthalate ND ug/L 05/29/15 23:28 84-74-205/26/15 18:305.0 1
4,6-Dinitro-2-methylphenol ND ug/L 05/29/15 23:28 534-52-105/26/15 18:3020.0 1
2,4-Dinitrophenol ND ug/L 05/29/15 23:28 51-28-505/26/15 18:3050.0 1
2,4-Dinitrotoluene ND ug/L 05/29/15 23:28 121-14-205/26/15 18:305.0 1
2,6-Dinitrotoluene ND ug/L 05/29/15 23:28 606-20-205/26/15 18:305.0 1
Di-n-octylphthalate ND ug/L 05/29/15 23:28 117-84-005/26/15 18:305.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 05/29/15 23:28 117-81-705/26/15 18:305.0 1
Fluoranthene ND ug/L 05/29/15 23:28 206-44-005/26/15 18:305.0 1
Fluorene ND ug/L 05/29/15 23:28 86-73-705/26/15 18:305.0 1
Hexachloro-1,3-butadiene ND ug/L 05/29/15 23:28 87-68-305/26/15 18:305.0 1
Hexachlorobenzene ND ug/L 05/29/15 23:28 118-74-105/26/15 18:305.0 1
Hexachlorocyclopentadiene ND ug/L 05/29/15 23:28 77-47-405/26/15 18:3010.0 1
Hexachloroethane ND ug/L 05/29/15 23:28 67-72-105/26/15 18:305.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 05/29/15 23:28 193-39-505/26/15 18:305.0 1
Isophorone ND ug/L 05/29/15 23:28 78-59-105/26/15 18:3010.0 1
Naphthalene ND ug/L 05/29/15 23:28 91-20-305/26/15 18:305.0 1
Nitrobenzene ND ug/L 05/29/15 23:28 98-95-305/26/15 18:305.0 1
2-Nitrophenol ND ug/L 05/29/15 23:28 88-75-505/26/15 18:305.0 1
4-Nitrophenol ND ug/L 05/29/15 23:28 100-02-705/26/15 18:3050.0 1
N-Nitrosodimethylamine ND ug/L 05/29/15 23:28 62-75-905/26/15 18:305.0 1
N-Nitroso-di-n-propylamine ND ug/L 05/29/15 23:28 621-64-705/26/15 18:305.0 1
N-Nitrosodiphenylamine ND ug/L 05/29/15 23:28 86-30-605/26/15 18:3010.0 1
Pentachlorophenol ND ug/L 05/29/15 23:28 87-86-505/26/15 18:3010.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Sample:TW-4 Lab ID:92250854002 Collected:05/20/15 12:00 Received:05/21/15 10:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Phenanthrene ND ug/L 05/29/15 23:28 85-01-805/26/15 18:305.0 1
Phenol ND ug/L 05/29/15 23:28 108-95-205/26/15 18:305.0 1
Pyrene ND ug/L 05/29/15 23:28 129-00-005/26/15 18:305.0 1
1,2,4-Trichlorobenzene ND ug/L 05/29/15 23:28 120-82-105/26/15 18:305.0 1
2,4,6-Trichlorophenol ND ug/L 05/29/15 23:28 88-06-205/26/15 18:3010.0 1
Surrogates
Nitrobenzene-d5 (S)40 %05/29/15 23:28 4165-60-005/26/15 18:3010-120 1
2-Fluorobiphenyl (S)32 %05/29/15 23:28 321-60-805/26/15 18:3015-120 1
Terphenyl-d14 (S)57 %05/29/15 23:28 1718-51-005/26/15 18:3011-131 1
Phenol-d6 (S)13 %05/29/15 23:28 13127-88-305/26/15 18:3010-120 1
2-Fluorophenol (S)20 %05/29/15 23:28 367-12-405/26/15 18:3010-120 1
2,4,6-Tribromophenol (S)47 %05/29/15 23:28 118-79-605/26/15 18:3010-137 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 05/29/15 01:25 71-43-20.50 1
Bromobenzene ND ug/L 05/29/15 01:25 108-86-10.50 1
Bromochloromethane ND ug/L 05/29/15 01:25 74-97-50.50 1
Bromodichloromethane ND ug/L 05/29/15 01:25 75-27-40.50 1
Bromoform ND ug/L 05/29/15 01:25 75-25-20.50 1
Bromomethane ND ug/L 05/29/15 01:25 74-83-95.0 1
n-Butylbenzene ND ug/L 05/29/15 01:25 104-51-80.50 1
sec-Butylbenzene ND ug/L 05/29/15 01:25 135-98-80.50 1
tert-Butylbenzene ND ug/L 05/29/15 01:25 98-06-60.50 1
Carbon tetrachloride ND ug/L 05/29/15 01:25 56-23-50.50 1
Chlorobenzene 1.0 ug/L 05/29/15 01:25 108-90-70.50 1
Chloroethane ND ug/L 05/29/15 01:25 75-00-31.0 1
Chloroform ND ug/L 05/29/15 01:25 67-66-30.50 1
Chloromethane ND ug/L 05/29/15 01:25 74-87-31.0 1
2-Chlorotoluene ND ug/L 05/29/15 01:25 95-49-80.50 1
4-Chlorotoluene ND ug/L 05/29/15 01:25 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 05/29/15 01:25 96-12-81.0 1
Dibromochloromethane ND ug/L 05/29/15 01:25 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 05/29/15 01:25 106-93-40.50 1
Dibromomethane ND ug/L 05/29/15 01:25 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 05/29/15 01:25 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 05/29/15 01:25 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 05/29/15 01:25 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 05/29/15 01:25 75-71-8 L30.50 1
1,1-Dichloroethane ND ug/L 05/29/15 01:25 75-34-30.50 1
1,2-Dichloroethane ND ug/L 05/29/15 01:25 107-06-20.50 1
1,1-Dichloroethene ND ug/L 05/29/15 01:25 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 05/29/15 01:25 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 05/29/15 01:25 156-60-50.50 1
1,2-Dichloropropane ND ug/L 05/29/15 01:25 78-87-50.50 1
1,3-Dichloropropane ND ug/L 05/29/15 01:25 142-28-90.50 1
2,2-Dichloropropane ND ug/L 05/29/15 01:25 594-20-70.50 1
1,1-Dichloropropene ND ug/L 05/29/15 01:25 563-58-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 9 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Sample:TW-4 Lab ID:92250854002 Collected:05/20/15 12:00 Received:05/21/15 10:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
cis-1,3-Dichloropropene ND ug/L 05/29/15 01:25 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 05/29/15 01:25 10061-02-60.50 1
Diisopropyl ether ND ug/L 05/29/15 01:25 108-20-30.50 1
Ethylbenzene ND ug/L 05/29/15 01:25 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 05/29/15 01:25 87-68-3 L32.0 1
Isopropylbenzene (Cumene)ND ug/L 05/29/15 01:25 98-82-80.50 1
Methylene Chloride ND ug/L 05/29/15 01:25 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 05/29/15 01:25 1634-04-40.50 1
Naphthalene ND ug/L 05/29/15 01:25 91-20-32.0 1
n-Propylbenzene ND ug/L 05/29/15 01:25 103-65-10.50 1
Styrene ND ug/L 05/29/15 01:25 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 05/29/15 01:25 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 05/29/15 01:25 79-34-50.50 1
Tetrachloroethene ND ug/L 05/29/15 01:25 127-18-40.50 1
Toluene ND ug/L 05/29/15 01:25 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 05/29/15 01:25 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 05/29/15 01:25 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 05/29/15 01:25 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 05/29/15 01:25 79-00-50.50 1
Trichloroethene ND ug/L 05/29/15 01:25 79-01-60.50 1
Trichlorofluoromethane ND ug/L 05/29/15 01:25 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/29/15 01:25 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 05/29/15 01:25 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 05/29/15 01:25 108-67-80.50 1
Vinyl chloride ND ug/L 05/29/15 01:25 75-01-41.0 1
m&p-Xylene ND ug/L 05/29/15 01:25 179601-23-11.0 1
o-Xylene ND ug/L 05/29/15 01:25 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %05/29/15 01:25 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %05/29/15 01:25 460-00-470-130 1
Toluene-d8 (S)99 %05/29/15 01:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
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Page 10 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Sample:TW-5 Lab ID:92250854003 Collected:05/20/15 13:00 Received:05/21/15 10:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Acenaphthene ND ug/L 05/29/15 23:56 83-32-905/26/15 18:305.0 1
Acenaphthylene ND ug/L 05/29/15 23:56 208-96-805/26/15 18:305.0 1
Anthracene ND ug/L 05/29/15 23:56 120-12-705/26/15 18:305.0 1
Benzo(a)anthracene ND ug/L 05/29/15 23:56 56-55-305/26/15 18:305.0 1
Benzo(a)pyrene ND ug/L 05/29/15 23:56 50-32-805/26/15 18:305.0 1
Benzo(b)fluoranthene ND ug/L 05/29/15 23:56 205-99-205/26/15 18:305.0 1
Benzo(g,h,i)perylene ND ug/L 05/29/15 23:56 191-24-205/26/15 18:305.0 1
Benzo(k)fluoranthene ND ug/L 05/29/15 23:56 207-08-905/26/15 18:305.0 1
4-Bromophenylphenyl ether ND ug/L 05/29/15 23:56 101-55-305/26/15 18:305.0 1
Butylbenzylphthalate ND ug/L 05/29/15 23:56 85-68-705/26/15 18:305.0 1
4-Chloro-3-methylphenol ND ug/L 05/29/15 23:56 59-50-705/26/15 18:305.0 1
bis(2-Chloroethoxy)methane ND ug/L 05/29/15 23:56 111-91-105/26/15 18:3010.0 1
bis(2-Chloroethyl) ether ND ug/L 05/29/15 23:56 111-44-405/26/15 18:305.0 1
bis(2-Chloroisopropyl) ether ND ug/L 05/29/15 23:56 108-60-105/26/15 18:305.0 1
2-Chloronaphthalene ND ug/L 05/29/15 23:56 91-58-7 L205/26/15 18:305.0 1
2-Chlorophenol ND ug/L 05/29/15 23:56 95-57-805/26/15 18:305.0 1
4-Chlorophenylphenyl ether ND ug/L 05/29/15 23:56 7005-72-305/26/15 18:305.0 1
Chrysene ND ug/L 05/29/15 23:56 218-01-905/26/15 18:305.0 1
Dibenz(a,h)anthracene ND ug/L 05/29/15 23:56 53-70-305/26/15 18:305.0 1
3,3'-Dichlorobenzidine ND ug/L 05/29/15 23:56 91-94-105/26/15 18:3025.0 1
2,4-Dichlorophenol ND ug/L 05/29/15 23:56 120-83-205/26/15 18:305.0 1
Diethylphthalate ND ug/L 05/29/15 23:56 84-66-205/26/15 18:305.0 1
2,4-Dimethylphenol ND ug/L 05/29/15 23:56 105-67-905/26/15 18:3010.0 1
Dimethylphthalate ND ug/L 05/29/15 23:56 131-11-305/26/15 18:305.0 1
Di-n-butylphthalate ND ug/L 05/29/15 23:56 84-74-205/26/15 18:305.0 1
4,6-Dinitro-2-methylphenol ND ug/L 05/29/15 23:56 534-52-105/26/15 18:3020.0 1
2,4-Dinitrophenol ND ug/L 05/29/15 23:56 51-28-505/26/15 18:3050.0 1
2,4-Dinitrotoluene ND ug/L 05/29/15 23:56 121-14-205/26/15 18:305.0 1
2,6-Dinitrotoluene ND ug/L 05/29/15 23:56 606-20-205/26/15 18:305.0 1
Di-n-octylphthalate ND ug/L 05/29/15 23:56 117-84-005/26/15 18:305.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 05/29/15 23:56 117-81-705/26/15 18:305.0 1
Fluoranthene ND ug/L 05/29/15 23:56 206-44-005/26/15 18:305.0 1
Fluorene ND ug/L 05/29/15 23:56 86-73-705/26/15 18:305.0 1
Hexachloro-1,3-butadiene ND ug/L 05/29/15 23:56 87-68-305/26/15 18:305.0 1
Hexachlorobenzene ND ug/L 05/29/15 23:56 118-74-105/26/15 18:305.0 1
Hexachlorocyclopentadiene ND ug/L 05/29/15 23:56 77-47-405/26/15 18:3010.0 1
Hexachloroethane ND ug/L 05/29/15 23:56 67-72-105/26/15 18:305.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 05/29/15 23:56 193-39-505/26/15 18:305.0 1
Isophorone ND ug/L 05/29/15 23:56 78-59-105/26/15 18:3010.0 1
Naphthalene ND ug/L 05/29/15 23:56 91-20-305/26/15 18:305.0 1
Nitrobenzene ND ug/L 05/29/15 23:56 98-95-305/26/15 18:305.0 1
2-Nitrophenol ND ug/L 05/29/15 23:56 88-75-505/26/15 18:305.0 1
4-Nitrophenol ND ug/L 05/29/15 23:56 100-02-705/26/15 18:3050.0 1
N-Nitrosodimethylamine ND ug/L 05/29/15 23:56 62-75-905/26/15 18:305.0 1
N-Nitroso-di-n-propylamine ND ug/L 05/29/15 23:56 621-64-705/26/15 18:305.0 1
N-Nitrosodiphenylamine ND ug/L 05/29/15 23:56 86-30-605/26/15 18:3010.0 1
Pentachlorophenol ND ug/L 05/29/15 23:56 87-86-505/26/15 18:3010.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Sample:TW-5 Lab ID:92250854003 Collected:05/20/15 13:00 Received:05/21/15 10:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Phenanthrene ND ug/L 05/29/15 23:56 85-01-805/26/15 18:305.0 1
Phenol ND ug/L 05/29/15 23:56 108-95-205/26/15 18:305.0 1
Pyrene ND ug/L 05/29/15 23:56 129-00-005/26/15 18:305.0 1
1,2,4-Trichlorobenzene ND ug/L 05/29/15 23:56 120-82-105/26/15 18:305.0 1
2,4,6-Trichlorophenol ND ug/L 05/29/15 23:56 88-06-205/26/15 18:3010.0 1
Surrogates
Nitrobenzene-d5 (S)94 %05/29/15 23:56 4165-60-005/26/15 18:3010-120 1
2-Fluorobiphenyl (S)78 %05/29/15 23:56 321-60-805/26/15 18:3015-120 1
Terphenyl-d14 (S)111 %05/29/15 23:56 1718-51-005/26/15 18:3011-131 1
Phenol-d6 (S)35 %05/29/15 23:56 13127-88-305/26/15 18:3010-120 1
2-Fluorophenol (S)51 %05/29/15 23:56 367-12-405/26/15 18:3010-120 1
2,4,6-Tribromophenol (S)92 %05/29/15 23:56 118-79-605/26/15 18:3010-137 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 05/29/15 01:41 71-43-20.50 1
Bromobenzene ND ug/L 05/29/15 01:41 108-86-10.50 1
Bromochloromethane ND ug/L 05/29/15 01:41 74-97-50.50 1
Bromodichloromethane ND ug/L 05/29/15 01:41 75-27-40.50 1
Bromoform ND ug/L 05/29/15 01:41 75-25-20.50 1
Bromomethane ND ug/L 05/29/15 01:41 74-83-95.0 1
n-Butylbenzene ND ug/L 05/29/15 01:41 104-51-80.50 1
sec-Butylbenzene ND ug/L 05/29/15 01:41 135-98-80.50 1
tert-Butylbenzene 1.3 ug/L 05/29/15 01:41 98-06-60.50 1
Carbon tetrachloride ND ug/L 05/29/15 01:41 56-23-50.50 1
Chlorobenzene ND ug/L 05/29/15 01:41 108-90-70.50 1
Chloroethane ND ug/L 05/29/15 01:41 75-00-31.0 1
Chloroform ND ug/L 05/29/15 01:41 67-66-30.50 1
Chloromethane ND ug/L 05/29/15 01:41 74-87-31.0 1
2-Chlorotoluene ND ug/L 05/29/15 01:41 95-49-80.50 1
4-Chlorotoluene ND ug/L 05/29/15 01:41 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 05/29/15 01:41 96-12-81.0 1
Dibromochloromethane ND ug/L 05/29/15 01:41 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 05/29/15 01:41 106-93-40.50 1
Dibromomethane ND ug/L 05/29/15 01:41 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 05/29/15 01:41 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 05/29/15 01:41 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 05/29/15 01:41 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 05/29/15 01:41 75-71-8 L30.50 1
1,1-Dichloroethane ND ug/L 05/29/15 01:41 75-34-30.50 1
1,2-Dichloroethane ND ug/L 05/29/15 01:41 107-06-20.50 1
1,1-Dichloroethene ND ug/L 05/29/15 01:41 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 05/29/15 01:41 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 05/29/15 01:41 156-60-50.50 1
1,2-Dichloropropane ND ug/L 05/29/15 01:41 78-87-50.50 1
1,3-Dichloropropane ND ug/L 05/29/15 01:41 142-28-90.50 1
2,2-Dichloropropane ND ug/L 05/29/15 01:41 594-20-70.50 1
1,1-Dichloropropene ND ug/L 05/29/15 01:41 563-58-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Sample:TW-5 Lab ID:92250854003 Collected:05/20/15 13:00 Received:05/21/15 10:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
cis-1,3-Dichloropropene ND ug/L 05/29/15 01:41 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 05/29/15 01:41 10061-02-60.50 1
Diisopropyl ether ND ug/L 05/29/15 01:41 108-20-30.50 1
Ethylbenzene ND ug/L 05/29/15 01:41 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 05/29/15 01:41 87-68-3 L32.0 1
Isopropylbenzene (Cumene)ND ug/L 05/29/15 01:41 98-82-80.50 1
Methylene Chloride ND ug/L 05/29/15 01:41 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 05/29/15 01:41 1634-04-40.50 1
Naphthalene ND ug/L 05/29/15 01:41 91-20-32.0 1
n-Propylbenzene ND ug/L 05/29/15 01:41 103-65-10.50 1
Styrene ND ug/L 05/29/15 01:41 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 05/29/15 01:41 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 05/29/15 01:41 79-34-50.50 1
Tetrachloroethene ND ug/L 05/29/15 01:41 127-18-40.50 1
Toluene ND ug/L 05/29/15 01:41 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 05/29/15 01:41 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 05/29/15 01:41 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 05/29/15 01:41 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 05/29/15 01:41 79-00-50.50 1
Trichloroethene ND ug/L 05/29/15 01:41 79-01-60.50 1
Trichlorofluoromethane ND ug/L 05/29/15 01:41 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 05/29/15 01:41 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 05/29/15 01:41 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 05/29/15 01:41 108-67-80.50 1
Vinyl chloride ND ug/L 05/29/15 01:41 75-01-41.0 1
m&p-Xylene ND ug/L 05/29/15 01:41 179601-23-11.0 1
o-Xylene ND ug/L 05/29/15 01:41 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %05/29/15 01:41 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %05/29/15 01:41 460-00-470-130 1
Toluene-d8 (S)100 %05/29/15 01:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/31910
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92250854002, 92250854003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1469964
Associated Lab Samples:92250854002, 92250854003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 05/29/15 01:08
1,1,1-Trichloroethane ug/L ND 0.50 05/29/15 01:08
1,1,2,2-Tetrachloroethane ug/L ND 0.50 05/29/15 01:08
1,1,2-Trichloroethane ug/L ND 0.50 05/29/15 01:08
1,1-Dichloroethane ug/L ND 0.50 05/29/15 01:08
1,1-Dichloroethene ug/L ND 0.50 05/29/15 01:08
1,1-Dichloropropene ug/L ND 0.50 05/29/15 01:08
1,2,3-Trichlorobenzene ug/L ND 2.0 05/29/15 01:08
1,2,3-Trichloropropane ug/L ND 0.50 05/29/15 01:08
1,2,4-Trichlorobenzene ug/L ND 2.0 05/29/15 01:08
1,2,4-Trimethylbenzene ug/L ND 0.50 05/29/15 01:08
1,2-Dibromo-3-chloropropane ug/L ND 1.0 05/29/15 01:08
1,2-Dibromoethane (EDB)ug/L ND 0.50 05/29/15 01:08
1,2-Dichlorobenzene ug/L ND 0.50 05/29/15 01:08
1,2-Dichloroethane ug/L ND 0.50 05/29/15 01:08
1,2-Dichloropropane ug/L ND 0.50 05/29/15 01:08
1,3,5-Trimethylbenzene ug/L ND 0.50 05/29/15 01:08
1,3-Dichlorobenzene ug/L ND 0.50 05/29/15 01:08
1,3-Dichloropropane ug/L ND 0.50 05/29/15 01:08
1,4-Dichlorobenzene ug/L ND 0.50 05/29/15 01:08
2,2-Dichloropropane ug/L ND 0.50 05/29/15 01:08
2-Chlorotoluene ug/L ND 0.50 05/29/15 01:08
4-Chlorotoluene ug/L ND 0.50 05/29/15 01:08
Benzene ug/L ND 0.50 05/29/15 01:08
Bromobenzene ug/L ND 0.50 05/29/15 01:08
Bromochloromethane ug/L ND 0.50 05/29/15 01:08
Bromodichloromethane ug/L ND 0.50 05/29/15 01:08
Bromoform ug/L ND 0.50 05/29/15 01:08
Bromomethane ug/L ND 5.0 05/29/15 01:08
Carbon tetrachloride ug/L ND 0.50 05/29/15 01:08
Chlorobenzene ug/L ND 0.50 05/29/15 01:08
Chloroethane ug/L ND 1.0 05/29/15 01:08
Chloroform ug/L ND 0.50 05/29/15 01:08
Chloromethane ug/L ND 1.0 05/29/15 01:08
cis-1,2-Dichloroethene ug/L ND 0.50 05/29/15 01:08
cis-1,3-Dichloropropene ug/L ND 0.50 05/29/15 01:08
Dibromochloromethane ug/L ND 0.50 05/29/15 01:08
Dibromomethane ug/L ND 0.50 05/29/15 01:08
Dichlorodifluoromethane ug/L ND 0.50 05/29/15 01:08
Diisopropyl ether ug/L ND 0.50 05/29/15 01:08
Ethylbenzene ug/L ND 0.50 05/29/15 01:08
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1469964
Associated Lab Samples:92250854002, 92250854003
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 05/29/15 01:08
Isopropylbenzene (Cumene)ug/L ND 0.50 05/29/15 01:08
m&p-Xylene ug/L ND 1.0 05/29/15 01:08
Methyl-tert-butyl ether ug/L ND 0.50 05/29/15 01:08
Methylene Chloride ug/L ND 2.0 05/29/15 01:08
n-Butylbenzene ug/L ND 0.50 05/29/15 01:08
n-Propylbenzene ug/L ND 0.50 05/29/15 01:08
Naphthalene ug/L ND 2.0 05/29/15 01:08
o-Xylene ug/L ND 0.50 05/29/15 01:08
sec-Butylbenzene ug/L ND 0.50 05/29/15 01:08
Styrene ug/L ND 0.50 05/29/15 01:08
tert-Butylbenzene ug/L ND 0.50 05/29/15 01:08
Tetrachloroethene ug/L ND 0.50 05/29/15 01:08
Toluene ug/L ND 0.50 05/29/15 01:08
trans-1,2-Dichloroethene ug/L ND 0.50 05/29/15 01:08
trans-1,3-Dichloropropene ug/L ND 0.50 05/29/15 01:08
Trichloroethene ug/L ND 0.50 05/29/15 01:08
Trichlorofluoromethane ug/L ND 1.0 05/29/15 01:08
Vinyl chloride ug/L ND 1.0 05/29/15 01:08
1,2-Dichloroethane-d4 (S)%100 70-130 05/29/15 01:08
4-Bromofluorobenzene (S)%102 70-130 05/29/15 01:08
Toluene-d8 (S)%101 70-130 05/29/15 01:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1469965LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 61.450 123 60-140
1,1,1-Trichloroethane ug/L 58.850 118 60-140
1,1,2,2-Tetrachloroethane ug/L 56.250 112 60-140
1,1,2-Trichloroethane ug/L 54.750 109 60-140
1,1-Dichloroethane ug/L 52.950 106 60-140
1,1-Dichloroethene ug/L 54.750 109 60-140
1,1-Dichloropropene ug/L 59.550 119 60-140
1,2,3-Trichlorobenzene ug/L 56.750 113 60-140
1,2,3-Trichloropropane ug/L 56.950 114 60-140
1,2,4-Trichlorobenzene ug/L 56.450 113 60-140
1,2,4-Trimethylbenzene ug/L 56.450 113 60-140
1,2-Dibromo-3-chloropropane ug/L 55.950 112 60-140
1,2-Dibromoethane (EDB)ug/L 58.950 118 60-140
1,2-Dichlorobenzene ug/L 54.750 109 60-140
1,2-Dichloroethane ug/L 51.850 104 60-140
1,2-Dichloropropane ug/L 53.950 108 60-140
1,3,5-Trimethylbenzene ug/L 56.350 113 60-140
1,3-Dichlorobenzene ug/L 53.750 107 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1469965LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 55.250 110 60-140
1,4-Dichlorobenzene ug/L 52.650 105 60-140
2,2-Dichloropropane ug/L 52.950 106 60-140
2-Chlorotoluene ug/L 53.450 107 60-140
4-Chlorotoluene ug/L 53.750 107 60-140
Benzene ug/L 54.850 110 60-140
Bromobenzene ug/L 53.650 107 60-140
Bromochloromethane ug/L 53.250 106 60-140
Bromodichloromethane ug/L 53.750 107 60-140
Bromoform ug/L 49.550 99 60-140
Bromomethane ug/L 56.650 113 60-140
Carbon tetrachloride ug/L 67.250 134 60-140
Chlorobenzene ug/L 53.050 106 60-140
Chloroethane ug/L 54.650 109 60-140
Chloroform ug/L 49.150 98 60-140
Chloromethane ug/L 59.050 118 60-140
cis-1,2-Dichloroethene ug/L 53.250 106 60-140
cis-1,3-Dichloropropene ug/L 60.250 120 60-140
Dibromochloromethane ug/L 57.550 115 60-140
Dibromomethane ug/L 53.450 107 60-140
Dichlorodifluoromethane ug/L 72.9 L05014660-140
Diisopropyl ether ug/L 52.650 105 60-140
Ethylbenzene ug/L 55.350 111 60-140
Hexachloro-1,3-butadiene ug/L 71.1 L05014260-140
Isopropylbenzene (Cumene)ug/L 60.750 121 60-140
m&p-Xylene ug/L 111100 111 60-140
Methyl-tert-butyl ether ug/L 50.950 102 60-140
Methylene Chloride ug/L 57.050 114 60-140
n-Butylbenzene ug/L 57.750 115 60-140
n-Propylbenzene ug/L 56.250 112 60-140
Naphthalene ug/L 58.950 118 60-140
o-Xylene ug/L 55.050 110 60-140
sec-Butylbenzene ug/L 61.750 123 60-140
Styrene ug/L 58.750 117 60-140
tert-Butylbenzene ug/L 49.650 99 60-140
Tetrachloroethene ug/L 55.650 111 60-140
Toluene ug/L 53.350 107 60-140
trans-1,2-Dichloroethene ug/L 52.350 105 60-140
trans-1,3-Dichloropropene ug/L 61.350 123 60-140
Trichloroethene ug/L 52.350 105 60-140
Trichlorofluoromethane ug/L 63.050 126 60-140
Vinyl chloride ug/L 59.450 119 60-140
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1469966MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92251034007
1469967
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 120 60-140120 020ND24.0 24.0
1,1,1-Trichloroethane ug/L 20 128 60-140126 220ND25.7 25.1
1,1,2,2-Tetrachloroethane ug/L 20 117 60-140116 120ND23.3 23.1
1,1,2-Trichloroethane ug/L 20 115 60-140111 320ND23.0 22.3
1,1-Dichloroethane ug/L 20 117 60-140113 420ND23.4 22.6
1,1-Dichloroethene ug/L 20 125 60-140122 220ND24.9 24.3
1,1-Dichloropropene ug/L 20 134 60-140130 220ND26.7 26.0
1,2,3-Trichlorobenzene ug/L 20 124 60-140128 320ND24.8 25.6
1,2,3-Trichloropropane ug/L 20 117 60-140120 220ND23.5 23.9
1,2,4-Trichlorobenzene ug/L 20 122 60-140120 220ND24.4 24.1
1,2,4-Trimethylbenzene ug/L 20 121 60-140121 020ND24.3 24.2
1,2-Dibromo-3-chloropropane ug/L 20 107 60-140112 420ND21.5 22.4
1,2-Dibromoethane (EDB)ug/L 20 120 60-140120 020ND24.1 24.0
1,2-Dichlorobenzene ug/L 20 114 60-140116 220ND22.9 23.3
1,2-Dichloroethane ug/L 20 112 60-140108 420ND22.4 21.6
1,2-Dichloropropane ug/L 20 114 60-140112 220ND22.8 22.4
1,3,5-Trimethylbenzene ug/L 20 122 60-140122 020ND24.3 24.3
1,3-Dichlorobenzene ug/L 20 115 60-140115 020ND22.9 23.0
1,3-Dichloropropane ug/L 20 115 60-140114 120ND22.9 22.8
1,4-Dichlorobenzene ug/L 20 112 60-140113 120ND22.4 22.6
2,2-Dichloropropane ug/L 20 125 60-140123 120ND25.0 24.7
2-Chlorotoluene ug/L 20 115 60-140115 020ND23.1 23.1
4-Chlorotoluene ug/L 20 117 60-140116 020ND23.3 23.3
Benzene ug/L 20 118 60-140115 220ND23.6 23.1
Bromobenzene ug/L 20 123 60-140116 620ND24.6 23.2
Bromochloromethane ug/L 20 116 60-140112 320ND23.1 22.5
Bromodichloromethane ug/L 20 109 60-140104 520ND21.8 20.7
Bromoform ug/L 20 93 60-14092 120ND18.6 18.4
Bromomethane ug/L 20 102 60-14099 320ND20.5 19.8
Carbon tetrachloride ug/L 20 140 60-140137 220ND27.9 27.4
Chlorobenzene ug/L 20 113 60-140111 220ND22.6 22.2
Chloroethane ug/L 20 122 60-140124 120ND24.5 24.7
Chloroform ug/L 20 106 60-140104 220ND21.2 20.8
Chloromethane ug/L 20 133 60-140121 1020ND26.7 24.2
cis-1,2-Dichloroethene ug/L 20 115 60-140112 220ND22.9 22.5
cis-1,3-Dichloropropene ug/L 20 117 60-140115 220ND23.5 23.1
Dibromochloromethane ug/L 20 108 60-140108 020ND21.6 21.6
Dibromomethane ug/L 20 111 60-140110 120ND22.2 22.0
Dichlorodifluoromethane ug/L M02016760-140162 320ND33.4 32.5
Diisopropyl ether ug/L 20 114 60-140110 320ND22.7 22.0
Ethylbenzene ug/L 20 121 60-140120 120ND24.2 23.9
Hexachloro-1,3-butadiene ug/L M02015260-140156 320ND30.3 31.2
Isopropylbenzene (Cumene)ug/L 20 129 60-140127 220ND25.9 25.3
m&p-Xylene ug/L 40 120 60-140120 040ND48.0 47.9
Methyl-tert-butyl ether ug/L 20 109 60-140106 320ND21.8 21.2
Methylene Chloride ug/L 20 109 60-140106 320ND21.8 21.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1469966MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92251034007
1469967
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 122 60-140122 120ND24.5 24.4
n-Propylbenzene ug/L 20 123 60-140123 020ND24.6 24.6
Naphthalene ug/L 20 124 60-140127 320ND24.8 25.4
o-Xylene ug/L 20 117 60-140115 120ND23.3 23.0
sec-Butylbenzene ug/L 20 131 60-140131 020ND26.2 26.2
Styrene ug/L 20 121 60-140120 120ND24.2 24.0
tert-Butylbenzene ug/L 20 106 60-140107 120ND21.3 21.5
Tetrachloroethene ug/L 20 120 60-140118 220ND24.0 23.6
Toluene ug/L 20 115 60-140114 120ND23.1 22.8
trans-1,2-Dichloroethene ug/L 20 117 60-140114 320ND23.4 22.7
trans-1,3-Dichloropropene ug/L 20 119 60-140115 320ND23.7 23.0
Trichloroethene ug/L 20 112 60-140110 120ND22.4 22.1
Trichlorofluoromethane ug/L M12014560-140139 420ND29.0 27.9
Vinyl chloride ug/L 20 135 60-140130 320ND26.9 26.1
1,2-Dichloroethane-d4 (S)%100 70-13097
4-Bromofluorobenzene (S)%101 70-13099
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/31923
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92250854001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1470867
Associated Lab Samples:92250854001
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 05/29/15 16:36
1,1,1-Trichloroethane ug/L ND 0.50 05/29/15 16:36
1,1,2,2-Tetrachloroethane ug/L ND 0.50 05/29/15 16:36
1,1,2-Trichloroethane ug/L ND 0.50 05/29/15 16:36
1,1-Dichloroethane ug/L ND 0.50 05/29/15 16:36
1,1-Dichloroethene ug/L ND 0.50 05/29/15 16:36
1,1-Dichloropropene ug/L ND 0.50 05/29/15 16:36
1,2,3-Trichlorobenzene ug/L ND 2.0 05/29/15 16:36
1,2,3-Trichloropropane ug/L ND 0.50 05/29/15 16:36
1,2,4-Trichlorobenzene ug/L ND 2.0 05/29/15 16:36
1,2,4-Trimethylbenzene ug/L ND 0.50 05/29/15 16:36
1,2-Dibromo-3-chloropropane ug/L ND 1.0 05/29/15 16:36
1,2-Dibromoethane (EDB)ug/L ND 0.50 05/29/15 16:36
1,2-Dichlorobenzene ug/L ND 0.50 05/29/15 16:36
1,2-Dichloroethane ug/L ND 0.50 05/29/15 16:36
1,2-Dichloropropane ug/L ND 0.50 05/29/15 16:36
1,3,5-Trimethylbenzene ug/L ND 0.50 05/29/15 16:36
1,3-Dichlorobenzene ug/L ND 0.50 05/29/15 16:36
1,3-Dichloropropane ug/L ND 0.50 05/29/15 16:36
1,4-Dichlorobenzene ug/L ND 0.50 05/29/15 16:36
2,2-Dichloropropane ug/L ND 0.50 05/29/15 16:36
2-Chlorotoluene ug/L ND 0.50 05/29/15 16:36
4-Chlorotoluene ug/L ND 0.50 05/29/15 16:36
Benzene ug/L ND 0.50 05/29/15 16:36
Bromobenzene ug/L ND 0.50 05/29/15 16:36
Bromochloromethane ug/L ND 0.50 05/29/15 16:36
Bromodichloromethane ug/L ND 0.50 05/29/15 16:36
Bromoform ug/L ND 0.50 05/29/15 16:36
Bromomethane ug/L ND 5.0 05/29/15 16:36
Carbon tetrachloride ug/L ND 0.50 05/29/15 16:36
Chlorobenzene ug/L ND 0.50 05/29/15 16:36
Chloroethane ug/L ND 1.0 05/29/15 16:36
Chloroform ug/L ND 0.50 05/29/15 16:36
Chloromethane ug/L ND 1.0 05/29/15 16:36
cis-1,2-Dichloroethene ug/L ND 0.50 05/29/15 16:36
cis-1,3-Dichloropropene ug/L ND 0.50 05/29/15 16:36
Dibromochloromethane ug/L ND 0.50 05/29/15 16:36
Dibromomethane ug/L ND 0.50 05/29/15 16:36
Dichlorodifluoromethane ug/L ND 0.50 05/29/15 16:36
Diisopropyl ether ug/L ND 0.50 05/29/15 16:36
Ethylbenzene ug/L ND 0.50 05/29/15 16:36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1470867
Associated Lab Samples:92250854001
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 05/29/15 16:36
Isopropylbenzene (Cumene)ug/L ND 0.50 05/29/15 16:36
m&p-Xylene ug/L ND 1.0 05/29/15 16:36
Methyl-tert-butyl ether ug/L ND 0.50 05/29/15 16:36
Methylene Chloride ug/L ND 2.0 05/29/15 16:36
n-Butylbenzene ug/L ND 0.50 05/29/15 16:36
n-Propylbenzene ug/L ND 0.50 05/29/15 16:36
Naphthalene ug/L ND 2.0 05/29/15 16:36
o-Xylene ug/L ND 0.50 05/29/15 16:36
sec-Butylbenzene ug/L ND 0.50 05/29/15 16:36
Styrene ug/L ND 0.50 05/29/15 16:36
tert-Butylbenzene ug/L ND 0.50 05/29/15 16:36
Tetrachloroethene ug/L ND 0.50 05/29/15 16:36
Toluene ug/L ND 0.50 05/29/15 16:36
trans-1,2-Dichloroethene ug/L ND 0.50 05/29/15 16:36
trans-1,3-Dichloropropene ug/L ND 0.50 05/29/15 16:36
Trichloroethene ug/L ND 0.50 05/29/15 16:36
Trichlorofluoromethane ug/L ND 1.0 05/29/15 16:36
Vinyl chloride ug/L ND 1.0 05/29/15 16:36
1,2-Dichloroethane-d4 (S)%99 70-130 05/29/15 16:36
4-Bromofluorobenzene (S)%101 70-130 05/29/15 16:36
Toluene-d8 (S)%101 70-130 05/29/15 16:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1470868LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 60.450 121 60-140
1,1,1-Trichloroethane ug/L 57.950 116 60-140
1,1,2,2-Tetrachloroethane ug/L 57.050 114 60-140
1,1,2-Trichloroethane ug/L 54.750 109 60-140
1,1-Dichloroethane ug/L 52.950 106 60-140
1,1-Dichloroethene ug/L 53.150 106 60-140
1,1-Dichloropropene ug/L 58.750 117 60-140
1,2,3-Trichlorobenzene ug/L 60.950 122 60-140
1,2,3-Trichloropropane ug/L 57.050 114 60-140
1,2,4-Trichlorobenzene ug/L 59.050 118 60-140
1,2,4-Trimethylbenzene ug/L 57.150 114 60-140
1,2-Dibromo-3-chloropropane ug/L 56.250 112 60-140
1,2-Dibromoethane (EDB)ug/L 59.050 118 60-140
1,2-Dichlorobenzene ug/L 55.850 112 60-140
1,2-Dichloroethane ug/L 51.350 103 60-140
1,2-Dichloropropane ug/L 53.850 108 60-140
1,3,5-Trimethylbenzene ug/L 57.050 114 60-140
1,3-Dichlorobenzene ug/L 55.550 111 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1470868LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 55.050 110 60-140
1,4-Dichlorobenzene ug/L 53.350 107 60-140
2,2-Dichloropropane ug/L 60.150 120 60-140
2-Chlorotoluene ug/L 53.850 108 60-140
4-Chlorotoluene ug/L 54.550 109 60-140
Benzene ug/L 54.050 108 60-140
Bromobenzene ug/L 54.450 109 60-140
Bromochloromethane ug/L 53.350 107 60-140
Bromodichloromethane ug/L 53.050 106 60-140
Bromoform ug/L 48.550 97 60-140
Bromomethane ug/L 58.950 118 60-140
Carbon tetrachloride ug/L 64.550 129 60-140
Chlorobenzene ug/L 52.750 105 60-140
Chloroethane ug/L 53.250 106 60-140
Chloroform ug/L 48.850 98 60-140
Chloromethane ug/L 55.250 110 60-140
cis-1,2-Dichloroethene ug/L 52.950 106 60-140
cis-1,3-Dichloropropene ug/L 60.750 121 60-140
Dibromochloromethane ug/L 57.350 115 60-140
Dibromomethane ug/L 53.050 106 60-140
Dichlorodifluoromethane ug/L 66.650 133 60-140
Diisopropyl ether ug/L 52.350 105 60-140
Ethylbenzene ug/L 55.250 110 60-140
Hexachloro-1,3-butadiene ug/L 70.150 140 60-140
Isopropylbenzene (Cumene)ug/L 59.650 119 60-140
m&p-Xylene ug/L 109100 109 60-140
Methyl-tert-butyl ether ug/L 51.950 104 60-140
Methylene Chloride ug/L 56.650 113 60-140
n-Butylbenzene ug/L 59.250 118 60-140
n-Propylbenzene ug/L 57.050 114 60-140
Naphthalene ug/L 62.750 125 60-140
o-Xylene ug/L 54.850 110 60-140
sec-Butylbenzene ug/L 61.150 122 60-140
Styrene ug/L 58.550 117 60-140
tert-Butylbenzene ug/L 49.550 99 60-140
Tetrachloroethene ug/L 55.250 110 60-140
Toluene ug/L 53.050 106 60-140
trans-1,2-Dichloroethene ug/L 52.150 104 60-140
trans-1,3-Dichloropropene ug/L 62.450 125 60-140
Trichloroethene ug/L 51.950 104 60-140
Trichlorofluoromethane ug/L 59.750 119 60-140
Vinyl chloride ug/L 57.650 115 60-140
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1470869MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92251072008
1470870
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 109 60-140113 320ND21.8 22.5
1,1,1-Trichloroethane ug/L 20 117 60-140119 220ND23.4 23.8
1,1,2,2-Tetrachloroethane ug/L 20 108 60-140116 720ND21.5 23.2
1,1,2-Trichloroethane ug/L 20 110 60-140112 220ND21.9 22.4
1,1-Dichloroethane ug/L 20 113 60-140115 220ND22.6 22.9
1,1-Dichloroethene ug/L 20 119 60-140121 220ND23.8 24.3
1,1-Dichloropropene ug/L 20 129 60-140132 220ND25.7 26.3
1,2,3-Trichlorobenzene ug/L 20 112 60-140128 1320ND22.4 25.6
1,2,3-Trichloropropane ug/L 20 110 60-140112 220ND22.0 22.5
1,2,4-Trichlorobenzene ug/L 20 115 60-140122 620ND23.0 24.5
1,2,4-Trimethylbenzene ug/L 20 121 60-140121 020ND24.1 24.1
1,2-Dibromo-3-chloropropane ug/L 20 92 60-140106 1420ND18.5 21.3
1,2-Dibromoethane (EDB)ug/L 20 114 60-140117 220ND22.9 23.3
1,2-Dichlorobenzene ug/L 20 114 60-140116 220ND22.7 23.2
1,2-Dichloroethane ug/L 20 100 60-140102 220ND20.0 20.5
1,2-Dichloropropane ug/L 20 115 60-140115 020ND23.0 22.9
1,3,5-Trimethylbenzene ug/L 20 121 60-140121 020ND24.1 24.2
1,3-Dichlorobenzene ug/L 20 112 60-140114 120ND22.5 22.8
1,3-Dichloropropane ug/L 20 113 60-140111 120ND22.6 22.3
1,4-Dichlorobenzene ug/L 20 111 60-140111 020ND22.2 22.3
2,2-Dichloropropane ug/L 20 103 60-140108 520ND20.6 21.7
2-Chlorotoluene ug/L 20 117 60-140115 220ND23.3 22.9
4-Chlorotoluene ug/L 20 116 60-140115 120ND23.2 23.0
Benzene ug/L 20 116 60-140117 120ND23.3 23.5
Bromobenzene ug/L 20 118 60-140118 020ND23.6 23.6
Bromochloromethane ug/L 20 111 60-140114 220ND22.2 22.8
Bromodichloromethane ug/L 20 98 60-140100 120ND19.6 19.9
Bromoform ug/L 20 85 60-14091 720ND17.0 18.2
Bromomethane ug/L 20 103 60-140105 220ND20.6 21.1
Carbon tetrachloride ug/L 20 118 60-140130 1020ND23.6 25.9
Chlorobenzene ug/L 20 111 60-140111 120ND22.3 22.2
Chloroethane ug/L 20 125 60-140123 120ND24.9 24.7
Chloroform ug/L 20 102 60-140103 120ND20.3 20.6
Chloromethane ug/L 20 135 60-140133 220ND27.1 26.6
cis-1,2-Dichloroethene ug/L 20 111 60-140113 220ND22.3 22.7
cis-1,3-Dichloropropene ug/L 20 108 60-140112 420ND21.6 22.4
Dibromochloromethane ug/L 20 98 60-140102 520ND19.5 20.5
Dibromomethane ug/L 20 105 60-140109 420ND21.0 21.9
Dichlorodifluoromethane ug/L M12015060-140153 220ND30.0 30.6
Diisopropyl ether ug/L 20 108 60-140109 120ND21.5 21.8
Ethylbenzene ug/L 20 118 60-140118 020ND23.5 23.6
Hexachloro-1,3-butadiene ug/L M12015260-140160 520ND30.3 32.0
Isopropylbenzene (Cumene)ug/L 20 123 60-140125 120ND24.7 25.0
m&p-Xylene ug/L 40 116 60-140117 040ND46.5 46.6
Methyl-tert-butyl ether ug/L 20 102 60-140107 520ND20.3 21.5
Methylene Chloride ug/L 20 100 60-140103 320ND20.1 20.6
REPORT OF LABORATORY ANALYSIS
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Page 22 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1470869MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92251072008
1470870
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 118 60-140119 020ND23.6 23.7
n-Propylbenzene ug/L 20 122 60-140123 120ND24.4 24.5
Naphthalene ug/L 20 113 60-140126 1120ND22.6 25.2
o-Xylene ug/L 20 114 60-140115 120ND22.8 23.1
sec-Butylbenzene ug/L 20 129 60-140128 120ND25.8 25.7
Styrene ug/L 20 118 60-140120 220ND23.6 24.0
tert-Butylbenzene ug/L 20 104 60-140105 120ND20.8 21.0
Tetrachloroethene ug/L 20 117 60-140120 220ND23.5 24.0
Toluene ug/L 20 114 60-140113 120ND22.7 22.6
trans-1,2-Dichloroethene ug/L 20 114 60-140115 020ND22.9 22.9
trans-1,3-Dichloropropene ug/L 20 103 60-140112 820ND20.6 22.4
Trichloroethene ug/L 20 110 60-140110 020ND22.1 22.1
Trichlorofluoromethane ug/L 20 134 60-140134 020ND26.9 26.8
Vinyl chloride ug/L 20 132 60-140135 320ND26.4 27.0
1,2-Dichloroethane-d4 (S)%91 70-13094
4-Bromofluorobenzene (S)%99 70-130100
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
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Page 23 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/35331
EPA 625
EPA 625
625 MSS
Associated Lab Samples:92250854001, 92250854002, 92250854003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1468218
Associated Lab Samples:92250854001, 92250854002, 92250854003
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 05/29/15 21:07
2,4,6-Trichlorophenol ug/L ND 10.0 05/29/15 21:07
2,4-Dichlorophenol ug/L ND 5.0 05/29/15 21:07
2,4-Dimethylphenol ug/L ND 10.0 05/29/15 21:07
2,4-Dinitrophenol ug/L ND 50.0 05/29/15 21:07
2,4-Dinitrotoluene ug/L ND 5.0 05/29/15 21:07
2,6-Dinitrotoluene ug/L ND 5.0 05/29/15 21:07
2-Chloronaphthalene ug/L ND 5.0 05/29/15 21:07
2-Chlorophenol ug/L ND 5.0 05/29/15 21:07
2-Nitrophenol ug/L ND 5.0 05/29/15 21:07
3,3'-Dichlorobenzidine ug/L ND 25.0 05/29/15 21:07
4,6-Dinitro-2-methylphenol ug/L ND 20.0 05/29/15 21:07
4-Bromophenylphenyl ether ug/L ND 5.0 05/29/15 21:07
4-Chloro-3-methylphenol ug/L ND 5.0 05/29/15 21:07
4-Chlorophenylphenyl ether ug/L ND 5.0 05/29/15 21:07
4-Nitrophenol ug/L ND 50.0 05/29/15 21:07
Acenaphthene ug/L ND 5.0 05/29/15 21:07
Acenaphthylene ug/L ND 5.0 05/29/15 21:07
Anthracene ug/L ND 5.0 05/29/15 21:07
Benzo(a)anthracene ug/L ND 5.0 05/29/15 21:07
Benzo(a)pyrene ug/L ND 5.0 05/29/15 21:07
Benzo(b)fluoranthene ug/L ND 5.0 05/29/15 21:07
Benzo(g,h,i)perylene ug/L ND 5.0 05/29/15 21:07
Benzo(k)fluoranthene ug/L ND 5.0 05/29/15 21:07
bis(2-Chloroethoxy)methane ug/L ND 10.0 05/29/15 21:07
bis(2-Chloroethyl) ether ug/L ND 5.0 05/29/15 21:07
bis(2-Chloroisopropyl) ether ug/L ND 5.0 05/29/15 21:07
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 05/29/15 21:07
Butylbenzylphthalate ug/L ND 5.0 05/29/15 21:07
Chrysene ug/L ND 5.0 05/29/15 21:07
Di-n-butylphthalate ug/L ND 5.0 05/29/15 21:07
Di-n-octylphthalate ug/L ND 5.0 05/29/15 21:07
Dibenz(a,h)anthracene ug/L ND 5.0 05/29/15 21:07
Diethylphthalate ug/L ND 5.0 05/29/15 21:07
Dimethylphthalate ug/L ND 5.0 05/29/15 21:07
Fluoranthene ug/L ND 5.0 05/29/15 21:07
Fluorene ug/L ND 5.0 05/29/15 21:07
Hexachloro-1,3-butadiene ug/L ND 5.0 05/29/15 21:07
Hexachlorobenzene ug/L ND 5.0 05/29/15 21:07
Hexachlorocyclopentadiene ug/L ND 10.0 05/29/15 21:07
Hexachloroethane ug/L ND 5.0 05/29/15 21:07
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
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Huntersville, NC 28078
[phone]
Page 24 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1468218
Associated Lab Samples:92250854001, 92250854002, 92250854003
Matrix:Water
Analyzed
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 05/29/15 21:07
Isophorone ug/L ND 10.0 05/29/15 21:07
N-Nitroso-di-n-propylamine ug/L ND 5.0 05/29/15 21:07
N-Nitrosodimethylamine ug/L ND 5.0 05/29/15 21:07
N-Nitrosodiphenylamine ug/L ND 10.0 05/29/15 21:07
Naphthalene ug/L ND 5.0 05/29/15 21:07
Nitrobenzene ug/L ND 5.0 05/29/15 21:07
Pentachlorophenol ug/L ND 10.0 05/29/15 21:07
Phenanthrene ug/L ND 5.0 05/29/15 21:07
Phenol ug/L ND 5.0 05/29/15 21:07
Pyrene ug/L ND 5.0 05/29/15 21:07
2,4,6-Tribromophenol (S)%62 10-137 05/29/15 21:07
2-Fluorobiphenyl (S)%56 15-120 05/29/15 21:07
2-Fluorophenol (S)%33 10-120 05/29/15 21:07
Nitrobenzene-d5 (S)%67 10-120 05/29/15 21:07
Phenol-d6 (S)%22 10-120 05/29/15 21:07
Terphenyl-d14 (S)%81 11-131 05/29/15 21:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1468219LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1468220
1,2,4-Trichlorobenzene ug/L 25.150 50 44-1426632.9 27 30
2,4,6-Trichlorophenol ug/L 29.5 R1505937-1448944.3 40 30
2,4-Dichlorophenol ug/L 29.8 R150601-1918240.8 31 30
2,4-Dimethylphenol ug/L 29.350 59 32-1197738.6 28 30
2,4-Dinitrophenol ug/L 174250 70 1-18193231 28 30
2,4-Dinitrotoluene ug/L 36.650 73 39-1398642.9 16 30
2,6-Dinitrotoluene ug/L 32.750 65 50-1588643.0 27 30
2-Chloronaphthalene ug/L 26.7 L0,R1505360-1187939.6 39 30
2-Chlorophenol ug/L 27.3 R1505523-1347537.6 32 30
2-Nitrophenol ug/L 30.3 R1506129-1828441.9 32 30
3,3'-Dichlorobenzidine ug/L 65.1100 65 1-2628181.2 22 30
4,6-Dinitro-2-methylphenol ug/L 74.3100 74 1-1819494.4 24 30
4-Bromophenylphenyl ether ug/L 35.250 70 53-1279045.2 25 30
4-Chloro-3-methylphenol ug/L 61.5100 61 22-1477675.8 21 30
4-Chlorophenylphenyl ether ug/L 31.650 63 25-1588542.3 29 30
4-Nitrophenol ug/L 62.9250 25 1-1323177.6 21 30
Acenaphthene ug/L 26.8 R1505447-1457839.1 37 30
Acenaphthylene ug/L 27.8 R1505633-1458241.0 39 30
Anthracene ug/L 37.650 75 1-1668944.5 17 30
Benzo(a)anthracene ug/L 38.850 78 33-1439246.0 17 30
Benzo(a)pyrene ug/L 39.850 80 17-1639547.5 18 30
Benzo(b)fluoranthene ug/L 39.650 79 24-1599447.2 18 30
Benzo(g,h,i)perylene ug/L 40.150 80 1-2199648.2 18 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
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Page 25 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1468219LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1468220
Benzo(k)fluoranthene ug/L 39.050 78 11-1629346.5 18 30
bis(2-Chloroethoxy)methane ug/L 30.5 R1506133-1848441.8 31 30
bis(2-Chloroethyl) ether ug/L 30.2 R1506012-1588542.3 33 30
bis(2-Chloroisopropyl) ether ug/L 31.0 R1506236-1668843.8 34 30
bis(2-Ethylhexyl)phthalate ug/L 36.650 73 8-1588944.7 20 30
Butylbenzylphthalate ug/L 36.750 73 1-1529045.0 20 30
Chrysene ug/L 39.850 80 17-1689447.1 17 30
Di-n-butylphthalate ug/L 37.550 75 1-1188843.9 16 30
Di-n-octylphthalate ug/L 35.750 71 4-1469245.8 25 30
Dibenz(a,h)anthracene ug/L 40.150 80 1-2279748.6 19 30
Diethylphthalate ug/L 34.550 69 1-1148240.8 17 30
Dimethylphthalate ug/L 31.650 63 1-1128039.9 23 30
Fluoranthene ug/L 37.450 75 26-1378643.2 14 30
Fluorene ug/L 31.950 64 59-1218442.2 28 30
Hexachloro-1,3-butadiene ug/L 21.6 R1504324-1165929.6 31 30
Hexachlorobenzene ug/L 37.850 76 1-1529246.0 20 30
Hexachlorocyclopentadiene ug/L 18.1 R1503625-1506231.0 52 30
Hexachloroethane ug/L 19.8 R1504040-1135728.6 37 30
Indeno(1,2,3-cd)pyrene ug/L 38.650 77 1-1719547.5 21 30
Isophorone ug/L 26.2 R1505221-1967537.7 36 30
N-Nitroso-di-n-propylamine ug/L 29.2 R150581-2308341.4 35 30
N-Nitrosodimethylamine ug/L 15.9 R1503225-1505025.0 44 30
N-Nitrosodiphenylamine ug/L 35.850 72 25-1508743.4 19 30
Naphthalene ug/L 27.850 56 21-1337236.1 26 30
Nitrobenzene ug/L 27.450 55 35-1807336.6 29 30
Pentachlorophenol ug/L 77.1100 77 14-1769797.3 23 30
Phenanthrene ug/L 36.050 72 54-1208542.6 17 30
Phenol ug/L 11.4 R150235-1123216.0 34 30
Pyrene ug/L 37.950 76 52-1158944.3 16 30
2,4,6-Tribromophenol (S)%81 10-13797
2-Fluorobiphenyl (S)%52 15-12076
2-Fluorophenol (S)%32 10-12046
Nitrobenzene-d5 (S)%56 10-12074
Phenol-d6 (S)%21 10-12030
Terphenyl-d14 (S)%92 11-131105
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
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[phone]
Page 26 of 30
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
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[phone]
Page 27 of 30
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92250854
GUSSMAN CLEANERS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92250854001 OEXT/35331 MSSV/10728TW-3 EPA 625 EPA 625
92250854002 OEXT/35331 MSSV/10728TW-4 EPA 625 EPA 625
92250854003 OEXT/35331 MSSV/10728TW-5 EPA 625 EPA 625
92250854001 MSV/31923TW-3 SM 6200B
92250854002 MSV/31910TW-4 SM 6200B
92250854003 MSV/31910TW-5 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/01/2015 05:49 PM
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[phone]
Page 28 of 30
Page 29 of 30
Page 30 of 30