19070_Polo_Fmr_Gussman_Phase II_20150210

Environmental Services
ECS Carolinas, LLP
Wilmington, North Carolina 28405
910-686-9114

Report of
Gussman Cleaners, New Bern, Craven County, North Carolina

Prepared for
Avolis Engineering, PA/ New Bern, NC
February 10, 2015
Gussman Cleaners
New Bern, Craven County, North Carolina
ECS Project No. 22:22171
February 10, 2015

TABLE OF CONTENTS

1. PROJECT INFORMATION ................................................................................................. 1
2. SCOPE OF SERVICES....................................................................................................... 1
3. RESULTS ............................................................................................................................ 4
4. SUMMARY, CONCLUSIONS, AND RECOMMENDATIONS .............................................. 5
5. QUALIFICATIONS OF REPORT ........................................................................................ 5

FIGURES
Figure 1 - Site Location Map
Figure 2 - Sample Location Map

TABLES

Table 1 - Summary of Soil Analytical Results
Table 2 - Summary of Groundwater Analytical Results
Table 3 - Summary of Soil Gas Analytical Results

APPENDIX

Photographs
Boring Logs
Laboratory Data Sheets and Chain of Custody Record
HASP Confirmation Sheet

Gussman Cleaners
New Bern, Craven County, North Carolina
ECS Project No. 22:22171
February 10, 2015

1

1. PROJECT INFORMATION

The site is located at 223 Craven Street in New Bern, Craven County, North Carolina (Figure 1).
ECS was provided with the Executive Summary of a Phase I Environmental Site Assessment (ESA)
prepared by Avolis Engineering, P.A. (Avolis). The Executive Summary referenced the following key
factors and observations which contributed to the recognized environmental conditions (RECs).

 A dry cleaner operated on the property from 1956 through 2007 with dry cleaning solvents
stored in aboveground storage tanks (ASTs) at the rear of the building.
 Automotive sales and service occurred on the adjoining property to the north from 1931
through 1958.
 An automotive sales and machine shop operated on the southern adjoining property dating
back to 1958 and a gasoline tank was located on this property, approximately 15 feet south
of the site building from 1931 through 1948.

The Executive summary made the following recommendations

 Test the soil and groundwater at the rear of the property and midway of the building, on the
southern side of the building for contaminants associated with dry cleaning and automotive
repair operations.
 Perform sub slab soil gas assessment within the building for dry cleaning solvents.

In an effort to determine if the site has been impacted by the on-site and off-site RECs identified
in the Avolis Phase I ESA report, ECS was requested to provide a proposal to conduct
additional assessment at the site. The samples locations were determined by Mr. Avolis.
Project information is based on correspondence between Mr. Avolis with Avolis Engineering,
P.A. and Mr. Brooks Wall with ECS.

2. SCOPE OF SERVICES

The environmental assessment consisted of collecting two soil samples, two groundwater
samples, and two soil gas samples to address the above mentioned RECs. Geoprobe®
equipment was used to collect the soil and groundwater samples. The Geoprobe® consists of a
hydraulic jack mounted on an all-terrain vehicle (ATV). The Geoprobe® is capable of driving
various forms of groundwater, soil, and soil gas sampling probes into the ground to depths
equivalent of auger refusal. The subcontractor used for this project was Mid Atlantic Drilling,
Inc. (MAD). Field activities were conducted on January 22, 2015.

Public Utility Clearance

Prior to commencing with field activities, ECS contacted North Carolina 811 to locate/mark
public utilities at the site. Required separation distances between subsurface activities and
marked utilities (typically 30-inches) were maintained during the field activities.

Health and Safety Plan

As part of this assessment, ECS prepared a site-specific health and safety plan (HASP) for the
site. The HASP documented the known or suspected hazards, applicable personal protective
Gussman Cleaners
New Bern, Craven County, North Carolina
ECS Project No. 22:22171
February 10, 2015

2

equipment (PPE) of site personnel, and emergency response procedures. Prior to commencing
with field activities, ECS site personnel reviewed the site-specific HASP. A copy of the HASP
review confirmation sheet is included in the Appendix.

Geoprobe® Soil Borings

On January 22, 2015, ECS and MAD mobilized to the site to perform the sampling activities.
Soil boring B-1 was advanced on the western side of the site at the rear of the building to
assess the ASTs. Soil boring B-2 was advanced along the south side of the building near the
former UST location (Figure 2). Soil boring B-1 was advanced to a depth of approximately
twelve feet below ground surface (bgs). Soil boring B-2 was advanced to a depth of
approximately fifteen feet bgs. The soil samples were collected at a depth of approximately
three feet bgs, which is above the groundwater elevation observed during drilling activities at
approximately six to seven feet bgs.

The soil borings were advanced by hydraulically driving a four-foot long, 1.5-inch soil sampling
probe into the soil. Prior to advancing each boring, the down hole equipment and Geoprobe®
drill rig were decontaminated utilizing a high pressure steam cleaner that utilized municipal
water. The down hole equipment and drill rig were decontaminated to prevent cross-
contamination between boring locations. The soil sampling probe is lined with a disposable
clear plastic tube, which is replaced with each four-foot interval. After the probe is driven, the
clear plastic tube filled with soil is removed from the probe. The clear plastic tube is then cut
open to remove the soil. ECS visually classified the soils collected from each boring and
screened the soil samples for relative levels of volatile organic vapors using a field screening
instrument. Boring logs, which include descriptions of the soils encountered and field screening
results, were prepared for each boring and are included in the Appendix. The soils encountered
were observed to be brown to gray fine sands to brown/gray clayey sands.

The soil samples (B-1 and B-2) collected in the field were transferred into a new, clean resealable
bag (half full), and the bag placed in a warm location. Approximately ten minutes after the time of
collection, the bag was opened slightly and the probe of a Mini Rae 22 photo ionization detector
(PID) organic vapor analyzer was inserted, and the bag immediately resealed using finger pressure.
The PID was monitored and the reading recorded. Volatile organic vapors were not detected in
the soils collected from the borings. The recorded PID responses are presented on the boring logs
included in the Appendix.

The soil samples were placed into laboratory prepared containers. The sample containers were
labeled with ECS project number, sample identification, sample date and time, and requested
analytical analysis. The containers were placed into protective packaging material and placed
into a cooler with ice to maintain the samples at approximately 4 Celsius (C). The soil samples
were submitted to Pace Analytical Services, Inc. (Pace) in Huntersville, North Carolina (NC
certification #11) for chemical analysis. The soil samples (B-1 and B-2) were analyzed for
volatile organic compounds (VOCs) using EPA Method 8260/5035 and semi-volatile organic
compounds (SVOCs) using EPA Method 8270. ECS maintained proper chain-of-custody (COC)
procedures throughout the sample collection and transportation process. A copy of the COC is
included in the Appendix.

Gussman Cleaners
New Bern, Craven County, North Carolina
ECS Project No. 22:22171
February 10, 2015
3
Geoprobe® Groundwater Borings
Groundwater borings TW-1 and TW-2 were advanced at soil borings B-1 and B-2, respectively
(Figure 2). The groundwater borings were advanced by hydraulically driving a four-foot long,
1.5-inch diameter water-sampling probe into the soil to an approximate depth of twelve feet bgs
for GW-1 and fifteen feet bgs for GW-2. Groundwater was encountered at approximately six
and seven feet bgs.
The groundwater sampling probe is equipped with a stainless steel screen and a disposable
drive point. The probe is driven to depth and then the rod is retracted to expose the screen.
Groundwater then flows through the screen into the hollow probe rods. The groundwater is
pumped to the surface using a peristaltic pump with dedicated plastic tubing lowered through
the center of the probe rods. Immediately after collection, the groundwater samples were
transferred into sample containers provided by the laboratory. Upon completion of sampling, each
boring was properly abandoned.
The groundwater samples were placed into laboratory prepared containers. The sample
containers were labeled with ECS project number, sample identification, sample date and time,
and requested analytical analysis. The containers were placed into protective packaging
material and placed into a cooler with ice to maintain the samples at approximately 4 Celsius
(C). The soil and groundwater samples were submitted to Pace for chemical analysis. The
groundwater samples were analyzed for VOCs using EPA Method 8260 and SVOCs using EPA
Method 8270. ECS maintained proper chain-of-custody (COC) procedures throughout the
sample collection and transportation process. A copy of the COC is included in the Appendix.
Soil Gas Sampling
Two soil gas samples (SG-1 and SG-2, Figure 2) were collected beneath the slab of the building
in the area of the laundry equipment. The samples were collected by drilling a 3/8-inch hole
through the slab at both locations inside of the building. The hole extended through the slab
into the underlying sub-base. ECS field personnel then placed a soil vapor probe into the hole
and down into the sub-base. The probe was constructed of ¼-inch stainless steel tubing and a
¼-inch stainless steel valve with compression Swag-Lok® fittings. The annular space around
the tubing and concrete was sealed with inert non-VOC emitting putty. A section of high density
poly-ethylene tubing was connected to the stainless steel probe.
Prior to collecting the soil vapor samples, laboratory grade helium gas was used as a quality
assurance control measure to confirm the integrity of the probe seal. A plastic cylinder
(approximately 1.75 quarts) was placed and sealed over the sampling point and purged with
laboratory grade helium. The probe point tubing and tracer gas tubing were placed through the
cylinder wall via 3/16-inch rubber grommets. The open end of the cylinder was placed on a
rubber seal and held securely to the slab with a heavy weight. As the cylinder was flooded with
laboratory grade helium via the hose placed through the cylinder wall, the probe tubing was
connected to a Model MGD-2002 Multi-Gas Leak detector and the air stream being purged was
measured for helium. A helium concentration of less than five percent helium was considered
acceptable. If concentrations greater than five percent helium were measured, the probe tube
seal was reseated and the leak detection process was repeated.
Gussman Cleaners
New Bern, Craven County, North Carolina
ECS Project No. 22:22171
February 10, 2015

4

The tubing was then connected to a six-liter Summa canister, used to collect sub slab soil gas
samples. The two samples were collected using six-liter Summa canisters with a regulator and
vacuum gauge. The samples were collected at a flow rate of 0.2 L/min. The vacuum in the
canister was measured and recorded at the beginning and the end of the thirty minute sampling
cycle. Following sample collection, the canister was labeled and shipped to Pace in
Minneapolis, Minnesota to be analyzed for VOCs using EPA Method TO-15. ECS maintained
proper COC procedures throughout the sample collection and transportation process. A copy of the
COC is included in the Appendix. The probe was removed and the hole was filled with soil
cuttings and/or bentonite following sampling.

3. RESULTS

Soil Analytical Results

Laboratory analysis of soil sample B-1 detected acetone and 1,2,4-trimethylbenzene above
laboratory detection limits; however, the concentrations were below their respective soil to
groundwater and industrial/commercial maximum soil contaminant concentrations (MSCCs).
Laboratory analysis of soil sample B-2 detected concentrations of various SVOCs above laboratory
detection limits and their respective soil to groundwater MSCCs. Benzo(a)anthracene and
benzo(a)pyrene were detected at concentrations exceeding their respective industrial/commercial
MSCCs. A summary of the soil sample analysis is provided in Table 1. The laboratory analytical
data sheets and Chain of Custody Records are included in the Appendix.

Groundwater Analytical Results

Laboratory analysis of groundwater sample TW-1 detected targeted VOCs and SVOCs at
concentrations above laboratory detection limits. 1-methylnaphthalene was detected at a
concentration exceeding its North Carolina 2L Groundwater Quality Standards (NC2LGWQS). The
concentration did not exceed its Gross Contamination Level (GCL). Targeted compounds were not
detected above laboratory detection limits in the groundwater sample collected from TW-2. A
summary of the groundwater sample analysis is provided in Table 2. The laboratory analytical data
sheets and Chain of Custody Records are included in the Appendix.

Soil Gas Analytical Results

Laboratory analysis of soil gas samples SG-1 and SG-2 detected a variety of petroleum and
chlorinated VOCs above laboratory detection limits. However the concentrations detected in both
samples did not exceed their respective North Carolina Department of Environment and Natural
Resources (NCDENR), Division of Waste Management (DWM), Inactive Hazardous Sites Branch
(IHSB) for Non-Residential and Residential Sub Slab and Exterior Soil Vapor Intrusion Screening
Levels. A summary of the results are provided in Table 3. The laboratory data sheets are included
in the Appendix.

Gussman Cleaners
New Bern, Craven County, North Carolina
ECS Project No. 22:22171
February 10, 2015
5
4. SUMMARY, CONCLUSIONS, AND RECOMMENDATIONS
Upon completion of this, ECS summarizes and concludes the following:
On January 22, 2015, ECS observed and documented the advancement of two soil and
groundwater borings and two sub-slab soil gas borings at the site.
Groundwater was encountered at a depth of approximately six to seven feet bgs.
Benzo(a)anthracene and benzo(a)pyrene were detected in soil sample B-2 at concentrations
exceeding their respective industrial/commercial MSCCs. B-2 is located on the south side
of the site building, near the location of a former UST. Concentrations of targeted
compounds were not detected in soil sample B-1 at concentrations exceeding their
respective MSCCs.
Laboratory analysis of groundwater sample TW-1 detected targeted VOCs and SVOCs at
concentrations above laboratory detection limits. 1-methylnaphthalene was detected at a
concentration exceeding its NC2LGWQS but not its GCL. Targeted compounds were not
detected above the laboratory detection limit in the groundwater sample collected from TW-
2.
Laboratory analysis of soil gas samples SG-1 and SG-2 detected a variety of petroleum and
chlorinated VOCs above laboratory detection limits. However the concentrations detected
in both samples did not exceed their respective IHSB Non-Residential or Residential Sub Slab
and Exterior Soil Vapor Intrusion Screening Levels.
Based on the results of the assessment, ECS recommends the following:
ECS understands that a reporting obligation exists. A petroleum release above the
regulatory standard was identified in both soil and groundwater sample locations. ECS
recommends that a copy of this report be provided to the property owner and that they
consult legal counsel regarding their reporting obligation.
Based on the results of the assessment, the NCDENR will most likely require additional
assessment of the petroleum impacted soil and groundwater and/or completion of a receptor
survey to identify the site risk ranking.
5. QUALIFICATIONS OF REPORT
The activities and evaluative approaches used in this assessment are consistent with those
normally employed in environmental assessment projects of this type. Our evaluation of site
conditions has been based on our understanding of the site project information and the data
obtained during our field activities. This report was prepared for the express use of Avolis
Engineering. Use of this report by other individuals or companies implies their acceptance of the
General Conditions of Service of the original contract.
SOURCE:
UNITED STATES GEOLOGICAL
SURVEY 7.5-MINUTE SERIES
TOPOGRAPHIC MAP:
NEW BERN
NORTH CAROLINA,
DATED 1994
FIGURE 1
SITE LOCATION MAP
GUSSMAN CLEANERS
223 CRAVEN STREET
NEW BERN, CRAVEN COUNTY, NORTH CAROLINA
ECS PROJECT NO. 22-22171
SITE
SOURCE:
GOOGLE EARTH 2014
SCALE SHOWN ABOVE
FIGURE 2
SAMPLE LOCATION MAP
GUSSMAN CLEANERS
223 CRAVEN STREET
NEW BERN, CRAVEN COUNTY, NORTH CAROLINA
ECS PROJECT NO. 22-22171
TW-1/ B-1
SG-1
B-1/TW-1
SG-1
APPROXIMATE PROPERTY BOUNDARY
SOIL GAS SAMPLE LOCATION
SOIL/GROUNDWATER SAMPLE LOCATION
TW-2/ B-2
SG-2
Compound B-1 B-2
Analytical
Method
Soil to
Groundwater
MSCC (mg/kg)
Industrial/Commercial
MSCC (mg/kg)
Acetone 0.113 ND 8260 24 360,000
Benzo(a)anthracene ND 8.40 8270 0.35 8
Benzo(a)pyrene ND 8.65 8270 0.096 0.78
Benzo(b)fluoranthene ND 7.79 8270 1.2 8
Benzo(g,h,i)perylene ND 5.46 8270 6400 12,264
Benzo(k)fluoranthene ND 7.18 8270 12 78
Chrysene ND 8.95 8270 39 780
Fluoranthene ND 14.00 8270 290 16,400
Indeno(1,2,3-cd)pyrene ND 5.09 8270 3.4 8
Phenanthrene ND 5.45 8270 56 12,264
Pyrene ND 11.30 8270 270.0 12,264
1,2,4-Trimethylbenzene 0.019 ND 8260 9 20,440
Remainng VOCs ND ND 8260 Varies Varies
Remaining SVOCs ND ND 8270 Varies Varies
Notes:
Parameters reported in milligrams per liter (mg/kg)
MSCC = Maximum Soil Contaminant Concentration
ND = Not Detected, NA = Not Analyzed
Bold values represent concentrations above Industrial MSCC Standards
Samples collected on January 22, 2015
New Bern, Craven County, North Carolina
ECS Project Number 22-22171
Table 1
Summary of Soil Analytical Results
223 Craven Street
Gussman Cleaners
Compound TW-1 TW-2
Analytical
Method
NCAC 2L
Groundwater
Standards
1-Methylnaphthalene 15.2 ND 8270 1
Chlorobenzene 10.1 ND 8260 50
1,3-Dichlorobenzene 8.4 ND 8260 200
1,4-Dichlorobenzene 1.4 ND 8260 6
4-Methyl-2-pentanone (MIBK)28.7 ND 8260 100
Remaining VOCs ND ND 8260 Various
Remaining SVOCs ND ND 8270 Various
Notes:
ND = Not Detected
Parameters reported in micrograms per liter (ug/L)
Bold values represent concentrations above 15A NCAC 2L Standards
Samples collected on January 22, 2015
New Bern, Craven County, North Carolina
ECS Project Number 22-22171
Table 2
Summary of Groundwater Analytical Results
223 Craven Street
Gussman Cleaners
Parameter ANALTYCIAL
RESULTS
ANALTYCIAL
RESULTS
Sample ID SG-1 SG-2
Collection Date 1/22/2015 1/22/2015
Acetone 34.0 30.1 2,720,000
Benzene 5.7 1.6 1,570
2-Butanone (MEK)14.1 9.0 438,000
Dichlorodifluoromethane (Freon 12)3.3 3.0 876
Ethyl acetate BRL 9.1 6,130
Ethylbenzene 3.4 BRL 4,910
4-Ethyltoluene 2.4 2.2 NS
n-Heptane 5.0 3.8 NS
n-Hexane 11.4 29.6 61,300
2-Hexanone 1.7 BRL 2,630
Methylene Chloride 7.0 33.7 52,600
Propylene 9.6 7.1 263,000
Tetrachloroethene 3.3 3.2 3,500
Tetrahydrofuran 10.9 BRL 175,000
Toluene 14.5 7.8 438,000
1,2,4-Trimethylbenzene 9.4 8.3 613
1,3,5-Trimethylbenzene 2.5 2.1 NS
total Xylenes 18.6 9.1 8,760
Notes:
Results presented in micrograms per cubic meter (ug/m3), analogous to parts per billion (ppb)
BRL = Compound not detected at a concentration above the method reporting limit
Compounds not listed were not detected above laboratory reporting limits
NS = No NCDENR IHSB Standard Available
NCDENR IHSB Non-
Residential Sub-Slab and
Exterior Soil Gas
Screening Level (ug/m3)
North Carolina Department of Environment and Natural Resources, Inactive Hazardous Sites Branch Standard
(current as of June 2014)
Table 3
Summary of Soil Gas Analytical Results
Gussman Cleaners
223 Craven Street
New Bern, Craven County, North Carolina
ECS Project Number 22-22171
PHOTOGRAPH LOG
GUSSMAN CLEANERS
223 CRAVEN STREET
NEW BERN, CRAVEN COUNTY, NORTH CAROLINA
ECS PROJECT: 22-22171
Photograph 1: View of the site building from Craven Street.
Photograph 2: View of the rear of the site.
0
1.5
3
4.5
6
7.5
9
10.5
17.5
24.0
Sample
Concrete
ABC Stone
SP-SM
SC
Concrete
ABC Stone
Gray silty SAND - possible fill
Gray clayey SAND
Boring Terminated at 8'
PROJECT:Gussman Cleaners BORING NUM.B-1
CLIENT:Avolis Engineering, PA PROJECT NO.22.22171
LOCATION:
225 Craven Street, New Bern, NC
ELEVATION:
NA
DRILLER:
Mid Atlantic Drilling
DATE DRILLED:
1/22/2015
LOGGED BY:
KBW
DRILL RIG:
Geoprobe
DEPTH TO WATER:
7'
Elevation/
Depth (Ft)PI
D
Re
a
d
i
n
g
Sa
m
p
l
e
Nu
m
b
e
r
Sa
m
p
l
e
Re
c
o
v
e
r
y
(in
/
i
n
)
Gr
a
p
h
i
c

L
o
g
So
i
l
Cl
a
s
s
i
f
i
c
a
t
i
o
n
SOIL DESCRIPTION
Th
i
s

i
n
f
o
r
m
a
t
i
o
n

p
e
r
t
a
i
n
s

o
n
l
y

t
o

t
h
i
s

b
o
r
i
n
g

a
n
d

s
h
o
u
l
d

n
o
t

b
e

i
n
t
e
r
p
r
e
t
e
d

a
s

b
e
i
n
g

i
n
d
i
c
a
t
i
v
e

o
f

t
h
e

s
i
t
e
.
Page1of1
0
1.5
3
4.5
6
7.5
9
10.5
0.0
0.0
Sample
Asphalt
SM
Brick
SC
Asphalt
Black silty SAND
Bricks and Debris
Brown/orange clayey SAND
Boring Terminated at 8'
PROJECT:Gussman Cleaners BORING NUM.B-2
CLIENT:Avolis Engineering, PA PROJECT NO.22.22171
LOCATION:
225 Craven Street, New Bern, NC
ELEVATION:
NA
DRILLER:
Mid Atlantic Drilling
DATE DRILLED:
1/22/2015
LOGGED BY:
KBW
DRILL RIG:
Geoprobe
DEPTH TO WATER:
6'
Elevation/
Depth (Ft)PI
D
Re
a
d
i
n
g
Sa
m
p
l
e
Nu
m
b
e
r
Sa
m
p
l
e
Re
c
o
v
e
r
y
(in
/
i
n
)
Gr
a
p
h
i
c

L
o
g
So
i
l
Cl
a
s
s
i
f
i
c
a
t
i
o
n
SOIL DESCRIPTION
Th
i
s

i
n
f
o
r
m
a
t
i
o
n

p
e
r
t
a
i
n
s

o
n
l
y

t
o

t
h
i
s

b
o
r
i
n
g

a
n
d

s
h
o
u
l
d

n
o
t

b
e

i
n
t
e
r
p
r
e
t
e
d

a
s

b
e
i
n
g

i
n
d
i
c
a
t
i
v
e

o
f

t
h
e

s
i
t
e
.
Page1of1
#=CL#
February 03, 2015
LIMS USE: FR - AMY CONCHAS
LIMS OBJECT ID: 92234851
92234851
Project:
Pace Project No.:
RE:
Amy Conchas
ECS Limited
,
Gussman Cleaners 22171
Dear Amy Conchas:
Enclosed are the analytical results for sample(s) received by the laboratory on January 26, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
Enclosures
cc:Ms. Amy Conchas, ECS
Jonathan Prevatte, ECS Carolinas
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 43
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 43
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92234851001 B-1 EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CEJK
92234851002 B-2 EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CEJK
92234851003 TW-1 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CGAW
92234851004 TW-2 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 43
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92234851001 B-1
Acetone 113 ug/kg 01/30/15 18:15108EPA 8260
1,2,4-Trimethylbenzene 10.9 ug/kg 01/30/15 18:155.4EPA 8260
Percent Moisture 24.9 %01/29/15 16:230.10ASTM D2974-87
92234851002 B-2
Benzo(a)anthracene 8400 ug/kg 01/30/15 15:294230EPA 8270
Benzo(a)pyrene 8650 ug/kg 01/30/15 15:294230EPA 8270
Benzo(b)fluoranthene 7790 ug/kg 01/30/15 15:294230EPA 8270
Benzo(g,h,i)perylene 5460 ug/kg 01/30/15 15:294230EPA 8270
Benzo(k)fluoranthene 7180 ug/kg 01/30/15 15:294230EPA 8270
Chrysene 8950 ug/kg 01/30/15 15:294230EPA 8270
Fluoranthene 14000 ug/kg 01/30/15 15:294230EPA 8270
Indeno(1,2,3-cd)pyrene 5090 ug/kg 01/30/15 15:294230EPA 8270
Phenanthrene 5450 ug/kg 01/30/15 15:294230EPA 8270
Pyrene 11300 ug/kg 01/30/15 15:294230EPA 8270
Percent Moisture 21.9 %01/29/15 16:230.10ASTM D2974-87
92234851003 TW-1
1-Methylnaphthalene 15.2 ug/L 01/29/15 14:1410.0EPA 8270
Chlorobenzene 10.1 ug/L 02/02/15 13:371.0EPA 8260
1,3-Dichlorobenzene 8.4 ug/L 02/02/15 13:371.0EPA 8260
1,4-Dichlorobenzene 1.4 ug/L 02/02/15 13:371.0EPA 8260
4-Methyl-2-pentanone (MIBK)28.7 ug/L 02/02/15 13:375.0EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Sample:B-1 Lab ID:92234851001 Collected:01/22/15 10:30 Received:01/26/15 09:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 01/30/15 15:01 83-32-901/27/15 14:454391
Acenaphthylene ND ug/kg 01/30/15 15:01 208-96-801/27/15 14:454391
Aniline ND ug/kg 01/30/15 15:01 62-53-301/27/15 14:454391
Anthracene ND ug/kg 01/30/15 15:01 120-12-701/27/15 14:454391
Benzo(a)anthracene ND ug/kg 01/30/15 15:01 56-55-301/27/15 14:454391
Benzo(a)pyrene ND ug/kg 01/30/15 15:01 50-32-801/27/15 14:454391
Benzo(b)fluoranthene ND ug/kg 01/30/15 15:01 205-99-201/27/15 14:454391
Benzo(g,h,i)perylene ND ug/kg 01/30/15 15:01 191-24-201/27/15 14:454391
Benzo(k)fluoranthene ND ug/kg 01/30/15 15:01 207-08-901/27/15 14:454391
Benzoic Acid ND ug/kg 01/30/15 15:01 65-85-001/27/15 14:4522001
Benzyl alcohol ND ug/kg 01/30/15 15:01 100-51-601/27/15 14:458791
4-Bromophenylphenyl ether ND ug/kg 01/30/15 15:01 101-55-301/27/15 14:454391
Butylbenzylphthalate ND ug/kg 01/30/15 15:01 85-68-701/27/15 14:454391
4-Chloro-3-methylphenol ND ug/kg 01/30/15 15:01 59-50-701/27/15 14:458791
4-Chloroaniline ND ug/kg 01/30/15 15:01 106-47-801/27/15 14:4522001
bis(2-Chloroethoxy)methane ND ug/kg 01/30/15 15:01 111-91-101/27/15 14:454391
bis(2-Chloroethyl) ether ND ug/kg 01/30/15 15:01 111-44-401/27/15 14:454391
bis(2-Chloroisopropyl) ether ND ug/kg 01/30/15 15:01 108-60-101/27/15 14:454391
2-Chloronaphthalene ND ug/kg 01/30/15 15:01 91-58-701/27/15 14:454391
2-Chlorophenol ND ug/kg 01/30/15 15:01 95-57-801/27/15 14:454391
4-Chlorophenylphenyl ether ND ug/kg 01/30/15 15:01 7005-72-301/27/15 14:454391
Chrysene ND ug/kg 01/30/15 15:01 218-01-901/27/15 14:454391
Dibenz(a,h)anthracene ND ug/kg 01/30/15 15:01 53-70-301/27/15 14:454391
Dibenzofuran ND ug/kg 01/30/15 15:01 132-64-901/27/15 14:454391
1,2-Dichlorobenzene ND ug/kg 01/30/15 15:01 95-50-101/27/15 14:454391
1,3-Dichlorobenzene ND ug/kg 01/30/15 15:01 541-73-101/27/15 14:454391
1,4-Dichlorobenzene ND ug/kg 01/30/15 15:01 106-46-701/27/15 14:454391
3,3'-Dichlorobenzidine ND ug/kg 01/30/15 15:01 91-94-101/27/15 14:4522001
2,4-Dichlorophenol ND ug/kg 01/30/15 15:01 120-83-201/27/15 14:454391
Diethylphthalate ND ug/kg 01/30/15 15:01 84-66-201/27/15 14:454391
2,4-Dimethylphenol ND ug/kg 01/30/15 15:01 105-67-901/27/15 14:454391
Dimethylphthalate ND ug/kg 01/30/15 15:01 131-11-301/27/15 14:454391
Di-n-butylphthalate ND ug/kg 01/30/15 15:01 84-74-201/27/15 14:454391
4,6-Dinitro-2-methylphenol ND ug/kg 01/30/15 15:01 534-52-101/27/15 14:458791
2,4-Dinitrophenol ND ug/kg 01/30/15 15:01 51-28-501/27/15 14:4522001
2,4-Dinitrotoluene ND ug/kg 01/30/15 15:01 121-14-201/27/15 14:454391
2,6-Dinitrotoluene ND ug/kg 01/30/15 15:01 606-20-201/27/15 14:454391
Di-n-octylphthalate ND ug/kg 01/30/15 15:01 117-84-001/27/15 14:454391
bis(2-Ethylhexyl)phthalate ND ug/kg 01/30/15 15:01 117-81-701/27/15 14:454391
Fluoranthene ND ug/kg 01/30/15 15:01 206-44-001/27/15 14:454391
Fluorene ND ug/kg 01/30/15 15:01 86-73-701/27/15 14:454391
Hexachloro-1,3-butadiene ND ug/kg 01/30/15 15:01 87-68-301/27/15 14:454391
Hexachlorobenzene ND ug/kg 01/30/15 15:01 118-74-101/27/15 14:454391
Hexachlorocyclopentadiene ND ug/kg 01/30/15 15:01 77-47-401/27/15 14:454391
Hexachloroethane ND ug/kg 01/30/15 15:01 67-72-101/27/15 14:454391
Indeno(1,2,3-cd)pyrene ND ug/kg 01/30/15 15:01 193-39-501/27/15 14:454391
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Sample:B-1 Lab ID:92234851001 Collected:01/22/15 10:30 Received:01/26/15 09:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 01/30/15 15:01 78-59-101/27/15 14:454391
1-Methylnaphthalene ND ug/kg 01/30/15 15:01 90-12-001/27/15 14:454391
2-Methylnaphthalene ND ug/kg 01/30/15 15:01 91-57-601/27/15 14:454391
2-Methylphenol(o-Cresol)ND ug/kg 01/30/15 15:01 95-48-701/27/15 14:454391
3&4-Methylphenol(m&p Cresol)ND ug/kg 01/30/15 15:0101/27/15 14:454391
Naphthalene ND ug/kg 01/30/15 15:01 91-20-301/27/15 14:454391
2-Nitroaniline ND ug/kg 01/30/15 15:01 88-74-401/27/15 14:4522001
3-Nitroaniline ND ug/kg 01/30/15 15:01 99-09-201/27/15 14:4522001
4-Nitroaniline ND ug/kg 01/30/15 15:01 100-01-601/27/15 14:458791
Nitrobenzene ND ug/kg 01/30/15 15:01 98-95-301/27/15 14:454391
2-Nitrophenol ND ug/kg 01/30/15 15:01 88-75-501/27/15 14:454391
4-Nitrophenol ND ug/kg 01/30/15 15:01 100-02-701/27/15 14:4522001
N-Nitrosodimethylamine ND ug/kg 01/30/15 15:01 62-75-901/27/15 14:454391
N-Nitroso-di-n-propylamine ND ug/kg 01/30/15 15:01 621-64-701/27/15 14:454391
N-Nitrosodiphenylamine ND ug/kg 01/30/15 15:01 86-30-601/27/15 14:454391
Pentachlorophenol ND ug/kg 01/30/15 15:01 87-86-501/27/15 14:4522001
Phenanthrene ND ug/kg 01/30/15 15:01 85-01-801/27/15 14:454391
Phenol ND ug/kg 01/30/15 15:01 108-95-201/27/15 14:454391
Pyrene ND ug/kg 01/30/15 15:01 129-00-001/27/15 14:454391
1,2,4-Trichlorobenzene ND ug/kg 01/30/15 15:01 120-82-101/27/15 14:454391
2,4,5-Trichlorophenol ND ug/kg 01/30/15 15:01 95-95-401/27/15 14:454391
2,4,6-Trichlorophenol ND ug/kg 01/30/15 15:01 88-06-201/27/15 14:454391
Surrogates
Nitrobenzene-d5 (S)56 %01/30/15 15:01 4165-60-001/27/15 14:4523-110 1
2-Fluorobiphenyl (S)55 %01/30/15 15:01 321-60-801/27/15 14:4530-110 1
Terphenyl-d14 (S)39 %01/30/15 15:01 1718-51-001/27/15 14:4528-110 1
Phenol-d6 (S)56 %01/30/15 15:01 13127-88-301/27/15 14:4522-110 1
2-Fluorophenol (S)65 %01/30/15 15:01 367-12-401/27/15 14:4513-110 1
2,4,6-Tribromophenol (S)64 %01/30/15 15:01 118-79-601/27/15 14:4527-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 113 ug/kg 01/30/15 18:15 67-64-11081
Benzene ND ug/kg 01/30/15 18:15 71-43-25.4 1
Bromobenzene ND ug/kg 01/30/15 18:15 108-86-15.4 1
Bromochloromethane ND ug/kg 01/30/15 18:15 74-97-55.4 1
Bromodichloromethane ND ug/kg 01/30/15 18:15 75-27-45.4 1
Bromoform ND ug/kg 01/30/15 18:15 75-25-25.4 1
Bromomethane ND ug/kg 01/30/15 18:15 74-83-910.8 1
2-Butanone (MEK)ND ug/kg 01/30/15 18:15 78-93-31081
n-Butylbenzene ND ug/kg 01/30/15 18:15 104-51-85.4 1
sec-Butylbenzene ND ug/kg 01/30/15 18:15 135-98-85.4 1
tert-Butylbenzene ND ug/kg 01/30/15 18:15 98-06-65.4 1
Carbon tetrachloride ND ug/kg 01/30/15 18:15 56-23-55.4 1
Chlorobenzene ND ug/kg 01/30/15 18:15 108-90-75.4 1
Chloroethane ND ug/kg 01/30/15 18:15 75-00-310.8 1
Chloroform ND ug/kg 01/30/15 18:15 67-66-35.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Sample:B-1 Lab ID:92234851001 Collected:01/22/15 10:30 Received:01/26/15 09:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloromethane ND ug/kg 01/30/15 18:15 74-87-310.8 1
2-Chlorotoluene ND ug/kg 01/30/15 18:15 95-49-85.4 1
4-Chlorotoluene ND ug/kg 01/30/15 18:15 106-43-45.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 01/30/15 18:15 96-12-85.4 1
Dibromochloromethane ND ug/kg 01/30/15 18:15 124-48-15.4 1
1,2-Dibromoethane (EDB)ND ug/kg 01/30/15 18:15 106-93-45.4 1
Dibromomethane ND ug/kg 01/30/15 18:15 74-95-35.4 1
1,2-Dichlorobenzene ND ug/kg 01/30/15 18:15 95-50-15.4 1
1,3-Dichlorobenzene ND ug/kg 01/30/15 18:15 541-73-15.4 1
1,4-Dichlorobenzene ND ug/kg 01/30/15 18:15 106-46-75.4 1
Dichlorodifluoromethane ND ug/kg 01/30/15 18:15 75-71-810.8 1
1,1-Dichloroethane ND ug/kg 01/30/15 18:15 75-34-35.4 1
1,2-Dichloroethane ND ug/kg 01/30/15 18:15 107-06-25.4 1
1,1-Dichloroethene ND ug/kg 01/30/15 18:15 75-35-45.4 1
cis-1,2-Dichloroethene ND ug/kg 01/30/15 18:15 156-59-25.4 1
trans-1,2-Dichloroethene ND ug/kg 01/30/15 18:15 156-60-55.4 1
1,2-Dichloropropane ND ug/kg 01/30/15 18:15 78-87-55.4 1
1,3-Dichloropropane ND ug/kg 01/30/15 18:15 142-28-95.4 1
2,2-Dichloropropane ND ug/kg 01/30/15 18:15 594-20-75.4 1
1,1-Dichloropropene ND ug/kg 01/30/15 18:15 563-58-65.4 1
cis-1,3-Dichloropropene ND ug/kg 01/30/15 18:15 10061-01-55.4 1
trans-1,3-Dichloropropene ND ug/kg 01/30/15 18:15 10061-02-65.4 1
Diisopropyl ether ND ug/kg 01/30/15 18:15 108-20-35.4 1
Ethylbenzene ND ug/kg 01/30/15 18:15 100-41-45.4 1
Hexachloro-1,3-butadiene ND ug/kg 01/30/15 18:15 87-68-35.4 1
2-Hexanone ND ug/kg 01/30/15 18:15 591-78-653.9 1
Isopropylbenzene (Cumene)ND ug/kg 01/30/15 18:15 98-82-85.4 1
p-Isopropyltoluene ND ug/kg 01/30/15 18:15 99-87-65.4 1
Methylene Chloride ND ug/kg 01/30/15 18:15 75-09-221.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/30/15 18:15 108-10-153.9 1
Methyl-tert-butyl ether ND ug/kg 01/30/15 18:15 1634-04-45.4 1
Naphthalene ND ug/kg 01/30/15 18:15 91-20-35.4 1
n-Propylbenzene ND ug/kg 01/30/15 18:15 103-65-15.4 1
Styrene ND ug/kg 01/30/15 18:15 100-42-55.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 01/30/15 18:15 630-20-65.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 01/30/15 18:15 79-34-55.4 1
Tetrachloroethene ND ug/kg 01/30/15 18:15 127-18-45.4 1
Toluene ND ug/kg 01/30/15 18:15 108-88-35.4 1
1,2,3-Trichlorobenzene ND ug/kg 01/30/15 18:15 87-61-65.4 1
1,2,4-Trichlorobenzene ND ug/kg 01/30/15 18:15 120-82-15.4 1
1,1,1-Trichloroethane ND ug/kg 01/30/15 18:15 71-55-65.4 1
1,1,2-Trichloroethane ND ug/kg 01/30/15 18:15 79-00-55.4 1
Trichloroethene ND ug/kg 01/30/15 18:15 79-01-65.4 1
Trichlorofluoromethane ND ug/kg 01/30/15 18:15 75-69-45.4 1
1,2,3-Trichloropropane ND ug/kg 01/30/15 18:15 96-18-45.4 1
1,2,4-Trimethylbenzene 10.9 ug/kg 01/30/15 18:15 95-63-65.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Sample:B-1 Lab ID:92234851001 Collected:01/22/15 10:30 Received:01/26/15 09:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
1,3,5-Trimethylbenzene ND ug/kg 01/30/15 18:15 108-67-85.4 1
Vinyl acetate ND ug/kg 01/30/15 18:15 108-05-453.9 1
Vinyl chloride ND ug/kg 01/30/15 18:15 75-01-410.8 1
Xylene (Total)ND ug/kg 01/30/15 18:15 1330-20-710.8 1
m&p-Xylene ND ug/kg 01/30/15 18:15 179601-23-110.8 1
o-Xylene ND ug/kg 01/30/15 18:15 95-47-65.4 1
Surrogates
Toluene-d8 (S)97 %01/30/15 18:15 2037-26-570-130 1
4-Bromofluorobenzene (S)89 %01/30/15 18:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %01/30/15 18:15 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 24.9 %01/29/15 16:230.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Sample:B-2 Lab ID:92234851002 Collected:01/22/15 12:30 Received:01/26/15 09:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 01/30/15 15:29 83-32-901/27/15 14:45423010
Acenaphthylene ND ug/kg 01/30/15 15:29 208-96-801/27/15 14:45423010
Aniline ND ug/kg 01/30/15 15:29 62-53-301/27/15 14:45423010
Anthracene ND ug/kg 01/30/15 15:29 120-12-701/27/15 14:45423010
Benzo(a)anthracene 8400 ug/kg 01/30/15 15:29 56-55-301/27/15 14:45423010
Benzo(a)pyrene 8650 ug/kg 01/30/15 15:29 50-32-801/27/15 14:45423010
Benzo(b)fluoranthene 7790 ug/kg 01/30/15 15:29 205-99-201/27/15 14:45423010
Benzo(g,h,i)perylene 5460 ug/kg 01/30/15 15:29 191-24-201/27/15 14:45423010
Benzo(k)fluoranthene 7180 ug/kg 01/30/15 15:29 207-08-901/27/15 14:45423010
Benzoic Acid ND ug/kg 01/30/15 15:29 65-85-001/27/15 14:452110010
Benzyl alcohol ND ug/kg 01/30/15 15:29 100-51-601/27/15 14:45845010
4-Bromophenylphenyl ether ND ug/kg 01/30/15 15:29 101-55-301/27/15 14:45423010
Butylbenzylphthalate ND ug/kg 01/30/15 15:29 85-68-701/27/15 14:45423010
4-Chloro-3-methylphenol ND ug/kg 01/30/15 15:29 59-50-701/27/15 14:45845010
4-Chloroaniline ND ug/kg 01/30/15 15:29 106-47-801/27/15 14:452110010
bis(2-Chloroethoxy)methane ND ug/kg 01/30/15 15:29 111-91-101/27/15 14:45423010
bis(2-Chloroethyl) ether ND ug/kg 01/30/15 15:29 111-44-401/27/15 14:45423010
bis(2-Chloroisopropyl) ether ND ug/kg 01/30/15 15:29 108-60-101/27/15 14:45423010
2-Chloronaphthalene ND ug/kg 01/30/15 15:29 91-58-701/27/15 14:45423010
2-Chlorophenol ND ug/kg 01/30/15 15:29 95-57-801/27/15 14:45423010
4-Chlorophenylphenyl ether ND ug/kg 01/30/15 15:29 7005-72-301/27/15 14:45423010
Chrysene 8950 ug/kg 01/30/15 15:29 218-01-901/27/15 14:45423010
Dibenz(a,h)anthracene ND ug/kg 01/30/15 15:29 53-70-301/27/15 14:45423010
Dibenzofuran ND ug/kg 01/30/15 15:29 132-64-901/27/15 14:45423010
1,2-Dichlorobenzene ND ug/kg 01/30/15 15:29 95-50-101/27/15 14:45423010
1,3-Dichlorobenzene ND ug/kg 01/30/15 15:29 541-73-101/27/15 14:45423010
1,4-Dichlorobenzene ND ug/kg 01/30/15 15:29 106-46-701/27/15 14:45423010
3,3'-Dichlorobenzidine ND ug/kg 01/30/15 15:29 91-94-101/27/15 14:452110010
2,4-Dichlorophenol ND ug/kg 01/30/15 15:29 120-83-201/27/15 14:45423010
Diethylphthalate ND ug/kg 01/30/15 15:29 84-66-201/27/15 14:45423010
2,4-Dimethylphenol ND ug/kg 01/30/15 15:29 105-67-901/27/15 14:45423010
Dimethylphthalate ND ug/kg 01/30/15 15:29 131-11-301/27/15 14:45423010
Di-n-butylphthalate ND ug/kg 01/30/15 15:29 84-74-201/27/15 14:45423010
4,6-Dinitro-2-methylphenol ND ug/kg 01/30/15 15:29 534-52-101/27/15 14:45845010
2,4-Dinitrophenol ND ug/kg 01/30/15 15:29 51-28-501/27/15 14:452110010
2,4-Dinitrotoluene ND ug/kg 01/30/15 15:29 121-14-201/27/15 14:45423010
2,6-Dinitrotoluene ND ug/kg 01/30/15 15:29 606-20-201/27/15 14:45423010
Di-n-octylphthalate ND ug/kg 01/30/15 15:29 117-84-001/27/15 14:45423010
bis(2-Ethylhexyl)phthalate ND ug/kg 01/30/15 15:29 117-81-701/27/15 14:45423010
Fluoranthene 14000 ug/kg 01/30/15 15:29 206-44-001/27/15 14:45423010
Fluorene ND ug/kg 01/30/15 15:29 86-73-701/27/15 14:45423010
Hexachloro-1,3-butadiene ND ug/kg 01/30/15 15:29 87-68-301/27/15 14:45423010
Hexachlorobenzene ND ug/kg 01/30/15 15:29 118-74-101/27/15 14:45423010
Hexachlorocyclopentadiene ND ug/kg 01/30/15 15:29 77-47-401/27/15 14:45423010
Hexachloroethane ND ug/kg 01/30/15 15:29 67-72-101/27/15 14:45423010
Indeno(1,2,3-cd)pyrene 5090 ug/kg 01/30/15 15:29 193-39-501/27/15 14:45423010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Sample:B-2 Lab ID:92234851002 Collected:01/22/15 12:30 Received:01/26/15 09:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 01/30/15 15:29 78-59-101/27/15 14:45423010
1-Methylnaphthalene ND ug/kg 01/30/15 15:29 90-12-001/27/15 14:45423010
2-Methylnaphthalene ND ug/kg 01/30/15 15:29 91-57-601/27/15 14:45423010
2-Methylphenol(o-Cresol)ND ug/kg 01/30/15 15:29 95-48-701/27/15 14:45423010
3&4-Methylphenol(m&p Cresol)ND ug/kg 01/30/15 15:2901/27/15 14:45423010
Naphthalene ND ug/kg 01/30/15 15:29 91-20-301/27/15 14:45423010
2-Nitroaniline ND ug/kg 01/30/15 15:29 88-74-401/27/15 14:452110010
3-Nitroaniline ND ug/kg 01/30/15 15:29 99-09-201/27/15 14:452110010
4-Nitroaniline ND ug/kg 01/30/15 15:29 100-01-601/27/15 14:45845010
Nitrobenzene ND ug/kg 01/30/15 15:29 98-95-301/27/15 14:45423010
2-Nitrophenol ND ug/kg 01/30/15 15:29 88-75-501/27/15 14:45423010
4-Nitrophenol ND ug/kg 01/30/15 15:29 100-02-701/27/15 14:452110010
N-Nitrosodimethylamine ND ug/kg 01/30/15 15:29 62-75-901/27/15 14:45423010
N-Nitroso-di-n-propylamine ND ug/kg 01/30/15 15:29 621-64-701/27/15 14:45423010
N-Nitrosodiphenylamine ND ug/kg 01/30/15 15:29 86-30-601/27/15 14:45423010
Pentachlorophenol ND ug/kg 01/30/15 15:29 87-86-501/27/15 14:452110010
Phenanthrene 5450 ug/kg 01/30/15 15:29 85-01-801/27/15 14:45423010
Phenol ND ug/kg 01/30/15 15:29 108-95-201/27/15 14:45423010
Pyrene 11300 ug/kg 01/30/15 15:29 129-00-001/27/15 14:45423010
1,2,4-Trichlorobenzene ND ug/kg 01/30/15 15:29 120-82-101/27/15 14:45423010
2,4,5-Trichlorophenol ND ug/kg 01/30/15 15:29 95-95-401/27/15 14:45423010
2,4,6-Trichlorophenol ND ug/kg 01/30/15 15:29 88-06-201/27/15 14:45423010
Surrogates
Nitrobenzene-d5 (S)0 %01/30/15 15:29 4165-60-0 D3,S401/27/15 14:4523-110 10
2-Fluorobiphenyl (S)0 %01/30/15 15:29 321-60-801/27/15 14:4530-110 10
Terphenyl-d14 (S)0 %01/30/15 15:29 1718-51-001/27/15 14:4528-110 10
Phenol-d6 (S)0 %01/30/15 15:29 13127-88-301/27/15 14:4522-110 10
2-Fluorophenol (S)0 %01/30/15 15:29 367-12-401/27/15 14:4513-110 10
2,4,6-Tribromophenol (S)0 %01/30/15 15:29 118-79-601/27/15 14:4527-110 10
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 01/30/15 18:35 67-64-11261
Benzene ND ug/kg 01/30/15 18:35 71-43-26.3 1
Bromobenzene ND ug/kg 01/30/15 18:35 108-86-16.3 1
Bromochloromethane ND ug/kg 01/30/15 18:35 74-97-56.3 1
Bromodichloromethane ND ug/kg 01/30/15 18:35 75-27-46.3 1
Bromoform ND ug/kg 01/30/15 18:35 75-25-26.3 1
Bromomethane ND ug/kg 01/30/15 18:35 74-83-912.6 1
2-Butanone (MEK)ND ug/kg 01/30/15 18:35 78-93-31261
n-Butylbenzene ND ug/kg 01/30/15 18:35 104-51-86.3 1
sec-Butylbenzene ND ug/kg 01/30/15 18:35 135-98-86.3 1
tert-Butylbenzene ND ug/kg 01/30/15 18:35 98-06-66.3 1
Carbon tetrachloride ND ug/kg 01/30/15 18:35 56-23-56.3 1
Chlorobenzene ND ug/kg 01/30/15 18:35 108-90-76.3 1
Chloroethane ND ug/kg 01/30/15 18:35 75-00-312.6 1
Chloroform ND ug/kg 01/30/15 18:35 67-66-36.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Sample:B-2 Lab ID:92234851002 Collected:01/22/15 12:30 Received:01/26/15 09:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloromethane ND ug/kg 01/30/15 18:35 74-87-312.6 1
2-Chlorotoluene ND ug/kg 01/30/15 18:35 95-49-86.3 1
4-Chlorotoluene ND ug/kg 01/30/15 18:35 106-43-46.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 01/30/15 18:35 96-12-86.3 1
Dibromochloromethane ND ug/kg 01/30/15 18:35 124-48-16.3 1
1,2-Dibromoethane (EDB)ND ug/kg 01/30/15 18:35 106-93-46.3 1
Dibromomethane ND ug/kg 01/30/15 18:35 74-95-36.3 1
1,2-Dichlorobenzene ND ug/kg 01/30/15 18:35 95-50-16.3 1
1,3-Dichlorobenzene ND ug/kg 01/30/15 18:35 541-73-16.3 1
1,4-Dichlorobenzene ND ug/kg 01/30/15 18:35 106-46-76.3 1
Dichlorodifluoromethane ND ug/kg 01/30/15 18:35 75-71-812.6 1
1,1-Dichloroethane ND ug/kg 01/30/15 18:35 75-34-36.3 1
1,2-Dichloroethane ND ug/kg 01/30/15 18:35 107-06-26.3 1
1,1-Dichloroethene ND ug/kg 01/30/15 18:35 75-35-46.3 1
cis-1,2-Dichloroethene ND ug/kg 01/30/15 18:35 156-59-26.3 1
trans-1,2-Dichloroethene ND ug/kg 01/30/15 18:35 156-60-56.3 1
1,2-Dichloropropane ND ug/kg 01/30/15 18:35 78-87-56.3 1
1,3-Dichloropropane ND ug/kg 01/30/15 18:35 142-28-96.3 1
2,2-Dichloropropane ND ug/kg 01/30/15 18:35 594-20-76.3 1
1,1-Dichloropropene ND ug/kg 01/30/15 18:35 563-58-66.3 1
cis-1,3-Dichloropropene ND ug/kg 01/30/15 18:35 10061-01-56.3 1
trans-1,3-Dichloropropene ND ug/kg 01/30/15 18:35 10061-02-66.3 1
Diisopropyl ether ND ug/kg 01/30/15 18:35 108-20-36.3 1
Ethylbenzene ND ug/kg 01/30/15 18:35 100-41-46.3 1
Hexachloro-1,3-butadiene ND ug/kg 01/30/15 18:35 87-68-36.3 1
2-Hexanone ND ug/kg 01/30/15 18:35 591-78-663.0 1
Isopropylbenzene (Cumene)ND ug/kg 01/30/15 18:35 98-82-86.3 1
p-Isopropyltoluene ND ug/kg 01/30/15 18:35 99-87-66.3 1
Methylene Chloride ND ug/kg 01/30/15 18:35 75-09-225.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/30/15 18:35 108-10-163.0 1
Methyl-tert-butyl ether ND ug/kg 01/30/15 18:35 1634-04-46.3 1
Naphthalene ND ug/kg 01/30/15 18:35 91-20-36.3 1
n-Propylbenzene ND ug/kg 01/30/15 18:35 103-65-16.3 1
Styrene ND ug/kg 01/30/15 18:35 100-42-56.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 01/30/15 18:35 630-20-66.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 01/30/15 18:35 79-34-56.3 1
Tetrachloroethene ND ug/kg 01/30/15 18:35 127-18-46.3 1
Toluene ND ug/kg 01/30/15 18:35 108-88-36.3 1
1,2,3-Trichlorobenzene ND ug/kg 01/30/15 18:35 87-61-66.3 1
1,2,4-Trichlorobenzene ND ug/kg 01/30/15 18:35 120-82-16.3 1
1,1,1-Trichloroethane ND ug/kg 01/30/15 18:35 71-55-66.3 1
1,1,2-Trichloroethane ND ug/kg 01/30/15 18:35 79-00-56.3 1
Trichloroethene ND ug/kg 01/30/15 18:35 79-01-66.3 1
Trichlorofluoromethane ND ug/kg 01/30/15 18:35 75-69-46.3 1
1,2,3-Trichloropropane ND ug/kg 01/30/15 18:35 96-18-46.3 1
1,2,4-Trimethylbenzene ND ug/kg 01/30/15 18:35 95-63-66.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Sample:B-2 Lab ID:92234851002 Collected:01/22/15 12:30 Received:01/26/15 09:00 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
1,3,5-Trimethylbenzene ND ug/kg 01/30/15 18:35 108-67-86.3 1
Vinyl acetate ND ug/kg 01/30/15 18:35 108-05-463.0 1
Vinyl chloride ND ug/kg 01/30/15 18:35 75-01-412.6 1
Xylene (Total)ND ug/kg 01/30/15 18:35 1330-20-712.6 1
m&p-Xylene ND ug/kg 01/30/15 18:35 179601-23-112.6 1
o-Xylene ND ug/kg 01/30/15 18:35 95-47-66.3 1
Surrogates
Toluene-d8 (S)92 %01/30/15 18:35 2037-26-5 1g70-130 1
4-Bromofluorobenzene (S)71 %01/30/15 18:35 460-00-470-130 1
1,2-Dichloroethane-d4 (S)123 %01/30/15 18:35 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 21.9 %01/29/15 16:230.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Sample:TW-1 Lab ID:92234851003 Collected:01/22/15 11:00 Received:01/26/15 09:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/29/15 14:14 83-32-901/27/15 16:1510.0 1
Acenaphthylene ND ug/L 01/29/15 14:14 208-96-801/27/15 16:1510.0 1
Aniline ND ug/L 01/29/15 14:14 62-53-301/27/15 16:1510.0 1
Anthracene ND ug/L 01/29/15 14:14 120-12-701/27/15 16:1510.0 1
Benzo(a)anthracene ND ug/L 01/29/15 14:14 56-55-301/27/15 16:1510.0 1
Benzo(a)pyrene ND ug/L 01/29/15 14:14 50-32-801/27/15 16:1510.0 1
Benzo(b)fluoranthene ND ug/L 01/29/15 14:14 205-99-201/27/15 16:1510.0 1
Benzo(g,h,i)perylene ND ug/L 01/29/15 14:14 191-24-201/27/15 16:1510.0 1
Benzo(k)fluoranthene ND ug/L 01/29/15 14:14 207-08-901/27/15 16:1510.0 1
Benzoic Acid ND ug/L 01/29/15 14:14 65-85-001/27/15 16:1550.0 1
Benzyl alcohol ND ug/L 01/29/15 14:14 100-51-601/27/15 16:1520.0 1
4-Bromophenylphenyl ether ND ug/L 01/29/15 14:14 101-55-301/27/15 16:1510.0 1
Butylbenzylphthalate ND ug/L 01/29/15 14:14 85-68-701/27/15 16:1510.0 1
4-Chloro-3-methylphenol ND ug/L 01/29/15 14:14 59-50-701/27/15 16:1520.0 1
4-Chloroaniline ND ug/L 01/29/15 14:14 106-47-801/27/15 16:1520.0 1
bis(2-Chloroethoxy)methane ND ug/L 01/29/15 14:14 111-91-101/27/15 16:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 01/29/15 14:14 111-44-401/27/15 16:1510.0 1
bis(2-Chloroisopropyl) ether ND ug/L 01/29/15 14:14 108-60-101/27/15 16:1510.0 1
2-Chloronaphthalene ND ug/L 01/29/15 14:14 91-58-701/27/15 16:1510.0 1
2-Chlorophenol ND ug/L 01/29/15 14:14 95-57-801/27/15 16:1510.0 1
4-Chlorophenylphenyl ether ND ug/L 01/29/15 14:14 7005-72-301/27/15 16:1510.0 1
Chrysene ND ug/L 01/29/15 14:14 218-01-901/27/15 16:1510.0 1
Dibenz(a,h)anthracene ND ug/L 01/29/15 14:14 53-70-301/27/15 16:1510.0 1
Dibenzofuran ND ug/L 01/29/15 14:14 132-64-901/27/15 16:1510.0 1
1,2-Dichlorobenzene ND ug/L 01/29/15 14:14 95-50-101/27/15 16:1510.0 1
1,3-Dichlorobenzene ND ug/L 01/29/15 14:14 541-73-101/27/15 16:1510.0 1
1,4-Dichlorobenzene ND ug/L 01/29/15 14:14 106-46-701/27/15 16:1510.0 1
3,3'-Dichlorobenzidine ND ug/L 01/29/15 14:14 91-94-101/27/15 16:1520.0 1
2,4-Dichlorophenol ND ug/L 01/29/15 14:14 120-83-201/27/15 16:1510.0 1
Diethylphthalate ND ug/L 01/29/15 14:14 84-66-201/27/15 16:1510.0 1
2,4-Dimethylphenol ND ug/L 01/29/15 14:14 105-67-901/27/15 16:1510.0 1
Dimethylphthalate ND ug/L 01/29/15 14:14 131-11-301/27/15 16:1510.0 1
Di-n-butylphthalate ND ug/L 01/29/15 14:14 84-74-201/27/15 16:1510.0 1
4,6-Dinitro-2-methylphenol ND ug/L 01/29/15 14:14 534-52-101/27/15 16:1520.0 1
2,4-Dinitrophenol ND ug/L 01/29/15 14:14 51-28-501/27/15 16:1550.0 1
2,4-Dinitrotoluene ND ug/L 01/29/15 14:14 121-14-201/27/15 16:1510.0 1
2,6-Dinitrotoluene ND ug/L 01/29/15 14:14 606-20-201/27/15 16:1510.0 1
Di-n-octylphthalate ND ug/L 01/29/15 14:14 117-84-001/27/15 16:1510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/29/15 14:14 117-81-701/27/15 16:156.0 1
Fluoranthene ND ug/L 01/29/15 14:14 206-44-001/27/15 16:1510.0 1
Fluorene ND ug/L 01/29/15 14:14 86-73-701/27/15 16:1510.0 1
Hexachloro-1,3-butadiene ND ug/L 01/29/15 14:14 87-68-301/27/15 16:1510.0 1
Hexachlorobenzene ND ug/L 01/29/15 14:14 118-74-101/27/15 16:1510.0 1
Hexachlorocyclopentadiene ND ug/L 01/29/15 14:14 77-47-401/27/15 16:1510.0 1
Hexachloroethane ND ug/L 01/29/15 14:14 67-72-101/27/15 16:1510.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 01/29/15 14:14 193-39-501/27/15 16:1510.0 1
Isophorone ND ug/L 01/29/15 14:14 78-59-101/27/15 16:1510.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Sample:TW-1 Lab ID:92234851003 Collected:01/22/15 11:00 Received:01/26/15 09:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene 15.2 ug/L 01/29/15 14:14 90-12-001/27/15 16:1510.0 1
2-Methylnaphthalene ND ug/L 01/29/15 14:14 91-57-601/27/15 16:1510.0 1
2-Methylphenol(o-Cresol)ND ug/L 01/29/15 14:14 95-48-701/27/15 16:1510.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/29/15 14:1401/27/15 16:1510.0 1
Naphthalene ND ug/L 01/29/15 14:14 91-20-301/27/15 16:1510.0 1
2-Nitroaniline ND ug/L 01/29/15 14:14 88-74-401/27/15 16:1550.0 1
3-Nitroaniline ND ug/L 01/29/15 14:14 99-09-201/27/15 16:1550.0 1
4-Nitroaniline ND ug/L 01/29/15 14:14 100-01-601/27/15 16:1520.0 1
Nitrobenzene ND ug/L 01/29/15 14:14 98-95-301/27/15 16:1510.0 1
2-Nitrophenol ND ug/L 01/29/15 14:14 88-75-501/27/15 16:1510.0 1
4-Nitrophenol ND ug/L 01/29/15 14:14 100-02-701/27/15 16:1550.0 1
N-Nitrosodimethylamine ND ug/L 01/29/15 14:14 62-75-901/27/15 16:1510.0 1
N-Nitroso-di-n-propylamine ND ug/L 01/29/15 14:14 621-64-701/27/15 16:1510.0 1
N-Nitrosodiphenylamine ND ug/L 01/29/15 14:14 86-30-601/27/15 16:1510.0 1
Pentachlorophenol ND ug/L 01/29/15 14:14 87-86-501/27/15 16:1525.0 1
Phenanthrene ND ug/L 01/29/15 14:14 85-01-801/27/15 16:1510.0 1
Phenol ND ug/L 01/29/15 14:14 108-95-201/27/15 16:1510.0 1
Pyrene ND ug/L 01/29/15 14:14 129-00-001/27/15 16:1510.0 1
1,2,4-Trichlorobenzene ND ug/L 01/29/15 14:14 120-82-101/27/15 16:1510.0 1
2,4,5-Trichlorophenol ND ug/L 01/29/15 14:14 95-95-401/27/15 16:1510.0 1
2,4,6-Trichlorophenol ND ug/L 01/29/15 14:14 88-06-201/27/15 16:1510.0 1
Surrogates
Nitrobenzene-d5 (S)49 %01/29/15 14:14 4165-60-001/27/15 16:1521-110 1
2-Fluorobiphenyl (S)44 %01/29/15 14:14 321-60-801/27/15 16:1527-110 1
Terphenyl-d14 (S)58 %01/29/15 14:14 1718-51-001/27/15 16:1531-107 1
Phenol-d6 (S)17 %01/29/15 14:14 13127-88-301/27/15 16:1510-110 1
2-Fluorophenol (S)26 %01/29/15 14:14 367-12-401/27/15 16:1512-110 1
2,4,6-Tribromophenol (S)68 %01/29/15 14:14 118-79-601/27/15 16:1527-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 02/02/15 13:37 67-64-125.0 1
Benzene ND ug/L 02/02/15 13:37 71-43-21.0 1
Bromobenzene ND ug/L 02/02/15 13:37 108-86-11.0 1
Bromochloromethane ND ug/L 02/02/15 13:37 74-97-51.0 1
Bromodichloromethane ND ug/L 02/02/15 13:37 75-27-41.0 1
Bromoform ND ug/L 02/02/15 13:37 75-25-21.0 1
Bromomethane ND ug/L 02/02/15 13:37 74-83-92.0 1
2-Butanone (MEK)ND ug/L 02/02/15 13:37 78-93-35.0 1
Carbon tetrachloride ND ug/L 02/02/15 13:37 56-23-5 L31.0 1
Chlorobenzene 10.1 ug/L 02/02/15 13:37 108-90-71.0 1
Chloroethane ND ug/L 02/02/15 13:37 75-00-31.0 1
Chloroform ND ug/L 02/02/15 13:37 67-66-31.0 1
Chloromethane ND ug/L 02/02/15 13:37 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/02/15 13:37 95-49-81.0 1
4-Chlorotoluene ND ug/L 02/02/15 13:37 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 02/02/15 13:37 96-12-82.0 1
Dibromochloromethane ND ug/L 02/02/15 13:37 124-48-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Sample:TW-1 Lab ID:92234851003 Collected:01/22/15 11:00 Received:01/26/15 09:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 02/02/15 13:37 106-93-41.0 1
Dibromomethane ND ug/L 02/02/15 13:37 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 02/02/15 13:37 95-50-11.0 1
1,3-Dichlorobenzene 8.4 ug/L 02/02/15 13:37 541-73-11.0 1
1,4-Dichlorobenzene 1.4 ug/L 02/02/15 13:37 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 02/02/15 13:37 75-71-81.0 1
1,1-Dichloroethane ND ug/L 02/02/15 13:37 75-34-31.0 1
1,2-Dichloroethane ND ug/L 02/02/15 13:37 107-06-21.0 1
1,1-Dichloroethene ND ug/L 02/02/15 13:37 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 02/02/15 13:37 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 02/02/15 13:37 156-60-51.0 1
1,2-Dichloropropane ND ug/L 02/02/15 13:37 78-87-51.0 1
1,3-Dichloropropane ND ug/L 02/02/15 13:37 142-28-91.0 1
2,2-Dichloropropane ND ug/L 02/02/15 13:37 594-20-71.0 1
1,1-Dichloropropene ND ug/L 02/02/15 13:37 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 02/02/15 13:37 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 02/02/15 13:37 10061-02-61.0 1
Diisopropyl ether ND ug/L 02/02/15 13:37 108-20-31.0 1
Ethylbenzene ND ug/L 02/02/15 13:37 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 02/02/15 13:37 87-68-31.0 1
2-Hexanone ND ug/L 02/02/15 13:37 591-78-65.0 1
p-Isopropyltoluene ND ug/L 02/02/15 13:37 99-87-61.0 1
Methylene Chloride ND ug/L 02/02/15 13:37 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)28.7 ug/L 02/02/15 13:37 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 02/02/15 13:37 1634-04-41.0 1
Naphthalene ND ug/L 02/02/15 13:37 91-20-31.0 1
Styrene ND ug/L 02/02/15 13:37 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 02/02/15 13:37 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 02/02/15 13:37 79-34-51.0 1
Tetrachloroethene ND ug/L 02/02/15 13:37 127-18-41.0 1
Toluene ND ug/L 02/02/15 13:37 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 02/02/15 13:37 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 02/02/15 13:37 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 02/02/15 13:37 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 02/02/15 13:37 79-00-51.0 1
Trichloroethene ND ug/L 02/02/15 13:37 79-01-61.0 1
Trichlorofluoromethane ND ug/L 02/02/15 13:37 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/02/15 13:37 96-18-41.0 1
Vinyl acetate ND ug/L 02/02/15 13:37 108-05-42.0 1
Vinyl chloride ND ug/L 02/02/15 13:37 75-01-41.0 1
Xylene (Total)ND ug/L 02/02/15 13:37 1330-20-72.0 1
m&p-Xylene ND ug/L 02/02/15 13:37 179601-23-12.0 1
o-Xylene ND ug/L 02/02/15 13:37 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %02/02/15 13:37 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %02/02/15 13:37 17060-07-070-130 1
Toluene-d8 (S)104 %02/02/15 13:37 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Sample:TW-2 Lab ID:92234851004 Collected:01/22/15 13:30 Received:01/26/15 09:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/29/15 14:45 83-32-901/27/15 16:1510.0 1
Acenaphthylene ND ug/L 01/29/15 14:45 208-96-801/27/15 16:1510.0 1
Aniline ND ug/L 01/29/15 14:45 62-53-301/27/15 16:1510.0 1
Anthracene ND ug/L 01/29/15 14:45 120-12-701/27/15 16:1510.0 1
Benzo(a)anthracene ND ug/L 01/29/15 14:45 56-55-301/27/15 16:1510.0 1
Benzo(a)pyrene ND ug/L 01/29/15 14:45 50-32-801/27/15 16:1510.0 1
Benzo(b)fluoranthene ND ug/L 01/29/15 14:45 205-99-201/27/15 16:1510.0 1
Benzo(g,h,i)perylene ND ug/L 01/29/15 14:45 191-24-201/27/15 16:1510.0 1
Benzo(k)fluoranthene ND ug/L 01/29/15 14:45 207-08-901/27/15 16:1510.0 1
Benzoic Acid ND ug/L 01/29/15 14:45 65-85-001/27/15 16:1550.0 1
Benzyl alcohol ND ug/L 01/29/15 14:45 100-51-601/27/15 16:1520.0 1
4-Bromophenylphenyl ether ND ug/L 01/29/15 14:45 101-55-301/27/15 16:1510.0 1
Butylbenzylphthalate ND ug/L 01/29/15 14:45 85-68-701/27/15 16:1510.0 1
4-Chloro-3-methylphenol ND ug/L 01/29/15 14:45 59-50-701/27/15 16:1520.0 1
4-Chloroaniline ND ug/L 01/29/15 14:45 106-47-801/27/15 16:1520.0 1
bis(2-Chloroethoxy)methane ND ug/L 01/29/15 14:45 111-91-101/27/15 16:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 01/29/15 14:45 111-44-401/27/15 16:1510.0 1
bis(2-Chloroisopropyl) ether ND ug/L 01/29/15 14:45 108-60-101/27/15 16:1510.0 1
2-Chloronaphthalene ND ug/L 01/29/15 14:45 91-58-701/27/15 16:1510.0 1
2-Chlorophenol ND ug/L 01/29/15 14:45 95-57-801/27/15 16:1510.0 1
4-Chlorophenylphenyl ether ND ug/L 01/29/15 14:45 7005-72-301/27/15 16:1510.0 1
Chrysene ND ug/L 01/29/15 14:45 218-01-901/27/15 16:1510.0 1
Dibenz(a,h)anthracene ND ug/L 01/29/15 14:45 53-70-301/27/15 16:1510.0 1
Dibenzofuran ND ug/L 01/29/15 14:45 132-64-901/27/15 16:1510.0 1
1,2-Dichlorobenzene ND ug/L 01/29/15 14:45 95-50-101/27/15 16:1510.0 1
1,3-Dichlorobenzene ND ug/L 01/29/15 14:45 541-73-101/27/15 16:1510.0 1
1,4-Dichlorobenzene ND ug/L 01/29/15 14:45 106-46-701/27/15 16:1510.0 1
3,3'-Dichlorobenzidine ND ug/L 01/29/15 14:45 91-94-101/27/15 16:1520.0 1
2,4-Dichlorophenol ND ug/L 01/29/15 14:45 120-83-201/27/15 16:1510.0 1
Diethylphthalate ND ug/L 01/29/15 14:45 84-66-201/27/15 16:1510.0 1
2,4-Dimethylphenol ND ug/L 01/29/15 14:45 105-67-901/27/15 16:1510.0 1
Dimethylphthalate ND ug/L 01/29/15 14:45 131-11-301/27/15 16:1510.0 1
Di-n-butylphthalate ND ug/L 01/29/15 14:45 84-74-201/27/15 16:1510.0 1
4,6-Dinitro-2-methylphenol ND ug/L 01/29/15 14:45 534-52-101/27/15 16:1520.0 1
2,4-Dinitrophenol ND ug/L 01/29/15 14:45 51-28-501/27/15 16:1550.0 1
2,4-Dinitrotoluene ND ug/L 01/29/15 14:45 121-14-201/27/15 16:1510.0 1
2,6-Dinitrotoluene ND ug/L 01/29/15 14:45 606-20-201/27/15 16:1510.0 1
Di-n-octylphthalate ND ug/L 01/29/15 14:45 117-84-001/27/15 16:1510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/29/15 14:45 117-81-701/27/15 16:156.0 1
Fluoranthene ND ug/L 01/29/15 14:45 206-44-001/27/15 16:1510.0 1
Fluorene ND ug/L 01/29/15 14:45 86-73-701/27/15 16:1510.0 1
Hexachloro-1,3-butadiene ND ug/L 01/29/15 14:45 87-68-301/27/15 16:1510.0 1
Hexachlorobenzene ND ug/L 01/29/15 14:45 118-74-101/27/15 16:1510.0 1
Hexachlorocyclopentadiene ND ug/L 01/29/15 14:45 77-47-401/27/15 16:1510.0 1
Hexachloroethane ND ug/L 01/29/15 14:45 67-72-101/27/15 16:1510.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 01/29/15 14:45 193-39-501/27/15 16:1510.0 1
Isophorone ND ug/L 01/29/15 14:45 78-59-101/27/15 16:1510.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Sample:TW-2 Lab ID:92234851004 Collected:01/22/15 13:30 Received:01/26/15 09:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1-Methylnaphthalene ND ug/L 01/29/15 14:45 90-12-001/27/15 16:1510.0 1
2-Methylnaphthalene ND ug/L 01/29/15 14:45 91-57-601/27/15 16:1510.0 1
2-Methylphenol(o-Cresol)ND ug/L 01/29/15 14:45 95-48-701/27/15 16:1510.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/29/15 14:4501/27/15 16:1510.0 1
Naphthalene ND ug/L 01/29/15 14:45 91-20-301/27/15 16:1510.0 1
2-Nitroaniline ND ug/L 01/29/15 14:45 88-74-401/27/15 16:1550.0 1
3-Nitroaniline ND ug/L 01/29/15 14:45 99-09-201/27/15 16:1550.0 1
4-Nitroaniline ND ug/L 01/29/15 14:45 100-01-601/27/15 16:1520.0 1
Nitrobenzene ND ug/L 01/29/15 14:45 98-95-301/27/15 16:1510.0 1
2-Nitrophenol ND ug/L 01/29/15 14:45 88-75-501/27/15 16:1510.0 1
4-Nitrophenol ND ug/L 01/29/15 14:45 100-02-701/27/15 16:1550.0 1
N-Nitrosodimethylamine ND ug/L 01/29/15 14:45 62-75-901/27/15 16:1510.0 1
N-Nitroso-di-n-propylamine ND ug/L 01/29/15 14:45 621-64-701/27/15 16:1510.0 1
N-Nitrosodiphenylamine ND ug/L 01/29/15 14:45 86-30-601/27/15 16:1510.0 1
Pentachlorophenol ND ug/L 01/29/15 14:45 87-86-501/27/15 16:1525.0 1
Phenanthrene ND ug/L 01/29/15 14:45 85-01-801/27/15 16:1510.0 1
Phenol ND ug/L 01/29/15 14:45 108-95-201/27/15 16:1510.0 1
Pyrene ND ug/L 01/29/15 14:45 129-00-001/27/15 16:1510.0 1
1,2,4-Trichlorobenzene ND ug/L 01/29/15 14:45 120-82-101/27/15 16:1510.0 1
2,4,5-Trichlorophenol ND ug/L 01/29/15 14:45 95-95-401/27/15 16:1510.0 1
2,4,6-Trichlorophenol ND ug/L 01/29/15 14:45 88-06-201/27/15 16:1510.0 1
Surrogates
Nitrobenzene-d5 (S)48 %01/29/15 14:45 4165-60-001/27/15 16:1521-110 1
2-Fluorobiphenyl (S)52 %01/29/15 14:45 321-60-801/27/15 16:1527-110 1
Terphenyl-d14 (S)55 %01/29/15 14:45 1718-51-001/27/15 16:1531-107 1
Phenol-d6 (S)20 %01/29/15 14:45 13127-88-301/27/15 16:1510-110 1
2-Fluorophenol (S)29 %01/29/15 14:45 367-12-401/27/15 16:1512-110 1
2,4,6-Tribromophenol (S)62 %01/29/15 14:45 118-79-601/27/15 16:1527-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 02/02/15 14:10 67-64-125.0 1
Benzene ND ug/L 02/02/15 14:10 71-43-21.0 1
Bromobenzene ND ug/L 02/02/15 14:10 108-86-11.0 1
Bromochloromethane ND ug/L 02/02/15 14:10 74-97-51.0 1
Bromodichloromethane ND ug/L 02/02/15 14:10 75-27-41.0 1
Bromoform ND ug/L 02/02/15 14:10 75-25-21.0 1
Bromomethane ND ug/L 02/02/15 14:10 74-83-92.0 1
2-Butanone (MEK)ND ug/L 02/02/15 14:10 78-93-35.0 1
Carbon tetrachloride ND ug/L 02/02/15 14:10 56-23-5 L31.0 1
Chlorobenzene ND ug/L 02/02/15 14:10 108-90-71.0 1
Chloroethane ND ug/L 02/02/15 14:10 75-00-31.0 1
Chloroform ND ug/L 02/02/15 14:10 67-66-31.0 1
Chloromethane ND ug/L 02/02/15 14:10 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/02/15 14:10 95-49-81.0 1
4-Chlorotoluene ND ug/L 02/02/15 14:10 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 02/02/15 14:10 96-12-82.0 1
Dibromochloromethane ND ug/L 02/02/15 14:10 124-48-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Sample:TW-2 Lab ID:92234851004 Collected:01/22/15 13:30 Received:01/26/15 09:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 02/02/15 14:10 106-93-41.0 1
Dibromomethane ND ug/L 02/02/15 14:10 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 02/02/15 14:10 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 02/02/15 14:10 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 02/02/15 14:10 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 02/02/15 14:10 75-71-81.0 1
1,1-Dichloroethane ND ug/L 02/02/15 14:10 75-34-31.0 1
1,2-Dichloroethane ND ug/L 02/02/15 14:10 107-06-21.0 1
1,1-Dichloroethene ND ug/L 02/02/15 14:10 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 02/02/15 14:10 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 02/02/15 14:10 156-60-51.0 1
1,2-Dichloropropane ND ug/L 02/02/15 14:10 78-87-51.0 1
1,3-Dichloropropane ND ug/L 02/02/15 14:10 142-28-91.0 1
2,2-Dichloropropane ND ug/L 02/02/15 14:10 594-20-71.0 1
1,1-Dichloropropene ND ug/L 02/02/15 14:10 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 02/02/15 14:10 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 02/02/15 14:10 10061-02-61.0 1
Diisopropyl ether ND ug/L 02/02/15 14:10 108-20-31.0 1
Ethylbenzene ND ug/L 02/02/15 14:10 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 02/02/15 14:10 87-68-31.0 1
2-Hexanone ND ug/L 02/02/15 14:10 591-78-65.0 1
p-Isopropyltoluene ND ug/L 02/02/15 14:10 99-87-61.0 1
Methylene Chloride ND ug/L 02/02/15 14:10 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/02/15 14:10 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 02/02/15 14:10 1634-04-41.0 1
Naphthalene ND ug/L 02/02/15 14:10 91-20-31.0 1
Styrene ND ug/L 02/02/15 14:10 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 02/02/15 14:10 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 02/02/15 14:10 79-34-51.0 1
Tetrachloroethene ND ug/L 02/02/15 14:10 127-18-41.0 1
Toluene ND ug/L 02/02/15 14:10 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 02/02/15 14:10 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 02/02/15 14:10 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 02/02/15 14:10 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 02/02/15 14:10 79-00-51.0 1
Trichloroethene ND ug/L 02/02/15 14:10 79-01-61.0 1
Trichlorofluoromethane ND ug/L 02/02/15 14:10 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/02/15 14:10 96-18-41.0 1
Vinyl acetate ND ug/L 02/02/15 14:10 108-05-42.0 1
Vinyl chloride ND ug/L 02/02/15 14:10 75-01-41.0 1
Xylene (Total)ND ug/L 02/02/15 14:10 1330-20-72.0 1
m&p-Xylene ND ug/L 02/02/15 14:10 179601-23-12.0 1
o-Xylene ND ug/L 02/02/15 14:10 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)98 %02/02/15 14:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %02/02/15 14:10 17060-07-070-130 1
Toluene-d8 (S)96 %02/02/15 14:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30201
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92234851003, 92234851004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1382356
Associated Lab Samples:92234851003, 92234851004
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 02/02/15 11:40
1,1,1-Trichloroethane ug/L ND 1.0 02/02/15 11:40
1,1,2,2-Tetrachloroethane ug/L ND 1.0 02/02/15 11:40
1,1,2-Trichloroethane ug/L ND 1.0 02/02/15 11:40
1,1-Dichloroethane ug/L ND 1.0 02/02/15 11:40
1,1-Dichloroethene ug/L ND 1.0 02/02/15 11:40
1,1-Dichloropropene ug/L ND 1.0 02/02/15 11:40
1,2,3-Trichlorobenzene ug/L ND 1.0 02/02/15 11:40
1,2,3-Trichloropropane ug/L ND 1.0 02/02/15 11:40
1,2,4-Trichlorobenzene ug/L ND 1.0 02/02/15 11:40
1,2-Dibromo-3-chloropropane ug/L ND 2.0 02/02/15 11:40
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/02/15 11:40
1,2-Dichlorobenzene ug/L ND 1.0 02/02/15 11:40
1,2-Dichloroethane ug/L ND 1.0 02/02/15 11:40
1,2-Dichloropropane ug/L ND 1.0 02/02/15 11:40
1,3-Dichlorobenzene ug/L ND 1.0 02/02/15 11:40
1,3-Dichloropropane ug/L ND 1.0 02/02/15 11:40
1,4-Dichlorobenzene ug/L ND 1.0 02/02/15 11:40
2,2-Dichloropropane ug/L ND 1.0 02/02/15 11:40
2-Butanone (MEK)ug/L ND 5.0 02/02/15 11:40
2-Chlorotoluene ug/L ND 1.0 02/02/15 11:40
2-Hexanone ug/L ND 5.0 02/02/15 11:40
4-Chlorotoluene ug/L ND 1.0 02/02/15 11:40
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 02/02/15 11:40
Acetone ug/L ND 25.0 02/02/15 11:40
Benzene ug/L ND 1.0 02/02/15 11:40
Bromobenzene ug/L ND 1.0 02/02/15 11:40
Bromochloromethane ug/L ND 1.0 02/02/15 11:40
Bromodichloromethane ug/L ND 1.0 02/02/15 11:40
Bromoform ug/L ND 1.0 02/02/15 11:40
Bromomethane ug/L ND 2.0 02/02/15 11:40
Carbon tetrachloride ug/L ND 1.0 02/02/15 11:40
Chlorobenzene ug/L ND 1.0 02/02/15 11:40
Chloroethane ug/L ND 1.0 02/02/15 11:40
Chloroform ug/L ND 1.0 02/02/15 11:40
Chloromethane ug/L ND 1.0 02/02/15 11:40
cis-1,2-Dichloroethene ug/L ND 1.0 02/02/15 11:40
cis-1,3-Dichloropropene ug/L ND 1.0 02/02/15 11:40
Dibromochloromethane ug/L ND 1.0 02/02/15 11:40
Dibromomethane ug/L ND 1.0 02/02/15 11:40
Dichlorodifluoromethane ug/L ND 1.0 02/02/15 11:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1382356
Associated Lab Samples:92234851003, 92234851004
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 1.0 02/02/15 11:40
Ethylbenzene ug/L ND 1.0 02/02/15 11:40
Hexachloro-1,3-butadiene ug/L ND 1.0 02/02/15 11:40
m&p-Xylene ug/L ND 2.0 02/02/15 11:40
Methyl-tert-butyl ether ug/L ND 1.0 02/02/15 11:40
Methylene Chloride ug/L ND 2.0 02/02/15 11:40
Naphthalene ug/L ND 1.0 02/02/15 11:40
o-Xylene ug/L ND 1.0 02/02/15 11:40
p-Isopropyltoluene ug/L ND 1.0 02/02/15 11:40
Styrene ug/L ND 1.0 02/02/15 11:40
Tetrachloroethene ug/L ND 1.0 02/02/15 11:40
Toluene ug/L ND 1.0 02/02/15 11:40
trans-1,2-Dichloroethene ug/L ND 1.0 02/02/15 11:40
trans-1,3-Dichloropropene ug/L ND 1.0 02/02/15 11:40
Trichloroethene ug/L ND 1.0 02/02/15 11:40
Trichlorofluoromethane ug/L ND 1.0 02/02/15 11:40
Vinyl acetate ug/L ND 2.0 02/02/15 11:40
Vinyl chloride ug/L ND 1.0 02/02/15 11:40
Xylene (Total)ug/L ND 2.0 02/02/15 11:40
1,2-Dichloroethane-d4 (S)%100 70-130 02/02/15 11:40
4-Bromofluorobenzene (S)%100 70-130 02/02/15 11:40
Toluene-d8 (S)%94 70-130 02/02/15 11:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1382357LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 58.250 116 70-130
1,1,1-Trichloroethane ug/L 62.250 124 70-130
1,1,2,2-Tetrachloroethane ug/L 48.250 96 70-130
1,1,2-Trichloroethane ug/L 52.350 105 70-130
1,1-Dichloroethane ug/L 51.550 103 70-130
1,1-Dichloroethene ug/L 52.450 105 70-132
1,1-Dichloropropene ug/L 56.150 112 70-130
1,2,3-Trichlorobenzene ug/L 52.950 106 70-135
1,2,3-Trichloropropane ug/L 55.650 111 70-130
1,2,4-Trichlorobenzene ug/L 55.650 111 70-134
1,2-Dibromo-3-chloropropane ug/L 59.350 119 70-130
1,2-Dibromoethane (EDB)ug/L 54.150 108 70-130
1,2-Dichlorobenzene ug/L 53.350 107 70-130
1,2-Dichloroethane ug/L 62.850 126 70-130
1,2-Dichloropropane ug/L 51.250 102 70-130
1,3-Dichlorobenzene ug/L 52.450 105 70-130
1,3-Dichloropropane ug/L 51.350 103 70-130
1,4-Dichlorobenzene ug/L 52.450 105 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1382357LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 62.750 125 58-145
2-Butanone (MEK)ug/L 118100 118 70-145
2-Chlorotoluene ug/L 49.150 98 70-130
2-Hexanone ug/L 120100 120 70-144
4-Chlorotoluene ug/L 52.950 106 70-130
4-Methyl-2-pentanone (MIBK)ug/L 121100 121 70-140
Acetone ug/L 130100 130 50-175
Benzene ug/L 48.850 98 70-130
Bromobenzene ug/L 52.250 104 70-130
Bromochloromethane ug/L 51.250 102 70-130
Bromodichloromethane ug/L 54.550 109 70-130
Bromoform ug/L 57.550 115 70-130
Bromomethane ug/L 57.050 114 54-130
Carbon tetrachloride ug/L 66.6 L35013370-132
Chlorobenzene ug/L 51.950 104 70-130
Chloroethane ug/L 55.450 111 64-134
Chloroform ug/L 53.850 108 70-130
Chloromethane ug/L 53.950 108 64-130
cis-1,2-Dichloroethene ug/L 56.150 112 70-131
cis-1,3-Dichloropropene ug/L 56.650 113 70-130
Dibromochloromethane ug/L 55.850 112 70-130
Dibromomethane ug/L 54.450 109 70-131
Dichlorodifluoromethane ug/L 59.550 119 56-130
Diisopropyl ether ug/L 54.550 109 70-130
Ethylbenzene ug/L 52.850 106 70-130
Hexachloro-1,3-butadiene ug/L 53.350 107 70-130
m&p-Xylene ug/L 108100 108 70-130
Methyl-tert-butyl ether ug/L 53.550 107 70-130
Methylene Chloride ug/L 59.150 118 63-130
Naphthalene ug/L 55.150 110 70-138
o-Xylene ug/L 52.650 105 70-130
p-Isopropyltoluene ug/L 53.350 107 70-130
Styrene ug/L 55.250 110 70-130
Tetrachloroethene ug/L 51.250 102 70-130
Toluene ug/L 51.750 103 70-130
trans-1,2-Dichloroethene ug/L 54.950 110 70-130
trans-1,3-Dichloropropene ug/L 61.550 123 70-132
Trichloroethene ug/L 51.350 103 70-130
Trichlorofluoromethane ug/L 63.650 127 62-133
Vinyl acetate ug/L 122100 122 66-157
Vinyl chloride ug/L 46.250 92 50-150
Xylene (Total)ug/L 160150 107 70-130
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30175
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92234851001, 92234851002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1381328
Associated Lab Samples:92234851001, 92234851002
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 4.6 01/30/15 11:57
1,1,1-Trichloroethane ug/kg ND 4.6 01/30/15 11:57
1,1,2,2-Tetrachloroethane ug/kg ND 4.6 01/30/15 11:57
1,1,2-Trichloroethane ug/kg ND 4.6 01/30/15 11:57
1,1-Dichloroethane ug/kg ND 4.6 01/30/15 11:57
1,1-Dichloroethene ug/kg ND 4.6 01/30/15 11:57
1,1-Dichloropropene ug/kg ND 4.6 01/30/15 11:57
1,2,3-Trichlorobenzene ug/kg ND 4.6 01/30/15 11:57
1,2,3-Trichloropropane ug/kg ND 4.6 01/30/15 11:57
1,2,4-Trichlorobenzene ug/kg ND 4.6 01/30/15 11:57
1,2,4-Trimethylbenzene ug/kg ND 4.6 01/30/15 11:57
1,2-Dibromo-3-chloropropane ug/kg ND 4.6 01/30/15 11:57
1,2-Dibromoethane (EDB)ug/kg ND 4.6 01/30/15 11:57
1,2-Dichlorobenzene ug/kg ND 4.6 01/30/15 11:57
1,2-Dichloroethane ug/kg ND 4.6 01/30/15 11:57
1,2-Dichloropropane ug/kg ND 4.6 01/30/15 11:57
1,3,5-Trimethylbenzene ug/kg ND 4.6 01/30/15 11:57
1,3-Dichlorobenzene ug/kg ND 4.6 01/30/15 11:57
1,3-Dichloropropane ug/kg ND 4.6 01/30/15 11:57
1,4-Dichlorobenzene ug/kg ND 4.6 01/30/15 11:57
2,2-Dichloropropane ug/kg ND 4.6 01/30/15 11:57
2-Butanone (MEK)ug/kg ND 91.6 01/30/15 11:57
2-Chlorotoluene ug/kg ND 4.6 01/30/15 11:57
2-Hexanone ug/kg ND 45.8 01/30/15 11:57
4-Chlorotoluene ug/kg ND 4.6 01/30/15 11:57
4-Methyl-2-pentanone (MIBK)ug/kg ND 45.8 01/30/15 11:57
Acetone ug/kg ND 91.6 01/30/15 11:57
Benzene ug/kg ND 4.6 01/30/15 11:57
Bromobenzene ug/kg ND 4.6 01/30/15 11:57
Bromochloromethane ug/kg ND 4.6 01/30/15 11:57
Bromodichloromethane ug/kg ND 4.6 01/30/15 11:57
Bromoform ug/kg ND 4.6 01/30/15 11:57
Bromomethane ug/kg ND 9.2 01/30/15 11:57
Carbon tetrachloride ug/kg ND 4.6 01/30/15 11:57
Chlorobenzene ug/kg ND 4.6 01/30/15 11:57
Chloroethane ug/kg ND 9.2 01/30/15 11:57
Chloroform ug/kg ND 4.6 01/30/15 11:57
Chloromethane ug/kg ND 9.2 01/30/15 11:57
cis-1,2-Dichloroethene ug/kg ND 4.6 01/30/15 11:57
cis-1,3-Dichloropropene ug/kg ND 4.6 01/30/15 11:57
Dibromochloromethane ug/kg ND 4.6 01/30/15 11:57
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1381328
Associated Lab Samples:92234851001, 92234851002
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 4.6 01/30/15 11:57
Dichlorodifluoromethane ug/kg ND 9.2 01/30/15 11:57
Diisopropyl ether ug/kg ND 4.6 01/30/15 11:57
Ethylbenzene ug/kg ND 4.6 01/30/15 11:57
Hexachloro-1,3-butadiene ug/kg ND 4.6 01/30/15 11:57
Isopropylbenzene (Cumene)ug/kg ND 4.6 01/30/15 11:57
m&p-Xylene ug/kg ND 9.2 01/30/15 11:57
Methyl-tert-butyl ether ug/kg ND 4.6 01/30/15 11:57
Methylene Chloride ug/kg ND 18.3 01/30/15 11:57
n-Butylbenzene ug/kg ND 4.6 01/30/15 11:57
n-Propylbenzene ug/kg ND 4.6 01/30/15 11:57
Naphthalene ug/kg ND 4.6 01/30/15 11:57
o-Xylene ug/kg ND 4.6 01/30/15 11:57
p-Isopropyltoluene ug/kg ND 4.6 01/30/15 11:57
sec-Butylbenzene ug/kg ND 4.6 01/30/15 11:57
Styrene ug/kg ND 4.6 01/30/15 11:57
tert-Butylbenzene ug/kg ND 4.6 01/30/15 11:57
Tetrachloroethene ug/kg ND 4.6 01/30/15 11:57
Toluene ug/kg ND 4.6 01/30/15 11:57
trans-1,2-Dichloroethene ug/kg ND 4.6 01/30/15 11:57
trans-1,3-Dichloropropene ug/kg ND 4.6 01/30/15 11:57
Trichloroethene ug/kg ND 4.6 01/30/15 11:57
Trichlorofluoromethane ug/kg ND 4.6 01/30/15 11:57
Vinyl acetate ug/kg ND 45.8 01/30/15 11:57
Vinyl chloride ug/kg ND 9.2 01/30/15 11:57
Xylene (Total)ug/kg ND 9.2 01/30/15 11:57
1,2-Dichloroethane-d4 (S)%96 70-132 01/30/15 11:57
4-Bromofluorobenzene (S)%90 70-130 01/30/15 11:57
Toluene-d8 (S)%101 70-130 01/30/15 11:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1381329LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 49.350.5 98 74-137
1,1,1-Trichloroethane ug/kg 45.450.5 90 67-140
1,1,2,2-Tetrachloroethane ug/kg 49.250.5 97 72-141
1,1,2-Trichloroethane ug/kg 46.250.5 91 78-138
1,1-Dichloroethane ug/kg 52.050.5 103 69-134
1,1-Dichloroethene ug/kg 50.650.5 100 67-138
1,1-Dichloropropene ug/kg 49.450.5 98 69-139
1,2,3-Trichlorobenzene ug/kg 49.950.5 99 70-146
1,2,3-Trichloropropane ug/kg 49.750.5 98 69-144
1,2,4-Trichlorobenzene ug/kg 50.950.5 101 68-148
1,2,4-Trimethylbenzene ug/kg 52.850.5 105 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1381329LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 48.450.5 96 65-140
1,2-Dibromoethane (EDB)ug/kg 51.850.5 103 77-135
1,2-Dichlorobenzene ug/kg 49.950.5 99 77-141
1,2-Dichloroethane ug/kg 42.050.5 83 65-137
1,2-Dichloropropane ug/kg 47.250.5 93 72-136
1,3,5-Trimethylbenzene ug/kg 51.350.5 102 76-133
1,3-Dichlorobenzene ug/kg 50.350.5 100 74-138
1,3-Dichloropropane ug/kg 49.950.5 99 71-139
1,4-Dichlorobenzene ug/kg 52.350.5 103 76-138
2,2-Dichloropropane ug/kg 45.650.5 90 68-137
2-Butanone (MEK)ug/kg 84J101 83 58-147
2-Chlorotoluene ug/kg 47.350.5 94 73-139
2-Hexanone ug/kg 103101 102 62-145
4-Chlorotoluene ug/kg 50.350.5 100 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 96.8101 96 64-149
Acetone ug/kg 107101 106 53-153
Benzene ug/kg 49.350.5 98 73-135
Bromobenzene ug/kg 41.950.5 83 75-133
Bromochloromethane ug/kg 44.050.5 87 73-134
Bromodichloromethane ug/kg 42.050.5 83 71-135
Bromoform ug/kg 46.550.5 92 66-141
Bromomethane ug/kg 39.650.5 78 53-160
Carbon tetrachloride ug/kg 48.450.5 96 60-145
Chlorobenzene ug/kg 49.950.5 99 78-130
Chloroethane ug/kg 60.850.5 120 64-149
Chloroform ug/kg 41.650.5 82 70-134
Chloromethane ug/kg 44.050.5 87 52-150
cis-1,2-Dichloroethene ug/kg 45.950.5 91 70-133
cis-1,3-Dichloropropene ug/kg 46.550.5 92 68-134
Dibromochloromethane ug/kg 47.650.5 94 71-138
Dibromomethane ug/kg 45.050.5 89 74-130
Dichlorodifluoromethane ug/kg 47.550.5 94 40-160
Diisopropyl ether ug/kg 51.750.5 102 69-141
Ethylbenzene ug/kg 52.550.5 104 75-133
Hexachloro-1,3-butadiene ug/kg 48.950.5 97 68-143
Isopropylbenzene (Cumene)ug/kg 52.950.5 105 76-143
m&p-Xylene ug/kg 109101 107 75-136
Methyl-tert-butyl ether ug/kg 49.850.5 99 68-144
Methylene Chloride ug/kg 56.150.5 111 45-154
n-Butylbenzene ug/kg 54.350.5 108 72-137
n-Propylbenzene ug/kg 46.950.5 93 76-136
Naphthalene ug/kg 49.850.5 99 68-151
o-Xylene ug/kg 51.150.5 101 76-141
p-Isopropyltoluene ug/kg 53.650.5 106 76-140
sec-Butylbenzene ug/kg 49.050.5 97 79-139
Styrene ug/kg 51.650.5 102 79-137
tert-Butylbenzene ug/kg 45.950.5 91 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1381329LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 44.650.5 88 71-138
Toluene ug/kg 47.650.5 94 74-131
trans-1,2-Dichloroethene ug/kg 51.150.5 101 67-135
trans-1,3-Dichloropropene ug/kg 47.050.5 93 65-146
Trichloroethene ug/kg 48.050.5 95 67-135
Trichlorofluoromethane ug/kg 60.150.5 119 59-144
Vinyl acetate ug/kg 68.8 F3,IC1016840-160
Vinyl chloride ug/kg 44.150.5 87 56-141
Xylene (Total)ug/kg 160152 105 76-137
1,2-Dichloroethane-d4 (S)%96 70-132
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1382107MATRIX SPIKE SAMPLE:
MSSpike
Result
92235328001
1,1,1,2-Tetrachloroethane ug/kg 19.817.9 111 70-130ND
1,1,1-Trichloroethane ug/kg 17.617.9 98 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 29.4 M117.9 165 70-130ND
1,1,2-Trichloroethane ug/kg 25.6 M117.9 143 70-130ND
1,1-Dichloroethane ug/kg 24.0 M117.9 134 70-130ND
1,1-Dichloroethene ug/kg 21.017.9 117 49-180ND
1,1-Dichloropropene ug/kg 18.317.9 103 70-130ND
1,2,3-Trichlorobenzene ug/kg 23.4 M117.9 131 70-130ND
1,2,3-Trichloropropane ug/kg 27.7 M117.9 155 70-130ND
1,2,4-Trichlorobenzene ug/kg 20.517.9 115 70-130ND
1,2,4-Trimethylbenzene ug/kg 20.317.9 114 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 33.1 M117.9 186 70-130ND
1,2-Dibromoethane (EDB)ug/kg 26.7 M117.9 149 70-130ND
1,2-Dichlorobenzene ug/kg 22.317.9 125 70-130ND
1,2-Dichloroethane ug/kg 21.217.9 118 70-130ND
1,2-Dichloropropane ug/kg 20.217.9 113 70-130ND
1,3,5-Trimethylbenzene ug/kg 19.817.9 111 70-130ND
1,3-Dichlorobenzene ug/kg 20.017.9 112 70-130ND
1,3-Dichloropropane ug/kg 24.1 M117.9 135 70-130ND
1,4-Dichlorobenzene ug/kg 20.717.9 116 70-130ND
2,2-Dichloropropane ug/kg 17.917.9 100 70-130ND
2-Butanone (MEK)ug/kg 52.6J M135.7 147 70-130ND
2-Chlorotoluene ug/kg 18.617.9 104 70-130ND
2-Hexanone ug/kg 69.7 M135.7 195 70-130ND
4-Chlorotoluene ug/kg 19.717.9 110 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 68.0 M135.7 190 70-130ND
Acetone ug/kg 72J M135.7 200 70-130ND
Benzene ug/kg 19.517.9 109 50-166ND
Bromobenzene ug/kg 21.617.9 121 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1382107MATRIX SPIKE SAMPLE:
MSSpike
Result
92235328001
Bromochloromethane ug/kg 21.817.9 122 70-130ND
Bromodichloromethane ug/kg 18.617.9 104 70-130ND
Bromoform ug/kg 24.0 M117.9 134 70-130ND
Bromomethane ug/kg 18.317.9 102 70-130ND
Carbon tetrachloride ug/kg 18.017.9 101 70-130ND
Chlorobenzene ug/kg 19.217.9 107 43-169ND
Chloroethane ug/kg 24.1 M117.9 135 70-130ND
Chloroform ug/kg 18.017.9 101 70-130ND
Chloromethane ug/kg 16.917.9 95 70-130ND
cis-1,2-Dichloroethene ug/kg 19.617.9 110 70-130ND
cis-1,3-Dichloropropene ug/kg 20.417.9 114 70-130ND
Dibromochloromethane ug/kg 22.417.9 125 70-130ND
Dibromomethane ug/kg 23.4 M117.9 131 70-130ND
Dichlorodifluoromethane ug/kg 18.517.9 104 70-130ND
Diisopropyl ether ug/kg 26.9 M117.9 150 70-130ND
Ethylbenzene ug/kg 18.817.9 105 70-130ND
Hexachloro-1,3-butadiene ug/kg 18.417.9 103 70-130ND
Isopropylbenzene (Cumene)ug/kg 18.017.9 101 70-130ND
m&p-Xylene ug/kg 37.535.7 105 70-130ND
Methyl-tert-butyl ether ug/kg 30.0 M117.9 168 70-130ND
Methylene Chloride ug/kg 29.4 M117.9 165 70-130ND
n-Butylbenzene ug/kg 18.717.9 105 70-130ND
n-Propylbenzene ug/kg 18.417.9 103 70-130ND
Naphthalene ug/kg 31.0 M117.9 174 70-130ND
o-Xylene ug/kg 18.017.9 101 70-130ND
p-Isopropyltoluene ug/kg 19.317.9 108 70-130ND
sec-Butylbenzene ug/kg 18.317.9 103 70-130ND
Styrene ug/kg 18.317.9 103 70-130ND
tert-Butylbenzene ug/kg 17.817.9 100 70-130ND
Tetrachloroethene ug/kg 15.617.9 87 70-130ND
Toluene ug/kg 18.517.9 104 52-163ND
trans-1,2-Dichloroethene ug/kg 21.117.9 118 70-130ND
trans-1,3-Dichloropropene ug/kg 22.617.9 126 70-130ND
Trichloroethene ug/kg 17.717.9 99 49-167ND
Trichlorofluoromethane ug/kg 22.617.9 127 70-130ND
Vinyl acetate ug/kg 93.6 M135.7 262 70-130ND
Vinyl chloride ug/kg 16.817.9 94 70-130ND
1,2-Dichloroethane-d4 (S)%109 70-132
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92234911023
1382106SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92234911023
1382106SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg 10.5JND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92234911023
1382106SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%109 1105
4-Bromofluorobenzene (S)%96 397
Toluene-d8 (S)%102 099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/32540
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:92234851001, 92234851002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1378500
Associated Lab Samples:92234851001, 92234851002
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 01/29/15 16:25
1,2-Dichlorobenzene ug/kg ND 330 01/29/15 16:25
1,3-Dichlorobenzene ug/kg ND 330 01/29/15 16:25
1,4-Dichlorobenzene ug/kg ND 330 01/29/15 16:25
1-Methylnaphthalene ug/kg ND 330 01/29/15 16:25
2,4,5-Trichlorophenol ug/kg ND 330 01/29/15 16:25
2,4,6-Trichlorophenol ug/kg ND 330 01/29/15 16:25
2,4-Dichlorophenol ug/kg ND 330 01/29/15 16:25
2,4-Dimethylphenol ug/kg ND 330 01/29/15 16:25
2,4-Dinitrophenol ug/kg ND 1650 01/29/15 16:25
2,4-Dinitrotoluene ug/kg ND 330 01/29/15 16:25
2,6-Dinitrotoluene ug/kg ND 330 01/29/15 16:25
2-Chloronaphthalene ug/kg ND 330 01/29/15 16:25
2-Chlorophenol ug/kg ND 330 01/29/15 16:25
2-Methylnaphthalene ug/kg ND 330 01/29/15 16:25
2-Methylphenol(o-Cresol)ug/kg ND 330 01/29/15 16:25
2-Nitroaniline ug/kg ND 1650 01/29/15 16:25
2-Nitrophenol ug/kg ND 330 01/29/15 16:25
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 01/29/15 16:25
3,3'-Dichlorobenzidine ug/kg ND 1650 01/29/15 16:25
3-Nitroaniline ug/kg ND 1650 01/29/15 16:25
4,6-Dinitro-2-methylphenol ug/kg ND 660 01/29/15 16:25
4-Bromophenylphenyl ether ug/kg ND 330 01/29/15 16:25
4-Chloro-3-methylphenol ug/kg ND 660 01/29/15 16:25
4-Chloroaniline ug/kg ND 1650 01/29/15 16:25
4-Chlorophenylphenyl ether ug/kg ND 330 01/29/15 16:25
4-Nitroaniline ug/kg ND 660 01/29/15 16:25
4-Nitrophenol ug/kg ND 1650 01/29/15 16:25
Acenaphthene ug/kg ND 330 01/29/15 16:25
Acenaphthylene ug/kg ND 330 01/29/15 16:25
Aniline ug/kg ND 330 01/29/15 16:25
Anthracene ug/kg ND 330 01/29/15 16:25
Benzo(a)anthracene ug/kg ND 330 01/29/15 16:25
Benzo(a)pyrene ug/kg ND 330 01/29/15 16:25
Benzo(b)fluoranthene ug/kg ND 330 01/29/15 16:25
Benzo(g,h,i)perylene ug/kg ND 330 01/29/15 16:25
Benzo(k)fluoranthene ug/kg ND 330 01/29/15 16:25
Benzoic Acid ug/kg ND 1650 01/29/15 16:25
Benzyl alcohol ug/kg ND 660 01/29/15 16:25
bis(2-Chloroethoxy)methane ug/kg ND 330 01/29/15 16:25
bis(2-Chloroethyl) ether ug/kg ND 330 01/29/15 16:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1378500
Associated Lab Samples:92234851001, 92234851002
Matrix:Solid
Analyzed
bis(2-Chloroisopropyl) ether ug/kg ND 330 01/29/15 16:25
bis(2-Ethylhexyl)phthalate ug/kg ND 330 01/29/15 16:25
Butylbenzylphthalate ug/kg ND 330 01/29/15 16:25
Chrysene ug/kg ND 330 01/29/15 16:25
Di-n-butylphthalate ug/kg ND 330 01/29/15 16:25
Di-n-octylphthalate ug/kg ND 330 01/29/15 16:25
Dibenz(a,h)anthracene ug/kg ND 330 01/29/15 16:25
Dibenzofuran ug/kg ND 330 01/29/15 16:25
Diethylphthalate ug/kg ND 330 01/29/15 16:25
Dimethylphthalate ug/kg ND 330 01/29/15 16:25
Fluoranthene ug/kg ND 330 01/29/15 16:25
Fluorene ug/kg ND 330 01/29/15 16:25
Hexachloro-1,3-butadiene ug/kg ND 330 01/29/15 16:25
Hexachlorobenzene ug/kg ND 330 01/29/15 16:25
Hexachlorocyclopentadiene ug/kg ND 330 01/29/15 16:25
Hexachloroethane ug/kg ND 330 01/29/15 16:25
Indeno(1,2,3-cd)pyrene ug/kg ND 330 01/29/15 16:25
Isophorone ug/kg ND 330 01/29/15 16:25
N-Nitroso-di-n-propylamine ug/kg ND 330 01/29/15 16:25
N-Nitrosodimethylamine ug/kg ND 330 01/29/15 16:25
N-Nitrosodiphenylamine ug/kg ND 330 01/29/15 16:25
Naphthalene ug/kg ND 330 01/29/15 16:25
Nitrobenzene ug/kg ND 330 01/29/15 16:25
Pentachlorophenol ug/kg ND 1650 01/29/15 16:25
Phenanthrene ug/kg ND 330 01/29/15 16:25
Phenol ug/kg ND 330 01/29/15 16:25
Pyrene ug/kg ND 330 01/29/15 16:25
2,4,6-Tribromophenol (S)%91 27-110 01/29/15 16:25
2-Fluorobiphenyl (S)%80 30-110 01/29/15 16:25
2-Fluorophenol (S)%72 13-110 01/29/15 16:25
Nitrobenzene-d5 (S)%70 23-110 01/29/15 16:25
Phenol-d6 (S)%72 22-110 01/29/15 16:25
Terphenyl-d14 (S)%85 28-110 01/29/15 16:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1378501LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 14101670 85 36-120
1,2-Dichlorobenzene ug/kg 14001670 84 41-120
1,3-Dichlorobenzene ug/kg 13401670 80 66-120
1,4-Dichlorobenzene ug/kg 13501670 81 42-120
1-Methylnaphthalene ug/kg 14601670 88 40-120
2,4,5-Trichlorophenol ug/kg 14601670 88 37-120
2,4,6-Trichlorophenol ug/kg 14501670 87 40-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1378501LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dichlorophenol ug/kg 14801670 89 33-120
2,4-Dimethylphenol ug/kg 14001670 84 36-120
2,4-Dinitrophenol ug/kg 65008330 78 22-121
2,4-Dinitrotoluene ug/kg 16201670 97 60-120
2,6-Dinitrotoluene ug/kg 16301670 98 54-120
2-Chloronaphthalene ug/kg 14101670 84 41-120
2-Chlorophenol ug/kg 14201670 85 39-120
2-Methylnaphthalene ug/kg 13501670 81 26-120
2-Methylphenol(o-Cresol)ug/kg 13201670 79 41-120
2-Nitroaniline ug/kg 25403330 76 45-120
2-Nitrophenol ug/kg 14701670 88 35-120
3&4-Methylphenol(m&p Cresol)ug/kg 12901670 77 35-120
3,3'-Dichlorobenzidine ug/kg 28203330 85 16-125
3-Nitroaniline ug/kg 28403330 85 45-120
4,6-Dinitro-2-methylphenol ug/kg 31103330 93 46-120
4-Bromophenylphenyl ether ug/kg 16001670 96 36-120
4-Chloro-3-methylphenol ug/kg 29803330 89 37-120
4-Chloroaniline ug/kg 25603330 77 35-120
4-Chlorophenylphenyl ether ug/kg 15601670 94 30-120
4-Nitroaniline ug/kg 30603330 92 48-120
4-Nitrophenol ug/kg 75908330 91 43-120
Acenaphthene ug/kg 14301670 86 46-120
Acenaphthylene ug/kg 14601670 88 46-120
Aniline ug/kg 11401670 68 33-120
Anthracene ug/kg 14701670 88 63-120
Benzo(a)anthracene ug/kg 15101670 91 61-120
Benzo(a)pyrene ug/kg 15601670 93 59-120
Benzo(b)fluoranthene ug/kg 14501670 87 55-120
Benzo(g,h,i)perylene ug/kg 14701670 88 57-120
Benzo(k)fluoranthene ug/kg 13801670 83 56-120
Benzoic Acid ug/kg 51208330 61 13-120
Benzyl alcohol ug/kg 27703330 83 34-120
bis(2-Chloroethoxy)methane ug/kg 12901670 77 21-120
bis(2-Chloroethyl) ether ug/kg 12701670 76 25-120
bis(2-Chloroisopropyl) ether ug/kg 9351670 56 13-120
bis(2-Ethylhexyl)phthalate ug/kg 16901670 102 56-123
Butylbenzylphthalate ug/kg 16601670 100 57-120
Chrysene ug/kg 15201670 91 64-120
Di-n-butylphthalate ug/kg 16601670 100 58-120
Di-n-octylphthalate ug/kg 16301670 98 47-121
Dibenz(a,h)anthracene ug/kg 15901670 95 56-120
Dibenzofuran ug/kg 15301670 92 43-120
Diethylphthalate ug/kg 16101670 96 55-120
Dimethylphthalate ug/kg 15301670 92 54-120
Fluoranthene ug/kg 16101670 96 61-120
Fluorene ug/kg 15601670 94 51-120
Hexachloro-1,3-butadiene ug/kg 15301670 92 22-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1378501LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 16201670 97 53-120
Hexachlorocyclopentadiene ug/kg 14701670 88 18-150
Hexachloroethane ug/kg 13601670 82 39-120
Indeno(1,2,3-cd)pyrene ug/kg 16301670 98 58-120
Isophorone ug/kg 13101670 78 38-120
N-Nitroso-di-n-propylamine ug/kg 12101670 73 30-120
N-Nitrosodimethylamine ug/kg 11401670 69 32-120
N-Nitrosodiphenylamine ug/kg 14901670 89 50-120
Naphthalene ug/kg 14001670 84 38-120
Nitrobenzene ug/kg 12801670 77 37-120
Pentachlorophenol ug/kg 31103330 93 10-120
Phenanthrene ug/kg 14501670 87 62-120
Phenol ug/kg 13701670 82 37-120
Pyrene ug/kg 14101670 85 63-120
2,4,6-Tribromophenol (S)%104 27-110
2-Fluorobiphenyl (S)%85 30-110
2-Fluorophenol (S)%82 13-110
Nitrobenzene-d5 (S)%74 23-110
Phenol-d6 (S)%81 22-110
Terphenyl-d14 (S)%88 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1378502MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92233871003
1378503
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 2010 57 18-11956 22010ND11501120
1,2-Dichlorobenzene ug/kg 2010 58 50-11063 82010ND11601260
1,3-Dichlorobenzene ug/kg 2010 55 27-11056 12010ND11001120
1,4-Dichlorobenzene ug/kg 2010 55 28-11056 12010ND11101120
1-Methylnaphthalene ug/kg 2010 60 24-11669 142010ND12001380
2,4,5-Trichlorophenol ug/kg 2010 69 28-11067 32010ND13901350
2,4,6-Trichlorophenol ug/kg 2010 64 17-11754 162010ND12801090
2,4-Dichlorophenol ug/kg 2010 56 21-12859 52010ND11301180
2,4-Dimethylphenol ug/kg R120102810-12020 352010ND570399
2,4-Dinitrophenol ug/kg 10000 73 10-10756 2610000ND72805590
2,4-Dinitrotoluene ug/kg 2010 90 36-10989 02010ND18001800
2,6-Dinitrotoluene ug/kg 2010 89 32-11081 92010ND17801630
2-Chloronaphthalene ug/kg 2010 61 30-10757 72010ND12201140
2-Chlorophenol ug/kg 2010 54 14-10655 32010ND10801110
2-Methylnaphthalene ug/kg 2010 54 10-13560 102010ND10901200
2-Methylphenol(o-Cresol)ug/kg 2010 37 10-12436 32010ND749728
2-Nitroaniline ug/kg 4010 67 26-11663 84010ND27102510
2-Nitrophenol ug/kg 2010 60 28-10349 212010ND1210987
3&4-Methylphenol(m&p
Cresol)ug/kg 2010 39 10-10940 42010ND775806
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1378502MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92233871003
1378503
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
3,3'-Dichlorobenzidine ug/kg 4010 65 10-15053 204010ND26102130
3-Nitroaniline ug/kg 4010 78 22-11082 54010ND31503300
4,6-Dinitro-2-methylphenol ug/kg R140109013-12159 414010ND36202380
4-Bromophenylphenyl ether ug/kg 2010 78 31-10971 92010ND15701430
4-Chloro-3-methylphenol ug/kg 4010 61 13-12868 124010ND24502750
4-Chloroaniline ug/kg 4010 54 18-10261 124010ND21702460
4-Chlorophenylphenyl ether ug/kg 2010 75 29-11269 72010ND15001400
4-Nitroaniline ug/kg 4010 87 16-11195 84010ND35203810
4-Nitrophenol ug/kg 10000 87 14-13578 1110000ND87407860
Acenaphthene ug/kg 2010 66 26-11462 62010ND13301250
Acenaphthylene ug/kg 2010 68 32-10863 92010ND13701260
Aniline ug/kg 2010 36 10-10734 52010ND729693
Anthracene ug/kg 2010 77 32-11172 62010ND15401450
Benzo(a)anthracene ug/kg 2010 76 25-11767 132010ND15301350
Benzo(a)pyrene ug/kg 2010 78 25-10672 82010ND15701440
Benzo(b)fluoranthene ug/kg 2010 77 24-11064 182010ND15501290
Benzo(g,h,i)perylene ug/kg 2010 75 19-11261 202010ND15001230
Benzo(k)fluoranthene ug/kg 2010 68 24-11466 22010ND13701330
Benzoic Acid ug/kg 10000 11 10-1101110000ND1110J1070J
Benzyl alcohol ug/kg 4010 57 24-10662 94010ND22902500
bis(2-Chloroethoxy)methane ug/kg 2010 52 13-11946 122010ND1050933
bis(2-Chloroethyl) ether ug/kg 2010 51 10-13452 12010ND10301040
bis(2-Chloroisopropyl) ether ug/kg 2010 39 10-11349 242010ND777994
bis(2-Ethylhexyl)phthalate ug/kg 2010 84 10-12564 272010ND16801280
Butylbenzylphthalate ug/kg 2010 84 18-11069 192010ND16801390
Chrysene ug/kg 2010 77 30-11073 52010ND15501480
Di-n-butylphthalate ug/kg 2010 85 19-11275 132010ND17101500
Di-n-octylphthalate ug/kg 2010 84 17-10580 42010ND16801620
Dibenz(a,h)anthracene ug/kg 2010 80 23-11169 142010ND16101400
Dibenzofuran ug/kg 2010 74 35-10369 72010ND14801380
Diethylphthalate ug/kg 2010 86 27-11378 102010ND17301570
Dimethylphthalate ug/kg 2010 81 26-11174 92010ND16401490
Fluoranthene ug/kg 2010 84 33-10980 52010ND16901610
Fluorene ug/kg 2010 78 32-11376 12010ND15601530
Hexachloro-1,3-butadiene ug/kg 2010 58 16-11651 142010ND11701020
Hexachlorobenzene ug/kg 2010 82 27-12075 92010ND16501510
Hexachlorocyclopentadiene ug/kg M020105910-10802010ND1180ND
Hexachloroethane ug/kg R120105410-11736 402010ND1090727
Indeno(1,2,3-cd)pyrene ug/kg 2010 83 10-12271 162010ND16801420
Isophorone ug/kg 2010 55 28-11452 62010ND11101040
N-Nitroso-di-n-propylamine ug/kg 2010 51 27-11363 212010ND10201260
N-Nitrosodimethylamine ug/kg 2010 46 10-10936 262010ND931714
N-Nitrosodiphenylamine ug/kg 2010 75 10-12864 162010ND15101280
Naphthalene ug/kg 2010 58 25-11056 22010ND11601130
Nitrobenzene ug/kg 2010 54 18-11446 152010ND1080924
Pentachlorophenol ug/kg 4010 84 10-12263 304010ND33902520
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1378502MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92233871003
1378503
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenanthrene ug/kg 2010 76 30-11471 62010ND15301430
Phenol ug/kg 2010 48 11-10249 22010ND962977
Pyrene ug/kg 2010 72 25-11664 122010ND14501290
2,4,6-Tribromophenol (S)%75 27-11061
2-Fluorobiphenyl (S)%57 30-11046
2-Fluorophenol (S)%44 13-11034
Nitrobenzene-d5 (S)%50 23-11043
Phenol-d6 (S)%46 22-11047
Terphenyl-d14 (S)%69 28-11063
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/32545
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92234851003, 92234851004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1378668
Associated Lab Samples:92234851003, 92234851004
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 01/29/15 11:15
1,2-Dichlorobenzene ug/L ND 10.0 01/29/15 11:15
1,3-Dichlorobenzene ug/L ND 10.0 01/29/15 11:15
1,4-Dichlorobenzene ug/L ND 10.0 01/29/15 11:15
1-Methylnaphthalene ug/L ND 10.0 01/29/15 11:15
2,4,5-Trichlorophenol ug/L ND 10.0 01/29/15 11:15
2,4,6-Trichlorophenol ug/L ND 10.0 01/29/15 11:15
2,4-Dichlorophenol ug/L ND 10.0 01/29/15 11:15
2,4-Dimethylphenol ug/L ND 10.0 01/29/15 11:15
2,4-Dinitrophenol ug/L ND 50.0 01/29/15 11:15
2,4-Dinitrotoluene ug/L ND 10.0 01/29/15 11:15
2,6-Dinitrotoluene ug/L ND 10.0 01/29/15 11:15
2-Chloronaphthalene ug/L ND 10.0 01/29/15 11:15
2-Chlorophenol ug/L ND 10.0 01/29/15 11:15
2-Methylnaphthalene ug/L ND 10.0 01/29/15 11:15
2-Methylphenol(o-Cresol)ug/L ND 10.0 01/29/15 11:15
2-Nitroaniline ug/L ND 50.0 01/29/15 11:15
2-Nitrophenol ug/L ND 10.0 01/29/15 11:15
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 01/29/15 11:15
3,3'-Dichlorobenzidine ug/L ND 20.0 01/29/15 11:15
3-Nitroaniline ug/L ND 50.0 01/29/15 11:15
4,6-Dinitro-2-methylphenol ug/L ND 20.0 01/29/15 11:15
4-Bromophenylphenyl ether ug/L ND 10.0 01/29/15 11:15
4-Chloro-3-methylphenol ug/L ND 20.0 01/29/15 11:15
4-Chloroaniline ug/L ND 20.0 01/29/15 11:15
4-Chlorophenylphenyl ether ug/L ND 10.0 01/29/15 11:15
4-Nitroaniline ug/L ND 20.0 01/29/15 11:15
4-Nitrophenol ug/L ND 50.0 01/29/15 11:15
Acenaphthene ug/L ND 10.0 01/29/15 11:15
Acenaphthylene ug/L ND 10.0 01/29/15 11:15
Aniline ug/L ND 10.0 01/29/15 11:15
Anthracene ug/L ND 10.0 01/29/15 11:15
Benzo(a)anthracene ug/L ND 10.0 01/29/15 11:15
Benzo(a)pyrene ug/L ND 10.0 01/29/15 11:15
Benzo(b)fluoranthene ug/L ND 10.0 01/29/15 11:15
Benzo(g,h,i)perylene ug/L ND 10.0 01/29/15 11:15
Benzo(k)fluoranthene ug/L ND 10.0 01/29/15 11:15
Benzoic Acid ug/L ND 50.0 01/29/15 11:15
Benzyl alcohol ug/L ND 20.0 01/29/15 11:15
bis(2-Chloroethoxy)methane ug/L ND 10.0 01/29/15 11:15
bis(2-Chloroethyl) ether ug/L ND 10.0 01/29/15 11:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1378668
Associated Lab Samples:92234851003, 92234851004
Matrix:Water
Analyzed
bis(2-Chloroisopropyl) ether ug/L ND 10.0 01/29/15 11:15
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 01/29/15 11:15
Butylbenzylphthalate ug/L ND 10.0 01/29/15 11:15
Chrysene ug/L ND 10.0 01/29/15 11:15
Di-n-butylphthalate ug/L ND 10.0 01/29/15 11:15
Di-n-octylphthalate ug/L ND 10.0 01/29/15 11:15
Dibenz(a,h)anthracene ug/L ND 10.0 01/29/15 11:15
Dibenzofuran ug/L ND 10.0 01/29/15 11:15
Diethylphthalate ug/L ND 10.0 01/29/15 11:15
Dimethylphthalate ug/L ND 10.0 01/29/15 11:15
Fluoranthene ug/L ND 10.0 01/29/15 11:15
Fluorene ug/L ND 10.0 01/29/15 11:15
Hexachloro-1,3-butadiene ug/L ND 10.0 01/29/15 11:15
Hexachlorobenzene ug/L ND 10.0 01/29/15 11:15
Hexachlorocyclopentadiene ug/L ND 10.0 01/29/15 11:15
Hexachloroethane ug/L ND 10.0 01/29/15 11:15
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 01/29/15 11:15
Isophorone ug/L ND 10.0 01/29/15 11:15
N-Nitroso-di-n-propylamine ug/L ND 10.0 01/29/15 11:15
N-Nitrosodimethylamine ug/L ND 10.0 01/29/15 11:15
N-Nitrosodiphenylamine ug/L ND 10.0 01/29/15 11:15
Naphthalene ug/L ND 10.0 01/29/15 11:15
Nitrobenzene ug/L ND 10.0 01/29/15 11:15
Pentachlorophenol ug/L ND 25.0 01/29/15 11:15
Phenanthrene ug/L ND 10.0 01/29/15 11:15
Phenol ug/L ND 10.0 01/29/15 11:15
Pyrene ug/L ND 10.0 01/29/15 11:15
2,4,6-Tribromophenol (S)%51 27-110 01/29/15 11:15
2-Fluorobiphenyl (S)%42 27-110 01/29/15 11:15
2-Fluorophenol (S)%22 12-110 01/29/15 11:15
Nitrobenzene-d5 (S)%39 21-110 01/29/15 11:15
Phenol-d6 (S)%14 10-110 01/29/15 11:15
Terphenyl-d14 (S)%56 31-107 01/29/15 11:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1378669LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1379095
1,2,4-Trichlorobenzene ug/L 19.550 39 31-1203517.6 10 30
1,2-Dichlorobenzene ug/L 21.650 43 38-1203819.1 12 30
1,3-Dichlorobenzene ug/L 20.650 41 30-1223618.2 12 30
1,4-Dichlorobenzene ug/L 21.250 42 37-1203718.4 14 30
1-Methylnaphthalene ug/L 20.350 41 34-1133919.5 4 30
2,4,5-Trichlorophenol ug/L 30.750 61 43-1135326.5 15 30
2,4,6-Trichlorophenol ug/L 26.050 52 42-1204723.7 9 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1378669LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1379095
2,4-Dichlorophenol ug/L 19.350 39 30-1203819.0 2 30
2,4-Dimethylphenol ug/L 17.850 36 29-1113617.8 0 30
2,4-Dinitrophenol ug/L 163250 65 19-13255139 16 30
2,4-Dinitrotoluene ug/L 40.550 81 58-1286632.8 21 30
2,6-Dinitrotoluene ug/L 39.050 78 54-1296432.2 19 30
2-Chloronaphthalene ug/L 25.450 51 43-1174824.0 6 30
2-Chlorophenol ug/L 19.7 L2503937-1203618.1 9 30
2-Methylnaphthalene ug/L 18.550 37 33-1203617.8 4 30
2-Methylphenol(o-Cresol)ug/L 15.4 L2503131-1203014.8 4 30
2-Nitroaniline ug/L 56.6100 57 48-1214848.4J 30
2-Nitrophenol ug/L 20.550 41 25-1163919.5 5 30
3&4-Methylphenol(m&p Cresol)ug/L 13.250 26 23-1202713.3 0 30
3,3'-Dichlorobenzidine ug/L 75.9100 76 10-1546060.1 23 30
3-Nitroaniline ug/L 72.2100 72 43-1156059.6 19 30
4,6-Dinitro-2-methylphenol ug/L 78.2100 78 44-1246363.0 22 30
4-Bromophenylphenyl ether ug/L 37.450 75 34-1136030.2 21 30
4-Chloro-3-methylphenol ug/L 48.0100 48 31-1104242.1 13 30
4-Chloroaniline ug/L 39.4100 39 20-1203838.4 3 30
4-Chlorophenylphenyl ether ug/L 32.950 66 34-1165628.2 15 30
4-Nitroaniline ug/L 78.7100 79 46-1286463.5 21 30
4-Nitrophenol ug/L 82.7250 33 11-1202869.8 17 30
Acenaphthene ug/L 26.650 53 48-1144823.9 11 30
Acenaphthylene ug/L 26.950 54 48-1124924.4 10 30
Aniline ug/L 16.150 32 26-1203015.1 7 30
Anthracene ug/L 37.350 75 57-1185929.7 23 30
Benzo(a)anthracene ug/L 37.350 75 56-1215929.6 23 30
Benzo(a)pyrene ug/L 40.950 82 55-1276231.2 27 30
Benzo(b)fluoranthene ug/L 40.750 81 53-1286331.7 25 30
Benzo(g,h,i)perylene ug/L 38.350 77 54-1255929.7 25 30
Benzo(k)fluoranthene ug/L 37.5 R1507551-1235527.6 31 30
Benzoic Acid ug/L 38.2J250 15 10-1201536.4J 30
Benzyl alcohol ug/L 35.2100 35 27-1203333.5 5 30
bis(2-Chloroethoxy)methane ug/L 22.850 46 32-1204321.6 5 30
bis(2-Chloroethyl) ether ug/L 20.450 41 33-1113819.1 6 30
bis(2-Chloroisopropyl) ether ug/L 14.850 30 15-1202713.5 9 30
bis(2-Ethylhexyl)phthalate ug/L 41.050 82 50-1456431.9 25 30
Butylbenzylphthalate ug/L 41.350 83 54-1386532.5 24 30
Chrysene ug/L 38.050 76 58-1276029.9 24 30
Di-n-butylphthalate ug/L 41.550 83 56-1256432.1 25 30
Di-n-octylphthalate ug/L 38.850 78 50-1346532.3 18 30
Dibenz(a,h)anthracene ug/L 39.850 80 53-1296431.8 22 30
Dibenzofuran ug/L 30.750 61 45-1205427.1 13 30
Diethylphthalate ug/L 38.850 78 53-1206331.5 21 30
Dimethylphthalate ug/L 35.650 71 55-1165929.4 19 30
Fluoranthene ug/L 40.850 82 57-1256331.7 25 30
Fluorene ug/L 34.650 69 53-1185829.1 17 30
Hexachloro-1,3-butadiene ug/L 19.450 39 23-1203517.6 9 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1378669LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1379095
Hexachlorobenzene ug/L 38.150 76 49-1166130.5 22 30
Hexachlorocyclopentadiene ug/L 20.050 40 26-1583919.5 2 30
Hexachloroethane ug/L 22.350 45 30-1144020.1 11 30
Indeno(1,2,3-cd)pyrene ug/L 42.650 85 55-1286733.3 25 30
Isophorone ug/L 17.450 35 31-1183417.0 3 30
N-Nitroso-di-n-propylamine ug/L 18.750 37 32-1193517.6 6 30
N-Nitrosodimethylamine ug/L 13.150 26 13-1202311.4 14 30
N-Nitrosodiphenylamine ug/L 35.450 71 43-1205728.4 22 30
Naphthalene ug/L 19.750 39 32-1203618.1 8 30
Nitrobenzene ug/L 18.550 37 33-1103417.2 7 30
Pentachlorophenol ug/L 70.1100 70 10-1375656.5 21 30
Phenanthrene ug/L 36.450 73 57-1175828.8 23 30
Phenol ug/L ND50 20 10-120199.4J 30
Pyrene ug/L 35.450 71 55-1225627.9 24 30
2,4,6-Tribromophenol (S)%80 27-11065
2-Fluorobiphenyl (S)%44 27-11042
2-Fluorophenol (S)%24 12-11022
Nitrobenzene-d5 (S)%36 21-11034
Phenol-d6 (S)%16 10-11016
Terphenyl-d14 (S)%73 31-10757
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/7471
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92234851001, 92234851002
Parameter Units
Dup
Result QualifiersRPDResult
92234851001
1380059SAMPLE DUPLICATE:
Percent Moisture %23.2 724.9
Parameter Units
Dup
Result QualifiersRPDResult
92235131002
1380060SAMPLE DUPLICATE:
Percent Moisture %17.3 117.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 43
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The internal standard response is below criteria. No hits associated with this internal standard. Results unaffected by
high bias.1g
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
The initial calibration for this compound was outside of method control limits. The result is estimated.IC
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 43
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92234851
Gussman Cleaners 22171
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92234851001 OEXT/32540 MSSV/10237B-1 EPA 3546 EPA 8270
92234851002 OEXT/32540 MSSV/10237B-2 EPA 3546 EPA 8270
92234851003 OEXT/32545 MSSV/10240TW-1 EPA 3510 EPA 8270
92234851004 OEXT/32545 MSSV/10240TW-2 EPA 3510 EPA 8270
92234851003 MSV/30201TW-1 EPA 8260
92234851004 MSV/30201TW-2 EPA 8260
92234851001 MSV/30175B-1 EPA 8260
92234851002 MSV/30175B-2 EPA 8260
92234851001 PMST/7471B-1 ASTM D2974-87
92234851002 PMST/7471B-2 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2015 09:52 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 43
Page 42 of 43
Page 43 of 43
#=CL#
January 30, 2015
LIMS USE: FR - AMY CONCHAS
LIMS OBJECT ID: 92234909
92234909
Project:
Pace Project No.:
RE:
Amy Conchas
ECS
6714 Netherlands Drive
Wilmington, NC 28405
GUSSMAN CLEANERS 22.22171
Dear Amy Conchas:
Enclosed are the analytical results for sample(s) received by the laboratory on January 26, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
Enclosures
cc:Ms. Amy Conchas, ECS
Brooks Wall, ECS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 17
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92234909
GUSSMAN CLEANERS 22.22171
Minnesota Certification IDs1700 Elm Street SE Suite 200, Minneapolis, MN 55414A2LA Certification #: 2926.01
Alaska Certification #: UST-078Alaska Certification #MN00064Alabama Certification #40770Arizona Certification #: AZ-0014Arkansas Certification #: 88-0680
California Certification #: 01155CAColorado Certification #PaceConnecticut Certification #: PH-0256EPA Region 8 Certification #: 8TMS-LFlorida/NELAP Certification #: E87605
Guam Certification #:14-008rGeorgia Certification #: 959Georgia EPD #: PaceIdaho Certification #: MN00064Hawaii Certification #MN00064
Illinois Certification #: 200011Indiana Certification#C-MN-01Iowa Certification #: 368Kansas Certification #: E-10167Kentucky Dept of Envi. Protection - DW #90062
Kentucky Dept of Envi. Protection - WW #:90062Louisiana DEQ Certification #: 3086Louisiana DHH #: LA140001Maine Certification #: 2013011Maryland Certification #: 322
Michigan DEPH Certification #: 9909
Minnesota Certification #: 027-053-137Mississippi Certification #: Pace
Montana Certification #: MT0092Nevada Certification #: MN_00064Nebraska Certification #: PaceNew Jersey Certification #: MN-002New York Certification #: 11647
North Carolina Certification #: 530North Carolina State Public Health #: 27700North Dakota Certification #: R-036Ohio EPA #: 4150Ohio VAP Certification #: CL101
Oklahoma Certification #: 9507Oregon Certification #: MN200001Oregon Certification #: MN300001Pennsylvania Certification #: 68-00563Puerto Rico Certification
Saipan (CNMI) #:MP0003South Carolina #:74003001Texas Certification #: T104704192Tennessee Certification #: 02818Utah Certification #: MN000642013-4
Virginia DGS Certification #: 251Virginia/VELAP Certification #: PaceWashington Certification #: C486West Virginia Certification #: 382West Virginia DHHR #:9952C
Wisconsin Certification #: 999407970
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 17
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92234909
GUSSMAN CLEANERS 22.22171
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92234909001 SG-1 TO-15 58 PASI-MMJL
92234909002 SG-2 TO-15 58 PASI-MMJL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 17
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92234909
GUSSMAN CLEANERS 22.22171
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92234909001 SG-1
Acetone 34.0 ug/m3 01/27/15 22:443.9TO-15
Benzene 5.7 ug/m3 01/27/15 22:440.52TO-15
2-Butanone (MEK)14.1 ug/m3 01/27/15 22:440.97TO-15
Dichlorodifluoromethane 3.3 ug/m3 01/27/15 22:441.6TO-15
Ethylbenzene 3.4 ug/m3 01/27/15 22:441.4TO-15
4-Ethyltoluene 2.4 ug/m3 01/27/15 22:441.6TO-15
n-Heptane 5.0 ug/m3 01/27/15 22:441.3TO-15
n-Hexane 11.4 ug/m3 01/27/15 22:441.2TO-15
2-Hexanone 1.7 ug/m3 01/27/15 22:441.3TO-15
Methylene Chloride 7.0 ug/m3 01/27/15 22:445.7TO-15
Propylene 9.6 ug/m3 01/27/15 22:440.56TO-15
Tetrachloroethene 3.3 ug/m3 01/27/15 22:441.1TO-15
Tetrahydrofuran 10.9 ug/m3 01/27/15 22:440.97TO-15
Toluene 14.5 ug/m3 01/27/15 22:441.2TO-15
1,2,4-Trimethylbenzene 9.4 ug/m3 01/27/15 22:441.6TO-15
1,3,5-Trimethylbenzene 2.5 ug/m3 01/27/15 22:441.6TO-15
m&p-Xylene 12.7 ug/m3 01/27/15 22:442.8TO-15
o-Xylene 5.9 ug/m3 01/27/15 22:441.4TO-15
92234909002 SG-2
Acetone 30.1 ug/m3 01/27/15 21:464.6TO-15
Benzene 1.6 ug/m3 01/27/15 21:460.62TO-15
2-Butanone (MEK)9.0 ug/m3 01/27/15 21:461.2TO-15
Dichlorodifluoromethane 3.0 ug/m3 01/27/15 21:461.9TO-15
Ethyl acetate 9.1 ug/m3 01/27/15 21:461.4TO-15
4-Ethyltoluene 2.2 ug/m3 01/27/15 21:461.9TO-15
n-Heptane 3.8 ug/m3 01/27/15 21:461.6TO-15
n-Hexane 29.6 ug/m3 01/27/15 21:461.4TO-15
Methylene Chloride 33.7 ug/m3 01/27/15 21:466.8TO-15
Propylene 7.1 ug/m3 01/27/15 21:460.67TO-15
Tetrachloroethene 3.2 ug/m3 01/27/15 21:461.3TO-15
Toluene 7.8 ug/m3 01/27/15 21:461.5TO-15
1,2,4-Trimethylbenzene 8.3 ug/m3 01/27/15 21:461.9TO-15
1,3,5-Trimethylbenzene 2.1 ug/m3 01/27/15 21:461.9TO-15
m&p-Xylene 6.0 ug/m3 01/27/15 21:463.4TO-15
o-Xylene 3.1 ug/m3 01/27/15 21:461.7TO-15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92234909
GUSSMAN CLEANERS 22.22171
Sample:SG-1 Lab ID:92234909001 Collected:01/22/15 15:20 Received:01/26/15 09:20 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 34.0 ug/m3 01/27/15 22:44 67-64-13.9 1.61
Benzene 5.7 ug/m3 01/27/15 22:44 71-43-20.52 1.61
Bromodichloromethane ND ug/m3 01/27/15 22:44 75-27-42.2 1.61
Bromoform ND ug/m3 01/27/15 22:44 75-25-23.4 1.61
Bromomethane ND ug/m3 01/27/15 22:44 74-83-93.2 1.61
1,3-Butadiene ND ug/m3 01/27/15 22:44 106-99-00.72 1.61
2-Butanone (MEK)14.1 ug/m3 01/27/15 22:44 78-93-30.97 1.61
Carbon disulfide ND ug/m3 01/27/15 22:44 75-15-01.0 1.61
Carbon tetrachloride ND ug/m3 01/27/15 22:44 56-23-51.0 1.61
Chlorobenzene ND ug/m3 01/27/15 22:44 108-90-71.5 1.61
Chloroethane ND ug/m3 01/27/15 22:44 75-00-30.87 1.61
Chloroform ND ug/m3 01/27/15 22:44 67-66-30.80 1.61
Chloromethane ND ug/m3 01/27/15 22:44 74-87-31.7 1.61
Cyclohexane ND ug/m3 01/27/15 22:44 110-82-71.1 1.61
Dibromochloromethane ND ug/m3 01/27/15 22:44 124-48-12.8 1.61
1,2-Dibromoethane (EDB)ND ug/m3 01/27/15 22:44 106-93-42.5 1.61
1,2-Dichlorobenzene ND ug/m3 01/27/15 22:44 95-50-12.0 1.61
1,3-Dichlorobenzene ND ug/m3 01/27/15 22:44 541-73-12.0 1.61
1,4-Dichlorobenzene ND ug/m3 01/27/15 22:44 106-46-72.0 1.61
Dichlorodifluoromethane 3.3 ug/m3 01/27/15 22:44 75-71-81.6 1.61
1,1-Dichloroethane ND ug/m3 01/27/15 22:44 75-34-31.3 1.61
1,2-Dichloroethane ND ug/m3 01/27/15 22:44 107-06-20.66 1.61
1,1-Dichloroethene ND ug/m3 01/27/15 22:44 75-35-41.3 1.61
cis-1,2-Dichloroethene ND ug/m3 01/27/15 22:44 156-59-23.2 1.61
trans-1,2-Dichloroethene ND ug/m3 01/27/15 22:44 156-60-51.3 1.61
1,2-Dichloropropane ND ug/m3 01/27/15 22:44 78-87-51.5 1.61
cis-1,3-Dichloropropene ND ug/m3 01/27/15 22:44 10061-01-51.5 1.61
trans-1,3-Dichloropropene ND ug/m3 01/27/15 22:44 10061-02-61.5 1.61
Dichlorotetrafluoroethane ND ug/m3 01/27/15 22:44 76-14-22.3 1.61
Ethyl acetate ND ug/m3 01/27/15 22:44 141-78-61.2 1.61
Ethylbenzene 3.4 ug/m3 01/27/15 22:44 100-41-41.4 1.61
4-Ethyltoluene 2.4 ug/m3 01/27/15 22:44 622-96-81.6 1.61
n-Heptane 5.0 ug/m3 01/27/15 22:44 142-82-51.3 1.61
Hexachloro-1,3-butadiene ND ug/m3 01/27/15 22:44 87-68-33.5 1.61
n-Hexane 11.4 ug/m3 01/27/15 22:44 110-54-31.2 1.61
2-Hexanone 1.7 ug/m3 01/27/15 22:44 591-78-61.3 1.61
Methylene Chloride 7.0 ug/m3 01/27/15 22:44 75-09-25.7 1.61
4-Methyl-2-pentanone (MIBK)ND ug/m3 01/27/15 22:44 108-10-13.4 1.61
Methyl-tert-butyl ether ND ug/m3 01/27/15 22:44 1634-04-41.2 1.61
Naphthalene ND ug/m3 01/27/15 22:44 91-20-34.3 1.61
Propylene 9.6 ug/m3 01/27/15 22:44 115-07-10.56 1.61
Styrene ND ug/m3 01/27/15 22:44 100-42-51.4 1.61
1,1,2,2-Tetrachloroethane ND ug/m3 01/27/15 22:44 79-34-51.1 1.61
Tetrachloroethene 3.3 ug/m3 01/27/15 22:44 127-18-41.1 1.61
Tetrahydrofuran 10.9 ug/m3 01/27/15 22:44 109-99-90.97 1.61
Toluene 14.5 ug/m3 01/27/15 22:44 108-88-31.2 1.61
1,2,4-Trichlorobenzene ND ug/m3 01/27/15 22:44 120-82-12.4 1.61
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/30/2015 07:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92234909
GUSSMAN CLEANERS 22.22171
Sample:SG-1 Lab ID:92234909001 Collected:01/22/15 15:20 Received:01/26/15 09:20 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 01/27/15 22:44 71-55-61.1 1.61
1,1,2-Trichloroethane ND ug/m3 01/27/15 22:44 79-00-50.89 1.61
Trichloroethene ND ug/m3 01/27/15 22:44 79-01-60.88 1.61
Trichlorofluoromethane ND ug/m3 01/27/15 22:44 75-69-41.8 1.61
1,1,2-Trichlorotrifluoroethane ND ug/m3 01/27/15 22:44 76-13-12.6 1.61
1,2,4-Trimethylbenzene 9.4 ug/m3 01/27/15 22:44 95-63-61.6 1.61
1,3,5-Trimethylbenzene 2.5 ug/m3 01/27/15 22:44 108-67-81.6 1.61
Vinyl acetate ND ug/m3 01/27/15 22:44 108-05-41.2 1.61
Vinyl chloride ND ug/m3 01/27/15 22:44 75-01-40.42 1.61
m&p-Xylene 12.7 ug/m3 01/27/15 22:44 179601-23-12.8 1.61
o-Xylene 5.9 ug/m3 01/27/15 22:44 95-47-61.4 1.61
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/30/2015 07:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92234909
GUSSMAN CLEANERS 22.22171
Sample:SG-2 Lab ID:92234909002 Collected:01/22/15 16:10 Received:01/26/15 09:20 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 30.1 ug/m3 01/27/15 21:46 67-64-14.6 1.92
Benzene 1.6 ug/m3 01/27/15 21:46 71-43-20.62 1.92
Bromodichloromethane ND ug/m3 01/27/15 21:46 75-27-42.6 1.92
Bromoform ND ug/m3 01/27/15 21:46 75-25-24.0 1.92
Bromomethane ND ug/m3 01/27/15 21:46 74-83-93.8 1.92
1,3-Butadiene ND ug/m3 01/27/15 21:46 106-99-00.86 1.92
2-Butanone (MEK)9.0 ug/m3 01/27/15 21:46 78-93-31.2 1.92
Carbon disulfide ND ug/m3 01/27/15 21:46 75-15-01.2 1.92
Carbon tetrachloride ND ug/m3 01/27/15 21:46 56-23-51.2 1.92
Chlorobenzene ND ug/m3 01/27/15 21:46 108-90-71.8 1.92
Chloroethane ND ug/m3 01/27/15 21:46 75-00-31.0 1.92
Chloroform ND ug/m3 01/27/15 21:46 67-66-30.95 1.92
Chloromethane ND ug/m3 01/27/15 21:46 74-87-32.0 1.92
Cyclohexane ND ug/m3 01/27/15 21:46 110-82-71.3 1.92
Dibromochloromethane ND ug/m3 01/27/15 21:46 124-48-13.3 1.92
1,2-Dibromoethane (EDB)ND ug/m3 01/27/15 21:46 106-93-43.0 1.92
1,2-Dichlorobenzene ND ug/m3 01/27/15 21:46 95-50-12.3 1.92
1,3-Dichlorobenzene ND ug/m3 01/27/15 21:46 541-73-12.3 1.92
1,4-Dichlorobenzene ND ug/m3 01/27/15 21:46 106-46-72.3 1.92
Dichlorodifluoromethane 3.0 ug/m3 01/27/15 21:46 75-71-81.9 1.92
1,1-Dichloroethane ND ug/m3 01/27/15 21:46 75-34-31.6 1.92
1,2-Dichloroethane ND ug/m3 01/27/15 21:46 107-06-20.79 1.92
1,1-Dichloroethene ND ug/m3 01/27/15 21:46 75-35-41.6 1.92
cis-1,2-Dichloroethene ND ug/m3 01/27/15 21:46 156-59-23.9 1.92
trans-1,2-Dichloroethene ND ug/m3 01/27/15 21:46 156-60-51.6 1.92
1,2-Dichloropropane ND ug/m3 01/27/15 21:46 78-87-51.8 1.92
cis-1,3-Dichloropropene ND ug/m3 01/27/15 21:46 10061-01-51.8 1.92
trans-1,3-Dichloropropene ND ug/m3 01/27/15 21:46 10061-02-61.8 1.92
Dichlorotetrafluoroethane ND ug/m3 01/27/15 21:46 76-14-22.7 1.92
Ethyl acetate 9.1 ug/m3 01/27/15 21:46 141-78-61.4 1.92
Ethylbenzene ND ug/m3 01/27/15 21:46 100-41-41.7 1.92
4-Ethyltoluene 2.2 ug/m3 01/27/15 21:46 622-96-81.9 1.92
n-Heptane 3.8 ug/m3 01/27/15 21:46 142-82-51.6 1.92
Hexachloro-1,3-butadiene ND ug/m3 01/27/15 21:46 87-68-34.2 1.92
n-Hexane 29.6 ug/m3 01/27/15 21:46 110-54-31.4 1.92
2-Hexanone ND ug/m3 01/27/15 21:46 591-78-61.6 1.92
Methylene Chloride 33.7 ug/m3 01/27/15 21:46 75-09-26.8 1.92
4-Methyl-2-pentanone (MIBK)ND ug/m3 01/27/15 21:46 108-10-14.0 1.92
Methyl-tert-butyl ether ND ug/m3 01/27/15 21:46 1634-04-41.4 1.92
Naphthalene ND ug/m3 01/27/15 21:46 91-20-35.1 1.92
Propylene 7.1 ug/m3 01/27/15 21:46 115-07-10.67 1.92
Styrene ND ug/m3 01/27/15 21:46 100-42-51.7 1.92
1,1,2,2-Tetrachloroethane ND ug/m3 01/27/15 21:46 79-34-51.3 1.92
Tetrachloroethene 3.2 ug/m3 01/27/15 21:46 127-18-41.3 1.92
Tetrahydrofuran ND ug/m3 01/27/15 21:46 109-99-91.2 1.92
Toluene 7.8 ug/m3 01/27/15 21:46 108-88-31.5 1.92
1,2,4-Trichlorobenzene ND ug/m3 01/27/15 21:46 120-82-12.9 1.92
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/30/2015 07:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92234909
GUSSMAN CLEANERS 22.22171
Sample:SG-2 Lab ID:92234909002 Collected:01/22/15 16:10 Received:01/26/15 09:20 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 01/27/15 21:46 71-55-61.3 1.92
1,1,2-Trichloroethane ND ug/m3 01/27/15 21:46 79-00-51.1 1.92
Trichloroethene ND ug/m3 01/27/15 21:46 79-01-61.0 1.92
Trichlorofluoromethane ND ug/m3 01/27/15 21:46 75-69-42.2 1.92
1,1,2-Trichlorotrifluoroethane ND ug/m3 01/27/15 21:46 76-13-13.1 1.92
1,2,4-Trimethylbenzene 8.3 ug/m3 01/27/15 21:46 95-63-61.9 1.92
1,3,5-Trimethylbenzene 2.1 ug/m3 01/27/15 21:46 108-67-81.9 1.92
Vinyl acetate ND ug/m3 01/27/15 21:46 108-05-41.4 1.92
Vinyl chloride ND ug/m3 01/27/15 21:46 75-01-40.50 1.92
m&p-Xylene 6.0 ug/m3 01/27/15 21:46 179601-23-13.4 1.92
o-Xylene 3.1 ug/m3 01/27/15 21:46 95-47-61.7 1.92
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/30/2015 07:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234909
GUSSMAN CLEANERS 22.22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
AIR/22361
TO-15
TO-15
TO15 MSV AIR Low Level
Associated Lab Samples:92234909001, 92234909002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1889020
Associated Lab Samples:92234909001, 92234909002
Matrix:Air
Analyzed
1,1,1-Trichloroethane ug/m3 ND 0.70 01/27/15 11:33
1,1,2,2-Tetrachloroethane ug/m3 ND 0.70 01/27/15 11:33
1,1,2-Trichloroethane ug/m3 ND 0.56 01/27/15 11:33
1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.6 01/27/15 11:33
1,1-Dichloroethane ug/m3 ND 0.82 01/27/15 11:33
1,1-Dichloroethene ug/m3 ND 0.81 01/27/15 11:33
1,2,4-Trichlorobenzene ug/m3 ND 1.5 01/27/15 11:33
1,2,4-Trimethylbenzene ug/m3 ND 1.0 01/27/15 11:33
1,2-Dibromoethane (EDB)ug/m3 ND 1.6 01/27/15 11:33
1,2-Dichlorobenzene ug/m3 ND 1.2 01/27/15 11:33
1,2-Dichloroethane ug/m3 ND 0.41 01/27/15 11:33
1,2-Dichloropropane ug/m3 ND 0.94 01/27/15 11:33
1,3,5-Trimethylbenzene ug/m3 ND 1.0 01/27/15 11:33
1,3-Butadiene ug/m3 ND 0.45 01/27/15 11:33
1,3-Dichlorobenzene ug/m3 ND 1.2 01/27/15 11:33
1,4-Dichlorobenzene ug/m3 ND 1.2 01/27/15 11:33
2-Butanone (MEK)ug/m3 ND 0.60 01/27/15 11:33
2-Hexanone ug/m3 ND 0.83 01/27/15 11:33
4-Ethyltoluene ug/m3 ND 1.0 01/27/15 11:33
4-Methyl-2-pentanone (MIBK)ug/m3 ND 2.1 01/27/15 11:33
Acetone ug/m3 ND 2.4 01/27/15 11:33
Benzene ug/m3 ND 0.32 01/27/15 11:33
Bromodichloromethane ug/m3 ND 1.4 01/27/15 11:33
Bromoform ug/m3 ND 2.1 01/27/15 11:33
Bromomethane ug/m3 ND 2.0 01/27/15 11:33
Carbon disulfide ug/m3 ND 0.63 01/27/15 11:33
Carbon tetrachloride ug/m3 ND 0.64 01/27/15 11:33
Chlorobenzene ug/m3 ND 0.94 01/27/15 11:33
Chloroethane ug/m3 ND 0.54 01/27/15 11:33
Chloroform ug/m3 ND 0.50 01/27/15 11:33
Chloromethane ug/m3 ND 1.0 01/27/15 11:33
cis-1,2-Dichloroethene ug/m3 ND 2.0 01/27/15 11:33
cis-1,3-Dichloropropene ug/m3 ND 0.92 01/27/15 11:33
Cyclohexane ug/m3 ND 0.70 01/27/15 11:33
Dibromochloromethane ug/m3 ND 1.7 01/27/15 11:33
Dichlorodifluoromethane ug/m3 ND 1.0 01/27/15 11:33
Dichlorotetrafluoroethane ug/m3 ND 1.4 01/27/15 11:33
Ethyl acetate ug/m3 ND 0.73 01/27/15 11:33
Ethylbenzene ug/m3 ND 0.88 01/27/15 11:33
Hexachloro-1,3-butadiene ug/m3 ND 2.2 01/27/15 11:33
m&p-Xylene ug/m3 ND 1.8 01/27/15 11:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/30/2015 07:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234909
GUSSMAN CLEANERS 22.22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1889020
Associated Lab Samples:92234909001, 92234909002
Matrix:Air
Analyzed
Methyl-tert-butyl ether ug/m3 ND 0.73 01/27/15 11:33
Methylene Chloride ug/m3 ND 3.5 01/27/15 11:33
n-Heptane ug/m3 ND 0.83 01/27/15 11:33
n-Hexane ug/m3 ND 0.72 01/27/15 11:33
Naphthalene ug/m3 ND 2.7 01/27/15 11:33
o-Xylene ug/m3 ND 0.88 01/27/15 11:33
Propylene ug/m3 ND 0.35 01/27/15 11:33
Styrene ug/m3 ND 0.87 01/27/15 11:33
Tetrachloroethene ug/m3 ND 0.69 01/27/15 11:33
Tetrahydrofuran ug/m3 ND 0.60 01/27/15 11:33
Toluene ug/m3 ND 0.77 01/27/15 11:33
trans-1,2-Dichloroethene ug/m3 ND 0.81 01/27/15 11:33
trans-1,3-Dichloropropene ug/m3 ND 0.92 01/27/15 11:33
Trichloroethene ug/m3 ND 0.55 01/27/15 11:33
Trichlorofluoromethane ug/m3 ND 1.1 01/27/15 11:33
Vinyl acetate ug/m3 ND 0.72 01/27/15 11:33
Vinyl chloride ug/m3 ND 0.26 01/27/15 11:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1889021LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 55.755.5 100 72-140
1,1,2,2-Tetrachloroethane ug/m3 65.769.8 94 68-137
1,1,2-Trichloroethane ug/m3 51.755.5 93 66-138
1,1,2-Trichlorotrifluoroethane ug/m3 80.677.9 103 70-132
1,1-Dichloroethane ug/m3 43.341.2 105 68-137
1,1-Dichloroethene ug/m3 40.640.3 101 73-138
1,2,4-Trichlorobenzene ug/m3 65.875.5 87 48-150
1,2,4-Trimethylbenzene ug/m3 49.450 99 75-134
1,2-Dibromoethane (EDB)ug/m3 79.178.1 101 75-132
1,2-Dichlorobenzene ug/m3 57.261.2 94 71-129
1,2-Dichloroethane ug/m3 44.341.2 108 73-139
1,2-Dichloropropane ug/m3 46.947 100 70-130
1,3,5-Trimethylbenzene ug/m3 45.650 91 75-133
1,3-Butadiene ug/m3 24.222.5 108 66-135
1,3-Dichlorobenzene ug/m3 57.161.2 93 75-131
1,4-Dichlorobenzene ug/m3 58.261.2 95 69-135
2-Butanone (MEK)ug/m3 30.730 102 67-131
2-Hexanone ug/m3 41.141.7 99 72-130
4-Ethyltoluene ug/m3 47.550 95 75-130
4-Methyl-2-pentanone (MIBK)ug/m3 37.341.7 90 68-134
Acetone ug/m3 20.924.2 86 63-144
Benzene ug/m3 29.132.5 90 64-139
Bromodichloromethane ug/m3 67.668.2 99 75-134
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/30/2015 07:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234909
GUSSMAN CLEANERS 22.22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1889021LABORATORY CONTROL SAMPLE:
LCSSpike
Bromoform ug/m3 99.1105 94 72-130
Bromomethane ug/m3 39.939.5 101 71-132
Carbon disulfide ug/m3 28.231.7 89 56-139
Carbon tetrachloride ug/m3 58.764 92 75-150
Chlorobenzene ug/m3 46.246.8 99 71-132
Chloroethane ug/m3 31.226.8 116 71-129
Chloroform ug/m3 46.749.7 94 73-136
Chloromethane ug/m3 22.121 105 52-143
cis-1,2-Dichloroethene ug/m3 43.840.3 109 64-137
cis-1,3-Dichloropropene ug/m3 47.846.2 104 75-128
Cyclohexane ug/m3 30.735 88 62-143
Dibromochloromethane ug/m3 83.086.6 96 75-136
Dichlorodifluoromethane ug/m3 54.250.3 108 70-141
Dichlorotetrafluoroethane ug/m3 73.771.1 104 71-139
Ethyl acetate ug/m3 36.236.6 99 64-137
Ethylbenzene ug/m3 41.544.2 94 71-136
Hexachloro-1,3-butadiene ug/m3 104108 96 51-150
m&p-Xylene ug/m3 81.588.3 92 71-134
Methyl-tert-butyl ether ug/m3 35.636.7 97 73-134
Methylene Chloride ug/m3 35.035.3 99 64-130
n-Heptane ug/m3 43.141.7 103 63-135
n-Hexane ug/m3 38.835.8 108 69-135
Naphthalene ug/m3 48.053.3 90 43-150
o-Xylene ug/m3 41.944.2 95 75-134
Propylene ug/m3 16.017.5 92 58-135
Styrene ug/m3 42.043.3 97 75-133
Tetrachloroethene ug/m3 66.969 97 66-137
Tetrahydrofuran ug/m3 27.930 93 58-135
Toluene ug/m3 31.038.3 81 70-129
trans-1,2-Dichloroethene ug/m3 39.540.3 98 61-140
trans-1,3-Dichloropropene ug/m3 47.846.2 103 75-134
Trichloroethene ug/m3 53.654.6 98 70-134
Trichlorofluoromethane ug/m3 58.357.1 102 67-140
Vinyl acetate ug/m3 34.035.8 95 60-139
Vinyl chloride ug/m3 26.626 102 72-129
Parameter Units
Dup
Result QualifiersRPDResult
92234909001
1889709SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/30/2015 07:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234909
GUSSMAN CLEANERS 22.22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92234909001
1889709SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 9.5 19.4
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 NDND
1,3,5-Trimethylbenzene ug/m3 2.2 122.5
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 NDND
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 14.8 514.1
2-Hexanone ug/m3 1.9 91.7
4-Ethyltoluene ug/m3 2.6 72.4
4-Methyl-2-pentanone (MIBK)ug/m3 3JND
Acetone ug/m3 33.6 134.0
Benzene ug/m3 6.2 95.7
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 .75JND
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 NDND
Chloromethane ug/m3 NDND
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 NDND
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 3.0 93.3
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 NDND
Ethylbenzene ug/m3 3.4 13.4
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 12.6 112.7
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 7.5 77.0
n-Heptane ug/m3 4.4 125.0
n-Hexane ug/m3 12.3 811.4
Naphthalene ug/m3 1.1JND
o-Xylene ug/m3 5.6 65.9
Propylene ug/m3 8.7 109.6
Styrene ug/m3 1.1JND
Tetrachloroethene ug/m3 2.6 243.3
Tetrahydrofuran ug/m3 11.4 410.9
Toluene ug/m3 14.7 114.5
trans-1,2-Dichloroethene ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/30/2015 07:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92234909
GUSSMAN CLEANERS 22.22171
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92234909001
1889709SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 NDND
Trichlorofluoromethane ug/m3 .96JND
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/30/2015 07:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 17
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92234909
GUSSMAN CLEANERS 22.22171
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - MinneapolisPASI-M
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/30/2015 07:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 17
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92234909
GUSSMAN CLEANERS 22.22171
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92234909001 AIR/22361SG-1 TO-15
92234909002 AIR/22361SG-2 TO-15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/30/2015 07:26 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 17
Page 16 of 17
Page 17 of 17
Health and Safety Plan
ECS Project No. 22:22171
Gussman Cleaners
New Bern, North Carolina
January 15, 2015

5

During the work covered by this Safety Plan, there were:

X No observed violations of the Safety Plan provisions.

__The following violations of the Safety Plan provisions (give details in space below and
indicate corrective action taken for each violation noted).

Signature: Date 1/22/2015
Field Representative

Health and Safety Plan
ECS Project No. 22:22171
Gussman Cleaners
New Bern, North Carolina
January 15, 2015

6
ON-SITE HEALTH AND SAFTEY MEETING

Location___Gussman Cleaners Site
Attendees:

Printed Name Signature Company Date
Brooks Wall ECS 1/22/15