20001_North_Graham_Phase II_20151208

3701 Saunders Ave • Richmond, Virginia 23227 • [phone] • FAX [phone]

December 8, 2015
Mr. Matt Cutshall Environmental Compliance Manager
Sheetz, Inc.
351 Sheetz Way Claysburg, PA 16625
RE: Supplemental Phase 2 Environmental Site Assessment Report
Proposed Sheetz Location North Graham Hopedale Road and North Church Street, Burlington, NC

Dear Mr. Cutshall:

Groundwater & Environmental Services, Inc. (GES) is pleased to provide the following Supplemental Phase 2 Environmental Site Assessment (ESA) Report to Sheetz, Inc. (Sheetz).
This investigation was conducted at the request of Sheetz in order to provide an additional assessment of soil and groundwater at the above referenced property concentrated on the western portion of the property. On October 13, 2015, GES submitted the Limited Phase 2 ESA to Sheetz
documenting the activities and findings of previous investigation of the property identified by
Sheetz for potential development of a Sheetz retail petroleum facility.
1.0 ENVIRONMENTAL SITE ASSESSMENT
The location of the Subject Property and surrounding area is illustrated on the Site Location Map presented on the U.S. Geological Survey (USGS) 7.5-Minute Topographic Map for Burlington,
North Carolina (1981) as Figure 1. The Subject Property is located in a mixed industrial, commercial, and residential area of Burlington, North Carolina. There are commercial properties
located to the south and west, government properties to the north, residential properties to the east
and a large former industrial facility to the northwest, as shown in the Local Area Map, Figure 2. The Subject Property consists primarily of impermeable pavement which is bisected by an old
section of railroad track running northwest to southeast. The Subject Property is illustrated on the
Site Map presented as Figure 3.
On November 16 and 17, 2015, GES supervised the advancement of nine soil borings (SS-1 through SB-9) on the western portion of the Subject Property. The soil borings were advanced to investigate the extent of existing contamination from previous uses of the Subject Property or the
migration of contaminants from surrounding properties. SS-1 through SS-5 were advanced in the southwest corner of the Subject Property to investigate the location of the proposed island fuel dispensers and their respective three Underground Storage Tanks (USTs). SS-6 and SS-7 were
installed in the vicinity of the proposed Sheetz store location. SB-8 was installed in the proposed location of the car wash drive-thru. SS-9 was installed along the old section of railroad track. The nine soil borings were advanced via direct-push technology and advanced to a depth of 25
feet below ground surface (bgs). The soil boring locations are shown on Figure 4. Following

soil boring completion, a temporary well was placed into boreholes SS-2, SS-4, SS-7 and SS-8,
identified as GW-1 through GW-4, respectively, in an attempt to collect a water sample. Each
temporary well was comprised of a PVC one-inch diameter well screen and allowed to collect water for a minimum of one hour. Water samples were collected from all four temporary wells
GW-1 through GW-4.
1.1 Soil Sampling and Results One soil sample was collected from each of the borings at the interval corresponding to the highest value detected with a photo-ionization detector (PID). If no PID response was observed,
the soil sample was collected directly above the observed water table. Following the collection of each sample, the sample was split into two parts. One part of the sample was placed into a zip-lock bag for field screening. The zip-lock bags of soil were screened with a PID to measure the
concentration of volatile organic compounds (VOCs) within the headspace. The PID values from the soil samples collected for laboratory analysis are included in Table 1. The second part of the sample was placed into the laboratory supplied soil sampling bottleware, immediately labeled,
and placed on ice in a cooler in preparation for laboratory analysis.
The soil samples were submitted to Air Water & Soil Laboratories (AWS) located at 1941
Reymet Road, Richmond, VA for analysis of the site specific constitutes of concern (COCs) including: benzene, toluene, ethylbenzene, and xylenes (BTEX), methyl tertiary butyl ether
(MTBE), and naphthalene via USEPA Method SW8260B, total petroleum hydrocarbons -
gasoline range organics (TPH-GRO) and total petroleum range hydrocarbons - diesel range organics (TPH-DRO) via USEPA Method 8015C, and RCRA 8 metals via Method SW6010C
and Method SW7471B. Soil samples collected from SS-8 and SS-9 were also analyzed for semi-volatile organic compounds (SVOCs) via USEPA method SW8270D and polychlorinated biphenyls (PCBs) via USEPA method SW8082A in addition to the aforementioned constituents,
as these compounds are commonly found in these areas of concern. The analytical results from the soil samples were screened against the North Carolina Department
of Environment and Natural Resources (NCDENR) soil to groundwater Maximum Soil Contaminant Concentrations (MSCC), and are presented in Table 1. The complete laboratory analytical report is included in Attachment A. A summary of the results of the soil sample
analysis is listed below.
Exceedances of MSCC:
• Chromium: SS-1, SS-2, SS-4, and SS-6 through SS-9, at concentrations ranging from
8.71 milligrams per kilogram (mg/kg) to 601 mg/kg with the greatest concentration
observed in SS-6 (MSCC – 5.4 mg/kg).
Detections above the reporting limit and below the MSCC:
• SS-1: Barium at 140 mg/kg (MSCC – 290 mg/kg), Cadmium at 2.96 mg/kg (MSCC – not
available), and Lead at 1.37 mg/kg (MSCC – 270 mg/kg);
• SS-2: Barium at 31.3 mg/kg (MSCC – 290 mg/kg), Cadmium at 2.31 mg/kg (MSCC – not available), Mercury at 0.013 mg/kg (MSCC – not available) and Lead at 7.74 mg/kg
(MSCC - 270 mg/kg);
• SS-3: Barium at 90.5 mg/kg (MSCC – 290 mg/kg), Cadmium at 0.346 mg/kg (MSCC –
not available), Chromium at 3.45 mg/kg (MSCC – 5.4 mg/kg) and Lead at 0.737 mg/kg
(MSCC – 270 mg/kg);
2

• SS-4: Barium at 95.2 mg/kg (MSCC – 290 mg/kg), Cadmium at 0.720 mg/kg (MSCC –
not available), Mercury at 0.022 mg/kg (MSCC – not available) and Lead at 1.28 mg/kg (MSCC - 270 mg/kg);
• SS-5: Barium at 25.4 mg/kg (MSCC – 290 mg/kg), Cadmium at 0.846 mg/kg (MSCC –
not available), Chromium at 5.23 mg/kg (MSCC – 5.4 mg/kg) and Lead at 3.83 mg/kg (MSCC – 270 mg/kg);
• SS-6: Barium at 288 mg/kg (MSCC – 290 mg/kg), Cadmium at 3.87 mg/kg (MSCC – not available), Mercury at 0.012 mg/kg (MSCC – not available) and Lead at 2.16 mg/kg
(MSCC - 270 mg/kg);
• SS-7: Barium at 183 mg/kg (MSCC – 290 mg/kg) and Cadmium at 2.85 mg/kg (MSCC –
not available);
• SS-8: Barium at 71.9 mg/kg (MSCC – 290 mg/kg) and Cadmium at 0.841 mg/kg (MSCC
– not available); and
• SS-9: Barium at 111 mg/kg (MSCC – 290 mg/kg) and Cadmium at 0.580 mg/kg (MSCC – not available).
1.2 Groundwater Sampling and Analysis
On November 16 and 17, 2015, following the installation of the temporary wells GW-1, GW-2, GW-3 and GW-4 within soil borings SS-2, SS-4, SS-7 and SS-8, respectively, groundwater
samples were collected from the middle of the screened interval at depths ranging from 17.5 feet bgs to 20 feet bgs. Groundwater samples were collected from each temporary well using a peristaltic pump and each well had dedicated polyethylene tubing. Each sample was placed in the
proper bottleware and immediately placed in a cooler containing packaged ice.
The groundwater samples and associated chain-of-custody form were submitted to AWS for analysis of the site specific COCs including; BTEX, MTBE, and naphthalene via USEPA
Method SW8260B, TPH-GRO and TPH-DRO via USEPA Method 8015C, and RCRA 8 metals via Method SW6010C and Method SW7470A. The groundwater analytical results were screened against the NCDENR 2L Groundwater (GW) Standards and are presented in Table 2. The
complete analytical laboratory report is included in Attachment A. A summary of the groundwater analytical results is listed below.

Exceedances of 2L GW Standard:
• GW-1: Barium at 2.5 milligrams per liter (mg/L) (2L GW Standard – 0.7 mg/L),
Cadmium at 0.0096 mg/L (2L GW Standard – 0.002 mg/L) and Chromium at 0.0284 mg/L (2L GW Standard – 0.01 mg/L);
• GW-2: Cadmium at 0.0066 mg/L (2L GW Standard – 0.002 mg/L) and Chromium at 0.0644 mg/L (2L GW Standard – 0.01 mg/L);
• GW-3: Arsenic at 0.0105 mg/L (2L GW Standard – 0.1 mg/L); and
• GW-4: Chromium at 0.0222 mg/L (2L GW Standard – 0.01 mg/L).

Detections above the reporting limit and below the 2L GW Standard:
• GW-2: Barium at 0.616 mg/L (2L GW Standard – 0.7 mg/L);
• GW-3: Barium at 0.121 mg/L (2L GW Standard – 0.7 mg/L); and
• GW-4: Barium at 0.313 mg/L (2L GW Standard – 0.7 mg/L).
2.0 SITE ASSESSMENT SUMMARY
The following is a summary of the analytical results collected during the Supplemental Phase 2 ESA:
3

• The analytical results indicate that target compounds in all soil samples were either not
detected or detected below the MSCC, with the exception of chromium detected above the MSCC in several soil borings.
• The analytical results indicate that arsenic exceeded the 2L standard in GW-3, barium
exceeded the 2L standard in GW-1, cadmium exceeded the 2L standard in GW-1 and GW-2 and chromium exceeded the 2L standard in GW-1, GW-2 and GW-4. All remaining target
compounds were either not detected or were detected below the 2L GW standard.
• Groundwater at the Subject Property ranged from 12.05 feet bgs in GW-3 to 13.40 feet bgs in GW-1 during the investigation.
Please do not hesitate to contact me at [phone] extension 4094 with any questions and/or comments.
Respectfully submitted, GROUNDWATER & ENVIRONMENTAL SERVICES, INC.

Daniel Breckenridge
Project Manager

Figures: Figure 1 – Site Location Map
Figure 2 – Local Area Map Figure 3 – Site Map Figure 4 – Soil Boring Location Map
Tables: Table 1 – Soil Quality Data Summary
Table 2 – Groundwater Quality Data Summary Attachments:
Attachment A – Laboratory Analytical Report
4

FIGURES
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N.B.
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TABLES
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-
-
-
N
D
N
D
2,
3
,
4
,
6
-
T
e
t
r
a
c
h
l
o
r
o
p
h
e
n
o
l

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
2,
4
,
5
-
T
r
i
c
h
l
o
r
o
p
h
e
n
o
l

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
2,
4
,
6
-
T
r
i
c
h
l
o
r
o
p
h
e
n
o
l

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
2,
4
-
D
i
c
h
l
o
r
o
p
h
e
n
o
l

u
g
/
k
g
3.
4
--
-
-
-
-
-
N
D
N
D
2,
4
-
D
i
m
e
t
h
y
l
p
h
e
n
o
l

u
g
/
k
g
64
0
--
-
-
-
-
-
N
D
N
D
2,
4
-
D
i
n
i
t
r
o
p
h
e
n
o
l

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
2,
4
-
D
i
n
i
t
r
o
t
o
l
u
e
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
2,
6
-
D
i
c
h
l
o
r
o
p
h
e
n
o
l

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
2,
6
-
D
i
n
i
t
r
o
t
o
l
u
e
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
2-
C
h
l
o
r
o
n
a
p
h
t
h
a
l
e
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
2-
C
h
l
o
r
o
p
h
e
n
o
l

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
2-
M
e
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e

u
g
/
k
g
3,6
0
0
--
-
-
-
-
-
N
D
N
D
2-
N
a
p
h
t
h
y
l
a
m
i
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
2-
N
i
t
r
o
a
n
i
l
i
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
2-
N
i
t
r
o
p
h
e
n
o
l

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
3,
3
’
-
D
i
c
h
l
o
r
o
b
e
n
z
i
d
i
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
3-
M
e
t
h
y
l
c
h
o
l
a
n
t
h
r
e
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
3-
N
i
t
r
o
a
n
i
l
i
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
4,
6
-
D
i
n
i
t
r
o
-
2
-
m
e
t
h
y
l
p
h
e
n
o
l

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
Un
i
t
s

S
o
i
l
-
t
o
-
G
W

M
S
C
C
GE
S

-

D
e
c
e
m
b
e
r

2
0
1
5
1 o
f

3
N Graham Hopedale Road, Burlington, NC
Ta
b
l
e

1
SO
I
L

Q
U
A
L
I
T
Y

D
A
T
A

S
U
M
M
A
R
Y
Pr
o
p
o
s
e
d

S
h
e
e
t
z

L
o
c
a
t
i
o
n
N
G
r
a
h
a
m

H
o
p
e
d
a
l
e

R
o
a
d

a
n
d

N

C
h
u
r
c
h

S
t
r
e
e
t
Bu
r
l
i
n
g
t
o
n
,

N
o
r
t
h

C
a
r
o
l
i
n
a
Sa
m
p
l
e

I
D

S
S
-
1

S
S
-
2

S
S
-
3

S
S
-
4

S
S
-
5

S
S
-
6

S
S
-
7

S
S
-
8

S
S
-
9
Sa
m
p
l
e

D
e
p
t
h

(
f
t

b
g
s
)

1
4
-
1
7

1
4
-
1
7

1
4
-
1
7

1
2
-
1
5

1
1
-
1
3

1
1
-
1
3

1
5
-
1
7

1
5
-
1
7

1
1
-
1
3
Da
t
e

S
a
m
p
l
e
d

1
1
/
1
6
/
2
0
1
5

1
1
/
1
6
/
2
0
1
5

1
1
/
1
6
/
2
0
1
5

1
1
/
1
6
/
2
0
1
5

1
1
/
1
7
/
2
0
1
5

1
1
/
1
7
/
2
0
1
5

1
1
/
1
6
/
2
0
1
5

1
1
/
1
6
/
2
0
1
5

1
1
/
1
7
/
2
0
1
5
Un
i
t
s

S
o
i
l
-
t
o
-
G
W

M
S
C
C
Se
m
i
-
V
o
l
a
t
i
l
e

O
r
g
a
n
i
c

C
o
m
p
o
u
n
d
s

(
S
V
O
C
s
)
4-
A
m
i
n
o
b
i
p
h
e
n
y
l

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
4-
B
r
o
m
o
p
h
e
n
y
l

p
h
e
n
y
l

e
t
h
e
r

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
4-
C
h
l
o
r
o
a
n
i
l
i
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
4-
C
h
l
o
r
o
p
h
e
n
y
l

p
h
e
n
y
l

e
t
h
e
r

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
4-
N
i
t
r
o
a
n
i
l
i
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
4-
N
i
t
r
o
p
h
e
n
o
l

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
7,
1
2
-
D
i
m
e
t
h
y
l
b
e
n
z

(
a
)

a
n
t
h
r
a
c
e
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
Ac
e
n
a
p
h
t
h
e
n
e

u
g
/
k
g
8,2
0
0
--
-
-
-
-
-
N
D
N
D
Ac
e
n
a
p
h
t
h
y
l
e
n
e

u
g
/
k
g
11
,
0
0
0
--
-
-
-
-
-
N
D
N
D
Ac
e
t
o
p
h
e
n
o
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
An
i
l
i
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
An
t
h
r
a
c
e
n
e

u
g
/
k
g
94
0
,
0
0
0
--
-
-
-
-
-
N
D
N
D
Be
n
z
i
d
i
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
Be
n
z
o

(
a
)

a
n
t
h
r
a
c
e
n
e

u
g
/
k
g
35
0
--
-
-
-
-
-
N
D
N
D
Be
n
z
o

(
a
)

p
y
r
e
n
e

u
g
/
k
g
96
--
-
-
-
-
-
N
D
N
D
Be
n
z
o

(
b
)

f
l
u
o
r
a
n
t
h
e
n
e

u
g
/
k
g
12
,
0
0
0
--
-
-
-
-
-
N
D
N
D
Be
n
z
o

(
g
,
h
,
i
)

p
e
r
y
l
e
n
e

u
g
/
k
g
6,4
0
0
,
0
0
0
--
-
-
-
-
-
N
D
N
D
Be
n
z
o

(
k
)

f
l
u
o
r
a
n
t
h
e
n
e

u
g
/
k
g
12
,
0
0
0
--
-
-
-
-
-
N
D
N
D
Be
n
z
o
i
c

a
c
i
d

u
g
/
k
g
12
0
,
0
0
0
--
-
-
-
-
-
N
D
N
D
Be
n
z
y
l

a
l
c
o
h
o
l

u
g
/
k
g
2,0
0
0
--
-
-
-
-
-
N
D
N
D
bi
s

(
2
-
C
h
l
o
r
o
e
t
h
o
x
y
)

m
e
t
h
a
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
bi
s

(
2
-
C
h
l
o
r
o
e
t
h
y
l
)

e
t
h
e
r

u
g
/
k
g
0.
1
6
--
-
-
-
-
-
N
D
N
D
bi
s

(
2
-
C
h
l
o
r
o
i
s
o
p
r
o
p
y
l
)

e
t
h
e
r

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
bi
s

(
2
-
E
t
h
y
l
h
e
x
y
l
)

p
h
t
h
a
l
a
t
e

u
g
/
k
g
6,6
0
0
--
-
-
-
-
-
N
D
N
D
Bu
t
y
l

b
e
n
z
y
l

p
h
t
h
a
l
a
t
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
Ch
r
y
s
e
n
e

u
g
/
k
g
39
,
0
0
0
--
-
-
-
-
-
N
D
N
D
Di
b
e
n
z

(
a
,
h
)

a
n
t
h
r
a
c
e
n
e

u
g
/
k
g
17
0
--
-
-
-
-
-
N
D
N
D
Di
b
e
n
z

(
a
,
j
)

a
c
r
i
d
i
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
Di
b
e
n
z
o
f
u
r
a
n

u
g
/
k
g
4,7
0
0
--
-
-
-
-
-
N
D
N
D
Di
e
t
h
y
l

p
h
t
h
a
l
a
t
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
Di
m
e
t
h
y
l

p
h
t
h
a
l
a
t
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
Di
-
n
-
b
u
t
y
l

p
h
t
h
a
l
a
t
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
Di
-
n
-
o
c
t
y
l

p
h
t
h
a
l
a
t
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
Di
p
h
e
n
y
l
a
m
i
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
Eth
y
l

m
e
t
h
a
n
e
s
u
l
f
o
n
a
t
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
Fl
u
o
r
a
n
t
h
e
n
e

u
g
/
k
g
29
0
,
0
0
0
--
-
-
-
-
-
N
D
N
D
Fl
u
o
r
e
n
e

u
g
/
k
g
47
,
0
0
0
--
-
-
-
-
-
N
D
N
D
He
x
a
c
h
l
o
r
o
b
e
n
z
e
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
He
x
a
c
h
l
o
r
o
b
u
t
a
d
i
e
n
e

u
g
/
k
g
23
0
--
-
-
-
-
-
N
D
N
D
He
x
a
c
h
l
o
r
o
c
y
c
l
o
p
e
n
t
a
d
i
e
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
He
x
a
c
h
l
o
r
o
e
t
h
a
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
In
d
e
n
o

(
1
,
2
,
3
-
c
d
)

p
y
r
e
n
e

u
g
/
k
g
3,4
0
0
--
-
-
-
-
-
N
D
N
D
Is
o
p
h
o
r
o
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
m+
p
-
C
r
e
s
o
l
s

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
Me
t
h
y
l

m
e
t
h
a
n
e
s
u
l
f
o
n
a
t
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
Na
p
h
t
h
a
l
e
n
e

u
g
/
k
g
16
0
--
-
-
-
-
-
N
D
N
D
Ni
t
r
o
b
e
n
z
e
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
n-
N
i
t
r
o
s
o
d
i
m
e
t
h
y
l
a
m
i
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
n-
N
i
t
r
o
s
o
d
i
-
n
-
b
u
t
y
l
a
m
i
n
e

u
g
/
k
g
~
--
-
-
-
-
-
N
D
N
D
GE
S

-

D
e
c
e
m
b
e
r

2
0
1
5
2 o
f

3
N Graham Hopedale Road, Burlington, NC
Ta
b
l
e

1
SO
I
L

Q
U
A
L
I
T
Y

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N
C

ATTACHMENT A
Laboratory Analytical Report
1941 Reymet Road l Richmond, Virginia 23237 l Tel: [phone] Fax: [phone]
Laboratory Order ID 15K0390
Certificate of Analysis
Client Name:
Enclosed are the results of analyses for samples received by the laboratory on 11/17/2015 16:15. If you have
any questions concerning this report, please feel free to contact the laboratory.
Sincerely,
Ted Soyars
Laboratory Manager
Richmond, VA 23227
3701 Saunders Ave.
Purchase Order:
[none]Project Number:
Date Issued:
Date Received:
Submitted To:
Client Site I.D.:
November 24, 2015 17:24
November 17, 2015 16:15Groundwater Environmental Services, Inc.-R
Daniel Breckenridge
End Notes:
The test results listed in this report relate only to the samples submitted to the laboratory and as received by the Laboratory.
Unless otherwise noted, the test results for solid materials are calculated on a wet weight basis. Analyses for pH, dissolved oxygen,
temperature, residual chlorine and sulfite that are performed in the laboratory do not meet NELAC requirements due to extremely
short holding times. These analyses should be performed in the field. The results of field analyses performed by the Sampler
included in the Certificate of Analysis are done so at the client’s request and are not included in the laboratory’s fields of certification
nor have they been audited for adherence to a reference method or procedure.
The signature on the final report certifies that these results conform to all applicable NELAC standards unless otherwise specified.
For a complete list of the Laboratory’s NELAC certified parameters please contact customer service.
This report shall not be reproduced except in full without the expressed and written approval of an authorized representative of Air
Water & Soil Laboratories, Inc.
Sheetz - Burlington Phase II Follow-up
Final Report
Page 1 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
ANALYTICAL REPORT FOR SAMPLES
Laboratory Order ID 15K0390
MatrixSample ID Laboratory ID Date Sampled Date Received
SS-1 (14-17)15K0390-01 11/17/2015 16:15Soil11/16/2015 12:45
SS-2 (14-17)15K0390-02 11/17/2015 16:15Soil11/16/2015 13:30
SS-3 (14-17)15K0390-03 11/17/2015 16:15Soil11/16/2015 14:30
SS-4 (12-15)15K0390-04 11/17/2015 16:15Soil11/16/2015 15:20
SS-7 (15-17)15K0390-05 11/17/2015 16:15Soil11/16/2015 15:55
SS-8 (15-17)15K0390-06 11/17/2015 16:15Soil11/16/2015 16:30
GW-1 15K0390-07 11/17/2015 16:15Ground Water 11/17/2015 07:45
GW-2 15K0390-08 11/17/2015 16:15Ground Water 11/17/2015 08:15
GW-3 15K0390-09 11/17/2015 16:15Ground Water 11/17/2015 08:45
GW-4 15K0390-10 11/17/2015 16:15Ground Water 11/17/2015 09:15
SS-9 (11-13)15K0390-11 11/17/2015 16:15Soil11/17/2015 09:30
SS-6 (11-13)15K0390-12 11/17/2015 16:15Soil11/17/2015 10:10
SS-5 (11-13)15K0390-13 11/17/2015 16:15Soil11/17/2015 10:45
Trip Blank 15K0390-14 11/17/2015 16:15Non-Potable Water 11/10/2015 09:20
Soil results have been calculated based on dry weight.
Page 2 of 63Page 2 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/16/2015 12:45Date/Time Sampled:
SS-1 (14-17)Laboratory Sample ID:Sample I.D.15K0390-01
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C KEW<0.632 mg/kg dry 0.632 101 11/19/15 10:20 11/20/15 15:04Silver
SW6010C KEW<1.26 mg/kg dry 1.26 101 11/19/15 10:20 11/20/15 15:04Arsenic
SW6010C 140 mg/kg dry KEW0.632 101 11/19/15 10:20 11/20/15 15:04Barium
SW6010C 2.96 mg/kg dry KEW0.253 101 11/19/15 10:20 11/20/15 15:04Cadmium
SW6010C 26.0 mg/kg dry KEW0.632 101 11/19/15 10:20 11/20/15 15:04Chromium
SW7471B MWL<0.010 mg/kg dry 0.010 101 11/23/15 15:00 11/24/15 11:04Mercury
SW6010C 1.37 mg/kg dry KEW0.632 101 11/19/15 10:20 11/20/15 15:04Lead
SW6010C KEW<3.16 mg/kg dry 3.16 101 11/19/15 10:20 11/20/15 15:04Selenium
Volatile Hydrocarbons by GC
SW8015C CL<0.10 mg/kg dry 0.10 101 11/19/15 12:30 11/19/15 12:30TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B MKD<6.47 ug/kg dry 6.47 101 11/19/15 12:50 11/19/15 12:50Benzene
SW8260B MKD<6.47 ug/kg dry 6.47 101 11/19/15 12:50 11/19/15 12:50Ethylbenzene
SW8260B MKD<6.47 ug/kg dry 6.47 101 11/19/15 12:50 11/19/15 12:50m+p-Xylenes
SW8260B MKD<6.47 ug/kg dry 6.47 101 11/19/15 12:50 11/19/15 12:50Methyl-t-butyl ether (MTBE)
SW8260B MKD<6.47 ug/kg dry 6.47 101 11/19/15 12:50 11/19/15 12:50Naphthalene
SW8260B MKD<6.47 ug/kg dry 6.47 101 11/19/15 12:50 11/19/15 12:50o-Xylene
SW8260B MKD<6.47 ug/kg dry 6.47 101 11/19/15 12:50 11/19/15 12:50Toluene
SW8260B MKD<19.4 ug/kg dry 19.4 101 11/19/15 12:50 11/19/15 12:50Xylenes, Total
80-120106 %Surr: 1,2-Dichloroethane-d4 MKD01SW8260B11/19/15 12:50 11/19/15 12:50
85-12094.5 %Surr: 4-Bromofluorobenzene MKD01SW8260B11/19/15 12:50 11/19/15 12:50
78-11998.7 %Surr: Dibromofluoromethane MKD01SW8260B11/19/15 12:50 11/19/15 12:50
85-11599.2 %Surr: Toluene-d8 MKD01SW8260B11/19/15 12:50 11/19/15 12:50
Page 3 of 63Page 3 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/16/2015 12:45Date/Time Sampled:
SS-1 (14-17)Laboratory Sample ID:Sample I.D.15K0390-01
Analytical Results
Semivolatile Hydrocarbons by GC
SW8015C JHV<12.8 mg/kg dry 12.8 101 11/20/15 11:13 11/23/15 13:18TPH-Semi-Volatiles (DRO)
40-16056.4 %Surr: Pentacosane JHV01SW8015C11/20/15 11:13 11/23/15 13:18
Wet Chemistry Analysis
SM18 2540G 77.3 %RCV0.10 101 11/19/15 15:12 11/19/15 15:12Percent Solids
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/16/2015 13:30Date/Time Sampled:
SS-2 (14-17)Laboratory Sample ID:Sample I.D.15K0390-02
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C KEW<0.648 mg/kg dry 0.648 102 11/19/15 10:20 11/24/15 15:21Silver
SW6010C KEW<1.30 mg/kg dry 1.30 102 11/19/15 10:20 11/24/15 15:21Arsenic
SW6010C 31.3 mg/kg dry KEW0.648 102 11/19/15 10:20 11/24/15 15:21Barium
SW6010C 2.31 mg/kg dry KEW0.259 102 11/19/15 10:20 11/24/15 15:21Cadmium
SW6010C 19.3 mg/kg dry KEW0.648 102 11/19/15 10:20 11/24/15 15:21Chromium
SW7471B 0.013 mg/kg dry MWL0.010 102 11/23/15 15:00 11/24/15 11:11Mercury
SW6010C 7.74 mg/kg dry KEW0.648 102 11/19/15 10:20 11/24/15 15:21Lead
SW6010C KEW<3.24 mg/kg dry 3.24 102 11/19/15 10:20 11/24/15 15:21Selenium
Volatile Hydrocarbons by GC
SW8015C CL<5.10 mg/kg dry 5.10 5002RE1 11/19/15 17:21 11/19/15 17:21TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B MKD<351 ug/kg dry 351 5002RE1 11/20/15 13:57 11/20/15 13:57Benzene
SW8260B MKD<351 ug/kg dry 351 5002RE1 11/20/15 13:57 11/20/15 13:57Ethylbenzene
Page 4 of 63Page 4 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/16/2015 13:30Date/Time Sampled:
SS-2 (14-17)Laboratory Sample ID:Sample I.D.15K0390-02
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B MKD<351 ug/kg dry 351 5002RE1 11/20/15 13:57 11/20/15 13:57m+p-Xylenes
SW8260B MKD<351 ug/kg dry 351 5002RE1 11/20/15 13:57 11/20/15 13:57Methyl-t-butyl ether (MTBE)
SW8260B MKD<7.02 ug/kg dry 7.02 102RE1 11/20/15 13:57 11/20/15 13:57Naphthalene
SW8260B MKD<351 ug/kg dry 351 5002RE1 11/20/15 13:57 11/20/15 13:57o-Xylene
SW8260B MKD<351 ug/kg dry 351 5002RE1 11/20/15 13:57 11/20/15 13:57Toluene
SW8260B MKD<21.1 ug/kg dry 21.1 102RE1 11/20/15 13:57 11/20/15 13:57Xylenes, Total
80-120106 %Surr: 1,2-Dichloroethane-d4 MKD02RE1SW8260B11/20/15 13:57 11/20/15 13:57
85-12086.9 %Surr: 4-Bromofluorobenzene MKD02RE1SW8260B11/20/15 13:57 11/20/15 13:57
78-11997.8 %Surr: Dibromofluoromethane MKD02RE1SW8260B11/20/15 13:57 11/20/15 13:57
85-115101 %Surr: Toluene-d8 MKD02RE1SW8260B11/20/15 13:57 11/20/15 13:57
Semivolatile Hydrocarbons by GC
SW8015C JHV<13.8 mg/kg dry 13.8 102 11/20/15 11:13 11/23/15 13:45TPH-Semi-Volatiles (DRO)
40-16071.6 %Surr: Pentacosane JHV02SW8015C11/20/15 11:13 11/23/15 13:45
Wet Chemistry Analysis
SM18 2540G 71.2 %RCV0.10 102 11/19/15 15:14 11/19/15 15:14Percent Solids
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/16/2015 14:30Date/Time Sampled:
SS-3 (14-17)Laboratory Sample ID:Sample I.D.15K0390-03
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C KEW<0.609 mg/kg dry 0.609 103 11/19/15 10:20 11/24/15 15:40Silver
SW6010C KEW<1.22 mg/kg dry 1.22 103 11/19/15 10:20 11/24/15 15:40Arsenic
Page 5 of 63Page 5 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/16/2015 14:30Date/Time Sampled:
SS-3 (14-17)Laboratory Sample ID:Sample I.D.15K0390-03
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C 90.5 mg/kg dry KEW0.609 103 11/19/15 10:20 11/24/15 15:40Barium
SW6010C 0.346 mg/kg dry KEW0.244 103 11/19/15 10:20 11/24/15 15:40Cadmium
SW6010C 3.45 mg/kg dry KEW0.609 103 11/19/15 10:20 11/24/15 15:40Chromium
SW7471B MWL<0.010 mg/kg dry 0.010 103 11/23/15 15:00 11/24/15 11:14Mercury
SW6010C 0.737 mg/kg dry KEW0.609 103 11/19/15 10:20 11/24/15 15:40Lead
SW6010C KEW<3.05 mg/kg dry 3.05 103 11/19/15 10:20 11/24/15 15:40Selenium
Volatile Hydrocarbons by GC
SW8015C CL<0.10 mg/kg dry 0.10 103 11/19/15 13:14 11/19/15 13:14TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B MKD<6.58 ug/kg dry 6.58 103 11/19/15 13:36 11/19/15 13:36Benzene
SW8260B MKD<6.58 ug/kg dry 6.58 103 11/19/15 13:36 11/19/15 13:36Ethylbenzene
SW8260B MKD<6.58 ug/kg dry 6.58 103 11/19/15 13:36 11/19/15 13:36m+p-Xylenes
SW8260B MKD<6.58 ug/kg dry 6.58 103 11/19/15 13:36 11/19/15 13:36Methyl-t-butyl ether (MTBE)
SW8260B MKD<6.58 ug/kg dry 6.58 103 11/19/15 13:36 11/19/15 13:36Naphthalene
SW8260B MKD<6.58 ug/kg dry 6.58 103 11/19/15 13:36 11/19/15 13:36o-Xylene
SW8260B MKD<6.58 ug/kg dry 6.58 103 11/19/15 13:36 11/19/15 13:36Toluene
SW8260B MKD<19.7 ug/kg dry 19.7 103 11/19/15 13:36 11/19/15 13:36Xylenes, Total
80-120112 %Surr: 1,2-Dichloroethane-d4 MKD03SW8260B11/19/15 13:36 11/19/15 13:36
85-12092.5 %Surr: 4-Bromofluorobenzene MKD03SW8260B11/19/15 13:36 11/19/15 13:36
78-119102 %Surr: Dibromofluoromethane MKD03SW8260B11/19/15 13:36 11/19/15 13:36
85-115103 %Surr: Toluene-d8 MKD03SW8260B11/19/15 13:36 11/19/15 13:36
Semivolatile Hydrocarbons by GC
SW8015C JHV<13.1 mg/kg dry 13.1 103 11/20/15 11:13 11/23/15 14:11TPH-Semi-Volatiles (DRO)
40-16070.5 %Surr: Pentacosane JHV03SW8015C11/20/15 11:13 11/23/15 14:11
Page 6 of 63Page 6 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/16/2015 14:30Date/Time Sampled:
SS-3 (14-17)Laboratory Sample ID:Sample I.D.15K0390-03
Analytical Results
Wet Chemistry Analysis
SM18 2540G 76.0 %RCV0.10 103 11/19/15 15:16 11/19/15 15:16Percent Solids
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/16/2015 15:20Date/Time Sampled:
SS-4 (12-15)Laboratory Sample ID:Sample I.D.15K0390-04
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C KEW<0.638 mg/kg dry 0.638 104 11/19/15 10:20 11/24/15 15:43Silver
SW6010C KEW<1.28 mg/kg dry 1.28 104 11/19/15 10:20 11/24/15 15:43Arsenic
SW6010C 95.2 mg/kg dry KEW0.638 104 11/19/15 10:20 11/24/15 15:43Barium
SW6010C 0.720 mg/kg dry KEW0.255 104 11/19/15 10:20 11/24/15 15:43Cadmium
SW6010C 21.8 mg/kg dry KEW0.638 104 11/19/15 10:20 11/24/15 15:43Chromium
SW7471B 0.022 mg/kg dry MWL0.010 104 11/23/15 15:00 11/24/15 11:16Mercury
SW6010C 1.28 mg/kg dry KEW0.638 104 11/19/15 10:20 11/24/15 15:43Lead
SW6010C KEW<3.19 mg/kg dry 3.19 104 11/19/15 10:20 11/24/15 15:43Selenium
Volatile Hydrocarbons by GC
SW8015C CL<0.10 mg/kg dry 0.10 104 11/19/15 13:37 11/19/15 13:37TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B MKD<6.40 ug/kg dry 6.40 104 11/19/15 14:00 11/19/15 14:00Benzene
SW8260B MKD<6.40 ug/kg dry 6.40 104 11/19/15 14:00 11/19/15 14:00Ethylbenzene
SW8260B MKD<6.40 ug/kg dry 6.40 104 11/19/15 14:00 11/19/15 14:00m+p-Xylenes
SW8260B MKD<6.40 ug/kg dry 6.40 104 11/19/15 14:00 11/19/15 14:00Methyl-t-butyl ether (MTBE)
SW8260B MKD<6.40 ug/kg dry 6.40 104 11/19/15 14:00 11/19/15 14:00Naphthalene
Page 7 of 63Page 7 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/16/2015 15:20Date/Time Sampled:
SS-4 (12-15)Laboratory Sample ID:Sample I.D.15K0390-04
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B MKD<6.40 ug/kg dry 6.40 104 11/19/15 14:00 11/19/15 14:00o-Xylene
SW8260B MKD<6.40 ug/kg dry 6.40 104 11/19/15 14:00 11/19/15 14:00Toluene
SW8260B MKD<19.2 ug/kg dry 19.2 104 11/19/15 14:00 11/19/15 14:00Xylenes, Total
80-120105 %Surr: 1,2-Dichloroethane-d4 MKD04SW8260B11/19/15 14:00 11/19/15 14:00
85-12095.1 %Surr: 4-Bromofluorobenzene MKD04SW8260B11/19/15 14:00 11/19/15 14:00
78-119101 %Surr: Dibromofluoromethane MKD04SW8260B11/19/15 14:00 11/19/15 14:00
85-115100 %Surr: Toluene-d8 MKD04SW8260B11/19/15 14:00 11/19/15 14:00
Semivolatile Hydrocarbons by GC
SW8015C JHV<12.0 mg/kg dry 12.0 104 11/20/15 11:13 11/23/15 14:38TPH-Semi-Volatiles (DRO)
40-16069.3 %Surr: Pentacosane JHV04SW8015C11/20/15 11:13 11/23/15 14:38
Wet Chemistry Analysis
SM18 2540G 78.2 %RCV0.10 104 11/19/15 15:18 11/19/15 15:18Percent Solids
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/16/2015 15:55Date/Time Sampled:
SS-7 (15-17)Laboratory Sample ID:Sample I.D.15K0390-05
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C KEW<0.610 mg/kg dry 0.610 105 11/19/15 10:20 11/24/15 15:48Silver
SW6010C KEW<1.22 mg/kg dry 1.22 105 11/19/15 10:20 11/24/15 15:48Arsenic
SW6010C 183 mg/kg dry KEW0.610 105 11/19/15 10:20 11/24/15 15:48Barium
SW6010C 2.85 mg/kg dry KEW0.244 105 11/19/15 10:20 11/24/15 15:48Cadmium
SW6010C 8.71 mg/kg dry KEW0.610 105 11/19/15 10:20 11/24/15 15:48Chromium
Page 8 of 63Page 8 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/16/2015 15:55Date/Time Sampled:
SS-7 (15-17)Laboratory Sample ID:Sample I.D.15K0390-05
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW7471B MWL<0.009 mg/kg dry 0.009 105 11/23/15 15:00 11/24/15 11:18Mercury
SW6010C KEW<0.610 mg/kg dry 0.610 105 11/19/15 10:20 11/24/15 15:48Lead
SW6010C KEW<3.05 mg/kg dry 3.05 105 11/19/15 10:20 11/24/15 15:48Selenium
Volatile Hydrocarbons by GC
SW8015C CL<4.30 mg/kg dry 4.30 5005 11/19/15 17:43 11/19/15 17:43TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B MKD<6.19 ug/kg dry 6.19 105 11/19/15 14:24 11/19/15 14:24Benzene
SW8260B MKD<6.19 ug/kg dry 6.19 105 11/19/15 14:24 11/19/15 14:24Ethylbenzene
SW8260B MKD<6.19 ug/kg dry 6.19 105 11/19/15 14:24 11/19/15 14:24m+p-Xylenes
SW8260B MKD<6.19 ug/kg dry 6.19 105 11/19/15 14:24 11/19/15 14:24Methyl-t-butyl ether (MTBE)
SW8260B MKD<6.19 ug/kg dry 6.19 105 11/19/15 14:24 11/19/15 14:24Naphthalene
SW8260B MKD<6.19 ug/kg dry 6.19 105 11/19/15 14:24 11/19/15 14:24o-Xylene
SW8260B MKD<6.19 ug/kg dry 6.19 105 11/19/15 14:24 11/19/15 14:24Toluene
SW8260B MKD<18.6 ug/kg dry 18.6 105 11/19/15 14:24 11/19/15 14:24Xylenes, Total
80-120107 %Surr: 1,2-Dichloroethane-d4 MKD05SW8260B11/19/15 14:24 11/19/15 14:24
85-12093.8 %Surr: 4-Bromofluorobenzene MKD05SW8260B11/19/15 14:24 11/19/15 14:24
78-119100 %Surr: Dibromofluoromethane MKD05SW8260B11/19/15 14:24 11/19/15 14:24
85-115102 %Surr: Toluene-d8 MKD05SW8260B11/19/15 14:24 11/19/15 14:24
Semivolatile Hydrocarbons by GC
SW8015C JHV<12.4 mg/kg dry 12.4 105 11/20/15 11:13 11/23/15 15:04TPH-Semi-Volatiles (DRO)
40-16065.9 %Surr: Pentacosane JHV05SW8015C11/20/15 11:13 11/23/15 15:04
Page 9 of 63Page 9 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/16/2015 15:55Date/Time Sampled:
SS-7 (15-17)Laboratory Sample ID:Sample I.D.15K0390-05
Analytical Results
Wet Chemistry Analysis
SM18 2540G 80.8 %RCV0.10 105 11/19/15 15:20 11/19/15 15:20Percent Solids
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/16/2015 16:30Date/Time Sampled:
SS-8 (15-17)Laboratory Sample ID:Sample I.D.15K0390-06
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C KEW<0.568 mg/kg dry 0.568 106 11/19/15 10:20 11/24/15 16:08Silver
SW6010C KEW<1.14 mg/kg dry 1.14 106 11/19/15 10:20 11/24/15 16:08Arsenic
SW6010C 71.9 mg/kg dry KEW0.568 106 11/19/15 10:20 11/24/15 16:08Barium
SW6010C 0.841 mg/kg dry KEW0.227 106 11/19/15 10:20 11/24/15 16:08Cadmium
SW6010C 56.9 mg/kg dry KEW0.568 106 11/19/15 10:20 11/24/15 16:08Chromium
SW7471B MWL<0.008 mg/kg dry 0.008 106 11/23/15 15:00 11/24/15 11:25Mercury
SW6010C KEW<0.568 mg/kg dry 0.568 106 11/19/15 10:20 11/24/15 16:08Lead
SW6010C KEW<2.84 mg/kg dry 2.84 106 11/19/15 10:20 11/24/15 16:08Selenium
Volatile Hydrocarbons by GC
SW8015C CL<0.10 mg/kg dry 0.10 106 11/19/15 13:59 11/19/15 13:59TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B MKD<5.85 ug/kg dry 5.85 106 11/19/15 14:47 11/19/15 14:47Benzene
SW8260B MKD<5.85 ug/kg dry 5.85 106 11/19/15 14:47 11/19/15 14:47Ethylbenzene
SW8260B MKD<5.85 ug/kg dry 5.85 106 11/19/15 14:47 11/19/15 14:47m+p-Xylenes
SW8260B MKD<5.85 ug/kg dry 5.85 106 11/19/15 14:47 11/19/15 14:47Methyl-t-butyl ether (MTBE)
SW8260B MKD<5.85 ug/kg dry 5.85 106 11/19/15 14:47 11/19/15 14:47Naphthalene
Page 10 of 63Page 10 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/16/2015 16:30Date/Time Sampled:
SS-8 (15-17)Laboratory Sample ID:Sample I.D.15K0390-06
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B MKD<5.85 ug/kg dry 5.85 106 11/19/15 14:47 11/19/15 14:47o-Xylene
SW8260B MKD<5.85 ug/kg dry 5.85 106 11/19/15 14:47 11/19/15 14:47Toluene
SW8260B MKD<17.6 ug/kg dry 17.6 106 11/19/15 14:47 11/19/15 14:47Xylenes, Total
80-120113 %Surr: 1,2-Dichloroethane-d4 MKD06SW8260B11/19/15 14:47 11/19/15 14:47
85-12087.0 %Surr: 4-Bromofluorobenzene MKD06SW8260B11/19/15 14:47 11/19/15 14:47
78-11998.1 %Surr: Dibromofluoromethane MKD06SW8260B11/19/15 14:47 11/19/15 14:47
85-115101 %Surr: Toluene-d8 MKD06SW8260B11/19/15 14:47 11/19/15 14:47
Semivolatile Organic Compounds by GCMS
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:251,2,4,5-Tetrachlorobenzene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:251,2,4-Trichlorobenzene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:251,2-Dichlorobenzene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:251,2-Diphenylhydrazine
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:251,3-Dichlorobenzene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:251,4-Dichlorobenzene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:251-Chloronaphthalene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:251-Naphthylamine
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:252,3,4,6-Tetrachlorophenol
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:252,4,5-Trichlorophenol
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:252,4,6-Trichlorophenol
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:252,4-Dichlorophenol
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:252,4-Dimethylphenol
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:252,4-Dinitrophenol
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:252,4-Dinitrotoluene
SW8270D JHV<390 ug/kg dry C 390 406RE1 11/23/15 10:16 11/23/15 17:252,6-Dichlorophenol
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:252,6-Dinitrotoluene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:252-Chloronaphthalene
Page 11 of 63Page 11 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/16/2015 16:30Date/Time Sampled:
SS-8 (15-17)Laboratory Sample ID:Sample I.D.15K0390-06
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:252-Chlorophenol
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:252-Methylnaphthalene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:252-Naphthylamine
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:252-Nitroaniline
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:252-Nitrophenol
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:253,3'-Dichlorobenzidine
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:253-Methylcholanthrene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:253-Nitroaniline
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:254,6-Dinitro-2-methylphenol
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:254-Aminobiphenyl
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:254-Bromophenyl phenyl ether
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:254-Chloroaniline
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:254-Chlorophenyl phenyl ether
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:254-Nitroaniline
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:254-Nitrophenol
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:257,12-Dimethylbenz (a)
anthracene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Acenaphthene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Acenaphthylene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Acetophenone
SW8270D JHV<390 ug/kg dry C 390 406RE1 11/23/15 10:16 11/23/15 17:25Aniline
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Anthracene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Benzidine
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Benzo (a) anthracene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Benzo (a) pyrene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Benzo (b) fluoranthene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Benzo (g,h,i) perylene
Page 12 of 63Page 12 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/16/2015 16:30Date/Time Sampled:
SS-8 (15-17)Laboratory Sample ID:Sample I.D.15K0390-06
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Benzo (k) fluoranthene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Benzoic acid
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Benzyl alcohol
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25bis (2-Chloroethoxy) methane
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25bis (2-Chloroethyl) ether
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25bis (2-Chloroisopropyl) ether
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25bis (2-Ethylhexyl) phthalate
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Butyl benzyl phthalate
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Chrysene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Dibenz (a,h) anthracene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Dibenz (a,j) acridine
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Dibenzofuran
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Diethyl phthalate
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Dimethyl phthalate
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Di-n-butyl phthalate
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Di-n-octyl phthalate
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Diphenylamine
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Ethyl methanesulfonate
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Fluoranthene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Fluorene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Hexachlorobenzene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Hexachlorobutadiene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Hexachlorocyclopentadiene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Hexachloroethane
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Indeno (1,2,3-cd) pyrene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Isophorone
Page 13 of 63Page 13 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/16/2015 16:30Date/Time Sampled:
SS-8 (15-17)Laboratory Sample ID:Sample I.D.15K0390-06
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25m+p-Cresols
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Methyl methanesulfonate
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Naphthalene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Nitrobenzene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25n-Nitrosodimethylamine
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25n-Nitrosodi-n-butylamine
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25n-Nitrosodi-n-propylamine
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25n-Nitrosodiphenylamine
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25n-Nitrosopiperidine
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25o+m+p-Cresols
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25o-Cresol
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25p-(Dimethylamino)
azobenzene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25p-Chloro-m-cresol
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Pentachloronitrobenzene
(quintozene)
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Pentachlorophenol
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Phenacetin
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Phenanthrene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Phenol
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Pronamide
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Pyrene
SW8270D JHV<390 ug/kg dry 390 406RE1 11/23/15 10:16 11/23/15 17:25Pyridine
35-12544.9 %Surr: 2,4,6-Tribromophenol JHV06RE1SW8270D11/23/15 10:16 11/23/15 17:25
45-10541.5 %Surr: 2-Fluorobiphenyl DS JHV06RE1SW8270D11/23/15 10:16 11/23/15 17:25
35-10555.2 %Surr: 2-Fluorophenol JHV06RE1SW8270D11/23/15 10:16 11/23/15 17:25
35-10056.8 %Surr: Nitrobenzene-d5 JHV06RE1SW8270D11/23/15 10:16 11/23/15 17:25
Page 14 of 63Page 14 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/16/2015 16:30Date/Time Sampled:
SS-8 (15-17)Laboratory Sample ID:Sample I.D.15K0390-06
Analytical Results
Semivolatile Organic Compounds by GCMS
40-10054.4 %Surr: Phenol-d5 JHV06RE1SW8270D11/23/15 10:16 11/23/15 17:25
30-12570.4 %Surr: p-Terphenyl-d14 JHV06RE1SW8270D11/23/15 10:16 11/23/15 17:25
Semivolatile Hydrocarbons by GC
SW8015C JHV<11.5 mg/kg dry 11.5 106 11/20/15 11:13 11/23/15 15:31TPH-Semi-Volatiles (DRO)
40-16061.2 %Surr: Pentacosane JHV06SW8015C11/20/15 11:13 11/23/15 15:31
Organochlorine Pesticides and PCBs by GC/ECD
SW8082A SKS<0.109 mg/kg dry 0.109 106 11/23/15 12:07 11/24/15 01:57PCB as Aroclor 1016
SW8082A SKS<0.109 mg/kg dry 0.109 106 11/23/15 12:07 11/24/15 01:57PCB as Aroclor 1221
SW8082A SKS<0.109 mg/kg dry 0.109 106 11/23/15 12:07 11/24/15 01:57PCB as Aroclor 1232
SW8082A SKS<0.109 mg/kg dry 0.109 106 11/23/15 12:07 11/24/15 01:57PCB as Aroclor 1242
SW8082A SKS<0.109 mg/kg dry 0.109 106 11/23/15 12:07 11/24/15 01:57PCB as Aroclor 1248
SW8082A SKS<0.109 mg/kg dry 0.109 106 11/23/15 12:07 11/24/15 01:57PCB as Aroclor 1254
SW8082A SKS<0.109 mg/kg dry 0.109 106 11/23/15 12:07 11/24/15 01:57PCB as Aroclor 1260
30-10570.0 %Surr: DCB SKS06SW8082A11/23/15 12:07 11/24/15 01:57
30-10595.0 %Surr: TCMX SKS06SW8082A11/23/15 12:07 11/24/15 01:57
Wet Chemistry Analysis
SM18 2540G 85.4 %RCV0.10 106 11/19/15 15:22 11/19/15 15:22Percent Solids
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 07:45Date/Time Sampled:
GW-1 Laboratory Sample ID:Sample I.D.15K0390-07
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
Page 15 of 63Page 15 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 07:45Date/Time Sampled:
GW-1 Laboratory Sample ID:Sample I.D.15K0390-07
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C KEW<0.0100 mg/L 0.0100 107 11/19/15 15:00 11/23/15 18:56Silver
SW6010C KEW<0.0100 mg/L 0.0100 107 11/19/15 15:00 11/23/15 18:56Arsenic
SW6010C 2.50 mg/L KEW0.0100 107 11/19/15 15:00 11/23/15 18:56Barium
SW6010C 0.0096 mg/L KEW0.0050 107 11/19/15 15:00 11/23/15 18:56Cadmium
SW6010C 0.0284 mg/L KEW0.0100 107 11/19/15 15:00 11/23/15 18:56Chromium
SW7470A MWL<0.00020 mg/L 0.00020 107 11/20/15 09:30 11/20/15 14:50Mercury
SW6010C KEW<0.0100 mg/L 0.0100 107 11/19/15 15:00 11/23/15 18:56Lead
SW6010C <0.0500 mg/L KEW0.0500 107 11/19/15 15:00 11/23/15 18:56Selenium
Volatile Hydrocarbons by GC Cl
SW8015C CL<0.10 mg/L 0.10 107 11/19/15 15:36 11/19/15 15:36TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B MKD<1.00 ug/L 1.00 107 11/20/15 12:23 11/20/15 12:23Benzene
SW8260B MKD<1.00 ug/L 1.00 107 11/20/15 12:23 11/20/15 12:23Ethylbenzene
SW8260B MKD<2.00 ug/L 2.00 107 11/20/15 12:23 11/20/15 12:23m+p-Xylenes
SW8260B MKD<1.00 ug/L 1.00 107 11/20/15 12:23 11/20/15 12:23Methyl-t-butyl ether (MTBE)
SW8260B MKD<1.00 ug/L 1.00 107 11/20/15 12:23 11/20/15 12:23Naphthalene
SW8260B MKD<1.00 ug/L 1.00 107 11/20/15 12:23 11/20/15 12:23o-Xylene
SW8260B MKD<1.00 ug/L 1.00 107 11/20/15 12:23 11/20/15 12:23Toluene
SW8260B MKD<3.00 ug/L 3.00 107 11/20/15 12:23 11/20/15 12:23Xylenes, Total
70-120112 %Surr: 1,2-Dichloroethane-d4 MKD07SW8260B11/20/15 12:23 11/20/15 12:23
75-12089.0 %Surr: 4-Bromofluorobenzene MKD07SW8260B11/20/15 12:23 11/20/15 12:23
80-119102 %Surr: Dibromofluoromethane MKD07SW8260B11/20/15 12:23 11/20/15 12:23
85-120102 %Surr: Toluene-d8 MKD07SW8260B11/20/15 12:23 11/20/15 12:23
Page 16 of 63Page 16 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 07:45Date/Time Sampled:
GW-1 Laboratory Sample ID:Sample I.D.15K0390-07
Analytical Results
Semivolatile Hydrocarbons by GC
SW8015C JHV<0.50 mg/L 0.50 107 11/23/15 14:30 11/23/15 22:19TPH-Semi-Volatiles (DRO)
40-16087.7 %Surr: Pentacosane JHV07SW8015C11/23/15 14:30 11/23/15 22:19
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 08:15Date/Time Sampled:
GW-2 Laboratory Sample ID:Sample I.D.15K0390-08
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C KEW<0.0100 mg/L 0.0100 108 11/19/15 15:00 11/23/15 19:01Silver
SW6010C KEW<0.0100 mg/L 0.0100 108 11/19/15 15:00 11/23/15 19:02Arsenic
SW6010C 0.616 mg/L KEW0.0100 108 11/19/15 15:00 11/23/15 19:01Barium
SW6010C 0.0066 mg/L KEW0.0050 108 11/19/15 15:00 11/23/15 19:02Cadmium
SW6010C 0.0644 mg/L KEW0.0100 108 11/19/15 15:00 11/23/15 19:02Chromium
SW7470A MWL<0.00020 mg/L 0.00020 108 11/20/15 09:30 11/20/15 14:53Mercury
SW6010C <0.0100 mg/L KEW0.0100 108 11/19/15 15:00 11/23/15 19:02Lead
SW6010C KEW<0.0500 mg/L 0.0500 108 11/19/15 15:00 11/23/15 19:02Selenium
Volatile Hydrocarbons by GC
SW8015C CL<0.10 mg/L 0.10 108 11/19/15 14:28 11/19/15 14:28TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B MKD<1.00 ug/L 1.00 108 11/20/15 12:47 11/20/15 12:47Benzene
SW8260B MKD<1.00 ug/L 1.00 108 11/20/15 12:47 11/20/15 12:47Ethylbenzene
SW8260B MKD<2.00 ug/L 2.00 108 11/20/15 12:47 11/20/15 12:47m+p-Xylenes
SW8260B MKD<1.00 ug/L 1.00 108 11/20/15 12:47 11/20/15 12:47Methyl-t-butyl ether (MTBE)
Page 17 of 63Page 17 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 08:15Date/Time Sampled:
GW-2 Laboratory Sample ID:Sample I.D.15K0390-08
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B MKD<1.00 ug/L 1.00 108 11/20/15 12:47 11/20/15 12:47Naphthalene
SW8260B MKD<1.00 ug/L 1.00 108 11/20/15 12:47 11/20/15 12:47o-Xylene
SW8260B MKD<1.00 ug/L 1.00 108 11/20/15 12:47 11/20/15 12:47Toluene
SW8260B MKD<3.00 ug/L 3.00 108 11/20/15 12:47 11/20/15 12:47Xylenes, Total
70-120109 %Surr: 1,2-Dichloroethane-d4 MKD08SW8260B11/20/15 12:47 11/20/15 12:47
75-12088.5 %Surr: 4-Bromofluorobenzene MKD08SW8260B11/20/15 12:47 11/20/15 12:47
80-119102 %Surr: Dibromofluoromethane MKD08SW8260B11/20/15 12:47 11/20/15 12:47
85-120100 %Surr: Toluene-d8 MKD08SW8260B11/20/15 12:47 11/20/15 12:47
Semivolatile Hydrocarbons by GC
SW8015C JHV<0.50 mg/L 0.50 108 11/23/15 14:30 11/23/15 22:45TPH-Semi-Volatiles (DRO)
40-16082.6 %Surr: Pentacosane JHV08SW8015C11/23/15 14:30 11/23/15 22:45
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 08:45Date/Time Sampled:
GW-3 Laboratory Sample ID:Sample I.D.15K0390-09
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C KEW<0.0100 mg/L 0.0100 109 11/19/15 15:00 11/23/15 19:06Silver
SW6010C 0.0105 mg/L KEW0.0100 109 11/19/15 15:00 11/23/15 19:06Arsenic
SW6010C 0.121 mg/L KEW0.0100 109 11/19/15 15:00 11/23/15 19:06Barium
SW6010C KEW<0.0050 mg/L 0.0050 109 11/19/15 15:00 11/23/15 19:06Cadmium
SW6010C <0.0100 mg/L KEW0.0100 109 11/19/15 15:00 11/23/15 19:06Chromium
SW7470A MWL<0.00020 mg/L 0.00020 109 11/20/15 09:30 11/20/15 14:55Mercury
SW6010C KEW<0.0100 mg/L 0.0100 109 11/19/15 15:00 11/23/15 19:06Lead
Page 18 of 63Page 18 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 08:45Date/Time Sampled:
GW-3 Laboratory Sample ID:Sample I.D.15K0390-09
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C KEW<0.0500 mg/L 0.0500 109 11/19/15 15:00 11/23/15 19:06Selenium
Volatile Hydrocarbons by GC
SW8015C CL<0.10 mg/L 0.10 109 11/19/15 14:51 11/19/15 14:51TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B MKD<1.00 ug/L 1.00 109 11/20/15 13:11 11/20/15 13:11Benzene
SW8260B MKD<1.00 ug/L 1.00 109 11/20/15 13:11 11/20/15 13:11Ethylbenzene
SW8260B MKD<2.00 ug/L 2.00 109 11/20/15 13:11 11/20/15 13:11m+p-Xylenes
SW8260B MKD<1.00 ug/L 1.00 109 11/20/15 13:11 11/20/15 13:11Methyl-t-butyl ether (MTBE)
SW8260B MKD<1.00 ug/L 1.00 109 11/20/15 13:11 11/20/15 13:11Naphthalene
SW8260B MKD<1.00 ug/L 1.00 109 11/20/15 13:11 11/20/15 13:11o-Xylene
SW8260B MKD<1.00 ug/L 1.00 109 11/20/15 13:11 11/20/15 13:11Toluene
SW8260B MKD<3.00 ug/L 3.00 109 11/20/15 13:11 11/20/15 13:11Xylenes, Total
70-120107 %Surr: 1,2-Dichloroethane-d4 MKD09SW8260B11/20/15 13:11 11/20/15 13:11
75-12087.2 %Surr: 4-Bromofluorobenzene MKD09SW8260B11/20/15 13:11 11/20/15 13:11
80-11999.2 %Surr: Dibromofluoromethane MKD09SW8260B11/20/15 13:11 11/20/15 13:11
85-120102 %Surr: Toluene-d8 MKD09SW8260B11/20/15 13:11 11/20/15 13:11
Semivolatile Hydrocarbons by GC
SW8015C JHV<0.50 mg/L 0.50 109 11/23/15 14:30 11/23/15 23:11TPH-Semi-Volatiles (DRO)
40-160100 %Surr: Pentacosane JHV09SW8015C11/23/15 14:30 11/23/15 23:11
Page 19 of 63Page 19 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 09:15Date/Time Sampled:
GW-4 Laboratory Sample ID:Sample I.D.15K0390-10
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C <0.0100 mg/L KEW0.0100 110RE1 11/19/15 15:00 11/24/15 16:28Silver
SW6010C KEW<0.0100 mg/L 0.0100 110 11/19/15 15:00 11/23/15 19:21Arsenic
SW6010C 0.313 mg/L KEW0.0100 110 11/19/15 15:00 11/23/15 19:21Barium
SW6010C KEW<0.0050 mg/L 0.0050 110 11/19/15 15:00 11/23/15 19:21Cadmium
SW6010C 0.0222 mg/L KEW0.0100 110 11/19/15 15:00 11/23/15 19:21Chromium
SW7470A MWL<0.00020 mg/L 0.00020 110 11/20/15 09:30 11/20/15 15:01Mercury
SW6010C KEW<0.0100 mg/L 0.0100 110 11/19/15 15:00 11/23/15 19:21Lead
SW6010C KEW<0.0500 mg/L 0.0500 110 11/19/15 15:00 11/23/15 19:21Selenium
Volatile Hydrocarbons by GC
SW8015C CL<0.10 mg/L 0.10 110 11/19/15 15:14 11/19/15 15:14TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B MKD<1.00 ug/L 1.00 110 11/20/15 13:34 11/20/15 13:34Benzene
SW8260B MKD<1.00 ug/L 1.00 110 11/20/15 13:34 11/20/15 13:34Ethylbenzene
SW8260B MKD<2.00 ug/L 2.00 110 11/20/15 13:34 11/20/15 13:34m+p-Xylenes
SW8260B MKD<1.00 ug/L 1.00 110 11/20/15 13:34 11/20/15 13:34Methyl-t-butyl ether (MTBE)
SW8260B MKD<1.00 ug/L 1.00 110 11/20/15 13:34 11/20/15 13:34Naphthalene
SW8260B MKD<1.00 ug/L 1.00 110 11/20/15 13:34 11/20/15 13:34o-Xylene
SW8260B MKD<1.00 ug/L 1.00 110 11/20/15 13:34 11/20/15 13:34Toluene
SW8260B MKD<3.00 ug/L 3.00 110 11/20/15 13:34 11/20/15 13:34Xylenes, Total
70-120105 %Surr: 1,2-Dichloroethane-d4 MKD10SW8260B11/20/15 13:34 11/20/15 13:34
75-12088.5 %Surr: 4-Bromofluorobenzene MKD10SW8260B11/20/15 13:34 11/20/15 13:34
80-11998.8 %Surr: Dibromofluoromethane MKD10SW8260B11/20/15 13:34 11/20/15 13:34
85-120102 %Surr: Toluene-d8 MKD10SW8260B11/20/15 13:34 11/20/15 13:34
Page 20 of 63Page 20 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 09:15Date/Time Sampled:
GW-4 Laboratory Sample ID:Sample I.D.15K0390-10
Analytical Results
Semivolatile Hydrocarbons by GC
SW8015C JHV<0.50 mg/L 0.50 110 11/23/15 14:30 11/23/15 23:38TPH-Semi-Volatiles (DRO)
40-16095.2 %Surr: Pentacosane JHV10SW8015C11/23/15 14:30 11/23/15 23:38
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 09:30Date/Time Sampled:
SS-9 (11-13)Laboratory Sample ID:Sample I.D.15K0390-11
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C KEW<0.682 mg/kg dry 0.682 111 11/19/15 10:20 11/24/15 16:13Silver
SW6010C KEW<1.36 mg/kg dry 1.36 111 11/19/15 10:20 11/24/15 16:14Arsenic
SW6010C 111 mg/kg dry KEW0.682 111 11/19/15 10:20 11/24/15 16:13Barium
SW6010C 0.580 mg/kg dry KEW0.273 111 11/19/15 10:20 11/24/15 16:14Cadmium
SW6010C 9.64 mg/kg dry KEW0.682 111 11/19/15 10:20 11/24/15 16:14Chromium
SW7471B MWL<0.011 mg/kg dry 0.011 111 11/23/15 15:00 11/24/15 11:27Mercury
SW6010C KEW<0.682 mg/kg dry 0.682 111 11/19/15 10:20 11/24/15 16:14Lead
SW6010C KEW<3.41 mg/kg dry 3.41 111 11/19/15 10:20 11/24/15 16:14Selenium
Volatile Hydrocarbons by GC
SW8015C CL<5.63 mg/kg dry 5.63 5011RE1 11/19/15 18:06 11/19/15 18:06TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B MKD<7.07 ug/kg dry 7.07 111 11/19/15 15:10 11/19/15 15:10Benzene
SW8260B MKD<7.07 ug/kg dry 7.07 111 11/19/15 15:10 11/19/15 15:10Ethylbenzene
SW8260B MKD<7.07 ug/kg dry 7.07 111 11/19/15 15:10 11/19/15 15:10m+p-Xylenes
SW8260B MKD<7.07 ug/kg dry 7.07 111 11/19/15 15:10 11/19/15 15:10Methyl-t-butyl ether (MTBE)
Page 21 of 63Page 21 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 09:30Date/Time Sampled:
SS-9 (11-13)Laboratory Sample ID:Sample I.D.15K0390-11
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B MKD<7.07 ug/kg dry 7.07 111 11/19/15 15:10 11/19/15 15:10Naphthalene
SW8260B MKD<7.07 ug/kg dry 7.07 111 11/19/15 15:10 11/19/15 15:10o-Xylene
SW8260B MKD<7.07 ug/kg dry 7.07 111 11/19/15 15:10 11/19/15 15:10Toluene
SW8260B MKD<21.2 ug/kg dry 21.2 111 11/19/15 15:10 11/19/15 15:10Xylenes, Total
80-120112 %Surr: 1,2-Dichloroethane-d4 MKD11SW8260B11/19/15 15:10 11/19/15 15:10
85-12092.0 %Surr: 4-Bromofluorobenzene MKD11SW8260B11/19/15 15:10 11/19/15 15:10
78-119100 %Surr: Dibromofluoromethane MKD11SW8260B11/19/15 15:10 11/19/15 15:10
85-115102 %Surr: Toluene-d8 MKD11SW8260B11/19/15 15:10 11/19/15 15:10
Semivolatile Organic Compounds by GCMS
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:531,2,4,5-Tetrachlorobenzene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:531,2,4-Trichlorobenzene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:531,2-Dichlorobenzene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:531,2-Diphenylhydrazine
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:531,3-Dichlorobenzene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:531,4-Dichlorobenzene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:531-Chloronaphthalene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:531-Naphthylamine
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:532,3,4,6-Tetrachlorophenol
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:532,4,5-Trichlorophenol
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:532,4,6-Trichlorophenol
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:532,4-Dichlorophenol
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:532,4-Dimethylphenol
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:532,4-Dinitrophenol
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:532,4-Dinitrotoluene
SW8270D JHV<117 ug/kg dry C 117 111 11/23/15 10:16 11/23/15 14:532,6-Dichlorophenol
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:532,6-Dinitrotoluene
Page 22 of 63Page 22 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 09:30Date/Time Sampled:
SS-9 (11-13)Laboratory Sample ID:Sample I.D.15K0390-11
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:532-Chloronaphthalene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:532-Chlorophenol
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:532-Methylnaphthalene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:532-Naphthylamine
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:532-Nitroaniline
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:532-Nitrophenol
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:533,3'-Dichlorobenzidine
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:533-Methylcholanthrene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:533-Nitroaniline
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:534,6-Dinitro-2-methylphenol
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:534-Aminobiphenyl
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:534-Bromophenyl phenyl ether
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:534-Chloroaniline
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:534-Chlorophenyl phenyl ether
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:534-Nitroaniline
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:534-Nitrophenol
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:537,12-Dimethylbenz (a)
anthracene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Acenaphthene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Acenaphthylene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Acetophenone
SW8270D JHV<117 ug/kg dry C 117 111 11/23/15 10:16 11/23/15 14:53Aniline
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Anthracene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Benzidine
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Benzo (a) anthracene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Benzo (a) pyrene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Benzo (b) fluoranthene
Page 23 of 63Page 23 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 09:30Date/Time Sampled:
SS-9 (11-13)Laboratory Sample ID:Sample I.D.15K0390-11
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Benzo (g,h,i) perylene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Benzo (k) fluoranthene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Benzoic acid
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Benzyl alcohol
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53bis (2-Chloroethoxy) methane
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53bis (2-Chloroethyl) ether
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53bis (2-Chloroisopropyl) ether
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53bis (2-Ethylhexyl) phthalate
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Butyl benzyl phthalate
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Chrysene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Dibenz (a,h) anthracene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Dibenz (a,j) acridine
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Dibenzofuran
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Diethyl phthalate
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Dimethyl phthalate
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Di-n-butyl phthalate
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Di-n-octyl phthalate
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Diphenylamine
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Ethyl methanesulfonate
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Fluoranthene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Fluorene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Hexachlorobenzene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Hexachlorobutadiene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Hexachlorocyclopentadiene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Hexachloroethane
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Indeno (1,2,3-cd) pyrene
Page 24 of 63Page 24 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 09:30Date/Time Sampled:
SS-9 (11-13)Laboratory Sample ID:Sample I.D.15K0390-11
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Isophorone
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53m+p-Cresols
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Methyl methanesulfonate
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Naphthalene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Nitrobenzene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53n-Nitrosodimethylamine
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53n-Nitrosodi-n-butylamine
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53n-Nitrosodi-n-propylamine
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53n-Nitrosodiphenylamine
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53n-Nitrosopiperidine
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53o+m+p-Cresols
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53o-Cresol
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53p-(Dimethylamino)
azobenzene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53p-Chloro-m-cresol
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Pentachloronitrobenzene
(quintozene)
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Pentachlorophenol
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Phenacetin
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Phenanthrene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Phenol
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Pronamide
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Pyrene
SW8270D JHV<117 ug/kg dry 117 111 11/23/15 10:16 11/23/15 14:53Pyridine
35-12563.0 %Surr: 2,4,6-Tribromophenol JHV11SW8270D11/23/15 10:16 11/23/15 14:53
45-10556.6 %Surr: 2-Fluorobiphenyl JHV11SW8270D11/23/15 10:16 11/23/15 14:53
35-10559.7 %Surr: 2-Fluorophenol JHV11SW8270D11/23/15 10:16 11/23/15 14:53
Page 25 of 63Page 25 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 09:30Date/Time Sampled:
SS-9 (11-13)Laboratory Sample ID:Sample I.D.15K0390-11
Analytical Results
Semivolatile Organic Compounds by GCMS
35-10060.2 %Surr: Nitrobenzene-d5 JHV11SW8270D11/23/15 10:16 11/23/15 14:53
40-10056.5 %Surr: Phenol-d5 JHV11SW8270D11/23/15 10:16 11/23/15 14:53
30-12579.7 %Surr: p-Terphenyl-d14 JHV11SW8270D11/23/15 10:16 11/23/15 14:53
Semivolatile Hydrocarbons by GC
SW8015C JHV<13.4 mg/kg dry 13.4 111 11/20/15 11:13 11/23/15 15:58TPH-Semi-Volatiles (DRO)
40-16069.5 %Surr: Pentacosane JHV11SW8015C11/20/15 11:13 11/23/15 15:58
Organochlorine Pesticides and PCBs by GC/ECD
SW8082A SKS<0.135 mg/kg dry 0.135 111 11/23/15 12:07 11/24/15 02:16PCB as Aroclor 1016
SW8082A SKS<0.135 mg/kg dry 0.135 111 11/23/15 12:07 11/24/15 02:16PCB as Aroclor 1221
SW8082A SKS<0.135 mg/kg dry 0.135 111 11/23/15 12:07 11/24/15 02:16PCB as Aroclor 1232
SW8082A SKS<0.135 mg/kg dry 0.135 111 11/23/15 12:07 11/24/15 02:16PCB as Aroclor 1242
SW8082A SKS<0.135 mg/kg dry 0.135 111 11/23/15 12:07 11/24/15 02:16PCB as Aroclor 1248
SW8082A SKS<0.135 mg/kg dry 0.135 111 11/23/15 12:07 11/24/15 02:16PCB as Aroclor 1254
SW8082A SKS<0.135 mg/kg dry 0.135 111 11/23/15 12:07 11/24/15 02:16PCB as Aroclor 1260
30-10570.0 %Surr: DCB SKS11SW8082A11/23/15 12:07 11/24/15 02:16
30-10565.0 %Surr: TCMX SKS11SW8082A11/23/15 12:07 11/24/15 02:16
Wet Chemistry Analysis
SM18 2540G 70.7 %RCV0.10 111 11/19/15 15:24 11/19/15 15:24Percent Solids
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 10:10Date/Time Sampled:
SS-6 (11-13)Laboratory Sample ID:Sample I.D.15K0390-12
Analytical Results
Page 26 of 63Page 26 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 10:10Date/Time Sampled:
SS-6 (11-13)Laboratory Sample ID:Sample I.D.15K0390-12
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C KEW<0.598 mg/kg dry 0.598 112 11/19/15 10:20 11/24/15 16:19Silver
SW6010C KEW<1.20 mg/kg dry 1.20 112 11/19/15 10:20 11/24/15 16:19Arsenic
SW6010C 288 mg/kg dry KEW0.598 112 11/19/15 10:20 11/24/15 16:19Barium
SW6010C 3.87 mg/kg dry KEW0.239 112 11/19/15 10:20 11/24/15 16:19Cadmium
SW6010C 601 mg/kg dry KEW0.598 112 11/19/15 10:20 11/24/15 16:19Chromium
SW7471B 0.012 mg/kg dry MWL0.009 112 11/23/15 15:00 11/24/15 11:30Mercury
SW6010C 2.16 mg/kg dry KEW0.598 112 11/19/15 10:20 11/24/15 16:19Lead
SW6010C KEW<2.99 mg/kg dry 2.99 112 11/19/15 10:20 11/24/15 16:19Selenium
Volatile Hydrocarbons by GC
SW8015C CL<0.10 mg/kg dry 0.10 112 11/19/15 15:51 11/19/15 15:51TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B MKD<6.05 ug/kg dry 6.05 112 11/19/15 15:34 11/19/15 15:34Benzene
SW8260B MKD<6.05 ug/kg dry 6.05 112 11/19/15 15:34 11/19/15 15:34Ethylbenzene
SW8260B MKD<6.05 ug/kg dry 6.05 112 11/19/15 15:34 11/19/15 15:34m+p-Xylenes
SW8260B MKD<6.05 ug/kg dry 6.05 112 11/19/15 15:34 11/19/15 15:34Methyl-t-butyl ether (MTBE)
SW8260B MKD<6.05 ug/kg dry 6.05 112 11/19/15 15:34 11/19/15 15:34Naphthalene
SW8260B MKD<6.05 ug/kg dry 6.05 112 11/19/15 15:34 11/19/15 15:34o-Xylene
SW8260B MKD<6.05 ug/kg dry 6.05 112 11/19/15 15:34 11/19/15 15:34Toluene
SW8260B MKD<18.2 ug/kg dry 18.2 112 11/19/15 15:34 11/19/15 15:34Xylenes, Total
80-120112 %Surr: 1,2-Dichloroethane-d4 MKD12SW8260B11/19/15 15:34 11/19/15 15:34
85-12091.8 %Surr: 4-Bromofluorobenzene MKD12SW8260B11/19/15 15:34 11/19/15 15:34
78-119101 %Surr: Dibromofluoromethane MKD12SW8260B11/19/15 15:34 11/19/15 15:34
85-115102 %Surr: Toluene-d8 MKD12SW8260B11/19/15 15:34 11/19/15 15:34
Page 27 of 63Page 27 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 10:10Date/Time Sampled:
SS-6 (11-13)Laboratory Sample ID:Sample I.D.15K0390-12
Analytical Results
Semivolatile Hydrocarbons by GC
SW8015C JHV<11.6 mg/kg dry 11.6 112 11/20/15 11:13 11/23/15 16:24TPH-Semi-Volatiles (DRO)
40-16067.7 %Surr: Pentacosane JHV12SW8015C11/20/15 11:13 11/23/15 16:24
Wet Chemistry Analysis
SM18 2540G 82.6 %RCV0.10 112 11/19/15 15:26 11/19/15 15:26Percent Solids
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 10:45Date/Time Sampled:
SS-5 (11-13)Laboratory Sample ID:Sample I.D.15K0390-13
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C KEW<0.558 mg/kg dry 0.558 113 11/19/15 10:20 11/24/15 16:24Silver
SW6010C KEW<1.12 mg/kg dry 1.12 113 11/19/15 10:20 11/24/15 16:24Arsenic
SW6010C 25.4 mg/kg dry KEW0.558 113 11/19/15 10:20 11/24/15 16:24Barium
SW6010C 0.846 mg/kg dry KEW0.223 113 11/19/15 10:20 11/24/15 16:24Cadmium
SW6010C 5.23 mg/kg dry KEW0.558 113 11/19/15 10:20 11/24/15 16:24Chromium
SW7471B MWL<0.009 mg/kg dry 0.009 113 11/23/15 15:00 11/24/15 11:32Mercury
SW6010C 3.83 mg/kg dry KEW0.558 113 11/19/15 10:20 11/24/15 16:24Lead
SW6010C KEW<2.79 mg/kg dry 2.79 113 11/19/15 10:20 11/24/15 16:24Selenium
Volatile Hydrocarbons by GC
SW8015C CL<0.10 mg/kg dry 0.10 113 11/19/15 16:14 11/19/15 16:14TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B MKD<5.77 ug/kg dry 5.77 113 11/19/15 15:58 11/19/15 15:58Benzene
SW8260B MKD<5.77 ug/kg dry 5.77 113 11/19/15 15:58 11/19/15 15:58Ethylbenzene
Page 28 of 63Page 28 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/17/2015 10:45Date/Time Sampled:
SS-5 (11-13)Laboratory Sample ID:Sample I.D.15K0390-13
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B MKD<5.77 ug/kg dry 5.77 113 11/19/15 15:58 11/19/15 15:58m+p-Xylenes
SW8260B MKD<5.77 ug/kg dry 5.77 113 11/19/15 15:58 11/19/15 15:58Methyl-t-butyl ether (MTBE)
SW8260B MKD<5.77 ug/kg dry 5.77 113 11/19/15 15:58 11/19/15 15:58Naphthalene
SW8260B MKD<5.77 ug/kg dry 5.77 113 11/19/15 15:58 11/19/15 15:58o-Xylene
SW8260B MKD<5.77 ug/kg dry 5.77 113 11/19/15 15:58 11/19/15 15:58Toluene
SW8260B MKD<17.3 ug/kg dry 17.3 113 11/19/15 15:58 11/19/15 15:58Xylenes, Total
80-120112 %Surr: 1,2-Dichloroethane-d4 MKD13SW8260B11/19/15 15:58 11/19/15 15:58
85-12091.2 %Surr: 4-Bromofluorobenzene MKD13SW8260B11/19/15 15:58 11/19/15 15:58
78-119101 %Surr: Dibromofluoromethane MKD13SW8260B11/19/15 15:58 11/19/15 15:58
85-115104 %Surr: Toluene-d8 MKD13SW8260B11/19/15 15:58 11/19/15 15:58
Semivolatile Hydrocarbons by GC
SW8015C JHV<11.3 mg/kg dry 11.3 113 11/20/15 11:13 11/23/15 16:51TPH-Semi-Volatiles (DRO)
40-16061.7 %Surr: Pentacosane JHV13SW8015C11/20/15 11:13 11/23/15 16:51
Wet Chemistry Analysis
SM18 2540G 86.7 %RCV0.10 113 11/19/15 15:28 11/19/15 15:28Percent Solids
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/10/2015 09:20Date/Time Sampled:
Trip Blank Laboratory Sample ID:Sample I.D.15K0390-14
Analytical Results
Volatile Hydrocarbons by GC
SW8015C CL<0.10 mg/L 0.10 114 11/19/15 12:33 11/19/15 12:33TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
Page 29 of 63Page 29 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Laboratory Order ID: 15K0390
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
11/10/2015 09:20Date/Time Sampled:
Trip Blank Laboratory Sample ID:Sample I.D.15K0390-14
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B MKD<1.00 ug/L 1.00 114 11/20/15 12:00 11/20/15 12:00Benzene
SW8260B MKD<1.00 ug/L 1.00 114 11/20/15 12:00 11/20/15 12:00Ethylbenzene
SW8260B MKD<2.00 ug/L 2.00 114 11/20/15 12:00 11/20/15 12:00m+p-Xylenes
SW8260B MKD<1.00 ug/L 1.00 114 11/20/15 12:00 11/20/15 12:00Methyl-t-butyl ether (MTBE)
SW8260B MKD<1.00 ug/L 1.00 114 11/20/15 12:00 11/20/15 12:00Naphthalene
SW8260B MKD<1.00 ug/L 1.00 114 11/20/15 12:00 11/20/15 12:00o-Xylene
SW8260B MKD<1.00 ug/L 1.00 114 11/20/15 12:00 11/20/15 12:00Toluene
SW8260B MKD<3.00 ug/L 3.00 114 11/20/15 12:00 11/20/15 12:00Xylenes, Total
70-120107 %Surr: 1,2-Dichloroethane-d4 MKD14SW8260B11/20/15 12:00 11/20/15 12:00
75-12088.7 %Surr: 4-Bromofluorobenzene MKD14SW8260B11/20/15 12:00 11/20/15 12:00
80-119102 %Surr: Dibromofluoromethane MKD14SW8260B11/20/15 12:00 11/20/15 12:00
85-12099.7 %Surr: Toluene-d8 MKD14SW8260B11/20/15 12:00 11/20/15 12:00
Page 30 of 63Page 30 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Analytical Summary
Preparation Method:
Preparation Method:
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
EPA200.2/R2.8Preparation Method:Metals (Total) by EPA 6000/7000 Series Methods
15K0390-07 BYK0585 SYK0763SW6010C AK5012050.0 mL / 50.0 mL
15K0390-08 BYK0585 SYK0763SW6010C AK5012050.0 mL / 50.0 mL
15K0390-09 BYK0585 SYK0763SW6010C AK5012050.0 mL / 50.0 mL
15K0390-10 BYK0585 SYK0763SW6010C AK5012050.0 mL / 50.0 mL
15K0390-10RE1 BYK0585 SYK0800SW6010C AK5013150.0 mL / 50.0 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
No Prep HalidesPreparation Method:Wet Chemistry Analysis
15K0390-01 BYK0572 SYK0655SM18 2540G 1.00 g / 1.00 mL
15K0390-02 BYK0572 SYK0655SM18 2540G 1.00 g / 1.00 mL
15K0390-03 BYK0572 SYK0655SM18 2540G 1.00 g / 1.00 mL
15K0390-04 BYK0572 SYK0655SM18 2540G 1.00 g / 1.00 mL
15K0390-05 BYK0572 SYK0655SM18 2540G 1.00 g / 1.00 mL
15K0390-06 BYK0572 SYK0655SM18 2540G 1.00 g / 1.00 mL
15K0390-11 BYK0572 SYK0655SM18 2540G 1.00 g / 1.00 mL
15K0390-12 BYK0572 SYK0655SM18 2540G 1.00 g / 1.00 mL
15K0390-13 BYK0572 SYK0655SM18 2540G 1.00 g / 1.00 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW3050BPreparation Method:Metals (Total) by EPA 6000/7000 Series Methods
15K0390-01 BYK0582 SYK0700SW6010C AK501131.02 g / 50.0 mL
15K0390-02 BYK0582 SYK0799SW6010C AK501311.08 g / 50.0 mL
15K0390-03 BYK0582 SYK0799SW6010C AK501311.08 g / 50.0 mL
15K0390-04 BYK0582 SYK0799SW6010C AK501311.00 g / 50.0 mL
15K0390-05 BYK0582 SYK0799SW6010C AK501311.02 g / 50.0 mL
15K0390-06 BYK0582 SYK0799SW6010C AK501311.03 g / 50.0 mL
15K0390-11 BYK0582 SYK0799SW6010C AK501311.04 g / 50.0 mL
Page 31 of 63Page 31 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
15K0390-12 BYK0582 SYK0799SW6010C AK501311.01 g / 50.0 mL
15K0390-13 BYK0582 SYK0799SW6010C AK501311.04 g / 50.0 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW3550BPreparation Method:Organochlorine Pesticides and PCBs by GC/ECD
15K0390-06 BYK0671 SYK0786SW8082A AK5009332.1 g / 5.00 mL
15K0390-11 BYK0671 SYK0786SW8082A AK5009331.4 g / 5.00 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW3550CPreparation Method:Semivolatile Organic Compounds by GCMS
15K0390-06 BYK0637 SYK0766SW8270D AJ5003930.0 g / 1.00 mL
15K0390-06RE1 BYK0637 SYK0766SW8270D AJ5003930.0 g / 1.00 mL
15K0390-11 BYK0637 SYK0766SW8270D AJ5003930.1 g / 1.00 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW5030BPreparation Method:Volatile Hydrocarbons by GC
15K0390-07 BYK0565 SYK0663SW8015C AJ501535.00 mL / 5.00 mL
15K0390-08 BYK0565 SYK0663SW8015C AJ501535.00 mL / 5.00 mL
15K0390-09 BYK0565 SYK0663SW8015C AJ501535.00 mL / 5.00 mL
15K0390-10 BYK0565 SYK0663SW8015C AJ501535.00 mL / 5.00 mL
15K0390-14 BYK0565 SYK0663SW8015C AJ501535.00 mL / 5.00 mL
SW5030BPreparation Method:Volatile Hydrocarbons by GC
15K0390-01 BYK0566 SYK0665SW8015C AJ500436.35 g / 5.00 mL
15K0390-02 BYK0566 SYK0665SW8015C AJ500436.95 g / 5.00 mL
15K0390-02RE1 BYK0566 SYK0665SW8015C AJ500436.89 g / 5.00 mL
15K0390-03 BYK0566 SYK0665SW8015C AJ500436.75 g / 5.00 mL
15K0390-04 BYK0566 SYK0665SW8015C AJ500436.34 g / 5.00 mL
15K0390-05 BYK0566 SYK0665SW8015C AJ500437.20 g / 5.00 mL
15K0390-05RE1 BYK0566 SYK0665SW8015C AJ500435.08 g / 5.00 mL
15K0390-06 BYK0566 SYK0665SW8015C AJ500437.10 g / 5.00 mL
15K0390-11 BYK0566 SYK0665SW8015C AJ500436.63 g / 5.00 mL
Page 32 of 63Page 32 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
15K0390-11RE1 BYK0566 SYK0665SW8015C AJ500436.28 g / 5.00 mL
15K0390-12 BYK0566 SYK0665SW8015C AJ500437.62 g / 5.00 mL
15K0390-13 BYK0566 SYK0665SW8015C AJ500437.34 g / 5.00 mL
SW5030BPreparation Method:Volatile Organic Compounds by GCMS
15K0390-07 BYK0595 SYK0683SW8260B AK500925.00 mL / 5.00 mL
15K0390-08 BYK0595 SYK0683SW8260B AK500925.00 mL / 5.00 mL
15K0390-09 BYK0595 SYK0683SW8260B AK500925.00 mL / 5.00 mL
15K0390-10 BYK0595 SYK0683SW8260B AK500925.00 mL / 5.00 mL
15K0390-14 BYK0595 SYK0683SW8260B AK500925.00 mL / 5.00 mL
SW5030BPreparation Method:Volatile Organic Compounds by GCMS
15K0390-01 BYK0600 SYK0689SW8260B AK500927.44 g / 5.00 mL
15K0390-02 BYK0600 SYK0689SW8260B AK500926.65 g / 5.00 mL
15K0390-02RE1 BYK0600 SYK0717SW8260B AK500926.89 g / 5.00 mL
15K0390-03 BYK0600 SYK0689SW8260B AK500925.76 g / 5.00 mL
15K0390-04 BYK0600 SYK0689SW8260B AK500927.18 g / 5.00 mL
15K0390-05 BYK0600 SYK0689SW8260B AK500928.69 g / 5.00 mL
15K0390-06 BYK0600 SYK0689SW8260B AK500927.29 g / 5.00 mL
15K0390-11 BYK0600 SYK0689SW8260B AK500925.58 g / 5.00 mL
15K0390-12 BYK0600 SYK0689SW8260B AK500926.34 g / 5.00 mL
15K0390-13 BYK0600 SYK0689SW8260B AK500928.05 g / 5.00 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW7470APreparation Method:Metals (Total) by EPA 6000/7000 Series Methods
15K0390-07 BYK0609 SYK0704SW7470A AK5011720.0 mL / 20.0 mL
15K0390-08 BYK0609 SYK0704SW7470A AK5011720.0 mL / 20.0 mL
15K0390-09 BYK0609 SYK0704SW7470A AK5011720.0 mL / 20.0 mL
15K0390-10 BYK0609 SYK0704SW7470A AK5011720.0 mL / 20.0 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW7471APreparation Method:Metals (Total) by EPA 6000/7000 Series Methods
15K0390-01 BYK0676 SYK0780SW7471B AK501260.512 g / 20.0 mL
15K0390-02 BYK0676 SYK0780SW7471B AK501260.584 g / 20.0 mL
15K0390-03 BYK0676 SYK0780SW7471B AK501260.551 g / 20.0 mL
Page 33 of 63Page 33 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
15K0390-04 BYK0676 SYK0780SW7471B AK501260.530 g / 20.0 mL
15K0390-05 BYK0676 SYK0780SW7471B AK501260.566 g / 20.0 mL
15K0390-06 BYK0676 SYK0780SW7471B AK501260.553 g / 20.0 mL
15K0390-11 BYK0676 SYK0780SW7471B AK501260.500 g / 20.0 mL
15K0390-12 BYK0676 SYK0780SW7471B AK501260.536 g / 20.0 mL
15K0390-13 BYK0676 SYK0780SW7471B AK501260.541 g / 20.0 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW8100Preparation Method:Semivolatile Hydrocarbons by GC
15K0390-01 BYK0594 SYK0759SW8015C AH5015350.5 g / 1.00 mL
15K0390-02 BYK0594 SYK0759SW8015C AH5015351.0 g / 1.00 mL
15K0390-03 BYK0594 SYK0759SW8015C AH5015350.3 g / 1.00 mL
15K0390-04 BYK0594 SYK0759SW8015C AH5015353.4 g / 1.00 mL
15K0390-05 BYK0594 SYK0759SW8015C AH5015350.1 g / 1.00 mL
15K0390-06 BYK0594 SYK0759SW8015C AH5015350.7 g / 1.00 mL
15K0390-11 BYK0594 SYK0759SW8015C AH5015352.8 g / 1.00 mL
15K0390-12 BYK0594 SYK0759SW8015C AH5015352.2 g / 1.00 mL
15K0390-13 BYK0594 SYK0759SW8015C AH5015351.2 g / 1.00 mL
SW8100Preparation Method:Semivolatile Hydrocarbons by GC
15K0390-07 BYK0646 SYK0760SW8015C AJ50157990 mL / 1.00 mL
15K0390-08 BYK0646 SYK0760SW8015C AJ501571000 mL / 1.00 mL
15K0390-09 BYK0646 SYK0760SW8015C AJ501571000 mL / 1.00 mL
15K0390-10 BYK0646 SYK0760SW8015C AJ50157980 mL / 1.00 mL
Page 34 of 63Page 34 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals (Total) by EPA 6000/7000 Series Methods - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0582 - SW3050B
Blank (BYK0582-BLK1)Prepared: 11/19/2015 Analyzed: 11/20/2015
2.48 mg/kg wet<2.48 mg/kg wetSelenium
0.496 mg/kg wet<0.496 mg/kg wetLead
0.496 mg/kg wet<0.496 mg/kg wetChromium
0.992 mg/kg wet<0.992 mg/kg wetArsenic
0.496 mg/kg wet<0.496 mg/kg wetSilver
0.198 mg/kg wet<0.198 mg/kg wetCadmium
0.496 mg/kg wet<0.496 mg/kg wetBarium
LCS (BYK0582-BS1)Prepared: 11/19/2015 Analyzed: 11/20/2015
0.198 99.0 80-12099.8mg/kg wet98.8 mg/kg wetCadmium
0.495 4.95 80-12099.4mg/kg wet4.92 mg/kg wetSilver
2.48 99.0 80-12097.1mg/kg wet96.2 mg/kg wetSelenium
0.495 99.0 80-120105mg/kg wet104 mg/kg wetLead
0.495 99.0 80-120103mg/kg wet102 mg/kg wetChromium
0.990 99.0 80-120103mg/kg wet102 mg/kg wetArsenic
0.495 99.0 80-120103mg/kg wet102 mg/kg wetBarium
LCS Dup (BYK0582-BSD1)Prepared: 11/19/2015 Analyzed: 11/20/2015
0.482 4.82 2080-12087.5 15.5mg/kg wet4.21 mg/kg wetSilver
0.482 96.3 2080-12091.3 15.2mg/kg wet87.9 mg/kg wetBarium
0.482 96.3 2080-12090.7 15.4mg/kg wet87.3 mg/kg wetChromium
0.482 96.3 2080-12092.8 14.6mg/kg wet89.4 mg/kg wetLead
0.963 96.3 2080-12090.8 15.4mg/kg wet87.4 mg/kg wetArsenic
2.41 96.3 2080-12085.7 15.2mg/kg wet82.5 mg/kg wetSelenium
0.193 96.3 2080-12088.1 15.1mg/kg wet84.9 mg/kg wetCadmium
Matrix Spike (BYK0582-MS1)Prepared: 11/19/2015 Analyzed: 11/20/2015Source: 15K0390-01
3.12 125 75-12577.8mg/kg dry97.1 mg/kg dry <3.12 mg/kg drySelenium
0.624 125 75-12583.3mg/kg dry244 mg/kg dry 140 mg/kg dryBarium
1.25 125 75-12568.7mg/kg dry85.8 mg/kg dry <1.25 mg/kg dryArsenic M
0.250 125 75-12587.7mg/kg dry112 mg/kg dry 2.96 mg/kg dryCadmium
0.624 125 75-12587.9mg/kg dry111 mg/kg dry 1.37 mg/kg dryLead
0.624 125 75-12595.3mg/kg dry145 mg/kg dry 26.0 mg/kg dryChromium
Page 35 of 63Page 35 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals (Total) by EPA 6000/7000 Series Methods - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0582 - SW3050B
Matrix Spike (BYK0582-MS1)Prepared: 11/19/2015 Analyzed: 11/20/2015Source: 15K0390-01
0.624 6.24 75-12583.6mg/kg dry5.22 mg/kg dry <0.624 mg/kg drySilver
Matrix Spike (BYK0582-MS2)Prepared: 11/19/2015 Analyzed: 11/24/2015Source: 15K0390-05
0.246 123 75-12596.4mg/kg dry122 mg/kg dry 2.85 mg/kg dryCadmium
0.615 123 75-12595.8mg/kg dry301 mg/kg dry 183 mg/kg dryBarium
1.23 123 75-12573.4mg/kg dry90.3 mg/kg dry <1.23 mg/kg dryArsenic M
3.08 123 75-12585.1mg/kg dry105 mg/kg dry <3.08 mg/kg drySelenium
0.615 123 75-12598.9mg/kg dry122 mg/kg dry <0.615 mg/kg dryLead
0.615 123 75-125102mg/kg dry134 mg/kg dry 8.71 mg/kg dryChromium
0.615 6.15 75-12591.3mg/kg dry5.62 mg/kg dry <0.615 mg/kg drySilver
Matrix Spike Dup (BYK0582-MSD1)Prepared: 11/19/2015 Analyzed: 11/20/2015Source: 15K0390-01
0.239 119 2075-12585.9 6.44mg/kg dry105 mg/kg dry 2.96 mg/kg dryCadmium
0.597 5.97 2075-12580.5 8.31mg/kg dry4.81 mg/kg dry <0.597 mg/kg drySilver
0.597 119 2075-12586.3 6.26mg/kg dry104 mg/kg dry 1.37 mg/kg dryLead
2.98 119 2075-12576.6 6.11mg/kg dry91.4 mg/kg dry <2.98 mg/kg drySelenium
1.19 119 2075-12567.8 5.85mg/kg dry80.9 mg/kg dry <1.19 mg/kg dryArsenic M
0.597 119 2075-12560.1 14.2mg/kg dry212 mg/kg dry 140 mg/kg dryBarium M
0.597 119 2075-12592.6 5.96mg/kg dry137 mg/kg dry 26.0 mg/kg dryChromium
Matrix Spike Dup (BYK0582-MSD2)Prepared: 11/19/2015 Analyzed: 11/24/2015Source: 15K0390-05
0.574 5.74 2075-12591.0 7.29mg/kg dry5.22 mg/kg dry <0.574 mg/kg drySilver
1.15 115 2075-12563.0 22.1mg/kg dry72.3 mg/kg dry <1.15 mg/kg dryArsenic M, P
2.87 115 2075-12576.5 17.5mg/kg dry87.9 mg/kg dry <2.87 mg/kg drySelenium
0.230 115 2075-12587.5 16.2mg/kg dry103 mg/kg dry 2.85 mg/kg dryCadmium
0.574 115 2075-12590.9 15.3mg/kg dry104 mg/kg dry <0.574 mg/kg dryLead
0.574 115 2075-12593.4 14.2mg/kg dry116 mg/kg dry 8.71 mg/kg dryChromium
0.574 115 2075-125155 18.3mg/kg dry361 mg/kg dry 183 mg/kg dryBarium M
Page 36 of 63Page 36 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals (Total) by EPA 6000/7000 Series Methods - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0585 - EPA200.2/R2.8
Blank (BYK0585-BLK1)Prepared: 11/19/2015 Analyzed: 11/23/2015
0.0100 mg/L<0.0100 mg/LArsenic
0.0100 mg/L<0.0100 mg/LBarium
0.0050 mg/L<0.0050 mg/LCadmium
0.0100 mg/L<0.0100 mg/LChromium
0.0100 mg/L<0.0100 mg/LLead
0.0500 mg/L<0.0500 mg/LSelenium
0.0100 mg/L<0.0100 mg/LSilver
LCS (BYK0585-BS1)Prepared: 11/19/2015 Analyzed: 11/23/2015
0.0100 0.500 80-120110mg/L0.550 mg/LArsenic
0.0100 0.500 80-120108mg/L0.541 mg/LBarium
0.0050 0.500 80-120108mg/L0.540 mg/LCadmium
0.0100 0.500 80-120108mg/L0.541 mg/LChromium
0.0100 0.500 80-120109mg/L0.545 mg/LLead
0.0500 0.500 80-120105mg/L0.523 mg/LSelenium
0.0100 0.100 80-120107mg/L0.107 mg/LSilver
LCS Dup (BYK0585-BSD1)Prepared: 11/19/2015 Analyzed: 11/23/2015
0.0100 0.500 2080-120107 2.62mg/L0.535 mg/LArsenic
0.0100 0.500 2080-120106 2.11mg/L0.530 mg/LBarium
0.0050 0.500 2080-120105 2.64mg/L0.526 mg/LCadmium
0.0100 0.500 2080-120106 2.38mg/L0.528 mg/LChromium
0.0100 0.500 2080-120107 1.53mg/L0.537 mg/LLead
0.0500 0.500 2080-120104 1.12mg/L0.518 mg/LSelenium
0.0100 0.100 2080-120105 1.83mg/L0.105 mg/LSilver
Matrix Spike (BYK0585-MS1)Prepared: 11/19/2015 Analyzed: 11/23/2015Source: 15K0390-09
0.0100 0.500 75-125108mg/L0.553 mg/L 0.0105 mg/LArsenic
0.0100 0.500 75-125108mg/L0.659 mg/L 0.121 mg/LBarium
0.0050 0.500 75-125106mg/L0.531 mg/L <0.0050 mg/LCadmium
0.0100 0.500 75-125108mg/L0.542 mg/L <0.0100 mg/LChromium
0.0100 0.500 75-125107mg/L0.536 mg/L <0.0100 mg/LLead
0.0500 0.500 75-125104mg/L0.522 mg/L <0.0500 mg/LSelenium
Page 37 of 63Page 37 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals (Total) by EPA 6000/7000 Series Methods - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0585 - EPA200.2/R2.8
Matrix Spike (BYK0585-MS1)Prepared: 11/19/2015 Analyzed: 11/23/2015Source: 15K0390-09
0.0100 0.100 75-125108mg/L0.108 mg/L <0.0100 mg/LSilver
Matrix Spike (BYK0585-MS2)Prepared: 11/19/2015 Analyzed: 11/23/2015Source: 15K0414-09
0.0100 0.500 75-125113mg/L0.565 mg/L <0.0100 mg/LArsenic
0.0100 0.500 75-125107mg/L0.542 mg/L <0.0100 mg/LBarium
0.0050 0.500 75-125105mg/L0.527 mg/L <0.0050 mg/LCadmium
0.0100 0.500 75-125107mg/L0.535 mg/L <0.0100 mg/LChromium
0.0100 0.500 75-125110mg/L0.548 mg/L <0.0100 mg/LLead
0.0500 0.500 75-125106mg/L0.528 mg/L <0.0500 mg/LSelenium
0.0100 0.100 75-125106mg/L0.106 mg/L <0.0100 mg/LSilver
Matrix Spike Dup (BYK0585-MSD1)Prepared: 11/19/2015 Analyzed: 11/23/2015Source: 15K0390-09
0.0100 0.500 2075-125108 0.473mg/L0.550 mg/L 0.0105 mg/LArsenic
0.0100 0.500 2075-125106 0.811mg/L0.654 mg/L 0.121 mg/LBarium
0.0050 0.500 2075-125105 1.25mg/L0.524 mg/L <0.0050 mg/LCadmium
0.0100 0.500 2075-125106 1.34mg/L0.535 mg/L <0.0100 mg/LChromium
0.0100 0.500 2075-125107 0.0607mg/L0.536 mg/L <0.0100 mg/LLead
0.0500 0.500 2075-125106 1.50mg/L0.530 mg/L <0.0500 mg/LSelenium
0.0100 0.100 2075-125106 1.82mg/L0.106 mg/L <0.0100 mg/LSilver
Matrix Spike Dup (BYK0585-MSD2)Prepared: 11/19/2015 Analyzed: 11/23/2015Source: 15K0414-09
0.0100 0.500 2075-125114 0.539mg/L0.568 mg/L <0.0100 mg/LArsenic
0.0100 0.500 2075-125107 0.646mg/L0.545 mg/L <0.0100 mg/LBarium
0.0050 0.500 2075-125106 1.01mg/L0.532 mg/L <0.0050 mg/LCadmium
0.0100 0.500 2075-125108 0.840mg/L0.540 mg/L <0.0100 mg/LChromium
0.0100 0.500 2075-125110 0.0900mg/L0.549 mg/L <0.0100 mg/LLead
0.0500 0.500 2075-125105 0.159mg/L0.527 mg/L <0.0500 mg/LSelenium
0.0100 0.100 2075-125108 1.44mg/L0.108 mg/L <0.0100 mg/LSilver
Page 38 of 63Page 38 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals (Total) by EPA 6000/7000 Series Methods - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0609 - SW7470A
Blank (BYK0609-BLK1)Prepared & Analyzed: 11/20/2015
0.00020 mg/L<0.00020 mg/LMercury
LCS (BYK0609-BS1)Prepared & Analyzed: 11/20/2015
0.00020 0.00250 80-120105mg/L0.00261 mg/LMercury
LCS Dup (BYK0609-BSD1)Prepared & Analyzed: 11/20/2015
0.00020 0.00250 2080-120104 0.951mg/L0.00259 mg/LMercury
Matrix Spike (BYK0609-MS1)Prepared & Analyzed: 11/20/2015Source: 15K0390-09
0.00020 0.00250 80-12053.5mg/L0.00134 mg/L <0.00020 mg/LMercury M
Matrix Spike (BYK0609-MS2)Prepared & Analyzed: 11/20/2015Source: 15K0322-04
0.00020 0.00250 80-12083.7mg/L0.00209 mg/L <0.00020 mg/LMercury
Matrix Spike (BYK0609-MS3)Prepared & Analyzed: 11/20/2015Source: 15K0321-03
0.00020 0.00250 80-12094.4mg/L0.00236 mg/L <0.00020 mg/LMercury
Matrix Spike (BYK0609-MS4)Prepared & Analyzed: 11/20/2015Source: 15K0321-04
0.00020 0.00250 80-12095.4mg/L0.00239 mg/L <0.00020 mg/LMercury
Matrix Spike Dup (BYK0609-MSD1)Prepared & Analyzed: 11/20/2015Source: 15K0390-09
0.00020 0.00250 2080-12056.8 6.05mg/L0.00142 mg/L <0.00020 mg/LMercury M
Matrix Spike Dup (BYK0609-MSD2)Prepared & Analyzed: 11/20/2015Source: 15K0322-04
0.00020 0.00250 2080-12082.3 1.67mg/L0.00206 mg/L <0.00020 mg/LMercury
Matrix Spike Dup (BYK0609-MSD3)Prepared & Analyzed: 11/20/2015Source: 15K0321-03
0.00020 0.00250 2080-12092.4 2.18mg/L0.00231 mg/L <0.00020 mg/LMercury
Page 39 of 63Page 39 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals (Total) by EPA 6000/7000 Series Methods - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0609 - SW7470A
Matrix Spike Dup (BYK0609-MSD4)Prepared & Analyzed: 11/20/2015Source: 15K0321-04
0.00020 0.00250 2080-12094.3 1.20mg/L0.00236 mg/L <0.00020 mg/LMercury
Batch BYK0676 - SW7471A
Blank (BYK0676-BLK1)Prepared: 11/23/2015 Analyzed: 11/24/2015
0.008 mg/kg wet<0.008 mg/kg wetMercury
LCS (BYK0676-BS1)Prepared: 11/23/2015 Analyzed: 11/24/2015
0.008 0.0949 80-120109mg/kg wet0.103 mg/kg wetMercury
LCS Dup (BYK0676-BSD1)Prepared: 11/23/2015 Analyzed: 11/24/2015
0.008 0.0978 2080-120110 4.30mg/kg wet0.108 mg/kg wetMercury
Matrix Spike (BYK0676-MS1)Prepared: 11/23/2015 Analyzed: 11/24/2015Source: 15K0390-01
0.010 0.125 80-120114mg/kg dry0.142 mg/kg dry <0.010 mg/kg dryMercury
Matrix Spike (BYK0676-MS2)Prepared: 11/23/2015 Analyzed: 11/24/2015Source: 15K0352-08
0.008 0.0916 80-120110mg/kg wet0.119 mg/kg wet 0.018 mg/kg wetMercury
Matrix Spike Dup (BYK0676-MSD1)Prepared: 11/23/2015 Analyzed: 11/24/2015Source: 15K0390-01
0.009 0.112 2080-120118 7.50mg/kg dry0.132 mg/kg dry <0.009 mg/kg dryMercury
Matrix Spike Dup (BYK0676-MSD2)Prepared: 11/23/2015 Analyzed: 11/24/2015Source: 15K0352-08
0.008 0.0876 2080-120129 9.57mg/kg wet0.131 mg/kg wet 0.018 mg/kg wetMercury M
Page 40 of 63Page 40 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Hydrocarbons by GC - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0565 - SW5030B
Blank (BYK0565-BLK1)Prepared & Analyzed: 11/19/2015
0.10 mg/L<0.10 mg/LTPH-Volatiles (GRO)
LCS (BYK0565-BS1)Prepared & Analyzed: 11/19/2015
0.10 1.00 70-13097.6mg/L0.98 mg/LTPH-Volatiles (GRO)
LCS Dup (BYK0565-BSD1)Prepared & Analyzed: 11/19/2015
0.10 1.00 2070-13097.3 0.308mg/L0.97 mg/LTPH-Volatiles (GRO)
Duplicate (BYK0565-DUP1)Prepared & Analyzed: 11/19/2015Source: 15K0407-01
0.10 20NAmg/L<0.10 mg/L <0.10 mg/LTPH-Volatiles (GRO)
Matrix Spike (BYK0565-MS1)Prepared & Analyzed: 11/19/2015Source: 15K0401-02
0.10 1.00 70-13098.6mg/L0.99 mg/L <0.10 mg/LTPH-Volatiles (GRO)
Matrix Spike Dup (BYK0565-MSD1)Prepared & Analyzed: 11/19/2015Source: 15K0401-02
0.10 1.00 2070-13099.1 0.535mg/L0.99 mg/L <0.10 mg/LTPH-Volatiles (GRO)
Batch BYK0566 - SW5030B
Blank (BYK0566-BLK1)Prepared & Analyzed: 11/19/2015
0.10 mg/kg wet<0.10 mg/kg wetTPH-Volatiles (GRO)
LCS (BYK0566-BS1)Prepared & Analyzed: 11/19/2015
0.10 0.973 70-130106mg/kg wet1.03 mg/kg wetTPH-Volatiles (GRO)
LCS Dup (BYK0566-BSD1)Prepared & Analyzed: 11/19/2015
0.10 0.978 2070-130107 1.20mg/kg wet1.04 mg/kg wetTPH-Volatiles (GRO)
Page 41 of 63Page 41 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Hydrocarbons by GC - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0566 - SW5030B
Duplicate (BYK0566-DUP1)Prepared & Analyzed: 11/19/2015Source: 15K0438-01
0.10 20NAmg/kg dry<0.10 mg/kg dry <0.10 mg/kg dryTPH-Volatiles (GRO)
Duplicate (BYK0566-DUP2)Prepared & Analyzed: 11/19/2015Source: 15K0449-03
0.10 20NAmg/kg wet<0.10 mg/kg wet <0.10 mg/kg wetTPH-Volatiles (GRO)
Matrix Spike (BYK0566-MS1)Prepared & Analyzed: 11/20/2015Source: 15K0449-03
0.10 0.998 70-13090.9mg/kg wet0.91 mg/kg wet <0.10 mg/kg wetTPH-Volatiles (GRO)
Matrix Spike Dup (BYK0566-MSD1)Prepared & Analyzed: 11/20/2015Source: 15K0449-03
0.10 0.965 2070-13082.0 13.5mg/kg wet0.79 mg/kg wet <0.10 mg/kg wetTPH-Volatiles (GRO)
Page 42 of 63Page 42 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0595 - SW5030B
Blank (BYK0595-BLK1)Prepared & Analyzed: 11/20/2015
1.00 ug/L<1.00 ug/LBenzene
1.00 ug/L<1.00 ug/LEthylbenzene
2.00 ug/L<2.00 ug/Lm+p-Xylenes
1.00 ug/L<1.00 ug/LMethyl-t-butyl ether (MTBE)
1.00 ug/L<1.00 ug/LNaphthalene
1.00 ug/L<1.00 ug/Lo-Xylene
1.00 ug/L<1.00 ug/LToluene
3.00 ug/L<3.00 ug/LXylenes, Total
50.0 70-120Surr: 1,2-Dichloroethane-d4 10753.5 ug/L
50.0 75-120Surr: 4-Bromofluorobenzene 88.144.1 ug/L
50.0 80-119Surr: Dibromofluoromethane 97.748.8 ug/L
50.0 85-120Surr: Toluene-d8 99.449.7 ug/L
LCS (BYK0595-BS1)Prepared & Analyzed: 11/20/2015
1 50.0 80-120102ug/L50.8 ug/LBenzene
1 50.0 75-125102ug/L51.0 ug/LEthylbenzene
2 100 75-130109ug/L109 ug/Lm+p-Xylenes
1 50.0 65-12593.7ug/L46.8 ug/LMethyl-t-butyl ether (MTBE)
1 50.0 55-140124ug/L62.0 ug/LNaphthalene
1 50.0 80-120109ug/L54.6 ug/Lo-Xylene
1 50.0 75-12099.3ug/L49.7 ug/LToluene
50.0 70-120Surr: 1,2-Dichloroethane-d4 10351.7 ug/L
50.0 75-120Surr: 4-Bromofluorobenzene 92.546.2 ug/L
50.0 80-119Surr: Dibromofluoromethane 99.849.9 ug/L
50.0 85-120Surr: Toluene-d8 99.349.7 ug/L
LCS Dup (BYK0595-BSD1)Prepared & Analyzed: 11/20/2015
1 50.0 3080-120101 0.738ug/L50.5 ug/LBenzene
1 50.0 3075-125102 0.119ug/L51.1 ug/LEthylbenzene
2 100 3075-130108 0.708ug/L108 ug/Lm+p-Xylenes
1 50.0 3065-125101 7.19ug/L50.3 ug/LMethyl-t-butyl ether (MTBE)
1 50.0 3055-140124 0.284ug/L61.9 ug/LNaphthalene
Page 43 of 63Page 43 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0595 - SW5030B
LCS Dup (BYK0595-BSD1)Prepared & Analyzed: 11/20/2015
1 50.0 3080-120110 0.775ug/L55.1 ug/Lo-Xylene
1 50.0 3075-12099.0 0.359ug/L49.5 ug/LToluene
50.0 70-120Surr: 1,2-Dichloroethane-d4 10552.5 ug/L
50.0 75-120Surr: 4-Bromofluorobenzene 92.146.0 ug/L
50.0 80-119Surr: Dibromofluoromethane 98.949.5 ug/L
50.0 85-120Surr: Toluene-d8 96.048.0 ug/L
Duplicate (BYK0595-DUP1)Prepared & Analyzed: 11/20/2015Source: 15K0471-02RE1
1.00 306.49ug/L6.92 ug/L 6.48 ug/LBenzene
1.00 30NAug/L<1.00 ug/L <1.00 ug/LEthylbenzene
2.00 30NAug/L<2.00 ug/L <2.00 ug/Lm+p-Xylenes J
1.00 30NAug/L<1.00 ug/L <1.00 ug/LMethyl-t-butyl ether (MTBE)
1.00 30NAug/L<1.00 ug/L <1.00 ug/LNaphthalene
1.00 307.51ug/L2.33 ug/L 2.52 ug/Lo-Xylene
1.00 300.276ug/L2.17 ug/L 2.18 ug/LToluene
3.00 308.94ug/L3.13 ug/L 3.42 ug/LXylenes, Total
50.0 70-120Surr: 1,2-Dichloroethane-d4 11155.6 ug/L
50.0 75-120Surr: 4-Bromofluorobenzene 90.345.1 ug/L
50.0 80-119Surr: Dibromofluoromethane 95.747.9 ug/L
50.0 85-120Surr: Toluene-d8 10150.7 ug/L
Matrix Spike (BYK0595-MS1)Prepared & Analyzed: 11/20/2015Source: 15K0390-10
1 50.0 80-12098.0ug/L49.0 ug/L <1 ug/LBenzene
1 50.0 75-12597.3ug/L48.7 ug/L <1 ug/LEthylbenzene
2 100 75-130103ug/L103 ug/L <2 ug/Lm+p-Xylenes
1 50.0 65-12595.7ug/L47.9 ug/L <1 ug/LMethyl-t-butyl ether (MTBE)
1 50.0 55-140121ug/L60.6 ug/L <1 ug/LNaphthalene
1 50.0 80-120105ug/L52.5 ug/L <1 ug/Lo-Xylene
1 50.0 75-12095.6ug/L47.8 ug/L <1 ug/LToluene
50.0 70-120Surr: 1,2-Dichloroethane-d4 10854.2 ug/L
50.0 75-120Surr: 4-Bromofluorobenzene 93.546.7 ug/L
Page 44 of 63Page 44 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0595 - SW5030B
Matrix Spike (BYK0595-MS1)Prepared & Analyzed: 11/20/2015Source: 15K0390-10
50.0 80-119Surr: Dibromofluoromethane 10452.2 ug/L
50.0 85-120Surr: Toluene-d8 97.848.9 ug/L
Matrix Spike Dup (BYK0595-MSD1)Prepared & Analyzed: 11/20/2015Source: 15K0390-10
1 50.0 3080-120103 4.51ug/L51.3 ug/L <1 ug/LBenzene
1 50.0 3075-125102 4.91ug/L51.1 ug/L <1 ug/LEthylbenzene
2 100 3075-130108 4.74ug/L108 ug/L <2 ug/Lm+p-Xylenes
1 50.0 3065-125102 6.04ug/L50.8 ug/L <1 ug/LMethyl-t-butyl ether (MTBE)
1 50.0 3055-140127 4.94ug/L63.7 ug/L <1 ug/LNaphthalene
1 50.0 3080-120108 3.12ug/L54.2 ug/L <1 ug/Lo-Xylene
1 50.0 3075-12099.8 4.33ug/L49.9 ug/L <1 ug/LToluene
50.0 70-120Surr: 1,2-Dichloroethane-d4 10552.3 ug/L
50.0 75-120Surr: 4-Bromofluorobenzene 94.047.0 ug/L
50.0 80-119Surr: Dibromofluoromethane 10150.7 ug/L
50.0 85-120Surr: Toluene-d8 98.049.0 ug/L
Batch BYK0600 - SW5030B
Blank (BYK0600-BLK1)Prepared & Analyzed: 11/19/2015
5.00 ug/kg wet<5.00 ug/kg wetBenzene
5.00 ug/kg wet<5.00 ug/kg wetEthylbenzene
5.00 ug/kg wet<5.00 ug/kg wetm+p-Xylenes
5.00 ug/kg wet<5.00 ug/kg wetMethyl-t-butyl ether (MTBE)
5.00 ug/kg wet<5.00 ug/kg wetNaphthalene
5.00 ug/kg wet<5.00 ug/kg weto-Xylene
5.00 ug/kg wet<5.00 ug/kg wetToluene
15.0 ug/kg wet<15.0 ug/kg wetXylenes, Total
49.9 80-120Surr: 1,2-Dichloroethane-d4 94.747.2 ug/kg wet
49.9 85-120Surr: 4-Bromofluorobenzene 94.747.3 ug/kg wet
49.9 78-119Surr: Dibromofluoromethane 97.148.5 ug/kg wet
49.9 85-115Surr: Toluene-d8 10150.4 ug/kg wet
Page 45 of 63Page 45 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0600 - SW5030B
LCS (BYK0600-BS1)Prepared & Analyzed: 11/19/2015
5 50.0 75-125105ug/L52.5 ug/LBenzene
5 50.0 75-12590.4ug/L45.2 ug/LEthylbenzene
5 100 80-12595.3ug/L95.3 ug/Lm+p-Xylenes
5 50.0 65-125107ug/L53.5 ug/LMethyl-t-butyl ether (MTBE)
5 50.0 40-125105ug/L52.7 ug/LNaphthalene
5 50.0 75-12598.6ug/L49.3 ug/Lo-Xylene
5 50.0 70-125101ug/L50.7 ug/LToluene
50.0 80-120Surr: 1,2-Dichloroethane-d4 98.049.0 ug/kg wet
50.0 85-120Surr: 4-Bromofluorobenzene 98.949.5 ug/kg wet
50.0 78-119Surr: Dibromofluoromethane 95.147.5 ug/kg wet
50.0 85-115Surr: Toluene-d8 98.049.0 ug/kg wet
LCS Dup (BYK0600-BSD1)Prepared & Analyzed: 11/19/2015
5 50.0 3075-125113 7.37ug/L56.5 ug/LBenzene
5 50.0 3075-12596.1 6.08ug/L48.0 ug/LEthylbenzene
5 100 3080-125101 6.25ug/L101 ug/Lm+p-Xylenes
5 50.0 3065-125111 3.67ug/L55.5 ug/LMethyl-t-butyl ether (MTBE)
5 50.0 3040-125109 3.14ug/L54.4 ug/LNaphthalene
5 50.0 3075-125104 5.47ug/L52.1 ug/Lo-Xylene
5 50.0 3070-125107 5.88ug/L53.7 ug/LToluene
49.7 80-120Surr: 1,2-Dichloroethane-d4 96.948.2 ug/kg wet
49.7 85-120Surr: 4-Bromofluorobenzene 96.948.2 ug/kg wet
49.7 78-119Surr: Dibromofluoromethane 99.549.5 ug/kg wet
49.7 85-115Surr: Toluene-d8 10049.9 ug/kg wet
Duplicate (BYK0600-DUP1)Prepared & Analyzed: 11/19/2015Source: 15K0352-05
5.00 30NAug/kg wet<5.00 ug/kg wet <5.00 ug/kg wetBenzene
5.00 30NAug/kg wet<5.00 ug/kg wet <5.00 ug/kg wetEthylbenzene
5.00 30NAug/kg wet<5.00 ug/kg wet <5.00 ug/kg wetm+p-Xylenes
5.00 30NAug/kg wet<5.00 ug/kg wet <5.00 ug/kg wetMethyl-t-butyl ether (MTBE)
5.00 30NAug/kg wet<5.00 ug/kg wet <5.00 ug/kg wetNaphthalene
5.00 30NAug/kg wet<5.00 ug/kg wet <5.00 ug/kg weto-Xylene
Page 46 of 63Page 46 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0600 - SW5030B
Duplicate (BYK0600-DUP1)Prepared & Analyzed: 11/19/2015Source: 15K0352-05
5.00 30NAug/kg wet<5.00 ug/kg wet <5.00 ug/kg wetToluene
15.0 30NAug/kg wet<15.0 ug/kg wet <15.0 ug/kg wetXylenes, Total
48.8 80-120Surr: 1,2-Dichloroethane-d4 10249.7 ug/kg wet
48.8 85-120Surr: 4-Bromofluorobenzene 96.347.0 ug/kg wet
48.8 78-119Surr: Dibromofluoromethane 96.247.0 ug/kg wet
48.8 85-115Surr: Toluene-d8 10350.5 ug/kg wet
Duplicate (BYK0600-DUP2)Prepared & Analyzed: 11/20/2015Source: 15K0390-02RE1
351 30NAug/kg dry<351 ug/kg dry <351 ug/kg dryBenzene
351 30NAug/kg dry<351 ug/kg dry <351 ug/kg dryEthylbenzene
351 30NAug/kg dry<351 ug/kg dry <351 ug/kg drym+p-Xylenes
351 30NAug/kg dry<351 ug/kg dry <351 ug/kg dryMethyl-t-butyl ether (MTBE)
7.02 30NAug/kg dry<7.02 ug/kg dry <7.02 ug/kg dryNaphthalene
351 30NAug/kg dry<351 ug/kg dry <351 ug/kg dryo-Xylene
351 30NAug/kg dry<351 ug/kg dry <351 ug/kg dryToluene
21.1 30NAug/kg dry<21.1 ug/kg dry <21.1 ug/kg dryXylenes, Total
51.0 80-120Surr: 1,2-Dichloroethane-d4 10654.0 ug/kg dry
51.0 85-120Surr: 4-Bromofluorobenzene 88.245.0 ug/kg dry
51.0 78-119Surr: Dibromofluoromethane 10151.6 ug/kg dry
51.0 85-115Surr: Toluene-d8 99.250.5 ug/kg dry
Matrix Spike (BYK0600-MS1)Prepared & Analyzed: 11/19/2015Source: 15K0352-08
5 50.0 75-12560.6ug/L30.3 ug/L <5 ug/LBenzene M
5 50.0 75-12548.7ug/L24.4 ug/L <5 ug/LEthylbenzene M
5 100 80-12548.6ug/L48.6 ug/L <5 ug/Lm+p-Xylenes M
5 50.0 65-12562.3ug/L31.2 ug/L <5 ug/LMethyl-t-butyl ether (MTBE)M
5 50.0 40-12522.6ug/L11.7 ug/L <5 ug/LNaphthalene M
5 50.0 75-12550.8ug/L25.6 ug/L <5 ug/Lo-Xylene M
5 50.0 70-12555.7ug/L27.9 ug/L <5 ug/LToluene M
47.3 80-120Surr: 1,2-Dichloroethane-d4 10750.7 ug/kg wet
47.3 85-120Surr: 4-Bromofluorobenzene 92.944.0 ug/kg wet
Page 47 of 63Page 47 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0600 - SW5030B
Matrix Spike (BYK0600-MS1)Prepared & Analyzed: 11/19/2015Source: 15K0352-08
47.3 78-119Surr: Dibromofluoromethane 10248.2 ug/kg wet
47.3 85-115Surr: Toluene-d8 98.046.4 ug/kg wet
Matrix Spike Dup (BYK0600-MSD1)Prepared & Analyzed: 11/19/2015Source: 15K0352-08
5 50.0 3075-12545.1 29.3ug/L22.5 ug/L <5 ug/LBenzene M
5 50.0 3075-12533.2 38.0ug/L16.6 ug/L <5 ug/LEthylbenzene M, P
5 100 3080-12533.1 37.8ug/L33.1 ug/L <5 ug/Lm+p-Xylenes P, M
5 50.0 3065-12559.8 4.14ug/L29.9 ug/L <5 ug/LMethyl-t-butyl ether (MTBE)M
5 50.0 3040-12522.6 0.0598ug/L11.7 ug/L <5 ug/LNaphthalene M
5 50.0 3075-12536.4 32.7ug/L18.4 ug/L <5 ug/Lo-Xylene M, P
5 50.0 3070-12539.5 34.1ug/L19.7 ug/L <5 ug/LToluene M, P
48.6 80-120Surr: 1,2-Dichloroethane-d4 11555.9 ug/kg wet
48.6 85-120Surr: 4-Bromofluorobenzene 95.046.2 ug/kg wet
48.6 78-119Surr: Dibromofluoromethane 10249.5 ug/kg wet
48.6 85-115Surr: Toluene-d8 10249.8 ug/kg wet
Page 48 of 63Page 48 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0637 - SW3550C
Blank (BYK0637-BLK1)Prepared & Analyzed: 11/23/2015
83.3 ug/kg wet<83.3 ug/kg wet1,2,4,5-Tetrachlorobenzene
83.3 ug/kg wet<83.3 ug/kg wet1,2,4-Trichlorobenzene
83.3 ug/kg wet<83.3 ug/kg wet1,2-Dichlorobenzene
83.3 ug/kg wet<83.3 ug/kg wet1,2-Diphenylhydrazine
83.3 ug/kg wet<83.3 ug/kg wet1,3-Dichlorobenzene
83.3 ug/kg wet<83.3 ug/kg wet1,4-Dichlorobenzene
83.3 ug/kg wet<83.3 ug/kg wet1-Chloronaphthalene
83.3 ug/kg wet<83.3 ug/kg wet1-Naphthylamine
83.3 ug/kg wet<83.3 ug/kg wet2,3,4,6-Tetrachlorophenol
83.3 ug/kg wet<83.3 ug/kg wet2,4,5-Trichlorophenol
83.3 ug/kg wet<83.3 ug/kg wet2,4,6-Trichlorophenol
83.3 ug/kg wet<83.3 ug/kg wet2,4-Dichlorophenol
83.3 ug/kg wet<83.3 ug/kg wet2,4-Dimethylphenol
83.3 ug/kg wet<83.3 ug/kg wet2,4-Dinitrophenol
83.3 ug/kg wet<83.3 ug/kg wet2,4-Dinitrotoluene
83.3 ug/kg wet<83.3 ug/kg wet2,6-Dichlorophenol
83.3 ug/kg wet<83.3 ug/kg wet2,6-Dinitrotoluene
83.3 ug/kg wet<83.3 ug/kg wet2-Chloronaphthalene
83.3 ug/kg wet<83.3 ug/kg wet2-Chlorophenol
83.3 ug/kg wet<83.3 ug/kg wet2-Methylnaphthalene
83.3 ug/kg wet<83.3 ug/kg wet2-Naphthylamine
83.3 ug/kg wet<83.3 ug/kg wet2-Nitroaniline
83.3 ug/kg wet<83.3 ug/kg wet2-Nitrophenol
83.3 ug/kg wet<83.3 ug/kg wet3,3'-Dichlorobenzidine
83.3 ug/kg wet<83.3 ug/kg wet3-Methylcholanthrene
83.3 ug/kg wet<83.3 ug/kg wet3-Nitroaniline
83.3 ug/kg wet<83.3 ug/kg wet4,6-Dinitro-2-methylphenol
83.3 ug/kg wet<83.3 ug/kg wet4-Aminobiphenyl
83.3 ug/kg wet<83.3 ug/kg wet4-Bromophenyl phenyl ether
83.3 ug/kg wet<83.3 ug/kg wet4-Chloroaniline
83.3 ug/kg wet<83.3 ug/kg wet4-Chlorophenyl phenyl ether
Page 49 of 63Page 49 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0637 - SW3550C
Blank (BYK0637-BLK1)Prepared & Analyzed: 11/23/2015
83.3 ug/kg wet<83.3 ug/kg wet4-Nitroaniline
83.3 ug/kg wet<83.3 ug/kg wet4-Nitrophenol
83.3 ug/kg wet<83.3 ug/kg wet7,12-Dimethylbenz (a) anthracene
83.3 ug/kg wet<83.3 ug/kg wetAcenaphthene
83.3 ug/kg wet<83.3 ug/kg wetAcenaphthylene
83.3 ug/kg wet<83.3 ug/kg wetAcetophenone
83.3 ug/kg wet<83.3 ug/kg wetAniline
83.3 ug/kg wet<83.3 ug/kg wetAnthracene
83.3 ug/kg wet<83.3 ug/kg wetBenzidine
83.3 ug/kg wet<83.3 ug/kg wetBenzo (a) anthracene
83.3 ug/kg wet<83.3 ug/kg wetBenzo (a) pyrene
83.3 ug/kg wet<83.3 ug/kg wetBenzo (b) fluoranthene
83.3 ug/kg wet<83.3 ug/kg wetBenzo (g,h,i) perylene
83.3 ug/kg wet<83.3 ug/kg wetBenzo (k) fluoranthene
83.3 ug/kg wet<83.3 ug/kg wetBenzoic acid
83.3 ug/kg wet<83.3 ug/kg wetBenzyl alcohol
83.3 ug/kg wet<83.3 ug/kg wetbis (2-Chloroethoxy) methane
83.3 ug/kg wet<83.3 ug/kg wetbis (2-Chloroethyl) ether
83.3 ug/kg wet<83.3 ug/kg wetbis (2-Chloroisopropyl) ether
83.3 ug/kg wet<83.3 ug/kg wetbis (2-Ethylhexyl) phthalate
83.3 ug/kg wet<83.3 ug/kg wetButyl benzyl phthalate
83.3 ug/kg wet<83.3 ug/kg wetChrysene
83.3 ug/kg wet<83.3 ug/kg wetDibenz (a,h) anthracene
83.3 ug/kg wet<83.3 ug/kg wetDibenz (a,j) acridine
83.3 ug/kg wet<83.3 ug/kg wetDibenzofuran
83.3 ug/kg wet<83.3 ug/kg wetDiethyl phthalate
83.3 ug/kg wet<83.3 ug/kg wetDimethyl phthalate
83.3 ug/kg wet<83.3 ug/kg wetDi-n-butyl phthalate
83.3 ug/kg wet<83.3 ug/kg wetDi-n-octyl phthalate
83.3 ug/kg wet<83.3 ug/kg wetDiphenylamine
83.3 ug/kg wet<83.3 ug/kg wetEthyl methanesulfonate
Page 50 of 63Page 50 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0637 - SW3550C
Blank (BYK0637-BLK1)Prepared & Analyzed: 11/23/2015
83.3 ug/kg wet<83.3 ug/kg wetFluoranthene
83.3 ug/kg wet<83.3 ug/kg wetFluorene
83.3 ug/kg wet<83.3 ug/kg wetHexachlorobenzene
83.3 ug/kg wet<83.3 ug/kg wetHexachlorobutadiene
83.3 ug/kg wet<83.3 ug/kg wetHexachlorocyclopentadiene
83.3 ug/kg wet<83.3 ug/kg wetHexachloroethane
83.3 ug/kg wet<83.3 ug/kg wetIndeno (1,2,3-cd) pyrene
83.3 ug/kg wet<83.3 ug/kg wetIsophorone
83.3 ug/kg wet<83.3 ug/kg wetm+p-Cresols
83.3 ug/kg wet<83.3 ug/kg wetMethyl methanesulfonate
83.3 ug/kg wet<83.3 ug/kg wetNaphthalene
83.3 ug/kg wet<83.3 ug/kg wetNitrobenzene
83.3 ug/kg wet<83.3 ug/kg wetn-Nitrosodimethylamine
83.3 ug/kg wet<83.3 ug/kg wetn-Nitrosodi-n-butylamine
83.3 ug/kg wet<83.3 ug/kg wetn-Nitrosodi-n-propylamine
83.3 ug/kg wet<83.3 ug/kg wetn-Nitrosodiphenylamine
83.3 ug/kg wet<83.3 ug/kg wetn-Nitrosopiperidine
83.3 ug/kg wet<83.3 ug/kg weto+m+p-Cresols
83.3 ug/kg wet<83.3 ug/kg weto-Cresol
83.3 ug/kg wet<83.3 ug/kg wetp-(Dimethylamino) azobenzene
83.3 ug/kg wet<83.3 ug/kg wetp-Chloro-m-cresol
83.3 ug/kg wet<83.3 ug/kg wetPentachloronitrobenzene (quintozene)
83.3 ug/kg wet<83.3 ug/kg wetPentachlorophenol
83.3 ug/kg wet<83.3 ug/kg wetPhenacetin
83.3 ug/kg wet<83.3 ug/kg wetPhenanthrene
83.3 ug/kg wet<83.3 ug/kg wetPhenol
83.3 ug/kg wet<83.3 ug/kg wetPronamide
83.3 ug/kg wet<83.3 ug/kg wetPyrene
83.3 ug/kg wet<83.3 ug/kg wetPyridine
3330 35-125Surr: 2,4,6-Tribromophenol 65.72190ug/kg wet
1670 45-105Surr: 2-Fluorobiphenyl 61.01020ug/kg wet
Page 51 of 63Page 51 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0637 - SW3550C
Blank (BYK0637-BLK1)Prepared & Analyzed: 11/23/2015
3330 35-105Surr: 2-Fluorophenol 64.22140ug/kg wet
1670 35-100Surr: Nitrobenzene-d5 67.41120ug/kg wet
3330 40-100Surr: Phenol-d5 61.92060ug/kg wet
1670 30-125Surr: p-Terphenyl-d14 86.91450ug/kg wet
LCS (BYK0637-BS1)Prepared & Analyzed: 11/23/2015
83.3 3310 44-14230.6ug/kg wet1010 ug/kg wet1,2,4-Trichlorobenzene L
83.3 3330 20-12434.0ug/kg wet1130 ug/kg wet1,4-Dichlorobenzene
83.3 6670 15-14034.3ug/kg wet2290 ug/kg wet4-Nitrophenol
83.3 3320 45-11031.0ug/kg wet1030 ug/kg wetAcenaphthene L
83.3 3320 40-11535.6ug/kg wet1180 ug/kg wetn-Nitrosodi-n-propylamine L
83.3 6600 25-12041.3ug/kg wet2720 ug/kg wetPentachlorophenol
83.3 6670 40-10032.6ug/kg wet2170 ug/kg wetPhenol L
83.3 3330 45-12529.9ug/kg wet996 ug/kg wetPyrene L
3330 35-125Surr: 2,4,6-Tribromophenol 78.42610ug/kg wet
1670 45-105Surr: 2-Fluorobiphenyl 64.61080ug/kg wet
3330 35-105Surr: 2-Fluorophenol 70.52350ug/kg wet
1670 35-100Surr: Nitrobenzene-d5 70.81180ug/kg wet
3330 40-100Surr: Phenol-d5 67.52250ug/kg wet
1670 30-125Surr: p-Terphenyl-d14 88.81480ug/kg wet
Matrix Spike (BYK0637-MS1)Prepared & Analyzed: 11/23/2015Source: 15K0390-11
116 4620 44-14215.2ug/kg dry702 ug/kg dry <116 ug/kg dry1,2,4-Trichlorobenzene M
116 4650 20-12414.7ug/kg dry684 ug/kg dry <116 ug/kg dry1,4-Dichlorobenzene M
116 9300 15-14022.7ug/kg dry2110 ug/kg dry <116 ug/kg dry4-Nitrophenol
116 4630 45-11017.1ug/kg dry792 ug/kg dry <116 ug/kg dryAcenaphthene M
116 4630 40-11519.3ug/kg dry894 ug/kg dry <116 ug/kg dryn-Nitrosodi-n-propylamine M
116 9210 25-12026.4ug/kg dry2440 ug/kg dry <116 ug/kg dryPentachlorophenol
116 9300 40-10015.8ug/kg dry1470 ug/kg dry <116 ug/kg dryPhenol M
116 4650 45-12524.5ug/kg dry1140 ug/kg dry <116 ug/kg dryPyrene M
4650 35-125Surr: 2,4,6-Tribromophenol 47.12190ug/kg dry
Page 52 of 63Page 52 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0637 - SW3550C
Matrix Spike (BYK0637-MS1)Prepared & Analyzed: 11/23/2015Source: 15K0390-11
2330 45-105Surr: 2-Fluorobiphenyl 33.8786ug/kg dry S
4650 35-105Surr: 2-Fluorophenol 30.01400ug/kg dry S
2330 35-100Surr: Nitrobenzene-d5 34.8810ug/kg dry S
4650 40-100Surr: Phenol-d5 32.21500ug/kg dry S
2330 30-125Surr: p-Terphenyl-d14 72.81690ug/kg dry
Matrix Spike Dup (BYK0637-MSD1)Prepared & Analyzed: 11/23/2015Source: 15K0390-11
118 4690 2044-14225.6 52.3ug/kg dry1200 ug/kg dry <118 ug/kg dry1,2,4-Trichlorobenzene M, P
118 4710 2020-12428.1 63.6ug/kg dry1320 ug/kg dry <118 ug/kg dry1,4-Dichlorobenzene P
118 9430 2015-14032.4 36.4ug/kg dry3050 ug/kg dry <118 ug/kg dry4-Nitrophenol P
118 4690 2045-11026.1 43.1ug/kg dry1230 ug/kg dry <118 ug/kg dryAcenaphthene M, P
118 4700 2040-11529.6 43.4ug/kg dry1390 ug/kg dry <118 ug/kg dryn-Nitrosodi-n-propylamine M, P
118 9330 2025-12037.6 36.1ug/kg dry3510 ug/kg dry <118 ug/kg dryPentachlorophenol P
118 9430 2040-10026.9 53.2ug/kg dry2540 ug/kg dry <118 ug/kg dryPhenol M, P
118 4710 2045-12529.7 20.6ug/kg dry1400 ug/kg dry <118 ug/kg dryPyrene M, P
4710 35-125Surr: 2,4,6-Tribromophenol 66.63140ug/kg dry
2360 45-105Surr: 2-Fluorobiphenyl 54.11280ug/kg dry
4710 35-105Surr: 2-Fluorophenol 57.82730ug/kg dry
2360 35-100Surr: Nitrobenzene-d5 57.61360ug/kg dry
4710 40-100Surr: Phenol-d5 54.52570ug/kg dry
2360 30-125Surr: p-Terphenyl-d14 86.72040ug/kg dry
Page 53 of 63Page 53 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Hydrocarbons by GC - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0594 - SW8100
Blank (BYK0594-BLK1)Prepared: 11/20/2015 Analyzed: 11/23/2015
10.0 mg/kg wet<10.0 mg/kg wetTPH-Semi-Volatiles (DRO)
4.91 40-160Surr: Pentacosane 58.52.88 mg/kg wet
LCS (BYK0594-BS1)Prepared: 11/20/2015 Analyzed: 11/23/2015
10.0 99.2 40-16060.1mg/kg wet59.7 mg/kg wetTPH-Semi-Volatiles (DRO)
4.96 40-160Surr: Pentacosane 61.23.04 mg/kg wet
Matrix Spike (BYK0594-MS1)Prepared: 11/20/2015 Analyzed: 11/23/2015Source: 15K0390-01
12.9 129 40-16065.2mg/kg dry84.0 mg/kg dry <12.9 mg/kg dryTPH-Semi-Volatiles (DRO)
6.44 40-160Surr: Pentacosane 66.04.25 mg/kg dry
Matrix Spike Dup (BYK0594-MSD1)Prepared: 11/20/2015 Analyzed: 11/23/2015Source: 15K0390-01
12.8 128 2040-16060.3 8.53mg/kg dry77.1 mg/kg dry <12.8 mg/kg dryTPH-Semi-Volatiles (DRO)
6.39 40-160Surr: Pentacosane 60.73.88 mg/kg dry
Batch BYK0646 - SW8100
Blank (BYK0646-BLK1)Prepared & Analyzed: 11/23/2015
0.50 mg/L<0.50 mg/LTPH-Semi-Volatiles (DRO)
0.250 40-160Surr: Pentacosane 77.90.195 mg/L
LCS (BYK0646-BS1)Prepared & Analyzed: 11/23/2015
0.50 5.00 40-16072.3mg/L3.6 mg/LTPH-Semi-Volatiles (DRO)
0.250 40-160Surr: Pentacosane 84.70.212 mg/L
Matrix Spike (BYK0646-MS1)Prepared: 11/23/2015 Analyzed: 11/24/2015Source: 15K0401-02
0.50 5.10 40-16064.3mg/L3.3 mg/L <0.50 mg/LTPH-Semi-Volatiles (DRO)
0.255 40-160Surr: Pentacosane 85.10.217 mg/L
Page 54 of 63Page 54 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Hydrocarbons by GC - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0646 - SW8100
Matrix Spike Dup (BYK0646-MSD1)Prepared: 11/23/2015 Analyzed: 11/24/2015Source: 15K0401-02
0.50 5.10 2040-16071.8 10.9mg/L3.7 mg/L <0.50 mg/LTPH-Semi-Volatiles (DRO)
0.255 40-160Surr: Pentacosane 86.00.219 mg/L
Page 55 of 63Page 55 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Organochlorine Pesticides and PCBs by GC/ECD - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0671 - SW3550B
Blank (BYK0671-BLK1)Prepared: 11/23/2015 Analyzed: 11/24/2015
0.100 mg/kg wet<0.100 mg/kg wetPCB as Aroclor 1016
0.100 mg/kg wet<0.100 mg/kg wetPCB as Aroclor 1221
0.100 mg/kg wet<0.100 mg/kg wetPCB as Aroclor 1232
0.100 mg/kg wet<0.100 mg/kg wetPCB as Aroclor 1242
0.100 mg/kg wet<0.100 mg/kg wetPCB as Aroclor 1248
0.100 mg/kg wet<0.100 mg/kg wetPCB as Aroclor 1254
0.100 mg/kg wet<0.100 mg/kg wetPCB as Aroclor 1260
0.0315 30-105Surr: DCB 95.00.0300 mg/kg wet
0.0315 30-105Surr: TCMX 85.00.0268 mg/kg wet
LCS (BYK0671-BS2)Prepared: 11/23/2015 Analyzed: 11/24/2015
0.100 0.148 60-140126mg/kg wet0.186 mg/kg wetPCB as Aroclor 1016
0.100 0.148 60-14096.0mg/kg wet0.142 mg/kg wetPCB as Aroclor 1260
0.0296 30-105Surr: DCB 90.00.0266 mg/kg wet
0.0296 30-105Surr: TCMX 90.00.0266 mg/kg wet
Matrix Spike (BYK0671-MS2)Prepared: 11/23/2015 Analyzed: 11/24/2015Source: 15K0390-11
0.141 0.236 60-140102mg/kg dry0.240 mg/kg dry <0.141 mg/kg dryPCB as Aroclor 1016
0.141 0.236 60-14072.0mg/kg dry0.170 mg/kg dry <0.141 mg/kg dryPCB as Aroclor 1260
0.0471 30-105Surr: DCB 65.00.0306 mg/kg dry
0.0471 30-105Surr: TCMX 1000.0471 mg/kg dry
Matrix Spike Dup (BYK0671-MSD2)Prepared: 11/23/2015 Analyzed: 11/24/2015Source: 15K0390-11
0.141 0.236 2060-140102 0.00mg/kg dry0.240 mg/kg dry <0.141 mg/kg dryPCB as Aroclor 1016
0.141 0.236 2060-14071.0 1.40mg/kg dry0.167 mg/kg dry <0.141 mg/kg dryPCB as Aroclor 1260
0.0471 30-105Surr: DCB 65.00.0306 mg/kg dry
0.0471 30-105Surr: TCMX 90.00.0424 mg/kg dry
Page 56 of 63Page 56 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Wet Chemistry Analysis - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BYK0572 - No Prep Halides
Blank (BYK0572-BLK1)Prepared & Analyzed: 11/19/2015
0.10 %100 %Percent Solids
Duplicate (BYK0572-DUP1)Prepared & Analyzed: 11/19/2015Source: 15K0390-01
0.10 200.106%77.4 %77.3 %Percent Solids
Duplicate (BYK0572-DUP2)Prepared & Analyzed: 11/19/2015Source: 15K0390-05
0.10 201.11%79.9 %80.8 %Percent Solids
Page 57 of 63Page 57 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
SW6010C in Non-Potable Water
Arsenic VELAP,NC,WVDEP
Barium VELAP,NC,WVDEP
Cadmium VELAP,NC,WVDEP
Chromium VELAP,NC,WVDEP
Lead VELAP,NC,WVDEP
Selenium VELAP,NC,WVDEP
Silver VELAP,NC
SW6010C in Solids
Arsenic VELAP,NC
Barium VELAP,NC,WVDEP
Cadmium VELAP,NC,WVDEP
Chromium VELAP,NC
Lead VELAP,NC,WVDEP
Selenium VELAP,NC,WVDEP
Silver VELAP,NC,WVDEP
SW7470A in Non-Potable Water
Mercury VELAP,NC,WVDEP
SW7471B in Solids
Mercury VELAP,WVDEP
SW8015C in Non-Potable Water
TPH-Semi-Volatiles (DRO)VELAP,NC,WVDEP
TPH-Volatiles (GRO)VELAP,NC,WVDEP
SW8015C in Solids
TPH-Semi-Volatiles (DRO)VELAP,NC,WVDEP
TPH-Volatiles (GRO)VELAP,NC,WVDEP
SW8082A in Solids
PCB as Aroclor 1016 VELAP,NC
PCB as Aroclor 1221 VELAP,NC
PCB as Aroclor 1232 VELAP,NC
PCB as Aroclor 1242 VELAP,NC
PCB as Aroclor 1248 VELAP,NC
PCB as Aroclor 1254 VELAP,NC
PCB as Aroclor 1260 VELAP,NC
SW8260B in Non-Potable Water
Benzene VELAP
Page 58 of 63Page 58 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
Ethylbenzene VELAP
m+p-Xylenes VELAP
Methyl-t-butyl ether (MTBE)VELAP
Naphthalene VELAP
o-Xylene VELAP
Toluene VELAP
Xylenes, Total VELAP
SW8260B in Solids
Benzene VELAP,NC
Ethylbenzene VELAP,NC
m+p-Xylenes VELAP,NC
Methyl-t-butyl ether (MTBE)VELAP,NC
Naphthalene VELAP,NC
o-Xylene VELAP,NC
Toluene VELAP,NC
Xylenes, Total VELAP,NC
Dibromofluoromethane VELAP
SW8270D in Solids
1,2,4,5-Tetrachlorobenzene NC,VELAP,WVDEP
1,2,4-Trichlorobenzene NC,VELAP,WVDEP
1,2-Dichlorobenzene NC,VELAP,WVDEP
1,2-Diphenylhydrazine NC,VELAP,WVDEP
1,3-Dichlorobenzene NC,VELAP,WVDEP
1,4-Dichlorobenzene NC,VELAP,WVDEP
1-Chloronaphthalene NC,VELAP,WVDEP
1-Naphthylamine NC,VELAP,WVDEP
2,3,4,6-Tetrachlorophenol NC,VELAP,WVDEP
2,4,5-Trichlorophenol NC,VELAP,WVDEP
2,4,6-Trichlorophenol NC,VELAP,WVDEP
2,4-Dichlorophenol NC,VELAP,WVDEP
2,4-Dimethylphenol NC,VELAP,WVDEP
2,4-Dinitrophenol NC,VELAP,WVDEP
2,4-Dinitrotoluene NC,VELAP,WVDEP
2,6-Dichlorophenol NC,VELAP,WVDEP
2,6-Dinitrotoluene NC,VELAP,WVDEP
2-Chloronaphthalene NC,VELAP,WVDEP
2-Chlorophenol NC,VELAP,WVDEP
Page 59 of 63Page 59 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
2-Methylnaphthalene NC,VELAP,WVDEP
2-Naphthylamine NC,VELAP,WVDEP
2-Nitroaniline NC,VELAP,WVDEP
2-Nitrophenol NC,VELAP,WVDEP
3,3'-Dichlorobenzidine NC,VELAP,WVDEP
3-Methylcholanthrene NC,VELAP,WVDEP
3-Nitroaniline NC,VELAP,WVDEP
4,6-Dinitro-2-methylphenol NC,VELAP,WVDEP
4-Aminobiphenyl NC,VELAP,WVDEP
4-Bromophenyl phenyl ether NC,VELAP,WVDEP
4-Chloroaniline NC,VELAP,WVDEP
4-Chlorophenyl phenyl ether NC,VELAP,WVDEP
4-Nitroaniline NC,VELAP,WVDEP
4-Nitrophenol NC,VELAP,WVDEP
7,12-Dimethylbenz (a) anthracene NC,VELAP,WVDEP
Acenaphthene NC,VELAP,WVDEP
Acenaphthylene NC,VELAP,WVDEP
Acetophenone NC,VELAP,WVDEP
Aniline NC,VELAP,WVDEP
Anthracene NC,VELAP,WVDEP
Benzidine NC,VELAP,WVDEP
Benzo (a) anthracene NC,VELAP,WVDEP
Benzo (a) pyrene NC,VELAP,WVDEP
Benzo (b) fluoranthene NC,VELAP,WVDEP
Benzo (g,h,i) perylene NC,VELAP,WVDEP
Benzo (k) fluoranthene NC,VELAP,WVDEP
Benzoic acid NC,VELAP,WVDEP
Benzyl alcohol NC,VELAP,WVDEP
bis (2-Chloroethoxy) methane NC,VELAP,WVDEP
bis (2-Chloroethyl) ether NC,VELAP,WVDEP
bis (2-Chloroisopropyl) ether NC,VELAP,WVDEP
bis (2-Ethylhexyl) phthalate NC,VELAP,WVDEP
Butyl benzyl phthalate NC,VELAP,WVDEP
Chrysene NC,VELAP,WVDEP
Dibenz (a,h) anthracene NC,VELAP,WVDEP
Dibenz (a,j) acridine NC,VELAP,WVDEP
Dibenzofuran NC,VELAP,WVDEP
Diethyl phthalate NC,VELAP,WVDEP
Page 60 of 63Page 60 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
Dimethyl phthalate NC,VELAP,WVDEP
Di-n-butyl phthalate NC,VELAP,WVDEP
Di-n-octyl phthalate NC,VELAP,WVDEP
Diphenylamine NC,VELAP,WVDEP
Ethyl methanesulfonate NC,VELAP,WVDEP
Fluoranthene NC,VELAP,WVDEP
Fluorene NC,VELAP,WVDEP
Hexachlorobenzene NC,VELAP,WVDEP
Hexachlorobutadiene NC,VELAP,WVDEP
Hexachlorocyclopentadiene NC,VELAP,WVDEP
Hexachloroethane NC,VELAP,WVDEP
Indeno (1,2,3-cd) pyrene NC,VELAP,WVDEP
Isophorone NC,VELAP,WVDEP
m+p-Cresols NC,VELAP,WVDEP
Methyl methanesulfonate NC,VELAP,WVDEP
Naphthalene NC,VELAP,WVDEP
Nitrobenzene NC,VELAP,WVDEP
n-Nitrosodimethylamine NC,VELAP,WVDEP
n-Nitrosodi-n-butylamine NC,VELAP,WVDEP
n-Nitrosodi-n-propylamine NC,VELAP,WVDEP
n-Nitrosodiphenylamine NC,VELAP,WVDEP
n-Nitrosopiperidine NC,VELAP,WVDEP
o+m+p-Cresols NC,VELAP,WVDEP
o-Cresol NC,VELAP,WVDEP
p-(Dimethylamino) azobenzene NC,VELAP,WVDEP
p-Chloro-m-cresol NC,VELAP,WVDEP
Pentachloronitrobenzene (quintozene)NC,WVDEP
Pentachlorophenol NC,VELAP,WVDEP
Phenacetin NC,VELAP,WVDEP
Phenanthrene NC,VELAP,WVDEP
Phenol NC,VELAP,WVDEP
Pronamide NC,VELAP,WVDEP
Pyrene NC,VELAP,WVDEP
Pyridine NC,VELAP,WVDEP
Page 61 of 63Page 61 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Code Description Lab Number Expires
341 12/31/2015Maryland DE Drinking WaterMdDOE
495 12/31/2015North Carolina DENRNC
460021 06/15/2016NELAC-Virginia Certificate #8074VELAP
350 11/30/2015West Virginia DEPWVDEP
Page 62 of 63Page 62 of 67
Client Site I.D.:
Project Number:Submitted To:
Date Issued:
Groundwater Environmental Services, Inc.-R
3701 Saunders Ave.
[none]Daniel Breckenridge
Richmond VA, 23227
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
November 17, 2015 16:15Date Received:
November 24, 2015 17:24
Sheetz - Burlington Phase II Follow-up
Final Report
Summary of Data Qualifiers
C Continuing calibarion verification response for this analyte is outside specifications.
Cl Residual Chlorine or other oxidizing agent was detected in the container used to analyze this sample.
DS Surrogate concentration reflects a dilution factor.
L LCS recovery is outside of established acceptance limits
M Matrix spike recovery is outside established acceptance limits
P Duplicate analysis does not meet the acceptance criteria for precision
S Surrogate recovery was outside acceptance criteria
Relative Percent DifferenceRPD
QualifersQual
Denotes sample was re-analyzed-RE
Dilution Factor. Please also see the Preparation Factor in the Analysis Summary section.D.F.
TIC Tentatively Identified Compounds are compounds that are identified by comparing the analyte mass spectral pattern with the NIST spectral library. A TIC
spectral match is reported when the pattern is at least 75% consistent with the published pattern. Compound concentrations are estimated and are calculated
using an internal standard response factor of 1.
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