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HomeMy WebLinkAbout20001_North_Graham_Phase II_20151013 3701 Saunders Ave • Richmond, Virginia 23227 • (866) 222-7786 • FAX (866) 902-2187 October 13, 2015 Mr. Matt Cutshall Environmental Compliance Manager Sheetz, Inc. 5700 Sixth Avenue Altoona, PA 16602 RE: Limited Phase 2 Environmental Site Assessment Report Proposed Sheetz Location North Graham Hopedale Road and North Church Street, Burlington, NC Dear Mr. Cutshall: Groundwater & Environmental Services, Inc. (GES) is pleased to provide the following Limited Phase 2 Environmental Site Assessment (ESA) Report to Sheetz, Inc. (Sheetz). This investigation was conducted in order to provide an additional assessment of potential impacts to soil and groundwater at the above referenced property identified by Sheetz for potential development of a Sheetz retail petroleum facility. 1.0 ENVIRONMENTAL SITE ASSESSMENT The location of the Subject Property and surrounding area is illustrated on the Site Location Map presented on the U.S. Geological Survey (USGS) 7.5-Minute Topographic Map for Burlington, North Carolina (1981) as Figure 1. The Subject Property is located in a mixed industrial, commercial, and residential area of Burlington, North Carolina. There are commercial properties located to the south and west, government properties to the north, residential properties to the east and a large former industrial facility to the northwest, as shown in the Local Area Map, Figure 2. The Subject Property consists primarily of impermeable pavement which is bisected by an old section of railroad track running northwest to southeast. The Subject Property is illustrated on the Site Map presented as Figure 3. On September 25, 2015, GES supervised the advancement of six soil borings (SB-1 through SB-6) on the Subject Property. The soil borings were advanced to investigate the extent of existing contamination from previous uses of the Subject Property or the migration of contaminants from surrounding properties. SB-1 was advanced in the northwest corner of the Subject Property to investigate the possible migration of contaminant plumes known to be located below the former industrial facility to the northwest. SB-2 was located adjacent to the existing underground storage tank (UST) field from the active retail petroleum facility directly across North Graham Hopedale Road. SB-3 was located in the southwest corner to investigate dissolved phase hydrocarbon contamination detected during previous investigations. The remaining three soil borings (SB-4 through SB-6) were located throughout the Subject Property to ensure no other contamination exists. The six soil borings were advanced via direct-push technology and advanced to a depth of 25 feet below ground surface (bgs). The soil boring locations are shown on Figure 4. The soil boring logs are provided in Attachment A and photo documentation of the investigation activities are provided in Attachment B. Following soil boring completion, a temporary well was placed into each borehole in an attempt to collect a water sample. Each temporary well was Mr. Matt Cutshall Limited Phase 2 Environmental Assessment Report Proposed Sheetz Location October 13, 2015 comprised of a PVC one-inch diameter well screen and allowed to collect water for a minimum of one hour. Water samples were collected from all six temporary wells, and named MW-1 through MW-6. 1.1 Soil Sampling and Results One soil sample was collected from each of the borings at the interval corresponding to the highest value detected with a photo-ionization detector (PID). If no PID response was observed, the soil sample was collected directly above the observed water table. Following the collection of each sample, the sample was split into two parts. One part of the sample was placed into a zip-lock bag for field screening. The zip-lock bags of soil were screened with a PID to measure the concentration of volatile organic compounds (VOCs) within the headspace. The PID values from the soil samples collected from the soil borings are presented on the boring logs, Attachment A. The second part of the sample was placed into the laboratory supplied soil sampling bottleware, immediately labeled, and placed on ice in a cooler in preparation for laboratory analysis. The soil samples were submitted to Air Water & Soil Laboratories (AWS) located at 1941 Reymet Road, Richmond, VA for analysis of the site specific constitutes of concern (COCs) including: benzene, toluene, ethylbenzene, and xylenes (BTEX), methyl tertiary butyl ether (MTBE), and naphthalene via USEPA Method SW8021B, total petroleum hydrocarbons - gasoline range organics (TPH-GRO) and total petroleum range hydrocarbons - diesel range organics (TPH-DRO) via USEPA Method 8015B and RCRA 8 metals via Method SW6010C and Method SW7471B. The analytical results from the soil samples were screened against the North Carolina Department of Natural Resources (NCDENR) soil to groundwater Maximum Soil Contaminant Concentrations (MSCC) and are presented in Table 1. The complete laboratory analytical report is included in Attachment B. A summary of the results of the soil sample analysis is listed below. Exceedances of MSCC: • SB-3: Naphthalene at 0.295 milligrams per kilogram (mg/kg) (MSCC - 0.16 mg/kg). Detections above the reporting limit and below the MSCC: • SB-1: Barium at 54.8 mg/kg (MSCC – 290 mg/kg), Cadmium at 0.460 mg/kg (MSCC – not available), and Chromium at 3.5 mg/kg (MSCC – 5.4 mg/kg); • SB-2: Barium at 59.0 mg/kg (MSCC – 290 mg/kg), Cadmium at 0.526 mg/kg (MSCC – not available), and Chromium at 0.776 mg/kg (MSCC - 5.4 mg/kg); • SB-3: Toluene at 0.030 mg/kg (MSCC – 4 mg/kg), Ethylbenzene at 0.142 mg/kg (MSCC – 5 mg/kg), Total Xylenes at 0.506 mg/kg (MSCC – 5 mg/kg). TPH-GRO concentrations at 11.1 mg/kg (MSCC - not available) and TPH-DRO at 16.8 mg/kg (MSCC – not available); and • SB-4: Mercury at 0.011 mg/kg (MSCC – not available). 1.2 Groundwater Sampling and Analysis On September 25, 2015, following the installation of the temporary wells within the soil borings, groundwater samples were collected from all six temporary wells (MW-1 through MW-6). Groundwater depths ranged from 13.43 feet bgs in MW-6 to 21.33 feet bgs in MW-5 during the investigation. Groundwater samples were collected from each temporary well using a peristaltic pump and each well Mr. Matt Cutshall Limited Phase 2 Environmental Assessment Report Proposed Sheetz Location October 13, 2015 had dedicated polyethylene tubing. Each sample was placed in the proper bottleware and immediately placed in a cooler containing packaged ice. The groundwater samples and associated chain-of-custody form were submitted to AWS for analysis of the site specific COCs including; BTEX, MTBE, and naphthalene via USEPA Method SW8021B, TPH- GRO and TPH-DRO via USEPA Method 8015B and RCRA 8 metals via Method SW6010C and Method SW7471B. The groundwater analytical results were screened against the NCDENR 2L Groundwater (GW) Standards and are presented in Table 2. The complete analytical laboratory report is included in Attachment B. A summary of the groundwater analytical results is listed below. Exceedances of 2L GW Standard: • MW-2: Chromium at 19.5 micrograms per Liter (ug/L) (2L GW Standard – 10 ug/L) • MW-3: Benzene at 212 ug/L (2L GW Standard – 1 ug/L), and Naphthalene at 29.6 ug/L (2L GW Standard – 6 ug/L), • MW-5: Chromium at 349 ug/L (2L GW Standard – 10 ug/L); and • MW-6: Barium at 2,640 ug/L (2L GW Standard – 700 mg/L), Cadmium at 7.7 ug/L (2L GW Standard – 2 ug/L), Chromium at 182 ug/L (2L GW Standard – 10 ug/L), and Lead at 74.5 ug/L (2L GW Standard – 15 ug/L). Detections above the reporting limit and below the 2L GW Standard: • MW-1: Barium at 226 ug/L (2L GW Standard – 700 ug/L), • MW-2: Barium at 212 ug/L (2L GW Standard – 700 ug/L), • MW-3: Toluene at 7.21 ug/L (2L GW Standard – 600 ug/L), Ethylbenzene at 6.64 ug/L (2L GW Standard – 600 ug/L), Total Xylenes at 12.4 ug/L (2L GW Standard – 500 ug/L), and Barium at 350 ug/L (2L GW Standard – 700 ug/L), and TPH-GRO at 0.66 milligrams per Liter (mg/L) (2L GW Standard – not available), • MW-4: Barium at 172 ug/L (2L GW Standard – 700 ug/L); and • MW-5: Barium at 506 ug/L (2L GW Standard – 700 ug/L). 2.0 SITE ASSESSMENT SUMMARY The following is a summary of the analytical results collected during the Limited Phase 2 ESA: • The analytical results indicate that target compounds in all soil samples were either not detected or detected below the MSCC, with the exception of naphthalene detected above the MSCC in SB-3. • The analytical results indicate that target compounds in all groundwater samples were either not detected or detected below the NCDENR 2L Groundwater Standards, with the exception of chromium in MW-2, benzene and naphthalene in MW-3, chromium in MW-5, and barium, cadmium, chromium, and lead in MW-6. • Groundwater at the Subject Property ranged from 13.43 feet bgs in MW-6 to 21.33 feet bgs in MW-5 during the investigation. Mr. Matt Cutshall Limited Phase 2 Environmental Assessment Report Proposed Sheetz Location October 13, 2015 Please do not hesitate to contact our office at (866) 222-7786 with any questions and/or comments. Respectfully submitted, GROUNDWATER & ENVIRONMENTAL SERVICES, INC. Prepared by: Nick Braun Staff Environmental Scientist Reviewed by: Daniel Breckenridge Project Manager Figures: Figure 1 – Site Location Map Figure 2 – Local Area Map Figure 3 – Site Map Figure 4 – Soil Boring Location Map Tables: Table 1 – Soil Quality Data Summary Table 2 – Groundwater Quality Data Summary Attachments: Attachment A – Boring Logs Attachment B – Photo Essay Attachment C – Laboratory Analytical Report FIGURES M:\ G r a p h i c s \ 1 2 0 0 - R i c h m o n d \ S h e e t z \ B u r l i n g t o n ( g r a h a m h o p e d a l e r d & c h u r c h ) \ b u r l i n g t o n ( g r a h a m h o p e d a l e r d & c h u r c h ) S L M . d w g , 1 0 / 1 / 2 0 1 5 1 1 : 5 9 : 0 0 A M , D W G T o P D F . p c 3 N.B. D.B. PROPOSED SHEETZ LOCATION RESIDENTIAL ALAMANCE COUNTY GOVERNMENT BUILDINGS FORMER TAMP FACILITY WESTERN STEAK HOUSE CO M M E R C I A L EXXON STATION CO M M E R C I A L THRIFTY TIRE RITE AID NC ARMORY M:\ G r a p h i c s \ 1 2 0 0 - R i c h m o n d \ S h e e t z \ B u r l i n g t o n ( g r a h a m h o p e d a l e r d & c h u r c h ) \ b u r l i n g t o n ( g r a h a m h o p e d a l e r d & c h u r c h ) L A M . d w g , 1 0 / 1 3 / 2 0 1 5 1 0 : 0 5 : 2 9 A M , D W G T o P D F . p c 3 N.B. D.B. M:\ G r a p h i c s \ 1 2 0 0 - R i c h m o n d \ S h e e t z \ B u r l i n g t o n ( g r a h a m h o p e d a l e r d & c h u r c h ) \ b u r l i n g t o n ( g r a h a m h o p e d a l e r d & c h u r c h ) S M . d w g , 1 0 / 1 / 2 0 1 5 3 : 4 9 : 3 2 P M , D W G T o P D F . p c 3 N.B. D.B. M:\ G r a p h i c s \ 1 2 0 0 - R i c h m o n d \ S h e e t z \ B u r l i n g t o n ( g r a h a m h o p e d a l e r d & c h u r c h ) \ b u r l i n g t o n ( g r a h a m h o p e d a l e r d & c h u r c h ) S M . d w g , 1 0 / 1 2 / 2 0 1 5 1 0 : 0 1 : 0 1 A M , D W G T o P D F . p c 3 N.B. D.B. TABLES Ta b l e 1 SO I L Q U A L I T Y D A T A S U M M A R Y Pr o p o s e d S h e e t z L o c a t i o n N G r a h a m H o p e d a l e R o a d a n d N C h u r c h S t r e e t Bu r l i n g t o n , N o r t h C a r o l i n a Sa m p l e I D S B - 1 S B - 2 S B - 3 S B - 4 S B - 5 S B - 6 Sa m p le D e p th ( f t b g s) S o i l - t o - G W M S C C 1 6 - 1 8 1 6 - 1 8 1 3 - 1 5 1 3 - 1 5 1 6 - 1 8 1 8 - 2 0 Da t e S a m p le d 9 / 2 5 / 2 0 1 5 9 / 2 5 / 2 0 1 5 9 / 2 5 / 2 0 1 5 9 / 2 5 / 2 0 1 5 9 / 2 5 / 2 0 1 5 9 / 2 5 / 2 0 1 5 Me t h y l - t - b u t y l e t h e r ( M T B E ) m g / k g 0. 0 9 1 ND N D N D N D N D N D Be n z e n e m g / k g 0. 0 0 5 6 ND N D N D N D N D N D To l u e n e m g / k g 4 ND N D 0. 0 3 0 ND N D N D Et h y l b e n z e n e m g / k g 5 ND N D 0. 1 4 2 ND N D N D To t a l X y l e n e s m g / k g 5 ND N D 0. 5 0 6 ND N D N D N ap h t h a l e n e m g / k g 0. 1 6 N D N D 0. 2 9 5 N D N D N D GR O m g / k g ~ N D N D 11 . 1 N D N D N D DR O m g / k g ~ ND N D 16 . 8 N D N D N D Si l v e r m g / k g 0. 2 5 ND N D N D N D N D N D Ar s e n i c m g / k g ~ ND N D N D N D N D N D Ba r i u m m g / k g 29 0 5 4 . 8 5 9 . 0 ND N D N D N D Ca d m i u m m g / k g ~ 0. 4 6 0 0 . 5 2 6 ND N D N D N D Ch r o m i u m m g / k g 5. 4 3 . 5 0 . 7 7 6 ND N D N D N D Me r c u r y m g / k g ~ ND N D N D 0. 0 1 1 ND N D Le a d m g / k g 27 0 ND 2. 2 3 ND N D N D N D Se l e n i u m mg / k g ~ N D N D N D N D N D N D No t e s : MS C C - M a x i m u m S o i l C o n t a m i n a n t C o n c e n t r a t i o n ( f r o m N o r t h C a r o l i n a D e p a r t m e n t o f E n v i r o n m e n t a n d N a t u r a l R e s o u r c e s ) ~ - N o M S C C a v a i l a b l e mg / k g - m i l l i g r a m s p e r k i l o g r a m s ND - N o n D e t e c t ft b g s - f e e t b e l o w g r o u n d s u r f a c e TP H - G R O T o t a l P e t r o l e u m H y d r o c a r b o n s G a s o l i n e R a n g e O r g a n i c s TP H - D R O T o t a l P e t r o l e u m H y d r o c a r b o n s D i e s e l R a n g e O r g a n i c s RC R A 8 M e t a l s TP H - G R O TP H - D R O Un i t s Vo l a t i l e O r g an i c C o m p ou n d s ( V O C s ) GE S - O c t o b e r 2 0 1 5 1 o f 1 N G r a h a m H o p e d a l e R o a d , B u r l i n g t o n , N C Ta b l e 2 GR O U N D W A T E R Q U A L I T Y D A T A S U M M A R Y Pr o p o s e d S h e e t z L o c a t i o n N G r a h a m H o p e d a l e R o a d a n d N C h u r c h S t r e e t Bu r l i n g t o n , N o r t h C a r o l i n a Sa m p l e I D M W - 1 M W - 2 M W - 3 M W - 4 M W - 5 M W - 6 Da t e S a m p l e d 9 / 2 5 / 2 0 1 5 9 / 2 5 / 2 0 1 5 9 / 2 5 / 2 0 1 5 9 / 2 5 / 2 0 1 5 9 / 2 5 / 2 0 1 5 9 / 2 5 / 2 0 1 5 De p t h t o W a t e r ( f t b g s ) 1 6 . 0 7 1 9 . 0 6 1 7 . 5 0 1 7 . 7 1 2 1 . 3 3 1 3 . 4 3 Me t h y l - t - b u t y l e t h e r ( M T B E ) u g / L 2 0 ND N D N D N D N D N D Be n z e n e u g / L 1 ND N D 21 2 ND N D N D To l u e n e u g / L 6 0 0 ND N D 7. 2 1 ND N D N D Et h y l b e n z e n e u g / L 6 0 0 ND N D 6. 6 4 ND N D N D To t a l X y l e n e s u g / L 5 0 0 ND N D 12 . 4 ND N D N D Na p h t h a l e n e u g / L 6 ND N D 29 . 6 ND N D N D GR O m g / L ~ ND N D 0. 6 6 ND N D N D DR O m g / L ~ ND ND N D N D N D N D Si l v e r u g / L 2 0 ND N D N D N D N D N D Ar s e n i c u g / L 1 0 ND N D N D N D N D N D Ba r i u m u g / L 7 0 0 22 6 2 1 2 3 5 0 1 7 2 5 0 6 2 , 6 4 0 Ca d m i u m u g / L 2 ND ND ND N D N D 7.7 Ch r o m i u m u g / L 1 0 ND 19 . 5 ND N D 349 1 8 2 Me r c u r y u g / L 1 ND N D N D N D N D N D Le a d u g / L 1 5 ND ND ND N D N D 74.5 Se l e n i u m ug / L 2 0 ND N D 1 9 . 5 N D N D N D No t e s : ~ - N C D E N R 2 L G r o u n d w a t e r S t a n d a r d n o t a v a i l a b l e ug / L - m i c r o g r a m s p e r L i t e r mg / L - m i l l i g r a m s p e r L i t e r ND - N o n D e t e c t DT W - D e p t h t o w a t e r ft b g s - f e e t b e l o w g r o u n d s u r f a c e TP H - G R O T o t a l P e t r o l e u m H y d r o c a r b o n s G a s o l i n e R a n g e O r g a n i c s TP H - D R O T o t a l P e t r o l e u m H y d r o c a r b o n s D i e s e l R a n g e O r g a n i c s TP H - G R O Un i t s Vo l a t i l e O r g a n i c C o m p o u n d s ( V O C s ) TP H - D R O RC R A 8 M e t a l s 2L G r o u n d w a t e r St a n d a r d GE S - O c t o b e r 2 0 1 5 1 o f 1 N G r a h a m H o p e d a l e R d , B u r l i n g t o n , N C ATTACHMENT A Boring Logs PROJECT MANAGER: DATES DRILLED: PROJECT INFORMATION DRILLING INFORMATION Soil Boring Log DEPTH DRILLING CO.: RIG TYPE: DRILLING METHOD: SOIL SYMBOLS BORING DEPTH: DRILLER: (ppm)SOIL DESCRIPTION Soil Boring ID: PID LOGGED BY: JOB NAME: SITE LOCATION: PROJECT: NOTES Soil Boring ID SAMPLING METHODS: Water Level Soil Sample Location Sheetz - Burlington, NCGES - October 2015 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 1202193 Nick Braun 9/25/2015 SB-1/MW-1 Danny Breckenridge 6620DT Geoprobe Geoprobe DT22 Continuous Dual Tube 25 feet Corey Gamwell SB-1/MW-1 Ground Zero Proposed Sheetz - N. Graham Hopedale Road Burlington, North Carolina Asphalt Orange CLAY, non-plastic, slightly moist, and soft. Orange SILTY CLAY, non-plastic, dry, and soft. Orange CLAYEY SILT, non-plastic, slightly moist,soft, and brittle. Light brown to orange, CLAYEY SILT, non-plastic, soft, and brittle. Black vertical striations observed at 16' below ground surface. Light brown to orange CLAYEY SILT, non-plastic, soft, and brittle. Light brown SAND and SILT, fine grained, non-plastic, moist, and soft. Soil sample collected at 16'-18' bls. Analyzed for BTEX, MTBE, Naphthalene, THP-GRO, TPH- DRO, and RCRA 8 Metals. Temporary 1" PVC schedule 40, 10 slot screen placed from 15'-25' bls. Groundwater was collected and analyzed for BTEX, MTBE,Naphthalene, TPH-GRO, TPH-DRO and RCRA 8 Metals. 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 PROJECT MANAGER: DATES DRILLED: PROJECT INFORMATION DRILLING INFORMATION Soil Boring Log DEPTH DRILLING CO.: RIG TYPE: DRILLING METHOD: SOIL SYMBOLS BORING DEPTH: DRILLER: (ppm)SOIL DESCRIPTION Soil Boring ID: PID LOGGED BY: JOB NAME: SITE LOCATION: PROJECT: NOTES Soil Boring ID SAMPLING METHODS: Water Level Soil Sample Location Sheetz - Burlington, NCGES - October 2015 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 1202193 Nick Braun 9/25/2015 SB-2/MW-2 Danny Breckenridge 6620DT Geoprobe Geoprobe DT22 Continuous Dual Tube 25 feet Corey Gamwell SB-2/MW-2 Ground Zero Proposed Sheetz - N. Graham Hopedale Road Burlington, North Carolina Asphalt and gravel Orange CLAY, non-plastic, slightly moist, and soft. Orange SANDY CLAY, fine grained, slightly plastic, slightly moist. Tan CLAY with fine SAND, with black vertical striations. Tan SANDY CLAY, fine grained, dry, and brittle. Tan SANDY CLAY, fine grained, slightly plastic, and moist.Soil sample collected at 16'-18' bls. Analyzed for BTEX, MTBE, Naphthalene, THP-GRO, TPH- DRO, and RCRA 8 Metals. Temporary 1" PVC schedule 40, 10 slot screen placed from 15'-25' bls. Groundwater was collected and analyzed for BTEX, MTBE,Naphthalene, TPH-GRO, TPH-DRO and RCRA 8 Metals. 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 PROJECT MANAGER: DATES DRILLED: PROJECT INFORMATION DRILLING INFORMATION Soil Boring Log DEPTH DRILLING CO.: RIG TYPE: DRILLING METHOD: SOIL SYMBOLS BORING DEPTH: DRILLER: (ppm)SOIL DESCRIPTION Soil Boring ID: PID LOGGED BY: JOB NAME: SITE LOCATION: PROJECT: NOTES Soil Boring ID SAMPLING METHODS: Water Level Soil Sample Location Sheetz - Burlington, NCGES - October 2015 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 1202193 Nick Braun 9/25/2015 SB-3/MW-3 Danny Breckenridge 6620DT Geoprobe Geoprobe DT22 Continuous Dual Tube 25 feet Corey Gamwell SB-3/MW-3 Ground Zero Proposed Sheetz - N. Graham Hopedale Road Burlington, North Carolina Asphalt and gravel Orange SILTY CLAY, non-plastic, dry, and brittle. Orange SANDY CLAY, fine grained, slightly plastic, slightly moist, and dry. Tan SILT non-plastic, slighltly moist, white mottling, and slight odor. Tan, SANDY SILT, fine grained, non-plastic, soft, strong odor. Tan SANDY SILT, fine grained, non-plastic, soft, and brittle. Brown SILTY CLAY, rounded pebbles, non-plastic,and moist. White to tan SILT, non-plastic, wet, and loose. Soil sample collected at 13'-15'bls. Analyzed for BTEX, MTBE, Naphthalene, THP-GRO, TPH- DRO, and RCRA 8 Metals. Temporary 1" PVC schedule 40, 10 slot screen placed from 15'-25' bls. Groundwater was collected and analyzed for BTEX, MTBE,Naphthalene, TPH-GRO, TPH-DRO and RCRA 8 Metals. 0.0 0.0 0.0 0.0 0.0 0.2 0.3 0.6 3.2 711 23.4 15.1 12.7 273 375 4.4 3.3 4.1 3.0 0.5 0.7 0.3 2.0 3.0 PROJECT MANAGER: DATES DRILLED: PROJECT INFORMATION DRILLING INFORMATION Soil Boring Log DEPTH DRILLING CO.: RIG TYPE: DRILLING METHOD: SOIL SYMBOLS BORING DEPTH: DRILLER: (ppm)SOIL DESCRIPTION Soil Boring ID: PID LOGGED BY: JOB NAME: SITE LOCATION: PROJECT: NOTES Soil Boring ID SAMPLING METHODS: Water Level Soil Sample Location Sheetz - Burlington, NCGES - October 2015 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 1202193 Nick Braun 9/25/2015 SB-4/MW-4 Danny Breckenridge 6620DT Geoprobe Geoprobe DT22 Continuous Dual Tube 25 feet Corey Gamwell SB-4/MW-4 Ground Zero Proposed Sheetz - N. Graham Hopedale Road Burlington, North Carolina Asphalt and gravel Orange SILTY CLAY, non-plastic, dry, and brittle. Orange SANDY CLAY, fine grained, slightly plastic, slightly moist, and strong. Brown to tan CLAYEY SILT, slightly moist, brittle, and loose. Black striations observed at 15' bgs. Brown to tan SILT, non-plastic, and black vertical striations. Brown to tan SILT, non-plastic, loose, and wet. Soil sample collected at 13'-15'bls. Analyzed for BTEX, MTBE, Naphthalene, THP-GRO, TPH- DRO, and RCRA 8 Metals. Temporary 1" PVC schedule 40, 10 slot screen placed from 15'-25' bls. Groundwater was collected and analyzed for BTEX, MTBE,Naphthalene, TPH-GRO, TPH-DRO and RCRA 8 Metals. 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 PROJECT MANAGER: DATES DRILLED: PROJECT INFORMATION DRILLING INFORMATION Soil Boring Log DEPTH DRILLING CO.: RIG TYPE: DRILLING METHOD: SOIL SYMBOLS BORING DEPTH: DRILLER: (ppm)SOIL DESCRIPTION Soil Boring ID: PID LOGGED BY: JOB NAME: SITE LOCATION: PROJECT: NOTES Soil Boring ID SAMPLING METHODS: Water Level Soil Sample Location Sheetz - Burlington, NCGES - October 2015 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 1202193 Nick Braun 9/25/2015 SB-5/MW-5 Danny Breckenridge 6620DT Geoprobe Geoprobe DT22 Continuous Dual Tube 25 feet Corey Gamwell SB-5/MW-5 Ground Zero Proposed Sheetz - N. Graham Hopedale Road Burlington, North Carolina Asphalt and gravel Tan SILTY CLAY, non-plastic, dry, and soft. Tan SILTY CLAY, slightly plastic, slightly moist. Black vertical striations. Tan SILTY CLAY, slightly plastic, slightly moist.Black vertical striations. Appeared wet and saturated at 18' bgs. Soil sample collected at 16'-18' bls. Analyzed for BTEX, MTBE, Naphthalene, THP-GRO, TPH- DRO, and RCRA 8 Metals. Temporary 1" PVC schedule 40, 10 slot screen placed from 15'-25' bls. Groundwater was collected and analyzed for BTEX, MTBE,Naphthalene, TPH-GRO, TPH-DRO and RCRA 8 Metals. 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 PROJECT MANAGER: DATES DRILLED: PROJECT INFORMATION DRILLING INFORMATION Soil Boring Log DEPTH DRILLING CO.: RIG TYPE: DRILLING METHOD: SOIL SYMBOLS BORING DEPTH: DRILLER: (ppm)SOIL DESCRIPTION Soil Boring ID: PID LOGGED BY: JOB NAME: SITE LOCATION: PROJECT: NOTES Soil Boring ID SAMPLING METHODS: Water Level Soil Sample Location Sheetz - Burlington, NCGES - October 2015 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 1202193 Nick Braun 9/25/2015 SB-6/MW-6 Danny Breckenridge 6620DT Geoprobe Geoprobe DT22 Continuous Dual Tube 25 feet Corey Gamwell SB-6/MW-6 Ground Zero Proposed Sheetz - N. Graham Hopedale Road Burlington, North Carolina Asphalt and gravel Tan SILTY CLAY, non-plastic, dry, and soft. Green to Blue CLAYEY SILT, non-plastic, and soft. Brown CLAYEY SILT, non-plastic, and soft. Tan SILT, non-plastic, slightly moist. Silt becomes a white SILT at 10' bgs. Tan to white SILTY CLAY, non-plastic, and soft. Light grey to tan SILT with black vertical striations. Soil sample collected at 14'-16' bls. Analyzed for BTEX, MTBE, Naphthalene, THP-GRO, TPH- DRO, and RCRA 8 Metals. Temporary 1" PVC schedule 40, 10 slot screen placed from 15'-25' bls. Groundwater was collected and analyzed for BTEX, MTBE,Naphthalene, TPH-GRO, TPH-DRO and RCRA 8 Metals. 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 ATTACHMENT B Photo Essay Groundwater & Environmental Services PHOTOGRAPHIC RECORD CLIENT: Sheetz, Inc. SITE NAME: SITE LOCATION: PHOTOGRAPHER: Nick Braun DATE: September 25, 2015 DIRECTION: South COMMENTS: PHOTOGRAPHER: Nick Braun DATE: September 25, 2015 DIRECTION: South COMMENTS: On September 25, 2015 GES and Ground Zero performed subsurface drilling activities on the Subject Property. Ground Zero utilized a 6620DT Geoprobe rig to collect soil and temporary groundwater samples. The drill rig in this photograph was set up on boring location SB-1/MW- 1 on the northwest corner of the property adjacent to the former industrial facility. Boring location SB-2/MW-2 was located downgradient across N Graham Hopedale adjacent to the UST tank field of the active retail petroleum facility. PHOTO NO. 1 & 2 Proposed Sheetz N Graham Hopedale Rd, Burlington, North Carolina N Graham Hopedale Rd and N Church St. Burlington, North Carolina, 27217 Groundwater & Environmental Services PHOTOGRAPHIC RECORD CLIENT: Sheetz, Inc. SITE NAME: SITE LOCATION: PHOTOGRAPHER: Nick Braun DATE: September 25, 2015 DIRECTION: West COMMENTS: PHOTOGRAPHER: Nick Braun DATE: September 25, 2015 DIRECTION: East COMMENTS: Boring location SB-3/MW-3 was located on the southwest corner of the Subject Property. Ground Zero utilized the DT22 continuous dual- tube sampling method. Once the boring was completed to 25-feet below ground surface, Ground Zero installed a 1-inch diameter PVC 10-slot screen and riser inside the borehole. GES collected groundwater six groundwater samples from each temporary well (MW-1 through MW- 6). PHOTO NO. 3 & 4 Proposed Sheetz N Graham Hopedale Rd, Burlington, North Carolina N Graham Hopedale Rd and N Church St. Burlington, North Carolina, 27217 ATTACHMENT C Laboratory Analytical Report 1941 Reymet Road l Richmond, Virginia 23237 l Tel: (804)-358-8295 Fax: (804)-358-8297 Laboratory Order ID 15I0632 Certificate of Analysis Client Name: Enclosed are the results of analyses for samples received by the laboratory on 09/28/2015 08:35. If you have any questions concerning this report, please feel free to contact the laboratory. Sincerely, Ted Soyars Laboratory Manager Richmond, VA 23227 3701 Saunders Ave. Purchase Order: [none]Project Number: Date Issued: Date Received: Submitted To: Client Site I.D.: October 5, 2015 16:49 September 28, 2015 8:35Groundwater Environmental Services, Inc.-R Nick Braun End Notes: The test results listed in this report relate only to the samples submitted to the laboratory and as received by the Laboratory. Unless otherwise noted, the test results for solid materials are calculated on a wet weight basis. Analyses for pH, dissolved oxygen, temperature, residual chlorine and sulfite that are performed in the laboratory do not meet NELAC requirements due to extremely short holding times. These analyses should be performed in the field. The results of field analyses performed by the Sampler included in the Certificate of Analysis are done so at the client’s request and are not included in the laboratory’s fields of certification nor have they been audited for adherence to a reference method or procedure. The signature on the final report certifies that these results conform to all applicable NELAC standards unless otherwise specified. For a complete list of the Laboratory’s NELAC certified parameters please contact customer service. This report shall not be reproduced except in full without the expressed and written approval of an authorized representative of Air Water & Soil Laboratories, Inc. Sheetz - Hopedale and Church Rd. Final Report Page 1 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Sample ID Laboratory ID Matrix Date Sampled Date Received ANALYTICAL REPORT FOR SAMPLES SB-1 (16-18')15I0632-01 09/28/2015 08:35Solids09/25/2015 10:50 SB-2 (16-18')15I0632-02 09/28/2015 08:35Solids09/25/2015 12:10 SB-3 (13-15)15I0632-03 09/28/2015 08:35Solids09/25/2015 13:30 SB-4 (13-15)15I0632-04 09/28/2015 08:35Solids09/25/2015 14:40 SB-5 (16-18)15I0632-05 09/28/2015 08:35Solids09/25/2015 15:30 SB-6 (14-16)15I0632-06 09/28/2015 08:35Solids09/25/2015 17:00 Trip Blank 15I0632-07 09/28/2015 08:35Ground Water 09/15/2015 15:30 MW-1 15I0632-08 09/28/2015 08:35Ground Water 09/25/2015 14:15 MW-2 15I0632-09 09/28/2015 08:35Ground Water 09/25/2015 14:50 MW-3 15I0632-10 09/28/2015 08:35Ground Water 09/25/2015 15:45 MW-4 15I0632-11 09/28/2015 08:35Ground Water 09/25/2015 16:35 MW-5 15I0632-12 09/28/2015 08:35Ground Water 09/25/2015 17:10 MW-6 15I0632-13 09/28/2015 08:35Ground Water 09/25/2015 17:45 Trip Blank 15I0632-14 09/28/2015 08:35Ground Water 09/15/2015 15:30 Page 2 of 36Page 2 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report ResultParameter Reporting LimitMethodQual Analyst Analysis Date/Time SB-1 (16-18') 09/25/2015 10:50 Analytical Results Laboratory Sample ID:Sample I.D. Date/Time Sampled: D.F. Samp ID 15I0632-01 Sample Prep Date/Time Metals (Total) by EPA 6000/7000 Series Methods SW6010C KEW<0.500 mg/kg 0.500 101 09/29/15 11:30 10/02/15 18:03Silver SW6010C KEW<1.00 mg/kg 1.00 101 09/29/15 11:30 10/02/15 18:03Arsenic SW6010C 54.8 mg/kg KEW0.500 101 09/29/15 11:30 10/02/15 18:03Barium SW6010C 0.460 mg/kg KEW0.200 101 09/29/15 11:30 10/02/15 18:03Cadmium SW6010C 3.49 mg/kg KEW0.500 101 09/29/15 11:30 10/02/15 18:03Chromium SW7471B AA<0.008 mg/kg 0.008 101 09/29/15 11:00 09/29/15 13:57Mercury SW6010C <0.500 mg/kg KEW0.500 101 09/29/15 11:30 10/02/15 18:03Lead SW6010C KEW<2.50 mg/kg 2.50 101 09/29/15 11:30 10/02/15 18:03Selenium Volatile Organic Compounds by GC SW8021B CL<5.00 ug/kg 5.00 101 09/30/15 15:33 09/30/15 15:33Methyl-t-butyl ether (MTBE) SW8021B CL<5.00 ug/kg 5.00 101 09/30/15 15:33 09/30/15 15:33Benzene SW8021B CL<5.00 ug/kg 5.00 101 09/30/15 15:33 09/30/15 15:33Toluene SW8021B CL<5.00 ug/kg 5.00 101 09/30/15 15:33 09/30/15 15:33Ethylbenzene SW8021B CL<10.0 ug/kg 10.0 101 09/30/15 15:33 09/30/15 15:33m+p-Xylenes SW8021B CL<5.00 ug/kg 5.00 101 09/30/15 15:33 09/30/15 15:33o-Xylene SW8021B CL<15.0 ug/kg 15.0 101 09/30/15 15:33 09/30/15 15:33Xylenes, Total SW8021B CL<5.00 ug/kg 5.00 101 09/30/15 15:33 09/30/15 15:33Naphthalene 80-12086.3 %Surr: 2,5-Dibromotoluene CL01SW8021B09/30/15 15:33 09/30/15 15:33 Volatile Hydrocarbons by GC SW8015C CL<0.10 mg/kg 0.10 101 09/30/15 15:33 09/30/15 15:33TPH-Volatiles (GRO) Semivolatile Hydrocarbons by GC SW8015C JHV<10.0 mg/kg 10.0 101 09/29/15 15:11 09/30/15 17:48TPH-Semi-Volatiles (DRO) 40-16079.3 %Surr: Pentacosane JHV01SW8015C09/29/15 15:11 09/30/15 17:48 Page 3 of 36Page 3 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report ResultParameter Reporting LimitMethodQual Analyst Analysis Date/Time SB-2 (16-18') 09/25/2015 12:10 Analytical Results Laboratory Sample ID:Sample I.D. Date/Time Sampled: D.F. Samp ID 15I0632-02 Sample Prep Date/Time Metals (Total) by EPA 6000/7000 Series Methods SW6010C KEW<0.500 mg/kg 0.500 102 09/29/15 11:30 10/02/15 18:08Silver SW6010C KEW<1.00 mg/kg 1.00 102 09/29/15 11:30 10/02/15 18:08Arsenic SW6010C 59.0 mg/kg KEW0.500 102 09/29/15 11:30 10/02/15 18:08Barium SW6010C 0.526 mg/kg KEW0.200 102 09/29/15 11:30 10/02/15 18:08Cadmium SW6010C 0.776 mg/kg KEW0.500 102 09/29/15 11:30 10/02/15 18:08Chromium SW7471B AA<0.008 mg/kg 0.008 102 09/29/15 11:00 09/29/15 14:05Mercury SW6010C 3.23 mg/kg KEW0.500 102 09/29/15 11:30 10/02/15 18:08Lead SW6010C KEW<2.50 mg/kg 2.50 102 09/29/15 11:30 10/02/15 18:08Selenium Volatile Organic Compounds by GC SW8021B CL<5.00 ug/kg 5.00 102 09/30/15 15:56 09/30/15 15:56Methyl-t-butyl ether (MTBE) SW8021B CL<5.00 ug/kg 5.00 102 09/30/15 15:56 09/30/15 15:56Benzene SW8021B CL<5.00 ug/kg 5.00 102 09/30/15 15:56 09/30/15 15:56Toluene SW8021B CL<5.00 ug/kg 5.00 102 09/30/15 15:56 09/30/15 15:56Ethylbenzene SW8021B CL<10.0 ug/kg 10.0 102 09/30/15 15:56 09/30/15 15:56m+p-Xylenes SW8021B CL<5.00 ug/kg 5.00 102 09/30/15 15:56 09/30/15 15:56o-Xylene SW8021B CL<15.0 ug/kg 15.0 102 09/30/15 15:56 09/30/15 15:56Xylenes, Total SW8021B CL<5.00 ug/kg 5.00 102 09/30/15 15:56 09/30/15 15:56Naphthalene 80-12085.8 %Surr: 2,5-Dibromotoluene CL02SW8021B09/30/15 15:56 09/30/15 15:56 Volatile Hydrocarbons by GC SW8015C CL<0.10 mg/kg 0.10 102 09/30/15 15:56 09/30/15 15:56TPH-Volatiles (GRO) Semivolatile Hydrocarbons by GC SW8015C JHV<10.0 mg/kg 10.0 102 09/29/15 15:11 09/30/15 18:15TPH-Semi-Volatiles (DRO) 40-16066.0 %Surr: Pentacosane JHV02SW8015C09/29/15 15:11 09/30/15 18:15 Page 4 of 36Page 4 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report ResultParameter Reporting LimitMethodQual Analyst Analysis Date/Time SB-3 (13-15) 09/25/2015 13:30 Analytical Results Laboratory Sample ID:Sample I.D. Date/Time Sampled: D.F. Samp ID 15I0632-03 Sample Prep Date/Time Metals (Total) by EPA 6000/7000 Series Methods SW6010C KEW<0.500 mg/kg 0.500 103 09/29/15 11:30 10/02/15 18:31Silver SW6010C KEW<1.00 mg/kg 1.00 103 09/29/15 11:30 10/02/15 18:32Arsenic SW6010C KEW<0.500 mg/kg 0.500 103 09/29/15 11:30 10/02/15 18:32Barium SW6010C KEW<0.200 mg/kg 0.200 103 09/29/15 11:30 10/02/15 18:32Cadmium SW6010C KEW<0.500 mg/kg 0.500 103 09/29/15 11:30 10/02/15 18:32Chromium SW7471B AA<0.008 mg/kg 0.008 103 09/29/15 11:00 09/29/15 14:07Mercury SW6010C KEW<0.500 mg/kg 0.500 103 09/29/15 11:30 10/02/15 18:32Lead SW6010C KEW<2.50 mg/kg 2.50 103 09/29/15 11:30 10/02/15 18:32Selenium Volatile Organic Compounds by GC SW8021B CL<5.00 ug/kg 5.00 103 10/01/15 00:55 10/01/15 00:55Methyl-t-butyl ether (MTBE) SW8021B CL<5.00 ug/kg 5.00 103 10/01/15 00:55 10/01/15 00:55Benzene SW8021B 30.7 ug/kg CL5.00 103 10/01/15 00:55 10/01/15 00:55Toluene SW8021B 142 ug/kg CL5.00 103 10/01/15 00:55 10/01/15 00:55Ethylbenzene SW8021B 316 ug/kg CL10.0 103 10/01/15 00:55 10/01/15 00:55m+p-Xylenes SW8021B 190 ug/kg CL5.00 103 10/01/15 00:55 10/01/15 00:55o-Xylene SW8021B 506 ug/kg CL15.0 103 10/01/15 00:55 10/01/15 00:55Xylenes, Total SW8021B 295 ug/kg CL5.00 103 10/01/15 00:55 10/01/15 00:55Naphthalene 80-120102 %Surr: 2,5-Dibromotoluene CL03SW8021B10/01/15 00:55 10/01/15 00:55 Volatile Hydrocarbons by GC SW8015C 11.1 mg/kg CL0.41 103 10/01/15 00:55 10/01/15 00:55TPH-Volatiles (GRO) Semivolatile Hydrocarbons by GC SW8015C 16.8 mg/kg JHV10.0 103 09/29/15 15:11 09/30/15 18:41TPH-Semi-Volatiles (DRO) 40-16078.0 %Surr: Pentacosane JHV03SW8015C09/29/15 15:11 09/30/15 18:41 Page 5 of 36Page 5 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report ResultParameter Reporting LimitMethodQual Analyst Analysis Date/Time SB-4 (13-15) 09/25/2015 14:40 Analytical Results Laboratory Sample ID:Sample I.D. Date/Time Sampled: D.F. Samp ID 15I0632-04 Sample Prep Date/Time Metals (Total) by EPA 6000/7000 Series Methods SW6010C KEW<0.500 mg/kg 0.500 104 09/29/15 11:30 10/02/15 18:36Silver SW6010C KEW<1.00 mg/kg 1.00 104 09/29/15 11:30 10/02/15 18:37Arsenic SW6010C KEW<0.500 mg/kg 0.500 104 09/29/15 11:30 10/02/15 18:37Barium SW6010C KEW<0.200 mg/kg 0.200 104 09/29/15 11:30 10/02/15 18:37Cadmium SW6010C KEW<0.500 mg/kg 0.500 104 09/29/15 11:30 10/02/15 18:37Chromium SW7471B 0.011 mg/kg AA0.008 104 09/29/15 11:00 09/29/15 14:09Mercury SW6010C KEW<0.500 mg/kg 0.500 104 09/29/15 11:30 10/02/15 18:37Lead SW6010C KEW<2.50 mg/kg 2.50 104 09/29/15 11:30 10/02/15 18:37Selenium Volatile Organic Compounds by GC SW8021B CL<5.00 ug/kg 5.00 104 09/30/15 23:24 09/30/15 23:24Methyl-t-butyl ether (MTBE) SW8021B CL<5.00 ug/kg 5.00 104 09/30/15 23:24 09/30/15 23:24Benzene SW8021B CL<5.00 ug/kg 5.00 104 09/30/15 23:24 09/30/15 23:24Toluene SW8021B CL<5.00 ug/kg 5.00 104 09/30/15 23:24 09/30/15 23:24Ethylbenzene SW8021B CL<10.0 ug/kg 10.0 104 09/30/15 23:24 09/30/15 23:24m+p-Xylenes SW8021B CL<5.00 ug/kg 5.00 104 09/30/15 23:24 09/30/15 23:24o-Xylene SW8021B CL<15.0 ug/kg 15.0 104 09/30/15 23:24 09/30/15 23:24Xylenes, Total SW8021B CL<5.00 ug/kg 5.00 104 09/30/15 23:24 09/30/15 23:24Naphthalene 80-12093.4 %Surr: 2,5-Dibromotoluene CL04SW8021B09/30/15 23:24 09/30/15 23:24 Volatile Hydrocarbons by GC SW8015C CL<0.10 mg/kg 0.10 104 09/30/15 23:24 09/30/15 23:24TPH-Volatiles (GRO) Semivolatile Hydrocarbons by GC SW8015C JHV<10.0 mg/kg 10.0 104 09/29/15 15:11 09/30/15 19:08TPH-Semi-Volatiles (DRO) 40-16070.4 %Surr: Pentacosane JHV04SW8015C09/29/15 15:11 09/30/15 19:08 Page 6 of 36Page 6 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report ResultParameter Reporting LimitMethodQual Analyst Analysis Date/Time SB-5 (16-18) 09/25/2015 15:30 Analytical Results Laboratory Sample ID:Sample I.D. Date/Time Sampled: D.F. Samp ID 15I0632-05 Sample Prep Date/Time Metals (Total) by EPA 6000/7000 Series Methods SW6010C KEW<0.500 mg/kg 0.500 105 09/29/15 11:30 10/02/15 18:41Silver SW6010C KEW<1.00 mg/kg 1.00 105 09/29/15 11:30 10/02/15 18:41Arsenic SW6010C KEW<0.500 mg/kg 0.500 105 09/29/15 11:30 10/02/15 18:41Barium SW6010C KEW<0.200 mg/kg 0.200 105 09/29/15 11:30 10/02/15 18:41Cadmium SW6010C KEW<0.500 mg/kg 0.500 105 09/29/15 11:30 10/02/15 18:41Chromium SW7471B AA<0.008 mg/kg 0.008 105 09/29/15 11:00 09/29/15 14:16Mercury SW6010C KEW<0.500 mg/kg 0.500 105 09/29/15 11:30 10/02/15 18:41Lead SW6010C KEW<2.50 mg/kg 2.50 105 09/29/15 11:30 10/02/15 18:41Selenium Volatile Organic Compounds by GC SW8021B CL<5.00 ug/kg 5.00 105 09/30/15 23:47 09/30/15 23:47Methyl-t-butyl ether (MTBE) SW8021B CL<5.00 ug/kg 5.00 105 09/30/15 23:47 09/30/15 23:47Benzene SW8021B CL<5.00 ug/kg 5.00 105 09/30/15 23:47 09/30/15 23:47Toluene SW8021B CL<5.00 ug/kg 5.00 105 09/30/15 23:47 09/30/15 23:47Ethylbenzene SW8021B CL<10.0 ug/kg 10.0 105 09/30/15 23:47 09/30/15 23:47m+p-Xylenes SW8021B CL<5.00 ug/kg 5.00 105 09/30/15 23:47 09/30/15 23:47o-Xylene SW8021B CL<15.0 ug/kg 15.0 105 09/30/15 23:47 09/30/15 23:47Xylenes, Total SW8021B CL<5.00 ug/kg 5.00 105 09/30/15 23:47 09/30/15 23:47Naphthalene 80-12094.8 %Surr: 2,5-Dibromotoluene CL05SW8021B09/30/15 23:47 09/30/15 23:47 Volatile Hydrocarbons by GC SW8015C CL<0.10 mg/kg 0.10 105 09/30/15 23:47 09/30/15 23:47TPH-Volatiles (GRO) Semivolatile Hydrocarbons by GC SW8015C JHV<10.0 mg/kg 10.0 105 09/29/15 15:11 09/30/15 19:35TPH-Semi-Volatiles (DRO) 40-16070.8 %Surr: Pentacosane JHV05SW8015C09/29/15 15:11 09/30/15 19:35 Page 7 of 36Page 7 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report ResultParameter Reporting LimitMethodQual Analyst Analysis Date/Time SB-6 (14-16) 09/25/2015 17:00 Analytical Results Laboratory Sample ID:Sample I.D. Date/Time Sampled: D.F. Samp ID 15I0632-06 Sample Prep Date/Time Metals (Total) by EPA 6000/7000 Series Methods SW6010C KEW<0.500 mg/kg 0.500 106 09/29/15 11:30 10/02/15 18:46Silver SW6010C KEW<1.00 mg/kg 1.00 106 09/29/15 11:30 10/02/15 18:46Arsenic SW6010C KEW<0.500 mg/kg 0.500 106 09/29/15 11:30 10/02/15 18:46Barium SW6010C KEW<0.200 mg/kg 0.200 106 09/29/15 11:30 10/02/15 18:46Cadmium SW6010C KEW<0.500 mg/kg 0.500 106 09/29/15 11:30 10/02/15 18:46Chromium SW7471B AA<0.008 mg/kg 0.008 106 09/29/15 11:00 09/29/15 14:18Mercury SW6010C KEW<0.500 mg/kg 0.500 106 09/29/15 11:30 10/02/15 18:46Lead SW6010C KEW<2.50 mg/kg 2.50 106 09/29/15 11:30 10/02/15 18:46Selenium Volatile Organic Compounds by GC SW8021B CL<5.00 ug/kg 5.00 106 10/01/15 00:09 10/01/15 00:09Methyl-t-butyl ether (MTBE) SW8021B CL<5.00 ug/kg 5.00 106 10/01/15 00:09 10/01/15 00:09Benzene SW8021B CL<5.00 ug/kg 5.00 106 10/01/15 00:09 10/01/15 00:09Toluene SW8021B CL<5.00 ug/kg 5.00 106 10/01/15 00:09 10/01/15 00:09Ethylbenzene SW8021B CL<10.0 ug/kg 10.0 106 10/01/15 00:09 10/01/15 00:09m+p-Xylenes SW8021B CL<5.00 ug/kg 5.00 106 10/01/15 00:09 10/01/15 00:09o-Xylene SW8021B CL<15.0 ug/kg 15.0 106 10/01/15 00:09 10/01/15 00:09Xylenes, Total SW8021B CL<5.00 ug/kg 5.00 106 10/01/15 00:09 10/01/15 00:09Naphthalene 80-12089.7 %Surr: 2,5-Dibromotoluene CL06SW8021B10/01/15 00:09 10/01/15 00:09 Volatile Hydrocarbons by GC SW8015C CL<0.10 mg/kg 0.10 106 10/01/15 00:09 10/01/15 00:09TPH-Volatiles (GRO) Semivolatile Hydrocarbons by GC SW8015C JHV<10.0 mg/kg 10.0 106 09/29/15 15:11 09/30/15 20:01TPH-Semi-Volatiles (DRO) 40-16075.2 %Surr: Pentacosane JHV06SW8015C09/29/15 15:11 09/30/15 20:01 Page 8 of 36Page 8 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report ResultParameter Reporting LimitMethodQual Analyst Analysis Date/Time Trip Blank 09/15/2015 15:30 Analytical Results Laboratory Sample ID:Sample I.D. Date/Time Sampled: D.F. Samp ID 15I0632-07 Sample Prep Date/Time Volatile Organic Compounds by GC SW8021B CL<5.00 ug/L 5.00 107 09/30/15 14:01 09/30/15 14:01Methyl-t-butyl ether (MTBE) SW8021B CL<1.00 ug/L 1.00 107 09/30/15 14:01 09/30/15 14:01Benzene SW8021B CL<1.00 ug/L 1.00 107 09/30/15 14:01 09/30/15 14:01Toluene SW8021B CL<1.00 ug/L 1.00 107 09/30/15 14:01 09/30/15 14:01Ethylbenzene SW8021B CL<4.00 ug/L 4.00 107 09/30/15 14:01 09/30/15 14:01m+p-Xylenes SW8021B CL<2.00 ug/L 2.00 107 09/30/15 14:01 09/30/15 14:01o-Xylene SW8021B CL<6.00 ug/L 6.00 107 09/30/15 14:01 09/30/15 14:01Xylenes, Total SW8021B <6.00 ug/L CL6.00 107 09/30/15 14:01 09/30/15 14:01Naphthalene 80-12087.8 %Surr: 2,5-Dibromotoluene CL07SW8021B09/30/15 14:01 09/30/15 14:01 Volatile Hydrocarbons by GC SW8015C CL<0.10 mg/L 0.10 107 09/30/15 14:01 09/30/15 14:01TPH-Volatiles (GRO) Page 9 of 36Page 9 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report ResultParameter Reporting LimitMethodQual Analyst Analysis Date/Time MW-1 09/25/2015 14:15 Analytical Results Laboratory Sample ID:Sample I.D. Date/Time Sampled: D.F. Samp ID 15I0632-08 Sample Prep Date/Time Metals (Total) by EPA 6000/7000 Series Methods SW6010C KEW<0.0100 mg/L 0.0100 108 09/28/15 16:50 10/01/15 18:56Silver SW6010C KEW<0.0100 mg/L 0.0100 108 09/28/15 16:50 10/05/15 15:16Arsenic SW6010C 0.226 mg/L KEW0.0100 108 09/28/15 16:50 10/01/15 18:56Barium SW6010C KEW<0.0050 mg/L 0.0050 108 09/28/15 16:50 10/01/15 18:56Cadmium SW6010C <0.0100 mg/L KEW0.0100 108 09/28/15 16:50 10/01/15 18:56Chromium SW7470A MWL<0.00020 mg/L 0.00020 108 09/30/15 12:45 10/01/15 11:42Mercury SW6010C KEW<0.0100 mg/L 0.0100 108 09/28/15 16:50 10/05/15 15:16Lead SW6010C KEW<0.0500 mg/L 0.0500 108 09/28/15 16:50 10/01/15 18:56Selenium Volatile Organic Compounds by GC Cl SW8021B CL<5.00 ug/L 5.00 108 10/01/15 03:13 10/01/15 03:13Methyl-t-butyl ether (MTBE) SW8021B CL<1.00 ug/L 1.00 108 10/01/15 03:13 10/01/15 03:13Benzene SW8021B CL<1.00 ug/L 1.00 108 10/01/15 03:13 10/01/15 03:13Toluene SW8021B CL<1.00 ug/L 1.00 108 10/01/15 03:13 10/01/15 03:13Ethylbenzene SW8021B CL<4.00 ug/L 4.00 108 10/01/15 03:13 10/01/15 03:13m+p-Xylenes SW8021B CL<2.00 ug/L 2.00 108 10/01/15 03:13 10/01/15 03:13o-Xylene SW8021B CL<6.00 ug/L 6.00 108 10/01/15 03:13 10/01/15 03:13Xylenes, Total SW8021B <6.00 ug/L CL6.00 108 10/01/15 03:13 10/01/15 03:13Naphthalene 80-12089.6 %Surr: 2,5-Dibromotoluene CL08SW8021B10/01/15 03:13 10/01/15 03:13 Volatile Hydrocarbons by GC Cl SW8015C CL<0.10 mg/L 0.10 108 10/01/15 03:13 10/01/15 03:13TPH-Volatiles (GRO) Semivolatile Hydrocarbons by GC SW8015C JHV<0.50 mg/L 0.50 108 09/30/15 11:15 09/30/15 23:34TPH-Semi-Volatiles (DRO) 40-16063.1 %Surr: Pentacosane JHV08SW8015C09/30/15 11:15 09/30/15 23:34 Page 10 of 36Page 10 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report ResultParameter Reporting LimitMethodQual Analyst Analysis Date/Time MW-2 09/25/2015 14:50 Analytical Results Laboratory Sample ID:Sample I.D. Date/Time Sampled: D.F. Samp ID 15I0632-09 Sample Prep Date/Time Metals (Total) by EPA 6000/7000 Series Methods SW6010C KEW<0.0100 mg/L 0.0100 109 09/28/15 16:50 10/01/15 19:01Silver SW6010C KEW<0.0100 mg/L 0.0100 109 09/28/15 16:50 10/05/15 15:20Arsenic SW6010C 0.212 mg/L KEW0.0100 109 09/28/15 16:50 10/01/15 19:01Barium SW6010C KEW<0.0050 mg/L 0.0050 109 09/28/15 16:50 10/01/15 19:01Cadmium SW6010C 0.0195 mg/L KEW0.0100 109 09/28/15 16:50 10/01/15 19:01Chromium SW7470A MWL<0.00020 mg/L 0.00020 109 09/30/15 12:45 10/01/15 11:44Mercury SW6010C KEW<0.0100 mg/L 0.0100 109 09/28/15 16:50 10/05/15 15:20Lead SW6010C KEW<0.0500 mg/L 0.0500 109 09/28/15 16:50 10/01/15 19:01Selenium Volatile Organic Compounds by GC SW8021B <5.00 ug/L CL5.00 109 10/01/15 03:35 10/01/15 03:35Methyl-t-butyl ether (MTBE) SW8021B CL<1.00 ug/L 1.00 109 10/01/15 03:35 10/01/15 03:35Benzene SW8021B CL<1.00 ug/L 1.00 109 10/01/15 03:35 10/01/15 03:35Toluene SW8021B CL<1.00 ug/L 1.00 109 10/01/15 03:35 10/01/15 03:35Ethylbenzene SW8021B CL<4.00 ug/L 4.00 109 10/01/15 03:35 10/01/15 03:35m+p-Xylenes SW8021B CL<2.00 ug/L 2.00 109 10/01/15 03:35 10/01/15 03:35o-Xylene SW8021B CL<6.00 ug/L 6.00 109 10/01/15 03:35 10/01/15 03:35Xylenes, Total SW8021B <6.00 ug/L CL6.00 109 10/01/15 03:35 10/01/15 03:35Naphthalene 80-12090.2 %Surr: 2,5-Dibromotoluene CL09SW8021B10/01/15 03:35 10/01/15 03:35 Volatile Hydrocarbons by GC SW8015C CL<0.10 mg/L 0.10 109 10/01/15 03:35 10/01/15 03:35TPH-Volatiles (GRO) Semivolatile Hydrocarbons by GC SW8015C JHV<0.50 mg/L 0.50 109 09/30/15 11:15 10/01/15 00:00TPH-Semi-Volatiles (DRO) 40-16067.9 %Surr: Pentacosane JHV09SW8015C09/30/15 11:15 10/01/15 00:00 Page 11 of 36Page 11 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report ResultParameter Reporting LimitMethodQual Analyst Analysis Date/Time MW-3 09/25/2015 15:45 Analytical Results Laboratory Sample ID:Sample I.D. Date/Time Sampled: D.F. Samp ID 15I0632-10 Sample Prep Date/Time Metals (Total) by EPA 6000/7000 Series Methods SW6010C KEW<0.0100 mg/L 0.0100 110 09/28/15 16:50 10/01/15 19:06Silver SW6010C KEW<0.0100 mg/L 0.0100 110 09/28/15 16:50 10/05/15 15:25Arsenic SW6010C 0.350 mg/L KEW0.0100 110 09/28/15 16:50 10/01/15 19:06Barium SW6010C KEW<0.0050 mg/L 0.0050 110 09/28/15 16:50 10/01/15 19:06Cadmium SW6010C <0.0100 mg/L KEW0.0100 110 09/28/15 16:50 10/01/15 19:06Chromium SW7470A MWL<0.00020 mg/L 0.00020 110 09/30/15 12:45 10/01/15 11:46Mercury SW6010C KEW<0.0100 mg/L 0.0100 110 09/28/15 16:50 10/05/15 15:25Lead SW6010C <0.0500 mg/L KEW0.0500 110 09/28/15 16:50 10/01/15 19:06Selenium Volatile Organic Compounds by GC SW8021B CL<5.00 ug/L 5.00 110 10/01/15 03:58 10/01/15 03:58Methyl-t-butyl ether (MTBE) SW8021B 212 ug/L CL1.00 110 10/01/15 03:58 10/01/15 03:58Benzene SW8021B 7.21 ug/L CL1.00 110 10/01/15 03:58 10/01/15 03:58Toluene SW8021B 6.64 ug/L CL1.00 110 10/01/15 03:58 10/01/15 03:58Ethylbenzene SW8021B 10.9 ug/L CL4.00 110 10/01/15 03:58 10/01/15 03:58m+p-Xylenes SW8021B <2.00 ug/L CL2.00 110 10/01/15 03:58 10/01/15 03:58o-Xylene SW8021B 12.4 ug/L CL6.00 110 10/01/15 03:58 10/01/15 03:58Xylenes, Total SW8021B 29.6 ug/L CL6.00 110 10/01/15 03:58 10/01/15 03:58Naphthalene 80-12093.3 %Surr: 2,5-Dibromotoluene CL10SW8021B10/01/15 03:58 10/01/15 03:58 Volatile Hydrocarbons by GC SW8015C 0.66 mg/L CL0.10 110 10/01/15 03:58 10/01/15 03:58TPH-Volatiles (GRO) Semivolatile Hydrocarbons by GC SW8015C <0.50 mg/L JHV0.50 110 09/30/15 11:15 10/01/15 00:27TPH-Semi-Volatiles (DRO) 40-16075.3 %Surr: Pentacosane JHV10SW8015C09/30/15 11:15 10/01/15 00:27 Page 12 of 36Page 12 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report ResultParameter Reporting LimitMethodQual Analyst Analysis Date/Time MW-4 09/25/2015 16:35 Analytical Results Laboratory Sample ID:Sample I.D. Date/Time Sampled: D.F. Samp ID 15I0632-11 Sample Prep Date/Time Metals (Total) by EPA 6000/7000 Series Methods SW6010C KEW<0.0100 mg/L 0.0100 111 09/28/15 16:50 10/01/15 19:11Silver SW6010C KEW<0.0100 mg/L 0.0100 111 09/28/15 16:50 10/05/15 15:30Arsenic SW6010C 0.172 mg/L KEW0.0100 111 09/28/15 16:50 10/01/15 19:11Barium SW6010C KEW<0.0050 mg/L 0.0050 111 09/28/15 16:50 10/01/15 19:11Cadmium SW6010C <0.0100 mg/L KEW0.0100 111 09/28/15 16:50 10/01/15 19:11Chromium SW7470A MWL<0.00020 mg/L 0.00020 111 09/30/15 12:45 10/01/15 11:48Mercury SW6010C KEW<0.0100 mg/L 0.0100 111 09/28/15 16:50 10/05/15 15:30Lead SW6010C KEW<0.0500 mg/L 0.0500 111 09/28/15 16:50 10/01/15 19:11Selenium Volatile Organic Compounds by GC Cl SW8021B CL<5.00 ug/L 5.00 111 10/01/15 04:21 10/01/15 04:21Methyl-t-butyl ether (MTBE) SW8021B CL<1.00 ug/L 1.00 111 10/01/15 04:21 10/01/15 04:21Benzene SW8021B CL<1.00 ug/L 1.00 111 10/01/15 04:21 10/01/15 04:21Toluene SW8021B CL<1.00 ug/L 1.00 111 10/01/15 04:21 10/01/15 04:21Ethylbenzene SW8021B CL<4.00 ug/L 4.00 111 10/01/15 04:21 10/01/15 04:21m+p-Xylenes SW8021B CL<2.00 ug/L 2.00 111 10/01/15 04:21 10/01/15 04:21o-Xylene SW8021B CL<6.00 ug/L 6.00 111 10/01/15 04:21 10/01/15 04:21Xylenes, Total SW8021B <6.00 ug/L CL6.00 111 10/01/15 04:21 10/01/15 04:21Naphthalene 80-12089.7 %Surr: 2,5-Dibromotoluene CL11SW8021B10/01/15 04:21 10/01/15 04:21 Volatile Hydrocarbons by GC Cl SW8015C CL<0.10 mg/L 0.10 111 10/01/15 04:21 10/01/15 04:21TPH-Volatiles (GRO) Semivolatile Hydrocarbons by GC SW8015C JHV<0.50 mg/L 0.50 111 09/30/15 14:23 10/02/15 01:35TPH-Semi-Volatiles (DRO) 40-16075.5 %Surr: Pentacosane JHV11SW8015C09/30/15 14:23 10/02/15 01:35 Page 13 of 36Page 13 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report ResultParameter Reporting LimitMethodQual Analyst Analysis Date/Time MW-5 09/25/2015 17:10 Analytical Results Laboratory Sample ID:Sample I.D. Date/Time Sampled: D.F. Samp ID 15I0632-12 Sample Prep Date/Time Metals (Total) by EPA 6000/7000 Series Methods SW6010C KEW<0.0100 mg/L 0.0100 112 09/28/15 16:50 10/01/15 19:16Silver SW6010C KEW<0.0100 mg/L 0.0100 112 09/28/15 16:50 10/05/15 15:35Arsenic SW6010C 0.506 mg/L KEW0.0100 112 09/28/15 16:50 10/01/15 19:16Barium SW6010C <0.0050 mg/L KEW0.0050 112 09/28/15 16:50 10/01/15 19:16Cadmium SW6010C 0.349 mg/L KEW0.0100 112 09/28/15 16:50 10/01/15 19:16Chromium SW7470A MWL<0.00020 mg/L 0.00020 112 09/30/15 12:45 10/01/15 12:01Mercury SW6010C KEW<0.0100 mg/L 0.0100 112 09/28/15 16:50 10/05/15 15:35Lead SW6010C <0.0500 mg/L KEW0.0500 112 09/28/15 16:50 10/01/15 19:16Selenium Volatile Organic Compounds by GC Cl SW8021B CL<5.00 ug/L 5.00 112 10/01/15 04:44 10/01/15 04:44Methyl-t-butyl ether (MTBE) SW8021B CL<1.00 ug/L 1.00 112 10/01/15 04:44 10/01/15 04:44Benzene SW8021B CL<1.00 ug/L 1.00 112 10/01/15 04:44 10/01/15 04:44Toluene SW8021B CL<1.00 ug/L 1.00 112 10/01/15 04:44 10/01/15 04:44Ethylbenzene SW8021B CL<4.00 ug/L 4.00 112 10/01/15 04:44 10/01/15 04:44m+p-Xylenes SW8021B CL<2.00 ug/L 2.00 112 10/01/15 04:44 10/01/15 04:44o-Xylene SW8021B CL<6.00 ug/L 6.00 112 10/01/15 04:44 10/01/15 04:44Xylenes, Total SW8021B <6.00 ug/L CL6.00 112 10/01/15 04:44 10/01/15 04:44Naphthalene 80-12090.7 %Surr: 2,5-Dibromotoluene CL12SW8021B10/01/15 04:44 10/01/15 04:44 Volatile Hydrocarbons by GC Cl SW8015C CL<0.10 mg/L 0.10 112 10/01/15 04:44 10/01/15 04:44TPH-Volatiles (GRO) Semivolatile Hydrocarbons by GC SW8015C JHV<0.50 mg/L 0.50 112 09/30/15 14:23 10/02/15 02:01TPH-Semi-Volatiles (DRO) 40-16074.7 %Surr: Pentacosane JHV12SW8015C09/30/15 14:23 10/02/15 02:01 Page 14 of 36Page 14 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report ResultParameter Reporting LimitMethodQual Analyst Analysis Date/Time MW-6 09/25/2015 17:45 Analytical Results Laboratory Sample ID:Sample I.D. Date/Time Sampled: D.F. Samp ID 15I0632-13 Sample Prep Date/Time Metals (Total) by EPA 6000/7000 Series Methods SW6010C KEW<0.0100 mg/L 0.0100 113 09/28/15 16:50 10/01/15 19:21Silver SW6010C KEW<0.0100 mg/L 0.0100 113 09/28/15 16:50 10/05/15 15:40Arsenic SW6010C 2.64 mg/L KEW0.0100 113 09/28/15 16:50 10/01/15 19:21Barium SW6010C 0.0077 mg/L KEW0.0050 113 09/28/15 16:50 10/01/15 19:21Cadmium SW6010C 0.182 mg/L KEW0.0100 113 09/28/15 16:50 10/01/15 19:21Chromium SW7470A MWL<0.00020 mg/L 0.00020 113 09/30/15 12:45 10/01/15 12:03Mercury SW6010C 0.0745 mg/L KEW0.0100 113 09/28/15 16:50 10/05/15 15:40Lead SW6010C <0.0500 mg/L KEW0.0500 113 09/28/15 16:50 10/01/15 19:21Selenium Volatile Organic Compounds by GC Cl SW8021B CL<5.00 ug/L 5.00 113 10/01/15 05:07 10/01/15 05:07Methyl-t-butyl ether (MTBE) SW8021B CL<1.00 ug/L 1.00 113 10/01/15 05:07 10/01/15 05:07Benzene SW8021B CL<1.00 ug/L 1.00 113 10/01/15 05:07 10/01/15 05:07Toluene SW8021B CL<1.00 ug/L 1.00 113 10/01/15 05:07 10/01/15 05:07Ethylbenzene SW8021B CL<4.00 ug/L 4.00 113 10/01/15 05:07 10/01/15 05:07m+p-Xylenes SW8021B CL<2.00 ug/L 2.00 113 10/01/15 05:07 10/01/15 05:07o-Xylene SW8021B CL<6.00 ug/L 6.00 113 10/01/15 05:07 10/01/15 05:07Xylenes, Total SW8021B <6.00 ug/L CL6.00 113 10/01/15 05:07 10/01/15 05:07Naphthalene 80-12092.0 %Surr: 2,5-Dibromotoluene CL13SW8021B10/01/15 05:07 10/01/15 05:07 Volatile Hydrocarbons by GC Cl SW8015C CL<0.10 mg/L 0.10 113 10/01/15 05:07 10/01/15 05:07TPH-Volatiles (GRO) Semivolatile Hydrocarbons by GC SW8015C JHV<0.50 mg/L 0.50 113 09/30/15 14:23 10/02/15 02:28TPH-Semi-Volatiles (DRO) 40-16075.4 %Surr: Pentacosane JHV13SW8015C09/30/15 14:23 10/02/15 02:28 Page 15 of 36Page 15 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report ResultParameter Reporting LimitMethodQual Analyst Analysis Date/Time Trip Blank 09/15/2015 15:30 Analytical Results Laboratory Sample ID:Sample I.D. Date/Time Sampled: D.F. Samp ID 15I0632-14 Sample Prep Date/Time Volatile Organic Compounds by GC SW8021B CL<5.00 ug/L 5.00 114 09/30/15 14:24 09/30/15 14:24Methyl-t-butyl ether (MTBE) SW8021B CL<1.00 ug/L 1.00 114 09/30/15 14:24 09/30/15 14:24Benzene SW8021B CL<1.00 ug/L 1.00 114 09/30/15 14:24 09/30/15 14:24Toluene SW8021B CL<1.00 ug/L 1.00 114 09/30/15 14:24 09/30/15 14:24Ethylbenzene SW8021B CL<4.00 ug/L 4.00 114 09/30/15 14:24 09/30/15 14:24m+p-Xylenes SW8021B CL<2.00 ug/L 2.00 114 09/30/15 14:24 09/30/15 14:24o-Xylene SW8021B CL<6.00 ug/L 6.00 114 09/30/15 14:24 09/30/15 14:24Xylenes, Total SW8021B <6.00 ug/L CL6.00 114 09/30/15 14:24 09/30/15 14:24Naphthalene 80-12086.1 %Surr: 2,5-Dibromotoluene CL14SW8021B09/30/15 14:24 09/30/15 14:24 Volatile Hydrocarbons by GC SW8015C CL<0.10 mg/L 0.10 114 09/30/15 14:24 09/30/15 14:24TPH-Volatiles (GRO) Page 16 of 36Page 16 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Analytical Summary Sample ID Preparation Factors Initial / Final Sequence ID Calibration IDBatch IDMethod EPA200.2/R2.8Preparation Method:Metals (Total) by EPA 6000/7000 Series Methods 15I0632-08 BYI0624 SYJ0055SW6010C AJ5000450.0 mL / 50.0 mL 15I0632-08 BYI0624 SYJ0120SW6010C AJ5001250.0 mL / 50.0 mL 15I0632-09 BYI0624 SYJ0055SW6010C AJ5000450.0 mL / 50.0 mL 15I0632-09 BYI0624 SYJ0120SW6010C AJ5001250.0 mL / 50.0 mL 15I0632-10 BYI0624 SYJ0055SW6010C AJ5000450.0 mL / 50.0 mL 15I0632-10 BYI0624 SYJ0120SW6010C AJ5001250.0 mL / 50.0 mL 15I0632-11 BYI0624 SYJ0055SW6010C AJ5000450.0 mL / 50.0 mL 15I0632-11 BYI0624 SYJ0120SW6010C AJ5001250.0 mL / 50.0 mL 15I0632-12 BYI0624 SYJ0055SW6010C AJ5000450.0 mL / 50.0 mL 15I0632-12 BYI0624 SYJ0120SW6010C AJ5001250.0 mL / 50.0 mL 15I0632-13 BYI0624 SYJ0055SW6010C AJ5000450.0 mL / 50.0 mL 15I0632-13 BYI0624 SYJ0120SW6010C AJ5001250.0 mL / 50.0 mL Sample ID Preparation Factors Initial / Final Sequence ID Calibration IDBatch IDMethod SW3050BPreparation Method:Metals (Total) by EPA 6000/7000 Series Methods 15I0632-01 BYI0660 SYJ0096SW6010C AJ500121.05 g / 50.0 mL 15I0632-02 BYI0660 SYJ0096SW6010C AJ500121.01 g / 50.0 mL 15I0632-03 BYI0660 SYJ0096SW6010C AJ500121.06 g / 50.0 mL 15I0632-04 BYI0660 SYJ0096SW6010C AJ500121.01 g / 50.0 mL 15I0632-05 BYI0660 SYJ0096SW6010C AJ500121.04 g / 50.0 mL 15I0632-06 BYI0660 SYJ0096SW6010C AJ500121.01 g / 50.0 mL Sample ID Preparation Factors Initial / Final Sequence ID Calibration IDBatch IDMethod SW5030BPreparation Method:Volatile Hydrocarbons by GC 15I0632-01 BYI0669 SYI0812SW8015C AI500765.11 g / 5.00 mL 15I0632-02 BYI0669 SYI0812SW8015C AI500765.22 g / 5.00 mL 15I0632-03 BYI0669 SYI0812SW8015C AI500761.22 g / 5.00 mL 15I0632-04 BYI0669 SYI0812SW8015C AI500765.20 g / 5.00 mL 15I0632-05 BYI0669 SYI0812SW8015C AI500765.01 g / 5.00 mL 15I0632-06 BYI0669 SYI0812SW8015C AI500765.13 g / 5.00 mL 15I0632-01 BYI0669 SYI0812SW8021B AI500765.11 g / 5.00 mL Page 17 of 36Page 17 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Sample ID Preparation Factors Initial / Final Sequence ID Calibration IDBatch IDMethod SW5030BPreparation Method:Volatile Organic Compounds by GC 15I0632-02 BYI0669 SYI0812SW8021B AI500765.22 g / 5.00 mL 15I0632-03 BYI0669 SYI0812SW8021B AI500761.22 g / 5.00 mL 15I0632-04 BYI0669 SYI0812SW8021B AI500765.20 g / 5.00 mL 15I0632-05 BYI0669 SYI0812SW8021B AI500765.01 g / 5.00 mL 15I0632-06 BYI0669 SYI0812SW8021B AI500765.13 g / 5.00 mL 15I0632-07 BYI0676 SYI0809SW8015C AI500765.00 mL / 5.00 mL 15I0632-08 BYI0676 SYI0809SW8015C AI500765.00 mL / 5.00 mL 15I0632-09 BYI0676 SYI0809SW8015C AI500765.00 mL / 5.00 mL 15I0632-10 BYI0676 SYI0809SW8015C AI500765.00 mL / 5.00 mL 15I0632-11 BYI0676 SYI0809SW8015C AI500765.00 mL / 5.00 mL 15I0632-12 BYI0676 SYI0809SW8015C AI500765.00 mL / 5.00 mL 15I0632-13 BYI0676 SYI0809SW8015C AI500765.00 mL / 5.00 mL 15I0632-14 BYI0676 SYI0809SW8015C AI500765.00 mL / 5.00 mL 15I0632-07 BYI0676 SYI0809SW8021B AI500765.00 mL / 5.00 mL 15I0632-08 BYI0676 SYI0809SW8021B AI500765.00 mL / 5.00 mL 15I0632-09 BYI0676 SYI0809SW8021B AI500765.00 mL / 5.00 mL 15I0632-10 BYI0676 SYI0809SW8021B AI500765.00 mL / 5.00 mL 15I0632-11 BYI0676 SYI0809SW8021B AI500765.00 mL / 5.00 mL 15I0632-12 BYI0676 SYI0809SW8021B AI500765.00 mL / 5.00 mL 15I0632-13 BYI0676 SYI0809SW8021B AI500765.00 mL / 5.00 mL 15I0632-14 BYI0676 SYI0809SW8021B AI500765.00 mL / 5.00 mL Sample ID Preparation Factors Initial / Final Sequence ID Calibration IDBatch IDMethod SW7470APreparation Method:Metals (Total) by EPA 6000/7000 Series Methods 15I0632-08 BYJ0006 SYJ0015SW7470A AJ5000120.0 mL / 20.0 mL 15I0632-09 BYJ0006 SYJ0015SW7470A AJ5000120.0 mL / 20.0 mL 15I0632-10 BYJ0006 SYJ0015SW7470A AJ5000120.0 mL / 20.0 mL 15I0632-11 BYJ0006 SYJ0015SW7470A AJ5000120.0 mL / 20.0 mL 15I0632-12 BYJ0006 SYJ0015SW7470A AJ5000120.0 mL / 20.0 mL 15I0632-13 BYJ0006 SYJ0015SW7470A AJ5000120.0 mL / 20.0 mL Sample ID Preparation Factors Initial / Final Sequence ID Calibration IDBatch IDMethod SW7471APreparation Method:Metals (Total) by EPA 6000/7000 Series Methods 15I0632-01 BYI0645 SYI0783SW7471B AI501240.502 g / 20.0 mL Page 18 of 36Page 18 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Sample ID Preparation Factors Initial / Final Sequence ID Calibration IDBatch IDMethod SW7471APreparation Method:Metals (Total) by EPA 6000/7000 Series Methods 15I0632-02 BYI0645 SYI0783SW7471B AI501240.526 g / 20.0 mL 15I0632-03 BYI0645 SYI0783SW7471B AI501240.509 g / 20.0 mL 15I0632-04 BYI0645 SYI0783SW7471B AI501240.500 g / 20.0 mL 15I0632-05 BYI0645 SYI0783SW7471B AI501240.527 g / 20.0 mL 15I0632-06 BYI0645 SYI0783SW7471B AI501240.517 g / 20.0 mL Sample ID Preparation Factors Initial / Final Sequence ID Calibration IDBatch IDMethod SW8100Preparation Method:Semivolatile Hydrocarbons by GC 15I0632-01 BYI0665 SYJ0005SW8015C AH5015350.4 g / 1.00 mL 15I0632-02 BYI0665 SYJ0005SW8015C AH5015350.5 g / 1.00 mL 15I0632-03 BYI0665 SYJ0005SW8015C AH5015350.5 g / 1.00 mL 15I0632-04 BYI0665 SYJ0005SW8015C AH5015350.7 g / 1.00 mL 15I0632-05 BYI0665 SYJ0005SW8015C AH5015352.1 g / 1.00 mL 15I0632-06 BYI0665 SYJ0005SW8015C AH5015351.6 g / 1.00 mL 15I0632-08 BYI0670 SYJ0007SW8015C AA500371000 mL / 1.00 mL 15I0632-09 BYI0670 SYJ0007SW8015C AA50037910 mL / 1.00 mL 15I0632-10 BYI0670 SYJ0007SW8015C AA50037830 mL / 1.00 mL 15I0632-11 BYI0675 SYJ0064SW8015C AA50037940 mL / 1.00 mL 15I0632-12 BYI0675 SYJ0064SW8015C AA50037940 mL / 1.00 mL 15I0632-13 BYI0675 SYJ0064SW8015C AA50037620 mL / 1.00 mL Page 19 of 36Page 19 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Qual Analyte Metals (Total) by EPA 6000/7000 Series Methods - Quality Control Air Water and Soil Laboratories, Inc. Batch BYI0624 - EPA200.2/R2.8 Blank (BYI0624-BLK1)Prepared: 09/28/2015 Analyzed: 09/29/2015 0.0100 mg/L<0.0100 mg/LArsenic 0.0100 mg/L<0.0100 mg/LBarium 0.0050 mg/L<0.0050 mg/LCadmium 0.0100 mg/L<0.0100 mg/LChromium 0.0100 mg/L<0.0100 mg/LLead 0.0500 mg/L<0.0500 mg/LSelenium 0.0100 mg/L<0.0100 mg/LSilver Blank (BYI0624-BLK2)Prepared: 09/28/2015 Analyzed: 10/01/2015 0.0100 mg/L<0.0100 mg/LArsenic 0.0100 mg/L<0.0100 mg/LBarium 0.0050 mg/L<0.0050 mg/LCadmium 0.0100 mg/L<0.0100 mg/LChromium 0.0100 mg/L<0.0100 mg/LLead 0.0500 mg/L<0.0500 mg/LSelenium 0.0100 mg/L<0.0100 mg/LSilver LCS (BYI0624-BS1)Prepared: 09/28/2015 Analyzed: 09/29/2015 0.0100 0.500 80-12094.1mg/L0.471 mg/LArsenic 0.0100 0.500 80-120101mg/L0.507 mg/LBarium 0.0050 0.500 80-12098.3mg/L0.491 mg/LCadmium 0.0100 0.500 80-12099.5mg/L0.498 mg/LChromium 0.0100 0.500 80-12098.4mg/L0.492 mg/LLead 0.0500 0.500 80-12096.7mg/L0.483 mg/LSelenium 0.0100 0.100 80-120103mg/L0.103 mg/LSilver LCS (BYI0624-BS2)Prepared: 09/28/2015 Analyzed: 10/01/2015 0.0100 0.500 80-12089.8mg/L0.449 mg/LArsenic 0.0100 0.500 80-12094.3mg/L0.472 mg/LBarium 0.0050 0.500 80-12095.4mg/L0.477 mg/LCadmium 0.0100 0.500 80-12095.9mg/L0.480 mg/LChromium 0.0100 0.500 80-12091.1mg/L0.455 mg/LLead 0.0500 0.500 80-12097.3mg/L0.487 mg/LSelenium Page 20 of 36Page 20 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Qual Analyte Metals (Total) by EPA 6000/7000 Series Methods - Quality Control Air Water and Soil Laboratories, Inc. Batch BYI0624 - EPA200.2/R2.8 LCS (BYI0624-BS2)Prepared: 09/28/2015 Analyzed: 10/01/2015 0.0100 0.100 80-12097.2mg/L0.0972 mg/LSilver LCS Dup (BYI0624-BSD1)Prepared: 09/28/2015 Analyzed: 09/29/2015 0.0100 0.500 2080-12094.3 0.190mg/L0.471 mg/LArsenic 0.0100 0.500 2080-120101 0.131mg/L0.506 mg/LBarium 0.0050 0.500 2080-12097.8 0.502mg/L0.489 mg/LCadmium 0.0100 0.500 2080-12099.2 0.354mg/L0.496 mg/LChromium 0.0100 0.500 2080-12099.0 0.649mg/L0.495 mg/LLead 0.0500 0.500 2080-12097.5 0.886mg/L0.488 mg/LSelenium 0.0100 0.100 2080-120104 1.06mg/L0.104 mg/LSilver LCS Dup (BYI0624-BSD2)Prepared: 09/28/2015 Analyzed: 10/01/2015 0.0100 0.500 2080-12090.1 0.317mg/L0.450 mg/LArsenic 0.0100 0.500 2080-12094.2 0.0956mg/L0.471 mg/LBarium 0.0050 0.500 2080-12095.3 0.125mg/L0.476 mg/LCadmium 0.0100 0.500 2080-12095.9 0.0695mg/L0.479 mg/LChromium 0.0100 0.500 2080-12091.7 0.662mg/L0.458 mg/LLead 0.0500 0.500 2080-12097.8 0.462mg/L0.489 mg/LSelenium 0.0100 0.100 2080-12097.8 0.585mg/L0.0978 mg/LSilver Matrix Spike (BYI0624-MS1)Prepared: 09/28/2015 Analyzed: 09/29/2015Source: 15I0617-04 0.0100 0.500 75-125101mg/L0.503 mg/L <0.0100 mg/LArsenic 0.0100 0.500 75-125103mg/L0.567 mg/L 0.0504 mg/LBarium 0.0050 0.500 75-125102mg/L0.511 mg/L <0.0050 mg/LCadmium 0.0100 0.500 75-125103mg/L0.532 mg/L 0.0191 mg/LChromium 0.0100 0.500 75-125102mg/L0.510 mg/L <0.0100 mg/LLead 0.0500 0.500 75-125104mg/L0.518 mg/L <0.0500 mg/LSelenium 0.0100 0.100 75-125103mg/L0.111 mg/L <0.0100 mg/LSilver Page 21 of 36Page 21 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Qual Analyte Metals (Total) by EPA 6000/7000 Series Methods - Quality Control Air Water and Soil Laboratories, Inc. Batch BYI0624 - EPA200.2/R2.8 Matrix Spike (BYI0624-MS2)Prepared: 09/28/2015 Analyzed: 09/29/2015Source: 15I0621-01 0.0100 0.500 75-125100mg/L0.500 mg/L <0.0100 mg/LArsenic 0.0100 0.500 75-125103mg/L0.530 mg/L 0.0168 mg/LBarium 0.0050 0.500 75-125100mg/L0.501 mg/L <0.0050 mg/LCadmium 0.0100 0.500 75-125101mg/L0.507 mg/L <0.0100 mg/LChromium 0.0100 0.500 75-12599.9mg/L0.500 mg/L <0.0100 mg/LLead 0.0500 0.500 75-125103mg/L0.516 mg/L <0.0500 mg/LSelenium 0.0100 0.100 75-125104mg/L0.104 mg/L <0.0100 mg/LSilver Matrix Spike (BYI0624-MS3)Prepared: 09/28/2015 Analyzed: 10/01/2015Source: 15I0617-04 0.0100 0.500 75-12593.0mg/L0.465 mg/L <0.0100 mg/LArsenic 0.0100 0.500 75-12593.6mg/L0.518 mg/L 0.0504 mg/LBarium 0.0050 0.500 75-12596.0mg/L0.480 mg/L <0.0050 mg/LCadmium 0.0100 0.500 75-12597.0mg/L0.504 mg/L 0.0191 mg/LChromium 0.0100 0.500 75-12591.5mg/L0.457 mg/L <0.0100 mg/LLead 0.0500 0.500 75-125101mg/L0.504 mg/L <0.0500 mg/LSelenium 0.0100 0.100 75-12597.6mg/L0.105 mg/L <0.0100 mg/LSilver Matrix Spike (BYI0624-MS4)Prepared: 09/28/2015 Analyzed: 10/01/2015Source: 15I0621-01 0.0100 0.500 75-12593.4mg/L0.467 mg/L <0.0100 mg/LArsenic 0.0100 0.500 75-12593.8mg/L0.486 mg/L 0.0168 mg/LBarium 0.0050 0.500 75-12595.4mg/L0.477 mg/L <0.0050 mg/LCadmium 0.0100 0.500 75-12596.7mg/L0.483 mg/L <0.0100 mg/LChromium 0.0100 0.500 75-12591.1mg/L0.455 mg/L <0.0100 mg/LLead 0.0500 0.500 75-125101mg/L0.503 mg/L <0.0500 mg/LSelenium 0.0100 0.100 75-12598.8mg/L0.0988 mg/L <0.0100 mg/LSilver Matrix Spike Dup (BYI0624-MSD1)Prepared: 09/28/2015 Analyzed: 09/29/2015Source: 15I0617-04 0.0100 0.500 2075-125mg/L<0.0100 mg/L <0.0100 mg/LArsenic M 0.0100 0.500 2075-125-10.1mg/L<0.0100 mg/L 0.0504 mg/LBarium M 0.0050 0.500 2075-125mg/L<0.0050 mg/L <0.0050 mg/LCadmium M 0.0100 0.500 2075-125-3.82mg/L<0.0100 mg/L 0.0191 mg/LChromium M 0.0100 0.500 2075-125mg/L<0.0100 mg/L <0.0100 mg/LLead M 0.0500 0.500 2075-125mg/L<0.0500 mg/L <0.0500 mg/LSelenium M Page 22 of 36Page 22 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Qual Analyte Metals (Total) by EPA 6000/7000 Series Methods - Quality Control Air Water and Soil Laboratories, Inc. Batch BYI0624 - EPA200.2/R2.8 Matrix Spike Dup (BYI0624-MSD1)Prepared: 09/28/2015 Analyzed: 09/29/2015Source: 15I0617-04 0.0100 0.100 2075-125-7.31mg/L<0.0100 mg/L <0.0100 mg/LSilver M Matrix Spike Dup (BYI0624-MSD2)Prepared: 09/28/2015 Analyzed: 09/29/2015Source: 15I0621-01 0.0100 0.500 2075-125100 0.255mg/L0.501 mg/L <0.0100 mg/LArsenic 0.0100 0.500 2075-125102 0.707mg/L0.526 mg/L 0.0168 mg/LBarium 0.0050 0.500 2075-125100 0.189mg/L0.500 mg/L <0.0050 mg/LCadmium 0.0100 0.500 2075-125102 0.170mg/L0.508 mg/L <0.0100 mg/LChromium 0.0100 0.500 2075-125100 0.165mg/L0.500 mg/L <0.0100 mg/LLead 0.0500 0.500 2075-125103 0.416mg/L0.514 mg/L <0.0500 mg/LSelenium 0.0100 0.100 2075-125104 0.518mg/L0.104 mg/L <0.0100 mg/LSilver Matrix Spike Dup (BYI0624-MSD3)Prepared: 09/28/2015 Analyzed: 10/01/2015Source: 15I0617-04 0.0100 0.500 2075-12593.3 0.294mg/L0.466 mg/L <0.0100 mg/LArsenic 0.0100 0.500 2075-12593.4 0.204mg/L0.517 mg/L 0.0504 mg/LBarium 0.0050 0.500 2075-12595.8 0.256mg/L0.479 mg/L <0.0050 mg/LCadmium 0.0100 0.500 2075-12596.9 0.160mg/L0.503 mg/L 0.0191 mg/LChromium 0.0100 0.500 2075-12591.3 0.121mg/L0.457 mg/L <0.0100 mg/LLead 0.0500 0.500 2075-125100 0.762mg/L0.500 mg/L <0.0500 mg/LSelenium 0.0100 0.100 2075-12597.3 0.274mg/L0.105 mg/L <0.0100 mg/LSilver Matrix Spike Dup (BYI0624-MSD4)Prepared: 09/28/2015 Analyzed: 10/01/2015Source: 15I0621-01 0.0100 0.500 2075-12594.0 0.657mg/L0.470 mg/L <0.0100 mg/LArsenic 0.0100 0.500 2075-12593.8 0.00657mg/L0.486 mg/L 0.0168 mg/LBarium 0.0050 0.500 2075-12596.2 0.853mg/L0.481 mg/L <0.0050 mg/LCadmium 0.0100 0.500 2075-12597.4 0.784mg/L0.487 mg/L <0.0100 mg/LChromium 0.0100 0.500 2075-12591.7 0.654mg/L0.458 mg/L <0.0100 mg/LLead 0.0500 0.500 2075-125101 0.934mg/L0.507 mg/L <0.0500 mg/LSelenium 0.0100 0.100 2075-12598.5 0.274mg/L0.0985 mg/L <0.0100 mg/LSilver Page 23 of 36Page 23 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Qual Analyte Metals (Total) by EPA 6000/7000 Series Methods - Quality Control Air Water and Soil Laboratories, Inc. Batch BYI0645 - SW7471A Blank (BYI0645-BLK1)Prepared & Analyzed: 09/29/2015 0.008 mg/kg<0.008 mg/kgMercury LCS (BYI0645-BS1)Prepared & Analyzed: 09/29/2015 0.008 0.0980 80-12094.4mg/kg0.093 mg/kgMercury LCS Dup (BYI0645-BSD1)Prepared & Analyzed: 09/29/2015 0.008 0.0951 2080-12094.1 3.40mg/kg0.089 mg/kgMercury Matrix Spike (BYI0645-MS1)Prepared & Analyzed: 09/29/2015Source: 15I0632-01 0.008 0.0952 80-12090.6mg/kg0.086 mg/kg <0.008 mg/kgMercury Matrix Spike Dup (BYI0645-MSD1)Prepared & Analyzed: 09/29/2015Source: 15I0632-01 0.008 0.0982 2080-120106 18.5mg/kg0.104 mg/kg <0.008 mg/kgMercury Batch BYJ0006 - SW7470A Blank (BYJ0006-BLK1)Prepared & Analyzed: 10/01/2015 0.00020 mg/L<0.00020 mg/LMercury LCS (BYJ0006-BS1)Prepared & Analyzed: 10/01/2015 0.00020 0.00250 80-120103mg/L0.00257 mg/LMercury LCS Dup (BYJ0006-BSD1)Prepared & Analyzed: 10/01/2015 0.00020 0.00250 2080-120103 0.117mg/L0.00256 mg/LMercury Matrix Spike (BYJ0006-MS1)Prepared & Analyzed: 10/01/2015Source: 15I0632-11 0.00020 0.00250 80-12099.4mg/L0.00248 mg/L <0.00020 mg/LMercury Page 24 of 36Page 24 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Qual Analyte Metals (Total) by EPA 6000/7000 Series Methods - Quality Control Air Water and Soil Laboratories, Inc. Batch BYJ0006 - SW7470A Matrix Spike Dup (BYJ0006-MSD1)Prepared & Analyzed: 10/01/2015Source: 15I0632-11 0.00020 0.00250 2080-12099.9 0.503mg/L0.00250 mg/L <0.00020 mg/LMercury Page 25 of 36Page 25 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Qual Analyte Volatile Organic Compounds by GC - Quality Control Air Water and Soil Laboratories, Inc. Batch BYI0669 - SW5030B Blank (BYI0669-BLK1)Prepared & Analyzed: 09/30/2015 5.00 ug/kg<5.00 ug/kgMethyl-t-butyl ether (MTBE) 5.00 ug/kg<5.00 ug/kgBenzene 5.00 ug/kg<5.00 ug/kgToluene 5.00 ug/kg<5.00 ug/kgEthylbenzene 10.0 ug/kg<10.0 ug/kgm+p-Xylenes 5.00 ug/kg<5.00 ug/kgo-Xylene 15.0 ug/kg<15.0 ug/kgXylenes, Total 5.00 ug/kg<5.00 ug/kgNaphthalene 100 80-120Surr: 2,5-Dibromotoluene 89.489.4 ug/L LCS (BYI0669-BS1)Prepared & Analyzed: 09/30/2015 5.00 99.0 70-13098.1ug/kg97.1 ug/kgMethyl-t-butyl ether (MTBE) 5.00 99.0 70-13098.7ug/kg97.8 ug/kgBenzene 5.00 99.0 70-130104ug/kg103 ug/kgToluene 5.00 99.0 70-130103ug/kg102 ug/kgEthylbenzene 10.0 198 70-130105ug/kg208 ug/kgm+p-Xylenes 5.00 99.0 70-130112ug/kg111 ug/kgo-Xylene 15.0 0-200ug/kg319 ug/kgXylenes, Total 5.00 99.0 70-130108ug/kg107 ug/kgNaphthalene 100 80-120Surr: 2,5-Dibromotoluene 90.990.9 ug/L LCS Dup (BYI0669-BSD1)Prepared & Analyzed: 09/30/2015 5.00 100 2070-13096.2 0.929ug/kg96.2 ug/kgMethyl-t-butyl ether (MTBE) 5.00 100 2070-13098.1 0.294ug/kg98.1 ug/kgBenzene 5.00 100 2070-130103 0.327ug/kg103 ug/kgToluene 5.00 100 2070-130102 0.0971ug/kg102 ug/kgEthylbenzene 10.0 200 2070-130104 0.460ug/kg207 ug/kgm+p-Xylenes 5.00 100 2070-130111 0.289ug/kg111 ug/kgo-Xylene 15.0 200-200 0.401ug/kg318 ug/kgXylenes, Total 5.00 100 2070-130103 3.52ug/kg103 ug/kgNaphthalene 100 80-120Surr: 2,5-Dibromotoluene 93.593.5 ug/L Page 26 of 36Page 26 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Qual Analyte Volatile Organic Compounds by GC - Quality Control Air Water and Soil Laboratories, Inc. Batch BYI0669 - SW5030B Matrix Spike (BYI0669-MS1)Prepared & Analyzed: 09/30/2015Source: 15I0632-02 5.00 99.0 70-130101ug/kg100 ug/kg <5.00 ug/kgMethyl-t-butyl ether (MTBE) 5.00 99.0 70-13097.8ug/kg96.9 ug/kg <5.00 ug/kgBenzene 5.00 99.0 70-130102ug/kg101 ug/kg <5.00 ug/kgToluene 5.00 99.0 70-130101ug/kg99.8 ug/kg <5.00 ug/kgEthylbenzene 10.0 198 70-130103ug/kg205 ug/kg <10.0 ug/kgm+p-Xylenes 5.00 99.0 70-130111ug/kg110 ug/kg <5.00 ug/kgo-Xylene 15.0 70-130ug/kg314 ug/kg <15.0 ug/kgXylenes, Total 5.00 99.0 70-130107ug/kg106 ug/kg <5.00 ug/kgNaphthalene 100 80-120Surr: 2,5-Dibromotoluene 100100ug/L Matrix Spike Dup (BYI0669-MSD1)Prepared & Analyzed: 09/30/2015Source: 15I0632-02 5.00 98.6 2070-13062.0 48.5ug/kg61.1 ug/kg <5.00 ug/kgMethyl-t-butyl ether (MTBE)M, P 5.00 98.6 2070-13065.4 40.2ug/kg64.5 ug/kg <5.00 ug/kgBenzene M, P 5.00 98.6 2070-13069.3 38.9ug/kg68.3 ug/kg <5.00 ug/kgToluene M, P 5.00 98.6 2070-13068.6 38.5ug/kg67.6 ug/kg <5.00 ug/kgEthylbenzene M, P 10.0 197 2070-13070.4 38.3ug/kg139 ug/kg <10.0 ug/kgm+p-Xylenes P 5.00 98.6 2070-13074.6 39.4ug/kg73.5 ug/kg <5.00 ug/kgo-Xylene P 15.0 2070-130 38.7ug/kg212 ug/kg <15.0 ug/kgXylenes, Total M 5.00 98.6 2070-13067.8 45.6ug/kg66.9 ug/kg <5.00 ug/kgNaphthalene M, P 100 80-120Surr: 2,5-Dibromotoluene 96.096.0 ug/L Batch BYI0676 - SW5030B Blank (BYI0676-BLK1)Prepared & Analyzed: 09/30/2015 5.00 ug/L<5.00 ug/LMethyl-t-butyl ether (MTBE) 1.00 ug/L<1.00 ug/LBenzene 1.00 ug/L<1.00 ug/LToluene 1.00 ug/L<1.00 ug/LEthylbenzene 4.00 ug/L<4.00 ug/Lm+p-Xylenes 2.00 ug/L<2.00 ug/Lo-Xylene 6.00 ug/L<6.00 ug/LXylenes, Total Page 27 of 36Page 27 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Qual Analyte Volatile Organic Compounds by GC - Quality Control Air Water and Soil Laboratories, Inc. Batch BYI0676 - SW5030B Blank (BYI0676-BLK1)Prepared & Analyzed: 09/30/2015 6.00 ug/L<6.00 ug/LNaphthalene J 100 80-120Surr: 2,5-Dibromotoluene 85.985.9 ug/L LCS (BYI0676-BS1)Prepared & Analyzed: 09/30/2015 5.00 100 70-13092.8ug/L92.8 ug/LMethyl-t-butyl ether (MTBE) 1.00 100 70-13097.1ug/L97.1 ug/LBenzene 1.00 100 70-130102ug/L102 ug/LToluene 1.00 100 70-130102ug/L102 ug/LEthylbenzene 4.00 200 70-130104ug/L209 ug/Lm+p-Xylenes 2.00 100 70-130111ug/L111 ug/Lo-Xylene 6.00 0-200ug/L319 ug/LXylenes, Total 6.00 100 70-13097.8ug/L97.8 ug/LNaphthalene 100 80-120Surr: 2,5-Dibromotoluene 87.287.2 ug/L LCS Dup (BYI0676-BSD1)Prepared & Analyzed: 09/30/2015 5.00 100 2070-13095.6 2.94ug/L95.6 ug/LMethyl-t-butyl ether (MTBE) 1.00 100 2070-13098.6 1.47ug/L98.6 ug/LBenzene 1.00 100 2070-130104 1.04ug/L104 ug/LToluene 1.00 100 2070-130103 0.890ug/L103 ug/LEthylbenzene 4.00 200 2070-130105 0.678ug/L210 ug/Lm+p-Xylenes 2.00 100 2070-130112 0.765ug/L112 ug/Lo-Xylene 6.00 200-200 0.708ug/L322 ug/LXylenes, Total 6.00 100 2070-130103 5.01ug/L103 ug/LNaphthalene 100 80-120Surr: 2,5-Dibromotoluene 90.990.9 ug/L Duplicate (BYI0676-DUP1)Prepared & Analyzed: 10/01/2015Source: 15I0615-01 5.00 30NAug/L<5.00 ug/L <5.00 ug/LMethyl-t-butyl ether (MTBE)J 1.00 30NAug/L<1.00 ug/L <1.00 ug/LBenzene 1.00 30NAug/L<1.00 ug/L <1.00 ug/LToluene 1.00 30NAug/L<1.00 ug/L <1.00 ug/LEthylbenzene 4.00 30NAug/L<4.00 ug/L <4.00 ug/Lm+p-Xylenes 2.00 30NAug/L<2.00 ug/L <2.00 ug/Lo-Xylene Page 28 of 36Page 28 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Qual Analyte Volatile Organic Compounds by GC - Quality Control Air Water and Soil Laboratories, Inc. Batch BYI0676 - SW5030B Duplicate (BYI0676-DUP1)Prepared & Analyzed: 10/01/2015Source: 15I0615-01 6.00 30NAug/L<6.00 ug/L <6.00 ug/LXylenes, Total 6.00 30NAug/L<6.00 ug/L <6.00 ug/LNaphthalene J 100 80-120Surr: 2,5-Dibromotoluene 97.497.4 ug/L Matrix Spike (BYI0676-MS1)Prepared & Analyzed: 09/30/2015Source: 15I0591-13RE1 5.00 100 70-13095.7ug/L95.7 ug/L <5.00 ug/LMethyl-t-butyl ether (MTBE) 1.00 100 70-13099.1ug/L100 ug/L 1.34 ug/LBenzene 1.00 100 70-130104ug/L104 ug/L <1.00 ug/LToluene 1.00 100 70-130103ug/L103 ug/L <1.00 ug/LEthylbenzene 4.00 200 70-130104ug/L210 ug/L <4.00 ug/Lm+p-Xylenes 2.00 100 70-130112ug/L112 ug/L <2.00 ug/Lo-Xylene 6.00 70-130ug/L321 ug/L <6.00 ug/LXylenes, Total 6.00 100 70-130104ug/L111 ug/L 6.29 ug/LNaphthalene 100 80-120Surr: 2,5-Dibromotoluene 97.697.6 ug/L Matrix Spike Dup (BYI0676-MSD1)Prepared & Analyzed: 09/30/2015Source: 15I0591-13RE1 5.00 100 2070-13096.9 1.23ug/L96.9 ug/L <5.00 ug/LMethyl-t-butyl ether (MTBE) 1.00 100 2070-13098.9 0.249ug/L100 ug/L 1.34 ug/LBenzene 1.00 100 2070-130103 0.702ug/L104 ug/L <1.00 ug/LToluene 1.00 100 2070-130102 0.710ug/L102 ug/L <1.00 ug/LEthylbenzene 4.00 200 2070-130104 0.550ug/L208 ug/L <4.00 ug/Lm+p-Xylenes 2.00 100 2070-130111 0.475ug/L111 ug/L <2.00 ug/Lo-Xylene 6.00 2070-130 0.524ug/L320 ug/L <6.00 ug/LXylenes, Total 6.00 100 2070-130110 5.05ug/L116 ug/L 6.29 ug/LNaphthalene 100 80-120Surr: 2,5-Dibromotoluene 97.097.0 ug/L Page 29 of 36Page 29 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Qual Analyte Volatile Hydrocarbons by GC - Quality Control Air Water and Soil Laboratories, Inc. Batch BYI0669 - SW5030B Blank (BYI0669-BLK1)Prepared & Analyzed: 09/30/2015 0.10 mg/kg<0.10 mg/kgTPH-Volatiles (GRO) LCS (BYI0669-BS1)Prepared & Analyzed: 09/30/2015 0.10 0.990 70-130111mg/kg1.10 mg/kgTPH-Volatiles (GRO) LCS Dup (BYI0669-BSD1)Prepared & Analyzed: 09/30/2015 0.10 1.00 2070-130110 0.256mg/kg1.10 mg/kgTPH-Volatiles (GRO) Matrix Spike (BYI0669-MS1)Prepared & Analyzed: 09/30/2015Source: 15I0632-02 0.10 0.990 70-130108mg/kg1.07 mg/kg <0.10 mg/kgTPH-Volatiles (GRO) Matrix Spike Dup (BYI0669-MSD1)Prepared & Analyzed: 09/30/2015Source: 15I0632-02 0.10 0.986 2070-13072.2 40.5mg/kg0.71 mg/kg <0.10 mg/kgTPH-Volatiles (GRO)M Batch BYI0676 - SW5030B Blank (BYI0676-BLK1)Prepared & Analyzed: 09/30/2015 0.10 mg/L<0.10 mg/LTPH-Volatiles (GRO) LCS (BYI0676-BS1)Prepared & Analyzed: 09/30/2015 0.10 1.00 70-130110mg/L1.10 mg/LTPH-Volatiles (GRO) LCS Dup (BYI0676-BSD1)Prepared & Analyzed: 09/30/2015 0.10 1.00 2070-130111 0.910mg/L1.11 mg/LTPH-Volatiles (GRO) Duplicate (BYI0676-DUP1)Prepared & Analyzed: 10/01/2015Source: 15I0615-01 0.10 20NAmg/L<0.10 mg/L <0.10 mg/LTPH-Volatiles (GRO) Page 30 of 36Page 30 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Qual Analyte Volatile Hydrocarbons by GC - Quality Control Air Water and Soil Laboratories, Inc. Batch BYI0676 - SW5030B Matrix Spike (BYI0676-MS1)Prepared & Analyzed: 09/30/2015Source: 15I0591-13RE1 0.10 1.00 70-130114mg/L1.89 mg/L 0.74 mg/LTPH-Volatiles (GRO) Matrix Spike Dup (BYI0676-MSD1)Prepared & Analyzed: 09/30/2015Source: 15I0591-13RE1 0.10 1.00 2070-130115 0.279mg/L1.89 mg/L 0.74 mg/LTPH-Volatiles (GRO) Page 31 of 36Page 31 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Qual Analyte Semivolatile Hydrocarbons by GC - Quality Control Air Water and Soil Laboratories, Inc. Batch BYI0665 - SW8100 Blank (BYI0665-BLK1)Prepared: 09/29/2015 Analyzed: 09/30/2015 10.0 mg/kg<10.0 mg/kgTPH-Semi-Volatiles (DRO) 4.84 40-160Surr: Pentacosane 69.93.39 mg/kg LCS (BYI0665-BS1)Prepared: 09/29/2015 Analyzed: 09/30/2015 10.0 100 40-16066.7mg/kg66.7 mg/kgTPH-Semi-Volatiles (DRO) 5.00 40-160Surr: Pentacosane 65.13.25 mg/kg Matrix Spike (BYI0665-MS1)Prepared: 09/29/2015 Analyzed: 09/30/2015Source: 15I0627-01 10.0 96.9 40-16064.5mg/kg74.6 mg/kg 12.1 mg/kgTPH-Semi-Volatiles (DRO) 4.84 40-160Surr: Pentacosane 76.13.69 mg/kg Matrix Spike Dup (BYI0665-MSD1)Prepared: 09/29/2015 Analyzed: 09/30/2015Source: 15I0627-01 10.0 98.8 2040-16069.4 7.90mg/kg80.7 mg/kg 12.1 mg/kgTPH-Semi-Volatiles (DRO) 4.94 40-160Surr: Pentacosane 1035.09 mg/kg Batch BYI0670 - SW8100 Blank (BYI0670-BLK1)Prepared & Analyzed: 09/30/2015 0.50 mg/L<0.50 mg/LTPH-Semi-Volatiles (DRO) 0.250 40-160Surr: Pentacosane 40.80.102 mg/L LCS (BYI0670-BS1)Prepared & Analyzed: 09/30/2015 0.50 5.00 40-16074.7mg/L3.7 mg/LTPH-Semi-Volatiles (DRO) 0.250 40-160Surr: Pentacosane 60.40.151 mg/L Matrix Spike (BYI0670-MS1)Prepared: 09/30/2015 Analyzed: 10/01/2015Source: 15I0645-01 0.50 5.15 40-16070.6mg/L3.6 mg/L <0.50 mg/LTPH-Semi-Volatiles (DRO) 0.258 40-160Surr: Pentacosane 70.50.182 mg/L Page 32 of 36Page 32 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Qual Analyte Semivolatile Hydrocarbons by GC - Quality Control Air Water and Soil Laboratories, Inc. Batch BYI0670 - SW8100 Matrix Spike Dup (BYI0670-MSD1)Prepared: 09/30/2015 Analyzed: 10/01/2015Source: 15I0645-01 0.50 5.05 2040-16068.0 5.88mg/L3.4 mg/L <0.50 mg/LTPH-Semi-Volatiles (DRO) 0.253 40-160Surr: Pentacosane 95.40.241 mg/L Batch BYI0675 - SW8100 Blank (BYI0675-BLK1)Prepared: 09/30/2015 Analyzed: 10/02/2015 0.50 mg/L<0.50 mg/LTPH-Semi-Volatiles (DRO) 0.250 40-160Surr: Pentacosane 75.50.189 mg/L LCS (BYI0675-BS1)Prepared: 09/30/2015 Analyzed: 10/02/2015 0.50 5.00 40-16078.9mg/L3.9 mg/LTPH-Semi-Volatiles (DRO) 0.250 40-160Surr: Pentacosane 94.20.236 mg/L Matrix Spike (BYI0675-MS1)Prepared: 09/30/2015 Analyzed: 10/02/2015Source: 15I0653-03 0.50 5.26 40-16079.5mg/L4.2 mg/L <0.50 mg/LTPH-Semi-Volatiles (DRO) 0.263 40-160Surr: Pentacosane 76.80.202 mg/L Matrix Spike Dup (BYI0675-MSD1)Prepared: 09/30/2015 Analyzed: 10/02/2015Source: 15I0653-03 0.50 5.32 2040-16032.8 82.3mg/L1.7 mg/L <0.50 mg/LTPH-Semi-Volatiles (DRO)M, P 0.266 40-160Surr: Pentacosane 18.50.0493 mg/L S Page 33 of 36Page 33 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Certified Analyses included in this Report CertificationsAnalyte SW6010C in Non-Potable Water Arsenic VELAP,NC,WVDEP Barium VELAP,NC,WVDEP Cadmium VELAP,NC,WVDEP Chromium VELAP,NC,WVDEP Lead VELAP,NC,WVDEP Selenium VELAP,NC,WVDEP Silver VELAP,NC SW6010C in Organic Arsenic VELAP Barium VELAP Silver VELAP SW7470A in Non-Potable Water Mercury VELAP,NC,WVDEP SW7471B in Solids Mercury VELAP,WVDEP SW8015C in Non-Potable Water TPH-Semi-Volatiles (DRO)VELAP,NC,WVDEP TPH-Volatiles (GRO)VELAP,NC,WVDEP SW8015C in Solids TPH-Semi-Volatiles (DRO)VELAP,NC,WVDEP TPH-Volatiles (GRO)VELAP,NC,WVDEP SW8021B in Non-Potable Water Methyl-t-butyl ether (MTBE)VELAP,NC,WVDEP Benzene VELAP,NC,WVDEP Toluene VELAP,NC,WVDEP Ethylbenzene VELAP,NC,WVDEP m+p-Xylenes VELAP,NC,WVDEP o-Xylene VELAP,NC,WVDEP Xylenes, Total VELAP,NC,WVDEP Naphthalene VELAP,NC,WVDEP SW8021B in Solids Methyl-t-butyl ether (MTBE)VELAP,NC,WVDEP Benzene VELAP,NC,WVDEP Toluene VELAP,NC,WVDEP Ethylbenzene VELAP,NC,WVDEP Page 34 of 36Page 34 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Certified Analyses included in this Report CertificationsAnalyte m+p-Xylenes VELAP,NC,WVDEP o-Xylene VELAP,NC,WVDEP Xylenes, Total VELAP,NC,WVDEP Naphthalene VELAP,NC,WVDEP Code Description Lab Number Expires 341 12/31/2015Maryland DE Drinking WaterMdDOE 495 12/31/2015North Carolina DENRNC 001 10/31/2015NELAC-PennsylvaniaPADEP 460021 06/15/2016NELAC-Virginia Certificate #8074VELAP 350 11/30/2015West Virginia DEPWVDEP Page 35 of 36Page 35 of 40 Client Site I.D.: Project Number:Submitted To: Date Issued: Groundwater Environmental Services, Inc.-R 3701 Saunders Ave. [none]Nick Braun Richmond VA, 23227 1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297 Certificate of Analysis Laboratory Order ID 15I0632 Client Name: Purchase Order: September 28, 2015 8:35Date Received: October 5, 2015 16:49 Sheetz - Hopedale and Church Rd. Final Report Summary of Data Qualifiers Cl Residual Chlorine or other oxidizing agent was detected in the container used to analyze this sample. M Matrix spike recovery is outside established acceptance limits P Duplicate analysis does not meet the acceptance criteria for precision S Surrogate recovery was outside acceptance criteria Relative Percent DifferenceRPD QualifersQual Denotes sample was re-analyzed-RE Dilution Factor. Please also see the Preparation Factor in the Analysis Summary section.D.F. TIC Tentatively Identified Compounds are compounds that are identified by comparing the analyte mass spectral pattern with the NIST spectral library. A TIC spectral match is reported when the pattern is at least 75% consistent with the published pattern. Compound concentrations are estimated and are calculated using an internal standard response factor of 1. Page 36 of 36Page 36 of 40 Page 37 of 40 Page 38 of 40 Page 39 of 40 Page 40 of 40