Item No 34 - Initial Abatement Action Report Incident 36354 -OCR

Io
ernired By
NCDENR
UST Section
INITIAL ABATEMENT ACTION REPORT
Morehead Common Site Area
1000 South Clarkson Street
Charlotte Mecklenburg County North Carolina
UST Incident No No Yet Assigned
ESP Project No E6-UD42.601
Dear Mr Schiff
On behalf of the property owner Beazer Homes ESP Associates P.A is pleased to provide the
attached Initial Abatement Action Report for the closure of the subject propertys petroleum
release ESP respectively requests classification of the release as Low Risk and issuance of no
further action notice
Thank you for your attention in this matter If you should have any questions please do not
hesitate to contact me at 803 835-0915
Sincerely
ESP Associates P.A
gar Rogers
Staff Scientist
cc Mr Jade Eastridge Beazer Homes
ard PG
Environmental Services ManagerNCLicenseNo1600
P.O Box 7030 Charlotte NC 28241
1.800.960.7317 NC 704383.4949 fax [phone] SC 8O3802.244O fax [phone]
wwwespassocjatescom
$ESP
ESP Associates P.A August 23 2007
Mooresville Regional Office
919 North Main Street
Mooresville North Carolina 28115
Attention Mr Allen Schiff
Reference
Initial Abatement Action Report
SITE ThFORMATION
Site Identification
Date of Report August 23 2007
Facility ID NA
UST Incident Number Not Yet Assigned
Site Name Morehead Common Site Area
Site Street Address 1000 South Clarkson Street
City/County/Zip Code Charlotte Mecklenburg County 28278
Description of Geographical Data Point Approximate center of UST
Location Method Mecklenburg County
Polaris GIS Map
Latitude 35.227104
Longitude -80.858606
Information about Contacts Associated with the Leaking UST System
UST Owner Beazer Homes
1300 Blvd Suite Charlotte NC 28203-4265
704.370.7200
UST Operator N/A
Property Owner Same as above
Property Occupant Same as above
Consultant/Contractor ESP Associates P.A Chris Ward PG
P0 Box 7030 Charlotte NC 28241
803.835.0915
Analytical Laboratory Prism Laboratories Inc
P0 Box 240543 Charlotte NC 28224-0403
704.529.6364
NC Certification No 402
Information about Release
Date Discovered August 2007
Estimated Quantity of Release Unknown
Cause of Release Unknown
Source of Release UST
Size and contents of UST
System from which release occurred 1300-Gallon Diesel UST
Chris Ward Professional Geologist for ESP Associates P.A do certifi that the
contained in this report is correct and accurate to the best of my knowledge
Associates P.A is licensed to practice both geology and engineering in North Carolina
Associates certification numbers are Geology C-347 and Engineering C-0587
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area August 23 2007
INTRODUCTION
The subject site location of former Duke Energy-Worth Keeter facility has an address of 1000
South Clarkson Street in Charlotte Mecklenburg County North Carolina see Figure
Topographic Site Location Map The area of the subject release associated with 1300-gallon
diesel underground storage tank UST uncovered on August 2007 has been designated by
ESP as Area of the Morehead Common site
SITE HISTORY AND CHARACTERIZATION
On August 2007 ESP responded on behalf of Beazer Homes to an encounter with UST and
impacted soil during mass grading operations at the subject site Upon arriving at the site ESP
observed 1300-gallon steel apparent diesel UST along with soils with petroleum odor located
on the west side of South Clarkson Street approximately 300 feet south of its intersection with
West Morehead Street on Tax Parcel No 07325207 see Figures and As required ESP
emailed notification of the release discovery along
with Release and UST Leak Reporting Form
to Mr Steve Bograd of the Mooresville Regional Office of NCDENR on August 2007
Release Location
The subject site is located within an urban area of Charlotte which historically included
warehouse and commercial structures The site the former location of Duke Energy-Worth
Keeter Inc was recently mass graded and is currently being developed as mixed-use
residential/commercial development see Figures and Previously documented UST
Incidents on the subject parcel include Incidents Nos 18101 9567 and 36331 Locations of
these two previously documented incidents relative to the subject release Area are depicted
on Figure
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area August 23 2007
Based on our review of the Geologic Map of North Carolina 1985 the subject site is located
within the Charlotte Belt locally comprised of intrusive metamorphosed granitic rocks locally
pinkish gray massive to weakly foliated and containing hornblende Soils encountered in this
area are the residual product of chemical weathering of rock presently underlying the site Soil
weathering is more advanced near the surface grading with depth to less weathered rock and
finally bedrock
UST Information
Following the August 2007 discovery of 1300-gallon diesel UST AD Environmental and
Industrial Services AD of High Point North Carolina was contacted to remove remaining
product/sludge from the tank following its removal from the excavation On August 2007
AD pumped 77 gallons of product/sludge from the tank for permitted recycling
at their
Archdale North Carolina facility see Product Material Manifest in Appendix Once
removed the tank was transported by AD to the Griffin recycling facility in Greensboro
North Carolina on August 2007 see Tank Disposal Manifest in Appendix See site
photographs in Appendix
PreviousTankInstallationRemovalSizeTankLastTank
No Date Date Gallons Dimensions Contents
an
Contents
Unknown 8-1-07 1300 12 ft 4.3 ft Diesel Unknown
completed UST-2 Form is included as Appendix The former location of the above UST is
depicted on Figure
Previous Reporting
ESP emailed release notification along with 24-Hour Release and UST Leak Reporting Form
to the Mooresville Regional Office of NCDENR on August 2007 see Appendix
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area August 23 2007
INITIAL ABATEMENT ACTIVITIES
Contaminated Soil Excavation
On August and 2007 ESP documented the excavation of 39.14 tons of impacted soil from
Area by the sites grading contractor Gelder Thompson of Midland North Carolina The
excavation was advanced based on
results of OVA field screening and evidence of visible
staining The resulting excavation measured approximately ft 18 ft ft deep The
excavated soil was placed on and covered with plastic awaiting subsequent off-site permitted
disposal Neither groundwater bedrock nor free product were encountered within the tank pit
See site photographs in Appendix
Post-Excavation Confirmatory Sampling
On August 2007 confirmatory soil samples were collected at depth of 3.5 feet BLS froii
each of the excavations four sides WS-1 through WS-4 while one sample was collected at
depth of feet BLS from the base of the excavation B-i The sidewall samples were collected
at the 3.5 foot depth due to the prevalence of elevated OVA readings at that depth The five soil
samples were hand delivered on ice to Prism Laboratories of Charlotte North Carolina to be
analyzed for risk-based parameters which include volatile organic compounds VOCs by EPA
Method 8260B semi-volatile organic compounds SVOCs by EPA Method 8270C VPH/EPH
by the Massachusetts Department of Environmental Protection MADEP method and for total
lead and chromium by EPA Method 60 lOB Sample locations and excavation dimensions are
depicted on Figure Soil Sample Location Map Sampling was performed in general
accordance with ESPs SOP see Appendix
Results of the laboratory analysis
of confirmatory samples WS-1 through WS-4 and B-i revealed
that all analyzed constituents were either below reporting limits BRLs or below the lowest of
the soil-to-groundwater or
residential MSCC Laboratory analytical results for the confirmatory
soil samples are summarized on Table B-i The Prism laboratory data report is included as
Appendix
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area August 23 2007
Stockpile Sampling and Soil Disposal
On August 2007 ESP collected composite stockpile soil sample for laboratory analysis
The
stockpile soil sample designated lA/lB was placed in laboratory provided containers labeled
and hand delivered on ice to Prism for compositing and subsequent analysis The sample was
analyzed for total petroleum hydrocarbons TPH for gasoline range organics GRO and diesel
range organics DRO by EPA Method 5030/3550 and for BTEX by EPA Method 8260B The
composite sample was collected and analyzed to confirm that release had occurred and to
characterize contaminant types and concentrations for subsequent off-site permitted
disposal/treatment
As revealed by the laboratory analysis
of stockpile composite soil sample 1A/1B TPH-DRO was
reported at concentration of 710 mg/Kg and TPH-GRO at concentration of 6.9 mg/Kg while
results for the remainder of analytes were BRLs Results of the stockpile sample analyses are
summarized on Table B-2 while the laboratory data report is included as Appendix
On August 16 and 17 2007 39.14 tons of stockpiled soil from the Area excavation was
transported by Gelder Thompson to the CMS Landfill in Concord North Carolina for permitted
disposal see Non-Hazardous Waste Manifest in Appendix
RECEPTOR SURVEY
On July 20 2007 Mr Eddie Rogers of ESP performed receptor survey to document the
presence or absence of active and/or inactive water supply wells within 1500-foot radius of the
subject UST release see Figure Receptor Survey Map The receptor survey included
interviews with available site occupants and visual observations for water supply wells and/or
municipal water meters All properties within 500 feet of the site were visited to determine well
status The area within 1000 feet of the subject release consists of commercial and industrial
development with numerous vacant structures No active or inactive water supply wells were
identified within 1000-foot radius of the subject release Municipal water and sewer have
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area August 23 2007
historically been available within the area of the site Additionally no surface water bodies were
identified within 500 feet of the release see Figure
CONCLUSIONS AND RECOMMENDATIONS
The following conclusions have been formulated based on our completion of field activities
including abatement activities receptor survey and our review of laboratory data from the
analysis of collected soil samples
The subject site the location of former Duke Energy-Worth Keeter facility has an
address of 1000 South Clarkson Street Tax Parcel No 07325207 in Charlotte
Mecklenburg County North Carolina
On August 2007 ESP responded on behalf of Beazer Homes to an encounter with
1300-gallon steel apparent diesel UST along with soils with petroleum odor during
mass grading operations
at the subject site
On August and 2007 ESP documented the excavation of 39.14 tons of impacted
soils from the release area The resulting excavation measured approximately ft 18 ft
ft deep
ci Neither groundwater bedrock nor free product were encountered within the tank pit
ci On August 2007 confirmatory soil samples were collected at depth of 3.5 feet BLS
from each of the excavations four sides WS-l through WS-4 while one sample was
collected at depth of feet BLS from the base of the excavation B-i
ci Results of the laboratory analysis
of confirmatory samples WS-i through WS-4 and B-l
revealed that all analyzed constituents were either below reporting limits BRLs or
below the lowest of the soil-to-groundwater or residential MSCC
ci On August 2007 ESP collected composite stockpile soil sample designated 1A/iB
for laboratory analysis
The composite sample was collected and analyzed to confirm
that release had occurred and to characterize contaminant types and concentrations for
subsequent off-site permitted disposal/treatment
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area August 23 2007
As revealed by the laboratory analysis of stockpile composite sample 1A/1B TPH-DRO
was reported at concentration of 710 mg/Kg and TPH-GRO at concentration of 6.9
mg/Kg while results for the remainder of analytes were BRLs
On August 16 and 17 2007
39.14 tons of stockpiled soil from the Area excavation was
transported to the CMS Landfill in Concord North Carolina for permitted disposal
Municipal water and sewer are available in the area of the release
ci No water supply wells were identified within 1000 feet of the release and
ci No surface water bodies were identified within 500 feet of the subject release
Based on
the absence of analyzed risk-based soil parameters above the lowest of the North
Carolina soil-to-groundwater or residential MSCCs lack of either groundwater bedrock or free
product within the tank pit the documented absence of water supply wells within 1000 feet of
the release and the absence of surface water feature within 500 feet of the release ESP
recommends that NCDENR issue notice of no further action for the subject release
Attachments
Table B-i Summary of Soil Sampling Results
Table B-2 Summary of Stockpile Soil Sampling Results
Figure Topographic Site Location Map
Figure 2005 Aerial Photograph
Figure Soil Sample Location Map
Figure Receptor Survey Map
Appendix 24-Hour Release Notification
Appendix UST-2 Form
Appendix Tank Disposal Manifest
Appendix Product Material Manifest
Appendix Site Photographs
Appendix ESPs SOP
Appendix Prism Laboratory Data Reports
Appendix Non-Hazardous Waste Manifests
ATTACHMENTS
TABLES
Date 8/20/07 Incident No Not Yet Assigned
Analytical Method
Coiifaminantof Concern
Samplp Date Ource Sanp1e Ilicident
Collected Ara Depth Phase
in/1yy ft B3S C-
WS1 8/2/07 South Pit initial
Wall Abatement
Table B-i Summary of Soil Sampling Results
Morehead Common Area Charlotte North Carolina
6010B 6010B
MADEP
EPH
MADEP
EPH
MADEP
EPJ-I
MADEP
VPH
MADEP
VPH
MADEP
VPH
CJDc.9
Eii
ID fl22 ID ID ID
O-
21 110 11 11 11 5.5 5.5 5.5
WS-2 8/2/07 West Pit
Wall 3.5 Initial
Abatement 18 58 11 11 11 5.6 5.6 5.6
WS-3 8/2/07 North Pit
Wall 3.5 Initial
Abatement 18 100 11 ii 11 5.7 5.7 5.7
WS-4 8/2/07 East Pit
Wall 3.5 initial
Abatement 23 150 15 11 11 5.6 5.6 5.6
24 98 11 11 11 5.6 5.6 5.6InitialB-i 8/2/07 Pit Floor Abatement
Soil to Groundwater MSCC mg/kg
Residential MSCC mg/kg
Industrial/C ohnnerciaI MSCC mg/kg
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNL Not Listed
270 34 3300 72 34
47 400 469 93860 9386
939 469 9386
1226 400 12264 245280 24528 12264 245280
Table B-i
Date 8/20/07 Incident No Not Yet Assigned
Analytical Method
Contaminant of Concern
Sample Date Source Sample Incident
ID collected Area Depth Phase
in/dd/yy ft I3GS
WS-1
Summary of Soil Sampling Results
Morehead Common Area Charlotte North Carolina
8/2/07
8260B 8260B 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C
South Pit
Wall 3.5 Initial
Abatement
ca
CO
aC
COaO
0.0051 0.0051 0.25J 0.32J 0.17J 0.16J 0.16J 0.19J 0.17J 0.37J
WS-2 8/2/07 West Pit
Wall 3.5 Initial
Abatement 0.0050 0.0050 0.37 0.37 0.37 0.37 0.37 0.37 0.37 0.37
WS-3 8/2/07 North Pit
Wall 3.5 Initial
Abatement 0.0048 0.0048 0.17J 0.21J 0.I1J 0.1OJ 0.37 0.37 0.37 0.25J
WS-4 8/2/07 East Pit
Wall 3.5 Initial
Abatement 0.0044 0.0044 0.28J 0.33J 0.l4J 0.16J 0.14J 0.14J 0.l7J 0.36J
Initial
Abatement 0.0052 0.0052 0.37 0.37 0.37 0.37 0.37 0.37 0.37 0.37
60 290 38 0.34 0.091 1.2 12 280
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
ft Health based level 100%
Considered immobileNANotAnalyzedNIL Not Listed
3129 3200
469 469 88 0.88 0.0088 0.88 620
81760 82000 12264 12264
780 0.78 78 16400
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg unless otherwise noted
Health based level 100%
Considered immobileNANotAnalyzedNL Not Listed
Table .B-2
Date 8/20/07 Incident No Not Yet Assigned
Analytical Method 3550
contaminant of Concern
Sample Date Source Sample Incident
1D Collected Area Depth Phase
m/dd/yy ft BGS
Stock InitiallA/lB 8/2/07 nile composite 710Abatement
Summary of Stockpile Soil Sampling Results
Morehead Common Area Charlotte North Carolina
5030 8260B 8260B 8260B 8260B
6.9 0.0033 0.0055
Soil to .rouiidwater MSCI mg/kg
Residential .\l 5CC nig/kg
nthistnal/oinniercial \IS lug/kg
0.0055
NL NL 0.0056 7.3 4.6
8.OJ
NL NL 164 82000 40000 81760
NL NL 18 3200 1560 3129
FIGURES
2.601I SHEET 77TLE FIGURECALENTST4QAPH/C 51Th LOCA liON MAP PA
ME 7/11/o7L USGS CHARLOTTE EAST QUADRANGLE
AV.YBY 1PROJECT
CHECKED BY MOREHEAD COMMON SiTE
MI
F/CURE CHARLOTTE NORTH CAROLINA
fr
U2.6O SHEET TITLE FiGURE
SCALE NTS 2005 AERIAL PHOTOGRAPH LIA7E7/11/07
RM$fY BYDMH PROJECT MOREHEAD COMMON SiTE JaiLCHECKEDCJWCHARLOTTE NORTH CAROLINA
ESP Associates P.A
PO Bos 7030ChdttNC28241
3475 Lakcsosi BId
Eon M7I SC 29700
774-583-4949 NC
903-802-2440 SC
DUNBAR STREET
WS-3
WS-2 WS-4
ws-1
LEGEND
CONRRMA TORY SOIL SAMPLE LOCA liON
FORMER LOCA liON OF UST
AREA EXCA VA liON DEPTH OF FEET
FiGURE
SOIL SAMPLE LOCA 770N MAP AREA
20
APPROXIMATE SCALE
IN FEET
MOREHEAD COMMON SITE
CHARLOTTE NORTH CAROLINA
ESP
\\
RaCTNO SHEET TiTLE FIGURECALENTSRECEPTORSURtY MAP
ATE 8/21/07 AREARABYQMHPROJECTMOREHEADCOMMON SiTEHECKED
CHARLOTTE NORTH CAROLINA
APPENDIX
24-HOUR RELEASE NOTIFICATION
UST61 24Hour Release and UST Leak Reporting Fomi
For Releases This farm
should be completed and submitted to he UST Sections regional olflce allowing Known or suspected release from
an underground storage tank USI system This lomi is required to be submitted within 24 hours of discovery of known or
In NC suspected release
DWM USE ONLY Suspected Contamination YIN Facility ID Number OIctuiL3
Incident Risk HILU_______Conlirmed GW Contamination Y/N Date Leak Discovered
Received On Received By Confirmed Soil Contamination YIN IV Comm/Non-Commercial oXm
Reported by circle one Phone Fax or Report Free Product YIN II Yes Stale Greatest ReglNon-regulated
Region ______Thickness it74
INCiDENT DESCRIPTION
tncident Name
Address O9O 5/77/4.5t9/J CoUnty
Regional Office circle one Ashevilt oresvil FayettevilleCity/Town Zip Code Z-3Z Raleigh Washington Wilmington
Latitude dcânl dgnas .loifI7 Longitude de adcgc Obtained by
Briefly describe suspected or confirmed release including but not limited to nature orelaase date of release amount GPSofreleaseamountoffreeproduct present
and recovery efforts initial responses conducted impacts to receptorse/0 47 Topographiomap
1Y-Jv-1L9 tJ id GIS Address matching//J Other
1/
ft fh1vs-c /2tui /Vr frt
64 Describe location
HOW RELEASE WAS DICOVRED
Check one
Release Detection Equipment or Methods Visual/Odor Groundwater Contamination
During UST ClosureRemoval Water in Tank Surface Water Contamination
Property Transfer Water Supply Well Contamination j4 Other specify 5i
SOURCE OF CONTAMINATION
Primary Source of Contamination Primary Contaminant Type Location Setting
Check one C/eck one Checkcnei4Gasoline/DiesellKerosene Facility Residential
Confirmed UST Release Check one below Heating Oil Residence Industrial
Dispenser Other Petroleum Products other UrbanLineReleaseMetalsRuralTankReleaseOtherInorganics
Spill/Overllll Other OrganicsExactFailureLocalionUnknownor
Multiple Failures
Ownership
Municipal Military Unknown 4ate Federal County State
Operation Type
Public Service Agricultural ential Education/Relig Industrial Mining
UST Form 6111/05 Page of
IMPACT ON DRINKING WATER SUPPLIES
WaterSupply Wells Affected Yes No
Number of Water Supply Wells Affected
//Tit/A/OP9 fr 72
Water Supply Wells Contaminated Include Users Names Addresses and Phone Numbers Attach additional sheet if necessar
UST SYSTEM OWNER
UST OwnedCompany
-t2 /7v14e
Point of Contact rRuc
City Stalecg7r NC
Address 2L V2 re
Zip Code Telephone Number2Zo3c/t2
Address
Zip Code Telephone Number
LANDOWNER AT LOCATIO
Landowner4ne 4-6o1
City State
OF UST INCIDENT
Telephone Numoer
Address
Zip COdE
Draw Sketch of Area showing two major road intersections or Attach Map
k714-74fe
Person Reporting Incident Chv-ij lLJa4 Company /J Telephone 4umber8ocq/litle AddressQ Date
UST ape
ator/Cpy
City
UST SYSTEM OF ERATOR
State
USTForrn6l 11/05 Page2of2
SHEET 71TLE FiGURE Ancit PANTS2005AERIALPHOTOGRAPHuATE7/fl/C0R4tV8r PROJECT rrDMHMOREHEADCOMMCWShE
CHARLO7Th N0R17-I CAROLINA
APPENDIX
UST-2 FORM
ST2 Site Investigation Report for Permanent Cosure or ChangeinService of UST
Return completed form to STATE USE ONLY
The DWM Regional Office located in the area where the facility is located Send copy to the Central Office in Iiti so that __________________the status of the tank may be changed to PERMANENTLY CLOSED and your tank fee account can be closed outSEEMAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES Date Received
INSTRUCTIONS READ THIS FIRST
For more than five UST systems you may attach additional forms as needed
Permanent closure For permanent closure complete all sections of this form
Change-in-service For change-in-service where UST systems will be converted from containing regulated
substance to storing non-regulatedsubstancecompletesectionsII III IV and VIII
Effective February 1995 all UST closurelchange-in-service reports must be submitted in the format provided in the UST-1 form UST closure and
change-in-services must be completed in accordance with the latest version of the Guidelines for Tank Closure copy of the UST-1 form and theGuidelinesforTankClosurecan be obtained at www.wastenotnc.org
You must make sure that USTs removed from your property
are disposed of properly When choosing closure contractor ask where the tanks will be
taken for disposal Usually
USIa are cleaned and cut up for scrap metal This is dangerous work and must be performed by qualified company Tanks
disposed of illegally in fields or other dumpsites can leak petroleum products
and sludge into the environment If your tanks are disposed of improperly youcouldbeheldresponsibleforthecleanupofanyenvironmentaldamagethatoccurs
NOTE If release from the tanks has occurred the se assessment portion of the tank closure must be conducted under the supervision of P.E orL.G with all closure site assessment reports bearing the signature and seal of the P.E or L.G
OWNERSHIP OF TANKS II LOCATION OF TANKS
Owner Name Corporation Individual Public Agency or Other Entity Facility Name or CompanyBeazerHomesNA
Street Address Facility ID If known1300BoulevardSuiteNA
City County Street Address
Charlotte Mecklenburg 1000 South Clarkson Street
State Zip Code City County Zip CodeNC28203-4265 Charlotte Mecklenburg 28278
Phone Number Phone Number
704-370-7200
III CONTACT PERSONNEL
Contact for Facility Job Title Phone NoN/A
Closure Contractor Name Closure Contractor Company Address Phone No
Jim Strattford Gelder Thompson P0 Box 288 Midland NC 28107 704-269-0070
Primary Consultant Name Primary Consultant Company Address Phone No
Chris Ward PG ESP Associates P.A P0 Box 7030 Charlotte NC 28241 704-802-2440
IV UST INFORMATION FOR REGISTERED UST SYSTEMS EXCAVATION CONDITION
Tank Size in Tank Last Last Use Permanent Change-in-Water in Free Notable odor or visible
ID No Gallons Dimensions Contents Date Close Date Service excavation product soil contminatiorr
Yes No Yes No Yes NoDateLU
UU
VI UST INFORMATION FOR UNREGISTERED UST SYSTEMS VII EXCAVATION CONDITION
Tank Size in Tank Last Last Use Permanent Tank Owner Water in Free Notable Odor or visibleIDNoGallonsDimensionsContentsDateCloseDateNameexcavationproductsoilcontaminationYesNoYesNoYesNo
1300 12 ft.x 4.3ff Dielsel Diels NA 8/1/07
UU UUUU
If the tank owner address is different from the one listed in Section then enter the street address city state zip code and telephone no belowCERTIFICATIO
certify under penalty of law that have personally examined and am familiar with the information submitted in this and all attached documents and thatbasedonmyinquiryofthoseindividualsimmediately responsible
for obtaining the information etIee that the submitted infowiation is true accurate andcomplete
Print name and official title of owner or owners authorized
Christopher Ward PG Department Manager ESP Associates PA
UST-2 Rev 11/2006
APPENDIX
TANK DISPOSAL MANIFEST
Environmental and Industrial Services
P.O Box 484 High Point NC Phonö 336 434-7750 FAX [phone]
TANK DISPOSAL MANIFEST
Tank Owner/Authorized Representative Name and Mailing Address _________________________________
\f f4L /J
Tank Owner/Authorized Representative Contact
Phone
DesiptionOfTanks
Tank No Capacity Previous Contents CommentsTO
Tank Owner/Authorized Representativejatjon The undersigned cerfies that the above listed storagetankshave been removed from the premises of the tank owiier
Printed/Typed Name Signature ManiA/Day/Year
Transporter The undersigned certifies that the above listed storage tanks have been transported to AD
Environmental and Industrial Services 2718 Uwharrie Road Archdale N.C 27263
Th
_/
Printed/Typed Name Signature Month/Day/Year
Disposal Certification The undersigned certifies that the above-named storage tanks have been cut
into scrap pieces
and accepted by the metal recycling facility
li
Recycling Facility
/1
Printed/Typed Name Signature Month/Day/Year
APPENDIX
PRODUCT MATERIAL MANIFEST
Manifest Document No
AD 10155
Environmental and
POST OFFICE BOX 484
HIGH POINT NC 27261
TERIAL
MANIFEST
EMERGENCY PHONE NO
t80O 434-7750
Industrial Services Inc
TEL [phone]
FAX [phone]
$1
Street Address
Page of
LiaLLAv
ADJobNo
DESCRIPTION OF MATERIALS
GENERATOR INFORMATION
USEPAIDNo
Phone No
Contac j1 L4
USDOT Proper Shipping
Name Hazard UN NA Packing Containers Total Unit
HM Complete All Items for Hazardous Materials Class or Div ID No Group Qty Type Quantity WtJ VolJdAJoft/V 3I
ADD TIONAL INFORMATION ERG No Profile Code Pafllty Use
-t fe
GENERATORS CERTIFICATION
This is to certify that the above-described materials are properly classified described packaged marked and labeled and are in
proper condition for transportation according to the applicable regulations of the Department of TranspÆrtation further certify
that none of the materials described above are hazardous waste as defined by EPA 40 CFR Part 261 or any applicable state lawandunlessspecificallyidentifiedabovethe materials contain less than 1000 ppm total halogens and do not contain quantifiablelevelsppmofPCBsasdefinedbyEPA40CFRParts279 and 761
Printed Typed Name Signature Mo Day Yr
TRANSPORTER INFORMATION
Transporter hereby acknowledge receipt of the above-described materials for transportENVIRONMENTALANDINDUSTRIAL SERVICES from the generator site listed above
Address
2718 UWHARRIE ROAD
ARCHDALE NC 27263 hereby acknowledge tthe above-described materials were received
Transporter or Unit No from the generator site and were transported to the facility listed belowEPAIDNONCD986232221yii_
TiPhone336434-7750 Signature Delivery Date
FACILITY INFORMATION
Facility hereby acknowledge receipt of the materials covered by this manifestENVIRONMENTAlANDINDUSTRIALSERVICESexceptforany discrepancy
noted below
Address
2718 UWHARRIE ROAD
Signature Recei DateARCHDALENC27263.DjscŁpancjes
Facility or
EPA ID No NCD986232221
Phone [phone]
Contact ERIC McMANUS
OPIrIN F-rlit Ppfj ...n rr
APPENDIX
SITE PHOTOGRAPHS
APPENDIX
ESPS SOP
STANbARb OPERATING PROCEDURE
SOP-
SOIL SAMPLE COLLECTION
ESP Associates P.A Revision bate 3/7/06
This standard operating procedure SOP covers the collection of soil sample for
laboratory analysis
Follow these steps when collecting the soil sample unless
otherwise instructed by the project manager
Gather needed field supplies noted below
Confirm lab cooler contains needed sample containers fill cooler with
ice
Upon arriving at site check in with the property owner or company
representative
becontaminate the stainless steel hand auger before and between sample
collection by washing
with Alconox soap and scrub brush rinsing with
distilled water and spraying with Isopropyl alcohol Wrap clean sampler
in aluminum foil
Wear disposal latex or nitrile gloves and change into new pair between
samples
During advancement of the hand auger collect soil samples at regular
intervals for describing lithology Note lithology and other
characteristics of soils in field book relative to depth
If appropriate place representative portion of soil sample into
resealable plastic bag label with boring number and depth interval and
allow to equilibrate Screen soil in bag for volatile organics using an OVA
or Hnu Enter results into field book
Advance hand auger boring to previously specified sampling depth
Collect soil sample from this depth and place in laboratory provided
containers Label containers with boring number and sample depth using
the following sampling scheme i.e B-i ft B-i 10 ft B-2 ft etc
Denote boring location in field book relevant to pertinent site features
10 Following collection of the soil samples abandon all boreholes feet or
greater in depth with cement grout
11 Complete and sign the labs chain-of-custody
12 Keep the sample cooler in secure location until delivered under normal
chain-of-custody procedures to laboratory
SOP-6 Soil Sample Collection Revision bate 3/7/06
ESP Associates Page of
SUPPLIES
LI SOP-6
LI Stainless steel hand auger with needed extensions or sampUng
spoon
OVA or Hnu
LI Measuring tape
LI Plastic zip-lock bags
LI Isopropyl alcohol
LI bistilled water
5-gallon wash bucket scrub brush and Alconox soap
LI Cement with wheel barrow for mixing
LI Cooler with sample containers and chain-of-custody
LI Ice
LI Permanent marker
LI bisposable gloves
Knife
LI Field book
LI Site plan with site specific sampling instructions
LI Camera
APPENDIX
PRISM LABORATORY DATA REPORTS
Case NarrativePRISM
IJBORATORIESINC
Date 08/1 0/07
Client Project ID Morehead Commons No
Company ESP Associates PA Prism COG Group No G0807084
Contact Chris Ward Collection Dates 08102107
Address Box 7030 Lab Submittal Dates 08102/07
Charlotte NC 28241
This data package contains the analytical results for the project identified above and includes Case Narrative Laboratory Report and Quality
Control Data totaling 44 pages chain-of-custody is also attached for the samples submitted to Prism for this project
Data qualifiers are flagged individually on each sample key reference for the data qualifiers appears at the end of this case narrative Quality
control statements and/or sample specific remarks are included in the sample comments section of the laboratory report for each sample
affected
Semi Volatile Analysis
No Anomalies Reported
Volatile Analysis
Analysis Note for Q25565 MS C9-C12 Aliphatics Recovery above the control limits
Analysis Note for Q25565 MSD C9-C12 Aliphatics Recovery above the control limits
Metals Analysis
Analysis Note for Q25521 MS Chromium MS recovery outside of the control limits Analysis was repeated with similar QC results
Analysis Note for Q25521 MS Lead MS recovery outside of the control limits Analysis was repeated with similar QC results
Analysis Note for Q25521 MSD Chromium RPD recovery outside of the control limits Analysis was repeated with similar QC
results
Analysis Note for Q25521 MSD Lead MSD recovery RPD were outside of the control limits Analysis was repeated with similar
QC results
Wet Lab and Micro Analysis
N/A
Please call if you have any questions relating to this analytical report
Date Reviewed by Paula Gilleland Project Manager
Signature TI.UQC.i22tftaL Signature
Review Date 0811 0/07 Approval Date
Data Qualifiers Key Reference
Compound also detected in the method blank
th Result outside of the QC limits
DO Compound diluted out
Estimated concentration calibration range exceeded
The analyte was positively identified but the value is estimated below the reporting limit
Estimated concentration with high bias
Estimated concentration with low bias
matrix effect is present
Angela Overcash
aAAQ KL
08110/07
Notes This report should not be reproduced except in its entirety without the writtten consent of Prism Laboratories Inc The results in this
report relate only to the samples submitted for analysis
449 Springbmok Road P.O aox 240543 Chao1te NC 28224-0403
Phone [phone] Tot Free 8001529-6364 Fax [phone]
NC Certification No 402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735 08/10/07
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 188652
Sample Matrix Soil coc Group G0807084
Time Collected 08/02/07 915
Time Submitted 08/02/07 1325
Percent Solids Determination
Percent Solids
5035
5035
5035
08/10/07 000 Ibrowi
08/10/07 000 brown
08/10/07 000 Ibrown
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Datellime ID
90.2 SM2540 08/03/07 1555 ddixon
Samp Weight Determination
Weight Bisulfate 5.31
Weight Bisulfate 5.32
Weight Methanol 5.73
Volatile Orcianic Comceunds by GC/MS
111-Trichioroethane BRL mg/kg 0.0051 0.00029 82606 08/03/07 1702 Iwitry 025514
1122-Tetrachioroethane BRL mg/kg 0.0051 0.00052 82608 08/03/07 1702 Iwitry 025514
112-Tiichloroethane BRL mg/kg 0.0051 0.00032 8260B 08/03/07 1702 Iwitry 025514
1.1-Dichioroethane BRL mg/kg 0.0051 0.00037 82606 08/03/07 1702 Iwihy 025514
11-Dichioroethene BRL mg/kg 0.0051 0.00039 8260B 08/03/07 1702 Jwiuiy 025514
1-Dichloropropene BRL mg/kg 0.0051 0.00045 8260B 08/03/07 1702 Iwitry 025514
123-Tiichlorobenzene BRL mg/kg 0.0051 0.00056 8260B 08/03/07 1702 Iwitry 025514
123-Tnchloroproparie BRL mg/kg 0.0051 0.00045 82606 08/03/07 1702 Iwihy 025514
124-Trichloroberizene BRL mg/kg 0.0051 0.00049 8260B 08/03/07 1702 IWitry 025514
124-Trirnethylbenzene BRL mg/kg 0.0051 0.00039 8260B 08/03/07 1702 lwitcy 025514
12-Dibromoethane EDB BRL mg/kg 0.0051 0.000092 8260B 08/03/07 1702 Iwitxy 025514
12-Dichioroberizene BRL mg/kg 0.0051 0.00028 82606 08/03/07 1702 Iwitry 025514
12-Dichtoroettn BRL mg/kg 0.0051 0.00051 82606 08/03/07 1702 twitr 025514
12-Dichioropropane BRL mg/kg 0.0051 0.00038 8260B 08/03/07 1702 lwitry 025514
13Thmethylbenzene BRL mg/kg 0.0051 0.00043 82606 08103/07 1702 025514
13-Dlchlorobenzene BRL mg/kg 0.0051 0.00044 8260B 08/03/07 1702 twitr 025514
1.3-Dichioropropane BRL mg/kg 0.0051 0.00035 8260B 08/03/07 1702 lwitry 025514
BRL mg/kg 0051 0004 8260B 0810307 1702 lWlttY 025514
22-Dichtoropropane BRL mg/kg 0.0051 0.00026 8260B 08/03/07 1702 lwitry 025514
2-Chiorotoluene SRI mg/kg 0.0051 0.00038 82606 08/0307 1702 lwit 025514
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of 35
Laboratory ReportScCertificationNo99012
NC Drinking Water Cert No 37735 08110/07
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 188652
Sample Matrbc Soil coc Group G0807064
Time Collected 08/02/07 915
Time Submitted 08/02/07 1325
This report should riot be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method
Limit
AnalystAnalysis Batch
Factor Date/Time ID
2-1-lexanone BRL mg/kg 0.051 0.00053 8260B 08/03/07 1102 Iwitry 025514
4-Chlorototuene BRL mg/kg 0.0051 0.00027 82603 08103/07 1702 lwitty Q5514
4-Methyl-2-pentanone MIBK BRL mg/kg 0.051 0.00051 8260B 08/03/07 1702 lwiuy 025514
Acetone BRL mg/kg 0.051 0.0020 826DB 08/03/07 1702 IWIIIY 025514
Benzene BRL mg/kg 0.0031 0.00041 82603 08/03/07 1702 IwItry 025514
Bromobenzene BRL mg/kg 0.0051 0.00036 82603 08/03/07 1702 witry 025514
Bromoohloromethane BRL mg/kg 0.0051 0.00031 82603 08/03/07 1702 twitii 025514
Bromodichloromethane BRL mg/kg 0.0051 0.00045 8260B 08103107 1702 Iwitzy 025514
Bromoform BRL mg/kg 0.0051 0.00038 826DB 08/03/07 1702 iwitry 025514
Bromomethane BRL mg/kg 0.010 0.0006 826DB 0803/07 1702 twitsy 025514
Carbon tetrachlode BRI mg/kg 0.0051 0.0003 8260B 08/03/07 1702 lwttiy 025514
Chlorobenzene BRL mg/kg 0.0051 0.00039 8260B 08/03107 1702 Iwitiy 025514
Chiorodibromometharie BRL mg/kg 0.0051 0.00035 826DB 08/03/07 1702 lwitiy Q25514
Chloroethane BRL mg/kg 0.010 0.00042 82603 08103/07 1702 Iwitry Q25514
Chloroform BRL mg/kg 0.0051 0.00038 82603 08/03/07 1702 Iwiby Q25514
Chtoromethane BRL mg/kg 0.0051 0.00036 826DB 08/03/07 1702 lwitri 025514
cis-1 2-Dithloroethene BRL mg/kg 0.0051 0.00023 826DB 08/03/07 1702 Iwitry 025514
cis-13-Dichloropropene BRL mg/kg 0.0051 0.00033 826DB 08/03/07 1702 lwitr 025514
Diohiorodifluoromethane BRL mg/kg 0.0051 00011 826DB 08/0307 1702 twitry 025514
Ethylbenzene BRL mg/kg 0.0051 0.00036 8260B 08/03/07 1702 lwitiy 025514
Isopropyl ether IPE BRL mg/kg 0.0051 0.00017 8260B 08/03/07 1702 lwitiy 025514
Isopropylbenzene BRL mg/kg 0.0051 0.00041 82603 08/03/07 1702 witty 025514
rnp-Xylenes BRL mg/kg 0.010 0.00072 826DB 08/03/07 1702 Iwitry Q25514
Methyl ethyl ketone MEK BRL mg/kg 0.10 0.0014 8260B 08/03/07 1702 Iwitry 025514
Methyl t-butyl ether MTBE BRI mg/kg 0.010 0.0003 8260B 08/03/07 1702 lwitty 025514
Methylene chloride BRL mg/kg 0.0051 0.00042 82603 08/03/07 1702 Iwitry 025514
n-Butylbenzene BRL mg/kg 0.0051 0.00041 82603 08/03/07 1702 lwitry 025514
Page of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
08110107
ESP Associates PA Project ID Morehead Commons No Client Sample ID WS-1
Attn Chris Ward Prism Sample ID 188652
Box 7030 Sample Matrix Soil COC Group G0807064
Charlotte NC 28241 Time Collected 08102107 915
lime Submitted 08/02/07 1325
Parameter Result Units Report MDL Diluthn Method Analyst Batch
ID
Analysis
Limit Factor Date/Time
0.0051 0.00031 8260B 08/03/07 1702 Iwttry 025514
0.010 0.0006 8260B 08/0307 1702 lwitzy Q25514
0.0051 0.00031 82608 08/03/07 1702 IWttnJ 025514
0.0051 0.00042 8260B 08/03/07 1702 IwiUy 025514
0.0051 0.00034 8260B 08/03107 1702 Iwltry 025514
0.0051 0.00051 8260B 08/03/07 1702 Iwitsy 025514
0.0051 0.00032 8260B 08103107 1702 Iwiliy 025514
0.0051 0.00088 8260B 08/03/07 1702 iwitry 025514
0.0051 0.00035 8260B 08/03/07 1702 Kitiy 025514
0.0051 0.00039 8260B 08/03107 1702 lwitiy 025514
0.0051 0.00036 8260B 08/03/07 1702 IwitAy Q25514
0.0051 0.00031 8260B 08/03/07 1702 Iwitry 025514
0.0051 0.00042 8260B 08/03/07 1702 Iwitsy 025514
0.026 0.0019 82608 08/03/07 1702 lwitry 025514
0.0051 0.00066 8260B 08/03/07 1702 willy 025514
n-Propylbenzene BRL
Naphthalene BRL
c-Xylene BRL
p-lsopropyltoluene BRL
sec-Butylbenzene BRL
Styrene BRL
tert-Butytbenzene SRI
Tetrachloroethene BRL
Toluene BRL
trans-I 2-Dichloroethene SRI
trans-i3-Dichloropnpene BRL
Trithioroethene BRL
Trichiorofluoromethane BRL
Vinyl acetate BRL
Vinyl chloride BRL
Semi-volatile Organic Compounds by GCMS
24-Trichlorobenzene BRL
2-Dichlorobenzene BRL
13-Dlchlorobenzene SRI
I4-Dichlorobenzene BRL
245-Trichlorophenot BRL
246-Trichiorophenol BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Surrogate Recovery Control Limits
Toluene-d8 97 81-128
Dibromofluoromethane 90 67-143
Bromofluombeozene 110 77-128
0.37
0.37
0.37
0.37
0.37
0.37
0.038
0.027
0.026
0.033
0.037
0.035
8270C
82700
8270C
8270C
82700
82700
08/07/07
08107/07
08/07/07
08/07/07
08107/07
08/07/07
1402
1402
1402
1402
1402
1402
kcamplgotto
kcarnpIotto
kcamplgotto
kcamplgotto
kcamplgotto
kcamplgotto
025550
025550
025550
025550
025550
025550
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of 35
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toil Free Number 1-8001529-8354 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full 2Mce Mly1kl lronmril Sluon
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
08/10/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
wS-l
188652
G0807064
08/02107 915
08/02/07 1325
Parameter Result Units Report MDL Dilution Method AnalystAnalysis Batch
Limit Factor Date/Time ID
24-Dichlorophenol BRL mg/kg 0.37 0.031 82700 08/07/07 1402 kcampigotto Q25550
24-Dlmethylphenol BRL mg/kg 0.37 0.035 82700 08/07/07 1402 kcampigouo 025550
2.4-Dinitrephenol BRL mg/kg 1.8 0.041 82700 08/07/07 1402 kcamplgotto 025550
24-Dinitrotoluene BRL mg/kg 0.37 0.021 8270C 08/07/07 1402 kcampigotto 025550
26-Dinitrotoluene BRL mg/kg 0.37 0.039 8270C 08/07/07 1402 kcampigotto 025550
2-ChIoronaphthatene BRL mg/kg 0.37 0.038 8270C 08/07/07 1402 keamplgotto 025550
2-Chiorophenol BRL mg/kg 0.37 0.029 62700 08/07/07 1402 kcampigofto 025550
2-Methylnaphthalene BRL mg/kg 0.37 0.029 82700 08/07/07 1402 keamplgotto 025550
2-Methyiphenol BRL mg/kg 0.37 0.034 8270C 08/07/07 1402 kcampigofto 025550
2-Nilrophenol BRL mg/kg 0.37 0.044 82700 08/07/07 1402 kcampigotto 025550
34Methylphenol BRL mg/kg 0.37 0.037 82700 08/07/07 1402 kcampigotto Q25550
33-Dichlorobenzidine BRL mg/kg 0.73 0.023 82700 08/07/07 1402 kcampigotto 025550
46-Dinitro-2-methylphenol BRL mg/kg 1.8 0.022 8270C 08/07/07 1402 keamplgotto 025550
4-Bromophenyiphenylether BRL mg/kg 0.37 0.035 8270C 08/07/07 1402 koampigotto 025550
4-Chloro-3-methylphenol BRL mg/kg 0.73 0.027 8270C 08/07/07 1402 kcampigotto 025550
4-Chloroaniline BRL mg/kg 0.37 0.047 82700 08/07/07 1402 kcamplgotto 025550
4-Chiorophenyiphanylether BRL mg/kg 0.37 0.023 82700 08/07/07 1402 kcampigotto 025550
4-Nitropheno BRL mg/kg 1.8 0.024 8270C 08/07/07 1402 kcamplgotto 025550
Acenaphthene BRL mg/kg 0.37 0.038 8270C 08/07/07 1402 kcamplgotto 025550
Acenaphthylene BRL mg/kg 0.37 0.036 82700 08/07/07 1402 kcampigotto Q25550
Anthracene BRL mg/kg 0.37 0.028 82700 08/07/07 1402 kcamplgotto 025550
Azobenzene BRL mg/kg 1.8 0.034 8270C 08/07/07 1402 kcamplgotto 025550
Berizoaanthracene 0.16 mg/kg 0.37 0.051 82700 08/07/07 1402 kcampigotto 025550
Benzoapyrene 0.18 mg/kg 0.37 0.042 82700 08/07/07 1402 kcamplgotto 025550
Benzobfiuoranthene 0.19 mg/kg 0.37 0.016 8270C 0807/07 1402 kcamplgotto 025550
Benzoghiperylene BRL mg/kg 0.37 0.017 8270C 08/07/07 1402 keamplgotto 025550
Benzokfiuoranthene 0.17 mg/kg 0.37 0.030 8270C 08/07/07 1402 kcamplgotto 025550
Page of 35
utoJ
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample 10
Prism Sample ID
Sample Matrix Soil COC Group
lime Coilected
Time Submitted
wS-1
188652
00807064
08102/07 915
08/02/07 1325
This report should not be reproduced except in its entirety without the wiitten consent of Prism Laboratories Inc
449 Sprlngbrook Road.P.O Box 240543 Charlotte NC 28224-0543
Phone [phone]-Toll Free Number 1.000/529-6364 Fax [phone]
NC Cerlilication No 402
SC Certification No 99012
NC Drinking Water CerL No 37735
Laboratory Report
08/10107
Parameter Result Units Report MDL Dilution Method Analyst Batch
ID
Analysis
Limit Factor Date/Time
Benzoic acid BRL mg/kg 1.8 0.16 8270C 08/07/07 1402 kcampigotto 025550
Benzyl alcohol BRL mg/kg 0.73 0.039 8270C 08/07/07 1402 kcampigotto 025550
Bis2-chloroethoxymethane SRI mg/kg 0.37 0.042 8270C 08/07/07 1402 kcampigotto 025550
Bis2-chloroethylether BRL mg/kg 0.37 0.040 8270C 08/07/07 1402 kcampigotto 025550
Bis2-chloroisopropylether BRL mg/kg 0.37 0.031 8270C 08/07/07 1402 kcampigotto 025550
Bls2-ethylhexytphthalate BRL mg/kg 0.37 0.018 8270C 08/07/07 1402 kcamplgotto 025550
Butylberizylphthalate BRL mg/kg 0.37 0.022 8270C 08/07/07 1402 kcampigotto 025550
Chrysene 0.17 mg/kg 0.37 0.061 8270C 08/07/07 1402 kcampigotto 025550
Di-n-butylphthalate BRL mg/kg 0.37 0.017 8270C 08/07/07 1402 kcampigotto 025550
Di-n-octylphthalate BRL mg/kg 0.37 0.027 8270C 08/07/07 1402 kcampigotto 025550
Dibenzoahanthracene BRL mg/kg 0.37 0.037 8270C 08/07/07 1402 kcampigolto 025550
Dibenzofuran BRL mg/kg 0.37 0.031 8270C 08/07/07 1402 kcampigotto 025550
Diethylphthalate BRL mg/kg 0.37 0.023 827CC 08/07/07 1402 kcampgoUo 025550
Dimethylphthalate BRL mg/kg 0.37 0.025 827CC 08/07/07 1402 kcampigotto 025550
Fluorantherie 0.37 mg/kg 0.37 0.025 827CC 08/07/07 1402 koampigotto 025550
Fluorene BRL mg/kg 0.37 0.022 8270C 08/07/07 1402 kcampigotto Q25550
Hexachlorobenzene BRL mg/kg 0.37 0.019 8270C 08/07/07 1402 kcamplgotto 025550
Hexachlorobutadlene BRL mg/kg 0.37 0.036 827CC 08/07/07 1402 kcampigotto 025550
Hexachiorocydopentadiene BRL mg/kg 0.37 0.039 827CC 08/07/07 1402 kcampigotto 025550
Hexachloroethane BRL mg/kg 0.37 0.037 8270C 08/07/07 1402 kcampigotto 025550
lndeno123-cdpyrene BRL mg/kg 037 0.038 827CC 08/07/07 1402 kcamplgotto 025550
Isophorone BRL mg/kg 0.37 0.033 827CC 08/07/07 1402 kcampigotto 025550
N-Nltrosodl-n-propylamlne BRL mg/kg 0.37 0.042 827CC 08/07/07 1402 kcampigotto 025550
N-Nitrosodiphenylamine BRL mg/kg 0.37 0.019 827CC 08/07/07 1402 kcamplgotto 025550
Naphthalene BRL mg/kg 0.37 0.040 8270C 08/07/07 1402 koampigotto 025550
Nitrobenzene BRL mg/kg 0.37 0.036 827CC 08/07/07 1402 kcampigotto 025550
Pentachiorophenol BRL mg/kg 1.8 0.031 8270C 08/07/07 1402 kcamplgotto 025550
Page of 35
Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735 08110/07
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 188652
Sample Matrix Soil COC Group G0807064
Time Collected 08/02/07 915
Time Submitted 08/02/07 1325
Sample Preparation 29.9 mL 3550B
11 5.9
Adjusted value
11 tO
11 3.5
08/04/07 900 pbarr 19082
This repoit should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529.6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box7OSO
Charlotte NC 28241
Parameter Result Units MDL MethodDilution
Factor
AnalystReportAnalysis Batch
Limit Date/Time ID
0.25 mg/kg 0.37 0.018 08/07/07 1402 kcampigotto 025550
BRL mg/kg 0.37 0.040 08/07/07 1402 kcamplgotto 025550
0.32 mg/kg 0.37 0.025 08/07/07 1402 kcampigotto 025550
827CC
827CC
827CC
Surrogate Recovery Control Limits
Terphenyl-d14 80 41 136
Phenol-d5 69 13-95
Nitrobenzene-d5 75 14-103
2-Fluorophenol 80 14-89
2-Fluombiphenyl 76 21 108
246-Tribromophenol 87 25 123
Phenanthrene
Phenol
Pyrene
Extractable Petroleum Hydrocarbons by GC-FlD
Cl 1-C22 Aromaflcs BRL mg/kg
nalysis Note for Cl1-C22 Aromatics
C16-C36 Aliphalics BRL mg/kg
C9-C1 Aliphatics BRL mg/kg
Sample Preparation
Metals by ICP
Chromium
Lead
MADEP EPH 08/07/07 2107 grappacdoll 025548
10.14g 2mL
MADEP EPH 08/07/07 2107 grappacdoll 025548
MADEP EPH 08/07107 2107 grappaccloll 025548
EPH 08/03/07 700 pbarr P19081
Surrogate Recovery Control Limits
o-Terphenyl 82 40 140
2-Fluorobiphenyl 84 40 140
2-Bromonaphthalene 90 40 140
1-Chloro-octadecane 57 40 140
21 mg/kg 0.27 0.015 601DB 08/03/07 1959 mcampbct Q25521
110 mg/kg 0.27 0.018 6010B 08/03/07 1959 mcampbeil 025521
Page of 35
Client Sample ID
Prism Sample ID
COG Group
Time Collected
Time Submitted
ws-1
188652
G0807064
08/02/07 915
08/02/07 1325
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Sample Preparation 2.02 50 mL 3050B 08/03/07 745 ddxon P19078
Volatile Petroleum Hydrocarbons by GC-PID/FID
C5-C8 Allphafics BRL mg/kg 5.5 1.1 MADEP VPH 08/07/07 431 hwagner Q25565
Analysis Note for C5-C8 AJ.iphatics Adjusted value
Ce-do Aromatics BRL mg/kg 5.5 0.033 MADEP VPH 08/07/07 431 hwagner Q25565
C9-C12 Aliphatics BRI mg/kg 5.5 1.7 MADEP VPH 08107107 431 hwagner Q25565
Analysis Note for C9-C12 Aliphatics Adjusted value
Surrogate Recovery Control Limits
25-Dibromotoluene-PID 102 70-130
2.5-Dibromotoluene-FID 109 70-130
$amls Weight Determination
Weight 21.79 MADEP VPH 08/08/07 000 Ibrown
Weight 20.04 MADEP VPH 08108/07 000 brown
Sample Comments
BRL Below Reporting Limit
.3-Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthose instances indicated in the case narrative and/or test comments
All results are reported on dr/-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in Its entirety thout the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
ESP Associates PA
Aftn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No
Sample Matrix Soil
Laboratory Report
08/10/07
Phone [phone] IoU Free Number 14001529-6364 Fax [phone] Page of 35
NC CertIfication No 402
SC Certification No 99012
NC Drinking Water Cert No 37735____-J
Full SeMccAnilytICal oinxntil Scuffon
ESP Associates PA Project ID
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analyst Batch
Limit Factor ID
Percent Solids Determination
Percent Solids 88.8
Sam ole Weight Determination
Weight Bisulfate
Weight Bisulfate
Weight Methanol
Laboratory Report
0811 0/07
Sample Matrix Soil
Morehead Commons No Client Sample ID
Prism Sample ID
COO Group
Time Collected
Time Submitted
WS-2
188653
G0807064
08/02/07 930
08/02/07 1325
Analysis
Date/Time
8M2540G 08/03/07 1555 ddixon
000
000
000
Ibrown
Ibrown
Ibrown
5.60
5.78
5.59
BRL
BRL
BRL
BRL
BRL
BRI
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRI
BRL
Volatile Organic Compounds by GC/MS
11 1-Tichloroetharte
11 22-Tetrachloroethane
11 .2-Trichloroethane
11 -Dichloroethane
11-Dichloroethene
1-Dichloroproperte
23-Trichlorobenzene
23-Trichtoropropane
24-Trtchtorobenzene
24-Tiimothylbenzene
2-Dibromoethane EDB
2-Dichlorobenzene
.2-Dichloroethane
12-Dichioropropane
.35-Trimethylbenzene
I3-Dichlorobenzene
.3-Dichloropropane
14-Diohlorobenzene
22-Dichioropropane
2-Chiorotoluene
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
08/10/07
08/10/07
08/10/07
08/03/07
08/03/07
08/03/07
08/03/07
08/03/07
08/03/07
08/03/07
08/03/07
08/03/07
08/03/07
08103/07
08/03/07
08/03/07
08/03/07
08/03/07
08/03/07
5035
5035
5035
8260B
82605
82608
82608
82605
82608
8260B
8260B
82605
8260B
8260B
82603
8260B
82605
8260B
8260B
82608
8260B
8260B
8260B
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.0050
0.00028
0.00051
0.00031
0.00036
0.00038
0.00044
0.00055
0.00044
0.00048
0.00038
0.00009
0.00027
0.0005
0.00037
0.00042
0.00043
0.00034
0.00039
0.00025
0.00037
1745 Iwitry
1745 Iwitry
1745 Pwitry
1745 Iwit
1745 Iwihy
1745 Iwity
1745 Iwitry
1745 Iwitiy
1745 Iwitry
1745 lwitiy
1745 Iwitry
1745 Iwihy
1745 Iwttry
1745 Iwitry
1745 Iwitry
1745 Iwitry
025514
025514
025514
025514
025514
025514
Q25514
Q25514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
025514
08/03/07 1745 lwitiy
08/03/07 1745 lwitnj
08/03/07 1745 Iwitry
08/03/07 1745 Iwitry
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toil Free Number 1-800/529-6364 Fax [phone] Page of 35
NC Certificati on No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6304 Fax [phone]
Mce Anilytf Cal EiwlraamanW Salullons
ESP Associates PA
RUn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
08/10/07
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 188653
Sample Matrix Soil CCC Group G0807064
Time Collected 08/02/07 930
Time Submitted 08/02/07 1325
Parameter Result Units Report MDL Dilution Method Analyst Batch
ID
Analysis
Limit Factor Date/Time
2-Hexanone BRL mg/kg 0.050 0.00052 8260B 08103/07 1745 lwflry 025514
4-Chiorotoluene BRL mg/kg 0.0050 0.00026 82603 08103107 1745 lw/ky 025514
4-Methyl-2-pentanoneMIBK BRL mg/kg 0.050 0.0005 8260B 08103/07 1745 Iwitry 025514
Acetone BRL mg/kg 0.050 0.0020 8260B 08103107 1745 Iwitry 025514
Benzene BRL mg/kg 0.0030 0.0004 8260B 08/03/07 1745 lwitry 025514
Bromobenzene BRL mg/kg 0.0050 0.00035 8260B 08/03107 1745 Iwitry 025514
Bromochiorornethane BRL mg/kg 0.0050 0.0003 8260B 08/03/07 1745 Iwitry 025514
Bromodichioromethane BRL mg/kg 0.0050 0.00044 8280B 08103/07 1745 Iwitry 025514
Bromoform BRL mg/kg 0.0050 0.00037 8260B 08103/07 1745 witry 025514
Bromornethane BRL mg/kg 0.010 0.00058 8260B 08/03/07 1745 wihy 025514
Carbon tetrachlorido BRL mg/kg 0.0050 0.00029 82603 08/03/07 1745 lwtuy 025514
Chlorobenzene BRL mg/kg 0.0050 0.00038 8260B 08/03/07 1745 Iwitry 025514
Chtorodibromomethane BRL mg/kg 0.0050 0.00034 82603 08103/07 1745 Iwilly 025514
Chloroethane BRL mg/kg 0.010 0.00041 8260B 08103107 1745 1w/ky 025514
Chloroform BRL mg/kg 0.0050 0.00037 82603 08103107 1745 IwiIr 025514
Chloromethane BRL mg/kg 0.0050 0.00035 82603 08/03/07 1145 Iwihy 025514
cis-12-Dichlooethene BRL mg/kg 0.0050 0.00022 8260B 08/03/07 1745 Iwitry 025514
cis-13-Dithloropropene BRL mg/kg 0.0050 0.00032 8260B 08/03/07 1745 lw/ky 025514
Dichlorodifluoromethane BRL mg/kg 0.0050 0.0011 8260B 08/03/07 1745 Iwitry 025514
Ethylbenzene BRL mg/kg 0.0050 0.00035 8260B 08/03/07 1745 lwitry 025514
Isopropyl ether IPE BRL mg/kg 0.0050 0.00017 82603 08/03/07 1745 Iwitry 025514
lsopropylbenene BRL mg/kg 0.0050 0.0004 8260B 08/03/07 1745 lw/ky 025514
mp-Xylenes BRL mg/kg 0.010 0.0007 8260B 08/03/07 1745 twitiy 025514
Methyl ethyl ketone MEK BRL mg/kg 0.10 0.0014 82603 08/03/07 1745 lwttw Q25514
Methyl t-butyl ether MTBE BRL mg/kg 0.010 0.00029 8260B 08/03/07 1745 Iwitry 025514
Methylerie chloride BRL mg/kg 0.0050 0.00041 8260B 08/03/07 1745 Iwitry 025514
n-Butylbenzene BRL mg/kg 0.0050 0.0004 82603 08/03/07 1745 IWitry 025514
Page of 35
FiO $rvke .jiytlCaI o.nnl SoIuUon
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-2
188653
G0807064
08/02/07 930
08/02107 1325
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
08/10/07
Parameter Result Units Report MDL Dilution Method Analyst Batch
ID
Analysis
Limit Factor Date/Time
0.0050 0.0003 82603 08103/07 1745 Iwiliy 025514
0.010 0.00058 82603 0803/07 1745 twftry 025514
0.0050 0.0003 826GB 0803/07 1745 Iwitry Q25514
0.0050 0.00041 82603 08/0307 1745 Iwitry 025514
0.0050 0.00033 826GB 08/0307 1745 Iwitry 025514
0.0050 0.0005 826GB 08/03/07 1745 iwitry 025514
0.0050 0.00031 826GB 08/03/07 1745 Iwitiy 025514
0.0050 0.00086 626GB 08/03/07 1745 Iwitry 025514
0.0050 0.00034 826GB 08/03/07 1745 lwitiy 025514
0.0050 0.00038 826GB 08/03/07 1745 Iwitry Q25514
00050 0.00035 626GB 08/03/07 1745 Iwitry 025514
0.0050 0.0003 826GB 08/03/07 1745 Iwitry 025514
0.0050 0.00041 8260B 08/03/07 1745 Iwitry 025514
0.025 0.0018 82603 08/03/07 1745 lwitiy 025514
0.0050 0.00064 826GB 08/03/07 1745 Iwihy 025514
n-Propylbenzene BRL
Naphthalene BRL
o-Xylene BRL
p-Isopropyltoluene BRL
seo.Butylbenzene BRL
Styrene BRL
tert-Butylbenzene BRL
Tetrachioroethene BRL
Toluene BRL
trans-I 2-Dichloroethene BRL
trans-I .3-Dichioropropene BRL
Trithioroethene BRI
Trichiorofluorornethane BRL
Vinyl acetate BRL
Vinyl chloride BRL
Semi-volatile Organic Compounds by GCIMS
12.4-Tiithlorobenzene BRL
12-Dichlorobenzene BRL
13-Dichlorobenzene BRL
4-Dichlorobenzerte BRL
245-Trithlorophenol BRL
246-Thchlorophenol BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Surrogate Recovery Control Limits
loluene-dB 99 81-128
Dibromofluoromethane 92 67-143
Bromofluorobenzene 108 77-128
0.37
0.37
0.37
0.37
0.37
0.37
0.036
0.027
0.027
0.033
0.038
0.035
82700
82700
82700
8270C
8270C
82700
08/07/07 1457 kcamplgotto
08/07107 1457 kcamplgotto
08/07/07 1457 kcamplgotto
08/07/07 1457 kcampigotto
08/07/07 1457 kampIgotto
08/07/07 1457 koamplgotto
025550
025550
025550
025550
025550
025550
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 10 of 35
NC Certification No 402
SC Certification No 99012
__________
NC Drinking Water Cert No 37735
nIAnatytC1 ElMroimiei54 SQIuIw
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter
24-Dichiorophenol
24.Dimethylphenol
24-Dinitrophenol
24-Dinitmtoluene
26-Olnitrotoluene
2-Chloronaphthalene
2-Chiorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
34-Methylphenol
33-Dichlorobenzidine
46-Dinitro-2-melhylphenol
4-Bromophenyiphenylether
4-Chloro-3-methylphenol
4-Chioroaniline
4-Chiorophenylphenylether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzoaanthracene
Benzoapyrene
Benzobfluoranthene
Benzoghiperylene
Benzokfluorantherie
mg/kg 0.37 0.031
mg/kg 0.37 0.035
mg/kg 1.8 0.041
mg/kg 0.37 0.021
mg/kg 0.37 0.039
mg/kg 0.37 0.038
mg/kg 0.37 0.029
mg/kg 0.37 0.029
mg/kg 0.37 0.034
mg/kg 0.37 0.044
mg/kg 0.37 0.038
mg/kg 0.74 0.023
mg/kg 1.8 0.022
mg/kg 0.37 0.035
mg/kg 0.74 0.027
mg/kg 037 0.047
mg/kg 0.37 0.023
mg/kg 1.8 0.024
mg/kg 0.37 0.036
mg/kg 037 0.037
mg/kg 0.37 0.028
mg/kg 1.8 0.034
mg/kg 0.37 0.051
mg/kg 0.37 0.042
mg/kg 0.37 0.016
mg/kg 0.37 0.017
mg/kg 0.37 0.030
Method Analysis Analyst
Batch
Date/Time ID
08107107 1457 kcampgotto 025550
08/07/07 1457 kcamplgotto 025550
08107107 1457 kcampgotto 025550
08/07/07 1457 kcampigotto 025550
08/07/07 1457 kcamplotto 025550
08/07/07 1457 kcampgotto 025550
08/07/07 1457 kcampigotto 025550
08/07/07 1457 koampigotto 025550
08/07/07 1457 kcampigotto 025550
08/07/07 1457 kcampigotto 025550
08/07/07 1457 koampigotto 025550
08/07/07 1457 kcampigotto 025550
08/07/07 1457 kcamplgotto 025550
08/07107 1457 keamplgotto 025550
08/07/07 1457 kcampigotto 025550
08/07/07 1457 kcampigotto 025550
08/07/07 1457 koampigotto 025550
08/07/07 1457 kcamplgotto 025550
08/07/07 1457 kcamplgotto 025550
08/07107 1457 kcamplgotto 025550
08/07/07 1457 kcamplgotto 025550
08/07/07 1457 kcamplgotto 025550
08/07/07 1457 kcampigotto 025550
08/07/07 1457 kcamplgotto 025550
08/07/07 1457 koampigotto 025550
08107/07 1457 kcampigotto 025550
08/07/07 1457 kcamplgotto 025550
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
Laboratory Report
08/10/07
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 188653
Sample Matrix Soil coo Group G0807064
Time Collected 08/02/07 930
Time Submitted 08/02/07 1325
Result Units Report MDL Dilution
Limit Factor
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRI
BRL
BRL
BRL
BRL
BRL
BRI
BRL
BRL
BRL
BRL
BRL
BRI
BRL
BRL
BRL
BRL
BRI
8270C
827CC
82700
827CC
8270C
82700
827CC
82700
82700
82700
82700
82700
8270C
82700
8270C
82700
82700
82700
82700
82700
82700
82700
82700
82700
82700
8270C
8270C
Page 11 of 35
Laboratory Report
08/10/07
WS-2
188653
G0807064
06/02/07 930
08/02/07 1325
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toil Free Number 1-800/529.6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method Analyst Batch
ID
Analysis
Limit Factor Date/Time
Benzoic acid BRL mg/kg 1.8 0.16 827CC 08/07/07 1457 kcampigotto Q25550
Benzyl alcohol BRL mg/kg 0.74 0.039 827CC 08/07/07 1457 kcampigotto Q25550
Bis2-chioroethoxymethane BRL mg/kg 0.37 0.042 827CC 08/07107 1457 kcampigotto 025550
Bis2-chloroethylether BRL mg/kg 0.37 11040 827CC 08/07/07 1457 kcampiotto Q25550
Bis2-chloroisopropylether BRL mg/kg 0.37 0.031 827CC 08/07/07 1457 kcampigotto 025550
Bis2-ethylhexylphthalate BRL mg/kg 0.37 0.018 827CC 08/07/07 1457 koampigotto Q2555Q
Butylbenzylphthalate SRI mg/kg 0.37 0.023 8270C 08/07/07 1457 kcaniplgotto 025550
Chrysene SRI mg/kg 0.37 0.081 827CC 08/07/07 1457 kcampigotto 025550
Di-n-but1phthaIate BRL mg/kg 0.37 0.017 827CC 08107/07 1457 kcampigotto 025550
Di-n.ootylphthalate SRI mg/kg 0.37 0.027 827CC 08/07/07 1457 kcarnpigotto 025550
Dibenzoahanthracene BRL mg/kg 0.37 0.037 827CC 08/07/07 1457 kcamplgotto 025550
DibenzofUran BRL mg/kg 0.37 0.032 827CC 08107/07 1457 kcarnpigotto 025550
Diethylphthalate SRI mg/kg 0.37 0.023 827CC 08/07/07 1457 kcarnpigotto Q25550
Dimethylphthalate BRL mg/kg 0.37 0.025 827CC 08/07/07 1457 kcampigotto 025550
Fluoranthene BRL mg/kg 0.37 0.025 827CC 08/07/07 1457 kcampigotto 025550
Fluorene BRL mg/kg 0.37 0.022 827CC 08/07/07 1457 kcampiyotto 025550
Hexachlorobenzene BRL mg/kg 0.37 0.019 827CC 08107/07 1457 kcampigotto 025550
Hexachiorobutadiene BRL mg/kg 0.37 0.036 827CC 08107/07 1457 koampigotto 025550
Hexachiorocyclopentadiene BRL mg/kg 037 0.039 827CC 08107/07 1457 kcamplgotto 025550
Hexachioroethane BRL mg/kg 0.37 0.037 827CC 08/07/07 1457 kcampigotto 025550
Indeno123-cdpyrene SRI mg/kg 0.37 0.038 8270C 08107/07 1457 kcampigotto 025550
lsophorone SRI mg/kg 0.37 0.033 827CC 08107/07 1457 kaampigotto 025551
N-Nitrosodi-n-propylamlne SRI mg/kg 0.37 0.042 8270C 08/0707 1457 kcampigotto 025550
N-Nitrosodiphenylamine SRL mg/kg 0.37 0.019 827CC 08/07/07 1457 kcampigotto 025550
Naphthalene BRL mg/kg 0.37 0.040 827CC 08107/07 1457 kcampigotto 025550
Nitrobenzene BRL mg/kg 0.37 0.036 827CC 08107/07 1451 kcarnpigotto 025550
Pentachiorophenol BRL mg/kg 1.8 0.031 827CC 08/07/07 1457 kcampgotto 025650
Page 12 of 35
Laboratory Report
08110/07
WS-2
188653
00807064
08/02/07 930
08/02/07 1325
Sample Preparation 30.32 mL 3550B
11 8.0
Adjusted value
11 1.7
11 3.6
Surrogate
o-Terphenyl
2-Fluorobiphenyl
2-Bromonaphthalene
1-Chloro-octadecane
08/04/07 900 pbarr
Recovery
87
96
99
80
P19082
Control Limits
40-140
40-140
40-140
40-140
This report should not be reproduced except in its entirety thout the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
Parameter Result Units MDL MethodReport
Limit
0.37
0.37
0.37
Dilution
Factor
0.018
0.040
0.025
Analyst Batch
ID
Analysis
Date/lime
08/07/07 1457
08107/07 1457
08107107 1457
8270C
8270C
8270C
kcampigotto
kcampigotto
kcampigotto
025550
Q25550
025550
Surrogate Recovery Control Limits
Terphenyl-d14 74 41-136
Phenol-d5 62 13-95
Nitrobenzene-d5 63 14-103
2-Fluorophenol 57 14 -89
2-Fluorobiphenyl 75 21 108
2.4.6-Tribromophenol 72 25-123
Phenanthrene BRL mg/kg
Phenol BRL mg/kg
Pyrene BRL mg/kg
Extractable Petroleum Hydrocarbons by OC-FID
C11-C22 Aromatics BRL mg/kg
Analysis Note for Cl.-C22 Aromatics
C19-C36 Aliphatics BRL mg/kg
C9-Cl8Alrphancs BRL mg/kg
Sample Preparation
Metals by
Chromium
Lead
MADEP EPH 08/07/07 2251 grappaccioll 025548
MADEP EPH
MADEP EPI-l
10.1 2mL
08107/07 2251 grappaccloll
08/07/07 2251 grappaccioli
EPH 08/03/07 700 pbarr
025548
025548
P19081
18 mg/kg 0.28 0.016 60106 08/03/07 2022 mcampbell 025521
56 mg/kg 0.28 0.018 601GB 08/03/07 2022 mcampbeli 025521
Page 13 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
08/10/07
WS-2
188653
00807064
08/02/07
08102/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Sample Preparation 2.01 50 mL 30503 08103107 745 dthxon P19078
Volatile Petroleum Hydrocarbons by GC-PIDIFID
C5-C8Aliphafics BRL mg/kg 5.6 1.1 MADEPVPH 08/077 515 hwagn 025565
Analysis Note for C5-C8 Aliphatics Adjusted value
C9-Cl0Aromallcs BRI mg/kg 5.6 0.034 MADEPVPH 08/07/07 515 hwagner Q25565
C9C12AIiphafics BRL mg/kg 5.6 1.7 MADEP VPH 08/07/07 515 hwagner Q25565
Analysis Note for C9-C12 Aliphatics Adjusted value
Surrogate Recovery Control Limits
25-Dlbromotoluene-PID 99 70 130
25-Dibromotoluene-FID 102 70-130
SamDle Weight Determination
Weight 22.04 MADEP VPH 08/08/07 000 lbrown
Weight 18.22 MADEP VPH 08/08/07 000 Ibrown
Sample Comments
I3RL Below Reporting Limit
J-Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthoseinstances indicated fr the case narrative and/or test comments
All results are reported on dy-weight basis
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
_______
FUll leAn1ytlC1l EiwTronmntISthfllan
Project ID Morehead Commons No
Sample Matrix Soil
Client Sample ID
Prism Sample ID
COC Group
Time Collected
Time Submitted
930
1325
Angela Overcash V.P Laboratory Services
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 14 of 35
NC CertifIcation No.402 Laboratory ReportScCortMcationNo99012
NC Drinking Water Cert No 37735 08110/07
Project ID Morehead Commons Nb Client Sample ID WS-3
Prism Sample ID 188654
Sample Matrix Soil COG Group G0807064
Time Collected 08/02/07 945
Time Submitted 08/02/07 1325
Percent Solids Determination
Percent Solids
5035
5035
5035
08/10/07 000 Ibrown
08110/07 000 lbtown
08/10/07 000 Ibrown
Volatile Organic compounds by GCIMS
lj1-Trlchloroethane
1.1 22-Tetrachioroethane
12-Trichloroethane
1-Dichloroethane
1-Dichloroethene
.1-Diclilompropene
12.3-Tiichlorobenzene
23-Trichboropropane
24-Trichlorobenzene
24-Trimethyibenzene
2-Dibromoetharie EDB
2-DicbIorobenzne
2-Dichloroethane
2-Dichloropropane
135-Trim ethylbenzene
3-Dichlorobenzene
3-Dichloropropane
4-Dichlorobenzene
2.2-Dichioropropane
2-Chiorotoluene
08103/07 1829 Iwitty
08103/07 1829 Iwitry
080307 1829 Iwhy
08103/07 1829 lwitry
08103/07 1829 Iwitry
08103/07 1829 Iwitry
0803/07 1829 lwitiy
08/03/07 1829 twiby
08/03/07 1829 twiby
08/03/07 1829 Iwiby
025514
Q25514
025514
Q25514
025514
025514
025514
Q25514
025514
025514
_____
Full S.vluMaly1ical Enn...IuI Solullurs
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Sample Weight Determination
Weight Bisulfate
Weight Bisulfate
Weight Methanol
88.2
5.88
5.79
5.23
SM2540 08/03/07 1555 ddixon
08/03/07 1829 twitry 025514
08/03/07 1829 Iwitry 025514
08/03/07 1829 Iwitry 025514
08/03/07 1829 lwitiy 025514
08/03/07 1829 lwitiy 025514
08/03/07 1829 Iwitry 025514
08/03/07 1829 Jwitjy Q25514
08/03/07 1829 IwlIjy 025514
0803/07 1829 Iwifry 025514
08/03107 1829 Iwitry 025514
BRL mg/kg 0.0048 0.00027 82609
BRL mg/kg 0.0048 0.00049 82609
BRL mg/kg 0.0048 0.0003 8260B
BRL mg/kg 0.0048 0.00035 8260B
BRL mg/kg 0.0048 0.00037 82608
BRL mg/kg 0.0048 0.00042 82609
BRL mg/kg 0.0048 0.00053 82609
BRL mg/kg 0.0048 0.00042 8260B
BRL mg/kg 0.0048 0.00046 8260B
BRL mg/kg 0.0048 0.00037 8260B
BRL mg/kg 0.0048 0.000087 82608
BRL mg/kg 0.0048 0.00026 826DB
BRL mg/kg 0.0048 0.00048 8260B
BRI mg/kg 0.0048 0.00036 82603
BRL mg/kg 0.0048 0.0004 82609
BRL mg/kg 0.0048 0.00041 8260B
BRL mg/kg 0.0048 0.00033 826DB
BRL mg/kg 0.0048 0.00038 82609
BRL mg/kg 0.0048 0.00024 8260B
BRL mg/kg 0.0048 0.00036 82603
This report should not be reproduced except in its entirety without the written consent Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240548 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 15 of 35
Fufl
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte N/C 28241
Laboratory Report
08/1 0/07
WS-3
188654
G0807064
08/02/07 945
08/02/07 1325
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories inc
449 Spiingbrock Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6304 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
2-Hexanone BRL mg/kg 0.048 0.0005 826GB 03/0307 1829 Iwb Q25514
4-Chiorotoluene BRL mg/kg 0.0048 0.00025 826GB 08/03/07 1829 Iwitry 025514
4-Methyl-2-pentanone MIBK BRL mg/kg 0.048 0.00048 826GB 03/03/07 1829 iwitiy 025514
Acetone BRL mg/kg 0.048 0.0019 826GB 08/0307 1829 iwitry 025514
Benzene BRL mg/kg 0.0029 0.00039 826GB 08/0307 1829 Iwltry 025514
Brornobenzene BRL mg/kg 0.0048 0.00034 826GB 08/03/07 1829 Iwitry 025514
Bromochioromethane BRL mg/kg 0.0048 000029 826GB 08/03/07 1829 Iwitry 025514
Bromodichioromethane BRL mg/kg 0.0048 0.00042 82609 08/03/07 1829 iwitry Q25514
Bromoform BRL mg/kg 0.0048 0.00036 826GB 08/03/07 1329 Iwitry 025514
Bromomethane BRL mg/kg 0.0096 0.00056 826GB 08/03/07 1829 Iwitry 025514
Carbon telrachloride BRL mg/kg 0.0048 0.00028 826GB 08/03/07 1829 Iwitry 025514
Chlorobenzene BRL mg/kg 0.0048 0.00037 826GB 08/03/07 1829 Iwitry 025514
ChlorodibromomeUiane BRL mg/kg 0.0048 0.00033 826GB 08/03/07 1829 Iwitry 025514
Chioroethane BRL mg/kg 0.0096 0.0004 826GB 08/03/07 1829 Iwitry 025514
Chloroform BRL mg/kg 0.0048 0.00036 826GB 08/03/07 1829 Iwitry 025514
Chioroniethane BRL mg/kg 0.0048 0.00034 826GB 08/03/07 1829 Iwitry 025514
cis-12-Dichloroethene BRL mg/kg 0.0048 0.00021 826GB 08/03/07 1829 Iwitry Q25514
cis-13-Dichloropropene BRL mg/kg 0.0048 0.00031 826GB 08/03/07 1829 iwity 025514
Dichlorodifluommethane BRL mg/kg 0.0048 0.0011 826GB 08/03/07 1829 witry 025514
Ethylbenzene BR1 mg/kg 0.0048 0.00034 826GB 08/03/07 1829 lwitiy 025514
Isopropyl ether IPE BRI mg/kg 0.0048 0.00016 826GB 08/03/07 1829 Iwiby 025514
isopropylberizene BRL mg/kg 0.0048 0.00039 826GB 08/03/07 1829 Iwitiy 025514
mp-Xylenes BRL mg/kg 0.0096 0.00067 826GB 03/03/07 1829 lwitsy 025514
Methyl ethyl ketone MEK BRL mg/kg 0.096 0.0013 826GB 08/03/07 1829 Iwitry 025514
Methyl t-butyl ether MTBE BRL mg/kg 0.0096 0.00028 826GB 08/03/07 1829 twitry 025514
Methylene chloride BRL mg/kg 0.0048 0.0004 826GB 08/03/07 1829 Iwifry 025514
n-Butylbenzene BRL mg/kg 0.0048 0.00039 826GB 08/03/07 1829 Iwihy 025514
Page 16 of 35
FL...ccAflaIyUc.EMronmN3oi.Jori
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
08/10/07
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 188654
Sample Matrix Soil COC Group 00807064
Time Collected 08/02/07 945
Time Submitted 08/02/07 1325
Parameter Result Units Report MDL Dilution Method AnalystAnalysis Batch
Limit Factor DatelTime ID
0.0048 0.00029 8260B 08/03107 1829 Iwitry 025514
0.0096 0.00056 826GB 08/03/07 1829 Iwitry 025514
0.0048 0.00029 82608 08/03/07 1829 Iwitiy 025514
0.0048 0.0004 826DB 08/03107 1829 iwitry 025514
0.0048 0.00032 82606 08/03I07 1829 Iwitry 025514
0.0048 0.00048 82606 08I03/07 1829 Iwitry 025514
0.0048 0.0003 826DB 08103/07 1829 Iwihy 025514
0.0048 0.00083 8260B 08103/07 1829 Iwitry 025514
0.0048 0.00033 826DB 08103/07 1829 lwftry 025514
0.0048 0.00037 82603 08/03/07 1829 twitry 025514
0.0048 0.00034 82608 08103/07 1829 Iwitry 025514
0.0048 0.00029 8260B 08/03/07 1829 Iwitry 025514
0.0048 0.0004 826DB 08/03/07 1829 lwitiy 025514
0.024 0.0017 826DB 08/03/07 1829 Iwitry 025514
0.0048 0.00062 826DB 08/03/01 1829 witry Q25514
n-Propylbenzene BRL
Naphthalerie BRL
o-Xylene BRL
p-lsopropyltoluene BRL
sec-Butylbenzene BRL
Styrene BRL
tert-Butylbonzene BRL
Tetrachioroethene BRL
Toluene BRL
trans-I 2-Dichloroethene BRL
trans-I 3-Dichloropropene BRL
Ttichloroethene BRL
Ttichlorofluoromethane BRL
Vinyl acetate BRL
Vinyl chloride BRL
Semi-volatile Organic Compounds by GC/MS
124-Trichlorobenzene BRL
12-Dichorobenzerie BRL
3-Dlchlorobenzene BRL
4-Dichlorobenzere BRL
245-Trichiorophenci BRL
246-Trichiorophenol BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Surrogate Recovery Control Limits
Toluenc-d8 97 81 128
Dibromofluoromethane 97 67-143
Bromoflujorobenzene 106 77-128
0.37
0.37
0.37
0.37
0.37
0.37
0.037
0.027
0.027
0.034
0.038
0.036
8270C
8270C
82700
8270C
8270C
8270C
08/07/07 1834 kcamplgotlo
08/07/07 1834 kcamplgotto
08/07/07 1834 kcamplgolto
08/07/07 1834 keamplgotto
08/07107 1834 kcamplgotto
08/07/07 1834 kcamplgotto
Q25550
025550
Q25550
Q25550
025550
025550
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road PA Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1400/529-6354 Fax [phone] Page 17 of 35
Fuil SkAnydClEwJronmr
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
This report should not be reproduced except in its entirety without the written consent or Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
08110/07
Project ID Morehead Commons No Cilent Sample ID WS-3
Prism Sample ID 188654
Sample Matrix Soil COO Group G0807064
Time Collected 08/02/07 945
Time Submitted 08/02/07 1325
Parameter Result Units Report MDL Dilution Method
Limit
Analyst Batch
ID
Analysis
Factor Date/Time
24-Dichiorophenol BRL mg/kg 0.37 0.031 82700 0810707 1834 Iccampfgotto Q25550
24-Dimethylphenol BRL mg/kg 0.37 0.036 8270C 08/07/07 1834 kcampigotto Q2555
24-Dinitrophenol BRL mg/kg 1.9 0.042 8270C 08/07/07 1834 kcampigotto 025550
24-Dinitrotoluene BRL mg/kg 0.37 0.021 8270C 08/07/07 1834 kcampigotto 025550
2.6-Dinitrotoluene BRL mg/kg 0.37 0.040 8270C 08/07/07 1834 kcampigotto 025550
2-Chloronaphthalene BRL mg/kg 0.37 0.038 827CC 08/07/07 1834 koampigotto 025550
2-Chiorophenol BRL mg/kg 0.37 0.029 827CC 08/07/07 1834 kcampigotto 025550
2-Methylnaphthalene BRL mg/kg 0.37 0.030 827CC 08107/07 1834 kcampigotto 025550
2-Methylphenot BRL mg/kg 0.37 0.035 827CC 08/07/07 1834 kcampigotto 025550
2-Nitrophenot BRL mg/kg 0.37 0.045 8270C 08/07/07 1834 kcampigotto 025550
34-Methylphenol BRL mg/kg 0.37 0.038 8270C 08/07107 1834 kcamplgotto 025550
33-Dlchlorobenzldlne BRL mg/kg 0.75 0.023 82700 08/07/07 1834 koampigotto 025550
46-Dinhtro-2-methylphenol BRL mg/kg 1.9 0.023 82700 08/07/07 1834 koampigotto 025550
4-Bromophenyiphenylether BRL mg/kg 0.37 0.035 82700 08/07/07 1834 kcampigotto 025550
4-Chloro-3-methylphenol BRL mg/kg 0.75 0.027 82700 08/07/07 1834 kcampigotto 025550
4Chloroanillne BRL mg/kg 0.37 0.048 8270C 08/07/07 1834 kcampigotto 025550
4ChlorophenylphenyIether BRL mg/kg 0.37 0.023 8270C 08/07/07 1834 kcampigotto 025550
4-Nitrophenol BRL mg/kg 1.9 0.025 8270C 08/07/07 1834 kcampigotto 025550
Acenaphthene BRL mg/kg 0.37 0.037 82700 08/07/07 1834 keamplgolto 025550
Acenaphthylene BRL mg/kg 0.37 0.037 8270C 08/07/07 1834 kcampigotto 025550
Anthracene BRL mg/kg 0.37 0.028 827CC 08/07/07 1834 koamplgotto 025550
Azobenzene BRL mg/kg 1.9 0.035 8270C 08107/07 1834 kcampigotto 025550
Benzoaanthracene 0.10 mg/kg 0.37 0.052 82700 08/07/07 1834 kcamplgotto 025550
Benzoapyrene BRL mg/kg 0.37 0.043 827CC 08/07/07 1834 koampigotto 025550
Benzobfluoranthene BRL mg/kg 0.37 0.011 82700 08/07/07 1834 kcampigotto 025550
Benzoghipetylene BRL mg/kg 0.37 0.018 8270C 08/07/07 1834 kcampigotto 025550
Benzokfluoranthene BRL mg/kg 0.37 0.030 82700 08107/07 1834 kcamplgotto 025550
Page 18 of 35
Laboratory Report
08/10107
WS-3
188654
00807064
08/02/07 945
08/02/07 1325
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Spilngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method
Limit Factor
Analyst Batch
ID
Analysis
Date/Time
Benzoic acid BRL mg/kg 1.9 0.16 8270C 08/07/07 1834 kcamplgotto 025550
Benzyl alcohol BRL mg/kg 0.75 0.039 8270C 08/07/07 1834 kcampigotto 025550
Bis2-chloroethoxymetharie BRL mg/kg 0.37 0.043 82700 08/0707 1834 kcamplgotto Q25550
Bis2-chloroethylether BRL mg/kg 0.37 0.041 8270C 08/07107 1834 kcampigotto 025550
Bis2-chlcroisopropylether BRL mg/kg 0.37 0.032 82700 08/07107 1834 kcampigotto 025550
Bis2-ethylhexylphthatate BRL mg/kg 0.37 0.018 82700 08/07107 1834 koampigotto 025550
Butylbenzylphthalate BRL mg/kg 0.37 0.023 82700 0810707 1834 kcampigotto 025550
Chrysene Oil mg/kg 0.37 0.062 8270C 08/07/07 1834 kcampigotto 025550
Di-n-buylphthalate BRL mg/kg 0.37 0.017 8270C 08101/07 1834 kcamplgotto 025550
DI-n-oct1phtha1ate BRL mg/kg 0.37 0.028 8270C 08/07/07 1834 kcampigotto 025550
ljibenzoahanthracene BRL mg/kg 0.37 0.037 827CC 08/07107 1834 kcamplgotto 025550
Dibenzofuran BRL mg/kg 0.37 0.032 8270C 08/07/07 1834 kcampigotto 025550
Diethylphthalate BRL mg/kg 0.37 0.023 827CC 08/07/07 1834 kcampigotto 025550
Dimethylphthalate BRL mg/kg 0.37 0.025 82700 08/07107 1834 koampigotto 025550
Fluoranthene 0.25 mg/kg 0.37 0.026 82700 08/07/07 1834 kcampigotto 025550
Fluorene BRL mg/kg 0.37 0.022 82700 08/0707 1834 kcampigotto 025550
Hexachlorobenzene BRL mg/kg 0.37 0.019 82700 08/0707 1834 kcampgoflo 025550
Hexachtorobutadiene ML mg/kg 0.37 0.036 8270C 0807/07 1834 kcampigotlo 025550
Hexachlorocyclopentadiene BRL mg/kg 0.37 0.039 82700 08/07/07 1834 kcamplgotto 025550
Hexachioroethane BRL mg/kg 0.37 0.038 8270C 08/07/07 1834 kcamplgotb 025550
lndeno123_cdpyrene BRL mg/kg 0.37 0.038 82700 08/07/07 1834 kcampigotto 025550
Isophorone BRL mg/kg 0.37 0033 82700 08/07/07 1834 kcampigotto 025550
N-Nitrosodi-n-propylamine BRL mg/kg 0.37 0.042 827CC 08/07/07 1834 kcampigotto 025550
N-Nitrosodiphenylamine BRL mg/kg 037 0.019 8270C 08/07/07 1834 kcampigotto 025550
Naphthalene BRL mg/kg 0.37 0.041 8270C 08/07/07 1834 kcampigctto 025550
Nitrobenzene BRL mg/kg 0.37 0.036 827CC 08/07/07 1834 kcamplgotto 025550
Pentachiorophenol BRL mg/kg 1.9 0.031 8270C 08/07/07 1834 kcamplgotto 025550
Page 19of35
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
SrvkoMaIyc.I EzwJrnii..
ESP Associates PA Project ID
Attn Chris Ward
Box 7030
Charlotte NC 28241
Extractable Petroleum Hydrocarbons by GC-FID
Cl 1-022 Aromatics BRL mg/kg
Analysis Note for Cll-C22 Aroniatics
Cl 9-036 Aliphatics BRL mg/kg
C9-C18 Aliphatics BRL mg/kg
Sample Preparation
Surrogate
o-Terphenyl
2-Fluorobiphenyl
2-Bromonaphthaene
1-Chioro-octadecane
Recovery
94
90
96
90
Control Limits
40-140
40-140
40-140
40-140
Metals by ICP
Chromium
Lead
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrqok Road P.O Box 240543-Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6354 Fax [phone]
Laboratory Report
08110107
Sample Matrix Soil
Morehead Commons No Client Sample ID
Prism Sample ID
COC Group
Time Collected
Time Submitted
WS-3
188654
G0807064
08/02/07 945
08/02/07 1325
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Phenanthrene 0.17 mg/kg 0.37 0.018 8270C 08/07/07 1834 kcampigotto 025550
Phenol BRL mg/kg 0.37 0.041 8270C 08/07/07 1834 kcampiotto 025550
Pyreno 0.21 mg/kg 0.37 0.025 8270C 08/07/07 1834 kcamplgotto Q25550
Sample Preparation 30.06 mL 3550B 08/04/07 900 pbarr P19082
Surrogate Recovery Control Limits
Terphenyl-di4 78 41 136
Phenol-d5 59 13-95
Nitrobenzene-d5 63 14-103
2-Fluómphenol 61 14-89
2-Fluorobiphenyl 75 21 -108
246-Tiibramophenol 81 25 123
11 6.2 MADEP EPH 08108/07 035 grappaccoU 025548
Adjusted value
11 1.7 MADEP EPH 08/08/07 035 grappacclot Q25548
11 3.7 MADEP EPH 08/08107 035 grappacclot 025548
9.89 mL EPH 08/03/07 700 pbarr P19081
18 mg/kg 0.28 0.016 6010B 08/03/07 2029 mcampbell 026521
100 mg/kg 0.28 0.018 6010B 08/03/07 2029 mcampbell 025521
Page 20 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
08/10/07
WS-3
188654
G0807064
08102107 945
08/02/07 1325
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Sample Preparation 1.99 50 mL 3050B 08/03/07 745 ddixon P19078
VtatiIe Petroleum Hydrocarbons by GC-PID/FID
C5-C8 ftJiphabcs BRL mg/kg 5.7 1.1 MADEP VPH 08107/07 558 tiwagner 025565
nalysis Note for CS-Ca Aliphatics Adjusted value
C9.Cl0komatics BRL mg/kg 5.7 0.034 MADEP VPH 08/07/07 558 hwagner Q25565
C9-C1 Aliphalics BRL mg/kg 5.7 1.7 MADEP VPH 08/07/07 558 tiwagner 025565
nalyais Note for C9-Cl2 Aliphatics Adjusted value
Surrogate Recovery Control LimIts
25-Dibromotoluene-PID 97 70-130
25-Dibromotoluene-FID 104 70-130
SamDle Weight Determination
Weight 21.95 MADEP VPH 08108/07 000 brown
Weight 16.95 MADEP VPH 08/08/07 000 brown
Sample Comments
BRL Below Reporting Urnit
J-Estimated value between the Reporting Limit and the MDL
The results in this report relate only/a the samples submitted fbr analysis and meet state certification requirements other thanNELAGcertificationexceptforthose instances indicated in the case narrative and/or test comments
All results are reported on dry-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except In its entirety thout the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
FiII 5Mco AiitytIcaI EnFronmntI So4uU
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Page 21 of 35
NC Certification No 402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735 08110/07
Project ID Morehead Commons No Client Sample ID WS-4
Prism Sample ID 188655
Sample Matrix Soil COC Group 00807064
Time Collected 08/02/07
Time Submitted 08/02/07
Percent Solids Determination
Percent Solids
5035
5035
5035
08110107 000 brown
08110/07 000 brown
08110/07 000 brown
ESP Associates PA
Attn Chris Ward
Box 7030
Chatiotte NC 28241 1000
1325
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Dateflime ID
88.7
5.91
6.42
5.51
SM2540 08103/07 1555 ddixon
Sample Weight Determination
Weight Bisulfate
Weight Bisulfate
Weight Methanol
Volatile Organic Compounds by GC/MS
111-Trichloroethane BRL mg/kg 0.0044 0.00025 826GB 08/03/07 1912 Iwitry Q25514
1122-Tetrachioroethane BRL mg/kg 0.0044 0.00045 82608 08/03/07 1912 Iwitiy 025514
112-Trichloroethane BRL mg/kg 0.0044 0.00027 82608 08/03/07 1912 Iwilry 025514
11-Dichioroethane BRL mg/kg 0.0044 0.00032 8260B 08/03/07 1912 Iwitry 025514
11-Dichioroethene SRL mg/kg 0.0044 0.00034 82603 08/03/07 1912 twiUy 025514
11-Dichioropropene BRL mg/kg 0.0044 0.00039 82608 08103/07 1912 lwitnj Q25514
123-Thchlorobenzene BRL mg/kg 0.0044 0.00049 8260B 08103/07 1912 Iwitry 025514
123-Trichioropropane BRL mg/kg 0.0044 0.00039 82603 08/03/07 1912 Iwitry 025514
124-Trichforobenzene BRL mg/kg 0.0044 0.00042 82603 08/03/07 1912 Iwitry 025514
l24-Trimethylbenzene BRL mg/kg 0.0044 0.00034 8260B 08/03/07 1912 Iwitry Q25514
12-Dibromoethane EDB BRL mg/kg 0.0044 0.00008 82603 08103/07 1912 lwftr 025514
12-Dlchlorobenzene BRL mg/kg 0.0044 0.00024 8260B 08/03/07 1912 Iwiby 025514
12-Dichioroethane BRL mg/kg 0.0044 0.00044 826GB 08/03/07 1912 lwitjy 025514
12-Dichioropropane BRL mg/kg 0.0044 0.00033 826GB 08/03/07 1912 lwitiy 025514
13.5-Trimethylbenzene BRL mg/kg 0.0044 0.00037 826GB 08/03/07 1912 IwliJy 025514
13-Dlchlorobenzene BRL mg/kg 0.0044 0.00038 826GB 08103/07 1912 Iwihy 025514
13-Dichioropropane BRL mg/kg 0.0044 0.0003 826GB 08/03/07 1912 lwitiy 025514
4-Dichlorobenzene BRL mg/kg 0044 00034 826GB 08/03/07 19 12 lwdry 025514
22-Dichioropropane BRL mg/kg 0.0044 0.00022 826GB 08/03/07 1912 Iwitry 025514
2-Chlorotolueno BRL mg/kg 0.0044 0.00033 826GB 08/03/07 1912 iwitry 025514
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224.0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 22 of 35
Laboratory Report
08/10/07
WS-4
188655
00807064
08/02/07 1000
08/02/07 1325
This report should not be repmduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6354 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cerl No 37735
FuIISocM
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COO Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method AnalystAnalysis Batch
Limit Factor Date/Time ID
2-Hexanone BRL mg/kg 0.044 0.00046 8260B 08/03/07 1912 lwitry 025514
4-Chlorotoluene BRL mg/kg 0.0044 0.00023 82608 08/03/07 1912 Iwitry Q25514
4-Methyl-2-pentanone MIBK BRL mg/kg 0.044 0.00044 8260B 08/03/07 1912 Iwitiy 025514
Acetone SRL mg/kg 0.044 0.0017 826DB 08/0307 1912 Iwihy 025514
Benzene BRL mg/kg 0.0027 0.00035 8260B 08/03/07 1912 twitry 025514
Bromobenzene SRI mg/kg 0.0044 0.00031 826DB 08/03/07 1912 lwitiy 025514
Bromochloromethane BRL mg/kg 0.0044 0.00027 826DB 08/03/07 1912 Iwity 025514
Bromodichioromethane BRL mg/kg 0.0044 0.00039 826DB 08/03/07 1912 Iwitry 025514
Bromoform BRL mg/kg 0.0044 0.00033 826DB 08/03/07 1912 Iwitry 025514
Bromomethane SRI mg/kg 0.0088 0.00051 826DB 08/03/07 1912 lwftiy 025514
Carbon tetrachioride BRL mg/kg 0.0044 0.00026 826DB 08/0307 1912 Iwitry 025514
Chlorobenzene BRL mg/kg 0.0044 0.00034 826DB 08103/07 1912 Iwitry 025514
Chlorodibromornethane BRL mg/kg 0.0044 0.0003 82608 08/03/07 1912 Iwitry 025514
Chioroethane SRI mg/kg 0.0088 0.00036 826DB 08/0307 1912 twitiy 025514
Chloroform BRL mg/kg 0.0044 0.00033 826DB 08/0307 1912 Iwihy 025514
Chioromethane BRL mg/kg 0.0044 0.00031 826DB 08/03/07 1912 iwitry 025514
cis-12-Dichloroethene BRL mg/kg 0.0044 0.00019 826DB 08/03/07 1912 lwiky 025514
cis-13-Dichloropropene BRL mg/kg 0.0044 0.00028 826DB 08/03/07 1912 Iwitry 025514
Dichiorodifluoromethane BRL mg/kg 0.0044 0.00099 82608 08/03/07 1912 lwitri 025514
Ethylbenzene BRL mg/kg 0.0044 0.00031 82608 08/03/07 1912 Iwitry 025514
Isopropyl ether IPE SRL mg/kg 0.0044 0.00015 826DB 08/03/07 1912 IWitry 025514
lsopropylbenzene BRL mg/kg 00044 0.00035 82608 08/03/07 1912 Iwitry 025514
mp-Xylenes SRI mg/kg 0.0088 0.00062 826DB 08/03/07 1912 willy 025514
Methyl ethyl ketoneMEK SRI mg/kg 0.088 0.0012 826DB 08103/07 1912 Iwitry 025514
Methyl t-butyl ether MTBE BRL mg/kg 0.0088 0.00026 826DB 08103/07 1912 Cwitty 025514
Methylene chloride SRI mg/kg 0.0044 0.00036 826DB 08/03/07 1912 Iwitry 025514
n-Butylbenzene BRL mg/kg 0.0044 0.00035 826DB 08/03/07 1912 Iwitry 025514
Page 23 of 35
Full Sov3c alydcI EnyI
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
0811 0/07
WS-4
188655
G0807064
08/02/07 1000
08/02/07 1325
NC Certificaon No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrbc Soil COG Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Date/Time IDLimitFactor
0.0044 0.00027 8260B 08/03/07 1912 lwitsy Q25514
0.0088 0.00051 8260B 08/03/07 1912 Fwitn 025514
0.0044 0.00027 826GB 08/03/07 1912 Iwitry 025514
0.0044 0.00036 826GB 08/03/07 1912 lwity 025514
0.0044 0.00029 8260B 08/03/07 1912 lwitiy 025514
0.0044 0.00044 826GB 08/03/07 1912 iwitry Q25514
0.0044 0.00027 826GB 08/03/07 1912 lwitiy 025514
0.0044 0.00076 82608 08/03/07 1912 Iwitiy 025514
0.0044 0.0003 8260B 08/03/07 1912 Iwitry 025514
0.0044 0.00034 826GB 08/03/07 1912 Iwitry 025514
0.0044 0.00031 826GB 08/03/07 1912 Iwitry 025514
0.0044 0.00027 826GB 08/03/07 1912 Iwitry 025514
00044 0.00036 8260B 08/03/07 1912 lwitry 025514
0.022 0.0016 8260B 08103/07 1912 Iwitry 025514
0.0044 0.00057 826GB 08/03/07 1912 iwitry 025514
n-Propylbenzene BRL
Naphthalene BRL
o-Xylene BRL
p-lsopropyltoluene BRL
sec-Butylbenzene BRL
Styrene BRL
tert-Butylbenzene BRL
Tetrachioroethene BRL
Toluene BRL
trans-I 2-Dichloroethene BRL
trans-I 3-Dichloropropene BRL
Ttichlcroethene BRL
Trichlorofluoromethane BRL
Vinyl acetate BRL
Vinyl chloride BRL
Semi-volatile Organic Corn nou nds by GC/MS
24-Trichtorobenzene BRL
2-Dichlorobenz BRL
3-Dichlorobenzene BRL
4.Dichlorobenzeno BRL
245-Trichlorophenol BRL
246-Trichlorophenol BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Surrogate Recovery Control Limits
Toluene-d8 97 81 128
Dibromofluorornethane 93 67-143
Bromoftuorobenzene 109 77-128
0.37
0.37
0.37
0.37
0.37
0.37
0.037
0.027
0027
0.033
0.038
0.035
8270C
8270C
8270C
8270C
8270C
8270C
08/07/07 1553 kcamplgotto
08/07/07 1553 kcamplgotto
08/07/07 1553 keamplgotto
08/07/07 1553 kcamplgotto
08/07/07 1553 kcamptgotto
08/07/07 1553 kcamplgotto
025550
025550
025550
025550
025550
025550
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 24 of 35
NC Certification No 402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735 08/10/07
Project ID Morehead Commons to Client Sample ID WS-4
Prism Sample ID 188655
Sample Matrix Soil COC Group 00807064
Time Collected 08/02/07 1000
Time Submitted 08/02/07 1325
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1400/529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method AnalystAnalysis Batch
Limit Factor Date/Time ID
24-Dichiorophenol BRL mg/kg 0.37 0.031 82700 08/07/07 1553 kampigotto 025550
24-Dimethylphenol SRL mg/kg 037 0.036 82700 08/07/07 1553 kcampigotto 025550
24-Dinilrnphenol SRI mg/kg 1.8 0.042 8270C 08/07/07 1553 kcempgotto 025550
24-Dinitrotoluene BRL mg/kg 0.37 0.021 82700 08/07/07 1553 kcampigotto 025550
26-Dinitrotoluene BRL mg/kg 0.37 0.039 8270C 06/07/07 1553 koampigotto 025550
2-Chloronaphthalene BRL mg/kg 0.37 0038 82700 08/07/07 1553 koampigotto Q25550
2-Chiorophenol BRL mg/kg 0.37 0.029 82700 0807/07 1553 kcampigotto 025550
2-Methylnaphthalene BRL mg/kg 0.37 0.029 82700 08/07/07 1553 kcampigotto 025550
2-Methyiphenol BRL mg/kg 0.37 0.035 82700 08/07/07 1553 kcarnplgotto 025550
2-Nitrophenol BRL mg/kg 0.37 0.044 8270C 08/07/07 1553 kcampigotto 025550
34-Methytphenol BRI mg/kg 0.37 0.038 82700 0807/07 1553 kcampgotto 025550
33-Dichlorobenzidine BRL mg/kg 0.74 0.023 82700 0807/07 1553 kcampigotto 025550
46-Dinitm-2-methylphenol BRL mg/kg 1.8 0.022 82700 08/07/07 1553 kcampigotto 025550
4-Bromophenyiphenylether BRL mg/kg 0.37 0.035 82700 08/07/07 1553 kcamplgotto 025550
4-Chloro-3-methylphenol BRI mg/kg 0.74 0.027 82700 08107/07 1553 kcamplgotto 025550
4-Chioroaniline SRI mg/kg 0.37 0.047 82700 08/07/07 1553 kcampigotto 025550
4-Chlorophenyiphenylether BRL mg/kg 0.37 0.023 82700 08/07/07 1553 kcamplgotto 025550
4-Nitrophenol SRI mg/kg 1.8 0.025 82700 08/07107 1553 kcarnplgotto 025550
Acenaphthene BRL mg/kg 0.37 0.036 8270C 08/07/07 1553 koamplgotto 025550
Acenaphthylene BRL mg/kg 0.37 0.037 8270C 08/07107 1553 kcamplgotto 025550
Anthracene BRI mg/kg 0.37 0.028 82700 08/07/07 1553 kcamptgotto 025550
Azobenzene BRL mg/kg 1.8 0.034 8270C 08/07/07 1553 kcampigotto 025550
Benzoaanthracene 0.IGJ mg/kg 0.37 0.052 82700 08/07/07 1553 kcampigotto 025550
Benzoapyreno 0.14J mg/kg 0.37 0.043 8270C 08107/07 1553 koamplgofto Q25550
8enzobfiuoranthene 0.14 mg/kg 0.37 0017 8270C 08/07/07 1553 kcamplgotto 025550
8enzoghiperylene BRL mg/kg 0.37 0.018 8270C 08/07/07 1553 kcampigotto 025550
Benzokfluoranthene 0.17J mg/kg 0.37 0.030 82700 06/07/07 1553 kcampigotto 025550
Page 25 of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
lime Submitted
WS-4
188655
G0807064
08/02/07 1000
08/02/07 1325
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224.0543
Phone [phone] Toll Free Number 1-800/529-6354 Fax [phone]
k..SiAnIy-Ofl1ronmailI SpIons
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
08/10/07
Parameter Result Units Report MDL Dilution Method Analyst Batch
ID
Analysis
Limit Factor Date/Time
Benzoic acid BRL mg/kg 1.8 0.16 82700 08107107 1553 1camiotto 025550
Benzyf alcohol BRL mg/kg 0.74 0.039 827CC 08/07/07 1553 kcampigotto Q25551
Bis2-chloroethoxyrnethane BRL mg/kg 0.37 0.042 8270C 08/07/07 1553 kCSmpigOtto Q25550
Bis2-chloroethylether BRL mg/kg 0.37 0.040 827CC 08/07/07 1553 kcamplgotto 025550
Bis2-chloroisopropylether BRL mg/kg 0.37 0.032 827CC 08/07/07 1553 kcrnplgotto 025550
Bis2-ethylhexylphthalate BRL mg/kg 0.37 0.018 8270C 08/07/07 1553 kcampigotto 025550
Butylbenzylphthalate BRL mg/kg 0.37 0.023 82700 08/07107 1553 kcampigotto 025550
Chrysene 0.14 mg/kg 0.37 0.061 8270C 08107/07 1553 kcamplgotto 025550
Di-n-butylphthalate BRL mg/kg 0.37 0.017 8270C 08/07/07 1553 kcampigotto 025550
Di-n-octylphthalate BRL mg/kg 0-37 0.028 8270C 08/07107 1553 kcampigotto 025550
Dibenzoahanthracene BRL mg/kg 0.37 0.037 82700 08/07/07 1553 kvampIgctto 025550
Dibenzofuran BRL mg/kg 0.37 0.032 8270C 08/07107 1553 kcampigotto Q25550
Dlethylphthalate BRL mg/kg 0.37 0.023 827CC 08107/07 1553 kcampigotto 025550
Dimethylphthalate BRL mg/kg 0.37 0.025 82700 08/07/07 1553 kcamplgotto 025550
Fluoranthene 0.36 mg/kg 0.37 0.025 827CC 08/07/07 1553 kcampigotto 025550
Fluorene BRL mg/kg 0.37 0.022 82700 08/07/07 1553 kcamplgotto 025550
Hexachlorobenzene BRL mg/kg 0.37 0.019 82700 08/07/07 1553 kcamplgotto 025550
Hexachiorobutadiene BRL mg/kg 0.37 0.036 82700 08/07/07 1553 kcampigotto 025550
Hexachlomcyclopentadiene BRL mg/kg 0.37 0.039 82700 08/07/07 1553 kcamplgotto 025550
Hexachioroethane BRL mg/kg 0.37 0.038 82700 08107/07 1553 kcamplgotto 025550
Indeno1 .23-Gdpyrene BRL mg/kg 0.37 0.038 82700 08/07/07 1553 kcamplgofto 025550
Isophorone BRL mg/kg 0.37 0.033 82700 08/07/07 1553 kcampigotto 025550
N-Nilrosodl-n.propylamine BRL mg/kg 0.37 0.042 827CC 08/07/07 1553 kcampigotto 025550
N-Nitrosodlphenylamine BRL mg/kg 0.37 0.019 82700 08/07/07 1553 kcamplgotto 025550
Naphthslene BRL mg/kg 0.37 0040 8270C 08/07/07 1553 kcampigctto 025550
Nitrobenzene BRI mg/kg 0.37 0.036 821CC 08/07/07 1553 kcsmpigotto 025550
Pentachlorophenol BRL mg/kg 1.8 0.031 827CC 08/07/07 1553 kcamplgotto 025550
Page 26 of 35
SMeMaIytCaI Enmenu5u1on
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil CCC Group
Time Collected
Time Submitted
WS-4
188655
G0807064
08/02/07 1000
08/02/07 1325
Sample Preparation 30.22 mL 3550B 08104107 900 pbarr P19082
Exiractabte Petroleum Hydrocarbons by GC-FID
C11-C22 Aromatics 15 mg/kg
xia1ysis Note for C11-C22 Aromatics
C19-C36 Aliphatics BRL mg/kg
C9-Cl8Aliphatics BRL mg/kg
Sample Preparation
Surrogate
o-Terphenyl
2-Fluorobiphenyl
2-Brorncnaphthalene
1-Chloro-octadecane
Recovery
102
97
102
85
Control LImits
40-140
40-140
40-140
40-140
23 mg/kg
150 mg/kg
0.28 0.016 60103
0.28 0.018 60108
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012 Laboratory Report
NC Drinking Water Cert No 37735 08/10/07
Parameter Result Units MDL MethodReport Analysis Batch
Limit Date/Time ID
Phenanthrene 0.28 mg/kg 0.37 0.018 8270C 08/07/01 1553 kcampigotto 025550
Phenol BRL mg/kg 0.37 0.040 8270C 08/07/07 1553 kcampigotto Q2555Q
Pyrene 0.33 mg/kg 037 0.025 8270C 08/07/07 1553 kcamplgotto 025550
Dilution
Factor
Analyst
Surrogate fo Recovery Control Limits
Terphenyl-d14 82 41-136
Phenol-dS 56 13-95
Nitrobenzene-d5 65 14 103
2-Fluorophenol 69 14-89
2-Flucitbiphenyl 70 21 108
2.46-Tribromophenol 81 25 123
11 6.0 MADEP EPH 08108/07 403 grappaccloll 025548
Adjusted value
11 1.7 MADEP EPH 08/08/07 403 grappaccloli 025548
11 3.5 MADEP EPH 08/08/07 403 grappacclotl 025548
10.18 mL EPH 08/03107 700 pbar P19081
Metals by
Chromium
Lead
08/03/07 2036 mcampbell
08/03/07 2036 mcampbell
025521
025521
Page 27 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
08/10/07
WS-4
188655
00807064
08/02/07 1000
08/02/07 1325
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Sample Preparation 2.02 50 mL 3050B 08103101 745 ddixon P19078
Volatile Petroleum Hydrocarbons by GC-PIDIFID
C5-C8 Aliphatics BRL mg/kg 5.6 1.1 MADEP VPH 08/07/07 641 hwagner 025565
Analysie Note for C5-C8 A.iphatics Adjusted value
C9-C10 Aromatics BRL mg/kg 5.6 0.034 MADEP VPH 08/07/07 641 hwagner Q25565
C9-Cl2Aliphatics BRI mg/kg 5.6 1.7 MADEPVPH 08/07/07 641 hwagner Q25565
Analysis Note for C9-C12 Aliphatics Adjusted value
Surrogate Recovery Control Limits
25-Dibromotoluene-PID 82 70-130
25-Dibromotoluene-FID 94 70-130
Sample Wektht Determination
WeIght 16.74 MADEP VPI-I 08108/07 000 brown
Weight 20.11 MADEP VPH 08108/07 000 Ibrown
Sample Comments
BRL Below Reporting Limit
J-Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthose instances indicated in the case narrative and/or test comments
All results are reported on dr/-weight basis
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 -Charlotte NC 2224-0543
Phone [phone] Toll Free Number 1-8001529-6354 Fax [phone]
Full ivlca Anahjlf Cal Envfrouiwoep SuJutluns
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Angela Overcash V.P Laboratory Services
Page 28 of 35
NC Certification No 402
SC Certification No 99012 Laboratoty Report
NC Drinking Water Cert No 37735 08110107
Project ID Morehead Commons No Client Sample 1D B1
Prism Sample ID 188656
Sample Matrix Soil COC Group G0807064
Time Collected 08/02/07 1015
Time Submitted 08/02/07 1325
Percent Solids Determination
Percent Solids
5035
5035
5035
08110/07 000 brown
0310/07 000 brown
08110/07 000 thrown
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
88.9 SM2540 08/03/07 1555 ddixon
Samnie Weight Determination
Weight Bisulfate 5.31
Weight Bisulfate 5.57
Weight Methanol 4.91
Volatile Organic Compounds by GC/MS
1Il-TrichIoroethane SRI mg/kg 0.0052 0.00029 826GB 08/03/07 1955 lwitry 025514
1122-Tetrachioroethane BRL mg/kg 0.0052 0.00053
8260B 08/03/07 1955 Iwitry 025514
112-Trichioroethane BRL mg/kg 0.0052 0.00032 82508 08/03/07 1955 Iwitry 025514
11-Dichloroethane BRL mg/kg 0.0052 0.00037 82608 08/03/07 1955 itry 025514
11-Dichloroethene BRL mg/kg 0.0052 0.00039 82608 08/03/07 1955 Iwitry 025514
11-Dichioropropene BRL mg/kg 0.0052 0.00045 826GB 08/03/07 1955 witty 025514
23-Tiichlorobenzene BRL mg/kg 0.0052 0.00057 826GB 08/03/07 1955 witty 02551
123-Trichioropropane BRL mg/kg 0.0052 0.00045 82608 08/03/07 1955 witty 025514
124-Trichlorobenzene BRL mg/kg 0.0052 0.00049 82508 08/03/07 1955 it 025514
124-Trimethylbeozene BRL mg/kg 0.0052 0.00039 82608 08103/01 1955 Iwitry 025514
12-Dibromoethane EDS BRL mg/kg 0.0052 0.000093 826GB 08/03/07 1955 Iwitry Q25514
12-Dichlorobenzene BRL mg/kg 0.0052 0.00028 82608 08/0307 1955 Iwitry 025514
12-Dichloroethane BRL mg/kg 0.0052 0.00052 82608 0803/07 1955 Iwitry 025514
12-Dichioropropane BRL mg/kg 0.0052 0.00038 82508 08/03/07 1955 Iwitry Q25514
135-Trimethbenzene BRL mg/kg 0.0052 0.00043 82608 0303107 1955 025514
13-Dichlcrobenzene BRL mg/kg 0.0052 0.00044 82608 0803/07 1955 witty 025514
13-Dichloropropane BRL mg/kg 0.0052 0.00035 82608 08/0307 1955 lwhy 025514
14-Dichlorobenzene BRL mg/kg 0.0052 CL0004 826GB 08/03/07 1955 Iwitry 025514
22-Dichloropropane BRL mg/kg 0.0052 0.00026 82608 08/03/07 1955 Iwilty 025514
2-Chiorotoluene BRL mg/kg 0.0052 0.00038 826GB 08/03/07 1955 witri 025514
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543-Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800529-6364 Fax [phone] Page 29 of 35
Project 1D Morehead Commons No Client Sample ID B-i
Prism Sample ID 188656
Sample Matiix Soil COC Group 00807064
Time Collected 08102107 1015
lime Submitted 08/02/07 1325
This report should not be reproduced except in Its enhirety without the written consent of Prism Laboratories Inc
449 Spzlngbrook Road P.O Box 240543.Charlotte NC 28224-0543
Phone [phone] ToIl Free Number 1-8001529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012 Laboratonj Report
NC Drinking Water Cerl No 37735 0810/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Daternme IDLimitFactor
2-Hexanone BRL mg/kg 0.052 0.00054 826GB 08/03/07 1955 Iwitry 025514
4-Chiorotoluene BRL mg/kg 0.0052 0.00027
826GB 08/03/07 1955 Iwitfy 025514
4-Methyl-2-pentanone MIBK BRL mg/kg 0.052 0.00052 826GB 08/03/07 1955 Iwitry 025514
Acetone SRI mg/kg 0.052 0.0020 82603 08/03/07 1955 lwitzy 025514
Denzene BRL mg/kg 0.0031 0.00041
82603 08103/01 1955 Iwitiy Q25514
Bromobenzene BRL mg/kg 0.0052 0.00036
82603 08103/07 1955 Iwitry Q25514
Bromochloromethane BRL mg/kg 0.0052 0.00031 82603 08103/07 1955 IWitry 025514
Bromodichioromethane BRL mg/kg 0.0052 0.00045 8260B 0803/07 1955 twitrY 025514
Bromoform BRL mg/kg 0.0052 0.00038 82603 0803/07 1955 Iwitry 025514
l3romomethane BRL mg/kg 0.010 0.0006 82603 08103/07 1955 Iwitri 025514
Carbon tetrachlortde BRL mg/kg 0.0052 0.0003 82603 08/03/07 1955 Iwihy 025514
Chlorobenzene BRL mg/kg 0.0052 0.00039 82603 08/03/07 1955 lwitiy 025514
Chiorodibromomethane BRL mg/kg 0.0052 0.00035 82603 08/03/07 1955 Iwiby 025514
Chioroethane BRL mg/kg 0.010 0.00042 82603 08/03/07 1955 lwitiy 025514
Chloroform BRL mg/kg 0.0052 0.00038 826GB 08/03/07 1955 Iwitiy 025514
Chioromethane BRL mg/kg 0.0052 0.00036 8260B 06/03/07 1955 Iwitry 025514
cis-12-Dichloroethene BRL mg/kg 0.0052 0.00023 826GB 0803/07 1955 Iwitrt 025514
cls-13-Dichloropropene SRI mg/kg 0.0052 0.00033 82603 08/03/07 1955 Iwitry 025514
Dichiorodifluoromethane BRL mg/kg 0.0052 0.0012 826GB 08/03/07 1955 Iwifry 025514
Ethylbenzene BRL mg/kg 0.0052 0.00036 826GB 08/03/07 1955 twitry 025514
Isopropyt ether IPE SRI mg/kg 0.0052 0.00018 826GB 08/03/07 1955 twitw 025514
Isopropylbenzene BRL mg/kg 0.0052 0.00041 82603 08/03/07 1955 twitry 025514
mp-Xylenes SRI mg/kg 0.010 0.00072 82603 08/03/07 1955 Iwitry Q25514
Methyl ethyl ketone MEK BRL mg/kg 0.10 0.0014 826GB 08/03/07 1955 Iwitry 025514
Methyl t-butyl ether MTBE BRL mg/kg 0.010 0.0003 826GB 08/03/07 1955 lwitry 025514
Methylene chloride BRL mg/kg 0.0052 0.00042 826GB 0803/07 1955 Iwitry 025514
n-Butylbenzene BRL mg/kg 0.0052 0.00041 82603 0803/07 1955 twitry 025514
Page 30 of 35
Laboratory Report
08/10/07
Project ID Morehead Commons No Client Sample ID B-I
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
NC Certillcation No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
188656
G0807064
08/02/07 1015
08/02/07 1325
Parameter Result Units Report MDL Dilution Method AnalystAnalysis Batch
Limit Factor Date/Time ID
0.0052 0.00031
826DB 08/03/07 1955 iwitry 025514
0.010 0.0006
826DB 08/03/07 1955 twitry Q2551
0.0052 0.00031 82608 08/03/07 1955 twitry 025514
0.0052 0.00042
826DB 08/03/07 1955 Iwitry 025514
0.0052 0.00034 8260B 0803/07
1955 witty 025514
0.0052 0.00052
826DB 0803/07 1955 Iwilty 025514
0.0052 0.00032 826DB 08103/07 1955 Iwitiy 025514
0.0052 0.00089 82608 08/03/07 1955 Iwitry 025514
0.0052 0.00035 826DB 08/03/07 1955 Iwitry 025514
0.0052 0.00039 82608 08/03/07 1955 Iwitry 025514
0.0052 0.00036 826DB 08103/07 1955 twitry 025514
0.0052 0.00031 826DB 08/03/07 1955 twilty Q25514
0.0052 0.00042 826DB 08/03/07 1955 twilry Q25514
0.026 0.0019 826DB 08/03/07 1955 twiby Q2551
0.0052 0.00066
82608 0803/07 1955 Iwitry 025514
n-Propylbenzene BRL
Naphthalene BRL
o-Xylene BRL
p-isopropyttoluene BRL
sec-Butylberzene BRL
Styrerie BRL
tert-Butylbenzene BRL
Tetrachioroethene BRL
Toluene BRL
trans-i 2-Dichtoroethene BRI
trans-I 3-Dichloropropene BRL
Trichioroethene BRL
Trichiorofluoromethane BRL
Vinyl acetate BRL
Vinyl chloride BRL
Semi-volatile Organic Compounds by GC/M$
t24-Trtchlorobenzene BRL
12-Dichlorobenzene BRL
3-Dichlorobenzene BRL
4-Dichlorobenzene BRL
245-Trithlorophenol BRL
246-Trichiorophenol BRI
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Surrogate Recovery Control Limits
Toluene-d8 95 81-128
Dibromofluoromethane 94 67-143
Bromofluorobenzene 103 77-128
0.37
0.37
0.37
0.37
0.37
0.37
0.037
0.027
0.027
0.033
0.038
0.036
8270C
8270C
8270C
8270C
8270C
8270C
08/07/07
08/07/07
08/07107
08/07/07
08/07107
08/07/07
1307 kcamplgotto
1307 kcampigotlo
1307 kcamptgotto
1307 kcamptgotto
1307 kcamplgotto
1307 keamplgotto
025550
Q25550
025550
Q25550
025550
025550
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529.6364 Fax [phone] Page 31 of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Pull Survke Aiulytlcal uonnionbl 801u110n5
ESP Associates PA Project ID
Attn Chris Ward
P.O.Box7030
Charlotte NC 28241
This report should not be reproduced except in its entirety without the written consent of Prism Labomtories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224.0543
Phone [phone] Toll Free Number 1400/529-6364 Fax [phone]
Laboratory Report
08/1 0/07
Sample Matrix Soil
Morehead Commons No Client Sample ID
Prism Sample ID
COC Group
Time Collected
lime Submitted
B-I
188656
G0807064
08102/07 1015
08/02/07 1325
Parameter Result Units Report MDL Dilution Method AnalystAnalysis Batch
Limit Factor Date/Time ID
24.Dichlorophenot BRL mg/kg 0.37 0.031 8270C 08107/07 1307 kcampigotto Q25550
24-Dimethyiphenol BRL mg/kg 0.37 0.036 827CC 08/07/07 1307 kcampigotio 025550
4-Dinitrophenol BRL mg/kg 1.9 0.042 827CC 08/07/07 1307 kcampigotto 025550
24-Dinifrotoluene BRL mg/kg 0.37 0.021 827CC 08/07/07 1307 kcampigotlD 025550
26-Dinitrotoluene BRL mg/kg 0.37 0.039 827CC 08/07/07 1301 kcamplgotto Q25550
2-Chtoronaphthalene BRL mg/kg 0.37 0.038 827CC 08/07/07 1307 kcampigotto 025550
2-Chlorophenol BRI mg/kg 0.37 0.029 827CC 08/07/07 1307 kcampigctlo Q25550
2-Methylnaphthalene BRL mg/kg 0.37 0.030 8270C 08/07/07 1307 kcampigotto 025550
2-Methyiphenol BRL mg/kg 0.37 0.035 8270C 08/07/07 1307 kcamplgotto 025550
2-Nitrophenol BRI mg/kg 0.37 0.044 827CC 08/07/07 1307 kcampiotto 025550
34-Methylphenot SRI mg/kg 0.37 0.038 827CC 08/07/07 1307 kcampigotto 025550
33-Dlchlorobenzidlne SRI mg/kg 0.74 0.023 827CC 08107/07 1307 kcampigotto 025550
46-Dinitro-2-methylphenol BRI mg/kg 1.9 0.023 827CC 08/07/07 1307 kcampigotto 025550
4-Bromophenyiphenylether SRI mg/kg 0.37 0.035 827CC 08/07/07 1307 kcampioUo 025550
4.Chloro.methylphenol BRL mg/kg 0.74 0.027 827CC 08/07/07 1307 kcampi9otto 025550
4-Chioroaniline SRI mg/kg 0.37 0.047 827CC 08/07/07 1307 kcamplgotto 025550
4-Chlorophenyiphenylether SRI mg/kg 0.37 0.023 827CC 08/07/07 1307 kcaxnplgotto 025550
4-Nitrophenot BRL mg/kg 1.9 0.025 827CC 08/07/07 1307 kcamplgotto 025550
Acenaphthene BRL mg/kg 0.37 0.036 827CC 08/07/07 1307 kcamptgollo 025550
Acenaphthylene BRL mg/kg 0.37 0.037 821CC 08/07/07 1307 kcamplgotto 025550
Anthracene SRI mg/kg 0.37 0.028 827CC 08/07/07 1307 kcamplgotto 025550
Azobenzene BRL mg/kg 1.9 0.034 827CC 08/07/07 1307 kcampigotto 025550
Benzoaanthracene SRI mg/kg 0.37 0.052 827CC 08/07/07 1307 kcamplgotto 025550
Benzoapyrene BRL mg/kg 0.37 0.043 827CC 08/07/07 1307 kcamplgotto 025550
Benzobfluoranthene BRL mg/kg 0.37 0.017 827CC 08/07/07 1307 kcamplgotto 025550
Benzoghlperylene BRL mg/kg 0.37 0.018 827CC 08/07/07 1307 kcarnpigotlo 025550
Benzokfiuoranthene BRL mg/kg 0.37 0.030 827CC 08/07/07 1307 kcampigotto 025550
Page 32 of 35
Laboratory ReportScCertilicationNo99012
NC Drinking Water Cert No 37735 08/10/07
Project ID Morehead Commons No Client Sample ID B-i
Prism Sample ID 188656
Sample Matrix Soil COG Group G0807064
Time Collected 08/02/07 1015
Time Submitted 08/02/07 1325
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 23224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Date/lime IDLimitFactor
Benzoio acid BRL mg/kg 1.9 0.16 8270C 08/07/07 1307 kcampigofto Q25551
Benzyl alcohol BRL mg/kg 0.74 0.039 8270C 08/07/07 1307 kcampigotto 025550
Bis2-chloroethoxymethane BRL mg/kg 0.37 0.043 8270C 08/07/07 1307 kcampigotto 025550
Bis2-chloroethylether BRL mg/kg 0.37 0.040 8270C 08/07/07 1307 kcamplgotto 025550
Bis2chIoroisoprupyIether BRL mg/kg 0.37 0.032 8270C 08/07/07 1307 kcampigotto 025550
Bis2-ethylhexylphthalate BRL mg/kg 0.37 0.018 8270C 08J07107 1307 kcampigotto 025550
Butylbenzylphthalate BRL mg/kg 037 0.023 8270C 08/07/07 1307 kcampigotto 025550
Chrysene BRL mg/kg 0.37 0.062 8270C 08/07/07 1307 kcampigotto Q25550
Di-n-butyiphthalate BRL mg/kg 0.37 0.017 8270C 08/07/07 1307 kcarnplgotto 025550
Di-n-octylphthalate BRL mg/kg 0.37 0.028 -1 8270C 08/07/07 1307 kcampigotto 025550
Dibenzoahanthracene BRL mg/kg 0.37 0.037 8270C 08/07/07 1307 kcamplgotto 025550
Dibenzofuran BRL mg/kg 0.37 0.032 8270C 08/07/07 1307 kcamplgotto Q25550
Dlethylphthalate BRL mg/kg 0.37 0.023 8270C 08107/07 1307 kcamplgotto 025550
Dimethylphthalate BRL mg/kg 0.37 0.025 8270C 08/07/07 1307 Iccampigotto Q25550
Fluoranthene BRL mg/kg 0.37 0.026 8270C 08/07/07 1307 kcampigotto 025550
Fluorene BRI mg/kg 037 0.022 8270G 08/07/07 1307 kcanipigotto Q25550
Hexachlorobenzene BRL mg/kg 0.37 0.019 8270C 08/07/07 1307 kcampigotto 025550
Hexachiorobutadiene BRL mg/kg 0.37 0.036 8270C 08/07/07 1307 kcampigotto 025550
Hexachiorocyclopentadiene BRL mg/kg 0.37 0.039 8270C 08/07/07 1307 kcamplgotto 025550
Hexachioroethane BRL mg/kg 0.37 0.038 8270C 08/07/07 1307 kcamplgotto 025550
lndeno123-cdpyrene BRL mg/kg 0.37 0.038 8270C 08/07/07 1307 keampigotto 025550
Isophorone BRL mg/kg 0.37 0.033 8270C 08/07/07 1307 kcampigotto 025550
N-Nitrosodin-propylamine BRL mg/kg 0.37 0.042 8270C 08/07/07 1307 koamplgotto 025550
N-Nitrosodlphenylamine BRL mg/kg 0.37 0.019 8270C 08/07/07 1307 kcamplgotto 025550
Naphthalene BRL mg/kg 0.37 0.040 8270C 08/07/07 1307 koamplgotto 025550
Nitrobenzene BRL mg/kg 0.37 0.036 827CC 08/07/07 1307 kcamplgotto 025550
Pentachiorophenol BRL mg/kg 1.9 0031 8270C 08/07107 1307 kcamplgotto 025550
Page 33 of 35
wvlco AnaIytIC1 nv1ronmonI
SMons
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
08/10/07
188656
G0807064
08102/07 1015
08/02/07 1325
Sample Preparation
Sample Preparation
30g lmL 3550B
1O.07g 2mL
08/04/07 900 pbarr
EPH 08/03107 700 pbarr
P19082
P19081
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364-Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID B-I
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units MDL MethodReport
Limit
0.37
0.37
0.37
Dilution
Factor
0.018
0.040
0.025
Analyst Batch
ID
8270C
8270C
8270C
Analysis
Date/Time
08/07/07 1307 keampigotto
08/07101 1307 kcampigotto
08/07/07 1307 kcampigotto
025550
025550
Q25550
Surrogate Recovery Control Limits
Terphenyl-d14 76 41 136
Pheno-d5 70 13-95
Nitrobenzene-d5 72 14-103
2-Huorophenol 78 14-89
2-Fluorobiphenyl 73 21 -108
246Tnbromophenol 86 25-123
Phenanthrene BRL mg/kg
Phenol BRL mg/kg
Pyrene BRL mg/kg
Extractable Petroleum Hydrocarbons by GC-FlD
Cl 1-C22 Aromatics BRL mg/kg
Analysis Note for Cll-C22 Aromatics
C19-C36Aliphatics BRL mg/kg
C9-Cl8AliphaUcs BRL mg/kg
Metals bylCP
Chromium
Lead
11 6.0
Adjusted value
11 1.7
11 3.6
MADEP EPH 08/08/07 547 grappaccf oil Q25548
MADEP EPH
MADEP EPH
08/08/07 547 grappaccloil
08/08/07 547 grappaccloll
025548
025548
Surrogate Recovery Control Limits
o-Terphenyt 73 40-140
2-Fluorobiphenyl 81 40-140
2-Bromonaphthalene 84 40-140
1-Chloro-octadecane 75 40-140
24 mg/kg 0.28 0.016 6010B 08/03/07 2044 mcampbell 025521
98 mgkg 0.28 0.018 60103 08/03/07 2044 nlcampbeil 025521
Page 34 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
08110/07
188656
G0807064
08/02107 1015
08102107 1325
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Sample Preparation 1.98 50 mL 30508 08/03/07 745 ddixon P19078
Volatile Petroleum Hydrocarbons by GC-PIDFIO
C5-C8 Aliphatlos BRL mg/kg 5.6 1.1 MADEP VPH 08/07/07 724 hwagner 025565
Analysis Note for C5-C8 Aliphatics Adjusted value
C9-C1O Aromatics BRL mg/kg 5.6 0.034 MADEP VPH 08/07/07 724 hwllgner 025565
C9-C12 Aliphatlcs BRL mg/kg 5.6 1.7 MADEP VPH 08/07/07 724 hwagner 025565
Analysis Note for C9-C12 Aliphatics Adjusted value
Surrogate Recovery Control Limits
25-Dibromotoluerie-PID 96 70-130
25-Dibromotoluene-FID 104 70-130
Sample Weight Determination
Weight 21.79 MADEP VPH 08/08/07 000 Ibrown
WeIght 20.04 MADEP VPH 08/08107 000 Ibrown
Sample Comments
BRL Below Reporting Limit
J-Estimated value between the Reporting Limit and the MDL
The results In this report relate only to the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthose Instances Indicated In the case naira five andlor test comments
All results are reported on dry-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Full Sorvku Analytical EnYIFOnmnW Solutlona
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID B-I
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Phone [phone] Toll Free Number 1-800529-6364 Fax [phone] Page 35 of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
ii coAnaIydc2t Eiiv1mmmnt1 Su1Ion
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte1 NC 28241
Level II QC Report
8/10107
Project ID Morehead Commons No COO Group Number G0807064
Date/Time Submitted 8/2/07 1325
JIIitn rginb rIpK .Th....l QAD
Method Blank QQBatth
Result RL Control Limit Units ID
1-Tiictiloroethane ND 0.005 0.0025 mg/kg 025514
1I22-Tetrachloroethane ND 0.005 0.0025 mg/kg Q25514
lj2-Trichloroethane ND 0.005 0.0025 mg/kg 025514
11-Dichioroethane ND 0.005 0.0025 mg/kg Q25514
ti-Dichloroethene ND 0.005 0.0025 mg/kg Q25514
11-Dichioropropene ND 0.005 0.0025 mg/kg 025514
23-Tdchlorobenzene ND 0.005 0.0025 mg/kg 025514
123-Trichioroproparie ND 0.005 00025 mg/kg 025514
124-Trichlorobenzene ND 0.005 0.0025 mg/kg 025514
24-Thmethylbenzene ND 0.005 0.0025 mg/kg 025514
2-Dibromoethane EDB ND 0.005 0.0025 mg/kg 025514
12-Dichlorobenzene ND 0.005 0.0025 mg/kg 025514
12-Dichioroethane ND 0.005 0.0025 mg/kg 025514
12-Dichioropropane ND 0.005 0.0025 mg/kg 025514
35-Trimethylbenzene ND 0.005 0.0025 mg/kg 025514
13-Dichlorobenzene ND 0.005 0.0025 mg/kg 025514
13-Dichioropropane ND 0.005 0.0025 mg/kg 025514
4-Dichlorobanzeno ND 0.005 0.0025 mg/kg 025514
22-Dichioropropane ND 0.005 0.0025 mg/kg 025514
2-Chiorotoluene ND 0.005 0.0025 mg/kg 025514
2-Hexanone ND 0.05 0.025 mg/kg 025514
4-Chiorotoluene NI 0.005 0.0025 mg/kg 025514
4-Methyt-2-pentanone MIBK ND 0.05 0.025 mg/kg 025514
Acetone ND 0.05 0.025 mg/kg 025514
Beozene ND 0.003 0.0015 mg/kg 025514
Bromobenzene ND 0.005 0.0025 mg/kg Q25514
Bromochloromethane ND 0.005 0.0025 mg/kg Q25514
Bromodichtoromethane ND 0.005 0.0025 mg/kg 025514
Bromoform ND 0.005 0.0025 mg/kg 025514
Bromomethane ND 0.01 0.005 mg/kg 025514
Carbon tetrachlotjde ND 0.005 0.0025 mg/kg Q25514
Chlorobenzene ND 0.005 0.0025 mg/kg 025514
Chlorodibromornethane ND 0.005 0.0025 mg/kg 025514
Chforoethane ND 0.01 0.005 mg/kg 025514
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SprlngbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] ToIl Free Number 1.800/529.6354 Fax [phone] Page of8
Level II QC Report
8/1 0/07
Prolect ID Morehead Commons No COG Group Number 00807064
Date/Time Submitted 8/2/07 1325
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SprlngbrookRoadP.O Box 240543 Charlotte MC 28224.0543
Phone [phone] Toll Free Number 1-500/529-6364 Fax [phone]
Fiu qAn wknmonbJ SIutIn5
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Method Blank 06 Batch
Resull RL Conhzal Umi Units ID
Chloroform ND 0.005 0.0025 mg/kg Q25514
Chloromethane ND 0.005 0.0025 mg/kg 025514
cia-I 2-Dichloroethene ND 0.005 0.0025 mg/kg 025514
cis-13-Dichloropropene ND 0.005 0.0025 mg/kg 025514
Dichiorodifluoromethane ND 0.005 0.0025 mg/kg 025514
Ethylbenzene ND 0.005 0.0025 mg/kg 025514
Isopropyl ether IPE ND 0.005 0.0025 mg/kg 025514
lsopropylbenzene ND 0.005 0.0025 mg/kg 025514
mp-Xylenes ND 0.01 0.005 mg/kg 025514
Methyl ethyl ketone MEK ND 0.1 0.05 mg/kg 025514
Methyl t-butyl ether MTBE ND 0.01 0.005 mg/kg 025514
Methylene chloride ND 0.005 0.0025 mg/kg 025514
n.Butylbenzene ND 0.005 0.0025 mg/kg 025514
nPropylbenzene ND 0.005 0.0025 mg/kg 025514
Naphthalene ND 0.01 0.005 mg/kg 025514
o-Xylene ND 0.005 0.0025 mg/kg Q25514
p-lsopropyltoluene ND 0.005 0.0025 mg/kg 025514
sec-Butylbenzene ND 0.005 0.0025 mg/kg 025514
Slyrene ND 0.005 0.0025 mg/kg 025514
tert-Butylbenzene ND 0.005 0.0025 mg/kg 025514
Teirachlorriethene ND 0.005 0.0025 mg/kg 025514
Toluene ND 0.005 0.0025 mg/kg Q25514
trans-12-Dichloroethene ND 0.005 0.0025 mg/kg 025514
trans-13-Dichloropropene ND 0.005 0.0025 mg/kg 025514
Ttichloroethene ND 0.005 0.0025 mg/kg 025514
Trichiorofluaromethane ND 0.005 0.0025 mg/kg 025514
Vinyl acete MD 0.025 0.0125 mg/kg 025514
Vinyl chloride ND 0.005 0.0025 mg/kg 025514
Laboratory Control Sample
Result Spike Amount
11-Diohloroethene
Benzene
Chlorobenzerie
Toluene
Trichioroetherie
Recovery Recovey
RangesUnits
0.05119
0.044
0.0478
0.05135
0.0605
0.05
0.05
0.05
0.05
0.05
OC Batch
ID
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
102
88
96
103
121
57-122
62-119
61 -1 24
57-1 22
59-129
025514
Q25514
025514
025514
025514
Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 2822I-0543
Phone [phone] Toil Free Number 1-800/529-6364 Fax [phone]
Full Savlce kiulyItct Ewtroemontal Soluttens
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No
Level II QC Report
8/10/07
COC Group Number G0807064
Date/Time Submitted 8/2107 1325
Matrix Spike Recovery Recovery
Ranges QOBatch
Sample ID Result SpikeAmount Units
188597 11-Dichloroethene 0.05093 0.05 mg/kg 102 44.140 025514
Benzene 0.04675 0.05 mg/kg 94 46-136 025514
Chlombenzene 0.04796 0.05 mg/kg 96 47-1 35 025514
Toluene 004701 0.05 mg/kg 94 47-1 36 025514
Trlchloroethene 0.0499 0.05 mg/kg 100 45-141 025514
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range QC Batch
Sample ID
Result Spike Amount Units ID
188597 11-Dichloroetherie 0.04928 0.05 mg/kg 99 44-140 0-23 025514
Benzene 0.04467 0.05 mg/kg 89 46-136 -22 025514
Chlorobenzene 0.04666 0.05 mg/kg 93 47-135 0-22 025514
Toluene 0.04496 0.05 mg/kg 90 47-136 0-22 Q25514
Trichloroethene 004657 0.05 mg/kg 93 45-141 0-23 025514
Metals by ICP method 601GB
Method Blank DC Batch
Result RL Control Limit Units ID
Chromium 0.0186 0.25 0.125 mg/kg 025521
Lead 0.0268 0.25 0.125 mg/kg 025521
Laboratory Control Sample Recovery Recovery
Ranges DC Batch
Result Spike Amount Units ID
Chromium 22.4199 25 mg/kg 90 80-120 025521
Lead 22.7376 25 mg/kg 91 80-120 025521
Matrix Spike Recovery Recovety
Ranges QC BelchSampleIiResultSpikeAmountUnIts
188652 Chromium 31.0259 25.380 mg/kg 46 75-125 025521
Lead 132.172 25.380 mg/kg 142 75-125 025521
Matrix Spike Duplicate Recovery Recovery RPD
ReIChesRPDReSampleIDResultSpikeAmountUnitsRaID
188652 Chromium 40.6402 24.630 mg/kg 87 75-1 25 27 0-20 025521
Lead 96.9916 24.630 mg/kg 75-125 31 0-20 025521
Page of
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No
Level II QC Report
8110107
COG Group Number G0807064
Date/Time Submitted 812/07 1325
Pvfr1ihle Pprthuim Wutir mrhn by GC-FlD method MADEP EPH
Method Blank OC Batch
Result RL Control tjmlt Units IL
Cl 1-C22 Aromatics ND 10 mg/kg 025548
C19-C36Pjiphatics ND 10 mg/kg 025548
C9-Cl8Aliphatlcs ND 10 mg/kg Q25548
Laboratory Control Sample Revovey Recovery QO BatchRangesResultSpikeAmountUnits1k
C11-C22Aromatics 140.38 170 mg/kg 83 40-140 025548
C19-C36Aiphatics 54.74 80 mg/kg 68 40-140 025548
C9-Cl8Aliphalics 30.28 60 mg/kg 50 40-140 025548
Matrix Spike Recovery Recovery
Ranges OCBatcl
Sample ID Result Spike Amount Units ID
188424 Cl 1-C22 Aromatics 131.86 170 mg/kg 78 40-1 40 025548
C19-C36Aliphatics 69.68 80 mg/kg 87 40-140 025548
C9-ClBAIiphatics 37.14 60 mg/kg 62 40-140 025548
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range CC Batch
Sample ID Result Spike Amount Untts ID
188424 C11-C22Aromaffcs 124.02 170 mg/kg 73 40-140 0-50 025548
C19-C36 Atiphatics 51.52 80 mg/kg 64 40-1 40 30 0-50 025548
C9-C18 Aliphatics 28.66 60 mg/kg 48 40-140 26 -50 025548
This report should not be reproduced except in its entirety without the written nsent of Prism Laboratories Inc449SprlngbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
ESP Associates PA
Attn Chris Ward
O.Box7030
Charlotte NC 28241
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
24-Trichlorobenzene
12-DichIorobenzene
13-Dichlorobenzene
14-Dichlorobenzene
Z45-Tnchlorophenol
2.46lrichlorophenol
2.4-Didlorophenol
24-Dimethylphenol
24-Dinitrophenol
24-Dinitrotoluene
26-Dinitiotoluene
2-Chloronaphthalene
2-Chiorophenol
2-Methylnaphthalene
2-Methyiphenol
2-Nitrophertol
34-Methylphenol
33-Dlchlorobenzidine
46-Dinilm-2-methylphenol
4Bromophenyfphenylether
4-Chloro-3-methylphenol
4-ChloroaniFine
4-Chlorophenylphenylether
4-Nftrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzoaanthracene
Benzoapyrene
Benzobfluorantheno
Benzogh.iperylene
Benzokfluoranthene
Benzolc acid
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 1.65 0.825
ND 0.33 0.165
ND 033 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0165
ND 0.66 0.33
ND 1.65 0.825
ND 0.33 0.165
ND 0.66 0.33
ND 0.33 0.165
ND 0.33 0.165
ND 1.65 0.825
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 1.65 0.825
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 1.65 0.825
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Q25550
025550
Q25550
025550
Q25550
025550
025550
Q25550
Q25550
025550
Q25550
025550
025550
025550
025550
025550
025550
025550
025550
025550
025550
025550
025550
025550
025550
025550
025550
Q25550
025550
Q25550
025550
025550
025550
025550
Level QC Report
8/10/07
Project ID Morehead Commons No COC Group Number G0807064
Date/Time Submitted 8/2/07 1325
by GtIMSS.SS SlS SflflNStIIS4 IIICII IUU VI
Method Blank
Batth
Result Rt Contid tJmit Units
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SprlngbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-8364 Fax [phone] Page of
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Recovery Recovery
RangesUnits
00 Batch
ID
ESP Associates PA
Attn Chris Ward
Box 7030
Chaiiotte NC 28241
Level II QC Report
8110107
Project ID Morehead Commons No COC Group Number G0807064
Date/Time Submitted 812/07 1325
Method Blank 00 Batch
Result RL Contrcl Umit Units ID
Benzyl alcohol ND 0.66 0.33 mg/kg 025550
Bis2-chforoethoxymethane ND 0.33 0.165 mg/kg 025550
Bis2-thloroethylether ND 0.33 0.165 mg/kg 025550
Bis2-chloroisopropylether ND 0.33 0.165 mg/kg Q25550
Bis2-ethylhexylphthalate ND 0.33 0.165 mg/kg 025550
Butylbenzylphthalate ND 033 0.165 mg/kg 025550
Chrysene ND 0.33 0.165 mg/kg 025550
Di-n-butylphthalate ND 0.33 0.165 mg/kg 025550
Di-n-octylphthalate ND 0.33 0.165 mg/kg 025550
Dibenzoahanthracene ND 0.33 0.165 mg/kg Q25550
Dibenzoftiran ND 0.33 0.165 mg/kg 025550
Diethylphthalate ND 0.33 0.165 mg/kg 025550
Dhnethylphthalate ND 0.33 0.165 mg/kg 025550
Fluoranthene ND 0.33 0.165 mg/kg 025550
Fluorene ND 0.33 0.165 mg/kg 025550
Hexachlorobenzene ND 0.33 0.165 mg/kg 025550
Hexachiorobutadjene ND 0.33 0.165 mg/kg 025550
Hexachiorocyclopentadlene ND 0.33 0.165 mg/kg 025550
Hexachioroethane ND 0.33 0.165 mg/kg 025550
lndeno1.23-cdpyrene ND 0.33 0.165 mg/kg 025550
Isophorone ND 0.33 0.165 mg/kg Q25550
N-Nitrosodi.n-propylamjne ND 0.33 0.165 mg/kg Q25550
N-Nltrosodiphenylamjne ND 0.33 0.165 mg/kg 025550
Naphthalene ND 0.33 0.165 mg/kg 025550
Nitrobenzene ND 0.33 0.165 mg/kg 025550
Pentachorophenol ND 1.65 0.825 mg/kg 025550
Phenanthrene ND 0.33 0.165 mg/kg 025550
Phenol ND 0.33 0.165 mg/kg 025550
Pene ND 0.33 0.165 mg/kg 025550
Laboratory Control Sample
Result Spike Amount
l24.Trichlorobenzene 1308.84 1669.7 mg/kg 78 39-98 025550
14-Dichlorobenzene 1239.73 1669.7 mg/kg 74 3795 025550
24-Dinihotoluene 1505.17 1669.7 mg/kg 90 56-128 025550
2-Chlomphenol 1236.39 1669.7 mg/kg 74 37-98 025550
4-ChIDID-3-methylphenol 1440.40 1669.7 mg/kg 86 45-111 025550
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SprIngbroolRoadP.O Box 240343 CharIotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
Full SMCGAtulytkai ironmuetsl Sfulioni
Level II QC Report
8/10/07
ESP Associates PA
Attn Chris Ward
Box 7030
Chailotte NC 28241
Project ID Morehead Commons No COO Group Number G0807064
Date/Time Submitted 8/2/07 1325
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SprlngbrookRoadP.O Rox 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number 1-8001529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Control Sample Rovmy Recovey
Result Spike Amount Units Ranges OC Batch
ID
4-Nitrophenol 1206.34 1669.7 mg/kg 72 20-157 025550
Aceriaphthene 1351.25 1669.7 mg/kg 81 44-110 025550
N-Nitrosodi-n-propylamine 1246.41 1669.7 mg/kg 75 38-101 025550
Pentachlorophenol 1687.14 1669.1 mg/kg 101 53-127 025550
Phenol 1279.13 1669.7 mg/kg 77 34-102 025550
Pyrerie 1379.96 1669.7 mg/kg 83 54-131 025550
Matrix Spike Recoveiy
Sample ID Result Spike Amount Units
Recoveiy Ranges QC Batch
ID
188424 124-Trichlorobenzene 1171.66 1667 mg/kg 70 26-97 025550
14-Dichlorobenzene 1110.33 1667 mg/kg 67 23-92 025550
24-Dinitrotoluene 1409.66 1667 mg/kg 85 45-127 025550
2-Chlorophenol 114966 1667 mg/kg 69 25-94 025550
4-Chloro--3-methylphenot 1299.33 1667 mg/kg 78 31-113 025550
4-Nltrophenot 1172.66 1667 mg/kg 70 17-150 025550
Acenaphthene 1238.33 1667 mg/kg 74 36-107 025550
N-Nitrosodi-n-propylamine 1121 1667 mg/kg 67 22-105 025550
Pentachlorophenol 1789.66 1667 mg/kg 107 38-1 37 025550
Phenol 1119.33 1667 mg/kg 67 23-97 025550
Ptiene 1603.56 1667 mg/kg 96 45-1 33 025550
Matrix Spike Duplicate Recoveiy Recoveiy RPD
Sample ID Resut Spike Amount Units Ranges RPD Range QC Batch--ID
185424 124-Tiichlorobenzene 1032.33 1667 mg/kg 62 26-97 13 0-37 025550
14-Qichlorobenene 1017 1667 mg/kg 61 23-92 0-36 025550
24-Dinitrotoluene 1453.33 1667 mg/kg 87 45-127 0-29 025550
2-Chlorophenol 1096.33 1667 mg/kg 66 25-94 0-37 025550
4-Chloro-3-methylphenol 1268 1667 mg/kg 76 31-113 0-32 025550
4-Nitrophenol 1219.66 1667 mg/kg 73 17-1 50 -32 025550
Acenaphthene 1221.33 1667 mg/kg 73 36-107 0-32 025550
N-Nltrosodi-n-propylamjne 1081.66 1667 mg/kg 65 22-105 0-37 025550
Pentachiorophenol 1709.66 1667 mg/kg 103 39-137 0-27 025550
Phenol 1062 1667 mg/kg 64 23-97 0-42 025550
Pyrene 1440 1667 mg/kg 86 45-133 11 0-27 025550
Page of
-See Case Narrative
This report should not be reproduced except in its entirety without the wiitten consent of Prism Laboratories Inc449SprlngbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toil Free Humbem 1-5001529-5364 Fax [phone]
1325
NC Certification No 402
SC Certification Wo 99t12
NC Drinking Water Cert No 37735
Level II QC Report
8/10/07
ESP Associates PA Project ID Morehead Commons COO Group Number G0807064
Attn Chris Ward Date/Time Submitted 8/2107
Box 7030
Charlotte NC 28241
I4f 1w -PIDIFID mthhl aaArmD VPHCLflJICUIIIflYUIUtAflhLJUII
Method Blank QC Batch
Resuft RL Control limit Units ID
C5-C8 Aliphatlcs ND 2.5 mg/kg 025565
C9-Cl0Aromatics ND 2.5 mg/kg 025565
C9-C12 Aliphalics ND 2.5 mg/kg 025565
Laboratory Control Sample covenJ Recovery
Ranges QC Batch
Result Spike Amount Units ID
C5-C8AliphatIcs 17.165 15 mg/kg 114 70-130 025565
C9-C10 Aromatics 4.924 mg/kg 98 70-130 025565
C9-Cl2Aliphatics 10.981 10 mg/kg 110 70-130 025565
Matrix Spike Recovery Recovery
nanges QC Batch
sample 10 Result SpIke Amount Units ID
188652 C5-C8 Aliphatics 17.575 15 mg/kg 117 70-1 30 025565
C9-ClOAromatjcs 5.116 mg/kg 102 70-130 025565
C9-Cl2Aliphafics 21.085 10 mg/kg 211 70-130 025565
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range OC BatCh
Sample ID Result Spike Amount Units ID
188652 C5-C8 Atiphafics 18.442 15 mg/kg 123 70-1 30 -25 025565
C9.C10 Aromafles 5.259 mg/kg 105 70-130 0-25 025565
C9-012 Aliphatics 22.641 10 mg/kg 226 70-130 0-25 025565
Page 8dB
Phone ________________
Email Yes No Email Address
Samplers Signature
Upon relinquishing th
submitted in writing
Sampled By Print Name 22-Affiliation .ri/
is Ct1n of Custo is your authorization for Prism to proceed with the anaIysec requested above Any changes
must be
the Prism Project Manager There will be charges for any changes after analyses have been Initialized
ReIinuisneo uy toignarure Received By SignaIure Dale Mllitaryfl-loura
ReltnuIshed By Signalura Received By Signature Data
Re etvedRelinquishedByStgnalur
ricu9
oratories By
Method of Shipment NELL FL OOLERS SHOULD BE TAPED SH
SAMES ARE NOT ACCEPTED AND VERIFIED AGAINSG UNTIL RECEIVED AT THE LABORATORY
Fed En UPS ad.dltvered Prism Field ServIce Other
Date
COO Group Noc1L
SEE REVERSE FORTERMSCONDITIONSNPDESU1GROUNDWATERDRINKINGWATERSOLIDWASTE RCRA CERCLA LANDFILL OTHERONCUSCIbfNCUSCUNC USC UNG USC UNC USC UNC USCI UNC USC UNC USC UNC USCD_U_..____lU_IU._____Q__ORtG1ALCONTAINER TYPE CODES Amber Clear Glass Plastic TL Teflon-Lined Cap VOA Volatile Organics Analysis Zero Head Space .I.
...P1usMLABORATORIESRIO
Full Service AnalytIcal Environmental SolutIons
449 Sprlngbrook Road P.O Box 240543 Charlotte1 NC 28224-0543
Phone [phone] Fax
Report To/Contact Name
Client Company Name ___________________________
Reporting Address ______________________________
CHAIN OF CUSTODY RECORD
PAGE 4..OF J_QUOTE TO ENSU PR ER BILLING _______________
Project Name Mbt4f1J CL4 ui.tt
Short Hold Analysis Yes No LIST Project Yes No
please ATTACH any project specific reporting QC LEVELI 11111 IV
provisions and/or QC Requirejts
Invoice
Fax Yes No
LAB USE ONLY
EDD Type PDF_Excel Othe
Site Location Name t--t v..jie_
Site Location Physical Address .$
ThS NO VA
Samples INTACT upon arflval
Received ON WET iCE Temp
PROPER PRESERVXTIVES indicated
Received WITHIN HOLDING TIMES
CUSTODYSEALS INTACT
VOLATILES recd W/OUT HEADSPACE
PROPER CONTAINERS used
Purchase Order No./Billing Reference
Requested Due Date Day 02 Days 08 Days 04 Days i5 Days
Working Days
6-9 Days Standard 10 days us Workust Be
Samples received after 1500 will be processed next business day
Turnaround time is based on business days excluding weekends and holidays
SEE REVERSE FOR TERMS CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES INC TO CLIENT
BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC_USACE....-FL_____NC.1
SC_OTHER _____N/A _____
Water Chlorinated YES_NO
Sample Iced Upon Collection YES
CLIENT
SAMPLE DESCRIPTION
-__._.-___
DATE
COLLECTED12
.I-_
TIME
COLLECTED
MILITARY
HOURSL.
MATRIX
SOILWATER OR
SLUDGE
i_L_
..L
SAMPLE CONTAINER
PRESERVA-TIVES
.__
/i
..L
/4v
IL
i.
ANALYES ./
$Y45VV
I-
UESTEDcfv/
REMARKS
_______
NO
14
1%
TYPE
SEE BELOW
TL/
-._
NO SIZE
.-
Additional Comments
PRISM USE ONLY
Site Arrival Time
Site Departure Time
Field Tech Fee
Mileage
fl
AUG 2007
Date 08/09/07
Company ESP Associates PA
Contact Chris Ward
Address Box 7030
Charlotte NC 28241
Client Project ID
Prism COC Group No
Collection Dates
Lab Submittal Dates
Morehead Commons No
G0807065
08/02/07
08/02/07
This data package contains the analytical results for the project identified above and includes Case Narrative Laboratory Report and Quality
Control Data totaling pages chain-of-custody is also attached for the samples submitted to Prism for this project
Data qualifiers are flagged individually on each sample key
reference for the data qualifiers appears at the end of this case narrative Qualitycontrolstatements and/or sample specific remarks are included in the sample comments section of the laboratory report for each sample
affected
Semi Volatile Analysis
No Anomalies Reported
Volatile Analysis
No Anomalies Reported
Metals Analysis
N/A
Wet Lab and Micro Analysis
N/A
Please call if you have any questions relating to this analyilcal report
Date Reviewed by Paula Gilleland Project Manager
Signature ._A ViQ.oL Signature
Review Date 08/09/07
P4igja Overcash
cL
Data Qualifiers Key Reference
Compound also detected in the method blank
1/Result outside of the QC limits
DO Compound diluted out
Estimated concentration calibration range exceeded
The analyte was positively identified but the value is estimated below the reporting limit
Estimated concentration with high bias
Estimated concentration with low bias
matrix effect is present
Notes This report should not be reproduced except in its entirety without the writtten consent of Prism Laboratories Inc The results in thisreportrelateonlytothesamplessubmittedforanalysis
449 Spngbrook Road P.O Box 240543 Chailotte NC 28224-0403
Phone [phone] Toll Free 800/529-6364 Fax [phone]
PiusM
LABORATORIESINC
Case Narrative
Approval Date
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
IA/lB COMPOSITE
188657
G0807065
08/02/07 1030
08/02/07 1325
Diesel Range Organics DRO by GC-FID
Diesel Range Organics DRO
Gasoline Range Organics GRO by GC-FID
Gasoline Range Organics GRO 6.9
Surrogate Recovery Control Limits
aaa-TFT 90 55 129
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full Service Analytical Environmental Solutions
Laboratory Report
08/09/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Percent Solids Determination
Percent Solids
Volatile Organic Compounds bvGC/MS
Benzene
Ethylbenzene
mp-Xylenes
o-Xylene
Toluene
SM2540 08/03/07 1555 ddixori89.2
BRL
BRL
4.3
3.7
BRL
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
3.3 0.44
5.5 0.38
11 0.77
5.5 0.33
5.5 0.37
8260B
8260B
8260B
8260B
8260B
Surrogate
Toluene-d8
Dibromofluoromethane
Bromofluorobenzene
08/08/07 2202 Iwitry Q25514
08/08/07 2202 Iwitry Q25514
08/08/07 2202 twitry Q25514
08/08/07 2202 witty Q25514
08/08/07 2202 witty Q25514
Recovery Control Limits
99 81-128
Sample Preparation
109
105
67-143
77-128
Q25614710mg/kg 200 4.9 8015B 08/07/07 2314 jvogel
25.08g mL 3545 08/06/07 1650 wconder P19098
Surrogate Recovery Control Limits
o-Terphenyl 49-124
mg/kg 6.7 3.6 50 8015B 08/08/07 030 hwagner 025589
Page of2
Full Service Analytical Environmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
08/09/07
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
INIB COMPOSITE
188657
G0807065
08/02/07 1030
08/02/07 1325
Parameter
Sample Comments
BRL Below Reporting Limit
J-Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthose instances indicated in the case narrative and/or test comments
All results are reported on dry-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
Full Service Anolytical Environmonttl Solutions
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
8/9/07
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No COC Group Number G0807065
Date/Time Submitted 8/2/07 1325
Volatile Organic ComDouflds by GC/MS method 826DB
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number 1-800/529-6364 Fax [phone]
Method Blank
Result RL control Limit Units
Benzene ND 0.003 0.0015 mg/kg
Ethylbenzene ND 0.005 0.0025 mg/kg
mp-Xylenes ND 0.01 0.005 mg/kg
o-Xytene ND 0.005 0.0025 mg/kg
Toluene ND 0.005 0.0025 mg/kg
QC Batch
ID
Laboratory Control Sample Recovery Recovery
RangesResultSpikeAmountUnits
0.044
0.04939
0.09958
0.04956
0.05135
0.05
0.05
0.1
0.05
0.05
025514
025514
025514
025514
025514
QC Batch
ID
025514
025514
025514
025514
025514
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
88
99
100
99
103
62-119
57-128
54-132
57-131
57-122
Result Spike Amount
Benzene
Ethylbenzene
p-Xylenes
o-Xylene
Toluene
Matrix Spike
Recovery Recovery
Sample tD Units Ranges DC Batch
188597 Benzene 0.04675 0.05 mg/kg 94 46-136 025514
Ethylbenzene 0.05109 0.05 mg/kg 102 51-135 Q25514
mp-Xylenes 0.10369 0.1 mg/kg 104 51-136 025514
o-Xylene 0.05162 0.05 mg/kg 103 49-137 025514
Toluene 0.04701 0.05 mg/kg 94 47-1 36 Q25514
Recovery ery RPD
Sample ID Result Spike Amount Units Ranges RPD Range Batch
ID
188597 Benzene 0.04467 0.05 mg/kg 89 46-136 0-22 Q25514
Ethylbenzene 0.04982 0.05 mg/kg 100 51-135 0-23 025514
mp-Xylenes 0.09579 0.1 mg/kg 96 51-136 -20 Q25514
o-Xylene 0.05082 0.05 mg/kg 102 49-137 -22 025514
Toluene 0.04496 0.05 mg/kg 90 47-136 -22 025514
Page of2
Full Service Analytical Environmental Solutions
ESP Associates PA
Atm Chris Ward
Box 7030
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No
Level II QC Report
8/9/07
COC Group Number G0807065
Date/Time Submitted 8/2/07 1325
Charlotte NC 28241
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
flrIins Ponr1A flrnnirm GRO by GCF1fl
muFk1
Method Blank QC Batch
Result RL Control Limit Units ID
Gasoline Range Organics ND 0.5 mg/kg 025589GRO
Laboratory Control Sample Recovery Recovery OC BatchRangesResultSpikeAmountUnitsID
Gasoline Range Organics 2.050 mg/kg 103 64-124 025589GRO
Matrix Spike Recovery Recovery
Ranges QC Batch
Sample ID IDResultSpikeAmountUnits
0/
188906 Gasoline Range Organics 1.948 mg/kg 97 37-126 025589GRO
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range OC Batch
Sample ID Result Spike Amount Units
0/ID
188906 Gasoline Range Organics 2.075 mg/kg 104 37-126 0-34 025589GRO
Diesel Range Organics DRO by GC-FID method 8015B
Method Blank
QC BatchResultRLControlLimitUnitsID
Diesel Range Organics DRO ND 3.5 mg/kg 025614
Laboratory Control Sample Recovery Recovery
Ranges DC BatchResultSpikeAmountUnitsID
Diesel Range Organics DRO 85.1 80 mg/kg 106 55-1 09 025614
Matrix Spike
Recovery Recovery
Ranges DC BatchSampleIDResultSpikeAmountUnitsID
188240 Diesel Range Organics DRO
Matrix Spike Duplicate
Sample ID
72.9 80
188240 Diesel Range Organics DRO 68.1
-See Case Narrative
Result Spike Amount
80
mg/kg 91 50-117 025614
Recovery Recovery RPD
Ranges RPD Range QC Batch
Units ID
mg/kg 85 50-117 0-24 025614
Page of
Full Service Analytical Environmental Solutions
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543Phone[phone] Fax [phone]
Client Company Name Ak
Report To/Contact Name
Reporting Address _______________________________
Phone ________________Fax Yes No
Email Yes No Email Address______________________
EDD Type PDF_Excel Othpr_
Site Location Name ____________________________
Site Location Physical Address jl
CHAIN OF CUSTODY RECORD
PAGE .L OF i_QUOTE TO ENS PROPER BILLING _______________
Project Name /4LJ tk
Short Hold Analysis Yes No UST Project Yes NopleaseATTACHanyprojectspecificreportingOCLEVEL111111IV
provisions and/or QC Re9yernents
Invoice To k-gAddrec
Purchase Order No./Billing Refere CO
Requested Due Date Day Days Days Days Days
Working Days 6-9 Days Standard 10 days sWorkMust Be
Samples received after 1500 will be processed next business dayTurnaroundtimeisbased on business days excluding weekends and holidaysSEE REVERSE FOR TERMS CONDITIONS REGARDiNG SERVICESRENDERED BY PRISM LABORATORIES INC TO CLIENT
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC USACE FL _____
SC__OTHER _____N/A _____
Water Chlorinated YES_NO
Sample Iced Upon Collection YES t-NO
.iI
SAMPLE DESCRIPTION
CLIENT
COLLECTEDDATE
TIME
MILITARY
HOURS
COLLECTED
MATRIX
WATER OR
SLUDGE
SOIL SAMPLE CONTAINER
TIVES
PRESERVA-
ANALYSES REQUESTED
EMARKS
/////l/o$9///////
////PRISM
LAB
ID NO
TYPE
SEE BELOW NO SIZE
77-
/o/-3 zsi
js ---iii C.t4pASiz/73k
i1__
Samplers Signature Sampled ByPnnt Name Affiliation
Upon relinquishing this C1in of Cust is your authorization for Prism to proceed with the analy es as requested above Any changes must besubmittedinwritingtothePrismProjectManagerTherewillbechargesforanychangesafteranalyseshave been initializedRelinquishedBySignatureMeceiveaSignature Date
Relinquished By Signature Received By Signature Date
Relinquished By Signature
Method of Shipment EJAMP C9LERS SHOULD BE TAPED SHU
SAIPLES ARE NOT ACCEPTED AND VERIFIED AGAINST
Rec vs For Pri aboratories By
WIT CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY
NTIL RECEIVED AT THE LABORATORY
atj
COC roup No
Fed By UPS Hand-delivered Prism Field Service Other
iviiiitaryniours
JJl-1
Additional Comments
NPDES GROUNDWATER DRINKING WATER SOLID WASTE RCRA CERCLA LANDFILL OTHERUNCUSCCUSC UNC USC UNC USC UNC USC UNC USC UNC USC UNC USC UNC USCU_U ____________________CONTAINER TYPE CODES Amber Clear Glass Plastic TL Tefin-I nRc Cn VCA \/rintile flrricinito nnloic 7mm I-lmarl cro.m\
ita Arrival Time
Site Departure Tim
Field Tech Fee
Mileage
SEE REVERSE FORTERMSCONDITIONS
ORIGINAL
APPENDIX
NON-HAZARDOUS WASTE MANIFESTS
ALLaD WAyproortypa
.1 Ii
No
Gror Fhorrn
poj-Comp1fly Nnrn
for MatRrIn Litod Abo
Ha6dIlflç Instructio and AdditionJ ntormon
17 ltmipôrtr Aoknowodgame of flaceipt of Marai
Prjntod /lypod Noni
----.-
Trnsportr AOIcnQW1OJPOmgnt of
Frlnted Typsd tiam
J-a-Eoo7 55 FROM BFI SCfLE HIILISE TI7823O97 TO 1EO391E.i
/S/
NC 22
fder pUlAttoflR for ppin propsr dInpeI of HrdouoPrfritodWpodNSI-TIB
0Isocpnncy Indioatto 8poc
FOOII Own or Oporao Crfjctio of of wat matorpa vrsd by this mrffe flotod InItom 19
ii
TISfDfçj CQpy AWL Form 12
Piea print or typorrjidnolgieoor ue on ciitn I1 ptrnf 1OwrjtrNONLHAZARDOIJS
.WA$TE.MANIFEST ___eI1efRtora tIam rini Mailing AdcrA
Goriamtorp Phoria
11neportor Company Nama
slnatoc raoliliy Nama arid SItAddm
CMS Lnndffll
5105 Morehad Rf
Concord NC27
11 Wnnte Shlpph Nüma and DanrIpHon
18 llanaportcr Aaknowladgernent of Roolpt Mtnjnia
grturo
Dlncrepaj-cy Indlooticin ..paoo
.-.-.-.----20 FciIity Own or OporotQr Oi-IflcajI of rcieclpt waatn rnÆtrracovOmd by hi uiiifot cixoapt aa n9otI In Itrm 18
4L1G222U17 1454 FROM BFI ScALE HOUSE 7447E2309
pr .ALLb WA1TLiDusTrtisINC
2.Piin1OcicumontNo
TO1El13E1225ls F5
1.2 i1C
lhcik 11o
C1ath22__2iL ii
U0 flPA JO N1ijmbr
10 Us EPA lDNumboi
TIan ortcirn Phone
FoiIItya Phone
704 782-2004
14
Unit
Wi/Vol
12 Contrilnora
No 1lpo
13
Ibtal
OuntJty
T/StO/F/copy
4LlG-2E--8IJOT i155 FROti BFI SCflLE HOLISE 44T823O97 TO 1803E022515 FT8
ALL1 W$TNOIJTPIENC
MnnIfe$
Dnoumrint
2wJ
ntcra Pho
Comptny Neme Odder Thompson
rpotter Company tkme
1000 South Clarkson Stt
charlattQ NC 223l
Petroleum hnpactcd Soil
0tNEflATORS CERTIFICATIoN rflry tttn rterfrt odbid 9ove on Hun resniHust are not aubject ragufetIon or repor1bj proper ctJnponI
of Hsnejs WantePtjntadTypedName
17.1r3portor1AaknQwkndpflmflI nf Recoipt of
Prfritd Typed Norncn
lB l1intnportor AotflowIedernent of fleIpt of MRterIinIn
Printed Typed Name
pecR
Daejgnathd Pactty
CMS Lnndflfl
5105 Morohod Rd
Concord NC 2027
li-Waste ShIppInt Nnmne end Description
IN
in
.3
RIGINAL RETUnNTO GENERATOR
Corporate Office
MailingP0Box 7030
Charlotte North Carolina 28241
Physical
3475 Lakemont Boulevard
Fort Mill SC 29708
8038022440
Raleigh
14001 Weston Parkway
Suite 100
Caiy North Carolina 27513
919.678.1070
Wilmington
2120-B Capital Drive
lmington North Carolina 28405
910.313.6648
Concord
4601 Corporate Drive NW
Suite 165
Concora North Carolina 28027
704 793.9855
800.960.7317
www.espassociates corn
ESP Associates P.A