Item No 30 - NFA Letter - Indcident No 36326 Morehead Common-OCR

NCDENR
North Carolina Department of Environment and Natural Resources
Beazer Homes
1300 South Boulevard Suite
Charlotte North Carolina 8203-4265
Attention Jade Eastridge
Dear Ms Eastridge
August 10 2007
Re Notice of No Further Action
ISA NCAC 2L .0407d
Risk-based Assessment and Corrective Action
for Petroleum Underground Storage Tanks
Morehead Common-Area
919 West Morehead Street
Mecklenburg County
Incident Number 36326
Risk Classification Low
The Initial Abatement Action Report received by the Underground Storage Tank UST Section
Mooresville Regional Office on August 2007 has been reviewed The review indicates that after tank
closure and soil excavation soil contamination does not exceed the lower of the soil-to-groundwater or
residential maximum soil contaminant concentrations MSCCs established in Title ISA NCAC 2L
.04 11
The UST Section determines that no further action is warranted for this incident This
determination shall apply unless the UST Section later finds that the discharge or release poses an
unacceptable risk or potentially unacceptable risk to human health or the environment Pursuant to Title
ISA NCAC 2L .0407a you have continuing obligation
to notify the Department of any changes that
might affect the risk or land use classifications that have been assigned
This No Further Action determination applies only
to the subject incident
Schiff
Hydrogeologist
Mooresville Regional Office
cc Shawna Caldwell LUESA-Mecklenburg County Health Department
ESP Associates Attention Christopher Ward
Michaet Easley Governor
WiUtam Ross Jr.Secretary
Division of Waste Management
Underground Storage Tank Section Dexter Matthews Director
If you have any questions regarding
this notice please contact me at 704 235-2172
ina2Sll5
By
IT
ii
Mo
Cliarlo
August 2007
$ESP
ESP Associates P.A
NCDENR
UST Section
Mooresvffle Regional Office
919 North Main Street
Mooresville North Carolina 28115
Attention Mr Allen Schiff
Reference INITIAL ABATEMENT ACTION REPORT
Morehead Common Site Area No
919 West Moreheaci Street
Charlotte Mecldenburg County North Carolina
UST Incident No No Yet Assigned
ESP Project No E6-UD42.601
Dear Mr Schiffi
August 2007
On behalf of the property owner Beazer Homes ESP Associates P.A is pleased to provide the
attached Initial Abatement Action Report for the closure of the subject propertys peiroleum
release ESP respectively requests
classification of the release as Low Risk and issuance of no
further action notice
Thank you for your attention in this matter If you should have any questions please do not
hesitate to contact me at 803 835-0915k
Sincerely
ESPAssociates P.A
Eagar Rogers
Staff Scientist
cc Jade Eastridge Beazer Homes
Environmental Services ManagerNCLicenseNo1600
P.O Box 7030 Charlotte NC 28241
1.800.960.7317 704.583.4949 fax [phone] SC 803.802.2440 fax [phone]
wW.espassociates.coiu
Initial Abatement Action Report
SITE iNFORMATION
Site Identification
Li Date of Report August 2007
Facility ID NA
UST Incident Number Not Yet Assigned
Li Site Name Morehead Common Site Area No
Site Street Address 919 West Morehead Street
Li City/County/Zip Code Charlotte Mecklenburg County
28278
ci Description of Geographical Data Point Approximate center of UST
ci Location Method Mecklenburg County
Polaris GIS Map
Latitude 35.2276
ci Longitude -80.8582
Information about Contacts Associated with the Leaking UST System
Li UST Owner Beazer Homes
1300 BIvd Suite Charlotte NC 28203-4265
704.370.7200
Li IJST Operator N/A
Li Property Owner Same as above
ci Property Occupant Same as above
Consultant/Contractor ES Associates P.A Chris Ward PG
P0 Box 7030 Charlotte NC 28241
803.835.0915
Analytical Laboratory Prism Laboratories Inc
P0 Box 240543 Charlotte NC 28224-0403
704.529.6364
NC Certification No 402
Information about Release
Date Discovered June 19 2007
Estimated Quantity of Release Unknown
Cause of Release Unknown
ci Source of Release USTs
Size and contents of UST
System from which release occurred 900-gal steel gasoline and 1500-gal diesel USTs
Chris Ward Professional Geologist for ESP Associates PA do certify that the
contained in this report is correct and accurate to the best of my knowledge
Associates P.A is licensed to practice both geology and engineering in North Carolina
Associates certification numbers are Geology C-347 and Engineering C-0587
InitialAbaternent Action Report ESP Project E6-UD42.601
Morehead Cwninon Site Area No August 2007
INTRODUCTION
The subject site has an address of 919 West Morehead Street in Charlotte Mecldenburg County
North Carolina see Figure Topographic Site Location Map The area of the subject release
associated with 900-gallon gasoline and 1500-gallon diesel underground storage tanks liSTs
uncovered on June 19 2007 has been designated by ESP as Area No of the Morehead
Common site
SITE HTSTORY AND CHARACTERIZATION
On June 19 2007
ESP responded on behalf of Beazer Homes to an encounter with several USTs
and impacted soil during mass grading operations at the subject site Upon arriving at the site
ES observed 900-gallon steel apparent gasoline UST and 1500-gallon steel apparent diesel
UST along with soils with petroleum odor located on the south side of West Morehead Street
approximately 150 feet west of its intersection with South Clarkson Street on Tax Parcel No
07325210 see Figures and As required following receipt of laboratory results confirming
release had occurred ES emailed notification of the release discovery along
with Release
and .1ST Leak Reporting Form to Mr Steve Bograd of the Mooresville Regional Office of
NCDENRon June 19 2007
Release Location
The subject site former auto repair facility is located within an urban area of Charlotte which
historically included warehouse and commercial structures Site structures associated with the
former auto repair facility were razed sometime between 2002 and 2005 The site is currently
mass graded with no surface structures present Facility ID No was not available for the site
Based on our review of the Geologic Map of North Carolina 1985 the subject site is located
within the Charlotte Belt locally comprised of intrusive metamorphosed granitic rocks locally
biltialAbaternent Action Report ESP ProJect E6-UD42.601
Morehead omrnoi Site Area No August 2007
pinkish gray massive to weakly foliated and containing hornblende Soils encountered in this
area are the residual product of chemical weathering of rock presently underlying the site Soil
weathering is more advanced near the surface grading with depth to less weathered rock and
finally bedrock
UST Information
Following the June 19 2007 discovery of 900-gallon gasoline UST and 1500-gallon diesel
UST AD Environmental and Industrial Services AD of High Point North Carolina was
contacted to remove remaining product/sludge from the tanks prior to their removal from the
excavation On June 19 2007 AD pumped less than 10 gallons of product/sludge from each
tank for permitted recycling at their Archdale North Carolina facility see Product Material
Manifest in Appendix Once removed the tanks were transported by AD to the I-I
Griffin recycling facility in Greensboro North Carolina on June 19 2007 see Tank Disposal
Manifest in Appendix See site photographs in Appendix
completed UST-2 Form is included as Appendix Former locations of the above USTs are
depicted on Figure
Previous Reporting
ESP emailed release notification along with 24-Hour Release and UST Leak Reporting Form
to the Mooresville Regional Office of NCDENR on June 19 2007 see Appendix
Additionally ESP submitted 20-Day Report to NCDENR on July 18 2007
JnitialAbatement Action Report ESP Project E6-UD42.601
Morehead common Site Area No August 2007
INITIAL ABATEMENT ACTIVITIES
Initial Contaminated Soil Excavation
On June 19 and 20 2007
ESP documented the excavation of 278.78 tons of impacted soil from
Area No by the sites grading contractor Gelder Thompson of Midland North Carolina The
excavation was advanced based on results of OVA field screening and evidence of visible
staining The resulting excavation measured approximately 20 ft 21 ft ft deep The
excavated soil was placed on and covered with plastic awaiting subsequent off-site permitted
disposal Neither groundwater bedrock nor free product were encountered within the tank pit
See site photographs in Appendix
Initial Post-Excavation Confirmatory Sampling
On June 20 2007 confirmatory soil samples were collected at depth of feet BLS from each
of the excavations four sides WS-l through WS-4 while one sample was collected at depth
of feet BLS from the base of the excavation B-i The sidewall samples were collected at the
foot depth due to the prevalence of elevated OVA readings at that depth The five soil samples
were hand delivered on ice to Prism Laboratories of Charlotte North Carolina to be analyzed for
risk-based parameters which include volatile organic compounds VOCs by EPA Method
8260B semi-volatile organic compounds SVOCs by EPA Method 8270C VPHIEPH by the
Massachusetts Department of Environmental Protection MADEP method and for total lead
and chromium by EPA Method 60 lOB Sample locations and excavation dimensions are
depicted on Figure Soil Sample Location Map Sampling was performed in general
accordance with BSPs SOP see Appendix
Results of the laboratory analysis of confirmatory samples WS-1 through WS-4 and B-I revealed
that all analyzed constituents were either below reporting limits BRLs or below the lowest of
the soil-to-groundwater or residential MSCC with the exception of several SVOCs in wall
samples WS-2 and Ci 1-C22 Aromatics in WS-3 while chromium was detected at
concentration of 120 mg/Kg in base sample B-i Laboratory analytical results for the
InitialAbatement Action Report ESP Project E6-UD42.601
Morehead Common Site Area No August 2007
confirmatory soil samples are summarized on Table B-i The Prism laboratory data report is
included as Appendix
Follow-up Contaminated Soil Excavation and Confirmatory Sampling
Due to the detection of elevated constituents above applicable standards in confirmatory samples
WS-2 WS-3 and B-i an additional two feet of soil was excavated from the southern and eastern
walls and from the base of the excavation on July 2007 Excavated soil was placed on the
previous soil stockpile for subsequent off-site permitted disposal The resulting excavation
measured approximately 22 ft 23 ft 10 ft deep See Figure for depiction of the
excavation limits and sample locations
On July 2007 following excavation of additional soil ES collected confirmatory soil
samples WS-2 and WS-3 at depth of feet BLS from the southern and eastern walls of the
excavation and B-I at depth of 10 feet from the base of the excavation Samples WS-2 and
WS-3 were submitted to Prism for analysis of SVOCs by EPA Method 8270C WS-3 for EPH by
the MADEP Method and B-i for total chromium by EPA Method 6OlOB Results of the analysis
of the July 2007 confirmatory sampling revealed that all analyzed organic
constituents were
BRLs while chromium was detected below the soil-to-groundwater MSCC see Table B-i The
Prism laboratory data report is included as Appendix
Stockpile Sampling and Soil Disposal
On June 20 2007 ESP collected two composite stockpile soil samples for laboratory analysis
The stockpile soil samples designated 1A and lB were placed in laboratory provided containers
labeled and hand delivered on ice to Prism for compositing and subsequent analysis The
samples were analyzed for TPH-GRO/DRO by EPA Method 5030/3550 and for BTEX by EPA
Method 8260B The composite samples were collected and analyzed to conlirin that release
had occurred and to characterize contaminant types and concentrations for subsequent offsite
permitted disposal/treatment
InitialAbat em ant Action Report ESP Project E6-UD42.601
More/wad Common Site Area No August 2007
As revealed by the laboratory analysis
of stockpile composite samples 1A and 113 TPH-DRO
was reported at concentrations of 400 and 76 mg/Kg respectively while results for the
remainder of organic analytes were BRLs Total lead was reported at concentration of 15
mg/Kg 1A and 13 mg/Kg 18 Results of the stockpile sample analyses are summarized on
Table B-2 while the laboratory data report is included as Appendix
On July 27 2007
total of 278.78 tons of stockpiled soil from the Area excavation was
transported by Gelder Thompson to the CMS Landfill in Concord North Carolina for permitted
disposal see Non-Hazardous Waste Manifest in Appendix
RECEPTOR STJRVEY
On July 20 2007
Mr Eddie Rogers of ESP performed receptor survey to document the
presence or absence of active and/or inactive water supply wells within 1500-foot radius of the
subject UST release see Figure Receptor Survey Map The receptor survey included
interviews with available site occupants and visual observations for water supply wells and/or
municipal water meters All properties within 500 feet of the site were visited to determine well
status The area within 1000 feet of the subject release consists of commercial and industrial
development with numerous vacant structures No active or inactive water supply wells were
identified within 1000-foot radius of the subject release Municipal water and sewer have
historically been available within the area of the site Additionally no surface water bodies were
identifed within 500 feet of the release see Figure
IniticilAbatement Action Report ESP Project E6-.UD42 601
Morehead Common Site Area No .5 August 2007
CONCLUSIONS ANIO R1COMMENDATIONS
The following conclusions have been formulated based on our completion of field activities
including abatement activities receptor survey and our review of laboratory data from the
analysis of collected soil samples
ci The subject site razed former auto repair facility has an address of 919 West
Morehead Street in Charlotte Mecldenburg County North Carolina
ci On June 19 2007
ESP responded on behalf of Beazer Homes to an encounter with
900-gallon steel apparent gasoline UST and 1500-gallon steel apparent diesel UST
along with soils with petroleum odor during excavations conducted ahead of mass
grading operations at the subject site
ci On June 19 and 20 2007 ESP documented the excavation of 278.78 tons of impacted
soils from the release area The resulting excavation measured approximately 20 ft 21
ft ft deep
ci Neither groundwater bedrock
nor free product were encountered within the tank pit
ci On June 20 2007 confirmatory soil samples were collected at depth of feet BLS
from each of the excavations four sides WS-through WS-4 while one sample was
collected at depth of feet BLS from the base of the excavation B-I
ci Results of the laboratory analysis
of confirmatory samples WS-l through WS-4 and B-i
revealed that all analyzed constituents were either below reporting limits BRLs or
below the lowest of the soil-to-groundwater or
residential MSCC with the exception of
several SVOCs in wall samples WS-2 and C1l-C22 Aromatics in WS-3 while chromium
was detected at concentration of 120 mgfKg in base sample B-i
ci Due to the detection of elevated constituents above applicable standards in confirmatory
samples WS-2 WS-3 and B-i an additional two feet of soil was excavated from the
southern and eastern walls and from the base of the excavation on July 2007 The
resulting excavation measured approximately 22 ft 23 ft 10 ft deep
On July 2007 following excavation of additional soil ESP collected confirmatory soil
samples WS.-2 and WS-3 at depth of feet BLS from the southern and eastern walls of
JnitialAbaternent Action Report ESP Project E6-UD42.601
Morehead Common Site Area No August 2007
the excavation and B-I at depth of 10 feet from the base of the excavation Samples
WS-2 and WS-3 were submitted to Prism for analysis of SVOCs by EPA Method 8270C
WS-3 for EPH by the MADE Method and B-i for total chromium by EPA Method
601 OB
Results of the analysis of the July 2007 confirmatory sampling revealed that all
analyzed organic
constituents were BRLs while chromium was detected below the soil-
to-groundwater MS CC
On June 20 2007 ESP collected two composite stockpile soil samples designated 1A
and 1B for laboratory analysis The composite samples were collected and analyzed to
confirm that release bad occurred and to characterize contaminant types and
concentrations for subsequent off-site permitted disposal/treatment
As revealed by the laboratory analysis of stockpile composite samples 1A and 1B TPH
DRO was reported at concentrations of 400 and 76 mg/Kg respectively while results for
the remainder of organic analytes were BRLs Total lead was reported at concentration
of 15 mg/Kg 1A and 13 mg/Kg IB
On July 27 2007 total of 278.78 tons of stockpiled soil from the excavation was
transported to the CMS Landfill in Concord North Carolina for permitted disposal
Municipal water and sewer are available in the area of the release
No water supply wells were identified within 1000 feet of the release and
No surface water bodies were identified within 500 feet of the subject release
Based on the absence of analyzed risk-based parameters above the lowest of the North Carolina
soil-to-groundwater or residential MSCCs laclc of either groundwater bedrock or free product
within the tank pit the documented absence of water supply wells within 1000 feet of the
release and the absence of surface water feature within 500 feet of the release ESP
recommends that NCDENR issue no further action notice for the subject release
Attachments
Table B-i Summary of Soil Sampling Results
Table B-2 Summary of Stockpile Soil Sampling Results
Figure Topographic Site Location Map
Figure 2-2005 Aerial Photograph
Figure Soil Sample Location Map
Figure 4-Receptor Survey Map
Appendix 24-Hour Release Notification
Appendix UST-2 Form
Appendix Tank Disposal Manifest
Appendix Product Material Manifest
Appendix Site Photographs
Appendix ESPs SOP
Appendix Prism Laboratory Data Reports
Appendix Non-Hazardous Waste Manifests
ATTACITMENTS
TABLES
Table B-i
7/1 6/07
Summary of Soil Sampling Results
Common Area No Charlofte No
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BOS feet below ground surface
Results reported in mgkg
Health based level 100%
Considered immobileNANotAnalyzedNL Not Listed
LJJJ
Table B-i
Date 7/1 6/07
II IiII Ic
Ii
iiijjfijSandipli
________________
11 Ii
WS-1 6/20/07 North Pit Initial
Wall Abatement
WS-2 6/20/07 West Pit Initial
Wall Abatement
WS 715/07 West Pit Initial
Wall Abatement
WS-3 6120/07 South Pit Initial
Wall Abatement
WS-3 7/5/07 South Pit liutial
Wall Abatement
Ws-4 6/20/07 East Pit Initial
Wall Abatement
B-i 6/20/07 Pit Floor Initial
Abatement
B-I 7/5/07 Pit Floor 10 Initial
________ ___________
Abatement
Summary of Soil Sampling Resuits
Morehead Common Area No Charlotte North CarolinaIncidentNoNotAssigned
6010B 6010B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B
_i .D
37 9.0 0.0055 0.0055 0011
29 84 0.0055 0.0055 0.011
NA NA NA NA NA
29 7.5 0.0053 0.0053 0.011
NA NA NA NA NA
14 8.2 0.0054 00054 0.011
120 12 0.0053 0.0053 0.011
26 NA NA NA NA
27 270 2.2 1.7 0.58
400 3128 626 313
0.11
0.10
NA
0.0053
NA
0.063
0.0053
NA
1564
rt0 rc.0 .0 I--0
0.0055 0.0055 0.0055 0.0055
00055 0.0055 0.0055 0.0055
NA NA NA NA
0.0053 0.0053 0.0053 0.0053
NA NA NA NA
0.0054 0.0054 0.0054 00054
0.0053 0.0053 0.0053 0.0053
NA NA NA NA
3.3 4.3
626 626 782 782
i/
226 400 81760 16 350 176 40 880 16 350 16 350 20440 20 440
BRL Below Reporting LimitMSCCmaximumsoilcontamination coricenfration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNL Not Listed
Table B-i
BRL Below Reporting LimitMSCCmaximumsoilcontamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNL Not Listed
Table B-i Summary of Soil Sampling Results
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNL Not Listed
usWF
CD
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TPH-DRO
t-t-
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Bcnzenc
Toluene
Ethylbenzcne
Xylenes
Lead
FJ
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FIGURES
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WESTMOREHEAD STREET
LEGEND
CONFIRMA TORY SOiL SAMPLE LOCA 710N
AREA EXCA VA liON DEPTH OF 10 FEET
AREA EXCA VA liON OEP7H OF 10 FEET 20
APPROXIMATE SCALEiNFEET
FiGURE
SOIL SAMPLE LOCA liON MAP AREAS AND
MOREHEAD COMMON ShE
CHARLO7TE NORTH CARCiJNA
AREA
w-1
WS-4 WS-2
WS-3
WS-4 WS-2
WS-3
AREA
APPENDIX
24-HOUR RELEASE NOTIFICATION
Page of
Chris Ward
From Chris Ward
Sent Tuesday June 19 2007 354 PM
To SteveBogradncma1I.net
Cc Jade Eastridge [e-mail] [e-mail]
Scott Jones [e-mail]
Subject 24-Hour Notice Morehead Common Releases and
Attachments AREA 424-Hr Notification.pdf AREA 5-24-Hr Notlfication.pdf
Steve
On behalf of Beozer Homes am herein providing 24-Hour Notification of the discovery of three orphan USTs on
Beazer Homes Morehead Common residential/commercial development currently being graded The Morehead
Commons property is located on the south side of West Morehead Street at its intersection with South Clarkson
Street in Charlotte North Carolina On June 18 2007 during grading operations an approximate 550-gallon steel
UST was uncovered on Parcel No 07325210 The UST was uncovered and determined to be partially filled with
sludge and some fluid with diesel odor this UST is being referred to as AREA An additional approximate
550-gallon likely diesel and an approximate 750-gallon likely gasoline were subsequently encountered side by
side approximately 25 feet from the first 550-gallon UST encountered on Parcel No 07325210 these USTs are
being referred to as AREA
On June 19 2007 Ab Environmental and Industrial Services pumped remaining fluid and sludge from the USTs
and transported the USTs off-site for permitted disposal The tops of the USTs were buried to depth of
approximately feet below original grade and were severely rusted with numerous holes 5oils adjacent to and
beneath all three USTs exhibited strong petroleum odor and were visibly stained Excavation of soils adjacent to
and beneath the three USTs was initiated on June 19 with soils being stockpiled on site on plastic for subsequent
off-site disposal
Preliminary investigation reveals that Parcel No 07325210 was once occupied by Tonys Auto Body Shop
and
Shorts Imports The releases are identified on the affached PbF map included with the 24-Hr Notification
Forms
The Responsible Party for the property is
Beazer Homes
1300 South Boulevard
Suite
Charlotte North Carolina 28203-4265
Mr Jade Eastridge
704.370.7200
Please call with any questions
Thanks
Chris Ward PG
Environmental Services Manager
E.5 Associates P.4
803.835.0915 direct office
803.802.2515 fax
7/fl/9flfl7
..r-UaT64I 2-oIrea UST qak Repodmg Fom
form ebould be completed and submitted to the UST Sections regIonal ofltee loitowing known or suspected release Fromore1eases
an underground storage tank UST system This 1mm Ia required to be submitted withIn 24 hoUrs oldiscavety ole known or
Iii NC aDapt ease
DWM USE ONLY Suspected Contamlnaflor YIN Faclitty ID Number N/A
Indclent FkElIL Confirmed GW Contemiriafion YIN Date Leak Discovered
ReceIvd On acatved by_______Confirmed Salt ContarnjaUon WN CoininlNon-Carnpierolal
Reportad by cite/a opeFhone FaiUr flpot Free Product YIN JL liVes Slate Greatest ReglNan.reguleted
Region Thickness
INCIDENT DESCRIPTION
Incident Name
Address 4JQ Mr%L.LQwL L.-County
Regional Office circle one Ashav ooresvllie ayetlevllleCIty/rovm Zip Code Z427T Raleigh Washington Wllmhiglon WInst
Latitude 773 Longihide thioIc1essi ..-17 Oblainedby
Briefly describe suspected orconflrmad releaset Including but not limited to nature ofre1aase dale ofrolease amount OPSofreleaseamountofluteproduct present and recovaty efibrts millet responses conducted Impacts In receptors5/Topographic map-q G1S Mdress matchingL4-pl/..AVJT Other
tL Unknownjie44-4 Ø11-
/7 Describe loentionftfrz1-3rr-ur 22..g4 ./7 jietçwfI-JfI1-_Z-ttrLe--2n._6fHOWRELEASE WAS DISCOVERED
Check one
Release Detection EquIpment or Methods VisuatiOdor Ci Groundwater Contamlnallai
During UST Closure/Removal Ct Water In Tank Ci Surface Water ContamInation
Property Transfer Water Supply Well Contamination .9thar 5pacify 2aiI riii__Oi4imSOURCEOFCONTAMINATION
Primary Source of Contamination Primary Contaminant Type location
Checkone Check one Checkone
GasoflrwlDleseljlçcrrjsene Fanifity Ci ResidentialCIConfirmedUSTReleasaChackonebelowtieaungonCIResidenceIndustrialDispenserOtherPebolaumProductsOtharUrbanUneRelease-i Metals RuralTankRelease
Other Inreganics
SpHhIOvarIHl Other OrganlcaExactFailureLocationUnknownor
Mulliple Failures
Ownership
MunicIpal MilItary Unknown Federal County Stale
Opetallon Type
PublIc Service Agricultural EZJUCaIIOn/ReIIg Industrial aal7 Mining
USTFOImBI11jog
Page
IMPACT ON DRINKING WATER SUPPUES
Weter Supply Wells Affected Yes No
Number of Water Supply Waits Affected_______________
Water uppIy Wells Cantamkmted lnr/ude Users Names Arfdrasses end Phone Numbers At/soft ecklitlonul sheet Wnecesserj
UST SYSTEM OWNER
UST Owner/Company
1gC.-d.e4 /ftt1kV
Point of Conthct .J 44ç
City
LiST SYSTEM 01
LJJ-Upemtar/Company
State
iare
Address
IiOO //%J4dr cl.Th
Zip Coda Telephone Number2r7-L7 W-3ii7zE
ERATOR
City
LANDOWNER AT LOCATIO
Lanr/nwner
City
JOFUSTINCIDENT
Address
Zip Code Telephone Number
Draw Sketch of Area showing two major road intersections or Attach Map
4Er r74C tj i44
Person Reportlng Inldent 1fJ Company
1il 46nas Address Pof3 Tsiwc Dale
Fonfl1 11/05 Pega2 of2
Adoress
Ztp Code Telepnona NureDer
Telephone Numbei24-c7
2005 MAP PO.U.7I
EC1t26p SHEET AREAS NO AND ESP r1ucuhnntUl.iLiAmvsr0PROJECTMORFJIEADCOMMONSShE7iaguioQW
HAALOTTh NOR Thi CAROIJNA flfla$flsurbiflflsfl
APPENDIX
UST-2 FORM
STATE USE ONLYReturncompletedformto
The DWM Regional Office located In the area whore the facility is located Send copy to the Central Office in Raleigh so that ________________the status of the tank may be changed to PERMANENTLY CLOSELY and your tank fee account can be closed out
SEE MAP ON ThE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSESNT
For more than five UST systems you may attach additional forms as needed
Permanent closure For permanent closure complete alt sections of this form
Change-In-service For change-In-service where UST systems wilt be converted from containing regulated
substance to storing non-regulated
substance complete sections II Ill IV and VIII
Effective February 1995 all UST closurelchange-ln-seMce reports must be submitted in the format provided in the UST-12 form UST closure and
change-In-services must be completed in accordance with the latest version of the Guidelines for Tank Closure copy of the UST-12 form and the
Guidelines for Tank Closure can be obtained at www.wastenotnc.org
You must make sure that USTs removed from your property are disposed of properly When choosing closure contractor ask where the tanks will be
taken for disposal Usually
USTs are cleaned and cut up for scrap metal This Is dangerous work and must be performed by qualified company Tanks
disposed of illegally In fields or other dumpaltes can leak petroleum products
and sludge into the environment If your tanks are disposed of improperly you
could be held responsible for the cleanup of any environmental damage that occurs
NOTE If release from the tanks has occurred the site assessment portion of the tank closure must be conducted under the supervision of P.E or
L.G with all closure site assessment reports bearing the signature and seat of the P.E or LG
Owner Name Corporation IndMdual Public Agency or Other Entity Facility Name or Company
Beazer 1-lomes NA
Street Address Facility ID 11 known
1300 Boulevard Suite NA
City County Street Address
Charlotte Meckienburg 919 West Morehead Street
State Zip Code City County Zip CodeNC29203-4265 Charlotte Mecktenburg 28278
Phone Number Phone Number
704-370-7200
Contact for Facility Job Title Phone No
N/A
Closure Contractor Name Closure Contractor Company Address Phone No
Jim Strattlord Gelder Thompson P0 Box 288 MIdland NC 28107 704-269-0070
Primary Consultant Name Primary Consultant Company Address Phone No
Chris Ward PG ESP associates P.A PC Box 7030 Charlotte NC 28241 704-802-2440
IV UST INFORMATION FOR REGISTERED UST SYSTEMS EXCAVATION CONDITION
Tank Size in Tank Last Last Use Permanent Change-in-Walarin Free Nolableodororvieible
ID No Gallons Dimensions Contents Date Close Date ServIce YXIIORNO Ye No Yes NoDate
El El
El El El El_D
El00El El00ElDO El
VI UST IWORMA11CJ FOR UNRLGISTERED LIST SYSTEiviS VII EXCAVATION CONDITION
Tank Size In Tank Last Last Use Permanent Tank Owner Walerin Free No able odor or fsIbeIDNoGallonsDimensionsContentsDateCloseDateNameeXcevSlIDflproductsoilccnarrinattonYesNoYesNoYeaNo900ft.x ft GasolIne NA 6/19107 El II
1500 ft 10 ft Dlelsel Diet NA 6/19/07 El El
El 000 DO
El El El 00 El
El DO
___ItIIUN
cartl1 under penalty of iaw that have personally examIned and am familiar with the Information submitted In this and all attached documents and thatbased on my inquiry of those Individuals Immediately responsible for obtaining the Information Jelieve that the Itted information Is true accurate andcomplete
PrInt name and official title of owner or owners authorized representative ihatureChrisupherJWardPUDepartmentManagerESMsociatcsP.A _________
UST-2 Rev 11/2006
LD
Date Received_________
If the tank owner address Is different from the one listed In Section then enter the street address city state zip code and telephone no below
Date Signed
8/8/2007
APPENDIX
TAXK DISPOSAL MANiFEST
Environmental and Industrial ServicesIJP.O Box 484 High Point NC Phone [phone] FAX [phone]
TANK DISPOSAL MANIFEST
Tank Owner/Autborzed Representative Name and Mailing Address
cMeiuc cL/
Tank Owner/Authorized Representative Contact
Phone
Description Of Tanks
Tank No pacity Previous Contents Commentsjq
7cv
-.....
...-
Tank Owner/Authorized Representative Certication The undersigned cerdfies that the above listed storagetankshavebeenremovedfromthepremisesofthetankàvner
rinted/Typed Name Signature Month/Day/Yea
Transporter The undersigned certifies that the above listed storage tanks have been transported to ADEnvironmentalandIndustrialServjces2718UwharijeRoadArchdaleN.C 27263
PriiueTyped Name iSjjnature Monrh/Day/Y
thsposal Certification The unde1sgtd certifies that the above-named storage tanks have been cutintoscrap pieces and accepted by
the metal recycling facility
Recycling Facility t4 ccidx.r
Prinledrryped Name Szgnature tJ Month/Day/Year
APPENDIX
PRODUCT MATERIAL MANIFEST
AQ1OI
Document NoMATERIALEnvironmentaland___________________
MANIFEST Industrial Services Ilic Page of
...EMERGENcy PHONE NO POST OFFICE BOX 484 ThL 336 434-7750 AD
BOO 434-7750 FilCH POIN.1 NC 27261 FAX [phone]
_T GENERATOR INFORMATION
Name US EPA ID No ______
Street Address Mailing Address Phone No1LJLf D3/4
Contactiio14
ESCRIPT1ON OF MATERIALS
USDOT Proper Shipping Name Hazard UN NA Packing Containers Total
HM Complete All Items for Hazardous Materials Class or Div 10 No Group QIy Type Quantity WI Vd
for I/1 fr1/ij J%i/7j-i2.I Co
_______________
ADDITIONALINFORMATION ...ERG No
opMii1trt 5tck.
GENERATORS CERTIFICATION
Facility hereby acknowlelfge recplpt of the materials covered by this manifest
ENVIRONMENTAL AND INDUSTRIAL SERVICES except for any disc epancy noted below
2718 UWRAJRfF ROAD su nature
rr C0-
ARCILDALE NC 27263 es Routirio CLdes l.Hàndliæa.Mathd5
Facility or
EPA ID No NCD986232221
.Ti
-s-----
mat This epioperlycfassifd.described packaged riced as led an
proper condition for transportation Taccorthng to the applicable regulations
of the Departmeril of Transportation further certify
hat none of the materials descnbed above are hazardous waste as defined by EPA 40 CFR Part 261 or any applicable state law
and unless specifically identified above the materials contain loss than 1000 ppm total halogens and do not contain quantifiable
Ieælà ppm of PCBs asdtined.by EPA 40.cFR Parts 279 and 761 ...5.
.t Mo.DaIYr/1071
Transporter or Unit No
EPA ID No 4CE9862222Jp
Phone [phone] J----
hereby acknowledge receipt or thfl above-described materials for transpr
from the generator silo listed above
...._..I t..i ..V71 -qI/7 .-o5
Signature /f L4-L.f 1.tiL.f..t._1 Shipment Date
hereby dcoJdgo that the above-described materials wers received
from the generatoyitand were transported to the falIitjilMed below
Signature DehlDate
r.336 434-7750
Th.Contact -....5
ERIC McMANLJS
APPENDIX
SITE PHOTOGRAPHS
MOREHEAD COMMON SITE AREA NO
APPENDIX
ESFS SOP
STANbARD OPERATING PROCEDURE
SOP-6
SOIL SAMPLE COLLECTION
ESP Associates PA Revision bate 3/7/06
This standard operating procedure SOP covers the collection of soil sample for
laboratory analysis
Follow these steps when collecting the soil sample unless
otherwise instructed by the project manager
Gather needed field supplies noted below
Confirm lob cooler contains needed sample containers fill cooler with
ice
Upon arriving at site check in with the property owner or company
representative
becontaminate the stainless steel hand auger before and between sample
collection by washing with Alconox soap and scrub brush rinsing with
distilled water and spraying with Isopropyl alcohol Wrap clean sampler
in aluminum foil
Wear disposal latex or nitrile gloves and change into new pair between
samples
buring advancement of the hand auger collect soil samples at regular
intervals for describing lithology Note lithology and other
characteristics of soils in field book relative to depth
II appropriate place representative portion of soil sample into
resealable plastic bag label with boring number and depth interval and
allow to equilibrate Screen soil in bag for volatile organics using
an OVA
or Hnu Enter results into field book
Advance hand auger boring to previously specified sampling depth
Collect soil sample from this depth and place in laboratory provided
containers Label containers with boring number and sample depth usingthefollowingsamplingschemei.e B-i ft B-i 10 ft 8-2 ft etc
benote boring location in field book relevant to pertinent site features10Followingcollectionofthesoilsamplesabandonallboreholes5feet or
greater in depth with cement grout
11 Complete and sign the labs chain-of-custody12Keepthesamplecoolerinsecurelocation until delivered under normal
chain-of-custody procedures to laboratory
SOP-6 501/5aniple Collection Revision bate 3/7/06
ESP Associates Page of
SUPPLIES
SOP-6
Stainless steel hand auger with needed extensions or sampling
spoon
OVA or Hnu
Measuring tape
Plastic zip-lock bags
Isopropyl alcohol
bistilled water
5-gallon wash bucket scrub brush and Alcoriox soap
Cement with wheel barrow for mixing
Cooler with sample containers and chain-of-custody
Ice
Permanent marker
bisposable gloves
Knife
Field book
Site plan with site specific sampling instructions
Camera
APPENDIX
PRISM LABORATORY DATA REPORTS
1e2aU7
Case NarrativePRISM
rrri1t LADORATORES.INC
Date 06/29/07 Client Project ID Morehead Commons No
Company ESP Associates PA Prism COC Group No G0607589
Contact Chris Ward Collection Dates 06/20107
Address P.O Box 7030 Lab Submittal Dates 06/20/07
Charlotte NC 28241
This data package contains the analytical results for the project identified above and includes Case Narrative Laboratory Report
and Quality
Control Data totalIng 44 pages chain-of-custody is also attached for the samples submitted to Prism for this projeci
Data qualifiers are flagged individually on each sample key reference for the data qualifiers appears at the end of this case narrative Qualitycontrolstatements and/or sample specific remarks are included in the sample comments section of the laboratory report for each sampleaffected
Semi Volatile Analysis
No Anomalies Reported
Volatile Analysis
Malysls note br Q24604 MSD C9-C12 Aliphatics Recovery above the control limits
Metals Analysis
Analysis Note for Q24537 Method Blank Lead MB RL of 1.0 mg/kg reported for associated samples
Analysis Note for Q24537 MS Chromium Matrix interference is suspected MS recovery outside of the control limits Post
digeslion spike recovery 72%Is outside the acceptance limits 75-125%
Analysis Note for 024537 MS Lead MS recovery outside of the control limits Post-digestion spike recovery 80%Is within the
acceptance limits 75-125%
Analysis Note for 024537 MS0 Chromiuni Matrix Interference is suspected
Analysis Note for 024537 MSD Lead Matrix interference Is suspected
WtLab and Micro AnaIyss
N/A
Please call if you have any questions relating to this analytical report
Date Reviewed by fita Gilleiand Project Manager An ela sh
Signature O.kA -..A 2t4 oL Signature ______
Review Date Q6/29/07 Approval Date
Data Qualifiers Key Reference
Compound also detected In the method blank
Resuti outside of the QC limits
D0 Compound diluted out
Estimated concentration calibration range exceeded
The analyte was positively identified but the value is estimated below the reporting limit
Estimated concentration with high bias
Estimated concentrafton with low bias
matrix effect is present
06/29/07/
Notes This report should not be reproduced except In its entirety without the writtten consent of Prism Laboratories Inc The results in thisreportrelateonlytothesamplessubmittedforanalysis
449 SprlngbmokRoad P.O 9ox 240543 Charlotte NC 282240403
Phone [phone] Tot Free 800/529-6364 Fec 704/529-0409
Percent Solids Determination
Percent Solids
No.402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735 06/29/07
Project ID Marehead Commons No Client Sample ID WS-1
Prism Sample 10 185081
Sample Matrix Sail coc Group G06Q758
Time Collected 06/20/07 1330
Time Submitted 06/20/07 1635
Sample Welpht Determination
Weight Blsulfate
Weight Blsulfate
Weight Methanol
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
81.9 SM2540 06/25/07 1745 Lthao
Ibrown
brown
thrown
5.98
5.52
4.93
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Volatile Organic Compounds by SC/MS
1.1-Tjichloroethane
11 .22-Tetrachloroathane
11 2-Trichloroethane
1-Dlchloroelhane
1-Dichloroethene
1-Dlchloropropene
t23-Trlchlorobenzene
123-Trichioropropane
24-Trlchlorobenzene
12.4-Tiimethyibenzene
2-Dlbromoethane EDB
2-Dichiorobenzerie
2-Dichloroethane
2-Dlchloroprcpane
35-Trlmethylbanzene
3-Dlchlorobenzene
3-Dlchloropropane
4-Dlchlorobenzene
22-Dichioropropane
2-Chlorotaluene
5035
5035
5035
82608
82609
82606
8260B
8260B
82606
8260B
8260B
82608
82608
8260B
82608
82608
8260B
8260B
82608
82608
82608
82506
82608
0.0055 0.00031
0.0055 0.00056
0.0055 0.00034
0.0055 0.0004
0.0055 0.00042
0.0055 0.00049
0.0055 0.00061
0.0055 0.00049
0.0055 0.00053
0.0055 0.00042
0.0055 0.0001
0.0055 0.0003
0.0055 0.00055
0.0055 0.00041
0.0055 0.00046
0.0055 0.00048
0.0055 0.00038
0.0055 0.00043
0.0055 0.00028
06/2707 000
06/27107 000
06/27/07 000
06/27/07 148 erussell 024552
0627/07 148 erussetl 024552
06/27/07 148 erussell 024552
06/27/07 148 erussell 024552
06/27107 148 erussell Q24552
06/2707 148 erussell 024552
06/27107 148 erussell 024552
06/27/07 148 erusseli 024552
06/27/07 148 erussell 024552
06/27/07 148 erussell 024552
06/27/07 148 erussell 024552
06/27/07 148 arussell 024552
06/27/07 148 erusset 024552
0627/07 148 erussell 024552
06/27/07 14B erussell 024552
06/27/07 148 enissell 024552
0627/07 148 erussell 024552
06/27/07 148 erussall 024552
06/27107 148 erussell 024552
0627/07 148 enisseli 024552mg/kg 0.0055 0.00041
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224O543
Phone [phone] Toil Free Number 1-800/529-6364 Fax [phone] Page of 35
TuIIMciAiiiyIkI En1nW8luiln
ESP Associates PA
Attn Chis Ward
Box 7030
Charlotte NC 28241
This report should riot be reproduced except In ita entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800529-6364 Fax [phone]
NC Certification No 402
SC Certification Mo 99012
NC Orinking Water Cert No 37735
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 185081
Sample Matrix Soil coc Group G0607589
Time Collected 06/20/07 1330
Time Submitted 06/20/07 1635
Parameter Result Units Report MDL Dilution Method AnalystAnalysis Batch
Limit Factor Date/Time ID
2-Hexanone BRL mg/kg 0.055 0.00055 826DB 05/27/07 148 erusseli 024552
4-Chiorotoluene BRL mg/kg 0.0055 0.00029 826DB 00127/07 148 enissell 024552
4-Methyl-2-pentanone MIBK BRL mg/kg 0.055 0.00055 82608 06/27/07 148 erussell 024552
Acetone 0.11 mg/kg 0.055 0.0022 826DB 06/27/07 148 erussell 024552
Benzene BRL mg/kg 0.0033 0.00044 826GB 06/27/07 148 enissell 024552
Bromobenzene BRL mg/kg 0.0055 0.00039 826DB 06/27/07 148 erussell 024552
Bromochloromethane BRL mg/kg 0.0055 0.00033 8260B 06/27/07 148 erusseli 024552
Bromodichioromethane BRL mg/kg 0.0055 0.00049 826DB 06/27/07 148 enissell 024552
Bromoforrn BRL mg/kg 0.0055 0.00041 826DB 00/27/07 148 erussell 024552
Bromomethane BRL mg/kg 001 0.00064 826DB 06/27/07 148 orussell 024552
Carbon tetrachloride BRL mg/kg 0.0055 0.00032 82608 06/27/07 148 erusseft 024552
Chlorobenzene BRL mg/kg 0.0055 0.00042 826GB 06/27/07 148 erussell 024552
Chlorodlbromomethane BRL mg/kg 0.0055 0.00038 8260B 06/27/07 148 erussell 024552
Chloroethane BRL mg/kg 0.011 0.00045 82608 06/27/07 148 erusseil Q24552
Chloroform BRL mg/kg 0.0055 0.00041 826DB 06/27/07 148 erussali 024552
Chloromethane BRL mg/kg 0.0055 0.00039 82608 06/27/07 146 erussell 024552
ole-I 2-Dlchloroetherie BRL mg/kg 0.0055 0.00024 826DB 06/27/07 148 enissell 024552
cls-13-Dichloropropene BRL mg/kg 0.0055 0.00035 826GB 06/27/07 148 erussell 024552
Dlchlorodlfluorometharie BRL mg/kg 0.0055 0.0012 826DB 06/27/07 148 erussell 024552
Ethylbenzene BRL mg/kg 0.0055 0.00039 828DB 05127/07 148 erussell Q24552
Isopropyl ether IPE BRL mg/kg 0.0055 0.00019 826DB 06/27/07 148 erussell 024552
lsopropylbenzene BRL mg/kg 0.0055 0.00044 826GB 06/27/07 148 erussell 024552
mp-Xylenes BRL mg/kg 0.011 0.00077 82608 0627/07 148 erussell 024552
Methyl ethyl ketone MEK BRL mg/kg 0.11 0.0015 826DB 06/27/07 148 ewssell 024552
Methyl t-butyl ether MTBE BRL mg/kg 0.011 0.00032 82608 06/27/07 148 erussell 024552
Methylene chloride BRL mg/kg 00055 0.00045 82608 08/27/07 148 erussell 024552
n-Butylbenzene BRL mg/kg 0.0055 0.00044 82608 05/27/07 148 erussell 024552
Page o135
NC Certification Na 402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735 06/29/07
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 185081
Sample Matrix Soil COG Group G0607589
Time Collected 06120107 1330
Time Submitted 06/20/07 1635
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
n-Propylbenzene
Parameter Result Units Report MDL Dilution Method
Limit Factor
Analyst Batch
ID
Analysis
Date/Time
BRL mg/kg 0.0055 0.00033 826DB 06/27/07 148 erussell 024552
BRL mg/kg 0.011 0.00064 82608 06/27107 148 erussell 024552
BRL mg/kg 0.0055 0.00033 82608 06/27/07 148 erussell Q24552
BRL mg/kg 0.0055 0.00045 8260B 06/27/07 148 erussell 024552
BRL mg/kg 0.0055 0.00035 82608 06/27/07 148 enisset 024552
BRL mg/kg 0.0055 0.00055 626DB 06/27/07 148 eiussell 024552
BRL mg/kg 0.0055 0.00034 826GB 06/27/07 148 erusseli 024552
BRL mg/kg 0.0055 0.00095 8260B 06/27/07 148 enisseli Q24552
BRL mg/kg 0.0055 0.00038 82608 06127/07 148 erussell 024552
BRL mg/kg 0.0055 0.00042 8260B 06/27/07 148 erussell 024552
BRL mg/kg 0.0055 0.00039 826GB 06/27/07 148 erusselt 024552
BRL mg/kg 0.0055 0.00033 8280B 06/27/07 t48 erussall 024552
BRL mg/kg 0.0055 0.00045 826DB 06/21/07 148 erussell 024552
BRL mg/kg 0.028 0.0020 82608 06/27/07 148 erussell 024552
BRL mg/kg 0.0055 0.00071 826DB 06/27/07 146 enissell 024552
Naphthalene
o-Xylerte
p-lsopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachioroethena
Toluene
trans-I 2-Dlchloroethene
trans-13-Dlchloropropene
Trichioroethene
Trichiorofluoromethane
Vinyl acetate
Vinyl chloride
Semi-volatile Organic Comnotinds by GC/MS
124-Trichlorobenzene BRL mg/kg
12-Dlchlorobenzene BRI mg/kg
13-Dichiorobeozene BRL mg/kg
14-Dlchlombenzene BRL mg/kg
245-Trichiorophenol BRL mg/kg
246-Trichiorophenol BRL mg/kg
Surrogate Recovery Control Umits
Bromofluorobenzene 101 77-128
Dlbromoflucromethane 98 67 143
Toluene-ciB 104 81-128
0.40
0.40
0.40
0.40
0.40
0.40
0.040
0.030
0.029
0.038
0.041
0039
8270C
8270C
8270C
8270C
8270C
8270C
06/27/07 1504 kcamplgotto
06/27/07 1504 kcamplgotto
06/27/07 1504 kcamplgotto
06/27/07 1504 kcamplgotto
06/27/07 1504 kcamplgotto
06/27/07 1504 kcampfgotto
024556
024556
024556
024556
024556
024556
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-5304 Fax [phone] Page of 35
AyJJAEw1wmtiS
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
This report should not be reproduced except In its entirety without the written consent or Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 185081
Sample Matrix Soil COG Group G0607589
Time Collected 06/20/07 1330
Time Submitted 06/20/07 1635
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
24-Dichiorophencl BRL mg/kg 0.40 0.034 8270C 06127/07 1504 kcamplgotto 024556
24-Dimethylphenol BRL mg/hg 0.40 0.039 827CC 06/27/07 1504 kcamplgotto 024556
24-Dinitmphenol BRL mg/kg 2.0 0.045 827CC 06127/07 1504 kcamplgotto 024556
24-Dinitrololuene BRL mg/kg 0.40 0023 6270C 05/27/07 1504 kcamplgotlo 024556
26-Dinltrotoluene BRL mg/kg 0.40 0.043 827CC 06/27/07 1504 kcamplgoto 024555
2-Chloronaphthalene BRL mg/kg 0.40 0.041 827CC 06/27/07 1504 kcampIQctto 024556
2-Chiorophenol BRI mg/kg 0.40 0.032 827CC 06/27/07 1504 kcamplgotto 024556
2-Methylnaphthalene BRL mg/kg 0.40 0.032 8270C 06/27/07 1504 kcamplotto 024556
2-Methyiphenol BRL mg/kg 0.40 0.038 6270C 06/27/07 1504 kcamplgouo Q24556
2-Nitrophenol BRL mg/kg 0.40 0.048 827CC 06/27/07 1504 kcampigctto 024555
34-Methylphenoi BRL mg/kg 0.40 0.041 827CC 06/27/07 1504 kcamplgotto 024556
33-Dlchtorobenzidlne BRL mg/kg 0.80 0.025 827CC 06/27/07 1504 kcamplgofto 024556
46-Dinltro-2-methylphenol BRL mg/kg 2.0 0.024 827CC 06/27/07 1504 kcampl9otto 024556
4-Bromophenylphenylether BRL mg/kg 0.40 0.038 827CC 06/27107 1504 kcamplgotto 024556
4-Chloro-3-methyiphenol BRL mg/kg 0.80 0.029 827CC 06/27/07 1504 kcamplgotto Q24555
4-Chloroaniline BRL mg/kg 0.40 0.051 827CC 06/27/07 1504 kcampigoto 024555
4-Chiorophenyiphenylether BRL mg/kg 0.40 0.025 827CC 06/27/07 1504 kcamplgotb 024556
4-Nitrophenot BRL mg/kg 2.0 0.027 8270C 06/27/07 1504 kcemplgolto 024556
Acenaphthene BRL mg/kg 0.40 0.039 827CC 06/27/07 1504 kcamplgottu 024556
Acenaphthylene BRL mg/kg 0.40 0.040 827CC 06/27/07 1504 kcamplgotto 024556
Anthracene BRL mg/kg 0.40 0.030 8270C 06/27/07 1504 kcamplgotto 024556
Azebenzene BRL mg/kg 2.0 0.037 8270C 06/27/07 1504 kcamplgcflo 024556
Benzoaanthracerje BRL mg/kg 0.40 0.056 827CC 06/27/07 1504 kcamplgolto 024556
Benzoapyrene BRL mg/kg 0.40 0.046 827CC 06/27/07 1504 kcamplgotto Q24556
Benzobfluoranthene BRL mg/kg 0.40 0.018 827CC 06/27/07 1504 kcamplgotto Q24555
Benzoghjperylene BRL mg/kg 0.40 0.019 827CC 06/27/07 1504 kcamplgctlo 024556
Benzokfluoranthene ERL mg/kg 040 0.033 827CC 06/27/07 1504 kcamplgotjo 024556
Page of 35
Fu urvkn AnIylcI EnvbnmntI ottIan
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Benzolc acid
Benzyl alcohol
Bls2-chloroethoxymethane
BIs2-chioroethylether
Bls2-chlorolsopropyelher
Bls2-ethylhexylphthalate
Butylbonzylphthalate
Chrysene
Dl-n-butylphthalate
Dl-n-cctylphthalate
Dibenzoahanthracene
Dlbenzoluran
Dlethylphthalate
Dlmethylphthalate
Fluoranthene
Fluorene
Hexachlorobenzena
Hexachiorobutadlene
Hexachlorocyciopentadlene
Hexachiorcethane
lndeno123-cdpyrene
Isophorone
N-Nltrosodl-n-propylamlne
N-Nitrosodlphenylamlne
Naphthalene
Nitmbenzene
Pentachiorophenol
06/27107 1504 kcampIgoto 024556
06/27/07 1504 kcamplgottc 024556
05/27/07 1504 kcamptgotlo 024556
06/27/07 1504 kcamplcttc 024556
06/27/07 1504 kcarnplgotlo 024556
06/27107 1504 kcamplgotto 024556
06/27/07 1504 kcarnplgotto 024556
06/27/07 1504 kcamplgotto 024556
06/27/07 1504 kcamplgotto 024556
06/27/07 1504 kcamplgouo Q24556
06/27/07 1504 kcamplgDtlo 024556
06/27/07 1504 kcamplgQttc 024555
06/27/07 1504 kcwnplgotto 024556
06/27/07 1504 kcamplgattc 024556
06/27/07 1504 kcamplgotto 024556
06/27/07 1504 kcarnplgotio 024556
06/27/07 1504 kcamplgotto 024556
06/27/07 1504 kcornplgotlo 024555
06/27107 1504 kcampigotlo 024556
06/27/07 1504 kcamplgutto 024556
06/27/07 1504 kcamplgotlo 024556
06127/07 1504 kcarnplgolto 024556
06/27/07 1504 kcamplgoflo 024556
06/27/07 1504 kcaniplgotlo 024556
06/27/07 1504 kcamplgotto 024556
06/27/07 1504 kcamplgotto 024555
06/27/07 1504 kcampl9otI 024558
This report should not be reproduced except In Its entirety without the written consent of Prism l2boratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 185081
Sample Matrix Soil coc Group G0607589
Time Collected 06/20/07 1330
Time Submitted 06/20/07 1635
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
BRL mg/kg 2.0 0.17 827CC
BRL mg/kg 0.80 0.042 82700
BRL mg/kg 0.40 0.046 827CC
BRL mg/kg 0.40 0.044 827CC
BRL mg/kg 0.40 0.034 827CC
BRL mg/kg 0.40 0.020 827CC
BRL mg/kg 0.40 0.025 827CC
BRL mg/kg 0.40 0.067 827CC
BRL mg/kg 0.40 0.018 827CC
BRL mg/kg 0.40 0.030 827CC
BRL mg/kg 0.40 0.040 82700
BRL mg/kg 0.40 0.034 82700
BRL mg/kg 0.40 0.025 827CC
BRL mg/kg 0.40 0.027 82700
BRL mg/kg 0.40 0.028 82700
BRL mg/kg 0.40 0.024 82700
BRL mg/kg 0.40 0.021 82700
BRL mg/kg 0.40 0.039 827CC
BRL mg/kg 0.40 0.043 827CC
BRL mg/kg 0.40 0041 827CC
BRL mg/kg 0.40 0.041 82700
BRL mg/kg 0.40 0.036 8270C
BRL mg/kg 0.40 0.046 827CC
BRL mg/kg 0.40 0.020 82700
BRL mg/kg 0.40 0.044 827CC
BRL mg/kg 0.40 0.039 82700
9RL mg/kg 2.0 0.034 82700
Page of 35
ivIcAnIytkI EnnmnbI5au
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
WS-i
185081
60607589
06120107 1330
06/20/07 1635
Surrogate recovery was outside of the control limits Matrix interference is suspected
Sample Preparation 30.OBg mL 3550B 06/23107 900 dpape P18716
Extractable Petroleum Hydrocarbons by GC-FID
Cl 1-C22 Aromatics BRL mg/kg
C19-C36 Aliphatics BRL mg/kg
C9-C18 Aliphatics BRL mg/kg
na1ysis Note for C1l-C22 Aromatics
Sample Preparation
Adjusted value
10.24 rnL EPH 06/25/07 1200 dpope
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
Parameter Result Units MDL MethodReportDilution Analysis Batch
Limit Factor Date/Time ID
Phenanthrene BRL mg/kg 0.40 0.020 827CC 06/27/07 1504 kcampgotto 024555
Phenol BRL mg/kg 0.40 0.044 827CC 06/27/07 1504 kcamplgotto 024555
Pyrene BRL mg/kg 0.40 0.027 8270C 06/27/07 1504 kcamplgoLto 024556
Analyst
Surrogate Recovery Control Limits
246-Tiibromophenol 99 25.123
2-Fluorobiphenyl 86 21 108
2-Flucropherici 78 14.89
Nltrobenzene-d5 86 14-103
Phenol-d5 83 13-95
Teihenyl-d14 142 41 136
12 6.4 MADEP EPH 0627/07 1003 grappacciotl 024555
12 1.8 MADEP EPH 06/27/07 1003 grappaccloll 024555
12 3.8 MADEP EPH 06/27/07 1003 grappaccloJl 024555
P18724
Metals by ICP
Chromium
Lead
Surrogate Recovery Control Limits
o-Terphenyl 93 40 140
1-Chloro-octadecane 107 40 -140
2-Bromonaphthalene 128 40 140
2-Fluoroblphenyl 134 40 140
37 mg/kg 0.27 0.016 601DB 06/25/07 2056 mcampbeli
9.0 mg/kg 1.1 0.022 60108 06/25/07 2056 mcampbeI
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc449SprlngbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6354 Fax [phone]
024537
024537
Page of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Sample Preparation 2.29 50 mL 30508 06/25/07 915 jhoppel P18720
Volatile Petroleum Hydrocarbons by GC-P1D/F1D
CS-Ca Aliphalics BRL mg/kg 6.1 1.2 MADEP VPH 06/27/07 2341 hwagner Q24604
C9-ClOAmmatlcs BRL mg/kg 6.1 0.037 MADEP VPU 06/27/07 2341 hwagner Q24604
C9-C12 Aliphatics BRL mg/kg 6.1 1.9 MADEP VPH 06/27/07 2341 hwagner Q24504
Analysis Note for C5-CB Aliphatics Adjusted value
Analysis Note for C9-C12 Aliphatics Adjusted value
Surrogate Recovery Control Limits
25-Dibromotoluene-FID 111 70-130
25-Dibromotoluene-PID 79 70 130
arnple Weight Determination
WeIght 20.43 MADEP VPK 06/25/07 000 brown
WeIght 19.05 MADEP VPI-I 06/25/07 000 thrown
Sample Comments
BRL Below Reporting Limit
J-Estimated value between the Reporting Umit and the MDL
The results Th this report relate only to the samples submitted for analysis and meet stale certification requirements other thanWELACcertificationexceptforthoseinstances indicated in the case narrative endfcir test comments
All results are reported one dry-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6354 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil coc Group
Time Collected
Time Submitted
wS-1
185081
G0607589
06/20/07 1330
06/20107 1635
Page of 35
Percent Solids Determination
Percent Solids
NC Certification No 402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 31735 06129107
Project ID Moreheaci Commons No Client Sample ID WS-2
PrIsm Sample ID 185082
Sample Matrix Soil COC Group G0607589
Time Collected 06/20/07 1345
Time Submitted 06/20/07 1635
Sample Weight Determination
Weight Bisulfate
Weight Bisuifate
Weight Methanol
ESP Associates PA
Atm Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
80.1 SM2540 06/25/07 1745 Uhao
5.59 5035 06/27/07 000 Ibrown
5.64 5035 06/27/07 000 Ibrown
5.59 5035 06/27/07 000 brown
Volatile Organic Compounds by GCIMS
111-Trichloroethane BRL mg/kg 0.0055 0.00031 826DB 06/27/07 219 eruselI 024652
1122TetrachIoroethane BRL mg/kg 0.0055 0.00056 82608 05/27/07 219 erusseil 024552
112-Trlthioroethane BRL mg/kg 0.0055 0.00034 826DB 06/27/07 219 ensset 024552
11-Dlchloroethane BRL mg/kg 0.0055 0.0004 826DB 06/27/07 219 erusseli 024552
11-Dlchloroethene SRI mg/kg 0.0055 0.00042 826DB 06/27/07 219 ewsseli 024552
11-Dlchtoropropene BRL mg/kg 0.0055 0.00049 826DB 06/27/07 219 erussell 024552
12.3Trichlorobenzene BRL mg/kg 0.0055 0.00061 826DB 06/27/07 219 erusseli 024552
12.3-Trichloropropane BRL mg/kg 0.0055 0.00049 826DB 06/27/07 219 erussetl 024552
124-Trichlorobenzene SRI mg/kg 0.0055 0.00053 826DB 06/27/07 219 erusseil 024552
124-Trimethylbenzene BRL mg/kg 0.0055 0.00042 82608 06/27/07 219 enissell 024552
12-Dibromoethane EDB BRL mg/kg 0.0055 0.0001 826DB 06127/07 219 erussdll 024552
12-Dlchlorobenzene BRL mg/kg 0.0055 0.0003 826DB 06/27/07 219 erusselt 024552
12-Dichioroethane BRL mg/kg 0.0055 0.00055 826DB 06127/07 219 erussetl 024552
12-Dichioropropane BRL mg/kg 0.0055 0.00041 826DB 06/27/07 219 enjsseti 024552
135-Triniethylbenzene SRI mg/kg 0.0055 0.00046 a26o8 08/27/07 219 erussell 024552
13-Dlchlorobanzene BRL mg/kg 0.0055 0.00048 82508 06/27/07 219 erussetl 024552
13-Dichioropropane SRI mg/kg 0.0055 0.00038 82808 06/27/07 219 erussetl 024552
14-Dlchlorobenzene BRL mg/kg 0.0055 0.00043 826DB 06/27/07 219 erussell 024552
22-Dichioropropane BRI mg/kg 0.0055 0.00028 826DB 06/27/07 219 erusseil 024552
2-Chiorototuene BRL mg/kg 0.0055 0.00041 826DB 06127/07 219 enissefi Q24552
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SprlngbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6384 Fax [phone] Page of 35
NC CertificatIon No.402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735 06/29107
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224.0543
Phone [phone] Toll Free Number 1-8001529.6364 Fax [phone]
FH Si AlytEnvknmnW S1itIn
ESP Associates PA
Atm Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 185082
Sample Matrix Soil COC Group G0607589
Time Collected 06/20/07 1345
Time Submitted 06/20/07 1635
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
2-Hexanone BRL mg/kg 0.055 0.00058 82608 05/27/07 219 erussell 024552
4-Chiorotoluene BRL mg/kg 0.0055 0.00029 62608 06/27/07 219 erussell 024552
4-Methyl-2-pentanone MIBK BRL mg/kg 0.055 0.00055 82603 06127/07 219 erusseli 024552
Acetone o.io mg/kg 0.065 0.0022 82803 06/27/07 219 erussell 024552
Benzerie BRL mg/kg 0.0033 0.00044 82608 06/27/07 219 enissell 024552
Bromobenzene BRL mg/kg 0.0055 0.00039 82603 06/27/07 219 erussell 024552
Bromochioromethane BRL mg/kg 0.0055 0.00033 82603 06/27/07 219 erassell 024552
Bromodlchloromethane BRL mg/kg 0.0055 0.00049 826DB 0627/07 219 erusseli 024552
BromoIorrn BRL mg/kg 0.0055 0.00041 82608 06/27/07 219 erussefl 024552
Bromornethane BRL mg/kg 0.011 0.00064 826DB 06/27/07 210 erussell 024552
Carbon tetrachlorkie BRL mg/kg 0.0055 0.00032 82608 06/27/07 219 erussell 024552
Chlorobenzene BRL mg/kg 0.0055 0.00042 826DB 06/27/07 219 erussell 024552
Chiorodibromomethane BRL mg/kg 0.0055 0.00038 82608 06/27/07 219 erussell 024552
Chloroethane BRL mg/kg 0.011 0.00045 826DB 06/27/07 219 enissell 024552
Chloroform BRL mg/kg 0.0055 0.00041 82608 06/27/07 219 enisseil 024552
Chioromethane BRL mg/kg 0.0055 0.00039 826DB 06/27/07 219 enissell 024552
cls-12-Dlchloroethene BRL mg/kg 0.0055 0.00024 826DB 06/27/07 219 erussell 024552
cis-13-Dlchloropropene BRL mg/kg 0.0055 0.00035 82608 0627/07 219 erussell 024552
Dichiorodlfluoromethane BRL mg/kg 0.0055 0.0012 82608 06/27/07 219 erussell 024552
Ethylbenzene BRL mg/kg 0.0055 0.00039 826DB 06/27/07 219 erusseil Q24552
lsopropyi ether IPE BRL mg/kg 0.0055 0.00019 826DB 06/27/07 219 erussell 024552
tsopropylbenzene BRL mg/kg 0.0055 0.00044 826DB 06/27/07 219 erusseil 024552
mp-Xylenes BRL mg/kg 0.011 0.00077 826DB 06/27/07 219 orusseil Q24552
Methyl ethyl ketorie MEK BRL mg/kg 0.11 0.0015 826DB 06/27/07 219 eiussell 024552
Methyl t-butyl ether MTBE BRL mg/kg 0.011 0.00032 82608 06/27/07 219 enissell 024552
Methylene chloride BRL mg/kg 0.0055 0.00045 82608 06/27/07 219 erussell 024552
n-Butylbenzene BRL mg/kg 0.0055 0.00044 82608 06/2707 219 enissell 024552
Page 90135
Laboratory Report
06/29/07
FWI StiJ EnvImChitf
ESP Associates PA WS-2
Attn Chris Ward 185082
Box 7030 G0607589
Charlotte NC 28241 06/20/07
06/20/07
NC Certification No.402
SC Certification No 99012
NC Drinking Water Ceit No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method
1345
1635
Analyst Batch
ID
Analysis
Limit Factor Daternme
0.0055 0.00033 82609 06/27/07 219 enmscll Q24552
0.011 0.00064 826DB 06/27107 219 erussell 024552
0.0055 0.00033 826DB 06/27/07 219 erusseli 024552
0.0055 0.00045 826DB 08/27/07 219 erussell 024552
0.0055 0.00037 826DB 06/27/07 219 enissell 024552
0.0055 0.00055 82609 06/27107 219 erusseli 024552
0.0055 000034 826DB 08/27/07 219 erussell 024552
0.0055 0.00095 82608 06/27/07 219 erussel 024552
0.0055 0.00038 82009 08/27/07 219 erussell 024552
0.0055 0.00042 826DB 06/27/07 219 erussell 024552
0.0055 0.00039 826DB 06/27/07 219 erussell 024552
0.0055 0.00033 826DB 06/27/07 219 enisseil 024552
0.0055 0.00045 826GB 06/27/07 219 erusseli 024552
0.028 0.0020 826GB 06/27/07 219 erussell 024552
0.0055 0.00071 826DB 06127/07 219 erussell 024552
n-Propylbenzene BRL
Naphthalene BRL
o-Xylene BRL
p4sopropyltoluene BRL
sec-Butylbenzene BRL
Styrene BRL
tert-Butylbenzene BRL
Tetrachioroethene BRL
Toluene BRL
bans-i 2-Dichloroethene SRL
trans-i 3-Dlchloropropene BRL
Trichioroethene BRL
Trichlorofluorornethane BRL
Vinyl acetate BRL
Vinyl chloride BRL
Semi-volatile Organic Compounds by GCIMS
12.4-Trlchlorcbenzerie BRL
2-Dlchlorobenzene BRL
3-Dlchturobenzene BRL
4-Djchlorobenzene BRL
2145-Trlchlorophenol BRL
2.4.6-Trichiorophenol BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Surrogate Recovery Control Umits
Bromofiuorobenzene 110 77-128
Dibromofluoromethane 94 67-143
Toluene-dB 98 81 128
0.41
0.41
0.41
0.41
0.41
0.41
0.041
0.030
0.030
0.037
0.042
0.039
8270C
8270C
9270C
8270C
8270C
8270C
06/28/07 1015 kcampigcitto
06/28/07 1015 kcamplgotto
06/28/07 1015 kcamplgotio
06/28/07 1015 kcamplgotta
06/28/07 1015 kcampgotto
06/28/07 1015 kcamplgotlo
024556
024556
024556
024556
024556
024556
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Spririgbrook Road P.O Box 240543 Charlotte1 NC 28224-0543
Phone [phone] Toil Free Number 1-8001529-6364 Fax [phone] Page 10 of 35
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 185082
Sample Matrbc Soil COC Group 00607589
Time Collected 06/20/07 1345
Time Submitted 06/20/07 1635
24-Olchlorophenol
24-Dimethyiphertol
24-Dinitrophenol
24-Dinitrotoluene
26-Dlnltrotoluene
2-Chloronaphthalena
2-Chiorophenol
2-Methylnaphthalene
2-Methyiphenol
2-Nitrophenol
34-Methylphenol
33-Dlchlorobenzldjne
46-Dinltro-2-methylphenol
4-Bromophenylphenylether
4-Chloro-3-methylphenol
4-Chioroanlilne
4-Chiorophenyiphenylether
4-Nitrophenol
Acenaphthene
Acenaphihylene
Anthracene
Azobenzene
Benzoaanthracerie
Beflzoapyrene
Benzobfluoranthene
Benzoghjperytene
Benzokfluoranthene
06/28/07 1015 kcamplgoUo 024556
06128107 1015 kcamplotto Q24556
06/28/07 1015 kcamplgotlo 024556
06125/07 1015 kcamplgottc 024556
05/28/07 1015 kcamptgritlo 024555
05/25/07 1015 kcamplgatto Q24556
05/28/07 1015 kcamplgctln 024556
06/28/07 1015 kcamplgolto 024556
06/25/07 1015 kcamplgotto 024556
06/28/07 1015 kcamplgotto 024556
06128107 1015 kcmplgutto 024556
06/28/07 1015 kcamplgoUD 024556
06/28/07 1015 kcamplgotto 024555
06/28/07 1015 kcamplgouo 024556
06 /28107 1015 kcamplgolto 024555
06/25/07 1015 kcamptgotto 024556
06/28/07 1015 kcamplgolto 024555
06/28/07 1015 kcampgcttD 024556
06/28/07 1015 kcamplgatto 024556
06/28/07 1015 kcarnplgotto 024556
06/28/07 1015 kcamplgotto Q24556
06/28/07 1015 kcamplgotto 024556
05/28/07 1015 kcarnplgotb 024556
06/28/07 1015 kcamplgotio 024556
06128/07 1015 kcamplgotto 024556
05/28/07 1015 kcmpIgcItn 024556
06/28/07 1015 kcamplotto 024556
This report should not be reproduced except in Its entirely without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Rox 240543 Charlotte NC 2224-0543
Phone [phone] Toll Free Number 14001529-5354 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012 Laboratory Report
NC Drinking Water Cert No 37735 06129/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
BRL mg/kg 0.41 0.034 82700
BRL mg/kg 0.41 0.040 8270C
BRL mg/kg 2.1 0.046 8270C
BRL mg/kg 0.41 0.023 82700
BRL mg/kg 0.41 0.044 82700
BRL mg/kg 0.41 0.042 8270C
BRL mg/kg 0.41 0.032 82700
BRL mg/kg 0.41 0.033 82700
BRL mg/kg 0.41 0.035 82700
BRL mg/kg 0.41 0.049 8270C
BRL mg/kg 0.41 0.042 82700
BRL mg/kg 082 0.026 827CC
BRL mg/kg 2.1 0.025 827CC
BRL mg/kg 0.41 0.039 82700
BRL mg/kg 0.52 0.030 827CC
BRL mg/kg 0.41 0.052 527CC
BRL mg/kg 0.41 0.025 82700
BRL mg/kg 2.1 0.027 827CC
BRL mg/kg 0.41 0.040 827CC
BRL mg/kg 0.41 0.041 82700
BRL mg/kg 0.41 0.031 82700
BRL mg/kg 2.1 0.038 82700
0.57 mg/kg 0.41 0.057 82700
1.1 mg/kg 0.41 0.047 827CC
0.96 mg/kg 0.41 0.018 52700
0.90 mg/kg 0.41 0.020 82700
1.1 mg/kg 0.41 0.033 827CC
Page 11 of 35
Laboratory Report
06129107
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 185082
Sample Matrix Soil COO Group G0607589
Time Collected 06/20/07 1345
Time Submitted 06/20/07 1635
This report should not be reproduced except In ha entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drtriklng Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 25241
Parameter Result Units Report MDL Dilution Method
Limit Factor
Analysis Analyst Batch
Date/Time ID
Benzolc add BRL mg/kg 2.1 0.17 827CC 06/28/07 1015 kcampgotto 024556
Benzyl alcohol BRL mg/kg 0.82 0.043 827CC 06/28/07 1015 kcamptgotk3 024556
Bis2-chloroethoxymethana BRL mg/kg 0.41 0.047 52700 05/28107 1015 kcamplgotto 024556
Bis2-chloroethylether BRL mg/kg 0.41 0.045 82700 0628/07 1015 kcamplgotto 024556
Bls2-chlorolsopropylether BRL mg/kg 0.41 0.035 827CC 06/28107 1015 kcamplgotto 024556
Bls2-ethylhexylphthalate BRL mg/kg 041 0.020 827CC 06/28/07 1015 kcampoItD 024556
Butylbenzylphthaiate BRL mg/kg 0.41 0.025 82700 06/28/07 1015 kcamplgotto 024556
Chrysene 0.68 mg/kg 0.41 0.068 82700 06/2807 1015 kcamplgotto 024556
Dl-n-butylphthalate BRL mg/kg 0.41 0.019 8270C 06/28/07 1015 kcamplgotto 024556
DI-n-cctylphthaiate BRL mg/kg 0.41 0.031 82700 06/28/07 1015 hcmplgotth 024556
Dlbenzoatianthracene BRL mg/kg 0.41 0.041 827CC 06/28/07 1015 kcamplgotto 024556
Dibenzoluran BRL mg/kg 0.41 0.035 82700 06/28/07 1015 kcamplgotlo 024556
Dlethylphthalate BRI mg/kg 0.41 0.025 82700 06/28/07 1015 kcamplgollo 024556
Dlmethylphthalate BRL mg/kg 0.41 0.025 827CC 06/28/07 1015 kcamplgotto 024555
Fluoranthene 1.5 mg/kg 0.41 0.028 82700 06/28/07 1015 kcampigotto 024556
Fiucrene SRI mg/kg 0.41 0.024 82700 06/2807 1015 kcamplgotlo 024556
Hexachiorobenzene BRL mg/kg 0.41 0.021 82700 06/28/07 1015 kcamplgouo 024556
Hexachlorobutadlene BRL mg/kg 0.41 0.040 827CC 06/28/07 1015 kcamplgotto 024556
I-iaxachlorocyclopentadlene BRL mg/kg 041 0.043 827CC 06/28/07 1015 kcamplgotlo 024555
Hexachioroethane BRL mg/kg 0.41 0.042 827CC 06/28/07 1015 kcamplgoUo 024556
indeno123-cdpyrene 0.96 mg/kg 0.41 0.042 82700 06/28/07 1015 kcamplgotto 024556
Isopharone BRI mg/kg 0.41 0.037 927CC 0628/07 1015 kcamplgotto 024555
N-Nltrosodi-n-propylamlne BRL mg/kg 0.41 0.047 827CC 0828/07 1015 kcamplgotlo 024556
N-NltrosoLliphenylamine SRI mg/kg 0.41 0.021 82700 06/28/07 1015 kcamplgotto 024556
Naphthaiene BRL mg/kg 0.41 5.045 827CC 06/28/07 1015 kcamplgotto 024556
Nitrobenzene BRL mg/kg 0.41 0.040 827CC 06/28/07 1015 kcamplgotto 024556
Pentachlorophenol BRL mg/kg 2.1 0.034 82700 06/28/07 1015 kcamplgatta 024556
Page 12 of 35
Full .uvk ArudyilulA EwlnmmnL...olUui
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
Parameter
Phenanthrene
Phenol
Pyrene
Result Units Report
Limit
0.98 mg/kg 0.41
BRL mg/kg 0.41
2.5 mg/kg 0.41
MDL Dilution
Factor
0.020
0.045
0.028
Surrogate recovery
was outside of the control limits Matrix interference is suspected
Sample Preparation 30.llg lmL 35508 06/23/07 900 dpope P18716
Extractable Petroleum Hydrocarbons by GC-FID
C11-C22Aromatlcs 20 mg/kg
Cl 9-C36 Aliphatics BRL mg/kg
C9-618 Atiphatics BRL mg/kg
Analysis Note for C1l-C22 Aromatics
Sample Preparation
Adjusted value
9.78 mL EPH 06/25/07 1200 dpope
29 mg/kg 0.25 0.015 6010B 06/25/07 2113 mcampbeil
84 mg/kg 1.0 0.021 6010B 06/25/07 2113 mcampbell
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.Q Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No99012
NC Drinking Water Cert No 37735
Laboratory Report
06/20/07
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 185082
Sample Matrix Soil COG Group G0607589
Time Collected 06/20/07 1345
Time Submitted 06/20/07 1635
Method Analysis Analyst Batch
Date/Time ID
8270C 06/28/07 1015 kcamplgotto 024556
8270C 06/28/07 1015 kcamplgotto 024556
8270C 06/26/07 1015 kcarnplgotlo 024556
Surrogate Recovery Control Limits
246-Tribromophenol 115 25-123
2-Fluoroblphenyl 105 21 106
2-Fluorophenol 85 14-89
Nitrobenzene-dS 84 14-103
Phenol-d5 101 13-95
Terphenyl-d14 160 41-136
13 6.9 MADEP EPH 06/27/07 1326 gmppaccloll 024555
13 1.9 MADEP EPH 06/27/07 1326 grappaccfolt 024555
13 4.1 MADEP EPI-I 06/27/07 1326 grappacclorl 024555
P18124
Metals by ICP
ChromIum
Lead
Surrogate Recovery Control Limits
1-Chloro-octaciecane 106 40 140
2-Bromonaphthalene 91 40 140
2-Fluoroblphenyl 92 40 -140
o-Terphenyl 88 40-140
024537
024537
Page 13 of 35
NC CertificatIon No 402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cart No 37735 06/29/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Sample Preparation 2.47 50 rnL 30508 06/25/07 915 Jhoppel P18720
Volatile Petroleum Hydrocarbons by GC-PID1FID
CS-Ca Aliphatics BR mg/kg 6.2 1.2 MADEP VPH 06/2807 024
hwagnet 024604
C9-ClOAromatlcs BRL mg/kg 6.2 0.037 MADEP VPH 06128/07 024 hwagner 024604
C9-Cl2Aliphatics BRL mg/kg 6.2 1.9 MADEP VPH 06/28/07 024 hwagner Q24604
Pnalysis Note for C5-C8 Aliphatics Adjusted value
alysis Note for C9-C12 Aliphatics Adjusted value
Surrogate Recovery Control Limits
25-Dlbromotoluene-FID 119 70 130
25-Dibromototuene-PID 64 70-130
Sample Weight Determination
Weight 14.40 MADEP VPH 06/2507 000 brown
Weight 18.95 MADEP VPH 06/25/07 000 thrown
Sample Comments
SRL Below Reporting Umit
J-Estimated va/ue between the Reporting Umit and the MOL
The results In this report relate only to the samples submitted far analysis and meet sta/e certification requirements other thanNELACcertificationexceptforthose instances indicated in the case narrative and/or test comments
Al results are reported on dry-weight basis
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-2
185062
00607589
06/20/07 1345
06/20/07 1635
Angela Overcash V.P Laboratory Services
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone] Page 14 bf 35
NC Certification No 402 Laboratory ReportScCertificationNo99012
NC Drinking Water Cet No 37735 08/29/07
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 185083
Sample Matrix Soil COG Group G0607589
Time Collected 06/20/07 1400
Time Submitted 06/20/07 1635
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Percent Solids Determination
Percent Solids
5.62
5.63
5.29
5035 05/27/07 000
5035 05127107 000
5035 06/27/07 000
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
83.9 SM2540 06/25/07 1745 Llhao
Sample Weight Determination
Weight Bisulfate Ibrown
Weight Blsulfate
Weight Methanol Ibrown
Volatile Organic Compounds by GCMS
111-Trtchloroethane BRL mg/kg 0.0053 0.0003 82803 06/27/07 251 erussell 024552
1122-Tetrachioroethane BRL mg/kg 0.0053 0.00054 826DB 06/27/07 251 erussell Q24552
112-Tiichloroethane BRL mg/kg 0.0053 0.00033 82603 05/27/07 151 erussell 024552
11-Dichloroethane BRL mg/kg 0.0053 0.00038 8260B 06/27/07 251 erussell 024552
11-Dtchtoroethene BRL mg/kg 0.0053 0.0004 82803 06/27107 151 erussell 024552
11-Dichioroprupene BRL mg/kg 0.0053 0.00047 8260B 06/27/07 251 erussell 024552
123-Trlchlorobenzene BR.mg/kg 0.0053 0.00058 82603 06/27/07 251 erussell 024552
23-Trlchloropropane BRL mg/kg 0.0053 0.00047 82608 06/27/07 251 erussell 024552
124-Tnchlombenzene BRI mg/kg 0.0053 0.00051 82603 06/27/07 251 erussell 024552
124-Trfrnethylbenzene BR mg/kg 0.0053 0.0004 82603 06/27/07 251 erussell 024552
12-Dibromoethane EDB BRL mg/kg 0.0053 0.000095 8260B 06/27/07 251 russell 024552
12-Dlchlorobenzene BRL mg/kg 0.0053 0.00029 82603 05/2707 251 erussell 024552
2-Dlchloroethane BRL mg/kg 0.0053 0.00053 826DB 06/27107 251 erussell 024552
12-Dlchloropropane BRL mg/kg 0.0053 0.00039 82603 06/27/07 251 erussell 024552
135-Trimelhylbenzene BRL mg/kg 0.0053 0.00044 82603 06/2707 251 erussell 024552
3-Dlchlorobenzene BRL mg/kg 0.0053 0.00046 826DB 06127/07 251 erussell 024552
3-Dlchloropropane BRL mg/kg 00053 0.00036 82603 06/27/07 251 erussell 024552
14-Dlchlombenzene BRL mg/kg 0.0053 0.00041 82603 08/27/07 251 erussell 024552
22-Dichioropropane BRL mg/kg 0.0053 0.00026 82608 06/21/07 251 erussell 024552
2-Chlorotoluene BRL mg/kg 0.0053 0.00039 82603 08/27/07 251 erussell 024552
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Sprlnybrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-900/529-6364 Far 704/525-0409 Page 15of35
ESP Associates PA
Afr Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil coc 3roup
Time Collected
Time Submitted
WS-3
185083
G0607589
06/20107 1400
06/20/07 1635
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29107
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
2-Hexanone SRI mg/kg 0.053 0.00055 82603 0627/07 251
erusselt 024552
4-Chiorotoluene BRL mg/kg 0.0053 0.00028 82603 0627/07 251
erussell 024552
4-Methyl-2-pentanone MIBK SRI mg/kg 0.053 0.00053 826DB 06/27/07 251 erussell 024552
Acetone SRI mg/kg 0.053 0.0021 826DB 08/27/07 251 erussell 024552
Benzene BRL mg/kg 0.0032 0.00042 82603 06/27/07 251 erusseft 024552
Bromobenzene BRL mg/kg 0.0053 0.00037 826DB 0627/07 251 erusseft 024552
Bromochioromethane BRL mg/kg 0.0053 0.00032 826DB 06/27/07 251 erusselt 024552
Bromodjohiorornethane BRL mg/kg 0.0053 0.00047 82603 06/27/07 251 erusselt 024552
Bromoform BRL mg/kg 0.0053 0.00039 82603 06/27/07 251 erusseli 024552
Bramornethane SRI mg/kg 0.011 0.00061 826DB 05127/07 251 erussolt Q24552
Carbon tetrachloride BRL mg/kg 0.0053 0.00031 826DB 06127/07 251 erust 024552
Chlorobenzene BRL mg/kg 0.0053 0.0004 826DB 06/27/07 251 emsset 024552
Chlomdlbromomethane BRL mg/kg 0.0053 0.00036 826DB 06127/07 251 erusset 024552
Chioroethane BRI mg/kg 0.011 0.00043 826DB 05/27/07 251 emesefi 024552
Chloroform BRI mg/kg 0.0053 0.00039 826DB 06/27/07 251 erussefl 024552
Chioromethane BRI mg/kg 0.0053 0.00037 82603 06/27/07 251 erusseti 024552
cls-1 2-Dlchlaroethene SRI mg/kg 0.0053 0.00023 62603 06/27/07 251 erussell 024552
cls-l 3-Dlchloropropene BRL mg/kg 0.0053 0.00034 826DB 06/27/07 251 erussell 024552
Dichiorodifluoromethane SRI mg/kg 0.0053 0.0012 826DB 06/27/07 251 emseell 024552
Ethylbenzene BRL mg/kg 0.0053 0.00037 82603 0627/07 251 erussell 024552
Isopropyl ether iP SRI mg/kg 0.0053 0.00018 82603 06/27/07 251 erussall 024552
Isopropylbenzene BRL mg/kg 0.0053 0.00042 826DB 06/27/07 251 erussell 024552
mp-Xylenes BRL mg/kg 0.011 0.00074 826DB 05/27/07 251 erussell 024552
Methyl ethyl ketoneMEK SRI mg/kg Dii 0.0015 826DB 06/27/07 251 emssefl 024552
Methyl t-butyl ether MTBE BRL mg/kg 0.011 0.00031 826DB 06/27/07 251 erussett 024552
Methylene chloride SRI mg/kg 0.0053 0.00043 82608 06127/07 251 erussell 024552
n-Butylbenzene BRL mg/kg 0.0053 0.00042 826DB 06/27/07 251 erussell Q24552
Page 16 of 35
ESP Associates PA
Attfl Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil 30C Group
Time Collected
Time Submitted
WS-3
185083
G0607589
06120107 1400
06/20/07 1635
This report should not be reproduced except in its entirely without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6354 Fax [phone]
NC CertlflcaUon No 402
SC Certilicatlon No 99012
NC Drinking Water Con No 37735
Laboratory Report
06129107
Parameter Result Units Report MDL Dilution Method Analyst Batch
ID
Analysis
Limit Factor Date/Time
0.0053 0.00032
826DB 06127/07 251 erussell 024552
0.011 0.00061 826DB 06/27/07 251 erussell 024552
0.0053 0.00032 826DB 08/27/07 251 erussell 024552
0.0053 0.00043
826DB 06/27/07 251 erussetl 024552
00053 0.00035 826DB 06/27/07 251 erussetl 024552
0.0053 0.00053 82608 05/27107 251 erusseil 024552
0.0053 0.00033 826DB 06/27107 251 omseell 024552
00053 0.00091 82608 06/27/07 251 erusseil 024552
0.0053 0.00036 82608 06/27/07 251 erussell 024552
0.0053 0.0004 826DB 06/27/07 251 erussell 024552
0.0053 0.00037 8260B 06/27/07 251 erussell 024552
0.0053 0.00032 826DB 06/27/07 251 erussell 024552
0.0053 0.00043 82608 06/27/07 251 erusseti 024552
0.026 0.0019 826DB 06/27/07 251 erussell 024552
0.0053 0.00068 82608 06127/07 251 erussell 024552
n-Propylbenzene BRL mg/kg
Naphthaiene BRL mg/kg
o-Xylene BRL mg/kg
p-Isopropyltoluene BRL mg/kg
sec-Butylbenzene BRL mg/kg
Styrene BRL mg/kg
tert-Bulylbenzene BRL mg/kg
Tetrachlorcethene BRL mg/kg
Toluene BRL mg/kg
trans-I 2-Dichloroethene BRL mg/kg
trans-I 3-Dlchiorepropsne BRL mg/kg
Trichlorootheno BRL mg/kg
Tnichlorotluoromethane BRL mg/kg
Vinyl acetate BRI mg/kg
Vinyl chloride BRL mg/kg
Semi-volatile Omanic Comnounds by CC/MS
124-Trlchlorobenzene BRL mg/kg
t2-Dlchlorobenzene BRL mg/kg
13-Dlchtorobenzene BRL mg/kg
14-Dlchlorobenzena BRL mg/kg
245-Trithlnmphenol BRL mg/kg
246-TdchIorophenal BRL mg/kg
Surrogate Recovery Control Limits
Toluene-d8 101 81 -128
Brcjmofluorobenzene 100 77-126
Dlbromotluoromethane 91 67-143
0.40
0.40
0.40
0.40
0.40
0.40
0.039
0.028
0.028
0.036
0.040
0.038
8270C
8270C
8270C
8270C
8270C
B27OC
06/27/07 2010 kcampigoflo
06/27/07 2010 kcampigolb
06/27/07 2010 kcamplgotto
06/27/01 2010 kcampiotlo
06/27/07 2010 kcampi8otto
06/27/07 2010 kcamptgotb
024556
024555
024556
024556
024056
024556
Page 17 o135
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
24-Dichiorophenol
24-Dlmethyiphenol
24-Dinitrophenol
24DInitrotoluene
26-Dinltrotoluene
2-Chioronaphihatene
2-Chiorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
34-Methylphenol
33-Dlthtorobenzldlne
46-DlnItm-2-methylphenot
4-BromophenylphenyIeth
4-Chloro-3-methylphenol
4-Chioroaniline
4-Chiorophenylpi
4-Nltmphenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benwaanthracene
Benzoapyrene
8enzobfluoranthene
Benzoghlperylene
Benzokfluoranthene
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 185083
Sample Matrix Soil coc Group G0607589
Time Collected 06/20/07 1400
Time Submitted 06/20/07 1635
06/27/07 2010 kcampgotto Q24556
06/27/07 2010 kcamplgottc 024556
06127107 2010 koampigotlo 024556
06/27/07 2010 kcampigotto 024556
06127/07 2010 kcamplgotto 024556
06/27/07 2010 kcampfgotto 024556
06127107 2010 kcampigotto 024556
05/27/07 2010 koamplgotto 024556
06127/07 2010 kcampgoIto 024555
06/27/07 2010 kcamplgotto 024556
06/27/07 2010 keamplgatto 024556
06127/07 2010 kcaniplgolto 024556
06/27/07 2010 kcamplgalto 024556
06/27/07 2010 kcamplgotto 024556
06/27/07 2010 kcamplgotio 024556
06/27/07 2010 kcampigotto 024556
06/27/07 2010 kcarnpgotto 024556
06/27/07 2010 luampIgotto 024556
06/27/07 2010 kcamp/gotto 024556
06/27/07 2010 kcamplgotto 024556
06/27107 2010 kcamplgotto 024556
06/27/07 2010 kcamplgotto 024556
06/27/07 2010 kcamplgotto 024556
06/27/07 2010 koamplgotto 024555
06/27/07 2010 koamplgotto 024556
06/27107 2010 kcamplgolto 024556
06127/07 2010 kcampigolto 024556
This report should not be reproduced except in its entirety without the written consentol Prism Laboratories Inc
449 Spsingbrook Road P.O Box 240543 Charlotte NC 26224-0543
Phone [phone] Toll Free Number 1-8001529.5364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
BRL mg/kg 0.40 0.033 8270C
BRL mg/kg 0.40 0.038 8270C
BRL mg/kg 2.0 0.044 8270C
BRL mg/kg 0.40 0.022 827CC
BRL mg/kg 0.40 0.042 827CC
BRL mg/kg 0.40 0041 8270C
BRJ.mg/kg 0.40 0.031 82700
BRL mg/kg 0.40 0.031 8270C
BRL mg/kg 0.40 0.037 827CC
BRL mg/kg 0.40 0.047 827CC
BRL mg/kg 0.40 0.040 8270C
BRL mg/kg 0.79 0.025 82700
BRL mg/kg 2.0 0.024 82700
BRL mg/kg 0.40 0.037 8270C
BRL mg/kg 0.79 0.029 8270C
BRL mg/kg 0.40 0.050 827CC
BRL mg/kg 0.40 0.024 827CC
BRL mg/kg 2.0 0.026 827CC
BRL mg/kg 0.40 0.039 827CC
SRI mg/kg 0.40 0.039 827CC
BRL mg/kg 0.40 0.030 827CC
BRL mg/kg 2.0 0.037 8270C
0.12 mg/kg 0.40 0.055 8270C
0.25 mg/kg 0.40 0.046 8270C
BRL mg/kg 0.40 0.018 82700
BRL mg/kg 0.40 0.019 82700
BRL mg/kg 0.40 0032 827CC
Page 18 of 35
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Benzolc acid
Benzyl alcohol
BIs2-chloroethoxymethane
BIs2-chloroethylether
BIs2-chlorolsopropylether
Bls2-ethylhexylphthalate
Butylbenzyiphthalate
Chrysene
Dl-n-butylphthalate
Dl.n-octylphlhalate
Dlbenzoahanthracene
Dlbenzofuran
Dlethylphthalate
Dlmethylphthalate
Fiuoranthene
Fluorene
Hexachlorobenzene
Hexachiorobutadlene
Hexachiorocydopentadiem
Hexachicroethane
Indsno123-cdpyrene
Isophorone
N-NltrosodIn-propylarnine
N-Nltrosodlphenylarnlne
Naphihalene
Nltmbenzene
Pentachiorophenol
Laboratory Report
06129107
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 185083
Sample Matrix Soil COC Group G0607589
Time Collected 06/20/07 1400
Time Submitted 06/20/07 1635
BRL mg/kg 0.79 0.042
mg/kg 0.40 0.045
mg/kg 0.40 0.043
mg/kg 0.40 0.034
mg/kg 0.40 0.019
mg/kg 0.40 0.024
mg/kg 0.40 0.066
mg/kg 0.40 0.018
mg/kg 0.40 0.029
mg/kg 0.40 0.040
mg/kg 0.40 0.034
mg/kg 0.40 0.024
mg/kg 0.40 0.027
mg/kg 0.40 0.027
mg/kg 0.40 0.023
mg/kg 0.40 0.020
mg/kg 0.40 0.038
mg/kg 0.40 0.042
mg/kg 0.40 0.040
mg/kg 0.40 0.040
mg/kg 0.40 0.035
mg/kg 0.40 0.045
mg/kg 0.40 0.020
mg/kg 0.40 0.043
mg/kg 0.40 0.038
mg/kg 2.0 0033
8270C
8270C
827CC
827CC
827CC
827CC
827CC
8270C
8270C
8210C
82700
6270C
827CC
827CC
827CC
827CC
827CC
827CC
827CC
8270C
8270C
6270C
827CC
827CC
82700
This report should not be repduced except in Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road-P.O Box 240543 Charlofte NC 28224-0543
Phone[phone] Toll Free NumbeR 1-8001529-6384 Fax [phone]
AnykaI EoniniW SatuU
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
BRL mg/kg 2.0 0.17 8270C 06/27/07 2010 kcamplgotto 024556
8270C 06/27/07 2010 koamplgotto 024556
BRL
BRL
BRL
BRL
BRL
0.14J
BRL
BRL
BRL
BRL
BRL
BRL
0.24
BRL
BRL
BRI
BRL
HRL
BRL
BRL
BRL
BRL
BRL
BRL
aRt
06/27/07 2010 kcamplgotto 024556
06/27/07 2010 kcampigottu 024556
05/27/07 2010 kcarnplgotto 024556
06/27/07 2010 kcamplgotto 024556
06/27/07 2010 kcamplgotto Q24556
06/27/07 2010 kcamplgotto Q24556
06/27/07 2010 kcamplgotto 024556
06/2707 2010 kcamplgofto 024556
06/27107 2010 kcamplgotb 024555
06/27/07 2010 kcamplgotto 024556
06/27/07 2010 kcamplgotto 024556
06/27/07 2010 kcamplgotto 024556
06/27/07 2010 kcamplgotto 024556
06/27/07 2010 kcsmplgatto Q24556
06/27/07 2010 kcamplgotto Q24559
06/27/07 2010 kcamplcdto 024556
06/27/07 2010 kcampjgolio 024556
06/27/07 2010 kcemplgouo 024556
06/27/07 2010 kcamplgotlo 024555
06/27/07 2010 kcamplgotto 024556
06/27/07 2010 kcamplgotto 024556
06/27107 2010 kcamplgotto 024556
06/27/01 2010 kcamplgottci 024556
06/27107 2010 kcamplgotto 024556
06/27/07 2010 kcarnplgotto 024556
Page 19 of 35
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrbc Soil COG Group
TIme Collected
Time Submitted
WS-3
185083
G0607589
0612007 1400
06/20/07 1635
Sample Preparation 29.87g mL 355DB 06/23/07 900 dpope P18716
Extractable Petroleum Hydrocarbons by GC.FID
C11-C22 Aromnatlcs 52
C19-C36 Atlphalics
Ce-Cia Aliphatics BRL
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-806/529-5354 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
Phenanthrene
Parameter Result Units Report MDL Dilution Method
Limit Factor
Phenol
Pyrene
BRL
BRL
0.42
mg/kg
mg/kg
mg/kg
0.40
0.40
0.40
0.019
0.043
0.027
Analyst Batch
ID
B270C
8270C
8270C
Analysis
Date/Time
06/27107 2010
06/27/07 2010
06/27/07 2010
kcarnplgotto
kcarnplgotto
kcamplgotto
024556
024556
Q24556
Surrogate Recovery Control Limits
246-Tribromophenol 100 25 123
Temphenyl-d14 118 41 136
Nltrobenzene-d5 77 14-103
2-Fluoroblphenyl 69 21 108
Phenol-d5 88 13-95
2-fluorophenol 78 14-89
mg/kg
11 mg/kg
mg/kg
12
12
12
6.3 MADEP EPH
1.8 MADEPEPH
3.7 MADEPEPH
Analysis Note for Cl1-C22 Aromatics Adjusted value
Surrogate recovery was outside of the control limits Matrix interference is suspected
05127/07 1510 etappacclolt
06/27/07 1510 giappaccloll
06/27/07 1510 giuppaccloll
024555
024555
024555
P18724SamplePreparation
Metals by ICP
ChromIum
Lead
10.2 mL EP1-I 06/2507 1200 dpape
Surrogate Recovery Control Limits
1-Chtoro-octadecane 151 40.140
2-Bmmonephthalene 132 40-140
2-Fluombiphenyl 135 40-140
o-Terphenyt 113 40-140
29 mg/kg
7.5 mg/kg
0.27 0.010 601GB
1.1 0.023 601DB
06/25/07 2120 mcampbell
06/25/07 2120 mcampbeil
024537
024537
Page 20 of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water CerL No 37735
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Daternme ID
Sample Preparation 2.22 50 mL 30506 06/25/07 915 Jhoppel P18720
Volatile Petroleum Hydrocarbons by GC-PIDFID
C5-C8 Aliphatics BRL mg/kg 6.0 1.1 MADEP VPH 06/28/07 107 hwagner 024604
C9-C10 Aromatics BRL mg/kg 6.0 0.036 MADEP VPH 06/28/07 107 hwagner 024604
C9-C12 Aliphatics BRL mg/kg 6.0 1.8 MADEP VPH 06/28107 107 hwagner 024604
Analysis Note for C5-C8 Aliphatics Adjusted value
Analysis Note for C9-C.2 Aliphatics Adjusted value
Surrogate Recovery Control Limits
25-Dlbmmotoiuene-FID 112 70-130
2.5-Dlbromotoluerie-PID 79 70-130
Sample WeIght Determination
Weight 18.11 MADEP VPH 06125/07 000 Ibrown
WeIght 19.81 MADEP VPH 06/25/07 000 lbrown
Sample Comments
BRL Below Reporting Limit
Estimated value between She Reporting Limit and the MDL
The results hi this report relate only to the samples submitted for analysis and meet state certifIcation requirements other thanNEL4CcertificationexceptforthoseInstances Indicated In the case narrative andlor test comments
Al/results are reported on dry-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/528-6354 Fae 7041525-0409
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-3
185083
G0607589
06/20/07 1400
06/20/07 1635
Page 21 of 35
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sompla Matrix Soil COC Group
Time Collected
Time Submitted
WS-4
185084
G0607589
06/20107 1415
06120107 1635
Percent Solids Determination
Percent Solids
Sample Weight Determination
Weight Blsulfate
Weight Risulfata
Weight Methanol
NC CertificatIon No.402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
85.7 SM2540 06125107 1745 Lthao
5.44
5.08
4.18
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
Volatile Organic Compounds by GC/MS
1.1-Trichloroethane
.12.2Tetrachloroethane
12-Trichioroethane
1Dlchloroethane
1-Dichloroethene
11-Dichioropropene
23-Trichlorobenzone
23-Trlchloropropane
2.4Trictilorobenzene
24-Trimethylbenzene
2-Dibrornoethane EDB
2-Dichlorobenzene
.2-Dlchloroethane
2-Dichloropropane
35-Trimethylbenzene
3-Dichlorobenzene
13-Dichloropropane
4-Dichlorobenzene
22-Dichioropropane
2Chiorotoluene
mg/kg 00054
mg/kg 0.0054
mg/kg 0.0054
mg/kg 0.0054
mg/kg 0.0054
mg/kg 0.0054
mg/kg 0.0054
mg/kg 0.0054
mg/kg 0.0054
mg/kg 0.0054
mg/kg 0.0054
mg/kg 011054
mg/kg 0.0054
mg/kg 0.0054
mg/kg 0.0054
mg/kg 0.0054
mg/kg 0.0054
mg/kg 0.0054
mg/kg 0.0054
mg/kg 0.0054
5035
5035
5035
82608
826DB
826DB
826DB
826DB
52608
826DB
82608
82608
826DB
82606
826DB
82608
826DB
826DB
82608
826DB
82606
826DB
826DB
0.0003
0.00055
0.00033
0.00039
0.00041
0.00047
0.00059
0.00047
0.00051
0.00041
0.000097
0.00029
0.00054
0.0004
0.00045
0.D0046
0.00036
0.00042
0.00027
0.0004
06/27/07 000 lbrowri
06/27/07 000 brown
06127/07 000 brown
06127107 322 erussell 024552
06/27/07 322 erussell Q24552
06/27/07 322 erusseil 024552
06/27/07 322 erusseir 024552
06/27/07 322 erussell 024552
06/27/07 322 eiusseli 024552
06/27/07 322 enisseil 024552
D6/27/07 322 erussefi 024552
06/27/07 322 erusseil Q24552
08/27/07 322 musseli 024552
06127/07 322 erussell 024552
06/27/07 322 erusseli 024552
06/27/07 322 enisselI 024552
05/27/07 322 erussell 024552
06/27/07 322 enisselt 024552
06/27/07 322 erussell 024552
06/27/07 322 enissell Q24552
06/27/07 322 erusseil 024552
05/27/07 322 erusseil 024552
D6/27/07 322 enissell 024552
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax 704I525-04t19 Page 22 of 35
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Prolect ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-4
185084
G0607589
06/20/07 1415
06/20/07 1635
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240643 Charlotte1 NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
NC Certification No.402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Date/Time IDLimit
erussell
Factor
2-F-Iexanone BRL mg/kg 0.054 0.00056 826GB 06/27/07 322 024552
4-Chlorotoluene BRL mg/kg 0.0054 0.00028
82608 08/27/07 322 etussell 024552
4MethyI-2-pentanone MJBK BRL mg/kg 0.054 0.00054
82608 06/27/07 322 eiussett 024552
Acetone 0.063 mg/kg 0.054 0.0021 8260B 06/27/07 322 erussell 024552
Benzene BRL mg/kg 0.0032 0.00043 82508 06/27/07 322 erussell 024552
Bromobeazene BRL mg/kg 0.0054 0.00038
826GB 06/27/07 322 erussell 024552
Bromochiorometharie BRL mg/kg 0.0054 0.00032 82608 06/27/07 322 emceeD 024552
Bromodichioromethane BRL mg/hg 0.0054 0.00047 8260B 06/27/07 322 erussell 024552
Bromotomi BRL mg/kg 0.0054 0.0004
826GB 06/27/07 322 erussell 024552
Bromomethane BRL mg/kg 0.011 0.00062 826GB 06/27/07 322 erussell 024552
Carbon tetrachlorlde BRL mg/kg 0.0054 0.00031 826DB 06/27/07 322 erussel 024552
Chlorobenzene BRL mg/kg 0.0054 0.00041 82608 06/27/07 322 emceeD 024552
Chiorodibromomethane BRL mg/kg 0.0054 0.00036 826DB 06/27/07 322 eruscell 024552
Chioroethano BRL mg/kg 0.011 0.00044 826DB 06/27/07 322 erusselt 024552
Chloroform BRL mg/kg 0.0054 0.0004 826GB 06/27/07 322 erussell 024552
Chloromethane BRL mg/kg 0.0GM 0.00038 82608 06/27/07 322 emssell 024552
dc-I 2-Dlchloroetherie BRL mg/kg 0.0054 0.00024 826DB 06/27/07 322 erussell 024552
dc-I 3-Dlchloropropene BRL mg/kg 0.0054 0.00034 8260B 06/27/07 322 enisse 024552
Dichiorodifluoromethane BRL mg/kg 0.0054 0.0012 826DB 06/27/07 322 erussell 024552
Ethylbenzene BRL mg/kg 0.0054 0.00038 826DB 06/27/07 322 aniseeD 024552
Isopropyl ether IPE BRL mg/kg 0.0054 0.00016 826GB 06/27/07 322 emceeD Q24552
Isopropylbenzene BRL mg/kg 0.0054 0.00043 82608 06/27/07 322 enissell 024552
mp-Xylenes BRI mg/kg 0.011 0.00075 826DB 06/27/07 322 erusseil 024552
Methyl ethyl ketone MEK BRL mg/kg 0.11 0.0015 82608 06127107 322 erussell 024552
Methyl t-butyl ether MTBE BRL mg/kg 0.011 0.00031 826DB 06/27/07 322 erussell 024552
Meihylene chloride BRL mg/kg 0.0054 0.00044 826GB 06127107 322 erussell Q24552
n-Butylbenzerre BRL mg/kg 0.0054 0.00043 826GB 0627/07 322 enissell 024552
Page 23 of 35
Fun SufYlci AiaIyUuI ..iwkunuISó.....nu
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No.402
SC Certification No 99012
NC Drinking Water Cert Mo 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-4
185084
G0607589
06/20107 1415
06/20/07 1635
Laboratory Report
06/29/07
Parameter Result Units Report MDL Dilution Method
Limit
Analyst
0.0054 0.00032
0.011 0.00062
0.0054 0.00032
0.0054 000044
0.0054 0.00035
0.0054 000054
0.0054 0.00033
0.0054 0.00092
0.0054 0.00036
0.0054 0.00041
0.0054 000038
0.0054 0.00032
0.0054 0.00044
0.027 0.0019
0.0054 0.00069
Analysis Batch
Factor Date/Time ID
8260B 0627/07 322
erussI 024552
826DB 06127/07 322 erussell 024552
826DB 06/27/07 322 erusseU 024562
82608 06/27107 322 erussell 024552
826DB 06/27/07 322 erussell 024552
826DB 06/27/07 322 enissell Q24552
82608 06/27/07 322 erussl 024552
826DB 06127/07 322 enissell 024552
826DB 0627/07 322 erussell Q24552
82608 06/27/07 322 erussetl 024552
826DB 06/27/07 322 ensseil 024552
8260B 06127/07 322 erussI 024552
82608 06/27/07 322 eruessll 024552
826DB 06/27/07 322 erussell 024552
826DB 06/27/07 322 erussell 024552
n-Propylbenzene BRL
Naphthaiene BRL
o-Xylene BRL
p-lsopropyltoluene BRL
sec-Butylbenzena BRL
Styrene BRL
tert-Butylbenzene BRL
Tetrachtorciethene BRL
Toluene BRL
trans-I 2-Dichloroethene BRL
trans-i 3-Dichioroproperie BRL
Trichioroethene BRL
Trichlorofluoromethane BRL
Vinyl acetate BRL
Vinyl chloride BRL
Semi.volatile Organic Compounds by GCMS
124-Trtchlorobenzene BRL
2-Dichloroberrzene BRL
3-Dlchlorobenzene BRL
4-Dlchlorcbenzene BRL
2.45-Trlchlorophenol BRL
246-Trichlorophenol BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Surrogate Recovenj Control Limits
Bromofluorobenzene 103 77-128
Dlbromolluoromethane 99 67 143
Toluene.d8 105 81.128
0.39
0.39
0.39
0.30
0.39
0.39
0.039
8.029
0.028
0.035
0.040
0.037
8270C
8270C
82700
62700
827CC
62700
06/27/07 1828 kcamplgotlo
08127/07 1828 kcamplgritlo
06/27/07 1828 kcamptgotto
06/27/07 1828 kcarnplgotlo
06/27/07 1828 kcamptgotb
06/27/07 1828 kcamplgottc
024558
024556
024556
024556
024556
024556
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number t800I529-6364 Fax [phone] Page 24 of 35
EnImnm.._..._..bfl
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
24Dlchlorophenol
24-Dimethylphenol
24-Dinllrephenol
24-Dinitrotoluene
26-Dinitrotoluene
2-Chloronaphthalene
2-Chiorophenol
2-Methylnaphthalerie
2-Methyiphenol
2-Nitrophenol
34-Methylphenol
33-Dlchlorobenzldlne
46-Dinhtro-2-methylphenol
4-Bromophenyiphenylether
4-Chloro-3-melhylphenol
4-Chioroanlilne
4-Chlorophenylphenylether
4-Nitrophenol
Aceriaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzoaanthracene
Benzoapyrerie
Benzobtluoranthene
BenzoghIperylene
Benaokfluoranthene
06/27107 1828 kcamplgotlo 024556
06/27107 1826 kcamplgolto 024556
06/27/07 1828 kcamplgotto 024558
06/27/0 1628 kcamplgotto 024555
06/27/07 1825 koamplgotto 024556
06/27/07 1828 kcamplgotto 024555
06/27/07 1828 kcamplgotto 024556
06/27/07 1828 kcamptgotto 024556
06/27/07 1828 kcamplgotto 024556
06/27/07 1828 kcamplgotto 024556
05/27/07 1828 kcamplgutlo 024556
06/27/07 1828 kcamplgolto 024556
06/27/07 1828 kcamplgotto 024556
06/27/07 1828 kcamplgotto 024556
06/27/07 1828 kamplgotlo Q24556
06/27/07 1826 kcamplgotto 024556
06/27/07 1828 kcamplgotlD 024556
06/27/07 1828 kcamplgotto Q24556
06/27/07 1828 kcamplgotto Q24556
0627/07 1828 kcampigotto 024556
06/27/07 1828 kcamplgollo 024556
06/27/07 1828 kcampigouo 024556
06/27/07 1828 kcamplgoito 024556
06/27/07 1828 kcamplgotto 024556
06/27/07 1828 kcamplgotio 024556
06/27/07 1828 kcarnplgotto 024556
06/27/07 1828 kcamplotto 024556
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No.402
SC Certification No 99012
NC DrinkIng Water Cert No 37735
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID WS-4
Prism Sample ID 185084
Sample Matrix Soil coc Group 60607589
Time Collected 06/20107 1415
Time Submitted 06/20107 1635
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
BRL mg/kg 0.39 0.033 827CC
BRL mg/kg 0.39 0.037 827CC
BRL mg/kg 1.9 0.044 827CC
BRL mg/kg 0.39 0.022 827CC
BRL mg/kg 0.39 0.041 8270C
BRL mg/kg 0.39 0.040 827CC
BRL mg/kg 0.39 0.031 827CC
BRL mg/kg 0.39 0.031 827CC
BRL mg/kg 0.39 0.036 827CC
BRL mg/kg 039 0.047 8270C
BRL mg/kg 0.39 0.040 8270C
BRL mg/kg 0.78 0.024 8270C
BRL mg/kg 1.9 0.024 827CC
BRL mg/kg 0.39 0.037 827CC
BRL mg/kg 0.78 0.029 8270C
BRL mg/kg 0.39 0.050 827CC
BRL mg/kg 0.39 0.024 827CC
BRL mg/kg 1.9 0.026 827CC
BRI mg/kg 0.39 0.038 8270C
BRL mg/kg 0.39 0.039 8270C
BRL mg/kg 0.39 0.029 827CC
BRL mg/kg 1.9 0.036 8270C
BRL mg/kg 0.39 0.054 827CC
BRL mg/kg 0.39 0.045 827CC
BRL mg/kg 0.39 0.017 827CC
BRL mg/kg 0.39 0.019 8270C
BRL mg/kg 0.39 0.032 827CC
Page 25 of 35
NC Certification No 402 Laboratory ReportSCCertificationNo99012
NC Drinking Water CarL No 37735 06/29/07
Project ID Morehead Commons No Client Samplo ID WS-4
Prism Sample ID 185084
Sample Matrix Soil COC Group G0607589
Time Collected 06/20107 1415
Time Submitted 06/20/07 1635
Parameter
Benzoic acid
Benzyl alcohol
BIs2-chloroethoxymethane
BIs2-chloroethylether
BIs2-chlaroisopropylether
Bis2-ethylhexylphthalate
Butylbenzylphthalate
Chysene
Dl-n-butylphthatate
Dl-n-octylphthalate
Dlbenzoaharithracene
Dlbenzofuran
Dlethylphthalate
Dlmethylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
F-lexachlorobutadlene
1-lexachlorocyclopentadlene
Hexachioroethane
Indeno1 23-cdpyrene
Isaphorone
N-Nltrosodl-n-propytamlne
N-Nltrosodiphenylamlne
Naphihalene
Nltrobenzene
Pentachlorophenol
Result Units Report MDL Dilution Method
Limit Factor
BRL mg/kg 1.9 0.17
BRL rTg/kg 0.76 0.041
BRL mg/kg 0.39 0.045
BRL mg/kg 0.39 0.042
BRL mg/kg 0.39 0.033
BRL mg/kg 0.39 0.019
BRL mg/kg 0.39 0.024
BRL mg/kg 0.39 0.065
BRL mg/kg 0.39 0.018
BRL mg/kg 0.39 0.029
BRL mg/kg 0.39 0.039
BRL mg/kg 0.39 0.033
BRL mg/kg 0.39 0.024
BRL mg/kg 0.39 0.027
BRL mg/kg 0.39 0.027
BRL mg/kg 0.39 0.023
BRL mg/kg 0.39 0.020
BRL mg/kg 0.39 0.038
BRL mg/kg 0.39 0.041
BRL mg/kg 0.39 0.040
BRL mg/kg 0.39 0.040
BRL mg/kg 0.39 0.035
BRL mg/kg 0.39 0.044
BRL mg/kg 0.39 0020
BRL mg/kg 0.39 0.042
BRL mg/kg 0.39 0.038
BRL mg/kg 1.9 0.033
Analysis Analyst
Batch
Date/Time ID
06/2707 1828 kcamptgotto 024556
06/27/07 1828 kcamploIto 024556
06/2707 1828 kcamploIto 024556
06/27/07 1828 kcamplgotto 024556
06/27/07 1828 kcamplgolto 024556
06/27/07 1828 kcamplgotto 024556
06/27/07 1828 kcamplgofto 024556
06/27/07 1828 kcamplgotlo Q24555
06/27/07 1828 kcaniplgotto 024556
06/27/07 1828 kcamplgoUo 024556
06/27/07 1828 kcaniplgotto 024556
06/27/07 1828 kcamplgotto 024556
06/27/07 1828 kcampgolto 024556
06/27/07 1828 kcamplgotto 024556
06/21/07 1828 kcamptgotw 024556
06/27/07 1828 kcamplgotto 024555
0627/07 1828 kcamplgotto 024556
06/27/07 1828 kcamplgotto 024556
06/27/01 1828 kcamplgotlo 024556
06/27/07 1828 kcamplgotto 024556
06/27/07 1828 kcamplgotto 024555
06/27/07 128 kcamplgodo 024556
0627/07 1828 kcamplgotto 024556
06/27/07 1828 kcamplgotto 024556
0627/07 1528 kcamplgotto 024556
06/27/07 1828 kcamplgotto 024556
06/27/07 1828 kcamplgotta 024556
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Springbrooiç Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte MC 28241
8270C
827CC
827CC
827CC
827CC
827CC
827CC
827CC
827CC
827CC
827CC
827CC
827CC
827CC
827CC
827CC
827CC
827CC
827CC
827CC
827CC
827CC
827CC
8270C
827CC
827CC
821CC
Page 26 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
PrIsm Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
WS-4
185084
30607589
06/20/07 1415
06120/07 1635
Sample Preparation 2969 mL 35508 06/23/07 900 dpope P18716
Extractable Petroleum Hydrocarbons by GC-FID
C11-C22Aromalics BRL mg/kg
C19-C36 Aliphatics BRL mg/kg
C9-C18 Allphallcs BRL mg/kg
Panalysis Note for Cl1-C22 Aromatics
Sample Preparation
14 mg/kg
8.2 mg/kg
0.28 0.017 60108
1.1 0.023 SO1OB
06/25/07 2127 nicarnpbelt
05125/07 2127 mcarnpbeti
024537
024537
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0643
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/2907
Parameter Result Units Report MDL Dilution Method
Limit Factor
Phenanthrere BRL rnglkg
Phenol BRL mg/kg
Pyrene BRL mg/kg
0.39
0.39
0.39
Analyst
0.019
0.042
0.027
8270C
8270C
8270C
Analysis
Date/Time
06/27/07 1828 kcaxnplgotto
06/27107 1828 kcamplgotto
06/27/07 1828 kcamplgotto
Batch
ID
024556
024556
024556
Surrogate Recovery Control Limits
Terphenyl-c114 102 41 136
246-Tribromophenol 90 25-123
2-Fluorophenol 66 14-59
Phenol-d5 82 13-95
2-Fluoroblphenyl 85 21 -108
Nltrobenzene-d5 64 14 103
12 6.3 MADEP EPH 06/27/07 1654 grappaccloll 024555
12 1.7 MADEP EPH 06/27107 1654 grappaccloli 024555
12 3.7 MADEP EPI-i 06/27/07 1854 grappaccloll 024555
Adjusted value
10.06 mL EPH 06/25/07 1200 dpope P18724
Metals bylCP
Chromium
Lead
Surrogate Recovery Control Limits
2-Bromonaphthalene 103 40-140
o-Terphenyl 91 40-140
1-Chloro-octadecane 103 40-140
2-Fluorcblphenyl 107 40-140
Page 27 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehoad Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil coc Group
Time Collected
Time Submitted
WS..4
185084
G0607589
06/20107 1415
06/20107 1635
Sample Preparation 2.09g 5OmL 3050B 06/25/07 915 jhoppel P18720
Volatile Petroleum Hydrocarbons by GC-PIDIFID
C5-C8 Aliphatics BRI mg/kg 5.8 1.1 MADEP VP-l 06128107 150 hwagner
BRL mg/kg 5.8 0.035
C9-Cl2AIlphatlcs BRL mg/kg 5.8 1.8 MADEP VPH 08/28/07 150 hwagner
Ina1ysis Note for CS-Ca Aliphatics Adjusted value
na1ysis Note for C9-Cl2 Aliphatics Adjusted value
One surrogate recovery
was outside the control limits No target compounds were detected inthissampleNofurtheractionwastaken
Sample Weight Determination
WeIght 23.03
Weight 20.43
Sample Comments
MADEP VPH 06/25/07 000 Ibrown
MADEP VPI-I 05/2507 000 brown
BR Below Reporting Limit
J-Estfrnatd value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis end meet stale certification requirements other thanNELAcertificationexceptforthoseInstances indicated in the case narrative and/or test comments
All results are reported on thy-weight basis
This report should not be reproduced except In its entirety without the written consent at Prism Laboratories inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529.6354 Fax [phone]
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert Mo 37735
Laboratory Report
06/29/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
CO-dO Arornatics MADEP VPH 06/28/07 150 hwagner
024604
024604
024604
Surrogate Recovery Control Limits
25-Dlbromotoluene-PID 118 70 -130
25-Dlbromotoluene-FID 157 70-130
Angela Overcash V.P Laboratory Services
Page 28 of 35
ESP Associates PA
Attn Chris Ward
Box7030
Charlotte MC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
B-I
185085
G0607589
06120107 1430
06/20/07 1635
Percent Solids Determination
Percent Solids
Sample Weight Determination
Weight Bisulfate
Weight Blsulfate
Weight Methanol
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
85.2 SM2540 06/25/07 1745 Lthao
5.34
5.54
5.39
BRL
BRL
BRL
BRI
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Volatile Organic Compounds by CC/MS
1.1 1-Trlchloroethane
11 2.2-Tetrachioroethane
11 2-Trichloroethane
1-Dlchloroethane
11-Dichioroethene
1-Dichloropropene
23-Trichtorobenzene
.23-Trichloropropane
124-Trichlorobenzene
124-Trlmethylbenzene
2-DIbromoethane EDB
2-Diclilorobenzene
12-Dichloroethane
2-Dlchloropropane
35-Trimethyibenzene
13-Dlchlorobenzene
.3-Dichloropropane
t4-Dlchlorobenzene
22-Dichioropropane
2-Chiorololuene
5035
5035
5035
826GB
8260B
826GB
826GB
826GB
826GB
826DB
828DB
826DB
826GB
8260B
826DB
825GB
826DB
826DB
82608
826GB
826GB
8260B
826DB
0.0053 0.0003
0.0053 0.00054
0.0053 0.00033
0.0053 0.00038
0.0053 0.0004
0.0053 0.00047
0.0053 0.00058
0.0053 0.00047
0.0053 0.00051
0.0053 0.0004
0.0053 0.000095
0.0053 0.00029
0.0053 0.00053
0.0053 0.00039
0.0053 0.00044
0.0053 0.00046
0.0053 0.00036
0.0053 0.00041
0.0053 0.00025
06/27/07 000
06/27/07 000
06/27/07 000
06/2707 354
06/27/07 364
08/27/07 354
06/27/07 354
06/27/07 354
05/27/07 354
06/27/07 354
06/27/07 354
06127107 354
05/27/07 354
06/27/07 354
0627/07 354
06/27/07 354
06/27107 354
05/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
brown
brown
ibrown
erussell
emusseli
erusselt
erussell
erusseil
erusseli
erussell
erussell
erusseli
enisseil
erussell
emussell
erusseli
erusseli
erussell
erusseli
erusseli
enisseli
erusseil
erussell
024552
024552
024552
024552
024652
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552BRLmg/kg 0.0053 0.00039
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240643 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 29 of 35
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
B-I
185085
G0607589
06/20107 1430
06/20/07 1635
This report should not be reproduced except In Its entirety without the wiitten consent of Prism Laboratories Inc
449 SprJngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06129107
Parameter Result Units Report MDL Dilution Method Analyst Batch
ID
Analysis
Limit Factor Date/Time
2-Hexanone BRL mg/kg 0.053 0.00055 826GB 06/27/07 354 erusseii 024552
4-Chiorotoluene BRL mg/kg 0.0053 0.00028 8260B 06/27/07 354 enissell 024552
4-Methyi-2-pentanone MIBK BRL mg/kg 0.053 0.00053 826DB 06127/07 354 erusseli 024552
Acetone BRL mg/kg 0.053 0.0021 826DB 08/27/07 354 erusseii 024552
Berizene BRL mg/kg 0.0032 0.00042
826DB 08/27/07 354 ewaseli 024552
Brorncbenzene BRL mg/kg 0.0053 0.00037 826DB 08/27107 354 erusseit 024552
Brornochiororriethane BRL mg/kg 0.0053 0.00032 826DB 06/27/07 354 erussell 024552
Bromodichioromethane BRL mg/kg 0.0053 0.00047 8260B 06/27/07 354 erusseli 024552
Bromolorm BRL mg/kg 0.0053 0.00039 826DB 06/27/07 354 erussetl 024552
Bromomethane BRL mg/kg 0.011 0.00061
826GB 06/27/07 354 enisseil 024552
Carbon tetrachiodde BRL mg/kg 0.0053 0.00031 8260B 06/27/07 354 enmsefl 024552
Chkirobenzene BRL mg/kg 0.0053 0.0004 8260B 06/27/07 354 erusseli Q24552
Chiorodibromomethane BRL mg/kg 0.0053 0.00036 8260B 06/27/07 354 erusseli 024552
Chiorcethane BRL mg/kg 0.011 0.00043 82606 06/27/07 354 erussetl 024552
Chloroform BRL mg/kg 0.0053 0.00039 826DB 06/27/07 354 enissell 024552
Chloromethane BRL mg/kg 0.0053 0.00037 826DB 06/27/07 354 erusseil Q24552
cis-i2-Dlchloroethene BRL mg/kg 0.0053 0.00023 826DB 06/27/07 354 erusseil 024552
cia-i 3-Dichloropropene BRL mg/kg 0.0053 0.00034 82608 06/27/07 354 erusseit 024552
Dichloroditiucromethane BRL mg/kg 0.0053 0.0012 8260B 08/27/07 354 erussell 024552
Ethyibenzene BRL mg/kg 0.0053 0.00037 826GB 08/27/07 354 erusseff 024552
Isopropyi ether IPE BRL mg/kg 0.0053 0.00018 826GB 06/27/07 354 eruseeti 024552
isopropyibenzene BRL mg/kg 0.0053 0.00042 826DB 06/27/07 354 enissetl 024552
mp-XyIenes BRL mg/kg 0.011 0.00074 826DB 06/27/07 354 erussetl Q24552
Methyl ethyl ketone MEi BRL mg/kg 0.11 0.0015 826DB 06/27/07 354 enisseli 024552
Methyl t-butyi ether MTBE BRL mg/kg 0.011 0.00031 826DB 06127/07 354 erusseli 024552
Methylene chloride BRL mg/kg 0.0053 0.00043 826DB 06/27/07 354 enisseli 024552
n-Butytbenzene BRL mg/kg 0.0053 0.00042 826DB 06/27/07 354 erusseli 024552
Page 30 of 35
..UVD Ai1yUT lmnmntfSoutkns
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
B-I
185085
G0607589
06/20/07 1430
06/20/07 1635
Semi-volatile Organic Comuounds by GCMS
24-Trlchlorobenzane BRL
2-Dlthlorobenzene BRL
3-Dlchlorobenzeg BRL
4-Dlchlorobnzene BRL
245-Trioblorophonol BRL
246-Thohlorophenol BRL
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
Parameter Result Units Report MDL Dilution Method Analyst
n-Propylbenzene
Naphthalene
o-Xylene
p-Isopropyltoluene
sec-Butylbenzerte
Styrene
tert-Butylbenzene
Tetrachioroethene
Thluene
trans-I 2-Dichloroelherie
trans-13-Dichloropropene
Thchtoroethene
Trichiorofluorornethane
Vinyl acetate
Vinyl chloride
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
Analysis Batch
Limit Factor Datornme ID
0.0053 0.00032 82609 06/27/07 354 erussell 024552
0.011 0.00061 82609 06/27/07 354 erussell 024552
0.0053 0.00032 826DB 06/27/07 354 erusset 024552
0.0053 0.00043 826DB 06/2707 354 erussell 024552
0.0053 0.00035 826DB 06I27/07 354 erussell 024552
0.0053 0.00053 82609 06/27/07 354 erussell 024552
0.0053 0.00033 826DB 06/27/07 354 eussell 024552
0.0053 0.00091 626DB 06/27/07 354 wussell 024552
0.0053 0.00036 826DB 06/27/07 354 erusseil 024552
0.0053 0.0004 826DB 06/27/07 354 enissell Q24552
0.0053 0.00037 82609 06/27/07 354 erussell 024552
0.0053 0.00032 82609 06127/07 354 erussell 024552
0.0053 0.00043 82609 06/27107 354 erussell 024552
0.026 0.0019 82609 06/27/07 354 erussell 024552
0.0053 0.00068 82609 06/27/07 354 erussell 024552
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Surrogate Recovery Control Limits
Dlbromofluaromethane 98 67-143
Bromofluorobenzane 104 77-128
Toluene-d8 96 81 128
0.39
0.39
0.39
0.39
0.39
0.39
0.039
0.029
0.028
0.035
0.040
0.038
8270C
8270C
8270C
8270C
82700
82700
06/27/07 1919 kcamplgoilo
06/27/07 1919 kcamplgotto
06/27/07 1919 kcamplgotto
08/27/07 1919 kcamplgolla
06/27/07 1919 kcamplgotto
06/27/07 1919 kcampigotto
024556
024556
024556
024556
024556
024556
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 31 of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06129107
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID B-I
PrIsm Sample ID 155085
Sample Matrix Soil COC Group G06075B9
Time Collected 06/20/07 1430
Time Submitted 06/20/07 1635
24-Dichiorophenol
24-Dimethyiphenol
24-Dinltrophenol
24-Dlnltrotoluene
26-Dinitiotoluene
2-Chloronaphthalene
2-Chiorophenol
2-Methyinaphthalene
2-Methyiphenol
2-Nitrophenol
34-Methylphenoi
33-DlchIorobenzldlne
46-Dlnltro-2-methyiphenol
4-Brornophenyiphenylether
4-Chloro-3-methylphenol
4-Chforoanilirie
4-Chiorophenyiphenylether
4-Nitrophenol
Acenaphthene
Acenaphthyiene
Arflhracene
Azoberizene
Benzoaanthracerie
Benzoapyrene
Benzobfluoranthene
Benzoghlperyiene
Denzokfluoranthene
Analysis
Date/Time
06/27/07 1919 kcamplgtto
06/27/07 1919 kcamplgotlo
06/27/07 1919 kcmpIgotto
06/27/07 1919 kcamplgotto
06/27/07 1919 keamplgotlo
06/27/07 1919 kcamplgolto
06/27/07 1919 kcamplgotto
06/27/07 1919 kcamplgotto
06/27/07 1919 kcampFgoilo
06/27/07 1919 kcamplgouo
06/27107 1919 kcamplgouo
06/27/07 1919 kcamplgotto
06/27/07 1919 kcampfgolto
06/27/07 1919 kcamplgotlo
06/27/07 1919 kcampgotto
06/27/07 1919 kcamplgotto
06/27/07 1919 kcamplgotta
06/27/07 1919 kcamplgotto
06/27/07 1919 kcampigolto
06/27/07 1919 kcamptgotto
06/27/07 1919 kcamplgotto
06/27/07 1919 kcamplgotio
06/27/07 1919 kcampigollo
06/27/07 1919 kcamptgolto
06/27/07 1919 kcamptgotto
06/27/07 1919 kcamplgolto
06/27/07 1919 kcampiotto
Analyst Batch
IL
024556
024556
024556
024556
024556
024556
Q24556
024556
Q24556
024556
024556
024556
024556
024556
024556
024556
024555
024556
024556
024556
Q24556
024556
024556
024556
024556
Q24566
024556
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 282240543
Phone [phone] Toll Free Number 1-8001529-8364 Fax [phone]
Parameter Result Units Report MDL Dilution Method
Limit Factor
BRL mg/kg 0.39 0.033 8270C
BRL mg/kg 0.39 0.038 827CC
BRL mg/kg 2.0 0.044 827CC
BRL mg/kg 0.39 0.022 8270C
BRL mg/kg 0.39 0.042 8270C
BRL mg/kg 0.39 0.040 827CC
BRL mg/kg 0.39 0.031 B270C
BRL mg/kg 0.39 0.031 8270C
BRL mg/kg 0.39 0.037 827CC
BRL mglkg 0.39 0.047 827CC
BRL mg/kg 0.39 0.040 827CC
BRL mg/kg 0.78 0.024 8270C
BRL mg/kg 2.0 0.024 827CC
BRL mg/kg 0.39 0.037 8270C
BRL mg/kg 0.78 0.029 827CC
BRL mg/kg 0.39 0.050 8270C
BRL mg/kg 0.39 0.024 827CC
BRL mg/kg 2.0 0.026 8270C
BRL mg/kg 0.39 0.038 8270C
BRL mg/kg 0.39 0.039 827CC
BRL mg/kg 0.39 0.030 827CC
BRL mg/kg 2.0 0.036 827CC
BRL mg/kg 0.39 0.055 8270C
BRL mg/kg 0.39 0.045 827CC
BRL mg/kg 0.39 0.018 827CC
BRL mg/kg 039 0.019 827CC
BRL mg/kg 0.39 0.032 827CC
Page 32 of 35
Laboratory Report
06129107
Project ID Morehead Commons No Client Sample ID B-I
PrIsm Sample ID 185085
Sample Matrix Soil COG Group G0607589
Time Collected 06/20/07 1430
lime Submitted 06/20107 1635
Parameter
Benzolc acid
Benzyl alcohol
BIs2-chioroethaxymethane
BIs2-chloroethylelher
Bls2-chioroisopropylether
Bls2-ethylhexylphthalate
Butylbenzylphthalate
Chrysene
Dl-n-butylphthalate
Di-n-octylphthaiate
Dlbenzoahanthracene
Dlbenzofuran
Dlethyiphthalate
Dlrnethylphthalate
Fiuoranthene
Fluorene
Hexachlorobenzene
1-lexachiorobutadlene
Hexachiorocyclopentadlene
i-iexachloroethane
Indeno123-cdpyrene
lsophorone
N-Nltrosodl-n-propylamlne
N-Nltrosodlphenylamfne
Naphthalene
Nitrobenzene
Pentachiorophenol
Analysis Analyst
Batch
Date/Time ID
08/21/07 1919 kcamplgctto 024558
06127/07 1919 kcamplgotlo 024556
06/27/07 1919 kcamplgott 024556
06/27/07 1919 kcampl9olto 024556
06/27/07 1919 kcamplgotb 024555
06127/07 1919 kcamplgotto 024556
08/27/07 1919 kcsmplgotto 024556
06/27/07 1919 kcsmprgoua Q24555
06/27/07 1919 kcamptgotto 024556
06/27107 1919 kcamptgotto 024556
06/27/07 1919 kcamplgolto 024556
06/27/07 1919 kcamplgDtto 024556
06/27/07 1919 kcmptgoUo 024556
08/27/07 1919 kcamplgotto 024555
06/27/07 1919 kcamploltD 024556
06/27/07 1919 kcamplgotto Q24555
06/27/07 1919 kcampigotto 024556
06/27/07 1919 kcamplgolto 024556
06/27/07 1919 kcampgotto 024555
06127/07 1919 kcamplgotlo 024556
06/27/07 1919 kcamptgclto 024556
06I27/07 1919 kcamplgotto 024556
06/27/07 1919 kcamplgotto 024556
06/27/07 1919 kcampigotto 024556
06/27/07 1919 kcampigotto 024556
06/27/07 1919 kcamplgotto 024556
06/27/07 1919 kcamplgotto 024556
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O flot 240543 Charlotte NC 28224-1543
Phone [phone] Toll Free Number 1-8001529-6364 Fax 704I525-0409
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
Result Units Report MDL Dilution Method
Limit Factor
BRL mg/hg 2.0 0.17 8270C
BRL mg/kg 0.78 0.041 92706
BRL mg/kg 0.39 0.045 62706
BRL mg/kg 0.39 0.042 8270C
SRI mg/kg 0.39 0.033 82706
BRL mg/kg 0.39 0.019 8270C
BRL mg/kg 0.39 0.024 8270C
SRI mg/kg 0.39 0.065 827CC
BRL mg/kg 0.39 0.015 827CC
BRL mg/kg 0.39 0.029 827CC
ORL mg/kg 0.39 0.039 827CC
BRL mg/kg 0.39 0.034 82706
BRL mg/kg 0.39 0.024 8270C
BRL mg/kg 0.39 0.027 8270C
BRL mg/kg 0.39 0.027 8270C
BRL mg/kg 0.39 0.023 82706
BRI mg/kg 0.39 0.020 82706
SRI mg/kg 0.39 0.038 827CC
BRL mg/kg 0.39 0.041 827CC
SRI mg/kg 0.39 0.040 8270C
BRL mg/kg 0.39 0.040 8270C
BRL mg/kg 0.39 0.035 82706
BRL mg/kg 0.39 0.044 82706
SRI mg/kg 0.39 0.020 827CC
BRL mg/kg 0.39 0.043 82706
SRL mg/kg 0.39 0.038 827CC
BRL mg/kg 2.0 0.033 82706
Page 33 of 35
NC Ceftiticatlon No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
-----
ESP Associates PA Project ID
Attn Chris Ward
Box 7030
Charlotte NC 28241
Morehead Commons No Client Sample ID
Prism Sample lD
COC Group
Time Collected
Time Submitted
B-I
185065
G0607589
06/20/07 1430
06/20/07 1635
Sample Preparation 29.61 mL 355DB 06/23/07 900 dpope 18716
Extractable Petroleum Hydrocarbons by C3C-FID
C11-C22 Aromatics BRL mg/kg
Cl 9-C36 Atiphatics BRL mg/kg
C9-C15 Aliphatics BRL mg/kg
Analysis Note for Cll-C22 Aromatica
Sample Preparation
This report thouid not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Laboratory Report
06/29/07
Sample Matrix Soil
Parameter Result Units
Phenanthrene
Phenol
Pyrene
MDL Method
BRL
BRL
BRL
Report
Limit
0.39
0.39
0.39
mg/kg
mg/kg
mg/kg
Dilution
Factor
0.019
0.043
0.027
Analyst Batch
ID
8270C
827CC
827CC
Analysis
Date/lime
08/27/07 1919 kcamplgotto
06/27/07 1919 kcamplgotto
06/27/07 1519 kcamplgotlo
024556
024556
Q24556
Surrogate Recovery Control Limits
2-Fluoroblphenyl 94 21 -108
Nitrobenzene-d5 67 14-103
Terphenyl-d14 107 41 136
246-TrIbromophenol 99 25 123
2-Fluorophenol 80 14-89
Phenol-dS 89 13-95
12 6.5
12 1.8
12 3.9
Adjusted value
9.75g 2mL
MADEP EPH
MADEP EPH
MADEP EPH
06/27/07
06/27/07
06/27/07
1838 gmppacclofl
1838 grappacclo1
1838 grappaccloll
024555
024555
024555
P18724EPH06/25/07 1200 dpope
Metals by ICP
Chromium
Lead
Surrogate Recovery Control Limits
1-Chloro-octadecane 114 40 140
2-Fluoroblphenyl 134 40-140
2-Bromonaphthalene 125 40-140
o-Terphenyl 108 40-140
120 mg/kg
12 mg/kg
0.26 0.018
1.1 0.022
80106
60105
08/25/07 2135 mcampbell
06/25/07 2135 mcampbelI
Q24537
024537
Page 34 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
B-I
185085
G0607589
06/20/07 1430
06/20/07 1635
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor DateTflme ID
Sample PreparatIon 2.22 50 mL 30508 06/25/07 915 jhoppel P18720
Volatile Petroleum Hydrocarbons by GC-PIDFID
CS-Ca Allphatics BRL mglkg 5.9 1.1 MADEP VPH 06128/07 233 hwagner Q24604
C9-C10 Aromatlcs BRL mg/kg 5.9 0.035 MADEP VPH 06/28/07 233 hwagner Q24604
C9-Cl2Allphatlcs BRL mg/kg 6.9 1.8 MADEPVPH 06/28/07 233 hwagner Q24604
nalysis Note for C5-C8 Aliphatics Adjusted value
Analysis Note for C9-C12 Aliphatics Adjusted value
One surrogate recovery
was outside tlie control limits No target compounds were detected in
this sample No further action was taken
Surrogate Recovery Control Limits
25-Dlbromotoluene-FID 135 70-130
25-Dlbromotoluene-PID 95 70-130
SampieWeight Determination
Weight 20.69 MADEP VPII 06/25/07 000 Ibrown
Weight 22.23 MADEP VPH 06/25/07 000 Ibrown
Sample Comments
BR Below Reporting Limit
J-Estimated value between the Reporting Limit and the MDL
The results In this report relate only to the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthose instances indicated in the case narrative and/or test ccmrnents
All results are reported on thy-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 244543 Charlotte NC 28224.0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
MC Drinking Water Cert No 37735
Laboratory Report
06/29/07
Page 35 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
184958 Chromium
Lead
68.1398 24.752
19.4685 24.752
mg/kg 147 75-125
mg/kg 62 1/75-125
0-20 024537
0-20 024537
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 26224-0543
Phone [phone] Toll Free Number 1-80W529-6364 Fax [phone]
NC CorUScation No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Level II QC Report
6/29107
M.J.I.-IS.trn ...$I....I RfltflR
Project ID Morehead Commons No COC Group Numbec 00607589
Date/Time Submitted 6/20107 1635
Ifl.nIo Ijy ....r .cfluu
Method Blank QO Batch
Result RL Conlroi Ugnlt Units ID
ChromIum 0.0461 0.25 0.125 mg/kg 024537
Lead 0.3158 0.25 0.125 mg/kg 024537
Laboratory Control Sample ReCovery Recoveiy
Result Spike Amount Units ID
Chromium 23.9028 25 mg/kg 96 80-120 024537
Lead 24.2285 25 mg/kg 97 80-120 024537
Matrix Spike Recovery Recovery OC Batch
Sample ID Result Spike Amount Units ID
184958 Chromium 67.0763 21.834 mg/kg 162 75-125 024537
Lead 18.1186 21.834 mg/kg 64 75-125 024537
Matrix Spike Duplicate Recovery Roovery RPJ QC Batch
Sample ID Result Spike Amount Units ID
Page lof8
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
VrIHfD flrnriIr fnmnnind liv cJIMS mfhnrf RRflR
Niethod Blank QC BIch
REsult RI Contid LImit Units ID
11.1-Trictiloroethane
1122-Tetrachioruethane
1.1 2-Trichloroethane
11-Dichioroeltiane
11-Dlthloroethene
11-Dlchloropropene
123-Trichlorobenzene
123-Ttichloropropane
124-Trichiomberizene
24-Trlmethyfbenzene
12-Dibromoethane EDB
12-Dlchtorobenzene
12-Dichioroethane
12-Dichioropropane
135-Trimethylbenzene
13-Dlchlorobenzene
13-Dichioropropane
4-Dlchlorobenzene
22-Dichioropropane
2-Chiorotoluene
2-Hexanone
4-Chiorotoluene
4-Methyl-2-pentanone MIBK
Acetone
Benzene
Bromobenzene
Bromochioromethane
Bromodichiorometharte
Bmmofomi
Bromomethane
Carbon tetractiloride
Chlorobenzene
Chlorodlbromomethane
Chioroethane
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.05 0.025
ND 0.005 0.0025
ND 0.05 0.025
ND 0.05 0.025
ND 0.003 0.0015
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.01 0.005
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.01 0.005
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/Kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Q24552
024552
024552
024552
024552
024552
024552
024552
Q24552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Numbem 1.8001529.6364 Fax 704l525.0409
NC CertIfication No.402
SC Certification No 05012
NC Drinking Water Cert No 37735
Level II QC Report
6/29/07
Project ID Morehead Commons No COC Group Numbec G0607589
Date/Time Submitted 6120107 1635
Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Method Blank ac
Result RL Control Umit unIts to
Chloroform ND 0.005 0.0025 mg/kg 024552
Chioromethane ND 0.005 0.0025 mg/kg Q24552
cis-12-Dlchloroethene ND 0.005 0.0025 mgJkg 024552
cts-13-Dlchloropropene ND 0.005 0.0025 mg/kg 024552
Dichiorocllfluoromethane ND 0.005 0.0025 mg/kg 024552
Ethylbenzene ND 0.005 0.0025 mg/kg 024552
Isopropyl ether IPE ND 0.005 0.0025 mg/kg Q24552
Isopropylbenzene ND 0.005 0.0025 mg/kg 024552
mp-Xylenes ND 0.01 0.005 mg/kg 024552
Methyl ethyl ketone MEK ND 0.1 0.05 mg/kg 024552
Methyl t-butyl ether MTBE ND 0.01 0.005 mg/kg 024552
Methylene chloride ND 0.005 0.0025 mg/kg 024552
n-Butylbenzene ND 0.005 0.0025 mg/kg 024552
n-Propylbenzene ND 0.005 0.0025 mg/kg 024552
Naphthalene ND 0.01 0.005 mg/kg 024552
o-Xylene ND 0.005 0.0025 mg/kg 024552
p-lsopropyltoluene Nt 0.005 0.0025 mg/kg 024552
sec-Butylbenzene ND 0.005 0.0025 mg/Kg 024552
Styrerte Nt 0.005 0.0025 mg/kg 024552
tert-Butytbenzene ND 0.005 0.0025 mg/kg 024552
Tetrachioroethene ND 0.005 0.0025 mg/kg 024552
Toluene ND 0.005 0.0025 mg/kg 024552
trans.12-DJthJoroethene NI 0.005 0.0025 mg/kg 024552
trans-I .3-Dichioropropene ND 0.005 0.0025 mg/kg 024552
Trichloroethene ND 0.005 0.0025 mg/kg 024552
Trichiorolluoromethane ND 0.005 0.0025 mg/kg 024552
Vinyl acetate ND 0.025 0.0125 mg/kg 024552
Vinyl chloride ND 0.005 0.0025 mg/kg 024552
Laboratory Control Sample Recovoly
Result Spike Amount Unts ID
11-Dlchioroethene 0.03808 0.05 mg/kg 76 57-122 024552
Benzene 0.04358 0.05 mg/kg 87 62-119 024552
Chlorobenzene 0.04441 0.05 mg/kg 89 61-124 024552
Toluene 0.04544 0.05 mg/kg 91 57-122 024552
Trichloroethene 0.04951 0.05 mg/kg 98 59-129 024552
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phoner 7041529-6384 Toll Free Numbem 1-600/529-6364 Fax [phone]
NC CertificatIon No.402
SC Certification No 99012
NC Drinking Water Cart No 37735
Level QC Report
8129107
Project ID Morehead Commons No COC Group Number G0607589
Date/limo SubmItted 6/20/07 1635
Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadsP.O Box 240543 Charlotte NC 29224.0543Phone[phone]TollFreeNumber1-8001529.0354 Fax [phone]
Piifl 5iceMiytict EnIrtmrIi8gIijt1ani
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
6129107
Project ID Morehead Commons No COG Group Numbec G0607589
Date/TIme Submitted 6/20/07 1635
Matrix Spike Recovery Recoveni
Ranges QCBatth
IDSampleIDResultSpikeAmountUnUs
185081 11-Dichloroethene 0.03118 0.05 mg/kg 62 44-140 024552
Benzene 0.03306 0.05 mg/kg 66 46-136 024552
Chlorobenzene 0.02555 0.05 mg/kg 51 47-135 024552
Toluene 0.0296 0.05 mg/kg 59 47-136 024552
Trichlomethene 0.03367 0.05 mg/kg 67 45-141 024552
Matrix Spike Duplicate Recovery Recovery RPD
BatchRangesRPDRangeS5rnpie1DResultSpkeAntountUnits
185081 11-Dichloroethene 0.03223 0.05 mg/kg 64 44-140 0-23 024552
Benzene 0.03495 0.05 mg/kg 70 46-136 0-22 Q24552
Chiorobenzerie 0.03 0.05 rag/kg 60 47-1 35 16 0-22 024552
Toluene 0.03187 0.05 mg/kg 64 47-1 36 0-22 024552
Trichiorcethene 0.03627 0.05 mg/kg 73 45-1 41 0-23 024552
Extractable Petroleum Hydrocarbons byGC-FlD method MADEP EPH
Method Blank 00 BatchResultRIControlUFTIILUnitsID
C11-C22Aromatlcs ND 10 mg/kg 024555
C19-C36 Aliphatics ND 10 mg/kg 024555
C9-Cl8Allphatics ND 10 mg/kg Q24555
Laboratory Control Sample Recovery Recovery
Ranges DC BatchResultSpikeAmountUnitsID
C11-C22Ammatlcs 159.38 170 mg/kg 94 40-140 024555
C19-C36 Aliphatlcs 70.52 80 mg/kg 88 40-140 024555
C9-C18 AtiphalIcs 44.82 60 mg/kg 75 40-140 024555
Matrix Spike Recovery Recovery
Ranges 00 BatchSample1DResultSpikeAmountunits
185126 C11-C22 Aromatiós 147.84 170 mg/kg 87 40-140 024555
C19-C36 Allphatics 66.68 80 mg/kg 83 40-140 024555
C9-C18 Aliphatics 37.94 60 mg/kg 63 40-140 024555
Recovery
Sample ID Result Spike timunt UnIts Ranges RPD Range DC
185126 Cl 1-C22 Mxnatlcs 145.68 170 mg/kg
C49-C36 Ailphatlcs 70.64 80 mg/kg
C9-C18 Aliphatlcs 44.58 60 mg/kg
86 40-140 0-50 024555
85 40-140 0-50 Q24555
74 40-140 16 0-50 024555
Page of
ESP Associates PA
Atth Chris Ward
Box 7030
Charlotte NC 28241
fl.nI..rn4 I-.IIIR RO1flC
Method Blank
Rssua RL Conirci Limft Units
ID
24-.Trlchiorobenzene
12-DichIorobenzene
13-Dichlcirobenzene
14-DichIcrobenene
245-Trlchlorophenol
24.Trich1orophenoI
24-Dichiorophenci
24-Dirnethyiphenol
24-Dinitrophenol
24-Dinilmtoluene
26-Dlnttrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methyiphenol
2-Mtmphenol
34-Methylphenoi
33-Dlchlorobenzldlne
46-Dlnitro-2-methylphenol
48romophenylphenylether
4-Chloro-3-methylphenol
4-Chioroaniline
4-Chlorophenylphenylether
4-Nltrnphenot
Acenaphthene
Acenaphthyiene
Anthracene
Azobenzene
Beflzoaanthracane
Benzoapyrane
Benzobfluoranthene
Benzoghiperylene
BenzokIluoranthene
Benzolc acid
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 1.65 0.825
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
Nfl 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.66 0.33
NI 1.65 0.825
ND 0.33 0.1 65
ND 0.66 0.33
ND 0.33 0.165
ND 0.33 0.165
ND 1.65 0.825
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 1.65 0.825
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 1.65 0.825
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
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mg/kg
mg/kg
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mg/kg
mg/kg
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mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
024556
024556
024556
024556
024556
024556
024556
024556
024556
024656
024556
024556
024556
024556
024556
024556
024556
024556
024556
024556
024556
024556
024556
024556
024556
024556
024556
024556
024556
024556
024556
024556
024555
024556
----______
FiiU5ertce AiwIyIicI Envkonmsntsi SotuUrnrc
NC Certification No.402
SC Certilicatlon No 99012
NC Drinking Water Cert No 37735
Level II QC Report
6129/07
Project ID Morehead Commons No COG Group Number G0607589
Date/Time Submitted 6/20/07 1635
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc449SprthgbrookRoadP.O Box 240543 Charlotte NC 262240543
Phone [phone] ToO Free Number 1-800529-6364 Fax[phone] Page of
NC Ceitificatlon No 402
SC Certification No 99012
Level QC Report
NC Drinking Water Cert No 37735
24-Trlchlorobenzene
4-Dlchlorobenzene
24-Otnltretoluene
2-Chlorophenol
4-ChIoro-3.mothylphencl
1.46143 1.6697
1.21969 1.6697
1.65308 1.6697
1.23973 1.6697
1.59666 1.6697
mg/kg 88 39-98
mg/kg 73 3795
mg/kg 99 55-128
mg/kg 74 37-98
mg/kg 96 45-111
024556
024556
024556
024556
024556
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
6129107
Project ID Morehead Commons No COG Group Number 00607589
Date/Time Submitted 6120/07 1635
Method Blank oc anicti
Resutt RL Cnntmt Umli Units to
Benzyl alcohol ND 0.66 0.33 mg/kg 024556
Bi2-chtcroethoxymethane ND 0.33 0.165 mg/kg 024556
Bls2-chtoroothylether ND 0.33 0.165 mg/kg 024556
Bls2-chlorolsopropylether ND 0.33 0.165 mg/kg 024556
Bls2-ethylhexylphthaiate ND 0.33 0.165 mg/kg Q24556
Butylbenzylphthalate ND 0.33 0.165 mg/kg 024556
Chrysene ND 0.33 0.165 mg/kg 024556
Dl-n-butylphthalate ND 0.33 0.165 mg/kg 024556
DI-n-octyiphthalate ND 033 0.165 mg/kg 024556
Dlbenzoahanthracene ND 0.33 0.165 mg/kg 024556
Dibenzcfuran ND 0.23 0.165 mg/kg 024556
EIethylphthalate ND 0.33 0.165 mg/kg 024556
Dlmethylphthalate NE 0.33 0.165 mg/kg 024556
Fluoranthene ND 0.33 0.165 mg/kg 024556
Fluorene ND 0.33 0.165 mg/kg 024556
Hexachlorobenzene ND 0.33 0.165 mg/kg 024556
Hexachiorobutadlene ND 0.33 0.165 mg/kg 024556
Hexachlorocyclopentadiene ND 0.33 0.165 mg/kg 024556
Hexachioroethane ND 0.33 0.165 mg/kg 024556
lndeno123-r.dpyrene ND 0.33 0.165 mg/kg 024556
Isophorone ND 0.33 0.165 mg/kg 024556
N-Nltrosodl-n-propyiamfne NI 0.33 0.165 mg/kg 024556
N-Nitmsodlphenylamlrte ND 0.33 0.165 mg/kg 024556
Naphthalene ND 0.33 0.165 mg/kg 024556
Nitrobenzene NI 0.33 0.165 mg/kg 024556
Pentachlorophenol ND 1.65 0.825 mg/kg 024556
Phenanthrene Nt 0.33 0.165 mg/kg 024556
Phenol ND 0.33 0.165 mg/kg 024556
Pyrene ND 0.33 0.185 mg/kg 024556
Laboratory Control Sample
oc BatchResultSpikeAmountUniteID
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toil Free Number 1800/529-5364 Fax [phone] Page of
NC Certification No 402 Level II .QC ReportSCCertificationNo99012
NC Drinking Water Cert No 37735
185039 1.24-Trichlorobenzene
4-Dichlorobenzene
2DlnlVbtoluene
2-Chiorophenol
4-Chlom-3-methylphenol
4-Nitrophenol
Acenaphthene
N-Nltrosodl-n-propyiamjne
Penlathlorophenol
Phenol
Pyrene
1.24221 1.6570
124817 1.6570
1.85005 1.6570
1.21172 1.6570
1.38933 1.6570
1.72001 1.6570
1.61729 1.6570
1.36315 1.6570
1.80351 1.6570
1.27269 1.6570
1.60371 1.6570
mg/kg 75 26-97
mg/kg 75 23-92
mg/kg 113 45-127
mg/kg 73 25-94
mg/kg 84 31-113
mg/kg 104 17-150 10
mg/kg 98 36-107
mg/kg 82 22-105
mg/kg 109 39-137
mg/kg 77 23-97
mg/kg 97 45-133
0-37 024556
0-38 024556
0-29 024556
0-37 024556
0-32 024556
0-32 024556
0-32 024556
0-37 024556
0-27 024556
0-42 024556
0-27 024556
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529.8354 Fax [phone]
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
6/29/07
Project ID Morehead Commons No COG Group Number G0607589
Dote/Time Submitted 6/20/07 1635
Laboratory Control Sample Recoveri
Ranges DC Batch
IDReaL/I Spike Amount tints
4-Nitrophenol 1.60500 1.6697 mg/kg 96 20-157 024556
Acenaphthene 1.53355 1.6697 mg/kg 92 44-110 024556
N-Nltrosodi-n-propyiamlne 1.48113 1.6697 mg/kg 89 38-101 024556
Pentachloraphenol 1.64674 1.6697 mg/kg 99 53-127 024556
Phenol 1.32821 1.6697 mg/kg 80 34-102 024558
Pyrene 1.67278 1.6697 mg/kg 100 54-131 024556
Matrix Spike Rv RCOVesy
Sample io Result Spike Amount Units
Ranges DC Batch
ii
185039 1.24-Trtchlorobenzene 1.34494 1.6587 mg/kg 51 26-97 024556
14-D1chIorthenene 1.24245 1.6587 mg/kg 75 23-92 024556
2.4-Dinitmioluerte 1.90679 1.6587 mg/kg 115 45-127 024556
2-Chlorophenol 1.23150 1.6587 mg/kg 74 25-94 024556
4-Chloro-3-methylphenol 1.32338 1.6587 mg/kg 80 31-113 024555
4-Nltrophenoi 1.55251 1.6587 mg/kg 94 17-150 024556
Acenaphthene 1.60398 1.6587 mg/kg 97 36-107 024556
N-Nltrosodl-n-propylarnine 1.45140 1.6587 mg/kg 88 22-105 024556
Pentachlorophenol 1.64046 1.6587 mg/kg 99 39-137 024556
Phenol 1.31840 1.6587 mg/kg 79 23-97 024556
Pyreno 1.53698 1.6587 mg/kg 93 45-133 024566
Matrix Spike Duplicate Recoveiy Resoveay RFD
Sample ID Result Spike Amount Units
Ranges Range DC BatCh
ID
Page of
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
nhHIe Pe5rnlm I1udrnrhnnQ hu tPlfllFIfl mothnd MAflFP VPIl
184956 CS-CS Aliphatics
C9-Cl0 Aromatics
C9-C12 Aiiphatics
-See Case Narrative
This report should not be repreduced except In Its entirety without the Written consent of Prism Laboratories Inc449SprlngbrookRoadP.O Box 240543 Charlotte NC 28224-9543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water CerL No 37735
Level II QC Report
6/29/07
Project ID Morehead Commons No COG Group Number G0607589
Date/TIme Submitted 6120107 1635
Method Blank tl Batch
Result RI Control UrnS UnSa
ID
CS-CS Aliphatics ND 2.5 mg/kg 024604
CO-dO Aromatics ND 2.5 mg/kg 024604
C9-C12 Aliphatics ND 2.5 mg/kg 024604
Laboratory Control Sample Recovery P.engea OG Batch
ResuR Spike Amount Units ID
C5-C8 AlIphalics 16.779 15 mg/kg 112 70-130 024604
CO-Cia Arcmatlcs 4.305 mg/kg 36 70430 024604
C9-C12 Allphatics 10.922 10 mg/kg 109 70-130 024604
Matrix Spike Recovery Recovery
P.arrges OCBatch
Sample 10 Result Spike Amount Units ID
184956 CS-Ca Allphatics 16.625 15 mg/kg 111 70-130 024604
C9-C10 Aromatics 4.148 mg/kg 83 70-130 024604
C9-Cl2AHphatics 12.627 10 mg/kg 126 70-130 024604
Matrix Spike Duplicate Recovery RPD
Ranges RPD Range OCflOtdv
Sample ID Result Spike Mrnunt Units ID
17.936 15 mg/kg 120 70-130 0-25 024604
4.279 mg/kg 86 70-1 30 0-25 024604
13.613 10 mg/kg 136 70-130 25 024604
Page of
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Short Hold Analysis Yes No UST Projeob No
Piease ATTACH any project specific reporting QC LEVEL 111111 IV
provisions and/or 00 ReqIjrIpent
Invoice To
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Requested Due Dale 01 Day 02 Days 03 Days 04 Days Days
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Samples received after 1500 wIll be processed next business day
Turnaround time Is based art busIness days excluding weekends and holidaysSEEREVERSE FOR TERMS CONDITIONS REGARDiNG SERtCES
RENDERED BY PRISM LABORATORIES INC TO cLIENT
Upon relinquishing this chaIn of Custy is your authorization for Prism to proceed with the anaIys as requested above Any changes must besubmittedInwritingtothe Prism Project Manager There will be charges for any changes after analyses have been initialized
rioiinquusne oy gnaturs ............MIIITary-Iours
Ralirtqutehed By Signature Racaived By Signaiure Dais
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Client Company Name _______________________
Report To/Contact Name ________________________
Reporting Address
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Email Yes No Email Address_____
EDt Type PIDF_ExceL.9thr
Site Location Name ________
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v2/i
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TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC_USACE_FL NC.J..
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Water Chlorinated YES_NO...
Sample Iced Upon Collection YES jNO
TIME MATRIX SAMPLE CONTAINER
ANALY SOUESTED PRiSMCUENTDATECOLLECTEDSOILPRESERVALABy/REMARKS ID NOSAMPLEDESCRiPTIONCOLLECTEDMILITARYWATERORTYPETIVESHOURSSLUDGESEEBELOWNOSIZE
Vie t5oSt
Jo
/D 5J
14ao iiJ-y _______________________IS58M
L5o
Samplers Snaiure Sampled By Print Name Affiliation
Additional Comments
-NPDES GROUNDWATER DRINKING WATER SOLID WASTE RCRA CERCLA LANDFILL OTHER0NCUSCINCUSCONC USC ONC USC ONC USC UNC USC UNC USC ONC USC ONIC USC____ ____
10 _______Io ________to ______to ____1U ________ ____-..-.-..--.-nr ._.i..r.i...ri...ci cii.-..t..rnnr.r.j nd r.-\trta /...t.II r.t.AI..7..I-J.....1
SEE REVERSE FORTERMSCONDITiONS
ORiGiNAL
Full Servtco AnL$Ecal Erwlmnmenthl oIulloiis
CLIENT SP 4ôks
A1TN Ctir k-c/
PRISM COC GROUP
6O1O-9
Please fill in the Site Location information on the attached VPH and/or EPH Forms
\NaSOflFOLD\COMMON\FORMSWH PH Site Location br Ciient.duc
VPH AliphaticslAromatics Laboratory Reporting Form
Client Name ESP Associates PA Laboratory Name Prism Laboratories Inc
Project Name Morehead Commons No NC Certification Lab 402
Site Location ________________________________Sample Matrix Soil
Sample Information and Analytical Results
Method for Ranges MADEP VPH
VPH Surrogate Standards Aliphatic 25-Dibromotoluene Aromatic 25-DibromotoluerieFJJrL
Sample Identification 185081 185082 185083 185084 185085
Coilectton Option for soll
f4t _________ _____________________________Date Collected _______Date Received 1cjlIjt ______________________________________Date Extracted _________ ________ ________Date Analyzed JPPI 411jII 6/27/2007 _________ ___________________ __________
Dry Solids jtfr/fir _____________________ _______Dilution Factor _________
Hydrocarbon Ranges in mg/kg ij Sample Results __________________ __________C5-C8 Aliphaticstm _________ ________ __________________C9-G12 Aliphatics9 ___________________ __________ __________C9 Cl Aromatlcs4.4
fiji it
LW
_________________________________________________________________________________________________________________
________________________________ _______________ ________________
______C9-C10 Aromatics P8II1 _______ _______ ______________ilEi4l
__________________________________________________________
111i1li ______________________ ______________________Surrogate Acceptance Range Blank 70-130 _________ ___________________AliphaticSurrogate%Rec-FID 130 111 119 112 157 135ff
Aromatic Surrogate Rec PID 97 79 84 79 118 96
Blank
RL
C5-C8 Allphatlcs
C9-C12 Allohatics
C9-C10 Arornatlcs
C5-C8 Aliphatics
C9-C12 Allphatics
C5-C8 Aliohatics
C9-C12 Aliphatics
C9-C10 Aromatics
6/20/2007
6/20/2007
6/28/2007
6/2812007
80.1
Sample Results
6.2
6.2
6.2
5.0
5.0
5.0
6.2
6.2
6.2
1.2
1.9
0.037
70-1 30
Option Established liii line on vial
Option Sampling
device indicate brand e.g EnCore TM
Option Field weight of soil
Unadjusted value should exclude the concentration of any surrogates Internal standards and/or
concentrations of other ranges that elute within the specified range
Adjusted value
MDL Method Detection Limit RL Reporting Limit Blank Laboratory Method Blank or Trip Blank
whichever Is higher indicate typeWereallperformance/acceptance standards for required ONCIC
procedures achieved YES No Details AttachedWereanysignificantmodificationstotheVPHmethodmadeNOYesDetailsAttachedCommentsVPHtripblankwasnotsubmittedtothelaboratory
Result outside of the CIC limits
MDL
6/20/2007
6/20/2007
6/27/2007
81.9
6.
5.0
5.0
5.0
6.1
6.1
6.1
1.2
1.9
0.037
6/20/2007
6/20/2007
6/28/2007
6/28/2007
83.9
Sample Results
6.0
6.0
6.0
5.0
5.0
5.0
6.0
6.0
6.0
1.1
1.8
0.036
70-1 30
6/20/2007
6/20/2007
6/28/2007
6/28/2007
85.7
Sample Results
5.8
5.8
5.8
5.0
5.0
5.0
5.8
5.8
5.8
1.1
1.8
0.035
70-130
6/20/2007
6/20/2007
6/28/2007
6/28/2007
85.2
Sample Results
5.9
5.9
5.9
5.0
5.0
5.0
5.9
5.9
5.9
1.1
1.8
0.035
70-1 30
Pageloll VPH Soil
EPH AHPhaflcslomjc5 Laborato Repo1ng Fon
Client Name ESPASSOCI2tPA Laboto Name Pdsm Laboratoes
Project Name Morehead Commons No NC Certification Lab 402
Site Location
Sample Max So
Sample Information and Analytical ResultsMethodforRangesMADEPEPHEPHSurro ate Standards All hatic lChlorooctadecane Aromatic o.TerphenEPHFractionationSUffOates2-Bromonaphthalene 2-Fluorobi henylSamIaIdentification
____185081 185082 185083 185084 185055
Date Collected
_______6/2Q/jo 6/20/2007 6/20/2007 fi/20/2cJ07 6/2012011
Date Received
_______6/20/2007 6/20/2007 6/20/2007 6/20/2007 6/20/2007
Date Extracted
____625/2007 6/25/2007 6/25/2007 6/25/2007 6/25/2037
Dale Anal zed
_____6/27/2007 6/27/2007 6/27/2007 6/27/2007 6/27/2007
Solids
81.9 80.1 83.9 85.7 85.2
Dlltj Factor
drocarbon Ran es in
SmpIe ResuJt Sampte Resuft Sampe Resul Sarnpre ReuI SampJ ResuI
C9-C18 All llatics 12 13 12 12 12CI9C36Aliphatics
_____12 13 ii 12 12C11-C22 Aromatics
________12 20 52 12 12C9-C1 All hatica
_____10 10 10 10 10C19C36Alhatics1010101010Cl1-C22 Aromatics 10 10 10 10
RL C9-Ci8AIiphatics -s-12 13 12 12 12Cl9C3GAiipilatics
_______12 13 12 12 12
Cl 1-C22 Arornatics
__________12 13 12 12 12
I.4DL C9-C18 All hatcs 3.8 4.1
3.7 3.9
Clg-C36 All hatics 1.8 1.9 1.8 1.7___Cl1_C22Aromafl
6.4 6.9 6.3 6.3 6.5
urro ate Acceptance Ran Blank 40-140 40-140 40-140 40-140 40-140
All heticSuo ate%Rec 104 107 106 151 103 114
Aromatic Surro ate Rec 87 93 88 113 91 108
fctiOflajon Surraqo Accep Range Blank 40-140 40-140 40-140 40-140 40-140
Frac.S0 ate1%Rec 128 91 132 103 125
Frac Surrogate Rec
134 92 135 107 134_1 nadjusted value should exclude the c000enh-allon of any surrogates internal standards and/oroncefltjoofotherrangesthatelutewithinthespecifiedrange/h.JUS value
Method Detection Limit RL Reporting Limit Blank Laboratory Method Blank
prccedures achieved
Details Attached
Was lank correction applied as slgflffI modification of the method Yes NOwsrnystgnificmocjffcaff35totheEPHmethodmadeNOYesDetails Attached
ents The analyte was Positively Identified but the value is estimatedbelowthereportinglimit
Result outskje of the QC Ilmita
Page of EPH Soil
EcO JUL27 2007
Case Narrative RevisedPRISM
L3ORATOR1E INC
Date 07/23107 Client Project ID Morehead Commons No
Company ESP Associates PA Prism COC Group No G0607587
Contact Chris Ward Collection Dates 06/20/07
Address Box7030 Lab Submittal Dates 06/20/07
Charlotte NC 28241
This Is revised report and supersedes our original laboratory report dated 0629J07 Lead was added to all samples
This data package contains the analytical results for the project identified above and includes Case Narrative Laboratory Report and Quality
Control Data totaling pages chain-of-custody is also attached for the samples submitted to Prism for this project
Data qualifiers are flagged individually on each sample key refrence for the data qualifiers appears at the end of this case narrative Quality
control statements and/or sample specific remarks are included in the sample comments section of the laboratory report for each sample
affected
Semi Volatile Analysis
No Anomalies Reported
Volatile Analysis
No Anomalies Reported
Metals Analysis
Analysis Note for Q251 61 MS Lead Matrix interference is suspected Post-digestion spike recovery 70%Is outsIde the
acceptance limits 75-125%
Analysis Note for 025161 MSD Lead RPD value outside the control limits Digestion was repeated with similar results
Wet Lab and Micro Analysis
N/A
Please call if you have any questions relating to this analytical report
Date Reviewed by Paula Gilleland Project Managec Angela D.ash
Signature KioL Signature __________________________
Review Date 07/23/07 Approval Date 07/23/07
Data Qualifiers Key Reference
Compound also detected In the method blank
Result outekie ol the QC limits
DO Compound dIluted out
Estimated concentration caflbrafion range exceeded
The analyte was positively Identified but the value is estimated below the reporting limit
Estimated concentration with high bias
Estimated concentration with low bias
matrix effect Is present
Notes This report should not be reproduced except in its entirety without the writtten consent of Prism Laboratories1 Inc The results in this
report relate only to the samples submitted for analysis
449 Springbmok Road P.O Box 240543 Charlotte NC 28224-0403
PhOne [phone] Tot Fine 80V529-8354 Fec 704/525-0409
SCCertilicationNo.99012 Laboratory Report
NC Drinking Water Cert No 37735 07/23/07
ESP Associates PA Project ID Morehead Commons No Client Sample ID IA-123 COMP
Attn Chris Warti Prism Sample ID 185077
Box 7030 Sample Matrix Soil COC Group G0607587
Charlotte NC 28241 Time Collected 06/20/07 1040
Time Submitted 08/20/07 1635
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Percent Solids Determination
Percent Solids 87.4 SM2540 06/27/07 1800 Lthao
Volatile Organic Comeounde by CC/MS
Benzene BRL pg/kg 3.4 0.51 826DB 06/27/07 806 erussell 024552
Ethyibenzene BRL pg/kg 5.7 0.44 8260B 0627/07 806 anissell 024552
m.p-Xylenes BRL pg/kg 11 0.88 82608 06/27/07 806 erusseli 024552
o-Xyiene BRL pg/kg 5.7 0.38 826DB 0627/07 806
erussell 024552
Toluene BRL pg/kg 5.7 0.43 826DB 06127/07 806 erussell Q24552
Surrogate Recovery Control Limits
Toluened8 93 81-128
DlbromolIuoromethane 93 67-143
Bromotluorobenzene 107 77-128
Diesel Ranae Organics DRO by GC-FID
Diesel Range Organics DRO 370 mg/kg 40 5.0 8015B 06127/07 1428 Jvogei 024575
Sample PreparatIon 25.36 mL 3545 06/25107 1515 wconder P18738
Surrogate Recovery Control Limits
o-Terphenyl 49-124
Gasoline Range Organics IGRO1 by GC-FID
Gasoline Range Organics CR0 BRL mg/kg 1.1 0.073 80158 06/27/07 441 hwagner 024580
Surrogate Recovery Control lJmits
aaa-TFT 85 55-129
Metals by ICP
Lead 15 mg/kg 0.28 0.018 601DB 07/19/07 2235 mcampbell 025151
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toil Free Number 1-8061529-6364 Fax [phone] Page of
ESP Associates PA
ALtn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
IA-123 COMP
185077
G0607587
06/20/07 1040
06/20/07 1635
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Sample Preparation 2.01 50 mL 305DB 07/19/07 715 Jhoppel P18933
Sample Comments
BRL Below Reporting Limit
f-Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted foranalysis and meet stale certification requirements other thanNEL4Ccertificationexceptforthose instances Indicated in the case narrative and/or test comments
All results are reported on dry-weight basis
Angela Overcash V.P Laboratory Services
This report shouki not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Spnngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6354 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
07/23/07
Page of
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil coc Group
Time Collected
Time Submitted
B-234 COMP
185078
00607587
06/20/07 1055
06/20/07 1635
Percent Solids Determination
Percent Solids
Diesel Range Organics DRO by GC-FID
Diesel Range Organics DRO
Surrogate Recovery Control Limits
Toluene-dB 94 81 128
Dibrornofluorornethane 92 67-143
Bromofiuorobenzene 104 77-128
140 mg/kg 7.9 0.99 8015B 06121/07 330 JvaaeI 024575
Sample Preparation 25.12g lmL 3545 06/25/07 1515 wconder P18738
Gasoline Range Oreanics 1GRO by GC-FID
Gasoline Range Organics GRO BRL
Metals by ICP
Lead
mg/kg 1.1 0.072
13 mg/kg 0.28 0.018
Surrogate Recovery Control Limits
o-Terphen1 77 49-124
8015B 06/27/07 512 hwaner Q24580
Surrogate Recovery Control Ltmits
aaa-TFT 89 55-129
601GB 07/19/07 2302 mcampbell Q25191
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-300/529-6354 Fax [phone]
Laboratory Report
07/23/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
88.1 SM2540 06127/07 1800 Lthao
Volatile Organic Comnounds by GCIMS
Benzene BRL pg/kg 3.4 0.50 82608 06127/07 837 erusadi Q24552
Ethylbenzene BRL pg/kg 5.7 0.44 82608 06/27/07 837 oruasall 024552
rnp-Xylenes BRL pg/kg 11 0.88 82608 06/21/07 837 erussell 024552
o-Xylene BRL pg/kg 5.7 0.38 8260B 06/27/07 837 erussell 024552
Toluene BRL pg/kg 5.7 0.43 8260B 06/27/07 837 erussell 024552
Page of
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
PrIsm Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
B-2314 COMP
185078
G0607587
08120107 1055
06120/07 1635
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Sample Preparation 2.02 50 mL 305DB 07119107 715 Jhopp P18933
Sample Comments
BRL Below Reporting Limit
.1-EstImated value between the Reporting Limit and the MOL
The results in this report relate only to the samples submitted for analysis and meet slate certification requirements other thanNELACcertificatIonexceptforthoseinstances indicated In the case narrative and/or test comments
Al results are reported on dry-weight basis
This report should not be reproduced except in Its entirety without the written consent of Prism thboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
______
rtaI Sv1 AnIylIcaI EnirnmtithISduU
NC Cerliflcatlon No 402
SC Certification No 99012
NC Drinking Water CerL No 37735
Laboratory Report
07/23/07
Angela Overcash V.P Laboratory Services
Phone [phone] Toll Free Number 1-801U529-6364 Fax [phone]a Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
This report should not be reproduced exceptin its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toil Free Number 1-8001529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level It QC Report
7123107
Project ID Morehead Commons No COC Group Number G0607587
Date/Time Submitted 6/20/07 1635
Volatile ---GCIMS mthnr4 RRflR....s.fl.s1ltlo ISV .-__.
Method Blank 06 Batch
Result RL Control UrnS Unite ID
Benzene ND 0.003 0.0015 mg/kg Q24552
Ethylbenzene ND 0.005 0.0025 mg/kg 024552
mp-Xylenes ND 0.01 0.005 mg/kg 024552
o-Xytene ND 0.005 0.0025 mg/kg 024552
Toluene ND 0.005 0.0025 mg/kg 024552
Laboratory Control Sample Recovery
Result Spike Amount Units
Jflg5 OC Bald
ID
Benzerte 0.04358 0.05 mg/kg 87 62-1 19 024552
Ethyibeniene 0.04417 0.05 mg/kg 88 57-128 024552
nip-Xylenes 0.09048 0.1 mg/kg 90 54-132 024552
o-Xylerie 0.04725 0.05 mg/kg 95 57-131 024552
Tuluene 0.04544 0.05 mg/kg 91 57-122 024552
Matrix Spike Recovery Recovery
Ssmple to Result Spike Amount Units itanites OC Batch
ID
185081 Benzene 0.03306 0.05 mg/kg 66 46-136 024552
Ethylbeazene 0.02888 0.05 mg/kg 58 51 -1 35 024552
mp-Xyienes 0.05588 0.1 Rig/kg 56 51-136 024552
o-Xyiene 0.02855 0.05 mg/kg 57 49-137 024552
Toluene 0.0296 0.05 mg/kg 59 47-1 36 024552
Matrix Spike Duplicate Recov Recovery RPD
Sample ID Result Spike Amount Units
Ranges RPD Range CC Batch
ID
185081 Benzene 0.03495 0.05 mg/kg 70 45-1 36 -22 024552
Ethylbenzene 0.03244 0.05 mg/kg 65 51-1 35 12 0-23 024552
mp-Xylenes 0.06374 0.1 mg/kg 64 51-1 36 13 -20 024552
o-Xylene 0.03337 0.05 mg/kg 67 49-137 16 0-22 024552
Toluene 0.031 87 0.05 mg/kg 64 47-136 0-22 024552
Pagel of3
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Gasoline Range Organics
_____CR0
Matrix Spike
Sample ID
185077 Gasoline Range Organics
_____CR0
Matrix Spike Duplicate
Sample ID
185077 Gasoline Range OrganicsCR0
This report should not be reproduced except In its entirety without the written consent ol Prism Laboratories Inc449SpnngbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Nwnber 1-8001529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No.37735
Level 11 QC Report
7/23/07
Project ID Morehead Commons No COG Group Number G0607587
Date/Time Submitted 6/20/07 1635
Diesel Range Organics DRO bjr_GC-FID method 8015B
Method Blank QC BSICh
Result RI Cantml LImit Units ID
Diesel Range Organics DRO ND 35 mg/kg 024575
Laboratory Control Sample RCVE RQcOVWY OC BatchRangesResultSplkeAmountUnitsID
Diesel Range Organics DRO 49.0 80 mg/kg 61 55-109 024575
Matrix Spike Recoveiy Ranges QCBalch
Sample ID Restjii SpHw MiOunI Units ID
184791 Diesel Range Organlcs DRO 45.8 80 mg/kg 57 50-117 024575
Matrix Spike Duplicate Recovery R1 OCBaichRangesRPDRange
Sample ID Result Spike Amount Units
184791 Diesel Range Organics DRO 51.9 80 mg/hg 65 50-117 12 0-24 024575
Gasoline Range Organics GRO byGC-FID method 8015B
Method Blank DC Belch
Result RI Control Umit Units ID
Gasoline Range Organics ND 0.5 mg/kg 024580CR0
Laboratory Control Sample Rv Ranges CC B8ICh
IDResultSpikeAmountUnits
1.956 mg/kg 98 64-124 024580
Recovery oc Batch
Result Spike Amount UnIts ID
2.016 mg/kg 101 37-126 024580
Result
1.968
Recovery Recovery RPD
Ranges RPO Range CC Batch
Spike Amount Units to
mg/kg 98 37-126 0-34 024580
Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Metals by ICP
method 6010B
Method Blank QC Batch
Result RI-Control Limit Units ID
Lead 0.0483 0.25 0.125 mglkg 025161
Laboratory Control Sample Recovey Ranges DC Batch
Result Spike Amount UnIts ID
Lead 23.4916 25 mglkg 94 80-120 025161
Matrix Spike Recovery Ranges OC Batch
Sample ID Result Spike Amount Units ID
185077 Lead 29.2856 24.630 mglkg 65 75-125 025161
Matrix Spike Duplicate Recovery Recavejy RPD
Ranges RPD Range OC Batch
Sample ID Result Spike Amount Units ED
185077 Lead 40.0598 24.630 mg/kg 108 75-125 31 0-20 Q25161
-See Case Narrative
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number 1-8001529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
7/23/07
Project ID Morehead Commons No COC Group Number G0607587
Date/Time Submitted 6/20/07 1635
PageS of
A$0RATOCIEe INC
Fufi Sen4ee Analytical Envlmnmentai 5otutlon
449 Springbrock Road P.O Box 240543 Charlotte NC 28224-0543Phone[phone] Fax [phone]y.CUen Company Name /-1i41t-
Report To/Contact Name tts
Reporting Address _____________________________
Phone ________________Fax Yes No
Email Yes No Email Address______________________EDDTyPe /7
Site Location Name _____________________________
Site Location Physical Address LL
Samplers Signature Sampled By Print Name Affiliation
Upon relinquishing this CH1 of custaçis your authorization for Prism to proceed with the analyses as requested above Any changes must besubmittedinwritingtothe Prism Project Manager There will be charges for any changes after analyses have been initialized
PetIflOuishid lSlnnntir.i MIIir/i1FtacetvetIBySIgnature
ReHnqushed Dy SIgnature Recalvad By SIgnature Date
SAMPI.eS ARE NO
CIFCdEX CIUPS afld-daHvarad
SHU BE
ACCEPTED AND VERIFI
QP4smFieId5eryg
sR ThE SOToRYED AGAIN 00 NiL RECEIVED AT THE L.AEORATORY
CIOther
ddpNo
NPDES US GROUNDWAR DRINKING WATER SOLID WASTE RCRA CERCLA LANDFILL OTHERONCCISCtCCISCONCCISCONCCISCONCCISCONCCISCONCCISCCINCCISCCINCUSC__________________ ______Iii ________tO ________...._i_.u_flE..s.7t r_r%_t.%1_I sti 4..__..4 fl-.1
Additional Comments Siie.ArrIvaJ .rlne.bptUŁ
FleidTechFe
SEE REVERSE FORTERMSCONDITIONS
CHAIN OF CUSTODY RECORD
NO NIAPAGE..L _L RUOTE ENSUR PROP 1NG 7anipsINThCT UPDn anival _x../
Project Name w.
Short Hold Analysis Yes No UST Project Yesj....4No Recevd W1THN fi0LDINBriMES JjPleaseATTACHanyproject specific reporting
00 LEVEL 111111 IV CUSTODY SEALS iNTACTprovisionsand/or QC Reuirms jIInvoiceTo_2 jj PR6IER cqlThiNERs UsedAddress-----/M Il/fiz
Purchase Order No./Biliing Reference 1111 4Z1
Requested Due Date Day 02 Days 03 Days 04 Days 4bays
Working Days 06-9 Days Standard 10 days usWarkust Be
Samples received after 1500 wIll be processed next business dayTurnaroundtimeisbasedonbusInessdaysexcludingweekends and holidaysSEEREVERSE FOR TERMS CDNDfl1QNS REGARDING SERVICESRENDEREDBY PRISM I.AS0NATORIES INC TO CLIENT
TO BE FILLED IN BY CUENT/SAMPLING PERSONNEL
Certification NELAC USACE_FL____NCLSC_OTHER _____ _____
Water Chlorinated YES_NO
Sample Iced Upon Collection YESj NO
CLIENT DATESAMPLEDESCRIPTIONCOLLECTED
JLLi
TIME
COLLECTED
MILITARY
HOURS
ia
//5__
MATRIX
SOILWATER OR
SLUDGE
__
SAMPLE CONTAINER
ANALYSES REQUESTED
PRESERVA--/TIVES REMARKS/S7i__iPRISM
ID NO
I5s
TYPE
SEE SELOW
-4/
NO SIZE
flRliIN AL
JUL ZOQ7
PRISM
ODIESINC
Date 07/16107
Company ESP Associates PA
Contact Chris Ward
Address Box 7030
Chariolle NC 28241
Client Project ID
Prism CCC Group No
Collection Dates
Lab Submittal Dates
Case Narrative
Morehead Commons No
G0707087
07/05107
07/05107
This data package contains the analytical results for the project identified above and Includes Case Narrative Laboratory Report
and QualityControlDatatotaling14pageschain-of-custody is also attached for the samples submitted to Prism for this project
Data qualifiers are flagged individually on each sample key reference for the data qualifiers appears at the end of this case narrative Qualitycontrolstatementsand/or sample specific remarks are Included in the sample comments section of the laboratory report for each sampleaffected
Semi Volatile Analysis
No Anomalies Reported
Volatile Analysis
WA
Metals Analysis
Analysis Note for 024880 NSf Chromium RPD value outside the control limits Sample is not homogeneous
Wet Lab and Micro Analysis
N/A
Please call if you have any questions relating to this analytical report
Date Reviewed by Robbi Jones Project Manager
Signature 11 Signature
Review Date 0711 6/07 Approval Date
Data Qualifiers Key Reference
Compound also detected in the method blank
Result outsldeof the 06 lImits
DO Compound diluted out
Estimated concentration calibration range exceeded
The analyte was podtlvety identified but the value Is estimated below the reporting limit
Estimated concentration with high bias
Estimated concentration with low bias
matrix effect Is present
7eroash 42
fj6I07
Notes This report should not be reproduced except In Its entirety without the writtten consent of Prism Laboratories inc The results in thisreportrelateonlytothesamplessubmittedfbianalysis
449 Spcfngbrook Road P.O Box 240543 Charlotte NC 282240403
Phonc 704/529-6394 Toll Fme 800/529-6364 Fax [phone]
ESP Associates PA
Atm Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
07/16/07
Project ID Moreliead Commons No Client Sample ID WS-2
Prism Sample ID 186280
Sample Matrix Soil COG Group G0707087
Time Collected 07/05/07 1500
Time SubmItted 07/05/07 1520
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Percent Solids Determination
Seml.volatlla Organic Compounds by GCMS
124-Trichlorobenzene BRI
12-Dlchlorobenzene BRL
3-Dlchlorobenzene BRL
14-Dlchlorobenzene BRL
245-Trichlorophenol BRL
246-Trichiarophenol BRL
24-Dichiorophenol BRL
24-Dimethyiphenol BRI.
24-Dinitrophenol BRL
24-Olnitrotoluene BRL
26-Din itrotoluene BRL
2-Chioronaphihalene BRL
2-Chiorophenol BRL
2-Methylnaphthalene BRL
2-Methyiphenol BRL
2-Nltmphenol BRL
34-Methylphenol BRL
3.3-Dlchiorobenzldlne BRJ.
46-Dlnltro-2-mettylphenol BRL
4-Bremophenyiphenylether BRL
4-Chloro-3-methylphenol BRL
4-Chioroaniline BRL
4-Chlorophenylphenylethej-BRL
4-Nitrophenol BRL
07/13/07 507 kcamplgotto 024946
07/13107 507 kcarnpigotto 024945
07/13/07 507 kcamplgotto Q24946
07/13107 507 küampigotlo 024940
07/13/07 507 kcamptgotlo 024946
07/13/07 507 kcamplgotlo 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampgoUo 024946
07/13/07 507 kcamplgotto 024946
07113/07 507 kcamplgotto 024946
07113/07 507 kcamptgotto 024946
07/13/07 507 kcernpisatto 024946
07/13/07 507 kcamplgolto 024946
07/13/07 507 kcampgotto 024946
8270C 0713/07 507 kcampigotto 024946
8270C 07/13/07 507 kcamplgotto 024945
827CC 07/13/07 507 kcamplotb Q4945
8270C 07/13/07 607 kcamplgotto 024946
82700 07/13/07 507 kcamplgotto 024946
82700 07/13/07 507 keamplgotto 024946
827CC 07/13/07 507 kcamplgotto Q24940
8270C 07/13/07 507 kcamplgotto 024946
B270C 07/13/07 507 kcamplgotto 024946
82700 07/13/07 507 kcamptgotto 024946
This report should not be reproduced except In Its entirety without the written consent of Prism Laborotories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/5294364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Percent Solids 93.5 SM2540 07/1007 1300 aihan
827CC
827CC
82700
8270C
8270C
827CC
827CC
827CC
827CC
82700
827CC
827CC
82700
82700
mg/kg 0.35 0.035
mg/kg 0.35 0.026
mg/kg 0.35 0.026
mg/kg 0.35 0.032
mg/kg 0.35 0.036
mg/kg 0.35 0.034
mg/kg 0.35 0.030
mg/kg 0.35 0.034
mg/kg 1.8 0.040
mg/kg 0.35 0.020
mg/kg 0.35 0.038
mg/kg 0.35 0.037
mg/kg 0.35 0.028
mg/kg 0.35 0.028
mg/kg 0.35 0.033
mg/kg 035 0.042
mg/kg 0.35 0.036
mg/kg 0.71 0.022
mg/kg 1.8 0.022
mg/kg 0.35 0.034
mg/kg 0.71 0.026
mg/kg 0.35 0.046
mg/kg 0.35 0.022
mg/kg 1.8 0.024
Page ot9
.4
Ft.MAnJytJcaI m5utroni
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
01/13/07 507 kcamplgotto 024946
0713/07 507 kcamptgoUp 024946
01/13/07 507 kcarnplgottc 024946
07/13107 507 kcampigolto 024946
07/13/07 507 kamptgouo 024945
07/13/07 507 kcampgottc 024946
07113107 507 kcsmplgoftc 024946
07/13/07 507 kcamplotto 024946
07/13/07 507 kcamplgotto 024945
07/13/07 507 keamplgotto 024946
07/13/07 507 kcamplgotto 024946
07/13/07 507 kcampigotto 024946
0713/07 507 kcamplgotio 024946
07/13/07 507 kcamplgotto 024945
07/13/07 507 kcamplgotto 024946
07/13/07 507 kcamplgotto 024946
07/13/07 507 kcampigctlo 024946
07113107 507 hcamplgotto 024946
07113/07 507 kcamplgotto 024946
07/13/07 507 kcamplgctto 024946
07/13/07 507 kcamplgotto 024946
07/13/07 507 kcamplgotto 024945
07/13/07 507 kcamplgotto 024946
07113107 507 kcamplgotto 024946
07/13/07 507 kcamplgatto Q24949
0711 307 507 keamplgotto 024946
07/13/07 507 kcamplgotto Q24945
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Laboratory Report
07/16/07
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 186280
Sample Matrbc Soil coc Group G0707087
Time Collected 07/05/07 1500
Time Submitted 07/05/07 1520
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
827CCAcenaphtheneBRLmg/kg 0.35 0.035
Acenaphlhylene BRL mg/kg 0.35 0.035 8270C
Anthracene BRL mg/kQ 0.35 0.027 827CC
Azcbenzene BRL mg/kg 1.8 0.033 627CC
Benzoaanthracene BRt mg/kg 0.35 0.050 8270C
Benzoapyrene BRL mg/kg 0.35 0.041 8270C
Benzobfiuoranthene BRL mg/kg 035 0.016 827CC
Benzoghlperylene BRL mg/kg 0.35 0.017 827CC
Benzokfiuorantjiene BRL mg/kg 0.35 0029 827CC
Benzoic acid BRL mg/kg 1.8 0.15 827CC
Benzyl alcohol BRL mg/kg 0.71 0.037 8270C
Bls2-chloroethoxymethane BRL mg/kg 0.35 0.041 827CC
8Is2-chloroethylether BRL mg/kg 0.35 0.038 827CC
Bls2-chlorolsopropy9ether BRL mg/kg 0.35 0.030 827CC
Bis2-ethythexylphthalate BRL mg/kg 0.35 0.017 8270C
Butylbenzylphthalate BRL mg/kg 0.35 0.022 827CC
Chrysene BRL mg/kg 0.35 0.059 827CC
DI-n-butylphthalate BRL mg/kg 0.35 0.016 8270C
Dl-n-octylphthalate BRL mg/kg 0.35 0.026 827CC
Dlbenzoahanthracene BRL mg/kg 0.35 0.036 827CC
Dlbenzofuran BRL mg/kg 0.35 0.030 627CC
Dlethylphthalate BRL mg/kg 0.35 0.022 8270C
Dlmethylphthalate BRL mg/kg 0.35 0.024 8270C
Fluoranthena 0.14 mg/kg 0.35 0.024 827CC
Fluorene BRL mg/kg 0.35 0.021 827CC
Hexachlorobenzene BRL mg/kg 0.35 0.018 8270C
Ilexathlornbutacftene BRL mg/kg 0.35 0.034 827CC
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc449SprlngbrookReadP.O Box 240543 Charlotto NC 28224-0543
Phone [phone] ToIl Free Number 1-80015294364 Fac 704/525-0409 Page of
ESP Associates PA
Attri Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
07/16/07
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 186280
Sample Matrix Soil COG Group G0707087
Time Collected 07/05/07 1500
Time Submitted 07/05/07 1520
07/13/07 507 kcamplgolto Q24945
07/1307 507 kcaniplgottu 024946
07/13/07 507 kcamplgotto 024946
07/13/07 507 kcampqotto 024946
07/13/07 507 kcamptgotto 024946
07/13/07 507 kcamptgotio 024946
07/13/07 507 kcamplgoltu 024946
07/13/07 507 kcamplgottc 024946
07/13/07 507 kcamplgotto 024946
07/13/07 507 kcamplgolto 024946
07/13/07 507 kcamplgotto 024946
07/13/07 507 kcamplgouo 024946
07/11/07 800 dpope P18865
Surrogate Recovery Control Limits
Terphenyl-d14 101 41-136
Pheriot-d5 73 13-95
Nltmbenzene-d5 76 14-103
2-Fluorophenol 63 14-89
2-Fluoroblphenyl 75 21 108
246-Tdbmmophenol 102 25-123
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Sprinybrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
SIoAnyI CvIiTrnlmft1
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
rhlnrir4nnnt2rIIon
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/lime ID
.....BRL mg/kg 0.35 0.038 8270C
Nexachioroethane SRI mg/kg 0.35 0.036 8270C
lndeno123-cdpyrene BRL mg/kg 0.35 0.036 8270C
tsophorone ERL mg/kg 0.35 0.032 8270C
NNitrosodi-ri-propyiamine BRL mg/kg 0.35 0.040 82700
N-Nitrosodlphenylamlne SRI mg/kg 0.35 0.018 82700
Naphthalene BRL mg/kg 0.35 0.039 82700
Nltrobenzene SRI mg/kg 0.35 0.035 8270C
Pentachlorophenal SRI mg/kg 1.8 0.030 8270C
Phenanthrene BRL mg/kg 0.35 0.017 8270C
Phenol SRI mg/kg 0.35 0.039 82700
Pyrene 0.16J mg/kg 0.35 0.024 82700
Sample Preparation 29.85g mL 3550B
Page of
NC Certification No 402 Laboratory ReportScCertificationNo99012
NC Drinking Water Cert No 37735 07116/07
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 18628G
Sample Matrix Soil COC Group G0707087
Time Collected 07/05/07 1500
Time Submitted 07/05/07 1520
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Sample Comments
BRL Below Reporting Limit
J-Estimated value between the Reporting Limit and the MDL
The results In this report relate only to the samples submitted br analysis and meet state certification requirements other thanNELACcertificationexceptforthose Instances Indicated In the case narrative and/or test comments
All results are reported on dry-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories be
449 Sprlngbrook Road P.O Box 240543 Charlotto NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6354 Fax [phone]
ESP Associates PA
Chris Ward
Box 7030
Charlotte NC 28241
Page of
NCCertItIcaUonNo.402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cart No 37735
Enmnt5bbjtt
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 186281
Sample Matrbc Soil COC Group G0707087
Time Collected 07/05/07 1505
Time Submitted 07105/07 1520
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Numbec 1-800/529-6364 Fax [phone]f9
ESP Associates PA
Aftn Chris Ward
Box 7030
Charlotte NC 28241
07/18/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Acenaphthene BRL mg/kg 0.35 0.034 827CC 07/13/07 559 kcamplgotlo 024946
Acenaphthylene BRL mg/kg 0.35 0.035 827CC 07/13/07 559 kcamplgolln Q24946
Anthracene BRL mg/kg 0.35 0.026 827CC 07/13/07 559 kcamplgotto 024946
Azobenzene BRL mg/kg 1.7 0.032 827CC 07/13/07 559 kcamplgotlo Q24946
.Benzoaanthracene BRL mg/kg 0.35 0.049 827CC 07/13/07 559 kcamplgotto Q24949
Benzoapyrene BRL mg/kg 0.35 0.040 827CC 07/13/07 559 kcampigolto 024946
Benzabfluoranlhene BRL mg/kg 0.35 0.016 827CC 07/13/07 559 kcamplgouo 024946
Benzoghjperylere BRL mg/kg 0.35 0.017 8270C 07113107 559 kcamplotto 024946
Benzokfluoranthene BRL mg/kg 0.35 0.028 8270C 07/13/07 559 kcamplgotto 024946
Benzoic acid BRL mg/kg 1.7 0.15 827CC 07/13/07 559 kcampIgotto 024946
Benzyl alcohol BRL mg/kg 0.70 0.037 827CC 07/13107 559 kcamplgctto 024946
Bls2-chloroethoxymethene BRL mg/kg 0.35 0.040 827CC 07/13/97 559 kcamplgotto 024945
BIs2-chloroethylether BRL mg/kg 0.35 0.038 827CC 07/13/07 559 kcamploUo 0.24948
Bls2-chlorolscpropylether BRL mg/kg 0.35 0.030 827CC 07/13101 559 kcamplgotto 024945
BIs2-etliylhexylphtl-ialate 8RL mg/kg 0.35 0.017 827CC 07/13/07 559 kcamplgolto 024946
Butylbenzylphthalaje BRL mg/kg 0.35 0.021 8270C 07/13/07 559 kcarrpigollo 024946
Chrysene BRL mg/kg 035 0.058 827CC 07/13/07 559 kcamptgotio 024946
DI-n-butylphthalate BRL mg/kg 0.35 0.016 827CC 07/13/07 559 kcamplgotio 024946
DI-n-octphthalate BRL mg/kg 0.35 0.026 827CC 07/13/07 559 kcamplgotto 024946
Dlbenzoahanthracene BRL mg/kg 0.35 0.035 827CC 07/13/07 559 kcampigolto 024946
Dlbenzofuran BRL mg/kg 0.35 0.030 827CC 07113/07 559 kcamplgotlo 024945
Dlethylphthalate URL mg/kg 0.35 0.021 8270C 07/13/07 559 kcamplgotio 024948
Dlmethylphthalate BRL mg/kg 0.35 0.024 8270C 07/13/07 559 kcamplgolb 024946
Fluoranthane 0.20 mg/kg 0.35 0.024 827CC 07/13/07 559 kcamplgctto 024946
Fluorene BRL mg/kg 0.35 0.021 827CC 07/13/07 559 koamplgotto 024946
l-Iexachlorobenzene BRL mg/kg 0.35 0.018 827CC 07/13/07 59 kcamplgottc 024946
Hexachiorobtitadlene BRL mg/kg 0.35 0.034 827CC 07/13/07 559 kcamplgotto 024946
Page of
No 402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cart No 37735 07/16/07
Project ID Morehead Commons No Client Sample ID WS-3
PrIsm Sample ID 186281
Sample Matrix Soil COC Group GO1O7O8T
lime Collected 07/05107 1505
Time Submitted 07/05/07 1520
Hexathlorocyclopentadlene
Hexachioroethane
Indeno123-cdpyrene
Isophorone
NNitrosoth-n-propy1amIne
N-Nltmsodiphenylamlne
Naphthalene
Mtrcbenzene
Pentachiorophenol
Phenanthrene
Phenol
Pyrene
BRL mg/kg 0.35 0.037
BRL mg/kg 0.35 0.035
BRL mg/kg 0.35 0.036
BRL mg/kg 0.35 0.031
BRL mg/kg 0.35 0.039
BRL mg/kg 0.35 0.018
SRL mg/kg 0.35 0.038
BRL mg/kg 0.35 0.034
BRL mg/kg 1.7 0.029
0.11 mg/kg 0.35 0.017
BRI mg/kg 0.35 0.038
0.22 mg/kg 0.35 0.024
07/13/07 559 kcamplgotto 024946
07/1307 559 kcamplgotto 024946
0713/07 559 kcamplgotto 024946
07/13/07 559 kcamplgotto Q24945
07/13/07 559 kcampl9otto 024946
07/13/07 559 kcamplgotlo 024946
07/1307 559 kcamplgotto 024946
07/13107 559 kcampboito 024946
07/13/07 559 kcamplgotta 024946
07/13107 559 kcamplgotto 024946
07/13107 559 kcamplgotto 024946
07/13107 559 kcamplgotto 024946
07/11/07 800 dpope P18865
Surrogate Reooveiy Control Limits
Terphenyl-d14 100 41 -136
Phenoki5 69 13-95
Nitsubenzene-d5 73 14-103
2-Fluorophenol 73 14-89
2-Fluoroblphenyl 72 21 108
24G-Trlbromophenol 113 25-123
Extractable Petroleum Hydrocarbons by GC-FID
C11-C22Ammatjcs BRL mg/kg 10 5.4 MADEP EPH 07/12/07 928 grappacctofi 024910iialysisNoteforCll-C22 Jtrotnatics Adjusted value
C19-C36 Aliphalics BRL mg/kg 10 1.5 MADE EPH 07/12/07 928 WaPPSCCIOH 024910
C9-C18 Aliphatics BRL mg/kg 10 3.2 MADEP EPH 07/12/07 928 grappaccloli 024910
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Numben 1-800/529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
827CC
8270C
8270C
827CC
827CC
827CC
827CC
827CC
827CC
8270C
8270C
8270C
Sample Preparation 29.73g mL 35508
Page of
ESP Associates PA
Atm Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-3
186281
G0707087
07/05/07 1505
07105/07 1520
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Sample Preparation 10.47g mL EPH 07/09107 1100 dpope P18855
Surrogate Recovery Control Limits
o-Terphenyl 74 40-140
2-Fluorobiphenyl 56 40-140
2-Bromonaphthalene 54 40 -140
1-Chloro-octadecane 79 40-140
Sample Comments
BRL Below Reporting Umit
J-Estimated value betheen the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis end meet state certification requirements other thanNELACcertificationexceptorthoseInstances Indicated in the case narrative and/or test comments
Al/results are reportedon thy-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704iS29-634 Toll Free Number 1-8001529-6354 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
07/1 6/07
Page of
ESP Associates PA
Atth Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No.402
SC Certification No 99012
NC Drinking Water Cart No 31735
Project ID Morehead Commons No Client Sample ID B-I
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
186282
G0707087
07/05/07 1510
07/05/07 1520
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Daternme ID
Metals by ICP
ChromIum 26 mg/kg 0.25 0.015 60108 07/10/07 2353 mcampbell Q24880
Sample Preparation 2g 50 mL 305DB 07/09/07 800 Jhoppal P18845
Sample Comments
BR Below Reporting Limit
J-Estimated value between the Reporting Limit and the MDL
The results In this report relate only to the samples submitted for analysis and meet state certification requirements other thanNEL.AC certification except for those Instances indicated in the case narrative and/or lest comment
All results are reportedon wet-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SprtngbrookRoadP.O Box 240543 Charlotte NC 2822441543
Phone [phone] Toll Free Number I-8001529.6364 Fax [phone]
eMc Ailyea2 ntcnnmtIS%Kfl5
Laboratory Report
07/16/07
Page 9019
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
7/16/2007
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No COC Group Number G0707087
Date/lime Submitted 7/5/2007 1520
This report should not be reproduced except In Ifs entirety without the written consent of Prism Laboratodes Inc449SprlngbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Foil Bar AnyIlmIB Erwknt$SekrUorrs
Metals hvlrn ....uk....1 BtHOR
Method Blank
Result RI Conlrot Unat Units 10
ChromIum 0.0662 0.25 0.125 mg/kg 024880
Laboratory Control Sample Recoy Recovery
RangesResultSpikeAmountUnits ID
Chromium 22.7819 25 mg/kg 91 80-120 024880
Matrix Spike Rvy Recovery cc BatchRangesIDSampleIDResult Spike Amount Units
186342 ChromIum 34.5949 25 mg/kg 113 75-125 024880
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD p.ge 00 BaIth
Sample ID Result Spike Amount Units
186342 ChromIum 27.9758 24.875 mg/kg 87 75-125 21 0-20 024680
Extractable Petroleum Hydrocarbons by 3C-FID method MADEP EPH
Method Blank
DCResultRLControl Urnit Units ID
C11-C22Aromatlcs ND 10 mg/kg 024910
C19-C36 Aliphatics ND 10 mg/kg 024910
C9-C18 Allphatics ND 10 mg/kg 024910
Laboratory Control Sample Recovery Iovery
Ranges DOBatchResultSpikeAmountUnitsID
C11-C22Ammafjcs 128.22 170 mg/kg 75 40-140 024910
C19-C36AllphatIcs 41.94 80 mg/kg 52 40-140 024910
C9-ClBAifphatlcs 31.9 60 mg/kg 53 40-140 024910
Matrix Spike Recovery Recovery
Ranges DC BatchSampleResultSpike inount Units ID
186445 C11-C22Aromatjcs 137.74 170 mg/kg 81 40-140 024910
C19-C3BAIIphaIics 44.08 80 mg/kg 55 40-140 024910
C9-C18 AlIphatics 32.06 60 mg/kg 53 40-140 024910
Matrix Spike Duplicate
Recovery Racovury RPD
Ranges RPI Range DC BatchSamplepiResultSpikeAmountUnitsID
186445 C11-C22 Ammaflcs 119.6 170 mg/kg
C19-C36 Allphatlcs 52.7 80 mg/kg
C9-Cl8AIiphatIcs 37.12 60 mg/kg
70 40-140 14 0-50 024910
66 40-140 18 0-50 024910
62 40-140 15 0-50 024910
Page lof
ESP Associates PA
Attn Chits Ward
O.Box 7030
Charlotte NC 28241
flrr.b 5..fI1RCC ......IL....l qne.......uICIJflJtI USIUJ
Method Blank
Result RI Conisul Umit Units ID
2.4-Trichlorobenzene
1.2-Dlchlorobenzene
13-Dlchlorobonzane
4-Olchlorobenzene
2.45-Trichiorophenol
246-Trlchiotophenol
24-Dlchiorophortol
24-Olmethyiphenol
24-Dinitropheriol
24-Dinitrotoluene
26-Dinitrotoluene
2-Chtoronaphthalene
2-Chiorophenol
2-Methylnaphthalene
2-Methyiphenol
2-Nitrophenol
34-Methyiphenol
33-Dichlorobenzldjne
46-Dlnitro-2-methylphenol
4-Bromopheriylphenylether
4-Chloro-3-methylphenol
4-Chioroanihne
4-Chloropheriylphenylether
4-Mtrophenol
Aceriaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzoaanthracene
Benzaapyrene
Benzobfluoranthene
Benzoghtperylene
Oenzokfluoranthene
Benzclc acid
NC CertIfication No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Level II QC Report
7/16/2007
Project ID Morehead Commons No COC Group Number G0707087
Date/Time Submitted 7/5/2007 1520
ND 0.33 0.165 mg/kg 024946
ND 0.33 0.165 mg/kg 024946
ND 0.33 0.165 mg/kg 024946
ND 0.33 0.165 mg/kg 024946
ND 0.33 0.165 mg/kg 024946
ND 0.33 0.165 mg/kg 024948
ND 0.33 0.165 mg/kg 024946
ND 0.33 0.165 mg/kg 024946
ND 1.65 0.825 mg/kg 024946
ND 0.33 0.165 mg/kg 024946
ND 0.33 0.165 mg/kg 024946
ND 0.33 0.165 mg/kg 024949
ND 0.33 0.165 mg/kg 024946
NI 0.33 0.165 mg/kg 024946
ND 0.33 0.165 mg/kg 024946
ND 0.33 0.165 mg/kg 024946
ND 0.33 0.165 mg/kg 024946
ND 0.68 0.33 mg/kg 024946
ND 1.65 0.825 mg/kg 024946
ND 0.33 0.165 mg/kg 024946
ND 0.66 0.33 mg/kg 024946
NI 0.33 0.165 mg/kg 024946
ND 0.33 0.165 mg/kg 024946
ND 1.65 0.825 mg/kg 024946
ND 0.33 0.165 mg/kg 024948
NI 0.33 0.165 mg/kg 024949
NI 0.33 0.165 mg/kg 024946
ND 1.66 0.825 mg/kg 024949
ND 0.33 o.iss mg/kg 024946
ND 0.33 0.165 mg/kg 024946
ND 0.33 0.165 mg/kg 024946
Ni 0.33 0.165 mg/kg 024946
NI 0.33 0.165 mg/hg 024946
ND 1.65 0.825 mg/kg 024946
This report should not be reproduced except In its entirety without the written consent ot Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone[phone]-s54 Toll Free Number 1-8001529-6354 Fax [phone] Page of
NC Certlflcation No 402 Level II QC ReportSCCertificationNc99012
NC Drinking Water Cart No 37735
5inds An fjticninvhsuimnbI aIutJnnn
124-Tdchlorobenzene
14-Dichlorobenzene
24-Dinitrotoluene
2-Chlorophenol
4-ChIoro-3-methyiphenol
1.26414 1.6742
1.22999 1.6742
1.51188 1.5742
1.41144 1.6742
1.40709 1.6742
mg/kg 76 39-98
mg/kg 73 3795
mg/kg 90 56-128
mg/kg 84 37-98
mg/kg 84 45-111
024946
024946
024946
024946
Q24946
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte MC 28241
7/16/2007
Project ID Morehead Commons No COC Group Number G0707087
Date/Time Submitted 7/5/2007 1520
Method Blank OC
Result RI Conimi Umit Units ID
Benzyl alcohol ND 0.66 0.33 mg/kg 024946
Bls2-chloroethoxymethane ND 0.33 0.165 mg/kg 024946
BIs2-chloroethylether ND 0.33 0.155 mg/kg 024946
Bis2-chlorolsopropylether ND 0.33 0.165 mg/kg 024946
Bls2-ethylhexylphthalate ND 0.33 0.165 mg/kg 024946
Butylbenzylphthalate ND 0.33 0.165 mg/kg 024946
Chrysene NI 0.33 0.165 mg/kg 024946
DI-n-butylphthalate ND 0.33 0.165 mg/kg 024946
Dl-n-octylphthalate ND 0.33 0.165 mg/kg 024946
Dibenzoahanthracene ND 0.33 0.165 mg/kg 024946
Dibenzoiuran ND 0.33 0.165 mg/kg 024946
Diethylphthalate MD 0.33 0.155 mg/kg 024946
Dimethyiphihalate ND 0.33 0.165 mg/kg 024946
Fluoranthene ND 0.33 0.165 mg/kg 024945
Fluorene MD 0.33 0.165 mg/kg 024946
Hexachlorobenzene ND 0.33 0.165 mg/kg 024946
Hexachiorobutadlena ND 0.33 0.165 mg/kg 024945
Hexathlorocyclopentadlene ND 0.33 0.165 mg/kg 024946
Hexachloroethane ND 0.33 0.165 mg/kg 024946
lndeno123-cdpyrene ND 0.33 0.165 mg/kg 024946
Isophorone ND 0.33 0.165 mg/kg 024946
N-Nltrosodi.n.propylamlne ND 0.33 0.165 mg/kg 024946
N-Nltrosodlphenylamine ND 0.33 0.165 mg/kg 024946
Naphthalene ND 0.33 0.165 mg/kg 024946
Nltrobenzene ND 0.33 0.185 mg/kg 024946
Pentachiorophenol MD 1.65 0.825 mg/kg Q24946
Phenanthrene ND 0.33 0.165 mg/kg 024946
Phenol Nt 0.33 0.165 mg/kg 024946
Pyreno ND 0.33 0.165 mg/kg 024946
Laboratory Control Sample RaCOVOF cc BatchResultSpikeAmountUnitsID.-.------
This report should not be reproduced except In Its entirety without the written consent of Prism t.aboratories Inc449SprlngbrookRoadP.O Box 240543 Charlotte NC 28224-0643Phone[phone] Toll Free Numbar 1-800/529-8354 Fax [phone] Page 3of4
186433 24-Trlchlorobenzerte
4-Olchlorobenzene
24-Dlnllrotofuene
2-Chiorophenol
4-Chloro-3-rnethylphenol
4-Nlfropheriol
Acenaphthene
N-Nltrosodl-n-propylamlne
Pentachlorophenol
Phenol
Pyrene
-See Case Narrative
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SprlngbrookRoadP.O Box 240543 Charlotte NC 282244543
Phone [phone] Toll Free Number 1-8001529-6394 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Level II QC Report
7116/2007
Project ID Morehead Commons No COC Group Number G0707087
Date/Time Submitted 7/5/2007 1520
Laboratory Control Sample Recovery Recovery
Ranges OC Batch
Result Spike Mrount Units 1k ID
4-Nltrophenol 0.97991 1.6742 mg/kg 59 20-157 024946
Acenaphthene 1.29092 1.6742 mg/kg 77 44-110 024946
N-Nltrosodl-n-propylamlne 1.38935 1.6742 mg/kg 83 38-101 024946
Pentachiorophenol t94174 1.6742 mg/kg 116 53-127 Q24946
Phenol 1.26146 1.6742 mg/kg 75 34-102 024946
Pyrene 1.54837 1.6742 mg/kg 92 54-131 024946
Matrix Spike Recovery Recovery
Ranges QC Batch
Sample ID Result Spike Amount UnUs ID
186433 124-Trichlorobenzene 1.23412 1.6537 mg/kg 75 26-97 024946
1.4-Dlchlorobenzene 1.13723 1.6537 mg/kg 69 23-92 024946
24-Dlnjtjotoluerie 1.65211 1.6537 mg/kg 100 45-127 024946
2-Chlorophenol 1.14351 1.6537 mg/kg 69 25-94 024948
4Chloro-3-methylphenol 1.25562 1.6537 mg/kg 76 31-113 024946
4-Nltropttenol 0.96197 1.6537 mg/kg 58 17-150 024946
Acenaphthene 1.28406 1.6537 mg/kg 78 36-107 024946
N-Nitmsodl-n-propylamlne 1.25661 1.6537 mg/kg 76 22-105 024946
Pentachlorophenol 1.88095 1.6537 mg/kg 114 39-137 024946
Phenol 1.12830 1.6537 mg/kg 68 23-97 024948
Pyrene 1.44907 1.6537 mg/kg 88 45-1 33 024946
Matrix Spike Duplicate Racovory Recovery RPD
Ranges RPD Range 00 Batch
Sample Result Spike Amount Units
1.37073 1.6743 mg/kg 82 26-97 10 0-37 024946
1.11520 1.6748 mg/kg 67 23-92 0-36 Q24948
1.36537 1.6748 mg/kg 82 45-1 27 19 0-29 024946
.201 94 1.6748 mg/kg 72 25-94 0-37 024948
1.43402 1.6748 mg/kg 86 31-113 13 0-32 0.24946
0.81212 1.6748 mg/kg 43 17-150 17 0-32 024946
1.15472 1.6748 mg/kg 69 36-107 11 0-32 024946
1.18687 1.6748 mg/kg 71 22-105 0-37 024946
1.84192 1.6748 mg/kg 110 39-137 0-27 Q24946
1.14902 1.6748 mg/kg 69 23-97 0-42 024948
1.47957 1.6748 mg/kg 83 45-133 0-27 Q24946
Page of
CHAIN OF CUSTODY RECORD
PAGE ....L QFJ QUOTE ENSfiE PR9PE IU.IHO.______________
ProJectName __________---.----PROPER RERVATiVE5l dic adShortHoldAnalysisYesNoliSTProjectYesNo
____________________________pleaes ATTACH any project specific reportin QC LEVEL II III IVprovsponsand/or QC Requirem
________________Purchase Order NoJEifling Reference 11j1 e-
Requested Due Date Day Days
03 Days 04 Days UDays ______Working Days
06-9 Days Standard 10 days 0U5Workust Be
Samples received after 15 will be processed next business dayTurnaroundlimeIsbased on busIness days excluding Weekends and holidaysSEEREVERSE FOR TERMS CONDmONs REGARDING SERVICESRENDEREDBY PRISM LABORATORIES INC TO CUENfl
TIME MATRIX SAMPLE CONTAINER NALYSES REQUESTED PRISMSAMPLEaESCRIpTIONCOLLECTEDswNO
PRESERVA-
/7/i///REMARKS
025-2 7-c-o__ioo__-__GTL ______________________________/c1 VI
j.iiz
iJ .-I.l4-Samplers Signature Sampled By Print Name 1W-ç.$Affiliation 2i ...cr
Upon relinquishing this Chain of Cst Is your authorization for Prism to proceed with the analyses as requested above Any changes must besubmittedinwritingtothe PrIsm Project Manager There wilt be charges for any changes after analyses have been Initialized
PIInqultha
0FdEx
By SI
Ours
gaature Recld ny Stgnalura
NoooERs
SE The BORATORYSAFPLEsARENOTACCEPTEDANDVERIFIEDAGAINSTCOCUNTILRECEIVEDATTHELABORATORY
end-doJIvere4 OPdsmFIeIcfSerice UOlher
Date
No
Full Sasviaa Analytical EnvIronmental Solutions
449 Sprlngbrook Road P.O Box 240643 Charlotte NC 28224-0543Phone[phone] Fax 704/5J9
Client Company Name .4.Ot/
Report To/Contact Name
Reporting Address _____________________________
Phone ________________Fax Yes No
Email Yes No Email Address_____________________
EDD Type PDF_ExceI._L.her
Site Location Name /lf/.ih.et.7 jA4LI1.i.1
Site Location Physical Address
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC_USAQE_FL_NC_
SC__OTHER _____N/A_____
Water Chlorinated YES_NO_
Sample Iced Upon Collection YES jNO
Jnqui5nso Uy aIrI5Wre SIgnature Date
MlIflarY/fIöu
Additional Comments r-
NPDES US7 GROUNDWATER DRINKING WATER SOLID WASTE RCRA CERCLA LANDFILL OTHER.DNC USC tNC USC ONC USC UNC USC UNC USC ONC osci UNC USC UNC USC ONC USC-U-____0 ____0__iU __________________I ____lo ____ ____n..nrrn.n nnt rnncc $._j...._nt...rs...nu....az...r r.ai..t....J r...JflA A$..I_141...I 4Y...._I_..._I I....b
SEE REVERSE FORTERMSCONDITIONS
ORIGINAL
SeMco AnaIyiTca Envlrunmental SoiuUons
SP Acoooks
rsCLIENT
AiTh
PRISM COG GROUP
P4
Please fill in the Site Location Information on the attached VPI-I and/or EPH Forms
EPH Site Location for Clienidoc
EPH AliphatlcsAromatics Laboratory Reporting Form
Client Name ESP Associates PA Laboratory Name Prism Laboratories Inc
Project Name Morehead Commons No NC Certification Lab 402
Site Location ______________________________Sample Matrix Soil
Blank
C19-C36 Aliphatics
Cl 1-022 Aromatlcs
C9-C18 Aliohatics
Cl 1-022 Aromatlcs
C9-C18 Alirhatlcs
Cl 9-036 Aliohatics
C11-C22 Aromatics
95.6
10
10
10
10
10
10
10
10
10
3.2
1.5
5.4
79
74
40-140
54
56
Sample Results
10
10
10
Sample Resulls
10
10
40-140
Sample Resull
10
10
10
Sample lnlbrmation and Analytical Results
Method for Ranges MADEP EPH
EPH Surrogate Standards Aliphatic 1-Chloro-octadecane Aromatic o-Terphenyl
EPH Fractionation Surrogates 2-Bromonaphthalene
2-Fluorobiphen I__________________ _________
Sample Identification rt.rir 186281 ___________________________ _________
Date Collected LII1W 7/5/2007 _________ ___________________________Date Received 1IIili 7/5/2007 ___________________________ _________
Date Extracted 7/9/2007 _________ _________ ________________Date Analyzed 7/12/2007 _________ _________ ________
Dry Solids llllll1 ______ __________________
Dilution Factor _________ _________ _________________
Hydrocarbon Ranges in mg/kg Sample Results _________ _________ _________________09 018 Aliphatlcs_jitijtF __________ ___________________ _________C19-C36 Aliphatics
Cl 1-C22 Aromatics _____________________ _______
C9-C18 Aliphatics __________________ ________ ________-iflt ________ ________ _______ _______
C19-C36 Aliphatics 1I 1N ________________ _______
________________________ ________ _______
Surrogate Acceptance Ranqe Blank 40-1 40 40-140 40-140 40-1 40 40-140
RL
MDL
Aliphatic Surrogate Rec
Aromatic Surrogate Rec
Fractionation Surrogate Accep Range
Frac Surrogate Rec
Frac Surrogate Rec
110
93
Blank
99
100
40-140 40-i 40
Sample Resulls
10
10
10
40-140
Unadjusted value should exclude the concentration of any surrogates Internal standards and/or
concentrations of other ranges that elute within the specified range
Adjusted value
MDL Method Detection Limit RL Reporting Limit Blank Laboratory Method Blank
Were all performancelacceptance standards for required QNQC
procedures achieved
Was blank correctIon applied as significant modification of the method
Were any significant modifications to the EPH method made
Comments
YES No Details Attached
Yes NO
NO Yes Details Attached
Page of EPH Soil
APPENDIX
NON-HAZA1DOUS WASTE MANI1STS
ALLIED WASTEPleaseprintortypeINDUSTRIESINC 1/Form designed br use on elIte 12 plIclIn typewriter
..__________
r5.rt
NC
USEPADNumb
Designa FacUlty Name arid Site Address 10 US EPAID Number Facilitys PhoneCMSLandifliQ47B2-20045105MoreheadRd.
13
Total UnitNoipoty
r-r1.cL
/7-
Æpecial Hditng iflSfruUon and
AonrI
Printed l1jped Name
Signature ___jMj
1/5/0/Fl COPY
ALIJED WASTEINDUSIPIEStNC
NON-HAZARDOUS Geæemtos.USp Manifest PageWASTEMANIFESTen
t3eneratorsName and Miffing Addiess Truci NoOJithck3t
Ganeralors Phona
Transporter Company Naæi Cekki--i US EPA ID Number
Transporter Company Name US EPA ID Number
Designated Facility Name and Site Address 10 US EPA ID Number
CMS Landfill
5105 Moreheacl Rd
Concord IIC 28027 ..
11.Waste Shipping Name and Description
biikpatd Su
Trnsporthcir_fl7
Transporters Phone
Facilitys Phone
7047B2-20b4
12 Containers
No Type
13
Total
Quantity
.f/
Additional Descriptions for Mslarias Listed Above Handling Codas br Wastes Listed Above
FU Y7i%
15 Special Handling Instruations and Additional Information ..
14
Unit
WtVol
16 GENERATORS CERTIfICATIONt Fcartity the Etascribed above Ia.mbet arenÆtsubecttefecjaai raculations for raporthig HnzÆdousWas.VV jV/7D Th
/.4.çf i.4f7Ii
lu
.-____________Printed /1jped Name lgnature 1/
-.x JJ 127JO7T-IS Transpolier Acknowledgement ol Receipt of Materials
Printsd/TypedNama Signature
__J01J1h19DiscrepancyIndIcationSpace
T/SIDIFI COPY-
Reese print ortype
Ponrndesfgnertforuee on.Œlla 1.2 pILÆhtyprti5r
.17Tansporte AcknowiàtigmŁfltbiRecaIpj otÆrluls
2e1 127897
Transporter Company Name ffl US EPA ID Number Transporh6jjf..Transporter Company Name US EPA.ID Number Transporters Phone
Dasignated FacjHty Nan and Site Address io US EPA ID Number FacftitysPhonoCMSLandfill7047822db45105 MorØhead Rd
Coflcord NC 28027
11.Waste Shipping Name and Description 12 Containers 13 14
Total UnitNoTypeQuanHWtM
iifl tIi It
ci
Additionai Descriptions for Materials Usled Above
Handling Codes for Wastes listed Above
1725
15 Special Handiin Instructions and Additional information
S.
....T ......SS.S
1...........116GENERATORCERTIFICATIONcarlitythematerialsdescribed aboas on this manlIest are not subject to tedemi regulations for reporting proper disposal of Hazardous WastePrintedTypedNametwaMoDel
17 Transporter Acknowledgement of Receipt of Materials
Printed/Typed Name
18 Transpolter2 Aoknawiedgemart of Recdpt of Mter1ais
Printed/Typed Name
Signature
19 Discrepancy Indication Space
Please
Forinc
Generators Name and
YE
Generators Phone
w1.ia Sr4ChneNC223
7tM-37O-72oO
Truck No
\ttrrjj
WASTE.INDU 5.1 RI SIN
NONHAZARDOUS I.GeneratorsUSEpAjDNo ManUF 2.PagelWASTEMANIFESTocumenof 7898
GenerÆthjs Nmee itnd Mailing Address Truck Nouthtt4
Generators Phone i4.7t7
Transporter Company Name jir US EPA ID Number
..ITII.I j........
Transporter Company Name US EPA ID Nimber Transponters Phone
Facilitys PhoneCMSLandifil704782-20045105 Morehead Rd
ConcOrd NC 28027
11 Waste Shipping Name end Description 12 Containers 13 14TotalUnitNoTypeQuantityWWoi
tW_
It
0-
5.
ci _________
Handling Codes for Wastes Listed Above
s-
15 SpecIal Handling instructions and Additional information
Printed /1rped Name
ynaure /1iL_zi17TransporterAcknowledgementofReceiptofMaterials
PdnIedu1pocf Mania
2oFediity Owner or Opaar CeriHcatio of racetoftIi
PiBase print or typeFormdesignedJar usoon elIte 12 plteb typswrttsrl 141V4
Additional Descriptions for Materials Listed Above
5/
wAsTE MANIFEST
Generatoe US EPA.JO No meniNo
Gdnsmtors Name and Molting Address Tmck No
tu1S.k hfi r.4 tli
LPNU
Generators Pllona
Transporter Company Name US EPA ID Number Transportera
Transporter 2.Company Name US EPA ID Number Transpor1ers Phone
DesIgnated Facility Name and Site Address 10 US EPA ID Number Facilitys Phone
CMS LdndIlti 704 782-20045105MoreheÆdRd
Concord NC 28027
11.Wasle Shipping Name and Doscription 12 Containers 13 14
Total UnitNoTypeQuantityWWoi
Additional Descriptions for Materials Usted Above
Handling Codes forWastes Listed Above
.Hi
15 Special Hartdllng inslructlons and Arldlilonai Information
16 GENERATORtS CERTIFICATION certify the matartes described Ubove on this manUset are not eubf act to federal regulatIons lot reporthig proper dlaposel
01 Hazardous WastePrintedhypedName
j2ure
17 Transporter Acknowledgement of i9aoeipt of Materials _r
Prtnted/TypedNgme Signature f/Mab
--Ig-18 Transporter Acknowledgemenl of Receipt of Materials
Printed /1%jped Name Signature
19 DIscrepancy indication Space
I.
20 Feclltiy Owner or Operator Cerlilcatlon of receipt of waste nteriafs covered by this manliest except as noted in tiara 19
Please pilot or type
Form designed trw use on alto 12 pItch typewriter
ALLIED WASTEW-INDUSTRIES INC H413Pr
15 Special liandiIng Instructions and Additional Informallon _______
Printed/Typed Name Sinnalure_
-u.l7 Transporter 1Acknàw Materials
-fl...
Printed I1jped Name
CMS Landfill
AWIFOrm121TIS/DIF/Copy
Plate ..Prm dTnd tar uaa on iftn Ia auth innwftaru
ALUED WASTE1Nbus1iStw
127891
Generators Nme and MaMn Address Truck NoIiOdIiLiriCuMC2.2
Generjlors Phone TrO4._3772
TransporterMhiit
Tranporlers Phone
Designated Facility Name andSita Address 1D US EPA ID Number Facilitys PhoneCMSLandfill704782-20045105MoroheadRd
CoricordNC 28027
11 Waste Shipping Name and Deer1pIlon 12 ContaIners 13 14TotalUnitNoTypeQuantityWI/Vol
upi iib.
Fl
72T
____________
16 GENERATos CER11FICATION cerilly itie.materiale described above on this manifest Bra not aubleci to federal ragulailone far reporting proper disposal of Hszardou WastePrinted/Typed Name Inaiurep iiry17TransporterAcknowledgementofReceiptof Materials
G7TYPed Name ____
c1of ratwaste
materials
TISJD/F/COPY
Please print ortypa
ALLIED WASTE
Form designed for use on elite 12 p11th typewriter
A/I 21
flT
NON-HAZARDOUS Gdfiratos US EPMD No ManIfest PageWASTEMANIFESTDocumentNo 127892
Printed/Typed Name Signature --j bay
4.tcc..t4 .r..rW34cfT
iz itb O1 Wu
r-tOftt7L
Transpartr1 Company Name US EPA ID Number
Transporter Company Name US EPA tD Number Transporteis Phone
Designated Faclifly Name andSite Address 10 US EPA ID Number Facilitys Phone
CMS Landfill 704 782 20045105MorsheadRd
anaord NC 28027
11 Waste Shipping Name and Doscrlptiori 12 Containers 13 14
No Type Quantity WtN
ii5
Actditiortal Descjiptlona for Materials Listed Above Handling Codes forWastes Listed Above
15 Special Handling instructions and Additional information
18 GENERATORS CERTIFICATION certify the materials described above on this manifest are not subject to federal ragulelkna tar reporting proper diSposal 01 Haztdous Waste
Printed/Typed Name .--.-Cay YeariiL2-.-27V-.--.---V17TransporterAcknowledgementofAdceiptdlMaterials._
Printed /1jpecf Name SIgnatur Man Cay tier
I-J2 -i18TransporterAcknowledgementofReceiptof Materials
20 Facility Owner or Operator Cerificatlon of receipt of waste materials covered by this manifest except noted In item 19CMSLàndfill
Printed/Type Name
Silinatura
AWl FormIl2l
T/S/D/F/COPY
19 DIscrepancy Indication Space
.VV._....___.._
._..._
....
......._...V
Please print or type
Form designed Icr use on eflte 12 pflctypqwrft
WA /7/4/5
Oenethtars Nam and Mailing Address
Generators Phone
Truck No
Ft
Genamlors Name and Malihig Address
GØæer1rPhone
Transporter Company Name
Transporter Company Name
Designated FaallJly Name end Site Address
CMS Landfill
5105 Morehead Rd
Concord NC 28027
11 Waste Shipping Name and Description
pleaeaportypa ALL1D wSTE
FmdaflnBdtorueeonellt12pIIchIypBwIjrer aT9i IN
NONHAZARDOUS Generators US EFAip No.ManIfest PageWASTEMANIFESTDocumentNo
.Ai.t ViJj
LV
Truck No
.1
US EPA ID TransporIh
US EPA ID Number
US EPA ID Number
Transporters Phone
...
Facilitys Phone
704 782-2004
Ipid $eiV
12 ContaIners
No Type
is
Total
Quantity
VILF
14
Unit
WI/Vol
Additional DescriptIon for Materials listed Al3ova
Handling Codes for Wastes listed
tt
lS Special Handling lnstruOtions and Additional information
VVVTransponer Ackno
LLJ
TIS/D/FJ COPY
Please prlntortpa
Form Ignedioruseon elite 12pilch tyjiawriierNONHAZARD.OUS 1.Generators US EPAID No Manifest Page
WASTE MANIFEST ocumen of 127884
Generators Name and Mailing Address Truck No
pj
NC az
Bwwrators Phone 7t
Transporter Company Name US EPA ID Number Transporte VlJon t4
Transporter Company Name US EPA Ii Number Transporters Phone
Designated FaIIiLy Name and Site Address 10 Us EPA ID Number Facilitys Phone
CMB Landfill 704782-20045105 Morehead Rd
Concord NC 28027
11 Waste Shipping Name and Description 12 Containers 13 14
Total UnitNoTypeQuantityWtNoi
Additionai Descriptions for Materials Listed Above Handling Codes for Wastes Listed Above
V..
15 SpecIal HandJin Instructions and Additional Information
16 GENERATORS CERTIFICATION certIfy the materIals dascdbad above on this manifest era not subject to fedaral regulations icr reporting proper dispssa
ni Hazardous Waste
Printed/Typed Name rmture Vrei
____________________________________________17 Transporter Acknowledgnmerrt of Receipt of MatBrlaIs
Printed Typed Name L..Signature asJ712.71 c718Transportar.2 Acknowledgement of Receipt of Metedls
Printed /ipea iJaiuo Sgnature JlfOflth Da Ther
Discrepancy Indication Space
2O Factiity Owner or Operator Cerificallon of receipt of waste materials covered by this manifest except as noted in item 19CMSLandfiii
Printed/Type Name VL I1.IIV
VV AWIForm121
TJS/OIFI COPY
ALLIED WASTEou.sT.RIE5-tN
IIUN-HAZAHDOUSWASTEMANIFFST
WAsTE-__TRIES
Generators Narn Ræd Maflhi Address
ujv itt
l3enerators Phone
........Transporter Company NamB
CMS Landfill
5105 Moreltead Rd ..Concord NC 28027
11 Waste Shipping Name and Description
_No Type ________
AddItional Descriptions for Materials Listed Above HartdIlngcowajd0
tj
15 SpecIal HandlIng Instruclioria and Additional Information
16 GENERATORS CERTIFICATION certify the materials de tbedabono on this ranhfast ale not subject to fidmal regulations for mportlflg proper disposal of Hawrcfofja Waste
17 Transpolier Acknowfacfgomern of Fieceipt of Materials
18 Transporter Acmow1odgerient of Receipt of Materials
OwnaroroperatorcBnficaUonorreIptftd
Please print or type
florm designed tar use on elIte 12 pItch typewriter
Ji .-..ntlest
cument No
Truck No
Transporto
..0.00USEPAIDNumberTransportersPhone
Facilitys Phone
704 782-2004
Fit
14
11011
WlNoi
12 Càntalnors 13
Total
______________Quantity
ALLILD WASTEV-INDUSTI iES..lNC ILI__
NQN-HAZSCRDOUS Genwators.US E1D N_...ll Manifest PageWASTEMANIFEST01
Generators Name and Msliing Address TIiJCk No
it ttb r1CthNC21
Generators Phone
Transporter Company Nams US EPA 10 Number
Transporter Company Name US EPA ID Number Transporter Phone
DesIgnated Facility Name and Site Address 10 US EPA ID Number FacilItys Phone
CMS Landfill 104 782-20045106 Morehead Rd
Concord NC 28027
II Waste Shipping Name and Description 12 ContaIners 13 14..Totel UnitNoTypeguntityWfoi
Listed Above
16 GENERATORS CERTIFICATiON certify the materials described above on this manifest are not subject to federal regulations for reporting proper diupocal ol Hazardous WastePrinted/Typed Name
PaIure JD Menbb
__________________________________________.4c/27 2717TransporterAcknowledgementofReceiptof Materials
Printed ITyped Name
Sigpature JZh18TransporterAcknowledgamentolReceiptMaterials
Printed /1\ipad Name Signature
10 Discrepancy indication Space
__20 FacilIty Ownor or Operator Carifiocitiort of receipt of waste materials covered by this manliest except as noted In item --CMS Landf iii
VV
Prtnei/1pe Name
VV
isi9naturG \i
AWL rm 121.VS/D/C0y ..1J .V
Piassa print or type
Form desigrmd tar use on autO t12 pitch typewriter
Piea5s1Thtorlype
.LLIED WArETRIESINC.jJIiAWUQUS
MANIFsr
UJcnD J4-.-
GeneratorsPhone -i
-.________________________._._._______._____.__.._____
Transporter Company Name nrr US EPA It Num
Transporter Company Name US EPA ID
10 IfS EPA ID Number
DesIgnated Facility Name and Site Address
CMS Landfill5105Morehead RdoncardNC28027
...11 Waste Shipping Name and DesoripUon
s0b0tMat0TT7b9tum ..
CMS LandfIll
rs
Os No
.1
704 782-2004
.....
Additional Descrlplioiis for MaterIals Listed Above
Handling Codes forWastes Listed Above
I3I 72
15 SpecIal Handling lnstructlonsand Additional Informatton _____________
LIED WASTE
/L-/51TRIE5INC
sogh LtttChbMC22
704 -37U-72tit
ManIfest PageNoof 1278 89
SlgnaIUr2...
.I IZ7 107
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Forni designed icr use on stile
NONWA
8eneratôrs Name
Generators Phono
Truck NoAtui
Transportr Company Name fA1tr-US EPA ID Number Tmnspo..i
Transporter Company Name US EPA ID Number Transporters Phone
Designated Facility Name and Site Address 10 US EPA ID Number Facllltys Phone
CMS Landfill 704 782-2004
5105 Morehead Rd ...
Concord NC 28027
11 Waste Shipping Name and Description 12 ContaIners 13 14
UnitNoTyeQuantityWtNoi
rttsz z_7
AdditIonal Descriptions for Materials Listed Above Handling Codes for Wastes Usted Above
15 SpecIal Handling
Instructions and Additional information
16 GENERATORS CERTLFIOA ON Icettty Ite tratericls descflbodbsvson tile manliest ore not sUbJect toledwal uietons lór rÆping pthiard posel of Hazardous Waste
Printed lTypod Name ...
Printed /TYedNàmo .B Hii 9gahire //tw c.
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17 Transporter Acknowledgement of flaceipt ol Materials
18 Transpottar2 Acknowl8dgemantof Receipt of Materials
PrlntedlTypedName
JSlgnature J.i.I ier
19 Discrepancy indication Space
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20 Facility Owner or Operator Cerifloation of receipt of waste materials covered by tht5 manifest C9pt as noted in item 10CMSLandfill
Printed /iljpe Name
SinaIura/
AWForm21-
ALLIED WASTEINDUSTplE5INC
NON-HAZARDOUS Generators US EPA 1D No Manifest PageWASTEMANIFESTot 27882
Generators Name tind Mailing Address thktI Truck Nok1SnhCfrtri vmMNC22
Generators Phone ..--
Transporter Company Name US EPA ID Number TransportsrRhopeç
Transporter Company Name US EPA ID Number Transporters Phone
DesIgnated Facility Name and Site Address 10 US EPA ID Number Faciiitys.PhonoCMSLandIilJ704782 20045105 Morehead Rd
Concord NC 28027
ll.WasteShlpplngNameandDescripuon 12 Containers 13 14
Total UnitNoTypeQuantityWtrVoI
Gb_______
Additional Descriptions for Materials Listed Above
Handling Codes for Wastes Listed Above
it iV
15 SpocisI Handling instructions end Additional Information
16 GENERATORS CERTIFICATION certify the materials described above on ibis manect are not ublect to federal Teguiattorr far reporting proper disposal at Hassitimia WastePrintedhypedNameFIg.iln3ture teaM Drr$__Z17TransporterAcknowledgementlRcaiptofMatetiats
Prlnlet P1jptd Name ..t Signature Mtk br
r7 1z7 O7l8.Transporter AcknowtadrnbnI of ReceIpt of Mateiisls
_____________PrInted/Typed Name
Signature j/_ii ______19 DIscrepancy Indication Space _______
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CMS Landfill
Please print or type
Form designed loruse on elite 12 plLcti typewriter
I-
At
ESP Associates PA
1i
Corporate Office
Mathng
POi3oi 7030
Cha lotte No ii Carolina 28241
Physical
3475 LakemoniBoulevawi
Fort Mill SC 29708
803 802 2440
Raleigh Wilmington concord
14001 Weston Pa kway 2120 capita/Drive 4601 CorporaleDrzveRWSuite100WilmingtonNmthCai a/inn 28405 Suite 16
caiy North Cam/inn 27513 910 313 6648 concord North carolina 2802791967810707047939855
8009607317
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