Item No 28 - Initial Abatement Action Report Incident 36326 -OCR

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$ESP
ESP Associates P.A
Dear Mr Schiff
On behalf of the property owner Beazer Homes ESP Associates P.A is pleased to provide the
attached Initial Abatement Action Report for the closure of the subject propertys petroleum
release ESP respectively requests classification of the release as Low Risk and issuance of no
further action notice
Thank you for your attention in this matter If you should have any questions please
do not
hesitate to contact me at 803 835-0915
Sincerely
ESP Associates P.A
-77
dgar Rogers
Staff Scientist
cc Jade Eastridge Beazer Homes
PG
Services ManagerNCLicenseNo1600
P.O Box 7030 Charlotte NC 28241
1.800.960.7317 NC 704.5834949 fax [phone] SC 803802.2440 fax [phone]
www.espassocjates.com
August 2007
NCDENR
UST Section
Mooresville Regional Office
919 North Main Street
Mooresville North Carolina 28115
Attention Mr Allen Schiff
Reference INITIAL ABATEMENT ACTION REPORT
Morehead Common Site Area No
919 West Morehead Street
Charlotte Mecklenburg County North Carolina
UST Incident No No Yet Assigned
ESP Project No E6-UD42.601
Initial Abatement Action Report
SITE INFORMATION
Site Identification
El Date of Report August 2007
El Facility ID NA
El UST Incident Number Not Yet Assigned
El Site Name Morehead Common Site Area No
El Site Street Address 919 West Morehead Street
El City/County/Zip Code Charlotte Mecklenburg County 28278
El Description of Geographical Data Point Approximate center of UST
El Location Method Mecklenburg County
Polaris GIS Map
Latitude 35.2276
El Longitude -80.8582
Information about Contacts Associated with the Leaking UST System
El UST Owner Beazer Homes
1300 Blvd Suite Charlotte NC 28203-4265
704.370.7200
El UST Operator N/A
El Property Owner Same as above
El Property Occupant Same as above
El Consultant/Contractor ESP Associates P.A Chris Ward PG
P0 Box 7030 Charlotte NC 28241
803.835.0915
El Analytical Laboratory Prism Laboratories Inc
P0 Box 240543 Charlotte NC 28224-0403
704.529.6364
NC Certification No 402
Information about Release
El Date Discovered June 19 2007
El Estimated Quantity of Release Unknown
El Cause of Release Unknown
Source of Release USTs
El Size and contents of UST
System from which release occurred 900-gal steel gasoline and 1500-gal diesel USTs
Lification
Chris Ward Professional Geologist for ESP Associates P.A do certify that the
on contained in this report is correct and accurate to the best of my knowledge
Associates P.A is licensed to practice both geology and engineering in North Carolina
Associates certification numbers are Geology C-347 and Engineering C-0587
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No August 2007
INTRODUCTION
The subject site has an address of 919 West Morehead Street in Charlotte Mecklenburg County
North Carolina see Figure Topographic Site Location Map The area of the subject release
associated with 900-gallon gasoline
and 1500-gallon diesel underground storage tanks USTs
uncovered on June 19 2007
has been designated by ESP as Area No of the Morehead
Common site
SITE HISTORY AND CHARACTERIZATION
On June 19 2007
ESP responded on behalf of Beazer Homes to an encounter with several USTs
and impacted soil during mass grading operations
at the subject site Upon arriving at the site
ESP observed 900-gallon steel apparent gasoline
UST and 1500-gallon steel apparent diesel
UST along with soils with petroleum odor located on the south side of West Morehead Street
approximately 150 feet west of its intersection with South Clarkson Street on Tax Parcel No
07325210 see Figures and As required following receipt of laboratory results confirming
release had occurred ESP emailed notification of the release discovery along
with Release
and UST Leak Reporting Form to Mr Steve Bograd of the Mooresville Regional Office of
NCDENR on June 19 2007
Release Location
The subject site former auto repair facility is located within an urban area of Charlotte which
historically included warehouse and commercial structures Site structures associated with the
former auto repair facility were razed sometime between 2002 and 2005 The site is currently
mass graded with no surface structures present Facility ID No was not available for the site
Based on our review of the Geologic Map of North Carolina 1985 the subject site is located
within the Charlotte Belt locally comprised of intrusive metamorphosed granitic rocks locally
Initial Abatement Action Report ESP Project E6-UD42 60
Morehead Common Site Area No August 2007
pinkish gray massive to weakly foliated and containing hornblende Soils encountered in this
area are the residual product of chemical weathering of rock presently underlying
the site Soil
weathering is more advanced near the surface grading with depth to less weathered rock and
finally bedrock
UST Information
Following the June 19 2007 discovery of 900-gallon gasoline
UST and 1500-gallon diesel
UST AD Environmental and Industrial Services AD of High Point North Carolina was
contacted to remove remaining product/sludge
from the tanks prior to their removal from the
excavation On June 19 2007
AD pumped less than 10 gallons of product/sludge from each
tank for permitted recycling
at their Archdale North Carolina facility see Product Material
Manifest in Appendix Once removed the tanks were transported by AD to the
Griffin recycling facility in Greensboro North Carolina on June 19 2007 see Tank Disposal
Manifest in Appendix See site photographs in Appendix
PreviousTankInstallationRemovalSizeTankLastTankTankNoDateDateGallonsDimensions Contents Contents
Unknown 6-19-07 900 ft ft Gasoline Unknown
Unknown 6-19-07 1500 ft 10 ft Diesel Unknown
completed UST-2 Form is included as Appendix Former locations of the above USTs are
depicted on Figure
Previous Reporting
ESP emailed release notification along with 24-Hour Release and UST Leak Reporting Form
to the Mooresville Regional Office of NCDENR on June 19 2007 see Appendix
Additionally ESP submitted 20-Day Report to NCDENR on July 18 2007
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No August 2007
INITIAL ABATEMENT ACTIVITIES
Initial Contaminated Soil Excavation
On June 19 and 20 2007 ESP documented the excavation of 278.78 tons of impacted soil from
Area No by the sites grading contractor Gelder Thompson of Midland North Carolina The
excavation was advanced based on results of OVA field screening and evidence of visible
staining The resulting excavation measured approximately 20 ft 21 ft ft deep The
excavated soil was placed on and covered with plastic awaiting subsequent off-site permitted
disposal Neither groundwater bedrock nor free product were encountered within the tank pit
See site photographs in Appendix
Initial Post-Excavation Confirmatory Sampling
On June 20 2007 confirmatory soil samples were collected at depth of feet BLS from each
of the excavations four sides WS-l through WS-4 while one sample was collected at depth
of feet BLS from the base of the excavation B-The sidewall samples were collected at the
foot depth due to the prevalence of elevated OVA readings at that depth The five soil samples
were hand delivered on ice to Prism Laboratories of Charlotte North Carolina to be analyzed for
risk-based parameters which include volatile organic compounds VOCs by EPA Method
8260B semi-volatile organic compounds SVOCs by EPA Method 8270C VPH/EPH by the
Massachusetts Department of Environmental Protection MADEP method and for total lead
and chromium by EPA Method 60 lOB Sample locations and excavation dimensions are
depicted on Figure Soil Sample Location Map Sampling was performed in general
accordance with ESPs SOP see Appendix
Results of the laboratory analysis
of confirmatory samples WS-through WS-4 and B-revealed
that all analyzed constituents were either below reporting limits BRLs or below the lowest of
the soil-to-groundwater or
residential MSCC with the exception of several SVOCs in wall
samples WS-2 and Cl 1-C22 Aromatics in WS-3 while chromium was detected at
concentration of 120 mg/Kg in base sample B-i Laboratory analytical results for the
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No August 2007
confirmatory soil samples are summarized on Table B-i The Prism laboratory data report is
included as Appendix
Follow-up Contaminated Soil Excavation and Confirmatory Sampling
Due to the detection of elevated constituents above applicable standards in confirmatory samples
WS-2 WS-3 and B-i an additional two feet of soil was excavated from the southern and eastern
walls and from the base of the excavation on July 2007 Excavated soil was placed on the
previous soil stockpile for subsequent off-site permitted disposal
The resulting excavation
measured approximately 22 ft 23 ft 10 ft deep See Figure for depiction of the
excavation limits and sample locations
On July 2007 following excavation of additional soil ESP collected confirmatory soil
samples WS-2 and WS-3 at depth of feet BLS from the southern and eastern walls of the
excavation and B-i at depth of 10 feet from the base of the excavation Samples WS..2 and
WS-3 were submitted to Prism for analysis of SVOCs by EPA Method 8270C WS-3 for EPH by
the MADEP Method and B-i for total chromium by EPA Method 60 lOB Results of the analysis
of the July 2007 confirmatory sampling revealed that all analyzed organic
constituents were
BRLs while chromium was detected below the soil-to-groundwater MSCC see Table B-i The
Prism laboratory data report is included as Appendix
Stockpile Sampling and Soil Disposal
On June 20 2007 ESP collected two composite stockpile soil samples for laboratory analysis
The stockpile soil samples designated 1A and lB were placed in laboratory provided containers
labeled and hand delivered on ice to Prism for compositing and subsequent analysis The
samples were analyzed for TPH-GROIDRO by EPA Method 5030/3550 and for BTEX by EPA
Method 8260B The composite samples were collected and analyzed to confirm that release
had occurred and to characterize contaminant types and concentrations for subsequent off-site
permitted disposal/treatment
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No August 2007
As revealed by the laboratory analysis
of stockpile composite samples 1A and 1B TPH-DRO
was reported at concentrations of 400 and 76 mg/Kg respectively while results for the
remainder of organic analytes
were BRLs Total lead was reported at concentration of 15
mg/Kg 1A and 13 mg/Kg 1B Results of the stockpile sample analyses are summarized on
Table B-2 while the laboratory data report is included as Appendix
On July 27 2007 total of 278.78 tons of stockpiled soil from the Area excavation was
transported by Gelder Thompson to the CMS Landfill in Concord North Carolina for permitted
disposal see Non-Hazardous Waste Manifest in Appendix
RECEPTOR SURVEY
On July 20 2007 Mr Eddie Rogers of ESP performed receptor survey
to document the
presence or absence of active and/or inactive water supply wells within 1500-foot radius of the
subject UST release see Figure Receptor Survey Map The receptor survey
included
interviews with available site occupants and visual observations for water supply wells and/or
municipal water meters All properties within 500 feet of the site were visited to determine well
status The area within 1000 feet of the subject release consists of commercial and industrial
development with numerous vacant structures No active or inactive water supply wells were
identified within 1000-foot radius of the subject release Municipal water and sewer have
historically been available within the area of the site Additionally no surface water bodies were
identified within 500 feet of the release see Figure
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No August 2007
CONCLUSIONS AND RECOMMENDATIONS
The following conclusions have been formulated based on our completion of field activities
including abatement activities receptor survey and our review of laboratory data from the
analysis of collected soil samples
The subject site razed former auto repair facility has an address of 919 West
Morehead Street in Charlotte Mecklenburg County North Carolina
On June 19 2007
ESP responded on behalf of Beazer Homes to an encounter with
900-gallon steel apparent gasoline
UST and 1500-gallon steel apparent diesel UST
along with soils with petroleum odor during excavations conducted ahead of mass
grading operations
at the subject site
On June 19 and 20 2007 ESP documented the excavation of 278.78 tons of impacted
soils from the release area The resulting excavation measured approximately 20 ft 21
ft ft deep
Neither groundwater bedrock nor free product were encountered within the tank pit
rJ On June 20 2007 confirmatory soil samples were collected at depth of feet BLS
from each of the excavations four sides WS-i through WS-4 while one sample was
collected at depth of feet BLS from the base of the excavation B-i
Results of the laboratory analysis
of confirmatory samples WS-i through WS-4 and B-i
revealed that all analyzed constituents were either below reporting limits BRLs or
below the lowest of the soil-to-groundwater or residential MSCC with the exception of
several SVOCs in wall samples WS-2 and Cl i-C22 Aromatics in WS-3 while chromium
was detected at concentration of 120 mg/Kg in base sample B-i
Due to the detection of elevated constituents above applicable standards in confirmatory
samples WS-2 WS-3 and B-i an additional two feet of soil was excavated from the
southern and eastern walls and from the base of the excavation on July 2007 The
resulting excavation measured approximately 22 ft 23 ft 10 ft deep
ri On July 2007 following excavation of additional soil ESP collected confirmatory soil
samples WS-2 and WS-3 at depth of feet BLS from the southern and eastern walls of
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No August 2007
the excavation and B-i at depth of 10 feet from the base of the excavation Samples
WS-2 and WS-3 were submitted to Prism for analysis of SVOCs by EPA Method 8270C
WS-3 for EPH by the MADEP Method and B-i for total chromium by EPA Method
6010B
Results of the analysis of the July 2007 confirmatory sampling revealed that all
analyzed organic
constituents were BRLs while chromium was detected below the soil-
to-groundwater MSCC
On June 20 2007 ESP collected two composite stockpile soil samples designated 1A
and for laboratory analysis
The composite samples were collected and analyzed to
confirm that release had occurred and to characterize contaminant types and
concentrations for subsequent off-site permitted disposal/treatment
As revealed by the laboratory analysis of stockpile composite samples 1A and 1B TPH
DRO was reported at concentrations of 400 and 76 mg/Kg respectively while results for
the remainder of organic analytes
were BRLs Total lead was reported at concentration
of 15 mg/Kg 1A and 13 mg/Kg 1B
On July 27 2007 total of 278.78 tons of stockpiled soil from the excavation was
transported to the CMS Landfill in Concord North Carolina for permitted disposal
Municipal water and sewer are available in the area of the release
No water supply wells were identified within 1000 feet of the release and
No surface water bodies were identified within 500 feet of the subject release
Based on the absence of analyzed risk-based parameters above the lowest of the North Carolina
soil-to-groundwater or residential MSCCs lack of either groundwater bedrock or free product
within the tank pit the documented absence of water supply wells within 1000 feet of the
release and the absence of surface water feature within 500 feet of the release ESP
recommends that NCDENR issue no further action notice for the subject release
Attachments
Table B-i Summary of Soil Sampling Results
Table B-2 Summary of Stockpile Soil Sampling Results
Figure Topographic Site Location Map
Figure 2005 Aerial Photograph
Figure Soil Sample Location Map
Figure Receptor Survey Map
Appendix 24-Hour Release Notification
Appendix UST-2 Form
Appendix Tank Disposal Manifest
Appendix Product Material Manifest
Appendix Site Photographs
Appendix ESPs SOP
Appendix Prism Laboratory Data Reports
Appendix Non-Hazardous Waste Manifests
ATTACHMENTS
TABLES
Table B-i
Date 7/16/07 Incident No Not Yet Assigned
Anaiftical Method
Contaminant of onceTrn
Sample Date Source amp1e Incident
ID Collected Area Depth Phase
rnJdd/yy ft I3GS
Summary of Soil Sampling Results
Carolina
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNIL Not Listed
Table B-i Summary of Soil Sampling Results
Date 7/16/07 Incident No Not Assigned ______Morehead Common Area No Charlotte North Carolina
AnatyticaFMthod
Contamin ant of Concern
Sample Date Source aile Icitent
ID collected Area Depth Phase
m/dd/yy ft._BGS ______
WS-l 6/0/07 North Pit Initial
Wall Abatement
6010B 6010B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B
.0 In .0
/1
.0
37 9.0 0.0055 0.0055 0.011 0.11 0.0055 0.0055 0.0055 0.0055
WS-2 6/20/07 West Pit
Wall
Initial
Abatement 29 84 0.0055 0.0055 0.011 0.10 0.0055 0.0055 0.0055 0.0055
WS-2 7/5/07 West Pit
Wall
Initial
Abatement NA NA NA NA NA NA NA NA NA NA
WS-3 6/20/07 South Pit
Wall
Initial
Abatement 29 7.5 0.0053 0.0053 0.011 0.0053 0.0053 0.0053 0.0053 0.0053
WS-3 7/5/07 South Pit
Wall
Initial
Abatement NA NA NA NA NA NA NA NA NA NA
WS-4 6/20/07 East Pit
Wall
Initial
Abatement 14 8.2 0.0054 0.0054 0.011 0.063 0.0054 0.0054 0.0054 0.0054
B-i 6/20/07 PitFloor Initial
Abatement 120 12 0.0053 0.0053 0.011 0.0053 0.0053 0.0053 0.0053 0.0053
Initial
Abatement 26 NA NA NA NA NA NA NA NA NA
27 270 2.2 1.7 0.58 3.3 4.3
47 400 3128 626 313 1564 626 626 782 782
LL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNL Not Listed
1226 400 81760 16350 8176 40880 16350 16350 20440 20440
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnaiyzedNL Not Listed
Table B-i Summary of Soil Sampling Results
Dale 7/16/07 Incident No Not Yet Assigned Morehead_Common Area No Charlotte North_Carolina
Ana1yticdtjtetIod
ontaininantof ojfŁern
Sample Date urce Sample Iirciden
ID Collected Area Depth Phase
m/dd/yy ft._BGS _____ ________________________
6P0107 North Pit Initial
Wall Abatement
8260B 8260B 8260B 8260B 8270C 8270C 8270C 8270C 8270C 8270C
baa
aa COaZ
0.011 0.0055 0.0055 0.0055 0.40 0.40 0.40 0.40 040 0.40
WS-2 6/20/07 West Pit
Wall
Initial
Abatement 0.011 0.0055 0.0055 0.0055 0.68 0.57 1.1 0.96 0.90 1.1
WS-2 7/5/07 West Pit
Wall
Initial
Abatement NA NA NA NA 0.35 0.35 0.35 0.35 0.35 0.35
WS-3 6/20/07 South Pit
Wall
Initial
Abatement 0.011 0.0053 0.0053 0.0053 0.14J 0.12J 0.25 0.40 0.40 0.40
WS-3 7/5/07 South Pit
Wall
Initial
Abatement NA NA NA NA 0.35 0.35 0.35 0.35 0.35 0.35
WS-4 6/20/07 East Pit
Wall
Initial
Abatement 0.011 0.0054 0.0054 0.0054 0.39 0.39 0.39 0.39 0.39 0.39
B-i 6/20/07 PitFloor Initial
Abatement 0.011 0.0053 0.0053 0.0053 0.39 0.39 0.39 0.39 0.39 0.39
Initial
Abatement NA NA NA NA NA NA NA NA NA NA
BRL Below Reporting Limit
4.6 0.0056 38 0.34 0.091 1.2 6700 12
3129 3200 1560
18 88 0.88 0.0088 0.88 469
81760 82000 40000
164 780 0.78 12264 78
Table B-i
Date 7/16/07 Incident No Not Yet Assigned
Analytical Method
contaminaneof onern
Sample Date Surce Sample Incident
ID Collected Area Depth Phase
m/dd/yy ft BGS
WS-1 61007 North Pit Initial
VaI1 Abatement
Summary of Soil Sampling Results
Morehead Common Area No Charlotte North Carolina
8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C
.C
NC
6_
ii.i
I-
r-l
v0
0.40 0.40 0.40 0.40 0.40 0.40 0.40 0.40 0.40 0.40
WS-2 6/20/07 West Pt
Wall
Initial
Abatement 0.98 2.5 0.41 0.41 0.41 0.41 0.41 0.41 1.5 0.96
WS-2 7/5/07 West Pit
Wall
Initial
Abatement 0.35 0.16J 0.35 0.35 0.35 0.35 0.35 0.35 0.14J 0.35
WS-3 6/20/07 South Pit
Wall
Initial
Abatement 0.40 0.42 0.40 0.40 0.40 0.40 0.40 0.40 0.24J 0.40
WS-3 7/5/07 South Pit
Wall
Initial
Abatement 0.11J 0.22J 0.35 0.35 0.35 0.35 0.35 0.35 0.20J 0.35
WS-4 6/20/07 East Pit
Wall
Initial
Abatement 0.39 0.39 0.39 0.39 0.39 0.39 0.39 0.39 0.39 0.39
B-i 6/20/07 Pit Floor Initial
Abatement 0.39 0.39 0.39 0.39 0.39 0.39 0.39 0.39 0.39 0.39
B-i InitialPitFloor10Abatement NA NA NA NA NA NA NA NA NA NA
60 290 44 1.7 ii
BRL Below Reporting Limit
1000 0.17 4.7 280 3.3
469 469 620 63 469 4600 0.088 62 620 0.88
12264 12264 16400 1635 12264 122000
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNL Not Listed
0.78 1635 16400
8015B 8260B 8260B 8260B 8260B 6010B
1.1
Cl
0.0034 0.0057
1.1
0.0057
Table B-2 Summary of Stockpile Soil Sampling Results
Dale 7/6/07 Incident No Not Assigned Morehead Common Area No Charlotte North Carolina
AnalyTicafMethd 8015B
Contaminanl oncern
__________________________________________
Sample Date Source Sample Incident
1D Collected Area Depth Phase
m/dd/yy cft BGS
Stock-Initial1A6/20/07 jIe coflipoSite 370Abatement
Stock-injtiailB6/20/07 lIe CompoSite 140Abatement
Soil to Groundwater MSCC mg/kg NL
Residential MSCC mg/kg
IndustrialIommercial MSCC mg/kg
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg unless otherwise noted
Health based level 100%
Considered immobileNANotAnalyzedNL Not Listed
0.0034
0.0 11
0.0057
15
NL
0.0057
0.0056
0.0 11
7.3
13
4.6
NL NL 18 3200 1560 3129
400
270
NL NL 164 82000 40000 81760 400
FIGURES
RQECT NO SHEET TITLE FiGUREUD4260
2005 AERIAL PHOTOGRAPH fl EP
ATE 7/11/07MH PROJECT MOREHEAD COMMON Mu
CJW CHARLOTTE NORTH CAROLINA
LEGEND
CONRRMA TORY SOIL SAMPLE LOCA liON
AREA EXCA VA 770N DEPTH OF 10 FEET
AREA EXCA VA liON DEPTH OF 10 FEET
WEST MOREHEAD STREET
FiGURE
SOIL SAMPLE LOCA liON MAP AREAS AND
MOREHEAD COMMON ShE
CEARLOTTE NORTH CAROLINA
ws-1 ////__
AREA
WS-4 WS-2
WS-3
ws-i
WS-4 WS-2
WS-3
AREA
20
APPROXIMA iF SCALEINFEET
MOREHEAD COMMON ShE
CHARLOTTE NORTH CAROLINA
1000
$ESP
APPENDIX
24-HOUR RELEASE NOTIFICATION
Page of2
Chris Ward
From Chris Ward
Sent Tuesday June 19 2007 354 PM
To SteveBogradncmail.net
Cc Jade Eastridge [e-mail] [e-mail] Scott Jones [e-mail]
Subject 24-Hour Notice Morehead Common Releases and
Attachments AREA 24-Hr Notification.pdf AREA 24-Hr Notification.pdf
Steve
On behalf of Beazer Homes am herein providing 24-Hour Notification of the discovery of three orphan USTs on
Beazer Homes Morehead Common residential/commercial development currently being graded The Morehead
Commons property is located on the south side of West Morehead Street at its intersection with South Clarkson
Street in Charlotte North Carolina On June 18 2007 during grading operations
an approximate 550-gallon steel
UST was uncovered on Parcel No 07325210 The UST was uncovered and determined to be partially filled with
sludge and some fluid with diesel odor this UST is being referred to as AREA An additional approximate
550-gallon likely diesel and an approximate 750-gallon likely gasoline were subsequently encountered side by
side approximately 25 feet from the first 550-gallon UST encountered on Parcel No 07325210 these USTs are
being referred to as AREA
On June 19 2007 Ab Environmental and Industrial Services pumped remaining fluid and sludge from the USTs
and transported the USTs off-site for permitted disposal The tops of the LiSTs were buried to depth of
approximately feet below original grade and were severely rusted with numerous holes Soils adjacent to and
beneath all three LiSTs exhibited strong petroleum
odor and were visibly stained Excavation of soils adjacent to
and beneath the three USTs was initiated on June 19 with soils being stockpiled on site on plastic for subsequent
off-site disposal
Preliminary investigation
reveals that Parcel No 07325210 was once occupied by Tonys Auto Body Shop and
Shorts Imports The releases are identified on the attached PbF map included with the 24-Hr Notification
Forms
The Responsible Party for the property is
Beazer Homes
1300 South Boulevard
Suite
Charlotte North Carolina 28203-4265
Mr Jade Eastridge
704.370.7200
Please call with any questions
Thanks
Chris Ward PG
Environmental Services Manager
ESP Associates
803835.0915 direct office
803.802.2515 fax
/-1rV
UST61 24i4oair eease id UST Leak ReportO Form
For Releases This form should be completed and submitted to the UST Sections regIonal cube following known or suspected release from
an underground storage tank UST system This Iorrn is required to be submitted within 24 hours of discovery of known orNCsuspectedrelease
pWM USE ONLY Suspected Conthmlnation WIN Eaclity ID Number N/A
Incident RiskHIL Confirmed GW Contamination YiN Ai Date Leak Discovered l4iReceivedOnReceivedConfirmedSoilContaminationY/N CommlNon-Commerclat 1.Ih4tVt
Reported by circle one Phone Fax or Report Free Product YIN If Yes State Greatest Reg/Non.regulated
Region Thickness
INCIDENT DESCRIPTION
Incident Name
Address 1AJ-MLlLt 4k County
Cltylrown Zip Code ReionaI Ollice circle one AsheviIKvifleayettevilleRaleighWashingtonWilmingtonWinsto
Latitude cn degrees 3d7 p773 Longitude neldegrses Obtained by
Briefly describe suspected or confirmed release including but not limited to nature of release dale of release amount GPSofreleaseamountoffreeproduct present
and recovery efforts initia responses conducted impacts to receptors
13 Topographlcmap
G1S Address matching
Otheri--
Unknownbej6pi4pDescribelocation
Ai-e JI
HOW RELEASE WAS DISCOVERED
Check one
During UST Ctasure/Rernoval tJ Water in Tank Surfce Water Contamination
Ii Release Detection Equipment or Methods VisuallOdor Groundwater Contamination
Property Transfer Water Supply Well Contamination ther specify rLSOURCEOFCONTAMINATION
Primary Source of Contamination Primary Contaminant Type Location Settin
Check one heck one Check Ones
GasolinelDlesel/Korosene Facirity ResidentialConfirmedUSTReleaseCheckonebelowHeatingonCIResidence13Industrial
Dispenser Other Petroleum Products Other JJibanLineRelease13MotelsRural_C Tank Release Other Inorganlos
Spill/Overfill Other Organlcs13ExactFailureLocationUnknownor
Muitiple Failures
Qhi
MunIcipal MIlitary Unknown Federal County Slate
Operation Type
PuhllcService Agricultural EducationlRelig Iridustilal 6erciaI Mining
UST Form bi 11IU Page
IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected Yes No no
Number of Water Supply WeflsAfiected _________________
Water Supply Wells Contaminated Include Users Names Addresses and Phone Numbers Attach additional sheet if necessaly
UST SYSTEM OWNER
IJST Owner/CompanyPiofContac AddressJeJ4r4 ifrh TL
City State Zip Code Telephone NumberLioto//cz
UST SYSTEM OPERATOR
iisr Opemtor/Company Address
State Zip Code Telephone Number
LANDOWNER AT LOCATIO OF UST INCIDENT
Draw Sketch of Area showing two major road intersections or Attach Map
ry/1-c tj /i44L/
Person Reporting Incident fl/AJ Company pª./
l11L Address QJdfçM c432-1%Date
UST Form 6111/05
Page of
Landowner
qi4t-4S
City state
Address
Zip Code Telephone Number
Telephone M1mbei t_ç-5--ti
r.
P..
cI2 SHEET 71111 AREAS Na AND tSPAucIa1PANTS2005ShEMAPATE
MlI.5CZI718oflAflrDMHPROJECTMOREIIEADCOMMONSShE
CHARLOTTE NORTH CAROLINA
APPENDIX
UST-2 FORM
Return completed form to
The DWM Regional Office located in the area where the facility is located Send copy to the Central Office in Raleigh so that ID
the status of the tank may be changed to PERMANENTLY CLOSED and your tank fee account can be
closed out
SEE MAP ON THE BACK OF TH FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES Date Recived__________
Permanent closure For permanent closure complete all sections of this form
Change-in-service For change-in-service where UST systems will be converted from containing regulated
substance to storing non-regulated
substance complete sections II Ill IV and VIII
Effective February 1995 all UST closure/change-in-service reports must be submitted in the format provided in the UST-12 form UST closure and
change-in-services must be completed in accordance with the latest version of the Guidelines for Tank Closure copy of the UST-12 form and the
Guidelines for Tank Closure can be obtained at www.wastenotnc.org
You must make sure that USTs removed from your property are disposed
of properly When choosing closure contractor ask where the tanks will be
taken for disposal Usually USTs are cleaned and cut up for scrap metal This is dangerous work and must be performed by qualified company Tanks
disposed of illegally in fields or other dumpsites can leak petroleum products
and sludge into the environment If your tanks are disposed of improperly youcouldbeheldresponsibleforthecleanupofanyenvironmentaldamagethatoccurs
NOTE If release from the tanks has occurred the site assessment portion of the tank closure must be conducted under the supervision of P.E orL.G with all closure site assessment reports bearing the signature and seal of the P.E or L.G
QWNERSHIP OFTANKS IL LOCATIONOFTANKS
Owner Name Corporation Individual Public Agency or Other Entity Facility Name or CompanyBeazerHomesNA
Street Address Facility ID If known
1300 Boulevard Suite NA
City County Street Address
Charlotte Mecklenburg 919 West Morehead Street
State Zip Code City County Zip CodeNC28203-4265 Charlotte Mecklenburg 28278
Phone Number Phone Number704-370-7200
III CONTACT PERSONNEL
Contact for Facility Job Title Phone No
N/A
Closure Contractor Name Closure Contractor Company Address Phone No
Jim Strattford Gelder Thompson P0 Box 288 Midland NC 28107 704-269-0070
Primary Consultant Name Primary Consultant Company Address Phone No
Chris Ward PG ESP associates P.A P0 Box 7030 Charlotte NC 28241 704-802-2440
IV UST INFORMATION FOR REGISTERED liST SYSTEMS EXCAVATION CONDITION
Tank Size in Tank Last Last Use Permanent Change-in-Water in Free Notable odor or visible
ID No Gallons Dimensions Contents Date Close Date Service Ye2t0flNo Yea
product
No
sod con-rninahon
Date LIE LI LI
LI LI LI LI LI
LI LI LI LI LI LI
LI LI LI LI LI LI
LI LI LI LI LI LIVLUSTINFORMATIONFORUNREGISTEREDliSTSYSTEMSVIIEXCAVATIONCONDITION
Tank Size in Tank Last Last Use Permanent Tank Owner
Waterin Free Notableodororvjsible
ID No Gallons Dimensions Contents Date Close Date Name excavation product soil contamination
Yes No Yes No Yes No
900 ft.x ft._-Gasoline NA 6/19/07 LI LI LI
1500 ft 10
ft._-Dielsel Dielt NA 6/19/07 LI LI LI
LI LI LI LI LI LI
LI LI LI LI LI LI
LI LI LI LI LI LI
If the tank owner address is different from the one listed in Section then enter the street address city state zip code and telephone no below
VIII CERTIFICATION
certify under penalty of law that have personally examined and am familiar with the information submitted in this and all attached documents and thatbasedonmyinquiryofthoseindividualsimmediately responsible
for obtaining the information .beIieve that the itted information is true accurate andcomplete
Print name and official title of owner or owners authorized representative
Christopher Ward PU Department Manager ESP Associates P.A
UST-2 Rev 11/2006
UST2 Site Investigation Report for Permanent Closure or Change-in-Service of UST
INSTRUCTIONS READ THIS FIST
For more than five UST systems you may attach additional forms as needed
STATE USE ONLY
Date Signed
8/8/2007
APPENDIX
TANK DISPOSAL MANIFEST
Environmental and Industrial Services
P.O Box 484 High Point NC Phone [phone] FAX [phone]
TANK DISPOSAL MANIFEST
Tank Owner/Authorized Representative Name and Mailing Address ____________________________________
Pc 6ii
Tank Owner/Authorized Representative Contact
Phone
Description Of Tanks
Tank No Capacity Previous Contents Comments
20
111/PTh/Lt SP
Tank Owner/Authorized Representative Certification The undersigned certifies that the above listed storagetankshavebeenremovedfromthepremisesofthetankowner
Printed/Typed Name Signature Month/Day/Year
Transporter The undersigned certifies that the above listed storage tanks have been transported to ADEnvironmentalandIndustrialServices2718UwharrieRoadArchdaleN.C 27263
4t M9
Printed/Typed IVame inazur Mont hiD ayIYar
Disposal Certification The undersigned certifies that the above-named storage tanks have been cut
into scrap pieces
and accepted by the metal recycling facility
Recycling Facility
Month/Day/Year
APPENDIX
PRODUCT MATERIAL MANIFEST
_\MATERIAL Environmental and
MANIFEST Industrial Services Inc
EMERGENCY PHONE NO POST OFFICE BOX 484
800 434 7750
HIGH POINT NC 27261
çT..MailiflgAddreSS
YflbPcih/dk __________
DESCRIPTIONOFMATERIALS _________
...USDOtPoper Shipping Name Hazard UN NA Packing Containers Total Unit
HM Complete All Items for Hazardous Materials Class or Div ID No Group Type Quantity Wt Vol
Ar lit //N11
ADDITIONAL INFORMATION ERG No äcIàItpUtdt.
.--........
GENERATORS .CERTIF.CAT1ON ....c.......
This is to certify that the above-descnbed materials are properly classified described packaged marked and labeled and are in
proper condition for transportation according to the applicable regulations
of the Department of Transportation further certify
that none of the materials descnbed above are hazardous waste as defined by EPA 40 CFR Part 261 or any applicable state law
and unless specifically identified above the materials contain less than 1000 ppm total halogens and do not contain quantifiable
levels ppm ófPCBs as defined by EPA 40 CFR Parts 279 and 761
Printed Typed Name -...Signature
Transporter ..ENV1RON1ENTAL AND INI$USThIAL SERVICES
Address
2718UWHARRIERO
ARCHDALE NC 27263
Transporter or Unit No
EPA ID NCq98623222
Phone [phone]
FACILITU\
Facility
ENVIRONMENTAL AND INDUSTRIAL SERVICES
Address
2718 UWHARRIE ROAD
ARCHDAI NC 27263
Facility or
NcD986232221EPAIDNo
Phone [phone]
Contact ERIC McMANUS
hereby acknowledge receipt or the above-described materials or transport
from the genera for site listed above
1/1 ii
Signature 14 44 Shipment Date
hereby acknovThdge that the above described materials were received
from the generatorslteand were transported to the facility listed below
Signature eIiiDa
AO1OI5
Manifest Document No
Page Of
AD Job No
$.fl
TEL[phone]
FAX [phone]
Narne--...
Lr if -.
US...EPA ID Ni
Phone-No --1bq-4-3ld-l
Contact
Mo lDay /Yr
-j.--b fIJI
thereby acknowlede recipt of he materials covered by this manifest
except for any dlscrepancy
noted below
-i
Signature 1T Receipt Date
APPENDIX
SITE PHOTOGRAPHS
APPENDIX
ESPS SOP
STANbARb OPERATING PROCEbURE
SOP-6
SOIL SAMPLE COLLECTION
ESP Associates P.A Revision bate 3/7/06
This standard operating procedure SOP covers the collection of soil sample for
laboratory analysis
Follow these steps when collecting the soil sample unless
otherwise instructed by the project manager
Gather needed field supplies noted below
Confirm lab cooler contains needed sample containers fill cooler with
ice
Upon arriving at site check in with the property owner or company
representative
becontaminate the stainless steel hand auger before and between sample
collection by washing with Alconox soap and scrub brush rinsing with
distilled water and spraying with Isopropyl alcohol Wrap clean sampler
in aluminum foil
Wear disposal latex or nitrile gloves and change into new pair between
samples
buring advancement of the hand auger collect soil samples at regular
intervals for describing lithology Note lithology and other
characteristics of soils in field book relative to depth
If appropriate place representative portion of soil sample into
resealable plastic bag label with boring number and depth interval and
allow to equilibrate Screen soil in bag for volatile organics using an OVA
or Hnu Enter results into field book
Advance hand auger boring to previously specified sampling depth
Collect soil sample from this depth and place in laboratory provided
containers Label containers with boring number and sample depth using
the following sampling scheme i.e B-I ft B-i 10 ft B-2 ft etc
benote boring location in field book relevant to pertinent site features
10 Following collection of the soil samples abandon all boreholes feet or
greater in depth with cement grout
ii Complete and sign the labs chain-of-custody
12 Keep the sample cooler in secure location until delivered under normal
chain-of-custody procedures to laboratory
SOP-6 Soil Satnpk Collection Revision bate 3/7/06
ESP Associates Page of
SUPPLIES
SOP-6
Stainless steel hand auger with needed extensions or sampling
spoon
OVA or Hnu
Measuring tape
Plastic zip-lock bags
Isopropyl alcohol
bistilled water
5-gallon wash bucket scrub brush and Alconox soap
Cement with wheel barrow for mixing
Cooler with sample containers and chain-of-custody
Ice
Permanent marker
bisposable gloves
Knife
Field book
Site plan with site specific sampling instructions
Camera
APPENDIX
PRISM LABORATORY DATA REPORTS
REcQJU iWO
Case NarrativePRISM
LABORATORIES INC
Date 06/29/07 Client Project ID Morehead Commons No
Company ESP Associates PA Prism COC Group No G0607589
Contact Chris Ward Collection Dates 06/20/07
Address Box 7030 Lab Submittal Dates 06/20/07
Charlotte NC 28241
This data package contains the analytical results for the project identified above and includes Case Narrative Laboratory Report and Quality
Control Data totaling 44 pages chain-of-custody is also attached for the samples submitted to Prism for this project
Data qualifiers are flagged individually on each sample key
reference for the data qualifiers appears at the end of this case narrative Quality
control statements and/or sample specific remarks are included in the sample comments section of the laboratory report for each sample
affected
Semi Volatile Analysis
No Anomalies Reported
Volatile Analysis
Analysis note for 024604 MSD C9-C1 Aliphatics Recovery above the control limits
Metals Analysis
Analysis Note for Q24537 Method Blank Lead MB RL of 1.0mg/kg reported for associated samples
Analysis Note for Q24537 MS Chromium Matrix interference is suspected MS recovery outside of the control limits Post-
digestion spike recovery 72%is outside the acceptance limits 75-125%
Analysis Note for 024537 MS Lead MS recovery outside of the control limits Post-digestion spike recovery 80%is within the
acceptance limits 75-125%
Analysis Note for 024537 MSD Chromium Matrix interference is suspected
Analysis Note for 024537 MSD Lead Matrix interference is suspected
Wet Lab and Micro Analysis
N/A
Please call if you have any questions relating to this analyilcal report
Date Reviewed by Paula Gilleland Project Manager Angela ash
Signature 4k4 Signature _______________________
Review Date O6/29/07 Approval Date
Data Qualifiers Key Reference
Compound also detected in the method blank
Result outside of the QC limits
DO Compound diluted out
Estimated concentration calibration range exceeded
The analyte was positively identified but the value is estimated below the reporting limit
Estimated concentration with high bias
Estimated concentration with low bias
matrix effect is present
06/29/07
Notes This report should not be reproduced except in its entirety without the writtten consent of Prism Laboratories Inc The results in this
report relate only to the samples submitted for analysis
449 Springbrook Road P.O Box 240543 chaone NC 28224-0403
Phone [phone] Toll Free 800/529-6364 Fax [phone]
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
Laboratory Report
06/29/07
Ws-1
185081
G0607589
06/20/07
06/20/07
Percent Solids Determination
Percent Solids
Result Units Report MDL
Sample Weight Determination
Weight Bisulfate
Weight Bisulfate
Weight Methanol
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter
1330
1635
Limit Factor
Dilution Method
81.9
Analysis
Date/Time
Analyst Batch
ID
SM2540 06/25/07 1745 Lthao
5.98
5.52
4.93
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Volatile Organic Compounds by GC/MS
11 1-Trichloroethane
11 22-Tetrachloroethane
11 2-Trichloroethane
11 -Dichloroethane
1-Dichloroethene
1-Dichloropropene
23-Trichlorobenzene
23-Trichloropropane
24-Trichlorobenzene
24-Trimethylbenzene
2-Dibromoethane EDB
2-Dichlorobenzene
2-Dichtoroethane
2-Dichloropropane
35-Trimethylbenzene
3-Dichlorobenzene
3-Dichloropropane
4-Dichlorobenzene
22-Dichioropropane
2-Chlorotoluene
5035
5035
5035
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
0.0055 0.00031
0.0055 0.00056
0.0055 0.00034
0.0055 0.0004
0.0055 0.00042
0.0055 0.00049
0.0055 0.00061
0.0055 0.00049
0.0055 0.00053
0.0055 0.00042
0.0055 0.0001
0.0055 0.0003
0.0055 0.00055
0.0055 0.00041
0.0055 0.00046
0.0055 0.00048
0.0055 0.00038
0.0055 0.00043
0.0055 0.00028
0.0055 0.00041
06/27/07 000 brown
06/27/07 000 brown
06/27/07 000 brown
06/27/07 148 erussell Q24552
06/27/07 148 erussell 024552
06/27/07 148 erussell Q24552
06/27/07 148 erussell Q24552
06/27/07 148 erussell 024552
06/27/07 148 ensseIl 024552
06/27/07 148 erussell Q24552
06/27/07 148 erussell 024552
06/27/07 148 erussell Q24552
06/27/07 148 erussell Q24552
06/27/07 148 erussell 024552
06/27/07 148 erussell Q24552
06/27/07 148 erussell Q24552
06/27/07 148 erussell 024552
06/27/07 148 erussell Q24552
06/27/07 148 erussell 024552
06/27/07 148 erussell 024552
06/27/07 148 erussell 024552
06/27/07 148 erussell 024552
06/27/07 148 erussell 024552
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of 35
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
Laboratory Report
06/29/07
WS-1
185081
G0607589
06/20/07
06/20/07
NC Certification No 402
ISM Sc Certification No 99012
NC Drinking Water Cert No 37735
luiI Service Analytical Environmental Solutions
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1330
1635
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
2-Hexanone BRL mg/kg 0.055 0.00058 8260B 06/27/07 148 erussell Q24552
4-Chlorotoluene BRL mg/kg 0.0055 0.00029 8260B 06/27/07 148 erussell Q24552
4-Methyl-2-pentanone MIBK BRL mg/kg 0.055 0.00055 8260B 06/27/07 148 erussell Q24552
Acetone 0.11 mg/kg 0.055 0.0022 8260B 06/27/07 148 erussell Q24552
Benzene BRL mg/kg 0.0033 0.00044 8260B 06/27/07 148 erussell 024552
Bromobenzene BRL mg/kg 0.0055 0.00039 8260B 06/27/07 148 erussell Q24552
Bromochloromethane BRL mg/kg 0.0055 0.00033 8260B 06/27/07 148 erussell 024552
Bromodichloromethane BRL mg/kg 0.0055 0.00049 8260B 06/27/07 148 erussell Q24552
Bromoform BRL mg/kg 0.0055 0.00041 8260B 06/27/07 148 erussell Q24552
Bromomethane BRL mg/kg 0.011 0.00064 8260B 06/27/07 148 erussell Q24552
Carbon tetrachloride BRL mg/kg 0.0055 0.00032 8260B 06/27/07 148 erussell 024552
Chlorobenzene BRL mg/kg 0.0055 0.00042 8260 06/27/07 148 erussell Q24552
Chlorodibromomethane BRL mg/kg 0.0055 0.00038 8260B 06/27/07 148 erussell Q24552
Chioroethane BRL mg/kg 0.011 0.00045 8260B 06/27/07 148 erussell 024552
Chloroform BRL mg/kg 0.0055 0.00041 8260B 06/27/07 148 erussell 024552
Chloromethane BRL mg/kg 0.0055 0.00039 8260B 06/27/07 148 ewssell 024552
cis-1 2-Dichloroethene BRL mg/kg 0.0055 0.00024 8260B 06/27/07 148 erussell Q24552
cis-13-Dichloropropene BRL mg/kg 0.0055 0.00035 8260B 06/27/07 148 erussell 024552
Dichlorodifluoromethane BRL mg/kg 0.0055 0.0012 8260B 06/27/07 148 erussell 024552
Ethylbenzene BRL mg/kg 0.0055 0.00039 8260B 06/27/07 148 erussell 024552
lsopropyl ether IPE BRL mg/kg 0.0055 0.00019 8260B 06/27/07 148 erussell 024552
lsopropylbenzene BRL mg/kg 0.0055 0.00044 8260B 06/27/07 148 erussell 024552
mp-Xylenes BRL mg/kg 0.011 0.00077 8260B 06/27/07 148 erussell 024552
Methyl ethyl ketone MEK BRL mg/kg 0.11 0.0015 8260B 06/27/07 148 erussell 024552
Methyl t-butyl ether MTBE BRL mg/kg 0.011 0.00032 8260B 06/27/07 148 erussell 024552
Methylene chloride BRL mg/kg 0.0055 0.00045 8260B 06/27/07 148 erussell Q24552
n-Butylbenzene BRL mg/kg 0.0055 0.00044 8260B 06/27/07 148 erussell Q24552
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of 35
Full Servico Anulyticul Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-1
185081
G0607589
06/20/07
06/20/07
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
Result Units Report MDL
Limit
1330
1635
Dilution Method
Factor
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
Analysis
Date/Time
06/27/07 148
06/27/07 148
06/27/07 148
06/27/07 148
06/27/07 148
06/27/07 148
06/27/07 148
06/27/07 148
06/27/07 148
06/27/07 148
06/27/07 148
06/27/07 148
06/27/07 148
06/27/07 148
06/27/07 148
Analyst Batch
ID
erussell 024552
erussell 024552
erussell Q24552
erussell Q24552
erussell 024552
erusseu 024552
erussell 024552
erussell Q24552
erussell Q24552
erussell Q24552
erussefl 024552
erussell 024552
erussell 024552
erussell 024552
erussell 024552
Parameter
n-Propylbenzene BRL
Naphthalene BRL
o-Xylene BRL
p-lsopropyltoluene BRL
sec-Butylbenzene BRL
Styrene BRL
tert-Butylbenzene BRL
Tetrachioroethene BRL
Toluene BRL
trans-i 2-Dichloroethene BRL
trans-I 3-Dichloropropene BRL
Trichioroethene BRL
Trichiorofluoromethane BRL
Vinyl acetate BRL
Vinyl chloride BRL
Semi-volatile Organic Comiounds by GC/MS
24-Trichlorobenzene BRL
2-Dichlorobenzene BRL
3-Dichlorobenzene BRL
4-Dichlorobenzene BRL
245-Trichlorophenol BRL
246-Trichlorophenol BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
0.0055
0.011
0.0055
0.0055
0.0055
0.0055
0.0055
0.0055
0.0055
0.0055
0.0055
0.0055
0.0055
0.028
0.0055
0.40
0.40
0.40
0.40
0.40
0.40
0.00033
0.00064
0.00033
0.00045
0.00036
0.00055
0.00034
0.00095
0.00038
0.00042
0.00039
0.00033
0.00045
0.0020
0.00071
0.040
0.030
0.029
0.036
0.041
0.039
Surrogate Recovery Control Limits
Bromofluorobenzene 101 77 128
Dibromofluoromethane 98 67 143
Toluene-d8 104 81 128
8270C
8270C
8270C
8270C
8270C
8270C
06/27/07
06/27/07
06/27/07
06/27/07
06/27/07
06/27/07
1504
1504
1504
1504
1504
1504
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampgotto
024556
024556
024556
024556
Q24556
024556
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Parameter
24-Dichiorophenol
24-Dimethylphenol
24-Dinitrophenol
24-Dinitrotoluene
26-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
34-Methylphenol
33-Dichlorobenzidine
46-Dinitro-2-methylphenol
4-Bromophenyiphenylether
4-Chloro-3-methylphenol
4-Chioroaniline
4-Chiorophenyiphenylether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzoaanthracene
Benzoapyrene
Benzobfluoranthene
Benzoghiperylene
Benzokfluoranthene
Analysis Analyst
Batch
Date/Time ID
06/27/07 1504 kcampigotto Q24556
06127/07 1504 kcampigotto Q24556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto Q24556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampgotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampigotto 024556
06/27/07 1504 kcampgotto 024556
06/27/07 1504 kcampigotto 024556
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
VR1SM
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 185081
Sample Matrix Soil COC Group G0607589
Time Collected 06/20/07 1330
Time Submitted 06/20/07 1635
Result Units Report MDL Dilution Method
Limit Factor
BRL mg/kg 0.40 0.034 8270C
BRL mg/kg 0.40 0.039 8270C
BRL mg/kg 2.0 0.045 8270C
BRL mg/kg 0.40 0.023 8270C
BRL mg/kg 0.40 0.043 8270C
BRL mg/kg 0.40 0.04 8270C
BRL mg/kg 0.40 0.032 8270C
BRL mg/kg 0.40 0.032 8270C
BRL mg/kg 0.40 0.038 8270C
BRL mg/kg 0.40 0.048 8270C
BRL mg/kg 0.40 0.041 8270C
BRL mg/kg 0.80 0.025 8270C
BRL mg/kg 2.0 0.024 8270C
BRL mg/kg 0.40 0.038 8270C
BRL mg/kg 0.80 0.029 8270C
BRL mg/kg 0.40 0.051 8270C
BRL mg/kg 0.40 0.025 8270C
BRL mg/kg 2.0 0.027 8270C
BRL mg/kg 0.40 0.039 8270C
BRL mg/kg 0.40 0.040 8270C
BRL mg/kg 0.40 0.030 8270C
BRL mg/kg 2.0 0.037 8270C
BRL mg/kg 0.40 0.056 8270C
BRL mg/kg 0.40 0.046 8270C
BRL mg/kg 0.40 0.018 8270C
BRL mg/kg 0.40 0.019 8270C
BRL mg/kg 0.40 0.033 8270C
Page 4of35
iSM
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
0.Box7030
Charlotte NC 28241
Laboratory Report
06/29/07
Ws-1
185081
G0607589
06/20/07 1330
06/20/07 1635
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method
Limit Factor
Analyst Batch
ID
Analysis
Date/Time
Benzoic acid BRL mg/kg 2.0 0.17 8270C 06/27/07 1504 kcampigotto 024556
Benzyt alcohol BRL mg/kg 0.80 0.042 8270C 06/27/07 1504 keampigotto Q24556
Bis2 chloroethoxymethane BRL mg/kg 040 046 8270C 06/27/07 15 04 kcampigotto 024556
Bis2-chloroethylether BRL mg/kg 0.40 0.044 8270C 06/27/07 1504 kcampigotto 024556
Bis2-chloroisopropylether BRL mg/kg 0.40 0.034 8270C 06/27/07 1504 kcampigotto 024556
Bis2-ethylhexylphthalate BRL mg/kg 0.40 0.020 8270C 06/27/07 1504 kcampigotto 024556
Butylbenzylphthalate BRL mg/kg 0.40 0.025 8270C 06/27/07 1504 kcampigotto Q24556
Chrysene BRL mg/kg 0.40 0.067 8270C 06/27/07 1504 kcampigotto 024556
Di-n-butylphthalate BRL mg/kg 0.40 0.018 8270C 06/27/07 1504 kcampigotto 024556
Di-n-octylphthalate BRL mg/kg 0.40 0.030 8270C 06/27/07 1504 kcampigotto 024556
Dibenzoahanthracene BRL mg/kg 0.40 0.040 8270C 06/27/07 1504 kcampigotto 024556
Dibenzofuran BRL mg/kg 0.40 0.034 8270C 06/27/07 1504 kcampigotto 024556
Diethylphthalate BRL mg/kg 0.40 0.025 8270C 06/27/07 1504 kcampigotto 024556
Dimethylphthalate BRL mg/kg 0.40 0.027 8270C 06/27/07 1504 kcampigotto 024556
Fluoranthene BRL mg/kg 0.40 0.028 8270C 06/27/07 1504 kcampigotto Q24556
Fluorene BRL mg/kg 0.40 0.024 8270C 06/27/07 1504 kcampigotto 024556
Hexachlorobenzene BRL mg/kg 0.40 0.021 8270C 06/27/07 1504 kcampigotto 024556
Hexachlorobutadiene BRL mg/kg 0.40 0.039 8270C 06/27/07 1504 kcampigotto 024556
Hexachiorocyclopentadiene BRL mg/kg 040 0.043 8270C 06/27/07 1504 kcampigotto Q24556
Hexachioroethane BRL mg/kg 0.40 0.041 8270C 06/27/07 1504 kcampigotto 024556
lndeno123-cdpyrene BRL mg/kg 0.40 0.041 8270C 06/27/07 1504 kcampigotto 024556
Isophorone BRL mg/kg 0.40 0.036 8270C 06/27/07 1504 kcampigotto Q24556
N-Nitrosodi-n-propylamine BRL mg/kg 0.40 0.046 8270C 06/27/07 1504 kcampigotto 024556
N-Nitrosodiphenylamine BRL mg/kg 0.40 0.020 8270C 06/27/07 1504 kcampigotto 024556
Naphthalene BRL mg/kg 0.40 0.044 8270C 06/27/07 1504 kcampigotto 024556
Nitrobenzene BRL mg/kg 0.40 0.039 8270C 06/27/07 1504 kcampigotto 024556
Pentachlorophenol BRL mg/kg 2.0 0.034 8270C 06/27/07 1504 kcampigotto 024556
Page of 35
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris
Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-1
185081
G0607589
06/20/07
06/20/07
Surrogate recovery
was outside of the control limits Matrix interference is suspected
Sample Preparation 30.06 mL 3550B 06/23/07 900 dpope P18716
Extractable Petroleum Hydrocarbons by GC-FID
Cl 1-C22 Aromatics BRL
C19-C36 Aliphatics BRL
C9-C18 Aliphatics BRL
Analysis Note for Cll-C22 Aromatics
Sample Preparation
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
1330
1635
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Phenanthrene BRL mg/kg 0.40 0.020 8270C 06/27/07 1504 kcampigotto 024556
Phenol BRL mg/kg 0.40 0.044 8270C 06/27/07 1504 kcampigotto Q24556
Pyrene BRL mg/kg 0.40 0.027 8270C 06/27/07 1504 kcampigotto Q24556
Surrogate Recovery Control Limits
246-Tribromophenol 99 25 123
2-Fluorobiphenyl 86 21 108
2-Fluorophenol 78 14 89
Nitrobenzene-d5 86 14 103
Phenol-d5 83 13-95
Terphenyl-d14 142 41 136
mg/kg
mg/kg
mg/kg
12 6.4
12 1.8
12 3.8
MADEP EPH
MADEP EPH
MADEP EPH
06/27/07 1003 grappaccioli
06/27/07 1003 grappaccioli
06/27/07 1003 grappaccioli
Adjusted value
10.24 niL EPH
Q24555
024555
024555
06/25/07 1200 dpope P18724
MetaIsbylCP
Chromium
Lead
Surrogate Recovery Control Limits
o-Terphenyl 93 40 140
1-Chloro-octadecarie 107 40 140
2-Bromonaphthalene 128 40 140
2-Fluorobiphenyl 134 40-140
37 mg/kg
9.0 mg/kg
0.27 0.016
1.1 0.022
6010B
6010B
06/25/07 2056 mcampbell
06/25/07 2056 mcampbell
024537
Q24537
Page of 35
Full Service Analytical Environmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
Result Units Report MDL Dilution
Limit Factor
Sample Preparation 2.29g 5OmL 3050B 06/25/07 915 jhoppel P1 8720
Volatile Petroleum Hydrocarbons by GC-PIDIFID
C5-C8 Aliphatics BRL mg/kg
C9-C10 Aromatics BRL mg/kg
C9-C1 Aliphatics
Analysis Note for C5C8 Aliphatics Adjusted value
Analysis Note for C9-C12 Aliphatics Adjusted value
Surrogate Recovery Control Limits
25-Dibromotoluene-FID 111 70 130
25-Dibromotoluene-PID 79 70-130
Sample Weight Determination
Weight 20.43
Weight 19.05
Sample Comments
BRL Below Reporting Limit
MADEP VPH 06/25/07 000 brown
MADEP VPH 06/25/07 000 Ibrown
J-Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanNECcertificationexceptforthose instances indicated in the case narrative and/or test comments
All results are reported on thy-weight basis
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter
WS-1
185081
G0607589
06/20/07
06/20/07
1330
1635
Method Analysis Analyst
Batch
Date/Time ID
6.1 1.2 MADEP VPH 06/27/07 2341 hwagner 024604
6.1 0.037 MADEP VPH 06/27/07 2341 hwagner 024604
BRL mg/kg 6.1 1.9 MADEP VPH 06/27/07 2341 hwagner 024604
Angela Overcash V.P Laboratory Services
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of 35
ESP Associates PA
Attn Chris Ward
O.Box7030
Charlotte NC 28241
Laboratory Report
06/29/07
WS-2
185082
G0607589
06/20/07
06/20/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Percent Solids Determination
Percent Solids
Sample Weight Determination
Weight Bisulfate
Weight Bisulfate
Weight Methanol
NC Certification No 402E1SMSCCertificationNo99012
NC Drinking Water Cert No 37735
Full Service Ace ylical Environmental Solutions
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1345
1635
80.1 SM2540 06/25/07 1745 Lthao
5.59
5.64
5.59
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Volatile Organic Compounds by GC/MS
11 1-Trichloroethane
11 22-Tetrachloroethane
11 2-Trichloroethane
1-Dichloroethane
11 -Dichloroethene
11 -Dichloropropene
23-Trichlorobenzene
23-Trichloropropane
24-Trichlorobenzene
24-Trimethylbenzene
2-Dibromoethane EDB
2-Dichlorobenzene
2-Dichloroethane
2-Dichloropropane
35-Trimethylbenzene
3-Dichlorobenzene
3-Dichloropropane
4-Dichlorobenzerie
22-Dichioropropane
2-Chiorotoluene
5035
5035
5035
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
0.0055 0.00031
0.0055 0.00056
0.0055 0.00034
0.0055 0.0004
0.0055 0.00042
0.0055 0.00049
0.0055 0.00061
0.0055 0.00049
0.0055 0.00053
0.0055 0.00042
0.0055 0.0001
0.0055 0.0003
0.0055 0.00055
0.0055 0.00041
0.0055 0.00046
0.0055 0.00048
0.0055 0.00038
0.0055 0.00043
0.0055 0.00028
0.0055 0.0004
06/27/07 000 Ibrown
06/27/07 000 brown
06/27/07 000 ibrown
06/27/07 219 erussell Q24552
06/27/07 219 erussell 024552
06/27/07 219 erussell Q24552
06/27/07 219 erussell Q24552
06/27/07 219 erussell Q24552
06/27/07 219 erussell 024552
06/27/07 219 erussell Q24552
06/27/07 219 erussell Q24552
06/27/07 219 erussell Q24552
06/27/07 219 erussell 024552
06/27/07 219 erussell 024552
06/27/07 219 erussell Q24552
06/27/07 219 erussell 024552
06/27/07 219 erusseH 024552
06/27/07 219 erussell Q24552
06/27/07 219 erussell 024552
06/27/07 219 erussell 024552
06/27/07 219 erussell 024552
06/27/07 219 erussell 024552
06/27/07 219 erussell 024552
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 8o135
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full Service Analytical Environmental Solutions
ESP Associates PA Project ID
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
Morehead Commons No Client Sample ID
Prism Sample ID
COC Group
Time Collected
Time Submitted
WS-2
185082
G0607589
06/20/07
06/20/07
2-Hexanone
4-Chiorotoluene
4-Methyl-2-pentanone MIBK
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chioromethane
cis-1 2-Dichloroethene
cis-1 3-Dichloropropene
Dichlorodifluoromethane
Ethylbenzene
lsopropyl ether IPE
Isopropylberizene
mp-Xylenes
Methyl ethyl ketone MEK
Methyl t-butyl ether MTBE
Methylene chloride
n-Butylbenzene
erussell
erussell
erussell
erussell
erussell
erussell
ewsseU
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
024552
Laboratory Report
06/29/07
Sample Matrix Soil
Parameter
1345
1635
Analyst Batch
ID
Result Units Report MDL Dilution Method Analysis
Limit Factor Date/Time
BRL mg/kg 0.055 0.00058 826DB 06/27/07 219
BRL mg/kg 0.0055 0.00029
826DB 06/27/07 219
BRL mg/kg 0.055 0.00055
826DB 06127/07 219
0.10 mg/kg 0.055 0.0022
826DB 06/27/07 219
BRL mg/kg 0.0033 0.00044
8260B 06/27/07 219
BRL mg/kg 0.0055 0.00039
826DB 06/27/07 219
BRL mg/kg 0.0055 0.00033 826DB 06/27/07 219
BRL mg/kg 0.0055 0.00049 826DB 06/27/07 219
BRL mg/kg 0.0055 0.00041 826DB 06/27/07 219
BRL mg/kg 0.011 0.00064 826DB 06/27/07 219
BRL mg/kg 0.0055 0.00032 826DB 06/27/07 219
BRL mg/kg 0.0055 0.00042 826DB 06/27/07 219
BRL mg/kg 0.0055 0.00038 826DB 06/27/07 219
BRL mg/kg 0.011 0.00045 826DB 06/27/07 219
BRL mg/kg 0.0055 0.00041 826DB 06/27/07 219
BRL mg/kg 0.0055 0.00039 826DB 06/27/07 219
BRL mg/kg 0.0055 0.00024 826DB 06/27/07 219
BRL mg/kg 0.0055 0.00035 826DB 06/27/07 219
BRL mg/kg 0.0055 0.0012 826DB 06/27/07 219
BRL mg/kg 0.0055 0.00039 826DB 06/27/07 219
BRL mg/kg 0.0055 0.00019 826DB 06/27/07 219
BRL mg/kg 0.0055 0.00044 826DB 06/27/07 219
BRL mg/kg 0.011 0.00077 826DB 06/27/07 219
BRL mg/kg 0.11 0.0015 826DB 06/27/07 219
BRL mg/kg 0.011 0.00032 826DB 06/27/07 219
BRL mg/kg 0.0055 0.00045 826DB 06/27/07 219
BRL mg/kg 0.0055 0.00044 826DB 06/27/07 219
Page of 35
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
WS-2
185082
G0607589
06/20/07 1345
06/20/07 1635
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full Service Analytical Environmental Solutlonc
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
Parameter Result Units Report MDL
Limit
Dilution Method
Factor
Analyst Batch
ID
0.0055 0.00033
0.011 0.00064
0.0055 0.00033
0.0055 0.00045
0.0055 0.00037
0.0055 0.00055
0.0055 0.00034
0.0055 0.00095
0.0055 0.00038
0.0055 0.00042
0.0055 0.00039
0.0055 0.00033
0.0055 0.00045
0.028 0.0020
0.0055 0.00071
8260B
82608
82608
8260B
8260B
8260B
8260B
8260B
82608
8260B
8260B
8260B
8260B
8260B
8260B
Analysis
Date/Time
06/27/07 219
06/27/07 219
06/27/07 219
06/27/07 219
06/27/07 219
06/27/07 219
06/27/07 219
06/27/07 219
06/27/07 219
06/27/07 219
06/27/07 219
06/27/07 219
06/27/07 219
06/27/07 219
06/27/07 219
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erusseH
erussell
erussell
erussefi
erusset
erussell
erussell
Q24552
024552
Q24552
024552
024552
024552
024552
024552
024552
Q24552
024552
024552
024552
024552
024552
n-Propylbenzene BRL
Naphthalene BRL
o-Xylene BRL
p-lsopropyltoluene BRL
sec-Butylbenzene BRL
Styrene BRL
tert-Butylbenzene BRL
Tetrachioroethene BRL
Toluene BRL
trans-i 2-Dichloroethene BRL
trans-i 3-Dichloropropene BRL
Trichioroethene BRL
Trichlorofluoromethane BRL
Vinyl acetate BRL
Vinyl chloride BRL
Semi-volatile Organic Comnounds by CC/MS
l24-Trichlorobenzene BRL
2-Dichlorobenzene BRL
3-Dichlorobenzene BRL
4-Dichlorobenzene BRL
245-Trichlorophenol BRL
246-Trichlorophenol BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Surrogate Recovery Control Limits
Bromofluorobenzene 110 77-128
Dibromofluoromethane 94 67 143
Toluene-d8 98 81 128
0.41
0.41
0.41
0.41
0.41
0.41
0.041
0.030
0.030
0.037
0.042
0.039
8270C
8270C
8270C
8270C
8270C
8270C
06/28/07 1015 kcampigotto
06/28/07 1015 keampigotto
06/28/07 1015 kcampigotto
06/28/07 1015 kcampigotto
06/28/07 1015 kcampigotto
06/28/07 1015 kcampigotto
024556
024556
Q24556
024556
024556
024556
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 10 of 35
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
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Laboratory Report
06/29/07
WS-2
185082
G0607589
06120/07 1345
06/20/07 1635
Parameter
24-Dichiorophenol
24-Dimethylphenol
24-Dinitrophenol
24-Dinitrotoluene
26-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methyiphenol
2-Nitrophenol
34-Methylphenol
33-Dichlorobenzidine
46-Dinitro-2-methylphenol
4-Bromophenylphenylether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chiorophenyiphenylether
4-Nitropheriol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzoaanthracene
Benzoapyrene
Benzobfluorartthene
Benzoghiperylene
Benzokfluoranthene
Batch
ID
024556
024556
024556
024556
Q24556
024556
024556
Q24556
Q24556
Q24556
024556
024556
Q24556
024556
024556
024556
024556
024556
024556
024556
024556
Q24556
024556
024556
024556
024556
024556
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Result Units Report MDL Dilution Method Analysis Analyst
Limit Factor Date/Time
BRL mg/kg 0.41 0.034 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 0.41 0.040 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 2.1 0.046 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 0.41 0.023 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 0.41 0.044 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 0.41 0.042 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 0.41 0.032 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 0.41 0.033 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 0.41 0.038 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 0.41 0.049 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 0.41 0.042 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 0.82 0.026 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 2.1 0.025 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 0.41 0.039 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 0.82 0.030 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 0.41 0.052 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 0.41 0.025 827oC 06/25/07 1015 kcampigotto
BRL mg/kg 2.1 0.027 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 0.41 0.040 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 0.41 0.041 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 0.41 0.031 8270C 06/28/07 1015 kcampigotto
BRL mg/kg 2.1 0.038 8270C 06/28/07 1015 kcampigotto
0.57 mg/kg 0.41 0.057 8270C 06/28/07 1015 kcampigotto
1.1 mg/kg 0.41 0.047 8270C 06/28/07 1015 kcampigotto
0.96 mg/kg 0.41 0.018 8270C 06/28/07 1015 kcampigotto
0.90 mg/kg 0.41 0.020 8270C 06/28/07 1015 kcampigotto
1.1 mg/kg 0.41 0.033 8270C 06/28/07 1015 kcampigotto
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 11 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
WS-2
185082
G0607589
06/20/07
06/20/07
Benzoic acid
Benzyl alcohol
Bis2-chloroethoxymethane
Bis2-chloroethylether
Bis2-chloroisopropylether
Bis2-ethylhexylphthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenzoahanthracene
Dibenzofuran
Diethylphthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachiorobutadiene
Hexachlorocyclopentadiene
Hexachioroethane
ndeno1 23-cdpyrene
lsophorone
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzerte
Pentachiorophenol
BRL mg/kg 2.1 0.17
BRL mg/kg 0.82 0.043
BRL mg/kg 0.41 0.047
BRL mg/kg 0.41 0.045
BRL mg/kg 0.41 0.035
BRL mg/kg 0.41 0.020
BRL mg/kg 0.41 0.025
0.68 mg/kg 0.41 0.068
BRL mg/kg 0.41 0.019
BRL mg/kg 0.41 0.031
BRL mg/kg 0.41 0.041
BRL mg/kg 0.41 0.035
BRL mg/kg 0.41 0.025
BRL mglkg 0.41 0.028
1.5 mg/kg 0.41 0.028
BRL mg/kg 0.41 0.024
BRL mg/kg 0.41 0.021
BRL mg/kg 0.41 0.040
BRL mg/kg 0.41 0.043
BRL mg/kg 0.41 0.042
0.96 mg/kg 0.41 0.042
BRL mg/kg 0.41 0.037
BRL mg/kg 0.41 0.047
BRL mg/kg 0.41 0.021
BRL mg/kg 0.41 0.045
BRL mg/kg 0.41 0.040
BRL mg/kg 2.1 0.034
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
024556
Q24556
024556
024556
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprinybrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Full Service Analytical Environmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter
1345
1635
Analyst Batch
ID
Result Units Report MDL Dilution Method Analysis
Limit Factor Date/Time
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
06/28/07 1015
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcarnpigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
024556
Q24556
024556
024556
Q24556
024556
024556
024556
024556
024556
Q24556
024556
Q24556
Q24556
024556
024556
024556
024556
024556
024556
024556
024556
024556
06/28/07 1015 kcampigotto
06/28/07 1015 kcampigotto
06/28/07 1015 kcampigotto
06/28/07 1015 kcampigotto
Page 12 of 35
Phenanthrene
Phenol
Pyrene
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-2
185082
G0607589
06/20/07 1345
06/20/07 1635
Surrogate recovery was outside of the control limits Matrix interference is suspected
Sample Preparation 30.11 mL 3550B 06/23/07 900 dpope P18716
13
13
13
6.9 MADEPEPH
1.9 MADEPEPH
4.1 MADEPEPH
Adjusted value
9.78g 2mL EPH
06/27/07 1326 grappaccioli
06/27/07 1326 grappaccioli
06/27/07 1326 grappaccioli
06/25/07 1200 dpope
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
024555
Q24555
Q24555
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
Parameter
Laboratory Report
06/29/07
Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
0.98 mg/kg 0.41 0.020 8270C 06/28/07 1015 kcampigotto 024556
BRL mg/kg 0.41 0.045 8270C 06/28/07 1015 kcampigotto 024556
2.5 mg/kg 0.41 0.028 8270C 06/28/07 1015 kcampigotto 024556
Surrogate Recovery Control Limits
246-Tribromophenol 115 25-123
2-Fluorobiphenyl 105 21 108
2-Fluorophenol 85 14 89
Nitrobenzene-d5 84 14 103
Phenol-d5 101 13-95
Terphenyl-d14 160 41 136
Extractable Petroleum Hydrocarbons by GC-FID
Cl 1-C22 Aromatics 20 mg/kg
C19-C36 Aliphatics BRL mg/kg
C9-C18 Aliphatics BRL mg/kg
Pnalysis Note for Cll-C22 Aromatics
Sample Preparation
Metals by ICP
Chromium
P1 8724
Lead
Surrogate Recovery Control Limits
1-Chloro-octadecane 106 40 140
2-Bromonaphthalene 91 40 140
2-Fluorobiphenyl 92 40 140
o-Terphenyl 88 40 140
29 mg/kg 0.25 0.015 6010B 06/25/07 2113 mcampbell Q24537
84 mg/kg 1.0 0.021 601GB 06/25/07 2113 mcampbell 024537
Page 13 of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-2
185082
G0607589
06/20/07 1345
06/20/07 1635
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Sample Preparation 2.47 50 mL 30506 06/25/07 915 jhoppel P18720
Volatile Petroleum Hydrocarbons by GC-PID/FID
C5-C8 Aliphatics BRL mg/kg 6.2 1.2 MADEP VPH 06/28/07 024 hwagner Q24604
C9-C10 Aromatics BRL mg/kg 6.2 0.037 MADEP VPH 06/28/07 024 hwagner Q24604
C9-C12 Aliphatics BRL mg/kg 6.2 1.9 MADEP VPH 06/28/07 024 hwagner Q24604
Analysis Note for C5-C8 Aliphatics Adjusted value
Analysis Note for C9-C12 Aliphatics Adjusted value
Surrogate Recovery Control Limits
25-Dibromotoluene-FID 119 70-130
25-Dibromotoluene-PID 84 70 130
Sample Weight Determination
Weight 14.40 MADEP VPH 06/25/07 000 Ibrown
Weight 18.95 MADEP VPH 06/25/07 000 brown
Sample Comments
BRL Below Reporting Limit
J-Estimated value beeen the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthose instances indicated in the case narrative and/or test comments
All results are reported on thy-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Full Service Analytical Environmental Solutions
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 14 of 35
SCCeflcaon No 99012 Laboratory Report
NC Drinking Water Cert No 37735 06/29/07
aU Service Analytical Environmental Solutions
ESP Associates PA Project ID Morehead Commons No Client Sample ID WS-3
ttn Chris Ward Prism Sample ID 185083
Box 7030 Sample Matrix Soil COC Group G0607589
Charlotte NC 28241 Time Collected 06/20/07 1400
Time Submitted 06/20/07 1635
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
ercent Solids Determination
ercent Solids 83.9 SM2540 06/25/07 1745 Lthao
amDIe Weight Determination
Weight Bisulfate 5.62 5035 06/27/07 000 brown
/eight Bisulfate 5.63 5035 06/27/07 000 Ibrown
eight Methanol 5.29 5035 06/27/07 000 brown
folatile Organic Corn nounds by GC/MS
111-Trichioroethane BRL mg/kg 0.0053 0.0003 826GB 06/27/07 251 erussell 024552
122-Tetrachloroethane BRL mg/kg 0.0053 0.00054 8260B 06/27/07 251 erussell 024552
2-Trichloroethane BRL mg/kg 0.0053 0.00033 826GB 06/27/07 251 erussefi 024552
1-Dichloroethane BRL mg/kg 0.0053 0.00038 826GB 06/27/07 251 erussell 024552
J1-Dichloroethene BRL mg/kg 0.0053 0.0004 826GB 06/27/07 251 erussell 024552
1-Dichloropropene BRL mg/kg 0.0053 0.00047 826GB 06/27/07 251 erusselt 024552
23-Trichlorobenzene BRL mg/kg 0.0053 0.00058 826GB 06/27/07 251 erusseH 024552
23-Trichloropropane BRL mg/kg 0.0053 0.00047 826GB 06/27/07 251 erussell 024552
24-Trichloroberizene BRL mg/kg 0.0053 0.0005 826GB 06/27/07 251 erussell 024552
124-Trimethylbenzene BRL mg/kg 0.0053 0.0004 826GB 06/27/07 251 erussefi Q24552
2-Dibromoethane EDB BRL mg/kg 0.0053 0.000095 826GB 06/27/07 251 erussell 024552
2-Dichlorobenzene BRL mg/kg 0.0053 0.00029 826GB 06/27/07 251 erussell 024552
2-Dichloroethane BRL mg/kg 0.0053 0.00053 826GB 06/27/07 251 erussefl 024552
2-Dichloropropane BRI mg/kg 0.0053 0.00039 826GB 06/27/07 251 erussell 024552
35-Trim ethylbenzene BRL mg/kg 0.0053 0.00044 826GB 06/27/07 251 erussell 024552
3-Dichlorobenzene BRL mg/kg 0.GG53 0.00046 826GB 06/27/07 251 erussell 024552
3-Dichloropropane BRL mg/kg 0.0053 0.00036 826GB 06/27/07 251 erussell 024552
4-Dichlorobenzene BRL mg/kg 0.GG53 0.00041 826GB 06/27/07 251 erussell 024552
22-Dichloropropane BRL mg/kg 0.0053 0.00026 826GB 06/27/07 251 erussell 024552
-ChIorotoIuene BRL mg/kg 0.0053 0.00039 826GB 06/27/07 251 erussell 024552
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 15 of 35
ull Service Analytical Environmental Solutions
ESP Associates PA
ttn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
WS-3
185083
G0607589
06/20/07
06/20/07
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1400
1635
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
-Hexanone BRL mg/kg 0.053 0.00055 8260B 06/27/07 251 erussell Q24552
4-Chlorotoluene BRL mg/kg 0.0053 0.00028 826GB 06/27/07 251 erussell Q24552
1-Methyl-2-pentanone MIBK BRL mg/kg 0.053 0.00053 826GB 06/27/07 251 erussell Q24552
Acetone BRL mg/kg 0.053 0.0021 826GB 06/27/07 251 erussefi Q24552
3enzene BRL mg/kg 0.0032 0.00042 826GB 06/27/07 251 erussell Q24552
romobenzene BRI mg/kg 0.0053 0.00037 826GB 06/27/07 251 erussell Q24552
Bromochloromethane BRL mg/kg 0.0053 0.00032 826GB 06/27/07 251 erussell Q24552
3romodichloromethane BRL mg/kg 0.0053 0.00047 8260B 06/27/07 251 erussell Q24552
Bromoform BRL mg/kg 0.0053 0.00039 826GB 06/27/07 251 erussell Q24552
3romornethane BRL mg/kg 0.011 0.00061 826GB 06/27/07 251 erussell Q24552
Carbon tetrachloride BRL mg/kg 0.0053 0.00031 826GB 06/27/07 251 erussell Q24552
hlorobenzene BRL mg/kg 0.0053 0.0004 826GB 06/27/07 251 erussell Q24552
Chlorodibromomethane BRL mg/kg 0.0053 0.00036 826GB 06/27/07 251 erussell Q24552
Chioroethane BRL mg/kg 0.011 0.00043 826GB 06/27/07 251 erussell Q24552
hloroform BRL mg/kg 0.0053 0.00039 826GB 06/27/07 251 erusset 024552
Chioromethane BRL mg/kg 0.0053 0.00037 826GB 06/27/07 251 erussell Q24552
is-1 2-Dichloroethene BRL mg/kg 0.0053 0.00023 826GB 06/27/07 251 erussell Q24552
cis-1 3-Dichloropropene BRL mg/kg 0.0053 0.00034 826GB 06/27/07 251 erussell 024552
ichlorodifluoromethane BRL mg/kg 0.0053 0.0012 826GB 06/27/07 251 erussell Q24552
Ethylbenzene BRL mg/kg 0.0053 0.00037 826GB 06/27/07 251 erussell 024552
sopropyl ether IPE BRL mg/kg 0.0053 0.00018 826GB 06/27/07 251 erussell Q24552
sopropyIbenzene BRL mg/kg 0.0053 0.00042 826GB 06/27/07 251 erussell Q24552
mpXylenes BRL mg/kg 0.011 0.00074 826GB 06/27/07 251 erussell Q24552
i1ethyl ethyl ketone MEK BRL mg/kg 0.11 0.0015 826GB 06/27/07 251 erussell Q24552
Methyl t-butyl ether MTBE BRL mg/kg 0.011 0.00031 826GB 06/27/07 251 erussefl Q24552
lethyIene chloride BRL mg/kg 0.0053 0.00043 826GB 06/27/07 251 erussel Q24552
n-Butylbenzene BRL mg/kg 0.0053 0.00042 826GB 06/27/07 251 erussell 024552
Page 16 of 35
uu1 Service Analytical Environmental Solutions
ESP Associates PA
ttn Chris Ward
P.O Box7030
Charlotte NC 28241
Laboratory Report
06/29/07
WS-3
185083
G0607589
06/20/07
06/20/07
arameter
i-Propylbenzene
Naphthalene
-Xylene
p-lsopropyltoluene
r5ec-Butylbenzene
Styrene
tert-Butylbenzene
retrachloroethene
Toluene
rans-I 2-Dichloroethene
trans-I 3-Dichloropropene
rrichloroethene
--rrichlorofluoromethane
Vinyl acetate
finyI chloride
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1400
1635
Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
BRL mg/kg 0.0053 0.00032 8260B 06/27/07 251 erussell Q24552
BRL mg/kg 0.011 0.00061 8260B 06/27/07 251 erussell 024552
BRL mg/kg 0.0053 0.00032 8260B 06/27/07 251 erussell Q24552
BRI mg/kg 0.0053 0.00043 8260B 06/27/07 251 erussell Q24552
BRL mg/kg 0.0053 0.00035 8260B 06127/07 251 erussell 024552
BRL mg/kg 0.0053 0.00053 8260B 06/27/07 251 erusseli Q24552
BRL mg/kg 0.0053 0.00033 8260B 06/27/07 251 erussell Q24552
BRL mg/kg 0.0053 0.00091 8260B 06/27/07 251 erussell 024552
BRL mg/kg 0.0053 0.00036 8260B 06/27/07 251 erussell 024552
BRL mg/kg 0.0053 0.0004 8260B 06/27/07 251 erussell 024552
BRL mg/kg 0.0053 0.00037 8260B 06/27/07 251 erusseli 024552
BRL mg/kg 0.0053 0.00032 8260B 06/27/07 251 erussell 024552
BRL mg/kg 0.0053 0.00043 8260B 06/27/07 251 erussetl Q24552
BRL mg/kg 0.026 0.0019 8260B 06/27/07 251 erussell Q24552
BRL mg/kg 0.0053 0.00068 8260B 06/27/07 251 erusself 024552
Surrogate Recovery Control Limits
Toluene-d8 101 81 128
Bromofluorobenzene 100 77-128
Dibromofluoromethane 91 67 143
.5emi-volatile Organic ComDoundS by GC/MS
24-Trichlorobenzene BRL mg/kg 0.40 0.039 8270C 06/27/07 2010 kcampigotto 024556
2-Dichlorobenzene BRL mg/kg 0.40 0.029 8270C 06/27/07 2010 kcampigotto 024556
3-Dichlorobenzene BRL mg/kg 0.40 0.028 8270C 06/27/07 2010 kcampigotto Q24556
4-Dichlorobenzene BRL mg/kg 0.40 0.036 8270C 06/27/07 2010 kcampigotto 024556
245-Trichlarophenol BRL mg/kg 0.40 0.040 8270C 06/27/07 2010 kcampigotto Q24556
246-Trichlorophenol BRL mg/kg 0.40 0.038 8270C 06/27/07 2010 kcampigotto Q24556
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 17 of 35
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
oil Service Analyircal Environmental Solutions
ESP Associates PA Project ID
Qtn Chris Ward
Box 7030
Charlotte NC 28241
Morehead Commons No Client Sample ID
Prism Sample ID
COG Group
Time Collected
Time Submitted
WS-3
185083
G0607589
06/20/07 1400
06/20/07 1635
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Laboratory Report
06/29/07
Sample Matrix Soil
3arameter Result Units Report MDL Dilution Method Analysis
Limit Factor Date/Time
06/27/07 2010
06/27/07 2010
06/27/07 2010
06/27/07 2010
06/27/07 2010
06/27/07 2010
06/27/07 2010
06/27/07 2010
06/27/07 2010
06/27/07 2010
06/27/07 2010
06/27/07 2010
06/27/07 2010
06/27/07 2010
06/27/07 2010
06/27/07 2010
06/27107 2010
06/27/07 2010
4-Dichlorophenol
24-Dimethyiphenol
4-DinitrophenoI
24-Dinitrotoluene
6-Dinitrototuene
--Chloronaphthalene
2-Chiorophenol
-Methylnaphthalene
2-Methyiphenol
-Nitrophenol
34-Methylphenol
c3-Dichlorobenzidine
46-Dinitro-2-methylphenol
4-Bromophenylphenylether
-Chloro-3-methylphenol
4-Chioroaniline
-Chlorophenylphenylether
4-Nitrophenol
cenaphthene
Acenaphthylene
nthracene
zobenzene
enzoaanthracene
enzoapyrene
Benzobfluoranthene
enzoghiperylene
Benzokfluoranthene
Analyst Batch
ID
kcampigotto Q24556
kcampigotto Q24556
kcampigotto 024556
kcampigotto Q24556
kcampigotto Q24556
kcampigotto Q24556
kcampigotto 024556
kcampigotto Q24556
kcampigotto 024556
kcampigotto Q24556
kcampigotto 024556
kcampigotto Q24556
kcampigotto 024556
kcampigotto Q24556
kcampigotto Q24556
kcampigotto Q24556
kcampigotto 024556
kcampigotto Q24556
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
0.12
0.25J
BRL
BRL
BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
0.40
0.40
2.0
0.40
0.40
0.40
0.40
0.40
0.40
0.40
0.40
0.79
2.0
0.40
0.79
0.40
0.40
2.0
0.40
0.40
0.40
2.0
0.40
0.40
0.40
0.40
0.40
0.033
0.038
0.044
0.022
0.042
0.041
0.031
0.031
0.037
0.047
0.040
0.025
0.024
0.037
0.029
0.050
0.024
0.026
0.039
0.039
0.030
0.037
0.055
0.046
0.018
0.019
0.032
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270G
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
06/27/07 2010 kcampigotto
06/27/07 2010 kcampigotto
06/27/07 2010 kcampigotto
06/27/07 2010 kcampigotto
06/27/07 2010 kcampigotto
06/27/07 2010 kcampigotto
06/27/07 2010 kcampigotto
06/27/07 2010 kcampigotto
06/27/07 2010 kcampigotto
024556
024556
Q24556
Q24556
024556
Q24556
Q24556
Q24556
024556
Page 18 of 35
ESP Associates PA
kiln Chris Ward
-P Box 7030
Charlotte NC 28241
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Dnnking Water Cert No 37735
ull Servico Analytical Environmental Sotutiono
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 185083
Sample Matrix Soil COC Group G0607589
Time Collected 06/20/07
Time Submitted 06/20/07
1400
1635
arameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
3erizoic acid BRL mg/kg 2.0 0.17 8270C 06/27/07 2010 kcampigotto 024556
Benzyl alcohol BRL mg/kg 0.79 0.042 8270C 06/27/07 2010 kcampigotto 024556
is2-chloroethoxymethane BRL mg/kg 0.40 0.045 8270C 06/27/07 2010 kcampigotto 024556
--3is2-chloroethylether BRL mg/kg 0.40 0.043 8270C 06/27/07 2010 kcampigotto 024556
3is2-chloroisopropylether BRL mg/kg 0.40 0.034 8270C 06/27/07 2010 kcampigotto Q24556
3is2-ethylhexylphthalate BRL mg/kg 0.40 0.019 8270C 06/27/07 2010 kcampigotto 024556
Butylbenzylphthalate BRL mg/kg 0.40 0.024 8270C 06/27/07 2010 kcampigotto 024556
hrysene 0.14 mg/kg 0.40 0.066 8270C 06/27/07 2010 kcampigotto 024556
Di-n-butylphthalate BRL mg/kg 0.40 0.018 8270C 06/27/07 2010 kcarnpigotto 024556
i-n-octylphthalate BRL mg/kg 0.40 0.029 8270C 06/27/07 2010 kcampigotto 024556
bibenzoaharithracene BRL mg/kg 0.40 0.040 8270C 06/27/07 2010 kcampigotto 024556
ibenzofuran BRI mg/kg 0.40 0.034 8270C 06/27/07 2010 kcampigotto 024556
iethyIphthalate BRL mg/kg 0.40 0.024 8270C 06/27/07 2010 kcampigotto 024556
--0imethylphthalate BRL mg/kg 0.40 0.027 8270C 06/27/07 2010 kcampigotto 024556
luoranthene 0.24 mg/kg 0.40 0.027 8270C 06/27/07 2010 kcampigotto 024556
Fluorene BRL mg/kg 0.40 0.023 8270C 06/27/07 2010 kcampigotto Q24556
lexachlorobenzene BRI mg/kg 0.40 0.020 8270C 06/27/07 2010 kcampigotto 024556
Hexachlorobutacjiene BRL mg/kg 0.40 0.038 8270C 06/27/07 2010 kcampigotto 024556
lexachlorocyclopentadiene BRI mg/kg 0.40 0.042 8270C 06/27/07 2010 kcampigotto 024556
ilexachioroethane BRL mg/kg 0.40 0.040 8270C 06/27/07 2010 kcampigotto 024556
rideno1 23-cdpyrene BRL mg/kg 0.40 0.040 8270C 06/27/07 2010 kcampigotto Q24556
-sophorone BRL mg/kg 0.40 0.035 8270C 06/27/07 2010 kcampigotto Q24556
N-Nitrosodi-n-propylamine BRL mg/kg 0.40 0.045 8270C 06/27/07 2010 kcampigotto 024556
Nitrosodiphenylamine BRL mg/kg 0.40 0.020 8270C 06/27/07 2010 kcampigotto 024556
Naphthalene BRL mg/kg 0.40 0.043 8270C 06/27/07 2010 kcampigotto Q24556
Jitrobenzene BRL mg/kg 0.40 0.038 8270C 06/27/07 2010 kcampigotto 024556
Pentachlorophenol BRL mg/kg 2.0 0.033 8270C 06/27/07 2010 kcampigotto 024556
Page 19 of 35
Extractable Petroleum Hydrocarbons by GC-FID
Q1 1-C22 Aromatics 52
19-C36iphatics 11
C9-C18 Aliphatics BRL
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
PISM
ATORiES
all Service Analytical Environmental Solutions
ESP Associates PA
\ttn Chris Ward
Box 7030
Charlotte NC 28241
arameter
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 185083
Sample Matrix Soil COC Group G0607589
Time Collected 06/20/07
Time Submitted 06/20/07
1400
1635
henanthrene
Phenol
yrene
Sam pie Preparation
Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
BRL mg/kg 0.40 0.019 8270C 06/27/07 2010 kcampigotto Q24556
BRL mg/kg 0.40 0.043 8270C 06/27/07 2010 kcampigotto Q24556
0.42 mg/kg 0.40 0.027 8270C 06/27/07 2010 kcampgotto Q24556
29.87 mL 355GB 06/23/07 900 dpope P18716
Surrogate Recovery Control Limits
246-Tribromophenol 100 25-123
Terphenyl-d14 118 41-136
Nitrobenzene-d5 77 14-103
2-Fluorobiphenyl 89 21 108
Phenol-d5 88 13-95
2-Fluorophenol 78 14-89
mg/kg
mg/kg
mg/kg
12 6.3
12 1.8
12 3.7
MADEP EPH
MADEP EPH
MADEP EPH
l\nalysis Note for Cll-C22 Aromatics Adjusted value
Surrogate recovery was outside of the control limits Matrix interference is suspected
06/27/07 1510 grappaccioli
06/27/07 1510 grappaccioli
06/27/07 1510 grappaccioli
Q24555
Q24555
Q24555
P1 872410.2 mL EPH 06/25/07 1200 dpopeSamplePreparation
letals by ICP
thromium
ead
Surrogate Recovery Control Limits
1-Chloro-octadecane 151 40-140
2-Bromonaphthalene 132 40 140
2-Fluorobiphenyl 135 40-140
o-Terphenyl 113 40-140
29 mg/kg 0.27 0.016 6010B 06/25/07 2120 mcampbeli Q24537
7.5 mg/kg 1.1 0.023 601GB 06/25/07 2120 mcampbell 024537
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 282240543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 20 of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
all Service Analytical Environmental Solutions
2arameter
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Sample Preparation 2.22g 5OmL 3050B 06/25/07 915 jhoppel P18720
BRL mg/kg 6.0 1.1 MADEP VPH 06/28/07 107 hwagner Q24604
BRL mg/kg 6.0 0.036 MADEP VPH 06/28/07 107 hwagner Q24604
BRL mg/kg 6.0 1.8 MADEP VPH 06/28/07 107 hwagner Q24604
Analysis Note for C5-C8 Aliphatics Adjusted value
Analysis Note for C9-Cl2 Aliphatics Adjusted value
Sample Weight Determination
Neight
Weight
MADEP VPH 06/25/07 000 brown
MADEP VPH 06/25/07 000 brown
Sample Comments -_______________________________
Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanVELACcertificationexceptforthose instances indicated in the case narrative and/or test comments
4ll results are reported on dry-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 282240543
ESP Associates PA
\ttn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
WS-3
185083
G0607589
06/20/07
06/20/07
1400
1635
Volatile Petroleum Hydrocarbons by GC-PlD/FID
Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
5-C8 Aliphatics
C9-C10 Aromatics
9-C12 Aliphatics
Surrogate Recovery Control Limits
25-Dibromotoluene-FID 112 70-130
25-Dibromotoluene-PID 79 70-130
18.11
19.81
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 21 of 35
Laboratory Report
06/29/07
ESP Associates PA WS-4
Attn Chris Ward 185084
Box 7030 G0607589
Charlotte NC 28241 06/20/07
06/20/07
Percent Solids Determination
Percent Solids 85.7
Sample Weight Determination
Weight Bisulfate
Weight Bisulfate
Weight Methanol
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1415
1635
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
SM2540 06/25/07 1745 Lthao
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
5.44
5.08
4.18
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
Volatile Organic Compounds by GC/MS
111 -Trichloroethane
11 22-Tetrachloroethane
11 2-Trichloroethane
11 -Dichloroethane
1-Dichloroethene
1-Dichloropropene
23-Trichlorobenzene
23-Trichloropropane
24-Trichlorobenzene
24-Trimethylbenzene
2-Dibromoethane EDB
2-Dichlorobenzene
2-Dichloroethane
2-Dichloropropane
35-Trimethylbenzene
3-Dichlorobenzene
3-Dichloropropane
14-Dichlorobenzene
22-Dichloropropane
2-Chlorotoluene
5035
5035
5035
8260B
8260B
826DB
8260B
8260B
8260B
826DB
826DB
8260B
826DB
8260B
8260B
826DB
826DB
8260B
8260B
8260B
8260B
8260B
826DB
0.0054
0.0054
0.0054
0.0054
0.0054
0.0054
0.0054
0.0054
0.0054
0.0054
0.0054
0.0054
0.0054
0.0054
0.0054
0.0054
0.0054
0.0054
0.0054
0.0054
0.0003
0.00055
0.00033
0.00039
0.00041
0.00047
0.00059
0.00047
0.00051
0.00041
0.000097
0.00029
0.00054
0.0004
0.00045
0.00046
0.00036
0.00042
0.00027
0.0004
06/27/07 000 brown
06/27/07 000 brown
06/27/07 000 brown
06/27/07 322 erussell 024552
06/27/07 322 erussell 024552
06/27/07 322 erussell Q24552
06/27/07 322 erusset 024552
06/27/07 322 erussel Q24552
06/27/07 322 erussell Q24552
06/27/07 322 erusseD Q24552
06/27/07 322 erussell Q24552
06/27/07 322 erussell 024552
06/27/07 322 erussell 024552
06/27/07 322 erussell 024552
06/27/07 322 erussell 024552
06/27/07 322 erussell 024552
06/27/07 322 erussell 024552
06/27/07 322 erussell 024552
06/27/07 322 erussell 024552
06/27/07 322 erussell 024552
06/27/07 322 erussell 024552
06/27/07 322 erussell 024552
06/27/07 322 erussell 024552
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 22 of 35
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-4
185084
G0607589
06/20/07 1415
06/20/07 1635
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
2-Hexanone BRL mg/kg 0.054 0.00056 826DB 06/27/07 322 erussell 024552
4-Chiorotoluene BRL mg/kg 0.0054 0.00028 8260B 06/27/07 322 erussell 024552
Methyl pentanone MIBK BRL mg/kg 054 00054 8260B 06/27/07 22 erussell 024552
Acetone 0.063 mg/kg 0.054 0.0021 8260B 06/27/07 322 erussell 024552
Benzene BRL mg/kg 0.0032 0.00043 8260B 06/27/07 322 erussell 024552
Bromobenzene BRL mg/kg 0.0054 0.00038 8260B 06/27/07 322 erussell 024552
Bromochloromethane BRL mg/kg 0.0054 0.00032 8260B 06/27/07 322 erussell 024552
Bromodichloromethane BRL mg/kg 0.0054 0.00047 826DB 06/27/07 322 erussell 024552
Bromoform BRL mg/kg 0.0054 0.0004 8260B 06/27/07 322 erussell Q24552
Bromomethane BRL mg/kg 0.011 0.00062 8260B 08/27/07 322 erussell 024552
Carbon tetrachloride BRL mg/kg 0.0054 0.00031 8260B 06/27/07 322 erussetl 024552
Chlorobenzene BRL mg/kg 0.0054 0.00041 8260B 06/27/07 322 erussell 024552
Chlorodibromomethane BRL mg/kg 0.0054 0.00036 8260B 06/27/07 322 erussell 024552
Chloroethane BRL mg/kg 0.011 0.00044 8260B 06/27/07 322 erussell 024552
Chloroform BRL mg/kg 0.0054 0.0004 8260B 06/27/07 322 erussell 024552
Chioromethane BRL mg/kg 0.0054 0.00038 8260B 06/27/07 322 erussell 024552
cis-12-Dichloroethene BRL mg/kg 0.0054 0.00024 8260B 06/27/07 322 erussell 024552
cis-1 3-Dichloropropene BRL mg/kg 0.0054 0.00034 8260B 06/27/07 322 erussell 024552
Dichlorodifluoromethane BRL mg/kg 0.0054 0.0012 8260B 06/27/07 322 erussell 024552
Ethylbenzene BRL mg/kg 0.0054 0.00038 8260B 06/27/07 322 erussell 024552
Isopropyl ether IPE BRL mg/kg 0.0054 0.00018 8260B 06/27/07 322 erussell 024552
lsopropylbenzene BRL mg/kg 0.0054 0.00043 8260B 06/27/07 322 erussell 024552
mp-Xylenes BRL mg/kg 0.011 0.00075 8260B 06/27/07 322 erussell 024552
Methyl ethyl ketone MEK BRL mg/kg 0.11 0.0015 8260B 06/27/07 322 erussell 024552
Methyl t-butyl ether MTBE BRL mg/kg 0.011 0.00031 8260B 06/27/07 322 erussell 024552
Methylerte chloride BRL mg/kg 0.0054 0.00044 8260B 06/27/07 322 erussell Q24552
n-Butylbenzene BRL mg/kg 0.0054 0.00043 826DB 06/27/07 322 erussell Q24552
Page 23 of 35
Laboratory Report
06/29/07
WS-4
185084
G0607589
08/20/07 1415
06/20/07 1635
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
R1SM
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method Analyst Batch
ID
Analysis
Limit Factor Date/Time
0.0054 0.00032 82608 06/27/07 322 erusset Q24552
0.011 0.00062 8260B 06/27/07 322 erussell Q24552
0.0054 0.00032 8260B 06/27/07 322 erussell Q24552
0.0054 0.00044 8260B 06/27/07 322 erussell 024552
0.0054 0.00035 8260B 06/27/07 322 erusseH 024552
0.0054 0.00054 8260B 06/27/07 322 erussell 024552
0.0054 0.00033 8260B 06/27/07 322 erussell 024552
0.0054 0.00092 8260B 06/27/07 322 erussell Q24552
0.0054 0.00036 8260B 06/27/07 322 erussell 024552
0.0054 0.00041 82608 06/27/07 322 erussell Q24552
0.0054 0.00038 8260B 06/27/07 322 erussell 024552
0.0054 0.00032 8260B 06/27/07 322 erusseH Q24552
0.0054 0.00044 8260B 06/27/07 322 erussefl 024552
0.027 0.0019 82608 06/27/07 322 erussefi 024552
0.0054 0.00069 8260B 06/27/07 322 erussell Q24552
n-Propylbenzene BRL
Naphthalene BRL
o-Xylene BRL
p-lsopropyltoluene BRL
sec-Butylbenzene BRL
Styrene BRL
tert-Butylbenzene BRL
Tetrachloroethene BRL
Toluene BRL
trans-i 2-Dichloroethene BRL
trans-i 3-Dichloropropene BRL
Trichioroethene BRL
Trichiorofluoromethane BRL
Vinyl acetate BRL
Vinyl chloride BRL
Semi-volatile Organic Compounds by GC/MS
124-Trichlorobenzene BRL
2-Dichlorobenzene BRL
3-Dichlorobenzene BRL
4-Dichlorobenzene BRL
245-Trichiorophenol BRL
246-Trichlorophenol BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Surrogate Recovery Control Limits
Bromofluorobenzene 103 77 128
Dibromofluoromethane 99 67 143
Toluene-d8 105 81 128
0.39
0.39
0.39
0.39
0.39
0.39
0.039
0.029
0.028
0.035
0.040
0.037
8270C
8270C
8270C
8270C
8270C
8270C
06/27/07
06/27/07
06/27/07
06/27/07
06/27/07
06/27/07
1828
1828
1828
1828
1828
1828
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
024556
Q24556
024556
Q24556
Q24556
024556
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 24 of 35
Full Service Analytical
Environmental Solutions
Laboratory Report
06/29/07
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
WS-4
185084
G0607589
06/20/07
06/20/07
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method
1415
1635
Limit Factor
AnalystAnalysis Batch
Date/Time ID
24-Dichlorophenol BRL mg/kg 0.39 0.033 827CC 06/27/07 1828 kcarnpigotto 024556
24-Dimethyiphenol BRL mg/kg 0.39 0.037 827CC 06/27/07 1828 kcampigotto 024556
24-Dinitrophenol BRL mg/kg 1.9 0.044 827CC 06/27/07 1828 kcampigotto 024556
24-Dinitrotoluene BRL mg/kg 0.39 0.022 827CC 06/27/07 1828 kcampigotto 024556
26-Dinitrotoluene BRL mg/kg 0.39 0.041 8270C 06/27/07 1828 kcampigotto Q24556
2-Chloronaphthalene BRL mg/kg 0.39 0.040 8270C 06/27/07 1828 kcampigotto Q24556
2-Chlorophenol BRL mg/kg 0.39 0.031 827CC 06/27/07 1828 kcampigotto 024556
2-Methylnaphthalene BRL mg/kg 0.39 0.031 827CC 06/27/07 1828 kcampigotto 024556
2-Methylphenol BRL mg/kg 0.39 0.036 8270C 06/27/07 1828 kcampigotto 024556
2-Nitrophenol BRL mg/kg 0.39 0.047 8270C 06/27/07 1828 kcampigotto Q24556
34-Methylphenol BRL mg/kg 0.39 0.040 827CC 06/27/07 1828 kcampigotto 024556
33-Dichlorobenzidine BRL mg/kg 0.78 0.024 827CC 06/27/07 1828 kcampigotto 024556
46-Dinitro-2-methylphenol BRL mg/kg 1.9 0.024 827CC 06/27/07 1828 kcampigotto 024556
4-Bromophenylphenylether BRL mg/kg 0.39 0.037 827CC 06/27/07 1828 kcampigotto 024556
4-Chloro-3-methylphenol BRL mg/kg 0.78 0.029 827CC 06/27/07 1828 kcampigotto 024556
4-Chloroaniline BRL mg/kg 0.39 0.050 827CC 06/27/07 1828 kcampigotto 024556
4-Chlorophenylphenylether BRL mg/kg 0.39 0.024 827CC 06/27/07 1828 kcampigotto 024556
4-Nitrophenol BRL mg/kg 1.9 0.026 8270C 06/27/07 1828 kcampigotto 024556
Acenaphthene BRL mg/kg 0.39 0.038 8270C 06/27/07 1828 kcampigotto 024556
Acenaphthylene BRL mg/kg 0.39 0.039 827CC 06/27/07 1828 kcampigotto 024556
Anthracene BRL mg/kg 0.39 0.029 827CC 06/27/07 1828 kcampigotto 024556
Azobenzene BRL mg/kg 1.9 0.036 827CC 06/27/07 1828 kcampigotto 024556
Benzoaanthracene BRL mg/kg 0.39 0.054 827CC 06/27/07 1828 kcampigotto 024556
Benzoapyrene BRL mg/kg 0.39 0.045 827CC 06/27/07 1828 kcampigotto 024556
Benzobfluoranthene BRL mg/kg 0.39 0.017 827CC 06/27/07 1828 kcampigotto 024556
Benzoghiperylene BRL mg/kg 0.39 0.019 827CC 06/27/07 1828 kcampigotto 024556
Benzokfluoranthene BRL mg/kg 0.39 0.032 827CC 06/27/07 1828 kcampigotto 024556
Page 25 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/2 9107
WS-4
185084
G0607589
06/20/07
06/20/07
Parameter
Benzoic acid
Benzyl alcohol
Bis2-chloroethoxymethane
Bis2-chloroethylether
Bis2-chloroisopropylether
Bis2-ethylhexylphthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenzoahanthracene
Dibenzofuran
Diethylphthalate
Dim ethylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachiorobutadiene
Hexachiorocyclopentadiene
Hexachioroethane
lndeno1 23-cdpyrene
Isophorone
N-Nitrosodi-n-propylamine
N-Nitrosodipheriylamine
Naphthalene
Nitrobenzene
Pentachiorophenol
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full Service Analytical Environmental Solutions
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Result Units Report MDL Dilution
1415
1635
Method Analysis Analyst Batch
IDLimitFactorDate/Time
BRL mg/kg 1.9 0.17 8270C 06/27/07 1828 kcampigotto 024556
BRL mg/kg 0.78 0.041 8270C 06/27/07 1828 kcampigotto Q24556
BRL mg/kg 0.39 0.045 8270C 06/27/07 1828 kcampigotto 024556
BRL mg/kg 0.39 0.042 8270C 06/27/07 1828 kcampigotto 024556
BRL mg/kg 0.39 0.033 8270C 06/27/07 1828 kcampigotto 024556
BRL mg/kg 0.39 0.019 8270C 06/27/07 1828 kcampigotto 024556
BRL mg/kg 0.39 0.024 8270C 06/27/07 1828 kcampigotto Q24556
BRL mg/kg 0.39 0.065 8270C 06/27/07 1828 kcampigotto Q24556
BRL mg/kg 0.39 0.018 8270C 06/27/07 1828 kcampigotto Q24556
BRL mg/kg 0.39 0.029 8270C 06/27/07 1828 kcampigotto Q24556
BRL mg/kg 0.39 0.039 8270C 06/27/07 1828 kcampigotto 024556
BRL mg/kg 0.39 0.033 8270C 06/27/07 1828 kcampigotto 024556
BRL mg/kg 0.39 0.024 8270C 06/27/07 1828 kcampigotto 024556
BRL mg/kg 0.39 0.027 8270C 06/27/07 1828 kcampigotto 024556
BRL mg/kg 0.39 0.027 8270C 06/27/07 1828 kcampigotto 024556
BRL mg/kg 0.39 0.023 8270C 06/27/07 1828 kcampigotto Q24556
BRL mg/kg 0.39 0.020 8270C 06/27/07 1828 kcampigotto Q24556
BRL mg/kg 0.39 0.038 8270C 06/27/07 1828 kcampigotto 024556
BRL mg/kg 0.39 0.041 8270C 06/27/07 1828 kcampigotto Q24556
BRL mg/kg 0.39 0.040 8270C 06/27/07 1828 kcampigotto 024556
BRL mg/kg 0.39 0.040 8270C 06/27/07 1828 kcampigotto 024556
BRL mg/kg 0.39 0.035 8270C 06/27/07 1828 kcampigotto Q24556
BRL mg/kg 0.39 0.044 8270C 06/27/07 1828 kcampigotto Q24556
BRL mg/kg 0.39 0.020 8270C 06/27/07 1828 kcampigotto 024556
BRL mg/kg 0.39 0.042 8270C 06/27/07 1828 kcampigotto 024556
BRL mg/kg 0.39 0.038 8270C 06/27/07 1828 kcampigotto Q24556
BRL mg/kg 1.9 0.033 8270C 06/27/07 1828 kcampgofto 024556
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 26 of 35
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris
Ward
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Laboratory Report
06/29107
WS-4
185084
G0607589
06/20/07
06/20/07
Extractable Petroleum Hydrocarbons by GC-FID
C11-C22 Aromatics BRL mg/kg
C19-C36 Aliphatics BRL mg/kg
C9-C18 Aliphatics BRL mg/kg
Analysis Note for Cll-C22 Aromatics
14 mg/kg 0.28 0.017
8.2 mg/kg 1.1 0.023
Surrogate
2-Bromonaphthalene
Recovery
103
o-Terphenyl 91
-Chloro-octadecane
2-Fluorobiphenyl
Control Limits
40-140
40-140
40-140
40-140
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter
Phenanthrene
Phenol
Pyrene
1415
1635
Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
BRL mg/kg 0.39 0.019 8270C 06/27/07 1828 kcampigotto 024556
BRL mg/kg 0.39 0.042 8270C 06/27/07 1828 kcampigotto Q24556
BRL mg/kg 0.39 0.027 8270C 06/27/07 1828 kcampigotto Q24556
Sample Preparation 29.69 mL 3550B 06/23/07 900 dpope P1 8716
Surrogate Recovery Control Limits
Terphenyl-d14 102 41 136
246-Tribromophenol 90 25 123
2-Fluorophenol 68 14 89
Phenol-d5 82 13-95
2-Fluorobiphenyl 85 21 108
Nitrobenzene-d5 64 14 103
12 6.3 MADEP EPH 06/27/07 1654 grappaccioli 024555
12 1.7 MADEP EPH 06/27/07 1654 grappaccioli 024555
12 3.7 MADEP EPH 06/27/07 1654 grappaccioli 024555
Adjusted value
10.06 mL EPH 06/25/07 1200 dpope P18724SamplePreparation
Metals by ICP
Chromium
Lead
103
107
601 OB 06/25/07 2127 mcampbell 024537
6010B 06/25/07 2127 mcampbell 024537
Page 27 of 35
LW
Full Service Analytical Environmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID WS-4
Prism Sample ID 185084
Sample Matrix Soil
Result Units Report MDL Dilution
Limit Factor
2.09g 5OmL
Volatile Petroleum Hydrocarbons byGC-PID/FID
C5-C8Aliphatics BRL mg/kg 5.8 1.1 MADEPVPH 06/28/07 150 hwagner
BRL mg/kg 5.8 0.035 MADEP VPH 06/28/07 150 hwagner
BRL mg/kg
Analysis Note for C5-C8 Aliphatics Adjusted value
Analysis Note for C9-Cl2 Aliphatics Adjusted value
One surrogate recovery was outside the control limits No target compounds were detected in
this sample No further action was taken
Sample Weight Determination
Weight
Weight
Sample Comments
BRL Below Reporting Limit
J-Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthose instances indicated in the case narrative and/or test comments
All results are reported on dry-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter
COC Group G0607589
Time Collected 06/20/07 1415
Time Submitted 06/20/07 1635
Sample Preparation
C9-C1 Aromatics
C9-C12 Aliphatics
Method Analysis Analyst
Batch
Date/Time ID
3050B 06/25/07 915 hoppel
5.8 1.8 MADEP VPH 06/28/07 150 hwagner
P18720
024604
024604
024604
Surrogate Recovery Control Limits
25-Dibromotoluene-PID 118 70-130
25-Dibromotoluene-FID 157 70-130
23.03
20.43
MADEP VPH 06/25/07 000 brown
MADEP VPH 06/25/07 000 Ibrown
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 28 of 35
Full Service Analytical
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Laboratory Report
06/29/07
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185085
G0607589
06/20/07 1430
06/20/07 1635
Percent Solids Determination
Percent Solids 85.2
Analyst Batch
ID
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method Analysis
Limit Factor Date/Time
06/27/07
06/27/07
06/27/07
000
000
000
brown
brown
brown
SM2540 06/25/07 1745 Lthao
Sample Weight Determination
Weight Bisulfate 5.34 5035
Weight Bisulfate 5.54 5035
Weight Methanol 5.39 5035
Volatile Organic Compounds by GC/MS
111-Trichioroethane BRL mg/kg 0.0053 0.0003 8260B
1122-Tetrachloroethane BRL mg/kg 00053 0.00054 8260B
112-Trichioroethane BRL mg/kg 0.0053 0.00033 8260B
11-Dichioroethane BRL mg/kg 0.0053 0.00038 8260B
11-Dichloroethene BRL mg/kg 0.0053 0.0004 8260B
11-Dichloropropene BRL mg/kg 0.0053 0.00047 8260B
123-Trichlorobenzene BRL mg/kg 0.0053 0.00058 8260B
23-Trichloropropane BRL mg/kg 0.0053 0.00047 8260B
l24-Trichlorobenzene BRL mg/kg 0.0053 0.00051 8260B
124-Trimethylbenzene BRL mg/kg 0.0053 0.0004 8260B
2-Dibromoethane EDB BRL mg/kg 0.0053 0.000095 8260B
12-Dichlorobenzene BRL mg/kg 0.0053 0.00029 8260B
12-Dichloroethane BRL mg/kg 0.0053 0.00053 8260B
12-Dichloropropane BRL mg/kg 0.0053 0.00039 8260B
135-Trimethylbenzene BRL mg/kg 0.0053 0.00044 8260B
13-Dichlorobenzene BRL mg/kg 0.0053 0.00046 8260B
3-Dichloropropane BRL mg/kg 0.0053 0.00036 8260B
14-Dichlorobenzene BRL mg/kg 0.0053 0.00041 8260B
22-Dichloropropane BRL mg/kg 0.0053 0.00026 8260B
2-Chlorotoluene BRL mg/kg 0.0053 0.00039 8260B
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
erussell
erussell
erusset
erussell
erussell
erussell
erussell
erusselt
erussell
erusselt
erusselt
erusselt
erusselt
erussell
erussell
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
06/27/07 354
024552
024552
024552
024552
024552
Q24552
024552
024552
Q24552
024552
Q24552
024552
024552
024552
024552
024552
Q24552
024552
024552
024552
erussell
erusseti
erussell
erussell
erussell
Page 29 of 35
Full Service Analytical Environmental SolutIons
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Attn Chris Ward
Box 7030
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Laboratory Report
06/29/07
B-I
185085
G0607589
06/20/07
06/20/07
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1430
1635
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
2-Hexanone BRL mg/kg 0.053 0.00055 826GB 06/27/07 354 erussell 024552
4-Chiorotoluene BRL mg/kg 0.0053 0.00028 826GB 06/27/07 354 erussefl 024552
4-Methyl-2-pentanone MIBK BRL mg/kg 0.053 0.00053 826GB 06/27/07 354 erussefi Q24552
Acetone BRL mg/kg 0.053 0.0021 826GB 06/27/07 354 erussell 024552
Benzene BRL mg/kg 0.0032 0.00042 826GB 06/27/07 354 erussell 024552
Bromobenzene BRL mg/kg 0.0053 0.00037 826GB 06/27/07 354 erussell 024552
Bromochioromethane BRL mg/kg 0.0053 0.00032 826GB 06/27/07 354 erussell 024552
Bromodichioromethane BRL mg/kg 0.0053 0.00047 826GB 06/27/07 354 erussell 024552
Bromoform BRL mg/kg 0.0053 0.00039 826GB 06/27/07 354 erussell 024552
Bromomethane BRL mg/kg 0.011 0.00061 826GB 06/27/07 354 erussell Q24552
Carbon tetrachloride BRL mg/kg 0.0053 0.00031 826GB 06/27/07 354 erusseH Q24552
Chlorobenzene BRL mg/kg 0.0053 0.0004 826GB 06/27/07 354 erussell Q24552
Chiorodibromomethane BRL mg/kg 0.0053 0.00036 826GB 06/27/07 354 erussell Q24552
Chloroethane BRL mg/kg 0.011 0.00043 826GB 06/27/07 354 erussell 024552
Chloroform BRL mg/kg 0.0053 0.00039 826GB 06/27/07 354 erussell 024552
Chloromethane BRL mg/kg 0.0053 0.00037 826GB 06/27/07 354 erussefl 024552
cis-12-Dichloroethene BRL mg/kg 0.0053 0.00023 826GB 06/27/07 354 erussell Q24552
cis-1 3-Dichioropropene BRL mg/kg 0.0053 0.00034 826GB 06/27/07 354 erussell 024552
Dichlorodifluoromethane BRL mg/kg 0.0053 0.0012 826GB 06/27/07 354 erussell 024552
Ethylbenzene BRL mg/kg 0.0053 0.00037 826GB 06/27/07 354 erussell 024552
Isopropyl ether IPE BRL mg/kg 0.0053 0.00018 826GB 06/27/07 354 erusseH 024552
lsopropylbenzene BRL mg/kg 0.0053 0.00042 826GB 06/27/07 354 erussell 024552
mp-Xylenes BRL mg/kg 0.011 0.00074 826GB 06/27/07 354 ewssell 024552
Methyl ethyl ketone MEK BRL mg/kg 0.11 0.GG15 826GB 06/27/07 354 erussell 024552
Methyl t-butyl ether MTBE BRL mg/kg 0.011 0.00031 826GB 06/27/07 354 erussell Q24552
Methylerie chloride BRL mg/kg 0.0053 G.GGG43 826GB 06/27/07 354 erussell 024552
n-Butylbenzene BRL mg/kg 0.0053 0.00042 826GB 06/27/07 354 erussell 024552
Page 30 of 35
Laboratory Report
06/29/07
B-IESPAssociatesPA
185085Attn Chris Ward
G0607589Box 7030
06/20/07CharlotteNC28241
06/20/07
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full Service Analytical Environmental Solutions
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1430
1635
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
n-Propylbenzene BRL mg/kg 0.0053 0.00032 8260B 06/27/07 354 erusset 024552
Naphthalene BRL mg/kg 0.011 0.00061 8260B 06/27/07 354 erussell Q24552
o-Xylene BRL mg/kg 0.0053 0.00032 8260B 06/27/07 354 erussell Q24552
p-lsopropyltoluene BRL mg/kg 0.0053 0.00043 8260B 06/27/07 354 erussell Q24552
sec-Butylbenzene BRL mg/kg 0.0053 0.00035 8260B 06/27/07 354 erussell 024552
Styrene BRL mg/kg 0.0053 0.00053 8260B 06/27/07 354 erussell 024552
tert-Butylbenzene BRL mg/kg 0.0053 0.00033 8260B 06/27/07 354 erussell 024552
Tetrachioroethene BRL mg/kg 0.0053 0.00091 8260B 06/27/07 354 erussell 024552
ToluØne BRL mg/kg 0.0053 0.00036 8260B 06/27/07 354 erussefl 024552
trans-i2-Dichloroethene BRL mg/kg 0.0053 0.0004 8260B 06/27/07 354 erussell 024552
trans-i 3-Dichloropropene BRL mg/kg 0.0053 0.00037 8260B 06/27/07 354 erussell 024552
Trichloroethene BRL mg/kg 0.0053 0.00032 8260B 06/27/07 354 erussell 024552
Trichlorofluoromethane BRL mg/kg 0.0053 0.00043 8260B 06/27/07 354 erussell Q24552
Vinyl acetate BRL mg/kg 0.026 0.0019 8260B 06/27/07 354 erusset 024552
Vinyl chloride BRL mg/kg 0.0053 0.00068 8260B 06/27/07 354 erussell Q24552
Surrogate Recovery Control Limits
Dibromofluoromethane 98 67 143
Bromofluorobenzene 104 77-128
Toluene-d8 96 81 128
Semi-volatile Organic Compounds by GC/MS
124-Trichlorobenzene BRL mg/kg 0.39 0.039 8270C 06/27/07 1919 kcampigotto 024556
12-Dichlorobenzene BRL mg/kg 0.39 0.029 8270C 06/27/07 1919 kcampigotto 024556
i3-Dichlorobenzene BRL mg/kg 0.39 0.028 8270C 06/27/07 1919 kcampigotto Q24556
14-Dichlorobenzene BRL mg/kg 0.39 0.035 8270C 06/27/07 1919 kcampigotto Q24556
245-Trichiorophenol BRL mg/kg 0.39 0.040 8270C 06/27/07 1919 kcampigotto 024556
246-TrichlorophenoI BRL mg/kg 0.39 0.038 8270C 06/27/07 1919 kcampigotto 024556
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone] Page 31 of 35
Full Service Analytical
Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
B-I
185085
G0607589
06/20/07 1430
06/20/07 1635
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
24-Dichlorophenol BRL mg/kg 0.39 0.033 827CC 06/27/07 1919 kcampigotto 024556
24-Dimethylphenol BRL mg/kg 0.39 0.038 827CC 06/27/07 1919 kcampigotto 024556
Dinltrophenol BRL mg/kg 044 827CC 06/27/07 19 19 kcampigotto 024556
24-Dinitrotoluene BRL mg/kg 0.39 0.022 827CC 06/27/07 1919 kcampigotto 024556
26-Dinitrotoluene BRL mg/kg 0.39 0.042 827CC 06/27/07 1919 kcampigotto Q24556
2-Chloronaphthalene BRL mg/kg 0.39 0.040 827CC 06/27/07 1919 kcampigotto Q24556
2-Chlorophenol BRL mg/kg 0.39 0.031 8270C 06/27/07 1919 kcampigotto 024556
2-Methylnaphthalene BRL mg/kg 0.39 0.031 827CC 06/27/07 1919 kcampigotto Q24556
2-Methylphenol BRL mg/kg 0.39 0.037 827CC 06/27/07 1919 kcampigotto 024556
2-Nitrophenol BRL mg/kg 0.39 0.047 827CC 06/27/07 1919 kcampigotto 024556
34-Methylphenol BRL mg/kg 0.39 0.040 827CC 06/27/07 1919 kcampigotto 024556
33-Dichlorobenzidine BRL mg/kg 0.78 0.024 827CC 06/27/07 1919 kcampigotto 024556
46-Dinitro-2-methylphenol BRL mg/kg 2.0 0.024 827CC 06/27/07 1919 kcampigotto Q24556
4-Bromophenylphenylether BRL mg/kg 0.39 0.037 827CC 06/27/07 1919 kcampigotto 024556
4-Chloro-3-methylphenol BRL mg/kg 0.78 0.029 827CC 06/27/07 1919 kcampigotto Q24556
4-Chioroaniline BRL mg/kg 0.39 0.050 827CC 06/27/07 1919 kcampigotto Q24556
4-Chlorophenylphenylether BRL mg/kg 0.39 0.024 8270C 06/27/07 1919 kcampigotto 024556
4-Nitrophenol BRL mg/kg 2.0 0.026 827CC 06/27/07 1919 kcampigotto 024555
Acenaphthene BRL mg/kg 0.39 0.038 827CC 06/27/07 1919 kcampigotto Q24556
Acenaphthylene BRL mg/kg 0.39 0.039 8270C 06/27/07 1919 kcampigotto 024556
Anthracene BRL mg/kg 0.39 0.030 827CC 06/27/07 1919 kcampigotto 024556
Azobenzene BRL mg/kg 2.0 0.036 827CC 06/27/07 1919 kcampigotto 024556
Benzoaanthracene BRL mg/kg 0.39 0.055 827CC 06/27/07 1919 kcampigotto Q24556
Benzoapyrene BRL mg/kg 0.39 0.045 827CC 06/27/07 1919 kcampigotto 024556
Benzobfluorantherie BRL mg/kg 0.39 0.018 827CC 06/27/07 1919 kcampgotto Q24556
BenzoghperyIene BRL mg/kg 0.39 0.019 827CC 06/27/07 1919 kcampigotto 024556
Benzokfluoranthene BRL mg/kg 0.39 0.032 8270C 06/27/07 1919 kcampigotto Q24556
Page 32 of 35
Full SeMoc Analytic3l Environmental Solutions
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Attn Chris Ward
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Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time CoHected
Time Submitted
B-I
185085
00607589
06/20/07 1430
06/20/07 1635
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Benzoic acid BRL mg/kg 2.0 0.17 8270C 06/27/07 1919 kcampigotto 024556
Benzyl alcohol BRL mg/kg 0.78 0.041 8270C 06/27/07 1919 kcampigotto 024556
Bis2-chloroethoxymethane BRL mg/kg 0.39 0.045 8270C 06/27/07 1919 kcampigotto 024556
Bis2-chloroethylether BRL mg/kg 0.39 0.042 8270C 06/27/07 1919 kcampigotto 024556
Bis2-chloroisopropylether BRL mg/kg 0.39 0.033 8270C 06/27/07 1919 kcampigotto Q24556
Bis2-ethylhexylphthafate BRL mg/kg 0.39 0.019 8270C 06/27/07 1919 kcampigotto 024556
Butylbenzylphthalate BRL mg/kg 0.39 0.024 8270C 06/27/07 1919 kcampigotto 024556
Chrysene BRL mg/kg 0.39 0.065 8270C 06/27/07 1919 kcampigotto 024556
Di-n-butylphthalate BRL mg/kg 0.39 0.018 8270C 06/27/07 1919 kcampigotto 024556
Di-n-octylphthalate BRL mg/kg 0.39 0.029 8270C 06/27/07 1919 kcampigotto 024556
Dibenzoahanthracene BRL mg/kg 0.39 0.039 8270C 06/27/07 1919 kcampigotto 024556
Diberizofuran BRL mg/kg 0.39 0.034 8270C 06/27/07 1919 kcampigotto 024556
Diethylphthalate BRL mg/kg 0.39 0.024 8270C 06/27/07 1919 kcampigotto 024556
Dimethylphthalate BRL mg/kg 0.39 0.027 8270C 06/27/07 1919 kcampigotto 024556
Fluoranthene BRL mg/kg 0.39 0.027 8270C 06/27/07 1919 kcampigotto 024556
Fluorene BRL mg/kg 0.39 0.023 8270C 06/27/07 1919 kcampigotto Q24556
Hexachlorobenzene BRL mg/kg 0.39 0.020 8270C 06/27/07 1919 kcampigotto Q24556
Hexachiorobutadiene BRL mg/kg 0.39 0.038 8270C 06/27/07 1919 kcampigotto 024556
Hexachiorocyclopentadiene BRL mg/kg 0.39 0.041 8270C 06/27/07 1919 kcampigotto 024556
Hexachloroethane BRL mg/kg 0.39 0.040 8270C 06/27/07 1919 kcampigotto 024556
Indeno123-cdpyrene BRL mg/kg 0.39 0.040 8270C 06/27/07 1919 kcampgotto 024556
lsophorone BRL mg/kg 0.39 0.035 8270C 06/27/07 1919 kcampigotto 024556
N-Nitrosodi-n-propylamine BRL mg/kg 0.39 0.044 8270C 06/27/07 1919 kcampigotto 024556
N-Nitrosodiphenylamine BRL mg/kg 0.39 0.020 8270C 06/27/07 1919 kcampigotto 024556
Naphthalene BRL mg/kg 0.39 0.043 8270C 06/27/07 1919 kcampigotto 024556
Nitrobenzene BRL mg/kg 0.39 0.038 8270C 06/27/07 1919 kcampigotto 024556
Pentachlorophenol BRL mg/kg 2.0 0.033 8270C 06/27/07 1919 kcampigotto 024556
Page 33 of 35
Full Service Analytical Environmental Solutions
ESP Associates PA
AUn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
B-I
185085
G0607589
06/20/07
06/20/07
Extractable Petroleum Hydrocarbons by GC-FID
Cli -C22 Aromatics
C19-C36 Aliphatics
C9-C18 Aliphatics
BRL mg/kg
BRL mg/kg
BRL mg/kg
Analysis Note for Cll-C22 Aromatics
Sample Preparation
7Metals by ICP
Chromium
Lead
Adjusted value
9.75g 2mL EPH
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil coc Group
Time Collected
Time Submitted
Parameter
Phenanthrene
Phenol
Pyrene
1430
1635
Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
BRL mg/kg 0.39 0.019 8270C 06/27/07 1919 kcampigotto 024556
BRL mg/kg 0.39 0.043 8270C 06/27/07 1919 kcampigotto 024556
BRL mg/kg 0.39 0.027 8270C 06/27/07 1919 kcampigotto 024556
Sample Preparation 29.67 mL 3550B 06/23/07 900 dpope P18716
Surrogate Recovery Control Limits
2-Fluorobiphenyl 94 21 108
Nitrobenzene-d5 67 14 103
Terphenyl-d14 107 41 136
246-Tribromophenol 99 25 123
2-Fluorophenol 80 14 89
Phenol-d5 89 13-95
12 6.5 MADEP EPH
12 1.8 MADEPEPH
12 3.9 MADEP EPH
06/27/07
06/27/07
06/27/07
1838 grappaccioli
1838 grappaccioli
1838 grappaccioli
024555
024555
024555
P1872406/25/07 1200 dpope
Surrogate Recovery Control Limits
1-Chloro-octadecane 114 40-140
2-Fluorobiphenyl 134 40 140
2-Bromonaphthalene 125 40 140
o-Terphenyl 108 40 140
120 mg/kg 0.26 0.016 6010B 06/25/07 2135 mcampbell Q24537
12 mg/kg 1.1 0.022 6010B 06/25/07 2135 mcampbell 024537
Page 34 of 35
FuI Servke AaIylicaI EwironmentalSoluUons
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil coc Group
Time Collected
Time Submitted
B-I
185085
G0607589
06/20/07 1430
06/20/07 1635
Parameter
Sample Preparation 2.22g 5OmL
Volatile Petroleum Hydrocarbons by GC-PIDIFID
C5-C8 Aliphatics BRL mg/kg
C9-C10 Aromatics BRL mg/kg 5.9 0.035 MADEP VPH 06/28/07 233 hwagner
C9-Cl2Aliphatics BRL mg/kg 5.9 1.8
MADEPVPH 06/28/07 233 hwagner
Analysis Note for C5-C8 Aliphatics Adjusted value
Analysis Note for C9-C12 Aliphatics Adjusted value
One surrogate recovery
was outside the control limits No target compounds were detected in
this sample No further action was taken
Surrogate Recovery Control Limits
25-Dibromotoluene-FID 135 70-130
25-Dibromotoluene-PID 96 70 130
SamDle Weight Determination
Weight
Weight
Sample Comments
BRL Below Reporting Limit
J-Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than
NELAC certification except for those instances indicated in the case narrative and/or test comments
All results are reported on thy-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
3050B 06/25/07 915 jhoppel P18720
5.9 1.1 MADEP VPH 06/28/07 233 hwagner 024604
024604
024604
20.69
22.23
MADEP VPH 06/25/07 000 brown
MADEP VPH 06/25/07 000 brown
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 35 of 35
SCCerflficaUonNo.99012
Level II QC Report
OTORlS NC Drinking Water Cert No 37735 6129/07
Fun Sevice Analytical Environmental Solutions
ESP Associates PA Project ID Morehead Commons No COC Group Number G0607589
Attn Chris Ward Date/Time Submitted 6/20/07 1635
Box 7030
Charlotte NC 28241
Metals by ICP method 6010B
Method Blank QC Batch
Result RL Control Limit Units JO
Chromium 0.0461 0.25 0.125 mg/kg Q24537
Lead 0.3158 0.25 0.125 mg/kg Q24537
Laboratory Control Sample Recovery Recovery
Ranges DC Batch
Result Spike Amount Units ID
Chromium 23.9028 25 mg/kg 96 80-1 20 Q24537
Lead 24.2285 25 mg/kg 97 80-1 20 Q24537
Matrix Spike Recovery Recovery
Ranges DC Batch
Sample ID Result Spike Amount Units U/ID
184958 Chromium 67.0763 21.834 mg/kg 162 75-125 Q24537
Lead 18.1186 21.834 mg/kg 64 75-125 Q24537
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range DC Batch
Sample ID Result Spike Amount Units
0/
ID
184958 Chromium 68.1398 24.752 mg/kg 147 75-125 0-20 Q24537
Lead 19.4685 24.752 mg/kg 62 75-125 0-20 Q24537
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
NC Certification No 402 Level II QC Re ortScCertificationNo99012
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Full Service Analytical Environmental Solutions
ESP Associates PA Project ID Morehead Commons No COO Group Number G0607589
Attn Chris Ward Date/Time Submitted 6/20/07 1635
Box 7030
Charlotte NC 28241
VtsIviihn Arravanir rsmnsnnrho hs IM thhn1 RflR
Method Blank QC Batch
Result RI Control Limit Units tO
11 1-TriChloroethane ND 0.005 0.0025 mg/kg Q24552
11 22-Tetrachloroethane ND 0.005 0.0025 mg/kg Q24552
112-Trichloroethane ND 0.005 0.0025 mg/kg Q24552
1-Dichloroethane ND 0.005 0.0025 mg/kg Q24552
1-Dichloroethene ND 0.005 0.0025 mg/kg 024552
11-Dichioropropene ND 0.005 0.0025 mg/kg 024552
23-Trichlorobenzene ND 0.005 0.0025 mg/kg 024552
23-Trichloropropane ND 0.005 0.0025 mg/kg 024552
24-Trichlorobenzene ND 0.005 0.0025 mg/kg 024552
24-Trimethylbenzerie ND 0.005 0.0025 mg/kg Q24552
2-Dibromoethane EDB ND 0.005 0.0025 mg/kg 024552
2-Dichlorobenzene ND 0.005 0.0025 mg/kg 024552
2-Dichloroethane ND 0.005 0.0025 mg/kg 024552
2-Dichloropropane ND 0.005 0.0025 mg/kg 024552
35-Trimethylbenzerie ND 0.005 0.0025 mg/kg 024552
3-Dichlorobenzene ND 0.005 0.0025 mg/kg 024552
3-Dichloropropane ND 0.005 0.0025 mg/kg 024552
4-Dichlorobenzene ND 0.005 0.0025 mg/kg 024552
22-Dichioropropane ND 0.005 0.0025 mg/kg 024552
2-Chlorotoluene ND 0.005 0.0025 mg/kg 024552
2-Hexanone ND 0.05 0.025 mg/kg 024552
4-Chiorotoluene ND 0.005 0.0025 mg/kg 024552
4-Methyl-2-pentanone MIBK ND 0.05 0.025 mg/kg Q24552
Acetone ND 0.05 0.025 mg/kg 024552
Benzene ND 0.003 0.0015 mg/kg 024552
Bromobenzene ND 0.005 0.0025 mg/kg 024552
Bromochioromethane ND 0.005 0.0025 mg/kg Q24552
Bromodichioromethane ND 0.005 0.0025 mg/kg Q24552
Bromoform ND 0.005 0.0025 mg/kg 024552
Bromomethane ND 0.01 0.005 mg/kg 024552
Carbon tetrachioride ND 0.005 0.0025 mg/kg 024552
Chlorobenzene ND 0.005 0.0025 mg/kg 024552
Chiorodibromomethane ND 0.005 0.0025 mg/kg 024552
Chioroethane ND 0.01 0.005 mg/kg 024552
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
SC Certification No 99012
Level II QC Report
INC NC Drinktng Water Cert No 37735 6/29/07
FuH Service Analytical Environmental Solutions
ESP Associates PA Project ID Morehead Commons No COG Group Number 00607589
Attn Chris Ward Date/Time Submitted 6/20/07 1635
Box 7030
Charlotte NC 28241
Method Blank QC Batch
Result RL Control Umit Units ID
Chloroform ND 0005 0.0025 mg/kg 024552
Chioromethane ND 0.005 0.0025 mg/kg 024552
cis-1 2-Dichloroethene ND 0.005 0.0025 mg/kg Q24552
cis-1 3-Dichloropropene ND 0.005 0.0025 mg/kg 024552
Dichlorodifluoromethane ND 0.005 0.0025 mg/kg Q24552
Ethylbenzene ND 0.005 0.0025 mg/kg 024552
Isopropyl ether IPE ND 0.005 0.0025 mg/kg Q24552
lsopropylbenzene ND 0.005 0.0025 mg/kg 024552
mp-Xylenes ND 0.01 0.005 mg/kg Q24552
Methyl ethyl ketone MEK ND 0.1 0.05 mg/kg 024552
Methyl t-butyl ether MTBE ND 0.01 0.005 mg/kg 024552
Methylene chloride ND 0.005 0.0025 mg/kg 024552
n-Butylbenzene ND 0.005 0.0025 mg/kg 024552
n-Propylbenzene ND 0.005 0.0025 mg/kg Q24552
Naphthalene ND 0.01 0.005 mg/kg 024552
o-Xylene ND 0.005 0.0025 mg/kg Q24552
p-lsopropyltoluene ND 0.005 0.0025 mg/kg Q24552
sec-Butylbenzene ND 0.005 0.0025 mg/kg 024552
Styrene ND 0.005 0.0025 mg/kg 024552
tert-Butylbenzene ND 0.005 0.0025 mg/kg 024552
Tetrachloroethene ND 0.005 0.0025 mg/kg 024552
Toluene ND 0.005 0.0025 mg/kg 024552
trans-i 2-Dichloroethene ND 0.005 0.0025 mg/kg Q24552
trans-13-Dichloropropene ND 0.005 0.0025 mg/kg 024552
Trichloroethene ND 0.005 0.0025 mg/kg 024552
Trichlorofluoromethane ND 0.005 0.0025 mg/kg Q24552
Vinyl acetate ND 0.025 0.01 25 mg/kg Q24552
Vinyl chloride ND 0.005 0.0025 mg/kg 024552
Laboratory Control Sample Recovery Recovery OC Batch
Result Spike Amount Units ID
11-Dichloroethene 0.03808 0.05 mg/kg 76 57-122 024552
Benzene 0.04358 0.05 mg/kg 87 62-119 024552
Chlorobenzene 0.04441 0.05 mg/kg 89 61-1 24 Q24552
Toluene 0.04544 0.05 mg/kg 91 57-1 22 Q24552
Trichloroethene 0.04951 0.05 mg/kg 99 59-129 024552
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 282240543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone] Page of
Full Service Analytical Environmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
6/29/0
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No COG Group Number G0607589
Date/Time Submitted 6/20/07 1635
Recovery Recovery
RangesUnits
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Matrix Spike Recovery Recovry OC Batch
Sample ID Result Spike Amount Units ID
185081 11-Dichloroethene 0.03118 0.05 mg/kg 62 44-140 Q24552
Benzene 0.03306 0.05 mg/kg 66 46-136 Q24552
Chlorobenzene 0.02555 0.05 mg/kg 51 47-135 Q24552
Toluene 0.0296 0.05 mg/kg 59 47-1 36 024552
Trichloroethene 0.03367 0.05 mg/kg 67 45-1 41 024552
Matrix Spike Duplicate Recovery Recovery RPD Fe QC Batch
Sample ID Result Spike Amount Units ID
185081 11-Dichloroethene 0.03223 0.05 mg/kg 64 44-140 -23 Q24552
Benzene 0.03495 0.05 mg/kg 70 46-136 0-22 024552
Chlorobenzene 0.03 0.05 mg/kg 60 47-135 16 -22 Q24552
Toluene 0.03187 0.05 mg/kg 64 47-1 36 0-22 024552
Trichloroethene 0.03627 0.05 mg/kg 73 45-141 23 024552
Extractable Petroleum Hydrocarbons by GC-FID method MADEP EPH
Method Blank
oc Batch
Result RL control Limit Units ID
Cl 1-C22 Aromatics ND 10 mg/kg 024555
C19-C36Aliphatics ND 10 mg/kg 024555
C9-Cl8Aliphatics ND 10 mg/kg Q24555
Laboratory Control Sample Recovery Recovery
Ranges SCResultSpikeAmountUnitsID
C11-C22Aromatics 15938 170 mg/kg 94 40-140 Q24555
C19-C36Aliphatics 70.52 80 mg/kg 88 40-140 024555
C9-C18 Aliphatics 44.82 60 mg/kg 75 40-1 40 024555
Matrix Spike
Sample ID Result Spike Amount QC Batch
ID
185126 Cl 1-C22 Aromatics 147.84 170 mg/kg 87 40-1 40 Q24555
C19-C36 Aliphatics 66.68 80 mg/kg 83 40-1 40 024555
C9-C18 Aliphatics 37.94 60 mg/kg 63 40-140 Q24555
Matrix Spike Duplicate Recovery Recovery RPD Range QC BatchSampleIDResultSpikeAmountUnits10
185126 C11-C22 Aromatics 145.68 170 mg/kg 86 40-140 0-50 024555
C19-C36 Aliphatics 70.64 80 mg/kg 88 40-140 0-50 024555
C9-C18 Aliphatics 44.58 60 mg/kg 74 40-1 40 16 0-50 024555
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Level II QC Report
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24-Trichlorobenzene
2-Dichlorobenzene
3-Dichlorobenzene
4-Dichlorobenzene
245-Trichiorophenol
246Trichlorophenol
24-Dichlorophenol
24-Dimethyiphenol
24-Dinitrophenol
24-Dinitrotoluene
26-Dinitrotoluerie
2-Chloronaphthalene
2-Chiorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitrophenol
34-Methylphenol
33-Dichlorobenzidjne
46-Dinitro-2-methylphenol
4-Bromophenyiphenylether
4-Chloro-3-methylphenol
4-Chloroanilirie
4-Chlorophenylphenylether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzoaanthracene
Benzoapyrene
Benzobfluoranthene
Benzoghiperylene
Benzokfluoranthene
Benzoic acid
Project ID Morehead Commons No COC Group Number G0607589
Date/Time Submitted 6/20/07 1635
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Semi-volatile ----7fll1L1tJIIStijiiiinjtiiitioLIVasIVICIIICLIILIU
Method Blank oc Batch
Result RL Control Limit Units ID
ND 0.33 0.165 mg/kg 024556
ND 0.33 0.165 mg/kg 024556
ND 0.33 0.165 mg/kg 024556
ND 0.33 0.165 mg/kg 024556
ND 0.33 0.165 mg/kg Q24556
ND 0.33 0.165 mg/kg Q24556
ND 0.33 0.165 mg/kg 024556
ND 0.33 0.165 mg/kg Q24556
ND 1.65 0.825 mg/kg Q24556
ND 0.33 0.165 mg/kg Q24556
ND 0.33 0.165 mg/kg 024556
ND 0.33 0.165 mg/kg 024556
ND 0.33 0.165 mg/kg 024556
ND 0.33 0.165 mg/kg 024556
ND 0.33 0.165 mg/kg 024556
ND 0.33 0.165 mg/kg 024556
ND 0.33 0.165 mg/kg 024556
ND 0.66 0.33 mg/kg 024556
ND 1.65 0.825 mg/kg 024556
ND 0.33 0.165 mg/kg 024556
ND 0.66 0.33 mg/kg Q24556
ND 0.33 0.165 mg/kg 024556
ND 0.33 0.165 mg/kg 024556
ND 1.65 0.825 mg/kg 024556
ND 0.33 0.165 mg/kg 024556
ND 0.33 0.165 mg/kg 024556
ND 0.33 0.165 mg/kg 024556
ND 1.65 0.825 mg/kg 024556
ND 0.33 0.165 mg/kg 024556
ND 0.33 0.165 mg/kg Q24556
ND 0.33 0.165 mg/kg 024556
ND 0.33 0.165 mg/kg Q24556
ND 0.33 0.165 mg/kg 024556
ND 1.65 0.825 mg/kg 024556
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ESP Associates PA
Attn Chris Ward
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24-Dinitrotoluene
2-Chlorophenol
4-Chloro-3-methylphenol
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
In $ervice Analytical Environmental Solutions
Level II QC Report
6/29/07
Project ID Morehead Commons No COC Group Number G0607589
Date/Time Submitted 6/20/07 1635
Method Blank QC Batch
Result RL Control Limit Units ID
Benzyl alcohol ND 0.66 0.33 mg/kg 024556
Bis2-chloroethoxymethane ND 0.33 0.165 mg/kg 024556
Bis2-chloroethylether ND 0.33 0.165 mg/kg Q24556
Bis2-chloroisopropylether ND 0.33 0.165 mg/kg Q24556
Bis2-ethylhexylphthalate ND 0.33 0.165 mg/kg Q24556
Butylbenzylphthalate ND 0.33 0.165 mg/kg 024556
Chrysene ND 0.33 0.165 mg/kg 024556
Di-n-butylphthalate ND 0.33 0.165 mg/kg 024556
Di-n-octylphthalate ND 0.33 0.165 mg/kg 024556
Dibenzoahanthracene ND 0.33 0.165 mg/kg 024556
Dibenzofuran ND 0.33 0.165 mg/kg 024556
Diethylphthalate ND 0.33 0.165 mg/kg Q24556
Dimethylphthalate ND 0.33 0.165 mg/kg 024556
Fluoranthene ND 0.33 0.165 mg/kg Q24556
Fluorene ND 0.33 0.165 mg/kg Q24556
Hexachlorobenzene ND 0.33 0.165 mg/kg 024556
Hexachiorobutadjene ND 0.33 0.165 mg/kg 024556
Hexachiorocyclopentadiene ND 0.33 0.165 mg/kg 024556
Hexachioroethane ND 0.33 0.165 mg/kg 024556
lndeno123-cdpyrene ND 0.33 0.165 mg/kg 024556
Isophorone ND 0.33 0.165 mg/kg 024556
N-Nitrosodi-n-propylamine ND 0.33 0.165 mg/kg 024556
N-Nitrosodiphenylamine ND 0.33 0.165 mg/kg 024556
Naphthalene ND 0.33 0.165 mg/kg 024556
Nitrobenzene ND 0.33 0.165 mg/kg 024556
Pentachiorophenol ND 1.65 0.825 mg/kg 024556
Phenanthrene ND 0.33 0.165 mg/kg 024556
Phenol ND 0.33 0.165 mg/kg 024556
Pyrene ND 0.33 0.165 mg/kg 024556
Laboratory Control Sample Recovery Recovery BChResultSpikeAmountUnits
n/n
ID
24-Trichlorobenzene
4-Dichlorobenzene
146143 1.6697 mg/kg 88 39-98 024556
1.21969 1.6697 mg/kg 73 3795 024556
1.65308 1.6697 mg/kg 99 56-128 024556
1.23973 1.6697 mg/kg 74 37-98 024556
1.59666 1.6697 mg/kg 96 45-111 024556
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
NC Certification No 402tR1SMSCCertificationNo99012
leArnmlEsieo NC Drinking Water Cert No 37735
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 282240543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
Level II QC Report
6/29/07
Project ID Morehead Commons No COG Group Number G0607589
Date/Time Submitted 6/20/07 1635
Laboratory Control Sample Recovery Recovery
Ranges QC Batch
Result Spike Amount Units ID
4-Nitrophenol 1.60500 1.6697 mg/kg 96 20-157 Q24556
Acenaphthene 1.53355 1.6697 mg/kg 92 44-110 024556
N-Nitrosodi-n-propylamine 1.48113 1.6697 mg/kg 89 38-101 Q24556
Pentachlorophenol 1.64674 1.6697 mg/kg 99 53-1 27 024556
Phenol 1.32821 1.6697 mg/kg 80 34-102 Q24556
Pyrene 1.67278 1.6697 mg/kg 100 54-131 Q24556
Matrix Spike Recovery Recovery
Ranges QC Batch
IDSampleIDResultSpikeAmountUnits
185039 24-Trichlorobenzene 1.34494 1.6587 mg/kg 81 26-97 024556
4-Dichlorobenzene 1.24245 1.6587 mg/kg 75 23-92 024556
24-Dinitrotoluene 1.90679 1.6587 mg/kg 115 45-127 Q24556
2-Chlorophenol 1.23150 1.6587 mg/kg 74 25-94 024556
4-Chloro-3-methylphenol 1.32338 1.6587 mg/kg 80 31-113 Q24556
4-Nitrophenol 1.55257 1.6587 mg/kg 94 17-150 Q24556
Acenaphthene 1.60398 1.6587 mg/kg 97 36-107 Q24556
N-Nitrosodi-n-propylamine 1.45140 1.6587 mg/kg 88 22-1 05 024556
Pentachlorophenol 1.64046 1.6587 mg/kg 99 39-137 024556
Phenol 1.31840 1.6587 mg/kg 79 23-97 Q24556
Pyrene 1.53698 1.6587 mg/kg 93 45-133 Q24556
Recovery Recovery RPD
Result SpikeAmount Units Ranges RPD Range QCBatch
ID
Matrix Spike Duplicate
Sample ID
185039 24-Trichlorobenzene
4-Dichlorobenzene
24-Dinitrotoluene
2-Chlorophenol
4-Chloro-3-methylphenol
4-Nitrophenol
Acenaphthene
N-Nitrosodi-n-propylamine
Pentachlorophenol
1.24221
1.24817
1.88005
1.21172
1.38933
1.72001
1.61729
1.36315
1.80351
1.27269
1.60371
1.6570
1.6570
1.6570
1.6570
1.6570
1.6570
1.6570
1.6570
1.6570
1.6570
1.6570
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
75
75
113
73
84
104
98
82
109
77
97
Phenol
Pyrene
26-97
23-92
45-127
25-94
31-113
17-1 50
36-1 07
22-105
39-137
23-97
45-1 33
0-37
0-36
0-29
0-37
0-32
10 0-32
0-32
0-37
0-27
0-42
0-27
Q24556
024556
024556
024556
024556
024556
Q24556
024556
024556
Q24556
024556
Page of
FuD Service Analylica Environmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
6/29/07
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Project ID Morehead Commons No COC Group Number G0607589
Date/Time Submitted 6/20/07 1635
Volatile Petroleum Hvdrocarbons by GC-PID/FID method MADEP VPH
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
Method Blank
ctc Batch
Result RL Control Limit Units ID
C5-C8 Aliphatics ND 2.5 mg/kg 024604
C9-C10 Aromatics ND 2.5 mg/kg 024604
C9-C12 Aliphatics ND 2.5 mg/kg 024604
Laboratory Control Sample Recovery Recovery QC BatchRangesResultSpikeAmountUnitsID
C5-C8 Aliphatics 16.779 15 mg/kg 112 70-130 Q24604
C9-C10 Aromatics 4.305 mg/kg 86 70-130 Q24604
C9-C12 Aliphatics 10.922 10 mg/kg 109 70-130 024604
Matrix Spike Recovery Recovery
Ranges QC Batch
Sample ID Result Spike Amount Units ID
184956 C5-C8 Aliphatics
C9-C1 Aromatics
C9-C12 Aliphatics
Matrix Spike Duplicate
Sample ID
184956 C5-C8 Aliphatics
C9-C10 Aromatics
C9-C12 Aliphatics
-See Case Narrative
16.625 15 mg/kg 111
4.148 mg/kg 83
12.627 10 mg/kg 126
Recovery
Result Spike Amount Units /n
17.936
4.279
13.613
024604
024604
Q24604
70-130
70-1 30
70-130
Recovery
Ranges
70-1 30
70-1 30
70-130
15
10
mg/kg
mg/kg
mg/kg
120
86
136
QcBatch
ID
RPDRPDRange___%
0-25
0-25
0-25
024604
024604
024604
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Email Yes No Email Address_____________________
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please ATTACH any project specific reporting QC LEVEL 111111 IV
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Requested Due Date Day Days Days Days
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Working Days 6-9 Days Standard 10 days US Work
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Samples received after 1500 will be processed next business day
Turnaround time is based on business days excluding weekends and holidays
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Certification NELAC USACE FL _____NC
SC_OTHER _____N/A _____
Water Chlorinated YES_NO_
Sample Iced Upon Collection YES VNO
SAMPLE DESCRIPTION
CLIENT
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tjS-2
COLLECTEDDATE
zto
TIME
MILITARY
COLLECTED
HOURS
LLO
MATRIX
WATER OR
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SAMPLE CONTAINER
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ANALY QUESTED
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SEE BELOW NO SIZE
Jvo 1iT5-1g-//4//c
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above Any changes must besubmittedinwritingtothePrismProjectManagerTherewillbechargesforanychangesafteranalyseshave been initialized
Received By Signature uaie
Relinquished By Signature Received By Signature Date
Relinquished ignature Re ived For Prism Laboratories By4_Met o_iflent .4OTEJ...LL SAMPLE COOLERS SHOULD BE TAPED SHIT WIT CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY
SAILES ARE NOT ACCEPTED
AND VERIFIED AGAINST..9C UNTIL RECEIVED AT THE LABORATORY
Fed Ex UPS and-delivered Prism Field Service Other
Date/2O7 /95
OC Group No
MuItary/I-iours Additional Comments
NPDES GROUNDWATER DRINKING WATER SOLID WASTE RCRA CERCLA LANDFILL OTHERNCSCNCSCNCSCNC SC NC SC NC SC NC SC NC SC NC SC
fl El _________ ___
Site Arrival Time
Site Departure Time
Field Tech Fee
Mileage
SEE REVERSE
FORTERMSCONOITIONS
Au
Fufl Service Analyticat Envircnmentaj Solutions
CLIENT SP 4s14
A1TN C1iri
PRISM COG GROUP
Please fill in the Site Location information on the attached VPH and/or EPH Forms
\NaSO1\FOLD\COMM0N\F0RMS\VPH EPH Site Location for Client.doc
VPH AliphaticslAromatics Laboratory Reporting Form
Client Name
Project Name
Site Location
ESP Associates PA
Morehead Commons No
Laboratory Name
NC Certification Lab
Sample Matrix
Prism Laboratories Inc
Blank C5-C8 Aliphatics
C9-C12 Aliphatics
C9-C10 Aromatics
RL C5-C8 Aliphàtics
C9-C12 Aliphatics
C9-C10 Aromatics
MDL C5-C8 Aliphatics
C9-C12 Aliphatics
C9-C10 Aromatics
Comments VPH trip blank was not submitted to the laboratory
Result outside of the QC limits
Sample Information and Analytical Results
Method for Ranges MADEP VPH
Si irrn ate Standards Aliphatic 25-Dibromotoluene Aromatic 25-Dibromotoluene
Collection Option for soil
402
Soil
Date Collected
Date Received
Date Extracted
ti
Date Analyzed
Dry Solids
Dilution Factor
185085
Hydrocarbon Rancies in mci/kci
C5-C8 Aliphatics
C9-C12 Aliohatics
C9-C10 Aromatics
6/20/2007 6/20/2007 6/20/2007 6/20/2007 6/20/2007
6/20/2007 6/20/2007 6/20/2007 6/20/2007 6/20/2007
6/27/2007 6/28/2007 6/28/2007 6/28/2007 6/28/2007
6/27/2007 6/28/2007 6/28/2007 6/28/2007 6/28/2007
81.9 80.1 83.9 85.7 85.2
Sample Results Sample Results Sample Results Sample Results Sample Results
6.1 6.2 6.0 5.8 5.9
6.1 6.2 6.0 5.8 5.9
6.1 6.2 6.0 5.8 5.9
5.0 5.0 5.0 5.0 5.0
5.0 5.0 5.0 5.0 5.0
5.0 5.0 5.0 5.0 5.0
6.1 6.2 6.0 5.8 5.9
6.1 6.2 6.0 5.8 5.9
6.1 6.2 6.0 5.8 5.9
1.2 1.2 1.1 1.1 1.1
1.9 1.9 1.8 1.8 1.8
0.037 0.037 0.036 0.035 0.035
Surroqate AcceDtance Rancie Blank 70-130% 70-130%70-130 70-1 30 70-1 30
AliphaticSurrogate%Rec.-FID 130 111 119 112 157 135
Aromatic Surrogate Rec PlO 97 79 84 79 118 96
Option Established flIl line on vial
Option Sampling device indicate brand e.g EnCore TM
Option Field weight of soil
Unadjusted value should exclude the concentration of any surrogates internal standards and/or
concentrations of other ranges that elute within the specified range
Adjusted value
MDL Method Detection Limit RL Reporting Limit Blank Laboratory Method Blank or Trip Blank
whichever is higher indicate typeWereallperformance/acceptance standards for required QNQC
procedures achieved YES No Details Attached
Were any significant modifications to the VPH method made NO Yes Details Attached
Page of VPH Soil
EPH Aliphatics/Aromatics Laboratory Reporting Form
Client Name
Project Name
Site Location
ESP Associates PA
Morehead Commons No
Laboratory Name
NC Certification Lab
Sample Matrix
Prism Laboratories Inc
402
Soil
5ample Identification
Date Collected
Date Received
Date Extracted
Date Analyzed
Dry Solids
Dilution Factor _____
Hydrocarbon Ranges in mg/kg
C9-C18 Aliphatics
C19-C36 Aliphatics
Cll-C22 Aromatics
Blank C9-C1 Aliphatics
Cl 9-C36 Aliphatics
________Cl l-C22 Aromatics
RL C9-C18 Aliphatics
Cl 9-C36 Aliphatics
________C1l-C22 Aromatics
MDL C9-C18 Aliphatics
Cl 9-C36 Aliphatics
_________Cl l-C22 Aromatics
Surrogate Acceptance Range
Sample Information and Analytical Results
Method for Ranges MAIDEP EPH
EPH Surrogate Standards Aliphatic 1-Chloro-octadecane Aromatic o-Terphenyl
EPH Fractionation Surrogates ne Fluorobiphenvl
185082
6/20/2007
185083 185084 185085
6/20/2007 6/20/2007 6/20/2007
ii
6/20/2007 6/20/2007 6/20/2007 6/20/2007 6/20/2007
6/2512007 6/25/2007 6/25/2007 6/25/2007 6/25/2007
6/27/2007 6/27/2007 6/27/2007 6/27/2007 6/27/2007
81.9 80.1 83.9 85.7 85.2
Sample Results Sample Results Sample Results Sample Results Sample Results
12 13 12 12 12
12 13 IIJ 12 12
12 20 52 12 12
10 10 10 10 10
10 10 10 10 10
10 10 10 10 10
12 13 12 12 12
12 13 12 12 12
12 13 12 12 12
3.8 4.1 3.7 3.7 3.9
1.8 1.9 1.8 1.7 1.8
6.4 6.9 6.3 6.3 6.5
Blank 40-140%40-140% 40-140% 40-140%40-140%
AliphaticSurrogate%Rec 104 107 106 151 103 114
Aromatic Surrogate Rec 87 93 88 113 91 108
Fractionation Surrogate Accep Range Blank 40-140 40-140 40-140 40-140 40-140
Frac.Surrogate1 %Rec 90 128 91 132 103 125
Frac.Surrogate2%Rec 95 134 92 135 107 134
Unadjusted value should exclude the concentration of any surrogates internal standards and/or
concentrations of other ranges that elute within the specified range
Adjusted value
MDL Method Detection Limit RL Reporting Limit Blank Laboratory Method Blank
Were all performance/acceptance standards for required QAIQC
procedures achieved
Was blank correction applied as significant modification of the method
Were any significant modifications to the EPH method made
Comments
YES No Details Attached
Yes NO
NO Yes Details Attached
The analyte was positively identified but the value is estimated
below the reporting limit
Result outside of the QC limits
Pate of EPH Soil
JUL 27 ZOO
07123107 Client Project ID Morehead Commons No
ESP Associates PA Prism COC Group No G0607587
Chris Ward Collection Dates 06/20/07
Box 7030 Lab Submittal Dates 06/20/07
Charlotte NC 28241
This is revised report and supersedes our original laboratory report dated 06/29/07 Lead was added to all samples
This data package contains the analytical results for the project identified above and includes Case Narrative Laboratory Report
and Quality
Control Data totaling pages chain-of-custody is also attached for the samples submitted to Prism for this project
Data qualifiers are flagged individually on each sample key reference for the data qualifiers appears at the end of this case narrative Quality
control statements and/or sample specific remarks are included in the sample comments section of the laboratory report for each sample
affected
Semi Volatile Analysis
No Anomalies Reported
Volatile Analysis
No Anomalies Reported
Metals Analysis
Analysis Note for Q25161 MS Lead Matiix interference is suspected Post-digestion spike recovery 70%is outside the
acceptance limits 75-125%
Analysis Note for Q251 61 MSD Lead RPD value outside the control limits Digestion was repeated with similar results
Wet Lab and Micro Analysis
N/A
Please call if you have any questions relating to this analyUcal report
Date Reviewed by Paula Gilleland
Signature CAcL Jci klk__________________________
Review Date 07/23/07
Data Qualifiers Key Reference
Compound also detected in the method blank
Result outside of the QC limits
DO Compound diluted out
Estimated concentration calibration range exceeded
The analyte was positively identified but the value is estimated below the reporting limit
Estimated concentration with high bias
Estimated concentration with low bias
matrix effect is present
Notes This report should not be reproduced except in its enfirety without the writtten consent of Prism Laboratories Inc The results in this
report relate only to the samples submitted for analysis
449 Spdng brook Road P.O Box 240543 chadone NC 28224-0403
Phone [phone] Toll Free 800/529-6364 Fax [phone]
PRISM
LAB ORATORESINC
Date
Company
Contact
Address
Case Narrative Revised
Project Manager
Signature
Approval Date
PngeIa Dash
07/23/07
Laboratory Report
07/23/07
Project ID Morehead Commons No Client Sample ID 1A-l23 COMP
Prism Sample ID 185077
Sample Matrix Soil COC Group G0607587
Time Collected 06/20/07 1040
Time Submitted 06/20/07 1635
Result Units Report
Limit
87.4
MDL Dilution Method
Factor
iesel Range Organics DRO by GC-FID
biesei Range Organics DRO
Sample Preparation
Surrogate Recovery Control Limits
Toluene-d8 93 81 128
Dibromofluoromethane 93 67-143
Bromofluorobenzene 107 77-128
370 mg/kg 40 5.0 8015B 06/27/07 1428 jvogel Q24575
25.36 mL 3545 06/25/07 1515 weonder P18738
asoline Range Organ ics IGRO by GC-FID
asoline Range Organics GRO BRL
Surrogate Recovery Control Limits
o-Terphenyl 49 124
mg/kg 1.1 0.073 8015B 06/27/07 441 hwagner Q24580
etals bjf
Lead 15 mg/kg 0.28 0.018
This report should not be reproduced except in its entirety without the wiitten consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ull Service Analytical Environmental Solutions
ESP Associates PA
\ttn Chris Ward
Box 7030
Charlotte NC 28241
2arameter Analysis
Date/Time
Analyst Batch
ID
ercent Solids Determination
ercent Solids SM2540 06/27/07 1800 Lthao
folatile Organic Compounds by GC/MS
Benzene BRL pg/kg 3.4 0.51 826GB 06/27/07 806 erusseu 024552
EthyIbenzene BRL pg/kg 5.7 0.44 8260B 06/27/07 806 erussell Q24552
.np-Xylenes BRL pg/kg 11 0.88 826GB 06/27/07 806 erusselt 024552
t-Xylene BRL pg/kg 5.7 0.38 826GB 06/27/07 806 erussetl Q24552
oluene BRL pg/kg 5.7 0.43 826GB 06/27/07 806 erussetl 024552
Surrogate
aaa-TFT
Recovery Control Limits
85 55-129
601GB 07/19/07 2236 mcampbell 025161
Page of4
PRISM SC Cerilficaflon No 99012 Laboratory Report
tBQ NC Drinking Water Cert No 37735 07/23/07
ult Service Analytical Environmental Sotubons
ESP Associates PA Project ID Morehead Commons No Client Sample ID 1A-123 COMP
\ttn Chris Ward Prism Sample ID 185077
Box 7030 Sample Matrix Soil COG Group G0607587
Charlotte NC 28241 Time Collected 06/20/07 1040
Time Submitted 06/20/07 1635
arameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Sample Preparation 2.01 50 mL 3050B 07/19/07 715 jhoppel P18933
Comments
BRL Below Reporting Limit
.J-Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanNECcertificationexceptforthose instances indicated in the case narrative and/or test comments
All results are reported on thy-weight basis
iAngela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone] Page of
SCCerflcaUonNo.99O12 Laboratory Report
NC Drinking Water Cert No 37735 07/23/07
rult Service Analytical Environmental Solutions
ESP Associates PA Project ID Morehead Commons No Client Sample ID 1B-234 COMP
Aitn Chris Ward Prism Sample ID 185078
Box 7030 Sample Matrix Soil COC Group G0607587
Charlotte NC 28241 Time Collected 06/20/07 1055
Time Submitted 06/20/07 1635
Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Percent Solids Determination
Percent Solids 88.1 SM2540 06127/07 1800 Lthao
volatile Organic Compounds by GC/MS
Benzene BRL pg/kg 3.4 0.50 8260B 06/27/07 837 erussell 024552
thyIbenzene BRL pg/kg 5.7 0.44 8260B 06/27/07 837 erussell Q24552
rnp-Xylenes BRL pg/kg 11 0.88 82608 06/27/07 837 erusselt Q24552
o-Xylene BRL pg/kg 5.7 0.38 8260B 06/27/07 837 erussell 024552
roluene BRL pg/kg 5.7 0.43 8260B 06/27/07 837 erussell 024552
Surrogate Recovery Control Limits
Toluene-d8 94 81 128
Dibromofluoromethane 92 67-143
Bromofluorobenzene 104 77-128
Diesel Range Orcianics DRO by GC-FID
Diesel Range Organics DRO 140 mg/kg 7.9 0.99 80158 06/27/07 330 Jvogel 024575
Sample Preparation 25.12 mL 3545 06/25/07 1515 wconder P18738
Surrogate Recovery Control Limits
o-Terphenyl 77 49-124
Oasoline Range Organ ics GRO by GC-FID
3asoline Range Organics GRO BRL mg/kg 1.1 0.072 80158 06/27/07 512 hwagner 024580
Surrogate Recovery Control Limits
aaa-TFT 89 55-129
Ietals by ICP
Lead 13 mg/kg 0.28 0.018 601DB 07/19/07 2302 mcampbell 025161
This report should not be reproduced except in its entirety without the wiitten consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Result Units Report
Limit
Sample Preparation 2.02 50 mL 3050B 07/19/07 715 jhoppel P18933
Comments
BRL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanVELACcertificationexceptforthose instances indicated in the case narrative and/or test comments
All results are reported on dry-weight basis
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
is
ull Service Analytical Environmental Solutions
ESP Associates PA
ttn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
07/23/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
arameter
B-234 COMP
185078
G0607587
06/20/07 1055
06/20/07 1635
MDL Dilution Method Analysis Analyst
Batch
Factor Date/Time ID
Angela Overcash V.P Laborato SeMces
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
Full Service Analytical Environmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
7/23/0
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No COC Group Number G0607587
Date/Time Submitted 6/20/07 1635
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Volatile Arnni bv1ttQ R2RflR
Method Blank OC Batch
Result RL Control Limit Units ID
Benzene ND 0.003 0.0015 mg/kg Q24552
Ethylbenzene ND 0.005 0.0025 mg/kg 024552
mp-Xylenes ND 0.01 0.005 mg/kg Q24552
o-Xylene ND 0.005 0.0025 mg/kg 024552
Toluene ND 0.005 0.0025 mg/kg 024552
Laboratory Control Sample Recovery Recovery
Result SpikeAmount Units Ranges QCBatch
ID
Benzene 0.04358 0.05 mg/kg 87 62-119 Q24552
Ethylbenzene 0.04417 0.05 mg/kg 88 57-128 024552
mp-Xylenes 0.09048 0.1 mg/kg 90 54-1 32 024552
o-Xylene 0.04725 0.05 mg/kg 95 57-1 31 024552
Toluene 0.04544 0.05 mg/kg 91 57-1 22 Q24552
Matrix Spike Recovery Recovery
Sample ID Result SpikeAmount Units
Ranges QCBatch
ID
185081 Benzene 0.03306 0.05 mg/kg 66 46-1 36 024552
Ethylbenzene 0.02888 0.05 mg/kg 58 51-1 35 Q24552
mp-Xylenes 0.05588 0.1 mg/kg 56 51-136 024552
o-Xylene 0.02855 0.05 mg/kg 57 49-1 37 024552
Toluene 0.0296 0.05 mg/kg 59 47-1 36 024552
Matrix Spike Duplicate Recovery Recovery RPD Range QCBatchSample ID
Result Spike Amount Units ID
185081 Benzene 0.03495 0.05 mg/kg 70 46-136 0-22 024552
Ethylbenzene 0.03244 0.05 mg/kg 65 51-135 12 0-23 024552
mp-Xylenes 0.06374 0.1 mg/kg 64 51-1 36 13 0-20 024552
o-Xylene 0.03337 0.05 mg/kg 67 49-1 37 16 0-22 024552
Toluene 0.03187 0.05 mg/kg 64 47-1 36 0-22 024552
Page of3
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Full Service Analytical Environmental Solutions
ESP Associates PA Project ID
Attn Chris Ward
Box 7030
Charlotte NC 28241
Level II QC Report
7/23/07
Morehead Commons No COC Group Number 00607587
Date/Time Submitted 6/20/07 1635
Diesel Range Orcianics DRO by GC-FID method 8015B
Method Blank CC Batch
Result RI Control Limit Units ID
Diesel Range Organics DRO ND 3.5 mg/kg Q24575
Laboratory Control Sample Recovery Recovery
Ranges CC Batch
Result Spike Amount Units ID
Diesel Range Organics DRO 49.0 80 mg/kg 61 55-1 09 024575
Matrix Spike Recovery Recovery
Ranges CC BSth
Sample ID Result Spike Amount Units 0/ID
184791 Diesel Range Organics DRO 45.8 80 mg/kg 57 50-117 024575
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range CC Batch
Sample ID IDResultSpikeAmountUnits
184791 Diesel Range Organics DRO 51.9 80 mg/kg 65 50-117 12 0-24 Q24575
Gasoline Range Organics GRO by GC-FID method 8015B
Method Blank
CC Batch
Result RL Control Limit Units ID
Gasoline Range Organics ND 0.5 mg/kg 024580GRO
Laboratory Control Sample Recovery Recovery
Ranges CC BatchResultSpikeAmountUnitsID
Gasoline Range Organics 1.966 mg/kg 98 64-1 24 024580GRO
Matrix Spike Recovery Recovery
Ranges CC BatchSampletOResultSpikeAmountUnitsID
185077 Gasoline Range Organics 2.016 mg/kg 101 37-1 26 024580CR0..Matrix Spike Duplicate
Recovery Recovery RPD
Ranges RPD Range CC BatchSampleIDResultSpikeAmountUnits0/ID
185077 Gasoline Range Organics 1.968 mg/kg 98 37-126 0-34 024580GRO
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
Full Service Analytical Environmental Sal Utons
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
7/23/0
ESP Associates PA
Attn Chris Ward
Box 7030
Project ID Morehead Commons No COC Group Number 00607587
Date/Time Submitted 6/20/07 1635
Charlotte NC 28241
10B
185077 Lead 40.0598 24.630
-See Case Narrative
mgfkg 108 75-125 31 -20 025161
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number 1-800/529-6364 Fax [phone]
Method Blank
QC Batch
Result RL Control Umit Units ID
Lead 0.0483 0.25 0.125 mg/kg Q25161
Laboratory Control Sample Recovery Recovery
Ranges QC BatchResultSpikeAmountUnitsID
Lead 23.4916 25 mg/kg 94 80-120 Q25161
Matrix Spike Recovery Recovery OC BatchRangesSampleIDResultSpikeAmountUnitsID
185077 Lead 29.2856 24.630 mg/kg 65 75-125 025161
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range QC Batch
Sample ID Result Spike Amount Units ID
Page of
isLBORATRIESINC
Full Service Analytical Environmental SolutIons
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Fax [phone]
Client Company Name ______________________
Report To/Contact Name
Reporting Address ______________________________-i rh fe..
Phone ________________Fax Yes No
Email Yes No Email
Address_______________________EDD Type PDF__ExceL.....3her
Site Location Name /i4u Liiii.sai
Site Location Physical Address tEs1
Project Name
Short Hold Analysis Yes No UST Project YesNo
please ATTACH any project specific reporting QC LEVEL 111111 IV
provisions and/or QC ReuisInvoiceTo
Address
CHAIN OF CUSTODY RECORD
PAGE OF
..L QUOTE ENSUR PROP ING _______________
/-YllIt I/
Purchase Order No./Billing Reference Ii
Requested Due Date Day Days
Days Days LDays
Working Days 6-9 Days Standard 10 days sWorkust Be
Samples received after 1500 will be processed next business day
Turnaround time is based on business days excluding weekends and holidays
SEE REVERSE FOR TERMS CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES INC TO CLIENT
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC USACE_FL ____NCJL
SC_OTHER J.1/A
Water Chlorinated YES_NO_
Sample Iced Upon Collection YES if NO
SAMPLE DESCRIPTION
CLIENT
-/
%542
4-2
COLLECTED
DATE
TIME
MILITARY
COLLECTED
HOURS
/OO
ico
ic
Jos
iio
MATRIX
WATER OR
SOIL
SLUDGE
SAMPLE CONTAINER
TIVES
PRESERVA-
ANALYSES REQUESTED
// // //
REMARKS
PRISM
LAB
ID NO
5B
TYPE
SEE BELOW NO SIZE
Rrhr qu ied By Signature
Samplers Signature Sampled By Print Name Affiliation
Upon relinquishing this of CustoIs your authorization for Prism to proceed with the analyses as requested above Any
chan
submitted in writing to the Prism Project Manager There will be charges for any changes after analyses have been initialized
ges must be
KeceIveo toy ttoignaturet Date
Relirquished By Signature Becetved By Signature Date
Reapived For Pri rn Laboratories ByelinquishedBySiqrgture
TAPED SHU1 TRANSPORTATION TO THE LABORATORYWITHCUSTODCOOLERS SHOULD SEMe11dclShpmottJOTESAMPLESARENOTACCEPTEDANDVERIFIED AGAINSTO5riNTlL RECEIVED AT THE LABORATORY
Fd Ex UPS and-delivered Prism Field Seivice Other
OC Group No
Militatyltiours Additional Comments Site ArdvalTime
Site Departure Time
NPDES USJ GROUNDWATER DRINKING WATER SOLID WASTE RCRA CERCLA LANDFILL OTHER
LANG USC DSC JNC USC UNC USC UNC SC NC CISC CINC CISC CINC CISC CINC CISC
LA ___LA ____LA ____LA _________LA ______________________LA _____
Field Tech Fee
Mileage
SEE REVERSE FORTERMSCONDITIONS
nR11NAL
Lj JUL OO7
Case NarrativePRISM
LABORATORIESINC
Date 07/16/07 Client Project ID Morehead Commons No
Company ESP Associates PA Prism COC Group No G0707087
Contact Chris Ward Collection Dates 07/05/07
Address Box 7030 Lab Submittal Dates 07/05/07
Charlotte NC 28241
This data package contains the analytical results for the project identified above and includes Case Narrative Laboratory Report and QualityControlDatatotaling14pageschain-of-custody is also attached for the samples submitted to Prismfor this project
Data qualifiers are flagged individually on each sample key reference for the data qualifiers appears at the end of this case narrative Qualitycontrolstatements and/or sample specific remarks are included in the sample comments section of the laboratory report for each sampleaffected
Semi Volatile Analysis
No Anomalies Reported
Volatile Analysis
N/A
Metals Analysis
Analysis Note for 024880 MSD Chromium RPD value outside the control limits Sample is not homogeneous
Wet Lab and Micro Analysis
N/A
Please call if you have any questions relating to this analytical report
Date Reviewed by Robbi Jones Project Manager An ercash
Signature
1T1k...s.d_
Signature ______________________________
Review Date _7/1 6/07 Approval Date 07/16/07
Data Qualifiers Key Reference
Compound also detected in the method blank
Result outside of the QC limits
DO Compound diluted out
Estimated concentraffon calibration range exceeded
The analyte was positively identified but the value is estimated below the reporting limit
Estimated concentrafion with high bias
Estimated concentrafion with low bias
matrixeffect is present
Notes This report should not be reproduced except in its enürety without the writtten consent of Prism Laboratories Inc The results in thisreportrelateonlytothesamplessubmittedforanalysis
449 Springbrook Road P.O Box 240543 Chaiotte NC 28224-0403
Phone [phone] Tot Free 800/529-6364 Fax [phone]
NC Certification No 402FtRisMSCCertificationNo99012
NC Drinking Water Cert No 37735
all Service Analytical EnvIronmental Solutions
ESP Associates PA Project ID
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
Morehead commons No Client Sample ID WS-2
Prism Sample ID 186280
COC Group G0707087
Time Collected 07/05/07 1500
Time Submitted 07/05/07 1520
07/16/07
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto Q24946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13107 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
07/13/07 507 kcampigotto 024946
Sample Matrix Soil
arameter Result Units Report MDL Dilution Method
Limit Factor
Analysis Analyst
Batch
Date/Time ID
SM2540 07/10/07 1300 athao
ercent Solids
ercent Solids 93.5
emi-volatjle Organic Compounds by GC/MS
24-Trichlorobenzene BRL
2-Dichlorobenzene BRL
3-Dichlorobenzene BRL
4-Dichlorobenzene BRL
45-TrichtorophenoI BRL
246-Trichlorophenol BRL
4-Dichlorophenol BRL
24-Dimethyiphenol BRL
4-Diriitrophenol BRL
24-Dinitrotoluene BRL
.6-Dinitrotojuene BRL
-Chloronaphthalene BRL
2-Chiorophenol BRL
LMethylnaphthalene BRL
2-Methyiphenol BRL
-Nitrophenol BRL
34-Methylphenol BRL
3-Dichlorobenzidine BRL
46-Dinitro-2-methylphenol BRL
-Bromophenylphenylether BRL
4chloro3methylphenol BRL
4-Chioroaniline BRL
-ChIorophenylphenyIether BRL
4-Nitrophenol BRI
mg/kg 0.35 0.035
mg/kg 0.35 0.026
mg/kg 0.35 0.026
mg/kg 0.35 0.032
mg/kg 0.35 0.036
mg/kg 0.35 0.034
mg/kg 0.35 0.030
mg/kg 0.35 0.034
mg/kg 1.8 0.040
mg/kg 0.35 0.020
mg/kg 0.35 0.038
mg/kg 0.35 0.037
mg/kg 0.35 0.028
mg/kg 0.35 0.028
mg/kg 0.35 0.033
mg/kg 0.35 0.042
mg/kg 0.35 0.036
mg/kg 0.71 0.022
mg/kg 1.8 0.022
mg/kg 0.35 0.034
mg/kg 0.71 0.026
mg/kg 0.35 0.045
mg/kg 0.35 0.022
mg/kg 1.8 0.024
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
Laboratory Report
07/16/07
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 186280
Sample Matrix Soil COC Group G0707087
Time Collected 07/05/07 1500
Time Submitted 07/05/07 1520
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ut Service Analytcal Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
iarameter Result Units Report MDL Dilution Method
Limit Factor Date/Time ID
Analysis Analyst Batch
\cenaphthene BRL mg/kg 0.35 0.035 8270C 07/13/07 507 kcampigotto 024946
Acenaphthylene BRL mg/kg 0.35 0.035 8270C 07/13/07 507 kcampigotto Q24946
\nthracene BRL mg/kg 0.35 0.027 8270C 07/13/07 507 kcampigotto 024946
zobenzene BRL mg/kg 1.8 0.033 8270C 07/13/07 507 kcampigotto 024946
-Benzoaanthracene BRL mg/kg 0.35 0.050 8270C 07/13/07 507 kcampigotto 024946
3enzoapyrene BRL mg/kg 0.35 0.041 8270C 07/13/07 507 kcampigotto 024946
Benzobfluoranthene BRL mg/kg 0.35 0.016 8270C 07/13/07 507 kcampigotto 024946
3enzoghiperylene BRL mg/kg 0.35 0.017 8270C 07/13/07 507 kcampigotto Q24946
Benzokfluoranthene BRL mg/kg 0.35 0.029 8270C 07/13/07 507 kcampigotto 024946
3enzoic acid BRL mg/kg 1.8 0.15 8270C 07/13/07 507 kcampigotto 024946
Benzyl alcohol BRL mg/kg 0.71 0.037 8270C 07/13/07 507 kcampigotto 024946
3is2-chloroethoxymethane BRL mg/kg 0.35 0.041 8270C 07/13/07 507 kcampigotto 024946
3is2-chloroethylether BRL mg/kg 0.35 0.038 8270C 07/13/07 507 kcampigotto 024946
3is2-chloroisopropylether BRL mg/kg 0.35 0.030 8270C 07/13/07 507 kcampgotto 024946
31s2-ethylhexylphthalate BRL mg/kg 0.35 0.017 8270C 07/13/07 507 kcampigotto 024946
Butylbenzylphthalate BRL mg/kg 0.35 0.022 8270C 07/13/07 507 kcampigotto 024946
hrysene BRL mg/kg 0.35 0.059 8270C 07/13/07 507 kcampigotto 024946
Di-n-butylphthalate BRL mglkg 0.35 0.016 8270C 07/13/07 507 kcampigotto 024946
i-n-octylphthalate BRL mg/kg 0.35 0.026 8270C 07/13107 507 keampigotto 024946
bibenzoahanthracene BRL mg/kg 0.35 0.036 8270C 07/13/07 507 kcampigotto 024946
ibenzofuran BRL mg/kg 0.35 0.030 8270C 07/13/07 507 kcampigotto Q24946
iethylphthaIate BRL mg/kg 0.35 0.022 8270C 07/13/07 507 kcampigotto 024946
imethyIphthalate BRL mg/kg 0.35 0.024 8270C 07/13/07 507 kcampigotto 024946
1uoranthene 0.14J mg/kg 0.35 0.024 8270C 07/13/07 507 kcampigotto 024946
Fluorene BRL mg/kg 0.35 0.021 8270C 07/13/07 507 keampigotto 024946
lexachlorobenzene BRL mg/kg 0.35 0.018 8270C 07/13/07 507 kcampigotto Q24946
Hexachiorobutadiene BRL mg/kg 0.35 0.034 8270C 07/13/07 507 kcampigotto 024946
Page of
Parameter
Hexachlorocyclopentadiene
Hexachloroethane
lndeno1 23-cdpyrene
lsophorone
-N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Pentachiorophenol
Phenanthrene
Phenol
Pyrene
Surrogate Recovery Control Limits
Terphenyl-d14 101 41 136
Phenol-d5 73 13 95
Nitrobenzene-d5 76 14 103
2-Fluorophenol 63 14 89
2-Fluorobiphenyl 75 21 108
246-Tribromophenol 102 25 123
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full Service Anulytical EnvIronmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
07/16/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-2
186280
G0707087
07/05/07 1500
07/05/07 1520
Analyst Batch
ID
Result Units Report MDL Dilution Method Analysis
Limit Factor Date/Time
BRL mg/kg 0.35 0.038 8270C 07/13/07 507
BRL mg/kg 0.35 0.036 8270C 07/13/07 507
BRL mg/kg 0.35 0.036 8270C 07/13/07 507
BRL mg/kg 0.35 0.032 8270C 07/13/07 507
BRL mg/kg 0.35 0.040 8270C 07113/07 507
BRL mg/kg 0.35 0.018 8270C 07/13/07 507
BRL mg/kg 0.35 0.039 8270C 07/13/07 507
BRL mg/kg 0.35 0.035 8270C 07/13/07 507
BRL mg/kg 1.8 0.030 8270C 07113/07 507
BRL mg/kg 0.35 0.017 8270C 07/13/07 507
BRL mg/kg 0.35 0.039 8270C 07/13/07 507
0.16J mg/kg 0.35 0.024 8270C 07/13/07 507
29.85g mL 3550B 07/11/07 800
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigolto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampgotto
kcampigotto
Q24946
024946
024946
024946
Q24946
024946
Q24946
024946
024946
024946
024946
024946
Sample Preparation dpope P18865
Page of
all Service Analyical Environmental Solutions
ESP Associates PA
\ttn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
07/16/07
WS-2
186280
G0707087
07/05/07 1500
07/05/07 1520
arameter Result Units Report
Limit
Method Analyst Batch
ID
3am pie Comments
BRL Below Reporting Limit
f-Estimated value between the Reporting Limit and the MDL
rhe results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthose instances indicated in the case narrative and/or test commentslIresultsarereportedondr/-weight basis
Pngela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
MDL Dilution
Factor
Analysis
Date/Time
Phone 7Q4/529-63M Toll Free Number 1-800/529-6364 Fax [phone] Page of
ull Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
07/16/07
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 186281
Sample Matrix Soil COC Group G0707087
Time Collected 07/05/07 1505
Time Submitted 07/05/07 1520
95.6 SM2540 07/10/07 1300 athao
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Percent Solids Determination
Percent Solids
Semi-volatile Organic Compounds by GC/MS
124-TrichIorobenzene BRL mg/kg 0.35 0.035 8270C 07/13/07 559 kcampigotto 024946
2-Dichlorobenzene BRL mg/kg 0.35 0.026 8270C 07/13/07 559 kcampigotto 024946
13-Dichlorobenzene BRL mg/kg 0.35 0.025 8270C 07/13/07 559 kcampigotto 024946
14-Dichlorobenzene BRL mg/kg 0.35 0.031 8270C 07113/07 559 kcampigotto 024946
245-Tiichlorophenol BRL mg/kg 0.35 0.036 8270C 07/13/07 559 kcampigotto Q24946
246-Trichicirophenol BRL mg/kg 0.35 0.033 8270C 07/13/07 559 kcampigotto 024946
M-Dichlorophenol BRL mg/kg 0.35 0.029 8270C 07/13/07 559 kcampigotto 024946
24-Dimethylphenol BRL mg/kg 0.35 0.034 8270C 07/13/07 559 kcampigotto 024946
4-Dinitrophenol BRL mg/kg 1.7 0.039 8270C 07/13/07 559 kcampgotto 024946
24-Dinitrotoluene BRL mg/kg 0.35 0.020 8270C 07/13/07 559 kcampigotto 024946
6-Dinitrotoluene BRL mg/kg 0.35 0.037 8270C 07/13/07 559 kcampigotto 024946
1-Chloronaphthalene BRL mg/kg 0.35 0.036 8270C 07/13/07 559 kcampigotto 024946
2-Chlorophenol BRL mg/kg 0.35 0.027 8270C 07/13/07 559 kcampigotto 024946
2-Methylnaphthalene BRL mg/kg 0.35 0.028 8270C 07/13/07 559 kcampigotto 024946
2-Methylphenol BRL mg/kg 0.35 0.033 8270C 07/13/07 559 kcampigotto 024946
-Nitrophenol BRL mg/kg 0.35 0.042 8270C 07/13/07 559 kcampigotto 024946
34-Methylphenol BRL mg/kg 0.35 0.036 8270C 07/13/07 559 kcampigotto 024946
3-Dichlorobenzidine BRL mg/kg 0.70 0.022 8270C 07/13/07 559 kcampgotto 024946
46-Dinitro-2-methylphenol BRL mg/kg 1.7 0.02 8270C 07/13/07 559 kcampigotto 024946
-BromophenylphenyIether BRL mg/kg 0.35 0.033 8270C 07/13/07 559 kcampigotto 024946
-IChloro3methylphenol BRL mg/kg 0.70 0.026 8270C 07/13/07 559 kcampigotto 024946
4-Chloroaniline BRL mg/kg 0.35 0.044 8270C 07/13/07 559 kcampigotto 024946
-ChlorophenyIphenylether BRL mg/kg 0.35 0.022 8270C 07/13/07 559 kcampigotto 024946
4-Nitrophenol BRL mg/kg 1.7 0.023 8270C 07/13/07 559 kcampigotto 024946
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ili Service Analytical Environmental Solutions
ESP Associates PA Project ID
ttn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
07/16/07
Morehead Commons No Client Sample ID WS-3
Prism Sample ID 186281
COC Group G0707087
Time Collected 07/05/07 1505
Time Submitted 07/05/07 1520
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Sample Matrix Soil
arameter Result Units Report MDL Dilution Method
Limit Factor
Analysis Analyst Batch
Date/Time ID
cenaphthene BRL mg/kg 35 034 8270C 07113/07 59 kcampigotto 024946
Acenaphthylene BRL mg/kg 0.35 0.035 8270C 07/13/07 559 kcampigotto 024946
nthracene BRL mg/kg 0.35 0.026 8270C 07/13/07 559 kcampigotto 024946
obenzene BRL mg/kg 1.7 0.032 8270C 07/13/07 559 kcampigotto 024946
enzoaanthracene BRL mg/kg 0.35 0.049 8270C 07/13/07 559 kcampigotto 024946
enzoapyrene BRL mg/kg 0.35 0.040 8270C 07/13/07 559 kcampigotto 024946
Benzobfluoranthene BRL mg/kg 0.35 0.016 8270C 07/13/07 559 kcampigotto 024946
enzoghiperylene BRL mg/kg 0.35 0.017 8270C 07/13/07 559 kcampigotto 024946
Benzokfluoranthene BRL mg/kg 0.35 0.028 8270C 07113/07 559 kcampigotto 024946
enzoicacid BRL mg/kg 1.7 0.15 8270C 07/13/07 559 kcampigotto 024946
Benzyl alcohol BRL mg/kg 0.70 0.037 8270C 07/13/07 559 kcampigolto 024946
is2-chloroethoxymethane BRL mg/kg 0.35 0.040 8270C 07/13/07 559 kcampigotto 024946
Jis2-chloroethylether BRL mg/kg 0.35 0.038 8270C 07/13/07 559 kcampigotto 024946
3is2-chloroisopropylether BRL mg/kg 0.35 0.030 8270C 07/13/07 559 kcampigotto 024946
is2-ethylhexylphthalate BRL mg/kg 0.35 0.017 8270C 07/13/07 559 kcampigotto 024946
Butylbenzylphthalate BRL mg/kg 0.35 0.021 8270C 07/13/07 559 kcampigotto 024946
Thrysene BRL mg/kg 0.35 0.058 8270C 07/13/07 559 kcampigotto Q24946
Di-n-butylphthalate BRL mg/kg 0.35 0.016 8270C 07/13/07 559 kcampigotto 024946
i-n-octylphthalate BRL mg/kg 0.35 0.026 8270C 07/13/07 559 kcampigotto 024946
Dibenzoahanthracene BRL mg/kg 0.35 0.035 8270C 07/13/07 559 kcampigotto 024946
ibenzofuran BRL mg/kg 0.35 0.030 8270C 07/13/07 559 kcampigotto 024946
iethyIphthalate BRL mg/kg 0.35 0.021 8270C 07/13/07 559 kcampigotto Q24946
imethylphthalate BRL mg/kg 0.35 0.024 8270C 07/13/07 559 kcampigotto 024946
luoranthene 0.20 mg/kg 0.35 0.024 8270C 07/13/07 559 kcampigotto 024946
Fluorene BRI mg/kg 0.35 0.021 8270C 07/13/07 559 kcampigotto 024946
Iexachlorobenzene BRI mg/kg 0.35 0.018 8270C 07/13/07 559 keampigotto 024946
Hexachlorobutadiene BRL mg/kg 0.35 0.034 8270C 07/13/07 559 kcampigotto 024946
Page of
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 186281
Sample Matrix Soil COG Group G0707087
Time Collected 07/05/07
Time Submitted 07/05/07
Extractable Petroleum Hydrocarbons by GC-FlD
C11-C22 Aromatics BRL mg/kg
Analysis Note for Cll-C22 Aromatics
Cl 9-C36 Aliphatics BRL mg/kg
9-C18 Aliphatics BRL mg/kg
10 5.4
Adjusted value
10 1.5
10 3.2
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
tervice Anulytical tinvirenmenlal Solutions
NC Certification No 402
SC Certification No 99012 Laboratory Report
NC Drinking Water Cert No 37735 07/16/07
ESP Associates PA
ttn Chris Ward
Box 7030
Charlotte NC 28241 1505
1520
arameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
exachIorocyclopentadiene BRL mg/kg 0.35 0.037 8270C 07/13/07 559 kcarnpigotto Q24946
Hexachloroethane BRL mg/kg 0.35 0.035 8270C 07/13/07 559 kcampigotto 024946
ndeno123-cdpyrene BRL mg/kg 0.35 0.036 8270C 07113/07 559 keampigotto 024946
ophorone BRL mg/kg 0.35 0.031 8270C 07/13/07 559 kcampigotto 024946
J-Nitrosodi-n-propyIamine BRL mg/kg 0.35 0.039 8270C 07/13/07 559 kcampigotto 024946
-Nitrosodiphenylamine BRL mg/kg 0.35 0.018 8270C 07/13/07 559 kcampigotto 024946
Naphthalene BRL mg/kg 0.35 0.038 8270C 07/13/07 559 kcampigotto Q24946
Jitrobenzene BRL mg/kg 0.35 0.034 8270C 07/13/07 559 kcampigotto Q24946
Pentachlorophenol BRL mg/kg 1.7 0.029 8270C 07/13/07 559 kcampigotto 024946
henanthrene 0.11 mg/kg 0.35 0.017 8270C 07/13/07 559 kcampigotto 024946
Phenol BRL mg/kg 0.35 0.038 8270C 07/13/07 559 kcampigotto 024946
yrene 0.22 mg/kg 0.35 0.024 8270C 07/13/07 559 keampigotto 024946
Sample Preparation 29.73g mL 3550B 07/11/07 800 dpope P18865
Surrogate Recovery Control Limits
Terphenyl-d14 100 41 136
Phenol-d5 69 13 -95
Nitrobenzene-d5 73 14-103
2-Fluorophenol 73 14-89
2-Fluorobiphenyl 72 21 108
246-Ttibrornophenof 113 25 123
MADEP EPH 07/12/07 928 grappaccioli
MADEP EPH
MADEP EPH
07/12/07 928 grappaccioli
07/12/07 928 grappaccioli
024910
024910
024910
Page of
PRISM SC Cerllflcation NO 99012 Laboratory Report
RnroRlcs INC NC Drinking Water Cert No 37735 07/16/07
uli S.rica Analytical Environinnnt.l Soltitiois
ESP Associates PA Project ID Morehead Commons No Client Sample ID WS-3
\ttn Chris Ward Prism Sample ID 186281
Box 7030 Sample Matrix Soil COC Group G0707087
Charlotte NC 28241 Time Collected 07/05/07 1505
Time Submitted 07/05/07 1520
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Sample Preparation 10.47g mL EPH 07109/07 1100 dpope P18855
Surrogate Recovery Control Limits
o-Terphenyl 74 40 140
2-Fluorobiphenyl 56 40 140
2-Bromonaphthalene 54 40 140
1-Chloro-octadecane 79 40 140
Sample Comments
3RL Below Reporting Limit
J-Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than4ELACcertificationexceptforthose instances indicated/n the case narrative and/or test comments
ll results are reported on thy-weight basis
ngela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
all Service Analytical Environmental Solutions
ESP Associates PA
ttn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
186282
G0707087
07/05/07 1510
07/05/07 1520
07/16/07
arameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
letals by ICP
chromium 26 mg/kg 0.25 0.015 6010B 07/10/07 2353 mcampbell 024880
Sample Preparation 2g 50 mL 3050B 07/09/07 800 jhoppel P18845
Sample Comments
RL Below Reporting Limit
3-Estimated value between the Reporting Limit and the MDL
Jhe results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanJELAcertificationexceptforthoseinstances indicated in the case narrative and/or test comments
lI results are reported on wet-weight basis
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Project ID Morehead Commons No Client Sample ID B-I
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
ngela Overcash V.P Laboratory Services
Phone [phone] ToIl Free Number 1-8001529-6364 Fax [phone] Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Metals by ICP method 601DB
Cl 1-C22 Aromatics
Cl 9-C36 Aliphatics
C9-C18 Aliphatics
Laboratory Control Sample
Cl 1-C22 Arornatics
Cl 9-C36 Aliphatics
C9-C1 Aliphatics
Matrix Spike
Sample ID
186445 Cl l-C22 Aromatics
Cl 9-C36 Aliphatics
C9-C1 Aliphatics
13774 170
44.08 80
32.06 60
Recovery Recovery
RangesUnits
mg/kg 75 40-140
mg/kg 52 40-140
mg/kg 53 40-140
Recovery Recovery
RangesUnits
mg/kg 81 40-1 40
mg/kg 55 40-1 40
mg/kg 53 40-1 40
Q249l0
024910
024910
QC Batch
ID
024910
024910
024910
QC Batch
ID
024910
024910
024910
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number 1-8001529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
7/16/2007
Project ID Morehead Commons No COC Group Number G0707087
Date/Time Submitted 7/5/2007 1520
Method Blank
QC BatchResultRLControlLimitUnitsID
Chromium 0.0662 0.25 0.125 mg/kg 024880
Laboratory Control Sample Recovery Recovery
Ranges DC BatchResultSpikeAmountUnitsID
Chromium 22.7819 25 mg/kg 91 80-1 20 024880
Matrix Spike Recovery Recovery
Ranges QC BatchSampleIDResultSpikeAmountUnitsID
186342 Chromium 34.5949 25 mg/kg 113 75-125 024880
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range DC BatchSample ID
Result Spike Amount Units
0/ID
186342 Chromium 27.9758 24.875 mg/kg 87 75-125 21 -20 Q24880
Extractable Petroleum Hydrocarbons by GC-FID method MADEP EPH
Method Blank
DC BatchResultRLControlLimitUnitsID
ND 10 mg/kg
ND 10 mg/kg
ND 10 mg/kg
Result Spike Amount
128.22 170
41.94 80
31.9 60
Result Spike Amount
Matrix Spike Duplicate
Recovery Recovery RPD
BatchRangesRPDRangeSampleIDResultSpikeAmountUnits
04 ID
186445 C11-C22Aromatics 119.6 170 mg/kg 70 40-140 14 0-50 Q24910
C19-C36 Aliphatics 52.7 80 mg/kg 66 40-140 18 0-50 024910
C9-C18 Aliphatics 37.12 60 mg/kg 62 40-140 15 0-50 024910
Page of4
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Full SeMce Analytical Enmroamental Solutlmts
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Semi-volatile ArnanE ffIftilQ R270C
Method Blank QC Bstch
Result RL Control Limit Units ID
Level II QC Report
7/16/2007
Project ID Morehead Commons No COG Group Number G0707087
Date/Time Submitted 7/5/2007 1520
24-Trichlorobenzerie ND 0.33 0.165 mg/kg Q24946
2-Dichlorobenzene ND 0.33 0.165 mg/kg 024946
3-Dichlorobenzene ND 0.33 0.165 mg/kg 024946
4-Dichlorobenzene ND 0.33 0.165 mg/kg 024946
245-Trichiorophenol ND 0.33 0.165 mg/kg Q24946
246-Trichiorophenol ND 0.33 0.165 mg/kg 024946
24-Dichlorophenol ND 0.33 0.165 mg/kg 024946
24-Dimethyiphenol ND 0.33 0.165 mg/kg 024946
24-Dinitrophenol ND 1.65 0.825 mg/kg Q24946
24-Dinitrotoluene ND 0.33 0.165 mg/kg Q24946
26-Dinitrotoluene ND 0.33 0.165 mg/kg 024946
2-Chloronaphthalene ND 0.33 0.165 mg/kg Q24946
2-Chiorophenol ND 0.33 0.165 mg/kg 024946
2-Methylnaphthalene ND 0.33 0.165 mg/kg 024946
2-Methyiphenol ND 0.33 0.165 mg/kg 024946
2-Nitrophenol ND 0.33 0.165 mg/kg 024946
34-Methylphenol ND 0.33 0.165 mg/kg Q24946
33-Dichlorobenzjdine ND 0.66 0.33 mg/kg 024946
4.6-Dinitro-2-methylphenol ND 1.65 0.825 mg/kg 024946
4-Bromophenyiphenylether ND 0.33 0.165 mg/kg 024946
4-Chloro-3-methyphenol ND 0.66 0.33 mg/kg 024946
4-Chioroaniline ND 0.33 0.165 mg/kg 024946
4-Chiorophenyiphenylether ND 0.33 0.165 mg/kg 024946
4-Nitrophenol ND 1.65 0.825 mg/kg Q24946
Acenaphthene ND 0.33 0.165 mg/kg 024946
Acenaphthylene ND 0.33 0.165 mg/kg 024946
Anthracene ND 0.33 0.165 mg/kg 024946
Azobenzene ND 1.65 0.825 mg/kg Q24946
Benzoaanthracene ND 0.33 0.165 mg/kg Q24946
Benzoapyrene ND 0.33 0.165 mg/kg 024946
Benzobfluoranthene ND 0.33 0.165 mg/kg 024946
Benzoghiperylene ND 0.33 0.165 mg/kg Q24946
Benzokfluoranthene ND 0.33 0.165 mg/kg 024946
Benzoic acid ND 1.65 0.825 mg/kg Q24946
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
SC Cerflflcation No 99012
Level QC Report
NC Drinking Water Cert No 37735 7/16/2007
irull Service Analytical Environmentai Solutions
ESP Associates PA Project ID Morehead Commons No COG Group Number G0707087
Attn Chris Ward Date/Time Submitted 7/5/2007 1520
Box 7030
Charlotte NC 28241
Method Blank QC Batch
Result RI Control Limit Units ID
Benzyl alcohol ND 0.66 0.33 mg/kg Q24946
Bis2-chloroethoxymethane ND 0.33 0.165 mg/kg Q24946
Bis2-chloroethylether ND 0.33 0.165 mg/kg 024946
Bis2-chloroisopropylether ND 0.33 0.165 mg/kg Q24946
Bis2-ethylhexylphthalate ND 0.33 0.165 mg/kg 024946
Butylbenzylphthalate ND 0.33 0.165 mg/kg Q24946
Chrysene ND 0.33 0.165 mg/kg Q24946
Di-n-butylphthalate ND 0.33 0.165 mg/kg Q24946
Di-n-octylphthalate ND 0.33 0.165 mg/kg Q24946
Dibenzoahanthracene ND 0.33 0.165 mg/kg Q24946
Dibenzofuran ND 0.33 0.165 mg/kg 024946
Diethylphthalate ND 0.33 0.165 mg/kg 024946
Dimethylphthalate ND 0.33 0.165 mg/kg 024946
Fluorantherie ND 0.33 0.165 mg/kg 024946
Fluorene ND 0.33 0.165 mg/kg 024946
Hexachlorobenzene ND 0.33 0.165 mg/kg 024946
Hexachlorobutadjene ND 0.33 0.165 mg/kg 024946
Hexachiorocyclopentadiene ND 0.33 0.165 mg/kg 024946
Hexachioroetharie ND 0.33 0.165 mg/kg 024946
lndeno1 23-cdpyrene ND 0.33 0.165 mg/kg 024946
Isophorone ND 0.33 0.165 mg/kg 024946
N-Nitrosodi-n-propylarnine ND 0.33 0.165 mg/kg 024946
N-Nitrosodiphenylamine ND 0.33 0.165 mg/kg 024946
Naphthalene ND 0.33 0.165 mg/kg 024946
Nitrobenzene ND 0.33 0.165 mg/kg 024946
Pentachlorophenol ND 1.65 0.825 mg/kg 024946
Phenanthrene ND 0.33 0.165 mg/kg 024946
Phenol ND 0.33 0.165 mg/kg 024946
Pyrene ND 0.33 0.165 mg/kg 024946
Laboratory Control Sample Recovery Recovery
BatchRangesResultSpikeAmountUnitsYeID
--..-o._
24-Trichlorobenzene 1.26414 1.6742 mg/kg 76 39-98 024946
14-Dichlorobenzene 1.22999 1.6742 mg/kg 73 37-95 024946
24-Dinitrotoluene 1.51188 1.6742 mg/kg 90 56-1 28 024946
2-Chlorophenol 1.41144 1.6742 mg/kg 84 37-98 024946
4-Chloro-3-methylphenol 1.40709 1.6742 mg/kg 84 45-111 Q24946
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number 1-8001529-6364 Fax [phone] Page of
Full Service Analytical Environmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 26241
Level II QC Report
7/16/2007
Project ID Morehead Commons No COG Group Number G0707087
Date/Time Submitted 7/5/2007 1520
Laboratory Control Sample Recovery Recovery
Ranges QC Batch
Result Spike Amount Units ID
4-Nitrophenol 0.97991 1.6742 mg/kg 59 20-157 024946
Acenaphthene 1.29092 1.6742 mg/kg 77 44-110 Q24946
N-Nitrosodi-n-propylamine 1.38935 1.6742 mg/kg 83 38-101 Q24946
Pentachlorophenol 1.94174 1.6742 mg/kg 116 53-127 Q24846
Phenol 1.26146 1.6742 mg/kg 75 34-102 Q24946
Pyrene 1.54837 1.6742 mg/kg 92 54-131 024946
Matrix Spike Recovery Recovery
Ranges OC Batch
Sample ID Result Spike Amount Units ID
1.23412 1.6537 mg/kg 75
1.13723 1.6537 mg/kg 69
1.65211 1.6537 mg/kg 100
1.14351 1.6537 mg/kg 69
1.25562 1.6537 mg/kg 76
0.96197 1.6537 mg/kg 58
1.28406 1.6537 mg/kg 78
1.25661 1.6537 mg/kg 76
1.88095 1.6537 mg/kg 114
1.12830 1.6537 mg/kg 68
1.44907 1.6537 mg/kg 88
Q24946
024946
024946
024946
024946
024946
024946
024946
024946
Q24946
024946
186433 24-Trichlorobenzene
4-Dichlorobenzene
24-Dinitrotoluene
2-Chiorophenol
4-Chloro-3-methylphenol
4-Nitrophenol
Acenaphthene
N-Nitrosodi-n-propylamine
Pentachiorophenol
Phenol
Pyrene
Matrix Spike Duplicate
Sample ID
186433 24-Trichlorobenzene
4-Dichlorobenzene
24-Dinitrotoluene
2-Chlorophenol
4-Chloro-3-methylphenol
4-Nitrophenol
Acenaphthene
N-Nitrosodi-n-propylamine
Pentachlorophenol
Phenol
Pyrene
-See Case Narrative
Recovery
Result Spike Amount Units
26-97
23-92
45-127
25-94
31-113
17-150
36-107
22-105
39-1 37
23-97
45-133
Recovery
Ranges
26-97
23-92
45-127
25-94
31-113
17-150
36-1 07
22-1 05
39-137
23-97
QC Batch
ID
1.37073
1.11520
1.36537
1.20194
1.43402
0.81212
1.15472
1.18687
1.84192
1.14902
1.6748
1.6748
1.6748
1.6748
1.6748
1.6748
1.6748
1.6748
1.6748
1.6748
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
82
67
82
72
86
48
69
71
110
69
RPD
RPD Range
10 0-37
0-36
19 0-29
0-37
13 0-32
17 0-32
11 0-32
0-37
0-27
0-42
024946
024946
024946
024946
024946
024946
024946
024946
024946
024946
1.47957 1.6748 mg/kg 88 45-1 33 -27 Q24946
Page of
CHAIN OF CUSTODY RECORD
PAGE .4L QUOTE ENS7RE PRPE ILLING _______________
Project Name
Short Hold Analysis Yes No UST Project Yes No
please ATTACH any project specific reportin9 OC LEVEL 111111 IV
provisions and/or QC Requiremçt
Invoice To
Address //II7j J5
Purchase Order NoiBilling Reference
Requested Due Date Day Days Days Days Days
Working Days 6-9 Days Standard 10 days us Work lust Be
Samples received after 1500 will be processed next business day
Turnaround time is based on business days excluding weekends and holidays
SEE REVERSE FOR TERMS CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES INC TO CLIENT
SAcrwaTme
Sita DepartUre Time
Fieci Tech Fee
Mileage
Full Service Analytical Environmental Solutions
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Client Company Name ____________________________
Phone [phone] Fax
Report To/Contact Name l/
Reporting Address _______________________________
Phone __________________
Email Yes No Email Address
EDD Type PDF__Excel
Site Location Name
Fax Yes No
CLfh.ar
Site Location Physical Address
IW.i4iLi
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC USACE FL ____NC
SC__OTHER _____N/A _____
Water Chlorinated YES_NO_
Sample Iced Upon Collection YES i/NO
CLIENT
SAMPLE DESCRIPTION
LLJ5-.Zs4
L4-I
DATE
COLLECTED
7Y
TIME
COLLECTED
MILITARY
HOURS
jooic
Jlb
MATRIX
SOIL
WATER OR
SLUDGE
SAMPLE CONTAINER PRESERVA
TIVES
NALYSES REQUESTED/////// //
//REMARKS
i7i
LAB
PRISM
ID NOTYPE
SEE BELOW
aTL
NO SIZE
Relinquished By Signature
Samplers Signature Sampled By Print Name Affiliation
Upon relinquishing this Chain of st6 is your authorization for Prism to proceed with the analyses as requested
above Any changes must besubmittedinwritingtothePrismProjectManagerTherewillbechargesforanychangesafteranalyseshave been initialized
eceivea uy ignaure uate Military/hours
Relinquished By Signature Received By Signature Date
Relinquished By Si re joratsBY
Method of Ship NOTE ALIMPLE COOLERS SHOULD BE TAPED SHU US OR TRANSPORTATION TO THE LABORATORY roup No
S9PLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY
Fed Ex UPS .and-delivered Prism Field Service Other
iI
Additional Comments
NPDES usj GROUNDWATER DRINKING WATER SOLID WASTE RCRA CERCLA LANDFILL OTHERNCSCNCSC NC SC NC SC NC SC NC SC NC SC NC SC NC SC___________________________________flflkflA i.irfl Ufl flflCt....L....flL...fl....fl nI.....i$.ri T.4i.....fl....alt L..u..s..A....._fl...i....t...
SEE REVERSE FORTERMSCONDITIONS
ORIGINAL
CLIENT 4SSocJ.J-CS
ATrN G4iris
PRISM COG GROUP
P4
Please fill in the Site Location information on the attached VPH and/or EPH Forms
FuU Service AnalyFcal Envfronmentai Solutions
\NaSO1FOLD\COMMON\FORMS\WH EPH Site Location for Cilenicloc
EPH Aliphatics/Aromatics Laboratory Reporting Form
Client Name
Project Name
Site Location
ESP Associates PA
Morehead Commons No
Laboratory Name
NC Certification Lab
Sample Matrix
Prism Laboratories Inc
402
Soil
Sample Information and Analytical Results
Method for Ranges MADEP EPH
EPH Surrogate Standards Aliphatic 1-C
EPH Fractionation Surrogates
Sample Identification
Date Collected
Date Received
Date Extracted
Date Analyzed
Dry Solids
Dilution Factor
Hydrocarbon Ranges in mg/kg
C9-C18 Aliphatics
C19-C36 Aliphatics
CII -C22 Aromatics
Blank C9-C18 Aliphatics
CI 9-C36 Aliphatics
_________CII -C22 Aromatics
RL C9-C18 AUphatics
CI 9-C36 Aliphatics
________C1I-C22 Aromatics
C9-C1 Aliphatics
Cl 9-C36 Aliphatics
Cl 1-C22 Aromatics
Were all performance/acceptance standards for required QNQC
procedures achieved
Was blank correction applied as significant modification of the method
Were any significant modifications to the EPH method made
Comments
YES No Details Attached
Yes NO
NO IYes Details Attached
o-Terphenvl
186281
3nyl
7/5/2007
95.6
eResults Sample Results Sample Results Sample Results Sample Results
10
10
10
MDL
Surrogate Acceptance Range
10 10 10 10 10
10 10 10 10 10
10 10 10 10 10
10
10
10
3.2
1.5
5.4
40-1 40 40-1 40 40-140 40-140 40-140
Aliphatic Surrogate Rec 110 79
Aromatic Surrogate Rec 93 74
Fractionation Surrogate Accep Range
Blank 40-140%40-140%40-140 40-140 40-140
Frac Surrogate Rec 99 54
Frac Surrogate Rec 100 56
Unadjusted value should exclude the concentration of any surrogates internal standards and/or
concentrations of other ranges that elute within the specified range
Adjusted value
MDL Method Detection Limit RL Reporting Limit Blank Laboratory Method Blank
Page of EPH Soil
APPENDIX
NON-HAZARDOUSWASTE MANIFESTS
NC
AW FOrm 121
Please print or type
Form designed for use on elite iteh
Generators Phono
ALLU WASTE 11lNDUSTPlESFNC
Manliest
Document No
Transporter Company Name us EPA ID Number Transporerhor.rr
Transporter Company Name US EPA ID Number Transporters Phone
Designated Facility Name and Site Address 10 US EPA ID Number Facilitys Phone
CMS LandfiH 704 782-2004
5105 Morehead Rd
Concord NC 28027
11 Waste Shipping Name and Description 12 Containers 13 14
Total Unit
No Type Quantity WtNol
Additional Descriptions for Materials Listed Above Handling Codes for Wastes Listed Above
15 Special Handling
Instructions and Additional Information
16 GENERATOR CERTIFICATION certify the materials described above on this manifest are riot subject to federal regulations for reporting proper disposal of Hazardous Waste
Printed/Typed Name _J 5T
17 1lansporter Acknowledgement of Receipt of Materials
.P Printed Typed Name Signatur Month DaY VarOkTtc
Transporter Acknowledgement of eceipt of Materials
Printed Typed Name Signature Month 0SY Year
Discrepancy lndicatiàn Space
..
20 Facility Owner or Operator Carificatiori of receipt of waste materials covered bS this manifest except as noted in item 19
CMS Landfill
Printed/Type Name tZJ Signature
M0
LDaI
Year
i/S/OfF COPY
.ALLE WASTE.lNDtJSTPIES INC
TiS/DfF rriDv
Please print or type
Form designed forline on elite 12 pitch typewriter
/r1-IL/NO.N-HAZARDQUS Generators US Doo Page 12789WASTE_MANIFEST
Generators Name and Mailing Address Truck No
Generators Phone
Transporter Company Nam 6.US EPA ID Number
Transporter Company Name US EPA ID Number Transporters Phone
Designated Facility Name and Site Address 10 US EPA ID Number Facilitys Phone
CMS Landfill 704782-20045105 Morehead Rd
Concord NC 28027
11 Waste Shipping Name and Description 12 Containers 13
No Type Quantity-WINol
/fl
Additional Descriptions for Materials Listed Above Handling Codes for Wastes Lited Above
15 Special Handling Instructions and Additional Information
IS GENERATORS CERTIFICATION certify the materials described above on this manifest arenot subject to federal regufatlofis for reporting proper dtdposal
of Hazardous Waste
Printed/Typed Name
natUre -7 /.ç MOuth Day Year
17 Transporter Acknowledgement of Receipt of Materials
Printed Typed Name -.ignature .-Month Day Yearhth
18 Transporter Acknowledgement of Receipt of Materials
Printed Typed Name Signature Month Day Year
19 Discrepancy IndicatFon-SpaCe
.-
20 Facility Owner or Operator Cerification of receipt of waste materialC covered byThis hianifej excpfes noted in item 19CMSLandfill
Printed Type Name ...-Signature Month Day YearAJ7/
AWl Firm V21
I.
Please
Form
EST
WATgAvyj
Mast
Document No
and Mailing Addres
Generators Phone
.ç
Transporter Company Name US EPA ID Number Transporter ho
Transporter Company Name US EPA ID Number Transporters Phone
Designated Facility Name and Site Address 10 US EPA ID Number Facilitys PhoneCMSLandfill704.7822dl5105 Morehead Rd
Concord NC 28027
ii Waste Shipping Name and Description
fli
Additional Descriptions for Materials Listed Above
Handling Codes for Wastes Listed Above
15 Special Handling Instructions and Additional Informafion
16 GENERATOR CERTIFICATION certify the materials descebed above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous WastePrinted/Typef Name Snf lure Month Day Year
17 Transporter Acknowledgement of Receipt of Materials
Printed Typed Name
pature M5h
Day Year
18 Transpolier Acknowledgement of ReoSipt of Materials
Printed Typed Name Signature Month Day Year
19 Discrepancy Indication Space
20 Facibty Owner or Operator Cerification of receipt of waste materials covered by this manifest except as noted In Item 19CMSLandfill_\._
Printed/Type Name Yk Signature L..
.TIS/DIF/
AWF6r
PALUJDWAST
INCI
NONHAZARDOUS Generators US EPA
ID No Manifest Page .--WASTE MANIFEST ocument No of 7898
Generators Name and Mailing Address JW tJU1LW Truck No
ji
ah
Generator.Phone
..-...-Transporter Company Name US EPA ID Number Transporteysphor
Transporter Company Name US EPA ID Number Transporter Phone-
Designated Facility Name and Site Address 10 US EPA ID Number Facilitys PhoneCMSLandfill704782-20d45105 Morehead Rd
Concord NC 28027 ._____11 Waste Shipping Name and Description 12 Containers 13 14
Total UnitNoTypeQuantityWtNol
ait
L1
Additional Descriptions for Materials Listed Above Handling Codes br Wastes Listed Above
-f .--
15 Special Handling Instructions and Additional Information
16 GENERATORS CERTIFICATION certify the materials described above on this manifest are-not subject to federal regulations for reporting proper disposal of Hazardous WastePrinted/Typed Name
Pature Month Day war
17 Transporter Acknowledgement of Receipt of Materials
Printed /Typed-Name ---.-----.1SigAatije-..Mo Day---Year --
02lBTansporter2AcknowledgementofReceiptofMaenaIs
Stgnature
19 Discrepancy Indication Space
ciliW Owner or Operator Cencabon of recpwt
.-TISID/FI.v --
Please print or type
Form designed for use on elite 12 pitch typewriter /4924
-S
-H
--Month DaY
Please print or type
Form designed for Use on elite 12 pitch typswriter
1DUS1RIES NC
NON-HAZARDOUS 1.Generators US EPA ID No iantfest aPagel
WASTE_MANIFEST ..__1
Generators Name and Mailing Address i%Truck No-..a..
iiLt
Generators Phone
Transporter Company Name US EPA ID Number TransportetsPbone
Transporter Company Name US EPA ID Number Transporters Phone
Designated Facility Name and Site Address 10 US EPA ID Number Facilitys Phone
CMS Landfill 704 782-20045105MoreheadRd
Concord NC 28027
11 Waste Shipping Name and Description 12 Containers 13.14
Total UnitNoTypeQuantityWI/Vol
Additional Descriptions for Materials Listed Above Handling Codes for Wastes Listed Above
II
15 Special Handling Instructions and Additional Information
16 GENERATOR CERTIFICATION certify the materials described above on this manifest are nat subject to federal regulations for reporting proper disposal of Hazardous Waste
Printed /Typed Name
Year
17 Transporter Acknowledgement of Receipt of Materials
Printed /Typed Name Signature MOyth Day YearIZIO718TransporterAcknowledgementofReceiptof Materials
Printed Typed Name Signature Month Day Year
19 Discrepancy Indication Space
..
20 Facility Owner or Operator Cerif cation of receipt of waste materials covered by this manifest except as noted in item 19CM.S Landfill
Punted/Type Name r/Signatur
..
T/SIDIF/COPY
AWl Form 121
Please print or type
Form designed for use on eite 12.pltch typewriter
/1 //
IiV/L li
AWl Form 121
.WST
IN DUI ES
NON.HAZARDOUS Generatbs US EPA ID No
Document No Page 899WASTEMANIFEST
Generators Name and Maihng Address Truck No
4i hFnr
Generators Phone
Transporter Company Name US EPA ID Number Transporters Phone
Designated Fagility Name and Site Address US EPA Number Facilitys Phone
CMS Landfill 704 782-20045105 Morehead Rd
COncord NC 28027
ii Waste Shipping Name and Description 12 Containers 13
No Type QUOntity WtNol
AC
..
Additional Descriptions for Materials Listed Above Handling Codes for Wastes Listed Above
15 Special Handling Instructions and Additional Information
16 GENERATORS CERTIFICATION certify the materials described above on this mahifest are notsublect to federal regulations for reporting proper disposal of Hazardous Wahte
Printed /Typd Name
Sjgnature Month Day Year
17 Transporter Acknowledgement of Receipt of Materials
Printed /Typed Name SIgnature Month Day Year27
18 Transpoller Acknowledgement of Receipt of Materials
Printed Typed Name Signature Month Day Year
19 Discrepancy Indication Space
20 Facility Owner or OpŁator Cerification of receipt of waste materiÆlscoverdd byths manife axdeptis æbed in item 19CMSLandfill
ntiType Name \V Signature \f1 If
Trt/r-V
Please print or type
Form designerJ for use on elite 12 pitbh typewriter
NON-HAZARDOUS
WASTE MANIFEST
Generators Name and Mailing Address
Generators Phone
Transporter Company Name
Transporter Company Name
Designated Facility Name and Site Address
CMS Landfill
5105 Morehead Rd
Concord NC 28027
Waste Shipping Name and Description
15 Special Handling Instructions and Additional Information
4.9eflj2
Truck No 4n
12 Containers 13 14
Total UnitNoTypeQuantityWIIVoI
Handling Codes for Wastes Listed
Lu wASTEtDUSTRlESIN
Generators US EPAID No Mahifest
Docurneh foM4
1t
r-
.i
US EPA ID Number
US EPA ID Number ters Phone
10 US EPA ID Number Facilitys Phone
704 782-2004
.4 ._-------------
--.-...-.-...-.-Additional Descriptions for Materials Listed Above
Printed/Typed Name itu Year
I7I17TransporterAcknowledgementofReceiptofMaterials________________________________________Printed Typed Name
Signature Year
Month1
Day Year
CMS Landfill
Printed /Type Name
TFcflfFl flDV
ALL WASTE..rl DU ST PIE INC
AWl Form 121
T/SID/F/COPY
Please print or type
orm designed for use on elite 12 pitch typewriter 1442NON-HAZARDOUS GeneratorsIJS EPAID No Manifest PageWASTEMANIFESTDqcumentNoof
Generators Name and Mailing Address Truck NoIth
L1
Generators Phone
Transporter Company Name us EPA ID Number Transporterl PhOnp
Transporter Company Name us EPA ID Number Trathporters Phone
Designated FacLllty Name and Site Address io us EPA ID Number Facilitys PhoneCMSLandfiH704782 20045105 Morehead Rd
Concord NC 28027
11 Waste Shipping Name and Dehcription 12 Containers 13 14
Total unitNoTypeQuantityWtlVol
...
-Th --
Additional Descriptions for Materials Listed Above Handling Codes for Wastes Listed Above
15 Special Handling Instructions and Additional Information
16 GENERATOR CERTIFICATION certify the materials described above on this manifest are not sublect to federal regulations for reporting proper disposal of Hazardous Waste
Printed Typed Name Ipature Month Day Year/44 .7 2717TransporterAcknowledgementofReceiptofMaterials
Printed Typed Name gnature//Month
los
Year
18 Transpol-ter Acknowledgement of Receipt of Materials
Printed /Typed Name Signature Month Day Year
19 Discrepancy Indication Space
...............
...-20 Facility Owner or Operathr Cerification of receipt of waste materials cdvŁrdd by this manifest except as nóikf in Item 19CMSLandfifl
Printed/Type Name1...Signature
please printortype
ItALL WAST 1/
Form designed for use on elite 12 pitch typewriter
/-i eTh..NON-HAZARDOUS GC US EPAID No Manifest PageWASTEMAMFESTDocumentNoof 12789.2
Generators Name and Mailing Address
th
GeneratorsPhone
Truck No
j_
Transporter Company Name c.Us EPA ID Number Transporter horLe
Transporter Company Name US EPA ID Number Transporters Phone
Designated Factity Name and Site Address 10.US EPA ID Number Facilitys Phone
CMS Landfill 704 782-20045105MorØdRd
Concord NC 28027
11 Waste Shipping Name and Description 12 Containers 13
No Type Quantity WtNoI
Additional Descriptions for Materials Listed Above E.Handling Codes for Wastes Listed Above
1J
15 Special Handling Instructions and Additional Information
16 GENERATOR CERTIFICATION certify the materials descnbed above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste
Printed /Typed Name ..Signature ......Month Day Yeardt
17 Transporter Acknowledgement of Redeipt of Materials
Printed Typed Name Signature Month Day Year4kk
18 Transporter Acknowledgement of Receipt of Materials
Printed Typed Name Signature Month bay Year
19 Discrepancy Indication Spaàe
20 racility Owner or Operator Cerification of receipt of waste materials covered by this manifest except as noted in item 19CMSLandfill...i
Printed /Type Name Signature
Ti
.T/SIPIF/CQPY
MonUi Day Year
AWl Form 121
ALL WASTEPleaseprintortype
Gæerators PhonepOrter1CompanyName
..i ............
...I
...________________Transporter Company Name
Designated Facility Name and Site Address
1Mi1 ko
16 GENERATORS CERTJFICATIONl certify the naterials described above on this manifest /e not subject to fedraj egulations for reporting poper dipoaal of Hazardou i.Aiaste.rinted/Typed Name
jjgature2 Month ba YearP44PZt717TransporterAcknowledgementofReciptofMaterials
Printed/Typed Name Snaie Month Da Year
18 Transponer Acknowledgement of Receipt of Materials
Pnnted Typed Name SIgnature Month Day Year
l9Dlscrepancy Indication Space
20 Facility Owner or Operator Cerification of receipt of waste materials covered by this manifest except as noted in item 19CMSLandfill
Signature
Manifest
Document No
Truck No
t1t
CMS Landfill
5105 Morehead Rd
Concord NC 28027
11 Waste Shipping Name and Description
US EPA ID Number Transporters Phone
10 US EPA ID Number Facilitys Phone
704 782-2004
Additional Descriptions for Materials Listed Above
15 Special Handling Instructions and Additional Information
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Mailing
P0 Box 7030
Charlotte North Carolina 28241
Physical
3475 Lakemont Boulevard
Fort Mill SC 29708
803.802.2440
Raleigh
14001 Weston Parkway
Suite 100
Cary North Carolina 27513
919.678.1070
Wilmington
2120-B Capital Drive
Wilmington North Carolina 28405
910.313.6648
Concord
4601 Corporate Drive NW
Suite 165
Concord North Carolina 28027
704 793.9855
800.960.7317
www.espassociales.com
ESP Associates P.A