HomeMy WebLinkAboutItem No 26 - NFA Letter - Indcident No 36325 Morehead Common-OCRNCDENR
North Caroflna Department of Environment and Natural Resources
Michael Easley Governor Division of Waste Management
William Ross Jr Secretary Underground Storage Tank Section Dexter Matthews Director
August 2007
Beazer Homes
1300 South Boulevard Suite
Charlotte North Carolina 28203-4265
Attention Jade Eastridge
Re Notice of No Further Action
15A NCAC 2L .0407d
Risk-based Assessment and Corrective Action
for Petroleum Underground Storage Tanks
Morehead Connon-Area
919 West Morehead Street
Meckienburg County
Incident Number 36325
Risk Classification Low
Dear Ms Eastridge
The Initial Abatement Action report received by the Underground Storage Tank UST Section
Mooresville Regional Office on August 2007 has been reviewed The review indicates that after tank
closure and soil removal soil contamination does not exceed the lower of the soil-to-groundwater or
residential maximum soil contaminant concentrations MSCCs established in Title 5A NCAC 2L
.0411
The UST Section determines that no further action is warranted for this incident This
determination shall apply unless the UST Section later finds that the discharge or release poses an
unacceptable risk or potentially unacceptable risk to human health or the environment Pursuant to Title
ISA NCAC 2L .0407a you have continuing obligation
to notify the Department of any changes
that
might affect the risk or land use classifications that have been assigned
This No Further Action determination applies only
to the subject incident
If you have any questions regarding this notice please contact me at 704 235-2172
Sincerely
Allen Schiff
Hydrogeologist
Mooresville Regional Office
cc Shawna Caidwell LUESA-Mecklenburg County Health Department
A1 FU
NED
I...-_
Prepared For
NCDENR
USI Section MRO
919 North Main Street
Mooresviile North Carolina 28115
Prepared By
ESP Associates P.A
P.O Box 7030
ChnrloUe North Carolina 28241
July 30 2007
II
II
ESP AssociaEes P.A
NCDENR
UST Section
Mooresville Regional Office
919 North Main Street
Mooresville North Carolina 28115
Attention Mr Allen Schiff
Reference INITIAL ABATEMENT ACTION REPORT
Morehead Common Site Area No.4
919 West Morehead Street
Charlotte Mecldenburg County North Carolina
UST Incident No No Yet Assigned
ESP Project No E6-UD42.601
Dear Mr Schiff
July 30 2007
On behalf of the property owner Beazer Homes ESP Associates PA is pleased to provide the
attached Initial Abatement Action Report for the closure of the subject propertys petroleum
release ESP respectively requests classification of the release as Low Risk and issuance of no
further action notice
Thank you for your attention in this matter If you should have any questions please
do not
hesitate to contact me at 803 835-0915
Sincerely
ESPAssocji-ites .A
Edgar Rogers
Staff Scientist
cc Jade Eastridge Beazer Homes
P.O Box 7030 Charlotte NC 28241
1.1100.960.7317 NC 704.583.4949 fax 704.583.49 SC 803.802.2440 fax 803.R02.255
Www.espassocjates.com
Environmental Services ManagerNCLicenseNo1600
Initial Abatement Action Report
SITE INFORMATION
Site Identification
Date of Report July 30 2007
Facility ID NA
TJST Incident Number Not Yet Assigned
Site Name Morehead Common Site Area No
Site Street Address 919 West Morehead Street
City/County/Zip Code Charlotte Mecklenburg County 28278
Description of Geographical Data Point Approximate center of UST
Ci Location Method Mecklenburg County Polaris GIS MapLatitude5.2277
Longitude -80.8582
Information about Contacts Associated with the Leaking UST SystemUSTOwnerBeazerHomes
1300 BIvd Suite Charlotte NC 28203-4265
704.370.7200USTOperatorN/A
Property Owner Same as above
Property Occupant Same as above
Consultant/Contractor ESP Associates P.A Chris Ward PGP0Box7030CharlotteNC28241
803.835.0915
Analytical Laboratory Prism Laboratories Inc
P0 Box 240543 Charlotte NC 28224-0403
704.529.6364
NC Certification No 402
Information about Release
ID Date Discovered June 18 2007
Estimated Quantity of Release Unknown
Cause of Release Unknown
Source of Release 350-gallon steel diesel UST
Size and contents of JJST
System from which release occurred 350-gallon steel diesel UST
Chris Ward Professional Geologist for ESP Associates PA do certif that theioncontainedinthisreportiscorrectandaccurateto the best of my knowledge
Associates P.A is licensed to practice both geology and engineering in North CarolinaAssociatescertificationnumbersareGeologyC-347 and Engineering C-0587
JnitialAbatenentAct ion Report ESP Project E6-UD42.601MoreheadcommonSite-Area No .hily 30 2007
INTRODUCTION
The subject site has an address of 919 West Morehead Street in Charlotte Mecldenburg County
North Carolina see Figure Topographic Site Location Map The area of the subject release
associated with an orphan 350-gallon diesel underground storage tank UST uncovered on June
18 2007 has been designated by ESP as Area No of the Morehead Common site
SITE HISTORY AND CHARACTERIZATION
On June 18 2007 ESP responded on behalf of Beazer Homes to an encounter with UST and
petroleum-impacted soil during excavations conducted ahead of mass grading operations at the
subject site Upon arriving at the site ESP observed 350-gallon steel diesel UST and soils with
petroleum-odor located on the south side of West Morehead Street approximately 190 feet west
of its intersection with South Clarkson Street on Tax Parcel No 07325210 see Figures and
As required ESP emailed notification of the release discovery along with Release and fiST
Leak Reporting Form to Mr Steve Bograd of the Mooresville Regional Office of NCDENR on
June 192007
Release Location
The subject site former auto repair facility is located within an urban area of Charlotte which
historically included warehouse and commercial structures Site structures associated with the
former auto repair facility were razed sometime between 2002 and 2005 The site is currently
mass graded with no surface structures present Facility ID No was not available for the site
Based on our review of the Geologic Map of North Carolina 1985 the subject site is located
within the Charlotte Belt locally comprised of intrusive metamorphosed granitic rocks locally
pinkish gray massive to weakly foliated and containing horublende Soils encountered in this
area are the residual product of chemical weathering of rock presently underlying the site Soil
InitialAbatement Action Report ESP Project E6-UD42.601
Iviorehead Common Site -Area No July 30 2007
weathering is more advanced near the surface grading with depth to less weathered rock and
finally bedrock
UST Information
Following the June 18 2007 discovery of the sites 350-gallon diesel UST AD Environmental
and Industrial Services AD of High Point North Carolina was contacted to remove remaining
product/sludge from the tank prior to its removal from the excavation On June 19 2007
AD
pumped less than 10 gallons of product/sludge from the tank for permitted recycling at their
Archdale North Carolina facility see Product Material Manifest in Appendix Once
removed the 350-gallon tank was transported by AD to the Griffin recycling facility in
Greensboro North Carolina on June 19 2007 see Tank Disposal Manifest in Appendix See
site photographs in Appendix
PreviousTankInstallationRemovalSizeTankLastTankTankNoDateDateGallonsDimensionsContentsContents
Unknown 6-18-07 350 6.7 ft ft Diesel Unknown
completed UST-2 Form is included as Appendix The former location of the above UST is
depicted on Figure
Previous Reporting
ESP ernailed release notification along with 24-Hour Release and UST Leak Reporting Form
to the Mooresyille Regional Office of NCDENR on June 19 2007 see Appendix
Additionally ESP submitted 20-Day Report to NCDENR on July 182007
InitialAbaternent Action Report ESP Project E6-UD42.601
Morehead omsnon Site Area No July 30 2007
INITIAL ABATEMENT ACTIVITIES
Initial Contaminated Soil Excavation
On June 19 and 202007 ESP documented the excavation of 196.64 tons of impacted soils from
Area No by the sites grading contractor Gelder Thompson of Midland North Carolina The
excavation was advanced based on results of OVA field screening and evidence of visible
staining The resulting excavation measured approximately 12 ft 28 ft 10 ft deep The
excavated soil was placed on and covered with plastic awaiting subsequent off-site permitted
disposal Neither groundwater bedrock nor free product were encountered within the tank pit
See site photographs in Appendix
Initial Post-Excavation Confirmatory Sampling
On June 19 2007 confirmatory soil samples were collected at depth of feet BLS from each
of the excavations four sides WS-1 through WS-4 while one sample was collected at depth
of 10 feet BLS from the base of the excavation B-I The sidewall samples were collected at
the foot depth due to the prevalence of elevated OVA readings at that depth The five soil
samples were hand delivered on ice to Prism Laboratories of Charlotte North Carolina to be
analyzed for risk-based parameters which include volatile organic compounds VOCs by EPA
Method 8260B semi-volatile organic compounds SVOCs by EPA Method 8270C VPH/EPH
by the Massachusetts Department of Enviromnental Protection MADEP method and for total
lead and chromium by EPA Method 6010B Sample locations and excavation dimensions are
depicted on Figure Soil Sample Location Map Sampling was performed in general
accordance with ESPs SOP see Appendix
Results of the laboratory analysis of confirmatory samples WS-1 through WS-4 and B-i revealed
that all analyzed constituents were either below reporting limits BRLs or below the lowest of
the soil-to-groundwater or residential MSCC with the exception of benzoaanthracene 0.89
mg/Kg benzoapyrene 0.95 mg/Kg benzobfluoranflirene 1.1 mg/Kg and MADEP EPH
Cl 1-C22 Aromatics 130 mg/Kg detected in wall sample WS-3 Laboratory analytical results
InitialAbatwnent Action Report ESP Project E6-UD42.601
Morehead Common Site Area No July30 2007
for the confirmatory soil samples are summarized on Table B-i The Prism laboratory data
report is included as Appendix
Follow-up Contaminated Soil Excavation and Confirmatory Sampling
Due to the detection of elevated constituents above applicable standards in confirmatory sample
WS-3 an additional two feet of soil was excavated from the southern wall of the excavation on
July 2007 Excavated soil was placed on the previous soil stockpile for subsequent offsite
permitted disposal
The resulting excavation measured approximately 14 ft 28 ft 10 ft
deep See Figure for depiction of the excavation limits and sample locations
On July 2007 following excavation of additional soil ESP collected confirmatory soil sample
WS-3 at depth of feet BLS from the southern wall of the excavation Sample WS-3 was
submitted to Prism for analysis of SVOCs by EPA Method 8270C and EPFI by the MADEP
method Results of the analysis of the July 2007 confirmatory sampling revealed that all
analyzed constituents were BRLs see Table B-i The Prism laboratory data report is included
as Appendix
Stockpile Sampling and Soil Disposal
On June 20 2007
ESP collected two composite stockpile soil samples for laboratory analysis
The stockpile soil samples designated iA and lB were placed in laboratory provided containers
labeled and band delivered on ice to Prism for compositing and subsequent analysis The
samples were analyzed for TPH-GRO/DRO by EPA Method 5030/3550 and for BTEX by EPA
Method 8260B The composite samples were collected and analyzed to confirm that release
had occurred and to characterize contaminant types and concentrations for subsequent off-site
permitted disposal/treatment
As revealed by the laboratory analysis of stockpile composite samples 1A and 1B TPH-DRO
was reported at concentrations of 400 and 76 mg/Kg respectively while results for the
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No July 30 2007
remainder of analytes were BRLs Results of the stockpile sample analyses are summarized on
Table B-2 while the laboratory data report is included as Appendix
On July 19 and 20 2007 196.64 tons of stockpiled soil from the excavation was transported by
Gelder Thompson to the CMS Landfill in Concord North Carolina for permitted disposal see
Non-hazardous Waste Manifest in Appendix
RECEPTOR SURVEY
On July 20 2007 Mr Eddie Rogers of ESP performed receptor survey
to document the
presence or absence of active and/or inactive water supply wells within 1500-foot radius of the
subject UST release see Figure Receptor Survey Map The receptor survey included
interviews with available site occupants and visual observations for water supply wells and/or
municipal water meters All properties within 500 feet of the site were visited to determine well
status The area within 1000 feet of the subject release consists of commercial and industrial
development with numerous vacant structures No active or inactive water supply wells were
identified within -a 1000-foot radius of the subject release Municipal water and sewer have
historically been available wiliiin the area of the site Additionally no surface water bodies were
identified within 500 feet of the release see Figure
initial Abatement Action Report ESP Project E6-UD42 601
Morehead onnnon Site.-Area No July 30 2007
CONCLUSIONS AN RECOMMENDATIONS
The following conclusions have been formulated based on our completion of field activities
including abatement activities receptor survey and our review of laboratory data from the
analysis of coilected soil samples
ci The subject site razed former auto repair facility has an address of 919 West
Morehead Street in Charlotte Mecklenburg County North Carolina
On June 18 2007 ESP responded on behalf of Beazer Homes to an encounter with
350-gallon UST and petroleum-impacted soil during excavations conducted ahead of
mass grading operations
at the subject site
ci On June 19 and 20 2007 ESP documented the excavation of 196.64 tons of impacted
soils from the release area The resulting excavation measured approximately 12 ft 28
ft 10 ft deep
ci Neither groundwater bedrock nor free product were encountered within the tank pit
ci On June 19 2007 confirmatory soil samples were collected at depth of feet BLS
from each of the excavations four sides WS-l through WS-4 while one sample was
collected at depth of 10 feet BLS from the base of the excavation B-i
ci Results of the laboratory analysis of confirmatory samples WS-1 through WS-4 and B-i
revealed that all analyzed constituents were either 3RLs or below the lowest of the soil-
to-groundwater or residential MSCC with the exception of benzoaanthracene 0.89
mg/Kg benzoapyrene 0.95 mg/Kg benzobfluoranthrene 1.1 mg/Kg and MADEP
EPH C11-C22 Aromatics 130 mg/Kg
detected in wall sample WS-3
ci Due to the detection of elevated constituents above applicable standards in confirmatory
sample WS-3 an additional two feet of soil was excavated from the southern wall of the
excavation on July 2007 The resulting excavation measured approximately 14 ft 28
ft 10 ft deep
ci On July 2007 following excavation of additional soil ESP collected follow-up
conmatory soil sample WS-3 at depth of feet BLS from the southern wall of the
excavation Results of the analysis of WS-3 revealed that all analyzed constituents were
InitialAbatement Action Report ESP Project E6-UD42 601
More/wad Common Site Area No July 30 2007
BRLs verifying that all impacted soil above applicable standards had been removed from
the excavation
On June 20 2007 ESP collected two composite stockpile soil samples designated 1A
and 113 for laboratory analysis The composite samples were collected and analyzed to
confirm that release bad occurred and to characterize contaminant types and
concentrations for subsequent off-site permitted disposal/treatment
As revealed by the laboratory analysis of stockpile composite samples IA and 1B TPH
DRO was reported at concentrations of 400 and 76 mg/Kg respectively while results for
the remainder of analytes were BRLs
On July 19 and 20 2007 196.64 tons of stockpiled soil from the excavation was
transported to the CMS Landfill in Concord North Carolina for permitted disposal
Municipal water and sewer are available in the area of the release
No water supply wells were identified within 1000 feet of the release and
ii No surface water bodies were identified within 500 feet of the subject release
Based on the absence of analyzed risk-based parameters above the lowest of the North Carolina
soil-to-groundwater or residential MSCCs lack of either groundwater bedrock or free product
within the tank pit the documented absence of water supply wells within 1000 feet of the
release and the absence of surface water feature within 500 feet of the release ESP
recommends that NCDENR issue no further action notice for the subject release
Attachments
Table B-i Summary of Soil Sampling Results
Table B-2 Summary of Stockpile Soil Sampling Results
Figure Topographic Site Location Map
Figure 2005 Aerial Photograph
Figure Soil Sample Location Map
Figure Receptor Survey Map
Appendix 24-Hour Release Notification
Appendix UST-2 Form
Appendix Tank Disposal Manifest
Appendix Product Material Manifest
Appendix Site Photographs
Appendix ESPs SOP
Appendix Prism Laboratory Data Reports
Appendix Non-Hazardous Waste Manifests
ATTACHMENTS
TABLES
Table B-i
Date 7/25/07 Incident No Not Yet Assigned
ii1Si II 9$rk$ie
II ItJ
IIII1
WS-1 6/19/07 NtWth Pt Initial NAWallAbatement
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNLNotListed
Summaryof Soil Sampling Results
Morehead Common Area No Charlotte North Carolina
8015B SOI5B
MADE
EPH
MADE
EPH
MADE
EPH
MADE
VVH
MADE
VPH
MADE
VPH 9071A
tu C-..-
d2
rl .-
NA 13 12
B-l 6/19/07
WS-2 6/19/07 West Pit
Wall
Initial
Abatement NA NA 13 13 13 6.7 6.7 6.7 NA
WS-3 6/19/07 South Pit
Wall
Initial
Abatement NA NA 130 12 12 6.1 61 6.1 NA
WS-3 7/5/07 South Pit
Wall
Initial
Abatement NA NA 11 11 NA NA NA
NA
WS.4 6/19/07 East Pit
Wall
Initial
Abatement NA NA 6.1 1.7 6.1 5.9 5.9 59 NA
NA
Pit Floor NA NA 12 12 12 6.2 6.2 6.2 NA
NIL NL 34 IW 3300 72 34 3300 NL
NL NL 469 93860 9386
939 469 9386 NL
NL NIL 12264 245280 24528 12264 245280 NL
Summaryof Soil Sampling Results
-ned Morelaead Common Area No.4 Charlotte North Carolina
6010B 6010B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B
ç5
.o
fl LE
29 48 0.0056 0.011 0.0056 0.0056 0.0056 0.0056 0.0056
WS-2 6/19/07 West Pit
Wall
Initial
Abatement 28 37 0.0053 0.0053 0.0049.1 0.0053 0.0053 0.0053 0.0023 00053
WS-3 6/19/07 South Pit
Wall
Initial
Abatement 46 110 0.0022 0.0053 0.013 0.053 0.0053 0.0053 0.0053 00053
WS-3 7/5/07 South Pit
Wall
Initial
Abatement NA NA NA NA NA NA NA NA NA NA
WS-4 6/19/07 East Pit
Wall
Initial
Abatement 28 22 0.0053 0.011 0.055 0.055 0.055 0.055 0.055 0.055
2.2 1.7 0.58
0.0048 0.0048 0.0048 0.0048
3.3 4.3
47 400 3128 626 313 1564 626 626 782 782
1226 400 81760 16350 8176 40880 16350 16350 20440 20440
Table B-i
71c/7
WS-1 6/19/07 North Pit
__________Wall
Initial
Abatement 0.0056
B-i 6/19/07 Pit Floor 32 23 0.0048 0.0048
27 270
0.0048 0.0048
3RL Below Leporthig Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNLNotListed
Summaryof Soil Sampling ResultsTableB-i
Date 7/25/07 Incident No Not Yet Assigned
lBIiI1p1couiainoioncern
ii iii
WS-1 6/19/07 North Pit Initial
__________Wall Abatement
Morehead Common Area No Charlotte North Carolina
827CC 827CC 827CC 8270C 827CC 827CC 827CC 827CC 8270C 8270C
c1._.1 ..Li
cia
CBQa
OBNQ.a .a
0.39 0.58 0.39 0.39 0.39 0.39 0.39 0.39 0.39 0.39
WS-2 6119/07 West Pit
Wall
Initial
Abatement 0.32 0.63 0.44 0.44 0.44 0.44 0.44 0.44 0.44 0.44
WS-3 6/19/07 South Pit
Wall
Initial
Abatement 0.83 2.1 0.33 0.133 0.24 0.41 0.24 0.14 0.33 0.33
WS-3 715/07 South Pit
Wall
Initial
Abatement 035 0.36 0.36 0.36 0.36 0.36 0.36 0.36 0.36 0.36
WS-4 6/1907 East Pit
Wall
Initial
Abatement 0.40 0.40 0.40 0.40 0.40 0.40 0.40 0.40 0.40 0.40
O.30 0.49 0.173 0.40 0.40 0.12
3.3 290 44 1.7 11
0.40 0.11 0.20 0.51
12264 16400
BRL Below Reporting LimitMSCCmaximumsoilcontamination conceniration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNLNotListed
0.88 469 620 63 469 4600 0.088 62 88 620
1000 0.17 4.7 38 280
1635 12264 122000
0.78 1635 780 16400
EitL Below Reporting LimitMSCCmaximumsoilcontamination concentration
ft BGS feet below ground surface
Results reported in mg/kg unless otherwise noted
Health based level 100%
Considered immobileNANotAnalyzedNL Not Listed
Table B-2 Summary of Stockpile Soil Sampling Results
Yet Morehead Common Area No Charlotte North Carolina
composite jAbatetment
8015B 8015B 8260B 826DB 8260B 8260B
E-E-r.z
400
InitialcompositeAbatement
1.2 3.7
76
6.2
1.2
6.2
3.6
NL
6.2
6.0
NL
6.0
0.0056 7.3 4.6
NL NL
NL NL 18 3200 1560 3129
164 82000 40000 81760
FIGURES
FiGURETOPOGRAPHIC7E LOC.4 liON MAPUSGSCH4RLOT7E_EAST QUADRANGLE
MOREIIEAD COMMON 7ECHARLOTTE NORTH CAROLINA ESP
26O7ET
TITLE fiGURE
tSP AsteI41 PA2005AERiALPHOTOQRAPFI
PROJECT ESP_______________3475 300111 flhd
Fool Mift SC 517111_____MOREHEAD COMMON ShiE
___________________7D4-3-454H$CCHARLOTTENORTHCAROLINA
WESTMOREHEj STREET
LEGEND
CONF7FWA TORY SOIL SAMPLE LOCA 770W
AREA EXCA VA 770W 0E77H OF 10 FEET
AREA EXCAVATiON DEPTh OP 10 FEET
AREA
20
APPROXIMATE SCALEINFEET
JSP Suctatcs PAPD70315
Chkfl.7.t SS4I
3475 W.dFboMOSC705
704.033.99 IND
WWWaflantcrjflaxfl
/AREA
WS-4 WS-2
WS-4 WS-2
WS-3
SOIL
MCYEHE140 COMMON SflEHARLO11ENORCAROIJIJA
ESP
7/
ioo
RECEPTOR SREY MAP
MORE HEAD COMMON snr
CHARLOTIE NORTH CAROLINA
ESP Assj tes Pd.ESP
APPENDiX
24-HOUR RELEASE NOTIFICATION
UST61 eaedLeak Reporting Form
For Releases This farm should be completed arid submitted to the LIST Sections regIonal office following known or suspected release from
an underground storage tank UST system This farm Is requbed to bE submitted within 24 hours ordiscovery or known orinNCsuspectedrelease
DWM USE ONLY Suspected Conlarninatlon Y/N Facility ID Number N/AlncldentRiskHiLU______Confirmed OW ContamInation Y/N Al Date Leak Discovered iQrl
Received On_______Received By_______Confirmed Soil Contarninalion Y/N CommWnn-Cemmerdal 4rItM
Reported by aim/c one Plione Fax or Report x.Free Product YIN J.L If Yes Slate fraatest ReglNonregulaled
Region ..Thickness
INCIDENT DESCRIPTION
Incident Name
Address MaitkJ 61-Counh Uec1fthw
City/Town f.i jJ Zip Code Regional Office auth one AshevIiIayeilev1ji
Raleigh Washington Wilmington Winsta1eiiT
1.atituzie inI dnsus 51 7731 Longitude cinwemos ..-Obtained by
Briefly describe suspected or confirmed release including but not limited to nature of release date of release amountofreleaseamountoffreeproduct present end recovery ollbrls initial responses conducted impacts Ic receptors
157__4_j_Topographlo map41018Addressmatching
DOther.7
tin lcnownhei4745JDescribelocation
HOW RELEASE WAS DISCOVERED
C/wch one
DurIng I/ST Closure/Removal Water fri Tank Surface Water ContamInatIon
Release Detection Equipment or Methods Visual/Odor Groundwater Contamination
Property Transfer CI Water Supply Wail Contarnhiatlom %ther specUy JJ
O11mSOURCEOFCONTAMINATION
Primary Source of Contamination Primary Contaminant Time Location ttinq
Check one Check one Check onei_Gasciine1Diesel/cerne Facility ResidentialConfirmedUSTReleaseCbeckonebelowitctinOilCIResidenceinsiustriatCIDispenserOilierPetroleum Products Other OirbanlineRelease
Cl Rural-CTank Release
Other Inorganics
Spill/Overfill Other OrganicsExactFailureLocationUnknownor
Mu1lite Failures
wnarshio
MunIcipal Military Unknown Federal County Slate
Oeratbn Tvua
PubllcServlce Agricultural EducationtRelig Industrial Mining
UST Forrir 61 11105
Page oF
IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected Ves No
Number of Water Supply Wells Affected________________
Water Supply Wells ContamInated include Users Names Addresses and Phone Numbers Attach eddlilo nat sheet fnacessaiy
UST SYSTEM OWNERUSTOwnarlCompany
$2L24/
LANDOWNER AT LOCATiON OF UST INCIDENT
Draw Sketch of Area showing two major road intersections or Attach Map
Person Reporikig Incident dc Company pç Telephone NumbeQg.Address Po-1o3L7 ChAwL 32.c/DateUSTForm6111/05
Zip 00e Telepnone Number2-o-%Z-3i.-7a
UST SYSTEM OPERATOR
Point Of
Cofltacr
City
Nc-
UST Operaioriompany
StateCity
AddmssiodJcL
Address
Zip Code Telephonó Numeer
LandownerS1c q-Address
City State Zip Code eiepnone Number
Pa9e of
777LE AREAS NO AND ESP rIPJ4LE
2005 SITE MAP
Wh.$Cfl924tIWth.7l
___________mt Mw.3CflU
U$N 8TDMf PROJECT .MOREHEAD COMMONS 7E 74UIUD
___QIARLOTTh W0I7H CAROL WA
APPENDIX
UST-2 FORM
Of UST
Return completed form to STATE USE ONLYTheDWMRegionalOffice located in the area where the factity Is located Send copy to the Central Office in Raleigh that _________________the status of the tank may be changed to PERMANENTLY CLOSED and your tank fee account can be closed outSEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES Reesived
lNSTRUTIONs READ THIS FlRS
For more than five UST systems you may attach additional forms as needed
Permanent closure For permanent closure complete all sections of this form
Change-in-service For change-in-service where UST systems will be converted from containing regulated
substance to storing non-regulatedsubstancecompletesectionsIIIllIVandVHf
Effective February 1995 all UST closurelchange-in-service reports must be submitted in the format provided in the UST-1 form UST closure andchange-in-services must be completed in accordance with the latest version of the Guidelines for Tank Closure copy of the UST-12 form and theGuidelinesfarTankClosurecanbeobtainedatwww.wastenotnc.org
You must make sure that USTs removed from your property are dflsposed of properly When choosing closure contractor ask where the tanks will betakenfordisposalUsuallyLISTsarecleanedandcutupforscrapmetalThisisdangerousworkandmustbeperformedbyqualifiedcompanyTanksdisposedofillegallyin fields or other dumpsites can leak petroleum products and sludge into the environment if your tanks are disposed of Improperly youcouldbeheldresponsibleforthecleanupofanyenvironmentaldamagethatoccursNOTEIfrelease from the tanks has occurred the site assessment portion of the tank closure must be conducted under the supervision of P.E orLGwithallclosuresiteassessmentreportsbearing the signature and seal of the P.E or LG
OWNERSHIP OF TANKS LOCATION OF TANKSOwnerNameCorporationIndivIdualPublicAgencyorOtherEntityFacilityNameorCompanyBeazerHomesWA
Street Address
Facility ID If known1300BoulevardSuiteNA
City County Street AddressCharlotteMeaktenburg919WestMorehead StreetStateZIpCodeCity County Zip CodeNC28203-4265 Charlotte Mecklenburg 28278Phone Number Phone Number704470-7200
lii CONTACT PERSONNELContactforFacilityJobTitle Phone NoN/A
Closure Contractor Name Closure Contractor Company Address Phone NoJimStrattloidGelderThompsonBox288MIdlandNC28107704-269-0070Primary Consultant Name Primary Consultant Company Address Phone NoChrisWardPGESPassociatesP.A P0 Box 7030 Charlotte NC 28241 704-802-2440IVUSTINFORMATIONFORREGISTEREDLISTSYSTEMSEXCAVATIONCONDITIONTankSizeinTankLastLastUsePermanentChange-in.Wteln Free liotableodororvislbleIDNoGallonsDimensionsContentsDateCloseDateServiceesOtloflsoilcenr-idnaljonYeslbYeslbY55ItoDate0_DODDDoD_uDO000000aD_o __DO DODD
Tank Owner Welerle Free
_________excsvstjo .__.aoduct
________________Yes Ito Yes Ito Yes___Dj1___DDDDD___DO DODDODD
if the tank owner address is different from the one fisted in Section then enter the street address city state zip code and telephone no below
VIII CERTIFICATION
certify under penalty of law that have personally examined and am familiar wIth the Information submitted In this and all attached documents and thatbasedonmyinquiryofthoseIndividualsimmediatelyresponsibleforobtainingtheInformationthatthesubmittedInformatIonIstrueaccurateandomplete
nnt name and official title of owner or owners authors
Thristopliei-.1 Ward Department Manager ES Associates P.A
Tank
ID No
VI usi
Size In
Gallons
350
Jt-ORMATIC
Tank
Dimensions
6.7 ft 3ff
FOR UNREGISTERED LIST SYSTEMS
Last
Contents
Dielsel Oleis
Last Use
Date
Permanent
Close Date
VII CAvATI CON ITION
Ilctabte odor or visible
soil
_______No
___
_____-D
___
APPENDIX
TANK DISPOSAL MANIFEST
Environmental and Industrial ServicesIEP.O Box 484 High Point NC Phone 336 434-7750 FAX 336 434-7752
TANK DISPOSAL MANIFEST
Tank OwnerlAuthorzed Representative Name and Mailing Address _________________________________
LI
C1ct-tohfe ..itc LJ
Tank Owner/Authorized Representative Contact
Description Of Tanks
Tank No Capacity Previous Contents Comments
.........
TankOwner/Authorized Representative Certification The undersigned certifies that the above listed storagetankshavebeenremovedfromthepremisesofthetankbner2/
rinted/Typed Wame Signature Month/Day/Year
Transporter The undersigned certifies that the above listed storage tanks have been transported to ADEnvironmentalandIndustrialServices2718iJwharrieRoadArchdaleN.C 27263 //Q.--7fPrisPuedTypedNameSjgnaure Month/Day/Year
Disposal Certification The undersigriedcertifjes that the above-named storage tanks have been cutintoscrap pieces and accepted by
the metal recycling facility
Recycling Facility -L rcr7 1.rc 4C
MoTh/Dajiier
APPENDIX
PRODUCT MATERIAL MANIFEST
APPENDIX
SITE PHOTOGRAPHS
MOREHEAD COMMON SITE AREA NO
VIEW OF 550-GALLON LTST FROM AREA NO.4 VIEW OF VISIBLY IMPACTED SOiL FROM EXCAVATION INAREANO.4
VIEW OF VISIBLY IMPACTED SOIL FROM EXCAVATION INAREANO
VIEW OF LEAKING 550-GALLON UST FROM AREA NO
APPENDIX
ESPS SOP
STANbARb OPERXrIN PROCEbURE
SOP-
SOIL SAMPLE COLLECTION
ESP Associates PA Revision bate 3/7/06
This standard operating procedure SOP covers The collection of soil sample for
laboratory analysis Follow these steps when collecting the soil sample unless
otherwise instructed by the project manager
Gather needed field supplies noted below
Confirm lab cooler contains needed sample containers fill cooler with
ice
Upon arriving at site check in with the property owner or company
representative
becontaminate the stainless steel hand auger before and between sample
collection by washing with Alconox soap and scrub brush1 rinsing with
distilled water and spraying with Isopropyl alcohol Wrap clean sampler
in aluminum foil
Wear disposal latex or nitrite gloves and change into new pair between
samples
buring advancement of the hand auger collect soil samples at regular
intervals for describing lithology Note lithotogy arid other
characteristics of soils in field book relative to depth
tf appropriate place representative portion of soil sample into
resealable plastic bag label with boring number and depth interval and
allow to equilibrate Screen soil in bag for volatile orgcinics using an OVA
or I-mu Enter results into field book
Advance hand auger boring to previously specified sampling depthCollectsoilsamplefromthisdepthandplaceinlaboratoryprovidedcontainersLabelcontainers with boring number and sample depth usingthefollowingsamplingschemei.e B-i ft B-i 10 ft B-2 ft etc
beriote boring location in field book relevant to pertinent site features10Followingcollectionofthesoilsamplesabandonallboreholesfeet or
greater in depth with cement grout
11 Complete and sign the labs chain-of-custody12KeepThesamplecoolerinsecurelocation until delivered under normal
chain-of-custody procedures to laboratory
SOP-6 Soil Sample Collection Revion Date 3/7/06ESPt4ssociafegPageof
5UPPLIES
SOP-6
ci Stainless steel hand auger with needed extensions or sampling
spoon
ci OVA orknu
Measuring tape
ci Plastic zip-lock bags
Isopropyl alcohol
ci Distilled water
ci 5-gallon wash bucket scrub brush and Alconox soap
ci Cement with wheel barrow for mixing
ci Cooler with sample containers and chain-of-custody
Ice
ci Permanent marker
El bisposable gloves
ci Knife
ci Field book
ci Site plan with Site Specific sampling instructions
ci Camera
APPENDIX
PRISM LABORATORYDATA REPORTS
JUL Zt2c
Case NarrativeRISM
LABOATORIEsINc
Date 06129/07 Client Project ID Morehead Conimcns No.4CompanyESPAssociatesPAPrismCOCGroupNoG0607542ContactChrisWardCollectionDates06/19107AddressBox 7030 Lab Submfttal Dates 06119/07
Charlotte1 NC 28241
This data package contains the analytical results for the project identified above and Includes Case Narrative Laboratory Report and QualityControlDatatotaling48pageschairi-of.custody is also attached for the samples submitted to Prism for this project
Data qualtilers are flagged individually on each sample key
reference for the data qualifiers appears at the end of this case narrative Qualitycontrolstatementsand/or sample specific remarks are included in the sample comments section of the laboratory report for each sampleaffected
Semi Volatile Analysis
No Anomalies Reported
MatiIe AnayLs
Analysis Note for 024604 MSD C9-C12 Aliphatics Recoveiy above the control UmilsisAnalysis
Analysis Note for Q24519 Method Blank Lead MB Is greater than 025 mg/kg
Wet Lab and Micro Analysis
N/A
Please call if you have any questions relating to this analytical reportDateReewedbyT9T
Review Date
Approval Date 06/29/07ataQualifiersKeyReference
Compound also detected In the method blank
Result outside of the QC limits
DO Compound diluted out
Estimated concentrallon calibration range exceededTheanalytewaspositivelyidentifiedbutthevalueIs estimated below the reporting limitEstimatedconcentratonwithhighbias
Estimated concentration with low bias
matrix effect Is present
Notes This report should not be reproduced1 except In its entirety without the writtten consent of Prism Laboratories1 Inc The results In thisreportrelateonlytothesamplessubmittedlbranalysis
449Spttngboaç Road P.O Box 240543 Chadotte NC 28224-0403
Phone 704/529-6354 ToN Free 8001529-6364 Fax 704152544Q9
SCCertlflcatlon No 99012 Laboratory ReportNCDrinkingWaterCartNo3773506/29/07
ESP Associates PA Prqject ID Morehead Commons No Client Sample ID WS-1ttnChrisWard
Prism Sample ID 184952.0 Box 7030 Sample Matrix Soil COC Group G0607542TharlotteNC28241TimeCollected06119/07 1608
Time Submitted 06/19/07 1735
parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time
ercerit Solids Determination
ercent SolIds 83.3 SM2540 06/25/07 1745 Lthao
ample Weight Determination
eight Blsutfate 5035 06/27/07 000 brown
eight Bisulfate 5.33 5035 06127107 000 brown
eight Methanol 5.36 5035 06/27/07 000 Ibrown
atlle Organic Corn pDunds by C/MS
l1-Trlchloroethane BRL mg/kg 0.0056 0.00032 826DB 06/23/07 1640 erussefI 024503
l22-Tetrachloroethane BRL mg/kg 0.0056 0.00057 8260B 06/23/07 1640 erussell 024503
I2-Tdchloroethane SRI mg/kg 0.0055 0.00035 825DB 06/23/07 1640 erussell 024503t-Pkthloroethane ....BL mg/kg .000560.00041 .62608 06/23/07 1640 erusseII Q245o3
1..Q245D3
DIchIoropropene BRL mg/kg 0.0056 0.0005 825GB 06123/07 1640 ewssell 0245033-Trlchlombenzene BRL mg/kg 0.0056 0.00062 8260B 05/23/07 1640 erussell 024503
.3-TrichIoropropane BRL mg/kg 0.0056 0.0005 82608 06/23/07 1640 erussefl Q245034-Trlchlorobenzene BRL mg/kg 0.0056 0.00054 826DB 06123/07 1640 erussell 024503
4-Trlrnethylbenzene BRL mg/kg 0.0056 0.00043 826DB 06/23/07 1640 erusset 024503DibromoethaneEDBBRLmg/kg 0.0058 0.0001 82603 06/23/07 1640 erusseH 024503DlchlorobenzeneBRLmg/kg 0.0055 0.0003 82603 06/23/07 1640 erusseli 024503DlchloroethaneSRImg/kg 0.0056 0.00056 8260B 06/23/07 1640 erussell Q24503DiohioropropaneBRLmg/kg 0.0056 0.00042 826GB 06/23/07 1640 erussell Q24503STrImeLhylbenzeneBRLmg/kg 0.0056 0.00047 826DB 06/23/07 1640 erussell 024503DlchlorobenzeneBRLmg/kg 0.0056 0.00048 82608 06/23/07 1640 erusseli 024503DichloropmpaneBRLmg/kg 0.0056 0.00038 826DB 06/23/07 1640 erussei 024503DichlorobenzeneBRLmg/kg 0.0056 0.00044 826GB 06/23/07 1640 erusseli 024503DichioropropaneBRLmg/kg 0.0056 0.00028 82603 05/23/07 1540 erussell 024503dorotolueneBRLmg/kg 0.0056 0.00042 826GB 06/23/07 1640 erussell 024503Thisreportshould not be repraducej except In Its enflrety without the written consent of Prism Laboratories Inc449SprlngI-ocj Road PO Box 240543 Charlotte NC 28224-0543PhonD7041529_6354 Tofl Free Number 1-80aJ529.63 Fax 704/525.0409 Page of 35
ESP Associates PA
\ttn Chris Ward
Box 7030
harIotte NC 28241
Laboratory Report
06/29/07
wS-1
184952
G0607542
06/19/07 1600
06/19/07 1735
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
PrIsm Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
ID
-Hexanone mg/kg eru5selI
-Chiorotofijene
Melhyl-2-pentanon MIBK
cetorie
enzene
ramobenzene
romochioromethane
rornodichloromethane
omofomi
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
0.0056
0.056
0.056
0.0034
0.0056
0.0056
0.0056
0.0056
0.011
0.00029
0.00056
0.0022
0.00045
0.00039
0.00034
0.0005
0.00042
0.00055
0.00033
826DB
826DB
526GB
82606
82606
826DB
82606
826DB
82508
826GB
06/23/07 1640 ewsseJJ
06/23/07 1640 eruseH
06/23/07 1640 erusset
06/23/07 1640 erusseIl
0623/07 1640 erussell
06/23/07 1640 erussell
06123/07 1640 arussell
06/23/07 1640 arussefl
06/23/07 1640 Orusseil
06/23/07 1640 erussell
024503
024503
024503
024503
024503
024503
024503
024503
024503
024503mg/kg 0.0056
omomethane
3rbon tetrachioride
orobenzee BRLrng/kg 0.P0560.00043 18260 00I23LP7-1.40.erusseII 024503BRrUOO5000038826DB--
024503
iloroeliiane
ilomform
doromethane
iZ-Dlthloroethene
-l.3-Dlchioropropene
hlorodlfluoromethane
iylbenzone
propyl ether IPE
propyIbenzan
-Xylenes
Ihyl ethyl ketone MEK
Ihyl t-butyl ether MTBE
thylene chloride
utylbenzene
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
0.011
0.0056
0.0056
0.0056
0.0056
0.0056
0.0056
0.0056
0.0056
0.011
0.11
0.011
0.0056
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/hg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
06/2307
06/23/07
06/23/07
0623/07
0612307
06/23/07
06/23/07
06/23/07
06/23/07
0.00046
0.00042
0.00039
0.00025
0.00035
0.0013
0.00039
0.00019
0.00045
0.00079
0.0016
0.00033
0.00045
1640 erusseil
1640 elusseji
1640 erusseIl
1640 erusse2j
1640 erlisseIl
1640 erussell
1640 enissell
1640 erussell
1640 erussell
826DB
82608
82603
826DB
82606
826DB
625DB
82606
826DB
82606
826DB
82608
82608
82606
024503
Q2450a
024503
024503
024503
024503
024503
024503
Q24503
024503
024503
024503
024503
024503
0.0056 0.00045
06/23/07 1640 erusseJi
06/23/07 1640 erussell
06/23/07 1640 erussejj
06/23/07 1640 erussefi
05/23/07 1640 erussell
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories lc449SprlngbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-5354 Toll Free Number 1-800/529.6364 Fax 704f525-4o9 Page of 35
ESP Associates PA
\tth Chris Ward
Box 7030
hariotte NC 28241
Project ID Morehead Commons No ClIent Sample ID
Prism Sample ID
Sample Matrix Soil coc Group
Time Collected
Time Submitted
ws-1
184952
G0607542
06119/07
06/19/07
Iaphthaiene
-Xylene
-Isopropyltoluene
se-Butylbenzene
lyrene
rt-Butyibenzene
trachloroethene
luene
ms-I 2-Dlchloroethene
ms-i .S-Dichloropropene
Date/Time
06/23/07 1640 erussefi
06/23/07 1640 eruss
06/23107 1640 erussell
06/23/07 1640 erussell
06/23/07 1640 erussell
06/23/07 1640 erussefi
06/2307 1640 erussell
06/23/07 1640 erussell
08/23/07 1640 erussefi
06/23107 1640 erussell
05/23/07 1640 erussefl
ID
024503
Q24503
024503
Q24503
024603
Q24503
Q24s03
024503
Q24503
024503
024503
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
ararneter Result Units Report
1600
1735
MDL Dilution Method Analysis Analyst Batch
Limit
-Propylbenzene BRL mg/kg 0.0056 0.00034
BRL mg/kg 0.011 0.00065
BRL mg/kg 0.0056 0.00034
BRL mg/kg 0.0056 0.00046
BRL mg/kg 0.0056 0.00031
BRL mg/kg 0.0056 0.00056
RRL mg/kg 0.0056 0.00035
BRI mg/kg 0.0056 0.00097
BRL mg/kg 0.0056 0.0003B
BRL mg/kg 0.0056 0.00043
BRL mg/kg 0.0056 0.00039
Factor
82608
826DB
826GB
82606
82608
82608
826DB
826DB
82606
82608
826DB
ichioroethene....0lg/k 0.00560.000341 .82508 06/23/0 i6 erussell -Q24503DiF
nyl acetate BRL mg/kg 0.028 0.0020 826DB 06/23/07 1640 erusset 024503ylchlorideBRLmg/kg 0.0056 0.00072 82508 06/23/07 1640 erusseli 024503
Surrogate Recovery Control Limits
Bromofiuorobenzene 92 77-128
Dibromofluoromeane 79 67-143
Toiuene.J8 85 81 128
iI-votatlie Ornanic Compquncjs bGC/MS
.4-Trlchlorobenzene BRL
-Dlcjiiorobenzene BRL
-Dlchlorobenzene BRL
Dlchiorobenzene BRL
5-Trichtorophenol BRL
6-Trichlorophenoi BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
0.39
0.39
0.39
0.39
0.39
0.39
0.039
0.029
0.028
0.038
0.040
0.038
8270C
8270C
8270C
8270C
8270C
8270C
06/26/07 1737 kcampigoijo
06/26/07 1737 kcamplgotto
06/26/07 1737 kcsmplgotto
06/26/07 1737 kcamprgotto
05/26/07 1737 kcsmplgoflo
06/2607 1737 kcampigotin
024532
024532
024532
024532
024532
024532
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc449SprlngbrookRoadP.O Box 240543 Charlotte NC 28224.0543Phone704/529-6364 Toll Free Number 1-800/529.6354 Fax 704/525-0409 Page of 35
NC Certification No 412
SC Certjfjcatjn No 99012
NC Drinking Water Cart No 37735
ESP Associates PA
Project ID Morehead Commons No Client Sample ID WS-1ttnChrisWard
Prism Sample ID 184952Box7030SampleMatrixSoilCOOGroupG0607542har1otteNC28241
Time Collected 06/1 9/07 1800
Time Submitted 06/19/07 1735
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
.4-Dimethyiphenol BRL mg/kg 0.39 0.038 82700
4DinItrophenoJ BRL mg/kg 2.0 0.044 82700
4-Dlnflrotcluene BRL mg/kg 0.39 0.022 82700
C-Dinifrotoluene BRL mg/kg 0.39 0.042 8270C
Chloronaphthaiene BRL mg/kg 0.39 0.041 82700
Chiorophenol BRL mg/kg 0.39 0.031 82700
Methylnaphtfalene BRL mg/kg 0.39 0.031 82700
Methyiphenol RRL mg/kg 0.39 0.037 82700
Jitrophenol BRL mg/kg 0.39 0.047 82700
4-Methylpheno BRL mg/kg 0.39 0.040 82700
LPrnbenzldfrIe BRL mg/kg 079 0025 82700 0626/07 1737 kcampigotio Q24s
lromophenyIphenyle BRE mg/kg 0.39 0.037 8270C
htoro-3.methyJphenoi BRL mg/kg 0.79 0.029 82700
hioroanitine BRL mg/kg 0.39 0.050 8270C
hIorophenylphery BRL mg/kg 0.39 0024 82700
Itrophenol BRL mg/kg 2.0 0.026 827CC
naphthene BRL mg/kg 0.39 0.039 82700
naphthyjene BRL mg/kg 0.39 0.039 8270ClmceneBRLmg/kg 0.39 0.030 82700benzeneBRLmg/kg 2.0 0.035 8270C
zoaanthracane 0.31 mg/kg 0.39 0.055 82700wapyrene0.32 mg/kg 0.39 0.046 82700
wbfluoranthene 0.45 mg/kg 0.39 0.018 82700
oghiperylene 0.22j mg/kg 0.39 0.019 8270Cokfluoranthene0.27 mg/kg 0.39 0.032 8270C
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
44 Sprlngbroop Road P.O Box 240543 Charlotte NC 28224-0543Phone704/529-6354 Toll Free Number 1-800/529.6354 Fax 704/525.0409
Laboratory Report
06/29/07
06/2607 1737 kcampigotto
06/26/07 1737 kcaniplgotto
06/26/07 1737 kcamplgotto
06/2607 1737 Icarnpigotto
06/26/07 1737 kcamplgotto
06/26/07 1737 kcampigolb
06/26/07 1737 kcamplgotto
06/26/07 1737 kcampigouo
06/26/07 1737 kcampigouc
0626/07 1737 kcampigottc
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
0626/07 1737 kcamplgouo
0626/07 1737 kcampigoj
06/2607 1737 kcamplgoito
06/26/07 1737 kcanpigo
06/26/07 1737 kcampl9o
06/26107 1737 kcarnpigoto
06/28/07 1737 kcampigotto
06/25/07 1737 kcamplgoo
06/26/07 1737 kcamplgouo
06/26/07 1737 kcampigoito
05/26/07 1737 kcamplgo
06/26/07 1737 koamplgotia
06/26/07 1737 kcamplgoft0
06/26/07 1737 kcampigottD
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
Page of 35
NC Cerllflcàtlon No.402
SC Certification No 99012
NC Drinking Water Cert No 37735
SP Associates PA
Project ID Morehead Commons No Client Sample ID WS-1ttnChrisWard
Prism Sample ID 184952.0 Box 7030 Sample Matrix Soil COO Group G0607542harlotteNC28241TImeCollected06/19107 1600
Time Submitted 06/19/07 1735
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
nzyl alcohol BRL mg/kg 0.79 0.042 82700 024532s2_chiDroethoxymethe BRL mg/kg 0.39 0.045 82700 024532
s2-chloroethylether BRL mg/kg 0.39 0.043 82700 024532
s2-chlorolsopropylether BRL mg/kg 0.39 0.034 8270C 02453232-ethyIhexylphaJa BRL mg/kg 0.39 0.019 82700 024532tytbenzyfphthafateBRLmg/kg 0.39 0.024 82700 024532rysene0.37 mg/kg 0.39 0.066 9270C 024532n-butylphthatate BRL mg/kg 0.39 0.018 82700 024532fl-octylphthalate BRL mg/kg 0.39 0.029 8270C 024532IenzoCahanthraceneBRLmg/kg 0.39 0.040 82700 024532enzofuranERLmg/kg 039 0034 8270C 06/28/07 17 37 kcampJo 024532
Iethyfphthalaje BRL mg/kg 0.39 0.027 82700
ranthene 0.65 mg/kg 0.39 0.027 82700
rene BRL mg/kg 0.39 0.023 82700
achiorobenzena BRL mg/kg 0.39 0.020 82700
achlorobudiene RRL mg/kg 0.39 0.038 82700
achlarocyclopentadiefle HRL mg/kg 0.39 0.042 8270C
schloroethane ORL mg/kg 0.39 0.040 82700
flol23-cdpyrene 0.39J mg/kg 0.39 0.040 82700
horone BR mg/kg 0.39 0.035 82700
trasodl.n-pmpylamine BRL mg/kg 0.39 0.045 8270C
trosodlphenylamlne BRL mg/kg 0.39 0.020 8270C
rihalene BRL mg/kg 0.39 0.043 82700
benzene BRL mg/kg 0.39 0.038 82700
3chforophenol BRL mg/kg 2.0 0.033 82700
This report should not be reprcducJ except in Its entirety without the written consent of Pnsm Laboratories Inc449SprIngbroojRoadP.O Box 240543 Chariofte NC 28224..Q3Phone704/529.6364 Toll Free Number 1-800/529-6354 Fax 704/525-0409
IIVkDAIIUL__..JImnmDntaI SbbUon
Laboratory Report
06/29/07
06/26/07 1737 kcamplgcuo
06/26/07 1737 kcamplgotb
06/26/07 1737 kcampigotlo
06/26/07 1737 kcampigoilo
06/26/07 1737 kcampiottc
06/26/07 1737 kcamplgotio
06/26/07 1737 kcamplgotto
06/26/07 1737 kcamplgatto
06/26/07 1737 kcampigottc
06/26/07 1737 kcamplgotto
06/26/07 1737 kcamp1gott
06/26/07 1737 kcamplgotto
06/26/07 1737 kcampIgo
06/26/07 1737 kcampjgotk
00/26/07 1737 kcamptgotto
06/26/07 1737 kcamplgouo
06/26/07 1737 kcamplgotto
06/26/07 1737 kcamplgotio
06/26/07 1737 kcampigotto
06/26/07 1731 kcamplgotto
06/26/07 1737 kcmplgtto
06/26/07 1737 kcamplgotin
06/26/07 1737 kcmplo
06/26/07 1737 kcamplgoiiu
Q24532
Q24532
024532
024532
024532
024532
Q24532
024532
024532
024532
024532
024532
024532
024532
Pages of 35
Laboratory Report
06/29107
Project ID Morehead Commons No Client Sample ID WS-.1
Prism Sample ID 164952SampleMatrixSoilCOCGroupG0607542
Time Collected 06/19/07 1600
Time Submitted 06/19/07 1735
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
henanthreno 0.38 mg/kg 0.39 0.019 8270C 05126/07 1737 kcamptgotta Q24532henolBRLmg/kg 0.39 0.043 8270C 05/2607 1737 kcamplgotia 024532
yrene 0.58 mg/kg 0.39 0.027 8270C 06/26/07 1737 kcamplgotto 024632
Sample Preparation
355DB 06/22/07 1100 dpope P18710
Surrogate Recovery Control Limits
214.6-Tdbromophenol 102 25 123
2-Fluombiphenyf 84 21 108
2-Fluorophenol 66 14 89
Nitrobenzene-d5 71 14-103
Phenol-d5 77 13-95
jTerphenj4
thbie Petroleum Hydrocarbons by GC-FID1-C22 Aromatjcs 13
9-C35 Aliphaijos
-C18 Aflphatics
mg/kg
BRI mg/kg
BRL mg/kg
Ara1ysjs ITote far Cll-C22 Aromatics
Sample Preparation
Surrogate Recovety Control Limits
o-Terphenyl 76 40-140
l-Chloro-octadecane 108 40-140
2-BromonaphaJe 86 40-140
2-Fluorobiphenyl 88 40-140
This report should not be reproducad except in Its entirety without tJie Wjjtten consent of Prism Laboratories Inc449SprIngbrODjRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6354 Toll Free Number 1-800/5293B4 Fax 704/525-o409
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
ttn Chris Ward
Box 7030
hariotte NC 28241
30.19 lmL
12 6.4
12 1.8
12 3.8
MADEP EPH
MADEP EP1-I
MADEP EPH
06/23/07 2303 grappscclofl
06/2307 2303 grappaccjolj
06/23/07 2303 grappacciojj
adjusted value
IO.2g 2rnL
024514
024514
024514
EPN 08/21/07 800 grappaccloli P18703
JQP
mFum 29 mg/kg
48 mg/kg
0.27 0.016
0.27 0.022
50108
60106
0625/o7 1332 mcarnpbefl
06/25/07 1332 mcampbelj
024519
024519
Page of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample IDSampleMatrixSoilCOCGroup
Time Collected
Time Submitted
wS-.1
184952
G0607542
06/19/07 1600
06/19/07 1735
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Datemme ID
Sample PreparaUon
ImoleWeIghtDetelna
eight
MADEP VPH 06/26107 000 ibrown
Below Reporting Limit
_stlmated value between the Reporting Limit and the MDLresultsInthisreport relate only to the samples submitted for analysis and meet state certification requirements other than
LAC certffcaffon except far those Instances indicated in the case nanatlve and/or test commentsresultsarereportedondry-weight basis
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
ofatflo Petroleum Hydrocarbons by Gc-PtplD5-C8 Aliphalics BRL
9-C10 Aroma
9-C12 Aliphatics
2.25 50 mL 30509 06/21107 905 Jhoppei P18702
mg/kg 6.0 1.2 MADEP VPH 06/27/07 712 hwagner 024582
BRL mg/kg 6.0 0.036 MADEP VPI-1 06/27/07 712 hwagnsr 024582
BRL mg/kg 6.0 1.5 MADEp VPH 06/27/07 712 hgner 0245822nalysisMoteforcs-ca Aliphatics Adjusted valueinalysjsNoteforC9-C12 Aliphatjcs Adjusted value
Surrogate Recovery Control Limits
2S-DibromotolueneFlD 116 70 130
2S-DibromotolueneplD 91 70-130
1991
lela Overcash V.P Laboratory ServIces
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SprlngbroRoadP.O Bo 24054 Charlotte NC 28224-0543Phone704/529-6384 Toll Free Number 1-800/529.6364 Fax 704/525-0409 Page of 35
ESP Associates PA
Attn Chris Ward
Box 7030
harlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample IDSmpIeMatrixSoilcocGroup
Time Collected
lime Submitted
WS-2
184953
G0507542
06/19/07 1615
06/19/07 1735
NC Cortlflcatlon No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
SM2540 06/25/07 1745 Lthao
arameter Result Units Report MDL Dilution Method Analysis Analyst BatchflhIdsDeteatloDate/Time ID
ercerit Solids 743
ample Weight Determination
eight Blsulfate 6.32
eight BisuIfate 640
eight Methanol 5.54
latiIe Organic Compounds GC1MS
tl-Trfchioroethane BRL mg/kg 0.0053 0.00029 826GB 06/23/07 1712 erussell 024503I22-Tetrachloroethane BRL mg/kg 0.0053 O.0oo5I 52608 06/23/07 1712 erussell 024503l2-Trichloroethane BRL mg/kg 0.0053 0.00033 82608 06/23/07 1712 erusseil Q24503-Pichlorqethane BRL mg/kg 0.0053 0.00038 826DB 06/23/07 1712 russI Q2450bichIróæ..3/77J 24o3-Dichioropropene BRL rig/kg 0.0053
5035
5035
5035
06/27/07
06/27/07
08/27/07
000
000
000
ibrown
ibrown
ibrown
0.00046 82608 06/23/07 1712 enlsseii 0245033-Trichlorobonzene BRL mg/kg 0.0053 0.00058 8260B 06/2307 1712 erussell 0245033-Trich1oropropane BRL mg/kg 0.0053 0.00045 8260B 06/23/07 1712 erusseil 0245034.-Trlchjorobenzene URL mg/kg 0.0053 0.0005 826DB 06/23/07 1712 erussall 0245034-TrImethyjbenze 0.0023 mg/kg 0.0053 0.0004 826GB 06/23/07 1712 erusseli 024503DibromoethaneEDBBRLmg/kg 0.0053 o.0000g5 82608 06/23/07 1712 enisseli 024503DlchIorobereneBRLmg/kg 0.0053 0.00028 82608 06/23/07 1712 erussall 024503DlchloroethaneBRLmg/kg 0.0053 0.00053 826DB 08/23/07 1712 erussell 024503DiChioropropaneBRLmg/kg 0.0053 0.00039 8260B 06/23/07 1712 erusseff 0245035-Trlmelhylberzene BRL mg/kg 0.0053 0.00044 8260B 06/23/07 1712 aniseeD 024503ichorobenzeneBRLmg/kg 00053 0.00045 826DB 06/23/07 1712 erusseli Q245Q3FchloropropaneBRLmg/kg 0.0053 0.00036 826DB 06/23/07 1712 erussell 024503lchiorobenzeneBRLmg/kg 0.0053 0.00041 826GB 06/23/07 1712 erusseil 024503ichioropropaneBRLmg/kg 00053 0.00026 82608 06/2307 1712 erussell 024503ForotolueneBRLmg/kg 00053 0.00039 825DB 06/23/07 1712 wusseli 0245Q3Thisreportshouldnotbereproducedexceptin Its entirety without the written consent of Prism LaboraLori inc449SpringbrooRoadP.O Box 240543 Charlotte NC 28224.0543Phone704/529.5354 Toll Free Number 1-8O0J529354 Fax 7041525.0409 Page8or
99012 Laboratory ReportNCDrinkingWaterCertNo37735
06/29/07
ESP Associates PA
Project ID Morehead Commons No Client Sample ID WS-.2AttnChrisWard
Prism Sample ID 184953Box7030SampleMatrixSoilCOCGroupG0607542CharlotteNC28241TimeCollected0619/07 1615
Time Submitted 06/1 9/07 1735
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time io
024503-Chiomtoluene BRL mg/kg 0.0053 0.00027 8260B 06/23/07 1712 erussell 024503-MathyI-2-peritanone Misk BRL mg/kg 0.053 0.00053 8260B 06/23/07 1712 erussell 024503CetoneBRLmg/kg 0.053 0.0021 82606 06/23/07 1712 erussell 024503enzeneBRLmg/kg 0.0032 0.00042 826DB 08/23/07 1712 erusseil 024503romobenzeneBRLmg/kg 0.0053 0.00037 826DB 08/23/07 1712 erusse 024503omochloromethaneBRLmg/kg 0.0053 0.00032 82608 06123/07 1712 erussell 024503omodlchioromethaneBRLmg/kg 0.0053 0.00046 8260B 06/23/07 1712 erussell 024503omofomBRLmg/kg 0.0053 0.00039 82606 08/23/07 1712 enissefl 024503omomethaneBRLmg/kg 0.011 0.00061 82606 06/23/07 1712 ewsset 024503irbontetrachiorideBRLmg/kg 0.0053 0.0003 8260B 0623/07 1712 erusseli 024503
rng/kg .j.Q053 Q004 82606 06/23/07 17 12 nsseIl Q24o3
loroethane BRL mg/kg 0.011 0.00043 82606 06/23/07 1712 enissell 024503ForoformBRLmg/kg 0.0053 0.00039 826DB 08/23/07 1712 erussell 024503IcrometlianeBRLmg/kg 0.0053 0.00037 82606 0623/07 1712 erussell 024503i2-Dlchloroethene BRL mg/kg 0.0053 0.00023 82608 06/23/07 1712 erusseti 024503l.3Dlchloropropene BRL mg/kg 0.0053 0.00034 82608 06/23/07 1712 erusseH 024503toradllluoromethanoBRLmg/kg 0.0053 0.0012 82606 06/23/07 1712 erusseil 024503lbenzene0.0047J mg/kg 0.0053 0.00037 82606 06/23/07 1712 erussell 024503IropyletherJPEBRLmg/kg 0.0053 0.00018 82606 06/23/07 1712 erusseIl 024503ropylbenzeneBRLmg/kg 0.003 0.00042 626DB 06/23/07 1712 erussell 024503Xylenes00034Jmg/kg 0.011 0.00074 82609 06/23/07 1712 erusselt 024503yIethylketoneMEIcBRLmg/kg 0.11 0.0015 82806 0623/07 1712 erussell 024503tylt-butyt ether MIBE BRL mg/kg 0.011 0.0003 826DB 06/23/07 1712 erusseH 024503ylenechlorideBRLmg/kg 00053 0.00043 82606 06/23/07 1712 erusseli 024503tYlbenzeneBRLmg/kg 0.0053 0.00042 82608 06/23/07 1712 erusseji Q245oa
This report should not be reproduced except In its enfirety without tie written consent of Prism Laboratories inc
449 SprJngtrj Road P.O Box 240543 Char1otte NC 28224-0543Phone704/529fi354 Toll Free Number 1-800/529.6364 Fax 7O4/525.o4Oy Page 0135
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Morehead Commons No Client Sample ID
Prism Sample ID
COC Group
lime Collected
Time Submitted
WS-2
B495
G0607542
06119/07 1615
06/19/07 1735
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Japhthajene 0.0049 mg/kg 0.011 0.00061 8280B 06/23/07 1712 erussell 024503-Xylene BRI mg/kg 0.0053 0.00032 8260B 06123/07 1712 enjssell 024503-tsopropyitoiLjene BRL mg/kg 0.0053 0.00043 82608 06/23107 1712 erusseli Q24503ec-Butylbenzene BRL mg/kg 0.0053 0.00035 8260B 06/23107 1712 enjssefl 024503tyreneBRLmg/kg 0.0053 0.00053 82608 06/23/07 1712 erusseil 024503rt-Sutyjbenzene BRL mg/kg 0.0053 0.00033 8260B 06/23/07 1712 erussell Q24503trachioroetheneBRLmg/kg 0.0053 0.0009 826DB 06/23/07 1712 erusseji Q24503IUefle
0.0082 mg/kg 0.0053 0.00036 82608 0623/07 1712 erusseH 024503flSl2-DiChIoroethene BRL mg/kg 0.0053 0.0004 82608 06/23/07 1712 erusse 024503flS-l.3-Dfchioropropene am mg/kg 0.0053 0.00037 8260B 06/23/07 1712 orusseli Q2453NoroetheneBRLmg/hg 00053 000032 82608 p/23/o717 12 rsell 024503
iyl acetate BRL mg/kg 0.026 0.0019 826DB 05/23/07 1712 erussell 024503y1chlorideBRLmg/kg 0.0053 0.00067 826DB 06/23/07 1712 erussell 0245Q3
AieyIkaI EnyIiu.
NC CertIfication No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID
Sample Matrix Soil
Laboratory Report
06129/07
Surrogate Recovery Control Limits
Bromofluorobenzene 82 77-128
Dibromdfluoromethane 68 67-143
ToIuene-d 83 81-128
nil-volatile 0rgan Cornpounej by GC/MS
4-Trlchlomberene BRL mg/kg 0.44 0.044 8270C
Dlchlorobenzene BRL mg/kg 0.44 0.033 8270CfchiorobenzeneBRLmg/kg 0.44 0.032 8270CIchIomberieneBRLmg/hg 0.44 0.040 8270C
i-Trichlorophenol BRL mg/kg 0.44 0045 8270C
-TrichiorOphenoi BRL mg/kg 0.44 0.043 827CC
06/26/07 1826 kcamplgotto
06/26/07 1825 kcamplgotig
06/26/07 1826 kcamplgotic
06/26/07 1826 kcamplgptto
0625107 1826 kcampjgotto
06/28/07 1826 kcampigouo
024532
024532
024532
024532
024532
Q24532
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc
449 SpringIro0 Road P.O Box 240543 Charlotte NC 28224.0543Phone704/629.6364 Toll Free Number 1-800/629-6394 Fax 704/525.0409 Page 10 of 35
06/26/07 1826 kcamplgaUo
06/26/07 1826 kcampgotto
06126/07 1826 kcampgotto
06/26/07 1826 kcamprgouo
06/26/07 1826 kcampgoto
06/26/07 1825 kcmpgotto
06/26/07 1826 kcamplgotto
0626/07 1826 kcamplgotto
06/26/07 1826 kcamplgoiio
06/26/07 1826 kcamplgotjo
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 184953SampleMatrixSoilCOOGrujG0607542
Time Collected 06/1 9/07 1615
Time SubmItted 06/19/07 1735
Result Units Report MDL Dilution Method AnalysIs Analyst Batch
4-Dlmethylphenol BRL mg/kg 0.44 0.043 6270C 0245324-Dlnflrophenol BRL mg/kg 2.2 0.050 827CC 0245324-Dfnjtrotolijena BRL mg/kg 0.44 0.025 82700 0245326-Dlnjtrotofuene BRL mg/kg 0.44 0.047 82700 024532-Chlorortaphthalene BRI mg/kg 0.44 0.046 827CC 024532ChlorophenolBRLmg/kg 0.44 0.035 8270C 024532MethylnaphthaleneBRLmg/kg 044 0.035 827CC 024532MethyiphenolBRLmg/kg 0.44 0.042 827CC 024532NitrophenoiBRLmg/kg 0.44 0.053 827CC 0245324-Melhylphenol BRL mg/kg 0.44 0.045 827CC 0245323DIchorobqnzjjjBRLmg/kg 0.89 .0.028 827CC .06/26/071826 k.mpioUo 0245323-Dlnhlro.2.metilyjpheflol BRL mg/kg 2.2 0.027 82700 06/26/07 1826 kcampIioito 0245323romophenylphenyjether
hloro3.meffiyrphenoI
hloroanII1ne
Thlorophenyiphenylether
Iltrophenol
naphthene
uiaphthylene
hracone
benzene
Zoaanthracene
zoapyreno
zobfluoranthene
wghIpei.yfe
okfILJoranthene
BRL
BRL
BRL
BRL
BRL
BRL
BRE
BRL
BRL
0.22
0.20
0.30J
D.12J
0.15J
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
0.44
0.69
0.44
0.44
2.2
0.44
0.44
0.44
2.2
0.44
0.44
0.44
0.44
0.44
0.042
0.033
0.057
0.027
0.02g
0.044
0.044
0.034
0.041
0.062
0.051
0.020
0.021
0.036
8270C
8270C
8270C
827CC
82700
82700
82700
82730
82700
82700
8270C
827CC
82700
82700
06/26/37 1826 kcamplgouo
06/2507 1826 koamplgotto
06/2607 1826 kcampIgotto
06/26/07 1826 kcamplgouo
06/26/07 1826 kcamplgouo
06/26/07 1826 kcamptgoucp
06/26/07 1826 kcamnplgotto
06/26/07 1826 kcampIgoo
06/26/07 1826 koamptgo
06/26/07 1826 kcampfgoug
06/26/07 1826 kcamplgouo
06/26/07 1826 kcaniplgotto
06/28/07 1825 kcamplgotto
06/26/07 1826 kcamplgotc
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
This report should not be reproduced except In Its entirely without the wrItten consent of Prism Laboratories Inc449Springbro0jRoadP.O Box 240543 Charlotte NC 2822t.0M3Phon7041529..6364 Toll Free Number 1-80o/5z Fax lO4J525J4Q9 Page 11 of 35
Laboratory Report
06/29/07
Project ID Morehead Coin mons No Client Sample ID WS-2
Prism Sample ID 184953SampleMatrixSoilCOCGroupG0607542
Time Collected 06119/07 1615
Time Submitted 06/19/07 1735
ararneter Result Units Report MDL Dilution Method Analysis Analyst
lenzyl alcohol BRL mg/kg 0.89 0.047 827CC 1826 kcampIgon 024532lis2_chloroethoxymethane BR mg/kg 0.44 0.051 827CC 1826 kcamptgotio 024532ts2-chloroethyfether BRL mg/kg 0.44 0.048 827CC 1825 lccampfgouo 024532is2-chIomIsoppylether BRL mg/kg 0.44 0.038 827CC 1826 kcamplgotio 024532BRLmg/kg 0.44 0.022 827CC 1826 kcamprgono Q24532UtYlbeflzyjphthafateBRLmg/kg 0.44 0.027 827CC 1826 kcamplgouo 024532hrysene0.24 mg/kg 0.44 0.074 827CC 1826 kcampgotto 024532FflbutylphtlialateBRLmg/kg 0.44 0.020 82700 1826 kcampIrouc 024532-fl-octyiphhajate BRL mg/kg 0.44 0.033 827CC 1826 kcamplgotto 024532benzoahanlhraceneBRLmg/kg 0.44 0.045 82700 1826 ccampIoIto 024532bflZOfüfl
thg/kg .0.44 0.035 1..0c 06/2.6/0.1 826 kampIo 024532thyJphthaIateBRLmg/kg 0.44 0.027 827CC 06/26/07 1826 kcarnpgotjo Q2453liethyiphilialateBRImg/kg 0.44 0.030 827CC
loranthene 0.65 mg/kg 0.44 0.031 827CC
Jorene BRI mg/kg 0.44 0.026 8270C
xachrorobenzene BRL mg/kg 0.44 0.023 827CC
xachlorobutadjene BRL mg/kg 0.44 0.043 827CC
cachIorocycfopendiene BRL mg/kg 0.44 0.047 827CC
achtoroethane BRL mg/kg 0.44 0.045 827CC
enol23-cdpyrene O.32J mg/kg 0.44 0.046 827CCThoroneBRLmg/kg 0.44 0.040 82700
Iitroscdl.npropylarn me BRL mg/kg 0.44 0.050 82700
itrosodiphenylamine BRL mg/kg 0.44 0.023 827CChthaleneBRLmg/kg 0.44 0.048 827CCbenzeneBRLmg/kg 0.44 0.043 827CCtachiorophenolBRLmg/kg 2.2 0.037 82700
This report should not be reproducJ except in its entirely without the written conse of Prism Laboratories Inc449SpringbroRoadP.O Box 240543 Charlotte NC 28224-g543Phone7O4/529.63M Toil Free Number 1-B0O/5295354 lax 704/625.0409
.Jc
NC Certification No 402
SC Certification No 99012
NC DrInking Water Cert No 37735
ESP AssocItos PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
06/26/07
06/26/07
06/26/07
06/26/07
06/26/07
06/26/07
06/25/07
06/26/07
06/26/07
06/26/07
06/26/07 1826 kcamptgoij
06/26/07 1825 kcamplgouo
06/26/07 1826 kcamplgotto
06/26/07 1826 kcamplgoo
06/26/07 1826 kcamplgoiio
06/28/07 1826 kcamplgotto
06/26/07 1826 lccemplgouo
06/26/07 1825 kcampIgotti
06/26/07 1825 kcampfgotto
06/28/07 1826 kcampigofto
06/26/07 1826 kcampIgoto
06/26/07 1825 kcampJgot
06/26/07 1826 kcamplgojb
06/28/07 1826 kcamplgofio
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
Page 12 of 35
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 184953SampleMatrixSoilCOGGroupG0607542
Time Collected 06/19107 1615
Time Submitted 0619/07 1735
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
BRL mg/kg 0.44 0.048 827CC 05/26/07 1826 kcampIotto Q2453z
0.63 mg/kg 0.44 0.030 827CC 06/26/07 1826 koamplgotto 024532
Surrogate Recovery Control Limits
2.4.6-Tribromophenol 94 25-123
2-Fluorobiphenyl 81 21 108
2-Fluorophenot 54 14-89
Nitrobenzene.d5 64 14-103
Phenol-d5 73 13-95
iO3 M-iascbiePetroleumHydrocarbonsbyGC-F1D
tl-C22Aromatico BRL mg/kg 13 7.1
9C36AltphatJcs BRL mg/kg 13 2.0
1-Cis Aliphalics BRL mg/kg 13 4.2
nalysjs Note for Cll-c22 romatjcs Adjusted value
Sample Preparation-
10.26 rnL EPI-f 06/21/01 800 grappoccioll P18703
Surrogate Recovery Control Limits
l-Chloro-ocfadecane 116 40-140
40-140
2-FIuoroblphnyl 40-140
o-Terphenyl 86 40-140
This report should not be reproduceij except in its entirety without the written consent of Prism Lab ratorIe Inc449SpririgbrRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Pree Number 1-800/529..5364 Fax 704/525.0409
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
P.O Box 7030
3harlotte NC 28241
hencI
yrene
Sample Preparation 29.98 rnL 35509 06/22/07 1100 dpope P18710
MADEP EPH
MADEP EPH
MADEP EPI-I
06/24/07 047 grappaccloll
06/24/07 047 grappaccloft
06/24/07 047 grappaccioll
Q24514
024514
024514
lCP
omlum 28 mg/kg
37 mg/kg
.0.31 0.019
0.31 0.020
60105
601DB
06/25/07 1339 mcampbeif
06/25/07 1339 rncampbeli
024519
024519
Page 13 of35
ESP Associates PA
ttn Chris Ward
Box 7030
hariotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample IDSampleMatrixSoilCocGroup
Time Collected
Ti me Submitted
WS-2
184953
G0607542
06/19/07 1615
06/19/07 1735
Sample Preparation
29flfe Pefroleum Hydrocarbons by GC-PID/FID
5-C8 AflphatJcs
9-Clo Aromatica
Analysis lote for cs-ce Aliphatj05AnalysisNoteforC9-CJ.2 Aliphatics Adjusted value
Adjusted value
Recovery Control Limits
Surrogate
2S-DlbromotoJu.FID 114 70 130
89 70-130j1tDerflhJnjon
illht-.1 .---1825---g --1 MADEPVPH b5l26/O7.ooo thrownight
Below Reporting Limit
stirnaIed value between the Reporting Umit and the MDLresults In this report relate only to the samples submitted for analysis and meet state certification requiremenf other than
L4C certiffcatjo except for those Instances indfcted in the case narrative and/or test commentsesujtsamreportedondry-weight basis
This report should not be reproduceJ except In Its entirety without the written consent of Prism Laboratori Inc449SprIngroRoadP.O Box 240543 Charlotte NC 28224.0543Phone704/529-53w Toll Free Number 1-800/5296364 Fax 704/525.4j4g9
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29107
9-C12 Aliphalics
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
1mit at0r Datefljme ID
2.16 50 mL 305ü 0621/07 905 Jhoppet
BRL mg/kg 6.7 1.3 MADEP VPI-i 06/27/07 755 hwagner
BRL mg/kg 6.7 0.040 MADEP VPH 06/27/07 755 hwagnen
BRL mg/kg 6.7 2.1 MADEP VPII 06127/07 755 hgner
P18702
024582
024682
Q24582
19.20 MADEP VPI-I 05/25/07 000 Ibrown
ieja Overcash V.P Laboratory Services
Page 14 of 35
SP Associates PA
Ito Chris Ward
Box 7030
harlotte NC 28241
NC CerUficaflon No 402
SC Certificatf on No 89012
NC Drinking Water Cert No 37735
Project ID
Sample Matrix Sofl
Laboratory Report
06/29/07
Morehead Commons No Client Sample ID WS-3
Prism Sample ID 184954
COC Group 0060 7542
Time Collected 06/19/07 1630
Time Submitted 06/19107 1735
rameter Result Units Report MDL Dilution Method Analysis Analyst BatchLimitFactorDatemeIDtroentSolidsDetermination
rcent Solids 62.4 SM2540 06125/07 1745 Lthao
noIe Weight Determjnatton
4ght Blsulfbte 5.49 5035 06/27107 000 lbiownIght Blsulfate 5.g 5035 06/27107 000 IbrownightMethanol5.01 5035 06/27/07 000 brown
atile Organic Compounds by /MS
l-Tlichloroetjane SRI mg/kg 00053 0.0003 82606 06123/07 2021 erusseIl 024503BR1mg/kg 0.0053 0.00054 826DB 06/23/07 2021 eruseIl 0245032-Trlchloroethane SRI mg/kg 0.0053 0.00033 826DB 06/23/07 2021 enlsselt 024503DlchloroethaneBRLmg/kg 0.0053 0.00030 826DB 06/23/07 2021 eruseetl 024503BRLmg/kg PQ53 0.00041 .1 82606 M6/3/o7 2021 etjseIl 024503JichlorapropeneBRI_mg/kg 0.0053 0.00047
3-Trichiorobenzene
-Trichioropropane
-Trlchiorobonzone
-Trlmethylbenzene
ibnmoethane EDB
tlchloroberi.zene
lchloroethane
Ichioropropane
Trlmethylber0
lchlorobenzene
thlorupmpane
Ghlorobenzene
chtoropropane
rOtoiuene
BRL
SRI
BRL
SRi
BRL
SRI
SRI
BRL
SRI
SRI
SRI
BRI
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
0.0053 0.00059
0.0053 0.00047
0.0053 0.00051
0.0053 0.00041
0.0053 0.000096
0.0053 0.00029
0.0053 0.00053
0.0053 0.00039
0.0053 0.00045
0.0053 0.00046
0.0053 0.00036
0.0053 0.00042
826DB 06/23/07 2021 erusseU
826DB 06/23/07 2021 erusseil
3269 06/23/07 2021 arussell
82606 06/23/07 2021 erusseIl
82606 06/23/07 2021 erussell
826DB 06123/07 2021 erusseji
82608 06/23/07 2021 erussel
82608 06/23/07 2021 erusselt
826DB 0B/23/Q7 2021 eruss1
826DB 06/23/07 2021 erussol
82606 06/23/07 2021 enissalt
82609 06/23/07 2021 enisseft
826DB 06/23/07 2021 enissell
826DB 06/23/07 2021 erussa
826DB 06/23/07 2021 erussetI
024503
024503
024503
024503
024503
024503
024503
Q24503
024503
024503
Q24503
024503
024503
Q245Q3
024503
BRL mg/kg 0.0053 0.00027
BRL mg/kg 0.0053 0.00039
This report should not be reproduced except In Its entirety without the written consent or Prism thborato Inc440SprJngbrooRoadP.O Box 240543 Charlotte NC 282249543Phone704/529-6364 Toll Free Number 1-800529.6304 lax 704/525-0409 Page 15 of 35
Laboratory Report
06/29107
Project ID Morehead Commons No CHant Sample ID WS-
Prism Sample ID 184954SampleMatrixSoilCOCGroup00607542
Time Collected 06/19/07 1630
Time SubmItted 06/19/07 1735
NC CertificatIon No.402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
ttn Chris Ward
.0 Box 7030
harIotte NC 28241
arameter Result Units Report MDL Dilution Method Analysis Analyst
Chlorotoluene BRI mg/kg 0.0053 0.00028 82608 06/23/07 2021 erussell 024503MethyI-2-pennon0 MIBK BRL mg/kg 0.053 0.00053 82608 06/23/07 2021 wussefl Q24503etoneBRLmg/kg 0.053 0.0021 82603 06/23107 2021 erussell Q245o3mzeneBRImg/kg 0.0032 0.00043 826DB 06/23/07 2021 enJeseil 024503omobenzeneBRLmg/kg 0.0053 0.00037 826DB 06/23/07 2021 enjsseti 024503mochloromethaneBRLmg/kg 0.0053 0.00032 82608 06/23/07 2021 erussell Q24503rn1odIchjorometheBRLmg/kg 0.0053 0.00047 82603 06/23/07 2021 enJsseIi 024503moforrnERLmg/kg 0.0053 0.00039 82603 06/23/07 2021 erusself Q24503miornethaneBRLmg/kg 0.011 0.00062 826DB 06/23/07 2021 erussell 024503toritetrachlorideERLmg/kg 0.0053 0.00031 82608 06/23107 2021 orusset 024503ombenzeneBRLrngg0.0053 0.00041 82608 06/23/07 2021 esleselI 024503oibjfrBRLi6/ooo53oooo36 820B 06/23iO72oç a245d3oroethaneBREmg/kg o.oii 0.00044 82608 06/23/07 2021 erUssell 024503DroformBRLmg/kg 0.0053 0.00039 82608 06/23/07 2021 enissejI 024503DromethaneBRLmg/kg 0.0053 0.00037 826DB 06/23/07 2021 enjssetl 024503I2-Dlchloroethene BRL mg/kg 0.0053 0.00023 826DB 06/23/07 2021 erussaIf 024503l3-DIchloroprapene BRL mg/kg 0.0053 0.00034 82608 06/23107 2021 erussI 024503IlorodlfluoronioflaneBRLmg/kg 0.0053 0.0012 826DB 06/23/07 202-1 erusset Q24503JbenzezieBRLmg/kg 0.0053 0.00037 82603 06/23107 2021 enisseIl 024503rOpYIetJlerJPEBRLmg/kg 0.0053 0.00018 82608 06/23107 2021 erussoll 024503opylbenzeneBRLmg/kg 0.0053 0.00043 8260B 06123/07 2021 erussall 024503XylenesBRLmg/kg 0.011 0.00075 826DB 06/23/07 2021 eflisseIl 024503ylethylketoneMEKBRImg/kg o.ii 0.0015 826DB 06/23/07 2021 emsseU 024503ylt.butyI ether MIRE BRL mg/kg o.oii 0.00031 82608 06/23/07 2021 oneself 024503yfenechlorideBRImg/kg 0.0053 0.00044 82608 06123/07 2021 erussali 024503ythenzeneBRLmg/kg 0.0053 0.00043 826DB 06123/07 2021 OrUssell 024503
This report should not be reproducecJ except In Its entirety without the written consent of Prism Laboratories Inc449SpingbrooRoadP.O Box 240543 Charlotte NC 28224.0543Phone7O4/529.54 Toll Free Number 1-800/529.6354 Fax 704/5250409 Page 16 of 35
SP Associates PA
ttn Chris Ward
Box 7030
hartotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample IDSampleMatrixSoilCOCGroup
Time Collected
Time Submitted
WS-3
184954
G0607542
06/19107 1630
06/19/07 1735
phthatere
ylene
Sopropyltoluene
-Butyibenzono
rena
-Butyibenzene
rachiOjtethe
ens
s-I 2-DIclIloroethene
s-I .3-DIchiomprope
0.00036
0.00041
0.00037
06/23/07 2021
06/23107 2021
06/23/07 2021
06/23/07 2021
06/23/07 2021
06/23/07 2021
06/23/07 2021
06/23/07 2021
06/23/07 2021
06/23/07 2021
NC Certification No 402
SC Certification No 99012
NC Drinking Water CerL No 37735
Laboratory Report
06/29/07
0.013 mg/kg 0.011 0.00062 82608 eUSSeJI 024503BRLmg/kg 0.0053 0.00032 8260B saisseil 024503BRLmg/kg 0.0053 0.00044 82608 eiussefl 024503BRLmg/kg 0.0053 0.00035 8260B erussetl 0245030.0022 mg/kg 0.0053 0.00053 826DB erusseli 024503BRLmg/kg 00053 0.00033 826DB erusseJi 024503BRLmg/kg 0.0053 0.00092 626DB erussell 0245030A1044mg/kg 0.0053 8260B Onissell 024503BRLmg/kg 00053 8260B erussefl 024503ORLmg/kg 0.0053 8260B erusseti 024503ngkgO.O053.OOOQ32 .i ...860B Q6123/07 2021 rtr 024503ionfluommethane-BRl--mg/kg -000530 00044--1 ---826OB-.-O6/23/07 20 21erussell--Q24503-lacetate BRL mg/kg 0.027 00019 82605 06123/07 2021 erusseli 024503chlorideBRLmg/kg 00053 0.00068 8260B 06/23/07 2021 erusseIl 024503
Surrogate Recovery Control Limits
Bromoffuorobepne 94 77-128
Dlbromofluommethwe 67-143
Toluene-cJ3
81 128iatlleOr.aanJc Cornooufl by GCIMSTdchlorobenzeneBRL
Jchlorobenzene Bpj
chlorobenne BRL
Chlorobej BRL
rrichiomphoi BRI
BRI
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
0.40 0.040 827cc 06/26/07 1915 kcamp1go 0245320.40 0.030 827CC 06/26/07 1915 kcamptgoo 0245320.40 0.029 82700 06/26/97 1915 kcamplgo 0245320.40 0.036 8270C 06/26/07 1915 kcamplgott0 0245320.40 0.041 827CC 06/26/07 1915 kcarripfgota Q245320.40 0.039 827CC 06/26/07 1915 kcampi9otio 024532ThisreportshouldnotbereprorjucerjexceptInItsentiretywithoutthewrittenconsentofPrismLaboratoriesInc449SprIngbroeRoadP.O Box 240543 Charlotte NC 28224-0543Phone7O4/529364 Toll Free Number l-800I529-6354 Fax 704/525.0409 Page 17 of 35
99012 La borato ry Re portNCDrinkingWaterCertNo37735
06129/07
Project ID Moreheaci Commons No Client Sample ID WS-3
Prism Sample ID 184954SampleMatrixSoilCOCGroup00607542
Time Collected 06/19/07 1630
Time Submitted 06/19/07 1735BhirameterResultUnitsReportMDLDiluflonMethodAnalysisAnalyst
-Dimethyfphenol BR mg/kg 0.40 0.039 8270C 06126/07 1915 kcaniplgofto Q24532-Dinitrophenol BRL mg/kg 2.0 0.045 8270C 06126/07 1915 kcarnptgotto 024532-Dlnitrotoluene BRL mg/kg 0.40 0.023 8270C 06/26/07 1915 kcarnpigotjo 024532DinItmtoIueneBRLmg/kg 0.40 0.043 8270C 06/26/07 1915 kcarnpJofto 024532hioronaphthajeneBRLmg/kg 0.40 0.041 8270C 06/26/07 19.15 kcarnplgctto 024532hloropheriojBRLmg/kg 0.40 0.032 8270C 06/26/07 1915 kcampigotio 024532lethyInaphthaJee0.13 mg/kg 0.40 0.032 a270c 06/26/07 1915 kcarnpigotto Q24532ethyiphenorBRLmg/kg 0.40 0.038 6270C 05/26/07 1915 kcampIoit 024532FtmphenolBRLmg/kg 0.40 0.048 8210C 06/26/37 1915 kcampIgofto 024532-Methyiphenol BRL rngg 0.40 0.041 827CC 06/26/07 1915 kcampIofto 024532jjCbiombepzjdjn0BRL.Jng/kg _Qj QQ 87OC Q6/26/Q7 1915 kcarnplgoito p24532
omopilenyiphenylether BRL mg/kg 0.40 0.038 8270C 06/26/07 1915 kcarnpigotte 024532Iloro-3-meffylphenoj BR mg/kg 0.80 0.029 8270C 06/2607 1915 kcempigottc 024532loroanlOneBRLmg/kg 0.40 0.051 8270C 06/26/07 1915 kcamplgoltc 024532BRLmg/kg 0.40 0.025 82700 06/26/07 1915 Jccarriprgotto 024532rophenolSRImg/kg 2.0 0.027 82700 06126107 1915 kcsniplgoflo 024532aphtheneBRmg/kg 0.40 0.039 827CC 06/26/07 1915 kcampigou.o 024532aphthylene0.24 mg/kg 0.40 0.040 8270C 06/26/07 1915 kcampigoko Q24532acene0.41 mg/kg 0.40 0.030 8270C 06/26/07 1915 kcampigotto 024532enzeneBRmg/kg 2.0 0.037 82700 06/26/07 1915 kcarnpigotto 024532aanUracene0.80 mg/kg 0.40 0.056 8270C 06/26/07 1915 kampIgouo 024532apyrene0.95 mg/kg 0.40 0.046 82700 06/26/07 1915 koamplgotto 024532bflUoranthene
1.1 mg/kg 0.40 0.018 82700 06/26/07 1915 kcamplgotto 024532g.hlperyiene 0.69 mg/kg 0.40 0.019 8270C 06/26/01 1915 kcamplgotto 024532k5ucronthene
1.1 mg/kg 0.40 0.033 827CC 06/26/07 1915 kcampouc 024532
This report shourd not be eproducJ except In Its entirety without the wdttei consent of Prism Laboraorie Inc449SprlngbroQRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529.6364 Toll Free Number 1-800/529.6364 Fax 704525.0409
SP Associates PA
ttn Chris Ward
.0 Box 7030
harlotte NC 28241
Page 18 of35
SP Associates PA
tin Chris Ward
Box 7030
harlotte MC 28241
NC Certification No 402
SC CerllficatJn No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample IDSampleMatrixSoilCOOGroup
Time Collected
Time Submitted
WS-3
184954
00607542
06/19/07 1630
06119/07 1735
nzyl alcohol
2chIoroethoxymethane
2-chbroethylether
2-thlcrolsopropylether
2-ethylhexylphthaiate
.ylbenzylphthaf ate
lSene
elhylphtha late
ranthene
rene
achiorabenzene
3chlorobutadiene
rchIorocycIopendiene
Ichioroethane
io1 .23-cdpyrene
rorone
rosodl.n.propylamjno
rosodlphenyjamfne
thalene
enzene
chiorophenol
06/26/07 1915 kcampigotto
06126107 1915 kcamplgatlo
06126/07 1915 kcarnpigotto
06/26/07 1915 kcampigorto
06126/07 1915 kcamplgarto
06126/07 1915 kcamplgotio
06126/07 1915 kcamplgc4to
06/26/07 1915 kcamplgotto
06/26107 1915 kcamplgotjo
06/26/07 1915 kcamplgouo
Laboratory Report
06/29/07
3rameter Result Units Report MDL Dilution Method Analysis Analyst
BRL mg/kg 0.80 0.042 827CC 024532BRLmg/kg 0.40 0.046 827CC 024532
BRL mg/kg 0.40 0.044 82700 024532BRLmg/kg 0.40 0.034 827CC 024532BRLmg/kg 0.40 0.020 827CC 024532BRLmg/kg 0.40 0.025 827CC 0245329.98 mg/kg 0.40 0.067 827CC 024532-butylphthafate BRL mg/kg 0.40 0.018 827CC 024532-octylphIhaIate BRL mg/kg 0.40 0.030 821CC 024532nZoa.hanthracene 0.24 mg/kg 0.40 0.040 827CC 024532flzofijran0.14.1 mg/kg 0.40 0.034 827CC 05/26/07 195 kcarnplgotro 024532hyIphthaltSRI0400025627CC6/Ôithl5kcnp1ottti 024532SRImg/kg 0.40 0.027 827CC 06/28/07 1915 kcamplgatio 0245321.7 mg/kg 0.40 0.028 827CC 06/26/07 1915 kcamplgojto 024532
0.33 mg/kg 0.40 0.024 821CC 06/26/07 1915 kcamplgotto 024532BRLmg/kg 0.40 0.021 82700 06/26/07 1915 Iccamplgotia 024532SRImg/kg 0.40 0.039 82700 08/26/07 1915 kcampigottc 024532BRImg/kg 0.40 0.043 82700 06/26/07 1915 kcamp1goltg 024532SRImg/kg 0.40 0.041 827CC 06/26/07 1915 kcamplgoito 0245320.83 mg/kg 0.40 0.041 827CC 06/26/07 1915 kcamplgotto 024532BRmg/kg 0.40 0.036 82700 06/26/07 1915 kcamplgotto 024532BRmg/kg 0.40 0.046 827CC 06126/07 1915 kcamplgotto Q24532BRmg/kg 0.40 0.020 82700 08128107 1915 kcamplgotio 0245320.23 mg/kg 0.40 0.044 82700 06126107 1915 kcamplgoito 024532BRmg/kg 0.40 0.039 82700 06/26/07 1915 kcampigatto 024532BRmg/kg 2.0 0.034 82700 06/26/07 1915 kcarnpl9oft 024532
This report should not be repmduced except In Its entirety Without the written consent of Prism Laborotoj Inc449SprinoJcRoadP.Q Box 240543 Charlotte1 NC 28224.0543Phone704/529.6304 Toll Free Number 1-800/525-6304 Fax 704/525-0409 Page 190135
SCficaflfl9gj Laboratory ReportNCDrinkingWaterCertNo3773506/29/07
sP Associates PA
Project ID Morehead Commons No Client Sample ID WS-3UnChrisWard
Prism Sample ID 184954Box 7030 Sample Matrix Salt COC Group G060 7542hariofteNC28241meCollected06/19/07 1630
Time Submitted 06/19/07 1735
rameter Result Units Report MDL DIIutlo Method Analysis Analyst
renal BRL mg/kg 0.40 0.044 8270C 06/26/07 1915 kcampfgouo Q24532rena
2.1 mg/kg 0.40 0.027 8270C 06/26107 1915 kcamptgcfto 024532
Sample Preparation
29.88 mL 355 06/22/07 1100 dpope P13710
Surrogate Recovery Control Limits
2.4.8-lribramophenol 94 25-123
2-FIuoroblpheny 87 21 108
2-Huorophenol 84 14-59
Mtrnbenzene.iJ 82 14-103
Phenoj-c15 92 13-9S
4j136Iii-
actable Petroleum HvdrocarbónsbyGC.FD-C22 Aromatles 130 mg/kg 12 6.4 MADEP EPH 06/24/01 232 grappacciolr Q24514-C3SAIIphafjcs BRI mg/kg 12 1.8 MADEP EPH 06/24/07 232 grappacojofi Q2451418AHphatlceBRLmg/kg 12 3.8 MADEP EPH 06/24/07 232 gappacci Q24514analysisNoteforC1l-C22 Arcnnatjcs Adjugtd valuemp1ePreparatfom
10.24 mL EPH 06/21107 800 wappacclofl P16703
Surrogate Recovery Contro Limits
l-Chlomocfdecene 81 40-140
2-Bromorlaphthalene 123 40-140
2-Fluorubfphmyi 103 40-140
o-Terphenyi 87 40-14
niuni 46 mg/kg 0.26 0.016 60103 06/25/07 1347 mcampbell 024519110mg/kg 0.26 0.022 60108 06/25107 1347 mcampbeU Q24519
This report should not be reproduced except In Its entirety without the wfltten consent of Prism Laboratorte Inc449SpringbrRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529e354 Toll Free Number 1-806/520.9354 Fax 704/525.0409 Page 20 0135
SP Associates PA
Project ID Morehead Commons No Client Sample ID WS-3ttnChrisWard
Prism Sample ID 184954Box7030SampleMatrixSoftCOCGroupG0607542harlotteNC28241TImeCollected06/19/07 1630
Time Submitted 05/19/07 1735
rameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Llmt Factor Date/Time ID
Sample Preparation
305GB 06/21/07 905 Ihoppel P18702
mg/kg 6.1 1.2 MADEP VP1-t 06/21/07 838 hwagner Q24582
Surrogate Recovery Control Limits
25-Dibromotouflepf 112 70-130
2S-DJbromototuenplD 87 70-130
WJe Weicjht Determination
ght4 _MADEpVp 0W07OoO lbght
MADEP VPI-I 06/26/07 000 Ibruwnomments
BelowReporfjng Urn/f
stlmated value between the Reporting Limit and f/ia MDL
results-in this report relate only to the samples submitted for analysis and meet state certification requirements other than
AC car/if ication except for those Instances Indicated/n the case narrative and/or test commentssulfsarereportedondry-weight basis
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06129107
lathe Petroleum Hydrocarbons by GC-PID/F1D
-cs Aliphatics BRL
-do Aromaj
-C12 Aliphatics
23g 5OmL
ialyss Note for C5-CB AliphatjcsAnalysisNoteforC9C12Aliphatjcs
BRL mg/kg 6.1 0.035 MADEP WI-I 06/27/07 838 hwagner Q24582SRImg/kg 6.1 1.9 MADEP VPH 06/27/07 838 hwaner Q24582
Adjusted value
Adjusted value
21.10
tie Overcash V.P Laboratory Services
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories inc449SprIngbrooRoadP.O Box 240543 Charlotte NC 28224-0543Phone7Q4/529..63 Toll Free Number 1-8001529..6354 Fax 704/525.0409 Page 21 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample IDSampleMatrixSoilCOCGroup
Time Collected
Time Submitted
WS-4
184955
G0607542
06/19/07 1645
06/19107 1735
5.16
5.34
5.62
5035
5035
5035
06/27/07 000 Ibrown
06/27/07 000 Ibrown
06/27/07 000 thrown
IciA
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
------ararneter Result Units Report MDL Dilution Method Analysis Analyst Batch
Date/Time ID
ersent SolIds 84.9 SM2540 06/25/07 1745 Lthao
.pIe WelgJt Determiraon
/elght Bisullate
ielght Bisullate
Ielght Methanol
olatije OrganIc Compounds by Gc/MS
l1-Trfchtomethane BRL mg/kg 0.0055 0.00031 82608 06/23107 1743 arussefl 024503l22-Tetrachlaroethane BRL mg/kg 0.0055 0.00056 8260B 06/23/07 1743 erusseIt 024503l2TrjchJomethaneBRLmg/kg 0.0055 0.00034 82608 06123/07 1743 enjssell Q245031Doroet1ianeBRLmg/kg 0J055 0004 82609 06123/07 43erusseH 024503
---l-Dlchioroprcpene BRL mg/kg 0.0055 0.00049 82608 05/23/07 1743 erussell 024503.3-Trlthiorobenzene BRL mg/kg o.ooss 0.00061 82608 0523/07 1743 erussell Q2403.3-TrIchIoropropane BRL mg/kg 0.0055 0.00049 82608 06/23/07 1743 erusselI 0245034-Trichlorobenzene BRL mg/kg 0.0055 0.00053 82608 06/23/07 1743 erusseil 0245034-Trimethylbenzene BRL mg/kg 0.0055 0.00042 82608 06123/07 1743 erussetl 024503-Dlbrornoethane EDB BRL mg/kg 0.0055 0.000099 82608 06/23/07 1743 erussell 024503-Dichlorobenzene BRI mg/kg 0.0055 0.0003 82608 06/23/07 1743 erussell 024503-Dlchjoroethone BRL mg/kg 0.0055 0.00055 82608 06/23/07 1743 siusseIl 024503DlchlorupropaneBRImg/kg 0.0055 0.00041 826DB 06/2307 1743 enissetI 024503S-Tdmethylbenzene BRL mg/kg 0.0055 0.00046 82608 08/23/07 1743 eiusseV 0.24503DichIoroberzeneBRLmg/kg 0.0055 0.00047 826DB 0623/07 1743 erusselI 024503DlchioropropaneBRLmg/kg 0.0055 0.00037 8260B 06/23/07 1743 erussell 024503DtchlorcbenzeneSRImg/kg 00055 0.00043 826DB 06123/07 1743 erusselt 024503DlchiompropanBRLmg/kg 0.0065 0.00028 82608 06/23/07 1743 erussell 024503ilorotolueneSRImg/kg 0.0055 0.00041 82608 05/23/07 1743 erussell 024503Thisreportshould not be reproduced except In its entirety without the Written consent of Prism Laboratories Inc
449 SprIngbro Road P.O Box 240543 Charloe NC 28224.0543Phone7O4/529-63M Toll Free Number 1-80Q/52g..354 Fax 704/525.0409 Page 22 of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
ttn Chris Ward
.0 Box 7030
harIotte NC 28241
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID WS-4
Prism Sample ID 184955SampleMatrixSoilCOGGroupG0607542
Time Collected 06/19/07
Time Submitted 06/19/07
1645
1735
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
024503ChlorotofueneBRLmg/kg 0.0055 0.00029 826DB 06/23/07 1743 erusseJi 024503
-Methyl-2-pentanone MIBK BRL mg/kg 0.055 0.00055 826DB 06/23/07 1743 erIjssell 024503cetoneBRLmg/kg 0.055 0.0022 826DB 06/23/07 1743 erusseIt 024503enzene0.0023 mg/kg 0.0033 0.00044 825DB 06/23/07 1743 erusseti 024503romobenzeneBRImg/kg 0.0055 0.00039 826DB 06/23107 1743 erussell 024503omocflloromeflianeBRLmg/kg 0.0055 0.00033 82609 06/23/07 1743 erusseil Q245o3omodlchloromethaneBRLmg/kg 0.0055 0.00049 82609 06/23/07 1743 erusself 024503omoformBRLmg/kg 00055 0.00041 825DB 06/23107 1743 erussell 024503OmomethaneBRLmg/kg 0.011 0.00064 826DB 06/23/07 1743 erusseil 024503wbontetrachiorideBRLmg/kg 0.0055 0.00032 826DB 05/23/07 143 erusseli 024503orcbenzene-BRL mg/kg 00055 D.0o42 8.26bB 023/07 -1.43 nJssefl 024503lorodibromornethaneBRLmg/kg 0.0055 0.00037 826DB 06/23/07 1743 erusseI
Joroethat-ie
loroform
loromethane
i2-Dlchtoroethene
i.3-Dlchloropropene
hlorodjfiuorcmethane
ylbenzene
ropyl ether IRE
ropylborizene
-Xylenes
hyl ethyl ketone MEI
hyl t-butyl ether MIBE
hylene chloride
itylbenzene
BRt
BRL
BRL
SRI
SRI
BRL
000313J
BRL
BRL
0.0026
BRL
BRL
BRL
BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
0.011 0.00045
0.0055 0.00041
0.0055 0.00038
0.0055 0.00024
0.0055 0.00035
0.0055 0.0012
0.0055 0.00039
0.0055 0.00019
0.0055 0.00044
0.011 0.00077
0.11 0.0015
0.011 0.00032
0.0055 0.00045
0.0055 0.00044
826DB
826DB
826GB
826DB
826DB
826DB
826DB
826DB
82603
82608
828DB
826DB
826DB
82608
06/23/07 1743 erussdl
06/23/07 1743 enjssejl
06/23/07 1743 erussell
06/23/07 1743 erusseIl
06/23/07 1743 erusseil
06/23/07 1743 erussefl
06/23/07 1743 erusseli
06/23/07 1743 enJsseI
06/23/07 1743 erussejj
06/23/07 1743 erusseil
06/23/07 1743 ewssi
06/23/07 1743 erusseil
06/23/07 1743 erusseji
06/23/07 1743 erUsseli
024503
024503
024503
024503
024503
024503
024503
024503
024503
024503
024503
024503
024503
024503
This report should not be reproduceri except in Its entirely without the written consent of Prism Laboratories Inc4495prlngbrocRoadP.O Box 240543 Charlotte NC 28224-0Phone704/529-63M Toll Free Number l-800/52953M Fax 704/525-0409 Page 23 of 35
Laboratory Report
06/29/07
Project ID MorehØad Conrnions No Client Sample ID WS4
PrIsm Sample ID 184955SampleMatrixSoilCOGGroupG0607542
Time Collected 06/19/07 1645
Time Submitted 06/19/07 1735
NC Certification No 402
SC Certification No 99012
NC Drinking Water CerL No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
charlotte NC 28241
arameter Result Units Report MDL Dllutjon Method Analysis Analyst Batch
ID
I-Propyrbenzene mg/kg
erusseji 024503iaphthalane
-Xyfene
-Isopropyftoluene
sc-Butylbenzene
tyrene
rt-Butylbenzene
trachloroethene
luena
Ins-I 2-Dlchloroethene
tns-1 3-DlchIoropropene
ERL
BRL
BRL
SRI
SRI
BRL
SRI
00067
BRL
ERL
mg/kg
mg/kg
mg/kg
mg/hg
mg/kg
mg/hg
mg/kg
mg/kg
mg/kg
mg/kg
0.011
0.0055
0.0055
0.0055
0.0055
0.0055
0.0055
0.0055
0.0055
0.0055
0.00064
0.00033
0.00045
0.00036
0.00055
0.00034
0.00095
0.00037
0.00042
00039
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
06/23/07 1743 erusseji
06/23/07 1743 erussefl
06/23/07 1743 erusseji
06/23/07 1743 erussefl
06/23/07 1743 erussefl
06/23/07 1743 erussejj
06/23/07 1743 erusseil
06/23107 1743 erussefi
06/23/07 1743 erusseli
06/23/07 1743 erussell
024503
024503
024503
024503
024503
024503
024503
024503
024503
024503chloroethereBRLmg/kg 0.0055 0.00033 826DB 06/23/07 1743 enissell 024503c.ilorofluoromethrie BRL Th/kg D0055-0.00045 82606 06/23/or1743erussel 024503ylacetateBRLmg/kg 0.028 0.0020 826DB 06/23/07 1743 erussoll 024503iylchlorideBRLmg/kg 0.0055 0.00071 82608 06/23/07 1743 erussejl 024503
Surrogate Recovery Control Limits
Bromofluorobenzene 82 77-128
Dlbromofluaromethane 68 67-143
Toluened5 81 81 128
nivoIatjJe Organlg Compounds by Gc/Ms
4Trfchiorobenzene SRI mg/kg 0.40 0.039
Dichlorobepze BRL mg/kg 0.40 0.029
Dlchlorobepzene BRL mg/kg 0.40 0.028
Dlchlorubenzene BRL mg/kg 0.40 0.036
5-Trlchtomphenol SRI mg/kg 0.40 0.040
i-Trichiorophenoi SRL mg/kg 0.40 0.038
827CC 06/26/07 2004 kcampigotto 024532
8270C 05/26/07 2004 kcamplgotio 024532
827CC 06/26/07 2004 kcwnplgofto 024532
8270C 06/26/07 2004 kcamplgoito Q24532
8270C 06/26/07 2004 kcamplgotio 024532
827CC 06/26/07 2004 kcaniptgana 024532
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SpringbrooRoadP.O Box 240543 Chariot NC 28224.0543Phone704/529-6364 ThU Free Number l-800/529-63s4 Fax 704/525-0409 Page 24 of 35
SC Ceat1n No 99012 Laboratory ReportNCDrinkingWaterCertNo37735
06/29/07
ESP Associates PA
Project ID Moreheaci Commons No Client Sample ID WS-4AttnChrisWard
Prism Sample ID 184955Box7030SampleMatrixSoilcocGroupG0607542CharlotteNC28241
Time Collected 06/19/07 1645
Time Submitted 06/19/07 1735BcarameterResultUnitsReportMDLDilutionMethodAnalysisAnalyst
4-Dlmeulylphenol BRL mg/kg 0.40 0.038 827CC 08/26/07 2004 kcampigou 0245324-Dlnitrophenoj BRL mg/kg 2.0 0.044 827CC 06/26/07 2004 kcamplgoLk 0245324-Dinitrotcluene BRL mg/kg 0.40 0.022 82700 06/26/07 2004 kcamplgotto Q245326-Dlnitrotoluene BRL mg/kg 0.40 0.042 827CC 06/26/07 2004 kcampigouj 024532-Chloronaphthalene BRL mg/kg 0.40 0.041 8270C 06/26/07 2004 kcamplgotto 024532ChlorophenolBRLmg/kg 0.40 0.O3 8270c 06/26/07 2004 kcamplgotto 024532MethylnaphthajeneBRLmg/kg 0.40 0.031 827CC 06/26/07 2004 kcampIgot 024532MethyiphenolBRLmg/kg 0.40 0.037 827CC 06/26/07 2004 kcampIgoi 024532NlirophenolBRLmg/kg 0.40 0.047 827Cc 06/26/07 2004 kcampigotio 0245324-MethyIphenol BRL mg/kg 0.40 0.040 827CC 06/26/137 2004 kcampjgona 024532LQrgbenzj_BftJ g/g çij Q25 2i0C l24532
607 pigclto3romophenyjphefly95BRLmg/kg 0.40 0.037 82700 06/26/07 2004 kcampigotto 024532Thloro-3-methylphenol BRL mg/kg 0.79 0.029 827CC 06/26/07 2004 kcamplgouo 024532hIoroanJleBRLmg/kg 0.40 0.050 827CC 08/26/07 2004 kcamplgotto 024532BRLmg/kg 0.40 0.024 827CC 08/26/07 2004 kcampigouo 024532IitrophenolBRLmg/kg 2.0 0.026 8270C 05/26107 2004 kcamplgot 024532maphtheneBRLmg/kg 0.40 0.039 8270C 06/28/07 2004 kcamptgc 024532maphthyleneBRLmg/kg 0.40 0.039 82700 06/26/07 2004 kcampigouo 024532hraceneBRLmg/kg 0.40 0.030 827CC 06/26/07 2004 kcampigott Q24532benzeneBRLmg/kg 2.0 0.037 827CC 06/26/07 2004 kcampigoo 024532ZoaanthraceneBRLmg/kg 0.40 0.055 821CC 06/26/07 2004 kcampIgoto 024532zoapyreneBRLmg/kg 0.40 0.046 827CC 06/26/07 2004 kcampfgot 024532zobfiuomntheneBRLmg/kg 0.40 0.018 827CC 06/26/07 2004 kcampigotjo 024532oghIperyleBRLrngikg 0.40 0.019 827CC 06/26/07 2004 kcampIgot0 024532rOkffuoranthsneBRLmg/kg 0.40 0.032 82700 06/26/07 2004 kcampigo 024532
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SprIngrRoadP.O Box 240543 Charloft6 NC 28224-0543Phon104/529-6364 Toll Free Number 1-80O/5g.6364 Fax 704/525.0409 Page 25 of 35
NC Certification No 402
SC Certification No 99012NCDrinkingWaterCertNo 37735
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
lenzyl alcohol BRL mg/kg 0.79 0.042 8270C 06/26107 2004 kcamplgutto 024532ls2-chloroathoxymeflana BRL mg/kg 0.40 0045 8270C 06/26/07 2004 kcamplotto 024532Is2-chloroethyrether BRI mg/kg 0.40 0.043 827CC 06/26/07 2004 kcampIgoIt 024532ls2-chloroisopropylether BRL mg/kg 0.40 0.034 827CC 06/26/07 2004 kcamplgotto 024532Is2-ethylhexytphtharate BRL mg/kg 0.40 0.019 8270C 06/26/07 2004 kcampjgotto 024532utylbenzylphthalateBRLmg/kg 0.40 0.024 527CC 06/26/07 2004 kcamplgotto 024532hryseneBRLmg/kg 0.40 0.065 527CC 06/26/07 2004 koamplgoito 024532-fl-butylphthala BRL mg/kg 0.40 0.015 527CC 06/26/07 2004 kcamplgouo 024532-n-octylphthaiate BRL mg/kg 0.40 0.029 827CC 0612507 2004 kcamplgotto 024532benzoahanlraceneERLmg/kg 0.40 0.040 8270C 00126/07 2004 kcmpIgotto 024532benzofumnBRLmg/hg 0.40 .0.034 -827CC..06/26/07.2004 kcampgotio 024532thylphthaIaLeBRLmg/kg 0.40 0.024 827CC 06/26/07 2004 kc2mpIoIto Q245I2BRLmg/kg 0.40 0.027 827CC
BRL mg/kg 0.40 0.027 827CC
BRL mg/kg 0.40 0.023 8270C
BRL mg/kg 0.40 0.020 827CC
BRI mg/kg 0.40 0.038 827CC
BRL mg/kg 0.40 0.042 827CC
BRL mg/kg 0.40 0.040 827CC
BRL mg/kg 0.40 0.040 8270C
BRL mg/kg 0.40 0.035 627CC
BRL mg/kg 0.40 0.045 827CC
BRL mg/kg 0.40 0.020 827CC
BRI mg/kg 0.40 0.043 5270C
BRL mg/kg 0.40 0.038 8270C
BRL mg/kg 2.0 0.033 527CC
This report should not be reproduced eccept in its entirety without the Writter consent of Prism Laboratories Inc449SprIngbroRoadP.O Box 240543 Charlotte NC 28224-0543Phone1041529-6354 Toll Free Number 1-800/52963k Fax 704/525-0409
ESP Associates PA
Attn Chris Ward
0.Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID
Prism Sample IDSampleMatrixSoilCocGroup
Time Collected
Time Submitted
WS-4
184955
G0607542
06119/07 1645
06/19/07 1735
llethylphthalate
loranthene
lorene
xachiorobep2ene
xachjorobUtodlene
caChlorocyciopentadjene
achioroethane
eno1 2.3-cdpyrene
3horone
Iltrosodiphenyjamine
hthalerie
benzene
taChiorophenol
06/26/07 2004 kcamplgolta
06/26/07 2004 kcampIoito
06/26/07 2004 kcamplgoiu
06/25/07 2004 koampigotto
06/26/07 2004 kcamplgouo
06/26/07 2004 hcamplgotto
06/26/07 2004 kcamplgoijo
06/25/07 2004 kcamplgouo
06/26/07 2004 hcamprgotto
06/26/07 2004 Iccampigotto
06/26/07 2004 kcamplgotto
08/25/07 2004 kcamplgoito
06/26/07 2004 kcampfgotto
05/26/07 2004 kcarnplgolb
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
Page 26 of 35
NC Certification No 402
Laboratory ReportScCertificationNo99012
06/29/07
NC Drinking Water Cert No 37735
llflflhlIfliI SbHIn
ESP Associates PA
Project ID Morehead Commons No Client Sample ID WS-4ttnChrisward
Prism Sample ID 184955Box7030SampleMatrixSoilcocGroupG0607542harlotteNC28241
Time Collected 06/19/07 1645
Time Submitted 06/19/07 1735
Batsh
aramater Result Units Report MDL Dilution Method Analysis Analyst
Date/TimeTrenRLmgkg0400019-
henol BRL mg/kg 0.40 0.043 82700 06/26/07 2004 kcamplgouo 024532yreneSRImg/kg 0.40 0.027 827CC 06/26/07 2004 kcamplgotto 024532
Sample Preparation
29.52 ml 355DB 06/22/07 1100 dpop P18710
Surrogate Recovery Control Limits
Z46-TribromophenoI 69 25-123
2-Fluoroblphenyl 66 21 108
2-Fluomphenol 49 14-89
Mtrobenzene-d5 53 14-103
Terphenyj-d14 41 136
Pjienol-d5 i39
Petroleum hydrocarbons by c_j1-C22 Aromatics BRL mg/kg 11 6.1 MADEP EPH 06/24/07 416 grappaccloll 0245149-036 Aliphatjcs SRI mg/kg ii 1.7 MADEP EPH 06124/07 416 grappacc1ol Q245j4-018 AlIphatics SRI mg/kg 11 3.6 MADEP EPH 06/24/07 416 grappacclolt 0245142na1ysisNoteforC11C22AromaticsAdjust.ed value
Sample Preparation
10.42 ml EPH 06/21/07 800 grappaccoft P18703
Surrogate %Recovery Control LimIts
2-Bromonaphfene 114 40-140
0-Terphenyl 40 140
i-Chic octadecane 122 40-140
2-Fluoroblphenyl 116 40-140icp
mlum 28 mg/kg 0.27 0.016 6010B 06/25/07 1354 mcampbelt 02451922mg/kg 0.27 0.022
06/25/07 1354 mcampbefl 024519
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Springbro Road P.O Bo 240643 Charlotte NC 28224-0543Phone7O4/529-53M Toil Free Number l-8OO/52g.M Fax 704/525-0409 Page 27 ci 35
ESP Associates PA
Project ID Morehead Commons No Client Sample ID WS-4AttnChrisWard
Prism Sample 1D 184955Box7030SampleMatrixSoilCOCGroupG0607542CharIotteNC28241TimeCollected06/19/07 1645
Time Submitted 06/19/07 1735
arametor Result Units Report MDL Dilution Method Analysis Analyst atc
do Date/Time IDar
Sample Preparation
30509 06121/07 905 ihoppel P18702
BRL mg/kg 5.9 1.1 MADEP VPH 06/27/07 921 hwagner 024582
BRL mg/kg 5.9 0.035 MADEP VPH 06/27/07 921 hwagner
BRL mg/kg 5.9 1.8 MADEP VPH 06/27/07 921 hwagner 024582
Surrogate Recovery Control Limits
2S-Dibromotoluenpj 70 130
2S-DibromotoIueneFlD 70 130
22.68
1--MADEPVPH06/261ObÔO.browneIght
IL Below Reporting limit
Estimated value between the Reporting Limit and the MDLresultsInthisreportre/ate only to the samples submitted foranalysis and meet state certification requiremepts other than
LAC certification except for those Instances Indicated in the case narrative andor test commentsresultsarereportedondry-weight basis
VIAI a.nlaI
NC Certification No 402
SC Certification No 99012
NC Dtinldng Water CerL No 37735
Laboratory Report
06/2g/07
Hydrocarbons by GC-PIDFID
5-c8 Afiphatics
2.2g 50 mL
9C1 Aromatica
9-C12 Aliphatics
Axa1ysis
Note for CS-C Aliphatics Adjusted valueNoteforC9.-C12 Aliphatjcs Adjusted value
024582
18.97
121
MADEP VPH 06/26107 000 brown
0vercash V.P Laboratory Services
This report should not be reproduc except In its entirety without the written consent of Prism Laboratories Inc449SprtngbrReactP.O Box 24O43 Charlotte NC 28224..0543Phone1041529-63M Toll Free Number 1-800/5295364 Fax 704/525-0409 Page 28 of 35
SC 99012 Laboratory ReportNCDrinkingWaterCertNo3773506/29/07
ESP Associates PA
Project ID Morehead Commons No Client Sample ID B-IttnChrisWard
Prism Sample ID 184955Box7030SampleMatrixSoicocGroupG0607542hadofteNC28241meCollected06/19/07 1700
Time Submitted 06/19/07 1735
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Dateme ID
percent olids Petqrmnanon
ercent Sotld
SM254o 06/25/07 1745 Lthso
nIe Weight Determination
eight Blsulfate 6.37 5035 06/27/07 000 brown/elght Blsulfate 6.42 5035 06/27/07 000 brown
leight Methanol 6.44 5035 06/27/07 000 brown
olatile Organic Compounds by GC1MS
l.l-Trlchloroethane BRL mg/hg 0.0049 0.00027 82608 06/26/07 506 erusseil 024504l22-Tetrachloroethane BRL mg/kg 0.0048 0.00049 82608 06/26/07 506 erusset 024504l2-Trichloroethane BRL mg/kg 0.0048 0.0003 826GB 06/26/07 505 erusseli 0245041-Dlchbmethane BRL mg/kg 00048 000034 82608 06/26/07506 erusseli 024504
04_lDtchloropropene BRL mg/kg 00045 0.00042 82609 06/26/07 506 erussefi 024504r3-Trichlorobeene BRL mg/kg 0.0048 0.00053 826DB 06/26/07 505 eIusseII 0245043.Trlchloroprcpane BRL mg/kg 0.0048 0.00042 826DB 06/26/07 505 elusseli 024504.4-Trichlorobenzene BRL mg/kg 0.0048 0.00046 826DB 06/26/07 506 erussI 024504.4-TrlmethyIbeene BRI mg/kg 0.0048 0.00036 826DB 06/2607 506 eusseIl 024504-Dibromoethane EDB BRL mg/kg 0.0048 0.000086 826DB 06/26/07 506 erusseil 024504DichiorobenieneBRLmg/kg 0.0048 0.00026 826DB 06/26/07 506 erusseli 024504DichioroethaneBRLmg/kg 0.0048 0.00048 826DB 06/26/07 505 erusseil Q24504DlchlorcprupaneBRLmg/kg 0.0048 0.00035 826DB 00/25107 506 elusseil 0245o4S-Tdmethyjbej.0 BRI mg/kg 0.0048 0.0004 82609 06/26/07 506 enissetl 024504DlchlorobenzeneBRLmg/kg 0.0048 000041 82609 06/26/07 506 erussoll 024504DlchloropropaneBRLmg/kg 0.0048 0.00033 82608 05/26/07 506 erussaji 024504DlchjorcbenzeneBRLmg/kg 0.0048 0.00037 82609 06/26/07 506 erusseii 024504DlchloropropaneBRLmg/ks 0.0048 0.00024 82608 05/26/07 506 enmesh 024504ilorotolueneBRLmg/kg 0.0048 0.00035 82609 06/26/07 606 eruseeli 024604ThisreportshouldnotbereprocluceriexceptInItsenflretywithouthewrittenconsentPrismLabottri55Inc449SpringbroojRoadP.O Box 240543 CharJotte NC 28224-0543Phone704/529..634 Toll Free Number 1-800/59.j Fax 704/525.0409 Page 29 of 35
Laboratory Report
06/29/07
Project ID Morel-iead Commons No Client Sample ID B-i
Prism Sample ID 184956SampleMatrixSoilCOCGroupG0607542
Time Collected 06/19/07 1700
Time Submitted 06/19/OT 1735
NC Certiflcatlon No 402
SC Cettilication No 99012
NC Drinking Water Cart No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
hadotte NC 28241
aremeter Result Units Report MDL Dilution Method Analysis Analyst atc
-Chiorotojuene ORL mg/kg 0.0048 0.00025 82608 06/26/07 506 erusseil 024504-MethyJ-2-pentanone MIBK BRL mg/kg 0.048 0.00048 82608 06/26107 506 orussail 024504.cetone BRL mg/kg 0.048 0.0019 826DB 06/26/07 506 erusseil 024504enzeneBRLmg/kg 0.0029 0.00038 82606 06/26/07 506 erusseli 024504romobenzeneBRLmg/kg 0.0048 0.00034 82606 06/26/07 506 erussell Q245o4romochioromethaneBRLmg/kg 0.0048 0.00029 826DB 06/26/07 506 erussoli 024504DmodlchioromoaneBR.mg/kg 0.0048 0.00042 826DB 06/26/07 506 erusseit 024504omolomiBRLmg/kg 0.0048 0.00035 826DB 05/26/07 505 erusseil 024504emomethaneBRLmg/kg 0.0096 0.00056 826DB 05/26/07 506 erusseii 024504rbontetrachlorideBRLmg/kg 0.0048 0.00028 82608 06/26/07 506 erusseli 024504BRLmg/kg......0 Pj8 0Q_i ../5qo L..SeIL 245o4
lometharie BRL mg/kg 0.0098 0.00039 82608 06/26/07 506 erusseM 024504loroformBRLmg/kg 0.0048 0.00035 826DB 06/26/07 506 erussell 024504loromethaneBRLmg/kg 0.0048 000034 826GB 06/26/07 506 erusseJt 02450412-Dlchfomethene BRL mg/kg 0.0048 0.00021 82608 06/26/07 506 erusseil Q24504l.3-Dlchtoitpropene BRL mg/kg 0.0048 0.00031 826DB 06/20/07 506 erusseli 024504hiorodifiucromethaneBRLmg/kg 0.0048 0.0011 826DB 06/26/07 506 erussell 024504ylbenzene0.0020 mg/kg 0.0048 0.00034 8260B 06/26/07 506 erusseli 024504ropyletherIPEBRLmg/kg 0.0048 0.00018 826DB 06/26/07 508 enisselI 024504ropylbenzeneBRLmg/kg 0.0048 000038 82608 06/26/07 508 erusseil 024504XyionesBRLmg/kg 0.0096 0.00067 826DB 06126/07 506 erusseli 024504iytethylketoneMEKBRLmg/kg 0.096 0.0013 82608 06/26/07 506 erusseli 024504yItbutyietherMTBEBRLmg/kg o.oog 0.00028 82608 06/26/07 506 erusseil 024504iylerjechlorideBRLmg/kg 0.0048 0.00039 826DB 06/26/07 506 erussetl 024504tylbenzeneBRLmg/kg 0.0048 0.00038 826GB 08/26/07 506 erusseti 024504
This report should not be reproduced except In lts.enfjre Without the Written consent ci Prism Laboratori Inc449SprngbroRoadP.O Box 240543 Charfotte NC 28fl4.gaPhone704f52g-63 Toil Free Number 1-8001529.6364 Fax 704/525.0499 Page 30 of 35
NC Certification No 402
Laboratory ReportSCCertificationNo99012
NC Drinking Water Cart No 37735
06/29/07
ESP Associates PA
Project ID Morehead Commons No Client Sample lD B-ittnChrisWard
Prism Sample ID 184956Box7030SampleMatrixSoilCCCGroupG0607542haijoLte1NC28241
Time Collected 06/19/07 1700
Time Submitted 06/19/07 1735
arameter Result Units Report MDL Dilution Method Analysis AnalysFactorDate/Time
0.0041
BRL
BRL
BRI
BRL
BRL
BRL
0.0048
BRL
SRI
05/28/07 505
06/26/07 506
06/26/07 506
06/26/07 506
06/26/07 506
06/26/07 506
06/26/07 506
06/26/07 506
06/26/07 506
06/26/07 505
laphthalene
mg/kg 0.0096 0.00058 826DB
-Xyiene mg/kg 0.0048 0.00029 82808
-lsopropyltottjene mg/kg 0.0048 0.00039 82608
ec-Butylbenzene
mg/kg 0.0048 0.00032 826DB
tyrene
mg/kg 0.0048 0.00048 626DB
rt-Butylbenzene
mg/kg 0.0045 0.0003 826DB
IrathIoroethene
mg/kg 0.0048 0.00062 82605
luene
mg/kg 0.0048 0.00033 826DB
ns-1 2-Dlchloroetfene mg/kg 0.0048 0.00036 826DB
fl-l.3-Dichoropropere mg/kg 0.0048 0.00034 826DBoroethenegB00002982605 D6/26/erussell 024504
yl acetate SRI mg/kg 0.024 0.0017 826DB 06/26/07 505 erussell 024504iylchlorideSRImg/kg 0.0048 0.00061 82605 06/26/07 506 erussell 024504
erusseil
erussell
erussell
erussell
erusseil
aflJsselJ
erussefl
erusseil
erussell
erusseji
024504
024504
024504
024504
Q245D4
024504
024504
024504
024504
024504
Surrogate Recovery Control Limits
Dlbrcmofluoromethane 96 67-143
Sromofluorobenzene 108 77-128
Toluene-dg 109 81 128
iryolatflo Organj Compounds by GC/MS
4-Trlchlorobenzene SRI mg/kg 0.40 0.040
Dlchlorober.zene BRL mg/kg 0.40 0.030
Dichlorobepzene SRI mg/kg 0.40 0.026
Dlchiorobenzene BRL mg/kg 0.40 0.036
S-Trlchlorophenof SRi.mg/kg 0.40 0.041
-TrIchIorophenol BRL mg/kg 0.40 0039
8270C 06/26/07 2053 hcamptgo 024532
8270C 06/26/07 2053 kcamplgotto 024532
8270c 06/25/07 2053 kcampigo 024532
8270C 05/26/07 2053 kcampl9otio 024532
8210C 06/26/07 2053 kcamplgoo 024532
82700 06/26/07 2053 kcampIoti 024532Thisreportshouldnotbereproducedexceptin Its entirety without the written consent of Prism Laboratories Inc449SpringbroOjçRoadP.O Box 240543 Charlotte NC 28224-9543Phone704/529-6364 Toll Free Number 1-8OO/529..63 iax 7041525.0409 Page 31 of 35
FL
ESP Associates PA
Attn Chris Ward
P.O Box 7030
harJotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons Nb Client Sample ID
Prism Sample IDSampleMatrixSoilCOCGroup
Time Collected
Time Submitted
B-I
184956
G0607542
06/19/07
06/19/07
arameter Result Units Report MDL Dllutio Method Analysis Analyst Batch
.4DlmethyIphenol BRL mg/kg 0.40 0.039 8270C
4-Dlnhtrophenol BRL mg/kg 2.0 0.045 827CC
.4-Dlnltrotoluene BRL mg/kg 0.40 0.023 8270C
S-Dlnltrololueno BRL mg/kg 0.40 0.043 8270C
-Chloronaphthajene BRI mg/kg 0.40 0.041 8270C
-Chlorophenol BRL mg/kg 0.40 0.032 627CC
Methylnaphthalene BRL mg/kg 0.40 0.032 827CC
Methylphenoi BRL mg/kg 0.40 0.038 8210C
Nitrophenol BRL mg/kg 0.40 0.048 827CC
i4-MethyIphenoI BRL mg/kg 0.40 0.041 827CC
3Lchiprobezk1Ine SRLjg 080 0025 827CC 06/26/07 2053 kcamplgouo 24532/k2o ..
Bromophel-iyfphenylether BRL mg/kg 0.40 0.038 8270C
ChIoro..3.methyjphenoi BRL mg/kg 0.80 0.030 827CC
hIoroanI1Ine BRL mg/kg 0.40 0.051 827CC
hIoiopheny1phenylether BRL mg/kg 0.40 0.025 8270C
Jitrophenol BRL mg/kg 2.0 0.027
enaphthene BRL mg/kg 0.40 0.030 827CC
enaphthyjene BRL mg/kg 0.40 0.040 827CC
thracene
0.12 mg/kg 0.40 0.030 827CCbenzeneBRLmg/kg 2.0 0.037 827CC
rlzoaanthracene 0.19 mg/kg 0.40 0.056 827CC
lzoapyrene 0.21 mg/kg 0.40 0.046 827CC
lzobfluoranthene 0.33 mg/kg 0.40 0.018 827CCzoghjpeye00.13.1 mg/kg 0.40 0.019 8270Czokfluoranthene0.23 mg/kg 0.40 0.033 827CC
This report should not be reproduced except In its entirety Without the written const of Prism Laboratofl Inc4498prIngbroRoadP.O Boar 240543 Charlotte NC 28224.0543Phone704/529..6364 Toll Free Number 1-800/529.6364 Fax 704/525o4g9
Laboratory Report
06/29/07
1700
1735
06/26/07 2053 kcamplgotlu
06/26/07 2053 kcamplgotia
06/26/07 2053 kcampgouo
06/26/07 2053 kcarnplgotto
06/26/07 2053 kaaniplgotto
06/26/07 2053 kcemplgotto
06/25/07 2053 kcamplgotjo
06/2607 2053 koamplgotto
06/26/07 2053 kampIgotto
06/26/07 2053 kcampgotto
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
06/26/07 2053 kcamplgoita
06/26107 2053 kcamplgofto
06/26/07 2053 kcampjgono
06/26/07 2053 kcamplgotjg
06/26/07 2053 kcempigouo
06/26/07 2053 kcamplgouo
06/26/07 2053 kcampigo
06/2607 2053 kcamplgotio
06/26/07 2053 kcamprgotto
06/26/07 2053 kcamplgoito
06/26/07 2053 kcampJgotjc
06/26/07 2053 kcamplgotto
06/26/07 2053 kcarnppgoLto
08/26/07 2053 kcamplgott
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
024532
Page 32 of 35
ESP Associates PA
ttn Clijs Ward.O Box 7030
Jharlotte NC 28241
Laboratory Report
06/29/07
B-I
184956
G0607542
06119/07 1700
06/19/07 1735
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample IDSampleMatrixSoilcocGroup
Time Collected
Time Submitted
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
enzyl alcohol BRL mg/kg 0.80 0.042 827CC 06/28/07 2053 kcamplgotto Q24532is2-chloroethoxymethane BRL mg/kg 0.40 0.046 827CC 06/26/07 2053 kcamplgoito 024532fs2-chioroethylether BRL mg/kg 0.40 0.044 827CC 05/26/07 2053 kc2rnplgctto 024532is2-chforo1sopropyI BRL mg/kg 0.40 0.034 827CC 06126/07 2053 kcamplgDtto 024532I52ethylhexyQphtha0BRLmg/kg 0.40 0.020 8270C 06/26/07 2053 kcamptgouo 024532utylbenzylphthalaeBRLmg/kg 0.40 0.025 827CC 06/28/07 2053 kcamplgono 024532hrysene0.20 mg/kg 0.40 0.067 827CC 05/26/07 2053 kcamplgallo 024532-flbutylphthalate ERL mg/kg 0.40 0.018 82700 06/26/07 2053 kcamplgotto 024532n-octylphthaIate BRL mg/hg 040 0.030 82700 06/26/07 2053 kcampfgotto 024532benzoal1anthraceneBRLmg/lg 0.40 0.040 82700 06/26/07 2053 kcarnpgotto 024532benzofur2n
0.034 827CC O6/2O7 2053 kcamcioito 024532thiphLhaIatcBRLmg/kg 0.40 0.025 827CC 06/26/07 2053 kcamptcoliethyiphihapateBRLmg/kg 0.40 0.027 82700 06/26/07 2053 kcamplgoo 024532lorantliena
0.51 mg/kg 0.40 0.028 62700 06/26/07 2053 kcarnpjgouj 024532loreneOilmg/kg 0.40 0.024 82700 06/26/07 2053 kcamplgotto 024532xachlorobenzeneBRLmg/kg 0.40 0.021 82700 06/26/07 2053 kcampl6ojto 024532xachlorobutadjeneBRLmg/kg 0.40 0.039 827CC 08/26/07 2053 kcemplgotio Q24532achlorocycIopefltadleneBRLmg/kg 0.40 0.043 82700 06/26/07 2053 kcamplgot 024532achioroethaneBRLmg/kg 0.40 0.041 82700 06/26/07 2053 kcampl9ottp 024532eno123cdpyne0.30 mg/kg 0.40 0.041 82700 06/26/07 2053 kcampigotto 024532horoneBRLmg/kg 0.40 0.036 82700 06/26/07 2053 kcamplgotto 024532fltrosodl.n.propyfamjne BRL mg/kg 0.40 0.046 82700 06/26/07 2053 koampIgollo 024532BRLmg/kg 0.40 0.020 82700 06/26/07 2053 kcamplgotto 024532hthaleneBRLmg/kg 0.40 0.044 82700 06/26/07 2053 kcampfgo 024532benzeneBRLmg/kg 0.40 0.039 82700 06/26/07 2053 kcarnpigotlo 024532tachiorophenolBRLmg/kg 2.0 0.034 82700 06/26/07 2053 koampigofto 024532
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories ma449SpringbjRoadP.0 Box 240543 Charlotte NC 28224.O3Phone704/529.6364 Toll Pree Number 1-80Q/52D6364 Fax 704/525-0409 Page 33 of 35
NC Certificallon No 402
Laboratory ReportScCertificationNo99012
6/29/07
NC Drinking Water Cert No 37735
iIctAajyVcI
ESP Associates PA
Project ID Morehead Commons Mci Client Sample ID B-IttnChrisWard
Prism Sample ID 184958.0 Box 7030 Sample Matrix SoD COG Group G0607542harlotteNC28241limeCollected06/19/07 1700
Time Submitted 06/19/07 1735
arametor Result Units Report MDL Dilution Method Analysis Analyst atch
Limit Factor Date/Time ID
henanthrene 0.38 mg/kg 0.40 0.020 827CC 06/26/07 20.53 camp 024532henolBRLmg/kg 0.40 0.044 8270C 06/26/07 2053 kcamplgotto Q24532yrene0.49 mg/kg 0.40 0.027 827CC 06/2607 2053 kcamplgotto 024532
Sample Preparation 30.27 mL 355DB 06/22/b7 1100 dpope P18710
Surrogate Recovery Control Limits
2-Fluoroblphenyl 78 21 108
Nftrobenzene.d5 73 14-103
Terphenyl-d14 106 41-136
246-Thbromophenol 91 25-123
2-Fluorophenol 63 14 -89
Phenoid5 74 _1395
ctractable Petroleum Hydrocarbons by GC-FID
ll-C22Aromatica BRL mg/kg 12 6.4 MADEP EPH 06/24/07 559 grappaccioll 02451419-C36 Allphallcs BRL mg/kg 12 1.8 MADEP EPH 06/24/07 559 grappaccioll 024514-C18 Aliphatics BRL mg/kg 12 3.8 MADEP EPH 06/24/07 559 grappaccloll 024514AnalysisNoteforCli.-c22 Aromatjcs Adjusted value
Sample PreparatIon
10.44 mL EPH 06/21/07 800 9SPPaCcIDH P18703
Surrogate Recovery Contro Limits
o-Terpheriyi 83 40-140
2-Fluorobiphenyl 91 40 140
2-Bromonaphthalene 40-140
l-ChIoro-octadecane 92 40-140
tL.kJCP
omlum 32 mg/kg 0.27 0.016 6010B 08/25/07 1402 mcampbeQ 02451923mg/kg 0.27 0.023 60106 06/25/07 1402 mcampbell 024519
This report should not be reproducj except In its entirety without the written consent of Prism Laboratories Inc449SpringbrooRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-c3 Toll Free Numbsr 1-8OO/529-63 Fax 704/525-0409 Page 34 of 35
SP Associates PA
ttn Chris Ward
Box 7030
Tharlotte NC 28241
NC CertIfication No.402
SC Certification No 09012
NC Drinking Water Cerl No 37735
Laboratory Report
06129/07
184956
G0607542
06/19/07
06/19/07
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Daternme ID
Sample Preparation
Surrogate Recovery Control Limits
70-130
2S-Dibromotoluene..FJD 126
eight 1.94
--MADEP-VpH---..ü5/26107.0.00_IbrowneIght
MADEP VPH 06/26/07 000 Ibrcw
Below Reporting Limit
Estimated value between the Reporting Limit and the MDLresultsInthisreport relate only to the samples submitted for analysis and meet state certification requirements other than
LAC certificazlo except for those Instances Indicated In the case narrative and/or test commentsresultsarereportedondry-weight basis
This report should not be reproducj except In Its entirety without the written consent of Prism Laboratories Inc449SpringbrooçRoadP.O Bx 240543 Charlotte NC 20224-0543Phone704/5g.354 Toll Free Number 1-0QO/529..8 Fax 704/525-0409
Project ID Morehead Commons No Client Sample ID B-I
PrIsm Sample IDSampleMatrixSoilCOCGroup
Time Collected
Time Submitted
1700
1735
olatile Petroleum Hydrocarbons by Gc-PIDIFIO
5-C8 Aliphatics
9-Cia Aromatics
9-C12 AUphalics
227 50 niL 3050B 06/21/07 905 jhoppei P18702
BRL mgkg 6.2 12 MADEP VPH 06/27/07 1922 hwagner 024604BRLmg/kg 6.2 0.037 MADEP VPH 06/27/07 1922 hwagner
SRI mg/kg 6.2 1.9 MADEP VPH 06/27/07 1922 hwagner 024504a1ysjsNoteforc-c Aliphatics Adjusted valueAnalyej9NoteforC9-c12 Aliphatjcs Adjusted value
18.28
70-130
eia Overcash V.P Laboratory Services
Page 35 of 35
NC Certification No 402 Level II QC ReportSCCertificationNo99012
6/29107NCDrinkingWaterCertNo37735
ESP Associates PA
Project ID Morehead Commons No COC Group Number 00607542AttnChrisWard
Date/Time Submitted 6/19/07 1735Box7030
Charlotte MC 28241
Volatile Organic Comeounds byGC1MS method 82609
QOBatchResultRLCUtUnts
lll-Tr1chometha-e ND 0.015 0.0025 mg/kg Q245031122-Tetrachloroethane ND 0.005 0.0025 mg/kg 024503ll2TrlchIoroethaneND0.005 0.0025 mg/kg 024503li-Dichioroethane ND 0.005 0.0025 mg/kg 024503ll-DlchjoroetJene ND 0.005 0.0025 mg/kg 024503ll-Dlchloropropene ND 0.005 0.0025 mg/kg 024503l23-Trichlorobenzene ND 0.005 0.0025 mg/kg 024503l.2.3-Trichloropropane ND 0.005 0.0025 mg/kg 02450324-Trjchlorobenzene ND 0.005 0.0025 mg/kg 024593l.214-Trimethyjbenzene ND 0.005 0.0025 mg/kg 024503l2-Dlbromoethane EBB ND 0.095 0.0025 mg/kg 024503l2-Dlcblorobenzene ND 0.005 0.0025 mg/kg 024503l2-DjchIcjroetha ND 0.005 0.0025 mg/kg 024503l2-DIchIomprope ND 0.005 0.0025 mg/kg 0245033S-Thme ND 005 0025 mg/kg 024503lj3DI5htcb5nzenj_-ND--0005 -00025rng/kg ---Q2i503l3-DlchIÆropropane ND 0.005 0.0025 mg/kg 024503l4-Dlchlorobenzene ND 0.005 0.0025 mg/kg 02450322-DIchloropropane ND 0.005 0.0925 mg/kg 0245032-Chloroofuene ND 0.005 0.0025 mg/kg 0245032-Hexanone ND 0.05 0.025 mg/kg 0245034-Chlorotoluene ND 0.005 0.0025 mg/kg 0245034-MethyI2pennone MIBK ND 0.05 0.025 mg/kg 024503AcetoneND0.05 0.025 mg/kg 024503BenzeneND0.003 0.0015 mg/kg
024503BmmabenzeneND0.005 0.0025 mg/kg 024503BromochlommeneND0.005 0.0025 mg/kg
024503BromodfthlommethafleND0.005 0.0025 mg/kg 024503BromoformND0.005 0.0025 mg/kg
Q24503BromometiraneND0.01 0.005 mg/kg
024503CarbontetrachiojicleND0.005 0.0025 mg/kg 024503ChlorobenzeneND0.005 0.0025 mg/kg 024503ChiorodibromomethaneND0.005 0.0025 mg/kg
024503ChlometheND0.01 0.005 mg/kg
024503
This report should not be reproduced except In Its enUrety without the written consent of Prism Laboratori Inc449Spr1ngbroojRoadP.O Box 240543 ChaIjotte NC 28224.0543Phone704/529.5304 Toll Free Number 1-8Oo/529.s04 Fax 704/525.04g9 Page 0112
NCCertlficauonNo.402 Level IV QC ReportSCCertificationNo99012
6/29107NCDrinkingWaterCartNo37735
ESP Associates PA Project ID Morehead Commons COC Group Nuniber 00607542AttriChrisWard
Date/TIme Submitted 6/i 9/07 1735P.O Box 7030
Charlotte1 NC 28241
Method Blank
QC BUkResultRLControlUmrtlJrft5
Chlorofbrm ND 0.005 0.0025 mg/kg 024503ChloromethaneND0.005 0.0025 mg/hg 024503cm-i 12-DlchloroothanºND 0.005 0.0025 mg/kg 024503
cls-1 3-Dlchloropropene ND 0.005 0.0025 mg/kg 024503
Dlchlomdlfluoromethane ND 0.005 0.0025 mg/kg 024503
Ethylbenzene ND 0.005 0.0025 mg/kg 024503
Isoprepyl ether IPE ND 0.005 00025 mg/kg ô24503
lsopropylbenzene ND 0.005 0.0025 mg/kg 024503mp-Xyjenes ND 0.01 0.005 mg/kg 024503MethylethylketoneMEKND0.1 0.05 mg/kg 024503
Methyl t-butyl ether MTBE ND 0.01 0.005 mg/kg 024503MethylenechlorideND0.005 0.0025 mg/kg 024503n-Butylbenzene ND 0.005 0.0025 mg/kg Q24503
n-Prcpylbenzene ND 0.005 0.0025 mg/kg 024503NaphthaleneND0.01 0095 mg/kg 024503
0.0025 mg/kg 024503p-lsopropyflojuene-Ni 0005 00025-mg/kg 024503-----------_L -_.z____
____-___secBtityJbenzene ND 0005 00025 mg/kg
Styrene ND 0.005 0.0025 mg/kg 024503tert-Butylbenzene ND 0.005 0.0025 mg/kg 024503TetrachloroatheneND0.005 0.0025 mg/kg 024503TolueneND0.005 0.0025 mg/kg 024503trans-l2.Dlchloroethene ND 0.005 0.0025 mg/kg 024503trans-i 3-Dlchlompropene ND 0.005 0.0025 mg/hg 024503TrichioroetheneND0.005 0.0025 mg/kg 024503TzichlorofJuoromethaneNI0.005 0.0025 mg/kg 024503VinylacetateNI0.025 0.0125 mg/kg 024503
mg/kg
Recoeiy
Result Spike Amount Unjik
ID
ll-Dlchloroethene 0.05169 0.05 mg/kg 103 57-122 Q24503Benzene0.04711 0.05 mg/kg 94 62-119 024503Chiorobenzene0.0465 0.05 mg/kg 93 61-124 024503Toluene0.0443 0.05 mg/kg gy 57-122 Q24503Trichloroeihene0.04755 005 mg/kg 95 59-129 024503
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratori Inc449SprIngbroojRoadP.O Box 241543 Chartotte NC 28224-054Phone704/529-5364 Toll Free Nwnber 1-810/529-6364 Fax 704525-0409 Page of 12
NC Cerliflcatjon No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Sample 10 Result SpIke Miount Unile ID
184829 l1-DichIoj-oeen 0.04873 0.05 mg/kg 97 44-140 024503Benzene0.04413 0.05 mg/kg 88 46-136 024503Chiorobenzene0.04321 0.05 mg/kg 65 47-135 024503loluene0.03721 0.05 mg/kg 74 47-136 024503Tnchloroethen004365005mg/kg
RPD RRfl$OCBaIchSampleIDResultSpikeMipuntuniteID184829ll-Dlchtoroethene 0.04634 0.05 mg/kg 93 44140 -.23 024503Benzone0.042 0.05 mg/kg 84 46-136 -22 024503Chlurobenzeno0.04175 0.05 mg/kg 84 47-135 -22 024503Toluene0.04015 0.05 mg/kg 80 47-136 -22 024503Thchloroethene0041540.05 mg/kg 83 45-141 -23 024503
This report should not be reproduced exceptln Its entirety without the Written Onsento1pm Laboratories Inc4498prlngbroojcRoadP.O Box 240543 Charlotte NC 28224-0543Phone704I52g..534 Toll Free Number 180Oj52.g.6364 Fax 704/525.0409
Level II QC Report
6/29/07
Project ID Morehead Commons COC Group Number G0607542DateSubmitted6/19/07 1735
Page of 12
NC Cerlificatlon No 402 Level II QC ReportsolflcanonNo99012
6/29/07NCDr1nkngWaterCartNo37735
ESP Associates PA
Project ID Moreheacl Commons No COC Group Number G0607542AttnChrisWard
Daterflrne Submitted 6/19/07 1735Box7c330
Charlotte NC 28241
Volatile Organic ComDounas by GCIMs method 8260B
CI BatchContratimlUnta
lll-Trjchioroethane ND 0.005 0.0025 mg/kg 0245041122-Tetracflloroethane ND 0.005 0.0025 mg/kg 024504112-Trichloroethare ND 0.005 0.0025 mg/kg 024504ll-Dichloroethane ND 0.005 0.0025 mg/kg 024504ll-DIchloroetjiene ND 0.005 0.0025 mg/kg 024504ll-Dlchtoropropene ND 0.O05 0.0025 mg/kg 024504l.23-Trfchloroberizene ND 0.005 0.0025 mg/kg 024504lZ3-Tdchlornpmpane ND 0.005 0.0025 mg/kg 02450424-Tflchlorobenzene ND 0.005 0.0025 mg/kg Q24504l24-Trimethybmzene ND 0.005 0.0025 mg/kg 0245042-Dlbromoeuian EDB ND 0.005 0.0025 mg/kg 0245042-Dichjorobz ND 0.005 0.0025 mg/kg Q24504l2-Djchioroeljiane ND 0.005 0.0025 mg/kg 024504I.2-Dlchioropropane ND 0.005 0.0025 mg/hg 02450435TflmethylbenzeneND00500025mg/kg 024504
---g/kg--Q24504l.3-DichIoropropane ND 0.005 0.0025 mg/kg 024504l4-Dichfcrobenzene ND 0.005 00025 mg/kg 024504212-Dichtoropropane ND 0.005 0.0025 mg/kg 0245042-Chiorotojuene ND 0.005 0.0025 mg/kg 0245042-Hexanone ND 0.05 0.025 mg/kg 0245044-Chforotoluene ND 0.005 0.0025 mg/kg 0245044-MelhyI-2.pennone MIBK ND 0.05 0.025 mg/kg 024504AcetoneND0.05 0.025 mg/kg 024504BenzeneND0.003 0.0015 mg/kg 024504SromobenzeneND0.005 0.0025 mg/kg
024504BromochioromethaneND0.005 0.0D25 mg/kg 024504BmmodichjoromethaneND0.005 0.0025 mg/kg
024504BromofboijNDOOQ50.0025 mg/kg 024504BromomethaneND0.01 0.005 mg/kg
024504Carbontetrachloijd8ND0.005 00025 mg/kg
024504ChiorobeazeneND0.005 0.0025 mg/kg
024504ChIorodjhiTjmomethaneND0.005 0.0025 mg/kg
024504ChioroetfianeND0.01 0.005 mg/kg
024504
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratmjes Inc44SpringbroocRoadP.O Box 240543 Chaflott NC 25224-0543Phone704/529.Toil Free Number l-809/529.esM Fax 704/525.0499 Pag840f12
NCCertUcatfonNo.402 Level II QC ReportScCertificationNo99012
612907NCDrinkingWaterCertNo37735
ESP Associates PA
Project ID Morehead Commons No COO Group Number G0607542AttnChrisWard
Date/TIme Submitted 6/19/07 1735Box7030
Charlotte NC 28241
UC BaichResultRLCoirlLimitUiI10
Chloroform ND 0.005 0.0025 mg/kg 024504ChioromethaneND0.005 0.0025 mg/kg 024504cls-1 2-Dfchloroethene ND 0.005 0.0025 mg/kg 024504cls-1 3-Dichlompropene ND 0.005 0.0025 mg/kg 024504DlchlorodjfluoromethaneND0.005 0.0025 mg/kg 024504EthylbenzeneND0.005 0.0025 mg/kg 024504Isopropyl ether IRE ND 0.005 0.0025 mg/kg 024504IsoprcpylbenzeneND0.005 0.0025 mg/kg 024504mp-Xylenes ND 0.01 0.005 mg/kg 024504MethylethylketoneMEKND010.05 mg/kg 024504Methylt-butyt ether MTBE ND 0.01 0.005 mg/kg 024504MethyjenechlorideND0.005 0.0025 mg/kg 024504n-Butyibenzene ND 0.005 0.0025 mg/kg 024504n-Propylbenzene ND 0.005 0.0025 mg/kg 024504NaphthaleneND0.01 0.005 mg/kg 024504........D mg/kg 024504ND---0jOo5--00025---mg/kg Q245o4-IeButlbetzene ND 0.005 00025 g/kg 024504SiyreneND0.005 0.0025 mg/kg 024504tert-Butylbenzene ND 0.005 0.0025 mg/kg 024504TetrachlooetheneND0.005 0.0025 mg/kg 024504TolueneND0.005 0.0025 mg/kg 024504trans.12.Dlchjro00 ND 0.005 0.0025 mg/kg 024504trans_i 3-Dlchloropwpene ND 0.005 0.0025 mg/kg Q24504TrichioroetheneND0.005 0.0025 mg/kg 024504IrichiorofluoromethaneND0.005 00025 mg/kg 024504VinylacetateND0.025 0.0125 mg/kg Q245a4
0.0025 mg/kg
Result Spike Amount Units
ID
ll-Dlchloroethene 0.05154 0.05 mg/kg 103 57-122 024504Benzene0052320.05 mg/kg 105 62-119 024504Chlorobenzene0.05096 0.Os mg/kg 102 61-124 024.504Toluene0.04808 0.05 mg/kg 95 57-122 024504Trlchtoroethena0.0533j 0.05 mg/kg 107 59-129 Q245a4
This report should not be reproducJ except In its entirety without the written consent of PrIsm Laboratoj Inc
449 Sprjngbrok Road P.O Box 240543 Charlotte NC 28224-0543Phone7041529-6354 Toll Free Number 1-80015294354 Fax 7041525-0409 PageS of 12
NCCertificatlonNo.402 Level II QC ReportScCertificationNo99012
6129/07NCDrinkingWaterCartNo37735
ESP Associates PA Project ID Morehead Commons No Coc Group Number 00607542AttriChrisWard
Date/lime Submitted 6119107 1735Box7030
Charlotte NC 28241
ely Renges QC BatsSample ID Resull SpJke Amount units ID
184929 ll-Dtchloroethene 0.04141 0.05 mg/lcg 83 44-140 024504Benzene0.0423 0.05 mg/kg 85 46-136 024504Chlorobenzene0.034 0.05 mg/kg 59 47-135 024504Toluane0.0377 0.05 mg/kg 75 47-136 024504Trichloroetbene00429605mu/kg 86 45-141 024504ipIkeDupIjcat
Result SPIkeAmDUnt Units
184929 lj-DIchloroethe 0.03788 0.05 mg/kg 76 44-140 -23 024504Benzene0.03917 0.05 mg/kg 78 45-138 -22 024504Chlctrobenzene0.03223 0.05 mg/kg 64 47-135 -22 024504ioluene0.03417 0.05 mg/kg 47-136 10 -22 Q24504Trichloroetliene0.03959 0.05 mg/kg 79 45-141 -23 024504
Extractable Petroleum Hvdrocarbop by GC.FID method MADEP EPH
Result RL Co Unni Units
C11-c22 Aromatics ND 10 mg/kg 024514Cl9-03AIphancs------ND.-_jQ----5----rug/kg---024514
mg/kg
Recovery Recovery
Result Spike Amount Units ID
C11-C22Aromadcs 140.16 170 mg/kg 82 40-140 024514C19-C3BAJjphaucs 66.18 80 mg/kg 83 40-140 Q24514S18AIIfi44.8260 mg/kg
Sample ID Result SreAnount Units ID184697C11-C22 Aromatlcs 135.2 170 mg/kg 80 40-140 024514C19-C36 Aliphatlcs 76.88 80 mg/kg 98 40-140 024514C9Cl8AHphatics469460
RecoverySamplelDResultSpIkeAmountults
ID184697Cll-C22Aromallcs 146.88 170 mg/kg 86 40-140 0-50 024514Cl9-C36 Allphatics 63.12 80 mg/kg 79 40-140 20 0-50 024514C9-C18 Allphatics 41.44 60 mg/kg 69 40-140 12 0-50 024514
This report should not be repraducecJ except In Its entirety without the written consent or Prism Laboratories Inc449SprJngbrOojRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529.5364 Toll Free Number 1-8001529-6364 Fax 704/525.0409 Page of 12
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Metals by ICP method 6jfldBlank-
acoResultRIoiflrilimitUnItsto
Chromium 0.0507 0.25 0.125 mg/kg 024519
Result SpIke Aiflount tinfls ID
Chmmlum 24.9411 25 mg/kg ioo 80-120 024519_________835 mg/kg 99 80-120 Q24519
SampleID alt SplkaAmount Unite ID184957ChromIum41.1677 20.746 mg/kg 102 75-125 Q24519
mg/kg
REtUVeIy Reca vary
Ranges APO RangeSampleIDResultSpikeMiountUnIIs%
to184957ChromIum42.4881 23.255 mg/kg 97 75-125 0-20 024519Lead35.0702 23.255 mg/kg 56 75-125 -20 024519
This report should not be reproduced except In Its entirety wIthout the written consent of Prism Laboratories Inc449SprfngbRoadP.O Box 240543 Charlotte1 NC 26224-0543Phone704/529.6354 Toll Free Number l-800/529-63M Fax 704/525.O4
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level QC Report
6129107
Project ID Morehead Commons No COG Group Nurn ber G0607542
Daternme Submitted 6/19107 j735
Page of 12
NCCerUficatIonNo.402 Level If QC ReportSCCertificafforiNo99012
6/29/07
NC Drinking Water Cert No 37735
ESP Associates PA
Project ID Morehead Commons No COC Group Number G0607542AttnChrisWard
Date/Time Submitted 6/19/07 1735Box7030
Charlotte1 NC 28241
ornJoIie Organjc Compounds GCIMS method 870C
ocRasultRLCoralULUnIID
i214-Trlchlorobenzene ND 0.33 0.165 mg/kg 024532l2-Dichtorobenzene ND 0.33 0.165 mg/kg 024532l3-Dlchiorobenzene ND 0.33 0165 mg/kg Q24532l4-Dlchlorobenzone ND 0.33 0.165 mg/kg 0245322.45-TuichIorophenoJ ND 0.33 0.165 mg/kg 0245322.46TdchlomphenoI ND 0.33 0.165 mg/kg Q24532214DIchIoropheriojND0.33 0.165 mg/kg 024532214-Dlrnethyfphenol ND 0.33 0.165 mg/kg Q24532214-Dlnhtmphenoj ND 1.65 0.825 mg/kg 024532214-Dlnjtmtoiuene ND 0.33 0.165 mg/kg 024532216-Dlnltmtoluene ND 0.33 0.165 mg/kg 0245322-Chloronaphthatene ND 0.33 0.165 mg/kg 0245322.ChIopheno1 ND 0.33 0.165 mg/kg 0245322-Methylnaphthalene ND 0.33 0.165 mg/kg 0245322-Methylpho ND 033 0165 mg/kg 024532---Æi----34-Mthyiphanol ND 0.33 0.165 mg/kg 0245323.3-DIchIorobenzIdlne ND 0.65 0.33 mg/kg 0245324.6-Dinhtm-2.methylphenoj ND 1.65 0.825 mg/kg 0245324-BromophenylphenyIe5 ND 0.33 0.165 mg/kg 024532ND0.66 0.33 mg/kg 0245324-Choroanlllne ND 0.33 0.165 mg/kg 0245324Chl0ropheflyIphenyIetherND0.33 0.165 mg/kg 0245324-Nltmphenoj ND 1.65 0.825 mg/kg 024532AcenaphtheneND0.33 0.165 mg/kg
Q24532AcenaphihyleneND0.33 0.165 mg/kg 024532AnlhraceneND0.33 0.165 mg/kg
024532AzobenzeneND1.65 0.825 mg/kg
024532BenzoaanthraceneND0.33 0.165 mg/kg
024532BenzoapyreneND0.33 0.165 mg/kg
024532BenzobgIuorantheneND0.33 0.165 mg/kg
024532BenzhipeiyleneND0.33 0.165 mg/kg
024532BerzokIIuorafltheneNI0.33 0.165 mg/kg
024532BenzoicajND1.65 0.625 mg/kg
Q24532
This report should not be reproduced except in its entirety withut the written consent of Prism Laboratories mo449SprfngbjrooçRoadP.O Box 240543 CharfoBo NC 2522.4-0543Phone104/52g..82 Toll Free Number 1-8001529.6354 Iax 704/525-0409 Page 0112
NC Certification No 402 Level II QC ReportSCCertificationNo99012
6/2907NCDrinkingWaterCertNo37735
ESP Associates PA
Project ID Morehead Commons No GOC Group Nurnber 00607542AttnChrisWard
Date/Time Submitted 6/19/07 1735Box7030
Charlotte NC 28241
OCResultRLCmtmllimitUnjis ID
Benzyl alcohol ND 0.66 0.33 mg/kg 024532
Bis2-chtoraethoxymethane ND 0.33 0.165 mg/kg 024532Bls2-chloroethyefij ND 0.33 0.165 mg/kg 024532
Bls2-dllorolsopropyiether ND 0.33 0.165 mg/kg Q24532Bls2-ethylhexyIph3t0 ND 0.33 0.165 mg/kg 024532ButylbenzyiphthatateND0.33 0.165 mg/kg 024532ChryserieND0.33 0.165 mg/kg 024532DI-fl.buLyIphthaIa ND 0.33 0.165 mg/kg 024532Di-n-octyIphthala ND 0.33 0.165 mg/kg 024532DibenzoahanthceneND0.33 0.165 mg/kg 024532DlbenzofljranND0.33 0.165 mg/kg 024532DlethyiphtlialateND0.33 0.165 mg/kg 024532DlmethyiphthajateNi0.33 0.165 mg/kg 024532FluorantheneND0.33 0.165 mg/hg 024532FluoreneND0.33 0165 mg/kg Q24532ND0.33 0.165 mg/hg 2453O3D165mg/kg---Q24532hlorooycIopeidjeneND033O.165 mg/kg 024532HexachioroethaneMD0.33 0.165 mg/hg 024532lndeno123JpyND0.33 0.165 mg/kg 024532IsophoroneND0.33 0.165 mg/kg 024532N-Nftrosodi..npropylamjne ND 0.33 0.165 mg/kg 024532N-NftrosodIphenyiamIe ND 0.33 0.165 mg/kg 024532NaphiftajeneND0.33 0.165 mg/kg 024532NlfrobenzeneND0.33 0.155 mg/kg 024532PentachiorophenolND1.65 0.825 mg/kg 024532PhenanthreneND0330.165 mg/kg Q24532PhenolND0330.I5 mg/kg 024532
mo/kg
Recoveiy VeY QCBatctiSaAmo
l24-Trlchlorobenzarie 1.2455g 1.6558 mg/kg 75 39-98 024532l4-DichIorobepz 1.15622 1.6658 mg/kg 69 37-95 024532Z4-Dinftrotofu6ne 171598 1.6658 mg/kg 103 56-128 0245322-Chlorophenol 1.14223 1.6658 mg/kg 89 37-98 0245324Chloro.3euyJphenol 1.42271 1.6658 mg/kg 85 45-111 024532ThisreportshouldnotbereproducedexceptInItsentiretywithoutthewrittenconsentofPrismLaboratojInc4495prngkg.c Road P.O Box 240543 Charlotte1 NC 28224-0543Phone704f523TollFreeNwnbec1-8001525-5364 Fax 704/525-0409 Page of 12
NC Certification No 402 Level II QC ReportSCCertificationNo99012
6/29/07NCDrinkingWaterCertNo37735
ESP Associates PA
Project ID Morehead Commons No COG Group Nurnber G0607542AttnChrisWard
Date/Time Submitted 6119107 1735Box7030
Charlotte NC 28241
Laboratory Control Sample RVY cc BatchReauJLSglkeAmountUnits
4Nltrophenol 1.60359 1.6558 mg/kg 96 20-157 024532Acenaphthene1.44903 1.6658 mg/kg 87 44-110 024532
N-Nilmsodi.mpropyjamine 1.33710 1.6658 mg/kg 50 38-101 024532
Pentachlorophenol 1.78014 1.6655 mg/kg 107 53-127 024532Phenol1.13091 1.6658 mg/kg 65 34-102 024532
Matrix Spike
13091 1658
Recoamy RySBnlptoIDReSUltSpHtMioUnLUnits ID
184696 l214-Tijchlorobenzene 1.18009 1.6547 mg/kg 71 26-97 024532l4-Dlchlorobenzane 1.14813 1.6647 mg/kg 69 23-92 02453224-Dinltrooiuene 1.57856 1.6547 mg/kg 95 45-127 024532
2-Chlomphenol 1.13681 1.6647 mg/kg 68 25-94 0245324Chiom-3.methphenol 1.29527 1.6647 mg/kg 78 31-113 0245324-Nitmphenoj 1.55225 1.5647 mg/kg 94 17-150 024532Acenaphthene1.34986 1.6647 mg/kg si 35-107 024532
024532__Q232Phenolt05525mg/kg 63 23-97 Q24532
Matrix Spike Duplicate Re RPD
Ranltos RPD RangeResultSpikeAmount
Urle
184696 l.24-Trichlorobenene 1.28538 1.6614 mg/kg 77 26-97 0-37 024532l4-Dlchlorobenzene 1.16843 1.6614 mg/kg io 23-92 -36 02453224-Dlnifrotoluene 1.59634 1.6614 mg/kg 96 45.127 0-29 Q245322-Chlorophenol 1.19966 1.6614 mg/kg 72 25-94 0-37 0245324-Chlom.3-methyiphenol 1.3465j 16614 mg/kg ai 31-113 -32 0245324-Nltrophenol 1.52624 1.6614 mg/kg 92 17-150 0-32 024532Acenaphthene1.40598 1.6614 mg/kg 85 38-107 0-32 024532N.Nftrosodl..n.propylam Inc 1.22958 1.6614 mg/kg 74 22-105 0-37 024532Pentachlorophenol1.75913 1.6614 mg/kg 105 39-137 0-27 024532Phenol1.04684 1.6614 mg/kg 63 23-97 0-42 024532Pyrene1.61229 16614 mg/kg 97 45-133 0-27 024532
This report should not be repmduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Springbro Road P.O Box 240543 Charlotte NC 28224.0543Phone704/529.6354 Toll free Numbec 1-890/529.6384 Pajc 1041525-0499 Page 10 0112
NC Certification No 402 Level II QC ReportScCertificationNo99012
6/29/07_______NC Drinking Water Cert No 37735
ESP Associates PA
Project ID Macahead Commons No Coc Group Number G0607542AttoChrisWard
Date/TIme Submitted 6/1 9107 1735Box7030
Charlotte NC 28241
Volatile Petroleum Hydrocarbons by GC-PLDIFID thOdMADEP VP1i
Method Blank
00 BatchResultRICOntrolLAnkUnftstoC5-C Aliphalics ND 2.5 mg/kg Q24582CO-Cia Aromatics ND 2.5 mg/kg Q24582
Result Sptke Amount tints ID
C5-C8 Aliphatics 17.765 15 mg/kg 118 70-130 Q24582CO-Cia Aromatios 5.138 mg/kg 103 70-130 Q24582xS11.317 10 mg/kg 113 70-130 Q24582
Resu Spke Amount Units ID184695C5-C8 Allphatics 15.220 15 mg/kg ioi 70-130 Q24552CD-C1QAroaflcs 4.333 mg/kg 87 70-130 Q245821Aliphaflcsiomg/kg Ra
---184695 5-8lphatlcs -l5 067 -----15-----0-25 Q24582CO-do Aromafles 4.446 mg/kg 89 70-1 31 -25 Q24582CO-Cl2AlIphaffcs 12.999 10 mg/kg 130 70-130 0-25 Q24582
This repozt should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SprinjbrotJRoadP.O Bo 240543 Charlotte NC 28224-0543Phone704/529..8305 Toll Free Number 1-8001529.8305 Fax 7041525-0409
wvtc AnaJytJcIi Env npnThj riiuUon
Page 11 o112
NC Certification No 402
SC Certification No 99012
______NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Chatiotte NC 28241
Volatile Petroleum Hydrocarbons bVGC-PIDIFID method NIADEP VPH
Method Blank
Uc BelchResultRLCmThoiUmItUnh.s ID
C5-CAllphatjcs ND 2.5 mg/kg Q24604C9-C1oAj ND 2.5 mg/kg Q24604C9-C12 Allphatics ND 2.5 mg/kg Q24604LaoratoryontrolSample
Recovery P.ari 00 BatchResultSpikeAmount
ID
C5-C8 Aliphalics 16.779 15 mg/kg 112 70-130 024604C9-C1O Aromatlcs 4.305 mg/kg 88 70130 02460410.922 10 mg/kg Re RovewSampIalDResultSpikeAmountUnits ID
184956 C5-C8 Allphatics 16.625 15 mg/kg iii 70-130 024604CO-CloAromatics 4.148 mg/kg 83 70130 024604
Reouvey Ranges RangeResultSplheAmountTL184956qC8Aiphpucs._17-936IS--mg/kg -120 70-180-----0-25-024604C9-ClQAromabcs 4.279 mo/kg 86 70-130 0-25 024604C9C12Aflphallcs13.613 10 mg/kg 136 70-130 0-25 024604/1-See Case Narrative
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc
449 Spijngbro Road P.O Box 240543 Charlotte NC 28224-0543Phone704/529.5364 Toll Free Numb 1-800/5294364 Fax 704/525-0409
Ansnm5aa
Level II QC Report
6/28/07
Project ID Morehead Commons No coc Group Number 00607542
Date/Time Submitted 8119/07 1735
Page 12 of 12
Full Sendce MaJyUcal EnvIronmental SolutIons
449 8prlnbrook Road P.O Box 240543 Charlotte NC 28224-054aPhone704/829-8364 Fax 704/5
Client Company Name
Report To/Contact Name
Reporting Address
Phone ________________Fax Yes No_____________
Email Yes No Email Address_
EDD Type PDF_ExceL_Ot _______________
Site Location Name ______________________________
Site Location Physical Address
CHAiN OF CUSTODVRECORD
Short I-laId AnalysIs Yes No US1Frojecb Yes NoPleasaATTACHanyprojectspecificrepLEVELIIIIIIIV
Purchase Order No./BiIling Reference bt TO BE FILLED IN BY CLIENT/SAMpLING PERSONNELRequestedDueDate01Day02Days Days iiays IDays Certiticatjon NELAC USACE FL_____Working Days 06-9 Days Standard 10 days WokMduat Be
SCSamplesreceivedafter1500willbeprocessednextbuIj-ie day _________Turnaround tIme Is based on busIness days exdudln i4hends and holIdays Water Chlorlnatadt YES NOSEEHEVERSEFOflTMscoNomoNsnàjlcEsRENDERaDByPEUSMLABORATOInssiic.ro ciiia1jj r________amp1e iceu ..pon .OiieCuofl
ANALYSES REQUESXEDvy PRISM/6 //LAB___Ac \/ID NO
liME MATRIX SAMPLE CONTAINERCUENTDATECOLLECTEDSOIL PHESEnvAiJSAMPLEDESCRIP11ONCOLLECTEDMIUTARYWATER OR TYPE TIVES REMARHOURSSLUDGESEEBELOWNOSIZEi-c DL/X4 IV___
-3 __________
___________/3-f ec
Samplers Signature Sampled By Print Name ________________LAffiljajUponrelinquishing1thihemofCustodyIsyourauthorizationforPrismtoproceedwith the analyses as requestàdiv Any changes must besubmittedInwriting to the Prism Project Manager There will be charges for any changes after analyses have beójflæjjallzaiRelnqulsheSignatureRacelvsd5ySignature
Dale MllllaryMours Additional CommentsRelinquishedMySignatureReivadBySignatureDale
Relinquishe Signatur ForP Labreatodes
is
at odo pment acoo we TAP ST DY EALSE PORTA11ON OThELAAOPATORY1 GrouSAMPLES ARE NOT ACCEPTED AND VEfiiFIE1 AOAINST coc UNTiL RECEIVED ATThE LAMoinAToRy
FadEx OUPS fld-dIIvared Dpmaeiciservlce EIOlherJPDESUSGROUNDWATERDRINKING WATER SOLID WASTE RCRA CEc2jt LANDFILL rrriueNflrn-sir r-or ii ur r-
CLIENT sP
A1TN ce rd
PRISM Coc GROUP
Please fill in the Site Location lnformaflon on the attached VPH and/or EPI-Forms
WaSO1\FOW%MMONORMS\EPH Site Location for CIIent4oc
Fuff 5ervt Analyfrcai nv nmnta SoJIflln
VPH AllphaticslAromatjcs Laboratory ReportIng Form
Client Name ESP Associates PA Laboratory Name Prism Laboratories1 IncProjectNameMoreheadCommonsNo.4 NC Certification Lab 402SiteLocation______________________________Sample Matrix Soil
Sample Information and Analytical ResultsMethodforRangesMADEPVPI-l
late Rec
Surrogate Rec..-
Option Established tIII line on vial
Option Sampling device Indicate brand1 e.g EnCore TMOptionFIeldweightofsoil
Unadjusted value should exclude the concentration of any surrogates Internal standards anchorconcentrationsofotherrangesthatelutewithinthespecifiedrangeAdjusted value
MDL Method Detection Limit RL Reporting Limit Blank Laboratory Method Blank or Trip Blank
whichever Is higher IndIcate typeWereallperformance/acceptance standards for required QA/QC
procedures achieved YES
Yes DetasAUached
Were any sIgnlflcan modifications to the VPH method made
Pagelofl VPH SOIl
EPH AIlphatJcsJAromatIcs Laboratory Reporting Form
MDL Method Detection Limit RL Reporting Limit
Laboratory Name
NC Certification Lab
_Sample Matrix
Were all performance/acceptance standards for required QNQCproceduresachieved EIYES 1NQ Details AttachedWasblankcorrectionappliedasslgnif1canmodificationofthemethodYesNOWereanysignificamodificationstotheEPHmethodmadeNOJYesDetailsAttachedComments
Client Name
Project Name
Site Location
ESP Associates PA
Morehead Commons No
Method for Ranges MADEP EPH
Surrr-
Sample information and Malvticai Results
Prism Laboratories Inc
402
Soil
ro-octadecana Aromatic o-Terphenyi
Received
Date Extracted
Date Analyzed
%Dry Solids ii
Pitlon Factor __j
rnSjn mg/kg II
-Fluorobiphen
184953 184954 184955 184956
6/19/2007 6/19/2007 6119/2007 6/19/2007
6/19/2007 6/19/2007 6/19/2007 6/19/2007
6/21/2007 6/21/2007 6/21/2007 6/21/2007
Cli
Blank
83.3
6/24/2007
74.3
6/24/2007
82.4
6/24/2007
JempIe ResultsL12
84.9
6/24/2007
Sample Resulls
13
13
RL
81.3
Sample Results SamDJe Results Samfe Results
________11
12 11
MDL
12
12
ii 13
10
10
10L12
L3.a
13 130
10 1010101010
13 12
13 12
13 12
4.2
_______
11
jo
10
10
11
11
11
12
10
10
10
12
12
12
LF
92
83
40-14 40-140%
114 90
116 91
Unadjusted value should exclude the concentration of any surrogates internal standards and/orconcentrationsofotherrangesthatelutewithinthespecifiedrangeAdjusted value
Blank Laboratory Method Blank
Pagelofi EPH Soil
EtU JUL
Case Narrativei.PRISMjjjLABORATORIESINC
Date 07/16/07 ClIent Project ID Morehead Commons NoCompanyESPAssociatesPAPrismCOCGroupNoG0707086ContactChrisWard
Collection Dates 07/05/07AddressBox7030LabSubmittalDates07/05107
Charlotte NC 28241
This data package contains the analytical results for the project identified above and includes Case Narrative Laboratory Report and QualityControlDatatotalingpageschain-of-custody is also attached for the samples submitted to Prism for this project
Data qualifiers are flagged Individually on each sample key reference for the data qualifiers appears at the end of this case narrative Qualityconlrolstatementsand/or sample specific remarks are included in the sample comments section of the laboratory report for each sampleaffected
.SornJ Volatile Anay
No Anomalies Reported
Yienal ala
NJAMAnaAnal sis
N/A
Wet Lab and Micro Ana1ls
N/A
Please call If you have any questions relating to this analytical report
Jones
Review Date
Data Qualifiers Key Reference
Compound also detected In the method blank
Result outside of the QC limitsDOCompounddilutedout
Estimated concentration calibration range exceededTheanalytewaspositively Identified but the value Is estimated below the reporting limitEstimatedconcentrationwithhigh bias
Estimated concentration with tow bias
matrix effect Is present
Notes This report should not be reproduced except in its entirety without the writilen consent of Prism Laboratories Inc The results in this
report relate only to the samples submitted for analysis
44 SpæbROd p.0 Box 240543 ChaVIOItSNC 28224.0403Phone704/529-6354 Toll Free 800529.6364 Fax 704/525.0409
Project ID Moreheari Commons No Client Sample ID WS-3
Prism Sample ID 186279SampleMatrixSoilCOOGroupG0707086
Time Collected 07/05/07 1430
Time SubmItted 07/05/07 1520
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
rntSolids Determination
percent Solids 92.0 SM2540 07/10/07 1300 athao
ml-volaUie Orgarliccompa5 by GO/MS
24-Trlchiorobenzene BRL mg/kg 0.35 0.035 82700 07/13/07 kcamptgotto 024946
2-Dlthiorabenzene BRL mg/kg 036 0.026 8270C 07/13107 743 kcamplgotto Q249463DIch1orabenzeneBRLmg/kg 0.36 0.026 52700 07/13/07 743 kcampigotto 024946
4-Dlchtorcbenzene BRL mg/kg 0.35 0.032 82700 07/13/07 743 kcamplgotto Q24945
45-Trichiorophenci BRL mg/kg 0.36 0.036 82700 07/13/07 743 kcamplgotlo 024946
4.6-Trichiorophenol BRL mg/kg 0.36 0.034 8270C 07/13/07 743 kcamplgono 0249464-Dichiorophenol BRL mg/kg 0.35 0.030 82700 07/13/07 743 kcampIgofl 024946
4-Dlmethyiphenol BRL mg/kg 0.35 0.034 62700 07/13/07 743 kcarnplgotto 024946
BJL mg/jcg 0040 82-.0713/o7_743 kcamgotto -024946..4-Dinltrotojuene BRL mg/kg 0.36 0.020 82700 07/13/07 743 kcampigotto 024946
BRL mg/kg 0.36 0.038 82700
BRL mg/kg 0.36 0.037 82700
BRL mg/kg 0.36 0.028 82700
BRL mg/kg 0.36 0.028 82700
BRL mg/kg 0.36 0.033 82700
BRL mg/kg 0.36 0.043 82700
BRL mg/kg 0.36 0.036 82700
BRL mg/kg 0.71 0.022 82700
BRL mg/kg 1.8 0.022 82700
BRL mg/kg 0.36 0.034 52700
BRL mg/kg 0.71 0.026 82700
BRL mg/kg 0.36 0.046 82700
ERL mg/kg 0.36 0.022 82700
BRL mg/kg 1.8 0.024 82700
This report should not be reproducecj except In Its entirety without the written consent of Prism Laboratories Inc449SprIngbrooRoadP.O Box 240543 Charlotte NC 28224.0543Phone704/529.6364 Toti Free Number 1-800/529364 Fax 704/525-9409
NC Certification No 402
SC Certification No 99012
_J NC Drinking Water Cert No 37735
IfOItmofltj SoIutJn5
ESP Associates PA
th Chris Ward.0 Box 7030
hariotte NC 28241
Laboratory Report
07/13/07
Limit Factor Date/Time ID
B-Dlnhttotojuene
Chioronaphthajene
Chiorophenol
ethyinaphthaj
Aethy1phenoi
fltrophenoi
4-Methyiphenol
I-DlchlorobendJne
.DIflltro_2..methyIphenoi
Iromophenylphenyl$lher
thloro.3.metiiylphenoi
hloroanlllne
thlorophenyiphenyjether
ItJphenoI
07/13/07 743
07/13/07 743
07/13107 743
07/13/07 743
07/13107 743
07/13/01 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
kcamplgotta
kcamplgotto
kcarnpigctto
kcamplgouo
kcarnplgatjo
kcamplgotto
kcamplgotto
kcampIotto
kcampgoo
kcampigotio
kcamplgo
kcamplgotti
kcampigat
Iccampigoib
024945
024945
024946
024946
024945
024546
024946
024946
024946
024946
024945
024946
Q24945
024945
Page lot
SC CertMcaUon No 99012 Laboratory ReportNCDrinkingWaterCei-t No 37735 07/13107
ESP Associates PA Project ID Morehead Commons No Client Sample ID WS-3ttnChrisWard
PrIsm Sample ID 186279Box 7030 Sample Matrix Soil COG Group G0707086har1otteNC28241TimeCollected07/05/07 1430
Time Submitted 07/05/07 1520
arameter Result Units Report MDL Dilution Method Analyss Analyst Batch
It Factor Daternme ID
icenaphihylene BRL mg/kg 0.36 0.035 82700 07/13/07 743 kcamplgoua 024946
nthracene RL mg/kg 0.35 0.027 827CC 07/13/07 743 kcamplgotto 024946zobenzaneBRLmg/hg 1.8 O.o33 82700 07/1307 743 kcampigotto 024946enzoaanthranaBRLmg/kg 0.35 0.050 827CC 07/13/07 743 kcamplgotlo 024946enzoapyreneBRLmg/kg 0.36 0.041 827CC 07/13/07 743 kcamplgouo 024945enzobfluoranUeBRLmg/kg 0.36 0.016 827CC 07/13/07 743 kcamplgotto 024946enzoghiperyleneBRLmg/kg 0.36 0.017 82700 07/13/07 743 kcamptgotta 024946enzokfluorantheneBRLmg/kg 0.36 0.029 827CC 07/13/07 743 kcampigoo 024946anzolc acid BRL mg/kg 1.8 0.15 827CC 07/13/07 743 kcamplgotto 024945nzylalcoholBRLmg/kg 0.71 0.038 82700 07/13/07 743 kcamptgoo Q24946it
mg/kg
s2-chlorolsopropyieth BRL mg/kg 0.36 0.030 82700 07/13/07 743 kcamplgotto Q24945S2-athylhexylphlhalate BRL mg/kg 0.36 0.018 827CC 07/13/07 743 kcamplgotto 024946tyIbenzylphUaIateBRLmg/kg 0.35 0.022 82700 07/13/07 743 kcampigoo 024945ryseneBRLmg/kg 0.36 0.059 82706 07/13/07 743 kcamplgotto Q24946il-butyjphthalate BRL mg/hg 0.36 0.016 82700 07/13/07 743 kcamplgotto 024946fl-octylptitha late BRL mg/kg 0.36 0.027 82700 07/13/07 743 kcamplgouo Q24946enzoahanthraceneBRLmg/kg 0.36 0.036 827CC 07/13/01 743 kcamplgoflc 024946enzofuranBRLmg/kg 0.36 0.031 827CC 07/13/07 743 kcamplgotto Q24946thyiphthaIaBRLmg/kg 0.35 0.022 827CC 07113/07 743 kcampgouo 024945nethyIphhalatsBRLmg/kg 0.35 0.024 827CC 07/13/07 743 kcampI9ouo 024945oranthene0.13.1 mg/kg 0.36 0.025 827CC 07/13/07 743 kcamplgotb 024946oreneBRLmg/kg 0.36 0.021 827CC 07/13/07 743 kcampfgono 024945kachlorobenzeneBRLmg/kg 0.35 0.018 827CC 07/13/07 743 kcampjgotto 024945cachlorobuthdleneBRLmg/kg 0.36 0.035 827CC 07/13/07 743 kcamplgotio 024946
This repo-hold not be reproduced except In its entirety without the written consent of Prism Laboratories Inc449SprJngbrooRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525.0409
iii An --nnnmunld SoIUUnt
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ESP Associates PA
Utn Chris Ward
.0 Box 7030
liarIotte NC 28241
Project ID MorehØad Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil CCC Group
Time Collected
Time Submitted
ws-3
186279
G0707086
07/05/07 1430
07/05/07 1520
This report should not be reproduej except In Its entirety without the Written consent of Prism Laboratories Inc449SprlngbraokRoadP.O Box 240543 Charlotte NC 28224-0M3Phone7O41529..6364 Toll Free Number 1-8001529-6364 Fax 704/525-0409
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
07/13/07
Result Units Report MDL Dilution Methodarameter
exaehlorocyclopentsdlene BRL
exachioroethane BRL
deno1 2.3-cdpyrene BRI.
ophorone BRL
-Nltmsodl.n.propylamine BRL
-Nltrosodiphenylamjne BRJ
phthalene BRL
trobenzene BRL
3ntachlorophenol BRL
lenanthrene BRL
enol BRL
Limit
0.36
0.35
0.36
0.35
0.38
0.36
0.36
0.35
1.8
036
0.35
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
0.038
0.036
0.037
0.032
0.040
0.018
0.039
0.035
0.030
0.017
0.039
Factor
827CC
827CC
827CC
827CC
827CC
8270C
827CC
827CC
527CC
827CC
827CC
Analysis
Date/Time
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
Analyst Batch
ID
kcaniprgottp 024946
kramplgotto Q24946
kcamplouo 024946
kcampgotto 024946
kcarnpgotto 024946
kcamplgotto 024946
kcarnplgotto 024946
kcamplgoo 024946
kcamplgottp 024946
kcampIotto 024946
kcampIofto 024946reeO.17.J mg/kg 0.6 827C 0711.3/07 743 mgpU 024946
Sample Preparation 30.16g mL 3550B 07/11/07 500 dpop P18565
Surrogate Recovery Control Limits
Terphenyl-cJJ4 104 41-135
Phenol-c15 64 13-95
Nltrobenzene..dS 69 14-103
2-Ftuorophenol 61 14-89
2-Fluoroblphenyl 69 21 108
24.6-Tribmmophenot 94 25-123
ir.tibIe Pefroleum HVdrocarbons by Gç-FID1-C22Amma5 BRL mg/kgAnalysisNoteforC11-c22 Aromatics
-C36 Allphatlcs BRL mg/kg
Cia Atiphailca BRL mg/kg
11 5.8
Adjusted value
11 1.6
11 3.5
MADEP EPH 07/12/07 744 wappacclolj
MADEP EPH 07/12/07 744 9PPaCctoIi
MADEP EPIHI 07/12/07 744 grappacckil
024910
024910
024910
Page of
ESP Associates PA
Attn Chris Ward
Box 7030
charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil coc Group
Time Collected
Time Submitted
WS-3
166279
G0707086
07/05/07 1430
07/05107 1520
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Sample Preparation 1O.OBg mL
RL Below Reporting Limit
Estimated value between the Reporting Limit and the MDLferesultsInThisreportrelateonlytothesamplessubmitted Ibr analysis and meet state certilicatfon requirements other than
EL.4C certification except for those aslances Indicated In the case narrative and/or test comments
This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SpJingbrojçRoadP.O Box 240543-Charlotte1 NC 28224-0543Phone7041529-8364 Toll Free Number 1-800/529.6364 Fax 1041525-0409
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Laboratory Report
07/13/07
EPFI 07/09/07 1100 dpape P18855
Surrogate Recovery Control Limits
o-Terphenyl 84 40-140
2-Fluorobiphenyl 64 40-140
2-Bromonaphthalene 61 40 140
l-ChIoro.actadecane 71 40 140
igela Overcash V.P Laboratory Services
Page of
NC Certificat ion No 402
SC CertJfIcatn No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
tt ePetroleum Hydrocarbons by Gc-FID method MADEP EPH
OCeatchRaauIIRIConoIUrnitUnitatO
C11-C22Aroma5 ND 10 mg/kg 024910Cl9-C36 Aliphatics ND 10 mg/kg 024910
RaauU SkBoUnt
C11-C22Aroj 128.22 170 mg/kg 75 40-140 024910Cl9-C36Aflpha 41.94 80 mg/kg 52 40-140 02491031.9 60 mg/kg 40-140 024910_1 Rasult anaa
186445 Cl 1-C22 Aromaffcs 137.74 170 mg/kg ai 40-140 024910C19-C35 AJiphlIcs 44.08 80 mg/kg 55 40-140 024910
Remvay
C19..C3BftJjphaflcs 52.7 mg/kg 66 40-140 18 0-50 024910C9-C18 AHphallcs 37.12 60 mg/kg 52 40-140 15 0-50 024910
This report should not be reproduced except in its entirety without the written consent of Prism Laboratort Inc
449 SprIngbr Road P.O Box 240543 Charlotte NC 28224-0543Phone7041529..634 Toll Frea Numbej l-899/5295354 Fax 7U4I525-O4
Level II QC Report
7116/2007
Project ID Morehead Commons No COG Group Number G0707086
Date/Time Submitted 7/5/2007 1520
Page lof
NC CerUlicatlon No 402 Level II QC ReportScCertificationNo99012
7/16/2007NCDrinkingWaterCertNo37735
ESP Associates PA
Project ID Morehead Commons No COC Group Number G0707086AttnChrisWard
Date/Time Submitted 7/5/2007 1520Box7030
Charlotte NC 28241
Semi-volatile Organic Comeounds by GCIMS method 8270C
oc eaicii_______________Rasult RI Contmj Unit Unks ID
I24-Trichlorobenzene ND 0.33 0.165 mg/kg Q24946l2-Dlchlorebenzone ND 0.33 0.165 mg/kg Q24948l3-Dlchlorobenzene ND 0.33 o.is mg/kg Q24946l4-Dlchlorobenzene ND 0.33 0.165 mg/kg Q24946
24S-Tlichlorophenol ND 0.33 0.165 mg/kg Q24946Ni0.33 0.165 mg/kg 02494624-DlcIIlorophenol ND 0.33 0.165 mg/kg 02494624-Dknethyjphenol ND 0.33 0.165 mg/kg Q2494624-DInhtrnphenol ND 1.65 0.825 mg/kg Q2494624-Dlr/krotoluene ND 0.33 0.165 mg/kg 02494626-Dlnltrothluene ND 0.33 0.165 mg/kg 0249452-Chloronaphthaiene ND 0.33 0.165 mg/kg Q249462-Chiorophenul ND 0.33 0.165 mg/kg 0249452-Methylnaphthajene ND 0.33 0.165 mg/kg Q249462-Methyiphenol ND 033 165 mg/kg Q24946
34-Methylphancl ND 0.33 0.165 mg/kg Q2494633-DfChIojTjbenzIdIne ND 0.66 0.33 mg/kg 0249484eUDlnibo2methylptjenolND1.65 0.825 mg/kg 0249464-Bromophenyiphefl8 ND 0.33 0.165 mg/kg 0249464.Chloro..3methylphenol ND 0.66 0.33 mg/kg 0249464-Chloroaniljne NI 0.33 0.165 mg/kg 0249454-ChlorophenyJphenyj Nt 0.33 0.165 mg/kg Q249454-Nitmphol ND 1.65 0.825 mg/kg Q24945AcenaphiheneND0.33 0.165 mg/kg 024945AcenaphtliyleneND0.33 0.165 mg/kg 024946AnthraceneMD0.33 0.165 mg/kg 024946AzobenzeneND1.65 0.825 mg/kg Q24946RenzoaanthreceneMD0.33 0.165 mg/kg
024946BenzoapyreneND0.33 0.165 mg/kg
Q24946BenzobfiuoranthoND0.33 0.165 mg/kg
024946ND0.33 0.165 mg/kg Q24946BeflZokfiuorantheneND0.33 0.165 mg/kg 024946BenzobacidND1.55 0.825 mg/kg 024946
This report should not be reproduced except In Its entirety without the wdtten consent of Prism Laboratories Inc449SprJngjRoadP.O Box 240543 Charlotte NC 28224-0543Phone7O4I5y.94 Toll Free Number 1-800J529.3g Fax 7041525-0409 Page of
NC Certificallon No 402 Level II QC ReportSCCerfificatlorNo98012
7/16/2007NCDrinkingWaterCarLNo37735
ESP Associates PA
Project ID Morehead Commons No COC GroUp Number G0707086AttnChrisWard
Datemme Submitted 7/5/2007 1520Box 7030
CharIotte NC 28241
QCBaIchResuIIConUIUnI
Benzyl alcohol ND 0.66 0.33 mg/kg 024946BIs2-chloroothoxymethane ND 0.33 0.165 mg/kg 024946Bls2-chIoroethyJether ND 0.33 0.165 mg/kg 024946Bls2-chloroIsoppylether ND 0.33 0.165 mg/hg 024946ND0.33 0.165 mg/kg 024946Butytbenzylphthaf ate ND 0.33 0.165 mg/kg 0.24946ChryseneND0.33 0.165 mg/kg Q24946Dl-n-butylphthate ND 0.33 0.165 mg/kg 024946Dl-n-octylphthate Nt 0.33 0.165 mg/kg 0.24946DlbenzoahaflthceneND0.33 0.165 mg/kg 024946DlbenzafuranND0.33 0.165 mg/kg 024946DlethyjphthalateND0.33 0.165 mg/kg 024946DlmathylphthalateND0.33 0.165 mg/kg
0.24946FluorantheneND0.33 0.195 mg/hg 024945I9uoreneND0.33 0.165 mg/kg
0.24946HexachlorobenzeneND0.33 0.165 mg/hg 024946iecathlörobutadIeneND_0 Q165mg/kg_--.------.-Q2494
Hexachioroethane ND 0.33 0.165 mg/kg Q24948Indeno12JpymneND0.33 0.165 mg/hg 024946IsophoroneND0330.165 mg/kg 024946N-NitrosocJfn.propyjamtne ND 0.33 0.165 mg/kg 024946NNJtrosadlphenylamIneND0.33 0.165 mg/kg
024946NaphttiatenaND0.33 0.165 mg/kg 024946NllrobenzeneND0.33 o.iss mg/kg
024946PentachlorophenolNI1.65 0.825 mg/kg
0.24946PhenanthreneND0.33 O.j mg/kg
0.24946PhenolND0.33 0.165 mg/hg
024945
mg/kg 024946
l4Dlchlombeene 1.22999 1.6742 mg/kg 73 02494624-Dlnhtroblueno 1.51198 1.6142 mg/hg 55-128 0249462-Chtorophenol 1.41144 1.6742 mg/kg 84 37-98 0249464-Chbro..3-methylphenol 1.40709 1.6742 mg/kg 84 45.111 024945ThjsreportshouldnotbereproducedexceptInItsentiretywithout the written consent of PrIsm Laboratorf Inc
449 Sprlngbrooj Road P.O Box 240543 Charlotte1 NC 28224.05Phon704/5294394 Toll Free Number i-8001529494 Fax 7041525-0409 Page of
NCCerttficationNo.402 Level II QC ReportSCCertificationNo99012
7/16/2007NCDrinkingWaterCartNo37735
ESP Associates PA
Project ID Morehead Commons No COC Group Number G0707085AttnChrisWardDatemmeSubmitted715/2007 1520Box7030
Charlofte NC 28241
cc SaldiRangosRssult$pkD Amount UnI fO
4-Nltrophenol 0.97991 1.6742 mg/kg 59 20-157 Q24946Acenaphthene1290921.5742 mg/kg 77 44-110 Q24945
N-NIfrosodi.n.propylamjne 1.38935 1.6742 mg/kg 83 36-101 024946Pentachlorophenol1.94174 1.6742 mg/kg 116 53-127 Q24946Phenol1.26146 1.6742 mg/kg 75 34-102 024946
154837 1.6742
RangusReaukSplkaAmnuntUnila
188433 l24-Trlchjortjbenzene 1.23412 1.6537 mg/kg 75 26-97 024946l4-Dichforobenzene 1.13723 1.6537 mg/kg 69 23-92 Q2494624-IInftrotoluene 1.65211 1.6537 mg/kg ioo 45-127 0249462-Chiorophenoi 1.14351 1.6537 mg/kg 69 25-94 Q249464-CNoro3.methyphenoJ 1.25562 1.6537 mg/kg 76 31-113 Q249464-Nltrophenot 0.96197 1.6537 mg/kg 58 17-150 Q24945Acenaphthene1.28406 1.5537 mg/kg 78 36-107 024946N-NItrosodj.npropy1anilne 125661 1.6537 mg/kg 76 22-105 024945Retachlorophenol1880956537-mg/kg-114 39137 --024946__________________
024946
--
Rangue RPD Range
SmnpID
--
RanuIt Spike Amount tinfls
ID188433l24-Trlchlorobenzene 1.37073 1.6748 mg/kg 82 26-97 10 0-37 Q24946l4-Dtohlorobenzene 1.1 1520 1.6748 mg/kg 67 23-92 0.36 02494624-Dinltrotofuene 1.36537 1.6748 mg/kg 82 45-127 19 0-29 0249462-Chlcrophenol 1.20194 1.6748 mg/kg 72 25-94 0-37 0249464-Gl1forQ.3.methyjphenol 1.43402 16748 mg/kg 85 31-113 13 0-32 0249464-Nitrophenol 0.81212 1.6748 mg/kg 48 17-150 17 0-32 024945Acenaphthee1.15472 1.6748 mg/kg 69 36-107 11 0-32 024945N-Nt coodI-n-propym me 1.1 8687 1.6748 mg/kg 71 22-105 0-37 024945Pentachlorophenol1.84192 1.6748 mg/kg iIO 39-137 0-27 Q24945Phenol1.14902 1.6748 mg/kg 69 23-97 0-42 024946Pyreno1.47957 1.6748 mg/kg as 45-133 0-27 024945-Soe Case Narrative
This report should not be reproduceJ except In Its entirety without the written consent of Prism Labomtojj inc449SprfngbrojçRoadP.O Box 240543 Charlotte NC 28224.5543Phone7041529-6354 Tori Free Number 1-8001529.6364 Fax 7041525-04Q9 Page of
RlESIC
Full Service Analytical Envlwnmenfaj SIutjon
449 Springbroolc Road P.O Box 240543 Charlotta l3C 2824-D543Phone704/529-6384 Fax 704/
Client Company Name _______________________
Report To/Contact Name LIJt2
Reporting Address ic
Phone Fax Yes No____________
Email Yes No Email AddressEDDTypePDF.._el Oths
Site Location Name
Site Location Physical Address
r.ptsufzQUo7rmLuNo
Short Hold Analysis jYes No UST Project Yes NopleaseATTACHanyjtspecificreportingQCLEVEL111111IVprovisionsand/or Qnent
Involod To ji
Address__
Li
Dat4c1-L ic
IflUflXp NO
Purchase Order No./4Referej
Requested Due Date 1J çIQ Days 03 Days 04 Days Days
WorkIng Days 6liao Standard 10 days
Samples received after 15ddlI.bo processed next business dayTurnaroundtimeIsbasedojbtisinessdaysexcludingweekendsand holidaysSEE REVERSE FOR TEIM CoNDmoNs REISARDING SERVICESRENDERED DY PRISM I1AB ORATORIES INC TO CUENT
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC_USACE_FL____NCSC_OThER _____N/A_____
Water Chlorinated YES_NO
Sample Iced Upon Collection YES
CLIENT DATE
jMPLE
DESCRIPTIoN coEcD
TIME
COLLECTED
kOURS
MATRIX
SOIL
SLUDGE
NALYSES REQUESTED
FRESERVA /4lIVES /7 REMARKS
PRISM
LAB
ID No
ws
SAMPLE CONTAIIL7
SEE BELOW NO
471
csIZE
amplers Signature Ø-.1--i Sampled flJlByPrintNameAffiiatIonUponrelinquishingthisCJaIofCustol5yourauthorizationforPrismtoproceedwithjàlsesas requested above Any changes must besubmittedinwritingtothePrismProjectManagerTherewillbechargesforanychanqasfteranaIyseshave been Initialized
jP
Retinquizhsd 5y Signafura Received 8y Signalure Dale Mfiflay/hours
Relinquithad 8y Stgceturn Receiypd 5y Signature Dale111___ ___________
cy slgnalU _______ ___________________________
jRiiid of Wptnani ULD es TAPED SHUT usoy sa Nsjók.j1oiio The LABORATORYSAMPL.E5 ARC NOTACCEp AND VERIRED AGAINST COO UN1II RECEIVED AT THE LABQIATpnYOFadExlfjpInd.del1vemd DPrfsniFSNPDESUTGROUNDWATER DRINKING WATER SOLID WASTEflRCRA CERCL4 LANDFILL OTHERONCQSCNCOSCONC0-SC UNC QSC ONC 0SC .QNO OSC ONC 050 ONC 050 aND OSOa________TVPF flJf Anher laq Pttfrr TI TcftnnIrurf Cn Vfl Vritlf itrnnie Aruh 7rn I4rt nera
Additional Comments
.-1-lL --
SEE REVEIISE FORTERMSCONDITUN5
ORIGINAL
CliENT E5P rn
ANN
PRISM Coc GROUP
Please fiR In the Site Lócat tori tnhormation on the affathed VPH nd/orEpH Forms
EPH Site Location for CIlefltdo
FUU Svfc MaIyirca Envfmnmenl4 SoJu1ion
EPH Aliphatics/Aromatics Laboratory Reporting Form
Client Name
Project Name
Site Location
Method for Ranges MADEP EPH
EPH Surrogate Standards Aliphatic 1-Chioro-
Sample Identification
Date Collected
Date Received
Date Extracted
Date Analyzed
Dry Solids
Dilution Factor
Hydrocarbon Ranges in mg/kg
C9-C1 Aliphatics
Cl9-C36 Atiphatics
Cl1C22Aornatlca
Blank C9-C18 Aliphatics
_C19-C35 Aliphatlcf_J
_______Cl 1-C22 AromaticsRLC9-C18 Aliphatlcsti
Cl 9-C36 Aliphatics
________romatlcs
402
Soil
MDL Method Detection Limit RL Reporting Limit
ESP Associates PA Laboratory Name
Morehead Commons No.4 NC Certification Lab
Sample Matrix
Samnie Information and Analytical Results
EPH Fractionation Surrogates -2
Prism Laboratories Inc
c-o-Terohenvl
Iphenyl
.1
7/9/2007
7/12/2007
92.0
Sample Results
11
11
11
10
10
10
11-11-
Sample Results Sample Results Sample Results Sample Results
MDL
Ill
10 10 10 101010101010101010
11
3.5
Unadjusted value should exclude the concentration of any surrogates internal standards and/orconcentrations of other ranges that elute within the specified rangeAdjusted value
Blank Laboratory Method Blank
Were all performance/aeptance standards for required QA/QCproceduresachieved
IN0 Details AttachedWasblankcorreclionappliedassignificantmodificationofthemethodYesNCWereanysignificantmodificationstotheEPHmethodmadeNODetailsAttachedComments
Page of EPI-I Soil
RECD JUL
Case NarrativePRISM
IJgDRATCRIESINC
Date 06/29107 Client Project ID Morehead Commons No
Company ESP Associates PA Prism COC Group No 60607586
Contact Chris Ward Collection Dates 06/20/07AddressBox 7030 Lab Submittal Dates 06/20/07
Charlotte NC 28241
This data package contains the analytical results far the project Identilled above and includes Case Narrative Laboratory Report
and QualitycontrolDatatotalingpageschain-of-custody is also attached for the samples submitted to Prism lbr this project
Data quafifiers are flagged individually on each sample key reference for the data qualifiers appears at the end of this case narrative Quatityantrolstatementsand/or sample specific remarks are included in the sample comments section of the laboratory report tbr each sampleaffected
3emi Volatile Analysis
No Anomaties Reported
/olatile Analysis
No Anomalies Reported
dletals Analysis
N/A
IVet Lab and Micro Analysis
N/A
lease call if you have any questions relating to this analytical repDrL /9ateReviewedbybbiJonesProjectManagerneia.YOvercash
SIgnature Signature ______________________eview Date 06/29/07 Approval Date _P/29/07
ata Qualifiers Key Reference
Compound also detected In the method blank
Result outside of the QC limits
DO Compound diluted out
Estimated concentration calibration range exceeded
The analyte was positively identified but the value Is estimated below the reporting limit
Estimated concentration with high bias
Estimated concentration with low bias
matrix effect Is present
Notes This report should not be reproduced except in its entirety without the wriliten consent of Prism Laboratories Inc The results in thisreportrelateonlytothesamplessubmittedforanalysis
449 Sprlngbrook Road P.O Dox 240543 Charlotte NC 28224-0403
Phone 704/529-6354 ioU Iree 800529-ssa4 Fa 7I14I57çJdflq
NC Certification No 402
SC Certification No 99012
NC l3rinklng Water Cart No 37735
rcent SoI4
rcent Solids
latlIe Organic Compounds by GC/MS
-nzene
iylbenzene
p-Xylenes
ylene
lueno
Surrogate Recovery Control L1mit
Brornofluorobenzene 106 77-128
Dlbromofluommefhane 93 67-143
Totuene-dU 93 81 128
Q24575
25.18 mL 3545 06/25/07 1515 Wconder P18738
Surrogate Recovery Control Limits
o-Terphenyl 64 46-124
Surrogate Recovery Control Limits
aaa-TFT 84 55-129
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SprtngbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 TII Fmp Numbpr nAI ArA Pv 1flAIcnnAA
3P Associates PA
tn Chris Ward
Box 7030
iarlotte NC 28241
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil coc Group
Time Collected
Time Submitted
IA-123
185079
00607588
06/20/07 1000
06/20/07 1635
rameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Dateflhme ID
83.8 SM2540 0612707 1800
Lthao
BRL pg/hg 3.7 0.50 826DB 06/27/07 909 emssell Q24552
ORL pg/kg 6.2 0.43 826DB 06/2707 909 enrnsell Q24552
BRL pg/kg 12 0.87 826DB 06/27/07 909 erussell Q24552
BRL pg/kg 6.2 0.37 826DB 06/27/07 909 erussell Q24552
BRL pg/kg 6.2 0.42 826DB 06/27/07 909 erussell Q24552
rsei Range Organics DRO by GC-FlD
seI Range Organics DRO
Sample Preparation
saline Range Organics GRO by GC-FID
soiine Range Organlcs GRO BRL
400 mg/kg 42 5.3 8015B 06/27/07 1505 jvogel
mg/kg 12 0.078 8015B 06/27/07 543 tiwagner Q24580
Pon nf
NC CertificatIon No.402
Sc Certification No 99012
NC Drinking Water Cert No 37735
irameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
mple Comments
IL Below Reporting Limit
Estimated value belween the Reporting limit and the MDL
results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanELACcertificationexceptforthose instances indicated In the case narrative and/or test comments
results are reported on diy-weight basis
igela Overcash V.P Laboratory Services
This report should not be reproduced except In its entirety without the written consent of Prism Laboratorjes Inc449SpringbrokRoad P.O Box 240543 Charlotte NC 28224-0543
Associates PA
tn ChrisWarci
Box 7030
arlotte NC 28241
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil Coc Group
Time Collected
Time Submitted
IAi 23
185079
G0507588
06/20/07 1000
06120107 1635
Phnng 7fldLçQ..Rj Thu Nrnhr Fy 7fliUc..nAne Paoe of
Associates PA
Chris Ward
Box 7030
arlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil coc Group
Time Collected
Time Submitted
B-234
185080
G0607588
06/20/07 1015
06/20/07 1535
rcent Solids 85.6 SM2540 06/27/07 1800 Llhao
tattle Organic Compounds by CC/MS
nzene BRL pg/kg
ylbenzene
-Xyienes BRL pg/kg
ylene
uene BRL pg/kg
sel Range Organics DRO by OC-FID
eel Range Organics DRO
ampIe Preparation
Surrogate Recovery Control Limits
Bromofluorobenene 105 77-128
Dibromofluoromethane 97 67-143
Toluene-dB 96 81 128
76 mg/kg 8.2 1.0 80153 06/28/07 808 Jvogel
25.36 mL 3545
024575
06/25/07 1515 wconder P18738
sotine Range Organics CR01 by GC-RD
soline Range Orgardos GRO BRL mg/kg .2 0.074
Surrogate Recovery Control Limits
o-Terphenyl 99 49-124
8015B 06/27/07 615 hwagner 024580
Surrogate Recovery Control Limits
aaa-119 83 55-129
This report should not be reproduced except In its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad-P.O Box 240543 Charlotte NC 28224-g54.3
Laboratory Report
06/29/07
.rameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
rcent Solids Determination
3.6 0.48 825DB 06/27/97 940 erusset 024552
BRL pg/kg 6.0 0.42 .82603 06/27/07 940 erusselt 024552
12 0.84 82503 06/27/07 940 erussefi 024552
BRL pg/kg 6.0 0.36 82603 06/27/07 940 erussell 024552
6.0 0.41 826GB 06/27/07 940 erussell 024552
PhnnB 7O4/5295 Thu Fran Numbpr i-flni cit Pv 7flefI..n.nri Panc nf
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
3rameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
mpIe Comments
Below Reporting limit
Estimated value between the Reporting Umit and the MDL
results In this report relate only to the samples submitted foranalysis and meet slate certification requirements other thanLACcertificationexceptforthose Instances Indicated in the case narrative and/or test commentsresulfsarereportedondry-weight basis
This report should not be repmduced except fri Its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Chart DUe NC 28224-0543
SP Associates PA
Itn Chris Ward
Box 7030
harlotte NC 26241
Laboratory Report
06129107
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrbc Soil COC Group
Time Collected
Time Submitted
B-234
185080
G0607588
06/20/07 1015
06/20/07 1635
gela Ovemash V.P Laboratory Services
Phone704/52963M Toll Free Number 1.800/529-6364 Fax 704/525-0409 Page 4of4
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
This report should not be reproduced except in Its entirety without the written consent of Prism Laboratories Inc449SprlnbrooçRoadP.O Box 240543 Charlotte1 NC 28224-0543Phone7041529.5364 Tell Free Number l-800I629-6364 Fax 7041525.0409
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
Level II QC Report
6/29/07
Project ID Morehead Commons No COC Group Number G0607588
Date/Time Submitted 6/20/07 1835
JnIiIn flrni hi IM 82605IULUUU
Method Blank
Rosuil RI Confroi Umit UnIts ID
Benzena ND 0.003 0.0015 mg/kg 024552
Ethylbanzene ND 0.005 0.0025 mg/kg 024552
rnp-Xylenes ND 0.01 0.005 mg/kg 024552
o-Xylene ND 0.005 0.0025 mg/kg Q24552
Toluene ND 0.005 0.0025 mg/kg 024552
Laboratory Control Sample
Recovery Recovery DC BatchRasuftSpikeAmountUnitsID
Benzene 0.04358 0.05 mg/kg 87 62-119 024552
Ethylbenzene 0.04417 0.05 mg/kg 83 57-128 024552
mp-XiIeries 0.09048 0.1 mg/kg go 54-132 024552
o-Xylene 0.04725 0.05 mg/kg 95 57-131 024552
Toluene 0.04544 0.05 mg/kg 91 57-122 024552
Matrix Spike
Recovery
Sample ID Result Spike Amount Units ID
185081 Benzene 0.03306 0.05 mg/kg 66 46-136 024552
Ethylbenzene 0.02888 0.05 mg/kg 59 51-135 024552
mp-Xylenes 0.05568 0.1 mg/kg 56 51-136 024552
o-Xylene 0.02855 0.05 mg/kg 57 49-137 024552
Toluene 0.0200 0.05 mg/kg 59 47-136 024552
Matrix Spike Duplicate
Recovery Recovery RPD
Sample ID ReSUR SJiko Amount Units ID
185081 Benzene 0.03495 0.05 mg/kg 70 40-136 0-22 024552
Ethylbenzene 0.03244 0.05 mg/kg 65 51-135 12 0-23 024552
mp-Xylenes 0.06374 0.1 mg/kg 64 51-136 13 -20 024552
o-Xyiena 0.03337 0.05 mg/hg 67 49-137 16 0-22 024552Toluene0.031 87 0.05 mg/kg 64 47-1 36 0-22 024552
Page of
ESP Associates PA
Attri Chris Ward
P.O Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ni Rnnnn ii-iflPfl by mthnd 80156
Method Blank DC Batch
Result RL Canimi Limit Units ID
Diesel Range Organics DRO ND 3.5 mg/kg 024575
Laboratory Control Sample Recovery Recovery Ll BatchRangesResultSpikeMauntUnitsID
Diesel Range Organlcs DRO 49.0 BC mg/kg 61 55-109 024575
Matrix Spike RBCOVeJY Recovery
Ranges DC Batch
Sample Result Spike Miount Units
184791 DIesel Range Organics DRO 45.8 80 mg/kg 57 50-117 024575
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPt Range DC Batch
Sample ID Result Spike Amaunt Units tO
184791 DIesel Range Organics DRO 51.9 BC mg/kg 65 50-117 12 0-24 024575
Gasoline Range Organlcs CR0 by GC-FJD method 801 SB
Method Blank
DC Batch
Result RL Control Limit Unfta ID
Gasoline Range Organlcs GRO ND 0.5 mg/kg 024580
Laboratory Control Sample itacovery Recovery
Ranges DC BatchRuultSpikenountUnitsID
Gasoline Range Organlcs CR0 1.955 mg/kg 98 64-124 024580
Matrix Spike RecoVery Recovery
Ranges DC Belch
Sample ID Result Spike Maunt Units ID
185077 GasolIne Range Organics CR0 2.016 mg/kg 101 37-128 Q24580
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range CC RetChSampleResultSpikeAmauntUnitetrID
mg/kg 93 37-126 0-34 024580185077GasolineRangeOrganicsCR01.968
-See Case Narrative
This report should not be reproduced except In Its entirety without the wdttwi consent of Prism Laboratories Inc449SpringbroolcRcadP.O Box 240543 Charlotte NC 28224-0543
Phone 7041529-6364 Toll Free Number 1.5001529-6364 Fax 7041525-0409
Level II QC Report
6/29107
Project ID Morehead Commons No COC Group Number 00607588
Date/TIme SubmItted 6/20/07 1635
Page of
Pull SorvlceMatytlcai Envhnmontal SoIuUos
449 Springbroók Road P.O Box 24543 Charlotte NC 28224-0543Phone704/529-8384 .Fax 704/
CitentCornpanyrnØ _____________________
Report To/Contact Name i.i-i-
Reporting Aidress _____________________________
Fhone Fax Yes No_____________
Email Yes NoEmai Address_____________________EDD Type PbFExcei ther
Site Location-Name
Site Location Physical Address
PAGE.....L0F...L QUOT TOE SUREP lLUNG _____________
Project Name
Short Hold Analysis Yes No UST Project Yes NopleaseATTACHanyprojectspecificreportingQCLEVEL11111IVprovisionsand/or OC Requir nts
invoice To
Address_
Purchase Order No./BlllIng Reference ________________________
Raquestacj Due Dat Day 02 Days US Days 04 Days cDaysWorkingDays06-9 Days Standard 10 days UStSamplesreceivedalter1500wIllbepruessednextbusinessdayTurnaroundtimeIsbasedonbusinessdaysexcludingweekendsandholidaysSEE REVERSE FOR TERMS CONDITiONS REGARDING SERVICESRENDERED BY PRISM LABORATOmES INC To CUENT
FIMI1 UP USTOUY RECORD
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC_USACE_1L____NC4SC_óTI-IER ______N/A_____
Water Chlorinated YES_NO_
Sample Iced Upon Collection YES NO
CLIENT
SAMPLEPESCRIPTIOPJ
/1
/43-%
DATE
COLLECTED
-2-
TIME
COLLECTED
MUTARY
HOURS
---m
JS-
pzz
MATRIX
SOIL
WATER OR
SLUDGE
SAMPLE CONTAINER
No SIZE
PRESERVA-
lIVES
ANALYSES REQUESTEDJ4
/4J l/REMARKS
I.
PRISM
IDNO
I5
TYPE
SEE ai.ow
LIb.-
-.-
$_____571_-K1ISignatre_____________________Sampled By Prlnt Nae _______________________Upon relinquIshing thisChÆla of Custody Is your authorlzion for Prism to proceed with the analyses as requested above Any changes must besubmittedin-writing to the Prism Project Manager There will be charges tar any chances after analyses have been InitializedRelbiquIsfied5yii-SJgnRca1ui
Date MBlary/Houm Additional CommentsRalInqutsJedBySI9nIUReCeIvedBySl9naturelDale
ReIInqulthdsf1atur
Meihed Shlpment -NO COa5 iIQUIJ3 BE TAPED SH OSTODY $EAi.s FOR ThANSFORTATON TO THE LASORATORY ctö mup Ne..ES ARE NOTACCEWJ-s AND VERIFIED AGAINST OC NTII RECEiVED AT THE LABORATORY
Fed Es ei us ddaiwered Jtsm Field SevjcoNPDES.f USJ GROUNDWATER DRINKING WATER SOLID WASTE RCRA CERCLA LANDFILL OTHERNCSC1JSCNCUSCNCSCNCSCNCSCNCUSCNCSC NC SCa__J0 U______ ____%FA fIU___...__--
SEE flEVERSE-FOnTERMSCONDITIONS
APPENDIX
NON-HAZARDOUS WASTE MANIFESTS
4-
NON-HAZARDOUS GeneratorsUS EPA ID No ManIfet Page
WASTE MANIFEST Document No of
Generators Name and Mailing Address Truck No iara
Generators Phone
Ft
Transporter Company Name riirpcit US EPA ID Number
Transporter Company Name US EPA Number Transporters Phone
Deslnated FaiIlty Name and Site Address 10 US EPA ID Number Facilitys Phone
CMS Landfifl 704 782-2004
5l05MorehaadRd
Concord NC 28027
11.Wasta ShIpping Name and Description 12 Containers 13.14
Total UnitNoTYPeQuantityWtIVol
Adcqtlonai Descriptions for Materials Usted Above Handling C6des for Wastes.Usted Above
15 Special Handling instructions and Additional Information
16 GENERATOR CERTIFICATION certify the materials described above on this manliest are not subject to federal regulations for reportIng prcper disposal of Hazardotis Waste
Printed/Typed Name $fl8tUre.7 17 Merilr4.4çcSs
17 Transporter Acknowledgement of ReceIpt of Materials
Printed/Typed Name .-Signature f/...2 a9 OaY
1/I/i I2
18 Transotier Acknovirpedgement of Receipt at Materials
Printed ITyped Name Signature MenTh DaY
19 DIscrepancy Indication Space
20 Facility Owner or Operator Cerlfloation of receipt of waste materials covered by thIs manifest except as noted In Item 19MSLandfill
PrlntedType Name -j MC
Ft
___________________________________________________________________________________________________________________________________
Ft _____________________________________
TJS1DIF/COpY j.4j 11
Please print er type
Form designed for use on sIte 12 pitch typewriter
ALLIED WASTEaseprlntortypeINDUSTRIESINCFOrmdesi9nedtoru5ocflt2pllthwrJ_______________NO AZA DOLJ Generatos US EPA ID
PageWASTEMANIFEST
Generators Name and Mailing Addros
KItth
Ganerator Phone
Transporter Company Name
US EPA ID Number Tmnsporte
Transporter Company Name
US EPA ID Number Transporters Phone
Designated Facilityhiame and Site Address 10 US EPA ID Number Facilitys PhoneOMSLandilU
704 782-2004
5105 Morehead Rd
Concord NC 28027
11 Waste Shipping Name and Description
12 COntainers
No Type Quantity Wi/Vol
-4ai
Additional DascripUor for Materials Listed Above
Handling Codes far Wastes Usted Above
15 Special Handling Instrucifons and Additional Information
16 GENERA CERTIFICATION certiiy the nrnterwls described above on this manifest are not subject to federal reguieti5 br reporlb proper disposal 01 Hezanjoas
Printed lTypad Name
Signature ...
MonthTransporiAcknowiedgementofReceiptofMaterjajsPrintedTypedName
Signature
Month Oey
4-
.-
.tLLr
18 Traflrj Acknowledgement of Receipt of Materials
Printed/Typed Name
Signature
Month Lbs hnr19DlscrepaçyindicationSpace
20 Facility Owner or Oporejo Ceniflcaon of receipt of waste materials covered by this manlisat except as noted In Item 19.
CMS Landifli
j..PnmnIecI/TypO Name
IiL
AWtFormijT/S/Djp copy
Please print or type
dealanad ror Use
ELLIED WASTENDUSPIEINC
Mailina
u.Ut.r EIdru Lc
Generators Phone 7t3i.72tsPorlercompanyNamer6_
ateci Facility Name and Site
CfvS Lanciffil
5105 Morehead Rd
Concorde NC 28027
11 Waste Shipping Name and Description
Additional Descriptions for Materials Listed Abov
Codes for Wastes Listed Above
SpeciHanngin5tmioflsafldAddifloflauiflfQaiiI
16.
More/%I nrfrk IJ7j17TransporterAcknowIedemantofReceiptof Materials
Printed/Typel Name
3ure18TranspofterAchinowledgemontofReceiptofMaterials
CMSLaridfJjj
Prlnted/yp0 Name
gnatu
AWI i1TIS/D/F/copy
V.ALLIEDWAST
IN
NON-HAZARDOUS 1.GeneratoUS EPA ID No Manifest PageWASTEMANIFESTDocumentNo i2 870
Generators Name anti Mailing Address Truck Nouib
oii
Generators Phone 772
Transporter Company Name US EPA ID Number Transporte hont..fiQ rf
Transporter Company Name US EPA ID Number 13 flansportors Phone
-. .........................I.........DesIgnated Facility Name and Site Address io US EPA It Number Facilitys Phone
CMS Landfill 704 7822D045105MoreheadRd
Concord NC 28027
11Waste Shipping Name and DescriptIon ..12 Containers 13 14
..Tofel UnitNoTypeQuantityWWoI
tL.4 jt
Additional iescrlplions for Materials Listed Above Handling Codas for Wastes Listed AbàvŁ
ci 77i
15 Special Randuing instructions and Additional Information
16
Prlnted/TypociNarna L7ii-jq..17 Transporter Acknowledgement of Receipt of Materials
Printed/1\pedNama ..Si ature Thnr
18
Printed/Typed Name
19 Discrepancy indication Space
....._..._..____._____._________20 FacIlity Owner or Operator Cerilication o1retieijt of waster te cóverjd byth ilestsxdapt noted hi 11am 19.
j9nahJre
Ptegse print or type
Form dasined for tiso on elite 12 pitch typewriter 1i icJ
GENERATORS CERTIFICATION certify the materials described above on this manifest are not sublect to tadami reguiatios iorrndrthg proper dispoabi
ct HsdousWaste
\j .--
..
________________________________________________________________________________________
___________
Additional Descriptions for Materials Ustod Above
Handling Codes for Wastes Listed Above
15 SpecIal Handling instructions and Additional information
Pripted /Typed Name
atureZ7 /7 Month DoY bar
14-./
CMSLanIfIJ ...
Please print or typo
Form designed br use onellt 12 pitch typewriter
..
FiAALLPED WASTElND.U5jnJ.ç
NON-HAZARDOUS Generators US EPA ID No Manifest PageWASTEMANIFESTDocumentNo
Generators Mama and Mailing Address Trucic No
.hiüt
Generators Phone
Transporter Company Name US EPA ID Number
Transporter Company Name US EPA ID Number
Designated Facility Name and Site Address 10 US EPA ID Number
OMS Landfill ...5P5Morehead Rd
Coricotc1NC 28027
Transporhdj_y
Transporters Phone
Facilitys Phoæo
11.WaithShipplng Name and Description 12 Containers 13 14
Total UnitNoTypeQuantityWI/Vol
704 782-2004
IL liIt
--
Please prtnt or type
Fbnn designed fdr CaB on elIte 12 pItch typewiler
16 GENERATORS QERTIFtOATION certity the materials deecdbd abOve on this manliest era not subject to federal regulations for reporting proper disposal of Hazardous Waste
17 Transpoijer Acknowledgement of ReceIpt of Mateilalo
18 Transporter Acknowledgement of Receipt of MaterialsLj20FacilityOwnerorOperatorCerlilcailon of receipt of waste materials covered by this manifest except as noterj In Item 19
NQN-HAZRDOijSWASTEMAnPT 1TI5 Jt
Fago 27.12of
Generators Name and Mailing Addre5s LRLnu sriiirc23LGeneratorsPhone
.U
--0der2mpanyNaj
DesIgnated Faculty Name and Site Address
CMS Landflli
5105 Morehoad Rd.
Concord NC 28027
Truck Mo
US EPA ID Number
4-ansPorlhoç3
10 US EPAID Number
Phone
Phone
704 782-2004
..
12 Containers
No
13 14.
Total Unit
Quanuty WiNd
WASTEINDUSTpjslNc
hi-LJTb NC 223GanemtorPhone
Transporter Company Nameorter2anyNaJ
CMS Landfill
704 7B2-20045105MoreheadFd
Concord NC 28027
Coe 13 14
11 ado pp ng amo an eec
Total Unit
kfl
eatai Handling neirucifons and Addlif
at HJou5 Waste
17 Transporter Acknowledgement of Receipt of Materials
Printed Typed Name
Signature
Mwflh
18 Transporter Acknowledgement Receipt of Materials
Printed /1ped Name
Signature MsnU Cy Yew19DiscrepancyIndicationSpace
Generatóig Name and Mailing Address
.-____
FacIiltys Phone
Pipase print or typo
iForni designed lór USO Ofl otto 12ptlch typewri1er
CMS Landfill
5105 Morehead Rd
Concord NC 28027
16 GENERATORS CERTIFICATION crIIfy the matorInI described above on Ihie manirost are not subject âiedo pUietFons for reporIIngpnipsr disposal c1HazadoueWestoPdflted/Typad18 Signaluro i-
17 Transporter Acknowledgement of Receipt of Materials
PrlnIerJITypecjarn5
WASTEiJINDUSIPIES1N
ON-RDQUS Generators US EPA Manliest 2.PaWASTEMAFEST..Document No
Genrators Name and Melting Address tr
Generators Phone
Transporter Company Name
ruth tistethMuNC3Z2
Transporter Company Name 3c-Thc4ynr US EPA ID Number
Truck No
Designated Facility Name and Site Address
i--US EPA ID Number
TransporiØbah5
10 US EPA ID Number
Transporters Phone
FaciHtys Phone
704 782-2004
..
AdditIonal Descriptions for Materials IJeted Above
Handflng Codes for Wastes Listed Above
.1
15 Speclal Handling Instructions and Additional Information
P.
.0
13
ALLIED WASTE
Genaralos us EPA Nd
Please print or type
Form designed fr use on elite 12 pitch typewriterNON-HAZARDOUS Dotlo f2WASTE_MANIFEST_____________________________Generators Name and Mailing Address rjj Lm-cthck Nt 242GeneratorsPhone
Transporter Company Name GØCk1-US EPA ID
Transporter Company Name US
Designated FacUlty Name md Site Address 10
CMS Landifif
5105 Morehead Rd
COncord NC 28D27
11.Vste Shipping Name and Description
ci
Addilional Descriptions for Mateilals Usted Above
15 SpecIal Handling instructions and Additional lnlormaton
16 GENERATORS CERTIFICATION certuy the nialertele described above on this manifest am not subject to federal regulØttopie for reportlnp preper disposal of Haoardoja WastePrintedITypedName
Signature
17 Transpotor Acknowledgement of Receipt of Materials
PrInted/Typed Name
Sinature.7 ./ThIIt JJ_lB Transporter Acknowledgement of Receipt of Materials
Printed/Typed Name
Signature 0a That
IJisorupancy Indication Space
20 FacilIty Owner or Operator Car Ulca lion ol receipt 01 waste materials covered by this maniI except as noad iæliernl9CMSLandtiII
Printed /Typs Name iture
MOfltfr That
I-S ___
--AWtForm 121.r/s/wpj-copy .5-
FtssSe print Or typeFormdeslnedfor use on elIte 12 pitch typewiiter
16 GENERATORS CERTIfICATj0N certify the materials descdbd above on thbninUesI are tIusbfect to federal rogulatloha for reporting propórdlsporrai of Hazardous WastePrintedhYpedNamenatur7/./Mnih DAy Af
17 Transporter Acknowledgement of Receipt of Materials .2
Printed Typed Name pahire7/
liownerorrcerliIgalionOfreseiptofstatridbth
ALLIED WASTENDilsipiESIFi
Transporter Company Name US EPA ID Number
NON-HAZARDOUS Generators US EPA ID No Manifest PageWASTEMANIFESTDocumentNoof
Generators Name and Mailing Address ..UJs55 Truck NoilUw4tCj itrtrf
Generators Phone 1J4..7.2t
Transporter Company Name jrAthr crc ii US EPA ID Number
DesIgnated Facility Name and SiteAddress 10 US EPA ID NumberCMSLandfill..
5105 Morehend Rd
Concord NC 28027
Transporters Phone
Facilitys Phone
704 782-2004
it Waste Shipping Name and DescriptIon 12 Containers 13 14
Total UnitNoTypeQuantityWtNoI
170
AddItional Descriptions for Materials Usted Above
15 Special Handling lnstwctlo and Additional Information
15 SpecIal Handling Instrucflons and Additional Information
Punted/Typed Name ii
_____17 Transporter Acknowledgement of Receipt of Materials .-________
__________Prinled/Typed Name Igpaturyti1
_____________________________J...Jp
CMS Landfill
TISID/I/.copy
Generators Name end MalHng Address
LLIED WASTEDV.1 NC
Generators Phone
ManlIest PageDocumentNool
VI
q.7
tdi4 .iuth Liknj
rr
127878
Truck No
Transporter Company Name US EPA ID Number A.1ansporte.ror_-1
Transportar2 Company Name US EPA ID Number Transporters Phone
DesIgnated Facility Name and Site Address 10 US EPA ID Number Facilitys PhoneCMSLandfill7347B220Q45105 Morehoad Rd
Concord NC 28027
11.Waste Shipping Name and Description 12 ContaIners 13 14
Total UnitNoTypeQuantityWtNoihd
_______________________.11
Addlttonai Descriptions for Materials Listed Above
Handling Codes for Wastes LlaIed Above
LLIED WASTEPiaaseprbnorlypeNDUSTRISINCiromldesgnnrItaruseaneUta12pItchtYpeWiIter-_for27879GeneratorsNameantiMailingAridress
Truck No-nh çIy
Generators Phone
.______-------
CMS Landfill
704 78-20045105MoreheadRd.
itaIn 13
Total Unit
pa ______
./5_IC
Addutial Descriptions for Materials Listed Above
Handling Codes for WasIs Listed Above7L
15 SpecIal Handling Instructions and Additional informatIon
tePriflted/Typ2d Name
S7ture 77 4/1117TransporterAcknowledgementofReceiptofMerIaIs
Prlntd flipecj Name
oorRe Mils
cIJl Owner or Operator coriflij_..........._
19
AWIForm 121T/S/D/p/Copy
Transporter 2.Cornpany Name
DesIgnated Facility Nam dSlie Address
CMS Landfjlj
5105 MorØhead Rd
Concord NC 2802T
11 Waste Shipping Name ÆndDesoription
Ft
ci
1AiLLIED WASTEPleasaprlntortypeSTPIESIN.CFoimdesignedtaruseonelite12pllctypewilter
NON-HAZARDOUS Generators US EPA It No ManlIest PageWASTEMANIFESTDocumentNoof
Generators Name and Mailing Address TruOk NOi$.-..1
Generators Phone
Transporter Company Name -ldtr US EPA ID Number TmnsporteLhoni jf
US EPA ID Number Transporters Phone
10 US EPA ID Number Facilitys Phone
704 782-2004
Additional Descriptions for Materials Usted Above
Handling Codas for Wastes Listed Above
15 SpecIal Handling Instructions and Additional Information ________
16 GENERArORS CERTFICAT1O Icartily the materials described above on this manilest are not subject to Federal reulaUons far reporting proper disposal of Hnzaidoua WastePrinted/1ped Name Li ftl aIuri7
/1jZ-/17 Io17TransporterAcknowledgementofReceIpt01Materials
Prlnted/fljpc1 Name
Ona/
I8flanpoj Ac owecfgemanj of RecTpt of Materials
Printed/Typed Name
Signature
19 DIscrepancy Indication Space
--
Piàasaprlntortypa
FormdeslgneUOr UBB On elIte 12 pitch typewriter
Generators Name and Mailing Address
ALLi WASTE...IN DUSIR IEV NC
NON-HAZARDOUS Generators US EPA ID NoWASTEMANIfT -_____
Generators PhonB
li/7
Transporter Company Name
Transporter Company Name
Liiti
Designated Faculty Name and Site Address 10 US EPA ID Number Facilitys Phone
CMS Landfii 704 78220045105 Morehead Rd
Concord NC 28027
11 Waste Shipping Name and Descripuon 12 Containers 13 14
Total UnitNoTypeQuantityWLJVOt
../2.7
Additional Descriptions for Materials Usleci Above
Handling Codes for Wastes Listed Above
15 Special Handling Insiwoilons and Additional information
16 GENERATOR CERTIFICATION certtly the materIals described above on this manliest are not sublect to laderal regulatIons for reporting proper dIaposprPrinted/Typed Memo
Signature..2 iiiiiI.prL_VirflS1 li17TransporterAcknowledgementofReceiptof Materials
.rtçPrintedTypedName
Signature a1j 4jL_________________________________ç_77f -%i18
Printed /1spad Name
Signature
19 DIscrepancy Indication Space
r-çI
..tI
20 FacilIty Owner or Operator Ceriticatlon of receipt of waste materials covered this qitfest excptaa
CMSLafldfjfl ft.Printed/Type Name
sIfletu
....______
___T
WASTE //-7
PfgisDptintDrtype STRI$INC
Form destgnBd ror use on eMs 12 pitch typewilterNON-HAZARDOUS Na Manliest aPagel
WASTE MANIFEST Document No of 127881
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Transporter Company Name ho .6.US EPA ID Number Transportd..fl1p
Transporter Company Name US EPA ID Number TransPDrtes Phone
DpslgnatedFaciury Name and Site Address 10 US EPA ID Number .C Facilitys Phone
OMS Landfill 704 762 20045105 Morehead Rd ..Concord NC 28027
11 Waste Shipping Name and Description 12 Containers 13 14
Total UnitNo1jpeQuantityWlIVoi
4M
Additional Descriptions forMatari.als Listed Above Handling Codes for Wastes Usted Above
11 II
15
.16 GEN6RATORS CERTIPICATION crtUy the materials dssciibudbove this estsrŁ.note to fØdGII
Printed Typed Name IatuIwp j7..
cliii Owner or OperÆtor Cgrhlicatjon or lacoI of waste maiØrfaisc
CMSLaridfluI
Printed/Type Name 4_J /7
Generators Name and Mailing Address
Generators Phone
Truck Nokt
Special Handling Instructions and Additional information
17 Transporter Acknowledgement of Receipt of Materials
Printed Typed Name Si natUre13e2kle114sok
--18._TranspotlergAoknowiodgomeritofRecarpt of Materials
PrinlalJilped Namo
19 Discrepancy indication Space
1.Sineture
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liSP Associates PA
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Corporate Office
41w hug
PU Bat 7030
Charlotte North Carolina 28241
Physical
3475 Laheniont Boulevard
Fort MIII SC29708
803 802 2440
Raleigh Wilmington Concurd
14001 Weston Pus kway 2120-B Capitaiflrive 4601 Corporate Drive NW
Suite 100 Wilmrngton North Carolina 28405 Suite 165
Casy North Carolina 27513 910 313 6648 Concord North CarolIna 28027
9196781070 7047939855
800 960 7317
www espassaclatescwn