HomeMy WebLinkAboutItem No 25 - Initial Abatement Action Report Incident 36325 -OCRepar
NCDENR
UST Section
Mooresville Regional Office
919 North Main Street
Mooresville North Carolina 28115
Attention Mr Allen Schiff
Dear Mr Schiff
INITIAL ABATEMENT ACTION REPORT
Morehead Common Site Area No
919 West Morehead Street
Charlotte Mecklenburg County North Carolina
UST Incident No No Yet Assigned
ESP Project No E6-UD42.601
On behalf of the property owner Beazer Homes ESP Associates P.A is pleased to provide the
attached Initial Abatement Action Report for the closure of the subject propertys petroleum
release ESP respectively requests classification of the release as Low Risk and issuance of no
further action notice
Thank you for your attention in this matter If you should have any questions please
do not
hesitate to contact me at 803 835-0915
Sincerely
ESP Associates P.A
gar Rogers
Staff Scientist
cc Jade Eastridge Beazer Homes
Ward PG
Environmental Services ManagerNCLicenseNo1600
RO Box 7030 Charlotte NC 28241
1.80096Oj317 NC 704.S83A949 fax 704583.495O SC 803.802.2440 fax 803.802.2515
Www.espassocjates.com
$ESP
ESP Associates P.A July 30 2007
Reference
Initial Abatement Action Report
SITE INFORMATION
Site Identification
i1 Date of Report July 30 2007
Facility ID NA
UST Incident Number Not Yet Assigned
Site Name Morehead Common Site Area No
Site Street Address 919 West Morehead Street
City/County/Zip Code Charlotte Mecklenburg County 28278
Description of Geographical Data Point Approximate center of UST
Location Method Mecklenburg County Polaris GIS Map
Latitude 35.2277
Longitude -80.8582
Information about Contacts Associated with the Leaking UST SystemUSTOwnerBeazerHomes
1300 Blvd Suite Charlotte NC 28203-4265
704.370.7200
UST Operator N/A
Property Owner Same as above
Property Occupant Same as above
Consultant/Contractor ESP Associates P.A Chris Ward PG
P0 Box 7030 Charlotte NC 28241
803.835.0915
Analytical Laboratory Prism Laboratories Inc
P0 Box 240543 Charlotte NC 28224-0403
704.529.6364
NC Certification No 402
Information about Release
ci Date Discovered June 18 2007
ci Estimated Quantity of Release Unknown
ci Cause of Release Unknown
ci Source of Release 350-gallon steel diesel UST
ci Size and contents of UST
System from which release occurred 350-gallon steel diesel UST
Ward Professional Geologist for ESP Associates P.A do certify that the
contained in this report is correct and accurate to the best of my knowledge
P.A is licensed to practice both geology and engineering in North Carolina
Associates certification numbers are Geology C-347 and Engineering C-0587
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No July 30 2007
INTRODUCTION
The subject site has an address of 919 West Morehead Street in Charlotte Mecklenburg County
North Carolina see Figure Topographic Site Location Map The area of the subject release
associated with an orphan 350-gallon diesel underground storage tank UST uncovered on June
18 2007
has been designated by ESP as Area No of the Morehead Common site
SITE HISTORY AND CHARACTERIZATION
On June 18 2007
ESP responded on behalf of Beazer Homes to an encounter with UST and
petroleum-impacted soil during excavations conducted ahead of mass grading operations
at the
subject site Upon arriving at the site ESP observed 350-gallon steel diesel UST and soils with
petroleum-odor located on the south side of West Morehead Street approximately 190 feet west
of its intersection with South Clarkson Street on Tax Parcel No 07325210 see Figures and
As required ESP emailed notification of the release discovery along
with Release and UST
Leak Reporting Form to Mr Steve Bograd of the Mooresville Regional Office of NCDENR on
June 19 2007
Release Location
The subject site former auto repair facility is located within an urban area of Charlotte which
historically included warehouse and commercial structures Site structures associated with the
former auto repair facility were razed sometime between 2002 and 2005 The site is currently
mass graded with no surface structures present Facility ID No was not available for the site
Based on our review of the Geologic Map of North Carolina 1985 the subject site is located
within the Charlotte Belt locally comprised of intrusive metamorphosed granitic rocks locally
pinkish gray massive to weakly foliated and containing hornblende Soils encountered in this
area are the residual product of chemical weathering of rock presently underlying the site Soil
Initial Abatement Action Report ESP Project E6-UD42 601MoreheadCommonSiteAreaNoJuly30 2007
weathering is more advanced near the surface grading with depth to less weathered rock and
finally bedrock
UST Information
Following the June 18 2007 discovery of the sites 350-gallon diesel UST AD Environmental
and Industrial Services AD of High Point North Carolina was contacted to remove remaining
product/sludge from the tank prior to its removal from the excavation On June 19 2007
AD
pumped less than 10 gallons of product/sludge from the tank for permitted recycling at their
Archdale North Carolina facility see Product Material Manifest in Appendix Once
removed the 350-gallon tank was transported by AD to the Griffin recycling facility in
Greensboro North Carolina on June 19 2007 see Tank Disposal Manifest in Appendix See
site photographs in Appendix
PreviousTankInstallationRemovalSizeTankLastTankNoDate Date Gallons Dimensions Contents an
Contents
Unknown 6-18-07 350 6.7 ft ft Diesel Unknown
completed UST-2 Form is included as Appendix The former location of the above UST is
depicted on Figure
Previous Reporting
ESP emailed release notification along with 24-Hour Release and UST Leak Reporting Form
to the Mooresville Regional Office of NCDENR on June 19 2007 see Appendix
Additionally ESP submitted 20-Day Report to NCDENR on July 18 2007
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No July 30 2007
INITIAL ABATEMENT ACTIVITIES
Initial Contaminated Soil Excavation
On June 19 and 20 2007 ESP documented the excavation of 196.64 tons of impacted soils from
Area No by the sites grading contractor Gelder Thompson of Midland North Carolina The
excavation was advanced based on results of OVA field screening and evidence of visible
staining The resulting excavation measured approximately 12 ft 28 ft 10 ft deep The
excavated soil was placed on and covered with plastic awaiting subsequent off-site permitted
disposal Neither groundwater bedrock nor free product were encountered within the tank pit
See site photographs in Appendix
Initial Post-Excavation Confirmatory Sampling
On June 19 2007 confirmatory soil samples were collected at depth of feet BLS from each
of the excavations four sides WS-1 through WS-4 while one sample was collected at depth
of 10 feet BLS from the base of the excavation B-i The sidewall samples were collected at
the foot depth due to the prevalence of elevated OVA readings at that depth The five soil
samples were hand delivered on ice to Prism Laboratories of Charlotte North Carolina to be
analyzed for risk-based parameters which include volatile organic compounds VOCs by EPA
Method 8260B semi-volatile organic compounds SVOCs by EPA Method 8270C VPH/EPH
by the Massachusetts Department of Environmental Protection MADEP method and for total
lead and chromium by EPA Method 60 lOB Sample locations and excavation dimensions are
depicted on Figure Soil Sample Location Map Sampling was performed in general
accordance with ESPs SOP see Appendix
Results of the laboratory analysis
of confirmatory samples WS-i through WS-4 and B-i revealed
that all analyzed constituents were either below reporting limits BRLs or below the lowest of
the soil-to-groundwater or residential MSCC with the exception of benzoaanthracene 0.89
mg/Kg benzoapyrene 0.95 mg/Kg benzobfluoranthrene 1.1 mg/Kg and MADEP EPH
Cl 1-C22 Aromatics 130 mg/Kg
detected in wall sample WS-3 Laboratory analytical results
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No July 30 2007
for the confirmatory soil samples are summarized on Table B-i The Prism laboratory data
report is included as Appendix
Follow-up Contaminated Soil Excavation and Confirmatory Sampling
Due to the detection of elevated constituents above applicable standards in confirmatory sample
WS-3 an additional two feet of soil was excavated from the southern wall of the excavation on
July 2007 Excavated soil was placed on the previous soil stockpile for subsequent off-site
permitted disposal
The resulting excavation measured approximately 14 ft 28 ft 10 ft
deep See Figure for depiction of the excavation limits and sample locations
On July 2007 following excavation of additional soil ESP collected confirmatory soil sample
WS-3 at depth of feet BLS from the southern wall of the excavation Sample WS-3 was
submitted to Prism for analysis of SVOCs by EPA Method 8270C and EPH by the MADEP
method Results of the analysis of the July 2007 confirmatory sampling revealed that all
analyzed constituents were BRLs see Table B-i The Prism laboratory data report is included
as Appendix
Stockpile Sampling and Soil Disposal
On June 20 2007 ESP collected two composite stockpile soil samples for laboratory analysis
The stockpile soil samples designated 1A and lB were placed in laboratory provided containers
labeled and hand delivered on ice to Prism for compositing and subsequent analysis The
samples were analyzed for TPH-GRO/DRO by EPA Method 5030/3550 and for BTEX by EPA
Method 8260B The composite samples were collected and analyzed to confirm that release
had occurred and to characterize contaminant types and concentrations for subsequent off-site
permitted disposal/treatment
As revealed by the laboratory analysis of stockpile composite samples 1A and 1B TPH-DRO
was reported at concentrations of 400 and 76 mg/Kg respectively while results for the
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No July 30 2007
remainder of analytes were BRLs Results of the stockpile sample analyses are summarized on
Table B-2 while the laboratory data report is included as Appendix
On July 19 and 20 2007 196.64 tons of stockpiled soil from the excavation was transported by
Gelder Thompson to the CMS Landfill in Concord North Carolina for permitted disposal see
Non-hazardous Waste Manifest in Appendix
RECEPTOR SURVEY
On July 20 2007 Mr Eddie Rogers of ESP performed receptor survey to document the
presence or absence of active and/or inactive water supply wells within 1500-foot radius of the
subject UST release see Figure Receptor Survey Map The receptor survey
included
interviews with available site occupants and visual observations for water supply wells and/or
municipal water meters All properties within 500 feet of the site were visited to determine well
status The area within 1000 feet of the subject release consists of commercial and industrial
development with numerous vacant structures No active or inactive water supply wells were
identified within 1000-foot radius of the subject release Municipal water and sewer have
historically been available within the area of the site Additionally no surface water bodies were
identified within 500 feet of the release see Figure
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No July 30 2007
CONCLUSIONS AND RECOMMENDATIONS
The following conclusions have been formulated based on our completion of field activities
including abatement activities receptor survey and our review of laboratory data from the
analysis of collected soil samples
The subject site razed former auto repair facility has an address of 919 West
Morehead Street in Charlotte Mecklenburg County North Carolina
On June 18 2007
ESP responded on behalf of Beazer Homes to an encounter with
350-gallon UST and petroleum-impacted soil during excavations conducted ahead of
mass grading operations
at the subject site
On June 19 and 20 2007 ESP documented the excavation of 196.64 tons of impacted
soils from the release area The resulting excavation measured approximately 12 ft 28
ft 10 ft deep
Neither groundwater bedrock nor free product were encountered within the tank pit
On June 19 2007 confirmatory soil samples were collected at depth of feet BLS
from each of the excavations four sides WS-1 through WS-4 while one sample was
collected at depth of 10 feet BLS from the base of the excavation B-i
ti Results of the laboratory analysis of confirmatory samples WS-1 through WS-4 and B-i
revealed that all analyzed constituents were either BRLs or below the lowest of the soil-
to-groundwater or residential MSCC with the exception of benzoaanthracene 0.89
mg/Kg benzoapyrene 0.95 mg/Kg benzobfluoranthrene 1.1 mg/Kg and MADEP
EPH Cl 1-C22 Aromatics 130 mg/Kg detected in wall sample WS-3
Due to the detection of elevated constituents above applicable standards in confirmatory
sample WS-3 an additional two feet of soil was excavated from the southern wall of the
excavation on July 2007 The resulting excavation measured approximately 14 ft 28
ft 10 ft deep
On July 2007 following excavation of additional soil ESP collected follow-up
confirmatory soil sample WS-3 at depth of feet BLS from the southern wall of the
excavation Results of the analysis of WS-3 revealed that all analyzed constituents were
Initial Abatement Action Report ESP Project E6-UD42 601
Morehead Common Site Area No July 30 2007
BRLs verifying that all impacted soil above applicable standards had been removed from
the excavation
On June 20 2007 ESP collected two composite stockpile soil samples designated 1A
and for laboratory analysis The composite samples were collected and analyzed to
confirm that release had occurred and to characterize contaminant types and
concentrations for subsequent off-site permitted disposal/treatment
As revealed by the laboratory analysis of stockpile composite samples 1A and 1B TPH
DRO was reported at concentrations of 400 and 76 mg/Kg respectively while results for
the remainder of analytes were BRLs
On July 19 and 20 2007 196.64 tons of stockpiled soil from the excavation was
transported to the CMS Landfill in Concord North Carolina for permitted disposal
Municipal water and sewer are available in the area of the release
No water supply wells were identified within 1000 feet of the release and
No surface water bodies were identified within 500 feet of the subject release
Based on the absence of analyzed risk-based parameters above the lowest of the North Carolina
soil-to-groundwater or residential MSCCs lack of either groundwater bedrock or free product
within the tank pit the documented absence of water supply wells within 1000 feet of the
release and the absence of surface water feature within 500 feet of the release ESP
recommends that NCDENR issue no further action notice for the subject release
Attachments
Table B-i Summary of Soil Sampling Results
Table B-2 Summary of Stockpile Soil Sampling Results
Figure Topographic Site Location Map
Figure 2005 Aerial Photograph
Figure Soil Sample Location Map
Figure Receptor Survey Map
Appendix 24-Hour Release Notification
Appendix UST-2 Form
Appendix Tank Disposal Manifest
Appendix Product Material Manifest
Appendix Site Photographs
Appendix ESPs SOP
Appendix Prism Laboratory Data Reports
Appendix Non-Hazardous Waste Manifests
ATTACHMENTS
TABLES
Table B-i
Date 7/25/07 Incident No Not Yet Assigned
1riflI
WS 6/19107 North Pit Initial
Wall Abatement
Summary of Soil Sampling Results
Morehead Common Area No Charlotte North Carolina
80l5B 8015B MADEP
EPH
MADEP
EPH
MADEP
EPH
MADEPVPH MADEP
VPH
MADEP
YPH 9071A
0C0 QC1
fl
OOCO C0
NA NA 13 12 12 NA
WS-2 6/19/07 West Pit
Wall
Initial
Abatement NA NA 13 13 13 6.7 6.7 6.7 NA
WS-3 6/19/07 South Pit
Wall
Initial
Abatement NA NA 130 12 12 6.1 6.1 6.1 NA
WS-3 7/5/07 South Pit
Wall
Initial
Abatement NA NA 11 11 11 NA NA NA NA
WS-4 6/19/07 East Pit
Wall
Initial
Abatement NA NA 6.1 1.7 6.1 5.9 5.9 5.9 NA
NA 12 12 12 6.2 6.2 6.2 NAInitialB-i 6/19/07 Pit Floor 10 NAAbatement
Soil to Groundwater MSCC mg/kg
II
Iiidustri Commeiial MSCC mg/kg
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNLNotListed
NL NL 34 3300 72 34 3300 Nt
NL Nt 469 93860 9386
939 469 9386 NIL
NL NL 12264 245280 24528 12264 245280
NL
Table B-i Summary of Soil Sampling Results
Date 7/25/07 Incident No Not Yet Assigned Morehead_Common Area No Charlotte North_Carolina
ucaI Method
_____ _____ _____ _____ __________ _____otantf cu
San4 1campi
ID Collect Area 1Łpth Phasem/dd/yy BQS rID
WS-l 6/19/07 NoiTh Pit Initial 29 48 0.0056 0.0056WallAbatement
6010B 6010B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B
-E .o
riEo
0.011 0.0056 0.0056 0.0056 0.0056 0.0056
6/19/07
WS-2 6/19/07 West Pit
Wall
Initial
Abatement 28 37 0.0053 0.0053 0.0049 0.0053 0.0053 0.0053 0.0023 0.0053
WS-3 6/19/07 South Pit
Wall
Initial
Abatement 46 110 0.0022 0.0053 0.013 0.053 0.0053 0.0053 0.0053 0.0053
WS-3 7/5/07 South Pit
Wall
Initial
Abatement NA NA NA NA NA NA NA NA NA NA
WS-4 6/19/07 East Pit
Wall
Initial
Abatement 28 22 0.0053 0.011 0.055 0.055 0.055 0.055 0.055 0.055
Initial
Abatement 32 23 0.0048 0.0048 0.0048 0.0048 0.0048 0.0048 0.0048 0.0048
27 270 2.2 1.7 0.58 3.3 4.3
47 400 3128 626 313 1564 626 626 782 782
BRL Below Reporting Limit
MSCC maximum soil contamination concenfration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzed
NILNot Listed
1226 400 81760 16350 8176 40880 16350 16350 20440 20440
Table B-iDate71 SummaryTnrtNoNotYetAs of Soil Sampling Results
Morehead Common Area No Charlotte North Carolina
North Pit
Wall
Initial
Abatement
8260B 8260B 8260B 8260B 8270C 8270C 8270C 8270C 8270C 8270C
00 N.
0.0056 0.0056 0.0056 0.0056 0.38 0.31 0.32 0.45 0.22 0.27
WS-2 6/19/07 West Pit
Wall
Initial
Abatement 0.0034 0.0082 0.0047 0.0032 0.35 0.0032 0.0032 0.0032 0.0032 0.0032
WS-3 6/19/07 South Pit
Wall
Initial
Abatement 0.0053 0.0044 0.0053 0.0032 0.34 0.89 0.95 1.1 0.69 1.1
WS-3 7/5/07 South Pit
Wall
Initial
Abatement NA NA NA NA 0.36 0.36 0.36 0.36 0.36 0.36
WS-4 6/19/07 East Pit
Wall
Initial
Abatement 0.0026 0.0067 0.0030 0.0023 0.40 0.40 0.40 0.40 0.40 0.40
B-i 6/19/07 Pit Floor 10 Initial
Abatement 0.0048 0.0048 0.0048 0.0048 0.38 0.19 0.21 0.33 0.13 0.23
4.6 0.0056 60 0.34
Soil to Groundwater Mcmg/
ResidentiMSg/
IidttriaIJommrcia1MStC mg/kg 760
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNLNotListed
3129 3200 1560
18 469 0.88 0.0088 0.88 469
0.091 1.2 6700 12
82000 40000
164 12264 0.78 12264 78
Table B-i
Date 7/25/07 Not Yet Assi
Summary of Soil Sampling Results
Morehead Common Area No Charlotte North Carolina
8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C
.n
-i NUuc
8270C
0.39 0.58 0.39 0.39 0.39 0.39 0.39
WS-2 6/19/07 West Pit
Wall
Initial
Abatement 0.32 0.63 0.44 0.44 0.44 0.44 0.44 0.44 0.44 0.44
WS-3 6/19/07 South Pit
Wall
Imtial
Abatement 0.83 2.1 0.33 0.13 0.24 0.41 0.24 0.14 0.33 0.33
WS-3 7/5/07 South Pit
Wall
Initial
Abatement 0.36 0.36 0.36 0.36 0.36 0.36 0.36 0.36 0.36 0.36
WS-4 6/19/07 East Pit
Wall
Initial
Abatement 0.40 0.40 0.40 0.40 0.40 0.40 0.40 0.40 0.40 0.40
0.39 0.39 0.39
0.30J 0.49 0.17 0.40 0.40 0.12
3.3 290 44 1.7 11
0.40 0.11 0.20J 0.51
1000 0.17 4.7 38 280
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BUS feet below ground surface
Results reported in mg/kg
Health based level 100%
Considered immobileNANotAnalyzedNLNotListed
0.88 469 620 63 469 4600 0.088 62 88 620
12264 16400 1635 12264 122000 0.78 1635 780 16400
Summary of Stockpile Soil Sampling Results
Morehead Common Area No Charlotte North Carolina
8015B 8015B 8260B 8260B 8260B 8260B
f2
Table B-2
Dare 7/6/07 Incident No Not Yet Assigned
AnalyticJ1Letho
utafcn-
Sample Date SJirci %s pie Incident
ID collected Area Depth j%Phase
mdd/yy Fiift
Stock-Initial1A6/20/07 1e composite 400Abatement
Stock-InitiallB6/20/07 ile composite 76Abatement
Soil to Groundwatk MSCCiigIkg
ResidentiatCC mg4g
ht Lt
IS1ustriaiiCo.thjrcia1 MCC NL
BRL Below Reporting Limit
MSCC maximum soil contamination concentration
ft BGS feet below ground surface
Results reported in mg/kg unless otherwise noted
ft Health based level 100%
Considered immobileNANotAnalyzedNL Not Listed
1.2 3.7 6.2
1.2
6.2
3.6
6.2
6.0
NL
6.0
0.0056
6.0
7.3 4.6
NL 164
NL NL 18 3200 1560 3129
82000 40000 81760
FIGURES
RQ.ECT NO SHEET TITLE FIGUREUD42601
DALE NTS TOPOGRAPHIC S/iF LOCATiON MAP P0 Box 7030Cha0ottoNC 2824
3475 Lokenon ROd
ATh 7/11/07 USGS CHARLOTTE EAST QUADRANGLE ip ESP Asoocates PA
1RAVVTV 8DMH PROJECT Fo M21 SC 29709CHECKEDBYMOREHEADCOMMONSiTE704 583 4949 NC
803-802 2440 SCCJWCHARLOTTE NORTH CAROLINA sooespaSxodarescon-FIGURE
FiGURE
2005 AERIAL PHOTOGRAPH
MOREHEAD COMMON SITE
CHARLOTTE NORTH CAROLINA
LEGEND
WEST MOREHEAD STREET
WS-4
WS-4
ws-1 ////
AREA
WS-2
AREA
.I
20
APPROXIMATE SCALEINFEET
ESP Asxoeates PA
P0 Box 7030
Chorlotte NC 2824
3475 Lokernont HOd
Foot MtlI SC 29700
704-583-494.9 NO
803-802-2480 SC
WS-3
WS-2
WS-3
CONRRMA TORY SOIL SAMPLE LOCA liON
AREA EXCA VA 770N DEPTH OF 10 FEET
AREA EXCA VA 770N DEPTH OF 10 FEET
FiGURE
SOIL SAMPLE LOCA 77GW MAPAREASAND/5
MOREHEAD COMMON SiTE
CHARLOTTE NORTH CAROUNA
ESP
ILLI IVV SHEET 77TLEUD4260
CALE NTS
47E 7/17/07
FiGURE
RECEPTOR SURLEY MAP
AREARAiN8DMHPROJECTMOREIIEADCG%VMON 7ECHECKED
cHARLOTTE NORTH CAROUNAFIGURE
ESP Associates PAESP
APPENDIX
24-HOUR RELEASE NOTIFICATION
Page of2
Chris Ward
From Chris Ward
Sent Tuesday June 19 2007 354 PM
To Steve.Bogradncmail.net
Cc Jade Eastridge jeastrid@beazer.com kholdenr@beazer.com Scott Jones scjones@beazer.com
Subject 24-Hour Notice Morehead Common Releases and
Attachments AREA 24-Hr Notification.pdf AREA 24-Hr Notiflcation.pdf
Steve
On behalf of Beazer Homes am
herein providing 24-Hour Notification of the discovery of three orphan USTs on
Beazer Homes Morehead Common residential/commercial development currently being graded The Morehead
Commons property is located on the south side of West Morehead Street at its intersection with South Clarkson
Street in Charlotte North Carolina On June 18 2007 during grading operations an approximate 550-gallon
steel
UST was uncovered on Parcel No 07325210 The UST was uncovered and determined to be partially filled with
sludge and some fluid with diesel odor this UST is being referred to as AREA An additional approximate
550-gallon likely diesel and an approximate 750-gallon likely gasoline were subsequently encountered side by
side approximately 25 feet from the first 550-gallon U5T encountered on Parcel No 07325210 these USTs are
being referred to as AREA
On June 19 2007 Ab Environmental and Industrial Services pumped remaining fluid and sludge from the USTs
and transported the USTs off-site for permitted disposal The tops of the USTs were buried to depth of
approximately feet below original grade and were severely rusted with numerous holes Soils adjacent to and
beneath all three USTs exhibited strong petroleum
odor and were visibly stained Excavation of soils adjacent to
and beneath the three USTs was initiated on June 19 with soils being stockpiled on site on plastic for subsequent
off-site disposal
Preliminary investigation
reveals that Parcel No 07325210 was once occupied by Tonys Auto Body Shop and
Shorts Imports The releases are identified on the attached PbF map included with the 24-Hr Notification
Forms
The Responsible Party for the property is
Beazer Homes
1300 South Boulevard
Suite
Charlotte North Carolina 28203-4265
Mr Jade Eastridge
704.370.7200
Please call with any questions
Thanks
Chris Ward PG
Environmental Services Manager
ESP Associates
803.835.0915 direct office
803.802.2515 fax
7/30/2007
Page of
704.506.7618 mobile
Chris Ward PG
Environmental Services Manager
ESP Associates
803.835.0915 direct office
803.802.2515 fax
704.506.7618 mobile
7/3 0/2 007
UST-61 24-Hour Reease and UST Leak Reporting Form
For Releases This farm should
be completed and submitted to the UST Sections regional office following known or suspected release from
an underground storage tank UST system This form is required to be submitted wiLhin 24 hours of discovery of known orinNCsuspectedrelease
FacUlty ID Number N/ADWMUSEONLYSuspectedContaminationYIN
Date Leak Discovered 1I oTIncidentRiskHlLU_______Confirmed OW Contamination YIN
Received On Received By Confirmed Soil Contamination YIN .j Comm/Non-Commercial t.vM
Reported by drcie one Phone Fax or Report Free Product YIN j4 If Yes State Greatest ReglNon.fegulated
._42c5Region..Thickness
INCIDENT DESCRIPTION
Incident Name 41t2 .9
Address LJQk-MD1FLLLL 41 County
Regional Office circle one AshevilltevilleCity/Town Ck f_JC Zip Code Raleigh Washington Wilmington
Winsto
Latitude tieini dagroos 51 773 Longitude anawogceoa Obtained by
Briefly describe suspected or confirmed release Including but not limited to nature of release dale of release amount 13 osofreleaseamountoffreeproduct present
and recovery efforts initial responses conducted Impacts to receptors/eØ-.--J Topographic map
.4 1-_t_J /7 GIS Address matching
1DOther
13 Unknown
Describe location
HOW RELEASE WAS DISCOVERED
Check one
Release Detection Equipment or Methods Visual/Odor Groundwater Contamination
13 During UST Closuret1emovat Water in Tank 13 Surfce Water Contamination
Property Transfer Water Supply Well Contamination her specify oTL4SOURCEOFCONTAMINATION
Primary Source of Contamination Primary Contaminant Type Location SettingheckonetheckoneCheckone
13 Confirmed UST Release Check one below
Gasolineloleselllcerosene 13 Facility 13 Residential
Heating Oil Residence Industrial13DispenserElOtherPetroleum Producls Other 1LJrbanLineReleaseMetalsRural-CTank Release Other Inorganics
SPill/Overfill 13 Other Organics13ExactFailureLocationUnknownor
Multiple Faflures
Ownershim
Municipal Military Unknown 1ate Federal County State
Operation Tripe
Public Service Agricultural Education/Relig Industrial 6Eal Mining
USI Form 5111/05 Page of
IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected Yes No
Number of Water Supply Wells Affected
Water Supply Wells Contaminated Include Users Names Addresses and Phone Numbers Attach additional sheet if necessary
LandownerSM /S
State
UST SYSTEM OWNER
UST OwnerlCornpany
2.L24/--Point of Contacrj sitri
StateCityA/C
Addressoo q%
Zip Code Telephone Number24737ry-
UST SYSTEM OPERATOR
UST Operator/Company
LANDOWNER AT LOCATIO
Telephone Number
OF UST INCIDENT
City
UII State
Address
Lp Code
Address
Zip Code Telephone Number
Person Reporting Incident Ch thif Company p_J t/C-9 Telephone Number c-Yi
Draw Sketch of Area showing two major road intersections or Attach Map
A-7--/fei /vj4
JL11-121Mlcr Address 113O d/rrV-2ct/tJate //j/UST FormBl 11/05 Page of
rGALE HIS 2005 SITE MAP________________P.O Ur TIflI
649/07
rv Msc7ua347 LnnnI flhI
LffJ2.6O SHEET TIJLE AREAS NO AND
sESP
ESPMocIuIc.P.\
RA$H 8rDMH PROJECT MOREHEAD COMMONS SITEHEQEVCJWCHARLO7TEINOR17I CAROLINA
APPENDIX
UST-2 FORM
ST2 Site Investigation Report for Permanent Closure or Change-in..Service of UST
Return completed form to STATE USE ONLYTheDWMRegionalOffice located in the area where the facility is located Send copy to the Central Office in Raleigh so that _________________the status of the tank may be changed to PERMANENTLY CLOSED and your tank fee acceunt can be closed outSEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES Date Received
INSTRUCTIONS READ THIS FIRST
For more than five UST systems you may attach additional forms as needed
Permanent closure For permanent closure complete all sections of this form
Change-in-service For change-in-service where UST systems will be converted from containing regulated
substance to storing non-regulatedsubstancecompletesectionsIlIIIIVandVIII
Effective February 1995 all UST closure/change-in-service reports must be submitted in the format provided in the ST-i form UST closure andchange-in-services must be completed in accordance with the latest version of the Guidelines for Tank Closure copy of the UST-1 form and theGuidelinesforTankClosurecanbeobtainedatwww.wastenotnc.org
You must make sure that USTs removed from your property are disposed of properly When choosing closure contractor ask where the tanks will betakenfordisposal Usually
USTs are cleaned and cut up for scrap metal This is dangerous work and must be performed by qualified company Tanksdisposedofillegallyin fields or other dumpsites can leak petroleum products and sludge into the environment If your tanks are disposed of improperly youcouldbeheldresponsibleforthecleanupofanyenvironmentaldamagethatoccurs
NOTE If release from the tanks has occurred the site assessment portion of the tank closure must be conducted under the supervision of P.E orL.G with all closure site assessment reports bearing the signature and seal of the P.E or L.G
OWNERSHIP OF TANKS IL LOCATION OF TANKSOwnerNameCorporationIndividualPublicAgencyorOtherEntityFacilityNameorCompanyBeazerHomesNA
Street Address Facility ID If known1300BoulevardSuiteNA
City County Street Address
Charlotte Mecklen burg 919 West Morehead StreetStateZipCodeCity County Zip CodeNC28203-4265 Charlotte Mecklenburg 28278Phone Number Phone Number704.370-7200
III CONTACT PERSONNELContactforFacilityJobTitle Phone NoN/A
Closure Contractor Name Closure Contractor Company Address Phone NoJimStrattfordGelderThompsonBox 288 Midland NC 28107 704-269-0070PrimaryConsultantNamePrimary Consultant Company Address Phone NoChrisWardPGESPassociatesP.A PG Box 7030 Charlotte NC 28241 704-802-2440IVUSTINFORMATIONFORREGISTERED UST SYSTEMS EXCAVATION CONDITIONTankSizeinTankLastLastUsePermanentChange-in-Water ifl Free Notable odor or visibleIDNoGallonsDimensionsContentsDateCloseDateServiceati0productsoilcontaminationYesNoYesNoYesNoDate
El El DEl El
El El El El 0_El
El 00 El El El
El El El DEl El
El El El El El ElVIUSTINFORMATIONFORUNREGISTEREDUST SYSTEMS VII EXCAVATION CONDITIONTankSizeinTankLastLastUsePermanentTank Owner Water in Free Notable odor or visibleIDNoGallonsDimensionsContentsDateCloseDateNameexcavationproductsoilcontroinaljonYesNoYesNoYesNo3506.7 ft.x3ft Dielsel Diels NA 6/18/07 El El .__jj ElElElElEl El
El El El El El El
El El
El
VIII CERTIFICATION
certify under penalty of law that have personally examined and am familiar with the information submitted in this and all attached documents and thatbased on my inquiry of those individuals immediately responsible
for obtaining the information that the submitted information is true accurate andcomplete
Print name and official title of owner or owners authorized representativeChristopherWardPGDepartmentManagerESPAssociatesP.A
UST-2 Rev 11/2006
000_________-000
If the tank owner address is different from the one listed in Section then enter the street address city state zip code and telephone no below
El
El
Date Signed
2007
APPENDIX
TANK DISPOSAL MANIFEST
Environmental atid Industrial ServicesJJP.O Box 484 High Point NC Phone 336 434-7750 FAX 336 434-7752
TANK DISPOSAL MANIFEST
Tank Owner/Authorzed Representative Name and Mailing Address _____________________________________k e4
Tank Owner/Authorized Representative Contact 9vPhone
Description Of Tanks
Transporter The undersigned certifies that the above listed storage tanks have been transported to ADEnvironmentalandIndustrialServices2718UwharrieRoadArchdaleN.C 27263
T1
Month/Day/Year
Printed/Typed Name 6/natur Month/Day/Year
Disposal Certification The undersigned certifies that the above-named storage tanks have been cut
into scrap pieces and accepted by the metal recycling facility
Recycling Facility ID rkro jj
Tank No Capacity Previous Contents Comments
I47t/7cZ
Ni-
Tank Psvner/Authorized Representative Certification The undersigned certifies that the above listed storagetankshave been removed from the premises of the tank owner
rinted/Typed Name
APPENDIX
PRODUCT MATERIAL MANIFEST
TEL 336 434-7750
FAX 336 434-7752
MAERIAL
MANIPEST
EMERGENCY PHONE NO
800 434-7750
Environmental and
Industrial Services Inc
POST OFFICE BOX 484.HIGH POINT NC 27261
AO IOI5
Manifest Document No
Page of
.1
Job No
GENERATOR iNFORMATION
USEPAlDN1JH
Street Address Mailing Address Phone No
ContacthM4kh--.y
DESCRIPTION OF MATERIALS
USDOT Proper Shipping
Name Hazard UN NA Packing Containers Total UnitHMCompleteAllItemsforHazardousMaterialsClassorDivIDNoGroupQtyTypeQuantityWtJVol
IUn fIu3Y1I31U
IADD
TIONAL INFORMATION ERG No
-----I_________
GENERATORS CERTIFICATION
1-This isfo crtifythät the above-described matetiaIsareproperiy classified -describedpackaged marked andIabeled and are in
proper condition for transportation aöcording to the applicable regulations
of the Department of Transportation further certifythatnoneof the materials described above are hazardous waste as defined by EPA 40 CFR Part 261 or any applicable state lawandunlessspecificallyidentifiedabovethe materials contain less then 1000 ppm total halogens and do not contain quantifiablelevelsppmofPCBsasdefinedbyEPA40CFRParts279 and 761
Printed Typed Narre Signature Mo Day YrJr441tzj4
TRANSPORTER INFORMATIOr1
Transporter hereby acknowledge receipt of the above-described materials for transportENVIRONMENTALANDINI$IJSflUAL SERVIFES from the genera for site lsted above
prnteARCHDALENC27263hereby acAnoithdge
that the above-described materials were received
Transporter or Unit No from he geherator ite1and were transported to the facility listed belowIENo --.J7A/Phone 336 434-7750 Signature /1/y Delivei4 Date
ACILTINFORMATIOàt //
IFacility hereby acknowIefgo receipt of the materials covered by this manifestENVIRONMENTALANDINDUSTRIALSERVICESexceptoranydlsciepancy noted below
IAdss
2718 UWHARRIE ROAD
Signature \_4O Receipt DateARCHDALENC27263
Facility or
EPA ID No NCD986232221
Phone 336 434-7750
iContact ERIC McMANUS
ORIGINAL Facility Retain COY Return to Generator COPY Transporter Retain COPY Generator Retain
APPENDIX
SITE PHOTOGRAPHS
APPENDIX
ESPS SOP
STANbARb OPERATING PROCEbURE
SOP-6
SOIL SAMPLE COLLECTION
ESP Associates P.A Revision bate 3/7/06
This standard operating procedure SOP covers the collection of soil sample for
laboratory analysis
Follow these steps when collecting the soil sample unless
otherwise instructed by the project manager
Gather needed field supplies noted below
Confirm lab cooler contains needed sample containers fill cooler with
ice
Upon arriving at site check in with the property owner or company
representative
becontaminate the stainless steel hand auger before and between sample
collection by washing with Alconox soap and scrub brush rinsing with
distilled water and spraying with Isopropyl alcohol Wrap clean sampler
in aluminum foil
Wear disposal latex or nitrile gloves and change into new pair between
samples
buring advancement of the hand auger collect soil samples at regular
intervals for describing lithology Note lithology and other
characteristics of soils in field book relative to depth
If appropriate place representative portion of soil sample into
resealable plastic bag label with boring number and depth interval and
allow to equilibrate Screen soil in bag for volatile organics using an OVA
or Hnu Enter results into field book
Advance hand auger boring to previously specified sampling depth
Collect soil sample from this depth and place in laboratory provided
containers Label containers with boring number and sample depth usingthefollowingsamplingschemei.e B-i ft B-i 10 ft B-2 ft etc
benote boring location in field book relevant to pertinent site features
10 Following collection of the soil samples abandon all boreholes feet or
greater in depth with cement grout
ii Complete and sign the labs chain-of-custody
12 Keep the sample cooler in secure location until delivered under normal
chain-of-custody procedures to laboratory
50P-6 Soil Sample Collection Revision bate 3/7/06
ESP Associates Page of
SUPPLIES
SOP-6
Stainless steel hand auger with needed extensions or sampling
spoon
OVA or Hnu
Measuring tape
Plastic zip-lock bags
Isopropyl alcohol
bistilled water
5-gallon wash bucket scrub brush and Alconox soap
Cement with wheel barrow for mixing
Cooler with sample containers and chain-of-custody
Ice
Permanent marker
bisposable gloves
Knife
Field book
Site plan with site specific sampling instructions
Camera
APPENDIX
PRISM LABORATORy DATA REPORTS
E1I JLL 10
Case NarrativePRISM1iLABOP.ATORESINC
Date 06/29/07 Client Project ID Morehead Conirnons NoCompanyESPAssociatesPAPrismCOCGroupNoG0607542ContactChrisWardCollectionDates06/19/07AddressBox7030LabSubmittalDates06/19/07
Charlotte NC 28241
This data package contains the analytical results for the project idenfied above and includes Case Narrative Laboratory Report and QualityControlDatatotaling48pageschain-of-custody is also attached for the samples submitted to Prism for this project
Data qualifiers are flagged individually on each sample key reference for the data qualifiers appears at the end of this case narrative Qualitycontrolstatements and/or sample specific remarks are included in the sample comments section of the laboratory report for each sampleaffected
Semi VolatiIe Analysis
No Anomalies Reported
Volatile AnaIy
Analysis Note for Q24604 MSD C9-C1 Aliphatics Recovery above the control limits
Metals Analysis
Analysis Note for Q24519 Method Blank Lead MB is greater than 0.25 mg/kg
Wet Lab and Micro Analysis
N/A
Please call if you have any questions relathg to this analytical report
Date Reviewed by .PauIaA.Gilleland Project Manager
Łignaturj
Review Date 06/29/07 Approval Date
Data Qualifiers Key Reference
Compound also detected in the method blank
Result outside of the QC limits
DO Compound diluted out
Estimated concentration calibration range exceeded
The analyte was positively identified but the value is estimated below the reporting limitEstimatedconcentrationwithhigh bias
Estimated concentration with low bias
matrix effect is present
Notes This report should not be reproduced except in its entirety without the writtten consent of Prism Laboratoes Inc The results in thisreport relate only to the samples submitted for analysis
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0403
Phone 704/529.6364 Toll Free 8001529-6364 Fax 704/525-0409
/2Anea
5035
5035
5035
Laboratory Report
06129107
06/27/07 000 brown
06/27/07 000 brown
06/27/07 000 Ibrown
Q24503
Q24503
Q245o3
Q24503
Q24503
Q24503
Q24503
Q24503
Q24503
Q24503
Q24503
Q24503
Full ServIce Analylical Envlronmenlal Soluff one
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA Project ID Morehead Commons No Client Sample ID WS-1Attn Chris Ward
Prism Sample ID 184952Box7030SampleMatrixSoilCOCGroupG0607542CharlotteNC28241TimeCollected06/19/07 1600
Time Submitted 06/19/07 1735
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
9rcent Solids Determination
Percent Solids 83.3 SM2540 06/25/07 1745 Lthao
Sample Weight Determination
Weight Bisulfate 5.93
Weight Bisulfate 5.33
Weight Methanol 5.36
olatiIe Organic Compounds by GCMS
i11-Trichloroethane BRL mg/kg 0.0056 0.00032 8260B 06/23/07 1640 erussefl Q245031122-Tetrachloroethane BRL mg/kg 0.0056 0.00057 8260B 06/23/07 1640 erussell Q24503
ll2-Trichloroethane BRL mg/kg 0.0056 0.00035 8260B 06/23/07 1640 erussell Q24503
il-Dichloroethane BRL mg/kg 0.0056 0.00041 8260B 06/23/07 1640 erussell Q245o3ll-Dichloroethene BRL mg/kg 0.0056 0.00043 8260B 06/23/07 1640 erussell Q24503llDichloropropeneBRLmg/kg 0.0056 0.0005 8260B 06/23/07 1640 erussell Q245032S-Trichlorobenzene BRL mg/kg 0.0056 0.00062 8260B 06/23/07 1640 erussell
l23-Trichloropropane BRL mg/kg 0.0056 0.0005 8260B 06/23/07 1640 erussell
24-Trichlorobenzene BRL mg/kg 0.0056 0.00054 8260B 06/23/07 1640 erussell
2.4-Trimethyjbenzene BRL mg/kg 0.0056 0.00043 8260B 06/23/07 1640 erussell
l2-jibromoethane EDB BRL mg/kg 0.0056 0.0001 8260B 06/23/07 1640 erussell
2-Dichlorobenzene BRL mg/kg 0.0056 0.0003 8260B 06/23/07 1640 erussell
l2-Dichloroethane BRL mg/kg 0.0056 0.00056 8260B 06/23/07 1640 enjssell
2-Dichloropropane BRL mg/kg 0.0056 0.00042 8260B 06/23/07 1640 erussell
l35-Trimethylbenzene BRL mg/kg 0.0056 0.00047 82608 06/23/07 1640 erussell
3-Dichlorobenzene BRL mg/kg 0.0056 0.00048 8260B 06/23/07 1640 erussell
lS-Dichioropropane BRL mg/kg 0.0056 0.00038 8260B 06/23/07 1640 enjssefl
4-Dichlorobenzene BRL mg/kg 0.0056 0.00044 8260B 06/23/07 1640 erussell
2-Dichloropropane BRL mg/kg 0.0056 0.00028 8260B 06/23/07 1640 erussell Q24503-Chlorotojuene BRL mg/kg 0.0056 0.00042 8260B 06/23/07 1640 erussell Q245o3Thisreportshouldnotbereproducedexceptinitsentiretywithout the written consent of Prism Laboratories Inc449SpringbroojRoadP.O Box 240543 Charlotte NC 28224-0543Phone7041529-6364 Toll Free Number 1-8001529-6364 Fax 704/525-0409 Page of 35
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
ESP Associates PA Project ID Morehead Commons No Client Sample ID WS-1ALtnChrisWard
Prism Sample ID 184952Box 7030 Sample Matrix Soil COC Group G0607542CharlotteNC28241TimeCollected06/19/07 1600
Time Submitted 06/19/07 1735
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
2-Hexanone BRL mg/kg 0.056 0.00059 826DB 06/23/07 1640 erussell 024503
4-Chiorotoluene BRL mg/kg 0.0056 0.00029 826DB 06/23/07 1640 erussell Q24503
4-Methyl-2-pentanone MIBK BRL mg/kg 0.056 0.00056 826DB 06/23/07 1640 erussell 024503
Acetone BRL mg/kg 0.056 0.0022 826DB 06/23/07 1640 erusseH 024503
Benzene BRL mg/kg 0.0034 0.00045 826DB 06/23/07 1640 erusseH Q24503
Bromobenzene BRL mg/kg 0.0056 0.00039 826DB 06/23/07 1640 erussell 024503
Bromochioromethane BRL mg/kg 0.0056 0.00034 826DB 06/23/07 1640 erussell Q24503
I3romodjchloromethane BRL mg/kg 0.0056 0.0005 8260B 06/23/07 1640 erussell Q24503
Bromoform BRL mg/kg 0.0056 0.00042 82608 06/23/07 1640 erussell 024503
i3romomethane BRL mg/kg 0.011 0.00065 8260B 06/23/07 1640 erussell 024503
Carbon tetrachioride BRL mg/kg 0.0056 0.00033 826DB 06/23/07 1640 erussell 024503
Thlorobenzene BRL mg/kg 00056 0.00043 826DB 06/23/07 1640 enissell 024503
hIorodibromornethane BRL mg7kg 0.0056 0.00038 8260B 06/23/07 1640 eruiI 024503
Chloroethane BRL mg/kg 0.011 0.00046 8260B 06/23/07 1640 erussell
mloroform BRL mg/kg 0.0056 0.00042 8260B 06/23/07 1640 erussefi
Chloromethane BRL mg/kg 0.0056 0.00039 8260B 06/23/07 1640 erussell
is-l2-Djchloroethene BRL mg/kg 0.0056 0.00025 8260B 06/23/07 1640 erussell
cis-l3-Dichloropropene BRL mg/kg 0.0056 0.00036 82608 06/23/07 1640 ewssell
ichlorodifluoromethane BRL mg/kg 0.0056 0.0013 826DB 06/23/07 1640 erussell
Ethylbenzene BRL mg/kg 0.0056 0.00039 82608 06/23/07 1640 erussell
sopropyl ether IPE BRL mg/kg 0.0056 0.00019 8260B 06/23/07 1640 erussell
.sopropylbenzene BRL mg/kg 0.0056 0.00045 826DB 06/23/07 1640 erussell
ip-XyIenes BRL mg/kg 0.011 0.00079 826DB 06/23/07 1640 erussell
lethyl ethyl ketone MEK BRL mg/kg 0.11 0.D016 826GB D6/23/D7 1640 erussell
Methyl t-butyl ether MTBE BRL mg/kg 0.011 0.00033 82608 D6/23/D7 1640 erussell
ethylene chloride BRL mg/kg 0.0056 0.00046 826DB 06/23/07 1640 erussell
n-Butylbenzene BRL mg/kg 0.0056 0.00045 826DB 06/23/07 1640 erussell
024503
024503
024503
Q24503
024503
024503
024503
024503
Q24503
024503
024503
Q245D3
Q245D3
024503
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page of 35
Laboratory Report
06/29/07
Project ID Moreheaci Commons No Client Sample ID WS-1
Prism Sample ID 184952
Sample Matrix Soil COC Group G0607542
Time Collected 0611 9/07 1600
Time Submitted 06/1 9/07 1735
Sarvica Analytical Environ.._..........jon
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Repo MDL Dilution Method Analysis Analyst Batch
IDLimitFactorDate/Time
n-Propylbenzene BRL mg/kg 0.0056 0.00034 8260B
Naphthalene
o-Xylene
p-lsopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
06/23/07 1640 erussell
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
0.011
0.0056
0.0056
0.0056
0.0056
0.0056
0.0056
0.0056
0.0056
0.0056
Tetrachloroethene
Toluerie
trans-i 2-Dichloroethene
trans-i 3-Dichloropropene
0.00065
0.00034
0.00046
0.00037
0.00056
0.00035
0.00097
0.00038
0.00043
0.00039
8260B
8260B
82603
82603
8260B
8260B
8260B
8260B
8260B
8260B
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
1640 erussell
1640 erussell
1640 erussell
1640 erussell
1640 erussell
1640 erussell
1640 erussell
1640 erussell
1640 enJssefl
024503
024503
024503
Q24503
024503
024503
024503
024503
024503
024503
06/23/07 1640 erussell 024503
Tiichloroethene BRL mg/kg 0.0056 0.00034 82603 06/23/07 1640 erussefl 024503
Trichlorofltjrom-ethane BRL mg/kg 0.0056 0.00046 826DB 06/23107 1640 erussell Q24503
Vinyl acetate BRL mg/kg 0.028 0.0020 8260B 06/23/07 1640 erussell Q245o3
Vinyl chloride BRL mg/kg 0.0056 0.00072 826DB 06/23/07 1640 erussell 024503
Surrogate Recovery Control Limits
Bromofluorobenzene 92 77 128
Dibromofluoromethane 79 67 143
Toluene-d8 85 81 128
3emi-vojatjle organic Compounds by CC/MS
124-Trjchlorobenzene BRL
2-Dichlorobenzene BRL
3Dichlorobenze BRL
14Dichlorobenzene BRL
45-Trichlorophenol BRL
246-Trichloroplienol BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
0.39
0.39
0.39
0.39
0.39
0.39
0.039
0.029
0.028
0.036
0.040
0.038
8270C
8270C
8270C
8270C
8270C
8270C
06/26/07
06/26/07
06/26/07
06/26/07
06/26/07
06/26/07
1737 kcampigotto
1737 kcampigotto
1737 kcampigotto
1737 kcamplgotto
1737 kcampigotto
1737 kcampJgofto
Q24532
024532
024532
024532
Q24532
024532
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449Springbi-ooiç Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page 30135
Full ServIce AnalytIcal Envlronmentl y.....ons
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
WS-
184952
G0607542
06/19/07 1600
06/19/07 1735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
24-Dichlorophenol BRL mg/kg 0.39 0.033 8270C 06/26/07 1737 kcampigotto 024532
24-Dimethyiphenol BRL mg/kg 0.39 0.038 8270C 06/26/07 1737 kcampigotto 024532
24-Dinitrophenol BRL mg/kg 2.0 0.044 8270C 06/26/07 1737 kcampigotto 024532
24-Dinitrotoluene BRL mg/kg 0.39 0.022 8270C 06/26/07 1737 kcampigotto Q24532
26-Dinitrotoluerie BRL mg/kg 0.39 0.042 82700 06/26/07 1737 kcampigotto 024532
2-Chloronaphthalene BRL mg/kg 0.39 0.041 82700 06/26/07 1737 kcampigotto Q24532
2-Chlorophenol BRL mg/kg 0.39 0.031 8270C 06/26/07 1737 kcampigotto 024532
2-Methylnaphthalene BRL mg/kg 0.39 0.031 82700 06/26/07 1737 kcampigotto Q24532
2-Methyiphenol BRL mg/kg 0.39 0.037 8270C 06/26/07 1737 kcampigotto 024532
2-Nitrophenol BRL mg/kg 0.39 0.047 8270C 06/26/07 1737 kcarnpigotto Q24532
.34-Methylphenol BRL mg/kg 0.39 0.040 82700 06/26/07 1737 kcampjgotto 024532
33-Dichlorobenzidine BRL mg/kg 0.79 0.025 8270C 06/26/07 1737 kcampigotto 024532
lSDinitro2methylpher1ol BRL ng/k 2.0 D.024 82700 06/26/07 1737 kbampigotto Q24532
4-Bromophenylphenylether BRL mg/kg 0.39 0.037 82700 06/26/07 1737 kcampigotto 024532
J-Chloro-3-methylphenol BRL mg/kg 0.79 0.029 8270C 06/26/07 1737 kcampigotto 0245324-Chloroaniljne BRL mg/kg 0.39 0.050 8270C 06/26/07 1737 kcampigotto Q24532ChiorophenylphenyletheBRLmg/kg 0.39 0.024 82700 06/26/07 1737 kcampigotto 024532NitrophenolBRLmg/kg 2.0 0.026 8270C 06/26/07 1737 kcampigofto 024532cenaphtheneBRLmg/kg 0.39 0.039 8270C 06/26/07 1737 kcampigotto 024532i-cenaphthylene BRL mg/kg 0.39 0.039 827oc 06/26/07 1737 kcampigotto Q24532AnthraceneBRLmg/kg 0.39 0.030 82700 06/26/07 1737 kcampigotto 024532zobenzeneBRLmg/kg 2.0 0.036 8270C 06/26/07 1737 kcampigofto 024532Benzoaanthracene0.31 mg/kg 0.39 0.055 8270C 06/26/07 1737 kcampigotto 024532enzoapyrene0.32 mg/kg 0.39 0.046 82700 06/26/07 1737 kcampigotto Q24532Benzobfluoranthene0.45 mg/kg 0.39 0.018 270C 06/26/07 1737 kcampigotto Q24532nzoghiperyIene0.22J mg/kg 0.39 0.019 82700 06/26/07 1737 kcampigotto 024532Benzokfluoranthene0.27 mg/kg 0.39 0.032 82700 06/26/07 1737 kcampigotto 024532
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrooRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page of 35
NC CertificaUori No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
.P Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS--1
184952
G0607542
0611 9/07 1600
0611 9/07 1735
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Benzoic acid BRL mg/kg 2.0 0.17 8270C 06/26/07 1737 kcampigotto Q24532
06/26/07 1737 kcampigotto Q24532
06/26/07 1737 kcampigotto 024532
06/26/07 1737 kcampgotto Q24532
06/26/07 1737 kcampigotto Q24532
06/26/07 1737 kcampigotto 024532
06/26/07 1737 kcampigotto Q24532
06/26/07 1737 kcampigotto 024532
06/26/07 1737 kcampigotto 024532
06/26/07 1737 kcampigotto 024532
06/26/07 1737 kcampigotto 024532
t3enzyl alcohol BRL mg/kg 0.79 0.042 82700
3is2-chloroethoxymethane BRL mg/kg 0.39 0.045 8270C
3is2-chloroethylether BRL mg/kg 0.39 0.043 82700
Bis2.chloroisopropylether BRL mg/kg 0.39 0.034 82700
$is2-ethylhexylphthalate BRL mg/kg 0.39 0.019 82700
Butylbenzylphthalate BRL mg/kg 0.39 0.024 8270C
hrysene 0.37J mg/kg 0.39 0.066 8270C
Di-n-butylphthalate BRL mg/kg 0.39 0.018 82700
i-n-octylphthalate BRL mg/kg 0.39 0.029 8270C
Jibenzoahanthracene BRL mg/kg 0.39 0.040 8270C
uibenzofuran BRL mg/kg 0.39 0.034 8270C 06/26/07 1737 kcampigotto 024532
ethylhthalate BRL mg/kg 0.39 0.024 82700 36/26/07 1737 kampigotto Q24532
Dimethylphthalate BRL mg/kg 0.39 0027 82700 06/26/07 1737 kcampigouo 024532
luoranthene 0.65 mg/kg 0.39 0.027 82700 06/26/07 1737 kcampigoo Q24532FluoreneBRLmg/kg 0.39 0.023 82700 06/26/07 1737 kcampigotto Q24532exachlorobenzeneBRLmg/kg 0.39 0.020 8270C 06/26/07 1737 kcamp9oo Q24532HexachlorobutadieneBRLmg/kg 0.39 0.038 82700 06/26/07 1737 kcampigouo 024532
exachlorocyclopentadiene BRL mg/kg 0.39 0.042 82700 06/26/07 1737 kcampigotto 024532
nexachioroethane BRL mg/kg 0.39 0.040 82700 06/26/07 1737 kcampigouo 024532deno123-cdpyrene 0.39 mg/kg 0.39 0.040 8270C 06/26/07 1737 kcampigotto 024532phoroneBRLmg/kg 0.39 0.035 8270C 06/26/07 1737 kcampigotto 024532
N-Nitrosodinpropylamine BRL mg/kg 0.39 0.045 82700 06/26/07 1737 kcampigotto 024532
Nitrosodiphenyjamine BRL mg/kg 0.39 0.020 82700 06/26/07 1737 kcampigotto 024532NaphthaleneBRLmg/kg 0.39 0.043 82700 06/26/07 1737 kcampigotto 024532robenzeneBRLmg/kg 0.39 0.038 82700 06/26/07 1737 kcampgouo 024532PeritachiorophenolBRLmg/kg 2.0 0.033 82700 06/26/07 1737 kcampigotto 024532
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrooçRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-800/529.6364 Fax 704/525-0409 Page of 35
Parameter Result Units Repo MDL Dilution Method Analysis Analyst Batch
Phenol BRL mg/kg 0.39 0.043 8270C 06/26/07 1737 kcampigouo 024532Pyrene0.58 mg/kg 0.39 0.027 82700 06/26/07 1737 kcampigouo Q24532
30.1 mL 3550B 06/22/07 1100 dpope P18710
Surrogate Recovery
246-Tribromophenol 102
2-Fluorobiphenyl 84
2-Fluorophenol 66
Nitrobenzene..d5 71 14-103
Phenol-d5 77 13-95
Terphenyl-di4 100 41 136
jEjtractabIe Petroleum Hydrocarbons by GC-FID
Cll-C22Aromatjcs 13 mg/kg 12 6.4
C19-C36Aliphatics BRL mg/kg 12 1.8
C9-Cl8Aljphatics BRL mg/kg 12 3.8
Analysis Note for Cll-C22 Aromatjcs
Sample Preparation
mL EPH 06/21/07 800 grappaccioji P18703
Surrogate Recovery Control Limits
o-Terphenyl 76 40 140
l-Chloro-octadecane 108 40 140
2-Bromonaphthalene 86 40 140
2-Fluorobiphenyl 88 40 140
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringjrOORoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-800/529.6364 Fax 704/525.0409
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Ice Analylftal EnvIronmcraj
ESP Associates PA
Attn Chris Ward
BOX 7030
Charlotte NC 28241
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID WS1
Prism Sample ID 184952SampleMatrixSoilCOCGroupG0607542
Time Collected 06/19/07
Time Submitted 06/19/07
1600
1735
Sample Preparation
Control Limits
25-123
21 -108
14-89
MADEP EPH
MADEP EPH
MADEP EPH
Adjusted value
10.2g
06/23/07 2303 grappaccjojj
06/23/07 2303 grappaccjoj
06/23/07 2303 grappaccioli
024514
024514
Q24514
MfsblCp
hromium
ead
29 mg/kg
48 mg/kg
0.27 0.016
0.27 0.022
6010B
6010B
06/25/07 1332 mcampbell
06/26/07 1332 mcampbell
Q24519
024519
Page of 35
99012 Laboratory ReportNCDrinkingWaterCertNo37735
06/29/07
Project ID Morehead Commons No Client Sample ID WS-1
Prism Sample ID 184952SampleMatrixSoilCOCGroupG0607542CharlotteNC28241
Time Collected 06/1 9/07 1600
Time Submitted 06/1 9/07 1735
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID---
Sample Preparation
2.25 50 mL 305DB 06/21/07 905 jhoppel P18702YitilePetroleumHydrocarbonsbyGC-pIp/I
C5-C8Aliphatics BRL mg/kg 6.0 1.2 MADEP VPH 06/27/07 712 hwagner Q24582C9-C10 Arornatics BRL mg/kg 6.0 0.036 MADEP VPH 06/27/07 712 hwagner Q24582C9-C12 Aliphatics BRL mg/kg 6.0 1.8 MADEP VPH 06/27/07 712 hwagner Q24582AnalysisNoteforC5-C8 Aliphatjcs Adjusted valueAnalysisNoteforC9-Cl2 Aliphatics Adjusted value
Surrogate Recovery Control Limits
25-DibromotolueneFjD 116 70 130
25-DibromotoIuenepi 91 70 130
9arjJIe Weight Determination
Veight --19.05 --MADEP VPH 06/26/07 000 brownVVeight219.91 MADEP VPH 06/26/07 000 brown
RL Below Reporting Limit
J-Estimated value between the Reporting Limit and the MDLT17eresultsin this report relate only to the samples submitted for analysis and meet state certification requirements other than
ELAC certification except for those instances indicated in the case narrative and/or test commentsIIresultsarereportedondly-weight basis
gela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety Without the written consent of Prism Laboratories Inc449SpringbroojçRoadP.O Box 240543 Charlotte NC 28224-0543Phone7O4/5296364 Toll Free Number 1-8OO/5296364 Fax 704/525-0409
ESP Associates PA
Attn Chris Ward
Box 7030
Page 7of35
Laboratory Report
06/29107
Project ID Morehead Commons No Client Sample ID WS2
Prism Sample ID 184953SampleMatrixSoilCOCGroupG0607542
Time Collected 06/19/07 1615
Time Submitted 06/19/07 1735
06/23/07 1712 erusselp
06/23/07 1712 erussell
06/23/07 1712 erussell
06/23/07 1712 en.jsselI
06/23/07 1712 erussefi
06/23/07 1712 erussell
06/23/07 1712 erussell
06/23/07 1712 erusseji
06/23/07 1712 erussejl
06/23/07 1712 erusseli
06/23/07 1712 erusseli
06/23/07 1712 erussetl
06/23/07 1712 erussefi
06/23/07 1712 erussell
06/23/07 1712 erusseli
Q245o3
024503
024503
Q24503
Q245o3
Q24503
024503
024503
024503
Q24503
024503
Q245o3
Q24503
Q24503
024503
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Date/Time ID
Percent Solids 743 SM2540 06/25/07 1745 Lthao
Sample Weight Determination
Weight Bisulfate
Weight Bisulfate
Weight Methanol
6.32
6.40
5.54
5035
5035
5035
06/27/07
06/27/07
06/27/07
000 brown
000 brown
000 brown
Volatile Organjc Compounds by GC/MS
lll-Trichloroethane BRL mg/kg 0.0053 0.00029 8260B 06/23/07 1712 erusseu 024503ll22-Tetrachloroethane BRL mg/kg 0.0053 0.00054 82606 06/23/07 1712 erussefl 024503112-Trichloroethane BRL mg/kg 0.0053 0.00033 8260B 06/23/07 1712 erussell 024503i.l-Dichloroethane BRL ng/kg 0.0053 0.00038 8260B 06/23/07 1712 erusseli Q245o3l-Dichleroethene BRL mg/kg 0.0053 0.0004 8260B 06/23/07 1712 erussell 024o3l.lDichIoropropene BRL mg/kg 0.0053 0.00046 8260B
23-Trichlorobenzene BRL mg/kg 0.0053 0.00058 8260B
l.23-Trichloropropane BRL mg/kg 0.0053 0.00046 8260B
24-Trichlorobenzene BRL mg/kg 0.0053 0.0005 8260B
24-Trimethylbenzene 0.0023 .J mg/kg 0.0053 0.0004 8260B
l2-Dibromoethane EDB BRL mg/kg 0.0053 0.000095 826GB
2-Dichlorobenzene BRL mg/kg 0.0053 0.00028 826GBl2-BRL mg/kg 0.0053 0.00053 8260B
2-Dichloropropane BRL mg/kg 0.0053 0.00039 8260B
l.35-Trimethyjbenzene BRL mg/kg 0.0053 0.00044 8260B
3-Dichjorobenzene BRL mg/kg 0.0053 0.00045 826GB
l3-Dichloropropane BRL mg/kg 0.0053 0.00036 826GB
4-Dichlorobenzene BRL mg/kg 0.0053 0.00041 8260B
..2-Dichloropropane BRL mg/kg 0.0053 0.00026 82606
-ChlorotoIuene BRL mg/kg 0.0053 0.00039 826GB
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbroORoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-800/529.6364 Fax 704/525-0409 Page of 35
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID WS2
Prism Sample ID 184953SampleMatrixSoilCOCGroupG0607542
Time Collected 06/1 9/07 1615
Time Submitted 06/1 9/07 1735
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
2-Hexanone BRL mg/kg 0.053 0.00055 8260B 06/23/07 1712 erussell Q245034-Chiorotoluene BRL mg/kg 0.0053 0.00027 8260B 06/23/07 1712 erussell Q24503
4-Methyl-2-pentanone MIBK BRL mg/kg 0.053 0.00053 8260B 06/23/07 1712 erussell Q24503AcetoneBRLmg/kg 0.053 0.0021 8260B 06/23/07 1712 erussell 024503BenzeneBRLmg/kg 0.0032 0.00042 8260B 06/23/07 1712 erussell 024503BromobenzeneBRLmg/kg 0.0053 0.00037 8260B 06/23/07 1712 erussell 024503BromochloromethaneBRLmg/kg 0.0053 0.00032 826DB 06/23/07 1712 erussell Q24503BromodichioromethaneBRLmg/kg 0.0053 0.00046 82608 06/23/07 1712 erussell Q24503l3romoformBRLmg/kg 0.0053 0.00039 82608 06/23/07 1712 erussell 024503I3romomethaneBRLmg/kg 0.011 0.00061 8260B 06/23/07 1712 erussell Q245o3Ca bon tetrachioride BRL mg/kg 0.0053 0.0003 8260B 06/23/07 1712 erussell Q24503hlorobenzeneBRLmg/Kg 0.0053 0.0004 8260B 0f23/07 1712 erussell 024503hlorodibromometae-BRL mg/kg 0.0053 0.00036 8260 b6/23107 1712 erussell Q24503Chloroethane
hloroforrn
Chloromethane
is-I 2-Dichjoroethene
cis-i 3-Dichloropropene
ichIorodifluoromethane
_thylbenzene
opropyI ether IPE
opropylbenzene
mp-Xylenes
ethyl ethyl ketone MEK
Methyl t-butyl ether MTBE
ethylene chloride
n-Butylbenzene
BRL
BRL
BRL
BRL
BRL
BRL
0.0047J
BRL
BRL
0.0034
BRL
BRL
BRL
BRL
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
0.011 0.00043
0.0053 0.00039
0.0053 0.00037
0.0053 0.00023
0.0053 0.00034
0.0053 0.0012
0.0053 0.00037
0.0053 0.00018
0.0053 0.00042
0.011 0.00074
0.11 0.0015
0.011 0.0003
0.0053 0.00043
0.0053 0.00042
1712
1712
1712
1712
1712
1712
1712
1712
1712
1712
erussell
erussell
erussell
erusset
erussell
erussefi
erussefi
erussell
erussell
erussefl
82608
826DB
826DB
826DB
826DB
826DB
826DB
826DB
8260B
8260B
8260B
826DB
826DB
8260B
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
Q24503
024503
024503
024503
024503
Q24503
024503
024503
024503
024503
024503
Q24503
024503
024503
1712 erusseu
1712 erusseli
1712 erussefi
1712 erusselj
Thi report should not be reproduced except in its entirety Without the written consent of Prism Laboratories Inc449SpringbroojRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page of 35
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 184953SampleMatrixSoilCOCGroupG0607542
Time Collected 06/1 9/07 1615
Time Submitted 06/1 9/07 1735
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
nDropylbenzene BRL mg/kg 0.0053 0.00032 82608 06/23/07 1712 erussell 024503Naphthalene0.0049J mg/kg 0.011 0.00061 8260B 06/23/07 1712 enjssell Q24503
o-Xylene BRL mg/kg 0.0053 0.00032 826DB 06/23/07 1712 erusset 024503
.p-lsopropyltoluene BRL mg/kg 0.0053 0.00043 826DB 06/23/07 1712 erussefl Q24503
sec-Butylbenzene BRL mg/kg 0.0053 0.00035 826DB 06/23/07 1712 erussell Q24503
Styrene BRL mg/kg 0.0053 0.00053 8260B 06/23/07 1712 erussell 024503
eri-Butylbenzene BRL mg/kg 0.0053 0.00033 82608 06/23/07 1712 enIssell 024503
leirachloroethene BRL mg/kg 0.0053 0.0009 8260B 06/23/07 1712 erussell 024503Toluene0.0082 mg/kg 0.0053 0.00036 8260B 06/23/07 1712 erussell 024503rans-12Dichloroethene BRL mg/kg 0.0053 0.0004 826DB 06/23/07 1712 erussell 024503
ransl3Dichloropropene BRL mg/kg 0.0053 0.00037 826DB 06/23/07 1712 erusset Q245o3TrichloroetheneBRLmg/kg 0.0053 0.00032 826DB 06/23/07 1712 erussell 024503richIorofluoronjhflBRTLmg/kg 0.0053 0.00043 8260B 06/23/07 1712 erussell Q24503VinylacetateBRLmg/kg 0.026 0.0019 82608 06/23/07 1712 erussell 024503inylchlorideBRLmg/kg 0.0053 0.00067 826DB 06/23/07 1712 erussell 024503
Full SeMceAnaIytI_...Ironmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
Surrogate Recovery Control Limits
Bromofluorobenzene 82 77 128
Dibrornofluoromethane 68 67 143
Toluene-d8 83 81 128
sinii-volatjle Organic compounds by GC/MS
24-Trichlorobenzene BRL mg/kg 0.44 0.044 8270C 06/26/07 1826 kcampigouo 0245322-Dichlorobenzene BRL mg/kg 0.44 0.033 8270C 06/26/07 1826 kcampigotto 024532-Dichlorobenzene BRL mg/kg 0.44 0.032 827DC 06/26/07 1826 kcampigoao 024532BRLmg/kg 0.44 0.040 827DC 06/26/07 1826 kcampigotto 024532I.STrichIorophenoI BRL mg/kg 0.44 0.045 8270C 06/26/07 1826 kcampigouo 024532246-Trichlorophenol BRL mg/kg 0.44 0.043 8270C 06/26/07 1826 kcampigofto 024532
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbroRoad P.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page 10 of 35
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
BOX 7030
Charlotte NC 28241
Laboratory Report
0612 9107
Project ID Morehead Commons No Client Sample ID WS-2
Prism Sample ID 184953SampleMatrixSoilCOOGroupG0607542
Time Collected 06/19/07 1615
Time Submitted 06/19/07 1735
Parameter Result Units Repo MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
24-DichloropherioJ BRL mg/kg 0.44 0.037 8270C
24-Dimethylphenol BRL mg/kg
24-Dinitrophenol BRL mg/kg
24-Dinitrotoluene BRL mg/kg
26-Djnitj-otojuene BRL mg/kg
2Chloronaphthalene BRL mg/kg
2ChJorophenol BRL mg/kg
2-Methylnaphthalene BRL mg/kg
2-Methylphenol BRL mg/kg
2-Nitrophenol BRL mg/kg
34-Methylphenol BRL mg/kg
Q2453233-Dichlorobenzjdjne BRL mg/kg 0.89 0.028 8270C /26/07 1826 Ca1pigotto 0245324Ł-DinfromethyIphenof BRL mg/kb 2.2 0.07 8270C O6/207 1826 kcmpigcuo 024532
06/26/07 1826 kcampigotto Q24532
0.44 0.043 8270C 06/26/07 1826 koampigotto Q24532
2.2 0.050 82700 06/26/07 1826 kcampigotto 024532
0.44 0.025 8270C 06/26/07 1826 kcampigotto Q24532
0.44 0.047 8270C 06/26/07 1826 kcampigotto 024532
0.44 0.046 8270C 06/26/07 1826 kcampigotto Q24532
0.44 0.035 82700 06/26/07 1826 kcampigotto 024532
0.44 0.035 82700 06/26/07 1826 kcampigotto Q24532
0.44 0.042 82700 06/26/07 1826 kcampigotto Q24532
0.44 0.053 8270C 06/26/07 1826 kcampigotto 024532
0.44 0.045 8270C 06/26/07 1826 kcampigotto
4-Bromophenylphenylether
I-Chloro3methyphenol
4-Chloroanjline
kChlorophenylphenylether
4-Nitrophenol
cenaphthene
cenaphthylene
Anthracene
zobenzene
Benzoaanthracene
anzoapyrene
Benzobfluoranthene
nzoghiperyIene
Benzokfluorantliene
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
0.22J
0.20
0.30
0.12J
0.15J
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
0.44
0.89
0.44
0.44
2.2
0.44
0.44
0.44
2.2
0.44
0.44
0.44
0.44
0.44
0.042
0.033
0.057
0.027
0.029
0.044
0.044
0.034
0.041
0.062
0.051
0.020
0.021
0.036
06/26/07
06/26/07
06/26/07
06/26/07
06/26/07
06/26/07
06/26/07
06/26/07
06/26/07
06/26/07
06/26/07
82700
8270C
8270C
8270C
8270C
82700
8270C
8270C
82700
82700
8270C
82700
8270C
8270C
1826 kcampigotto
1826 kcampigotto
1826 kcampigotto
1826 kcampigotto
1826 kcampigotto
1826 kcampigotto
1826 kcampigotto
1826 kcampigouo
1826 kcampigotto
1826 kcampigotto
1826 kcampigotto
024532
024532
Q24532
024532
024532
024532
024532
024532
024532
024532
Q24532
024532
Q24532
Q24532
06/26/07 1826 kcampigotto
06/26/07 1826 kcampigotto
06/26/07 1826 kcampigotto
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529.6364 Toll Free Number 1-800/529.6364 Fax 704/525.0409 Page 11 of 35
WS-2
184953
G0607542
06/19/07
06/19/07
1615
1735
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
F..Service AnaIyticl Environmntai
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Repo MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Benzoicacid BRL mg/kg 2.2 0.19 8270C 06/26/07 1826 kcampigotto 024532
Benzyl alcohol BRL mg/kg 0.89 0.047 8270C
..Bis2-chloroethoxymethane BRL mg/kg 0.44 0.051 82700
.Bis2-chloroethylether BRL mg/kg 0.44 0.048 8270C
Bis2-chloroisopropylether BRL mg/kg 0.44 0.038 82700
Bis2ethylhexylphthaIat BRL mg/kg 0.44 0.022 8270C
Butylbenzylphthalate BRL mg/kg 0.44 0.027 82700
Chrysene 0.24 mg/kg 0.44 0.074 8270C
BRL mg/kg 0.44 0.020 827CC
BRL mg/kg 0.44 0.033 82700
06/26/07
06/26/07
06/26/07
06/26/07
06/26/07
06/26/07
06/26/07
06/26/07
06/26/07
Di-n-butylphthalate
Di-n-octylphthalate
Jibenzoahanthracene BRL mg/kg 0.44 0.045
Dibenzofuran BRL mn/kr fl 11 AflQQ
1826 kcampigotto 024532
1826 kcampigotto 024532
1826 kcampigotto Q24532
1826 kcampigotto 024532
1826 kcampigotto Q24532
1826 kcampigotto 024532
1826 kcampigotto Q24532
1826 kcampigotto 024532
1826 kcampigotto Q24532
1826 koampigotto Q245328270C06/26/07
IIULQ
iethylphthalate BRL mg/kg 0.44 0.027 8270C 06/26/07 1826 kcampigouo 024532
Dimethylphthalate BRL mg/kg 0.44 0.030 82700 06/26/07 1826 kcampigotto 024532uoranthene0.65 mg/kg 0.44 0.031 8270C 06/26/07 1826 kcampigotto 024532FluoreneBRLmg/kg 0.44 0.026 82700 06/26/07 1826 kcampigotto 024532lexachlorobenzeneBRLmg/kg 0.44 0.023 82700 06/26/07 1826 kcampigotto 024532HexachlorobutadieneBRLmg/kg 0.44 0.043 827CC 06/26/07 1826 kcampgotto 024532
exachiorocyclopentadjene BRL mg/kg 0.44 0.047 82700 06/26/07 1826 kcampigotto 024532dexachloroethaneBRLmg/kg 0.44 0.045 82700 06/26/07 1826 kcampigotto 0245321deno123cdpyrene0.32 mg/kg 0.44 0.046 827CC 06/26/07 1826 kcampigotto 024532ophoroneBRLmg/kg 0.44 0.040 827CC 06/26/07 1826 kcamplgotto Q24532N-Nitrosodi.n.propylamine BRL mg/kg 0.44 0.050 827CC 06/26/07 1826 kcampigotto 024532-Nitrosodiphenyjamine BRL mg/kg 0.44 0.023 82700 06/26/07 1826 kcampjgotto 024532NaphthaleneBRLmg/kg 0.44 0.048 82700 06/26/07 1826 kcampjgouo Q24532trobenzeneBRLmg/kg 0.44 0.043 8270C 06/26/07 1826 kcampigotto Q24532PentachlorophenolBRLmg/kg 2.2 0.037 82700 06/26/07 1826 kcampigotto 024532
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525.0409 Page 12 of 35
ESP Associates PA Project ID Morehead Commons No Client Sample ID WS-2Attn Chris Ward Prism Sample ID 184953Box7030SampleMatrixSoilCOCGroupG0607542CharlotteNC28241TimeCollected06119/07
Time Submitted 06/1 9/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID-.-..-.Phenanthrene 0.35 mg/kg 0.44 0.022 8270C 06/26/07 1826 kcampigotto Q24532
Phenol BRL mg/kg 0.44 0.048 8270C 06/26/07 1826 kcampigotto Q24532
Pyrene 0.63 mg/kg 0.44 0.030 8270C 06/26/07 1826 kcampigotto Q24532
Sample Preparation 29.98 mL
Surrogate Recovery Control Limits
246-Tribromophenol 94 25-123
2-Fluorobiphenyl 81 21 108
2-Fluorophenot 54 14 89
Nitrobenzene-d5 64 14 103
Phenol-d5 73 13-95
Terphenyl-d14 1Q3 41 136
Extractable Petroleum Hydrocarbons by GC-FlD
Cll-C22Aromatics BRL mg/kg 13 7.1
.19-C36Atiphatjcs BRL mg/kg 13 2.0
C9-Cl8Aliphatics BRL mg/kg 13 4.2
Surrogate Recovery Control Limits
l-Chloro-octadecane 116 40-140
2-Bromonaphthalene 97 40 140
2-Fluorobiphenyl 99 40 140
o-Terphenyl 86 40-140
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrooiçRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
NC Certification No 402AlSCCertificationNo99012
NC Drinking Water Cert No 37735
Full Sarvice Analytical Envlronmnnlal Solutions
Laboratory Report
06/29/07
1615
1735
3550B 06/22/07 1100 dpope 18710
Analysi5 Note for Cll-C22 Aromatics
Sample Preparation
MADEP EPH
MADEP EPH
MADEP EPH
06/24/07 047 grappaccioj
06/24/07 047 grappaccioli
06/24/07 047 grappaccjoli
Adjusted value
10.26 mL EPH
024514
024514
Q24514
06/21/07 800 grappaccjofl P18703
MsyjCP
hromium 28 mg/kg .0.31
37 mg/kg 0.31
0.019
0.026
6010B
6010B
06/25/07 1339 mcampbejl
06/25/07 1339 mcampbejj
024519
024519
Page 13 of 35
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Sample Preparation
Volatile Petroleum Hydrocarbons by GC-PlDIFlDC5C8AliphaticsBRL
C9-C1Q Aromatics
C9-C1 Aliphatics
Analysis Note for C5-C8 Aliphatjcs Adjusted valueAnalysisNoteforC9-C12 Aliphatjcs Adjusted value
ngela Overcash V.P Laboratory Services
Laboratory Report
WS-2
184953
G0607542
06/19/07
06/19/07
06/29/07
teivlcsAnaIytuIEpronmsn Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected 1615
Time Submitted 1735
Parameter Result Units Repo MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
2.16 50 mL 3050B 06/21/07 905 jhoppel P18702
mg/kg 6.7 1.3 MADEP VPH 06/27/07 755 hwagner Q24582
BRL mg/kg 6.7 0.040 MADEP VPH 06/27/07 755 hwagner Q24582
BRL mg/kg 6.7 2.1 MADEP VPH 06/27/07 755 hwagner Q24582
Surrogate Recovery Control Limits
25-DibromotolueneFlD 114 70 130
25-Dibromotojuenep 89 70 130
SarnDle Weight Determination
/VØight 16 4ADEP VH 06/26/07 000 Ibron
Weight 19.20 MADEP VPH 06/26/07 000 brown
JRL Be/ow Reporting Limit
Estimated value between the Reporting Limit and the MDLheresultsin this report relate only to the samples submitted for analysis and meet state certification requirements other than
ELAC certification except for those instances indicated in the case narrative and/or test commentsIlresultsarereportedondry-weight basis
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone70415296364TollFreeNumber1-800/529-6364 Fax 704/525-0409 Page 14 of 35
--
Full Servlc Ansi ...nvtronmnnIaJ Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
.23-Trichlorobenzene
23-Trichloropropane
l24-Trichlorobenzene
2.4-Trimethyjbenzene
2-Dibromoethaj EDB
2-Dichlorobenzene
2-Dichloroethare
2-Dichloropropane
l35TrimethyIbenzene
3-Dichlorobenzer
-Dichloropropane
4-Dichlorobenzene
-DichIoropropane
-Chiorotoluene
5.49
5.69
5.01
BRL mg/kg
BRL mg/kg
BRL mg/kg
BRL mg/kg
BRL mg/kg
SRI mg/kg
SRI mg/kg
BRL mg/kg
BRL mg/kg
BRL mg/kg
BRL mg/kg
BRL mg/kg
BRI mg/kg
SRI mg/kg
0.0053 0.00059
0.0053 0.00047
0.0053 0.00051
0.0053 0.00041
0.0053 0.000096
0.0053 0.00029
0.0053 0.00053
0.0053 0.00039
0.0053 0.00045
0.0053 0.00046
0.0053 0.00036
0.0053 0.00042
0.0053 0.00027
0.0053 0.00039
5035
5035
5035
06/23/07 2021
06/23/07 2021
Q24503
Q24503
024503
024503
024503
Q24503
024503
Q24503
024503
Q24503
Q24503
024503
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 184954SampleMatrixSoilCOCGroupG0607542
Time Collected 06/19/07
Time Submitted 06/19/07
1630
1735
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time IDPercentSolidsDetermination
Percent Solids 82.4 SM2540 06/25/07 1745 Lthao
SamIe Weight Determination
Weight Bisulfate
Weight Bisulfate
Neight Methanol
06/27/07 000 Ibrown
06/27/07 000 Ibrown
06/27/07 000 Ibrown
/olatile Organic Compounds by GcIIVJS
l-Trichloroethane BRL mg/kg 0.0053 0.0003 8260B 06/23/07 2021 erusseli Q2450311.22-Tetrac-iloroethane BRI mg/kg 0.0053 0.00054 8260B 06/23/07 2021 erussell 0245032-TrichIoroeth BRL mg/kg 0.0053 0.00033 8260B 06123/07 2021 erussell 024503l-.Dichloroethane BRL mg/kg 0.0053 0.00038 8260B 06/23/07 2021 erussell Q245031DIchIoroetheBRLmg/kg 0.0053 0.00041 8260B 06/23/07 202 Łrussell 024503l-DichIoroprope BRL mg/kg 0.0053 0.00047 82608 06/23/07 2021 erussell 024503
8260B 06/23/07 2021 erussell
8260B 06/23/07 2021 erussell
82605 06/23/07 2021 erussell
8260B 06/23/07 2021 erussell
826GB 06/23/07 2021 erussell
826GB 06/23/07 2021 erussefi
8260B 06/23/07 2021 erussell
8260B 06/23/07 2021 erussell
8260B 06/23/07 2021 erusseji
82608 06/23/07 2021 erussell
8260B 06/23/07 2021 erussell
826GB 06/23/07 2021 erussell
8260B
826GB
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbroORoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
erussell
erussejf
024503
Q24503
Page 15of35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
O.Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 184954
Sample Matrix Soil COC Group G0607542
Time Collected 06/19/07
Time Submitted 06/19/07
1630
1735
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
4-Chlorotoluene BRL mg/kg 0.0053 0.00028 82608 06/23/07 2021 erussell Q24503
-4-Methyl-2-pentanone MIBK BRL mg/kg 0.053 0.00053 826DB 06/23107 2021 erussell 024503
Acetone BRL mg/kg 0.053 0.0021 82608 06/23107 2021 erusseil 024503
BRL mg/kg 0.0032 0.00043 8260B 06/23/07 2021 erussell Q24503
BRL mg/kg 0.0053 0.00037 826DB 06/23/07 2021 erusseii 024503
BRL mg/kg 0.0053 0.00032 826DB 06/23/07 2021 erussell Q24503
BRL mg/kg 0.0053 0.00047 82608 06/23/07 2021 erusseli Q24503
BRL mg/kg 0.0053 0.00039 8260B 06/23/07 2021 erusseli 024503
BRL mg/kg 0.011 0.00062 826DB 06/23/07 202 erussell Q245D3
BRL mg/kg 0.0053 0.00031 82608
E3enzene
3rornobenzene
Bromochioromethane
3romodichloromethane
Eromoform
3romorn ethane
.2arbon tetrachjoride
06/23/07 2021 erusseli 024503hIorobenzeneBRLmg/kg 0.0053 0.00041 826DB 06/23/07 2021 erusseH Q245D3hloiodibromomethaneBRLmg/kg W0053 000036 82608 06/23/07 2021 ruŒll Q2403
06/23/07 2021 erussell
Chloroethane
hloroform
Chioromethane
s-I 2-Dichloroethene
cia-I 3-Dichloropropene
chlorodifluoromethane
.thylbenzene
9propyl ether IPE
propylbenzene
rnp-Xylenes
thyl ethyl ketone MEK
Methyl t-butyl ether MTBE
tthylene chloride
fl-Butylbenzene
BRL
BRL
SRI
BRL
BRL
BRL
BRI
BRL
BRL
BRL
BRL
BRL
BRL
BRL
0.011
0.0053
0.0053
0.0053
0.0053
0.0053
0.0053
0.0053
0.0053
0.011
0.11
0.011
0.00044
0.00039
0.00037
0.00023
0.00034
0.0012
0.00037
0.00018
0.00043
0.00075
0.0015
0.00031
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
8260B
826DB
8260B
826DB
826DB
826DB
826DB
826DB
82608
826DB
826DB
826DB
82608
82608
06/23/07 2021
06/23/07 2021
06/23/07 2021
06/23/07 2021
06/23/07 2021
06/23/07 2021
06/23/07 2021
06/23/07 2021
06/23/07 2021
06/23/07 2021
06/23/07 202
06/23/07 2021
06/23/07 2021
enJsselI
erussell
erussejl
erusseli
erussell
erussell
erussell
erusseli
erussell
erussell
erussell
erussell
erussell
Q24503
024503
Q24503
024503
024503
024503
Q24503
024503
Q24503
024503
024503
024503
024503
024503
0.0053
0.0053
0.00044
0.00043
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbroRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 IoU Free Number 1-800/529-6364 Fax 704/525-0409 Page 16 0135
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time io
i-Propylbenzene BRL mg/kg 0.0053 0.00032 8260B 06/23/07 2021 erussell 024503Japhthalene0.013 mg/kg 0.011 0.00062 8260B 06/23/07 2021 erussell Q24503cs-Xylene BRL mg/kg 0.0053 0.00032 8260B 06/23/07 2021 erussell 024503
-lsopropyltoluene BRL mg/kg 0.0053 0.00044 8260B 06/23/07 2021 erussefl 024503sec-Butylbenzene BRL mg/kg 0.0053 0.00035 8260B 06/23/07 2021 erussefl 024503$tyrene 0.0022 mg/kg 0.0053 0.00053 8260B 06/23/07 2021 erussell 024503tert-Butylbenzene BRL mg/kg 0.0053 0.00033 8260B 06/23/07 2021 erussell 024503etrachloroetheneBRLmg/kg 0.0053 0.00092 8260B 06/23/07 2021 erussefi 024503okiene0.0044 mg/kg 0.0053 0.00036 8260B 06/23/07 2021 erussell Q24503ans-1 2-Dichloroethene BRL mg/kg 0.0053 0.00041 8260B 06/23/07 2021 erusseH Q24503ans-1 3-Dictiloropropene BRL mg/kg 0.0053 0.00037 8260B 06/23/07 202 erussell 024503TrichioroetheneBRLmg/kg 0.0053 0.00032 8260B 06/23/07 2021 erussell 024503hIdJóoiethaieBRLmg/kg 0.0053 0.0O044 82º0B 06/23/07 20.21 erusseH 024503VinylacetateBRLmg/kg 0.027 0.0019 8260B 06/23/07 2021 erussell 024503inylchlorideBRLmg/kg 0.0053 0.00068 8260B 06/23/07 2021 erusseti Q24503
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Full Survke AnalytIcal Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 184954SampleMatrixSoilCOCGroupG0607542
Time Collected 06/19/07
Time Submitted 06/19/07
1630
1735
Surrogate Recovery Control Limits
Bromofluorobenzene 94 77-128
Dibromofluoromethane 75 67 143
Toluene-dB 94 81 128
mi-volatile Organic Compounds by GC/MS
.4-Trichlorobenzene BRL mg/kg 0.40 0.040 8270C
L2-Dichlorobenzene BRL mg/kg 0.40 0.030 8270C-DichIorobe BRL mg/kg 0.40 0.029 8270C
4-DichIorobenzene BRL mg/kg 0.40 0.036 8270C
S-Trichlorophenol BRL mg/kg 0.40 0.041 8270C
46-Thchlorophenol BRL mg/kg 0.40 0.039 8270C
06/26/07 1915 keampigotto
06/26/07 1915 keampigotto
06/26/07 1915 kcampigouo
06/26/07 1915 kcarnpigotto
06/26/07 1915 kcarnpigofto
06/26/07 1915 kcarnpigotto
024532
024532
024532
024532
024532
024532
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpnngbrooçRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number l-800/529-63M Fax 704/525-0409 Page 17 of35
NC Certification No 402
Laboratory ReportScCertificationNo99012
NC Drinking Water Cert No 37735 06/29/07
Project ID Morehead Commons No Client Sample ID WS-3
Prism Sample ID 184954
Sample Matrix Soil COC Group G0607542
Time Collected 06/19/07 1630
Time Submitted 06/1 9107 1735
ESP Associates PA
ttn Chris Ward
Box 7030
Charlotte NC 28241
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/lime ID
4-Dichlorophenol BRL mg/kg 0.40 0.034 8270C 06/26/07 1915 koanipigotto Q24532
4-Dimethy1phenoI BRL mg/kg 0.40 0.039 8270C 06/26/07 1915 kcarnpigotto Q24532
4-Dinitrophenol BRL mg/kg 2.0 0.045 8270C 06/26/07 1915 kcarnpigotto 024532
4-Dinitrotoluene BRL mg/kg 0.40 0.023 8270C 06/26/07 1915 kcarripigotto 024532
26-Dinitrotoluene BRL mg/kg 0.40 0.043 8270C 06/26/07 1915 kcarnpigotto Q24532
-Chloronaphthalene BRL mg/kg 0.40 0.041 8270C 06/26/07 1915 kcarnpigotto Q24532
2Chlorophenoj BRL mg/kg 0.40 0.032 8270C 06/26/07 1915 kcarnpigotto Q24532
Methylnaphthalene 0.13 mg/kg 0.40 0.032 8270C 06/26/07 1915 kcarnpigotto Q24532
2-Methyiphenol BRL mg/kg 0.40 0.038 8270C 06/26/07 1915 kcarnpigotto 024532
Nitropheno BRL mg/kg 0.40 0.048 8270C 06/26/07 1915 kcampigotto Q24532
4-MethyIphenoI BRL mg/kg 0.40 0.041 8270C 06/26/07 1915 kcanipigotto 024532
3-DichIorobrizjdine BRL mg/kg 0.80 0.025 8270C 06/26/07 1915 kcanipigotto Q24532
5-Dinitro-2rejhylphenol BRL mg/kg 2.0 0.024 8270C 06126/07 19i kcanipigotto 024532
4-Bromophenyphenylether BRL mg/kg 0.40 0.038 8270C 06/26/07 1915 kcarnpigotto 024532
horo-3-methyIphenol BRL mg/kg 0.80 0.029 8270C 06/26/07 1915 kcampigotto 0245324-Chloroariline BRL mg/kg 0.40 0.051 8270C 06/26/07 1915 keampigotto 024532
Dhlorophenylphenylether BRL mg/kg 0.40 0.025 8270C 06/26/07 1915 kcampigotto 0245324-Nitrophenol BRL mg/kg 2.0 0.027 8270C 06/26/07 1915 kcampigofto Q24532enaphtheneBRLmg/kg 0.40 0.039 8270C 06/26/07 1915 kcampigotto 024532eenaphthyIene0.24 mg/kg 0.40 0.040 8270C 06/26/07 1915 kcampigotto Q24532thracene0.41 mg/kg 0.40 0.030 8270C 06/26/07 1915 kcampigotto Q24532benzeneBRLmg/kg 2.0 0.037 8270C 06/26/07 1915 keampigotto Q24532enzoaanthracene0.89 mg/kg 0.40 0.056 8270C 06/26/07 1915 kcampigotto Q24532izoapyrene0.95 mg/kg 0.40 0.046 8270C 06/26/07 1915 kcampigotto 024532enzobfluoranthene1.1 mg/kg 0.40 0.018 8270C 06/26/07 1915 kcampigotto 024532izoghipeyl0.69 mg/kg 0.40 0.019 8270C 06/26/07 1915 kcarnpigotto Q24532lenzokfluoranthene1.1 mg/kg 0.40 0.033 8270C 06/26/07 1915 kcampigouo 024532
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrooçRoad P.O Box 240543 Charlotte NC 28224-0543Phone704/529-6354 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page 18 of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
oil Service Anaiytlcai Environmental Solutions
ESP Associates PA Project ID
ttn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
Sample Matrix Soil
Morehead Commons No Client Sample ID WS-3
Prism Sample ID 184954
COC Group G060 7542
Time Collected 06/19/07 1630
Time Submitted 06/19/07 1735
Result Units Report MDL Dilution Methodtarameter
Analysis Analyst
Batch
Limit Factor Date/Time ID
erzoic acid BRL mg/kg 2.0 0.17 82700 06/26/07 1915 keampigotto Q24532
enzyl alcohol BRL mg/kg 0.80 0.042 8270C 06/26/07 1915 kcampigotto 024532
is2-chloroethoxymethane BRL mg/kg 0.40 0.046 82700 06/26/07 1915 kcampigotto Q24532
is2-chloroethylether BRL mg/kg 0.40 0.044 8270C 06/26/07 1915 kcampigotto Q24532
Bis2-chloroisopropylether BRL mg/kg 0.40 0.034 8270C 06/26/07 1915 kcampigotto Q24532
is2-ethylhexylphthalate BRL mg/kg 0.40 0.020 8270C 06/26/07 1915 kcampigotto 024532
Butylbenzylphthalate BRL mg/kg 0.40 0.025 8270C 06/26/07 1915 kcampigotto 024532
hrysene 0.98 mg/kg 0.40 0.067 82700 06/26/07 1915 kcampigotto Q24532
Di-n-butylphthalate BRL mg/kg 0.40 0.018 82700 06/26/07 1915 kcampigotto Q24532
l-n-octylphthalate BRL mg/kg 0.40 0.030 8270C 06/26/07 1915 kcampigotto Q24532
benzoahanthracene 0.24 mg/kg 0.40 0.040 82700 06/26/07 1915 kcampigotto 024532
rMbenzofuran 0.14 mg/kg 0.40 0.034 8270C 06/26/07 1915 kcarnpigotto Q24532
thylhthalate BRL mg/kg 040 0025
Dimethylphthalate BRL mg/kg 0.40 0.027 8270C 06/26/07 1915 kcampigotto 024532
uoranthene 1.7 mg/kg 0.40 0.028 82700 06/26/07 1915 kcampigotto 024532
Flijorene 0.33 mg/kg 0.40 0.024 82700 06/26/07 1915 kcampigotto 024532
xchlorobenzene BRJ.mg/kg 0.40 0.021 8270C 06/26/07 1915 kcampigotto 024532
Hexachlorobutadiene BRL mg/kg 0.40 0.039 82700 06/26/07 1915 keampigotto 024532
xachlorocyclopentadiene BRL mg/kg 0.40 0.043 8270C 06/26/07 1915 kcampigotto Q24532
..ixachloroethan BRL mg/kg 0.40 0.041 82700 06/26/07 1915 kcampigotto 024532erio123-cdpyrene 0.83 mg/kg 0.40 0.041 8270C 06/26/07 1915 kcampigotto Q24532
phorone BRL mg/kg 0.40 0.036 8270C 06/26/07 1915 kcampigotto 024532
J-Nitrosodi-n-propylamine BRL mg/kg 0.40 0.046 8270C 06/26/07 1915 kcampigotto Q24532
itrosodiphenylam me BRL mg/kg 0.40 0.020 8270C 06/26/07 1915 kcampigotto 024532
1aphthalene 0.23 mg/kg 0.40 0.044 8270C 06/26/07 1915 kcampigotto Q24532
BRL mg/kg 0.40 0.039 8270C 06/26/07 1915 kcampigotto 024532
BRL mg/kg 2.0 0.034 8270C 06/26/07 1915 kcampigotto 024532
oZUU UohoiV.w3bKcarnpjgTQ24S32
robenzene
entachlorophenol
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FuU ServIce Analytical ironmantal Soh4ons
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
arameter
henanthrene
----.henol
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Surrogate Recovery Control Limits
1-Chloro-octadecane 81 40 140
2-Bromonaphtl-alene 123 40 140
2-Fluorobiphenyl 103 40 140
o-Terphenyl 87 40 140
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbroolçRoadP.O Box 240543 Charlotte NC 28224.0543
Phone 7041529-6364 Toll Free Number 1-8001529-6364 Fax 704/525-0409
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil coc Group
Time Collected
Time Submitted
WS-3
184954
G0607542
06/19/07 1630
06/19/07 1735
Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
0.34 mg/kg 0.40 0.020 8270C 06/26/07 1915 kcampigotto Q24532
BRL mg/kg 0.40 0.044 8270C 06/26/07 1915 kcampigotto Q24532
2.1 mg/kg 0.40 0.027 8270C 06/26/07 1915 kcampigotto 024532
ryrene
Sample Preparation 29.88 mL 3550B 06/22/07 1100 dpope P1 8710
Surrogate Recovery Control Limits
246-Tribromophenol 94 25 123
2-Fluorobiphenyl 87 21 108
2-Fluorophenol 84 14-89
Nitrobenzene-d5 82 14-103
Phenol-d5 92 13-95
Terphenyl-d14 96 41 136
xtractable Petroleum Hydrocarbons by GC-FID
Cl 1-C22 Aromatics 130 mg/kg 12 6.4 MADEP EPH 06/24/07 232 grappaccioli 024514
lg-036 Aliphatics BRL mg/kg 12 1.8 MADEP EPH 06/24/07 232 grappacciot 024514
C9-Cl8Aliphatics BRL mg/kg 12 3.8 MADEP EPH 06/24/07 232 grappaccioli Q24514
Analysis NQte for C.l-C22 Aromatics Adjusted value
Sample Preparation 10.24 mL EPH 06/21/07 800 grappaccioli P18703
VJiJs bvlCP
romium
ad
46 mg/kg
110 mg/kg
0.26 0.016
0.26 0.022
6010B
6010B
06/25/07 1347 mcampbell
06/25/07 1347 mcampbell
024519
Q2451
Page 20 of 35
Laboratory Report
06129/07
ESP Associates PA WS-3AttnChrisWard
184954Box7030
G0607542CharlotteNC28241
06/19/07 1630
06/19/07 1735
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Sample Preparation 2.3 50 mL
Volatile Petroleum Hydrocarbons by GC-PID/FID
5-C8Aliphatics BRL mg/kg 6.1 1.2 MADEPVPH 06/27107 838 hwagner Q24582
.J9-C10 Aromatics BRL mg/kg 6.1 0.036 MADEP VPH 06/27/07 838 hwagner Q24582
.c9-C12 Aliphatics BRL mg/kg 6.1 1.9 MADEP VPH 06/27/07 838 hwagrier Q24582
Analysis Note for C5-C8 Aliphatics Adjusted valueAnalysisNoteforC9-C12 Alphatjcs Adjusted value
Surrogate Recovery Control Limits
25-Dibroniotoluene..FID 112 70 130
25-Dibromotolueflep 87
.mple Weight Determination
Øight-l 1683 MADEPVPH 06/26/07 0O0 lb6n
Weight 21.10 MADEP VPH 06/26/07 000 brown
Below Reporting Limit
Estimated value between the Reporting Limit arid the MDLTheresultsinthisreport relate only to the samples submitted for analysis and meet state certification requirements other thanMCcertificationexceptforthoseinstancesindicatedinthecasenarrativeand/or test commentsresultsarereportedondry-weight basis
rnull Servlco Analytical tinvlronmenlal Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
30508 06/21/07 905 jhoppel P18702
70-130
gela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrooRoadP.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 ToH Free Number 1-800/529-6364 Fax 7041525-0409 Page 21 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
WS-4
184955
G0607542
06/19/07
06/19/07
Percent Solids Determination
Percent Solids
Sample Weight Determination
Weight Bisulfate
Weight Bisulfate
Weight Methanol
Result Units Report
Limit
MDL Dilution Method
Factor
Analysis Analyst
Batch
Date/Time ID
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter
1645
1735
84.9
5.16
5.34
5.62
SM2540 06/25/07 1745 Lthao
5035 06/27/07 000 brown
5035 06/27/07 000 Ibrown
5035 06/27/07 000 brown
Volatile Organic Compounds by GCIMS
111-Trichloroethane BRL mg/kg 0.0055 0.00031 8260B 06/23/07 1743 erussell
l122-Tetrachloroethane BRL mg/kg 0.0055 0.00056 8260B 06/23/07 1743 erussell
112-Trichioroethane BRL mg/kg 0.0055 0.00034 8260B 06/23/07 1743 erussell
i1-Dichloroethane BRL mg/kg 0.0055 0.0004 8260B 06/23/07 1743 erussell
i1-DiOhlbthene BRL mg/k 0.0055 000042
024503
Q245o3
024503
024503
Q24503iui
1F1-Dichloropropene BRL mg/kg 0.0055 0.00049 8260B 06/23/07 1743 erussell 024503
l23-Trichlorobenzene BRL mg/kg 0.0055 0.00061 8260B 06/23/07 1743 erussell 024503
l23-Trichloropropane BRL mg/kg 0.0055 0.00049 8260B 06/23/07 1743 erussell 024503
I24-Trichlorobenzene BRL mg/kg 0.0055 0.00053 8260B 06/23/07 1743 erussell Q24503
l24-Trimethylbenzene BRL mg/kg 0.0055 0.00042 8260B 06/23/07 1743 erussell Q24503
I2Dibromoethane EDB BRL mg/kg 0.0055 0.000099 8260B 06/23/07 1743 erussell 024503
2-DichIorobenzene BRL mg/kg 0.0055 0.0003 8260B 06/23/07 1743 erussell 024503
l2-Dichloroethane BRL mg/kg 0.0055 0.00055 8260B 06/23/07 1743 erussell 024503
2-DichJoropropane BRL mg/kg 0.0055 0.00041 8260B 06/23/07 1743 erussell Q24503
t35-Trimethylbenzene BRL mg/kg 0.0055 0.00046 8260B 06/23/07 1743 ewssell Q24503
3-Dichlorobenzene BRL mg/kg 0.0055 0.00047 8260B 06/23/07 1743 erussell Q24503
l3-Dichloropropane BRL mg/kg 0.0055 0.00037 8260B 06/23/07 1743 erusselt 024503
4-Dichlorobenzene BRL mg/kg 0.0055 0.00043 8260B 06/23/07 1743 erussell 024503
22-Dichloropropane BRL mg/kg 0.0055 0.00028 826DB 06/23/07 1743 erussell 024503
-Chlorotoluene BRL mg/kg 0.0055 0.00041 8260B 06/23/07 1743 erussell Q245o3
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page 22 of 35
WS-4
184955
G0607542
06/1 9/07 1645
06/19/07 1735
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
FuH Seivice AnalyScal Environmental
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Result Units Report MDL Dilution Method Analyst Batch
ID
Analysis
Limit Factor Date/Time
2-Flexanone BRL mg/kg 0.055 0.00057 8260B 06/23/07 1743 erussell Q24503
4-ChorotoIuene BRL mg/kg 0.0055 0.00029 8260B 06/23/07 1743 erussell Q24503
4-Methyl-2-pentanone MIBK BRL mg/kg 0.055 0.00055 8260B 06/23/07 1743 erussell 024503
Acetone BRL mg/kg 0.055 0.0022 8260B 06/23/07 1743 erussell 024503
3enzene 0.0023 mg/kg 0.0033 0.00044 8260B 06/23/07 1743 erussell 024503
Brornobenzene BRL mg/kg 0.0055 0.00039 826GB 06/23/07 1743 erussell 024503
Bromochioromethane BRL mg/kg 0.0055 0.00033 8260B 06/23/07 1743 erussell 024503
Bromodichioromethane BRL mg/kg 0.0055 0.00049 826GB 06/23/07 1743 erussell 024503
Bromoform BRL mg/kg 0.0055 0.00041 8260B 06/23/07 1743 erussell 024503
Bromomethane BRL mg/kg 0.011 0.00064 826GB 06/23/07 1743 erussell 024503
Carbon tetrachloride BRL mg/kg 0.0055 0.00032 8260 06/23/07 1743 erusselt 024503
Chloroberizee-SRI.mg/kg 0.0055 0.00042 --8260B_
--
O6I23/0 1743 erussell 024503
ChIoodibrorromethane BRL mg/kg a0055 0.00037 8260B 06/23/07 1743 erussell Q24503
Chioroethane BRL mg/kg 0.011 0.00045
Chloroform BRL mg/kg 0.0055 0.00041
Chioromethane BRL mg/kg 0.0055 0.00039
is-1 2-Dichloroethene BRL mg/kg 0.0055 0.00024
cis-1 3-Dichloropropene BRL mg/kg 0.0055 0.00035
ichlorodifluoromethane BRL mg/kg 0.0055 0.0012
Ethylbenzene 0.0030 mg/kg 0.0055 0.00039
sopropyl ether IPE BRL mg/kg 0.0055 0.00019
sopropylbenzene BRL mg/kg 0.0055 0.00044
p-Xylenes 0.0026J mg/kg 0.011 0.00077
ilethyl ethyl ketone MEK BRL mg/kg 0.11 0.0015
Methyl t-butyl ether MTBE BRL mg/kg 0.011 0.00032
lethylene chloride BRL mg/kg 0.0055 0.00045
Butylbenzene BRL mg/kg 0.0055 0.00044
826GB
8260B
826GB
8260B
826GB
8260B
8260B
82608
8260B
8260B
8260B
826GB
8260B
82608
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
06/23/07
1743 erussell
1743 erussell
1743 erussell
1743 erussell
1743 erussell
1743 erussell
1743 erussell
1743 erussell
1743 erusseU
1743 erussell
1743 erussell
1743 erussell
1743 erussell
1743 erussejl
024503
024503
024503
024503
024503
024503
024503
024503
024503
024503
024503
024503
024503
024503
Page 23 of 35
Full Servica Anal
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COO Group
Time Collected
Time Submitted
WS-4
184955
G0607542
06/19/07 1645
06/19/07 1735
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
Result Units Report MDL Dilution Method Analysis
Limit Factor Date/Time
mg/kg 0.0055 0.00033 826DB 06/23/07 1743 erussefl
mg/kg 0.011 0.00064 8260B 06/23/07 1743 erussefl
mg/kg 0.0055 0.00033 826DB 06/23/07 1743 erussefi
mg/kg 0.0055 0.00045 826DB 06/23/07 1743 erusset
mg/kg 0.0055 0.00036 8260B 06/23/07 1743 erussell
mg/kg 0.0055 0.00055 826oB 06/23/07 1743 erussell
mg/kg 0.0055 0.00034 826DB 06/23/07 1743 erussell
mg/kg 0.0055 0.00095 826DB 06/23/07 1743 enjssell
mg/kg 0.0055 0.00037 826DB 06/23/07 1743 erussell
mg/kg 0.0055 0.00042 826DB 06/23/07 1743 erusseli
mg/kg 0.0055 0.00039 826DB 06/23/07 1743 erussell Q24503
Parameter
Analyst Batch
ID
nPropylbenzeneBRL 024503
Naphthaene BRL 024503
o-Xylene BRL Q24503
p-lsopropyltoluene BRL Q24503
sec-Butyfbenzene BRL Q24503
Styrerie BRL Q24503
te.rtButylbenzene BRL 024503
Tetrachioroethene BRL 024503
Tcluene 0.0067 024503
trans-i2-Dichloroethene BRL Q24503
trans-i 3-Dichloropropene BRL
Trichioroethene
--
BRL mg/kg 0.0055 0.00033 8260B 06/23/07 1743 erussell 024503
TrihtorOflujbnjethane BRL æi7kg 0.0055 000045 826DB 06/23/07 1743 5ru5eII Q24503
JinyI acetate BRL mg/kg 0.028 0.0020 826DB 06/2307 1743 erussell 024503
Vinyl chloride BRL mg/kg 0.0055 0.00071 826DB 06/23/07 1743 erussell 024503
Surrogate Recovery Control Limits
Bromofluorobenzene 82 77 128
Dibromofluoromethane 68 67 143
Toluerie-d8 81 81 128
3emi-volatite Orqanic Compounds by GC1MS
24-Trichlorobenzene BRL mg/kg 0.40 0.039 8270C 06/26/D7 2004 kcampigotto 024532
2-Dichlorobenzene BRL mg/kg 0.40 0.029 827DC 06/26/07 2004 kcampigotto Q24532
3-Dichjorobenzene BRL mg/kg 0.40 0.028 827DC 06/26/07 2004 kcampigotto Q24532
l4-Dichlorobenzene BRL mg/kg 0.40 0.036 82700 06/26/07 2004 kcampigotto Q24532
45-Trichlorophenol BRL mg/kg 0.40 0.040 8270C 06/26/07 2004 kcampigotto 024532
246-Trichlorophenol BRL mg/kg 0.4D 0.038 8270C 06/26/07 2004 kcampigotto 024532
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page 24 of 35
Laboratory Report
06/29/07
ESP Associates PA WS4
Attn Chris Ward 184955
Box 7030 G0607542
Charlotte NC 28241 0611 9/07
06/19/07
Full Service Analytical Environme......putlons
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
24-Dichiorophenol BRL
24-Dimethylphenol BRL
24-Dinitrophenol BRL
24-Dinitrotoluene BRL
26-Dinitrotoluene BRL
2-Chloronaphthalene BRL
2-Chiorophenol BRL
BRL
BRL
BRL
BRL
1645
1735
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
mg/kg 0.40 0.033 8270C 06/26/07 2004 kcampigotto 024532
mg/kg 0.40 0.038 8270C 06/26/07 2004 kcampigotto 024532
mg/kg 2.0 0.044 82700 06/26/07 2004 kcampigotto Q24532
mg/kg 0.40 0.022 82700 06/26/07 2004 kcampigotto 024532
mg/kg 0.40 0.042 8270C 06/26/07 2004 kcampigotto Q24532
mg/kg 0.40 0.041 8270C 06/26/07 2004 kcampigotto 024532
mg/kg 0.40 0.031 82700 06/26/07 2004 kcampigotto 024532
2-Methylnaphthalene mg/kg 0.40 0.031 8270C 06/26/07 2004 kcampigotto 024532
2-Methylphenol mg/kg 0.40 0.037 8270C 06/26/07 2004 kcampigotto Q24532
-Nitrophenol mg/kg 0.40 0.047 8270C 06/26/07 2004 kcampigotto 024532
34-Methylphenol mg/kg 0.40 0.040 82700 06/26/07 2004 kcampigotto 024532
13-Dichlorobenzidine BRL mgLkg 0.79 0.025 8270C 06/26/072004 kcarnpigotto 024532
heDinIethyIphenot BRL mg/kg 2.0 0.024 870C O6/26/07204 kcamp1tto 024532
4-Bromophenylphenylether BRL mg/kg 0.40 0.037 82700 06/26/07 2004 kcampigotto 024532
-Chloro-3-methylphenoj BRL mg/kg 0.79 0.029 8270C 06/26/07 2004 kcampigotto 024532
4-Chioroaniline BRL mg/kg 0.40 0.050 82700 06/26/07 2004 kcampigotto Q24532
-Chlorophenylphenylether BRL mg/kg 0.40 0.024 82700 06/26/07 2004 keampigotto 024532
4-Nitrophenol BRL mg/kg 2.0 0.026 82700 06/26/07 2004 kcampigotto 024532
cenaphthene BRL mg/kg 0.40 0.039 82700 06/26/07 2004 koampigotto Q24532
Acenaphthytene BRL mg/kg 0.40 0.039 8270C 06/26/07 2004 kcampigotto 024532
nthracene BRL mg/kg 0.40 0.030 8270C 06/26/07 2004 kcampigotto 024532
2obenzene BRL mg/kg 2.0 0.037 8270C 06/26/07 2004 kcampigoffo 024532
Benzoaanthracene BRL mg/kg 0.40 0.055 8270C 06/26/07 2004 kcampigotto Q24532
opyrene BRL mg/kg 0.40 0.046 82700 06/26/07 2004 kcampigotto Q24532
Benzobfluoranthene BRL mg/kg 0.40 0.018 82700 06/26/07 2004 kcampigotto Q24532
nzoghiperylene BRL mg/kg 0.40 0.019 82700 06/26/07 2004 keampigotto 024532
Benzokfluoranthene BRL mg/kg 0.40 0.032 82700 06/26/07 2004 kcampigotto Q24532
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 7041525-0409 Page 25 of 35
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-4
184955
G0607542
06/19/07 1645
06/19/07 1735
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
FL...e Analytical Envimnmenbl Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Parameter
Laboratory Report
06/29/07
Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Benzoic acid BRL mg/kg 2.0 0.17 8270C 06/26/07 2004 kcampigotto 024532
Benzyl alcohol BRL mg/kg 0.79 0.042 8270C 06/26/07 2004 kcamplgotto Q24532
Bis2-chloroethoxymethane BRL mg/kg 0.40 0.045 8270C 06/26/07 2004 kcampigotto 024532
Bis2-chloroethylether BRL mg/kg 0.40 0.043 82700 06/26/07 2004 kcampigotto 024532
Bis2-chloroisopropylether BRL mg/kg 0.40 0.034 8270C 06/26/07 2004 kcampigotto Q24532
Bis2-ethylhexylphthalate BRL mg/kg 0.40 0.019 8270C 06/26/07 2004 kcampigotto 024532
I3utylbenzylphthalate BRL mg/kg 0.40 0.024 8270C 06/26/07 2004 kcampigotto Q24532
Chrysene BRL mg/kg 0.40 0.066 8270C 06/26/07 2004 kcampigotto Q24532
Di-n-butylphthalate BRL mg/kg 0.40 0.018 8270C 06/26/07 2004 kcampigotto Q24532
Di-ncctylphthalate BRL mg/kg 0.40 0.029 82700 06/26/07 2004 kcampigotto Q24532
Dibenzoahanthracene BRL mg/kg 0.40 0.040 82700 06/26/07 2004 kcampigotto 024532
ibenzofuran -BRL mg/kg 0.40 0.034 8270C 06/26/07 2004 kcarnpigotto 024532
Qiethylphthalate BRL mg/kg 0.40 0.024 8270C 06/26/07 2004 kcampigotto 024532
Jimethylphthalate BRL mg/kg 0.40 0.027 82700 06/26/07 2004 kcampigotto 024532
9uoranthene BRL mg/kg 0.40 0.027 8270C 06/26/07 2004 kcampigouo 024532
Fluorene BRL mg/kg 0.40 0.023 8270C 06126/07 2004 kcampigotto 024532
lexachlorobenzene BRL mg/kg 0.40 0.020 82700 06/26/07 2004 kcampigotto 024532
Hexachlorobutadiene BRL mg/kg 0.40 0.038 82700 06/26/07 2004 kcampigotto 024532
lexachlorocyclopentadiene BRL mg/kg 0.40 0.042 8270C 06/26/07 2004 kcampigotto 024532
Hexachioroethane BRL mg/kg 0.40 0.040 82700 06/26/07 2004 kcampigotto Q24532
ideno1 23-cdpyrene BRL mg/kg 0.40 0.040 82700 06/26/07 2004 kcampigotto 024532
isophorone BRL mg/kg 0.40 0.035 82700 06/26/07 2004 kcampigotto 024532
kNitrosodi-npropyIamine BRL mg/kg 0.40 0.045 82700 06/26/07 2004 kcampigotto 024532
-Nitrosodiphenylamine BRL mg/kg 0.40 0.020 82700 06/26/07 2004 kcampigotto 024532
Naphthalene BRL mg/kg 0.40 0.043 82700 06/26/07 2004 kcampigotto 024532
itrobenzene BRL mg/kg 0.40 0.038 82700 06/26/07 2004 kcampigotto 024532
Pentachlorophencl BRL mg/kg 2.0 0.033 82700 06/26/07 2004 kcampigotto Q24532
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 ToH Free Number 1-800/529-6364 Fax 704/525-0409 Page 260135
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report
Limit
Analysis Analyst Batch
Date/Time
06/26/07 2004 kcampigotto Q24532
06/26/07 2004 kcampigotto Q24532
06/26/07 2004 kcampigotto Q24532
Sample Preparation 29.52 mL 3550B 06/22/07 1100 dpope P18710
Surrogate Recovery Control Limits
2-Bromonaphthalene 114 40 140
o-Terphenyl 90 40 140
1-Chloro-octadecane 122 40-140
2-Fluorobiphenyl 116 40-140
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
Pull Service Analytical Environmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
WS-4
184955
00607542
06/19/07
06/19/07
1645
1735
MDL Dilution Method
Factor
Phenanthrene BRL mg/kg 0.40 0.019 8270C
Phenol BRL mg/kg 0.40 0.043 8270C
Pyrene BRL mg/kg 0.40 0.027 8270C
ID
Surrogate Recovery Control Limits
246-Tribromophenol 69 25 123
2-Fluorobiphenyl 66 21 108
2-Fluorophenol 49 14 89
Nitrobenzene-d5 53 14 103
Terphenyl-d14 100 41 136
Phenol-d5 62 13-95
Extractable Petroleum Hydrocarbons by GC-FID
C11-C22 Aromatics BRL mg/kg 11 6.1 MADEP EPH 06/24/07 416 grappaccioli Q24514
19-C36AIiphatics BRL mg/kg 11 1.7 MADEP EPH 06/24/07 416 grappaccioli Q24514
C9-Cl8Aliphatics BRL mg/kg 11 3.6 MADEP EPH 06/24/07 416 grappaccioli Q24514
Analysis Note for C11-C22 Aromatjcs Adjusted value
Sample Preparation 10.42 mL EPH 06/21/07 800 grappaccioli P18703
hromium
.ead
28 mg/kg
22 mg/kg
0.27 0.016
0.27 0.022
6010B
601DB
06/25/07 1354 mcampbell
06/25/07 1354 mcampbell
Q24519
Q24519
Page 27 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
WS-4
184955
G0607542
06/19/07
06/19/07
Report MDL Dilution
Limit Factor
Method Analysis
Date/Time
Analyst Batch
ID
Sample Preparation
Volatile Petroleum Hydrocarbons by GC-PIDIFID
C5-C8 Aliphatics BRL
C9-C1 Aromatics
C9-C12 Aliphatics
Analysis Note for C5-C8 Aliphatics
Analysis Note for C9-C12 Aliphatics
2.2 50 mL 3050B 06/21107 905 jhoppel
mg/kg 5.9 1.1 MADEP VPH 06/27/07 921 hwagner
Adjusted value
Adjusted value
arnpleWeightDetermjnatjon --
----Vºight
--
--22.68 MADEPVPH 06/26107cj00 Ibrown
MADEP VPH 06/26/07 000 brown
Sample Comments
Below Reporting Limit
J-Estimated value between the Reporting Limit and the MDL
he results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanIELACcertificationexceptforthoseinstances indicated in the case narrative and/or test commentsAuresultsarereportedondry-weight basis
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
tervice Analytical Environmental Sc._....nn
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units
1645
1735
BRL mg/kg 5.9 0.035 MADEP VPH 06/27/07 921 hwagner
BRL mg/kg 5.9 1.8 MADE VPH 06/27/07 921 hwagner
P18702
Q24582
Q24582
Q24582
Weight
Surrogate Recovery Control Limits
25-Dibromotoluene-PID 94 70 130
25-Dibromotoluene-FID 121 70 130
18.97
.ngela Overcash V.P Laboratory Services
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page 28 of 35
Laboratory Report
NC Drinking Water Cert No 37735 06/29/07
ESP Associates PA Project ID Morehead Commons No Client Sample ID B-i
Attn Chris Ward Prism Sample ID 184956
Box 7030 Sample Matrix Soil COO Group 00607542
Charlotte NC 28241 Time Collected 06/1 9/07 1700
Time Submitted 06/19/07 1735
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Percent Solids Determination
Percent Solids 81.3 8M2540 06/25/07 1745 Lthao
Sample Weight Determination
Weight Bisulfate 6.37 5035 06/27/07 000 Ibrown
Weight Bisulfate 6.42 5035 06/27/07 000 brown
Weight Methanol 6.44 5035 06/27/07 000 brown
Vo atile Organic Compounds by GC/MS
11-TrichIoroethane BRL mg/kg 0.0048 0.00027 8260B 06/26/07 506 erussell 024504
1122-Tetrachioroethane BRL mg/kg 0.0048 0.00049 8260B 06/26/07 506 erussell Q24504
112-Trichioroethane BRL mg/kg 0.0048 0.0003 8260B 06/26/07 506 erusseH 024504
11-Dichioroethane BRL mg/kg 0.0048 0.00034 8260B 06/26/07 506 erussell 024504
l1Dihloroethene BRL mg/kg 0.0048 0.00036 8260B 06/26/07 506 erussell 024504
11Dichloropropene BRL mg/kg 0.0048 0.00042 8260B 06/26/07 506 erussell Q24504
I23-Trichlorobenzene BRL mg/kg 0.0048 0.00053 8260B 06/26/07 506 erussell 024504
23-Trichloropropane BRL mg/kg 0.0048 0.00042 8260B 06/26/07 506 erussell Q24504
24-Trichlorobenzene BRL mg/kg 0.0048 0.00046 8260B 06/26/07 506 erussell Q24504
24-Trimethylbenzene BRL mg/kg 0.0048 0.00036 82608 06/26/07 506 erusseu 024504
2-Dibromoethane EDB BRL mg/kg 0.0048 0.000086 8260B 06/26/07 506 erussell Q24504
2-Dichlorobenzene BRL mg/kg 0.0048 0.00026 8260B 06/26/07 506 erussell Q24504
2-Dichioroethane BRL mg/kg 0.0048 0.00048 8260B 06/26/07 506 erussell 024504
2-Dichloropropane BRL mg/kg 0.0048 0.00035 8260B 06/26/07 506 erussell 024504
l35-Trimethyibenzene BRL mg/kg 0.0048 0.0004 82608 06/26/07 506 erussell 024504
3-Dichlorobenzene BRL mg/kg 0.0048 0.00041 8260B 06/26/07 506 erussell Q24504
3-Dichloropropane BRL mg/kg 0.0048 0.00033 8260B 06/26/07 506 erussell Q24504
4-Iichloroberzene BRL mg/kg 0.0048 0.00037 826GB 06/26/07 506 erussell 024504
22-Dichloropropane BRL mg/kg 0.0048 0.00024 8260B 06/26/07 506 erussell 024504
Chlorotoluene BRL mg/kg 0.0048 0.00035 82603 06/26/07 506 ewssell 024504
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page 29 of 35
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report
B-I
184956
G0607542
06/19/07 1700
06/19/07 1735
MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
2-Hexanone BRL mg/kg 0.048 0.0005 826DB 06/26/07 506 erussell Q24504
4-Chlorotoluene BRL mg/kg 0.0048 0.00025 8260B 06/26/07 506 erussell Q24504
4-Methyl-2-pentanone MIBK BRL mg/kg 0.048 0.00048 826DB 06/26/07 506 erusset Q24504
Acetone BRL mg/kg 0.048 0.0019 826DB 06/26/07 506 erussell Q24504
Benzene BRL mg/kg 0.0029 0.00038 8260B 06/26/07 506 erussell Q24504
Bromobenzene BRL mg/kg 0.0048 0.00034 826DB 06/26/07 506 erussell Q24504
Bromochloromethane BRL mg/kg 0.0048 0.00029 826DB 06/26/07 506 erussell Q245D4
Bromodichioromethane BRL mg/kg 0.0048 0.00042 826DB 06/26/07 506 erussell Q24504
l3romoform BRL mg/kg 0.0048 0.00035 8260B 06/26/07 506 erussefi Q24504
3romomethane BRL mg/kg 0.0096 0.00056 8260B 06/26/07 506 ewssefl 024504
Carbon tetrachioride BRL mg/kg 0.0048 0.00028 82608 06/26/07 506 erussell 024504
hlQrobenzene BRL mg/kg 0.0048 0.00036 82608 Q6/26/07 506 erussefi Q24504
ioodibrmomethane BRL mikg O.oo4 0.00033 O6/26TO 506 en.issefl Q45o4
Chloroethane BRL mg/kg 0.0096 0.00039 82608 06/26107 506 erussell Q24504
hbroform BRL mg/kg 0.0048 0.00035 8260B 06/26/07 506 erussell 024504
Chioromethane BRL mg/kg 0.0048 0.00034 82608 06/26/07 506 erussefl Q24504
is-i 2-Dichloroethene BRL mg/kg 0.0048 0.00021 8260B 06/26/07 506 erussefl 024504
cis-i3-Dichjoropropene BRL mg/kg 0.0048 0.00031 8260B 06/26/07 506 erussell 024504
ichiorodifluoromethane BRL mg/kg 0.0048 0.0011 8260B 06/26/07 506 erussell Q24504
Lthylbenzene 0.0020 mg/kg 0.0048 0.00034 8260B 06/26/07 506 erussell Q24504
opropyl ether IPE BRL mg/kg 0.0048 0.00016 826DB 06/26/07 506 erussell Q24504
opropylbenzene BRL mg/kg 0.0048 0.00038 8260B 06/26/07 506 erussell 024504
rnp-Xylenes BRL mg/kg 0.0096 0.00067 8260B 06/26/07 506 erussell 024504
ethyl ethyl ketone MEK BRL mg/kg 0.096 0.0013 8260B 06/26/07 506 erussell Q24504
Methyl t-butyl ether MTBE BRL mg/kg 0.0096 0.00028 826DB 06/26/07 506 erussell 024504
sthylene chloride BRL mg/kg 0.0048 0.00039 82608 06/26/07 506 erussell 024504
n-Butylbenzene BRL mg/kg 0.0048 0.00038 826DB 06/26/07 506 erussell 024504
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 26224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page 30 of 35
CflC 99012 Laboratory Report
NC Drinking Water Cert No 37735 06/29/07
Project ID Morehead Commons No Client Sample ID B-I
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
n-Propylbenzene BRL mg/kg 0.0048 0.00029 8260B 06/26/07 506 erussell 024504
Naphthalene 0.0047 mg/kg 0.0096 0.00056 82606 06/26/07 506 erussell 024504
o-Xylene BRL mg/kg 0.0048 0.00029 8260B 06/26/07 506 erussell Q24504
p-lsopropyltoluene BRL mg/kg 0.0048 0.00039 82606 06/26/07 506 erussell 024504
sec-Butylbenzene BRL mg/kg 0.0048 0.00032 8260B 06/26/07 506 erussell Q24504
Styrene BRL mg/kg 0.0048 0.00048 8260B 06/26/07 506 erussell 024504
tert-Butylbenzene BRL mg/kg 0.0048 0.0003 8260B 06/26/07 506 erussell 024504
Tetrachioroethene BRL mg/kg 0.0048 0.00082 826DB 06/26/07 506 erusselJ Q24504
Toluene 0.0048 mg/kg 0.0048 0.00033 8260B 06/26/07 506 ewssell Q24504
trans-I 2-Dichloroethene BRL mg/kg 0.0048 0.00036 8260B 06/26/07 506 erussell 024504
trans-I 3-Dichloropropene BRL mg/kg 0.0048 0.00034 82606 06/26/07 506 erussefl 024504
Trichioroethene BRL mg/kg 0.0048 0.00029 860B 06/26/07 506 erussell Q24504
ThFoToTihan BJ ng/kg 0.0048 00O039 826DB 06126/O75O6 ertissell Q24504
Vinyl acetate BRL mg/kg 0.024 0.0017 82606 06/26/07 506 erussell 024504
Vinyl chloride BRL mg/kg 0.0048 0.00061 8260B 06/26/07 506 erussell 024504
Full ..eMce Analytlal Envlronmsnlal Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
184956
G0607542
06/19/07
06/1 9/07
1700
1735
Surrogate
Dibromofluoromethane
Recovery
96
Control Limits
67-143
77-128Bromofluorobenzene108
Toluene-d8 109 81 128
emi-voIatile Organic Comrounds by GCIMS
124-Trichlorobenzene BRL mg/kg 0.40 0.040 8270C 06/26/07 2053 kcampigotto 024532
2-Dichlorobenzene BRL mg/kg 0.40 0.030 8270C 06/26/07 2053 kcampigotto 024532
-.3-Dichlorobenzene BRL mg/kg 0.40 0.029 8270C 06/26/07 2053 kcampigotto 024532
14-Dichlorobenzene BRL mg/kg 0.40 0.036 8270C 06/26/07 2053 kcampigotto 024532
45-TrichIorophenol BRL mg/kg 0.40 0.041 8270C 06/26/07 2053 kcampigotto 024532
246-Trichlorophenol BRL mg/kg 0.40 0.039 8270C 06/26/07 2053 kcampigotto 024532
Thjs report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page 31 of35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/29/07
184956
G0607542
06/19/07 1700
06/19/07 1735
II Service Analytical Envlron ._..olutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID B-I
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
24-Dichiorophenol BRL mg/kg 0.40 0.034 8270C 06/26/07 2053 kcampigotto Q24532
24-Dimethyiphenol BRL mg/kg 0.40 0.039 8270C 06/26/07 2053 kcampigotto 024532
24-Dinitrophenof BRL mg/kg 2.0 0.045 8270C 06/26/07 2053 kcampigotto 024532
24-Dinitrotojuene BRL mg/kg 0.40 0.023 8270C 06/26/07 2053 kcampigotto Q24532
26-Din itrotoluene BRL mg/kg 0.40 0.043 8270C 06/26/07 2053 kcampigotto 024532
2-Chloronaphthalene BRL mg/kg 0.40 0.041 8270C 06/26/07 2053 kcampigotto 024532
2-Chiorophenol BRL mg/kg 0.40 0.032 8270C 06/26/07 2053 kcampigotto 024532
2-Methylnaphthalene BRL mg/kg 0.40 0.032 8270C 06/26/07 2053 kcampigotto 024532
2-Methyiphenol BRL mg/kg 0.40 0.038 8270C 06/26/07 2053 keampigotto 024532
2-Nitrophenol BRL mg/kg 0.40 0.043 8270C 06/26/07 2053 kcampigotto 024532
34-Methylphenol BRL mg/kg 0.40 0.041 8270C 06/26/07 2053 kcampigotto 024532
3-DichIorobenzidi BRL mg/kg _0.80 0.025 8270C 06/26/072053 kcampigotto 024532
46-Dinitro-2-methylphenol BRL mg/kg 2.0 0.025 870C ö612/07 2d53 kcanfpigótto Q22
4-Bromophenylphenylether BRL mg/kg 0.40 0.038 8270C 06/26/07 2053 kcampigotto Q24532
1-Chloro-3-methylphenof BRL mg/kg 0.80 0.030 3270C 06/26/07 2053 kcampigotto 024532
4-Chioroaniline BRL mg/kg 0.40 0.051 8270C 06/26/07 2053 kcampigotto Q24532
-ChlorophenylphenyIether BRL mg/kg 0.40 0.025 8270C 06/26/07 2053 kcampigotto 024532
4-Nitrophenol BRL mg/kg 2.0 0.027 8270C 06/26/07 2053 kcampigouo 024532
\cenaphthene BRL mg/kg 0.40 0.039 8270C 06/26/07 2053 kcampigotto Q24532
Acenaphthylene BRL mg/kg 0.40 0.040 8270C 06/26/07 2053 kcampigotto 024532
nthracene 0.12 mg/kg 0.40 0.030 8270C 06/26/07 2053 kcampigotto Q24532
.zobenzene BRL mg/kg 2.0 0.037 8270C 06/26/07 2053 kcampigofto 024532
Benzoaanthracene 0.19 mg/kg 0.40 0.056 8270C 06/26/07 2053 kcampigotto 024532
enzoapyrene 0.21 mg/kg 0.40 0.046 8270C 06/26/07 2053 kcampigofto 024532
enzobfluoranthene 0.33 mg/kg 0.40 0.018 8270C 06/26/07 2053 kcampigotto Q24532
enzoghipelene 0.13 mg/kg 0.40 0.019 8270C 06/26/07 2053 kcampigouo Q24532
Benzokfluoranthene 0.23 mg/kg 0.40 0.033 8270C 06/26/07 2053 kcampigotto 024532
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-8001529-6364 Fax 704/525-0409 Page 32 of 35
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
B-i
184956
G0607542
06/19/07 1700
06/19/07 1735
Jarvice Analytical Environmental
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Benzoic acid BRL mg/kg 2.0 0.17 8270C 06/26/07 2053 kcampigotto 024532
Benzyl alcohol BRL mg/kg 0.80 0.042 827CC 06/26/07 2053 kcampigotto Q24532
Bis2-chloroethoxymethane BRL mg/kg 0.40 0.046 827CC 06/26/07 2053 kcampigotto Q24532
Bis2-chloroethylether BRL mg/kg 0.40 0.044 827CC 06/26/07 2053 kcampigotto Q24532
Bis2-chloroisopropyjether BRL mg/kg 0.40 0.034 827CC 06/26/07 2053 kcampigotto Q24532
Bis2-ethylhexylphthalate BRL mg/kg 0.40 0.020 827CC 06/26/07 2053 kcampigotto 024532
Butylbenzylphthalate BRL mg/kg 0.40 0.025 827CC 06/26/07 2053 kcampigotto 024532
Chrysene 0.20 mg/kg 0.40 0.067 827CC 06/26/07 2053 kcampigotto 024532
Di n-butylphthalate BRL mg/kg 0.40 0.018 827CC 06/26/07 2053 kcampigotto 024532
Di-n-octylphthalate BRL mg/kg 0.40 0.030 827CC 06/26/07 2053 kcampigotto 024532
Dibenzoahanthracene BRL mg/kg 0.40 0.040 827CC 06/26/07 20.53 kcampigotto Q24532
Dibenzofuran 0.11 J-mg/kg-0.40 0.034 827CC C6/26/07 2053 campigotto Q24532
Diethylphthalate BRL mg/kg 0.40 0025 827CC 06/26/07 2053 kcampigotto 024532
Dimethylphthalate BRL mg/kg 0.40 0.027 827CC 06/26/07 2053 kcampigotto 024532
luoranthene 0.51 mg/kg 0.40 0.028 827CC 06/26/07 2053 kcampigotto 024532
Fluorene 0.17J mg/kg 0.40 0.024 827CC 06/26/07 2053 kcampigotto 024532
iexachlorobenzene BRL mg/kg 0.40 0.021 827CC 06/26/07 2053 kcampigotto 024532
Hexachiorobutadiene BRL mg/kg 0.40 0.039 827CC 06/26/07 2053 kcampigofto 024532
iexachlorocyclopentadiene BRL mg/kg 0.40 0.043 827CC 06/26/07 2053 kcampgotto 024532
Hexachioroethane BRL mg/kg 0.40 0.041 827CC 06/26/07 2053 kcampiotto Q24532
ndeno123-cdpyrene 0.30 mg/kg 0.40 0.041 827CC 06/26/07 2053 kcampigotto Q24532
sophorone BRL mg/kg 0.40 0.036 827CC 06/26/07 2053 kcampigotto Q24532
-Nitrosodi-n-propyIamjne BRL mg/kg 0.40 0.046 827CC 06/26/07 2053 kcampigotto Q24532
l-Nitrosodiphenylamine BRL mg/kg 0.40 0.020 827CC 06/26/07 2053 kcampigotto 024532
Naphthalene BRL mg/kg 0.40 0.044 827CC 06/26/07 2053 kcampigotto 024532
Iitrobenzene BRL mg/kg C.4C 0.039 827CC 06/26/07 2053 kcampgofto Q24532
Pentachiorophenol BRL mg/kg 2.0 0.034 827CC 06/26/07 2053 kcampigotto 024532
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 ToIl Free Number 1-800/529-6364 Fax 704/525-0409 Page 33 of 35
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29/07
B-I
184956
G0607542
06/19/07
06/19/07
Analyst Batch
30.27 mL 3550B 06/22/07 1100 dpope P18710
MsyjCP
hromium
Lad
Surrogate Recovery Control Limits
o-Terphenyl 83 40 140
2-Fluorobiphenyl 91 40 140
2-Bromoriaphthalene 90
l-Chloro-octadecane 92 40 140
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrooiçRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-8001529-6364 Fax 704/525-0409
ervice Anulytical L..ronmnntaI Solutions
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1700
1735
Parameter Result Units Report MDL Dilution Method Analysis
Limit Factor Date/Time ID
Phenanthrene 0.38 mg/kg 0.40 0.020 8270C 06/26/07 2053 kcampigotto Q24532
Phenol BRL mg/kg 0.40 0.044 8270C 06/26/07 2053 kcampigotto Q24532
Pyrene 0.49 mg/kg 0.40 0.027 8270C 06/26/07 2053 kcampigotto Q24532
Sample Preparation
Surrogate Recovery Control Limits
2-Fluorobiphenyl 78 21 108
73 14-103Nitrobenzene-d5
Terphenyl-dl
246-Tribromophenol
106
91
41 136
25-123
2-Fluorophenol 63 14-89
Phenol-d5 74 13-95
Extractable Petroleum Hydrpcarbons by GC-FID
r11C22 Aromatics BRL mg/kg 12 6.4 MADEP EPH 06/24/07 559 grappaccioll
19-C36 Aliphatics BRL mg/kg 12 1.8 MADEP EPH 06/24/07 559 grappaccioli
C9-C18 Aliphafics BRL mg/kg 12 3.8 MADEP EPH 06/24/07 559 grappaccioli
Analysis Note for Cll-C22 Aromatics
Sample Preparation
Adjusted value
10.44 mL EPH
Q24514
Q24514
Q24514
06/21/07 800 grappaccioli P15703
32 mg/kg
23 mg/kg
0.27 0.016
0.27 0.023
40.140
601DB
6010B
06/25/07 1402 mcampbell
06/25/07 1402 mcampbeli
Q24519
Q24519
Page 340135
99012 Laboratory Report
NC Drinking Water Cert No 37735 06/29/07
SnMce Analytical Environmental Soluti
ESP Associates PA Project ID Morehead Commons No Client Sample ID B-i
Attn Chris Ward Prism Sample ID 184956Box7030SampleMatrixSoilCOCGroupG0607542
Charlotte NC 28241 Time Collected 06/19/07 1700
Time Submitted 06/19/07 1735
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Sample Preparation 2.27 50 mL 3050B 06/21/07 905 jhoppel P18702
Yolatile Petroleum Hydrocarbons by GC-PID/FID
C5-C8Aliphatics BRL mg/kg 6.2 1.2 MADEP VPH 06/27/07 1922 hwagner Q24604
C9-Clo Aromatics BRL mg/kg 6.2 0.037 MADEP VPF-l 06/27/07 1922 hwagner Q24604
C9-Cl2Aliphatics BRL mg/kg 6.2 1.9 MADEPVPH 06/27/07 1922 hwagner Q24604
Analysis Note for C5-C8 Aliphatics Adjusted value
Analysis Note for C9-C12 Aliphatics Adjusted value
Surrogate Recovery Control Limits
25-Dibromotoluene-PID 94 70 130
25-Dibromotoluene-FID 125 70 130
Sample weight Determination --c---
Weight 1694 MADEP VPH 06/26/07 000-Ibrown
Weight 18.28 MADEP VPH 06126/07 000 brown
Sample Comments
BRL Below Reporting Limit
I-Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanVELACcertificationexceptforthoseinstances indicated in the case narrative and/or test commentsAllresultsarereportedondry-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page 35 of 35
NC Certification No 402 Lev II QC ReportSCCertificationNo99012
6/29/07NCDrinkingWaterCertNo37735
Full Service Analytical Envirnnmentat SoluLns
ESP Associates PA Project ID Morehead Commons No COC Group Number G0607542AttnChrisWard
Date/Time Submitted 6/19/07 1735Box7030
Charlotte NC 28241
Ytfle Organic mpounds byGcIMS method 82O
Method Blank
QCBatchResultRLcontrolLimitUnitsID
ll1-Trjchloroethane ND 0.005 0.0025 mg/kg 0245031122-Tetrachloroethane ND 0.005 0.0025 mg/kg 024503112-Trichloroethane ND 0.005 0.0025 mg/kg 024503
l-Dichloroethane ND 0.005 0.0025 mg/kg 024503I-Dichloroeene ND 0.005 0.0025 mg/kg 024503
I-Dichloropropene ND 0.005 0.0025 mg/kg 024503
l23-Trichlorobenzene ND 0.005 0.0025 mg/kg Q24503
I23-Trichloropropane ND 0.005 0.0025 mg/kg 024503I24-Trichlorobenzene ND 0.005 0.0025 mg/kg Q24503l24-Trimethylbenzene ND 0.005 0.0025 mg/kg 024503l2-Dibromoethane EDB ND 0.005 0.0025 mg/kg 024503l2-Dichlorobenzene ND 0.005 0.0025 mg/kg 0245032-Diohloroen ND 0.005 0.0025 mg/kg 024503I2-Dichloropropane ND 0.005 0.0025 mg/kg Q24503I35-Trimethylbenzene ND 0005 0025 mg/kg 024503l3-Dicfikobenene ND 0.005 O.Ot25 iig/k Q2403I3-Dichloropropane ND 0.005 0.0025 mg/kg 024503I4-Dichlorobenzene ND 0.005 0.0025 mg/kg Q2450322-Dichloropropane ND 0.005 0.0025 mg/kg Q245032-Chlorotoluene ND 0.005 0.0025 mg/kg 0245032-Hexanone ND 0.05 0.025 mg/kg 0245034-Chlorotoluene ND 0.005 0.0025 mg/kg 0245034-Methyl-2-pentanone MIBK ND 0.05 0.025 mg/kg 024503AcetoneND0.05 0.025 mg/kg 024503BenzeneND0.003 0.0015 mg/kg Q24503BromobenzeneND0.005 0.0025 mg/kg Q24503BromochioromethaneND0.005 0.0025 mg/kg 024503BromodichioromethaneND0.005 0.0025 mg/kg Q24503BromoforniND0.005 0.0025 mg/kg 024503BromomethaneND0.01 0.005 mg/kg 024503CarbontetrachlorideND0.005 0.0025 mg/kg 024503ChlorobenzeneND0.005 0.0025 mg/kg 024503ChlorodibromomethaneND0.005 0.0025 mg/kg Q24503ChioroethaneND0.01 0.005 mg/kg Q24503
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page of 12
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Method Blank
Chloroform
Chloromethane
cis-i 2-Dichloroethen
cis-i 3-Dichloropropene
Dichlorodjfluoromethane
Ethylbenzene
Isopropyl ether IPE
lsopropylbenzene
mp-Xylenes
Methyl ethyl ketorie MEK
Methyl t-butyl ether MTBE
Methylene chloride
n-Butylbenzene
n-Propylbenzene
Naphthalene
tert-Butylbenzene
Tetrachioroethene
Toluene
trans-I 2-Dichloroethene
trans-i 3-Dichloropropene
Trichioroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
ND 0.005 0.0025
0.0025
0.0025
0.0025
0.0025
0.0025
0.0125
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Q24503
024503
Q24503
024503
024503
Q24503
024503
024503
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level QC Report
6/29/07
Project ID Morehead Commons No COC Group Number G0607542
Date/Time Submitted 6/19/07 1735
Result RL Control Limit Units
QC Batch
ID
ND 0.005 0.0025 mg/kg 024503
ND 0.005 0.0025 mg/kg 024503
ND 0.005 0.0025 mg/kg 024503
ND 0.005 0.0025 mg/kg 024503
ND 0.005 0.0025 mg/kg 024503
ND 0.005 0.0025 mg/kg 024503
ND 0.005 0.0025 mg/kg 024503
ND 0.005 0.0025 mg/kg 024503
ND 0.01 0.005 mg/kg 024503
ND 0.1 0.05 mg/kg 024503
ND 0.01 0.005 mg/kg 024503
ND 0.005 0.0025 mg/kg 024503
ND 0.005 0.0025 mg/kg 024503
ND 0.005 0.0025 mg/kg 024503ND0.01 0.005 mg/kg Q24503
o-Xylene ND 0.005 0.0025 mg/kg 0245C3
PIsopropyltoiuene ND 0.005 0.0025 mg/kg Q24503
sec-Butylbenzene ND 0.005 0.0025 mg/kg Q24503
Styrene ND /k 0245030.005
ND 0.005
0.0025
0.0025
ND 0.005
ND 0.005
ND 0.005
ND 0.005
ND 0.005
ND 0.025
ND 005 0025 mg/kg Q24503
QC BachRangesResultSpikeAmountUnitsID
ll-Dichloroethene 0.05169 0.05 mg/kg 103 57-122 024503Benzene0.04711 0.05 mg/kg 94 62-119 024503Chlorobenzene0.0466 0.05 mg/kg 93 61-124 Q24503Toluene0.0443 0.05 mg/kg 89 57-122 Q24503Trichloroethene0.04755 0.05 mg/kg 95 59-129 024503
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbroolçRoad P.O Box 240543 Charlotte NC 28224-0543Phone7041529-6354 Toll Free Number 1800J529-5354 Fax 7041525-0409 Page of 12
NC Certificaon No 402 Level QC ReportScCertificationNo99012
6/29/NC Drinking Water Cert No 37735
ESP Associates PA Project ID Morehead Commons No COC Group Number G0607542
Attn Chris Ward Date/Time Submitted 6/19/07 1735Box 7030
Charlotte NC 28241
Matrix Spike
Recovery DC BatchSample ID Result Spike Amount Units ID
184829 11 -Dichloroethene 0.04873 0.05 mg/kg 97 44-140 Q24503
Benzene 0.04413 0.05 mg/kg 88 46-136 Q24503
Chlorobenzene 0.04321 0.05 mg/kg 86 47-135 Q24503
Toluene 0.03721 0.05 mg/kg 74 47-1 36 Q24503Trichloroethene0.04365 0.05 mg/kg 87 45-141 Q24503
Matrix Spike Duphcate
Recovery RPD Range DC BatchSample ID Result Spike Amount Units
0/0/0/ID
184829 l1-Dichloroethene 0.04634 0.05 mg/kg 93 44-140 -23 Q245o3Benzene0.042 0.05 mg/kg 84 46-1 36 -22 Q24503
Chlorobenzene 0.041 75 0.05 mg/kg 84 47-135 -22 Q24503Toluene0.04015 0.05 mg/kg 80 47-1 36 -22 Q24503
Trichloroethene 0.04154 0.05 mg/kg 83 45-1 41 -23 Q24503
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page of 12
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No
Level QC Report
6/29/0
COC Group Number G0607542
Date/Time Submitted 6/19/07 1735
Volatile Orcianic ComDounds by GC/MS method 8260B
Method Blank
QC Batch
to
11 1-Trichjoroethane
Result RL Control Limit Units
ND 0.005 0.0025 mg/kg 024504
ll22-Tetrachloroethane ND 0.005 0.0025 mg/kg Q24504
11 2-Trichloroethane ND 0.005 0.0025 mg/kg 024504
1-Dichloroethane ND 0.005 0.0025 mg/kg Q24504
1-Dichloroethene ND 0.005 0.0025 mg/kg Q24504
1-Dichloropropene ND 0.005 0.0025 mg/kg Q24504
23-Trichtorobenzene ND 0.005 0.0025 mg/kg 024504
l23-Trichloropropane ND 0.005 0.0025 mg/kg 024504
I24-Trichlorobenzene ND 0.005 0.0025 mg/kg Q24504
24-Trimethylbenzene ND 0.005 0.0025 mg/kg 024504
l2-Dibromoethane EDB ND 0.005 0.0025 mg/kg 024504
2-Dichlorobenzene ND 0.005 0.O05 mg/kg 024504
l2-Dichloroethane ND 0.005 0.0025 mg/kg 024504
2-Dichloropropane ND 0.005 0.0025 mg/kg 024504
l3.5-Trimethylbenzene ND 0.005 0.0025 mg/kg Q24504DichInrnhnn
fl fl flflc mn/It 024504
024504
024504
024504
Q24504
Q24504
Q24504
Q24504
024504
024504
024504
Q24504
Q24504
024504
024504
Q24504
Q24504
Q24504
024504
.._
3-Dichloropropan ND 0.005 0.0025 mg/kg
4-Dichlorojenz ND 0.005 0.0025 mg/kg
22-Dichloropropane ND 0.005 0.0025 mg/kg
2-Clijorotoluene ND 0.005 0.0025 mg/kg
2-Hexanone ND 0.05 0.025 mg/kg
4-Chiorotoluene ND 0.005 0.0025 mg/kg
4-Methyl-2pentanone MIBK ND 0.05 0.025 mg/kg
Acetone ND 0.05 0.025 mg/kg
Benzene ND 0.003 0.0015 mg/kg
Bromobenzene ND 0.005 0.0025 mg/kg
Bromochioromethane ND 0.005 0.0025 mg/kg
Bromodichioromethane ND 0.005 0.0025 mg/kg
Bromoform ND 0.005 0.0025 mg/kg
Bromomethane ND 0.01 0.005 mg/kg
Carbon tetrachloride ND 0.005 0.0025 mg/kg
Chlorobenzene ND 0.005 0.0025 mg/kg
Chiorodibromomethane ND 0.005 0.0025 mg/kg
Chloroethane ND 0.01 0.005 mg/kg
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbroojçRoadP.O Box 240543 Charlotte NC 282240543Phone704/529-6364 Toll Free Number 1-800/529.6364 Fax 704/525.0409 Page of 12
NC Certification No 402 Level QC ReportScCertificationNo99012
6/29/07NCDrinkingWaterCertNo37735
ESP Associates PA
Project ID Morehead Commons No COC Group Number G0607542AttnChrisWardDate/Time Submitted 6/19/07 1735O.Box7030
Charlotte NC 28241
Method Blank
QC BatchResultRLControlLimitUnitsID
Chloroform ND 0.005 0.0025 mg/kg 024504
Chloromethane ND 0.005 0.0025 mg/kg 024504
cis-1 2-Dichloroethene ND 0.005 0.0025 mg/kg 024504
cis-i 3-Dichloropropene ND 0.005 0.0025 mg/kg 024504
Dichlorodifluoromethane ND 0.005 0.0025 mg/kg 024504
Ethylbenzene ND 0.005 0.0025 mg/kg Q24504
Isopropyl ether IPE ND 0.005 0.0025 mg/kg 024504
lsopropylbenzene ND 0.005 0.0025 mg/kg Q24504
mp-Xylenes ND 0.01 0.005 mg/kg 024504
Methyl ethyl ketone MEK ND 0.1 0.05 mg/kg 024504
Methyl t-butyl ether MIBE ND 0.01 0.005 mg/kg Q24504
Methylene chloride ND 0.005 0.0025 mg/kg 024504
n-Butylbenzene ND 0.005 0.0025 mg/kg Q24504
n-Propylbenzene ND 0.005 0.0025 mg/kg 024504
Naphthalene ND 0.01 0.005 mg/kg 024504
o-Xylene ND 0.005 0.0025 mg/kg Q24504
.PiSppropyEtoluene-NP Q0O5 _.Q.Q025 mg/kg 024504
sec-Butylbenzene ND 0.005 0.0025 mg/kg 024504
Styrene ND 0.005 0.0025 mg/kg 024504
tert-Butylbenzene ND 0.005 0.0025 mg/kg 024504
Tetrachioroethene ND 0.005 0.0025 mg/kg 024504TolueneND0.005 0.0025 mg/kg Q24504transl2DjchloroetheneND0.005 0.0025 mg/kg 024504trans-i3-Dichloropropene ND 0.005 0.0025 mg/kg 024504TrichioroetheneND0.005 0.0025 mg/kg Q24504TrichiorofluoromethaneND0.005 0.0025 mg/kg 024504VinylacetateND0.025 0.0125 mg/kg 024504
0.005 0.0025 mg/kg
Recovery Recovry
QCBthResultSpikeAmountUnitsanges
ID
ll-Dichloroethene 0.05154 0.05 mg/kg 103 57-122 024504Benzene0.05232 0.05 mg/kg 105 62-119 Q24504Chlorobenzene0.05096 0.05 mg/kg 102 61-124 024504Toluene0.04808 0.05 mg/kg 96 57-1 22 Q24504Trichloroetherie0.05331 0.05 mg/kg 107 59-129 024504
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbroojçRoadP.O Box 240543 Charlotte NC 28224.0543Phone704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page of 12
Put ServIce Analytical Environmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Recovery Recovery QCBatch
Units
ID
mg/kg 83 44-140 Q24504
mg/kg 85 46-1 36 Q24504
mg/kg 68 47-1 35 Q24504
mg/kg 75 47-136 Q24504
mg/kg 86 45-141 Q24504
184929 11-Dichloroethene 0.04141 0.05
Benzene 0.0423 0.05
Chloroberizene 0.034 0.05
ToluenŁ 0.0377 0.05
Trichloroethene 0.04296 0.05
Matrix Spike Duplicate
Recovery Recovery RPD QC BatchSampleIDResultSpikeAmountUnitsID
184929 11-Dichloroethene 0.03788 0.05 mg/kg 76 44-140 23 Q24504
Benzene 0.03917 0.05 mg/kg 78 46-136 22 Q24504
Chiorobenzene 0.03223 0.05 mg/kg 64 47-135 -22 Q24504
TolUene 0.03417 0.05 mg/kg 68 47-136 10 22 Q24504
Trichloroethene 0.03959 0.05 mg/kg 79 45-141 -23 Q24504
Extractable Petroleum Hydrocarbons by GC-FID method MADEP EPH
Method Blank
QCBatchResultRLControlUmitUnitsID
l1-C22Aromafics ND 10 mg/kg 024514
O19-C36AIiphatics ND mg/kg Q24514
C9-C18 Aliphatics ND 10 mg/kg Q24514
Laboratory Control Sample
Recovery ecovery QC BatchRangesResultSpikeAmountUnitsID
Cll-C22Aromatics 140.16 170 mg/kg 82 40-140 Q24514
C19-C36Aliphatics 66.18 80 mg/kg 83 40-140 Q24514
C9-Cl8Aliphatics 44.82 60 mg/kg 75 40-140 Q24514veryMatrixSpike
Recovery Ranges QC BatchSampleIDResultSpikeAmountUnitsID
184697 C11-C22 Aromatics 135.2 170 mg/kg 80 40-140 Q24514C19-C36 Aliphatics 76.88 80 mg/kg 96 40-140 Q24514C9-C18 Aliphatics 46.94 60 mg/kg 78 40-140 Q24514
Ranges RPD Range QC BatchSampleIDResultSpikeAmountUnitsID
184697 Cll-C22Aromatics 146.88 170 mg/kg 86 40-140 0-50 Q24514
C19-C36Aliphatjcs 63.12 80 mg/kg 79 40-140 20 0-50 Q24514
C9-Cl8Aliphatics 41.44 60 mg/kg 69 40-140 12 0-50 Q24514
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Level QC Report
6/29/07
Matrix Spike
Sample 10
Result Spike Amount
Project ID Morehead Commons No COC Group Number G0607542
DatelTime Submitted 6/19/07 1735
Page of 12
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Q24519veMatrixSpike
Recovery Ranger QC BatchSample ID Result Spike Amount Units ID
184957 Chromium 41.1677 20.746 mg/kg 102 75-125 024519
Lead 37.9519 20.746 mg/kg 110 75-125 024519ORpOMatrixSpikeDuplicate
Recovery lan RPD Range OC BatchSampelDResultSpikeAmountUnitsID
184957 Chromium 42.4881 23.255 mg/kg 97 75-125 20 Q24519
Lead 35.0702 23.255 mg/kg 86 75-125 20 Q24519
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level QC Report
6129/07
Project ID Morehead Commons No COC Group Number G0607542
Date/Time Submitted 6/19/07 1735
Metals by ICP method 6010B
Method Blank
Result
Chromium 0.0507
Lead
Laboratory Control Sample
RL Control Umit Units
0.25 0.125
0.3843 0.25 0.125
mg/kg
mg/kg
Result Spike Amount
Chromium 24.9411 25
Lead 24.4983 25
QC Batch
ID
Recovery Recovery
RangesUnits
024519
Q2451
QC Batch
ID
Q24519mg/kg 100 80-120
mg/kg 98 80-1 20
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page 7of12
NC Certification No.402 Level QC ReportScCertificationNo99012
6/29/07NCDrinkingWaterCertNo37735
ESP Associates PA
Project ID Morehead Commons No COC Group Number G0607542AttnChrisWard
Date/Time Submitted 6/19/07 1735Box7030
Charlotte NC 28241
Semi-volatile Organic Compounds by GC/MS method 8270C
Method Blank
QC BatchResultRLControlLimitUnitsID
24-Trichlorobenzene ND 0.33 0.165 mg/kg Q24532
2-Dichlorobenzene ND 0.33 0.165 mg/kg 024532
3-Dichlorobenzene ND 0.33 0.165 mg/kg Q24532
4-Dichlorobenzene ND 0.33 0.165 mg/kg Q24532
245-Trichlorophenol ND 0.33 0.165 mg/kg 024532
246-TrichlorophenoI ND 0.33 0.165 mg/kg Q24532
24-Dichiorophenol ND 0.33 0.165 mg/kg Q24532
24DimethyIphenoI ND 0.33 0.165 mg/kg Q24532
24-Dinitrophenol ND 1.65 0.825 mg/kg 024532
24-Dinitrotoluene ND 0.33 0.165 mg/kg Q24532
26-Dinitrotoluene ND 0.33 0.165 mg/kg Q24532
2-Chloronaphthalene ND 0.33 0.165 mg/kg 024532
2-Chlorophenol ND 0.33 0.165 mg/kg Q24532
2-Methylnaphthajene ND 33 0.165 mg/kg Q24532
2-Methyiphenol ND 0.33 0.165 mg/kg Q245322hj--ND-033 0.i5 mg/kg ---Q2453234-Methylphenol ND 0.33 0.165 mg/kg Q24532
33-Dichlorobenzidine ND 0.66 0.33 mg/kg Q24532
4.6-Dinitro-2methylphenoI ND 1.65 0.825 mg/kg Q24532
4-Bromophenylphenylether ND 0.33 0.165 mg/kg Q24532
4-ChIoro-3-methylphenol ND 0.66 0.33 mg/kg 0245324-Chioroaniline ND 0.33 0.165 mg/kg Q24532
4.Chlorophenylpheflylether ND 0.33 0.165 mg/kg 0245324-Nitrophenol ND 1.65 0.825 mg/kg Q24532AcenaphtheneND0.33 0.165 mg/kg Q24532AcenaphthyleneND0.33 0.165 mg/kg Q24532AnthraceneND0.33 0.165 mg/kg Q24532AzobenzeneND1.65 0.825 mg/kg 024532BenzoaanthraceneND0.33 0.165 mg/kg 024532BenzoapyreneND0.33 0.165 mg/kg 024532BenzobfluorantheneND0.33 0.165 mg/kg 024532BenzoghiperylenND0.33 0.165 mg/kg 024532Benzokfjuoran5flND0.33 0.165 mg/kg Q24532BenzoicacidND1.65 0.825 mg/kg Q24532
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrooçRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6394 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page of 12
NC Certification No 402 Level QC ReportScCertificationNo99012
6/29/07NCDrinkingWaterCertNo37735
ESP Associates PA Project ID Morehead Commons No COC Group Number G0607542AttnChrisWardDate/Time Submitted 6/19/07 1735P.O.Box7030
Charlotte NC 28241
Method Blank
Result RL control Limit
Benzyl alcohol ND 0.66 0.33
Bis2-chloroethoxymethane ND 0.33 0.165
Bis2-chloroethylether ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165
ND 0.33 0.165 024532
Di-n-butylphthalate ND 0.33 0.165 024532
Di-n-octylphthalate ND 0.33 0.165 Q24532
Dibenzoahanthracane ND 0.33 0.165 mg/kg 024532
Dibenzofuran ND 0.33 0.165 mg/kg 024532
Diethylphthalate ND 0.33 0.165 mg/kg Q24532
Dimethylphthalate ND 0.33 0.165 mg/kg Q24532
Fluoranthene ND 0.33 0.165 mg/kg 024532
Fluorene ND 0.33 0.165 mg/kg 024532HexachlorobenzeneND0.33 0.165 mg/kg 024532
i-lexachorobutadjene ND 0.165 mg/kg 024532
Hexachiorocyclopentadiene ND 0.33 0.165 mg/kg 024532
Hexachioroethane ND 0.33 mg/kg 024532lndeno123-cdpyrene ND 0.33 mg/kg 024532
lsophorone ND 0.33
ND 0.33
ND 0.33
ND 0.33
ND 0.33
ND 1.65
ND 0.33
ND 0.33
atontrolSampl_0.33 0.165 mg/kg
Recove Recovery
024532
Ranges QC BatchResultSpikeAmountUnitsID
l24-Trichlorobenzene 1.24550 1.6658 mg/kg 75 39-98 024532l4-Dichlorobenzene 1.15622 1.6658 mg/kg 69 37-95 Q2453224-Dinitrotoluene 1.71 685
1.14223
1.42271 mg/kg 85 45-111
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrooçRoad P.O Box 240543 Charlotte NC 28224-0543Phone704/529-6394 Toll Free Number 1-800/529-6364 Fax 7041525-0409
Units
Bis2-chloroisopropylether
Bis2-ethylhoxylphthalate
Butylbenzylphthalate
Chrysene
oc Batch
ID
Q24532
024532
024532
024532
024532
024532
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
0.165
0.165
0.165
0.165
0.165
0.165
N-NitrosodinpropyIamine
N-Nitrosodiphenylamjne
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
0.165
0.825
0.165
0.165
024532
Q24532
024532
024532
024532
024532
024532
Q24532
2-Chlorophenol
4-Chloro-3methyfpheflol
1.6658
1.6658
1.6658
mg/kg 103 56-1 28
mg/kg 69 37-98
Q24532
Q24532
024532
Page of 12
NC Certification No 402 Level II QC ReportSCCertificationNo99012
6/29/07NCDrinkingWaterCertNo37735
lull Service Analytical Environmental Solutions
ESP Associates PA Project ID Morehead Commons No COG Group Number G0607542Attn Chris Ward Date/Time Submitted 6/19/07 1735Box7030
Charlotte NC 28241
Laboratory Control Sample
Recovery Isnge QC BatchResultSpikeAmountUnitsID
4-Nitrophenol 1.60359 1.6658 mg/kg 96 20-157 024532
Acenaphthene 1.44903 1.6658 mg/kg 87 44-110 Q24532
N-Nitrosodinpropyjamine 1.33710 1.6658 mg/kg 80 38-101 024532
Pentachlorophenol 1.78014 1.6658 mg/kg 107 53-127 Q24532
Phenol 1.13091 1.6658 mg/kg 68 34-102 Q24532
Pyrene 1.63091 1.6658 mg/kg 98 54-131 Q24532oveMatrixSpike
Recovery oc BatchRangesSamle1DResultSpikeAmountUnitsID
184696 24-Trichlorobenzene 1.18009 1.6647 mg/kg 7j 26-97 024532
4-Dichlorobenzene 1.14813 1.6647 mg/kg 69 23-92 024532
24-Dinitrotoluene 1.57856 1.6647 mg/kg 95 45-127 024532
2-Chiorophenol 1.13681 1.6647 mg/kg 68 25-94 Q24532
4-Chloro-3-methylphenol 1.29527 1.6647 mg/kg 78 31-113 Q24532
4-Nitrophenol 1.56225 1.6647 mg/kg 94 17-150 024532Acenaphthene1.34986 1.6647 mg/kg 81 36-107 024532
N-NltrosodInpropyJamine 1.21504 1.6647 mg/kg 73 22-1 05 Q24532Pentachiorophenol-1 1.664-7 mg/kg 106 39437-Q24532henol1.05525 1.6647 mg/kg 63 23-97 Q24532Pyrene1.52829 1.6647 mg/kg 92 45-133 Q24532
RPD OC BatchRangesRangeSampleIDResultSpikeAmountUnitsID
184696 l24-Trichlorobenzene 1.28538 1.6614 mg/kg 77 26-97 -37 024532l4-Dichjorobenzene 1.16843 1.6614 mg/kg 70 23-92 -36 Q2453224-Dinitrotoluene 1.59634 1.6614 mg/kg 96 45-127 -29 Q245322-Chlorophenol 1.19966 1.6614 mg/kg 72 25-94 -37 0245324-Chloro-3methyIphenol 1.34651 1.6614 mg/kg 81 31-113 -32 0245324-Nitrophenol 1.52624 1.6614 mg/kg 92 17-150 -32 Q24532Acenaphthene1.40598 1.6614 mg/kg 85 36-107 -32 Q24532
N-Nitrosodin.propyIamjne 1.22956 1.6614 mg/kg 74 22-105 0-37 024532Pentachlorophenol1.75913 1.6614 mg/kg 106 39-137 -27 024532Phenol1.04684 1.6614 mg/kg 63 23-97 -42 024532Pyrene1.61229 1.6614 mg/kg 97 45-133 -27 024532
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page 10 of 12
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No COC Group Number G0607542
Date/Time Submitted 6/19/07 1735
Volatile Petroleum Hydrocarbons by GC-PID/FJD method MADEP VPH
Method Blank
QC BatchResultRLControlLimitUnitsID
C5-C8 Aliphatics ND 2.5 mg/kg Q24582C9-C10 Aromatics ND 2.5 mg/kg Q24582
C9-Cl2Aliphatics ND 2.5 mg/kg Q24582
Laboratory Control Sample
Recovery Ran e1 QC BatchResultSpikeAmountUnitsID
C5-C8Aliphatics 17.766 15 mg/kg 118 70-130 Q24582C9-C1O Aromatics 5.138 mg/kg 103 70-130 Q24582
C9-Cl2Aliphatjcs 11.317 10 mg/kg 113 70-130 Q24582
Sample tO Result Spike Amount Units ID
184695 C5-C8 Aliphatics 15.220 15 mg/kg 101 70-1 30 Q24582C9-ClQAromatjce 4333 mg/kg 87 70-130 Q24582C9-C12 Aliphatics 12 157 10 mg/kg 122 70-1 30 Q24582XSpikeDupIic-
RPD
Ranges RPD Range QC BatchSampleIDResultSpikeAmountUnits
0/ID----0
15.067 15 -mg/kg 100--70-139 25 Q24582CO-ClOAromatics 4.446 mg/kg 89 70-130 0-25 Q24582C9-C12 Aliphafics 12.999 10 mg/kg 130 70-1 30 0-25 Q24582
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6354 Toll Free Number 1-800/529.6354 Fax 704/525-0409
Full Survice Analytical EnvIronmental
ESP Associates PA
Attn Chris Ward
O.Box7030
Charlotte NC 28241
Level II QC Report
6129/07
Page 11 of 12
NC Certification No 402 Level QC ReportSCCertificationNo99012
6/29/07NCDrinkingWaterCertNo37735
Analytical nvironmentat Solutions
ESP Associates PA Project ID Morehead Commons No COC Group Number G0607542
Attn Chris Ward Date/Time Submitted 6/19/07 1735Box7030
Charlotte NC 28241
Volatile Petroleum Hydrocarbons by GC-PID/FiD method MADEP VPH
Method Blank
QC BatchResultRLControlLimitUnitsID
C5-C8Aliphatics ND 2.5 mg/kg 024604
C9-C10 Aromatics ND 2.5 mg/kg 024604
C9-C12 Atiphatics ND 2.5 mg/kg 024604
ReseLaboratoryControlSample
Recovery Ra QC BatchResultSpikeAmountUnitsID
C5-C8Aliphatics 16.779 15 mg/kg 112 70-130 024604
C9-C10 Aromatics 4.305 mg/kg 86 70-1 30 024604C9-C12 Aliphatics 10.922 10 mg/kg 109 70-130 024604oveMatrixSpike
Recovery Ran QC ButchSampletDResultSpikeAmountUnitsID
184956 C5-C8 Aliphalics 16.625 15 mg/kg 111 70-130 024604
C9-ClOAron-jaflcs 4.148 mg/kg 83 70-130 024604
C9-Cl2Atiphatics 12.627 10 mg/kg 126 70-130 024604
Matrix Spike Duplicate
Recovery Range1 RPD Range OC BatchSample ID Result SptkeAmount Units IDi49aAlipcs17.96 15 mg/kg--120 70-130 --0-25024604
C9-ClOAromatjcs 4.279 mg/kg 86 70-130 0-25 024604C9-C12 Aliphatics 13.613 10 mg/kg 136 70-130 -25 024604-See Case Narrative
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbroojRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-800/529-6354 Fax 704/525-0409 Page 12 of 12
CHAIN OF CUSTODY RECORD
PAGE _L OF _L QUOTE USE PROPER BILüNG ________________
Project Name NOV2Ln.J Cn
Short Hold Analysis Yes No UST 9roject Yes NopleaseATTACHanyproject specific reporting QC LEVEL 111111 IVprovisionsand/or OC Requepnt
Invoice To
Address f4r14.ç
NO N/A
$ahipIe INTICT-upqriarftiaI
Received ONWET lCE Temp
PROPER PRESERVATIVES indicated
V.ReidwlTH1MHotDNGMEs --
-CUSTODY SEALSINTAct VVV
VOLATILES reed WJOUT I-IEADSPACE n.
PROPER CONTAINERS used
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC USACE FL____NCL
SC_OTHER ______N/A _____
Water Chlorinated YES_NO_
Sample Iced Upon Collection YES
Full Service Analytical Environmental Solutions
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Fax 704/9O4p
Client Company Name
Report To/Contact Name ________________________
Reporting Address
Phone ________________Fax Yes No
Email Yes No Email Address______________________
EDD Type PDF_Excel __Otlij
Site Location Name _________IMIrJWA it
Site Location Physical Address
Purchase Order No./Billing Reference
Requested Due Date Day 02 Days 03 Days thDays WDays
Working Days 06-9 Days Standard 10 days us Woi-kust Be
Samples received after 1500 will be processed next busires day
Turnaround time is based on business days excluding We4ends and holidaysSEEREVERSE FOR TERMS CONDITIONS REGARDIN ERVICESRENDERED BY PRISM LABORATORIES INC TO CLIENTh
CLIENT
SAMPLE DESCRIPTION
j-
L-.2
DATE
COLLECTED
-J9o
TIME MATRIX
COLLECTED SOIL
MILITARY
SLUDGE
/6ooJ4
PRESERVA-
TIVES
ANALYSES R1EQUETE
/b7//MA
eIJJ
LAB
ID NOSEE BELOW
DL/
NO SIZE
121
/i.cy$/fc
7cc J_
.-w
--/A4
Relinquished By Signature
Samplers Sampled By Print Name Affiliation
Upon relinquishing thisiain of Custody is your authorization for Prism to proceed with the analyses as requested4rnve Any changes must besubmittedinwritingtothePrismProjectManagerTherewillbechargesforanychangesafteranalyseshavebeeniniialized
Received ......._
Relinquished By Signature
Relinsh79natp
Method oj$tpment NOTBrLL SAMPLSAMPLES ARE No
OFedEx OUPS .d-delivered
COOLERS SHOULD BEACCEPTED AND VERIF
OPriamFisidService
Re ivect By Signature
sLaboratorie
TAPED SHUT 1S1TH STODY SEALS FOR
lED AGAINST COC UNTIL RECEIVED AT THE
OOther
RANPORTATION TO THE LABORATOYLABORATORY
Date
lTôGro No
c6qI
ijaw Military/I-tours Additional Comments
NPDES US1 GROUNDWATER DRINKING WATER SOLID WASTE RCRA CERCI4ONCOSCipicDSCIJNC080ONCIJSCONC OSC UNC IJSC 0NChLSC__________________rm
.itfçi4ITiriie
-Site Departure Time
V1d Tech Fee VVV
Mileag
LANDFILL OTHER
IJNC osc ONC OSC
SEE REVERSE FORTERMSCONDITIONS
CLIENT ES
A1TN vS
PRISM COC GROUP
Please fill in the Site Location information on the attached VPH and/or EPH Forms
\NaSO1\FOLD\COMMON\FORMS\VP EPH Site Location for Cllent.doc
Full Service Analyflcal EnvironentaI SoJutIon
VPH AliphaticslAromatics Laboratory Reporting Form
Client Name
Project Name
Site Location
ESP Associates PA
Morehead Commons No
Laboratory Name
NC Certification Lab
Sample Matrix
Prism Laboratories Inc
Unadjusted value should exclude the concentration of any surrogates internal standards and/orconcentrationsof other ranges that elute within the specified rangeAdjusted value
MDL Method Detection Limit RL Reporting Limit
Were all performance/acceptance standards for required QNQC
procedures achieved
Were any significant modifications to the VPH method madeCommentsVPHtripblankwasnotsubmittedto the laboratory
Method for Ranges MADEP VPHVPHF----ards
Samrle Information and Analytical Results
cation
Collection Option for soil
Date Collected
402
Soil
rnotoluer flbromc
Date Received
Date Extracted
Lt
ne
Date Analyzed
II
Dry Solids
184954
Dilution Factor
184955
Hydrocarbon Ranges in mg/kg
C5-C8 Aliphatics
C9-C12 AliDhatics
6/19/2007
6/19/2007
6/27/2007
6/27/2007
Sample Results
6.0
6.0
6.0
5.0
5.0
5.0
6/19/2007
6/1 9/200
6/27/2007
6/27/2007
74.3
Sample Results
6.7
6.7
6.7
5.0
5.0
5.0
C9-C10 Aromatics
Blank Lc5-C8 Aliphatics
C9-C12 Aliphatics
6/19/2007
6/19/2007
6/27/2007
6/27/2007
82.4
Sample Results
6.1
6.1
6.1
5.0
5.0
5.0RL
6/1 9/200
6/19/2007
6/27/2007
6/27/2007
84.9
Sample Results
5.9
5.9
5.9
5.0
5.0
5.0Aromatics
6/19/2007
6/19/2007
6/27/2007
6/27/2007
81.3
Sample Results
6.2
6.2
6.2
5.0
5.0
5.0
6.0
6.0
6.7
Surrogate Acceptance Range Blank
Aliphatic Surrogate Rec FID 130
Surrogate Rec PID 97
6.7
6.1
6.1
6.7
5.9
61
5.9
6.2
6.2
70-1 30
6.2
116
91
7J-130
114
Option Established fill line on vial
Option Sampling device indicate brand e.g EnCore TMOptionFieldweightofsoil
11287 121
70-130
125
94 94
Blank Laboratory Method Blank or Trip Blank
whichever is higher indicate type
YES iNo Details AttachedLNoIYesDetailsAttached
Page of VPH Soil
EPH Aliphatics/Aromatics Laboratory Reporting Form
Client Name
Project Name
Site Location
ESP Associates PA
Morehead Commons No
Laboratory Name
NC Certification Lab
Sample Matrix
Prism Laboratories Inc
402
Soil
Sample Information and Analytical Results
Method for Ranges MADEP EPH
EPH Surrogate Standards Aliphatic 1-Chloro-
EPH Fractionation Surrogates
Sample Identification
Date Collected
Date Received
Date Extracted
Date Analyzed
%Dry Solids
Dilution Factor
Hydrocarbon Ranges in ma/ka
C9-C18 Aliphatics
C19-C36 AIihatics
Cli-C22 Aromatics
MDL
C9-C18 Aliphatics
Cl 9-C36 Aliphatics
CI 1-C22 Aromatics
C9-C18 Aliphatics
Cl 9-C36 Aliphatics
Cl 1-C22 Aromatics
flClQ AI.-I..-.4
Aromatic Surrogate
Fractionation Surrogate Accep Range
ne Aromatic o-Terphenyl
me Fluorobiphenyl
184952 184953 184954 184955 184956
Blank
RL
6/19/2007 6/19/2007 6/19/2007 6/19/2007 6/19/2007
6/19/2007 6/1912007 6/19/2007 6/19/2007 6/19/2007
6/21/2007 6/21/2007 6/21/2007 6/21/2007 6/21/2007
6/23/2007 6/24/2007 6/24/2007 6/24/2007 6/24/2007
83.3 74.3 82.4 84.9 81.3
Sample Results Sample Results Sample Results Sample Results Sample Results1213 12 11 1212 13 12 11 12
13 13 130 11 1210 10 10 10 101010 10 10 10101010 10 10
12 13 12 11 12
12 13 12 11 12
12 13 12 11 12
3.8 3.6
94
116
Blank 40-140
86
81
40-140
87
122
40-140
90
40-140%40-140FracSurrogateRec118869712311490FracSurrogate2%Rec 120 88 99 103 116 91
Unadjusted value should exclude the concentration of any surrogates internal standards and/or
concentrations of other ranges that elute within the specified range
Adjusted value
MDL Method Detection Limit RL Reporting Limit Blank Laboratory Method Blank
Were all performance/acceptance standards for required QNQC
procedures achieved
Was blank correction applied as significant modification of the methodWereanysignificantmodificationstotheEPHmethodmade
Comments
YES No Details Attached
Yes NO
NO Yes Details Attached
Page of EPH Soil
JUL
Case NarrativePRISM
LABORATORIESINC
Date 07/16/07 Client Project ID Morehead Commons No
Company ESP Associates PA Prism COC Group No G0707086
Contact Chris Ward Collection Dates 07/05/07AddressBox 7030 Lab Submittal Dates 07/05/07
Charlotte NC 28241
This data package contains the analytical results for the project identified above and includes Case Narrative Laboratory Report and QualityControlDatatotalingpageschain-of-custody is also attached for the samples submitted to Prism for this project
Data qualifiers are flagged individually on each sample key
reference for the data qualifiers appears at the end of this case narrave Qualitycontrolstatements and/or sample specific remarks are included in the sample comments section of the laboratory report for each sampleaffected
Semi Volatile Analysis
No Anomalies Reported
Volatile Analysis
N/A
Metals Analy
N/A
Wet Lab and Micro Analysis
N/A
Please call if you have any questions relating to this analycal report
Pate.ReviE wed by Robbi Jones Project Manager igela lrOVŁrcash
Review Date 07/16/07 Approval Date 07116/07
Data Qualifiers Key Reference
Compound also detected in the method blank
Result outside of the OC limits
DO Compound diluted out
Estimated concentration calibration range exceeded
The analyte was positively identified but the value is estimated below the reporting limit
Estimated concentraon with high bias
Estimated concentration with low bias
matrix effect is present
Notes This report should not be reproduced except in its enfirety without the writtten consent of Prism Laboratories Inc The results in thisreportrelateonlytothesamplessubmittedforanalysis
449 Springbnok Road P.O Box 240543 Chariott.e NC 28224-0403
Phone 704/529-6364 Toll Free 800/529-6364 Fax 7041525-0409
Ecu Service Analytical Environment...olutlons
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-3
186279
G0707086
07/05/07 1430
07/05/07 1520
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
07/13/07
Result Units Report MDL Dilution
Limit Factor
Method Analysis
Date/Time
Analyst Batch
ID
SM2540 07/10/07 1300 athao
82700 07/13/07 743 kcampigotto 024946
82700 07/13/07 743 kcampigotto 024946
82700 07/13/07 743 kcampigotto Q24946
8270C 07/13/07 743 kcarnpigotto Q24946
8270C 07/13/07 743 kcampigotto 024946
8270C 07/13/07 743 kcampigotto 024946
8270C 07/13/07 743 kcampigotto Q24946
Parameter
Percent Solids Determination
Percent Solids 92.0
Semi-volatile Orcianjc Compounds by GC/MS
124-Trjchlorobenzene BRL mg/kg 0.36 0.035
12-Dichlorobenzene BRL mg/kg 0.36 0.026
13-Dichlorobenzene BRL mg/kg 0.36 0.026
14-Dichlorobenzene BRL mg/kg 0.36 0.032
245-Trichiorophenol BRL mg/kg 0.36 0.036
246-Trichiorophenol BRL mg/kg 0.36 0.034
24-Dichiorophenol BRL mg/kg 0.36 0.030
24-Dimethyiphenol BRL mg/kg 0.36 0.034
24-Dinitropheriol BRL-mg/kg t8 a040 1-
24-Dinitrotoluene BRL mg/kg 0.36 0.020
26-Dinitrotofuene BRL mg/kg 0.36 0.038
2-Chloronaphthalene BRL mg/kg 0.36 0.037
2-Chiorophenol BRL mg/kg 0.36 0.028
2-Methylnaphthalene BRL mg/kg 0.36 0.028
2-Methylphonol BRL mgfkg 0.36 0.033
2-Nitrophenol BRL mg/kg 0.36 0.043
34-Methylphenol BRL mg/kg 0.36 0.036
33-DichJorobenzidine BRL mg/kg 0.71 0.022
6-Dinitro-2-methylphenol BRL mg/kg 1.8 0.022
4-Bromophenylphenylether BRL mg/kg 0.36 0.034
-Chloro-3-rnethylphenol BRL mg/kg 0.71 0.026
4-Chloroaniljne BRL mg/kg 0.36 0.046
-ChlorophenylphenyIether BRL mg/kg 0.36 0.022
4-Nitrophenol BRL mg/kg 1.8 0.024
8270C 07/13/07 743 kcampigotto 024946
-827OC 07/-i 3/07 743 kcampigotto 024946
8270C 07/13/07 743 kcampigotto 024946
8270C
82700
8270C
82700
8270C
8270C
8270C
8270C
8270C
8270C
82700
82700
8270C
8270C
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
07/13/07 743
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
kcampigotto
keampigotto
kcampigotto
kcampigotto
kcampigotto
keampigotto
kcampigotto
kcampigotto
024946
Q24946
Q24946
024946
024946
Q24946
024946
024946
024946
024946
024946
024946
Q24946
024946
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page of4
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
WS-3
186279
G0707086
07/05/07 1430
07/05/07 1520
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
07/13/07
Parameter
Analyst Batch
ID
Result Units Report MDL Dilution Method Analysis
Limit Factor Date/Time
Acenaphthene BRL mg/kg 0.36 0.035 8270C 07/13/07 743 kcampigotto Q24946
Acenaphthytene BRL mg/kg 0.36 0.035 8270C 07/13/07 743 kcampigotto Q24946
Anthracene BRL mg/kg 0.36 0.027 827CC 07/13/07 743 kcampigotto Q24946
Azobenzene BRL mg/kg 1.8 0.033 8270C 07/13/07 743 kcampigotto Q24946
Benzoaanthracene BRL mg/kg 0.36 0.050 827CC 07/13/07 743 kcampigotto Q24946
Benzoapyrene BRL mg/kg 0.36 0.041 827CC 07/13/07 743 kcampigotto 024946
Benzobfluoranfhene BRL mg/kg 0.36 0.016 827CC 07/13/07 743 kcampigotto Q24946
Benzoghiperylene BRL mg/kg 0.36 0.017 827CC 07/13/07 743 kcampigotto 024946
Benzokfiuoranthene BRL mg/kg 0.36 0.029 827CC 07/13/07 743 kcampigotto 024946
Benzoic acid BRL mg/kg 1.8 0.15 827CC 07/13/07 743 kcampigotto 024946
Benzyl alcohol BRL mg/kg 0.71 0.038 827CC 07/13/07 743 kcampigotto Q24946
9isi2-chIoethoxyethane .RL rng/kg_0.36 0.041 827CC 07/13/07 743 kcampigotto Q249463cthØk92T0T2Th7T13ka5ffö244
Bis2-chloroisopropylether BRL mg/kg 0.36 0.030 827CC 07/13/07 7.43 kcampigotto Q24946
3is2-ethylhexylphthalate BRL mg/kg 0.36 0.018 8270C 07/13/07 743 kcampigotto Q24946
Butylbenzylphthalate BRL mg/kg 0.36 0.022 827CC 07/13/07 743 kcampigotto 024946
Thryserie BRL mg/kg 0.36 0.059 827CC 07/13/07 743 kcampigotto 024946
Di-n-butylphthajate BRL mg/kg 0.36 0.016 827CC 07/13/07 743 kcampgouo Q24946
i-n-octylphthalate BRL mg/kg 0.36 0.027 8270C 07/13/07 743 kcampigotto 024946
iiibenzoahanthracene BRL mg/kg 0.36 0.036 827CC 07/13/07 743 kcampigotto 024946
ibenzofuran BRL mg/kg 0.36 0.031 8270C 07/13/07 743 kcampigotto 024946
iethylphthaIate BRL mg/kg 0.36 0.022 827CC 07/13/07 743 kcampigotto 024946
Dimethylphthalate BRL mg/kg 0.36 0.024 827CC 07/13/07 743 kcampigotto 024946
uoranthene 0.13 mg/kg 0.36 0.025 827CC 07/13/07 743 kcampigotto Q24946
Fluorene BRL mg/kg 0.36 0.021 827CC 07/13/07 743 kcampigotto 024946
exachlorobenzene BRL mg/kg 0.36 0.018 8270C 07/13/07 743 kcampigotto 024946
Hexachiorobutadiene BRL mg/kg 0.36 0.035 827CC 07/13/07 743 kcampigotto 024946
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page of
Project ID MorehØad Commons No Client Sample ID WS-3
Prism Sample ID 186279
Sample Matrix Soil COC Group G0707086
Time Collected 07/05/07 1430
Time Submitted 07/05/07 1520
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
_________Limit Factor Date/Time ID
l-lexachlorocyclopentadiene BRL mg/kg 0.36 0.038 827CC 07/13/07 743 kcampigotto Q24946
Hexachioroethane BRL mg/kg 0.36 0.036 827CC 07/13/07 743 kcampigotto Q24946
lndeno123-ccjpyrene BRL mg/kg 0.36 0.037 827CC 07/13/07 743 keampigotto Q24946
Isophorone BRL mg/kg 0.36 0.032 827CC 07/13/07 743 kcampigotto Q24946
N-Nitrosodi-n-propylamjne BRL mg/kg 0.36 0.040 827CC 07/13/07 743 kcampigotto Q24946
N-Nitrosodiphenylamjne BRL mg/kg 0.36 0.018 827CC 07/13/07 743 kcampigotto Q24946
Naphthalene BRL mg/kg 0.36 0.039 827CC 07/13/07 743 kcampgotto Q24946
Jitrobenzene BRL mg/kg 0.36 0.035 827CC 07/13/07 743 kcampigotto Q24946
Pentachiorophenol BRL mg/kg 1.8 0.030 827CC 07/13/07 743 kcampigotto Q24946
henanthrene BRL mg/kg 0.36 0.017 827CC 07/13/07 743 kcampigotto Q24946
Phenol BRL mg/kg 0.36 0.039 827CC 07/13/07 743 kcampigotto Q24946
0.17 mg/kg Q.36 Cr024 827CC 07/13/07 7.43 kcamgoffo 024946
Sample Preparation 30.16g mL 3550B 07/11/07 800 dpope P18865
txtractable Petroleum Hydrocarbons by GC-FID
C11-C22 Aromatics BRL mg/kg
Analysis Note for Cll-C22 Aromatics
L19-C36 Aliphatics BRL mg/kg
9-C18 Aliphatics BRL mg/kg
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
07/13/07
Surrogate Recovery Control Limits
Terphenyl-d14 104 41 136
Phenol-d5 64 13-95
Nitrobenzene-d5 69 14-103
2-Fluorophenol 61 14-89
2-Fluorobiphenyl 69 21 108
246-Tribromophenol 94 25 123
11 5.8 MADEP EPH 07/12/07 744 grappaccioli Q2491ctAdjustedvalue
11 1.6 MADEP EPH 07/12/07 744 grappaccioji Q2491o
11 3.5 MADEP EPH 07/12/07 744 grappaccioli 024910
Page of
Client Sample ID
Prism Sample ID
COC Group
Time Collected
Time Submitted
WS-3
186279
G0707086
07/05/07 1430
07/05/07 1520
Parameter Result Units Report MDL Analysis Analyst
Batch
Date/Time ID
Sample Preparation 10.06g mL EPH 07/09/07 1100 dpope P18855
Surrogate
o-Terphenyl
2-Fluorobiphenyl
2-Bromonaphthalene
-Chloro-octadecane
Recovery Control Limits
64
64
61
71
40-140
40-140
40-140
40-140
Sample Comments
BRL Below Reporting Limit
J-Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthoseinstancesindicatedinthecasenarrativeand/or test comments
.Altesultsarereportedoadryweighfbjs
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Full Jervice Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No
Sample Matrix Soil
Laboratory Report
07/13/07
Limit
Dilution
Factor
Method
Angela Overcash V.P Laboratory Services
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704525-0409 Page of
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
Attn Chris Ward
Box7030
Charlotte NC 28241
Extractable Petroleum Hydrocarbons by GC-FID method MADEP EPH
Method Blank
QC BatchResultRI.Control Linift Units ID
C11-C22Aromatjcs ND 10
Cl 9-C36 Aliphatics ND 10
C9-C18 All hatics ND 10 mg/kg Q24910LaboratoryControlSample
Recovery Ranges QC BatchResultSpikeAmountUnitsID
Cll-C22Aromatics 128.22 170 mg/kg 75 40-140 024910
41.94 80 mg/kg 52 40-140 024910C9-C18Aliphats 31 60 mg/kg 53 40-140 024910
QC BatchRangesSample ID Result Spike Amount Units /0 ID
186445 Cl 1-C22 Aromatics 137.74 170 mg/kg 81 40-140 024910
44.08 80 mg/kg 55 40-140 024910C9-C18 Aliphatics 32.06 60 mg/kg 53 40-140 024910
Sample ID Result Spike Amount Units ID/0
..ls6i44Sc1i-22Atomatics 119.T6 .170.mg/kg 70 40i4Q.-.14-0--SO-O2410Cl9-C36Aliphatics 52.7 80 mg/kg 66 40-140 18 0-50 02491037.12 60 mg/kg 62 40-1 40 15 0-50 024910
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrooj Road P.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-800/529-6364 Fax 7041525-0409
Lev QC Report
7/16/2007
Project ID Morehead Commons No COC Group Number G0707086
Date/Time Submitted 7/5/2007 1520
mg/kg
mg/kg
Cl 9-C36 Aliphatics
024910
024910
Cl 9-C36 Aliphatics
C9-C18 Aliphatics
Page of4
NC Certification No 402 Level QC ReportScCertificationNo99012
7/16/2007NCDrinkingWaterCertNo37735
Project ID Morehead Commons No COG Group Number G0707086
Date/Time Submitted 7/5/2007 1520
Semi-volatile Organic Comnounds by CC/MS method 8270C
QC BatchResultRLControlLimitUnitsID
l24-Trichlorobenzene ND 0.33 0.165 mg/kg Q249462-Dichlorobenzene ND 0.33 0.165 mg/kg 0249463-Dichlorobenzen ND 0.33 0.165 mg/kg Q249464-Dichjorobenzene ND 0.33 0.165 mg/kg Q2494624S-TrichlorophenoJ ND 0.33 0.165 mg/kg 02494624S-TrichlorophenoI ND 0.33 0.165 mg/kg Q2494624-Dichloropheno ND 0.33 0.165 mg/kg Q2494624-Dimethyjphenol ND 0.33 0.165 mg/kg 02494624-Dinitrophenoj ND 1.65 0.825 mg/kg 02494624-Dinitrotoluene ND 0.33 0.165 mg/kg Q2494626-Dinifrotoluene ND 0.33 0.165 mg/kg 0249462ChloronaphthaleneND0.33 0.165 mg/kg Q249462-Chlorophenol ND 0.33 0.165 mg/kg Q249462-Methylnaphthalene ND 0.33 0.165 mg/kg 0249462-tItyjhenoj ND 0.33 0.165 mg/kg Q24946----Nb-m/k
34-Methylphenol ND 0.33 0.165 mg/kg 02494633-DichJorobenzldine ND 0.66 0.33 mg/kg 02494646-Dinitro-2methyIphenoJ ND 1.65 0.825 mg/kg 0249464BromophenylphenyletheND0.33 0.165 mg/kg Q249464-ChIoro.3methylphenol ND 0.66 0.33 mg/kg 0249464-Chloroaniljne ND 0.33 0.165 mg/kg 0249464-Chlorophenylphenylether ND 0.33 0.165 mg/kg Q249464-Nitrophenol ND 1.65 0.825 mg/kg 024945AcenaphtheneND0.33 0.165 mg/kg Q24946AcenaphthyjeneND0.33 0.165 mg/kg 024946AnthraceneND0.33 0.165 mg/kg Q24946AzobenzeneND1.65 0.825 mg/kg 024946BenzoaanthraceneND0.33 0.165 mg/kg
Q24946BenzoapyreneND0.33 0.165 mg/kg Q24946BenzobfluontheneND0.33 0.165 mg/kg
Q24946BenzoghipeienND0.33 0.165 mg/kg
024946BenzokfluorantheneND0.33 0.165 mg/kg 024946BenzoicacidND1.65 0.825 mg/kg 024946
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringrRoadP.O Box 240543 Charlotte NC 28224-0543Phone7O4I529.63 Toll Free Number 1-800/529.6364 Fax 704/525-0409
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Page of
A__
Full Service Analytical Environmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
7/16/2007
Project ID Morehead Commons No COC Group Number G0707086
Date/Time Submitted 7/5/2007 1520
Result RL Control Limit Units
QC Batch
ID
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Method Blank
Benzyl alcohol ND 0.66 0.33 mg/kg Q24946
Bis2-chloroethoxymethane ND 0.33 0.165 mg/kg Q24946
Bis2-chloroethylether ND 0.33 0.165 mg/kg Q24946
Bis2-chloroisopropyjether ND 0.33 0.165 mg/kg Q24946
Bis2-ethylhexylphthalate ND 0.33 0.165 mg/kg Q24946
Butylbenzyjphthalate ND 0.33 0.165 mg/kg Q24946
Chrysene ND 0.33 0.165 mg/kg Q24946
Di-n-butylphthalate ND 0.33 0.165 mg/kg Q24946
Di-n-octylphthalate ND 0.33 0.165 mg/kg Q24946
Dibenzoahanthracene ND 0.33 0.165 mg/kg Q24946
Dibenzofuran ND 0.33 0.165 mg/kg Q24946
Diethylphthalate ND 0.33 0.165 mg/kg Q24946
Dimethylphthalate ND 0.33 0.165 mg/kg Q24946
Fluoranthene ND 0.33 0.165 mg/kg Q24946
Fluorene ND 0.33 0.165 mg/kg Q24946HexachlorobenzeneND0.33 0.165 mg/kg Q24946
iene -ND 033 0.165 mg/kg Q24946
HexathloroycIopentadiene ND 0.33 0.165 mg/kg Q24946F-lexachjoroethane ND 0.33 0.165 mg/kg Q24946Indeno123-cdpyrene ND 0.33 0.165 mg/kg Q24946lsophoroneND0.33 0.165 mg/kg Q24946
N-NitrosodinpropyIamine ND 0.33 0.165 mg/kg Q24946
N-Nitrosodiphenylamine ND 0.33 0.165 mg/kg Q24946NaphthaleneND0.33 0.165 mg/kg Q24946NitrobenzeneND0.33 0.165 mg/kg Q24946
Pentachlorophenol ND 1.65 0.825 mg/kg Q24946PhenanthreneND0.33 0.165 mg/kg Q24946PhenolND0.33 0.165 mg/kg Q24946PyreneND033165mg/kg Q24946
QCBatchRangesResultSpikeAmountUnitsID
l24-Trichlorobenzene 1.26414 1.6742 mg/kg 76 39-98 Q249464-Dichlorobenzene 1.22999 1.6742 mg/kg 73 3795 Q2494624-Dinitrotoluene 1.51188 1.6742 mg/kg oo 56-123 Q249462-Chlorophenol 1.41144 1.6742 mg/kg 84 37-98 Q249464-ChIoro-3methylphenoI 1.40709 1.6742 mg/kg 84 45-111 Q24946
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
4-Nitrophenol
Acenaphthene
N-Nitrosodi-n-propylamjne
Pentachlorophenol
Phenol
Result Spike Anount
0.97991 1.6742
1.29092 1.6742
1.38935 1.6742
1.941 74 1.6742
1.26146 1.6742
1.6537
1.6537
31-113
17-1 50
36-107
024946
024946
Q24946
024946
024946
024946
OC Batch
ID
Q24946
024946
Q24946
024946
024946
024946
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543Phone7O4/529-Toll Free Number 1-800/529-6364 Fax 704/525-0409
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Level QC Report
7116/2007
Project ID Morehead Commons No COC Group Number G0707086
Date/Time Submitted 7/5/2007 1520
ontrol Sample
Recovery Recovery
RangesUnits
0/
mg/kg
mg/kg
59
77
QC Batch
ID
20-1 57
44-110
mg/kg 83 38-101
mg/kg 116 53-127
mg/kg 75 34-102
Pyrene 1.54837 1.6742 mg/kg 92 54-131
Matrix Spike
Recovery Recovery
RangesSampleIDResultSpikeMiountUnits
186433 24-Trichlorobenzene 1.23412 1.6537 mg/kg 75 26-97 024946
4-Dichlorobenzen 1.13723 1.6537 mg/kg 69 23-92
24-Dinitrotoluene 1.65211 1.6537 mg/kg 100 45-127
2-Chlorophenol 1.14351 1.6537 mg/kg 69 25-94
4-Chloro-3-methylphenol 1.25562 1.6537 mg/kg 76
4-Nitrophenol 0.96197 mg/kg 58
Acenaphthene 1.28406 mg/kg 78
N-Nitrosodinpropylanijne 1.25661 1.6537 mg/kg 76 22-105 024946
Pentachlorophenol 1.88095 16537 mg/kg. 114 39-137 024946PhTj/k
Pyrene 1.44907 1.6537 mg/kg 88 45-133 024946MatrixSpikeDuplicate
Recovery Recovry
RPD Ige QC BatchSampleIDResultSpikeMiountUnitsVoID
186433 24-Trichlorobenzene 1.37073 1.6748 mg/kg 82 26-97 10 37 Q24946l4-Dichloiobenzene 1.11520 1.6748 mg/kg 67 23-92 0-36 02494624-Dinitrotoluene 1.36537 1.6748 mg/kg 82 45-127 19 0-29 Q249462-Chlorophenol 1.20194 1.6748 mg/kg 72 25-94 0-37 Q24946
4-ChIoro-3methylphenoI 1.43402 1.6743 mg/kg 86 31-113 13 0-32 Q249464-Nitrophenol 0.81212 1.6748 mg/kg 48 17-150 17 0-32 Q24946Acenaphthene1.15472 1.6748 mg/kg 69 36-107 ii 0-32 024946N-NitrosodinpropyTamine 1.18687 1.6748 mg/kg 71 22-105 0-37 024946Pentachlorophenol1.84192 1.6743 mg/kg 110 39-137 0-27 024946Phenol1.14902 1.6748 mg/kg 69 23-97 0-42 024946Pyrene1.47957 1.6748 mg/kg 88 45-133 0-27 024946-See Case Narrative
Page of
nPi cJuroDY RECORD
PAGE
Full Service Analytical Environmental Solutions
Project Name449SpringbrookRoad P.O Box 240543 Charlotte rCPhone704/529-6364 Fax-704/5 Short Hold Analysis Łs No liST Project Yes NoClientCompanyName____________________________please ATTACH any reàt specific reporting QC LEVEL 111111 IVReport To/Contact Name __________________________provisions and/or
Invoice ToReportingAddress________________________________________________________Address Ij
Phone _______________Fax Yes No____________
Email Yes No Email Address___________________________________________Purchase Order No./Bfl1rg Reference _4/74Z gZ2 TO BE FILLED IN B\CLIENT/SAMPLING PERSONNELEDOType..._PDF...._eI Flequested Due Date 01 Days 03 Days 04 Days Days Certification NELAC USACE FL _____NCJLIWorkingDaysStandard10daysSiteLocation
Samples received after 154diili be processed next business day SC....._....OTHER ________N/A ________Site Location Physical Address ______________Turnaround time is based Hisiness days excluding weekends and holidays Water Chlorinated YES NO_________________________________________________________SEE REVERSE FOR TERMS CONDITIONS REGARDING SERVICESRENDEREDBYPRISMBORATORIESINCTOCLIENT Sample Iced Upon Collection YES/NO
EQUESTEDCLIENTDATECOLLECTEDSOIL__________________________PRESERVA
TIME MATRIX SAMPLE CONTAINER
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR TYPE TIVESOURSSLUDGESEEBELOWNO
SlZE
NALYSES
REMARKS
PRISM
LAB
__________ID NO
___
___________
_________________________________________________________________________________________________________________________________________________________________________________________________________________________
Lpies
Signature Sampled By Print Name Affiliation
Upon
relinquishing this Custis your authorization for Prism to proceed with 4e haIyses as requested above Any changes must besubmittedinwriting to the Prism Project Manager There will be charges for any changes tr analyses have been initializedRelinquishedBySignatureReceivedBySignature Date Militaty/Hours
iinquished By Signature
Fteceiyd By Signature Date
Relinquished By Signature
of Shipment
Oat
jTi5kj-i157ôERSSHOULDBETAPED SHUT SItORTATION TO THE LABORATORY Log-tn Gro NoSAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABOIA7bRyUFedExUUPstnd-delivered OPrismFieldSeice UOther
_______________________
Additional Comments
NPDES UT GROUNDWATER-DRINKING WATER SOLID WASTE RCRA CERCL.A LANDFILL OTHERUNCUSCJCUSCUNC USC ONC USC UNC USC ONC USC UNC USC ONC USC UNC USC_________________1VPF Amhor fl lr Pltj-Ti Tpflnlinp nn \Itufjla rnnt Anahmie 7ern
SEEREVERSEFORTERMSCONDITIONS
ORIGINAL
CLIENT ESP 4SSoccc5
A1TN Wro1
PRISM COG GROUP
Ploase fill in the Site Location information on the attached VPH and/or EPH Forms
Full Service Analylical nvlrcnrne Solutions
\asO1FoLD\CoMMON\pbRMS\WH EPH Site Location for Cflent.doc
Rec
Aromatic SurroQate Rec
EPH AliphaticsAromatjcs Laboratory Reporting Form
MDL Method Detection Limit RL Reporting Limit
Were aD performance/acceptance standards for required QNQC
procedures achieved
Was blank correction applied as significant modification of the method
Were any significant modifications to the EPH method made
Comments
Client Name
Project Name
Site Location
ESP Associates PA
Morehead Commons No
Laboratory Name
NC Certification Lab
Sample Matrix
Prism Laboratories Inc
EPH Fractionation Surrogates 1-2
SamDle Identification
Date Collected
Sample Information and Analytical Results
Method for Ranges MADEP EPH
EPH Surrogate Standards Aliphatic 1-Chloro-octadecane Aromatic o-Terphenyl
402
Soil
Date Received
Date Extracted
Fluorobiphenyl
Date Analyzed
Dry Solids
7/5/2007
Dilution Factor
07
Hydrocarbon Ranqes in ma/ka
C9-C18 AliDhatics
II
C19-C36 Aliihatjcs
Cli-C22 Aromatics
Blank
Sample Results
C9-C18 Aliphatics
Cl 9-C36 Aliphatics
C11-C22 Aromatics
RL
Sample Results Sample Results
C9-C18 Aliphatics
Sample Results11
11
11
10
10
10
11
ii
11MDL
10
10
10
Cl9-C36 Aliphatics
Cl 1-C2 Aromaticslj
C9-C
10
10
10
10
10
10
10
10
10
ii
93
71
64
Fractionation Surrogate Accep Range Blank 40-140 40-140 40-140 40-140%Frac Surrogate Rec 99 61
Frac Surrogate Rec 100 64
Unadjusted value should exclude the concentration of any surrogates internal standards and/orconcentrationsofotherrangesthatelutewithinthespecifiedrange
Adjusted value
Blank Laboratory Method Blank
YES
No
Details Attached
Yes NO
NO Yes Details Attached
Page of EPH Soil
RECO JUL 2007
Case NarrativePRISM
LAOAtORIE$f NC
06/29/07 Client Project ID Morehead Commons No
ESP Associates PA Prism COC Group No G0607588
Chris Ward Collection Dates 06/20/07Box 7030 Lab Submittal Dates 06/20/07
Charlotte NC 28241
This data package contains the analyilcal results for the project identified above and includes Case Narrative Laboratory Report and QualityControlDatatotalingpageschain-of-custody is also attached for the samples submitted to Prism for this project
Data qualifiers are flagged individually on each sample key reference for the data qualifiers appears at the end of this case narrative Qualitycontrolstatementsand/or sample specific remarks are included in the sample comments section of the laboratory report for each sampleaffected
Semi Volatile Analysis
No Anomalies Reported
Volatile Analysis
No Anomalies Reported
Metals Analysis
N/A
Wet Lab and Micro Analysis
N/A
Please call if you have any questions relating to this analytical report
Date Reviewed by bbi Jones ______________________________
06/29/07 ______________________________
Data Qualifiers Key Reference
Compound also detected in the method blank
Result outside of the QC limits
DO Compound diluted out
Estimated concentrafion calibration range exceeded
The analyte was positively identified but the value is estimated below the reporting limit
I-I Estimated concentraon with high bias
Estimated conceniraion with low bias
maffix effect is present
Notes This report should not be reproduced except in its entirety without the writtten consent of Prism Laboratories Inc The results in this
report relate only to the samples submitted for analysis
449 Spngbrook Road
P.O Box 240543 Charlotte NC 28224-0403
Phone 704/529-6364 Toll Free 800/529-6364 Fax 704/525-0409
Date
Company
Contact
Address
Signature
Review Date
Project Manager
Signature
Approval Date
AngelaDOvercash 1/
06/29/07
ESP Associates PA
Attn Chris Ward
Box 7030
harIotte NC 28241
Laboratory Report
06/29/07
lAi 23
185079
00607588
06/20/07
06/20/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Sample Comments
3RL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanVELACcertificationexceptforthose instances indicated in the case narrative and/or test comments
All results are reported on dry-weight basis
ngeIa Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1000
1635
Phon 7O4/529-664 Toll Free Nijmhcr 1-Rflfl2q-RR4 7n4I5-n4nq Page 2of4
Project ID Morehead Commons No Client Sample ID 1B-234
Prism Sample ID 185080
Sample Matrix Soil COG Group G0607588
Time Collected 06/20/07 1015
Time Submitted 06/20/07 1635
Parameter
Percent Solids Determination
Percent Solids
Method Analysis
Date/Time
Analyst Batch
ID
SM2540 06/27/07 1800 Lthao
Surrogate
Bromofluorobenzene
Dibromofluoromethane
Toluene-d8
Recovery
105
97
96
Control Limits
77-128
67-143
81 128
Diesel Range Organics DROI by GC-FID
iesel Range Organics DRO 76 mg/kg 8.2 1.0 8015B 06/28/07 808 ivoge Q24575
Sample Preparation 25.36 mL 3545 06/25/07 1515 wconder P18738
asoline Range Organics GIRO by GC-FID
Gasoline Range Organics GRID BRL
Surrogate
aaa-TFT
Recovery
83
Control Limits
55-129
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprinybrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page of
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
......ervce AnIyUcaI .nvironmenta .elutlons
ESP Associates PA
Attn Chris Ward
Box 7030
Tharlotte NC 28241
Laboratory Report
06/29/07
Result Units Report MDL Dilution
Limit Factor
85.6
Volatile Organic Compounds by GC/MS
enzene BRL pg/kg 3.6 0.48 826DB 06/27/07 940 erusselt Q24552
cthylbenzene BRL pg/kg 6.0 0.42 826DB 06/27/07 940 erussell Q24552
ip-Xylenes BRL pg/kg 12 0.84 826DB 06/27/07 940 erussell Q24552
-Xylene BRL pg/kg 6.0 0.36 826DB 06/27/07 940 erussell Q24552
Toluene BRL pg/kg 6.0 0.41 826DB 06/27/07 940 erussell Q24552
Surrogate
o-Terphenyl
Recovery Control Limits
99 49-124
mg/kg 1.2 0.074 8015B 06/27/07 615 hwagner Q24580
ESP Associates PA
Attn Chris Ward
Box 7030
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/29107
B-234
185080
G0607588
06/20/07 1015
06/20/07 1635
Parameter Result Units Report
Limit
MDL Dilution Method
Factor
Analysis Analyst Batch
Date/Time ID
Sample Comments
BRL Below Reporting Umit
Estimated value between the Reporting Umit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthoseinstances indicated in the case narrative and/or test comments
All results are reported on dy-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
SeMc AnaIytica Environmental S.....lions
Charlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COc Group
Time Collected
Time Submitted
Phone 7041529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page 4of4
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 7041529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Project ID
Level II QC Report
6/29/07
Morehead Commons No COC Group Number G0607588
Date/Time Submitted 6/20/07 1635
VoIatil Ornink nmnnunrI -I R2ROR
Method Blank
QC BatchResultRLControl Limit Units II
Benzene ND 0.003 0.0015 mg/kg 024552
Ethylbenzene ND 0.005 0.0025 mg/kg Q24552
rnp-Xylenes ND 0.01 0.005 mg/kg 024552
o-Xylene ND 0.005 0.0025 mg/kg Q24552
Toluene ND 0.005 0.0025 mg/kg 024552
Laboratory Control Sample Recovery Recovery
Result Spike Amount Units Ranges QC Batch
ID
Benzene 0.04358 0.05 mg/kg 87 62-119 024552
Ethylbenzene 0.04417 0.05 mg/kg 88 57-1 28 024552
mp-Xylenes 0.09048 0.1 mg/kg 90 54-132 024552
o-Xylene 0.04725 0.05 mg/kg 95 57-131 024552
Toluene 0.04544 0.05 mg/kg 91 57-122 Q24552
Matrix Spike Recovery Recovery
Sample ID Result Spike Amount Units
Ranges OC Batch
ID
185081 Benzene 0.03306 0.05 mg/kg 66 46-136 024552
Ethylbenzene 0.02888 0.05 mg/kg 58 51-135 024552
mp-Xylenes 0.05588 0.1 mg/kg 56 51-1 36 024552
o-Xylene 0.02855 0.05 mg/kg 57 49-1 37 024552
Toluene 0.0296 0.05 mg/kg 59 47-1 36 024552
Matrix Spike Duplicate Recovery RPD
Sample ID
Result Spike Amount Units Recvery Ranges RPD Range QC Batch
ID
185081 Benzene 0.03495 0.05 mg/kg 70 46-1 36 0-22 Q24552
Ethylbenzene 0.03244 0.05 mg/kg 65 51-1 35 12 0-23 024552
mp-Xylenes 0.06374 0.1 mg/kg 64 51-136 13 -20 Q24552
o-Xylene 0.03337 0.05 mg/kg 67 49-137 16 -22 024552
Toluene 0.03187 0.05 mg/kg 64 47-1 36 0-22 024552
Page of
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No
Level II QC Report
6/29/07
COC Group Number G0607588
Date/Time Submitted 6/20/07 1635
185077 Gasoline Range Organics GRO 2.016
Matrix Spike Duplicate
Sample ID
185077 Gasoline Range Organics GRO 1.968
-See Case Narrative
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone 704/529.6364 Toll Free Number 1-8001529-6364 Fax 7041525-0409
Diesel Penn flrnn IflDt Fm OnIrD
Method Blank QC Batch
Result RL Control Limit Units ID
Diesel Range Crganics DRO ND 3.5 mg/kg Q24575
Laboratory Control Sample Recovery Recovery
Ranges 00 Batch
Result Spike Amount Units ID
Diesel Range Organics DRO 49.0 80 mg/kg 61 55-109 Q24575
Matrix Spike Recovery Recovery
Ranges OC Batch
Sample ID Result Spike Amount Units ID
184791 Diesel Range Organics DRO 45.8 80 mg/kg 57 50-117 024575
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range OC Batch
Sample ID Result Spike Amount Units ID
184791 Diesel Range Organics DRO 51.9 80 mg/kg 65 50-117 12 0-24 Q24575
Gasoline Range Organics GRO by GC-FID method 8015B
Method Blank 00 Batch
Result RI Control Limit Units ID
Gasoline Range Organics GRO ND 0.5 mg/kg 024580
Laboratory Control Sample Recovery Recovery
Ranges QC Batch
IDResultSpikeAmountUnits
Gasoline Range Organics GRO 1.966 mg/kg 98 64-124 024580
Matrix Spike Recovery Recovery QC BatchRangesIDSampleIDResultSpikeAmountUnits
mg/kg 101 37-1 26 024580
Recovery Recovery RPD
Ranges RPD Range 00 Batch
Result Spike Amount Units ID
mg/kg 98 37-126 0-34 024580
Page of
CHAIN OF CUSTODY RECORD
PAGE _..L OF ...L QUOT TO SURE ILLING _______________
Project Name 41
Short Hold Analysis Yes No UST Project Yes No
please ATTACH any project specific reporting QC LEVEL 111111 IV
provisions and/or QC Requir ts
Invoice To 1.1l
Address
Purchase Order NoJBilIing Reference JI 12 I2
Requested Due Date CI Day Days 03 Days 04 Days EDays
Working Days 6-9 Days LI Standard 10 days ci us Work ust Be
Samples received after 1500 will be processed next business day
Turnaround time is based on business days excluding weekends and holidaysSEEREVERSE FOR TERMS CONDITIONS REGARDING SERVICESRENDERED BY PRISM LABORATORIES INC TO CLIENT
Samplers Signature 4jP AIY_S Sampled By Print Name Affiliation
Upon relinquishing thisCiiæof Custody is your authorization for Prism to proceed with the analyses as requested above Any changes
must besubmittedinwriting to
the Prism Project Manager There will be charges for any changes after analyses have been InitializedPS
Relinquished By Signature Received By Signature Date
Relinquished By Slgn-Receved
Method of Shipment NOgASAMPLE ERS SHOULD BE TAPED SHU WITH USTODY SEALS FOR TRANSPORTATION TO THE LABORATORYSMESARE NOT ACCEPTED AND VERIFIED AGAINST 5tiNTIL RECEIVED AT THE LABORATORY
Fed Ex
CI UPS 4arid-delivered Prism Field Service CI Other
COC Group NO
ci$g
NPDES US GROUNDWATER DRINKING WATER SOLID WASTE RCRA CERCLA LANDFILL OTHERONC USC 6C USC IJNC USC UNC USC IJNC USC ONC USC ONC USC UNC USC UNC USC________________lJ ____________________lj _____ ____
____nn.rra.cfl flJflt flflflO ._..t.....CS CSI_..CS tSL.._fl flI__S_.I r..XI__L.....J CS...CSA L.j...aI.fl.....-.t.-.-__V_lW_I_V
Site Departure Time
Field e6h FeeV
Mileqge
Pull Service Malytical EnvinmentaI Solutions
449 Springbroók Road P.O Box 240543 Charlotte NC 28224-0543Phone704/529-6364 Fax 704/525.-04Q9
Client Company Name _______________________
Report To/Contact Name
Reporting Address ______________________________iZi 41r
Phone ________________Fax Yes No
Email Yes No Email Address_____________________
EDD Type PDF......_Excel 9ther
Site Location Name __________
Site Location Physical Address
.1
Samples INTACTupon arrivel7
N/A
ReceivedON
PRQPE1 PRESERVATIVES indicted
Received WITHIN HOLDING TIMES
CUSTODY SEALS INTACT
VOLATILES rec W/OUT HEADSPAE
PROPER CONTAINERS used
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC_USACE__FL____NC 4/
SC_OTHER ______N/A ______
Water Chlorinated YES_NO_
Sample Iced Upon Collection YES NO
CLIENT
SAMPLE DESCRIPTION
/_2/-/42
41
DATE
COLLECTED
TIME
COLLECTED
MILITARY
HOURS
ivi
iic
/2Zio
MATRIX
SOIL
WATER OR
SLUDGE
j-1
SAMPLE CONTAINER
PRESERVA-
TIVES
ANALYSES REQUESTED
A/REMARKS
l/
--
PRISM
LAB
ID NO
Ist5o
TYPE
SEE BELOW
izJ
NO SIZE
.....lgnature Received By Signature Date miiiarynuurs Additional Comments
SEE REVERSE FORTERMSCONDITIONS
I..I Al
APPENDIX
NON-HAZARDOUS WASTE MANIFESTS
yr ALL WASTINDUSTRiESNc
Transporter Company Name US EPA ID Number
Transporter Company Name US EPA ID Number
Designated Facility Name and Site Address
CMS Landfill
5105 Morehead
Rd
Concord NC 28027
10 US EPA ID Number
Transporters Phone
Facilitys Phone
15 Special Handling Instructions and Additional Information
Printed Typed Name
20 FacilityOwner or Operator Cerification of receipt of waste materlalscovered by this manifest except as noted in item 19
CMS Landfill
Please print or type
Form designed for use on elite .12 pitch typewriter
Transport 7O
NON-HAZARDOUS Generators US EPA ID No Manifet Page
WASTE MANIFEST Document No of
Generators Name and Mailing Address Truck No
Generators Phone
704 782-2004
11 Waste Shipping Name and Description 12 Containers 13 14
Total Unit
No Type Quantity WtNol
Additional Descriptions for Materials Listed Above Handling Codes for Wstes.Listed Above
17 Transporter AcknowledgØmentof Receipt of Materials
16 GENERATORS CERTIFICATION certify the materials despribed above on this manifest are not sublect to federal regulations for reporting proper disposal of Hazardous Waste
Printed Typed Name
Printed Typed Name Fm
18 Transpolter Acknowledgement of Receipt of Materials
19 Discrepancy Indication Space
Printed /Type Name Signature
TISJD/FI COPY .t
ALL WASTtyp
on elite 12 pitch typewriter
Generators Name and Mailing Address Truck No
Generators Phone
Transporters Ihone
ansporter2CompanyName8
Designated FacilityName and Site Address 10 US EPA ID Number Facilitys PhoneCMSLandfill704782-20045105MoreheadRd
12 Containers 13 14TotalUnit________________No Type Quantity WtNol
__________________________________________________________
_______________
Additional Descriptions for Materials Listed Above
Handling Codes for Wastes Listed Above
eciaI Handling Instructions and Add itional Information
16 GENERATORS CERTIFICATION certify the materials described above on this manifest are not subiect to federal regulations for reporting proper disposal of Hazardous Waste
17 Transporter Acknowledgement of Receipt of Materials
Printed/Typed Name
Signature .-.--Monh DY Veer
18 Transporter Acknowledgement of Receipt of Materials
T/S/D/F/Copy orm
VALUD whSr..INOUSTRIES INC
NON-HAZARDOUS Generators US EPA ID No ManifestWASTEMANIFESTDocument No
-Yyi4 aJ
-4 Snature
Please print or type
Form designed for use on elite 12 pitch typewriter
Generators Name and Mailing Address
Generators Phone
/7
11
Transporter Company Name US EPA ID Number
Transporter Company Name US EPA ID Number Transporters Phone
Designated Facility Name and Site Address io US EPA ID Number Facilitys Phone
ClefS Landfill 704 782-20045105 Morehead Rd
Concord NC 28027
l1.Waste Shipping Name and Description 12 Containers
No Type Quantity WtNol
pc Ti
Additional Descriptions for Materials Listed Above Handling Codes for Wastes Listed Above
15 Special Handling Instructions and Additional Information
16.GENERATORS CERTIFICATION certify the materials described above on this manifest arenot.subiect to federal regulations for reporting proper disposal of HazardoUs Waste
Printed/Typed Name signatu 73 4/De.v Ye4-11717TransporterAcknowledgementofReceiptof Materials
PrInted Typed Name
gnaure t5th 1Z2 k518TransporterAcknowledgementofReceiptofMaterials
Printed/Typed Name Signature Month bay Year
19 Discrepancy lndication.Space
CMS Landfill
...
Printed lType Name Month Veery2
TISIDIFI
AWJ Iorn1 121
Please print or type
Form designed for use on elite 12 pitch typewriter
1.eratorslJS EPA ID tlo Manitea
Document
ALLWA$T.INDUSTRIES IN
NON-HAZARDOUS
WASTE MANIFEST
Generators Name and Mailing Address
Generators Phone
Transporter Company Name US EPA ID Number
Transporter Company Name US EPA ID Number Transporters Phone
Designated Facility Name and Site Address 10 US EPA ID Number Facilitys Phone
CMS Landfill 704 782-2004
5105 Morehead Rd
Concord NC 28027
11 Waste Shipping Name and Description
Additional Descriptions for Materials Listed Above
15 Special Handling Instructions and Additional Information
16 GENERATORS CERTIFICATION certify the materials desôribed above on this manifest are not subject to federal regulations for repdrtiilg proper disposal of Hazardous Waste
Printed /Typed Name ./Month Dj YeariL
17 Transporter Acknowledgement of Receipt of Materials
./
Printed /Tped Name Month Day Year
Itc
18 Transporter Acknowledgement of Receipt of Materials
Printed Typed Name Signature Month Day Year
19 DIscrepancy Indication Space
..
20 Facility Owner or Operator Cerification of receipt of waste materials covered by this manifest except as noted in item 19
CMS Landfill
Printed hype Name Signature
Morih
Day ar
\/l --AIFflr12Y
T/SIDIF/COPY
Please print or type
Form designed for use on erite 12 pitch typewriter
ALLD WST
Transporter Company Name US EPA ID Number
Transporter Company Name US EPA ID Number
NON-HAZARDOUS Generators US EPA IDNo Manifest PageWASTEMANIFESTDocumentNoof 127873
Generators Name and Mailing Address Truck No
o.-h
Generators Phone
Transporteqrit
Transporters Phone
Facilitys Phohe
704 782-2004
Designated Facility Name and Site Address 10 US EPA ID Number
CMS Landfill
5105Morehead Rd
CohcordIC 28027
11.WastehippiægName and Description 12 Containers 13 14
Total Unit
..___________________________________________________________________________________________No Type Quantify WW0I
Additional DescriPtkr Material tisted Abov Handling Codes fo Wastes Listed Above
15 Special Handling Instructions and Additional Information
16 GENERATORS CERTIFICATION certify the materials described above on thismanifest arenot sublect to federal regulations for reporting prope disposal of HaardoUs Waste
Prited /Typed Name patut7 .4 //Month Day Year
.../.2
17 Transporter Acknowledgement of Receipt of Materials
..
PrInted/Typed Name Signature Month Day Yearih
18 Transporter Acknowledgement of Recetpt of Materials
Printed Typed Name Signature Month Day Year
19 Discrepancy lndicafi6n Space
........
20.Facility Owner or Operator Cerification of receipt of waste materials covered by this manifest except as hoted in itemCMLandfill
Printed/Type Name
1\
Signatue 1h 1Y
Si TISIfl/F/NWV
r./AWl Form 121-
._Transporter Company Name US EPA ID Number Transporters Phone
DesignatedFacllity Name and Site Address 10 US EPA ID Number Facilitys Phone
CMS Landfill 704 782-20045105MoreheadRd
Concord NC 28027
11 Waste Shipping Name and Description 12 Containers 13 14
Total UnitNoTypeQuantityWt/Vol
J/L.\_----
iation.nT5
ist
Abo
Printed /Typed Name ture ii Month Da Year---/17 Transporter Acknowledgement of Receipt of Materials ..1
Printed/TypedName Signature -Mànth Day Yearfl4
Year
20 Facility Owner or Operator Cerification of receipt of waste materials àovered bythis manifest except as noted iri iteth 19CMSLandfill
Signatue
--.1
Please print or type
Form designed for use on dllte 12 pItch typewriter
NON-HAZARDOUS Gen rators US EPAID No
WASTE MANIFFST --
Generators Name and Mailing Address
Generators Phone
Transporter Company Name 6.-US EPA ID NijmbØr Transportehoiq .-Ytii
Printed/Type Name
AVIFrnh2
TISID1F/COPY
Printed Typed Name kk
16 Transporter Acknowledgefflerit of Receipt of Materials
Printed Typed Name
19 Discrepancy Indication Space
Please print or type
Form designed for use on elite 12 pitch typewriter
ir Aw wAsy L71
NON-HAZARDOUS Generators US EPA ID No Manifest Page
.L WASTE MANIFEST DocumentNo --127874GeneratorsNameandMailingAddress1LhTruckNo
dr
.iI
Generators Phone
---.-.-.----.--.- ---.--.--Transporter Company Name US EPA ID Number TransporterpIhorae
.-------..----..-.---Transporter Company Name US EPA-ID Number Transporters Phone
Designated Facility Name and Site Address 10 US EPA ID Number Facilitys PhoneCMSLandfill704782-20045105MoreheadRd
Concord NC 28027
Waste Shipping Name and Description 12 Containers 13 14
--Tdtal UnitNoTveQuantityWtNol
--
1-
Additional Descriptions for Materials Listed Above
--7
1-
Special Handling Instructions and Additional Information15
Handllng Codes for Wastes Ld Above
GENERATORS CERTIFICATION certify the materials described above on this manifest are not subject to federal regulations forrepdtWi proper disposai of Hazadous WastePrinted/Typed Name Signature-7 Month bay Year
17 Transporter Acknowledgement of-Receipt of Materials --
--
SnatureYoar__________________________________________________________________________________
__________________________________________________
jMmthfrYJv
T/S/D1F/copy
.0
Ii
Pitase print or type
Form designed for use on elite 12 pitch typewriter
IALuib WASTE
_________INDUS1RIS INt
Transporter Company Name US EPA ID Number
Transporter Company Name US EPA ID Number
Designated Facility Name and Site Address
CMS Landfill
5105 Morehead Rd
Concord NC 28027
NONHAZARDOUS Generators USEPA Manifest PageWASTEMANIFESTDocumentNoof 27 875
Generators Name and Mailing Address MV Truck No
yt
Generators Phone t.37
Transporte.hy
11 Waste Shipping Name and Description
US EPA ID Number
Transporters Phone
Facilitys Phone
704 782-2004
tàiE
Additional Descriptions for Materials Listed Above
15 pecial Handling Instructions and Additional Information
16 GENERATORS CERTIFIcATION certify the materials described above on this manifedt are not subject to federal regulations for reponingproper disposal of Hazardous Waste
Printed/Typed Name
jpture Mdnth
17 Transpàrter.I Acknowledgement of Receipt of Materials .....
Printed/Typed Name
th ba Ve
18 Transpofler Acknowledgemert bt Receipt of Materials
Printed /Typed Name Signature Month bay Year
19 Discrepancy Indication SpØbe
20 Faciltty Owner or Operator Certfication of receipt of waste materials covered by thts manifest except as noted in item 19CMSLandfill
Printed Type Name 1\\IiiT
TISID/FI COPY
AWED WASTE
A..lNOUs1pIEsNc
çjh
-r-v
Signature
Please print or type
Farm designed for use on elite 12 pitch typewriterNON-HAZARDOLJS
WASTE MANIFEST
Generators Name and Mailing Address
Generators Phone
Generators US ElAi1J
Transporter Company Name US EPA ID Number Transportdbdn
Transporter Company Name USEPA ID Number Transporters Phone
Designated Facility Name and Site Address 10 US EPA ID Number Facilitys PhoneCMSLandfill704782-20045105MoreheadRd
Concord NC 28027
11 Waste Shipping Name and Description 12 Containers 13 14
Total UnitNoTypeQuantityWtNolPt.._..c./-c
Additional Descriptions for Materials Listed Above Handling Codes for Wastes Listed Above
15 Special Handling Instructions and Additional Information
Printed/TypedName
Signatur9 Month Daj Year
18 Transporter Acknowledgement of Receipt of Materials
Printed Typed Name .-
19 Discrepancy Indication Space
Printed Type Name
CMS Landfill
.-
-A
TISID/F/COPy
Designated Facility Name and Site Address io
CMS Landfill
5105 Morehead Rd
Concord NC 28027
Printed /Typed Name
Please print or type
Form designed for use on elite 12 pItch typewriter
ALL1E WASTEDIJS1PIES.INC /t/i/
NON-HAZARDOUS Generators US EPA ID No Manifest PageWASTEMANIFESTDocumentNoof
Generators Name and Mailing Address Truck No
UD nc4
fr
Generators Phone
Transporter Company Name US EPA fD Number Transport
Transporter Company Name US EPA ID Number Transporters Phone
US EPA ID Number Facilitys Phone
704 782-2004
11 Waste Shipping Name and Description
Additional Descriptions for Materials Listed Above
15 Special Handling Instructions and Additional Information
Ft
Ft
ignaturj/7/
19 Discrepancy Indication Space
nspdrter1Acknow
Printed/Typed Name
atuu1
Receipt at MeriIs
Signature nth bay Year
Month Day Year12IJ5
20 Facility Owner or Operator Cerificatiort of receipt ofOMSLandfill
Printed /Type Name
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Form designed for use on elite 12 pitch typewriter
Month Day Year
AWl Form 121
LL WASTENOSIRlEINC
j/f7/NONHAZARDOUS Generators US EPA ID No Manifest PageWASTEMANIFEST..Document No of
Generators Name and Mailing Address Truck No
.c
farr yk.if1.r
Generators Phone
..-.-..Transporter Company Name US EPA ID Number
Transporter Company Name US EPA ID Number Transporters Phone
Designated Facility Name and Site Address io US EPA ID Number Facilitys Phone
CMS Landfill 704 782-20045105 MorehØad Rd
Concord NC 28027
11.Waste Shipping Name and Description 12 Containers 13
No Type Quantity WtNol
t.ra ff
Additional Descriptions for Materials Listed Above Handling Codes for Wastes Listed Above
____________.___.__.._____15 Special Handling Instructions and Additional InformatIon
16 GENERATOR CERTIFICATION certify the materials described above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste
Printed Typed Name ItUreçJ-n-Month Da Year
-l ..--.r/--/417TransporterAcknowledgementofReceipt-of Materials
Printed Typed Name Signature Month Day Year
Ii
19 Discrepancy Indication Space
CMS Landfill
Printed Type Name ZçJJ Signature ///
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pr AjjWASTEINDUSTRIESINCNONHRDOUSGeneratorsus
Generators Name and Mailing Address
Truck No
c11GeneratorsPhonesporterlcompanyName
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Form designed for use on elite 12 pItch typewriter
TransportetiiJonsporter2CompanyNam
Facilitys PhoneCMSLandfill
704 782-20045105MoreheadRd
12 Containers 13 14
Total UnitNo1\jpe Quantity WtNol
___iI
Additional Descriptions for Materials Listed Above
15 Special Handling Instructions and Additional Information
Printed Typed Name
iathrey2 Month Da Year
17 Transporter Acknowledgement of Receipt of Materials
Printed Typed Name
Signature
Month Day Year19DiscrepancyIndicationSpace
20 Facility Owner or Operator Cerlfication of receipt of waste materials covered by this manifest except as noted in1itm 19CMSLandfill
Printed /Type Name .._Signature ....MsnLfr..Day Yaar
AWl Form 121T/S/D/p/COPY
NON-HAZARDOUSWASTEMANIFEST
GeneratOrs Name and Mailing Address
Generators Phone
Transporter 2.Company Name
Designated Facility Name and Site Address
CMS Landfill
5105 MorØhead Rd
Concord NC 28027
____
16 GENERATORS CERTIFICATION certify the materials described above on this manifest are riot subject to federal regulations for repoi-ting proper disposal of Hazardous WastePrintedTypedName
PaturC2 My Year
17 Transporter Acknowledgement of Receipt of Materials
Printed Typed Name jn
Month De.v Year
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Form designed for use on elite 12 pitch typewriter
AJJ WAS
.....USTRIES.IN.
Generators US EPA ID No TTMaifst iaa
.1
DocumnNo of
N7
Tiubk Na
127871
US EPA ID Nu
US EPA ID NUmber
TransportŒhy
Transporters Phone
10 US EPA ID Number Facilitys Phone
11 Waste Shipping Name and Description
704 782-2004
Containers 13
TotalNoTvgeQuantity
14
Unit
WtNol
bAdditional Descriptions for Materials Listed AbOve
15 Special Handling Instructions and Additional Information
cm
p..
Ft
Handling Codes for Wastes Listed Above
Signaturhóv
f1h
18 Transporter Acknowledgemert of Receipt of MÆteriäls
Printed Typed Name
19 Discrepancy Indication Space
20 Facility Owner or Operator Cerification of receipt of waste materials coyCMSLandfill
Printed Type Name
Please print or type
Form designed for use on elite 12 pitch typewriter
ALLIED WsyV.INDUSTPIES INC
/11/1-7ii9I
NON-HAZARDOUS Generators US EPAID No Manifest PageWASTEMANIFESTjocumentNoof 127880GeteratorsNameandMailingAddressifTruckNo
--b \vGeneratorsPhone
Transporter Company Name US EPA ID Number Transporterahone
..Transporter Company Name US EPA ID Number Transporters Phone...Designated Facility Name and Site Address 10 US EPA ID Number Facilttys PhoneCMSLandfill704782-20045105MoreheadRd
Concord NC 28027
11 Waste Shipping Name and Description 12 Containers 13 14
Total UnitNoTypeQuantityWtNol
Additional Descriptions for Materials Listed Above
/2.
15 Special Handling Instructions and Additional Information
Jandling
Codes for Wastes
Lte
Above
16 GENERATORS CERTIFICATION certify the materials described above on this manife
Printed /Typed Name
Printed Typed Name
17 Transporter Acknowledgement of Receipt of Materials
ikf
Signature
11AALU WAS1W
--18 ES
Transporter Company Name US EPA ID Number
Transporter Company Name
US EPA ID Number
ii Waste Shipping Name and Description
US EPA ID Number
17 Transporter Acknowledgement of Receipt of Materials
ior type
for use on elite 12 pItch typewriter
I/Z
ON-HAZARDOUS GØnØrators US EPA ID No Manifest Rage
NASTE MANIFEST
Document No of
Generators Name and Mailing Address Truck No
--
i3L
.4 Generators Phone
Dsignated Facility Name and Site Address 10
CMS Landfill
5105 Morehead
Rd
Concord NC 28027
Transporters Phone ________________________
Facilitys Phone _______________________
704 782-2004
12 Containers
No Type
13
Total
Quantity
14
Unit
WtNol
5c
Additional Descriptions for Materials Listed Above Handling Codes for Wastes Listed Above
7-I-2
15 Special Handling Instructions and Additional Information
Printed Typed Name
.16 GENERATORS CERTIFICATION certify the materials described above on
thisrhanifest are not subjec
9ignature7/-
Printed /Typed Name
18 Transporter AcknowlºdgernŁnt of Rebeipt of Materials
Printed Typed Name
Sgnature
Signature
19 Discrepancy Indiàation Space
20 Facility Owner or Operator Cenfication of receipt of waste materials cc
CMS Landfill
Printed Type Name %.j /c
Corporate Office
MailingP0Box 7030
Charlotte North Carolina 28241
Physical
3475 Lakemont Boulevard
Fort Mill SC 29708
803.8022440
Raleigh
14001 Weston Parkway
Suite 100
Caiy North Carolina 27513
919.678 1070
Wilmington
2120-B Capital Drive
Wilmington North Carolina 28405
910.313.6648
Concord
4601 Corporate Drive NW
Suite 165
Concord North Carolina 28027
704793.9855
800.960.7317
www.espassociates corn
ESP Associates P.A