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Home My WebLink AboutItem No 23 - 20Day Report - Morehead Common Site Area No 5-OCRNCDENR UST Section Mooresville Regional Office 919 North Main Street Mooresville North Carolina 28115 Attention Mr Allen Schiff Dear Mr Schiff 20-DAY REPORT Morehead Common Site Area No 919 West Morehead Street Charlotte North Carolina Incident No Not Yet Assigned ESP Project No E6-UD42.601 On behalf of the property owner and our client Beazer Homes ESP Associates P.A is pleased to provide the attached 20-Day Report for release of petroleum product at the subject site as discovered during mass grading operations of this area Thank you for your attention in this matter If you should have any questions please do not hesitate to contact me at 803 835-0915 Sincerely isifir-Ward PG Environmental Services NC License No 1600 P.O Box 7030 Charlotte NC 28241 1.800.960.7317 NC 704.583.4949 fax 704.5834950 SC 803.802.2440 fax 803.802.2515 www.espassociates.com 4ESP ESP Associates PA July 18 2007 Reference ESP As cc Mr Jade Eastridge 20-Day Report SITE INFORMATION Site Identification Date of Report July 18 2007 Facility ID N/A El UST Incident Number Not Yet Assigned Site Name Morehead Common Site Area No Site Street Address 919 West Morehead Street City/County/Zip Code Charlotte Mecklenburg County 28278 Description of Geographical Data Point Approximate center of UST Location Method Mecklenburg County Polaris GIS Map Latitude 5.2276 Longitude -80.8582 Information about Contacts Associated with the Leaking UST System UST Owner Beazer Homes 1300 Blvd Suite Charlotte NC 28203-4265 704.370.7200 UST Operator N/A Property Owner Same as above Property Occupant Same as above Consultant/Contractor ESP Associates PA Chris Ward PG P0 Box 7030 Charlotte NC 28241 803.835.0915 Analytical Laboratory Prism Laboratories Inc P0 Box 240543 Charlotte NC 28224-0403 704.529.6364 NC Certification No 402 Information about Release Date Discovered June 19 2007 Estimated Quantity of Release Unknown Cause of release Unknown Source of Release UST Size and contents of UST system from which release occurred 550-gallon steel diesel and 750-gallon gasoline USTs Certification Chris Ward Professional Geologist for ESP Associates P.A do certify that the information contained in this report is correct and accurate to the best of my knowledge ESP Associates P.A is licensed to practice both geology and engineering in North Carolina ESP Associates certification numbers are Geology C-347 Engineering C-OS 87 2O4Jay Report ESP Project E6-UD42 601 Morehead Common Site Area No July 18 2007 INTRODUCTION On June 19 2007 ESP responded on behalf of Beazer Homes to an encounter with an underground storage tank UST and impacted soil during mass grading operations at the subject site Upon arriving at the site ESP observed 550-gallon steel apparent diesel UST and 750- gallon steel apparent gasoline UST along with petroleum odor located on the south side of West Morehead Street approximately 150 feet west of its intersection with South Clarkson Street on Tax Parcel No 07325210 see Figures and The incident area has been designated as Area No As required following receipt of laboratory results confirming release had occurred ESP emailed notification of the release discovery along with Release and UST Leak Reporting Form tO Mr Steve Bograd of the Mooresville Regional Office of NCDENR on June 19 2007 The subject site is located within an urban area of Charlotte which historically included warehouse and retail structures The site is currently mass graded and being developed as mixed-use development see Figures and Based on our review of the Geologic Map of North Carolinal985 the subject site is located within the Charlotte Belt locally comprised of intrusive metamorphosed granitic rocks locally pinkish gray massive to weakly foliated and containing hornblende Soils encountered in this area are the residual product of chemical weathering of rock presently underlying the site Soil weathering is more advanced near the surface grading with depth to less weathered rock and finally bedrock INITIAL ABATEMENT ACTIVITIES On June 19 and 20 2007 ESP documented the excavation of approximately 100 cubic yards of impacted soils from Area No by the sites grading contractor Gelder Thompson of Midland North Carolina The excavation was advanced based on OVA readings and evidence of visible staining The resulting excavation measured approximately 23 ft 24 ft 10 ft deep Neither groundwater bedrock nor free product were encountered within the tank pit 20-Day Report ESP Project E6-UD42 601 Morehead Common Site Area No July 18 2007 The excavated soil was placed on and covered with plastic awaiting subsequent off-site permitted disposal On June 20 2007 ESP collected two composite soil samples for laboratory analysis The soil samples designated 1A and lB were placed in laboratory provided containers labeled and hand delivered on ice to Prism Laboratories for compositing and subsequent analysis The samples were analyzed for TPH-GRO/DRO and BTEX On June 20 2007 confirmatory soil samples were collected at depth of feet BLS from each of the excavations four sides WS-i through WS-4 while one sample was collected at depths of 10 feet BLS from the base of the excavation B-i The five soil samples were hand delivered on ice to Prism Laboratories to be analyzed for NCDENR risk-based parameters which include VOCs by EPA Method 8260B SVOCs by EPA Method 8270C VPH/EPH by the Massachusetts Department of Environmental Protection MADEP method and for total lead and chromium by EPA Method 60 lOB Sample locations and excavation dimensions are depicted on Figure Soil Sample Location Map Sampling was performed in general accordance with ESPs SOP see Appendix FUTURE REPORTING An Initial Abatement Action Report is currently being prepared for this release ATTACHMENTS FIGURES WESTMOREHEAD STREET WS-4 WS-4 ws-i WS-3 ws-1 WS-3 ///7 AREA WS-2 LEGEND CONF1RMA TORY SOIL SAMPLE LOCA liON AREA EXCA VA liON DEPThI OF FEET AREA EXCAVATiON DEPTH OF FEET FiGURE SOIL SAMPLE LOCA 710N MAP AREAS AND MOREHEAD COMMON SITE CHARLOTTE NORTH CAROUNA 20 APPROX/MA 1E SCALE IN FEET ESP A5s00i9689 PA P0 Box 7030 ChorloSo NC 3024 3475 Loknon 954 For MI SC 29706 704-563-4949 NC 603-602-2440 SC woxv.espassocIaes corn WS-2 AREA SITE PHOTOGRAPIIS MOREHEAD COMMON SITE AREA NO VJEWOFTJSTSFROMAREANO VIEW OF USTS FROM AREA 5-LOOKThG EAST VIEW OF AREA TANKS BEING PUMPED OF LIQUIDVIEWOFEXCAVTIONAROUMTANKSFROMAREA VIEW OF LEAKING UST AREA NO MOREHEAD COMMON SITE AREA NO VIEW OF LEAKING UST FROM AREA NO -s VIEW OF VISIBLY IMPACTED SOIL FROM EXCAVATION IN AREANOVIEW OF TWO USTS FROM AREA 5-LOOKING NORTHWEST 24-HOUR RELEASE AND UST REPORTING FORM Steve On behalf of eazer Homes am herein providing 24-Hour Notification of the discovery of three orphan USTs on Beuzer Homes Morehead Common residential/commercial development currently being graded The Moreheod Commons property is located on the south side of West Morehead Street at its intersection with South Clarkson Street in Charlotte North Carolina On June 18 2007 during grading operations an approximate 550- gallon steel UST was uncovered on Parcel No 07325210 The UST was uncovered and determined to be partially filled with sludge and some fluid with diesel odor this UST is being referred to as AREA An additional approximate 550-gallon likely diesel and an approximate 750-gallon likely gasoline were subsequently encountered side by side approximately 25 feet from The first 550-gallon UST encountered on Parcel No 07325210 these USTs are being referred to as AREA On June 19 2007 Ab Environmental and Industrial Services pumped remaining fluid and sludge from the USTs and transported the USTs off-site for permitted disposal The tops of the USTs were buried to depth of approximately feet below original grade and were severely rusted with numerous holes Soils adjacent to and beneath all three USTs exhibited strong petroleum odor and were visibly stained Excavation of soils adjacent to and beneath the three USTs was initiated on June 19 with soils being stockpiled on site on plastic or subsequent off-site disposal Preliminary investigation reveals that Parcel No 07325210 was once occupied by Tonys Auto Body Shop and Shorts Imports The releases are identified on the attached PbF map The Responsible Party for the properly is Beazer Homes 1300 South Boulevard Suite Charlotte North Carolina 28203-4265 Mr Jade Eastridge 704.370.7200 Reàie aud UST Lak Reporthi Form For Releases This form should be completed arid submitted to the UST Sections regional office following known or suspected release from an underground storage tank UST system This form is required to be submitted within 24 hours of discovery of known or hi NC suspected release DWM USE ONLY Suspected Contamination YIN Facility ID Number N/A Incident Risk U_______Confirmed GW Contamination Y/N Date Leak Discovered Jgi tYT Received On Received By Confirmed Soil Contamiration YIN CommNon Commercial 1-tP4tM Reported by circle one Phone Fax or Report Free Product YIN If Yes State Greatest ReglNon regulated Region Thickness INCIDENT DESCRIPTION Incident Name 4ee4 ress JrtJ 6k County Regional Office circle one Ashevill esville ayetteville CitylTown Zip Code Z49Z7 Raleigh Washington Wilmington Winsto Latitude decai degrees Longitude deimaI degrs5s 53 Obtained by Briefly describe suspected or confirmed release including but not limited to nature of release date of release amount Li GPS of release amount of free product present and recovery efforts initial responses conducted impacts to receptors/r i/YL 13 Topographic map ctto 2a-q2 GIS Address matching Otherg14fl4r-v-c//--rr Duinknown444 Describe location U2f-J p-f-ZLe----HOW RELEASE WAS DISCOVERED Check one 13 Release Detection Equipment or Methods Li Visual/Odor Groundwater Contamination Li During UST Closure/Removal Li Water in Tank Surface Water Contamination Li Property Transfer Li Water Supply Well Contamination 9ther specify i-JJLtj --SOURCE OF CONTAMINATION Primary Source of Contamination Primary Contaminant Type Location Settig Checkone Checkone Check one GasolinelDiesel/Kerosene Li Facility Li Residential Li Confirmed UST Release Check one below Heating Oil Li Residence 13 Industrial Li Dispenser Other Petroleum Products Other ikhan Line Release Metals Rural -.-C Tank Release Other Inorganics Spill/Overfill Other Organics 13 Exact Failure Location Unknown or Multiple Failures Owhip Municipal Military Unknown rivate Federal County State Oneration Tvne Public Service Agricultural denti Education/Relig Industrial ercial Mining UST Form 61 11/D5 Page of IMPACT ON DRINKING WATER SUPPUES Water Supply Wells Affected Yes No Number of Water Supply Wells Affected Water Supply Wells Contaminated Include Users Names Addresses arid Phone Numbers Attach additional sheet ifnecessai LiST SYSTEM OWNER UST Owner/Company14//1/IAkY Point of Contact1 City StateNc Address /C20 i% Zip Code Telephone Number/zS 1-oc 772c USTSYSTEM OPERATOR UST Operator/Company Address City State zp Uode Telephone Number LANDOWNER AT LOCATION OF UST INCIDENT Landowner q-iic-4-4-4cfr Address City State Zip Code Teleptlone Numter Draw Sketch of Area showing two major road intersections or Attach Map ri-4c I-e JTephoneNumbe552/LL7 USTFormGl 11/05 Page2of2 PRISM LABORATORY DATA REPORT 1ECU JUL Case Narrative PRISM LAB ORATORIES INC Date 06/29/07 Client Project ID Morehead Commons No Company ESP Associates PA Prism COC Group No G0607587 Contact Chris Ward Collection Dates 06/20/07 Address Box 7030 Lab Submittal Dates 06120/07 Chariotte MC 28241 This data package contains the analytical results for the project identified above and includes Case Narrative Laboratory Report and Quality Control Data totaling pages chainof -custody is also attached for the samples submitted to Prism for this project Data qualifiers are flagged individually on each sample key reference for the data qualifiers appears at the end of this case narrative Quality control statements and/or sample specific remarks are included in the sample comments section of the laboratory report for each sample affected Semi Volatile Analysis No Anomalies Reported Volatile Analysis No Anomalies Reported Metals Analysis N/A Wet Lab and Micro Analysis N/A Please call if you have any questions relating to this analytical report 77 Date Reviewed by Robbi Jones Project Manager Angela W6iercash Signature 1E4--Signature Review Date 06/29/07 Approval Date 06/29/07 Data Qualifiers Key Reference Compound also detected in the method blank Result outside of the QC limits DO Compound diluted out Estimated concentration calibration range exceeded The analyte was positively identified but the value is estimated below the reporting limit Estimated concentration with high bias Estimated concentration with low bias matrix effect is present Notes This report should not be reproduced except in its entirety without the writtten consent of Prism Laboratories Inc The results in this report relate only to the samples submitted for analysis 449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0403 Phone 704/529-6364 Toll Free 800/529-6364 Fax 704/525-0409 ESP Associates PA Attn Chris Ward Box 7030 Charlotte NC 28241 IA-123 COMP 185077 G0607587 06/20/07 1040 06/20/07 1635 Parameter Percent Solids Determination Percent Solids Result Units Report MDL Dilution Limit Factor Diesel Range Organics DRO by GC-FID Diesel Range Organics DRO Sample Preparation 370 mg/kg 40 5.0 25.36 Surrogate Recovery Control Limits Bromofluorobenzene 107 77 128 Dibromofluoromethane 93 67 143 Toluene-d8 93 81 128 8015B 06/27/07 1428 jvogel Q24575 mL 3545 06/25/07 1515 wconder P18738 Surrogate Recovery Control Limits o-Terphenyl 49 124 Gasoline Range Organics GRO by GC-FID Gasoline Range Organics GRO BRL mg/kg tI 0073 8015B 06/27/07 441 hwagner Q24580 Surrogate aaa-TFT Recovery 85 Control Limits 55-129 This report should not be reproduced except in fts entirety without the written consent of Prism Laboratories Inc 449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543 Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 NC Certification No 402 SC Certification No 99012 NC Drinking Water Cert No 37735 Laboratory Report 06/29/07 Project ID Morehead Commons No Client Sample ID Prism Sample ID Sample Matrix Soil COC Group Time Collected Time Submitted Method 87.4 Analysis Date/Time Analyst Batch ID SM2540 06/27/07 1800 Lthao Volatile Organic Compounds by GC1MS Benzene Ethylbenzene mp-Xytenes o-Xylene Toluene BRL BRL BRL BRL BRL pg/kg pg/kg pg/kg pg/kg pg/kg 3.8 0.51 6.3 044 13 0.88 6.3 0.38 6.3 0.43 8260B 8260B 8260B 8260B 8260B 06/27/07 806 erussell 024552 06/27/07 806 erussell 024552 06/27/07 806 erussell 024552 06/27/07 806 erussell Q24552 06/27/07 806 erussell 024552 Page of ESP Associates PA Attn Chris Ward Box 7030 Charlotte NC 28241 Laboratory Report 06/29/07 IA-123 COMP 185077 G0607587 06/20/07 1040 06/20/07 1635 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Sample Comments BRL Below Reporting Limit Estimated value between the Reporting Limit and the MDL The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than NELAC certification except for those instances indicated in the case narrative and/or test comments All results are reported on drj-weight basis Angela Overcash V.P Laboratory Services This report should not be reprdduced except in its entirety without the written consent of Prism Laboratories Inc 449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543 FiII Sec Analytical Environmental NC Certification No 402 SC Certification No 99012 NC Drinking Water Cert No 37735 Project ID Morehead Commons No Client Sample ID Prism Sample ID Sample Matrix Soil COC Group Time Collected Time Submitted Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page of ESP Associates PA Attn Chris Ward Box 7030 Charlotte NC 28241 Project ID Morehead Commons No Client Sample ID Prism Sample ID Sample Matrix Soil COC Group Time Collected Time Submitted B-234 COMP 185078 G0607587 06/20/07 1055 06/20/07 1635 Percent Solids Determination Percent Solids Surrogate Bromofluorobenzene Dibromofluoromethane Toluene-d8 Recovery 104 92 94 Control Limits 77-128 67-143 81 128 Diesel Range Organ ics DRO by GC-FID Diesel Range Organics DRO 140 mg/kg 7.9 0.99 8015B 06/27/07 330 jvogel 024575 Sample Preparation 25.12 mL 3545 06/25/07 1515 wconder P18738 Gasoline Range Organics GRO by GC-FID Gasoline Range Organics GRO BRL mg/kg Surrogate Recovery Control Limits o-Terphenyl 77 49 124 1.1 0.072 8015B 06/27/07 512 hwagner 024580 Surrogate Recovery Control Limits aaa-TFT 89 55-129 This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc 449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543 Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Full Service MaIyal Environmern_ NC Certification No 402 SC Certification No 99012 NC Drinking Water Cert No 37735 Laboratory Report 06/29/07 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 88.1 SM2540 06/27/07 1800 Lthao Volatile Organic Compounds by GC/MS Benzene Ethylbenzene mp-Xylenes o-Xylene Toluene BRL BRL BRL BRL BRL pg/kg pg/kg pg/kg pg/kg pg/kg 3.8 0.50 6.3 0.44 13 0.88 6.3 0.38 6.3 0.43 8260B 8260B 8260B 8260B 8260B 06/27/07 837 erussell 024552 06/27/07 837 erussell 024552 06/27/07 837 erussell 024552 06/27/07 837 erussell 024552 06/27/07 837 erussell 024552 Page of NC Certification No 402 Sc Certification No 99012 NC Drinking Water Cert No 37735 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DatelTime ID Sample Comments BRL Below Reporting Limit Estimated value between the Reporting Limit and the MDL The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than NELAC certification except for those instances indicated in the case narrative and/or test comments All results are reported on dr/-weight basis Angela Overcash V.P Laboratory Services This report shourd not be reproduced except in its entirety without the written consent of Prism Laboratories Inc 449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543 Fufl ServicE Analylical Environmental Soi..jons ESP Associates PA Attn Chris Ward P.O Box 7030 Charlotte NC 28241 Laboratory Report 06/29/07 Project ID Morehead Commons No Client Sample ID IB-234 COMP Prism Sample ID 185078 Sample Matrix Soil COC Group G0607587 Time Collected 06/20/07 1055 Time Submitted 06/20/07 1635 Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page of ESP Associates PA Attn Chris Ward Box 7030 Charlotte NC 28241 NC Certification No 402 SC Certification No 99012 NC Drinking Water Cert No 37735 This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc 449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543 Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Level II QC Report 6/29/07 Project ID Morehead Commons No COC Group Number G0607587 Date/Time Submitted 6/20/07 1635 Volatile nh-mnninrI hv R2ROB Method Blank QC Batch Result RL Control Limit Units ID 11 1-Trichloroethane ND 0.005 0.0025 mg/kg 024552 11 22-Tetrachloroethane ND 0.005 0.0025 mg/kg Q24552 11 2-Trichloroethane ND 0.005 0.0025 mg/kg 024552 11-Dichloroethane ND 0.005 0.0025 mg/kg 024552 1-Dichloroethene ND 0.005 0.0025 mg/kg 024552 1-Dichloropropene ND 0.005 0.0025 mg/kg Q24552 23-Trichlorobenzene ND 0.005 0.0025 mg/kg 024552 23-Trichloropropane ND 0.005 0.0025 mg/kg Q24552 24-Trichlorobenzene ND 0.005 0.0025 mg/kg 024552 24-Trimethylbenzene ND 0.005 0.0025 mg/kg 024552 2-Dibromoethane EDB ND 0.005 0.0025 mg/kg 024552 2-Dichlorobenzene ND 0.005 0.0025 mg/kg Q24552 12-Dichioroethane ND 0.005 0.0025 mg/kg Q24552 2-Dichloropropane ND 0.005 0.0025 mg/kg Q24552 35-Trimethylbenzene ND 0.005 0.0025 mg/kg Q24552 3-Dichlorobenzene ND 0.005 0.0025 mg/kg 024552 3-Dichloropropane ND 0.005 0.0025 mg/kg Q24552 4-Dichlorobenzene ND 0.005 0.0025 mg/kg Q24552 22-Dichioropropane ND 0.005 0.0025 mg/kg 024552 2-Chiorotoluene ND 0.005 0.0025 mg/kg 024552 2-Hexanone ND 0.05 0.025 mg/kg 024552 4-Chiorotoluene ND 0.005 0.0025 mg/kg 024552 4-Methyl-2-pentanone MIBK ND 0.05 0.025 mg/kg 024552 Acetone ND 0.05 0.025 mg/kg 024552 Benzene ND 0.003 0.0015 mg/kg 024552 Bromobenzene ND 0.005 0.0025 mg/kg 024552 Bromochioromethane ND 0.005 0.0025 mg/kg 024552 Bromodichloromethane ND 0.005 0.0025 mg/kg 024552 Bromoform ND 0.005 0.0025 mg/kg 024552 Bromomethane ND 0.01 0.005 mg/kg Q24552 Carbon tetrachloride ND 0005 0.0025 mg/kg 024552 Chlorobenzene ND 0.005 0.0025 mg/kg Q24552 Chlorodibromomethane ND 0.005 0.0025 mg/kg 024552 Chioroethane ND 0.01 0.005 mg/kg 024552 Page of Method Blank QC Batch Result RL Control Limit Units ID Chloroform ND 0.005 00025 mg/kg 024552 Chloromethane ND 0.005 0.0025 mg/kg Q24552 cis-12-Dichloroethene ND 0.005 0.0025 mg/kg 024552 cis-1 3-Dichloropropene ND 0.005 0.0025 mg/kg 024552 Dichlorodifluoromethane ND 0.005 0.0025 mg/kg Q24552 Ethylbenzene ND 0.005 0.0025 mg/kg 024552 lsopropyl ether IPE ND 0.005 0.0025 mg/kg 024552 lsopropylbenzene ND 0.005 0.0025 mg/kg Q24552 mp-Xylenes ND 0.01 0.005 mg/kg 024552 Methyl ethyl ketone MEK ND 0.1 0.05 mg/kg 024552 Methyl t-butyl ether MTBE ND 0.01 0.005 mg/kg Q24552 Methylene chloride ND 0.005 0.0025 mg/kg Q24552 n-Butylbenzene ND 0.005 0.0025 mg/kg 024552 n-Propylbenzene ND 0.005 0.0025 mg/kg 024552 Naphthalene ND 0.01 0.005 mglkg 024552 o-Xylene ND 0.005 0.0025 mg/kg 024552 p-lsopropyltoluene ND 0.005 0.0025 mg/kg Q24552 sec-Butylbenzene ND 0.005 0.0025 mg/kg 024552 Styrene ND 0.005 0.0025 mg/kg 024552 tert-Butylbenzene ND 0.005 0.0025 mg/kg 024552 Tetrachloroethene ND 0005 0.0025 mg/kg 024552 Toluene ND 0.005 0.0025 mg/kg Q24552 trans-I 2-Dichloroethene ND 0.005 0.0025 mg/kg 024552 trans-i 3-Dichloropropene ND 0.005 0.0025 mg/kg 024552 Trichloroethene ND 0.005 0.0025 mg/kg 024552 Trichlorofluoromethane ND 0.005 0.0025 mg/kg 024552 Vinyl acetate ND 0.025 0.0125 mg/kg 024552 Vinyl chloride ND 0.005 0.0025 mg/kg 024552 Laboratory Control Sample Recovery Recovery UC Batch Result Spike Amount Units lu ID 11-Dichloroethene 0.03808 0.05 mg/kg 76 57-122 024552 Benzene 0.04358 0.05 mg/kg 87 62-119 024552 Chlorobenzene 004441 0.05 mg/kg 89 61-124 024552 Toluene 0.04544 0.05 mg/kg 91 57-122 024552 Trichloroethene 0.04951 0.05 mg/kg 99 59-1 29 Q24552 This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc 449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543 Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 NC Certification No 402 Level II QC Report SC Certification No 99012 NC Drinking Water Cert No 37735 6/29/07 Full Serviuo Analylical Ennironmontal SaluCons ESP Associates PA Attn Chris Ward Box 7030 Charlotte NC 28241 Project ID Morehead Commons No COC Group Number G0607587 DatelTime Submitted 6/20/07 1635 Page of ESP Associates PA Attn Chris Ward Box 7030 Charlotte NC 28241 184791 Diesel Range Organics DRO 5t9 80 mg/kg 65 50-117 12 0-24 024575 This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc 449 Sprinybrook Road P.O Box 240543 Charlotte NC 28224-0543 Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 ervlce AnlylicI Envlronmrntal Solu6on NC Certification No 402 SC Certification No 99012 NC Drinking Water Cert No 37735 Level II QC Report 6/29107 Project ID Morehead Commons No COC Group Number G0607587 Date/Time Submitted 6/20/07 1635 Matrix Spike Recovery Recovery Ranges QC Batch Sample ID Result Spike Amount Units 185081 1-Dichloroethene 0031 18 0.05 mg/kg 62 44-140 024552 Benzene 0.03306 0.05 mg/kg 66 46-1 36 024552 Chlorobenzene 0.02555 0.05 mg/kg 51 47-135 024552 Toluene 0.0296 0.05 mg/kg 59 47-1 36 Q24552 Trichloroethene 0.03367 0.05 mg/kg 67 45-141 Q24552 Matrix Spike Duplicate Recovery Recovery RPD Ranges RPD Range DC Batch Sample ID Result Spike Amount Units ID 185081 1-Dichloroethene 0.03223 0.05 mg/kg 64 44-140 -23 024552 Berizene 0.03495 0.05 mg/kg 70 46-1 36 22 024552 Chlorobenzene 0.03 0.05 mg/kg 60 47-135 16 0-22 024552 Toluene 0.031 87 0.05 mg/kg 64 47-1 36 0-22 024552 Trichloroethene 0.03627 0.05 mg/kg 73 45-141 -23 024552 Diesel Range Organics 1DRO by GC-FID method 8015B Method Blank DC Batch Result RI Control Umit Units ID Diesel Range Organics DRO ND 3.5 mg/kg 024575 Laboratory Control Sample Recovery Recovery Ranges oc Batch Result Spike Amount Units Yo ID Diesel Range Organics DRO 49.0 80 mg/kg 61 55-109 024575 Matrix Spike Recovery Recovery Ranges DC Batch Sample ID Result Spike Amount Units ID 184791 Diesel Range Organics DRO 45.8 80 mg/kg 57 50-117 024575 Matrix Spike Duplicate Recovery Recovery RPD Ranges RPD Range DC Batch Sample ID Result Spike Amount Units ID Page 3of4 NC Certification No 402 Sc Certification No 99012 NC Drinking Water Cert No 37735 Project ID Morehead Commons No Level II QC Report 6/29/07 COG Group Number G0607587 DateiTime Submitted 6/20/07 1635 Box 7030 Charlotte NC 28241 ItPfl hi GC.FII mfhnd RflI5B 185077 Gasoline Range Organics GRO 1.968 -See Case Narrative mg/kg 98 37-126 34 024580 This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc 449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543 Phone 7041529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 ESP Associates PA Attn Chris Ward Method Blank QC Batch Result RL Control Limit Units ID Gasoline Range Organics GRO ND 0.5 mg/kg 024580 Laboratory Control Sample Recovery Recovery Ranges QC Batch IDResultSpikeAmountUnits Gasoline Range Organics GRO 1.966 mg/kg 98 64-124 024580 Matrix Spike Recovery Recovery Ranges DC Batch Sample ID Result Spike Amount Units ID 185077 Gasoline Range Organics GRO 2.016 mg/kg 101 37-126 024580 Matrix Spike Duplicate Recovery Recovery RRD Ranges RPD Range DC Batch Sample ID Result Spike Amount Units ID Page of CHAIN OF CUSTODY RECORD PAGE..L..OF...LQUOTET ENSUR PROP INGt ____________ Project Name /2L1ti 7W Short Hold Analysis Yes No UST Project YesL._o please ATTACH any project specific reporting QC LEVEL 111111 IV pro visions and/or QC Requireninfs Invoice To _Jl/l5 t/l-T Address /1/--pi/r.j iz Purchase Order NoJBiIling Reference .- Requested Due Date Day Days 03 Days Days 4Days Working Days 6-9 Days Standard 10 days usWork Must Be Samples received after 1500 will be processed next business day Turnaround time is based on business days excluding weekends and holidays SEE REVERSE FOR TERMS CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES INC TO CLIENT Relinquished By Signature Received By Signature uate Relinquished By Signature Received By Signature Date ReIinqulshedSignre ReeivedFomLororiesBy Method ci Shipm4otOTE AtL COOLERS SHOULD BE TAPED SHU sJITH USTOD FOR TRANSPORTATION TO THE LABORATORY SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST OC NTIL RECEIVED AT THE LABORATORY 7rOSGroup No Fed Ex UPS tlIand-delivered Prism Field Service Other PR-5B NPDES USJ GROUNDWATER DRINKING WATER SOLID WASTE RCRA CERCLA LANDFILL OTHER CC RlC fl cr fl Mr fl SC flNC SC NC USC NC SC NC USC NC SC NC SC Full Seniice Analytical Environmental Solutions 449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543 Client Company Name ____________________________ Phone 704/529-6364 Fax Report To/Contact Name Reporting Address _______________________________ Phone _______ Email Yes No Email Addrs EDD Type PDF__Ex Site Location Name Site Location Physical Address Fax Yes No lfhgr 7f7t 7J TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Certification NELAC_USACE__FL_____NCiL SC_OTHER Water Chlorinated YES_NO_ Sample Iced Upon Collection YES NO CLIENT SAMPLE DESCRIPTION DATE COLLECTED TIME COLLECTED MILITARY HOURS MATRIX SOIL WATER OR SLUDGE SAMPLE CONTAINER PRESERVA- TIVES ANALYSES REQUESTED -c/AC jXJ 11p REMARKS3____ PRISM ID NOTYPE SEE BELOW NO SIZE -I /-245/6_2/Ø5 -2 io9o /Dcp Josç /25 I/--cczz/1f1 pLcL p15---IS5 Samplers Signature e-S Sampled By Print Name Upon relinquishing this In of Custols your authorization for Prism to proceed with the analyses as requested above Any changes must be submitted in writing to the Prism Project Manager There will be charges for any changes after analyses have been initialized ___________ -I I111j Additional Comments FgTe2t1ee SEEREVERSEFORTERMSCONDITIONS