Item No 20 - 20Day Report - Morehead Common Site Area No 1-OCR

Pr
Preoar dBy
Dear Mr Schiff
On behalf of the property owner and our client Beazer Homes ESP Associates P.A is pleased
to provide the attached 20-Day Report for release of petroleum product
at the subject site as
discovered during mass grading operations
of this area
Thank you for your attention in this matter If you should have any questions please
do not
hesitate to contact me at 803 835-0915
Sincerely
ard PG
Environmental Services
NC License No 1600
P.O Box 7030 Charlotte NC 28241
1.800.960.7317 NC 704.583.4949 fax [phone] SC 803.802.2440 fax [phone]
www.espassociates.com
July 18 2007
$ESP
ESP Associates P.A
NCDENR
UST Section
Mooresville Regional Office
919 North Main Street
Mooresville North Carolina 28115
Attention Mr Allen Schiff
Reference 20-DAY REPORT
Morehead Common Site Area No
1000 South Clarkson Street
Charlotte North Carolina
Incident No Not Yet Assigned
ESP Project No E6-UD42.601
ESP Associates P.Av7
cc Mr Jade Eastridge
20-Day Report
SITE INFORMATION
Site Identification
Date of Report July 18 2007
Facility ID N/A
UST Incident Number Not Yet Assigned
Site Name Morehead Common Site Area No
Site Street Address 1000 South Clarkson Street
CD City/County/Zip Code Charlotte Mecklenburg County 28278
CD Description of Geographical Data Point Approximate center of UST
Location Method Mecklenburg County
Polaris GIS Map
Latitude 35.22702
Longitude -80.85892
Information about Contacts Associated
with the Leaking UST System
UST Owner Beazer Homes
1300 Blvd Suite Charlotte NC 28203-4265
704.370.7200
CD UST Operator N/A
Property Owner Same as above
CD Property Occupant Same as above
Consultant/Contractor ESP Associates P.A Chris Ward PG
P0 Box 7030 Charlotte NC 28241
803.835.0915
CD Analytical Laboratory Prism Laboratories Inc
P0 Box 240543 Charlotte NC 28224-0403
704.529.6364
NC Certification No 402
Information about Release
Date Discovered May 15 2007
CD Estimated Quantity of Release Unknown
CD Cause of Release Unknown
Source of Release Suspect UST found crushed and pitted in adjacent
debris stockpile
CD Size and contents of UST
system from which release occurred Approximate 500-gallons
Certification
Chris Ward Professional Geologist for ESP Associates P.A do certif that the
information contained in this report is correct and accurate to the best of my knowledge
ESP Associates P.A is licensed to practice both geology and engineering in North Carolina
ESP Associates certification numbers are Geology C-347 Engineering C-0587
20-Day Report ESP Project E6-UD42 601
Morehead Common Site Area No July 18 2007
INTRODUCTION
On May 15 2007
ESP responded on behalf of Beazer Homes to an encounter with impacted soil
during mass grading operations
at the subject site Upon arriving at the site ESP observed soils
with an apparent petroleum odor located on the west side of South Clarkson Street approximately
500 feet south of its intersection with West Morehead Street on Tax Parcel No 07325207 see
Figures and The incident area has been designated as Area No As required ESP
emailed notification of the release discovery to Mr Steve Bograd of the Mooresville Regional
Office of NCDENR on May 16 2007
During subsequent soil excavation activities as detailed below abandoned MACTEC monitor
well 18101 associated with closed-out Incident No 18101 was uncovered approximately 15
feet southwest of the southwestern end of the excavation see Figure
The subject site is located within an urban area of Charlotte which historically included
warehouse and retail structures The site is currently mass graded and being developed as
mixed-use development see Figures and Based on our review of the Geologic Map of
North Carolina 1985 the subject site is located within the Charlotte Belt locally comprised of
intrusive metamorphosed granitic rocks locally pinkish gray massive to weakly foliated and
containing hornblende Soils encountered in this area are the residual product of chemical
weathering of rock presently underlying the site Soil weathering is more advanced near the
surface grading with depth to less weathered rock and finally bedrock
INITIAL ABATEMENT ACTIVITIES
Waste Characterization Sampling
On May 15 2007
ESP collected waste characterization soil sample PS-i from the impacted
area at depth of approximately feet below land surface BLS using backhoe
20-Day Report ESP Project E6-UD42 601
Morehead Common Site Area No July 18 2007
representative portion of the soil sample was screened in the field with an organic vapor analyzer
OVA and recorded reading of 150 ppm Soil sample PS-i was submitted to Prism
Laboratories of Charlotte North Carolina for analysis of total petroleum hydrocarbons TPH for
diesel range organics DRO and gasoline range organics GRO oil grease OG by EPA
Method 9071A volatile organic compounds VOCs by EPA Method 8260B pesticides by EPA
Method 8081A PCBs by EPA Method 8082 and for total lead and chromium by EPA Method
601 OB Waste characterization soil sample PS-i was collected and analyzed to document that
release of petroleum had occurred and to characterize contaminant concentrations for subsequent
off-site permitted disposal/treatment
As revealed by the attached laboratory data report for PS-i TPH-DRO was reported at
concentration of 3600 mg/Kg OG was reported at 10000 mg/Kg
while several VOCs were
reported above reporting limits Results for TPH-GRO were below reporting limits See Figure
for soil sample location map See the attached Prism laboratory data report
Soil Excavation and Confirmatory Sampling
On May 30 June and 2007 ESP documented the excavation of approximately 1100 cubic
yards of impacted soils from Area No by the sites grading contractor Gelder Thompson of
Midland North Carolina The excavation was advanced based on OVA readings and evidence
of visible staining The resulting excavation measured approximately 25 ft 110 ft 10 ft
deep Neither groundwater bedrock nor free product were encountered within the tank pit
The excavated soil was placed on and covered with plastic awaiting subsequent off-site
permitted disposal
On June 2007 ESP collected six composite soil samples for laboratory
analysis The soil samples designated AB through AB were placed in laboratory
provided containers labeled
and hand delivered on ice to Prism Laboratories for compositing
and subsequent analysis The samples were analyzed for TPH-GRO/DRO BTEX TCLP-metals
and TCLP-Toxicity
20-Day Report ESP Project E6-UD42 601
Morehead Common Site Area No July 18 2007
On June 2007 confirmatory soil samples were collected at depth of feet BLS from each of
the excavations four sides WS-through WS-4 while two samples were collected at depths of
10 feet BLS from the base of the excavation BS-1 and BS-2 The six soil samples were hand
delivered on ice to Prism Laboratories to be analyzed for NCDENR risk-based parameters
which include volatile and semi-volatile organics by EPA Methods 8260B and 8270C and for
VPH/EPH by the Massachusetts Department of Environmental Protection MADEP method
Sample locations and excavation dimensions are depicted on Figure Soil Sample Location
Map Sampling was performed in general accordance with ESPs SOP see Appendix
FUTURE REPORTING
An Initial Abatement Action Report is currently being prepared
for this release
ATTACHMENTS
FIGURES
FiGURE
TOPOGRAPHIC ShE LOCA liON MAPUSGS CHARLOTTE EAST QUADRANGLE
MOREHEAD COMMON ShE
CHARLOTTE NORTH CAROLINA
ESP
FiGURE
2005 AERIAL PHOTOGRAPH
MOREHEAD COMMON SiTE
CHARLOTTE NORTH CAROLINA
ESP
LEGEND
WS-3
WS-4
CONRRMA TORY SOIL SAMPLE LOCA T1ON
EXCA VA 710N DEPTH OF 10 FEET
20
APPIOX/MA 7E SCALE
IN FEET
FiGURE
SOIL SAMPLE LOCA 11CW MAP AREA
MOREHEAD CQVMON SITE
CHARLOTTE NORTH CAROLINA ESP ESP Associates PA
P0 7030
Chcrlotte tIC 28231
3472 Lkcsosr BOd
Forr Mdl Sc 20708
704-583-4940 NC
803-802-2440 SC
ws-1
SITE PHOTOGRAPHS
24-HOUR RELEASE AND UST REPORTING FORM
rage ot
Chris Ward
From Chris Ward
Sent Wednesday May 16 2007 1120 AM
To Steve.BogradncmaiLnet
Cc Jade Eastridge [e-mail]
Subject 24-Hour Notification
Attachments morehead commons.pdf
Steve
On behalf of Beazer Homes am herein providing 24-Hour Notification of the discovery of soils with
petroleum/chemical odor on Beozer Homes Moreheod Commons residential development currently being graded
The Morehead Commons property is located on the south side of West Morehead Street at its intersection with
South Clarkson Street in Charlotte North Carolina On May 15 2007 Mr Chris Ward of ES observed apparent
environmentally-impacted soils encountered during grading operations on the subject site The apparent impacted
soils with petroleum/chemical odor were encountered beneath an old building foundation located on the west side
of South Clarkson Street approximately 500 feet south of its intersection with West Morehead Street on Tax
Parcel No 07325207 see attached map as PbF The vicinity of the impacted soils was once occupied by
various
warehouses and industrial and commercial businesses before being demolished
On May 15 2007 ci waste characterization soil sample was collected from depth of approximately 5.5 feet below
land surface BLS and submitted to Prism Laboratories for rush analysis An OVA reading of 150 ppm was
recorded at the 5.5 foot depth interval which appeared to include the most impacted soil The soil sample will be
analyzed for volatile organic compounds VOCs by EPA Method 82608 pesticides by EPA Method 8081
polychlorinated biphenyls PCBs by EPA Method 8082 oil and grease by EPA Method 9071 for total petroleum
hydrocarbons by EPA Methods 3550 and 5030 and for total lead and chromium by EPA Method 3051
Following receipt of the laboratory results for the waste characterization sample ESP will direct the excavation of
impacted soils and their transported to an off-site permitted disposal facility Confirmatory soil samples will then
be collected from the walls and base of the excavation Assuming acceptable results soil closure report will then
be prepared for submittal to NCbENR
The Responsible Party for the property is
Beazer Homes
1300 South Boulevard
Suite
Charlotte North Carolina 28203-4265
Mr Jade Eastridge
704.370.7200
Please call with any questions
Thanks
Chris Ward PG
Environmental Services Manager
7/17/2007
rage 01
ESP ASSOCIGtSS
803.835.0915 direct office
803.802.2515 fax
704.506.7618 mobile
711 7/fl7
nvtcJ VU SHEET 7YTLE
2005 AERIAL PHO100RAPH5/16/07 _____________________________________________WAWr7 PROJECT MORE7IEAD CCWMONS 17
OHARLOTTC NW CAROUNA
EO JUN 2007
Case Narrative RevisedPRISM
LABORATORIESINC
Date 06/20/07 Client Project ID Morehead Commons No
Company ESP Associates PA Prism COC Group No G06071 10
Contact Chris Ward Collection Dates 06/05/07
Address Box 7030 Lab Submittal Dates 06/05/07
Charlotte NC 28241
This is revised report and supersedes our original laboratory report dated 06/13/07 Client added full list 8260 8270
This data package contains the analytical results for the project identified above and includes Case Narrative Laboratory Report Quality
Control and Subcontracted Laboratory Report with corresponding Chain-of-Custody totaling 66 pages chain-of-custody is also attached for
the samples submitted to Prism for this project
Data qualifiers are flagged individually on each sample key reference for the data qualifiers appears at the end of this case narrative Quality
control statements and/or sample specific remarks are included in the sample comments secfion of the laboratory report for each sample
affected
Semi Volatile Analysis
No Anomalies Reported
Volatile Analysis
No Anomalies Reported
Metals Analysis
No Anomalies Reported
Wet Lab and Micro Analysis
N/A
Please call if you have any quesfions relating to this analycal report
Date Reviewed by Paula Gilleland Project Manager Angela vercash
Signature P.uIc 1ia cL Signature ____________________________
Review Date 06/20/07 Approval Date 06/20/07
Data Qualifiers Key Reference
Compound also detected in the method blank
Result outside of the QC limits
DO Compound diluted out
Estimated concentration calibration range exceeded
The analyte was positively identified but the value is estimated below the reporting limit
Estimated concentraon with high bias
Estimated concentration with low bias
matrix effect is present
Notes This report should not be reproduced except in its entirety without the writtten consent of Prism Laboratories Inc The results in this
report relate only to the samples submitted for analysis
449 Springbrook Road P.O Box 240543 Chariotte NC 28224-0403
Phone [phone] Toll Free 800/529-6364 Fax [phone]
NC Certification No 402 Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID AB
Prism Sample ID 183468
Sample Matrix Soil COC Group G06071 10
Time Collected 06/05/07 1100
Time Submitted 06/05/07 1610
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
ESP Associates PA
ttn Chris Ward
P.O Box7030
harlotte NC 28241
06/20/07
Limit Factor Date/Time ID
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
ercet1t Solids Determination
Percent Solids 82.6 SM2540 06/11/07 1700 brown
olatile Organic Compounds by GC/MS
111 2-Tetrachloroetharie BRI pg/kg 6.1 0.66 8260B 06/07/07 1846 erussell 024080
11-Trichloroethane BRL pg/kg 6.1 0.38 8260B 06/07/07 1846 erussell 024080
11 22-Tetrachloroethane BRL pg/kg 6.1 0.69 8260B 06/07/07 1846 erussell 024080
2-Trichloroethane BRL pg/kg 6.1 0.42 8260B 06/07/07 1846 erussell 024080
11-Dichioroethane BRL pg/kg 6.1 0.49 8260B 06/07/07 1846 erussell 024080
11-Dichloroethene BRL pg/kg 6.1 0.51 8260B 06/07/07 1846 erussell 024080
1-Dichloropropene BRL pg/kg 6.1 0.59 8260B 06/07/07 1846 erussell 024080
23-Trichlorobenzene BRL pg/kg 12 0.74 8260B 06/07/07 1846 erussell 024080
23-Trichloropropane BRL pg/kg 6.1 0.59 8260B 06/07/07 1846 erussell 024080
24-Trichlorobenzene BRL pg/kg 12 0.65 8260B 06/07/07 1846 erusseu 024080
24-Trimethylbenzene 560 pg/kg 300 23 50 82608 06/08/07 1933 erussell 024080
2-Dibromc-3-chloropropane BRL pg/kg 6.1 1.1 8260B 06/07/07 1846 erussell 024080
2-Dibromcethane EDB BRL pg/kg 6.1 0.12 8260B 06/07/07 1846 erussell 024080
i2-Dichlorobenzene BRL pg/kg 12 0.36 8260B 06/07/07 1846 erussell Q24080
2-DichIoroethane BRL pg/kg 6.1 0.67 8260B 06/07/07 1846 erussell 024080
.2-Dichloropropane BRL pg/kg 6.1 0.50 82608 06/07/07 1846 erussell 024080
135-Trimethylbenzene 83 pg/kg 12 0.57 8260B 06/07/07 1846 erussell Q24080
3-Dichlorobenzene BRL pg/kg 12 0.58 8260B 06/07/07 1846 erusserl 024080
13-Dichloropropane BRL pg/kg 6.1 0.46 82608 06/07/07 1846 erussell 024080
4-Dichlorobenzene BRL pg/kg 12 0.53 82608 06/07/07 1846 erussell 024080
22-Dichloropropane BRL pg/kg 6.1 0.34 8260B 06/07/07 1846 erussel 024080
-Chloroethyl vinyl ether BRL pg/kg 12 0.50 826DB 06/07/07 1846 erussell 024080
-Chlorotoluene BRL pg/kg 12 0.50 826DB 06107/07 1846 erussell 024080
-Hexanone BRL pg/kg 61 0.70 826DB 06/07/07 1846 erussell Q24080
Page of 42
Laboratory Report
06/20/07
Project ID Morehead Commons No Client Sample ID AB
Prism Sample ID 183468
Sample Matrix Soil COC Group G06071 10
Time Collected 06/05/07 11100
Time Submitted 06/05/07 1610
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 23224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Dnnking Water Cert No 37735
iufl Service Analytical Environmental Solutions
ESP Associates PA
ttn Chris Ward
Box 7030
harIotte NC 28241
Parameter Result Units Report MDL Dilution Method
Limit Factor Date/Time ID
Analysis Analyst Batch
-Chlorotoluene BRL pg/kg 12 0.35 82608 06/07/07 1846 erussell Q24080
4-Methyl-2-pentanone MIBK BRL pg/kg 12 0.67 8260B 06/07107 1846 erussell 024080
cetone BRL pg/kg 24 2.6 8260B 06/07/07 1846 erusseH Q24080
Benzene BRL pg/kg 3.6 0.54 8260B 06/07/07 1846 erussell Q24080
tromobenzene BRL pg/kg 6.1 0.47 8260B 06/07/07 1846 erussell Q24080
romochIoromethane BRL pg/kg 6.1 0.40 8260B 06/07/07 1846 erussell Q24080
Iromodichioromethane BRL pg/kg 6.1 0.59 8260B 06/07/07 1846 erussefl 024080
Jromoform BRL pg/kg 6.1 0.50 82608 06/07/07 1846 erussell 024080
Jromomethane BRL pg/kg 12 0.78 8260B 06/07/07 1846 erussell 024080
arbon disulfide BRL pg/kg 12 0.43 8260B 06/07/07 1846 erussell 024080
Carbon tetrachloride BRL pg/kg 6.1 0.39 82608 06/07/07 1846 ewssefl Q24080
hIorobenzene BRL pg/kg 6.1 0.51 8260B 06/07/07 1846 erussell Q24080
Chlorodibromomethane BRL pg/kg 6.1 0.46 82608 06/07/07 1846 erussell 024080
hIoroethane BRL pg/kg 12 0.55 82608 06/07/07 1846 erusseH 024080
Ôhloroform BRL pg/kg 6.1 0.50 8260B 06/07/07 1846 erussell 024080
hloromethane BRL pg/kg 12 0.47 8260B 06/07/07 1846 erussell 024080
.is-1 2-Dichloroethene BRL pg/kg 6.1 0.30 8260B 06/07/07 1846 erussell 024080
is-i 3-Dichloropropene BRL pg/kg 6.1 0.43 82608 06/07/07 1846 erusseD 024080
ibromomethane BRL pg/kg 6.1 0.50 8260B 06/07/07 1846 erussell 024080
Dichiorodifluoromethane BRL pg/kg 12 1.5 82608 06/07/07 1846 erussell Q24080
thylbenzene BRL pg/kg 6.1 0.47 8260B 06/07/07 1846 erussell Q2408o
Hexachiorobutadiene BRL pg/kg 18 0.84 8260B 06/07/07 1846 erussell 024080
opropyl ether IPE BRL pg/kg 6.1 0.23 8260B 06/07/07 1846 erussell Q24080
Isopropylbenzene BRL pg/kg 12 0.54 8260B 06/07/07 1846 erussell Q24080
ip-Xylenes 14 pg/kg 12 0.94 8260B 06/07/07 1846 erussell Q24080
i1ethyI ethyl ketone MEK BRL pg/kg 24 1.9 8260B 06/07/07 1846 erussell Q24080
lethyl t-butyl ether MTBE BRL pg/kg 6.1 0.39 82608 06/07/07 1846 erussell 024080
Page of 42
NC Certification No 402AI1iJVItPiiIScCertificationNo99012
NC Drinking Water Cert No 37735
--dull Service Analytical Environmental Solutions
ESP Associates PA
\ttn Chris Ward
Box 7030
Oharlotte NC 28241
Project ID
Sample Matrix
Laboratory Report
06/20/07
Morehead Commons No Client Sample ID
Prism Sample ID
Soil COC Group
Time Collected
Time Submitted
AB
183468
G06071 10
06/05/07 1100
06/05/07 1610
Result Units Report MDL Dilution Method Analysis
Limit Factor Date/Time
Analyst Batch
ID
i5arameter
Aethylene chloride 20 pg/kg 12 0.55 826GB 06/07/07 1846 erussell Q24080
n-Butylbenzene 17J pg/kg 18 0.54 826GB 06/07/07 1846 erusseH Q24080
i-Propylbenzene 4.2 pg/kg 12 0.40 826GB 06/07/07 1846 erussell Q24080
Naphthalene 380 pg/kg 300 35 50 826GB 06/08/07 1933 erussell 024080
-Xylene BRL pg/kg 6.1 0.40 826GB 06/07/07 1846 erussell 024080
-lsopropyltouene 97 pg/kg 18 0.55 826GB 06/07/07 1846 erusseH 024080
ec-Butylbenzene 16J pg/kg 18 0.44 826GB 06/07/07 1846 erussell 024080
3tyrene BRL pg/kg 6.1 0.67 826GB 06/07/07 1846 erussefl 024080
ert-Butylbenzene 12J pg/kg 24 0.42 826GB 06/07/07 1846 erussell 024080
etrachloroethene BRL pg/kg 12 1.2 826GB 06/07/07 1846 erussefl 024080
Toluene BRL pg/kg 6.1 0.46 826GB 06/07/07 1846 erussell 024080
rans-12-Dichloroethene BRL pg/kg 6.1 0.51 826GB 06/07/07 1846 erussell 024080
trans-I 3-Dichloropropene BRL pg/kg 6.1 0.47 826GB 06/07/07 1846 erussell 024080
richloroethene BRL pg/kg 6.1 0.40 826GB 06/07/07 1846 erussell 024080
lrichlorofiuoromethane BRL pg/kg 6.1 0.55 826GB 06/07/07 1846 erusseH 024080
/inyl chloride BRL pg/kg 12 0.86 826GB 06/07/07 1846 erussell Q24080
Two surrogate recoveries were outside of the control limits Matrix interference is suspected
emi-voIatile Orcianic Compounds bvGC/MS
24-Trichlorobenzene BRL
2-Dichlorobenzene BRL
3-Dichlorobenzene BRL
4-Dichlorobenzene BRL
Surrogate Recovery Control Limits
Bromofluorobenzene 167 77 128
Dibromofluoromethane 146 67 143
Toluene-d8 107 81 128
pg/kg
pg/kg
pg/kg
pg/kg
400 40 8270C
400 30 827GC
400 29 8270C
400 36 827GC
06/19/07 906 kcampigotto
06/19/07 906 kcampigotto
06/19/07 906 kcampigotto
06/19/07 906 koampigotto
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Q24348
Q24348
Q24348
024348
Page of 42
Laboratory Report
06/20/07
Project ID Morehead Commons No Client Sample ID AB
Prism Sample ID 183468
Sample Matrix Soil COC Group G06071 10
Time Collected 06/05/07 1100
Time Submitted 06/05/07 1610
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Result Units Report MDL Dilution Method
Limit Factor Date/Time ID
Analysis Analyst Batch
SP Associates PA
ttn Chris Ward
Box 7030
1harlotte NC 28241
1arameter
45-Trichlorophenol
246-Trichiorophenol
4-Dichlorophenol
24-Dimethylphenol
4-Dinitrophenol
24-Dinitrotoluene
T6-Dinitrotoluene
-ChIoronaphthalene
2-Chlorophenol
-Methylnaphthalene
2-Methyiphenol
-Nitrophenol
34-Methylphenol
3-Dichlorobenzidine
46-Dinitro-2-methylphenol
-Bromophenylphenylether
-Chloro-3-methylphenol
4-Chiorophenylphenylether
-Nitrophenol
Acenaphthene
.cenaphthylene
Anthracene
enzoaanthracene
enzoapyrene
enzobfluoranthene
..enzoghiperylene
enzokfluoranthene
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
790
860
350
690
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
400 41
400 38
400 34
400 39
400 45
400 23
400 43
400 41
400 32
400 32
400 38
400 48
400 41
400 25
400 24
400 38
400 29
400 25
400 27
400 39
400 40
400 30
400 56
400 46
400 18
400 19
400 33
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcarnpigotto Q24348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto 024348
Page of 42
NC Certification No 402
Sc Certification No 99012
NC Dnnking Water Cert No 37735
u1l Sn on Analytical Environmental Solutions
ESP Associates PA Project ID
Utn Chris Ward
Box 7030
harIotte NC 28241
Laboratory Report
Morehead Commons No Client Sample ID AB
Prism Sample ID 183468
COG Group G0607110
Time Collected 06/05/07 1100
Time Submitted 06/05/07 1610
06/20/07
Limit Factor
400 46 8270C
400 44 8270C
400 34 8270C
400 20 8270C
400 25 8270C
400 67 8270C
400 18 8270C
400 30 8270C
400 40 8270C
400 34 8270C
400 25 8270C
400 27 8270C
400 28 8270C
400 24 8270C
400 21 8270C
400 39 8270C
400 42 8270C
400 41 8270C
400 41 8270C
400 36 8270C
400 45 8270C
400 20 8270C
400 44 8270C
400 39 8270C
400 34 8270C
400 20 8270C
400 44 8270C
Analysis Analyst
Batch
Date/Time ID
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampgotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampgotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto Q24348
06/19/07 906 kcampigotto 024348
06/19/07 906 kcampigotto Q24348
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Sample Matrix Soil
Parameter Result Units Report MDL Dilution Method
is2-chIoroethoxymethane BRL pg/kg
Bis2-chloroethylether BRL pg/kg
is2-chloroisopropylether BRL pg/kg
Bis2-ethylhexylphthalate BRL pg/kg
utylbenzylphthalate BRL pg/kg
Chrysene BRL pg/kg
i-n-butylphthalate BRL pg/kg
i-n-octyIphthalate BRL pg/kg
ribenzoahanthracene 240 pg/kg
iibenzofuran BRL pg/kg
Diethylphthalate BRL pg/kg
1imethylphthalate BRL pg/kg
Fluoranthene 2200 pg/kg
luorene BRL pg/kg
Hexachlorobenzene BRL pg/kg
lexachlorobutadiene BRL pg/kg
exachIorocyclopentadiene BRL pg/kg
exachIoroethane BRL pg/kg
ideno1 23-cdpyrene 650 pg/kg
sophorone BRL pg/kg
-Nitrosodi-n-propylamine BRL pg/kg
N-Nlitrosodiphenylamine BRL pg/kg
aphthalene BRL pg/kg
Nitrobenzene BRL pg/kg
entachlorophenol BRL pg/kg
-tienanthrene 1900 pg/kg
Dhenol BRL pg/kg
Page of 42
dill Service Analytical Environmental Solutions
SP Associates PA
ttn Chris Ward
P.O Box7030
Tharlotte NC 28241
Laboratory Report
06/20/07
AB
183468
G0607110
06/05/07
06/05/07
1arameter
yrene
Result Units Report
Limit
Analysis
Date/Time
Analyst Batch
ID
Sample Preparation
iesel Range Organics DRO by GC-FID
iesel Range Organics DRO 3000
Sample Preparation
Gasoline Range Organics GRO by GC-FID
asoIine Range Organics GRO
CLP Extraction for Metals
CLP Extraction
29.86 mL 3550B 06/15/07 900 dpope P1 8642
Surrogate Recovery Contirol Limits
246-Tribromophenol 57 25-123
2-Fluorobiphenyl 91 21 108
2-Fluorophenol 59 14-89
Phenol-d5 64 13-95
Terphenyl-d14 86 41 136
Nitrobenzene-d5 91 14 103
mg/kg 170 21 20 8015B 06/08/07 1104 ivogel Q24180
25.24 mL 3545 06/07/07 910 wconder P1 8568
Surrogate Recovery Control Limits
o-Terphenyl DO 49 124
Q241215.2 mg/kg 1.2 0.077 8015B 06/07/07 2355 hwagner
Complete
Surrogate Recovery Control Limits
aaa-TFT 102 55-129
1311 06/06/07 1345 jhoppel
CLP Leachable Mercury by CVAA
1ercury
Sample Preparation
BRL mgIL 0.010 0.000042
2OmL 3OmL
7470A 06/08/07 1600 jhoppel
7470A 06/08/07 715 jhoppel
Q24140
P18573
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
1100
1610
MDL Dilution Method
Factor
1600 ig/kg 400 27 8270C 06/19/07 906 kcampigotto Q24348
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of 42
ample Comments
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
BRL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
Jhe results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthoseinstances indicated in the case narrative and/or test comments
results are reported on dry-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
.SP Associates PA
ttn Chris Ward
Box 7030
harlotte NC 28241
Laboratory Report
06/20/07
AB
183468
G06071 10
06/05/07
06/05/07
Result Units Report MDL Dilution
Limit Factor
III 00
1610
Method Analysis
Date/Time
Parameter
CLP Leachable Metals by ICP
Arsenic
arium
admium
hromium
tead
Selenium
Sample Preparation
otaI Halocien by Method 9076
Subcontract Report
Analyst Batch
ID
O.0042J mg/L 0.050 0.0029 6010B 06/11/07 1541 mcampbell 024175
0.82J mg/L 5.0 0.0019 6010B 06/11/07 1541 rncampbell 024175
BRL mg/L 0.025 0.00034 6010B 06/11/07 1541 mcampbell Q24175
0.0049 mg/L 0.25 0.0006 6010B 06/11/07 1541 mcampbell Q24175
0.016J mg/L 0.050 0.0021 6010B 06/11/07 1541 mcampbell 024175
0.0077J mg/L 0.050 0.0035 6010B 06/11/07 1541 mcampbell Q24175
BRL mg/L 0.25 0.00025 6010B 06/11/07 1541 mcampbell 024175
See
Attached
50 mL 50 mL 3010A 06/11/07 900 jhoppel P1 8570
9076
Analysis Note for Subcontract Report Analysis subcontracted to NC certified lab 618
Page of 42
Project ID Morehead Commons No Client Sample ID AB
Prism Sample ID 183469
Sample Matrix Soil COG Group G0607110
Time Collected 06/05/07 1200
Time Submitted 06/05/07 1610
Parameter Result Units Report MDL Dilution Method
Limit Factor
Analysis
Dateflime
Analyst Batch
ID
ercent Solids Determination
Percent Solids 83.0 SM2540 06111/07 1700 brown
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224.0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
ttn Chris Ward
Box7030
Oharlotte NC 28241
Laboratory Report
06/20/07
olatile Organic Comeounds by GC/MS
111 2-Tetrachloroethane BRL pg/kg 6.0 0.61 826GB 06/07/07 1929 erussell Q24080
111 -Trichloroethane BRL pg/kg 6.0 0.35 826GB 06/07/07 1929 erussell 024080
11 22-Tetrachloroethane BRL pg/kg 6.0 0.63 826GB 06/07/07 1929 erussell 024080
11 2-Trichloroethane BRL pg/kg 6.0 0.38 826GB 06/07/07 1929 erussell 024080
11-Dichloroethane BRL pg/kg 6.0 0.45 826GB 06/07/07 1929 erussell Q24080
11-Dichioroethene BRL pg/kg 6.0 0.47 826GB 06/07/07 1929 erussell Q24G80
I1-DichIoropropene BRL pg/kg 6.0 0.54 826GB 06/07/07 1929 erusseH Q24080
23-Trichlorobenzene BRL pg/kg 12 0.68 826GB 06/07/07 1929 erussell 024080
123-Trichioropropane BRL pg/kg 6.0 0.54 826GB 06/07/07 1929 erussell 024080
24-Trichlorobenzene BRL pg/kg 12 0.59 826GB 06/07/07 1929 erussell Q24G80
l24-Trimethylbenzene 500 pg/kg 300 23 50 826GB 06/08/07 1817 erussell Q24G8G
12-Dibromo-3-chloropi-opane BRL pg/kg 6.0 0.98 826GB 06/07/07 1929 erussell Q24G80
I2-Dibromoethane EDB BRL pg/kg 6.0 0.11 826GB 06/07/07 1929 erussell 024080
I2-Dichlorobenzene BRL pg/kg 12 0.33 826GB 06/07/07 1929 erussell 024080
2-Dichloroethane BRL pg/kg 6.0 0.62 826GB 06/07/07 1929 erussell 024080
i2-Dichloropropane BRL pg/kg 6.0 0.46 826GB 06/07/07 1929 erussell Q24G8G
35-Trimethylbenzene 88 pg/kg 12 0.52 826GB 06/07/07 1929 erussell Q24G80
3-Dichlorobenzene BRL pg/kg 12 0.53 826GB 06/07/07 1929 erusseU Q24G8G
13-Dichioropropane BRL pg/kg 6.0 0.42 826GB 06/07/07 1929 erussell 024080
Dichlorobenzene BRL pg/kg 12 48 826GB 06/07/07 1929 erussell Q24G80
22-Dichioropropane BRL pg/kg 6.0 0.31 826GB 06/07/07 1929 erussell 024080
-Chloroethyl vinyl ether BRL pg/kg 12 0.46 826GB 06/07/07 1929 erussell 024080
2-Chlorotoluene BRL pg/kg 12 0.46 826GB 06/07/07 1929 ewssell Q24G80
2-Hexanone BRL pg/kg 60 0.64 826GB 06/07/07 1929 erussell Q24080
Page of 42
Laboratory Report
06/20/07
Project ID Morehead Commons No Client Sample ID AB
Prism Sample ID 183469
Sample Matrix Soil COC Group G0607110
Time Collected 06/05/07 1200
Time Submitted 06/05/07 1610
Parameter
-Chiorotoluene
4-Methyl-2-pentanone MIBK
cetone
Benzene
romobenzene
omochloromethane
Iromodichloromethane
-iromofomi
Bromomethane
arbon disulfide
Carbon tetrachioride
hIorobenzene
Chiorodibroniomethane
hloroethane
chloroform
hloromethane
us-I 2-Dichloroethene
cis-1 3-Dichloropropene
ibromomethane
Dichiorodifluoromethane
thylbenzene
Hexachiorobutadjene
sopropyl ether IPE
isopropylbenzene
ip-Xylenes
ethyl ethyl ketone MEK
Methyl t-butyl ether MTBE
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
----ill Service Analytical Environmental Solutions
SP Associates PA
ttn Chris Ward
P.O Box 7030
Iharlotte NC 28241
Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
BRL pg/kg 12 0.32 8260B 06/07/07 1929 erussell Q24080
BRL pg/kg 12 0.62 826GB 06/07/07 1929 erussell Q24080
BRL pg/kg 24 2.4 826GB 06/07/07 1929 erussell 024080
BRL pg/kg 3.6 0.49 826GB 06/07/07 1929 erussell Q24080
BRL pg/kg 6.0 0.43 826GB 06/07/07 1929 erussefl 024080
BRL pg/kg 6.0 0.37 826GB 06107/07 1929 erussell Q24080
BRL pg/kg 6.0 0.54 826GB 06/07/07 1929 erussell Q24G80
BRL pg/kg 6.0 0.46 826GB 06/07/07 1929 erussell 024080
BRL pg/kg 12 0.72 826GB 06/07/07 1929 erussell 024080
BRL pg/kg 12 0.40 826GB 06/07/07 1929 erussell 024080
BRL pg/kg 6.0 0.36 826GB 06/07/07 1929 erussell 024080
BRL pg/kg 6.0 0.47 826GB 06/07/07 1929 erussell 024080
BRL pg/kg 60 0.42 826GB 06/07/07 1929 erussell Q2408o
BRL pg/kg 12 0.51 826GB 06/07/07 1929 erussefl 024080
BRL pg/kg 6.0 0.46 82608 06/07/07 1929 erussefl Q24080
BRL pg/kg 12 0.43 826GB 06/07/07 1929 erussell 024080
BRL pg/kg 6.0 0.27 826GB 06/G7I07 1929 erusseH Q24G50
BRL pg/kg 6.0 0.40 82608 06/07/07 1929 erussell Q24080
BRL pg/kg 6.0 0.46 826GB 06/07/07 1929 erussell 024080
BRL pg/kg 12 1.4 826GB 06/07/07 1929 erussoll 024080
BRL pg/kg 6.0 0.43 8260B 06/07/07 1929 erussefl 024080
BRL pg/kg 18 0.77 826GB 06/07/07 1929 erusseU 024080
BRL pg/kg 6.0 0.21 826GB 06/07/07 1929 erussell Q24G8G
BRL pg/kg 12 0.49 826GB 06/07/07 1929 erussell Q24G8G
7.3 pg/kg 12 0.87 826GB 06/07/07 1929 erussell Q24G8G
BRL pg/kg 24 1.7 82608 06/07/07 1929 erussell 024080
BRL pg/kg 6.0 0.36 826GB 06/07/07 1929 erussell 024080
Page of 42
ESP Associates PA
\ttn Chris Ward
Box 7030
charlotte NC 28241
Laboratory Report
06/20/07
AB
183469
G06071 10
06/05/07
06/05/07
One surrogate recovery was outside of the control limits Matrix interference is suspected
2-Dichlorobenzene
3-Dichjorobenzene
4-Dichlorobenzene
Surrogate
Bromofluorobenzene
Dibromofluoromethane
Toluene-d8
40 8270C
30 8270C
29 8270C
36 8270C
Recovery
146
142
103
06/19/07 955 kcampgotto
06/19/07 955 kcampigotto
06/19/07 955 kcampigotto
06/19/07 955 kcampigotto
Q24348
Q24348
Q24348
Q24348
Servico Analytical Environmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter
1200
1610
Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
thY chloride 15 pg/kg 12 0.51 8260B 06/07/07 1929 erusseH Q24080
n-Butylbenzene 22 pg/kg 18 0.49 826GB 06/07/07 1929 erussell Q24080
-Propylbenzene BRL pg/kg 12 0.37 8260B 06/07/07 1929 erussefl Q24080
Naphthalene 1200 pg/kg 300 35 50 826GB 06/08/07 1817 erussell Q24080
-Xylene BRL pg/kg 6.0 0.37 826GB 06/07/07 1929 erussell Q24080
-lsopropyItoluene 70 pg/kg 18 0.51 8260B 06/07/07 1929 erussell Q24080
ec-ButyIbenzene BRL pg/kg 18 0.41 8260B 06/07/07 1929 erussell Q24G80
tyrene BRL pg/kg 6.0 0.62 8260B 06/07/07 1929 erussell Q24080
tert-Butylbenzene 9.1 pg/kg 24 0.38 82603 06/07/07 1929 erussell Q24080
Łtrachloroethene BRL pg/kg 12 1.1 8260B 06/07/07 1929 erussell Q24080
Toluene BRL pg/kg 6.0 0.42 826GB 06/07/07 1929 erussell Q2408G
ans-12-Dichloroethene BRL pg/kg 6.0 0.47 8260B 06/07/07 1929 erussell Q24G80
trans-I 3-Dichloropropene BRL pg/kg 6.0 0.43 826GB 06/07/07 1929 erussell Q24080
richloroethene BRL pg/kg 6.0 0.37 826GB 06/07/07 1929 erussell Q2408G
richlorofluoromethane BRL pg/kg 6.0 0.51 826GB 06/07/07 1929 erussell Q24080
inyl chloride BRL pg/kg 12 0.79 82606 06/07/07 1929 erusselt Q24080
ei-volatile Organic ComDounds by GCMS
24-Trichlorobenzene
Control Limits
77-128
67-143
81 -128
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
BRL pg/kg 400
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone] Page 10 of42
Laboratory Report
06/20/07
Project ID Morehead Commons No Client Sample ID AB
Prism Sample ID 183469
Sample Matrix Soil COC Group G06071 10
Time Collected 06/05/07 1200
Time Submitted 06/05/07 1610
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRI
960
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRI
BRL
BRL
BRL
BRL
1100
620
760
260
560
Limit
pg/kg 400 41
pg/kg 400 38
pg/kg 400 34
pg/kg 400 39
pg/kg 400 45
pg/kg 400 23
pg/kg 400 43
pg/kg 400 41
pg/kg 400 32
pg/kg 400 32
pg/kg 400 38
pg/kg 400 48
pg/kg 400 41
pg/kg 400 25
pg/kg 400 24
pg/kg 400 38
pg/kg 400 29
pg/kg 400 25
pg/kg 400 27
pg/kg 400 39
pg/kg 400 40
pg/kg 400 30
pg/kg 400 56
pg/kg 400 46
pg/kg 400 18
pg/kg 400 19
pg/kg 400 33
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
Analysis Analyst
Batch
Date/Time ID
06/19/07 955 kcampigotto 024348
06/19/07 955 kcampigotto Q24348
06/19/07 955 kcampigotto Q24348
06/19/07 955 kcampigotto Q24348
06/19/07 955 kcampigotto 024348
06/19/07 955 kcampigotto Q24348
06/19/07 955 kcampigotto 024348
06/19/07 955 kcampigotto 024348
06/19/07 955 kcampigotto 024348
06/19/07 955 kcampigotto 024348
06/19/07 955 kcampigotto 024348
06/19/07 955 kcampgotto 024348
06/19/07 955 kcampigotto 024348
06/19/07 955 kcampigotto 024348
06/19/07 955 kcampigotto Q24348
06/19/07 955 kcampigotto 024348
06/19/07 955 kcampigotto 024348
06/19/07 955 kcampigotto 024343
06/19/07 955 kcampigotto 024348
06/19/07 955 kcampigotto 024348
06/19/07 955 kcampigotto 024348
06/19/07 955 kcampigotto Q24348
06/19/07 955 kcampigotto 024348
06/19/07 955 kcampigotto 024348
06/19/07 955 kcampigotto Q24348
06/19/07 955 kcampigotto 024348
06/19/07 955 kcampigotto Q24348
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
II Service Analytical Environmeni
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
SP Associates PA
ttn Chris Ward
Box 7030
harlotte NC 28241
arameter Result Units Report MDL Dilution Method
Factor
45-Trichlorophenol
246-Trichlorophenol
4.Dichlorophenol
24-Dimethylphenol
4-Dinitrophenol
4-Dinitrotoluene
6-Dinitrotoluene
-Chloronaphthalene
2-Chlorophenol
-Methylnaphthalene
2-Methylphenol
-Nitrophenol
34-Methylphenol
3-Dichlorobenzidine
6Dinitro.2methyIphenol
-Bromophenylphenylether
-Chloro-3-methylphenol
4-Chlorophenylphenylether
-Nitrophenol
Acenaphthene
cenaphthylene
Anthracene
ienzoaanthracene
enzoapyrene
enzobfluoranthene
Jenzoghiperylene
Benzokfluoranthene
Page 11 of42
Laboratory Report
06/20/07
Project ID Morehead Commons No Client Sample ID AB
Prism Sample ID 183469
Sample Matrix Soil COG Group G06071 10
Time Collected 06/05/07 1200
Time Submitted 06/05/07 1610
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
ttri Chris Ward
P.O Box 7030
Oharlotte NC 28241
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
3is2-chloroethoxymethane BRL pg/kg 400 46 8270C 06/19/07 955 kcampigotto Q24348
Bis2-chloroethylether BRL pg/kg 400 44 8270C 06/19/07 955 kcampigotto Q24348
3is2-chloroisopropylether BRL pg/kg 400 34 8270C 06/19/07 955 kcampigotto 024348
Bis2-ethylhexylphthalate BRL pg/kg 400 20 8270C 06/19/07 955 kcampigotto 024348
utyIbenzylphthalate BRL pg/kg 400 25 8270C 06/19/07 955 kcampigotto Q24348
Chrysene 1100 pg/kg 400 67 8270C 06/19/07 955 kcampigotto 024348
i-n-butylphthalate BRL pg/kg 400 18 8270C 06/19/07 955 kcarnpigotto Q24348
i-n-octylphthalate BRL pg/kg 400 30 8270C 06/19/07 955 kcampigotto 024348
Dibenzoahanthracene 160 pg/kg 400 40 8270C 06/19/07 955 kcampigotto Q24348
ibenzofuran BRL pg/kg 400 34 8270C 06/19/07 955 kcampigotto 024348
Diethylphthalate BRL pg/kg 400 25 8270C 06/19/07 955 kcampigotto Q24348
imethylphthalate BRL pg/kg 400 27 8270C 06/19/07 955 kcampigotto 024348
Fluoranthene 1900 pg/kg 400 28 8270C 06/19/07 955 kcampigotto Q24348
luorene BRL pg/kg 400 24 8270C 06/19/07 955 kcampigotto Q24348
r1exachIorobenzene BRL pg/kg 400 21 8270C 06/19/07 955 kcampigotto 024348
iexachlorobutadiene BRL pg/kg 400 39 8270C 06/19/07 955 kcampigotto Q24348
lexachlorocyclopentadiene BRL pg/kg 400 43 6270C 06/19/07 955 kcampigotto Q24348
Hexachloroethane BRL pg/kg 400 41 8270C 06/19/07 955 kcampigotto 024348
rideno123-cdpyrene 500 pg/kg 400 41 8270C 06/19/07 955 kcampigotto 024348
Isophorone BRL pg/kg 400 36 8270C 06/19/07 955 kcampigotto Q24348
J-Nitrosodi-n-propylamine BRL pg/kg 400 46 8270C 06/19/07 955 kcampigotto 024348
N-Nitrosodiphenylamine BRL pg/kg 400 20 8270C 06/19/07 955 kcampigotto Q24348
aphthaIene BRL pg/kg 400 44 8270C 06/19/07 955 kcampigotto 024348
rJitrobenzene BRL pg/kg 400 39 8270C 06/19/07 955 kcampigotto Q24348
entachlorophenol BRL pg/kg 400 34 8270C 06/19/07 955 kcampigotto 024348
Thenanthrene 1900 pg/kg 400 20 8270C 06/19/07 955 kcampigotto Q24348
Phenol BRL pg/kg 400 44 8270C 06/19/07 955 kcampigotto 024345
Page 12 of42
.SP Associates PA
ttn Chris Ward
Box 7030
harloffe NC 28241
Laboratory Report
06/20/07
AB
183469
G06071 10
06/05/07
06/05/07
iarameter Result Units Report MDL Dilution
Limit Factor
yrene 1300 pg/kg 400 27 8270C 06/19/07 955 kcampigotto Q24348
One surrogate recovery
was outside of the control limits Matrix interference is suspected
Sample Preparation
DRO by GC-FID
Diesel Range Organics DRO 2000
Sample Preparation
asoline Ranee Orpanics GRO by GC-FID
Sasoline Range Organics CR0 1.9
TCLP Leachable Mercury by CVAA
BRL mg/L 0.010 0.000042 7470A 06/08/07 1626 jhoppel Q24140
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Sprinybrook Road P.O Box 240543 Charlotte NC 28224-0543
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1200
1610
Method Analysis
Date/Time
Analyst Batch
ID
29.68 mL 3550B 06/15/07 900 dpope P18642
mg/kg 84 11
25.lg
mg/kg 1.2 0.077
Surrogate Recovery Control Limits
Nitrobenzene-d5 101 14-103
Phenol-d5 82 13-95
246-Tribromophenol 85 25 123
Terphenyl-d14 87 41 136
2-Fluorobiphenyl 95 21 108
2-Fluorophenol 90 14-89
10 80159 06/07/07 2221 jvogel Q24180
mL 3545 06/07/07 910 wconder P18568
Surrogate Recovery Control Limits
o-Terphenyl DO 49-124
8015B 06/08/07 026 hwagner Q24121
Surrogate Recovery Control Limits
aaa-TFT 109 55 129
CLP Extraction for Metals
TCLP Extraction Complete 1311 06/06/07 1345 jhoppel
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 13 of 42
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
uS Service Analytical Environmental Solutions
tESP Associates PA Project ID
ttn Chris Ward
Box 7030
Oharlotte NC 28241
Morehead Commons No Client Sample ID
Prism Sample ID
COG Group
Time Collected
Time Submitted
AB
183469
G06071 10
06/05/07 1200
06/05/07 1610
ampie Comments
ARL Below Reporting Limit
Estimated value between the Reporting Umit and the MDL
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanJELACcertificationexceptforthose instances indicated in the case narrative and/or test comments
All results are reported on dry-weight basis
ngela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Laboratory Report
06/20/07
Sample Matrix Soil
Farameter Result Units Report MDL
Limit
Sample Preparation
CLp Leachable Metals by ICP
rsenic
Dilution Method Analysis Analyst Batch
Factor Date/Time ID
2OmL 3OmL 7470A 06/08/07 715 jhoppel P18573
BRL mg/L 0.050 0.0029 6010B 06/11/07 1548 mcampbell 024175
Barium 0.78J mg/L 5.0 0.0019 6010B 06111/07 1548 mcampbell 024175
admium BRL mg/L 0.025 0.00034 6010B 06/11/07 1548 mcampbell Q24175
Chromium o.ooaoj mg/L 0.25 0.0006 6010B 06/11/07 1548 mcampbell Q24175
ead 0.018J mg/L 0.050 0.0021 6010B 06/11/07 1548 mcampbell 024175
3elenium 0.0068 mg/L 0.050 0.0035 6010B 06/11/07 1548 mcampbefl 024175
liver BRL mg/L 0.25 0.00025 6010B 06/11/07 1548 mcampbell 024175
Sample Preparation
otal Halogen by Method 9076
ubcontract Report
Analysis Note for
5OmL 5OmL
See
Attached
3010A 06/11/07 900 jhoppei
9076
Subcontract Report Analysis subcontracted to
P1 8570
NC certified lab 618
Page 14 of42
Project ID Morehead Commons No Client Sample ID AB
Prism Sample ID 183470
Sample Matrix Soil COC Group G06071 10
Time Collected 06/05/07 1305
Time Submitted 06/05/07 1610
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
ttn Chris Ward
Box 7030
charlotte NC 28241
Laboratory Report
06/20/07
87.1 SM2540 06/11/07 1700 brown
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
ercent Solids Determination
-percent Solids
latiIe Organic Corn Dounds by GC/MS
111 2-Tetrachloroethane BRL pg/kg 5.7 0.70 826GB 06/07/07 2011 erussell 024080
1-Trichloroethane BRL pg/kg 5.7 0.40 826GB 06/07/07 2011 erussell Q24080
i122-Tetrachloroethane BRL pg/kg 5.7 0.73 826GB 06/07/07 2011 erussell Q24080
11 2-Trichloroethane BRL pg/kg 5.7 0.44 826GB 06/07/07 2011 erussell Q24080
1-Dichloroethane BRL pg/kg 5.7 0.52 826GB 06/07/07 2011 erussell Q24080
11-Dichloroethene BRL pg/kg 5.7 0.54 826GB 06/07/07 2011 erussell 024080
1-Dichloropropene BRL pg/kg 5.7 0.63 826GB 06/07/07 2011 erussell 024080
23-Trichlorobenzene BRL pg/kg 11 0.79 826GB 06/07/07 2011 erussell 024080
23-Trichloropropane BRL pg/kg 5.7 0.63 826GB 06/07/07 2011 erussell 024080
24-Trichlorobenzene BRL pg/kg 11 0.69 826GB 06/07/07 2011 erussell Q24080
24-Trimethylbenzene 110 pg/kg 11 0.54 826GB 06/07/07 2011 erussell Q24080
2-Dibromo-3-chloropropane BRL pg/kg 5.7 1.1 826GB 06/07/07 2011 erussel 024080
2-DibromoethaneEDB BRL pg/kg 5.7 G.13 826GB 06/07/07 2011 erussell 024080
2-Dichlorobenzene BRL pg/kg 11 0.39 826GB 06/07/07 2011 erussell Q24080
2-Dichloroethane BRL pg/kg 5.7 0.72 826GB 06/07/07 2011 erusseH 024080
2-Dichloropropane BRL pg/kg 5.7 0.53 826GB 06/07/07 2011 erussefl 024080
35-Trimethylbenzene 69 pg/kg 11 G.6G 826GB 06/07/07 2011 erussell 024080
3-Dichlorobenzene BRL pg/kg 11 0.62 826GB 06/07/07 2011 erussell 024080
3-Dichloropropane BRL pg/kg 5.7 0.49 826GB 06/07/07 2011 erussell 024080
4-Dichlorobenzene BRL pg/kg 11 G.56 826GB 06/07/07 2011 erussell Q2408G
.2-DichIoropropane BRL pg/kg 5.7 0.36 8260B 06/07/07 2011 erussell 024080
-Chloroethyl vinyl ether BRL pg/kg 11 0.53 826GB 06/07/07 2011 erussell 024080
-ChIorotoluene BRL pg/kg 11 0.53 826GB 06/07/07 2011 erussell 024080
2-Hexanone BRE pg/kg 57 0.74 826DB 06/07/07 2011 erussell Q24G8G
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 15 of42
Sorvice Analytical Environmental Solutions
ESP Associates PA
ttn Chris Ward
Box 7030
Qharlotte NC 28241
Laboratory Report
06/20/07
AB
183470
G0607110
06/05/07
06/05/07
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1305
1610
2arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
-Chlorotoluene BRL pg/kg 11 0.37 8260B 06/07/07 2011 erussell Q24G80
4-Methyl-2-pentanone MIBK BRI pg/kg 11 072 826GB 06/07/07 2011 erussell Q24080
cetone BRI pg/kg 23 2.8 826GB 06/07/07 2011 erussell Q24080
Benzene BRI pg/kg 3.4 0.57 826GB 06/07/07 2011 erusseH Q24080
romobenzene BRL pg/kg 5.7 0.50 826GB 06/07/07 2011 erussell Q24080
Jromochloromethane BRL pg/kg 5.7 0.43 826GB 06/07/07 2011 erussell Q24080
Bromodichloromethane BRL pg/kg 5.7 0.63 826GB 06/07/07 2011 erusseil Q24080
romoform BRL pg/kg 5.7 0.53 8260B 06/07/07 2011 erussell Q24080
Brornomethane BRL pg/kg 11 0.83 8260B 06/07/07 2011 erusselt Q24080
arbon disulfide BRL pg/kg 11 0.46 826GB 06/07/07 2011 erussell 024080
Carbon tetrachloride BRL pg/kg 5.7 0.42 826GB 06/07/07 2011 erussell 024080
hlorobenzene BRL pg/kg 5.7 0.54 826GB 06/07/07 2011 erussefi Q24080
Chlorodibromomethane BRL pg/kg 5.7 0.49 826GB 06/07/07 2011 erussell 024080
hloroethane BRL pg/kg 11 0.59 8260B 06/07/07 2011 erussell Q24080
hIoroform BRI pg/kg 5.7 0.53 826GB 06/07/07 2011 erussell Q24080
Chioromethane BRL pg/kg 11 0.50 826GB 06/07/07 2011 erussell Q24080
is-I 2-Dichloroethene BRL pg/kg 5.7 0.31 826GB 06/07/07 2011 erussell Q24080
cis-1 3-Dichloropropene BRL pg/kg 5.7 0.46 826GB 06/07/07 2011 erussell Q24080
ibromomethane BRL pg/kg 5.7 0.53 826GB 06/07/07 2011 erussell 024080
Dichlorodifluoromethane BRL pg/kg 11 1.6 826GB 06/07/07 2011 erussefl Q24080
thylbenzene BRL pg/kg 5.7 0.50 826GB 06/07/07 2011 erussell 024080
iiexachIorobutadiene BRL pg/kg 17 0.89 826GB 06/07/07 2011 erussell Q24080
opropyI ether IPE BRL pg/kg 5.7 0.24 826GB 06/07/07 2011 erussell 024080
opropylbenzene BRL pg/kg 11 0.57 826GB 06/07/07 2011 erussell Q24080
mp-Xylenes BRL pg/kg 11 1.0 826GB 06/07/07 2011 erussell 024080
lethyl ethyl ketone MEK BRL pg/kg 23 2.0 826GB 06/07/07 2011 erussell Q24G80
Methyl t-butyl ether MTBE BRL pg/kg 5.7 0.42 826GB 06/07/07 2011 erussell Q24080
Page 16 of 42
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Analysis
Date/Time
06/07/07 2011
06/07/07 2011
06/07107 2011
06107/07 2011
06/07/07 2011
06/07/07 2011
06/07/07 2011
06/07/07 2011
06/07/07 2011
06/07/07 2011
06/07/07 2011
06/07/07 2011
06/07/07 2011
06/07/07 2011
06/07/07 2011
06/07/07 2011
Analyst Batch
ID
erussell Q24080
ewssell Q24G80
erussell 024080
erussell 024080
erussell 024080
erussell Q24080
erussell Q24080
erussefi 024080
erusseH 024080
erussell Q24G80
erussetl 024080
erusseli Q24080
erussell 024080
erussell 024080
erussell 024080
erussell 024080
37 8270C
28 8270C
27 8270C
34 8270C
06/18/07 2033 kcampigotto
06/18/07 2033 kcampigotto
06/18/07 2033 kcampigotto
06/18/07 2033 kcampigotto
Q24348
024348
024348
024348
ESP Associates PA
ttn Chris Ward
_1b Box 7030
Charlotte NC 28241
Laboratory Report
06/20/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
arameter
AB
183470
G06071 10
06/05/07 1305
06/05/07 1610
Result Units Report MDL Dilution Method
Limit Factor
.4ethylene chloride 17 pg/kg 11 0.59 826GB
n-Butylbenzene BRL pg/kg 17 0.57 826GB
i-Propylbenzene BRL pg/kg 11 0.43 826GB
JaphthaIene 83 pg/kg 5.7 0.83 826GB
-Xylene BRL pg/kg 5.7 0.43 826GB
p-lsopropyltoluene 58 pg/kg 17 0.59 82608
cutythenz 3.4 pg/kg 17 0.47 826GB
3tyrene BRL pg/kg 5.7 0.72 826GB
tert-Butylbenzene 8.2 pg/kg 23 0.44 826GB
letrachloroethene 5.8 pg/kg 11 1.2 826GB
Toluene BRL pg/kg 5.7 0.49 826GB
rars-12-Dichloroethene BRL pg/kg 5.7 0.54 8260B
irans-13-Dichloropropene BRL pg/kg 5.7 0.50 826GB
Trichloroethene BRL pg/kg 5.7 0.43 82606
Irichlorofluoromethane BRL pg/kg 5.7 0.59 826GB
Vinyl chloride BRL pg/kg 11 0.92 82608
Two surrogate recoveries were outside of the control limits Matrix interference is suspected
lemi-volatile Organic Compounds by GC/MS
124-Trichloroberizene BRL
2-Dichlorobenzene BRL
3-Dichlorobenzene BRL
4-Dichlorobenzene BRL
Surrogate Recovery Control Limits
Bromofluorobenzene 134 77 128
Dibromofluoromethane 144 67-143
Toluene-d8 107 81 128
pg/kg
pg/kg
pg/kg
pg/kg
380
380
380
380
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone] Page 17 of42
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Service Analytical Environmental Solutions
ESP Associates PA Project ID
ttn Chris Ward
Box 7030
charlotte NC 28241
Laboratory Report
06/20/07
Morehead Commons No Client Sample ID AB
Prism Sample ID 183470
COC Group G0607110
Time Collected 06/05/07
Time Submitted 06/05/07
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Sample Matrix Soil
.arameter Result Units Report MDL Dilution Method
1305
1610
Analyst Batch
ID
Analysis
Limit Factor Date/Time
45-Trichlorophenol BRL pg/kg 380 39 8270C 06/18/07 2033 kcampigotto 024348
246-Trichloropheriol BRL pg/kg 380 36 8270C 06/18/07 2033 kcampigotto 024348
4-Dichlorophenol BRL pg/kg 380 32 8270C 06/18/07 2033 kcampigotto Q24348
24-Dimethylphenol BRL pg/kg 380 36 8270C 06/18/07 2033 kcampigotto 024348
4-Dinitrophenol BRL pg/kg 380 42 8270C 06/18/07 2033 kcampigotto 024348
4-Dinitrotoluene BRL pg/kg 380 21 8270C 06/18/07 2033 kcampigotto Q24348
26-Dinitrotoluene BRI pg/kg 380 40 8270C 06/18/07 2033 kcampigotto Q24348
-Chloronaphthalene BRL pg/kg 380 39 8270C 06/18/07 2033 kcampigotto Q24348
2-Chiorophenol BRL pg/kg 380 30 8270C 06/18/07 2033 kcampigotto Q24348
Methylnaphthalene BRL pg/kg 380 30 8270C 06/18/07 2033 kcampigotto 024348
2-Methyiphenol BRL pg/kg 380 35 8270C 06/18/07 2033 kcampigotto 024348
-Nitrophenol BRL pg/kg 380 45 8270C 06/18/07 2033 kcampigotto Q24348
i4-Methylphenol BRI pg/kg 380 39 8270C 06/18/07 2033 kcampigotto Q24348
3-Dichlorobenzidjne BRL pg/kg 380 24 8270C 06/18/07 2033 kcampigotto 024348
6-Dinitro-2-methylphenol BRL pg/kg 380 23 8270C 06/18/07 2033 kcampigotto Q24348
4-Bromophenyiphenylether BRL pg/kg 380 36 8270C 06/18/07 2033 kcampigotto Q24348
-Chloro-3-methylphenol BRL pg/kg 380 28 8270C 06/18/07 2033 koampigotto 024348
4-Chiorophenyiphenylether BRL pg/kg 380 23 8270C 06118/07 2033 kcampigotto 024348
-Nitrophenol BRL pg/kg 380 25 8270C 06/18/07 2033 kcampigotto Q24348
Acenaphthene BRL pg/kg 380 37 8270C 06/18/07 2033 kcampigotto 024348
cenaphthylene BRL pg/kg 380 38 8270C 06/18/07 2033 kcampigotto Q24348
iinthracene BRL pg/kg 380 29 8270C 06/18/07 2033 kcampigotto 024348
Thnzoaanthracerie 130 pg/kg 380 53 8270C 06/18/07 2033 kcampigotto 024348
enzoapyrene 100 pg/kg 380 44 8270C 06/18/07 2033 kcampigotto Q24348
Benzobfluoranthene BRL pg/kg 380 17 8270C 06/18/07 2033 kcanipigotto Q24348
enzoghiperylene BRL pg/kg 380 18 8270C 06/18/07 2033 kcampigotto Q24348
Benzokfluoranthene BRL pg/kg 380 31 8270C 06/18/07 2033 kcampigotto 024348
Page 18 of42
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06120107
Project ID Morehead Commons No Client Sample ID AB
Prism Sample ID 183470
Sample Matrix Soil COC Group G0607110
Time Collected 06/05/07 1305
Time Submitted 06/05/07 1610
ut Service Analytical Environmental Solutions
ESP Associates PA
\ttn Chris Ward
Box 7030
Charlotte NC 28241
ara meter
3is2-chloroethoxymethane
Bis2-chloroethylether
3is2-chloroisopropylether
3is2-ethylhexylphthalate
9ulylbenzylphthalate
Thrysene
Di-n-butylphthaate
i-n-octylphthalate
Dibenzoahanthracene
ibenzofuran
Diethylphthalate
methylphthaiate
.luoranthene
luorene
lexachlorobenzene
Hexachiorobutadjene
lexachiorocyclopentadiene
Hexachioroetharie
ideno1 23cdpyrene
Isophororie
l-Nitrosodi-n-propylamine
J-NitrosodiphenyIamine
aphthalene
itrobenzene
Pentachlorophenol
henanthrene
Phenol
Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
BRL pg/kg 380 43 8270C 06/18/07 2033 kcampigotto Q24348
BRL pg/kg 380 41 8270C 06/18/07 2033 kcampigotto Q24348
BRL pg/kg 380 32 8270C 06/18107 2033 kcampigotto 024348
BRL pg/kg 380 19 8270C 06/18/07 2033 kcampgotto Q24348
BRL pg/kg 380 23 8270C 06/18/07 2033 kcampigotto Q24348
130 pg/kg 380 63 8270C 06/18/07 2033 kcampigotto Q24348
BRL pg/kg 380 17 8270C 06/18/07 2033 kcampigotto Q24348
BRL pg/kg 380 28 8270C 06118/07 2033 kcampigotto Q24348
BRL pg/kg 380 38 8270C 06/18/07 2033 kcampigotto 024348
BRL pg/kg 380 32 8270C 06/18/07 2033 kcampigotto Q24348
BRL pg/kg 380 23 8270C 06/18/07 2033 kcampigotto 024348
BRL pg/kg 380 26 8270C 06/18/07 2033 kcampigotto 024348
310 pg/kg 380 26 8270C 06/18/07 2033 kcampigotto Q24348
BRL pg/kg 380 22 8270C 06/18/07 2033 kcampigotto Q24348
BRL pg/kg 380 20 8270C 06/18/07 2033 kcampgollo 024348
BRL pg/kg 380 37 8270C 06/18/07 2033 kcampigotto Q24348
BRL pg/kg 380 40 8270C 06/18/07 2033 kcampigotto Q24348
BRL pg/kg 380 38 8270C 06/18/07 2033 kcampigotto 024348
BRL pg/kg 380 39 8270C 06/18/07 2033 kcampigotto Q24348
BRL pg/kg 380 34 8270C 06/18/07 2033 kcampigotto 024348
BRL pg/kg 380 43 8270C 06/18/07 2033 kcampigotto 024348
BRL pg/kg 380 19 8270C 06/18/07 2033 kcampigotto 024348
BRL pg/kg 380 41 8270C 06118/07 2033 kcampigotto 024348
BRL pg/kg 380 37 8270C 06/18/07 2033 kcampigotto 024348
BRL pg/kg 380 32 8270C 06/18/07 2033 kcampigofto 024348
100 pg/kg 380 18 8270C 06/18/07 2033 kcampjgotto 024348
BRL pg/kg 380 41 8270C 06/18/07 2033 kcampigofto 024348
Page 19 of 42
iull Service Analytical Environmental Solutions
ESP Associates PA
ttn Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/20/07
AB
183470
G0607I10
06/05/07
06/05/07
arameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
yrene 310 rig/kg 380 26 8270C 06/18/07 2033 kcampigotto 024348
Sample Preparation 30.09 mL 3550B 06/15/07 900 dpope P18642
Diesel Range Organics DRO by GC-FID
iesel Range Organics DRO 1400
asoline Range Organics GRO by GC-FID
Gasoline Range Organics GRO 2.2 mg/kg 1.1 0.073 8015B 06/08/07 058 hwagner 024121
One surrogate recovery was outside of the control limits Matrix interference is suspected
Surrogate Recovery Control Limits
aaa-TFT 149
CLP Extraction for Metals
TCLP Extraction Complete 1311 06/06/07 1345 jhoppel
CLP Leachable Mercury by CVAA
BRL mg/L 0.010 0.000042 7470A 06/08/07 1630 jhoppel 024140
This report should not be reproduced except in its entirety thout the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1305
1610
Sample Preparation
Surrogate Recovery Control Limits
246-Tribromophenol 110 25-123
2-Fluorobiphenyl 102 21 108
2-Fluorophenol 76 14-89
Nitrobenzene-d5 103 14-103
Phenol-d5 77 13 95
Terphenyl-d14 118 41-136
20 8015B 06/08/07 1353 jvogel 024180
mL 3545 06/07/07 910 wconder P18568
Surrogate Recovery Control Limits
mg/kg 160 20
25.28
o-Terphenyl DO 49-124
Mercury
55-129
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 20 of 42
Full Service Analytical Environmental Solutions
ESP Associates PA
Attn Chris Ward
P.O Box 7030
Charlotte NC 28241
Laboratory Report
06/20/07
AB
183470
G0607110
06/05/07
06/05/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Sample Preparation 20 mL 30 mL 7470A 06/08107 715 jhoppel P18573
TCLP Leachable Metals by ICP
Arsenic BRL mgIL 0.050 0.0029 6010B 06/11/07 1554 mcampbeii 024175
Barium 0.89 mgIL 5.0 0.0019 6010B 06/11/07 1554 mcampbeH 024175
Cadmium BRL mg/L 0.025 0.00034 6010B 06/11/07 1554 mcampbeii 024175
Chromium 0.0046 mg/L 0.25 0.0006 6010B 06/11/07 1554 mcampbeii 024175
Lead 0.013J mg/L 0.050 0.0021 6010B 06/11/07 1554 mcampbeil 024175
Selenium 0.0048 mgIL 0.050 0.0035 6010B 06/11/07 1554 mcampbefl Q24175
Silver BRL mg/L 0.25 0.00025 6010B 06/11/07 1554 mcampbeit 024175
Sample Preparation 50 mL 50 mL 3010A 06/11/07 900 Jhoppel P18570
1otal Halogen by Method 9076
Subcontract Report See 9076
Attached
Analysis Note for Subcontract Report Analysis subcontracted to NC certified lab 618
Sample Comments
3RL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
Jhe results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanIELACcertificationexceptforthose instances indicated in the case narrative and/or test comments
All results are reported on dry-weight basis
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 282240543
Phone 704I529-6364 Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
ii 305
IF 610
ngela Overcash V.P Laboratory Services
Page 21 of 42
oil Service Analytical Environmental Solutions
ESP Associates PA
t1n Chris Ward
Box 7030
Charlotte NC 28241
rcent Solids Determination
dercent Solids
fjatile Organic Compounds by GC/MS
11 2-Tetrachloroethane
1-Trichloroethane
22-Tetrachloroethane
2-Trichloroethane
1-Dichloroethane
11Dichloroethene
1Dichloropropene
23-Trichlorobenzene
23-Trichloropropane
24-Trichlorobenzene
24-Tiimethylbenzene
i2-Dibromo-3-chloropropane
12Dibromoethane EDB
2-Dichlorobenzene
2Dichloroethane
2Dichloropropane
35-Trimethylbenzene
3-Dichlorobenzene
3-Dichloropropane
4Dichlorobenzene
2Dichloropropane
-Chloroethyl vinyl ether
i-Chlorotoluene
2-Hexanone
Result Units Report MDL Dilution Method Analysis
Date/Time
Analyst Batch
ID
06/07/07 2054 erussell
06/07/07 2054 erussell
06/07/07 2054 erussell
06/07/07 2054 erussell
06/07/07 2054 erussell
024080
024080
024080
Q2408G
024080
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/20/07
arameter
Project ID Morehead Commons No Client Sample ID AB
Prism Sample ID 183471
Sample Matrix Soil COC Group G06071 10
Time Collected 06/05/07 1115
Time Submitted 06/05/07 1610
Limit Factor
SM2540 06/11/07 1700 brown88.4
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
99
BRL
BRL
BRL
BRL
BRL
47
BRL
BRL
BRI
BRL
BRL
BRL
BRL
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
06/07/07 2054
06/07/07 2054
06/07/07 2054
06/07/07 2054
06/07/07 2054
06/07/07 2054
06/07/07 2054
06/07/07 2054
06/07/07 2054
06/07/07 2054
06/07/07 2054
06/07/07 2054
06/07/07 2054
06/07/07 2054
06/07/07 2054
06/07/07 2054
06/07/07 2054
06/07/07 2054
06/07/07 2054
5.7 0.54
5.7 0.31
5.7 0.56
5.7 0.34
5.7 0.39
5.7 0.42
5.7 0.48
11 0.60
5.7 0.48
11 0.53
11 0.42
5.7 0.87
5.7 0.099
11 0.30
5.7 0.55
5.7 0.41
11 0.46
11 0.47
5.7 0.37
11 0.43
5.7 0.27
11 0.41
11 0.41
57 0.57
erusseD
erusseil
erussell
erussell
erusseI
erussell
erussell
enissell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
erussell
024080
024080
Q24080
024080
024080
024080
Q24080
024080
024080
024080
024080
024080
024080
024080
024080
024080
024080
024080
024080
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
826GB
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 22 of 42
4IP3IIII1 NC Certification No 402iiSCCertificationNo99012
NC Drinking Water Cert No 37735
utt Service Anatytical Environmental Solutions
ESP Associates PA
Mtn Chris Ward
Box 7030
Charlotte NC 28241
2arameter
-ChIorotoluene
4-Methyl-2-pentanone MIBK
cetone
i3enzene
-3romobenzene
3romochloromethane
BromodichIoromethane
3romoform
Bromomethane
arbon disulfide
Carbon tetrachioride
hlorobenzene
shIorodibromomethane
hloroethane
Thloroform
Chioromethane
is-I 2-Dichloroethene
cis-1 3-Dichloropropene
ibromomethane
Dichlorodifluoromethane
thylbenzene
i-iexachlorobutadiene
opropyI ether IPE
5opropylbenzene
mp-Xylenes
lethyl ethyl ketone MEK
Methyl t-butyl ether MTBE
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 282240543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Laboratory Report
06/20/07
Project ID Morehead Commons No Client Sample ID AB
Prism Sample ID 183471
Sample Matrix Soil COC Group G06071 10
Time Collected 06/05/07 1115
Time Submitted 06/05/07 1610
Result Units Report MDL Dilution
Limit
Method
Factor
Analysis Analyst
Batch
Date/Time ID
BRL pg/kg 11 0.28 8260B 06/07/07 2054 erussell Q24080
BRL pg/kg 11 0.55 8260B 06/07/07 2054 erussell Q24080
BRL pg/kg 23 2.1 8260B 06/07/07 2054 erussell Q24080
BRL pg/kg 3.4 0.44 8260B 06/07/07 2054 erussell Q24080
BRL pg/kg 5.7 0.38 8260B 06/07/07 2054 erussell Q24080
BRL pg/kg 5.7 0.33 826DB 06/07/07 2054 erussell Q24080
BRL pg/kg 5.7 0.48 826DB 06/07/07 2054 erussefl Q24080
BRL pg/kg 5.7 0.41 8260B 06/07/07 2054 erussefl Q24080
BRL pg/kg 11 0.64 8260B 06/07/07 2054 erussell Q24080
BRL pg/kg 11 0.35 8260B 06/07/07 2054 erusseD Q24080
BRL pg/kg 5.7 0.32 826DB 06/07/07 2054 erussell Q24080
BRL pg/kg 5.7 0.42 826DB 06/07/07 2054 erussell Q24080
BRL pg/kg 5.7 0.37 8260B 06/07/07 2054 erussell Q24080
BRI pg/kg 11 0.45 8260B 06/07/07 2054 erusseil Q24080
BRL pg/kg 5.7 0.41 826DB 06/07/07 2054 erussefl Q24080
BRL pg/kg 11 0.38 826DB 06/07/07 2054 erussefl Q24080
BRL pg/kg 5.7 0.24 8260B 06/07/07 2054 erussell 024080
BRL pg/kg 5.7 0.35 826DB 06/07/07 2054 erussefi 024080
BRL pg/kg 5.7 0.41 826DB 06/07/07 2054 erusseil Q24080
BRL pg/kg 11 1.2 826DB 06/07/07 2054 erusseli Q24D80
BRL pg/kg 5.7 0.38 826DB 06/07/07 2054 erussell 024080
BRL pg/kg 17 0.68 8260B 06/07/07 2054 erussefl Q24080
BRL pg/kg 5.7 0.19 826DB 06/07/07 2054 erussell 024080
BRI pg/kg 11 0.44 826DB 06/07/07 2054 erussefi Q24080
BRL pg/kg 11 0.77 826DB 06/07/07 2054 erussell 024080
BRL pg/kg 23 1.5 826DB 06/07/07 2054 erussell 024080
BRL pg/kg 5.7 0.32 826DB 06/07/07 2054 erussell 024080
Page 23 of 42
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
uS Service Analytical Environmental Solutions
ESP Associates PA Project ID
\ttiri Chris Ward
Box 7030
Charlotte NC 28241
Laboratory Report
06/20/07
Morehead Commons No Client Sample ID AB
Prism SampJe ID 183471
COC Group G06071 10
Time Collected 06/05/07
Time Submitted 06/05/07
Surrogate
Bromofluorobenzene
Dibromofluoromethane
Toluene-d8
38 8270C
28 8270C
27 8270C
34 8270C
39 8270C
141
106
06/18/07 1944 kcampigouo
06/18/07 1944 kcampigotto
06/18/07 1944 kcampigotto
06/18/07 1944 kcampigotto
06/18/07 1944 kcampigotto
Q24348
Q24348
Q24348
Q24348
024348
Sample Matrix Soil
1115
1610
arameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
1ethylene chloride 15 pg/kg 11 0.45 8260B 06/07/07 2054 erussell 024080
n-Butylbenzene BRL pg/kg 17 0.44 8260B 06/07/07 2054 erussell Q24080
-Propylbenzene BRL pg/kg 11 0.33 826GB 06/07/07 2054 erussell 024080
.iaphthalene 610 pg/kg 280 33 50 826GB 06/08/07 1855 erussell Q2408G
-Xylene BRI pg/kg 5.7 0.33 826GB 06/07/07 2054 erussell 024080
-Isopropyltoluene 32 pg/kg 17 0.45 826GB 06/07/07 2054 erussell Q24080
sec-Butylbenzene 7.0 pg/kg 17 0.36 826GB 06/07/07 2054 erussell Q24G80
tyrene BRL pg/kg 5.7 0.55 826GB 06/07/07 2054 erussell 024080
tert-Butylbenzene 3.9 pg/kg 23 0.34 826GB 06/07/07 2054 erussefl Q24080
etrachioroethene BRL pg/kg 11 0.94 826GB 06/07/07 2054 erussell Q2408o
ioluene BRL pg/kg 5.7 0.37 826GB 06/07/07 2054 erussell Q24080
ans-1 2-Dichloroethene BRL pg/kg 5.7 0.42 8260B 06/07/07 2054 erussell 024080
ans-1 3-Dichloropropene BRL pg/kg 5.7 0.38 826GB 06/07/07 2054 erussell 024080
Trichloroethene BRL pg/kg 5.7 0.33 826GB 06/07/07 2054 erussell 024080
richlorofluoromethane BRL pg/kg 5.7 0.45 826GB 06/07/07 2054 erussell 024080
Vinyl chloride BRL pg/kg 11 0.70 826GB 06/07/07 2054 erussell Q2408G
%Recovery Control Limits
123 77-128
Semi-volatile Organic Compounds by GC/MS
24-TrichIorobenzene BRL pg/kg 380
t2-Dichlorobenzene BRL pg/kg 380
3-Dichlorobenzene BRL pg/kg 380
14-DichlorObenzene BRL pg/kg 380
2.45-Trichiorophenot BRL pg/kg 380
67-143
81 128
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 24 of 42
ull Service Analytical Eriviro
ESP Associates PA
\ttn Chris Ward
1b Box 7030
Charlotte NC 28241
Laboratory Report
06/20107
AB
183471
G0607110
06/05/07 1115
06/05/07 1610
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Tnchlorophenol BRL pg/kg 380 36 8270C 06/18/07 1944 kcampigotto Q24348
24-Dichiorophenol BRL pg/kg 380 32 8270C 06/18/07 1944 kcampigotto Q24348
4-Dimethylphenol BRL pg/kg 380 37 8270C 06/18/07 1944 kcampigotto Q24343
24-linitrophenol BRL pg/kg 380 43 8270C 06/18/07 1944 kcampigotto Q24348
4-DinitrotoIuene BRL pg/kg 380 21 8270C 06/18/07 1944 kcampigotto Q24348
6-DinitrotoIuene BRL pg/kg 380 40 8270C 06/18/07 1944 kcampigotto Q24348
2-Chloronaphthalene BRL pg/kg 380 39 8270C 06/18/07 1944 kcampigotto Q24348
-Chlorophenol BRL pg/kg 380 30 8270C 06/18/07 1944 kcampigotto Q24348
2-Methylnaphthalene 1300 pg/kg 380 30 8270C 06/18/07 1944 kcampigotto 024348
-Methyiphenol BRL pg/kg 380 35 8270C 06/18/07 1944 kcampigotto Q24348
2-Nitrophenol BRL pg/kg 380 45 8270C 06/18/07 1944 kcampigotto Q24348
4-Methylphenol BRL pg/kg 380 39 8270C 06/18/07 1944 kcampigotto Q24348
3-Dichlorobenzidine BRL pg/kg 380 24 8270C 06/18/07 1944 kcampigotto 0243486-BRL pg/kg 380 23 8270C 06/18/07 1944 kcampigotto Q24348
-BroniophenyIphenyIether BRL pg/kg 380 36 8270C 06/18/07 1944 kcampigotto 024348
4-Chloro-3-methylphenol BRI pg/kg 380 28 8270C 06/18/07 1944 kcampigotto 024348
-Chiorophenyiphenylether BRL pg/kg 380 23 8270C 06/18/07 1944 kcampigotto Q24348
4-Nitrophenol BRL pg/kg 380 25 8270C 06/18/07 1944 kcampigotto Q24348
cenaphthene BRL pg/kg 380 37 8270C 06/18/07 1944 kcampigotto 024348
Acenaphthylene BRL pg/kg 380 38 8270C 06/18/07 1944 kcampigotto 024348
nthracene BRL pg/kg 380 29 8270C 06/18/07 1944 kcampigotto 024348
benzoaanthracene BRL pg/kg 380 53 8270C 06/18/07 1944 kcampgotto 024348
enzoapyrene BRL pg/kg 380 44 8270C 06/18/07 1944 kcampigotto Q24348
enzobfluoranthene BRL pg/kg 380 17 8270C 06/18/07 1944 kcampigotto 024348
Benzoghiperylene BRL pg/kg 380 18 8270C 06/18/07 1944 kcampigotto 024348
enzokfluoranthene BRL pg/kg 380 31 8270C 06/18/07 1944 kcampigotto 024348
Bis2-chloroethoxymethane BRL pg/kg 380 44 8270C 06/18/07 1944 kcampigotto 024348
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 282240543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 25 of 42
Laboratory Report
06/20/07
Project ID Morehead Commons No Client Sample ID AB
Prism Sample ID 183471
Sample Matrix Soil COC Group G06071 10
Time Collected 06/05/07 1115
Time Submitted 06/05/07 1610
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
ttn Chris Ward
Box 7030
Charlotte NC 28241
arameter Result Units Report MDL Dilution
Limit
Method
Factor
Analysis Analyst
Batch
Date/Time ID
3is2-chloroethylether BRL pg/kg 380 41 8270C 06118/07 1944 kcampigotto Q24348
Bis2-chloroisopropylether BRL pg/kg 380 32 8270C 06/18/07 1944 kcampigotto Q24348
is2-ethylhexylphthalate BRL pg/kg 380 19 8270C 06/18/07 1944 kcampigotto Q24348
utylbenzylphthalate BRL pg/kg 380 23 8270C 06/18/07 1944 kcampigotto Q24348
hrysene BRL pg/kg 380 63 8270C 06/18/07 1944 kcampigotto Q24348
inbutyIphthalate BRL pg/kg 380 17 8270C 06/18/07 1944 kcampigotto Q24348
Di-n-octylphthalate BRL pg/kg 380 28 8270C 06/18/07 1944 kcampigotto Q24348
ibenzoahanthracerie BRL pg/kg 380 38 8270C 06/18/07 1944 keampigotto Q24348
Dibenzofuran BRL pg/kg 380 32 8270C 06/18/07 1944 kcampigotto Q24348
iethylphthalate BRL pg/kg 380 23 8270C 06/18/07 1944 kcampigotto Q24348
Dimethylphthalate BRL pg/kg 380 26 8270C 06/18/07 1944 kcampigotto Q24348
luoranthene 200 pg/kg 380 26 8270C 06/18/07 1944 kcampigotto 024348
rluorene 440 pg/kg 380 23 8270C 06/18/07 1944 kcampigotto 024348
9exachlorobenzene BRL pg/kg 380 20 8270C 06/18/07 1944 kcampgoUo Q24348
lexachlorobutadiene BRL pg/kg 380 37 8270C 06/18/07 1944 kcampigotto Q24348
Hexachlorocyclopentadiene BRL pg/kg 380 40 8270C 06/18/07 1944 kcampigotto 024348
lexachioroethane BRL pg/kg 380 39 8270C 06/18/07 1944 kcampigotto Q24348
Indeno1 23-cdpyrene BRL pg/kg 380 39 8270C 06/18/07 1944 kcampigotto Q24348
BRL pg/kg 380 34 8270C 06/18/07 1944 kcampigotto Q24348
N-Nitrosodi-n-propylamine BRL pg/kg 380 43 8270C 06/18/07 1944 kcampigotto Q24348
-Nitrosodiphenylamine BRL pg/kg 380 19 8270C 06/18/07 1944 kcampigotto 024348
iaphthaIene 120 pg/kg 380 41 8270C 06/18/07 1944 kcampigotto Q24348
itrobenzene BRL pg/kg 380 37 8270C 06/18/07 1944 kcampigotto 024348
entchIorophenol BRL pg/kg 380 32 8270C 06/18/07 1944 kcampigotto 024348
Phenanthrene 680 pg/kg 380 18 8270C 06118/07 1944 kcampigofto Q24348
henol BRL pg/kg 380 41 8270C 06/18/07 1944 kcampigotto Q24348
Pyrene 190 pg/kg 380 26 8270C 06/18/07 1944 kcampigotto 024348
Page 26 of 42
ESP Associates PA
ttn Chris Ward
Box 7030
Charlotte NC 28241
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Result Units Report MDL Dilution
Limit Factor
Analysis Analyst
Batch
Date/Time
One surrogate recovery
was outside of the control limits Matrix interference is suspected
Sample Preparation 29.56 mL 3550B 06/15/07 900 dpope P18642
Diesel Range OrganicsDRObyGC-FID
liesel Range Organics DRO
Sample Preparation
cLp Extraction for Metals
CLP Extraction Complete 1311 06/06/07 1345 jhoppel
CLP Leachable Mercury by CVAA
BRL mg/L 0.010 0.000042 7470A 06/08/07 1634 jhoppel Q24140
7470A 06/08/07 715 jhoppel P18573
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
ull SeMce Analytical Environmeii
Laboratory Report
06/20/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
arameter
AB
183471
G0607110
06/05/07 1115
06/05/07 1610
Method
ID
1300 mg/kg 160 20
25.35
Surrogate Recovery Control Limits
246-Tribromophenol 95 25 123
2-Fluorobiphenyl 97 21 108
2-Fluorophenol 90 14 89
Nitrobenzene-cj5 99 14-103
Phenol-d5 86 13 95
Terphenyl-d14 101 41 136
20 8015B 06/08/07 1141 jvogel Q24180
mL 3545 06/07/07 910 wconder P18568
Surrogate Recovery Control Limits
o-Terphenyl DO 49 124
8015B 06/08/07 129 hwagner Q24121
Surrogate Recovery Control Limits
aaa-TFT 129 55-129
asoline Range Organics GRO by GC-FID
Gasoline Range Organics GRO 1.3 mg/kg 1.1 0.072
Sample Preparation 2OmL 3OmL
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 27 of 42
NC Certification No 402AiMUSCCertificationNo99012
NC Drinking Water Cert No 37735
Full SeMce Analytical Environmental Solutions
ESP Associates PA Project ID
Attn Chris Ward
Box 7030
Charlotte NC 28241
Morehead Commons No Client Sample ID
Prism Sample ID
COC Group
Time Collected
Time Submitted
AB
183471
G0607110
06/05/07
06/05/07
Method Analysis
Date/Time
Analyst Batch
ID
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone]M Toll Free Number 1-800/529-6364 Fax [phone]
Laboratory Report
06/20/07
Sample Matrix Soil
Result Units Report MDL Dilution
Limit Factor
11115
1610
Parameter
TCLP Leachable Metals by ICP
Llr$enjC
arium
Cadmium
Chromium
ead
Selenium
Silver
BRL mg/L 0.050 0.0029 6010B 06/11/07 1601 mcampbell Q24175
0.80J mg/L 5.0 0.0019 6010B 06/11/07 1601 mcampbefl Q24175
BRL mg/L 0.025 0.00034 6010B 06/11/07 1601 mcampbeH Q24175
0.0044 mgIL 0.25 0.0006 6010B 06/11/07 1601 mcampbell Q24175
0.016J mgIL 0.050 0.0021 6010B 06/11/07 1601 mcampbell Q24175
0.0086J mg/L 0.050 0.0035 6010B 06/11/07 1601 mcampbell Q24175
BRL mg/L 0.25 0.00025 6010B 06/11/07 1601 mcampbell Q24175
P18570SamplePreparation50mL50mL3010A06/11/07 900 ihoppel
rotal Halogen by Method 9076
.3ubcontract Report See 9076
Attached
Analysis Note for Subcontract Report Analysis subcontracted to NC certified lab 41 618
3ample Comments
BRL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
rhe results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanVELACcertificationexceptforthoseinstances indicated in the case narrative and/or test comments
All results are reported on diy-weight basis
Angela Overcash V.P Laboratory Services
Page 28 of 42
A11IIIII NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
uii Service Analytical Environmental Solutions
SP Associates PA Project ID
kttn Chris Ward
P.O Box 7030
harlotte NC 28241
1arameter Result Units Report MDL Dilution Method Analysis
Limit Factor Date/Time
ercent Solids Determination
Percent Solids 84.1
Laboratory Report
06/20/07
Morehead Commons No Client Sample ID AB
Prism Sample ID 183472
Sample Matrix Soil COC Group G06071 10
Time Collected 06/05/07 1215
Time Submitted 06/05/07 1610
Analyst Batch
ID
SM2540 06/11/07 1700 Ibrown
dolatile Organic Compounds by GC/MS
111 2-Tetrachloroethane BRL pg/kg 5.9 0.71 826GB 06/07/07 2137 erussefl 024080
1-Trichioroethane BRL pg/kg 5.9 0.40 826GB 06/07/07 2137 erussell Q24080
11 22-Tetrachloroethane BRL pg/kg 5.9 0.74 826GB 06/07/07 2137 erussell Q24080
2-Trichloroethane BRL pg/kg 5.9 0.45 826GB 06/07/07 2137 erussell Q24080
1-Dichloroethane BRL pg/kg 5.9 0.52 826GB 06/07/07 2137 erussell Q24080
1-Dichloroethene BRL pg/kg 5.9 0.55 826GB 06/07/07 2137 erussell 024080
i1-Dichloropropene BRL pg/kg 5.9 0.63 826GB 06/07/07 2137 erussell 024080
123-Trichlorobenzene BRL pg/kg 12 0.79 82608 06/07/07 2137 erussell Q24080
23-Trichloropropane BRL pg/kg 5.9 0.63 826GB 06/07/07 2137 erussell Q24080
24-Trichlorobenzene BRL pg/kg 12 0.69 826GB 06/07/07 2137 erusselt Q2408G
24-Trimethylbenzene 860 pg/kg 590 23 50 826GB 06/08/07 1739 erussell 024080
12-Dibromo-3-chloropropane BRL pg/kg 5.9 1.1 826GB 06/07/07 2137 erussell Q24G8G
2-Dibromoethane EDB BRL pg/kg 5.9 0.13 826GB 06/07/07 2137 erussell Q24G8G
i2-Dichlorobenzene BRL pg/kg 12 0.39 826GB 06/07/07 2137 erussell Q24G80
2-DichIoroethane BRL pg/kg 5.9 0.72 826GB 06/07/07 2137 erussell 024080
2-DichIoropropane BRL pg/kg 5.9 0.53 826GB 06/07/07 2137 erussell Q24G80
135-Trimethylbenzene 270 pg/kg 12 0.61 826GB 06/07/07 2137 erussl 024080
3-Dichlorobenzene BRL pg/kg 12 0.62 826GB 06/07/07 2137 erussefi 024080
3-lichloropropane BRL pg/kg 5.9 0.49 826GB 06/07/07 2137 erussell 024080
4-Dichlorobenzene BRL pg/kg 12 0.56 826GB 06/07/07 2137 erussell 024080
22-Dichioropropane BRL pg/kg 5.9 0.36 826GB 06/07/07 2137 erussell Q2408G
-Chioroethyl vinyl ether BRL pg/kg 12 0.53 826GB 06/07/07 2137 erusseD Q24080
2Chlorotoluene BRL pg/kg 12 0.53 826GB 06/07/07 2137 erussell 024080
LHexanone BRL pg/kg 59 0.75 8260B 06/07/07 2137 erussell 024080
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 29 of 42
Laboratory Report
06/20/07
Project ID Morehead Commons No Client Sample ID AB
Prism Sample ID 183472
Sample Matrix Soil COG Group G06071 10
Time Collected 06/05/07 1215
Time Submitted 06/05/07 1610
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
all Service Analytical Environmental Solutions
ESP Associates PA
tttn Chris Ward
P.O Box 7030
harlotte NC 28241
Parameter Result Units Report MDL Dilution
Limit
Method
Factor
Analysis Analyst
Batch
Date/Time ID
-ChIorotoluene BRL pg/kg 12 0.38 826DB 06/07/07 2137 erussefl 024080
4-Methyl-2-pentanone MIBK BRL pg/kg 12 0.72 8260B 06107107 2137 erussell 024080
cetone BRL pg/kg 24 8260B 06/07/07 21 37 erussell 024080
Benzene BRL pg/kg 3.6 0.58 8260B 06/07/07 2137 erussefl 024080
3romobenzene BRL pg/kg 5.9 0.51 826DB 06/07/07 2137 erussell 024080
romochloromethane BRL pg/kg 5.9 0.43 826GB 06/07/07 2137 erussefi 024080
3romodichIoromethane BRL pg/kg 5.9 0.63 8260B 06/07/07 2137 erussell Q24080
3romoform BRL pg/kg 5.9 0.53 826DB 06/07/07 2137 erussell 024080
Bromomethane BRL pg/kg 12 0.84 8260B 06/07/07 2137 erussell 024080
arbon disutfide BRL pg/kg 12 0.46 826DB 06/07/07 2137 erussell 024080
Carbon tetrachioride BRL pg/kg 5.9 0.42 8260B 06/07/07 2137 enissell 024080
hlorobenzene BRL pg/kg 5.9 0.55 8260B 06/07/07 2137 erussefl 024080
Chlorodibromomethane BRL pg/kg 5.9 0.49 8260B 06/07/07 2137 erussell 024080
hloroethane BRL pg/kg 12 0.59 826DB 06/07/07 2137 erussell 024080
Chloroform BRL pg/kg 5.9 0.53 826DB 06/07/07 2137 erussell 024080
hIoromethane BRL pg/kg 12 0.51 826DB 06/07/07 2137 erussell Q24080
is-1 2-Dichloroethene BRL pg/kg 5.9 0.32 826GB 06/07/07 2137 erussell Q24080
cis-1 3-Dichloropropene BRL pg/kg 5.9 0.46 8260B 06/07/07 2137 erussell Q24080
ibromornethane BRL pg/kg 5.9 0.53 826GB 06/07/07 2137 erussell 024080
Dichlorodifluoromethane BRL pg/kg 12 1.6 8260B 06/07/07 2137 erussell 024080
thylbenzene 7.0 pg/kg 5.9 0.51 826GB 06/07/07 2137 erussell 024080
Hexachiorobutadiene BRL pg/kg 18 0.89 8260B 06/07/07 2137 erussell 024080
opropyl ether IPE BRL pg/kg 5.9 0.25 8260B 06/07/07 2137 ewssell 024080
isopropylbenzene 15 pg/kg 12 0.58 826GB 06/07/07 2137 erussell 024080
ip-Xylenes 22 pg/kg 12 1.0 826DB 06/07/07 2137 erussell 024080
Jethyl ethyl ketone MEK BRL pg/kg 24 2.0 826DB 06/07/07 2137 erussefi 024080
Methyl t-butyl ether MTBE BRL pg/kg 5.9 0.42 8260B 06/07/07 2137 erussefi 024080
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 30 of 42
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
One surrogate recovery was outside of the control limits Matrix interference is suspected
Toluene-d8
39 8270C
29 8270C
28 8270C
35 8270C
139
105
67-143
81 128
06118/07 1538 kcampigotto
06118/07 1538 kcampigotto
06/18107 1538 kcampigotto
06/18/07 1538 kcampigotto
024348
024348
024348
Q24348
SP Associates PA
ttn Chris Ward
Box 7030
harlotte NC 28241
Parameter
Laboratory Report
06/20/07
Project ID Moreheaci Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
AB
183472
G0607110
06/05/07 1215
06/05/07 1610
Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
thylene chloride 39 pg/kg 12 0.59 8260B 06/07/07 2137 erussell 024080
n-Butylbenzene 97 pg/kg 18 0.58 8260B 06/07/07 2137 erussell 024080
Propylbenzene 28 pg/kg 12 0.43 82608 06/07/07 2137 erussell Q24080
Naphthalene 1300 pg/kg 300 34 50 8260B 06/08/07 1739 erussell 024080
Xylene BRL pg/kg 5.9 0.43 8260B 06/07/07 2137 erussell Q24080
p-Isopropyltoluene 140 pg/kg 18 0.59 8260B 06/07/07 2137 erussell Q24080
sc-Butylbenzene 44 pg/kg 18 0.48 8260B 06/07/07 2137 erussell 024080
iyrene BRL pg/kg 5.9 0.72 8260B 06/07/07 2137 erussell 024080
tert-Butylbenzene 18J pg/kg 24 0.45 8260B 06/07/07 2137 erussell Q24080
trachloroethene 7.1 pg/kg 12 1.2 8260B 06/07/07 2137 erussell 024080
Toluene BRL pg/kg 5.9 0.49 8260B 06/07/07 2137 erussell Q24080
sns Dichloroethene BRL pg/kg 55 8260B 06/07/07 21 37 erussell 024080
trans-i 3-Dichloropropene BRL pg/kg 5.9 0.51 8260B 06/07/07 2137 erusselJ 024080
ichioroethene BRL pg/kg 5.9 0.43 8260B 06/07/07 2137 erussell 024080
ichlorofluoromethane BRL pg/kg 5.9 0.59 8260B 06/07/07 2137 erussell Q24080
nyl chloride BRL pg/kg 12 0.92 8260B 06/07/07 2137 erussell Q24080
Surrogate Recovery Control Limits
Bromofluorobenzene 159 77-128
Dibromofluoromethane
mi-volatjle Organic ComDouflds by GCIMS
24-Trichlorobenzene BRL pg/kg 390
2-Dichlorobenzene BRL pg/kg 390
3-Dichlorobenzene BRL pg/kg 390
4-Dichlorobenzene BRL pg/kg 390
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 31 of 42
-ull Service Analytical Environmental Solutions
SP Associates PA
ttn Chris Ward
P.O Box7030
Oharlotte NC 28241
1arameter
45-TrichlorophenoI
246-Trichiorophenol
4-DichIorophenol
24-Dimethylphenol
4-DinitrophenoI
24-Dinitrotoluene
6-Dinitrotoluene
J-Chloronaphthalene
2-Chlorophenol
-MethyInaphthalene
2-Methylphenol
-Nitrophenol
34-Methylphenol
3-Dichlorobenzjdjne
46-Dinitro-2-methyIphenol
-Bromophenyiphenylether
-Chloro-3-methyIphenoI
1-Chlorophenylphenylether
-Nitrophenol
Acenaphthene
cenaphthyIene
Anthracene
enzoaanthracene
Benzoapyrene
enzobfluoranthene
enzoghiperyIene
enzokfluoranthene
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/20/07
Project ID Morehead Commons No Client Sample ID AB
Prism Sample ID 183472
Sample Matrix Soil COG Group G06071 10
Time Collected 06/05/07
Time Submitted 06/05/07
1215
1610
Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
BRL pg/kg 390 40 8270C 06/18/07 1538 kcampigotto 024348
BRL pg/kg 390 37 82700 06/18/07 1538 kcampigotto Q24348
BRL pg/kg 390 33 82700 06118/07 1538 kcampigotto Q24348
BRL pg/kg 390 38 8270C 06/18/07 1538 kcampgotto 024348
BRL pg/kg 390 44 82700 06/18/07 1538 kcampigotto Q24348
BRL pg/kg 390 22 8270C 06/18/07 1538 kcarnpigotto Q24348
BRL pg/kg 390 41 8270C 06/18/07 1538 kcampigotto Q24348
BRL pg/kg 390 40 82700 06/18/07 1538 kcampigotto 024348
BRL pg/kg 390 31 8270C 06/18/07 1538 kcampigotto 024348
370 pg/kg 390 31 82700 06/18/07 1538 kcampigotto Q24348
BRL pg/kg 390 37 82700 06/18/07 1538 kcampigotto Q24348
BRL pg/kg 390 47 82700 06/18/07 1538 kcampgofto 024348
BRL pg/kg 390 40 8270C 06/18/07 1538 kcampigotto Q24348
BRL pg/kg 390 24 82700 06/18/07 1538 kcampigotto Q24348
BRL pg/kg 390 24 82700 06/18/07 1538 kcampgouo Q24348
BRL pg/kg 390 37 82700 06/18/07 1538 kcampigctto 024348
BRL pg/kg 390 29 8270C 06/18/07 1538 kcampigotto 024348
BRL pg/kg 390 24 82700 06/18/07 1538 kcampigotto 024348
BRL pg/kg 390 26 8270C 06/18/07 1538 keampigotto 024348
BRL pg/kg 390 38 8270C 06/18/07 1538 keampigotto 024348
BRL pg/kg 390 39 82700 06/18/07 1538 kcampigotto 024348
BRL pg/kg 390 30 82700 06/18/07 1538 kcampigotto 024348
BRL pg/kg 390 55 82700 06/18/07 1538 kcampigotto 024348
BRL pg/kg 390 45 82700 06/18/07 1538 kcampigotto Q24348
BRL pg/kg 390 18 82700 06/18/07 1538 kcampigotto 024348
BRL pg/kg 390 19 8270C 06/18/07 1538 kcampigotto Q24348
BRL pg/kg 390 32 8270C 06/18/07 1538 kcanipigotto Q24348
Page 32 of 42
Laboratory Report
Project ID Morehead Commons No Client Sample ID AB
Prism Sample ID 183472
Sample Matrix Soil COC Group G0607110
Time Collected 06/05/07 1215
Time Submitted 06/05/07 1610
06/20/07
Parameter
s2-chloroethoxymethane
Bis2-chloroethylether
iis2-chloroisopropylether
Bis2-ethylhexylphthalate
utylbenzylphthalate
chiysene
i-n-butyIphthaIate
Ji-n-octylphthalate
Dibenzoahanthracene
ibenzofuran
Diethyphthalate
imethytphthalate
Fluoranthene
luorene
dexachlorobenzene
exachlorobutadiene
Jexachlorocyclopentadjene
Hexachioroethane
ideno1 23-cdpyrene
Isophorone
J-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
aphthalene
Nitrobenzene
entachlorophenol
henanthrene
Phenol
Analysis Analyst Batch
Date/Time ID
06/18/07 1538 kcampigotto 024348
06/18/07 1538 kcampigotto 024348
06/18/07 1538 kcampigotto Q24348
06118/07 1538 kcampigotto Q24348
06/18/07 1538 kcampigotto Q24348
06/18/07 1538 kcampigotto Q24348
06/18/07 1538 kcampigotto Q24348
06/18/07 1538 kcampigotto 024348
06/18/07 1538 kcampigotto Q24348
06/18/07 1538 kcampigotto 024348
06/18/07 1538 kcampigotto 024348
06/18/07 1538 kcampigotto Q24348
06/18/07 1538 kcampigotto Q24348
06/18/07 1538 keampigotto 024348
06/18/07 1538 kcampigotto 024348
06/18/07 1538 kcampigotto 024348
06/18/07 1538 kcampigotto Q24348
06/18/07 1538 kcampigotto Q24348
06/18/07 1538 kcampigotto Q24348
06/18/07 1538 kcampigotto 024348
06/18/07 1538 kcampigotto 024348
06/18/07 1538 kcampigotto Q24348
06/18/07 1538 kcampigotto Q24348
06/18/07 1538 kcampigotto 024348
06/18/07 1538 kcampigotto 024348
06/18/07 1538 kcampigotto 024348
06/18/07 1538 kcampigotto Q24348
--NC Certification No 402
411 VRM11 SC Certification No 99012
NC Dnnking Water Cert No 37735
iull ServIce Analytical Environmental Solutions
E5P Associates PA
kiln Chris Ward
Box7030
Tharlotte NC 28241
Result Units Report MDL Dilution Method
Limit Factor
BRL pg/kg 390 45 8270C
BRL pg/kg 390 42 8270C
BRL pg/kg 390 33 8270C
BRL pg/kg 390 19 8270C
BRL pg/kg 390 24 8270C
BRL pg/kg 390 65 8270C
BRL pg/kg 390 18 8270C
BRL pg/kg 390 29 8270C
BRL pg/kg 390 39 8270C
BRL pg/kg 390 34 8270C
BRL pg/kg 390 24 8270C
BRL pg/kg 390 27 8270C
BRL pg/kg 390 27 8270C
670 pg/kg 390 23 8270C
BRL pg/kg 390 20 8270C
BRL pg/kg 390 38 8270C
BRL pg/kg 390 41 8270C
BRL pg/kg 390 40 8270C
BRL pg/kg 390 40 8270C
BRL pg/kg 390 35 8270C
BRL pg/kg 390 44 8270C
BRL pg/kg 390 20 8270C
BRL pg/kg 390 43 8270C
BRL pg/kg 390 38 8270C
BRL pg/kg 390 33 8270C
790 pg/kg 390 19 8270C
BRL pg/kg 390 43 8270C
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 33 of 42
ull Service Analytical Ewlronmental Solutions
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/20/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
arameter Result Units Report
Limit
MDL Dilution Method Analysis Analyst Batch
Factor Date/Time ID
tyrene 110 pg/kg 390 27 8270C 06/18/07 1538 kcampigotto 024348
Sample Preparation 30.1 mL 3550B 06/15/07 900 dpope P18642
Surrogate
246-Tribromophenol
2-Fluorobiphenyl
Nitrobenzene-d5
Terphenyl-dI
2-Fluorophenol
Phenol-d5
Recovery Control Limits
57 25-123
87
98
90
87
79
21 108
14-103
41 136
14 89
13-95
mg/kg 420 52 50 8015B 06/08/07 1218 jvogel 024180
25.22 mL 3545 06/07/07 910 wconder P18568
Surrogate Recovery Contirol Limits
o-Terphenyl DO 49 124
Surrogate Recovery Control Limits
aaa-TFT 111 55 129
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543
CLP Leachable Mercury by CVAA
lercury BRL mg/L 0.010 0.000042
Sample Preparation 20 mL 30 mL
SP Associates PA
ttn Chris Ward
Box 7030
Tharlotte NC 28241
AB
183472
G06071 10
06/05/07
06/05/07
1215
1610
Jsel Range Organjcs DRO by GC-FID
iesel Range Organics DRO 2100
Sample Preparation
Gasoline Range Organics GRO by GC-FID
Gasoline Range Organics GRO 6.6 mg/kg 1.2 0.076 8015B 06/08/07 200 hwagner 024121
CLP Extraction for Metals
CLP Extraction Complete 1311 06/06/07 1345 jhoppel
7470A 06/08/07 1637 jhoppel
7470A 06/08/07 715 jhoppel
024140
P1 8573
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 34 of 42
ul Service Analytical Environmental Solutions
ESP Associates PA
ttn Chris Ward
Box 7030
-Charlotte NC 28241
Morehead Commons No Client Sample ID
Prism Sample ID
COC Group
Time Collected
Time Submitted
AB
183472
G06071 10
06/05/07 1215
06/05/07 1610
Parameter
fC-P Leachable Metals by ICP
Arsenic
arium
-Cadmium
hromium
ead
Selenium
3ilver
Sample Preparation
otal Halogen by Method 9076
Subcontract Report
Analysis Note for Subcontract Report Analysis subcontracted to NC certified lab 618
ample Comments
BRL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
7ie results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanNELACcertificationexceptforthoseinstances indicated in the case narrative and/or test comments
tll results are reported on dry-weight basis
Angela Overcash V.P Laboratory Services
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID
Sample Matrix Soil
Laboratory Report
06/20/07
Result Units Report MDL Dilution Method
Limit Factor
Analysis Analyst Batch
Date/Time ID
BRL mg/L 0.050 0.0029 6010B 06/11/07 1608 mcampbefl Q24175
0.87J mg/L 5.0 0.0019 6010B 06111/07 1608 mcampbell Q24175
BRL mg/L 0.025 0.00034 6010B 06/11/07 1608 mcampbell Q24175
0.0064J mg/L 0.25 0.0006 6010B 06/11/07 1608 mcampbell 024175
0.013J mg/L 0.050 0.0021 6010B 06/11/07 1608 mcampbell Q24175
0.0092J mg/L 0.050 0.0035 6010B 06/11/07 1608 mcampbell 024175
BRL mg/L 0.25 0.00025 601DB 06/11/07 1608 mcampbell Q24175
5OmL 5OmL
See
Attached
3010A 06/11/07 900 jhoppel
9076
P1 8570
Page 35 of 42
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
SP Associates PA
ttn Chris Ward
P.O Box 7030
harlofte NC 28241
larameter
Laboratory Report
06/20/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COG Group
Time Collected
Time Submitted
AB
183473
G06071 10
06/05/07 1315
06/05/07 1610
Result Units Report MDL
Limit
Dilution Method
Factor
Analysis Analyst Batch
Date/Time ID
ercent Solids Determination
Percent Solids 84.1 5M2540 06/11/07 1700 Ibrown
dolatile Organic Compounds by GC/MS
11 2-Tetrachloroethane BRL pg/kg 5.9 0.59 8260B 06/07/07 2220 erussell 024080
11-Trichloroethane BRL pg/kg 5.9 0.34 826GB 06/07/07 2220 erussell 024080
11 22-Tetrachloroethane BRL pg/kg 5.9 0.61 826GB 06/07/07 2220 erussell 024080
2-Trichloroethane BRL pg/kg 5.9 0.37 82603 06/07/07 2220 erussell Q24080
1-Dichloroethane BRL pg/kg 5.9 0.43 826GB 06/07/07 2220 erussell 024080
1-Dichloroethene BRL pg/kg 5.9 0.46 826GB 06/07/07 2220 erussefl 024080
J1-Dichloropropene BRL pg/kg 5.9 0.53 8260B 06/07/07 2220 erusseli 024080
123-Trichlorobenzene BRL pg/kg 12 0.66 82603 06/07/07 2220 erussell Q2408o
23-Trichloropropane BRL pg/kg 5.9 0.53 826GB 06/07107 2220 erussell 024080
24-Trichlorobenzene BRL pg/kg 12 0.58 826GB 06/07/07 2220 erusseJi 024080
24-Trim ethylbenzene 1100 pg/kg 590 23 50 826GB 06/08/07 1701 erussell Q24080
2-Dibromo-3-chloropropane BRL pg/kg 5.9 0.95 826GB 06/07/07 2220 erussell 024080
2-Dibromoethane EDB BRL pg/kg 5.9 0.11 826GB 06/07/07 2220 eussell 024080
2-Dichlorobenzene BRL pg/kg 12 0.32 8260B 06107/07 2220 erussell 024080
2-Dichloroethane BRL pg/kg 5.9 0.60 826GB 06/07/07 2220 erussell 024080
..2-Dichloropropane BRL pg/kg 5.9 0.44 826GB 06/07/07 2220 erussell 024080
l35-Trimethylbenzene 83 pg/kg 12 0.50 826GB 06/07/07 2220 erussell 024080
3-Dichlorobenzene BRL pg/kg 12 0.52 826GB 06/07/07 2220 erussell 024080
13-Dichloropropane BRL pg/kg 5.9 0.41 826GB 06/07/07 2220 erussell 024080
4-Dichlorobenzene BRL pg/kg 12 0.47 8260B 06/07/07 2220 erussell 024080
22-Dichioropropane BRL pg/kg 5.9 0.3G 82603 06/07/07 2220 erussell 024080
-Chloroethyl vinyl ether BRL pg/kg 12 0.44 826GB 06/07/07 2220 erusseH 024080
2-Chlorotoluene BRL pg/kg 12 0.44 8260B 06/07/07 2220 erussell 024080
-Hexanone BRL pg/kg 59 0.62 82603 06/07/07 2220 erusseH 024080
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 36 of 42
romoform
Bromomethane
carbon disulfide
NC Certification No 402
Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID AB
Prism Sample ID 183473
Sample Matrix Soil COC Group G06071 10
Time Collected 06/05/07 1315
Time Submitted 06/05/07 1610
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRI pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
BRL pg/kg
6.6 pg/kg
BRL pg/kg
BRL pg/kg
13 pg/kg
23 pg/kg
BRL pg/kg
BRL pg/kg
12 0.60
24 2.3
3.6 0.48
5.9 0.42
5.9 0.36
5.9 0.53
5.9 0.44
12 0.70
12 0.38
5.9 0.35
5.9 0.46
5.9 0.41
12 0.49
5.9 0.44
12 0.42
5.9 0.26
5.9 0.38
5.9 0.44
12 1.3
5.9 0.42
18 0.74
5.9 0.20
12 0.48
12 0.84
24 1.7
5.9 0.35
_H Service Ana..cal Envionmentat Solutions
06/20/07
SP Associates PA
Attn Chris Ward
Box 7030
vchar1ofte NC 28241
arat
4-Chiorotoluene
4-Methyl-2-pentanone MIBK
cetone
Benzene
3romobenzene
aromochioromethane
r3romodjchIoromethane
Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
BRL pg/kg 12 0.31 8260B 06/07/07 2220 erussell Q2408o
8260B 06/07/07 2220 erussell 024080
8260B 06/07/07 2220 erussell Q24080
8260B 06/07/07 2220 erussell 024080
8260B 06/07/07 2220 erussell 024080
8260B 06/07/07 2220 erussell 024080
8260B 06/07/07 2220 erusseil 024080
8260B 06/07/07 2220 erussell Q24080
8260B 06/07/07 2220 erussell Q2408o
82608 06/07/07 2220 erussell Q24080
82608 06/07/07 2220 erusseil 024080
8260B 06/07/07 2220 erussell 024080
8260B 06/07/07 2220 erusseD 024080
8260B 06/07/07 2220 erussell Q2408o
8260B 06/07/07 2220 erussell Q24080
82608 06/07/07 2220 erussell 024080
8260B 06/07107 2220 erusseH 024080
826GB 06/07/07 2220 erusseU Q24080
8260B 06/07/07 2220 erussell 024080
826GB 06/07/07 2220 erussefi 024080
8260B 06/07/07 2220 erussell Q24080
82608 06/07/07 2220 erussell Q24080
826GB 06/07/07 2220 erusselt Q2408o
8260B 06/07/07 2220 erussefl Q24080
8260B 06/07/07 2220 erussell 024080
82608 06/07/07 2220 erussell Q24080
8260B 06/07/07 2220 erussell Q2408o
Carbon tetrachioride
hIorobenzene
Chiorodibromomethane
Thioroethane
hIoroform
Ohiorornethane
is-1 2-Dichloroethene
cis-1 3-Dichloropropene
ibromomethane
Dichlorodjfluoromethane
Ethylbenzene
Hexachiorobutadjene
sopropyl ether IPE
Isopropylberizene
np-Xylenes
1ethyl ethyl ketone MEK
Methyl t-butyl ether MTBE
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224.0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 37 of 42
ESP Associates PA
tttn Chris Ward
Box 7030
harlotte NC 28241
Laboratory Report
06/20/07
AB
183473
G06071 10
06/05/07
06/05/07
Parameter
ethylene chloride
n-Butylbenzene
-Propylbenzene
Naphthalene
-XyIene
p-lsopropyltoluene
ec-Bulbenzene
-tyrene
tert-Butylbenzene
etrachloroethene
Toluene
rans-i 2-Dichloroethene
trans-i 3-Dichloropropene
richloroethene
rrichlorofluoromethane
finyl chloride
one surrogate recovery was outside of the control limits Matrix interference is suspected
pg/kg
pg/kg
pg/kg
pg/kg
400 40 8270C
400 29 8270C
400 29 8270C
400 36 8270C
06/18/07 1855 kcampigotto
06/18/07 1855 kcampigotto
06/18/07 1855 kcampigotto
06/18/07 1855 kcampigotto
Q24348
Q24348
Q24348
Q24348
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
1315
1610
Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
13 pg/kg 12 0.49 8260B 06/07/07 2220 erussell Q24080
67 pg/kg 18 0.48 8260B 06/07/07 2220 erusseil Q24o8o
23 pg/kg 12 0.36 82603 06/07/07 2220 erussell Q24080
1200 pg/kg 300 34 50 8260B 06/08/07 1701 erussell Q24080
BRL pg/kg 5.9 0.36 8260B 06/07/07 2220 erusseil Q24080
130 pg/kg 18 0.49 8260B 06/07/07 2220 erussell Q24o8o
43 pg/kg 18 0.40 8260B 06/07/07 2220 erussell Q24080
BRL pg/kg 5.9 0.60 8260B 06/07/07 2220 erussell Q24080
18J pg/kg 24 0.37 8260B 06/07/07 2220 erussell Q2408o
BRL pg/kg 12 1.0 8260B 06/07/07 2220 erussell Q24080
BRL pg/kg 5.9 0.41 82603 06/07/07 2220 erussell Q24o80
BRL pg/kg 5.9 0.46 82603 06/07/07 2220 erussefi Q2408o
BRL pg/kg 5.9 0.42 8260B 06/07/07 2220 erussell Q2408o
BRL pg/kg 5.9 0.36 8260B 06/07/07 2220 erussell Q2408o
BRL pg/kg 5.9 0.49 8260B 06/07/07 2220 erussell 024080
BRL pg/kg 12 0.77 8260B 06/07/07 2220 erussell Q24080
temi-voJatile Organic ComDOunds by GC/MS
24-Trichlorobenzene BRL
2-Dichlorobenzene BRL
3-Dichlorobenzene BRL
4-Dichlorobenzene BRL
Surrogate Recovery Control Limits
Dibromofluoromethane 139 67-143
Bromofluorobenzene 169 77-128
Toluene-d8 105 81 128
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 38 of 42
Laboratory Report
06/20/07
Project ID Morehead Commons No Client Sample ID AB
Prism Sample ID 183473
Sample Matrix Soil COC Group G0607110
Time Collected 06/05/07
Time Submitted 06/05/07
Parameter Batch
______________________ID
45-TrichIorophenol Q24348
246-Trichiorophenol Q24348
Dichlorophenol 024348
24-Dimethylphenol 024348
4-Dinitrophenol Q24348
4-Dinitrotoluene
024348
6-Dinitrotoluene Q24348
-ChloronaphthaIene 024348
2-Chlorophenol 024348
-Methylnaphthalene 024348
2-Methyphenol 024348
-Nitrophenol Q24348
34-Methylphenol 024348
3-Dichlorobenzidine
024348
46Dinitro-2-methylphenol
024348
1r-Bromophenylphenylether 024348
-Choro-3-mothylphenoI 024348
4-Chlorophenyiphenylether 024348
-Nitrophenol
024348
Acenaphthene 024348
kcenaphthylene
024348
Anthracene
Q24348
3enzoaanthracene
Q24348
8enzoapyrene
024348
3enzobfluoranthene
Q24348
Jenzoghiperylene
Q24348
Renzokfluoranthene
024348
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ESP Associates PA
ttn Chris Ward
Box 7030
harlotte NC 28241 1315
1610
Result Units Report MDL Dilution Method Analysis Analyst
Limit Factor Date/Time
BRL pg/kg 400 41 8270C 06/18/07 1855 kcampigotto
BRL pg/kg 400 38 827oC 06/18/07 1855 kcampigotto
BRL pg/kg 400 33 8270C 06/18/07 1855 kcampigotto
BRL pg/kg 400 38 8270C 06/18/07 1855 kcampigotto
BRL pg/kg 400 45 8270C 06/18/07 1855 kcampigotto
BRL pg/kg 400 23 8270C 06/18/07 1855 kcarnpigotto
BRL pg/kg 400 42 8270C 06/18/07 1855 kcampigotto
BRL pg/kg 400 41 8270C 06/18/07 1855 kcampigotto
BRL pg/kg 400 31 8270C 06/18/07 1855 kcampigotto
BRL pg/kg 400 32 8270C 06/18/07 1855 kcampigotto
BRL pg/kg 400 37 8270C 06/18/07 1855 kcampigotto
BRL pg/kg 400 48 8270C 06/18/07 1855 kcampigotto
BRL pg/kg 400 41 8270C 06/18/07 1855 kcarnpigotto
BRL pg/kg 400 25 8270C 06/18/07 1855 kcampigotto
BRL pg/kg 400 24 8270C 06/18/07 1855 kcampigotto
BRL pg/kg 400 38 8270C 06/18/07 1855 kcampigotto
BRL pg/kg 400 29 8270C 06/18/07 1855 kcampigotto
BRL pg/kg 400 25 8270C 06/18/07 1855 kcampfgotto
BRL pg/kg 400 26 8270C 06/18/07 1855 kcamplgotto
BRL pg/kg 400 39 8270C 06/18/07 1855 kcampigotto
BRL pg/kg 400 40 8270C 06/18/07 1855 kcampigotto
BRL pg/kg 400 30 8270C 06/18/07 1855 kcampigotto
190J pg/kg 400 56 8270C 06/18/07 1855 kcampigotto
150 pg/kg 400 46 8270C 06/18/07 1855 kcampigotto
250J pg/kg 400 18 8270C 06/18/07 1855 kcampigotto
BRL pg/kg 400 19 8270C 06/18/07 1855 kcampigotto
IIOJ pg/kg 400 32 8270C 06/18/07 1855 kcampigotto
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Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 39 of 42
s2-chloroethoxymethane
Bis2-chloroethyiether
s2-chloroisopropylether
Bis2-ethylhexylphthalate
tylbenzyIphthalate
Chrysene
Tn..butyIphthalate
_-n-octyphthalate
tibenzoahanthracene
jbenzofuran
Diethylphthalate
methylphthalate
Fluoranthene
uorene
Ffexachlorobenzene
exachIorobutadjene
xachIorocyclopentadiene
Hexachloroethane
derio1 23-cdpyrene
Isophorone
Nitrosodi-n-propylamjne
N-Nitrosodiphenylamine
aphthalene
Nltrobenzene
3ntachlorophenol
enanthrene
Phenol
Project ID Morehead Commons No Client Sample ID AB
Prism Sample ID 183473
Sample Matrix Soil COC Group G06071 10
Time Collected 06/05/07 1315
Time Submitted 06/05/07 1610
TSP Associates PA
ttn Chris Ward
Box 7030
harlotte NC 28241
NC Certification No 402
Laboratory ReportSCCertificationNo99012
NC Drinking Water Cert No 37735 06/20/07
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
BRL pg/kg 400 46 8270C 06/18/07 1855 kcampigotto Q24348
BRL pg/kg 400 43 8270C 06/18/07 1855 kcampgotto Q24348
BRL pg/kg 400 34 8270C 06/18/07 1855 kcampigotto 024348
BRL pg/kg 400 20 8270C 06/18/07 1855 kcampigotto Q24348
BRL pg/kg 400 24 8270C 06/18/07 1855 kcampigotto 024348
180 pg/kg 400 66 8270C 06118/07 1855 kcampigotto Q24348
BRL pg/kg 400 18 8270C 06118/07 1855 kcampigotto 024348
BRL pg/kg 400 30 8270C 06/18/07 1855 kcampigotto Q24348
BRL pg/kg 400 40 827oC 06/18/07 1855 kcampigotto Q24348
BRL pg/kg 400 34 8270C 06/18/07 1855 kcampigotto Q24348
BRL pg/kg 400 25 8270C 06/18/07 1855 kcampigotto Q24348
BRL pg/kg 400 27 8270C 06/18/07 1855 kcampigotto Q24348
450 pg/kg 400 27 8270C 06/18/07 1855 kcampigotto 024348
620 pg/kg 400 24 8270C 06/18/07 1855 kcampigotto 024348
BRL pg/kg 400 21 8270C 06/18/07 1855 kcampigotto 024348
BRL pg/kg 400 39 8270C 06/18/07 1855 kcampigotto Q24348
BRL pg/kg 400 42 8270C 06/18/07 1855 kcampigotto 024348
BRL pg/kg 400 41 8270C 06/18/07 1855 kcampigotto Q24348
BRL pg/kg 400 41 8270C 06/18/07 1855 kcampigotto 024348
BRL pg/kg 400 36 8270C 06/18/07 1855 kcampigotto 024348
BRL pg/kg 400 45 8270C 06/18/07 1855 kcampigotto 024348
BRL pg/kg 400 20 8270C 06/18/07 1855 kcampigotto 024348
BRL pg/kg 400 44 8270C 06/18/07 1855 kcampigotto 024348
BRL pg/kg 400 39 8270C 06/18/07 1855 kcampigotto 024348
BRL pg/kg 400 33 8270C 06/18/07 1855 kcampigotto 024348
750 pg/kg 400 19 8270C 06/18/07 1855 kcampigotto Q24348
BRL pg/kg 400 44 8270C 06/18/07 1855 kcampigotto 024346
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 40 of 42
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Laboratory Report
06/20/07
ESP Associates PA
ttn Chris Ward
Box 7030
Oharlotte NC 28241
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil COC Group
Time Collected
Time Submitted
AB
183473
G06071 10
06/05/07 1315
06/05/07 1610
Parameter Result Units Report
Limit
MDL Dilution Method Analysis Analyst
Batch
Factor Date/Time ID
yrene 550 pg/kg 400 27 8270C 06/18/07 1855 kcampigotto Q24348
Sample Preparation 2951 mL 3550B 06/15107 900 dpope P18642
Surrogate
Phenol-d5
Nitrobenzene-d5
Terphenyl-d14
246-Tribromophenol
2-Fluorophenol
2-Fluorobiphenyl
Recovery Control Limits
80
95
117
81
83
97
13-95
14-103
41 136
25-123
14-89
21 -108
-iesel Range Organ ice DRO by GC-FID
iesel Range Organics DRO
Sample Preparation 25.11 mL 3545
Q24180
06/07/07 910 wconder P18568
Gasoline Range Organ ics GRO by GC-FID
Surrogate Recovery Control Limits
o-Terphenyl DO 49-124
Gasoline Range Organics GRO 7.2 mg/kg 1.2 0.076 8015B 06/08/07 231 hwagner Q24121
One surrogate recovery was outside of the control limits Matrix interference is suspectedL
CLP Extraction for Metals
TCLP Extraction Complete
Surrogate Recovery Control Limits
aaa-TFT 150 55 129
1311 06/06/07 1345 Jhoppel
TCLP Leachable Mercury by CVAA
rlercury BRL mg/L 0.010 0.000042 7470A 06/08/07 1641 jhoppel Q24140
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543
2500 mg/kg 170 21 20 8015B 06/08/07 1426 jvogel
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page 41 of 42
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Analysis Note for Subcontract Report Analysis subcontracted to NC certified lab 618
Sample Comments
JRL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
he results in this report relate only to the samples submitted for analysis and meet state certification requirements other thanIELACcertificationexceptforthoseinstances indicated in the case narrative and/or test commentsA/i results are reported on thy-weight basis
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
Laboratory Report
06/20/07
Project ID Morehead Commons No Client Sample ID
Prism Sample ID
Sample Matrix Soil coc Group
Time Collected
Time Submitted
AB
183473
G06071 10
06/05/07 1315
06/05/07 1610
Result Units Report MDL
Limit
SP Associates PA
ttn Chris Ward
Box 7030
Oharlotte NC 28241
Parameter
Sample Preparation
CLP Leachable Metals by ICP
rsenic
Barium
aclmium
Chromium
ead
elenium
Sample Preparation
7otal Halogen by Method 9076
ubcontract Report
Dilution Method
Factor
2OmL 3OmL
Analysis Analyst Batch
Date/Time ID
7470A 06/08/07 715 jhoppel P18573
BRL mg/L 0.050 0.0029 6010B 06/11/07 1614 mcampbell Q24175
0.77J mg/L 5.0 0.0019 6010B 06/11/07 1614 mcampbefl Q24175
BRL mgIL 0.025 0.00034 6010B 06/11/07 1614 mcampbefl Q24175
0.0044J mg/L 0.25 0.0006 6010B 06/11/07 1614 mcampbeli Q24175
0.015J mg/L 0.050 0.0021 6010B 06/11/07 1614 mcampbell Q24175
0.0069J mgIL 0.050 0.0035 6010B 06/11/07 1614 mcampbell Q24175
BRL mg/L 0.25 0.00025 6010B 06/11/07 1614 mcampbell Q24175
See
Attached
50 mL 50 mL 3010A 06/11/07 900 jhoppel P1 8570
9076
ngela Overcash V.P Laboratory Services
Page 42 of 42
11-Ttichloroeth
11 22-Tetrachloroethane
11 2-Trichloroethane
1-Dichloroethane
1-Dichloroethene
1-Dichloropropene
23-Trichjorobenzene
23-Trichloropropane
24-Trichlorobenzene
24-Trimethylbenzene
2-Dibromoe EDB
2-Dichlorobenzen
2-Dichloroethane
2-Dichloropropane
35-Trimethylbenzene
3-Dichlorobenzene
3-Dichloropropane
4-Dichlorobenzene
22-Dichloropropane
2-Chiorotoluene
2-Hexanone
4-Chiorotoluene
Brornomethane
Carbon tetrachioride
Chlorobenzene
Chiorodibromomethane
Chioroethane
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.05 0.025
ND 0.005 0.0025
0.05 0.025
0.05 0.025
0.003 0.0015
0.005 0.0025
0.005 0.0025
0.005 0.0025
0.005 0.0025
ND 0.01 0.005
ND 0.005 0.0025
ND 0.005 0.0025
ND 0.005 0.0025
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
024080
024080
024080
024080
024080
024080
024080
024080
Q24080
024080
024080
024080
024080
024080
024080
024080
024080
024080
024080
Q24080
024080
024080
024080
024080
024080
024080
Q24080
Q24080
024080
024080
024080
024080
Q24080
024080
ESP Associates PA
Attn Chris Ward
Box 7030
Charlotte NC 28241
Level II QC Report
6/20/07
Project ID Morehead Commons No COC Group Number G0607110
Date/Time Submitted 6/5/07 1610
VoltiIp Ornnin mnnu.nrI by IfIMC......aunj IIICLIIJLI UCVUO
Method Blank
OC BatchResultRLControlUmitUnitsID
ND 0.005 0.0025 mg/kg
ND 0.005 0.0025 mg/kg
ND 0.005 0.0025 mg/kg
ND 0.005 0.0025 mg/kg
ND 0.005 0.0025 mg/kg
ND 0.005 0.0025 mg/kg
ND 0.005 0.0025 mg/kg
ND 0.005 0.0025 mg/kg
ND 0.005 0.0025 mg/kg
ND 0.005 0.0025 mg/kg
ND 0.005 0.0025 mg/kg
ND 0.005 0.0025 mg/kg
ND 0.005 0.0025 mg/kg
ND 0.005 0.0025 mg/kg
ND 0.005 0.0025 mg/kg
ND 0.005 0.0025 mg/kg
4-Methyl-2-pentanone MIBK ND
Acetone ND
Benzene ND
Bromobenzene ND
Bromochioromethane ND
Bromodichioromethane ND
Bromoform ND
ND 0.01 0.005
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of9
4I SC Certification No 99012 Level II QC Report
NC Drinking Water Cert No 37735 6/20/07
Full Service Analytical Environmental Solutions
ESP Associates PA Project ID Morehead Commons No COC Group Number G06071 10
Attn Chris Ward Date/Time Submitted 6/5/07 1610
Box 7030
Charlotte NC 28241
Method Blank
OC Batch
Result RL Control Limit Units ID
Chloroform ND 0.005 0.0025 mg/kg 024080
Chloromethane ND 0.005 0.0025 mg/kg 024080
cis-1 2-Dichloroethene ND 0.005 0.0025 mg/kg 024080
cis-13-Dichloropropene ND 0.005 0.0025 mg/kg Q24080
Dichlorodifluoromethane ND 0.005 0.0025 mg/kg 024080
Ethylbenzene ND 0.005 0.0025 mg/kg 024080
Isopropyl ether IPE ND 0.005 0.0025 mg/kg 024080
lsopropylbenzene ND 0.005 0.0025 mg/kg 024080
mp-Xylenes ND 001 0.005 mg/kg 024080
Methyl ethyl ketone MEK ND 0.1 0.05 mg/kg 024080
Methyl t-butyl ether MTBE ND 0.01 0.005 mg/kg 024080
Methylene chloride ND 0.005 0.0025 mg/kg 024080
n-Butylbenzene ND 0.005 0.0025 mg/kg 024080
n-Propylbenzene ND 0.005 0.0025 mg/kg 024080
Naphthalene ND 0.01 0.005 mg/kg 024080
o-Xylene ND 0.005 0.0025 mg/kg Q24080
p-lsopropyltoluene ND 0.005 0.0025 mg/kg Q24080
sec-Butylbenzene ND 0.005 0.0025 mg/kg 024080
Styrene ND 0.005 0.0025 mg/kg 024080
tert-Butylbenzene ND 0.005 0.0025 mg/kg 024080
Tetrachloroethene ND 0.005 0.0025 mg/kg 024080
Toluene ND 0.005 0.0025 mg/kg 024080
trans-12-Dichloroethene ND 0.005 0.0025 mg/kg Q2408o
trans-I 3-Dichloropropene ND 0.005 0.0025 mg/kg 024080
Trichloroethene ND 0.005 0.0025 mg/kg 024080
Trichlorofluoromethane ND 0.005 0.0025 mg/kg 024080
Vinyl acetate ND 0.025 0.0125 mg/kg 024080
Vinyl chloride ND 0.005 0.0025 mg/kg 024080
Laboratory Control Sample Recovery Recovery QC tchRangesResultSpikeAmountUnitsID/0
11-Dichloroethene 0.05511 0.05 mg/kg 110 57-122 024080
Benzene 0.05834 0.05 mg/kg 117 62-119 024080
Chlorobenzene 0.05586 0.05 mg/kg 112 61-124 Q24080
Toluene 0.05693 0.05 mg/kg 114 57-122 Q24080
Trichloroethene 0.05593 0.05 mg/kg 112 59-129 024080
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
AII SC Cerflflcaon No 99012 Level II QC Report4LINCDrinkingWaterCertNo377356/20/07
Full Service Analytical Environmental Solutions
ESP Associates PA Project ID Morehead Commons No COC Group Number 30607110
Attn Chris Ward Date/Time Submitted 6/5/07 1610
Box 7030
Charlotte NC 28241
Matrix Spike Recovery Recovery CC BatchRangesSampleIDResultSpikeAmountUnitsID
183203 1-Dichloroethene 0.05258 0.05 mg/kg 105 44-1 40 Q24080
Benzene 0.05355 0.05 mg/kg 107 46-1 36 024080
Chlorobenzene 0.05174 0.05 mg/kg 103 47-135 Q24080
Toluene 0.05193 0.05 mg/kg 104 47-136 024080
Trichloroethene 0.04907 0.05 mg/kg 98 45-141 024080
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD RangeSampleIDResultSpikeAmountUnits
183203 11-Dichloroethene 0.05102 0.05 mg/kg 102 44-140 0-23 Q24080
Benzene 0.0532 0.05 mg/kg 106 46-136 0-22 024080
Chlorobenzene 0.05156 0.05 mg/kg 103 47-135 0-22 024080
Toluene 0.05101 0.05 mg/kg 102 47-1 36 0-22 024080
Trichloroethene 004714 005 mg/kg 94 45-141 0-23 024080
Gasoline Range Organics GRO by GC-FID method 8015B
Method Blank
CC BatchResultRLControl Limit Units ID
Gasoline Range Organics GR ND 0.5 mg/kg 024121
Laboratory Control Sample Recovery Recovery
Ranges CC BatchResultSpikeAmountUnitsID
Gasoline Range Organics GR 2.062 mg/kg 103 64-124 024121
Matrix Spike
Recovery Recovery
Ranges CC BatchSample ID
Result Spike Amount Units ID
--
182950 Gasoline Range Organics OR 2.032 mg/kg 102 37-126 024121
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range CC BatchSample ID
Result Spike Amount Units ID
182950 Gasoline Range Organics GR 2036 mg/kg 102 37-126 0-34 024121
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SprinybrookRoadP.O Box 240543 Charlotte NC 28224-0543
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Full Service Analytical Er_._
ESP Associates PA
Attn Chris Ward
Box 7030
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NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
Project ID Morehead Commons No
Level II QC Report
6/20/07
COC Group Number 30607110
Date/Time Submitted 6/5/07 1610
TCLP Leachable Mercury by CVAA method 7470A
Method Blank QC Batch
Result RL Control Limit Units ID
Mercury -0.00006 0.01 0.005 mg/L 024140
Laboratory Control Sample Recovery Recovery
Ranges OC Batch
Result Spike Amount Units ID
Mercury 0.00937 0.0093 mgIL 100 80-120 024140
Matrix Spike Recovery Recovery
Ranges QC Batch
Sample ID
Result Spike Amount Units ID
183468 Mercury 0.00914 0.0093 mgIL 98 80-120 024140
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range QC BatchSample ID
Result Spike Amount Units ID
183468 Mercury 0.00907 0.0093 mg/L 97 80-1 20 -20 024140
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Barium
Cadmium
Chromium
Lead
Selenium
Silver
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
0.2888 0.25
0.1969 0.25
0.2125 0.25
0.218 0.25
0.2431 0.25
0.2354 0.25
mg/L 81 75-125
mg/I 79 75-125
mgIL 82 75-125
mgIL 80 75-125
mg/L 95 75-1 25
mg/I 95 75-125
0-20 Q24175
0-20 024175
0-20 024175
0-20 024175
0-20 Q24175
0-20 Q24175
0-20 024175
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 23224-0543
Phone [phone] Toll Free Number 1-8001529-6364 Fax [phone]
ESP Associates PA
Attn Chris Ward
Box 7030
Level II QC Report
6/20/07
Charlotte NC 28241
TCLP ICP 801 OR
Project ID Morehead Commons No COC Group Number G06071 10
Date/Time Submitted 6/5/07 1610
Method Blank QC Batch
Result RL Control Limit Units ID
Arsenic 0.0023 0.05 0.025 mg/L 024175
Barium 0.0011 2.5 mg/L 024175
Cadmium -0.0014 0.025 0.0125 mg/L 024175
Chromium 0.0035 0.25 0.125 mg/L Q24175
Lead 0.0062 0.05 0.025 mg/L 024175
Selenium -0.0011 0.05 0.025 mgFL 024175
Silver ND 0.25 0.125 mg/I Q24175
Laboratory Control Sample Recovery Recovery
Result Spike Amount Units Ranges CC Batch
ID
Arsenic 0.2424 0.25 mgIL 97 80-120 024175
Barium 0.2223 0.25 mg/L 89 80-120 024175
Cadmium 0.2237 0.25 mg/L 89 80-120 Q24175
Chromium 0.2216 0.25 mg/I 89 80-120 024175
Lead 0.221 0.25 mg/L 88 80-120 Q24175
Selenium 0.245 0.25 mg/L 98 80-1 20 024175
Silver 0.2357 0.25 mgIL 94 80-120 Q24175
Matrix Spike Recovery Recovery
Sample ID Result Spike Amount Units Ranges CC Batch
ID
183459 Arsenic 0.2346 0.25 mg/I 96 75-1 25 024175
Barium 0.2932 0.25 mg/I 83 75-125 024175
Cadmium 0.1973 0.25 mgIL 79 75-125 024175
Chromium 0.2135 0.25 mgIL 83 75-125 024175
Lead 0.216 0.25 mg/L 79 75-125 024175
Selenium 0.2453 0.25 mg/I 96 75-125 Q24175
Silver 0.2377 0.25 mg/L 96 75-125 024175
Matrix Spike Duplicate
Recovery Recovery RPD
Sample ID
Result Spike Amount Units Ranges RPD Range QC Batch
ID
183459 Arsenic 0.2315 0.25 mg/L 95 75-125
Page of
NC Certification No 402
Sc Certification No 99012
NC Drinking Water Cert No 37735
Level II QC Report
6120107
ESP Associates PA
Attn Chris Ward
P.O Box7030
Charlotte NC 28241
fliI Pnng Arini.lflPfl by GCF1fl
ifhn 8015B
182898 Diesel Range Organics DRO 130 80
Project ID Morehead Commons No COC Group Number G06071 10
Date/Time Submitted 6/5/07 1610
mg/kg 70 50-117 0-24 Q241 80
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
FutI SeMen Analytical Environmental Solutions
Method Blank QC Batch
Result RL Control Umit Units ID
Diesel Range Organics DRO ND 3.5 mglkg Q241 80
Laboratory Control Sample Recovery Recovery
Ranges QC Batch
Result Spike Amount Units Va ID
Diesel Range Organics DRO 60.34 80 mg/kg 75 55-109 Q241 80
Matrix Spike Recovery Recovery
Ranges OC Batch
Sample ID Result Spike Amount Units ID
182898 Diesel Range Organics DRO 132 80 mg/kg 73 50-117 024180
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range QC Batch
Sample ID Result Spike Amount Units 0/
ID
Page of
NC Certification No 402 Level II QC Report
SC Certification No 99012 6/20/07
NC Drinking Water Cert No 37735
Fu.Service Analytical
Environmental
ESP Associates PA Project ID Morehead Commons No coc Group Number G06071 10
Attn Chris
Ward Date/Time Submitted 6/5/07 1610
Box 7030
Charlotte NC 28241
Semi-volatile Organic ComBounds by GC/MS method 8270C
Method Blank QC Batch
Result RL Control Umit Units
ID
24-Trichlorobenzefle ND 0.33 0.165 mg/kg 024348
2-Dichlorobenzene ND 0.33 0.165 mg/kg Q24348
3-Dichlorobenzene ND 0.33 0.165 mg/kg Q24348
4-DichlorobenZene ND 0.33 0.165 mg/kg Q24348
245-Trichioropheflol ND 0.33 0.165 mg/kg Q24348
246-Trichloropheflol ND 0.33 0.165 mg/kg 024348
24-Dichiorophenol ND 0.33 0.165 mg/kg Q24348
24-Dimethyiphenol ND 0.33 0.165 mg/kg Q24348
24-Dinitrophenol ND 1.65 0.825 mg/kg 024348
24-Dinitrotoluene ND 0.33 0.165 mg/kg 024348
26-Dinitrotoluene ND 0.33 0.165 mg/kg 024348
2-Chloronaphthalene ND 0.33 0.165 mg/kg 024348
2-Chiorophenol ND 0.33 0.165 mg/kg 024348
2-Methylnaphthalene ND 0.33 0.165 mg/kg Q24348
2-Methylphenol ND 0.33 0.165 mg/kg Q24348
2-Nitrophenol ND 0.33 0.165 mg/kg 024348
34-Methylphenol ND 0.33 0.165 mg/kg Q24348
33-Dichlorobenzidifle ND 0.66 0.33 mg/kg 024348
46-Dinitro-2-methylphenol ND 1.65 0.825 mg/kg 024348
4-Bromophenyiphenylether ND 0.33 0.165 mg/kg Q24348
4-Chloro-3-methylpllenol ND 0.66 0.33 mg/kg 024348
4-Chloroaniline ND 0.33 0.165 mg/kg Q24348
4-Chlorophenylphenylether ND 0.33 0.165 mg/kg 024348
4-Nitrophenol ND 1.65 0.825 mg/kg 024348
Acenaphthene ND 0.33 0.165 mg/kg 024348
Acenaphthylene ND 0.33 0.165 mg/kg 024348
Anthracene ND 0.33 0.165 mg/kg 024348
Azobenzene ND 1.65 0.825 mg/kg 024348
Benzoaanthracene ND 0.33 0.165 mg/kg 024348
Benzoapyrene ND 0.33 0.165 mg/kg 024348
Benzobfluoranthene ND 0.33 0.165 mg/kg 024348
Benzoghiperylene ND 0.33 0.165 mg/kg 024348
Benzokfluoranthene ND 0.33 0.165 mg/kg 024348
Benzoic acid ND 1.65 0.825 mg/kg 024348
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories
Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
99012
Level II QC Report
NC Drinking Water Cert No 37735 6/20/07
Full Service Analytical Environmental Solutions
ESP Associates PA Project ID Morehead Commons No COG Group Number 00607110
Attn Chris Ward Date/Time Submitted 6/5/07 1610
Box 7030
Charlotte NC 28241
Method Blank QC Batch
Result RI Control Umit Units ID
Benzyl alcohol ND 0.66 0.33 mg/kg 024348
Bis2-chloroethoxymethane ND 0.33 0.165 mg/kg 024348
Bis2-chloroethylether ND 0.33 0.165 mg/kg Q24348
Bis2-chloroisopropylether ND 0.33 0.165 mg/kg Q24348
Bis2-ethylhexylphthalate ND 0.33 0.165 mg/kg Q24348
Butylbenzylphthalate ND 0.33 0.165 mg/kg Q24348
Chrysene ND 0.33 0.165 mg/kg Q24348
Di-n-butylphthalate ND 0.33 0.165 mg/kg 024348
Di-n-octylphthalate ND 0.33 0.165 mg/kg 024348
Dibenzoahanthracene ND 0.33 0.165 mg/kg 024348
Dibenzofuran ND 0.33 0.165 mg/kg 024348
Diethylphthalate ND 0.33 0.165 mg/kg Q24348
Dimethylphthalate ND 0.33 0.165 mg/kg Q24348
Fluoranthene ND 0.33 0.165 mg/kg 024348
Fluorene ND 0.33 0.165 mg/kg 024348
Hexachlorobenzene ND 0.33 0.165 mg/kg 024348
Hexachiorobutadiene ND 0.33 0.165 mg/kg 024348
Hexachlorocyclopentadiene ND 0.33 0.165 mg/kg Q24348
Hexachloroethane ND 0.33 0.165 mg/kg 024348
lndeno123-cdpyrene ND 0.33 0.165 mg/kg 024348
lsophorone ND 0.33 0.165 mg/kg 024348
N-Nitrosodi-n-propylamine ND 0.33 0.165 mg/kg 024348
N-Nitrosodiphenylamine ND 0.33 0.165 mg/kg 024348
Naphthalene ND 0.33 0.165 mg/kg Q24348
Nitrobenzene ND 0.33 0.165 mg/kg 024348
Pentachlorophenol ND 1.65 0.825 mg/kg 024348
Phenanthrene ND 0.33 0.165 mg/kg Q24348
Phenol ND 0.33 0.165 mg/kg 024348
Pyrene ND 0.33 0.165 mg/kg 024348
Laboratory Control Sample Recovery Recovery DC BatchRangesResultSpikeAmountUnitsOleID
24-Trichlorobenzene 1.39016 1.6620 mg/kg 84 39-98 Q24348
4-Dichlorobenzene 1.27185 1.6620 mg/kg 77 37-95 024348
24-Dinitrotoluene 1.72881 1.6620 mg/kg 104 56-128 024348
2-Chlorophenol 1.30242 1.6620 mg/kg 78 37-98 Q24348
4-Chloro-3-methylphenol 1.47391 1.6620 mg/kg 89 45-111 Q24348
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoad P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
SCCflon990i2 Level II QC Report
NC Drinking Water Cert No 37735 6/20/07
Full Service Analytical
Environmental Solution
ESP Associates PA Project ID Morehead Commons No coc Group Number G06071 10
Attn Chris Ward Date/Time Submitted 6/5/07 1610
Box 7030
Charlotte NC 28241
Laboratory Control Sample Recovery Recovery
Ranges OC Batch
Result Spike Amount Units ID
4-Nitrophenol 2.24094 1.6620 mg/kg 135 20-157 024348
Acenaphthene 1.52143 1.6620 mg/kg 92 44-110 024348
N-Nitrosodi-n-propylamine 1.32436 1.6620 mg/kg 80 38-101 024348
Pentachlorophenol 2.01495 1.6620 mg/kg 121 53-1 27 Q24348
Phenol 1.21801 1.6620 mg/kg 73 34-102 024348
Pyrene 1.51944 1.6620 mg/kg 91 54-131 Q24348
Matrix Spike Recovery Recovery DC BatchRangesResultSpikeAmountUnitsSampleID
184315 24Tiichlorobenzene 1.35823 1.6603 mg/kg 82 26-97 024348
4-Dichlorobenzene 1.27124 1.6603 mg/kg 77 23-92 024348
24-Dinitrotoluene 1.85292 1.6603 mg/kg 112 45-1 27 Q24348
2-Chlorophenol 1.30179 1.6603 mg/kg 78 25-94 Q24348
4-Chloro-3-methylphenol 1.64774 1.6603 mg/kg 99 31-113 024348
4-Nitrophenol 2.07835 1.6603 mg/kg 125 17-150 024348
Acenaphthene 1.58366 1.6603 mg/kg 95 36-107 024348
N-Nitrosodi-n-propylamine 1.50332 1.6603 mg/kg 91 22-105 024348
Pentachlorophenol 2.03353 1.6603 mg/kg 122 39-137 Q24348
Phenol 1.24302 1.6603 mg/kg 75 23-97 024348
Pyrene 1.77954 1.6603 mg/kg 107 45-133 Q24348
Matrix Spike Duplicate Recovery Recovery RPD
Ranges RPD Range DC Ba
Sample ID Result Spike Amount Units
184315 124-Tiichlorobenzene 1.26892 1.6603 mg/kg 76 26-97 0-37 024348
14-Dichlorobenzene 1.19223 1.6603 mg/kg 72 23-92 0-36 024348
24-Dinitrotoluene 1.75298 1.6603 mg/kg 106 45-127 0-29 024348
2-Chlorophenol 1.20019 1.6603 mg/kg 72 25-94 0-37 Q24348
4-Chloro-3-methylphenol 1.49535 1.6603 mg/kg 90 31-113 10 0-32 Q24348
4-Nitrophenol 2.22045 1.6603 mg/kg 134 17-150 0-32 024348
Acenaphthene 1.45252 1.6603 mg/kg 87 36-107 0-32 024348
N-Nitrosodi-n-propylamine 1.27954 1.6603 mg/kg 77 22-105 16 0-37 024348
PentaChlorophenol 1.97908 1.6603 mg/kg 119 39-137 0-27 Q24348
Phenol 1.20219 1.6603 mg/kg 72 23-97 0-42 Q24348
Pyrene 1.57270 1.6603 mg/kg 95 45-133 12 0-27 024348
-See Case Narrative
This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone] Page of
ACCESS
ANALYrICAL INC
ANALYTICAL REPORT
CLIENT
Prism Laboratories Inc
P0 BOX 240543
Charlotte NC 28224
ATTENTION
Angie Overcash
PROJECT ID
Prism Lab-G06071 10
LABORATORY REPORT NUMBER
207060709
DATE
06/12/2007
Primary Data Review By Secondary Data Review By
Curtis Ekker Ashley Amick
Data Validation Manager GCAL Project Manager Access Analytical
[e-mail]
PLEASE NOTE
Unless otherwise noted all analysis on this report performed at Gulf Coast Analytical Labs GCAL 7979 GSRI
Rd Baton Rouge LA 70820
GCAL is SCDHEC certified laboratory 73006 NCDENR certified lab 618 GA certified lab LA-Ol 955 NELAP
certified laboratory 01955
Local support services for this project are provided by Access Analytical Inc.Access Analytical is representative of
GCAL serving clients in the SC/NC/GA areas All questions regarding this report should be directed to your local Access
Analytical representative at 803.781.4243 or toll free at 888.315.4243
CASE NARRATIVE
Client Prism Laboratories
Inc Report 207060709
Gulf Coast Analytical Laboratories received and analyzed the samples listed
on the sample cross-reference page of this report Receipt of the samples is documented
by the attached chain of custody This applies only to the samples listed in this report
No sample integrity or quality control exceptions were identified unless noted below
No anomalies were found for the analyzed samples
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the
Environmental Protection Agency or other recognized agencies The samples and their corresponding
extracts will be maintained for period of 30 days unless otherwise arranged Following this retention
period the samples will be disposed in accordance with GCALs Standard Operating Procedures
Common Abbreviations Utilized in this Report
ND Indicates the result was Not Detected at the specified RDL
DO Indicates the result was Diluted Out
Ml Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub-Contracted
FLD Indicates the analysis was performed in the Field
PQL Practical Quantitation Limit
MDL Method Detection Limit
RDL Reporting Detection Limit
0000 Reported as time equivalent to 1200 AM
Reporting Flags Utilized in this Report
Indicates an estimated value
Indicates the compound was analyzed for but not detected
ORGANICS Indicates the analyte was detected in the associated Method Blank
INORGANICS Indicates the result is between the RDL and MDL
Sample receipt at GCAL is documented through the attached chain
of custody In accordance with ISO
Guide 25 and NELAC this report shall be reproduced only in full and with the written permission of GCAL
The results contained within this report relate only to the samples reported The documented results are
presented within this report
This report pertains only
to the samples listed in the Report Sample Summary and should be retained as
permanent record thereof The results contained within this report are intended for the use of the client
Any unauthorized use of the information contained in this report is prohibited
certify that this data package is in compliance with the terms and conditions of the contract and
Statement of Work both technically and for completeness for other than the conditions in the case
narrative Release of the data contained in this hardcopy data package and in the computer-readable
data submitted has been authorized by the Quality Assurance Manager or his/her designee as verified by
the following signature
CURTIS EKKER
DATA VALIDATION MANAGER
GCAL REPORT 207060709
THIS REPORT CONTAINS PAGES
Report Sample Summary
GCAL ID Client ID Matrix Collect Date/Time Receive Date/Time
20706070901 183468
Solid 06/05/2007 1100 06/07/2007 0915
20706070902 183469
Soild 06/05/2007 1200 06/07/2007 0915
20706070903 183470
Solid 06/05/2007 1300 06/07/2007 0915
20706070904 183471 Solid 06/05/2007 1115 06/07/2007 0915
20706070905 183472 Solid 06/05/2007 1215 06/07/2007 0915
20706070906 183473 Solid 06/05/2007 1315 06/07/2007 0915
GCAL Report 207060709
Summary of Compounds Detected
ID Client ID Matrix Collect Date/Time Receive Date/Time
20706070901 183468 Solid 06/05/2007 1100 06/07/2007 0915
SW-846 9056 Organic Halides
CAS Parameter Result ROL MDL Units
59473-04-0 Total Organic Halides 232 49.1 21.2 mg/kg
GCAL ID Client ID Matrix Collect Date/Time Receive Date/Time
20706070902 183469 Solid 06/05/2007 1200 06/07/2007 0915
SW-846 9056 Organic Halides
CAS Parameter Result RDL MDL Units
59473-04-0 Total Organic Halides 177 47.2 20.4 mglkg
GCAL ID Client ID Matrix Collect Date/Time Receive Date/Time
20706070903 183470 Solid 06/05/2007 1300 06/07/2007 0915
SW-846 9056 Organic Halides
CAS Parameter Result RDL MDL Units
59473-04-0 Total Organic Halides 149 46.9 20.3 mg/kg
GCAL ID Client ID Matrix Collect Date/Time Receive Date/Time
20706070904 183471 Solid 06/05/2007 1115 06107/2007 0915
SW-846 9056 Organic Halides
CAS Parameter Result RDL MDL Units
59473-04-0 Total Organic Halides 189 45.5 19.7 mg/kg
GCAL ID Client ID Matrix Collect Date/Time Receive Date/Time
20706070905 183472 Solid 06/05/2007 1215 06/07/2007 0915
SW-846 9056 Organic Halides
CAS Parameter Result RDL MDL Units
59473-04-0 Total Organic Halides 176 47.5 20.6 mg/kg
GCAL ID Client ID Matrix Collect Date/Time Receive Date/Time
20706070906 183473 Solid 06/05/2007 1315 06/07/2007 0915
SW-846 9056 Organic Halides
CAS Parameter Result RDL MDL Units
59473-04-0 Total Organic Halides 136 48.2 20.8 mg/kg
GCAL Report 207060709
ID Client ID Matrix Collect Date/Time Receive Date/Time
20706070901 183468 Solid 06105/2007 1100 06/07/2007 0915
SW-846 9056 Organic Halides
Prep Date Prep Batch Prep Method Dilution Analyzed By Analytical Batch
06/05/2007 0900 350786 SW-846 5050 06/08/2007 1506 AEL 350788
CAS Parameter Result RDL MDL Units
59473-04-0 Total Organic Halides 232 49.1 21.2 mg/kg
RESULTS REPORTED ON DRY WEIGHT BASIS
GCAL Report 207060709
SW-846 9056 Organic Halides
59473-04-0 Total Organic Halides
RESULTS REPORTED ON DRY WEIGHT BASIS
177 20.4 mg/kg
ID Client ID Matrix Collect Date/Time Receive Date/Time
183469 Solid 06/05/2007 1200 06/07/2007 0915
CAS Parameter
Prep Date Prep Batch Prep Method Dilution Analyzed By Analytical Batch
06/08/2007 0900 350786 5W-846 5050
06/08/2007 1558 AEL 350788
Result RDL
47.2
MDL Units
GCAL Report 207060709
SW-846 9056 Organic Halides
5947304-0 Total Organic Halides
RESULTS REPORTED ON DRY WEIGHT BASIS
ID Client ID Matrix Collect Date/Time Receive Date/Time
L6070903 183470 Solid 06/05/2007 1300 06/07/2007 0915
CAS Parameter
Prep Date Prep Batch Prep Method Dilution Analyzed By Analytical Batch
06/08/2007 0900 350786 SW-846 5050 06/08/2007 1616 AEL 350788
Result
149
RDL
46.9
MDL
20.3
Units
mg/kg
GCAL Report 207060709
ID Client ID Matrix Collect Date/Time Receive Date/Time
LO6070904 183471 Solid 06/05/2007 1115 06/07/2007 0915
SW-846 9056 Organic Halides
Prep Date Prep Batch Prep Method Dilution Analyzed By Analytical Batch
0610812007 0900 350786 SW-846 5050 06/08/2007 1634 AEL 350788
CAS Parameter Result RDL MDL Units
59473-04-0 Total Organic Halides 189 45.5 19.7 mg/kg
RESULTS REPORTED ON DRY WEIGHT BASIS
GCAL Report 207060709
ID Client ID Matrix Collect Date/Time Receive Date/Time
183472 Solid 06/05/2007 1215 06/07/2007 0915
SW-846 9056 Organic Halides
Prep Date Prep Batch Prep Method Dilution Analyzed By Analytical Batch
06/08/2007 0900 350786 SW-846 5050 06/08/2007 1651 AEL 350788
CAS Parameter Result RDL MDL Units
59473-04-0 Total Organic Halides 176 47.5 20.6 mg/kg
RESULTS REPORTED ON DRY WEIGHT BASIS
GCAL Report 207060709
ID Client ID Matrix Collect DateiTime Receive DateiTime
L60709o6 183473 Solid 06/05/2007 1315 06/07/2007 0915
SW-846 9056 Organic Halides
Prep Date Prep Batch Prep Method Dilution Analyzed By Analytical Batch
06/08/2007 0900 350786 SW-846 5050 06/08/2007 1709 AEL 350788
CAS Parameter Result RDL MDL Units
59473-04.0 Total Organic Halides 136 48.2 20.8 mg/kg
RESULTS REPORTED ON DRY WEIGHT BASIS
GCAL Report 207060709
General Chemistry Quality Control Summary
Analytical Batch 350788
Prep Batch 350786
Prep Method SW-846 5050
Client ID
GCAL ID
Sample Type
Prep Date
Analytical Date
Matrix
183468
20706070901
SAMPLE
06/08/2007 0900
06/08/2007 1506
Solid
494525DUP
495086
DUP
06/08/2007 0900
06/08/2007 1523
Solid
SW-846 9056 Organic Halides Units mg/kg
Result RDL
RPDResultRPDLimit
59473-04-0 Total Organic Halides 189 17.3 197 4.1 25
Analytical Batch 350837
Prep Batch 350836
Prep Method SW-846 5050
Client ID
GCAL ID
Sample Type
Prep Date
Analytical Date
Matrix
MB350836
495472
Method Blank
06/08/2007 1330
06108/2007 1801
Solid
LCS350836
495473
LCS
06/08/2007 1330
06/08/2007 1819
Solid
SW-846 9056 Inorganic Anions Units mg/kg Rd Result %R Limits%R
16887-00-6 Chloride
16984-48-8 Fluoride
24959-67-9 Bromide
WET-036 Total Halides
2.50U 2.50
2.40U 2.40
5.40U 5.40
17U 17
500
500
1000
2000
472
503
1040
2010
94.4
101
104
101
80 120
80 120
80 120
80 120
Analytical Batch 350837
Prep Batch 350836
Prep Method SW-846 5050
Client ID
GCAL ID
Sample Type
Prep Date
Analytical Date
Matrix
18346
20706070901
SAMPLE
06/08/2007 1330
06/08/2007 1837
Solid
494525MS
495475
MS
06/08/2007 1330
06/08/2007 1912
Solid
SW-846 9056 Inorganic Anions Units mg/kg
RUded Result %R Lirnits%R
16887-00-6 Chloride
16984-48-8 Fluoride
24959-67-9 Bromide
WET-036 Total Halides
112 2.50
83.0 2.40
0.000 5.40
195 17
500
500
1000
2000
587
624
1020
2230
95
108
102
102
75 125
75 125
75 125
75 125
GCAL Report 207060709
General Chemistry Quality Control Summary
Analytical Batch 350837
Prep Batch 350836
Prep Method SW-846 5050
Client ID
GCAL ID
Sample Type
Prep Date
Analytical Date
Matrix
183468
20706070901
SAMPLE
06/08/2007 1330
06/08/2007 1837
Solid
494525DUP
495474
DUP
0t/O8/2007 330
06/08/2007 1854
Solid
SW-846 9056 Inorganic Anions Result RPD
1688700-6 Chloride
16984-48-8 Fluoride
24959-67-9 Bromide
WET-036 Total Halides
112 2.50
83.0 2.40
0.000 5.40
195 17
114
87.0
0.000
201
1.8
4.7
25
25
25
25
GCAL Report 207060709
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CHAIN OF CUSTODY RECORD
PAGE L.OF..j QUOTE TO EN7RE PRO BILLING
Project Name c2iio.c
Short Hold Analysis Yes No UST Project Yes No
please ATTACH any project specific reporting QC LEVEL Ill Ill IV
provisions and/or QC Requirei1ts
Invoice To r..c /I4rzc
Address
Purchase Order No./Billing Reference jj7424
Requested Due Date Day Days Days Days Days
Working Days 6-9 Days Standard 10 days us Work ust Be
Samples received after 1500 will be processed next business day
Turnaround time is based on business days excluding weekends and holidays
SEE REVERSE FOR TERMS CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES INC TO CLIENT __________________
PRISM
LABORATORIES INC
Full Service Analytical Environmental Solutions
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Fax [phone]
Client Company Name _______________________
Report To/Contact Name 1/J 2vI43
Reporting Address ______________________________/34/7/c
LAB USE ONLY
Phone ________________Fax Yes No
Email Yes No Email Address_____________________
EDD Type PDF__Excel Ot _________________
Site Location Name
Site Location Physical Address /i
YES NO
Samples INTACT upon arrival
Received ON WET ICE Temp
PROPER PRESERVATIVES indicated J1
Received WITHIN HOLDING TIMES
CUSTODY SEALS INTACT
VOLATILES recd W/OUT HEADSPACE
PROPER CONTAINERS used _T
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC_USACE__FL NCL
SC_OTHER _____N/A
Water Chlorinated YES_NO_
Sample Iced Upon Collection YES NO __________
CLIENT
SAMPLE DESCRIPTION
tvL4Li___42a/p-
DATE
COLLECTEDOI5
ii
TIME
COLLECTED
MILITARY
HOURS
J//
/jt7J/
//4p
120V
/.ZD$
IyJo
MA SAMPLE CONTAINER
WATER OR TYPE
SLUDGE SEE BELOW NO SIZE
YSESAt \z
TIVES çi /\/v/..J A/REMARKS
/I4
--------
--------
PRISM
ID NO
1WL
Relinquished By Signature
Samplers Signature /Zt i-1S Sampled By Print Name YOffi Affihiati
CO
on
Upon relinquishing this Clfin of Custodçis your authorization for Prism to proceed with the analyses àequested above Any changes must be
submitted in writing to the Prism Project Manager There will be charges for any changes after analyses have been initialized
Date Military/Hours-teceivea ny oignaiuret
Relinquished By Signature Received By Signature
Dat
Relinquished By Signature Received Pris aboratories By
Method of Shipment OOOULD BE TAPED
SHW WITH TRANSPORTATION TO THE LABORATORY
SAP ARE NOT ACCEPTED
AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY
U_Fed_Ex__U_UPS Hand-deIivered U_Prism_Field_Service Other
COG GrNo
90 Ito
Additional Comments
NPDES 14T GROUNDWATER DRINKING WATER SOLID WASTE RCRA CERCLA LANDFILL OTHER
UNC USC USC UNC
USC UNC USC UNC USC
UNC USC UNC USC
UNC USC UNC USC
_____ _____
_______________________rrAIRl TVD rrrQ Arrk Ioo PIefk TI ThflrnI irorl an \IflA \/rlatilm flrrianire Anhiciq 7rn HAad Snr
Site Arrival Time
Site Departure Tirtte
Field Tech Fee
Mileage
SEE REVERSE
FOR
TERMS CONDITIONS
ORNAL
PRISM
LABORATORIES tNC
Full Service Analytical Environmental Solutions
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Fax [phone]
Client Company Name ___________________________
Report To/Contact Name _________________________
Reporting Address _______________________________
Phone ________________Fax Yes No
Email Yes No Email
Address______________________EDD Type PDF__Excel__Other
Site Location Name _______________________________
Site Location Physical Address _____________________
CHAIN OF CUSTODY RECORD
PAGE2_OF 7_QUOTE ENSURE PROP7 ING
Project Name beIt
Short Hold Analysis Yes No UST Project Yes No
please ATTACH any project specific reporting OC LEVEL 111111 IV
provisions and/or QC Requirements
Invoice To
Address
IJ.j
YES-NO N/A
amjtIes INTACT upon arrival ..
Received ON WET ICE Temp tT
1AOPER PRESERVATIVES indicatedl
Received WITHIN HOLDINe
TIMES
CUSTODYSEALSINTACT
VOLATILES rscd W/OLT HEADSPACE
PROPER CONTAINERS used ...t
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC__USACE FL _____NC___
SC__OTHER _____N/A _____
Water Chlorinated YES_NO_
Sample Iced Upon Collection YESj NO
Purchase Order No./Billing Reference
Requested Due Date Day Days Days
Days Days
Working Days 6-9 Days Standard 10 days WOlkMJst Be
Samples received after 1500 will be processed next business day
Turnaround time is based on business days excluding weekends and holidays
SEE REVERSE FOR TERMS CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES INC TO CLIENT __________________
SAMPLE DESCRIPTION
2L--ga-/
-5S42
3b4f
TIME
COLLECTED
HOURS/23
/t7/oS
/1
MATRIX SAMPLE CONTAINER
WATER OR TYPE
SLUDGE SEE BELOW NO SIZE
7Z__
i//_liii_____
LYSES REQUESTED
PRESERVA-//7_______
----_--_-
iiiiIiuiiiii
REMARKS
PRISM
iL
L-U-
I_i
/120
Relinquished By Signature
Samplers Signature Sampd By Print Name ffji
Upon relinquishing this C1i of dy is your authorization for Prism to proceed with the anaIyses requested above Any changes
must be
submitted in writing to the Prism Project Manager There Will be charges for any changes after analyses have been initialized
rieceivea iy Signature uate
Relinquished By Signature Received By Signature Date
Relinquished By Signature
Method of
ReoeLababoratorles
By
N5_LL SAMPLEOOLERS SHOULD BE TAPED SHUt 11TH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY
SAMy1S ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY
Fed Es UPS and-delivered Prism Field Service Other
Date
çs
COC Group No
/tfô
no
4-
Military/Hours Additional Comments
NPDES 146T GROUNDWATER DRINKING WATER SOLID WASTE RCRA CERCLA LANDFILL OTHERNCSCNCSCIONCSCNCUSCONC USC UNC USC UNC
USC UNC USC lONG USC
_____ ___________ _________
____________lJ _____ _____trRrrAIM rvD JO Anh k.or Iao PIctIr TI TofIrtnl nod flan \/flA \InItile Orrwtnirs Anilvsis Zero Head Snace
Site Arrival Time
Site Departure Time
Field Tech Fee
Mileage
SEE REVERSE
FORTERMSCONDITIONS
ORGNAL
PRISM
LABORATORIES INC
Full Service Analytical Environmental Solutions
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Fax [phone].
Client Company Name ___________________________
Report To/Contact Name _________________________
Reporting Address _______________________________
CHAIN OF CUSTODY RECORD
PAGE_OF .i QUOTE JENSU7E PROrlLLING
Project Name
Short Hold Analysis Yes No UST Project Yes No
please ATTACH any project specific reporting QC LEVEL 111111 IV
provisions and/or QC Requirements
Invoice To
YES NO
N/A
Samples INTACT upon arrival __
Received ON WET CE Temp
PROPER PRESERVATIVES indicated
Received WITHIN HOLDING TIMES
CUSTODY SEALS INTACT
VOLATILES recd W/OUT HEADSPACE
PROPER CONYAINERS used
Phone ________________Fax Yes No
Email Yes No Email Address_____________________
EDD Type PDF__Excel__Other_________________
Site Location Name _______________________________
Site Location Physical Address
Purchase Order NoiBilIing Reference IYD Z/Z 1O
Requested Due Date Day Days Days Days Days
Working Days 6-9 Days Standard 10 days aWorkfiust Be
Samples received after 1500 will be processed next business day
Turnaround time is based on business days excluding weekends and holidays
SEE REVERSE FOR TERMS CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES INC TO CLIENT
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC__USACE__.._FL____NCj1_
SC_OTHER _____N/A
Water Chlorinated YES_NO_
Sample Iced Upon Collection YES_V NO _________
CLIENT
SAMPLE DESCRIPTIONZ-4k-II/-3
DATECOLLECTED
6s-
TIME MATRIX
COLLECTED SOIL
MILITARY WATER OR
HOURS SLUDGEmcJ//1W
SAMPLE CONTAINER
PRESERVA-
TIVES
.\AYSESEOUD//\kz /i/V\REMARKS/49
-------
------
PRISM
LAB
ID NO
LWL
TYPE
SEE BELOW
GrL
NO SIZE
46-7 Jz2i$l
-LL//
cI21
/zzi/1W ----____
______
cA .-jzc
Relinquished By Signature
Samplers Signature Sampled ByPnnt Name Affiliation
Upon relinquishing thl CIiiI of Custo is your authorization for Prism to proceed with the anaIyses4 requested above Any chang
submitted in writing to the Prism Project Manager There will be charges for any changes after analyses have been initialized
es must be
Hecelvea Dy iwgnaiure Date
Relinquished By Signature Received By Signature Date
Relinquished By SineP Received aiesBy
Method of Shrpment OT SAMPLE C09RS SHOULD BE TAPED SHUl WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORYSAMVLESARE NOT
ACEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY
Fed Ex UPS nd-detivered Prism Field Service Other
/tciô
Group No
14bO1
MIlitary/flours Additional Comments
NPDES qST GROUNDWATER DRINKING WATER SOLID WASTE RCRA
CERCLA LANDFILL OTHER
UNC USC 1NC USC UNC USC UNC
USC UNC USC UNC USC
UNC USC UNC USC UNC
USC_______________________________________
ru.-f-s L....ri -e..-r.FrA -I-tn-.is i7.Qss\
Site Arrival Tfrne
Site Eleparture Time
Field Tech Feet
Mileage
SEE REVERSE FOR
TERMS CONDITIONS
O8NAL
Full ServIce Analytical Environmental Solutions
449 Springbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Fax [phone]
Client Company Name ___________________________
Report To/Contact Name __________________________
Reporting Address _______________________________
Phone ________________Fax Yes No
Email Yes No Email Address__
EDD Type PDF__Excel __Other
Site Location Name _____________
Site Location Physical Address
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification NELAC_USACE__FL ____NC____
SC__OTHER _____N/A
Water Chlorinated YES_NO_
Sample Iced Upon Collection YES JLO _________
CHAIN OF CUSTODY RECORD
PAGE OF ._.9 QUOTE/TO ENS7RE PRBILLiNG
Project Name
Short Hold Analysis Yes No UST Project Yes No
please ATTACH any project specific reporting QC LEVEL 111111 IV
provisions and/or QC Requirements
InVoice To
Address
LABUSEoNLYYE NO N/A
Samples INTACT upon arrival
Received ON WET ICE Temp ______
PROPER PRESERVATIVES indicated
Received WITHIN HOLDING
TIMES __
CUSTODY SEALS INTACT __
VOLATILES recd W/OUT HEADSPACE
PROPER CONTAINERS used
Purchase Order No./Billing Reference /t7/2 oO
Requested Due Date Day Days VDays Days Days
Working Days 6-9 Days Standard 10 days us Work Fiust Be
Samples received after 1500 will be processed next business day
Turnaround time is based on business days excluding weekends and holidays
SEE REVERSE FOR TERMS CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES INC TO CLIEN1 __________________
CLIENT
SAMPLE DESCRIPTION
6a6a6iZk
DATE
COLLECTED
-o
TIME MATRI SAMPLE CONTAINER
COLLECTED SOIL
MILITARY WATER OR TYPE
HOURS SLUDGE SEE BELOW NO SIZE
ii
zL
/wc
PRESERVA-
TIVES Ak
Q\
ii
i1
REMARKS LAB
ID NO
jW3
Helinquisnea uy uignaturej
Samplers Signature Sampled By Print Name Affiliation ci2
Upon relinquishing this OIn of Cust is your authorization for Prism to proceed with the analys as requested
above Any changes
must be
submitted in writing to the Prism Project Manager There will be charges for any changes after analyses have been
initialized
Sineetoret Date MiUta/Hours
Relinquished By Signature Received By Signature
Received Fo atones By Date
Relinquished By Signature
Method of Shipment NOT.sLL SAMPLE RS SHOULD BE TAPED
SHU 111TH CVTO SEALS FOR TRANSPORTATION TO THE LABORATORY
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COG UNTIL RECEIVED AT THE LABORATORY
U_Fed_Ex__U_UPS 1and-delivered U_Prism_Field_Service Other
tpko /Wo
COC Group No
htO ID
Additional Comments
NPDES I4ST GROUNDWATER DRINKING WATER SOLID WASTE RCRA CERCLA LANDFILL OTHER
UNC DSC
NC LSC NC LISC LINC IJSC UNC JSC LINC USC UNC
USC UNC
USC UNC USC
______________________rI.DI.fb-TI Tfl-J od er \/CA \Irltil rnaniCe Anahcic 7rn Hisd Snate
Site Arrival
Tfrne
Site Departure Time
Field Tech Fee
Mileage
SEE REVERSE
FOR
TERMS CONDITIONS
ORINAL