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Item No 17 - Analytical Results Morehead Commons No 2 Incide-OCR
NC Cerilfication No 402 SC Certification No 99012 Laboratory Report NC Drinking Water Cert No 37735 05/24/07 Project ID Morehead Commons No Client Sample ID SP-1 Prism Sample ID 182049 Sample Matrix Soil COC Group G0507568 Time Collected 05/17/07 1600 Time Submitted 05/17/07 1636 Percent Solids Percent Solids ---_I.VCLCIIIIIII@IItJJ This report should not be reproduced except in Its entirety thout the written consent of Prism Laboratories Inc449SpiingbrookRoadP.O Box 240543 Charlotte NC 28224-0543 Phone 704/529-6364 Toll Free Number 1-8O0/529364 Fax 7041525-0409 Page of6 SeMt AiaIyIaI Env ESP Associates PA Atltn Chris Ward P.O Box 7030 Charlotte NC 28241 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Daternme ID SM2541 05/22/07 1258 ibrowi 05/20/07 1037 jvoeI 05/20/07 1037 jvoggi 05/20/07 1037 jvogeI 91.2 ganochIone Pesticides by Gas Chromatography 44-DDD BRL pg/kg 44-DDE BL pg/kg 44--DDT BRL pg/kg 44-Methoxychlor BRL pg/kg a-B-f BRL pg/kg a-Chlordane BRL pg/kg Aldrin BRL pg/kg b-BHC BRL pg/kg Chlordane BRL pg/kg d-6HC BRL pg/kg DieIdrFn BRL pg/kg pg/kg Ed pg/kg Endosuifan Sulfate BRL pg/kg Endrin BRL pg/kg EndrdnAldehyde BRL pg/kg Endriri Ketone BRL pg/kg g-BHC BRL pg/kg g-Chlordane BRL pg/kg Heptachlor BRL pg/kg Heptachlor Epoxide BRL pg/kg Toxaphene 05/20/07 05/20/07 05/20/07 05/20/07 05/20/07 05/20/07 05/20/07 05/207 0- 05Luiu7 05/20/07 2.2 0.67 8081A 2.2 0.47 8081A 2.2 0.79 8051A 4.4 1.5 8081A 2.2 0.20 8081A 2.2 0.38 8081A 2.2 0.44 8081A 22 0.55 8081A 55 12 8081A 2.2 0.31 8081A 1.1 0.45 8081A 2.2 8081A 2.2 8081A 2.2 0.57 8081A 2.2 0.66 8081A 2.2 0.61 SOBIA 2.2 0.43 8081A 2.2 0.26 8091A 2.2 0.36 8081A 2.2 0.52 SOBIA 2.2 0.40 8081A 1037 Jvogel 1037 jvogel 1037 jvogei 1037 jvogel 1037 ivogel 1037 jvogel 1037 jvogei 1037 jvogeI 1037 jvog T337 jvog1 1037 jvogeI 1037 jvogel Q23643 023643 023643 023643 023643 023643 023643 023643 023643 Q2343 Q2 023643 023843 023643 023643 023643 023643 Q236- Q23643 05120/07 1037 jvogel 05/20/07 1037 jvogel 05/20/07 1037 jvogel 05/20/07 1037 jYogel 05/20/07 1037 jvogel 05/20107 1037 jvogei BRL pg/kg 55 12 8081A 05/20/07 1037 jvogel SGO60flNO99O12 Laboratory ReportNCDrinkingWaterCerLNo3773505/24/07 Project ID Morehead Commons No Client Sample ID SP-I Prism Saniple ID 182049 Sample Matrix Soil COG Group G0507568 Time Collected 05117/07 1600 Time Submitted 05/17/07 1636 Parameter Result Units Report MDL Diluon Method Analysis Analyst Batch ___________Limit Factor Date/Time ID Sample Preparation ..or eAnay1J0I Envrnmntt ESP Associates PA Attn Chris Ward 0.Box 7030 Charlotte NC 28241 30.1 10 mL 35503 05/19/07 900 dpope P18411 Surrogate Recovery Control Limits Decachlorobiphen DCB 71 26 -204 Tetrachloro-m-xylene TCMX 48 40-162 oychIorinated Biphenyls PCBs by GC-ECD FC8-l016 BRL mg/kg 0.055 0.010 8082 05/20107 1037 jvogel Q23642 PCI3-1221 BRL mg/kg 0.11 0044 8082 05/20/07 1037 jvoget 023642 PCI3-1232 BRL mg/kg 0.055 0018 8082 05/20/07 1037 jvogel 023642 P013-1242 BRL mg/kg 0.055 0.019 8082 05/20/07 1037 Jvogel Q23642 PCB-1248 BRL mg/kg 0.055 0.0076 8082 05/20/07 1037 Jvogel 023642 PCB-1254 BRL mg/kg 0.055 0.019 8082 05/20/07 1037 ivogel Q23642 PCB-1260 5.1 mg/kg 0.65 0.15 10 8082 05/21/07 941 ivogel 0236.12 Spie Prepsratjon 30.1 10 niL 355DB 0fE17 P2-dnp Surronf 0/ Tetrochoro-n--Iene TCi 3u Decachlorobiphenyl DCB 55 34 182 tile Organic Conpotjnd by CC/MS ll12-Tetrathloroethane BRL pg/kg 6.8 0.67 82603 05/22/07 1603 erussell Q237 ll1-Trlchloroethane BRL pg/kg 6.8 0.38 8260B 05/22/07 1603 enissell 023657 lj22-Tetrachloroethane BRL pg/kg 6.8 0.70 82603 05/22/07 1603 ewseell 023657 llThchloroethane BRL pg/kg 6.8 0.42 82603 05/22/07 1603 erussell Q23657 Il-Dichioroethane BRL pg/kg 68 82603 052fl7 1603 ewsseU 11-DchJoroethene BRL pg/kg 6.8 0.52 8260B 05/22/07 1603 erussell 023657 11-Dichioropropene BRL pg/kg 6.8 0.60 8260B 05/22/07 1603 enissell 023657 l23-rrichlorobenzena BRL pg/kg 14 0.75 82603 05/22/07 1603 erussell 023657 This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543 -- Phone 704/529-6364 Toll Free Number 1-800/529.5364 Fax 704/525-0409 Page of Parameter 23-Trlchloropropane 24-Trichlorobenzene .24-Trim ethylbenzene 2-Dibromo-3cJiloropropane .2-Dibromoethane EDB 2-Dichlorobenzene 12-Dichioroethane 2-Dchloropropane 35-Trim ethyl benzene 3-Dichlorobenzn .3-Dichloropropane 4-Diehlorobenzerie 22-Dichioropropane 2-Chioroethyl vinyl ether NC Certification No 402 Laboratory ReportSCCertificationNo99012 NC Drinking Water Cert No 37735 05/24/07 Project ID Morehead Commons No Client Sample ID SP-1 Prism Sample ID 182049 Sample Matrix Soil COC Group G0507568 Time Collected 05/17/07 1600 Time Submitted 05/17107 1636 Irv Anaydcat EronmDnl ESP Associates PA Altn Chris Ward Box 7030 Charlotte NC 28241 Result Units Report MDL Dilution Limit Factor Method Analysis Date/Time Analyst Batch ID BRL pg/kg 6.8 060 82608 05/22/07 1603 ersseII Q23657 BRL pg/kg 14 0.66 826GB 05/22/07 1603 erussell Q23657 BRL pg/kg 14 0.52 826GB 05/22107 1603 erussell Q23657 BRL pg/kg 6.8 ti 82603 05/22/07 1603 erusseU 023657 BRL pg/kg 6.8 0.12 826GB 05/22107 1603 erussefi 023657 BRL pg/kg 14 0.37 82603 05/22107 1603 erussell Q23657 BRL pg/kg 6.8 0.58 8260B 05/22/07 1603 enissell 023657 SRL pg/kg 6.8 0.51 82603 05/22/07 1603 erussell Q23657 BRL pg/kg 14 057 8260B 05/22/07 1603 erusset 023657 BRL pg/kg 14 0.59 8260B 05/22/07 1603 erussell 023657 BRL pg/kg 6.8 0.48 8260B 05/22/07 1603 erussell Q23657 BRL pg/kg 14 053 826GB 05/22/07 1603 erussell 023657 BRL pg/kg 6.8 0.34 826GB 05/22/07 1603 erusell 023657 api pV 14 0.61 82605 Q/eUr.U Qr E/14 5flfl Li pikg 14 033 8260b 03/..-1 .u eu Q23 BRL pg/kg 14 0.68 626GB 052iJi7 1603 erussell Q2353 BRL pg/kg 27 2.7 826GB 05122107 1603 erusseli Q22 BRL pg/kg 4.1 0.55 82603 0522107 1603 erusseU 021 BRL pg/kg 6.8 0.48 82608 05122/07 1603 en.issell Q233 BRL pg/kg 6.8 0.41 82603 05/22/07 1603 erussell 023657 BPL pg/kg 6.8 0.0 826DB 0522107 1603 ensselJ Q72 BRL pg/kg 6.8 0.51 82605 05/2217 1603 enjssell BRL pg/kg 14 0.79 8260B 05/22/07 1603 erussell 023657 BRL pg/kg 14 0.44 82608 05/22/07 1603 erussell 023657 BRL pg/kg 6.8 0.40 826GB 05/22/07 1603 erussell 023657 4-/ioroLu 4-Methyl-2-pentanone MIBK Acetone Brizene Bron.iobenzene Brornochloromethane rornodichici-om ethane Burofomi Brornornethane Carbon disulfide Carbon tetrachlorjde This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotto NC 28224-0543 Phone 704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page of NC Certification No 402 Laboratory ReportSCCertificationNo99012 NC Drinking Water Cert No 37735 Project ID Morehead Commons No Client Sample ID SP-1 Prism Sample ID 182049 Sample Matrix Soil COC Group G0507568 Time Collected 05/17/07 1600 Time Submitted 05/17107 1636 ESP Associates PA Athri Chris Ward Box 7030 Charlotte NC 28241 05/24/07 ------- Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Chlorobenzene BRL pg/kg 6.8 0.52 8260B 05122/07 1603 erussell 023657 Chlorodibromomethane BRL pg/kg 6.8 0.46 826DB 05/22/07 1603 erussell 023657 Chioroethane BRL pg/kg 14 0.56 826DB 05/22/07 1603 erussell 023657 Chloroform BRL pg/kg 6.8 0.51 826DB 05/22/07 1603 erussel 023657 Chioromethane BRL pg/kg 14 0.48 826DB 05/22/07 1603 erussell 023657 cisi 2-Dichloroethene BRL pg/kg 6.8 0.30 826DB 05/22/07 603 erussell 023657 cisi3-Dichloropropene BRL pg/kg 6.8 0.44 826DB 05/22/07 1603 erussell 023657 Dibromomethane BRL pg/kg 6.8 0.51 82608 05/22/07 1603 erussell 023657 Dchlorodifluoromethane BRL l.rg/kg 14 1.5 82608 05/22/07 1603 en.jssell 023657 Ethylbenzene BRL pg/kg 6.8 048 826DB 05/22/07 1603 erussell 023657 Hexachiorobutadiene BRL pg/kg 21 0.85 8260B 05/22107 1603 erusseil 023657 lsopropyl ether IPE B-RL pg/kg 6.8 0.23 8260B 05/22/07 1603 erusselt Q23657 Isopropylhenzene E.FL pg/kg 14 055 826DB 0512227 1603 erjsselt Q231 07 ET -- .-t- Methylene chloride BRL pg/kg 27 0.56 82608 OS 2/07 1603 erusseEl n-L .iberjzre FOL pg/kg 21 0.52 826DB GUi .77 1603 erussell nfl ylherizne pg/kg 14 825DB r-.--U .-1/e pg/kg 6.5 0.7 826Gb .-iaU o-Xyiiie BRL pg/kg 6.8 0.41 82608 05LS/57 1603 erussel p-lsopropyltoluerte BRL pg/kg 21 0.56 8260B 05/22107 1603 erussefl 0237-27 s--Pr4benzene BI pg/kg 21 826DB 07 1603 eruseerl CT BRL pg/kg 6.8 0.00 82600 05i07 1603 eruss tert-Butylbenzene BRL pg/kg 27 0.42 826DB 05/22/07 1603 erussell Q23557 Tetraohloroethene BRL pg/kg 14 1.2 826DB 05/22/07 1603 erussell Q23657 Tolueiie BRL pg/kg 6.8 0.46 826DB 05/22/07 1603 erussetl 023657 This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SprlngbrooicRoadP.O Box 240543 Charlotte NC 28224-0543 Phone 704/529-63M Toil Free Number 1-800/529-6364 Fax 704/525-0409 Page of ESP Associates PA Attri Chris Ward ROBox7O3O Charlotte NC 28241 5atrle was analyzed as 5030 due to bad purges resulting from the 5035 vials Laboratory Report 05/24/07 sp-1 182049 G0507568 05/17/07 1600 05/17/07 1636 5.32 CR0 05/22107 000 brown CR0 05/22107 000 brown This report should not be reproduced except In Its entirety without the written consent of Prism Laboratories Inc449SprlngbrookRoadP.O Box 240543 Charlotte NC 28224-0543 Phone 704/529-6354 Toll Free Number 1-800/529.6364 Fax 704/525-0409 NC Certification No 402 Sc Certification No 99012 NC Drinking Water Cert No 37735 Project ID Morehead Commons No Client Sample ID Prism Sample 1D Sample Matrix Soil COC Group Time Collected Time Submitted Parameter Result Units Report MDL Dilution Method Limit Factor trans-I 2-Dichloroethene trans-i .3-Dichioropropene Trkhloroethene Trichiorofluoromethane Vinyl chloride BRL BRL BRL BRL BRL pg/kg pg/kg pg/kg pg/kg pg/kg Analyst Batch ID 6.8 0.52 6.8 0.48 6.8 0.41 6.8 0.56 14 088 826DB 82608 826DB 826DB 82608 Analysis Date/Time 05122/07 1603 05/22/07 1603 05/22/07 1603 05/22107 1603 05122/07 1603 erussell erussell erussell erusseH erussIl 023657 Q2367 023657 023657 023657 Surrogate Bromolluorobenzene Toluene-d8 Dibrornofluoromethane Recovery Control Limits 105 77-128 101 81-128 94 67-143 SPmpIeWhtDeterminatjon te nnd Crease by Soxhief L.UI Oil and Grease Dp1 Range Organics DRO Sample Preparation pIe Weight Determination Weight Weight 5235 052 52. 3100 mg/kg 38 30 9071A 05/24/07 700 snianiveh 023755 77 82 jvI 25.14 mL 3545 05/19/07 1200 weonder Pi3flg Surroqfe Rece Confrol Limits o-Terphenyl DO 49-124 4.39 Page of Project ID Morehead Commons No Client Sample ID Prism Sample ID Sample Matrix Soil coc Group Time Collected Time Submitted sP..1 182049 G0507568 05/17107 1600 05/17/07 1636 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Gasoline Range Organics GRO by GC-FID Gasoline Range Organics GRO BRL mg/kg 5.5 0.57 50 8015B 05/22/07 2147 hwagner 023706 Surrogate Recovery Control Limits aaa-TFT 102 55-129 lsbfCP Chromium 22 mg/kg 0.81 0.049 6010B 05/23/07 1343 mcampbeI 023662 Lead 51 mg/kg 0.81 0.068 60108 05/23/07 1343 nlcampbefl 023662 Sample Preparation 2.03 50 mL 3050B 05/21/07 700 jhoppel P15415 Sample Comments BRL Below Repi1ing LimitJr This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc449SpringbrookRoadP.O Box 240543 Charlotte NC 28224-0543 4C Certification No 402 SC Certification No 99012 NC Drinking Water Cert No 37735 ESP Associates PA Attn Chris Ward Box 7030 Charlotte NC 28241 Laboratory Report 05/24/07 Phone704/529-6364 Toll Free Number 1-800/529-6364 Fax 704/525-0409 Page of LPRISM CHAINFCJ4OHTORIEEINCPAGEL_OF_L OUQE 7taPER oiI.I iI Service Analytical Envhonmental lutlons Project Name 1JJLLI449SprlngbrookRoadP.O Box 240543 CharlottJC 28224-0543 Hold An ii sis Yes USPhone704/529-6384 Fax 704/525-0409 fl J1C_5/1i.//VJease ATTACI iny project .icific repoi inj LiiClientCompanyName.---provisIons and/or QCJ3 uirPIiI ts Report TofContact Name 4/invoice To 1Jpt Reporting Address /4t7I-1_______________________-____________________Phone _________________Fax Yes No Purchase Order No./Billing Reference IA Di Email Yes No Email Address Requested Due Date Day Days Days Day Working Days 6-9 Days Standard 10 days Samples received otter 1500 will be cssed next bu.i-v ___________________________Turnaround time Is based on busine days excluding seit SEE REVERSE FOIl TERMS Ci ii TIONS RECARDINCRENDEREDBYPRISMLABORJiIISINC 10 CLIL TIME MATRIX SAMPLE CONTAINER CLIENTSAMPLEDESCRIPTION DATE COLLECTED COLLECTED MILFrARY HOURS SOil WATER OR SLUDGE PRESERVA TIVESTYPE SEE BELOW SIZEWIC-J-O /o rz Samplers Signature Sampled By Print Name Upon relInquishing thIs CIn of Cufdy is your authorization for Prism to proceed with the aiOlVS as requesod aiju submitted In writing to the Prism Project Manager There will be charges for any changes after analyses have been 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TYPE CODES Amber Clear Glass Plastic TL Teflon-Lined Cap VGA Volatile Orgal IJ Additional Comments Sife AriivallmØ Sit Dpthtiire Time ClDNC USC____ is Zero Head Space .FJeld Tech Fee ..Milesge TERMS CONDITIONS ORIGINAL