Item No 8 - Phase I Limited Site Assessment - Incident 9567-OCR

REPORT OF
PHASE LIMITED SITE ASSESSMENT
FORMER WORTH KEETER PROPERTY
1000 SOUTH CLARKSON STREET
CHARLOTTE MECKLENBURG COUNTY NORTH CAROLINA
INCIDENT NO .9567
PREPARED FOR
WEST END LLC
P.O BOX 471721
CHARLOTFE NORTH CAROLINA 28247
PREPARED BY
MACTEC ENGINEERING AND CONSULTING INC
280.1 YORKMONT ROAD
CHARLOTTE NORTH CAROLiNA 28208
MACTEC Project 6228-05-2694
April 15 2005
MACTEC
11 MACTEC
April 15 2005
Mr Chuck Starnes
West End LLC
P.O Box 471 721
Charlotte North Carolina 28247
Subject Report of Phase Limited Site Assessment
Former Worth Keeter Property
1000 South Clarkson Street
Charlotte Meclctenburg county North CarolinaMACTECProject6228-05-2694
Dear Mr Starnes
As authorized by your acceptance of our Proposal No Prop05chltlO6 dated March 2005MACTECEngineeringandConsultingIncVIACTECsubmitsthisPhaseLimitedSite
Atsecnient Report This report includes description of the field activities the results obtained
and MACTECS conclusions and recomrnendations
This report is intended for the use of West End LLC only Reliahce on this document by anyotherpartyisforbiddenwithouttheexpresswrittenconsentofMACTECandthatpartys
acceptance of mutually agreeable terms and conditions Use of this report for purposes beyohd
those reasonably intended by West Enth LLC and MACTEC will he at the sole risk of the user
MACTEC appreciates the continued opportunity to provide our environmental consulting services
If you have questions concerning this report or this project please contact us at 704-357-8600
Sincerely
MACThC ENGINEERING AND CONSULTING INC.-7
Man Miller Lltobert Foster P.G
Staff Environmental Scientist Principal Geogist
Enclosures
MACTEC Engineering and Consulting no
2801 morkrnond Rd Suite 100 Charlotte MC 28208
7OC2S78$0O Fax 7O4357-863g
Report of Phase Limited Site Assessment April 15 2005
Former Worth Keeter PropertyMACTECProject6228-05-2694
TABLE OF CONTENTS
EXECUTIVE SUMMARY
1.0 GENERAL INFORMATION
2.0 SITE HISTORY AND SOURCE CHARACTERISTICS
3.0 RISK CIARACTEfflT1ON
4.0 RECEPTOR INFORMATION
4.1 WATER-SUPPLY WELLS
4.2 PUBLIC WATER SUPPLIES
4.3 SURFACE WATER
4.4 WELLIIEAD PROTECTION AJEAS
4.5 DEEP AQUIFERS IN THE COASTAL PLAIN REGION
4.6 SUBSURFACE STRUCTURES
4.7 AREA LAND USE
4.8 PROPERTY OWNERS AND OCCUPANTS
5.0 GEOLOGY AND IYDROGEOLOGY 10
5.1 TOPOGRAPHIC CONDITIONS 10
5.2 GEOLOGY 10
5.2.1 SiteGeology 10
5.2.2 Regional Geology 10
6.0 SOIL SAMPLING RESULTS 11
6.1 SoIL SAMPLING 11
6.2 LABORATORY TEST RESULTS 11
7.0 GROUNDWATER SAMPLING RESULTS 12
7.1 GROUNDWATER SAMPLING 127.2 LABORATORY TEST RESULTS 12
8.0 CONCLUSIONS AND RECOMMENDATIONS 14
9.0 REFERENCES
Report of Phase ILimited Site Assessment April 15 2005
Former Worth Keeter Properly
MACTEC Project 622845-2694
TABLES
Table 2.1 UST Information
Table 2.2 Tank Closure Soil Analytical Summary
Table 4.1 Owners of Properties Contiguous to Subject Site
Table 6.1 Summary of Soil Laboratory Test Results
Table 7.1 Monitoring Well Installation Data
Table 7.2 Groundwater Analytical Summary
FIGURES
Figure Site Topographic Map
Figure Site Plan
Figure Well Survey Map
Figure Zoning Map
APPENDICES
Appendix Well Construction Records and Boring Logs
Appendix Field Methods
Appendix Laboratory Test Reports and Chain of Custody Records
Appendix Water Well Survey Forms
11
Report of Phase ILimited Site Assessment April 15 2005
Former Worth Keeter Property
MACTEC Project 6228-05-2694
EXECUTIVE SUMMARY
The subject site is the Former Worth Keeter Property located at 1000 South Clarkson Street in
Charlotte North Carolina West End LLC engaged MACTEC Engineering and Consulting Inc
to conduct Phase Limited Site Assessment LSA at the site Atlantic Environmental Services
Inc performed UST Closure Assessment in 1992 The results identified TPH concentrations in
the soil that exceeded the State Action Levels established by the North Carolina Department of
Environment and Natural Resources NCDENR Additional excavation of petroleum-impacted
soils was performed in the former UST area to about 11 feet below ground surface
In March 2005 MACTEC installed three monitoring wells to check for the presence of groundwater
contamination at the site Monitoring wells 9567-1 9567-2 and 9567-3 were installed to depths of
12-14 feet below ground surface bgs MACTEC also collected soil samples The laboratory tested
soil samples for petroleum hydrocarbons
On March 23 2005 MACTEC collected groundwater samples from the three monitoring wells for
analysis Based upon the physical and chemical data collected during this assessment MACTEC
offers the followingconclusions
concentration of aromatic hydrocarbon fractions C9-C22 was identified in
the soil sample 3-4 feet collected from boring 9567-3 that exceeded the
residential MSCC North Carolina General Statues Chapter 143 restricts
residential land use where soil contamination remains in excess of this
standard
The results of the groundwater analysis identified concentration of petroleum
aromatics exceeding the NC 2L standard in well 95 67-3 Chapter 143-B
prohibits installation of water supply well where groundwater contamination
will remain in excess of unrestricted use standards Chapter 143-B also
requires that the owner or responsible party prepare Notice of Residual
Petroleum to be recorded by the Register of Deeds office
The site is located in mixed commercial and industrial area The properties
within 1000-foot radius of the site are connected to municipal water
MACTEC did not identify water-supply wells within 1000-foot radius of the
release area
If residential development is planned for this property MACTEC recommends that Soil
Assessment be performed to assess the vertical and horizontal extent of the affected soils in the
area of boring 9567-3 that exceed the residential standard MACTEC further recommends that the
affected soils be excavated and disposed off-site at permitted facility Soil Cleanup Report
should then be submitted to NCDENR with Request for Site Closure
111
Report of Phase ILimited Site Assessment April 15 2005
Former Worth Keeter Prop ery
MACTEC Project 6228-05-2694
1.0 GENERAL INFORMATION
The property at 1000 South Clarkson Street represents portion of the proposed West End
Development Five diesel fuel underground storage tanks USTs and one new oil UST were
removed from the property in 1992 The diesel tanks were located along South Clarkson Street
and varied in capacity from 1000 to 6000 gallons The single new oil tank was located at the rear
of the shop building separate from the diesel USTs The six USTs were removed with three
resultant excavations
Atlantic Environmental Services AES performedthe UST Closure Assessment and collected soil
samples for analysis from the three excavations The results of the analyses confirmed petroleum-
affected soil in the diesel UST area along Clarkson Street In addition groundwater was
encountered in the excavations and groundwater samples were collected and analyzed for Total
Petroleum Hydrocarbons-Diesel Range Organics TPH-DRO detectable concentration of TPH
was identified in one of the groundwater samples Analysis of the soil samples collected from the
new oil tank excavation did not identif detectable petroleum hydrocarbons
Information regarding site ownership facility information project contacts UST details and
characteristics of the site is presented below
1.1 Ownership of USTs
Worth Keeter Inc
1000 South Clarkson Street
Charlotte North Carolina 28231
1.2 Facility Information
Facility ID 0-014432
Incident 9567
Current Owner Crescent Resources Inc
P.O Box 1003
Charlotte North Carolina 28201-1003
Latitude Longitude
Of Release 35 13.6 80 51.55
1.3 Contacts
Primary Contact Mr Kevin Doherty Crescent Resources Inc
Post Office Box 1003
Charlotte North Carolina 28201-1003
Primary Consultant Mr Robert Foster P.G
MACTEC Engineering and Consulting Inc
2801 Yorkmont Road Suite 100
Charlotte North Carolina 28208
704 357-5530
Report of Phase Limited Site Assessment April 15 2005
Former Worth Keeter Property
MACTEC Project 6228-05-2694
Laboratory Pace Analytical Inc
9800 Kincey Avenue Suite 100
Huntersville North Carolina 28078
704 875-9092
North Carolina Certification Number 37706
14 Release Information
Date release discovered September 1992
Estimated quantity of release Unknown
Source of release Diesel Fuel USTs
Size and contents of USTs from which release occurred Five tanks ranging from 1000 to
6000 gallon capacities
Report of Phase ILimited Site Assessment April 15 2005
Former Worth Keeter Properly
MACTEC Project 6228-05-2694
2.0 SITE HISTORY AND SOURCE CHARACTERISTICS
The Former Worth Keeter property is located at 1000 South Clarkson Street in mostly industrial
and commercial area of Charlotte North Carolina Figure Six USTs formerly used to store
diesel fuel and new motor oil were removed from the site in September 1992 Atlantic
Environmental Services AES submitted the UST Closure Report dated October 30 1992 The
UST information is shown in Table 2.1
Table 2.1 UST Information
Tank Capacity Gallons Last Coittents Date of Removal
6000 Diesel 9-15-92
3000 Diesel 9-15-92
2000 Diesel 9-15-92
1000 Diesel 9-15-92
6000 Diesel 9-15-92
5000 New Oil 9-19-92
Closure soil sampling identified TPH concentrations above the State Action Levels relative to
Tanks and Figure indicates the approximate position of USTs superimposed on the
present day vacant parcel The position of the tanks is based on review of available scaled maps
and MACTEC field observations
Reportedly excavation of petroleum-affected soils was completed at the locations of Tanks
and and the former fuel dispenser island AES reported that the excavations were backfihled
with clean soil The AES report indicates that an unknown quantity of petroleum-affected soil was
disposed off-site Table 2.2 summarizes the analytical data from the UST Closure Assessment
Report of Phase Limited Site Assessment April 15 2005
Former Worth Keeter Prop eriy
MACTECProject 6228-05-2694
Table 2.2 Tank Closure Soil Analytical Summary Taken from AES Report
Sidewall Oil
Depth DRO GROor GreaseSampleIDfeetmg/kg mg/kg mgBottom
2-11 SW 10 10
13
11 10 10 40
2-11 SW 10 10 26
11 10 10 49
2-11 SW 10 10 10
2-11 SW 10 10 10
2-11 SW 10 10 10
11 10 88 14
10 2-11 SW 10 32 15
11 2-11 SW 10 10 12
12 2-11 SW 10 10 10
13 2-11 SW 10 10 10
14 11 10 169 18
15 11 10 94 27
16 11 10 145 10
DRO Diesel Range Organics PreparedlDate RCF 3-31-05
GRO Gasoline Range Oiganics Checked Date JDJ 4-5-05
NA Not analyzed
SW Sidewall Soil Sample
Bottom Soil Sample
In24ch 2005 MACTEC was retained by the prospective site developer to perform Limited Site
Assessment LSA activities at the site
Report of Phase Limited Site Assessment April 15 2005
Former Worth Keeter PropertyMACTECProject6228-05-2694
3.0 RISK CHARACTERIZATION
The following sections are reproduced from the Limited Site Assessment Report format Appendix
pages B-i through B-20 of the Guidelines
LIMITED SITE ASSESSMENT RISK CLASSIFICATION AND LAND USE FORM
Part Groundwater/Surface Water/Vapor Impacts
High Risk
Has the discharge or release contaminated any water supply well including any
used for non-drinking purposes
Not to the owners knowledge
Is water supply well used for drinking water located within 1.000 feet of the
source area of the discharge or releaseNO
Is water supply well used for any purpose e.g irrigation washing cars
industrial cooling water filling swimming pools located within 250 feet of the
source area
of the release or dischargeNO
Does the groundwater within 500 feet of the source area of the discharge or
release have the potential for future use in that there is no other source of water
supply other than the groundwaterNO
Do vapors from the discharge or release pose threat of explosion because of
accumulation of the vapors in confined space or pose any
other serious threat to
public health public safety
or the environmentNO
Are there any other factors that would cause the discharge or release to pose an
imminent danger to public health public safety
or the environmentNO
Intermediate Risk
Is surface water body located within 500 feet of the source area of the
discharge-releaseNO
If yes does the maximum groundwater contaminant concentration exceed the
surface water quality standards and criteria found in 15A NCAC 2B.0200 by
factor of 10NO
Report of Phase ILimited Site Assessment April 15 2005
Former Worth Keeter Property
MACTEC Proj ect 6228-05-2694
Is the source area of the discharge or release located with designated welihead
protection area as defined in 42 Usc 300heNO
Is the release located in the Coastal Plain Physiographic region as designated on
map entitled Geology of North Carolina published by the Department in 1985NO
Do the levels of groundwater contamination for any contaminant exceed the gross
contamination levels GCL established Table by the DepartmentNO
Part II-Land Use
Property Containing Source Area of Release
Does the property contain one or more primary or secondary residences
permanent or temporaryNO
Does the property contain school daycare center hospital playground park
recreation area church nursing home or other place of public assemblyNO
Does the property contain commercial or industrial enterprise an inactive
commercial or enterprise or is the land undeveloped
No the land is presently undeveloped
Do children visit the propertyNO
Is the access to the property reliably restricted consistent with its use e.g fences
security personnel or both
Yes the property is enclosed with chain-link fence and locked gates
Do pavement buildings or
other structures cap the contaminated soilNO
If yes what mechanisms are in place or can be put into place to ensure that the
contaminated soil will remain capped in the foreseeable future
What is the zoning status of the property
Mixed-use DevelOpment MUDD
Report of Phase ILimited Site Assessment April 15 2005
Former Worth Keeter PropertyMACTECProject6228-05-2694
Is the use of the property likely to change in the next 20 yearsYesmixed-use business and residential development is planned for the
site
Part ifi Land Use
Property Surrounding Source Area of Release
The questions below pertain to the area within 1500 feet of the source area of the release
What is the distance from the source area
of the release to the nearest primary or
secondary residence
No residences were observed within 1500-foot radius of the site at the time
of our visit
What is the distance from the source area of the release to the nearest sØhool
daycare center hospital playground park recreation area church nursing home
or other place of public assembly
The Bank of America NFL Stadium is located approximately 1800 feet from
the subject site No other places of public assembly were observed
What is the zoning status of the properties in the surrounding area
Industrial 1-2 and mhed-use MUDD See Figure for zoning in the area
Briefly characterize the use and activities of the land in the surrounding area
Primarily industrial to the south and west Primarily commercial to the
north and the east Immediate surrounding properties are used for vehicle
parking for events at the NFL Stadium
Report of Phase ILimited Site Assessment April 15 2005
Former Worth Keeter Properly
MACTEC Project 6228-05-2694
4.0 RECEPTOR UFORMATION
Potential receptors considered as part of the LSA included identification of water-supply wells
public water supplies surface waters welihead protection areas subsurface structures land use
and property owners and occupants The following sections provide our results of the receptor
investigation
4.1 Water-Supply Wells
MACTEC personnel did not identify water-supply wells within 1000-foot radius of the site The
site area is served by public water supply hi addition MACTEC observed water-meter vaults
along the streets within the required radius 1000-foot radius receptor survey map is included
as Figure
4.2 Public Water Supplies
The site and surrounding facilities within 1500-foot radius are provided public water by
Mecklenburg County Charlotte-Mecklenburg obtains its municipal water from Mountain Island
Lake on the Catawba River
4.3 Surface Water
Irwin Creek is located approximately 1000 feet west-northwest of the release area
4.4 Wellhead Protection Areas
The area is not in welihead protection area
4.5 Deep Aquifers in the Coastal Plain Region
The subject site is not located in the Atlantic Coastal Plain Physiographic Province of North
Carolina
4.6 Subsurface Structures
Basements are not present at the subject site
4.7 Area Land Use
The area within 1500-foot radius of the site consists of commercial and industrial property The
zoning for the site and surrounding properties
is shown on Figure
4.8 Property Owners and Occupants
Contiguous property owners to the subject site are shown on Figure The address of each owner is
listed in Table 4.1
Report of Phase ILimited Site Assessment April 15 2005
Former Worth Keeter Property
IVIACTEC Project 6228-05-2694
Table 4.1
Owners Of Properties Contiguous To Former Worth Keeter Site
Report of Phase Limited Site Assessment
Former Worth Keeter Site
Charlotte North Carolina
MACTEC Project 6228-05-2694
PARCEL NUMBER_LAND OWNER AND ADDRESS PROPERTY ADDRESS
Crescent Resources Inc
073-252-06 P.O Box 1003 912 Post Street
Charlotte NC 28201-1003 Charlotte NC 28202
073-252-02 Charlotte Pipe Foundry 1100 Clarkson StreetP.O Box 35430
Charlotte NC 28202
Charlotte NC 28235
Charlotte Pipe Foundry
073-251-14 P.O Box 35430 1101 1117 Clarkson Street
Charlotte NC 28202
Charlotte NC 28235
073-255-01 Crescent Resources 1001 Clarkson StreetP.O Box 1003
Charlotte NC 28201-1003 Charlotte NC 28202
073-252-08 Crescent Resources 921 Dunbar StreetP.O Box 1003
Charlotte NC 28201-1003 Charlotte NC 28202
Crescent Resources
073-252-09 P.O Box 10t3 914 Clarkson Street
Charlotte NC 28201-1003 Charlotte NC 28202
Crescent Resources
073-256-01 P.O Box 1003 815 Morehead Street
Charlotte NC 28201-1003 Charlotte NC 28202
Crescent Resources
073-252-10 P.O Box 1003 917W Morehead Street
Charlotte NC 28201-1003 Charlotte NC 28202
Report of Phase ILimited Site Assessment April 15 2005
Former Worth Keeter PropertyMACTECProject6228-05-2694
5.0 GEOLOGY AND HYDROGEOLOGY
The following sections describe the regional geologic
conditions and the methods employed to obtain
physical data that support our discussion of the local geologic and environmental conditions
5.1 Topographic Conditions
According to the Charlotte East Topographic Quadrangle Figure and based on site
observations the topography in the vicinity of the site slopes to the north and west The property
is situated at an approximate elevation of 670 feet NGVD
5.2 Geology
5.2.1 Site Geology
The following interpretation of the site geology was developed based on data obtained from the
three soil borings advanced for the three groundwater monitoring wells 9567-1 9567-2 and 9567-3
installed during this assessment The locations of these wells are shown on Figure
MACTEC personnel examined soil samples during the drilling of the three borings Borings
9567-1
and 95 67-3 were advanced within the former tank excavations Reportedly these excavations were
extended to about 11 feet below land surface when the tanks were removed in 1992 AES also
reported that weathered bedrock was encountered at this depth and groundwater was observed in the
open excavations Based on MACTECs soil boring data the soils encountered in borings 9567-1
and 9567-3 were fill material placed in the open excavations following removal of the tanks
Boring 95 67-2 was advanced near the northern end of the former fuel dispenser island location Fill
material consisting of gravel and silty sand was encountered to about 11.5 feet below land surface in
this boring
Groundwater was encountered at depths ranging from to 10 feet below land surface in the three
borings Copies of the boring logs including well construction records for monitoring wells are
provided in Appendix
5.2.2 Regional Geology
According to the Geologic Map .of North Carolina 1985 this area of Charlotte is underlain by
granitic rock Unconsolidated materials found overlying this material are likely weathered rock of
similar composition
10
Report of Phase ILimited Site Assessment April 15 2005
Former Worth Keeter PropertyMACTECProject6228-05-2694
6.0 SOIL SAMPLING RESULTS
6.1 Soil Sampling
On March 18 2005
Probe Technology Inc subcontractor to MACTEC advanced soil borings
9567-1 9567-2 and 9567-3 to depths ranging from 11 to 12.5 feet below ground surface
Borings 9567-1 and 9567-3 were advanced within the former tank excavations Boring 9567-2 was
advanced near the northern end of the former fuel dispenser island location The criteria for the
placement of this boring was primarily because AES reported that their soil samples from the
northern end of the fuel island exhibited the highest TPH concentrations
MACTEC personnel retained soil samples from each boring and placed them in laboratory-
supplied jars for delivery under chain-of-custody to Pace Analytical Inc Pace in Huntersville
North Carolina Soil samples were analyzed for volatile and semi-volatile organic compounds
EPA Methods 8260 and 8270 and volatile and extractable petroleum hydrocarbons MADEP
YPH/EPH detailed description of field methods is presented in Appendix
6.2 Laboratory Test Results
concentration of aromatic hydrocarbon fractions C9-C22 was identified in the soil sample from
boring 9567-3 that exceeded the residential MSCC No detectable concentrations of semi-volatile
organic compounds were identified Laboratory test reports and chain of custody forms are
presented in Appendix The soil sampling results are summarized in Table 6.1 This table also
includes the applicable residential Maximum Soil Contaminant Concentrations MSCCs
Table 6.1 Soil Analytical Data
Residential
Constituent 9567-1 9567-2 9567-3 MSCC
mg/kg ngfkg mg/kg
______________________3-4 ft 7-8 ft 3-4 ft 7-8 ft 3-4 ft 7-8 ft
N-butylbenzene 0.0042 0.0047 0.0048 0.0043 0.014 0.0054 156
Sec-butylbenzene 0.0042 0.0047 0.0048 0.0043 0.011 0.0054 156
Ethvlbenzene 0.0042 0.0047 0.0048 0.0043 0.012 0.0054 1560
lsopropylbenzene 0.0042 0.0047 0.0048 0.0043 0.0095 0.0054 1564
P-Isopropyltoluene 0.0042 0.0047 0.0048 0.0043 0.017 0.0054 None
Naphthalene 0.0042 0.0047 0.0048 0.0043 0.03 0.0054 63
N-propylbenzene 0.0042 0.0047 0.0048 0.0043 0.022 0.0054 156
Toluene 0.0042 0.0047 0.0048 0.0043 0.0046 0.0054 3200
124-trimethylbenzene 0.0042 0.0047 0.0048 0.0043 0.082 0.0054 782
135-trimethylbenzene 0.0042 0.0047 0.0048 0.0043 0.085 0.0054 782
Total Xylenes 0.0042 0.0047 0.0048 0.0043 0.0 16 0.0054 32000
AliphaticsC9-C18 133 12 13 11 4080 12 9386
AliphaticsC19-C36 12 12 13 11 3000 12 93860
AromaticsC9-C22 37 12 13 11 1Ei0 12 469
Aliphatics C5-C8 29 9.6 9.6 11 190 10 939
mg/kg milligrams per kilogram Prepared Date RCF 3/30/05
Checked Date JDJ 4/5/05
11
Report of Phase ILimited Site Assessment April 15 2005
Former Worth Keeter Property
MACTEC Project 6228-05-2694
7.0 GROUNDWATER SAMPLING RESULTS
7.1 Groundwater Sampling
On March 21 and 22 2005
McCall Brothers Inc subcontractor to MACTEC installed
monitoring wells 9567-1 9567-2 and 9567-3 at the locations of the borings with the same
designations described in Section 6.1
Table 7.1 Monitoring Well Installation Data
Bentomte Screened
Total
Sand
Seal Interval
Cement
Depth to WaterWellPackSealDepthfeetbelowfeetbelowfeetbelowtopNofeetbelowfeetbelowftgroundgroundofcaslnggroundsurfacesurfacesurfacegroundsurface
9567-1 12.5 1.5-12.5 1-1.5 2.5-12.5 tooundsurface 10.35
9567-2 12 1.542 11.5 2-12 to ground surface 12.54
95673 14 3-14 2-3 to ground surface 12.09
Water level measured on March 23 2005 from top of casing Prepared/Date RCF3-3 1-05Thecasing stickup
on each well is feet above land surface Checked/Date JDJ 4-8-05
Upon completing the installation of the three wells MACTEC personnel developed the wells by
bailing Prior to sampling MACTEC personnel purged the wells using dedicated disposable
bailers On March 23 2005 MACTEC collected groundwater samples from the wells and
submitted the groundwater samples to Pace The laboratory analyzed the groundwater samples for
volatile organic compounds EPA Method 602 semi-volatile organic compounds EPA Method
625 and volatile and extractable petroleum hydrocarbons by the MADEP methods descriptionofsamplingproceduresisprovidedinAppendix
7.2 Laboratory Test Results
The results of the groundwater analysis identified concentration of petroleum aromatics
exceeding the NC 2L standard in monitoring well 9567-3 Laboratory test reports and chain of
custody forms are included in Appendix Table 7.2 below sinnmarizes the results
12
Report of Phase ILimited Site Assessment April 15 2005
Former Worth Keeter Property
MACTEC Project 6228-05-2694
Table 7.2 Groundwater Analytical Summary
NC2L
Constituents Units 9567i 9567-2 9567-3 Standards
____mgfL
Benzene mg/L 0.001 0.001 0.001 0.001
Methyl tert-butyl ether mg/L 0.00 0.001 0.001 0.2
Ethylbenzene rngfL 0.001 0.001 0.001 0.029
Toluene mg/L 0.001 0.001 0.001 1.0
Xylenes total mg/L 0.001 0.001 0.001 0.53
Naphthalene mg/L 0.005 0.005 0.005 0.021
Petroleum Aliphatics mg/L 0.100 0.100 0.100 0.42
Petroleum Aromatics mgit 100 170 O34U 210
Petroleum Aliphatics C-9-C18 mgfL 0.170 0.640 0.170 4.2
Petroleum Aliphatics C19-C36 mgfL 0.100 0.140 0.170 42.0
Notes Shaded values indicate NC2L Standard exceeded Prepared By/Date RCF 3-31-05
Checked Date JDJ 45-05
13
Report of Phase ILimited Site Assessment April 15 2005
Former Worth Keeter PropertyMACTECProject6228-052 694
8.0 CONCLUSIONS AND RECOMMENDATIONS
Based on the results of our assessment activities we offer the following conclusions
concentration of aromatic hydrocarbon fractions C9-C22 was identified in the soil
sample 3-4 feet collected from boring 9567-3 that exceeded the residential MSCC
North Carolina General Statues Chapter 143 restricts residential land use where
soil contamination remains in excess of this standard Therefore MACTEC
recommends that the affected soils be excavated and disposed off-site at permitted
facility
The results of the groundwater analysis identified concentration of petroleum
aromatics exceeding the NC 2L standard in well 9567-3 Chapter 143-B prohibits
installation of water supply well where groundwater contamination will remain in
excess of unrestricted use standards Chapter 143-B also requires that the owner or
responsible party prepare Notice of Residual Petroleum to be recorded by the
Register of Deeds office
The site is located in mixed commercial and industrial area The properties within
1000-foot radius of the site are connected to municipal water
MACTEC did not identify water-supply wells within 1000-foot radius of the
release area
If residential development is planned for this property MACTEC recommends that Soil
Assessment be performed to assess the vertical and horizontal extent of the affected soils in the
area of boring 95 67-3 that exceed the residential standard MACTEC further recommends that the
affected soils be excavated and disposed off-site at permitted facility Soil Cleanup Report
should be submitted to NCDENR with Request for Site Closure
14
Report of Phase ILimited Site Assessment April 15 2005
Former Worth Keeter Property
MACTEC Project 6228-05-2694
9.0 R1IFERENCES
North Carolina Administrative Code Title 15A Chapter Subchapter 2L Classification and Water
Quality Standards Applicable to the Groundwaters of North Carolina North Carolina Environmental
Management Commission Raleigh North Carolina November 1993
State of North Carolina Department of Environment and Natural Resources Division of Waste
Management UST Section Guidelines for Assessment and Corrective Action April 2001
USGS 7.5-minute Topographic Map Charlotte East North Carolina Quadrangle dated 1993
published by the United States Geological Survey
Geologic Map of North Carolina dated 1985 compiled by the North Carolina Geological Survey
Atlantic Enviromnental Services Inc UST Closure Report dated October 30 1992
Atlantic Environmental Services Inc Comprehensive Site Assessment dated June 25 1993
15
, ir;karltr/il'hi1$e,J;LimittxMiiteAs!essf1fe~i : Fofm,el·. Wort!t l{.flfili~r:fr~~ ·
. MAl:'lBC'Prajcct6WMJ5~1694
USGS KEX
Noturo Vi
Areas
Roads
1000 500 1000
TOPOGRAPHIC MAP
FORMER WORTH KEETER SITE
CHARLOTTE NORTH CAROUNA
Structures
JL Streams
EXPLANATION
QUADRAICI1 L0CATO
1AP OF CHARLOTTE EAST NC DATED 1957 PHOT0RESE 1988
/1 ATF
MAC TEC
EHGINERING CGNWiTIiG INC
CHARLOTtE NORTH CAROLINA
APPROXThATE SCALE iN 1EET
1DATFI JO3NO -r FGURE
EXPLANATION
APPROXIMATE LOCATION OF
FORMER WORTH KEETER SITE BOUNDARY
APPROXIMATE LOCATION OF
GROUNDWATER MONFIORING WELL
REF 2002 AERIAL PHOTOGRAPH OF MECKLENBURG COUNTY NC POLARIS PROPERTY OWNERSHIP LAND RECORDS INFORMATION SYSTEM
SMACTEC SITE PLAN
CNGMJEW4G CONSLYWG pjç FORMER WORTH KEETER SITE
CHARLOTTE NORTH CAROLiNA CHARLOTTE NORTH CAROUNA
JOB NOPREPAREOrtDATEJCHECKEDiYij/jDATE 6228052694 FIGURE
EXPLANATION
-H iOOO FOOT RADIUS
Wa
Wa
a.OW
to
REF MECKLENURG COUNTY NORTH CAROUNA IS GEOGRAPHIC INFORMATION SYSTEM
REPARP jr/i DATE
MACTEC WELL SURVEY MAP
ENCNEERNG CONSULflNG FORMER WORTH KEETER SITE
CHARLOTTE NORTH CAROLiNA CHARLOTTE NORTH CAROUNA
bATE JOB NO FIGURE
20
SOIL CLASSIFICATIONAND REMARKS
SEE KEY SYMBOL SHEET FOR EXPLANATION OFSYMBOLS AND ABBREVIATIONS BELOW
FILL Gravel and Silty Fine SAND
ft
SAMPLES
N-COUNT
NM%LL%
FINES
SPTIbpI
10 20 30 40 50 60 70 80 90 100
It
FILL-Brown Micaceous Silly FiXD
10
-Soil Very Wet Rt 11 Feet flieel flie
1.5
WEATHERED ROCKat12Fee
Auger Refusal at 12.5 FtGroundwater Measured at 8.35 Ft Below Ground
25
30
35
40
Cd
...
Cd
DRILLER Foster
EQUIPMENT
METHOD Hollow-stem AugerHOLEDIA
PREPARED BY
CHECKED BY
REMARKS Set PVC Casing and 10 Ft 0.010 Slotted PVC
Screen to 12.5 Ft Depth with Ft Stick up
10 20 30 40 50 60 70 80 90 100
Former Worth Keeter
THIS RECORD IS REASONABLE INTERPRETATIONOFSUBSURFACECONDITiONSAT THE EXPLORATIONLOCATIONSUBSURFACECONDITIONSAT OTHERLOCATIONSAND AT OTHER TIMES MAY DIFFERINTERFACESBETWEENSTRATAAREAPPROXIMATETRANSITIONSBETWEENSTRATAMAYBEGRADUAL
PROJECT
LOCATION
PROJECT NO 6228-05-2694
DRILLED March 21 2005
BORI1G NO 9567-1
./dl
__j0rMACTEC
PAGE OF
ft
SAMPLES
N-COUNT
PL NM%
FINES
SPTlbpf
10 20 30 40 50 60 70 80 90 101
Auger Kelusal and Well Terminated at I2.0FtGroundwaterMeasuredat10.5 Ft Below Ground
SOIL CLASSIFICATIONAND REMARKS
SEE KEY SYMBOL SHEET FOR EXPLANATION OF
ft SYMBOLS AND ABBREVIATIONS BELOW
FILL Gravel and Silty Fine SAND
FILL-Brown Micaceous Silty Fine SAND DieselOdor
10
WEATHERED ROCKat 11.5 Feet
15
20
25
30
35
40
DRILLER Foster
EQUIPMENT
METHOD Hollow-stem AugerHOLEDIA
PREPARED BY
CHECKED BY
REMARKS Set PVC Casing and 10 Ft 0.010 Slotted PVC
Screea to 12 Ft Depth with Ft Stickup
10 20 30 40 50 60 70 80 90 100
THIS RECORD IS REASONABLE INTERPRETATIONOFSUBSUREACEC0NDrn0NSAT THE EXPLORATIONLOCATIONSUBSURPACECONDITIONSATOTHERLOCATIONSANDATOTHERTIMESMAYDIFFERINTERFACESBETWEENSTRATAAREAPPROXIMATETRANSITIONSBETWEENSTRATAMAYBEGRADUAl
PROJECT Former Worth KeeterLOCATION
PROJECT NO 6228-05-2694DRILLEDMarch212005
F011IG NO 9567-2 PAGE OF
fMACTEC
SOIL CLASSIFICATION
AND REMARKS
SEE KEY SYMBOL SHEET FOR EXPLANATION OF
SYMBOLS AND ABBREVIATIONS BELOW
SAMPLES
ft
NM
N-COUNT
LL
FINES
SPTbpf
10 20 30 40 50 60
FILL Red Brown Silty Fine SAND
FILL Dark Gray Silty Fine SAND
70 80 90 100
WEATHERED BEDROCK-Air-Drilled from
II-l4Feet
-5
10
15
20
25
30
35
40
Auger Refusal at 14.0 FtGroundwaterMeasuredat 10 Ft Below Ground
1-
DRILLER Foster
EQUIPMENT
METHOD Auger and Air RigHOLEDIA
PREPARED BY
CHECKED BY
REMARKS Set PVC Casing and 10 Ft 0.010 Slotted PVC
Screm to 14 Ft Depth
THIS RECORD IS REASONABLE iNTERPRETATIONOFSUBSURFACECONDITIONSAT THE EXPLORATIONLOCATIONSUBSURFACECONDITIONSATOTHERLOCATIONSANDATOTHERTIMESMAYDIFFERINTERFACESBETWEEN STRATA ARE APPROXIMATETRANSITIONSBETWEENSTRATAMAYBEGRADUAL
10 20 30 40 50 60 70 80 90 100
PROJECT Former Worth Keeter
LOCATION
PROJECT NO 6228-05-2694
DRILLED March 21 22 2005BORINGNO9567-3
MACTEC
PAGE O1
Report of Phase ILimited Site Assessment April 15 2005
Former Worth Keeter Property
MACTEC Project 6228-05-2694
FIELD METHODS
Listed below are the
standard field methods usedduring this project
Soil Borings and Well Installation
On March 18 2005 soil samples were collected from borings 9567-1 9567-2
and 9567-3 using
Direct Push Technology employing stainless-steel core barrels to advance the boreholes
Continuous soil samples were obtained in four-foot lengths with stainless-steel sampling tube
and acetate tube liners To reduce the potential for cross-contamination the subcontractor
decontaminated down-hole probing equipment by steam-cleaning before beginning the project and
between the boreholes
The soil samples were placed in laboratory-prepared sample containers marked with unique
identifying number placed on ice in sample cooler and delivered to Pace Analytical Inc
North Carolina certified laboratory located in Huntersville North Carolina for analysis The
samples were maintained under chain-of-custody protocol
On March 21 and 22 2005 groundwater monitoring wells 9567-1 9567-2 and 9567-3 were
installed at the site The borings were drilled using truck-mounted drilling rig equipped with 8-
inch O.D hollow-stem augers The termination depth of each boring was selected based on the
depth to auger refusal
Type II monitoring well was installed in each of the borings Each Type II well was constructed
with 2-inch diameter Schedule 40 PVC flush-threaded casing and screen The PVC screen and
casing were lowered into the open borehole 10-foot length of slotted well screen with machined
0.010-inch slot widths and threaded bottom plug was installed at the bottom of each well solid
section of PVC riser was placed above the screened interval and extended to point approximately
two feet above the ground surface The annular space around each well was filled with filter sand
to approximately to feet above the top of the screen
seal of bentonite pellets was placed immediately above the sand pack After placement in the
well the bentonite pellets were allowed to hydrate approximately
24 hours After hydrating the
bentonite pellets bentonite/neat cement mixture containing approximately 4%bentonite was
pumped down the borehole to fill the annular space from the bentonite seal to the ground surface
The top of each well casing was equipped with lockable watertight well plug Well construction
records are included in Appendix
Monitoring Well Groundwater Sampling
The monitoring wells were developed by bailing an amount equal to casing volumes of water
until the waters turbidity was reduced and it was determined that each monitoring well was
functioning properly
Prior to sampling the volume of water in each well was measuredMACTECfieldrepresentativepurgedeachwellofanadditionalcasingvolumesofwater
Groundwater samples were collected using disposable polyethylene
bailers
The collected groundwater samples were placed in laboratory-prepared sample containers marked
with unique identifying number preserved as required placed on ice in sample cooler and
delivered to Pace for analysis The samples were maintained under chain-of-custody protocol
Repori i:Jlf ht#~•1L,irfzil~.$iier4sspsm~tti
Furm.er;'fftctth Jfeeter Propeit)' . : MACTEifJW;~d 6228-0.~·2694 ,·.' ' ' : ' , ,· ·~ ·'
! :
7ZAnaIyflcar
tn4tpaneJabscom
Mr Rob Foster
Mactec
2801 Forionont Road
Suite 100
Charlotte NC 28208
RE Lab Project Number
Client Project ID
Dear Mr Foster
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Enclosed are the analytical results for samples received by the laboratory on March 18 2005 Results reported
herein conform to the most current NEWC standards where applicable unless otherwise narrated in the body of
the report.
Phone [phone]
Fax [phone]
If you have any questions concerning this report please feel free to contact me
Sincerely
iLetó 44t
nnette Scott
Znnette .Scottpacelabs .com
Project Manager
Enclosures
Asheville Certification IDs
NC Wasiewater 40
NC Drinking Water 27712
SC Environmental 99030
FLPAELAP E87648
REPORT OF LABORATORY ANALYSIS
Thin report shall not be reproduced except in lull
without the written consent ot Pace Analytical Services Inc
Qhatlottn Certitication IDa
NCWatewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
March 29 2005
9290353
West End 6228052694
Pace Analytical Ser.vices Inc
9800 Kinney Avenue Suite 100
Huntersvile NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 622805-2694
Lab Sample No 925409690
Client Sample ID 9567-2
Project Sample Number 9290353-016
Matrix Soil
Date Collected 03/18/05 1110
Date Received 03/18/05 1525
Wet Chistry
Percent Moisture Method Moisture
Percent Moisture 10.4
analyzed Br We
1.0 03/21/05 0852 TNS
Asheville Certification Do
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in tell
without the written consent of Pace Analytical Seivices Inc
Cha4olte Certification lOs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87527
tnits Report Limit
GC/MS Semivo.atiles
Semiolati1e Organics Prep/Method EPA 3545 EPA 8270
Acenaphthene ND ug/kg 370 1.1 03/24/05 1547 BET 83329
Acenaphthylene ND ug/kg 370 1.1 03/24/05 1547 BET 208968
thracene ND ug/kg 370 1.103/24/05 1547 BET 120-127
Benzokfluoranthene ND ug/kg 370 1.1 03/24/05 1547 BET 20708-9
Benzobfluoranthene ND ug/kg 370 1.1 03/24/05 1547 BET 205-99-2
Benzoaanthracene ND ug/kg 370 1.1 03/24/05 1547 BET 56-553
Benzoic acid ND ug/kg 1800 1.1 03/24/05 1547 BET 65850
Benzoghiperylane ND ug/kg 370 1.1 03/24/05 1547 BET 191242
Benzyl alcohol ND ug/kg 740 1.1 03/24/05 1547 BET 100-51-6
Benzoapyrene ND ug/kg 370 1.1 03/24/05 1547 BET 50328
4-Bromophenylphenyl ether ND ug/kg 370 1.1 03/24/05 1547 BET 101-55-3
Butylbenzylphthalate ND ug/kg 370 1.1 03/24/05 1547 BET 85-687
4-Chloro-3-methylphenol ND ug/kg 740 1.1 03/24/05 1547 BET 59-507
4-hloroani1ine ND ug/kg 740 1.1 03/24/05 1547 BET 106478
his 2-chloroethoxymethane ND ug/kg 370 1.1 03/24/05 1547 BET 111-91-1
bis2-Chloroethyl ether ND ug/kg 370 1.1 03/24/05 1547 BET 11144-4
bis2-hloroisopropyl ether ND ug/kg 370 1.1 03/24/05 1547 BET 39638329
2-Chloronaphthalene ND ug/kg 370 1.1 03/24/05 1547 BET 91-587
2-Chlorophenol ND ug/kg 370 1.1 03/24/05 1547 BET 95-578
4-Chiorophenyiphenyl ether ND ug/kg 370 1.1 03/24/05 1547 BET 7005-72-3
Chrysene ND ug/kg 370 1.1 03/24/05 1547 BET 218019
Dibenzahanthracene ND ug/kg 370 1.1 03/24/05 1547 BET 53703
Dibenzofuran ND iig/kg 370 1.1 03/24/05 1547 BET 132649
12-Dichlorobenzene ND ug/kg 370 1.1 03/24/05.1547 BET 95-501
13-Dichiorobensexie ND ug/kg 370 1.1 03/24/05 1547 BET 54173-1
14-Dichlorobenzena ND ug/kg 370 1.1 03/24/05 1547 BET 106-46-7
33Dichlorobenzidine ND ug/kg 740 1.1 03/24/05 1547 BET 91941
24-Dichlorophenol ND ug/kg 370 1.1 03/24/05 1547 BET 120832
Diethylphthalate ND ug/kg 370 1.1 03/24/05 1547 BET 84662
24Dimethyiphenol ND ug/kg 370 1.1 03/24/05 1547 BET 105679
Dimethylphthalate ND ug/kg 370 11 03/24/05 1547 BET 131-11-3
Di-n-butylphthalate ND ug/kg 370 1.1 03/24/05 1547 BET 84-742
46-Dinitro-2-methylpheno ND ug/kg 370 11 03/24/05 1547 BET 534-52-1
Qi.Fceglant
Page 28 of 79Oate03/29/05
Pace Analytical Serilces Inc
9800 KinceyAvenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID Weet End 6228-05-2694
Lab Sample No 925409690
Client Sample ID 9567-2
Project Sample Number 9290353016
Matrix Soil
Date Collected 03/18/05 1110
Date Received 03/18/05 1525
catinID
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in tell
without the written consent of Pace MaIytica Services Inc
Charlotte Certiticatton IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
wrn.pacIabccsm
51285
121-142
6062Q2
117840
122667
117 -81-7
2064408737
87683
11874-1
77474
Results Units Report Limit Analyzed By CAB No QL ReaList
24Dinitrophenol ND ug/k 1800 1.1 03/24/05 1547 BET
24Dinitrotoluene ND ug/kg 370 1.1 03/24/05 1547 BET
26Dinitrotoluene ND ug/kg 370 1.1 03/24/05 15o47 BET
Di-n-octylphthalate ND ug/kg 370 1.1 03/24/05 1547 BET
l2Diphenylhydrazjne ND ug/kg 370 1.1 03/24/05 1547 BET
bis2-Ethylhexylphthalate ND ug/kg 370 1.1 03/24/05 1547 BET
Fluoranthane ND ug/kg 370 1.1 03/24/05 1547 BET
Fluorene ND ug/kg 370 1.1 03/24/05 1547 BET
Heicachloro-13-butadjene ND ug/kg 370 1.1 03/24/05 1547 BET
Hexachlorobenzene ND ug/kg 370 1.1 03/24/05 1547 BET
Rexachlorocyclopentadjene ND ug/kg 370 1.1 03/24/05 1547 BET
Raxachloroethane ND ug/kg 370 1.1 03/24/05 1547 BET 67721
Indeno123-cdpyrene ND ug/kg 370 1.1 03/24/05 1547 BET 193-39-5
Isophorone ND ug/kg 370 1.1 03/24/05 1547 BET 78591
2-Methylnaphthalene ND ug/kg 370 1.1 03/24/05 1547 BET 91-576
2-Methylphenol oCresol ND ug/kg 370 1.1 03/24/05 1347 BET 95-487
34Methylphenol ND ug/kg 370 1.1 03/24/05 1547 BET
Naplithalene ND ug/kg 370 1.1 03/24/05 1547 BET 91-203
2Nitroaniline ND ug/kg 1800 1.1 03/24/05 1547 BET 88744
3Nitroaniline ND uglkg 1800 1.1 03/24/05 1547 BET 99092
4Nitroaniline ND nc/hg 1800 1.1 03/24/05 1547 BET 100-01-6
Nitrobenzene ND ug/kg 370 1.1 03/24/05 1547 BET 98-953
2Nitrophenol ND ug/kg 370 1.1 03/24/05 1547 BET 88-755
4-Nitrophenol ND ug/kg 1800 1.1 03/24/05 1547 BET 10002-7
N-Nitroso-di-n-prolamjne ND ug/kg 370 1.1 03/24/05 1547 BET 621-64-7
N-Nitrosodiphenylamjne ND ug/kg 370 1.1 03/24/05 1547 BET 86-306
Peutacohlorophenol ND ug/kg 1800 1.1 03/24/05 1547 BET 87-865PhenanthreneNDugfkg3701.1 03/24/05 1547 BET 85-018
Phenol ND ug/kg 370 1.1 03/24/05 1547 BET 108952
Pyrene ND ug/kg 370 1.1 03/24/05 1547 BET 129000
124-Trichlorobanzerxe ND ug/kg 370 1.1 03/24/05 1547 BET 120-82-1
245-Trichlorophenol ND ug/kg 370 1.1 03/24/05 1547 BET 95-954
246-Trjchlorophanol ND ug/kg 370 1.1 03/24/05 1547 BET 88-062Nitrobenzened5561.0 03/24/05 1547 BET 4165600
2-Fluorobiphenyl 54 1.0 03/24/05 1547 BET 32160-8Terphenyld14CS761.0 03/24/05 1547 BET 171851-0Phenold5601.0 03/24/05 1547 BET 4165622
2-Fluorophenol 55 1.0 03/24/05 1547 BET 367124246-Trjbromophanol CS 65 9o 1.0 03/24/05 1547 BET
Page 29 of 79
Date 93/29/05
Analyticalwwpetabcnm
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
Lab Project Nuber 9290353
Client Project ID West End 622805-2694
Lab Sample No 925409690
Client Sample ID 9567-2
Project Sample Nuthher 9290353016
Matd.x Soil
Date Collected 03/18/05 1110
Date Received 03/18/05 1525
Date Extracted
GC Semivo.atiles
EPE in Soil by Mass Method
Aliphatic C09-C18
Aliphatic C19-C36
Aromatic Cll22
2-Fluorobiphenyl
2-Eromonaphthalene
Nonatriacontane
o-Terhenyl
Date Extracted
11 1.1 03/25/05 1038 EBB
11 1.1 03/25/05 1038 EBB
11 1.1 03/25/05 1038 EBS
1.0 03/25/05 1038 KBS
1.0 03/25/05 1038 KBS
1.0 03/25/05 1038 KBS
1.0 03/25/05 1038 EBB
03 /22/05
11 1.1 03/23/05 0113 DEW
11 1.1 03/23/05 0113 DHW
11 1.1 03/23/05 0113 DEW
1.0 03/23/05 0113 DEW
1.0 03/23/05 0113 DEW
32160
58013
7194867
84151
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services In
Ohnrlofle Certification IDs
NC Watitewater 12
NC Drinking Water 37706
Sc gg006
ft NELAP t87627
Units Report Limit UF Analyzed By CAB No QgL RecLmt
03/21/05 03/21/05
Prep/Method
ND
ND
ND
109
134
53
92
03/22/05
Method VPH
ND
ND
ND
111
114
Method EPA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
EPA 3550 EPH
mg/kg
mg/kg
mg/kg
nag/kg
nag/kg
mg/kg
8260
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
nag/kg
nag/kg
nag/kg
ug/kg
nag/kg
ug/kg
GC Volatiles
VPE in Soil by Mass Method
Aliphatic C05-C08
Aliphatic C09C12
Aromatic C09ClO
25-Dibronnotoluene PIDS
25-Dibromotoluene PID
GC/MS Volatiles
GC/MS VOCs 5035/8260 low level
Acetone
Benzene
Brcenobenzene
Bromochloromethane
Bromodichioronnethane
Bromoform
Bromonnethane
2-Butanone 1Z1c
n-Butylbenzene
sec-Buty.benzene
tert-Butylbenzene
Carbon tetrachioride
Chlorobenzene
Chloroethane
Chloroform
Chioromethane
Date 03/29/05
03/22/05 1045 RWS
03/22/05 1045 RWS
03/22/05 1045 RWS
03/22/05 1045 RWS
85
4.3
4.3
4.3
4.3
4.3
8.5
85
4.3
4.3
4.3
4.3
4.3
8.5
4.3
8.5
0.9
0.9
0.9
0.9
0.9
0.9
0.9
0.9
0.9
0.9
0.9
0.9
0.9
0.9
0.9
0.9
67 641
71432
108861
74975
75-274
75-252
74839
7893
104518
13598
98066
56235
108907
75-003
67 663
03 /22/05
03/22/05
03/22/05
03/22/05
03/22/05
03/22/05
03/22/05
03122/05
031 22/05
03/22/05
03/22/05
1045 RWS
1045 RWS
1045 RWS
1045 RWS
1045 RWS
1045 RWS
1045 RWS
1045 RWS
1045 RWS
1045 RWS
1045 RWS
03/22/05 1045 RWS 74873
Page 30 of 79
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Nurflber 9290353
Client Project ID West End 6228-05-2694
Lab Sample No 925409690
Client Sample ID 9567-2
Project Sample Nuinkber 9290353016
Natrix Soil
Date Collected 03/18/05 1110
Date Received 03/18/05 1525
-Chiorotoluene
4-Chiorotoluene
2-Dibromo-3-chloropropane
Dibrnoohloromethane
2-Dibrcanoethane 5DB
Dibramomethane
2-Dichiorobensene
3-Dichlorobenzene
4-Dichlorobenzene
Dichlorodifluoromethane
1-Dichloroethane
2-Diobloroethane
2.1 1-Dichloroethene
cis-12-Dichloroethene
trans-i 2-Diehioroethene
2-Dichloropropane
3-Dichloropropane
2-Dichloropropane
1-Dichioropropene
cia-i 3-Dichloropropene
trans-i 3-DicbJ.oropropene
Diisopropyi ether
Ethylbenzene
Hezachloro-1 3-butadiene
2-Bexanone
Isopropylbenzeae umene
p-Isopropyltoluene
I1ethylene chloride
4-Zdethyi-2-pentanone MIBI
Methyl-tert-butyl ether
Naphthalene
n-Propylbanzene
Styrene1112 -Tetrachloroethane
122-Tetrachioroetbane
Tetrachioroethene
Toluene123-Trichiorobeozena
124-Trichiorobeozene
Results tYnits
ND ugfkg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND uglkg
ND ug/kg
ND us/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND nag/kg
ND nag/kg
ND nag/kg
ND nag/kg
ND ug/kg
ND ug/kg
ND nag/kg
ND nag/kg
ND nag/kg
ND nag/kg
ND nag/kg
ND nag/kg
ND ug/kg
ND nag/kg
ND nag/kg
ND nag/kg
ND ug/kg
ND nag/kg
ND nag/kg
ND nag/kg
ND nag/kg
ND nag/kg
ND nag/kg
ND ug/kg
ND ug/kg
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/OS 1045 RWS
0.9 03122/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22105 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 PJi7S
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/03 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/OS 1045 RWS
0.9 03/22/05 1045 RWS
0.9 03/22/05 1045 RWS
9549 -8
106434
96128
124-48-i
106934
74..95..3
95501
541731
106467
75718
75343
107 062
7535-4
156592
156605
8-873
142289
594207
563586
10061015
1006102
108 203
10 0414
87683
391786
98 828
99876
75 092
108-101
163404
9120-3
10 3651
100425
630206
79 -345
127184
10 8883
8761-6
Ashevifte Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSiS
Tho report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certificajpjp
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NEI.AP E87627
Ztnalyzed By CIIS NoRenortLimitDF
4.3
4.3
4.3
4.3
4.3
4.3
4.3
4.3
4.3
8.5
4.3
4.3
4.3
4.3
4.3
4.3
4.3
4.3
4.3
4.3
4.3
4.3
4.3
4.3
43
4.3
4.3
4.3
43
4.3
4.3
4.3
4.3
4.3
4.3
4.3
4.3
4.3
Q3a1 RegLmt
Page of 79
Oats 03/29/05
4.3 0.9 03/22/03 1045 RWS 120821
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
I4untersville NC 28078
Phone [phone]
Fax [phone]
La Project Number 9290353
Client Project ID West End 6228-05-2694
Lab Sample No 925409690
Client Sample ID 9567-2
Project Sample Nuniber 9290353-016
latrix Soil
Date Collected 03/18/05 1110
Date Received 03/18/05
1525
Units Reioxt Limit DF Analyzed By CAB No QL RegLmt111-Trichloroethane
11 2-Trichioroethane
Trichloroethene
Trichlorofluorometane123-Trichloropropane124-Triinethylbenzene135-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene Total
mp-Xylene
o-Xylene
Toluene-d8
4-Bramofluorobenzene
Dibromofluoromathane
2-Dichloroethane-d4 Si
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND sag/kg
ND ug/kg
ND sag/kg
ND sag/kg
ND ug/icg
97
89
98
96
0.9 03/22/05
0.9 03/22/05
0.9 03/22/05
0.9 03/22/05
0.9 03/22/05
0.9 03/22/05
0.9 03/22/05
0.9 03/22/05
0.9 03/22/05
0.9 0/22/05
0.9 03/22/05
1.0 03/22/05
1.0 03/22/05
1.0 03/22/05
1.0 03/22/05
1045 RWS
1045 RWS
1045 RWS
1045 RWS
1045 RWS
1045 RWS
1045 RWS
1045 RWS
1045 RWS
1.045 RWS
1045 RWS
1045 RWS
1045 RWS
1045 RWS
1045 RWS
Asheville Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the wrttten consent of Pace Analytical Services Inc
Charlotte Certification lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
4.3 0.9 03/22/05 1045 RWS 71556
4.3
4.3
4.3
43
4.3
4.3
43
8.5
4.3
8.5
4.3
79005
79016
75694
96184
95636
108678
108054
75014
1330 20-7
5476
2037265
460-004
1868537
1706007
Date 03/29/05 Page 32 79
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID WeSt End 6228-05-2694
Lab Sample No 925409708
Client Sample ID 956733-4
Project Sample Number 9290353-017
Matrix Soil
Date Collected 03/18/05 1115
Date Received 03/18/05 1525
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
Method 9u Moisture
17.4
Asheville Ce lit icaticrnjfl
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
Ties report shall net be reproduced except in lull
without the written consent of Pace Analytical Services Inc
Charlotte Certification Dx
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP 87627
www.paCeIabs.eom
Ac 4-c Units Report Lixit _pj_Itinalvzed By CAS No QgL RegLmt
10 03/21/05 0852 TNS
GC/MS Semivo.atiles
Seinivolatile Organics Prep/Method EPA 3545 EPA 8270
Acenaphthene ND ug/kg 10000 30.2 03/25/05 0935 BET 83329
Acenaphthylene ow ug/kg 10000 30.2 03/25/05 0935 BET 208968
tnthraoene ND ug/kg 10000 30.2 03/25/05 0935 BET 120127
Benzokfluoranthene ND ug/kg 10000 30.2 03/25/05 0935 BET 20708-9
Benzobfliioranthene ND ug/kg 10000 30.2 03/25/05 0935 BET 205992
Benzoaanthracene ND uglkg 10000 30.2 03/25/05 0935 BET 56553
Benzoic acid ND ug/kg 50000 30.2 03/25/05 0935 BET 65850
Benzoghiperylexaa ND ug/kg 10000 30.2 03/25/05 0935 BET 191242
Benzyl alcohol ND ug/kg 20000 30.2 03/25/05 0935 BET 100516
Benzoapyrene ND ug/kg 10000 30.2 03/25/05 0935 BET 50328
4-Broinophenylphenyl ether ND uglkg 10000 30.2 03/25/05 0935 BET 101-55-3
Butylbenzylphthalate ND ug/kg 10000 30.2 03/25/05 0935 BET 85687
4-CAloro-3-methylphenol ND ug/kg 20000 30.2 03/25/05 0935 BET 59-507
4-Chloroaniline ND ug/kg 20000 30.2 03/25/05 0935 BET 106478
bis2-Chloroethoxymethane ND ug/kg 10000 30.2 03/25/05 0935 BET 111911
bis2Chloroethyl ether ND ug/kg 10000 30.2 03/25/05 0935 BET 111444
bis2Chloroisopropyl ether ND ug/kg 10000 30.2 03/25/05 0935 BET 39638329
2-Chloronapbthalerae ND ug/kg 10000 30.2 03/25/05 0935 BET 91587
2Chlorophenol ND ug/kg 10000 30.2 O3/25/05 0935 BET 95-578
4Chiorophenyiphenyl ether ND ug/kg 10000 30.2 03/25/05 0935 BET 7005-723
Chrysene ND ug/kg 10000 30.2 03/25/05 0935 BET 21801-9
Dibenzahanthracene ND ug/kg 10000 30.2 03/25/05 0935 BET 53703
Dibenzofuran ND ug/kg 10000 30.2 03/25/05 0935 BET 132649
l2Dichlorobenzene ND ugfkg 10000 30.2 03/25/05 0935 BET 95-501
13Dichiorobeuzene ND ug/kg 10000 30.2 03/25/05 0935 BET 541731
14-Dichlorobenzene ND nag/kg 10000 30.2 03/25/05 0935 BET 10646-7
33Dich1orobenzjdine ND ug/kg 20000 30.2 03/25/05 0935 BET 91941
24Dichlorophenol ND ug/kg 10000 30.2 03/25/05 0935 BET 120832
Diethylphthalate ND ug/kg 10000 30.2 03/25/05 0935 BET 84662
24Dimethyiphenol MD nag/kg 10000 30.2 03/25/05 0935 BET 105679
Dinuethylphthalate ND nag/kg 10000 30.2 03/25/05 0935 BET 131113
Dinbutylphthalate ND nag/kg 10000 30.2 03/25/05 0935 BET 84-742
46Dinitro2methylphenol ND nag/kg 10000 30.2 03/25/05 0935 BET 53452-1
Date 03/29/05 Page 33 of 79
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 622805-2694
Lab Sample No 925409708
Client Sample ID 9567-334
Project Sample Number 9290353-017
l4atriz Soil
Date Collected 03/18/05 1115
Date Received 03/18/05 1525
4-Dinitrophenol
4Dinitrotoluene
6-DinItroto.uane
Di-n-octylphthalate
12 -Diphenyihydrazine
his 2-Ethylhexylphthalate
Fluoranthene
Fluorene
Hexachloro-1 3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadjexie
Bexachloroethane
Indeno123-cdpyrene
Isophorone
-Methylnaphthalene
-Nethyiphenol o-Cresol
34-Methylphenol
Naphthalene
-Nitroanjljne
3-Nitroaniline
4-Nitroaniline
Nitrobeuzene
-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylainjne
Pentachioropheno
Phenanthrene
Phenol
Pyrene124-Trichlorobenzene245-Trichiorophenol246-Trichiorophenol
Nitrobenzene-d5
-Fluorobiphenyl
Terphenyl-d14
Phenol-aS
2-Fluoropheno
246-Tribromophenol
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
30.2 03/25/05 0935 BET
1.0 03/25/05 0935 BET
1.0 03/25/05 0935 BET
1.0 03/25/05 0935 BET
1.0 03/25/05 0935 BET
1.0 03/25/05 0935 BET
1.0 03/25/05 0935 BET
51285
121142
60620
11784-0
122667
117817
206440
86737
87683
118741
77-474
67721
193395
7859i
9157
.95487
9120
88744
99-092
100016
98953
88-755
10002
621647
86306
87 65
85-018
108952
129000
120821
95954
88-062
4165600
321608
1718510
4165622
367-124
Asheville Certification Os
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
Thin report shall est be reproduced accept in tul
wittiest the written censerit ef Pace Analytical Services Inc
Charlotte CertificahoiiIp
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
wpetebscorn
Results Dnit Report Limit ..ianalvzed By CAS No QiL RepLant
50000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
50000
50000
50000
10000
10000
50000
10000
10000
50000
10000
10000
10000
10000
10000
10000
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND tog/kg
ND tog/kg
ND tog/kg
ND ug/kg
ND tog/kg
ND ug/kg
ND ug/kg
ND tog/kg
ND ug/kg
ND tog/kg
ND tog/kg
ND tog/kg
ND tog/kg
ND ug/kg
ND tog/kg
ND ug/kg
ND tog/kg
ND tog/kg
ND tog/kg
ND tog/kg
ND tog/kg
ND tog/kg
ND up/kg
ND tog/kg
ND tog/kg
96
96
Date 03/29/05
345
345
345
345
345
345
Page 34 79
Pace Analylical Services Inc
9800 Kircey Avenue Suite 100
Huntersville NC 28078
Phone [phone]
Far 704.875.9091
Lab 9ro3ect Number 9290353
Client Project ID West End 622805-2694
Iaab Saorale No 925409708
Client Senle ID 956733-4
Project Sample Number 9290353-017
Matrix Soil
Date Collected 03/18/05 1115
Date Received 03/18/05 1525
GC Volatiles
VPH in Soil by Mass Method
Aliphatic C05-C08
Aliphatic C09-C12
Aromatic C09-C10
25-Dibromotoluene FID CS
25-Dibromotoluene PID
190 mg/kg
280 mg/kg
100 mg/kg
111
93
8.8 0.9 03/23/05 0326
8.8 0.9 03/23/05 03o26
8.8 0.9 03/23/05 0326
1.0 03/23/05 0326
1.0 03/23/05 0326
DEW
DEW
DEW
DEW
DEW
Asheville Certification IDe
NC Wastewater 40
NC Drinking Water 37712
Sc Environmental 99030
FLNELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall net be repmduccd except in tall
without the written consent of Pace Analytical Services Inc
Charlotte Certification Us
NC Wastewater 12
NC Drinking Water 7706
SC 99005
FL NaAp E57627
Date Extracted
GC Seinivolatiles
MPH in Soil by Mass Method
A.iphatic C09-C18
Aliphatie C19-C36
Aromatic C1122
2-Fluorobiphenyl
2-aromonaphthalene
Nonatriacontane
e-Terphenyl
Date Extracted
Results Units ReDort Limit DF Itnalvzed Mv CAS No QL RegLmt
03/21/05
Prep/Method
3800
3000
1700
796
1070
111
727
03/22/05
Method VPH
EPA 3550 EPH
mg/kg
mg/kg
mg/kg
03/21/05
60 6.0 03/24/05
60 6.0 03/24/05
60 6.0 03/24/05
1.0 03/24/05
1.0 03/24/05
1.0 03/24/05
1.0 03/24/05
03/22/05
1841 XES
1841 KBS
1841 IcES
1841 IcES
1841 IcES
1841 IcES
1841 IBS
GC/t4S Volati.es
GC/MS VOCs 5035/8260 low level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichlcromethane
Bromoform
Broseomethane
2-Butanorsa 0tt
n-Butylbenzene
sac-Butylbenzene
tert-Butylbenzene
Carbon tetrachioride
Chlorobenzene
Chioroethane
Chloroform
Chloromethane
Date 03/29/05
321608
580132
7194867
84-15i
67641
71432
108861
76975
75274
75-252
74-83
78 933
104-518
133988
98066
5623
108907
75-003
67663
74873
Method
ND
ND
ND
ND
ND
ND
ND
ND
14
11.
ND
ND
ND
ND
ND
ND
0.9 03/23/05 2144 RWS
0.9 03/23/05 2144 RWS
0.9 03/23/05 2144 RWS
0.9 03/23/05 2144 RWS
0.9 03/23/05 2144 RWS
0.9 03/23/05 2144 RWS
0.9 03/23/05 2144 RWS
EPA 8260
ug/kg
ng/kg
ug/kg
ng/kg
ug/kg
uglkg
us/kg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
nag/kg
92
4.6
4.6
4.6
4.6
4.6
9.2
92
4.6
4.6
4.6
4.6
4.6
9.2
4.6
9.2
0.9 03/23/05
0.9 03/23/05
0.9 03/23/05
0.9 03/23/05
0.9 03/23/05
0.9 03/23/05
0.9 03/23/05
0.9 03/23/05
0.9 03/23/05
2144 RWS
2144 RWS
2144 RWS
2144 RWS
2144 RWS
2144 RWS
2144 RWS
2144 RWS
2144 RWS
Page 35 of 79
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Huntersville NC 28078
Phone 704.8 75.U92
Fax [phone]
Lab Project Nuzitber 9290353
Client Project ID West End 6228-052694
Lab Sample No 925409708
Client Sample ID 9567334 Project Sample Number 9290353-017
Matrz Soil
Date Collected 03118105 1115
Date Received 03/18/05 1525
-Chiorotoluene
4-chlorotoluene
2-Dibromo-3-chloropropane
Dibrnochloromethane
12-Dibromoethane EDB
Dibromomethane
12-Dichlorobenzene
l3-Dichlorobenzene
4-Dichlorobenzene
Dichiorodifluoromethane
11-Dichloroethane
12-Dichioroethane
11 -Dichioroethene
cis-12-Dichloroethene
trana-1 -Diehioroethene
2-Dichioropropana
3-Dichloropropane
2-Dichloropropane
1-Dichloropropene
cia-i 3-Dichioropropene
trans-i 3-Dichioropropene
Diisopropyl ether
Ethylbenzene
Uexachloro-1 -butadiene
2-Hezanone
Isopropylbenzene Cumene
p-Iaopropyltoluene
Nethylene chloride
4-Nethyl-2-pentanone MIBE
Methyl-tert-butyl ether
Naptxthalene
n-Propylbenzene
Styrena11l2-etrachloroethane
1l22-Thtrachloroethane
Tetrachioroethene
Poluene123-rrichlorobenzene
124 -richlorobenzene
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 P3/PS
0.9 03/23/05 2144 RWS
0.9 03/23/05 2144 ENS
0.9 03123/05 2144 ENS
0.9 03/23/05 2144 RWS
0.9 03/23/05 2144 RNS
0.9 03/23/05 2144 ENS
0.9 03123/05 2144 ENS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 RWS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 P.WS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 EWS
0.9 03/23/05 2144 RWS
0.9 03/23/05 2144 RWS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 ENS
09 03/23/05 2144 ENS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 RWS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 ENS
0.9 03/23/05 2144 ENS
9549
106-43-4
96128
12448-1
10693-4
74-953
95-501
541-73-1
106-46-7
75718
7534
10706-2
75-354
156592
15660-5
7887
142-28-9
594207
563-58-6
10061015
10061026
108-20-3
100-41-4
87683
59178-6
9882
99-876
75092
10810-1
1634044
91203
103-65-1
100-42-5
63020-6
79-345
127-18-4
108883
87 -616
12082-1
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
ndac
Charlotte Certification Os
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
tw.pace1absoin
Eesults Units EeDort Limit DF isnalvzad By CAS No QL ReaLmt
ND us/kg 4.6
ND ug/kg 4.6
ND ug/kg 4.6
ND ug/kg 4.6
ND ug/kg 4.6
ND ug/kg 4.6
ND ug/kg 4.6
ND ug/kg 4.6
ND nag/kg 4.6
ND ug/kg 9.2
ND nag/kg 4.6
ND nag/kg 4.6
ND ugfkg 4.6
ND ug/kg 4.6
ND nag/kg 4.6
ND nag/kg 4.6
ND nag/kg 4.6
ND nag/kg 4.6
ND nag/kg 4.6
ND nag/kg 4.6
ND nag/kg 4.6
ND nag/kg 4.6
12 nag/kg 4.6
ND nag/kg 4.6
ND nag/kg 46
9.5 ug/kg 4.6
17 nag/kg 4.6
ND nag/kg 4.6
ND uglkg 46
ND uglkg 4.6
31 nag/kg 4.6
22 nag/kg 4.6
ND nag/kg 4.6
ND nag/kg 4.6
ND nag/kg 4.6
ND nag/kg 4.6
ND nag/kg 4.6
ND nag/kg 4.6
ND nag/kg 4.6
flate 03/29/05
Page 36 of 79
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
11 1-Trich.oroetljane
12-Trichioroethane
Trichioroethane
Trichlorofluoroinetbane
123 -Triabloropropane
124-Triinethylbenzene135-Trimathylbenzene
Vinyl acetate
Vinyl chloride
Xylene Total
asp-Xylene
o-Xylene
Toluene-dS
4-Bronrofluorobenzene
Dibromofluoroanathane
12-Dichloroetbane-d4 CS
0.9 03/23/05 2144 RWS
0.9 03/23/05 2144 RWS
0.9 03/23/05 2144 RWS
0.9 03/23/05 2144 flOPS
0.9 03/23/05 2144 flOPS
0.9 03/23/05 2144 fiwS
0.9 03/23/05 2144 flOPS
0.9 03/23/05 2144 RWS
0.9 03/23/05 2144 RWS
0.9 03/23/05 2144 RWS
0.9 03/23/05 2144 flOPS
0.9 03/23/05 2144 RWS
1.0 03/23/05 2144 RWS
1.0 03/23/05 2144 flOPS
1.0 03/23/05 2144 flOPS
1.0 03/23/05 2144 flOPS
CAB No QnL RegLmt
71556
79005
79016
75694
96184
95636
108678
108-05-4
75014
133 0207
9547
037-265
60-00-4
1868-537
170 60070
jfjjnDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E8764
REPORT OF LABORATORY ANALYSIS
This report shall riOt he reproduced eucept in lull
without the written consent of Pace Analytical Services Inc
Ctiarkttn Certification IDe
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
aeAnaIj4icar
mpacJabscono
Lab Sample No 925409708
Client Sample ID 9567334
Lab Project Number 9290353
Client Project ID West bid 622805-2694
Project Sample Nutinber 9290353-017 Date Collected 03/18/05 1115
Matrix Soil Date Received 03/18/05 1525
Results Units Report Limit
ND ug/kg 4.6
ND ug/kg 4.6
ND ug/kg 4.6
ND ug/kg 4.6
ND ug/kg 4.6
82 ug/kg 4.6
85 uglkg 4.6
ND ug/kg 46
ND ug/kg 9.2
16 uglkg 4.6
ND ug/kg 9.2
14 ug/kg 4.6
97
70 9s
107
109 Os
Pater 03/29/05 Page 37 of 79
Pace Analytical Sari/ices Inc
9800 KinceyAvenue Suite 100
Hunters yule NC 28078
FYione 704.875.9092
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Project Sample Number 9290353-018
Natrix Soil
Date Collected 03/18/OS 1130
Date Received 03/18/05 1525
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
Method Moisture
17.7
lJnits Report Limit _PE_
1.0 03/21/05 0852 TNS
CAS No QiL RegLmt
jnlD
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP 687648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inn
Charlotte Certification
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP t87827
wpacdabLcom
Lab Sasp1e No 925409716
Client Sample ID 9567378
GC/MS Sem.ivo.atiles
Semivolatile Organics Prep/Method EPA 3545 EPA 8270
Acenaphthene ND ug/kg 400 1.2 03/24/05 2357 BET 83329
Acenaphthylene ND ug/kg 400 1.2 03/24/05 2357 BET 208-96-8
Anthracexie ND ugfkg 400 1.2 03/24/05 2357 BET 120127
Benzokfluoranthene ND ugfk 400 1.2 03/24/05 2357 BET 207089
Benzobfluoranthexxe ND tag/kg 400 1.2 03/24/05 2357 BET 20599-2
Benzoaanthracexxe ND ugfkg 400 1.2 03/24/05 2357 BET 56-55-3
Benzoic acid ND nag/kg 2000 1.2 03/24/05 2357 BET 65850
Benzoghiperylene ND ug/kg 400 1.2 03/24/05 2357 BET 191-242
Bensyl alcohol ND ug/kg 800 1.2 03/24/05 2357 BET 100-516
Bexxzoapyrene ND nag/kg 400 1.2 03/24/05 2357 BET 50328
4-Bramophenylphenyl ether ND ug/kg 400 1.2 03/24/05 2357 BET 101-55-3
Butylberazylphthalate ND nag/kg 400 1.2 03/24/05 2357 BET 85-68-7
4-Chloro-3methylphenol ND nag/kg 800 1.2 03/24/05 2357 BET 59-50-7
4-Chioroaniline 8W nag/kg 800 1.2 03/24/05 2357 BET 106-47-8
bis2chloroethoxymethane ND nag/kg 400 1.2 03/24/05 2357 BET 111-911
bis2Chloroethyl ether ND nag/kg 400 1.2 03/24/05 2357 BET 111-444
bis2hloroiaopropyl ether ND ug/kg 400 1.2 03/24/05 2357 BET 3963832-9
2-Chloronaphtbalene ND ug/kg 400 1.2 03/24/05 2357 BET 91-587
2-Chloropheno3 ND ug/kg 400 1.2 03/24/05 2357 BET 95578
4-Chlorophenylphenyl ether ND nag/kg 400 1.2 03/24/05 2357 BET 7005-72-3
hrysene ND nag/kg 400 1.2 03/24/05 2357 BET 218-019
Dibenzahanthracene ND nag/kg 400 1.2 03/2.4/05 2357 BET 53-70-3
Dibenzofuran ND ugfkg 400 1.2 03/24/05 2357 BET 132-649
12-Dichlorobenzene ND ug/kg 400 1.2 03/24/05 2357 BET 95-501
13-Dichlorobenzene ND nag/kg 400 1.2 03/24/05 2357 BET 541-731
14-Dichiorobeazene ND nag/kg 400 1.2 03/24/05 2357 BET 106-467
33Dichlorobenzidjne ND nag/kg 800 1.2 03/24/05 2357 BET 91-941
24-Dichiorophenol ND ugfkg 400 1.2 03/24/05 2357 BET 120-83-2
Diethylphthalate ND nag/kg 400 1.2 03/24/OS 2357BET 84-662
24-DimethylpOzenol ND ug/kg 400 1.2 03/24/05 2357 BET 105-679
Dimethylphthalate ND ugfkg 400 1.2 03/24/05 2357 BET 131-11-3
Di-nbutylphthalate ND nag/kg 400 1.2 03/24/05 2357 BET 84-74-2
46-Dinitro-2-methylphenol ND nag/kg 400 1.2 03/24/05 2357 BET 534-52-1
Date 03129/05 Page 38 of 79
Pace Analytical Seriices Inc
9800 KinceyAvenue Suite 100
Huntersvills NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-052694
Lab Sample No 925409716
Client Sample ID 9567-37-8
24-Dinitrophenol
4-Dinitrotoluane
6-Dinitrotoluene
Di-noctylphthalate
2-Diphenylhydrazine
his 2-Ethy1hex-lphthalate
Fluorantixene
Pluorene
Bexachloro-l3-butadjene
Hexachiorobensene
Hexachlorooyclopentadj.ene
Hexachioroethane
Indeno1 23-cdpyrene
Isophorone
-Methylnaphthalene
2-Methylphenol o-Cresol
3a4-Methylphenol
Naphthalene
2-Nitroaniljne
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4Nitrophenol
N-Nitroso-di-n-propylanajne
N-Nitroaodiphanylaiaine
Pentachiorophenol
Phenanthrene
Phenol
Pyrene124-Trichlorobanzene
45-Tricxhlorophenol246-Trichlorophenol
Nitrobenzene-d5
2-Fluorobipheny
Terphenyl-d14
Phenol-d5 CS
2-Fluorophenol
246-Tribroanophenol
1.2 03/24/05.2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/.05 2357 BET
1.2 03/24/05 2337 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.2 03/24/05 2357 BET
1.0 03/24/05 2357 BET
1.0 03/24/05 2357 BET
1.0 03/24/05 2357 BET
1.0 03/24/05 2357 BET
1.0 03/24105 2357 BET
1.0 03/24/05 2357 BET
Date Collected 03/18/05 1130
Date Received 03/18/05 1525
51285
12114-2
606202
117840
12266
117 -81-7
206440
86737
87683
118-74-1
77474
67721
193395
8591
91576
9548
91203
88-744
99 092
100 016
8953
88755
100 027
621-64-7
86306
87 865
85018
108952
129000
120821
95954
88 062
4165600
321608
1718 -510
4165622
367-124
QiaL_ReLint
ionlDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the Written consent of Puce Analytical Services Inc
Charlotte Certification Os
NOWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E7627
Project Sample Number 9290353-018
Matrix Soil
Units Report Limit DF ra exsResults
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
52
59
78
45
34
44
2000
400
400
400
400
400
400
400
400
400
400
400
400
400
400
400
400
400
2000
2000
2000
400
400
2000
400
400
2000
400
400
400
400
400
400
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
ug/kg
ug/k
ug/kg
ug/kg
ug/kg
tag/kg
tag/kg
tag/kg
tag/kg
ug/kg
tag/kg
ug/kg
tag/kg
tag/kg
tag/kg
tag/kg
tag/kg
ug/kg
tag/kg
tag/kg
tag/kg
tag/kg
ug/kg
ug/kg
uglkg
tag/kg
ug/kg
Date 03/29/05 Page 39 of 79
1/aceAnaiyticar
Pace Analytical Sasvices Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
one 704875.9092
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Lab Samp.e No 925409716
Client Sample ID 9567-37-8
Project Sample Number 9290353-018
Matrix Soil
Date Collected 03/18/05 1130
Date Eaceived 03/18/05 1525
Date Extracted
GC Semivolatiles
EPE in Soil by Mass Method
Aliphatic C09C18
Aliphatic C19C36
Arcmatic C11-22
2-Fluorobiphenyl
2-Bromonaphthalene
Nonatriacontane
o-rerpheny1 CS
Date Extracted
03/21/05
TJnits Beport Limit DF Acalyzed BY CAS No RecxLmt
03/21/05
12 1.2 03/25/05 0912 IBS
12 1.2 03/25/05 0912 KBS
12 1.2 83/25/05 0912 IS
1.0 03/25/05 0912 KBS
1.0 03/25/05 0912 KBS
1.803125/05 0912 K.BS
1.0 03/25/05 0912 KBS
03/22/05
321608
58013
7194-86-7
84151
GC Volatiles
VPH in Soil by Mass Method
Aliphatic C05-C08
Aliphatic C09-Cl.2
Aconsatic C09-C10
25-Dibronaotoluene FID CS
25-Dibromotoluene PID
Method VPH
ND
ND
ND
105
109
mg/kg
mg/kg
mg/kg
10 1.0 03/23/05
10 1.0 03/23/05
10 1.0 03/23/05
1.0 03/23/05
1.0 03/23/05
0157 DHW
0157 DEW
0157 DEW
0157 DEW
0157 DEW
Date 03/29/05 Page 40 cC 79
fcationlD
NC Wastewter 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in tell
withoat the written consent of Pace Analytical Services Inc
Charlotte Certification ID
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
Prep/Method
ND
ND
ND
123
154
46
99
03 /.22/05
EPA 3550 EPH
mg/kg
mg/kg
mg/kg
GC/MS Volatiles
GC/NS VOCs 5035/8260 low level Method EPA 8260
Acetone ND ug/kg 110 1.1 03/22/05 1102 RWS 6764i
Benzene ND ug/kg 5.4 1.3 03/22/05 1102 RWS 71432
Bromobenzene ND ug/kg 5.4 1.1 03/22/05 1102 RWS 10886-1
Eromoclaloxomethane ND ug/kg 5.4 1.1 03/22/05 1102 RWS 74975
Broonodichloromgthane ND ug/kg 5.4 1.1 03/22/05 1102 RWS 75-27-4
Bromoform ND ug/kg 5.4 1.1 03/22/05 1102 RWS 75-252
Bromametharae ND ugfkg 11.1.1 03/22/05 1102 B.WS 74-839
2Butanone ND ug/kg 110 1.1 03/22/05 1102 RWS 78-933
n-Butylbenzene ND ug/kg 5.4 1.1 03/22/05 1102 RWS 104-51-8
secButylbenzene ND ug/kg 5.4 1.1 03/22/05 1102 EWS 135-98-8
tertButylberszene ND ug/kg 5.4 1.1 03/22/05 1102 RWS 98066
Carbon tetrachioride OW ug/kg 5.4 1.1 03/22/05 1102 RWS 56-23-5
Chlorobenzene ND ug/kg 5.4 1.1 03/22/05 1102 EWS 10890-7
Chloroethane ND ug/kg 11 1.1 03/22/05 1102 RWS 75003
h1oroform ND ug/kg 5.4 1.1 03/22/05 1102 RWS 67663
Chioromethane ND ug/kg 11 1.1 03/22/05 1102 RWS 74873
aeAnalYtical
wpazabsrrm
Pace Analytical Sariices Inc
9800 KinceyAvenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Lab Sample No 925409716
Client Sample ID 9567-37-8
-Chlorotoluene
4-Chlorotoluene
2-Dibromo-3-chloropropane
Dibchloroisethane
2-Dibromoethane EDB
Dibromoinethane
12 -Dichlorobenzene
13 Dichlorobenzene
4-Dichlorobenzene
Dichlorodifluoromethane
1-Dichioroethane
2-Dichioroethane
1Dichioroethene
cia-i 2-Dichioroethene
trans-i 2-Dichioroethene
12 -Dichioropropane
3-Dichioropropane
2-Dichloropropane
1-Dichloropropene
ciai 3-Dichioropropene
3-Dich1oroprpene
Diisopropyl ether
Ethylbenzene
Rezachioro-1 3-butadiene
2-Hecanone
Isopropylbenzane Cumene
p-Isopropyltoluene
t4ethylene chloride
4-Methyl-2-pentanone MIBK
Nethyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1112 -Tetrachloroethane1122-Tetrachlóroethane
etrach1oroethena
Loluene
123 -Trichlorobenzene
124 -Trichlorobenzene
Project Sample Number 9290353-018
Natriz Soil
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RWS
11 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RiPS
5.4 1.1 03/22/05 1102 RiPS
5.4 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/OS 1102 RWS
54 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RiPS
5.4 1.1 03/22/05 1102 RiPS
5.4 1.1 03/22/05 1102 RiPS
54 1.1 03/22/05 1102 RWS
5.4 1.1 03/22/05 1102 RiPS
5.4 1.1 03/22/05 1102 RiPS
5.4 1.1 03/22/05 1102 RiPS
5.4 1.1 03/22/05 1102 RiPS
5.4 1.1 03/22/05 1102 RiPS
5.4 1.1 03/22/05 1102 RiPS
5.4 1.1 03/22/05 1102 RiPS
5.4 1.1 03/22/05 1102 RiPS
5.4 1.1 03/22/05 1102 RiPS
5.4 1.1 03/22/05 1102 RiPS
Date Collected 03/18/05 1130
Date Received 03/18/05 1525
QL RegLint
95-498
106434
6128
124-481
106-93-4
74953
95501
541731
1064.67
75-718
75343
107 62
7535
156-59-2
15660
78875
142-289
59420
563586
1006101S
10061026
108203
100414
87683
591786
9882
99876
7509
108101
1634-044
9120
10365i
100425
630-206
79345
127-184
108883
87616
120821
Ashevite Certification IDs
NC Wastawater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be repmduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certification Do
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP f87627
Units Report LimitResults
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ugikg
uglkg
ug/kg
tog/kg
ug/kg
tog/kg
tog/kg
tog/kg
tog/kg
tog/kg
tog/kg
tog/kg
ug/kg
ug/kg
ug/kg
ug/kg
tog/kg
ug/kg
ug/kg
tog/kg
uglkg
ug/kg
tog/kg
tog/kg
ug/kg
tog/kg
tog/kg
tog/kg
tog/kg
tog/kg
tog/kg
tog/kg
tog/kg
tog/kg
tog/kg
ug/kg
tog/kg
tog/kg
tog/kg
Date 03/29/05 Page 41 of 79
Analytical
s.v.par.eiaba.corn
Pace Analytical Services Inc
9800 KirzceyAvenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Project Nuiæber 9290353
Client Project ID West End 6228-05-2694
Lab Sample No 925409716
Client Sample ID 9567378 Project Sample Number 9290353-018
Natrix Soil
Date Collected 03/18/05 1130
Date Received 03/18/05 1525
ll-Trichloroethane
112 -Tricliloroethane
Trichioroethene
Trichlorofluoroiaethane123-Trichloropropane124-Trimethylbenzene135-Trinaethylbenzene
Vinyl acetate
Vinyl chloride
Xylene Total
mp-Xylene
o-Xylene
Toluene-d8
4-Brounofluorobeuzene
Dibrounofluoromethane
12-Dichloroethane-d4
Results Tjnits ReDort Limit
ND ug/kg 5.4 1.1
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
96
94
94
88
1.3 03/22/05 1102 RES
1.1 03/22/05 1102 RWS
1.1 03/22/05 1102 RWS
1.1 03/22/05 1102 RWS
1.3 03/22/05 1102 RWS
1.3 03/22/05.1102 ENS
1.1 03/22/05 1102 ENS
1.3 03/22/05 1102 RWS
1.1 03/22/05 1102 RWS
1.3 03/22/05 1102 ENS
1.1 03/22/05 1102 ENS
1.0 03/22/05 1102 RWS
1.0 03/22/05 1102 ENS
1.0 03/22/05 1102 RWS
1.0 03/22/05 1102 ENS
Asheville Certiftcation IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Chaiiotte Certification lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E7627
analyzed By CAS No ReLmt
03/22/05 1102 ENS 71556
5.4
5.4
5.4
5.4
5.4
5.4
54
11
5.4
11
5.4
79005
7901
75694
96184
95636
108678
108054
75014
1330-207
95476
2037265
460004
1868-53-7
17060070
Date 03/29/05 Page 42 79
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228052694
Wet chemistry
Percent Moisture
Percent Moisture
Method 9u Moisture
19.7
Units Report Limit DF Maalvzed By CAS No QBEL RegLnat
1.0 03/21/05 0853 TNS
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
83329
208968
120127
207089
205992
56-553
65850
191242
100516
50328
101553
85687
59507
106478
111911
111444
39638329
91587
95-578
7005-72-3
218019
53703
132649
95501
541731
106467
91941
120832
84662
10567
131113
84742
53452
IlificationID
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E8Th48
REPORT OF LABORATORY ANALYSIS
This report shall not be reprnduced except in full
wfthout the wrttten consent of Pace Analytical Services Inc
Ctiatlcntte CertiticatiopJ
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP 87627
wspeneabcrn
Lab Saia1e No 925409724
Client Sanle XD 9567-1
Project Sample Number 9290353-019
Matrix Soil
Date Collected 03/18/05 1100
Date Received 03/18/05 1525
GC/MS Semivolatiles
Seanivolatile Organics Prep/Method EPA 3545 EPA 8270
Acenaphthene ND ug/kg 410
Acenaphthylene ND ug/kg 410
Zanthracene ND ug/kg 410
Benzokfluoranthene ND ug/kg 410
Benzobfluoranthene ND ug/kg 410
Benzoaanthracene ND ug/kg 410
Benzoic acid ND ugfkg 2100
Benzoghiperylene ND ug/kg 410
Benzyl alcohol ND ug/kg 820
Benzoapyrene ND ug/kg 410
d-Brconophanylphenyl ether ND ug/kg 410
Butylbenzylphthalate ND ug/kg 410
4-Chloro-3-methylphenol ND ug/kg 820
4-Chloroanjlina ND ug/kg 820
his 2-Chloroethoxymethans ND ug/kg 410
bis2-Chloroethyl ether ND nag/kg 410
bis2-Cbloroisopropyl ether ND nag/kg 410
2-Chloronaphthalene ND nag/kg 410
2-Chlorophano ND ug/kg 410
4-Chlorophenylphenyl ether ND nag/kg 410
Chrysene ND ug/kg 410
Dibenzahanthracene ND nag/kg 410
Dibenzofuran ND nag/kg 410
l2-Dichlorobenzene ND ug/kg 410
l3-Diclalorobenzene ND nag/kg 410
l4-Dichlorobeuzene ND ug/kg 410
33-Dichlorobenzidine ND ug/kg 820
24-Diohloropheno ND nag/kg 410
Diethylphtha.ate ND ug/kg 410
24-Dixaethy1phaol ND nag/kg 410
Dimethylphthalate ND ug/kg 410
Di-n-butylphthalate ND nag/kg 410
416-Dinitro-2-nnethylphenol ND nag/kg 410
0140 BET
0140 BET
0140 BET
0140 BET
0140 BET
0140 BET
0140 BET
0140 BET
0140 BET
0140 BET
0140 BET
0140 BET
0140 BET
0140 BET
0140 BET
0140 BET
0140 BET
0140 BET
0140 BET
0140 BET
Date 03/29/05
Page 43 of 79
Pace Analytical Serlic8s Inc
9800 KinceyAvenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Sample No 925409724
Client Sale XD 9567-1
Project Sample Nuiüber 9290353Oi.9
Natriz Soil
Date Collected 03/18/05 1100
Date Received 03/18/05 1525
24-Dinitrophenol
4-Dinitroto.uene
6-Dinitrotoluene
Di-n-octylphthalate
l2-Diphenylhydrazjne
bis 2-Ethylhexyl phtbalate
Oluoranthene
Fluorene
liexachloro-1 3-butadiene
Hexachlorobenzene
Hexachlorocyclopexutadiene
Hexachloroethane
Indeno12 3-cdpyrene
Isophorone
2-Nethylruaphthalene
2-Methylphenol o-Cresol
34-Z4ethylphenol
Naphthalene
2-Nitroanjljne
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamjne
N-Nitrosodiphenyljne
Pentachlorophenol
Phenanthrene
Phenol
Pyene
24-Trichlorobenzene245-Trichlorophenol246-Tricklorophenol
Nitrobenzene-d5
2-Pluorobiphenyl IS
Terphenyl-d14
Phenol-d5
2-Fluorophenol
246-Tribromophenol
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2 03/25/05
1.2
1.2
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.2 03/25/05 0140 BET
1.0 03/25/05 0140 BET
1.0 03/25/05 0140 BET
1.0 03/25/05 0140 BET
1.0 03/25/05 0140 BET
1.0 03/25/05 0140 BET
1.0 03/25/05 0140 BET
77-474
67721
193395
78591
91576
95-487
91-203
88744
99092
100016
98953
88755
10002-7
62164-7
86306
87865
85018
108952
12900-0
120821
95-954
88-062
4165600
32160-8
1/18-510
4165622
367-12-4
jonIDs
NC Wastwater 40
NC Drinking Water 37712
Sc Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in lull
without the written consent of Pace Analytical Services Inc
Charlotte Certification lls
FdCWastewater 12
tIC Drinking Water 37706
SC 99006
FL NELAP E87627
..2eAriaIyt/ca/
Lab Project Number 9290353
Client Project ID West End 622805-2694
Units ReDort Limit DF na1vzed NV CAS No ReaLint
1.2 03/25/05 0140 BET 51285
1.2 03/25/05 0140 BET 121142
0140
0140
0140
0140
0140
01 40
BET 606-202
BET 117-84-0
BET 122667
BET 117817
BET 206440
BET 86737
03/25/05 0140 BET 87683
03/25/05 0140 BET 118741
Results
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
35
38
83
24
12
23
2100
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
2100
2100
2100
410
410
2100
410
410
2100
410
410
410
410
410
410
ug/kg
up/kg
up/kg
up/kg
ug/kg
ug/kg
up/kg
up/kg
up/kg
up/kg
up/kg
up/kg
up/kg
up/kg
up/kg
up/kg
up/kg
ug/kg
up/kg
up/kg
up/kg
up/kg
ug/kg
ug/kg
up/kg
ug/kg
up/kg
up/kg
up/kg
up/kg
up/kg
up/kg
up/kg
St
St
Date 03/29105
10
Page 44 79
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Lab Sample No 925409724
Client Sample ID 9567-1
Date Extracted 03/21/05
12 1.2 03/25/05 0955 XBS
12 1.2 03/25/05 0955 EBS
12 1.2 03/25/05 0955 KBS
1.0 03/25/05 0955 321608
1.0 03/25/05 0955 ENS 580132
1.0 03/25/05 0955 EBB 7194867
1.0 03/25/05 0955 EBB 84-151
03/22/05
eii5ationIfln
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSiS
This report shall net be reproduced except in full
without the written consent of Pace Analytical Services Inc
Chailoftn Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
wwpace1absccrn
Paraoneters Results Units Regort Limit _p
Project Sample Number 9290353019
Matrix Soil
Date Collected 03/18/05 1100
Date Received 03/18/05 1525
Analyzed Nv CAB No Qp RemLmt
03/21/05
Prep/Method
ND
ND
ND
100
128
43
91
03/22/05
Method VPH
ND
ND
ND
105
112
EPA 3550 BPS
mg/kg
mg/kg
mg/kg
ye
mg/kg
mg/kg
mg/kg
GC Semivolatiles
EPE in SQl by Mass Method
Zhliphatic C09-C18
Aliphatic Cl9C36
Aromatic Cl1-22
2-Fluorobiphenyl
2-Bromonaphthalene
Nonatriacontane
o-Terphenyl
Date Extracted
GC Volatiles
VPH in Soil by Mass Method
Aliphatic C05-C08
Aliphatic C09-Cl2
Aromatic C09Cl0
25-Dibromatoluene FID
25-Dibromotoluene PIDS
GC/MS Volatiles
GC/MB VOCS 5035/8260 low level
Acetone
Benzene
Bromobenzene
Bromochiaromethane
Brainodichloromathane
Bromoform
Bromomethane
-Butanone bK
n-Butylbenzene
sec-Butylbenzene
tart -Butylbenzene
Carbon tetrachloride
Chiorobensena
Chioroethane
Chloroform
Chloransathane
Date 03/09/05
9.6 1.0
9.6 1.0
9.6 1.0
1.0
1.0
03/23/05
03 /23/05
03 /23/05
03/23/05
03/23/05
Method
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
EPA 8260
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0242 DEW
0242 DEW
0242 DEW
0242 DEW
0242 DEW
2137 RWS
2137 RWS
2137 RWS
2137 RWS
2137 RWS
2137 RWS
2137 RWS
2137 RWS
2137 RWS
2137 RWS
2137 RWS
2137 RWS
2137 RWS
2137 EWS
2137 RWS
2137 RWS
94
4.7
4.7
4.7
4.7
4.7
9.4
94
4.7
4.7
4.7
4.7
4.7
9.4
4.7
9.4
0.9 03/22/05
0.9 03/22/05
0.9 03/22/05
0.9 03/22/05
0.9 03/22/05
0.9 03/22/05
0.9 03/22/05
0.9 03/22/05
0.9 03/22/05
0.903/22/05
0.9 03/22/05
0.9 03/22/05
0.9 03/22/05
0.9 03/22/05
0.9 03/22/05
0.9 03/22/05
67-641
71432
108861
74-975
75274
75252
7483
78933
104518
135988
98066
56-235
108907
75003
67663
7487
Page 45 79
2eAnaIyticaI
Pace Analytical Sarices inn
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Lab Sale No 925409724
Client Sample ID 9567-1
Project Sample Number 9290353019
Matrix Soil
Date Collected 03/18/05 1100
Date Received 03/18/05 1525
-chiorotoluene
4-Chiorotoluene
i2-Dibromo-3-chloropropane
Dibroxnochlorcnuethane
2-Dibromoethane EDB
Dibromoniathane
3.12 -Dichlorobenzene
13 -Dichlorobenzene
4-Dichlorobenzene
Dichlorodifluoxnethane
11-Dichloroethane
12-Dichloroethazie
l-Diehioroethene
cis-l2-Dichloroethene
trans-i2-Dichloroethene
2-Dichloropropane
3-Dichloropropaue
2-Dichloropropane
1-Dichloropropene
cis-1 3-Dichloropropene
trans-i3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1 3-butadiene
2-Hexanone
Xsopropylbenizana Cumene
p-Isopropyltoluene
Methylane chloride
4-Methyl-2-pentanone MIB1
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene1112 Tetrachloroethane1122etrachloroethene
Tetrachloroethene
Toluene
123 -Trichlorobanzene
124 -Trichlorobenzena
Analyzed By
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 MS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 MS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 EMS
0.9 03/22/05 2137 ENS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 ENS
0.9 03/22/05 2137 MOPS
0.9 03/22/05 2137 ENS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 EMS
0.9 03/22/05 2137 ENS
0.9 03/22/05 2137 ENS
0.9 03/22/05 2137 MOPS
0.9 03/22/05 2137 ENS
0.9 03/22/05 2137 ENS
0.9 03/22/05 2137 ENS
0.903/22/05 2137 RWS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 ENS
0.9 03/22/05 2137 ENS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 RWS
0.9 03/22/05 2137 RWS
CAS No QisL ReLmt
106434
96128
124481
106934
74953
95501
541731
106467
75718
75343
107062
75354
15 6592
156605
78875
142289
594207
563-586
10061015
10061026
108-203
100-41-4
87683
591-786
98828
99876
75092
10810i
1634044
91203
103-65i
100425
63 0206
79345
127184
108883
87616
120-82i
leCejcafjonIDs
NC Wastewater 40
NC Drinking Water 37112
SC Environmentel 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduceni except
in lull
without the written consent at Pane Analytical Servlczs Inc
clutlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
Units Report Limit _P.__
4.7 0.9 03/22/05 2137 MS 95498NDug/kg
ND ug/kg 4.7
ND ug/kg 4.7
ND ug/kg 4.7
ND ugikg 4.7
ND ug/kg 4.7
ND uglkg 4.7
ND ug/kg 4.7
ND ugfkg 4.7
ND ug/kg 9.4
ND ug/kg 4.7
ND ug/kg 4.7
NO ug/kg 4.7
ND tag/kg 4.7
ND ug/kg 4.7
ND tag/kg 4.7
ND tag/kg 4.7
ND tag/kg 4.7
ND tag/kg 4.7
ND tag/kg 4.7
ND tag/kg 4.7
ND tag/kg 4.7
ND tag/kg 4.7
ND ugikg 4.7
ND tag/kg 47
ND ug/kg 4.7
ND tag/kg 4.7
ND tag/kg 4.7
ND tag/kg 47
ND tag/kg 4.7
ND tag/kg 4.7
ND tag/kg 4.7
ND tag/kg 4.7
NO ug/kg 4.7
ND tag/kg 4.7
ND tag/kg 4.7
ND ug/kg 4.7
ND tag/kg 4.7
ND tag/kg 4.7
Data 03/29/05 Page 46 cC 79
Lab Sample No 925409724
Client Sample ID 9567-1
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunters villa NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West P.nd 6228-05-2694
Project Sample Number 9290353019
Natrix Soil
11 1-richloroethane112-rrichloroethane
rich1oroethene
Trichiorofluorosnethane123-richloropropane124-Trimethylbenzane135-Triinethylbenzene
Vinyl acetate
Vinyl chloride
Xylene rotal
mp-Xylene
o-Xylene
Toluene-d8
4-Brosnofluorobenzene
Dibromofluoramethane
l2-Dichloroethane-d.4
4.7 0.9 03/22/05 2137 RWS
4.7 0.9 03/22/05 2137 RWS
4.7 0.9 03/22/05 2137 RWS
4.7 0.9 03/22/05 2137 RWS
4.7 0.9 03/22/05 2137 RWS
4.7 0.9 03/22/05 2137 RWS
47 0.9 03/22/05 2137 RWS
47 0.9 03/22/05 2137 RWS
9.4 0.9 03/22/05 2137 RWS
4.7 0.9 03/22/05 2137 ENS
9.4 0.9 03/22/05 2137 RWS
4.7 0.9 03/22/05 2137 RWS
1.0 03/22/05 2137 RWS
1.0 03/22/05 2137 RWS
1.0 03/22/05 2137 RWS
1.0 03/22/05 2137 ENS
71556
79005
79016
75694
6184
5636
108678
10805-4
75014
1330-207
9547
2037-265
460004
1868-537
17060070
Asheville Certification lOs
NC Wastewater 40
NC brinking Water 37712
Sc Environmental 99030
FL WELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in lull
without the written consent of Pace Analytical Services Inc
hprlot1e Certification lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NAP E87027
Dnnmaf are
ND ug/kg
Results Units Report Limit fl
Date Collected 03/18/05 1100
Date Received 03/18/05 1525
Analyzed By CAS No
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
93
86
108
113
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
99
99
2B_ReaLmt
Page 47 79
Date 03/29/05
MalyikarwpaLom
PJRAMETER FOOTNOTES
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Ilunfersville NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-052694
Dilution factor shown represents the factor applied to the reported result and reporting limit due to changes
in sample preparation dilution of the extract or
moisture content
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic
testing was performed at our Pace Charlotte laboratory unless otherwise footnoted
Method 90715 modified to use ASE
All pK Pree Chlorine total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate
hold time
ND Not detected at or above adjusted reporting limit
NC Not Calculable
Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
NDL Adjusted Method Detection Limit
Surrogate
13 Common laboratory contaminant
23 Surrogate recovery outside of control limits The data was accepted based on valid recovery of remainingsurrogate
Surrogate standards were not recovered due to sample dilution
14 The sample extract could not be concentrated to the normal final volume This resulted in an elevated
reporting limit
The sample was diluted to reduce matrix interference resulting in elevated reporting limits
The surrogate recovery was outside QC acceptance limits due to matrix interference
The reported result may be biased high due to matrix interference with the internal standard This wasconfirmedbyreanalysisof the sample
Low surrogate recovery was confirmed as matrix effect by second analysis
The surrogate recovery was above the QC recovery limit The sample was not re-extracted since no targetanalytesweredetectedinthesample10Acidsurrogaterecoveryoutside of control limits The data was accepted based on valid recovery of the two
remaining acid surrogates
Date 93/29/05 PaSe 48 of 79
shev8le Certification IDs
NC Wastewater 40
NC Drinking Water 37712
Sc Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in lull
without the written consent of Pace Analytical Services Inc
41thct
itlcttn Certification IDs
NC Wastewater 12
NO Drinking Water 37706
SC 99006
FL NELAP E87627
QUALITY CONTROL DATA
Pace Analytical Ser/ices Inc
9800 KinceyAvenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax[phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
QC Batch 123887 Analysis Method EPE
QC Batch Method EPA 3550 Analysis Description EPE in Soil by Mass Method
Associated Lab Samples 925409500 925409518 925409534
lIROD BLANK 925411803
Associated Lab Samples 925409500 925409518 925409534
Blank ReportingParameterUnitsResultLimit Footnotes
Aliphatic C09-C18 mg/kg ND 10
Ai.iphatic C19-C36 mg/kg ND 10
Aromatic Cll-22 mg/kg ND 10
2-Fluorobiphenyl 112
2Bromonaphthalene 113
Nonatriacontane 104
o-Terphenyl 117
LABORATORY CO9ROL SAMPLE 925411811
Spike LCS LCSParameterUnitsConcResultRec Footnotes
Aliphatic C09C18 mg/kg 10.00 9.193 92
Aliphatic C19C36 mg/kg 13.33 12.16 91
Aromatic C1122 mg/kg 28.33 24.27 86
2-Fluorobiphenyl 74
2-Brcmonaphthalene 47
Nonatriacontane 118
o-Terphenyl 109
MATRIX SPIIE MATRIX SPIKE DUPLICATE 925411829 925411837
eriliicationID
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
ttarictte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELP.P E87627
wWEpace1bsom
Parameter
Aliphatic C09-C18
Aliphatic C19-C36
Aromatic C1122
2-Fluorobiphenyl
2-Bromonaphthalene
Date 03/29/05
925404717 Spike MS NSD
Units Result Conc Result Result
mg/kg 19.05 12.18 8.740 10.90
mg/kg 4.597 16.24 11.51 13.73
mg/kg 8.174 34.51 31.59 23.06
MS MSD
Rec tv Rec
43 56
68 43
104 86
110 89
RPD
22
18
31
Footnotes
11
Page 49 of 79
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 KinceyAvenue Suits 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228052694
MiTRIX SPlicE TRIX SPIKE tWLICATE 925411829 925411837
925404717 Spike MS MSD MS MSD
Parameter Units Result Conc Result Result 9aRec Rec RPD Footnotes
Nonatriacontane 76 87
o-Terphenyl 95 76
SAiLE DUPI.ICTE 925411845
cationlD
NC Wastewater 40
NC Drinking Water 37712
SC EnvironnTental 99030
FLNELAP E87648
REPORT OF LABORATORY ANALYSIS
This report ohall et be reproduced except
in full
without the wiitten consent of Pace Analytical SeMces Inc
Chailotte Certification Do
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
wiwpaeIabscom
925404733 DUP
Parameter Units Result Result
Aliphatic C09C18 mg/kg 68.00 63.00
Aliphatic C19C36 nig/kg 19.00 21.00
rnatic C11-22 mg/kg 25.00 31.00
2-Fluorobiphenyl 119 116
2-Bromonaphthalene 171 191
Nonatriacontane 110 98
o-Perpheny1 114 107
RPD
24
Footnotes
Date 03/29/05 Page 50 of 79
Pace Analytical Services Inc
aceAnalytical
9800 KiX äj2I
wpaoelahsom Phone [phone]
Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9290353
Client Project lit West End 6228-05-2694
QC Batch 123964 Inalysis Method EPA 8015
QC Batch Method EPA 3545 Asalysis Description
EPS in Soil by 3545/8015
Associated Lab Samples 925409575 925409583 925409591 925409609 925409617
925409625 925409633 925409641 925409658 925409666
925409674 925409682
MSThOD BLIrMR 925414682
Associated Lab Samples 925409575 925409583 925409591 925409609 925409617 925409625 925409633
925409641 925409658 925409666 925409674 925409B2
Blank Reporting
Parameter Units Result Limit Footnotes
Diesel Fuel mg/kg MD 5.0
n-Pantacosane 128
LABORATORY CONTROL SiMPI.E 925414690
Spike LCS LCS
Parameter Units Conc Result Footnotes
Diesel Fuel mg/kg 166.70 147.6 89
n-Pentacosane 146
MATRIX SPIKE MATRIX SPIKE DUPLICATE 925414716 925414724
925410755 Spike MS MSD MS MSD
Parameter Units Result Conc Result Result Footnotes
Diesel Fuel mg/kg 0.9523 208.10 186.1 325.1 89 156 54 24
n-Pentacosane 138 117
SMLE DUPLICATE 925414708
925410748 DUD
Parameter Units Result Result EDit Footnotes
Diesel Fuel ing/kg ND ND NCn-Pentacosane CS 100 105
Date 03/29/05 Page 51 Of 79
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS Charlotte Certification lOsNCWastewater40ThisreportshaMnothereproducedexceptinNCWastewater12NCDrinking Water 37712 whhout the wrhten consent of Pace Analytical Services Inc NC Drinking Water 37706SCEnvironmental99030SC99006FLtJELAPE87648FLNELAPE87627
Pace Analytical Serilces Inc
9800 Kincey Avenue Suite 100
Huntersville NC 28078
Phorie 704.875.9092
www.paceIabLcorn FaK 704.875.9091
QUALITY CONTROL DATA
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
QC Batch 124037 Analysis Method MPH
QC Batch Method EPA 3550 Analysis Description MPH in Soil by Mass Method
Associated Lab Samples 925409690 925409708 925409716 925409724
METHOD BLANK 925416703
Associated Lab Samples 925409690 925409708 925409716 925409724
Blank Reporting
Parameter Units Result Limit Footnotes
Aliphatic C09-C18 mg/kg ND 10
Aliphatic C19-C36 mg/kg MD 10
Aromatic Cil-22 mg/kg ND 10
2-Fluorobiphenyl 106
2-Brcexionaphthalene 103
Nonatriacontane 114
o-Perphenyl 109
LABORATORY CONTROL S7eLE 925416711
Spike LCS LCS
Parameter Units Conc Result 9uRec Footnotes
Aliphatic C09C18 mg/kg 10.00 7.540 75
Aliphatic Cl9C36 mg/kg 13.33 13.60 102
Aromatic Cl122 mg/kg 28.33 23.16 82
2-Fluorobiphenyl CS 91
2-Brcenonaphthalene 93
Nonatriacontane 105
o-Terphenyl 90
NKTRIX SPIKE NKTRIX SPIIE DUPLICATE 925416729 925416737
925409690 Spike MS MSD MS MSD
Units Result Cone Result Result 9uRec RPD Footnotes
A3.iplsatic C09C18 mg/kg 11.16 5.808 6.174 52 55
Aliphatic C19C36 mg/kg 14.88 13.01 13.90 87 93
Aromatic C11-22 mg/kg 31.63 22.81 20.76 72 66
tate 03/29/05 Oage 52 of 79
Asheville Certif icat ion ID REPORT OF LABORATORY ANALYSIS Charlotte CertiticatigJQNCWastewater40ThiSreportshallriotbereproducedexceptis full
NC Wastewater 12NCDrinking Water 37712 without the written consent of Pace Analytical Services
NC Drinking Water 37706SCEnvironmental99030SC99006FLNELAPE87648FLNELAPE87627
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
aceAnaIyticaIabs.Gom Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
MTBIX SPIRE MAIRIX SPIKE DUPLICA1E 925416729 925416737
925409690 Spike MS MSD MS MSD
_________________________Units Result Conc Result Result 96Rec Footnotes
2-Fluorobiphenyl 99 94
2-Bromonaphthalene 95 84
Nonatriacontane 87 84
o-Terphenyl 80 73
nate 03129/05 Sega 33 79
Ashevthe Ceriffication REPORT OF LABORATORY ANALYSIS M10 CerfficatjpyjNCWastewater40
This report shall not be reproduced except in ND Wastewater 12NCDrinkingWater37712without the written consent of Pace Analytical Services Inc
NC Drinking Water 37706SCEnvironmental99030Sc99006FLNELAPE8748FLNELAP87627
Pace Analytical Services Inc
aceAnalyticar 980KieSS
wwwpaceIabscom Phone [phone]
Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
QC Batch 123959 na1ysis Method EPA 8015
QC Batch Method EPA 8015 Imalysis Description GAS Soil North Carolina
Associated Lab Samples 925409575 925409583 925409591 925409609 925409617
925409625 925409633 925409641 925409658 925409666
925409674 925409682
MSTHOD BLASK 925414195
Associated Lab Samples 925409575 925409583 925409591 925409609 925409617 925409625 925409633
925409641 925409658 925409666 925409674 925409682
Blank Reporting
Parameter Units Result Limit Footnotes
Gasoline mg/kg ND 5.0
4-Bromofluorobensene 114
LABORATORY CONTROL SA2PLE LCSD 925414203 925414211
Spike LCS LCSD LCS LCSDParameterUnitsConcResultResult%Rec 9sRec RPD Footnotes
Gasoline mg/kg 25.00 28.09 25.09 112 100 11
4-Bromofluorobenzene 85 101
MATRIX SPIxE 925414229
925409575 Spike MS MS
Parameter Units Result Conc Result Rec Footnotes
Gasoline mg/kg 0.6703 23.05 27.24 115
4-Bromofluorobenzene 71
SAMPLE DUPLICATE 925414237
925409591 DUP
Parameter Units Result Result RPt Footnotes
Gasoline mg/kg ND ND NC4-Brainofluorobenzene 93 93
Date 03129/05
Page 54 of 79
9yilI it ix lion lOs REPORT OF LABORATORY ANALYSIS ttotte CertificapJgNCWastewater40Thisreport shall not be reproriocerl except in toll
NC Wastewater 12NCDrinkingWater37712wimathe written consent of Pace Analytical Services Inc
NC Drinking Water 37706SCEnvironmental99030SC99006FLNELARE87648FLNELAPE87627
/eAnaIyticar
w.v pa2eab.corn
Pace Analytical Seriices Inc
9800 Kincey Avenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
QC Batch 124057 tna1ysis Method VPH
QC Batch Method VPH analysis Description
VPR in Soil by Mass Method
Associated Lab Samples 925409500 925409518 925409534 925409690 925409708
925409716 925409724
METHOD BLANK 925418352
Associated Lab Samples 925409500 925409518 925409534 925409690 925409708 925409716 925409724
Blank Reporting
Parameter Units Result Limit Footnotes
Aliphatic C05-C08 mg/kg ND 10
Aliphatic C09-C12 mg/kg ND 10
Arnatic C09C10 mg/kg ND 10
25-Dibromotoluene FID lu 102
25-Dibromotoluene PIDS lu 102
LABORATORY CONTROL S7NPLE 925418360
Spike LCS LCSParameterUnitsConcResult9nRec Footnotes
Aliphatic C05C08 mg/kg 20.00 19.98 100
Aliphatic C09C12 mg/kg 5.000 5.013 100
Aromatic C09Cl0 mg/kg 5.000 5.021 100
25-Dibromotoluene FIDS 104
25-Dibroniotoluene PIDS 106
M7dRIX SPIKE MATRIX SPIKE DUPLICATE 925418378 925418386
Aliphatic C05-C08
Aliphatic C09-C12
Aromatic C09-C10
5-Dibromotoluene FlU
25-Dibrozetotolnene PID
cati
NC Waxtewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report ohall not be reproduced except in lull
without the written consent of Pace Analytical Services Inc
Charlotte Certification los
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP 87627
925409500 Spike MS MSD MS MSD
Units Result Conc Result Result 9g 9sg
cog/kg 0.5052 24.29 24.18 24.43 98 98
nag/kg 0.6090 6.073 6.148 6.195 91 92
mg/kg 0.1641 6.073 6.119 5.956 98 95
119 106
119 107
Date 03/29/05
Footnotes
Page 55 of 79
Pace Analytical 3w/ices Inc
9800 KinceyAvenue Suite 100
Hunters yule NC 28078
Phone [phone]wwpace18bScomFax704.875.9091
QUALITY CONTROL DATA
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
SXMPLE DUPLIC1TE 925418394
925409518 DtW
____________________________Units Result Result RPD ootnotes
Aliphatic C05-C08 mg/kg ND ND NC
Aliphatic C09-C12 mg/kg ND ND NC
Aromatic C09-C10 mg/kg ND ND NC
25-Dibromotoluene IDS 96 110 109
25Dibromotoluene PIDS 112 111
Date 03/29/05 Page 56 of 79
llleifjationlD REPORT OF LABORATORY ANALYSiS rIte Certification IDeNCWastewater40ThisreportchatnotbereprodocedexceptNCWaslewater12NCDrinkingWater37712without the written consent of Pace Analytical Services Inc NC Drinking Water 37706SCEnvironmental99030SC99006FLNELAPE87648FLNELAPE87627
Pace Analytical Seivices Inc
9800 KinceyAvenue Suite 100
Huntersvile NC 28078
Phone [phone]
Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
QC Batch 123953 Analysis Method EPA 8270
QC Batch Method EPA 3545 Analysis Description
Semivolatile Organics
Associated Lab Samples 925409500 925409518 925409534 925409690 925409708
925409716 925409724
METHOD BLANR 925413924
Associated Lab Samples 925409500 925409518 925409534 925409690 925409708 925409716 925409724
Blank Reporting
____________________________Units Restilt Limit ootnotes
Acenaphthene ug/kg ND 330
Acenaphthylene tag/kg ND 330
Anthracene ug/kg ND 330
Benzokfluoranthene tag/kg ND 330
Benzobflnoranthene ug/kg ND 330
Benzoaanthracene ug/kg ND .330
Benzoic acid tag/kg ND 1600
Benzoghiperylene ug/kg ND 330
Benzyl alcohol tag/kg ND .660
Benzoapyrene tag/kg ND 330
4-Bromophenylphenyl ether tag/kg ND 330
Butylbenzylphthalate ug/kg MD 330
4-Chloro-3-methylphenol tag/kg ND 660
4-Chioroaniline tag/kg ND 660
his 2-Chloroethoxynuethane tag/kg ND 330
bis2-Chloroethy ether ug/kg MD 330
bis2-Chloroisopropyl ether tag/kg ND 330
2-Chloronaphthalene ug/kg ND 330
2-Chiorophenol tag/kg ND 330
4-Chlorophexzylpbenyl ether tag/kg ND 330
Chrysezie ug/kg MD 330
Dibenzahanthracene tag/kg MD 330
Dibenzoduran tag/kg ND 330
12-Dichlorobenzene tag/kg ND 330
13-Diohlorobenzene tag/kg MD 330
14-Dichlorobenzene tag/kg ND 330
33-Dichlorobgnzidixie tag/kg ND 660
24-Dichiorophenol tag/kg MD 330
Diethylphthalate tag/kg MD 330
24-Diosethyiphextol tag/kg ND 330
Date 03/29/05 Page 57 of 79
tigill.CeiffjcgiionlD REPORT OF LABORATORY ANALYSIS Charlotte Cerhtication IDaNCWastewater40Thisreportshall not be reproduced except in lot NC Wastewater 12NCDrinkingWater37712withoutthe written consent of Pace Analytical services Inc NC Drinking Water 37706SCEnvironmental99030SC99006
FL NELAP E87646 FL NELAP E87627
Pace Analytical Services inc
9800 KiiceyAvenue Suite 100
Hunlersvifle NC 28078
Phone [phone]
Fax [phone]
QUALITY CONTROL DATA
Lab Project NunIber 9290353
Client Project ID West End 6228-052694
THOD BLANK 925413924
Associated Lab Samples 925409500 925409518 925409534 925409690 925409708 925409716 925409724
Blank Reporting
____________________________Units Result Limit Footnotes
Dimathylphthalate ug/kg ND 330
Di-n-butylphthalate uglkg ND 330
46-Diuitro-2-methylphenol ug/kg ND 330
24-Dinitropheno3 uglkg ND 1600
2.4-Dinitrotoluene ug/kg ND 330
26-Dinitrotoluene ug/kg ND 330
Di-n-octylphthalate ug/kg ND 330
l2-Diphenylhydrazine ug/kg ND 330
bis2-Ethyliaezylphthalate ug/kg ND 330
Fluoranthene ug/kg ND 330
Fluorene ug/kg ND 330
Bexachloro-l3-butadiene uglkg ND 330
Bexachlorobenzene ug/kg ND 330
Hexachlorocyclopentadiene ug/kg ND 330
Hexachloroethane ug/kg ND 330
Indeno123-cdpyrene nag/kg ND 330
Isophorone nag/kg ND 330
2-Methylnaphthalene nag/kg ND 330
2-Nethylphanol o-Cresol nag/kg ND 330
34-Nethylphenol nag/kg ND 330
Naphthalene nag/kg ND 330
2-Nitroaniline nag/kg ND 1600
3Nitroaniline nag/kg ND 1600
4-Nitroaniline ug/kg ND 1600
Nitrobenzene nag/kg ND 330
2-Nitrophenol ug/kg ND 330
4-Nitrophenol ug/kg ND 1600
N-Nitroso-di-n-propylannine nag/kg ND 330
N-Nitrosodiphenylamine ug/kg ND 330
Pentachlorophenol nag/kg ND 16D0
Phenanthrene nag/kg ND 330
Phenol ug/kg ND 330
Pyrexae ug/kg ND 330
124-Trichlorobexazene nag/kg ND 330
245-Trichlorophenol nag/kg ND 330
246-Trichlorophenol nag/kg ND 330
nate 03/29/05 Page 58 of 79
Asheville Certification IDt REPORT OF LABORATORY ANALYSIS Ctiarlotte Certification Dx
NC Wastewater 40 ThIn report shaH not be reproduced except in full NC Wactewater 12NCDrinking Water 37712 without the written consent of Pace Analytical Services Inc NC Drinking Water 37706SCEnvironmental99030SC99006
FL NELAP E87648 FL NELAP E87627
QT.TALITY CONTROL DATA
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
MEitOD BLANK 925413924
Associated Lab Samples 925409500 925409518 925409534 925409690 925409708 9254097.16 925409724
Blank Reporting
Parameter Units Result Limit Footnotes
Nitrobenzene-d5 CS 53
2-Fluorobiphenyl IS 58
rerphenyl-d14 77
Phenol-d5 54
2-Fluorophenol 49
246-Tribromophenol 57
LABORATORY CONTROL SAaLE 925413932
lle Co if iced ion Os
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced oxcept in hill
without the written concern ot Pace Analytical Services Inc
Charlotte CertItjcatiogJs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
Spike LCS LCS
Parameter Units Conc Result Footnotes
Acenaphthene ug/kg 1667.00 973.2 58
Aoenaphthylene ug/kg 1667.00 1024 61
Anthracens ug/kg 1667.00 1136 68
Benzokfluoranthene ug/kg 1667.00 1287 77
Benzobfluoranthene ug/kg 1667.00 1186 71
Benzoaanthracene ug/kg 1667.00 1158 70
Benzoic acid ug/kg 1667.00 579.3 35
Benzoghipery.ene ug/kg 1667.00 916.8 55
Benzyl alcohol ug/kg 1667.00 990.7 59
Benzoapyrene ug/kg 1667.00 1154 69
4-Bromophenylphenyl ether ug/kg 1667.00 1070 64
Butylbenzylphthalate ug/kg 1667.00 1151 69
4-Chloro-3-xaethylphenol ug/kg 1667.00 1101 66
4Chloroaniline ug/kg 1667.00 895.8 54
bis2-Ch.oroethoxymethane ug/kg 1667.00 883.0 53
bis2-Chloroethyl ether ug/kg 1667.00 825.1 50
bis2-Chloroisopropyl ether ug/kg 1667.00 868.1 52
2-Chloronaphthalane ug/kg 1667.00 956.0 57
2-Chiorophenol uglkg 1667.00 833.7 50
4-Chlorophanylphenyl ether ug/kg 1667.00 1087 65
Chrysene ug/kg 1667.00 1121 67
Dibenzahanthraoene ug/kg 1667.00 973.1 58
Dibenzofuran ug/kg 1667.00 1077 65
12Dichlorobenzene ug/kg 1667.00 839.9 50
Date 03/29/05 Page 59 of 19
QTJALIT CONTROL DATA
Pace Analytical Services Inc
9800.KinceyAvenue Suite 100
Hunlersville NC 28078
Phone [phone]
Fax [phone]
LABORATORY CONTROL SaNPLE 925413932
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
AhevllIe Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in lull
without the written consent of Pace Analytical Services Inc
Cliarlofle Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FLNEI.AP E87627
paeJabLcom
Spike LCS LCS
Parameter Units Cono Result %Rec Pootnotes
13Dichlorobenzene ug/kg 1667.00 806.0 48
14-Dicrhlorobenzene ug/kg 1667.00 830.7 50
33Dich1orobenzidine ug/kg 3333.00 766.6 23
24-Dichiorophenol ug/kg 1667.00 947.4 57
Diethylphthalate uglkg 1667.00 1144 69
24Dimethyipheno ug/kg 1667.00 884.4 53
Dizsethylphthalate ug/kg 1667.00 1118 67
Di-n-butylphthalate ug/kg 1667.00 3.146 69
46Dinitro-2-methylpheno ug/kg 1667.00 1351 81
24Dinitrophenol mg/kg 1667.00 1207 72
24-Dinitrotoluene mg/kg 1667.00 1222 73
26-Dinitrotoluene mg/kg 1667.00 1175 70
Di-n-octylphthalate mg/kg 1667.00 1178 71
12-Diphenylhydrazine mg/kg 1667.00 988.3 59
bis2-Ethylhexylphthalate mg/kg 1667.00 1205 72
Fluoranthene mg/kg 1667.00 1125 68
Fluorene ug/kg 1667.00 1086 65
Hexachloro-13butadiene mg/kg 1667.00 823.1 49
Hexachlorobenzene ug/kg 1667.00 1019 61
Hexachlorocyclopentadiene mg/kg 1667.00 666.2 40
Hexachioroethane ug/kg 1667.00 778.9 47
Indeno123-cdpyrene ug/kg 1667.00 984.3 59
Isophorone mg/kg 1667.00 974.1 58
2Methylnaphthalene mg/kg 1667.00 904.5 54
2-Nethyiphenol o-Cresol ug/kg 1667.00 908.1 54
34Methylphenol mg/kg 1667.00 969.1 58
Naphthalene ug/kg 1667.00 848.5 51
2-Nitroaniline mg/kg 1667.00 938.5 56
3Nitroaniline mg/kg 1667.00 1134 68
4Nitroaniline mg/kg 1667.00 1433 86
Nitrobeozane mg/kg 1667.00 840.9 50
2-Nitrophenol ug/kg 1667.00 896.2 54
4Nitropheno mg/kg 1667.00 1138 68
N-Nitroso-di-n-propylazujne mg/kg 1667.00 907.8 54
N-Nitrosodiphenylanjne mg/kg 1667.00 1229 74
Pentachlorophenol ug/kg 1667.00 1085 65
Phenaixthrane mg/kg 1667.00 1115 67
Date 03/29/05 ae 60 79
Pace Analytical Serilcas Inc
9800 KinceyAvenue Suite 100
Hunters villa NC 28078
Phone [phone]
Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
LABORATORY CONTROL SA1LE 925413932
LCS
Footnotes
Phenol 52
Pyrene
124 -Trichlorobenzene
245-Triehiorophenol246-Trichlorophenol
Nitrobenzene-d5
2-Fluorobiphenyl
Terphenyl-dl4
Phenol-d5
2-Fluorophenol
246-Tribromophanol
MATRIX SPXKE MATRIX SPIKE DUPLICATE 925413940 925413957
Acenaphthene
4-Chloro-3-methylphenol
2-Chlorophenol
14-Di.chlorobenzene
4-Dinitroto inane
4-Nitrophenol
N-Nitroso-di-n-propy1ane
Pentachlorophenol
Phenol
Pyrene
12 4-Trichlorobenzene
Nitrobenzane-d5
2-Fluorobipheny
Terphenyl-d14
Pbenol-d5
2-Fluorophenol
246-Tribromophanoj
siinilIeCrtjficationlDs REPORT OF LABORATORY ANALYSIS Charlotte Certification OsNCWastewater40
This report shall not be aprodeced except NC Wastewater 12NCDnnkingWater37712without the written consent of Pace Analytical Services NC Drunkin Water 37706SCEnvironmental99030SC99006FLNELAPE87648FLNELAP087627
wwwpaabscern
Spike LCS
Units Conc Result
ug/kg l667.D0 870.0
ug/kg 1667.00 1166
ug/kg 1667.00 829.1
ug/kg 1667.00 1152
ug/kg 1667.00 1073
70
50
69
64
51
60
74
52
49
66
Footnotes
925409500 Spike MS MSD MS MSDUniteResultConcResultResult
ug/kg 2024.00 1095 973.7 54 48 12
nag/kg 2024.00 1202 1059 59 52 13
ug/kg 2024.00 996.3 895.5 49 44 11
ug/kg 2024.00 1005 914.3 50 45 10
ug/kg 2024.00 1366 1223 68 60 11
ug/kg 2024.00 1246 1119 62 55 11
nag/kg 2024.00 1096 944.8 54 47 15
nag/kg 2024.00 1199 1029 59 51 15
nag/kg 2024.00 997.9 902.9 49 45 10
nag/kg 2024.00 1361 1239 67 61
ug/kg 2024.00 1002 928.4 50 46
DaCe 03129/05
48 46
53 50
69 61
48 44
44 41
54 48
Page 61 of 79
Pace Analytical Serilces Inc
9800 KioceyAvenue Suite 100
aceAnalytical
vw.pacJabcorn Fax [phone]
QUALITY CONTROL DATA
Lab Project Nuniber 9290353
Client Project ID West End 6228-05-2694
SI35PLE DUPLICATE 925413965
925409716 DTJP
Units Result Result Footnotes
Acanaphthene ug/kg ND ND NC
Acenaphthylene ug/kg ND ND NC
Zenthraaene ug/kg ND ND NC
Benzokfluoranthene ug/kg ND ND NC
Benzobfluoranthene ug/kg ND ND NC
Benzoaanthracene ug/kg ND ND NC
Benzoic acid ug/kg ND ND NC
Eenzoghiperylene ug/kg ND ND NC
Benzyl alcohol ug/kg ND ND NC
--Benzoapyene ug/kg ND OW NC
4-Bromophenyiphenyl ether nag/kg ND ND NC
Butylbenzylphthalate ug/kg ND ND NC
4-Chloro-3-methylphenol ug/kg ND ND NC
4-Chloroaniline nag/kg ND ND NC
bis 2-Ch1oroethoxymethaie nag/kg ND ND NC
bis2-Chloroethyl ether nag/kg ND ND NC
bis2-Chloroisopropy ether nag/kg ND ND NC
2-Chloronaphthalane ug/kg ND ND NC
2-Chioropheno nag/kg ND ND NC
4-Chlorophenylphenyl ether nag/kg ND ND NC
Chrysene nag/kg ND ND NCDibenzahanthraceneug/kg ND ND NCDibeuzofurannag/kg ND ND NC
12-Dichlorobenzene nag/kg ND ND NC
13-Diclilorobarizane nag/kg ND ND NC
14-Dich.orobenzene nag/kg ND ND NC
33-Dichlorobenzidjn ug/kg ND ND NC
24-Dichlorophenol nag/kg ND ND NC
Diethylphtbalate nag/kg ND ND NC24-Dimethyiphenol nag/kg ND ND NC
Dimethylphthalate nag/kg ND ND NCDi-n-butylphthalate ug/kg ND ND NC
46-Diuitro-2-mathy1pano1 nag/kg ND ND NC24-Dinitropheno ug/kg ND ND NC24-Dinjtrotoluene nag/kg ND ND NC26-Djnitrotoluene ug/kg ND ND NC
Di-n-octylphthalate ug/kg ND ND NC
Date 03/29/05
Page 52 of 79
AifleCfflcas REPORT OF LABORATORY ANALYSIS Charlotte Certification DoNCWastewater40Thisreport shall not be reproduced except in NC Wastewater 12NCDrinkingWater37712withoutthwrittenconsentofpaceAnalyticalServicesnoNCDrinking Water 37706SCEnvironmental99030SC99006FLNEI.AP E87648 FL NELAP E87627
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
SIIHPLE DDPLICATE 925413965
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Asheville Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSiS
This report shell not be reproduced except in tell
without the written conseet of Pace Analytical Services Inc
Charlotte Certification lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
paceI8bstxm
925409716 naP
Units Result Result fl Footnotes
12-Diphenyihydrazine ug/kg ND ND NC
bis2-Ethylhexylphthalate ug/kg ND ND NC
fluoranthene ug/kg ND ND NC
Fluorerse ug/kg ND ND NC
liexachloro-13-butadjene ug/kg ND ND NC
liexachlorobenzene ug/kg ND ND NC
Hexachlorocyclopentadjene ug/kg ND ND NC
Hexachloroethane ug/kg ND ND NC
Indeno123-cdpyrene ug/kg ND ND NC
Isophorone ug/kg ND ND NC
2-Methylnaplithalene ugfkg ND ND NC
2-Mathyiphenol o-Cresol ug/kg ND ND NC
34-Methylphenol ug/kg ND ND NC
Naphthalene ng/kg ND ND NC
2-Nitroaniline ug/kg ND ND NC
3-Nitroaniline ug/kg ND ND NC
4-Nitroaniline ug/kg ND ND NC
Nitrobenzene ug/kg ND ND NC
2-Nitrophenol ug/kg ND ND NC
4-Nitrophenol ug/kg ND ND NC
N-Nitroso-di-n-propylainjne ug/kg ND ND NC
N-Nitrosodiphenylainine ug/kg ND ND NC
Pentachlorophanol ug/kg ND ND NC
Phenanthrene ug/kg ND ND NCPhenolug/kg ND ND NC
Pyrene ugfkg ND ND NC
124-Trichlorobenzena ug/kg ND ND NC
245-Irichlorophenol ug/kg ND ND NC
246-3rjchloropbano1 ugfkg ND ND NC
Nitrobenzene-d5 9o 52 54
2-Fluorobiphexoyl 59 60
1erphenyl-d14 78 80
Phenol-dS 48
2-Fluorophenol 34 36
246-rribromopheno1 44 43
Date 03/29/05
Page 63 of 79
Ana4ici
wpaceJabcbm
QUALITY CONTROL DATA
Pace Analytical Ser.rices Inc
9800 Kincey Avenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
lTHOD BLANK 925415432
Associated Lab Samples
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Acetone
Benzane
Bromobenzene
Bromochloromethane
Bromodichioromethane
Bromoform
Broiriomethane
2-Butanone 0K
n-Butylbenzene
sac-Butylbanzene
tart -Butylbenzene
Carbon tetrachloride
Chiorobensene
Chioroethane
chloroform
Chlorcauethane
2-Chlorotoluene
4-Chiorotoluene
2-Dibromo-3-chloropropane
Dibromochloromethane
2-Eibroinoethane EDB
Dibrosomethane
12 -Dichlorobenzene
13 -Dichlorobenzene
4-Dichlorobenzene
Dichlorodifluoromethane
1-Dichioroethane
12-Dichioroethane
1-Dichioroethene
cis-1 2-Dichloroethene
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall nat be reproduced except in tell
without the written consent of Pacv Analytical Services Inc
Charlotte Certification Os
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP 687627
QC Batch 123972 Analysis Method EPA 8260
QC Batch Method EPA 8260 Analysis Description GC/MS VOCs 5035/8260 law level
Associated Lab Samples 925409500 925409518 925409534 925409690 925409716
925409724
Di rg.nn4ar
925409300 925409518 925409534 925409690 925409716 925409724
Blank Reporting
Units Result Limit Footnotes
ug/kg ND 100
ug/kg ND 5.0
ug/kg ND 5.0
uglkg ND 5.0
nag/kg ND 5.0
ug/kg ND 5.0
ug/kg ND 10
nag/kg ND 100
nag/kg ND 5.0
nag/kg ND 5.0
ug/kg ND 5.0
ug/kg ND 5.0
nag/kg ND 5.0
nag/kg MD 10
nag/kg MD 3.0
nag/kg ND 10
nag/kg MD 5.0
nag/kg ND 5.0
nag/kg ND 5.0
ug/kg MD 5.0
ug/kg ND 5.0
ug/kg ND 5.0
ug/kg MD 5.0
ug/kg ND 5.0
nag/kg ND 5.0
ug/kg ND 10
ug/kg ND 5.0
nag/kg MD 5.0
nag/kg MD 5.0
nag/kg ND 3.0
Date 03/29/05 Page 64 79
Pace Analytical Services Inc
9800 Kisicey4venue Sut8 100
aceAiiaI$icaI Huntersville NC 28078
Fax [phone]
QUALITY CONTROL DATA
Lab Project Nuiuber 9290353
Client Project ID West End 6228-05-2694
0TH0D BLi1K 925415432
Associated Lab Saijles 925409500 925409518 925409534 925409690 925409716 925409724
Blank Reporting
____________________________Units Result Limit Footnotes
trans-12-Dichloroethene ug/kg ND 5.0
l2-Dichloropropane ug/kg ND 5.0
13-Dichloropropane ug/kg ND 5.0
2-Dichloropropane ug/kg ND 5.0
ll-Dichloropropene ug/kg ND 5.0
cis-13-Dichloropropene ug/kg ND 5.0
trans-13-Dichloropropene ug/kg ND 5.0
Diisopropyl ether ug/kg ND 5.0
Ethylbenzena ug/kg ND 5.0
Rexachloro-l3-butadiene ug/kg ND 5.0
2-Rexanone ug/kg ND 50
Isopropylbenzene Cumnene ug/kg ND 5.0
p-Isopropyltoluene ug/kg ND 5.0
Nethylene chloride ugfkg ND 5.0
4-Methyl-2-pentanone 1IBI ugfkg ND 50
Methyl-tert-butyl ether ug/kg ND 5.0
Naphthalene ug/kg ND 5.0
n-Propylbenzene ug/kg ND 5.0
Styrene ug/kg ND 5.0
1112-Tetrachioroethane ug/kg ND 5.0
1122-Tetrach1oroetne ug/kg ND 5.0
Tetrachioroethene ugfkg ND 5.0
Toluene ug/kg ND 5.0
123-Trichlorobenzene ug/kg ND 5.0
l24-Trichlorobenzene ug/kg ND 5.0
111-Trichioroethane ugtkg ND 5.0
1l2-Trjclsloroethane ugfkg ND 5.0
Trichloroet3sene ug/kg ND 5.0
Trichlorofluoraxnethane ug/kg ND 5.0
123-Trichioropropane ug/kg ND 5.0
124-Trimethylbenzene ug/kg ND 5.0
135-Trjmethylbenzene ug/kg ND 5.0
Vinyl acetate ug/kg ND 50
Vinyl chloride ugfkg ND 10
Xylene Total ug/kg ND 5.0
mp-Xylene ug/kg ND 10
Date 03/29/05 Page 65 79
ficat ion IDs REPORT OF LABORATORY ANALYSiS Charlotte Certification IDsNCWastewater40Thisreport okall riot be reproduced except in full NC Wastewater 12NCDrinking Water 37712 without the written consent at Pace Analytical Services Inc
PlC Drinking Water 37706SCEnvironrrrenfal99030SC99006FLNELAPE87648FLNELAP87627
Pace Analytical Sereices Inc
aceAnalyticar
9800 KeX
Phone [phone]
Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
METHOD BL7 925415432
Associated Lab Samples 925409500 925409518 925409534 925409690 925409716 925409724
Blank Reporting
Parameter Units Result Limit Footnotes
o-Xylene ug/kg ND 5.0
Toluene-d8 9o 98
4-Bromofluorobenzene 92
Dibromofluoromethane 108
l2-Dichloroethane-d4 9u 107
LABORATORY CONTROL SaEPLE 925415440
Spike LCS LCS
Parameter Units Conc Result 9Rec Footnotes
Acetone ug/kg 100.00 125.4 125
Benzene ug/kg 50.00 51.70 103
Broouobenzene ug/kg 50.00 54.31 109
Brceuochlorcenethane ug/kg 50.00 54.86 110
Bramodicliloromathane ugfkg 50.00 51.51 103
Bromofozm ug/kg 50.00 53.33 107
Bromomethane ug/kg 50.00 54.32 109
2Bistanone HEx ug/kg 100.00 93.76 94
nButylbenzene ug/kg 50.00 48.12 96
secButylbenzene ug/kg 50.00 56.16 112
tertButylbenwene nag/kg 50.00 57.67 115
Carbon tetrachloride nag/kg 50.00 54.82 110
chlorobenzene ug/kg 50.00 51.28 103
Chioroethane ugfkg 50.00 52.09 104
Chloroform ug/kg 50.00 54.19 108
Chloramethane nag/kg 50.00 45.40 91
2Chlorotoluene ug/kg 50.00 55.88 112
4-Chiorotoluene nag/kg 30.00 52.62 105
l2-Dibromo-3-chloropropane ug/kg 50.00 56.17 112
Dibromochlorthana nag/kg 50.00 52.93 10612DibramoeteEDBug/kg 50.00 5458 109
Dibromomethane ug/kg 50.00 52.38 105
l2Dichlorobenzene nag/kg 50.00 53.72 107l3Djch1orobzenenag/kg 50.00 51.73 103
l4Dichlorobenzene nag/kg 50.00 50.82 102
Date 03/29/05
Page 66 00 79
REPORT OF LABORATORY ANALYSIS liarictte Certification lOsNCWastewater40
Thin shall not be reproduced except in fut
NC Wastewater 12NCDrinkingWater37712without the written consent at Pace Analytical Services xc
NC Drinking Water 37706SCEnvironmental99030SC99006ftNELAPE87648FLNELAPE87627
Pace Analytical Sarvicas Inc
9800 KinceyAvenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax[phone]
QUALITY CONTROL DATA
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
L.BORATORY CONTROL SZuMPLE 925415440
Dichiorodifluoromethane
1-Dichioroethane
2-Dichloroethaxie
l-Dichloroethene
cis-l2-Dichioroethene
trans-l2-Dichloroethene
2-Dichloropropane
3-Dichioropropane
2-Dichloropropane
1-Dichloropropene
cia-i 3-Diohioropropene
trans-i 3-Dichloropropene
Dilsopropyl ether
Etl3ylbenzene
Hexach3oro-1 -butadiene
2-Hezanone
Isopropylbeuzene Cumene
p-Isopropyitoluene
Methylens chloride
44lethyi-2-pentanone NIEK
Nethyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1l2-Tetrachloroethane
1122 -Tetrachioroethane
Tetrachioroethene
Toluene
123-Trichlorobenzene124-Trichlorobenzane111-Trichioroethane
112 -Trichloroethana
Trichioroethene
Trichiorofluorcajiethane
3-Triabloropropane
124-TrimethyThenzene
135-Trimethylbeuzene
Date 03/29/05 Page 67 of 79
AshevitieCertjficatjon lOs REPORT OF LABORATORY ANALYSIS Certification lOsNCWastewater40Thisreportshall not be reproduced excepts
NC Wastewater 12NCDrinkingWater37712without the written consent of Pace Analytical Services Inc
NC Drinking Water 37706SCEnvironniental99030SC99006FLNELAPE87648FLNELAPE87627
wvw.pacatabscom
Spike LCS LCS
Units Conc Result Footnotes
ug/kg 50.00 45.25 90
ag/kg 50.00 53.14 106
ag/kg 50.00 54.33 109
ag/kg 50.00 54.67 109
ag/kg 50.00 54.39 109
ag/kg 50.00 53.73 107
ag/kg 50.00 54.48 109
ug/kg 50.00 52.93 106
ag/kg 50.00 53.83 108
ag/kg 50.00 55.32 111
ug/kg 50.00 50.60 101
ag/kg 50.00 50.32 101
ug/kg 50.00 58.44 117
ag/kg 50.00 51.51 103
ag/kg 50.00 55.96 112
ag/kg 100.00 103.3 103
ag/kg 50.00 55.83 112
ag/kg 50.00 49.83 100
ag/kg 50.00 58.53 117
ug/kg 100.00 102.1 102
ug/kg 50.00 55.47 111
ag/kg 50.00 47.66 95
ug/kg 50.00 55.45 iii
ag/kg 50.00 51.04 102
ag/kg 50.00 53.59 107
ag/kg 50.00 52.11 104
ug/kg 50.00 50.97 102
ag/kg 50.00 50.62 101
ugfkg 50.00 49.35 99
ag/kg 50.00 46.27 92
ag/kg 50.00 54.43 109
ag/kg 50.00 51.95 104
ag/kg 50.00 49.28 99
ag/kg 50.00 47.86 96
ag/kg 50.00 56.47 113
ag/kg 50.00 48.65 97
ug/kg 50.00 50.09 100
Pace Analytical Seriices Inc
9800 KinceyAvenue Suite 100
HunlersviIe NC 28078
Phone [phone]
Fax [phone]
QUALITY CONTROL flATA
Lab Project Nusiber 9290353
Client Project ID West End 6228-05-2694
LABORATORY CONTROL SANPLE 925415440
Spike LCS LCS
___________________________Units Conc Result Footnotes
Vinyl acetate ug/kg 100.00 20.91 21
vinyl chloride ug/kg 50.00 51.52 103
Xylene Total ug/kg 150.00 153.8 103
uip-Xylene ug/kg 100.00 101.6 102
oXylene ug/kg 50.00 52.19 104
Toluene-d8 100
4-Bromofluorobenzene 94
Dibrcenofluoromethane 106
l2-Dichloroethaned4 99
MATRIX SPIKE 925429748
925409534 Spike MS MS
____________________________Units Result Conc Result 9s Footnotes
Bensene ug/kg 48.47 47.82 99
Chlorobenzene log/kg 48.47 48.22 100
l1-Diohloroethene ug/kg 48.47 48.45 100
Toluene ug/kg 48.47 47.40 98
Trichloi-oethene ug/kg 48.47 46.74 96
oluene-dB 100
4-Bromofluorobenzene 98
Dibrcesofluoromethane 102
l2-Dich1oroethaed4 95
SZ4NPLE DUPLICATE 925429730
925399768 DUP
______________________________Units Result Result RPD Footnotes
Acetone ug/kg ND ND NCBenzeneug/kg ND ND NC
Brainobenzene ug/kg ND ND NC
Brcenochloroniethane ug/kg ND ND NCBromodichioromethaneug/kg ND ND NCEromodormug/kg ND ND NC
Bromainethane ug/kg ND ND NC
Date 03/29/05 Page 68 79
REPORT OF LABORATORY ANALYSIS ftariotte Certitication lOsNCWastewatr40Thisreport shall not itt reprothiceh excepts NC Wastewater 12NCDrinking Water 37112 without the written conceal of Pace Analytical Services NC Drinking Water 37706SCEnvironmental99030SC99006FLNELAPE87648FLNELAPES7627
QUALITY CONTROL DATA
Pace Analytical Serilces Inc
9800 KinceyAvenue Suite 100
Wunters villa NC 28078
Phone [phone]
Fax [phone]
SLE DUPLICATE 925429730
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Asheville Ceicatipn lDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 9030
FL NELAP E8748
REPORT OF LABORATORY ANALYSES
This report shall set be reproduced except in lull
without the written consent nf Pace Analytical Services Inc
Charlotte Certificatiopjg
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
wpabs.wn
925399768 DUP
Units Result Result Footnotes
2-Butanone MEK ug/kg ND ND NC
n-Butylbenzene ug/kg ND ND NC
sec-Butylbenzene ug/kg ND ND NC
tert-Butylbenzene ug/kg ND ND NC
Carbon tetrachioride ug/kg ND ND NC
Chlorobenzene ug/kg ND ND NC
Chioroethane ug/kg ND ND NCChlorefozug/kg ND ND NC
Chlorometbane ugfkg ND ND NC
2-Chiorotoluene ug/k ND ND NC
4-Chiorotoluene ug/kg ND ND NC
l2-Dibromo-3-chloropropane uglkg ND ND NC
Dibramoabloromethane uglkg ND ND NC
i.2-Dibraunoethane EDB rag/kg ND ND NC
Dibramometbane rag/kg Nt ND NC
l2-Dichlorobenzene rag/kg ND ND NC
13-Dichiorobensene rag/kg ND ND NC
l4-Dichlorobenzene rag/kg ND ND NC
Dichlorodifluoromethane uglkg ND ND NC
ll-Dichloroethana ug/kg ND ND NC
l2-Dichloroethane rag/kg ND ND NC
ll-DIchloroethene rag/kg ND ND NC
cis-l2-Dichloroethena ug/kg ND ND tiC
trans-l2-Djchloroethene ug/kg ND ND NC
l2-Dichloropropane ug/kg ND ND NC
l3-Dichloropropane rag/kg ND ND NC
22-Dichloropropane ug/kg ND ND NC
ll-Dichloxopropene rag/kg ND ND NC
cis-l3-Dichloropropene rag/kg ND ND NC
trans-l3-Dicbloropropene rag/kg ND ND NC
Diisopropyl ether rag/kg ND ND NC
Ethylbenzena ug/kg ND ND NC
tlexachloro-j 3-butadiene rag/kg ND ND NC
2-Rexanone rag/kg ND ND NC
Isopropylbenzene Cumene rag/kg ND ND NC
p-Isopropyltoluane ug/kg ND ND NC
Methylene chloride rag/kg ND ND NC
Oate 53/29/05
Page 69 of 79
QUALITY CONTROL DATA
Pace Analytical Serilces Inc
9800 Kiocey Avenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
SMLE DtJPLXCATE 925429730
Lab Project Number 929O35
Client Project ID West End 6228-05-2694
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall flat he repmdeced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certification IDs
PlC Wastewater 12
NC Drinking Water .37706
SC 99006
FL NELAP E87627
Footnotes
925399768 DUP
Units Result Result
4-Methyl-2-pentanono MIBK ug/kg ND ND NC
Methyl-tert-butyl ether ug/k ND ND NC
Naphthalene ug/kg ND ND NC
n-Propylbenzene tag/kg ND ND NC
Styrene tag/kg ND ND NC
lll2-Tetrachloroethane tag/kg ND ND NC
ll22-Tetrachloroetbane tag/kg ND ND NC
Tetrachloroethene tag/kg ND ND NC
Toluene ug/kg ND ND NC
l23-Trichlorobenzene tag/kg ND NC
l24-Trichlorobenzene ug/kg ND ND NC
111-Trichioroethane ug/kg ND ND NC
l12-Trichloroethane ug/kg ND ND NC
Trichloroethene tag/kg ND ND NC
Trichiorofluoronnetbane ug/kg ND ND NC
l23-Trichloropropazne tag/kg ND ND NC
l24-Trinethylbenzene tag/kg ND ND NC
l35-Trimethylbenzene tag/kg ND ND NC
Vinyl acetate tag/kg ND ND NC
Vinyl chloride tag/kg ND ND NC
Xylene Total tag/kg ND ND NC
nnp-Xylene tag/kg ND ND NC
o-Xylene tag/kg ND ND NC
Toliaene68 98 100
4-Bromofluorobenzene 87 98
Dibromofluoromethane 101 97
l2-Dichloroetharne-d4 97 97
Date 03/99/05 Page 70 of 79
/eAria/yticaI
wtcr.poceIabsrAn1
Pace Analytical Services Inc
9800 KinceyAverwe Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
QUALITY CONTROL DkTA
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
QC Batch 124167 Analysis Method EPA 8260
QC Batch Method EPA 8260 Analysis Description GC/MS VOCs 5035/8260 low level
Associated Lab Samp.es 925409708
METHOD BLAME 925425175
Associated Lab Samples
cationl0
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
Thin report shall not be reproduced except in lull
without the written consent of Pace Analytical Services Inc
flhgriotte Certification Ig
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
925409708
Blank Reporting
Parameter Units Result Limit Footnotes
Acetone ug/kg MD 100
Benzene ug/kg MD 5.0
Broniobenzene ug/kg ND 5.0
Bromoohiorounethane ug/kg MD 5.0
Bromodichloromethane ug/kg ND 5.0
BromoCorm ug/kg MD 5.0
Bromosnetbane ug/kg MD 10
2-Batanone NEIc ug/kg ND 100
n-Biitylbenzene nag/kg MD 5.0
sec-Butylbenzene nag/kg ND 5.0
tert-Butylbenzene nag/kg ND 5.0
Carbon tetrachloride nag/kg MD 5.0
Chlorobenzene nag/kg MD 5.0
h1oroethane nag/kg MD 10
Chlorofor3n nag/kg ND 5.0
Chloromethane ug/kg ND 10
2-Chlorotoluena ug/kg ND 5.0
4-Chlorotoluene nag/kg MD 5.0
l2-Dibromo-3-chloropropane nag/kg MD 5.0
Dibromoch1oromete ug/kg MD 5.0
12-Dibranioethane EDB nag/kg ND 5.0
Dibromcanethane nag/kg ND 5.0
12-Dichlorobenzena ug/kg ND 5.0
l3-Dichlorobenzene nag/kg MD 5.0
l4-Dichlorobenzene nag/kg ND 5.0
Xichlorodifmuoromethane ug/kg ND 10
l1-Dichloroethane nag/kg MD 5.0
12-Diobloroethane nag/kg ND 5.0
l1-Dichloroethene nag/kg ND 5.0
cis-12-Dichloroethene nag/kg MD 5.0
trans-12-Dichloroethene ug/kg MD 5.0
Date 03/29/05
lage of 19
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
tiuntersville NC 28078
Phone [phone]
Fax [phone]
Th0D BLANK 925425175
Associated Lab Samples 925409708
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Parameter
12-Dichioropropane
3-Dichioropropane
2-Dichloropropane
1-Dichioropropene
cia-i 3-Dichloropropene
trans-i 3-Dichloropropene
Dilsopropyl ether
Etliylbenzene
Hexachloro-i3-butadiene
2-Rexanone
Isopropyibenzene Cumene
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone MINK
Methyl-tert-butyl ether
Naphthalene
nPropyibenzene
Styrene
Asheville Certification Os
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shot not be repnxiilced except
is tall
without the written consent of Pace Analytical Services Incnd
Charlotte Certification lOs
NCWastewater 12
NC Drjnkin Water 37706
SC 99006
FLNELAP E87627
Units
ug/kg
ug/kg
ugfkg
uglkg
ug/kg
uglkg
ugfkg
ug/kg
uglkg
uglkg
ug/kg
nag/kg
ugfkg
nag/kg
uglkg
nag/kg
üg/kg
nag/kg
nag/kg
nag/kg
nag/kg
nag/kg
ug/kg
nag/kg
nag/kg
nag/kg
nag/kg
nag/kg
nag/kg
nag/kg
nag/kg
nag/kg
ug/kg
nag/kg
nag/kg
nag/kg
Blank
Result
ND
ND
ND
ND
ND
RD
ND
ND
ND
ND
ND
ND
RD
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Reporting
Limit Footnotes
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
50
5.0
5.0
5.0
50
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
50
10
5.0
10
5.0
112-Tetrachioroethane
i22-Tetrachloroetne
Tetrachioroethene
Toluene123-Trichlorobenzana
12 4-Trichlorobenzene111-Trichloroetbane112-Trichioroethane
Trichioroethene
Trichlorofluortethane123-Trichioropropano
i24-Trinaethylbenzene135-Trmmethylbenzene
Vinyl acetate
Vinyl chloride
Xylene Total
asap-Xylene
o-Xylene
Date 03129/05 Page 72 oC 79
/eAnalytical
wwwpaceiat3s corn
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Huntersyille NC 28078
Phone [phone]
Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9290353
Client Project ID West End 6228052694
9JETHOI BL7NK 925425175
Associated Lab Samples 925409708
Blank Reporting
Parameter Units Result Limit Footnotes
roluene-d8 100
4-Brantofluorobenzene 98
Dibromofluoromathaxue 103
12-Dichloroethane-d4 103
LBORAT0RY CONTROL SM.LE 925425183
tiotDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87848
REPORT OF LABORATORY ANALYSiS
This report shall not be reproduced except in lull
without the written consent of Pace Analytical Services Inc
Charlotte Certification lOs
NCWastewater 12
NC Drinkinp Water 37706
SC 99006
FL NELAP E87627
Spike LCS LCS
Units Conc jtasult %Rec Footnotes
Icetone ug/kg 100.00 114.5 115
Benzane ug/kg 50.00 48.68 97
Bromobenzeue ug/kg 50.00 50.65 101
Bromochloromethane ug/kg 50.00 50.28 101
Ercenodichioromathane ug/kg 50.00 49.01 98
Broneoform ug/kg 50.00 51.85 104
Brcenceithane ug/kg 50.00 45.75 92
2-Butanone ug/kg 100.00 94.15 94
n-Butylbanzene ug/kg 50.00 42.57 85
sec-Butylbenzene ug/kg 50.00 49.16 98
tert-Butylbanzene uglkg 50.00 49.46 99
Carbon tetrachloride ugfkg 50.00 49.79 100
Chlorobenzene ug/kg 50.00 48.93 98
Chloroetbane ug/kg 50.00 55.19 110
Chloroform ug/kg 50.00 51.40 103
Chioromethane ug/kg 50.00 42.82 86
2-Chloroto.uane uglkg 50.00 48.88 98
4-Chiorotoluene ug/kg 50.00 48.96 98
12-Dibromo-3-chloropropane ug/kg 50.00 47.08 94
Dibronrochloromethane ug/kg 50.00 48.08 96
12-Dibromoethane EDE ug/kg 50.00 49.12 98
Dibrojacenethane ug/kg 50.00 51.59 103
12-Dichlorobenzene rig/kg 50.00 50.09 100
l3-Dichlorobenzene rig/kg 50.00 47.47 95
14-Dichlorobenzene rig/kg 50.00 48.14 96
Dichlorodifluoromethane ug/kg 50.00 42.05 84
Date 03/29/05 Page 73 of 79
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
aceArzaIytic.i
www.paceiabs.com Fax [phone]
QUALITY CONTROL DATA
Lab Project Nuriber 9290353
Client Project ID West End 6228-05-2694
L7BORATORY CONTROL StXILPLE 925425183
Spike LCS LCS
______________________________Units Conc Result Footnotes
11Dichioroethane ug/kg 50.00 49.82 100
12-Dichloroethane ug/kg 50.00 47.50 95
1l-Dichloroethene ug/kg 50.00 49.68 99
cis-12-Dichloroethene ug/kg 50.00 49.81 100
trans-12Dichloroethene ug/kg 50.00 49.11 98
12Dichioropropane uglkg 50.00 51.22 102
13-Dichioropropane ug/kg 50.00 47.51 95
22-Dichioropropane ug/kg 50.00 44.61 89
11-Dichioropropene ugfkg 50.00 48.42 97
cis-13-Dichloropropene ug/kg 50.00 49.73 100
trans-13-Dichloropropene ugfkg 50.00 49.80 100
Diisopropyi ether ug/kg 50.00 52.87 106
Ethy1benene ug/kg 50.00 47.65 95
Hexachloro-13-butadjene ug/kg 50.00 49.79 100
2Hexanone nag/kg 100.00 101.3 101
Isopropylbenzene Cuneene nag/kg 50.00 52.00 104
p-Isopropyltoluene ug/kg 50.00 43.37 87
Nethylene chloride nag/kg 50.00 49.23 98
4-Methyl-2-pentaxrnna 1.BR nag/kg 100.00 106.0 106
Methyl-tert-butyl ether nag/kg 50.00 49.90 100
Naphtbalene nag/kg 50.00 43.95 88
n-Propylbenzene nag/kg 50.00 48.97 98
Styrene ug/kg 50.00 48.40 97
1112-Tetrachioroethane nag/kg 50.00 49.80 100
1122-Tetrachieroetbane nag/kg 50.00 47.84 96
Thtrachloroathene nag/kg 50.00 15.90 92
Toluene nag/kg 50.00 47.51 95
123-Trichlorobenzene nag/kg 50.00 48.28 97
l24-Trichlorobenzene ugfkg 50.00 46.44 93
111-Trichioroethane ug/kg 50.00 48.61 97
112-Trickloroethane nag/kg 50.00 50.20 100
Trichloroethene nag/kg 50.00 47.40 95
Trichlorofluoromethane ug/kg 50.00 44.55 89
123-Trichloropropane nag/kg 50.00 48.26 96
124-Trimethylbenzeue nag/kg 50.00 43.93 88
135-Triixiethy1benze nag/kg 50.00 44.93 90
Vinyl acetate nag/kg 100.00 102.2 102
Date 03/29/05 Pa 74 79
Ashevifle Certif cat ion Os REPORT OF LABORATORY ANALYSIS Chaiotte Certification OsNCWastewater40Thisreport shall not be reproduced except in tell NC Wastewater 12NCDrinkingWater37712wfthutthe wrttten consent of Pace Analytical Seivices Inc NC Drinking Water 37706SCEnvironmental99030SC99006FLNELAPE87648FLNELAPE87627
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vu/c NC 28078
Phone [phone]
Fax [phone]
LABORATORY CONTROL SAMPLE 925425183
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Vinyl chloride
Xylene Total
mp-Xyiene
o-Xylene
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
12-Dichloroethane-d4
LCS
Rec Footnotes
94
96
95
99
100
98
101
102
shmilIe Cerifica08jD
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 90030
FLNELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in tell
without the written consent of Pace Analytical Services Inc
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
Spike LCS
Units Cotic Result
ug/kg 50.00 46.84
uglkg 150.00 144.4
ugfkg 100.00 95.03
ug/kg 50.00 49.40
Date 03/39/05 Page 75 of 79
Pace Analytical Seriices Inc
aceAnalyticar 98ooKIKe
Phone [phone]
Fax.[phone]
QUALITY CONTROL DATA
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
QC Batch 123978 analysis Method EPA 6010
QC Batch Method EPA 3050 3nalysis Description Metals Trace ICP
Associated Lab Samples 925409500 925409518 925409534
METHOD BLANK 925415598
Associated Lab Samples 925409500 925409518 925409534
Blank Reporting
Parameter Units Result Limit Footnotes
Chromium mg/kg ND 0.20
Lead mg/kg ND 0.50
LABOBATORY CONTROL SAMPLE 925415606
Spike LCS LCS
Parameter Units Conc Result Footnotes
Chromium mg/kg 50.00 45.50 91
Lead mg/kg 50.00 42.50 85
MATRIX SPIKE MATRIX SPIKE DUPLICATE 925415614 925415622
925410748 Spike MS MSD MS HSDParameterUnitsResultConcResult Result 3Rec aRec RPD Footnotes
Chromium mg/kg 3.900 71.74 64.04 53.87 84 77 17
Lead mg/kg 1.718 71.74 57.52 54.00 78 80
SAMPLE DUPLICATE 925415986
925410755 DTJP
Units Result Result BPD Footnotes
Chromium mg/kg 3.400 3.000 12
Lead mg/kg 1.500 2.200 41
Date 03129/05 Page 76 79
IIe-CeifijionID REPORT OF LABORATORY ANALYSIS Otiarfotte Certification lOsNCWastewater40ThisrepOlmacacNCWastewatar12NCDrinking Water 37712 without the written consent at Pace Analytical Ssvices Inc
NC Drinking Water 37706SCEnyironnientaj99030SC99006FLNELAPE87648FLNELAP-E87627
Pace Analytical Serilces Inc
aceAnalyticar
9800 KIYA 8Io
wpaabstrnt Phone [phone]
Fax.[phone]
QUALITY CONTROL DATA
Lab Project Number 9290353
Client Project ID Nest End 622805-2694
QC Batch 123921 Analysis Method 9u Moisture
QC Batch Method Analysis Description
Percent Moisture
Associated Lab Samples 925409500 925409518 925409534 925409575 925409583
925409591 925409609 925409617 925409625 925409633
925409641 925409658
SAMPLE DUPLICATE 925413098
925407645 flU
Parameter Units Result Result RPD footnotes
Percent Moisture 19.40 20.00
Date 03/29/05
Page 77 of 75
ication IDA REPORT OF LABORATORY ANALYSIS ariofte CeflificajpjDNCWastewater40Thisreport shall not be reproduced except in full NC Waslewater 12NCDrinkingWater37712wIthout the written consent of Pace Analytical Services inc NC Drinking Water 37708SCEnvironmental99030SC99006FLNELAPE87648FLSJELAPE87627
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 KincoyAvenue Suite 100
Hunt ersyille NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project XD West End 6228-05-2694
QC Batch 123929 Inalysis Method 9s Moisture
QC Batch Method Analysis Xescription
Percent Moisture
Associated Lab Samples 925409666 925409674 925409682 925409690 925409708
925409716 925409724
SALE DUPLICATE 925413270
Parameter
Percent Moisture
925409666
Units Result
12.40
DUP
Result
19.70
ohoyi Is Certification IDs
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NC Drinking Water 37712
Sc Environmental 99030
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REPORT OF LABORATORY ANALYSIS
This report shall net be reproduced except intuit
without the written consent of Pace Analytical ServIces Inc
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paceIeicoxn
RPD
46
Pootnotes
Oute 03/29/05 Page 78 79
12eAnaMICaI
QUALITY CONTROL DATA PARATER FOOTNOTES
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax[phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Consistent with EPA guidelines unrounded concentrations are displayed
and have been used to calculate Rec and RPD values
LCSD
WSD
DUP
ND
NC
MDL
RPD
Laboratory Control Sample Duplicate
Matrix Spike Duplicate
Sample Duplicate
Not detected at or above adjusted reporting limit
Not Calculable
Estimated concentration above the adjutited method detection limit and below the adjusted reporting limit
adjusted Method Detection Limit
Relative Percent Difference
Surrogate
The spike recovery was outside acceptance limits for the MS and br MSD due to matrix interference The LCS
and/or LCSD were within acceptance limits shoving that the laboratory is in control and the data is
acceptable
12 The calculated BPD was outside QC acceptance limits
The surrogate recovery was outside QC acceptance limits due to matrix interference
The surrogate and/or spike recovery was outside acceptance limits
Date 03/29/05 Page 79 of 79
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This report shaH not be reproduced accept in full
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FL NEIAP E87627
SAMPLE CONDITION
Temp in
Received on lcejJN
Seated Cooler YINl
Samptes Intac1J
PceAnaIyticai
www.paceiah.c.m
_________________________________________________________FleponTo
Required Client Information Section tz -kr Page of
Company \-c.1 Copy To
______________________Client Information Check quote/contract jJ V-.Y
in raw .la
The
Section
Chain-of-Custody Is LEGAL DOCUMENT All relevant fields must be completed accurately3632
To Be Completed by
Pace Analytical and Client SectIon
Quote Reference
j._CT c___
lolce To
P.O
Requested Due Date TAT5.JyTumaroundtimelessthan14days subject to
laboratory and contractual obligations and may result In
Project Manager
Pmject
Project Na Rush Turnaround Surcharge Profiles-i-c_r Turn Around lime ifAT in calendar daysFaxPectNbO-r0 //Section Required Client Information Codes
PreservativesDRINKINGWATEROWLI1GROUNDWATEROWDO
SURFACEWATER SWluWASTEWATERWWPRODUCT J0 COLLECTED CoOnebox
START
Sample IDs MUST BE UNIQUE OThER OT DATE TIME DATE TIME RomarkpLablo
fE IllIIi.I2IJ 3-/r1IIIIIIIIII45.7OO1----I ILoG__1IID_Z-I11 ____cp_
$5 1100 Vj
.I _e1 el4k
GA NPDES GROUND WATER El gNKINo WATER
Hi 4/ier SC I-fl 1d
SAMPLE NOTES
Additional Commôæts
P$u I.
PRINT Name7-bf /Duuc Sr2c8TbATESignedDDYY
SEE RE1RSE SIDE FOR INSTRUCTIONS Form COCOI Rev 0304
March 30 2005
Mr Rob Poster
Mactec
2801 Yorlanont Road
Suite 100
Charlotte NC 28208
RE Lab Proiect Number 9290677
Client Project ID West End 6228-05-2694
Dear Mr Poster
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Huntersvi/Ie NC 28078
Phone [phone]
Fax [phone]
Enclosed are the analytical results for samples received by the laboratory on March 23 2005hereinconformtothemostcurrentMELACstandardswhereapplicable unless otherwise narratedthereport
If you have any questions concerning this report please feel free to contact me
Sincerely
Results reported
in the body of
1nnette Scott
Znnette Scott@pacelaba .com
Project Manager
Enclosures
tjn
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in lull
without the written consent of Pace Analytical Services Inc
litil
NC Wastewater 12
NC Drinking Water .37706
SC 99006
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ifc tin
NC Wastewater 40
NC Drinking Water 37712
SC Environniental 00030
FLNELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Puce Analytical Services Inc
idac
iacthtte Certification IDs
NC Wastewater 12
NC Drinking Water .37706
SC 99006
FLNELAP E87627
Pace Analytical Sarilces Inc
9800 KinceyAvenue Suite 100
Huntersvilte NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290677
Client Project ID West End 6228-05-2694
..Lab Sample No 925426504 Project Sample Number 9290677-001 Date Collected 03/23/05 1440ClientSampleID9567-3 Matrix Water Date Received 03/23/05 1710
Parameters Results Units Report LimitGC/MS Seinivolatjles
Extractables in Water by 625 Prep/Method EPA 625 SF EPA 625
Acenaphthene ND ug/l 5.0 1.0 03/28/05 2201 BET 83-32-9
Acenaplithylene ND ugh 5.0 1.0 03/28/05 2201 BET 208-96-8AnthraceneNDugfl5.0 1.0 03/28/05 2201 BET 120-12-7BeruzidjneNDug/l 50 1.0 03/28/05 2201 BET 92-87-5BenzokflezorantheneNDug/1 5.0 1.0 03/28/05 2201 BET 207-08-9BenzobfluorantheneNDugh5.0 1.0 03/28/05 2201 BET 205-99-2BenzoaanthraceneNDug/l 5.0 1.0 03/28/05 2201 BET 56-55-3BenzoghiperyleneNDug/l 5.0 1.0 03/28/05 2201 BET 191-24-2BenzoapyreneNDug/l 5.0 1.0 03/28/05 2201 BET 50-32-8
4-Bromophenylpheny ether ND ug/1 5.0 1.0 03/28/05 2201 BET 101-55-3ButylbenzylphthalateNDug/l 5.0 1.0 03/28/05 2201 BET 85-68-74-Chloro-3-methylphenol ND ugh 5.0 1.0 03/28/05 2201 BET 59-50-7bis2-Chloroethoxymethane ND ugh 5.0 1.0 03/28/05 2201 BET 111-91-1bis2-Chloroethyl ether ND up/i 5.0 1.0 03/28/05 2201 BET 111-44-4bis2-Chloroisopropyl ether ND up/i 5.0 1.0 03/28/05 2201 BET 39638-32-92-Chloronaphthalene ND ug/1 5.0 1.0 03/28/05 2201 BET 91-58-72-Chlorophenol ND ug/l 5.0 1.0 03/28/05 2201 BET 95-57-8
4-Clilorophenyiphenyl ether ND ug/l 5.0 1.0 03/28/05 2201 BET 7005-72-3ChryseneNDug/l 5.0 1.0 03/28/05 2201 BET 218-01-9DibenzahanthraceneNDup/i 5.0 1.0 03/28/05 2201 BET 53-70-3l2-Dicliiorobenzeae ND ug/l 5.0 1.0 03/28/05 2201 BET 95-50-1l3-Djchlorobenzene ND up/i 5.0 1.0 03/28/05 2201 BET 541-73-114-Dichlorobenzene ND ugh 5.0 1.0 03/28/05 2201 BET 106-46-733-Dichlorobenzjdine ND ug/l 10 1.0 03/28/05 2201 BET 91-94-124-Dichiorophenol ND ug/l 5.0 1.0 03/28/05 2201 BET 120-83-2DiothylplithalateNDug/1 5.0 1.0 03/28/05 2201 BET 84-66-224-Dionethylplienol ND ug/1 5.0 1.0 03/28/05 2201 BET 105-67-9DimethyiplithalateNDugh5.0 1.0 03/28/05 2201 BET 131-11-3Di-n-butylphthalate ND ug/l 5.0 1.0 03/28/05 2201 BET 84-74-24G-Dinitro-2-methy1phenol ND ug/l 25 1.0 03/28/05 2201 BET 534-52-124-Dinitrophexiol ND ug/l 25 1.0 03/28/05 2201 BET 51-28-524-Dinitrotoluene ND up/i 5.0 1.0 03/28/05 2201 BET 121-14-22E-Dinitrotoluene ND up/i 5.0 1.0 03/28/05 2201 BET 606-20-2Di-n-octylphthalate ND up/i 5.0 1.0 03/28/05 2201 BET 117-84-0bis2-Ethyihexyiplithalate ND up/i 5.0 1.0 03/28/05 2201 BET 117-81-7FluorantheneNDugh5.0 1.0 03/28/05 2201 BET 206-44-0FluoreneNDugh5.0 1.0 03/28/05 2201 BET 86-73-7
Qital_RegLmt
Page of 23
nate 03/30/05
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunte isv/lie NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290677
Client Project ID West End 6228-05-2694
Lab Sample No 925426504
Client Sample ID 9567-3
Project Sample Number 9290677-001
Matrix Water
Date Collected 03/23/05 1440
Date Received 03/23/05 1710
Hexachloro-i -butadjene
Hexachlorobenzene
Eexachlorocyciopentadiene
Hexachioroethane
Indenoi 23-cd pyrene
Isophorone
Naphthaiene
Nitrobenzene
2-Nitrophenol
-Nitrophenol
N-Nitrosodimethyiaxnine
N-Nitroso-di-n-propyiamine
N-Nitrosodiphenylamine
Pentachiorophenol
Phenanthrerne
Phenol
Pyrene124-Trichlorebenzene
24 6-Trichiorophenol
Nitrobezizene-d5
-Fluorobiphenyl
Terphenyi-d14
Phenol-d5
2-Fluorophenol246-Tribromophenol
Date Extracted
GC Seinivolatj.eg
EPH in Water by Mass Method
Aliphatic C09-C18
Aliphatic C19-C36
Aromatic Cil-22
2-Fluorobiphenyl
-Bromonaphthaiene
Nonatrjacontane
o-Terphenyi
Date Extracted
5.0 1.0 03/28/05 2201 BET
5.0 1.0 03/28/05 2201 BET
10 1.0 03/28/05 2201 BET
5.0 1.0 03/28/05 2201 BET
5.0 1.0 03/28/05 2201 BET
5.0 1.0 03/28/05 2201 BET
5.0 1.0 03/28/05 2201 BET
5.0 1.0 03/28/05 2201 BET
5.0 1.0 03/28/05 2201 BET
25 1.0 03/28/05 2201 BET
5.0 1.0 03/28/05 2201 BET
5.0 1.0 03/28/05 2201 BET
5.0 1.0 03/28/05 2201 BET
25 1.0 03/28/05 2201 BET
5.0 1.0 03/28/05 2201 BET
5.0 1.0 03/28/05 2201 BET
5.0 1.0 03/28/05 2201 BET
5.0 1.0 03/28/05 2201 BET
5.0 1.0 03/28/05 2201 BET
1.0 03/28/05 2201 BET
1.0 03/28/05 2201 BET
1.0 03/28/05 2201 BET
1.0 03/28/05 2201 BET
1.0 03/28/05 2201 BET
1.0 03/28/05 2201 BET
03/24/05
87-683
118-74-i
77-474
67-72-1
193-39-5
78-59-i
91-203
98-953
8.8-755
100-02-7
62-759
621-64-7
86306
87865
85-018
10 8-95-2
129-00-0
120-82-i
88-06-2
4165-60-0
21-60-8
1718-51-0
4165-62-2
57-12-4
iD
NC Wastewater 40
NC Drinking Water 37712
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FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduceit except in full
without the written consent of Pace Analytical Seivicex Inc
ficatinlDs
NCWastewater 12
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FL NELAP E87627
wwwpaoelabsccom
Results Units Report Limit DF Analyzed By CAS No ReQLmt
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
50
53
64
16
22
57
.03/24/05
Prep/Method
170
170
340
136
169
61
80
03 /2 5/05
ug/i
ugh
ugh
up/i
tag/i
ug/1
up/i
up/i
up/i
up/i
up/i
up/i
up/i
up/i
up/i
up/i
ug/i
up/i
up/i
EPA 3510
up/i
up/i
ugh
EPH
100 1.0 03/30/05 1345 KES
100 1.0 03/30/05 1346 KBS
100 1.0 03/30/05 1346 KBS
10 03/30/05 1346 KES 321-60-8
1.0 03/30/05 1346 EBB 580-13-2
1.0 03/30/05 1346 EBS 7194-86-7
1.0 03/30/05 1346 EBB 84-isi
03 /2 5/05
Date 03/30/05 MOe oC 23
Lab Sample No 925426504
Client Sample ID 9567-3
Parameters
GC Volatiles
Purgeable Aromatics
Benzeue
Chiorobesizene
12 -Dichlorobenzene
13 -Dichlorobennene
l4-Dichlorobenzene
Diisopropyl ether
Ethylbsnzene
Methyl -tert-butyl ether
Toluene
Xylene Total
mp-Xylene
o-Xylene
l-Chloro-3 -fluorobenzene
ND ugh
ND ug/l
ND ugh
ND ugh
ND ugh
ND ugh
ND ug/l
ND up/i
ND up/i
ND up/i
ND up/i
ND ug/i
98
100 1.0 03/25/05
100 1.0 03/25/05
100 1.0 03/25/05
1.0 03/25/05
1.0 03/25/05
1754 DEW
1754 DEW
1754 DEW
1754 DHW
1754 DEW
Date Collected 03/23/05 1440
Date Received 03/23/05 1710
Oate 03/30/05
Page of 23
ConlDNCWastewater40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be repreiuced except in full
without the written consent of Pace Analytical Services Inc
itit all
NC Wastewater 12
NC Drinking Water .37706
SC 99006
FL NELAP E87027
wwpaoeIabsrorn
Pace Analytical Services Inc
9800 Kiiicey 4venue Suite 100
Hunters v/lie NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290677
Client Project ID West End 6228-05-2694
Project Sample Number 9290677-001
Matrix Water
Results Unite Reoort Litnit .Q
Method EPA 602
Analyzed By CAS No QjL ReLmt
1.0 10 03/27/05 0941 PPM 71-43-2
1.0 1.0 03/27/05 0941 PPM 108-90-7
10 1.0 03/27/05 0941 PPM 95-50-1
1.0 1.0 03/27/05 0941 PPM 541-73-1
1.0 1.0 03/27/05 0941 PPM 106-46-7
1.0 1.0 03/27/05 0941 PPM 108-20-3
1.0 1.0 03/27/05 0941 PPM 100-41-4
1.0 1.0 03/27/05 0941 PPM 1634-04-4
1.0 1.0 03/27/05 0941 PPM 108-883
1.0 1.0.03/27/05 0941 PPM 1330-20-7
2.0 1.0 03/27/05 0941 PPM
1.0 1.0 03/27/05 0941 PPM 95-47-6
1.0 03/27/05 0941 PPM 625-98-9
VPI6 in Water by Mass Method Method VPH
Aliphatic C05-C08 ND up/i
Aliphatic C09-Cl2 ND up/i
Aromatic C09-Clo ND ugh
25-Dibromotoluene PID 92
25-Dibromotoluene PID 88
Ana/yticar
wvM.paceJabs.com
Lab Project Number 9290677
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NO 28078
Phone [phone]
Fax [phone]
Client Project ID West End 6228-05-2694
Lab Sample No 925426512
Client Sample ID 9567-i
Project Sample Number 9290677-002
Matrix Water
03/28/05
03/28/05
03 /2 8/05
3/2 8/05
03 /2 8/05
03/28/05
03 /2 8/05
03/28/05
03/28/05
DateCoilected 03/23/05 1510
Date Received 03/23/05 1710
CAS No QiL RegLmt
83-32-9
208-96-8
120-12-7
92-875
207-08-9
205-99-2
56-55-3
191-24-2
50-32-8
101-55-3
85-68-7
59-50-7
111-91-1
111-44-4
39638-32-9
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
95-50-1
541-73-1
106-46-7
91-94-1
120-83-2
131-11-3
84-74-2
534-52-1
51-28 -5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
etinD
NC Wastewater 40
NC Drinking Water 37712
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FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproducecl.except in full
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NC Waslewater 12
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Parameters Results Units Report Limit Analyzed ByGC/MS Semivolatiles
Extractabies in Water by 625 Prep/Method EPA 625 SF EPA 625
Acenaphthene ND up/i 5.0 1.0 03/28/05 2236 BET
Acenaphthyiene ND ugh 5.0 1.0 03/28/05 2236 BET
Itnthracene ND ugh 5.0 1.0 03/28/05 2236 BET
Benzidine ND ugh 50 1.0 03/28/05 2236 BETBenzokfluorantheneNDugh5.0 1.0 03/28/05 2236 BET
Benzobfluoranthene ND up/i 5.0 1.0 03/28/05 2236 BET
Benzoaanthracene ND ugh 5.0 1.0 03/28/05 2236 BET
Benzoghiperyiene ND up/i 5.0 1.0 03/28/05 2236 BET
Benzoapyrene ND up/i 5.0 1.0 03/28/05 2236 BET
4-Bromophenyiphenyl ether ND ug/i 5.0 1.0 03/28/05 2236 BET
Butylbenzylphthalate ND up/i 5.0 1.0 03/28/05 2235 BET
4-Chloro-3-methyiphenoi ND ug/i 5.0 1.0 03/28/05 2236 BET
bis2-Chloroethoxymethane ND ug/i 5.0 1.0 03/28/05 2236 BET
bis2-Chioroethyi ether ND up/i 5.0 1.0 03/28/05 2236 BET
bis2-Chioroiaopropyl ether ND ug/1 5.0 1.0 03/28/05 2236 BET
2-Chloronaphthalene ND up/i 5.0 1.0 03/28/05 2236 BET
2-Chiorophenol ND ugh 5.0 1.0 03/28/05 2236 BET
4-Chiorophenylphenyi ether ND ug/1 5.0 1.003/28/05 2236 BET
Chrysene ND ugh 5.0 1.0 03/28/05 2236 BETDibenzahanthraceneNDup/i 5.0 1.0 03/28/05 2236 BET
l2-Dichiorobenzene ND up/i 5.0 1.0 03/28/05 2236 BET
13-Dichlorobenzene ND ugh 5.0 1.0 03/28/05 2236 BET14-Djchlorobenzene ND up/i 5.0 1.0 03/28/05 2236 BET
33-Dichlorobenzjdine ND up/i 10 1.0 03/28/05 2236 BET24-Dichiorophenol ND up/i 5.0 1.0 03/28/05 2236 BET
Diethylphthalate ND up/i 5.0 1.0 03/28/05 2236 BET 84-66-224-Dimethylphenol ND up/i 5.0 1.0 03/28/05 2236 BET 105-67-9DimethylphthalateNDugh5.0 1.0 2236 BET
Di-n-butylphthaiate ND ugh 5.0 1.0 2236 BET
4E-Dinitro-2-methylphenol ND up/i 25 1.0 2236 BET
24-Dinitrophenol ND up/i 25 1.0 2236 BET24-Djujtrotoluene ND ugh 5.0 1.0 2236 BET26-Dinitrotolue MD up/i 5.0 1.0 2236 BETDi-n-octyiphthalate ND up/i 5.0 i.0 2236 BETbis2-Ethylhexyiphthaiate ND up/i 5.0 1.0 2235 BETFluoramtheneNDup/i 5.0 1.0 2236 BETFiuoreneNDup/i 5.0 1.0 03/28/05 2236 BET 86-73-7
Date 03/20/05
Page oC 23
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax[phone]
GC Semivolati.es
EPE in Water by Mass Method
Aliphatic C09-c18
Aliphatic C19-C36
Aromatic C1l-22
-F.uorobiphenyl
2-Brornonaphthalene CS
Nonatrjacontaxse
o-Terpheuyl Cs
Date Extracted
100 1.0 03/30/05
100 1.0 03/30/05
100 1.0 03/30/05
1.0 03/30/05
1.0 03/30/05
1.0 03/30/05
1.0 03/30/05
03/25/05
1428 BS
1428 NDS
1428 KBS
1428 ICES
1428 ICES
1428 ICES
1428 ICBS
iishevile CertiflcattoçjpNCWastewater40
Nc Drinking Water 37712
SC Enviroertinotal 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report Shall net be reprothiced except In full
without the written consent of Pace Analytical Services Inc
IfItiI
NC Wastewater 12
NC Dlinking Water 37706
SC 99006
FL NELAP E87627
7eAnaIYticaI
www pacelabs corn
Lab Sample No 925426512
Client Sample ID 9567-1
Lab Project Number 9290677
Client Project ID West End 6228-05-2694
Date Collected 03/23/05 1510
Date Received 03/23/05 1710
malvzed By CAS No QiL ReLmtHexachloro-1 -butadiene
Rexachlorobenzene
Rexachiorocyc lopentadiene
Hexachloroethane
Indenol23-cdpyrene
Isophorone
Naphthalene
Nitrobenzene
2-Nitrophenol
-Nitrophenol
N-Nitrosodimethylamine
N-Ni troso-di -n-propylanuine
N-I0itrosodiphenylamine
Pentactalorophenol
Phenanthrene
Phenol
Pyrene124-Trichlorobenzene
246 -Trich.orophenol
Nitrobenzene-d5
-Fluorobiphenyl
Terphenyl-d14 CS
Phenol-d5 IS
2-Pluorophenol246-Tribromophenol
Date Extracted
Project Sample Number 9290677-002
Matrix Water
Results Units Report Limit DF _________
5.0 1.0 03/28/05
5.0 1.0 03/28/Os
10 1.0 03/28/05
5.0 1.0 03/28/05
5.0 1.0 03/28/05
5.0 1.0 03/28/05
5.0 1.0 03/28/05
50 1.0 03/28/05
5.0 1.0 03/28/05
25 1.0 03/28/05
5.0 1.0 03/28/05
5.0 1.0 03/28/05
5.0 1.0 03/28/05
25 1.0 03/28/05
5.0 1.0 03/28/05
5.0 1.0 03/28/05
5.0 1.0 03/28/05
5.0 1.0 03/28/05
5.0 1.0 03/28/05
1.0 03/28/05
1.0 03/28/05
1.0 03/28/05
1.0 03/28/05
1.0 03/28/05
1.0 03/28/05
.03/24/05
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
2236 BET
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
48
51
76
15
19
67
03/24/05
Prep/Method
170
ND
ND
125
146
43
61
03/25/05
ug/l
ugh
ug/l
ug/l
ug/1
ug/l
ug/1
ug/l
ugh
ug/l
ug/l
ug/l
ug/l
ug/1
ugh
ug/l
ug/l
ug/l
ug/l
EPA 3510 EPH
ug/l
ug/1
ug/l
87-683
118-74-1
77-47-4
67-72-1
193-39-5
8-59-1
91-20-3
98-953
88-75-5
100-02-7
62-75-9
62 1-64-7
86-30
87-86-5
85-01-8
10895-2
12900-0
12082-1
8-062
4165-60-0
321-60-B
1718-51-0
4165-62-2
367-12-4
321-60-8
580-13-2
7194-86-7
84-15-1
Date 03/30/05
Page 23
Analyticar
WwMtpaceIabscom
Paie Analytical Sarvices Inc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290677
Client Project ID West End 6228-05-2694
Lab Sample No 925426512
Client Sample ID 9567-1
Project Sample Number 9290677-002
Matrix Water
Date Collected 03/23/05 1510
Date Received 03/23/05 1710
Parameters
GC Volatiles
Purgeable Aromatics
Benzene
Chlorobenzeue
12-Dichlorobenzeue
13 -Dichlorobenzecue
14 -Dichiorobensene
Diisopropyl ether
Ethylbensene
Methyl-tert-butyl ether
Toluene
Xylene Total
mp-Xylene
o-Xylene
1-Chloro-3 -fluorobensene
ND ug/1
ND ug/l
ND ugh
ND ugh
ND ugh
ND ugh
ND ug/l
ND ug/l
ND ugh
ND ug/l
ND ug/1
ND ugh
103
1.0 1.0 03/27/05
1.0 1.0 03/27/05
1.0 1.0 03/27/05
1.0 1.0 03/27/05
1.0 1.0 03/27/05
1.0 1.0 03/27/05
1.0 1.0 03/27/05
1.0 1.0 03/27/05
1.0 1.0 03/27/05
2.0 1.0 03/27/05
1.0 1.0 03/27/05
1.0 03/27/05
1023 PPM
1023 PPM
1023 PPM
1023 PPM
1023 PPM
1023 PPM
1023 PPM
1023 PPM
1023 PPM
1023 PPM
1023 PPM
1023 PPM
Data 03/30/05
100 1.0 03/25/05
100 1.0 03/25/05
100 1.0 03/25/05
1.0 03/25/05
1.0 03/25/05
1922 DEW
1922 DEW
1922 DEW
1922 DEW
1922 DEW
Page 23
on Do
NC Wastewator 40
NC Drinking Water 37712
SC Environniental 99030
FL NELAP E67648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Cefiti
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
Results Units Report Limit UF
Method EPA 602
na1yzed By CAS No QL ReniLntt
1.0 1.0 03/27/05 1023 PPM 71-43-2
108-90-7
95-501
541-73
106-46 -7
108-20-3
100-41-4
163 4-04-4
108-88-3
133 0-20-7
95-476
625-98-9
VPH in Water by Mass Method Method VPH
Aliphatic C05-C08 ND ugh
Aliphatic C09-Cl2 ND ugh
Aromatic C09-ClO ND ugh
25-Dibronjotoluene PID 95
25-Dibromotoluene PID 99
Lab Sample No 925426520
Client Sample ID 9567-2
Extractabies in Water by 625
Acenaphthene
Acenapbthylene
Pnthracene
Benzidjne
Benzo fluoranthene
Benco fiuorathene
Benzo axsthracene
Benzogh iperylene
Benzo pyrene
-Bronsophanylphenyl ether
Butyibenzylphthalate
4-Chloro-3-inethylphenoi
his -Chloroethoxymethaxse
bia2-Ch.oroethyl ether
bia 2-Chloroisopropyl ether
.-Chloronaphthaiene
-Chlorophenol
4-Chiorophenyiphenyl ether
Chrysene
Dibenzahanthracene
12 -Dichiorobensene
3-Dichlorobenzene
4-Dichiorobexuzene
33 -Dichlorobenzjdiue
24 -Dichloropherso
Diethyiphthalate
24 -Dimethylphenoi
Dimethylphtha.ate
Di-n-butyiphthalate
6-Dinitro-2 -methyiphenol
4-Dinitrophenol
4-Dinitrotoiuene
6-Dinitrotoiuene
Di -n-octyiphthalate
his -Ethylhexyi plithalate
Fluorantbene
Fluorene
Project Sample Number 9290677-003
Matrix Water
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
10 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
1.0 03/28/05 2310 BET
Date Collected 03/23/05 1600
Date Received 03/23/05 1710
83-32-9
08-96-8
12 0-12-7
92-87-5
07-08-9
205-99-2
56-55-3
191-24-2
50-32-8
101-55-3
85-68-7
9-50-7
111-91 -1
111-44-4
39638-32-9
1-58-7
5-57-8
005-72-3
218-01-9
53 -70-3
95-50-1
541-73-1
106-46-7
91-94-1
12 0-83-2
84-662
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
06-44-0
86-73-7
Qi_Reglimt
Ic ion ID
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shaH not berepreducect except in full
without the wiitten consent of Pace Analytical Services Inc
tth
Charlotte CertificafftIS
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP 587627
wwwpacelabs.com
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hw7tersville NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290677
Client Project ID West End 6228-05-2694
Parameters
GC/MS Semivoatiies
Results Units AeDort Limit
Prep/Metho6 EPA 625 SF EPA 625
Anvnri ran
ND up/i 5.0
ND ugh 5.0
ND up/i 5.0
ND up/i 50
ND tog/i 5.0
ND up/i 5.0
ND up/i 5.0
ND ug/l 5.0
ND up/i 5.0
ND up/i 5.0
ND up/i 5.0
ND ug/l 5.0
ND up/i 5.0
NI up/i 5.0
ND ugh 5.0
ND up/i 5.0
ND up/i 5.0
ND up/i 5.0
ND up/i 5.0
ND up/i 5.0
ND up/i 5.0
ND up/i 5.0
ND up/i 5.0
ND ugh 10
ND up/i 5.0
ND up/i 5.0
ND up/i 5.0
ND up/i 5.0
ND up/i 5.0
ND ugh 25
ND up/i 25
ND ug/l 5.0
ND up/i 5.0
ND ug/l 5.0
ND tog/i 5.0
ND up/i 5.0
ND ugh 5.0
Date 03/30/05
Page oi 23
eAnaIYticawepaceIacem
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290677
Client Project ID West End 6228-05-2694
Lab Sample No 925426520
Client Sample ID 9567-2
Project Sample Number 9290677-003
Matrix Water
Date Collected 03/23/05 1600
Date Received 03/23/05 1710
AshevilleCertjflcatjon IDs
NC Wastewater 40
NC DrinkinO Water 37712
SC Environmental 99030
FLNELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be roproducet except in lull
without the written consent of Pace Analytical Services Inc
Ctlarite Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
Results Units Report Limit DF Analyzed By CAS No
Hexachloro-i3-butarIjena ND up/i 5.0 1.0 03/28/05 2310 BET 87-68-3
Mexachlorobenzene ND ug/l 5.0 1.0 03/28/05 2310 BET 118-74-1
Rexachiorocyciopentadiene ND up 10 1.0 03/28/05 2310 BET 77-47-4
Hexachioroethane ND ugh 5.0 1.0 03/28/05 2310 BET 67-72-1
Indenol23-cdpyrene ND ug/l 5.0 1.0 03/28/05 2310 BET 193-39-5
Isophorone ND up/i 5.0 1.0 03/28/05 2310 BET 78-59-1
Naphthalene ND up/i 5.0 1.0 03/28/05 2310 BET 91-20-3
Nitrobanzene ND up 5.0 1.0 03/28/05 2310 BET 98-95-3
2-Nitrophenol ND ugh 5.0 1.0 03/28/05 2310 BET 88-75-5
4-Nitrophenol ND up/i 25 1.0 03/28/05 2310 BET 100-02-7
N-Nitrosodimethyiamine ND up/i 5.0 1.0 03/28/05 2310 BET 62-75-9
N-Nitroso-di-n-propylamine ND ugh 5.0 1.0 03/28/05 2310 BET 621-64-7
N-Nitrosodiphenyiamine ND ugh 5.0 1.0 03/28/05 2310 BET 86-30-6
Perstachiorophenol ND ugh 25 1.0 03/28/05 2310 BET 87-86-5
Phenanthrene ND up/i 5.0 1.0 03/28/05 2310 BET 85-01-8
Phenol ND up/i 5.0 1.0 03/28/05 2310 BET 108-95-2
Pyrezee ND ug/i 5.0 1.0 03/28/05 2310 BET 129-00-0
124-Trichiorobeneene ND ug/1 5.0 1.0 03/28/05 2310 BET 120-82-1
246-Trichioropheno ND ug/l 5.0 1.0 03/28/05 2310 BET 88-06-2
Nitrobenzene-d5 47 1.0 03/28/05 2310 BET 4165-60-0
2-Pluorobiphenyl 47 1.0 03/28/05 2310 BET 321-608
Terphenyi-d14 65 1.0 03/28/05 2310 BET 1718-51-0Phenol-d5 18 1.0 03/28/05 2310 BET 4165-62-2
2-Piuorophenoi 23 1.0 03/28/05 2310 BET 367-12-4
246-Tribrounophenol 56 1.0 03/28/05 2310 BETDateExtracted03/24/05 03/24/05
GC Semivolatiles
EPH in Water by Mass Method Prep/Method EPA 3510 EPH
Aliphatic C09-C18 640 up/i 100 1.0 03/30/05 1511 HBSAiiphaticC19-C36 140 up 100 1.0 03/30/05 1511 KBSAromaticC11-22 170 up/i 100 1.0 03/30/05 1511 KBS
2-Pluorobiphenyi 133 1.0 03/30/05 1511 KBS 321-60-82-Bromonaphthalenes i98 1.0 03/30/05 1511 ICBS 580-13-2Nonatriacontane471.0 03/30/05 1511 KBS 7194-86-7o-Terphenyl 86 1.0 03/30/05 1511 EBS 84-15-1DateExtracted03/25/05 03/25/05
QL RegLmt
Page of 23
Bate 03/30/05
VPB in Water by Mass Method
Aliphatic C0S-c08
Aliphatic C09 -C12
Aromatic C09-C1O
25-Dibromotoluene FlU
25-Dibromotoluene PID
100 1.0 03/25/05 2006 DHW
100 1.0 03/25/05 2006 DHW
100 1.0 03/25/05 2006 DEW
1.0 03/25/05 2006 DEW
1.0 03/25/05 2006 DEW
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shah not be reproduced except in full
without the written consent of Pace Analytical Services Inc
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
Lab Sample No 925426520
Client Sample ID 9567-2
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290677
Client Project ID West End 6228-05-2694
Project Sample Number 92Gi677-0O3
Matrix Water
Date Collected 03/23/05 1600
Date Received 03/23/05 1710
Results Units Report Limit __Analyzed By CAS No QL ReLmt
Method EPA 602
Parameters
GC Vo.atiles
Purpeable Aromatics
Benzene
Ctilorobenzene
12 -Dichlorobenzene
13 -Dichlorobenzene
4-Dichlorobenzene
Diisopropyl ether
Ethylbenzene
Methyl-tert-butyl ether
Toluene
Xylene Total
mp-Xylene
o-Xylene
1-Chloro-3 -fluorobenzene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
99
Method VPB
ug/l
up/i
up/i
up/i
ug/l
up/i
ug/i
ug/l
ug/l
ug/l
up/i
ug/1
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
.1.0
1.0
2.0
1.0
1105
1105
1105
1105
1105
1105
1105
1105
1105
1105
1105
1.0 03/27/05
1.0 03/27/05
1.0 03/27/05
1.0 03/27/05
1.0 03/27/05
1.0 03/27/05
1.0 03/27/05
1.0 03/27/05
1.0 03/27/05
1.0 03/27/05
1.0 03/27/05
1.0
1.0
PPM
PPM
PPM
PPM
PPM
PPM
PPM
PPM
PPM
PPM
PPM
71-432
108-90-7
95-501
541-73-1
106-46-7
108-20-3
100-41-4
1634-04-4
108-88-3
1330-20-7
03/27/05 1105 PPM 95-47-6
03/27/05 1105 PPM 625-98-9
ND ug/l
ND up/i
ND ugh
93
107
Date 03/30/05
Page of 23
9800 KinceyAvenue Suite 100
Hunters yule NC 28078
Pace Analytical Services Inc
Phone [phone]wwpaJabsixrmFax704.875.9091
Lab Project Nuonberz 9290677
Client Project ID West End 6228-05-2694
PARAMETER FOOTNOTES
Dilution factor shown represents the factor applied to the reported result and reporting limit due to changes
in sample preparation dilution of the extract or moisture content
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic
testing was performed at our Pace Charlotte laboratory unless otherwise footnoted
Method 907lB modified to use ASE
All pM Free Chlorine Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediateholdtime
1W Not detected at or above adjusted reporting limit
NC Not Calculable
Estimated concentration above the adjusted method detection limit and below the adjusted reporting
limitMDLAdjustedMethodDetectionLimit
Surrogate
The surrogate recovery was outside QC acceptance limits due to matrix interference
The surrogate and/or spike recovery was outside acceptance limits
Oate 03/30/05
Page 10 of 23
gjll9yjjflatD REPORT OF LABORATORY ANALYSIS otteCititinlNCWastewater40Thisreport shall nat be reproduced except in full NC Wastewater 12NCDrinkingWater37712without the written consent of Pace Analytical Services Inc NC Drinking Water 37706SCEnvironmental99030SC99006FLNELAPE87648FLNELAPE87627
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Huntesvilie NC 28078
Phone [phone]
Fax[phone]
Lab Project Number 9290677
Client Project ID West End 6228-05-2694
QC Batch 121834 Analysis Method EPE
QC Batch Method EPA 3510 Analysis Description
EPE in Water by Mass Method
Associated Lab Samples 925426504 925426512 925426520
METHOD BLANtC 925437139
Associated Lab Samples 925426504 925426512 929426520
Blank ReportingParameterUnitsResultLimit Footnotes
Aliphatic C09-Cl8 ugh ND 100
Aliphatic C19-C36 ug/l ND 100
Aromatic Cll-22 ug/l ND 100
2-Fluorobiphenyl 83
2-Bromonaphthalene 102
Nonatriacontane 41
o-Terphenyl 52
LABORATORY CONTROL SABPLE 925307852
Spike LCS LCS
Parameter Units Conc Result %Rec Footnotes
Aliphatic C09-C18 up/i 300.00 264.0 88
Aliphatic C19-C36 ugh 400.00 578.8 145
Aromatic Cil-22 ugh 850.00 729.1 86
2-Fluorobiphenyl 111
2-Bromonaphthalene 84
Nonatriacontane 71
o-Terphenyl 94
LABORATORY CONTROL SAO.PLE 925437147
Aliphatic C09-C18
Aliphatic C19-C36
Aromatic C11-22
-Fluorobiphenyl
2-Bromonaphthalene
LCS
Footnotes
48
84
55
Oate 03/30/05
Page of 23
llicjnlD
NC Wastewater 40
NC Driekin9 Water 37712
SC Environmental 99030
FLNELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced except In full
wrthout the written consent of Pace Analytical Services Inc
Ct1tte_Certuiication IOn
NCwastewater 12
NC Drinking Wafer .37706
SC 99006
FL NELAP 87827
Wwpace1ai$.om
Spike LCS
Units Cone Result
up/i 300.00 143.9
up/i 400.00 336.8
ugh 850.00 468.7
96
92
Arialyticar
www.paelabcom
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Huntersvilie NC 28078
Phone [phone]
Fax [phone]
La Project Number 9290677
Client Project ID West End 6228-05-2694
LABORATORY CONTROL SAMPLE 925437147
Spike LCS LCS
Parameter Units Conc Result FootnoteE
Nonatriacontane 40
o-Terphenyl 61
MATRIX SPIRE MATRIX SPI1E DUPLICATE 925307860 925307878
Parameter
Aliphatic C09-C18
Aliphatic C19-C36
Aromatic C11-22
2-Fluorobiphenyl
-Bromonaphthalene
Nonatriacontane
o-Terphenyl CS
MS MSD MS MSD
Result Result Rec Rec
343.0 480.5 53 76
898.7 844.0 110 103
1299 1296 76 76
109 116
100 73
58 52
93 71
RPD Footnotes
33
AshevilleCertftjcatipn IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall riot be reprodoced except in lull
without the written consent of Pace Analytical Services Inc
Charlotte Certification
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
925306441 Spike
Units Result Conc
ug/l 27.57 600.00
ugh 20.03 800.00
up/i 1700.00
Date 03/30/05
Page 12 of 23
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunters vu/c NC 28078
Phone [phone]
Fax [phone]
Lab Project Njber 9290677
Client Project ID West End 6228-05-2694
QC Batch 124345 Analysis Method VPH
QC Batch Method VPII Analysis Description VPI9 in Water by Mass MethodAssociatedLabSamples925426504925426512 925426520
METHOD BLANK 925436909
Associated Lab Samples 925426504 925426512 925426520
Blank ReportingParameterUnitsResultLimit Footnotes
Aliphatic C05-C08 up/i MD 100
Aliphatic C09-C12 ug/l ND 100
Aromatic C09-C10 ugh ND 100
25-Dibromotoluene FID 95
25-Djbromotoluene PID 103
LANORJLTORY CONTROL SAMPLE LCSD 925436917 925436925
Spike LCS LCSD LCS LCSDParameterUnitsConcResultResult%Rec RPD FootnotesAliphaticC05-C08 ugh 400.00 459.5 445.8 115 iiiAliphaticC09-C12 ugh 100.00 122.2 112.7 122 113AromaticC09-Cl0 ug/l 100.00 119.1 111.6 119 11225-Dibromotoluene FID 136 11825-Dibromotoluene PID 139 125
SAMPLE DUPLICATE 925436933
Parameter
Aliphatic cO5-co8
Aliphatic C09-C12
Aromatic C09-ClO
2S-Dibromotoluene FID
25-Dibromotoluene PID
Footnotes
NC
NC
NC
iflonlD
NC Wastewitter 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report Shall nSt be reproduced except in full
without the written consent of Pace Analytical Services Inc
fitinlDs
NCWasfewater 12
NC Drinking Water 7706
Sc 99006
FL NELAP E87627
wwwpace1abscorn
Units
up/i
up/i
up/i
925426504 flU
Result Result
MD ND
ND ND
ND ND
92 99
88 98
Oate 03/30/05
age 13 of 23
Pace Analytical Services inc
9800 KinceyAvenue Suite 100
aceArialyticar
FaK 704875.9091
QUALITY CONrROL DATA
Lab Project Number 9290677
Client Project ID West End 6228-052694
QC Batch 124387 Analysis Method EPA 602
QC Batch Method EPA 602 Analysis Description Purgeable Aromatics
Associated Lab Samples 925426504 925426512 925426520
METHOD BLANI 925439150
Associated Lab Samples 925426504 925426512 925426520
Blank Reporting
Parameter Units Result Limit Footnotes
Benzene ug/l ND 1.0
Chlorobenzene ug/l ND 1.0
l2-Dichlorobenzene ug/l ND 1.0
l3-Dichlorobenzene ugh 1.0
l4-Dichlorobenzene ug/l ND 1.0
Diisopropyl ether ug/l ND 1.0
Ethylbenzens ugh ND 1.0
Methyl-tert-buty ether ugh MD 1.0
Toluene ug/l ND 1.0
Xylene Total ugh ND 1.0
mp-Xylene ugh ND 2.0
o-Xylene ugh ND 1.0
1-Chloro-3-fluorobenzene 100
LABORATORY CONTROL SAMPLE 925439168
Spike LCS LCS
Parameter Units Conc Result %Rec Footnotes
Benzene ug/l 20.00 19.80 99
Chlorobenzene ugh 20.00 20.47 102
l2-Dichlorobenzene ug/l 20.00 21.23 106
13-Dichlorobenzene ug/l 20.00 19.36 97
14-Dichlorobenzene ug/l 20.00 20.98 105
Diisopropyl ether ugh 20.00 19.60 98
Ethylbenzene ugh 20.00 21.48 107
Methyl-tert-butyl ether ug/l 20.00 21.50 108
Toluene ugh 20.00 20.83 104
Xylene Total ugh 60.00 64.15 107
xn.p-Xylene ug/l 40.00 43.02 108
o-Xylene ug/l 20.00 21.13 106
Date 03/30/05
Page 3.4 23
Iltjfjctonl REPORT OF LABORATORY ANALYSIS QIiticatioisNCWastewater40Thisreport shall not be reproduced except in NC Wastewater 12NCDrinking Water 37712 without the written consent 0f Pace Analytical Services Inc
NC Drinking Water .37706SCEnvironmental99030SC99006FLNELAPE87648FLNELAPE87627
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 KinceyAvnnie Suite 100
Huntersvlle NC 28078
Phone [phone]
Fax [phone]
Lab Project Ntimber 9290677
Client Project ID West End 6228-05-2694
LABORATORY CONTROL SAMPLE 925439168
Spike LCS LCS
Parameter Units Cone Result Rec Footnotes
1-Chioro-3-fluorobenzene 101
MATRIX SPIXE 925439176
925423493 Spike MS MS
Parameter Units Result Cone Result %Rec Footnotes
Benzena up/i 20.00 19.72 99
Chlorobenzaue up/i 20.00 20.14 101
12-Dichlorobenzene ugh 20.00 20.66 103
l3-Dichlorobenzene ugh 20.00 17.18 86
l4-Dichlorobenzene up/i 20.00 20.23 101
Diisopropyl ether up/i 20.00 20.23 101
Etbylbenzene up/i 20.00 21.04 105
Mathyl-tert-butyl ether ug/l 20.00 20.79 104
Toiuene ug/l 20.00 20.71 104
Xyiene Total up/i 60.00 62.12 104
mp-Xyiene up/i 40.00 41.81 104
o-Xylene up/i 20.00 20.31 102
1-Chloro-3-fluorobenze 99
MATRIX SPIKE 925439184
cationlD
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except In tull
without the written consent of Pam Analytical Services Inc
lrdac\
l1ariotte CerificpfJQ
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
wwwpaceiabs.com
925432494 Spike MS MS
Units Result Cone Result FootnotesBenzeneug/1 20.00 19.75 99Chlorobenzeneup/i 20.00 20.14 101l2-Dichlorobenzene up/i 20.00 20.75 104i3-Diehlorobenzene up/i 20.00 20.76 104
14-Dichiorobenjene up/i 20.00 20.32 102
Diisopropyl ether ug/l 20.00 19.95 100
Ethylbenzene up/i 20.00 21.15 106
Methyl-tert-butyl ether ug/l 20.00 20.84 104Tolueneugh20.00 20.76 104
Xylene Total up/i 60.00 62.75 105mp-Xylene up/i 40.00 42.10 105
Oata 03/30/05
Page 15 of 23
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290677
Client Project ID West End 6228-052694
MATRIX SPIKE 925439184
925432494 Spike MS MS
Parameter Units Result Conc Result Footnotes
o-Xyiene up/i 20.00 20.65 103
l-Chloro-3-fluorobenzene 99
SAMPLE DUPLICATE 925439192
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 90030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in tell
without the written consent of Pace Analytical Services Inc
rtifiatinls
NC Wastewater 12
NC Drinking Water 37706
S.C 99006
FL NELAP E87627
Footnotes
925432510 DUP
Units Result Result RPD
Benzene up/i 32.00 33.00
Chlorobenzene rig/i ND ND NC
12-Dichlorobenzene ugh ND ND NC
13-Dichiorobenzene ug/1 ND ND NC
14-Dichiorobensene up/i ND ND NC
Diisopropyl ether up/i ND ND NC
Ethylbensene up/i 2.700 2.800
Methyl-tert-butyl ether up/i 12.00 14.00 11
Toluene up/i ND ND NC
Xyiene Total ug/l 110.0 110.0
mp-Xylene ug/l 68.00 70.00
o-Xylene up/i 40.00 41.00
l-Chloro-3-fluorobenze 98 99
Oate 03/3e/05
Page 16 of 23
QUALITY CONTROL DATA
Pace Anayticai Serilces
Inc
9800 KinceyAvenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax[phone]
Lab Project NuMber 9290677
Client Project ID West End 6228-05-2694
QC Batch 124213
QC Batch Method EPA 625 SF
Associated Lab Samples
Analysis Method EPA 625
Analysis Description
Extractables in Water by 625
925426504 925426512 925426520
METHOD BLANK 925427601
Associated Lab Samples 925426504 925426512 925426520
rtificintDs
NC Wastewater 40
NC Drinking Water 37712
SC Eevir000Ten tat 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except ri full
without the written consent sit Pace Analytical Services Ins
hsctotte Certification Do
NCWa9tewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87027
Footnotes
Blank Reporting
Units Result Limit
Acenaphtherue ugh ND 5.0
Acenaphthylene ug/1 ND 5.0
Anthracene ugh ND 5.0
Benzidine ug/l ND 50
Benzokfli.soranthene ugh ND 5.0
Benzobfluoranthene ugh ND 5.0
Benzoaanthracene ugh ND 5.0
Bsnzoghiperylene ugh ND 5.0
Benzoapyrene ugh ND 5.0
4-Breniophenyiphenyl ether ug/l NI 5.0
Butylberuzylphthalate ug/l ND 5.0
4-Chloro-3-methylphenol ug/l NI 5.0
bis2-Chloroethoxymethane ugh ND 5.0
bis2-Chloroethyl ether ugh ND 5.0
bis2-Chloroisopropyl ether rig/i ND 5.0
2-Chloronaphthalene ugh ND 5.0
2-Chiorophenol ugh ND 5.0
4-Chiorophenyiphenyl ether tug/i ND 5.0
Chrysene ugh ND 5.0
Dibenzahanthracene ugh ND 5.0
12-Dichlorobenzene ug/ND 5.0
13-Dichiorobeozene rig/i NI 5.0
i4-Dichlorobenzane ug/i ND 5.0
33-Dichiorobaxuzjdjne rig/i ND 10
24-Dichioropheno ugh ND 5.0
Dietluylphtha.ate ugh ND 5.0
24-Dimethyiphenol up/i ND 5.0
Dimethyiphthaiate ug/ND 5.0
Di-n-butylphtha.ate rig/i ND 5.0
d6-Dixuitro-2-methylphenoi up/i ND 25
24-Dinitrophexuol ugh ND 25
Date 03/30/05
Page 17 of 23
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9290677
Client Project ID West End 6228-05-2694
METHOD BLANK 925427601
Associated Lab Saniples
CaL alItL.tL
4-Dinitrotoluene
6-Dinitrotoluene
Di-n-octylphthalate
bis2-Ethylhexylphthalate
Fluoranthene
Fluorene
Hexachloro-l -butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Bexachloroethane
Indenol23-cdpyrene
Isophorone
Naphthalene
Ni trobenzene
2-Nitrophenol
-Nitrophenol
N-Nitrosodimethylanrine
N-Ni troso-di -n -propylamine
N-Nitrosodiphenyla.mine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene124-Trichlorobenzene
246 -Trichiorophenol
Nitrobenzene-dS
2-Fluorobipheny
Terphenyl-d14
Phenol-d5
-Fluorophenol246-Tribromopheno CS
Date 03/30/05
Page 18 of 23
haticaille Certification lOs REPORT OF LABORATORY ANALYSIS Certification IDaNCWastewater40ThIsreport shall nut repmdtat lull NC Wastewater 12NCDrinkingWater37712without the written consent of Pace Analytical Services Inc NC Drinking Water .37706SCEnvironrnerttal99030SC99006FLNELAPE87648FLNRAPE87627
925426504 925426512 925426520
Blank Reporting
Units Result Limit Footnotes
ugh ND 5.0
ugh ND 5.0
ugh ND 5.0
ugh ND 5.0
ugh ND 5.0
ugh ND 5.0
ugh ND 5.0
ugh ND 5.0
ugh ND 10
ugh ND 5.0
ugh ND 5.0
ugh ND 5.0
ugh ND 5.0
ugh ND 5.0
ug/l ND 5.0
ug/l ND 25
ug/1 ND 5.0
ugh ND 5.0
uig/1 ND 5.0
ugh ND 25
ugh ND 5.0
ug/ND 5.0
ugh ND 5.0
ug/l ND 5.0
ugh ND S.D
44
50
76
17
22
63
Analyticaiw
wwwpaceIaJs.ofl
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290677
Client Project ID West End 6228-05-2694
LABORATORY CONR0L SJtPLE 925427619
Sate 03/30/05
Units
ugh
ugh
ugh
ugh
ugh
ugh
ug/
ug/1
ugh
ugh
ugh
ugh
ugh
ugh
ug/l
ugh
ugh
ugh
ugh
ugh
ug/
ug/
tog/i
ugh
ugh
ug/
tog/i
ugh
ugh
tog/i
tog/i
ugh
ugh
ug/1
tog/i
ugh
ugh
Spike
Conc
50.00
50.00
50.00
100.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
100.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
LCS
Result
29.21
30.10
35.44
1.076
34.01
35.40
35.22
35.47
33.88
34.29
35.77
28.74
29.42
27.81
29.35
29.30
22.41
33.93
34.68
35.54
25.60
23.86
24.55
27.45
27.61
37.48
14.74
35.77
38.59
62.04
56.71
40.22
37.13
34.70
35.53
35.75
33.30
Page 19 of 23
ll.itionlD
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shaH not he reproduced except in full
without the written consent of Pace Anaintical Services Inc
Chac1ott Certificafjpj
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
Parameter
Acenaphthene
Acenaphthylene
nthracene
Benzidine
Beozo fluoranthene
Beazo fluoranthene
Benzo anthracene
Benzogh iperyiene
Bonzoapyrene
4-Broxnophenylphenyi ether
Butylbenzyiphthalate
4-Chloro-3 -methyiphenol
his -Chloroethoxy methane
bis2-Chioroethyl ether
his 2-Chioroisopropyl ether
-Chioronaphthalerie
-Chlorophenol
4-Chiorophenylphenyl ether
Chrysene
Dibenzahanthracene
12 -Dichlorobenzene
3-Dichlorobenzexie
14 -Dichlorobenzene33-Dichlorobenzidjne
24 -Dichlorophenol
Diethylphthaiate
24 -Dimethylphenol
Dimethylphthalate
Di-n-butyiphthalate
6-Dinitro-2 -methylphenol
4-Dinitrophenol
24 -Dinitrotoluene
26 -Dinitrotoluena
Di-n-octyiphthalate
his 2-Bthylhexylphthaiate
Fluoranthene
Fluorene
LOS
Rec Footnotes
58
60
7113
68
71
70
71
68
69
72
58
59
56
59
59
45
68
69
71
51
48
49
27
55
75
30
72
77
124
113
80
74
69
71
72
67
QUALITY COWROL DATA
Pace Analytical Services Inc
QSUU Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
LABORATORY CONTROL SN6PLE 925427619
Lab Project Number 9290677
Client Project ID West End 6228-05-2694
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in lull
without the written consent of Pace Analytical Services Inc
Ctisilolte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
wtcpaceJabs.com
Footnotes
Hexachloro-1 -baitadiene
Hexachlorobenzena
Eexachlorocyclopentadiene
Hexachioroethane
Indeno1 23 -cdpyrene
Isophorone
Naphthalene
titrobenzene
-Nitropheno
-itrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propy.amine
N-Nitrosodiphenylamine
Pentachiorophenol
Phenanthrene
Phenol
Pyrene124-Trichlorobenzene246-Trichlorophenol
Nitrobenzene-d5
2-Fluorobiphenyl
Terphenyl-d14
Phenol-dS CS
-Fluorophenol246-Tribromophenol CS
MATRIX SPlICE MATRIX SPlICE
Spike LCS LCS
Units Conic Result
ugh 50.00 25.13 50
ugh 50.00 31.66 63
ug/50.00 18.33 37
ug/l 50.00 2266 45
ug/l 50.00 34.70 69
ug/l 50.00 31.18 62
ugh 50.00 27.05 54
ug/l 50.00 29.60 59
ugh 50.00 29.30 59
ugh 50.00 14.22 28
ugh 50.00 17.53 35
ug/l 50.00 29.56 59
ug/l 50.00 37.55 75
ugh 50.00 41.75 84
ugh 50.00 35.67 71
ugh 50.00 10.23 20
ugh 50.00 35.39 71
ugh 50.00 25.64 51
ugh 50.00 32.51 65
59
62
72
20
26
71
DUPLICATE 925427627 925427635
925426520 Spike MS MSD MS MSDUnitsResultConicResultResult%Rec RPDAcenaphtheneugh100.00 60.19 61.19 60 61Acenaphthyleaeugh100.00 55.19 58.33 55 58Anthraceneug/l 100.00 82.62 77.22 83 77Benzidineug/l 200.00
Benzokfluoranthene ugh 100.00 85.45 77.90 86 78Benzothfluoranthoneug/l 100.00 86.54 78.62 86 79 10
Oate 03/30/05
Footnotes
33
Page 20 of 23
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Iiuntersville NC 28078
Phone [phone]
Fax [phone]
MATRIX SPIKE MATRIX SPIKE DIJPLICATEt 925427627 925427635
Date 03/30/05
Lab Project Nunther 9290677
Client Project ID West End 6228-05-2694
age 21 of 23
on ID
NC Wastewater 40
NC Drinking Water 37712
Sc Environmental 09030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall net be reproduced except In tuft
without the written consent of Pace Analytical Services Inc
ificetjI
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP 587627
It4tw.paceabs.cont
925426520 Spike MS MSD MS MSD
Units Result Conc Result Result %_%jg FoothotesBenzoaanthraceneup/i 100.00 82.37 76.64 82 77Benzoghiperylelleup/i 100.00 69.11 64.92 69 65BenzoapyrexLeup/i 100.00 80.49 73.54 80 74
4-Bromophenyiphenyl ether up/i 100.00 72.45 69.36 72 69Butyibenzylphthalateup/i 100.00 85.06 80.99 85 81
4-Chioro-3-methylphenol up/i 100.00 61.34 55.94 61 56bis2-Chloroethoxymethane up/i 100.00 60.58 56.00 61 56
bis2-Chloroethyi ether up/i 100.00 139.3 126.2 139 126 10bis2-Chloroisopropy ether up/i 100.00 60.20 53.28 60 53 122-Chloronaphthalene up/i 100.00 58.18 57.55 58 58 332-Chlorophenoi up/i 100.00 45.39 39.13 45 39 15
4-Ch1oxophenyipheny1 ether ug/l 100.00 73.23 71.79 73 72Chryseneup/i 100.00 82.35 76.20 82 76Dibenzahathraceneup/i 100.00 70.00 64.74 70 65l2-Djchlorobenzene up/i 100.00 51.44 46.17 51 46 11l3-Dichlorobenzene up/i 100.00 46.82 41.78 47 42 11i4-Dichiorobenzene up/i 100.00 48.69 43.47 49 44 ii33-Eichlorobenzidine up/i 100.00 29.49 23.99 30 24 2124-Dichloropheno up/i 100.00 56.71 52.24 57 52Diethyiphtha.ate up/i 100.00 84.52 77.18 84 7724-Dimethy1phenoi tug/i 100.00 7.460 4.847 42 323Dimethyiphthaiateup/i 100.00 78.93 75.13 79 75D-n-butyiphthaiate tug/i 100.00 87.18 81.72 87 824S-Dinitro-2-snethyiphenoi up/i 100.00 140.2 125.5 140 126 ii24-Diuitropherioi up/i 100.00 130.0 119.3 130 11924-Dizajtrotoluene up/i 100.00 90.71 84.98 91 852S-Dinjtrotoiuene up/i 100.00 80.54 78.73 80 79Di-n-octylphthalate ugh 100.00 84.35 75.62 84 76 11bis2-Ethyihexyiphthalate up/i 100.00 91.58 82.54 92 82 10Pluorantheeup/i 100.00 82.52 78.25 82 78Fiuoreneup/i iOO.00 76.60 74.35 77 74Rexachloro-13-butadjene ugh 100.00 48.57 42.40 49 42 i4Hexachlorobezeneup/i 100.00 69.44 65.37 69 65Hexachlorocyciopentadjeneup/i 100.00 30.08 27.14 30 27 10Hexachioroetheup/i 100.00 44.81 39.iS 45 39 13Indenol23_cdpyrene ug/l 100.00 70.79 65.76 71 66Isopitoroneup/i 100.00 65.66 52.15 66 62
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
aceArialyticar
Ww.parelabs.corn Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9290677
Client Project ID West End 6228-05-2694
MATRIX SPIKE MATRIX SPIKE DUPLICATE 925427627 925427635
925426520 Spike MS MSD MS MSD
______________________________Units Result Conc Result Result %_%Rec RPD Footnotes
Naphthalene ugh 100.00 54.15 49.46 54 50
Nitrobenzene ugh 100.00 60.96 55.92 61 56
2-Nitrophenol ug/l 100.00 60.11 54.40 60 54 10
4-Nitrophenol ugh 100.00 70.14 61.35 70 61 13
N-Nitrosodimethylamjne ugh 100.00 36.37 31.96 36 32 13
N-Nitroso-di-n-propy.atnne ugh 100.00 61.93 57.45 62 58
N-Nitrosodiphenylamine ugh 100.00 82.09 77.46 82 78
Pentachiorophenol ugh 100.00 113.2 101.3 113 101 11
Phenanthrene ugh 100.00 78.74 74.33 79 74
Phenol ug/l 2.593 100.00 24.50 20.94 22 18 16
Pyrene ug/l 100.00 84.48 80.98 84 81
124-Trichlorobenzene ugh 100.00 50.16 45.23 50 45 10
246-Trich.orophenol ugh 1d0.00 67.95 66.01 68 66
Nitrobenzene-d5 58 53
2-Fluorobiphenyl 62 60
Terphenyl-dl4 86 72
Pheruol-d5 20 18
2-Fluorophenol 26 23
246-Tribromophenol 76 69
Date 03/30/05
Page 22 od 23
ianlD REPORT OF LABORATORY ANALYSIS CharlottgCeiatiNCWastewater40ThisrepetshallriotbereproducedexceptfullNCWastewater 12NCDrinking Water 37712 wfthout the written consent of Pace Anatytical Services Inc
NC Drinking Water 37706SCEnvironmental99030SC99006FLNELAPE87648FLNELAPE87627
QUALITY CONTROL DATA P1RANETER FOOTNOTES
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290677
Client Project ID West End 6228-05-2694
Consistent with EPA guidelines unrounded concentrations are displayed and have been used to calculate Rec and RPD values
LCS Laboratory Control Sample Duplicate
Matrix Spike Duplicate
Sample Duplicate
Not detected at or above adjusted reporting limit
Not Calculable
Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
Adjusted Method Detection Limit
Relative Percent Difference
Surrogate
The LCS recovery was outside of the acceptance rangeThecalculatedRPDwasoutsideQCacceptancelimits
The surrogate and/or spike recovery was outside acceptance limits
Asheville Certification IDe
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 9g03o
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall ant be reproduced except in full
without the written consent of Pace Analytical Services Inc
CtrloIte Certification Do
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87027
MS
DUP
ND
MC
MDL
RPD
Date 03/30/05
Page 23 of 23
..tI.J JL.U
Clierd to ma Section
Renulted Client tnfopiatort SectiontL2EirVc Jpage of
V__VV .....-
client lnromiition tciieck quotncontracIJ
To Be ComeIed by Face Analytical and Cliont Section
Quite Reference__lnvaice Ta flequesled DuO Date oect Manager
PVO Tum around less than 14 days subi Ic
laboratory 8nd conirSOlual obtgatlons and may result in
Prolect jame Rush Turnaround SumhargeIIIVVVIVVTurnAroundmmaTAnincalendar days
3ectlon RequIred Client Information %tnx Codes
Preservatives //DRlJtGWAThf3 OW VfGflOUIDWATEROW4OçcEn /\7/pnooucT COLIEGTEO cc /s.f/\V/Olie character per box 77i4Y/Sample IDa MUST BE UNIQUE UT TIME rt.r Vi/il RemsrKsILabIDthITTIA__L$It iIIiiuii____
Li ii
____
__
/.V0
f2
//3
--
---------
XIcXZ
F.RCRA
NOTES
GA
thor_________
COI4UITION
naC
ed on Ice YIN
Cooler YiN
as Intact tY1NJ
ial Comments
DCOther_I _VVJVV
5Jf ofSAMPLER DATE Slgnd MM DO VY15
Data File /chem/hpmsd6.i/032805.b/03280522.d
Report Date 29-Mar-2005 1127
Pace Analytical Services Charlotte
TENTATIVELY IDENTIFIED COMPOUNDS
Page
Client Name 92-MAQTEC
Lab Smp Id 925426504
Operator BET
Sample Location
Sample Matrix WATER
Analysis Type SV
Number TICs found
Client SDG 9290677
Client Smp ID 9567-3
Sample Date 23-MAR-2005
Sample Point
Date Received 23-MAR-2005 0000LevelLOW
CONCENTRATION UNITS
ug/L or ug/KG ug/L
CAS NUMBER COMPOUND NAME RT EST CONC
Data File /chem/hprnsd6.i/032805.b/03280523.d
Report Date 29-Mar-2005 1130
Pace Analytical Services Charlotte
TENTATIVELY IDENTIFIED COMPOUNDS
Page
Client Name 92MACTEC
Lab Smp Id 925426512
Operator BET
Sample Location
Sample Matrix WATER
Analysis Type SV
Number TICs found
Client SDG 9290677
Client Smp ID 9567-1
Sample Date 23-MAR-2005
Sample Point
Date Received 23-MAR--2005 0000LevelLOW
CONCENTRATION UNITS
ug/L or ug/KG ug/L
CAS NUMBER RT
12.353
13 159
EST CONC
12
5.25
COMPOUND NAME
C-13 or larger alkane
C-14 or larger alkane
Pata File /chem/hprnsd6.i/032805.b/03280524.d
Report Date 29-Mar-2005 1128
Pace Analytical Services Charlotte
TENTATIVELY IDENTIFIED COMPOUNDS
Page
Client Name 92-MACTEC
Lab Srnp Id 925426520
Operator BET
Sample Location
Sample Matrix WATER
Analysis Type SV
Number TICs found
Client SDG 9290677
Client Smp ID 9567-2
Sample Date 23-MAR-2005
Sample Point
Date Received 23-MAR-2005 0000
Level LOW
CONCENTRATION UNITS
ug/L or ug/KG ug/L
CAS NUMBER COMPOUND NAME RT EST CONC
Pace Analytical Services Inc
9800 KinceyAvenue Stile 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9291338
Client Project ID West End/6228-05-2694
Results Units Report Limit DF analyzed By CAB No ReaLant
Wet Chemistry
Percent Moisture Method 9a Moisture
Percent Moisture 22.7 1.0 04/06/05 0835 TNS
GCIS Semivolatiles
Samivolatile Organics
Aeengphthene
Aeenaphthylene
Retbracene
Benzok fluoranthene
Benzo fluoranthene
Benzoa anthracene
Benzoic acid
Benzoghiperylene
Benzyl alcohol
Benzoapyrene
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Clnloro-3-metbylphenol
4-Ch1oroaii1ine
big 2-Chloroethoxymethane
big 2-Chioroethyl ether
bis2-Chloroisopropyl ether
2-Chloronaphthalene
2-Chiorophenol
4-Cblorophenylphenyl ether
Chrysene
Dibenz ah anthracene
Dibenzofuran
12 -Dichlorobenzene
13 -Dichlorobonzene
4-Dichlorobenzene33-Dichlorobenzjdine
4-Dichlorophenol
Diethylphthalate
24-Dimethyiphenol
Dimethylphthalate
Di-n-butylphthalate
6-Dinitro-2-methylphenol
Psineville Certification IDe REPORT OF LABORATORY ANALYSIS Charlotte Certification IDsNCWastewater40ThisreportshallnstbereproducedexceptinfullNCWastewater12NCDrinkingWater37712without the written consent of Pace Analytical Services NC Drinking Water 37706SCEnvironmental99030..SC 99006FLNELAPE87648FLNELAPE87627
Lab Sample No 925467417
Client Samp.e ID 9567-2
Project Sample Number 9291338002
Matrix Soil
Date Collected 04/04/05 1100
Date Received 04/04/05 1550
Prep/Method EPA 3545 EPA 8270
ND ug/kg 430 1.3 04/06/05 1900 BET 83-329
ND up/kg 430 1.3 04/06/05 1900 BET 208968
ND up/kg 430 1.3 04/06/05 1900 BET 120-127
ND up/kg 430 1.3 04/06/05 1900BET 207089
ND up/kg 430 1.3 04/06/05 1900 BET 205992
ND up/kg 430 1.3 04/06/05 1900 BET 56-553
ND ug/kg 2100 1.3 04/06/05 1900 BET 65850
ND ugfkg 430 1.3 04/06/05 1900 BET 191242
ND ug/kg 850 1.3 04/06/05 1900 BET 100516
ND ug/kg 430 1.3 04/06/05 1900 BET 50328
ND ug/kg 430 1.3 04/06/05 1900 BET 101-553
ND up/kg 430 1.3 04/06/05 1900 BET 85687
ND nag/kg 850 1.3 04/06/05 1900 BET 59-507
ND ug/kg 850 1.3 04/06/05 1900 BET 106-478
ND ug/kg 430 1.3 04/06/05 1900 BET 111-911
ND up/kg 430 1.3 04/06/05 1900 BET 111444
ND nag/kg 430 1.3 04/06/05 1900 BET 3963832-9
ND ug/kg 430 1.3 04/06/05 1900 BET 91587
ND ug/kg 430 1.3 04/06/05 1900 BET 95578
ND up/kg 430 1.3 04/06/05 1900 BET 700572-3
ND nag/kg 430 1.3 04/06/05 1900 BET 218019
ND up/kg 430 1.3 04/06/05 1900 BET 53703
ND nag/kg 430 1.3 04/06/05 1900 BET 132649
ND nag/kg 430 1.3 04/06/05 1900 BET 95-50-1
ND nag/kg 430 1.3 04/06/05 1900 BET 541731
ND up/kg 430 1.3 04/06/05 1900 BET 106-467
ND ug/kg 850 1.3 04/06/05 1900 BET 91-94-1
ND up/kg 430 1.3 04/06/05 1900 BET 120832
ND ug/kg 430 1.3 04/06/05 1900 BET 8466-2
ND nag/kg 430 1.3 04/06/05 1900 BET 105679
ND ug/kg 430 1.3 04/06/05 1900 BET 131113
ND nag/kg 430 1.3 04/06/05 1900 BET 84-742
ND nag/kg 430 1.3 04/06/05 1900 BET 534-52-1
Date 04/08/05 Page of 40
eAnaiyticaI
wpezabs.com
Pace Analytical Services inc
9800 Kincey Avenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9291338
Client Project ID West End/6228-05-2694
Lab Sample No 925467417
Client Sample ID 9567-2
Project Sample Number 9291338-002
Matrix Soil
Date Collected 04/04/05 1100
Date Received 04/04/05 1550
1.304106/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.3 04/06/05 1900 BET
1.0 04/06/05 1900 BET
1.0 04/06/05 1900 BET
1.0 04/06/05 1900 BET
1.0 04/06/05 1900 BET
1.0 04/06/05 1900 BET
1.0 04/06/05 1900 BET
51285
121142
606202
117840
122667
117 817
206440
6-737
87683
118-741
77-474
67721
193395
78-591
91-576
95-487
91203
88744
99092
100016
98953
88755
100 027
621647
86306
87865
85018
108952
129000
120821
95954
88062
4165600
321608
1718510
4165622
367 -124
sireille Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmerrtal 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
ibis report shall ent be reproduced except
in tell
without the written consent of Pace Analytical Services Inc
Cherlotte Certification Dx
NcWastewater 12
NC Drinking Water 37705
SC 99006
FLNELAP E87627
Xiteort Limit 7enalvzed By CJS No
4-Dinitrophenol
4-Dinitrotoluene
6-Dinitrotoluene
Di-n-octylphthalate
2-Diphenylhydrazine
bis 2-Ethylhexylphthalate
Fluoranthene
Pluorene
Bexachloro-13 -butadiene
Rexachlorobenzene
Hexachlorccyclapentadiene
Rexachloroethane
Indemo12 3-cdpyrene
Isophorona
2-Methylnaphthalene
2-Methyiphenol o-Creaol
34-Methylphenol
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobensene
2-Nitrophexiol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphanylaanina
Pentachlorophenol
Phenanthrene
Phenol
Pyrene124-Trichlorobenzene245-Trichlorophenol246-Trichlorophenol
Nitrobenzene-d5
2-Fluorobiphenyl
Terphenyl-dl4
Phenol-d5
2-Fluorophenol
246-Tribromophenol
OSte 04/08/05
2100
430
430
430
430
430
430
430
430
430
430
430
430
430
430
430
430
430
2100
2100
2100
430
430
2100
430
430
2100
430
430
430
430
430
430
Results
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
45
44
62
43
36
40
Units
ug/kg
sag/kg
sag/kg
ug/kg
ug/kg
uglkg
sag/kg
sag/kg
sag/kg
sag/kg
sag/kg
sag/kg
sag/kg
sag/kg
ug/kg
sag/kg
sag/kg
sag/kg
sag/kg
sag/kg
sag/kg
sag/kg
ug/kg
sag/kg
sag/kg
sag/kg
sag/kg
sag/kg
sag/kg
sag/kg
sag/kg
sag/kg
sag/kg
Sf
QWn_RecLmt
Page of 40
Pace Analytical Sflrvices Inc
9800 Kincey Avenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9291338
Client Project ID West End/6228-05-2694
Date Extracted 04/04/05
Units Report Limit __ltnalvzed
04/04/05
Qa._RegLmt
GC Seinivolatiles
EPE in Soil by Mass Method
Aliphatic C09-C18
P1iphatic ClS-C36
.romatic C11-22
2-Fluorobiphenyl
2-Rromonaphthalene
Nonatriacontana
o-Terphenyl
Date Extracted
GC Volatiles
VPH in Soil by Mass Method
Aliphatic C05C08
Aliphatic C09C12
ltromatic C09-C10
25-Dibromotoluene PID
23-Dibramotoluene PIP
9.6 1.0 04/06/05 1751 DEW
9.6 1.0 04/06/05 1751 DEW
9.6 1.0 04/06/05 1751 DEW
1.0 04/06/05 1751 DEW
1.0 04/06/05 1751 DEW
321608
580132
7194867
84151
ion Dx
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not De reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certification lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELItP E87627
wwwpaciabsCon
Lab Sample No 925467417
Client Sample ID 9567-2
Project Sample Number 9291338-002
Matrix Soil
Date Collected 04/04/05 1100
Date Received 04/04/05 1550
13 1.3 04/07/05 0833 NDS
13 1.3 04/07/05 0833 KBS
13 1.3 04/07/05 0833 NDS
1.0 04/07/05 0833 NDS
1.0 04/07/05 0833 XBS
1.0 04/07/05 0833 KBS
1.0 04/07/05 0833 RBS
04/05/05
Prep/Method
ND
NP
ND
20
116
96
61
04/05/03
Method VPH
ND
ND
ND
134
132
Method EPA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
EPA 3550 EPH
mg/kg
mg/kg
mg/kg
xx
xx
xx
mg/kg
mg/kg
mg/kg
xx
xx
8260
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
sag/kg
GC/MS Volatiles
GCIPL5 VOCs 5035/8260 low level
acetone
Banzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromof arm
Brontamethane
2-Butanone MEK
n-Butylbenzezse
sac-Butylbeuzene
tert-Butylbenzene
Carbon tetrachlorjde
Chlorobenzarae
Chloroethane
Chloroform
Chloroxnathane
Iwte 04/os/os
96
4.8
4.8
4.8
4.8
4.8
9.6
96
4.8
4.8
4.8
4.8
4.8
9.6
4.8
9.6
1.0 04/06/05 1519 RWS
1.0 04/06/05 1519 RWS
1.0 04/06/05 1519 RWS
1.0 04/06/05 1519 RWS
1.0 04/06/05 1519 RWS
1.0 04/06/05 1519 RWS
1.0 04/06/05 1519 EWE
1.0 04/06/05 1519 RWS
1.0 04/06/05 1519 RWS
1.0 04/06/05 1519 RWS
1.0 04/06/05 1519 RWS
1.0 04/06/05 1519 RWS
1.0 04/06/05 1519 RWS
1.0 04/06/05 1519 RWS
1.0 04/06/05 1519 EWS
1.0 04/06/05 1519 RWS
67641
71432
108861
7497
75274
75252
74839
8933
104518
135 88
98066
56235
108907
5003
67663
74873
Page of 40
/eAnaIyticar
wwpaCeabS corn
Pace Analytical Services Inc
9800 Kiricey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9291338
Client Project ID West End/6228-05-2694
Lab Sample No 925467417
Client Sample ID 95672
Project Sample Number 9291338002
Matrix Soil
Date Collected 04/04/05 1100
Date Received 04/04/05 1550
Date 04/98/05 Page 40
Asheville Certification ID
NC Wastevater 40
NC Drinking Water 37712
Sc Environmental 99030
FLNELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certification IDe
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
Results Units Report Limit PP lenalvzed By CAS No ReLmt
2Chlorotoluene ND nag/kg 4.8 1.0 04/06/05 1519 RWS 95498
4Chiorotoluene ND nag/kg 4.8 1.0 04/06/05 1519 RWS 106-43-4
l2-Dibromo-3-chloropropane ND nag/kg 4.8 1.0 04/06/05 1519 RWS 96-128
Dibromochlornethana ND üg/kg 4.8 1.0 04/06/05 1519 RWS 124-48-1
l2Dibrmsoethane EPa ND nag/kg 4.8 1.0 04/06/05 1519 RWS 106-93-4
Dibromomethane ND nag/kg 4.8 1.0 04/06/05 1519 RWS 74953
l2Dichlorobenzene ND nag/kg 4.8 1.0 04/06/05 1519 RWS 95-501
l3Dichlorobenzene ND nag/kg 4.8 1.0 04/06/05 1519 RWS 541-73-1
l4-Dichlorobenzene ND nag/kg 4.8 1.0 04/06/05 1519 RWS 106-46-7
Dichlorodifluoroasethane ND nag/kg 9.6 1.0 04/06/05 1519 RWS 75718
11-Dichioroethane ND ug/kg 4.8 1.0 04/06/05 1519 RWS 75343
12Dichloroethane ND ug/kg 4.8 1.0 04/06/05 1519 RWS 107-06-2
ll-Dichloroethene ND nag/kg 4.8 1.0 04/06/05 1519 RWS 75-35-4
cisl2-Dichloroethene ND nag/kg 4.8 1.0 04/06/05 1519 RWS 15659-2
trans-12Djchloroethene ND nag/kg 4.8 1.0 04/06/05 1519 RWS 15660-5
12-Dichioropropane ND nag/kg 4.8 1.0 04/06/05 1519 RWS 78-87-5
13-Dichloropropane ND nag/kg 4.8 1.0 04/06/05 1519 RWS 142-28-9
22Dichloropropane ND nag/kg 4.8 1.0 04/06/05 1519 RWS 594-20-7
l1Dichloropropene MD nag/kg 4.8 1.0 04/06/05 1519 RWS 563-586
cisl3-Dichloropropene ND nag/kg 4.8 1.0 04/06/05 1519 RWS 10061015
trans-l3-Dichloropropene ND nag/kg 4.8 1.0 04/06/05 1519 RWS 10061026
Dilsopropyl ether ND nag/kg 4.8 1.0 04/06/05 1519 RWS 108-203
Ethylbenzene ND nag/kg 4.8 1.0 04/06/05 1519 RWS 100-41-4
Bexachloro-.13butadiane ND nag/kg 4.8 1.0 04/06/05 152.9 RWS 87683
2Hexanone ND nag/kg 48 1.0 04/06/05 1519 RWS 59178-6
Isopropylbenzene Cumene MD nag/kg 4.8 1.0 04/06/05 1519 RWS 98-82-B
p-Isopropyltolnaene ND nag/kg 4.8 1.0 04/06/05 1519 RWS 99676
Nethylene chloride ND ug/kg 4.8 1.0 04/06/05 1519 RWS 75-092
4Methyl-2-pentanone MIBK ND nag/kg 48 1.0 04/06/05 1519 RWS 108-10-1
Nethyltertbutyl ether ND nag/kg 4.8 1.0 04/06/05 1519 RWS 1634044
Naphtbalene MD nag/kg 4.8 1.0 04/06/05 1519 RWS 91-203
n-ropylbenzene ND ug/kg 4.8 1.0 04/06/05 1519 RWS 103-65-1
Styrene MD nag/kg 4.8 1.0 04/06/05 1519 RWS 100-425
1l12-petrachloroatae ND nag/kg 4.8 1.0 04/06/05 1519 RWS 630-206
1122Thtrachloroetbane ND nag/kg 4.8 1.0 04/06/OS 1519 RWS 79-34-5
Tetrachloroethene ND nag/kg 4.8 1.0 04/06/05 1519 RWS 127184
o1naene ND nag/kg 4.8 1.0 04/06/05 1519 RWS 10888-3
123-Trjchlorobenzene ND nag/kg 4.8 1.0 04/06/05 1519 RWS 8761-6124rrichlorobenzeueNDnag/kg 4.8 1.0 04/06/05 1519 RWS 12082-1
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunters vOle NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9291338
Client Project ID West End/6228-05-2694
Lab Sample No 925467417
Client Sample ID 9567-2
Project Sample Number 9291338-002
Matrix Soil
Date Collected 04/04/05 1100
Date Received 04/04/05 1550
UnIts ReDort Limit _fl Jnalyzed By CAS No ReaLmt
4.8 1.0 04/06/05 1519 RWS
4.8 1.0 04/06/05 1519 RWS
4.8 1.0 04/06/05 1519 RWS
4.8 1.0 04/06/05 1519 ROtS
4.8 1.0 04/06/05 1519 ROtS
4.8 1.0 04/06/05 1519 RWS
4.8 1.0 04/06/05 1519 RWS
48 1.0 04/06/05 1519 RWS
9.6 1.0 04/06/05 1519 ROtS
4.8 1.0 04/06/05 1519 RWS
9.6 1.0 04/06/05 1519 ROtS
4.8 1.0 04/06/05 1519 RWS
1.0 04/06/05 1519 ROtS
1.0 04/06/05 1519 ROtS
1.0 04/06/05 1519 ROtS
1.0 04/06/05 1519 ROtS
95476
2037-26-5
460004
1868-53-7
170 60070
Date 04/08/05
AshevilleCertificationlDs
NC Wastewater 40
NC Drioldng Water 37712
SC Environmental 99030
FLNELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shot nut be reproduced except ri lull
without the written consent of Pace Analytical Services Inc
Ctariofle Certification IDe
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
Paae 10 of 40
11-Trichloroethane
112-Trichloroethane
Trichloroethene
Trichlorofluornethane123-Trichloropropane
l24-Trimethylbanzene135-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene Total
xnp-Xylene
o-Xylene
Toluene-d8
4-Bromofluorobamsane
Dibromofluoromathane
l2-Djchloroethane-d4
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND tag/kg
ND ug/kg
ND ug/kg
ND uglkg
ND ug/kg
ND tag/kg
ND tag/kg
ND ug/kg
99
97
98 54
98 54
71556
79005
79016
75694
6-184
95636
10 8678
108054
75014
1330-207
Pace Analytical Serilcu Inc
9800 Kincey Avenue Suite 100
luntersviIe NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9291338
Client Project ID West End/6228052694
Lab Sample No 925467425
Client Sample ID 95671
Project Sample Number
9291338-003
Matrix Soil
Date Collected 04/04/05 1115
Date Received 04/04/05 1550
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
Results Units Report Limit DF Znalyzed Bv CAS No QL ReaLmt
Method 96 Moisture
13.8 1.0 04/06/05 0835 TNS
Date 04/08/05 Page 11 at 40
Asheville Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSfS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certification lOs
NC Wastewater 12
tIC Drinking Water 37706
SC 99006
FL NELAP E87627
wviw.paceJab corn
GC/MS Semivo.atiles
Semivolatile Organics Prep/Method EPA 3545 EPA 8270
Acenaphthene ND tog/kg 380 1.2 04/06/05 1938 BET 83-329
Acenaphthylene ND tog/kg 380 1.2 04/06/05 1938 BET 20896-8
Anthracene ND tog/kg 380 1.2 04/06/05 1938 BE 12012-7
Benzokfluoranthene ND tog/kg 380 1.2 04/06/05 1938 BET 20708-9
Benzobfluoranthene ND ug/kg 380 1.2 04/06/05 1938 BET 20599-2
Benzoaanthracene ND tog/kg 380 1.2 04/06/05 1938 BET 56-553
Benzoic acid ND tog/kg 1900 1.2 04/06/05 1938 BE 65850
Benzoghiperylene ND tog/kg 380 1.2 04/06/05 1938 BET 19124-2
Benzyl alcohol ND tog/kg 770 1.2 04/06/05 1938 BET 100-51-6
Benzoapyrene ND tog/kg 380 1.2 04/06/05 1938 BET 50-32B
4-Bromophenylpheny3 ether ND tog/kg 380 1.2 04/06/05 1938 BET 101-55-3
Butylbenzylphthalate ND ug/kg 380 1.2 04/06/05 1938 BET 85687
4-Chloro-3methylphenol ND tog/kg 770 1.2 04/06/05 1938 BET 59507
4-Chloroaniline MD tog/kg 770 1.2 04/06/05 1938 BET 106-478
bis2Chloroethozymethane ND tog/kg 380 1.2 04/06/05 1938 BET 11191-1
bis2-Chloroethyl ether ND tog/kg 380 1.2 04/06/05 1938 BET 111-44-4
bis2-Chloroisopropyl ether ND tog/kg 380 1.2 04/06/05 1938 BET 39638329
2-Chloronaphthalene ND tog/kg 380 1.2 04/06/05 1938 BET 91-587
2-Chlorophenol ND tog/kg 380 1.2 04/06/05 1938 BET 95578
4-Chlorophenylphenyl ether ND tog/kg 380 1.2 04/06/05 1938 BET 700572-3
Chrysene ND tog/kg 380 1.2 04/06/05 1938 BET 218-01-9
Dibenzahanthracene ND tog/kg 380 1.2 04/06/05 1938 BE 53703
Dibenzofuran ND tog/kg 380 1.2 04/06/051938 BET 13264-9
12-Dichlorobenzene ND tog/kg 380 1.2 04/06/05 1938 BET 95501
13-Dichlorobenzene ND ug/kg 380 1.2 04/06/05 1938 BET 541731
14-Dichlorohenzene ND tog/kg 380 1.2 04/06/05 1938 BET 10646-7
33Dichlorobenzidine ND tog/kg 770 1.2 04/06/05 1938 BET 91941
24-Dichlorophenol ND tog/kg 380 1.2 04/06/05 1938 BET 120832
Diethylphthalate ND tog/kg 380 1.2 04/06/05 1938 BET 84-66-2
24Dimethylphenol MD tog/kg 380 1.2 04/06/05 1938 BET 105679
Dimethylphthalate MD tog/kg 380 1.2 04/06/05 1938 BET 131-11-3
Di-n-btotylphthalate ND tog/kg 380 1.2 04/06/05 1938 BET 84742
46-Dinitro-2methylphenol ND tog/kg 380 1.2 04/06/05 1938 BE 534521
/eAnaIyticar
wwvpabsnom
Pace Analytical Sen/ices Inc
9800 KinceyAvenue Suite 100
Hunters yule NC 28078
Phone [phone]
FaK 704875.9091
Lab Project Number 9291338
Client Project ID West End16228-05-2 694
Lab Sample No 925467425
Client Sample ID 9567-1
Project Sample Number 9291338-003
Matrix Soil
Date Collected 04/04/05 1115
Date Received 04/04/05 1550
4-Dinitrophenol
4-Dinitrotoluene
6-Dinitrotoluene
Di-n-octylphthalate
2-Diphenylhydrazine
his 2-Ethylhezylphthalate
Fluoranthene
luorene
Itexachlor-1 -butadiene
Bexachiorocyclopentad lane
Hexachioroethane
Indeno12 3-cdpyrena
Isophorone
2-Methylnaphthalene
24tethylphenol o-Cresol
34Methylphenol
Naphthalene
2-Nitroaniline
-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophanol
4-Nitrophenol
N-Nitroso-di-n-propylamjne
N-Nitrosodiphenylaagjne
Pentachlorophenol
Phenanthrene
Phenol
Pyrane124-Trichlorobenzene245-Tich1orophenol246-Trichlorophenol
Nitrobenzene-d5 CS
2-Pluorobiphenyl
Terphenyl-d14
Phenol-d5
2-Fluorophenol CS
246-Tribromophenol CS
ND i.sg/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/k
ND uglkg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ugfkg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ugfkg
ND uglkg
ND ug/kg
ND ugfcg
48
32
73
50
47
61
_________nalvzed By
1900 1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.2 04/06/05 1938 BET
1.0 04/06/05 1938 BET
1.0 04/06/05 1938 BET
1.0 04/06/05 1938 BET
1.0 04/06/05 1938 BET
1.0 04/06/05 1938 BET
1.0 04/06/05 1938 BET
CbS No Qp_RegLmt
5128
121-14-2
60620
117840
122-667
117-81-7
206440
6737
87 683
118741
77 -474
67721
193395
7859
9157
95487
91203
88744
99092
100016
9895
88755
100027
62164-7
8630
87865
85 018
108952
129000
120-82-1
9595
88062
4165600
321608
1718510
4165622
36712
leertificat9nlfl
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Anahdical Services IncSt
Charlotte Certification tDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
Results Units Report Limit DF
380
380
380
380
380
380
380
380
380
380
380
380
380
380
380
380
380
1900
1900
1900
380
380
1900
380
380
1900
380
380
380
380
380
380
Oate 04/08/05 Page 12 of 40
/1ceAnafyticar
wpaca1bs.com
Pace Analytical Seriices inc
9800 KinceyAvenue Suite 100
Huntersvila NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9291338
Client Project ID West End/6228-05-2694
Lab Sample No 925467425
Client Sample ID 9567-1
Project Sample Number 9291338003
Matrix Soil
Date Collected 04/04/05 1115
Date Received 04/04/05 1550
GC Semivolatiles
in Soil by Mass Method
Aliphatic C09-C18
Aliphatic C19-C36
Aromatic C1122
2-Fluorobiphenyl
2-Bromonaphthalene
Nonatriacontane
o-Terphenyl
Date Extracted
Date 04/08/05 Page 1.3 oC 40
AshevllleCertificationlfls
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87646
REPORT OF LABORATORY ANALYSiS
This report shall sot be reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certification IDa
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E07627
Date Extracted
Parameters Units ReDort Limit DF Analyzed By CAS No Qg ReLnut
04/04/05
12 1.2 04/08/05
12 1.2 04/08/05
12 1.2 04/08/05
1.0 04/08/05
1.0 04/08/05
1.0 04/08/05
1.0 04/08/05
04/07/05
7.9 0.8 04/07/05
GC Volatiles
VPE in Soil by Mass Method
Aliphatic C05C08
Aliphatic C09C12
Aromatic C09-C10
25-Dibroaotoluene FIDS
5-Dibromotoluene PID
GC/MS Vo3.atiles
GC/MS VOCs 5035/8260 low level
Aratone
Benzene
Bromobeuzene
04/04/05
Prep/Method
23
ND
ND
46
115
104
83
04/07/OS
Method VPH
29
110
37
103
98
Method EPA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
MID
ND
ND
ND
ND
7.9 0.8
7.9 0.8
1.0
1.0
04/07/05
04/07/05
04/07/05
04/07/05
EPA 3550 EPH
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
8260
ug/kg
ug/kg
uglkg
ug/kg
tog/kg
ug/kg
ug/kg
ug/kg
tog/kg
tog/kg
tog/kg
tog/kg
tog/kg
tog/kg
tog/kg
tog/kg
1132 EBS
1132 KBS
1132 RES
1132 KBS
1132 icas
1132 KBS
1132 icES
1840 DEW
1840 DEW
1840 DEW
1840 DEW
1840 DEW
1537 EWS
1537 EWS
1537 RWS
1537 RWS
1537 RWS
1537 RWS
1537 RWS
1537 RWS
1537 RWS
1537 RWS
1537 RWS
1537 RWS
1537 AWS
1537 RWS
1537 RWS
1537 RWS
321608
580-132
7194 67
84-151
67641
71-43
108861
74975
5274
75-252
7483
8933
104518
13598
98066
56-235
108-907
73003
67 663
74873
Bromoform
Bromomethane
2-Butanone ITK
n-Butylbenzene
sec-Butylbenzene
tert-Btotylbenzene
Carbon tetrachloride
Chiorobensene
Chloroethane
Chloroform
Chioromethane
83
4.2
4.2
4.2
4.2
4.2
8.3
83
4.2
4.2
4.2
4.2
4.2
8.3
4.2
8.3
0.8 04/06/05
0.8 04/06/05
0.8 04/06/05
0.8 04/06/05
0.8 04/06/05
0.8 04/06/05
0.8 04/06/05
0.8 -04/06/05
0.8 04/06/05
0.8 04/06/05
0.8 04/06/05
0.8 04/06/05
0.8 04/06/05
0.8 04/06/05
0.8 04/06/05
0.8 04/06/05
/eAnaIYticar
www.pneIabsCbm
Pace Analytical Sar.ices Inc
9800 KIncey Avenue Suite 100
Hunleisvie NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9291338
Client Project ID West End/6228-05-2694
Lab Sample No 925467425
Client Sample ID 9567-1
Project Sample Number 9291338-003
Matrix Soil
Date Collected 04/04/05 1115
Date Received 04/04/05 1550
-Chiorotoiuene
4-Chiorotoluene
2-Dibromo-3-chloropropane
Dibromoch1orothane
2-Dibromoethane EDB
Dibromomethane
l2-Dichlorobenzene
13 -Dichlorobenzene
4-Dichiorobensene
Dichlorodifluoromethane
i-Dichloroethaxae
12 -Dichioroethane
1-Dichioroethene
cia-i 2-Dichioroethene
trans-i 2-Dichioroethene
2-Dichioropropane
13 -Dichloropropane
2-Dichloropropane
1-Dichioropropene
cia-i -Dichioropropene
trans-i -Dichioropropene
Diisopropyi ether
Ethyibenzene
Baxachioro-i -butadiene
-Hexanone
Isopropylbenzene Cuxaene
p-Isopropyltoluene
Nethylene chloride
4-Methyl-2-pentanone MINK
Nethyi-tert-butyl ether
Z4aphthaiene
n-ropyibenzene
Styrene1112 -Thtrachloroethane22-Petrachloroethane
Petrachioroethene
123 -Trichlorobenzene
12 4-Trichlorobenzene
ND ug/kg
ND ug/kg
ND ug/kg
ND
ND uglkg
ND ug/kg
ND ug/kg
ND uglkg
ND ug/kg
ND ug/kg
ND uglkg
ND ug/kg
ND ug/kg
ND ug/kg
ND ig/kg
ND lag/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ugfkg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND tag/kg
ND tag/kg
ND tag/kg
ND tag/kg
ND tag/kg
ND tag/kg
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RWB
0.8 04/06/05 1537 RiPS
0.8 04/06/05 1537 RiPS
0.8 04/06/05 1537 NiPS
0.8 04/06/05 1537 RiPS
0.8 04/06/05 1537 RiPS
0.8 04/06/05 1537 RiPS
0.8 04/06/05 1537 RiPS
0.8 04/06/05 1537 RiPS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RiPS
0.8 04/06/05 1537 RiPS
0.8 04/06/05 1537 RiPS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RiPS
0.8 04/06/05 1537 RiPS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RiPS
0.8 04/06/05 1537 RWS
0.8 04/06/05 1537 RiPS
0.8 04/06/05 1537 RiPS
0.8 04/06/05 1537 RiPS
0.8 04/06/05 1537 RiPS
95498
10643 -4
96128
124481
106934
74953
9550i
54173-1
106467
757i8
75343
107062
75-354
156-592
156605
78875
142289
594207
563-586
10061015
10061026
108203
100414
87683
591786
8828
99876
75092
i08iO1
1634-044
9i203
103651
10042-5
630206
79345
127184
108883
876i6
12082i
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproducerl except
in lull
without the written consent of Pace Analytical Services Inc
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FLNtLAP E87627
Units Report Limit Ienalvzed By CAB No QpL RagLmt
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
8.3
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
42
4.2
4.2
4.2
42
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
Date oiioaies Page 14 of 40
7eAnaIyticaI
Pace Analytical Serilces Inc
9800 KinceyAvenue Suite 100
lluntersville NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9291338
Client Project ID West End/6228-05-2694
Lab Sample No 925467425
Client Sample ID 9567-1
Project Sample Number 9291338-003
Matrix Soil
Date Collected 04/04/05 1115
Date Received 04/04/05 1550
Asheville Certification ID
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87048
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written cxneeut of Pace Analytical Services nc
Ctiaeiotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
Results Units Report Limit DO Itnalvzed By CAS No Qp RecLust
1l1Trichloroethane ND sag/kg 4.2 0.8 04/06/05 1537 RWS 71-556
ll2Trichloroethane ND sag/kg 4.2 0.8 04/06/05 1537 RWS 79-005
Trich.oroethane ND ug/kg 4.2 08 04/06/05 1537 RWS 79016
Trichlorofluoromethane ND sag/kg 4.2 0.8 04/06/05 1537 RWS 75-694
l23-Trichloropropana ND ug/kg 4.2 0.8 04/06/05 1537 RWS 96-184
124-Tri.methylbenzene ND sag/kg 4.2 0.8 04/06/05 1537 RWS 95636
l35-Trianethylbenzene ND sag/kg 4.2 0.8 04/06/05 1537 RWS 10867-8
Vinyl acetate ND sag/kg 42 0.8 04/06/05 1537 P.WS 10805-4
Vinyl chloride ND ugfkg 8.3 0.8 04/06/05 1537 EWS 75014
Xylene Thtal ND sag/kg 4.2 0.8 04/06/05 1537 RWS 1330-20-7
mp-Xylene ND sag/kg 8.3 0.8 04/06/05 1537 EWS
o-Xylene ND sag/kg 4.2 0.8 04/06/05 1537 RWS 95476
Toluened8 98 1.0 04/06/05 1537 RWS 2037-26-5
4-Bromofluorobesazene 89 1.0 04/06/05 1537 RWS 460-004
Dibrcmiofluorometlsane 98 1.0 04/06/05 1537 RWS 186853-7
l2Dichloroethane-d4 98 1.0 04/06/05 1537 RWS 17060070
Date 04/88/05 Page 15 of 40
Pace AnayticaI Services Inc
9800 Kincey Avenue Suite 100
aceAnalyticar I452
Fax [phone]
Lab Project Number 9291338
Client Project ID West End/6228052694
PIR4ETER FOOTNOTES
Dilution factor shown represents the factor applied to the reported result and reporting limit due to changes
in sample preparation dilution of the extract or moisture content
Inorganic Wet Chemistry and Metals nalyses were performed at our Pace Asheville laboratory and Organic
testing was performed at our Pace Charlotte laboratory unless otherwise footnoted
Method 9071B modified to use ASE
All pH Free Chlorine Total Chlorine and Ferrous Iron analyses conducted outside of EPA reconunended iimuediate
hold time
ND Not detected at or above adjusted reporting limit
NC Not Calculable
Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
NDL Mjusted Method Detection Limit
Surrogate
Surrogate recovery outside of control limits The data was accepted based on valid recovery of remainingsurrogate
The surrogate recovery was above the QC recovery limit The sample was not re-extracted since no target
analytes were detected in the sample
Date 04/08/35 Page 16 of 40
iIleejfiionlD REPORT OF LABORATORY ANALYSIS Chaotte Certification UsNCWastewater40Thisreport shaft not be reprodscet oucept NC Wastewater 12NCDrLnkIngWater37712without the written consent of Pace Analytical Services Inc
NC Dunking Water 37706SCEnvuronmeniaf99030SC99006FLNELAP687648FLNELAP687627
/9 Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
aceAriaIyticaI Huntrswlle NC 280Th
wvpsce1abcom Fac 704875.9091
QUALITY CONTROL DATA
Lab Project Number 9291338
Client Project ID West End/6228-05-2694
QC Batch 124037 Amalysis Method EPH
QC Batch Method EPA 3550 Analysis Description EPH in Soil by Mass Method
Associated Lab Samples 925467425
METHOD BLANK 925479859
Associated Lab Samples 925467425
Blank Reporting
Parameter Units Result Limit Footnotes
Aliphatic C09-C18 mg/kg ND 10
Aliphatic C19-C36 mg/kg ND 10
Aromatic C11-22 mg/kg MD 10
2-Fluorobiphenyl 41
2-Brcmtonaphthalene 88
Nonatriacontane 96
o-Terphenyl 63
LABORATORY CONTROL SZjMPLE 925416711
Spike LCS LCS
Parameter Units Colic Result Footnotes
A.liphatic C09-C18 mg/kg 10.00 7.540 75
Aliphatic C19C36 mg/kg 13.33 13.60 102
Aromatic Cll22 mg/kg 28.33 23.16 82
2-Fluorobiphenyl 91
2-Brcenonaphthalene 93
Nonatriacocutane 105
o-Terphenyl 90
LABORATORY CONTROL SAMPLE 925438509
Spike LCS LCS
Units Cone Result 9GRec Footnotes
Aliphatic C09C18 mg/kg 10.00 10.39 104
Aliphatic C19C36 mg/kg 13.33 17.42 131
Aromatic Cll22 mg/kg 28.33 25.18 89
2-Pluorobiphenyl 126
2-Broxnonaphthalene 95
Date 04/08/05 Page 17 of 40
AsiaxiilleCe If Ic ton Os REPORT OF LABORATORY ANALYSIS Charlotte Certiftation DoNCWastewater40Thisreportshall not be reproduced except in NC Wastewater 12NCDrinkwgWater37712wiflhoiitthe written consent of Pace Analytical Services Inc FJC Drinking Water 37706SCEnvironmental99030SC99006FLNELAPE87648FLNELAP87627
QUALITY CONTROL DATA
Pace Analytical Serarices Inc
9800 KinceyAvenue
Suite 100
Huntersville NC 28078
Phone [phone]
Fac 704.875.9091
Lab Project Number 9291338
Client Project ID West End/6228-052694
LABORATORY CONTROL SANPLE 925438509
Spike LCS LCS
Parameter Units Conc Result Footnotes
Nonatriacontane 53
o-Terphenyl 100
LABORATORY CONTROL SAMPLE 925479867
Spike LCS LCS
Parameter Units Cone Result 9Rec Footnotes
Aliphatic C09C18 mg/kg 10.00 5.782 58
Aliphatic C19C36 mg/kg 13.33 10.85 81
Aroatatic C11-22 mg/kg 28.33 12.05 42
2-Fluorobiphenyl CS
2-Bromonaphthalene CS 43
Nonatriacontane 117
o-Terphenyl 70
MATRIX SPIRE MATRIX SPIRE DUPLICATE 925416729 925416737
Aliphatic C09-C18
Aliphatic C19-C36
Aromatic C11-22
2-Fluorobiphenyl
2-Bromonaphtha1ene
Nonatriacontane
o-Terphenyl
99 94
95 84
87 84
80 73
Footnotes
Asheville Certification lOs
NC Wastswater 40
NC Drinking water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in fell
without the written Consent of Pace Analytical Services InC
Charlotte Certification lOs
NcWastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
www.pacelabs.com
925409690 Spike MS MSD MS MSD
Units Result Come Result Result
mg/kg 11.16 5.808 6.174 52 55
mg/kg 14.88 13.01 13.90 87 93
mg/kg 31.63 22.81 20.76 72 66
Date 04/08/05 Page 10 40
Anaytkai
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QUALITY CONTROL DATA
Pace Analytical Services inc
9800 KinceyAvenue Suite 100
Hunters v/lie NC 28078
Phone [phone]
Fax [phone]
Pager 19 oC 40
Asheville Certification IDa
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This repot shall not be reproduced except in full
without the written consent of Pace Analytical Seivices Inc
Cliaricfle Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
Lab Project Nu3nbex 9291338
Client Project XD West Endf6228-05-2694
QC Batch 124753 Ianalysis Method EPH
QC Batch Method EPA 3550 Analysis Description
EPH in Soil by Mass Method
Zsociated Lab Samples 925467409 925467417
ZITTHOD BLANK 925469561
Associated Lab Samples 925467409 925467417
Blank Reporting
Parameter Units Result Limit Footnotes
Aliphatic C09-C18 mg/kg MD 10
Aliphatic C19-C36 mg/kg MD 10
Aromatic C11-22 mg/kg ND 10
Nonatriacontane CS 95
o-Terphenyl 67
LABORATORY CONTROL SAMPLE 925455107
Spike LCS LCS
Parameter Units Conc Result rRec Footnotes
Aliphatic C09C18 mg/kg 10.00 7.345 73
Aliphatic C19C36 mg/kg 13.33 13.35 100
Aromatic Cl122 mg/kg 28.33 19.01 67
2-Fluorobiphenyl 43
2-Bromonaphthalene 37
Nonatriacontane 120
o-Terphenyl 82
LABORATORY CONTROL SAMPLE 925469579
A.liphatic C09-C18
AJ.iphatic Cl9C36
Aromatic C1l22
2-Pluorobiphenyl CS
2-Bromonaphthalene
Nonatriacontane
o-Terphenyl
Date 04/08/05
Spike LCS LCS
Units Conc Result Footnotes
mg/kg 10.00 5.284 53
mg/kg 13.33 11.47 86
mg/kg 28.33 20.08 71
92
117
134
81
Pace Analytical Serilces Inc
aceAnaytiOar Phone [phone]
Fax [phone]
QUALITY CONTROL DATA
Iab Project Number 9291338
Client Project ID West End/6228052694
81A1RIX SPIKE NATRfl SPIKE DUPLIC.TE 925455115 925455123
925449092 Spike MS MSD MS NSD
Parameter Units Result Conc Result Result %Rac ttRec RPD Footnotes
Aliphatic C09C18 mgtkg 10.00 4.146 4.095 42 41
Aliphatic C19C36 mg/kg 13.33 12.22 10.76 92 81 13
Arnatic C1122 mg/kg 28.33 15.33 14.76 54 52
2-Fluorobiphenyl 57 17
2-Bromonaphthalene 34 31 12
Nonatriacontane 97 76
o-Terphenyl 63 74
SAMPLE DUPLICATE 925455131
92549100 EU
Units Result Result RPD Footnotes
Aliphatic C09-Cl8 mg/kg ND ND MC
Aliphatic C19-C36 mg/kg ND ND NC
Aromatic C11-22 mg/kg ND NJ NC
2-Fluorobiphenyl 96 12 63
2-Broauonaphthalane 96 42 92
Nonatriacontane 9t 107 69
o-Terphenyl 96 82 103
Date 04/08/05 Page 20 of 40
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS Charlotte Certification UsNCWastewater40Thisreportshall nut be repredecesi except in full NC Wastewater 12NCDrinking Water 37712 without the writes consent of Pace Analytical Services Inc NC Drinking Water 37706SCEnvironmental99030SC99006
FL NEL4P E87648 FL NELAP E87627
Pace Analytical Services Inc
aceAnalytical
9800 KiA
Phone [phone]
Fax [phone]
QUALITY CONTROL DATA
Lab Project Nmiber 9291338
Client Project ID West End/622805-2694
QC Batch 125129 Analysis Method VPOI
QC Batch Method VPH Analysis Description
VPH in Soil by Mass Method
Associated Lab Samples 925467409 925467417 925467425
METHOD BWiMK 925474504
Associated Lab Samples 925467409 925467417 925467425
Blank Reporting
Parameter Units Result Limit Footnotes
Aliphatic C05-C08 mg/kg ND 10
Aliphatic C09-C12 mg/kg NI 10
Aromatic C09-C10 mg/kg NI 10
25-Dibromotoluene FIDS 9o 109
25-Dibromotoluene PIDS 116
LABORATORY CONTROL SABPLE 925474512
Spike LCS LCS
Parameter Units Conc Result %Rec Footnotes
Aliphatic C05-C08 mg/kg 20.00 21.90 110
Aliphatic C09-C12 mg/kg 5.000 6.171 123
Aromatic C09-ClO mg/kg 5.000 5.805 116
25-Dibromotoluene FIDS 148
25-Dibromotoluene PIDS 148
MATRIX SPIKE MATRIX SPIKE DUPLICATE 925474520 925474538
925467409 Spike MS MSD MS MED
Parameter Units Result Conc Result Result Footnotes
Aliphatic C05C08 mg/kg 0.1320 16.43 18.42 17.82 111 108
Aliphatic C09C12 mg/kg 0.1719 4.107 5.369 5.025 126 118
Aromatic C09C10 mg/kg 0.1750 4.107 4.741 4.618 111 108
25-Dibromotoluene FIDS 177 145 22
25-Dibromotoluene PXD$171 142 22
Date 04/08/05 Page 21 of 40
Asheville Certification lOs REPORT OF LABORATORY ANALYSIS Charlotte Certification IDsNCWastewater40ThISreport shali not be reproduced except in lull NC Wastewater 12NCDrinking Water
37712 without the written consent of Pace Analytical Services Inc
NC-Drinking Water 37706SCEnvironmental99030SC99006FLWELAPE8748FLNELAPE87627
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
HuntersvilIe NC 28078
Phone [phone]
Fax [phone]
StNPLE DUPLICATE 925474546
La Project Number 9291338
Client Project ID West End/6228-O5-2694
leertifijonlDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced except in tall
without the written consent of Pace Analytical Services Inc
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
925467417 ED
Parameter Units Result Result
Aliphatic C05-C08 mg/kg ND ND
Aliphatic C09-C12 mg/kg ND ND
Aromatic C09-C1O mg/kg ND ND
25-flibroniotolojene PIE9 9ri 134 127
25-Dibromotoluene PIE 132 127
FootnotesRPD
NC
NC
NC
Date 04/08/05
Page 22 40
aeAnticar Pace Analytical Sereices Inc
9800 KinceyAvernie Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
QUALITY CONTROL DATA
IHOD BLZtNK 925465643
Associated Lab Samples
Lab Project Nhixaber 9291338
Client Project ID West End/6228-05-2694
Acenaphthene
Acenaphthylene
Ianthracene
Benzo fluoranthene
Benso fluoranthene
Benzo anthracene
Benzoic acid
Benzoghiperylene
Benzyl alcohol
Benzo pyrene
4-Broinophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-aaethylphenol
4-Chloroanil Inc
bis2-Chloroethoxyiuethane
his 2-Chloroethyl ether
bis2-Chloroisopropyl ether
2-Chloronaphthalene
2-Chloropheno
4-Chlorophenylphenyl ether
chrysene
Dibenz ah anthraoene
Dibenzofssran
2-Dichlorobeijzene
3-Dichlorobenzene
4-Dichlorobenzene
-Dichiorobeuzidine
4-Dichlorophenol
Diethylphthalate
4-Dimethylphenol
Dimethylphthalate
hevile Certification Dx
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87645
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certification Dx
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
QC Batch 124957 analysis Method EPA 8270
QC Batch Method EPA 3545 Analysis Description
Semivolatile Organics
Associated Lab Samples 925467409 925467417 925467425
Parameter
925467409 925467417 925467425
Blank Reporting
Units Result Limit Footnotes
ug/kg ND 330
ug/kg ND 330
ug/kg ND 330
ug/kg ND 330
uglkg ND 330
ug/kg ND 330
ug/kg ND 1600
ug/kg ND 330
ug/kg ND 660
ug/kg ND 330
ugfkg MD 330
tag/kg ND 330
ug/kg ND 660
sag/kg ND 660
tag/kg MD 330
sag/kg ND 330
tag/kg ND 330
ug/kg ND 330
sag/kg ND 330
sag/kg ND 330
ug/kg ND 330
sag/kg ND 330
tag/kg ND 330
sag/kg ND 330
tag/kg ND 330
tag/kg ND 330
tag/kg ND 660
ug/kg ND 330
sag/kg ND 330
sag/kg ND 330
sag/kg ND 330
Date Oe/08f05 Page 23 40
/eAnaIyticaI
ow tpaelabS om
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
QUALITY CONTROL DATA
Lab Project Nwnber 9291.338
Client Project ID West Bnd/622805-2694
ThOD BLANK 925465643
Associated Lab Samples
Di-u-butylphthalate
6-Dinitro-2-methylphenol
24-Dinitropheno
4-Dinitrotolnaene
6-Dinitrotolnaene
Di-noctylphtha1ate
12-Diphansyihydrazine
his 2-Ethylhexylphthalate
Fluoranthene
Elnaorene
Bexachloro-l 3-butadiene
Hexachiorobeuzene
Rexachlorocyclopentadjene
Hexachioroethane
Indenol23-cdpyrena
Isophorone
2-Methylnaphthalene
2-Methyiphenol oCresol
34-Methylphenol
Naphthalene
2-Nitroanji ins
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophexaol
N-Nitroso-di-n-propylajnjne
N-Nitrosodiphenylamjne
Pentachiorophenol
Phenanthrene
Phenol
Pyrene
124-rrjch1orobenzene
24 5-richloropheno1246-Triohlorophaxaol
Nitrobenzene-65
Asheville Certification lOs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E67648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproducef except In fat
without the written consent of Pace Analytical Services Inc
charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FLNEL.AP E87627
925467409 925467417 925467425
Blank Reporting
tinits Result Limit Footnotes
nag/kg ND 330
ug/kg ND 330
nag/kg ND 1600
nag/kg ND 330
nag/kg ND 330
nag/kg ND 330
nag/kg ND 330
nag/kg ND 330
nag/kg ND 330
nag/kg ND 330
nag/kg ND 330
nag/kg ND 330
ug/kg ND 330
ug/kg ND 330
nag/kg ND 330
nag/kg ND 330
nag/kg ND 330
nag/kg ND 330
nag/kg ND 330
ug/kg ND 330
nag/kg ND 1600
ug/kg ND 1600
nag/kg ND 1600
nag/kg ND 330
nag/kg ND 330
nag/kg ND 1600
nag/kg ND 330
nag/kg ND 330
nag/kg ND 1600
ug/kg ND 330
nag/kg ND 330
nag/kg ND 330
nag/kg ND 330
nag/kg ND 330
nag/kg ND 330
59
Oate 04/08/05 Page 24 of 40
Pace Analytical Ser/ices Inc
9800 KinceyAvenue Suite 100
Huntersvi/e NC 28078
Phone [phone]
Fax [phone]
QUALITY CONTROL D.TA
Iab Project Nuniber 9291338
Client Project ID West End/6228-05-2694
METHOD BLARR 925465643
Associated Lab Samples 925467409 925467417 925467425
Blank Reporting
Parameter Units Result Lindt ootnotes
2-Fluorobiphenyl 61
Terphenyl-dl4 96 87
Phenol-dS 96 58
2-Fluorophenol 54
246-Tribrainophenol 96 67
LABORATORY CONTROL SAMPLE LCSD 925465650 925465668
LCSD LCS LCSD
_________ ________________Result footnotes
Acenaphthene
Jhcenaphthylene
Anthracene
Benzo Ic fluoranthene
Benzo fluoranthene
Benzo anthracene
Benzoic acid
Benzoghiperylene
Benzyl alcohol
Benzoapyrene
4-Bronoophenyiphenyl ether
Butylbenzylphthalate
4Chloro-3-methylphenol
4-Chioroaniline
his 2-Chloroethoxyxnetbane
bis 2-Chloroethyl ether
bis2-Chloroisopropyl ether
2-Chloronaphthalene
2-Chiorophenol
-Chlorophenylphenyl ether
Chrysene
Dibenz ah anthracene
Dibennofuran
l2-Dichlorobenzene
3-Dichlorobenzene
Date 04/08/05
Page 25 of 40
Anhsvi0ecWQotoojDs REPORT OF LABORATORY ANALYSIS Charlotte Certification lOsNCWastewater40Thisreportohllnotbereproduced excepts
NC Wastewater 12NCDrinkintWater37712without the written cOnsent of Pace Analytical Services Inc
NC DnnlcIfl Water 37706SCEnvironmental99030SC99006FLNELAP687648FLNELAP687627
wpaLelacn3
Spike LCS
Units Conc Result
ug/kg 1667.00 1130 1286 68 77 13
ug/kg 1667.00 1131 1297 68 78 14
ug/kg 1667.00 1417 1491 85 90
ug/kg 1667.00 1435 1389 86 83
ug/kg 1667.00 1354 1494 81 90 10
ug/kg 1667.00 1408 1446 84 87
ug/kg 1667.00 624.5 648.5 38 39
ug/kg 1667.00 1414 1442 85 86
ug/kg 1667.00 1191 1255 71 75
ug/kg 1667.00 1449 1479 87 89
sag/kg 1667.00 1361 1452 82 87
sag/kg 1667.00 1437 1487 86 89
ug/kg 1667.00 1276 1461 77 88 13
ug/kg 1667.00 1188 1307 71 78 10
sag/kg 1667.00 1125 1203 68 72
sag/kg 1667.00 1083 1130 65 68
ug/kg 1667.00 1140 1172 68 70
ug/kg 1667.00 1082 1214 65 73 11
ug/kg 1667.00 1080 1142 65 68
sag/kg 1667.00 1265 1397 76 84 10
sag/kg 1667.00 1369 1446 82 87
sag/kg 1667.00 1440 1502 86 90
up/kg 1667.00 1196 1367 72 82 13
sag/kg 1667.00 1061 1097 64 66
up/kg 1667.00 1027 1077 62 65
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Huntersville NC 28078
nalyLical Phone [phone]
Fax [phone]
QUALITY CONTROL DATA
Lah Project Nuniber 9291338
Client Project ID West End/6228-05-2694
LABORATORY CONTROL SItNPLE LCSD 925465650 925465668
spike LCS LCSD LCS LCSD
_________________________Units Conc Result Result 5ootnotes
14-Dichlorobenzena ug/lcg 1667.00 1027 1045 62 63
33Dich1orobenzjdjne ug/kg 3333.00 1106 1233 33 37 11
24-Dichlorophenol ug/kg 1667.00 1172 1276 70 77
Diethylphthalate ug/kg 1667.00 1388 1474 83 88
24-Dinoethyiphenol ug/kg 1667.00 1078 1147 65 69
Dhiuethylphthalate ug/kg 1667.00 1319 1435 79 86
Di-n-butylphthalate ug/kg 1667.00 1457 1513 87 91
46Dinitro-2methylphenol ug/kg 1667.00 1412 1435 85 86
24-Dinitrophenol ug/kg 1667.00 1160 1213 70 73
24-Dinitrotoluene ug/kg 1667.00 1438 1519 86 91
26Dinitroto1uene ug/kg 1667.00 1359 1479 82 89
Di-n-octylphthalate ug/kg 1667.00 1455 1485 87 89
12-Diphexxylhydrazine ug/kg 1667.00 1158 1259 70 76
bis2-Zthylhecy1pbtha1ate ug/kg 1667.00 1424 1470 86 88
Fluoranthene ug/kg 1667.00 1438 1472 86 88
Fluorena ug/kg 1667.00 1232 1373 74 82 11
Hex ch1oro13betadje ug/kg 1667.00 1077 1130 65 68
Hexachlorobenzene ugfkg 1667.00 1351 1412 81 85
Hexachiorocyclopentadjene ug/kg 1667.00 920.7 993.5 55 60
Hexachloroethane uglkg 1667.00 1058 1096 64 66
Indeno123cdpyrene ug/kg 1667.00 1428 1484 86 89
Isophorone tag/kg 1667.00 1221 1348 73 81 10
24iethylnaphthalene tag/kg 1667.00 1128 1212 68 73
2-Methylphenol o-Cresol ug/kg 1667.00 1165 1210 70 73
34Methylphenol tag/kg 1667.00 1165 1241 70 74
Naphthalene tag/kg 1667.00 1063 1119 64 67
2Nitroanilina ug/kg 1667.00 1157 1275 69 76 10
3-Nitroanjljne ug/kg 1667.00 1461 1541 88 92
4-Nitroaniline tag/kg 1667.00 2069 2046 124 123
Nitrobetazene ug/kg 1667.00 1120 1176 67 70
2-Nitrophenol tag/kg 1667.00 1124 1182 68 71
4-Nitrophenol tag/kg 1667.00 1550 1596 93 96
N-Nitroso-di-npropylancine tag/kg 1667.00 1174 1248 70 75
N-NitrosOdiphenylaanjne tag/kg 1667.00 1672 1746 100 105
Pantachiorophenol tag/kg 1667.00 1647 1698 99 102
Phenanthrene ug/kg 1667.00 1354 1427 81 86Phenoltag/kg 1667.00 1092 1154 66 69
Date 04/08/05
Page 26 of 40
gljfjcajionlDs REPORT OF LABORATORY ANALYSIS CeicatippjQgNCWastewater40Thoreport shall ant be reproduced except in full NC Wastewater 12NCDrinkingWater37712without the written consent of Pace Analytical SeMces Inn NC Drinking Water 37706SCEnvironmental99030SC99006FLNELAPE87648FLNELAPE87627
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
QUALITY CONTROL DATA
Lab Project Nunber 9291338
Client Project ID West End/6228-05-2694
L7BORATORY CONTROL SANPLE LCSD 925465650 925465668
Spike LCS LCSD LCS LCSD
___________________________Units Conc Result Result ootnotes
Pyrane ug/kg 1667.00 1366 1419 82 85
124-Trichlorobenzene ug/kg 1667.00 1053 1107 63 66
245-Triclilorophenol ug/kg 1667.00 1206 1426 72 86 17
246-Triohlorophenol ug/kg 1667.00 1181 1363 71 82 14
Nitrobenzene-dS 66 68
2-Fluorobiphenyl 66 73
Terphenyl-d14 87 89
Pbenol-d5 64 66
2-Fluorophenol 61 63
246-Tribromophenol 89 93
L7BORATORY dONTROL S1flPLE 925478802
Spike LCS LCS
______________________________Units Conc Result rootnotes
Acenaphthene ug/kg 1667.00 1165 70
Acenaphthylene tog/kg 1667.00 1165 70
1nthracene ug/kg 1667.00 1440 86
Benzokfluoranthene tog/kg 1667.00 1375 82
Benzobfluoranthene ug/kg 1667.00 1432 86
Benzoaanthracene ug/kg 1667.00 1409 84
Benzoic acid ug/kg 1667.00 734.6 44
Benzoghijpexylene ug/kg 1667.00 1372 82
Benzyl alcohol ug/kg 1667.00 1133 68
Benzoapyrene ug/kg 1667.00 1436 86
4-Bromophenylphenyl ether ug/kg 1667.00 1372 82
Butylbenzylphthalate ug/kg 1667.00 14.31 86
4-Chloro-3-methylphenol ug/kg 1667.00 1328 80
4Chloroaniljne tog/kg 1667.00 1187 71
bis2-Chloroethoxymethane tog/kg 1667.00 1049 63
bis2-chloroethyl ether ug/kg 1667.00 950.8 57
bis2-h1oroisopropy1 ether tog/kg 1667.00 1017 61
2-cliloronaphthalene tog/kg 1667.00 1Q89 65
2Chiorophenol tog/kg 1667.00 968.5 58
4-Chlorophenylphenyl ether tog/kg 1667.00 1298 78
Chrysene tog/kg 1667.00 1380 83
Date 04/08/05 Page 27 40
DifcationDo REPORT OF LABORATORY ANALYSIS Ctprloffe Certification IDsNCWastewater40mcreportshallnotbereproducedNCWastewater12NCDrinkingWater37712witlnoat the written consent of Pace Analytical Services NC Drinking Water 37706SCEnvironmental99030SC99006FLNELAPE87648FLNELAPE87627
Pace Analytical Services inn
9800 Kincey Avenue Suite 100
aceAnaIjticai
ipnce1abcom Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9291338
Client Project 113 West End/6228-05-2694
WBORATORY CONTROL SANPLE 925478802
Spike LCS LCS
____________________________Units Conc Result rootnotesDibenzahanthraceneug/kg 1667.00 1404 84
Dibenzofuran ugfkg 1667.00 1242 74
l2-Dichlorobenzene ug/kg 1667.00 933.7 56
13Dichlorobenzene ug/kg 1667.00 909.6 55
14-Dichlorobenzene ug/kg 1667.00 891.5 54
33Dichlorobenzidine ug/kg 3333.00 1154 35
24-Dichiorophenol ug/kg 1667.00 1147 69
Diethylphthalate ug/kg 1667.00 1396 84
24-Dimethyiphenol ug/kg 1667.00 1117 67
Dimethylphthalate uglkg 1667.00 1351 81
Di-nbutylphthalate uglkg 1667.00 1476 89
46Dinitro-2-methylphenol ug/kg 1667.00 1108 66
24-Dinitrophenol nag/kg 1667.00 968.2 58
24-Dinitrotoluene nag/kg 1667.00 1438 86
26-Dinitrotoluene nag/kg 1667.00 1386 83
Di-n-octylphthalate nag/kg 1667.00 1425 86
12-Dipheny.hydrazjne nag/kg 1667.00 1169 70
bis2..Ethylhexy1phthalat ug/kg 1667.00 1413 85
Fluoranthene nag/kg 1667.00 1411 85
Fluorane nag/kg 1667.00 1274 76
Hexachloro-13-butadjene nag/kg 1667.00 983.7 59
Hexachiorobensene nag/kg 1667.00 1371 82
Hexachiorocyclopentadiene nag/kg 1667.00 464.8 28
Hexacliloroethane ug/kg 1667.00 837.8 50Indeno123cdpyrenenag/kg 1667.00 1391 83
Isophorone ug/kg 1667.00 1187 71
2-Mathylnaphthalene ug/kg 1667.00 1091 66
2-Methyiphenol o-Cresol nag/kg 1667.00 1080 65
34-Methylphanol nag/kg 1667.00 1101 66
Naphthalene ugfkg 1667.00 987.0 59
2Nitroaniline ug/kg 1667.00 1177 71
3-Nitroanjijue nag/kg 1667.00 1546 93
4-Nitroaxijljne nag/kg 1667.00 2136 128
Nitrobenzene nag/kg 1667.00 1029 62
2-Nitrophenol nag/kg 1667.00 1035 62
4-Nitrophenol nag/kg 1667.00 1559 94
N-Nitroso-di-n_propy1apjna nag/kg 1667.00 1111 67
Dater 04/08/05
Page 28 40
REPORT OF LABORATORY ANALYSiS Charlotte Certification IDsNCWastewater40Thisreport shall not be reproduced except in lull NC Wastewater 12NCDrinkingWater37712without the written consent of Pace Analytical Services Inc NC Drinking Water 37706SCEnvironmental99030SC99006FLNELAPE8748FL NEL.AF E87627
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
LABORATORY CONTROL SLE 925478802
Lab Project Number 9291338
Client Project Ia West Red16228-05-2694
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
124 -Trichlorobenzene
24 5-Trichiorophenol246-Trichlorophenol
Nitrobenzene-d5 CS
2-Pluorobiphenyl
Terphenyl-d14
henol-65
2-Fluoropheno
246-Tribrosnopheno
MATRIX SPIKE MATRIX SPIRE
Acenaphthene
4-Chloro-3-methylphenol
2-Chiorophenol
14 -Dichiorobeuzene
24-Dinitrotoluene
4-Nitrophenol
N-Nitroso-di-n-propylaapjne
Pentachlorophenol
Phenol
Pyrene
12 4-Trichlorobenzene
Nitrobenzene-d5
2-Fluorobiphenyl
Terpheny1-1.4
Phenol-d5
2-Fluorophenol
246-Trjbromophenol CS
ZIUPLICATZ 925468332 925468340
1.15 8151
ti Rec 9e Rec RPD Footnotes
72 71
82 81
61 60
55 57
87 87
91 92
66 65
93 82 13
62 60
86 87
58 61
59 62
64 66
90 92
58 59
56 57
89 89
caiion lOs
NC Wastewater 40
NC Drinking Water 37712
Sc Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
Ties report shaH not be reproduced except in lull
withoxt the written consent of Pace Analytical Services Inc
Charlotte ceriification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
wwpnceiabscorn
Rec Footnotes
Spike LCS LCS
Units Conc Result
ug/kg 1667.00 1698 102
ug/kg 1667.00 1589 95
ug/kg 1667.00 1375 82
ug/kg 1667.00 988.7 59
ug/kg 1667.00 1370 82
ug/kg 1667.00 969.1 58
ug/kg 1667.00 1317 79
uglkg 1667.00 1227 74
61
67
89
59
54
94
925465973 Spike MS 8151
Units Result Cono Result Result
ug/kg 1793.00 1286 1273
ug/kg 1793.00 1467 1448
ug/kg 1793.00 1087 1069
nag/kg 1793.00 987.1 1020
ug/kg 1793.00 1556 1555
nag/kg 1793.00 1633 1647
nag/kg 1793.00 1176 1167
ug/kg 1793.00 1670 1467
ug/kg 1793.00 1102 1081
nag/kg 1793.00 1539 1556
ug/kg 1793.00 1042 1087
Date 04/08/05
Page 29 of 40
9800 KinceyAvenue Suite 100
Pace Analytical Services Inc
areAnalyticalPYfl Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9291338
Client Project ID West End/6228-05-2694
SAILE DUPLICATE 925468324
925467409 DUP
Parameter Units Result Result RPD Footnotes
Acenaphthene ug/kg ND ND NC
Acenaphthylene ugfkg ND ND NC
Inthracene ug/kg ND ND NC
Benzokfluoranthene ug/kg ND ND NC
Benzobf.uoranthene uglkg ND ND NC
Benzoaanthracene ug/kg ND ND NCBenzoicacidug/kg ND ND NCBenzoghiperyleneug/kg ND ND NC
Benzyl alcohol ug/kg ND ND NCBenzoapyreneugfkgNDNDNC
4-Broxnophenylphenyl ether ug/kg ND ND NC
Butylbenzylphthalate ug/kg ND ND NC
4-Chloro-3-methylphenol ug/kg ND ND NC4-Chloroaniline ug/kg ND ND NC
his 2-Chloroethoxymethame ug/kg ND ND NC
bis2-Chloroethyl ether ug/kg ND ND NC
bis2-Chloroisopropyl ether ug/kg ND ND NC
2-Chloronaphthajene ug/kg ND ND NC
2-Chioropheno ug/kg ND ND NC
4-Chiorophenyipheny ether uglkg ND ND NC
Chrysene ug/kg ND ND NCDibenzahanthraceneug/kg ND ND NCDibenzofuranug/kg ND ND NCl2-Djch.orobenzene ugfkg ND ND NCl3-Dichlorobenzene ug/kg NI ND NC
l4-Dichlorobenzene ug/hg ND ND NC33-Dich1orobezidine ug/kg ND ND NC24-Dichioropheno ug/kg ND ND NCDietbylphthalateug/Icg ND ND NC24-Dinuetbylphenol ug/kg ND ND NC
Dintethylphtha.ate ug/kg ND ND NCDi-n-butylphthalate ugfkg ND ND NC
46-Dinitro-2-methylphenol nag/kg ND ND NC24-Djnjtrophol ug/kg ND ND NC24-Dinjtrotoluene ug/kg ND ND NC216-Djnitrotoluena ug/kg ND ND NCDi-n-octylphthalate ug/kg ND ND NC
nate 04/08/05 a58 30 40
iiyjile Certification IDs REPORT OF LABORATORY ANALYSIS rJciie Certification lOsNCWastewater40Thisreport shall not be reproducerj except in jet NC Wastewater 12NCDrinkingWater37712without the written consent of Pace Analytical Services Inc
PlC Drinking Water 37706SCEnvironmental99030SC99006FLNELAPE87648FLNELAPE67627
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
QUALITY CONTROL DATA
Lab Project NumbØrt 9291338
Client Project ID West En6/6228-05-2694
S7LE DUPLICATEs 925468324
925467409 flU
_____________________________Units Result Result RPD Footnotes
12-Diphenylhydrazine ug/kg ND ND NC
bis2-Ethylhexylphthalate ug/kg ND ND NC
Fluoranthane ug/kg ND ND NC
Fluorene ug/kg ND ND NC
Hexachloro-13-butadjene up/kg ND ND NC
Hexachlorobenzene up/kg ND ND NC
Hezachiorocyclopentadiene up/kg ND ND NC
Hexachioroethane ug/kg ND ND NC
Indeno123-cdpyrene up/kg ND ND NC
Isophorone ug/kg ND ND NC
2-Nethylnaphthalene ug/kg ND ND NC
2-Methyiphenol o-Cresol ug/kg ND ND NC
34-Methylphenol ug/kg ND ND NC
Naphthalene ug/kg ND ND NC
2-Nitroaniljne up/kg ND ND NC
3-Nitroaniline ug/kg ND ND NC
4-Nitroaniline ug/kg ND ND NC
Nitrobeuzene ugfkg ND ND NC
2-Nitrophenol up/kg ND ND NC
4-Nitrophenol ug/kg ND ND NC
N-Nitroso-di-n-propylasnjne up/kg ND ND NC
K-Nitrosodiphenylanijne up/kg ND ND NC
Pentachiorophenol ug/kg ND ND NC
Phananthrene ug/kg ND ND NC
Phenol ug/kg ND ND NC
Pyrene up/kg ND ND NC
124-Trjchlorobenzene up/kg ND ND NC
245-Trioblorophanol up/kg ND ND NC
246-Trioh.orophenol up/kg ND ND NC
Witrobenzene-dS 51 43
2Fluorobiphenyl 58 48
Terphanyl-dl4 80 65
Phenol-d5 44 40
2Fluorophenol 33 33
246-rribromophenol 57 52
Oats 04/08105
Page 31 of 40
AlleCefljigjonjDs REPORT OF LABORATORY ANALYSIS Certifation OsNCWastowater40TInereport shall not be reproduced excepts
NC Wastewater 12NCDrinkingWater37712without the written consent of Pace Analytical Services nc NC Drinking Water 37708SCEnvironmental 99fl30 SC 99006FLNELAPE87648FLNELAPE87627
pnceiabscorn
Analytical
wif.v.paceIabs.com
Pace Analytical Serlicas Inc
9800 KinccyAvenue Suite 100
Huntersville NC 28078
Phore 704.875.9092
Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9291338
Client Project ID West End/6228-052694
QC Batch 125128 analysis Method EPA 8260
QC Batch Method EPA 8260 Asalysis Description GC/MS VOCs 5035/8260 low level
Associated Lab Samples 925467409 925467417 925467425
I2Th0D BLZtNK 92547442
Associated Lab Samples 925467409 925467417 925467425
Date 04108/05 Page 32 of 40
ationlDs
NC Wastewater 40
NC Drinking Water 37712
SC Environcetintal 99030
FLNELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in tnt
without the written consent of Pace Analytical Services Inc
Ctl8tlofle Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP 687627
Footnotes
Blank Reporting
Units Result Limit
Acetone ug/kg ND 100
Benzene ug/kg MD 5.0
Broinobenzene ug/kg ND 5.0
Bromochlorauuethaxie ug/kg ND 5.0
Bromodichloromethane ug/kg ND 5.0
Brcraoform ug/kg ND 5.0
Bromoanethane ug/kg ND 10
2-Butanone 81EK uglkg ND 100
n-Butylbenzene ug/kg ND 5.0
sec-Butylbenzene ug/kg ND 5.0
tert-Butylbenzene ugfkg ND 5.0
Carbon tetrachloride ugfkg ND 5.0
Chlorobenzene ug/kg ND 5.0
Chioroethane ug/kg ND 10
Chloroform ug/kg MD 5.0
Chloromethane ugfkg MD 10
2-Chlorotojueue ug/kg ND 5.0
4-Chlorotoluene ug/kg ND 5.0
l2-Dibromo-3-chloropropane ug/kg ND 5.0
Dibroatochloroijnethana ug/kg ND 5.0
l2-Dibrcenoethane EDE ug/kg ND 5.0
Dibroxnometharae ug/kg ND 5.0
12-Dichiorobensene tog/kg MD 5.0
13-Dichioroberizene tog/kg ND 5.0
14-Dichlorobenzane tog/kg ND 5.0
Dichlorodjfluoromethane tog/kg ND 10
l1-Dichloroethane ugfkg ND 5.0
l2-Dichloroethane tog/kg ND 5.0
3.l-Diohloroethene tog/kg 5.0
cis-l2-Djchloroethene tog/kg ND 5.0
trans-12-Dichloroethane ug/kg ND 5.0
aeAna1Yticai
www pace s.ccm
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9291338
Client Project ID West End/6228-05-2694
ZIB0D BLK 925474462
Associated Lab San1es 925467409 925467417 925467425
2-Dichloropropane
13 -Dicliloropropane
2-Dichioropropane
1-Dichloropropene
cia-i 3-Dichioropropene
trans-i 3-Dichloropropene
Dilsopropyl ether
Ethyibenzene
Rexachloro-1 3-butadiene
-Hexanone
Isopropylbenzene Cuncene
p-Isopropy.toiuene
Nethylene chloride
4-Methyi-2-pentanone NIB3
Nethyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrena1112Tetrach.oroethane
112 2-Tetrachioroethane
Tetrachloroethene
o1uene
123 -Trichlorobenzene
i24Trjchlorobenzane111-Trichioroethane112-Trichioroethane
Trichioroetherue
Triahiorofluoromethane
123 -Trichiorepropane124-Trimethylbeuzene135-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xyiene Total
ntp-Xyiene
o-Xylene
IeCettlfjfjonlD
NC Wastewater 40
NC Drinking Water 37712
SC Environmeettai 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report strati not be reproduced except
in lull
without the written consent of Pace Analytical Services inc
Charlotte Certification IDS
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NAP E67627
Footnotes
Blank Reporting
Tjnjts esu1t Limit
ug/kg ND 5.0
ug/kg ND 5.0
ug/kg ND 5.0
ug/kg ND 5.0
ugfkg ND 5.0
ugfkg ND 5.0
ug/kg ND 5.0
ug/kg ND 5.0
ug/kg ND 5.0
ug/kg ND 50
ug/kg ND 5.0
uglkg ND 5.0
ugfkg ND 5.0
ug/kg ND 50
ug/kg ND 5.0
uglkg ND 5.0
ug/kg ND 5.0
ug/kg ND 5.0
ug/kg ND 5.0
ug/kg ND 5.0
ug/kg ND 5.0
ug/kg ND 5.0
ugfkg ND 5.0
ugfkg ND 5.0
nag/kg ND 5.0
nag/kg ND 5.0
nag/kg ND 5.0
ug/kg ND 5.0
nag/kg ND 5.0
nag/kg ND 5.0
nag/kg ND 5.0
nag/kg ND 50
nag/kg ND 10
nag/kg Nt 5.0
nag/kg ND 10
ug/kg ND 5.0
Date 04/08/05 Peas 33 cC 40
Analytical
pacefnbscm
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9291338
Client Project ID West End/6228-05-2694
ZIETHOD BLitI 925474462
Associated Lab Samples 925467409 925467417 925467425
Blank ReportingParameterUnitsResultLimit Footnotes
Toluene-d8 100
4-Bromofluorobenzene 100
Dibromofluorosnethane 96
12-Dichloroethane-d4 99
IJBORAT0RY CONTROL SZtMPLE 925474470
Asheville Certification lOs
NC WastewOter 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
Thts report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certificptioppg
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
Footnotes
Spike LCS LCS
Units Conc Result
Acetone ug/kg 100.00 123.0 123
Berizene ug/kg 50.00 46.56 93
Broinobenzene ug/kg 50.00 50.25 100
Bromoabloramethana ug/kg 50.00 46.90 94
Brontodichloromethane ug/kg 50.00 47.88 96
Brotnofomm ug/kg 50.00 48.28 97
Brontomethane tog/kg 50.00 53.75 108
2-Butanona MEK tog/kg 100.00 103.0 103
n-Butylbeuzene tog/kg 50.00 43.95 88
sec-Butylbenzene üg/kg 50.00 49.33 99
tert-Butylbennene ug/kg 50.00 49.17 98
Carbon tetrachlorjde tog/kg 50.00 48.73 98
Chlorobenzane ugfkg 50.00 47.76 96
Chloroethane tog/kg 50.00 45.76 92
Chlorofoxm tog/kg 50.00 47.54 95
Chioromathana tog/kg 50.00 42.21 84
2-Chiorotoluene tog/kg 50.00 48.37 97
4-Chiorotoluene ug/kg 50.00 48.92 98
l2-Dibranlo-3-ohloropropana tog/kg 50.00 48.49 97
Dibromoobloromethane tog/kg 50.00 47.45 95
12flibroneoethena EUB ugfkg 50.00 47.56 95
Dibromomethane tog/kg 50.00 48.45 97
l2-Dichlorobenzene tog/kg 50.00 48.50 97
l3-flichlorobenzene tog/kg 50.00 48.62 97
l4-Dichlorobenzene tog/kg 50.00 46.80 94
Dich1orodjfluoropthane ug/kg 50.00 40.39 81
Data 04/08/05
Page 34 of 40
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
ace Anaiyticai
Coin Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 929i.338
Client Project ID West End/6228-05-2694
LABORATORY CONTROL SAMPLE 925474470
Spike LCS LCS
___________________________Units Conc Result Pootnotes
ll-flichloroethane ug/kg 50.00 46.31 93
12-Dichioroethane up/kg 50.00 46.89 94
11-Dichioroethene up/kg 50.00 48.22 96
cis-l2-Dichloroethene up/kg 50.00 48.27 96
trans-12-Dichloroethene up/kg 50.00 46.91 94
12-Dichioropropane ug/kg 50.00 48.22 96
13-Dichioropropane up/kg 50.00 48.08 96
22-Dichioropropane up/kg 50.00 53.88 108
11-Dichloropropene ug/kg 50.00 47.19 94
cisl3-Dichloropropene ug/kg 50.00 47.91 96
trans-13-Dichloropropene up/kg 50.00 49.36 99
Diisopropy-1 ether up/kg 50.00 48.03 96
Ethylbenzene up/kg 50.00 47.15 94
8iexachloro-13-butadiene up/kg 50.00 51.34 103
2-liexanone up/kg 100.00 92.65 93
Isopropylbenzene Cumene ug/kg 50.00 50.84 102
p-Isopropyltoluene up/kg 50.00 44.37 89
Methylene chloride ug/kg 50.00 47.71 95
4-Nethyl-2-pantanone MIBK ug/kg 100.00 94.86 95
Methyl-tert-butyl ether ug/kg 50.00 45.34 91
Naphthalene ug/kg 50.00 43.33 87
n-Propylbenzene up/kg 50.00 49.17 98
Styrene up/kg 50.00 48.03 96
lll2-Tetrachloroetbana up/kg 50.00 48.57 97l122-Tetrach1oroete ug/kg 50.00 46.75 94
Tetrachioroethene ug/kg 50.00 46.45 93
Toluene up/kg 50.00 45.97 92
l23-Triahlorobenzene up/kg 50.00 47.67 95
124-Trichlorobanzene up/kg 50.00 46.67 93
l11-Trichloroethana up/kg 50.00 47.75 96
112-Trichloroethane ug/kg 50.00 47.02 94
Trichloroethene ug/kg 50.00 46.91 94
Trichlorofluoromethane ug/kg 50.00 44.79 90
l23-Tric1zloropropane up/kg 50.00 47.30 95
124-Trimethylbenzene ug/kg 50.00 43.77 88
l35-Trinethylbenzene up/kg 50.00 44.12 88
Vinyl acetate up/kg 100.00 99.14 99
Date 04/08/05
Page 35 of 40
ohniiieCetificattonlD REPORT OF LABORATORY ANALYSIS Charlotte Certification OsNCWastewater40
This report shaH fiat be reproduced NC Wastewater 12NCDrinking Water 37712 without the written contest of pace Analytical Services
NC Drinking Water 37706SCEnvironnigntal99030SC99006FLNELAPE87648FLNELAPE87627
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
LAEORATORY CONTROL SANPLE 925474470
Parameter
Vinyl chloride
Zylene Total
mp-Xylene
o-Zylene
Toluene-d8
4-Broxnofluorobenzene
Dibraofluoromethane
l2-Dichloroethane-d4
ERTRIX SPIKE 925482341
Benzene
Chlorobenzene
11 -Dichioroethene
Toluene
Trichloroethene
To1une-d8
4-Broniofluorobenzgne
Dibrceatofluoromethane
12-Dichloroethane-d4
Lab Project Number 9291338
Client Project ID West End/6228-05-2694
onDs
NC Wastewater 40
NC Dnnklng Water 37712
SC EnvironeTental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shut not be reproduced except in full
without the written consent of Pace Analytical Services Inc
CharLotte CeriificytIs
NOWastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP
www.pnce1abcom
Spike LCS
Units Conc Result
ugIk 50.00 40.09
ug/kg 150.00 140.9
uglkg 100.00 94.14
ug/kg 50.00 46.75
LCS9_Footnotes
80
94
94
94
100
97
99
97
925467417 Spike MS 355
Units Result Conc Result %Rec Footnotes
ug/kg 45.10 40.58 90
ug/kg 45.10 40.27 89
ug/kg 45.10 43.43 96
uglkg 45.10 40.06 89
ug/kg 45.10 39.65 88
SALE DUPLICATE 925482333
100
97
100
96
925467334 DUP
Parameter Units Result Result FootnotesAcetoneug/kg ND NCBenzeneug/kg ND ND NCEromobenzeneug/kg ND ND NCBromochioromethaneug/kg ND ND NCBromodichloromethaneug/kg ND ND NCBromoformnag/kg ND ND NCBromomethanenag/kg ND ND NC2-Butanone I4EK ug/kg ND ND NC
Oate 04/08/05 Page 36 40
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax[phone]
QUALITY CONTROL DATA
Lab Project Nwnber 9291338
Client Project ID West nd/622805-2694
SiLE DUPLICA1E 925482333
925467334 DUP
____________________________Units Result Result RPD Footnotes
n-Butylbenzene ug/kg ND ND NC
sec-Butylbenzene ug/kg ND ND NC
tert-Butylbenzene ug/kg ND ND NC
Carbon tetrachioride ug/kg ND ND NC
Chlorobenzene ug/kg ND ND NC
Chloroethane ug/kg ND ND NC
Chloroform ug/kg ND ND NC
Chioramathane ugfkg ND ND NC
2-Chiorotoluene sag/kg ND ND NC
4-Chiorotoluane sag/kg ND ND NC
l2-Dibromo-3-chloropropane ug/kg ND ND NC
Dibromochloromethane ug/kg ND ND NC
12-Dibronioethane DB ug/kg ND ND NC
Dibroanomethane ug/kg ND ND NC
12-Dichlorebenzene sag/kg ND ND NC
13-Dichiorobeuzene ug/Itg ND ND NC
l4-Dichlorobenzene sag/kg ND ND NC
Dichiorodifluoromethane sag/kg ND 24.00
l-Dichloroethaxae sag/kg ND ND NC
l2-Dichloraatbene ug/kg ND ND NC
11-Dichioroethene sag/kg ND ND NC
cis-j.2-Djchloroethene sag/kg ND ND NC
trans-12-Dichloroathane sag/kg ND ND NC
l2-Dichloropropaxie uglkg ND ND NC
13-Dichloropropane ugfkg ND ND NC
22-Dichloropropane sag/kg ND ND NC
l1-Dichloropropene sag/kg ND ND NC
cis-13-Dichloropropene sag/kg ND ND NC
trans-13-Dichloropropene sag/kg ND ND NC
Diisopropyl ether sag/kg ND ND NC
Rthylbenzena sag/kg ND ND NC
Hexachloro-l3-butadjene sag/kg ND ND NC2-Bexanone sag/kg ND ND NC
Isopropylbenzane Cumene sag/kg ND ND NC
p-Isopropyltoluexae sag/kg ND ND NC
Nethylene chloride sag/kg ND ND NC
d-X4ethyl-2-pentanone MTBK sag/kg ND ND NC
Date 04/08/as Page 37 of 40
CetinIDs REPORT OF LABORATORY ANALYSIS ClarIotte CertificationINCWastewater40Threreport shall not be reproduced except in lull NC Wastewater 12NCDrinking Water 37712 without the written consent of Pace Analytical Services Inc NC Drinking Water 37706SCEnvironnnental99030SC99006FLNELAPE87648FL NEL.AP E87627
wvwpaie1abscm
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
aceArialytical
ipace1abswn Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9291338
Client Project XD West End/6228-052694
SLE DUPLICATE 925482333
925467334 DUP
_____________________________Units Result Result RPD Footnotes
I4ethyl-tert-butyl ether ug/kg ND ND NC
Naphthalene ugfkg ND ND NC
n-ropylbenzene uglkg ND ND NC
Styrene ug/kg ND ND NC
11l2-Tetrachloroethane ug/kg ND ND NC
l122-Tetrahlovoet1iane ug/kg ND ND NC
retrachloroethene ugfkg ND ND NC
Toluene ugfkg ND ND NC
123-Trichlorobenzene uglkg ND ND NC
124-Trichlorobenzenie nag/kg ND ND NC
111-Trichloroethane ug/kg ND ND NC
112-Trichloroethane nag/kg ND ND NC
Trichloroethene nag/kg ND ND NC
Trichloroflnaoxnethane ug/kg ND ND NC
123-Trichioropropane ug/kg ND ND NC
124-Triznethylbenzene ug/kg ND ND NC
135-Trimethylbenzene nag/kg ND ND NC
Vinyl acetate nag/kg ND ND NC
Vinyl chloride nag/kg ND ltD NC
Xylene Total nag/kg ND ND NC
tnp-Xylene nag/kg ND ND NC
o-Xylene ugfkg ND ND NC
Toluene-d8 101 100
4-Bromofluoroberazene 101 97
Dibromofluorometbane 92 94
12-Dichloroethane-d4 90 97
Oate 04/08/05 Page 38 of 40
Asheville Certification lOs REPORT OF LABORATORY ANALYSIS ariot1e Certiticatig IDsNCWastewater40Thisreportshall not 1w reproduced except NC Wastewater 12NCDrinkingWater37712without the written consent of Pace Analytical Services mc NC Drinking Water 37706SCEnvironmental99030SC99006FLNELAPE$7648 FL NELAP E87627
QUALITY CONTROL DkTA
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunlersville NC 28078
Pt7one 704.875.9092
Fax [phone]
Lab Project Number 9291338
Client Project ID West End/6228-05-2694
QC Batch 125108 Analysis Method Moisture
QC Batch Method Analysis Description Percent Moisture
Associated Lab Saxnp.es 925467409 925467417 925467425
SPLE DUPLICATE 925473597
Percent Moisture
Onto .04/08/05
925469090 DUP
Units Result Result RPD Footnotes
12.90 12.90
Page 39 oC 40
icatjonlD
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall ent be reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
wp8Cetabcorn
Pace Analytical Sir/ices Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9291338
Client Project ID West Exid/6228052694
QUALITY CONTROL DATA PAR7it1IETER FOOTNOTES
Consistent with EPA guidelines unrounded concentrations are displayed and have been used to calculate Rec and RPD values
LCSD Laboratory Control Sample Duplicate
Z85D 74atrix Spike Duplicate
DUP Sample Duplicate
ND Not detected at or above adjusted reporting limit
NC Not Calculable
Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
NDL .djusted Method Detection Limit
RPD Relative Percent Difference
Surrogate
Surrogate recovery outside of control limits The data was accepted based on valid recovery of remainingsurrogate
The surrogate and/or spike recovery was outside acceptance limits
Acid surrogate recovery outside of control limits The data was accepted based on valid recovery of the two
remaining acid surrogates
ttate 04108105
Page 40 cC 40
REPORT OF LABORATORY ANALYSiS riQfte Certification DoNCWastewater40
This report shall not be reproduced except NC Wastewater 12NCDrinkIng Water 37712 without the written consent of Pace Airalyitcal Services Inc
NC Drinking Water 37706SCEnvironmentalg9030SC99006FLNELAPE87648FLNELAPE87627
PaceAnalytical
WWW.paceiabs.cotn
Required Client Information Section
Company
________Adthess
P.O 3523
Project Name cp
GROUNDWATER GW
Project
Nun1berc
DRINKING WATER OW
URFACE WATER SWWASTE WATER WWPRODUCTSoOnecharacterperbox011
0-9.--ZR ARSampleIDsMUSTBE UNIQUE OTHER OT
Page of
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Requested Due Dale TAT Project Manager_____Jil lic-Ai
turn around time less than 14 days SutjPct
to
toratory and contractual obligations and may result fl
Rush Turnaround Surcharge
Turn Around Time TAT in calendar days
-r --
PRINTarT15djSAMpLER fr
SlGNATUREQISAMPLEft
He utreci Client tnformajion Section
Copy To
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if A5 uu..i1e11TheChain-of-Custody is LEGAL DOCUMENT All relevant fields must be completed accurately
______________________
To Be Completed by Pace Analytical and Client Sectior
Quote Reference
Project if
Projile if
COLLECTED
sAr-..-.
q1j L/
1-0
Ill
-J-J
1ME-
END
DATE TIME
Requested
Analysis
Preservatives
0m0CJZO CaIi52Oizi___LL.7i/p J/L/o3
----
Remarks/L
ri-icw L1-
IIIIIIII11I
NC gNLwAi
__
iuWcEH1
SAMPLE NOTESSAMPLECONDITION
Temp in ec
Received on Ice i/N
Sealed Cooler YIN
Samples Intact YIN
Additional Comments
V1b J9_j ic tL
ci DQu-ctIrt ECD iMcrrc th-erp r....rrrm
This line to be completed by Responsible Party or their representative
IncidentNumber //rd 55O -___________Please Provide the Following Information to the best of your knowledge
Addresofprcvingsvey7Zô CJ /1kE
City County
What is the source of your drinking wate Public Water Water Supply Well Stream Intake Other please
explain below
Is there water supply well on this property Yes6 If No disregard remaining questions and return survey
Name and address of owners of property with water supply well
How many water supply wells are on your propertyWhatisthewellsusedforcheckallthatapply Drinking ______Irrigation Swimming Pool ______Water Livestock ______Other specify You do not use the Well
How many residences are connected to the well list addresses below
How deep is the wells Date well was installed
What is the casing depth of the wells
What is the screen interval of the wells
Additional water supply well information
This part to be completed by Responsible Party or their representative
Please returnconipleted survey to by using one of the followingmethods
l.Faxto FoSer
Mail to rVlZO YQrkvov 7c9 r/o7/LJC Z2-o
Telephone 70 7-
E-mail to /C -R5t-er iq Co
If you have any questions please contact the consultant indicated above
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This line to be completed by Responsible Party or their representative
Incident Number 550
Please Provide the Following Information to the best of your k9owledgeJ1F7tW/ii
Address of roperty receiving survey JJM2 45
Count pc.K
What is the source of your drinking water ublic Water ater Supply Well Stream Intake Other pleaseexplainbelow
Is there water supply well on this property Yes If No disregard remaining questions and return survey
Name and address of owners of property with water supply well
How many water supply wells are on your propertyWhatisthewellsusedforcheckallthatapply Drinking Irrigation Swimming Pool ______Water Livestock Other specify You do not use the WellHowmanyresidencesareconnectedtothewelllistaddressesbelow
Now deep is the wells Date well was installed
What is the casing depth of the wells
What is the screen interval of the wells
Additional water supply well information
This part to be completed by Responsible Party or their representativePleasereturncompletedsurveytofe by using one of the followingmethods
1.Faxto 7o Fser
2.Mailto 21
3.Telephone
4.E-mailto TC-POe1CTE.Con7
If you have any questions please contact the consultant indicated above
F-22
This line to be completed by Responsible Party or their representativeIncidentNumber5fo7ffoirdS5o
ame and telep
Please Provide the Following Information to the best of your knowledge
hone number of person completing the surveyAddressofproperty receiving survey f3/Ic 2cj gMo rcc
City Ck-fJC-ounty
Is there water supply well on this property Ye If No disregard remaining questions and return survey
Name and address of owners of property with water supply well
How many Water SUpplywelsare on your propertyWhatisthewellusedforcheckallthatapplyDrinking irrigation Swimming Pool ______Water Livestock ______Other snecify ________You do not use the WellHowmanyresidences are connected to the well iit addresses below
How deep is the wells Date well wos installedWhatisthecasingdepthofthewellsWhatisthe screen interval of the wells
Additional water supply well information
This part to be completedby Responsible Party or their representativePleasereturncompletedsurveyto5f-by using one of the followingmethods
axto Rt Fosr
2.Mailto
7d1
3.Telcphone 7/3S 7-8oO FAX 70 3574E-mail to /cf-iiyfty Co
If you have any questions please contact the consultant indicated above
MAR 29 25 1O2 7ll4 374 9129 PAGE
Mr 29 05 1017a DougLas Bia1 704-374-S1S
4-7TA i7-7
What is the source of your drinking water Public Water Water Supply Well Stream Intake Other pleaseemlalnbelowLhtjA
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Sent By CPI
7043671215 Mar-28-05 251PM Page 1/1
Name and address of owners of property with water supply well
Please Provide the Following InformatIon to the best of your knowledge
Name and telephone number or person completing
the survey j/ta.c kit.o tl
Address of property recevirg survey 2e
City Cj-L.--Conty
is there water supply well on this property est7 If No di
Now many water suoolv wells are on -your property
What is the source of your drinking water Public Water Water Supply Well Stream Intake Other please
explain beow j4 t1t PtLl lAi.
.1
regard rernainin questions and return survey
What is the wells used for check all that apply Drinking
Water Liveatock Other speelfv Von tin notS-How many residences are connected to the well list addresses below
How deep is the wells
What is the casing deDth of the wells
What is-the screen interval of the wells
Additional water sulv well information
Irrigation .Swlmming Fool
etiie Well
Date well was installed
This part to be completed by Responsible Farty
Or their representati
Please return completed survey to t-e by using one of the following
methods
LFaxto
2.Mailto
a8-C1 ot7c9d r/cIitk gzor
3.Telephone 7/3S go
E-mail to fc -cS-t.y-9c Er-Corv7
If you have any questions please contact the consultant indicated above
This line to be completed by Responsible Party or their representativeIncidentNumber95a7/2/01 i55o
r-
F-22
MAR 28 2005 1404 7043671215 FAOE.81
This line to be completed by Responsible
Party or their representative
Incident Number /01 550
Please Provide the Following Information to the best of your knowledge
Name and telephone number of person completing the survey o.M 737 _ff
Address of property receiving survey 7/4 tü /L1cvii cd 7TE /EJç
City C-hcnq/l-e /V-County /v1 ckjp Ii
c-I
What is the source of your drinking ater Supply Well Stream Intake Other please
exnlain below
Name and address of owners of property with water supply well
How many water sunolv wells are on your property i-------
What is the wells used for check all that apply Drinking Irrigation Swimming PoolWaterLivestockOtherspedfyYoudonotusetheWell
How many residences are connected to the well list addresses below
How deep is the wells Date well was installed
What is the casing depth of the wells
What is the screen interval of the wells
Additional water supply well information
This part to be completed by Responsible Party or their representative
Please returncompleted survey
to f1e.t by using one of the followingmethods
1.Faxto 7oL3 F$er
2.Mailto ZOrvt4orç-7cO /oçILk Z2O
Telephone [phone]
E-mail to fc -o5--ey-ij T-c TE.Con1
If you have .any questions please contact the consultant indicated above
e4i 7L
Is there water supply well on this property Yesd7 If No disregard remaining questions and return survey
F-22
This line to be completed by Responsible Party or their representativeIncidentNumber070155
Please Provide the Following Information to the best of your knowledge
Name and telephone number of person completin the strvey see attached for other prop rties
Address of property receiving survey John ayne Adams 600 Norris Street
City Charlotte County Necklenburg
What is the source of your drinking watericWat/Water Supply Well Stream Intake Other pleaseexplainbelow
Is there water supply well on this property Yes If No disregard remaining questions and return survey
Name and address of owners of property with water supply well
How many water supply wells are on your propertyWhatisthewellsusedforcheckallthatapply Drinking Irrigation Swimming Pool ______Water Livestock Other specify You do not use the WellHowmanyresidencesareconnectedtothewelllistaddressesbelow
I-low deep is the wells Date well was installed
What is the casing depth of the wells
What is the screen interval of the wells
Additional water supply well information
This part to be completed by Responsible Party or their representative
Please return completed survey to Dfe by using one of the followingmethods
l.Faxto 7c F6r
Mail to 3l t1ZO 1orktiioyt-7c9d C4cjt-/o/fr/Lk ZR2O
Telephone 7CW357-8oo
E-mail to tc 1c05 ii rlc
If you have any questions please contact the consultant indicated above
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John Adams
Page of
03/28/05
The following properties are located within this survey and are listed as follows
801 Hill Street
809 Hill Street
510 Morehead Street
600 Morris Street
601 Morris Street
701 Morris Street
704 Morris Street
This line to be completed by Responsible Party or their representativeIncidentNumberffc
Please Provide the Following Information to the best of your knowledge
Name and telephone number of person completing
the survey
Address of property receiving survey L1 cA/AJV
City County
What is the source of your drinking water Public Water Water Supply Well/Stream Intake Other pleaseexplainbelowiiLhfrr
Is there water supply well on this property Yes If No disregard remaining questions and return survey
Name and address of owners of property with water supply well
How many water supply wells are on your property
What is the wells used for check all that apply Drinking Irrigation Swimming Pool ______Water Livestock ______Other specify You do not use the WellHowmanyresidences are connected to the well list addresses below
I-low deep is the wells Dale well was installed
What is the casing depth
of the wells
What is the screen interval of the wells
Additional water supply well information
This part to be completed by Responsible Party or their representative
Please return completed survey to teC by using one of the followingmethods
1.Faxto 7ôL FeSer
2Mai1to zO Yorkviar C/r/oi4cAk z2-c
Telephone 70 /7 7-
4.E-mailto OecT Cori
If you have any questions please contact the consultant indicated above
-22
Please Provide the Following Information to the best of your knowledge
Name and telephone number of person completing the survey 4-Address property receiving survey iO
City CiIôJ County iL1L1
What is the source of your drinking wat rT Ic Wa ri Water Supply Well Stream Intake Other pleaseexplainbelowlit
Is there water supply well on this property YesNo If No disregard remaining questions and return survey
Name and address of Owners of property with water supply vell
How many water suppJly wells are on your oronertv
What is the wells used for check all that apply Drinking Irrigation Swimming Pool ______Water Livestock Other specify You do not use the WellHowmanyresidencesareconnectedtothewelllistaddressesbelow
How deep is the wells Date well was installed
What is the casing depth
of the wells
What is the screen interval of the wells
Additional water supply well information
This part to be completed by Responsible Party or their representative
Please return completed survey to by using one of the followingmethods
l.Faxto 7o Fôer
2.Mailto zO YQr1zv140ri CJ/0Ak zg2-o
Telephone 7C//3S7-1oo
E-mail to cos1-ey-a 4-cTEc Con1
If you haveany questions please contact the consultant indicated above
This line to be completed by Responsible Party or their representativeIncidentNumber757//j nd S5o
F-22
GrubbE11is
Wibon/KibIertupcnySolutionsWorldwide
April 26 2005
Mr RobertC Foster Ill
Principal Geologist
MACTEC Engineering Consultin Inc
2801 Yorkmont Road 100
Charlotte North Carolina 28208
RE 923 West Hill Street
Dear Mr Foster
Your letter of March 232005 addressed to LPT Enterprises has been referred to this
writer for reply
We have no knowledge of any wells past or present We purchased the property in 1976
At that time the building was connected to city water
Sincerely
Gorham Boynton
Industrial Division
GBIdd
cc James Leventis
VdsSthIer
P.O Box 11312 Iii Laurel Sheet 29201 Columbia SC 29211 803.779.8600 803.252.4323 ix www.wilaonkibiar.comLrNLMfICMSW4IIkWnMI
This line to be completed by Responsible
Party or Iheir representativelncidentNumber///
Please Provide the Following Information to the best of your knowledge L__
Name and telephone number of person completing
the survey
Address of property receiving survey Ui
City County
Name and address of owners of property with water SUpply well _____________
How many water supply wells are on your property
What is the wells used for check all that apply Drinking Irrigation Swimming Pool ______Water Livestock ______Other specify You do not use the Well
How many residences are connected to the well list addresses below
Flow deep is the wells Date well was installed
What is the casing depth of the wells
What is the screen interval of the wells
Additional water supply well information
This part to be completed by Responsible Party or their representative
Please return completed survey to S-f2 by using one of the followingmethods
zFaxto /C FS
2.Mailto fl1EcZOYorkVlWrL Rc9 zio
3.Telephone 7O-/73S7-o00
E-mail to fc -Rosev-re-C Coni
If you have any questions please contact the consultant indicated above
What is the source of your drinking Water Supply Well Stream intake Other pleaseexplainbelowWt
Is there water supply well on this pronerty Ye4 No If No disregard remaining nuestions and return survey
-22
line to be completed by Responsible Path or their representative
Incident Number 1816 Incident Name a-Pô JLij1--ujgiH Jjl jfj
Please Provide the Following Information to the best of your knowledgeMJNameandtelephonenumberotpersoncompleungthesirve
Address ofpropertv receiving
survey 311 e_jp1 Si _________________
City Ai_County
What is the source of your drinking water ub11ie Water Supply Well Stream Intake Other please
explain below
Is there water supply well on this prope Yes IINo disregard remaining questions and return sunev
Name and address of owners of propert\with water supply well
llow many water supply wells are on our property
What is the weIls used ford check all that apply Drinking ______lrrigatio Swinyrin P1IWaterLivestockOtherspecifyYoudonotusetheWell/\J tfHowmanyresidencesareconnectedtothewelllistaddresses bel wj
How deep is the wells te/eI vas installed
What is the casing depth of the wells
What is the screen interval of the wells
Additional weter supply vell information
This part to be completed by Responsible Party or their representative
Please return completed survey to Name of Consulting Firm by Date using one of the followingmethods
Fax to Consultants Fax fumber
Mail to Consulting Firm Name and Address
Telephone Consultants Telephone Number
E-mail to Consultants E-mail Address
If you have an questions please contact the consultant indicated above or the US1 Section _________________OtIiceat _____
F-22
This line to be completed by Responsible Path or their representative
Incident Number I7 Incident Name rR-Mt i-t-312 t-7j
Please Provide the Following Information to the best of your knowledge
Name and telephone number of peIon completing the suriev
2-ON /i.jJIj1
Address of proper receiving surrey iOl1 1LJ4Xt Sif6_-i __________________
City 4MTh County -à
What is the scarce of your drinking Water Supply Well Stream Intake Other please
esplain below
Is there ater supply well on this property Yes If No disregani remaining questions and return surve
Name and address of owners of property with water supply well
I-low many ater supply wells arc on your propertY
What is the wells used for check all that apply Drinking ______Irrigation 1sv/q4ning Pool
Water Livestock Other spedfr You do not use the Well If /1
l-lo many residences are connected to the well list addresses below
flU/A
Ho deep is the wellsf Date well was installed
What is the casing depth of the velIs
What is the screen interval of the wells
Additional vater supply well intrmation
This part to be completed by Responsible Parts or their representative
Please return completed survey to Name of Consulting Firrn by Date using one of the followingmethods
Fax to Consultaflts Fax Number
Mad to Consultum Firm Name and Address
lelephone Consultant slelephone Number
E-mail to Consultants EmaiI Address
If you have any questions please contact the consultant indicated above or the UST Section ___________________Office at
-22
incident Number -ftJ Jncident Name rYCrL-i1
Please Provide the Following Information to the best of your lnowledge
RoiJ Miwi 7ô4ç j367Nameandtelephonenumberotpermncompletuigthesurvey
Address of property receiving survey j/tuOl __________________City County
What is the source of your drinking Water Supply Well/Stream Intake/Other please
explain below
is there water supply well on this propert Yes If No disregard remaining questions and return survey
Name and address of owners of property with water supply well
tJ/A
I-low many water supply wells arc on our property
What is the wells used for check all that apply Drinking Irrigation Swi in JolWaterLivestock______Other specify You do not use the Well
How many residences are connected to the well list addresses below
Ai/4
iowdeep is the Wells Iate well was installed
What is the casing depth of the v.clls /\j /_4
What is the screen interval of the wells
Additional water supply well infomiation
This part to be completed Responsible Party or their representative
Please return completed survey to Name of Consultin2 Firm using one ol the followingmethods
Fax to Consultants Fax Nwnbertt
Mail to Consulting Firm Name and Address
Telephone Consultants Telephone Number
E-mail to Consultants E-mail Address
If you have any questions please contact the consultant indicated above or the UST Section
Office at __________________
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