Item No 7 - Phase II Environmental Assessment Report - Propo-OCR

PHASE ENVITh NMENTAL.ASSESSMENT ORT
PROPOSEIWE$T END DEVELMN
WESTMOREIIEAD STREET
CHARLOTTE NORTH CAROLINA
Prepared far
WEST END .LLC
P.O BOX 471721
CflARLOTTE NORTH CAROLINA 28247
by
MACTEC ENGINEERING CONSULTl1G ThC
ZSOi Yorkinont Roail Suite .100
Charlatte North Carolina 28208
April 15 2005
MACTEC Project 6228-05-269.4
MACTEC
MACTiC
April 152005
Mr Chuck Starnçs
WastEhd LLC
Ff3 BOa 471121
charlotte North carolina 28247
Subject Report of Phase II Environmental Asiessment
Tax Parcel LD.s 073-25-0409 IS i404 073-142-01
Proposed West End Development
Charlotte Mecklenllurg County North CarolinaMACTECProject6228-05-2694
Dear Mt Starnes
As authorized by your acceptance of our Proposal No Prop05chltl06 dated March 2005MACTECEngineeringandConsultingInc.MACTEC submits this Phase if Eririroimettcd
Anessmcnt Report This report includes desŁription of the field activities the results obtained
and MACTECs conclusions and recommendations
This report is intended for the use of West End LLC only Reliance on this dOcument by any other
party is forbidden svithout the express written consent of MACTEC and that partys acceptance of
mutually agreeable terms and conditions Use of this report for purpqses beyond those reasonably
intended by West End LLC and MACTEC will be at the sole risk of the user
MACTEC appreciates the continued opportunity to provide our environmental consulting senieeà.
If you have questions concerning this report or this project piease.contact us at 7O4357-8600
Sincerely
MACTEC ENGINEERING AND coNs.uLmwq4c/1
Kelly Hoffman bert Foster Ff3
Staff Scientist Principal
KRRIRCFjew
Attachments
EnØlosures
MACTEC Engineering and Consulting Inc
2801 Yorkmond Rd Suite 100 Charlotte tIC 28208
704-357-8600 Fax [phone]
Proposed West End Development Phase 11 Assessment Report April 152005MACTECProject6228-05-2694
TABLE OF CONTENTS
INTRODUCTION 1-1
1.1 BACKGROUND INFORMATION 1-1
1.2 PURPOSE AND SCOPE 1-1
1.3 SITE DESCRJPTION 1-2
FIELD ACTIVITIES 2-1
2.1 PCB SOIL ASSESSMENT 2-1
2.2 PETROLEUM SOIL ASSESSMENT 2-1
2.3 UNDERGROUND STORAGE TANK ASSESSMENT 2-2
2.4 GROUNDWATER SAMPLING AND ANALYSIS 2-2
RESULTS 3-1
3.1 PCB SOIL ASSESSMENT 3-1
3.2 PETROLEUM SOIL ASSESSMENT 3-2
3.3 UNDERGROUND STORAGE TANK ASSESSMENT 3-2
3.4 GROUNDWATER SAMPLING AND ANALYSIS 3-3
CONCLUSIONS 4-1
QUALIFICATION OF REPORT 5-1
FIGURES
APPENDICES
11
Proposed West End 1evelopnient-Flwse flAssessment Report April15 2005MACTECProject6228-05-2694
LIST OF TABLES
Tables
1.1 General Information
3.1 Soil Analytical Summary PCB Assessment
3.2 Soil Analytical Summary Petroleum Assessment
3.3 Groundwater Analytical Summary
LIST OF HGURES
Figures
SitePlan
PCB Soil Assessment
Former Gasoline Station Parcels
Former Gasoline Station Parcel and Coffee Cup Diner
LIST OF APPENDICES
Appendices
Field Procedures
Photograph
UST Closure Report GeoSyntec Consultants
Laboratory Reports
in
1.1 BACKGROUND INFORMATION
MACTEC recently completed Phase Environmental Assessment of the subject site in Uptown
Charlotte North Carolina The results of the Phase Assessment were summarized in our report
dated January 13 2005
The subject property consists of twenty 20 contiguous parcels of mostly vacant land located
between West Morehead Street Interstate 277 Interstate 77 and Post Street Only of the 20
parcels were developed at the time of our visit The 18 remaining parcels are used for vehicle
parking for events held at the adjacent NFL stadium Nearly all of the parcels were historically
developed at various times from the early 20th century through the 1990s
Our review of historical information indicated that some prior usage of various parcels such as
storage of electrical equipment constitute recognized environmental conditions Furthermore
several gasoline stations were formerly situated along West Morehead Street from the 193 Os until
the early 1970s
The table below summarizes the
assessment
parcel and ownership information and basis for the Phase II
Table 1.1 General information
Tax Parcel ID Number Property Owner Reason for Phase Ii Assessment
073 -252-06 Crescent Resources Past storage of Electrical Equipment
073 -252M9 Crescent Resources Former Gasoline Service Station
073-252-13 Crescent Resources Past storage of Electrical Equipment
073-252.44 Crescent Resources Past storage of Electrical Equipment
073 25 6-03 Crescent Resources Former Gasoline Service Station
073256M4 Crescent Resources Former Gasoline Service Station
073-142-01 Crescent Resources Presence of LAW monitoring well
1.2 PURPOSE AND SCOPE
In March 2005 MACTEC performed Phase II Environmental Assessment activities at the
subject parcels The Environmental Assessment included
Proposed West End Developmeni Phase IlAssessment Report April15 2005MACTECProject6228-05-2694
INTRODUCTION
11
Proposed West End Development Phase IlAssessment Report April15 2005MACTECProject6228-05-2694
underground utility and Underground Storage Tank UST location at Parcel
073-252-13
collection and analysis of soil samples for Polychiorinated Biphenyls PCBs
at Parcels 073-252-06 13 and 14
collection and analysis of soil samples for Total Petroleum HydrocarbonsTPHatParcels073-256-03 04 and 073-252-09
sampling and analysis of groundwater from the existing monitoring well at
Parcel 073-142-01 and
review and analysis of data
The purpose of the assessment was to evaluate the potential for soil contamination related
to the historical storage of electrical equipment at Parcels 073-252-06 13 and 14 the
potential for soil contamination related to the former gasoline stations at Parcels 073-252-09
and 073-256-03 and 04 the potential for groundwater contamination at the LAW well at
Parcel 073-142-0 The following report presents
the methods used and the results of the
environmental assessment preformed by MACTEC at the subject parcels
1.3 SITE DESCRIPTION
The proposed West End Development site consist of approximately 20 acres in Uptown
Charlotte North Carolina Figure Review of U.S Geologic Survey topographic map
Charlotte East North Carolina indicated that the land surface elevation at the site ranges
from approximately 710 feet above mean sea level MSL near 1-277 to low of about 650
feet above MSL near Irwin Creek and 1-77
1-2
Proposed West End Development Phase IlAssessnent Report April iS 2005MACTECProject6228415-2694
FIELD ACTIVITIES
2.1 PCB SOIL ASSESSMENT
Historical maps reviewed by MACTEC indicated that Duke Power Company operated storage
yard for transformers and electrical devices on the parcels shown on Figure from the 1920s to
the 1960s These storage yard facilities were clearly noted on historical resource maps reviewed
for this project
On March 17 2005 MACTECs subcontractor advanced total of 29 soil probe borings P-i
through P-29 at the three parcels shown on Figure Each of the borings was advanóed to feet
below land surface
MACTEC personnel retained one soil sample from each boring for laboratory analysis
The
sample depths for the borings are shown in Table 3.1 Soil samples were submitted to Pace
Analytical Inc Pace in Huntersville North Carolina for the analysis of PCBs by EPA Method
545/8082 The field procedures employed by MACTEC are summarized in Appendix
2.2 PETROLEUM SOIL ASSESSMENT
MACTEC recommended that soil assessment be performed at the parcels shown on Figures and
These properties were occupied by service stations prior to the implementation of UST
regulations in 1988 Therefore it is unlikely that closure testing was performed when the stations
terminated operations The soil assessment consisted of 12 soil probe borings advanced to depths
ranging from to 16 feet below ground surface Each boring was advanced to probe refusal
Probe refusal was encountered at the interface of fill material or residual soil and weathered
bedrock MACTEC retained one soil sample from near the termination depth of each boring for
laboratory analysis
The analysis included Total Petroleum Hydrocarbons TPH Gasoline and
Diesel Range Organics GRO and DRO
In addition to the 12 boring locations shown on Figures and MACEC extended boring P-22
Figure of PCB assessment to depth of 16 feet to collect sample for TPH analysis Based on
conversations with the present property owner and the patched asphalt pavement MACTEC
personnel concluded that the location of boring P-22 was formerly the location of buried gasoline
UST MACTECs subcontractor advanced the probe sampler through the fill soil material to the
2-1
Proposed West End Development Phase II Assessment Report April iS 2005
MACTEC Project 6228-05-2694
native soil The fill material was noted from just beneath the asphalt pavement to about 13 feet
below land surface MACTEC retained soil sample from the 14-15 foot interval for TPH GRO
analysis
2.3 UNDERGROUND STORAGE TANK ASSESSMENT
On March 18 2005
MACTEC personnel observed an apparent Underground Storage Tank UST
vent pipe along the exterior wall of the 1017 Elliott Street warehouse building Therefore MACTEC
retained private underground locating service to confirm the presence of tank at this location
The fieldmeasurements taken by MACTEC personnel indicated the tank diameter is approximately
feet About inch of residual oillsludge was noted in the bottom of the tank The tank location and
orientation is shown on the Photograph in Appendix MACTEC personnel informed
representatives of Crescent Resources property owner of the presence of the tank During our
conversations with Crescent personnel it was confirmed that an 8000-gallon UST was removed from
Parcel 073-252-14 on March 82005 GeoSyntec Consultants prepared UST Closure Report dated
April 2005 The report is included as Appendix
2.4 GROUNDWATER SAMPLING AND ANALYSIS
On March 25 2005 MACTEC personnel collected groundwater samples
from the monitoring well
LAW on Parcel 073-142-01 Figure Prior to sampling the well was purged of water
Following recharge of water in the well the well was sampled using disposable
polyethylene bailer
and disposable nylon rope
The ground-water samples were placed in containers with the
appropriate preservative packed on ice until delivery to the laboratory for analysis chain of
custody form accompanied the samples The samples were analyzed by Pace for volatile organics
EPA Method 8260 and total metals RCRA Metals by
EPA Methods 3010/6010/7470
2-2
Proposed West End Development Phase IlAssessment Report April15 2005
MACTEC Project 6228-05-2694
RESULTS
3.1 PCB SOiL ASSESSMENT
The results of the PCB analyses identified detectable ôoncentrations of PCBs in probe borings P-i
P-4P.-5 and P-6 Figure The PCB concentrations ranged from 0.110 to 0.980 parts per
million
The Soil Remediation Goal SRG for P03s is part per
million None of the identified PCB
concentrations exceeded the SRG established by the North Carolina Department of Environment and
Natural Resources NCDENR
Table 3.1 summarizes the soil analytical results for this assessment copy ol the laboratory report
is included as Appendix
Table 3.1 Soil Analviical Stirnniar PCB Assessnient
Probe Boring Sample Depth feet PUBs Soil Remediation
Number ppb Goal
ppb
P-I 1-2 320 1.000
P-2 2-3 40 L000
P-3 1-2 40 1000
P-4 2-3 130 1000
P-5 1-2 110 1000
P-6 2-3 980 1000
P-7 1-2 43 1000
P-8 2-3 35 1000
P-9 1-2 41 1000
P-l0 2-3 40 1000
P-il 1-2 39 1000
P-12 1-2 45 1000
P-13 1-2 40 1000
P-14 2-3 39 1000
P-iS 3-4 35 1000
P-16 1-2 38 1000
P-17 2-3 41 1000
P48 3-4 37 1000
P-19 2-3 39 1000
P-20 1-2 39 1000
P-21 2-3 40 1000
P-22 3-4 39 1000
P-23 3-4 36 1000
P-24 1-2 42 1000
P-25 2-3 41 1000
P-26 2-3 41 1000
3-1
April15 2005ProposedWestEndDevelopmentPhasellAssessraentReportMACTECProject6228-05-2694
P-27 2-3 41 1000
P-28 3-4 42 1000
P-29 3-4 40 1000
Notes All units reported in ppb parts per billion
3.2 PETROLEUM SOIL ASSESSMENT
Prepared/Date RCF 4-8-05
Checked/Date JDJ 4-11-05
The results of the TPH analyses identified detectable concentration
of TPH DRO in the sample
collected from probe boring P-37 of 10 ppm The State Action level is 10 ppm No detectable
concenirations of TPH were identified in the remaining samples Table 3.2 summarizes the soil
analytical results The laboratory report
is included as Appendix
Table 3.2 Soil Analytical Summary Petroleum Assessment
PB
P-22 14-15 7.0 Not Analyzed
P-31 7-8 4.5 5.7
P-32 8-9 4.4 5.4
P-33 10 4.0 5.6
P-34 3-4 4.0 5.6
P-35 4.0 5.4
P-36 7-8 5.1 6.5
P-37 11-12 4.5 10
P-38 3-4 4.9 5.6
P-39 6-7 4.2 5.3
P40 7-8 4.3 5.3
P.41 15-16 4.6 5.9
P.42 13.5-14.5 3.7 5.4
Notes All units reported in ppm parts per million
3.3 TJTDERGROU1D STORAGE TANK ASSESSMENT
Prepared/Date RCF 4-8-05
Checkedltkate JDJ 4-11-05
No soil sampling was performed around the UST identified at the 1017 Elliot Street Warehouse
MACTEC and West End LLC decided the appropriate course of action was to inform the present
property owner of the presence of the tank and allow them to assume responsibility for removal
and the associated closure testing
The closure sampling and analysis related to the 8000-gallon tank described in Section 2.3
Appendix did not identify petroleum hydrocarbons in excess of the soil-to-water Maximum
Soil Contaminant Concentrations MSCCs
3-2
April15 2005
Proposed West End Development Phase Assessment Report
MA CTEC Project 6228-05-2694
3A GROUNDWATER SAMPLING AND ANALYSIS
Analysis of the groundwater sample from the LAW well identified detectable concentration of
barium 0.077 mgfL No volatile organiçs were identified in the groundwater in this well The
concentration did not
exôeed the NC 2L standard of 2.0 mg/L for barium Table 3.3 summarizes the
data The laboratory report
is included in Appendix
Table 3.3 Groundwater Analytical Summary
Barium total
Prepared/Date RCF 4-14-05
Checked/Date KRH 4-20-05
3-3
Proposed West End Development Phase II Assessment Report April 152005
MACTJ3C Project 6228-05-2694
CONCLUSIONS
Based on
the assessment results MACTEC offers the following conclusions
PCB Soil Assessment
The results of the PCB analyses detectable concentrations of PCBs in probe borings P-i P-4 P-5
and P.6 Figure The PCB concentrations ranged from 0.110 to 0.980 parts per
million The Soil
Remediation Goal SRG for PCBs is part per million None of the identified PCB concentrations
exceeded the SRG established by the NCDENR
MACTEC does not recommend further assessment relative to the former electrical equipment
storage yards
Petroleum Soil Assessment
The results of the TPH analyses identified detectable concentration of TPH DRO in the sample
collected from probe boring P037 of 10 ppm The State Action level is 10 ppm No detectable
concentrations of TPH were identified in the remaining samples
MACTEC does not recommend further assessment relative to the former service station sites
UST Assessment
No soil sampling was performed around the UST identified at the 1017 Elliot Street Warehouse
MACTEC and West End LLC decided the appropriate course of action was to inform the present
property owner of the presence of the tank and allow them to assume responsibility for removal
and the associated closure testing
The closure sampling and analysis performed by GeoSyntec See report in Appendix did not
identify petroleum hydrocarbons
iii excessof the soil-to-water MSCCs
MACTEC recommends removal of the identified UST at the 1017 Elliot Street warehouse
MACTEC does not recommend additional assessment relative to the UST removed in March 2005
by GeoSyntec
Consultants It should be noted that 20-acre tract of land in an historical urban
4-1
Prop osed West End Development Phase IlAssessnient Report April15 2005
MACTEC Project 6228-05-2694
setting may include buried orphan USTs It is common for these tanks .to be discovered during
grading at this type of property
Groundwater Assessment
Analysis of the groundwater sample from the LAW well identified detectable concentration of
barium 0.077 mgtL No volatile organics were identified in the groundwater The concentration
did not
exceed the NC 2L standard of 2.0 mg/L for barium
MACTEC does not recommend further assessment of the groundwater at the site The
LAW well should be abandoned by licensed driller prior to the initiation of grading
activities
4-2
Proposed West End Development Phase IlAssessment Report April15 2005
MACTEC Project 6228-05-2694
QUALIFICATION OF REPORT
The activities and evahiative approaches used in this assessment are consistent with those normally
empkyed in environmental assessment and waste-management projects of this nature Our
evaluation of site conditions was based on our understanding of the site project information
provided to us and data obtained in our exploration The general subsurface conditions utilized in
ourevaluation were based on interpolation of subsurface data
between borings
5-1
ID
ft
ft
ft
I-
ft
ft
ft
SC
ft4
ft
EXELANATIOJi
_____APPROXIMATE LOCATION
OF PROJECT SITE BOUNDARY
APROX1VtATE LOCATION OF
LAW MONITORING WELL
APPROXIMATE LOCA11ON orIC4PARCELSASSESSED
REF 2002 AERIAL PHOTOGRAPH OF MECKLENRURO COUNTY NC POLARIS POPERTf OWNERSHIP LAND RECONDS tNFORMMION Istiai5
PREPARED izu1 OATE1
fljMACTEC SItE PLAN
SI WGJKEEDP/G CCsYSULflNG PROPOSED WEST DEVELOPMENT
CHARLOTTE NORTH CAROLINA CHARLOTTE NORTh tAROUNA
IDAT 410B NO
RCB SOIL ASSESSMENT
PRPOSEI WEST END DEVELOPMENT
CHARLOTTE NORTH CAROLINA
ii
ZXP AN All ON
APPROXIMATE LOCATION OF
PROBE gORING
REF 2002 AERIAL PHOTOGRAPH CF MECKLENBQRG .CoUN1 NC POLARIS PROPERtY OWNERSHIP LAND ItCORDS IMFORMATICIN SYSTEM
JMACTEC
ENO/NEERVIG CONS WIINE
CHARLOTTE HORN CAROLINA
REPAREOr DATE CHECKED DATE J09 140
ci
EXPLANATtON
APPROXIMATE LOCA1ION OF
PROBE BORING
LI
REF 2082 AERIAL PKOTOGRAPH OF MCKLEN8URG COUNTY NC POLARIS .P1OPERTY flW4ER$HIP LAND TECORDS .ItWORMAflQN SYSTEM
MACTECMNEB1WCCWSULWG
CHARLOTTE NORTh CAROLINA
PQRMEfl.ASOUNE 8TAflON FARCELS
PROPOSED WEST END DEVELOPMENT
CHARLOTrE NORm CAROLINA
fTEPANEO fl ..J DAlE ICHECKED DATE iDa NO PIOURE
EXPLANATION
SULVNG iNC
ARLOTtE WORTh CAROLINA
FORMER QASOUNE sr.PARQELICOFFEE OUP DINEF
PROPOSED WEST END DEVELOPMENT
CHARLOTTE NORtH tAROUNA
POLARIa.PROPERTY OWNERSHIP LAND RECORDS INFQRMAIKN SYSTEM
CHECXED DATE4_At 408 NO 697Rfl5---Rq4 fIGURE
Ienqwsed WnzEndDsye1apnrqnzPha IIAssasrneniRepuri April JS..2OO.5
MACTEC Project 62284 294
FIELD PRXSDURES
The iinld procedures used in the performanre of MACTBfl worh are as follows
Soil Borings/Sd Samphug
Soil sathples were edileoted frorn.bod sbyuSgDireet Push Teelmologyc yigstainloss-steel
core barràls to advance the boreholes Continuous soil samples were obtained four-fo lengths
i4thIastaipiesssteelsSpling tube and acetateinbe liners
To reduce the potential for cross-contamination the subcontractor dceontuiunated down-hole
prohingeqt4pnsentbysteam-cleaning
The soil .saipples Were liluad in laboràtoiy-prepared sample eontthsrs marked with unique
identifying number p140cc on ccc in sample cooler and delivered to Pace North Carolina
certifiedlaboratory located in Runersville North Carolina for analysis The samples were
inairitaitied wider chain-of-custody protocol
MonitoringWØll Groundwater Sampling
The waterlevelin the well was measured withan electric water level indicator
todetennine depth to
the aier surfiree from the top of the PVC riser pipe The measured water depth was used in
oonjunetion with tlttotal easing depth to determine the height Of the.wacer eolumnand.thc volume of
water in the monitoring well
Priono sampling MACTEC fieldrepresentative purged the well of atleast thme casing volumes of
water groundwater sample was collected using disposable polyethylene
bailer After samphngMACTECplacedthecontainersonicefordeliverytothelaboratoryMACfECmaintained
appropriate thain-of custody records for thesainplc
Photograph Paint niarkingson asphalt pavemen
and orientation of
North Carolina
Departmentof Environment and Natural Resources
Underground Storage Tank UST-12 Closure Report
NCDENR FACILITY ID 0-031324
1017 ELLIOT STREET
CHARLOTTE NORTH CAROLINA
Prepared by
GEOSYNTEC CONSULTANTS
1255 Roberts Blvd NW Suite 200
Kennesaw Georgia 30144
GeoSyntec Number GK3363
April 2005
Prepared for
Crescent Resources LLC
400 South Tryon Street
Charlotte North Carolina
TABLE OF CONTENTS
1.0 GENERAL INFORIVL4.TION
LI Facility Information
12 Contacts
1.3 Underground Storage Tank Information US1
1.4 Site Characteristics
2.0 CLOSURE PROCEDURE
2.1 Closure.Preparations
2.2 Soil Excavation Activities
3.0 SITE iNVESTIGATION
3.1 Field Screening
3.2 Soil Sampling
3.3 Groundwater Sampling
3.4 Analytical Results and Discussion
4.0 CONCLUSIONS AND RECOMMENDATIONS .6
FIGURES
Figure Site Location
Figure Plan View of UST Location
Figure Vertical Proffle of Tank Pit with Sampling Locations
TABLES
Table Underground Storage Tank Infonnation
Table Readiugs
Table Sample Summary
Table Analytical Results Appendix
Table Detected Compounds
APPENDICES
Appendix Table Analytical Results
Appendix Notification of Intent UST Permanent Closure or Change-in-Service
UST-3 Form
Appendix Site Investigation Report for Permanent Closure or Change-in-Services
of UST IJST-2 Form
AppendixD Certificate of UST disposal
Appendix Copy of all laboratory analytical records and Chain-of-Custody
Appendix Photographs
of closure activities
Appendix Geologic logs for excavation
11
North Carolina Department of Environmental and Natural Resources
Underground Storage Tank Closure Report EJST-12 Form
NCDENR Facility ID 0-031324
1017 Elliot Street Charlotte
NC
Crescent Resources
1.0 GENERAL INFORMATION
The information in this report follows the general outline identified in the UST-12
Form format UST-3 Form Notice of Intent UST Permanent Closure or Change-in
Service Closure Appen and UST-2 Fo Sits Investigation Report for Permanent
Closure or Change-hi Service of UST Appendix are included in this report
11 Facihty Information
Vacant Duke Power Pool Car Garage
Facility ID 0-031324
1017 Elliot Street
Charlotte North Carolina
MecUenburg Coty
Date of Report 31 March 2005
UST Owner and Operator
Crescent Resources LLC
400 South Tiyon Street Suite 1300
Charlotte NC 28201
704.382.8009
1.2 Contacts
Primary Contact Person Kevin Doherty Regional
Director Property Management
Crescent resources LLC 400 South Tryon Street Charlotte
NC 28201 Telephone
704.382.8009
Closure Contractor AD Environmental and Industrial Services Inc 2718 Uwharrie
Road Archdale NC 27263 Telephone [phone]
Primary Consultant Ronald Santini GeoSyntec Consultants 16049 Stonemont Road
Huntersville NC 28078 Telephone [phone]
Primary Laboratoiy
Prism Laboratories 449 Springbrook Road Charlotte NC 28224-
O4O3Teiephone7045296364-Contact--MgeiaD-Overcash-
1.3 UST Information
The characteristics and pertinent information about the UST are listed out in Table
Table Underground Storage Tank Information
Tank ID Tank FACID 0-031324
Installation Date 1989
Size gallons 8000
Tank Dimensions 25 ft long ft diameter
Tank Construction Fiberglass
Last Known Tank Contents Gasoline
1.4 Site Characterislics
No known petroleum releases have occurred at the facility The property was
formerly the Duke Power Pool Car Facility The facility was closed in 1990 and
transferred to Crescent Resources LLC Crescent subsidiary of Duke Energy in 1992
and is currently vacant The pool cars were fueled at the facility from an 8000 gallon
underground gasoline storage
tank Duke Power consolidated the operation of pool car
facilities in the late 1980s which resulted in the closing of the facility and tempOraiy
closing of the UST in 1989
The current uses of adjacent and surroundings properties are commercial industrial
and vacant lands Adjacent property to the north is Interstate Highway 1-77 site
location map showing the site and surrounding properties is presented on Figure
Mecklenburg County is located within the Inner Piedmont Belt of the Piedmont
Physiographic Province of North Carolina Sites in this area are underlain by
metamorphic and intrusive rocks consisting predominately of various forms of schist
gneiss granite gabbros and diorites that near the ground surface have been weathered
into distinctive residual soil known as saprolite The site soils from the tank excavation
floor and side walls consist of texture similar to sandy loam and were light brownish
yellow in color from the surface to depth of 20 feet below ground surface bgs
Appendix
Piedmont topography is characterized by gently rolling hills separated by small to
moderately sized streams Surface water and groundwater drainage patterns within the
Piedmont generally indicate the movement of water from topographic highs to
topographic lows Piedmont hydrogeology is characterized by single water table flow
system that includes the saprolIte partially weathered rock and unweathered bedrock
Recharge typically occurs in hill-top areas and discharge occurs in streams rivers and
lakes It can be assumed for Piedmont areas that the surface topography approximates
groundwater flow direction However due to the urbanized nature of the area
surrounding the property it can be assumed the natural groundwater flow patterns have
been altered
Groundwater at the site is presumed to flow from the topographic highs in the south
southeast section of the property to the topographic lows at the north-northwest
section
of the property Groundwater was not encountered in the excavation at depth of 20 feet
2.0 UNDERGROUND STORAGE TANK CLOSURE PROCEDURES
2.1 Closure Preparations
Preparations for tank closure included notification of the Charlotte City Fire
Department by the tank removal contractor Crescent requested marking of all
underground utilities in the excavation and adjacent areas which was completed by local
utilities pnor to excavation An initial measurement of residual petroleum product
remaining in the tank was gauged with tank measuring stick by the tank removal
contractor and the gauging indicated the tank was thy This was confirmed by visual
observations once the tank was removed from the excavation
2.2 Soil Excavation Activities
The excavation was accomplished using track hoe The concrete surface was first
removed from the area to be excavated exposmg the if material surrounding the tank
The fill material was excavated approximately four feet on each side and at the ends of
the tank Care was taken to minimize damage to the tank during excavation In addition
care was taken to minimize damage to piping systems Excavation continued until the
subsurface native soils were exposed on the pit bottom and sidewalls The area
surrounding the tank was filled with inch gravel from top to bottom Once the fill
material was removed exposing the entire tank the tank was lifted from the excavation
by the track hoe and placed on fiat bed trailer for transport and disposal Certificate of
UST Disposal Appendix Approximately 50 cubic yards cyd of gravel material
was removed from the excavation The excavated gravel was clean with no staining
odors or measurable readings on the photo ionization detector PID Water free
product or bedrock were not encountered during the excavation process photographic
log of excavation activities is included as Attachment
The material placed back in the excavation consisted of excavated materials and
approximately 50 cyd of clean soil obtained from the Martin Marietta Quany Beatys
Ford Road Charlotte NC The soils were compacted using the track hoe prior to placing
final cover of crushed stone on the excavated area
Field observations and measurements during excavation did not identify the presence
of petroleum impacted
soils
3.0 SITE INVESTIGATION
3.1 Field Screening
Field Screening Field screening was conducted using Photovac Model 2020 Pro
PID Prior to use the PID was calibrated using indoor air to set the zero gas to parts per
million ppm The instrument was then calibrated against 100 ppm isobutylene
calibration gas standard The instrument reading was 99.9 ppm and no calibration
adjustments were made
Sixteen P11 measurements were
made from the excavation including areas under
the dispenser main product line and the tank The layout of the UST and associated
appurtenances is shown on Figure In addition during initial excavation preparations
measurement was also taken from the tank fill port to determine the presence of
petroleum products
PID readings during
excavation ranged from 0.4 ppm to 8.5 ppm
and the fill port measured 27.8 ppm Table Based on the relatively low P11 readings
less than 10 ppm the data suggests that petroleum products
have not appreciably
impacted the fill materials or the soils beneath the tank In addition the low P11 reading
from the tank fill port suggested minimal residual product was remaining in the tank
This was confirmed by physical measurements and observations once the tank was
removed from the excavation Both physical measurements and visual observations
indicated the tank was thy The 27.8 ppm reading can be explained by residual vapors
remaining in the tank
Table P11 Readings
SAMPLE DEPTH
SAMPLE LOCATION SAMPLE ID feet DATE TIME PID ppm
Gravel Fill Material NA Random 318/2005 NA 3.4
Gravel Fill Material NA Samples 3/8/2005 NA 2.6
Gravel Fill Material NA Collected 3/8/2005 NA 1.8
Gravel Fill Material NA from Irack hoe 3/8/2005 NA 7.4
Gravel Fill Material NA bucket 3/8/2005 NA 7.1
Gravel Fill Material NA during 3/8/2005 NA 3.5
Gravel Fill Material NA excavation 3/8/2005 NA 8.5
Gravel Fill Material NA activities 3/8/2005 NA 2.5
Gravel Fill Material NA 3/8/2005 NA 6.3
Tank Bottom West Ti 22 3/8/2005 1200 1.3
Tank Bottom Center T2 22 3/8/2005 1245 2.4
Tank Bottom East T3 22 3/8/2005 1300 2.1
Dispenser Pad Dl 05 3/8/2005 1230 1.2
Dispenser Pad NA 5-i 3/8/2005 1240 0.9
Dispenser Pad NA 10-15 3/8/2005 1245 0.6
Product Une NA NA 3/8/2005 1130 0.4
Tank Fill Port NA NA 3/8/2005 0935 27.8
Field screen samples collected from the track
hoe bucket were placed in oz amber
colored glass jars leaving room for headspace and covered with tin foil rubber band
was placed over the tin foil around the jar lip to seal the container The samples were
allowed to equilibrate for approximately 10 minutes At the end of 10 minutes the
headspace was analyzed for total
volatile organic compounds by inserting the probe of
the PID through the tin foil to make field measurements The highest P11 reading
observed was then recorded This process was completed for excavation field screening
and initial screening of soil samples submitted to the laboratory for analysis
3.2 Soil Sampling
Soil sampling locations are
identified on Figure In accordance with Guidelines for
Tank Removal North Carolina Underground Storage Tank Section four soil samples
were collected three from the bottom of the tank footprint and one from below the
dispenser Samples were not collected from the product lines or other piping systems
because visual observations suggested leaks had not occurred from the piping system
Table summarizes the sample locations sample IDs sample depths date and time P11
readings and analytical methods All samples collected were grab samples from
excavated soil and analyzed using EPA Method 5030/8260B and MADEP VPH
methods
Table Sample Summary
EPA
SAMPLE SAMPLE DEPTH MADEP Method
SAMPLE LOCAtiON ID ft bgs DATE 1ME PID ppm VPH 603S8260
Tank Bottom West Ti 22 3/8/2005 1200
Tank Bottom Center T2 22 38/2005 1245
Tank Bottom East T3 22 3/8/2005 1300
Dispenser Pad Dl 3/8/2005 1230 1.2
Tank Fill Port NA NA 3/8/2005 935 27.8 NA NA
The excavation pit was dry at the time of tank removal No groundwater samples
were collected
All soil samples were collected in pre-preserved sample containers provided by the
laboratory All sampling equipment used was disposable eliminating
the need for
equipment decontamination between samplings
Prior to sample collection sample containers were labeled with client sample
ID sample location date time analyte and samplers initials
New gloves were used and then discarded after each sampling
Samples analyzed by EPA Method 5035/8260 were collected in triplicate
pre-weighed VOA vials using disposable coring
device to collect
minimum grams of soil
The soil sample was immediately transferred to the VOA vial tightly capped
and swirled gently to expose the sample to the Sodium Bisulfate preservative
second sample with Sodium Bisulfate preservative was collected in the
same manner
The third sample was preserved with methanol and collected in the same
manner as the Sodium Bisulfate preserved samples
fourth sample was collected for dry weight determination and for soil
characterization
One sample for MADEP VPH analysis was collected with an EnCore
sampler the EnCore sampler was then labeled and placed in the sample bag
provided with the EnCore sampler Duplicate samples for MADEP VPH
were not collected
sample was also collected for field screening with PB
All samples with the exception of the P11 sample were then immediately
stored in cooler at until delivered to the laboratory
The Chain-of Custody for each sample was completed and the process was
repeated until all four samples were collected
3.3 Groundwater Sampling
Groundwater samples from the excavation pit were not collected because the
excavation was dry at the time of tank removal
3.4 Analytical Results and Discussion
Analytical results are presented in Table Appendix and Appendix Four soil
samples were analyzed using EPA Methods 503518260B and MADEP VPH method.
Results of the analysis indicate all samples were
below the reporting limits for petroleum
hydrocarbons gasoline However Iwo samples contained acetone above the reporting
limits 67 microgram per kilogram ugfKg Dl 78 ugfKg and one sample contained
methyl ethyl ketone MEK T3 30 uglKg The laboratory reporting limit for acetone
and MEK is 22 ug/Kg Laboratory QC results for these samples were below the reporting
limits and not detected Acetone is known laboratory contaminant and even though it
was not present in the lab QC samples does not necessarily rule out lab contaminationMEKisanindustrialsolventandisnotassociatedwithgasolineThefact that MEK was
not detected in any of the other samples would suggest it presence is isolated Both
compounds were compared to the Maximum Soil Contaminant Concentrations found in
Table of Guidelines for Assessment and Corrective Action North Carolina
Underground Storage Tank Section and both were significantly below the
Residential/Industrial/Commercial Soil Cleanup Levels as follows Table
Table Detected Compounds
Sample Sample
Residental Soil lndustraillCommercial
T3 Dl Cleanup Level Soil Cleanup Leves
Compound uglkg uglKg mg/Kg mg/Kg
Acetone 67 78 1564 40880
Methyl ethyl ketone 30 BRL 9385 245280
4.0 CONCLUSIONS AND RECOMMENDATIONS
Removal of the 8000 gallon fiberglass gasoline tank at 1017 Elliot Street Charlotte
NC was completed in timely and safe manner All product piping systems dispenser
piping and tank were free of leaks and/or cracks at the time of excavation The tank was
void of liquid and the inside dry at the time of removal Visual observation of excavation
pit soil conditions field PID screening of soils tank condition and laboratory results
suggested release from the tank or piping system had not occurred prior to excavation
However two compounds acetone and methyl ethyl ketone were detected at low
concentrations in two pit floor samples These concentrations were compared to the
Table Maximum Soil Contaminant Concentrations found in Guidelines for Assessment
and Corrective Action North Carolina Underground Storage Tank Section
Residentialllndustrial/Commercjal Maximum Soil Contaminant Concentrations and were
significantly below the cleanup levels
GeoSyntec concludes that no further action associated with tank closure is necessary
and the tank closure should be made permanent with regulatory concurrence based on
the following findings
The tank was intact at the time of excavation
The tank was free of liquid
There was no
evidence of leakage
Soils staining was not evident on the pit floor
Sample results do not show indications of petroleum leak and
Both acetone and MEK the only two compounds detected were significantly
below the residential/industrial/commercial cleanup levels
FIGURES
Figure Site Location Parcel ID 07325214 Outlined in Green
UST Location
1017 EllIot Street
Charlotte NC
Crescent Resources LLC
23 Much 220
IS 20
oNNuLs.ri812IobtslrtiVSitg2001uuaw30144
Figure Plan View ofUST Location
ILIT
1CFTC APOP 1ST PT SST
OVA
bc. 0.cu
ThTP tC 1O PO.J
rI
Figure Vertical Profile of Tank Pit with Sampling Locations
Test Pit RŁord
APPENDIX
Table Analytical Results
Table Analytical Resulis
2851.8 ne 091 S.s99.8 I54 0890t AS
--TI 3/87256 5001675 112102 11I.2.T8te 835-34-6 2808 SRI 5.1519919
TI 3/8l2956 34601815 112702 1l1-Thd4o91hai 11-55-6 12606 810 5.1 9119
TI 38 5507675 1177172 l.I.2.2-T91r87I6hae 1-34-5 1606 6511 5.1 p9819
Ti 319 5007675 112702 1.l.2.TsIdl50o-1.2.2-T50o91hae 1-13-i 286 SRI 1078119
TI 3912051 6007675 112702 112-TId4.550ne 1-10-5 1606 6511 5.1 991g
TI 319l3/X18 5507675 112702 1l-OIdSou91hae 7534-3 2808 BR 51 919
Ti 3813505 34007675 112102 1I-0Id9.o918.le 78-35-4 1608 650 5.1 99q
TI 3185282 34007675 112702 ll-15dr.e 83-586 SRI 5.1 91kg
TI 3813506 5007675 112702 1.23-T4dthe 87-61-6 2606 SRI p98q
TI 31912035 5007675 112702 IZ3-Tfld1rr79a1e 95-18-4 82808 581 5.1 p9819
TI 2812525 0801615 112702 lZ4-T4dth.iz.e 135-52-i 80806 SRI I/419159
TI 3812516 0807675 112102 124-Tdmhe.e 95.826 2808 681 II 10
Ti 382025 10001675 112702 12.0m.-3n515ne 95-12-8 26081 SRI 8-I 9119
Ti 3l8l5 34001615 112702 1.2-011r.noe85ae 008 106-82-4 82808 SRI 5.1 9119
TI 31 34001615 112702 1.243d491.e 5-50-I SRI 10 919
TI 38l 28007675 1127172 12-1787091556 101-00-2 2818 SRI 5.1 i98tg
TI 3/8 34001675 112702 1.2-UIthkoopq.e 8.57-5 2608 SRI 5.1 945
TI 3I8I 35007875 1127172 i.3-5-T15si91fl4b.51 108-817-8 2808 68 ii 999
Ti 319/2825 35007675 112702 1.3-0I.z..e 41-73-I RI II ig9g
TI 34007875 112702 l.3-OIdlaçxqsa8-142-28-9 82660 SRI 5.1 1i989
Ti 3l8/5 .18607675 112102 i4-75dl.ob.w.106-46.7 872808 SRI 519519
Ti 3/80805 26001675 117702 1404d4674x4a 110-56-4 83508 6541 II 559119
TI 3183558 1007675 117702 L2-DdIsa 600-34-7 82808 881 5.1 19819
Ti 35912835 5007675 112702 2-C h494 61-or 110-75-8 82608 SRI ii 1919
TI Y9I 1007675 112702 2-CtlorUdo.95.49-8 82956 SRI 10 pglkg
Ti 3191 1007675 1127172 41ele 91-78-6 62808 SRI 51 pgikg
Tl 39 5007675 112702 4Cl4wrtdo.108-43-4 8288 BR 10 519919
TI N81 34007975 112702 kM6h5-2.pez..MI5X 108-10-I 2608 BR 1055919
Ti 3/81382 35007875 112702 M6.i 7-64-1 2808 SRI 32 949
Ti 3l5l 35007675 112102 onS91 107-02.8 2508 SRI Ill 989
Ti 3513506 1007675 1i2702 A568o 107-13-1 2608 881 16049
TI 218I 5007975 112702 8.0.e 1-43-2 82608 SRI 3.1 59119
TI 381285 35007675 112702 Segone 108-85-I 2808 SRI 5.1 55949
Ti 3812015 35007675 112702 koroMas61-.74-67-5 82608 SRI 8-I 9119
Ti 2/852165 34007675 112702 8-onoSdlorm10t.no 15-27-4 82608 SRI 5.1 ig81g
TI 28285 5007675 112702 6-omothu 5-25-2 82808 SRI 5.1 pg1g
Ti l8I 5107875 1127172 8500.6556 4-83-9 82608 810 10519919
TI 39/3335 34001675 112702 Cb6iflde 8-15-0 SRI 10 919
Ti 391 5001975 1127172 Cabw6ra199ale 56-73-5 82808 681 5.1 I91
Ti 31S5 1001875 112702 18-95-7 82606 SRI 5.1 59919
Ti 3/8/385 5001675 112702 Ct4uu99r.uaudt.ie 124-46.1 28118 88 5.1 911g
TI 319/2335 5001675 112702 3.61-.7560-3 2608 661 10 5919
Tl 3/813516 5107675 112702 Ct450.nI 67-95.3 2808 8511 5.1 559819
II 3185285 5107675 112702 C4..n.4-87-3 2808 6511 1078119
Ti 3/873182 1007675 112702 su-13-0t45oe 156-55-4 82606 8511 5.1 51916
Ti N8108 34507675 112702 .I3-D5ct8orrop.ne 10001-01-5 82808 SRI 5.15989
Ti 30d 35007675 112102 D8ruaI 7480-3 2808 8511 5.1 5159
Ti 3/8/2/165 35007675 112702 D18756i1156561-au 75-61-6 8511 10 9159
TI 319/382 34087675 112102 B9t.ze 10041-4 2908 SRI 6.1 p94g
TI 3953165 5607675 112702 Hob58891.ne 87-86-3 2938 SRI 15 7/kg
Ti 3812015 5007875 1i27972 lsqwopyl 8e IFS 108-22.3 2608 8551 5.1 95g
TI 35007875 112702 Iik...6-82.8 2608 SRI ID 9819
TI 5007875 1127172 m6-X34eu 13477741-2 82608 SRI IS 949
TI Y50 5007615 1127172 A61-8915lk19aioMEI4 79-93-3 872808 8511 95kg
Ti 38/3805 25007875 112102 MdkgI .68 4-88-4 82808 SRI 556/69
Ti 31513551 35007675 112102 M6kg5H556kerMrSE 1634-04-4 82808 8511 5.1 gIkgTI3553552007675112702.814uflde 75-450.2 8511 iO 51899
Ti 3/$5 5007615 112702 n-11.0.104-51-8 8288 SRI 15 19415
Ti 30/355 5001875 112702 n-P.wt..une 103-95-I 82608 SRI 559819
Ti 3/0/27151 5607675 1i2702 NRI496e 91-20-3 2608 8511 8.1 519418
Ti 3852015 1007675 112702 rX4ne 95-41-9 288 5541 5.159919
Ti 362106 20007875 i12102 rIsrurs6duore 9-87-8 82858 SRI 1555916
Ti Y8I 2007875 112702 0.-or..se 136-986 82808 8511 5919
Ti 36285 25007675 112102 9cet 106-425 82808 651/5.1 559/kg
Ti 3/613285 36007615 112702 .t-So8ythenz.9-00-08 83808 SRI 35515919
Ti 35012531 25007975 112702 127-16-4 2608 SRI 41949
Ti 319/255 857675 1i2102 ok.105-88-3 82808 SRI Si 249
Ti 3181285 25027875 112702 k.-i.2-OIthIoro6ti.e 156-60-5 288 SRI 6.1 989
TI 36001915 ii27172 -ipoore 1861-826 2818 SRI 5.1 45999
TI 316/205 26007615 1127172 rss4o.6k.19-01-6 82608 SRI 5.1 9819
TI 31813855 1007675 112702 I446kuan6hw 5-99-4 2608 SRI 5.1 51919
Ti 319131168 5607675 112793 ksyId81e 8-15.0 08 SRI l04g
TI 3/61 5657975 112793 //kRIthIc4de 75-01-4 53808 SRI 107819
TI 3813505 34007975 112702 CS-CS 59/th6Ics N/A MAOEPVPH 8541 8.4 mglkg
Ti 31912015 5607675 112702 CCiOA.udics N/A 0AOEPVPI-I 8511 8.4 mg/kg
TI /S 5007675 112702 35CI248k65cu N/A 4ADEPVFH SRI 84 mgIkg
/keIaD
Sample ID S.Oe SamID PPsmID anpaest CASS 080/RI nO
12 3/82005 5007676 112103 l.1j2-Tmiie 630-20-6 62606 SRI 52 g/kg
12 3/612005 25001676 112703 1.1.1-Ticfllaoehaie 71-55-6 62608 SRI 5.2 gtg
12 3/812005 5007676 112703 1.122-TetrachIoeIheie 9-34-5 82608 SRI 5.2 08Cg
12 3/012005 5007676 112703 1.t2-T6c12.2-T5i01nOhe5e 6-13-1 2806 SRI 10 g8g
72 3/8/2005 5007676 112703 l.l.2-T0cflIee4hane 79-00-5 02606 SRI 5.2 pg/kg
12 3/8/2005 25007676 112703 1.1-DcInOoase 75-34-3 82608 SRI 52 g/kg
12 3/8/2005 25007676 112703 1.l-Dichbotiee 5-35-4 82608 SRI 5.2 gtg
12 3/82005 5007676 112703 1.1-D/choprcpe 03-58-6 82808 SRI 52 g/kg
12 3/8/2005 5007676 112703 l.23-1dcaben08e 7-61-6 2606 SRI 10 pg/kg
12 3/8/2005 20607676 112703 123-Tdthlaqrqsane 96-18-4 82806 SRI 5.2 glcg
12 3/812005 5007676 112703 1Z4-Trenzam 120-82-1 82806 SRI 10 gilsg
12 318/2005 25007676 112703 1.Z4-ThmeIhslbenzane 5-63-6 82806 SRI 10 pg/kg
12 3/82005 5007676 112703 12-Da3-thnOcpmpane 98-12-8 62606 SRI 5.2 pg/kg
12 3/8/2005 5057676 112703 12-D81unoetheeSD8 106-93-4 82606 SRI 5.2 g/kg
12 3/82005 25007876 112703 1.2-DchIrzene 5-50-1 62608 SRI ID g15g
12 3/8/2005 25007876 112703 12Iiaflse 107-06-2 82608 SRI 5279/kg
12 3/812005 25003675 112703 12-DIch1ropragene 78-87-5 82606 SRI 52 pg/kg
12 3/8/2005 25007678 112703 1.3.5-T0methtenzeie 108-67-8 82608 SRI 10 pg/kg
12 318/2005 25007676 112763 1.3DhnOthze 41-73-1 82608 SRI 10 g/kg
12 3/8/2005 5007676 112703 1.3-DlchnOsgmp98e 142-26-9 82608 SRI 5.2 9619
12 3/8/2005 5007676 l1270 1.4-D/chtthizene 106-46-7 82606 SRI ID g/kg
12 3/8/2005 25007976 112703 1.4-Dkhlorokutane 150-56-5 82608 SRI 10 pglcg
12 3/8/2005 25007676 112703 2.2-opnpane 590-20-7 02605 SRI 5279/19
12 3/812005 5007576 112705 2-ChIaoeth4 inl dher 110-75-8 82608 881 10 g/kg
12 318/2005 25007676 112703 2-ChkXtdUase 95-48-8 82606 SRI 107986
12 3/8/2605 25007676 112703 -Hmiae 591-78-0 52608 SRI 52 g/kg
12 3/812005 5007676 112703 4-ChiacOdugie 106-43-4 26DB SRI 10 pg/kg
12 31812005 5007676 112703 4-Mdh51-2-penanaseMISI 108-10-1 62608 SRI 10 pg/kg
12 318/2005 25007676 112703 Ac0/ae 7-84-1 82606 SRI 21 08g
12 3/8/2005 25007676 112703 Acrde/k 107-03-8 02608 SRI 100 gAcg
12 3/82005 25007076 112703 cc4o4tJ1g 107-13-1 82608 SRI 100 15980
12 3/82005 5007676 112703 Bgizgia 1-43-2 82608 SRI 3-1 p9/kg
12 3/8/2005 5007676 112703 SrcmcOenzenc 108-86-1 82608 SRI 5219/kg
12 3/8/2005 5007676 112703 Srngihksrume/flgie 74-97-5 82608 SRI 5.2 19/kg
12 3/8/2005 5007676 112703 SnnOcfltaainOlse 75-27-4 82608 SRI 5.279159
12 3/82005 25007675 112703 Bmmdaln 75-25-2 52608 SRI 5.2 pg/kg
12 318/2005 25007676 112703 Scmafldhese 483-9 8260B SRI 10 pg/kg
12 3/82065 25007676 112703 Caibas dsulflde 75-15-0 02606 SRI 10 pg/kg
12 3/8/2005 25007676 112703 Carbas Istaichialde 56-Z3-5 82608 SRI 52 pg/kg
12 3/0/2005 25007676 112703 hiarchgizege 108-90-7 82608 SRI 52 pg/kg
12 3/82005 5007676 112703 Chlao69rananethaise 124-48-1 82606 SRI 52 pg/kg
12 3/8/2005 25007676 112703 ChigocOhege 5-00-3 52606 SRI 10 pg/kg
12 3/812005 25007676 112703 Chiar060mi 67-66-3 82606 SRI 5.2 pg/kg
12 3/8/2005 25007876 112703 Chigomeosaise 4-87-3 82608 SRI 10 pg/kg
12 3182005 25007676 512703 s-l.2-D1hlabahgie 156-55-4 8250B SRI 52 pg/kg
12 318/2005 25007676 152703 cis-1.3-Dbhlompmpgie 50061-01-5 826DB 881 52 pg/kg
12 3/812005 25007676 112703 Dadhege 74-95-3 826DB SRI 5.2 pg/kg
12 3/8/2005 25007676 512703 Ohlarod6lucucncOhege 75-61-6 82608 SRI 10 pg/kg
12 3/8/2005 25007676 112703 Eth81enzene 100-41-4 82608 SRI 62 pg/kg
12 3/82005 25007676 112703 Ham chutudene 67-88-3 8260B SRI 16 pg/kg
12 3/812005 25007876 112703 sopmp4 elhar IPE 108-20-3 82608 SRI 52 pg/kg
12 3/8/2005 25007676 112703 sop4begzene 98-82-8 82608 SRI 10 pg/kg
12 3/82005 25007676 112703 I.p-XI.lenes 136777-61-2 2608 SRI 16 gg
12 3/8/2605 25007675 112703 Me0fll dh4 bagie MEK 78-93-3 82508 SRI 21 pg/kg
12 3/82008 25007676 112703 Methyl bade 74-88-4 82608 SRI 10 pg/kg
12 3/82005 5007670 112703 McOt-buty4dharMT5E 1054-04-4 62608 SRI 5.2 pg/kg
12 3/82005 25007676 112703 Methyieneclosxide 75-09-2 2608 881 10 98cg
12 3/8/2005 25007676 112703 0-81itylbelzene 104-51-8 82608 SRI 16 pg/kg
12 3/8/2005 25007676 112703 -Pljlbg5zg1e 103-65-1 82608 SRI 10 pg/kg
12 3/8/2005 25007676 112703 NihthaIgo 91-20-3 82606 SRI 6.2 pg/kg
12 3/82005 25007676 112703 o-Xslene 95-47-6 2606 881 52 pg/kg
12 3/82005 5007676 112703 p-leqsryltdue 99-07-6 82906 SRI 16 pg/kg
12 3/82000 25007676 112703 sec-Suty6enzgie 135-98-8 52608 SRI IS pg/kg
12 3/8/2005 25007676 112703 %Tene 100-42-5 82608 SRI 5.2 pg/kg
12 3/8/2005 25007676 152703 est-Butylbaszeie 98-06-06 82608 SRI 21 pg/kg
12 3/5/2005 25007676 112703 Telrach/abahese 127-16-4 82606 SRI 10 pg/kg
12 3/8/2005 25007076 112703 Tcluene 109-88-3 62608 SRI 5.2 pg/kg
12 3/8/2005 28007676 112703 ram-I .2-Dich/acethase 158-80-5 02608 SRI 5.2 pg/kg
12 318/2005 25007675 112703 5-ess-1.3utarcgrcgene 10061-02-6 02008 SRI 5.2 pg/kg
12 3/8/2005 25007676 112703 TrIchlaoelhene 79-01-6 82608 SRI 52 pg/kg
12 3/812005 25007676 112703 lichlaolkjaunethane 75-69-4 826DB SRI 5.2 pg/kg12318/2005 25007676 112703 Onyl acetate 75-15-0 62605 SRI 10 pg/kg
12 3/5/2005 25007676 112703 lInyl ctilaitle 75-01-4 82608 SRI 10 pg/kg123/82005 25007076 112703 CS-Ca .6IIPhaIICS N/A MAIDBP 5/PH SRI 8.3 mg/kg
12 3/8/2005 25007676 512703 COAraoetIcs N/A MAOEPWH SRI 82 ig/kg123/8/2005 25007676 112703 3/-C12ftlhe6cs /A MADEPVPH SRI 8.3 sgi59
06eL
58nçIe82 e0 1918ID P495n93 ar-ut AS Me8800 U._
13 3/80805 5007671 112704 .1.1.2-TdracNaoShane 830-26-6 SRI 53 9kg
13 3/63205 5007677 112704 l.1j-TflchIooh /1-55-6 2808 SRI 5.5 pg6g
12 3812005 5007677 112704 1.1.2.2-TdtcflIahane 9-34-5 12608 SRI 5.5 pg.6g
73 3812606 26007677 112704 1.12-malol.2a-Tr/ftjaceth83e 8-13-1 2808 BRL II 969
13 3/82005 5007677 112704 l.12-TrIclroethaie 9-00-5 2808 SRI 5.5 jig6g
13 3812605 25007677 112704 1.1-diIciohie 5-343 2606 8141 5.5 u91w
T3 3/812605 20007871 112704 1.1-DicIiloroethie 5-35-4 82605 SRI 5.5 pg/kg
13 362005 5007677 112704 1.1-33oie 33-58-8 82608 SRI 5.5 pg/kg
13 38/2005 25007677 112704 123-Tflclsoraiens8le 7-61-6 2808 SRI Ii pg6g
13 3/82005 6007677 112704 1.Z3-Tria4orq%c9e 3-18-4 2608 SRI 5.5 p96g
13 3/812005 25007877 112704 12.4-TrI4dzie 120-82-1 82608 SRI 11 pg/kg
13 3/82606 25007677 112704 1l4-Tr8nIenz1e 95-63-6 82608 SRI 11 10-kg
13 3/8/2005 25007677 112704 12-t9bra1o3Iorr6SRe 96.12-8 82805 SRI 9kg
13 380805 0007877 112704 l.2-2brunohane EDO 108-93-4 82608 SRI 5.5 pg1g
73 3/812005 5007877 112704 1.2-2chIod281e 3-50-1 82608 SRI II pgKg
13 3/62805 3007077 112704 1.2-C5chIooethie 107-58-2 82608 SRI 5.5 pg/kg
13 3/82605 5007617 112704 12-l3d46r4838800 5-87-5 82808 SRI igfkg
13 3/82005 5007677 112704 1.3.5-Trnts8enze 105-61-8 62008 SRI 11 9kg
13 3/82605 0007677 112704 1.3-2thr46enz6e 41-73-1 82608 SRI 11 ig/kg
73 3/62005 25007677 112704 1.33ChI8cps/8afle 142-28-9 82608 SRI 53 p9kg
13 3/8/2005 5007677 112704 1.4-iIothenzie 105-46-7 8260B SRI 11 9kg
13 382805 5007677 112704 1.4-DIcflIctthuan 110-56-5 82608 SRI 11 919
13 3/8/2005 25007677 112704 .2-33cIiIor9r9we 60-26-7 82608 SRI 5.5 919
13 3/8/2005 26007677 112704 -oilher 110-75-8 82808 SRI 11 p919
13 3/80805 5007677 112704 -400dUe 95-49-8 2605 081 11 pg/kg
13 3/80805 5001677 112706 -I-I4arIa6 591-78-6 82608 SRI 55 19kg
13 380805 25007677 112704 4-Cl4cnXduene 106-43-4 62608 SRI 11 ig1g
73 3/80805 25007677 112706 4-M8I96-2-p1tneMiSI 108-10-I 82608 SRI Ii pg/kg
33 38/2005 26007611 112704 Accne 7-64-1 82608 67 22 pg/kg
13 382005 25007877 112704 csdn 107-02-8 82608 SRI 110 96kg
13 3/80805 25007677 112704 /kry$oI4Irie 07-13-1 82600 SRI 110 pg/kg
13 3/8/2605 5007677 112704 S0030r16 71-43-2 82608 SRI 33 iglcg
13 3/82805 5007617 112104 SnoOeizene 108-96-1 2608 SRI 5.5 96kg
13 38/2005 5001677 112704 S6aanethrn 4-97-5 8260B SRI 5.5 96kg
13 382005 5007677 112704 Branol5chomdhana 5-27-4 8260B SRI 5.5 pg/kg
73 318/2005 5007677 112704 Sranofam 75-25-2 82608 SRI 5.5 pg/kg
13 3/812605 25007677 112704 Bcmomhane 4-83-9 62808 SRI 11 p81g
13 3/82005 5007677 112704 Crban8suI8de 75-15-0 82608 SRI 11 pg/kg
73 360805 5001877 112704 Crboitrathblde 56-23-5 82608 SRI 5.5 pglg
15 382805 5007677 112704 C34a-46ezue 105-60-7 82605 SRI 53 pg/kg
13 3592005 26007677 112704 51ao6ananeflsne 124-48-I 62608 SRI p91cg
13 3/62005 5007677 112704 Ct4aoMne 5-00-3 2808 SRI 11 pg/kg
13 380805 25007877 112704 ChIan 67-86.3 82608 SRI 5.5 pg/kg
13 3/82605 25007677 112704 3Iaun5ane 74-87-3 82608 SRI 11 p91cg
13 3/82005 25001677 112704 c4-1.2-DilthIaof1ene 155-56-4 62808 SRI 5.5 pg/kg
13 3/80805 5007677 112704 ds-1.3-Dlcl6acpccgene 10061-01-5 82608 SRI 5.5 pg/kg
73 3/80805 5007677 112704 D81cunanethe 4-95-3 82608 SRI 5.5 9kg
13 3/8/2805 26007677 112704 D4ac/88uaanh2ne 75-81-6 2608 SRI 11 pg/kg
13 3/80805 5007677 112704 0hg/bzene 100-41-4 2608 SRI 6.6 96g
13 3/62005 5007677 112704 HxacI4a46uta8en 87-64-3 2608 SRI 17 pkg
73 3/82605 26007677 112704 Is9rqM8h-lPE 105-26-3 82608 SRI 5.5 pg/kg
13 3/80805 25007677 112704 IsWrc81Iaize 6-82-8 82608 SRI 11 91cg
13 3/80805 5007677 112704 X54n.8 136777-61-2 82608 SRI 17 g6g
13 3/82805 26007677 112104 Mh4 d396 kaMB 76-93-3 82808 30 22 pg/kg
13 318/2805 5007677 112704 Me8AóJde 7488-4 82608 SRI 11 pg1g
13 3/82005 5007677 112704 M851/t-bi14 48ec MT8E 1634-04-4 82608 SRI 5.5 p919
13 380805 5007677 112704 Meth4eecI4alde 5-09-2 2608 SRI 11 0/kg
13 36/2005 25007677 112704 n-ButybzIe 04-51-5 2608 SRI 17 969
13 3/80805 5007677 112706 n-PrcpIbenzene 103-60-1 82608 SRI 11 p/kg
13 3/8/2005 5007677 112704 N9hthne 91-20-3 2608 SRI 8.6 9kg
13 3/80805 5007677 112704 X4ene 95-47-6 82608 SRI 5.5 p/kg
13 3/80805 5007877 112704 p-scrcp/kcje 66-87-6 82808 SRI 17 gkg
13 382805 25007677 112704 sec-8/Itze 135-98-8 82608 SRI 17 pg/kg
13 382005 5007677 112706 5tee 100-62-5 82600 SRI 5.5 p/kg
13 380805 26007677 112704 et-8/8j8eozene 96-08-06 2608 SRI 22 p/kg
13 3192005 26007677 112704 Ua59bee 127-18-4 8280 SRI 11 glkg
13 3592605 5007677 112704 Tie 108-88-3 2608 SRI 5.5 p91q
13 3/00805 5007677 112704 fr-1.2-DIdro8hene 156-60-5 2608 SRI 5.5 pg/kg
13 3/80805 26001677 112704 Has-l.3-33cI4apiopeno 10061-02-8 82608 SRI 5.5 pg-kg
13 3/82005 25007877 112704 Trld4aoS04n 78-01-6 82808 SRI 5.5 pp/kg
13 3/8/2805 5007677 112704 16 hlao81ggan46iane 75-64-4 82608 SRI 5.5 p919
13 3/82005 5007677 112704 4cc 73-15-0 82806 SRI 11 91/8
13 380805 25007677 112704 0n4 d4oide 5-014 82808 SRI 11 p/kg
13 3/80805 5607677 112104 C5-C8ftJiphIcs N/A MASJEPVPH SRI 8.3 96/8
13 3/82605 25007677 112104 CS-dO kana8cs N/A MADEP VPH SRI igg
13 3/8/2805 5007677 112704 3-C12ftJh46cs N/A MASDEP\/PH SRI /8/kg
nr40me 8r94 82
01 25007678 112705 l.l.1.2-1e1caoethne 30-20-6 82608 SRI
Dl 25007678 112705 l.11-Ti1chIaoflane 1-55-6 62608 SRI 52 /969
Dl 25607678 112705 1.122-TelrathIathe 9-34-5 2608 SRI 5.2 /15109
Dl 28007678 112705 l.t2-TrNas-122-Tohane 76-13-1 2608 SRI 10 pg/log
Dl 3/8/2005 25007678 112705 1.12-Tdctdooettwne 9-00-5 82608 SRI 5.2 Jg0cg
01 31812005 25007678 112705 11-l3chI8/oh8e 5-34-3 0608 SRI 5.2 Ug/lOg
Dl 3/8/2005 5007678 112705 l1-d4ovhoe 5-35-4 82608 SRI 5.2/1969
Dl 3/812005 25007678 112705 1.1-C/chlo6060e 563-58-6 2608 SRL 5.2 pgg
Dl 3/8/2005 5007678 112705 1.Z3-TrthI/8thzene 7-61-6 82608 SRI 10 i96g
Dl 3/8/2005 5007678 112705 1.23-TfloflIowq1ane 96-18-4 2608 SRI 5.2 p1g
Dl 3/8/2005 25007678 112705 124-TrIthIth60z8/e 120-82-I 0608 SRL 10 p9/og
Dl 318/2005 5007678 112705 1.Z4-Tsne89/blzene 0-63-5 82609 SRI IS igg
01 3/812005 5007678 112705 1.2-Co3-cI4cqoane 0-12-8 2608 601 5.2 ig/cg
01 3/8/2005 25507678 112705 1.2-DIbianoeIIneEDS 100-93-4 82608 881 5.2 904g
Dl 3/8/2005 25007678 112705 12-DdlIathize 5-59-1 8260B SRI 10 41g
01 05 20058 112705 1.3 S0the 107-00-2 0808 SRI 5.2/1969
Dl 3/872005 25007678 112705 1.2-UcIoroqene 8-87-5 1608 SRI 5.2 P969
Dl 3/82005 26007678 112705 1.35-Trbnell9/b8/lzene 108-67-8 2608 SRI 10 pgg
Dl 31872605 25607678 102705 1-73-1 1608 SRI 10 g81g
Dl 3/812005 26607678 112705 1.2chlcocwo 142-25-9 2606 SRI pg/log
DI 3/812005 25007678 112705 1.4-Qchlorobenzuie 106-46-7 2606 SRI 10 pglcg
01 3/8/2005 20007678 112705 14 hu05oe 110-56-5 82608 SRI 10 /1969
01 3/872005 25067678 112705 L2-Dthlscçrqomoe 590-20-7 2608 SRI 5.2 196g
01 3/8/2005 25007678 112705 -0aoc4hnib 116-75-8 52608 SRI 10 Mlg
01 /2005 25007678 112705 2-due 9-8 2008 SRI 10 pg4g
Dl 3/812005 25007678 112705 2-1108/sole 591-76-6 2608 SRI 52 g/0g
Dl 3/812005 20007678 112705 4-Oikictduene 108-43-4 82600 881 109949
Dl 3/872005 25007678 112705 4-M11h54-2-pent000leMISK 105-10-1 62806 SRI 101/8.49
01 3/8/2000 25007678 112705 10e 7-84-1 2608 78 21 g/cg
Dl 3/8/2005 25007678 112705 A0010n 107-02-8 82600 SRI 1001860
Dl 3/8/2005 25007678 112705 Aaylcnode 107-13-I 260B SRI 100 p4/09
Dl 3/8/2005 25007678 112705 8/800010 /1-43-2 2608 881 3.1 p8/kg
Dl 3/612005 25607678 112705 Ssxntholz000 08-86-I 62608 5/41 52 p96g
Dl 3/812005 5007678 112705 Si60oa4olaunhane /4-97-5 82608 SRL 5.2 gI1Og
01 3/872005 25007678 112705 8ranI5aaIiane 75-27-4 2608 SRI 5.2 p8/kg
Dl 3/6/2005 25007678 112705 Sis/8sm 5-20-2 82608 SRI pglog
Dl 318/2005 25007678 112705 Sranaflhoe 4-82-9 02608 SRI 10 pglcg
Dl 3/82005 25007676 112705 Cwbaoolso/fcle 75-15-0 2606 SRI 11 pg/log
01 3/8/2005 25067678 112705 C/8bcnte99chlo1de 8-23-5 2608 RI 5.2/19819
Dl 3/8/2005 25007678 112705 Cl4aosooe 108-90-7 2608 SRI 196g
11 31872005 25607678 112705 3/Iao/6unomdhgne 124-48-1 2608 SRI 5.29949
Dl 3/80805 25007678 112705 34ocflaoe 5-00-3 2608 SRI 10 pg0cg
Dl 3/872005 25607678 112705 Ch//8nl 67-66-3 2608 SRI 5.2 p9/og
Dl 31812005 25057678 112705 Chloanothee 4-87-3 2608 SRI IS p96
Dl 3/812005 25007678 112705 c/s-12-Clolokroetflecig 156-59-4 2600 SRI 5.2 ug/ko
Dl 31812055 28007678 112705 cIs-l.3ON/4ar60ole 10061-01-5 2608 SRI pg/log
01 3/8/2005 25007618 112705 0//ga a8gthale 74-95-3 82608 8101 5.2 J9log
Dl 3/872005 25007678 112705 Dacdfluuemhole 75-61-6 8260B SRI IS /19409
Dl 3/8/2005 25007678 112705 Bh4D/81zgoc 100-41-4 62608 SRI 6.2 j94cg
Dl 31872005 25007678 112705 HsoehlaUg/lac0eme 7-68-3 82608 881 18 oglcg
01 3/872005 25007678 112705 sqorog9/dh/81P8 108-20-3 82608 SRI 5.2 /1g/6g
Dl 3/812005 25067678 112705 sqxq9/bwzeie 98-82-8 2608 SRI 10 pgkg
Dl 3/8/2005 25607678 112705 rtp-X4enes 138777-61-2 2608 SRI 181110kg
Dl 3/8/2005 28007675 112705 MIlIcotmeMElQ 79-93-3 2508 SRI 21 p9/og
DI 3/812605 25057678 117705 Me8131 iO/6le 74-88-4 82608 SRI 10 li94cg
Dl 3/8/2005 25007678 112705 Ml-4lO/t4hMTSE 163.4-04-4 2608 SRI 5.29949
01 3/8/2005 20007878 112705 Me/hSOenoeloloeide 75-09-2 2608 SRL 10 pg/kg
01 3/8/2005 25007678 112705 n-81jlteozeoe 104-51-8 2608 SRI 16 i4cg
Dl 3/872005 25007678 112705 n-P100Slbolz080 103-65-1 2608 SRI 10 u94cg
Dl 3/5/2005 25007078 112705 Nop//lh6oe 91-20-3 2608 SRI 6.3 p9/og
Dl 3682005 25007678 112705 0-X54eI10 5-47-6 82508 54/5.21969
01 3/8/2005 25007678 112705 p-kclgopyfld000e 99-87-6 82608 SRI 16 p8/og
Dl 3/8/2005 25007678 112705 8ec-Su1taozene 135-98-S 2608 SRI 18 u0%g
01 3/8/2605 20607678 112705 SIW00e 100-42-5 2608 SRI 5.2110109
Dl 3/8/2005 25007675 112705 ot-8ut81enzene 98-06-06 2608 SRI 21 o96g
Dl 3/5/2005 25007678 112705 TOSBcSI/8OeSp4e 127-18-4 2908 SRI 10 /19/09
Dl 3182005 25007078 112705 109-3 8260B SRI 5.2 pg4g
Dl 3/82005 25067676 112705 1rol-12-0/chIoe1hene 156-60-S 2908 SRI 5.2 /1949
01 3/8/2005 26607878 112705 -13-0/d//arene 16081-02-6 2608 SRI 5.2/19/log
Dl 3/82005 25607978 112705 TrIchheie 79-01-6 2608 SRI 5.2 pg10g
Dl 3/8/2005 25007678 112705 Tr4flkrc8uorohsne 75-68-4 2608 SRI 5.2 pg/log
Dl 3/8/2005 25007678 112705-89/ace/ale 75-15-0 2608 SRI 10 J94cg
Dl 3/8/2005 25007678 112705 s9/chaiSe 75-01-4 82808 SRI 10 /09109
Dl 3/872005 25007678 112705 5-C8PI4ha5cs N/A MAI7EPVPH SRI 8.4 mg/log
Dl 3/6/2005 25007678 112705 C9-Clokacahlcs P/iA MAOEPVPH SRI mg%g
Dl 3/8/2005 28007676 112705 9-Cl2Mphe/ics N/A MADPVPH SRI 4mg/cg
Appendix
Notification ofIntent UST Fennanent Closure or Change-in-Service
UST-3 Form
tice of kitent UST Permanent Cbsure of ChangtnService
STATE USE CrY
Return completed form to
The DWM Regional Othce located in the area where the facility is located SEE MAP ON THE BACK
OF THIS FORM FOR REGIONAL
OFFICE ADDRESSES ________
IIlIAIkTCPLtLICcaL t.LEntitFpany
Street Address Facittv _fALciT.jk k1 iLt
city Cit4flode City County Zip Code
4Oj Code Phone Nrmiher Area Code Phone Nirnber
ttamejUhY Job The LLa7 Phone Number 7C -.3
vwiiiwi
Contactlocalllrernarshal Provide sketch locating piping tanks and P.E or L.G.with all dosure site
soil sampling locations assessment reports bearing the signaturePlanentireclosuree/SnL and seal of the P.E or LG If release hasSubmitclosurereportinthe format of not occurred the supervision signature orConductSiteSotAssessmentUST-12 ncludiog the form UST-2 din seal of P.E or L.G not required
thirty 30 days Following the siteIfremovingtanksorclosinginplacerefertosvestigabon Keep closure records for three yearsAPIPublication2015CleaningPelroleum
Storage Tanks and 1604 Removal and If release from the tanks has occurred the
CLsposaI of USed Urwieround ilmeum site assessment portion of the lank closure
Storage Tanks must be conducted under the supervion of
ContractorName
Address 27 dAt AM State____________ZipCodeL2-
ContactPerson5LTJ RL1 Phone No /JTJAATPhoneNO.74-8iS
1cLi..Je
iii
IeI4e1AlfIit JP4It
FOR TANKS INNC
Cu ._
provides supervision
for closure or change-in-service site assessment ad
is reouired
ties and signs and seals all closure reports
ft CcTACTPERSOfEL ____
Vi TANKS SCHEDULED FOR CLOSUREOR CHANGE-IN-SERVICE
U6T4 Rev t2Q01
uncierstarid that can be hek responsible for ennrormer1al damage reàulting irom me irnpioper ursposal army USs Read note on the back of this form
official fjtie_/A1
Sigratie Date Signe1 SCHEDULED REMOVAL DATE Nolify your DWM Regional1/_L_-Office 48 hours before this
___
Regional Oftice Yellow Copy Certral Office Pink Copy Owner
Appendix
Site Investigation Report for Permanent Closure or Change-in-Services of UST
UST-2 Form
Appendix
Certificate of UST disposal
J-.9 .--
óiypjrrimibE ITpt
--
cJe
-__--_I
wfl AitPLCE
w4-$bmlm1v
Al1J.L FICdu
1O4 --cacd4P
Ict.hwkw MSO
au
It 1_HzT ThA
03/24/05 1204 PAl 704 382 63U__CRESCENT RESOUItCES INC
ERT Pgr2012 6-03-24 i644 GUT
002
j7044WT Frrn RON SANIIN
V$-
AO1
I4 çq 7Lb
441 ziz L_441
7o4
03/23/05 1223 FAX [phone] CRESCE RESOURCES INC IO03r.
Environmental and Industrial Services
P0.$x84.HhOa333434-7750FAX[phone]
TANK DISPOSAL MANIFEST
Tank OwanrfAathananj sentaflve Nne dMgiljng ALtkessC9-cuZe ic Ski
JO LL rt 7A Ldfr AL
Tank Ow preseniadye i2aniz
iptklcorTaaks
1nk Ne thy revious CotenÆ comII.
Tank Oivnór/jkutjiorjzetj RpreeutatCertifk The uudesignI a1Ifie3thaL the abOVe 1Isa tcige
ianke IiavbeeLzeuw from die premizes thc tuIØ owmx
PrjpcdNwp Mo.uhLDayff
Transporter The undcgnd fic dint theabave listed toinge tmks havebeen nniupored to AD
Eavironmznaj ndIodiiszri Seivces 2718iJwbiriŁRiid M4I NC 272
DtpÆai Cfr1fcagloa edcthits dift the above-eainŁd swrage ranks
have bean cnLpdtpedtheinecflntŁiULy
--
Rceyling Ftethy i1JL6_4piQ..-
cSPTN4am SLgnanzr
Appendix
Copy of all laboratory analytical records and Chain-of-Custody
Case Narrative
Datec 3/17/05
Company DukeEnCorporatton Client Project 1D 05-MAR.0199
ContaCt Jay Perkins PrismCOC Group No G0305190
Address 13339 Hagers Feny Road
Huntemiiile NC 28078
The attached Lthoratory Report
containsihe analytical resulta for the prectidentilled above and indudes Quality Control Data and
Chain-of-Custody copy
DpaIIlIersamflaggedhidMduaHyon each sample KeyRenrthedataqualIfiersappeara atthebottoniofthispage
Quality conbd statements end/cr erknpte spedhic
remarks are included in the sample comments section of the
labo report for each sample affected
Please call if you have any questions relating to this analytical report
Data Rovlewed by Paula GMeland Prolect Managec MgeI Overcash
t3xIJat Signatare_____________
Review Date 317/05 Approval Date 3/17/05
Data Qualifier Key Reference
outsldeofQCLhnlta
Compound also detected in the method blank
DO Compound diluted out
Estimated concentration calibration range exceeded
.1 The analyte was positively identilled but the value is estimated belowlhe reporting limit
JH Estimated concentration with bigh bias
JL Estimated concentration with bias
Amahixeffectlspresent
Tentatively Identified compound The concentration is estimated
Note This report should not be reproduced except in its entirety without the written consent of Prism Laboratories Inc
442 Spdngbrcok Road P.O Box 240543 Charlotte NC 28224-0403
Phone [phone] Toll Free 800/529-6364 Fac 704/525-0409
Revised4I2rWO4
NC Certification No 402
SC Ceilfficatlan No 99012
NC Di9ldng WaterCert No 37735
Certification No E87519
Project ID 05-MAR-0199
Sample Matrbc Soil
Laboratory Report
3/17/05
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Duke Energy CorPoTation Client Sample ID 26007675
Attn Jay Perkins Prism Sample ID 112702
13339 Hagers Ferry Road COG Group 60305190
Huntersvflle NC 28078 Time Collected 03/08/05 1200
Time Submitted 03/08105 1555
Percent Solids fleterminion
Pelcent Soffds 83.2 31 SM2540 0310905 1450 5iten
SNnslo We Dnnation
Weight Stsulfate 5.91 5035 03109/05 000 bn
Weight l3lsulfate 8.14 5035 03109/05 000 broen
Vl9ht 5035 03/09105 000 Ibrnen
Volatile Oilc Comeounde liv GCIS
1.1.12-Tetiachioroethane SRI pg/kg 5.1 0.68 82608 03115105 37 kfl2l9Cttb 003831
111-Tridilomethane BRL isglkg 5.1 0.83 826CR 03/15/05 37 kcampigolb 003831
1j22-Te1Iomethne SRi pg/kg 5.1 0.62 82608 03/15/05 37 kcafligotb 003831
ll2-Tllthlom-1.22-Thfluoroethane SRI pg/kg 10 2.1 82608 03/15/05 37 kmpigotio 003831
112-Trichloroethane SRi pglkg 5.1 0.49 82608 0315/05 37 kniPisote 00383111eSRIpg/kg 5.1 0.98 8260B 03115105 37 kOSniPigutto 003831
11-Dlchlosoethene BRL pg/kg 5.1 0.75 8250B 03115105 37 kmPtoo 003831
11-Dichloropropene SRI pg/kg 5.1 0.87 82608 03/15/05 37 kunptgotto 003831
t23-Tdchlorcbenzene SRI pg/kg 10 3.6 82608 0315/05 37 kOaIIPi 003831
1.Z3-Trlchloropropane SRI pg/kg 5.1 0.20 82608 03/15/05 37 kc11p19090 003831
1.2.4-Tdchlorcbenzene SRI pg/kg 10 3.5 82608 03/15/05 837 luninpigOtlO 003831
124-TrImeth1benzene BRL pg/kg 10 3.7 82608 0311505 837 kcanpigulto 003831
124Ibmmo-3-thloropropane SRi pg/kg 5.1 1.4 82608 0315105 837 kcattptgotto 003831
1.2-OlbromoelhaneEDB SRI pg/kg 5.1 0.51 8260B 03/15/05 837 kcaiPiaolto 003831
12-Dtchlombenzene BRL pgikg 10 2A 82608 03115 837 kcalRlgolto 003831
12-Olduloroethane BRL pg/kg 5.1 1.2 82608 03/15/05 837 kcamplgotto 003831
12-Dlchloropropane SRI pg/kg 5.1 1.1 82608 03/15/05 837 kcwupigotto 003831
1.35-Tilmethylbenzene SRi pg/kg 10 3.8 82608 03/15105 837 kcamplgolto 003331
13-Dlchlcmbenzme 891 pg/kg 10 2.9 82608 03/15/05 837 keampigolto Q03831
L3-0thlotopropane SRI pg/kg 5.1 0.91 82808 03115/05 837 kcampiotto 003631
449 Sprtngbrook Road P.O Box 240543 Charlotte NC 29224-0543
Phone [phone] Toll Free Nwnber 1-80015294384 Fax [phone] Page of 16
fluke Energy Corporation
Attn Jay Perkins
13339 Hagem Ferry Road
Huntersville NC 28078
4Dhbwbezene
1.4-Dichiorobutane
22chiorogmpane
2-Chlooeh4 wiyl ether
2-Cldoraloluene
2-Hexanone
4hlorodue
4-Methyl-2.pentanone MEUK
Acrolein
Bne
Smmobenzene
Bromodikiomothano
BromodicNorofnethane
Samo
Bmmnethane
Oabcn disulfide
carbon teath
cNobenne
hIorodlbmmomethane
Chtoroethane
Chbrrm
Chioromethane
d84.2-Dlchlomethene
cia-I .3Dithloropropene
Dibromomethane
Dithlcndlfluorome1hane
82608
82608
82600
82608
82608
32608
82608
82608
82608
8280B
82608
82608
8260B
8260B
82608
82808
82608
82608
Laboratory Report
Client Sample 10 25007675
Prism Sample ID 112702
COC Group 30305190
lime Collected 03/08/05 1200
lime SubmItted 03/08/05 1555
03/15/06 837 leampigotto 003831
03/15/US 837 kcwnpigcao 003831
03/15/05 837 kcamplgotto QQ3331
03/15105 37 kcamplgotto Q03031
03/15/05 837 kcampgotto 003331
03/15/05 837 Iaamplgotto 003831
03/15/05 837 kcampgotto 003331
03/16/05 837 kcamplgotto 003331
03/15/05 837 taampigotto 003831
03/15/05 837 kcampgotLo 003831
03/15105 837 kcamplgdllo Q03831
03/15/05 837 kcainploUo 003331
03/15/05 837 kcanpigo4to 003331
03/15/05 931 tanplgoth 003831
03/15/05 831 kcampgolto Q0333j
03115/05837 Iampigoeo 0.03831
03115/05 837 kcampigottc 003831
03/15/05 837 kcaniplgoito 003831
449 3ngbrook Road P.0 Box 240543 Charlotte NC 28224.0543
Isil Fr.Numbor 1400/520-6364 Fax[phone]
NC Certilication No 402
Sc Certification No 99012
NC Drinking Water Cart No 37735
FL Certification No E8119
Project ID 05-MAR-0199
Sample Matrix Soil
3/17/05
Parameter Result Unitti Report MDL Dftutjon Method Analysis Analyst Batcti
LimiL Factor Date/lime ID
82608 03/15/05 837 WzTlpfgofto 003831
82608 03/15105 837 kcampigotto 003331
82808 03115/05 837 kraniptgclto 003831
82608 03/15/05 837 kcanipigslio 003831
82608 03/15105 837 kcanlptgotb 003831
SRI pg/kg
am g/kg
SRI pg/kg
SRI rig/kg
SRI pg/kg
SRI pg/kg
BRI pg/kg
BRL pg/kg
8RL jig/kg
SRI pg/kg
SRI pg/kg
SRI pg/kg
SRI pg/kg
SRI pg/kg
SRI pg/kg
SRI pg/kg
SRI pg/kg
SRI pg/kg
SRI pgg
SRi pg/kg
SRI pg/kg
BRL pg/kg
SRI pgkg
10 2.3
10 6.5
5.1 0.92
10 0.79
10 2.5
51 0.64
10 2.6
10 0.93
20 52
100 5.5
100 2.1
3.1 0.99
5.1 0.72
5.1 0.83
5.1 0.63
5.1 0.82
10 0.80
10 0.73
5.1 0.78
5.1 0.87
5.1 1.0
10 12
5.1 0.63
SRI pg/kg 10 0.50
SRI pg/kg 5.1 0.88
SRI pg/kg 5.1 1.1
SRI pg/kg 51 0.46
SRI pg/kg 10 0.64
82808 03/1545 837 kranigotto 003331
82806 03/15/05 837 aigotto 003831
82608 03/15/05 837 kcangolta 003831
82608 03115/05 837 kcarrigotto Q03831
82600 03/15/05 837 kcampigollo 003831
Page of 16
Laboratory Report
NC Drinking Water Cart No 37735 3117105
FL CediScallon No E87519
Client Sample ID 25007675
Pnsm Sample ID 112702
COC Group 60305190
Time Collected 03/08/05 1200
Time Submitted 03108/05 1555
ReSUIL trilts Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Datefflme ID
Ethylbenzene
Hexachlorobutadlene
Isopisp4 ether IPE
lsopmpyUenzane
mp-X4enes
Meth4 eth4 ketone MEK
Me9iyflodlde
Meth4 teut4 ether MTBE
Melhylene chloride
n-Bune
n-Propylbenzene
Naphthalene
o-Xylene
p4socwcpyltoluene
se9ubenzene
Sne
tert-Butlbenzene
Tetrachloruethene
Toluene
frns-1.2-Dklloroethene
trans-I 3-Dichloroptcpene
Trichioroethene
Trlchloro6uonmethaze
Anyl acetate
Vinyl chloride
BRI pglkg 61 1.9
BRL pg/kg 15 51
BRL pg/kg 5.1 0.98
BRL pg/kg 10 3.4
BRL aig/kg 15 4.2
82608 03/15/05 837 kcampigotte 003831
82508 03/15/05 837 krarnplUofte 003831
82608 03115105 837 tesnplgatin 003831
82608 03/15105837 kcampIoUo 003831
03/15/05 837 pigatto Q03831
03/15105 837 kcamplgolto 003831
03115105 837 keniipotla 003831
03/15105837 kcampiolto 003831
03/IM5 837 kimpaeo Q93831
03115/06 837 kcmipigolto 003831
03/15/05 837 kmpigotto 003531
03/15/05 837 kcamplgoito 003831
03/15105 837 kcanipigclto Q0353
03/15/05 837 kcenpigclio 003831
03115/05 837 kcam$gono
03/15/05 837 kcanpgoflo Q03831
03/15105 837 kctoipfgotto 003831
03115/05 837 kcwnplgo5o Q03831
03/15105 837 kcampgolto 003831
03115/05 837 kcarnpigotto 003531
03115/05 837 kcampio1to 003831
03/15/05 837 kcamplgotto 003831
03115/05 837 kcarnplgotb 003831
82608 03/15/05 837 kcampItto 003831
449 Spdpgbrook Road-P.O Box 240343 Chat1c1te NC 28224-0543
Phone [phone] Toll Free Number.1-80015294364 Fax [phone]
Duke Energy Corporation
A11n Jay Perkins
13339 Hagers Ferry Road
1-luntersvllle NC 28078
Pmject.1D 05-MAR-0199
Sample Matdx Soil
Parameter
82608 03/15/05 837 kcamplgolto 003831
BRL pg/kg
BR pg/kg
BR pg/kg
URL pg/kg
BR pg/kg
BRL pg/kg
BRL pg/kg
BR pg/kg
BRL pg/kg
BR pgilcg
BR pg/kg
BR pg/kg
BR pg/kg
DR pkg
BRI pg/kg
BR pg/kg
BRL pg/kg
BRL pg/kg
BR pg/kg
20 1.9
10 1.2
5.1 0.60
10 1.2
15 4.7
10 4.0
6.1 2.0
5.1 1.6
15 4.6
15 4.9
5.1 1.2
20 8.7
10 1.9
5.1 1.1
5.1 0.96
5.1 1.1
5.1 1.0
5.1 0.88
10 0.69
82608
826GB
8260B
82608
82608
82609
82609
82608
82608
82608
82608
82608
82608
82608
826GB
82606
82608
82608
82608
BR pg/kg 10 0.62
Page of 16
All results we mpcmedon dl y-weight beefs
BRL Below Repelling LImit
imatedvaIjj between the Repotng limit and the MDL
Angela Ovemash V.P Laboratory ServIces
440 Sprlngbrook Road P.0 Box 240543 Charlotte NC 282240543
Phone [phone] Toll Free Number 1-8001529-5364-Fax [phone]
NC Cedulicalion No 402
SC CerOfIcallon No 99012
NC Drinking Water Cet No 37735
FL Ceiliflcalion No E87519
Project ID
Sample MatrIx
Duke Energy Corporation
Atm Jay Perkins
13339 Hagers Ferry Road
Htmtersvifte NC 28078
Laboratory Repoit
3/17/05
05-MAR-0199
Soil
Client Sample ID
PrismSample ID
COC Group
Tune Collected
Time Submitted
25007675
112702
00305190
03/08/05 1200
03/08/05 1555
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Surrogate Recovery Control Umita
Toluene-dS 98 81-128
Dlbromolluoromethane 105 67-143
Bmmolluoroberkzene 102 77-128
Volae PcIeian Hvcfrocarbons bvGC-PIDIFID
CS-CS AIIPhaUCS BRL rnglkg 84 4.2 MADEP VPH 03/05 1241 awheeler 003658
CO-ClO Aromalics BRL mgkg 8.4 42 MADEP VPH 03109/05 1241 awheeler 003658
C9-C12 A0hatlcs BRL mglkg 8.4 4.2 MADEP VPH 03/09105 1241 whealer Q03658
Surrogate Recovery Control Umits
25-Dthroniotoluene-PID 95 70-130
25-Dllxomoteluene-FlD 106 70-130
Sanmi Walaht Determination
W6lght 2t45 MADEPVPI-I 03/14/05 000 Ibrown
Sampte Comments
Page of 16
Duke Enelpy Coporation
AIIm Jay Perkins
13339 Hagers Feny Road
Huntersvllle NC 28078
Perceid ScUds Detersucetlon
Percent Solds
Satiate Welaht Drmiallon
Weiit Bteulfate
Welt Bisulfate
Weight Methaict
Project ID 05-MAR-0199
Sample Matrhc Soil
54.7 8/42540
Laboratory Report
3117/05
Client Sample 1D 25007676
Prism Sample ID 112703
COC Group G0305190
Time Collected 03/08/05 1230
Time Submitted 03108/05 1556
03109/05 1450 lbmwn
NC Ceitlffcatton No 402
SC Certiticalion No 99012
NC Drinking Water Ceit No 37735
FL Certification No E87519
Parameter Result Units Report MDL Dilution Method AnalysIs Analyst
Batch
Limit Factor Dateflhine ID
5.69
5.61
5.25
pg/kg
pg/kg
pg/kg
p9/kg
pg/kg
p1kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
pg/kg
Volatife Orueiüc Comnoimds by GC/MS
1.1.1.2-Telraddoroethane
1.l1-Tfidmethane
112.2-Tetgaduloroethane
112-Tricbforo-1.2.2-Tjfluogoethane
tl.2-Trichtomethane
1.1-Olduloreethane
11-Diddomethene
1.1-Diddoreprepane
1.23-Tkhlorobenzene
1.2.3-Trithloropropane
1.24-Trtchlorobenzene
t24-Tdmethylbenzene
12-Dbcmo-3-chlomprnpane
12-Dthromoethane EDB
12-Dichlorobenzene
12-Olchloroethane
12-Didileropropane
135-Tdmeth8enzene
13-Dichlorebenzene
13-Dichiorepropane
BRI
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
Bitt
BRL
BRL
SRI
BRL
BRL
BRL
SRI
5035
5035
5035
82806
.82606
82608
82608
82808
82608
.82608
82608
82606
82608
82608
82608
82808
82608
82608
82608
82608
82808
82609
82608
5.2
5.2
5.2
10
5.2
5.2
52
5.2
10
5.2
10
10
5.2
5.2
10
5.2
5.2
10
10
52
03/09/05 000
03/09105 000
03/09105 000
03/15/05 922
.03/15/05 922
03/15/05 922
0315/05922
03115/05 922
03/1805 922
03115/059-22
03115106922
03/15105922
03115/05922
03/15105922
03/15/05 922
03/18/05922
03115105 922
03/15/05922
03/15/05 922
03115105922
0315105922
03115105 922
0315/05 922
0.70
0.85
0.63
2.1
0.50
10
0.77
0.89
3.6
0.27
3.5
3.7
1.5
0.52
2.5
1.2
1.1
3.8
3.5
0.92
leamplgotto 003831
003831
003831
kcacçigctto 003831
kcen1gotto Q03831
kcerçigoto 003831
keanigotio Q03821
kcumpi9olto 003831
keei 003831
kcano 003831
kcanoflo 003831
kcampigottc 003831
kcamptgotto 003831
kcanigotto 003831
kcaliptotto 003831
kcatplgctto 003831
kcarningoltc 003831
kcanplgottc 003831
kcatptgotto 003831
kCaupIoao 003831
449 Spdngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1400/5294364 Fax [phone] Page of 16
1.4-Dlthlorobizene
Z2-DlchIoroppane
2-Clilomethl vinyl ether
2-hlerotoluex.e
2-Hewnone
4-Owobluerie
4Methyl-2.pentenone MIBK
Acetene
.AcrofeIn
AadcnItnlŁ
Benzene
Bomcbenzene
Bamodommethane
Bromo9cfdorcmethare
Bromofonn
Bromoniethane
Cbcn sde
Casbon etsachloride
hlorobenzene
Oilorodibmmomethne
cNomethe
Chioromethane
ds-l2-Dichjoroethene
ds-1.3-Dfdilompropene
Dibromomethane
DidiQrodifluosomethane
BR p91kg-10 2.4
BRL pg/kg 10 6.6
BR pg/kg 5.2 0.93
SRI pgkg 10 0.81
SRI pg/kg 10 2.8
BR pg/kg 52 0.65
BR pg/kg 10 2.7
RRL pg/kg 10 094
BR pg/kg 21 5.3
BR pg/kg 100 5.6
BR pg/kg 100 2.2
BR pg/kg 3.1 1.0
BR jig/kg 5.2 0.74
BR pg/kg 5.2 0.85
BR pg/kg 5.2 0.64
BR pg/kg 5.2 0.84
BR pg/kg 10 0.82
SRI pg/kg 10 0.75
SRI pg/kg 5.2 0.80
SRI pg/kg 5.2 0.89
-BR pg/kg 5.2 1.0
BR.pg/kg 10 1.2
BR pg/kg 5.2 0.64
BR pg/kg 10 0.51
SRI pg/kg 52 0.90
SRI pg/kg 5.2 1.1
BR pg/kg 5.2 0.47
BRI-pg/kg Ia 0.65
NCCerIIhcatjon No 402
SC Cer8ftcaljcn No 99012
NC DrInking Water Cart No 37736
FL Cedification No E87519
Duke Energy Corporation Project ID 05-MAR-0199
Attn Jay Peddns Sample Matrbc Soil
13339 Hagers Feny Road
Huntaravflle NC 28018
Laboratory Report
3117/05
Client Sample ID 25007676
Prism Sample 10 112703
COC Group 60305190
Time Collected 03/0805 1230
Time Submitted 03/08/05 1555
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Uadt ractor Date/Time ID
82608 03115/05922 kcaap 003831
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
8260B
8280B
82606
82608
82608
82608
03/15/05 922 kcapigoIo 003831
03/15/05 922 kcnp1gaIb 003831
03/15/05 922 kcamplgotto 003831
03/1505 922 kcampigatb 003831
03/1505 922 keampigatto 003831
0315/05922 kcamp/golb 003831
0315/05 922 kcamptgollo 003831
0315105 922 kcampigotlo 003831
0315/06 922 kcamp5gotto Q3j
03/15105 922 kcanrpigutto Q03831
03/1506 922 kcamplgotto 003831
0311505 922 kcampigofto 003831
0315105 922 kcamplgauo 003831
03115105 922 kcampigotto Q03531
03/15/05 922 kcamplgotto 003831
O3115 922 kcamplgouo 003831
03/l8t5 922 kcamplgotto 003831
03/15105 922 kcampigatto 003531
03115106 922 kcampigoe 003831
03/15105 922 kcampi9otto 003831
03/15105 922 keamplgolto 003531
03/15/05 922 kcempigotta Q03531
03/1505 922 kmpIgatIo 003831
03/1505 922 kcamplgatto Q03831
03115105 922 kcamplgotto 003831
03/15/05 922 kcamplgolto 003831
03115/06 922 kcanpigofto 003831
Page otl6
449 Sprbrgbrook Road P.O Box 240543 Chailotte NC 28224-0543
Phanó 7041529-5364 ToIl Free Number 1-80015294354 Faic 7041525-0409
NC Certification No 402
SCCertilicatlon No 99012
NC Odnkiig Waler Cart No 37735
FL Certification No B7519
Project ID 05-MAR-0199
Sample Matrbc Soil
Ethylbenrene
HexEttiorobutadlene
lsoprcpyl ether IPE
m.p-Xylenes
Methyl ethyl ketone MEK
Methyl iodide
Methyl t-but4 ether MTBE
Methylene chiodde
n.ButyIbenzie
n-Pmpylbenzerie
Neththatene
o-Xylene
pmpyltoioane
se8ubenzene
Styrefle
tert-Butylbenzene
Tetrachioroethene
Totuane
bans-1.2-Dichloroethene
1.3-Dlthiaropropene
Trichioroethene
Trichtorofiuoromethane
Vicylacetate
V1r14 chloiide
ORL pg/kg 62 2.0
SRI pg/kg 16 5.2
SRI pg/kg 52 10
SRI pglkg 10 3.4
SRI pg/kg 16 4.3
SRI pg/kg 21 .2.0
BRL pg/kg 10 1.2
SRI p91kg 5.2 0.61
SRI pg/kg 10 1.2
SRI pg/kg 16 4.8
BRL pg/kg 10 4.0
SRI p91kg 6.2 2.1
SRI pg/kg 5.2 1.7
SRI pg/kg 16 4.7
SRI.pg/kg 16 5.0
SRI pg/kg 82 1.2
SRI pg/kg 21 5.8
SRI pg/kg 10 2.0
SRI pg/kg 5.2 1.1
SRI pg/kg 5.2 0.98
SRI pg/kg 5.2 1.1
SRI pg/kg 5.2 1.0
SRI pg/kg 5.2 0.90
SRI pg/kg 10 0.71
BRL jig/kg 10 0.63
82608
82608
82608
82608
6260B
82608
82606
82608
8260B
82608
82608
82608
82608
8260B
8260B
82608
82608
82608
82608
82608
8260B
82800
82600
82608
82608
03/15/05922 kcameotk 003831
03/15/059.22 angotto 003831
03/15/05 922 kcamplgot 003831
03/15105 922 kcemplgottc 003831
03/15/05 922 kangoifo 003831
03/15105922 kcaniç4gctto 003831
03/15105922 icaagoUo 003831
03/15105 9fl OO38Si
03/15/05 922 kcamplgotto 003831
03/15/059.22 kcanigctto 003831
0315105 922 kcampigat 003831
0315105 922 kcanpigott 003831
03/15/05 922 kcamplgo1to 003831
0315/05 922 camIgo1 003831
03/15/05 922 kcenpigolto 003331
03/15105 922 kramplgotlo 003831
03/15/05 9.22 leamplgotto 003831
03115105 922 kcampigotb Q03831
03115105 922 kcamplgotto 003331
03115105 922 laampi9olto 003831
03/1505 922 tarnplgoIto 003831
03/15105922 kcampigotto 003831
03115/05 922 teampigoito 003831
03/15105922 icapgto 003831
03115/05 922 kcarnpigotto 003831
449 SprI gbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-80015294364 Fc 704/5254409
Duke Energy Corporation
Atlu Jay Perkins
13339 Ilagers Ferry Road
Hunteceville MC 28078
Laboratory Report
3/17/05
Client Sample ID 25007676
Prism Sample ID 112703
COG Group 60305190
lime Collected 03/08105 1230
lime Submitted 03108105 1555
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Page of 16
All mautis are tepoztedcn adiyweight basis
BRI Bekw Reporting Limit
Estimated tahe between the Rxwimg LIm and the MDL
Angela Overcash VP Laboratory Sevkes
Client Sample ID
Prism Sample ID
COC Group
Thne Collected
lime Submitted
25007676
112703
G0305190
03/08/05 1230
03108/05 1555
449 Srlngbrook Road P.O Box 240545 Charlotte NC 282244543
Phofle704l529-6 Toll Free Number 1-1001529-6384 Pax 704/525-0409
NC Certification No 402
SC Certification No 99012
NC Drtnkkig Water Cod No 37735
FL Certification No E87519
Project ID 05-MAR-0199
Sample Matrbc Soil
Delce Enety Corporation
Alto Jay Peddns
13339 FIngers Feny Road
Huntamvilfe NC 28078
Laboratory Report
3/17/05
Parameter Result Units Report MDL Dilution Method Analysis Anast Batch
Umit Factor DatefTlme ID
Surrogate Recovey Control Umits
Tokiene-dS 99 81-128
Dtbromofluoromethane 106 67-143
Bromoflucrobeamne 103 77 -128
Volatile Pefroleuni Hvkocabons bvGC.PIDfl9D
C5-C8 Aliphalics BRL mg/kg 8.3 4.1 MADEP VPH 03/09/05 1941
arbeelet 003658
C9-Cl0Aromatice BRL mg/kg 83 4.1 MADEPVPH 03109105 1941 ew$ieeler 003658
C9.Cl2A3phallcs BRL mgflcg 83 4.1 MADEPVPH 03/09105 1t41 5VAeI 003658
Surrogate Recovery Control Umits
Z5-Dlbromotoluene-PID 92 70-130
DlbromotolueneflO 101 70-130
Samole Wektht Determteaflon
WeIght 21.65 MADEP VPH 03/14105 000 bIOW
Sample Comments
Page of 16
NC Certification No 402
SCCeilflIcation No 99012
NC DrInking Water Cerl No 37735
FL Certlfltlon No E87519
Duke EnergY CorpoOn Project ID 05-MAR-01 99
Attn Jay Pens Sample Matruc Sod
Percent Solids 844 Sk540 03109/05 1450 Ibrown
6035
5035
5035
03/09105000
03/09/05 000
03109105000
Vo11ls Oroanic Comeo.inds by GC/MS
1112-Tetrachloroethane
11.1-Tdchlomethane
1.12.2-Tetrachlcroethane
112-Tddoro-1.2.2-Thlluomethane
112-Triddoroethane
11methane
11-Dlchloroethene
1j-Domprepene
123-Tæchlombenzene
123-Tilthloropropene
12.4Ttichlambenzene
i24-Trknethylbenzerie
1.2-Othrcmo-3-chloroprvpane
12-Dthromodhane EDB
12-Olchlorobenzene
12-Dicldoroethane
1caloropropane
13.5-Tr9nethylbenzcne
13-Dlchlorcbenzene
13chbmpmpane
449 Spdngbrook Road P.O Box 240543 Charlotte NC 2224-0543
PhónÆ 704/529-6364 Toll Free Numben 1-8091529-6364 Fac 704/525-0409
13339 Hagers Feny Road
HtmtersviUe NC 28078
Laboratory Report
3/17/05
Client Sample 1D 25007677
Pxlsni Sample ID 112704
COG Group G0305190
lime Collected 008/05 1245
Time Submitted 03/08/05 1555
Parameter Result Units Report MDL Dilution Method Malysis Analyst Batch
Limit Factor DatefTime ID
SanDI wfaeteniation
Weltt Blaulfate 5.35 -g
Wetght Bisulfate 5.40
Weight Methanol 4.93
SRI pg/kg 5.5 0.74 82608 03/15/05 1005 knip%gotto 003831
SRI pg/kg 5.5 0.91 8260B 03/15105 1005 kcaiotto Q03831
SRI pg/kg 5.5 0.68 8260B 03/15105 1005 keamplgotto 003831
SRI pg/kg 11 2.2 82608 03/15105 1005 Iaampigotto 003331
SRI pg/kg 5.5 0.53 82608 03115105 1005 kcaTigotto 003831
BRL pg/kg 5.5 1.1 82608 03/15105 1005 kcamplgotto 003831
SRI pg/kg 5.5 0.82 82608 03/15/05 1005 kcarnplgotto 003831
BRL pglkg 5.5 0.95 82608 03115/05 1005 keampigotto 003831
SRI pg/kg 11 3.9 82608 03/15/05 1005 kcanWigotto 003831
SRI pg/kg 5.5 0.29 8260B 03/15/05 1005 kmpigotto 003831
BRI pg/kg 11 3.8 8260B 03/15105 1005 kceaigotto 003831
BRL pg/kg 11 4.0 82008 03/15/05 1005 kcampgotto 003831
SRI pg/kg 5.5 1.6 8260B 03/15/05 1005 kcanplgotto 003831
SRI pg/kg 5.5 055 82608 03/15105 1005 koaiigotto 003831
SRL pg/kg 11 21 82608 03/15/05 1005 kcainplgotto 003831
SRI.pg/kg 5.5 1.3 82609 03/15105 1005 kcanpigotto 003831
SRI pg/kg 5.5 1.2 82608 031151051005 .kcenplgotlo 003831
BRL pg/kg 11 4.1 82608 03/15/05 1005 koanpigotto Qj3831
BRL pg/kg 11 3.2 82608 0315/05 1005 kcanplgotto 003831
SRi.pg/kg 5.5 0.99 82608 03/15/05 1005 kcanpigotto 003831
Page of 16
NC Certification No 402
SC Certification No 99012
NC Diinldng Water CerL No 37735
FL Certification No 587519
449 Sprtngbrook Road P.O Box 240543 Charlotte NC 28224-0543
PhOne [phone] Toll Free Number 14001529-0384 Fax [phone]
Duke Energy CorporationMnJayPerkins
13339 HageraFerryRoad
Hunt.ersvllte NC 28078
Project ID 05-MAR-01 99
Sample Matrbc Soil
Laboratory Report
3/17/05
Client Sample 1D 25007677
Ptlsm Sample 1D 112704
COC Group 30305190
lime Collected 03/0W05 1245
lime Submltted 03/08/05 1555
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
1.4thiorob.zene SRI gig/kg 11 2.5 82606 03115/05 1005 kcmwlgOtto 003831
14-flidtorobutene SRI pg/kg 11 7.1 82608 0311510$1005 kcaiipgoIto Q03331
2ithmpropane BRL pg/kg 5.5 10 82608 03115/05 1005 ioPc 003831
2-CNoroethyldnyIeUier BRL pg/kg 11 0.86 82608 03/15105 1005 kCalflPiticUG 003831
2-Chiorotoluene RL pg/kg 11 2.8 82608 03/15/05 1005 kcamplgo5o 003521
2-Heranone SRi pg/kg 55 0.70 82608 03/15/05 1005 kcanpgotlo 003831
4-Chiorototuene SRi pg/kg 11 2.9 82608 03/15/05 1005 kCenpigc4Io 003831
P418K BRL P9/kg 11 1.0 82608 03115105 1005 kcenplgoao 003831
Acetone 67 pg/kg 22 56 82608 03/15/05 1005 kcamplgoo 003831
Acrulein BRL pg/kg 110 6.0 8260B 03115/05 1005 kaiapiMo 003831
Aayloniljlle BRI pg/kg 110 2.3 82608 03/15/05 1005 kcainpsoao 003831
Benzene BRL pg/kg 3.3 1.1 8260B 03/15105 1005 kCmlPiOOItO 003831
Bmmobenzene SRI pg/kg 5.5 0.79 82608 03/15/05.1005 cenpigotin 003531
Smmochlominethaie SRI pg/kg 5.5 0.91 82608 03/15/05 1005 kcanpigab 003831
Bromodlcliloromethane SRI ig1kg 5.5 0.69 82608 03/15/05 1005 IPigotto 003831
Bmmofonn BRI.pg/kg 5.5 0.90 8260B 03115/05 1005 kcanplgotfo 003831
Bromomethane SRI pg/kg 11 0.87 82606 03/15/05 1005 kcenplgofto 003831
Carbon cisulfide SRI pg/kg 11 0.80 8260B 03/15/05 1005 kcanplgotto Q03831
Carbon tetrachlotde SRI pg/kg 6.5 0.85 82606 03/15/05 1005 kcasnplgolto 003831
Chlorobenzene SRI pg/kg 55 0.95 82608 03/15/05 1005 camDlgotto 003831
Chlorodlbiomometiiane SRI lag/kg 5.5 1.1 82608 03/15/05 1005 kcamptgotto Q03831
Chloroethane SRI pg/kg 11 1.3 82608 03/15/05 1005 kcamplgolto 003831
Chiorofomi SRi pg/kg 5.5 0.69 82606 03/15/05 1005 kcamplgotb Q03831
Chioromethane SRI pg/kg 11 0.54 82608 03/15/05 1005 kcamIlgoIio 003831
cls-t2-Dlcbloroelhene SRI pg/kg 5.5 0.96 82608 03/15/05 1005 kcaniplgotto 003831
ds-13-Dichloroprcpene SRI pg/kg 5.5 1.2 82608 03/15105 1005 kcenplgotio 003831
Dlbmmomethane 88L pg/kg 5.5 0.50 8280B 03115/05 1005 kcamplgotto 003831
Dichkmdlfluorornethane SRI /k 11 0.70 82608 03/15/05 1005 kcamplgotto 003831
Page 10 of 16
NC Cetitlcalion No 402
SC CedlllcaUon No 99012
NC Drinking Waler Ceit No 37735
FL Certification No E87519
Laboratory Report
3/17/05
Client Sample ID 25007677
Prism Sample ID 112704
COC Group G0305190
Time Coilected 03/08/05 1246
lime Submitted 03108/0$1555
Sp1ngbroak Rood P.O Box 240543 Chertotte NC 28224-0543
Plione 7045204364 TOU Fme Number 1-80515204364- Fax [phone]
Duke Energy Corporation
Afln Jay Perkics
13339 Hagers Feny Road
Huntersvlile NC 28078
Project 1D 05-MAR-0109
Sample Matrbc Soil
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batth
Limit Factor Date/lime ID
Ett04benzene BRL pgfkg 6.6 2.1 32603 03/15105 1005 kCpgottO 003831
Heachlonbutadlane BR pglkg 17 5.5 82608 03/15/05 1005 kramplgcMto 013831
Isopropyt ether IPE BRL pg/kg 5.5 1.1 82609 03115/05 1005 kcanpIotto 013831
lsopropylbenzene BRL pg/kg 11 3.7 82608 03/15/05 1005 kcanplgotto Q03831
m.p.Xytones BRL pg/kg 17 4.5 82609 03/15/05 1005 kcamplgotto 003831
Meth$etfr1 ketonekEK 30 pg/kg 22 2.1 82608 03/15105 1005 kcanptgalta Q03831
Methyt Iodide BRL pg/kg 11 1.3 82609 03/15105 1005 kcauplgotto 003831
Methyt t-butyl ether MTBE BRL iig/kg 6.5 0.65 82606 0315/05 1005 k1WO 003831
Methylene chloride BRL pg/kg 11 1.3 82608 03/15/05 1005 kcsmpiootlo 003831
n-Butytbenzene URL pg/kg 17 5.1 82609 03115105 1005 kcmnpigottD 003831
--rrPropythenzene BR pg/kg 11 4.3 82608 03/1505 1005 kcamlgotto 003831
Naphthalene BPI pg/kg 8.6 2.2 82808 03/15105 1005 cainplfto 003831
o-Xytene BRL pg/kg 5.5 1.8 82608 031505 1005 kcanplartlo 003831
.p-lsopropyltoluene BRL pglkg 17 .5.0 82608 03/15105 1005 kfl1PigOtto 003831
sec-Butylhenzene BR pg/kg 17 5.3 82608 03/15105 1005 kmpltto 003831
Styrerie BR pg/kg 5.5 1.3 82608 03/15/051005 kCamPiOidtC 003831
tert.Butylbenzene RRL pg/kg 22 82 82608 03/15105 1005 kcamplgctto 003831
Tebachlcroelhene BR pg/kg 11 2.1 82608 0315/05 1005 kcamplgctto Q03331
Toluene BR pg/kg 55 1.2 62808 03/15 1005 kcto 003831
rans-12-Dlthlomethene BR pg/kg 5.5 1.0 82608 03115106 1005 kcan4tO 003831
bnns-1.3-Dlctdorcpropene BRL pg/kg 5.5 12 82608 03/15105 1005 kcamplgotto 003831
Tridiloroethene BR pgikg 5.5 1.1 82606 0311605 1005 kcamptgato Q03831
BR pg/kg 5.5 0.96 82608 03/15/05 1005 1cainpgotto 003831
Vinyl acetate BRL pg/kg 11 0.75 82608 03/15/05 1005 korsnplgoflo 103831
Vmyl chloride BRL pg/kg 11 0.68 82808 0315/05 1005 kcanipigotto Q03831
Pagell of 18
Affresultswe reported on thy-wei ght
basis
BRL Below Reporting Limit
Estimated value between the Reporting Limit and the MDL
Angela Overcash V.P Laboratory SeMces
449 Sprlngbrook Road P.O Box 240543 Chadotte NC 28224-0543
Phase 704/529-6364 Toll Free Number 14001529-6394 Fax [phone]
NC Certification No 402
SC Cedificalton No 99012
NC Ddnkirig Water Cot No 37735
FL Certlilcalion No E87519
Laboratory Report
3/17/05
Duke EnergY Corporation Project ID 05-MAR-0199 Client Sample ID 25007677
AtLn Jay Perkins Sample Mabtc SoIl Prism Sample ID 112704
13339 Hagers Feffy Road COC Group G0305190
Huntersville NC 28078 lime Collected 03/08/06 1245
lime Submitted 03/08/05 1555
Parameter Result lhiits Report MDL Dilution Method Analysis Analyst Batch
Umit Factor Datefllme ID
Surrogate Recovery Control Limita
Toluered8 99 81-128
Olbiumofluomrnethane 98 67-143
Dromolluombenzene 102 77-128
Volatile Petraleean Hydmcarhone bvGC-PIDIFID
C5-C8AJIphaUcs SRI mg/kg 8.3 4.1 MADEPVPH 03/10/05 1257 aetieete 003658
CO-Cia Aromafics SRI mg/kg 8.3 4.1 MADEP VPH 03/10/05 1257 aeheei 003958
C9.Cl2PJIphatlcs SRI mg/kg 8.3 4.1 MADEPVPH 03/10/05 1257 aateeler Q03658
Surrogate Recovery Control Limits
25-Dlbromotaluene-PID 85 70-130
25-Dlbmmotoluene-FID 101 70-130
Semete Walaht Determination
WeIght 19.91 MADE VPH 03/14105 000 lbemn
Sample Comments
Page 12 of 16
Laboratory Report
3/17/05
Client Sample ID 25007678
Prism Sample ID 112705
COC Group 00305190
mme Collected 03/08/05 1300
Time Submittet 03/08/05 1555
Percent Solids Determination
Percent Solids
Sannl.Weloht Deternthalion
Weight Hisulfate
Weight Bisulfate
Weight Methanol
VolalSo 0riIcCoiceounds by GC1MS
11.12-Tefraddoroethane
111-Tdchbroethane
1122-Tetrachbloathane
112-Tjichlom-12.2-Tiifluoroethane
112-Tvlchlocoethane
1Iddorcethane
11orceIhene
11-DNorcprcpene
1.2.3-Ttlddorobenzene
123-Trlctdoropropane
1Z4-Trldulombenzeae
124-Tdmethylbenzeno
1.2-DUmmo-3.ddompmpane
12-Dibromoethane EDB
1.2-Dlchlorcbenzene
12-Diclilomethane
-12-Dlthloropropane
13.5-Tdmethylbenzene
1.3-Dichlorobenzene
13-Dichlompropane
03/15/05 1049
03/15/05 1049
03/15/05 1049
03/15105 1049
03/15105 1049
03/15105 1049
03/15/05 1049
03/15/05 1049
03115/05 1049
03115/05 1049
03/15/05 1049
03/15105 1049
03/15/05 1049
03/15 1049
03/15105 1049
03/15/05 1049
03115105 1049
03/15105 1049
03/1545 1049
03/15/05 1049
aao 003831
003831
idanwo 003831
003831
0Ib 003831
kcwn 003831
003831
-003831
koanplgotto 003831
003831
003831
kcamplotto 003831
koam 003831
003831
kcampigotlo 003831
kcamptgotlo 003831
003831
kCam 003831
kcampollo 003831
koampb 003831
.449 Spdngbrook Road P.O Box 240543 Chalolte tIC 28224.0543
Pfione 100529-6364 Toll Free Numben 1400/529.6304 Fax [phone]
Duke Enemy Corporation
NC Certification No 402
SC Certificalion No 99012
NC Drinking Waler Cert No 37735
FL CerIlficalfon llo 887519
Project ID 05-MAR-0199
Sample Mabix SoilAttnJayPerkins
13339 HagersFeriy Road
Huntersvllle NC 28078
Parameter Result Urits Report MDL Dilution Method Analysis Analyst Batch
Umit Factor Date/Time ID
SM2540 03109/05 1450 Ibn
5035 03/09/05 000 Ibrown
5035 03/09105000 IbOMI
5035 03109/05 000 Ibrown
93.7
532
5.92
4.81
SRI pg/kg 5.2 0.70 82608
SRI p91kg 52 0.86 82608
SRI pg/kg 5.2 0.64 82608
SRI pg/kg 10 2.1 82608
SRi p91kg 5.2 0.50 8260B
BRL jig/kg 5.2 1.0 82608
pg/kg 5.2 0.77 82808
SRI pg/kg 5.2 0.90 82608
BRL pg/kg 10 3.7 82608
BRI pg/kg 5.2 0.27 82605
BRI pg/kg 10 3.6 82808
BRL pg/kg 10 38 82608
SRI pg/kg 5.2 1.5 82608
SRI pg/kg 5.2 0.52 82608
SRI pg/kg 10 2.5 82608
SRI pg/kg 5.2 1.3 82608
SRI pg/kg 5.2 1.1 82605
SRI pg/kg 10 3.9 82608
SRI pg/kg 10 3.0 82608
BR pg/kg 5.2 0.93 82608
Page 13of 16
NC Certlitcatign No 402
SC Certification No 99012
NC Driliking Water Cert No 37735
FL Certification No E87519
Project 1D 05-MAR-0199
Sample Matrbc Soil
Duke Energy CorporationMnJayPerkins
13339 Hagera Feny
Road
Huntersvllte NC 28078
Laboratory Report
3/17/05
Client Sample ID 25007878
Prism Sample ID 112705
COC Group G0305190
lime Collected 03108105 1300
lime Submltfed 03108105 1555
Parameter Result Units Report pi Diluion Method Analysis Analyst
Batch
Umit Factor Date/Time ID
14-OIchlc.obenzsne BRL .pglkg 10 2.4 8260B 03/15/05 1049 kCaapigoeo 003831
1.4-Dichlarobutane BRI pg/kg 10 67 82609 03/15105 1049 kcamplgotto 003831
Z2-Dchlompropane BRL pg/kg 52 0.94 82608 03/15105 1049 kcm08atto 003831
2-Chloroelhyl vhiyl ether BRL pg/kg 10 0.81 82608 03/15105 1049 kcanpigolto Q03831
2-Chlocotduene BRL pg/kg 10 2.6 82608 03/15/05 1049 kcamclgotto 003831
2-f-lexanone BIlL pg/kg 52 0.66 82809 03/15/05 1049 kiipoU.o 003831
4-Chiorotoluene SRI pg/kg 10 2.7 82606 03115/05 1048 kcamPigolto 003831
4Methy-2-pentanoneMLBK BIlL pg/kg 10 0.95 82608 03/15105 1049 kPloo4to 003831
Acetone 78 pg/kg 21 5.3 82609 03/1 5/05 1049 kcsmgolto 003831
Acrolein BIlL pg/kg 100 5.6 82609 0315105 1049 kcampigotto 003831
Acnflonibile SRI pg/kg 100 2.2 82608 03/15/05 1049 kcanlpigolk 003831
pj pg/kg 2.1 1.0 8260B 03/15105 1049 kcan1P1UOb 003831
Bromobermene pg/kg 5.2 074 82608 03/15/05 1048 kcanpi9ollo 00383195pSRipg/kg 52 0.86 82609 0315105 1049 kPiOOtio 003831
Bromodiottloromethane BIlL pg/kg 52 0.65 82609 0311505 1049 kcampl9oflO 003831
Bromoform SRI pg/kg 52 0.85 82608 03/15/05 1049 Irmniotio 003831
Bromomethane BRL pg/kg 10 0.83 82608 03/15/05 1049 kcamilootlo 003831
Carbon disulfide BIlL pg/kg 10 0.75 82608 03/15105 1049 kcamtto 003831
Carbon tetracttioiide BRL ig/kg 5.2 0.80 82609 03/16/05 1049 kcnetto 003831
Chlorobenzene BIlL pg/kg 5.2 0.90 82808 031505 1049 kcwttto 003831
ChIonxxoniomethane SRI pg/kg 5.2 1.0 82606 03115/05 1049 kcanIgotto 003831
Chloiioethane BRL pg/kg 10 1.3 82608 03/15/05 1049 kcamplootto Q03831
Chloroform BRL pg/kg 5.2 0.65 82808 03/15/05 1049 kCampi9o 003831
Chioromethane SRI pg/kg 10 0.51 8260B 03/15105 1049 keamPlootto 003831
cia-I 2-Dichlomethena pg/kg 52 0.91 82608 03/1505 1049 V9tiO 003831
ds-1.3-Dichloropmpene BRL pg/kg 5.2 1.1 8260B 03/15/05 1049 Inainvluotto 003831
Dibromomethane BIlL pg/kg 52 0.47 82806 0315/05 1049 kcaeplgotio 003831
D1thJorodiffuorjje ait pgikg 10 0.66 82608 03/15/05 1049 lrmrnfooIto 003831
440 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1400/529-6364 Fax [phone] Page 14 of 16
.449 $pctngrook Road P.O Box 240043 Charlotte NC 28224-0543
Phone [phone] loft Free Ntflnber 1-8001529-6364 Parc 7041525-0409
NC Certification No 402
SC Certification No 99012
NC Ditnldng Water CerI No.37735
FLCertlfIcatIon No E87519
Project ID
Samplo Matitc
Duke Energy Corporation
Attn Jay Petidne
13339 Hagers Feny Road
Huntersvitie NC 28078
05-MAR-0199
Soti
Laboratory Report
3117105
Client Sample ID 25007678
Prism Sample ID 112705
CCC Group G0305190
Time Collected 03108/05 1300
lime Submitted 0308/05 1555
Parameter ResUlt Units Report MDL Dilution Method AnaIyss Analyst Batch
Umit Factor Datetflme ID
Ethylbena pg/kg 6.3 2.0 8260B 03115/05 1049 003831
Hatombene 16 52 $260B 03/15105 1049 003831
lsoprcp4etherQPE SRI pg/kg 52 1.0 8260B 03/15105 1049 kmigo 003831
lsopiepylbenznee SRI pg/kg 10 3.4 82608 03/15/05 1049 U9Otb 003831
mp-Xylenes BRL pg/kg 16 4.3 82608 03/15/05 1049 ksamp9otto 003831
MethI ethd ketona MEK SRI pg/kg 21 2.0 82608 03/15105 1049 kcampigotto 003831
Meihyl iodide BRL pg/kg 10 12 8280B 03/15/05 1049 kcanIsotto 003831
Methyl t-butl ether MTBE BR jig/kg .5.2 0.62 82608 03/15105 1049 kcanclgotto 003831
Methylene chloride SRI pg/kg 10 1.3 82608 03/15105 1049 krampigotto 003831
n-Bub4benzeme 5111 pg/kg
16 4.8 8260B 03/15/05 1049 Iccanwigotto 003831
n-Pmptenzene SRt pg/kg 10 4.1 82608 03/15/05 1049 kcampigotto 003831
Naçhlhalene BR pg/kg 6.3 2.1 82608 03/15/05 1049 kCaflWlgOttO 003631
o-Xylane BR pg/kg 52 1.7 82608 03/15/05 1049 kcaircigotto 003831
p-Isopcopyltoluene BR pg/kg 16 82608 03/15/05 1049 nigotto 003831
sBubne BR pacg 18 5.0 82608 03/15/05 1049 gotto 003831
Styrene BR pg/kg 5.2 1.3 82608 0315/05 1049 kcanIgotto 003831
tert-Butylbenzene SRI pg/kg 21 5.8 82608 03/15/05 1049 kcanipotto 003831
Tetrachioroethene BRL pa 10 2.0 82608 03/15/05 1049 kcamplootto 003831
Toluene BR pgflcg 52 1.1 82608 03/15/05 1049 cnplgotto 003831
frane-12-Dichloroelhene BR pg/kg 5.2 0.98 82608 0311505 1049 kcwiigo1io 003831
trans.13-Dlchloropmpene SRI.pg/kg 5.2 1.1 8260B 03115/05 1049 kcapigotto 003831
Tiithloroethene BR pg/kg 5.2 1.0 82608 03/15/05 1049 canpigotto 003831
.1 Trichlomfluommelhane BR pg/kg 5.2 0.91 8280B 03/15105 1049 kcarigotic Q03831
Vinyl acetate BR pg/kg 10 0.71 82608 03/15/05 1049 kclootto 003831
Vinyl ridarlde BR.pg/kg.10 0.64 82608 03/15105 1049 kcaflPi9OttO 003831
Page 15 of 16
Ailesalts as ispattedon thy4ceight basis
BRL Below Reporting LImit
Esnated value between the Reporting Limit and the MDI
Angela Ovaroash VP Laboratory Services
449 Sprlngbrook Road P.O Boa 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number t-80W5294364 Faz 7041525-0409
NOCediOcation No 402
SC Cedillcalion No 99012
NC Drinking Water CerL No 37735
FLCertlflcmffon No E87519
Laboratory Report
3/17105
Duke Energy C0TP00n Project ID 05-MAR-01 99
Client Sample ID 25007678
Alto JaY Perkins Sample Matrbc Sofi Prism Sample ID 112705
13339 Hagers Feny Road COC Group G030190
Huntersvifle NC 28078 TIme Collected 03108105 1300
Time Submitted 03/08/05 1555
Parsmeter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/lime ID
The internal standard area responses for this sample were below the method control limits The
analysis was repeated with no improvement of the areas llatrix interference is suspected
Surrogate Recovery Control Limits
Toluene-d8 88 81-128
Dlbromofluommethane 128 87-143
Bromofluorobeozene 101 77-128
VoletOs Petroleum Hwtrocarbons bvGC-PIDIRD
C5-C8Aliphabcs BRI.mg/kg 84 4.2 MADEPVPH osioecs 21.26 aheeler 003658
COClO Aromatics BR mg/kg 8.4 42 MADEP WH 03109/05 2126 asheeler 053658
C9-Cl24AJiphalics BRL mg/kg 84 42 MADEPVPH 03/09/05 2128 aaieeler 003658
Surrogate Recovery Control Limits
25-Dlbjvmototuerie-PlD 87 70 -130
25-Dlbmmotoluene-FIO 101 70-130
Sarnole Wekiht Determination
WeIght 21.39 MADE VPH 03114/05 000 bonn
Sample Comments
Page 16of16
Nth Jay Perkins
13339 Hagers Ferry Road
HuntersvtUe NC 28078
NC CeilillcaUon No 402
SC CeiliScetion No.99012
NC D.91ck9 Wator Cert No 37735
FL Certification No E87519
Project 1D 05-MAR-01 99
Level II QC Report
COC Group Numbec 80305190
3/1Th5
Daternrne Submitted 3/8/05 1555
Voletfl OmComounds bvGCIMS method 8200B
1112-Tetrachloroethane ND
.1 1-Trlchloroethane ND
112.2-Telrachloroethane ND
112-Tdditoro-122-Trtfluomethane ND
1.l.2-Tdchloroelle ND
11-Deiethane ND
lj-OlrAroethene ND
11osopropene ND
1.2.3-Trlchlorobeazene ND
1Z3-TdchIorcropane PC
1.2.4-Tj1chlorcbenene PC
12.4-TIlmethlbanzeoe PC
12-Dlbromo-3-diiompropane PC
12-Dthrsmoellie0B ND
ND
ND
PC
ND
ND
U-Dkhlompropeae ND
1.4thchlomberwene ND
1ombutane PC
2.2-Oldiloropropane
2-ChIometh4 vioyl ether
2-NoroiokEene
2-Hareinone
4Harototoene
4-Meth4-2.pen1ancne MISK
Acetone
AaolelnAe
Benzane
Bmmobenzene
Bromochioromethane
Bromodichloromethane
Bromonn
Bromomethane
Carbon disultide
Carbon tetrachlodde
hiombenzene
mdibmmanethnee
cblomethane
.5 ik
2.5 pglkg
2.5 1191k0
10
2.5 1.slkg
2.5 V91k9
2.5 Re
2.5 pgflg
10 p91kg
2.5 pglkg
10 r91kg
10
2.5 pgflrg
2.5 pgæcg
10 igkg
2.5 pgikg
10 pgslcfl
10 1191kg
50 25 1101kg
10 p91kg
10 p91kg
20 10 pglkg
100 50 10
100 50 pgtcg
1.5 I199
2.5 pgdkg.5 p91kg
2.5 pglkg
2.5 pg1kg
10 p91kg
10 ig
ND 2.5 tlkg
ND .5 $Jglkg
ND .5 p91kg
ND 10 kg
003831
003831
003831
0038
003831
003831
003831
003831
003831
003831
Q038
003831
003831
003831
003831
003831
003831
003831
003831
003831
449 Spdngbrsok Road P.O Box 240543 CbarIotte NC 25254-0543
Phoner 704/5294364 Toll Fran t4wnber 14001529-6364 Fec 7041525.0409
Duke Energy Corporatbn
Method Blank
RSIII Uirdl Unks
Qc sw
ID
003931
12-Oichkircbel2one
12-Dtthlaroethane
12-Dlchtompropane
t3.5-Tdmeth1benzenelorobemene
003831
003831
003831
Q038
003831
003831
003831
003831
003831
003831
003831
003831
003331
2.5 pgi1 002831
2.5 IjeIco 003831
10 p01kg 003831
10 1o 003831
-2.5 pg1kg 003831
10 p91kg 003831
10 pglkg 003831
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page of
Duke Energy CorporationMnJayPerkins
13339 Hagers Ferry Road
Huntersdlle NC 28078
NC CerSilcalion No 402
SC Certification No 99012
NC Udnking Water Cert No 37735
FL Certification No E87519
Project ID 05.MAR-0199
Level II QC Report
3/17105
COC Group Number 00305190
DatelTime Submitted 3/8/05 1555
chiofonn
Oflommethane
ds-1.2-Dithbtetheneiompmpene
bmmometham
Dlchlorodlfluoromethejie
Ethylbenzene
Heerth1oroIutadIene
Iaoprop1 ether IPE
mpX4lenesMethethyie
MethI iodide
Methtl thut$
ether MTEE
Methylene chiodde
fl-Butylberizane
n-Pmpyibenzene
Na
o-X4ene
p-teopropyltoluene
seButylbonne
Slyrerto
tert-8uti4benzene
Tefrthloroethene
TOluena
trana-1.3-Dlchlompropene
Thdilomethene
Tilchlorofluorognelhane
acetate
/1nyl chloride
Re5 re uwa Unhli
ND 2.5 iwg
ND 10 pg5q
ND 2.5 igg
ND 2.5 pg/kg
ND 2.5 pg/kg
Nt 10 pg/kg
ND tO/kg
ND 15 7.5 19
ND 2.5 pg/kg
ND 10 pg/kg
ND 15 7.5 pg/kg
ND 20 10 pg/kg
ND 10 pg/kg
ND 2.5 pg/kg
ND 10 pg/kg
ND 15 7.5 pg/kg
ND 10 pg/kg
ND
PS 2.5 jO/kg
ND 15 7.5 pg/kg
ND 15 7.5 pg/kg
ND 2.5 pg/kg
Nt 20 10 p9/kg
ND 10 pg/kg
ND 2.5 jO/kg
ND 2.5
ND 2.5 i9
ND 2.5 19
ND 2.5 pg/kg
ND 10 pg/kg
ND 10 pg/kg
003831Q03
Q03831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003331
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
Riit M.i1t tkifts
50 pg/kg 104 57-122
50 pg/kg 106 62-119
50 pg/kg 110 61-124
50 pg/kg 109 57-122
60 pg/kg 118 59-129
ccBat ID
003831
003831
003831
003831
003831
Method Blank OCBa
Laboratoly Control Sample
11-Dichloroethene
Henzene
Chlorthenene
Toluene
Tflchloroethene
518
53.2
55.2
54.5
58.8
449 8pdawock Road P.O Box 240543 GharIotle NC 282240543
Photac 704/538-6364 Toll Free Number 14001529.0364 FeE 704/525-0409 Page of
112702 ti-Llchlomethene
Benzene
chlorobenzene
Iduene
TfldilolteUlene
NC Certification No 402
SC Certification No 98012
NC Dlnklng Water Cart No 37735
FL CertIficatiOn No E87518
449 Sprlngbrook Road P.O Box
240543 Charlotte NC 282240543
Phone [phone] TOS Free Nwnbec 1-800I529-6364 Fax [phone]
Duke Ene OSonMnJayPeddns
13339 Hagers Foxy
Road
Huntarsvtile NC 28078
Project ID 05-MAR-01 99
Level II QC Report
3117106
COC Group Numbec 00305190
Date/Time Submitted
31805 1555
Maftix Spike RsvySpRaeyRange 00
Saefl Rit jnwnl diID
112702 11-Dlchieroethene 54.1 50 i91 108 44-140 003831
Benzeae 52.1 50 vOice 104 46-136 003831
Chlodenzene 53.5 50 vOice 107 47-135 003831
Toluece 54.6 SC pgæcg 109 47-136 003831
TIchlcmethene 6t1 50 pIIcg 122 45 -141 003831
MatrtxsplkeDupftcate Rac RW
SampCe 10 jt Miecait Un Bidi
51.3 50 103 44-140 0-23 003631
50.8 50 102 46-136 0-22 003831
532 50 108 47-135 0-22 003831
52.6 50 105 47-136 0-22 003831
58.5 50 117 45-141 0-23 003831
Page of
NC Certlilcatlon No 402
SC CorUScation No 99012
NC Drinking Water CarL No 37735
FL Certification No E87519
Duke Enety Corporation Project 1D 05-MAR-0199
Atth Jay Perkins
13339 Hagers Feny Road
HunteravUle NC 28078
_________
Rzyy Range Range QcRanmMIcMdUnf$BatthID
6.59 9.23 mgIlcg 71 70-130 52 0-25 Q03658
2.97 32 nigflcg 93 70-130 0-25 003658
9.71 9.23 mgcg 105 70-130 17 0-25 Q03658
Analysis Note fix C5-C8 Aliphalics RPD ove the ooioJ limits
440 Sprlngbrook Road P.O Box 240543 Chat1ofte NC 25224-0543
Phone [phone] Toll Free Number 14001529-6364 Fwc 7041525.0409
Level QC Report
3117/05
COC Group Number 00305190
Date/Time Submittnd 318106 1555
M0th0 Utenk Ccnbel QCBelri
Pait RI eer Unite
CS-CS Afiphatics ND 3.5 mglkg 003858
CO-ClOAromatics ND 3.5 mgit 003658
C9Cl2AllphaIics ND 3.5 no 003658
Laboraimy Control Sample Rew
Spite Recay Range
Rant Mtoad
CC8frJhatics 18.2 15 nngIk 121 70-130 003658
C9-ClDAntmaIJcs 4.86 flgkg 97 70-130 003658
C9-C12 Aliphatics 15.9 15 mgflcg 108 70-130 003658
Matrix Spike Ratery
Sptee Range5antM1DRanuttAmaniS Setdi ID
112702 C5-CS-15pha6cs 11.3 9.23 mglkg 122 70-130 003658
C9-ClOMomatlcs 2.93 3.07 nflca 95 70-130 003658
C9-Cl2Ahphalkn 8.15 9.23 mglkg 88 70-130 003658
Matrix Spike Duplicate
8anWIIO
112702 C5C8Aflphalics
co-Cio Ammalics
cO-C12 AllphalIcs
Page of
Duke Power
Analytical Laboratory
ChaIn of Custody
Sample Log
LABUSEONLY
Lab lb
i2501 2i
13SampIe DescrIption or ID
SMLE PROGRAM
Ground Waler
NPDES.._
Orinkine WaterUST_RCM WaSte
ICPage_of_
DISTRIBUTION
ORIGINAL to LAB
COPY to CLIENT
CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM
Duke Power AflyticaI Laboratory Analytical Laboratory Use Only
Mail Code M003A2 Building 7405J
13339 liagers Ferry
Rd
Huntersvllle 28078
704 875-3245
1lMs JSample Ctas S.np1es NC_Ovialnaling
______________________________________________________________From
jLe2ud 011.1 Ilir/r/x
1Rroi.ct NameSWat 4f TA-K Q-LOo 3Phone No
cltefll jCT 4Fus No
5us1n1ss Unti t-uL1 13
5ProJICl IDVT0clltProc.u2jJ 7Rps Centar TO
11
lotMali Cod
Vundof
CoolAr Tm
MR
12Chem
Desktop No
iii
Customer to complete all
appropriate non-shaded areas
CoIlectIon InformatIon
rh
Date fine Stgr7r
Ii TZ I_L_
liii
Iqgtor 73
DI
/244 k4i-t/3ILL.L
J-
-H-
--
------
r.j.....1 11.4a b4..
O1t.rnrn
17
Z3Cornin.nls
peternm3//f c-o
ReIutahad
7Y
Suiiiuked Sy
/L4-
DatatTlm
Dat.RhnI/r5
%.Thm
Oat.mne
l__
Ace ted
Oat.tFtm
O.tT1m
/f
5.ock.d ey Oulagem $.alecned OaWflrne
pIe
oe
27Requested Turnaround
14 Oys ___________
Days ____________
-48 Hr _____________
Add Coal WIlt Apply
C-rOY l1D
Appendix
Photographs of closure activities
GE0SYNTEC CONSULTANTS
Photographic Record
Client Crescent Resources LLC Project Number GK3363
Site Name Elliot Street Tank Removal
March 2005
Site Location 1017 Elliot Street
Charlotte NC
Photograph
Date
March 2005
Direction
Looking South
Comments
Start of excavation
Photograph
Date
Direction
Comments
View of exposed tank
Photograh
Date
March 2005
Direction
Comments
Tank being secured for
removal
Photograph
Date
March 2005
Direction
Comments
Tank Removed
GEOSYNTEC CONSULTANTS
Photographic Record
Client Crescent Resources LLC Project Number 013363
Site Name Elliot Street Tank removal Site Location 1017 Elliot Street
Charlotte NCkC4ETh-_
-----HYH H21H
_H__
rt
Ic -ar
-.$-__-_
--r-dt_
Photograph
Date
March 2005
Direction
Comments
Excavation backfilling
Photograph
Date
March 2005
Direction
Comments
Completed backfill
GE0SYNmc CONSULTAInS
Photographic Record
Client Crescent resources LLC Project Number GK3363
Site Name Elliot Street Tank Removal Site Location 1017 Elliot Street
Charlotte NC
GEOSYNTEC CONSULTANTS
Photographic Record
Client Crescent Resources LLC ProjectNumber GK3363
Site Name Elliot Street Tank Removal Site Location 1071 Elliot Street
_________________Charlotte NC
Photograph
Date
March2005
Direction
Comments
Piping piping secondary
containment and
dispenser island
remnants
Photograph
Date
March 2005
Direction
Comments
Vacuum truck leaving
site Truck was not used
Appendix
Geologic logs for excavation
-.7
GE0SYNTEc CONSULTANTS
Soil Sample Record
Client Crescent Resources LLC Project Number GK3363
Soil Sample SS2
Date
March 2005
Site Name 1017 Elliot Street Tank removal
Soil Sample SS
Date
Site Location 1017 Elliot St
Charlotte NC
March 2005
Location Excavation
floor below tank
Soil yellowish brown
sandy loam This soil
type was consistent from
surface to pit bottom
Location Material
surrounding tank
Material consists of
gravel approximately
in size
Mr Rob Foster
Mactec
2801 Yorkmont Road
Suite 100
Charlotte NC 28208
RE Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Dear Mr Foster
Pace Analytical Services inc
9800 Kincey Avenue Suite 100
-luntersville NC 28078
Phone [phone]
Fax [phone]
Enclosed are the analytical results for samples received by the laboratory on March 17 2005 Results reported
herein conform to the most current NELAC standards where applicable unless otherwise narrated in the body of
the report
If you have any questions concerning this report please feel free to contact me
Sincerely
çiZ__Annette Scott
Annette.Scott@pacel abs corn
Project Manager
Enclosures
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
ila
Charlotte Certification lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
ce Analytical
www.pacelabs.com
March 25 2005
Th
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
ace Analytical
www.pacelabs.com Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Solid results are reported on dryeight basis
Lab Sample No 925404444 Project Sample Number 9290289-001 Date Collected 03/17105 1134
Client Sample ID P-i 1-2 Matrix Soil Date Received 03/17/05 1600
Parameters Results Units Report Limit OF Analyzed By CAS No Qual RegLjnt
Wet Chemistry
Percent Moisture Method Moisture
Percent Moisture 9.7 1.0 03/18/05 1130 INS
GC Semivolatiles
Organechiorine PCBs Prep/Method EPA 3545 EPA 8082
PCB-1016 Aroclor 1016 ND ug/kg 37 1.1 03/23/05 2236 JEM 12674-11-2
PCB-1221 Aroclor 1221 ND ug/kg 37 1.1 03/23/05 2236 JEM 11104-28-2
PCB1232 Aroclor 1232 ND ug/kg 37 1.1 03/23/05 2236 JEM 11141-16-5
PCB-1242 Aroclor 1242 ND ug/kg 37 1.1 03/23/05 2236 JEM 53469-21-9
PCB-1248 Aroclor 1248 ND ug/kg 37 1.1 03/23/05 2236 JEM 12672-29-6
PCB-1254 Aroclor 1254 ND ug/kg 37 1.1 03/23/05 2236 JEM 11097-69-1
PCB-1260 Aroclor 1260 320 ug/kg 37 1.1 03/23/05 2236 JEM 11096-82-5
Decachlorobiphenyl 70 1.0 03/23/05 2236 JEM 2051-24-3
Date Extracted 03/19/05 03/19/05
Date 03/25/05
Page of 39
REPORT OF LABORATORY ANALYSIS
Asheville Certification lOs Ihis report shall not be reproduced except in full Charlotte Certification lOsNCWastewater40without the written consent of Pace Analytical Services Inc NC Wastewater 12NCDrinkingWater37712NCDrinkingWater37706SCEnvironmental99030SC99006FLNELAPE87648ItICFLNELAPE87627
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Sample No 925404469
Client Sample ID P-22-3
Project Sample Number 9290289-002
Matrix Soil
Date Collected 03/17/05 1140
Date Received 03/17/05 1600
Parameters Results Units Report Limit DF Analyzed By CAS No lL ReLmt
Wet Chemistry
Percent Moisture Method Moisture
Percent Moisture 17.4
GC Senilvolatiles
Organochiori tie PCBs
PCB-11fl6 Aroclor 1016
PCB4221 Aroclor 1221
PCB-1232 Aroclor 1232
PCB-1242 Aroclor 1242
PCB-1248 Aroclor 1248
PCB-1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachl orobiphenyl
Date Extracted
40 L2 03/23/05
40 1.2 03/23/05
40 1.2 03/23/05
40 1.2 03/23/05
40 1.2 03/23/05
40 1.2 03/23/05
40 1.2 03/23/05
1.0 03/23/05
03/19/05
JEM 12674-11-2
JEM 11104.28-2
JEM 11141-16-5
JEM 53469-21-9
JEM 12672-29-6
JEM 11097-69-1
JEM 11096-82-5
JEM 2051-24-3
AsiwvilIe Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
gt_CCOq0tieh
Charlotte Certification lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
ce Analytical
Www.pacelabs.com
Lab Project Number 929289
Client Project ID West End 6228-05-2694
Prep/Method EPA 3545 EPA 8082
1.0 03/18/05 1130 TNS
ND uglkg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
55
03/ 19/05
Date 03/25/05
Page of 39
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
I-luntersville NC 28078
Phone [phone]
Fax [phone]
Lab Sample No 925404477
Client Sample ID P-3 1-2
Project Sample Number 9290289-003
Matrix Soil
Date Collected 03/17/05 1145
Date Received 03/17/05 1600
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
Method Moisture
18.2
Units Report Limit DF Analyzed By CAS No Dual RegLmt
1.0 03/18/05 1130 TNS
GC Semivolatiles
Organochi orine PCBs
PCB-1016 Aroclor 1016
CB-1221 Arocior 1221
PCB-1232 Aroclor 1232
PCB-1242 Aroclor 1242
PCB-1248 Aroclor 1248
PCB-1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachl orobiphenyl
Date Extracted
Asheville Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
Analytical
www.pacelabs.com
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Prep/Method EPA 3545 EPA 8082
ND ug/kg 40 1.2 03/24/05 0007 JEM 12674-11-2
ND ug/kg 40 1.2 03/24/05 0007 JEM 11104-28-2
ND ug/kg 40 1.2 03/24/05 0007 JEM 11141-16-5
ND ug/kg 40 1.2 03/24/05 0007 JEM 53469-21-9
ND ug/kg 40 1.2 03/24/05 0007 JEM 12672-29-6
ND uglkg 40 1.2 03/24/05 0007 JEll 11097-691
ND ug/kg 40 1.2 03/24/05 0007 JEll 11096-82-5
57 1.0 03/24/05 0007 JEll 2051-24-3
03/19/05 03/19/05
Date 03/25/05 Page of 39
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Lab Sample No 925404485
Client Sample ID P4 2-3
Project Sample Number 9290289-004
Matrix Soil
Date Collected 03/17/05 1150
Date Received 03/17/05 1600
Results Units Report Limit 1W Analyzed By CAS No Qual RegLmt
Method Moisture
1.0 03/18/05 1130 INS
GC Semivolatiles
Organochior-irie PCBs
PCB-J.t16 Aroclor 1016
PCB-1221 Aroclor 1221
PCB4232 Aroclor 1232
PCB-124 Aroclor 1242
PCB-1248 Aroclor 1248
PCB-1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachl orobiphenyl
Date Extracted
ND ug/kg
ND ug/kg
ND ug/kg
ND uglkg
ND ug/kg
ug/kg
ug/kg
41 1.2 03/24/05
41 1.2 03/24/05
41 1.2 03/24/05
41 1.2 03/24/05
41 1.2 03/24/05
41 1.2 03/24/05
41 1.2 03/24/05
1.0 03/24/05
03/19/05
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
thetÆ
Charlotte Certification lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
ace MaIWcaI
www.pacelabs.com
Pace Analytical Services inc
9800 Kincey Avenue Suite 100
Hunters v/lie NC 28078
Phone [phone]
Fax [phone]
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture 19.7
Prep/Method EPA 3545 EPA 8082
ND
130
52
03/19/05
0025 .JEM
0025 .EM
0025 JEM
0025 JEM
0025 JEll
0025 JEll
0025 JEll
0025 JEll
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69.1
11096-82-5
2051 -24-3
Date 03/25/05 Page of 39
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Sample No 925404493
Client Sample ID P-S 1-2
Project Sample Number 9290289-005
Matrix Soil
Date Collected 03/17/05 1150
Date Received 03117/05 1600
Parameters Results
Wet Chemistry
Units Report Limit OF Analyzed By CAS No Qual RegLmt
Percent Moisture Method Moisture
Percent Moisture 19.6
GC Semivolatiles
Organochlorine PCBs
PCB-ifJl6 Aroclor
PCB-1221 Aroclor
PCB-1232 Aroclor
PCB-1242 Aroclor
PCB-1248 Aroclor
PCB-1254 Aroclor
PCB-1260 Aroclor
Decachlorobiphenyl
Date Extracted 03/19/05
41 1.2 03/24/05 0044 JEM
41 1.2 03/24/05 0044 JEM
41 1.2 03/24/05 0044 JEM
41 1.2 03/24/05 044 JEM
41 1.2 03124/05 0044 JEM
41 1.2 03/24/05 0044 JEM
41 1.2 03/24/05 0044 JEM
1.0 03/24/05 0044 JEM
03/19/05
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
2051-24-3
Asheville Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
12
37706
99006
E87627
/2 www.pacelabs.com
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
1.0 03/18/05 1131 TNS
Prep/Method EPA 3545 EPA 8082
1016
1221
1232
1242
1248
1254
1260
120 ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
110 ug/kg
78
Date 03/25/05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Indath
Page of 39
Charlotte Certification lOs
NC Wastewater
NC Drinking Water
SC
FLNELAP
Pace Analytical Services Iiic
9800 Kincey Avenue Suite 100
Hunters vOle NC 28078
Phone [phone]
Fax [phone]
Lab Sample No 925404501
Client Sample ID P-6 2-3
Project Sample Number 9290289-006
Matrix Soil
Date Collected 03/17/05 1200
Date Received 03/17/05 1600
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
GC Sernivolatiles
Organochlorine PCBs
PCB-10f6 Aroclor 1016
PC9-1221 Aroclor 1221
PCB-1232 Aroclor 1232
PCB-1242 Aroclor 1242
PCB-1248 Aroclor 1248
PCB-1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachlorobiphenyl
Date Extracted
43 1.3 03/25/05 0317
43 1.3 03/25/05 0317
43 1.3 03/25/05 0317
43 1.3 03/25/05 0317
43 1.3 03/25/05 0317
43 1.3 03/25/05 0317
43 1.3 03/25/05 0317
1.0 03/25/05 0317
03/19/05
RPJ 12674-11-2
RPJ 11104-28-2
RPJ 11141-16-5
RPJ 53469-21-9
RPJ 12672-29-6
RPJ 11097-69-1
RPJ 11096-82-5
RPJ 2051-24-3
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
Analytical
www.pacelabs.com
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Results Units Report Limit DF Analyzed By GAS No RegLint
Method Moisture
22.4
Prep/Method EPA 3545 EPA 8082
1.0 03/18/05 1131 INS
ND
ND
ND
ND
980
ND
ND
55
03/19/05
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Page of 39
Date 03/29/05
Asheville Certilication IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSiS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
AC 0.04
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
nth
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
ce Analytical
www.pacelabs.com
Lab Sample No 925404519
Client Sample ID P-7 1-2
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]LabProjectNumber9290289
Client Project ID West End 6228-05-2694
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
Project Sample Number 9290289.007 Date Collected 03/17/05 1205
Matrix Soil Date Received 03/17/05 1600
Results Units Report Limit DF Analyzed By CAS No QL RegLmt
Method Moisture
22.6 1.0 03/18/05 1131 TNS
GC Semivolatiles
0rganoch1oine PCBs Prep/Method EPA 3545 EPA 8082
PCB-I0l.6 Aroclor 1016 ND ug/kg 43 1.3 03/24/05 0121 JEM 12674-11-2
PCB-1221 Aroclor 1221 ND ug/kg 43 1.3 03/24/05 0121 JEM 11104-28-2
PC8 1232 Aroclor 1232 ND ug/kg 43 03/24/05 01 21 JEH 11141 16
PCB-1242 Aroclor 1242 ND ug/kg 43 1.3 03/24/05 0121 JEM 53469-21-9
PCB-1248 Aroclor 1248 ND ug/kg 43 1.3 03/24/05 0121 JEM 12672-29-6
PCB-1254 Aroclor 1254 ND ug/kg 43 1.3 03124/05 0121 JEM 11097-69-1
PCB-1260 Aroclor 1260 ND ug/kg 43 1.3 03/24/05 0121 JEM 11096-82-5
Decachlorobiphenyl 60 1.0 03/24/05 0121 JEM 2051-24-3
Date Extracted 03/19/05 03/19/05
Date 03/25/OS Page of
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Lab Sample No 925404527
Client Sample ID P-8 2-3
Project Sample Number 9290289-008
Matrix Soil
Date Collected 03/17/05 1210
Date Received 03/17/05 1600
Parameters
Wet Chemistry
GC Semi vol atIl es
0rganochlrine PCBs
PC8-.i016 Aroclor 1016
PCB1221 Aroclor 1221
PCB-1232 Aroclor 1232
PCB-1242 Aroclor 1242
PCD-1248 Aroclor 1248
PCB-1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachiorobi phenyl CS
Date Extracted
Asheville Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Incsa
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
ace AnaIicaI
Www.pacelabs.com
Results
Percent Moisture
Percent Moisture
Method Moisture
7.0
Units Report Limit OF Analyzed By CAS No Qual RegLet
1.0 03/18/05 1132 INS
Prep/Method
ND
ND
ND
EPA 3545 EPA 8082
ug/kg
ug/kg
ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
69
03/19/05
35 1.1 03/24/05 0217 JEM 12674-11-2
35 1.1 03/24/05 0217 JEM 11104-28-2
35 1.1 03/24/05 0217 JEM 11141-16-5
35 1.1 03/24/05 0217 JEM 53469-21-9
35 1.1 03/24/05 0217 JEM 12672-29-6
35 1.1 03/24/05 0217 JEM 11097-69-1
35 1.1 03/24/05 0217 JEM 11096-82-5
1.0 03/24/05 0217 JEM 2051-24-3
03/19/05
Date 03/25/05 Page of 39
Pace Analytical Services Inc
9800 Kiacey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Lab Sample No 925404535
Client Sample ID P.9 1-2
Project Sample Number 9290289-009
Matrix Soil
Date Collected 03/17/05 1215
Date Received 03117/05 1600
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
GC Semivolatiles
Organochiorine PCBs
PCB-1016 Aroclor 1016
PCB-1221 Aroclor 1221
PCB-1232 Aroclor 1232
PCB-1242 Aroclor 1242
PCB-1248 Aroclor 1248
PCB-1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachlorobiphenyl
Date Extracted
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ugtkg
ND ug/kg
ND ug/kg
40
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
2051-24-3
hville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
ce Analytical
www.pacelabs.com
Results Units Report Limit DF Analyzed By CAS No RegLmt
Method Moisture
19.8
Prep/Method EPA 3545 EPA 8082
1.0 03/18/05 1132 TNS
41 1.2 03/24/05 0236 JEM
41 1.2 03/24/05 0236 JEM
41 1.2 03/24/05 0236 JEM
41 1.2 03/24/05 0236 JEM
41 1.2 03/24/05 0236 JEM
41 1.2 03/24/05 0236 JEM
41 1.2 03/24/05 0236 JEM
1.0 03/24/05 0236 JEM
03/19/0503/19/05
Date 03/25/05 Page of 39
Lab Sample No 925404543
Client Sample ID P-10 2-3
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
GC Semi volati es
Organochloriiie PCBs
PCB-1016 Aroclor 1016
PCB 1221
PCB 1232
PCB- 1242
PCB-1248
PCB-1254
PCB- 1260
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Decachl orobiphenyl
Date Extracted
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
ACCO
fnelac
tiariotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
ce Analytical
www.pacelaljs.com
Pace Analytical Sereices Inc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Project Sample Number 9290289-010 Date Collected 03/17/05 1220
Matrix Soil Date Received 03/17/05 1600
Results Units Report Limit DF Analyzed By CAS No Qual RepLmt
Method Moisture
16.7 1.0 03/18/05 1132 INS
Prep/Method EPA 3545 EPA 8082
ND ug/kg 40 1.2 03/24/05
ND ug/kg 40 1.2 03/24/05
ND ug/kg 40 1.2 03/24/05
ND uglkg 40 1.2 03/24/05
ND ug/kg 40 1.2 03/24/05
ND ug/kg 40 1.2 03/24/05
ND ug/kg 40 1.2 03/24/05
88 1.0 03/24/05
03/19/05 03/19/05
0254 JEM
0254 JEM
0254 JEM
0254 JEM
0254 JEM
0254 JEM
0254 JEM
0254 JEM
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
2051-24-3
Date 03/25/05 Page 10 of 39
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
GC Semi volat ii es
Organochior-me PCBs
PCB 1016 Aroclor 1016
PCB- 1221
PCB 1232
PCB-1242
PCB-1248
PCB- 1254
PCB-1260
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Decachl orobiphenyl
Date Extracted
39 1.2 03/24/05 0313 JEM
39 L2 03/24/05 0313 JEM
39 1.2 03/24/05 0313 JEM
39 1.2 03/24/05 0313 JEM
39 L2 03/24/05 0313 JEt-I
39 1.2 03/24/05 0313 JEM
39 1.2 03/24/05 0313 JEM
1.0 03/24/05 0313 JEM
03/19/05
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
2051-24-3
AsheviHe Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
ace AnaIicaI
www.pacelabs.com
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Lab Sample No 925404550 Project Sample Number 9290289-011 Date Collected 03/17/05 1305
Client Sample ID P-li 1-2 Matrix Soil Date Received 03/17/05 1600
Method Moisture
15.3
Results Units Report Limit OF Analyzed By CAS No Qual RegLmt
1.0 03/18/05 1133 INS
Prep/Method
ND
ND
ND
ND
ND
ND
ND
65
03/19/05
EPA 3545 EPA 8082
ugfkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Date 03125105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
meh
Page 11 of 39
Charlotte Certification lOs
NC Wastewater
NC Drinking Water
SC
FL NELAP
12
37706
99006
E87627
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
FaK 704.875.9091
Lab Sample No 925404568
Client Sample ID P-12 1-2
Project Sample Number 9290289-012
Matrix Soil
Date Collected 03/17/05 1310
Date Received 03/17/05 1600
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
Method Moisture
27.4
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certification IDs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
ce Analytical
www.pacelabs.com
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Results Units Rejort Limit DF Analyzed By CAS No Qual RegLnit
Prep/Method
ND
ND
ND
ND
ND
ND
ND
64
03/19/05
1.0 03/18/05 1217 TNS
EPA 3545 EPA 8082
ug/kg 45 1.4 03/24/05 0332 JEM
ug/kg 45 1.4 03/24/05 0332 JEM
ug/kg 45 1.4 03/24/05 0332 JEM
ug/kg 45 1.4 03/24/05 0332 JEM
ug/kg 45 1.4 03/24/05 0332 JEM
ug/kg 45 1.4 03/24/05 0332 JEM
uglkg 45 1.4 03/24/05 0332 JEll
1.0 03/24/05 0332 JEM
03/19/05
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
2051-24-3
GC Semivo1ti1es
Organochiorine PCBs
PCB-1O16 Aroclor 1016
PCB-1221 Aroclor 1221
PCB-1232 Aroclor 1232
PCB-1242 Aroclor 1242
PCB-1248 Aroclor 1248
PCB-1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachlorobiphenyl
Date Extracted
Date 03/25/OS
Page 12 of 39
Lab Sample No 925404576
Client Sample ID P.13 1-2
Parameters
Wet Chemistry
Percent Moisture
Percent Mosture
GC Semivolatiles
Organochi orine PCBs
PCB-1016 Aroclor 1016
PCB- 1221 Aroclor 1221
PC81232 Aroclor 1232
PCB-1242 Aroclor 1242
PCB-1248 Aroclor 1248
PCB-1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachlorobiphenyl
Date Extracted
Project Sample Number 9290289-013
Matrix Soil
Date Collected 03/17/05 1320
Date Received 03/17/05 1600
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
ne1a
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
ce Analytical
www4lacelabs.com
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters v/lie NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Results
Method Moisture
Units Report Limit OF Analyzed By CAS No Qual RegLmt
1.0 03/18/05 1218 TNS16.9
Prep/Method
ND
ND
ND
ND
ND
ND
ND
39
03/19/05
EPA 3645 EPA
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
8082
40
40
40
40
40
40
40
1.2 03/24/05
1.2 03/24/05
1.2 03/24/05
1.2 03/24/05
1.2 03/24/05
1.2 03/24/05
1.2 03/24/05
1.0 03/24/05
03 /19/05
0350 JEM
0350 JEll
0350 JEll
0350 JEM
0350 JEM
0350 JEM
0350 JEll
0350 JEM
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
2051-24-3
Date 03/25/05 Page 13 of 39
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
Lab Sample No 925404584
Client Sample ID P-14 2-3
Project Sample Number 9290289-014
Matrix Soil
Date Collected 03/17/05 1325
Date Received 03/17/05 1600
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
GC Sernivo1ati1es
Organochiorine PCBs
PCB or
PCB-1221 Aroclor
PCB-1232 Aroclor
PCB-1242 Aroclor
PCB-1248 Aroclor
PCB-1254 Aroclor
PCB-1260 Aroclor
Decachiorobiphenyl
Date Extracted
ND ug/kg
ND ugfkg
39 1.2 03/24/05 0409 JEll
39 1.2 03/24/05 0409 JEll
39 1.2 03/24/05 0409 JEM
39 1.2 03/24/05 0409 JEll
39 1.2 03/24/05 0409 JEM
39 1.2 03/24/05 0409 JEM
39 1.2 03/24/05 0409 JEll
1.0 03/24/05 0409 JEll
03/19/05
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
2051-24-3
MieviIle Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
\M ACC0
ne
liariotte Certification lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NE.LAP E87627
ce Analytical
www.pacelabs.com
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Method Moisture
15.7
Prep/Method EPA 3545 EPA 8082
Units Report Limit OF Anal yzed By CAS No 9L RegLmt
1.0 03/18/05 1219 INS
1016
1221
1232
1242
1248
1254
1260
ND
ND
ND
ND
ND
47
03/19/05
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Date 03/2S105 Page 14 of 39
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Date Collected 03/17/05 1330
Date Received 03/17/05 1600
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
GC Semivol..atiles
Organochiorine PCBs
PCB 1016 Aroclor 1016
PCB-1221 Aroclor 1221
PCB-1232 Aroclor 1232
PCB-1242 Aroclor 1242
PCB-1248 Aroclor 1248
PCB-1254 Aroclor 1254
PCB-126D Aroclor 1260
Decachlorobiphenyl
Date Extracted
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
ND ug/kg
ND uglkg
ND ug/kg
ND ugfkg
ND ug/kg
ND ug/kg
ND ug/kg
64
35 1.1 03/24/05 0427 JEM
35 1.1 03/24/05 0427 JEM
35 1.1 03/24/05 0427 JEM
35 1.1 03/24/05 0427 JEM
35 1.1 03/24/05 0427 JEM
35 1.1 03/24/05 0427 JEM
35 1.1 03/24/05 0427 JEM
03/19/05
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
12
37706
99006
E87627
ace AnaIicaI
www.pacelabs.com
Lab Sample No 925404592 Project Sample Number 9290289-015
Client Sample ID P-15 3-4 Matrix Soil
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Results
Method Moisture
5.0
Prep/Method EPA 3545 EPA 8082
Units Report Limit DF Analyzed By CAS No Qual RegLnit
1.0 03/18/05 1219 TNS
1.0 03/24/05 0427 JEM 2051-24-3
03/19/05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
tACco
Date 03125/05 Page 35 of 39
Charlotte Certification lDs
NC Wastewater
NC Drinking Water
SC
FL NELAP
Wet Chemistry
Percent Moisture
Percent Moisture
GC Seanvolatiles
Organochi opine PCBs
PCB40116
PCB 1221
PCB 1232
PCB-1242
PCB- 1248
PCB- 1254
PCB-1260
Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Decachi orobiphenyl
Date Extracted
Project Sample Number 9290289-016
Matrix Soil
Date Collected 03/17/05 1335
Date Received 03/17/05 1600
JEM 12674-11-2
JEM 11104-28-2
JEtI 11141-16-5
JEM 53469-21-9
JEM 12672-29-6
JEM 11097-69-1
JEM 11096-82-5
JEll 2051-24-3
Ashevifle Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Ate04nela
Charlotte Certification lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
Analytical
www.pacelabs.com
925404600
P-16 1-2
Lab Sample No
Client Sample ID
Parameters
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Results Units Report Limit OF Analyzed By CAS No QL RegLmt
Method Moisture
13.5 1.003/18/05 1219 TNS
Prep/Method EPA 3545 EPA 8082
ND ug/kg 38 L2 03/24/05 0446
ND ug/kg 38 1.2 03/24/05 0446
ND ug/kg 38 L2 03/24/05 0446
ND ug/kg 38 L2 03/24/05 0446
ND ug/kg 38 1.2 03/24/05 0446
ND ug/kg 38 1.2 03/24/05 0446
ND ug/kg 38 1.2 03/24/05 0446
48 1.0 03/24/05 0446
03/19/05 03/19/05
Date 03125/05 Page 16 of 39
Analytical
Lab Sample No
www.pacelahs.com
925404618
Client Sample ID P-17 2-3
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
I-luntersville NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Project Sample Number 9290289-017
Matrix Soil
Date Collected 03/17/05 1340
Date Received 03/17105 1600
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
CC Sennvolatiles
Organochi on ne PCBs
PCB-1016Aroclor 1016
PCB-1221 Aroclor 1221
PCB-1232 Aroclor 1232
PCB-1242 Aroclor 1242
PCB-1248 Aroclor 1248
PCB-1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachlorobiphenyl
Date Extracted
Asheville Certification iDs
NC Wastewater 40
NC Drinking Water 37712
Sc Environmental 99030
FL NELAP E87648
Method Moisture
20.1 1.0 03/18/05 1220 INS
Results Units Report Limit OF Analyzed By CAS No Qual RegLmt
PrepiMethod EPA 3545 EPA 8082
ND tag/kg 41 L2 03/24/05 0505 JEM 12674-11-2
ND ug/kg 41 1.2 03/24/05 0505 JEM 11104-28.2
ND ug/kg 41 1.2 03/24/05 0505 JEM 11141-16-5
ND ug/kg 41 1.2 03/24/05 0505 JEM 53469-21-9
ND ug/kg 41 1.2 03/24/05 0505 JEM 12672-29-6
ND ug/kg 41 1.2 03/24/05 0505 JEM 11097-69-1
ND ug/kg 41 1.2 03/24/05 0505 JEM 11096-82-5
50 1.0 03/24/05 0505 JEM 2051-24-3
03/19/05 03/19/05
Page 17 of 39
Charlotte Certification IDs
Date a3/25/os
REPORT OF LABORATORY ANALYSIS
This report shafl not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Thela
NC Wastewater
NC Drinking Water
Sc
FL NELAP
12
37706
99006
E87627
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
/-Iuntersvi/le NC 28078
Phone [phone]
Fax [phone]
Lab Sample No 925404626
Client Sample ID P-18 3-4
Project Sample Number 9290289-018
Matrix Soil
Date Collected 03/17/05 1350
Date Received 03/17/05 1600
Parameters
1et Chemistry
Percent Moisture
Percent Hoisture
GC Semivolatiles
Organochl Orine PCBs
PCB-1016 Aroclor 1016
PCB-1221 Aroclor 1221
PCB-1232 Aroclor 1232
PCB-1242 Aroclor 1242
PCB-1248 Aroclor 1248
PCB- 1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachiorobiphenyl
Date Extracted
Prep/Method EPA 3545 EPA 8082
ND ug/kg
ND ug/kg
ND ug/kg
ND uglkg
ND uglkg
ND ug/kg
ND ug/kg
58
03 /19/05
37 1.1 03/24/05 0523 JEM
37 1.1 03/24/05 0523 JEM
37 1.1 03/24/05 0523 JEM
37 1.1 03/24/05 0523 JEM
37 1.1 03/24/05 0523 JEM
37 1.1 03/24/05 0523 JEM
37 1.1 03/24/05 0523 JEM
1.0 03/24/05 0523 JEll
03/19/05
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
2051-24-3
Asheville Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
0004
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
ce Analytical
www.pacelabs.com
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
11.0
Results Units Report Limit OF Analyzed By CAS No QL RegLmt
Method Moisture
LO 03/18/05 1220 INS
Date 03/25/05 Page 18 of 39
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
ace Analytical Huntrsville NC 28078
wwW.pacelabs.com Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Lab Sample No 925404634 Project Sample Number 9290289-019
Date Collected 03/17/05 1355
Client Sample ID P.19 2-3 Matrix Soil Date Received 03/17/05 1600
Parameters Results Units Report Limit OF Analyzed By CAS No Qual RegLmt
Wet Chemistry
Percent Moisture Method Moisture
Percent Moisture 14.5 1.0 03/18/05 1220 TNS
GC Semivolatiles
Organochiorine PCBs PreplMethod EPA 3545 EPA 8082
PCB1Dt6Aroclor 1016 NO ug/kg 39 1.2 03/24/05 0542 JEM 12674-11-2
.c1221 Aroclor 1221 ND ug/kg 39 1.2 03/24/05 0542 JEM 11104-28-2
PCB-1232 Aroclor 1232 ND ug/kg 39 1.2 03/24/05 0542 JEM 11141-16-5
PCB-1242 Aroclor 1242 ND ug/kg 39 1.2 03/24/05 0542 JEM 53469-21-9
PCB-1248 Aroclor 1248 ND ug/kg 39 1.2 03/24/05 0542 JEM 12672-29-6
PCB-1254 Aroclor 1254 ND ug/kg 39 1.2 03/24/05 0542 JEM 11097-69-1
PCB-1260 Aroclor 1260 ND ug/kg 39 1.2 03/24/05 0542 JEM 11096-82-5
Decachlorobiphenyl 71 1.0 03/24/05 0542 JEM 2051-24-3
Date Extracted 03/19/05 03/19/05
Date 03/25/05 Page 19 of 39
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced except in full Charlotte Certification lOs
NC Wastewater 40 without the written consent of Pace Analytical Services Inc NC Wastewater 12
NC Drinking Water 37712 oo4 NC Drinking Water 37706
SC Environmental 99030 1-SC 99006
FL NELAP E87648 Ii JIC FL NELAP E87627
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Lab Sample No 925404642
Client Sample ID P-20 1-2
Project Sample Number 9290289-020
Matrix Soil
Date Collected 03/17/05 1400
Date Received 03/17/05 1600
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
GC Semivo1t.i les
Organochiorine PCBs
PCB-1016 Aroclor 1016
PCB-1221 Aroclor 1221
PCB-1232 Aroclor 1232
PCB-1242 Aroclor 1242
PCB-1248 Aroclor 1248
PCB-1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachlorobiphenyl CS
bate Extracted
39 1.2 03/24/05 0131
39 L2 03/24/05 0131
39 1.2 03/24/05 0131
39 1.2 03/24/05 0131
39 1.2 03/24/05 0131
39 1.2 03/24/05 0131
39 1.2 03/24/05 0131
1.0 03/24/05 0131
JEM 12674-11-2
JEM 11104-28-2
JEll 11141-16-5
JEM 53469-21-9
JEll 12672-29-6
JEM 11097-69-1
JEll 11096-82-5
JEll 2051-24-3
Asheville Certification lOs
40
37712
99030
E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certification lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
Ce Analytical
Www.pacoiabs.com Phone [phone]
Lab Project Number 9290289
Fax [phone]
Client Project ID West End 6228-05-2694
Results Units Report Limit DF Analyzed By CAS No Qual ReqLmt
Method Moisture
14.3 1.0 03/18/05 1220 TNS
Prep/Method EPA 3545 EPA 8082
ND
ND
ND
ND
ND
ND
ND
86
03/21/05
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
03 /21/05
Date 03/25/05
NC Wastewater
NC Drinking Water
SC Environmental
FL NELAP
Page 20 of a9
Lab Sample No 925404659
Client Sample ID P-21 2-3
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
GC Semi vol atil es
Organochi onne PCBs
PCB-i016 Aroclor 1016
PCB-1221 Aroclor 1221
PCB 1232 Aroclor 1232
PCB-1242 Aroclor 1242
PCB-1248 Aroclor 1248
PCB-1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachl orobi phenyl CS
Date Extracted
Project Sample Number 9290289-021
Matrix Soil
40 1.2 03/24/05 0150 .JEM
40 1.2 03/24/05 0150 JEM
40 1.2 03/24/05 0150 JEM
40 1.2 03/24/05 0150 JEM
40 1.2 03/24/05 0150 JEll
40 1.2 03/24/05 0150 JEll
40 1.2 03/24/05 0150 JEll
1.0 03/24/05 0150 JEll
03/21/05
Date Collected 03/17/05 1410
Date Received 03/17/05 1600
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
2051-24-3
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
12
37706
99006
87627
cc Analytical
www.pacelabs.com
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunlersville NC 28075
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
_______Results Units Report Limit OF Analyzed By CAS No Qual RegLmt
Method Moisture
1.0 03/18/05 1221 INS
Prep/Method EPA 3545 EPA 8082
ND uglkg
ND ug/kg
ND
ND
ND
ND
ND
51
03/21/05
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Date 03/25/OS
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced except in full
without the written consent of Pace Analytical Services Inc
nela
Page 21 of 39
Charlotte Certification IDs
NC Wastewater
NC Drinking Water
SC
FL NELAP
Analytical
www.pacelabs.com
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
I-Iuntersville NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Lab Samp4e No 925404667
Client Sample ID P-22 3-4
Project Sample Number 9290289-022
Matrix Soil
Date Collected 03/17/05 1415
Date Received 03/17/05 1600
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
GC Semivolatiles
Organochlorine PCBs
PCB-IOi6 Aroclor
PCB-1221 Aroclor
PCB-1232 Aroclor
PCB-1242 Aroclor
PCB-1248 Aroclor
PCB-1254 Aroclor
PCB-1260 Aroclor
Decachlorobi phenyl
Date Extracted
39 1.2 03/24/05 0055
39 1.2 03/24/05 0055
39 1.2 03/24/05 0055
39 1.2 03/24/05 0055
39 1.2 03/24/05 0055
39 1.2 03/24/05 0055
39 1.2 03/24/05 0055
1.0 03/24/05 0055
03/21/05
JEM 12674-11-2
JEM 11104-28-2
JEM 11141-16-5
JEM 53469-21-9
JEM 12672-29-6
JEM 11097-69-1
JEM 11096-82-5
JEM 2051-24-3
Asheville CertifLcation IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certificalion lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
16.4
Results Units Report Limit OF Analyzed By GAS No Qual RegLint
Method Moisture
1.0 03/18/05 1221 TNS
Prep/Method EPA 3545 EPA 8082
1016 ND ug/kg
1221 ND ug/kg
1232 ND ug/kg
1242 ND ug/kg
1248 ND ug/kg
1254 ND ug/kg
1260 ND ug/kg
61
03/21/05
Date 03/25/05 Page 22 of 39
Lab Sample No 925404675
Client Sample ID P-23 3-4
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
GC Semivolatiles
Organochlôrine PCBs
PCB-1016 Aroclor 1016
PCB-1221 Aroclor 1221
PCB 1232 Aroclor 1232
PCB 1242 Aroclor 1242
PCB-1248 Aroclor 1248
PCB-1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachlorobiphenyl
Date Extracted
36 1.1 03/24/05
36 1.1 03/24/05
36 1.1 03/24/05
36 1.1 03/24/05
36 1.1 03/24/05
36 1.1 03/24/05
36 1.1 03/24/05
1.0 03/24/05
03/21/05
JEM 12674-11-2
JEM 11104-28-2
JEM 11141-16-5
JEM 53469-21-9
JEM 12672-29-6
JEM 11097-69-1
JEM 11096-82-5
JEM 2051-24-3
Atheville Certification liDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certification liDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
ce Analytical
www.pacelabs.com
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Project Sample Number 9290289-023 Date Collected 03/17/05 1435
Matrix Soil Date Received 03/17/05 1600
Results Units Report Limit DF Analyzed By
CASNo Qual RegLmt
Method Moisture
8.0 1.0 03/18/05 1221 TNS
Prep/Method
ND
ND
ND
ND
ND
ND
ND
EPA 3545 EPA 8082
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
56
03/21/05
Date 03/25/05 Page 23 of 39
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
GC Sennvolatiles
Organochlorne PCBs
PCB 101 Aroclor 1016
PCB 1221 Aroclor 1221
PCB4232 AroclOr 1232
PCB-1242 Aroclor 1242
PCB-1248 Aroclor 1248
PCB-1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachiorobiphenyl
Date Extracted
Project Sample Number 9290289-024
Matrix Soil
1.3 03/25/05 0259 RPJ
1.3 03/25/05 0259 RPJ
1.3 03/25/05 0259 RPJ
1.3 03/25/05 0259 RPJ
1.3 03/25/05 0259 RPJ
1.3 03/25/05 0259 RPJ
1.3 03/25/05 0259 RPJ
1.0 03/25/05 0259 RPJ
03/24/05
Date Collected 03/17/05 1440
Date Received 03/17/05 1600
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
205 1-24-3
Asheville Certification lDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
kCCThnela
Charlotte Certification lDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
Analytical
www.pacelabs.com
Lab Sample No 925404683
Client Sample ID P-24 1-2
Pace Analylical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Results Units Report Limit DF Analyzed By CAS No Qual RegLmt
Method Moisture
21.8 1.0 03/18/05 1222 INS
Prep/Method EPA 3545 EPA 8082
ND uglkg 42
ND ug/kg 42
ND ug/kg 42
ND ug/kg 42
ND ug/kg 42
ND ug/kg 42
ND ug/kg 42
89
03/24/05
Date 03/25/05 Page 24 of 39
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End
6228-05-2694
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
Results Units Report Limit DF Analyzed By CAS No Qual RegLmt
Method Moisture
19.0 1.0 03/18/05 1222 TNS
GC Semivolatiles
Organochiorine PCBs
PCB-1Q16 Aroclor 1016
PCB-1221 Aroclor 1221
PCB-1232 Aroclor 1232
PCB-1242 Aroclor 1242
PCB-1248 Aroclor 1248
PCB-1254 Aroclor 1254
PCB-1260 Aroclor 1260
Dec achl orobi phenyl
Date Extracted 03/21/05
41 1.2 03/24/05 0226 JEM
41 1.2 03/24/05 0226 JEM
41 1.2 03/24/05 0226 JEM
41 1.2 03/24/05 0226 JEM
41 1.2 03/24/05 0226 JEM
41 1.2 03/24/05 0226 JEM
41 1.2 03/24/05 0226 JEM
1.0 03/24/05 0226 JEM
03/21/05
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
2051-24-3
Asheville Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
\$
iela
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
//Analytical
www.pacelabs.com
Lab Sample No 925404691
Client Sample ID P-25 2-3
Project Sample Number 9290289-025
Matrix Soil
Date Collected 03/17/05 1450
Date Received 03/17/05 1600
Prep/Method EPA 3545 EPA 8082
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
88
Uate O325IO5 Page 25 of 39
Pace Analytical Services Inc
9800 KinceyAveriue Suite 100
Hunters vile fl/C 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Lab Sample No 925404709
Client Sample ID P-26 2-3
Project Sample Number 9290289-026
Matrix Soil
Date Collected 03/17/05 1455
Date Received 03/17/05 1600
Parameters Results Units Report Limit OF Analyzed By CAS No QL RegLet
Wet Chemistry
Percent Moisture
GC Semivolatiles
Organochlorine PCBs
PCB1016 Aroclor 1016
PCB-1221 Aroclor 1221
PCB-1232 Aroclor 1232
PCB-1242 Aroclor 1242
PCB-1248 Aroclor 1248
PCB-1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachi orobipheriyl
Date Extracted
ND ug/kg
ND ug/kg
ND ug/kg
ug/kg
ug/kg
Asheville Certification lOs
NC Wastewater 40
NC Drinking Water 37712
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FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
iheIÆ
Charlotte Certification lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
rce Analytical
www.pacelabs.com
Percent Moisture
Method Moisture
19.3 1.0 03/18/05 1222 INS
Prep/Method EPA 3545 EPA 8082
ND ug/kg 41 1.2 03/24/05 0245 JEM 12674-11-2
ND ug/kg 41 1.2 03/24/05 0245 JEM
41 1.2 03/24/05 0245 JEM 11141-16-5
41 1.2 03/24/05 0245 JEM 53469-21-9
41 1.2 03/24/05 0245 JEM 12672-29-6
ND 41 1.2 03/24/05 0245 JEM 11097-69-1
ND 41 1.2 03/24/05 0245 JEM 11096-82-5
60 1.0 03/24/05 0245 JEM 2051-24-3
03/21/05 03/21/05
Date 03125/05 Page 26 of 39
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
GC Semivolatiles
Organochlorine PCBs
PCB 1016 Aroclor 1016
PC8-1221 Aroclor 1221
PCB 1232 Aroclor 1232
PCB-1242 Aroclor 1242
PCB-1248 Aroclor 1248
PCB-1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachi orobiphenyl CS
Date Extracted
1.2 03/25/05 0241 RPJ
1.2 03/25/05 0241 RPJ
1.2 03/25/05 0241 RPJ
1.2 03/25/05 0241 RPJ
1.2 03/25/05 0241 RPJ
1.2 03/25/05 0241 RPJ
12 03/25/05 0241 RPJ
1.0 03/25/05 0241 RPJ
03/21/05
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Date Collected 03/17/05 1505
Date Received
03/17/05 1600
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
2051-24-3
Ashevifle Certification lDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
ce Analytical
www.pacelabs.com
Lab Sample No 925404725
Client Sample ID P.27 2-3
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Project Sample Number 9290289-027
Matrix Soil
Results Units Report
Limit OF Analyzed By CAS No Qual RegLmt
Method Moisture
1.0 03/18/05 1222 TNS18.6
Prep/Method
ND
ND
ND
ND
ND
ND
ND
57
03/21/05
EPA 3545 EPA
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
8082
41
41
41
41
41
41
41
Date 03/25/05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
ACCp9
ida
Page 27 of 39
Charlotte Certification IDs
NC Wastewater
NC Drinking Water
SC
FLNELAP
12
37706
99006
E87627
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunt ers villa NC 28078
Phone [phone]
Fax [phone]
Lab Sample No 925404741
Client Sample ID P-28 3-4
Project Sample Number 9290289-028
Matrix Soil
Date Collected 03/17/05 1510
Date Received 03/17/05 1600
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
Results Units Report Limit OF Anal yzØd By CAS No Qual RegLat
Method Moisture
21.0 1.0 03/18/05 1223 TNS
GC Semi vol atil es
Organochlarine PCBs
PCB-1016 Aroclor 1016
PCB-1221 Aroclor 1221
PCB-1232 Aroclor 1232
PCB-1242 Aroclor 1242
PCB-1248 Aroclor 1248
PCB-1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachlorobiphenyl
Date Extracted
Ashevifle Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
44
42 1.3 03/24/05 0321
42 1.3 03/24/05 0321
42 1.3 03/24/05 0321
42 1.3 03/24/05 0321
42 1.3 03/24/05 0321
42 1.3 03/24/05 0321
42 1.3 03/24/05 0321
1.0 03/24/05 0321
JEll 12674-11-2
JEll 11104-28-2
JEll 11141-16-5
JEll 53469.21-9
JEM 12672-29-6
JEll 11097-69-1
JEll 11096-82-5
JEll 2051-24-3
12
37706
99006
E87627
Analytical
www.pacelabs.com
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Prep/Method EPA 3545 EPA 8082
03/21/05 03/21/05
REPORT OF LABORATORY ANALYSiS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
mea
Date 03/25/OS Page 28 of 39
Charlotte Certification lOs
NC Wastewater
NC Drinking Water
SC
FLNELAP
Lab Sample No 925404758
Client Sample ID P-29 3-4
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
GC Semivolatiles
Organochlorine PCBs
PCB-1016 Aroclor 1016
PCB-1221 Aroclor 1221
PCB-1232 Aroclor 1232
PCB-1242 Aroclor 1242
PCB-1248 Aroclor 1248
PCB1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachlorobiphenyl
Date Extracted
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 89030
FL NELAP E87648
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
ND ug/kg
41
Project Sample Number 9290289-029
Matrix Soil
40 1.2 03/24/05 0340 .JEM
40 1.2 03/24/05 0340 JEM
40 1.2 03/24/05 0340 JEM
40 1.2 03/24/05 0340 JEM
40 1.2 03/24/05 0340 JEM
40 1.2 03/24/05 0340 lEN
40 1.2 03/24/05 0340 JEM
1.0 03/24/05 0340 JEM
03/21/05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
oo
iehth
Date Collected 03/17/05 1515
Date Received 03/17/05 1600
12674-11-2
11104-28-2
11141-165
53469-21-9
12672-29-6
11097-69-1
11096-82-5
2051-24-3
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
ace AnaIicaI
www.pacelabs.com
Pace Analytical Services inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Rciil
Method Moisture
17.9
Prep/Method EPA 3545 EPA 8082
Units Report
Limit LW Analyzed By CAS No Qual ReqLmt
1.0 03/18/05 1223 INS
03/21/05
Date 03/25/05 Pa9e 29 of 39
72 Analytical
www.pacelabs.com
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Lab Sample No 925404782
Client Sample ID P-22 TANK 14-15
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
Project Sample Number 9290289-030
Matrix Soil
Date Collected 03/17/05 1425
Date Received 03/17/05 1600
GC Volatiles
GAS Soil
Gasol1
4-Brómofluorobenzene
Date 03/25/05
Method EPA 8015
ND mg/kg
88
7.0 1.2 03/18/05 2321 DHW
1.0 03/18/05 2321 DHW 460.00-4
Page 30 of 39
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
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REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
lt CCQ
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627
Results Units Report Limit DF
Method Moisture
14.9
Analyzed By CAS No Qual RegLmt
1.0 03/18/05 1223 TNS
PARAMETER FOOTNOTES
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule
NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
Dilution factor shown represents the factor applied to the reported result and reporting limit due to changes
in sample preparation dilution of the extract or moisture content
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic
testing was performed at our Pace Charlotte laboratory unless otherwise footnoted
Method 9071B modified to use ASE
All pH Free Chlorine Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate
hold time
ND Not detected at or above adjusted reporting limit
NC Not Calculable
Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
CS Surrogate
Compound concentration exceeds the calibration range of the instrument CLP E-Flag
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
Charlotte Certification ls
NC Wastewater
NC Drinking Water
SC
FLNELAP
Analytical
www.pacelabs.com
Date 03/25/OS Page 31 of 39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
i1ithà
12
37706
99006
E87627
/eAnaIYticawww.pacelabs.com
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters villa NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-D52694
Reporting
Limit Footnotes
33
LABORATORY CONTROL SAMPLE 925411860
Spike LCS LCS
Parameter Units Conc Result XRec Footnotes
PCB-1016 Aroclor 1016 ug/kg 166.70 140.8
84
PCB-1260 Aroclor 1260 ug/kg 166.70 137.0 82
Decachlorobiphenyl 78
MATRIX SPIKE MATRIX SPIKE DUPLICATE 925435158 925435166
Parameter
PCB-1016 Aroclor 1016
PCB-1260 Aroclor 1260
Decachi orobi phenyl
Asheville Certification lDs
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REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
DC Batch 123888 Analysis Method EPA 8082
DC Batch Method EPA 3545 Analysis Description Organochlorine PCBs
Associated Lab Samples 925404444 925404469 925404477 925404485 925404493
925404501 925404519 925404527 925404535 925404543
925404550 925404568
925404576 925404584 925404592
925404600 925404618
925404626 925404634
METHOD BLANK 925411852
Associated Lab Samples
Parameter
PCB-1O16 Aroclor 1016
PCB1221 Aroclor 1221
PCB-1232 Aroclor 1232
PCB.1242 Aroclor 1242
PCB.1248 Aroclor 1248
PCB.1254 Aroclor 1254
PCB-1260 Aroclor 1260
Decachlorobiphenyl CS
925404444 925404469 925404477 925404485 925404493 925404501 925404519
925404527 925404535 925404543 925404550 925404568 925404576 925404584
925404592 925404600 925404618 925404626 925404634
Units
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Blank
Result
ND
ND
ND
ND
ND
ND
ND
85
33
33
33
33
33
33
Date 03/25105
925382871 Spike MS MSD MS MSD
Units Result Conc Result Result %Rec IRec RPD Footnotes
ug/kg 214.90 184.7 200.6 86 93
ug/kg 214.90 179.4 191.2 84 89
64 85
Page 32 of 39
9800 Kincey Avenue Suite 100
Hunters vile NC 28078Analytical
Pace Aaalytica Services Inc
www.pacelabs.com QUALITY CONTROL DATA
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
SAMPLE DUPLICATE 925411878
925404444 DUP
Parameter Units Result Result RPD Footnotes
PCB-1016 Aroclor 1016 ug/kg ND ND NC
PCB-1221 Aroclor 1221 ug/kg ND ND NC
PCB-1232 Aroclor 1232 ug/kg ND ND NC
PCB-1242 Aroclor 1242 ug/kg ND ND NC
PCB-124Aroclor 1248 uglkg ND ND NC
PCB-1254 Aroclor 1254 ug/kg ND ND NC
PtB-1260 Aroclor 1260 ug/kg 320.0 250.0 27
Decachlorobiphenyl CS 70 62
Date 03/25105 Page 33 of 39
REPORT OF LABORATORY ANALYSiS
Asheville Certification lOs This report shall not be reproduced except in full Charlotte Certification lOs
NC Wastewater 40 without the written consent of Pace Analytical Services Inc NC Wastewater 12
NC Drinking Water 37712 NC Drinking Water 37706
SC Environmental 99030 SC 99006
FL NELAP E87648 FL NELAP E87627
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End 622805-2694
OC Batch 123933 Analysis Method EPA 8082
QC Batch Method EPA 3545 Analysis Description Organochlorine PCBs
Associated Lab Samples 925404642 925404659 925404667 925404675 925404683
925404691 925404709 925404725 925404741 925404758
METHOD BLANK 925413296
Associ ated Lab Samples 925404642 925404659 925404667 925404675 925404683 925404691 925404709
925404725 925404741 925404758
Blank Reporting
Parameter Units Result Limit Footnotes
PCB.1016 Aroclor 1016 ugfkg ND 33
PCB.1221 Aroclor 1221 ug/kg ND 33
PCB-1232 Aroclor 1232 ug/kg ND 33
PCB1242 Aroclor 1242 ugfkg ND 33
PCB-1248 Aroclor 1248 uglkg ND 33
PCB-1254 Aroclor 1254 ugfkg ND 33
PCB-1260 Aroclor 1260 ug/kg ND 33
Decachlorobiphenyl CS 71
LABORATORY CONTROL SAMPLE 925413304
Spike LCS LCS
Parameter Units Conc Result XR.ec Footnotes
PCB-1016 Aroclor 1016 ug/kg 166.70 147.0 88
PCB1260 Aroclor 1260 ug/kg 166.70 142.5 86
Decachlorobiphenyl 80
MATRIX SPIKE MATRIX SPIKE DUPLICATE 925435208 925435216
Asheville Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
ACCO4
Charlotte Certification lOs
NCWastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
rce Analytical
www.pacelabs.com QUALITY CONTROL DATA
Units
ug/kg
ug/kg
Parameter
PCB-1016 Aroclor 1016
PCB-1260 Aroclor 1260
Decachlorobiphenyl CS
Oate 03/25/05
925404683 Spike MS MSD MS MSD
Result Coiic Result
Result IRec tRec RPD Footnotes
213.10 170.5 185.9 80 87
213.10 155.1 176.9 73 83 13
68 76
Page 34 of 39
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
ace Analytical
QUALITY CONTROL DATA
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
SAMPLE DUPLICATE 925413312
925404667 DUP
Parameter Units Result Result RPD Footnotes
PCB-1016 Aroclor .1016 uglkg ND ND NC
PCB-1221 Aroclor 1221 uglkg ND ND NC
PCB 1232 Aroclor 1232 ug/kg ND ND NC
PCB-1242 .iwÆclor 1242 ug/kg ND ND NC
PCB-1248iwoclor 1248 ug/kg ND ND NC
PCB-1254 Aroclor 1254 uglkg ND ND NC
.PCB-1260 Aroclor 1260 ug/kg ND ND NC
Decachlorobiphenyl 61 51
Date 03125/05 Page 35 of 35
REPORT OF LABORATORY ANALYSIS
Asheville Certification lOs This report shall not be reproduced except in full Charlotte Certification Os
NC Wastewater 40 without the written consent of Pace Analytical Services Inc NC Wastewater 12
NC Drinking Water 37712 NC Drinking Water 37706
SC Environmental 99030 SC 99006
FL NELAP E87648 FL NELAP E87627
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hvntersville NC 28078
Phone [phone]
Fax [phone]
Parameter
Gasoline
4-Bromofluorobenzene
Blank Reporting
Units Result Limit Footnotes
mg/kg ND 6.0
71
LABORATORY CONTROL SAMPLE 925408528
Spike LCS LCS
Parameter Units Conc Result IRec Footnotes
Gasoline mg/kg 31.25 51.39 164
4-Bromofluorobenzene 65
MATRIX SPIKE MATRIX SPIKE DUPLICATE 925408536 925408544
925370116 Spike MS MSD MS MSD
Parameter Units Result Conc Result Result IRec IRec RPD Footnotes
Gasoline mg/kg 3.852 60.13 76.77 56.82 121 88 30
4-Bromofluorobenzene CS 82 91
SAMPLE DUPLICATE 925408551
925370124 DUP
Parameter
Gasol The
Bromofluorobenzene CS
Date 03/25/05
Units Result Result RPD Footnotes
mg/kg ND ND NC
108 102
Page 36 of 39
Asheville Certification lDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
aceAnaIicaI
wwwpacelabs corn QUALITY CONTROL DATA
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
METHOD BLANK 925408510
Associated Lab Samples
QC Batch 123849 Analysis Method EPA 8015
Batch Method EPA 8015 Analysis Description GAS Soil
Associated Lab Samples 925404782
925404782
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
tida
Charlotte Certification lDs
NC Wastewater
NC Drinking Water
SC
FL NELAP
12
37706
99006
E87627
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
QC Batch 123831 Analysis Method Moisture
QC Batch Method Analysis Description Percent Moisture
Associ ated Lab Samples 925404444 925404469 925404477 925404485 925404493
925404501 925404519 925404527 925404535 925404543
925404550
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
ELNELAP E87648
Charlotte Certification lDs
NC Wastewater 12
NC Drinking Water 37706
99006
E87627
ace Ana1icaI
www.pacelabs.com QUALITY CONTROL DATA
SAMPLE DUPLICATE 925407199
Parameter
925403289 DUP
Units Result Result RPD Footnotes
Percent Moisture 8.600 8.800
Date 03/25/05 Page 37 of 39
REPORT OF LABORATORY ANALYSIS
Asheville Certification lDs This report shall not be reproduced except in full _____________________
without the written consent of Pace Analytical Services Inc
SC
FL NELAP
Analytical
www.pacelabs.com
925407389
Pace Analytical Services Inc
.9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NEI..AP E87627
QUALITY CONTROL DATA
Lab Project Number 9290289
Client Project ID West End 622805-2694
QC Batch 123839 Analysis Method Moisture
QC Batch Method Analysis Description Percent Moisture
Associated Lab Samp1es 925404568 925404576 925404584 925404592 925404600
925404618 925404626 925404634
925404642 925404659
925404667 925404675 925404683 925404691 925404709
925404725 925404741 925404758 925404782
925404568 DUP
Units Result Result RPD Footnotes
27.40 25.90
SAMPLE DUPLICATE
Parameter
Percent Moisture
Date 0312S/05
Asheville Certification lDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Page 38 of 39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
LtcneIÆ
Passe Analylical Services Inc
9800 Kincey Avenue Suite 100
ace Analytical Hu 28
www.pacelabs.com Fax [phone]
Lab Project Number 9290289
Client Project ID West End 6228-05-2694
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Consistent with EPA guidelines unrounded concentrations are displayed and have been used to calculate Rec and RPD values
LCSD LaboratoryControl Sample Duplicate
MSD Matrix Spike Duplicate
DUP Saniple.Duplicate
ND Not detected at or above adjusted reporting limit
NC Not Calculable
Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
RPD Relative Percent Difference
Surrogate
Date 03125/05 Page 39 of 39
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced except in full Charlotte Certification lOs
NC Wastewater 40 without the written consent of Pace Analytical Services Inc NC Wastewater 12NCDrinkingWater37712NCDrinkingWater37706SCEnvironmental99030SC99006
FL NELAP E87648 fl ac FL NELAP E87627
PaceAna/yticaI
wwWpaeelabs.cem
Required Client Information
Section
Company A14 rc-c
Report TOrç of
%.1sI L1 IlaayLflaI IJIJ.UuIeIJL
The Chain-of-Custody is LEGAL DOCUMENT All relevant fields must be completed accurately
Required Qltent Information Section
Copy To Quote Reference
Client Information Check quote/contract
To Be Completed by Pace Analytical and Client Section
Addrees Zr3C 7o /tyQ/trivoicejo//rc
P.O
tequested Due Date TAT
Turn atound time less than 14 days subject to
laboratory and contractual oblrgations and may result ins
Flush Turnaround Surcharge
TurtaAround Time TAT in calendar days
Project Manager
Project
Profile
Requested
Anatjtsts
X/
RernarhslLablD
.1 A/Project Nameie7
Phone Fatr Project Numb9t7/j3 76
Section RequIred Client information Matrle Codes
SAMPLE ID
PRODUCT
Onecharacterperbox
Sample IDs MUST BE UNIQUE OTHER OT
COLLSCTEO
START
Preservatives
OATS rCME OATS TiME
L_i__IiiII_IIIII
i3.So
//io
3--.---m7rIululicziIi
NC Sc GA NPDES GFtsUD WATER DRINKING WATER
Other UST RCRA Other
211tLL
7_f hH-
11 5/$J5
SAMPLE CONDITION SAMPLE NOTES
Temp In
Received on lcelYN
Sealed Cooler
Samples Intact IJJ
Additional Comments
PRINT Name at SAMPLER
SIGNATURE of SAMPLER DATE SIgned MM DO YY
SEE REVERSE SlD FOR INSTRUCTIONS Form COCO1 Rev 0104
//FaceAnalyticalm
www.pacelabni
Required Client Information Sjion
TempiriC
Received on Ice
Sealed Cooler YNi
Samples Intact
Company ft Copy To
MrIalyuIa1 rlequesL
uoIumIL
The Chain-of-Custody Is LEGAL DOCUMENT All relevant fields must be completed accurately
Required Client Information
SectionRepo Ipage of$
Quote Reference
Client Information iCteck quote/contract
To Be Completed by Pace Analytical and Client Section
AddressZô YrI/1cJr Invoice To r-Requested Due Date TAT5rt4jP Project Manager
L/.1
pQ Tum around time iess than 14 days subject
to
laboratory and contractual obligations and may resuit ri
Rush Turnaround Surcharge
Turn Around lime TAT in calendar days
Project
J/i.a rr S.O
Phone
Project Name tJ
ProjectNuniber
Profile
Requested ////////////////
/c///
Remarks/Lab ID
iiL
Section Required Client Information MCO
SURFACE WATER SW
One character per box SO
START
COLLECTED
END
Sample lDs MUST BE UNIQUE istq DATE TIME DATE TIME
P-7 z------------io/5
.e ILI1I I25
.0
ii
Cu
liii
iii
2NC Sc GA NPDES GROUND WATER DRINKING WATER
Other UST RCRA Other F-
HEEiI
y/4 I7
SAMPLE CONDITION SAMPLE NOTES
Addltlonel Comments
PRINT Name ot SAMPLEi-r
SiGNATURE ol SAMPLER DATE Signed MM DD Vi
SEE REVERSE SIDE FOR INSTRUCTIONS Eorrn coCol Rev 0304
Lab Sample No 925409575
Client Sample ID P-41
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
GC Semi vol ati es
TPH in Soi lby 3545/8015
Diesel Fuel
nPentacosane
Date Extracted
Method Moisture
15.9
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Project Sample Number 9290353-004
Matrix Soil
Prep/Method EPA 3545 EPA 8015
ND mg/kg
86
03/21/05
5.9 1.2 03/24/05 0503 KBS
1.0 03/24/05 0503 KBS
03/21/05
GC Volatiles
GAS Soil North Carolina
Gasoline
4-Bromofluorobenzene CS
Date 03/29/OS
Method EPA 8015
ND mg/kg
76
4.6 0.9 03/21/05 1706 DHW
1.0 03/21/05 1706 DHW 460-00-4
Page 16 of 79
Ashevifle Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certification lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
ace Analytical
www.pacelabs.com
Pace Analytical Services inc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Results Units Report Limit OF Anlv7M
1.0 03/21/05 0831 TNS
Date Collected 03/18/05 1410
Date Received 03/18/05 1525
CAS No Dual RegLet
68334-30-5
629-99-2
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
fax [phone]
Lab Sample No 925409583
Client Sample ID P-42
Project Sample Number 9290353-005
Matrix Soil
Date Collected 03/18/05 1430
Date Received 03/18/05 1525
GC Volatiles
GAS Soil North Carolina
Gasoline
-Bromofi uorobenzene
Results
Method Moisture
7.5 .%
Prep/Method EPA 3545 EPA 8015
ND mg/kg 5.4
113
03/21/05
Method
ND
97
0601 KBS 68334-30-5
0601 KBS 629-99-2
3.7 0.7 03/21/05 1808 DHW
1.0 03/21/05 1808 DHW 460-004
Asheville Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E8764
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
heIa
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
ace AnaIicaI
www.pacelabs.com
Par amtrs
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Wet Chemistry
Percent Moisture
Percent Moisture
GC Semivolatiles
IPH in Soil by 3545/8015
Diesel Fuel
nPentacosane
Date Extracted
EPA 8015
mg/kg
Units Report Limit OF Analyzed By CAS No Dual RegLet
1.0 03/21/05 0832 TNS
1.1 03/24/05
1.0 03/24/05
03/21/05
Page 17 of 79Date03/29/05
ace Analytical
www.pacelabs.com
Lab Sample No 925409591
Client Sample ID P-34
Wet Chemistry
Percent Moisture
Percent Moisture
GC Semi vol t1es
TPH in Soil by 3545/8015
Diese1Fiel
p-Pentacosane
Date Extracted
GC Volatilºs
GAS Soil North Carolina
Gasoline
4-Broniofl uorobenzene
Method Moisture
10.7
Prep/Method
ND
108
03/21/05
ND mg/kg
93
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vu/c NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
1.1 03/24/05 0035 KBS 68334-30-5
1.0 03/24/05 0035 KBS 629-99-2
03/21/05
4.0 0.8 03/21/05 1838 DHW
1.0 03/21/05 1838 DHW 460-00-4
Asheville Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
ne1a
Charlotte Certification lDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
IThsiil ts
EPA 3545 EPA 8015
mg/kg 5.6
Method EPA 8015
Project Sample Number 9290353-006 Date Collected 03/18/05 1300
Matrix Soil Date Received 03/18/05 1525
Units Report Limit OF Analyzed By CAS No Dual RegLmt
1.0 03/21/05 0832 TNS
Page 18 of 79Date03/29/95
Analytical
www.pacelabs.com
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vu/c NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Lab Sample No 925409609
Client Sample ID P-38
Project Sample Number 9290353-007
Matrix Soil
Date Collected 03/18/05 1250
Date Received 03/18/05 1525
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
Method Moisture
10.3
GC Semivolatiles
TPH in Soil oy 3545/8015
Diesei Fuel
p-Pentacosane
Date Extracted
Prep/Method EPA 3545 EPA 8015
ND mg/kg
89
03 /21/05
5.6 1.1 03/24/05 0105 KBS 68334-30-5
1.0 03/24/05 0105 KBS 629-99-2
03/21/05
GC Volatiles
GAS Soil North Carolina
Gasoline
4-Bromofl uorobenzene
Date 03/29/05
Method EPA 8015
ND mg/kg
91
4.9 tO 03/21/05 1940 DHW
1.0 03/21/05 1940 DHW 460-00-4
Page 19 of 79
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
Results Units Report Limit OF Analyzed By CAS No .Oual RegLmt
1.0 03/21/05 0832 TNS
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
ace Analytical
www.pacelabs.com Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Lab Sample No 925409617 Project Sample Number 9290353-008 Date Collected 03/18/05 1300
Client Sample ID P-40 Matrix Soil Date Received 03/18/05 1525
Parameters Results Units Report Limit DF Analyzed By GAS No Qual RegLmt
Wet Chemistry
Percent Moisture Method Moisture
Percent Moisture 6.4 1.0 03/21/05 0832 TNS
GC Semi volati les
TPH in Soil by 3545/8015 Prep/Method EPA 3545 EPA 8015
Diesel Fuel ND mg/kg 5.3 1.1 03/24/05 0532 KBS 68334-30-5
n4entacosane CS 108 1.0 03/24/05 0532 KBS 629-99-2
Date Extracted 03/21/05 03/21/05
GC Volatiles
GAS Soil North Carolina Method EPA 8015
Gasoline ND mg/kg 4.3 0.9 03/21/05 2010 DHW
4-Bromofluorobenzene 89 1.0 03/21/05 2010 DHW 460-00-4
Date 03/29/05 Page 20 of 79
REPORT OF LABORATORY ANALYSIS
Asheville Certification lOs This report shall not be reproduced except in full Charlotte Certification OsNCWastewater40without the written consent of Pace Analytical Services Inc NC Wastewater 12NCDrinkingWater37712NCDrinkingWater37706SCEnvironmental99030SC99006FLNELAPE87648IIdCFLNELAPE87627
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Lab Sample No 925409625
Client Sample ID P-37
Project Sample Number 9290353-009
Matrix Soil
Date Collected 03118/05 1230
Date Received 03/18/05 1525
Parameters
Wet Cheniistry
Percent Moisture
Percent Moisture
Results Units Report Limit DF Analyzed By CAS No QaL RegLint
Method Moisture
5.2 1.0 03/21/05 0833 INS
GC Seinivolatiles
TPH in Soil by 3545/8015
Diese Fuel
flPefltacosane
bate Extracted
Prep/Method EPA 3545 EPA 8015
10 mg/kg
107
03/21/05
5.3 1.1 03/24/05 0005 KBS 68334-30-5
1.0 03/24/05 0005 KBS 29-99-2
03/21/05
GC Volatiles
GAS Soil North Carolina
Gasoline
4-Bromofl uorobenzene CS
Date fl3/29/05
Method EPA 8015
ND mg/kg
92
4.5 0.9 03/21/05 2041 0MW
LO 03/21/05 2041 0MW 460-00-4
Page 21 of 79
Asheville Certification lDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSiS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Iida
Charlotte Certification lDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
Fl NFl AP FR7R27
ace AnaIicaI
www.pacelabs.com
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Pace Analylical Services Inc
9800 Kincey Avenue Suite 100
Honters villa NC 28078
Phone [phone]
Fax [phone]
Lab Sample No 925409633
Client Sample ID P-39
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
GC Sennvolaties
TPH in Soil by 3545/8015
Diesel Fuel
n-Pefltacosane
late Extracted
GC Volatiles
GAS Soil North Carolina
Gasoline
4-Bromofl uorobenzene CS
Method Moisture
Prep/Method EPA 3545 EPA 8015
ND mg/kg 5.3
Date Collected 03/18/05 1255
Date Received 03/18/05 1525
KBS 68334-30-5
KBS 629-99-2
Asheville Certification IDs
NCWastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the wrilten consent of Pace Analytical Services Inc
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP E87627
aceAnaIicaI
www.pacelabs.com
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Results
76
03/21/05
Method
ND
91
EPA 8015
mg/kg
Project Sample Number 9290353-010
Matrix Soil
Units Report Limit DF Analyzed By CAS No QL RegLmt
4.9 1.0 03/21/05 0833 TNS
1.1 03/24/05 0532
1.0 03/24/05 0532
03/21/05
4.2 0.8 03/21/05 2112 DHW
1.0 03/21/052112 DHW 460-00-4
Page 22 of 79Date03129105
ace AnaIicaI
www.pacelabs.com
Lab Sample No 925409641
Client Sample ID P-36
Project Sample Number 9290353.011
Matrix Soil
Date Collected 03/18/05 1325
Date Received 03/18/05 1525
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
GC Sennvolatiles
TPH in Soilby 3545/8015
Di ese1 Fuel
nPØntacosane CS
Date Extracted
GC Volatiles
GAS Soil North Carolina
Gasoline
4-Bromofluorobenzene CS
EPA 3545 EPA 8015
mg/kg 6.5 1.3 03/24/05 0503 KBS
1.0 03/24/05 0503 KBS
03/21/05
5.1 1.0 03/21/05 2140 DHW
1.0 03/21/05 2140 DHW 460-00-4
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
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FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
A0C0q0ne1a
Charlotte Certification lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FLNELAP F87B27
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Results Units Report Limit OF Analyzed By CAS No RegLet
Method Moisture
23.3 1.0 03121/05 0833 TNS
Prep/Method
MD 68334-30-5
116 629-99-2
03/21/05
Method EPA 8015
ND mg/kg
88
Page 23 of 79
Date 03/29/05
Pace AnalytIcal Services Inc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Lab Sample No 925409658
Client Sample ID P-35
Project Sample Number 9290353-012
Matrix Soil
Date Collected 03/18/05 1315
Date Received 03/18/05 1525
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
GC Semivolatales
TPH in Soil by 3545/8015
Diesel FUel
nPertacosane
Extracted
GC Volatiles
GAS Soil North Carolina
Gasoline
4-Bromofl uorobenzene
Method Moisture
79
Prep/Method EPA 3545 EPA 8015
ND mg/kg 54
81
03/21/05
1.1 03/24/05 0304 KBS 68334-30-5
1.0 03/24/05 0304 KBS 629-99-2
03/21/05
4.0 0.8 03/21/05 2211 01-lW
1.0 03/21/05 2211 DHW 460-00-4
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced except in futl
without the written Consent of Pace Analytical Services Inc
Charlotte Certification lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
Ft NFl AP FRTh27
ace Analytical
www.pacelabs.com
Results Units Report Limit OF Analyzed By
1.0 03/21/05 0834 INS
Method EPA 8015
ND mg/kg
88
CAS No RegLmt
Page 24 of 79
Date 03/29/05
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Huntersville ti/C 28078
Phone [phone]
Fax [phone]
Lab Sample No
Client Sample ID P-31
925409666 Project Sample Number 9290353-013
Matrix Soil
Date Collected 03/18/05 1210
Date Received 03/18/05 1525
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
Results Units Report Limit OF Analyzed By CAS No Qual RegLmt
Method Moisture
12.4 1.0 03/21/05 0850 TNS
GC Semivolatiles
TPH in Soil by 3545/8015
Diesel Fuel
-Pentacosane
Date Extracted
Prep/Method EPA 3545 EPA 8015
ND mg/kg
118
03/21/05
5.7 1.1 03/24/05 0135 KBS 68334-30-5
1.0 03/24/05 0135 KBS 629-99-2
03/21/05
GC Volatiles
GAS Soil North Carolina
Gasoline
4-Bromofi uorobenzene
Date 03/29105
Method EPA 8015
ND mg/kg
93
4.5 0.9 03/21/05 2242 DUW
1.0 03/21/05 2242 DHW 460-00-4
Page 25 of 79
Asheville Certification IDs
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REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Acco
Charlotte Certification lOs
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FL NELAP E87627
Analytical
www.pacelabs.com
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hwitersville NC 28078
Phone [phone]
Fax [phone]
Lab Sample No 925409674
Client Sample ID P-32
Project Sample Number 9290353-014
Matrix Soil
Date Collected 03/18/05 1200
Date Received 03/18/05 1525
Parameters
Wet Chemistry
Percent Moisture
Percent Moisture
Results Units Report Limit DF
Method Yb Moisture
6.9 Yb
Analyzed By CAS No Qual RegLmt
1.0 03/21/05 0851 TNS
GC Semivolatiles
TPH in Soil by 3545/8015
Diesel Fuel
n-Pentacosane
Date Extracted
Prep/Method EPA 3545 EPA 8015
ND mg/kg 5.4
91 Yb
03/21/05
1.1 03/24/05 0334 KBS 68334-30-5
1.0 03/24/05 0334 KBS 629-99-2
03/21/05
GC Volatiles
GAS Soil North Carolina
Gasoline
-Bromofl uorobenzene
Date 03/29/05
Method EPA 8015
ND mg/kg
84
4.4 0.9 03/21/05 2313 DI-IW
1.0 03/21/05 2313 DHW 460-00-4
Page 26 of 79
Asheville Certification IDs
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REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
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AOS
theh\
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
Fl Nil AP FR727
Ana1yticaI
www.pacelabs.com
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Parameters
Wet Chemistry
Percent Moisture
GC Semi volati es
TPH in Soi1.by 3545/8015
Diesel Fuel
nPentacosane CS
Date Extracted
GC Volatiles
GAS Soil North Carolina
Gasoline
Prep/Method EPA 3545 EPA 8015
ND mg/kg 5.6
105
03/21/05
1.1 03/24/05 0234
1.0 03/24/05 0234
03/21/05
4.0 0.8 03/21/05 2343 DHW
10 03/21/05 2343 DHW 460-00-4
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Ate0
ThØlath
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
ce Analytical
www.pacelabs.com
925409682
Results
Lab Sample No
Client Sample ID P.33
Percent Moisture
Method Moisture
10.7
4-Bromofl uorobenzene CS
Method
ND
81
EPA 8015
mg/kg
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax[phone]LabProjectNumber9290353
Client Project ID West End 6228-05-2694
Project Sample Number 9290353-015 Date Collected 03/18/05 1230
Matrix Soil Date Received 83/18/05 1525
Units Report Limit OF Analyzed By GAS No Qual RegLat
1.0 03/21/05 0851 TNS
KBS 68334-30-5
KBS 629-99-2
Page 27 of 79
Oate 03/29/05
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Dilution factor shown represents the factor applied to the reported result and reporting limit due to changes
in sample preparation dilution of the extract or moisture content
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic
testing was performed at our Pace Charlotte laboratory unless otherwise footnoted
Nethod 90718 modified to use ASE
All pH Free Chlorine Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended mmediate
hold time
ND Not detected at or above adjusted reporting limit
NC Not Calculable
Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
CS Surrogate
Common laboratory contaminant
Surrogate recovery
outside of control
limits The data was accepted based on valid recovery of remaining
surrogate
Surrogate standards were not recovered due to sample dilution
The sample extract could not be concentrated to the normal
final volume This resulted in an elevated
reporting limit
The sample was diluted to reduce matrix interference resulting in elevated reporting limits
The surrogate recovery was outside OC acceptance limits due to matrix interference
The reported result may bebiased high due to matrix interference with the internal standard This was
confirmed by reanalysis of the sample
Low surrogate recovery
was confirmed as matrix effect by second analysis
The surrogate recovery
was above the QC recovery limit The sample was not re-extracted since no target
analytes were detected in the sample
Acid surrogate recovery outside of control limits The data was accepted based on valid recovery of the two
remaining acid surrogates
Date 03/29/05 Page 48 of 79
REPORT OF LABORATORY ANALYSIS
Asheville Certification lOs This report shall not be reproduced except in full Charlotte Certification lOs
NC Wastewater 40 without the written consent of Pace Analytical Services Inc NC Wastewater 12
NC Drinking Water 37712 NC Drinking Water 37706SCEnvironmental99030SC99006IlrSPflritrirn
ce Analytical
www.pacelabs.com
PARAMETER FOOTNOTES
Analytical
www.pacelabs.com
METHOD BLANK 925411803
Associated Lab Samples
Parameter
Aliphatic C09-C18
Aliphatic C19-C36
Aromatic C11-22
2-Fluorabiphenyl CS
2-Bromonaphthal ene CS
Nonatriacontane CS
o-Terphenyl CS
LABORATORY CONTROL SAMPLE 925411811
Blank
Result
ND
ND
ND
112
113
104
117
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Parameter
Aliphatic C09-C18
Aliphatic C19-C36
Aromatic C11-22
2-Fl uorobiphenyl CS
2-Bromonaphthalene
Nonatriacontane CS
o-Terphenyl CS
LCS
Rec Footnotes
92
91
86
MATRIX SPIKE MATRIX SPIKE DUPLICATE 925411829 925411837
Asheville Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
Ft NFi AP FR7c4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certification lDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
ri .lrI Ar
QUALITY CONTROL DATA
Pace Analytical Services nc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
QC Batch 123887 Analysis Method EPH
QC Batch Method EPA 3550 Analysis Description EPH in Soil by Mass Method
Associated Lab Samples 925409500 925409518 925409534
925409500 925409518 925409534
Units
mg/kg
mg/kg
mg/kg
Reporting
Limit Footnotes
10
10
10
Spike LCS
Units Conc Result
mg/kg 10.00 9.193
mg/kg 13.33 12.16
mg/kg 28.33 24.27
74
47
118
109
925404717 Spike MS MSD MS MSD
Parameter Units Result Conc Result Result IRec Rec RPD Footnotes
Aliphatic C09-C18 mg/kg 19.05 12.18 8.740 10.90 22 1.1
Aliphatic CC19-C36 mg/kg 4.597 16.24 11.51 13.73 43 56 18
Aromatic CC11-22 mg/kg 8.174 34.51 31.59 23.06 68 43 31
2-Fluorobiphenyl CS 104 86
2-Bromonaphthalene CS 110 89
Date 03/29/05 Page 49 of 79
Parameter
Aliphatic C09-C18
Aliphatic C19-C36
Aromatic C11-22
2-Fluorobiphenyl CS
2-Bromonaphthal ene CS
Nonatriacontane
o-Terphenyl CS
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Footnotes
24
Asheville Certification lDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
CCo8
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
ci
Analytical
www.pacelabs.com QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hiintersville NC 28078
Phone [phone]
Fax [phone]
KAThIX SPIKE MATRIX SPIKE DUPLICATE 925411829 925411837
925404717 Spike MS MSD MS HSD
Parameter Units Result Conc Result Result tRec Rec RPD Footnotes
Nonatriacontane CS 76 87
o-Terphenyl CS 95 76
SAMPLE DUPLICATE 925411845
Units
mg/kg
mg/kg
mg/kg
925404733 DUP
Result Result
68.00 63.00
19.00 21.00
25.00 31.00
119 116
171 191
110 98
114 107
Date 03/29/05 Page 50 of 79
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
LABORATORY CONTROL SAMPLE 925414690
Spike LCS LCS
Parameter Units Conc Result Rec Footnotes
Diesel Fuel mg/kg 166.70 147.6 89
n-Peritacosane 146
MATRIX SPIKE MATRIX SPIKE DUPLICATE 925414716 925414724
925410755 Spike MS MSD MS MSD
Parameter Units Result Conc Result Result Rec %Rec RPD Footnotes
Diesel Fuel mg/kg 0.9523 208.10 186.1 325.1 89 156 54 24
n-Pentacosane 138 117
SAMPLE DUPLICATE 925414708
Parameter
Diesel Fuel
nPentacosane CS
925410748
Result
ND
100
Result Footnotes
ND NC
105
Asheville Certification lOs
NC Wastewater 40
NC Drinking Water 37712
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FL NELAP E87F48
REPORT OF LABORATORY ANALYSiS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
ACCe
Charlotte Certification lOs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
Ci MCI AD Co7Cr7
ce Analytical
www.pacelabs.com QUALITY CONTROL DATA
QC Batch 123964 Analysis Method EPA 81115
QC Batch Method EPA 3545 Analysis Description TPH in Soil by 3545/8015
Associated Lab Samples 925409575 925409583 925409591 925409609 925409617
925409625 925409633 925409641 925409658 925409666
925409674 925409682
METHOD BLANK 925414682
Associated Lab Samples
Parameter
Diesel Fuel
n-Pentacosane CS
925409575 925409583 925409591 925409609 925409617 925409625 925409633
925409641 925409658 925409666 925409674 925409682
Blank Reporting
Units Result Limit Footnotes
mg/kg ND 5.0
128
Units
mg/kg
DUP
Date 03129/05 Page 51 79
eAnaIicaI QUALITY CONTROL DATA
Pace Analyiical Services Inc
9800 Kincey Avenue Suite 100
1-lunters villa NC 28078
Phone [phone]
Fax [phone]
NC Wastewater
NC Drinking Water
SC
ci iiici An
12
37706
99006
www.pacelabs.com
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
QC Batch 124037 Analysis Method EPH
QC Batch Method EPA 3550 Analysis Description EPH in Soil by Mass Method
Associated Lab Samples 925409690 925409708 925409716 925409724
METHOD BLANK 925416703
Associated Lab Samples 925409690 925409708 925409716 925409724
Blank Reporting
Parameter Units Result Limit Footnotes
Aliphatic C09-C18 mg/kg ND 10
Aliphatic C19-C36 mg/kg ND 10
Aromatic C11-22 mg/kg ND 10
2-Fluorobiphenyl CS 106
2-Bromànaphthalene CS 103
Nonatriacontane 114
o-Terphenyl CS 109
LABORATORY CONTROL SAMPLE 925416711
Spike LCS LCS
Parameter Units Conc Result XRec Footnotes
Aliphatic C09-C18 iag/kg 10.00 7.540 75
Aliphatic C19-C36 mg/kg 13.33 13.60 102
Aromatic C11-22 mg/kg 28.33 23.16 82
2-Fluorobiphenyl CS 91
2-Bromonaphthalene CS 93
Nonatriacontane 105
o-Terphenyl 90
MATRIX SPIKE MATRIX SPIKE DUPLICATE 925416729 925416737
925409690 Spike MS MSD MS 1150
Parameter Units Result Conc Result Result tRec tRec RPO Footnotes
Aliphatic C09-C18 mg/kg 11.16 5.808 6.174 52 55
Aliphatic C19-C36 mg/kg 14.88 13.01 13.90 87 93
Aromatic C11-22 mg/kg 31.63 22.81 20.76 72 66
Date 03/29/05
Ashevflle Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
PJfl AP
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Incic
Page 52 of 79
Jiarlotte Certification IDs
MATRIX SPIKE MATRIX SPIKE DUPLICATE 925416729 925416737
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID blest End 6228-05-2694
Parameter
2-Fl uorobiphenyl CS
2-Bromonaphthalene -S
Nonatriacontane
o.Terphenyl CS
MS MSD MS MSD
Units Result Conc Result Result XRec %Rec
99 94
95 84
87 84
80 73
RPD Footnotes
Ashevifle Certification lDs
NC Wastewater 40
NC Drinking Water 37712
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FL NFl AP FR7f4R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
barJotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
rtci CO7V7
/29 Analytical
www.pacelabs.com QUALITY CONTROL DATA
925409690 Spike
Date 03/29/05 Page 53 of 79
QUALITY CONTROL DATA
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
QC Batch 123959 Analysis Method EPA 8015
DC Batch Method EPA 8015 Analysis Description
GAS Soil North Carolina
Associated Lab Samples 925409575 925409583 925409591 925409609 925409617
925409625 925409633 925409641 925409658 925409666
925409674 925409682
METHOD BLANK 925414195
Associated Lab Samples 925409575 925409583 925409591 925409609 925409617 925409625 925409633
925409641 925409658 925409666 925409674 925409682
Blank Reporting
Parameter Units Result Limit Footnotes
Gasoline mg/kg ND 5.0
4-Bromofluorobenzene 114
LABORATORY CONTROL SAMPLE LCSD 925414203 925414211
Spike LCS LCSD LCS LCSD
Parameter Units Conc Result Result ZRec %Rec RPD Footnotes
Gasoline mg/kg 2500 28.09 25.09 112 100 11
4-Bromofluorobenzene CS 85 101
MATRIX SPIKE 925414229
925409575 Spike MS MS
Parameter Units Result Conc Result XRec Footnotes
Gasoline mg/kg 0.6703 23.05 27.24 115
4-Bromofluorobenzene 71
SAMPLE DUPLICATE 925414237
925409591 DUP
Parameter
Gasoline
4Bromofl uorobenzene CS
Date 03/29/OS
Units Result Result RPD
mg/kg ND ND NC
93 93
Footnotes
Page 54 of 79
Asheville Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FLNELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
nelath
Charlotte Certification lOs
NC Wastewator 12
NC Drinking Water 37706
SC 99006
Fl JFI AP FR797
Pace Analytical Services Inc
9800 KinceyAveriue Suite 100
Hunters villa NC 28078
Phone [phone]
Fax [phone]
METHOD BLANK 925418352
Associated Lab Samples
Aliphatic C05 C08
Aliphatic C09-C12
Aromatic C09-ClO
2.5-Dibromotoluene FIDS
25-Dibromotoluene PlO
QUALITY CONTROL DATA
Blank Reporting
Result Limit Footnotes
ND 10
ND 10
MD 10
102
102
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
LABORATORY CONTROL SAMPLE 925418360
Spike LCS LCS
Parameter Units Conc Result tRec Footnotes
Aliphatic C05-COB mg/kg 20.00 19.98 100
Aliphatic C09-C12 mg/kg 5.000 5.013 100
Aromatic C09-C1O mg/kg 5.000 5.021 100
2.5-Dibromotoluene FID5 104
2.5-Dibromotoluene PIDS 106
MATRIX SPIKE MATRIX SPIKE DUPLICATE 925418378 925418386
Aliphatic CO5-C08
Aliphatic C09-C12
Aromatic C09-C10
25-Dibromotoluene FIDS
2.5-Dibromotoluene PIDS
Asheville Certification lOs
NC Wastevater 40
NC Drinking Water 37712
SC Environmental 99030
NFl AP FR7R48
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in lull
without the written consent of Pace Analytical Services Inc
ACt04
iijiotte Certification lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
ci ruci AD
Analytical
www.pacelabs.com
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
OC Batch 124057 Analysis Method VPH
QC Batch Method VPH Analysis Description VPH in Sail by Mass Method
Associated Lab Samples 925409500 925409518 925409534 925409690 925409708
925409716 925409724
Parameter
925409500 925409518 925409534 925409690 925409708
Units
mg/kg
mg/kg
mg/kg
925409716 925409724
Parameter
925409500 Spike MS MSD MS MSD
Units Result Conc Result Result tRec tRec RPD
mg/kg 0.5052 24.29 24.18 24.43 98 98
mg/kg 0.6090 6.073 6.148 6.195 91 92
mg/kg 0.1641 6.073 6.119 5.956 98 95
Date 03/29/05
119 106
119 107
Footnotes
Page 55 of 79
9800 Kincey Avenue Suite IOU
Pace Analytical Services Inc
ace Analytical
QUALITY CONTROL DATA
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
SAMPLE DUPLICATE 925418394
925409518 DUP
Parameter Units Result Result RPD Footnotes
Aliphatic C05-C08 mg/kg ND ND NC
Aliphatic C09C12 mg/kg ND ND NC
Aromatic C09C1D mg/kg ND ND NC
25-Dibroniotoluene FIDS 110 109
Dthromotoluene PIDS 112 111
Date 03129/OS
Page 56 of 79
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced except in full hrJofte Certification lOsNCWastewater40without the written consent of Pace Anaiytical Services Inc NC Wastewater 12NCDrinkingWater37712NCDrinkingWater37706SCEnvironmental99030SC99006FtNFlAPFR7A4R
ci Mi AD
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunt ers v/lie NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
QC Batch 123953 Analysis Method EPA 8270
QC Batch Method EPA 3545 Analysis Description Semivolatile Organics
Associated Lab Samples 925409500 925409518 925409534 925409690 925409708
925409716 925409724
METHOD BLANK 925413924
Associated Lab Samples 925409500 925409518 925409534 925409690 925409708 925409716 925409724
iiaville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
Fl NFl AP F7R4R
REPORT OF LABORATORY ANALYSIS
This report shaH not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Ate04
Charlotte Certification lDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
CI IICl AD E07CD7
Analytical
www.pacelabs.com QUALITY CONTROL DATA
Footnotes
Blank Reporting
Parameter units Result Limit
Acenaphthene ug/kg ND 330
Acenaphthylene ug/kg ND 330
Anthracene ug/kg ND 330
Benzokfluoranthene ug/kg ND 330
Benzobflucranthene ug/kg ND 330
Benzoaanthracene ug/kg MD 330
Benzoic acid ug/kg ND 1600
Benzogh.iperylene ug/kg ND 330
Benzyl alcohol ug/kg ND 660
Benzoapyrene ug/kg ND 330
4-Broniophenylphenyl ether ug/kg MD 330
Butylbenzylphthalate ug/kg ND 330
4-Chloro-3.methylphenol ug/kg ND 660
4-Chioroaniline ug/kg ND 660
bis2-Chloroethoxyinethane ug/kg ND 330
bis2-Chloroethyl ether ug/kg ND 330
bis2-Chloroisopropyl ether ug/kg ND 330
2Chloronaphthalene ug/kg ND 330
2-Chlorophenol ug/kg MD 330
4Chlorophenylphenyl ether ug/kg ND 330
Chrysene ug/kg ND 330
Dibenzahanthracene ug/kg ND 330
Dibenzofuran ug/kg ND 330
12-Dichlorobenzene ug/kg ND 330
1.3-Dichlorobenzerie ug/kg ND 330
1.4-Dichlorobenzene ug/kg ND 3303.3 -Dichlorobenzjdine ug/kg ND 660
2.4-Dichlorophenol ug/kg ND 330
Diethylphthalate ug/kg ND 330
2.4-Diinethyl phenol ug/kg ND 330
Date 03/29/05
Page 57 of 79
ice Analytical
www.pacelabs.com QUALITY CONTROL DATA
METHOD BLANK 925413924
Associated Lab Samples 925409500
Units
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ugfkg
ugfkg
ug/kg
ug/kg
ugf kg
ug/kg
ugfkg
ug/kg
ug/kg
ug/kg
ugfkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Blank
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Reporting
Limit Footnotes
330
330
330
1600
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1600
1600
1600
330
330
1600
330
330
1600
330
330
330
330
330
330
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vu/c NC 28078
Phone [phone]
Fax [phone]
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
Fl NFl AP FR7R4R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Act0
ha.rlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
ri ruiI AD
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
925409518 925409534 925409690 925409708
Parameter
Dimethylphthal ate
Di -n-butylphthal ate
46-Dinitro-2methylphenol
.4-Di.nitrophenol
24-Dinitrotoluene
26-Dinitrotoluene
Di-n-octylphthal ate
2-Diphenylhydrazine
bis2-Ethylhexyl phthalate
Fluoranthene
Fluorene
Hexachi oro-13 butadiene
Hexachlorobenzene
Hexachl orocycl opentadi ene
Hexachloroethane
lndeno12.3-cdpyrene
Isophorone
2-Methyl naphthal
ene
2-Methyiphenol o-Cresol
34-Methylphenol
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Ni trophenol
4-Nitrophenol
N-Nitroso-di -n-propyl amine
N-Nitrosodiphenyl amine
Pentachi orophenol
Phenanthrene
Phenol
Pyrene
L24-Trichlorobenzene
2.4 5-Trichlorophenol
2.46-Trichiorophenol
Date 03/29/05
925409716 925409724
Page 58 of 79
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
METHOD BLANK 925413924
Associated Lab Samples 925409500 925409518 925409534 925409690 925409708 925409716 925409724
Parameter
Nitrobenzene-d5
2-FTuorobiphenyl CS
Terphenyl-d14 CS
Phenol-d5 CS
2-Fluorophenol CS
Tribromophenol
Blank Reporting
Units Result Limit Footnotes
53
58
77
54
49
57
LABORATORY CONTROL SAMPLE 925413932
Ashnvule Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
Fl NFl AP
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in tull
without the written consent of Pace Analytical Services IncCC0
Charlotte Certification lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
llt AD O7cr7
ceAnaIicaI
QUALITY CONTROL DATAwww.pacelabs.com
Spike LCS LCS
Parameter Units Conc Result tRec Footnotes
Acenaphthene ug/kg 1667.00 973.2 58
Acenaphthylene ug/kg 1667.00 1024 61
AnthracØne ug/kg 1667.00 1136 68
BenzoCkfluoranthene ug/kg 1667.00 1287 77
Berizobfluoranthene ug/kg 1667.00 1186 71
BerizoCaanthracene ug/kg 1667.00 1158 70
Benzoic acid ug/kg 1667.00 579.3 35
Benzog.h.iperylene ug/kg 1667.00 916.8 55
Benzyl alcohol ug/kg 1667.00 990.7 59
Benzoapyrene ug/kg 1667.00 1154 69
4-Bromophenylphenyl ether ug/kg 1667.00 1070 64
Butylbenzylphthalate ug/kg 1667.00 1151 69
4-Chloro-3-methylphenol ug/kg 1667.00 1101 66
4-Chloroaniline ug/kg 1667.00 895.8 54
bisC2Chloroethoxymethane ug/kg 1667.00 883.0 53
bisC2-Chloroethyl ether ug/kg 1667.00 825.1 50
bis2-Chloroisopropyl ether ug/kg 1667.00 868.1 52
2-Chloronaphthalene ug/kg 1667.00 956.0 57
2-Chiorophenol ug/kg 1667.00 833.7 50
4-Chlorophenylphenyl ether ug/kg 1667.00 1087 65
Chrysene ug/kg 1667.00 11.21 67
Dibenza.hanthracene ug/kg 1667.00 973.1 58
Dibenzofuran ug/kg 1667.00 1077 65
12-Dichlorobenzene ug/kg 1667.00 839.9 50
Date 03/29105 Page 59 of 79
LABORATORY CONTROL SAMPLE 925413932
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vu/c NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 622B-O52694
Ashevifle Certification lDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
Fl NFl AP FR7R4R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
/neIc
Charlotte Certification lDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
ci MI AD
ace AnalicaI
www.pacelabs.com QUALITY CONTROL DATA
Spike LCS LCS
Parameter Units Conc Result tRec Footnotes
13-Dichlorobenzene ug/kg 1667.00 806.0 48
14-Dichlorobenzene ug/kg 1667.00 830.7 50
3.3-Dichlorobenzidjne ug/kg 3333.00 766.6 23
2.4Dich1orophenol ug/kg 1667.00 947.4 57
Diethyiplithalate ug/kg 1667.00 1144 69
2.4-Dimethyiphenol ug/kg 1667.00 884.4 53
Dirnethy1phtha1ate ug/kg 1667.00 1118 67
Di-n-butylphthalate ug/kg 1667.00 1146 69
4.6-Dinitro-2-methylphenol ug/kg 1667.00 1351 81
24Dinitrophenol ug/kg 1667.00 1207 72
24-Dinitrotoluene ugIkg 1667.00 1222 73
26-Dinitrotoluene ug/kg 1667.00 1175 70
Di-n-äctylphthalate ug/kg 1667.00 1178 71
1.2-Diphenyihydrazine ug/kg 1667.00 988.3 59
bis2-Ethylhexylphthalate ug/kg 1667.00 1205 72
Fluoranthene ug/kg 1667.00 1125 68
Fluorene ug/kg 1667.00 1086 65
Hexachloro-1.3-butadiene ug/kg 1667.00 823.1 49
Hexachlorobenzene ug/kg 1667.00 1019 61
Hexachiorocyclopentadiene ug/kg 1667.00 666.2 40
Hexachioroethane ug/kg 1667.00 778.9 47
Indeno1.2.3-cdpyrene ug/kg 1667.00 984.3 59
Isophorone ug/kg 1667.00 974.1 58
2-Methylnaphthalene ug/kg 1667.00 904.5 54
2-Methyiphenol o-Cresol ug/kg 1667.00 908.1 54
34-Mettyl phenol ug/kg 1667.00 969.1 58
Naphthalene ug/kg 1667.00 848.5 51
2-Nitroaniline ug/kg 1667.00 938.5 56
3-Nitroaniline ug/kg 1667.00 1134 68
4-Nitroaniline ug/kg 1667.00 1433 86
Nttrobenzene ug/kg 1667.00 840.9 50
2-Nitrophenol ug/kg 1667.00 896.2 54
4-Nitrophenol ug/kg 1667.00 1138 68
N-NltrOso-di-n-propylamine ug/kg 1667.00 907.8 54
N-Nitrosodiphenylamine uglkg 1667.00 1229 74
Pentachlorophenol ug/kg 1667.00 1085 65
Phenanthrene ug/kg 1667.00 1115 67
Date 03/29/05 Page 60 of 79
Parameter
Phenol
Pyrene
12 4-Trichlorobenzene
2.4 5-Trichi orophenol
24.6 -Trichi orophenol
NitrObenzene-d5 CS
2-Fluorobiphenyl CS
Terphenyl d14 CS
Phenol-d5 CS
2-Fluorophenol CS
2.4.6-Tribromophenol CS
Spike LCS
Conc Result
1667.00 870.0
1667.00 1166
1667.00 829.1
1667.00 1152
1667.00 1073
MATRIX SPiKE MATRIX SPIKE DUPLICATE 925413940 925413957
Parameter
Acenaphthene
4-Chi oro-3-methyl phenol
2-Chlorophenol
14-Dichlorobenzene
24-Dinitrotoluene
4-Nitrophenol
N-Nitroso-di -n-propylaniine
Pentachl orophenol
Phenol
Pyrene124-Trichl orobenzene
Nitrobenzene-d5 CS
2-Fl uorobiphenyl CS
Terphenyl-d14
Phenol-d5
Fl uorcphenol CS
2.4.6-Tribroinophenol CS
69 61
48 44
44 41
54 48
Footnotes
12
13
11
10
11
11
15
15
10
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NC Wastewater 40
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0Jl AP
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
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t_J9_toqo
Charlotte Certification lOs
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SC 99006
ce Analytical
www.pacelabs.com QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE 925413932
Pace Analytical Services Inc
.9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
LCS
Rec Footnotes
52
70
50
69
64
51
60
74
52
49
66
925409500 Spike MS MSD MS MSD
Units Result Conc Result Result XRec tRec
ug/kg 2024.00 1095 973.7 54 48
ug/ky 2024.00 1202 1059 59 52
ug/kg 2024.00 996.3 895.5 49 44
ug/kg 2024.00 1005 914.3 50 45
ug/kg 2024.00 1366 1223 68 60
ug/kg 2024.00 1246 1119 62 55
uglkg 2024.00 1096 944.8 54 47
ug/kg 2024.00 1199 1029 59 51
ug/kg 2024.00 997.9 902.9 49 45
ug/kg 2024.00 1361 1239 67 61
ug/kg 2024.00 1002 928.4 50 46
48 46
53 50
Date 03/29105
Page 61 of 79
SAMPLE DUPLICATE 925413965
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Parameter
Acenaphthene
Acenaphthyl ene
Anthracene
Benzokfluoranthene
Benzobjfl uoranthene
Benzoaanthracene
Benzoic acid
Eenzog.hiperylene
Benzyl alcohol
Benzoapyrene
4-Broinophenyl phenyl
ether
Butyl benzyl phthal
ate
4-Chloro-3 -methyl phenol
4-Chloroaniline
bis2-Chloroethoxyjnethane
bis2-Chloroethyl ether
bis2-Chloroisopropyl ether
2-Chl oronaphthalene
2-Chlorophenol
4-Chiorophenyl phenyl
ether
Chrysene
Dibenz anthracene
Di benzofuran
2-Dichlorobenzne
1.3-Di chi orobenzene
1.4-Dichlorobenzene33-Dichl orobenzidjne
24-Di chl orophenol
Di ethyl phthal ate
2.4-Dimethylphenol
Dimethyl phthal ate
Di -n-butyl phthal ate
4.6-Dinitro-2-methylphenol
24 -Di nitrophenol
2.4-Dinitrotoluene
6-Dinitrotol uene
Di -n-octyl phthal ate
_________Result RPD
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
ND ND NC
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
Mfl AD
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced exceptin full
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Charlotte Certification IDs
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SC 99006
/ace Analytical
www.pacelabs.com QUALITY CONTROL DATA
925409716
Result
DUP
FootnotesUnits
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
ug/kg
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
Date 03/29/05
Page 62 of 79
SAMPLE DUPLICATE 925413965
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
925409716 DUP
AsheviUe Certification liDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
CI MCI 110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services inc
ai1ofte Gerfif icaf ion his
NC Wastewater 12
NC Drinking Water 37706
SC 99006
ace Analytical
www.pacelabs.com QUALITY CONTROL DATA
Parameter Units Result Result RPD Footnotes
12-Diphenyihydrazine ug/kg ND ND NC
bis2-Ethylhexylphthalate ug/kg ND ND NC
Fluoranthene ug/kg ND ND NC
Fluorene uglkg ND ND NC
Hexachloró-13.butad-iene ug/kg ND ND NC
Hexachlorobenzene uglkg ND ND NC
Hexachlorocyclopentadiene ug/kg ND ND NC
Hexachioroethane ug/kg ND ND NC
Indeno123-cdpyrene ug/kg ND ND NC
Isophorone ug/kg ND ND NC
2-Methylnaphthalene uglkg ND ND NC
2-Hethyiphenol o-Cresol ug/kg ND ND NC
34-Methyl phenol ugikg ND ND NC
Naphthalene ug/kg ND ND NC
2-Nitroaniline ug/kg ND ND NC
3-Nitroaniline ug/kg ND ND NC
4-Nitroaniline ug/kg ND ND NC
Nitrobenzene ug/kg ND ND NC
2-Nitrophenol ug/kg ND ND NC
4-Nitrophenol ugfkg ND ND NC
N-Nitroso-di-npropylamjne uglkg ND ND NC
N-Nitrasodiphenyl amine ug/kg ND ND NC
Pentachiorophenol ugfkg ND ND NC
Phenanthrene uglkg ND ND NC
Phenol ug/kg ND ND NC
Pyrene ug/kg ND ND NC
l24-Trichlorobenzene ugfkg ND ND NC
24.5-Trichiorophenol ug/kg ND ND NC
2.4.6-Trichlorophenol ug/kg ND ND NC
Nitrobenzene-d5 52 54
2-Fluorobiphenyl CS 59 60
Terphenyl-d14 CS 78 80
Phenol-d5 CS 45 48
2-Fluorophenol CS 34 36
24.6-Tribromophenol 44 43
Date 03129/OS
Page 63 of 79
Date 03/29/OS
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters villa NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Page 64 of 79
Asheville Certification lDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
ri MCI An tO7AO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
AC04
Charlotte Certification lOs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
ce Analytical
www.pacelabs.com QUALITY CONTROL DATA
QC Batch 123972 Analysis Method EPA 8260
QC Batch Method EPA 8260 Analysis Description
GC/MS VOCs 5035/8260 low level
Associated Lab Samples 925409500 925409518 925409534 925409690 925409716
925409724
METHOD BLANK 925415432
Associated Wab Samples 925409500 925409518 925409534 925409690 925409716 925409724
Blank Reporting
Parameter Units Result Limit Footnotes
Acetone ug/kg ND 100
Benzene ug/kg NO 5.0
Bromobenzene ug/kg ND 5.0
Bromochiorometliane ug/kg ND 5.0
Bromodichloromethane ug/kg ND 5.0
Bromoform ug/kg ND 5.0
Bromomethane ug/kg ND 10
2-Butanone MEK ugfkg ND 100
n-Butylbenzene ug/kg ND 5.0
sec-Butylbenzene ug/kg ND 5.0
tert-Butylbenzene ug/kg ND 5.0
Carbon tetrachioride ug/kg ND 5.0
Chioroberizene ug/kg ND 5.0
Chioroethane ug/kg ND 10
Chloroform ug/kg ND 5.0
Chloromethane ug/kg ND 10
2-Chlorotoluene ug/kg ND 5.0
4-Chiorotoluene ug/kg ND 5.0
1.2-Dibromo-3-chloropropane ug/kg ND 5.0
Dibromochioromethane ug/kg ND 5.0
1.2-Dibromoethane EDS ug/kg ND 5.0
Dibromomethane ug/kg ND 5.0
12-Dichlorobenzerie ug/kg ND 5.0
13-Dichlorobenzene ug/kg ND 5.0
14-Dichlorobenzene ug/kg ND 5.0
Dichiorodifluoromethane ug/kg ND 10
1.1-Dichioroethane ug/kg ND 5.0
1.2-Dichioroethane ug/kg ND 5.0
11-Dichloroethene ug/kg ND 5.0
cis-12-Dichloroethene ug/kg ND 5.0
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REPORT OF LABORATORY ANALYSIS
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Analytical
www.pacelabs.com QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
METHOD BLANK 925415432
Associated Lab Samples 925409500 925409518 925409534 925409690 925409716
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
925409724
Blank Reporting
Parameter Units Result Limit Footnotes
trans-12-Dichloroethene ug/kg ND 5.0
1.2-Dichioropropane ug/kg ND 5.0
Dichioropropane ug/kg ND
Dichioropropane ug/kg ND
Dichloropropene ug/kg ND
cis Dichloropropene ug/kg ND
trans-1.3-Dichloropropene ug/kg ND 5.0
Olisopropyl ether ug/kg ND 5.0
Ethylbenzene ug/kg ND 5.0
Hexachioro-13-butadiene ug/kg ND 5.0
2-Hexanone ug/kg ND 50
Isopropylbenzene Cumene ug/kg ND 5.0
p-Isopropyltoluene ug/kg ND 5.0
Methylene chloride ug/kg ND 5.0
4-Methyl -2-pentanone MIBK ug/kg ND 50
Methyl -tert-butyl ether ug/kg ND 5.0
Naphthalene ug/kg ND 5.0
n-Propylbenzene ug/kg ND 5.0
Styrene ug/kg ND 5.0
1.11.2-Tetrachioroethane ug/kg ND 5.0
1.1.2.2-Tetrachioroethane ug/kg NO 5.0
Tetrachloroethene ug/kg ND 5.0
Toluene ugikg ND 5.0
l.23-Trichlorobepzene ug/kg ND 5.0
1.2.4-Trichlorobenzene ug/kg ND 5.0
11.1-Trichioroethane ug/kg NO 5.0
112-Trichioroethane ug/kg ND 5.0
Trichioroethene ug/kg ND 5.0
Trichiorofluoromethane ug/kg ND 5.0
12.3-Trichloropropane ug/kg ND 5.0
124-Trimethylbenzene ug/kg ND 5.0
13.5-Triuiethylbenzene ug/kg ND 5.0
Vinyl acetate ug/kg ND 50
Vinyl chloride ug/kg ND 10
Xylene Total ugfkg ND 5.0
mp-Xylene ug/kg ND 10
Date Q3/29/05
Page 65 of 79
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SC Environmental 99030
11 tHI AD
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
hunters villa NC 28078
Phone [phone]
Fax [phone]
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
Cl MCI Afl
eAnaIicaI
QUALITY CONTROL DATAwww.pacelabs.com
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
METHOD BLANK 925415432
Associ ated Lab Sampi es 925409500 925409518 925409534 925409690 925409716 925409724
Blank Reporting
Parameter Units Result Limit Footnotes
o-Xylene ug/kg ND 5.0
Toluene-d8 CS 98
4-Bromofluorobenzene 92
Dibrornofl.uoromethane CS 108
1-Dichloroethane-d4 107
LABORATORY CONTROL SAMPLE 925415440
Spike LCS LCS
Parameter Units Conc Result Rec Footnotes
Acetone uglkg 100.00 125.4 125
Benzene ug/kg 50.00 51.70 103
Bromobenzene ug/kg 50.00 54.31 109
Bromochloromethane ugfkg 50.00 54.86 110
Bromodicliloromethane ug/kg 50.00 51.51 103
Bronioform ug/kg 50.00 53.33 107
Bromomethane ug/kg 50.00 54.32 109
2-Butanone MEK ug/kg 100.00 93.76 94
n-Butylbenzene up/kg 50.00 48.12 96
sec-Butylbenzene uglkg 50.00 56.16 112
tert-Butylbenzene ug/kg 50.00 57.67 115
Carbon tbtrachloride ug/kg 50.00 54.82 110
Chlorobenzene ug/kg 50.00 51.28 103
Chloroethane ug/kg 50.00 52.09 104
Chloroform ug/kg 50.00 54.19 108
Chioromethane ug/kg 50.00 45.40 91
2-Chlorotoluene ug/kg 50.00 55.88 112
4-Chlorotoluene uglkg 50.00 52.62 105
1.2-Oibromo-3-chloropropane uglkg 50.00 56.17 112
Dibromochloromethane ug/kg 50.00 52.93 106
12-Dibromoethane EDS uglkg 50.00 54.58 109
Oibromomethane ug/kg 50.00 52.38 105
12-Dichlorobenzene ug/kg 50.00 53.72 107
13-Dichlorobenzene uglkg 50.00 51.73 103
1.4Oichlorobenzene ug/kg 50.00 50.82 102
Date 03129/05
Page 66 of 79
LABORATORY CONTROL SAMPLE 925415440
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Huntersville IVC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
heviile Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
ct ci ao iQ7AQ
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certification iDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
ace AnaIicaI
www.pacelabs.com QUALITY CONTROL DATA
Spike LCS LCS
Parameter Units Conc Result XRec Footnotes
Dichlorodifluorojnethane ug/kg 50.00 45.25 90
11-Dich1oroethane ug/kg 50.00 53.14 106
12-Dichioroethahe ug/kg 50.00 54.33 109
11-Dichioroethene ug/kg 50.00 54.67 109
cis-1.2-Dichloroethene ug/kg 50.00 54.39 109
trans-1.2-Dichloroethene ug/kg 50.00 53.73 107
2-Dichioropropane ugIkg 50.00 54.48 109
13Dichloropropane ug/kg 50.00 52.93 106
2.2-Dichioropropane ug/kg 50.00 53.83 108
1.1-Dichioropropene ug/kg 50.00 55.32 111
cis-1.3-Dichloropropene ug/kg 50.00 50.60 101
trans-1.3-Dichloropropene ug/kg 50.00 50.32 101
Dilsopropyl ether ug/kg 50.00 58.44 117
Ethylbenzene ug/kg 50.00 51.51 103
Hexachloro-13-butadiene ug/kg 50.00 55.96 112
2-Hexanorie ug/kg 100.00 103.3 103
Isopropylbenzene Cuinene ug/kg 50.00 55.83 112
p-Isopropyltoluene uglkg 50.00 49.83 100
Hethylene chloride ug/kg 50.00 58.53 117
4-Methyl -2-pentanone MIBK ug/kg 100.00 102.1 102
t4ethyl-tert-butyl ether ug/kg 50.00 55.47 1.1
Naphthalene ug/kg 50.00 47.66 95
n-Propylbenzene ug/kg 50.00 55.45 111
Styrene ug/kg 50.00 51.04 102
111.2-Tetrachloroethane uglkg 50.00 53.59 107
11.2.2-Tetrachloroethane ug/kg 50.00 52.11 104
Tetrachioroethene ug/kg 50.00 50.97 102
Toluene ug/kg 50.00 50.62 101
123-Trichlorobenzene ugfkg 50.00 49.35 99
12.4-Trichlorobenzene uglkg 50.00 4627 92
1.11-Trichioroethane ug/kg 50.00 54.43 109
1.12-Trichloroethane ug/kg 50.00 51.95 104
Trichioroethene ug/kg 50.00 4928 99
Trichlorofluoromethane ug/kg 50.00 47.86 96
1.2.3-Trichloropropane ug/kg 50.00 56.47 113
1.24-Triniethylbenzene ug/kg 50.00 48.65 97
1.35-Trimethylbenzene ug/kg 50.00 50.09 100
Date 03/29/05
Page 67 of 79
Parameter
Benzene
Chlorobenzene
1-Dichloroethene
Toluene
Tn chl oroethene
Toluene-d8
4-Brornoll uorobenzene
Di broiiiof uoromethane
1.2-Dichloroethane-d4
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REPORT OF LABORATORY ANALYSIS
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SC 99006
Analytical
www.pacelabs.com QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE 925415440
Spike
Conc
100 00
50.00
150.00
100.00
50.00
LCS
Result
20.91
51.52
153.8
101.6
52.19
Parameter Units
Vinyl acetate ug/kg
Vinyl chloride ug/kg
Xylene Total ugf kg
mp-Xylene ugf kg
oXylene ug/kg
Toluene-d8 100
4-Bromofluorobenzene 94
Dibromofluoromethane 106
1.2-Dichloroethane-d4 99
LCS
Rec Footnotes
21
103
103
102
104
MATRIX SPIKE 925429748
925409534 Spike MS MS
Units Result Conc Result Rec Footnotes
ug/kg 48.47 47.82 99
ug/kg 48.47 48.22 100
ug/kg 48.47 48.45 100
ug/kg 48.47 47.40 98
ugfkg 48.47 46.74 96
SAMPLE DUPLICATE 925429730
100
98
102
95
925399768 DUP
Parameter Units Result Result RPD
Acetone ug/kg ND ND NC
Benzene ug/kg ND ND NC
Broniobenzene ug/kg ND ND NC
Bromochioromethane ug/kg ND ND NC
Bromodichloromethane ug/kg ND Nil NC
Bromoform ug/kg ND ND NC
Bromouiethane ug/kg ND ND NC
Footnotes
Date 83/29/05
Page 68 of 79
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iri Ar rn-nAn
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services Inc
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Phone [phone]
Fax [phone]
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
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Analytical
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Footnotes
SAMPLE DUPLICATE 925429730
925399768 DUP
Parameter Units Result Result RPD
2-Rutanone MEK ug/kg ND ND NC
n-Butylbenzene ug/kg ND ND NC
sec-Butylbenzene ug/kg ND ND NC
tert-Butyibenzene ug/kg ND ND NC
Carbon tetrachlorjde ug/kg ND ND NC
Chlotcbenzene ug/kg ND ND NC
Chioroethane ug/kg ND ND NC
Chloroform ug/kg ND ND NC
Chloromethane ug/kg ND ND NC
2-Chlorotoluene ug/kg ND ND NC
4-Chlorotoluene ug/kg ND ND NC
l2-Dibromo-3-chloropropane ug/kg ND ND NC
Dibromochioromethane ug/kg ND ND NC
1.2-Dibromoethane EDB ug/kg ND ND NC
Dibromomethane ug/kg ND ND NC
1.2-Dichlorobenzene ug/kg ND ND NC
13-Dichlorobenzene ug/kg ND ND NC
14-Dichlorobenzene ug/kg ND ND NC
Dichlorodifluoromethane ug/kg ND ND NC
1j-Dichloroethane uglkg ND ND NC
1.2-Dichloroethane ug/kg ND ND NC
il-Dichioroethene ug/kg ND ND NC
cis-l2-Dichloroethene ug/kg ND ND NC
trans-12-Dichloroethene ug/kg ND ND NC
1.2-Dichloropropane ugfkg ND ND NC
1.3-Dichloropropane ug/kg ND ND NC
22-Dichloropropane uglkg ND ND NC
1J-Dichloropropene ug/kg ND ND NC
cis-1.3-Dichloropropene ug/kg ND ND NC
trans-13-Dichloropropene ug/kg ND ND NC
Diisopropyl ether ug/kg ND ND NC
Ethyl benzene ug/kg ND ND NC
I-iexachloro-l3.butadiene ug/kg ND ND NC
2-Hexanone ug/kg ND ND NC
Isopropylbenzene Cumene ug/kg ND ND NC
p-Isopropyltoluene ug/kg ND ND NC
Methylene chloride ug/kg ND ND NC
Date 03129/05
Page 69 ol 79
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Analytical
www.pacelabs.com QUALITY CONTROL DATA
SAMPLE DuPLICATE 925429730
Pace Analytical Services Inc
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Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
925399768 DIJP
Parameter Units Result Result RPD Footnotes
4-Methyl -2-pentanoneP4IBK ug/kg ND ND NC
Methyl -tert-butyl ether ug/kg ND ND NC
Naphthalene ug/kg ND ND NC
n-Propylbenzene uglkg ND ND NC
Styrene ug/kg ND ND NC
111.2-Tetrachloroethane ug/kg ND ND NC
ug/kg ND ND NC
Tetrachloroethene ug/kg ND ND NC
Toluene uglkg ND ND NC
123-Trichlorobenzene ugfkg ND ND NC
12.4-Trichlorobenzene ug/kg ND ND NC
11.1-Trichioroethane ug/kg ND ND NC
112-Trichloroethane ug/kg ND ND NC
Trichloroethene ug/kg ND ND NC
Trichiorofluoromethane ug/kg ND ND NC
1.2.3-Trichloropropane ug/kg ND ND NC
1.24-Trimethylbenzene ug/kg ND ND NC
1.3.5-Trimethylbenzene ug/kg ND ND NC
Vinyl acetate ugf kg ND ND NC
Vinyl chloride ug/kg ND ND NC
Xylene Total ug/kg ND ND NC
mp-Xylene ug/kg ND ND NC
o-Xylene ug/kg ND ND NC
Toluene-d8 CS 98 100
4-Bromofluorobenzene 87 98
Dibromofluoromethane CS 101 97
12-Dichloroethane-d4 97 97
Date 03129/05
Pago 70 of 79
Pace Analytical Services Inc
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Ashevifle Certification lOs
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SC Environmental 99038
ri Mn rn-ran
REPORT OF LABORATORY ANALYSiS
This report shall not be reproduced except in lull
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co
Charlotte Certification lOs
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Analytical
www.pacelabs.com QUALITY CONTROL DATA
METHOD BLANK 925425175
Associated Lab Samples 925409708
QC Batch 124167 Analysis Method EPA 8260
QC Batch Method EPA 826O Analysis Description GC/MS VOCs 5035/8260 low level
Associated Lab Samples 925409708
Footnotes
Blank Reporting
Parameter Units Result Limit
Acetone ug/kg ND 100
Benzene ug/kg ND 5.0
Bromobenzene uglkg ND 5.8
Broniochloromethane ug/kg ND 5.0
Bromodichloroniethane ug/kg ND 5.0
Bromoform ug/kg ND 5.0
Bromomethane ug/kg ND 10
2-Butanone MEK ug/kg ND 100
n-Butylbenzene ug/kg ND 5.0
sec-Butylbenzene uglkg ND 5.0
tert-Butylbenzene uglkg MD 5.0
Carbon tetrachlorjde ug/kg ND 5.0
Chlorobenzene ug/kg ND 5.0
Chloroethane ug/kg MD 10
Chloroform ug/kg ND 5.0
Chioroniethane ug/kg ND 10
2-Chlorotoluene ug/kg ND 5.0
4-Chiorotoluene ug/kg ND 5.0
1.2-Dibromo-3-chloropropane ug/kg ND 5.0
Dibromochioromethane ug/kg ND 5.0
12-Dibromoethane EDB ug/kg ND 5.0
Dibromometharie ug/kg MD 5.0
1.2-Dichlorobenzene ug/kg MD 5.0
13-Dichlorobenzene uglkg ND 5.0
14-Dichlorobenzene uglkg MD 5.0
Dichlorodifluoromethane ug/kg ND 10
1.1-Dichloroethane ug/kg MD 5.0
12-Dichloroethane ug/kg ND 5.0
1.1-Dichloroethene ug/kg ND 5.0
cis-12-Dichloroethene ug/kg ND 5.0
trans-12-Djchloroethene ug/kg ND 5.0
Date 03/29/05
Page 71 of 79
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SC Environmental 99030
REPORT OF LABORATORY ANALYSIS
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I_CCO
Charlotte Certification IDs
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SC 99006
ce Analytical
www.pacelabs.com
925409706
QUALITY CONTROL DATA
METHOD BLANK 925425175
Associated Lab Samples
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
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Footnotes
Blank Reporting
Parameter Units Result Limit
12-Dichioropropane ug/kg MD 5.0
1.3-Dichioropropane ügfkg ND 5.0
2.2-Dichlocopropane ug/kg ND 5.0
1.1-Dichioropropene ug/kg MD 5.0
cis-1.3-Dichloropropene uglkg ND 5.0
.Htrans.13.Dichloroproperie ug/kg MD 5.0
Diisopropyl ether uglkg ND 5.0
Ethylbenzene ug/kg ND 5.0
Hexachloro-13butadiene uglkg ND 5.0
2-Hexanone ug/kg ND 50
Isopropylbenzene Cumene uglkg ND 5.0
p-Isopropyltoluene ug/kg ND 5.0
Methylene chloride ug/kg MD 5.0
4-Methyl -2-pentanone MIBK ug/kg ND 50
Methyl-tert-butyl ether ug/kg ND 5.0
Naphthalene ug/kg ND 5.0
n-Propylbenzene ug/kg ND 5.0
Styrene ug/kg ND 5.0
1112-Tetrachloroethane uglkg ND 5.0
1.1.2.2-Tetrachloroethane ug/kg ND 5.0
Tetrachloroethene uglkg ND 5.0
Toluene ug/kg ND 5.0
1.2.3-Trichlorobenzene ug/kg ND 5.0
l24-Trichlorobenzene ug/kg ND 5.0
1.11-Trichloroethane ug/ky ND 5.0
112-Trichloroethane ug/kg ND 5.0
Trichloroethene uglkg ND 5.0
Trichlorofluorometharie ug/kg ND 5.0
1.2.3-Trichloropropane ug/kg ND 5.0
12.4-Trimethylbenzene ug/kg ND 5.0
l.35-Trimethylbenzene ug/kg ND 5.0
Vinyl acetate ugf kg ND 50
Vinyl chloride ug/kg ND 10
Xylene Total ug/kg ND 5.0
mp-Xylene ug/kg ND 10
o-Xylene ug/kg ND 5.0
Date 03/29/05 Page 72 of 79
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
METHOD BLANK 925425175
Associated Lab Samples 925409708
Blank Reporting
Parameter Units Result Limit Footnotes
Toluene-d8 100
4-Bromofluorobenzene 98
Dibromofluoromethane 103
12Dichloroethaned4 103
LABORATORY CONTROL SAMPLE 925425183
Asheville Certification lBs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
11 MI P7AP
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
Charlotte Certification IDs
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SC 99006
Analytical
wvw.pacelabscom QUALITY CONTROL DATA
Footnotes
Spike LCS LCS
Parameter Units Conc Result tRec
Acetone ug/kg 100.00 114.5 115
Benzene ug/kg 50.00 48.68 97
Bromobenzene ug/kg 50.00 50.65 101
Bromochloromethane ug/kg 50.00 50.28 101
Bromodichioromethane ug/kg 50.00 49.01 98
Bromoform ug/kg 50.00 51.85 104
Bromomethane ug/kg 50.00 45.75 92
2-Butanone MEK ugfkg 100.00 94.15 94
n-Butylbenzene ug/kg 50.00 42.57 85
sec-Butylbenzene ug/kg 50.00 49.16 98
tert-Butylbenzene ug/kg 50.00 49.46 99
Carbon tetrachioride ug/kg 50.00 49.79 100
Chlorobenzene ug/kg 50.00 48.93 98
Chioroethane ug/kg 50.00 55.19 110
Chloroform ug/kg 50.00 51.40 103
Chloromethane ug/kg 50.00 42.82 86
2-Chlorotoluene ug/kg 50.00 48.88 98
4-Chiorotoluene ug/kg 50.00 48.96 98
l.2-Dibromo-3-chloropropane ug/kg 50.00 47.08 94
Dibroinochlorometliane ug/kg 50.00 48.08 96
12-Dibromoethane EDB ug/kg 50.00 49.12 98
Dibromomethane ug/kg 50.00 51.59 103
1.2-Dichlorobenzene ug/kg 50.00 50.09 100
1.3-Dichlorobenzene ug/kg 50.00 47.47 95
14-Dichlorobenzene ug/kg 50.00 48.14 96
Dichlorodjfluoromethane ug/kg 50.00 42.05 84
Date 03/29/05
Page 73 of 79
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
1.1-Dichioroethane
.2-Dichloroethane
1.1 -Dichloroethene
ci s-i 2-Di chioroethene
trans-i .2-Dichl oroethene
2-Dtchloropropane
1.3-Dichloropropane
2.2-Dichloropropane
1-Dichloropropene
cis-13-Dichloropropene
trans-1.3-Dichloropropene
Diisopropyl ether
Ethyl benzene
2-Hexanone
Isopropyl benzene Cumene
p-Isopropyltoluene
Methyl ene chloride
4-Methyl -2-pentanone MIBK
Methyl -tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
11 1.2 -Tetrachl oroethane
1.12 2-Tetrachl oroethane
Tetrachloroethene
Toluene
1.23-Trichlorobenzene
2.4-Trichlorobenzene
1-Trichloroethare
1.1 2-Trichloroethae
Tn chi aroethene
Trichi oro-fi uoromethane
1.203 -Tn chi oropropane
4-Tn methyl benzene
1.35 -Tnimethyl berizene
Vinyl acetate
REPORT OF LABORATORY ANALYSIS
Asheville Certification Os This report shall not be reproduced except in full Charlotte Certification lOsNCWastewater40without the written consent of Pace Analytical Services Inc NC Wastewater 12NCDrinkingWater37712to4NCDrinkingWater37706SCEnvironmental99030
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rce Analytical
www.pacelabs.com QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
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Phone [phone]
Fax [phone]
LABORATORY CONTROL SANPLE 925425183
Paramtr Spike LCS LCS
Units Conc Result XRec Footnotes
ug/kg 50.00 49.82 100
ug/kg 50.00 47.50 95
ug/kg 50.00 49.68 99
ug/kg 50.00 49.81 100
ug/kg 50.00 49.11 98
uglkg 50.00 51.22 102
uglkg 50.00 47.51 95
uglkg 50.00 44.61 89
ug/kg 50.00 48.42 97
uglkg 50.00 49.73 100
ug/kg 50.00 49.8O 100
uglkg 50.00 52.87 106
ug/kg 50.00 47.65 95
ugikg 50.00 49.79 100
ug/kg 100.00 101.3 101
ug/kg 50.00 52.00 104
ug/kg 50.00 43.37 87
ug/kg 50.00 49.23 98
ug/kg 100.00 106.0 106
uglkg 50.00 49.90 100
uglkg 50.00 43.95 88
ugfkg 50.00 48.97 98
uglkg 50.00 48.40 97
uglkg 50.00 45.80 100
uglkg 50.00 47.84 96
ug/kg 50.00 45.90 92
ug/kg 50.00 47.51 95
ug/kg 50.00 48.28 97
ug/kg 50.00 46.44 93
ug/kg 50.00 48.61 97
ug/kg 50.00 50.20 100
ug/kg 50.00 47.40 95
uglkg 50.00 44.55 89
uglkg 50.00 48.26 96
ug/kg 50.00 43.93 88
ug/kg 50.00 44.93 90
uglkg 10000 102.2 102
Date 03129105
Page 74 of 79
LABORATORY CONTROL SAMPLE 925425183
Parameter
Vinyl chloride
Xylene Total
mp-Xylene
o-Xylene
Toluened8
4-Bromofluorobenzene
.Oibromofluoromethane
12-Oichloroethane-d4
Pace Analytical Services Inc
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MC tO7AO
REPORT OF LABORATORY ANALYSIS
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Analytical
www.pacelabs.com QUALITY CONTROL DATA
Units
ug/kg
ug/kg
ug/kg
ug/kg
Spike
Conc
50.00
150.00
100.00
50.00
LCS
Result
46.84
144.4
95.03
49.40
LCS
Rec Footnotes
94
96
95
99
100
98
101
102
Date 03/29/05 Page 75 of 79
QUALITY CONTROL DATA
METHOD BLANK 925415598
Associated Lab Samples 925409500 925409518 925409534
Lab Project Number 9290353
Client Project ID West End 6228-05-2694
Blank Reporting
Result Limit Footnotes
ND 0.20
ND 0.50
LABORATORY CONTROL SAMPLE 925415606
Spike LCS LCS
Parameter Units Conc Result Rec Footnotes
Chromium mg/kg 50.00 45.50 91
Lead mg/kg 50.00 42.50 85
MATRIX SPIKE MATRIX SPIKE DUPLICATE 925415614 925415622
925410748 Spike MS MSD MS 1150
Parameter Units Result Conc Result Result tRec tRec RPD Footnotes
Chromium mg/kg 3.900 71.74 64.04 53.87 84 77 17
Lead mg/kg 1.718 71.74 57.52 54.00 78 80
SAMPLE DUPLICATE 925415986
Parameter
Chromium
Lead
925410755
Result
3.400
1.500
Result RPD Footnotes
3.000 12
2.200 41
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REPORT OF LABORATORY ANALYSIS
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ce Analytical
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Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
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Phone [phone]
Fax [phone]
QC Batch 123978 Analysis Method EPA 6010
QC Batch Method EPA 3050 Analysis Description Metals Trace ICP
Associated Lab Samples 925409500 925409518 925409534
Paraieter
.Chromi urn
Lead
Units
mg/kg
mg/kg
Units
mg/kg
mg/kg
DtJP
Date 03/29/05
Page 76 of 79
Asheville Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
CI MCI lb CC7CAO
Pace Analytical Services Inc
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ace AnaIicaI
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Lab Project Number 9290353
Client Project ID West End 6228-05-2694
QC Batch 123921 Analysis Method Moisture
QC Batch Method Analysis Description
Percent Moisture
Associated Lab Samples 925409500 925409518 925409534 925409575 925409583
925409591 925409609 925409617 925409625 925409633
925409641 925409658
SAMPLE DUPLICATE 925413098
.JParameter
Percent Moisture
Date 03/29/95
925407645 DUP
Units Result Result RPD Footnotes
19.40 20.00
REPORT OF LABORATORY ANALYSIS
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Charlotte Certification Ds
NC Wastewater
NC Drinking Water
SC
12
37706
99006
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290353
Client Project ID West End 6228-052694
Asheville Certification
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
tlCI CO7CAo
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services Inc
fl ACC0
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
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ceAnaiytical
www.pacelabs.com QUALITY CONTROL DATA
tIC Batch 123929 Analysis Method Moisture
QC Batch Method Analysis Description Percent Moisture
Associated Lab Samples 925409666 925409674 925409682 925409690 925409708
925409716 925409724
925413270
Units
925409666 DUP
Result Result EE
12.40 19.70 46
Footnotes
SAMPLE DUPLICATE
Parameter
Percent Moisture
Sate 03/29/05
Page 78 of 79
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Consistent with EPA guidelines unrounded concentrations are displayed and have been used to calculate Rec and RPD values
Laboratory Control Sample Duplicate
Matrix Spike Duplicate
Sample Duplicate
Not detected at or above adjusted reporting limit
Not Calculable
Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
Adjusted Method Detection Limit
Relative Percent Difference
Surrogate
The spike recovery was outside acceptance limits for the MS and /orMSD due to matrix interference The LCS
and/or LCSD were within acceptance limits showing that the laboratory is in control and the data is
acceptable
The calculated RPD was outside QC acceptance limits
The surrogate recovery was outside QC acceptance limits due to matrix interference
The surrogate and/or spike recovery was outside acceptance limits
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fl 1L lip 7tAn
REPORT OF LABORATORY ANALYSiS
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ace AnaIicar
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Pace Analytical Services Inc
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Lab Project Number 9290353
Client Project ID West End 6228-05-2694
LCSD
MS CD
DUP
ND
NC
.1
MDL
Date 03/29/05
Page 79 of 79
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l-Iuntersvile NC 28078
Phone [phone]
Fwc 704.875.9091
ltr Rob Foster
Mactac
2801 Yorkmont Road
SUite 100
Charlotte NC 28208
RE Lab Project Number 9290855
Client Project West End 6228-05-2694
Dear Mr Foster
Enclosed are the analytical results for samples received by the laboratory on March 25 2005 Results reportedhereinconformtothemostcurrentNELACstandardswhereapplicableunlessotherwisenarratedinthebodyofthereport
If you have any questions concerning this report please feel free to contact me
Sincerely
innette Scott
nnette.$cott@pacelabs .com
Project Manager
Enclosures
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shut not be reproduced except in tuft
without the written consent of Pace Analytical Services IncfC
CQfls.6Ditil
NC Wastewater 12
NC Drinking Water 377Q6
Sc 99006
FL OIELAP 87627
vmwyiacJabscom
Metals by Trace IC
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Date Digested
Mercury CVAAS in Water
Mercury
GC/MS Volatiles
GC/MS VOCs by 8260 low level
Benzene
Bromodjch1oromethe
Bromoform
Bromomethene
n-Butylbenzene
sec-ButyThenzene
Carbon tetrachiorjde
Chlorobenzeae
Chioroethane
Chloroform
Chioromethane
Dibromochloromethame
l2-Djbromoethane 8DB
12 -Dichlorobenzene
l3-Dichlorobenzene
4-Dich1orob
Dichlorodif1uorometne
i-Djchloroethane
l2-Dichioroethane
l-Dichloroethene
trans-l2-Djchloroethene12-Dichloropropaiie
Diisopropy ether
Prep/Method EPA 3010 EPA 6010
ND mg/i
0.077 mg/i
ND mg/I
ND mg/i
ND org/i
ND
ND
03/27/05 0020
Method EPA 7470
ND mg/i
03/29/05 1155 BCE
03/29/05 1155 BCE
03/29/05 1155 BCE
03/29/05 1155 BCE
03/29/05 1155 BCE
03/29/05 1155 BCE
03/29/05 1155 BCE
03/29/05 1155 BCE
03/29/05 1155 BCE
03/29/05 1155 BCE
03/29/05 1155 BCE
03/29/05 1155 BCE
1155
1155
1155
1155
1155
1155
1155
1155
1155
Pace Analytical Saivices his
9800 Kincey Avenue Suite 100
Iluntersville NC 28078
Phone[phone]
Fax [phone]
Date Collected 03/25/051155
Date Received 03/25/05 1320
7440-38-2
7440-39 -3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
1-43-2
75-274
75-25-2
74-839
104-51-8
13 5-98-8
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
12448-1
ion ID
NC WastewMer 40
NC Drinking Water 37712
SC Ezwironnienta 9N130
FL NEI.AP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be repreijucerl except hr lull
without the written consent of Pace Analytical Services Inc
NC Wastewater 12
NC Drhrldng Water 37706
SC 99006
FL NELAP E87027
www.pacelabs.com
Lab Sample No 925437352
Client Sample ID LAW
rameters
Metals
Lab Project Number 9290855
Client Project ID West End 6228-05-2694
Project Sample Number 9290855-001
Matrix Water
.._Results Units Renort Limit _P_Analyzed By CAS No QL Reg
0.0050
0.0050
0.0010
0020
050
0050
0.0020
sng/l
mg/i
1.003/3l/05 1834 ALV
1.0 03/31/05 1834 ALV
1.0 03/31/05 1834 ALV
1.0 03/31/05 1834 ALV
1.0 03/31/05 1834 ALV
1.0 03/31/05 1834 ALV
1.0 03/31/05 1834 ALV
03/27/05 0020
0.00020 1.0 03/31/05 0700 ALV 7439-97-6
Method EPA
ND
ND
ND
ND
ND
NDND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
8260
rig/i
ugh
ug/1
ugh
rig/i
ugh
rig/i
ug/1
ugh
rig/i
rig/i
ug/l
ug/l
ugh
ug/i
rig/i
ug/l
ug/l
ug/l
rig/i
ug/1
rig/i
rig/i
1.0
1.0
1.0
10
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
1.0
10
1.0
1.0
1.0
1.0
1.0 03/29/05
1.0 03/29/05
1.0 03/29/05
1.0 03/29/05
1.0 03/29/05
1.0 03/29/05
1.0 03/29/OS
1.0 03/29/05
1.0 03/29/05
03/29/05 1155 BCE 106-93-4
03/29/05 1155 BCE 95-50-1
Date 04/01/09
BCE 541-73-1
BCE 106-46-7
BCE 75-71-8
BCE 75-34-3
BCE 107-06-2
BCE 75-35-4
BCE 156-60-5
BCE 78-87-5
BCE 108-20-3
Page of 25
Ethylbenzene
Iaopropylbenzene Cumene
p-Isopropyltoluene
Methylene chloride
Methyl-tert-butyl ether
Napbthalena
n-Propylbenzene
112 2-Tetrachloraethane
Tetrachioroethene
Toluene
11 1-Trichioroethame
112 -Trichloroethane
Trichloroethene
Trich1orof1uoromethe
l.24-Trimethylbenzene135-Trimethylbenzene
Vinyl chloride
Xylene Total
flLp-Xylene
o-Xylene
Toluene-dS
-Bromofluorobenzene
Dibromofluoromethe
12 -Dichloroetbane-d4 IS
Results Units
ND ug/l
1W up/i
ND up/i
ND ugh
ND ug/l
ND up/i
ND up/i
ND up/i
ND ug/l
ND up/i
ND up/i
ND ugh
ND up/i
ND up/i
ND ugf
ND up/i
ND up/i
ND ugh
ND ugh
ND ugh
100
94
95
87
1.0 03/29/05 1155 BCIC
1.0 03/29/05 1155 ECK
1.0 03/29/05 1155 BCK
1.0 03/29/05 1155 BCK
1.0 03/29/05 1155 BCK
1.0 03/29/05 1155 BCK
1.0 03/29/05 1155 ECK
1.0 03/29/05 1155 OCX
1.0 03/29/05 1155 OCX
1.0 03/29/05 1155 OCX
1.0 03/29/05 1155 OCX
1.0 03/29/05 1155 OCX
1.0 03/29/05 1155 OCX
1.0 03/29/05 1155 OCX
1.0 03/29/05 1155 OCX
1.0 03/29/05 1155 BCK
1.0 03/29/05 1155 OCX
1.0 03/29/05 1155 OCX
1.0 03/29/05 1155 OCX
1.0 03/29/05 1155 OCX
1.0 03/29/05 1155 OCX
1.0 03/29/05 1155 OCX
1.0 03/29/05 1155 OCX
1.0 03/29/05 1155 OCX
100-41-4
8-82-8
99-876
75-09-2
1634-04-4
91-20-3
10365-i
79-34-5
127184
10888-3
1-556
79-00-5
79-01-6
75-69-4
95-63-6
108-67-8
75-01-4
1330-20-7
95-47-6
037-26-5
60004
18 68-53-7
17 06007-0
QiL RegLort
Data 04/01/05
AshoilleCertification lOs
NCWastewater 40
NC Drinking Water 37712
Sc Environmental 99030
FL IIEI.AP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in lull
without the written consent of Pace Malytical Services Inc
tItilDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
Page of 25
AnaiyticaI
wwpaoelabncorn
Lab Sample No 925437352
Client Sample ID LAW
Pace Analytical Services inc
9800 KioceyAvenue Suite 100
fluntersvlle NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290855
Client Project ID West End 6228-05-2694
Project Sample Number 9290855-001
Matrix Water
Report Limit DF Analyzed By CAS No
Date Collected 03/25/05 1155
Date Received 03/25/05 1320
1.0
1.0
2.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
Pace Analytical Satvices Inc
9800 KinceyAvenue Suite 100
Analyticar iluntrs v/lie NC 280 78
Phone [phone]JS.COlfl
Fax [phone]
Lab Project Number 9290855
Client Project ID West End 6228-05-2694
PARMETER FOOTNOTES
Dilution factor shown represents the factor applied to the reported result and reporting limit due to changesinsamplepreparationdilutionoftheextractormoisturecontent
Inorganic Wet Chemistry and Metals Inalyses were performed at our Pace Asheville laboratory and OrganictestingwasperformedatourPaceCharlottelaboratory unless otherwise footnoted
Method 9071B modified to use ASE
All pa Free Chlorine Total Chlorine and Ferrous Iron analyses conducted outside of EPlvrecoumiended imxnediteholdtime
ND Not detected at or above adjusted reporting limitNCNotCalculable
Estimated concentration above the adjusted method detection limit and below the adjusted reporting limitMDLAdjustedMethodDetectionLimit
Surrogate
Date 04/01/05
Page of 25
REPORT OF LABORATORY ANALYSIS briotkiVfitilNCWastewater40
This report shall cotta reproduced except in NC Watewater 12NCDrinking Water 37712
wittiest the written consent of Pace NC Drinking Water 37706SCEnvironmental99030SC99006FlNELAPE87648
FL NELAP E87627
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 KincoyAvenue Suite 100
Huntersville NC 28078
Phone [phone]
Fax 704.8 75 ..G 091
Lab Project Number 9290855
Client Project ID West End 6228-05-2694
QC Batch 123935 Analysis Method EPH
QC Batch Method EPA 3510 Ailalysis Description EPH in Water by Mass Method
Associated Lab Samples 925437360
METEOD BLANK 925447922
Associated Lab Samples 925437360
Blank ReportingParameterUnitsResultLimit Footnotes
Aliphatic 1C09-C18 ugh ND 100
Aliphatic C19C36 ugh ND 100
Aromatic C11-22 ugh ND 100
2-Fluorobiphenyl 72
2-Bromonaphthalene 95
Nonatrjacontane 43
o-Terphenyl 94
LABORATORY CONTROL SAMPLE 925413403
Spike LCS LCS
Parameter Units Conc Result Footnotes
Aliphatic C09-C18 rig/i 300.00 139.3 46
Aliphatic C19-C36 ugh 400.00 396.5 99Aromat.c Cll-22 ugh 850.00 459.6 54
Nonatriacontane 122
o-Terphenyl 86
LABORATORY CONTROL SAMPLE 925447930
Ashevifte Certification lOs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except In full
without the written consent of Pace Analytical Services Inc
Chalotte Certification lOs
liCWaStewater 12
NC Drinking Water 37706
SC 99006
FINELAP E87627
Prnmn4r Spike LCS LCS
Aliphatic C09-C18
Alipbatic C19 -C36
Aromatic C1i-22
-Fluorobiphenyl
2-Bromonaphthalane
Nonatriacontane
o-Terphenyl
Date 04/0./05
Units Conc Result %Rec Footnotes
up/I 300.00 193.2 64
ug/l 400.00 387.5 97
ug/l 850.00 486.0 57
55
65
47
79
Page 29
Unite
tug/i
up/i
ug/
tug/i
tug/i
tug/i
up/i
up/i
tug/i
tug/i
ugh
ugh
QUALITY CONTROL DATA
Blank
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
100
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
Pace Analytical Services Inc
9800 KinceyAveniie Suite 100
Huntersville NC 28078
Phone [phone]
Fax [phone]
NC Wastewttter 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced except In tot
without the written consent of Pace Malytical Services Inc
SIC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NEIAP E87827
wwwpacelabs.com
Lab Project Number 9290855
Client Project ID West End 6228-05-2694
METhOD BLANK 925439150
Associated Lab Samples
QC Batch 124387 Analysis Method EPA 602
QC Batch Method EPA 602 Analysis Description Purgeabie Aromatics
Associated Lab Samples 925437360
925437360
Reporting
Limit Footnotes
1.0
Parameter
Benzena
Chiorobenzeae
i2-Dichlorobenzene
-Dichiorobeazena
4-Dichiorobenzene
Diisopropyl ether
Ethytheazene
Methyl tert-butyl ether
Toluene
Xylene Total
m$cp-Xyiene
o-Xyiene
i-Chioro-3-fluorobenzene
LABORATORY CONTROL SAMPLE 925439168
Spike LCS LCSarameterUnitsCoric
Bezene ugh 20.00 19.80 99Chiorobenzenetug/i 20.00 20.47 102l2-Dichiorobenzene ugh 20.00 21.23 106l3-Dichlorchenzene ugh 20.00 19.36 97i4-Dichlorobenzene tug/i 20.00 20.98 105
Diisopropyl ether ugh 20.00 19.60 98Ethylbenzeneug/l 20.00 21.48 107
Methyi.tert-butyl ether tug/i 20.00 21.50 108Tolueneup/i 20.00 20.83 104XyleneTotaltug/i 60.00 64.15 107mp-Xylene tug/i 40.00 43.02 108o-Xyiene tug/i 20.00 21.13 106
Footnotes
Date 04101/05
Pagei of 25
Pace Analytical Services Inc
9800 KiaceyAveniie Suit8 100
Huntersville NC 28078
Phone [phone]wWwpaceIabscomFax704.875.9091
QUALITY CONTROL DATA
Lab Project Number 9290855
Client Project ID West End 6228-05-2694
LAEORATQRY CONTROL SAMPLE 925439168
Spike LCS LCS
Parameter Units Cone Result F00tflote
l-Chioro-3-fluorobenzene 101
MATRIX SPIKE 925439176
925423493 Spike MS MS
Parameter Units Result Conc Result %Rec Pootnotes
Benzene ugh 20.00 19.72 99
Chlorobenzene ug/i 20.00 20.14 101l2-Dichiorobzene rig/i 20.00 20.66 103
l3-Djchlorobenzane ugh 20.00 17.18 86
i4-Djchiorobenzene ugh 20.00 20.23 101
Diisopropyl ether up/i 20.00 20.23 101
Ethyibenzene ugh 20.00 21.04 105
Methyi-tert-butyi ether ug/1 20.00 20.79 104Tolueneup/i 20.00 20.71 104
Xyiene Total rig/i 60.00 62.12 104
mp-Xyiene up/i 40.00 41.81 104
o-Xyiene up/i 20.00 20.31 102
l-Chloro-3-fiuorobenzene 99
MATRIX SPIKE 925439184
925432494 Spike MS MS
pits Result Cone Result %Rec PootnoteaBonzeneup/i 20.00 19.75 99Chlorohenzeneup/i 20.00 20.14 101l2-Dichlorobenzene up/i 20.00 20.75 104i3-Djchlorobenzene up/i 20.00 20.76 104i4-Dichlorobenzene up/i 20.00 20.32 102
Diisopropyi ether ug/i 20.00 19.95 100
Ethylbenzena rig/i 20.00 21.15 106Methyl-tert-butyl ether up/i 20.00 20.84 104Tolueneup/i 20.00 20.76 104XyieneTotalup/i 60.00 62.75 105mp-Xyiene up/i 40.00 42.10 105
hate 04/01/05
Page of 25
h5hntIIpfjonjQ REPORT OF LABORATORY ANALYSIS hottCeriuticafinofNCWastewater40ThisreportshallnottierisceriexceptinNCWastewater 12NCDrinking Water 37712 wfliit the written consent of Pace ieraiyticai senices Inc
NC Drinking Water 37706SCEnvrronmntal99030SC99006FLNELAPE87648FLNELAP687627
.Arialyticar
wwwpacelahscom
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hnteisville NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290855
Client Project ID West End 6228-05-2694
MATRIX SPIKE 925439184
925432494 Spike MS MSParameterUnitsResultConcResult%Rec Pootsioteso-Zyiene up/i 20.00 20.65 103i-Chioro-3-fluorobenze 99
SAMPLE DUPI.ICATE 925439192
NC Wastewater 40
NC Drinking Water 37712
SC Envfronnnental 99030
FL bRiAR E87648
REPORT OF LABORATORY ANALYSIS
Tins report strati not be reprorluced except In tint
without the written consent of Pace Analytical Services Inc
it
NCWatitewater 12
NC Drinking Water 37706
SC 99006FLNELPE87627
925432510 DUP
Result ResultParameterUnit
Beazene up/i 32.00 33.00
Chiorobensena ugh ND ND
l2-Dichlorobenzene up/i ND ND
l3-Dichlorobenzene up/i ND NDl4-Dichlorobenzena ugh ND NI
Diisopropyi ether up/i ND ND
Ethyibexrzene up/i 2.700 2.800
Methyl-tert-butyi ether up/i 12.00 14.00Tolueneup/i ND ND
Xyiene Total ugh 110.0 110.0
mp-Xylene ugh 68.00 70.00o-Xyiene up/i 40.00 41.00l-Chioro-3-fluorobenzene 98 99
fl Footsiotes
NC
NC
NC
NC
NC
ii
NC
Date O4/O/O5
Page 10 oti 25
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Jluntejsvlle NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290855
Client Project ID West End 6228-05-2694
QC Batch 124472 Analysis Method VPR
QC Batch Method VPH Analysis Description VPR in Water by Mass MethodAssociatedLabSamples925437360
METHOD BUNK 925442212
Associated Lab Samples 925437360
Parameter
Aliphatic C05-C08
Aliphatic C09-C12
Aromatic C09-Cl0
25-Dibromotoluane FIn
25-Dibromotaluene PID
Units
up/i
ugh
up/i
105
LABORATORY CONTROL SAMPLE 925442220
Aliphatic C05-C08
Aliphatic C09-C12
Aromatic C09-C10
25-Dibromotoluane FID
25-Djbromotoiuene PIn
Spike LCS
Result
400.00 391.8
100.00 99.94
100.00 104.8
LCS
Rec
98
100
105
136
132
if ion ID
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 00630
FL NELAI E87648
REPORT OF LABORATORY ANALYSIS
This report shall riot be meprodeceit except
in full
wdhout the written consent of Pace Malytical Services Inc
Ch0QuLC6tI6itins
NC Wastewater 12
NC Drinking Water 37706
S.C 99006
FLNELAP E87627
Blank
Result
ND
ND
ND
110
Reporting
Limit Footnotes
100
100
100
Units
up/i
up/i
up/i
Footnotes
Date 04/01/05
Pages 11 of 25
Analyticar
www.paceIabscom
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunters yule NC 28078
Phone [phone]
Far 7048759091
Lab Project Number 9290855
Client Project ID West End 6228-05-2694
QC Batch 124516 Analysis Method EPA 625
QC Batch Method EPA 625 SF Analysis Description Extractables in Water by 625AssociatedLabSamples925437360
METHOD BLANK 925443848
Associated Lab Samples
ejjonl
NC Wastewater 40
NCDiinking Water 37712
SC Environrne 99030
FL NELAP E87048
REPORT OF LABORATORY ANALYSIS
This report shall not be repmdueed except in full
without the written consent of Pace Analytical ServIces Inc
NC Wastewater 12
NC Drinking Water 37706
SC 99006
ft NELAP E87527
Footnotes
925437360
Blank ReportingParameterniteReBultLimit
Acenaphthene ugh ND 5.0
Acenaphthylene ug/l ND 5.0Anthracenetag/i ND 5.0
Benzidine tag/i ND 50Benzokflcjoranthaneup/i ND 5.0
Benzobfiuoranthene ugh ND 5.0
Benzoaanthracene up/i ND 5.0
Benzoghijperyiene -up/i ND 5.0Benzoapyreneug/i ND 5.0
4-Bromophenyiphenyl ether ugh ND 5.0
--Buty1benzyiphtiate ugh ND 5.0
4-Chioro-3-methylpheaol up/i ND 5.0his2-Ch1oroethoxymethe ugh ND 5.0
bis2-Chioroethyi ether up/i ND 5.0
bis2-Chioroisopropyj ether up/i ND 5.0
2-Chioronaphthalene ugh ND 5.02-Chiorophenol ug/l ND 5.0
4-Chlorophenyipheuyi ethsr up/i ND 5.0Chrysenetag/i ND 5.0Dibenzahantaceneup/i ND 5.0l2-Dicbiorobenze up/i liD 5.0
l3-Djchlorobenzene sag/i ND 5.0i4-Djchiorobenzene up/i ND 5.0i3-Dichiorobenzjdjne up/i ND 10
24-Dichlorophenol up/i ND 5.0Diethyiphthaiateup/i ND 5.0
24-Dimethyiphenol up/i ND 5.0Dimethylphthaiateup/i ND 5.0
Di-n-butyiphthajate up/i ND 5.0
i.6-Dinitro-2-methyiphenoi up/i liD 25
24-Diaiitrophenoi up/i ND 25
DOte 04/01/05
Page 12 of 25
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 KinceyAveniie Suite 100
Hunters yule NC 28078
Phone [phone]
Fax[phone]
METHOD BLANK 925443848
Associated Lab Sampiee 925437360
Lab Project Number 9290855
Client Project ID West End 6228-05-2694
24 -Dinitrotoluena
26 -Dinitrotoluene
Di -n-Octyiphthaiate
his 2-Ethyihexyi plithalate
Fluoranthene
Fluorene
Rexachioro-l -butadiene
Itezachiorobeozene
Hexachlorocycopentadiene
Reicachioreethane
Indenol2 -cdpyrene
Isophorone
Naphthaiene
Nitrobenzene
-Nitrophenol
4-Nitrophenol
N-Nitrosodiinethyiajnine
N-Nitroso-di-n-propyianaine
N-Nitrosodiphenylamine
Pentachlorophenoi
Phenanthrene
Phenol
Pyrene124-Trichlovobenzene
246 -Triclulorophenol
Nitrobenzene-d5
-Fluorobiphersyl
Terphenyi-d14
Phenol-d5
2-Fluorophenol246-Tribromophenoi
Reporting
Limit Footnotes
-5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
25
5.0
5.0
5.0
25
5.0
5.0
5.0
5.0
5.0
NC Wastewafer 40
NC Drinking Water 37712
SC Environmental 9030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
this report shall eat tin reproduced except in fat
without the written consent of Pace Analytical Services Inc
Olmrlotte Certification IDs
NOWatitewater 12
NC-Drinking Water 37706
SC 99006
FLNELAP E87627
Units
up/i
up/i
up/i
up/i
up/i
nip/i
up/i
ugh
up/i
up/i
ugh
up/i
ugh
up/i
up/i
up/i
ugh
ug/i
up/i
up/i
up/i
up/i
up/i
up/i
up/i
Biank
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
54
58
85
24
32
66
Date 04/01/05
Page 13 of 25
Pace Analytical Services Inc
9800 KinceyAveiiue Suite 100
Huntersville IC 28078
Phone [phone]wwwpacelabs.com Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9290855
Client Project ID West End 6228-05-2694
LABORATORY CONTROL SNPLE 925443830
Spike LCS LCS
Parameter Units Conc Result Footnotes
Acenaphthene up/i 50.00 26.57 53
Acenaphthyiene up/i 50.00 26.88 54
Anthracene ugh 50.00 39.07 78
Benzidine up/I 100.00 2.623
Benzokfluoranthene ugh 50.00 44.25 88
Benzobfluoranthene up/i 50.00 36.61 73
Benzoaanthracene up/i 50.00 40.56 81
Benzoghipery.ane up/i 50.00 42.10 84
Benzoapyrene up/i 50.00 39.75 80
4-Bromophenyiphenyl ether up/i 50.00 35.29 71
Butyibenzylphthalate up/i 50.00 41.28 83
4-Chioro-3-methylpheno up/i 50.00 28.26 56
bis2-Chioroethôymethame up/i 50.00 22.12 44
bis2-Chioroethy ether ugh 50.00 19.88 40
bis2-Chloroisopropyl ether up/i 50.00 21.32 43
2-Chioronaphthalene up/i 50.00 22.90 46
2-Chioropheno ugh 50.00 17.06 34
4-Chlorophenyipheny ether up/i 50.00 33.73 68
Chrysene up/i 50.00 39.41 79
Dibenzahanthracene ugh 50.00 41.17 82
i2-Dichiorobenzene ugh 50.00 17.87 36
l3-Dichiorobenzene up/i 50.00 16.77 34
i4-Dichlorobenzene up/i 50.00 17.27 34
3.3-Dichiorobenzjdjne up/i ioo.oo 33.78 34
24-Dichiorophenol up/i 50.00 21.51 43
Diethyiphthaiate up/i 50.00 40.90 82
2.4-Dimethy3.phenol up/i 50.00 23.71 47
Dimethyiphtha.ate up/i 50.00 37.80 76
Di-n-butyiphthaiate up/i 50.00 41.46 83
4E-Dinitro-2-methyipheno1 ug/i 50.00 62.9i 126
24-Dinitrophenol up/i 50.00 53.09 10624-Djnjtrotoiuene up/i so.oo 44.26 88
26-Dinjtrotoiuene up/i 50.00 39.14 78
Di-n-octyiphthalate up/i so.oo 41.32 83
bis2-Ethylhexylphthalate up/i 50.00 42.46 85Fluorantheneup/i so.oo 39.10 78Fiuoreneup/i so.oo 33.67 67
Date 04/01/05
Page 14 of 25
REPORT OF LABORATORY ANALYSIS XCethfkaflon DsNCWastewater40stiimproducIiiNCWaStewater12NCDrinkingWater37712wWioutthe written conseilt of Pace Malyticat Services
NC Drinking Water 37706SCEnvironmental99030..SC 99006FLNELAPE87648FLNELAPE87627
Pace Analytical Sarilces Inc
9800 KinceyAyenue Suite 100
Hunteisville NC 28078
Phone [phone]
Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9290855
Client Project ID West End 6228-05-2694
LABORATORY CONTROL SANPLB 925443830
Spike LCS LCS
Enjs Conc Result %Rec Pootnoteg
Ke2cachioro-i3-butadjene up/i 50.00 17.90 36
Bexachlorobenzene up/i 50.00 34.40 69
Rexachlorocyclopentadjene up/i 50.00 9.319 19
Hexachioroethane up/i 50.00 16.05 32
Indenol23-cdpyrene up/i 50.00 40.95 82
Isophorone up/i 50.00 24.67 49
Napbthalena up/i 50.00 19.15 38
Nitrobeuzene ug/50.00 21.05 42
2-Nitrophenol up/i 50.00 21.61 43
4-Nitrophenol up/i 50.00 16.58 33
N-Nitrosodimethyiamine up/i 50.00 14.66 29
N-Nitroso-di-12-prOpylamjne up/i 50.00 23.27 46
N-Nitroaodipheny.amina up/i 50.00 41.90 84
Pentachlorophenol up/i 50.00 47.08 94
Phenanthrene ugh 50.00 38.20 76
Phenol up/i 50.00 9.362 19
Pyrene up/i 50.00 41.01 82
l24-Trjchiorobenzene up/i 50.00 18.33 37
246-Trichiorophenol ugh 50.00 28.48 57
Nitrobenzene-d5 42
2-Fluorobiphenyl 48
Terphenyi-di4 85
Phenol-d5 19
2-Fluorophenoi 24
246-Tribromophenol 76
MATRIX SPIKE MATRIX SPIKE DUPLICATE 925443913 925443921
925427965 Spike MS MSD MS MSDParameterUnitsResultConeReu1tResult%Rec RPD FootntegAcenapbtheneup/i 100.00 65.64 68.53 66 68Acenaphthyieneup/i 100.00 66.02 68.67 66 69linthraceneup/i 100.00 86.61 85.45 87 86Benzokfluorantheneup/i 100.00 90.53 82.44 90 82Benzobf.uoranthene up/i 100.00 89.44 92.24 89 92Senzoaantbraceneup/i 100.00 83.75 79.34 84 79
Date 04/01/05
Page 15 of 25
hli1ooanj REPORT OF LABORATORY ANALYSIS i1otte Certification IDsNCWastewater40Thicreport shaft not roricceti except
ur ton NC Waxtewator 12NCDrinkingWater37712wIfltthewrittenconsentofPaceAnalytical Services IRS NC Drinking Water 37706SCEnvironmental99030....SC 99006FLNELAPE87648FLNELAPE87627
Analytical
wwwpacetabs.com
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 KincoyAvenue Suite 100
Hunters v/lie NC 28078
Phone [phone]
Fax [phone]
MATRIX SPIKE MATRIX SPIKE DUPLICATE 9254439.13 925443921
Lab Project Number 9290855
Client Project ID West End 6228-05-2694
SAMPLE DUPLICATE 925443871
Parameter
Acenaphthene
Acenaphthyiene
Anthracene
Eeuzo axithraaene
Benzo pyrene
Benzo fiuoraxsthene
Benzo gh iperyiene
Beuzo fluoraxsthene
Chrys ens
Dibenz ah anthracene
Fluoranthene
Fluorene
Indenoi23-cdpyrene
Naphthaiene
Phenanthreue
Pyrane
Nitrobenzene-dS
-Fluorobiphenyl
RPD Footnotes
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
10
NC
NC
lcnlD
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYStS
This report strut not be reproduced except in lull
without the wriften consent of Pace Analytical Services Inc
Caflf0ertifiopjg
NOWantewater 12
NC Drinking Water 37706
SC 99006
FL Ntl.AP E87627
Benzo ghi perylene
Benzo pyrene
Chrysene
Dibenz ah anthracene
Fluoranthene
Pluot-ene
Indeno12 3-cd pyrene
Naphthalene
Phenanthrene
Pyrene
Nitrobenzene-dS
-Fluorobiphenyl
Terphenyl-d14
Units Result
ugh
up/i
up/i
ug/l
up/i
up/i
ugh
up/i
up/i
up/i
925427965 Spike MS MSD MS MSD
Conc Result Result %Rec %Rec
100.00 60.96 55.22 61 55
100.00 89.90 85.88 90 86
100.00 84.89 80.73 85 81
100.00 65.01 58.30 65 58
100.00 8050 78.38 80 78
2.601 100.00 80.62 83.56 78 81
100.00 65.53 58.74 66 59
87.31 100.00 142.7 136.2 55 49
3.681 100.00 82.88 82.70 79 79
100.00 88.31 82.36 88 82
62 57
61 62
58 64
Footnotes
10
ii
ii
Units
ugh
up/i
ug/i
up/i
up/i
up/i
up/i
up/i
up/i
up/i
up/i
up/i
up/i
ugh
up/i
ugh
925427999 DUP
Result Result
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
26.00 28.00
ND ND
ND ND
48 53
55 54
Date 04/01/05
Page 16 of 25
Paca Analytical Satvicas Inc
9800 KinceyAvenue Suite 100
Huntuxsviile NC 28078
Phone [phone]
Fax[phone]
QUALITY CONTROL DATA
La Project Number 9290855
Client Project IU West End 6228-05-2694
SAUPLE DUPLICPTE 925443871
925427999 DUP
Parameter Units Result Result RPD Footnotes
Terphenyl-d14 68 59
Data 04/01/05
Page 17 of 25
Asheville Centificaon REPORT OF LABORATORY ANALYSIS cbtojtioioNCWastaWater40ThisreportsatnotNCWastewater 12NCDrinkingWater37712without the written consent of Pace Analytical Services Inc NC Drinking Water 37706SCEnvironments99030SC99006FLNELAPE87648FLNELAP87627
QUALITY CONTROL DATA
Pace Analytical Servicas Inc
9800 KincoyAvenue Suite WV
I-Iuntersville NC 28075
Phone [phone]
FaK 704.875.9091
QC Batch 124471
QC Batch Method EPA 8260
Associated Lab Samples 925437352
Lab Project Number 9290855
Client Project ID West End 6228-05-2694
Analysis Method EPA 8260
Analysis Description CC/MS VOCs by 8260 low level
NC Wastewater 40
NC Drinking Water 37712
SC Environmenf 99030
FL NELAP 87648
REPORT OF LABORATORY ANALYSIS
This report shall nut be reproduced uscept in full
without the written consent of Pace Analyitcal Sewices Inc
ititiID
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
WW.pace1abscom
METHOD BLANX 925442113
Associated Lab Samples
Parameter
Benzene
Bromodjchloronethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
Carbon tetrachiorida
Ch1orobenzee
Chlcroethane
chloroform
Chloromethane
Dibromochloromethe
l2-Djbromoethe EDB
12 -Dichlorobenzene
13 -Dicblorobenzane
14 -Dichlorobezene
Dichlorodjfluoromethane
l-Djch1oro
2-Djch1oroet
l-Dichloroethane
trans-l 2-Djchloroethe
12 -Dichloropropana
Diisopropyl ether
Ethylbenzee
Isopropylbeazene Cuanene
P-Isopropyltaluene
Methylene chloride
Methyl-tert-butyl ether
Raphthalene
n-Propylbenzene
lr22-Tetrachloroethane
Date 04/01/05
925437352
Units
ug/l
ugh
ugh
ug/l
ugh
ugh
ug/l
ugh
ugh
tig/l
ugh
ug/l
ugh
ug/l
ug/1
ugh
ug/l
up/i
up/i
ugh
ugh
ug/1
up/i
ug/l
ugh
up/i
ug/1
up/i
up/i
ug/l
up/i
Blank
_Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Reporting
Limit Footnotes
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1.0
Page 18 of 25
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunteisville NC 28078
Fone 704.B 75 .9092IabomFax704.875.9091
QUALITY CONTROL DATA
Lab Project Number 9290855
Client Project ID West nd 6228-05-2694
METROD BLANK 925442113
Associated Lab Samples 925437352
Blank ReportingParameterUnitsResultLimit Footnotes
Tetrachioroethene up/i ND 1.0
Toiuene up/i ND 1.0
lli-Trichloroethaxie up/i ND 1.0
li2-Trjchioroethane up/i ND 1.0
Trichioroethene up/i ND 1.0
Trich1orof1uoromete up/i ND 1.0124-Triinethylbenzene up/i ND 1.0
135-Trimethylbanzene uci/l ND 1.0
Vinyl chloride up/i ND 1.0
Zylene Total ug/l ND 1.0
mp-Xylene ugh ND 2.0
O-Xylene up/i ND 1.0
Toluene-d8 97
4-Bromofluorobezene 94
Dibroinofluoromathane 106
l2-Dichloroethane-d4 100
LABORATORY CONTROL SAMPLE 925442121
Spike LCS LCS
Units Conc Result FootnotesBanzeneughso.oo 43.54 87
Bromodichioromethane up/i 50.00 45.28 91Bromoformup/i 50.00 45.13 90
Bromomethazie up/i 66.94 134
n-Butylbenzexie ug/1 50.00 48.92 98
sec-Eutylbenzee ug/i 50.00 51.24 102Carbontetrachlorideug/1 50.00 46.14 92Chiorobenzeneup/i 50.00 45.76 92Chioroethaneup/i 50.00 42.74 86
Chioroforat ugh 50.00 46.23 92
Chioroxuethane ug/l 50.00 44.08 88Dibromochloromethaneup/i 50.00 44.55 89l2-Dibromoethane 5DB ugh 50.00 45.49 91i2-Dichiorobenzene up/i 50.00 46.83 94
Date 04/01/05
Page 39 of 25
REPORT OF LABORATORY ANALYSIS IiNCWastewater40
TInts report shall not he reproduced except in full Wastewater 12NCDockingWater37712wWouttee written consent of Pace tit ices NC Drinking Water 37706SCEnvironmy99030SC99006FLNELAPt87648FLNELAPE87627
Pace Analytical Services Inc
9800 Kincey Avenue Suite 100
Hunters yule NC 28078
Phone [phone]rmw.pacelabs corn Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9290855
Client Project ID West End 6228-05-2694
LABORATORY CONTROL SAKPLE 925442121
Spike LCS LCS
Units Conc Result Footnotes
13-Dichlorobenzena ugh 50.00 46.68 93
i4-Dichiorobenzejie up/i 50.00 44.17 88Dich1orodjfluoretheugh50.00 56.93 114
li-Dichloroethane up/i 50.00 43.99 88l2-Dichioroethe up/i 50.00 43.19 86li-Dichioroethene up/i 50.00 49.05 98
trans-i2-Djchioroethene up/i 50.00 45.26 90
l2-Dich1oropropane up/i 50.00 46.90 94
Diisopropyi ether up/i 50.00 45.85 92
Rthyibenzexse up/i 50.00 46.81 94
lsopropy.benzene Cumene up/i 50.00 53.22 106
p-Ieopropyltoluene up/I 50.00 46.68 93
t4ethylene chloride up/i so.oo 47.86 96
Methyl-tert.butyi ether up/i 50.00 44.77 90
Naphthalene ugh 50.00 50.59 101
n-Propylbenzene up/i 50.00 49.89 100
li22-Tetrachioroethe up/i so.oo 37.45 75
Tetrchioroethene up/i 50.00 47.68 95Tolueneup/i 50.00 45.50 91
lii-Trichioroethane ugh 50.00 46.17 92li2-Trjchloroethe up/i so.oo 45.02 90
Trichioroethene up/i 50.00 51.56 103Trichiorof1uoretheup/i 50.00 43.79 88
124-Trimethyibenzene up/i 50.00 44.65 89
i35.TrimethyTheaze ug/1 50.00 44.44 89Vinylchlorideup/i 50.00 48.56 97XyieneTotalup/i 150.00 144.4 96mp-Xyleae ug/i 100.00 96.10 96o-Xyiene up/i so.oo 48.28 97Toiuene-dB 1014-Bromofluorobenzene 98DibrGmofiuoromethe93i2-Dich1oroethe..d4 100
Date 04/01/05
Page 20 of 25
REPORT OF LABORATORY ANALYSISNCWastewater40
ThIs sigH not be repesduced except In full NC Waatewater 12NCDrinkingWater37712wittiestthewrittenconsentofPaceAnaliticalServicesIncNCDrinkingWater37706SCEnvIronmental99030SC99006NELAP87648
FL NaN E87627
Pace Analytical Serelces Inc
9800 AinceyAvenue Suite 100
Huntersvilte NC 28078
Phone [phone]wipace1abscomFax704.875.8091
QUALITY CONTROL DATA
Lab Project Number 9290855
Client Preect ID West End 6228-05-2694
MATRIX SPIKE MATRIX SPIKE DUPLICATE 925444069 925444077
925432296 Spike MS MSD 145 MSD
__________________________Units Result Conc Result Result %_g fl Footnotes
Benzexie ug/l 50.00 44.34 44.11 89 88
Chlorobenzena ug/l 50.00 47.43 46.30 95 93
ll-Dihloroethene ug/l 61.68 50.00 109.2 106.7 95 90
Toluesee ugh 50.00 46.58 46.50 93 93
Trichioroetbene ug/l 6.789 50.00 54.91 54.16 96 95Toluene-d8 100 99
4-Bromofluorobensena 98 99Dibromofluoromethane959512-Djch1oroethe-d4 97 99
Date 04/01/05
Page 21 of 25
DI REPORT OF LABORATORY ANALYSIS otkiCenifcatiottjsNCWastewater40
This report shaH not be reproduceri except in lulL NC Wastewater 12NCDrinkingWater37712wHhthewiftenconsentofPaceAnalyticalSevjcesIncNCDrinkingWater37706SCEnvironmental99030sc99006FLNELAPE87648FLNELAPE87627
Pace Analytical Services Inc
9800 Kincey4venue Suite 100
Hunters vile NC 28078
Fone 704875.9092
Fax [phone]
QUALITY CONTROL DATA
Lab Project Number 9290855
Client Project ID West End 6228-05-2694
QC Batch 124572 Analysis Method EPA 7470
QC Batch Method EPA 7470 Analysis Description Mercury CVAAS in WaterAssociatedLabSamples925437352
METHOD BL7NP 925446965
Associated Lab Samples 925437352
Blank ReportingParameterUnitsResultLimit Footnotes
Mercury mg/i ND 0.0002
LABORATORY CONTROL SAMPLR 925446973
Spike LCS LCSRaarnwterUnitsConcResult%Rec toteMercurymg/i 0.0025 0.0025 100
SPIMETRIXSpIKEflLITE92544698l925446999
925436099 Spike MS MSD MS MEDametergj__Ansii1t Coc Result _ilt %Rec %Rec gootesMercurymg/i 0.0025 0.0041 0.0026 163 103 45 233
Date 04/01105
Page 22 of 25
REPORT OF LABORATORY ANALYSISNCWastewater40
report shut not be reproduced NC Wastewater 12NCDnnkingWater37712without the written conseet of Pace Analytical Services Inc
NC Dnnking Water 37706SCEnvironmentel99030SC99006FLNAPE87648FLNELARE87527
Pace Analytical Satvlces Inc
9800 KinceyAvenue Suite 100
Huntetsville NC 28078
Phone [phone]www.paoelabscom
Fac 704.875.9091
QUALITY CONTROL DATA
Lab Project Number 9290855
Client Project ID West End 6228-05-2694
QC Batch 124415 naiysis Method EPA 6010
QC Batch Method EPA 3010 Analysis Description Metals by Trace ICPAssociatedLabSamples925437352
MBTUOD BLANX 925440257
Associated Lab Samples 925437352
Blank ReportingParameterUnitsResultLimit FootnotesArsenicmg/i ND 0.0050Bariummg/i ND 0.0050
Cadmium mg/i ND 0.0010
Chromium mg/i ND 0.0020
Lead mg/l MD 0.0050
Selenium rag/i ND 0.0050
Silver mg/i MD 0.0020
LABORATORY CONTROL SA3tPLE 925440265
Spike LCS LCSParameterUnitsConeResult%Rec FootnotesArsenicmg/i 0.5000 0.4250 85Bariummg/i o.sooo 0.4230 85Cadmiummg/i 0.5000 0.4100 82Chromiumag/i 0.5000 0.4090 82Leadmg/i 0.5000 0.4120 82Seleniummg/l 0.5000 0.4180 84Silvermg/i 0.5000 0.4360 87
MATRIX SPIKE MATRIX SPIKE DUPLICATE 925440273 925440281
925438152 Spike MS MSD MS MSDParameterpitsResultConcResultResult%Rec %Rec FootnotesArsenicmg/l 0.00270 0.5000 0.4780 0.4160 95 83 14Bariummg/i 0.2590 0.5000 0.7660 0.6570 101 80 15Cadmiummg/i o.oooii 0.5000 0.4540 0.3970 91 79 13Chromiummg/i 0.00167 0.5000 0.4620 0.3900 92 78 17Leadmg/i 0.00209 0.5000 0.4570 0.3990 91 79 14
Date 04/01/05
rage 23 25
REPORT OF LABORATORY ANALYSIS CflEieCeuicetiiNCWastewater40
This report shall not be reproduced except NC Waetewater 12NCDrinbngWater37712without the written consent of Pace Analytical Services Inc
NC DrinkinO Water 37706SCEnvironmental99030SC99006FLNELAPE87648FLNELAP687627
QUALITY CONTROL DATA
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunters v/lie NC 28078
Phone [phone]
Fax [phone]
La1 Project Number 9290855
Client Project ID West End 6228-05-2694
MATRIX SPIKE MATRIX SPIKE DUPLICATE 925440273 925440281
925438152 Spike MS MSD MS MSDParameterThjtsConcResult Result %g fl FootnotenSeleniummg/i 0.00223 0.5000 0.4640 0.4060 92 81 13Silvermg/i 0.00064 0.5000 0.4770 0.4320 95 86 10
SAMPLE DUPLICATE 925440299
Paramete
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
mg/i
mg/i
mg/i
mg/i
mg/i
mg/i
mg/i
925438160 DUP
Result Result Pootnotes
ND ND NC
ND
ND
ND
ND
ND
HthonlD
NC Waslewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NEIAP E87648
REPORT OF LABORATORY ANALYSIS
This repolt sisli not be reproduced except In full
without the written cnnsent of Puce Andytical Services
Inc
itin
NC Wastewater 12
NC Drinking ter .37706
SC 99006
FL NELAP 87627
0.01100 0.OiiOO
ND NC
ND NC
ND NC
ND NC
ND NC
Date 04/Oj/05
Page 24 25
QUALIrY CONTROL DATA PARAMETER FOOTNOTES
Pace Analytical Services Inc
9800 KinceyAvenue Suite 100
Hunters vile NC 28078
Phone [phone]
Fax [phone]
Lab Project Number 9290855
Client Project ID West End 6228-05-2694
Consistent with EPA guidelines unrounded concentrations are displayed and have been used to calculate Rec and RPD values
LCS Laboratory Control ainple Duplicate15DMatrixSpikeDuplicate
DUP Sample Duplicate
ND Not detected at or above adjusted reporting limit
NC Not Calculable
Estimated concentration above the adjusted method detection limit and below
MDL Adjusted Method Detection Limit
RPD Relative Percent Difference
Surrogate
The surrogate and/or spike recovery was outside acceptance limits
The spike recovery was outside acceptance limits for the MS and br MSD due
and/or LCSD were within acceptance limits showing that the laboratory is in
acceptable
The calculated RPD was outside QC acceptance limits
Date 04/01/05
the adjusted reporting
limit
to matrix interference The LCS
control and the data is
Page 25 of 25
iionlD
NC Wastewater 40
NC Drinking Water 37712
SC Environienl 09030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
The report ohall not be reproduced except hi lut
without the written consent of Pace Analytical Services Inc
lisiiuflo Certification lOs
NOWatitewater 12
NC Drinking Water 37706
SC 99006
FL NEI.AP 87627
Cl
Cl
SOIL CLASSIFICATION
AND REMARKS
SEE KEY SYMBOL SHEET FOR EXPLANATION OF
ifi SYMBOLS AND ABBREVIATIONS BELOW ir
SAMPLES PL NM%LL%
N-COUNTco0
ri
FINES
SPTbpt
10 20 30
40 50 60 70 80 90 100
3-4-4 .4
4-5-7
SS-1
SS-2
SS-3
SS-4
SS-5
SS-6
SS-7
SS-8
FILL Gray Silty Fine Sandy CLAY with Trace of
Roots and Sandy Seams
FILL Gray Olive Micaceous Silty Fine to MediumSANDwithTraceofRoots and Decayed Deposits
RESIDUUM-Very Firm Olive Brown Micacous
Silty Fme SAND
-10-
Dense to Very Dense Olive Gray Micaceous Silty FineSAND
15
20-
25
-HitRnck77 Feet
Auger Refusal and Boring Terminated at 2.7.0 FtGround Water Encountered at 22.4 Ft at Time of
Boring
30
-35-
-40-
8-10-11
8-12-14
14-19-17
1246-19
7-12-27
50/0
21
i_--------10
15
IIIiIIIII
100
30
DRILLERS Cain
EQUIPMENTD-50METHODHollow-stem Auger
HOLE DIA
REMARKS
PREPARED BYCHECKEDBY
THIS RECORD IS REASONABLE INTERPRETATIONOFSUBSURFACECONDITIONSATTHE EXPLORATION
LOCATION SUBSURFACE CONDITIONS AT OTHERLOCATIONSANDATOTHERTIMESMAYDIFFER
INTERFACES BETWEEN STRATA ARE APPROXIMATE
TRANSITIONS BETWEEN STRATA MAY BE GRADUAL
10 20 30 40 50 oO 70 80 90 100
PROJECT Celenese Tank BORING NO B-I
COORD
COORD
DRILLED June 14 2005
PROJ NO 6234-05-3016 PAGE OF
MACTEC Engineering Consulting Inc
SOIL CLASSIFICATION
AND REMARKS
SEE KEY SYMBOL SHEET FOR EXPLANATION OF
SYMBOLS AND ABBREVIATIONS BELOW FT
SAMPLES NM%LL%
N-COUNT
r-i
FINES
SPTbpf
10 20 30 40 50 60 70 80 90 100
12
SS-I
SS-2
SS-3
SS-4
ss-5
SS-6
SS-7
SS-8
5-7-7
4-5-7
7-9-10
11-14-15
10-14-15
12-16-17
11-15-12
7-11-50/4
FILL Brown Gray Silty Fine to Coarse SAND
FILL Olive Gray Silty CLAY with Coarse SAND
and Rock FragmentsRESIDUUMBrown Gray Micaceous Silty CLAY
with Fine to Medium Sandy Pockets-5-
Firm Olive Gray Silty Fine SAND
Very Firm Olive Gray Micaceous Silty Fine SAND
10
15
Finn to Dense Dark Brown Micaceous Silty FineSAND
-20-
V-H..
VeDjinti Gray Micaceous Silty Fine to Medium -1-SAND with Rock Fragments
-25-
PARTIALLY WEATHREI ROCK-S.ampled asWhiteOliveMicaceousSiltyFinetoMediumSANDwith Mottled Rock
30 Auger Refusal and Boring Terminated at 30.0 FtGround Water Encountered at 21 Ft at Time of Boring
35-
-40-
19
10
--15
-------20
Ii25
.1
DRILLER Cain
EQUIPMENTD-50
METHOD Hollow-stem AugerHOLEDIA
REMARKS
PREPARED BY
CHECKED BY
10 20 30 40 bO 70 80 90 100
Celenese Tank
THIS RECORD IS REASONABLE INTERPRETATIONOFSUBSURFACECONDITIONSAT THE EXPLORATIONLOCATIONSUBSURFACECONDITIONSAT OTHERLOCATIONSANDATOTHERTIMESMAYDIFFERINTERFACESBETWEENSTRATAAREAPPROXIMATETRANSITIONSBETWEENSTRATAMAYBEGRADUAL
PROJECT
COORD
COORD
DRILLED
PROJ NO June 14 2005
6234-05-3016
BORING NO B-2
PAGE OF
MACTEC Engineering Consulting Inc
SOIL CLASSIFICATION
AND REMARKS
SEE KEY SYMBOL SHEET FOR EXPLANATION OFSYMBOLS AND ABBREVIATIONS BELOW FT
SAMPLES
N-COUNT
im
PL NM%LL%
FINES
SPTbpf
10 20 30 40 50 60 70 80 90 100
P12
SS-1
SS-2
SS-3
SS-4
SS-5
SS-6
3-4-7
4-5-7
9-10-9
7-8-12
17-29-30
9-9-10
10
FILL Gray Olive Silty CLAY with Trace of Sand
FILL Brown to Yellow Brown Micaceous FineSandyCLAY
5-
RESIDUUM-Firm Brown Yellow to OliveMictceousSiltyFineSANDwithTraceofClay
Particles
10
Very Dense t.o Firm Olive Gray to Dark BrownMicaceousSiltyFineSAND
-15-fls
20
Boring Terminated at 20.0 FtNoGround Water Encountered at Time of BoringBoreholeCavedandDiyat16.0 Ft
25
30
-35
40
19
19
15
20
Cd
30
35
DRILLER Cain
EQUTPMENTD-50METHODHollow-stem AugerHOLEDIA
REMARKS
PREPARED BYCHECKEDBY
10 20 30 40 50 60 70 90 100
Celenese TankPROJECT
COORD
COORD
DRILLED
PROJ NOTHISRECORDISREASONABLEINTERPRETATIONOF SUBSURFACE CONDITIONS AT THE EXPLORATIONLOCATIONSUBSURFACECONDITIONSATOTHERLOCATIONSAND AT OTHER TIMES MAY DIFFERINTERFACESBETWEENSTRATAAREAPPROXIMATETRANSITIONSBETWEENSTRATAMAYBEGRADUAL
June 142005
6234-05-3016
BORING NO B-3
PAGE OF
MACTEC Engineering Consulting Inc