Item No 6 - UST 12 Closure Report-OCR

Prepared for
Crescent Resources LLC
400 South Tryon Street
Charlotte North Carolina
North Carolina
Department of EnvirOnment and Natural Resources
Underground Storage Tank UST42 Closure Report
NCDENR FMIILITY ID 0031324
1017 ELLIOT STREET
CHARLOTTE NORTH CAROLINA
Prepared by
GEOSYNTEC CONSULTANTS
1255 Roberts Blvd NW Suite 200
Kennesaw Georgia 30144
GeoSyntec Consi
April 2005
TABLE OF CONTENTS
1.0 GENERAL INFORMATION
Ii Facility Inlormation
1.2 Contacts
1.3 Underground Storage Tank Information UST
1.4 Site Charactenstics
2.0 CLOSURE PROCEDURE
2.1 Closure Preparations
2.2 Soil Excavation Activities
3.0 SITE INVESTIGATION
3.1 Field Screening
3.2 Soil Sampling
3.3 Groundwater Sampling
3.4 Analytical Results and Discussion
4.0 CONCLUSIONS AND RECOMMENDATIONS .6
FIGURES
Figure Site Location
Figure Plan View of UST Location
Figure Vertical Profile of Tank Pit with Sampling Locations
TABLES
Table Underground Storage Tank Information
Table PID Readings
Table Sample Summary
Table Analytical Results Appendix
Table Detected Compounds
APPENDICES
Appendix Table Analytical Results
Appendix Notification of Intent UST Permanent Closure or Change-in-Service
UST-3 Form
Appendix Site Investigation Report for Permanent Closure or Change-in-Services
of UST UST-2 Form
Appendix Certificate of UST disposal
Appendix Copy of all laboratory analytical records and Chain-of-Custody
Appendix Photographs of closure activities
Appendix Geologic logs for excavation
ii
North Carolina Department of Environmental and Natural Resources
Underground Storage Tank Closure Report UST-12 Form
NCDENR Facility ID 0-031324
1017 Elliot Sfreet Charlotte
NC
Crescent Resources LLC
1.0 GENERAL INFORMATION
The information in this report follows the general outline identified in the UST-12
Form format UST-3 Form Notice of Intent UST Permanent Closure or Change-in
Service Closure Appendix and UST-2 Form Site investigation Report for Permanent
Closure or Change-hi Service of UST Appendix are included in this report
1.1 Facility Information
Vacant Duke Power Pool Car Garage
Facility ID 0-031324
1017 Elliot Street
Charlotte North Carolina
Mecklenburg County
Date of Report 31 March 2005
UST Owner and Operator
Crescent Resources LLC
400 South Tryon Street Suite 1300
Charlotte NC 28201
704.382.8009
L2 Contacts
Pnmary Contact Person Kevin Doherty Regional Director Property Management
Crescent resources LLC 400 South Tryon Street Charlotte NC 28201 Telephone
704.382.8009
Closure Contractor AD Environmental and industrial Services Inc 2718 Uwharrie
Road Archdale NC 27263 Telephone [phone]
Pnmaiy Consultant Ronald Santini GeoSyntec Consultants 16049 Stonemont Road
Huntersville NC 28078 Telephone [phone]
Primary Laboratory Prism Laboratories 449 Spnngbrook Road Charlotte NC 28224-
0403 Telephone [phone] Contact Angela Overcash
1.3 UST Information
The charactensncs and pertinent information about the UST are listed out in Table
Table Underground Storage Tank infOrmation
Tank ID Tank FACID 0-031324
installation Date 1989
Size gallons 8000
Tank Dimensions 25 ft long ft diameter
Tank Construction Fiberglass
Last Known Tank Contents Gasoline
1.4 Site Characteristics
No known petroleum releases have occurred at the facility The property was
formerly the Duke Power Pool Car Facility The facility was closed in 1990 and
transferred to Crescent Resources LLC Crescent subsidiaiy of Duke Energy in 1992
and is currently vacant The pool cars were fueled at the facility from an 8000 gallon
underground gasoline storage
tank Duke Power consolidated the operation of pool car
facilities in the late 1980s which resulted in the closing of the facility and temporaiy
closing of the UST iii 1989
The current uses of adjacent and surroundings properties are commercial industrial
and vacant lands Adjacent property to the north is interstate Highway 1-77 site
location map showing the site and surrounding properties is presented on Figure
Mecklenburg County
is located within the timer Piedmont Belt of the Piedmont
Physiographic Province of North Carolina Sites in this area are underlain by
metamorphic and intrusive rocks consisting predominately of various forms of schist
gneiss granite gabbros and diorites that near the ground surface have been weathered
into distinctive residual soil known as saprolite The site soils from the tank excavation
floor and side walls consist of texture similar to sandy loam and were light brownish
yellow in color from the surface to depth of 20 feet below ground surface bgs
Appendix
Piedmont topography is characterized by gently rolling hills separated by small to
moderately sized streams Surface water and groundwater drainage patterns within the
Piedmont generally indicate the movement of water from topographic highs
to
topographic lows Piedmont hydrogeology is characterized by single water table flow
system that includes the saprolite partially weathered rock and unweathered bedrock
Recharge typically occurs in hill-top areas and discharge occurs
in streams rivers and
lakes It can be assumed for Piedmont areas that the surface topography approximates
groundwater flow direction However due to the urbanized nature of the area
surrounding the property it can be assumed the natural groundwater flow patterns have
been altered
Groundwater at the site is presumed to flow from the topographic highs in the south-
southeast section of the property to the topographic lows at the north-northwest section
of the property Groundwater was not encountered in the excavation at depth of 20 feet
2.0 UNDERGROUND STORAGE TANK CLOSURE PROCEDURES
2.1 Closure Preparations
Preparations for tank closure included notification of the Charlotte City Fire
Department by
the tank removal contractor Crescent requested marking
of all
underground utilities in the excavation and adjacent areas which was completed by
local
utilities prior to excavation An initial measurement of residual petroleum product
remaining in the tank was gauged with tank measuring stick by the tank removal
contractor and the gauging indicated the tank was dry This was confirmed by visual
observations once the tank was removed from the excavation
2.2 Soil Excavation Activities
The excavation was accomplished using track hoe The concrete surface was first
removed from the area to be excavated exposing the fill material surrounding the tank
The fill material was excavated approximately four feet on each side and at the ends of
the tank Care was taken to minimize damage to the tank during excavation In addition
care was taken to minimize damage to piping systems Excavation continued until the
subsurface native soils were exposed on the pit bottom and sidewalls The area
surrounding the tank was filled with inch gravel from top to bottom Once the fill
material was removed exposing the entire tank the tank was lifted from the excavation
by the track hoe and placed on flat bed trailer for transport and disposal Certificate of
UST Disposal Appendix Approximately 50 cubic yards cyd of gravel material
was removed from the excavation The excavated gravel was clean with no staining
odors or measurable readings on the photo ionization detector PID Water free
product or bedrock were not encountered during the excavation process photographic
log of excavation activities is included as Attachment
The material placed back in the excavation consisted of excavated materials and
approximately 50 cyd of clean soil obtained from the Martin Marietta Quarry Beatys
Ford Road Charlotte NC The soils were compacted using the track hoe prior to placing
final cover of crushed stone on the excavated area
Field observations and measurements during excavation did not identify the presence
of petroleum impacted soils
3.0 SITE INVESTIGATION
3.1 Field Screening
Field Screening Field screening was conducted using Photovac Model 2020 Pro
PID Prior to use the PID was calibrated using indoor air to set
the zero gas to parts per
million ppm The instrument was then calibrated against 100 ppm isobutylene
calibration gas standard The instrument reading was 99.9 ppm and no calibration
adjustments were made
Sixteen PID measurements were
made from the excavation including areas under
the dispenser main product line and the tank The layout of the UST and associated
appurtenances is shown on Figure In addition during initial excavation preparations
measurement was also taken from the tank fill port to determine the presence of
petroleum products
PID readings during excavation ranged from 0.4 ppm to 8.5 ppm
and the fill port measured 27.8 ppm Table Based on the relatively low PID readings
less than 10 ppm the data suggests that petroleum products
have not appreciably
impacted the fill materials or the soils beneath the tank In addition
the low P11 reading
from the tank fill port suggested minimal residual product was remaining in the tank
This was confirmed by physical measurements and observations once the tank was
removed from the excavation Both physical measurements and visual observations
indicated the tank was dry The 27.8 ppm reading can be explained by residual vapors
remaining in the tank
Table PID Readings _______ _______ _______
SAMPLE DEPTH
SAMPLE LOCATION SAMPLE ID feet bgs DATE TIME PID ppm
Gravel Fill Material NA Random 318/2005 NA 3.4
Gravel Fill Material NA Samples 3/8/2005 NA 2.6
Gravel Fill Material NA Collected 3/8/2005 NA 1.8
Gravel Fill Material NA from track hoe 3/8/2005 NA 7.4
Gravel Fill Material NA bucket 3/8/2005 NA 7.1
Gravel Fill Material NA during 3/8/2005 NA 3.5
Gravel Fill Material NA excavation 3/8/2005 NA 8.5
Gravel Fill Material NA activities 3/8/2005 NA 2.5
Gravel Fill Material NA 3/8/2005 NA 6.3
Tank Bottom West Ti 22 3/8/2005 1200 1.3
Tank Bottom Center T2 22 3/8/2005 1245 2.4
Tank Bottom East T3 22 3/8/2005 1300 2.1
Dispenser Pad Dl 0-5 3/8/2005 1230 1.2
Dispenser Pad NA 5-lO 3/8/2005 1240 0.9
Dispenser Pad NA 10-15 3/8/2005 1245 0.6
Product Line NA NA 3/8/2005 1130 0.4
Tank Fill Port NA NA 3/8/2005 0935 27.81
Field screen samples collected from the track hoe bucket were placed in oz amber
colored glass jars leaving room for headspace and covered with tin foil rubber band
was placed over the tin foil around the jar lip to seal the
container The samples were
allowed to equilibrate for approximately 10 minutes At
the end of 10 minutes the
headspace was analyzed for total volatile organic compounds by inserting the probe of
the PID through the tin foil to make field measurements The highest PH reading
observed was then recorded This process was completed for excavation field screening
and initial screening of soil samples submitted to the laboratory for analysis
3.2 Soil Sampling
Soil sampling locations are
identified on Figure In accordance with Guidelines for
Tank Removal North Carolina Underground Storage Tank Section four soil samples
were collected three from the bottom of the tank footprint and one from below the
dispenser Samples were not collected from the product lines or other piping systems
because visual observations suggested leaks had not occurred from the piping system
Table summarizes the sample locations sample IDs sample depths date and time P11
readings and analytical methods All samples collected were grab samples from
excavated soil and analyzed using EPA Method 503018260B and MAIEP VPH methods
Table Sample Summary
EPA
SAMPLE SAMPLE DEPTH MADEP Meihod
SAMPLE LOCATION ID ft bgs DATE TIME PID ppm VPH 603518260
Tank Bottom West TI 22 3/8/2005 1200
Tank Bottom Center T2 22 3/8/2005 1245
Tank Bottom East T3 22 3/8/2005 1300
Dispenser Pad Dl 3/8/2005 1230 1.2
Tank Fill Port NA NA 3/8/2005 935 27.8 NA NA
The excavation pit was dry at the time of tank removal No groundwater samples
were collected
All soil samples were collected in pre-preserved sample containers provided by the
laboratory All sampling equipment used was disposable eliminating the need for
equipment decontamination between samplings
Prior to sample collection sample containers were labeled with client sample
ID sample location date time analyte and samplers initials
New gloves were used and then discarded after each sampling
Samples analyzed by EPA Method 503518260 were collected in triplicate
pre-weighed VOA vials using disposable coring
device to collect
minimum grams of soil
The soil sample was immediately transferred to the VOA vial tightly capped
and swirled gently to expose the sample to the Sodium Bisulfate preservative
second sample
with Sodium Bisulfate preservative was collected in the
same manner
The third sample was preserved with methanol and collected in the same
manner as the Sodium Bisulfate preserved samples
fourth sample was collected for dry weight determination and for soil
characterization
One sample for MADEP VPH analysis was collected with an EnCore
sampler the EnCore sampler was then labeled and placed in the sample bag
provided with the EnCore sampler Duplicate samples for MADEP VPH
were not collected
sample was also collected
for field screening with PID
All samples with the exception of the PU sample were then immediately
stored in cooler at 40 until delivered to the laboratory
The Chainof Custody for each sample was completed and the process was
repeated until all four samples were collected
3.3 Groundwater Sampling
Groundwater samples from the excavation pit were not collected because the
excavation was dry at the time of tank removal
3.4 Analytical Results and Discussion
Analytical results are presented in Table Appendix and Appendix Four soil
samples were analyzed using
EPA Methods 5035/8260B and MADEP VPH method
Results of the analysis indicate all samples were below the reporting limits for petroleum
hydrocarbons gasoline However two samples contained acetone above the reporting
limits 67 microgram per kilogram ugfKg Dl 78 ugfKg and one sample contained
methyl ethyl ketone MEK T3 30 ug/Kg The laboratory reporting
limit for acetone
and MEK is 22 uglKg Laboratory QC results for these samples were below the reporting
limits and not detected Acetone is known laboratory contaminant and even though it
was not present in the lab QC samples does not necessarily rule out lab contamination
MEK is an industrial solvent and is not associated with gasoline The fact that MEK was
not detected in any of the other samples would suggest it presence is isolated Both
compounds were compared to the Maximum Soil Contaminant Concentrations found in
Table of Guidelines for Assessment and Corrective Action North Carolina
Underground Storage Tank Section and both were significantly below the
ResidentialfindustriallComniercial Soil Cleanup Levels as follows Table
Table Detected Compounds
Sample Sample
Residential Soil Industrail/Commercial
T3 Dl Cleanup Level Sod Cleanup Levels
Compound ug/Kg uglkg mg/Kg mg/Kg
Acetone 67 78 1564 40880
Methyl ethyl ketone 30 BRL 9385 245280
4.0 CONCLUSIONS AND RECOMMENDATIONS
Removal of the 8000 gallon fiberglass gasoline tank at 1017 Elliot Street CharlotteNCwascompletedtimelyandsafemannerAllproductpipingsystemsdispenser
piping and tank were free of leaks and/or cracks at the time of excavation The tank was
void of liquid and the inside thy at the time of removal Visual observation of excavation
pit soil conditions field PID screening of soils tank condition and laboratory results
suggested release from the tank or piping system had not occurred prior to excavation
However two compounds acetone and methyl ethyl ketone were detected at low
concentrations in Iwo pit floor samples These concentrations were compared to the
Table4 Maximum Soil Contaminant Concentrations found in Guidelines for Assessment
and Corrective Action North Carolina Underground Storage Tank Section
Residentjal/Jndusj-jal/Comjnercjal Maximum Soil Contaminant Concentrations and were
significantly below the cleanup levels
GeoSyntec concludes that no further action associated with tank closure is necessary
and the tank closure should be made permanent with regulatomy concurrence based on
the following findings
The tank was intact at the time of excavation
The tank was free of liquid
There was no evidence of leakage
Soils staining was not evident on the pit floor
Sample results do not show indications of petroleum leak and
Both acetone and MEK the only Iwo compounds detected were significantly
below the residential/industriallcommercial cleanup levels
FIGURES
Figure Site Location Parcel ID 07325214 Outlined in Green
LIST Location
1017 EllIot Street
Charlotte NC
Crescent Resources LLC
20 2005
v4
IC 20 30
IsNI ULJ..CTN
Ietc Eir4 N\V Siije 0OucwCii3L4-4
Figure Plan View of UST Location
IC
MPOF pit WE
Toot
fIi r.J
________
Figure Vertical Profile of Tank Pit with Sampling Locations
Fi OVA
MAP OP TEST Pit PiiOPSi
cr -5
j-.OI
APPENDIX
Table Analytical Results
Table Analytical Results
s_10 Sapie 08e
/5/ke IAs_e 10 /kn 10 ogt A5 Ah59 6a8 i9
Ti 3/8/215 25007675 112702 1i12-T00i446hne 630-20-6 82608 SRI 5.1 pg.kg
TI 3/8/2/305 25007675 112702 tIi-Tthne 71-56-6 82606 SRI 5.1 pg/kg
Ti 3/8/2005 25007675 112702 i.IZ2-Trhor00hane 79-34-5 82606 SRI 6-I iig%g
Ti 3/8/266 25007675 112702 76-13-I 82606 SRI 10 g8/g
TI 361285 25007975 112702 1i2-Tiic//59iiane 82608 SRI 51 pg/kg
Ti 3/8/2505 25607675 112702 ii-0ithIo46e 75-34-3 82606 SRI 6-i pg/kg
Ti 3/9/2065 25007675 112702 li-0io46ene 75-35-4 82609 SRI 5.1 pg/kg
Ti 3/62505 25007675 112702 lI-9dcrcprcpie 563-59-6 8260B SRI 5.1 pg/kg
Ti 3/8/2/98 25007675 112702 l23-Tæc94the.ie 87-61-6 82606 SRI 10 iig/kg
Ti 3/8/2005 25007675 112702 l.23-T4-Jmrgrqme 96-19-4 8260B BRI 5.1 pg/kg
Ti 3/8266 25007675 112702 124Tæthevme 120-82-i 82606 SRI 10 pg/kg
TI 3/8/2005 25007675 112702 lZ4-T6mhyIbenzm 95-63-6 82606 881 10 g8g
Ti 3/82/98 25007675 112772 I.2-D91rmno-3-ct/mqircpgne 86-12-8 82606 SRI 5.1 pg/kg
Ti 3/82005 25007675 i12702 i.2-D9mmodhaleEDS 100-93-4 82606 SRI 5.1 pg/kg
TI 3/8/2005 25007675 112702 I2-0m.zmm 95-50-i 8296B SRI 10 pg/kg
Ti 3/8/2005 25007675 112702 12-0icNo8he 107-06-2 82609 SRI 5.1 pg/kg
Ti 3/8/2/XiS 25917675 112702 i2-DNrgmm 78-87-5 82606 SRI 5.1 pg/kg
Ti 3/87266 25007675 112702 135.TSm8/5y9mizmie 108-67-8 82606 SRI lOpg8gTI3/8/2/95 25007675 112702 I3-9mizene 541-73-1 82838 SRI 10 pg/kg
TI 3/8/2915 35007675 112702 13-thkroprcmgm 142-28-9 82608 SRI 5.1 pg/kg
Ti 3/8/2095 25007675 112702 14-0cbize 100-46-7 82606 SRI 1/pg/kg
Ti 3/82005 25007675 112702 14-059/o6464oe 110-56-5 826DB SRI 1/pg/kg
Ti 3/82065 28007675 112712 Z2-Di59rqe 590-20-7 82605 SRI 5.1 g/kg
Ti 3/82305 25007675 112702 2-Ckc4w4 he 110-75-8 82608 SRI 10 pg/kg
TI 3/8/2/98 25007675 112702 Chk95due 95.49-8 826DB SRI 10 pg/kgTi3/8/2065 25007675 112712 -Hmaone 501-78-6 82606 SRI 51 pg/kg
Ti 3/8/2065 5007675 112702 4hfde 106-43-4 82919 SRI 10 pg/kg
TI 3/91289 25007675 112702 4-Mh2-pen00one MISS 106-10-i 826DB 881 10 pg/kgTi3/5/2065 25007675 112702 A54cne 67-54-1 82606 SRI 20 998/9
Ti 3/8/265 25007675 112702 Crd46 107-02-8 82600 BRI 100 pg/kgTi3/9/2915 25007675 112702 Acr4m959e 107-13-i 8260B SRI l00 pg/kg
Ti 3/8/25/5 25007675 1I2702 Bmizene 1-43-2 82608 SRI 3.1 pg/kgTi3/8/2006 25007675 112702 0bmzene 108-86-i 82600 081 5.1 pg/kg
Ti 3/8/2065 25007675 112702 5-m1od4c.miiae 74-97-5 82838 SRI 5.1 pg/kgTi3/8/5 25007675 112702 5-mlm46mne 75-27-4 82605 BRI 5.1 pg/kgTi3/8/2505 25007675 112712 6omolann 75-25-2 82605 SRI 5.1 pg/kgTI3/8/285 25007675 112702 Smnmt59haie 748/3.9 82605 SRI 10 94g
Ti 3/8/2/915 25007675 ii2712 Catcithm4fide 75.15-0 8280S SRI 10 pg/kgTi3/9/2065 25007675 112702 Cd54/54 56-23-5 82608 SRI 5.1 pg/kgTi3/P12 25007675 112702 C/rthmumm 109-83-7 8260B SRI 5i pg/kgTI3/8/31816 25007675 Ii2702 CNmodgrcmane6lmne 124-48-i 82838 BRI 5.1 pg/kgTI3/872065 25007675 112702 ChIoIimie 75-00-3 92605 SRI 10 pg/kgTi3/8/25007675 112702 CSIoofmm 67-00-3 82606 SRI 5.1 pg/kgTi3/5/2005 25007675 112702 CNmm08he 74-87-3 82608 SRI 10 9/kgTI318/2095 25007675 112702 Æ-i2-DichI59bmm 156-59-4 82608 SRI 51 pg/kgTi3/8/25007675 112702 ds-13-Dc/knpropmm 10061-01-5 826DB SRI 5.1 pg/kgTi3/82065 5007675 112702 O9/rmnmnhmm 7495-3 82600 SRI 5.1 pg/kgTi3/8/2065 25007675 112702 Did /ae 75-61-6 82608 SRI 10 94gTi3/6/2505 25007675 ii2702 BSnzmm 100-41-4 82908 SRI 6.1 pg/kgTI3/8285 25067675 1127122 thmdimiam 87-68-3 82918 SRI is pg/kgTI3/9/2065 25007675 1i2702 qrc /176 108.20-3 82606 SRI 5.i pg/kgTI3/9/295 007675 112702 scprpIbmizne 98-82-8 82606 SRL 10 pg/kgTI3/8/2005 25007675 112712 mp-Xes 136777-6i-2 82606 681 15 pg/kgTi3/8/2085 25007975 112702 94ii9 hyi kdme MEK 78-93-3 82608 SRI 20 pg/kgTI3/8/2066 25007675 112702 MhI io8de 74-88-4 82808 SRI pg/kgTi3/912065 25007675 112702 Mh4IgJ/M15E 1834-04-4 82608 SRI 6-1 pg/kgTI3/9/205 25007975 112702 Mk5lm ddde 75-06-2 82608 SRI 10 pg/kgTIY/5 28307675 112702 n-Buty91izie 104-51-8 82808 681 iS pg/kgTi3/28007675 112702 n-Popgyibmimie 103-86-I 82609 SRI I0 pg/kgTi3fg/2 25007675 112702 N61kthaiem 91-20-3 82606 SRI 8.1 pg/kgTI3/8/2/XIS 25007675 112702 o-ylmm 65-47-6 82508 SRI 5i pg/kgTi3/92605 28007675 112702 p-sqrqIyfloe 96-87-8 82608 SRI 15 pg/kgTI3/9/28/5 25007675 112702 sec-91Ay91mzmm 136-98-8 82908 SRI 11 pg/kgTi3/5 28007675 112702 5yr 100-42-5 82606 SRI 5.1 pg/kgTI3/8/5 5007675 112702 imI-But1benze-m 98/08-08 82608 SRI 20 pg/kgTi3/8/2008 25007675 112702 ctgm59hee 127-18-4 82808 SRI pg/kgTI3/50905 28007675 112702 ckme 108-88-3 2608 SRI 5.1 pg/kgTI3/5/289 35007675 112702 tr-m-12-0ith/okme 156-90-5 82906 SRI 51 pg/kgTi3/872065 25067675 112702 b-i.3-Dthkoprcpm 10051-02-6 82606 SRI 6-1 pg/kgTi38/2005 28007675 112702 659khme 79-01-6 82608 881 Sipg/kgTi3/8/2095 5007675 112707 mc ad/u ndlmne 75-96-4 82608 SRI 5.1 pg/kgTi3/g 5007675 112702 ruiylacdae 75-15-0 82609/SRI 10 pg/kgTi3/8/2065 25007675 112702 Vkiy/c/5918e 75-01-4 82806 SRI 10 pg/kgTi3/8/2005 25007675 112702 C5-728 Al/phd/cs N/A MADEPVPI-i 881 84 mg/kgTi3/92505 J25007675 112702 C9-CiOAc.nd/cs N/A M/kDEPVPI-9 SRI 84 mg/kgTi3/82005 125007875 112702 C9-Cl2AJiphd/cs N/A MAOEPVPI4 SRI 84 9/kg
ukc Lb
Srçe Sani4e DIe Sanpe ID 81 ID 56npait AS MIcd Resuft
12 3/8/2005 25007676 112703 1.1.I.2-Tetrachkucthane 630-20-6 92608 BIlL
12 3/8/2005 25007676 112703 11.l-Tjjcklcu-cethane 71-55-6 82608 BR
12 3/82005 25007676 112703 11.2.2-TrachIcucethane 79-34-5 82608 BR
12 3/8/2005 25007676 112703 1.12-Tr/thIao-42.2-Tr/flucoethane 79-13-1 82608 BR
12 3/8/2005 25007676 112703 11.2-Tnchlcwcethane 79-00-5 82600 BIlL
12 3/9/2005 25007678 112703 1.1-Dichlcrodkane 75-34-3 82608 BR
12 3/6/2005 25007676 112703 1.1-Dchlcro91hme 75-35.4 82600 BIlL
T2 3/8/2005 25007676 112703 1.1-D/chlcrgircpene 563-58-6 826GB BR
12 3/812005 25007676 112703 1.2.3-Tæchac8enzene 87-61-6 8260B BR
12 3/8/2005 25007676 112703 l.23-TrithIaqrcgmne 98-18-4 82608 BR
12 3/8.12005 25007676 112703 1.2.4-Tr/chkectenzane 120-82-I 82608 BR
12 3/6/2005 25007676 112703 1.2.4-Trimeth1benzene 95-63-6 82608 BR
12 3/8/2005 5007676 112703 l2-90-12-8 82608 BRL
T2 3/8/2005 25007676 112703 1.2-DOrcinoethane EDB 108-93-4 826GB BRL
12 3/8/2005 25007676 112703 l.2-Dichkrobanzere 95-50-1 8260B BRL
12 3/8/2005 25007676 112703 1.2-I3cl4orodhane 107-06-2 6260B BR
12 3/8/2005 25007678 112703 1.2-DichlctcFopane 78-87-5 8260B BR
12 3/8/2005 25007676 112703 1.3.5-Tr/meth4benzene 108-67-8 82608 BIlL
T2 3/812005 25007676 112703 1.3-Dich/crohoezene 541-73-1 82608 BRL
12 3/812005 25007676 112703 13-DchIoroprcane 142-28-9 82600 BIlL
12 3/812005 25007676 112703 1.4-Dchlorthenzene 106-46-7 8260B BR
12 3/82005 25007676 112703 1.4-D/chlcrobutane 110-56-5 82608 BR
T2 3/812005 25007676 112703 2.2-Dichlcropropane 590-20-7 62608 BIlL
12 3/6/2005 25007676 112703 2-Cl oat vmyl Rher 110-75-8 826GB 681
12 3/8/2005 25007676 112703 2-Chlcicgdueie 95-49-8 82608 BRL
12 3/8/2005 25007676 112703 2-Hexesone 591-79-6 82600 BR
12 3/8/2005 25007678 112703 4-Chkac1duene 106-43-4 8260B BRI
T2 3/8/2005 25007676 112703 4-Mhyl-2-pentancneMlBK 108-18-I 82608 BIlL
12 3/8/2005 25007676 112703 AcRcne 67-64-I 82608 BRL
12 3/8/2005 25007676 112703 Acrde/n 107-02-8 82608 BR
12 3/8/2005 25007676 112703 Acncni1r6e 107-13-i 82608 88
72 3/812005 25007676 112783 Benzene 71-43-2 8260B BRL
12 3/8/2005 25007676 112703 Brorncbenzane 108-86-1 82608 8RL
12 318/2005 25007676 112703 Brcncchlorcwnethxne 74-97-5 82608 BIlL
T2 3/8/2005 25007676 112703 Brcmcdichlam-16hane 75-27-4 82608 BR
12 3/812005 25007676 112703 Brando-rn 75-25-2 82608 BR
12 3/812005 25007676 112703 Bronan91hane 74-83-9 82000 BRI
12 31812005 25007676 142703 Carbon 4-sulfIde 75-15-0 82608 BR
12 3/8/2005 25007678 112703 Carbon tIdrachtoide 56-23-5 82608 BR
12 3/8/2005 25007676 112703 Chlcrthenene 108-90-7 82608 BR
12 3/8/2005 25007676 112703 Chlceod81rcenandhane 124-48-1 8260B BR
12 3/8i2005 25007676 112703 Chtceodhane 75-00-3 8260B BR
12 3/8/2005 25007676 112703 Chlorofcrm 67-66-3 8260B BRL
12 3/8/2005 25007676 112703 Chlcrcenethane 74-87-3 82808 BR
12 3/8/2005 25007676 142703 cIs-12-Dichtcrodhone 156-59-4 82600 BR
12 3/8/2005 25007676 112703 cis-1.3-Dichlacpropene 10061-01-5 82608 BIll
12 3/8/2005 25007676 412703 D81ranaodhane 74-95-3 82608 88
12 3/8/2005 25007676 112703 Dichtcrodltiucromdhane 75-61-6 82608 881
12 3/6/2005 25007678 112703 Ethy6/enzene 100-41-4 82608 BIlL
12 3/8/2005 25007676 112703 Hexuchla-ctutadene 87-68-3 8260B 881
12 3/8/2005 25007676 112703 Isoprcp4 ether IPE 108-20-3 82608 BIlL
12 3/8/2005 25007676 112703 Iscprop4benzene 98-82-8 82608 BIlL
12 3/82005 25007676 112703 m.p-Xylenes 136777-81-2 8260B BRL
12 3/8/2005 25007676 112703 Me6h54koneMEç 78-93-3 82608 BR
12 3/8/2005 25007676 112703 Meth4kxtfaJe 74-88-4 82608 BR
12 3/9/2005 25007676 112703 Meth5I-but54IdhMTBE 18.34-04-4 82608 BRI
12 3/8/2005 25007676 112703 Meth4ene chtcaide 75-09-2 82608 BR
12 3/8/2005 25007676 112703 ntht5bonzene 104-51-8 826gB 881
12 3/8/2005 25007676 112703 -Sop5benzene 103-65-I 82608 BIll
12 3/8/2005 25007676 112703 Nephlhalene 91-20-3 8280B BR
12 3/612005 25007676 112703 o-X5ena 95-47-6 82608 881
12 3/8/2065 25007676 112703 p-cp3ltduene 99-87-6 82608 BR
12 3/812005 25007676 112703 sec-Butyftmzene 135-98-8 82608 BIlL
12 3/812005 25007676 112703 Styrene 100-42-5 82608 881
12 3/812005 25007676 112703 et-But4berciene 98-06-06 92608 881
12 3/8/2005 25007676 112703 TeirachioroIdhene 127-18-4 82600 BIlL
12 3/8/2005 25007676 112703 Tohiene 108-88-3 82608 BIlL
12 3/8/2005 25007676 112703 ans-12-Dthtacethgie 156-60-5 82608 88
12 3/8/2005 25007676 112703 ans-l.3-Dithkrcuropene 10064-02-6 82608 BR
12 3/812005 25007676 112703 TIchkeoeihene 79-01-6 82608 8/IL
12 3/8/2005 25007676 112703 Trichtorofhjaanethane 75-69-4 82608 BIll123/812005 25007676 112703 n5 acefate 75-15-0 82608 BR
12 3/812005 5007676 112703 .91ytthIIde 75-01-4 9260B BIlL123/8/2005 25007676 112703 C5-C8Mhutics 91/A MADEPVPJ-t BIlL
12 3/8/2005 25007676 142703 C9-C10 kanatics N/A MADEP WH BR
12 3/8/2005 25007676 112703 C9-Cl2P8pbafIcs N/A MADEPVPH BR
1516
5.2 jig/kg
5.2 pg/kg
5.2 pg/kg
10 PgAg
5.2 pg/kg
5.2 pg/kg
52 pg/kg
5.2 pg/kg
10 pg/kg
5.2 jig/kg
10 pg/kg
10 pg/kg
5.2 pg/kg
5.2 1.10/kg
10 pg/kg
5.2 pg/kg
5.2 pg/kg
10 pg/kg
10 pg/kg
5.2 pg/kg
30 pg/kg
10 jig/kg
5.2 jig/kg
10 pg/kg
10 jig/kg
52 pg/kg
10 pg/kg
40 pg/kg
21 pg/kg
100 pg/kg
100 pg/kg
3.3 P11/kg
5.2 pg/kg
5.2 pg/kg
5.2 pg/kg
5.2 Pjhllg
10 pg/kg
10 pg/kg
5.2 iig/kg
5.2 jig/kg
5.2 pg/kg
10 pg/kg
8-2 p04cg
10 pg/kg
5.2 pg/kg
5.2 ikg
5.2 pc/hg
10 pg/kg
6.2 pg/kg
46 pgikg
52 pg/kg
10 pg/kg
16 pg/kg
21 pg/kg
10 pg/kg
5.2 pg/kg
40 g/kg
16 pg/kg
30 pg/kg
6.2 pg/kg
5.2 pglg
16 pg/kg
16 pg/kg
5.2 pg/kg
21 pg/kg
10 pg/kg
52 pg/kg
5.2 pg/kg
5.2 pg/kg
5.2 pg/kg
52 pg/kg
10 pg/kg
10 pg/kg
8.3 mg/kg
8.3 mg/kg
9-3 mg/kg
Lke Lth
Spi1e 93 Se 36e Sa194e 93 93 AS Mthai Resu RI 156
13
13
13
13
13
T3
13
13
13
13
13
T3
13
13
13
13
13
TI
13
T3
13
T3
13
13
T3
T3
T3
13
13
TI
TI
13
13
13
13
13
13
13
T3
13
13
TI
13
T3
13
TI
TI
T3
TI
13
TI
13
TI
T3
T3
TI
13
TI
TI
13
TI
13
TI
13
T3
13
TI
TI
13
TI
T3
13
13
T3
13
13
3812005 25007677 112704 1.1I.2-Tetmchkx56hane 630-20-6 1260B BRI
3/8/2005 25007677 112704 11.1-Tr/chlcrcethane 71-55-6 82608 BRL
3/6/2005 25007677 112704 l.12.2-TrechI56hane 9-34-5 82606 8/41
3/8/2005 25007677 112704 l.1.2-Tntho-o-l.2.2-Tn6ucroethane 76-13-i 82608 BRL
3/8/2005 25007677 112704 lj2-Trichlcroethane 79-00-5 82608 BRL
3/8/2005 25007677 112704 1.1-I3thkx56hane 75-34-3 82608 B/lL
3/8/2005 25007677 112704 1.1-Dchlcr00hene 75-35-4 826DB BRI
3/8/2005 25007877 112704 1.1-f3thIcrcprW 563-58-6 82608 8141
3/8/2005 25007677 112704 1.2.3-T0chk.thenzene 87-61-6 82608 BRL
38/2005 25007677 112704 12.3-Trjct4ccgrcpane 96-18-4 82608 8141
3/8/2005 25007677 112704 1.2.4-TrichIc81enzene 120-82-1 82608 BRL
3/8/2005 25007677 112704 12.4-Trheth5tenze1e 95-63-6 8260B BRL
318/2005 25007677 112704 1.2-96-12-8 826DB BRL
3/8/2005 25007677 112704 1.2-106-93-4 82608 8141
3/82005 25007677 112704 1.2-L6thJcc6ize 95-50-1 82608 861
3/8/2005 25007677 112704 1.2-LthIcrcethane 107-06-2 82608 861
3/8/2005 25007677 112704 i.2-/th/orcwcpane 78-87-5 82608 BRL
3/8/2005 25007677 112704 13.5-Tr9dby8enze 108-67-8 82608 BRL
3/8/2005 25007677 112704 1.3-L3chtezne 541-73-1 82608 8/41
3/8/2005 25007677 112704 i.3-L9chIcrprrane 142-28-9 82608 8141
3/8/2005 25007677 112704 1.4-L9chlcthen2e 106-46-7 82608 861
3/8/2005 25007677 112704 1.4-C11/kIcrthutane 110-58-5 82608 SRI
3/8/2005 25007677 112704 2.2-Dd4cprqane 590-20-7 82608 BRL
3/82005 25007677 112704 110-75-8 82608 8141
3/812005 25007677 112704 2-ChIc4duene 95-45-8 82608 8141
3/8/2005 25007677 112704 2-Hexancne 591-78-6 82608 BR
3/8/2005 25007677 112704 4-ChIc6cIuene 106-43-4 82608 BRI
3/812805 25007877 1/2704 4-Mtg/-2-penLanoneM8K 108-10-I 82608 BRL
3/8/2005 25007677 112704 Acetcne 67-64-I 82608 67
3/8/2005 25007677 112704 cion 107-02-8 8260B BRI
3/8/2005 25007677 112704 AcrylcrlhIle 107-13-1 82608 8141
3/8/2005 25007677 112704 Bizene 71-43-2 82608 BRL
3/8/2005 25007677 112704 Bracbizene 108-66-1 82606 BRL
3/8/2005 25007677 /12704 Branoch/orethore 74-97-5 82608 B/IL
3/8/2005 25007677 112704 Branoc9chIccmhane 75-27-4 82608 BRL
3/8/2005 25007677 112704 B/crnofcm 75-25-2 82608 8/IL
3/8/2005 25007677 112704 Brancmethane 74-83-9 82608 8141
3/8/2005 25007677 112704 Ctnc9s./I1de 75-15-0 8260B BRL
3/8/2005 25007677 112704 Catch/ckje 56-23-5 82608 8141
3/8/2005 25007677 112704 Che 108-90-7 82608 B/IL
3/8/2005 25007677 112704 Ch/acx9fracmethane 124-48-1 8260B B/IL
3/82005 25007677 112704 Chk00hane 75-00-3 82608 B/IL
3/8/2005 25007677 112704 Chaclorm 67-66-3 82608 861
3/82005 25007677 112704 C11lacn56hane 74-87-3 82608 BRL
3/8/2005 25007677 112704 ds-1.2-Djc/IIao5ene 156-59-4 826DB SRI
3/8/2005 25007677 112704 cs-l.3-OichIacprqene 10061-01-5 82608 8141
3/812005 25007677 112704 D6rn/a11ethie 74-95-3 82608 BRL
3/82005 25007677 112704 DthI56i8ua50h 75-61-6 82608 8141
3/8/2005 25007677 112704 Ethbenzene 100-41-4 8260B B/Il
3/8/2005 25007677 112704 HacNtadene 87-68-3 82608 BRL
3/8/2005 25007677 112704 JsqrcpI eth IPE 108-20-3 82608 B/IL
3/8/2005 5007677 112704 Isqrcpybnzene 98-82-8 826DB 8141
3/8/2005 25007677 112704 m.p-Xyenes 136777-61-2 82608 8141
3/8/2005 25007677 112704 Mdh54h4k/4cieMEK 78-93-3 82608 30
3/8/2005 5007677 112704 Meth4 ioc9de 74-88-4 8260B 8141
3/812005 25007677 112704 M/4h1t-but549herMTBE 1634-04-4 82608 8141
3/8/2005 25007677 112704 Meth4ec8a/de 75-09-2 82608 SRI
3/8/2605 25007677 112704 n-Sut/kenzne 104-51-8 826gB B/IL
3/82005 25007677 112704 n-Pr4benzene 103-65-1 82608 SRI
3/812005 25007677 112704 NaphthIJese 91-20-3 82608 861
3/82005 25007677 112704 o-X4ene 95-47-6 826DB 8141
3/8/2005 25007677 112704 p-Iscprayftdue 98-87-6 8260B SRI
3/812005 25007677 112704 sec-Buty81zene 135-98-8 82608 BRL
3/8/2005 25007677 112704 Ste 100-42-5 82608 SRI
3/8/2005 25007677 112704 t-81beizme 96-96-06 82608 SRI
3/8/2005 25007677 112704 Tefrathoethene 127-18-4 82608 B/Il
3/8/2005 25007677 112704 Tce 108-88-3 8260B BR
3/8/2005 25007677 112704 rs-l.2-0jth/ohene 156-60-5 82608 BRI
3/8/2005 25007677 112704 rs-1.3-Ochkrcprcpene 10061-02-6 82609 SRI
3/8/2005 25007677 112704 TrlchIaohene 79-01-9 826DB SRI
3/8/2005 25007677 112704 TrchJaofiuccgi56hane 75-95-4 826DB B/IL
3/8/2005 25007677 112704 mylacethte 75-15-0 8260B B/IL
3/8/2005 25007677 112704 rrl34chIaide 75-01-4 82608 SRI
3/8/2005 25007677 112704 C5-CBMlphaScs N/A MADEPWH B/IL
3/82005 25007677 112704 C9-Clokanatcs N/A MADEPVPH 8141
3/82005 25007677 112704 C9-C12/8g956cs N/A MADEP VP-BRI
5.5 pg/kg
5.5 pg/kg
5.5 Pg/kg
11 pg/kg
5.5 p9119
5.5 pg/kg
5.5 Pg/kg
pg/kg
11 pg/kg
5.5 8/1119
11 pg/kg
II pg/kg
5.5 pg/kg
5.5 pg/kg
11 g/kg
5.5 pglkg
5.5 pg/kg
11 pg/kg
11 pg/kg
5.5 pg/kg
11 pg/kg
11 pg/kg
5.5 pg/kg
11 pg/kg
11 pg/kg
55 pg/kg
11 pg/kg
11 pg/kg
22 pg/kg
1/0 pg/kg
110 pgkg
3.3 pg/kg
5.5 19/19
5.5 pg/kg
5.5 pgkg
55 pglcg
11 pg/kg
II pg/kg
5.5 pg/kg
5.5 pg/kg
5.5 pg/kg
11 /Jg/kg
5.5 pg/kg
11 pg/kg
5.5 pg/kg
5.5 pg/kg
5.5 pg/kg
i/pg/kg
6.6 pg/kg
17 pg/kg
5.5 pgkg
11 pg/kg
/7 pg/kg
22 pg/kg
ii pg/kg
5.5 pg/kg
11 pg/kg
17 pg/kg
11/1968/
6.6 pgllg
5.5 pg/kg
17 pg/kg
17 pg/kg
5.5 pg/kg
22 pg/kg
11 pg/kg
5.5 pgkg
5.5 u9/cg
5.5 pg/kg
5.5 pa/kg
5.5 pg/kg
II pg/kg
11 pg/kg
8.3 mg/kg
8.3 mg/kg
8.3 mg/kg
n4e ID Saj8e Oe üke
SrçIe ID ism ID CaTpmd Ig8 Re /1 L94t
Dl
Dl
Dl
01
01
01
Dl
01
01
Dl
01
Dl
01
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
01
Dl
Dl
01
Dl
Dl
Dl
Dl
01
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
01
Dl
01
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
01
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
Dl
78
3/82005 25007678 112705 1112-Tetradiloroethane 630-20-5 82608 BR
3/82005 25007678 112705 1.l1-Tric5kscdtan 71-55-6 82608 BR
382005 25007678 112705 l1.22-TetmchIocoethaje 79-34-5 82608 BRL
38/2005 25007078 112705 11.2-TrichIao-l.22-TritIijaohane 76-13-i 82608 BR
3/8/2005 25007678 112705 1.l.2-TrithIcohane 79-00-5 8260B 881
3/8/2005 25007678 112705 1.1-0thIco8hane 75-34-3 8260B BRL
3/82005 25007678 112705 1.l-CchIodhene 75-35-4 8260B BIlL
3/8/2005 25007678 112705 l.1-thcwcpes1e 563-58-6 8260B 881
3/8/2005 25007678 112705 i.23-Trichkctzene 87-61-6 82608 BRL
3/82005 25007678 112705 l.23-TnchIaqcane 96-18-4 2608 BRL
3/82005 25007678 112705 l.2.4-TrchIathenze 120-82-I 82608 BIll
3/8/2005 25007678 112705 1.24-TrImeth4bzene 95-63-6 82608 BRL
3/8/2005 25007678 112705 l.2-09/3-ct4cropccpane 96-12-8 8260B BR
3/8/2005 25007678 112705 12-DbcanohaneEDB 106-93-4 8260B 881
3/8/2005 25007678 112705 12-95-50-1 82608 881
3/82005 25007670 112705 l.2-flchIo8bane 107-06-2 82608 BRL
3/82005 25007678 112705 l.2-E0chIorcxcpane 8-87-5 52608 BRL
38/2005 25007678 112705 l3.5-Trlmeth54benzene 109-67-8 8260B BR
3/82005 25007678 112705 l.3-C5thIcbenze 541-73-1 82608 881
3/8/2005 25007678 112705 3-EchIocçcpeje 142-28-9 82608 BR
3/8/2005 25007678 112705 1.4-DchIobenze 106-46-7 82608 BR
3/8/2005 25007678 112705 14-I3chIorcIane 118-56-5 826GB BR
3/8/2005 25607678 112705 2.2-Dctiloroçxqane 590-20-7 82608 881
3/8/005 25007678 112705 110-75-8 82608 BRL
3/8/2005 25007678 112705 2-CI1Iacfuene 95-49-8 82608 BR
3/8/2005 25007678 112705 2-Hencne 591-78-6 82608 BR
3/92005 25007678 112705 4-Clkrckcluene 106-43-4 82608 BR
3/9/2005 25007678 112705 4-M8hy-2-peniaeIBK 108-10-1 826GB BR
3/82005 25007678 112705 Acetae 67-54-1 82608
3/82005 25007678 112705 coIn 107-02-8 82608 BIlL
3/8/2005 25007678 112705 cr0/a8r9e 107-13-1 82608 BR
3/8/2005 25007678 112705 Bizefie 71-43-2 82608 881
3/8/2005 25007678 112705 Branthenze 108-86-1 82608 881
3/8/2005 25007678 112705 BrcmcEhlcran8Ilane 74-97-5 82608 BIlL
3/812005 25007678 112705 Bunc/8d4amtane 75-27-4 82608 BR
3/8/2005 25007678 112705 Brancfcnn 75-25-2 82608 BIlL
3/9/2005 25007678 112705 Brart1nhane 74-83-9 82608 BRL
3/8/2005 25007578 112705 Carbon /8so/fide 75-15-0 82608 BR
3/82005 25117678 112705 Car-bcar tetrathlor/de 58-23-5 2608 BR
3/82005 25007678 112705 CBIac6enzene 108-90-7 82608 BR
3/8/2005 25007678 112705 ChIaoi.nancfl1Jlane 124-48-1 82608 BR
38/2005 25007678 112708 ChIao8hane 75-00-3 82608 BR
38/2005 25007678 112705 Cha4ccm 67-66-3 82608 BR
3/82005 25437678 112705 Chkranethane 74-87-3 82608 881
3/82005 25007678 112705 cis-l2-D4chIactrene 156-59-4 82608 BR
38/2005 25007678 112705 ciS-13-Dchkl-cprop000 10061-01-5 82608 BRL
38/2005 25007678 112705 Dtwananhane 74-95-3 82608 BR
3/8/2005 25437678 112705 Dau66uanhane 75-61-6 82608 BR
38/2005 25107678 1/2705 EUr4bonzene 100-41-4 8260B BR
38/2005 25007678 112705 Heaachtactrjla4jerre 87-66-3 82608 BR
3/812005 25007678 112705 IsWrq4hmIPE 108-20-3 82608 BR
38/2005 25007678 112705 Isqarc959/onzene 98-82-8 82608 BRL
382005 25007878 112705 m.p-Xylenes 136777-61-2 82608 BR
3/8/2005 25067678 112705 Methf/94kcneMEK 75-93-3 8260B 881
3/8/2005 25007678 112705 Meth4 iochde 74-68-4 82606 601
3/8/2005 25067678 112705 Methl4 1-buty
8her JMTBE 1634-04-4 82608 BR
3/8/2005 25007678 112705 Mchkxida 75-09-2 8260B BR
382005 25007678 112705 n-But.berrzarre 104-51-8 82608 BIlL
382005 25007678 112705 n-Prup4bmzene 103-65-1 82608 BR
38/2005 25007678 112705 r4apthaIone 91-20-3 82608 BR
38/2005 25607676 112705 o-Xylene 5-47-6 82608 BR
38/2005 25007678 112705 p-/sc6rWyflcluene 99-87-6 82608 BR
3/82005 25607678 112708 sec-But9/enzmre 135-98-8 82608 BR
3/8/2005 25007678 112705 Strene 100-42-5 82608 BR
3/8/2005 25007678 112705 ert-Buttarnzene 98-06-06 8260B 881
3/82005 25007678 112705 Telrachkwoeharre 127-18-4 8260B BRI
38/2005 25007678 112705 duese 108-68-3 82608 BR
38/2005 25007678 112705 t2-J/chlaoethene 155-60-5 8260B BRI
3/8/2005 25007678 112705 ans-13-DchIcrrqene 10061-02-6 8260B BRI
3/8/2005 25007678 112705 TrichIaohene 79-01-6 82608 BR
3/812005 25007678 112705 TrichIofiuorcmhane 75-60-4 26GB BR
3/8/2005 25067678 112705 a06ate 75-15-0 82608 BR
3/82005 25067678 112705 14cI4aide 75-01-4 82608 BR
3/82005 25007678 112705 C5-C8Ahphatjcs N/A MADEPVPH BR
3/8/2005 25007678 112705 C9-ClOkanat4cs N/A MADEPVPH BR
25007678 C9-Cl28phics N/A MADEPVPH BIlL
5.2 /Ig4g
52 /19/99
52 /1919
10 pMg
5.2 pg/kg
5.2 /i94g
5.2 pg8g
5.2 ig/kg
10 pg/kg
5.2 1949
10 pg/kg
10 pg/kg
52 .1949
5.2 Jig/kg
10 pg/kg
5.2 pg/kg
52 pglcg
10 /1949
10 pg/9g
5.2 pg/kg
10 19/kg
10 pg/kg
5.2 /1949
10 /19/99
10 JgMg
52 pg/kg
10 /1919
10 69/10
21/1949
lOU pg8g
100 JIg/kg
3.1 pg/kg
5.2 pg/kg
5.2 /1g4g
5.2 /1949
5.2 igArq
10 pgMg
10 pg8g
8-2 pg/kg
5.2 pgikg
5.2 JIg/kg
10 pgArg
5.2/19/19
10 pg/kg
52 /1989
52 pg4cg
5.2 /19/19
10 /1919
6.3 /19/kg
16 .1949
5.2 pgflcg
10 /1949
16 1949
21 /19/kg
10 JIg/kg
5/2 pg/kg
10/1919
15 pg/kg
10 igflcg
63/19/99
52 /19/19
16 41949
16 pg/kg
5.2 pg/kg
21 pg/kg
10 pg/kg
5.2 pg/9g
5.2 /19-19
5.2 pg/kg
pg/kg
5.2 pg/kg
1/pg1g
I0 pg/kg
8.4 mg/kg
8.4 rng1g
8.4 rug/kg
112705
Appendix
Notiticalion of Intent UST Permanent Closure or Change-in-Service
UST-3 Form
Notice of Intent UST Permanent Closure of Change-tn-Service
Return completed form toFOR TANKS
AEUSECL
DWM Regional Office located in the area where the facility is located SEE MAP ON THE RACK a___________
OF THIS FORM FOR REGIONAL OFFICE ADDRESSES 4ecwed____________
LLC
Entity anpan
dd Fcittv ID If wflLinLJJ7
City County WThtT11 MPLJ
Stt74 City County ZipCode
Area Code Phone Number rea Code Phone P4jmber
Name LCIELTV Job Title_____________Phone Number17O c/i2
.Lii
ir I.tsIk14iLYi11
Contact local fire marshal Provide sketciti locating piping tanks and P.E or LG.with all ctosur site
soil sampling locations assessment reports bearing the signaturePlanentireclosureeventandsealoftheREorLGIfreleasehasSubmit dosure report in the format of not occurred the supervision signature orConductSite Soil Assessment UST-12 çncluding the form UST2 seal of or L.G is not required
thirty 30 days following the siteIfremovingtanksorclowrginplacerefer to -estigation Keep closure records for three yearsAPIPublication2015CleaningPetroleum
Storage Tanks and l4 Removal arid lfareleassfromthetankshasoccurred theDisposalofUserUndergroundPeUoIe.urn site assessment portion of the tank closure
Storage Tanks must be conducted under the supervision of
ConitactorName /\1 OKiA.kLi11t bjI ij
Address -kjdSei242..iE State pCodeLL4
ContadPerson5c-1T 1Uz Phone No 35 44
PitmaCofanttjSflJThL cJ14iT Phone No 74-
LI
Tart ID Tar Capaczy Last Contents Proposeii ctivity
Removal Anandonment Place New Contents Sci
lJ
Lu n-acne ssionat teem cm
provides supervision for closure or change-in-service site assessment activities and signs and seals all closure reports Otherwise thmrty 30 day notice
is reguired
.W.ORTO8EPERFORMEDBy
_t
understand that can oe netii responsible tom envirorrnentaI damage resulting from the improper disposal
of my USs Read note on me Dacl of mrs tomi
offaI 4D9/irfC-JIC7 Lok1th/MsT
Signature Date Signd SCHEDULED REMOVAL DATE Nolify your DWM Regional.--1 Office 48 hours before this
_________ddremovst
Yellow Copy Central OfficelJT-3 Rev p-iRegional Off ce Pink Copy Owner
Appendix
Site Investigation Report for Permanent Closure or Change-in-Services of UST
UST-2 Form
Appendix
Certificate of UST disposal
tx yAiLIOY41LTcT
TM cU.ictiCI Ce
Jth 14 .3Z iLbPJL212b1tL4L34
1eiP 1O4 f2____
TP4O 74-Z1.4
rc pi 4oicitJtMkIACUVW
ND se esoritpoethn i1iiPE.-vth___ ___ive PE iLG
utk NIUSNWRQAQOb1dcrsnItt
ko4 fii-4b
WFu iI
-.-I
VbISoi-qov
rirrr
LL
Iriy MmRd.1Id dtKfliY4eCioU.rpj.and
rt
j2vzr a14 /izZrr
03/24i0 1204 FAX [phone]_CRESCENT RESOuRCES INC
Th KEVIN OOIRTY Ppe ot iO624 15244 011
NC
OO2
17O443O72 Fronr RON SANTINI
tPE ant
bt QOQLLL
Mt.lID
ci
6-ts fi _______
boe
Ta
çL
03/23/05 1223 FAX [phone] CRESCENT RESOURCES INC
Environmental and Industrial Serviees
8o 484 High Point NC Phone [phone] FAX [phone]
TANK DISPOSAL MANIFEST
Timk OwerAjthonzed ReprasenttIvE N3rfle süd Mailing AkhessC/-actq
/1517 LL Tt Lfr 1tL
z-
eripaonOrTsnks
Thuk caeadty revious Contcnrs Comm
-------
Tauk OwnØ4uthpred Reprentive tiflentioii The imdusgned cenifethai the above Jisted stoge
lanks ba been removed from the pem ses uf the aek Owner
FypdN MouhlDayff ear
Transpertiev The UdCSZfled CCXtifleS diet the abeve listed StOIBe t1cs have been rranspoiied to AtEvflm6nWandlbduzirialSeivices 27lSlJwhiriØ RiM ithleN.C 272w
dt/f1
DLcpaJ Cºr11caLJon The usigne6cthiIIcs thÆt 1e above-named stuxsge ranks have been cutPcedacceptedbythe-mebIretydllnhdflj1y
Reeyeiing Piy iiQ
Er fttPrgWimze
--
MonflWJayTthr
Appendix
Copy of all laboratory analytical records and Chain-of-Custody
Case Narrative
Date 3/17fl5
Company Duke Energy Corporation Client Project ID 05-MAR-0199
Contact Jay Perkins Prism COC Group No G0305190
Address 13339 Hagers Ferry Rcad
Huntersvllle NC 28078
The attached Laboratory Report
contains the analytical results for the project identified above and inchides Quality Control Data and
Chain-of-Cuskxiy copy
Data qualifiers are liagged individually on each sample Key Reference for Ihe data quahflers appears at the bottom of this page
Quality cotWol statements andlor sample speolfic remarks are included in the sample comments section of the
laboratory report for each sample affected
Please call if you have any questions relating to this analytical report
Data Reviewed by Paula Gilleland Project Manager MgelD Overcash
Signature çLJL ç4 Signature
Review Date 311 7/05 Approval Date 3/17105
Data Qualifier Key Reference
Result outside of QC Umits
Compound also detected in the method blank
DO Compound diluted out
Estimated concentration calibration range exceeded
The analyte was positively identified but the value is estimated below the reporting limitJHEstimatedconcentration with high bias
JL Esfimatedconcentrationwithahw
Amatrixeffactispresent
Tentatively Identified compound The concentration is estimated
Note This report should not be reproduced except in its entirety without the wntten consent of Prism Laboratodes Inc
449 Springbrcok Road Box 240543 Chailotte NC 28224-0403
Phone [phone] Toll Free 8001529-6364 Fax [phone]
F\comnn\casenantjve Revised 4/20104 Revised 4/20/04
Project ID 05-MAR-0199
Sample Matrbc Soil
Laboratory Report
3/17/05
Client Sample ID 25007675
Prism Sample ID 112702
COG Group G0305190
Time Collected 03108/05 12.00
Time Submitted 03/08/05 1555
Percent Solids Determination
Percent Solids 83.2 SM2540 03/09/05 1450 ftrown
5035
5035
5035
826GB
92608
8260B
82608
826DB
8260B
8260B
826GB
826GB
82608
82608
82603
82608
826GB
826GB
826GB
826DB
82608
826DB
826GB
03/09/05 000 Ibrown
03/09/05 000 Ibnn
03/09/05 000 Ibrown
03115105 837 kcarvgotto Q03831
03115/05 837 kcavvigoIto 003831
03/15/05 837 kanotto 003831
0315/05 837 kcamplgolio Q03831
0315/05 837 kcanlgobo 003831
03/15/05 837 kcanplgotto 003831
03115/05 837 kcampigotto 003831
03/15/05 837 kcampgoeo Q03531
03/15/05 837 kcaniplgctto 003831
03115105 837 kcwnpigotto Q03831
03/15/05 837 kcamplgotb 003831
03/15/05 837 kcampigottr 003831
03/15/06 837 kcamplgotla 003831
0315/05 837 kcampigotb 003831
03/15105 837 kcamplgolto 003831
03/15105 837 kcamplgolto 003931
03/15/05 837 kcanpigotto 003831
03/15/05 837 kcenplgofls 003831
03/15/05 837 keamplgotte Q9393j
03/15/05 8.37 kca7npigolb 003831
449 Sprlrigbrook Road P.O Box 240543 Charlotte NC 23224-0543
Phone [phone] loll Free Number 1-809/529-9364 Fax[phone]
NC Certification No 402
SC Certilication No 99012
NC Dking Water Cert No 37735
FL Certification No E87519
Duke Energy Corporation
Aftn Jay Perkins
13339 Hagers Ferry Road
Huntersvdle NC 28078
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/lime ID
SamDIe Welciht Determination
Weight Bleulfate 5.91
Weight Blsulfate 6.14
Weight Methanol 5.31
Volatile Oceanic Comoomds by GC/MS
11.12-Tetrachioroethane BRL pg/kg 5.1 0.68
111-Trithloroethane BRL pg/kg 5.1 0.83
1122-Tetrathloroethane BRL pg/kg 5.1 0.62
112-Trichloro-1.22-Tdfluoroethane SRI.jig/kg 10 2.1
112-Tichloroethane BRL pg/kg 5.1 0.49
11-Dichloroethane SRI pg/kg 5.1 0.98
11-Dichioroethene BRL pg/kg 5.1 0.75
lj-Oichloropropcne BRL pg/kg 5.1 0.87
123-Trlchforobenzene BRI pg/kg 10 3.6
123-Trichioropropane ERL pg/kg 5.1 0.26
124-Tdchlombenzene BRL pg/kg 10 3.5
124-Trlrnethylbenzene SRI pg/kg 10 3.7
12-Dlbromo-3-thtoropropane BRL pg/kg 5.1 1.4
12-DibromoethaneEDB SRI pg/kg 5.1 0.51
12-Dlchlorobenzene BRL pg/kg 10 2.4
12-Dlthloroethane BRL pg/kg 5.1 1.2
12-Dichloropropano BRL pg/kg 5.1 1.1
1A5-Tflmethbenzene BPJ pg/kg 10 3.8
13-Dicblombenzene BRL pg/kg 10 2.9
l3-Dlchloropropane SRI pg/kg 5.1 0.91
Page of 16
Duke Energy Corporation
Attn Jay Perkins
13339 Hagers Ferry Road
Uuntersville NC 28078
Laboratory Report
3/17105
Client Sample ID 25007675
Prism Sample ID 112702
COC Group 30305190
lime Collected 03108/05 1200
Time SubmItted 03/08/05 1555
449 Springbrook Road P.O Box 240543 CharIotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/5296364 Fax [phone]
NC Cerlitication No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
FL Certification No E87519
Project ID 05-MAR-01 99
Sample Matrix Soil
Parameter Result Onit Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
14-Dichlorobenzene BRL pg/kg 10 23 82509 03/15/05 837 kcamplgotto 003831
4-Dichorobutane BRL pg/kg 10 6.5 82609 03/15/05 837 kcampigotto 003831
22-Dichioropropane BRI pg/kg 5.1 0.92 826DB 03115105 837 kcarnplgotto 003831
2-Chloroethyl vinyl ether BRL pg/kg 10 0.79 82609 03/15/05 837 kcampigotto 003831
2-Chiorotoluene BRL pg/kg 10 2.5 82609 03115/05 837 kcamplgotto 003831
2-Hexanone BRL pg/kg 51 0.64 826DB 03115/05 837 kcampigotto QfJ333j
4-Chtoluene BRL pg/kg 10 2.6 82608 03/15/05 837 kcmwgotto 003831
4-Methyt-2-pentanone MIBK BRL pg/kg 10 093 826DB 03/15/05 837 kcamptgotto 003831
Acetone BRL pg/kg 20 5.2 82608 03/15105 837 keamplgotto 003831
Aaolein BRL pg/kg 100 5.5 826DB 03115/05 837 kcampigouo 003831
Acrdonitiile BRL pg/kg 100 2.1 82609 03/15105 837 kcamplgotto 003831
Benzene BRL pg/kg 3.1 0.99 826DB 03115/05 837 campigotlo 003831
Bromobonzene BRL pg/kg 5.1 0.72 826DB 03/15105 837 kcampigotlo 003331
Bromochiorornethane BRL pg/kg 5.1 0.83 82608 03/15/05 837 kCarTlPigOttO 003831
Bromodichioromethane BRL pg/kg 5.1 0.63 82608 03/15/05 837 kcampgo1to 003831
Bromoform BRL pg/kg 5.1 0.82 826DB 03/15105 837 kcamplgotto Qi333j
Bromomethane BRL pg/kg 10 0.80 828DB 03/15/05 837 knplgo8o 003831
Carbon disuifide SRI pg/kg 10 0.73 62608 03/15/05 837 kcmpgotto Q03831
Carbon tetrodiloride BRL pg/kg 5.1 0.78 82608 03/15/05 837 kcamplgotto 003831
Chlorobenzene BRI pg/kg 5.1 0.87 826DB 0315/05 837 kcampigotto 003831
Chlorodibromomethane BRL pg/kg 5.1 1.0 826DB 03/15/05 837 kcampigotto 003831
Chioroethane BRL pg/kg 10 12 826DB 03/15/05 837 kcampigotlo 003831
Chloroform BRL pg/kg 5.1 0.63 82608 03/15/05 837 kcamplgollo 003331
Chloromethane BRL pg/kg 10 0.50 82608 03/15/05 837 kcarnplgotto 003831
cls-12-Dlchloroelhene BRI pg/kg 5.1 0.88 82608 03/15/05 837 ktenlv4oollo 003831
ds-13-Dichtoropropene BRL /g/kg 5.1 1.1 82608 03/15/05 837 kcamplgolto 003831
Dibromomethane SRi pg/kg 5.1 0.46 82608 03115/05 837 kcampigolto 003831
DlchlorodJlluorcmethane BRL pg/kg 10 0.64 82605 03/15/05 837 kcamplgotto 003831
Page of 16
F41 Ske MWP4
Duke Energy corporation
Attn Jay Perkins
13339 Hagers Feny Road
Huntersviile NC 26078
Laboratory Report
3/17/05
Client Sample ID 25007675
Prism Sample ID 112702
COC Group G0306190
Time Collected 03/08/05 1200
Time Submitted 03/08/05 1555
Ethylberizene
Hexachlorobutadierie
isopropyl ether IPE
tsopropylbenzene
mp-Xylenes
Methyl ethyl ketone MEK
Methyl iodide
Methyl t-butyl ether M1BE
Methyhoe chloride
n-Butylbenzene
n-Propytbenzene
Naphthalene
o-Xlene
p-lsopropyltoluene
seo-Butylbenzene
Styrene
tert-Butylbenzena
Tetrachloroethene
Toluene
trans-12-Dichjoroethene
trans-i .3-Dichloropropene
Trichioroethene
Thchiorofluoromethane
Vinyl acetate
Vinyl chloride
BRL pg/kg-6.1 1.9
BRL pg/kg 15 5.1
BRL pglkg 5.1 0.98
BRL pg/kg 10 3.4
BRL pg/kg 15 4.2
BRL pg/kg 20 1.9
BRL pg/kg 10 1.2
BRL pg/kg 5.1 0.60
BRL pg/kg 10 1.2
BRL pg/kg 15 4.7
BRL pg/kg 10 4.0
BRL pg/kg 6.1 2.0
BRL pg/kg 5.1 1.6
BRL pg/kg 15 4.6
BRL pg/kg 15 4.9
BkL pg/kg 5.1 1.2
BRL pg/kg 20 5.7
BRL pg/kg 10 1.9
URL pg/kg 5.1 1.1
BRL jig/kg 5.1 0.95
BRL pg/kg 5.1 1.1
BRL pg/kg 5.1 1.0
BRL pg/kg 5.1 0.88
BRL pg/kg 10 0.69
BRL pg/kg-10 0.62
82609 03/15/05 837 kcanplgoso 003831
82609 03/15/05 837 kcarupigotto 003831
82609 03/15/05 837 kcsmplgolto 003831
82609 03115/05 837 kcsmpigotto Q03831
82600 03/15/98 837 kcropIgoUo 003831
8260B 03115/05 37 kconpigotte 003831
82606 03/15/05 837 kcamplgotto 003831
82603 03/15105 837 kcampigolto 003831
82603 03/15/05 837 kcamplgotto 003831
8280B 03/15/05 837 kcampigottD 003831
82600 03/15105 837 kcampigotbt 003831
8260B 03/15105 837 kcampigotb 003831
8260B 03/15/05-837 kcarnplgollo Q03831
8260B 03/15/05 837 kcanp3golto 003831
8260B 03115105 837 koarapigotto 003831
82606 03/1505 837 koxepigotto Q03831
826GB 03/15/05 837 kcanplgotto 003831
82603 03/15/05 837 kcanpigotto Q03831
8260B 03/15/05 837 kcwnplgolto 003831
8260B 03/15/05 837 kcarnpigotto Q03831
82606 03/15/05 837 kcarnpigouc 003831
8260B 03/15/05 837 kcarnplgotto 003831
82608 03115/05 837 kcarnplgolte 003831
82609 03115105 837 kcarnplgotto 003831
8260B 03/15/05 837 kcarnplgofto 003831
449 Sprlngbroojc Road P.O Box 240543 Charlotte NC 28224-0543Phone7O4/529.6394 TollFreeNumbe1-80o/52g354 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinkng Water Cert No 37735
FL Cetiftcatlon No E87519
Project ID 05-MAR-0199
Sample Matrix Soil
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Page of 16
Duke Energy CorporationMnJayPerkins
13339 Hagers Ferry Road
Huntersville NC 28078
Client Sample ID
Piism Sample ID
COC Group
Time Collected
Time Submitted
25007675
112702
G0305190
03/08/05 1200
03/08/05 1555
AU results are reported on dry-weight basis
BRL Below Reporting Limit
Esemated value between the Reporting Limit and the MDL
Angela Overcash V.P Laboratory Services
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1-800/529-6364 Fax [phone]
NC Certification No 402
Sc Certification 99012
NC Drinking Water Ceil No 37735
FL Certification No E87515
Project ID 05-MAR-01 99
Sample Matrbc Soil
Laboratory Report
3/17105
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor DateTflme ID
Surrogate Recovery Control Limits
Toluene-d8 98 81 128
Dibromoljuoromethane 105 57 -143
Bromoltuorobenzeno 102 77-128
Vobtite Petroleum Hydrocarbons by 1C-PDIF1D
CS-CS Ailphaflcs BRL mg/kg 8.4 4.2 MADEP VPH 03/09/05 1241 awhaeter 003658
C9-C10 Ammatics BRL mg/kg 8.4 4.2 MADEP VPH 03/09/05 1241 awheeler 003658
C9-C12 AiiFhatics BRL mg/kg 8.4 42 MADEP VPH 03/09105 1241 wheuIer 003658
Surrogate Recovwy Control Limits
25-Dibromotoluene-PlO 95 70-130
25-Dibromotoluene-FID 106 70-130
Samele Welabt DetermInation
Weight 21A8 MADEPVPH 03114/05 000 Ibrmn
Sample Comments
Page of 16
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
FL Cerlification No E875i9
Project ID 05.MAR-0199
Sample Matrix Soil
Laboratory Report
3/17/05
Client Sample ID 25007676
Prism Sample ID 112703
COC Group G0305190
lime Collected 03108/05 1230
Time Submitted 03/08/05 1555
Percent Solids Determination
Percent Soflde 84.7 825403 03109/05 1450 Ibrowi
5035
5035
5035
03/09/05 000 Ibroen
03/09/05 000 Ibrovn
03109/05 000 lbrc
Volatile Organic Compounds by GC/MS
1112-Tetrachtooethane ORL pg/kg 5.2 0.70
1.11-Trithloroethane URL pg/kg 5.2 0.85
i122-Tetrathtoroethane BRL pg/kg 5.2 0.63
l12-Irichloro-1.2.2-Tniluoroethane BRL pg/kg 10 2.1
112-Trichloroethane BRL pg/kg 5.2 0.50
1.1-Dlthloroethane BRL pg/kg 5.2 10
11Dich1oroethene BRL pg/kg 5.2 0.77
1-Dlchlorcpropene ORL pg/kg 5.2 0.89
123-Trlchlombenzene BRL pg/kg 10 3.6
123-Trichloropropane BRL pg/kg 5.2 0.27
124-Trichlorobenzene BRL pg/kg 10 35
124-Thmethylbenzene BRI pg/kg 10 3.7
l2-Dwcmo-3-chloropropane BRL pg/kg 5.2 1.5
1.2-Dromoethane EDB SRI pg/kg 5.2 0.52
12-Dichlorobenzene BRL pg/kg 10 2.5
12-Dichloroethane BRL pg/ks 5.2 1.2
12-Dichioropropane BRI pg/kg 5.2 1.1
135-TrimethyLeezene BRL pg/kg 10 38
13-Dichlorobenzene BRL pgkg 10 3.0
13-Dichioropropane BRL pg/kg 5.2 0.92
82600
82608
82608
82608
8260B
82608
.82608
8260B
82608
8260B
82609
8250B
32608
8260B
82608
82608
82808
82608
82608
82606
03/15/05 922 kcamplgotto 003831
03/15/05 922 kcarnPiotto Q03831
03/15/05 922 keampigotto 003831
03/15/05 922 kcanigotb 003831
03/15/05 9-22 kcarnplgotto 003831
03/15/05 922 keampigotto 003831
03/15/05 922 kC gOttO 003831
03/15/05 922 kcarrgotto 003831
03/15/05 922 koUo 003831
03/15/05 922 kcarnpigotlo 003831
03/15/05 922 kcamplgotto 003831
03/15105 922 kcampigotfo 003831
03/15105 922 kcanipigot$o 003831
03/15/05 922 kcampigotlo 003831
03/15/05 922 kcanplgotto 003831
03/15/05 922 kcanplgotto 003831
03/15/05 922 kcanplgcto 00383$
03/15/05 922 kcanptgotto 003831
03115105 922 kcanpigotto 003831
03115/05 922 kcamptgotlo 003831
449 Spnngbrook Read P.O Box 240543 Charlofte NC 28224-0543Phone[phone] Toll Free Number 1-80W529-6354 Fax [phone]
Duke Energy Corporation
Attri Jay Perkins
13339 Hagers Ferry Road
Huntersviile NC 28078
Parameter Result Units Report MDL Dilution Method AnalysIs Analyst
Batch
Limit Factor Date/Time ID
Saniole Weiaht Determination
Weight Blsuifate
Weight Bisulfate
Weight Methanol
5.69
5.61
5.25
Page of 16
14-Dlchlorobenzene
14-Dldiorobutane
22-Dlchloropixpane
2-Chloroeth4 vinyl ether
2-chlorotoluene
2-Hexanone
4Omloluene
4-Methyl-2-pentanone MIBK
Acetone
Acroisin
Acrylonltrile
Benzene
Brorncbenzene
Bromoditorornethane
BromcdcNoromethaie
Bromoform
Bromomethane
Cerbon bde
Carbon tetrachiorkie
hlorobenzene
thlorodjbwmomethane
chioroethanc
Chloroform
Chioromethane
cia-I 2-Dichloroelherie
cia-i .3-Dichloropropeno
Dibromomethane
Dichlorodifluoromethane
5.2 1.1
SRI pg/kg 5.2 0.47
BRL pg/kg 10 0.65
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phonó 704/529-6364 Toll Free Number 1-800529-8364 Fax [phone]
NC-Cerlillcation No 402
SC CertificatIon No 99012
NC Drinking Water Cert No 37735
FL Certification No E87519
Laboratory Report
3/17/05
Duke Energy Corporation Project ID 05-MAR-01 99 Client Sample ID 25007676
Aim Jay Perkins Sample Matrix Soil Prism Sample ID 112703
13339 Hagers Ferry Road COC Group 00305190
Huntersvfile NC 28078 Time ColIected 03/08/05 1230
Time Submitted 03/08/05 1555
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
BRI pg/kg 10 2.4 8260B 03/15/05 922 kcpigto 003831
ORL pg/kg 10 6.6 82606 03/15/05 922 kcarnpigotto 003831
SRI pg/kg 5.2 0.93 8260B 03/15105 922 kcampigoto Q383f
SRI pg/kg 10 0.81 82608 03/15/05 922 kcarnplgotb 003831
SRI pg/kg 10 2.8 8260B 03/15/05 922 kcainpigo4to 003831
SRI pg/kg 52 0.65 82608 03/15/05 922 kcaznpsgottcr 003831
BRL pg/kg 10 2.7 82606 03/15/05 922 kcainpgofto Q03831
SRI pg/kg 10 0.94 82606 03/15/05 922 kcarnplgotto 003831
DPI pg/kg 21 5.3 82608 03/15/05 922 kcarnpigotlo 003831
pj pg/kg 100 5.6 82608 0315/05 922 kcanpigoIr 003831
BRI pg/kg 100 22 82608 03/15/05 922 kcarnpigotto 003831
BRL pg/kg 3.1 1.0 8260B 03/15/05 922 kcarflplgotte 003831
BRL pg/kg 52 0.74 8260B 03/15/05 922 kcatnpigotb 003831
BRL pg/kg 5.2 0.85 82606 03/15/05 922 kcampigotb 003831
BRI pg/kg 5.2 0.64 82608 03/15/05 9.22 kcampigoo Q03831
BRL pg/kg 5.2 0.84 82600 03/15/05 922 kcamplgotto 003831
BRI pg/kg 10 0.82 82603 03/15/05 922 kcanplgotto Q03831
SRI pg/kg 10 0.75 82608 03/15/05 922 kcamplgotto 003831
BRI pg/kg 5.2 0.80 82606 03/15105 922 kcampigotto 003831
BRI pg/kg 5.2 0.89 8260B 03/15/05 922 kcrnp.gotto Q03831
BIll pg/kg 5.2 1.0 82608 03/15105 922 kcarnpigotto 003831
BRL pg/kg 10 1.2 8260B 03/15/05 922 kCarnPJgOUO 003831
BRL pg/kg 5.2 0.64 82606 03/15/05 922 kcarnpl9oUo 003831
SRI pg/kg 10 0.51 82608 03/15/05 922 kcarnpigofto 003831
SRI pg/kg 52 0.90 82608 03/15/05 922 otto 003831
BRL pg/kg 8260B 03/15/05 922 kcarnpigotto Q03331
82608 03/15/05 922 kcamplgotto 003831
82608 03/15/05 922 kcarnpouo 003831
Page of 16
Laboratory Report
3/17105
Client Sample ID 25007676
Prism Sample ID 112703
COG Group G0305190
Time Collected 03/08105 1230
Time Submitted 03108/05 lö55
NC Certification No 402
SC Certification No 99012___NC Drinking Waler Cert No 37735
FL Certification No E87519
Duke Energy Corporation Project ID 05-MAR-01 99
Attn Jay Peddns Sample Matrix Soil
13339 Hagers Ferry Road
Huntersville NC 28078
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Ethylbenzene BRL pg/kg 62 2.0 8260B 03/15/05 922 keunpigollo 003831
Hexaclilorobutadjene BRL pg/kg 16 5.2 8260B 03/15/05 922 kC5flpigOttO 003831
Isopropyl ether IPE URL pg/kg 5.2 10 82608 03/15/05 922 kcarnlIOflo 003831
Isopropylbenzene BRL pg/kg 10 3.4 8260B 03115/05 922 kcampigotlo 003831
m.p-Xylenes BRL pg/kg 16 4.3 82608 03/15/05 922 keampIgotto 003831
Methyl ethyl ketone MEK BRL pg/kg 21 2.0 8260B 03/15/05 922 kcampigotto 003831
Methyl iodide BRL pg/kg 10 1.2 82608 03/15/05 922 kCatrIPiOOttO 003831
Methyl t-butyl ether MTBE BRL pg/kg 5.2 0.61 82608 03/15/05 922 kcanigotb 003831
Methylene chloride BRL pg/kg 10 1.2 8260B 03/15/05 922 kcaoplgotto 003831
n-Butylbenzene BRL pg/kg 16 4.8 82608 03/15/05 922 kcaiçigotb 003831
n-Propylbenzene BRL pg/kg 10 4.0 82608 03/15/05 922 koampigotto 003831
Naphthalene BRL pg/kg 6.2 2.1 8260B 03/15105 922 kcpigoHo 003831
o-Xylene BRL pg/kg 52 1.7 82608 03/15/05 922 kcainplgolto 003831
p-Isopropyttoluene BRL pg/kg 16 4.7 82608 03/15/05 922 kcamplgotto 003831
sec-Butylbenzene BRL pg/kg 18 5.0 8260B 03/15/05 922 kcaingoUo 003831
Styrene BRL pg/kg 5.2 1.2 8260B 03/15/05 922 kcainplgotto 003831
tert-butylbenzene BRL pg/kg 21 5.8 8260B 03/15/05 922 kcamplgotto 003831
Tetrathloroethene BRL pg/kg 10 2.0 82608 03/15/05 922 kcarnpigottc 003831
Totuene BRL pg/kg 5.2 1.1 82608 03/15/05 922 kcernplgotto 003831
12-Dithloroethene BRL pg/kg 5.2 0.98 8260B 03/15/05 922 kCarnpiOltc 003831
trans-i3-Dlchloropropene BRI pg/kg 5.2 1.1 8260B 03115/05 922 kcPigotto 003831
Trichloroethene BRL pg/kg 5.2 1.0 8260B 03/15105 922 kCanWigolO 003831
Trichiofluoromane BRL p9/kg 5.2 0.90 82608 03/15/05 922 kCaflipigotto 003831
Vinyl acetate BRL pg/kg 10 0.71 8260B 03/15/05 922 kcarnplgotto 003631
Viiyl chloride BRL jig/kg 10 063 82608 03/15/05 922 kcarnpigotto QQ33j
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543Phone[phone] Toll Free Number 1-800/529-8364 Fc.7lj4/525.g4gg Page 70116
Duke Energy Corporation
Attn Jay Perkins
13339 Hagers Ferry Road
Huntersville NC 28078
Client Sample ID
Pzism Sample ID
COC Group
Time Collected
Time Submitted
25007676
112703
G0305190
03/08/05 1230
03/08/05 1555
Result Units Report MDL Dilution
Limit Factor
Method Analysis Analyst
Batch
Date/Time ID
Volatile Petroleum Hydrocarbons by GC-P1DIFID
C5-C8 AJiphaUcs BRL
CO-dO Aromatics
C9-C12 AJiphatics
Sample Welpht Determination
Weight 21.65 MADEP VPH 03/14/05 000 brown
Sample Comments
All results are repoitedon diy-weight
bests
BRL Below Reporting Limit
Estimated value bolwoen the Reporting Limit and the MDL
Angela Overcash V.P Laboratoiy Services
449 Spilngbrook Road P.O Box 240543 Charlotte NC 26224-0543
Photie 704/529-0304 Toll Free Number 1-800/529.6364 tax 7041525-0409
NC Certification No 402
SC Ceilificallon No 99012
NC DrinkIng Water Cad No 37735
FL Certification No 87519
Project ID
Sample Matrhc
Laboratory Report
3/1 7/05
05-MAR-01 99
Soil
Parameter
nglkg 8.3 4.1
BRL mg/kg 8.3 41
BRL mg/kg 8.3 4.1
Surrogate Recovery Control Limits
Toluene48 99 81 -128
Dlbromofiuoroniethane 106 67-143
Bromolluorobenzene 103 77-128
MADEP VPH 03/09/05 1941 awtweler Qj3658
MADEP VPH 03/09/05 1941 awteeler Q3858
MADEPVPH 03/09/05 1941 awheeler QJ3658
Surrogate Recovery Control Limits
25-Dlbromotoluene-PID 92 70-130
25-Dibromotoluene-FID 101 70-130
Page of 16
Duke Energy Corporation
Attn Jay Perkins
13339 Hagers Ferry Road
Huntersville NC 28078
Client Sample ID
Prism Sample ID
COC Group
Time Collected
Time Submitted
25C07677
112704
00305190
03/08/05 1245
03/08/05 1555
Percent Soflds Determination
Percent Solids 84.4 SM2540 03/09/05 1450 Ibrown
5.35 -g
5.40
4.93
5035 03/09/05 001
5035 03/09/05 000
5035 03/09105 000 Ibrown
449 Spilnybrook Road P.O Box 240543 Charlotte NC 28224-0543hónŁ704/529-6364 Toil Free Number 1-6091529-9364 Fax [phone]
NC Certilicatlon No 402
SC Ceililicatlon No 99012
NC DunkIng Water Cert No 37735
FL CertificatIon No E87519
Project ID 05-MAR-01 99
Sample Matrix Soil
Laboratory Report
3/17/05
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
SanrnleWelqhj DetermInation
Weight Blstdfate
Weight BisuIfate
Weight Methanol
Volatils Oroanic Comvounds by GC/MS
11l.2-Telrachloroethane BRI pg/kg 5.5 074 8260B O3/15 1005 kcanpigotto 003831
1lj-Tdchloroethane BRL pg/kg 5.5 0.91 8260B 03/15105 1005 kcamplgotto 003831
112.2-Tetrachleroethare ORL pg/kg 5.5 0.68 8260B 03/15105 1005 kcamplgotlo 003831
tI2-Trithloro-l22-Trjfiuomethane BRL pg/kg 11 2.2 82606 0315/05 1005 kcanpigoflo 003831
112-Trichloroethane BRL pg/kg 5.5 0.53 8260B 03/15/05 1005 kcanipigotto 003831
11-DlcNoroethane BRL pg/kg 5.5 1.1 82600 03115/05 1005 kcamplgotto 003831
1.1-Dichioroethene BRI pg/kg 55 0.82 82606 03/15/05 1005 keamplgotto 003831
11-Dichloropropene BRL pg/kg 5.5 0.95 82808 03/15/05 1005 kcampigotto 003831
1.2.3-Trichlorobenzene BRL pg/kg 11 3.9 8260B 0315105 1005 kcampigotto 003831
i23-Trlchlompropane BRL pg/kg 5.5 0.29 8260B 03/15/05 1005 kcaaotto 003831
124-Trithlorobenzene BRL pgfkg 11 3.8 8260B 03115/05 1005 kcampigotto 003831
1Z4-Trfmethylbenzene BRL pg/kg 11 4.0 82606 0315/05 1005 kcaJflPl9Otb 003831
12-Dilxomo-3-chloropropane BRL pg/kg 5.5 1.6 82608 03/15/05 1005 kcainpigotto 003831
12-Diuromodhane EDB BRL pg/kg 5.5 055 82606 03/15105 1005 kcanpigetto 003831
1.2-Dlchlorobenzerte BRL pg/kg 11 27 8260B 03/15/05 1005 kcauiplgono 003831
12Dithloroethane BRL pg/kg 5.5 1.3 82608 03/15105 1005 kcanpigoo 003831
l2-Dlchlovopropane BRL pg/kg 5.5 1.2 82600 03115105 1005 .kcarnplgotto 003831
13.5-Trimethylbenzcne BRL pg/kg 11 4.1 82608 0315/05 1005 kcanpigotto 003831
13-Dichlorobenzene BRL pg/kg 11 3.2 82608 03115/05 1005 kceiflpigolio 003831
13-Dichioroprapane BRL pg/kg 5.5 0.99 82608 03115/05 1005 kcanpigotio 003831
Page9ofl6
Duke Energy Corporation
Attn Jay Perkins
13339 Hagers Ferry Road
I-Iuntersville NC 28078
Project ID 05-MAR-01 99
Sample Matrbc Soil
Laboratory Report
3/17/05
Client Sample ID 25007677
Prism Sample ID 112704
COC Group 00305190
Time Collected 03/08/05 1245
Time Submitted 03/08/05 1555
449 $prlngbrook Road P.O Box 240543 Charlotte NC 28224-0543Phase7041529-6364 Toll Free Number 14001529-6364 Fax [phone]
IcA.yt1cL Enhwiwnt
NC CertiflcaLlon No 402
SC Certificallon No 99012
NC Drinking Water Cert No 37735
FLCetliIicalion No E87519
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/lime ID
1.4-Dithiorobenzene BRL jig/kg 11 25 82608 03115/05 1005 kcaupigotlo 003831
14-Dichiorobutane BRL pg/kg 11 7-1 8260B 03/15/05 1005 kcmpigono 003331
22-Dichioropropane BRL pg/kg 5.5 10 82608 03/15/05 1005 kcp4gotIo 003831
2-Chloroeth$Vinyl ether BRL pg/kg 11 0.86 82608 03/15/05 1005 kcampictIo Q03831
2-ChiorotoJuene BRI /k 11 2.8 826DB 03/15/05 1005 keanplgotto Q03831
2-1-lexanone BRL pg/kg 55 0.70 82608 03/15/05 1005 kcaiotto 003831
4-Chlorotoluene DPi pg/kg 11 2.9 8260B 03/15/05 1005 kcamvigotto 003831
4-Methyl-2--penlanone MIRK BRL pg/kg 11 1.0 826DB 03/15/5 1005 kCanWlgoUD Q03831
Acetone 67 pg/kg 22 5.6 826GB 03/15/05 1005 kcamplgotb 003831
Acrolein BRL pg/kg 110 6.0 8260B 03115105 1005 kcampigotto Q03331
Acrylonitrile BRL pg/kg 110 2.3 82808 03115/05 1005 kcampigoto Q03831
8enene BRL pg/kg 3.3 1.1 8260B 03115/05 1005 kcaplpoUo 003831
Brcmobenzene BRL pg/kg 5.5 179 82608 03/15/05 1005 kcplgotto 003831
Bromochkjromethene BRL pg/kg 5.5 0.91 826GB 03/15/05 1005 kcanplgotto 003831
BromocUchloromethane URL jig/kg 5.5 0.69 8260B 03/15/05 1005 kcwPootto 003831
Bromoform BR1.pg/kg 5.5 0.90 826GB 03/15/05 1005 kcmwlgofto 003831
Bromomethane SRI pg/kg 11 0.87 826DB 03/15105 1005 kcamplgotto 003831
Carbon dlsulilde BRL pg/kg 11 080 826DB 03115/05 1005 kcamptgotlo 003831
Carbon tetrachioride BRL pg/kg 5.5 0.85 82608 03115105 1005 mpigolto 003831
Chlorobenzene BRL pg/kg 5.5 0.95 82608 03/15/05 1005 kcampiotto 003831
CNorod1bromometne BR pg/kg 5.5 1.1 826DB 03/15/05 1005 kcampçctto 003831
Chloroethane BRI pg/kg 11 1.3 82608 03/15/06 1005 kmplgo4to Q03331
Chloroform BRI pg/kg 5.5 0.69 826GB 03/15/05 1005 kcamplgotto 003831
Chloromethane BR pg/kg 11 0.54 826GB 03/15/05 1005 kcampigotto Q038l
ds-1.2-Dlchloroethene BRL pg/kg 5.5 0.98 826GB 03/15/05 1005 kcanoUo 003831
cls-13-Dichloroprcjpene BR pg/kg 5.5 1.2 82608 03/15/05 1005 kcainpigotto 003831
Dibromomethane -spi pg/kg 5.5 0.50 826DB 03/15/05 1005 kcampgotto 003831
Dichtoiodllluorornethane BRL pg/kg 11 0.70 826DB 03/15/05 1005 kcarnplgotto 003831
Page 10 of 16
Duke Energy Corporation
Atm Jay Perkins
13339 Hagers Ferry Road
Huntersville NC 28078
Laboratory Report
3/17/05
Client Sample ID 25007677
Prism Sample ID 112704
COC Group G0305190
Time Collected 03/08/05 1245
Time Submitted 03/08/05 1555
NC Certification No 402
SC Certification No 99012
NC Driking Water Ceit No 37735
FL Certification No E87519
Project ID 05-MAR-0199
Sample Matrix Soil
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
Ethylbenzene BRL pg/kg 6.8 2.1 82608 03115/05 1005 kcaTpigoLto
Hexachlorobutadlene BRL pg/kg 17 5.5 82603 03/15/05 1005 kcanipigotto
Isepropyl ether IPE BRL pg/kg 5.5 1.1 82603 03/15/05 1005 kcaipigoUo
lsopmpylbenzene BRL pg/kg 11 3.7 82608 03/1505 1005 kcp1gotto
mp-Xylenes BRL pg/kg 17 4.5 82608 03/15105 1005 kcamplgotto
Methyl ethyl ketone MEK .30 pg/kg 22 2.1 826DB 03/15/05 1005 kcanplgotto
Methyl Iodide BRL pg/kg 11 1.3 8260B 0315/05 1005 kcamplgollo
Methyl t-butyl ether MTBE BRL pg/kg 5.5 0.65 82603 03/15/05 1005 kCpi9ott
Methytenechkide BRL pg/kg ii 1.3 8260B 03/15105 1005 kcatnpigotio
n-Butylbenzene BR.L pg/kg 1.7 5.1 826DB 0315/05 1005 kcarnpigotb
n-Propytbenzene BRL pg/kg 11 4.3 826DB 03/15105 1005 kcarnplgotto
Naphthalene BRL pg/kg 6.6 2.2 82608 03/15/05 1005 kcainpltto
o-Xyiene BRL pg/kg 5.5 1.3 82603 03/15/05 1005 kcamplgottt
p-tsopropyItokerie BR pg/kg 17 5.0 826DB 03/15/05 1005 kcarnpi1to
seo-Butytbenzene BRi pg/kg 17 5.3 826DB 03/15/05 1005 kcanplgolto
Styrene BRL pg/kg 5.5 1.3 826DB 03/15/05 1005 kfnPigc4to
tert-Butylbenzene BRL pg/kg 22 6.2 82608 0311M5 1005 kcampigofto
Tetrachioroethene BRL pg/kg 11 2.1 82608 03/15/05 1005 kcampotIo
Toluene BRL pg/kg 5.5 1.2 826DB 03/15/05 1005 koamplgotto
trans-I 2-Dlthloroethene BRL pg/kg 5.5 1.0 826DB 03/15105 1005 kcarnptgotto
trans-i 3-Dlchloropropene BRL pg/kg 5.5 1.2 82608 03115/05 1005 kcarnplgotto
Tricliloroethene BRL pglkg 5.5 1.1 826DB 03/15/05 1005 kcarnplgolto
Trichiorofluoromethane BRL jig/kg 5.5 0.96 8260B 03/15/05 1005 kcarnplgotto
Vinyl acetate BRL pg/kg 11 0.75 826DB 03/15/05 1005 kcarnplgotto
Vinyl chloride BRL pg/kg Ii 0.68 82608 03/15/05 1005 kcamplgotto 003831
Q03831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
Q03831
003831
003831
003831
Q03831
003831
003831
003831
446 Sprlngbrook Road P.O Box 240543 Chartotte NC 28224-0543
Phone [phone] Toll Free Number l-80W529-0364 Fax [phone] Page 11 of 16
Duke Energy Corporation
AIIm Jay Perkins
13339 Hagers Ferry Road
Jluntersville NC 28078
NC Certilicalion No 402
SC Certificallon No 99012
NC Drinking Water Cert No 37735
FL Certification No E87519
Laboratory Report
311
Client Sample ID
Prism Sample ID
COC Group
Time Collected
Time Submitted
25007877
112704
00305190
03/08/05 1245
03108/05 1555
Recovery Conhol Limits
99 81-128
98 67-143
BromofluorOtjene 102 77-128
Samole Wektht Determination
Weight 19.91
Surrogate Recoveiy Control Limits
25-Dlbromotoluene..plD 85 70-130
25-DibromotokJene-FID 101 70-130
MADEP WH 03114105 000 lbqm
All results are oepcedon diy-weight basis
BRL Bekw Reporting Limit
Estimated value between the Repoig Limit and the MDL
449 Springbrook Road P.O Box 240543 Charloti NC 29224-0543Phone[phone] Toll Free Number l-8001529-93M Fax [phone]
Project ID 05-MAR-01 99
Sample Matrix Soil
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Umit Factor DÆtelflme ID
Surrogate
Volatile Petroleum Hydrocjb by GC-PIDJFID
C5-C8 Aflphatics BRL
Toluene-d8
Dibromofluoromethane
C9-C10 Ammatics
C9.C12 Allphalics
mg/kg 8.3 4.1 MADEP VPH 03/10105 1257 awbeeler 003658
BRL mg/kg 8.3 4.1 MADEP VPH 03/10105 1257 awheeler 003658
BRL mg/kg 83 4.1 MADEP VPH 03/10105 1257 awbeeler QQ355
Angela Overcash V.P Laboratoiy Services
Page 12 of 16
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
FL Certification No.E87519
Laboratory Report
3/17/06
Client Sample ID 25007678
Prism Sample ID 112705
COC Group 00305190
lime Collected 03108/05 1300
Time Submitted 03/08/05 1555
Percent Solids Determinatiort
Percent So5ds 93.7 SM2540 03/09/05 1450 Ibrn
Sam Die Weight Determination
Weight Bisuffate
Weight Bisulfate
Weight Methanol
.449 Springbrook Road P.O Box 240543 Cha1oUe NC 28224-0543Phone[phone] Toll Free Number 1-809/529-5354 Fax [phone]
ronm.148
Duke Energy Corporation
Attn Jay Perkins
13339 Hagers Feny Road
Huntersville NC 28078
Project ID 05-MAR-0199
Sample Matrix Soil
Parameter ResUlt Units Report MDI.Dilution Method Analysis Analyst Batch
Limit Factor DateIlime ID
5.72 5035 03/09/05 000 Ibrcn
5.82 5035 03/09/05 000 lbrovm
4.81 5135 03/09/05 000 Ibtwfl
Volatile Oceanic Comoound by GCJMS
11.12-Tetrathloroethane BRL pg/kg 52 0.70 82608 03/15/05 1049 kcarnpigott 003831
111-Trichkroethane BRI pg/kg 5.2 0.86 82608 03/15/05 1049 kcaflWigOtb 003831
1.122-Tetrathlocoethane SRI pg/kg 52 0.64 82808 03/15/05 1049 kCaThPlgotb 003831
l12-Tichloro-122-Trjfluoroothane SRI pg/kg 10 2.1 82608 03/15/05 1049 koenpigofto Q03831
l12..Tirktiloroethane BRL pg/kg 5.2 0.50 8260B 03115/05 1049 kCaTbplgOttO 003831
11-Diddoroethane BRI pg/kg 6.2 1.0 8260B 03/15/05 1049 kcamPtiOttD 003831
11-Dldiloreethene BRL pg/hg 52 0.77 82608 03/15/05 1049 kcampigotto 003831
i.l.Dichlompropene BRL pg/kg 52 0.90 82608 03/15/05 1049 kcarnplgoflo -003831
f23-Trldwobenzene SRi pg/kg 10 3.7 82608 03/15/05 1049 kcarnplgotto 003831
l23..Trithlairopropane BRL pg/kg 5.2 027 82608 03/15/05 1049 kCmplgOttO 003831
124-Tdctilorobenzene SRI pg/kg 10 3.6 82608 03/15/05 1049 kcinpigotto 003831
124-Trlmefhytbenzenc BRL pg/kg IC 3.8 8260B 03/15/05 1049 kcarnpIgotto 003831
t2-Oibromo.3.ciiforopropane BRL pg/kg 5.2 1.5 82608 03/15/05 1049 kcarwigotlo 003831
12-Dibrernoethane EDB BRL pg/kg 5.2 0.52 82608 03/15/05 1049 kcamrgofto 003831
lhiorobenzene SRI pg/kg 10 25 8260B 03/15/05 1049 kcamiigotto 003831
12-Dlchioroethane BRL pg/kg 5.2 1.3 82608 03/15/05 1049 kearripigotto 003831
-1.2-Dichloropropane SRL pg/kg 5.2 .1.1 8260B 03/15/05 1049 kcauwigotto 003831
135-Trlmethylbenzene BRL pg/kg 10 3.9 8260B 03/15/05 1049 kcarnoUo 003831
13-Dithlorobenzene BRL pg/kg 10 3.0 82608 03115/05 1049 kcamiootto 003831
I3-Dlchlompmpane BRL pg/kg 5.2 0..93 82608 03/15106 1049 koampigotto Q03831
Page l3of 16
Am tlicI
Duke Energy Corporation
Attn Jay Perkins
13339 Hagers Fernj Road
Huntersville NC 28078
Client Sample ID
Prism Sample ID
COC Group
Time Collected
Time Submitted
25007678
112705
G0305190
03/08/05 1300
03108/05 1555
NC Certificati No 402
SC Certification No 99012
NC Drinking Water Cart No 37735
FL Certification No E87519
Project ID 05-MAR-01 99
Sample Matrix Soil
Laboratory Report
317/05
Parameter Result Units Report MDL Diluhon Method Analysis Analyst
Batch
Limit Factor Date/Time ID
14-Dichlorobenzene BRL pg/kg 10 2.4 82608 03/15/05 1049 kcampipotto Q03831
1.4-Dichiorobutane BRL pg/kg 10 67 8260B 03/15/05 1049 kcamplgotto 003831
22-Dichioropropane BRL pg/kg 5.2 0.94 62608 03/15/05 1049 kCaipigotto 003831
2-Chioroethyl vinyl ether BRI pg/kg 10 0.81 826GB 03/15/05 1049 kcamplgolto 003831
2-Chiorotoluene BRL pg/kg 10 2.6 82608 03/15/05 1049 kcampJolto 003831
2-Hexanone SRI.pg/kg 52 0.66 8260B 03115/05 1049 kcampigotto 003831
4-Chiorolojuene BRL pg/kg 10 2.2 8260B 03/15/05 1049 kcwnpJgolio 003831
4.MethyI2..pentanonaMIBx BRL pg/kg 10 0.95 8260B 03/15/05 1049 koampigolto Q03a31
Acetone 78 pg/kg 21 5.3 82608 03/15/05 1049 kcampigo4to 003831
Acrolein BRL pg/kg 100 5.6 8260B 03115/05 1049 kcamraotIo 003831
Acrylonitrile SRI pg/kg 100 2.2 82608 03/1M5 1049 npgotto 003831
Benzene BRI pg/kg 3.1 1.0 82608 03/15/05 1049 koamplgotto 003831
Bromobenzene BRL pg/kg 5.2 0.74 82608 03/15105 1049 kcampigollo 003831
Bromochloromethane 5JJ pg/kg 5.2 0.86 826GB 03115/05 1049 kcaenpigotto 003831
Bromodichlorpmethane BRL pg/kg 5.2 0.65 826GB 03/15/05 1049 kcarnplgotio 003831
Brornoform WL pgiig 5.2 0.85 826GB 03/15/05 1049 kcarflPlgotto 003831
Bromomethane BRL pg/kg 10 0.83 82608 03/15/05 1049 kcampigollo 003831
Carbon disulfide J3RL pg/kg 10 0.75 826GB 03/15/05 1049 kcarnpigono 003831
Carbon tetrachloide BRL pg/kg 52 0.80 8260B 03/15/05 1049 kaniplgotto 003831
Chlorobenzene BRL pg/ky 5.2 0.90 82608 03/15/05 1049 keamplgotto 003831
Chlorocrornomeane BRL pg/kg 5.2 1.0 82608 03/15/05 1049 kcarnplgotto 003831
Chioroethane BRL pg/kg 10 1.3 82608 03/15/05 1049 kcarnplgotto 003831
Chloroform BRI pg/kg 5.2 0.65 82608 03115/05 1049 keampigotto 003831
Chioromethane BRL pg/kg 10 0.51 826GB 0315/05 1049 Jccamplgotto Q03831
cis-1.2-DichjoroetAcne BRL pg/kg 52 0.91 826GB 0315/05 1049 kcarnpfgott 003831
CI8-1.3Dichioropropene BRL pg/kg 5.2 1.1 82508 0315/05 1049 kcamplgotto 003831
Dibromomethane SRI.pg/kg 5.2 0.47 8260B 0315/05 1049 kcarnplgotto 003831
0Ichiorodfluoronjj BRL pg/kg 10 0.66 8260B 03/15/05 1049 kcampigotto Q03831
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 28224-0543
Phone[phone] Toll Free Number 1-800/529-6394 Fax [phone] Page 14 o116
Duke Energy Corporation
Atm Jay Peiidns
13339 Hagers Ferry Road
Huntersville NC 28078
NC Certiffcation No 402
SC Certilicalion No 99012
NC Drinking Water Cest No 37735
FL Certification No E87519
Laboratory Report
3/17/05
Client Sample ID 25007678
Prism Sample ID 112705
CCC Group G0305190
lime Collected 03/08/05 1300
Time Submitted 03/08/05 1555
Road P.0 Box 240543 Charlotte NC 28224-0543
Phone [phone] roll Free Number 1-800/5294354 Fax[phone]
Project ID 05-MAR-0199
Sample Matrix Soil
Parameter ResUlt Units Report MDL Dilution Method Analysis Analyst Batch
Umit Factor Date/Time ID
Ethylbenzene BRI pg/kg 6.3 2.0 8260B 03/15/05 1049 koampigotto 003831
Hexachlombutac9ene BRL pg/kg 16 5.2 8260B 03/15/05 1049 kcanIgoUo 003831
Isopropyl ether IPE BRL pg/kg 5.2 1.0 826DB 03/15/05 1049 kcampigotto 003831
lsopropyibenzene BRL pg/kg 10 3.4 82608 03/15105 1049 kcinpigotto Q03831
mp-Xylenes BRL pg/kg 16 4.3 8260B 03/15/05 1049 kcampigotto 003831
Methyl ethyl ketone MEK BRL pg/kg 21 2.0 826DB 03/15/05 1049 kcampigotto 003821
Methyl iodide BRL pg/kg 10 1.2 826DB 03115105 1049 kcamplgotlo Q03531
Methyl t-butyi ether MTBE BRI pg/kg 5.2 0.62 82608 03115/05 1049 kcairçlgotlo 003831
Methylene chloride BRL pg/kg 10 1.3 826DB 03/15/05 1049 kcarnpigotlo 003831
n-Buiylbenzene BRL pg/kg 16 4.8 826DB 03/15/05 1049 kcanwigotlo 003831
n-Propythenzene BRL pg/kg 10 4.1 826DB 03/15/05 1049 kcamioono 003831
Naphthalene BRL pg/kg 6.3 2.1 82608 03/15/05 1049 kcarrigotto 003531
o-Xylene BRL pg/kg 52 1.7 826DB 03/15/05 1049 kmpigotlo 003821
p-Isopropyltoluene BRL pg/kg 16 4.7 82808 03/15105 1049 kcanipigotlo Q03531
sec-Butylbenzene BRL pg/kg 16 5.0 826DB 03/15105 1049 keampigotto Q03831
Styrene BRL pg/kg 5.2 1.3 82608 03/15/05 1049 kcarrgotto 003831
tert-Butylbenzene BRL pg/kg 21 5.8 82606 03/15/05 1049 kcampigotto 003831
Tetrachloroethene BRL pg/kg 10 2.0 82608 03/15105 1049 kcanigotlo 003831
Toluene BRL pg/kg 5.2 1.1 826DB 03/15/05 1049 kcampigotto 003831
trans-1.2-Dichlomethene BRL pg/kg 5.2 0.98 826DB 03/15/05 1049 kcampigotto 003831
trans-13-Dichloroproperie BRI pg/kg 5.2 1.1 826DB 03/1505 1049 kcampigotto 003531
Tiichloroethene BRL pg/kg 5.2 1.0 82608 03/15/05 1049 kcornplgotto Q03831
Trichlorofluorometjiane BRL pg/kg 52 0.91 826DB 03/15/06 1049 kcaapigotb Q03531
Vinyl acetate BRL pg/kg 10 031 82608 03115/05 1049 kcanplgotbo 003331
Wyl chloride BRL pg/kg 10 0.64 82808 03115/05 1049 kcarnpigotto 003831
Page 15 of 16
Duke Energy Corporation
Attn Jay Perkins
13339 Hagers Feny Road
Huntersville NC 28078
Client Sample ID
Prism Sample ID
COG Group
limo Collected
Time Submitted
25007678
112705
G0305190
03/08105 1300
03/08105 1555
All results aie mpoitedon thy-weight basis
BRL Below Reporting Limit
Estimated value between the Reporting limit and the MDL
Angela ft Overcash V.P Laboratory Services
449 Sprlngbrook Road PO BOA 240543 Charlotte NC 28224-0543
Phone [phone] Toll Free Number 1.800/529-9384 Fax [phone]
NC Certification No 402
SC Certification No 99012
NC Drinking Water Cert No 37735
FL Certification No E87519
Project ID 05-MAR-01 99
Sample Matrix Soil
Laboratory Report
3/17105
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Batch
Limit Factor Date/Time ID
The inLernal standard area responses for this sample were below the method control linults The
analysis was repeated with no improvement of the areas Matrix interference
is suspected
Surrogate Recovery Control LimIts
Toluene-d8 88 81-128
Dlbromofluoromethane 128 67 -143
Bromofluorobenzene 101 77-128
Volatile Petroleum Hyocarbons bY GC-PtD/FID
C5C8 Aliphatics BRL mg/kg 84 4.2 MADEP VPH 03/09/05 2126 aMee4er 003658
C9-C1O Aromatics BR mg/kg 8.4 4.2 MADEP VPH 03109/05 2126 awheelcr 003658
C9-C12 Aliphatics BR mg/kg 8.4 4.2 MADEP VPH 03/08/05 2t26 aeeIer 003658
Surrogate Recovery Control Limits
25-Dlbromototuene-PID 87 70-130
25-Dibrornotoruene-FID 101 70-130
Sample Weiciht Determination
Weight 21.39 MAflEP VPH 03114/05 000 Ibrown
Sample Comments
Page 16 of 16
Attn Jay Perkins
13339 Hagers Ferry Road
HuntersvflIe NC 28078
NC Cellillcation No 402
SC Certification No 90012
NC Drinking Water Con No 37735
FL Certification No E87519
Project 1D 05W1R0199
Level II QC Report
COC Group Number 30305190
3/17/05
Date/Time Submitted 318/05 1555
Volatile OraanlcComvounds by GCIMS method 8200B
1.lj2-Tetrachloroetjiane ND
1lj.Trlthloroethane ND
112.2-Tetrachforoeihane ND
112-Tæthloro-12.2-Tlfluoroethane ND
1j2-TrithIerosthwo ND
1.1-Dithlcroethane ND
l.1-Didroeitiene ND
ti-Dichioropropene ND
.23-Trlchlorobeazene ND
12.3-Trlchloropropane ND
124-Tjchlorcbenzone ND
12Trlmethylbenzene ND
12-Dibroino-3-th1onpropane ND
12-Thbmmoeth EDB ND
12-Dichlorobenzene ND
12-DichIoroethane ND
12-Dlchloropropane ND
l35-Trlmethylbenzene ND
13-Dichlcrobenzene ND
t3-Dlchloropropone ND
l4-Dichlorobenzene ND
l4-Dichlorvbufane ND
22-DIthkropropane ND
2-hlocoelhyl vinyl ether ND
2-chiorotoluene ND
2-Hexanone ND
4-hlorolo1uene ND
4-Meth4-2-pentanone MISK ND
Acetone ND
Acmleln ND
AcrylonMe ND
Benzene ND
Brornobenzene ND
Bromochlccomethane ND
Bromodichioromethane ND
Bromofonn ND
Bromomeihane ND
Carbon disulfide ND
Carbon tebathlonide ND
hlomberkzene ND
Ghlorodlbromomethane ND
Caloroethane ND
2.5 IJg/kg
2.5 pg/kg
2.5 pg/kg
10 pg/kg
2.5 pg/kg
2.5 pg/kg
2.5 pg/kg25pg/kg
10 pg/kg
2.5 pg/kg
10 pg/kg
10 119/kg
2.5 pglkg
2.5 pg/kg
10 p9/119
2.5 pg/kg
2.5 pg/kg
10 1.19/kg
10 pgikg
2.5 pg/kg
10 pg/kg
10 pg/kg
2.5 pg/kg
10 pg/kg
10 pg/kg
50 25 pg/kg
10 pg/kg
10 pg/kg
20 10 pg/kg
100 50 pg/kg
100 50 iigg
1.5 pg/kg
2.5 119/kg
2.5 pg/kg
2.5 pg/kg
2.5 pg/kg
10 pg/kg
10 pg/kg
2.5 pg/kg
2.5 pg/kg
2.5 pg/kg
10 pg/kg
oc Otd
ID
003831
003831
003831
003831
003831
003831
003831
003831
Q03831
003831
003831
003831
003831
003831
003831
003831
003831
003831
Q03831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
Q038
003831
Q03831
003831
003831
003831
449 Sprlngbrook Road P.O Box 240543 CharIotte NC 25V4-0543
Phone [phone] Toll Pr.e Number 14001529-6354 Pax 7041525-0409
Duke Energy Corporatbn
Method Blank CcnkiI
RsuIt RI 1/ni/I Un/Is
Page of
NC Certification No 402
SC Certification No 99012
NC Dunking Water Cert No 37735
FL Certification No E87519
Duke Energy Corporation Project 1D 05-MAR-a 199
AIIm Jay Perkins
13339 Hagers Ferry Road
Huntermelle NC 28078
Chloroform
Chioromethane
ds-12-Dichboethene
cis-13-Dlchtoropropene
Dibromomethane
Dichlorodlfluoromethane
Ethylbeozene
Hexachtorobutadiene
isopropyt ether IPE
isoprcpylbenzene
mp-Xylenes
Methyl ethyl ke$one MEK
Methyl iodide
Methyl t-butyi ether MTBE
Methytene chr1de
n8utylbenzane
n-Propylbenzerue
Naphihalene
o-Xylene
p-lsopropyltoluene
seo-Butylbenzene
Styrene
tert-Butylbenzene
Totrachlomethene
Toluemo
bans-12-DooetJene
trana-l.3-Dlthkuropropene
Tndiioroelhene
Trthorornethane
Vinyl acetate
Vinyl Chloride
Co
Result 1JITt Units
2.5 pg/kg
10 pg/kg
2.5 pg/kg
2.5 pg/kg
2.5 pg/kg
10 pg/kg
pg/kg
15 7.5 pg/kg
2.5 pg/kg
10 pg/kg
15 7.5 pg/kg
20 10 pg/kg
10 pg/kg
2.5 pg/kg
10 p9/kg
15 75 pg/kg
10 pg/kg
pg/kg
2.5 pg/kg
15 7.5 pg/kg
15 7S pg/kg
2.5
20 10 pg/kg
10 p9/kg
2.5 pg/kg
2.5 pg/kg
2.5 pg/kg
2.5 pg/kg
2.5 tjg/kg
10 pg/kg
10 pg/kg
OC Batch
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003831
003331
003831
003831
003831
003831
003831
003831
003831
003831
taboratoiy Control Sample
11-Doroethe
Benzene
Chlornbgnzene
Toluene
Thkroethejje
ReryikeReesyRangRsitMiountUnits
51.8 50 pg/kg 104 57-122
53.2 50 pg/kg 106 62-119
55.2 50 pg/kg 110 61-124
54.5 50 pg/kg 109 57-122
68.8 50 pg/kg 118 59-129
QCBthID
003831
003831
003831
Q03831
003831
449 Sprlngbrook Road P.O Box 240543 Charlotte NC 282244543
Phone[phone]-Toll Free Number 1-8001529.6364 Fax [phone]
Method Blank
Level II QC Report
3/17105
COC Group Number 00305190
Date/Time Submitted 3/3/05 1555
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page of
Duke Energy CorporallonMnJayPerkins
13339 Hagers Ferry Road
Huntersville NC 28078
NC Certification No 402
SC Certification Na 99012
NC Drinking Water Cert No 37735
FL Certification No E87519
Project ID 05-MAR-U 199
Level II QC Report
3/17/05
COC Grow Number 00305190
Date/Time Submitted 3/8105 1555
112702 11-DidlIonethene
Benzene
Chlorobenzene
Toluene
Trlthjoroelhene
51.3
50.8
532
52.5
58.5
449 Sprtngbrook Road-P.O Box 240543 Charlotte1 NC 28224-0543
Phone [phone] Toll Free Number 1-80W529-6364 Fax [phone]
Matrix Spike Reoovy
Space Range QC
SerIe emit Amount IJnit5 th ID
112702 11-Dichloroethene 54.1 50 p9/kg 108 44-140 003831
Benzone 52.1 50 pg/kg 104 46-136 003831
Chlorobenzene 53.5 50 p9/ku 107 47-135 003831
Toluene 54.6 50 pg/kg 109 47-136 003831
Tnchlomethene 61.1 50 pg/kg 122 45-141 003831
Matrix Spike Duplicate RPt
Sptke Rge Rge ocSnptetORasitAmOLMtUnftsBekh ID
50 pg/kg 103 44-140 0-23 003831
50 pg/kg 102 46-136 0-22 003831
50 pg/kg 108 47-135 0-22 003831
50 Jig/kg 105 47-136 0-22 003831
50 pg/kg 117 45-141 0-23 003831
Page of
Duke Energy Corporation
Atm Jay Perkins
13339 Hagers Feny Road
NC Certification No 402
SC Certification No 99012
NC Dunking Water Ceit No 37735
FL Certification No E87519
Project ID 05-MAR-0199
Level II QC Report
3/17/05
COG Group Number G0305190
Date/Time Submitted 3/8/05 1555
Huntersvffle NC 28078
Volatlle Petroleum HvcWocarbons by GC-PIDIFID method MADEP VPH
Recove RPD
Recovery Range RPD
Batch ID
9.23 mg/kg 71 70-130 52 0-25 Q03658
3.2 mg/kg 93 70-130 0-25 003658
9.23 mg/kg 105 70-130 17 0-25 Q03658
Analysis Note for C5-C8 Mphallcs RPD above the control limits
449 Sprlngbrook Road P.O Box 240543 Chaulotte NC 28224-0543
Phone [phone] Toll Free Number 1-800j529-6394 Fac 7041525.0409
Method Blank QCBatch
Reetit RL LUTe Unite
CS-CS Aliphatics ND 3.5 mg/kg Q03858
C9-CloAiromatlcs ND 35 mg/kg QJ3559
C9-Cl2AJIphaIics ND 3.5 mg/kg 003658
LaboraforyControl Sample RecovefySpdmRacyRange OC
Reach Amount Units Batch ID --CS-CS Aliphatics 182 15 mg/kg 121 70 -130 Q03658
C9-ClDAromaljcs 4.86 mg/kg 97 70-130 003658
C9-C12 Aliphatics 15.9 15 mg/kg 106 70 130 Q03658
--Matrix Spike Recovery
RangeReniu1tAmintLh%BatchiD
112702 CS-C8Ahphatics 11.3 923 mg/kg 122 70-130 003658C9-C1OAxoma 2.93 3.07 ma/kg 95 70-130 Q03658
C9-Cl2Mphatlcs 8.15 9..23 mg/kg 88 70-130 003658
Matrix Spike Duplicate
Spate
8anptelD Ranch Miami tints
112702 CS-CS Alipliatics
9C10 Ammatics
G9-C12 Aliphatics
6.59
2.97
9.71
Page ci
CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORMDukePowerAnIcLaboratory
Malt Code MGO3A2 Building 7405AnalyticalLaboratory13339HagersFerryRdChainofCustodyHuntersvllle28078 L0Qgee Date Time
...
LIMS ISampte CIaOf/72/..5o//_
S.rnples
Origtn.tIng
J1Project NameLLOf TAK Q-LOo-12Phon Noc49-3
3Cllent 4Foa NoOO9CLL
SiBuelnesa Unit l6Process-UL1 2j 7Rpsp Canter To5A-xit
5Projact ID JaAeUvIty ID 1OMaII Coda
cc4
Vertdortrns
Page of
DISTRIBUTiON
ORIGINAL to LABCOPYtoCLIENT
Cooler Tern
SAMPLE ROCJM
Ground WalerNPDES
Drinking Water
UST
RCRA Waste
12Chem
Desktop No
iMR HH
13SampJe Descrptlon or ID
Customer to complete all
appropriate non-shaded areas
72
14Coliecflon Information
bate Time L4
LABUSE ONLY
Lablb5oO7 2c1
5c1e 71j.t$o77742O77SL
.0
.0
.3iju
pi
5kJ
iUOsKI24 W-kADI
Acceuted
RenIhd ii
ROIl ulahed By
Datef7Ime-___j/2/
DatelTlme
tefflma Acc ted
Date/Tim
Pr1m
Date/Time
Oatatflme
$ealockd By
SwaVLoc.d By
Datefllme SeaIedlLo
Date/Time
Open
2CmnIi
9tefflme/7ts /7z0 .3
ZE
.3
-B
Vt
22Requested Turnaround
14 Days ____________
Days ____________
48 Hr__________
Add Cost WIll Apply
c-ro ico
Appendix
Photographs of closure activities
II
GEOSYNTEC CONSULTANTS
Photographic Record
Client Crescent Resources LLC Project Number GK3363
Site Name Elliot Street Tank Removal
Photograph
Date
March 2005
Direction
Looking South
Comments
Start of excavation
Photograph
Date
March 2005
Direction
Comments
View of exposed tank
Site Location 1017 Elliot Street
Charlotte NC
GEOSYNTEC CONSULTANTS
Photographic Record
Client Crescent Resources LLC Project Number GK3363
Site Name Elliot Street Tank removal
Photograph
Date
March 2005
Direction
Comments
Tank being secured for
removal
Photograph
Date
Site Location
March 2005
Direction
Comments
Tank Removed
1017 Elliot Street
Charlotte NC
GE0SYNTEC CoNsuLTANTs
Photographic Record
Client Crescent resources
LLC Project Number GK3363
Site Name Elliot Street Tank Removal
Photograph
Date
March 2005
Direction
Comments
Excavation backfihling
Photograph
Date
Site Location
March 2005
Direction
Comments
Completed backfill
1017 Elliot Street
Charlotte NC
Comments
Piping piping secondary
containment and
dispenser island
remnants
Photograph
Date
March 2005
Direction
Comments
Vacuum truck leaving
site Truck was not used
GEOSYNTEC CONSULTANTS
Photographic Record
Client Crescent Resources LLC Project Number GK3363
Site Name Elliot Street Tank Removal Site Location 1071 Elliot Street
Charlotte NC
Photograph
Date
March 2005
Direction
Appendix
Geologic logs for excavation
GEOSYNTEC CONSULTANTS
Soil Sample Record
Client Crescent Resources LLC Project Number GK3363
Site Name 1017 Elliot Street Tank removal Site Location 1017 Elliot St
__________________Charlotte NC
Soil Sample SSI
Date
March 2005
Location Excavation
floor below tank
Soil yellowish brown
sandy loam This soil
type was consistent from
surface to pit bottom
SI.IL SA\iPIJ.i ssi
Soil Sample SS2
Date
March 2005
SOIL Si
Location Material
surrounding tank
Material consists of
gravel approximately Y2
in size