HomeMy WebLinkAboutItem No 2 - Phase II Soil and Ground Water Assessment-OCRClarkson Street, LLC
Phase II Soil and Groundwater
Assessment
18.56 Acre Beazer Property
Charlotte, North Carolina
September 9, 2010
Project Number 0118084
Rick Tarravechia, P.G.
Principal-in-Charge
Michael Pressley, P.G.
Project Manager
ERM NC, PC
8000 Corporate Center Drive, Suite 200
Charlotte, NC 28226
704-541-8345
ERM i 18 ACRE BEAZER PROPERTY PHASE II
EXECUTIVE SUMMARY 1
1.0 INTRODUCTION 4
1.1 SITE DESCRIPTION AND BACKGROUND 4
1.2 PREVIOUS INVESTIGATIONS 5
1.3 PURPOSE 5
2.0 PHASE II INVESTIGATION ACTIVITIES 6
2.1 SOIL SAMPLING 6
2.2 GROUNDWATER SAMPLING 7
3.0 ENVIRONMENTAL SETTING 9
3.1 TOPOGRAPHY 9
3.2 SITE-SPECIFIC GEOLOGY 9
3.3 SITE-SPECIFIC HYDROGEOLOGY 9
3.4 EVALUATION CRITERIA 9
4.0 LABORATORY ANALYTICAL RESULTS 10
4.1 SOIL ANALYSES AND RESULTS 10
4.2 GROUNDWATER ANALYSES AND RESULTS 10
5.0 CONCLUSIONS 12
ERM ii 18 ACRE BEAZER PROPERTY PHASE II
LIST OF FIGURES
1 Site Location Map
2 Soil Boring Locations Map
3 Temporary Monitor Well Locations Map
LIST OF TABLES
1 Soil Analytical Results
2 Groundwater Analytical Results
LIST OF APPENDICES
A Soil Lithologic Logs and Field Screening Results
B Laboratory Analytical Data Sheets – Soil Samples
C Laboratory Analytical Data Sheets – Groundwater Samples
ERM 1 18 ACRE BEAZER PROPERTY PHASE II
EXECUTIVE SUMMARY
ERM NC, PC (ERM) conducted a Phase II Environmental Site Assessment
(ESA) at an 18.56 acre property (comprised of 10 parcels) located near
uptown Charlotte, North Carolina. The property is generally bounded by
West Morehead Street to the northeast, Post Street to the southwest, and
Interstate 77 to the northwest (the “subject property”). The purpose of the
Phase II ESA was to assess the subject property for potential soil and
groundwater impact associated with historical automobile repair and
maintenance facilities and historic manufacturing uses of surrounding
properties.
The Phase II ESA field activities were conducted in two phases. The first
phase occurred on July 8-9, 2010 and included the following tasks:
Advancement of six borings and characterization of subsurface;
Collection of soil samples at three of the six borings (one sample
per location) with laboratory analyses for volatile organic
compounds (VOCs) by EPA Method 8260B, and
Installation of temporary monitor wells at each of the six boring
locations for the collection and laboratory analyses of groundwater
samples for VOCs by EPA Method 8260B.
Chlorinated VOCs and petroleum VOCs were detected in select soil and
groundwater samples during the initial assessment phase. In order to
further characterize the extent of impact, ERM therefore re-mobilize to the
subject property on August 16-18, 2010 for the following tasks:
Advancement of 13 soil borings for the collection of two soil
samples per location for laboratory analyses for VOCs by EPA
Method 8260; and
Installation of three temporary monitor wells for the collection and
laboratory analyses of groundwater samples for VOCs by EPA
Method 8260B and for 13 target analyte list (TAL) metals by EPA
Methods SW6010/7470A.
Based on data collected during the Phase II ESA, the subject property is
underlain by a combination of fill material, saprolite, silty sand, and
fractured bedrock. Air rotary drilling was required to advance borings
ERM 2 18 ACRE BEAZER PROPERTY PHASE II
where bedrock was encountered. Groundwater was encountered at the
subject property at depths ranging from 11 to 25 feet below ground
surface (bgs). Groundwater is present in both the saprolite material and
within fractured bedrock.
Soil Sampling Results
During the initial phase of the Phase II ESA, soil sampling results
indicated that tetrachloroethene (PCE) is present at three of the boring
locations (B-1, B-3, and B-4) at concentrations ranging from 22 micrograms
per kilogram (µg/kg) to 47 µg/kg. These concentrations exceed the North
Carolina Department of Environment and Natural Resources (NCDENR)
Inactive Hazardous Sites Branch (IHSB) Soil Remediation Goal for the
Protection of Groundwater of 5 µg/kg.
Based on these results, an additional 11 soil borings were installed on the
subject property (including two in a stockpile located in the southeast
corner of the property) to assess for additional PCE impacts. Laboratory
analyses of the additional soil samples did not detect additional PCE or
other VOC impacts in soils on the subject property.
A summary of the soil sample analytical results is presented in Table 1.
Groundwater Sampling Results
Six temporary monitor wells (B-1 through B-6) were installed during the
initial phase of the Phase II ESA. Four of the wells (B-1 through B-4)
detected VOCs, with trichloroethene (TCE) being the most predominant
compound. TCE was detected in B-1 at 120 micrograms per liter (µg/L),
B-2 at 470 µg/L, B-3 at 68 µg/L, and B-4 at 1.7 µg/L. The North Carolina
Administrative Code (NCAC) 2L Groundwater Standard (2L Standard)
for TCE is 3 µg/L. Temporary monitor wells B-1 and B-2 detected
additional chlorinated VOCs as well as toluene, a petroleum derived
compound.
Based on these results, ERM installed three additional temporary monitor
wells (B-7 through B-9) to further evaluate groundwater conditions at the
subject property with respect to VOCs. TCE was detected in groundwater
at monitor well B-7 at 340 µg/L and at B-8 at 410 µg/L. No VOC
compounds were detected in groundwater at temporary monitor well B-9.
Groundwater samples collected during the second phase of Phase II work
also were analyzed for a target list of metal compounds. Several target list
ERM 3 18 ACRE BEAZER PROPERTY PHASE II
metals were detected in the B-7, B-8, and B-9 samples. Total chromium
was detected slightly above the 2L Standard of 0.01 mg/L in B-7 at 0.014
mg/L, in B-8 at 0.014 mg/L, and in B-9 at 0.062 mg/L. Iron was detected
above the 2L Standard of 0.3 mg/L in B-7 at 0.34 mg/L, in B-8 at 1.3
mg/L, and in B-9 at 1.3 mg/L. The manganese 2L Standard of 0.5 mg/L
was exceeded in B-7 at 0.53 mg/L.
A summary of the groundwater sample analytical results is presented in
Table 2.
ERM 4 18 ACRE BEAZER PROPERTY PHASE II
1.0 INTRODUCTION
This report presents the results of the Phase II Soil and Groundwater
Assessment activities conducted on behalf of Clarkson Street, LLC at an
18.56 acre property (comprised of 10 parcels) located near uptown
Charlotte, North Carolina. The property is generally bounded by West
Morehead Street to the northeast, Post Street to the southwest, and
Interstate 77 to the northwest (the “subject property”)(see Figure 1). The
Phase II assessment was conducted by ERM NC, PC (ERM) in accordance
with ERM’s proposal No. CLT1005024 dated May 20, 2010 and ERM’s
proposal No. CLT1007072 dated July 30, 2010.
1.1 SITE DESCRIPTION AND BACKGROUND
According to the Mecklenburg County Property Ownership and Land
Records Information System (POLARIS), the subject property is owned by
Beazer Homes Corporation and is comprised of the following 10 parcels
and acreages: 07314105- 1.70 acres; 07314201 - 3.31 acres; 07325602 - 0.68
acres; 07325601 - 0.65 acres; 07325501 - 2.75 acres; 07325207 - 4.94 acres;
07325209 - 0.64 acres; 07325210 - 0.52 acres; 07325211 - 0.70 acres;
07325213 - 2.67acres.
The earliest known activity on the subject property (from readily available
sources) is the presence of St. Catherine’s Gold Mine which operated on
the southeastern portion of the property in the late 1800s to early 1900s
(exact dates not known). Commercial development occupied the northern
three-fourths of the property through the 1900s, which included Duke
Power’s storage of electrical equipment, a stone cutting company, a
trucking/freight terminal, multiple automobile body and shops and
repair facilities, two retail gasoline stations, a restaurant, and assorted
small businesses. The southeastern quarter of the property contained a
cluster of single-family residential homes from at least the 1920s through
the 1980s. Many of the commercial businesses began leaving the property
in the late 1980s through the 1990s. Mass grading activities then took
place in 2005 for redevelopment of the property for mixed use (residential,
retail, office). Usage of the property since that time has been limited to
parking lot leases and most recently a temporary equestrian performing
arts show (Cavalia) which vacated the property in late June 2010.
ERM 5 18 ACRE BEAZER PROPERTY PHASE II
1.2 PREVIOUS INVESTIGATIONS
As many as 22 underground storage tanks (USTs), containing petroleum
products, have been present on the subject property since the 1920s.
Numerous reports have documented the removal of many USTs and
petroleum-impacted soil. Section 4.2 of ERM’s Phase I Environmental Site
Assessment for the subject property, dated June 10, 2010 (ERM Phase I
report), summarizes 21 previous environmental reports for the subject
property. The ERM Phase I report identified the following recognized
environmental conditions (RECs) for the subject property:
Historical automobile body shops and automobile repair facilities have
operated in the central and northeastern portions of the subject
property, including Tony’s Paint & Body, Turbo’s Auto Repair,
Finnell’s Foreign Car Clinic, Import Car Repair, Associated Transport
Motor Freight Lines repair/maintenance shop, and Autopare Paint &
Body Specialists. Autopare, located at 912 S. Clarkson Street (Parcel
No. 07325209), was listed on the RCRA Non-Generator of hazardous
wastes for handling spent non-halogenated solvents on the property.
Although no violations were reported, this listing indicates that
solvents have been handled on the property in the past. In addition, it
is possible that the other former on- site automobile service businesses
used solvents (halogenated and non-halogenated) in the past and the
potential for subsurface impact exists.
1.3 PURPOSE
The purpose of the Phase II ESA was to assess the potential for impacted
soil and groundwater from historic operations on the subject property and
historic manufacturing uses of surrounding properties.
ERM 6 18 ACRE BEAZER PROPERTY PHASE II
2.0 PHASE II INVESTIGATION ACTIVITIES
The Phase II ESA activities were conducted by ERM in two phases. The
first phase took place on July 8-9, 2010. A total of six borings were
installed in the northern portion of the property with soil samples
collected from three of the borings and groundwater samples collected
from temporary wells installed in each of the six borings.
The second phase of assessment activities took place on August 16
through 18, 2010 and included a total of 13 borings for the collection of
soil samples and three borings for the installation of temporary monitor
wells for the collection of groundwater samples. Soil boring locations
from both phases are shown on Figure 2 and temporary monitor wells
from both phases are shown on Figure 3.
2.1 SOIL SAMPLING
Soil borings installed during the first phase of assessment activities (B-1,
B-3, and B-4) were advanced with a truck-mounted drill rig equipped with
hollow stem augers and a split spoon sampler for the collection of soil
samples.
Soil borings installed during the second phase of assessment activities (B-
10 through B-20 and SP-1/SP-2) were advanced with a track-mounted
Geoprobedrill rig using 2-inch diameter by 5-foot long stainless steel
samplers equipped with disposable acetate liners.
As part of the soil sampling activities for both phases, the soil samples
were: (1) visually examined to characterize the subsurface geology; (2)
evaluated for visible evidence of contamination; and (3) field screened
with a photo-ionization detector (PID) for the presence of organic vapors.
Prior to use, the PID was calibrated using an isobutylene standard of
known concentration. Soil samples collected for field screening were
placed in Ziplock
bags and allowed to volatilize for 15 minutes. The PID
was then used to screen volatile organic vapors in the headspace of the
bags and then recorded. Soil descriptions and PID screening results are
documented on the soil boring logs included in Appendix A.
In addition to soil samples collected for field inspection and screening, soil
samples were submitted for laboratory analysis for volatile organic
compounds (VOCs) by EPA Method 8260B.
ERM 7 18 ACRE BEAZER PROPERTY PHASE II
Soil samples collected for laboratory analyses were transferred into
properly labeled, laboratory-supplied, sample containers and submitted
under chain-of-custody protocol to Shealy Environmental Services in West
Columbia, South Carolina.
Field sampling equipment was decontaminated prior to being brought on-
site with water and non-phosphate soap followed by a water rinse. Once
sampling activities were completed at each location, soil cuttings were
placed in a sealable steel 55-gallon drum and properly labeled until they
could be characterized for disposal. Upon the completion of each soil
boring, the boreholes were abandoned with granular bentonite clay.
2.2 GROUNDWATER SAMPLING
Borings B-1 through B-9 were drilled for the installation of temporary
monitor wells with a truck mounted drill rig capable of advancing hollow
stem augers or air rotary. Hollow stem augers were used to drill borings
B-3 and B-4 while the remaining borings were drilled using air rotary.
Fractured bedrock was encountered in borings B-1, B-2, B-7, and B-9,
which required a 6-inch air rotary button bit for advancement.
Upon the encounter of saturated soil, or a water-bearing fracture in the
bedrock wells, temporary monitor wells were constructed in each of the
boreholes using 2-inch inner diameter (I.D.) Schedule 40 PVC flush-
threaded casing and screen. The PVC screen and casing were lowered into
each of the open boreholes. A 10-foot length of slotted well screen with
machined 0.010-inch slot widths and a threaded bottom plug were installed
at the bottom of the wells. A solid section of PVC casing was placed above
the screened interval and extended to approximately two to three feet
above ground surface. The annular space around the wells was then filled
with a washed and graded medium sand to a minimum of two feet above
the top of the screen. Lithologic description logs for each of the temporary
well borehole locations are provided in Appendix A.
Once groundwater elevations stabilized in the wells, ERM utilized a mini-
Typhoon submersible pump to remove fines from the well pipe and sand
pack. Approximately 20 to 30 gallons of water was pumped from each well
during development activities. Development water from B-1 through B-6
was discharged onto the ground surface near the well head and
development water from B-7 through B-9 was containerized in 55-gallon
drums.
ERM 8 18 ACRE BEAZER PROPERTY PHASE II
Once the temporary wells were developed and allowed to recharge to the
initial measurement, ERM utilized new disposable polyethylene bailers and
twine to collect groundwater samples. The samples were placed in
laboratory-provided containers and packed in a cooler with sufficient ice to
maintain a temperature of 4º Celsius and sent via courier to Shealy
Environmental Services in West Columbia, South Carolina for analysis.
Groundwater samples collected from temporary wells B-1 through B-6
were analyzed for VOCs using EPA Method 8260. Groundwater samples
collected from temporary wells B-7 through B-8 were analyzed for VOCs
by EPA Method 8260 and a 13 target analyte list (TAL) of metals to assess
for potential impacts from an off-site, up-gradient source. The metal
samples were lab filtered using EPA Method 3030C and then analyzed
according to by EPA Methods SW6010/7470A.
ERM 9 18 ACRE BEAZER PROPERTY PHASE II
3.0 ENVIRONMENTAL SETTING
3.1 TOPOGRAPHY
Elevation at the subject property ranges from approximately 710 feet
above mean sea level (AMSL) in the southeast portion to approximately
650 feet AMSL in the northwest portion. Based on the topographic map, it
appears that there is a general topographic slope to the northwest, toward
Irwin Creek, which is approximately 250 feet northwest of the
northwestern property boundary.
3.2 SITE-SPECIFIC GEOLOGY
Based on data collected during the Phase II ESA, the subject is underlain
by a combination of fill material, saprolite, silty sand, and fractured
bedrock. Lithologic description logs for each borehole are provided in
Appendix A
3.3 SITE-SPECIFIC HYDROGEOLOGY
Groundwater was measured in temporary monitor wells at depths
ranging from 11 to 25 feet below ground surface (bgs). Wells B-1, B-2, B-7
and B-9 were installed within a water-bearing fracture of bedrock. The
remaining wells (B-3 through B-6 and B-8) were installed in saprolite soil.
The bedrock wells exhibited a high flow rate, as evidenced by a maximum
drawdown of only one foot after purging at 2 gallons per minute for 20
minutes (during well development). The saprolite wells produced
moderate recovery, with B-6 being the slowest (pumped dry during
development).
3.4 EVALUATION CRITERIA
Soil analytical results were compared to the NCDENR Inactive Hazardous
Sites Branch (IHSB) Soil Remediation Goals (RG) for the Protection of
Groundwater. Groundwater analytical results were compared to the
North Carolina groundwater standards set forth in Title 15A of the North
Carolina Administrative Code (NCAC) Section 02L .0202 (2L Standard).
ERM 10 18 ACRE BEAZER PROPERTY PHASE II
4.0 LABORATORY ANALYTICAL RESULTS
Soil and groundwater samples collected during the Phase II ESA were
submitted to Shealy Environmental Services in West Columbia, South
Carolina for laboratory analyses. The analytical results are presented in
the sections below.
4.1 SOIL ANALYSES AND RESULTS
Twenty-eight (28) soil samples were submitted for laboratory analyses for
VOCs. A summary of the soil analytical results is provided below and is
also presented in Table 1. The complete laboratory reports are included in
Appendix B.
Tetrachloroethene (PCE) was detected in three of the soil samples. PCE
was detected at B-1 at 2-3 feet bgs (22 µg/kg), B-3 at 9-10 feet bgs (23
µg/kg), and B-4 at 9-10 feet bgs (47 µg/kg). All PCE concentrations
exceed the NCDENR IHSB RG of 5 µg/kg.
4.2 GROUNDWATER ANALYSES AND RESULTS
Nine (9) groundwater samples were submitted for laboratory analyses for
VOCs as part of site assessment activities. Three of the samples also were
analyzed for 13 TAL metals. A summary of the groundwater analytical
results is provided below and is also presented in Table 2. The complete
laboratory reports are included in Appendix C.
VOCs were detected in six of the nine temporary wells installed on the
property. Trichloroethene (TCE) was the most predominant compound
with concentrations ranging from 1.7 µg/L to 470 µg/L. Five of the wells
containing TCE exceeded the 2L Standard for TCE of 3 µg/L. TCE was
detected in groundwater monitor wells installed in both saprolite and
fractured bedrock at the subject property.
Daughter compounds of TCE also were detected in groundwater samples,
including cis-1,2-dichloroethene (DCE) and trans 1,2-DCE. Cis-1,2-DCE
was detected in a groundwater sample at B-2 at 86 µg/L, which exceeded
the 2L Standard of 70 µg/L.
ERM 11 18 ACRE BEAZER PROPERTY PHASE II
Toluene was detected at low concentrations in B-1 (1.6 µg/L) and B-2 ( 3.8
µg/L) (the 2L Standard for toluene is 600 µg/L). Both of these temporary
wells were installed in the vicinity of former gasoline stations.
Several TAL metals were detected in the groundwater samples collected
at B-7, B-8, and B-9. Total chromium was detected slightly above the 2L
Standard of 0.01 mg/L in B-7 at 0.014 mg/L, in B-8 at 0.014 mg/L, and in
B-9 at 0.062 mg/L. Iron was detected above the 2L Standard of 0.3 mg/L
in B-7 at 0.34 mg/L, in B-8 at 1.3 mg/L, and in B-9 at 1.3 mg/L. The
manganese 2L Standard of 0.5 mg/L was exceeded in B-7 at 0.53 mg/L.
ERM 12 18 ACRE BEAZER PROPERTY PHASE II
5.0 CONCLUSIONS
Soil Sampling Results
During the initial Phase II site assessment, soil sampling results indicated
that PCE is present at three of the boring locations (B-1, B-3, and B-4) at
concentrations ranging from 22 µg/kg to 47 µg/kg. These concentrations
exceed the NCDENR IHSB Soil Remediation Goal for the Protection of
Groundwater of 5 µg/kg.
These borings were located in areas formerly used by automobile repair
facilities. Additional soil sampling activities would be required to
delineate the vertical and horizontal extent of PCE impacted soil.
Groundwater Sampling Results
VOCs were detected in six of the nine temporary monitor wells installed
on the subject property. TCE was the most predominant compound with
concentrations ranging from 1.7 µg/L to 470 µg/L. In five of the wells (B-
1, B-2, B-3, B-7, and B-8), TCE exceeded the 2L Standard of 3 µg/L. TCE
was detected in groundwater in monitor wells installed in both saprolite
and fractured bedrock. Based on the results of the Phase II ESA, VOCs
have impacted the shallow aquifer (saprolite and fractured bedrock) in the
northern portion of the subject property. Further assessment would be
necessary to delineate the vertical and horizontal extent of VOC impacts
to groundwater on the subject property.
The three temporary monitor wells sampled for 13 TAL metals (B-7, B-8,
and B-9) detected total chromium, iron, and manganese at concentrations
slightly above their respective 2L Standard. Further assessment would be
necessary (1) to determine if the metal detected in groundwater is
naturally occurring, and if not, (2) to delineate the vertical and horizontal
extent of metals impacts to groundwater the subject property
Figures
ERM, NC PC 1SITE LOCATION MAP
SOURCE: CHARLOTTE EAST, NC 7.5 MINUTE TOPOGRAPHIC QUADRANGLE (1988)
SITE
Figure
Subject Property
18.56 ACRE BEAZER PROPERTY
CHARLOTTE, NORTH CAROLINA
Sample IDSample Depth (feet)
S
a
m
p
l
e
D
a
t
e
Tetrachloroethene B-1 2-3 7-8-10 22 B-3 9-10 7-8-10 23 B-4 9-10 7-8-10 47 B-10 4-6 8-16-10 ND B-11 1-2 8-16-10 ND B-11 6-7 8-16-10 ND B-12 3-5 8-16-10 ND B-12 13-15 8-16-10 ND B-13 3-5 8-16-10 ND B-13 8-10 8-16-10 ND B-14 3-5 8-16-10 ND B-14 8-10 8-16-10 ND B-15 3-5 8-16-10 ND B-15 13-15 8-16-10 ND B-16 3-5 8-16-10 ND B-16 13-15 8-16-10 ND B-17 3-5 8-16-10 ND B-17 13-15 8-16-10 ND B-18 0-2 8-16-10 ND B-18 13-15 8-16-10 ND B-19 3-5 8-17-10 ND B-19 13-15 8-17-10 ND B-20 3-5 8-17-10 ND B-20 13-15 8-17-10 ND SP-1 6-8 8-17-10 ND SP-1 16-18 8-17-10 ND SP-2 6-8 8-17-10 ND SP-2 16-18 8-17-10 ND 5 Notes:BOLD values indicate an exceedence of Soil Remediation Goal ND = Not Detected above mimium quantitation limits ug/kg = Micrograms/kilogramVolatile Organic Compounds (VOCs) EPA Method 8260B (ug/kg)Inactive Hazardous Sites Branch Soil Remediation Goal (Protection of Groundwater)
Sa
m
p
l
e
I
D
Sample DateDepth to Water Below Ground Surface (feet)Chloroform Chloromethane cis-1,2-Dichloroethene trans-1,2-Dichloroethene Toluene Tetrachloroethene (PCE)Trichloroethene (TCE)Aluminum Barium Calcium Chromium Copper Iron Magnesium Manganese Sodium Zinc Mercury
B-
1
7-9-10 24.83
1
.
5
N
D
2
6
N
D
1
.
6
N
D
120 NA
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
B-
2
7-9-10 26.00
N
D
4.7
8
6
4.1
3
.
8
N
D
470 NA
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
B-
3
7-8-10 24.00
1
.
7
N
D
1
1
N
D
N
D
N
D
68 NA
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
B-
4
7-8-10 24.25
N
D
N
D
N
D
N
D
N
D
N
D
1
.
7
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
B-
5
7-9-10 15.50
N
D
N
D
N
D
N
D
N
D
N
D
N
D
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
B-
6
7-9-10 27.58
N
D
N
D
N
D
N
D
N
D
N
D
N
D
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
B-
7
8
-
1
9
-
1
0
1
6
.
6
5
7
.
1
N
D
3
4
N
D
N
D
1.9
3
4
0
1.1
0
.
6
2
2
4
0.019 0.014 1.3 12 0.53 18
N
D
0
.
0
0
0
1
3
B-
8
8
-
1
9
-
1
0
1
4
.
0
0
1
.
3
N
D
5
7
2
N
D
2
4
1
0
1.6
0
.
0
4
4
6
0.014 0.011 1.3 16
0
.
1
2
1
6
N
D
N
D
B-
9
8
-
1
9
-
1
0
1
1
.
7
0
N
D
N
D
N
D
N
D
N
D
N
D
N
D
0
.
2
3
0
.
0
6
5
8
0.062 ND 0.34 19
0
.
0
9
1
8
0
.
0
2
0
.
0
0
0
2
5
70
3
7
0
1
0
0
6
0
0
0
.
7
3
N
E
0
.
7
N
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0
.
0
1
1
0
.
3
N
E
0
.
5
N
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.
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o
t
D
e
t
e
c
t
e
d
a
b
o
v
e
m
i
n
i
m
u
m
q
u
a
n
t
i
t
a
t
i
o
n
l
i
m
i
t
s
NE
=
N
o
t
E
s
t
a
b
l
i
s
h
e
d
ug
/
L
=
M
i
c
r
o
g
r
a
m
s
/
l
i
t
e
r
V olatile Organic Compounds (VOCs) EPA Method 8260B (ug/L)
NC
2
L
G
r
o
u
n
d
w
a
t
e
r
S
t
a
n
d
a
r
d
Target Analyte List of Metals by EPA Method 6010C (mg/L)EPA Method 7470A (mg/L)
Tables
TABLE 1
SOIL SAMPLE ANALYTICAL RESULTS
18-ACRE BEAZER PROPERTY
CHARLOTTE, NORTH CAROLINA
Sample ID
Sample Depth
(feet) Sample Date Te
t
r
a
c
h
l
o
r
o
e
t
h
e
n
e
B-1 2-3 7-8-10 22
B-3 9-10 7-8-10 23
B-4 9-10 7-8-10 47
B-10 4-6 8-16-10 ND
B-11 1-2 8-16-10 ND
B-11 6-7 8-16-10 ND
B-12 3-5 8-16-10 ND
B-12 13-15 8-16-10 ND
B-13 3-5 8-16-10 ND
B-13 8-10 8-16-10 ND
B-14 3-5 8-16-10 ND
B-14 8-10 8-16-10 ND
B-15 3-5 8-16-10 ND
B-15 13-15 8-16-10 ND
B-16 3-5 8-16-10 ND
B-16 13-15 8-16-10 ND
B-17 3-5 8-16-10 ND
B-17 13-15 8-16-10 ND
B-18 0-2 8-16-10 ND
B-18 13-15 8-16-10 ND
B-19 3-5 8-17-10 ND
B-19 13-15 8-17-10 ND
B-20 3-5 8-17-10 ND
B-20 13-15 8-17-10 ND
SP-1 6-8 8-17-10 ND
SP-1 16-18 8-17-10 ND
SP-2 6-8 8-17-10 ND
SP-2 16-18 8-17-10 ND
5
Notes:
BOLD values indicate an exceedence of Soil Remediation Goal
ND = Not Detected above mimium quantitation limits
ug/kg = Micrograms/kilogram
Volatile Organic
Compounds (VOCs) EPA
Method 8260B (ug/kg)
Inactive Hazardous Sites Branch Soil Remediation
Goal (Protection of Groundwater)
TABLE 2
GROUNDWATER SAMPLE ANALYTICAL RESULTS
18-ACRE BEAZER PROPERTY
CHARLOTTE, NORTH CAROLINA
Sample ID Sample Date
Depth to Water
Below Ground
Surface (feet)Ch
l
o
r
o
f
o
r
m
Ch
l
o
r
o
m
e
t
h
a
n
e
ci
s
-
1
,
2
-
D
i
c
h
l
o
r
o
e
t
h
e
n
e
tr
a
n
s
-
1
,
2
-
D
i
c
h
l
o
r
o
e
t
h
e
n
e
To
l
u
e
n
e
Te
t
r
a
c
h
l
o
r
o
e
t
h
e
n
e
(
P
C
E
)
Tr
i
c
h
l
o
r
o
e
t
h
e
n
e
(
T
C
E
)
Al
u
m
i
n
u
m
Ba
r
i
u
m
Ca
l
c
i
u
m
Ch
r
o
m
i
u
m
Co
p
p
e
r
Ir
o
n
Ma
g
n
e
s
i
u
m
Ma
n
g
a
n
e
s
e
So
d
i
u
m
Zi
n
c
Me
r
c
u
r
y
B-1 7-9-10 24.83 1.5 ND 26 ND 1.6 ND 120 NA NA NA NA NA NA NA NA NA NA NA
B-2 7-9-10 26.00 ND 4.7 86 4.1 3.8 ND 470 NA NA NA NA NA NA NA NA NA NA NA
B-3 7-8-10 24.00 1.7 ND 11 ND ND ND 68 NA NA NA NA NA NA NA NA NA NA NA
B-4 7-8-10 24.25 ND ND ND ND ND ND 1.7 NA NA NA NA NA NA NA NA NA NA NA
B-5 7-9-10 15.50 ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA
B-6 7-9-10 27.58 ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA
B-7 8-19-10 16.65 7.1 ND 34 ND ND 1.9 340 1.1 0.62 24 0.019 0.014 1.3 12 0.53 18 ND 0.00013
B-8 8-19-10 14.00 1.3 ND 57 2 ND 2 410 1.6 0.044 46 0.014 0.011 1.3 16 0.12 16 ND ND
B-9 8-19-10 11.70 ND ND ND ND ND ND ND 0.23 0.055 58 0.062 ND 0.34 19 0.092 18 0.02 0.00025
70 3 70 100 600 0.7 3 NE 0.7 NE 0.01 1 0.3 NE 0.5 NE 1 0.001
Notes:
BOLD values indicate an exceedence of 2L Groundwater Standards
NA = Not Analyzed
ND = Not Detected above minimum quantitation limits
NE = Not Established
ug/L = Micrograms/liter
Volatile Organic Compounds (VOCs) EPA
Method 8260B (ug/L)
NC 2L Groundwater Standard
Target Analyte List of Metals by EPA Method 6010C (mg/L)
EPA
Method
7470A
(mg/L)
Appendix A
Soil Lithologic Logs and Field
Screening Results
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
ML 0 20 80 18.8
100 ML 0 20 80 9.5
3.1
100 ML 0 20 80 3.9
100 2.0
25-35 ft Bedrock; changed from auger to air
Set temporary well at 35 ft bgs with 10 ft of well screen
Water level stabilized at 24.83 feet below grade
Fracture in bedrock encountered at 33 feet below grade
Boring terminated at 35 feet due to presence of water36
40
20
24
28
32
52
64
56
60
44
48
B-1
MO
N
I
T
O
R
WE
L
L
4
8
12
16
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
2-3' collected for lab
Post Hole to 4' bgs
5-6 ft Brown, silty SAND, dry, manganese deposits,
slight hydrocarbon odor
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
6-25 ft Brown, silty SAND, dry, no odor
7/8/2010
135
7/8/2010
18 acre Beazer Property Charlotte, NC118084
SAEDACCO Steve
START DATE/TIME
Air / Auger
6.25 inches8.25 Auger/ 6" Button Bit
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Gus Pech Combo Rig
DEPTH
(feet)
DPT
None
0 - 5 ft Brown, silty SAND, dry, slight odor
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
SM 0 70 30
ML 0 70 30
ML 0 70 30
Water level stabilized at 26 feet below grade
Boring terminated at 37 feet due to presence of water
Same as above, water bearing fracture at 35 ft
36
40
20
24
28
32
52
64
56
60
44
48
B-2
MO
N
I
T
O
R
WE
L
L
4
8
12
16
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
20-37 ft Bedrock
Post Hole to 4' bgs
2-4 ft Brown, sandy SILT, dry,no odor
5-8 ft Brown, sandy SILT, dry, no odor, asphalt at 7.5 ft
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
8-20 ft Partially weathered rock
7/9/2010
137
7/9/2010
18 acre Beazer Property Charlotte, NC118084
SAEDACCO Steve
START DATE/TIME
Air / Auger
6.25 inches6" Button Bit
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Gus Pech Combo Rig
DEPTH
(feet)
DPT
None
0 - 2 ft Brown, silty SAND with gravel, dry, no odor
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
Set temporary well at 37 ft bgs with 10 ft of well screen
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
SM 0 70 30 17.1
100 SM 0 70 30 3.5
SM 0 70 30 1.7
100 SM 0 70 30 1.9
100 SM 0 70 30 1.9
Set temporary well at 35 ft bgs with 10 ft of well screen
0 - 2 ft Brown, silty SAND with gravel, dry, no odor
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
Air / Auger
8.25 inchesHollow Steam Auger
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Gus Pech Combo Rig
DEPTH
(feet)
DPT
None
7/8/2010
18 acre Beazer Property Charlotte, NC118084
SAEDACCO Steve
START DATE/TIME
7/8/2010
135
Same as above, moist at 18 ft
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
8-35 ft Reddish orange/brown, silty SAND and gravel,
dry (8-18 ft), no odor
Hand auger to 4' bgs
9-10' collected for lab
Advance with augers to 35 ft
2-4 ft Brown, sandy SILT, dry,no odor
5-8 ft Brown, sandy SILT, dry, no odor, asphalt at 7.5 ft
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
44
48
B-3
MO
N
I
T
O
R
WE
L
L
4
8
12
16
52
64
56
60
36
40
20
24
28
32
Water level stabilized at 24 feet below grade
Same as above, wet at 32 ft
Boring terminated at 35 feet due to presence of water
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
SM 0 70 30 18.5
100 SM 0 70 30 0.6
0.6
100 SM 0 70 30 4.3
100 0.3
0-4 ft Brown, silty SAND with gravel, dry, slight odor
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
Air / Auger
8.25 inchesHollow Steam Auger
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Gus Pech Combo Rig
DEPTH
(feet)
DPT
None
7/8/2010
18 acre Beazer Property Charlotte, NC118084
SAEDACCO Steve
START DATE/TIME
7/8/2010
135
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
Hand auger to 4' bgs
9-10 ft collected for lab
4-32 ft Brown, silty SAND, dry, slight odor
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
44
48
B-4
MO
N
I
T
O
R
WE
L
L
4
8
12
16
52
64
56
60
36
40
20
24
28
32
Set temporary well at 35 ft bgs with 10 ft of well screen
32-35 ft Partially weathered rock
Boring terminated at 35 feet due to presence of water
Water level stabilized at 24.25 feet below grade
Same as above
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
SM 0 70 30
100 SM 0 70 30
SM 0 70 30
100 SM 0 70 30
100
100
100
100
100
100
100
0 - 2 ft Brown, silty SAND with gravel, dry, no odor
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
Air / Auger
6.25 inches6" Button Bit
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Gus Pech Combo Rig
DEPTH
(feet)
DPT
None
7/9/2010
18 acre Beazer Property Charlotte, NC118084
SAEDACCO Steve
START DATE/TIME
7/9/2010
135
Water level stabilized at 15.5 feet below grade
Same as above, moist at 18 ft
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
8-35 ft Reddish orange/brown, silty SAND and gravel,
dry (8-18 ft), no odor
Post Hole to 4' bgs
2-4 ft Brown, sandy SILT, dry,no odor
5-8 ft Brown, sandy SILT, dry, no odor, asphalt at 7.5 ft
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
44
48
B-5
MO
N
I
T
O
R
WE
L
L
4
8
12
16
52
64
56
60
36
40
20
24
28
32
Set temporary well at 35 ft bgs with 10 ft of well screen
Same as above, wet at 32 ft
Boring terminated at 35 feet due to presence of water
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
SM 0 70 30
100
100 SM 0 70 30
100
100
SM 0 70 30
100
100
100
100
100
Water level stabilized at 27.58 feet below grade
36
40
20
24
28
32
52
64
56
60
44
48
B-6
MO
N
I
T
O
R
WE
L
L
4
8
Set temporary well at 40 ft bgs with 10 ft of well screen
12
16
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
no odor
Post Hole to 4' bgs
gravel, dry, no odor
15-40 ft Orangish-brown, silty SAND, saprolite
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
7-15 ft Reddish orange, black, fill material, silty SAND,
dry, no odor
7/9/2010
140
7/9/2010
18 acre Beazer Property Charlotte, NC118084
SAEDACCO Steve
START DATE/TIME
Air / Auger
6.25 inches6" Button Bit
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Gus Pech Combo Rig
DEPTH
(feet)
DPT
None
0-7 ft Brown, fill material comprised of silty SAND with
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
Boring terminated at 40 feet due to presence of water
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
100
100
100
100
100
100
100 Fracture hit at ~26 ft
Boring terminated at 30 feet due to water presence
Set temporary well at 30 ft bgs with 10 ft of well screen
36
40
20
24
28
32
52
64
56
60
44
48
B-7
MO
N
I
T
O
R
WE
L
L
4
8
12
16
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
N/A
M. Pressley
0 degrees
DESCRIPTION
Water level stabilized at 16.65 feet below grade
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
6-30 ft PWR and bedrock
8/19/2010
130
8/19/2010
18 acre Beazer Property Charlotte, NC118084
SAEDACCO Robert
START DATE/TIME
Air
6.25 inches6" Button Bit
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Gus Pech Combo Rig
DEPTH
(feet)
DPT
None
0-6 ft Brown, silt, sand, and gravel, dry, no odor
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
100
100
100
100
100
100
100
0-34 ft Orangish-brown, silt, sand, and gravel,
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
Air
6.25 inches6" Button Bit
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Gus Pech Combo Rig
DEPTH
(feet)
DPT
None
8/19/2010
18 acre Beazer Property Charlotte, NC118084
SAEDACCO Robert
START DATE/TIME
8/19/2010
134
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
Moisture increasing with depth
Water level stabilized at 14 feet below grade
no odor.
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
N/A
M. Pressley
0 degrees
DESCRIPTION
44
48
B-8
MO
N
I
T
O
R
WE
L
L
4
8
12
16
52
64
56
60
36
40
20
24
28
32
Set temporary well at 34 ft bgs with 10 ft of well screen
Boring terminated at 34 feet due to water presence
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
100
100
100
100
100
100
100
Set temporary well at 34 ft bgs with 10 ft of well screen
36
40
20
24
28
32
52
64
56
60
44
48
B-9
MO
N
I
T
O
R
WE
L
L
4
8
12
16
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
N/A
M. Pressley
0 degrees
DESCRIPTION
no odor.
Boring terminated at 34 feet due to water presence
Water bearing fracture encountered at 17 feet
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
Water level stabilized at 11.7 feet below grade
8/19/2010
120
8/19/2010
18 acre Beazer Property Charlotte, NC118084
SAEDACCO Robert
START DATE/TIME
Air
6.25 inches6" Button Bit
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Gus Pech Combo Rig
DEPTH
(feet)
DPT
None
0-10 ft Orangish-brown, silt, sand, and gravel,
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
30 30 40 3.2
100 5.7
81
36
40
20
24
28
32
52
64
56
60
44
48
B-10
MO
N
I
T
O
R
WE
L
L
4
8
12
16
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
Collected 4-6 for lab
Hand auger to 4' bgs
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
Boring terminated at 6 feet due to refusal
8/16/2010
16
8/16/2010
18 acre Beazer Property Charlotte, NC118084
Probe Technology Terry White
START DATE/TIME
Direct Push
2.25 inches5 ft long by 2.25 in. macro core
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Geoprobe 6200
DEPTH
(feet)
DPT
None
0-6 ft Brown, silt, sand, and gravel, dry, no odor
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
SM 0 70 30 9.8
100
8.2
100 6.2
Boring terminated at 8 feet due to refusal
0-8 ft Tan, orange, black, white silty SAND, dry, no odor
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
WATER LEVEL
Collected 1-2 for lab
Direct Push
2.25 inches5 ft long by 2.25 in. macro core
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Geoprobe 6200
DEPTH
(feet)
DPT
None
8/16/2010
18 acre Beazer Property Charlotte, NC118084
Probe Technology Terry White
START DATE/TIME
8/16/2010
28
NO. OF SAMPLES
Brown, partially weathered rock at 7 ft
Collected 6-7 for lab
Hand auger to 4' bgs
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
44
48
B-11
MO
N
I
T
O
R
WE
L
L
4
8
12
16
52
64
56
60
36
40
20
24
28
32
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
30 30 40 0.7
100
2.5
100 4.7
0 70 30 3.5
100 4.3
100 5.9
36
40
20
24
28
32
52
64
56
60
44
48
B-12
MO
N
I
T
O
R
WE
L
L
4
8
12
16
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
sand, and gravel, dry, no odor
Collected 13-15 for lab
Boring terminated at target depth of 15 feet
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
no odor
8-15 ft Orangish-brown, silty SAND, saprolite, dry,
8/16/2010
215
8/16/2010
18 acre Beazer Property Charlotte, NC118084
Probe Technology Terry White
START DATE/TIME
Direct Push
2.25 inches5 ft long by 2.25 in. macro core
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Geoprobe 6200
DEPTH
(feet)
DPT
None
0-8 ft Orangish-brown, fill material comprised of silt,
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
Hand auger to 4' bgs
Collected 3-5 for lab
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
30 30 40 5.9
100
29.5
100 30 30 40 22.6
10.5
0-6 ft Orangish-brown, fill material comprised of silt,
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
Direct Push
2.25 inches5 ft long by 2.25 in. macro core
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Geoprobe 6200
DEPTH
(feet)
DPT
None
8/16/2010
18 acre Beazer Property Charlotte, NC118084
Probe Technology Terry White
START DATE/TIME
8/16/2010
210
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
6-9 ft Orangish-brown with black manganese saprolite
9-10 ft Tan, partially weathered rock at 9 ft
Boring terminated at 10 feet due to refusal
Hand auger to 4' bgs
Collected 8-10 for lab
sand, and gravel, dry, no odor
Collected 3-5 for lab
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
44
48
B-13
MO
N
I
T
O
R
WE
L
L
4
8
12
16
52
64
56
60
36
40
20
24
28
32
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
30 30 40 2.1
100
4
100 30 50 20 6.2
18.4
100 1.6
Boring terminated at 12 feet due to refusal
36
40
20
24
28
32
52
64
56
60
44
48
B-14
MO
N
I
T
O
R
WE
L
L
4
8
12
16
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
Collected 8-10 for lab
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
6-12 ft Brown/white, saprolite, dry, no odor
comprised of clay, silt, sand, and gravel, dry, no odor
8/16/2010
212
8/16/2010
18 acre Beazer Property Charlotte, NC118084
Probe Technology Terry White
START DATE/TIME
Direct Push
2.25 inches5 ft long by 2.25 in. macro core
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Geoprobe 6200
DEPTH
(feet)
DPT
None
0-6 ft Brownish orange, white, black, fill material
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
Hand auger to 4' bgs
Collected 3-5 for lab
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
SM 0 30 70 15.1
100
115
100 14.9
25.4
100 32.2
0 40 30 40.5
0-13 ft Brownish orange, fill material comprised of sandy
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
Direct Push
2.25 inches5 ft long by 2.25 in. macro core
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Geoprobe 6200
DEPTH
(feet)
DPT
None
8/16/2010
18 acre Beazer Property Charlotte, NC118084
Probe Technology Terry White
START DATE/TIME
8/16/2010
215
no odor
Boring terminated at target depth of 15 feet
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
Hand auger to 4' bgs
Collected 13-15 for lab13-15 ft Gray and orange with black saprolite, dry,
SILT with some clay, dry, no odor
Collected 3-5 for lab
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
44
48
B-15
MO
N
I
T
O
R
WE
L
L
4
8
12
16
52
64
56
60
36
40
20
24
28
32
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
SM 0 70 30 2.5
100
24.4
100 SM 0 70 30 26
5.8
100 22.5
100 11.4
36
40
20
24
28
32
52
64
56
60
44
48
B-16
MO
N
I
T
O
R
WE
L
L
4
8
12
16
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
Collected 3-5 for lab
Hand auger to 4' bgs
Collected 13-15 for lab
gravel, dry, no odor
Boring terminated at target depth of 15 feet
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
7-15 ft Reddish orange, black, fill material, silty SAND,
dry, no odor
8/16/2010
215
8/16/2010
18 acre Beazer Property Charlotte, NC118084
Probe Technology Terry White
START DATE/TIME
Direct Push
2.25 inches5 ft long by 2.25 in. macro core
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Geoprobe 6200
DEPTH
(feet)
DPT
None
0-7 ft Brown, fill material comprised of silty SAND with
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
SM 0 70 30 0
100
0.8
100 3.3
4.1
100 0.6
100 5.7
0-15 ft Layers of reddish orange and brown silty SAND
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
Direct Push
2.25 inches5 ft long by 2.25 in. macro core
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Geoprobe 6200
DEPTH
(feet)
DPT
None
8/16/2010
18 acre Beazer Property Charlotte, NC118084
Probe Technology Terry White
START DATE/TIME
8/16/2010
215
Boring terminated at target depth of 15 feet
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
Hand auger to 4' bgs
Collected 13-15 for lab
and clay, fill material, dry, no odor
Collected 3-5 for lab
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
44
48
B-17
MO
N
I
T
O
R
WE
L
L
4
8
12
16
52
64
56
60
36
40
20
24
28
32
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
30 30 40 192
100
163
100 110
SM 0 70 30 238
100 278
100 499
36
40
20
24
28
32
52
64
56
60
44
48
B-18
MO
N
I
T
O
R
WE
L
L
4
8
12
16
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
Hand auger to 4' bgs
Collected 0-2 for lab
Collected 13-15 for lab
Boring terminated at target depth of 15 feet
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
9-15 ft Brown, white, orange saprolite (silty SAND), dry,
no odor
8/16/2010
215
8/16/2010
18 acre Beazer Property Charlotte, NC118084
Probe Technology Terry White
START DATE/TIME
Direct Push
2.25 inches5 ft long by 2.25 in. macro core
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Geoprobe 6200
DEPTH
(feet)
DPT
None
0-9 ft Fill material, dry, no odor
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
0 30 70 206
100
SM 0 70 30 55
100 187
137
100 401
100 367
0-5 ft Orangish brown, fill material comprised of sandy
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
Direct Push
2.25 inches5 ft long by 2.25 in. macro core
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Geoprobe 6200
DEPTH
(feet)
DPT
None
8/17/2010
18 acre Beazer Property Charlotte, NC118084
Probe Technology Terry White
START DATE/TIME
8/17/2010
215
Boring terminated at target depth of 15 feet
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
Hand auger to 4' bgs
Collected 13-15 for lab
SILT and clay with gravel, dry, no odor
5-15 ft Orange, white, brown, black, silty SAND saprolite Collected 3-5 for lab
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
44
48
B-19
MO
N
I
T
O
R
WE
L
L
4
8
12
16
52
64
56
60
36
40
20
24
28
32
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
0 30 70 0
100
0
100 0
0
100 0
100 10.1
36
40
20
24
28
32
52
64
56
60
44
48
B-20
MO
N
I
T
O
R
WE
L
L
4
8
12
16
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
Collected 3-5 for lab
Hand auger to 4' bgs
Collected 13-15 for lab
SILT and clay with gravel, dry, no odor
Boring terminated at target depth of 15 feet
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
8/17/2010
215
8/17/2010
18 acre Beazer Property Charlotte, NC118084
Probe Technology Terry White
START DATE/TIME
Direct Push
2.25 inches5 ft long by 2.25 in. macro core
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Geoprobe 6200
DEPTH
(feet)
DPT
None
0-15 ft Orangish brown, fill material comprised of sandy
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
SM 0 70 30
100
0
100
0
100
100 0
100 0
36
40
20
24
28
32
52
64
56
60
44
48
SP-1
MO
N
I
T
O
R
WE
L
L
4
8
12
16
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
Collected 6-8 for lab
Collected 16-18 for lab
silty SAND with gravel, dry, no odor
Boring terminated at target depth of 20 feet
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
8/17/2010
220
8/17/2010
18 acre Beazer Property Charlotte, NC118084
Probe Technology Terry White
START DATE/TIME
Direct Push
2.25 inches5 ft long by 2.25 in. macro core
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Geoprobe 6200
DEPTH
(feet)
DPT
None
0-20 ft Orangish brown, all fill material comprised of
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
SM 0 70 30
100
0
100
0
100
100 0
100 0
0-20 ft Orangish brown, all fill material comprised of
US
C
S
S
Y
M
B
O
L
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
Direct Push
2.25 inches5 ft long by 2.25 in. macro core
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
Geoprobe 6200
DEPTH
(feet)
DPT
None
8/17/2010
18 acre Beazer Property Charlotte, NC118084
Probe Technology Terry White
START DATE/TIME
8/17/2010
220
Boring terminated at target depth of 20 feet
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
NO. OF SAMPLES
WATER LEVEL
silty SAND with gravel, dry, no odor
Collected 6-8 for lab
Collected 16-18 for lab
LI
T
H
O
L
O
G
Y
ESTIMATED
PERCENT OF
NA N/A
M. Pressley
0 degrees
DESCRIPTION
44
48
SP-2
MO
N
I
T
O
R
WE
L
L
4
8
12
16
52
64
56
60
36
40
20
24
28
32
Appendix B
Laboratory Analytical Data
Sheets – Soil Samples
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
ERM-Southeast, Inc
8000 Corporate Center Drive
Suite 200
Charlotte, NC 28226
Attention: Michael Pressley
LG12019Lot Number:
0118084Project Number:
Beazer PropertyProject Name:
07/20/2010Date Completed:
Nisreen Saikaly
Project Manager
*LG12019*
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
ERM-Southeast, Inc
Lot Number: LG12019
SC DHEC No: 32010 NC DEHNR No: 329 NELAC No: E87653
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
ERM-Southeast, Inc
Lot Number: LG12019
Sample Number Sample ID Matrix Date Sampled Date Received
001 07/08/2010 1000B-1 2-3'Solid 07/12/2010
002 07/08/2010 1135B-3 9-10'Solid 07/12/2010
003 07/08/2010 1415B-4 9-10'Solid 07/12/2010
(3 samples)
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
ERM-Southeast, Inc
Lot Number: LG12019
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 B-1 2-3'Solid Tetrachloroethene 8260B 22 ug/kg 5
002 B-3 9-10'Solid Tetrachloroethene 8260B 23 ug/kg 7
003 B-4 9-10'Solid Tetrachloroethene 8260B 47 ug/kg 9
(3 detections)
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-1 2-3'
LG12019-001
07/08/2010 1000
07/12/2010
Solid
% Solids:82.7 07/12/2010 2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 07/20/2010 0456 DLB 38078 5.23
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg23
Benzene 71-43-2 8260B ND 1ug/kg5.8
Bromodichloromethane 75-27-4 8260B ND 1ug/kg5.8
Bromoform 75-25-2 8260B ND 1ug/kg5.8
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg5.8
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg12
Carbon disulfide 75-15-0 8260B ND 1ug/kg5.8
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg5.8
Chlorobenzene 108-90-7 8260B ND 1ug/kg5.8
Chloroethane 75-00-3 8260B ND 1ug/kg5.8
Chloroform 67-66-3 8260B ND 1ug/kg5.8
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg5.8
Cyclohexane 110-82-7 8260B ND 1ug/kg5.8
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg5.8
Dibromochloromethane 124-48-1 8260B ND 1ug/kg5.8
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg5.8
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg5.8
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg5.8
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg5.8
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg5.8
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg5.8
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg5.8
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg5.8
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg5.8
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg5.8
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg5.8
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg5.8
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg5.8
Ethylbenzene 100-41-4 8260B ND 1ug/kg5.8
2-Hexanone 591-78-6 8260B ND 1ug/kg12
Isopropylbenzene 98-82-8 8260B ND 1ug/kg5.8
Methyl acetate 79-20-9 8260B ND 1ug/kg5.8
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg5.8
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg12
Methylcyclohexane 108-87-2 8260B ND 1ug/kg5.8
Methylene chloride 75-09-2 8260B ND 1ug/kg5.8
Styrene 100-42-5 8260B ND 1ug/kg5.8
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg5.8
Tetrachloroethene 127-18-4 8260B 22 1ug/kg5.8
Toluene 108-88-3 8260B ND 1ug/kg5.8
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg5.8
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg5.8
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg5.8
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg5.8
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-1 2-3'
LG12019-001
07/08/2010 1000
07/12/2010
Solid
% Solids:82.7 07/12/2010 2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 07/20/2010 0456 DLB 38078 5.23
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg5.8
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg5.8
Vinyl chloride 75-01-4 8260B ND 1ug/kg5.8
Xylenes (total)1330-20-7 8260B ND 1ug/kg5.8
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 77 53-142
Bromofluorobenzene 91 47-138
Toluene-d8 87 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-3 9-10'
LG12019-002
07/08/2010 1135
07/12/2010
Solid
% Solids:73.1 07/12/2010 2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 07/20/2010 0519 DLB 38078 6.19
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg22
Benzene 71-43-2 8260B ND 1ug/kg5.5
Bromodichloromethane 75-27-4 8260B ND 1ug/kg5.5
Bromoform 75-25-2 8260B ND 1ug/kg5.5
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg5.5
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg11
Carbon disulfide 75-15-0 8260B ND 1ug/kg5.5
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg5.5
Chlorobenzene 108-90-7 8260B ND 1ug/kg5.5
Chloroethane 75-00-3 8260B ND 1ug/kg5.5
Chloroform 67-66-3 8260B ND 1ug/kg5.5
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg5.5
Cyclohexane 110-82-7 8260B ND 1ug/kg5.5
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg5.5
Dibromochloromethane 124-48-1 8260B ND 1ug/kg5.5
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg5.5
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg5.5
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg5.5
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg5.5
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg5.5
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg5.5
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg5.5
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg5.5
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg5.5
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg5.5
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg5.5
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg5.5
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg5.5
Ethylbenzene 100-41-4 8260B ND 1ug/kg5.5
2-Hexanone 591-78-6 8260B ND 1ug/kg11
Isopropylbenzene 98-82-8 8260B ND 1ug/kg5.5
Methyl acetate 79-20-9 8260B ND 1ug/kg5.5
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg5.5
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg11
Methylcyclohexane 108-87-2 8260B ND 1ug/kg5.5
Methylene chloride 75-09-2 8260B ND 1ug/kg5.5
Styrene 100-42-5 8260B ND 1ug/kg5.5
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg5.5
Tetrachloroethene 127-18-4 8260B 23 1ug/kg5.5
Toluene 108-88-3 8260B ND 1ug/kg5.5
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg5.5
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg5.5
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg5.5
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg5.5
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 7 of 23
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-3 9-10'
LG12019-002
07/08/2010 1135
07/12/2010
Solid
% Solids:73.1 07/12/2010 2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 07/20/2010 0519 DLB 38078 6.19
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg5.5
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg5.5
Vinyl chloride 75-01-4 8260B ND 1ug/kg5.5
Xylenes (total)1330-20-7 8260B ND 1ug/kg5.5
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 75 53-142
Bromofluorobenzene 88 47-138
Toluene-d8 84 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-4 9-10'
LG12019-003
07/08/2010 1415
07/12/2010
Solid
% Solids:78.2 07/12/2010 2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 07/20/2010 1953 LBS 38129 5.80
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg22
Benzene 71-43-2 8260B ND 1ug/kg5.5
Bromodichloromethane 75-27-4 8260B ND 1ug/kg5.5
Bromoform 75-25-2 8260B ND 1ug/kg5.5
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg5.5
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg11
Carbon disulfide 75-15-0 8260B ND 1ug/kg5.5
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg5.5
Chlorobenzene 108-90-7 8260B ND 1ug/kg5.5
Chloroethane 75-00-3 8260B ND 1ug/kg5.5
Chloroform 67-66-3 8260B ND 1ug/kg5.5
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg5.5
Cyclohexane 110-82-7 8260B ND 1ug/kg5.5
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg5.5
Dibromochloromethane 124-48-1 8260B ND 1ug/kg5.5
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg5.5
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg5.5
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg5.5
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg5.5
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg5.5
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg5.5
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg5.5
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg5.5
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg5.5
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg5.5
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg5.5
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg5.5
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg5.5
Ethylbenzene 100-41-4 8260B ND 1ug/kg5.5
2-Hexanone 591-78-6 8260B ND 1ug/kg11
Isopropylbenzene 98-82-8 8260B ND 1ug/kg5.5
Methyl acetate 79-20-9 8260B ND 1ug/kg5.5
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg5.5
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg11
Methylcyclohexane 108-87-2 8260B ND 1ug/kg5.5
Methylene chloride 75-09-2 8260B ND 1ug/kg5.5
Styrene 100-42-5 8260B ND 1ug/kg5.5
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg5.5
Tetrachloroethene 127-18-4 8260B 47 1ug/kg5.5
Toluene 108-88-3 8260B ND 1ug/kg5.5
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg5.5
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg5.5
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg5.5
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg5.5
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 9 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-4 9-10'
LG12019-003
07/08/2010 1415
07/12/2010
Solid
% Solids:78.2 07/12/2010 2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 07/20/2010 1953 LBS 38129 5.80
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg5.5
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg5.5
Vinyl chloride 75-01-4 8260B ND 1ug/kg5.5
Xylenes (total)1330-20-7 8260B ND 1ug/kg5.5
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 87 53-142
Bromofluorobenzene 101 47-138
Toluene-d8 99 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
QC Summary
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:LQ38078-001
38078 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL Units Analysis DateDil
Acetone ND 07/20/2010 032420ug/kg1
Benzene ND 07/20/2010 03245.0 ug/kg1
Bromodichloromethane ND 07/20/2010 03245.0 ug/kg1
Bromoform ND 07/20/2010 03245.0 ug/kg1
Bromomethane (Methyl bromide)ND 07/20/2010 03245.0 ug/kg1
2-Butanone (MEK)ND 07/20/2010 032410ug/kg1
Carbon disulfide ND 07/20/2010 03245.0 ug/kg1
Carbon tetrachloride ND 07/20/2010 03245.0 ug/kg1
Chlorobenzene ND 07/20/2010 03245.0 ug/kg1
Chloroethane ND 07/20/2010 03245.0 ug/kg1
Chloroform ND 07/20/2010 03245.0 ug/kg1
Chloromethane (Methyl chloride)ND 07/20/2010 03245.0 ug/kg1
Cyclohexane ND 07/20/2010 03245.0 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 07/20/2010 03245.0 ug/kg1
Dibromochloromethane ND 07/20/2010 03245.0 ug/kg1
1,2-Dibromoethane (EDB)ND 07/20/2010 03245.0 ug/kg1
1,4-Dichlorobenzene ND 07/20/2010 03245.0 ug/kg1
1,2-Dichlorobenzene ND 07/20/2010 03245.0 ug/kg1
1,3-Dichlorobenzene ND 07/20/2010 03245.0 ug/kg1
Dichlorodifluoromethane ND 07/20/2010 03245.0 ug/kg1
1,2-Dichloroethane ND 07/20/2010 03245.0 ug/kg1
1,1-Dichloroethane ND 07/20/2010 03245.0 ug/kg1
trans-1,2-Dichloroethene ND 07/20/2010 03245.0 ug/kg1
1,1-Dichloroethene ND 07/20/2010 03245.0 ug/kg1
cis-1,2-Dichloroethene ND 07/20/2010 03245.0 ug/kg1
1,2-Dichloropropane ND 07/20/2010 03245.0 ug/kg1
trans-1,3-Dichloropropene ND 07/20/2010 03245.0 ug/kg1
cis-1,3-Dichloropropene ND 07/20/2010 03245.0 ug/kg1
Ethylbenzene ND 07/20/2010 03245.0 ug/kg1
2-Hexanone ND 07/20/2010 032410ug/kg1
Isopropylbenzene ND 07/20/2010 03245.0 ug/kg1
Methyl acetate ND 07/20/2010 03245.0 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 07/20/2010 03245.0 ug/kg1
4-Methyl-2-pentanone ND 07/20/2010 032410ug/kg1
Methylcyclohexane ND 07/20/2010 03245.0 ug/kg1
Methylene chloride ND 07/20/2010 03245.0 ug/kg1
Styrene ND 07/20/2010 03245.0 ug/kg1
1,1,2,2-Tetrachloroethane ND 07/20/2010 03245.0 ug/kg1
Tetrachloroethene ND 07/20/2010 03245.0 ug/kg1
Toluene ND 07/20/2010 03245.0 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 07/20/2010 03245.0 ug/kg1
1,2,4-Trichlorobenzene ND 07/20/2010 03245.0 ug/kg1
1,1,1-Trichloroethane ND 07/20/2010 03245.0 ug/kg1
1,1,2-Trichloroethane ND 07/20/2010 03245.0 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 12 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:LQ38078-001
38078 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL Units Analysis DateDil
Trichloroethene ND 07/20/2010 03245.0 ug/kg1
Trichlorofluoromethane ND 07/20/2010 03245.0 ug/kg1
Vinyl chloride ND 07/20/2010 03245.0 ug/kg1
Xylenes (total)ND 07/20/2010 03245.0 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 89 47-138
1,2-Dichloroethane-d4 76 53-142
Toluene-d8 84 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 13 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:LQ38078-002
38078 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 86 07/20/2010 01528610042-1491
Benzene 48 07/20/2010 0152955069-1231
Bromodichloromethane 48 07/20/2010 0152955069-1211
Bromoform 43 07/20/2010 0152865061-1191
Bromomethane (Methyl bromide)45 07/20/2010 0152915035-1441
2-Butanone (MEK)82 07/20/2010 01528210057-1481
Carbon disulfide 54 07/20/2010 01521075058-1221
Carbon tetrachloride 52 07/20/2010 01521045058-1361
Chlorobenzene 46 07/20/2010 0152925059-1291
Chloroethane 45 07/20/2010 0152905050-1321
Chloroform 48 07/20/2010 0152965071-1251
Chloromethane (Methyl chloride)45 07/20/2010 0152915034-1341
Cyclohexane 50 07/20/2010 01521005053-1391
1,2-Dibromo-3-chloropropane (DBCP)44 07/20/2010 0152885055-1251
Dibromochloromethane 45 07/20/2010 0152905066-1191
1,2-Dibromoethane (EDB)43 07/20/2010 0152875074-1241
1,4-Dichlorobenzene 46 07/20/2010 0152915052-1331
1,2-Dichlorobenzene 45 07/20/2010 0152915057-1311
1,3-Dichlorobenzene 46 07/20/2010 0152915051-1341
Dichlorodifluoromethane 43 07/20/2010 0152865010-1571
1,2-Dichloroethane 44 07/20/2010 0152885067-1291
1,1-Dichloroethane 49 07/20/2010 0152985071-1271
trans-1,2-Dichloroethene 49 07/20/2010 0152995068-1311
1,1-Dichloroethene 47 07/20/2010 0152935069-1381
cis-1,2-Dichloroethene 48 07/20/2010 0152955070-1221
1,2-Dichloropropane 46 07/20/2010 0152935072-1241
trans-1,3-Dichloropropene 46 07/20/2010 0152925070-1241
cis-1,3-Dichloropropene 46 07/20/2010 0152935070-1261
Ethylbenzene 47 07/20/2010 0152945059-1281
2-Hexanone 81 07/20/2010 01528110054-1371
Isopropylbenzene 50 07/20/2010 01521005050-1361
Methyl acetate 42 07/20/2010 0152845059-1371
Methyl tertiary butyl ether (MTBE)46 07/20/2010 0152915072-1221
4-Methyl-2-pentanone 82 07/20/2010 01528210060-1341
Methylcyclohexane 51 07/20/2010 01521025041-1441
Methylene chloride 48 07/20/2010 0152955077-1291
Styrene 48 07/20/2010 0152965054-1361
1,1,2,2-Tetrachloroethane 44 07/20/2010 0152885069-1321
Tetrachloroethene 46 07/20/2010 0152935070-1301
Toluene 47 07/20/2010 0152935061-1291
1,1,2-Trichloro-1,2,2-Trifluoroethane 54 07/20/2010 01521075049-1361
1,2,4-Trichlorobenzene 43 07/20/2010 0152875034-1451
1,1,1-Trichloroethane 50 07/20/2010 01521015063-1281
1,1,2-Trichloroethane 43 07/20/2010 0152865055-1281
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 14 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:LQ38078-002
38078 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 47 07/20/2010 0152955062-1261
Trichlorofluoromethane 47 07/20/2010 0152945045-1381
Vinyl chloride 49 07/20/2010 0152975042-1321
Xylenes (total)96 07/20/2010 01529610058-1281
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 96 47-138
1,2-Dichloroethane-d4 76 53-142
Toluene-d8 88 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 15 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:LQ38078-003
38078 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Acetone 98 07/20/2010 02159810042-14913 201
Benzene 54 07/20/2010 02151075069-12312 201
Bromodichloromethane 55 07/20/2010 02151105069-12114 201
Bromoform 50 07/20/2010 02151005061-11914 201
Bromomethane (Methyl bromide)50 07/20/2010 02151005035-1449.9 201
2-Butanone (MEK)98 07/20/2010 02159810057-14817 201
Carbon disulfide 58 07/20/2010 02151165058-1227.8 201
Carbon tetrachloride 57 07/20/2010 02151145058-1369.3 201
Chlorobenzene 53 07/20/2010 02151065059-12915 201
Chloroethane 49 07/20/2010 0215985050-1328.2 201
Chloroform 55 07/20/2010 02151105071-12513 201
Chloromethane (Methyl chloride)49 07/20/2010 0215985034-1348.1 201
Cyclohexane 55 07/20/2010 02151095053-1399.1 201
1,2-Dibromo-3-chloropropane (DBCP)50 07/20/2010 0215995055-12512 201
Dibromochloromethane 54 07/20/2010 02151085066-11918 201
1,2-Dibromoethane (EDB)51 07/20/2010 02151035074-12417 201
1,4-Dichlorobenzene 53 07/20/2010 02151055052-13314 201
1,2-Dichlorobenzene 52 07/20/2010 02151035057-13113 201
1,3-Dichlorobenzene 53 07/20/2010 02151065051-13415 201
Dichlorodifluoromethane 47 07/20/2010 0215945010-1577.9 201
1,2-Dichloroethane 52 07/20/2010 02151045067-12917 201
1,1-Dichloroethane 54 07/20/2010 02151095071-12711 201
trans-1,2-Dichloroethene 54 07/20/2010 02151095068-1319.7 201
1,1-Dichloroethene 52 07/20/2010 02151045069-13810 201
cis-1,2-Dichloroethene 54 07/20/2010 02151075070-12212 201
1,2-Dichloropropane 53 07/20/2010 02151055072-12413 201
trans-1,3-Dichloropropene 54 07/20/2010 02151085070-12416 201
cis-1,3-Dichloropropene 54 07/20/2010 02151095070-12616 201
Ethylbenzene 54 07/20/2010 02151095059-12814 201
2-Hexanone 100 07/20/2010 0215+100100 54-13721 201
Isopropylbenzene 57 07/20/2010 02151135050-13612 201
Methyl acetate 49 07/20/2010 0215985059-13715 201
Methyl tertiary butyl ether (MTBE)50 07/20/2010 02151005072-1229.2 201
4-Methyl-2-pentanone 97 07/20/2010 02159710060-13417 201
Methylcyclohexane 55 07/20/2010 02151105041-1447.1 201
Methylene chloride 52 07/20/2010 02151035077-1298.4 201
Styrene 55 07/20/2010 02151105054-13614 201
1,1,2,2-Tetrachloroethane 51 07/20/2010 02151015069-13214 201
Tetrachloroethene 54 07/20/2010 02151085070-13016 201
Toluene 54 07/20/2010 02151075061-12914 201
1,1,2-Trichloro-1,2,2-Trifluoroethane 58 07/20/2010 02151175049-1368.5 201
1,2,4-Trichlorobenzene 49 07/20/2010 0215995034-14513 201
1,1,1-Trichloroethane 56 07/20/2010 02151125063-12811 201
1,1,2-Trichloroethane 51 07/20/2010 02151025055-12816 201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 16 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:LQ38078-003
38078 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Trichloroethene 54 07/20/2010 02151085062-12613 201
Trichlorofluoromethane 51 07/20/2010 02151025045-1388.3 201
Vinyl chloride 49 07/20/2010 0215995042-1321.3 201
Xylenes (total)110 07/20/2010 021510810058-12812 201
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 106 47-138
1,2-Dichloroethane-d4 83 53-142
Toluene-d8 96 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 17 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:LQ38129-001
38129 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL Units Analysis DateDil
Acetone ND 07/20/2010 192820ug/kg1
Benzene ND 07/20/2010 19285.0 ug/kg1
Bromodichloromethane ND 07/20/2010 19285.0 ug/kg1
Bromoform ND 07/20/2010 19285.0 ug/kg1
Bromomethane (Methyl bromide)ND 07/20/2010 19285.0 ug/kg1
2-Butanone (MEK)ND 07/20/2010 192810ug/kg1
Carbon disulfide ND 07/20/2010 19285.0 ug/kg1
Carbon tetrachloride ND 07/20/2010 19285.0 ug/kg1
Chlorobenzene ND 07/20/2010 19285.0 ug/kg1
Chloroethane ND 07/20/2010 19285.0 ug/kg1
Chloroform ND 07/20/2010 19285.0 ug/kg1
Chloromethane (Methyl chloride)ND 07/20/2010 19285.0 ug/kg1
Cyclohexane ND 07/20/2010 19285.0 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 07/20/2010 19285.0 ug/kg1
Dibromochloromethane ND 07/20/2010 19285.0 ug/kg1
1,2-Dibromoethane (EDB)ND 07/20/2010 19285.0 ug/kg1
1,4-Dichlorobenzene ND 07/20/2010 19285.0 ug/kg1
1,3-Dichlorobenzene ND 07/20/2010 19285.0 ug/kg1
1,2-Dichlorobenzene ND 07/20/2010 19285.0 ug/kg1
Dichlorodifluoromethane ND 07/20/2010 19285.0 ug/kg1
1,2-Dichloroethane ND 07/20/2010 19285.0 ug/kg1
1,1-Dichloroethane ND 07/20/2010 19285.0 ug/kg1
trans-1,2-Dichloroethene ND 07/20/2010 19285.0 ug/kg1
cis-1,2-Dichloroethene ND 07/20/2010 19285.0 ug/kg1
1,1-Dichloroethene ND 07/20/2010 19285.0 ug/kg1
1,2-Dichloropropane ND 07/20/2010 19285.0 ug/kg1
trans-1,3-Dichloropropene ND 07/20/2010 19285.0 ug/kg1
cis-1,3-Dichloropropene ND 07/20/2010 19285.0 ug/kg1
Ethylbenzene ND 07/20/2010 19285.0 ug/kg1
2-Hexanone ND 07/20/2010 192810ug/kg1
Isopropylbenzene ND 07/20/2010 19285.0 ug/kg1
Methyl acetate ND 07/20/2010 19285.0 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 07/20/2010 19285.0 ug/kg1
4-Methyl-2-pentanone ND 07/20/2010 192810ug/kg1
Methylcyclohexane ND 07/20/2010 19285.0 ug/kg1
Methylene chloride ND 07/20/2010 19285.0 ug/kg1
Styrene ND 07/20/2010 19285.0 ug/kg1
1,1,2,2-Tetrachloroethane ND 07/20/2010 19285.0 ug/kg1
Tetrachloroethene ND 07/20/2010 19285.0 ug/kg1
Toluene ND 07/20/2010 19285.0 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 07/20/2010 19285.0 ug/kg1
1,2,4-Trichlorobenzene ND 07/20/2010 19285.0 ug/kg1
1,1,2-Trichloroethane ND 07/20/2010 19285.0 ug/kg1
1,1,1-Trichloroethane ND 07/20/2010 19285.0 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 18 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:LQ38129-001
38129 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL Units Analysis DateDil
Trichloroethene ND 07/20/2010 19285.0 ug/kg1
Trichlorofluoromethane ND 07/20/2010 19285.0 ug/kg1
Vinyl chloride ND 07/20/2010 19285.0 ug/kg1
Xylenes (total)ND 07/20/2010 19285.0 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 103 47-138
1,2-Dichloroethane-d4 90 53-142
Toluene-d8 96 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 19 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:LQ38129-002
38129 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 110 07/20/2010 175011310042-1491
Benzene 51 07/20/2010 17501025069-1231
Bromodichloromethane 52 07/20/2010 17501045069-1211
Bromoform 51 07/20/2010 17501025061-1191
Bromomethane (Methyl bromide)46 07/20/2010 1750935035-1441
2-Butanone (MEK)100 07/20/2010 175010410057-1481
Carbon disulfide 58 07/20/2010 17501155058-1221
Carbon tetrachloride 54 07/20/2010 17501085058-1361
Chlorobenzene 52 07/20/2010 17501045059-1291
Chloroethane 46 07/20/2010 1750935050-1321
Chloroform 55 07/20/2010 17501105071-1251
Chloromethane (Methyl chloride)47 07/20/2010 1750945034-1341
Cyclohexane 50 07/20/2010 17501005053-1391
1,2-Dibromo-3-chloropropane (DBCP)51 07/20/2010 17501025055-1251
Dibromochloromethane 53 07/20/2010 17501075066-1191
1,2-Dibromoethane (EDB)53 07/20/2010 17501065074-1241
1,4-Dichlorobenzene 53 07/20/2010 17501075052-1331
1,3-Dichlorobenzene 53 07/20/2010 17501065051-1341
1,2-Dichlorobenzene 52 07/20/2010 17501045057-1311
Dichlorodifluoromethane 46 07/20/2010 1750925010-1571
1,2-Dichloroethane 53 07/20/2010 17501065067-1291
1,1-Dichloroethane 54 07/20/2010 17501075071-1271
trans-1,2-Dichloroethene 54 07/20/2010 17501085068-1311
cis-1,2-Dichloroethene 54 07/20/2010 17501085070-1221
1,1-Dichloroethene 53 07/20/2010 17501065069-1381
1,2-Dichloropropane 52 07/20/2010 17501035072-1241
trans-1,3-Dichloropropene 56 07/20/2010 17501115070-1241
cis-1,3-Dichloropropene 53 07/20/2010 17501075070-1261
Ethylbenzene 53 07/20/2010 17501055059-1281
2-Hexanone 100 07/20/2010 175010210054-1371
Isopropylbenzene 55 07/20/2010 17501105050-1361
Methyl acetate 53 07/20/2010 17501065059-1371
Methyl tertiary butyl ether (MTBE)53 07/20/2010 17501075072-1221
4-Methyl-2-pentanone 100 07/20/2010 175010110060-1341
Methylcyclohexane 53 07/20/2010 17501065041-1441
Methylene chloride 51 07/20/2010 17501025077-1291
Styrene 55 07/20/2010 17501115054-1361
1,1,2,2-Tetrachloroethane 53 07/20/2010 17501075069-1321
Tetrachloroethene 51 07/20/2010 17501035070-1301
Toluene 51 07/20/2010 17501025061-1291
1,1,2-Trichloro-1,2,2-Trifluoroethane 60 07/20/2010 17501215049-1361
1,2,4-Trichlorobenzene 54 07/20/2010 17501095034-1451
1,1,2-Trichloroethane 51 07/20/2010 17501025055-1281
1,1,1-Trichloroethane 55 07/20/2010 17501105063-1281
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 20 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:LQ38129-002
38129 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 51 07/20/2010 17501035062-1261
Trichlorofluoromethane 46 07/20/2010 1750925045-1381
Vinyl chloride 46 07/20/2010 1750925042-1321
Xylenes (total)110 07/20/2010 175010910058-1281
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 111 47-138
1,2-Dichloroethane-d4 87 53-142
Toluene-d8 97 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 21 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:LQ38129-003
38129 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Acetone 110 07/20/2010 181411410042-1490.93 201
Benzene 53 07/20/2010 18141065069-1233.5 201
Bromodichloromethane 55 07/20/2010 18141105069-1215.8 201
Bromoform 53 07/20/2010 18141075061-1194.1 201
Bromomethane (Methyl bromide)46 07/20/2010 1814935035-1440.13 201
2-Butanone (MEK)110 07/20/2010 181411010057-1485.1 201
Carbon disulfide 57 07/20/2010 18141155058-1220.80 201
Carbon tetrachloride 55 07/20/2010 18141095058-1360.94 201
Chlorobenzene 53 07/20/2010 18141065059-1291.4 201
Chloroethane 46 07/20/2010 1814915050-1321.8 201
Chloroform 55 07/20/2010 18141105071-1250.33 201
Chloromethane (Methyl chloride)47 07/20/2010 1814945034-1340.071 201
Cyclohexane 50 07/20/2010 1814995053-1391.4 201
1,2-Dibromo-3-chloropropane (DBCP)51 07/20/2010 18141025055-1250.65 201
Dibromochloromethane 55 07/20/2010 18141095066-1192.5 201
1,2-Dibromoethane (EDB)55 07/20/2010 18141105074-1243.6 201
1,4-Dichlorobenzene 54 07/20/2010 18141085052-1330.91 201
1,3-Dichlorobenzene 54 07/20/2010 18141075051-1340.91 201
1,2-Dichlorobenzene 53 07/20/2010 18141065057-1311.7 201
Dichlorodifluoromethane 43 07/20/2010 1814875010-1575.5 201
1,2-Dichloroethane 55 07/20/2010 18141095067-1293.3 201
1,1-Dichloroethane 54 07/20/2010 18141085071-1270.65 201
trans-1,2-Dichloroethene 54 07/20/2010 18141085068-1310.81 201
cis-1,2-Dichloroethene 53 07/20/2010 18141075070-1220.73 201
1,1-Dichloroethene 52 07/20/2010 18141045069-1381.9 201
1,2-Dichloropropane 54 07/20/2010 18141085072-1245.0 201
trans-1,3-Dichloropropene 58 07/20/2010 18141155070-1243.7 201
cis-1,3-Dichloropropene 57 07/20/2010 18141145070-1266.3 201
Ethylbenzene 54 07/20/2010 18141075059-1281.8 201
2-Hexanone 110 07/20/2010 181411410054-13711 201
Isopropylbenzene 55 07/20/2010 18141095050-1360.93 201
Methyl acetate 55 07/20/2010 18141105059-1374.1 201
Methyl tertiary butyl ether (MTBE)54 07/20/2010 18141085072-1221.3 201
4-Methyl-2-pentanone 110 07/20/2010 181411010060-1348.7 201
Methylcyclohexane 54 07/20/2010 18141095041-1442.6 201
Methylene chloride 52 07/20/2010 18141045077-1291.9 201
Styrene 57 07/20/2010 18141145054-1363.1 201
1,1,2,2-Tetrachloroethane 55 07/20/2010 18141095069-1322.5 201
Tetrachloroethene 51 07/20/2010 18141035070-1300.074 201
Toluene 54 07/20/2010 18141095061-1296.1 201
1,1,2-Trichloro-1,2,2-Trifluoroethane 59 07/20/2010 18141185049-1362.0 201
1,2,4-Trichlorobenzene 51 07/20/2010 18141025034-1456.1 201
1,1,2-Trichloroethane 52 07/20/2010 18141045055-1282.1 201
1,1,1-Trichloroethane 56 07/20/2010 18141115063-1281.3 201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 22 of 23
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:LQ38129-003
38129 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Trichloroethene 53 07/20/2010 18141065062-1263.2 201
Trichlorofluoromethane 45 07/20/2010 1814915045-1381.2 201
Vinyl chloride 46 07/20/2010 1814925042-1320.12 201
Xylenes (total)110 07/20/2010 181410910058-1280.10 201
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 105 47-138
1,2-Dichloroethane-d4 82 53-142
Toluene-d8 94 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 23 of 23
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
ERM-Southeast, Inc
8000 Corporate Center Drive
Suite 200
Charlotte, NC 28226
Attention: Michael Pressley
LH17057Lot Number:
0118084Project Number:
Beazer PropertyProject Name:
08/20/2010Date Completed:
Nisreen Saikaly
Project Manager
*LH17057*
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
ERM-Southeast, Inc
Lot Number: LH17057
SC DHEC No: 32010 NC DEHNR No: 329 NELAC No: E87653
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
ERM-Southeast, Inc
Lot Number: LH17057
Sample Number Sample ID Matrix Date Sampled Date Received
001 08/16/2010 1030B-10 4-6'Solid 08/17/2010
002 08/16/2010 1110B-11 1-2'Solid 08/17/2010
003 08/16/2010 1115B-11 6-7'Solid 08/17/2010
004 08/16/2010 1145B-12 3-5'Solid 08/17/2010
005 08/16/2010 1150B-12 13-15'Solid 08/17/2010
006 08/16/2010 1250B-13 3-5'Solid 08/17/2010
007 08/16/2010 1255B-13 8-10'Solid 08/17/2010
008 08/16/2010 1320B-14 3-5'Solid 08/17/2010
009 08/16/2010 1325B-14 8-10'Solid 08/17/2010
010 08/16/2010 1405B-15 3-5'Solid 08/17/2010
011 08/16/2010 1410B-15 13-15'Solid 08/17/2010
012 08/16/2010 1440B-16 3-5'Solid 08/17/2010
013 08/16/2010 1445B-16 13-15'Solid 08/17/2010
014 08/16/2010 1520B-17 3-5'Solid 08/17/2010
015 08/16/2010 1525B-17 13-15'Solid 08/17/2010
016 08/16/2010 1555B-18 0-2'Solid 08/17/2010
017 08/16/2010 1600B-18 13-15'Solid 08/17/2010
018 08/17/2010 0930B-19 3-5'Solid 08/17/2010
019 08/17/2010 0935B-10 13-15'Solid 08/17/2010
020 08/17/2010 1010B-20 3-5'Solid 08/17/2010
021 08/17/2010 1015B-20 13-15'Solid 08/17/2010
022 08/17/2010 1050SP-1 6-8'Solid 08/17/2010
023 08/17/2010 1055SP-1 16-18'Solid 08/17/2010
024 08/17/2010 1115SP-2 6-8'Solid 08/17/2010
025 08/17/2010 1120SP-2 16-18'Solid 08/17/2010
(25 samples)
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
ERM-Southeast, Inc
Lot Number: LH17057
Sample Sample ID Matrix Parameter Method Result Q Units Page
(0 detections)
Page: 4 of 76
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-10 4-6'
LH17057-001
08/16/2010 1030
08/17/2010
Solid
% Solids:88.0 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/18/2010 1756 SJS1 40376 5.70
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg20
Benzene 71-43-2 8260B ND 1ug/kg5.0
Bromodichloromethane 75-27-4 8260B ND 1ug/kg5.0
Bromoform 75-25-2 8260B ND 1ug/kg5.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg5.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg10
Carbon disulfide 75-15-0 8260B ND 1ug/kg5.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg5.0
Chlorobenzene 108-90-7 8260B ND 1ug/kg5.0
Chloroethane 75-00-3 8260B ND 1ug/kg5.0
Chloroform 67-66-3 8260B ND 1ug/kg5.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg5.0
Cyclohexane 110-82-7 8260B ND 1ug/kg5.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg5.0
Dibromochloromethane 124-48-1 8260B ND 1ug/kg5.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg5.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg5.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg5.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg5.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg5.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg5.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg5.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg5.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg5.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg5.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg5.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg5.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg5.0
Ethylbenzene 100-41-4 8260B ND 1ug/kg5.0
2-Hexanone 591-78-6 8260B ND 1ug/kg10
Isopropylbenzene 98-82-8 8260B ND 1ug/kg5.0
Methyl acetate 79-20-9 8260B ND 1ug/kg5.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg5.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg10
Methylcyclohexane 108-87-2 8260B ND 1ug/kg5.0
Methylene chloride 75-09-2 8260B ND 1ug/kg5.0
Styrene 100-42-5 8260B ND 1ug/kg5.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg5.0
Tetrachloroethene 127-18-4 8260B ND 1ug/kg5.0
Toluene 108-88-3 8260B ND 1ug/kg5.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg5.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg5.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg5.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg5.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 5 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-10 4-6'
LH17057-001
08/16/2010 1030
08/17/2010
Solid
% Solids:88.0 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/18/2010 1756 SJS1 40376 5.70
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg5.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg5.0
Vinyl chloride 75-01-4 8260B ND 1ug/kg5.0
Xylenes (total)1330-20-7 8260B ND 1ug/kg5.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 81 53-142
Bromofluorobenzene 92 47-138
Toluene-d8 95 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 6 of 76
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-11 1-2'
LH17057-002
08/16/2010 1110
08/17/2010
Solid
% Solids:91.3 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/18/2010 1820 SJS1 40376 5.10
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg21
Benzene 71-43-2 8260B ND 1ug/kg5.4
Bromodichloromethane 75-27-4 8260B ND 1ug/kg5.4
Bromoform 75-25-2 8260B ND 1ug/kg5.4
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg5.4
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg11
Carbon disulfide 75-15-0 8260B ND 1ug/kg5.4
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg5.4
Chlorobenzene 108-90-7 8260B ND 1ug/kg5.4
Chloroethane 75-00-3 8260B ND 1ug/kg5.4
Chloroform 67-66-3 8260B ND 1ug/kg5.4
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg5.4
Cyclohexane 110-82-7 8260B ND 1ug/kg5.4
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg5.4
Dibromochloromethane 124-48-1 8260B ND 1ug/kg5.4
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg5.4
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg5.4
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg5.4
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg5.4
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg5.4
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg5.4
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg5.4
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg5.4
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg5.4
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg5.4
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg5.4
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg5.4
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg5.4
Ethylbenzene 100-41-4 8260B ND 1ug/kg5.4
2-Hexanone 591-78-6 8260B ND 1ug/kg11
Isopropylbenzene 98-82-8 8260B ND 1ug/kg5.4
Methyl acetate 79-20-9 8260B ND 1ug/kg5.4
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg5.4
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg11
Methylcyclohexane 108-87-2 8260B ND 1ug/kg5.4
Methylene chloride 75-09-2 8260B ND 1ug/kg5.4
Styrene 100-42-5 8260B ND 1ug/kg5.4
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg5.4
Tetrachloroethene 127-18-4 8260B ND 1ug/kg5.4
Toluene 108-88-3 8260B ND 1ug/kg5.4
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg5.4
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg5.4
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg5.4
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg5.4
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 7 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-11 1-2'
LH17057-002
08/16/2010 1110
08/17/2010
Solid
% Solids:91.3 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/18/2010 1820 SJS1 40376 5.10
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg5.4
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg5.4
Vinyl chloride 75-01-4 8260B ND 1ug/kg5.4
Xylenes (total)1330-20-7 8260B ND 1ug/kg5.4
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 99 53-142
Bromofluorobenzene 110 47-138
Toluene-d8 115 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 8 of 76
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-11 6-7'
LH17057-003
08/16/2010 1115
08/17/2010
Solid
% Solids:77.9 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/18/2010 1844 SJS1 40376 6.15
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg21
Benzene 71-43-2 8260B ND 1ug/kg5.2
Bromodichloromethane 75-27-4 8260B ND 1ug/kg5.2
Bromoform 75-25-2 8260B ND 1ug/kg5.2
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg5.2
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg10
Carbon disulfide 75-15-0 8260B ND 1ug/kg5.2
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg5.2
Chlorobenzene 108-90-7 8260B ND 1ug/kg5.2
Chloroethane 75-00-3 8260B ND 1ug/kg5.2
Chloroform 67-66-3 8260B ND 1ug/kg5.2
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg5.2
Cyclohexane 110-82-7 8260B ND 1ug/kg5.2
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg5.2
Dibromochloromethane 124-48-1 8260B ND 1ug/kg5.2
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg5.2
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg5.2
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg5.2
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg5.2
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg5.2
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg5.2
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg5.2
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg5.2
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg5.2
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg5.2
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg5.2
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg5.2
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg5.2
Ethylbenzene 100-41-4 8260B ND 1ug/kg5.2
2-Hexanone 591-78-6 8260B ND 1ug/kg10
Isopropylbenzene 98-82-8 8260B ND 1ug/kg5.2
Methyl acetate 79-20-9 8260B ND 1ug/kg5.2
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg5.2
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg10
Methylcyclohexane 108-87-2 8260B ND 1ug/kg5.2
Methylene chloride 75-09-2 8260B ND 1ug/kg5.2
Styrene 100-42-5 8260B ND 1ug/kg5.2
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg5.2
Tetrachloroethene 127-18-4 8260B ND 1ug/kg5.2
Toluene 108-88-3 8260B ND 1ug/kg5.2
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg5.2
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg5.2
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg5.2
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg5.2
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 9 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-11 6-7'
LH17057-003
08/16/2010 1115
08/17/2010
Solid
% Solids:77.9 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/18/2010 1844 SJS1 40376 6.15
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg5.2
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg5.2
Vinyl chloride 75-01-4 8260B ND 1ug/kg5.2
Xylenes (total)1330-20-7 8260B ND 1ug/kg5.2
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 93 53-142
Bromofluorobenzene 98 47-138
Toluene-d8 99 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 10 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-12 3-5'
LH17057-004
08/16/2010 1145
08/17/2010
Solid
% Solids:85.5 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/18/2010 1908 SJS1 40376 6.00
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg19
Benzene 71-43-2 8260B ND 1ug/kg4.9
Bromodichloromethane 75-27-4 8260B ND 1ug/kg4.9
Bromoform 75-25-2 8260B ND 1ug/kg4.9
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg4.9
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg9.7
Carbon disulfide 75-15-0 8260B ND 1ug/kg4.9
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg4.9
Chlorobenzene 108-90-7 8260B ND 1ug/kg4.9
Chloroethane 75-00-3 8260B ND 1ug/kg4.9
Chloroform 67-66-3 8260B ND 1ug/kg4.9
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg4.9
Cyclohexane 110-82-7 8260B ND 1ug/kg4.9
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg4.9
Dibromochloromethane 124-48-1 8260B ND 1ug/kg4.9
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4.9
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg4.9
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg4.9
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg4.9
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.9
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg4.9
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg4.9
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg4.9
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4.9
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg4.9
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4.9
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg4.9
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4.9
Ethylbenzene 100-41-4 8260B ND 1ug/kg4.9
2-Hexanone 591-78-6 8260B ND 1ug/kg9.7
Isopropylbenzene 98-82-8 8260B ND 1ug/kg4.9
Methyl acetate 79-20-9 8260B ND 1ug/kg4.9
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg4.9
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg9.7
Methylcyclohexane 108-87-2 8260B ND 1ug/kg4.9
Methylene chloride 75-09-2 8260B ND 1ug/kg4.9
Styrene 100-42-5 8260B ND 1ug/kg4.9
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg4.9
Tetrachloroethene 127-18-4 8260B ND 1ug/kg4.9
Toluene 108-88-3 8260B ND 1ug/kg4.9
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg4.9
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg4.9
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4.9
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4.9
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 11 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-12 3-5'
LH17057-004
08/16/2010 1145
08/17/2010
Solid
% Solids:85.5 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/18/2010 1908 SJS1 40376 6.00
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg4.9
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg4.9
Vinyl chloride 75-01-4 8260B ND 1ug/kg4.9
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.9
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 101 53-142
Bromofluorobenzene 112 47-138
Toluene-d8 115 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 12 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-12 13-15'
LH17057-005
08/16/2010 1150
08/17/2010
Solid
% Solids:83.5 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/18/2010 1931 SJS1 40376 5.83
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg21
Benzene 71-43-2 8260B ND 1ug/kg5.1
Bromodichloromethane 75-27-4 8260B ND 1ug/kg5.1
Bromoform 75-25-2 8260B ND 1ug/kg5.1
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg5.1
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg10
Carbon disulfide 75-15-0 8260B ND 1ug/kg5.1
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg5.1
Chlorobenzene 108-90-7 8260B ND 1ug/kg5.1
Chloroethane 75-00-3 8260B ND 1ug/kg5.1
Chloroform 67-66-3 8260B ND 1ug/kg5.1
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg5.1
Cyclohexane 110-82-7 8260B ND 1ug/kg5.1
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg5.1
Dibromochloromethane 124-48-1 8260B ND 1ug/kg5.1
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg5.1
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg5.1
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg5.1
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg5.1
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg5.1
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg5.1
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg5.1
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg5.1
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg5.1
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg5.1
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg5.1
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg5.1
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg5.1
Ethylbenzene 100-41-4 8260B ND 1ug/kg5.1
2-Hexanone 591-78-6 8260B ND 1ug/kg10
Isopropylbenzene 98-82-8 8260B ND 1ug/kg5.1
Methyl acetate 79-20-9 8260B ND 1ug/kg5.1
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg5.1
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg10
Methylcyclohexane 108-87-2 8260B ND 1ug/kg5.1
Methylene chloride 75-09-2 8260B ND 1ug/kg5.1
Styrene 100-42-5 8260B ND 1ug/kg5.1
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg5.1
Tetrachloroethene 127-18-4 8260B ND 1ug/kg5.1
Toluene 108-88-3 8260B ND 1ug/kg5.1
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg5.1
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg5.1
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg5.1
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg5.1
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 13 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-12 13-15'
LH17057-005
08/16/2010 1150
08/17/2010
Solid
% Solids:83.5 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/18/2010 1931 SJS1 40376 5.83
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg5.1
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg5.1
Vinyl chloride 75-01-4 8260B ND 1ug/kg5.1
Xylenes (total)1330-20-7 8260B ND 1ug/kg5.1
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 99 53-142
Bromofluorobenzene 115 47-138
Toluene-d8 113 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 14 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-13 3-5'
LH17057-006
08/16/2010 1250
08/17/2010
Solid
% Solids:87.3 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0313 SJS1 40358 6.58
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg17
Benzene 71-43-2 8260B ND 1ug/kg4.4
Bromodichloromethane 75-27-4 8260B ND 1ug/kg4.4
Bromoform 75-25-2 8260B ND 1ug/kg4.4
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg4.4
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg8.7
Carbon disulfide 75-15-0 8260B ND 1ug/kg4.4
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg4.4
Chlorobenzene 108-90-7 8260B ND 1ug/kg4.4
Chloroethane 75-00-3 8260B ND 1ug/kg4.4
Chloroform 67-66-3 8260B ND 1ug/kg4.4
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg4.4
Cyclohexane 110-82-7 8260B ND 1ug/kg4.4
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg4.4
Dibromochloromethane 124-48-1 8260B ND 1ug/kg4.4
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4.4
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg4.4
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg4.4
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg4.4
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.4
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg4.4
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg4.4
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg4.4
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4.4
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg4.4
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4.4
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg4.4
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4.4
Ethylbenzene 100-41-4 8260B ND 1ug/kg4.4
2-Hexanone 591-78-6 8260B ND 1ug/kg8.7
Isopropylbenzene 98-82-8 8260B ND 1ug/kg4.4
Methyl acetate 79-20-9 8260B ND 1ug/kg4.4
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg4.4
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg8.7
Methylcyclohexane 108-87-2 8260B ND 1ug/kg4.4
Methylene chloride 75-09-2 8260B ND 1ug/kg4.4
Styrene 100-42-5 8260B ND 1ug/kg4.4
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg4.4
Tetrachloroethene 127-18-4 8260B ND 1ug/kg4.4
Toluene 108-88-3 8260B ND 1ug/kg4.4
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg4.4
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg4.4
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4.4
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4.4
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 15 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-13 3-5'
LH17057-006
08/16/2010 1250
08/17/2010
Solid
% Solids:87.3 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0313 SJS1 40358 6.58
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg4.4
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg4.4
Vinyl chloride 75-01-4 8260B ND 1ug/kg4.4
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.4
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 80 53-142
Bromofluorobenzene 94 47-138
Toluene-d8 93 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 16 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-13 8-10'
LH17057-007
08/16/2010 1255
08/17/2010
Solid
% Solids:87.3 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0336 SJS1 40358 6.32
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg18
Benzene 71-43-2 8260B ND 1ug/kg4.5
Bromodichloromethane 75-27-4 8260B ND 1ug/kg4.5
Bromoform 75-25-2 8260B ND 1ug/kg4.5
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg4.5
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg9.1
Carbon disulfide 75-15-0 8260B ND 1ug/kg4.5
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg4.5
Chlorobenzene 108-90-7 8260B ND 1ug/kg4.5
Chloroethane 75-00-3 8260B ND 1ug/kg4.5
Chloroform 67-66-3 8260B ND 1ug/kg4.5
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg4.5
Cyclohexane 110-82-7 8260B ND 1ug/kg4.5
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg4.5
Dibromochloromethane 124-48-1 8260B ND 1ug/kg4.5
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4.5
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg4.5
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg4.5
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg4.5
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.5
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg4.5
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg4.5
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg4.5
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4.5
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg4.5
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4.5
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg4.5
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4.5
Ethylbenzene 100-41-4 8260B ND 1ug/kg4.5
2-Hexanone 591-78-6 8260B ND 1ug/kg9.1
Isopropylbenzene 98-82-8 8260B ND 1ug/kg4.5
Methyl acetate 79-20-9 8260B ND 1ug/kg4.5
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg4.5
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg9.1
Methylcyclohexane 108-87-2 8260B ND 1ug/kg4.5
Methylene chloride 75-09-2 8260B ND 1ug/kg4.5
Styrene 100-42-5 8260B ND 1ug/kg4.5
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg4.5
Tetrachloroethene 127-18-4 8260B ND 1ug/kg4.5
Toluene 108-88-3 8260B ND 1ug/kg4.5
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg4.5
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg4.5
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4.5
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4.5
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 17 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-13 8-10'
LH17057-007
08/16/2010 1255
08/17/2010
Solid
% Solids:87.3 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0336 SJS1 40358 6.32
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg4.5
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg4.5
Vinyl chloride 75-01-4 8260B ND 1ug/kg4.5
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.5
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 93 53-142
Bromofluorobenzene 108 47-138
Toluene-d8 107 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 18 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-14 3-5'
LH17057-008
08/16/2010 1320
08/17/2010
Solid
% Solids:82.8 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0359 SJS1 40358 5.99
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg20
Benzene 71-43-2 8260B ND 1ug/kg5.0
Bromodichloromethane 75-27-4 8260B ND 1ug/kg5.0
Bromoform 75-25-2 8260B ND 1ug/kg5.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg5.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg10
Carbon disulfide 75-15-0 8260B ND 1ug/kg5.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg5.0
Chlorobenzene 108-90-7 8260B ND 1ug/kg5.0
Chloroethane 75-00-3 8260B ND 1ug/kg5.0
Chloroform 67-66-3 8260B ND 1ug/kg5.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg5.0
Cyclohexane 110-82-7 8260B ND 1ug/kg5.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg5.0
Dibromochloromethane 124-48-1 8260B ND 1ug/kg5.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg5.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg5.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg5.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg5.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg5.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg5.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg5.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg5.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg5.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg5.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg5.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg5.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg5.0
Ethylbenzene 100-41-4 8260B ND 1ug/kg5.0
2-Hexanone 591-78-6 8260B ND 1ug/kg10
Isopropylbenzene 98-82-8 8260B ND 1ug/kg5.0
Methyl acetate 79-20-9 8260B ND 1ug/kg5.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg5.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg10
Methylcyclohexane 108-87-2 8260B ND 1ug/kg5.0
Methylene chloride 75-09-2 8260B ND 1ug/kg5.0
Styrene 100-42-5 8260B ND 1ug/kg5.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg5.0
Tetrachloroethene 127-18-4 8260B ND 1ug/kg5.0
Toluene 108-88-3 8260B ND 1ug/kg5.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg5.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg5.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg5.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg5.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 19 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-14 3-5'
LH17057-008
08/16/2010 1320
08/17/2010
Solid
% Solids:82.8 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0359 SJS1 40358 5.99
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg5.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg5.0
Vinyl chloride 75-01-4 8260B ND 1ug/kg5.0
Xylenes (total)1330-20-7 8260B ND 1ug/kg5.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 94 53-142
Bromofluorobenzene 114 47-138
Toluene-d8 104 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 20 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-14 8-10'
LH17057-009
08/16/2010 1325
08/17/2010
Solid
% Solids:90.0 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0422 SJS1 40358 5.30
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg21
Benzene 71-43-2 8260B ND 1ug/kg5.2
Bromodichloromethane 75-27-4 8260B ND 1ug/kg5.2
Bromoform 75-25-2 8260B ND 1ug/kg5.2
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg5.2
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg10
Carbon disulfide 75-15-0 8260B ND 1ug/kg5.2
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg5.2
Chlorobenzene 108-90-7 8260B ND 1ug/kg5.2
Chloroethane 75-00-3 8260B ND 1ug/kg5.2
Chloroform 67-66-3 8260B ND 1ug/kg5.2
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg5.2
Cyclohexane 110-82-7 8260B ND 1ug/kg5.2
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg5.2
Dibromochloromethane 124-48-1 8260B ND 1ug/kg5.2
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg5.2
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg5.2
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg5.2
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg5.2
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg5.2
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg5.2
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg5.2
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg5.2
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg5.2
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg5.2
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg5.2
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg5.2
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg5.2
Ethylbenzene 100-41-4 8260B ND 1ug/kg5.2
2-Hexanone 591-78-6 8260B ND 1ug/kg10
Isopropylbenzene 98-82-8 8260B ND 1ug/kg5.2
Methyl acetate 79-20-9 8260B ND 1ug/kg5.2
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg5.2
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg10
Methylcyclohexane 108-87-2 8260B ND 1ug/kg5.2
Methylene chloride 75-09-2 8260B ND 1ug/kg5.2
Styrene 100-42-5 8260B ND 1ug/kg5.2
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg5.2
Tetrachloroethene 127-18-4 8260B ND 1ug/kg5.2
Toluene 108-88-3 8260B ND 1ug/kg5.2
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg5.2
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg5.2
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg5.2
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg5.2
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 21 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-14 8-10'
LH17057-009
08/16/2010 1325
08/17/2010
Solid
% Solids:90.0 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0422 SJS1 40358 5.30
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg5.2
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg5.2
Vinyl chloride 75-01-4 8260B ND 1ug/kg5.2
Xylenes (total)1330-20-7 8260B ND 1ug/kg5.2
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 92 53-142
Bromofluorobenzene 108 47-138
Toluene-d8 107 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 22 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-15 3-5'
LH17057-010
08/16/2010 1405
08/17/2010
Solid
% Solids:86.1 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0446 SJS1 40358 6.33
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg18
Benzene 71-43-2 8260B ND 1ug/kg4.6
Bromodichloromethane 75-27-4 8260B ND 1ug/kg4.6
Bromoform 75-25-2 8260B ND 1ug/kg4.6
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg4.6
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg9.2
Carbon disulfide 75-15-0 8260B ND 1ug/kg4.6
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg4.6
Chlorobenzene 108-90-7 8260B ND 1ug/kg4.6
Chloroethane 75-00-3 8260B ND 1ug/kg4.6
Chloroform 67-66-3 8260B ND 1ug/kg4.6
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg4.6
Cyclohexane 110-82-7 8260B ND 1ug/kg4.6
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg4.6
Dibromochloromethane 124-48-1 8260B ND 1ug/kg4.6
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4.6
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg4.6
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg4.6
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg4.6
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.6
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg4.6
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg4.6
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg4.6
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4.6
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg4.6
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4.6
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg4.6
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4.6
Ethylbenzene 100-41-4 8260B ND 1ug/kg4.6
2-Hexanone 591-78-6 8260B ND 1ug/kg9.2
Isopropylbenzene 98-82-8 8260B ND 1ug/kg4.6
Methyl acetate 79-20-9 8260B ND 1ug/kg4.6
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg4.6
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg9.2
Methylcyclohexane 108-87-2 8260B ND 1ug/kg4.6
Methylene chloride 75-09-2 8260B ND 1ug/kg4.6
Styrene 100-42-5 8260B ND 1ug/kg4.6
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg4.6
Tetrachloroethene 127-18-4 8260B ND 1ug/kg4.6
Toluene 108-88-3 8260B ND 1ug/kg4.6
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg4.6
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg4.6
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4.6
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4.6
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 23 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-15 3-5'
LH17057-010
08/16/2010 1405
08/17/2010
Solid
% Solids:86.1 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0446 SJS1 40358 6.33
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg4.6
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg4.6
Vinyl chloride 75-01-4 8260B ND 1ug/kg4.6
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.6
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 98 53-142
Bromofluorobenzene 116 47-138
Toluene-d8 115 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 24 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-15 13-15'
LH17057-011
08/16/2010 1410
08/17/2010
Solid
% Solids:93.5 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0509 SJS1 40358 5.45
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg20
Benzene 71-43-2 8260B ND 1ug/kg4.9
Bromodichloromethane 75-27-4 8260B ND 1ug/kg4.9
Bromoform 75-25-2 8260B ND 1ug/kg4.9
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg4.9
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg9.8
Carbon disulfide 75-15-0 8260B ND 1ug/kg4.9
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg4.9
Chlorobenzene 108-90-7 8260B ND 1ug/kg4.9
Chloroethane 75-00-3 8260B ND 1ug/kg4.9
Chloroform 67-66-3 8260B ND 1ug/kg4.9
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg4.9
Cyclohexane 110-82-7 8260B ND 1ug/kg4.9
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg4.9
Dibromochloromethane 124-48-1 8260B ND 1ug/kg4.9
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4.9
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg4.9
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg4.9
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg4.9
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.9
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg4.9
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg4.9
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg4.9
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4.9
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg4.9
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4.9
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg4.9
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4.9
Ethylbenzene 100-41-4 8260B ND 1ug/kg4.9
2-Hexanone 591-78-6 8260B ND 1ug/kg9.8
Isopropylbenzene 98-82-8 8260B ND 1ug/kg4.9
Methyl acetate 79-20-9 8260B ND 1ug/kg4.9
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg4.9
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg9.8
Methylcyclohexane 108-87-2 8260B ND 1ug/kg4.9
Methylene chloride 75-09-2 8260B ND 1ug/kg4.9
Styrene 100-42-5 8260B ND 1ug/kg4.9
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg4.9
Tetrachloroethene 127-18-4 8260B ND 1ug/kg4.9
Toluene 108-88-3 8260B ND 1ug/kg4.9
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg4.9
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg4.9
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4.9
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4.9
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 25 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-15 13-15'
LH17057-011
08/16/2010 1410
08/17/2010
Solid
% Solids:93.5 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0509 SJS1 40358 5.45
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg4.9
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg4.9
Vinyl chloride 75-01-4 8260B ND 1ug/kg4.9
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.9
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 81 53-142
Bromofluorobenzene 96 47-138
Toluene-d8 94 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 26 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-16 3-5'
LH17057-012
08/16/2010 1440
08/17/2010
Solid
% Solids:91.6 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0532 SJS1 40358 5.65
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg19
Benzene 71-43-2 8260B ND 1ug/kg4.8
Bromodichloromethane 75-27-4 8260B ND 1ug/kg4.8
Bromoform 75-25-2 8260B ND 1ug/kg4.8
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg4.8
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg9.7
Carbon disulfide 75-15-0 8260B ND 1ug/kg4.8
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg4.8
Chlorobenzene 108-90-7 8260B ND 1ug/kg4.8
Chloroethane 75-00-3 8260B ND 1ug/kg4.8
Chloroform 67-66-3 8260B ND 1ug/kg4.8
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg4.8
Cyclohexane 110-82-7 8260B ND 1ug/kg4.8
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg4.8
Dibromochloromethane 124-48-1 8260B ND 1ug/kg4.8
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4.8
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg4.8
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg4.8
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg4.8
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.8
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg4.8
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg4.8
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg4.8
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4.8
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg4.8
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4.8
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg4.8
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4.8
Ethylbenzene 100-41-4 8260B ND 1ug/kg4.8
2-Hexanone 591-78-6 8260B ND 1ug/kg9.7
Isopropylbenzene 98-82-8 8260B ND 1ug/kg4.8
Methyl acetate 79-20-9 8260B ND 1ug/kg4.8
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg4.8
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg9.7
Methylcyclohexane 108-87-2 8260B ND 1ug/kg4.8
Methylene chloride 75-09-2 8260B ND 1ug/kg4.8
Styrene 100-42-5 8260B ND 1ug/kg4.8
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg4.8
Tetrachloroethene 127-18-4 8260B ND 1ug/kg4.8
Toluene 108-88-3 8260B ND 1ug/kg4.8
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg4.8
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg4.8
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4.8
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4.8
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 27 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-16 3-5'
LH17057-012
08/16/2010 1440
08/17/2010
Solid
% Solids:91.6 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0532 SJS1 40358 5.65
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg4.8
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg4.8
Vinyl chloride 75-01-4 8260B ND 1ug/kg4.8
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.8
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 91 53-142
Bromofluorobenzene 110 47-138
Toluene-d8 107 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 28 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-16 13-15'
LH17057-013
08/16/2010 1445
08/17/2010
Solid
% Solids:88.4 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0556 SJS1 40358 6.20
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg18
Benzene 71-43-2 8260B ND 1ug/kg4.6
Bromodichloromethane 75-27-4 8260B ND 1ug/kg4.6
Bromoform 75-25-2 8260B ND 1ug/kg4.6
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg4.6
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg9.1
Carbon disulfide 75-15-0 8260B ND 1ug/kg4.6
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg4.6
Chlorobenzene 108-90-7 8260B ND 1ug/kg4.6
Chloroethane 75-00-3 8260B ND 1ug/kg4.6
Chloroform 67-66-3 8260B ND 1ug/kg4.6
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg4.6
Cyclohexane 110-82-7 8260B ND 1ug/kg4.6
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg4.6
Dibromochloromethane 124-48-1 8260B ND 1ug/kg4.6
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4.6
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg4.6
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg4.6
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg4.6
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.6
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg4.6
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg4.6
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg4.6
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4.6
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg4.6
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4.6
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg4.6
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4.6
Ethylbenzene 100-41-4 8260B ND 1ug/kg4.6
2-Hexanone 591-78-6 8260B ND 1ug/kg9.1
Isopropylbenzene 98-82-8 8260B ND 1ug/kg4.6
Methyl acetate 79-20-9 8260B ND 1ug/kg4.6
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg4.6
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg9.1
Methylcyclohexane 108-87-2 8260B ND 1ug/kg4.6
Methylene chloride 75-09-2 8260B ND 1ug/kg4.6
Styrene 100-42-5 8260B ND 1ug/kg4.6
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg4.6
Tetrachloroethene 127-18-4 8260B ND 1ug/kg4.6
Toluene 108-88-3 8260B ND 1ug/kg4.6
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg4.6
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg4.6
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4.6
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4.6
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 29 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-16 13-15'
LH17057-013
08/16/2010 1445
08/17/2010
Solid
% Solids:88.4 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0556 SJS1 40358 6.20
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg4.6
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg4.6
Vinyl chloride 75-01-4 8260B ND 1ug/kg4.6
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.6
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 95 53-142
Bromofluorobenzene 111 47-138
Toluene-d8 110 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 30 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-17 3-5'
LH17057-014
08/16/2010 1520
08/17/2010
Solid
% Solids:89.8 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0620 SJS1 40358 6.65
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg17
Benzene 71-43-2 8260B ND 1ug/kg4.2
Bromodichloromethane 75-27-4 8260B ND 1ug/kg4.2
Bromoform 75-25-2 8260B ND 1ug/kg4.2
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg4.2
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg8.4
Carbon disulfide 75-15-0 8260B ND 1ug/kg4.2
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg4.2
Chlorobenzene 108-90-7 8260B ND 1ug/kg4.2
Chloroethane 75-00-3 8260B ND 1ug/kg4.2
Chloroform 67-66-3 8260B ND 1ug/kg4.2
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg4.2
Cyclohexane 110-82-7 8260B ND 1ug/kg4.2
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg4.2
Dibromochloromethane 124-48-1 8260B ND 1ug/kg4.2
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4.2
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg4.2
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg4.2
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg4.2
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.2
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg4.2
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg4.2
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg4.2
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4.2
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg4.2
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4.2
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg4.2
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4.2
Ethylbenzene 100-41-4 8260B ND 1ug/kg4.2
2-Hexanone 591-78-6 8260B ND 1ug/kg8.4
Isopropylbenzene 98-82-8 8260B ND 1ug/kg4.2
Methyl acetate 79-20-9 8260B ND 1ug/kg4.2
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg4.2
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg8.4
Methylcyclohexane 108-87-2 8260B ND 1ug/kg4.2
Methylene chloride 75-09-2 8260B ND 1ug/kg4.2
Styrene 100-42-5 8260B ND 1ug/kg4.2
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg4.2
Tetrachloroethene 127-18-4 8260B ND 1ug/kg4.2
Toluene 108-88-3 8260B ND 1ug/kg4.2
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg4.2
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg4.2
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4.2
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4.2
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 31 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-17 3-5'
LH17057-014
08/16/2010 1520
08/17/2010
Solid
% Solids:89.8 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0620 SJS1 40358 6.65
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg4.2
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg4.2
Vinyl chloride 75-01-4 8260B ND 1ug/kg4.2
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.2
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 84 53-142
Bromofluorobenzene 97 47-138
Toluene-d8 94 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 32 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-17 13-15'
LH17057-015
08/16/2010 1525
08/17/2010
Solid
% Solids:85.6 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0644 SJS1 40358 6.32
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg18
Benzene 71-43-2 8260B ND 1ug/kg4.6
Bromodichloromethane 75-27-4 8260B ND 1ug/kg4.6
Bromoform 75-25-2 8260B ND 1ug/kg4.6
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg4.6
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg9.2
Carbon disulfide 75-15-0 8260B ND 1ug/kg4.6
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg4.6
Chlorobenzene 108-90-7 8260B ND 1ug/kg4.6
Chloroethane 75-00-3 8260B ND 1ug/kg4.6
Chloroform 67-66-3 8260B ND 1ug/kg4.6
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg4.6
Cyclohexane 110-82-7 8260B ND 1ug/kg4.6
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg4.6
Dibromochloromethane 124-48-1 8260B ND 1ug/kg4.6
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4.6
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg4.6
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg4.6
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg4.6
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.6
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg4.6
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg4.6
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg4.6
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4.6
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg4.6
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4.6
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg4.6
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4.6
Ethylbenzene 100-41-4 8260B ND 1ug/kg4.6
2-Hexanone 591-78-6 8260B ND 1ug/kg9.2
Isopropylbenzene 98-82-8 8260B ND 1ug/kg4.6
Methyl acetate 79-20-9 8260B ND 1ug/kg4.6
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg4.6
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg9.2
Methylcyclohexane 108-87-2 8260B ND 1ug/kg4.6
Methylene chloride 75-09-2 8260B ND 1ug/kg4.6
Styrene 100-42-5 8260B ND 1ug/kg4.6
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg4.6
Tetrachloroethene 127-18-4 8260B ND 1ug/kg4.6
Toluene 108-88-3 8260B ND 1ug/kg4.6
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg4.6
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg4.6
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4.6
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4.6
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 33 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-17 13-15'
LH17057-015
08/16/2010 1525
08/17/2010
Solid
% Solids:85.6 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0644 SJS1 40358 6.32
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg4.6
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg4.6
Vinyl chloride 75-01-4 8260B ND 1ug/kg4.6
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.6
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 92 53-142
Bromofluorobenzene 110 47-138
Toluene-d8 110 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 34 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-18 0-2'
LH17057-016
08/16/2010 1555
08/17/2010
Solid
% Solids:86.1 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0707 SJS1 40358 5.74
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg20
Benzene 71-43-2 8260B ND 1ug/kg5.1
Bromodichloromethane 75-27-4 8260B ND 1ug/kg5.1
Bromoform 75-25-2 8260B ND 1ug/kg5.1
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg5.1
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg10
Carbon disulfide 75-15-0 8260B ND 1ug/kg5.1
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg5.1
Chlorobenzene 108-90-7 8260B ND 1ug/kg5.1
Chloroethane 75-00-3 8260B ND 1ug/kg5.1
Chloroform 67-66-3 8260B ND 1ug/kg5.1
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg5.1
Cyclohexane 110-82-7 8260B ND 1ug/kg5.1
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg5.1
Dibromochloromethane 124-48-1 8260B ND 1ug/kg5.1
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg5.1
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg5.1
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg5.1
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg5.1
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg5.1
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg5.1
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg5.1
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg5.1
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg5.1
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg5.1
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg5.1
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg5.1
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg5.1
Ethylbenzene 100-41-4 8260B ND 1ug/kg5.1
2-Hexanone 591-78-6 8260B ND 1ug/kg10
Isopropylbenzene 98-82-8 8260B ND 1ug/kg5.1
Methyl acetate 79-20-9 8260B ND 1ug/kg5.1
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg5.1
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg10
Methylcyclohexane 108-87-2 8260B ND 1ug/kg5.1
Methylene chloride 75-09-2 8260B ND 1ug/kg5.1
Styrene 100-42-5 8260B ND 1ug/kg5.1
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg5.1
Tetrachloroethene 127-18-4 8260B ND 1ug/kg5.1
Toluene 108-88-3 8260B ND 1ug/kg5.1
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg5.1
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg5.1
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg5.1
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg5.1
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 35 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-18 0-2'
LH17057-016
08/16/2010 1555
08/17/2010
Solid
% Solids:86.1 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0707 SJS1 40358 5.74
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg5.1
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg5.1
Vinyl chloride 75-01-4 8260B ND 1ug/kg5.1
Xylenes (total)1330-20-7 8260B ND 1ug/kg5.1
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 86 53-142
Bromofluorobenzene 104 47-138
Toluene-d8 104 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 36 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-18 13-15'
LH17057-017
08/16/2010 1600
08/17/2010
Solid
% Solids:84.5 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
2 5035 8260B 1 08/19/2010 1407 SJS1 40410 6.72
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 2ug/kg18
Benzene 71-43-2 8260B ND 2ug/kg4.4
Bromodichloromethane 75-27-4 8260B ND 2ug/kg4.4
Bromoform 75-25-2 8260B ND 2ug/kg4.4
Bromomethane (Methyl bromide)74-83-9 8260B ND 2ug/kg4.4
2-Butanone (MEK)78-93-3 8260B ND 2ug/kg8.8
Carbon disulfide 75-15-0 8260B ND 2ug/kg4.4
Carbon tetrachloride 56-23-5 8260B ND 2ug/kg4.4
Chlorobenzene 108-90-7 8260B ND 2ug/kg4.4
Chloroethane 75-00-3 8260B ND 2ug/kg4.4
Chloroform 67-66-3 8260B ND 2ug/kg4.4
Chloromethane (Methyl chloride)74-87-3 8260B ND 2ug/kg4.4
Cyclohexane 110-82-7 8260B ND 2ug/kg4.4
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 2ug/kg4.4
Dibromochloromethane 124-48-1 8260B ND 2ug/kg4.4
1,2-Dibromoethane (EDB)106-93-4 8260B ND 2ug/kg4.4
1,2-Dichlorobenzene 95-50-1 8260B ND 2ug/kg4.4
1,3-Dichlorobenzene 541-73-1 8260B ND 2ug/kg4.4
1,4-Dichlorobenzene 106-46-7 8260B ND 2ug/kg4.4
Dichlorodifluoromethane 75-71-8 8260B ND 2ug/kg4.4
1,1-Dichloroethane 75-34-3 8260B ND 2ug/kg4.4
1,2-Dichloroethane 107-06-2 8260B ND 2ug/kg4.4
1,1-Dichloroethene 75-35-4 8260B ND 2ug/kg4.4
cis-1,2-Dichloroethene 156-59-2 8260B ND 2ug/kg4.4
trans-1,2-Dichloroethene 156-60-5 8260B ND 2ug/kg4.4
1,2-Dichloropropane 78-87-5 8260B ND 2ug/kg4.4
cis-1,3-Dichloropropene 10061-01-5 8260B ND 2ug/kg4.4
trans-1,3-Dichloropropene 10061-02-6 8260B ND 2ug/kg4.4
Ethylbenzene 100-41-4 8260B ND 2ug/kg4.4
2-Hexanone 591-78-6 8260B ND 2ug/kg8.8
Isopropylbenzene 98-82-8 8260B ND 2ug/kg4.4
Methyl acetate 79-20-9 8260B ND 2ug/kg4.4
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 2ug/kg4.4
4-Methyl-2-pentanone 108-10-1 8260B ND 2ug/kg8.8
Methylcyclohexane 108-87-2 8260B ND 2ug/kg4.4
Methylene chloride 75-09-2 8260B ND 2ug/kg4.4
Styrene 100-42-5 8260B ND 2ug/kg4.4
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 2ug/kg4.4
Tetrachloroethene 127-18-4 8260B ND 2ug/kg4.4
Toluene 108-88-3 8260B ND 2ug/kg4.4
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 2ug/kg4.4
1,2,4-Trichlorobenzene 120-82-1 8260B ND 2ug/kg4.4
1,1,1-Trichloroethane 71-55-6 8260B ND 2ug/kg4.4
1,1,2-Trichloroethane 79-00-5 8260B ND 2ug/kg4.4
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 37 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-18 13-15'
LH17057-017
08/16/2010 1600
08/17/2010
Solid
% Solids:84.5 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
2 5035 8260B 1 08/19/2010 1407 SJS1 40410 6.72
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 2ug/kg4.4
Trichlorofluoromethane 75-69-4 8260B ND 2ug/kg4.4
Vinyl chloride 75-01-4 8260B ND 2ug/kg4.4
Xylenes (total)1330-20-7 8260B ND 2ug/kg4.4
AcceptanceRun 2
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 78 53-142
Bromofluorobenzene 91 47-138
Toluene-d8 92 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 38 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-19 3-5'
LH17057-018
08/17/2010 0930
08/17/2010
Solid
% Solids:82.4 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0755 SJS1 40358 5.63
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg22
Benzene 71-43-2 8260B ND 1ug/kg5.4
Bromodichloromethane 75-27-4 8260B ND 1ug/kg5.4
Bromoform 75-25-2 8260B ND 1ug/kg5.4
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg5.4
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg11
Carbon disulfide 75-15-0 8260B ND 1ug/kg5.4
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg5.4
Chlorobenzene 108-90-7 8260B ND 1ug/kg5.4
Chloroethane 75-00-3 8260B ND 1ug/kg5.4
Chloroform 67-66-3 8260B ND 1ug/kg5.4
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg5.4
Cyclohexane 110-82-7 8260B ND 1ug/kg5.4
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg5.4
Dibromochloromethane 124-48-1 8260B ND 1ug/kg5.4
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg5.4
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg5.4
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg5.4
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg5.4
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg5.4
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg5.4
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg5.4
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg5.4
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg5.4
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg5.4
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg5.4
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg5.4
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg5.4
Ethylbenzene 100-41-4 8260B ND 1ug/kg5.4
2-Hexanone 591-78-6 8260B ND 1ug/kg11
Isopropylbenzene 98-82-8 8260B ND 1ug/kg5.4
Methyl acetate 79-20-9 8260B ND 1ug/kg5.4
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg5.4
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg11
Methylcyclohexane 108-87-2 8260B ND 1ug/kg5.4
Methylene chloride 75-09-2 8260B ND 1ug/kg5.4
Styrene 100-42-5 8260B ND 1ug/kg5.4
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg5.4
Tetrachloroethene 127-18-4 8260B ND 1ug/kg5.4
Toluene 108-88-3 8260B ND 1ug/kg5.4
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg5.4
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg5.4
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg5.4
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg5.4
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 39 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-19 3-5'
LH17057-018
08/17/2010 0930
08/17/2010
Solid
% Solids:82.4 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0755 SJS1 40358 5.63
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg5.4
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg5.4
Vinyl chloride 75-01-4 8260B ND 1ug/kg5.4
Xylenes (total)1330-20-7 8260B ND 1ug/kg5.4
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 87 53-142
Bromofluorobenzene 104 47-138
Toluene-d8 104 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 40 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-10 13-15'
LH17057-019
08/17/2010 0935
08/17/2010
Solid
% Solids:87.5 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0818 SJS1 40358 6.02
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg19
Benzene 71-43-2 8260B ND 1ug/kg4.7
Bromodichloromethane 75-27-4 8260B ND 1ug/kg4.7
Bromoform 75-25-2 8260B ND 1ug/kg4.7
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg4.7
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg9.5
Carbon disulfide 75-15-0 8260B ND 1ug/kg4.7
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg4.7
Chlorobenzene 108-90-7 8260B ND 1ug/kg4.7
Chloroethane 75-00-3 8260B ND 1ug/kg4.7
Chloroform 67-66-3 8260B ND 1ug/kg4.7
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg4.7
Cyclohexane 110-82-7 8260B ND 1ug/kg4.7
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg4.7
Dibromochloromethane 124-48-1 8260B ND 1ug/kg4.7
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4.7
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg4.7
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg4.7
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg4.7
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.7
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg4.7
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg4.7
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg4.7
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4.7
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg4.7
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4.7
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg4.7
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4.7
Ethylbenzene 100-41-4 8260B ND 1ug/kg4.7
2-Hexanone 591-78-6 8260B ND 1ug/kg9.5
Isopropylbenzene 98-82-8 8260B ND 1ug/kg4.7
Methyl acetate 79-20-9 8260B ND 1ug/kg4.7
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg4.7
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg9.5
Methylcyclohexane 108-87-2 8260B ND 1ug/kg4.7
Methylene chloride 75-09-2 8260B ND 1ug/kg4.7
Styrene 100-42-5 8260B ND 1ug/kg4.7
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg4.7
Tetrachloroethene 127-18-4 8260B ND 1ug/kg4.7
Toluene 108-88-3 8260B ND 1ug/kg4.7
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg4.7
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg4.7
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4.7
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4.7
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 41 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-10 13-15'
LH17057-019
08/17/2010 0935
08/17/2010
Solid
% Solids:87.5 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0818 SJS1 40358 6.02
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg4.7
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg4.7
Vinyl chloride 75-01-4 8260B ND 1ug/kg4.7
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.7
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 92 53-142
Bromofluorobenzene 109 47-138
Toluene-d8 108 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 42 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-20 3-5'
LH17057-020
08/17/2010 1010
08/17/2010
Solid
% Solids:87.4 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0842 SJS1 40358 6.66
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg17
Benzene 71-43-2 8260B ND 1ug/kg4.3
Bromodichloromethane 75-27-4 8260B ND 1ug/kg4.3
Bromoform 75-25-2 8260B ND 1ug/kg4.3
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg4.3
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg8.6
Carbon disulfide 75-15-0 8260B ND 1ug/kg4.3
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg4.3
Chlorobenzene 108-90-7 8260B ND 1ug/kg4.3
Chloroethane 75-00-3 8260B ND 1ug/kg4.3
Chloroform 67-66-3 8260B ND 1ug/kg4.3
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg4.3
Cyclohexane 110-82-7 8260B ND 1ug/kg4.3
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg4.3
Dibromochloromethane 124-48-1 8260B ND 1ug/kg4.3
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4.3
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg4.3
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg4.3
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg4.3
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.3
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg4.3
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg4.3
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg4.3
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4.3
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg4.3
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4.3
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg4.3
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4.3
Ethylbenzene 100-41-4 8260B ND 1ug/kg4.3
2-Hexanone 591-78-6 8260B ND 1ug/kg8.6
Isopropylbenzene 98-82-8 8260B ND 1ug/kg4.3
Methyl acetate 79-20-9 8260B ND 1ug/kg4.3
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg4.3
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg8.6
Methylcyclohexane 108-87-2 8260B ND 1ug/kg4.3
Methylene chloride 75-09-2 8260B ND 1ug/kg4.3
Styrene 100-42-5 8260B ND 1ug/kg4.3
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg4.3
Tetrachloroethene 127-18-4 8260B ND 1ug/kg4.3
Toluene 108-88-3 8260B ND 1ug/kg4.3
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg4.3
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg4.3
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4.3
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4.3
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 43 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-20 3-5'
LH17057-020
08/17/2010 1010
08/17/2010
Solid
% Solids:87.4 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0842 SJS1 40358 6.66
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg4.3
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg4.3
Vinyl chloride 75-01-4 8260B ND 1ug/kg4.3
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.3
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 76 53-142
Bromofluorobenzene 92 47-138
Toluene-d8 91 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 44 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-20 13-15'
LH17057-021
08/17/2010 1015
08/17/2010
Solid
% Solids:85.3 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0906 SJS1 40358 7.36
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg16
Benzene 71-43-2 8260B ND 1ug/kg4.0
Bromodichloromethane 75-27-4 8260B ND 1ug/kg4.0
Bromoform 75-25-2 8260B ND 1ug/kg4.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg4.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg8.0
Carbon disulfide 75-15-0 8260B ND 1ug/kg4.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg4.0
Chlorobenzene 108-90-7 8260B ND 1ug/kg4.0
Chloroethane 75-00-3 8260B ND 1ug/kg4.0
Chloroform 67-66-3 8260B ND 1ug/kg4.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg4.0
Cyclohexane 110-82-7 8260B ND 1ug/kg4.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg4.0
Dibromochloromethane 124-48-1 8260B ND 1ug/kg4.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg4.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg4.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg4.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg4.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg4.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg4.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg4.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg4.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4.0
Ethylbenzene 100-41-4 8260B ND 1ug/kg4.0
2-Hexanone 591-78-6 8260B ND 1ug/kg8.0
Isopropylbenzene 98-82-8 8260B ND 1ug/kg4.0
Methyl acetate 79-20-9 8260B ND 1ug/kg4.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg4.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg8.0
Methylcyclohexane 108-87-2 8260B ND 1ug/kg4.0
Methylene chloride 75-09-2 8260B ND 1ug/kg4.0
Styrene 100-42-5 8260B ND 1ug/kg4.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg4.0
Tetrachloroethene 127-18-4 8260B ND 1ug/kg4.0
Toluene 108-88-3 8260B ND 1ug/kg4.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg4.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg4.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 45 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-20 13-15'
LH17057-021
08/17/2010 1015
08/17/2010
Solid
% Solids:85.3 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 0906 SJS1 40358 7.36
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg4.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg4.0
Vinyl chloride 75-01-4 8260B ND 1ug/kg4.0
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 96 53-142
Bromofluorobenzene 111 47-138
Toluene-d8 108 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 46 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
SP-1 6-8'
LH17057-022
08/17/2010 1050
08/17/2010
Solid
% Solids:87.8 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 1431 SJS1 40410 6.88
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg17
Benzene 71-43-2 8260B ND 1ug/kg4.1
Bromodichloromethane 75-27-4 8260B ND 1ug/kg4.1
Bromoform 75-25-2 8260B ND 1ug/kg4.1
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg4.1
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg8.3
Carbon disulfide 75-15-0 8260B ND 1ug/kg4.1
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg4.1
Chlorobenzene 108-90-7 8260B ND 1ug/kg4.1
Chloroethane 75-00-3 8260B ND 1ug/kg4.1
Chloroform 67-66-3 8260B ND 1ug/kg4.1
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg4.1
Cyclohexane 110-82-7 8260B ND 1ug/kg4.1
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg4.1
Dibromochloromethane 124-48-1 8260B ND 1ug/kg4.1
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4.1
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg4.1
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg4.1
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg4.1
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.1
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg4.1
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg4.1
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg4.1
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4.1
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg4.1
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4.1
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg4.1
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4.1
Ethylbenzene 100-41-4 8260B ND 1ug/kg4.1
2-Hexanone 591-78-6 8260B ND 1ug/kg8.3
Isopropylbenzene 98-82-8 8260B ND 1ug/kg4.1
Methyl acetate 79-20-9 8260B ND 1ug/kg4.1
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg4.1
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg8.3
Methylcyclohexane 108-87-2 8260B ND 1ug/kg4.1
Methylene chloride 75-09-2 8260B ND 1ug/kg4.1
Styrene 100-42-5 8260B ND 1ug/kg4.1
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg4.1
Tetrachloroethene 127-18-4 8260B ND 1ug/kg4.1
Toluene 108-88-3 8260B ND 1ug/kg4.1
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg4.1
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg4.1
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4.1
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4.1
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 47 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
SP-1 6-8'
LH17057-022
08/17/2010 1050
08/17/2010
Solid
% Solids:87.8 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 1431 SJS1 40410 6.88
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg4.1
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg4.1
Vinyl chloride 75-01-4 8260B ND 1ug/kg4.1
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.1
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 91 53-142
Bromofluorobenzene 103 47-138
Toluene-d8 109 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 48 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
SP-1 16-18'
LH17057-023
08/17/2010 1055
08/17/2010
Solid
% Solids:78.9 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 1455 SJS1 40410 6.53
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg19
Benzene 71-43-2 8260B ND 1ug/kg4.9
Bromodichloromethane 75-27-4 8260B ND 1ug/kg4.9
Bromoform 75-25-2 8260B ND 1ug/kg4.9
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg4.9
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg9.7
Carbon disulfide 75-15-0 8260B ND 1ug/kg4.9
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg4.9
Chlorobenzene 108-90-7 8260B ND 1ug/kg4.9
Chloroethane 75-00-3 8260B ND 1ug/kg4.9
Chloroform 67-66-3 8260B ND 1ug/kg4.9
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg4.9
Cyclohexane 110-82-7 8260B ND 1ug/kg4.9
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg4.9
Dibromochloromethane 124-48-1 8260B ND 1ug/kg4.9
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4.9
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg4.9
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg4.9
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg4.9
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.9
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg4.9
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg4.9
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg4.9
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4.9
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg4.9
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4.9
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg4.9
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4.9
Ethylbenzene 100-41-4 8260B ND 1ug/kg4.9
2-Hexanone 591-78-6 8260B ND 1ug/kg9.7
Isopropylbenzene 98-82-8 8260B ND 1ug/kg4.9
Methyl acetate 79-20-9 8260B ND 1ug/kg4.9
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg4.9
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg9.7
Methylcyclohexane 108-87-2 8260B ND 1ug/kg4.9
Methylene chloride 75-09-2 8260B ND 1ug/kg4.9
Styrene 100-42-5 8260B ND 1ug/kg4.9
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg4.9
Tetrachloroethene 127-18-4 8260B ND 1ug/kg4.9
Toluene 108-88-3 8260B ND 1ug/kg4.9
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg4.9
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg4.9
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4.9
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4.9
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 49 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
SP-1 16-18'
LH17057-023
08/17/2010 1055
08/17/2010
Solid
% Solids:78.9 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 1455 SJS1 40410 6.53
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg4.9
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg4.9
Vinyl chloride 75-01-4 8260B ND 1ug/kg4.9
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.9
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 86 53-142
Bromofluorobenzene 96 47-138
Toluene-d8 104 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 50 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
SP-2 6-8'
LH17057-024
08/17/2010 1115
08/17/2010
Solid
% Solids:86.9 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 1519 SJS1 40410 6.09
2 5035 8260B 1 08/20/2010 1145 SJS1 40511 6.57
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 2ug/kg18
Benzene 71-43-2 8260B ND 1ug/kg4.7
Bromodichloromethane 75-27-4 8260B ND 1ug/kg4.7
Bromoform 75-25-2 8260B ND 1ug/kg4.7
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg4.7
2-Butanone (MEK)78-93-3 8260B ND 2ug/kg8.8
Carbon disulfide 75-15-0 8260B ND 1ug/kg4.7
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg4.7
Chlorobenzene 108-90-7 8260B ND 1ug/kg4.7
Chloroethane 75-00-3 8260B ND 1ug/kg4.7
Chloroform 67-66-3 8260B ND 1ug/kg4.7
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg4.7
Cyclohexane 110-82-7 8260B ND 1ug/kg4.7
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg4.7
Dibromochloromethane 124-48-1 8260B ND 1ug/kg4.7
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4.7
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg4.7
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg4.7
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg4.7
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.7
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg4.7
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg4.7
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg4.7
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4.7
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg4.7
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4.7
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg4.7
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4.7
Ethylbenzene 100-41-4 8260B ND 1ug/kg4.7
2-Hexanone 591-78-6 8260B ND 1ug/kg9.5
Isopropylbenzene 98-82-8 8260B ND 1ug/kg4.7
Methyl acetate 79-20-9 8260B ND 1ug/kg4.7
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg4.7
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg9.5
Methylcyclohexane 108-87-2 8260B ND 1ug/kg4.7
Methylene chloride 75-09-2 8260B ND 1ug/kg4.7
Styrene 100-42-5 8260B ND 1ug/kg4.7
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg4.7
Tetrachloroethene 127-18-4 8260B ND 1ug/kg4.7
Toluene 108-88-3 8260B ND 1ug/kg4.7
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg4.7
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg4.7
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4.7
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 51 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
SP-2 6-8'
LH17057-024
08/17/2010 1115
08/17/2010
Solid
% Solids:86.9 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 1519 SJS1 40410 6.09
2 5035 8260B 1 08/20/2010 1145 SJS1 40511 6.57
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4.7
Trichloroethene 79-01-6 8260B ND 1ug/kg4.7
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg4.7
Vinyl chloride 75-01-4 8260B ND 1ug/kg4.7
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.7
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
1,2-Dichloroethane-d4 89 53-142 84 53-142
Bromofluorobenzene 102 47-138 108 47-138
Toluene-d8 107 68-124 99 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 52 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
SP-2 16-18'
LH17057-025
08/17/2010 1120
08/17/2010
Solid
% Solids:85.1 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 1543 SJS1 40410 6.51
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/kg18
Benzene 71-43-2 8260B ND 1ug/kg4.5
Bromodichloromethane 75-27-4 8260B ND 1ug/kg4.5
Bromoform 75-25-2 8260B ND 1ug/kg4.5
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg4.5
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg9.0
Carbon disulfide 75-15-0 8260B ND 1ug/kg4.5
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg4.5
Chlorobenzene 108-90-7 8260B ND 1ug/kg4.5
Chloroethane 75-00-3 8260B ND 1ug/kg4.5
Chloroform 67-66-3 8260B ND 1ug/kg4.5
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg4.5
Cyclohexane 110-82-7 8260B ND 1ug/kg4.5
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg4.5
Dibromochloromethane 124-48-1 8260B ND 1ug/kg4.5
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4.5
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg4.5
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg4.5
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg4.5
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.5
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg4.5
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg4.5
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg4.5
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4.5
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg4.5
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4.5
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg4.5
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4.5
Ethylbenzene 100-41-4 8260B ND 1ug/kg4.5
2-Hexanone 591-78-6 8260B ND 1ug/kg9.0
Isopropylbenzene 98-82-8 8260B ND 1ug/kg4.5
Methyl acetate 79-20-9 8260B ND 1ug/kg4.5
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg4.5
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg9.0
Methylcyclohexane 108-87-2 8260B ND 1ug/kg4.5
Methylene chloride 75-09-2 8260B ND 1ug/kg4.5
Styrene 100-42-5 8260B ND 1ug/kg4.5
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg4.5
Tetrachloroethene 127-18-4 8260B ND 1ug/kg4.5
Toluene 108-88-3 8260B ND 1ug/kg4.5
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg4.5
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg4.5
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4.5
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4.5
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 53 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
SP-2 16-18'
LH17057-025
08/17/2010 1120
08/17/2010
Solid
% Solids:85.1 08/17/2010 2157
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/19/2010 1543 SJS1 40410 6.51
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/kg4.5
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg4.5
Vinyl chloride 75-01-4 8260B ND 1ug/kg4.5
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.5
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 97 53-142
Bromofluorobenzene 108 47-138
Toluene-d8 110 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 54 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
QC Summary
Page: 55 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:LQ40358-001
40358 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL Units Analysis DateDil
Acetone ND 08/19/2010 002520ug/kg1
Benzene ND 08/19/2010 00255.0 ug/kg1
Bromodichloromethane ND 08/19/2010 00255.0 ug/kg1
Bromoform ND 08/19/2010 00255.0 ug/kg1
Bromomethane (Methyl bromide)ND 08/19/2010 00255.0 ug/kg1
2-Butanone (MEK)ND 08/19/2010 002510ug/kg1
Carbon disulfide ND 08/19/2010 00255.0 ug/kg1
Carbon tetrachloride ND 08/19/2010 00255.0 ug/kg1
Chlorobenzene ND 08/19/2010 00255.0 ug/kg1
Chloroethane ND 08/19/2010 00255.0 ug/kg1
Chloroform ND 08/19/2010 00255.0 ug/kg1
Chloromethane (Methyl chloride)ND 08/19/2010 00255.0 ug/kg1
Cyclohexane ND 08/19/2010 00255.0 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 08/19/2010 00255.0 ug/kg1
Dibromochloromethane ND 08/19/2010 00255.0 ug/kg1
1,2-Dibromoethane (EDB)ND 08/19/2010 00255.0 ug/kg1
1,3-Dichlorobenzene ND 08/19/2010 00255.0 ug/kg1
1,2-Dichlorobenzene ND 08/19/2010 00255.0 ug/kg1
1,4-Dichlorobenzene ND 08/19/2010 00255.0 ug/kg1
Dichlorodifluoromethane ND 08/19/2010 00255.0 ug/kg1
1,1-Dichloroethane ND 08/19/2010 00255.0 ug/kg1
1,2-Dichloroethane ND 08/19/2010 00255.0 ug/kg1
1,1-Dichloroethene ND 08/19/2010 00255.0 ug/kg1
cis-1,2-Dichloroethene ND 08/19/2010 00255.0 ug/kg1
trans-1,2-Dichloroethene ND 08/19/2010 00255.0 ug/kg1
1,2-Dichloropropane ND 08/19/2010 00255.0 ug/kg1
cis-1,3-Dichloropropene ND 08/19/2010 00255.0 ug/kg1
trans-1,3-Dichloropropene ND 08/19/2010 00255.0 ug/kg1
Ethylbenzene ND 08/19/2010 00255.0 ug/kg1
2-Hexanone ND 08/19/2010 002510ug/kg1
Isopropylbenzene ND 08/19/2010 00255.0 ug/kg1
Methyl acetate ND 08/19/2010 00255.0 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 08/19/2010 00255.0 ug/kg1
4-Methyl-2-pentanone ND 08/19/2010 002510ug/kg1
Methylcyclohexane ND 08/19/2010 00255.0 ug/kg1
Methylene chloride ND 08/19/2010 00255.0 ug/kg1
Styrene ND 08/19/2010 00255.0 ug/kg1
1,1,2,2-Tetrachloroethane ND 08/19/2010 00255.0 ug/kg1
Tetrachloroethene ND 08/19/2010 00255.0 ug/kg1
Toluene ND 08/19/2010 00255.0 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 08/19/2010 00255.0 ug/kg1
1,2,4-Trichlorobenzene ND 08/19/2010 00255.0 ug/kg1
1,1,2-Trichloroethane ND 08/19/2010 00255.0 ug/kg1
1,1,1-Trichloroethane ND 08/19/2010 00255.0 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 56 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:LQ40358-001
40358 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL Units Analysis DateDil
Trichloroethene ND 08/19/2010 00255.0 ug/kg1
Trichlorofluoromethane ND 08/19/2010 00255.0 ug/kg1
Vinyl chloride ND 08/19/2010 00255.0 ug/kg1
Xylenes (total)ND 08/19/2010 00255.0 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 98 47-138
1,2-Dichloroethane-d4 87 53-142
Toluene-d8 99 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 57 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:LQ40358-002
40358 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 370 08/18/2010 2316N36910042-1491
Benzene 56 08/18/2010 23161135069-1231
Bromodichloromethane 57 08/18/2010 23161155069-1211
Bromoform 52 08/18/2010 23161035061-1191
Bromomethane (Methyl bromide)54 08/18/2010 23161085035-1441
2-Butanone (MEK)100 08/18/2010 231610010057-1481
Carbon disulfide 63 08/18/2010 2316N1265058-1221
Carbon tetrachloride 60 08/18/2010 23161195058-1361
Chlorobenzene 54 08/18/2010 23161085059-1291
Chloroethane 51 08/18/2010 23161035050-1321
Chloroform 57 08/18/2010 23161145071-1251
Chloromethane (Methyl chloride)58 08/18/2010 23161155034-1341
Cyclohexane 65 08/18/2010 23161295053-1391
1,2-Dibromo-3-chloropropane (DBCP)52 08/18/2010 23161045055-1251
Dibromochloromethane 55 08/18/2010 23161095066-1191
1,2-Dibromoethane (EDB)54 08/18/2010 23161095074-1241
1,3-Dichlorobenzene 57 08/18/2010 23161155051-1341
1,2-Dichlorobenzene 55 08/18/2010 23161105057-1311
1,4-Dichlorobenzene 56 08/18/2010 23161115052-1331
Dichlorodifluoromethane 86 08/18/2010 2316N1725010-1571
1,1-Dichloroethane 57 08/18/2010 23161145071-1271
1,2-Dichloroethane 53 08/18/2010 23161065067-1291
1,1-Dichloroethene 58 08/18/2010 23161155069-1381
cis-1,2-Dichloroethene 55 08/18/2010 23161105070-1221
trans-1,2-Dichloroethene 56 08/18/2010 23161125068-1311
1,2-Dichloropropane 56 08/18/2010 23161125072-1241
cis-1,3-Dichloropropene 57 08/18/2010 23161135070-1261
trans-1,3-Dichloropropene 57 08/18/2010 23161145070-1241
Ethylbenzene 58 08/18/2010 23161155059-1281
2-Hexanone 100 08/18/2010 231610210054-1371
Isopropylbenzene 67 08/18/2010 23161335050-1361
Methyl acetate 58 08/18/2010 23161155059-1371
Methyl tertiary butyl ether (MTBE)57 08/18/2010 23161145072-1221
4-Methyl-2-pentanone 99 08/18/2010 23169910060-1341
Methylcyclohexane 66 08/18/2010 23161325041-1441
Methylene chloride 54 08/18/2010 23161085077-1291
Styrene 60 08/18/2010 23161195054-1361
1,1,2,2-Tetrachloroethane 55 08/18/2010 23161115069-1321
Tetrachloroethene 57 08/18/2010 23161135070-1301
Toluene 57 08/18/2010 23161155061-1291
1,1,2-Trichloro-1,2,2-Trifluoroethane 69 08/18/2010 2316N1385049-1361
1,2,4-Trichlorobenzene 56 08/18/2010 23161125034-1451
1,1,2-Trichloroethane 54 08/18/2010 23161085055-1281
1,1,1-Trichloroethane 60 08/18/2010 23161205063-1281
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 58 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:LQ40358-002
40358 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 56 08/18/2010 23161115062-1261
Trichlorofluoromethane 66 08/18/2010 23161325045-1381
Vinyl chloride 59 08/18/2010 23161185042-1321
Xylenes (total)120 08/18/2010 231611710058-1281
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 114 47-138
1,2-Dichloroethane-d4 92 53-142
Toluene-d8 111 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 59 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:LQ40358-003
40358 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Acetone 160 08/18/2010 2339N,+156100 42-14981 201
Benzene 57 08/18/2010 23391145069-1231.0 201
Bromodichloromethane 59 08/18/2010 23391185069-1213.3 201
Bromoform 51 08/18/2010 23391035061-1190.79 201
Bromomethane (Methyl bromide)55 08/18/2010 23391105035-1442.4 201
2-Butanone (MEK)100 08/18/2010 233910210057-1482.3 201
Carbon disulfide 65 08/18/2010 2339N1305058-1223.5 201
Carbon tetrachloride 62 08/18/2010 23391235058-1363.3 201
Chlorobenzene 55 08/18/2010 23391095059-1291.3 201
Chloroethane 54 08/18/2010 23391085050-1325.2 201
Chloroform 59 08/18/2010 23391195071-1254.7 201
Chloromethane (Methyl chloride)61 08/18/2010 23391215034-1344.7 201
Cyclohexane 65 08/18/2010 23391315053-1391.1 201
1,2-Dibromo-3-chloropropane (DBCP)53 08/18/2010 23391055055-1251.1 201
Dibromochloromethane 54 08/18/2010 23391085066-1190.84 201
1,2-Dibromoethane (EDB)54 08/18/2010 23391085074-1240.63 201
1,3-Dichlorobenzene 56 08/18/2010 23391125051-1342.5 201
1,2-Dichlorobenzene 54 08/18/2010 23391085057-1311.7 201
1,4-Dichlorobenzene 56 08/18/2010 23391125052-1330.69 201
Dichlorodifluoromethane 92 08/18/2010 2339N1835010-1576.7 201
1,1-Dichloroethane 59 08/18/2010 23391195071-1274.3 201
1,2-Dichloroethane 55 08/18/2010 23391115067-1294.2 201
1,1-Dichloroethene 59 08/18/2010 23391185069-1382.4 201
cis-1,2-Dichloroethene 58 08/18/2010 23391165070-1224.7 201
trans-1,2-Dichloroethene 59 08/18/2010 23391185068-1315.1 201
1,2-Dichloropropane 58 08/18/2010 23391165072-1243.5 201
cis-1,3-Dichloropropene 58 08/18/2010 23391165070-1262.5 201
trans-1,3-Dichloropropene 57 08/18/2010 23391155070-1240.44 201
Ethylbenzene 58 08/18/2010 23391155059-1280.17 201
2-Hexanone 100 08/18/2010 233910210054-1370.47 201
Isopropylbenzene 65 08/18/2010 23391305050-1362.2 201
Methyl acetate 62 08/18/2010 23391235059-1376.8 201
Methyl tertiary butyl ether (MTBE)60 08/18/2010 23391195072-1224.3 201
4-Methyl-2-pentanone 99 08/18/2010 23399910060-1340.37 201
Methylcyclohexane 67 08/18/2010 23391345041-1442.0 201
Methylene chloride 56 08/18/2010 23391115077-1293.5 201
Styrene 61 08/18/2010 23391215054-1361.3 201
1,1,2,2-Tetrachloroethane 54 08/18/2010 23391095069-1321.7 201
Tetrachloroethene 57 08/18/2010 23391145070-1300.44 201
Toluene 58 08/18/2010 23391175061-1291.5 201
1,1,2-Trichloro-1,2,2-Trifluoroethane 71 08/18/2010 2339N1425049-1362.3 201
1,2,4-Trichlorobenzene 55 08/18/2010 23391105034-1451.9 201
1,1,2-Trichloroethane 53 08/18/2010 23391055055-1282.3 201
1,1,1-Trichloroethane 63 08/18/2010 23391275063-1285.6 201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 60 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:LQ40358-003
40358 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Trichloroethene 57 08/18/2010 23391135062-1261.8 201
Trichlorofluoromethane 67 08/18/2010 23391335045-1381.0 201
Vinyl chloride 61 08/18/2010 23391215042-1322.8 201
Xylenes (total)120 08/18/2010 233911810058-1280.049 201
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 117 47-138
1,2-Dichloroethane-d4 94 53-142
Toluene-d8 115 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 61 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:LQ40376-001
40376 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL Units Analysis DateDil
Acetone ND 08/18/2010 121520ug/kg1
Benzene ND 08/18/2010 12155.0 ug/kg1
Bromodichloromethane ND 08/18/2010 12155.0 ug/kg1
Bromoform ND 08/18/2010 12155.0 ug/kg1
Bromomethane (Methyl bromide)ND 08/18/2010 12155.0 ug/kg1
2-Butanone (MEK)ND 08/18/2010 121510ug/kg1
Carbon disulfide ND 08/18/2010 12155.0 ug/kg1
Carbon tetrachloride ND 08/18/2010 12155.0 ug/kg1
Chlorobenzene ND 08/18/2010 12155.0 ug/kg1
Chloroethane ND 08/18/2010 12155.0 ug/kg1
Chloroform ND 08/18/2010 12155.0 ug/kg1
Chloromethane (Methyl chloride)ND 08/18/2010 12155.0 ug/kg1
Cyclohexane ND 08/18/2010 12155.0 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 08/18/2010 12155.0 ug/kg1
Dibromochloromethane ND 08/18/2010 12155.0 ug/kg1
1,2-Dibromoethane (EDB)ND 08/18/2010 12155.0 ug/kg1
1,2-Dichlorobenzene ND 08/18/2010 12155.0 ug/kg1
1,3-Dichlorobenzene ND 08/18/2010 12155.0 ug/kg1
1,4-Dichlorobenzene ND 08/18/2010 12155.0 ug/kg1
Dichlorodifluoromethane ND 08/18/2010 12155.0 ug/kg1
1,1-Dichloroethane ND 08/18/2010 12155.0 ug/kg1
1,2-Dichloroethane ND 08/18/2010 12155.0 ug/kg1
trans-1,2-Dichloroethene ND 08/18/2010 12155.0 ug/kg1
cis-1,2-Dichloroethene ND 08/18/2010 12155.0 ug/kg1
1,1-Dichloroethene ND 08/18/2010 12155.0 ug/kg1
1,2-Dichloropropane ND 08/18/2010 12155.0 ug/kg1
cis-1,3-Dichloropropene ND 08/18/2010 12155.0 ug/kg1
trans-1,3-Dichloropropene ND 08/18/2010 12155.0 ug/kg1
Ethylbenzene ND 08/18/2010 12155.0 ug/kg1
2-Hexanone ND 08/18/2010 121510ug/kg1
Isopropylbenzene ND 08/18/2010 12155.0 ug/kg1
Methyl acetate ND 08/18/2010 12155.0 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 08/18/2010 12155.0 ug/kg1
4-Methyl-2-pentanone ND 08/18/2010 121510ug/kg1
Methylcyclohexane ND 08/18/2010 12155.0 ug/kg1
Methylene chloride ND 08/18/2010 12155.0 ug/kg1
Styrene ND 08/18/2010 12155.0 ug/kg1
1,1,2,2-Tetrachloroethane ND 08/18/2010 12155.0 ug/kg1
Tetrachloroethene ND 08/18/2010 12155.0 ug/kg1
Toluene ND 08/18/2010 12155.0 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 08/18/2010 12155.0 ug/kg1
1,2,4-Trichlorobenzene ND 08/18/2010 12155.0 ug/kg1
1,1,2-Trichloroethane ND 08/18/2010 12155.0 ug/kg1
1,1,1-Trichloroethane ND 08/18/2010 12155.0 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 62 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:LQ40376-001
40376 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL Units Analysis DateDil
Trichloroethene ND 08/18/2010 12155.0 ug/kg1
Trichlorofluoromethane ND 08/18/2010 12155.0 ug/kg1
Vinyl chloride ND 08/18/2010 12155.0 ug/kg1
Xylenes (total)ND 08/18/2010 12155.0 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 110 47-138
1,2-Dichloroethane-d4 95 53-142
Toluene-d8 108 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 63 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:LQ40376-002
40376 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 100 08/18/2010 101710010042-1491
Benzene 53 08/18/2010 10171055069-1231
Bromodichloromethane 53 08/18/2010 10171065069-1211
Bromoform 49 08/18/2010 1017985061-1191
Bromomethane (Methyl bromide)46 08/18/2010 1017925035-1441
2-Butanone (MEK)97 08/18/2010 10179710057-1481
Carbon disulfide 59 08/18/2010 10171195058-1221
Carbon tetrachloride 57 08/18/2010 10171135058-1361
Chlorobenzene 50 08/18/2010 10171015059-1291
Chloroethane 44 08/18/2010 1017885050-1321
Chloroform 53 08/18/2010 10171055071-1251
Chloromethane (Methyl chloride)50 08/18/2010 10171015034-1341
Cyclohexane 59 08/18/2010 10171195053-1391
1,2-Dibromo-3-chloropropane (DBCP)49 08/18/2010 1017985055-1251
Dibromochloromethane 49 08/18/2010 1017975066-1191
1,2-Dibromoethane (EDB)50 08/18/2010 10171005074-1241
1,2-Dichlorobenzene 50 08/18/2010 10171015057-1311
1,3-Dichlorobenzene 52 08/18/2010 10171055051-1341
1,4-Dichlorobenzene 52 08/18/2010 10171035052-1331
Dichlorodifluoromethane 90 08/18/2010 1017N1805010-1571
1,1-Dichloroethane 54 08/18/2010 10171075071-1271
1,2-Dichloroethane 50 08/18/2010 10171015067-1291
trans-1,2-Dichloroethene 53 08/18/2010 10171065068-1311
cis-1,2-Dichloroethene 51 08/18/2010 10171035070-1221
1,1-Dichloroethene 54 08/18/2010 10171095069-1381
1,2-Dichloropropane 52 08/18/2010 10171045072-1241
cis-1,3-Dichloropropene 52 08/18/2010 10171055070-1261
trans-1,3-Dichloropropene 53 08/18/2010 10171075070-1241
Ethylbenzene 53 08/18/2010 10171055059-1281
2-Hexanone 98 08/18/2010 10179810054-1371
Isopropylbenzene 59 08/18/2010 10171185050-1361
Methyl acetate 55 08/18/2010 10171115059-1371
Methyl tertiary butyl ether (MTBE)54 08/18/2010 10171085072-1221
4-Methyl-2-pentanone 93 08/18/2010 10179310060-1341
Methylcyclohexane 62 08/18/2010 10171255041-1441
Methylene chloride 49 08/18/2010 1017985077-1291
Styrene 54 08/18/2010 10171085054-1361
1,1,2,2-Tetrachloroethane 51 08/18/2010 10171025069-1321
Tetrachloroethene 52 08/18/2010 10171035070-1301
Toluene 53 08/18/2010 10171065061-1291
1,1,2-Trichloro-1,2,2-Trifluoroethane 64 08/18/2010 10171295049-1361
1,2,4-Trichlorobenzene 53 08/18/2010 10171065034-1451
1,1,2-Trichloroethane 49 08/18/2010 1017985055-1281
1,1,1-Trichloroethane 56 08/18/2010 10171135063-1281
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 64 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:LQ40376-002
40376 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 52 08/18/2010 10171035062-1261
Trichlorofluoromethane 62 08/18/2010 10171235045-1381
Vinyl chloride 48 08/18/2010 1017975042-1321
Xylenes (total)110 08/18/2010 101710710058-1281
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 120 47-138
1,2-Dichloroethane-d4 98 53-142
Toluene-d8 116 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 65 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:LQ40376-003
40376 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Acetone 100 08/18/2010 092810510042-1495.2 201
Benzene 57 08/18/2010 09281135069-1237.2 201
Bromodichloromethane 57 08/18/2010 09281145069-1217.1 201
Bromoform 50 08/18/2010 0928995061-1191.5 201
Bromomethane (Methyl bromide)52 08/18/2010 09281045035-14412 201
2-Butanone (MEK)100 08/18/2010 092810010057-1482.6 201
Carbon disulfide 64 08/18/2010 0928N1295058-1227.8 201
Carbon tetrachloride 61 08/18/2010 09281225058-1367.3 201
Chlorobenzene 54 08/18/2010 09281085059-1296.6 201
Chloroethane 48 08/18/2010 0928975050-1329.8 201
Chloroform 58 08/18/2010 09281165071-12510 201
Chloromethane (Methyl chloride)55 08/18/2010 09281095034-1347.9 201
Cyclohexane 64 08/18/2010 09281285053-1397.7 201
1,2-Dibromo-3-chloropropane (DBCP)50 08/18/2010 09281015055-1252.1 201
Dibromochloromethane 52 08/18/2010 09281045066-1196.7 201
1,2-Dibromoethane (EDB)53 08/18/2010 09281075074-1246.7 201
1,2-Dichlorobenzene 55 08/18/2010 09281105057-1319.2 201
1,3-Dichlorobenzene 56 08/18/2010 09281135051-1347.4 201
1,4-Dichlorobenzene 56 08/18/2010 09281125052-1338.4 201
Dichlorodifluoromethane 99 08/18/2010 0928N1995010-1579.7 201
1,1-Dichloroethane 59 08/18/2010 09281185071-1279.0 201
1,2-Dichloroethane 54 08/18/2010 09281095067-1297.5 201
trans-1,2-Dichloroethene 58 08/18/2010 09281155068-1318.5 201
cis-1,2-Dichloroethene 56 08/18/2010 09281135070-1229.3 201
1,1-Dichloroethene 60 08/18/2010 09281205069-1389.5 201
1,2-Dichloropropane 57 08/18/2010 09281145072-1249.4 201
cis-1,3-Dichloropropene 57 08/18/2010 09281145070-1268.6 201
trans-1,3-Dichloropropene 57 08/18/2010 09281145070-1246.2 201
Ethylbenzene 57 08/18/2010 09281135059-1287.4 201
2-Hexanone 98 08/18/2010 09289810054-1370.28 201
Isopropylbenzene 67 08/18/2010 09281345050-13613 201
Methyl acetate 59 08/18/2010 09281195059-1376.7 201
Methyl tertiary butyl ether (MTBE)58 08/18/2010 09281175072-1227.5 201
4-Methyl-2-pentanone 96 08/18/2010 09289610060-1342.3 201
Methylcyclohexane 66 08/18/2010 09281325041-1445.6 201
Methylene chloride 54 08/18/2010 09281085077-12910 201
Styrene 59 08/18/2010 09281175054-1368.2 201
1,1,2,2-Tetrachloroethane 55 08/18/2010 09281105069-1327.8 201
Tetrachloroethene 55 08/18/2010 09281105070-1306.2 201
Toluene 57 08/18/2010 09281135061-1296.9 201
1,1,2-Trichloro-1,2,2-Trifluoroethane 70 08/18/2010 0928N1395049-1367.6 201
1,2,4-Trichlorobenzene 54 08/18/2010 09281075034-1450.63 201
1,1,2-Trichloroethane 53 08/18/2010 09281055055-1287.4 201
1,1,1-Trichloroethane 61 08/18/2010 09281235063-1288.7 201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 66 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:LQ40376-003
40376 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Trichloroethene 55 08/18/2010 09281095062-1266.0 201
Trichlorofluoromethane 67 08/18/2010 09281345045-1388.1 201
Vinyl chloride 54 08/18/2010 09281085042-13211 201
Xylenes (total)110 08/18/2010 092811410058-1286.9 201
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 115 47-138
1,2-Dichloroethane-d4 94 53-142
Toluene-d8 114 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 67 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:LQ40410-001
40410 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL Units Analysis DateDil
Acetone ND 08/19/2010 134220ug/kg1
Benzene ND 08/19/2010 13425.0 ug/kg1
Bromodichloromethane ND 08/19/2010 13425.0 ug/kg1
Bromoform ND 08/19/2010 13425.0 ug/kg1
Bromomethane (Methyl bromide)ND 08/19/2010 13425.0 ug/kg1
2-Butanone (MEK)ND 08/19/2010 134210ug/kg1
Carbon disulfide ND 08/19/2010 13425.0 ug/kg1
Carbon tetrachloride ND 08/19/2010 13425.0 ug/kg1
Chlorobenzene ND 08/19/2010 13425.0 ug/kg1
Chloroethane ND 08/19/2010 13425.0 ug/kg1
Chloroform ND 08/19/2010 13425.0 ug/kg1
Chloromethane (Methyl chloride)ND 08/19/2010 13425.0 ug/kg1
Cyclohexane ND 08/19/2010 13425.0 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 08/19/2010 13425.0 ug/kg1
Dibromochloromethane ND 08/19/2010 13425.0 ug/kg1
1,2-Dibromoethane (EDB)ND 08/19/2010 13425.0 ug/kg1
1,4-Dichlorobenzene ND 08/19/2010 13425.0 ug/kg1
1,3-Dichlorobenzene ND 08/19/2010 13425.0 ug/kg1
1,2-Dichlorobenzene ND 08/19/2010 13425.0 ug/kg1
Dichlorodifluoromethane ND 08/19/2010 13425.0 ug/kg1
1,2-Dichloroethane ND 08/19/2010 13425.0 ug/kg1
1,1-Dichloroethane ND 08/19/2010 13425.0 ug/kg1
trans-1,2-Dichloroethene ND 08/19/2010 13425.0 ug/kg1
cis-1,2-Dichloroethene ND 08/19/2010 13425.0 ug/kg1
1,1-Dichloroethene ND 08/19/2010 13425.0 ug/kg1
1,2-Dichloropropane ND 08/19/2010 13425.0 ug/kg1
trans-1,3-Dichloropropene ND 08/19/2010 13425.0 ug/kg1
cis-1,3-Dichloropropene ND 08/19/2010 13425.0 ug/kg1
Ethylbenzene ND 08/19/2010 13425.0 ug/kg1
2-Hexanone ND 08/19/2010 134210ug/kg1
Isopropylbenzene ND 08/19/2010 13425.0 ug/kg1
Methyl acetate ND 08/19/2010 13425.0 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 08/19/2010 13425.0 ug/kg1
4-Methyl-2-pentanone ND 08/19/2010 134210ug/kg1
Methylcyclohexane ND 08/19/2010 13425.0 ug/kg1
Methylene chloride ND 08/19/2010 13425.0 ug/kg1
Styrene ND 08/19/2010 13425.0 ug/kg1
1,1,2,2-Tetrachloroethane ND 08/19/2010 13425.0 ug/kg1
Tetrachloroethene ND 08/19/2010 13425.0 ug/kg1
Toluene ND 08/19/2010 13425.0 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 08/19/2010 13425.0 ug/kg1
1,2,4-Trichlorobenzene ND 08/19/2010 13425.0 ug/kg1
1,1,2-Trichloroethane ND 08/19/2010 13425.0 ug/kg1
1,1,1-Trichloroethane ND 08/19/2010 13425.0 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 68 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:LQ40410-001
40410 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL Units Analysis DateDil
Trichloroethene ND 08/19/2010 13425.0 ug/kg1
Trichlorofluoromethane ND 08/19/2010 13425.0 ug/kg1
Vinyl chloride ND 08/19/2010 13425.0 ug/kg1
Xylenes (total)ND 08/19/2010 13425.0 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 109 47-138
1,2-Dichloroethane-d4 93 53-142
Toluene-d8 113 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 69 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:LQ40410-002
40410 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 110 08/19/2010 120711110042-1491
Benzene 54 08/19/2010 12071075069-1231
Bromodichloromethane 54 08/19/2010 12071095069-1211
Bromoform 49 08/19/2010 1207985061-1191
Bromomethane (Methyl bromide)60 08/19/2010 12071205035-1441
2-Butanone (MEK)100 08/19/2010 120710110057-1481
Carbon disulfide 65 08/19/2010 1207N1295058-1221
Carbon tetrachloride 58 08/19/2010 12071165058-1361
Chlorobenzene 52 08/19/2010 12071045059-1291
Chloroethane 57 08/19/2010 12071155050-1321
Chloroform 53 08/19/2010 12071075071-1251
Chloromethane (Methyl chloride)67 08/19/2010 12071345034-1341
Cyclohexane 59 08/19/2010 12071195053-1391
1,2-Dibromo-3-chloropropane (DBCP)45 08/19/2010 1207895055-1251
Dibromochloromethane 51 08/19/2010 12071015066-1191
1,2-Dibromoethane (EDB)51 08/19/2010 12071025074-1241
1,4-Dichlorobenzene 52 08/19/2010 12071055052-1331
1,3-Dichlorobenzene 52 08/19/2010 12071055051-1341
1,2-Dichlorobenzene 51 08/19/2010 12071015057-1311
Dichlorodifluoromethane 77 08/19/2010 12071545010-1571
1,2-Dichloroethane 49 08/19/2010 1207985067-1291
1,1-Dichloroethane 53 08/19/2010 12071065071-1271
trans-1,2-Dichloroethene 55 08/19/2010 12071105068-1311
cis-1,2-Dichloroethene 52 08/19/2010 12071055070-1221
1,1-Dichloroethene 57 08/19/2010 12071145069-1381
1,2-Dichloropropane 52 08/19/2010 12071055072-1241
trans-1,3-Dichloropropene 52 08/19/2010 12071045070-1241
cis-1,3-Dichloropropene 53 08/19/2010 12071055070-1261
Ethylbenzene 55 08/19/2010 12071105059-1281
2-Hexanone 100 08/19/2010 120710210054-1371
Isopropylbenzene 61 08/19/2010 12071215050-1361
Methyl acetate 51 08/19/2010 12071025059-1371
Methyl tertiary butyl ether (MTBE)52 08/19/2010 12071045072-1221
4-Methyl-2-pentanone 97 08/19/2010 12079710060-1341
Methylcyclohexane 63 08/19/2010 12071265041-1441
Methylene chloride 51 08/19/2010 12071025077-1291
Styrene 55 08/19/2010 12071115054-1361
1,1,2,2-Tetrachloroethane 50 08/19/2010 12071005069-1321
Tetrachloroethene 55 08/19/2010 12071105070-1301
Toluene 55 08/19/2010 12071105061-1291
1,1,2-Trichloro-1,2,2-Trifluoroethane 78 08/19/2010 1207N1565049-1361
1,2,4-Trichlorobenzene 51 08/19/2010 12071015034-1451
1,1,2-Trichloroethane 50 08/19/2010 12071005055-1281
1,1,1-Trichloroethane 57 08/19/2010 12071135063-1281
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 70 of 76
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:LQ40410-002
40410 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 54 08/19/2010 12071075062-1261
Trichlorofluoromethane 65 08/19/2010 12071305045-1381
Vinyl chloride 69 08/19/2010 1207N1385042-1321
Xylenes (total)110 08/19/2010 120711110058-1281
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 119 47-138
1,2-Dichloroethane-d4 91 53-142
Toluene-d8 114 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
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Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:LQ40410-003
40410 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Acetone 110 08/19/2010 123111110042-1490.020 201
Benzene 54 08/19/2010 12311095069-1231.4 201
Bromodichloromethane 55 08/19/2010 12311115069-1211.6 201
Bromoform 49 08/19/2010 1231995061-1190.44 201
Bromomethane (Methyl bromide)60 08/19/2010 12311205035-1440.43 201
2-Butanone (MEK)100 08/19/2010 123110210057-1481.5 201
Carbon disulfide 63 08/19/2010 1231N1275058-1222.0 201
Carbon tetrachloride 58 08/19/2010 12311165058-1360.038 201
Chlorobenzene 52 08/19/2010 12311035059-1290.087 201
Chloroethane 55 08/19/2010 12311105050-1324.1 201
Chloroform 55 08/19/2010 12311095071-1252.4 201
Chloromethane (Methyl chloride)68 08/19/2010 1231N1355034-1341.3 201
Cyclohexane 60 08/19/2010 12311205053-1390.95 201
1,2-Dibromo-3-chloropropane (DBCP)47 08/19/2010 1231955055-1256.2 201
Dibromochloromethane 51 08/19/2010 12311015066-1190.069 201
1,2-Dibromoethane (EDB)50 08/19/2010 12311005074-1242.2 201
1,4-Dichlorobenzene 51 08/19/2010 12311035052-1331.9 201
1,3-Dichlorobenzene 52 08/19/2010 12311045051-1341.2 201
1,2-Dichlorobenzene 51 08/19/2010 12311015057-1310.21 201
Dichlorodifluoromethane 76 08/19/2010 12311525010-1571.7 201
1,2-Dichloroethane 51 08/19/2010 12311035067-1294.5 201
1,1-Dichloroethane 54 08/19/2010 12311085071-1272.5 201
trans-1,2-Dichloroethene 55 08/19/2010 12311105068-1310.23 201
cis-1,2-Dichloroethene 54 08/19/2010 12311085070-1222.9 201
1,1-Dichloroethene 56 08/19/2010 12311125069-1381.4 201
1,2-Dichloropropane 54 08/19/2010 12311075072-1242.5 201
trans-1,3-Dichloropropene 53 08/19/2010 12311055070-1241.1 201
cis-1,3-Dichloropropene 54 08/19/2010 12311095070-1263.1 201
Ethylbenzene 54 08/19/2010 12311085059-1281.3 201
2-Hexanone 100 08/19/2010 123110410054-1371.4 201
Isopropylbenzene 59 08/19/2010 12311175050-1363.5 201
Methyl acetate 54 08/19/2010 12311085059-1376.2 201
Methyl tertiary butyl ether (MTBE)54 08/19/2010 12311085072-1224.1 201
4-Methyl-2-pentanone 100 08/19/2010 123110110060-1343.2 201
Methylcyclohexane 62 08/19/2010 12311245041-1441.3 201
Methylene chloride 51 08/19/2010 12311025077-1290.029 201
Styrene 55 08/19/2010 12311115054-1360.031 201
1,1,2,2-Tetrachloroethane 50 08/19/2010 1231995069-1320.44 201
Tetrachloroethene 53 08/19/2010 12311065070-1303.3 201
Toluene 56 08/19/2010 12311115061-1290.93 201
1,1,2-Trichloro-1,2,2-Trifluoroethane 77 08/19/2010 1231N1545049-1361.7 201
1,2,4-Trichlorobenzene 52 08/19/2010 12311035034-1452.1 201
1,1,2-Trichloroethane 49 08/19/2010 1231995055-1281.5 201
1,1,1-Trichloroethane 57 08/19/2010 12311145063-1280.79 201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:LQ40410-003
40410 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Trichloroethene 55 08/19/2010 12311095062-1262.0 201
Trichlorofluoromethane 59 08/19/2010 12311185045-1389.3 201
Vinyl chloride 68 08/19/2010 1231N1355042-1322.4 201
Xylenes (total)110 08/19/2010 123110910058-1282.5 201
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 118 47-138
1,2-Dichloroethane-d4 93 53-142
Toluene-d8 114 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
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Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:LQ40511-001
40511 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL Units Analysis DateDil
Acetone ND 08/20/2010 092320ug/kg1
2-Butanone (MEK)ND 08/20/2010 092310ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 109 47-138
1,2-Dichloroethane-d4 82 53-142
Toluene-d8 99 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
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Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:LQ40511-002
40511 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 84 08/20/2010 08368410042-1491
2-Butanone (MEK)78 08/20/2010 08367810057-1481
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 117 47-138
1,2-Dichloroethane-d4 83 53-142
Toluene-d8 103 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:LQ40511-003
40511 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Acetone 94 08/20/2010 08599410042-14911 201
2-Butanone (MEK)95 08/20/2010 08599510057-14820 201
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 119 47-138
1,2-Dichloroethane-d4 84 53-142
Toluene-d8 105 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 76 of 76
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Appendix C
Laboratory Analytical Data
Sheets – Groundwater Samples
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
ERM-Southeast, Inc
8000 Corporate Center Drive
Suite 200
Charlotte, NC 28226
Attention: Michael Pressley
LG12017Lot Number:
0118084Project Number:
Beazer PropertyProject Name:
07/19/2010Date Completed:
Nisreen Saikaly
Project Manager
*LG12017*
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
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Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
ERM-Southeast, Inc
Lot Number: LG12017
SC DHEC No: 32010 NC DEHNR No: 329 NELAC No: E87653
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
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Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
ERM-Southeast, Inc
Lot Number: LG12017
Sample Number Sample ID Matrix Date Sampled Date Received
001 07/09/2010 1215B-1 Aqueous 07/12/2010
002 07/09/2010 1255B-2 Aqueous 07/12/2010
003 07/08/2010 1450B-3 Aqueous 07/12/2010
004 07/08/2010 1700B-4 Aqueous 07/12/2010
005 07/09/2010 1240B-5 Aqueous 07/12/2010
006 07/09/2010 1405B-6 Aqueous 07/12/2010
007 07/12/2010 0948Trip Blank Aqueous 07/12/2010
(7 samples)
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
ERM-Southeast, Inc
Lot Number: LG12017
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 B-1 Aqueous Chloroform 8260B 1.5 ug/L 5
001 B-1 Aqueous cis-1,2-Dichloroethene 8260B 26 ug/L 5
001 B-1 Aqueous Toluene 8260B 1.6 ug/L 5
001 B-1 Aqueous Trichloroethene 8260B 120 ug/L 6
002 B-2 Aqueous Chloromethane (Methyl chloride)8260B 4.7 ug/L 7
002 B-2 Aqueous trans-1,2-Dichloroethene 8260B 4.1 ug/L 7
002 B-2 Aqueous cis-1,2-Dichloroethene 8260B 86 ug/L 7
002 B-2 Aqueous Toluene 8260B 3.8 ug/L 7
002 B-2 Aqueous Trichloroethene 8260B 470 ug/L 8
003 B-3 Aqueous Chloroform 8260B 1.7 ug/L 9
003 B-3 Aqueous cis-1,2-Dichloroethene 8260B 11 ug/L 9
003 B-3 Aqueous Trichloroethene 8260B 68 ug/L 10
004 B-4 Aqueous Trichloroethene 8260B 1.7 ug/L 12
(13 detections)
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-1
LG12017-001
07/09/2010 1215
07/12/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 07/14/2010 1746 AAE 37682
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/L20
Benzene 71-43-2 8260B ND 1ug/L1.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L1.0
Bromoform 75-25-2 8260B ND 1ug/L1.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L2.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L10
Carbon disulfide 75-15-0 8260B ND 1ug/L1.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L1.0
Chlorobenzene 108-90-7 8260B ND 1ug/L1.0
Chloroethane 75-00-3 8260B ND 1ug/L2.0
Chloroform 67-66-3 8260B 1.5 1ug/L1.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L1.0
Cyclohexane 110-82-7 8260B ND 1ug/L1.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L1.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L1.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L1.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L1.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L1.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L1.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L2.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L1.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L1.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L1.0
cis-1,2-Dichloroethene 156-59-2 8260B 26 1ug/L1.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L1.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L1.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L1.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L1.0
Ethylbenzene 100-41-4 8260B ND 1ug/L1.0
2-Hexanone 591-78-6 8260B ND 1ug/L10
Isopropylbenzene 98-82-8 8260B ND 1ug/L1.0
Methyl acetate 79-20-9 8260B ND 1ug/L1.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L1.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10
Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0
Methylene chloride 75-09-2 8260B ND 1ug/L1.0
Styrene 100-42-5 8260B ND 1ug/L1.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L1.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L1.0
Toluene 108-88-3 8260B 1.6 1ug/L1.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L1.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L1.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L1.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L1.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-1
LG12017-001
07/09/2010 1215
07/12/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 07/14/2010 1746 AAE 37682
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B 120 1ug/L1.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L1.0
Vinyl chloride 75-01-4 8260B ND 1ug/L1.0
Xylenes (total)1330-20-7 8260B ND 1ug/L1.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 95 70-130
Bromofluorobenzene 96 70-130
Toluene-d8 98 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-2
LG12017-002
07/09/2010 1255
07/12/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 2 07/14/2010 1701 AAE 37682
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/L40
Benzene 71-43-2 8260B ND 1ug/L2.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L2.0
Bromoform 75-25-2 8260B ND 1ug/L2.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L4.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L20
Carbon disulfide 75-15-0 8260B ND 1ug/L2.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L2.0
Chlorobenzene 108-90-7 8260B ND 1ug/L2.0
Chloroethane 75-00-3 8260B ND 1ug/L4.0
Chloroform 67-66-3 8260B ND 1ug/L2.0
Chloromethane (Methyl chloride)74-87-3 8260B 4.7 1ug/L2.0
Cyclohexane 110-82-7 8260B ND 1ug/L2.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L2.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L2.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L2.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L2.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L2.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L2.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L4.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L2.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L2.0
trans-1,2-Dichloroethene 156-60-5 8260B 4.1 1ug/L2.0
cis-1,2-Dichloroethene 156-59-2 8260B 86 1ug/L2.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L2.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L2.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L2.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L2.0
Ethylbenzene 100-41-4 8260B ND 1ug/L2.0
2-Hexanone 591-78-6 8260B ND 1ug/L20
Isopropylbenzene 98-82-8 8260B ND 1ug/L2.0
Methyl acetate 79-20-9 8260B ND 1ug/L2.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L2.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L20
Methylcyclohexane 108-87-2 8260B ND 1ug/L10
Methylene chloride 75-09-2 8260B ND 1ug/L2.0
Styrene 100-42-5 8260B ND 1ug/L2.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L2.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L2.0
Toluene 108-88-3 8260B 3.8 1ug/L2.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L2.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L2.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L2.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L2.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-2
LG12017-002
07/09/2010 1255
07/12/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 2 07/14/2010 1701 AAE 37682
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B 470 1ug/L2.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L2.0
Vinyl chloride 75-01-4 8260B ND 1ug/L2.0
Xylenes (total)1330-20-7 8260B ND 1ug/L2.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 95 70-130
Bromofluorobenzene 95 70-130
Toluene-d8 98 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 8 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-3
LG12017-003
07/08/2010 1450
07/12/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 07/14/2010 1251 AAE 37682
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/L20
Benzene 71-43-2 8260B ND 1ug/L1.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L1.0
Bromoform 75-25-2 8260B ND 1ug/L1.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L2.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L10
Carbon disulfide 75-15-0 8260B ND 1ug/L1.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L1.0
Chlorobenzene 108-90-7 8260B ND 1ug/L1.0
Chloroethane 75-00-3 8260B ND 1ug/L2.0
Chloroform 67-66-3 8260B 1.7 1ug/L1.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L1.0
Cyclohexane 110-82-7 8260B ND 1ug/L1.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L1.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L1.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L1.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L1.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L1.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L1.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L2.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L1.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L1.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L1.0
cis-1,2-Dichloroethene 156-59-2 8260B 11 1ug/L1.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L1.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L1.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L1.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L1.0
Ethylbenzene 100-41-4 8260B ND 1ug/L1.0
2-Hexanone 591-78-6 8260B ND 1ug/L10
Isopropylbenzene 98-82-8 8260B ND 1ug/L1.0
Methyl acetate 79-20-9 8260B ND 1ug/L1.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L1.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10
Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0
Methylene chloride 75-09-2 8260B ND 1ug/L1.0
Styrene 100-42-5 8260B ND 1ug/L1.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L1.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L1.0
Toluene 108-88-3 8260B ND 1ug/L1.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L1.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L1.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L1.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L1.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 9 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-3
LG12017-003
07/08/2010 1450
07/12/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 07/14/2010 1251 AAE 37682
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B 68 1ug/L1.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L1.0
Vinyl chloride 75-01-4 8260B ND 1ug/L1.0
Xylenes (total)1330-20-7 8260B ND 1ug/L1.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 95 70-130
Bromofluorobenzene 96 70-130
Toluene-d8 98 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 10 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-4
LG12017-004
07/08/2010 1700
07/12/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 07/14/2010 1313 AAE 37682
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/L20
Benzene 71-43-2 8260B ND 1ug/L1.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L1.0
Bromoform 75-25-2 8260B ND 1ug/L1.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L2.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L10
Carbon disulfide 75-15-0 8260B ND 1ug/L1.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L1.0
Chlorobenzene 108-90-7 8260B ND 1ug/L1.0
Chloroethane 75-00-3 8260B ND 1ug/L2.0
Chloroform 67-66-3 8260B ND 1ug/L1.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L1.0
Cyclohexane 110-82-7 8260B ND 1ug/L1.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L1.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L1.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L1.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L1.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L1.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L1.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L2.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L1.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L1.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L1.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L1.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L1.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L1.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L1.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L1.0
Ethylbenzene 100-41-4 8260B ND 1ug/L1.0
2-Hexanone 591-78-6 8260B ND 1ug/L10
Isopropylbenzene 98-82-8 8260B ND 1ug/L1.0
Methyl acetate 79-20-9 8260B ND 1ug/L1.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L1.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10
Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0
Methylene chloride 75-09-2 8260B ND 1ug/L1.0
Styrene 100-42-5 8260B ND 1ug/L1.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L1.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L1.0
Toluene 108-88-3 8260B ND 1ug/L1.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L1.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L1.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L1.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L1.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 11 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-4
LG12017-004
07/08/2010 1700
07/12/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 07/14/2010 1313 AAE 37682
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B 1.7 1ug/L1.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L1.0
Vinyl chloride 75-01-4 8260B ND 1ug/L1.0
Xylenes (total)1330-20-7 8260B ND 1ug/L1.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 96 70-130
Bromofluorobenzene 96 70-130
Toluene-d8 97 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 12 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-5
LG12017-005
07/09/2010 1240
07/12/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 07/14/2010 1336 AAE 37682
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/L20
Benzene 71-43-2 8260B ND 1ug/L1.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L1.0
Bromoform 75-25-2 8260B ND 1ug/L1.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L2.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L10
Carbon disulfide 75-15-0 8260B ND 1ug/L1.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L1.0
Chlorobenzene 108-90-7 8260B ND 1ug/L1.0
Chloroethane 75-00-3 8260B ND 1ug/L2.0
Chloroform 67-66-3 8260B ND 1ug/L1.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L1.0
Cyclohexane 110-82-7 8260B ND 1ug/L1.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L1.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L1.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L1.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L1.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L1.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L1.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L2.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L1.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L1.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L1.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L1.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L1.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L1.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L1.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L1.0
Ethylbenzene 100-41-4 8260B ND 1ug/L1.0
2-Hexanone 591-78-6 8260B ND 1ug/L10
Isopropylbenzene 98-82-8 8260B ND 1ug/L1.0
Methyl acetate 79-20-9 8260B ND 1ug/L1.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L1.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10
Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0
Methylene chloride 75-09-2 8260B ND 1ug/L1.0
Styrene 100-42-5 8260B ND 1ug/L1.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L1.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L1.0
Toluene 108-88-3 8260B ND 1ug/L1.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L1.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L1.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L1.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L1.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 13 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-5
LG12017-005
07/09/2010 1240
07/12/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 07/14/2010 1336 AAE 37682
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/L1.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L1.0
Vinyl chloride 75-01-4 8260B ND 1ug/L1.0
Xylenes (total)1330-20-7 8260B ND 1ug/L1.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 95 70-130
Bromofluorobenzene 94 70-130
Toluene-d8 98 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 14 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-6
LG12017-006
07/09/2010 1405
07/12/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 07/14/2010 1358 AAE 37682
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/L20
Benzene 71-43-2 8260B ND 1ug/L1.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L1.0
Bromoform 75-25-2 8260B ND 1ug/L1.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L2.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L10
Carbon disulfide 75-15-0 8260B ND 1ug/L1.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L1.0
Chlorobenzene 108-90-7 8260B ND 1ug/L1.0
Chloroethane 75-00-3 8260B ND 1ug/L2.0
Chloroform 67-66-3 8260B ND 1ug/L1.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L1.0
Cyclohexane 110-82-7 8260B ND 1ug/L1.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L1.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L1.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L1.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L1.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L1.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L1.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L2.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L1.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L1.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L1.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L1.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L1.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L1.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L1.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L1.0
Ethylbenzene 100-41-4 8260B ND 1ug/L1.0
2-Hexanone 591-78-6 8260B ND 1ug/L10
Isopropylbenzene 98-82-8 8260B ND 1ug/L1.0
Methyl acetate 79-20-9 8260B ND 1ug/L1.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L1.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10
Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0
Methylene chloride 75-09-2 8260B ND 1ug/L1.0
Styrene 100-42-5 8260B ND 1ug/L1.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L1.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L1.0
Toluene 108-88-3 8260B ND 1ug/L1.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L1.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L1.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L1.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L1.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 15 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-6
LG12017-006
07/09/2010 1405
07/12/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 07/14/2010 1358 AAE 37682
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/L1.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L1.0
Vinyl chloride 75-01-4 8260B ND 1ug/L1.0
Xylenes (total)1330-20-7 8260B ND 1ug/L1.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 97 70-130
Bromofluorobenzene 94 70-130
Toluene-d8 98 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 16 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
Trip Blank
LG12017-007
07/12/2010 0948
07/12/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 07/14/2010 1421 AAE 37682
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/L20
Benzene 71-43-2 8260B ND 1ug/L1.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L1.0
Bromoform 75-25-2 8260B ND 1ug/L1.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L2.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L10
Carbon disulfide 75-15-0 8260B ND 1ug/L1.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L1.0
Chlorobenzene 108-90-7 8260B ND 1ug/L1.0
Chloroethane 75-00-3 8260B ND 1ug/L2.0
Chloroform 67-66-3 8260B ND 1ug/L1.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L1.0
Cyclohexane 110-82-7 8260B ND 1ug/L1.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L1.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L1.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L1.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L1.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L1.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L1.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L2.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L1.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L1.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L1.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L1.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L1.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L1.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L1.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L1.0
Ethylbenzene 100-41-4 8260B ND 1ug/L1.0
2-Hexanone 591-78-6 8260B ND 1ug/L10
Isopropylbenzene 98-82-8 8260B ND 1ug/L1.0
Methyl acetate 79-20-9 8260B ND 1ug/L1.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L1.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10
Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0
Methylene chloride 75-09-2 8260B ND 1ug/L1.0
Styrene 100-42-5 8260B ND 1ug/L1.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L1.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L1.0
Toluene 108-88-3 8260B ND 1ug/L1.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L1.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L1.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L1.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L1.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 17 of 18
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
Trip Blank
LG12017-007
07/12/2010 0948
07/12/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 07/14/2010 1421 AAE 37682
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/L1.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L1.0
Vinyl chloride 75-01-4 8260B ND 1ug/L1.0
Xylenes (total)1330-20-7 8260B ND 1ug/L1.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 94 70-130
Bromofluorobenzene 95 70-130
Toluene-d8 97 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 18 of 18
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
ERM-Southeast, Inc
8000 Corporate Center Drive
Suite 200
Charlotte, NC 28226
Attention: Michael Pressley
LH20038Lot Number:
0118084Project Number:
Beazer PropertyProject Name:
08/23/2010Date Completed:
Nisreen Saikaly
Project Manager
*LH20038*
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
ERM-Southeast, Inc
Lot Number: LH20038
SC DHEC No: 32010 NC DEHNR No: 329 NELAC No: E87653
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
ERM-Southeast, Inc
Lot Number: LH20038
Sample Number Sample ID Matrix Date Sampled Date Received
001 08/19/2010 1220B-7 Aqueous 08/20/2010
002 08/19/2010 1335B-8 Aqueous 08/20/2010
003 08/19/2010 1055B-9 Aqueous 08/20/2010
004 08/20/2010 1555Trip Blank Aqueous 08/20/2010
(4 samples)
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
ERM-Southeast, Inc
Lot Number: LH20038
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 B-7 Aqueous Chloroform 8260B 7.1 ug/L 5
001 B-7 Aqueous cis-1,2-Dichloroethene 8260B 34 ug/L 5
001 B-7 Aqueous Tetrachloroethene 8260B 1.9 ug/L 5
001 B-7 Aqueous Trichloroethene 8260B 340 ug/L 6
001 B-7 Aqueous Aluminum 6010C 1.1 mg/L 7
001 B-7 Aqueous Barium 6010C 0.062 mg/L 7
001 B-7 Aqueous Calcium 6010C 24 mg/L 7
001 B-7 Aqueous Chromium 6010C 0.019 mg/L 7
001 B-7 Aqueous Copper 6010C 0.014 mg/L 7
001 B-7 Aqueous Iron 6010C 1.3 mg/L 7
001 B-7 Aqueous Magnesium 6010C 12 mg/L 7
001 B-7 Aqueous Manganese 6010C 0.53 mg/L 7
001 B-7 Aqueous Sodium 6010C 18 mg/L 7
001 B-7 Aqueous Mercury 7470A 0.00013 mg/L 8
002 B-8 Aqueous Chloroform 8260B 1.3 ug/L 9
002 B-8 Aqueous trans-1,2-Dichloroethene 8260B 2.0 ug/L 9
002 B-8 Aqueous cis-1,2-Dichloroethene 8260B 57 ug/L 9
002 B-8 Aqueous Tetrachloroethene 8260B 2.0 ug/L 9
002 B-8 Aqueous Trichloroethene 8260B 410 ug/L 10
002 B-8 Aqueous Aluminum 6010C 1.6 mg/L 11
002 B-8 Aqueous Barium 6010C 0.044 mg/L 11
002 B-8 Aqueous Calcium 6010C 46 mg/L 11
002 B-8 Aqueous Chromium 6010C 0.014 mg/L 11
002 B-8 Aqueous Copper 6010C 0.011 mg/L 11
002 B-8 Aqueous Iron 6010C 1.3 mg/L 11
002 B-8 Aqueous Magnesium 6010C 16 mg/L 11
002 B-8 Aqueous Manganese 6010C 0.12 mg/L 11
002 B-8 Aqueous Sodium 6010C 16 mg/L 11
003 B-9 Aqueous Aluminum 6010C 0.23 mg/L 15
003 B-9 Aqueous Barium 6010C 0.055 mg/L 15
003 B-9 Aqueous Calcium 6010C 58 mg/L 15
003 B-9 Aqueous Chromium 6010C 0.062 mg/L 15
003 B-9 Aqueous Iron 6010C 0.34 mg/L 15
003 B-9 Aqueous Magnesium 6010C 19 mg/L 15
003 B-9 Aqueous Manganese 6010C 0.092 mg/L 15
003 B-9 Aqueous Sodium 6010C 18 mg/L 15
003 B-9 Aqueous Zinc 6010C 0.020 mg/L 15
003 B-9 Aqueous Mercury 7470A 0.00025 mg/L 16
(38 detections)
Page: 4 of 18
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-7
LH20038-001
08/19/2010 1220
08/20/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 08/22/2010 2112 DLB 40611
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/L20
Benzene 71-43-2 8260B ND 1ug/L1.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L1.0
Bromoform 75-25-2 8260B ND 1ug/L1.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L2.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L10
Carbon disulfide 75-15-0 8260B ND 1ug/L1.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L1.0
Chlorobenzene 108-90-7 8260B ND 1ug/L1.0
Chloroethane 75-00-3 8260B ND 1ug/L2.0
Chloroform 67-66-3 8260B 7.1 1ug/L1.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L1.0
Cyclohexane 110-82-7 8260B ND 1ug/L1.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L1.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L1.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L1.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L1.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L1.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L1.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L2.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L1.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L1.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L1.0
cis-1,2-Dichloroethene 156-59-2 8260B 34 1ug/L1.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L1.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L1.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L1.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L1.0
Ethylbenzene 100-41-4 8260B ND 1ug/L1.0
2-Hexanone 591-78-6 8260B ND 1ug/L10
Isopropylbenzene 98-82-8 8260B ND 1ug/L1.0
Methyl acetate 79-20-9 8260B ND 1ug/L1.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L1.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10
Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0
Methylene chloride 75-09-2 8260B ND 1ug/L1.0
Styrene 100-42-5 8260B ND 1ug/L1.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L1.0
Tetrachloroethene 127-18-4 8260B 1.9 1ug/L1.0
Toluene 108-88-3 8260B ND 1ug/L1.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L1.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L1.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L1.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L1.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 5 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-7
LH20038-001
08/19/2010 1220
08/20/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 08/22/2010 2112 DLB 40611
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B 340 1ug/L1.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L1.0
Vinyl chloride 75-01-4 8260B ND 1ug/L1.0
Xylenes (total)1330-20-7 8260B ND 1ug/L1.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 89 70-130
Bromofluorobenzene 86 70-130
Toluene-d8 87 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 6 of 18
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
ICP-AES
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-7
LH20038-001
08/19/2010 1220
08/20/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3030 C 6010C 1 08/21/2010 0041 CDF 08/20/2010 1840 40506
2 3030 C 6010C 1 08/23/2010 1321 CDF 08/20/2010 1840 40506
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Aluminum 7429-90-5 6010C 1.1 1mg/L0.20
Antimony 7440-36-0 6010C ND 1mg/L0.010
Arsenic 7440-38-2 6010C ND 1mg/L0.010
Barium 7440-39-3 6010C 0.062 1mg/L0.025
Beryllium 7440-41-7 6010C ND 1mg/L0.0040
Cadmium 7440-43-9 6010C ND 1mg/L0.0020
Calcium 7440-70-2 6010C 24 1mg/L5.0
Chromium 7440-47-3 6010C 0.019 1mg/L0.0050
Cobalt 7440-48-4 6010C ND 1mg/L0.025
Copper 7440-50-8 6010C 0.014 2mg/L0.0050
Iron 7439-89-6 6010C 1.3 1mg/L0.10
Lead 7439-92-1 6010C ND 2mg/L0.010
Magnesium 7439-95-4 6010C 12 1mg/L5.0
Manganese 7439-96-5 6010C 0.53 1mg/L0.015
Nickel 7440-02-0 6010C ND 1mg/L0.040
Potassium 7440-09-7 6010C ND 1mg/L5.0
Selenium 7782-49-2 6010C ND 1mg/L0.010
Silver 7440-22-4 6010C ND 1mg/L0.0050
Sodium 7440-23-5 6010C 18 1mg/L5.0
Thallium 7440-28-0 6010C ND 1mg/L0.050
Vanadium 7440-62-2 6010C ND 1mg/L0.050
Zinc 7440-66-6 6010C ND 1mg/L0.020
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-7
LH20038-001
08/19/2010 1220
08/20/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 08/20/2010 2323 BNW 08/20/2010 1948 40534
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury 7439-97-6 7470A 0.00013 1mg/L0.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 8 of 18
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-8
LH20038-002
08/19/2010 1335
08/20/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 08/22/2010 2134 DLB 40611
2 5030B 8260B 2 08/23/2010 1208 AAE 40645
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/L20
Benzene 71-43-2 8260B ND 1ug/L1.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L1.0
Bromoform 75-25-2 8260B ND 1ug/L1.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L2.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L10
Carbon disulfide 75-15-0 8260B ND 1ug/L1.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L1.0
Chlorobenzene 108-90-7 8260B ND 1ug/L1.0
Chloroethane 75-00-3 8260B ND 1ug/L2.0
Chloroform 67-66-3 8260B 1.3 1ug/L1.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L1.0
Cyclohexane 110-82-7 8260B ND 1ug/L1.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L1.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L1.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L1.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L1.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L1.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L1.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L2.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L1.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L1.0
trans-1,2-Dichloroethene 156-60-5 8260B 2.0 1ug/L1.0
cis-1,2-Dichloroethene 156-59-2 8260B 57 1ug/L1.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L1.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L1.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L1.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L1.0
Ethylbenzene 100-41-4 8260B ND 1ug/L1.0
2-Hexanone 591-78-6 8260B ND 1ug/L10
Isopropylbenzene 98-82-8 8260B ND 1ug/L1.0
Methyl acetate 79-20-9 8260B ND 1ug/L1.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L1.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10
Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0
Methylene chloride 75-09-2 8260B ND 1ug/L1.0
Styrene 100-42-5 8260B ND 1ug/L1.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L1.0
Tetrachloroethene 127-18-4 8260B 2.0 1ug/L1.0
Toluene 108-88-3 8260B ND 1ug/L1.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L1.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L1.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L1.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 9 of 18
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-8
LH20038-002
08/19/2010 1335
08/20/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 08/22/2010 2134 DLB 40611
2 5030B 8260B 2 08/23/2010 1208 AAE 40645
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L1.0
Trichloroethene 79-01-6 8260B 410 2ug/L2.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L1.0
Vinyl chloride 75-01-4 8260B ND 1ug/L1.0
Xylenes (total)1330-20-7 8260B ND 1ug/L1.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
1,2-Dichloroethane-d4 91 70-130 87 70-130
Bromofluorobenzene 88 70-130 82 70-130
Toluene-d8 90 70-130 85 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 10 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
ICP-AES
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-8
LH20038-002
08/19/2010 1335
08/20/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3030 C 6010C 1 08/21/2010 0045 CDF 08/20/2010 1840 40506
2 3030 C 6010C 1 08/23/2010 1326 CDF 08/20/2010 1840 40506
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Aluminum 7429-90-5 6010C 1.6 1mg/L0.20
Antimony 7440-36-0 6010C ND 1mg/L0.010
Arsenic 7440-38-2 6010C ND 1mg/L0.010
Barium 7440-39-3 6010C 0.044 1mg/L0.025
Beryllium 7440-41-7 6010C ND 1mg/L0.0040
Cadmium 7440-43-9 6010C ND 1mg/L0.0020
Calcium 7440-70-2 6010C 46 1mg/L5.0
Chromium 7440-47-3 6010C 0.014 2mg/L0.0050
Cobalt 7440-48-4 6010C ND 1mg/L0.025
Copper 7440-50-8 6010C 0.011 2mg/L0.0050
Iron 7439-89-6 6010C 1.3 1mg/L0.10
Lead 7439-92-1 6010C ND 2mg/L0.010
Magnesium 7439-95-4 6010C 16 1mg/L5.0
Manganese 7439-96-5 6010C 0.12 1mg/L0.015
Nickel 7440-02-0 6010C ND 1mg/L0.040
Potassium 7440-09-7 6010C ND 1mg/L5.0
Selenium 7782-49-2 6010C ND 1mg/L0.010
Silver 7440-22-4 6010C ND 1mg/L0.0050
Sodium 7440-23-5 6010C 16 1mg/L5.0
Thallium 7440-28-0 6010C ND 1mg/L0.050
Vanadium 7440-62-2 6010C ND 1mg/L0.050
Zinc 7440-66-6 6010C ND 1mg/L0.020
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 11 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-8
LH20038-002
08/19/2010 1335
08/20/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 08/20/2010 2325 BNW 08/20/2010 1948 40534
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury 7439-97-6 7470A ND 1mg/L0.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 12 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-9
LH20038-003
08/19/2010 1055
08/20/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 08/22/2010 2155 DLB 40611
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/L20
Benzene 71-43-2 8260B ND 1ug/L1.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L1.0
Bromoform 75-25-2 8260B ND 1ug/L1.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L2.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L10
Carbon disulfide 75-15-0 8260B ND 1ug/L1.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L1.0
Chlorobenzene 108-90-7 8260B ND 1ug/L1.0
Chloroethane 75-00-3 8260B ND 1ug/L2.0
Chloroform 67-66-3 8260B ND 1ug/L1.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L1.0
Cyclohexane 110-82-7 8260B ND 1ug/L1.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L1.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L1.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L1.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L1.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L1.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L1.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L2.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L1.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L1.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L1.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L1.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L1.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L1.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L1.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L1.0
Ethylbenzene 100-41-4 8260B ND 1ug/L1.0
2-Hexanone 591-78-6 8260B ND 1ug/L10
Isopropylbenzene 98-82-8 8260B ND 1ug/L1.0
Methyl acetate 79-20-9 8260B ND 1ug/L1.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L1.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10
Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0
Methylene chloride 75-09-2 8260B ND 1ug/L1.0
Styrene 100-42-5 8260B ND 1ug/L1.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L1.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L1.0
Toluene 108-88-3 8260B ND 1ug/L1.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L1.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L1.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L1.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L1.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 13 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-9
LH20038-003
08/19/2010 1055
08/20/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 08/22/2010 2155 DLB 40611
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/L1.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L1.0
Vinyl chloride 75-01-4 8260B ND 1ug/L1.0
Xylenes (total)1330-20-7 8260B ND 1ug/L1.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 91 70-130
Bromofluorobenzene 87 70-130
Toluene-d8 91 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 14 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
ICP-AES
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-9
LH20038-003
08/19/2010 1055
08/20/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3030 C 6010C 1 08/21/2010 0048 CDF 08/20/2010 1840 40506
2 3030 C 6010C 1 08/23/2010 1332 CDF 08/20/2010 1840 40506
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Aluminum 7429-90-5 6010C 0.23 1mg/L0.20
Antimony 7440-36-0 6010C ND 1mg/L0.010
Arsenic 7440-38-2 6010C ND 1mg/L0.010
Barium 7440-39-3 6010C 0.055 1mg/L0.025
Beryllium 7440-41-7 6010C ND 1mg/L0.0040
Cadmium 7440-43-9 6010C ND 1mg/L0.0020
Calcium 7440-70-2 6010C 58 1mg/L5.0
Chromium 7440-47-3 6010C 0.062 1mg/L0.0050
Cobalt 7440-48-4 6010C ND 1mg/L0.025
Copper 7440-50-8 6010C ND 2mg/L0.0050
Iron 7439-89-6 6010C 0.34 1mg/L0.10
Lead 7439-92-1 6010C ND 2mg/L0.010
Magnesium 7439-95-4 6010C 19 1mg/L5.0
Manganese 7439-96-5 6010C 0.092 1mg/L0.015
Nickel 7440-02-0 6010C ND 1mg/L0.040
Potassium 7440-09-7 6010C ND 1mg/L5.0
Selenium 7782-49-2 6010C ND 1mg/L0.010
Silver 7440-22-4 6010C ND 1mg/L0.0050
Sodium 7440-23-5 6010C 18 1mg/L5.0
Thallium 7440-28-0 6010C ND 1mg/L0.050
Vanadium 7440-62-2 6010C ND 1mg/L0.050
Zinc 7440-66-6 6010C 0.020 1mg/L0.020
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 15 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-9
LH20038-003
08/19/2010 1055
08/20/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 08/20/2010 2328 BNW 08/20/2010 1948 40534
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury 7439-97-6 7470A 0.00025 1mg/L0.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 16 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
Trip Blank
LH20038-004
08/20/2010 1555
08/20/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 08/22/2010 2050 DLB 40611
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/L20
Benzene 71-43-2 8260B ND 1ug/L1.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L1.0
Bromoform 75-25-2 8260B ND 1ug/L1.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L2.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L10
Carbon disulfide 75-15-0 8260B ND 1ug/L1.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L1.0
Chlorobenzene 108-90-7 8260B ND 1ug/L1.0
Chloroethane 75-00-3 8260B ND 1ug/L2.0
Chloroform 67-66-3 8260B ND 1ug/L1.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L1.0
Cyclohexane 110-82-7 8260B ND 1ug/L1.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L1.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L1.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L1.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L1.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L1.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L1.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L2.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L1.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L1.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L1.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L1.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L1.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L1.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L1.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L1.0
Ethylbenzene 100-41-4 8260B ND 1ug/L1.0
2-Hexanone 591-78-6 8260B ND 1ug/L10
Isopropylbenzene 98-82-8 8260B ND 1ug/L1.0
Methyl acetate 79-20-9 8260B ND 1ug/L1.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L1.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10
Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0
Methylene chloride 75-09-2 8260B ND 1ug/L1.0
Styrene 100-42-5 8260B ND 1ug/L1.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L1.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L1.0
Toluene 108-88-3 8260B ND 1ug/L1.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L1.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L1.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L1.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L1.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 17 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
Trip Blank
LH20038-004
08/20/2010 1555
08/20/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 08/22/2010 2050 DLB 40611
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/L1.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L1.0
Vinyl chloride 75-01-4 8260B ND 1ug/L1.0
Xylenes (total)1330-20-7 8260B ND 1ug/L1.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 92 70-130
Bromofluorobenzene 87 70-130
Toluene-d8 89 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 18 of 18
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1