HomeMy WebLinkAboutItem No 1 - Limited Phase II Environmental Site Assessment-OCR
ERM NC, PC
8000 Corporate Center Drive
Suite 200
Charlotte, NC 28226
(704) 541-8345
(704) 541-8416 (fax)
October 11, 2010
Mr. Max Justice
Clarkson Street, LLC
c/o Parker Poe Adams & Bernstein, LLP
Three Wachovia Center
401 S. Tryon Street
Suite 3000
Charlotte, North Carolina
Re: Limited Phase II Environmental Site Assessment - Addendum
18.56-Acre Beazer Property
Charlotte, North Carolina
Dear Mr. Justice:
ERM NC, PC (ERM) is pleased to present the results of the additional site
assessment work that was performed subsequent to the completion of
ERM’s Phase II Soil and Groundwater Assessment report (Phase II), dated
September 9, 2010. The subject property is an 18.56 acre property
(comprised of 10 parcels) located near uptown Charlotte, North Carolina
(see Figure 1).
BACKGROUND
The purpose of the Phase II ESA was to assess the subject property for
potential soil and groundwater impact associated with historical
automobile repair and maintenance facilities and historic manufacturing
uses of surrounding properties. Tetrachloroethene (PCE) was detected in
three soil borings at concentrations ranging from 22 micrograms per
kilogram (µg/kg) to 47 µg/kg. These concentrations exceed the North
Carolina Department of Environment and Natural Resources (NCDENR)
Inactive Hazardous Sites Branch (IHSB) Soil Remediation Goal for the
Protection of Groundwater of 5 µg/kg. In addition, groundwater
samples collected from nine temporary monitor wells installed on the
subject property in July and August 2010 detected trichloroethene (TCE)
at concentrations ranging from 1.7 micrograms per liter (µg/L) to 410
µg/L. The North Carolina Administrative Code (NCAC) 2L
Groundwater Standard (2L Standard) for TCE is 3 µg/L.
Mr. Max Justice
October 11, 2010
Page 2
Clarkson Street, LLC requested the installation of two additional
temporary monitor wells to further evaluate the lateral extent of TCE
impacted groundwater on the subject property in the vicinity of Parcel
Nos. 07314201 and 07325501.
PHASE II ADDENUM ACTIVITIES
Boring B-21 was drilled with air rotary drill rig due to anticipated
shallow bedrock at this location. Partially weather rock was encountered
at approximately seven feet below ground surface (bgs) and fractured
bedrock was encountered at approximately 15 feet bgs. B-21 was
advanced until groundwater was encountered at approximately 40 feet
bgs.
Boring B-22 was drilled with a Geoprobe® drill rig capable of advancing
hollow stem augers and air rotary equipment. Boring B-22 was located
on top of a soil stockpile that was approximately 20 feet above the
surrounding land surface. The boring was initially drilled with hollow
stem augers to minimize disturbance of the stockpile. The augers were
changed to air rotary at approximately 47 feet below the top of the
stockpile (27 feet bgs) as this depth was near the limit of auger
capabilities for the Geoprobe. The air rotary drill rods, equipped with a
4-inch button bit, were then advanced to approximately 57 feet below the
top of the stockpile (37 feet bgs), where groundwater was encountered.
Bedrock was not encountered during the advancement of B-22. Soil
types included mixtures of sand, silt, and clay. Soil cuttings generated
from B-21 and B-22 were placed in 55-gallon drums, sealed, and properly
labeled for temporary on-site storage. Figure 2 illustrates the locations of
B-21 and B-22 as well as previous temporary monitor wells installed
during Phase II activities.
Temporary monitor wells were constructed in both of the boreholes
using 2-inch inner diameter (I.D.) Schedule 40 PVC flush-threaded casing
and well screen. Ten feet of 0.010-inch slot well screen and a threaded
end cap were placed at the bottom of the borehole. The remainder of the
well was completed using solid PVC casing to a height of approximately
two feet above the ground surface. The annular space around the wells
was then filled with a washed and graded medium sand to a minimum
of two feet above the top of the screen. Lithologic description logs for B-
21 and B-22 are provided as an attachment to this report.
Once groundwater elevations stabilized in the wells, ERM utilized a
submersible pump to remove fines from the well casing and sand pack.
Mr. Max Justice
October 11, 2010
Page 3
Approximately 20 gallons of water were pumped from each well during
development activities. Development water from B-21 and B-22 was
containerized and left on-site in properly labeled and sealed in 55-gallon
drums.
Once the temporary wells were developed and allowed to recharge to the
initial depth to water measurement, ERM utilized new disposable
polyethylene bailers and twine to collect groundwater samples. The
samples were placed in laboratory-provided containers and packed in a
cooler with sufficient ice to maintain a temperature of 4º Celsius and sent
via courier to Shealy Environmental Services in West Columbia, South
Carolina for analysis using EPA Method 8260 for volatile organic
compounds (VOCs).
Once the temporary monitor wells were sampled, the drilling contractor
removed the PVC pipe from each borehole and abandoned the borings
with neat cement in accordance with state standards.
GROUNDWATER ANALTYICAL RESULTS
TCE was detected in B-21 at 2.3 µg/L, which is below the 2L Standard of 3
µg/L. No VOCs were detected in the B-22 sample. Based on these
results, the TCE plume is present in shallow groundwater on Parcel No.
07314201. Table 1 summarizes analytical results from B-21 and B-22 as
well as previous temporary monitor wells installed during Phase II
activities. The complete laboratory reports are included as an attachment
to this report.
ERM appreciates the opportunity to be of service on this important
project. Please contact us with any questions regarding the information
presented in this addendum report.
Sincerely,
Rick Tarravechia, P.G. Michael Pressley, P.G.
Principal in Charge Project Manager
Attachments: Figure 1 – Site Location Map
Figure 2 – Temporary Monitor Well Locations Map
Table 1 – Groundwater Analytical Results
Soil Boring Logs
Laboratory Analytical Data Sheets
ERM, NC PC 1SITE LOCATION MAP
SOURCE: CHARLOTTE EAST, NC 7.5 MINUTE TOPOGRAPHIC QUADRANGLE (1988)
SITE
Figure
Subject Property
18.56 ACRE BEAZER PROPERTY
CHARLOTTE, NORTH CAROLINA
Sa
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I
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Sample DateDepth to Water Below Ground Surface (feet)Chloroform Chloromethane cis-1,2-Dichloroethene trans-1,2-Dichloroethene Toluene Tetrachloroethene (PCE)Trichloroethene (TCE)Aluminum Barium Calcium Chromium Copper Iron Magnesium Manganese Sodium Zinc Mercury B-1 7-9-10 24.83
1
.
5
N
D
2
6
N
D
1
.
6
N
D
120 NA
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
B-2 7-9-10 26.00
N
D
4.7
8
6
4.1
3
.
8
N
D
470 NA
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
B-3 7-8-10 24.00
1
.
7
N
D
1
1
N
D
N
D
N
D
68 NA
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
B-4 7-8-10 24.25
N
D
N
D
N
D
N
D
N
D
N
D
1
.
7
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
B-5 7-9-10 15.50
N
D
N
D
N
D
N
D
N
D
N
D
N
D
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
B-6 7-9-10 27.58
N
D
N
D
N
D
N
D
N
D
N
D
N
D
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
B-7
8
-
1
9
-
1
0
1
6
.
6
5
7
.
1
N
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3
4
N
D
N
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1.9
3
4
0
1.1
0
.
6
2
2
4
0.019 0.014 1.3 12 0.53 18
N
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0
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0
0
0
1
3
B-8
8
-
1
9
-
1
0
1
4
.
0
0
1
.
3
N
D
5
7
2
N
D
2
4
1
0
1.6
0
.
0
4
4
6
0.014 0.011 1.3 16
0
.
1
2
1
6
N
D
N
D
B-9
8
-
1
9
-
1
0
1
1
.
7
0
N
D
N
D
N
D
N
D
N
D
N
D
N
D
0
.
2
3
0
.
0
6
5
8
0.062 ND 0.34 19
0
.
0
9
1
8
0
.
0
2
0
.
0
0
0
2
5
B-2
1
9
-
1
5
-
1
0
2
6
.
0
0
1
.
3
N
D
N
D
N
D
N
D
N
D
2
.
3
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
B-2
2
9
-
1
5
-
1
0
3
0
.
4
5
N
D
N
D
N
D
N
D
N
D
N
D
N
D
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
N
A
70
3
7
0
1
0
0
6
0
0
0
.
7
3
N
E
0
.
7
N
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0
.
0
1
1
0
.
3
N
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0
.
5
N
E
1
0
.
0
0
1
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Target Analyte List of Metals by EPA Method 6010C (mg/L)EPA Method 7470A (mg/L)
TABLE 1
GROUNDWATER SAMPLE ANALYTICAL RESULTS
18-ACRE BEAZER PROPERTY
CHARLOTTE, NORTH CAROLINA
Sample ID Sample Date
Depth to Water
Below Ground
Surface (feet)Ch
l
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Zi
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B-1 7-9-10 24.83 1.5 ND 26 ND 1.6 ND 120 NA NA NA NA NA NA NA NA NA NA NA
B-2 7-9-10 26.00 ND 4.7 86 4.1 3.8 ND 470 NA NA NA NA NA NA NA NA NA NA NA
B-3 7-8-10 24.00 1.7 ND 11 ND ND ND 68 NA NA NA NA NA NA NA NA NA NA NA
B-4 7-8-10 24.25 ND ND ND ND ND ND 1.7 NA NA NA NA NA NA NA NA NA NA NA
B-5 7-9-10 15.50 ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA
B-6 7-9-10 27.58 ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA
B-7 8-19-10 16.65 7.1 ND 34 ND ND 1.9 340 1.1 0.62 24 0.019 0.014 1.3 12 0.53 18 ND 0.00013
B-8 8-19-10 14.00 1.3 ND 57 2 ND 2 410 1.6 0.044 46 0.014 0.011 1.3 16 0.12 16 ND ND
B-9 8-19-10 11.70 ND ND ND ND ND ND ND 0.23 0.055 58 0.062 ND 0.34 19 0.092 18 0.02 0.00025
B-21 9-15-10 26.00 1.3 ND ND ND ND ND 2.3 NA NA NA NA NA NA NA NA NA NA NA
B-22 9-15-10 30.45 ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA
70 3 70 100 600 0.7 3 NE 0.7 NE 0.01 1 0.3 NE 0.5 NE 1 0.001
Notes:
BOLD values indicate an exceedence of 2L Groundwater Standards
NA = Not Analyzed
ND = Not Detected above minimum quantitation limits
NE = Not Established
ug/L = Micrograms/liter
Volatile Organic Compounds (VOCs) EPA
Method 8260B (ug/L)
NC 2L Groundwater Standard
Target Analyte List of Metals by EPA Method 6010C (mg/L)
EPA
Method
7470A
(mg/L)
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
64
60
56
52
48
44 Set temporary well at 41 ft bgs with 10 ft of well screen
Well pumped dry twice. Slow to moderate recharge.
40 Boring terminated at 41 feet due to water presence
36 30-40 feet, brown PWR, very moist.
32 Water level stabilized at 30.45 feet below grade
28
"Soft" zone encountered at 30 feet below grade
24
20
16 Bedrock encountered at 15 feet below grade. Brown-
grey dust blowing.
12
8
4 Brown, partially weathered rock at 7 ft
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
0-8 ft Tan, orange, black, white silty SAND, dry, no odor
MO
N
I
T
O
R
WE
L
L
DESCRIPTION
US
C
S
S
Y
M
B
O
L
ESTIMATED
PERCENT OF
LI
T
H
O
L
O
G
Y
DEPTH
(feet)
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
DPT M. Pressley
None 0 degrees N/AWATER LEVEL
NO. OF SAMPLES6" Button Bit 6.25 inches
Sandvik T25KW Air 41 1
Geologic Explorations Jerry 9/15/2010 9/15/2010
START DATE/TIME
B-21
18 acre Beazer Property 118084 Charlotte, NC
FIELD LOG OF BORING
BORING NUMBER
SHEET 1 OF 1
PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM
DRILLING COMPANY DRILLER COMPLETION DATE/TIME
DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES
SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER
DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS
SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE
TYPE DRIVING WT.DROP
GR SA FI
surface.
64 recharge. Well pumped dry once.
60
56
52
Set temporary well at 57 ft bgs with 10 ft of well screen
Water present within saprolite, slow to moderate
48 stockpile, or approximately 26 feet below ground
Boring terminated at 57 feet due to water presence
44 Water level stabilized at 46 feet below the top of the
40
36
32
28
24 moist, no odor.
20 20-57 feet Dark organish-brown sandy SILT. Slightly
16
12
8
4 Fill Material. 0-20 ft is part of a stockpile, above the
surrounding surface grade.
PI
D
R
E
A
D
I
N
G
S
(p
p
m
)
COMMENTS/
LAB SAMPLE
IDENTIFICATIONS
0-20 ft Orangish brown silty SAND with gravel,
MO
N
I
T
O
R
WE
L
L
DESCRIPTION
US
C
S
S
Y
M
B
O
L
ESTIMATED
PERCENT OF
LI
T
H
O
L
O
G
Y
DEPTH
(feet)
SA
M
P
L
E
S
RE
C
O
V
E
R
Y
%
DPT M. Pressley
None 0 degrees N/AWATER LEVEL
NO. OF SAMPLES4.25" Auger / 4" Button 6.25 inches
Geoprobe 7822DT 4.25" 'HSA/ 4" Button Bit 57 1
Geologic Explorations Johnny Burr 9/15/2010 9/15/2010
START DATE/TIME
B-22
18 acre Beazer Property 118084 Charlotte, NC
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
ERM-Southeast, Inc
8000 Corporate Center Drive
Suite 200
Charlotte, NC 28226
Attention: Michael Pressley
LI15066Lot Number:
0116961Project Number:
Beazer PropertyProject Name:
09/16/2010Date Completed:
Kelly M. Maberry
Project Manager
*LI15066*
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Page: 1 of 17
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
ERM-Southeast, Inc
Lot Number: LI15066
SC DHEC No: 32010 NC DEHNR No: 329 NELAC No: E87653
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Page: 2 of 17
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
ERM-Southeast, Inc
Lot Number: LI15066
Sample Number Sample ID Matrix Date Sampled Date Received
001 09/15/2010 1240B-21 Aqueous 09/15/2010
002 09/15/2010 1250B-22 Aqueous 09/15/2010
003 09/15/2010TRIP BLANK Aqueous 09/15/2010
(3 samples)
Page: 3 of 17
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
ERM-Southeast, Inc
Lot Number: LI15066
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 B-21 Aqueous Chloroform 8260B 1.3 ug/L 5
001 B-21 Aqueous Trichloroethene 8260B 2.3 ug/L 6
(2 detections)
Page: 4 of 17
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-21
LI15066-001
09/15/2010 1240
09/15/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/16/2010 1405 DLB 42492
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/L20
Benzene 71-43-2 8260B ND 1ug/L1.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L1.0
Bromoform 75-25-2 8260B ND 1ug/L1.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L2.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L10
Carbon disulfide 75-15-0 8260B ND 1ug/L1.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L1.0
Chlorobenzene 108-90-7 8260B ND 1ug/L1.0
Chloroethane 75-00-3 8260B ND 1ug/L2.0
Chloroform 67-66-3 8260B 1.3 1ug/L1.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L1.0
Cyclohexane 110-82-7 8260B ND 1ug/L1.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L1.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L1.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L1.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L1.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L1.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L1.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L2.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L1.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L1.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L1.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L1.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L1.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L1.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L1.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L1.0
Ethylbenzene 100-41-4 8260B ND 1ug/L1.0
2-Hexanone 591-78-6 8260B ND 1ug/L10
Isopropylbenzene 98-82-8 8260B ND 1ug/L1.0
Methyl acetate 79-20-9 8260B ND 1ug/L1.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L1.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10
Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0
Methylene chloride 75-09-2 8260B ND 1ug/L1.0
Styrene 100-42-5 8260B ND 1ug/L1.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L1.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L1.0
Toluene 108-88-3 8260B ND 1ug/L1.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L1.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L1.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L1.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L1.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 5 of 17
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-21
LI15066-001
09/15/2010 1240
09/15/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/16/2010 1405 DLB 42492
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B 2.3 1ug/L1.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L1.0
Vinyl chloride 75-01-4 8260B ND 1ug/L1.0
Xylenes (total)1330-20-7 8260B ND 1ug/L1.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 105 70-130
Bromofluorobenzene 101 70-130
Toluene-d8 98 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 6 of 17
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-22
LI15066-002
09/15/2010 1250
09/15/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/16/2010 1427 DLB 42492
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/L20
Benzene 71-43-2 8260B ND 1ug/L1.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L1.0
Bromoform 75-25-2 8260B ND 1ug/L1.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L2.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L10
Carbon disulfide 75-15-0 8260B ND 1ug/L1.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L1.0
Chlorobenzene 108-90-7 8260B ND 1ug/L1.0
Chloroethane 75-00-3 8260B ND 1ug/L2.0
Chloroform 67-66-3 8260B ND 1ug/L1.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L1.0
Cyclohexane 110-82-7 8260B ND 1ug/L1.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L1.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L1.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L1.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L1.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L1.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L1.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L2.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L1.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L1.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L1.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L1.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L1.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L1.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L1.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L1.0
Ethylbenzene 100-41-4 8260B ND 1ug/L1.0
2-Hexanone 591-78-6 8260B ND 1ug/L10
Isopropylbenzene 98-82-8 8260B ND 1ug/L1.0
Methyl acetate 79-20-9 8260B ND 1ug/L1.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L1.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10
Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0
Methylene chloride 75-09-2 8260B ND 1ug/L1.0
Styrene 100-42-5 8260B ND 1ug/L1.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L1.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L1.0
Toluene 108-88-3 8260B ND 1ug/L1.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L1.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L1.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L1.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L1.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 7 of 17
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
B-22
LI15066-002
09/15/2010 1250
09/15/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/16/2010 1427 DLB 42492
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/L1.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L1.0
Vinyl chloride 75-01-4 8260B ND 1ug/L1.0
Xylenes (total)1330-20-7 8260B ND 1ug/L1.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 105 70-130
Bromofluorobenzene 100 70-130
Toluene-d8 96 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 8 of 17
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
TRIP BLANK
LI15066-003
09/15/2010
09/15/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/16/2010 1448 DLB 42492
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B ND 1ug/L20
Benzene 71-43-2 8260B ND 1ug/L1.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L1.0
Bromoform 75-25-2 8260B ND 1ug/L1.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L2.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L10
Carbon disulfide 75-15-0 8260B ND 1ug/L1.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L1.0
Chlorobenzene 108-90-7 8260B ND 1ug/L1.0
Chloroethane 75-00-3 8260B ND 1ug/L2.0
Chloroform 67-66-3 8260B ND 1ug/L1.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L1.0
Cyclohexane 110-82-7 8260B ND 1ug/L1.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L1.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L1.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L1.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L1.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L1.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L1.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L2.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L1.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L1.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L1.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L1.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L1.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L1.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L1.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L1.0
Ethylbenzene 100-41-4 8260B ND 1ug/L1.0
2-Hexanone 591-78-6 8260B ND 1ug/L10
Isopropylbenzene 98-82-8 8260B ND 1ug/L1.0
Methyl acetate 79-20-9 8260B ND 1ug/L1.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L1.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10
Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0
Methylene chloride 75-09-2 8260B ND 1ug/L1.0
Styrene 100-42-5 8260B ND 1ug/L1.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L1.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L1.0
Toluene 108-88-3 8260B ND 1ug/L1.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L1.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L1.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L1.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L1.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 9 of 17
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
ERM-Southeast, Inc
TRIP BLANK
LI15066-003
09/15/2010
09/15/2010
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/16/2010 1448 DLB 42492
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Trichloroethene 79-01-6 8260B ND 1ug/L1.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L1.0
Vinyl chloride 75-01-4 8260B ND 1ug/L1.0
Xylenes (total)1330-20-7 8260B ND 1ug/L1.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 108 70-130
Bromofluorobenzene 98 70-130
Toluene-d8 98 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria
_
H = Out of holding time
Page: 10 of 17
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
QC Summary
Page: 11 of 17
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:LQ42492-001
42492 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Acetone ND 09/16/2010 103420ug/L1
Benzene ND 09/16/2010 10341.0 ug/L1
Bromodichloromethane ND 09/16/2010 10341.0 ug/L1
Bromoform ND 09/16/2010 10341.0 ug/L1
Bromomethane (Methyl bromide)ND 09/16/2010 10342.0 ug/L1
2-Butanone (MEK)ND 09/16/2010 103410ug/L1
Carbon disulfide ND 09/16/2010 10341.0 ug/L1
Carbon tetrachloride ND 09/16/2010 10341.0 ug/L1
Chlorobenzene ND 09/16/2010 10341.0 ug/L1
Chloroethane ND 09/16/2010 10342.0 ug/L1
Chloroform ND 09/16/2010 10341.0 ug/L1
Chloromethane (Methyl chloride)ND 09/16/2010 10341.0 ug/L1
Cyclohexane ND 09/16/2010 10341.0 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)ND 09/16/2010 10341.0 ug/L1
Dibromochloromethane ND 09/16/2010 10341.0 ug/L1
1,2-Dibromoethane (EDB)ND 09/16/2010 10341.0 ug/L1
1,4-Dichlorobenzene ND 09/16/2010 10341.0 ug/L1
1,2-Dichlorobenzene ND 09/16/2010 10341.0 ug/L1
1,3-Dichlorobenzene ND 09/16/2010 10341.0 ug/L1
Dichlorodifluoromethane ND 09/16/2010 10342.0 ug/L1
1,2-Dichloroethane ND 09/16/2010 10341.0 ug/L1
1,1-Dichloroethane ND 09/16/2010 10341.0 ug/L1
cis-1,2-Dichloroethene ND 09/16/2010 10341.0 ug/L1
trans-1,2-Dichloroethene ND 09/16/2010 10341.0 ug/L1
1,1-Dichloroethene ND 09/16/2010 10341.0 ug/L1
1,2-Dichloropropane ND 09/16/2010 10341.0 ug/L1
trans-1,3-Dichloropropene ND 09/16/2010 10341.0 ug/L1
cis-1,3-Dichloropropene ND 09/16/2010 10341.0 ug/L1
Ethylbenzene ND 09/16/2010 10341.0 ug/L1
2-Hexanone ND 09/16/2010 103410ug/L1
Isopropylbenzene ND 09/16/2010 10341.0 ug/L1
Methyl acetate ND 09/16/2010 10341.0 ug/L1
Methyl tertiary butyl ether (MTBE)ND 09/16/2010 10341.0 ug/L1
4-Methyl-2-pentanone ND 09/16/2010 103410ug/L1
Methylcyclohexane ND 09/16/2010 10345.0 ug/L1
Methylene chloride ND 09/16/2010 10341.0 ug/L1
Styrene ND 09/16/2010 10341.0 ug/L1
1,1,2,2-Tetrachloroethane ND 09/16/2010 10341.0 ug/L1
Tetrachloroethene ND 09/16/2010 10341.0 ug/L1
Toluene ND 09/16/2010 10341.0 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 09/16/2010 10341.0 ug/L1
1,2,4-Trichlorobenzene ND 09/16/2010 10341.0 ug/L1
1,1,2-Trichloroethane ND 09/16/2010 10341.0 ug/L1
1,1,1-Trichloroethane ND 09/16/2010 10341.0 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 12 of 17
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:LQ42492-001
42492 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Trichloroethene ND 09/16/2010 10341.0 ug/L1
Trichlorofluoromethane ND 09/16/2010 10341.0 ug/L1
Vinyl chloride ND 09/16/2010 10341.0 ug/L1
Xylenes (total)ND 09/16/2010 10341.0 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 99 70-130
1,2-Dichloroethane-d4 100 70-130
Toluene-d8 97 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 13 of 17
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:LQ42492-002
42492 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acetone 130 09/16/2010 090913010046-1531
Benzene 48 09/16/2010 0909975072-1271
Bromodichloromethane 51 09/16/2010 09091015071-1431
Bromoform 58 09/16/2010 09091175065-1311
Bromomethane (Methyl bromide)47 09/16/2010 0909945036-1681
2-Butanone (MEK)120 09/16/2010 090912310060-1401
Carbon disulfide 48 09/16/2010 0909955060-1401
Carbon tetrachloride 54 09/16/2010 09091075037-1661
Chlorobenzene 50 09/16/2010 0909995078-1291
Chloroethane 42 09/16/2010 0909845042-1631
Chloroform 49 09/16/2010 0909975063-1231
Chloromethane (Methyl chloride)35 09/16/2010 0909705020-1581
Cyclohexane 46 09/16/2010 0909925070-1301
1,2-Dibromo-3-chloropropane (DBCP)62 09/16/2010 09091255070-1301
Dibromochloromethane 58 09/16/2010 09091165074-1341
1,2-Dibromoethane (EDB)52 09/16/2010 09091055070-1301
1,4-Dichlorobenzene 49 09/16/2010 0909995070-1301
1,2-Dichlorobenzene 51 09/16/2010 09091035070-1301
1,3-Dichlorobenzene 51 09/16/2010 09091025070-1301
Dichlorodifluoromethane 30 09/16/2010 0909605010-1581
1,2-Dichloroethane 49 09/16/2010 0909975059-1431
1,1-Dichloroethane 48 09/16/2010 0909965069-1321
cis-1,2-Dichloroethene 50 09/16/2010 0909995070-1301
trans-1,2-Dichloroethene 49 09/16/2010 0909985067-1411
1,1-Dichloroethene 48 09/16/2010 0909965050-1321
1,2-Dichloropropane 47 09/16/2010 0909935071-1261
trans-1,3-Dichloropropene 50 09/16/2010 0909995073-1311
cis-1,3-Dichloropropene 52 09/16/2010 09091035069-1301
Ethylbenzene 53 09/16/2010 09091055079-1321
2-Hexanone 110 09/16/2010 090911510060-1401
Isopropylbenzene 56 09/16/2010 09091125070-1301
Methyl acetate 55 09/16/2010 09091105015-1281
Methyl tertiary butyl ether (MTBE)55 09/16/2010 09091095060-1401
4-Methyl-2-pentanone 110 09/16/2010 090911010060-1401
Methylcyclohexane 51 09/16/2010 09091025070-1301
Methylene chloride 45 09/16/2010 0909905069-1291
Styrene 52 09/16/2010 09091045070-1301
1,1,2,2-Tetrachloroethane 53 09/16/2010 09091055060-1551
Tetrachloroethene 51 09/16/2010 09091025070-1301
Toluene 50 09/16/2010 09091005075-1251
1,1,2-Trichloro-1,2,2-Trifluoroethane 49 09/16/2010 0909975070-1301
1,2,4-Trichlorobenzene 54 09/16/2010 09091075070-1301
1,1,2-Trichloroethane 50 09/16/2010 09091005077-1321
1,1,1-Trichloroethane 53 09/16/2010 09091055077-1321
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 14 of 17
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:LQ42492-002
42492 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Trichloroethene 49 09/16/2010 0909995073-1241
Trichlorofluoromethane 44 09/16/2010 0909885041-1731
Vinyl chloride 42 09/16/2010 0909835029-1591
Xylenes (total)110 09/16/2010 090910810070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 99 70-130
1,2-Dichloroethane-d4 97 70-130
Toluene-d8 96 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 15 of 17
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:LQ42492-003
42492 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Acetone 120 09/16/2010 093112110046-1536.7 201
Benzene 48 09/16/2010 0931975072-1270.16 201
Bromodichloromethane 51 09/16/2010 09311015071-1430.13 201
Bromoform 55 09/16/2010 09311115065-1315.4 201
Bromomethane (Methyl bromide)47 09/16/2010 0931935036-1681.2 201
2-Butanone (MEK)120 09/16/2010 093111610060-1406.3 201
Carbon disulfide 47 09/16/2010 0931955060-1400.61 201
Carbon tetrachloride 54 09/16/2010 09311075037-1660.0093 201
Chlorobenzene 50 09/16/2010 09311005078-1291.0 201
Chloroethane 43 09/16/2010 0931875042-1632.8 201
Chloroform 48 09/16/2010 0931975063-1230.25 201
Chloromethane (Methyl chloride)35 09/16/2010 0931705020-1580.50 201
Cyclohexane 46 09/16/2010 0931925070-1300.48 201
1,2-Dibromo-3-chloropropane (DBCP)56 09/16/2010 09311125070-13010 201
Dibromochloromethane 57 09/16/2010 09311145074-1341.1 201
1,2-Dibromoethane (EDB)52 09/16/2010 09311035070-1301.5 201
1,4-Dichlorobenzene 49 09/16/2010 0931995070-1300.039 201
1,2-Dichlorobenzene 51 09/16/2010 09311025070-1300.86 201
1,3-Dichlorobenzene 51 09/16/2010 09311015070-1300.47 201
Dichlorodifluoromethane 30 09/16/2010 0931615010-1582.1 201
1,2-Dichloroethane 48 09/16/2010 0931965059-1430.80 201
1,1-Dichloroethane 48 09/16/2010 0931965069-1320.46 201
cis-1,2-Dichloroethene 50 09/16/2010 09311005070-1300.10 201
trans-1,2-Dichloroethene 49 09/16/2010 0931995067-1410.23 201
1,1-Dichloroethene 49 09/16/2010 0931985050-1322.4 201
1,2-Dichloropropane 47 09/16/2010 0931955071-1261.7 201
trans-1,3-Dichloropropene 49 09/16/2010 0931995073-1310.17 201
cis-1,3-Dichloropropene 52 09/16/2010 09311045069-1300.52 201
Ethylbenzene 53 09/16/2010 09311055079-1320.23 201
2-Hexanone 110 09/16/2010 093110710060-1407.1 201
Isopropylbenzene 55 09/16/2010 09311115070-1300.58 201
Methyl acetate 52 09/16/2010 09311055015-1285.0 201
Methyl tertiary butyl ether (MTBE)54 09/16/2010 09311075060-1401.5 201
4-Methyl-2-pentanone 100 09/16/2010 093110310060-1407.0 201
Methylcyclohexane 52 09/16/2010 09311035070-1301.1 201
Methylene chloride 45 09/16/2010 0931905069-1290.17 201
Styrene 52 09/16/2010 09311045070-1300.061 201
1,1,2,2-Tetrachloroethane 51 09/16/2010 09311025060-1552.8 201
Tetrachloroethene 51 09/16/2010 09311035070-1300.76 201
Toluene 50 09/16/2010 09311015075-1250.26 201
1,1,2-Trichloro-1,2,2-Trifluoroethane 50 09/16/2010 0931995070-1302.1 201
1,2,4-Trichlorobenzene 54 09/16/2010 09311075070-1300.099 201
1,1,2-Trichloroethane 49 09/16/2010 0931995077-1321.5 201
1,1,1-Trichloroethane 53 09/16/2010 09311055077-1320.24 201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 16 of 17
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:LQ42492-003
42492 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Trichloroethene 49 09/16/2010 0931985073-1240.67 201
Trichlorofluoromethane 44 09/16/2010 0931885041-1730.38 201
Vinyl chloride 42 09/16/2010 0931845029-1590.89 201
Xylenes (total)110 09/16/2010 093110810070-1300.15 201
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 99 70-130
1,2-Dichloroethane-d4 95 70-130
Toluene-d8 96 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 17 of 17
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1