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HomeMy WebLinkAboutItem No 1 - Limited Phase II Environmental Site Assessment-OCR ERM NC, PC 8000 Corporate Center Drive Suite 200 Charlotte, NC 28226 (704) 541-8345 (704) 541-8416 (fax) October 11, 2010 Mr. Max Justice Clarkson Street, LLC c/o Parker Poe Adams & Bernstein, LLP Three Wachovia Center 401 S. Tryon Street Suite 3000 Charlotte, North Carolina Re: Limited Phase II Environmental Site Assessment - Addendum 18.56-Acre Beazer Property Charlotte, North Carolina Dear Mr. Justice: ERM NC, PC (ERM) is pleased to present the results of the additional site assessment work that was performed subsequent to the completion of ERM’s Phase II Soil and Groundwater Assessment report (Phase II), dated September 9, 2010. The subject property is an 18.56 acre property (comprised of 10 parcels) located near uptown Charlotte, North Carolina (see Figure 1). BACKGROUND The purpose of the Phase II ESA was to assess the subject property for potential soil and groundwater impact associated with historical automobile repair and maintenance facilities and historic manufacturing uses of surrounding properties. Tetrachloroethene (PCE) was detected in three soil borings at concentrations ranging from 22 micrograms per kilogram (µg/kg) to 47 µg/kg. These concentrations exceed the North Carolina Department of Environment and Natural Resources (NCDENR) Inactive Hazardous Sites Branch (IHSB) Soil Remediation Goal for the Protection of Groundwater of 5 µg/kg. In addition, groundwater samples collected from nine temporary monitor wells installed on the subject property in July and August 2010 detected trichloroethene (TCE) at concentrations ranging from 1.7 micrograms per liter (µg/L) to 410 µg/L. The North Carolina Administrative Code (NCAC) 2L Groundwater Standard (2L Standard) for TCE is 3 µg/L. Mr. Max Justice October 11, 2010 Page 2 Clarkson Street, LLC requested the installation of two additional temporary monitor wells to further evaluate the lateral extent of TCE impacted groundwater on the subject property in the vicinity of Parcel Nos. 07314201 and 07325501. PHASE II ADDENUM ACTIVITIES Boring B-21 was drilled with air rotary drill rig due to anticipated shallow bedrock at this location. Partially weather rock was encountered at approximately seven feet below ground surface (bgs) and fractured bedrock was encountered at approximately 15 feet bgs. B-21 was advanced until groundwater was encountered at approximately 40 feet bgs. Boring B-22 was drilled with a Geoprobe® drill rig capable of advancing hollow stem augers and air rotary equipment. Boring B-22 was located on top of a soil stockpile that was approximately 20 feet above the surrounding land surface. The boring was initially drilled with hollow stem augers to minimize disturbance of the stockpile. The augers were changed to air rotary at approximately 47 feet below the top of the stockpile (27 feet bgs) as this depth was near the limit of auger capabilities for the Geoprobe. The air rotary drill rods, equipped with a 4-inch button bit, were then advanced to approximately 57 feet below the top of the stockpile (37 feet bgs), where groundwater was encountered. Bedrock was not encountered during the advancement of B-22. Soil types included mixtures of sand, silt, and clay. Soil cuttings generated from B-21 and B-22 were placed in 55-gallon drums, sealed, and properly labeled for temporary on-site storage. Figure 2 illustrates the locations of B-21 and B-22 as well as previous temporary monitor wells installed during Phase II activities. Temporary monitor wells were constructed in both of the boreholes using 2-inch inner diameter (I.D.) Schedule 40 PVC flush-threaded casing and well screen. Ten feet of 0.010-inch slot well screen and a threaded end cap were placed at the bottom of the borehole. The remainder of the well was completed using solid PVC casing to a height of approximately two feet above the ground surface. The annular space around the wells was then filled with a washed and graded medium sand to a minimum of two feet above the top of the screen. Lithologic description logs for B- 21 and B-22 are provided as an attachment to this report. Once groundwater elevations stabilized in the wells, ERM utilized a submersible pump to remove fines from the well casing and sand pack. Mr. Max Justice October 11, 2010 Page 3 Approximately 20 gallons of water were pumped from each well during development activities. Development water from B-21 and B-22 was containerized and left on-site in properly labeled and sealed in 55-gallon drums. Once the temporary wells were developed and allowed to recharge to the initial depth to water measurement, ERM utilized new disposable polyethylene bailers and twine to collect groundwater samples. The samples were placed in laboratory-provided containers and packed in a cooler with sufficient ice to maintain a temperature of 4º Celsius and sent via courier to Shealy Environmental Services in West Columbia, South Carolina for analysis using EPA Method 8260 for volatile organic compounds (VOCs). Once the temporary monitor wells were sampled, the drilling contractor removed the PVC pipe from each borehole and abandoned the borings with neat cement in accordance with state standards. GROUNDWATER ANALTYICAL RESULTS TCE was detected in B-21 at 2.3 µg/L, which is below the 2L Standard of 3 µg/L. No VOCs were detected in the B-22 sample. Based on these results, the TCE plume is present in shallow groundwater on Parcel No. 07314201. Table 1 summarizes analytical results from B-21 and B-22 as well as previous temporary monitor wells installed during Phase II activities. The complete laboratory reports are included as an attachment to this report. ERM appreciates the opportunity to be of service on this important project. Please contact us with any questions regarding the information presented in this addendum report. Sincerely, Rick Tarravechia, P.G. Michael Pressley, P.G. Principal in Charge Project Manager Attachments: Figure 1 – Site Location Map Figure 2 – Temporary Monitor Well Locations Map Table 1 – Groundwater Analytical Results Soil Boring Logs Laboratory Analytical Data Sheets ERM, NC PC 1SITE LOCATION MAP SOURCE: CHARLOTTE EAST, NC 7.5 MINUTE TOPOGRAPHIC QUADRANGLE (1988) SITE Figure Subject Property 18.56 ACRE BEAZER PROPERTY CHARLOTTE, NORTH CAROLINA Sa m p l e I D Sample DateDepth to Water Below Ground Surface (feet)Chloroform Chloromethane cis-1,2-Dichloroethene trans-1,2-Dichloroethene Toluene Tetrachloroethene (PCE)Trichloroethene (TCE)Aluminum Barium Calcium Chromium Copper Iron Magnesium Manganese Sodium Zinc Mercury B-1 7-9-10 24.83 1 . 5 N D 2 6 N D 1 . 6 N D 120 NA N A N A N A N A N A N A N A N A N A N A B-2 7-9-10 26.00 N D 4.7 8 6 4.1 3 . 8 N D 470 NA N A N A N A N A N A N A N A N A N A N A B-3 7-8-10 24.00 1 . 7 N D 1 1 N D N D N D 68 NA N A N A N A N A N A N A N A N A N A N A B-4 7-8-10 24.25 N D N D N D N D N D N D 1 . 7 N A N A N A N A N A N A N A N A N A N A N A B-5 7-9-10 15.50 N D N D N D N D N D N D N D N A N A N A N A N A N A N A N A N A N A N A B-6 7-9-10 27.58 N D N D N D N D N D N D N D N A N A N A N A N A N A N A N A N A N A N A B-7 8 - 1 9 - 1 0 1 6 . 6 5 7 . 1 N D 3 4 N D N D 1.9 3 4 0 1.1 0 . 6 2 2 4 0.019 0.014 1.3 12 0.53 18 N D 0 . 0 0 0 1 3 B-8 8 - 1 9 - 1 0 1 4 . 0 0 1 . 3 N D 5 7 2 N D 2 4 1 0 1.6 0 . 0 4 4 6 0.014 0.011 1.3 16 0 . 1 2 1 6 N D N D B-9 8 - 1 9 - 1 0 1 1 . 7 0 N D N D N D N D N D N D N D 0 . 2 3 0 . 0 6 5 8 0.062 ND 0.34 19 0 . 0 9 1 8 0 . 0 2 0 . 0 0 0 2 5 B-2 1 9 - 1 5 - 1 0 2 6 . 0 0 1 . 3 N D N D N D N D N D 2 . 3 N A N A N A N A N A N A N A N A N A N A N A B-2 2 9 - 1 5 - 1 0 3 0 . 4 5 N D N D N D N D N D N D N D N A N A N A N A N A N A N A N A N A N A N A 70 3 7 0 1 0 0 6 0 0 0 . 7 3 N E 0 . 7 N E 0 . 0 1 1 0 . 3 N E 0 . 5 N E 1 0 . 0 0 1 No t e s : BO L D va l u e s i n d i c a t e a n e x c e e d e n c e o f 2 L G r o u n d w a t e r S t a n d a r d s NA = N o t A n a l y z e d ND = N o t D e t e c t e d a b o v e m i n i m u m q u a n t i t a t i o n l i m i t s NE = N o t E s t a b l i s h e d ug / L = M i c r o g r a m s / l i t e r Volatile Organic Compounds (VOCs) EPA Method 8260B (ug/L) NC 2 L G r o u n d w a t e r S t a n d a r d Target Analyte List of Metals by EPA Method 6010C (mg/L)EPA Method 7470A (mg/L) TABLE 1 GROUNDWATER SAMPLE ANALYTICAL RESULTS 18-ACRE BEAZER PROPERTY CHARLOTTE, NORTH CAROLINA Sample ID Sample Date Depth to Water Below Ground Surface (feet)Ch l o r o f o r m Ch l o r o m e t h a n e ci s - 1 , 2 - D i c h l o r o e t h e n e tr a n s - 1 , 2 - D i c h l o r o e t h e n e To l u e n e Te t r a c h l o r o e t h e n e ( P C E ) Tr i c h l o r o e t h e n e ( T C E ) Al u m i n u m Ba r i u m Ca l c i u m Ch r o m i u m Co p p e r Ir o n Ma g n e s i u m Ma n g a n e s e So d i u m Zi n c Me r c u r y B-1 7-9-10 24.83 1.5 ND 26 ND 1.6 ND 120 NA NA NA NA NA NA NA NA NA NA NA B-2 7-9-10 26.00 ND 4.7 86 4.1 3.8 ND 470 NA NA NA NA NA NA NA NA NA NA NA B-3 7-8-10 24.00 1.7 ND 11 ND ND ND 68 NA NA NA NA NA NA NA NA NA NA NA B-4 7-8-10 24.25 ND ND ND ND ND ND 1.7 NA NA NA NA NA NA NA NA NA NA NA B-5 7-9-10 15.50 ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA B-6 7-9-10 27.58 ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA B-7 8-19-10 16.65 7.1 ND 34 ND ND 1.9 340 1.1 0.62 24 0.019 0.014 1.3 12 0.53 18 ND 0.00013 B-8 8-19-10 14.00 1.3 ND 57 2 ND 2 410 1.6 0.044 46 0.014 0.011 1.3 16 0.12 16 ND ND B-9 8-19-10 11.70 ND ND ND ND ND ND ND 0.23 0.055 58 0.062 ND 0.34 19 0.092 18 0.02 0.00025 B-21 9-15-10 26.00 1.3 ND ND ND ND ND 2.3 NA NA NA NA NA NA NA NA NA NA NA B-22 9-15-10 30.45 ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA 70 3 70 100 600 0.7 3 NE 0.7 NE 0.01 1 0.3 NE 0.5 NE 1 0.001 Notes: BOLD values indicate an exceedence of 2L Groundwater Standards NA = Not Analyzed ND = Not Detected above minimum quantitation limits NE = Not Established ug/L = Micrograms/liter Volatile Organic Compounds (VOCs) EPA Method 8260B (ug/L) NC 2L Groundwater Standard Target Analyte List of Metals by EPA Method 6010C (mg/L) EPA Method 7470A (mg/L) FIELD LOG OF BORING BORING NUMBER SHEET 1 OF 1 PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM DRILLING COMPANY DRILLER COMPLETION DATE/TIME DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE TYPE DRIVING WT.DROP GR SA FI 64 60 56 52 48 44 Set temporary well at 41 ft bgs with 10 ft of well screen Well pumped dry twice. Slow to moderate recharge. 40 Boring terminated at 41 feet due to water presence 36 30-40 feet, brown PWR, very moist. 32 Water level stabilized at 30.45 feet below grade 28 "Soft" zone encountered at 30 feet below grade 24 20 16 Bedrock encountered at 15 feet below grade. Brown- grey dust blowing. 12 8 4 Brown, partially weathered rock at 7 ft PI D R E A D I N G S (p p m ) COMMENTS/ LAB SAMPLE IDENTIFICATIONS 0-8 ft Tan, orange, black, white silty SAND, dry, no odor MO N I T O R WE L L DESCRIPTION US C S S Y M B O L ESTIMATED PERCENT OF LI T H O L O G Y DEPTH (feet) SA M P L E S RE C O V E R Y % DPT M. Pressley None 0 degrees N/AWATER LEVEL NO. OF SAMPLES6" Button Bit 6.25 inches Sandvik T25KW Air 41 1 Geologic Explorations Jerry 9/15/2010 9/15/2010 START DATE/TIME B-21 18 acre Beazer Property 118084 Charlotte, NC FIELD LOG OF BORING BORING NUMBER SHEET 1 OF 1 PROJECT NAME PROJECT NUMBER LOCATION ELEVATION AND DATUM DRILLING COMPANY DRILLER COMPLETION DATE/TIME DRILLING EQUIPMENT DRILLING METHOD COMPLETION DEPTH TOTAL NO. OF SAMPLES SIZE AND TYPE OF BIT HOLE DIAMETER BULK SS DRIVE PITCHER DRILLING FLUID DRILLING ANGLE FIRST AFTER _____ HOURS SAMPLE HAMMER GEOLOGIST/DATE CHECKED BY/DATE TYPE DRIVING WT.DROP GR SA FI surface. 64 recharge. Well pumped dry once. 60 56 52 Set temporary well at 57 ft bgs with 10 ft of well screen Water present within saprolite, slow to moderate 48 stockpile, or approximately 26 feet below ground Boring terminated at 57 feet due to water presence 44 Water level stabilized at 46 feet below the top of the 40 36 32 28 24 moist, no odor. 20 20-57 feet Dark organish-brown sandy SILT. Slightly 16 12 8 4 Fill Material. 0-20 ft is part of a stockpile, above the surrounding surface grade. PI D R E A D I N G S (p p m ) COMMENTS/ LAB SAMPLE IDENTIFICATIONS 0-20 ft Orangish brown silty SAND with gravel, MO N I T O R WE L L DESCRIPTION US C S S Y M B O L ESTIMATED PERCENT OF LI T H O L O G Y DEPTH (feet) SA M P L E S RE C O V E R Y % DPT M. Pressley None 0 degrees N/AWATER LEVEL NO. OF SAMPLES4.25" Auger / 4" Button 6.25 inches Geoprobe 7822DT 4.25" 'HSA/ 4" Button Bit 57 1 Geologic Explorations Johnny Burr 9/15/2010 9/15/2010 START DATE/TIME B-22 18 acre Beazer Property 118084 Charlotte, NC SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis ERM-Southeast, Inc 8000 Corporate Center Drive Suite 200 Charlotte, NC 28226 Attention: Michael Pressley LI15066Lot Number: 0116961Project Number: Beazer PropertyProject Name: 09/16/2010Date Completed: Kelly M. Maberry Project Manager *LI15066* This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist. Page: 1 of 17 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Case Narrative ERM-Southeast, Inc Lot Number: LI15066 SC DHEC No: 32010 NC DEHNR No: 329 NELAC No: E87653 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Page: 2 of 17 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary ERM-Southeast, Inc Lot Number: LI15066 Sample Number Sample ID Matrix Date Sampled Date Received 001 09/15/2010 1240B-21 Aqueous 09/15/2010 002 09/15/2010 1250B-22 Aqueous 09/15/2010 003 09/15/2010TRIP BLANK Aqueous 09/15/2010 (3 samples) Page: 3 of 17 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Executive Summary ERM-Southeast, Inc Lot Number: LI15066 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 B-21 Aqueous Chloroform 8260B 1.3 ug/L 5 001 B-21 Aqueous Trichloroethene 8260B 2.3 ug/L 6 (2 detections) Page: 4 of 17 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: ERM-Southeast, Inc B-21 LI15066-001 09/15/2010 1240 09/15/2010 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 09/16/2010 1405 DLB 42492 AnalyticalCAS Parameter Number Method Result Q PQL Units Run Acetone 67-64-1 8260B ND 1ug/L20 Benzene 71-43-2 8260B ND 1ug/L1.0 Bromodichloromethane 75-27-4 8260B ND 1ug/L1.0 Bromoform 75-25-2 8260B ND 1ug/L1.0 Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L2.0 2-Butanone (MEK)78-93-3 8260B ND 1ug/L10 Carbon disulfide 75-15-0 8260B ND 1ug/L1.0 Carbon tetrachloride 56-23-5 8260B ND 1ug/L1.0 Chlorobenzene 108-90-7 8260B ND 1ug/L1.0 Chloroethane 75-00-3 8260B ND 1ug/L2.0 Chloroform 67-66-3 8260B 1.3 1ug/L1.0 Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L1.0 Cyclohexane 110-82-7 8260B ND 1ug/L1.0 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L1.0 Dibromochloromethane 124-48-1 8260B ND 1ug/L1.0 1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L1.0 1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L1.0 1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L1.0 1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L1.0 Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L2.0 1,2-Dichloroethane 107-06-2 8260B ND 1ug/L1.0 1,1-Dichloroethane 75-34-3 8260B ND 1ug/L1.0 trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L1.0 cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L1.0 1,1-Dichloroethene 75-35-4 8260B ND 1ug/L1.0 1,2-Dichloropropane 78-87-5 8260B ND 1ug/L1.0 trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L1.0 cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L1.0 Ethylbenzene 100-41-4 8260B ND 1ug/L1.0 2-Hexanone 591-78-6 8260B ND 1ug/L10 Isopropylbenzene 98-82-8 8260B ND 1ug/L1.0 Methyl acetate 79-20-9 8260B ND 1ug/L1.0 Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L1.0 4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10 Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0 Methylene chloride 75-09-2 8260B ND 1ug/L1.0 Styrene 100-42-5 8260B ND 1ug/L1.0 1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L1.0 Tetrachloroethene 127-18-4 8260B ND 1ug/L1.0 Toluene 108-88-3 8260B ND 1ug/L1.0 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L1.0 1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L1.0 1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L1.0 1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L1.0 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria _ H = Out of holding time Page: 5 of 17 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: ERM-Southeast, Inc B-21 LI15066-001 09/15/2010 1240 09/15/2010 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 09/16/2010 1405 DLB 42492 AnalyticalCAS Parameter Number Method Result Q PQL Units Run Trichloroethene 79-01-6 8260B 2.3 1ug/L1.0 Trichlorofluoromethane 75-69-4 8260B ND 1ug/L1.0 Vinyl chloride 75-01-4 8260B ND 1ug/L1.0 Xylenes (total)1330-20-7 8260B ND 1ug/L1.0 AcceptanceRun 1 Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 105 70-130 Bromofluorobenzene 101 70-130 Toluene-d8 98 70-130 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria _ H = Out of holding time Page: 6 of 17 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: ERM-Southeast, Inc B-22 LI15066-002 09/15/2010 1250 09/15/2010 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 09/16/2010 1427 DLB 42492 AnalyticalCAS Parameter Number Method Result Q PQL Units Run Acetone 67-64-1 8260B ND 1ug/L20 Benzene 71-43-2 8260B ND 1ug/L1.0 Bromodichloromethane 75-27-4 8260B ND 1ug/L1.0 Bromoform 75-25-2 8260B ND 1ug/L1.0 Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L2.0 2-Butanone (MEK)78-93-3 8260B ND 1ug/L10 Carbon disulfide 75-15-0 8260B ND 1ug/L1.0 Carbon tetrachloride 56-23-5 8260B ND 1ug/L1.0 Chlorobenzene 108-90-7 8260B ND 1ug/L1.0 Chloroethane 75-00-3 8260B ND 1ug/L2.0 Chloroform 67-66-3 8260B ND 1ug/L1.0 Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L1.0 Cyclohexane 110-82-7 8260B ND 1ug/L1.0 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L1.0 Dibromochloromethane 124-48-1 8260B ND 1ug/L1.0 1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L1.0 1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L1.0 1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L1.0 1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L1.0 Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L2.0 1,2-Dichloroethane 107-06-2 8260B ND 1ug/L1.0 1,1-Dichloroethane 75-34-3 8260B ND 1ug/L1.0 trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L1.0 cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L1.0 1,1-Dichloroethene 75-35-4 8260B ND 1ug/L1.0 1,2-Dichloropropane 78-87-5 8260B ND 1ug/L1.0 trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L1.0 cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L1.0 Ethylbenzene 100-41-4 8260B ND 1ug/L1.0 2-Hexanone 591-78-6 8260B ND 1ug/L10 Isopropylbenzene 98-82-8 8260B ND 1ug/L1.0 Methyl acetate 79-20-9 8260B ND 1ug/L1.0 Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L1.0 4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10 Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0 Methylene chloride 75-09-2 8260B ND 1ug/L1.0 Styrene 100-42-5 8260B ND 1ug/L1.0 1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L1.0 Tetrachloroethene 127-18-4 8260B ND 1ug/L1.0 Toluene 108-88-3 8260B ND 1ug/L1.0 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L1.0 1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L1.0 1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L1.0 1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L1.0 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria _ H = Out of holding time Page: 7 of 17 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: ERM-Southeast, Inc B-22 LI15066-002 09/15/2010 1250 09/15/2010 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 09/16/2010 1427 DLB 42492 AnalyticalCAS Parameter Number Method Result Q PQL Units Run Trichloroethene 79-01-6 8260B ND 1ug/L1.0 Trichlorofluoromethane 75-69-4 8260B ND 1ug/L1.0 Vinyl chloride 75-01-4 8260B ND 1ug/L1.0 Xylenes (total)1330-20-7 8260B ND 1ug/L1.0 AcceptanceRun 1 Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 105 70-130 Bromofluorobenzene 100 70-130 Toluene-d8 96 70-130 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria _ H = Out of holding time Page: 8 of 17 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: ERM-Southeast, Inc TRIP BLANK LI15066-003 09/15/2010 09/15/2010 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 09/16/2010 1448 DLB 42492 AnalyticalCAS Parameter Number Method Result Q PQL Units Run Acetone 67-64-1 8260B ND 1ug/L20 Benzene 71-43-2 8260B ND 1ug/L1.0 Bromodichloromethane 75-27-4 8260B ND 1ug/L1.0 Bromoform 75-25-2 8260B ND 1ug/L1.0 Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L2.0 2-Butanone (MEK)78-93-3 8260B ND 1ug/L10 Carbon disulfide 75-15-0 8260B ND 1ug/L1.0 Carbon tetrachloride 56-23-5 8260B ND 1ug/L1.0 Chlorobenzene 108-90-7 8260B ND 1ug/L1.0 Chloroethane 75-00-3 8260B ND 1ug/L2.0 Chloroform 67-66-3 8260B ND 1ug/L1.0 Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L1.0 Cyclohexane 110-82-7 8260B ND 1ug/L1.0 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L1.0 Dibromochloromethane 124-48-1 8260B ND 1ug/L1.0 1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L1.0 1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L1.0 1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L1.0 1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L1.0 Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L2.0 1,2-Dichloroethane 107-06-2 8260B ND 1ug/L1.0 1,1-Dichloroethane 75-34-3 8260B ND 1ug/L1.0 trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L1.0 cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L1.0 1,1-Dichloroethene 75-35-4 8260B ND 1ug/L1.0 1,2-Dichloropropane 78-87-5 8260B ND 1ug/L1.0 trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L1.0 cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L1.0 Ethylbenzene 100-41-4 8260B ND 1ug/L1.0 2-Hexanone 591-78-6 8260B ND 1ug/L10 Isopropylbenzene 98-82-8 8260B ND 1ug/L1.0 Methyl acetate 79-20-9 8260B ND 1ug/L1.0 Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L1.0 4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10 Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0 Methylene chloride 75-09-2 8260B ND 1ug/L1.0 Styrene 100-42-5 8260B ND 1ug/L1.0 1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L1.0 Tetrachloroethene 127-18-4 8260B ND 1ug/L1.0 Toluene 108-88-3 8260B ND 1ug/L1.0 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L1.0 1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L1.0 1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L1.0 1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L1.0 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria _ H = Out of holding time Page: 9 of 17 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: ERM-Southeast, Inc TRIP BLANK LI15066-003 09/15/2010 09/15/2010 Aqueous Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B 1 09/16/2010 1448 DLB 42492 AnalyticalCAS Parameter Number Method Result Q PQL Units Run Trichloroethene 79-01-6 8260B ND 1ug/L1.0 Trichlorofluoromethane 75-69-4 8260B ND 1ug/L1.0 Vinyl chloride 75-01-4 8260B ND 1ug/L1.0 Xylenes (total)1330-20-7 8260B ND 1ug/L1.0 AcceptanceRun 1 Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 108 70-130 Bromofluorobenzene 98 70-130 Toluene-d8 98 70-130 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"N = Recovery is out of criteria _ H = Out of holding time Page: 10 of 17 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 QC Summary Page: 11 of 17 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS - MB Batch:Prep Method: Sample ID:LQ42492-001 42492 5030B Analytical Method:8260B Matrix:Aqueous Parameter Result Q PQL Units Analysis DateDil Acetone ND 09/16/2010 103420ug/L1 Benzene ND 09/16/2010 10341.0 ug/L1 Bromodichloromethane ND 09/16/2010 10341.0 ug/L1 Bromoform ND 09/16/2010 10341.0 ug/L1 Bromomethane (Methyl bromide)ND 09/16/2010 10342.0 ug/L1 2-Butanone (MEK)ND 09/16/2010 103410ug/L1 Carbon disulfide ND 09/16/2010 10341.0 ug/L1 Carbon tetrachloride ND 09/16/2010 10341.0 ug/L1 Chlorobenzene ND 09/16/2010 10341.0 ug/L1 Chloroethane ND 09/16/2010 10342.0 ug/L1 Chloroform ND 09/16/2010 10341.0 ug/L1 Chloromethane (Methyl chloride)ND 09/16/2010 10341.0 ug/L1 Cyclohexane ND 09/16/2010 10341.0 ug/L1 1,2-Dibromo-3-chloropropane (DBCP)ND 09/16/2010 10341.0 ug/L1 Dibromochloromethane ND 09/16/2010 10341.0 ug/L1 1,2-Dibromoethane (EDB)ND 09/16/2010 10341.0 ug/L1 1,4-Dichlorobenzene ND 09/16/2010 10341.0 ug/L1 1,2-Dichlorobenzene ND 09/16/2010 10341.0 ug/L1 1,3-Dichlorobenzene ND 09/16/2010 10341.0 ug/L1 Dichlorodifluoromethane ND 09/16/2010 10342.0 ug/L1 1,2-Dichloroethane ND 09/16/2010 10341.0 ug/L1 1,1-Dichloroethane ND 09/16/2010 10341.0 ug/L1 cis-1,2-Dichloroethene ND 09/16/2010 10341.0 ug/L1 trans-1,2-Dichloroethene ND 09/16/2010 10341.0 ug/L1 1,1-Dichloroethene ND 09/16/2010 10341.0 ug/L1 1,2-Dichloropropane ND 09/16/2010 10341.0 ug/L1 trans-1,3-Dichloropropene ND 09/16/2010 10341.0 ug/L1 cis-1,3-Dichloropropene ND 09/16/2010 10341.0 ug/L1 Ethylbenzene ND 09/16/2010 10341.0 ug/L1 2-Hexanone ND 09/16/2010 103410ug/L1 Isopropylbenzene ND 09/16/2010 10341.0 ug/L1 Methyl acetate ND 09/16/2010 10341.0 ug/L1 Methyl tertiary butyl ether (MTBE)ND 09/16/2010 10341.0 ug/L1 4-Methyl-2-pentanone ND 09/16/2010 103410ug/L1 Methylcyclohexane ND 09/16/2010 10345.0 ug/L1 Methylene chloride ND 09/16/2010 10341.0 ug/L1 Styrene ND 09/16/2010 10341.0 ug/L1 1,1,2,2-Tetrachloroethane ND 09/16/2010 10341.0 ug/L1 Tetrachloroethene ND 09/16/2010 10341.0 ug/L1 Toluene ND 09/16/2010 10341.0 ug/L1 1,1,2-Trichloro-1,2,2-Trifluoroethane ND 09/16/2010 10341.0 ug/L1 1,2,4-Trichlorobenzene ND 09/16/2010 10341.0 ug/L1 1,1,2-Trichloroethane ND 09/16/2010 10341.0 ug/L1 1,1,1-Trichloroethane ND 09/16/2010 10341.0 ug/L1 Note:Calculations are performed before rounding to avoid round-off errors in calculated results PQL = Practical quantitation limit ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" J = Estimated result < PQL and > MDL N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + - RPD is out of criteria_ Page: 12 of 17 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS - MB Batch:Prep Method: Sample ID:LQ42492-001 42492 5030B Analytical Method:8260B Matrix:Aqueous Parameter Result Q PQL Units Analysis DateDil Trichloroethene ND 09/16/2010 10341.0 ug/L1 Trichlorofluoromethane ND 09/16/2010 10341.0 ug/L1 Vinyl chloride ND 09/16/2010 10341.0 ug/L1 Xylenes (total)ND 09/16/2010 10341.0 ug/L1 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 99 70-130 1,2-Dichloroethane-d4 100 70-130 Toluene-d8 97 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results PQL = Practical quantitation limit ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" J = Estimated result < PQL and > MDL N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + - RPD is out of criteria_ Page: 13 of 17 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS - LCS Batch:Prep Method: Sample ID:LQ42492-002 42492 5030B Analytical Method:8260B Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/L)(ug/L) Acetone 130 09/16/2010 090913010046-1531 Benzene 48 09/16/2010 0909975072-1271 Bromodichloromethane 51 09/16/2010 09091015071-1431 Bromoform 58 09/16/2010 09091175065-1311 Bromomethane (Methyl bromide)47 09/16/2010 0909945036-1681 2-Butanone (MEK)120 09/16/2010 090912310060-1401 Carbon disulfide 48 09/16/2010 0909955060-1401 Carbon tetrachloride 54 09/16/2010 09091075037-1661 Chlorobenzene 50 09/16/2010 0909995078-1291 Chloroethane 42 09/16/2010 0909845042-1631 Chloroform 49 09/16/2010 0909975063-1231 Chloromethane (Methyl chloride)35 09/16/2010 0909705020-1581 Cyclohexane 46 09/16/2010 0909925070-1301 1,2-Dibromo-3-chloropropane (DBCP)62 09/16/2010 09091255070-1301 Dibromochloromethane 58 09/16/2010 09091165074-1341 1,2-Dibromoethane (EDB)52 09/16/2010 09091055070-1301 1,4-Dichlorobenzene 49 09/16/2010 0909995070-1301 1,2-Dichlorobenzene 51 09/16/2010 09091035070-1301 1,3-Dichlorobenzene 51 09/16/2010 09091025070-1301 Dichlorodifluoromethane 30 09/16/2010 0909605010-1581 1,2-Dichloroethane 49 09/16/2010 0909975059-1431 1,1-Dichloroethane 48 09/16/2010 0909965069-1321 cis-1,2-Dichloroethene 50 09/16/2010 0909995070-1301 trans-1,2-Dichloroethene 49 09/16/2010 0909985067-1411 1,1-Dichloroethene 48 09/16/2010 0909965050-1321 1,2-Dichloropropane 47 09/16/2010 0909935071-1261 trans-1,3-Dichloropropene 50 09/16/2010 0909995073-1311 cis-1,3-Dichloropropene 52 09/16/2010 09091035069-1301 Ethylbenzene 53 09/16/2010 09091055079-1321 2-Hexanone 110 09/16/2010 090911510060-1401 Isopropylbenzene 56 09/16/2010 09091125070-1301 Methyl acetate 55 09/16/2010 09091105015-1281 Methyl tertiary butyl ether (MTBE)55 09/16/2010 09091095060-1401 4-Methyl-2-pentanone 110 09/16/2010 090911010060-1401 Methylcyclohexane 51 09/16/2010 09091025070-1301 Methylene chloride 45 09/16/2010 0909905069-1291 Styrene 52 09/16/2010 09091045070-1301 1,1,2,2-Tetrachloroethane 53 09/16/2010 09091055060-1551 Tetrachloroethene 51 09/16/2010 09091025070-1301 Toluene 50 09/16/2010 09091005075-1251 1,1,2-Trichloro-1,2,2-Trifluoroethane 49 09/16/2010 0909975070-1301 1,2,4-Trichlorobenzene 54 09/16/2010 09091075070-1301 1,1,2-Trichloroethane 50 09/16/2010 09091005077-1321 1,1,1-Trichloroethane 53 09/16/2010 09091055077-1321 Note:Calculations are performed before rounding to avoid round-off errors in calculated results PQL = Practical quantitation limit ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" J = Estimated result < PQL and > MDL N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + - RPD is out of criteria_ Page: 14 of 17 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS - LCS Batch:Prep Method: Sample ID:LQ42492-002 42492 5030B Analytical Method:8260B Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/L)(ug/L) Trichloroethene 49 09/16/2010 0909995073-1241 Trichlorofluoromethane 44 09/16/2010 0909885041-1731 Vinyl chloride 42 09/16/2010 0909835029-1591 Xylenes (total)110 09/16/2010 090910810070-1301 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 99 70-130 1,2-Dichloroethane-d4 97 70-130 Toluene-d8 96 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results PQL = Practical quantitation limit ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" J = Estimated result < PQL and > MDL N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + - RPD is out of criteria_ Page: 15 of 17 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS - LCSD Batch:Prep Method: Sample ID:LQ42492-003 42492 5030B Analytical Method:8260B Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date% RPD % Rec Limit % RPD LimitDil(ug/L)(ug/L) Acetone 120 09/16/2010 093112110046-1536.7 201 Benzene 48 09/16/2010 0931975072-1270.16 201 Bromodichloromethane 51 09/16/2010 09311015071-1430.13 201 Bromoform 55 09/16/2010 09311115065-1315.4 201 Bromomethane (Methyl bromide)47 09/16/2010 0931935036-1681.2 201 2-Butanone (MEK)120 09/16/2010 093111610060-1406.3 201 Carbon disulfide 47 09/16/2010 0931955060-1400.61 201 Carbon tetrachloride 54 09/16/2010 09311075037-1660.0093 201 Chlorobenzene 50 09/16/2010 09311005078-1291.0 201 Chloroethane 43 09/16/2010 0931875042-1632.8 201 Chloroform 48 09/16/2010 0931975063-1230.25 201 Chloromethane (Methyl chloride)35 09/16/2010 0931705020-1580.50 201 Cyclohexane 46 09/16/2010 0931925070-1300.48 201 1,2-Dibromo-3-chloropropane (DBCP)56 09/16/2010 09311125070-13010 201 Dibromochloromethane 57 09/16/2010 09311145074-1341.1 201 1,2-Dibromoethane (EDB)52 09/16/2010 09311035070-1301.5 201 1,4-Dichlorobenzene 49 09/16/2010 0931995070-1300.039 201 1,2-Dichlorobenzene 51 09/16/2010 09311025070-1300.86 201 1,3-Dichlorobenzene 51 09/16/2010 09311015070-1300.47 201 Dichlorodifluoromethane 30 09/16/2010 0931615010-1582.1 201 1,2-Dichloroethane 48 09/16/2010 0931965059-1430.80 201 1,1-Dichloroethane 48 09/16/2010 0931965069-1320.46 201 cis-1,2-Dichloroethene 50 09/16/2010 09311005070-1300.10 201 trans-1,2-Dichloroethene 49 09/16/2010 0931995067-1410.23 201 1,1-Dichloroethene 49 09/16/2010 0931985050-1322.4 201 1,2-Dichloropropane 47 09/16/2010 0931955071-1261.7 201 trans-1,3-Dichloropropene 49 09/16/2010 0931995073-1310.17 201 cis-1,3-Dichloropropene 52 09/16/2010 09311045069-1300.52 201 Ethylbenzene 53 09/16/2010 09311055079-1320.23 201 2-Hexanone 110 09/16/2010 093110710060-1407.1 201 Isopropylbenzene 55 09/16/2010 09311115070-1300.58 201 Methyl acetate 52 09/16/2010 09311055015-1285.0 201 Methyl tertiary butyl ether (MTBE)54 09/16/2010 09311075060-1401.5 201 4-Methyl-2-pentanone 100 09/16/2010 093110310060-1407.0 201 Methylcyclohexane 52 09/16/2010 09311035070-1301.1 201 Methylene chloride 45 09/16/2010 0931905069-1290.17 201 Styrene 52 09/16/2010 09311045070-1300.061 201 1,1,2,2-Tetrachloroethane 51 09/16/2010 09311025060-1552.8 201 Tetrachloroethene 51 09/16/2010 09311035070-1300.76 201 Toluene 50 09/16/2010 09311015075-1250.26 201 1,1,2-Trichloro-1,2,2-Trifluoroethane 50 09/16/2010 0931995070-1302.1 201 1,2,4-Trichlorobenzene 54 09/16/2010 09311075070-1300.099 201 1,1,2-Trichloroethane 49 09/16/2010 0931995077-1321.5 201 1,1,1-Trichloroethane 53 09/16/2010 09311055077-1320.24 201 Note:Calculations are performed before rounding to avoid round-off errors in calculated results PQL = Practical quantitation limit ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" J = Estimated result < PQL and > MDL N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + - RPD is out of criteria_ Page: 16 of 17 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 Volatile Organic Compounds by GC/MS - LCSD Batch:Prep Method: Sample ID:LQ42492-003 42492 5030B Analytical Method:8260B Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date% RPD % Rec Limit % RPD LimitDil(ug/L)(ug/L) Trichloroethene 49 09/16/2010 0931985073-1240.67 201 Trichlorofluoromethane 44 09/16/2010 0931885041-1730.38 201 Vinyl chloride 42 09/16/2010 0931845029-1590.89 201 Xylenes (total)110 09/16/2010 093110810070-1300.15 201 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 99 70-130 1,2-Dichloroethane-d4 95 70-130 Toluene-d8 96 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results PQL = Practical quantitation limit ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" J = Estimated result < PQL and > MDL N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + - RPD is out of criteria_ Page: 17 of 17 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Level 1 Report v2.1